WS-5268_18105_CA_IAR_20230406

UST CLOSURE AND INITIAL ABATEMENT ACTION REPORT

DODSON’S AMOCO
306 WEST CENTER STREET
MEBANE, NORTH CAROLINA

PREPARED FOR:
MR. MICHAEL TOMPKINS
MCLEOD OIL COMPANY, INC.
PO BOX 100
MEBANE, NORTH CAROLINA 27302

PREPARED BY:
PILOT GEOLOGICAL, PLLC
PO BOX 128
KERNERSVILLE, NORTH CAROLINA 27285

APRIL 6, 2023
PILOT PROJECT NO. G-8098

SITE INFORMATION

Site Name and Location Dodson Amoco
306 West Center Street
Mebane, Alamance County, North Carolina

Incident No. 18105

Facility ID: #00-0-0000023229

Latitude and Longitude: 36.097666° N; 79.272196° W

Land Use Category: Commercial
Contacts
Owner of UST: McLeod Oil Company, Inc.
PO Box 100
Mebane, North Carolina 27302
[phone]

Primary Contact: Mr. Michael Tompkins
McLeod Oil Company, Inc.
[phone]

Consultant: Pilot Geological, PLLC
PO Box 128
Kernersville, North Carolina 27285
[phone]

Closure Contractor: D.H. Griffin Wrecking Company, Inc.
4716 Hilltop Road
Greensboro, North Carolina 27407
[phone]

Laboratory: Pace Analytical
1377 South Park Drive
Kernersville, North Carolina 27284
[phone]
Laboratory I.D. # Various

Release Information: The release was discovered by others during UST removal activities in October 1997.
The estimated quantity of release is unknown. The release occurred from a former gasoline UST system
consisting of three 1,000-gallon gasoline USTs, associated dispensers and piping.

TABLE OF CONTENTS

1.0 SITE HISTORY ................................................................................................................... 1
2.0 SITE CHARACTERISTICS ..................................................................................................... 1
3.0 UST CLOSURE AND INITIAL RESPONSE .............................................................................. 2
3.1 UST Information ............................................................................................................... 2
3.2 UST Closure Activities ........................................................................................................ 2
4.0 FIELD ACTIVITIES .............................................................................................................. 3
4.1 Soil Samples - UST Closure ............................................................................................... 3
4.2 Soil Samples - Over Excavation ......................................................................................... 3
5.0 LABORATORY ANALYTICAL RESULTS ................................................................................. 4
5.1 Soil Sample Analysis – UST Closure ................................................................................... 4
5.2 Soil Sample Analysis – Over Excavation ............................................................................ 4
6.0 CONCLUSIONS ................................................................................................................. 4
7.0 RECOMMENDATIONS ....................................................................................................... 5

DRAWINGS

Drawing 1 USGS Topographic Map
Drawing 2 Site Map
Drawing 3 UST and Sample Location Map
Drawing 4 Excavation Location Map
TABLES

Table 1 UST Information
Table 2 Summary of Soil Analytical Results

APPENDICIES

Appendix A UST-2, UST-3, Material Manifest (Liquids) and Tank Disposal Manifest
Appendix B Non-Hazardous Soil Disposal Manifests
Appendix C Laboratory Data Sheets and Chain of Custody Records

UST Closure and Initial Abatement Action Report
Dodson’s Amoco
Mebane, North Carolina
April 6, 2023
1.0 SITE HISTORY

Dodson Amoco is located at 306 West Center Street in Mebane, Alamance County, North Carolina
(Drawings 1 and 2). The property is currently developed with an automotive repair facility. In
October of 1997, three 1,000-gallon gasoline underground storage tanks (USTs) were removed from
the site and a release was detected. Mark Creel & Associates, Inc. completed the UST closure
activities and associated report. The release was confirmed through laboratory analysis of soil
samples collected during the UST closure activities. Subsequent to the UST removal activities, three
2,000-gallon gasoline USTs were installed in the former UST location at the site in October 1997.

Apex Environmental, Inc. completed an LSA for the site dated March 12, 2004. The site was classified
as an intermediate risk site based on the presence of benzene above its Gross Contaminant Level
(GCL).

Based on the intermediate risk classification of the site, the NCDEQ issued a Notice of Regulatory
Requirements (NORR) dated February 13, 2023 requiring that an additional groundwater
monitoring event be completed.

Pilot completed a Groundwater Monitoring Report for the site dated March 7, 2023. On February
23, 2023, Pilot collected groundwater samples from monitoring wells MW-1 through MW-4 and
DW-1. Laboratory analysis of the groundwater samples detected targeted compounds above
their respective 2L standards, with benzene exceeding its GCL in MW-2.

Pilot was requested by Mr. Michael Tompkins with McLeod Oil Company, Inc. to provide UST
closure services associated with the existing USTs.

2.0 SITE CHARACTERISTICS

The United States Geological Survey (USGS) Topographic Map, Mebane and Efland, North
Carolina Quadrangle depicts the site as an urban area (Drawing 1). The site elevation is
approximately 670 feet above mean sea level. Unamend tributaries to Haw River are located
approximately 1,670 feet southwest of the site. Based on the review of the USGS topographic
map and observations of the general area and site topography, surface run-off would be
expected to flow generally to the southwest across the site.

The subject site is located within the Piedmont Physiographic Province. The Piedmont
Physiographic Province generally consists of hills and ridges which are dissected by a system of
swales and streams. The Piedmont Physiographic Province is predominantly underlain by
metamorphic rock (formed by heat, pressure and/or chemical action) and igneous rock (formed
directly from molten material). The topography and relief of the Piedmont Province has
developed from differential weathering of the igneous and metamorphic rock. Ridges and hills
have been developed in areas of less weathered rock. Because of the continued chemical and
physical weathering rock in the Piedmont Physiographic Province is generally covered with a
UST Closure and Initial Abatement Action Report
Dodson’s Amoco
Mebane, North Carolina
April 6, 2023
mantle of soil that has weathered in place from the parent bedrock. These soils vary in thickness
and are referred to as residuum or residual soils. The residuum is typically finer grained and has
higher clay content near the surface because of the advanced weathering. Similarly, the soils
typically become coarser grained with increasing depth because of decreased weathering. As the
weathering decreases, the residual soils generally retain the overall appearance, texture and
foliations of the parent rock.

In general, groundwater movement in the Piedmont Physiographic Province is from higher to
lower elevations. As such, the presumed direction of groundwater flow is generally to the south
across the site. Based on the presumed groundwater flow direction, areas to the north are
potentially up-gradient of the site.

3.0 UST CLOSURE AND INITIAL RESPONSE

3.1 UST Information

A release was identified during the previous removal of three 1,000-gallon gasoline USTs by
others in October 1997. Three 2,000-gallon gasoline USTs were removed on March 20, 2023.
UST information is summarized in Table 1.

3.2 UST Closure Activities

On March 20, 2023, the pea gravel surrounding the USTs was excavated and temporarily
stockpiled on-site for re-use as backfill unless impacted. Prior to removal of the USTs, Pilot
submitted the UST-3 form to the North Carolina Department of Environmental Quality (NCDEQ).
The USTs were removed by D.H. Griffin Wrecking Company, Inc. (D.H. Griffin) using a track
mounted excavator. UST removal activities were observed by Pilot. Prior to removal,
approximately 154 gallons of non-hazardous liquids were removed from the UST system by D.H.
Griffin using a vacuum truck and properly disposed. Once the residual liquids had been
evacuated, the USTs were purged of vapors, removed from the excavations and loaded onto a
trailer for recycling. A representative of the Alamance County Fire Marshal’s Office was on-site
to approve the UST removal activities. The three USTs were observed in good condition with no
obvious signs of damage or corrosion. Monitoring well MW-1 was inadvertently destroyed during
the UST removal activities, based on it being set into the pea gravel surrounding the USTs.

The UST-2 and UST-3 forms, the Material Manifest for the non-hazardous liquids, and the Tank
Disposal Manifest are included in Appendix A.

UST Closure and Initial Abatement Action Report
Dodson’s Amoco
Mebane, North Carolina
April 6, 2023
4.0 FIELD ACTIVITIES

4.1 Soil Samples - UST Closure

Upon removal of the USTs, six soil samples (T-1 through T-6, Drawing 3) were collected from
beneath each end of the USTs. Upon removal of the dispenser island, three soil samples (D-1
through D-3, Drawing 3) were collected beneath the former dispenser locations. Soil samples for
product lines were not collected since the lines were located directly over the UST and less than
10 feet long. The soil samples were visually classified in the field and screened for volatile organic
vapors using a photoionization detector (PID). The soil samples were placed into laboratory
prepared containers, labeled and transported to Pace Analytical (Pace) in Kernersville, North
Carolina and analyzed for gasoline range total petroleum hydrocarbons (TPH) using EPA Method
8015/5035. A chain of custody record was maintained and is included in Appendix C.

4.2 Soil Samples - Over Excavation

Based on observations and field screening results indicating that impacted soil was present,
approximately 100.29 tons of petroleum impacted soil was excavated from the tank basin. The
release appeared to be from the previous USTs and pre-approval was obtained from the NCDEQ
for the soil removal. Neither groundwater nor bedrock were encountered during the removal of
the approved amount of impacted soil. Additional impacted soil was not removed based on the
previously determined risk classification of the site and reaching the pre-approved tonnage
allowed by the NCDEQ. The petroleum impacted soil was transported to Earthtec of NC, Inc.
(Earthtec) for treatment and disposal. One soil sample (C-1 through C-5) per load of excavated
soil was collected to confirm impact in accordance with NCDEQ, UST Section Guidelines. The
disposal confirmation soil samples (C-1 through C-5) were analyzed on-site via a mobile lab using
ultraviolent fluorescence (UVF) technology by Red Lab. The UVF technology was not utilized to
analyze the stockpiled overburden due to the material being pea gravel. The pea gravel was
returned to the excavation as backfill. The Non-Hazardous Waste Manifests and weight
verification tickets for the impacted soil are included in Appendix B.

Upon completion of the soil excavation activities, confirmation soil samples (N-1, E-1, S-1, W-1,
and B-1) were collected from the sidewalls and base of the final excavation. The excavation was
rectangular shaped with its greatest dimensions being approximately 26.5 feet by 19.5 feet by 19
feet in depth. The approximate locations of the confirmation soil samples are shown on Drawing
4. The excavation was backfilled with imported ABC stone from a quarry in Mebane, North
Carolina and compacted using the excavation equipment.

The confirmation soil samples were submitted to Pace to be analyzed for volatile organic
compounds (VOCs) using EPA Method 8260 and for volatile petroleum hydrocarbons (VPH) using
the Massachusetts Department of Environmental Protection (MADEP) Method.

UST Closure and Initial Abatement Action Report
Dodson’s Amoco
Mebane, North Carolina
April 6, 2023
5.0 LABORATORY ANALYTICAL RESULTS

5.1 Soil Sample Analysis – UST Closure

Laboratory analysis of soil samples T-1 through T-6 detected gasoline range TPH above its NC
Action Level of 50 mg/Kg. Laboratory analysis of soil samples D-1 through D-3 did not detect
gasoline range TPH at concentrations above its laboratory detection limit. A summary of the
laboratory analytical results is presented in Table 2. The laboratory data sheets and chain of
custody record are included in Appendix C.

5.2 Soil Sample Analysis – Over Excavation

Laboratory analysis of soil samples S-1 and B-1 detected targeted compounds above the
Residential Soil Cleanup Levels, with naphthalene being detected above its respective
Industrial/Commercial Soil Cleanup Level.

Each of the confirmation disposal soil samples C-1 through C-5, analyzed on-site by Red Lab,
detected gasoline range TPH above its NC Action Level of 50 mg/Kg. A summary of the laboratory
analytical results is presented in Table 2. The laboratory data sheets and chain of custody record
are included in Appendix C.

6.0 CONCLUSIONS

Based on the field observations and laboratory analytical results, Pilot concludes the following:

 On March 20, 2023, three 2,000-gallon gasoline USTs were removed from the site.

 Based on field screening results and observations, a petroleum release was identified during
the removal of the UST system that appeared to have occurred from the previously removed
USTs.

 Approximately 100.29 tons of petroleum impacted soil was excavated from beneath the USTs
and the immediately surrounding area. The impacted soil was transported to EarthTec for
treatment and disposal. Additional impacted soil was not removed due to reaching the
tonnage pre-approved by the NCDEQ.

 Laboratory analysis of soil samples T-1 through T-6 detected gasoline range TPH above its NC
Action Level of 50 mg/Kg. Laboratory analysis of soil samples D-1 through D-3 did not detect
gasoline range TPH at concentrations above the laboratory detection limit.

 Laboratory analysis of soil samples S-1 and B-1 detected targeted compounds above the
Residential Soil Cleanup Levels, with naphthalene being detected above its respective
Industrial/Commercial Soil Cleanup Levels. Each of the confirmation disposal soil samples C-1
UST Closure and Initial Abatement Action Report
Dodson’s Amoco
Mebane, North Carolina
April 6, 2023
through C-5, analyzed on-site by Red Lab, detected gasoline range TPH above its NC Action
Level of 50 mg/Kg.

7.0 RECOMMENDATIONS

Pilot recommends that a copy of this report be submitted to the NCDEQ, Winston-Salem Regional
Office for their review. Prior to a property transaction occurring a Notice of Residual Petroleum
(NORP) will need to be recorded.

8.0 QUALIFICATIONS

The activities and evaluative approaches used in this assessment are consistent with those
normally employed in assessment projects of this type. Our evaluation of site conditions has
been based on our understanding of the site project information and the data obtained during
our field activities.

DRAWINGS
SITE
USGS Topographic Map
Dodson’s Amoco
306 West Center Street
Mebane, Alamance County, NC
Pilot Project G-8098
Drawing 1
USGS Topographic Map
Mebane & Efland, NC Quadrangles
Scale: 1” = 2,000’
LEGEND
Site Boundary
Site Map
Dodson’s Amoco
306 West Center Street
Mebane, Alamance County, NC
Pilot Project G-8098
Drawing 2
Google Earth
Interactive Mapping Software
Scale : 1”= 80’
LEGEND
Site BoundaryU. Former UST System
U
UST and Sample Location Map
Dodson’s Amoco
306 West Center Street
Mebane, Alamance County, NC
Pilot Project G-8098
Drawing 3
Google Earth
Interactive Mapping Software
Scale : 1”= 10’
LEGEND
Site Boundary
UST
Product Lines
Soil Sample
T-1
D-1 D-3D-2
T-3
T-5
T-2 T-4
T-6
Excavation Location Map
Dodson’s Amoco
306 West Center Street
Mebane, Alamance County, NC
Pilot Project G-8098
Drawing 4
Google Earth
Interactive Mapping Software
Scale : 1”= 10’
LEGEND
Site Boundary
UST
Excavation Area
Soil Sample
B-1
E-1
N-1
W-1
S-1

TABLES
UST ID
Number Owner Last
Contents
Previous
Contents
Capacity
(in Gallons)
Construction
Details
Tank
Dimensions
Installation
Date Status Release
Single Wall
Steel
Single Wall
Steel
Single Wall
Steel
2,000
2,000
1,000 YesRemoved
19971960's
12' x 64"
12' x 64"
12' x 46"
NoRemoved10/2/1997
10/2/1997 Removed No
12' x 64" 10/2/1997 Removed NoSingle Wall
Steel6Gasoline Gasoline 2,000
McLeod Oil Company
PO Box 100
Mebane, North Carolina 27302
5
4
3
Gasoline
Gasoline
Gasoline
Gasoline
Gasoline
Gasoline
Table 1 - UST Information
Dodson's Amoco
Mebane, North Carolina
1960's Removed
1997 Yes2Gasoline Gasoline 1,000 Single Wall
Steel 12' x 46"
1 Gasoline Single Wall
SteelGasoline 12' x 46" 1960's Removed
19971,000 Yes
5035
Sample ID Approximate Sample
Depth (ft. bgs)Sample Collection Date GR
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D-1 3 3/20/2023 ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
D-2 3 3/20/2023 ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
D-3 3 3/20/2023 ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
T-1 8 3/20/2023 889 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
T-2 8 3/20/2023 542 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
T-3 8 3/20/2023 17,100 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
T-4 8 3/20/2023 19,200 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
T-5 8 3/20/2023 17,300 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
T-6 8 3/20/2023 6,970 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
N-1 8 3/21/2023 NA 0.055 0.10 0.028 0.74 0.081 0.076 ND 0.16 0.25 ND 0.73 1.5 0.45 2.7 ND ND ND
E-1 8 3/21/2023 NA ND ND ND ND ND ND 0.076 ND ND ND ND ND ND ND ND ND ND
S-1 8 3/21/2023 NA 1.9 25.6 ND 140 22.7 23.1 ND 111 77.9 ND 2.1 538 159 522 1,700 ND 2,600
W-1 8 3/21/2023 NA ND ND ND 0.018 ND ND ND ND ND 0.018 ND ND ND 0.079 ND ND ND
B-1 19 3/21/2023 NA 7.0 20.7 6.1 179 19.7 15.2 ND 60.0 59.6 ND 54.6 294 93.0 443 3,400 ND 1,300
*C-1 -- 3/21/2023 3,300 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
*C-2 -- 3/21/2023 2,205 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
*C-3 -- 3/21/2023 2,973 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
*C-4 -- 3/21/2023 1,671 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
*C-5 -- 3/21/2023 6,029 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
50 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A
N/A 0.0072 2.4 2.2 8 1.3 0.12 0.023 0.2 1.4 0.9 5.4 6.6 6.6 6 68 540 31
N/A 12 782 1,560 60.3 1,560 1,560 93.8 5.5 1,560 3,120 1,250 156 156 3,120 625 1,560 469
N/A 59.4 11,600 23,300 297 23,300 23,300 1,400 27 23,300 46,700 18,600 2,330 2,330 46,700 9,340 23,330 7,000
= Soil Sample Above the NC Action Level or Soil-to-Groundwater MSCC
= Soil Sample Above the Residential Soil Cleanup Levels
= Soil Sample Above the Industrial/Commercial Soil Cleanup Levels
mg/Kg = Milligrams per Kilogram (analogous to parts per million)
BGS = Below Ground Surface
N/A = Not Applicable
MSCC = Maximum Soil Contaminant Concentration
* = Analyzed by Mobile Lab
NS = No Standard
ND = Not Detected
Table 2 - Summary of Soil Analytical Results
Analytical Method
Dodson's Amoco
Mebane, North Carolina
VPH8260
Standards
NC Action Level (mg/Kg)
Soil-to-Groundwater MSCC (mg/Kg)
Residential Soil Cleanup Levels (mg/Kg)
Industrial/Commercial Soil Cleanup Levels (mg/Kg)

APPENDIX A
UST-2A Site Investigation Report for Permanent Closure or Change-in-
Service of
REGISTERED UST

Return completed form to:
NC DEQ / DWM / UST SECTION
1646 MAIL SERVICE CENTER
RALEIGH, NC 27699-1646
ATTN: REGISTRATION & PERMITTING

phone [phone] fax [phone] http://www.wastenotnc.org/

STATE USE ONLY:
Facility ID #

Date Received

INSTRUCTIONS (READ THIS FIRST)
1. UST permanent closure or change in service must be completed in accordance with the latest version of the Guidelines for Site Checks, Tank
Closure and Initial Response and Abatement. The guidelines can be obtained at http://deq.nc.gov/about/divisions/waste-management/waste-
management-permit-guidance/underground-storage-tanks-section.
2. Permanent closure: Complete all sections of this form.
3. Change-in-service: Where a UST system will be converted from storing a regulated substance to a non-regulated substance, complete sections I, II,
III, IV, and VI
4. For more than 5 registered UST systems, attach additional forms as needed
5. Tank Fee Refund: An annual tank fee may be refunded for a tank for which a tank fee was not required. An owner or operator must submit
a written request and include: (1) contact information, (2) federal identification # or SSN, and (3) a copy of UST-2 form. The annual tank
fee will be prorated based on the date of permanent closure.
6. UNREGISTERED USTs use Form UST-2B
I. OWNERSHIP OF TANKS II. LOCATION OF TANKS
Owner Name (Corporation, Individual, Public Agency, or Other Entity)
McLeod Oil Company, Inc.
Facility Name or Company
Dodson's Amoco
Street Address
PO Box 100
Facility ID # (If known)
00-0-0000023229
City
Mebane
County
Alamance
Street Address
306 West Center Street
State
NC
Zip Code
27302
City
Mebane
County
Alamance
Zip Code
27302
Phone Number
919-563-3172
Phone Number
563-3172
III. CONTACT PERSONNEL
Contact for Facility:
Michael Tompkins
Job Title:
Owner Representative
Phone #:
919-563-3172
Closure Contractor Name:
Eric McManus
Closure Contractor Company:
D.H. Griffin Wrecking Company
Address:
Greensboro, NC
Phone #
336-214-9012
Primary Consultant Name:
Jason Ricks
Primary Consultant Company:
Pilot Geological, PLLC
Address:
Kernersville, NC
Phone #
336-870-3095
IV. UST INFORMATION FOR REGISTERED UST SYSTEMS
UNREGISTERED USTs use Form UST-2B
V. EXCAVATION CONDITION
Tank ID
No.
Size in
Gallons
Last
Contents
Last
Use
Date
Permanent
Close Date
Method of Permanent Closure:
Indicate REMOVED or enter fill
material, such as foam/
concrete/ sand
Change-in-
Service
Date
Water in
excavation Free product
Notable
odor or
visible soil
contaminatio
n
Yes No Yes No Yes No
1 2000 Gasoline, Gas Mix2/11 4/20/21 Removed
2 2000 Gasoline, Gas Mix2/11 4/20/21 Removed
3 2000 Gasoline, Gas Mix2/11 4/20/21 Removed

VI. CERTIFICATION
I certify under penalty of law that I have personally examined and am familiar with the information submitted in this and all attached documents and that
based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the submitted information is true accurate
and complete.
Print name and official title of owner or owner’s authorized representative
Jason Ricks, Licensed Geologist - Agent
Signature Date Signed
4/5/23
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE [phone] FAX [phone] http://www.wastenotnc.org/ 1/2016
UST-3 Notice of Intent: UST Permanent Closure or Change-in-Service
Return completed form to:
The DWM Regional Office located in the area where the facility is located. Also send a copy to the Central Office in Raleigh.
SEE MAP ON THE BACK OF THIS FORM FOR THE CENTRAL AND REGIONAL OFFICE ADDRESSES.
STATE USE ONLY

I.D. #_____________________

Date Received______________
INSTRUCTIONS (READ THIS FIRST)
Complete and return a UST-3 form at least thirty (30) days prior to closure or change-in-service activities.
Completed UST closure or change-in-service site assessment reports, along with a copy of the UST-2A and/or 2B forms, should be submitted
to the appropriate Division of Waste Management (DWM) Regional Office within thirty (30) days following closure activities. The UST-2 form
should also be submitted to the Central Office in Raleigh so that the status of the tanks may be changed to permanently closed and your
tank fee account can be closed out. Note: Tank fees may be due for unregistered tanks.
UST closure and change-in-service site assessments must be completed in accordance with the latest version of the Guidelines for Site
Checks, Tank Closure and Initial Response. The guidelines can be obtained at https://deq.nc.gov/about/divisions/waste-management/ust.
Note: To close tanks in place you must obtain prior approval from the DWM Regional office located in the region where the facility is located.
You must make sure that USTs removed from your property are disposed of properly. When choosing a closure contractor, ask where the
tank(s) will be taken for disposal. Usually, USTs are cleaned and cut up for scrap metal. This is dangerous work and must be performed
by a qualified company. Tanks disposed of illegally in fields or other dumpsites can leak petroleum products and sludge into the environment.
If your tanks are disposed of improperly, you could be held responsible for the cleanup of any environmental damage that occurs.
I. OWNERSHIP OF TANKS II. LOCATION
Owner Name (Corporation, Individual, Public Agency, or Other Entity)
McLeod Oil Company, Inc.
Facility Name or Company
Dodson's Amoco
Street Address
PO Box 100
Facility ID # (If known)
0000023229
City
Mebane
County
Alamance
Street Address
306 West Center Street
State
NC
Zip Code
27302
City
Mebane
County
Alamance
Zip Code
27302
Phone Number
919-563-3172
Email
[e-mail]
Phone Number
563-3172
III. CONTACT PERSONNEL
Name:
Jason Ricks
Company Name:
Pilot Geological, PLLC
Job Title:
Geologist
Phone Number:
870-3095
IV. TANK REMOVAL, CLOSURE IN PLACE, CHANGE-IN SERVICE
1. Contact local fire marshal.
2. Plan entire closure event.
3. Conduct Site Soil Assessment.
4. If removing tanks or closing in place, refer to
API Publication 2015 Cleaning Petroleum
Storage Tanks and 1604 Removal and
Disposal of Used Underground Petroleum
Storage Tanks.
5. Provide a sketch locating piping, tanks and
soil sampling locations.
6. Submit a closure report in the format of UST-
12 (including the form UST-2) within thirty
(30) days following the site investigation.
7. If a release from the tanks has occurred, the
site assessment portion of the tank closure
must be conducted under the supervision of
a P.E. or L.G., with all closure site assessment
reports bearing the signature and seal of the
P.E. or L.G. If a release has not occurred, the
supervision, signature or seal of a P.E. or L.G.
is not required.
8. Keep closure records for three (3) years.
V. WORK TO BE PERFORMED BY
Contractor Name:
Eric McManus
Contractor Company Name:
DH Griffin Wrecking Company, Inc.
Address:
4716 Hilltop Road, Greensboro
State:
NC
Zip Code:
27407
Phone No:
336-214-9012
Primary Consultant Name:
Jason Ricks
Primary Consultant Company Name:
Pilot Geological, PLLC
Consultant Phone No:
336-870-3095
VI. TANKS SCHEDULED FOR CLOSURE OR CHANGE-IN-SERVICE

Tank ID No.

Size in Gallons

Last Contents
Proposed Activity
Closure Change-In-Service
Removal Abandonment in Place * New Contents Stored
1 2000 Gasoline, Gas Mix
2 2000 Gasoline, Gas Mix
3 2000 Gasoline, Gas Mix

* Prior written approval to abandon a tank in place must be received from a DWM Regional Office.
VII. OWNER OR OWNER’S AUTHORIZED REPRESENTATIVE
Has a release from a UST system occurred at this location? Yes No Unknown
I understand that I can be held responsible for environmental damage resulting from the improper disposal of my USTs.
Print name and official title: Jason Ricks, Principal Geologist
Signature Date Signed
2/23/23
SCHEDULED REMOVAL DATE
3/20/23
Notify your DWM Regional Office
48 hours before this date if
scheduled removal date changes
UST-3 Rev 2/2021

APPENDIX B

APPENDIX C
Hydrocarbon Analysis Results
Client:PILOT Samples taken Tuesday, March 21, 2023
Address:Samples extracted Tuesday, March 21, 2023
Samples analysed Tuesday, March 21, 2023
Contact:JASON RICKS Operator MAX MOYER
Project:DODSON'S AMOCO
5 F03640
Matrix Sample ID Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid %
heavy
s C-1 0900 903.0 1260 3300 <22.6 3300 139.9 <7.2 <0.9 99.9 0.1 0 Deg.Gas 93.4%,(FCM)
s C-2 0902 1159.0 1062 2205 <29 2205 92.8 <9.3 <1.2 99.9 0.1 0 Deg.Gas 92.7%,(FCM)
s C-3 0903 1025.0 1281 2973 <25.6 2973 147.8 <8.2 <1 99.9 0.1 0 Deg.Gas 92%,(FCM)
s C-4 0907 756.0 885 1671 <18.9 1671 65.1 <6 <0.76 99.8 0.1 0 Deg.Gas 87.3%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 112.3 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:PILOT Samples taken Tuesday, March 21, 2023
Address:Samples extracted Tuesday, March 21, 2023
Samples analysed Tuesday, March 21, 2023
Contact:JASON RICKS Operator MAX MOYER
Project:DODSON'S AMOCO
1 F03640
Matrix Sample ID Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid %
heavy
s C-5 1115 935.0 2601 6029 <23.4 6029 280.9 10.9 <0.94 99.9 0.1 0 Deg.Gas 91.8%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 97.9 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
#=CL#
March 28, 2023
LIMS USE: FR - JASON RICKS
LIMS OBJECT ID: 92657761
92657761
Project:
Pace Project No.:
RE:
Jason Ricks
Pilot Geological
P.O. Box 128
Kernersville, NC 27285
G-8098
Dear Jason Ricks:
Enclosed are the analytical results for sample(s) received by the laboratory on March 20, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stephanie Knott
[e-mail]
Project Manager
704-977-0981
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 1 of 14
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92657761
G-8098
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 2 of 14
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92657761
G-8098
Lab ID Sample ID Matrix Date Collected Date Received
92657761001 D-1 Solid 03/20/23 09:45 03/20/23 16:15
92657761002 D-2 Solid 03/20/23 09:50 03/20/23 16:15
92657761003 D-3 Solid 03/20/23 09:55 03/20/23 16:15
92657761004 T-1 Solid 03/20/23 14:55 03/20/23 16:15
92657761005 T-2 Solid 03/20/23 15:08 03/20/23 16:15
92657761006 T-3 Solid 03/20/23 14:50 03/20/23 16:15
92657761007 T-4 Solid 03/20/23 15:12 03/20/23 16:15
92657761008 T-5 Solid 03/20/23 14:35 03/20/23 16:15
92657761009 T-6 Solid 03/20/23 15:18 03/20/23 16:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 3 of 14
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92657761
G-8098
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92657761001 D-1 EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92657761002 D-2 EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92657761003 D-3 EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92657761004 T-1 EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92657761005 T-2 EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92657761006 T-3 EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92657761007 T-4 EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92657761008 T-5 EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92657761009 T-6 EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 4 of 14
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92657761
G-8098
Sample:D-1 Lab ID:92657761001 Collected:03/20/23 09:45 Received:03/20/23 16:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 03/22/23 19:5203/22/23 16:529.2 1
Surrogates
4-Bromofluorobenzene (S)99 %03/22/23 19:52 460-00-403/22/23 16:5266-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 26.4 %03/21/23 16:35 N20.10 1
Sample:D-2 Lab ID:92657761002 Collected:03/20/23 09:50 Received:03/20/23 16:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 03/22/23 20:4403/22/23 16:529.5 1
Surrogates
4-Bromofluorobenzene (S)100 %03/22/23 20:44 460-00-403/22/23 16:5266-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 26.6 %03/21/23 16:36 N20.10 1
Sample:D-3 Lab ID:92657761003 Collected:03/20/23 09:55 Received:03/20/23 16:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 03/22/23 21:0903/22/23 16:52101
Surrogates
4-Bromofluorobenzene (S)102 %03/22/23 21:09 460-00-403/22/23 16:5266-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 28.5 %03/21/23 16:36 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:09 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 5 of 14
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92657761
G-8098
Sample:T-1 Lab ID:92657761004 Collected:03/20/23 14:55 Received:03/20/23 16:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)889 mg/kg 03/22/23 21:3503/22/23 16:5211.3 1
Surrogates
4-Bromofluorobenzene (S)160 %03/22/23 21:35 460-00-4 S503/22/23 16:5266-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 35.1 %03/21/23 16:36 N20.10 1
Sample:T-2 Lab ID:92657761005 Collected:03/20/23 15:08 Received:03/20/23 16:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)542 mg/kg 03/23/23 21:38 D303/23/23 17:4121.9 2
Surrogates
4-Bromofluorobenzene (S)169 %03/23/23 21:38 460-00-4 S203/23/23 17:4166-130 2
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 30.7 %03/21/23 16:36 N20.10 1
Sample:T-3 Lab ID:92657761006 Collected:03/20/23 14:50 Received:03/20/23 16:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)17100 mg/kg 03/23/23 22:3003/23/23 17:4122520
Surrogates
4-Bromofluorobenzene (S)138 %03/23/23 22:30 460-00-4 S203/23/23 17:4166-130 20
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 32.0 %03/21/23 16:36 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:09 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 6 of 14
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92657761
G-8098
Sample:T-4 Lab ID:92657761007 Collected:03/20/23 15:12 Received:03/20/23 16:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)19200 mg/kg 03/23/23 22:5503/23/23 17:4129525
Surrogates
4-Bromofluorobenzene (S)121 %03/23/23 22:55 460-00-403/23/23 17:4166-130 25
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 33.2 %03/21/23 16:36 N20.10 1
Sample:T-5 Lab ID:92657761008 Collected:03/20/23 14:35 Received:03/20/23 16:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)17300 mg/kg 03/23/23 23:2103/23/23 17:4128425
Surrogates
4-Bromofluorobenzene (S)109 %03/23/23 23:21 460-00-403/23/23 17:4166-130 25
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 30.8 %03/21/23 16:36 N20.10 1
Sample:T-6 Lab ID:92657761009 Collected:03/20/23 15:18 Received:03/20/23 16:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)6970 mg/kg 03/23/23 22:0403/23/23 17:4113112.5
Surrogates
4-Bromofluorobenzene (S)117 %03/23/23 22:04 460-00-403/23/23 17:4166-130 12.5
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 28.5 %03/21/23 16:36 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:09 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 7 of 14
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657761
G-8098
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
763094
EPA 5030B
EPA 8015C
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92657761001, 92657761002, 92657761003, 92657761004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3963295
Associated Lab Samples:92657761001, 92657761002, 92657761003, 92657761004
Matrix:Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 03/22/23 19:26
4-Bromofluorobenzene (S)%99 66-130 03/22/23 19:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3963296LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 49.749.8 100 70-130
4-Bromofluorobenzene (S)%100 66-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3963298MATRIX SPIKE SAMPLE:
MSSpike
Result
92657761002
Gas Range Organics (C6-C10)mg/kg 93.478.8 116 57-154ND
4-Bromofluorobenzene (S)%103 66-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92657761001
3963297SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg ND 30ND
4-Bromofluorobenzene (S)%9999
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:09 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 8 of 14
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657761
G-8098
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
763430
EPA 5030B
EPA 8015C
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92657761005, 92657761006, 92657761007, 92657761008, 92657761009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3965086
Associated Lab Samples:92657761005, 92657761006, 92657761007, 92657761008, 92657761009
Matrix:Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 03/23/23 19:55
4-Bromofluorobenzene (S)%98 66-130 03/23/23 19:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3965087LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 51.350.4 102 70-130
4-Bromofluorobenzene (S)%102 66-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3965089MATRIX SPIKE SAMPLE:
MSSpike
Result
92657732001
Gas Range Organics (C6-C10)mg/kg 76.373.6 100 57-154ND
4-Bromofluorobenzene (S)%102 66-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92658478001
3965088SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg ND 30ND
4-Bromofluorobenzene (S)%9696
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:09 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 9 of 14
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657761
G-8098
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
762784
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92657761001, 92657761002, 92657761003, 92657761004, 92657761005, 92657761006, 92657761007,
92657761008, 92657761009
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92657840018
3961512SAMPLE DUPLICATE:
Percent Moisture %11.5 N222511.2
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92657761009
3961513SAMPLE DUPLICATE:
Percent Moisture %27.5 N242528.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:09 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 10 of 14
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92657761
G-8098
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).S2
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:09 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 11 of 14
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92657761
G-8098
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92657761001 763094 763110D-1 EPA 5030B EPA 8015C
92657761002 763094 763110D-2 EPA 5030B EPA 8015C
92657761003 763094 763110D-3 EPA 5030B EPA 8015C
92657761004 763094 763110T-1 EPA 5030B EPA 8015C
92657761005 763430 763437T-2 EPA 5030B EPA 8015C
92657761006 763430 763437T-3 EPA 5030B EPA 8015C
92657761007 763430 763437T-4 EPA 5030B EPA 8015C
92657761008 763430 763437T-5 EPA 5030B EPA 8015C
92657761009 763430 763437T-6 EPA 5030B EPA 8015C
92657761001 762784D-1 SW-846
92657761002 762784D-2 SW-846
92657761003 762784D-3 SW-846
92657761004 762784T-1 SW-846
92657761005 762784T-2 SW-846
92657761006 762784T-3 SW-846
92657761007 762784T-4 SW-846
92657761008 762784T-5 SW-846
92657761009 762784T-6 SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:09 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 12 of 14
Pa
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Page 14 of 14
#=CL#
April 03, 2023
LIMS USE: FR - JASON RICKS
LIMS OBJECT ID: 92657988
92657988
Project:
Pace Project No.:
RE:
Jason Ricks
Pilot Geological
P.O. Box 128
Kernersville, NC 27285
G-8098 Dodsons
Dear Jason Ricks:
Enclosed are the analytical results for sample(s) received by the laboratory on March 21, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stephanie Knott
[e-mail]
Project Manager
704-977-0981
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 1 of 63
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 2 of 63
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Lab ID Sample ID Matrix Date Collected Date Received
92657988001 N-1 Solid 03/21/23 11:30 03/21/23 13:10
92657988002 E-1 Solid 03/21/23 09:30 03/21/23 13:10
92657988003 S-1 Solid 03/21/23 09:20 03/21/23 13:10
92657988004 W-1 Solid 03/21/23 09:10 03/21/23 13:10
92657988005 B-1 Solid 03/21/23 12:00 03/21/23 13:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 3 of 63
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92657988001 N-1 EPA 8260D 71 PASI-CLMB
SW-846 1 PASI-CKDF
92657988002 E-1 EPA 8260D 71 PASI-CCL
SW-846 1 PASI-CKDF
92657988003 S-1 EPA 8260D 71 PASI-CCL
SW-846 1 PASI-CKDF
92657988004 W-1 EPA 8260D 71 PASI-CLMB
SW-846 1 PASI-CKDF
92657988005 B-1 EPA 8260D 71 PASI-CLMB
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 4 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Sample:N-1 Lab ID:92657988001 Collected:03/21/23 11:30 Received:03/21/23 13:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 03/28/23 20:30 67-64-103/28/23 17:120.19 1
Benzene 0.055 mg/kg 03/28/23 20:30 71-43-203/28/23 17:120.0095 1
Bromobenzene ND mg/kg 03/28/23 20:30 108-86-103/28/23 17:120.0095 1
Bromochloromethane ND mg/kg 03/28/23 20:30 74-97-503/28/23 17:120.0095 1
Bromodichloromethane ND mg/kg 03/28/23 20:30 75-27-403/28/23 17:120.0095 1
Bromoform ND mg/kg 03/28/23 20:30 75-25-203/28/23 17:120.0095 1
Bromomethane ND mg/kg 03/28/23 20:30 74-83-9 v203/28/23 17:120.038 1
2-Butanone (MEK)ND mg/kg 03/28/23 20:30 78-93-303/28/23 17:120.19 1
n-Butylbenzene 0.10 mg/kg 03/28/23 20:30 104-51-803/28/23 17:120.0095 1
sec-Butylbenzene 0.028 mg/kg 03/28/23 20:30 135-98-803/28/23 17:120.0095 1
tert-Butylbenzene ND mg/kg 03/28/23 20:30 98-06-603/28/23 17:120.0095 1
Carbon tetrachloride ND mg/kg 03/28/23 20:30 56-23-503/28/23 17:120.0095 1
Chlorobenzene ND mg/kg 03/28/23 20:30 108-90-703/28/23 17:120.0095 1
Chloroethane ND mg/kg 03/28/23 20:30 75-00-303/28/23 17:120.019 1
Chloroform ND mg/kg 03/28/23 20:30 67-66-303/28/23 17:120.0095 1
Chloromethane ND mg/kg 03/28/23 20:30 74-87-303/28/23 17:120.019 1
2-Chlorotoluene ND mg/kg 03/28/23 20:30 95-49-803/28/23 17:120.0095 1
4-Chlorotoluene ND mg/kg 03/28/23 20:30 106-43-403/28/23 17:120.0095 1
1,2-Dibromo-3-chloropropane ND mg/kg 03/28/23 20:30 96-12-803/28/23 17:120.0095 1
Dibromochloromethane ND mg/kg 03/28/23 20:30 124-48-103/28/23 17:120.0095 1
1,2-Dibromoethane (EDB)ND mg/kg 03/28/23 20:30 106-93-403/28/23 17:120.0095 1
Dibromomethane ND mg/kg 03/28/23 20:30 74-95-303/28/23 17:120.0095 1
1,2-Dichlorobenzene ND mg/kg 03/28/23 20:30 95-50-103/28/23 17:120.0095 1
1,3-Dichlorobenzene ND mg/kg 03/28/23 20:30 541-73-103/28/23 17:120.0095 1
1,4-Dichlorobenzene ND mg/kg 03/28/23 20:30 106-46-703/28/23 17:120.0095 1
Dichlorodifluoromethane ND mg/kg 03/28/23 20:30 75-71-803/28/23 17:120.019 1
1,1-Dichloroethane ND mg/kg 03/28/23 20:30 75-34-303/28/23 17:120.0095 1
1,2-Dichloroethane ND mg/kg 03/28/23 20:30 107-06-203/28/23 17:120.0095 1
1,1-Dichloroethene ND mg/kg 03/28/23 20:30 75-35-403/28/23 17:120.0095 1
cis-1,2-Dichloroethene ND mg/kg 03/28/23 20:30 156-59-203/28/23 17:120.0095 1
trans-1,2-Dichloroethene ND mg/kg 03/28/23 20:30 156-60-503/28/23 17:120.0095 1
1,2-Dichloropropane ND mg/kg 03/28/23 20:30 78-87-503/28/23 17:120.0095 1
1,3-Dichloropropane ND mg/kg 03/28/23 20:30 142-28-903/28/23 17:120.0095 1
2,2-Dichloropropane ND mg/kg 03/28/23 20:30 594-20-703/28/23 17:120.0095 1
1,1-Dichloropropene ND mg/kg 03/28/23 20:30 563-58-603/28/23 17:120.0095 1
cis-1,3-Dichloropropene ND mg/kg 03/28/23 20:30 10061-01-503/28/23 17:120.0095 1
trans-1,3-Dichloropropene ND mg/kg 03/28/23 20:30 10061-02-603/28/23 17:120.0095 1
Diisopropyl ether ND mg/kg 03/28/23 20:30 108-20-303/28/23 17:120.0095 1
Ethanol ND mg/kg 03/28/23 20:30 64-17-503/28/23 17:120.38 1
Ethylbenzene 0.74 mg/kg 03/28/23 20:30 100-41-403/28/23 17:120.0095 1
Hexachloro-1,3-butadiene ND mg/kg 03/28/23 20:30 87-68-303/28/23 17:120.019 1
2-Hexanone ND mg/kg 03/28/23 20:30 591-78-603/28/23 17:120.095 1
Isopropylbenzene (Cumene)0.081 mg/kg 03/28/23 20:30 98-82-803/28/23 17:120.0095 1
p-Isopropyltoluene 0.076 mg/kg 03/28/23 20:30 99-87-603/28/23 17:120.0095 1
Methylene Chloride ND mg/kg 03/28/23 20:30 75-09-203/28/23 17:120.038 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 5 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Sample:N-1 Lab ID:92657988001 Collected:03/21/23 11:30 Received:03/21/23 13:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND mg/kg 03/28/23 20:30 108-10-103/28/23 17:120.095 1
Methyl-tert-butyl ether ND mg/kg 03/28/23 20:30 1634-04-403/28/23 17:120.0095 1
Naphthalene 0.16 mg/kg 03/28/23 20:30 91-20-303/28/23 17:120.0095 1
n-Propylbenzene 0.25 mg/kg 03/28/23 20:30 103-65-103/28/23 17:120.0095 1
Styrene ND mg/kg 03/28/23 20:30 100-42-503/28/23 17:120.0095 1
1,1,1,2-Tetrachloroethane ND mg/kg 03/28/23 20:30 630-20-603/28/23 17:120.0095 1
1,1,2,2-Tetrachloroethane ND mg/kg 03/28/23 20:30 79-34-503/28/23 17:120.0095 1
Tetrachloroethene ND mg/kg 03/28/23 20:30 127-18-403/28/23 17:120.0095 1
Toluene 0.73 mg/kg 03/28/23 20:30 108-88-303/28/23 17:120.0095 1
1,2,3-Trichlorobenzene ND mg/kg 03/28/23 20:30 87-61-603/28/23 17:120.0095 1
1,2,4-Trichlorobenzene ND mg/kg 03/28/23 20:30 120-82-103/28/23 17:120.0095 1
1,1,1-Trichloroethane ND mg/kg 03/28/23 20:30 71-55-603/28/23 17:120.0095 1
1,1,2-Trichloroethane ND mg/kg 03/28/23 20:30 79-00-503/28/23 17:120.0095 1
Trichloroethene ND mg/kg 03/28/23 20:30 79-01-603/28/23 17:120.0095 1
Trichlorofluoromethane ND mg/kg 03/28/23 20:30 75-69-403/28/23 17:120.0095 1
1,2,3-Trichloropropane ND mg/kg 03/28/23 20:30 96-18-403/28/23 17:120.0095 1
1,2,4-Trimethylbenzene 1.5 mg/kg 03/28/23 20:30 95-63-603/28/23 17:120.0095 1
1,3,5-Trimethylbenzene 0.45 mg/kg 03/28/23 20:30 108-67-803/28/23 17:120.0095 1
Vinyl acetate ND mg/kg 03/28/23 20:30 108-05-403/28/23 17:120.095 1
Vinyl chloride ND mg/kg 03/28/23 20:30 75-01-403/28/23 17:120.019 1
Xylene (Total)2.7 mg/kg 03/28/23 20:30 1330-20-703/28/23 17:120.019 1
m&p-Xylene 2.1 mg/kg 03/28/23 20:30 179601-23-103/28/23 17:120.019 1
o-Xylene 0.60 mg/kg 03/28/23 20:30 95-47-603/28/23 17:120.0095 1
Surrogates
Toluene-d8 (S)103 %03/28/23 20:30 2037-26-503/28/23 17:1270-130 1
4-Bromofluorobenzene (S)98 %03/28/23 20:30 460-00-403/28/23 17:1270-130 1
1,2-Dichloroethane-d4 (S)102 %03/28/23 20:30 17060-07-003/28/23 17:1270-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 31.8 %03/22/23 15:47 N20.10 1
Sample:E-1 Lab ID:92657988002 Collected:03/21/23 09:30 Received:03/21/23 13:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 03/28/23 00:03 67-64-103/27/23 17:120.21 1
Benzene ND mg/kg 03/28/23 00:03 71-43-203/27/23 17:120.010 1
Bromobenzene ND mg/kg 03/28/23 00:03 108-86-103/27/23 17:120.010 1
Bromochloromethane ND mg/kg 03/28/23 00:03 74-97-503/27/23 17:120.010 1
Bromodichloromethane ND mg/kg 03/28/23 00:03 75-27-403/27/23 17:120.010 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 6 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Sample:E-1 Lab ID:92657988002 Collected:03/21/23 09:30 Received:03/21/23 13:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Bromoform ND mg/kg 03/28/23 00:03 75-25-203/27/23 17:120.010 1
Bromomethane ND mg/kg 03/28/23 00:03 74-83-9 v203/27/23 17:120.041 1
2-Butanone (MEK)ND mg/kg 03/28/23 00:03 78-93-303/27/23 17:120.21 1
n-Butylbenzene ND mg/kg 03/28/23 00:03 104-51-803/27/23 17:120.010 1
sec-Butylbenzene ND mg/kg 03/28/23 00:03 135-98-803/27/23 17:120.010 1
tert-Butylbenzene ND mg/kg 03/28/23 00:03 98-06-603/27/23 17:120.010 1
Carbon tetrachloride ND mg/kg 03/28/23 00:03 56-23-503/27/23 17:120.010 1
Chlorobenzene ND mg/kg 03/28/23 00:03 108-90-703/27/23 17:120.010 1
Chloroethane ND mg/kg 03/28/23 00:03 75-00-303/27/23 17:120.021 1
Chloroform ND mg/kg 03/28/23 00:03 67-66-303/27/23 17:120.010 1
Chloromethane ND mg/kg 03/28/23 00:03 74-87-303/27/23 17:120.021 1
2-Chlorotoluene ND mg/kg 03/28/23 00:03 95-49-803/27/23 17:120.010 1
4-Chlorotoluene ND mg/kg 03/28/23 00:03 106-43-403/27/23 17:120.010 1
1,2-Dibromo-3-chloropropane ND mg/kg 03/28/23 00:03 96-12-803/27/23 17:120.010 1
Dibromochloromethane ND mg/kg 03/28/23 00:03 124-48-103/27/23 17:120.010 1
1,2-Dibromoethane (EDB)ND mg/kg 03/28/23 00:03 106-93-403/27/23 17:120.010 1
Dibromomethane ND mg/kg 03/28/23 00:03 74-95-303/27/23 17:120.010 1
1,2-Dichlorobenzene ND mg/kg 03/28/23 00:03 95-50-103/27/23 17:120.010 1
1,3-Dichlorobenzene ND mg/kg 03/28/23 00:03 541-73-103/27/23 17:120.010 1
1,4-Dichlorobenzene ND mg/kg 03/28/23 00:03 106-46-703/27/23 17:120.010 1
Dichlorodifluoromethane ND mg/kg 03/28/23 00:03 75-71-803/27/23 17:120.021 1
1,1-Dichloroethane ND mg/kg 03/28/23 00:03 75-34-303/27/23 17:120.010 1
1,2-Dichloroethane ND mg/kg 03/28/23 00:03 107-06-203/27/23 17:120.010 1
1,1-Dichloroethene ND mg/kg 03/28/23 00:03 75-35-403/27/23 17:120.010 1
cis-1,2-Dichloroethene ND mg/kg 03/28/23 00:03 156-59-203/27/23 17:120.010 1
trans-1,2-Dichloroethene ND mg/kg 03/28/23 00:03 156-60-503/27/23 17:120.010 1
1,2-Dichloropropane ND mg/kg 03/28/23 00:03 78-87-503/27/23 17:120.010 1
1,3-Dichloropropane ND mg/kg 03/28/23 00:03 142-28-903/27/23 17:120.010 1
2,2-Dichloropropane ND mg/kg 03/28/23 00:03 594-20-703/27/23 17:120.010 1
1,1-Dichloropropene ND mg/kg 03/28/23 00:03 563-58-603/27/23 17:120.010 1
cis-1,3-Dichloropropene ND mg/kg 03/28/23 00:03 10061-01-503/27/23 17:120.010 1
trans-1,3-Dichloropropene ND mg/kg 03/28/23 00:03 10061-02-603/27/23 17:120.010 1
Diisopropyl ether ND mg/kg 03/28/23 00:03 108-20-303/27/23 17:120.010 1
Ethanol ND mg/kg 03/28/23 00:03 64-17-503/27/23 17:120.41 1
Ethylbenzene ND mg/kg 03/28/23 00:03 100-41-403/27/23 17:120.010 1
Hexachloro-1,3-butadiene ND mg/kg 03/28/23 00:03 87-68-303/27/23 17:120.021 1
2-Hexanone ND mg/kg 03/28/23 00:03 591-78-603/27/23 17:120.10 1
Isopropylbenzene (Cumene)ND mg/kg 03/28/23 00:03 98-82-803/27/23 17:120.010 1
p-Isopropyltoluene ND mg/kg 03/28/23 00:03 99-87-603/27/23 17:120.010 1
Methylene Chloride 0.076 mg/kg 03/28/23 00:03 75-09-2 C903/27/23 17:120.041 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 03/28/23 00:03 108-10-103/27/23 17:120.10 1
Methyl-tert-butyl ether ND mg/kg 03/28/23 00:03 1634-04-403/27/23 17:120.010 1
Naphthalene ND mg/kg 03/28/23 00:03 91-20-303/27/23 17:120.010 1
n-Propylbenzene ND mg/kg 03/28/23 00:03 103-65-103/27/23 17:120.010 1
Styrene ND mg/kg 03/28/23 00:03 100-42-503/27/23 17:120.010 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 7 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Sample:E-1 Lab ID:92657988002 Collected:03/21/23 09:30 Received:03/21/23 13:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1,1,2-Tetrachloroethane ND mg/kg 03/28/23 00:03 630-20-603/27/23 17:120.010 1
1,1,2,2-Tetrachloroethane ND mg/kg 03/28/23 00:03 79-34-503/27/23 17:120.010 1
Tetrachloroethene ND mg/kg 03/28/23 00:03 127-18-403/27/23 17:120.010 1
Toluene ND mg/kg 03/28/23 00:03 108-88-303/27/23 17:120.010 1
1,2,3-Trichlorobenzene ND mg/kg 03/28/23 00:03 87-61-603/27/23 17:120.010 1
1,2,4-Trichlorobenzene ND mg/kg 03/28/23 00:03 120-82-103/27/23 17:120.010 1
1,1,1-Trichloroethane ND mg/kg 03/28/23 00:03 71-55-603/27/23 17:120.010 1
1,1,2-Trichloroethane ND mg/kg 03/28/23 00:03 79-00-503/27/23 17:120.010 1
Trichloroethene ND mg/kg 03/28/23 00:03 79-01-603/27/23 17:120.010 1
Trichlorofluoromethane ND mg/kg 03/28/23 00:03 75-69-403/27/23 17:120.010 1
1,2,3-Trichloropropane ND mg/kg 03/28/23 00:03 96-18-403/27/23 17:120.010 1
1,2,4-Trimethylbenzene ND mg/kg 03/28/23 00:03 95-63-603/27/23 17:120.010 1
1,3,5-Trimethylbenzene ND mg/kg 03/28/23 00:03 108-67-803/27/23 17:120.010 1
Vinyl acetate ND mg/kg 03/28/23 00:03 108-05-403/27/23 17:120.10 1
Vinyl chloride ND mg/kg 03/28/23 00:03 75-01-403/27/23 17:120.021 1
Xylene (Total)ND mg/kg 03/28/23 00:03 1330-20-703/27/23 17:120.021 1
m&p-Xylene ND mg/kg 03/28/23 00:03 179601-23-103/27/23 17:120.021 1
o-Xylene ND mg/kg 03/28/23 00:03 95-47-603/27/23 17:120.010 1
Surrogates
Toluene-d8 (S)102 %03/28/23 00:03 2037-26-503/27/23 17:1270-130 1
4-Bromofluorobenzene (S)99 %03/28/23 00:03 460-00-403/27/23 17:1270-130 1
1,2-Dichloroethane-d4 (S)111 %03/28/23 00:03 17060-07-003/27/23 17:1270-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 27.1 %03/22/23 15:47 N20.10 1
Sample:S-1 Lab ID:92657988003 Collected:03/21/23 09:20 Received:03/21/23 13:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 03/30/23 08:12 67-64-103/29/23 22:4818.0 100
Benzene 1.9 mg/kg 03/30/23 08:12 71-43-203/29/23 22:480.90 100
Bromobenzene ND mg/kg 03/30/23 08:12 108-86-103/29/23 22:480.90 100
Bromochloromethane ND mg/kg 03/30/23 08:12 74-97-503/29/23 22:480.90 100
Bromodichloromethane ND mg/kg 03/30/23 08:12 75-27-403/29/23 22:480.90 100
Bromoform ND mg/kg 03/30/23 08:12 75-25-203/29/23 22:480.90 100
Bromomethane ND mg/kg 03/30/23 08:12 74-83-9 v203/29/23 22:483.6 100
2-Butanone (MEK)ND mg/kg 03/30/23 08:12 78-93-303/29/23 22:4818.0 100
n-Butylbenzene 25.6 mg/kg 03/30/23 08:12 104-51-803/29/23 22:480.90 100
sec-Butylbenzene ND mg/kg 03/30/23 08:12 135-98-803/29/23 22:480.90 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 8 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Sample:S-1 Lab ID:92657988003 Collected:03/21/23 09:20 Received:03/21/23 13:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
tert-Butylbenzene ND mg/kg 03/30/23 08:12 98-06-603/29/23 22:480.90 100
Carbon tetrachloride ND mg/kg 03/30/23 08:12 56-23-503/29/23 22:480.90 100
Chlorobenzene ND mg/kg 03/30/23 08:12 108-90-703/29/23 22:480.90 100
Chloroethane ND mg/kg 03/30/23 08:12 75-00-303/29/23 22:481.8 100
Chloroform ND mg/kg 03/30/23 08:12 67-66-303/29/23 22:480.90 100
Chloromethane ND mg/kg 03/30/23 08:12 74-87-303/29/23 22:481.8 100
2-Chlorotoluene ND mg/kg 03/30/23 08:12 95-49-803/29/23 22:480.90 100
4-Chlorotoluene ND mg/kg 03/30/23 08:12 106-43-403/29/23 22:480.90 100
1,2-Dibromo-3-chloropropane ND mg/kg 03/30/23 08:12 96-12-803/29/23 22:480.90 100
Dibromochloromethane ND mg/kg 03/30/23 08:12 124-48-103/29/23 22:480.90 100
1,2-Dibromoethane (EDB)ND mg/kg 03/30/23 08:12 106-93-403/29/23 22:480.90 100
Dibromomethane ND mg/kg 03/30/23 08:12 74-95-303/29/23 22:480.90 100
1,2-Dichlorobenzene ND mg/kg 03/30/23 08:12 95-50-103/29/23 22:480.90 100
1,3-Dichlorobenzene ND mg/kg 03/30/23 08:12 541-73-103/29/23 22:480.90 100
1,4-Dichlorobenzene ND mg/kg 03/30/23 08:12 106-46-703/29/23 22:480.90 100
Dichlorodifluoromethane ND mg/kg 03/30/23 08:12 75-71-8 v203/29/23 22:481.8 100
1,1-Dichloroethane ND mg/kg 03/30/23 08:12 75-34-303/29/23 22:480.90 100
1,2-Dichloroethane ND mg/kg 03/30/23 08:12 107-06-203/29/23 22:480.90 100
1,1-Dichloroethene ND mg/kg 03/30/23 08:12 75-35-403/29/23 22:480.90 100
cis-1,2-Dichloroethene ND mg/kg 03/30/23 08:12 156-59-203/29/23 22:480.90 100
trans-1,2-Dichloroethene ND mg/kg 03/30/23 08:12 156-60-503/29/23 22:480.90 100
1,2-Dichloropropane ND mg/kg 03/30/23 08:12 78-87-503/29/23 22:480.90 100
1,3-Dichloropropane ND mg/kg 03/30/23 08:12 142-28-903/29/23 22:480.90 100
2,2-Dichloropropane ND mg/kg 03/30/23 08:12 594-20-703/29/23 22:480.90 100
1,1-Dichloropropene ND mg/kg 03/30/23 08:12 563-58-603/29/23 22:480.90 100
cis-1,3-Dichloropropene ND mg/kg 03/30/23 08:12 10061-01-503/29/23 22:480.90 100
trans-1,3-Dichloropropene ND mg/kg 03/30/23 08:12 10061-02-603/29/23 22:480.90 100
Diisopropyl ether ND mg/kg 03/30/23 08:12 108-20-303/29/23 22:480.90 100
Ethanol ND mg/kg 03/30/23 08:12 64-17-503/29/23 22:4836.0 100
Ethylbenzene 140 mg/kg 03/30/23 08:12 100-41-403/29/23 22:480.90 100
Hexachloro-1,3-butadiene ND mg/kg 03/30/23 08:12 87-68-303/29/23 22:481.8 100
2-Hexanone ND mg/kg 03/30/23 08:12 591-78-603/29/23 22:489.0 100
Isopropylbenzene (Cumene)22.7 mg/kg 03/30/23 08:12 98-82-803/29/23 22:480.90 100
p-Isopropyltoluene 23.1 mg/kg 03/30/23 08:12 99-87-603/29/23 22:480.90 100
Methylene Chloride ND mg/kg 03/30/23 08:12 75-09-203/29/23 22:483.6 100
4-Methyl-2-pentanone (MIBK)ND mg/kg 03/30/23 08:12 108-10-103/29/23 22:489.0 100
Methyl-tert-butyl ether ND mg/kg 03/30/23 08:12 1634-04-403/29/23 22:480.90 100
Naphthalene 111 mg/kg 03/30/23 08:12 91-20-303/29/23 22:480.90 100
n-Propylbenzene 77.9 mg/kg 03/30/23 08:12 103-65-103/29/23 22:480.90 100
Styrene ND mg/kg 03/30/23 08:12 100-42-503/29/23 22:480.90 100
1,1,1,2-Tetrachloroethane ND mg/kg 03/30/23 08:12 630-20-603/29/23 22:480.90 100
1,1,2,2-Tetrachloroethane ND mg/kg 03/30/23 08:12 79-34-503/29/23 22:480.90 100
Tetrachloroethene ND mg/kg 03/30/23 08:12 127-18-403/29/23 22:480.90 100
Toluene 2.1 mg/kg 03/30/23 08:12 108-88-303/29/23 22:480.90 100
1,2,3-Trichlorobenzene ND mg/kg 03/30/23 08:12 87-61-603/29/23 22:480.90 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 9 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Sample:S-1 Lab ID:92657988003 Collected:03/21/23 09:20 Received:03/21/23 13:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2,4-Trichlorobenzene ND mg/kg 03/30/23 08:12 120-82-103/29/23 22:480.90 100
1,1,1-Trichloroethane ND mg/kg 03/30/23 08:12 71-55-603/29/23 22:480.90 100
1,1,2-Trichloroethane ND mg/kg 03/30/23 08:12 79-00-503/29/23 22:480.90 100
Trichloroethene ND mg/kg 03/30/23 08:12 79-01-603/29/23 22:480.90 100
Trichlorofluoromethane ND mg/kg 03/30/23 08:12 75-69-403/29/23 22:480.90 100
1,2,3-Trichloropropane ND mg/kg 03/30/23 08:12 96-18-403/29/23 22:480.90 100
1,2,4-Trimethylbenzene 538 mg/kg 03/30/23 08:12 95-63-603/29/23 22:480.90 100
1,3,5-Trimethylbenzene 159 mg/kg 03/30/23 08:12 108-67-803/29/23 22:480.90 100
Vinyl acetate ND mg/kg 03/30/23 08:12 108-05-403/29/23 22:489.0 100
Vinyl chloride ND mg/kg 03/30/23 08:12 75-01-403/29/23 22:481.8 100
Xylene (Total)522 mg/kg 03/30/23 08:12 1330-20-703/29/23 22:481.8 100
m&p-Xylene 512 mg/kg 03/30/23 08:12 179601-23-103/29/23 22:481.8 100
o-Xylene 9.2 mg/kg 03/30/23 08:12 95-47-603/29/23 22:480.90 100
Surrogates
Toluene-d8 (S)101 %03/30/23 08:12 2037-26-503/29/23 22:4870-130 100
4-Bromofluorobenzene (S)97 %03/30/23 08:12 460-00-403/29/23 22:4870-130 100
1,2-Dichloroethane-d4 (S)102 %03/30/23 08:12 17060-07-003/29/23 22:4870-130 100
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 31.3 %03/22/23 15:47 N20.10 1
Sample:W-1 Lab ID:92657988004 Collected:03/21/23 09:10 Received:03/21/23 13:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 03/28/23 18:01 67-64-103/28/23 17:120.19 1
Benzene ND mg/kg 03/28/23 18:01 71-43-203/28/23 17:120.0093 1
Bromobenzene ND mg/kg 03/28/23 18:01 108-86-103/28/23 17:120.0093 1
Bromochloromethane ND mg/kg 03/28/23 18:01 74-97-503/28/23 17:120.0093 1
Bromodichloromethane ND mg/kg 03/28/23 18:01 75-27-403/28/23 17:120.0093 1
Bromoform ND mg/kg 03/28/23 18:01 75-25-203/28/23 17:120.0093 1
Bromomethane ND mg/kg 03/28/23 18:01 74-83-9 v2,v303/28/23 17:120.037 1
2-Butanone (MEK)ND mg/kg 03/28/23 18:01 78-93-303/28/23 17:120.19 1
n-Butylbenzene ND mg/kg 03/28/23 18:01 104-51-803/28/23 17:120.0093 1
sec-Butylbenzene ND mg/kg 03/28/23 18:01 135-98-803/28/23 17:120.0093 1
tert-Butylbenzene ND mg/kg 03/28/23 18:01 98-06-603/28/23 17:120.0093 1
Carbon tetrachloride ND mg/kg 03/28/23 18:01 56-23-503/28/23 17:120.0093 1
Chlorobenzene ND mg/kg 03/28/23 18:01 108-90-703/28/23 17:120.0093 1
Chloroethane ND mg/kg 03/28/23 18:01 75-00-303/28/23 17:120.019 1
Chloroform ND mg/kg 03/28/23 18:01 67-66-303/28/23 17:120.0093 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 10 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Sample:W-1 Lab ID:92657988004 Collected:03/21/23 09:10 Received:03/21/23 13:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Chloromethane ND mg/kg 03/28/23 18:01 74-87-303/28/23 17:120.019 1
2-Chlorotoluene ND mg/kg 03/28/23 18:01 95-49-803/28/23 17:120.0093 1
4-Chlorotoluene ND mg/kg 03/28/23 18:01 106-43-403/28/23 17:120.0093 1
1,2-Dibromo-3-chloropropane ND mg/kg 03/28/23 18:01 96-12-803/28/23 17:120.0093 1
Dibromochloromethane ND mg/kg 03/28/23 18:01 124-48-103/28/23 17:120.0093 1
1,2-Dibromoethane (EDB)ND mg/kg 03/28/23 18:01 106-93-403/28/23 17:120.0093 1
Dibromomethane ND mg/kg 03/28/23 18:01 74-95-303/28/23 17:120.0093 1
1,2-Dichlorobenzene ND mg/kg 03/28/23 18:01 95-50-103/28/23 17:120.0093 1
1,3-Dichlorobenzene ND mg/kg 03/28/23 18:01 541-73-103/28/23 17:120.0093 1
1,4-Dichlorobenzene ND mg/kg 03/28/23 18:01 106-46-7 M103/28/23 17:120.0093 1
Dichlorodifluoromethane ND mg/kg 03/28/23 18:01 75-71-803/28/23 17:120.019 1
1,1-Dichloroethane ND mg/kg 03/28/23 18:01 75-34-303/28/23 17:120.0093 1
1,2-Dichloroethane ND mg/kg 03/28/23 18:01 107-06-203/28/23 17:120.0093 1
1,1-Dichloroethene ND mg/kg 03/28/23 18:01 75-35-403/28/23 17:120.0093 1
cis-1,2-Dichloroethene ND mg/kg 03/28/23 18:01 156-59-203/28/23 17:120.0093 1
trans-1,2-Dichloroethene ND mg/kg 03/28/23 18:01 156-60-503/28/23 17:120.0093 1
1,2-Dichloropropane ND mg/kg 03/28/23 18:01 78-87-503/28/23 17:120.0093 1
1,3-Dichloropropane ND mg/kg 03/28/23 18:01 142-28-903/28/23 17:120.0093 1
2,2-Dichloropropane ND mg/kg 03/28/23 18:01 594-20-703/28/23 17:120.0093 1
1,1-Dichloropropene ND mg/kg 03/28/23 18:01 563-58-603/28/23 17:120.0093 1
cis-1,3-Dichloropropene ND mg/kg 03/28/23 18:01 10061-01-503/28/23 17:120.0093 1
trans-1,3-Dichloropropene ND mg/kg 03/28/23 18:01 10061-02-603/28/23 17:120.0093 1
Diisopropyl ether ND mg/kg 03/28/23 18:01 108-20-303/28/23 17:120.0093 1
Ethanol ND mg/kg 03/28/23 18:01 64-17-5 M103/28/23 17:120.37 1
Ethylbenzene 0.018 mg/kg 03/28/23 18:01 100-41-403/28/23 17:120.0093 1
Hexachloro-1,3-butadiene ND mg/kg 03/28/23 18:01 87-68-303/28/23 17:120.019 1
2-Hexanone ND mg/kg 03/28/23 18:01 591-78-603/28/23 17:120.093 1
Isopropylbenzene (Cumene)ND mg/kg 03/28/23 18:01 98-82-803/28/23 17:120.0093 1
p-Isopropyltoluene ND mg/kg 03/28/23 18:01 99-87-603/28/23 17:120.0093 1
Methylene Chloride ND mg/kg 03/28/23 18:01 75-09-203/28/23 17:120.037 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 03/28/23 18:01 108-10-103/28/23 17:120.093 1
Methyl-tert-butyl ether ND mg/kg 03/28/23 18:01 1634-04-403/28/23 17:120.0093 1
Naphthalene ND mg/kg 03/28/23 18:01 91-20-3 M103/28/23 17:120.0093 1
n-Propylbenzene ND mg/kg 03/28/23 18:01 103-65-103/28/23 17:120.0093 1
Styrene 0.018 mg/kg 03/28/23 18:01 100-42-503/28/23 17:120.0093 1
1,1,1,2-Tetrachloroethane ND mg/kg 03/28/23 18:01 630-20-603/28/23 17:120.0093 1
1,1,2,2-Tetrachloroethane ND mg/kg 03/28/23 18:01 79-34-503/28/23 17:120.0093 1
Tetrachloroethene ND mg/kg 03/28/23 18:01 127-18-403/28/23 17:120.0093 1
Toluene ND mg/kg 03/28/23 18:01 108-88-303/28/23 17:120.0093 1
1,2,3-Trichlorobenzene ND mg/kg 03/28/23 18:01 87-61-6 M103/28/23 17:120.0093 1
1,2,4-Trichlorobenzene ND mg/kg 03/28/23 18:01 120-82-1 M103/28/23 17:120.0093 1
1,1,1-Trichloroethane ND mg/kg 03/28/23 18:01 71-55-603/28/23 17:120.0093 1
1,1,2-Trichloroethane ND mg/kg 03/28/23 18:01 79-00-503/28/23 17:120.0093 1
Trichloroethene ND mg/kg 03/28/23 18:01 79-01-603/28/23 17:120.0093 1
Trichlorofluoromethane ND mg/kg 03/28/23 18:01 75-69-403/28/23 17:120.0093 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 11 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Sample:W-1 Lab ID:92657988004 Collected:03/21/23 09:10 Received:03/21/23 13:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2,3-Trichloropropane ND mg/kg 03/28/23 18:01 96-18-403/28/23 17:120.0093 1
1,2,4-Trimethylbenzene ND mg/kg 03/28/23 18:01 95-63-603/28/23 17:120.0093 1
1,3,5-Trimethylbenzene ND mg/kg 03/28/23 18:01 108-67-803/28/23 17:120.0093 1
Vinyl acetate ND mg/kg 03/28/23 18:01 108-05-403/28/23 17:120.093 1
Vinyl chloride ND mg/kg 03/28/23 18:01 75-01-403/28/23 17:120.019 1
Xylene (Total)0.079 mg/kg 03/28/23 18:01 1330-20-703/28/23 17:120.019 1
m&p-Xylene 0.064 mg/kg 03/28/23 18:01 179601-23-103/28/23 17:120.019 1
o-Xylene 0.015 mg/kg 03/28/23 18:01 95-47-603/28/23 17:120.0093 1
Surrogates
Toluene-d8 (S)100 %03/28/23 18:01 2037-26-503/28/23 17:1270-130 1
4-Bromofluorobenzene (S)99 %03/28/23 18:01 460-00-403/28/23 17:1270-130 1
1,2-Dichloroethane-d4 (S)102 %03/28/23 18:01 17060-07-003/28/23 17:1270-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 30.6 %03/22/23 15:47 N20.10 1
Sample:B-1 Lab ID:92657988005 Collected:03/21/23 12:00 Received:03/21/23 13:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 03/28/23 22:03 67-64-103/28/23 17:129.4 50
Benzene 7.0 mg/kg 03/28/23 22:03 71-43-203/28/23 17:120.47 50
Bromobenzene ND mg/kg 03/28/23 22:03 108-86-103/28/23 17:120.47 50
Bromochloromethane ND mg/kg 03/28/23 22:03 74-97-503/28/23 17:120.47 50
Bromodichloromethane ND mg/kg 03/28/23 22:03 75-27-403/28/23 17:120.47 50
Bromoform ND mg/kg 03/28/23 22:03 75-25-203/28/23 17:120.47 50
Bromomethane ND mg/kg 03/28/23 22:03 74-83-9 v203/28/23 17:121.9 50
2-Butanone (MEK)ND mg/kg 03/28/23 22:03 78-93-303/28/23 17:129.4 50
n-Butylbenzene 20.7 mg/kg 03/28/23 22:03 104-51-803/28/23 17:120.47 50
sec-Butylbenzene 6.1 mg/kg 03/28/23 22:03 135-98-803/28/23 17:120.47 50
tert-Butylbenzene ND mg/kg 03/28/23 22:03 98-06-603/28/23 17:120.47 50
Carbon tetrachloride ND mg/kg 03/28/23 22:03 56-23-503/28/23 17:120.47 50
Chlorobenzene ND mg/kg 03/28/23 22:03 108-90-703/28/23 17:120.47 50
Chloroethane ND mg/kg 03/28/23 22:03 75-00-303/28/23 17:120.94 50
Chloroform ND mg/kg 03/28/23 22:03 67-66-303/28/23 17:120.47 50
Chloromethane ND mg/kg 03/28/23 22:03 74-87-303/28/23 17:120.94 50
2-Chlorotoluene ND mg/kg 03/28/23 22:03 95-49-803/28/23 17:120.47 50
4-Chlorotoluene ND mg/kg 03/28/23 22:03 106-43-403/28/23 17:120.47 50
1,2-Dibromo-3-chloropropane ND mg/kg 03/28/23 22:03 96-12-803/28/23 17:120.47 50
Dibromochloromethane ND mg/kg 03/28/23 22:03 124-48-103/28/23 17:120.47 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 12 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Sample:B-1 Lab ID:92657988005 Collected:03/21/23 12:00 Received:03/21/23 13:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dibromoethane (EDB)ND mg/kg 03/28/23 22:03 106-93-403/28/23 17:120.47 50
Dibromomethane ND mg/kg 03/28/23 22:03 74-95-303/28/23 17:120.47 50
1,2-Dichlorobenzene ND mg/kg 03/28/23 22:03 95-50-103/28/23 17:120.47 50
1,3-Dichlorobenzene ND mg/kg 03/28/23 22:03 541-73-103/28/23 17:120.47 50
1,4-Dichlorobenzene ND mg/kg 03/28/23 22:03 106-46-703/28/23 17:120.47 50
Dichlorodifluoromethane ND mg/kg 03/28/23 22:03 75-71-803/28/23 17:120.94 50
1,1-Dichloroethane ND mg/kg 03/28/23 22:03 75-34-303/28/23 17:120.47 50
1,2-Dichloroethane ND mg/kg 03/28/23 22:03 107-06-203/28/23 17:120.47 50
1,1-Dichloroethene ND mg/kg 03/28/23 22:03 75-35-403/28/23 17:120.47 50
cis-1,2-Dichloroethene ND mg/kg 03/28/23 22:03 156-59-203/28/23 17:120.47 50
trans-1,2-Dichloroethene ND mg/kg 03/28/23 22:03 156-60-503/28/23 17:120.47 50
1,2-Dichloropropane ND mg/kg 03/28/23 22:03 78-87-503/28/23 17:120.47 50
1,3-Dichloropropane ND mg/kg 03/28/23 22:03 142-28-903/28/23 17:120.47 50
2,2-Dichloropropane ND mg/kg 03/28/23 22:03 594-20-703/28/23 17:120.47 50
1,1-Dichloropropene ND mg/kg 03/28/23 22:03 563-58-603/28/23 17:120.47 50
cis-1,3-Dichloropropene ND mg/kg 03/28/23 22:03 10061-01-503/28/23 17:120.47 50
trans-1,3-Dichloropropene ND mg/kg 03/28/23 22:03 10061-02-603/28/23 17:120.47 50
Diisopropyl ether ND mg/kg 03/28/23 22:03 108-20-303/28/23 17:120.47 50
Ethanol ND mg/kg 03/28/23 22:03 64-17-503/28/23 17:1218.9 50
Ethylbenzene 179 mg/kg 03/28/23 22:03 100-41-403/28/23 17:120.47 50
Hexachloro-1,3-butadiene ND mg/kg 03/28/23 22:03 87-68-303/28/23 17:120.94 50
2-Hexanone ND mg/kg 03/28/23 22:03 591-78-603/28/23 17:124.7 50
Isopropylbenzene (Cumene)19.7 mg/kg 03/28/23 22:03 98-82-803/28/23 17:120.47 50
p-Isopropyltoluene 15.2 mg/kg 03/28/23 22:03 99-87-603/28/23 17:120.47 50
Methylene Chloride ND mg/kg 03/28/23 22:03 75-09-203/28/23 17:121.9 50
4-Methyl-2-pentanone (MIBK)ND mg/kg 03/28/23 22:03 108-10-103/28/23 17:124.7 50
Methyl-tert-butyl ether ND mg/kg 03/28/23 22:03 1634-04-403/28/23 17:120.47 50
Naphthalene 60.0 mg/kg 03/28/23 22:03 91-20-303/28/23 17:120.47 50
n-Propylbenzene 59.6 mg/kg 03/28/23 22:03 103-65-103/28/23 17:120.47 50
Styrene ND mg/kg 03/28/23 22:03 100-42-503/28/23 17:120.47 50
1,1,1,2-Tetrachloroethane ND mg/kg 03/28/23 22:03 630-20-603/28/23 17:120.47 50
1,1,2,2-Tetrachloroethane ND mg/kg 03/28/23 22:03 79-34-503/28/23 17:120.47 50
Tetrachloroethene ND mg/kg 03/28/23 22:03 127-18-403/28/23 17:120.47 50
Toluene 54.6 mg/kg 03/28/23 22:03 108-88-303/28/23 17:120.47 50
1,2,3-Trichlorobenzene ND mg/kg 03/28/23 22:03 87-61-603/28/23 17:120.47 50
1,2,4-Trichlorobenzene ND mg/kg 03/28/23 22:03 120-82-103/28/23 17:120.47 50
1,1,1-Trichloroethane ND mg/kg 03/28/23 22:03 71-55-603/28/23 17:120.47 50
1,1,2-Trichloroethane ND mg/kg 03/28/23 22:03 79-00-503/28/23 17:120.47 50
Trichloroethene ND mg/kg 03/28/23 22:03 79-01-603/28/23 17:120.47 50
Trichlorofluoromethane ND mg/kg 03/28/23 22:03 75-69-403/28/23 17:120.47 50
1,2,3-Trichloropropane ND mg/kg 03/28/23 22:03 96-18-403/28/23 17:120.47 50
1,2,4-Trimethylbenzene 294 mg/kg 03/28/23 22:03 95-63-603/28/23 17:120.47 50
1,3,5-Trimethylbenzene 93.0 mg/kg 03/28/23 22:03 108-67-803/28/23 17:120.47 50
Vinyl acetate ND mg/kg 03/28/23 22:03 108-05-403/28/23 17:124.7 50
Vinyl chloride ND mg/kg 03/28/23 22:03 75-01-403/28/23 17:120.94 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 13 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Sample:B-1 Lab ID:92657988005 Collected:03/21/23 12:00 Received:03/21/23 13:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Xylene (Total)443 mg/kg 03/28/23 22:03 1330-20-703/28/23 17:120.94 50
m&p-Xylene 389 mg/kg 03/28/23 22:03 179601-23-103/28/23 17:120.94 50
o-Xylene 53.9 mg/kg 03/28/23 22:03 95-47-603/28/23 17:120.47 50
Surrogates
Toluene-d8 (S)102 %03/28/23 22:03 2037-26-503/28/23 17:1270-130 50
4-Bromofluorobenzene (S)98 %03/28/23 22:03 460-00-403/28/23 17:1270-130 50
1,2-Dichloroethane-d4 (S)96 %03/28/23 22:03 17060-07-003/28/23 17:1270-130 50
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 32.9 %03/22/23 15:47 N20.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 14 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
764089
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92657988002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3968040
Associated Lab Samples:92657988002
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 03/27/23 15:58
1,1,1-Trichloroethane mg/kg ND 0.0050 03/27/23 15:58
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 03/27/23 15:58
1,1,2-Trichloroethane mg/kg ND 0.0050 03/27/23 15:58
1,1-Dichloroethane mg/kg ND 0.0050 03/27/23 15:58
1,1-Dichloroethene mg/kg ND 0.0050 03/27/23 15:58
1,1-Dichloropropene mg/kg ND 0.0050 03/27/23 15:58
1,2,3-Trichlorobenzene mg/kg ND 0.0050 03/27/23 15:58
1,2,3-Trichloropropane mg/kg ND 0.0050 03/27/23 15:58
1,2,4-Trichlorobenzene mg/kg ND 0.0050 03/27/23 15:58
1,2,4-Trimethylbenzene mg/kg ND 0.0050 03/27/23 15:58
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 03/27/23 15:58
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 03/27/23 15:58
1,2-Dichlorobenzene mg/kg ND 0.0050 03/27/23 15:58
1,2-Dichloroethane mg/kg ND 0.0050 03/27/23 15:58
1,2-Dichloropropane mg/kg ND 0.0050 03/27/23 15:58
1,3,5-Trimethylbenzene mg/kg ND 0.0050 03/27/23 15:58
1,3-Dichlorobenzene mg/kg ND 0.0050 03/27/23 15:58
1,3-Dichloropropane mg/kg ND 0.0050 03/27/23 15:58
1,4-Dichlorobenzene mg/kg ND 0.0050 03/27/23 15:58
2,2-Dichloropropane mg/kg ND 0.0050 03/27/23 15:58
2-Butanone (MEK)mg/kg ND 0.10 03/27/23 15:58
2-Chlorotoluene mg/kg ND 0.0050 03/27/23 15:58
2-Hexanone mg/kg ND 0.050 03/27/23 15:58
4-Chlorotoluene mg/kg ND 0.0050 03/27/23 15:58
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 03/27/23 15:58
Acetone mg/kg ND 0.10 03/27/23 15:58
Benzene mg/kg ND 0.0050 03/27/23 15:58
Bromobenzene mg/kg ND 0.0050 03/27/23 15:58
Bromochloromethane mg/kg ND 0.0050 03/27/23 15:58
Bromodichloromethane mg/kg ND 0.0050 03/27/23 15:58
Bromoform mg/kg ND 0.0050 03/27/23 15:58
Bromomethane mg/kg ND 0.020 v203/27/23 15:58
Carbon tetrachloride mg/kg ND 0.0050 03/27/23 15:58
Chlorobenzene mg/kg ND 0.0050 03/27/23 15:58
Chloroethane mg/kg ND 0.010 03/27/23 15:58
Chloroform mg/kg ND 0.0050 03/27/23 15:58
Chloromethane mg/kg ND 0.010 03/27/23 15:58
cis-1,2-Dichloroethene mg/kg ND 0.0050 03/27/23 15:58
cis-1,3-Dichloropropene mg/kg ND 0.0050 03/27/23 15:58
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
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1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 15 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3968040
Associated Lab Samples:92657988002
Matrix:Solid
Analyzed
Dibromochloromethane mg/kg ND 0.0050 03/27/23 15:58
Dibromomethane mg/kg ND 0.0050 03/27/23 15:58
Dichlorodifluoromethane mg/kg ND 0.010 03/27/23 15:58
Diisopropyl ether mg/kg ND 0.0050 03/27/23 15:58
Ethanol mg/kg ND 0.20 03/27/23 15:58
Ethylbenzene mg/kg ND 0.0050 03/27/23 15:58
Hexachloro-1,3-butadiene mg/kg ND 0.010 03/27/23 15:58
Isopropylbenzene (Cumene)mg/kg ND 0.0050 03/27/23 15:58
m&p-Xylene mg/kg ND 0.010 03/27/23 15:58
Methyl-tert-butyl ether mg/kg ND 0.0050 03/27/23 15:58
Methylene Chloride mg/kg ND 0.020 03/27/23 15:58
n-Butylbenzene mg/kg ND 0.0050 03/27/23 15:58
n-Propylbenzene mg/kg ND 0.0050 03/27/23 15:58
Naphthalene mg/kg ND 0.0050 03/27/23 15:58
o-Xylene mg/kg ND 0.0050 03/27/23 15:58
p-Isopropyltoluene mg/kg ND 0.0050 03/27/23 15:58
sec-Butylbenzene mg/kg ND 0.0050 03/27/23 15:58
Styrene mg/kg ND 0.0050 03/27/23 15:58
tert-Butylbenzene mg/kg ND 0.0050 03/27/23 15:58
Tetrachloroethene mg/kg ND 0.0050 03/27/23 15:58
Toluene mg/kg ND 0.0050 03/27/23 15:58
trans-1,2-Dichloroethene mg/kg ND 0.0050 03/27/23 15:58
trans-1,3-Dichloropropene mg/kg ND 0.0050 03/27/23 15:58
Trichloroethene mg/kg ND 0.0050 03/27/23 15:58
Trichlorofluoromethane mg/kg ND 0.0050 03/27/23 15:58
Vinyl acetate mg/kg ND 0.050 03/27/23 15:58
Vinyl chloride mg/kg ND 0.010 03/27/23 15:58
Xylene (Total)mg/kg ND 0.010 03/27/23 15:58
1,2-Dichloroethane-d4 (S)%108 70-130 03/27/23 15:58
4-Bromofluorobenzene (S)%93 70-130 03/27/23 15:58
Toluene-d8 (S)%102 70-130 03/27/23 15:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3968041LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.500.5 100 70-130
1,1,1-Trichloroethane mg/kg 0.500.5 99 70-130
1,1,2,2-Tetrachloroethane mg/kg 0.500.5 101 70-130
1,1,2-Trichloroethane mg/kg 0.480.5 97 70-130
1,1-Dichloroethane mg/kg 0.540.5 108 70-130
1,1-Dichloroethene mg/kg 0.550.5 111 70-130
1,1-Dichloropropene mg/kg 0.560.5 112 70-130
1,2,3-Trichlorobenzene mg/kg 0.500.5 100 70-130
1,2,3-Trichloropropane mg/kg 0.530.5 105 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 16 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3968041LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 0.520.5 105 70-130
1,2,4-Trimethylbenzene mg/kg 0.550.5 111 70-130
1,2-Dibromo-3-chloropropane mg/kg 0.580.5 117 67-130
1,2-Dibromoethane (EDB)mg/kg 0.500.5 100 70-130
1,2-Dichlorobenzene mg/kg 0.520.5 103 70-130
1,2-Dichloroethane mg/kg 0.470.5 94 70-130
1,2-Dichloropropane mg/kg 0.480.5 96 70-130
1,3,5-Trimethylbenzene mg/kg 0.520.5 104 70-130
1,3-Dichlorobenzene mg/kg 0.520.5 104 70-130
1,3-Dichloropropane mg/kg 0.500.5 100 70-130
1,4-Dichlorobenzene mg/kg 0.500.5 100 70-130
2,2-Dichloropropane mg/kg 0.520.5 104 67-130
2-Butanone (MEK)mg/kg 1.01 105 66-130
2-Chlorotoluene mg/kg 0.510.5 103 70-130
2-Hexanone mg/kg 1.01 105 70-130
4-Chlorotoluene mg/kg 0.510.5 102 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 1.01 104 70-130
Acetone mg/kg 0.961 96 67-130
Benzene mg/kg 0.510.5 102 70-130
Bromobenzene mg/kg 0.490.5 99 70-130
Bromochloromethane mg/kg 0.500.5 101 70-130
Bromodichloromethane mg/kg 0.480.5 97 70-130
Bromoform mg/kg 0.520.5 103 70-130
Bromomethane mg/kg 0.37 v30.5 74 53-175
Carbon tetrachloride mg/kg 0.540.5 108 70-130
Chlorobenzene mg/kg 0.500.5 100 70-130
Chloroethane mg/kg 0.520.5 103 70-135
Chloroform mg/kg 0.510.5 101 70-130
Chloromethane mg/kg 0.590.5 119 64-130
cis-1,2-Dichloroethene mg/kg 0.520.5 105 70-130
cis-1,3-Dichloropropene mg/kg 0.530.5 105 70-130
Dibromochloromethane mg/kg 0.510.5 102 70-130
Dibromomethane mg/kg 0.500.5 100 70-130
Dichlorodifluoromethane mg/kg 0.660.5 133 63-145
Diisopropyl ether mg/kg 0.510.5 103 68-130
Ethanol mg/kg 20.320 101 70-130
Ethylbenzene mg/kg 0.470.5 95 70-130
Hexachloro-1,3-butadiene mg/kg 0.580.5 116 70-130
Isopropylbenzene (Cumene)mg/kg 0.540.5 108 70-130
m&p-Xylene mg/kg 1.01 103 70-130
Methyl-tert-butyl ether mg/kg 0.480.5 96 70-130
Methylene Chloride mg/kg 0.480.5 96 67-130
n-Butylbenzene mg/kg 0.550.5 109 70-130
n-Propylbenzene mg/kg 0.500.5 101 70-130
Naphthalene mg/kg 0.540.5 108 70-130
o-Xylene mg/kg 0.520.5 104 70-130
p-Isopropyltoluene mg/kg 0.550.5 110 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
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1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 17 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3968041LABORATORY CONTROL SAMPLE:
LCSSpike
sec-Butylbenzene mg/kg 0.540.5 107 70-130
Styrene mg/kg 0.540.5 108 70-130
tert-Butylbenzene mg/kg 0.500.5 101 64-130
Tetrachloroethene mg/kg 0.540.5 107 70-130
Toluene mg/kg 0.490.5 98 70-130
trans-1,2-Dichloroethene mg/kg 0.540.5 108 70-130
trans-1,3-Dichloropropene mg/kg 0.530.5 107 70-130
Trichloroethene mg/kg 0.510.5 102 70-130
Trichlorofluoromethane mg/kg 0.500.5 99 70-130
Vinyl acetate mg/kg 1.11 106 70-134
Vinyl chloride mg/kg 0.490.5 98 68-130
Xylene (Total)mg/kg 1.61.5 103 70-130
1,2-Dichloroethane-d4 (S)%92 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3968042MATRIX SPIKE SAMPLE:
MSSpike
Result
92658806003
1,1,1,2-Tetrachloroethane mg/kg 0.730.6 121 58-140ND
1,1,1-Trichloroethane mg/kg 0.780.6 128 58-144ND
1,1,2,2-Tetrachloroethane mg/kg 0.760.6 125 52-139ND
1,1,2-Trichloroethane mg/kg 0.710.6 116 56-140ND
1,1-Dichloroethane mg/kg 0.840.6 138 58-145ND
1,1-Dichloroethene mg/kg 0.860.6 142 57-158ND
1,1-Dichloropropene mg/kg 0.820.6 135 58-151ND
1,2,3-Trichlorobenzene mg/kg 0.17 M10.6 28 48-149ND
1,2,3-Trichloropropane mg/kg 0.730.6 121 54-132ND
1,2,4-Trichlorobenzene mg/kg 0.440.6 72 51-151ND
1,2,4-Trimethylbenzene mg/kg 0.690.6 114 38-170ND
1,2-Dibromo-3-chloropropane mg/kg 0.550.6 91 44-134ND
1,2-Dibromoethane (EDB)mg/kg 0.690.6 115 60-138ND
1,2-Dichlorobenzene mg/kg 0.680.6 113 59-147ND
1,2-Dichloroethane mg/kg 0.710.6 118 57-139ND
1,2-Dichloropropane mg/kg 0.740.6 123 62-145ND
1,3,5-Trimethylbenzene mg/kg 0.660.6 110 47-159ND
1,3-Dichlorobenzene mg/kg 0.650.6 107 58-144ND
1,3-Dichloropropane mg/kg 0.710.6 117 60-142ND
1,4-Dichlorobenzene mg/kg 0.620.6 103 57-143ND
2,2-Dichloropropane mg/kg 0.730.6 121 37-144ND
2-Butanone (MEK)mg/kg 1.31.2 109 28-146ND
2-Chlorotoluene mg/kg 0.650.6 107 55-158ND
2-Hexanone mg/kg 1.31.2 109 44-141ND
4-Chlorotoluene mg/kg 0.640.6 106 55-146ND
4-Methyl-2-pentanone (MIBK)mg/kg 1.41.2 117 50-138ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
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1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 18 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3968042MATRIX SPIKE SAMPLE:
MSSpike
Result
92658806003
Acetone mg/kg 1.11.2 94 20-136ND
Benzene mg/kg 0.780.6 129 60-145ND
Bromobenzene mg/kg 0.680.6 112 59-145ND
Bromochloromethane mg/kg 0.770.6 128 57-143ND
Bromodichloromethane mg/kg 0.720.6 119 53-133ND
Bromoform mg/kg 0.730.6 120 48-133ND
Bromomethane mg/kg 0.52 v30.6 85 10-167ND
Carbon tetrachloride mg/kg 0.610.6 101 57-147ND
Chlorobenzene mg/kg 0.760.6 106 61-144113 ug/kg
Chloroethane mg/kg 0.570.6 95 10-153ND
Chloroform mg/kg 0.770.6 127 58-141ND
Chloromethane mg/kg 0.880.6 145 54-165ND
cis-1,2-Dichloroethene mg/kg 0.790.6 131 59-144ND
cis-1,3-Dichloropropene mg/kg 0.770.6 127 56-137ND
Dibromochloromethane mg/kg 0.720.6 119 53-139ND
Dibromomethane mg/kg 0.720.6 118 60-136ND
Dichlorodifluoromethane mg/kg 0.880.6 145 49-177ND
Diisopropyl ether mg/kg 0.790.6 131 53-136ND
Ethanol mg/kg ND M124.2 0 70-130ND
Ethylbenzene mg/kg 0.650.6 107 53-1503.1J ug/kg
Hexachloro-1,3-butadiene mg/kg 0.720.6 119 42-186ND
Isopropylbenzene (Cumene)mg/kg 0.740.6 122 62-154ND
m&p-Xylene mg/kg 1.41.2 114 49-156ND
Methyl-tert-butyl ether mg/kg 0.740.6 122 54-133ND
Methylene Chloride mg/kg 0.800.6 132 50-153ND
n-Butylbenzene mg/kg 0.650.6 107 44-174ND
n-Propylbenzene mg/kg 0.620.6 102 52-157ND
Naphthalene mg/kg 0.19 M10.6 31 37-150ND
o-Xylene mg/kg 0.720.6 119 54-150ND
p-Isopropyltoluene mg/kg 0.700.6 116 50-164ND
sec-Butylbenzene mg/kg 0.710.6 117 58-161ND
Styrene mg/kg 0.760.6 125 60-148ND
tert-Butylbenzene mg/kg 0.670.6 110 44-151ND
Tetrachloroethene mg/kg 0.660.6 108 53-1513.7J ug/kg
Toluene mg/kg 0.720.6 118 52-148ND
trans-1,2-Dichloroethene mg/kg 0.810.6 133 60-148ND
trans-1,3-Dichloropropene mg/kg 0.750.6 124 55-133ND
Trichloroethene mg/kg 0.730.6 120 60-148ND
Trichlorofluoromethane mg/kg 0.640.6 106 10-154ND
Vinyl acetate mg/kg 1.51.2 123 50-149ND
Vinyl chloride mg/kg 0.680.6 112 57-157ND
Xylene (Total)mg/kg 2.11.8 116 52-153ND
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%103 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
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[phone]
Page 19 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92658806004
3968043SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg ND 30ND
1,1,1-Trichloroethane mg/kg ND 30ND
1,1,2,2-Tetrachloroethane mg/kg ND 30ND
1,1,2-Trichloroethane mg/kg ND 30ND
1,1-Dichloroethane mg/kg ND 30ND
1,1-Dichloroethene mg/kg ND 30ND
1,1-Dichloropropene mg/kg ND 30ND
1,2,3-Trichlorobenzene mg/kg ND 30ND
1,2,3-Trichloropropane mg/kg ND 30ND
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2,4-Trimethylbenzene mg/kg ND 30ND
1,2-Dibromo-3-chloropropane mg/kg ND 30ND
1,2-Dibromoethane (EDB)mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,2-Dichloroethane mg/kg ND 30ND
1,2-Dichloropropane mg/kg ND 30ND
1,3,5-Trimethylbenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,3-Dichloropropane mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
2,2-Dichloropropane mg/kg ND 30ND
2-Butanone (MEK)mg/kg ND 30ND
2-Chlorotoluene mg/kg ND 30ND
2-Hexanone mg/kg ND 30ND
4-Chlorotoluene mg/kg ND 30ND
4-Methyl-2-pentanone (MIBK)mg/kg ND 30ND
Acetone mg/kg ND 30ND
Benzene mg/kg ND 30ND
Bromobenzene mg/kg ND 30ND
Bromochloromethane mg/kg ND 30ND
Bromodichloromethane mg/kg ND 30ND
Bromoform mg/kg ND 30ND
Bromomethane mg/kg ND v230ND
Carbon tetrachloride mg/kg ND 30ND
Chlorobenzene mg/kg 0.053 D6333073.6 ug/kg
Chloroethane mg/kg ND 30ND
Chloroform mg/kg ND 30ND
Chloromethane mg/kg ND 30ND
cis-1,2-Dichloroethene mg/kg ND 30ND
cis-1,3-Dichloropropene mg/kg ND 30ND
Dibromochloromethane mg/kg ND 30ND
Dibromomethane mg/kg ND 30ND
Dichlorodifluoromethane mg/kg ND 30ND
Diisopropyl ether mg/kg ND 30ND
Ethanol mg/kg ND 30ND
Ethylbenzene mg/kg ND 30ND
Hexachloro-1,3-butadiene mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 20 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92658806004
3968043SAMPLE DUPLICATE:
Isopropylbenzene (Cumene)mg/kg ND 30ND
m&p-Xylene mg/kg ND 30ND
Methyl-tert-butyl ether mg/kg ND 30ND
Methylene Chloride mg/kg ND 30ND
n-Butylbenzene mg/kg ND 30ND
n-Propylbenzene mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
o-Xylene mg/kg ND 30ND
p-Isopropyltoluene mg/kg ND 30ND
sec-Butylbenzene mg/kg ND 30ND
Styrene mg/kg ND 30ND
tert-Butylbenzene mg/kg ND 30ND
Tetrachloroethene mg/kg ND 30ND
Toluene mg/kg ND 30ND
trans-1,2-Dichloroethene mg/kg ND 30ND
trans-1,3-Dichloropropene mg/kg ND 30ND
Trichloroethene mg/kg ND 30ND
Trichlorofluoromethane mg/kg ND 30ND
Vinyl acetate mg/kg ND 30ND
Vinyl chloride mg/kg ND 30ND
Xylene (Total)mg/kg ND 30ND
1,2-Dichloroethane-d4 (S)%108103
4-Bromofluorobenzene (S)%9999
Toluene-d8 (S)%102102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 21 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
764398
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92657988001, 92657988004, 92657988005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3969564
Associated Lab Samples:92657988001, 92657988004, 92657988005
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 03/28/23 17:05
1,1,1-Trichloroethane mg/kg ND 0.0050 03/28/23 17:05
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 03/28/23 17:05
1,1,2-Trichloroethane mg/kg ND 0.0050 03/28/23 17:05
1,1-Dichloroethane mg/kg ND 0.0050 03/28/23 17:05
1,1-Dichloroethene mg/kg ND 0.0050 03/28/23 17:05
1,1-Dichloropropene mg/kg ND 0.0050 03/28/23 17:05
1,2,3-Trichlorobenzene mg/kg ND 0.0050 03/28/23 17:05
1,2,3-Trichloropropane mg/kg ND 0.0050 03/28/23 17:05
1,2,4-Trichlorobenzene mg/kg ND 0.0050 03/28/23 17:05
1,2,4-Trimethylbenzene mg/kg ND 0.0050 03/28/23 17:05
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 03/28/23 17:05
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 03/28/23 17:05
1,2-Dichlorobenzene mg/kg ND 0.0050 03/28/23 17:05
1,2-Dichloroethane mg/kg ND 0.0050 03/28/23 17:05
1,2-Dichloropropane mg/kg ND 0.0050 03/28/23 17:05
1,3,5-Trimethylbenzene mg/kg ND 0.0050 03/28/23 17:05
1,3-Dichlorobenzene mg/kg ND 0.0050 03/28/23 17:05
1,3-Dichloropropane mg/kg ND 0.0050 03/28/23 17:05
1,4-Dichlorobenzene mg/kg ND 0.0050 03/28/23 17:05
2,2-Dichloropropane mg/kg ND 0.0050 03/28/23 17:05
2-Butanone (MEK)mg/kg ND 0.10 03/28/23 17:05
2-Chlorotoluene mg/kg ND 0.0050 03/28/23 17:05
2-Hexanone mg/kg ND 0.050 03/28/23 17:05
4-Chlorotoluene mg/kg ND 0.0050 03/28/23 17:05
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 03/28/23 17:05
Acetone mg/kg ND 0.10 03/28/23 17:05
Benzene mg/kg ND 0.0050 03/28/23 17:05
Bromobenzene mg/kg ND 0.0050 03/28/23 17:05
Bromochloromethane mg/kg ND 0.0050 03/28/23 17:05
Bromodichloromethane mg/kg ND 0.0050 03/28/23 17:05
Bromoform mg/kg ND 0.0050 03/28/23 17:05
Bromomethane mg/kg ND 0.020 v203/28/23 17:05
Carbon tetrachloride mg/kg ND 0.0050 03/28/23 17:05
Chlorobenzene mg/kg ND 0.0050 03/28/23 17:05
Chloroethane mg/kg ND 0.010 03/28/23 17:05
Chloroform mg/kg ND 0.0050 03/28/23 17:05
Chloromethane mg/kg ND 0.010 03/28/23 17:05
cis-1,2-Dichloroethene mg/kg ND 0.0050 03/28/23 17:05
cis-1,3-Dichloropropene mg/kg ND 0.0050 03/28/23 17:05
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 22 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3969564
Associated Lab Samples:92657988001, 92657988004, 92657988005
Matrix:Solid
Analyzed
Dibromochloromethane mg/kg ND 0.0050 03/28/23 17:05
Dibromomethane mg/kg ND 0.0050 03/28/23 17:05
Dichlorodifluoromethane mg/kg ND 0.010 03/28/23 17:05
Diisopropyl ether mg/kg ND 0.0050 03/28/23 17:05
Ethanol mg/kg ND 0.20 03/28/23 17:05
Ethylbenzene mg/kg ND 0.0050 03/28/23 17:05
Hexachloro-1,3-butadiene mg/kg ND 0.010 03/28/23 17:05
Isopropylbenzene (Cumene)mg/kg ND 0.0050 03/28/23 17:05
m&p-Xylene mg/kg ND 0.010 03/28/23 17:05
Methyl-tert-butyl ether mg/kg ND 0.0050 03/28/23 17:05
Methylene Chloride mg/kg ND 0.020 03/28/23 17:05
n-Butylbenzene mg/kg ND 0.0050 03/28/23 17:05
n-Propylbenzene mg/kg ND 0.0050 03/28/23 17:05
Naphthalene mg/kg ND 0.0050 03/28/23 17:05
o-Xylene mg/kg ND 0.0050 03/28/23 17:05
p-Isopropyltoluene mg/kg ND 0.0050 03/28/23 17:05
sec-Butylbenzene mg/kg ND 0.0050 03/28/23 17:05
Styrene mg/kg ND 0.0050 03/28/23 17:05
tert-Butylbenzene mg/kg ND 0.0050 03/28/23 17:05
Tetrachloroethene mg/kg ND 0.0050 03/28/23 17:05
Toluene mg/kg ND 0.0050 03/28/23 17:05
trans-1,2-Dichloroethene mg/kg ND 0.0050 03/28/23 17:05
trans-1,3-Dichloropropene mg/kg ND 0.0050 03/28/23 17:05
Trichloroethene mg/kg ND 0.0050 03/28/23 17:05
Trichlorofluoromethane mg/kg ND 0.0050 03/28/23 17:05
Vinyl acetate mg/kg ND 0.050 03/28/23 17:05
Vinyl chloride mg/kg ND 0.010 03/28/23 17:05
Xylene (Total)mg/kg ND 0.010 03/28/23 17:05
1,2-Dichloroethane-d4 (S)%104 70-130 03/28/23 17:05
4-Bromofluorobenzene (S)%94 70-130 03/28/23 17:05
Toluene-d8 (S)%100 70-130 03/28/23 17:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3969565LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.490.5 99 70-130
1,1,1-Trichloroethane mg/kg 0.480.5 97 70-130
1,1,2,2-Tetrachloroethane mg/kg 0.480.5 97 70-130
1,1,2-Trichloroethane mg/kg 0.440.5 89 70-130
1,1-Dichloroethane mg/kg 0.500.5 100 70-130
1,1-Dichloroethene mg/kg 0.520.5 104 70-130
1,1-Dichloropropene mg/kg 0.520.5 104 70-130
1,2,3-Trichlorobenzene mg/kg 0.460.5 92 70-130
1,2,3-Trichloropropane mg/kg 0.490.5 98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 23 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3969565LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 0.510.5 102 70-130
1,2,4-Trimethylbenzene mg/kg 0.520.5 104 70-130
1,2-Dibromo-3-chloropropane mg/kg 0.510.5 103 67-130
1,2-Dibromoethane (EDB)mg/kg 0.470.5 95 70-130
1,2-Dichlorobenzene mg/kg 0.490.5 97 70-130
1,2-Dichloroethane mg/kg 0.420.5 85 70-130
1,2-Dichloropropane mg/kg 0.430.5 86 70-130
1,3,5-Trimethylbenzene mg/kg 0.490.5 98 70-130
1,3-Dichlorobenzene mg/kg 0.510.5 102 70-130
1,3-Dichloropropane mg/kg 0.450.5 91 70-130
1,4-Dichlorobenzene mg/kg 0.470.5 94 70-130
2,2-Dichloropropane mg/kg 0.490.5 98 67-130
2-Butanone (MEK)mg/kg 0.921 92 66-130
2-Chlorotoluene mg/kg 0.480.5 95 70-130
2-Hexanone mg/kg 0.961 96 70-130
4-Chlorotoluene mg/kg 0.490.5 99 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 0.931 93 70-130
Acetone mg/kg 0.841 84 67-130
Benzene mg/kg 0.490.5 98 70-130
Bromobenzene mg/kg 0.480.5 97 70-130
Bromochloromethane mg/kg 0.480.5 95 70-130
Bromodichloromethane mg/kg 0.470.5 94 70-130
Bromoform mg/kg 0.500.5 101 70-130
Bromomethane mg/kg 0.34 v30.5 69 53-175
Carbon tetrachloride mg/kg 0.530.5 106 70-130
Chlorobenzene mg/kg 0.480.5 97 70-130
Chloroethane mg/kg 0.500.5 99 70-135
Chloroform mg/kg 0.470.5 94 70-130
Chloromethane mg/kg 0.560.5 112 64-130
cis-1,2-Dichloroethene mg/kg 0.460.5 91 70-130
cis-1,3-Dichloropropene mg/kg 0.500.5 100 70-130
Dibromochloromethane mg/kg 0.510.5 101 70-130
Dibromomethane mg/kg 0.480.5 97 70-130
Dichlorodifluoromethane mg/kg 0.610.5 123 63-145
Diisopropyl ether mg/kg 0.460.5 92 68-130
Ethanol mg/kg 16.420 82 70-130
Ethylbenzene mg/kg 0.450.5 89 70-130
Hexachloro-1,3-butadiene mg/kg 0.530.5 105 70-130
Isopropylbenzene (Cumene)mg/kg 0.530.5 105 70-130
m&p-Xylene mg/kg 1.01 101 70-130
Methyl-tert-butyl ether mg/kg 0.450.5 90 70-130
Methylene Chloride mg/kg 0.440.5 87 67-130
n-Butylbenzene mg/kg 0.540.5 108 70-130
n-Propylbenzene mg/kg 0.480.5 97 70-130
Naphthalene mg/kg 0.480.5 96 70-130
o-Xylene mg/kg 0.490.5 98 70-130
p-Isopropyltoluene mg/kg 0.530.5 107 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 24 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3969565LABORATORY CONTROL SAMPLE:
LCSSpike
sec-Butylbenzene mg/kg 0.510.5 101 70-130
Styrene mg/kg 0.530.5 105 70-130
tert-Butylbenzene mg/kg 0.490.5 98 64-130
Tetrachloroethene mg/kg 0.530.5 105 70-130
Toluene mg/kg 0.470.5 93 70-130
trans-1,2-Dichloroethene mg/kg 0.510.5 101 70-130
trans-1,3-Dichloropropene mg/kg 0.480.5 97 70-130
Trichloroethene mg/kg 0.490.5 97 70-130
Trichlorofluoromethane mg/kg 0.480.5 95 70-130
Vinyl acetate mg/kg 0.961 96 70-134
Vinyl chloride mg/kg 0.450.5 89 68-130
Xylene (Total)mg/kg 1.51.5 100 70-130
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3969566MATRIX SPIKE SAMPLE:
MSSpike
Result
92657988004
1,1,1,2-Tetrachloroethane mg/kg 0.590.94 63 58-140ND
1,1,1-Trichloroethane mg/kg 0.600.94 64 58-144ND
1,1,2,2-Tetrachloroethane mg/kg 0.570.94 61 52-139ND
1,1,2-Trichloroethane mg/kg 0.580.94 62 56-140ND
1,1-Dichloroethane mg/kg 0.670.94 72 58-145ND
1,1-Dichloroethene mg/kg 0.700.94 75 57-158ND
1,1-Dichloropropene mg/kg 0.660.94 71 58-151ND
1,2,3-Trichlorobenzene mg/kg 0.21 M10.94 23 48-149ND
1,2,3-Trichloropropane mg/kg 0.570.94 62 54-132ND
1,2,4-Trichlorobenzene mg/kg 0.43 M10.94 46 51-151ND
1,2,4-Trimethylbenzene mg/kg 0.590.94 63 38-170ND
1,2-Dibromo-3-chloropropane mg/kg 0.490.94 52 44-134ND
1,2-Dibromoethane (EDB)mg/kg 0.560.94 60 60-138ND
1,2-Dichlorobenzene mg/kg 0.570.94 62 59-147ND
1,2-Dichloroethane mg/kg 0.560.94 61 57-139ND
1,2-Dichloropropane mg/kg 0.600.94 64 62-145ND
1,3,5-Trimethylbenzene mg/kg 0.560.94 60 47-159ND
1,3-Dichlorobenzene mg/kg 0.570.94 61 58-144ND
1,3-Dichloropropane mg/kg 0.590.94 63 60-142ND
1,4-Dichlorobenzene mg/kg 0.52 M10.94 56 57-143ND
2,2-Dichloropropane mg/kg 0.590.94 63 37-144ND
2-Butanone (MEK)mg/kg 1.01.9 55 28-146ND
2-Chlorotoluene mg/kg 0.570.94 61 55-158ND
2-Hexanone mg/kg 1.01.9 55 44-141ND
4-Chlorotoluene mg/kg 0.560.94 61 55-146ND
4-Methyl-2-pentanone (MIBK)mg/kg 1.11.9 59 50-138ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 25 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3969566MATRIX SPIKE SAMPLE:
MSSpike
Result
92657988004
Acetone mg/kg 0.881.9 47 20-136ND
Benzene mg/kg 0.630.94 68 60-145ND
Bromobenzene mg/kg 0.550.94 59 59-145ND
Bromochloromethane mg/kg 0.600.94 64 57-143ND
Bromodichloromethane mg/kg 0.570.94 61 53-133ND
Bromoform mg/kg 0.550.94 59 48-133ND
Bromomethane mg/kg 0.41 v30.94 43 10-167ND
Carbon tetrachloride mg/kg 0.590.94 64 57-147ND
Chlorobenzene mg/kg 0.590.94 62 61-144ND
Chloroethane mg/kg 0.550.94 59 10-153ND
Chloroform mg/kg 0.630.94 67 58-141ND
Chloromethane mg/kg 0.750.94 81 54-165ND
cis-1,2-Dichloroethene mg/kg 0.640.94 69 59-144ND
cis-1,3-Dichloropropene mg/kg 0.630.94 67 56-137ND
Dibromochloromethane mg/kg 0.570.94 62 53-139ND
Dibromomethane mg/kg 0.570.94 61 60-136ND
Dichlorodifluoromethane mg/kg 0.780.94 83 49-177ND
Diisopropyl ether mg/kg 0.610.94 65 53-136ND
Ethanol mg/kg ND M137.3 0 70-130ND
Ethylbenzene mg/kg 0.540.94 56 53-1500.018
Hexachloro-1,3-butadiene mg/kg 0.590.94 63 42-186ND
Isopropylbenzene (Cumene)mg/kg 0.620.94 66 62-154ND
m&p-Xylene mg/kg 1.21.9 63 49-1560.064
Methyl-tert-butyl ether mg/kg 0.580.94 62 54-133ND
Methylene Chloride mg/kg 0.550.94 59 50-153ND
n-Butylbenzene mg/kg 0.580.94 63 44-174ND
n-Propylbenzene mg/kg 0.540.94 58 52-157ND
Naphthalene mg/kg 0.27 M10.94 29 37-150ND
o-Xylene mg/kg 0.610.94 63 54-1500.015
p-Isopropyltoluene mg/kg 0.610.94 65 50-164ND
sec-Butylbenzene mg/kg 0.620.94 67 58-161ND
Styrene mg/kg 0.610.94 64 60-1480.018
tert-Butylbenzene mg/kg 0.550.94 60 44-151ND
Tetrachloroethene mg/kg 0.550.94 59 53-151ND
Toluene mg/kg 0.600.94 64 52-148ND
trans-1,2-Dichloroethene mg/kg 0.630.94 68 60-148ND
trans-1,3-Dichloropropene mg/kg 0.600.94 64 55-133ND
Trichloroethene mg/kg 0.610.94 65 60-148ND
Trichlorofluoromethane mg/kg 0.570.94 61 10-154ND
Vinyl acetate mg/kg 1.21.9 62 50-149ND
Vinyl chloride mg/kg 0.600.94 64 57-157ND
Xylene (Total)mg/kg 1.92.7 63 52-1530.079
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%105 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 26 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92658837001
3969567SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg ND 30ND
1,1,1-Trichloroethane mg/kg ND 30ND
1,1,2,2-Tetrachloroethane mg/kg ND 30ND
1,1,2-Trichloroethane mg/kg ND 30ND
1,1-Dichloroethane mg/kg ND 30ND
1,1-Dichloroethene mg/kg ND 30ND
1,1-Dichloropropene mg/kg ND 30ND
1,2,3-Trichlorobenzene mg/kg ND 30ND
1,2,3-Trichloropropane mg/kg ND 30ND
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2,4-Trimethylbenzene mg/kg ND 30ND
1,2-Dibromo-3-chloropropane mg/kg ND 30ND
1,2-Dibromoethane (EDB)mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,2-Dichloroethane mg/kg ND 30ND
1,2-Dichloropropane mg/kg ND 30ND
1,3,5-Trimethylbenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,3-Dichloropropane mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
2,2-Dichloropropane mg/kg ND 30ND
2-Butanone (MEK)mg/kg ND 30ND
2-Chlorotoluene mg/kg ND 30ND
2-Hexanone mg/kg ND 30ND
4-Chlorotoluene mg/kg ND 30ND
4-Methyl-2-pentanone (MIBK)mg/kg ND 30ND
Acetone mg/kg ND 30ND
Benzene mg/kg ND 30ND
Bromobenzene mg/kg ND 30ND
Bromochloromethane mg/kg ND 30ND
Bromodichloromethane mg/kg ND 30ND
Bromoform mg/kg ND 30ND
Bromomethane mg/kg ND v230ND
Carbon tetrachloride mg/kg ND 30ND
Chlorobenzene mg/kg ND 30ND
Chloroethane mg/kg ND 30ND
Chloroform mg/kg ND 30ND
Chloromethane mg/kg ND 30ND
cis-1,2-Dichloroethene mg/kg 0.070 3 3068.1 ug/kg
cis-1,3-Dichloropropene mg/kg ND 30ND
Dibromochloromethane mg/kg ND 30ND
Dibromomethane mg/kg ND 30ND
Dichlorodifluoromethane mg/kg ND 30ND
Diisopropyl ether mg/kg ND 30ND
Ethanol mg/kg ND 30ND
Ethylbenzene mg/kg ND 30ND
Hexachloro-1,3-butadiene mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 27 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92658837001
3969567SAMPLE DUPLICATE:
Isopropylbenzene (Cumene)mg/kg ND 30ND
m&p-Xylene mg/kg ND 30ND
Methyl-tert-butyl ether mg/kg ND 30ND
Methylene Chloride mg/kg ND 30ND
n-Butylbenzene mg/kg ND 30ND
n-Propylbenzene mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
o-Xylene mg/kg ND 30ND
p-Isopropyltoluene mg/kg ND 30ND
sec-Butylbenzene mg/kg ND 30ND
Styrene mg/kg ND 30ND
tert-Butylbenzene mg/kg ND 30ND
Tetrachloroethene mg/kg 0.76 2 30774 ug/kg
Toluene mg/kg ND 30ND
trans-1,2-Dichloroethene mg/kg ND 30ND
trans-1,3-Dichloropropene mg/kg ND 30ND
Trichloroethene mg/kg 0.050 6 3052.8 ug/kg
Trichlorofluoromethane mg/kg ND 30ND
Vinyl acetate mg/kg ND 30ND
Vinyl chloride mg/kg ND 30ND
Xylene (Total)mg/kg ND 30ND
1,2-Dichloroethane-d4 (S)%101108
4-Bromofluorobenzene (S)%102100
Toluene-d8 (S)%102101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 28 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
764749
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92657988003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3971097
Associated Lab Samples:92657988003
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 03/29/23 23:11
1,1,1-Trichloroethane mg/kg ND 0.0050 03/29/23 23:11
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 03/29/23 23:11
1,1,2-Trichloroethane mg/kg ND 0.0050 03/29/23 23:11
1,1-Dichloroethane mg/kg ND 0.0050 03/29/23 23:11
1,1-Dichloroethene mg/kg ND 0.0050 03/29/23 23:11
1,1-Dichloropropene mg/kg ND 0.0050 03/29/23 23:11
1,2,3-Trichlorobenzene mg/kg ND 0.0050 03/29/23 23:11
1,2,3-Trichloropropane mg/kg ND 0.0050 03/29/23 23:11
1,2,4-Trichlorobenzene mg/kg ND 0.0050 03/29/23 23:11
1,2,4-Trimethylbenzene mg/kg ND 0.0050 03/29/23 23:11
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 03/29/23 23:11
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 03/29/23 23:11
1,2-Dichlorobenzene mg/kg ND 0.0050 03/29/23 23:11
1,2-Dichloroethane mg/kg ND 0.0050 03/29/23 23:11
1,2-Dichloropropane mg/kg ND 0.0050 03/29/23 23:11
1,3,5-Trimethylbenzene mg/kg ND 0.0050 03/29/23 23:11
1,3-Dichlorobenzene mg/kg ND 0.0050 03/29/23 23:11
1,3-Dichloropropane mg/kg ND 0.0050 03/29/23 23:11
1,4-Dichlorobenzene mg/kg ND 0.0050 03/29/23 23:11
2,2-Dichloropropane mg/kg ND 0.0050 03/29/23 23:11
2-Butanone (MEK)mg/kg ND 0.10 03/29/23 23:11
2-Chlorotoluene mg/kg ND 0.0050 03/29/23 23:11
2-Hexanone mg/kg ND 0.050 03/29/23 23:11
4-Chlorotoluene mg/kg ND 0.0050 03/29/23 23:11
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 03/29/23 23:11
Acetone mg/kg ND 0.10 03/29/23 23:11
Benzene mg/kg ND 0.0050 03/29/23 23:11
Bromobenzene mg/kg ND 0.0050 03/29/23 23:11
Bromochloromethane mg/kg ND 0.0050 03/29/23 23:11
Bromodichloromethane mg/kg ND 0.0050 03/29/23 23:11
Bromoform mg/kg ND 0.0050 03/29/23 23:11
Bromomethane mg/kg ND 0.020 v203/29/23 23:11
Carbon tetrachloride mg/kg ND 0.0050 03/29/23 23:11
Chlorobenzene mg/kg ND 0.0050 03/29/23 23:11
Chloroethane mg/kg ND 0.010 03/29/23 23:11
Chloroform mg/kg ND 0.0050 03/29/23 23:11
Chloromethane mg/kg ND 0.010 03/29/23 23:11
cis-1,2-Dichloroethene mg/kg ND 0.0050 03/29/23 23:11
cis-1,3-Dichloropropene mg/kg ND 0.0050 03/29/23 23:11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 29 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3971097
Associated Lab Samples:92657988003
Matrix:Solid
Analyzed
Dibromochloromethane mg/kg ND 0.0050 03/29/23 23:11
Dibromomethane mg/kg ND 0.0050 03/29/23 23:11
Dichlorodifluoromethane mg/kg ND 0.010 v203/29/23 23:11
Diisopropyl ether mg/kg ND 0.0050 03/29/23 23:11
Ethanol mg/kg ND 0.20 03/29/23 23:11
Ethylbenzene mg/kg ND 0.0050 03/29/23 23:11
Hexachloro-1,3-butadiene mg/kg ND 0.010 03/29/23 23:11
Isopropylbenzene (Cumene)mg/kg ND 0.0050 03/29/23 23:11
m&p-Xylene mg/kg ND 0.010 03/29/23 23:11
Methyl-tert-butyl ether mg/kg ND 0.0050 03/29/23 23:11
Methylene Chloride mg/kg ND 0.020 03/29/23 23:11
n-Butylbenzene mg/kg ND 0.0050 03/29/23 23:11
n-Propylbenzene mg/kg ND 0.0050 03/29/23 23:11
Naphthalene mg/kg ND 0.0050 03/29/23 23:11
o-Xylene mg/kg ND 0.0050 03/29/23 23:11
p-Isopropyltoluene mg/kg ND 0.0050 03/29/23 23:11
sec-Butylbenzene mg/kg ND 0.0050 03/29/23 23:11
Styrene mg/kg ND 0.0050 03/29/23 23:11
tert-Butylbenzene mg/kg ND 0.0050 03/29/23 23:11
Tetrachloroethene mg/kg ND 0.0050 03/29/23 23:11
Toluene mg/kg ND 0.0050 03/29/23 23:11
trans-1,2-Dichloroethene mg/kg ND 0.0050 03/29/23 23:11
trans-1,3-Dichloropropene mg/kg ND 0.0050 03/29/23 23:11
Trichloroethene mg/kg ND 0.0050 03/29/23 23:11
Trichlorofluoromethane mg/kg ND 0.0050 03/29/23 23:11
Vinyl acetate mg/kg ND 0.050 03/29/23 23:11
Vinyl chloride mg/kg ND 0.010 03/29/23 23:11
Xylene (Total)mg/kg ND 0.010 03/29/23 23:11
1,2-Dichloroethane-d4 (S)%104 70-130 03/29/23 23:11
4-Bromofluorobenzene (S)%96 70-130 03/29/23 23:11
Toluene-d8 (S)%100 70-130 03/29/23 23:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3971098LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.540.5 107 70-130
1,1,1-Trichloroethane mg/kg 0.520.5 104 70-130
1,1,2,2-Tetrachloroethane mg/kg 0.520.5 105 70-130
1,1,2-Trichloroethane mg/kg 0.510.5 102 70-130
1,1-Dichloroethane mg/kg 0.540.5 108 70-130
1,1-Dichloroethene mg/kg 0.560.5 111 70-130
1,1-Dichloropropene mg/kg 0.560.5 112 70-130
1,2,3-Trichlorobenzene mg/kg 0.580.5 115 70-130
1,2,3-Trichloropropane mg/kg 0.550.5 109 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 30 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3971098LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 0.580.5 116 70-130
1,2,4-Trimethylbenzene mg/kg 0.570.5 114 70-130
1,2-Dibromo-3-chloropropane mg/kg 0.570.5 114 67-130
1,2-Dibromoethane (EDB)mg/kg 0.530.5 105 70-130
1,2-Dichlorobenzene mg/kg 0.540.5 108 70-130
1,2-Dichloroethane mg/kg 0.490.5 98 70-130
1,2-Dichloropropane mg/kg 0.490.5 99 70-130
1,3,5-Trimethylbenzene mg/kg 0.550.5 110 70-130
1,3-Dichlorobenzene mg/kg 0.540.5 107 70-130
1,3-Dichloropropane mg/kg 0.520.5 104 70-130
1,4-Dichlorobenzene mg/kg 0.510.5 102 70-130
2,2-Dichloropropane mg/kg 0.520.5 104 67-130
2-Butanone (MEK)mg/kg 1.01 104 66-130
2-Chlorotoluene mg/kg 0.530.5 106 70-130
2-Hexanone mg/kg 1.11 107 70-130
4-Chlorotoluene mg/kg 0.530.5 106 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 1.11 106 70-130
Acetone mg/kg 0.941 94 67-130
Benzene mg/kg 0.530.5 106 70-130
Bromobenzene mg/kg 0.510.5 103 70-130
Bromochloromethane mg/kg 0.520.5 104 70-130
Bromodichloromethane mg/kg 0.510.5 102 70-130
Bromoform mg/kg 0.560.5 112 70-130
Bromomethane mg/kg 0.39 v30.5 78 53-175
Carbon tetrachloride mg/kg 0.570.5 113 70-130
Chlorobenzene mg/kg 0.520.5 105 70-130
Chloroethane mg/kg 0.530.5 106 70-135
Chloroform mg/kg 0.520.5 104 70-130
Chloromethane mg/kg 0.580.5 116 64-130
cis-1,2-Dichloroethene mg/kg 0.520.5 105 70-130
cis-1,3-Dichloropropene mg/kg 0.540.5 109 70-130
Dibromochloromethane mg/kg 0.540.5 109 70-130
Dibromomethane mg/kg 0.560.5 111 70-130
Dichlorodifluoromethane mg/kg 0.59 v30.5 117 63-145
Diisopropyl ether mg/kg 0.510.5 103 68-130
Ethanol mg/kg 19.520 97 70-130
Ethylbenzene mg/kg 0.500.5 100 70-130
Hexachloro-1,3-butadiene mg/kg 0.580.5 116 70-130
Isopropylbenzene (Cumene)mg/kg 0.580.5 115 70-130
m&p-Xylene mg/kg 1.11 111 70-130
Methyl-tert-butyl ether mg/kg 0.510.5 103 70-130
Methylene Chloride mg/kg 0.460.5 91 67-130
n-Butylbenzene mg/kg 0.570.5 114 70-130
n-Propylbenzene mg/kg 0.530.5 106 70-130
Naphthalene mg/kg 0.590.5 117 70-130
o-Xylene mg/kg 0.550.5 110 70-130
p-Isopropyltoluene mg/kg 0.570.5 115 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 31 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3971098LABORATORY CONTROL SAMPLE:
LCSSpike
sec-Butylbenzene mg/kg 0.560.5 112 70-130
Styrene mg/kg 0.570.5 115 70-130
tert-Butylbenzene mg/kg 0.520.5 104 64-130
Tetrachloroethene mg/kg 0.570.5 113 70-130
Toluene mg/kg 0.510.5 103 70-130
trans-1,2-Dichloroethene mg/kg 0.530.5 105 70-130
trans-1,3-Dichloropropene mg/kg 0.550.5 111 70-130
Trichloroethene mg/kg 0.550.5 109 70-130
Trichlorofluoromethane mg/kg 0.510.5 102 70-130
Vinyl acetate mg/kg 1.11 109 70-134
Vinyl chloride mg/kg 0.490.5 98 68-130
Xylene (Total)mg/kg 1.71.5 110 70-130
1,2-Dichloroethane-d4 (S)%92 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3971099MATRIX SPIKE SAMPLE:
MSSpike
Result
92659357001
1,1,1,2-Tetrachloroethane mg/kg 0.740.63 116 58-140ND
1,1,1-Trichloroethane mg/kg 0.710.63 112 58-144ND
1,1,2,2-Tetrachloroethane mg/kg 0.740.63 116 52-139ND
1,1,2-Trichloroethane mg/kg 0.710.63 111 56-140ND
1,1-Dichloroethane mg/kg 0.790.63 124 58-145ND
1,1-Dichloroethene mg/kg 0.850.63 134 57-158ND
1,1-Dichloropropene mg/kg 0.770.63 121 58-151ND
1,2,3-Trichlorobenzene mg/kg 0.13 M10.63 20 48-149ND
1,2,3-Trichloropropane mg/kg 0.750.63 117 54-132ND
1,2,4-Trichlorobenzene mg/kg 0.360.63 56 51-151ND
1,2,4-Trimethylbenzene mg/kg 0.700.63 110 38-170ND
1,2-Dibromo-3-chloropropane mg/kg 0.460.63 71 44-134ND
1,2-Dibromoethane (EDB)mg/kg 0.720.63 113 60-138ND
1,2-Dichlorobenzene mg/kg 0.680.63 107 59-147ND
1,2-Dichloroethane mg/kg 0.720.63 113 57-139ND
1,2-Dichloropropane mg/kg 0.700.63 109 62-145ND
1,3,5-Trimethylbenzene mg/kg 0.670.63 105 47-159ND
1,3-Dichlorobenzene mg/kg 0.680.63 106 58-144ND
1,3-Dichloropropane mg/kg 0.700.63 110 60-142ND
1,4-Dichlorobenzene mg/kg 0.650.63 102 57-143ND
2,2-Dichloropropane mg/kg 0.690.63 108 37-144ND
2-Butanone (MEK)mg/kg 1.31.2 104 28-146ND
2-Chlorotoluene mg/kg 0.660.63 104 55-158ND
2-Hexanone mg/kg 1.21.2 97 44-141ND
4-Chlorotoluene mg/kg 0.660.63 103 55-146ND
4-Methyl-2-pentanone (MIBK)mg/kg 1.41.2 107 50-138ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 32 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3971099MATRIX SPIKE SAMPLE:
MSSpike
Result
92659357001
Acetone mg/kg 1.01.2 82 20-136ND
Benzene mg/kg 0.750.63 117 60-145ND
Bromobenzene mg/kg 0.660.63 103 59-145ND
Bromochloromethane mg/kg 0.740.63 117 57-143ND
Bromodichloromethane mg/kg 0.720.63 113 53-133ND
Bromoform mg/kg 0.760.63 119 48-133ND
Bromomethane mg/kg 0.51 v30.63 80 10-167ND
Carbon tetrachloride mg/kg 0.650.63 102 57-147ND
Chlorobenzene mg/kg 0.710.63 111 61-144ND
Chloroethane mg/kg 0.630.63 99 10-153ND
Chloroform mg/kg 0.760.63 119 58-141ND
Chloromethane mg/kg 0.820.63 129 54-165ND
cis-1,2-Dichloroethene mg/kg 0.770.63 120 59-144ND
cis-1,3-Dichloropropene mg/kg 0.740.63 115 56-137ND
Dibromochloromethane mg/kg 0.730.63 114 53-139ND
Dibromomethane mg/kg 0.720.63 113 60-136ND
Dichlorodifluoromethane mg/kg 0.83 v30.63 130 49-177ND
Diisopropyl ether mg/kg 0.740.63 116 53-136ND
Ethanol mg/kg ND M125.5 0 70-130ND
Ethylbenzene mg/kg 0.650.63 102 53-150ND
Hexachloro-1,3-butadiene mg/kg 0.660.63 104 42-186ND
Isopropylbenzene (Cumene)mg/kg 0.780.63 122 62-154ND
m&p-Xylene mg/kg 1.51.2 115 49-156ND
Methyl-tert-butyl ether mg/kg 0.710.63 111 54-133ND
Methylene Chloride mg/kg 0.700.63 110 50-153ND
n-Butylbenzene mg/kg 0.660.63 104 44-174ND
n-Propylbenzene mg/kg 0.640.63 101 52-157ND
Naphthalene mg/kg 0.13 M10.63 20 37-150ND
o-Xylene mg/kg 0.750.63 118 54-150ND
p-Isopropyltoluene mg/kg 0.720.63 113 50-164ND
sec-Butylbenzene mg/kg 0.690.63 109 58-161ND
Styrene mg/kg 0.750.63 117 60-148ND
tert-Butylbenzene mg/kg 0.640.63 101 44-151ND
Tetrachloroethene mg/kg 0.720.63 110 53-1510.019
Toluene mg/kg 0.720.63 113 52-148ND
trans-1,2-Dichloroethene mg/kg 0.800.63 125 60-148ND
trans-1,3-Dichloropropene mg/kg 0.730.63 115 55-133ND
Trichloroethene mg/kg 0.750.63 117 60-148ND
Trichlorofluoromethane mg/kg 0.660.63 104 10-154ND
Vinyl acetate mg/kg 1.41.2 112 50-149ND
Vinyl chloride mg/kg 0.640.63 101 57-157ND
Xylene (Total)mg/kg 2.21.9 116 52-153ND
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%105 70-130
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 33 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92659357002
3971100SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg ND 30ND
1,1,1-Trichloroethane mg/kg ND 30ND
1,1,2,2-Tetrachloroethane mg/kg ND 30ND
1,1,2-Trichloroethane mg/kg ND 30ND
1,1-Dichloroethane mg/kg ND 30ND
1,1-Dichloroethene mg/kg ND 30ND
1,1-Dichloropropene mg/kg ND 30ND
1,2,3-Trichlorobenzene mg/kg ND 30ND
1,2,3-Trichloropropane mg/kg ND 30ND
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2,4-Trimethylbenzene mg/kg ND 30ND
1,2-Dibromo-3-chloropropane mg/kg ND 30ND
1,2-Dibromoethane (EDB)mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,2-Dichloroethane mg/kg ND 30ND
1,2-Dichloropropane mg/kg ND 30ND
1,3,5-Trimethylbenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,3-Dichloropropane mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
2,2-Dichloropropane mg/kg ND 30ND
2-Butanone (MEK)mg/kg ND 30ND
2-Chlorotoluene mg/kg ND 30ND
2-Hexanone mg/kg ND 30ND
4-Chlorotoluene mg/kg ND 30ND
4-Methyl-2-pentanone (MIBK)mg/kg ND 30ND
Acetone mg/kg ND 30ND
Benzene mg/kg ND 30ND
Bromobenzene mg/kg ND 30ND
Bromochloromethane mg/kg ND 30ND
Bromodichloromethane mg/kg ND 30ND
Bromoform mg/kg ND 30ND
Bromomethane mg/kg ND v230ND
Carbon tetrachloride mg/kg ND 30ND
Chlorobenzene mg/kg ND 30ND
Chloroethane mg/kg ND 30ND
Chloroform mg/kg ND 30ND
Chloromethane mg/kg ND 30ND
cis-1,2-Dichloroethene mg/kg ND 30ND
cis-1,3-Dichloropropene mg/kg ND 30ND
Dibromochloromethane mg/kg ND 30ND
Dibromomethane mg/kg ND 30ND
Dichlorodifluoromethane mg/kg ND v230ND
Diisopropyl ether mg/kg ND 30ND
Ethanol mg/kg ND 30ND
Ethylbenzene mg/kg ND 30ND
Hexachloro-1,3-butadiene mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 34 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92659357002
3971100SAMPLE DUPLICATE:
Isopropylbenzene (Cumene)mg/kg ND 30ND
m&p-Xylene mg/kg .0058J 30ND
Methyl-tert-butyl ether mg/kg ND 30ND
Methylene Chloride mg/kg ND 30ND
n-Butylbenzene mg/kg ND 30ND
n-Propylbenzene mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
o-Xylene mg/kg ND 30ND
p-Isopropyltoluene mg/kg ND 30ND
sec-Butylbenzene mg/kg ND 30ND
Styrene mg/kg ND 30ND
tert-Butylbenzene mg/kg ND 30ND
Tetrachloroethene mg/kg 0.0090 7 300.0084
Toluene mg/kg ND 30ND
trans-1,2-Dichloroethene mg/kg ND 30ND
trans-1,3-Dichloropropene mg/kg ND 30ND
Trichloroethene mg/kg ND 30ND
Trichlorofluoromethane mg/kg ND 30ND
Vinyl acetate mg/kg ND 30ND
Vinyl chloride mg/kg ND 30ND
Xylene (Total)mg/kg ND 30ND
1,2-Dichloroethane-d4 (S)%99107
4-Bromofluorobenzene (S)%10296
Toluene-d8 (S)%101101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 35 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
763056
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92657988001, 92657988002, 92657988003, 92657988004, 92657988005
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92658020001
3962965SAMPLE DUPLICATE:
Percent Moisture %5.6 N23255.5
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92657988005
3962966SAMPLE DUPLICATE:
Percent Moisture %31.5 N242532.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 36 of 63
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92657988
G-8098 Dodsons
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Common Laboratory Contaminant.C9
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 37 of 63
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92657988
G-8098 Dodsons
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92657988001 764398 764542N-1 EPA 5035A/5030B EPA 8260D
92657988002 764089 764290E-1 EPA 5035A/5030B EPA 8260D
92657988003 764749 764883S-1 EPA 5035A/5030B EPA 8260D
92657988004 764398 764542W-1 EPA 5035A/5030B EPA 8260D
92657988005 764398 764542B-1 EPA 5035A/5030B EPA 8260D
92657988001 763056N-1 SW-846
92657988002 763056E-1 SW-846
92657988003 763056S-1 SW-846
92657988004 763056W-1 SW-846
92657988005 763056B-1 SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/03/2023 04:25 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 38 of 63
Pa
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Page 40 of 63
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
March 29, 2023
Stephanie Knott
Pace Analytical Services - NC
1377 South Park Dr.
Kernersville, NC 27284
Project Location: G-8098 Dodsons
Client Job Number:
Project Number: 92657988
Laboratory Work Order Number: 23C2411
Enclosed are results of analyses for samples as received by the laboratory on March 22, 2023. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Rebecca Faust
Project Manager
Page 1 of 23
Table of Contents
Page 41 of 63
Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 5
23C2411-01 5
23C2411-02 7
23C2411-03 9
23C2411-04 11
23C2411-05 13
Sample Preparation Information 15
QC Data 16
Petroleum Hydrocarbons Analyses - VPH 16
B334978 16
Flag/Qualifier Summary 18
Certifications 19
Chain of Custody/Sample Receipt 20
Page 2 of 23
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
3/29/2023
Pace Analytical Services - NC
1377 South Park Dr.
Kernersville, NC 27284
ATTN: Stephanie Knott
92657988
23C2411
The results of analyses performed on the following samples submitted to CON-TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
G-8098 Dodsons
N-1 23C2411-01 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
E-1 23C2411-02 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
S-1 23C2411-03 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
W-1 23C2411-04 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
B-1 23C2411-05 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
[TOC_1]Sample Summary[TOC]
Page 3 of 23
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method MA VPH only hydrocarbon ranges were requested and reported.
[TOC_1]Case Narrative[TOC]
MADEP-VPH-Feb 2018 Rev 2.1
Qualifications:
Surrogate recovery outside of control limits due to suspected sample matrix interference. Chromatogram(s) is attached.
Analyte & Samples(s) Qualified:
S-15
2,5-Dibromotoluene (FID)
23C2411-03[S-1]
2,5-Dibromotoluene (PID)
23C2411-03[S-1]
MADEP-VPH-Feb 2018 Rev 2.1
No significant modifications were made to the method. All VPH samples were received preserved properly in methanol with a soil/methanol ratio of 1:1 +/- 25% completely
covered by methanol in the proper containers specified on the chain-of-custody form unless specified in this narrative.
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
The results of analyses reported only relate to samples submitted to Con-Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Meghan E. Kelley
Reporting Specialist
Page 4 of 23
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Date Received: 3/22/2023
Work Order: 23C2411Sample Description:Project Location: G-8098 Dodsons
Sample ID: 23C2411-01
Field Sample #: N-1
Sample Matrix: Soil
Sampled: 3/21/2023 11:30
[TOC_2]23C2411-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.04
Petroleum Hydrocarbons Analyses - VPH
ND 16 3/24/23 7:06 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 16 3/24/23 7:06 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 16 3/24/23 7:06 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 16 3/24/23 7:06 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 16 3/24/23 7:06 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)104 3/24/23 7:0670-130
2,5-Dibromotoluene (PID)102 3/24/23 7:0670-130
[TOC_1]Sample Results[TOC]
Page 5 of 23
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/22/2023
Work Order: 23C2411Sample Description:Project Location: G-8098 Dodsons
Sample ID: 23C2411-01
Field Sample #: N-1
Sample Matrix: Soil
Sampled: 3/21/2023 11:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
68.0 3/23/23 7:19 WDC% Wt 3/23/23SM 2540G1% Solids
Page 6 of 23
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Date Received: 3/22/2023
Work Order: 23C2411Sample Description:Project Location: G-8098 Dodsons
Sample ID: 23C2411-02
Field Sample #: E-1
Sample Matrix: Soil
Sampled: 3/21/2023 09:30
[TOC_2]23C2411-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.73
Petroleum Hydrocarbons Analyses - VPH
ND 9.5 3/23/23 16:16 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 9.5 3/23/23 16:16 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 9.5 3/23/23 16:16 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 9.5 3/23/23 16:16 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 9.5 3/23/23 16:16 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)79.7 3/23/23 16:1670-130
2,5-Dibromotoluene (PID)78.5 3/23/23 16:1670-130
Page 7 of 23
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/22/2023
Work Order: 23C2411Sample Description:Project Location: G-8098 Dodsons
Sample ID: 23C2411-02
Field Sample #: E-1
Sample Matrix: Soil
Sampled: 3/21/2023 09:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
72.9 3/23/23 7:19 WDC% Wt 3/23/23SM 2540G1% Solids
Page 8 of 23
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Date Received: 3/22/2023
Work Order: 23C2411Sample Description:Project Location: G-8098 Dodsons
Sample ID: 23C2411-03
Field Sample #: S-1
Sample Matrix: Soil
Sampled: 3/21/2023 09:20
[TOC_2]23C2411-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.05
Petroleum Hydrocarbons Analyses - VPH
1700 890 3/23/23 17:45 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
50Unadjusted C5-C8 Aliphatics
1700 890 3/23/23 17:45 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
50C5-C8 Aliphatics
3700 890 3/23/23 17:45 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
50Unadjusted C9-C12 Aliphatics
ND 890 3/23/23 17:45 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
50C9-C12 Aliphatics
2600 890 3/23/23 17:45 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
50C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)135 3/23/23 17:45*S-1570-130
2,5-Dibromotoluene (PID)135 3/23/23 17:45*S-1570-130
Page 9 of 23
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Date Received: 3/22/2023
Work Order: 23C2411Sample Description:Project Location: G-8098 Dodsons
Sample ID: 23C2411-03
Field Sample #: S-1
Sample Matrix: Soil
Sampled: 3/21/2023 09:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
71.7 3/23/23 7:19 WDC% Wt 3/23/23SM 2540G1% Solids
Page 10 of 23
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Date Received: 3/22/2023
Work Order: 23C2411Sample Description:Project Location: G-8098 Dodsons
Sample ID: 23C2411-04
Field Sample #: W-1
Sample Matrix: Soil
Sampled: 3/21/2023 09:10
[TOC_2]23C2411-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.13
Petroleum Hydrocarbons Analyses - VPH
ND 17 3/23/23 16:46 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 17 3/23/23 16:46 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 17 3/23/23 16:46 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 17 3/23/23 16:46 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 17 3/23/23 16:46 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)88.0 3/23/23 16:4670-130
2,5-Dibromotoluene (PID)85.6 3/23/23 16:4670-130
Page 11 of 23
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Date Received: 3/22/2023
Work Order: 23C2411Sample Description:Project Location: G-8098 Dodsons
Sample ID: 23C2411-04
Field Sample #: W-1
Sample Matrix: Soil
Sampled: 3/21/2023 09:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
68.6 3/23/23 7:19 WDC% Wt 3/23/23SM 2540G1% Solids
Page 12 of 23
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Date Received: 3/22/2023
Work Order: 23C2411Sample Description:Project Location: G-8098 Dodsons
Sample ID: 23C2411-05
Field Sample #: B-1
Sample Matrix: Soil
Sampled: 3/21/2023 12:00
[TOC_2]23C2411-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.14
Petroleum Hydrocarbons Analyses - VPH
3500 860 3/23/23 18:14 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
50Unadjusted C5-C8 Aliphatics
3400 860 3/23/23 18:14 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
50C5-C8 Aliphatics
2000 860 3/23/23 18:14 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
50Unadjusted C9-C12 Aliphatics
ND 860 3/23/23 18:14 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
50C9-C12 Aliphatics
1300 860 3/23/23 18:14 EEHmg/Kg dry 3/23/23MADEP-VPH-Feb 2018
Rev 2.1
50C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)120 3/23/23 18:1470-130
2,5-Dibromotoluene (PID)117 3/23/23 18:1470-130
Page 13 of 23
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Date Received: 3/22/2023
Work Order: 23C2411Sample Description:Project Location: G-8098 Dodsons
Sample ID: 23C2411-05
Field Sample #: B-1
Sample Matrix: Soil
Sampled: 3/21/2023 12:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
67.2 3/23/23 7:19 WDC% Wt 3/23/23SM 2540G1% Solids
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Sample Extraction Data
Prep Method: MA VPH Analytical Method: MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B334978 03/23/2315.6 16.523C2411-01 [N-1]
B334978 03/23/2317.3 12.023C2411-02 [E-1]
B334978 03/23/2310.5 13.423C2411-03 [S-1]
B334978 03/23/2311.3 13.123C2411-04 [W-1]
B334978 03/23/2311.4 13.223C2411-05 [B-1]
Prep Method: % Solids Analytical Method: SM 2540G
Lab Number [Field ID]Batch Date
B334958 03/23/2323C2411-01 [N-1]
B334958 03/23/2323C2411-02 [E-1]
B334958 03/23/2323C2411-03 [S-1]
B334958 03/23/2323C2411-04 [W-1]
B334958 03/23/2323C2411-05 [B-1]
[TOC_1]Sample Preparation Information[TOC]
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]
Batch B334978 - MA VPH
[TOC_3]B334978[TOC]
Blank (B334978-BLK1) Prepared & Analyzed: 03/23/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10ND
C5-C8 Aliphatics mg/Kg wet10ND
Unadjusted C9-C12 Aliphatics mg/Kg wet10ND
C9-C12 Aliphatics mg/Kg wet10ND
C9-C10 Aromatics mg/Kg wet10ND
Benzene mg/Kg wet0.050ND
Butylcyclohexane mg/Kg wet0.050ND
Decane mg/Kg wet0.050ND
Ethylbenzene mg/Kg wet0.050ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050ND
2-Methylpentane mg/Kg wet0.050ND
Naphthalene mg/Kg wet0.50ND
Nonane mg/Kg wet0.050ND
Pentane mg/Kg wet0.050ND
Toluene mg/Kg wet0.050ND
1,2,4-Trimethylbenzene mg/Kg wet0.050ND
2,2,4-Trimethylpentane mg/Kg wet0.050ND
m+p Xylene mg/Kg wet0.10ND
o-Xylene mg/Kg wet0.050ND
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)88.835.5
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)87.435.0
LCS (B334978-BS1) Prepared & Analyzed: 03/23/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10 7.50 70-1301027.66
Unadjusted C9-C12 Aliphatics mg/Kg wet10 7.50 70-13099.57.46
C9-C10 Aromatics mg/Kg wet10 2.50 70-1301012.51
Benzene mg/Kg wet0.050 2.50 70-1301072.67
Butylcyclohexane mg/Kg wet0.050 2.50 70-1301082.70
Decane mg/Kg wet0.050 2.50 70-13080.52.01
Ethylbenzene mg/Kg wet0.050 2.50 70-1301022.56
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050 2.50 70-1301072.66
2-Methylpentane mg/Kg wet0.050 2.50 70-1301052.63
Naphthalene mg/Kg wet0.50 2.50 70-13093.12.33
Nonane mg/Kg wet0.050 2.50 30-1301102.75
Pentane mg/Kg wet0.050 2.50 70-1301042.60
Toluene mg/Kg wet0.050 2.50 70-1301032.59
1,2,4-Trimethylbenzene mg/Kg wet0.050 2.50 70-1301012.51
2,2,4-Trimethylpentane mg/Kg wet0.050 2.50 70-13096.92.42
m+p Xylene mg/Kg wet0.10 5.00 70-1301015.07
o-Xylene mg/Kg wet0.050 2.50 70-1301022.55
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)11044.1
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)11043.9
[TOC_1]QC Data[TOC]
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B334978 - MA VPH
LCS Dup (B334978-BSD1) Prepared & Analyzed: 03/23/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10 7.50 2570-130101 0.7197.60
Unadjusted C9-C12 Aliphatics mg/Kg wet10 7.50 2570-13098.7 0.8047.40
C9-C10 Aromatics mg/Kg wet10 2.50 2570-130101 0.8242.53
Benzene mg/Kg wet0.050 2.50 2570-130107 0.4902.68
Butylcyclohexane mg/Kg wet0.050 2.50 2570-130108 0.05382.70
Decane mg/Kg wet0.050 2.50 2570-13079.5 1.231.99
Ethylbenzene mg/Kg wet0.050 2.50 2570-130103 0.5012.57
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050 2.50 2570-130102 4.662.54
2-Methylpentane mg/Kg wet0.050 2.50 2570-130104 1.612.59
Naphthalene mg/Kg wet0.50 2.50 2570-13083.7 10.62.09
Nonane mg/Kg wet0.050 2.50 2530-130109 1.232.72
Pentane mg/Kg wet0.050 2.50 2570-130106 1.802.65
Toluene mg/Kg wet0.050 2.50 2570-130104 0.5502.60
1,2,4-Trimethylbenzene mg/Kg wet0.050 2.50 2570-130101 0.8242.53
2,2,4-Trimethylpentane mg/Kg wet0.050 2.50 2570-13094.5 2.512.36
m+p Xylene mg/Kg wet0.10 5.00 2570-130102 0.9325.12
o-Xylene mg/Kg wet0.050 2.50 2570-130103 0.9412.58
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)99.339.7
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)98.839.5
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FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
†Wide recovery limits established for difficult compound.
‡Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
Surrogate recovery outside of control limits due to suspected sample matrix interference. Chromatogram(s) is
attached.
S-15
[TOC_1]Flag/Qualifier Summary[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
MADEP-VPH-Feb 2018 Rev 2.1 in Soil
CT,NC,ME,NH-PUnadjusted C5-C8 Aliphatics
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PUnadjusted C9-C12 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
[TOC_1]Certifications[TOC]
Con-Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations:
Code Description Number Expires
PH-0821Connecticut Department of Public HealthCT 12/31/2024
652North Carolina Div. of Water QualityNC 12/31/2023
MA00100State of MaineME 06/9/2023
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2023
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