WS-5813_20918_CA_LTRRPT_20230905

S&ME, Inc. | 8646 W Market St, Ste 105 | Greensboro, NC 27409 | p 336.288.7180 | www.smeinc.com

September 5, 2023
High Falls Oil Company
P.O. Box 1360
Robbins, NC 27325
Attention: Mr. Steven Majors

Reference: Report of Limited Groundwater Assessment
Eskimo Joes/Incident #20918/UST #WS-5813
1705 Cotton Grove Road, Lexington, Davidson County, North Carolina
S&ME Project No. 1584-02-045F

Dear Mr. Majors:
S&ME, Inc. (S&ME) submits this Letter Report for the above-referenced site in accordance with S&ME’s Proposal
No. 22380059A, dated April 26, 2023. This work was performed at the request of the North Carolina Department
of Environmental Quality (NCDEQ) as pre-approved under Task Authorization No. 20918-17 and signed by the
Trust Fund Section of the Central Office on April 26, 2023.
The scope of services included the following tasks. Measure depth to water and collect groundwater samples
from monitoring wells MW-1 and MW-2 for analyses by Method 6200B and by Method 504.1. Submit a letter
report. Tasks were completed as proposed.
Current Site Assessment Information
Current Liquid Levels
On August 18, 2023, S&ME measured the depth to groundwater from the top of casing in monitoring wells MW-1
and MW-2 using an electronic water level indicator. The depth-to-water measurements ranged from 17.99 feet
below top of casing (ft-BTOC) in monitoring well MW-1 to 17.75 ft-BTOC in monitoring well MW-2. Compared to
the previous sampling event performed during February 2023, groundwater occurrence in monitoring wells MW-1
and MW-2 decreased approximately 3.5 feet in elevation. The depth to groundwater measurements and relative
groundwater elevations are provided in Table 1.
Groundwater Monitoring Event
On August 18, 2023, after measuring the depth-to-water, S&ME personnel purged monitoring wells MW-1 and
MW-2, using disposable polyethylene bailers of approximately three well volumes. Field parameters pH, specific
conductivity and temperature were measured during the well purging process and recorded on the groundwater
sampling forms, which are included in Attachment I. After completing the well purging, S&ME personnel
collected groundwater samples from monitoring wells MW-1 and MW-2.
OHL OHL OHL OHL OHL OHL OHL OHL OHL OHL OHL OHL OHL
OHL
OHL
OHL
OHL
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
OH
L
C C C C C C C C C C VVVVVVV
OHL
OHL
OHL
OHL
OHL
OHL
OHL
OHL
OHL
OHL
OHL
OHL
OHL
OHL
OHL
OHL
OHL
WLWLWLWLWLWLWLWLWLWLWLWLWL
WL
WL
WL
WL
WL
NG
NG
NG
NG
NG
NG
NG
NG
NG
NG
NG
NG
NG
NGNGNGNGNGNGNGNGNGNGNG
x x x x x
x
x
x
x
x
xxxxx
x
x
x
x
x
SVE-2
NC

H
I
G
H
W
A
Y

8

-

C
O
T
T
O
N

G
R
O
V
E

R
O
A
D
ES
K
I
M
O

J
O
E
'
S
ASPHALT
TEMPORARY FENCING
- MONITORING WELL LOCATION
- OVERHEAD UTILITY LINE
- VENT LINE
- CATHODIC PROTECTION
- CONDUITS
- WATER LINE
- LEXINGTON UTILITIES ELECTRICAL POLE
V
C
WL
OHL
CA
N
O
P
Y
APPROXIMATE PROPERTY BOUNDARY
MW-3
MW-2
MW-4
MW-1
RI
G
H
T
-
O
F
-
W
A
Y
- WATER SAMPLE LOCATION
NG - NATURAL GAS LINE
P1
DW-1
ALL LOCATIONS SHOWN ARE APPROXIMATE
NOTE
MW-5
MW-6
KEY
JIMMY'S BBQ
APPROXIMATE EXTENT OF NEW ISLAND
SVE-1
AS-1
AS-2
- PROPOSED SOIL VAPOR EXTRACTION WELL LOCATION
- PROPOSED AIR SPARGE WELL LOCATION
- 2" DEDICATED PVC AIR SPARGE CHASE PIPE
- 3" PVC SVE PIPE
APPROXIMATE
EQUIPMENT
LOCATION
AS-3
FIGURE NO.
Dr
a
w
i
n
g

p
a
t
h
:

Z:\
S
h
a
r
e
d
\
S
M
E
\
R
e
s
o
u
r
c
e
\
C
A
D
D
a
t
a
\
G
r
e
e
n
s
b
o
r
o
\
1
5
8
4
\
2
0
0
2
\
0
2
-
0
4
5

-

E
S
K
I
M
O

J
O
E
S
\
D
\
E
s
k
i
m
o

J
o
e
s

F
i
g
s
.
d
w
g
PROJECT NUMBER
DATE:
SCALE:
0 10 20
(IN FEET)GRAPHIC SCALE (IN FEET)GRAPHIC SCALE
ES
K
I
M
O

J
O
E
'
S
17
0
5

C
O
T
T
O
N

G
R
O
V
E

R
O
A
D
LE
X
I
N
G
T
O
N
,

N
O
R
T
H

C
A
R
O
L
I
N
A
GR
O
U
N
D
W
A
T
E
R

S
A
M
P
L
I
N
G

R
E
S
U
L
T
S

M
A
P
In
c
i
d
e
n
t

N
o
.

2
0
9
1
8
AS SHOWN
- GROSS CONTAMINATION LEVELSGCL
(NS)
(NS)
(NS)(NS)
(ALL<GCL)
(ALL<GCL)
(NS)
TANK #1
TANK #2
TANK #3
NOTES
DATE: 10/23/2020
METHODS: 6200B, 504.1
- NOT SAMPLEDNS
N
1
August 2023
1584-02-045F
Well I.D.
Installation Date
Total Depth1
Top of Casing Elevation
Casing Diameter
Consultant
Screen Interval Depth1
Date DTW GWE DTW GWE DTW GWE DTW GWE DTW GWE DTW GWE DTW GWE
06/25/02 23.35 77.26 23.68 77.07 23.43 77.19 22.91 76.59 NI -NI -NI -
09/27/02 25.11 75.50 25.17 75.58 24.96 75.66 23.43 76.07 25.55 76.06 23.08 76.41 24.86 74.92
08/21/07 21.01 79.60 20.95 79.80 21.16 79.46 19.98 79.52 20.97 80.64 20.41 79.08 22.04 77.74
07/20/12 17.67 82.94 17.73 83.02 17.72 12.48 17.92 11.88 17.97 12.03 15.70 14.30 15.90 54.10
05/05/14 12.82 87.79 12.82 87.93 NG NG NG NG NG NG NG NG 13.33 86.45
07/23/15 21.43 79.18 21.42 79.33 NG NG NG NG NG NG NG NG 22.46 77.32
06/30/17 14.79 85.82 15.01 85.74 NG NG NG NG NG NG NG NG NG NG
07/07/17 14.59 86.02 15.61 85.14 NG NG NG NG NG NG NG NG NG NG
10/07/17 24.91 75.70 28.58 72.17 NG NG NG NG NG NG NG NG NG NG
11/15/17 19.16 81.45 18.39 82.36 NG NG NG NG NG NG NG NG NG NG
12/12/17 23.72 76.89 22.32 78.43 NG NG NG NG NG NG NG NG NG NG
07/03/18 18.33 82.28 18.33 82.42 NG NG NG NG NG NG NG NG NG NG
10/15/20 12.71 87.90 12.70 88.05 12.44 88.18 11.20 88.30 13.03 88.58 9.49 90.00 12.61 87.17
10/23/20 12.91 87.70 12.92 87.83 NG NG NG NG NG NG NG NG NG NG
02/17/23 14.31 86.30 14.43 86.32 NG NG NG NG NG NG NG NG NG NG
08/18/23 17.99 82.62 17.75 83.00 NG NG NG NG NG NG NG NG NG NG
Notes: All measurements are in feet
DTW = Depth to groundwater measured from the top of casing
GWE = Groundwater elevation
NI = Monitor well had not been installed at the time of data collection
NG = Not gauged
1 Depth below ground surface in feet
2-inch
9/10/2002
DW-1
7/3/2002
70.0
99.7899.49
MW-1
27.1
100.61
30.0
101.61
9/10/2002
MW-3
30.2
6/26/2002
99.50
6/25/2002
MW-2
28.8
100.75 100.62
6/26/2002
2-inch 2-inch 2-inch
6/25/2002
S&ME S&ME S&ME
15.3 - 29.8 15 - 3012.6 - 27.1 14.3 - 28.8 15.8 - 30.2 65 - 70
MW-4 MW-5 MW-6
S&ME S&ME
15 - 30
29.8
2-inch 2-inch
S&ME S&ME
30.0
2-inch
S&ME PROJECT NO. 1584-02-045F
TABLE 1
MONITOR WELL / GROUNDWATER ELEVATION DATA
ESKIMO JOE'S; INCIDENT No.: 20918
1705 COTTON GROVE ROAD, LEXINGTON, NORTH CAROLINA
Updated August 29, 2023
Date
Collected Be
n
z
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
To
l
u
e
n
e
Xy
l
e
n
e
s

(
t
o
t
a
l
)
Ch
l
o
r
o
f
o
r
m
1,2

D
i
b
r
o
m
o
e
t
h
a
n
e

(
E
D
B
)
1,2
-
D
i
c
h
l
o
r
o
e
t
h
a
n
e
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e

1,2
,
3
-
T
r
i
c
h
l
o
r
o
p
r
o
p
a
n
e
Dii
s
o
p
r
o
p
y
l

e
t
h
e
r
Me
t
h
y
l

t
e
r
t
-
b
u
t
y
l

e
t
h
e
r
Na
p
h
t
h
a
l
e
n
e
1,2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1,3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
Te
t
r
a
c
h
l
o
r
o
e
t
h
e
n
e
te
r
t
-
A
m
y
l

A
l
c
o
h
o
l
te
r
t
-
A
m
y
l

m
e
t
h
y
l

e
t
h
e
r
te
r
t
-
B
u
t
y
l

A
l
c
o
h
o
l
n-
P
r
o
p
y
l

B
e
n
z
e
n
e
Well ID Method 602/6200B 6200B 6200B 6200B 6200B 6200B 6200B 6200B 6200B 6200B 6200B 6200B 6200B 6200B 6200B 6200B 6200B 6200B 6200B
MW-1 7/23/2015 14,000 1,510 26,600 12,660 541 67.0 125 <50.0 NR 757 11,600 580 1,480 381 ND NR NR NR NR
10/7/2017 12,700 1,210 26,000 16,280 NR NR NR <250 NR 881 12,600 571 NR NR ND NR NR NR NR
11/15/2017 6,500 <500 7,400 18,500 NR NR NR NR NR <250 15,400 NR NR NR ND NR NR NR NR
12/12/2017 3,650 590 6,420 18,100 <250 19.6 <250 <250 <250 1,080 19,700 640 3,420 1,900 ND NR NR NR NR
7/3/2018 5,580 1,890 19,000 18,080 <62.5 111*134 75.6 <62.5 582 9,300 522 2,920 <62.5 ND NR NR NR NR
10/23/2020 1,270 1,200 630 1,261 21.2 12.0*22.5 68.9 20.2 76 2,400 843 577 478 ND NR NR NR NR
2/17/2023 2,680 1,820 2250 2,920 <10.0 3.7*20.9 69.9 <10.0 124 3,010 738 903 322 <10.0 12,600 345 2560 203
8/18/2023 1,130 1,060 4,470 10,210 31.9 7.7*37.3 51.7 <20.0 35.4 1,200 640 1,940 541 <20.0 NR NR NR 141
MW-2 7/23/2015 9,700 2,650 29,900 18,960 274 <100 109 <100 NR 382 3,330 458 2,190 668 ND NR NR NR NR
11/15/2017 1.9 <250 2.0 2.8 NR NR NR NR NR 6.0 321 NR NR NR ND NR NR NR NR
12/12/2017 8.88 24.6 2.97 177 <0.5 0.50 <0.5 1.55 <250 3.08 186 12.3 73 49 ND NR NR NR NR
7/3/2018 26.4 146 518 2,490 <5.0 0.16*<5.0 11.6 <5.0 <5.0 115 75.1 478 <5.0 ND NR NR NR NR
10/23/2020 444 460 2,210 6,040 27.3 6.4*21.5 35.9 <12.5 19.5 520 566 1,630 <12.5 ND NR NR NR NR
2/17/2023 552 482 2,170 5,290 29.1 4.0*23.6 22.8 <6.2 17.8 506 285 887 269 <6.2 11600 <125 1220 56.4
8/18/2023 1,670 2,090 2,900 4,110 <12.5 5.2*19.3 89.1 <12.5 80.0 2,360 903 1,380 533 <12.5 NR NR NR 268
W-14 2/17/2023 <0.50 <0.50 <0.50 <0.50 <0.50 <0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 0.58 <100 <10.0 <50.0 <0.50
1 600 600 500 70 0.02 0.4 70 0.005 70 20 6 400 400 0.7 40 128 10 70
5,000 80,000 260,000 50,000 70,000 50 400 30,500
No
Standard 70,000 20,000 6,000 28,500 24,100 700 40,000 128,000 10,000 26,100
Notes
Concentrations shown in microgram per liter (parts per billion).
Only compounds detected by analyses are shown.
Concentrations in bold exceed the corresponding 2L Groundwater Standard
Shaded cells indicate concentrations greater than the corresponding NCDEQ Gross Contamination Levels (GCLs)
< = Below the noted report limit
NR = Not Requested
ND = Not Detected
* Analyzed by Method 504.1
Updated 8/30/2023
Gross Contamination
Levels (GCLs)
Table 2
1705 Cotton Grove Road, Lexington, North Carolina
S&ME Project No. 1584-02-045F
2L Groundwater Quality
Standard (2L Standards)
Summary of 2015-2023 Groundwater Analytical Results
Eskimo Joe's; Incident No.: 20918
T:\Greensboro-1580\Projects\2002\1584-02-045 Eskimo Joes\045F_Eskimos Joes_Monitoring August 2023\REPORT\Tables 1-2-3__2023.xlsx

Attachment I – Groundwater Sampling Forms and Environmental
Field Reports
° F
Date Time
8/18/23 09:00 4.0 10.0
8/18/23 09:00 µS/cm
17.99 ft-TOC inch
27.20 ft-TOC gal
9.21 feet gal
ft-GRD gal
ft-GRD
End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
09:30 6.2 22.6 131 1.0
09:45
Qty Container Pres.Qty Pres.
4 40mL VOAs HCl
3 40mL VOAs NaS2O3
(1)
Notes:
Form Revision Date:
Purge Time (Min.):
GROUNDWATER SAMPLING FORM
Project Name:
Project Location:
Project Number:
Source Well:
Eskimo Joe's
Lexington, NC
1584-02-045E
MW-1
Purge Date:August 18, 2023
VOCs 6200
EDB 504.1
Analytical Data
Method Method
9/13/17 8:00 AM
Name Signature
Gary Simcox
Date
8/18/2023
Container
Sample Method:Sample Time:Bailer
5.0 Petroleum Odors
Total Volume Purged:5.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
(Gal)
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:
Total Well Depth:Well Volume
Height of Water Column:3 * Well Volume
Screen Length:5 * Well Volume
1.5
4.5
7.5
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter
Conductivity 1,413 1,413
7.0
µS/cm
2
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
pH 4.00, 7.00, 10.00
Air Temp:
August 18, 2023
85
09:45Sample Time:
Sample Date:
Weather:
Locked?:
Sampled By:
Yes
Gary Simcox
Sunny
° F
Date Time
8/18/23 09:00 4.0 10.0
8/18/23 09:00 µS/cm
17.75 ft-TOC inch
29.10 ft-TOC gal
11.35 feet gal
ft-GRD gal
ft-GRD
End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
10:25 6.4 21.9 400 1.0
10:40
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
3 40mL VOAs NaS2O3
(1)
Notes:
Form Revision Date:
Gary Simcox 8/18/2023
9/13/17 8:00 AM
Name Signature Date
EDB 504.1
Analytical Data
Method Method Container
VOCs 6200
Sample Method:Bailer Sample Time:
(Gal)
6.0 Petroleum Odors
Total Volume Purged:6.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 9.3
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:
Total Well Depth:Well Volume 1.9
Height of Water Column:3 * Well Volume 5.6
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Weather:Sunny Air Temp:85
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:August 18, 2023
Sampled By:Gary Simcox Sample Time:10:40
Project Number:1584-02-045B Purge Date:August 18, 2023
Source Well:MW-2 Purge Time (Min.):
GROUNDWATER SAMPLING FORM
Project Name:Eskimo Joe's
Project Location:Lexington, NC

Hours Mileage Signature of S&ME Personnel
3.5 90

S&ME, Inc. | www.smeinc.com
Environmental Field Report
Date:
August 18, 2023
Job Number:
1584-02-045E
Project Name:
Eskimo Joe’s
Weather/Temperature:
Sunny, 85°F
Project Location:
Lexington, NC
Notes By:
☒
Present at the Site:
Gary Simcox
☐

On site to purge and sample MW-1 and MW-2.
After arriving on site, I opened both wells to allow liquid levels to equilibrate before taking depth to water
measurements. After letting the wells sit for approximately 10-15 minutes, I began measuring DTW.
After taking DTW measurements, I began purging and sampling MW-1 and MW-2. I collected both
samples after purging each well of at least 3 volumes. Each collected sample was placed in a laboratory
supplied container. After sampling MW-1 and MW-2, I closed both wells.

I stored the samples in a cooler on ice as they were collected. The samples were delivered to Pace
Laboratories in Kernersville, NC.
Equipment Used
Bailers and string
pH / conductivity meter
Water level meter

Attachment II – Laboratory Report and Chain-of-Custody Form

#=CL#
August 24, 2023
LIMS USE: FR - ED HENRIQUES
LIMS OBJECT ID: 92683440
92683440
Project:
Pace Project No.:
RE:
Mr. Ed Henriques
S&ME, Inc.
8646 West Market Street
Suite 105
Greensboro, NC 27409
Eskimo Joes
Dear Mr. Henriques:
Enclosed are the analytical results for sample(s) received by the laboratory on August 18, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc:Cody McMechen
Cody McMechen, S+ME
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 30
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92683440
Eskimo Joes
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 30
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92683440
Eskimo Joes
Lab ID Sample ID Matrix Date Collected Date Received
92683440001 MW-1 Water 08/18/23 09:45 08/18/23 11:25
92683440002 MW-2 Water 08/18/23 10:40 08/18/23 11:25
92683440003 Trip Blank Water 08/18/23 00:00 08/18/23 11:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 30
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92683440
Eskimo Joes
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92683440001 MW-1 EPA 504.1 4 PASI-CHH
SM 6200B 63 PASI-CSAS
92683440002 MW-2 EPA 504.1 4 PASI-CHH
SM 6200B 63 PASI-CSAS
92683440003 Trip Blank SM 6200B 63 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 30
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92683440
Eskimo Joes
Method:
Client:S&ME - Greensboro
EPA 504.1
Date:August 24, 2023
Description:504 GCS EDB and DBCP
General Information:
2 samples were analyzed for EPA 504.1 by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 504.1 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: 795052
S4: Surrogate recovery not evaluated against control limits due to sample dilution.
• MW-1 (Lab ID: 92683440001)
• 1-Chloro-2-bromopropane (S)
• MW-2 (Lab ID: 92683440002)
• 1-Chloro-2-bromopropane (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
QC Batch: 795052
D6: The precision between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID: 4119668)
• 1,2-Dibromoethane (EDB)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 30
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92683440
Eskimo Joes
Method:
Client:S&ME - Greensboro
EPA 504.1
Date:August 24, 2023
Description:504 GCS EDB and DBCP
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 30
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92683440
Eskimo Joes
Method:
Client:S&ME - Greensboro
SM 6200B
Date:August 24, 2023
Description:6200B MSV
General Information:
3 samples were analyzed for SM 6200B by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 795157
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92683720001
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 4120105)
• 1,1-Dichloroethene
• 1,1-Dichloropropene
• Chloroethane
• Dichlorodifluoromethane
• MSD (Lab ID: 4120106)
• 1,1-Dichloroethene
• 1,1-Dichloropropene
• Chloroethane
• Dichlorodifluoromethane
• Trichlorofluoromethane
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 30
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92683440
Eskimo Joes
Method:
Client:S&ME - Greensboro
SM 6200B
Date:August 24, 2023
Description:6200B MSV
QC Batch: 795384
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92683609002
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 4121183)
• 1,1-Dichloroethane
• 1,1-Dichloroethene
• 1,1-Dichloropropene
• 1,2-Dichloropropane
• Benzene
• Chloroethane
• Dichlorodifluoromethane
• Diisopropyl ether
• Trichlorofluoromethane
• trans-1,2-Dichloroethene
• MSD (Lab ID: 4121184)
• 1,1-Dichloroethene
• 1,1-Dichloropropene
• 1,2-Dichloropropane
• Bromomethane
• Chloroethane
• Dichlorodifluoromethane
• Trichlorofluoromethane
• n-Butylbenzene
• trans-1,2-Dichloroethene
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683440
Eskimo Joes
Sample:MW-1 Lab ID:92683440001 Collected:08/18/23 09:45 Received:08/18/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1
Pace Analytical Services - Charlotte
504 GCS EDB and DBCP
1,2-Dibromo-3-chloropropane <0.51 ug/L 08/23/23 13:21 96-12-808/22/23 11:490.51 0.048 10
1,2-Dibromoethane (EDB)7.7 ug/L 08/23/23 13:21 106-93-408/22/23 11:490.20 0.057 10
1,2,3-Trichloropropane <0.51 ug/L 08/23/23 13:21 96-18-408/22/23 11:490.51 0.10 10
Surrogates
1-Chloro-2-bromopropane (S)0 %08/23/23 13:21 301-79-56 S408/22/23 11:4970-130 10
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 1130 ug/L 08/23/23 15:00 71-43-220.0 3.1 40
Bromobenzene <20.0 ug/L 08/23/23 15:00 108-86-120.0 5.4 40
Bromochloromethane <20.0 ug/L 08/23/23 15:00 74-97-520.0 3.8 40
Bromodichloromethane <20.0 ug/L 08/23/23 15:00 75-27-420.0 6.8 40
Bromoform <20.0 ug/L 08/23/23 15:00 75-25-220.0 7.9 40
Bromomethane <200 ug/L 08/23/23 15:00 74-83-92008.9 40
n-Butylbenzene <20.0 ug/L 08/23/23 15:00 104-51-820.0 2.7 40
sec-Butylbenzene <20.0 ug/L 08/23/23 15:00 135-98-820.0 3.4 40
tert-Butylbenzene <20.0 ug/L 08/23/23 15:00 98-06-620.0 3.4 40
Carbon tetrachloride <20.0 ug/L 08/23/23 15:00 56-23-520.0 6.8 40
Chlorobenzene <20.0 ug/L 08/23/23 15:00 108-90-720.0 3.4 40
Chloroethane <40.0 ug/L 08/23/23 15:00 75-00-340.0 6.9 40
Chloroform 31.9 ug/L 08/23/23 15:00 67-66-320.0 2.8 40
Chloromethane <40.0 ug/L 08/23/23 15:00 74-87-340.0 7.0 40
2-Chlorotoluene <20.0 ug/L 08/23/23 15:00 95-49-820.0 5.2 40
4-Chlorotoluene <20.0 ug/L 08/23/23 15:00 106-43-420.0 3.8 40
1,2-Dibromo-3-chloropropane <40.0 ug/L 08/23/23 15:00 96-12-840.0 7.2 40
Dibromochloromethane <20.0 ug/L 08/23/23 15:00 124-48-120.0 5.9 40
1,2-Dibromoethane (EDB)<20.0 ug/L 08/23/23 15:00 106-93-420.0 5.9 40
Dibromomethane <20.0 ug/L 08/23/23 15:00 74-95-320.0 7.5 40
1,2-Dichlorobenzene <20.0 ug/L 08/23/23 15:00 95-50-120.0 3.8 40
1,3-Dichlorobenzene <20.0 ug/L 08/23/23 15:00 541-73-120.0 3.9 40
1,4-Dichlorobenzene <20.0 ug/L 08/23/23 15:00 106-46-720.0 3.6 40
Dichlorodifluoromethane <20.0 ug/L 08/23/23 15:00 75-71-820.0 4.9 40
1,1-Dichloroethane <20.0 ug/L 08/23/23 15:00 75-34-320.0 2.2 40
1,2-Dichloroethane 37.3 ug/L 08/23/23 15:00 107-06-220.0 4.2 40
1,1-Dichloroethene <20.0 ug/L 08/23/23 15:00 75-35-420.0 3.1 40
cis-1,2-Dichloroethene <20.0 ug/L 08/23/23 15:00 156-59-220.0 4.4 40
trans-1,2-Dichloroethene <20.0 ug/L 08/23/23 15:00 156-60-520.0 4.0 40
1,2-Dichloropropane <20.0 ug/L 08/23/23 15:00 78-87-520.0 5.4 40
1,3-Dichloropropane <20.0 ug/L 08/23/23 15:00 142-28-920.0 3.4 40
2,2-Dichloropropane <20.0 ug/L 08/23/23 15:00 594-20-720.0 4.9 40
1,1-Dichloropropene <20.0 ug/L 08/23/23 15:00 563-58-620.0 2.6 40
cis-1,3-Dichloropropene <20.0 ug/L 08/23/23 15:00 10061-01-520.0 3.6 40
trans-1,3-Dichloropropene <20.0 ug/L 08/23/23 15:00 10061-02-620.0 5.3 40
Diisopropyl ether 35.4 ug/L 08/23/23 15:00 108-20-320.0 2.9 40
Ethylbenzene 1060 ug/L 08/23/23 15:00 100-41-420.0 3.2 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2023 01:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683440
Eskimo Joes
Sample:MW-1 Lab ID:92683440001 Collected:08/18/23 09:45 Received:08/18/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Hexachloro-1,3-butadiene <80.0 ug/L 08/23/23 15:00 87-68-380.0 14.0 40
Isopropylbenzene (Cumene)51.7 ug/L 08/23/23 15:00 98-82-820.0 4.2 40
Methylene Chloride <80.0 ug/L 08/23/23 15:00 75-09-280.0 75.6 40
Methyl-tert-butyl ether 1200 ug/L 08/23/23 15:00 1634-04-420.0 2.1 40
Naphthalene 640 ug/L 08/23/23 15:00 91-20-380.0 4.0 40
n-Propylbenzene 141 ug/L 08/23/23 15:00 103-65-120.0 4.2 40
Styrene <20.0 ug/L 08/23/23 15:00 100-42-520.0 5.5 40
1,1,1,2-Tetrachloroethane <20.0 ug/L 08/23/23 15:00 630-20-620.0 3.6 40
1,1,2,2-Tetrachloroethane <20.0 ug/L 08/23/23 15:00 79-34-520.0 3.0 40
Tetrachloroethene <20.0 ug/L 08/23/23 15:00 127-18-420.0 3.4 40
Toluene 4470 ug/L 08/23/23 15:00 108-88-320.0 3.6 40
1,2,3-Trichlorobenzene <80.0 ug/L 08/23/23 15:00 87-61-680.0 4.8 40
1,2,4-Trichlorobenzene <80.0 ug/L 08/23/23 15:00 120-82-180.0 6.2 40
1,1,1-Trichloroethane <20.0 ug/L 08/23/23 15:00 71-55-620.0 4.3 40
1,1,2-Trichloroethane <20.0 ug/L 08/23/23 15:00 79-00-520.0 3.8 40
Trichloroethene <20.0 ug/L 08/23/23 15:00 79-01-620.0 6.8 40
Trichlorofluoromethane <40.0 ug/L 08/23/23 15:00 75-69-440.0 5.8 40
1,2,3-Trichloropropane <20.0 ug/L 08/23/23 15:00 96-18-420.0 6.9 40
1,2,4-Trimethylbenzene 1940 ug/L 08/23/23 15:00 95-63-620.0 1.2 40
1,3,5-Trimethylbenzene 541 ug/L 08/23/23 15:00 108-67-820.0 2.9 40
Vinyl chloride <40.0 ug/L 08/23/23 15:00 75-01-440.0 6.0 40
m&p-Xylene 6490 ug/L 08/23/23 15:00 179601-23-140.0 3.7 40
o-Xylene 3720 ug/L 08/23/23 15:00 95-47-620.0 5.8 40
Surrogates
1,2-Dichloroethane-d4 (S)106 %08/23/23 15:00 17060-07-070-130 40
4-Bromofluorobenzene (S)96 %08/23/23 15:00 460-00-470-130 40
Toluene-d8 (S)96 %08/23/23 15:00 2037-26-570-130 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2023 01:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683440
Eskimo Joes
Sample:MW-2 Lab ID:92683440002 Collected:08/18/23 10:40 Received:08/18/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1
Pace Analytical Services - Charlotte
504 GCS EDB and DBCP
1,2-Dibromo-3-chloropropane <0.51 ug/L 08/23/23 13:31 96-12-808/22/23 11:490.51 0.048 10
1,2-Dibromoethane (EDB)5.2 ug/L 08/23/23 13:31 106-93-408/22/23 11:490.20 0.057 10
1,2,3-Trichloropropane <0.51 ug/L 08/23/23 13:31 96-18-408/22/23 11:490.51 0.099 10
Surrogates
1-Chloro-2-bromopropane (S)0 %08/23/23 13:31 301-79-56 S408/22/23 11:4970-130 10
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 1670 ug/L 08/23/23 14:42 71-43-212.5 2.0 25
Bromobenzene <12.5 ug/L 08/23/23 14:42 108-86-112.5 3.4 25
Bromochloromethane <12.5 ug/L 08/23/23 14:42 74-97-512.5 2.4 25
Bromodichloromethane <12.5 ug/L 08/23/23 14:42 75-27-412.5 4.2 25
Bromoform <12.5 ug/L 08/23/23 14:42 75-25-212.5 4.9 25
Bromomethane <125 ug/L 08/23/23 14:42 74-83-91255.6 25
n-Butylbenzene <12.5 ug/L 08/23/23 14:42 104-51-812.5 1.7 25
sec-Butylbenzene <12.5 ug/L 08/23/23 14:42 135-98-812.5 2.1 25
tert-Butylbenzene <12.5 ug/L 08/23/23 14:42 98-06-612.5 2.1 25
Carbon tetrachloride <12.5 ug/L 08/23/23 14:42 56-23-512.5 4.2 25
Chlorobenzene <12.5 ug/L 08/23/23 14:42 108-90-712.5 2.1 25
Chloroethane <25.0 ug/L 08/23/23 14:42 75-00-325.0 4.3 25
Chloroform <12.5 ug/L 08/23/23 14:42 67-66-312.5 1.7 25
Chloromethane <25.0 ug/L 08/23/23 14:42 74-87-325.0 4.4 25
2-Chlorotoluene <12.5 ug/L 08/23/23 14:42 95-49-812.5 3.2 25
4-Chlorotoluene <12.5 ug/L 08/23/23 14:42 106-43-412.5 2.4 25
1,2-Dibromo-3-chloropropane <25.0 ug/L 08/23/23 14:42 96-12-825.0 4.5 25
Dibromochloromethane <12.5 ug/L 08/23/23 14:42 124-48-112.5 3.7 25
1,2-Dibromoethane (EDB)<12.5 ug/L 08/23/23 14:42 106-93-412.5 3.7 25
Dibromomethane <12.5 ug/L 08/23/23 14:42 74-95-312.5 4.7 25
1,2-Dichlorobenzene <12.5 ug/L 08/23/23 14:42 95-50-112.5 2.4 25
1,3-Dichlorobenzene <12.5 ug/L 08/23/23 14:42 541-73-112.5 2.4 25
1,4-Dichlorobenzene <12.5 ug/L 08/23/23 14:42 106-46-712.5 2.2 25
Dichlorodifluoromethane <12.5 ug/L 08/23/23 14:42 75-71-812.5 3.1 25
1,1-Dichloroethane <12.5 ug/L 08/23/23 14:42 75-34-312.5 1.4 25
1,2-Dichloroethane 19.3 ug/L 08/23/23 14:42 107-06-212.5 2.6 25
1,1-Dichloroethene <12.5 ug/L 08/23/23 14:42 75-35-412.5 2.0 25
cis-1,2-Dichloroethene <12.5 ug/L 08/23/23 14:42 156-59-212.5 2.8 25
trans-1,2-Dichloroethene <12.5 ug/L 08/23/23 14:42 156-60-512.5 2.5 25
1,2-Dichloropropane <12.5 ug/L 08/23/23 14:42 78-87-512.5 3.4 25
1,3-Dichloropropane <12.5 ug/L 08/23/23 14:42 142-28-912.5 2.1 25
2,2-Dichloropropane <12.5 ug/L 08/23/23 14:42 594-20-712.5 3.0 25
1,1-Dichloropropene <12.5 ug/L 08/23/23 14:42 563-58-612.5 1.6 25
cis-1,3-Dichloropropene <12.5 ug/L 08/23/23 14:42 10061-01-512.5 2.2 25
trans-1,3-Dichloropropene <12.5 ug/L 08/23/23 14:42 10061-02-612.5 3.3 25
Diisopropyl ether 80.0 ug/L 08/23/23 14:42 108-20-312.5 1.8 25
Ethylbenzene 2090 ug/L 08/23/23 14:42 100-41-412.5 2.0 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2023 01:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683440
Eskimo Joes
Sample:MW-2 Lab ID:92683440002 Collected:08/18/23 10:40 Received:08/18/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Hexachloro-1,3-butadiene <50.0 ug/L 08/23/23 14:42 87-68-350.0 8.8 25
Isopropylbenzene (Cumene)89.1 ug/L 08/23/23 14:42 98-82-812.5 2.6 25
Methylene Chloride <50.0 ug/L 08/23/23 14:42 75-09-250.0 47.2 25
Methyl-tert-butyl ether 2360 ug/L 08/23/23 14:42 1634-04-412.5 1.3 25
Naphthalene 903 ug/L 08/23/23 14:42 91-20-350.0 2.5 25
n-Propylbenzene 268 ug/L 08/23/23 14:42 103-65-112.5 2.6 25
Styrene <12.5 ug/L 08/23/23 14:42 100-42-512.5 3.4 25
1,1,1,2-Tetrachloroethane <12.5 ug/L 08/23/23 14:42 630-20-612.5 2.3 25
1,1,2,2-Tetrachloroethane <12.5 ug/L 08/23/23 14:42 79-34-512.5 1.8 25
Tetrachloroethene <12.5 ug/L 08/23/23 14:42 127-18-412.5 2.1 25
Toluene 2900 ug/L 08/23/23 14:42 108-88-312.5 2.2 25
1,2,3-Trichlorobenzene <50.0 ug/L 08/23/23 14:42 87-61-650.0 3.0 25
1,2,4-Trichlorobenzene <50.0 ug/L 08/23/23 14:42 120-82-150.0 3.9 25
1,1,1-Trichloroethane <12.5 ug/L 08/23/23 14:42 71-55-612.5 2.7 25
1,1,2-Trichloroethane <12.5 ug/L 08/23/23 14:42 79-00-512.5 2.4 25
Trichloroethene <12.5 ug/L 08/23/23 14:42 79-01-612.5 4.3 25
Trichlorofluoromethane <25.0 ug/L 08/23/23 14:42 75-69-425.0 3.6 25
1,2,3-Trichloropropane <12.5 ug/L 08/23/23 14:42 96-18-412.5 4.3 25
1,2,4-Trimethylbenzene 1380 ug/L 08/23/23 14:42 95-63-612.5 0.77 25
1,3,5-Trimethylbenzene 533 ug/L 08/23/23 14:42 108-67-812.5 1.8 25
Vinyl chloride <25.0 ug/L 08/23/23 14:42 75-01-425.0 3.7 25
m&p-Xylene 1910 ug/L 08/23/23 14:42 179601-23-125.0 2.3 25
o-Xylene 2200 ug/L 08/23/23 14:42 95-47-612.5 3.6 25
Surrogates
1,2-Dichloroethane-d4 (S)107 %08/23/23 14:42 17060-07-070-130 25
4-Bromofluorobenzene (S)95 %08/23/23 14:42 460-00-470-130 25
Toluene-d8 (S)97 %08/23/23 14:42 2037-26-570-130 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2023 01:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683440
Eskimo Joes
Sample:Trip Blank Lab ID:92683440003 Collected:08/18/23 00:00 Received:08/18/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene <0.50 ug/L 08/22/23 12:55 71-43-20.50 0.079 1
Bromobenzene <0.50 ug/L 08/22/23 12:55 108-86-10.50 0.14 1
Bromochloromethane <0.50 ug/L 08/22/23 12:55 74-97-50.50 0.094 1
Bromodichloromethane <0.50 ug/L 08/22/23 12:55 75-27-40.50 0.17 1
Bromoform <0.50 ug/L 08/22/23 12:55 75-25-20.50 0.20 1
Bromomethane <5.0 ug/L 08/22/23 12:55 74-83-95.0 0.22 1
n-Butylbenzene <0.50 ug/L 08/22/23 12:55 104-51-80.50 0.066 1
sec-Butylbenzene <0.50 ug/L 08/22/23 12:55 135-98-80.50 0.085 1
tert-Butylbenzene <0.50 ug/L 08/22/23 12:55 98-06-60.50 0.086 1
Carbon tetrachloride <0.50 ug/L 08/22/23 12:55 56-23-50.50 0.17 1
Chlorobenzene <0.50 ug/L 08/22/23 12:55 108-90-70.50 0.085 1
Chloroethane <1.0 ug/L 08/22/23 12:55 75-00-31.0 0.17 1
Chloroform <0.50 ug/L 08/22/23 12:55 67-66-30.50 0.069 1
Chloromethane <1.0 ug/L 08/22/23 12:55 74-87-31.0 0.18 1
2-Chlorotoluene <0.50 ug/L 08/22/23 12:55 95-49-80.50 0.13 1
4-Chlorotoluene <0.50 ug/L 08/22/23 12:55 106-43-40.50 0.096 1
1,2-Dibromo-3-chloropropane <1.0 ug/L 08/22/23 12:55 96-12-81.0 0.18 1
Dibromochloromethane <0.50 ug/L 08/22/23 12:55 124-48-10.50 0.15 1
1,2-Dibromoethane (EDB)<0.50 ug/L 08/22/23 12:55 106-93-40.50 0.15 1
Dibromomethane <0.50 ug/L 08/22/23 12:55 74-95-30.50 0.19 1
1,2-Dichlorobenzene <0.50 ug/L 08/22/23 12:55 95-50-10.50 0.094 1
1,3-Dichlorobenzene <0.50 ug/L 08/22/23 12:55 541-73-10.50 0.098 1
1,4-Dichlorobenzene <0.50 ug/L 08/22/23 12:55 106-46-70.50 0.090 1
Dichlorodifluoromethane <0.50 ug/L 08/22/23 12:55 75-71-80.50 0.12 1
1,1-Dichloroethane <0.50 ug/L 08/22/23 12:55 75-34-30.50 0.056 1
1,2-Dichloroethane <0.50 ug/L 08/22/23 12:55 107-06-20.50 0.11 1
1,1-Dichloroethene <0.50 ug/L 08/22/23 12:55 75-35-40.50 0.079 1
cis-1,2-Dichloroethene <0.50 ug/L 08/22/23 12:55 156-59-20.50 0.11 1
trans-1,2-Dichloroethene <0.50 ug/L 08/22/23 12:55 156-60-50.50 0.10 1
1,2-Dichloropropane <0.50 ug/L 08/22/23 12:55 78-87-50.50 0.14 1
1,3-Dichloropropane <0.50 ug/L 08/22/23 12:55 142-28-90.50 0.085 1
2,2-Dichloropropane <0.50 ug/L 08/22/23 12:55 594-20-70.50 0.12 1
1,1-Dichloropropene <0.50 ug/L 08/22/23 12:55 563-58-60.50 0.066 1
cis-1,3-Dichloropropene <0.50 ug/L 08/22/23 12:55 10061-01-50.50 0.090 1
trans-1,3-Dichloropropene <0.50 ug/L 08/22/23 12:55 10061-02-60.50 0.13 1
Diisopropyl ether <0.50 ug/L 08/22/23 12:55 108-20-30.50 0.072 1
Ethylbenzene <0.50 ug/L 08/22/23 12:55 100-41-40.50 0.081 1
Hexachloro-1,3-butadiene <2.0 ug/L 08/22/23 12:55 87-68-32.0 0.35 1
Isopropylbenzene (Cumene)<0.50 ug/L 08/22/23 12:55 98-82-80.50 0.11 1
Methylene Chloride <2.0 ug/L 08/22/23 12:55 75-09-22.0 1.9 1
Methyl-tert-butyl ether <0.50 ug/L 08/22/23 12:55 1634-04-40.50 0.053 1
Naphthalene <2.0 ug/L 08/22/23 12:55 91-20-32.0 0.10 1
n-Propylbenzene <0.50 ug/L 08/22/23 12:55 103-65-10.50 0.10 1
Styrene <0.50 ug/L 08/22/23 12:55 100-42-50.50 0.14 1
1,1,1,2-Tetrachloroethane <0.50 ug/L 08/22/23 12:55 630-20-60.50 0.091 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2023 01:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683440
Eskimo Joes
Sample:Trip Blank Lab ID:92683440003 Collected:08/18/23 00:00 Received:08/18/23 11:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane <0.50 ug/L 08/22/23 12:55 79-34-50.50 0.074 1
Tetrachloroethene <0.50 ug/L 08/22/23 12:55 127-18-40.50 0.086 1
Toluene <0.50 ug/L 08/22/23 12:55 108-88-30.50 0.090 1
1,2,3-Trichlorobenzene <2.0 ug/L 08/22/23 12:55 87-61-62.0 0.12 1
1,2,4-Trichlorobenzene <2.0 ug/L 08/22/23 12:55 120-82-12.0 0.16 1
1,1,1-Trichloroethane <0.50 ug/L 08/22/23 12:55 71-55-60.50 0.11 1
1,1,2-Trichloroethane <0.50 ug/L 08/22/23 12:55 79-00-50.50 0.096 1
Trichloroethene <0.50 ug/L 08/22/23 12:55 79-01-60.50 0.17 1
Trichlorofluoromethane <1.0 ug/L 08/22/23 12:55 75-69-41.0 0.14 1
1,2,3-Trichloropropane <0.50 ug/L 08/22/23 12:55 96-18-40.50 0.17 1
1,2,4-Trimethylbenzene <0.50 ug/L 08/22/23 12:55 95-63-60.50 0.031 1
1,3,5-Trimethylbenzene <0.50 ug/L 08/22/23 12:55 108-67-80.50 0.071 1
Vinyl chloride <1.0 ug/L 08/22/23 12:55 75-01-41.0 0.15 1
m&p-Xylene <1.0 ug/L 08/22/23 12:55 179601-23-11.0 0.094 1
o-Xylene <0.50 ug/L 08/22/23 12:55 95-47-60.50 0.14 1
Surrogates
1,2-Dichloroethane-d4 (S)108 %08/22/23 12:55 17060-07-070-130 1
4-Bromofluorobenzene (S)93 %08/22/23 12:55 460-00-470-130 1
Toluene-d8 (S)96 %08/22/23 12:55 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2023 01:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683440
Eskimo Joes
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
795157
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683440003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4120088
Associated Lab Samples:92683440003
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.50 0.50 08/22/23 12:180.091
1,1,1-Trichloroethane ug/L <0.50 0.50 08/22/23 12:180.11
1,1,2,2-Tetrachloroethane ug/L <0.50 0.50 08/22/23 12:180.074
1,1,2-Trichloroethane ug/L <0.50 0.50 08/22/23 12:180.096
1,1-Dichloroethane ug/L <0.50 0.50 08/22/23 12:180.056
1,1-Dichloroethene ug/L <0.50 0.50 08/22/23 12:180.079
1,1-Dichloropropene ug/L <0.50 0.50 08/22/23 12:180.066
1,2,3-Trichlorobenzene ug/L <2.0 2.0 08/22/23 12:180.12
1,2,3-Trichloropropane ug/L <0.50 0.50 08/22/23 12:180.17
1,2,4-Trichlorobenzene ug/L <2.0 2.0 08/22/23 12:180.16
1,2,4-Trimethylbenzene ug/L <0.50 0.50 08/22/23 12:180.031
1,2-Dibromo-3-chloropropane ug/L <1.0 1.0 08/22/23 12:180.18
1,2-Dibromoethane (EDB)ug/L <0.50 0.50 08/22/23 12:180.15
1,2-Dichlorobenzene ug/L <0.50 0.50 08/22/23 12:180.094
1,2-Dichloroethane ug/L <0.50 0.50 08/22/23 12:180.11
1,2-Dichloropropane ug/L <0.50 0.50 08/22/23 12:180.14
1,3,5-Trimethylbenzene ug/L <0.50 0.50 08/22/23 12:180.071
1,3-Dichlorobenzene ug/L <0.50 0.50 08/22/23 12:180.098
1,3-Dichloropropane ug/L <0.50 0.50 08/22/23 12:180.085
1,4-Dichlorobenzene ug/L <0.50 0.50 08/22/23 12:180.090
2,2-Dichloropropane ug/L <0.50 0.50 08/22/23 12:180.12
2-Chlorotoluene ug/L <0.50 0.50 08/22/23 12:180.13
4-Chlorotoluene ug/L <0.50 0.50 08/22/23 12:180.096
Benzene ug/L <0.50 0.50 08/22/23 12:180.079
Bromobenzene ug/L <0.50 0.50 08/22/23 12:180.14
Bromochloromethane ug/L <0.50 0.50 08/22/23 12:180.094
Bromodichloromethane ug/L <0.50 0.50 08/22/23 12:180.17
Bromoform ug/L <0.50 0.50 08/22/23 12:180.20
Bromomethane ug/L <5.0 5.0 08/22/23 12:180.22
Carbon tetrachloride ug/L <0.50 0.50 08/22/23 12:180.17
Chlorobenzene ug/L <0.50 0.50 08/22/23 12:180.085
Chloroethane ug/L <1.0 1.0 08/22/23 12:180.17
Chloroform ug/L <0.50 0.50 08/22/23 12:180.069
Chloromethane ug/L <1.0 1.0 08/22/23 12:180.18
cis-1,2-Dichloroethene ug/L <0.50 0.50 08/22/23 12:180.11
cis-1,3-Dichloropropene ug/L <0.50 0.50 08/22/23 12:180.090
Dibromochloromethane ug/L <0.50 0.50 08/22/23 12:180.15
Dibromomethane ug/L <0.50 0.50 08/22/23 12:180.19
Dichlorodifluoromethane ug/L <0.50 0.50 08/22/23 12:180.12
Diisopropyl ether ug/L <0.50 0.50 08/22/23 12:180.072
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2023 01:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683440
Eskimo Joes
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4120088
Associated Lab Samples:92683440003
Matrix:Water
AnalyzedMDL
Ethylbenzene ug/L <0.50 0.50 08/22/23 12:180.081
Hexachloro-1,3-butadiene ug/L <2.0 2.0 08/22/23 12:180.35
Isopropylbenzene (Cumene)ug/L <0.50 0.50 08/22/23 12:180.11
m&p-Xylene ug/L <1.0 1.0 08/22/23 12:180.094
Methyl-tert-butyl ether ug/L <0.50 0.50 08/22/23 12:180.053
Methylene Chloride ug/L <2.0 2.0 08/22/23 12:181.9
n-Butylbenzene ug/L <0.50 0.50 08/22/23 12:180.066
n-Propylbenzene ug/L <0.50 0.50 08/22/23 12:180.10
Naphthalene ug/L <2.0 2.0 08/22/23 12:180.10
o-Xylene ug/L <0.50 0.50 08/22/23 12:180.14
sec-Butylbenzene ug/L <0.50 0.50 08/22/23 12:180.085
Styrene ug/L <0.50 0.50 08/22/23 12:180.14
tert-Butylbenzene ug/L <0.50 0.50 08/22/23 12:180.086
Tetrachloroethene ug/L <0.50 0.50 08/22/23 12:180.086
Toluene ug/L <0.50 0.50 08/22/23 12:180.090
trans-1,2-Dichloroethene ug/L <0.50 0.50 08/22/23 12:180.10
trans-1,3-Dichloropropene ug/L <0.50 0.50 08/22/23 12:180.13
Trichloroethene ug/L <0.50 0.50 08/22/23 12:180.17
Trichlorofluoromethane ug/L <1.0 1.0 08/22/23 12:180.14
Vinyl chloride ug/L <1.0 1.0 08/22/23 12:180.15
1,2-Dichloroethane-d4 (S)%109 70-130 08/22/23 12:18
4-Bromofluorobenzene (S)%98 70-130 08/22/23 12:18
Toluene-d8 (S)%97 70-130 08/22/23 12:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4120089LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 19.720 99 60-140
1,1,1-Trichloroethane ug/L 19.320 96 60-140
1,1,2,2-Tetrachloroethane ug/L 21.720 109 60-140
1,1,2-Trichloroethane ug/L 20.420 102 60-140
1,1-Dichloroethane ug/L 20.720 103 60-140
1,1-Dichloroethene ug/L 21.820 109 60-140
1,1-Dichloropropene ug/L 22.020 110 60-140
1,2,3-Trichlorobenzene ug/L 18.920 95 60-140
1,2,3-Trichloropropane ug/L 20.620 103 60-140
1,2,4-Trichlorobenzene ug/L 19.220 96 60-140
1,2,4-Trimethylbenzene ug/L 21.220 106 60-140
1,2-Dibromo-3-chloropropane ug/L 17.920 89 60-140
1,2-Dibromoethane (EDB)ug/L 20.520 103 60-140
1,2-Dichlorobenzene ug/L 21.320 107 60-140
1,2-Dichloroethane ug/L 20.820 104 60-140
1,2-Dichloropropane ug/L 21.320 106 60-140
1,3,5-Trimethylbenzene ug/L 21.520 107 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2023 01:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683440
Eskimo Joes
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4120089LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 21.320 106 60-140
1,3-Dichloropropane ug/L 21.120 105 60-140
1,4-Dichlorobenzene ug/L 21.320 107 60-140
2,2-Dichloropropane ug/L 18.520 93 60-140
2-Chlorotoluene ug/L 21.420 107 60-140
4-Chlorotoluene ug/L 21.220 106 60-140
Benzene ug/L 20.820 104 60-140
Bromobenzene ug/L 21.020 105 60-140
Bromochloromethane ug/L 19.720 99 60-140
Bromodichloromethane ug/L 18.920 94 60-140
Bromoform ug/L 17.420 87 60-140
Bromomethane ug/L 20.720 103 60-140
Carbon tetrachloride ug/L 18.620 93 60-140
Chlorobenzene ug/L 20.620 103 60-140
Chloroethane ug/L 24.020 120 60-140
Chloroform ug/L 19.520 98 60-140
Chloromethane ug/L 16.620 83 60-140
cis-1,2-Dichloroethene ug/L 20.220 101 60-140
cis-1,3-Dichloropropene ug/L 19.020 95 60-140
Dibromochloromethane ug/L 18.520 92 60-140
Dibromomethane ug/L 19.020 95 60-140
Dichlorodifluoromethane ug/L 21.920 110 60-140
Diisopropyl ether ug/L 21.320 107 60-140
Ethylbenzene ug/L 20.720 104 60-140
Hexachloro-1,3-butadiene ug/L 20.220 101 60-140
Isopropylbenzene (Cumene)ug/L 20.920 105 60-140
m&p-Xylene ug/L 41.740 104 60-140
Methyl-tert-butyl ether ug/L 18.820 94 60-140
Methylene Chloride ug/L 20.020 100 60-140
n-Butylbenzene ug/L 22.420 112 60-140
n-Propylbenzene ug/L 21.820 109 60-140
Naphthalene ug/L 19.220 96 60-140
o-Xylene ug/L 20.720 104 60-140
sec-Butylbenzene ug/L 21.420 107 60-140
Styrene ug/L 21.020 105 60-140
tert-Butylbenzene ug/L 17.520 88 60-140
Tetrachloroethene ug/L 19.620 98 60-140
Toluene ug/L 19.520 97 60-140
trans-1,2-Dichloroethene ug/L 21.220 106 60-140
trans-1,3-Dichloropropene ug/L 18.320 92 60-140
Trichloroethene ug/L 20.220 101 60-140
Trichlorofluoromethane ug/L 20.220 101 60-140
Vinyl chloride ug/L 17.520 87 60-140
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2023 01:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683440
Eskimo Joes
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4120105MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92683720001
4120106
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 120 60-140123 3 3020ND24.0 24.7
1,1,1-Trichloroethane ug/L 20 122 60-140128 4 3020ND24.5 25.6
1,1,2,2-Tetrachloroethane ug/L 20 131 60-140133 1 3020ND26.3 26.6
1,1,2-Trichloroethane ug/L 20 123 60-140125 2 3020ND24.6 25.0
1,1-Dichloroethane ug/L 20 130 60-140133 3 3020ND25.9 26.7
1,1-Dichloroethene ug/L M12014460-140148 3 3020ND28.8 29.6
1,1-Dichloropropene ug/L M12014360-140148 4 3020ND28.6 29.6
1,2,3-Trichlorobenzene ug/L 20 107 60-140115 7 3020ND21.5 23.0
1,2,3-Trichloropropane ug/L 20 125 60-140125 1 3020ND24.9 25.1
1,2,4-Trichlorobenzene ug/L 20 111 60-140114 2 3020ND22.2 22.8
1,2,4-Trimethylbenzene ug/L 20 126 60-140128 1 3020ND25.2 25.5
1,2-Dibromo-3-
chloropropane ug/L 20 104 60-140103 1 3020ND20.9 20.6
1,2-Dibromoethane (EDB)ug/L 20 124 60-140126 2 3020ND24.8 25.3
1,2-Dichlorobenzene ug/L 20 126 60-140128 1 3020ND25.2 25.6
1,2-Dichloroethane ug/L 20 125 60-140128 2 3020ND25.0 25.5
1,2-Dichloropropane ug/L 20 132 60-140135 2 3020ND26.5 27.1
1,3,5-Trimethylbenzene ug/L 20 131 60-140131 0 3020ND26.1 26.2
1,3-Dichlorobenzene ug/L 20 126 60-140129 2 3020ND25.3 25.7
1,3-Dichloropropane ug/L 20 126 60-140129 3 3020ND25.2 25.9
1,4-Dichlorobenzene ug/L 20 126 60-140128 2 3020ND25.1 25.6
2,2-Dichloropropane ug/L 20 111 60-140115 4 3020ND22.1 23.0
2-Chlorotoluene ug/L 20 128 60-140130 2 3020ND25.5 26.0
4-Chlorotoluene ug/L 20 125 60-140130 4 3020ND25.1 26.0
Benzene ug/L 20 131 60-140133 2 3020ND26.1 26.7
Bromobenzene ug/L 20 126 60-140127 1 3020ND25.1 25.4
Bromochloromethane ug/L 20 121 60-140123 2 3020ND24.2 24.6
Bromodichloromethane ug/L 20 111 60-140114 3 3020ND22.2 22.8
Bromoform ug/L 20 101 60-140105 4 3020ND20.3 21.0
Bromomethane ug/L 20 112 60-140135 18 3020ND22.5 27.0
Carbon tetrachloride ug/L 20 120 60-140124 3 3020ND23.9 24.7
Chlorobenzene ug/L 20 128 60-140131 3 3020ND25.5 26.2
Chloroethane ug/L M12015460-140160 4 3020ND30.8 31.9
Chloroform ug/L 20 125 60-140123 1 3020ND24.9 24.7
Chloromethane ug/L 20 109 60-140112 3 3020ND21.7 22.5
cis-1,2-Dichloroethene ug/L 20 125 60-140129 3 3020ND25.1 25.9
cis-1,3-Dichloropropene ug/L 20 110 60-140113 2 3020ND22.0 22.5
Dibromochloromethane ug/L 20 109 60-140113 3 3020ND21.9 22.6
Dibromomethane ug/L 20 116 60-140116 1 3020ND23.1 23.2
Dichlorodifluoromethane ug/L M12015560-140160 3 3020ND31.0 32.0
Diisopropyl ether ug/L 20 130 60-140133 2 3020ND26.0 26.6
Ethylbenzene ug/L 20 130 60-140133 2 3020ND25.9 26.6
Hexachloro-1,3-butadiene ug/L 20 123 60-140123 0 3020ND24.6 24.6
Isopropylbenzene
(Cumene)
ug/L 20 130 60-140133 3 3020ND25.9 26.6
m&p-Xylene ug/L 40 129 60-140131 2 3040ND51.4 52.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2023 01:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683440
Eskimo Joes
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4120105MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92683720001
4120106
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 20 113 60-140116 3 3020ND22.6 23.3
Methylene Chloride ug/L 20 122 60-140124 2 3020ND24.3 24.7
n-Butylbenzene ug/L 20 133 60-140136 2 3020ND26.7 27.1
n-Propylbenzene ug/L 20 132 60-140134 2 3020ND26.3 26.8
Naphthalene ug/L 20 110 60-140116 5 30200.41J 22.4 23.5
o-Xylene ug/L 20 125 60-140127 2 3020ND25.0 25.4
sec-Butylbenzene ug/L 20 130 60-140132 2 3020ND25.9 26.5
Styrene ug/L 20 126 60-140129 3 3020ND25.2 25.8
tert-Butylbenzene ug/L 20 107 60-140107 1 3020ND21.3 21.5
Tetrachloroethene ug/L 20 126 60-140130 3 3020ND25.2 26.0
Toluene ug/L 20 124 60-140125 1 3020ND24.8 24.9
trans-1,2-Dichloroethene ug/L 20 131 60-140137 4 3020ND26.2 27.3
trans-1,3-Dichloropropene ug/L 20 108 60-140110 2 3020ND21.5 21.9
Trichloroethene ug/L 20 127 60-140129 1 3020ND25.4 25.8
Trichlorofluoromethane ug/L M12013660-140143 5 3020ND27.3 28.6
Vinyl chloride ug/L 20 117 60-140120 3 3020ND23.3 24.0
1,2-Dichloroethane-d4 (S)%104 70-130106
4-Bromofluorobenzene (S)%98 70-130100
Toluene-d8 (S)%97 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2023 01:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683440
Eskimo Joes
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
795384
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683440001, 92683440002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4121181
Associated Lab Samples:92683440001, 92683440002
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.50 0.50 08/23/23 12:160.091
1,1,1-Trichloroethane ug/L <0.50 0.50 08/23/23 12:160.11
1,1,2,2-Tetrachloroethane ug/L <0.50 0.50 08/23/23 12:160.074
1,1,2-Trichloroethane ug/L <0.50 0.50 08/23/23 12:160.096
1,1-Dichloroethane ug/L <0.50 0.50 08/23/23 12:160.056
1,1-Dichloroethene ug/L <0.50 0.50 08/23/23 12:160.079
1,1-Dichloropropene ug/L <0.50 0.50 08/23/23 12:160.066
1,2,3-Trichlorobenzene ug/L <2.0 2.0 08/23/23 12:160.12
1,2,3-Trichloropropane ug/L <0.50 0.50 08/23/23 12:160.17
1,2,4-Trichlorobenzene ug/L <2.0 2.0 08/23/23 12:160.16
1,2,4-Trimethylbenzene ug/L <0.50 0.50 08/23/23 12:160.031
1,2-Dibromo-3-chloropropane ug/L <1.0 1.0 08/23/23 12:160.18
1,2-Dibromoethane (EDB)ug/L <0.50 0.50 08/23/23 12:160.15
1,2-Dichlorobenzene ug/L <0.50 0.50 08/23/23 12:160.094
1,2-Dichloroethane ug/L <0.50 0.50 08/23/23 12:160.11
1,2-Dichloropropane ug/L <0.50 0.50 08/23/23 12:160.14
1,3,5-Trimethylbenzene ug/L <0.50 0.50 08/23/23 12:160.071
1,3-Dichlorobenzene ug/L <0.50 0.50 08/23/23 12:160.098
1,3-Dichloropropane ug/L <0.50 0.50 08/23/23 12:160.085
1,4-Dichlorobenzene ug/L <0.50 0.50 08/23/23 12:160.090
2,2-Dichloropropane ug/L <0.50 0.50 08/23/23 12:160.12
2-Chlorotoluene ug/L <0.50 0.50 08/23/23 12:160.13
4-Chlorotoluene ug/L <0.50 0.50 08/23/23 12:160.096
Benzene ug/L <0.50 0.50 08/23/23 12:160.079
Bromobenzene ug/L <0.50 0.50 08/23/23 12:160.14
Bromochloromethane ug/L <0.50 0.50 08/23/23 12:160.094
Bromodichloromethane ug/L <0.50 0.50 08/23/23 12:160.17
Bromoform ug/L <0.50 0.50 08/23/23 12:160.20
Bromomethane ug/L <5.0 5.0 08/23/23 12:160.22
Carbon tetrachloride ug/L <0.50 0.50 08/23/23 12:160.17
Chlorobenzene ug/L <0.50 0.50 08/23/23 12:160.085
Chloroethane ug/L <1.0 1.0 08/23/23 12:160.17
Chloroform ug/L <0.50 0.50 08/23/23 12:160.069
Chloromethane ug/L <1.0 1.0 08/23/23 12:160.18
cis-1,2-Dichloroethene ug/L <0.50 0.50 08/23/23 12:160.11
cis-1,3-Dichloropropene ug/L <0.50 0.50 08/23/23 12:160.090
Dibromochloromethane ug/L <0.50 0.50 08/23/23 12:160.15
Dibromomethane ug/L <0.50 0.50 08/23/23 12:160.19
Dichlorodifluoromethane ug/L <0.50 0.50 08/23/23 12:160.12
Diisopropyl ether ug/L <0.50 0.50 08/23/23 12:160.072
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2023 01:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683440
Eskimo Joes
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4121181
Associated Lab Samples:92683440001, 92683440002
Matrix:Water
AnalyzedMDL
Ethylbenzene ug/L <0.50 0.50 08/23/23 12:160.081
Hexachloro-1,3-butadiene ug/L <2.0 2.0 08/23/23 12:160.35
Isopropylbenzene (Cumene)ug/L <0.50 0.50 08/23/23 12:160.11
m&p-Xylene ug/L <1.0 1.0 08/23/23 12:160.094
Methyl-tert-butyl ether ug/L <0.50 0.50 08/23/23 12:160.053
Methylene Chloride ug/L <2.0 2.0 08/23/23 12:161.9
n-Butylbenzene ug/L <0.50 0.50 08/23/23 12:160.066
n-Propylbenzene ug/L <0.50 0.50 08/23/23 12:160.10
Naphthalene ug/L <2.0 2.0 08/23/23 12:160.10
o-Xylene ug/L <0.50 0.50 08/23/23 12:160.14
sec-Butylbenzene ug/L <0.50 0.50 08/23/23 12:160.085
Styrene ug/L <0.50 0.50 08/23/23 12:160.14
tert-Butylbenzene ug/L <0.50 0.50 08/23/23 12:160.086
Tetrachloroethene ug/L <0.50 0.50 08/23/23 12:160.086
Toluene ug/L <0.50 0.50 08/23/23 12:160.090
trans-1,2-Dichloroethene ug/L <0.50 0.50 08/23/23 12:160.10
trans-1,3-Dichloropropene ug/L <0.50 0.50 08/23/23 12:160.13
Trichloroethene ug/L <0.50 0.50 08/23/23 12:160.17
Trichlorofluoromethane ug/L <1.0 1.0 08/23/23 12:160.14
Vinyl chloride ug/L <1.0 1.0 08/23/23 12:160.15
1,2-Dichloroethane-d4 (S)%109 70-130 08/23/23 12:16
4-Bromofluorobenzene (S)%95 70-130 08/23/23 12:16
Toluene-d8 (S)%96 70-130 08/23/23 12:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4121182LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 20.220 101 60-140
1,1,1-Trichloroethane ug/L 20.220 101 60-140
1,1,2,2-Tetrachloroethane ug/L 22.720 114 60-140
1,1,2-Trichloroethane ug/L 20.820 104 60-140
1,1-Dichloroethane ug/L 21.920 109 60-140
1,1-Dichloroethene ug/L 23.020 115 60-140
1,1-Dichloropropene ug/L 23.020 115 60-140
1,2,3-Trichlorobenzene ug/L 18.120 90 60-140
1,2,3-Trichloropropane ug/L 21.420 107 60-140
1,2,4-Trichlorobenzene ug/L 19.120 95 60-140
1,2,4-Trimethylbenzene ug/L 21.620 108 60-140
1,2-Dibromo-3-chloropropane ug/L 17.720 89 60-140
1,2-Dibromoethane (EDB)ug/L 21.520 107 60-140
1,2-Dichlorobenzene ug/L 21.520 108 60-140
1,2-Dichloroethane ug/L 21.320 106 60-140
1,2-Dichloropropane ug/L 22.020 110 60-140
1,3,5-Trimethylbenzene ug/L 21.820 109 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2023 01:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683440
Eskimo Joes
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4121182LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 21.520 108 60-140
1,3-Dichloropropane ug/L 21.820 109 60-140
1,4-Dichlorobenzene ug/L 21.720 108 60-140
2,2-Dichloropropane ug/L 19.420 97 60-140
2-Chlorotoluene ug/L 21.620 108 60-140
4-Chlorotoluene ug/L 21.520 108 60-140
Benzene ug/L 21.520 107 60-140
Bromobenzene ug/L 21.120 105 60-140
Bromochloromethane ug/L 20.420 102 60-140
Bromodichloromethane ug/L 18.720 94 60-140
Bromoform ug/L 16.820 84 60-140
Bromomethane ug/L 23.420 117 60-140
Carbon tetrachloride ug/L 19.920 100 60-140
Chlorobenzene ug/L 21.520 108 60-140
Chloroethane ug/L 24.820 124 60-140
Chloroform ug/L 21.020 105 60-140
Chloromethane ug/L 18.120 90 60-140
cis-1,2-Dichloroethene ug/L 21.420 107 60-140
cis-1,3-Dichloropropene ug/L 19.320 96 60-140
Dibromochloromethane ug/L 18.520 92 60-140
Dibromomethane ug/L 19.320 97 60-140
Dichlorodifluoromethane ug/L 22.020 110 60-140
Diisopropyl ether ug/L 21.920 110 60-140
Ethylbenzene ug/L 21.320 107 60-140
Hexachloro-1,3-butadiene ug/L 20.520 103 60-140
Isopropylbenzene (Cumene)ug/L 21.720 108 60-140
m&p-Xylene ug/L 42.440 106 60-140
Methyl-tert-butyl ether ug/L 19.420 97 60-140
Methylene Chloride ug/L 20.720 103 60-140
n-Butylbenzene ug/L 22.420 112 60-140
n-Propylbenzene ug/L 22.120 110 60-140
Naphthalene ug/L 19.020 95 60-140
o-Xylene ug/L 21.020 105 60-140
sec-Butylbenzene ug/L 21.520 107 60-140
Styrene ug/L 21.620 108 60-140
tert-Butylbenzene ug/L 17.720 89 60-140
Tetrachloroethene ug/L 20.520 102 60-140
Toluene ug/L 19.920 99 60-140
trans-1,2-Dichloroethene ug/L 22.420 112 60-140
trans-1,3-Dichloropropene ug/L 18.320 92 60-140
Trichloroethene ug/L 20.820 104 60-140
Trichlorofluoromethane ug/L 21.220 106 60-140
Vinyl chloride ug/L 18.020 90 60-140
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2023 01:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683440
Eskimo Joes
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4121183MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92683609002
4121184
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 132 60-140130 2 3020ND26.4 25.9
1,1,1-Trichloroethane ug/L 20 137 60-140132 3 3020ND27.4 26.5
1,1,2,2-Tetrachloroethane ug/L 20 140 60-140139 1 3020ND28.0 27.8
1,1,2-Trichloroethane ug/L 20 135 60-140131 3 3020ND27.0 26.1
1,1-Dichloroethane ug/L M12014660-140140 4 3020ND29.1 27.9
1,1-Dichloroethene ug/L M12015960-140153 4 3020ND31.8 30.5
1,1-Dichloropropene ug/L M12015760-140149 5 3020ND31.4 29.8
1,2,3-Trichlorobenzene ug/L 20 113 60-140111 2 3020ND22.7 22.1
1,2,3-Trichloropropane ug/L 20 133 60-140130 2 3020ND26.6 26.1
1,2,4-Trichlorobenzene ug/L 20 116 60-140115 1 3020ND23.1 23.0
1,2,4-Trimethylbenzene ug/L 20 133 60-140132 1 3020ND26.7 26.5
1,2-Dibromo-3-
chloropropane ug/L 20 112 60-140109 2 3020ND22.3 21.9
1,2-Dibromoethane (EDB)ug/L 20 136 60-140132 3 3020ND27.2 26.5
1,2-Dichlorobenzene ug/L 20 132 60-140133 1 3020ND26.5 26.6
1,2-Dichloroethane ug/L 20 139 60-140134 4 3020ND27.8 26.8
1,2-Dichloropropane ug/L M12014360-140141 1 3020ND28.5 28.2
1,3,5-Trimethylbenzene ug/L 20 136 60-140137 0 3020ND27.3 27.3
1,3-Dichlorobenzene ug/L 20 133 60-140132 1 3020ND26.6 26.4
1,3-Dichloropropane ug/L 20 139 60-140134 4 3020ND27.9 26.8
1,4-Dichlorobenzene ug/L 20 133 60-140133 0 3020ND26.5 26.5
2,2-Dichloropropane ug/L 20 117 60-140114 3 3020ND23.5 22.8
2-Chlorotoluene ug/L 20 135 60-140135 0 3020ND27.0 27.1
4-Chlorotoluene ug/L 20 133 60-140135 2 3020ND26.6 27.0
Benzene ug/L M12014260-140138 3 3020ND28.5 27.6
Bromobenzene ug/L 20 133 60-140132 1 3020ND26.7 26.5
Bromochloromethane ug/L 20 134 60-140130 3 3020ND26.7 25.9
Bromodichloromethane ug/L 20 124 60-140121 3 3020ND24.8 24.1
Bromoform ug/L 20 114 60-140111 2 3020ND22.8 22.3
Bromomethane ug/L M12013560-140151 11 3020ND27.0 30.2
Carbon tetrachloride ug/L 20 135 60-140131 3 3020ND26.9 26.1
Chlorobenzene ug/L 20 138 60-140135 2 3020ND27.5 27.0
Chloroethane ug/L M12017160-140162 5 3020ND34.2 32.4
Chloroform ug/L 20 137 60-140129 6 30200.59 28.1 26.4
Chloromethane ug/L 20 117 60-140115 1 3020ND23.3 23.1
cis-1,2-Dichloroethene ug/L 20 139 60-140133 4 3020ND27.8 26.7
cis-1,3-Dichloropropene ug/L 20 119 60-140116 2 3020ND23.7 23.3
Dibromochloromethane ug/L 20 123 60-140120 3 3020ND24.6 23.9
Dibromomethane ug/L 20 126 60-140122 3 3020ND25.2 24.4
Dichlorodifluoromethane ug/L M12016460-140158 4 3020ND32.8 31.5
Diisopropyl ether ug/L M12014460-140138 4 3020ND28.8 27.6
Ethylbenzene ug/L 20 137 60-140135 2 3020ND27.4 27.0
Hexachloro-1,3-butadiene ug/L 20 134 60-140127 5 3020ND26.8 25.5
Isopropylbenzene
(Cumene)
ug/L 20 138 60-140136 1 3020ND27.6 27.3
m&p-Xylene ug/L 40 137 60-140133 3 3040ND54.9 53.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2023 01:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683440
Eskimo Joes
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4121183MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92683609002
4121184
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 20 125 60-140122 3 3020ND25.0 24.4
Methylene Chloride ug/L 20 134 60-140127 5 3020ND26.7 25.4
n-Butylbenzene ug/L M12013860-140141 2 3020ND27.7 28.3
n-Propylbenzene ug/L 20 138 60-140139 1 3020ND27.6 27.9
Naphthalene ug/L 20 115 60-140116 1 3020ND23.0 23.3
o-Xylene ug/L 20 132 60-140130 2 3020ND26.5 26.1
sec-Butylbenzene ug/L 20 138 60-140136 1 3020ND27.5 27.3
Styrene ug/L 20 135 60-140132 2 3020ND27.1 26.5
tert-Butylbenzene ug/L 20 113 60-140113 0 3020ND22.6 22.6
Tetrachloroethene ug/L 20 132 60-140131 1 3020ND26.5 26.2
Toluene ug/L 20 130 60-140128 2 3020ND26.1 25.6
trans-1,2-Dichloroethene ug/L M12014560-140142 2 3020ND29.0 28.4
trans-1,3-Dichloropropene ug/L 20 118 60-140115 3 3020ND23.5 22.9
Trichloroethene ug/L 20 137 60-140134 2 3020ND27.4 26.7
Trichlorofluoromethane ug/L M12014960-140145 3 3020ND29.9 28.9
Vinyl chloride ug/L 20 126 60-140122 4 3020ND25.2 24.4
1,2-Dichloroethane-d4 (S)%106 70-130106
4-Bromofluorobenzene (S)%99 70-13099
Toluene-d8 (S)%97 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2023 01:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683440
Eskimo Joes
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
795052
EPA 504.1
EPA 504.1
GCS 504 EDB DBCP
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683440001, 92683440002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4119665
Associated Lab Samples:92683440001, 92683440002
Matrix:Water
AnalyzedMDL
1,2,3-Trichloropropane ug/L <0.050 0.050 08/22/23 19:170.0097
1,2-Dibromo-3-chloropropane ug/L <0.050 0.050 08/22/23 19:170.0047
1,2-Dibromoethane (EDB)ug/L <0.020 0.020 08/22/23 19:170.0056
1-Chloro-2-bromopropane (S)%116 70-130 08/22/23 19:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4119666LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
4119667
1,2,3-Trichloropropane ug/L 0.210.25 86 70-130780.19 10 20
1,2-Dibromo-3-chloropropane ug/L 0.240.25 95 70-130920.23 4 20
1,2-Dibromoethane (EDB)ug/L 0.240.25 96 70-130900.22 7 20
1-Chloro-2-bromopropane (S)%92 70-13090
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4119669MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92683546002
4119670
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,3-Trichloropropane ug/L 0.25 91 65-13592 2 200.25<0.0099 0.22 0.23
1,2-Dibromo-3-
chloropropane ug/L 0.25 97 65-13596 2 200.25<0.0048 0.24 0.24
1,2-Dibromoethane (EDB)ug/L 0.25 96 65-13595 1 200.25<0.0057 0.24 0.24
1-Chloro-2-bromopropane
(S)%93 70-13093
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683546001
4119668SAMPLE DUPLICATE:
1,2,3-Trichloropropane ug/L <0.051 20<0.0096
1,2-Dibromo-3-chloropropane ug/L <0.051 20<0.0046
1,2-Dibromoethane (EDB)ug/L 0.034 D635200.048
1-Chloro-2-bromopropane (S)%9192
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2023 01:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 30
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92683440
Eskimo Joes
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2023 01:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 30
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92683440
Eskimo Joes
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92683440001 795052 795203MW-1 EPA 504.1 EPA 504.1
92683440002 795052 795203MW-2 EPA 504.1 EPA 504.1
92683440001 795384MW-1 SM 6200B
92683440002 795384MW-2 SM 6200B
92683440003 795157Trip Blank SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2023 01:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 30
Page 28 of 30
Page 29 of 30
Page 30 of 30

Attachment III- Receptor Survey Update Documentation

Updated November 5, 2020
Owner's Name Approximate Well Use
Parcel Number Source Well # and Well Address Owners Mailing Address Well Depth Well Casing Distance From
(Lexington, N.C.)(feet)Depth (feet)Source (feet)
0600200000010B Owner interview (2020)W14 Bruce Lopp P.O. Box 284 Potable Water Well
Survey form ( 2014)1710 Cotton Grove Lexington, NC 27293 185 135 200 Bathroom use only
[phone] No water service- 2020
06002B0000073 W6 Efird Wilson P.O. Box 2014 Unknown Unknown 460 Irrigation Well
Owner and resident interviews (2014)6 Mayfair Road Lexington, NC 27293 Active Municipal Water Account
06002B0000069 W5 Bethany D. Bee 196 Woodwind Drive 80 60 510 Irrigation Well
Survey form-previous owner (2014)8 Mayfair Rd. Lexington, NC 27295 Active water account- 2020
06002B0000065 W1 Deborah Gay Davis 100 Mayfair Road Unknown Unknown 660 Inactive Well
Owner interview (2014)100 Mayfair Road Lexington, NC 27292 Active Municipal Water Account
0600200000007 W7 Paul and Stella Baker 104 Fuller Rd.Inactive Well
Owner/resident interview (2014)104 Fuller Road Lexington, NC 27292 Unknown Unknown 760 Meter observed, owner verified municipal
water service
06002B0000015 W16 Daniel C. Ennett, Jr.165 Brown Street Unknown Unknown 740 Active water account- 2020
Survey form-previous owner (2014)101 Mayfair Road Lexington, NC 27292 Observed inactive well and water meter
06002B0000056 W3 John T. Tetter 104 Mayfair Road Inactive Well
Survey form (2014)104 Mayfair Rd. Lexington, NC 27292-5834 55 Unknown 830 Observed water meter
Owner/resident interview (2020)Active Municipal Water Account
06002B0000019 W15 Matthew and Tanya Bordonaro 103 Mayfair Road Potable Water Well
Survey form, owner interview (2014)103 Mayfair Road Lexington, NC 27292 Unknown Unknown 850 Observed well, no water meter
No water service-2020
06002C00A0015 W10 EE Wilson Investments, LLC P.O. Box 2014 Unknown Unknown 840 Two inactive wells
Owner/resident interview (2014)W11 8 S. Avondale Road Lexington, NC 27293 850 Active Municipal Water Account
06002C00H0001 W12 Polly Jane Kepley 1724 South View Drive Inactive Well
Owner/resident stated no well 1724 South View Drive Lexington, NC 27292 Unknown Unknown 860 Observed water meter
on form and by interview (2014)Active Municipal Water Account
06002B0000025 W4 Iris M. Latham et.al.107 Mayfair Road Unknown Unknown 960 Inactive Well; observed water meter
Survey form (2014)107 Mayfair Road Lexington, NC 27292 Active water account-2020
PROPERTIES WITH POTENTIAL WATER WELLS WITHIN 1,000 FOOT RADIUS
ESKIMO JOE'S; INCIDENT No.: 20918
1705 COTTON GROVE ROAD, LEXINGTON, NORTH CAROLINA
S&ME PROJECT NO. 1584-02-045E
W11
W10 W12
W4
W3W1W5
W6
W7
N.C
.

R
O
U
T
E

8
CO
T
T
O
N

G
R
O
V
E

R
D
MAYFAIR RD
AVONDA
L
E

R
D
GLENDALE

R
D
HE
D
R
I
C
K

R
D
1,0
0
0

f
t
.
KEY
- POTABLE WELL
W14
W16
W15
- IRRIGATION WELL
- INACTIVE WELL
- UNKNOWN APPROXIMATE WATER SUPPLY WELL LOCATION
SO
U
T
H
V
I
E
W

R
D

(
S
R

2
2
4
0
)
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
Dr
a
w
i
n
g

P
a
t
h
:

Z:
\
S
h
a
r
e
d
\
S
M
E
\
R
e
s
o
u
r
c
e
\
C
A
D
D
a
t
a
\
G
r
e
e
n
s
b
o
r
o
\
1
5
8
4
\
2
0
0
2
\
0
2
-
0
4
5

-

E
S
K
I
M
O

J
O
E
S
\
D
\
E
s
k
i
m
o

J
o
e
s

A
r
e
a

M
a
p
.
d
w
g
0 400 800
(IN FEET)GRAPHIC SCALE (IN FEET)GRAPHIC SCALE
ESKIMO JOE'S
1705 COTTON GROVE ROAD
LEXINGTON, NORTH CAROLINA 1584-02-045D
NOV. 2020
AS SHOWNWATER WELL LOCATION MAP
Incident No. 20918
250

f
t
.
N