WS-4699_15269_CA_MRP_20220210

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
February 14, 2022
Ms. Linda Estkowski
NCDEQ-UST Section
Winston-Salem Regional Office
450 W. Hanes Mill Road
Suite 300
Winston-Salem, NC 27105
Re: Ground Water Monitoring Report
December 2021
Garrison’s Store
5040 NC 65
Reidsville, Rockingham County
North Carolina
Facility ID Number: 00-0-0000018626
Incident Number: 15269
GRI Project Number: 5784
Dear Ms. Estkowski,
Please find enclosed the referenced report for the above mentioned site.
If you have any questions, please contact William Regenthal at 704-845-4010.
Sincerely,
Geological Resources, Inc.
Leslie Maxtone-Graham
Administrative Assistant
Enclosure
Cc: John D. Love Oil Company, Inc., file
3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Ground Water Monitoring Report
December 2021
Garrison’s Store
5040 NC 65
Reidsville, Rockingham County
North Carolina
Facility ID Number: 00-0-0000018626
Incident Number: 15269
GRI Project Number: 5784
Prepared for:
John D. Love Oil Company, Inc.
Post Office Box 1148
Reidsville, North Carolina 27320
February 10, 2022
Project Manager Report Writer
___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 10, 2022 Garrison’s Store
Project Manager: William Regenthal, P. G. GRI Project No. 5784
i
SITE INFORMATION
1. Site Identification
 Garrison’s Store (Facility ID 00-0-0000018626)
 Incident Number 15269 – High Risk (H160)
 Location of Source Area: 5040 NC 65
Reidsville, NC 28314
Rockingham County
36.232503N, 79.822263°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System
UST Owner
John D. Love Oil Company, Inc.
Post Office Box 1148
Reidsville, North Carolina 27320
[e-mail]
336-349-8414
UST Operator
John D. Love Oil Company, Inc.
Post Office Box 1148
Reidsville, North Carolina 27320
[e-mail]
336-349-8414
Property Owner
Melinda Martin Hawkins
5040 NC 65
Reidsville, NC 27320
Email unknown
Phone unknown
Property Occupant
Unknown
Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010
Analytical Laboratory
SGS- North America, Inc.
4405 Vineland Road, Suite C-15
Orlando, FL 32811
State Certification No. 573
407-425-6700
3. Information about Release
 Release was discovered on March 11, 1996.
 An unknown amount of product was released from the leaking UST System.
 One 2000-gallon gasoline UST, one 1000-gallon gasoline UST, two 550-gallon gasoline USTs and
one 280-gallon kerosene UST were removed from the site in 1988. No USTs remain on site.
___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 10, 2022 Garrison’s Store
Project Manager: William Regenthal, P. G. GRI Project No. 5784
ii
EXECUTIVE SUMMARY
Garrison’s Store is located at 5040 NC 65 in Reidsville, Rockingham County, North Carolina. The site is
currently owned by Melinda Martin Hawkins. One 2000-gallon gasoline UST, one 1000-gallon gasoline
UST, two 550-gallon gasoline USTs and one 280-gallon kerosene UST were removed from the site in 1988.
No USTs remain at the site. In March 1996, a water sample from the site’s water supply well confirmed
the presence of petroleum hydrocarbons.
In 1997, fourteen Type II monitoring wells and two Type III monitoring wells were installed at the site. A
CSA was submitted in 1997 and a CAP approved in August 1998. An AS system and a SVE system were
started in August 1999. The system was still in operation in 2004 and deactivated sometime prior to 2008.
An updated receptor survey was conducted in November 2021. The adjoining properties are residential
or undeveloped land. No potable wells are located within 1,000 feet of the site. Public water is available
to the site and surrounding area.
On November 24, 2021, six Type II and two Type III monitoring wells were gauged, purged and sampled.
Free product was not found during the November 2021 sampling event. Contaminant concentrations that
exceeded the MACs were reported in the ground water samples collected from MW-3, MW-5, MW-8, and
TW-1. All of the reported contaminant concentrations were less than the GCLs.
Based on this information, the risk classification for the site should be reclassified as low. Subsequent to
filing an NRP and completing public notification, the incident should be closed and no further action
should be required.
___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 10, 2022 Garrison’s Store
Project Manager: William Regenthal, P. G. GRI Project No. 5784
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons
___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 10, 2022 Garrison’s Store
Project Manager: William Regenthal, P. G. GRI Project No. 5784
TABLE OF CONTENTS
SITE INFORMATION ............................................................................................................................ i
EXECUTIVE SUMMARY ....................................................................................................................... ii
ACRONYMS ....................................................................................................................................... iii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................2
3.0 FREE PRODUCT REMOVAL ........................................................................................................4
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................4
5.0 CONCLUSIONS .........................................................................................................................4
6.0 LIMITATIONS ...........................................................................................................................5
7.0 STATEMENTS AND CERTIFICATION ...........................................................................................5
FIGURES
Figure 1: Site Location Map
Figure 2A: Site Vicinity Map
Figure 2B: Land Use Map
Figure 3: Site Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map
Figure 6: Estimated Contaminant Mass Map
TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Water Supply Well Owner Information
Table 4: Adjacent Property Owner Information
Table 5: Land Use Information
Table 6: Well Construction and Gauging Information
Table 7: Summary of Ground Water Sample Analytical Results
APPENDICES
Appendix A: State Correspondence
Appendix B: Historical Ground Water Gauging Data
Appendix C: Historical Ground Water Quality Data
Appendix D: County Parcel Cards
Appendix E: Laboratory Report – Ground Water Samples
Appendix F: Contaminant Mass Calculations
___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 10, 2022 Garrison’s Store
Project Manager: William Regenthal, P. G. GRI Project No. 5784
1
1.0 SITE HISTORY AND CHARACTERIZATION
GRI presents the results of the November 24, 2021, updated receptor survey activities and ground water
sampling event at the Garrison’s Store site located at 5040 NC 65 in Reidsville, Rockingham County, North
Carolina (Figures 1 and 2A). These activities were conducted in accordance with GRI Proposal No. 21-564,
which was submitted to the North Carolina Department of Environmental Quality (NCDEQ) on September
3, 2021 and was approved as Task Authorization No. 15269-24 on October 27, 2021. State
correspondence has been included as Appendix A.
The site is currently owned by Melinda Martin Hawkins. Four various sized gasoline USTs and one 280-
gallon kerosene UST were removed from the site in 1988. No USTs remain at the site.
On March 11, 1996, a release was discovered when a water sample collected from the on-site water
supply well (WSW-1) confirmed the presence of petroleum hydrocarbons. In 2007, the site connected to
public water and WSW-1 is no longer in service. The store is not in use and no petroleum products are
being sold. UST owner/operator information and UST system information are included as Tables 1 and 2,
respectively. The Registered Tank Report is shown below:
In 1997, fourteen Type II monitoring wells (MW-1 through MW-14) and two Type III monitoring wells (TW-
1 and TW-2) were installed at the site. A Site Map showing the locations of the monitoring wells and the
structures on-site has been included as Figure 3. Historical ground water gauging and quality information
are included as Appendix B and Appendix C, respectively.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 10, 2022 Garrison’s Store
Project Manager: William Regenthal, P. G. GRI Project No. 5784
2
A CSA Report was submitted May 14, 1997; and, a CAP was submitted in March 1998 and approved in
August 1998.

An AS system consisting of fifteen AS wells and a SVE system consisting of eight SVE wells was started in
August of 1999. A report from a previous consultant indicated the system was still in operation in 2004
and deactivated sometime prior to 2008. The actual date of deactivation is unknown.

The surrounding area is a mixture of residential, and undeveloped land. The site contains two buildings
and is partially capped with concrete and asphalt. The overall topography at the site is relatively flat.

In 2013, a Comprehensive Water Supply Survey identified four private wells within 1,500 feet of the site
with the closest well approximately 1,150 feet away. Subsequent receptor surveys have indicated the
location and status of the water supply wells had not changed. In November 2021, GRI conducted an
updated receptor survey at the site. Three of the four properties reported with private potable wells
(WSW-4, WSW-5, and WSW-7) do not have municipal water connections. A well survey was provided to
WSW-6, but no response has been received at the submission of this report; WSW-6 is located beyond
1,000 feet from the site. Public water is available to the site and surrounding area.

Land use in the surrounding area is agricultural and residential. A Site Vicinity Map depicting the locations
of water supply wells has been included as Figure 2A. A Land Use Map is included as Figure 2B. Well
owner information is summarized in Table 3. Adjacent property owner information is presented in Table
4. Land use information is presented in Table 5. County parcel cards are included as Appendix D.

Although GRI cannot verify the accuracy of information obtained from previous reports, for the purposes
of this report, it is assumed to be correct. Please refer to previous submittals for further historical
information regarding the site.
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
On November 24, 2021, six Type II monitoring wells (MW-1, MW-3, MW-4, MW-5, MW-8, and MW-9) and
two Type III monitoring wells (TW-1, and TW-2) were gauged. Wells MW-2, MW-6, MW-7, MW-10 and
MW-11 were not located. Depths to ground water in the Type II monitoring wells ranged from 16.69 feet
to 18.73 feet. Depths to ground water in the Type III monitoring wells ranged from 16.69 feet to 18.73
feet. Ground water elevations in the Type II monitoring wells relative to a temporary benchmark with an
assumed datum of 100.00 feet ranged from 13.66 to 17.12 feet. Based on this information, ground water
flow direction is generally toward the east. The horizontal hydraulic gradient across the site from MW-5
to MW-9 was approximately 0.01 feet per foot. Well construction and gauging information is presented
in Table 6. A Water Table Surface Map is included as Figure 4. A summary of the current ground water
gauging data is shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 10, 2022 Garrison’s Store
Project Manager: William Regenthal, P. G. GRI Project No. 5784
3
Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
MW-1 3-23 23 98.8 16.69 --- 82.11
MW-2 10-25 25 101.06 NF --- NF
MW-3 10-25 25 99.03 16.87 --- 82.16
MW-4 10-25 25 101.12 18.73 --- 82.39
MW-5 3-23 23 100.47 18.05 --- 82.42
MW-6 10-25 25 103.18 NF --- NF
MW-7 10-25 25 100.95 NF --- NF
MW-8 10-25 25 99.85 17.75 --- 82.10
MW-9 10-25 25 99.51 17.43 --- 82.08
MW-10 5-15 15 90.81 NF --- NF
MW-11 5-10 10 91.37 NF --- NF
TW-1 35-40 40 99.28 17.12 --- 82.16
TW-2 95-100 100 NM 13.66 --- NM

On November 24, 2021, six Type II monitoring wells (MW-1, MW-3, MW-4, MW-5, MW-8, and MW-9) and
two Type III monitoring wells (TW-1 and TW-2) were purged and sampled. Ground water samples
collected from the monitoring wells were submitted for laboratory analyses using EPA Method 6200B.
Concentrations of benzene, toluene, xylenes, MTBE, naphthalene, TAA, TBA, EDB, 1,2-dichloroethane, 1,2-
dichloropropane, methylene chloride, n-propylbenzene, 1,1,2-trichloroethane, 1,2,4-trimethylbenzene,
and/or 1,3,5-trimethylbenzene that exceeded the MACs were reported in the ground water samples
collected from MW-3, MW-5, MW-8, and TW-1. All the reported contaminant concentrations were below
the GCLs. A summary of the analytical results for ground water samples collected on November 24, 2021
is presented in Table 7. A Ground Water Quality Map based on the November 24, 2021 data is included
as Figure 5. A complete report of laboratory analyses of the ground water samples collected from the
monitoring wells during the November 2021 sampling event has been included as Appendix E. A summary
of the current ground water analytical data is shown below:

Contaminant of
Concern 
Be
n
z
e
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e

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e

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Well ID
MACs (µg/l) 1 600 600 500 20 6
GCL (µg/l) 5,000 260,000 80,000 50,000 20,000 6,000
MW-1 <0.13 <0.13 <0.13 <0.26 <0.13 <0.13
MW-3 1,860 10,200 1,870 9,020 <63 378
MW-4 0.24 J <0.13 <0.13 <0.26 <0.13 <0.13
MW-5 111 3.8 J 143 598 3.2 J 193
MW-8 13 0.96 8.7 10.7 <0.13 83.8
MW-9 <0.13 0.29 J 0.20 J 0.58 J <0.13 2
TB <0.13 <0.13 <0.13 <0.26 <0.13 <0.13
TW-1 4.2 0.36 J 0.61 J 0.52 J 46.2 1.1
TW-2 0.13 J 4.5 <0.13 <0.26 <0.13 0.25 J

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 10, 2022 Garrison’s Store
Project Manager: William Regenthal, P. G. GRI Project No. 5784
4
The baseline contaminant mass at the site was determined based on the total BTEX, MTBE and
naphthalene concentrations from the November 2018 ground water sampling event, as well as the
maximum historical water column height. The November 2018 data were selected because it was the
most recent, comprehensive monitoring event. A theoretical contaminant mass area was calculated
around MW-3, MW-5, and MW-8 and used in the contaminant mass calculations. The total contaminant
mass at the site has increased 1,096% since November 2018. However, this increase is reflective of the
decrease in depth to water measured in monitoring wells in 2021. Contaminant mass calculations have
been included as Appendix F. A map of the contaminant mass areas has been included as Figure 6. A
chart depicting the overall trend in contaminant mass is shown below:

The site is located in the Piedmont Physiographic Province of North Carolina. The water table has a
seasonal high depth to water of approximately 15 to 20 feet below ground surface (bgs).
3.0 FREE PRODUCT REMOVAL
No free product was present at the subject site.
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
No natural attenuation monitoring plan is currently in place at the site.
5.0 CONCLUSIONS
 Garrison’s Store is a former retail petroleum facility. No USTs or ASTs are in use at the site. The
store is no longer in use.
0.00
1.00
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Time
Total Contaminant Mass vs. Time
Garrison's Store (Incident No: 15269)
Contaminant Mass (grams)Water Column Height (ft)Linear (Contaminant Mass (grams))

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 10, 2022 Garrison’s Store
Project Manager: William Regenthal, P. G. GRI Project No. 5784
5
 Municipal water is available to the site. No water supply wells are located within 1,000 feet of
the site.
 On November 24, 2021, eight monitoring wells were gauged, purged and sampled. Ground water
flow at the site was generally toward the east.
 Concentrations of benzene, toluene, xylenes, MTBE, naphthalene, TAA, TBA, EDB, 1,2-
dichloroethane, 1,2-dichloropropane, methylene chloride, n-propylbenzene, 1,1,2-
trichloroethane, 1,2,4-trimethylbenzene, and/or 1,3,5-trimethylbenzene that exceeded the MACs
were reported in the ground water samples collected from MW-3, MW-5, MW-8, and TW-1.
 All the reported contaminant concentrations were below the GCLs.
 Based on this information, the risk classification for the site should be reclassified as low.
Subsequent to filing an NRP and completing public notification, the incident should be closed and
no further action should be required.
6.0 LIMITATIONS
This report has been prepared for the exclusive use of John D. Love Oil Company, Inc. for specific
application to the referenced site in Rockingham County, North Carolina. The assessment was conducted
based on the scope of work and level of effort desired by NCDEQ and with resources adequate only for
that scope of work. Our findings have been developed in accordance with generally accepted standards
of environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.
7.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. N/A Will this report be submitted after the
established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO
IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain
what was missing and why.
3 If applicable, will any of the proposed attenuation milestones under the schedule approved
in the Corrective Action Plan not be met? (within a reasonable margin of error)
YES NO
IF the answer to question #3 is “NO”, skip to the certification under #8 below.
IF the answer to question #3 is “YES”, please generally describe in this cell the possible reason(s) and
outline proposed remedies. (This should be described in more detail in the report text above.)

N/A

FIGURES
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SITE
795300757534
795300981148
795300666754
795300665613
795300778778
WSW-7
WSW-6
WSW-5
WSW-4
NC 65
IRON WORKS RD
³
FIGURE 2A: SITE VICINITY MAPGARRISON'S STORE5040 NC HIGHWAY 65REIDSVILLE, ROCKINGHAM COUNTYNORTH CAROLINAINCIDENT NO. 15269GRI PROJECT NO. 5784
PREPARED BY:GEOLOGICAL RESOURCES, INC.NOVEMBER 11, 2021
0 300150Feet1 inch = 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS 500-FOOT RADIUS
250-FOOT RADIUS
LEGEND
"J Water Supply Well
Roads
USGS_Streams
Ponds_&_Rivers
Well Owners and Adjacent Properties
Parcels795300882778
795300872511
"J
"J
"J
"J
SITE
WSW-7
WSW-6
WSW-5
WSW-4
NC 65
IRON WORKS RD
³

0 300150Feet1 inch = 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS 500-FOOT RADIUS
250-FOOT RADIUS
LEGEND
ZONING - RA
ZONING - HC
"J Water Supply Well
Roads
USGS_Streams
Ponds_&_Rivers
Parcels
FIGURE 2B: LAND USE MAPGARRISON'S STORE5040 NC HIGHWAY 65REIDSVILLE, ROCKINGHAM COUNTYNORTH CAROLINAINCIDENT NO. 15269GRI PROJECT NO. 5784
PREPARED BY:GEOLOGICAL RESOURCES, INC.NOVEMBER 11, 2021
NF: NOT FOUND
NM: NOT MEASURED

TABLES
UST ID Number 1-5 Facility ID Number
Owner or Operator?
Owner/Operator
TABLE 1
UST OWNER/OPERATOR INFORMATION
GARRISON'S STORE (INCIDENT NO. 15269)
00-0-0000018626
Name of Owner or Operator Dates of Ownership / Operation
John D. Love Oil Co., Inc.11/05/1980 - 1988
Address
Post Office Box 1148, Reidsville, North Carolina 27320 336-349-8414
Telephone Number
Page 1 of 1
Date: 11/24/21 Facility ID # : 00-0-0000018626
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline 2,000 05/01/80 Single Wall Steel 64″ x 12′Single Wall Steel Removed
12/01/1988 Yes
2 Gasoline 1,000 05/04/71 Single Wall Steel 46″ x 12′Single Wall Steel Removed
12/01/1988 Yes
3 Gasoline 550 05/07/56 Single Wall Steel 48″ x 6′Single Wall Steel Removed
12/01/1988 Yes
4 Kerosene 280 05/05/66 Single Wall Steel 36" x 62"Single Wall Steel Removed
12/01/1988 Yes
5 Gasoline 550 05/07/56 Single Wall Steel 45-1/2" x 76"Single Wall Steel Removed
12/01/1988 Yes
TABLE 2
UST SYSTEM INFORMATION
GARRISON'S STORE (INCIDENT NO. 15269)
Status
of
UST
UST
ID
No.
Current
or Most
Recent
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Page 1 of 1
Facility ID #: 00-0-0000018626
Well No.Parcel #Well Owner Mailing Address Well Location Address Well Usage Municipal
Water
Distance From
Approximate
Center of Site (ft)
WSW-4 795300666754 Robert B. & Linda Wilson 5189 NC Highway 65
Reidsville NC 27320-9335
5189 NC Highway 65
Reidsville NC 27320-9335 Potable No ~1500 SW
WSW-5 795300665613 Ronald Lee Wilson 4241 NC Highway 65
Reidsville NC 27320-9326
5193 NC Highway 65
Reidsville NC 27320-9335 Potable No ~1200 SW
WSW-6 795300882778 Catherine E Garrison 3238 Erwin Trace Drive
Charlotte, NC 28213-4896
3917 Iron Works Road
Reidsville NC 27320 Unknown No ~1150 SE
WSW-7 795300981148 Brian J. & Kelly Ann Berenger 3981 Iron Works Road
Reidsville NC 27320-8420
3981 Iron Works Road
Reidsville NC 27320-8420 Potable No ~1300 SE
Notes:
● The water supply wells are keyed to Figure 2B.
● Water supply well distances are based on measurements from the middle of the plume.
TABLE 3
SUMMARY OF WATER SUPPLY WELL OWNER INFORMATION
GARRISON'S STORE (INCIDENT NO. 15269)
Date: 11/24/21
Page 1 of 1
Facility ID #: 00-0-0000018626
795300778778 (Site) Melinda Martin Hawkins 5040 NC Highway 65
Reidsville, North Carolina 27320-9334
795300882778 Catherine E Garrison 3238 Erwin Trace Drive
Charlotte, North Carolina 28213-4896
795300872511 Paje Properties LLC 114 W Murphy St.
Madison, North Carolina 27025-1924
795300757534 Ivie Ann W. Ellington 287 Lovings Road
Reidsville, North Carolina 27320-8573
Note:
• Properties are keyed to Figure 2A.
TABLE 4
ADJACENT PROPERTY OWNER INFORMATION
GARRISON'S STORE (INCIDENT NO. 15269)
Date: 11/24/21
Tax PIN / Map ID Owner Address
Date: 11/24/21 Facility ID #: 00-0-0000018626
Map ID No.Land Use Feature Zoning Description Address
Distance from
Source Area
(feet)
n/a HC Highway Commercial n/a n/a
n/a RA Residential/ Agricultural n/a n/a
Note:
• Properties are keyed to Figure 2B.
TABLE 5
LAND USE INFORMATION
GARRISON'S STORE (INCIDENT NO. 15269)
Page 1 of 1
Date: 11/24/2021
11/18/2018 17.74 ---81.06
11/24/2021 16.69 ---82.11
11/18/2018 20.50 ---80.56
11/24/2021 NF ---NF
11/18/2018 18.00 ---81.03
11/24/2021 16.87 82.16
11/18/2018 12.95 ---88.17
11/24/2021 18.73 ---82.39
11/18/2018 19.37 ---81.10
11/24/2021 18.05 ---82.42
11/18/2018 NF ---NF
11/24/2021 NF ---NF
11/18/2018 20.79 ---80.16
11/24/2021 NF ---NF
11/18/2018 19.26 ---80.59
11/24/2021 17.75 ---82.10
11/18/2018 18.93 ---80.58
11/24/2021 17.43 ---82.08
11/18/2018 NF ---NF
11/24/2021 NF ---NF
11/18/2018 NM ---NM
11/24/2021 NF ---NF
11/18/2018 13.79 ---87.41
11/24/2021 NM ---NM
11/18/2018 24.41 ---80.52
11/24/2021 NM ---NM
11/18/2018 NF ---NF
11/24/2021 NM ---NM
11/18/2018 NF ---NF
11/24/2021 17.12 ---82.16
11/18/2018 20.10 ---NM
11/24/2021 13.66 ---NM
Notes:
• NF: Not found.
• NM: Not measured.
35 35-40 40 99.28
95-100 100 NM95
MW-14
TW-1
TW-2
01/16/97
09/09/97
04/09/97 10 10-25 25 100.57
101.20
MW-13 04/09/97 10 10-25 25 104.93
MW-12 04/09/97 10 10-25 25
MW-11 04/09/97 91.3755-10 10
99.51
MW-10 04/09/97 5 5-15 15 90.81
MW-9 01/20/97 10 10-25 25
100.95
MW-8 01/20/97 10 10-25 25 99.85
MW-7 01/20/97 10 10-25 25
100.47
MW-6 04/09/97 10 10-25 25 103.18
MW-5 01/16/97 3 3-23 23
01/20/97 10 10-25 25 101.06
99.03
MW-4 01/16/97 10 10-25 25 101.12
MW-3 01/20/97 10 10-25 25
• 2018 measurements are from December 2018 Ground Water Monitoring Report (Gipe & Assoc. PA)
TABLE 6
WELL CONSTRUCTION AND GAUGING INFORMATION
GARRISON'S STORE (INCIDENT NO. 15269)
Well ID Date Installed
(mm/dd/yy)
Date Water
Level Measured
(mm/dd/yyyy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation*
(ft.)
Depth to
Water from
Top of Casing
(feet)
Facility ID #: 00-0-0000018626
• * : Reference point for elevation measurements.
• ft BGS : feet below ground surface.
• Well Construction and top of casing information from April 2004 CSA (CBM Engineering, lnc)
Free Product
Thickness**
(ft.)
Ground
Water
Elevation
(ft.)
Comments
MW-1 3 3-23 23 98.8001/16/97
MW-2
Page 1 of 1
Date: 12/24/2021
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 40 10 0.02 0.4 0.6 400 70 0.6 400 400
5,000 260,000 80,000 50,000 20,000 6,000 40,000 10,000 50 400 600 400000 26100 600 28500 24100
MW-1 11/24/21 <0.13 <0.13 <0.13 <0.26 <0.13 <0.13 <2.0 <2.0 <0.13 <0.13 <0.13 <1.0 <0.13 <0.13 <0.13 <0.13
MW-3 11/24/21 1,860 10,200 1,870 9,020 <63 378 <1000 <1000 190 J <63 <63 751 J 121 J <63 787 434
MW-4 11/24/21 0.24 J <0.13 <0.13 <0.26 <0.13 <0.13 <2.0 <2.0 <0.13 <0.13 <0.13 <1.0 <0.13 <0.13 <0.13 <0.13
MW-5 11/24/21 111 3.8 J 143 598 3.2 J 193 448 33.6 J <1.3 6.7 <1.3 <10 32.9 <1.3 150 70.2
MW-8 11/24/21 13 0.96 8.7 10.7 <0.13 83.8 17.2 51.1 <0.13 3.7 <0.13 2.8 J 6.5 <0.13 10 1.4
MW-9 11/24/21 <0.13 0.29 J 0.20 J 0.58 J <0.13 2 <2.0 <2.0 <0.13 <0.13 <0.13 <1.0 <0.13 <0.13 0.16 J <0.13
TB 11/24/21 <0.13 <0.13 <0.13 <0.26 <0.13 <0.13 <2.0 <2.0 <0.13 <0.13 <0.13 1.4 J <0.13 <0.13 <0.13 <0.13
TW-1 11/24/21 4.2 0.36 J 0.61 J 0.52 J 46.2 1.1 25,600 E 898 <0.25 828 31.4 <2.0 <0.25 1.5 0.48 J <0.25
TW-2 11/24/21 0.13 J 4.5 <0.13 <0.26 <0.13 0.25 J <2.0 2.0 J <0.13 <0.13 <0.13 <1.0 <0.13 <0.13 <0.13 <0.13
Notes:
• Results reported in micrograms per liter (µg/l).
• < : Less than the method detection limit specified in the laboratory report.
• 2L Standard specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
• NE: Not Established
• Concentrations in bold face type exceeded the 2L standards.
• Concentrations in italics exceeded the gross contamination levels.
• Refer to laboratory report for detected constituents that did not exceed the MACs, or for which no standard has been established.
• J: Estimated concentration
TABLE 7
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
GARRISON'S STORE (INCIDENT NO: 15269)
Facility ID # : 00-0-0000018626
Analytical Method SM 6200B SM 6200B
1,
2
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4
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GCL (µg/l)
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Page 1 of 1

APPENDICES

APPENDIX A
State Correspondence

APPENDIX B
Historic Ground Water Gauging Data

APPENDIX C
Historic Ground Water Quality Data

APPENDIX D
County Parcel Cards

11/17/21, 1:34 PM Rockingham County NC Property Card
https://www.webgis.net/nc/rockingham/PropertyCard.php?pid=129841 1/4
DATE 10/02/21 ROCKINGHAM COUNTY PAGE 1 TIME 10:58:20 PROPERTY CARD PROG# AS2006 USER RKMARKMC FOR YEAR 2021 FLYING GRASS INC PARCEL ID.. 129841 PIN... 7953 00 77 8778 00 LOCATION... 5040 NC 65 DEED YEAR/BOOK/PAGE.. 2018 1552 1012 ASSESSMENT NONE .00 .00 .00 5040 NC HIGHWAY 65 PLAT BOOK/PAGE.. 82 65 OWNER ID.. 1326245 LEGAL DESC:0.88 AC LTS A & B & ADDL DISTRICT.. 113 BETHANY FD LOT FLYING GRASS SURVEY Area/Fire: 913 NEW BETHEL (BETHANY) TOWNSHIP... 5 NEW BETHEL REIDSVILLE NC 27320-9334 FLYING GRASS INC SURVEY NBRHOOD... C110 HWY 158 WEST DESCRIPTION CONVENIENCE STORE NH CLASS.. DESCRIPTION COMMERCIAL RES AG/HWY COMM CTY MAINTAINED.. 1/15/2021 BY RKCED VALUED.. 2/07/2020 BY RKGWIKE VISITED..... 2/04/2020 BY GW TYPE OF REVIEW ROUTING#.. 7801 PARCEL STATUS... ACTIVE CATEGORY.. REAL & PERSONAL . DISCLAIMER-OWNERSHIP, ZONING AND OTHER INFORMATION SHOULD BE VERIFIED. INFORMATION AND VALUE SUBJECT TO CHANGE. . ***** * LAND VALUED BY NEIGHBORHOOD BASE RATE METHOD * -------------------------------------------- SALES HISTORY ---------------------------------------------------- DEED BK/PAGE SALE DATE SALES INSTRUMENT DISQUALIFIED SALE AMOUNT STAMP AMOUNT DEED NAME 1592 2893 1/12/2021 DEED STAMPS BELOW MI HAWKINS MELINDA MARTIN 1552 1012 12/20/2018 DEED QUALIFIED 81,500 FLYING GRASS INC 17E 518 1/17/2017 ESTATE RELATED BUS OR FOULKS BRENDA H (1/2) & GARRIS 14E 228 1/01/2015 ESTATE RELATED BUS OR FOULKS BRENDA H(1/2); GARRISON 0001 0001 7/01/1986 DEED CONVERTED HINSON BESSIE C HEIRS -------------------------------------------- LAND SEGMENTS ---------------------------------------------------- LND STRAT LAND AVERAGE TOT CURRENT # ZONE CODE TYPE/CODE LAND QTY LAND RATE DPT% SHP% LOC% SIZ% OTH% TOP% ADJ FMV 1 RA/HC 100 AC RP .880 16,022.73 .00 .00 .00 .00 100.00 100.00 .00 14,100 TOTAL ACRES.. .880 TOTAL LAND FMV.. 14,100 ---------------------------------- IMPROVEMENT # 1 MAJOR IMPR-M ------------------------------------------------- MAIN FIN AREA.. 928.00 ACT/EFF YR/AGE.. 1939 1989 30 VISITED.. 2/04/2020 BY GW STRAT.......... 100 DESCRIPT.... RETAIL BLDG MAINTAINED.. 7/09/2020 BY RKDIWILSON MAIN GROUND SF.... 928.000 BUILT USE...... 40 RETAIL BLDG CURRENT USE.... CC CURRENT USE COMMERICAL LOCATION #..... 5040 NC 65 #BED: #BTH: #HBTH: COMPONENT TYPE/CODE/DESC PCT UNITS RATE STR# STR% SIZ% HGT% PER% CDS% COST %CMPL ----------------------------------------------------------------------------------------------------------------------- AC OPG OPEN PORCH GRADE 100 45.00 9.60 432 MA C02 GENERAL RETAIL FRAME 100 928.00 63.50 1.00 100.00 122.00 71,892 EW 03 ALUMINUM SIDING 100 122.00 .00 0 - AR 200 COMM NO HEAT 100 928.00 .00 0 - PD CL07 WOOD OR CEILING BOAR100 1.00 .00 0 - PD EL03 AVERAGE ELECTRIC 100 1.00 .00 0 - PD EX03 ALUMINUM SIDING 100 1.00 .00 0 - PD FL04 HARDWOOD 100 1.00 .00 0 - PD FN34 CONTINUOUS WALL BRIC100 1.00 .00 0 - PD IF05 INT FINISH WALLBOARD100 1.00 .00 0 - PD PL02 PLUMBING POOR 100 1.00 .00 0 - PD RF01 GABLE ROOF 100 1.00 .00 0 - PD RM01 RF MATERIAL ASPHALT 100 1.00 .00 0 --------------- RCN... PCT COMPLETE 100 x 72,324 RCN... COUNTY RCN ADJ 100.00 x 72,324 QUAL.. QG E+ CONSTRUCTION GRADE E 85.00 x 61,475 DEPR.. CGW GOOD WOOD FRAME 33.00 - 20,286 20,286 T --FMV... 41,189
11/17/21, 1:34 PM Rockingham County NC Property Card
https://www.webgis.net/nc/rockingham/PropertyCard.php?pid=129841 2/4
DATE 10/02/21 ROCKINGHAM COUNTY PAGE 2 TIME 10:58:20 PROPERTY CARD PROG# AS2006 USER RKMARKMC FOR YEAR 2021 FLYING GRASS INC PARCEL ID.. 129841 PIN... 7953 00 77 8778 00 ---------------------------------- IMPROVEMENT # 1 MAJOR IMPR-M ------------------------------------------------- +--------29---------+ : : : : : : : : : : 3 3 2 2 : : : : : : : : : +------+A-29-+------+ 5 5 +--9--+ ------------- AC OPG OPEN PORCH GRADE --------- TRAVERSE ------------------------------ M R 10.00 D R 9.00 D D 5.00 D L 9.00 D U 5.00 ------------- MA C02 GENERAL RETAIL FRAME FLOOR: 1.00 --------- TRAVERSE ------------------------------ D U 32.00 D R 29.00 D D 32.00 D L 29.00 ---------------------------------- IMPROVEMENT # 2 MISC IMPR-X ------------------------------------------------- MAIN FIN AREA.. ACT/EFF YR/AGE.. 1960 1960 59 VISITED.. BY STRAT.......... 100 DESCRIPT.... ASP PAVING MAINTAINED.. 7/09/2020 BY RKDIWILSON BUILT USE...... 57 ASP PAVING CURRENT USE.... CC CURRENT USE COMMERICAL LOCATION #..... 5040 NC 65 #BED: #BTH: #HBTH: COMPONENT TYPE/CODE/DESC PCT UNITS RATE STR# STR% SIZ% HGT% PER% CDS% COST %CMPL ----------------------------------------------------------------------------------------------------------------------- MS PA1 ASPHALT PAVING 2"/AV 100 4320.00 2.00 1.00 8,640 --------------- RCN... PCT COMPLETE 100 x 8,640 QUAL.. QG 000 000 100.00 x 8,640 DEPR.. 10P 10 YR LIFE POOR 90.00 - 7,776 7,776 T --FMV... 864 ---------------------------------- IMPROVEMENT # 4 MISC IMPR-X ------------------------------------------------- MAIN FIN AREA.. ACT/EFF YR/AGE.. 1947 1987 32 VISITED.. BY STRAT.......... 100 DESCRIPT.... STORAGE BLDG MAINTAINED.. 7/09/2020 BY RKDIWILSON BUILT USE...... 10 STORAGE BLDG CURRENT USE.... CC CURRENT USE COMMERICAL LOCATION #..... NC 65 #BED: #BTH: #HBTH: COMPONENT TYPE/CODE/DESC PCT UNITS RATE STR# STR% SIZ% HGT% PER% CDS% COST %CMPL ----------------------------------------------------------------------------------------------------------------------- MS UT2 UT BLDG AVG COST FRA 100 80.00 20.00 1.00 1,600 --------------- RCN... PCT COMPLETE 100 x 1,600 QUAL.. QG 000 000 100.00 x 1,600 DEPR.. 25A 25 YR LIFE AVERAGE 85.00 - 1,360 1,360 T --FMV... 240 ---------------------------------- IMPROVEMENT # 6 MAJOR IMPR-M ------------------------------------------------- MAIN FIN AREA.. 1,886.00 ACT/EFF YR/AGE.. 1947 1987 32 VISITED.. 2/04/2020 BY GW STRAT.......... 100 DESCRIPT.... SINGLE FAMILY DWELLING MAINTAINED.. 7/09/2020 BY RKDIWILSON MAIN GROUND SF.... 1,271.000 BUILT USE...... 01 SINGLE FAMILY DWELLING CURRENT USE.... CR CURRENT USE RESIDENTIAL LOCATION #..... 5040 NC 65 #BED: #BTH: #HBTH: COMPONENT TYPE/CODE/DESC PCT UNITS RATE STR# STR% SIZ% HGT% PER% CDS% COST %CMPL -----------------------------------------------------------------------------------------------------------------------
11/17/21, 1:34 PM Rockingham County NC Property Card
https://www.webgis.net/nc/rockingham/PropertyCard.php?pid=129841 3/4
DATE 10/02/21 ROCKINGHAM COUNTY PAGE 3 TIME 10:58:20 PROPERTY CARD PROG# AS2006 USER RKMARKMC FOR YEAR 2021 FLYING GRASS INC PARCEL ID.. 129841 PIN... 7953 00 77 8778 00 ---------------------------------- IMPROVEMENT # 6 MAJOR IMPR-M ------------------------------------------------- COMPONENT TYPE/CODE/DESC PCT UNITS RATE STR# STR% SIZ% HGT% PER% CDS% COST %CMPL ----------------------------------------------------------------------------------------------------------------------- AC EPF ENCLOSED PORCH FINIS 100 112.00 38.40 4,300 AC OPR OPEN PORCH RAISED 100 40.00 12.80 512 AC PT PATIO 100 248.00 6.40 1,587 AC ST STOOP 100 81.00 6.40 518 AC 1.5 1.5 STORY RES 100 615.00 48.00 1.00 29,520 MA R01 SFR MAIN AREA FRAME 100 1271.00 64.50 1.00 100.00 81,979 EW 03 ALUMINUM SIDING 100 144.00 .00 0 - AR 004 FORCED HOT AIR & CEN100 1271.00 5.50 6,990 - AS 004S FORCED HOT AIR & CEN100 615.00 5.50 3,382 - PD EL03 AVERAGE ELECTRIC 100 1.00 .00 0 - PD EX03 ALUMINUM SIDING 100 1.00 .00 0 - PD FL99 MULTIPLE FLOOR TYPES100 1.00 .00 0 - PD FN35 CONTINUOUS WALL BLOC100 1.00 .00 0 - PD IF01 INT FINISH DRYWALL 100 1.00 .00 0 - PD PL03 PLUMBING AVERAGE 100 1.00 .00 0 - PD RF01 GABLE ROOF 100 1.00 .00 0 - PD RM01 RF MATERIAL ASPHALT 100 1.00 .00 0 - PL 002 3 FIXTURE BATH 100 1.00 2830.00 2,830 --------------- RCN... PCT COMPLETE 100 x 131,618 RCN... COUNTY RCN ADJ 100.00 x 131,619 QUAL.. QG D- CONSTRUCTION GRADE D 95.00 x 125,038 DEPR.. RVG VERY GOOD CONDITION 10.00 - 12,503 12,503 T --FMV... 112,535
11/17/21, 1:34 PM Rockingham County NC Property Card
https://www.webgis.net/nc/rockingham/PropertyCard.php?pid=129841 4/4
DATE 10/02/21 ROCKINGHAM COUNTY PAGE 4 TIME 10:58:20 PROPERTY CARD PROG# AS2006 USER RKMARKMC FOR YEAR 2021 FLYING GRASS INC PARCEL ID.. 129841 PIN... 7953 00 77 8778 00 ---------------------------------- IMPROVEMENT # 6 MAJOR IMPR-M ------------------------------------------------- +-10-+ +6+ 1 6 +-6+-9-+ 65-+ 9 9 9 F : H : +--+-----41--+---+-+ : : : : 3 3 1 18-+ : : 1 : : 4 A B : +------+-41+-------+-8+ G 5 5-8-+ ------------- AC EPF ENCLOSED PORCH FINIS --------- TRAVERSE ------------------------------ M R 41.00 M U 1.00 D U 14.00 D R 8.00 D D 14.00 D L 8.00 ------------- AC OPR OPEN PORCH RAISED --------- TRAVERSE ------------------------------ M R 16.00 D D 5.00 D R 8.00 D U 5.00 D L 8.00 ------------- AC PT PATIO --------- TRAVERSE ------------------------------ M U 31.00 M R 8.00 D U 6.00 D R 5.00 D U 6.00 D R 6.00 D U 8.00 D R 10.00 D D 11.00 D L 6.00 D D 9.00 D L 15.00 ------------- AC ST STOOP --------- TRAVERSE ------------------------------ M U 31.00 M R 29.00 D U 9.00 D R 9.00 D D 9.00 D L 9.00 ------------- MA R01 SFR MAIN AREA FRAME FLOOR: 1.00 --------- TRAVERSE ------------------------------ D U 31.00 D R 41.00 D D 31.00 D L 41.00 ---------------------------------- IMPROVEMENT # 7 MISC IMPR-X ------------------------------------------------- MAIN FIN AREA.. ACT/EFF YR/AGE.. 2019 2019 VISITED.. 2/04/2020 BY GW STRAT.......... 100 DESCRIPT.... SHED OPEN SIDES MAINTAINED.. 7/09/2020 BY RKDIWILSON BUILT USE...... 20 SHED OPEN SIDES CURRENT USE.... CC CURRENT USE COMMERICAL LOCATION #..... 5040 NC 65 #BED: #BTH: #HBTH: COMPONENT TYPE/CODE/DESC PCT UNITS RATE STR# STR% SIZ% HGT% PER% CDS% COST %CMPL ----------------------------------------------------------------------------------------------------------------------- MS B24GW SHED/4 SIDES OPEN GO 100 1440.00 7.25 98.00 10,231 --------------- RCN... PCT COMPLETE 100 x 10,231 QUAL.. QG 000 000 100.00 x 10,231 DEPR.. 25A 25 YR LIFE AVERAGE 20.00 - 2,046 2,046 T --FMV... 8,185 TOTAL PARCEL VALUES---- LAND / OVR IMPROVEMENTS / OVR TOTAL LAND/IMPROVE 2020 VALUE FMV...... 14,100 163,013 177,113 177,113 APV...... 14,100 163,013 177,113 177,113
12/16/21, 10:09 AM Rockingham County NC Property Card
https://www.webgis.net/nc/rockingham/PropertyCard.php?pid=129840 1/2
DATE 11/17/21 ROCKINGHAM COUNTY PAGE 1 TIME 8:54:22 PROPERTY CARD PROG# AS2006 USER RKTHURST FOR YEAR 2021 ELLINGTON IVIE ANN WASHBURN PARCEL ID.. 129840 PIN... 7953 00 75 7534 00 LOCATION... 5091 NC 65 DEED YEAR/BOOK/PAGE.. 2019 1524 1099 ASSESSMENT NONE .00 .00 .00 287 LOVINGS RD PLAT BOOK/PAGE.. OWNER ID.. 1269218 LEGAL DESC:92.50 AC WAYNE ELLINGTON DISTRICT.. 113 BETHANY FD SURVEY Area/Fire: 913 NEW BETHEL (BETHANY) TOWNSHIP... 5 NEW BETHEL REIDSVILLE NC 27320-8573 ELLINGTON WAYNE SURVEY NBRHOOD... R104 BETHANY DESCRIPTION AG/VAC/W/BUILDINGS NH CLASS.. DESCRIPTION LAND USE AGRICULTURE RESIDENTIAL RES AG COUNTY MAINTAINED.. 7/09/2020 BY RKDIWILSON VALUED.. 1/16/2019 BY DIWILSON VISITED..... 3/23/2018 BY GW TYPE OF REVIEW ROUTING#.. 300 PARCEL STATUS... ACTIVE CATEGORY.. REAL & PERSONAL . DISCLAIMER-OWNERSHIP, ZONING AND OTHER INFORMATION SHOULD BE VERIFIED. INFORMATION AND VALUE SUBJECT TO CHANGE. . -------------------------------------------- SALES HISTORY ---------------------------------------------------- DEED BK/PAGE SALE DATE SALES INSTRUMENT DISQUALIFIED SALE AMOUNT STAMP AMOUNT DEED NAME 1524 1099 8/24/2019 ESTATE RELATED BUS OR ELLINGTON IVIE ANN WASHBURN 1524 1099 5/09/2017 DEED QUALIFIED 350,000 ELLINGTON EDGAR WAYNE & ELLING 1328 0357 8/06/2007 DEED RELATED BUS OR WILSON ROGER M & RAMONA P 0001 0001 7/01/1986 DEED CONVERTED WILSON DOROTHY M -------------------------------------------- LAND SEGMENTS ---------------------------------------------------- LND STRAT LAND TOT CURRENT # ZONE CODE TYPE/CODE LAND QTY LAND RATE DPT% SHP% LOC% SIZ% OTH% TOP% ADJ FMV 2 RA 100 AC AA 11.910 6,100.00 .00 .00 .00 86.00 100.00 75.00 64.50 46,859 LUV.. LU A3 11.910 645.00 LU ADJ & VALUE.. .00 7,681 3 RA 100 AC AA 31.330 6,100.00 .00 .00 .00 86.00 100.00 75.00 64.50 123,267 OTHER ADJ... 100.00 .00 .00 .00 LUV.. LU A4 31.330 420.00 LU ADJ & VALUE.. .00 13,158 4 RA 100 AC AA 43.630 6,100.00 .00 .00 .00 86.00 100.00 75.00 64.50 171,662 OTHER ADJ... 100.00 .00 .00 .00 LUV.. LU F2 43.630 255.00 LU ADJ & VALUE.. .00 11,125 5 RA 100 AC AW 4.630 700.00 .00 .00 .00 .00 .00 .00 .00 3,241 LUV.. LU F2 4.630 255.00 LU ADJ & VALUE.. .00 1,180 6 RA 100 AC AA 1.000 6,100.00 .00 .00 .00 86.00 100.00 75.00 64.50 3,934 OTHER ADJ... 100.00 .00 .00 .00 TOTAL ACRES.. 92.500 TOTAL LAND FMV.. 348,963 TOTAL IN LU.. 91.500 TOTAL LAND LUV.. 37,078 ---------------------------------- IMPROVEMENT # 5 MISC IMPR-X ------------------------------------------------- MAIN FIN AREA.. ACT/EFF YR/AGE.. 1930 1930 89 VISITED.. 3/23/2018 BY GW STRAT.......... 100 DESCRIPT.... STORAGE BLDG MAINTAINED.. 7/09/2020 BY RKDIWILSON BUILT USE...... 10 STORAGE BLDG CURRENT USE.... CA CURRENT USE AGRICULTURAL LOCATION #..... 5091 NC 65 #BED: #BTH: #HBTH: COMPONENT TYPE/CODE/DESC PCT UNITS RATE STR# STR% SIZ% HGT% PER% CDS% COST %CMPL ----------------------------------------------------------------------------------------------------------------------- MS B44 AG STORAGE BLDG FRAM 100 192.00 10.25 104.00 2,046 MS UT2 UT BLDG AVG COST FRA 100 240.00 20.00 1.00 104.00 4,992 --------------- RCN... PCT COMPLETE 100 x 7,038 QUAL.. QG 000 000 100.00 x 7,038 DEPR.. 25A 25 YR LIFE AVERAGE 85.00 - 5,982 5,982 T --FMV... 1,056 ---------------------------------- IMPROVEMENT # 7 MISC IMPR-X ------------------------------------------------- MAIN FIN AREA.. ACT/EFF YR/AGE.. 1950 1950 69 VISITED.. 3/23/2018 BY GW STRAT.......... 100 DESCRIPT.... GARAGE MAINTAINED.. 7/09/2020 BY RKDIWILSON BUILT USE...... 09 GARAGE CURRENT USE.... CR CURRENT USE RESIDENTIAL LOCATION #..... 5091 NC 65 #BED: #BTH: #HBTH: COMPONENT TYPE/CODE/DESC PCT UNITS RATE STR# STR% SIZ% HGT% PER% CDS% COST %CMPL -----------------------------------------------------------------------------------------------------------------------
12/16/21, 10:09 AM Rockingham County NC Property Card
https://www.webgis.net/nc/rockingham/PropertyCard.php?pid=129840 2/2
DATE 11/17/21 ROCKINGHAM COUNTY PAGE 2 TIME 8:54:22 PROPERTY CARD PROG# AS2006 USER RKTHURST FOR YEAR 2021 ELLINGTON IVIE ANN WASHBURN PARCEL ID.. 129840 PIN... 7953 00 75 7534 00 ---------------------------------- IMPROVEMENT # 7 MISC IMPR-X ------------------------------------------------- COMPONENT TYPE/CODE/DESC PCT UNITS RATE STR# STR% SIZ% HGT% PER% CDS% COST %CMPL ----------------------------------------------------------------------------------------------------------------------- MS G06 FAIR QTY GAR/WOOD/W 100 400.00 22.00 1.00 114.00 10,032 --------------- RCN... PCT COMPLETE 100 x 10,032 QUAL.. QG 000 000 100.00 x 10,032 DEPR.. 50A 50 YR LIFE AVERAGE 80.00 - 8,025 8,025 T --FMV... 2,007 ---------------------------------- IMPROVEMENT # 8 MISC IMPR-X ------------------------------------------------- MAIN FIN AREA.. ACT/EFF YR/AGE.. 2016 2016 3 VISITED.. 3/23/2018 BY GW STRAT.......... 100 DESCRIPT.... STORAGE BLDG MAINTAINED.. 7/09/2020 BY RKDIWILSON BUILT USE...... 10 STORAGE BLDG CURRENT USE.... CR CURRENT USE RESIDENTIAL LOCATION #..... 5091 NC 65 #BED: #BTH: #HBTH: COMPONENT TYPE/CODE/DESC PCT UNITS RATE STR# STR% SIZ% HGT% PER% CDS% COST %CMPL ----------------------------------------------------------------------------------------------------------------------- MS UT3 UT BLDG GD COST FRA 100 280.00 25.00 7,000 --------------- RCN... PCT COMPLETE 100 x 7,000 QUAL.. QG 000 000 100.00 x 7,000 DEPR.. 25A 25 YR LIFE AVERAGE 20.00 - 1,400 1,400 T --FMV... 5,600 TOTAL PARCEL VALUES---- LAND / OVR IMPROVEMENTS / OVR TOTAL LAND/IMPROVE 2020 VALUE FMV...... 348,963 8,663 357,626 357,626 APV...... 37,078 8,663 45,741 45,741 DEFERRED. 311,885 0 311,885 311,885

APPENDIX E
Laboratory Report – Ground Water Samples

12/23/21
Technical Report for
GRI (Geological Resources Inc.)
Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
5784
SGS Job Number: FA91156
Sampling Date: 11/24/21
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: William Regenthal
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, IL, UT, VT, WA, WI, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc.  4405 Vineland Road  Suite C-15  Orlando, FL 32811  tel: [phone]  fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Orlando, FL 12/23/21
e-Hardcopy 2.0
Automated Report
68
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
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FA91156
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................7
3.1: FA91156-1: MW-1 ........................................................................................................8
3.2: FA91156-2: MW-3 ........................................................................................................11
3.3: FA91156-3: MW-4 ........................................................................................................14
3.4: FA91156-4: MW-5 ........................................................................................................17
3.5: FA91156-5: MW-8 ........................................................................................................20
3.6: FA91156-6: MW-9 ........................................................................................................23
3.7: FA91156-7: TW-1 .........................................................................................................26
3.8: FA91156-8: TW-2 .........................................................................................................29
3.9: FA91156-9: TB .............................................................................................................32
Section 4: Misc. Forms ............................................................................................................35
4.1: Chain of Custody ...........................................................................................................36
Section 5: MS Volatiles - QC Data Summaries .....................................................................38
5.1: Method Blank Summary ................................................................................................39
5.2: Blank Spike Summary ...................................................................................................49
5.3: Matrix Spike Summary ..................................................................................................59
5.4: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................62
1
2
3
4
5
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Sample Summary
GRI (Geological Resources Inc.)
Job No:FA91156
Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Project No: 5784
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FA91156-1 11/24/21 12:14 KP 11/30/21 AQ Ground Water MW-1
FA91156-2 11/24/21 12:25 KP 11/30/21 AQ Ground Water MW-3
FA91156-3 11/24/21 12:33 KP 11/30/21 AQ Ground Water MW-4
FA91156-4 11/24/21 12:41 KP 11/30/21 AQ Ground Water MW-5
FA91156-5 11/24/21 12:05 KP 11/30/21 AQ Ground Water MW-8
FA91156-6 11/24/21 11:56 KP 11/30/21 AQ Ground Water MW-9
FA91156-7 11/24/21 13:36 KP 11/30/21 AQ Ground Water TW-1
FA91156-8 11/24/21 13:16 KP 11/30/21 AQ Ground Water TW-2
FA91156-9 11/24/21 11:00 KP 11/30/21 AQ Trip Blank Water TB
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1
Summary of Hits Page 1 of 3
Job Number:FA91156
Account:GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Collected:11/24/21
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA91156-1 MW-1
No hits reported in this sample.
FA91156-2 MW-3
Benzene a 1860 250 63 ug/l SM 6200B
1,2-Dibromoethane a 190 J 250 63 ug/l SM 6200B
Ethylbenzene a 1870 250 63 ug/l SM 6200B
Methylene Chloride b 751 J 1000 500 ug/l SM 6200B
Naphthalene a 378 250 63 ug/l SM 6200B
n-Propylbenzene a 121 J 250 63 ug/l SM 6200B
Toluene a 10200 250 63 ug/l SM 6200B
1,2,4-Trimethylbenzene a 787 250 63 ug/l SM 6200B
1,3,5-Trimethylbenzene a 434 250 63 ug/l SM 6200B
m,p-Xylene a 5770 500 63 ug/l SM 6200B
o-Xylene a 3250 250 63 ug/l SM 6200B
FA91156-3 MW-4
Benzene a 0.24 J 0.50 0.13 ug/l SM 6200B
FA91156-4 MW-5
Benzene a 111 5.0 1.3 ug/l SM 6200B
n-Butylbenzene a 3.2 J 5.0 1.3 ug/l SM 6200B
sec-Butylbenzene a 3.3 J 5.0 1.3 ug/l SM 6200B
1,2-Dichloroethane a 6.7 5.0 1.3 ug/l SM 6200B
Ethylbenzene a 143 5.0 1.3 ug/l SM 6200B
Isopropylbenzene a 16.9 5.0 1.3 ug/l SM 6200B
Methyl Tert Butyl Ether a 3.2 J 5.0 1.3 ug/l SM 6200B
Naphthalene a 193 5.0 1.3 ug/l SM 6200B
n-Propylbenzene a 32.9 5.0 1.3 ug/l SM 6200B
Tert-Amyl Alcohol a 448 100 20 ug/l SM 6200B
Tert-Butyl Alcohol c 33.6 J 100 20 ug/l SM 6200B
Toluene a 3.8 J 5.0 1.3 ug/l SM 6200B
1,2,4-Trimethylbenzene a 150 5.0 1.3 ug/l SM 6200B
1,3,5-Trimethylbenzene a 70.2 5.0 1.3 ug/l SM 6200B
m,p-Xylene a 281 10 1.3 ug/l SM 6200B
o-Xylene a 317 5.0 1.3 ug/l SM 6200B
FA91156-5 MW-8
Benzene 13.0 0.50 0.13 ug/l SM 6200B
n-Butylbenzene 2.1 0.50 0.13 ug/l SM 6200B
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Summary of Hits Page 2 of 3
Job Number:FA91156
Account:GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Collected:11/24/21
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
sec-Butylbenzene 2.0 0.50 0.13 ug/l SM 6200B
Chloroethane d 0.24 J 0.50 0.20 ug/l SM 6200B
1,2-Dichloroethane 3.7 0.50 0.13 ug/l SM 6200B
Ethylbenzene 8.7 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 8.4 0.50 0.13 ug/l SM 6200B
p-Isopropyltoluene 0.97 0.50 0.13 ug/l SM 6200B
Methylene Chloride e 2.8 J 4.0 2.0 ug/l SM 6200B
Naphthalene f 83.8 1.0 0.25 ug/l SM 6200B
n-Propylbenzene 6.5 0.50 0.13 ug/l SM 6200B
Tert-Amyl Alcohol 17.2 10 2.0 ug/l SM 6200B
Tert-Butyl Alcohol g 51.1 10 2.0 ug/l SM 6200B
Toluene 0.96 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 10 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 1.4 0.50 0.13 ug/l SM 6200B
m,p-Xylene 9.0 1.0 0.13 ug/l SM 6200B
o-Xylene 1.7 0.50 0.13 ug/l SM 6200B
FA91156-6 MW-9
Ethyl Alcohol h 112 100 65 ug/l SM 6200B
Ethylbenzene 0.20 J 0.50 0.13 ug/l SM 6200B
Naphthalene i 2.0 0.50 0.13 ug/l SM 6200B
Toluene 0.29 J 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.16 J 0.50 0.13 ug/l SM 6200B
m,p-Xylene 0.58 J 1.0 0.13 ug/l SM 6200B
FA91156-7 TW-1
Benzene j 4.2 1.0 0.25 ug/l SM 6200B
n-Butylbenzene j 0.43 J 1.0 0.25 ug/l SM 6200B
sec-Butylbenzene j 1.5 1.0 0.25 ug/l SM 6200B
1,1-Dichloroethane j 1.2 1.0 0.25 ug/l SM 6200B
1,2-Dichloroethane f 828 10 2.5 ug/l SM 6200B
1,2-Dichloropropane j 31.4 1.0 0.25 ug/l SM 6200B
Di-Isopropyl Ether j 21.6 1.0 0.25 ug/l SM 6200B
Ethylbenzene j 0.61 J 1.0 0.25 ug/l SM 6200B
Isopropylbenzene j 2.8 1.0 0.25 ug/l SM 6200B
Methyl Tert Butyl Ether j 46.2 1.0 0.25 ug/l SM 6200B
Naphthalene j 1.1 1.0 0.25 ug/l SM 6200B
Tert-Amyl Alcohol k 25600 E 200 40 ug/l SM 6200B
Tert-Butyl Alcohol l 898 20 4.0 ug/l SM 6200B
Toluene j 0.36 J 1.0 0.25 ug/l SM 6200B
1,1,2-Trichloroethane j 1.5 1.0 0.25 ug/l SM 6200B
1,2,4-Trimethylbenzene j 0.48 J 1.0 0.25 ug/l SM 6200B
m,p-Xylene j 0.52 J 2.0 0.25 ug/l SM 6200B
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Summary of Hits Page 3 of 3
Job Number:FA91156
Account:GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Collected:11/24/21
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA91156-8 TW-2
Benzene 0.13 J 0.50 0.13 ug/l SM 6200B
Naphthalene i 0.25 J 0.50 0.13 ug/l SM 6200B
Tert-Butyl Alcohol g 2.0 J 10 2.0 ug/l SM 6200B
Toluene 4.5 0.50 0.13 ug/l SM 6200B
FA91156-9 TB
Methylene Chloride e 1.4 J 2.0 1.0 ug/l SM 6200B
(a) Associated internal standard response outside control limits. Confirmed by reanalysis.
(b) Associated internal standard response outside control limits. Confirmed by reanalysis. Associated BS recovery
outside control limits low. Suspected laboratory contaminant.
(c) Associated internal standard response outside control limits. Confirmed by reanalysis. Associated BS recovery
outside control limits high.
(d) Associated CCV outside of control limits high.
(e) Sample analyzed beyond hold time; reported results are considered minimum values. Suspected laboratory
contaminant.
(f) Sample analyzed beyond hold time; reported results are considered minimum values.
(g) Associated CCV outside control limits low.
(h) Associated Initial Calibration invalid.
(i) Suspected carry-over.
(j) Associated internal standard response outside control limits.
(k) Sample analyzed beyond hold time; reported results are considered minimum values. Outside control limits, no
sample available for reanalysis.
(l) Associated internal standard response outside control limits. Associated CCV outside control limits low.
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Sample Results
Report of Analysis
Orlando, FL
Section 3
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SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-1
Lab Sample ID:FA91156-1 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a E109779.D 1 12/07/21 16:07 JL n/a n/a VE2597
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-1
Lab Sample ID:FA91156-1 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol b ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride c ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol d ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane d ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 110%70-130%
17060-07-0 1,2-Dichloroethane-D4 118%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-1
Lab Sample ID:FA91156-1 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 93%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
(a) Internal standard response outside control limits; associated analytes ND.
(b) Associated Initial Calibration outside control limits (%RSD > 15%).
(c) Associated BS recovery outside control limits low.
(d) Associated BS recovery outside control limits high; however sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:MW-3
Lab Sample ID:FA91156-2 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a E109795.D 500 12/07/21 22:15 JL n/a n/a VE2597
Run #2 b E110000.D 250 12/17/21 20:28 JL n/a n/a VE2605
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1860 250 63 ug/l
108-86-1 Bromobenzene ND 250 63 ug/l
74-97-5 Bromochloromethane ND 250 63 ug/l
75-27-4 Bromodichloromethane ND 250 63 ug/l
75-25-2 Bromoform ND 250 63 ug/l
104-51-8 n-Butylbenzene ND 250 63 ug/l
135-98-8 sec-Butylbenzene ND 250 63 ug/l
98-06-6 tert-Butylbenzene ND 250 63 ug/l
56-23-5 Carbon Tetrachloride ND 250 63 ug/l
108-90-7 Chlorobenzene ND 250 63 ug/l
75-00-3 Chloroethane ND 250 100 ug/l
67-66-3 Chloroform ND 250 63 ug/l
95-49-8 o-Chlorotoluene ND 250 63 ug/l
106-43-4 p-Chlorotoluene ND 250 63 ug/l
124-48-1 Dibromochloromethane ND 250 63 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 250 120 ug/l
106-93-4 1,2-Dibromoethane 190 250 63 ug/l J
75-71-8 Dichlorodifluoromethane ND 250 100 ug/l
95-50-1 1,2-Dichlorobenzene ND 250 63 ug/l
541-73-1 1,3-Dichlorobenzene ND 250 63 ug/l
106-46-7 1,4-Dichlorobenzene ND 250 63 ug/l
75-34-3 1,1-Dichloroethane ND 250 63 ug/l
107-06-2 1,2-Dichloroethane ND 250 63 ug/l
75-35-4 1,1-Dichloroethylene ND 250 63 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 250 63 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 250 63 ug/l
78-87-5 1,2-Dichloropropane ND 250 63 ug/l
142-28-9 1,3-Dichloropropane ND 250 63 ug/l
594-20-7 2,2-Dichloropropane ND 250 63 ug/l
563-58-6 1,1-Dichloropropene ND 250 63 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 250 63 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 250 63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-3
Lab Sample ID:FA91156-2 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 250 63 ug/l
64-17-5 Ethyl Alcohol c ND 50000 33000 ug/l
100-41-4 Ethylbenzene 1870 250 63 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 250 63 ug/l
87-68-3 Hexachlorobutadiene ND 250 63 ug/l
98-82-8 Isopropylbenzene ND 250 63 ug/l
99-87-6 p-Isopropyltoluene ND 250 63 ug/l
74-83-9 Methyl Bromide ND 250 100 ug/l
74-87-3 Methyl Chloride ND 250 100 ug/l
74-95-3 Methylene Bromide ND 250 63 ug/l
75-09-2 Methylene Chloride d 751 1000 500 ug/l J
1634-04-4 Methyl Tert Butyl Ether ND 250 63 ug/l
91-20-3 Naphthalene 378 250 63 ug/l
103-65-1 n-Propylbenzene 121 250 63 ug/l J
100-42-5 Styrene ND 250 63 ug/l
75-85-4 Tert-Amyl Alcohol ND 5000 1000 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 500 100 ug/l
75-65-0 Tert-Butyl Alcohol e ND 5000 1000 ug/l
762-75-4 Tert-Butyl Formate ND 5000 1000 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 250 63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 250 63 ug/l
127-18-4 Tetrachloroethylene ND 250 63 ug/l
108-88-3 Toluene 10200 250 63 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 250 63 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 250 63 ug/l
71-55-6 1,1,1-Trichloroethane ND 250 63 ug/l
79-00-5 1,1,2-Trichloroethane ND 250 63 ug/l
79-01-6 Trichloroethylene ND 250 63 ug/l
75-69-4 Trichlorofluoromethane e ND 250 100 ug/l
96-18-4 1,2,3-Trichloropropane ND 250 63 ug/l
95-63-6 1,2,4-Trimethylbenzene 787 250 63 ug/l
108-67-8 1,3,5-Trimethylbenzene 434 250 63 ug/l
75-01-4 Vinyl Chloride ND 250 63 ug/l
m,p-Xylene 5770 500 63 ug/l
95-47-6 o-Xylene 3250 250 63 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 111%115%70-130%
17060-07-0 1,2-Dichloroethane-D4 115%113%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-3
Lab Sample ID:FA91156-2 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 95%93%70-130%
460-00-4 4-Bromofluorobenzene 99%101%70-130%
(a) Associated internal standard response outside control limits. Confirmed by reanalysis.
(b) Confirmation run beyond holdtime.
(c) Associated Initial Calibration outside control limits (%RSD > 15%).
(d) Associated BS recovery outside control limits low. Suspected laboratory contaminant.
(e) Associated BS recovery outside control limits high; however sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-4
Lab Sample ID:FA91156-3 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a E109780.D 1 12/07/21 16:30 JL n/a n/a VE2597
Run #2 b E109988.D 1 12/17/21 15:52 JL n/a n/a VE2605
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.24 0.50 0.13 ug/l J
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-4
Lab Sample ID:FA91156-3 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol c ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride d ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol e ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane e ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 115%116%70-130%
17060-07-0 1,2-Dichloroethane-D4 125%118%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-4
Lab Sample ID:FA91156-3 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 90%97%70-130%
460-00-4 4-Bromofluorobenzene 99%103%70-130%
(a) Associated internal standard response outside control limits. Confirmed by reanalysis.
(b) Confirmation run beyond holdtime.
(c) Associated Initial Calibration outside control limits (%RSD > 15%).
(d) Associated BS recovery outside control limits low.
(e) Associated BS recovery outside control limits high; however sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-5
Lab Sample ID:FA91156-4 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a E109796.D 10 12/07/21 22:38 JL n/a n/a VE2597
Run #2 b E110001.D 10 12/17/21 20:51 JL n/a n/a VE2605
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 111 5.0 1.3 ug/l
108-86-1 Bromobenzene ND 5.0 1.3 ug/l
74-97-5 Bromochloromethane ND 5.0 1.3 ug/l
75-27-4 Bromodichloromethane ND 5.0 1.3 ug/l
75-25-2 Bromoform ND 5.0 1.3 ug/l
104-51-8 n-Butylbenzene 3.2 5.0 1.3 ug/l J
135-98-8 sec-Butylbenzene 3.3 5.0 1.3 ug/l J
98-06-6 tert-Butylbenzene ND 5.0 1.3 ug/l
56-23-5 Carbon Tetrachloride ND 5.0 1.3 ug/l
108-90-7 Chlorobenzene ND 5.0 1.3 ug/l
75-00-3 Chloroethane ND 5.0 2.0 ug/l
67-66-3 Chloroform ND 5.0 1.3 ug/l
95-49-8 o-Chlorotoluene ND 5.0 1.3 ug/l
106-43-4 p-Chlorotoluene ND 5.0 1.3 ug/l
124-48-1 Dibromochloromethane ND 5.0 1.3 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 2.5 ug/l
106-93-4 1,2-Dibromoethane ND 5.0 1.3 ug/l
75-71-8 Dichlorodifluoromethane ND 5.0 2.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 5.0 1.3 ug/l
541-73-1 1,3-Dichlorobenzene ND 5.0 1.3 ug/l
106-46-7 1,4-Dichlorobenzene ND 5.0 1.3 ug/l
75-34-3 1,1-Dichloroethane ND 5.0 1.3 ug/l
107-06-2 1,2-Dichloroethane 6.7 5.0 1.3 ug/l
75-35-4 1,1-Dichloroethylene ND 5.0 1.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.3 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.3 ug/l
78-87-5 1,2-Dichloropropane ND 5.0 1.3 ug/l
142-28-9 1,3-Dichloropropane ND 5.0 1.3 ug/l
594-20-7 2,2-Dichloropropane ND 5.0 1.3 ug/l
563-58-6 1,1-Dichloropropene ND 5.0 1.3 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-5
Lab Sample ID:FA91156-4 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 5.0 1.3 ug/l
64-17-5 Ethyl Alcohol c ND 1000 650 ug/l
100-41-4 Ethylbenzene 143 5.0 1.3 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 5.0 1.3 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 1.3 ug/l
98-82-8 Isopropylbenzene 16.9 5.0 1.3 ug/l
99-87-6 p-Isopropyltoluene ND 5.0 1.3 ug/l
74-83-9 Methyl Bromide ND 5.0 2.0 ug/l
74-87-3 Methyl Chloride ND 5.0 2.0 ug/l
74-95-3 Methylene Bromide ND 5.0 1.3 ug/l
75-09-2 Methylene Chloride d ND 20 10 ug/l
1634-04-4 Methyl Tert Butyl Ether 3.2 5.0 1.3 ug/l J
91-20-3 Naphthalene 193 5.0 1.3 ug/l
103-65-1 n-Propylbenzene 32.9 5.0 1.3 ug/l
100-42-5 Styrene ND 5.0 1.3 ug/l
75-85-4 Tert-Amyl Alcohol 448 100 20 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 10 2.0 ug/l
75-65-0 Tert-Butyl Alcohol e 33.6 100 20 ug/l J
762-75-4 Tert-Butyl Formate ND 100 20 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.3 ug/l
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/l
108-88-3 Toluene 3.8 5.0 1.3 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.3 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 5.0 1.3 ug/l
79-00-5 1,1,2-Trichloroethane ND 5.0 1.3 ug/l
79-01-6 Trichloroethylene ND 5.0 1.3 ug/l
75-69-4 Trichlorofluoromethane f ND 5.0 2.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/l
95-63-6 1,2,4-Trimethylbenzene 150 5.0 1.3 ug/l
108-67-8 1,3,5-Trimethylbenzene 70.2 5.0 1.3 ug/l
75-01-4 Vinyl Chloride ND 5.0 1.3 ug/l
m,p-Xylene 281 10 1.3 ug/l
95-47-6 o-Xylene 317 5.0 1.3 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 110%118%70-130%
17060-07-0 1,2-Dichloroethane-D4 116%116%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-5
Lab Sample ID:FA91156-4 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 94%95%70-130%
460-00-4 4-Bromofluorobenzene 99%99%70-130%
(a) Associated internal standard response outside control limits. Confirmed by reanalysis.
(b) Confirmation run beyond holdtime.
(c) Associated Initial Calibration outside control limits (%RSD > 15%).
(d) Associated BS recovery outside control limits low.
(e) Associated BS recovery outside control limits high.
(f) Associated BS recovery outside control limits high; however sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-8
Lab Sample ID:FA91156-5 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E109806.D 1 12/08/21 15:27 JL n/a n/a VE2598
Run #2 a E110023.D 2 12/18/21 16:15 JL n/a n/a VE2606
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 13.0 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform b ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 2.1 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene 2.0 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane c 0.24 0.50 0.20 ug/l J
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane 3.7 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-8
Lab Sample ID:FA91156-5 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol d ND 100 65 ug/l
100-41-4 Ethylbenzene 8.7 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 8.4 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene 0.97 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride e 2.8 f 4.0 2.0 ug/l J
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene 83.8 f 1.0 0.25 ug/l
103-65-1 n-Propylbenzene 6.5 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol 17.2 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol g 51.1 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 0.96 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 10 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 1.4 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 9.0 1.0 0.13 ug/l
95-47-6 o-Xylene 1.7 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 108%120%70-130%
17060-07-0 1,2-Dichloroethane-D4 118%123%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-8
Lab Sample ID:FA91156-5 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 91%90%70-130%
460-00-4 4-Bromofluorobenzene 96%97%70-130%
(a) Sample analyzed beyond hold time; reported results are considered minimum values.
(b) Associated BS recovery outside control limits high; however sample is ND.
(c) Associated CCV outside of control limits high.
(d) Associated Initial Calibration invalid.
(e) Suspected laboratory contaminant.
(f) Result is from Run# 2
(g) Associated CCV outside control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-9
Lab Sample ID:FA91156-6 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E109807.D 1 12/08/21 15:50 JL n/a n/a VE2598
Run #2 a E110016.D 1 12/18/21 13:31 JL n/a n/a VE2606
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform b ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane c ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-9
Lab Sample ID:FA91156-6 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol d 112 100 65 ug/l
100-41-4 Ethylbenzene 0.20 0.50 0.13 ug/l J
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride e ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene f 2.0 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol g ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 0.29 0.50 0.13 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.16 0.50 0.13 ug/l J
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 0.58 1.0 0.13 ug/l J
95-47-6 o-Xylene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%115%70-130%
17060-07-0 1,2-Dichloroethane-D4 111%116%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-9
Lab Sample ID:FA91156-6 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 89%89%70-130%
460-00-4 4-Bromofluorobenzene 96%98%70-130%
(a) Confirmation run beyond holdtime.
(b) Associated BS recovery outside control limits high; however sample is ND.
(c) Associated CCV outside of control limits high, sample was ND.
(d) Associated Initial Calibration invalid.
(e) Associated ECC and BS outside control limits low.
(f) Suspected carry-over.
(g) Associated CCV outside control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:TW-1
Lab Sample ID:FA91156-7 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a E109822.D 2 12/08/21 21:37 JL n/a n/a VE2598
Run #2 b E110031.D 20 12/18/21 19:18 JL n/a n/a VE2606
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 4.2 1.0 0.25 ug/l
108-86-1 Bromobenzene ND 1.0 0.25 ug/l
74-97-5 Bromochloromethane ND 1.0 0.25 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.25 ug/l
75-25-2 Bromoform c ND 1.0 0.25 ug/l
104-51-8 n-Butylbenzene 0.43 1.0 0.25 ug/l J
135-98-8 sec-Butylbenzene 1.5 1.0 0.25 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.25 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.25 ug/l
108-90-7 Chlorobenzene ND 1.0 0.25 ug/l
75-00-3 Chloroethane d ND 1.0 0.40 ug/l
67-66-3 Chloroform ND 1.0 0.25 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.25 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.25 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.25 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 1.0 0.49 ug/l
106-93-4 1,2-Dibromoethane ND 1.0 0.25 ug/l
75-71-8 Dichlorodifluoromethane ND 1.0 0.40 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.25 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.25 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.25 ug/l
75-34-3 1,1-Dichloroethane 1.2 1.0 0.25 ug/l
107-06-2 1,2-Dichloroethane 828 e 10 2.5 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.25 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.25 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.25 ug/l
78-87-5 1,2-Dichloropropane 31.4 1.0 0.25 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.25 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.25 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.25 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.25 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.25 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:TW-1
Lab Sample ID:FA91156-7 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 21.6 1.0 0.25 ug/l
64-17-5 Ethyl Alcohol f ND 200 130 ug/l
100-41-4 Ethylbenzene 0.61 1.0 0.25 ug/l J
637-92-3 Ethyl Tert Butyl Ether ND 1.0 0.25 ug/l
87-68-3 Hexachlorobutadiene ND 1.0 0.25 ug/l
98-82-8 Isopropylbenzene 2.8 1.0 0.25 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.25 ug/l
74-83-9 Methyl Bromide ND 1.0 0.40 ug/l
74-87-3 Methyl Chloride ND 1.0 0.40 ug/l
74-95-3 Methylene Bromide ND 1.0 0.25 ug/l
75-09-2 Methylene Chloride g ND 4.0 2.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 46.2 1.0 0.25 ug/l
91-20-3 Naphthalene 1.1 1.0 0.25 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.25 ug/l
100-42-5 Styrene ND 1.0 0.25 ug/l
75-85-4 Tert-Amyl Alcohol h 25600 e 200 40 ug/l E
994-05-8 Tert-Amyl Methyl Ether ND 2.0 0.40 ug/l
75-65-0 Tert-Butyl Alcohol i 898 20 4.0 ug/l
762-75-4 Tert-Butyl Formate ND 20 4.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.25 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.25 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.25 ug/l
108-88-3 Toluene 0.36 1.0 0.25 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 1.0 0.25 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 1.0 0.25 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l
79-00-5 1,1,2-Trichloroethane 1.5 1.0 0.25 ug/l
79-01-6 Trichloroethylene ND 1.0 0.25 ug/l
75-69-4 Trichlorofluoromethane ND 1.0 0.40 ug/l
96-18-4 1,2,3-Trichloropropane ND 1.0 0.25 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.48 1.0 0.25 ug/l J
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.25 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.25 ug/l
m,p-Xylene 0.52 2.0 0.25 ug/l J
95-47-6 o-Xylene ND 1.0 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%106%70-130%
17060-07-0 1,2-Dichloroethane-D4 112%103%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:TW-1
Lab Sample ID:FA91156-7 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 90%98%70-130%
460-00-4 4-Bromofluorobenzene 98%101%70-130%
(a) Associated internal standard response outside control limits.
(b) Sample analyzed beyond hold time; reported results are considered minimum values.
(c) Associated BS recovery outside control limits high; however sample is ND.
(d) Associated CCV outside of control limits high, sample was ND.
(e) Result is from Run# 2
(f) Associated Initial Calibration invalid.
(g) Associated ECC and BS outside control limits low.
(h) Outside control limits, no sample available for reanalysis.
(i) Associated CCV outside control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:TW-2
Lab Sample ID:FA91156-8 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E109808.D 1 12/08/21 16:13 JL n/a n/a VE2598
Run #2 a E110017.D 1 12/18/21 13:54 JL n/a n/a VE2606
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.13 0.50 0.13 ug/l J
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform b ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane c ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:TW-2
Lab Sample ID:FA91156-8 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol d ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride e ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene f 0.25 0.50 0.13 ug/l J
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol g 2.0 10 2.0 ug/l J
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 4.5 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%112%70-130%
17060-07-0 1,2-Dichloroethane-D4 111%113%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:TW-2
Lab Sample ID:FA91156-8 Date Sampled:11/24/21
Matrix:AQ - Ground Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 93%96%70-130%
460-00-4 4-Bromofluorobenzene 96%96%70-130%
(a) Confirmation run beyond holdtime.
(b) Associated BS recovery outside control limits high; however sample is ND.
(c) Associated CCV outside of control limits high, sample was ND.
(d) Associated Initial Calibration invalid.
(e) Associated ECC and BS outside control limits low.
(f) Suspected carry-over.
(g) Associated CCV outside control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:TB
Lab Sample ID:FA91156-9 Date Sampled:11/24/21
Matrix:AQ - Trip Blank Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0229140.D 1 12/13/21 16:46 JL n/a n/a VA3012
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:TB
Lab Sample ID:FA91156-9 Date Sampled:11/24/21
Matrix:AQ - Trip Blank Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride b 1.4 2.0 1.0 ug/l J
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:TB
Lab Sample ID:FA91156-9 Date Sampled:11/24/21
Matrix:AQ - Trip Blank Water Date Received:11/30/21
Method:SM 6200B Percent Solids:n/a
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 96%70-130%
(a) Sample analyzed beyond hold time; reported results are considered minimum values.
(b) Suspected laboratory contaminant.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
 Chain of Custody
Orlando, FL
Section 4
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FA91156: Chain of Custody
Page 1 of 2
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Job Number:FA91156 Client:GRI
Date / Time Received:11/30/2021 3:00:00 PM Delivery Method:FX
Project:GARRISON'S STARE
Airbill #'s:1009 6379 3112
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (2.4);
Cooler 1: (2.6);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.2; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:STEPHENP Date:Date:11/30/2021 3:00:00 P
FA91156: Chain of Custody
Page 2 of 2
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MS Volatiles
QC Data Summaries
Includes the following where applicable:
 Method Blank Summaries
 Blank Spike Summaries
 Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
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Method Blank Summary Page 1 of 3
Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2597-MB E109772.D 1 12/07/21 JL n/a n/a VE2597
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-1, FA91156-2, FA91156-3, FA91156-4
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
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Method Blank Summary Page 2 of 3
Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2597-MB E109772.D 1 12/07/21 JL n/a n/a VE2597
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-1, FA91156-2, FA91156-3, FA91156-4
CAS No.Compound Result RL MDL Units Q
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 106%70-130%
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Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2597-MB E109772.D 1 12/07/21 JL n/a n/a VE2597
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-1, FA91156-2, FA91156-3, FA91156-4
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 111%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
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Method Blank Summary Page 1 of 3
Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2598-MB E109803.D 1 12/08/21 JL n/a n/a VE2598
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-5, FA91156-6, FA91156-7, FA91156-8
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
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Method Blank Summary Page 2 of 3
Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2598-MB E109803.D 1 12/08/21 JL n/a n/a VE2598
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-5, FA91156-6, FA91156-7, FA91156-8
CAS No.Compound Result RL MDL Units Q
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 99%70-130%
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Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2598-MB E109803.D 1 12/08/21 JL n/a n/a VE2598
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-5, FA91156-6, FA91156-7, FA91156-8
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 113%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
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Method Blank Summary Page 1 of 3
Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3012-MB A0229139.D 1 12/13/21 JL n/a n/a VA3012
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-9
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
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Method Blank Summary Page 2 of 3
Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3012-MB A0229139.D 1 12/13/21 JL n/a n/a VA3012
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-9
CAS No.Compound Result RL MDL Units Q
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 100%70-130%
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Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3012-MB A0229139.D 1 12/13/21 JL n/a n/a VA3012
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-9
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 96%70-130%
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Method Blank Summary Page 1 of 1
Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2606-MB E110013.D 1 12/18/21 JL n/a n/a VE2606
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-5, FA91156-7
CAS No.Compound Result RL MDL Units Q
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 110%70-130%
17060-07-0 1,2-Dichloroethane-D4 110%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
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Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2597-BS a E109770.D 1 12/07/21 JL n/a n/a VE2597
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-1, FA91156-2, FA91156-3, FA91156-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.2 102 70-130
108-86-1 Bromobenzene 10 9.3 93 70-130
74-97-5 Bromochloromethane 10 9.7 97 70-130
75-27-4 Bromodichloromethane 10 9.8 98 70-130
75-25-2 Bromoform 10 8.5 85 70-130
104-51-8 n-Butylbenzene 10 9.5 95 70-130
135-98-8 sec-Butylbenzene 10 10.1 101 70-130
98-06-6 tert-Butylbenzene 10 9.8 98 70-130
56-23-5 Carbon Tetrachloride 10 11.0 110 70-130
108-90-7 Chlorobenzene 10 10.6 106 70-130
75-00-3 Chloroethane 10 11.3 113 60-140
67-66-3 Chloroform 10 9.9 99 70-130
95-49-8 o-Chlorotoluene 10 9.4 94 70-130
106-43-4 p-Chlorotoluene 10 9.4 94 70-130
124-48-1 Dibromochloromethane 10 8.9 89 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.4 94 70-130
106-93-4 1,2-Dibromoethane 10 9.0 90 70-130
75-71-8 Dichlorodifluoromethane 10 11.6 116 60-140
95-50-1 1,2-Dichlorobenzene 10 9.2 92 70-130
541-73-1 1,3-Dichlorobenzene 10 9.4 94 70-130
106-46-7 1,4-Dichlorobenzene 10 10.1 101 70-130
75-34-3 1,1-Dichloroethane 10 10.4 104 70-130
107-06-2 1,2-Dichloroethane 10 11.2 112 70-130
75-35-4 1,1-Dichloroethylene 10 10.8 108 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.0 100 70-130
156-60-5 trans-1,2-Dichloroethylene 10 11.0 110 70-130
78-87-5 1,2-Dichloropropane 10 9.8 98 70-130
142-28-9 1,3-Dichloropropane 10 9.0 90 70-130
594-20-7 2,2-Dichloropropane 10 11.8 118 70-130
563-58-6 1,1-Dichloropropene 10 10.5 105 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.7 97 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.3 93 70-130
108-20-3 Di-Isopropyl Ether 10 10.1 101 70-130
64-17-5 Ethyl Alcohol 500 930 186*70-130
100-41-4 Ethylbenzene 10 10 100 70-130
637-92-3 Ethyl Tert Butyl Ether 10 8.8 88 70-130
* = Outside of Control Limits.
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Blank Spike Summary Page 2 of 3
Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2597-BS a E109770.D 1 12/07/21 JL n/a n/a VE2597
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-1, FA91156-2, FA91156-3, FA91156-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
87-68-3 Hexachlorobutadiene 10 11.3 113 70-130
98-82-8 Isopropylbenzene 10 10 100 70-130
99-87-6 p-Isopropyltoluene 10 9.7 97 70-130
74-83-9 Methyl Bromide 10 11.8 118 60-140
74-87-3 Methyl Chloride 10 12.3 123 60-140
74-95-3 Methylene Bromide 10 9.1 91 70-130
75-09-2 Methylene Chloride 10 6.5 65* b 70-130
1634-04-4 Methyl Tert Butyl Ether 10 11.1 111 70-130
91-20-3 Naphthalene 10 8.9 89 70-130
103-65-1 n-Propylbenzene 10 9.6 96 70-130
100-42-5 Styrene 10 9.1 91 70-130
75-85-4 Tert-Amyl Alcohol 100 105 105 70-130
994-05-8 Tert-Amyl Methyl Ether 10 8.8 88 70-130
75-65-0 Tert-Butyl Alcohol 100 135 135* b 70-130
762-75-4 Tert-Butyl Formate 100 71.9 72 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.8 98 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.5 95 70-130
127-18-4 Tetrachloroethylene 10 10.0 100 70-130
108-88-3 Toluene 10 10.3 103 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.5 95 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.3 93 70-130
71-55-6 1,1,1-Trichloroethane 10 10.5 105 70-130
79-00-5 1,1,2-Trichloroethane 10 9.3 93 70-130
79-01-6 Trichloroethylene 10 10.4 104 70-130
75-69-4 Trichlorofluoromethane 10 14.2 142*60-140
96-18-4 1,2,3-Trichloropropane 10 9.7 97 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.1 91 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.7 97 70-130
75-01-4 Vinyl Chloride 10 12.1 121 60-140
m,p-Xylene 20 19.5 98 70-130
95-47-6 o-Xylene 10 9.6 96 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 102%70-130%
* = Outside of Control Limits.
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Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2597-BS a E109770.D 1 12/07/21 JL n/a n/a VE2597
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-1, FA91156-2, FA91156-3, FA91156-4
CAS No.Surrogate Recoveries BSP Limits
17060-07-0 1,2-Dichloroethane-D4 112%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 95%70-130%
(a) No MSD available for this run.
(b) Sporadic marginal failure.
* = Outside of Control Limits.
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Blank Spike Summary Page 1 of 3
Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2598-BS E109801.D 1 12/08/21 JL n/a n/a VE2598
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-5, FA91156-6, FA91156-7, FA91156-8
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 8.4 84 70-130
108-86-1 Bromobenzene 10 7.7 77 70-130
74-97-5 Bromochloromethane 10 7.9 79 70-130
75-27-4 Bromodichloromethane 10 7.8 78 70-130
75-25-2 Bromoform 10 6.9 69*70-130
104-51-8 n-Butylbenzene 10 8.1 81 70-130
135-98-8 sec-Butylbenzene 10 8.5 85 70-130
98-06-6 tert-Butylbenzene 10 8.3 83 70-130
56-23-5 Carbon Tetrachloride 10 9.0 90 70-130
108-90-7 Chlorobenzene 10 8.4 84 70-130
75-00-3 Chloroethane 10 10.8 108 60-140
67-66-3 Chloroform 10 8.3 83 70-130
95-49-8 o-Chlorotoluene 10 7.9 79 70-130
106-43-4 p-Chlorotoluene 10 7.7 77 70-130
124-48-1 Dibromochloromethane 10 7.2 72 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.2 82 70-130
106-93-4 1,2-Dibromoethane 10 7.3 73 70-130
75-71-8 Dichlorodifluoromethane 10 11.1 111 60-140
95-50-1 1,2-Dichlorobenzene 10 8.0 80 70-130
541-73-1 1,3-Dichlorobenzene 10 8.0 80 70-130
106-46-7 1,4-Dichlorobenzene 10 8.6 86 70-130
75-34-3 1,1-Dichloroethane 10 8.5 85 70-130
107-06-2 1,2-Dichloroethane 10 9.2 92 70-130
75-35-4 1,1-Dichloroethylene 10 8.9 89 70-130
156-59-2 cis-1,2-Dichloroethylene 10 8.1 81 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.0 90 70-130
78-87-5 1,2-Dichloropropane 10 8.1 81 70-130
142-28-9 1,3-Dichloropropane 10 7.4 74 70-130
594-20-7 2,2-Dichloropropane 10 9.8 98 70-130
563-58-6 1,1-Dichloropropene 10 8.4 84 70-130
10061-01-5 cis-1,3-Dichloropropene 10 7.9 79 70-130
10061-02-6 trans-1,3-Dichloropropene 10 7.6 76 70-130
108-20-3 Di-Isopropyl Ether 10 8.5 85 70-130
64-17-5 Ethyl Alcohol 500 896 179*70-130
100-41-4 Ethylbenzene 10 8.0 80 70-130
637-92-3 Ethyl Tert Butyl Ether 10 7.3 73 70-130
* = Outside of Control Limits.
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Blank Spike Summary Page 2 of 3
Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2598-BS E109801.D 1 12/08/21 JL n/a n/a VE2598
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-5, FA91156-6, FA91156-7, FA91156-8
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
87-68-3 Hexachlorobutadiene 10 9.7 97 70-130
98-82-8 Isopropylbenzene 10 8.2 82 70-130
99-87-6 p-Isopropyltoluene 10 8.5 85 70-130
74-83-9 Methyl Bromide 10 11.4 114 60-140
74-87-3 Methyl Chloride 10 11.4 114 60-140
74-95-3 Methylene Bromide 10 7.4 74 70-130
75-09-2 Methylene Chloride 10 5.6 56*70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.1 91 70-130
91-20-3 Naphthalene 10 7.7 77 70-130
103-65-1 n-Propylbenzene 10 8.0 80 70-130
100-42-5 Styrene 10 7.4 74 70-130
75-85-4 Tert-Amyl Alcohol 100 87.4 87 70-130
994-05-8 Tert-Amyl Methyl Ether 10 7.3 73 70-130
75-65-0 Tert-Butyl Alcohol 100 118 118 70-130
762-75-4 Tert-Butyl Formate 100 69.5 70 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 8.1 81 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 7.5 75 70-130
127-18-4 Tetrachloroethylene 10 8.3 83 70-130
108-88-3 Toluene 10 8.4 84 70-130
87-61-6 1,2,3-Trichlorobenzene 10 8.4 84 70-130
120-82-1 1,2,4-Trichlorobenzene 10 8.2 82 70-130
71-55-6 1,1,1-Trichloroethane 10 8.8 88 70-130
79-00-5 1,1,2-Trichloroethane 10 7.6 76 70-130
79-01-6 Trichloroethylene 10 8.6 86 70-130
75-69-4 Trichlorofluoromethane 10 13.3 133 60-140
96-18-4 1,2,3-Trichloropropane 10 7.7 77 70-130
95-63-6 1,2,4-Trimethylbenzene 10 7.8 78 70-130
108-67-8 1,3,5-Trimethylbenzene 10 8.2 82 70-130
75-01-4 Vinyl Chloride 10 11.5 115 60-140
m,p-Xylene 20 15.9 80 70-130
95-47-6 o-Xylene 10 7.8 78 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 97%70-130%
* = Outside of Control Limits.
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Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2598-BS E109801.D 1 12/08/21 JL n/a n/a VE2598
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-5, FA91156-6, FA91156-7, FA91156-8
CAS No.Surrogate Recoveries BSP Limits
17060-07-0 1,2-Dichloroethane-D4 111%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 95%70-130%
* = Outside of Control Limits.
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2
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2
Blank Spike Summary Page 1 of 3
Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3012-BS A0229137.D 1 12/13/21 JL n/a n/a VA3012
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-9
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 11.7 117 70-130
108-86-1 Bromobenzene 10 11.4 114 70-130
74-97-5 Bromochloromethane 10 10.8 108 70-130
75-27-4 Bromodichloromethane 10 10.3 103 70-130
75-25-2 Bromoform 10 9.5 95 70-130
104-51-8 n-Butylbenzene 10 11.4 114 70-130
135-98-8 sec-Butylbenzene 10 12.6 126 70-130
98-06-6 tert-Butylbenzene 10 11.9 119 70-130
56-23-5 Carbon Tetrachloride 10 11.3 113 70-130
108-90-7 Chlorobenzene 10 11.3 113 70-130
75-00-3 Chloroethane 10 8.2 82 60-140
67-66-3 Chloroform 10 10.8 108 70-130
95-49-8 o-Chlorotoluene 10 11.4 114 70-130
106-43-4 p-Chlorotoluene 10 11.4 114 70-130
124-48-1 Dibromochloromethane 10 9.6 96 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 10.5 105 70-130
106-93-4 1,2-Dibromoethane 10 10.8 108 70-130
75-71-8 Dichlorodifluoromethane 10 8.4 84 60-140
95-50-1 1,2-Dichlorobenzene 10 11.3 113 70-130
541-73-1 1,3-Dichlorobenzene 10 11.6 116 70-130
106-46-7 1,4-Dichlorobenzene 10 11.2 112 70-130
75-34-3 1,1-Dichloroethane 10 11.3 113 70-130
107-06-2 1,2-Dichloroethane 10 10.9 109 70-130
75-35-4 1,1-Dichloroethylene 10 11.9 119 70-130
156-59-2 cis-1,2-Dichloroethylene 10 11.3 113 70-130
156-60-5 trans-1,2-Dichloroethylene 10 11.5 115 70-130
78-87-5 1,2-Dichloropropane 10 11.2 112 70-130
142-28-9 1,3-Dichloropropane 10 10.6 106 70-130
594-20-7 2,2-Dichloropropane 10 11.2 112 70-130
563-58-6 1,1-Dichloropropene 10 11.8 118 70-130
10061-01-5 cis-1,3-Dichloropropene 10 10.4 104 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.6 106 70-130
108-20-3 Di-Isopropyl Ether 10 11.4 114 70-130
64-17-5 Ethyl Alcohol 500 631 126 70-130
100-41-4 Ethylbenzene 10 11.7 117 70-130
637-92-3 Ethyl Tert Butyl Ether 10 9.9 99 70-130
* = Outside of Control Limits.
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Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3012-BS A0229137.D 1 12/13/21 JL n/a n/a VA3012
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-9
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
87-68-3 Hexachlorobutadiene 10 12.7 127 70-130
98-82-8 Isopropylbenzene 10 12.2 122 70-130
99-87-6 p-Isopropyltoluene 10 12.3 123 70-130
74-83-9 Methyl Bromide 10 8.9 89 60-140
74-87-3 Methyl Chloride 10 9.2 92 60-140
74-95-3 Methylene Bromide 10 10.1 101 70-130
75-09-2 Methylene Chloride 10 10.1 101 70-130
1634-04-4 Methyl Tert Butyl Ether 10 11.0 110 70-130
91-20-3 Naphthalene 10 11.0 110 70-130
103-65-1 n-Propylbenzene 10 11.8 118 70-130
100-42-5 Styrene 10 11.4 114 70-130
75-85-4 Tert-Amyl Alcohol 100 104 104 70-130
994-05-8 Tert-Amyl Methyl Ether 10 10.1 101 70-130
75-65-0 Tert-Butyl Alcohol 100 123 123 70-130
762-75-4 Tert-Butyl Formate 100 77.2 77 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 11.4 114 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 11.2 112 70-130
127-18-4 Tetrachloroethylene 10 11.6 116 70-130
108-88-3 Toluene 10 11.6 116 70-130
87-61-6 1,2,3-Trichlorobenzene 10 11.2 112 70-130
120-82-1 1,2,4-Trichlorobenzene 10 11.1 111 70-130
71-55-6 1,1,1-Trichloroethane 10 11.2 112 70-130
79-00-5 1,1,2-Trichloroethane 10 11.1 111 70-130
79-01-6 Trichloroethylene 10 11.7 117 70-130
75-69-4 Trichlorofluoromethane 10 10.5 105 60-140
96-18-4 1,2,3-Trichloropropane 10 10.9 109 70-130
95-63-6 1,2,4-Trimethylbenzene 10 11.3 113 70-130
108-67-8 1,3,5-Trimethylbenzene 10 12.0 120 70-130
75-01-4 Vinyl Chloride 10 9.5 95 60-140
m,p-Xylene 20 23.0 115 70-130
95-47-6 o-Xylene 10 11.5 115 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 99%70-130%
* = Outside of Control Limits.
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Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3012-BS A0229137.D 1 12/13/21 JL n/a n/a VA3012
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-9
CAS No.Surrogate Recoveries BSP Limits
17060-07-0 1,2-Dichloroethane-D4 98%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
* = Outside of Control Limits.
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Blank Spike Summary Page 1 of 1
Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2606-BS E110011.D 1 12/18/21 JL n/a n/a VE2606
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-5, FA91156-7
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
107-06-2 1,2-Dichloroethane 10 11.1 111 70-130
75-09-2 Methylene Chloride 10 9.5 95 70-130
91-20-3 Naphthalene 10 8.4 84 70-130
75-85-4 Tert-Amyl Alcohol 100 84.2 84 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 107%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
* = Outside of Control Limits.
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Matrix Spike Summary Page 1 of 3
Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA91156-2MS E110004.D 250 12/17/21 JL n/a n/a VE2597
FA91156-2 a E109795.D 500 12/07/21 JL n/a n/a VE2597
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-1, FA91156-2, FA91156-3, FA91156-4
FA91156-2 Spike MS MS
CAS No.Compound ug/l Q ug/l ug/l %Limits
71-43-2 Benzene 1860 2500 5090 129 70-130
108-86-1 Bromobenzene ND 2500 2600 104 70-130
74-97-5 Bromochloromethane ND 2500 2730 109 70-130
75-27-4 Bromodichloromethane ND 2500 2970 119 70-130
75-25-2 Bromoform ND 2500 2150 86 70-130
104-51-8 n-Butylbenzene ND 2500 2750 110 70-130
135-98-8 sec-Butylbenzene ND 2500 2970 119 70-130
98-06-6 tert-Butylbenzene ND 2500 2890 116 70-130
56-23-5 Carbon Tetrachloride ND 2500 3300 132*70-130
108-90-7 Chlorobenzene ND 2500 2780 111 70-130
75-00-3 Chloroethane ND 2500 3240 130 60-140
67-66-3 Chloroform ND 2500 2960 118 70-130
95-49-8 o-Chlorotoluene ND 2500 2830 113 70-130
106-43-4 p-Chlorotoluene ND 2500 2700 108 70-130
124-48-1 Dibromochloromethane ND 2500 2560 102 70-130
96-12-8 1,2-Dibromo-3-chloropropane ND 2500 2490 100 70-130
106-93-4 1,2-Dibromoethane 190 J 2500 2870 107 70-130
75-71-8 Dichlorodifluoromethane ND 2500 2720 109 60-140
95-50-1 1,2-Dichlorobenzene ND 2500 2650 106 70-130
541-73-1 1,3-Dichlorobenzene ND 2500 2750 110 70-130
106-46-7 1,4-Dichlorobenzene ND 2500 2630 105 70-130
75-34-3 1,1-Dichloroethane ND 2500 3080 123 70-130
107-06-2 1,2-Dichloroethane ND 2500 3090 124 70-130
75-35-4 1,1-Dichloroethylene ND 2500 3330 133*70-130
156-59-2 cis-1,2-Dichloroethylene ND 2500 2970 119 70-130
156-60-5 trans-1,2-Dichloroethylene ND 2500 3040 122 70-130
78-87-5 1,2-Dichloropropane ND 2500 2960 118 70-130
142-28-9 1,3-Dichloropropane ND 2500 2590 104 70-130
594-20-7 2,2-Dichloropropane ND 2500 3140 126 70-130
563-58-6 1,1-Dichloropropene ND 2500 3190 128 70-130
10061-01-5 cis-1,3-Dichloropropene ND 2500 2910 116 70-130
10061-02-6 trans-1,3-Dichloropropene ND 2500 2750 110 70-130
108-20-3 Di-Isopropyl Ether ND 2500 3090 124 70-130
64-17-5 Ethyl Alcohol ND 125000 164000 131*70-130
100-41-4 Ethylbenzene 1870 2500 4990 125 70-130
637-92-3 Ethyl Tert Butyl Ether ND 2500 2760 110 70-130
* = Outside of Control Limits.
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Matrix Spike Summary Page 2 of 3
Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA91156-2MS E110004.D 250 12/17/21 JL n/a n/a VE2597
FA91156-2 a E109795.D 500 12/07/21 JL n/a n/a VE2597
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-1, FA91156-2, FA91156-3, FA91156-4
FA91156-2 Spike MS MS
CAS No.Compound ug/l Q ug/l ug/l %Limits
87-68-3 Hexachlorobutadiene ND 2500 2990 120 70-130
98-82-8 Isopropylbenzene ND 2500 3010 120 70-130
99-87-6 p-Isopropyltoluene ND 2500 2920 117 70-130
74-83-9 Methyl Bromide ND 2500 3120 125 60-140
74-87-3 Methyl Chloride ND 2500 2940 118 60-140
74-95-3 Methylene Bromide ND 2500 2660 106 70-130
75-09-2 Methylene Chloride 751 J 2500 2760 80 70-130
1634-04-4 Methyl Tert Butyl Ether ND 2500 3040 122 70-130
91-20-3 Naphthalene 378 2500 2950 103 70-130
103-65-1 n-Propylbenzene 121 J 2500 2930 112 70-130
100-42-5 Styrene ND 2500 2530 101 70-130
75-85-4 Tert-Amyl Alcohol ND 25000 31300 125 70-130
994-05-8 Tert-Amyl Methyl Ether ND 2500 2720 109 70-130
75-65-0 Tert-Butyl Alcohol ND 25000 27800 111 70-130
762-75-4 Tert-Butyl Formate ND 25000 22100 88 70-130
630-20-6 1,1,1,2-Tetrachloroethane ND 2500 2790 112 70-130
79-34-5 1,1,2,2-Tetrachloroethane ND 2500 2690 108 70-130
127-18-4 Tetrachloroethylene ND 2500 2840 114 70-130
108-88-3 Toluene 10200 2500 12900 108 70-130
87-61-6 1,2,3-Trichlorobenzene ND 2500 2600 104 70-130
120-82-1 1,2,4-Trichlorobenzene ND 2500 2690 108 70-130
71-55-6 1,1,1-Trichloroethane ND 2500 3160 126 70-130
79-00-5 1,1,2-Trichloroethane ND 2500 2630 105 70-130
79-01-6 Trichloroethylene ND 2500 3030 121 70-130
75-69-4 Trichlorofluoromethane ND 2500 3630 145*60-140
96-18-4 1,2,3-Trichloropropane ND 2500 2550 102 70-130
95-63-6 1,2,4-Trimethylbenzene 787 2500 3800 121 70-130
108-67-8 1,3,5-Trimethylbenzene 434 2500 3410 119 70-130
75-01-4 Vinyl Chloride ND 2500 3160 126 60-140
m,p-Xylene 5770 5000 12300 131*70-130
95-47-6 o-Xylene 3250 2500 6720 139*70-130
CAS No.Surrogate Recoveries MS FA91156-2 Limits
1868-53-7 Dibromofluoromethane 113%111%70-130%
* = Outside of Control Limits.
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Matrix Spike Summary Page 3 of 3
Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA91156-2MS E110004.D 250 12/17/21 JL n/a n/a VE2597
FA91156-2 a E109795.D 500 12/07/21 JL n/a n/a VE2597
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-1, FA91156-2, FA91156-3, FA91156-4
CAS No.Surrogate Recoveries MS FA91156-2 Limits
17060-07-0 1,2-Dichloroethane-D4 106%115%70-130%
2037-26-5 Toluene-D8 98%95%70-130%
460-00-4 4-Bromofluorobenzene 101%99%70-130%
(a) Associated internal standard response outside control limits. Confirmed by reanalysis.
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA91209-2MS E109825.D 10 12/08/21 JL n/a n/a VE2598
FA91209-2MSD E109826.D 10 12/08/21 JL n/a n/a VE2598
FA91209-2 E109824.D 10 12/08/21 JL n/a n/a VE2598
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-5, FA91156-6, FA91156-7, FA91156-8
FA91209-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 771 E 100 855 84 100 841 70 2 70-130/20
108-86-1 Bromobenzene ND 100 94.2 94 100 88.9 89 6 70-130/20
74-97-5 Bromochloromethane ND 100 98.1 98 100 95.2 95 3 70-130/20
75-27-4 Bromodichloromethane ND 100 87.0 87 100 84.0 84 4 70-130/20
75-25-2 Bromoform ND 100 54.4 54*100 51.9 52*5 70-130/20
104-51-8 n-Butylbenzene 77.8 100 209 131*100 206 128 1 70-130/20
135-98-8 sec-Butylbenzene 39.3 100 159 120 100 153 114 4 70-130/20
98-06-6 tert-Butylbenzene ND 100 106 106 100 99.1 99 7 70-130/20
56-23-5 Carbon Tetrachloride ND 100 102 102 100 97.1 97 5 70-130/20
108-90-7 Chlorobenzene ND 100 97.4 97 100 93.6 94 4 70-130/20
75-00-3 Chloroethane ND 100 115 115 100 135 135 16 60-140/20
67-66-3 Chloroform ND 100 113 113 100 107 107 5 70-130/20
95-49-8 o-Chlorotoluene ND 100 116 116 100 110 110 5 70-130/20
106-43-4 p-Chlorotoluene ND 100 98.1 98 100 92.8 93 6 70-130/20
124-48-1 Dibromochloromethane ND 100 70.7 71 100 64.9 65*9 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 100 102 102 100 98.1 98 4 70-130/20
106-93-4 1,2-Dibromoethane ND 100 96.1 96 100 90.4 90 6 70-130/20
75-71-8 Dichlorodifluoromethane ND 100 116 116 100 121 121 4 60-140/20
95-50-1 1,2-Dichlorobenzene ND 100 98.4 98 100 91.8 92 7 70-130/20
541-73-1 1,3-Dichlorobenzene ND 100 99.6 100 100 94.4 94 5 70-130/20
106-46-7 1,4-Dichlorobenzene ND 100 101 101 100 97.9 98 3 70-130/20
75-34-3 1,1-Dichloroethane ND 100 108 108 100 103 103 5 70-130/20
107-06-2 1,2-Dichloroethane ND 100 114 114 100 106 106 7 70-130/20
75-35-4 1,1-Dichloroethylene ND 100 110 110 100 103 103 7 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 100 106 106 100 102 102 4 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 100 113 113 100 107 107 5 70-130/20
78-87-5 1,2-Dichloropropane ND 100 111 111 100 104 104 7 70-130/20
142-28-9 1,3-Dichloropropane ND 100 95.0 95 100 89.5 90 6 70-130/20
594-20-7 2,2-Dichloropropane ND 100 115 115 100 110 110 4 70-130/20
563-58-6 1,1-Dichloropropene ND 100 112 112 100 106 106 6 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 100 72.4 72 100 69.7 70 4 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 100 68.9 69*100 64.8 65*6 70-130/20
108-20-3 Di-Isopropyl Ether 2.3 J 100 108 106 100 102 100 6 70-130/20
64-17-5 Ethyl Alcohol ND 5000 6400 128 5000 9180 184*36*70-130/20
100-41-4 Ethylbenzene 1840 E 100 2080 240* a 100 2040 200* a 2 70-130/20
637-92-3 Ethyl Tert Butyl Ether 4.8 J 100 97.2 92 100 94.8 90 3 70-130/20
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA91209-2MS E109825.D 10 12/08/21 JL n/a n/a VE2598
FA91209-2MSD E109826.D 10 12/08/21 JL n/a n/a VE2598
FA91209-2 E109824.D 10 12/08/21 JL n/a n/a VE2598
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-5, FA91156-6, FA91156-7, FA91156-8
FA91209-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
87-68-3 Hexachlorobutadiene ND 100 107 107 100 92.0 92 15 70-130/20
98-82-8 Isopropylbenzene 185 100 328 143*100 321 136*2 70-130/20
99-87-6 p-Isopropyltoluene 11.6 100 119 107 100 113 101 5 70-130/20
74-83-9 Methyl Bromide ND 100 112 112 100 115 115 3 60-140/20
74-87-3 Methyl Chloride ND 100 107 107 100 102 102 5 60-140/20
74-95-3 Methylene Bromide ND 100 97.3 97 100 94.3 94 3 70-130/20
75-09-2 Methylene Chloride 10.0 J 100 72.6 63*100 70.8 61*3 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 100 124 124 100 121 121 2 70-130/20
91-20-3 Naphthalene 770 E 100 947 177* a 100 887 117 7 70-130/20
103-65-1 n-Propylbenzene 513 E 100 722 209* a 100 703 190* a 3 70-130/20
100-42-5 Styrene ND 100 76.4 76 100 72.3 72 6 70-130/20
75-85-4 Tert-Amyl Alcohol ND 1000 1300 130 1000 1540 154*17 70-130/20
994-05-8 Tert-Amyl Methyl Ether ND 100 94.0 94 100 91.7 92 2 70-130/20
75-65-0 Tert-Butyl Alcohol 383 1000 1310 93 1000 1790 141*31*70-130/20
762-75-4 Tert-Butyl Formate ND 1000 616 62*1000 759 76 21*70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 100 101 101 100 97.0 97 4 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 100 109 109 100 100 100 9 70-130/20
127-18-4 Tetrachloroethylene ND 100 104 104 100 96.9 97 7 70-130/20
108-88-3 Toluene 748 E 100 903 155* a 100 878 130 3 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 100 108 108 100 92.7 93 15 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 100 103 103 100 91.1 91 12 70-130/20
71-55-6 1,1,1-Trichloroethane ND 100 106 106 100 101 101 5 70-130/20
79-00-5 1,1,2-Trichloroethane ND 100 107 107 100 102 102 5 70-130/20
79-01-6 Trichloroethylene ND 100 116 116 100 110 110 5 70-130/20
75-69-4 Trichlorofluoromethane ND 100 138 138 100 140 140 1 60-140/20
96-18-4 1,2,3-Trichloropropane ND 100 103 103 100 97.1 97 6 70-130/20
95-63-6 1,2,4-Trimethylbenzene 921 E 100 1160 239* a 100 1140 219* a 2 70-130/20
108-67-8 1,3,5-Trimethylbenzene 122 100 254 132*100 246 124 3 70-130/20
75-01-4 Vinyl Chloride ND 100 125 125 100 135 135 8 60-140/20
m,p-Xylene 1110 E 200 1410 150* a 200 1370 130 3 70-130/20
95-47-6 o-Xylene 231 100 351 120 100 344 113 2 70-130/20
CAS No.Surrogate Recoveries MS MSD FA91209-2 Limits
1868-53-7 Dibromofluoromethane 99%98%106%70-130%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA91209-2MS E109825.D 10 12/08/21 JL n/a n/a VE2598
FA91209-2MSD E109826.D 10 12/08/21 JL n/a n/a VE2598
FA91209-2 E109824.D 10 12/08/21 JL n/a n/a VE2598
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-5, FA91156-6, FA91156-7, FA91156-8
CAS No.Surrogate Recoveries MS MSD FA91209-2 Limits
17060-07-0 1,2-Dichloroethane-D4 100%98%113%70-130%
2037-26-5 Toluene-D8 98%97%95%70-130%
460-00-4 4-Bromofluorobenzene 100%99%100%70-130%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA91244-4MS A0229151.D 10 12/13/21 JL n/a n/a VA3012
FA91244-4MSD A0229152.D 10 12/13/21 JL n/a n/a VA3012
FA91244-4 A0229150.D 10 12/13/21 JL n/a n/a VA3012
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-9
FA91244-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 244 100 346 102 100 328 84 5 70-130/20
108-86-1 Bromobenzene ND 100 98.7 99 100 91.5 92 8 70-130/20
74-97-5 Bromochloromethane ND 100 98.1 98 100 90.8 91 8 70-130/20
75-27-4 Bromodichloromethane ND 100 85.0 85 100 80.2 80 6 70-130/20
75-25-2 Bromoform ND 100 64.4 64*100 60.5 61*6 70-130/20
104-51-8 n-Butylbenzene 8.4 100 106 98 100 99.2 91 7 70-130/20
135-98-8 sec-Butylbenzene 8.1 100 118 110 100 112 104 5 70-130/20
98-06-6 tert-Butylbenzene ND 100 105 105 100 97.3 97 8 70-130/20
56-23-5 Carbon Tetrachloride ND 100 107 107 100 96.9 97 10 70-130/20
108-90-7 Chlorobenzene ND 100 100 100 100 93.2 93 7 70-130/20
75-00-3 Chloroethane ND 100 94.5 95 100 94.4 94 0 60-140/20
67-66-3 Chloroform ND 100 99.7 100 100 91.8 92 8 70-130/20
95-49-8 o-Chlorotoluene ND 100 100 100 100 93.9 94 6 70-130/20
106-43-4 p-Chlorotoluene ND 100 98.3 98 100 90.7 91 8 70-130/20
124-48-1 Dibromochloromethane ND 100 72.4 72 100 67.3 67*7 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 100 98.9 99 100 90.2 90 9 70-130/20
106-93-4 1,2-Dibromoethane ND 100 95.8 96 100 89.2 89 7 70-130/20
75-71-8 Dichlorodifluoromethane ND 100 95.5 96 100 98.3 98 3 60-140/20
95-50-1 1,2-Dichlorobenzene ND 100 99.6 100 100 94.0 94 6 70-130/20
541-73-1 1,3-Dichlorobenzene ND 100 101 101 100 94.3 94 7 70-130/20
106-46-7 1,4-Dichlorobenzene ND 100 98.2 98 100 91.4 91 7 70-130/20
75-34-3 1,1-Dichloroethane ND 100 106 106 100 97.2 97 9 70-130/20
107-06-2 1,2-Dichloroethane ND 100 99.0 99 100 91.5 92 8 70-130/20
75-35-4 1,1-Dichloroethylene ND 100 105 105 100 96.5 97 8 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 100 103 103 100 93.3 93 10 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 100 105 105 100 96.5 97 8 70-130/20
78-87-5 1,2-Dichloropropane ND 100 101 101 100 92.4 92 9 70-130/20
142-28-9 1,3-Dichloropropane ND 100 93.5 94 100 86.7 87 8 70-130/20
594-20-7 2,2-Dichloropropane ND 100 93.3 93 100 86.8 87 7 70-130/20
563-58-6 1,1-Dichloropropene ND 100 108 108 100 98.4 98 9 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 100 75.0 75 100 70.5 71 6 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 100 75.5 76 100 70.4 70 7 70-130/20
108-20-3 Di-Isopropyl Ether 116 100 222 106 100 210 94 6 70-130/20
64-17-5 Ethyl Alcohol ND 5000 6000 120 5000 6180 124 3 70-130/20
100-41-4 Ethylbenzene 80.7 100 184 103 100 176 95 4 70-130/20
637-92-3 Ethyl Tert Butyl Ether ND 100 89.5 90 100 82.2 82 9 70-130/20
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA91244-4MS A0229151.D 10 12/13/21 JL n/a n/a VA3012
FA91244-4MSD A0229152.D 10 12/13/21 JL n/a n/a VA3012
FA91244-4 A0229150.D 10 12/13/21 JL n/a n/a VA3012
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-9
FA91244-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
87-68-3 Hexachlorobutadiene ND 100 108 108 100 101 101 7 70-130/20
98-82-8 Isopropylbenzene 53.8 100 163 109 100 156 102 4 70-130/20
99-87-6 p-Isopropyltoluene ND 100 107 107 100 100 100 7 70-130/20
74-83-9 Methyl Bromide ND 100 97.3 97 100 99.4 99 2 60-140/20
74-87-3 Methyl Chloride ND 100 110 110 100 113 113 3 60-140/20
74-95-3 Methylene Bromide ND 100 93.3 93 100 86.6 87 7 70-130/20
75-09-2 Methylene Chloride 12.5 J 100 101 89 100 94.9 82 6 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 100 113 113 100 106 106 6 70-130/20
91-20-3 Naphthalene 149 100 250 101 100 244 95 2 70-130/20
103-65-1 n-Propylbenzene 153 100 254 101 100 243 90 4 70-130/20
100-42-5 Styrene ND 100 62.6 63*100 58.9 59*6 70-130/20
75-85-4 Tert-Amyl Alcohol 188 1000 1110 92 1000 1040 85 7 70-130/20
994-05-8 Tert-Amyl Methyl Ether ND 100 91.1 91 100 84.4 84 8 70-130/20
75-65-0 Tert-Butyl Alcohol 423 1000 1540 112 1000 1500 108 3 70-130/20
762-75-4 Tert-Butyl Formate ND 1000 697 70 1000 669 67*4 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 100 104 104 100 96.0 96 8 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 100 102 102 100 94.4 94 8 70-130/20
127-18-4 Tetrachloroethylene ND 100 103 103 100 94.6 95 9 70-130/20
108-88-3 Toluene 8.3 100 112 104 100 104 96 7 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 100 97.0 97 100 90.8 91 7 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 100 96.4 96 100 91.1 91 6 70-130/20
71-55-6 1,1,1-Trichloroethane ND 100 105 105 100 96.1 96 9 70-130/20
79-00-5 1,1,2-Trichloroethane ND 100 102 102 100 92.3 92 10 70-130/20
79-01-6 Trichloroethylene ND 100 104 104 100 95.2 95 9 70-130/20
75-69-4 Trichlorofluoromethane ND 100 120 120 100 123 123 2 60-140/20
96-18-4 1,2,3-Trichloropropane ND 100 96.5 97 100 90.4 90 7 70-130/20
95-63-6 1,2,4-Trimethylbenzene 19.3 100 118 99 100 112 93 5 70-130/20
108-67-8 1,3,5-Trimethylbenzene 2.3 J 100 106 104 100 99.2 97 7 70-130/20
75-01-4 Vinyl Chloride ND 100 105 105 100 105 105 0 60-140/20
m,p-Xylene 34.9 200 241 103 200 225 95 7 70-130/20
95-47-6 o-Xylene 4.1 J 100 108 104 100 101 97 7 70-130/20
CAS No.Surrogate Recoveries MS MSD FA91244-4 Limits
1868-53-7 Dibromofluoromethane 101%101%102%70-130%
* = Outside of Control Limits.
66 of 68
FA91156
5
5.
4
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Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA91244-4MS A0229151.D 10 12/13/21 JL n/a n/a VA3012
FA91244-4MSD A0229152.D 10 12/13/21 JL n/a n/a VA3012
FA91244-4 A0229150.D 10 12/13/21 JL n/a n/a VA3012
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-9
CAS No.Surrogate Recoveries MS MSD FA91244-4 Limits
17060-07-0 1,2-Dichloroethane-D4 101%100%103%70-130%
2037-26-5 Toluene-D8 100%100%98%70-130%
460-00-4 4-Bromofluorobenzene 97%97%96%70-130%
* = Outside of Control Limits.
67 of 68
FA91156
5
5.
4
.
2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FA91156
Account:GRINCC GRI (Geological Resources Inc.)
Project:Garrison's Store; 5040 NC Hwy 65, Reidsville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA91490-1MS E110035.D 10 12/18/21 JL n/a n/a VE2606
FA91490-1MSD E110036.D 10 12/18/21 JL n/a n/a VE2606
FA91490-1 E110034.D 10 12/18/21 JL n/a n/a VE2606
The QC reported here applies to the following samples:Method: SM 6200B
FA91156-5, FA91156-7
FA91490-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
107-06-2 1,2-Dichloroethane ND 100 133 133*100 126 126 5 70-130/20
75-09-2 Methylene Chloride 10.7 J 100 121 110 100 118 107 3 70-130/20
91-20-3 Naphthalene 12.0 100 107 95 100 103 91 4 70-130/20
75-85-4 Tert-Amyl Alcohol ND 1000 1030 103 1000 1050 105 2 70-130/20
CAS No.Surrogate Recoveries MS MSD FA91490-1 Limits
1868-53-7 Dibromofluoromethane 117%114%115%70-130%
17060-07-0 1,2-Dichloroethane-D4 112%115%117%70-130%
2037-26-5 Toluene-D8 95%97%95%70-130%
460-00-4 4-Bromofluorobenzene 100%97%98%70-130%
* = Outside of Control Limits.
68 of 68
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APPENDIX F
Contaminant Mass Calculations

Area ID Well ID Area
(ft²)
Average Well
Depth
(ft.)
Average
Depth to
Water
(ft.)
Water Column
Height
(ft)
Volume
(ft³)
Volume
(L)
Effective
Porosity
Effective
Volume
(L)
MW-3
MW-5
MW-8
Area Date Well Benzene
(μg/L)
Toluene
(μg/L)
Ethylbenzene
(μg/L)
Xylenes
(μg/L)
MTBE
(μg/L)
Naphthalene
(μg/L)
Total
(μg/L)
DTW
(ft.)
Average Water
Column Height
(ft.)
Total Average
Mass
(g)
Percent Red.To Date Red.
MW-3 287.00 652.00 241.00 1,154.00 2.95 70.30 2,407.25 18.00
MW-5 17.20 3.39 17.20 62.80 0.00 13.00 113.59 19.37
MW-8 2.35 0.00 1.11 10.03 10.03 0.00 23.52 19.26
Avg.102.18 218.46 86.44 408.94 4.33 27.77 848.12 18.88
MW-3 1,860.00 10,200.00 1,870.00 9,020.00 0.00 378.00 23,328.00 16.87
MW-5 111.00 3.80 143.00 598.00 3.20 193.00 1,052.00 18.05
MW-8 13.00 0.96 8.70 10.70 0.00 83.80 117.16 17.75
Avg.661.33 3,401.59 673.90 3,209.57 1.07 218.27 8,165.72 17.56
Date
Average Water
Column Height
(ft.)
11/19/18 5.45
11/24/21 6.77
Notes:
• FP: Free Product
• Area of the contaminant plume is calculated from Figure 6
• Height of the water column is calculated by subtracting the average depth to water from the average well depth of the referenced monitoring wells
• Volume of the contaminant plume is calculated by multiplying the area of the plume by the average height of the water column during each sampling event
• Effective porosity is assumed based on the sub-surface soil profile obtained from well construction records and soil boring logs
• Total mass was calculated by multiplying the total contaminant concentrations for the sampling event with effective volume
• Contaminant mass cannot be calculated in wells containing FP; therefore, the total contaminant mass is based on the known concentrations in the area for each sampling event.
• When areas couldn’t be sampled, the last known concentrations were used in the calculations.
APPENDIX C
CONTAMINANT MASS CALCULATIONS
GARRISON'S STORE (INCIDENT NO: 15269)
Baseline Event
1 4,463.4 24.33 18.88 5.45 24,326 688,823 0.20 137,765
Area 1
5.45 ------11/19/18
11/24/21 6.77 1,398.10 -1095.9%-1095.9%
116.91
1,398.10 -1096%-1096%
Total Contaminant Mass
(g)
Percent Reduction Compared
to Previous Event Percent Reduction To Date
116.91 ------