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HomeMy WebLinkAboutWS-3891_12913_CA_RMR_20170327 P.O. Box 16265 • Greensboro, NC 27416 503 Industrial Ave • Greensboro, NC 27406 Phone (336)335-3174 • Fax (336)691-0648 • Toll Free (866)545-9507 Email: Info@pyramidenvironmental.com www.pyramidenvironmental.com March 27, 2017 Ms. Mindy Lepard NC Department of Environmental Quality Winston-Salem Regional Office 450 West Hanes Mill Road, Suite 300 Winston-Salem, NC 27105 RE: January-March 2017 Monitoring Report Harold Smith Grocery, Burlington, North Carolina NCDEQ Incident # 12913 Pyramid Project #2016-338 Ms. Lepard: As authorized by T.A.C., Inc., Pyramid Environmental & Engineering, P.C. has completed the Groundwater Monitoring Report for the above referenced site. This report summarizes the results of the first quarterly sampling event in 2017. Please review the enclosed monitoring report, and if you have any questions concerning this report, please call me at (336) 335-3174 ext. 139. Pyramid is planning to meet with Scott Ryals and Vance Jackson of NCDEQ UST Trust Fund to discuss future assessment and remediation activities that need to address the remaining contamination near the former UST area and the pump island at the site. The meeting should be held on March 30, 2017. We will inform you about the meeting results. Sincerely, Brett S. Higgins Project Manager Attachments: Groundwater Monitoring Report Pyramid Environmental Project #2016-339 GROUNDWATER MONITORING REPORT March 29,2017 HAROLD SMITH GROCERY 2774 UNION RIDGE RD.,BURLINGTON,NC ALAMANCE COUNTY Groundwater Incident #: UST Facility ID: Site Ranking: Monitoring Period: UST Owner/Operator: Report prepared for: Report prepared by: ~.~. Brett S.Higgins ~ Project Manager 12913 0-024148 (All USTs Removed) H755E January-March 2017 T.A.C.,Inc. T.A.C.,Inc. 2200 Bessemer Ave. Greensboro,NC 27405 336-273-8663 Report reviewed by: PYRAMID ENVIRONMENTAL &ENGINEERING,P.C. P.O.BOX 16265 GREENSBORO,NC 27416-0265 (336)335-3174 NC Geology License C-257 NC Engineering License C-125111 TABLE OF CONTENTS ACRONYMS ................................................................................................. 4  1.0 INTRODUCTION .............................................................................. 1  1.1 SITE INFORMATION .................................................................................................. 1  1.2 ADJOINING PROPERTIES AND POTENTIAL RECEPTORS ............................................. 1  1.3 SITE HYDROLOGY & GEOLOGY ............................................................................... 2  1.4 PREVIOUS REPORTS ................................................................................................. 2  2.0 GROUNDWATER SAMPLING ....................................................... 2  2.1 MONITORING WELL SAMPLING ................................................................................ 2  2.2 POTABLE WATER SUPPLY WELL SAMPLING ............................................................ 3  3.0 SOIL & GROUNDWATER ASSESSMENT ................................... 3  3.1 GROUNDWATER ANALYTICAL RESULTS .................................................................. 3  3.2 SUPPLY WELL ANALYTICAL RESULTS ..................................................................... 4  4.0 CONCLUSIONS & RECOMMENDATIONS ................................ 5  5.0 CLOSURE ........................................................................................... 6  Page I TABLE OF CONTENTS (Continued) FIGURES: 1. Topographic Map 2. Site Map 3a. Adjoining Properties and Water Supply Wells 3b. Adjoining Properties and Water Supply Wells 4. Potentiometric Surface Map (2/28/17) 5. Benzene Isoconcentration Map (2/28/2017) 6. MTBE Isoconcentration Map (2/28/17) 7. 1,2-Dichloroethane Isoconcentration Map (2/28/17) TABLES: 1. Monitoring Well Construction Details 2. Groundwater Elevation Data 3. Monitoring Well Analytical Results 4. Water Supply Well Analytical Results APPENDICES: A. Standard Field Procedures B. Groundwater Laboratory Report & Chain of Custody C. Supply Well Results Letters Page II ACRONYMS BLS ................Below Land Surface BTEX ............Benzene, Toluene, Ethylbenzene, & Xylenes CFR ................Code of Federal Regulations COC ...............Chain of Custody CSA ................Comprehensive Site Assessment DEQ ...............Department of Environmental Quality EPH ................Extractable Petroleum Hydrocarbons GCLs ..............Gross Contaminant Levels HASP .............Health & Safety Plan MADEP..........Massachusetts Department of Environmental Protection MSCC ............Maximum Soil Contaminant Concentration MTBE ............Methyl Tertiary Butyl Ether µg/L ................Micrograms per Liter mg/kg .............Milligrams per kilogram MW ................Monitoring Well NCAC ............North Carolina Administrative Code O&M ..............Operations and Maintenance OSHA .............Occupational Safety and Health Administration OVA ...............Organic Vapor Analyzer PPM................Parts Per Million PID .................Photo-ionization Detector P&ID ..............Process & Instrumentation Diagram PVC ................Poly-vinyl Chloride QA/QC ...........Quality Assurance / Quality Control SCFM .............Standard Cubic Feet per Minute SVE ................Soil Vapor Extraction SW..................Water Supply Well UST ................Underground Storage Tank US EPA ..........United States Environmental Protection Agency VPH Volatile Petroleum Hydrocarbons Page III Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 1 Pyramid Project # 2016-339 03/29/2017 ACTIVE REMEDIATION MONITORING REPORT Harold Smith Grocery Burlington, North Carolina 1.0 INTRODUCTION 1.1 Site Information SITE NAME: Harold Smith Grocery ADDRESS: 2774 Union Ridge Road CITY: Burlington, NC COUNTY: Alamance CURRENT PROPERTY OWNER: Jessica Alton CURRENT PROPERTY USE: Inactive Store (used as storage) OWNER OF USTs: T.A.C., Inc. (All USTs were removed in 1994) RESPONSIBLE PARTY: T.A.C., Inc. NCDEQ UST FACILITY ID: 0-024148 GROUNDWATER INCIDENT NO.: 12913 SITE RANKING: H755E UNDERGROUND STORAGE TANKS (USTs) UST-ID SIZE (gallons) CONTENTS STATUS DATE 1 550 Kerosene Removed 8/01/94 2 550 Gasoline Removed 8/01/94 3 550 Gasoline Removed 8/01/94 4 1,000 Gasoline Removed 8/01/94 FIGURES: Figure 1: Topographic Map Figure 2: Site Map Figure 3a: Adjoining Properties and Water Supply Wells Figure 3b: Adjoining Properties and Water Supply Wells 1.2 Adjoining Properties and Potential Receptors ADJOINING PROPERTY USE: Residential/Agricultural PUBLIC WATER AVAILABILITY: Unavailable SUPPLY WELLS (SW) WITHIN 1000 FEET: Yes (see Figure 3a/b) SW IMPACTED ABOVE NCAC 2L STANDARDS: Yes, SW-2765 Union Ridge Rd. (POE System) Yes, SW-2773 Union Ridge Rd. (Bottled Water) NEAREST SURFACE WATER: Intermittent Creek – 500-600’ SE BASEMENTS: None SUBSURFACE UTILITIES: None near source area Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 2 Pyramid Project # 2016-339 03/29/2017 1.3 Site Hydrology & Geology GEOLOGIC PROVINCE: Carolina Slate Belt BEDROCK TYPE: Felsic Intrusive Complex DEPTH TO BEDROCK: 25-38 feet BGS (below ground surface) CURRENT DEPTH TO WATER TABLE: 12.27-14.05 feet BGS (02/28/17) HISTORIC GW FLUCTUATIONS: Over the past 15 years, the groundwater has fluctuated in the source area from 5-15 feet BGS POTENTIOMETRIC GRADIENT: Southeast ~ 0.025 ft. /ft. HYDRAULIC CONDUCTIVITY (K): 6.17–6.25 x 10-7 ft. /sec. GROUNDWATER VELOCITY: ~0.4–1.3 feet/year 1.4 Previous Reports REPORT TITLE CONSULTANT DATE OF REPORT COMMENTS UST Closure Report Pyramid Environmental 8/30/94 Soil TPH > Action Level GW Sampling Report Pyramid Environmental 1/2/95 Confirmed GW impact Comprehensive Site Assessment (CSA) Pyramid Environmental 9/20/96 Delineated extent of contamination Corrective Action Plan (CAP) Pyramid Environmental 1/30/97 Original CAP report Corrective Action Plan (CAP) Pyramid Environmental 4/7/97 Revision with changes requested by NCDEQ Pre-CAP Monitoring Report Pyramid Environmental 6/7/99 Received by NCDEQ Active Remediation Monitoring Report Pyramid Environmental 11/99 to 01/13 Received by NCDEQ Soil Cleanup Report Pyramid Environmental 5/31/2011 Received by NCDEQ Active Rem. Mon. Report Pyramid Environmental 4/8/13 to 12/26/16 Received by NCDEQ 2.0 GROUNDWATER SAMPLING 2.1 Monitoring Well Sampling On February 28, 2017, selected monitoring wells at the Harold Smith Site were sampled. WELLS SAMPLED: MW-1A, MW-10, MW-11, MW-12, MW-13, and MW-15A LAB ANALYSES: Standard Method 6200B FREE PRODUCT: No free product has been observed on this site. TABLES & GRAPHS: Table 1: Monitoring Well Construction Details Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 3 Pyramid Project # 2016-339 03/29/2017 Table 2: Groundwater Elevation Data Table 3: Monitoring Well Analytical Results FIGURES: Figure 4: Potentiometric Surface Map Figure 5: Benzene Isoconcentration Map Figure 6: MTBE Isoconcentration Map Figure 7: 1, 2-Dichloroethane Isoconcentration Map STANDARD FIELD PROCEDURES: Appendix A LABORATORY REPORT & CHAIN OF CUSTODY: Appendix B 2.2 Potable Water Supply Well Sampling SAMPLING DATE: February 28, 2017 WELLS SAMPLED: 2765 INF, 2765 MID, 2765 EFF, and 2773 The house at 2779 Union Ridge Road no longer uses the supply well in the front yard, but uses the well located on an adjacent eastern property. The property at 2768 Union Ridge Road uses the supply well in the back yard and is automatically switched to the well in the front yard (2768-A) if the water level gets too low. LAB ANALYSES: Standard Method 6200B TABLES: Table 4: Water Supply Well Analytical Results FIGURES: Figure 3 a/b: Adjoining Properties and Water Supply Wells. STANDARD FIELD PROCEDURES: Appendix A LABORATORY REPORTS & CHAIN OF CUSTODY: Appendix B *NOTE* Supply wells are named by the address of the residence they serve and not the property owner. All supply well addresses sampled are on Union Ridge Road. Mr. James McMillan requested that Pyramid inform him of the POE system analytical results after each sampling. The well analytical evaluation letter is presented in Appendix C. 3.0 SOIL & GROUNDWATER ASSESSMENT 3.1 Groundwater Analytical Results The results of the February 28, 2017 sampling events showed that remaining petroleum contaminants were detected at low concentrations. The concentrations of targeted compounds for this sampling event have shown no significant changes in the monitoring wells. The highest concentrations for this sampling event are shown below. Concentrations above NCAC 2L groundwater standards are shown in bold and the associated well numbers are shown in parentheses. All of the reported concentrations are listed in micrograms per liter (µg/L). Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 4 Pyramid Project # 2016-339 03/29/2017 • Benzene 67 µg/L (MW-1A) • Toluene 4.8 µg/L (MW-1A) • Ethylbenzene 38 µg/L (MW-1A) • Total Xylenes 180 µg/L (MW-1A) • MTBE 29 µg/L (SW-2765 Influent) • Isopropyl Ether (IPE) 170 µg/L (MW-1A) • 1,2-Dichloroethane 11 µg/L (MW-1A) • Naphthalene 85 µg/L (MW-1A) • 1,2,4-Trimethylbenzene 470 µg/L (MW-1A) Over the past 17 years of groundwater and soil remediation, the concentrations in the groundwater monitoring wells have decreased and are now approaching 2L drinking water standards. The benzene concentration in MW-1A has decreased from over 8,000 µg/L in 1998 to 67 µg/L for the current monitoring period. The benzene concentration in MW-1A had been below or slightly above 1.0 µg/L since November 2013; however, the February 2017 sampling event showed a concentration of 67 µg/L. This is most likely due to the influx of the contaminants back diffused from the area beneath the Harold Smith Grocery building. The MTBE concentration in MW-1A has decreased from 610 µg/L in 1999 to 20 µg/L for the current monitoring period. During the current sampling the highest MTBE level recorded was a concentration of 29 µg/L, detected in SW-2765 Influent. In February 2017, monitoring well MW-1A was the well with the highest contaminant concentrations. In addition to MTBE and benzene, 1,2-Dichloroethane (11 µg/L), naphthalene (85 µg/L), 1,2,4-Trimethylbenzene (470 µg/L), and isopropyl ether (170 µg/L) were identified at concentrations above the 2L Groundwater Standard levels in MW-1A. As shown in Table 3, the groundwater contaminant concentrations in the source area decreased significantly after the contaminated soil excavation was performed in May 2011. In planning for the soil excavation project, Pyramid recommended that the DEQ consider the placement of oxygen-release compounds in the open excavation to help clean up the site. Since cleanup is to stringent NCAC 2L Standards, any remedial process that can help reach regulatory closure more quickly should be considered by the DEQ. Pyramid’s request was not approved for Trust Fund reimbursement, and no oxygen-release compounds were used in the excavation. In the future, the Trust Fund should consider reimbursing the use of oxygen-release compounds while excavations are open to help reduce the overall costs for petroleum incident closures. Active soil and groundwater remediation are needed to reduce the remaining petroleum contaminant concentrations in the groundwater. 3.2 Supply Well Analytical Results Supply well sampling was conducted on February 28, 2017 as required by the State. Pyramid sampled supply wells 2765 and 2773. Influent, mid-fluent and effluent samples were collected from the point of entry (POE) treatment system for SW-2765. All samples were collected using Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 5 Pyramid Project # 2016-339 03/29/2017 clean, disposable nitrile gloves, preserved in laboratory provided containers, packed in ice and shipped to Prism Analytical Laboratories for analysis using Standard Method 6200B. Supply Well SW-2765 (McMillan POE System) Groundwater pumped from the supply well at address 2765 (SW-2765) is treated by a Point-of- Entry (POE) treatment system installed in 2000. The POE system consists of particulate and carbon filters that remove petroleum contaminants from the groundwater. This residential treatment system has shown effective groundwater treatment since 2000. The laboratory results of treated water samples collected from the supply well in February 2017 show no detections of petroleum contaminants. Only chloromethane was detected at a concentration of 0.8 µg/L, which is below the 2L Groundwater Standard. Chloromethane is not a petroleum-related contaminant and its presence is most likely associated with the supply well chlorination. Pyramid will continue to monitor concentrations of chloromethane in the POE system. For the untreated water (influent) from SW-2765, MTBE (29 µg/L) and 1,2-Dichloroethane (5.2 µg/L) were detected above their respective (20 µg/L and 0.4 µg/L) NCAC 2L Groundwater Standards. Table 4 shows the recent supply well analytical results. A copy of the laboratory report and chain of custody form is presented in Appendix B. A copy of the supply well 2765 analytical result letter sent to the well owner is presented in Appendix C. Supply Well SW-2773 (Ricky Lassiter Residence) The most recent supply well sampling at the Lassiter residence (SW-2773) showed detections of MTBE (1.8 µg/L), IPE (2 µg/L), and 1,2-Dichloroethane (0.59 µg/L). Only the identified concentration of 1,2-Dichloroethane is above the 2L Groundwater Standard. This supply well has shown few petroleum impacts in the past several years. The Lassiter residence is on bottled water at this time and has been using the account regularly. Since the residence is provided with bottled water, the potential for exposure is mitigated. Pyramid requests that the NC DEQ request a Health Risk Evaluation (HRE) from the central office for this well. T.A.C./Pyramid will continue to monitor the petroleum concentrations for this water supply well. A copy of the supply well 2773 analytical result letter sent to the well owner is presented in Appendix C. Supply Well Recommendations Pyramid recommends continued POE treatment of supply well 2765 and continued sampling of the closest supply wells (2765 & 2773) on a quarterly basis. Pyramid recommends sampling of the wells further from the source area (2761, 2768A, 2774, and 2779) on an annual basis. The next quarterly sampling event will be in May 2017. 4.0 CONCLUSIONS & RECOMMENDATIONS Pyramid has completed the first groundwater monitoring event at the Harold Smith Grocery site in 2017. Based on the current groundwater concentrations of benzene, MTBE, and 1,2- Dichloroethane remaining above the 2L Groundwater Standards, the site remains high risk. The Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 6 Pyramid Project # 2016-339 03/29/2017 remediation goal is to reduce dissolved groundwater contamination below 2L Standards to protect local water supply well users. • The contaminated soil excavation was completed in May 2011. Contaminated soil beneath the NC DOT Right-of-Way and under the store building was unable to be removed. Since petroleum concentrations that exceed the STGW levels remain under the building and near the roadway, continued soil remediation using the SVE system is recommended at the site. The recent increased benzene concentration in groundwater appear to be the result of back-diffusion from the contaminated soil source. • Based on the risk to private well users, Pyramid recommended a new air-sparge system with deeper air sparge wells to enhance the groundwater cleanup. This new system was designed, bid, pre-approved, and built from October 2012 through April 2013. The system was successfully started on April 3, 2013. The new system has shown significant reductions in the remaining petroleum contaminants. • The most recent supply well sampling showed petroleum contamination in two of the closest downgradient water supply wells. One of the wells is on a POE treatment system, and the other residence is supplied with bottled water. The petroleum concentrations in the local water supply wells will continue to be monitored. • The continued presence of concentrations of petroleum contaminants in monitoring wells MW-1A and MW-15A as well as in water supply wells SW-2765, and SW-2773 show that groundwater contamination remains above regulatory closure levels. • Continued groundwater remediation and monitoring is recommended for the Harold Smith site. The next sampling of the monitoring wells and selected supply wells will be conducted in May 2017. Pyramid plans to meet with the State to discuss how to achieve site remediation and regulatory closure. 5.0 CLOSURE This report is prepared for and made available solely for the use of T.A.C, Inc. and the NCDEQ, and the contents thereof may not be used or relied upon by any other person without the express written consent and authorization of Pyramid Environmental & Engineering, P.C. The observations, conclusions, and recommendations documented in this report are based on site conditions and information reviewed at the time of the investigation. Pyramid Environmental & Engineering, P.C. appreciates the opportunity to provide this environmental service. FIGURES USGS ,.5 MINUTE IW' OlI111NAL DATE: "'ar........DAm I I I1--­ I 0 I 0 I 0 USGS TOPOGRAPHIC MAP 2774 UNION RIDGE RD. WI BURlJNGl1lN.Me I 1/2 0 """lls.~Iiiiiiiiiiiiiiiiiiiiiiiiiiiiiii~1~~~~~~~~ ...1000 11lllll1lllllllllll~2000I"-;;;;iiiiiiiiiiiiiiiiiii4000I~"IIIIII"'IIIIII..iii""1III"'"I -=PRIIIMY l-IGHMY.HMO SURFH:E I"_2000' "'I'HDI'OREVlSlClNS DENCIlED IN I'URI'LEIILIGHT-DUTY RQfD HMD OR IIWPROYEDSURFH:E w.G1r£T1C COUNTY IW'OF:II UN~"""""""I NORl11 NORTH CAROLINA II STAlE """I tIIU.UUIE I B 1000'""ALAMANCE 1II'NlEIlSTAlE ROUlE I 0 1.........lE Srn:LOCATION 1 I-~T.A~.C~.~~~~==II7-:_1'--...NClES o'"IIo «z -.Ja0::«u :r: >-~0:::awzuO~ 0:: Cl :r: !:::::::;: VJ o.-1uO•0:::<J;« I-:::C HB HI 31-'0S ::lIHd'nlf> SW-28DD® 1------ I I I I Demolished : House I 2800 I I I I I L J DOT Righi-of-Way House 2779 MW'--5~ MW-l1 c$: c$:MW-12 Q c$:MW-15A MW-6 MW-lA c$: Lassiter Residence 2773 MW-9 c$: MW'-7c$: t!J>• MW-13c$:. G;O SW-2768-BtDeep ..-. MW-3 ....!t 4SW-2768-A Shollow Union Ridge Road House 2765 MW-4c$: MW-l0 SW-27~c$: /./ ./.-/ .~~ t .~ ?SW-276D House 2761 ®----SW-2761 -........-_w--_-w---.J ®Water Supply Well @ Utility Pole --0--0-Fence .......Property Bound . -DOT Ri9ht-Of-~Z. LEGEND MW-B c$: I I I I I I I I .....SYMBOl S "Momtoring Well Q Vertical Extent Well (8!Test Observation Well Wekome tothe Alamance (ountyGLSSite.THIS IS NOT ALEGALDOCUMENT.Alamance County shallassume no liability (Of anyerrors,omissions,orinaccurades inthe informationprovidedregardless of how caused;or arrydedsions made or actions takenor not taken by user in reliance upon anyinformation ordata furnishedhereunder.The user knowinglywaives anyand all claims for damages against anyand all ofthe entities comprisingthe ALAMANCE COUNTY GIS SYSTEM that CONNECTGIS wt:8 HOSnNG Client:TAC.Berico /Harold Smith Grocery Site:2774 Union Ridge Road City/State:Burlington,NC Title:Surrounding Properties Map (#1 -50) -'PVRAMID EtMIIOtN8(fAL &ENGItlEERlNQ,P.e. 7 County:Alamance Scale:1"=500' Job Number:2013-055 Figure #:3a NW.E ~O'<"tf S ,::.-.... ~,.-.,-::~-::-'Client:TAC.Berico /Harold Smith Grocery Site:2774 Union Ridge Road City/State:Burlington,NC Title:Surrounding Properties Map (#51 -69) , PVRAMID ElMlIONlielTAI.&ENGlHESlING,P.C. 1 :500 FeetI County:Alamance Scale:1"=500' Job Number:2013-055 Figure #:3b TABLES TABLE 1 Monitoring Well Construction Details Harold Smith Grocery Incident #12913 Union Ridge Road, Burlington, North Carolina WELL INSTALLED DEPTH BEDROCK CASING INTERVAL INTERVAL INTERVAL INTERVAL INTERVAL MW-1 11/21/94 20’ NBE NA 0-10’ 10-20’ 0-6’ 6-7.5 7.5-20’ MW-1A 6/27/11 24’ NBE NA 0-4’ 4-24’ 0-1’ 1-3’ 3-24’ MW-2 10/11/95 25’ 25’ NA 0-10’ 10-20’ 0-6’ 6-8’ 8-20’ MW-3 10/11/95 22’ NBE NA 0-7’ 7-22’ 0-3’ 3-5’ 5-22’ MW-4 11/8/95 20’ NBE NA 0-5’ 5-20’ 0-2’ 2-4’ 4-20’ MW-5 11/8/95 20’ NBE NA 0-5’ 5-20’ 0-2’ 2-4’ 4-20’ MW-6 1/2/96 53’ 25’ 0-30’ 0-43’ 43-53’ 0-38’ 38-41’ 41-53’ MW-7 1/3/96 13.8’ NBE NA 0-3.8’ 3.8-13.8’ 0-0.5’ 0.5-1.5’ 1.5-13.8’ MW-8 5/6/96 14.3’ 15’ NA 0-4.3’ 4.3-14.3’ 0-1.8’ 1.8-3.3’ 3.3-14.3’ MW-9 5/6/96 15’ NBE NA 0-5’ 5-15’ 0-2.5’ 2.5-4’ 6/4-15’ MW-10 11/30/99 20’ NBE NA 0-5’ 5-20’ 0.5-2’ 2-4’ 4-20’ MW-11 7/25/00 20’ NA NA 0-5’ 5-20’ 0.5-2’ 2-4’ 4-20’ MW-12 11/6/01 30’ NBE NA 0-10’ 10-30’ 0-6’ 6-8’ 8-30’ MW-13 3/5/09 25’ NBE NA 0-5’ 5-25’ 0-1’ 1-3’ 3-25’ MW-14 3/5/09 25’ NBE NA 0-5’ 5-25’ 0-1’ 1-3’ 3-25’ MW-15 3/5/09 25’ 24’ NA 0-5’ 5-25’ 0-1’ 1-3' 3-25’ MW-15A 6/27/11 24’ NBE NA 0-4’ 4-24’ 0-1’ 1-3’ 3-24’ TS-1 12/17/99 15’ NBE NA 0-5’ 5-15’ 0-2’ 2-4’ 4-15’ TS-2 12/17/99 15’ NBE NA 0-5’ 5-15’ 0-2’ 2-4’ 4-15’ TS-3 12/17/99 15’ NBE NA 0-5’ 5-15’ 0-2’ 2-4’ 4-15’ ALL MONITORING WELLS HAVE 2” PVC CASING/RISER AND 2” PVC SCREEN WITH 0.01” SLOTS. OUTER CASING FOR TYPE III WELL IS 6” PVC. NBE = NO BEDROCK ENCOUNTERED. NA = NOT APPLICABLE. SHADED WELLS ARE CLOSED. TOC Depth Depth Free Free Corrected Corrected Well Date Elevation To To Product Product Depth To Water Number Gauged Groundwater Product Thickness Adjustment Water Elevation (feet)(feet)(feet) (feet) (feet) (feet) (feet) MW-1A 06-30-11 94.650 12.24 0.00 0.00 0.00 12.24 82.41 09-8-11 94.650 13.59 0.00 0.00 0.00 13.59 81.06 12-8-11 94.650 13.49 0.00 0.00 0.00 13.49 81.16 03-13-12 94.650 13.49 0.00 0.00 0.00 12.35 82.30 06-5-12 94.650 12.14 0.00 0.00 0.00 12.14 82.51 09-11-12 94.650 13.22 0.00 0.00 0.00 13.22 81.43 12-12-12 94.650 13.85 0.00 0.00 0.00 13.85 80.80 03-12-13 94.650 11.83 0.00 0.00 0.00 11.83 82.82 05-29-13 94.650 10.44 0.00 0.00 0.00 10.44 84.21 09-10-13 94.650 8.96 0.00 0.00 0.00 8.96 85.69 11-6-13 94.650 10.96 0.00 0.00 0.00 10.96 83.69 03-19-14 94.650 8.07 0.00 0.00 0.00 8.07 86.58 06-26-14 94.650 8.72 0.00 0.00 0.00 8.72 85.93 08-22-14 94.650 10.13 0.00 0.00 0.00 10.13 84.52 11-7-14 94.650 12.00 0.00 0.00 0.00 12.00 82.65 03-4-15 94.650 11.21 0.00 0.00 0.00 11.21 83.44 06-25-15 94.650 11.48 0.00 0.00 0.00 11.48 83.17 09-22-15 94.650 13.50 0.00 0.00 0.00 13.50 81.15 12-9-15 94.650 10.67 0.00 0.00 0.00 10.67 83.98 03-2-16 94.650 7.96 0.00 0.00 0.00 7.96 86.69 05-31-16 94.650 8.70 0.00 0.00 0.00 8.70 85.95 09-1-16 94.650 11.18 0.00 0.00 0.00 11.18 83.47 11-28-16 94.650 12.02 0.00 0.00 0.00 12.02 82.63 02-28-17 94.650 12.27 0.00 0.00 0.00 12.27 82.38 MW-3 09-9-09 93.065 12.03 0.00 0.00 0.00 12.03 81.04 12-3-09 93.065 10.40 0.00 0.00 0.00 10.40 82.67 03-24-10 93.065 7.34 0.00 0.00 0.00 7.34 85.73 06-24-10 93.065 8.07 0.00 0.00 0.00 8.07 85.00 09-8-10 93.065 9.62 0.00 0.00 0.00 9.62 83.45 12-10-10 93.065 10.77 0.00 0.00 0.00 10.77 82.30 03-8-11 93.065 10.60 0.00 0.00 0.00 10.60 82.47 06-30-11 93.065 10.74 0.00 0.00 0.00 10.74 82.33 09-8-11 93.065 12.16 0.00 0.00 0.00 12.16 80.91 12-8-11 93.065 12.06 0.00 0.00 0.00 12.06 81.01 03-13-12 93.065 13.49 0.00 0.00 0.00 10.52 82.55 06-5-12 93.065 10.71 0.00 0.00 0.00 10.71 82.36 09-11-12 93.065 11.79 0.00 0.00 0.00 11.79 81.28 12-12-12 93.065 12.37 0.00 0.00 0.00 12.37 80.70 03-12-13 93.065 10.53 0.00 0.00 0.00 10.53 82.54 05-29-13 93.065 9.04 0.00 0.00 0.00 9.04 84.03 09-10-13 93.065 7.53 0.00 0.00 0.00 7.53 85.54 11-6-13 93.065 8.88 0.00 0.00 0.00 8.88 84.19 03-19-14 93.065 6.69 0.00 0.00 0.00 6.69 86.38 06-26-14 93.065 7.46 0.00 0.00 0.00 7.46 85.61 08-22-14 93.065 8.82 0.00 0.00 0.00 8.82 84.25 11-7-14 93.065 10.84 0.00 0.00 0.00 10.84 82.23 03-4-15 93.065 8.51 0.00 0.00 0.00 8.51 84.56 06-25-15 93.065 10.22 0.00 0.00 0.00 10.22 82.85 09-22-15 93.065 12.35 0.00 0.00 0.00 12.35 80.72 12-9-15 93.065 9.42 0.00 0.00 0.00 9.42 83.65 03-2-16 93.065 6.54 0.00 0.00 0.00 6.54 86.53 05-31-16 93.065 7.38 0.00 0.00 0.00 7.38 85.69 09-1-16 93.065 9.92 0.00 0.00 0.00 9.92 83.15 MW-4 09-9-09 91.470 10.81 0.00 0.00 0.00 10.81 80.66 12-3-09 91.470 9.11 0.00 0.00 0.00 9.11 82.36 03-24-10 91.470 6.10 0.00 0.00 0.00 6.10 85.37 06-24-10 91.470 6.76 0.00 0.00 0.00 6.76 84.71 09-8-10 91.470 8.41 0.00 0.00 0.00 8.41 83.06 12-10-10 91.470 9.55 0.00 0.00 0.00 9.55 81.92 03-8-11 91.470 9.37 0.00 0.00 0.00 9.37 82.10 06-30-11 91.470 9.53 0.00 0.00 0.00 9.53 81.94 09-8-11 91.470 11.12 0.00 0.00 0.00 11.12 80.35 12-8-11 91.470 10.81 0.00 0.00 0.00 10.81 80.66 03-13-12 91.470 13.49 0.00 0.00 0.00 8.58 82.89 06-5-12 91.470 9.50 0.00 0.00 0.00 9.50 81.97 09-11-12 91.470 10.67 0.00 0.00 0.00 10.67 80.80 12-12-12 91.470 11.15 0.00 0.00 0.00 11.15 80.32 03-12-13 91.470 8.84 0.00 0.00 0.00 8.84 82.63 05-29-13 91.470 7.80 0.00 0.00 0.00 7.80 83.67 09-10-13 91.470 6.33 0.00 0.00 0.00 6.33 85.14 11-6-13 91.470 7.70 0.00 0.00 0.00 7.70 83.77 03-19-14 91.470 5.51 0.00 0.00 0.00 5.51 85.96 06-26-14 91.470 6.18 0.00 0.00 0.00 6.18 85.29 08-22-14 91.470 7.58 0.00 0.00 0.00 7.58 83.89 11-7-14 91.470 9.62 0.00 0.00 0.00 9.62 81.85 03-4-15 91.470 7.55 0.00 0.00 0.00 7.55 83.92 06-25-15 91.470 8.97 0.00 0.00 0.00 8.97 82.50 09-22-15 91.470 11.11 0.00 0.00 0.00 11.11 80.36 12-9-15 91.470 8.11 0.00 0.00 0.00 8.11 83.36 03-2-16 91.470 5.29 0.00 0.00 0.00 5.29 86.18 05-31-16 91.470 6.15 0.00 0.00 0.00 6.15 85.32 09-1-16 91.470 8.72 0.00 0.00 0.00 8.72 82.75 TABLE 2 Union Ridge Road, Burlington, North carolina Groundwater Elevation Data Harold Smith GrocerIncident #12913 Page 1 of 6 TOC Depth Depth Free Free Corrected Corrected Well Date Elevation To To Product Product Depth To Water Number Gauged Groundwater Product Thickness Adjustment Water Elevation (feet)(feet)(feet) (feet) (feet) (feet) (feet) TABLE 2 Union Ridge Road, Burlington, North carolina Groundwater Elevation Data Harold Smith GrocerIncident #12913 MW-5 09-9-09 95.045 12.81 0.00 0.00 0.00 12.81 82.24 12-3-09 95.045 6.35 0.00 0.00 0.00 6.35 88.70 03-24-10 95.045 6.63 0.00 0.00 0.00 6.63 88.42 06-24-10 95.045 8.25 0.00 0.00 0.00 8.25 86.80 09-8-10 95.045 10.34 0.00 0.00 0.00 10.34 84.71 12-10-10 95.045 9.78 0.00 0.00 0.00 9.78 85.27 03-8-11 95.045 7.20 0.00 0.00 0.00 7.20 87.85 06-30-11 95.045 8.53 0.00 0.00 0.00 8.53 86.52 09-8-11 95.045 12.62 0.00 0.00 0.00 12.62 82.43 12-8-11 95.045 8.74 0.00 0.00 0.00 8.74 86.31 03-13-12 95.045 13.49 0.00 0.00 0.00 10.94 84.11 06-5-12 95.045 10.87 0.00 0.00 0.00 10.87 84.18 09-11-12 95.045 11.98 0.00 0.00 0.00 11.98 83.07 12-12-12 95.045 13.20 0.00 0.00 0.00 13.20 81.85 03-12-13 95.045 7.32 0.00 0.00 0.00 7.32 87.73 05-29-13 95.045 9.38 0.00 0.00 0.00 9.38 85.67 09-10-13 95.045 8.16 0.00 0.00 0.00 8.16 86.89 11-6-13 95.045 9.53 0.00 0.00 0.00 9.53 85.52 03-19-14 95.045 2.87 0.00 0.00 0.00 2.87 92.18 06-26-14 95.045 7.78 0.00 0.00 0.00 7.78 87.27 08-22-14 95.045 9.06 0.00 0.00 0.00 9.06 85.99 11-7-14 95.045 11.16 0.00 0.00 0.00 11.16 83.89 03-4-15 95.045 1.70*0.00 0.00 0.00 1.70* 93.35 06-25-15 95.045 10.78 0.00 0.00 0.00 10.78 84.27 09-22-15 95.045 13.05 0.00 0.00 0.00 13.05 82.00 12-9-15 95.045 7.19 0.00 0.00 0.00 7.19 87.86 03-2-16 95.045 4.93 0.00 0.00 0.00 4.93 90.12 05-31-16 95.045 7.38 0.00 0.00 0.00 7.38 87.67 09-1-16 95.045 10.68 0.00 0.00 0.00 10.68 84.37 MW-6 09-9-09 94.935 14.28 0.00 0.00 0.00 14.28 80.66 12-3-09 94.935 12.98 0.00 0.00 0.00 12.98 81.96 03-24-10 94.935 9.07 0.00 0.00 0.00 9.07 85.87 06-24-10 94.935 9.90 0.00 0.00 0.00 9.90 85.04 09-8-10 94.935 11.76 0.00 0.00 0.00 11.76 83.18 12-10-10 94.935 12.91 0.00 0.00 0.00 12.91 82.03 03-8-11 94.935 12.89 0.00 0.00 0.00 12.89 82.05 06-30-11 94.935 12.91 0.00 0.00 0.00 12.91 82.03 09-8-11 94.935 14.50 0.00 0.00 0.00 14.50 80.44 12-8-11 94.935 14.20 0.00 0.00 0.00 14.20 80.74 03-13-12 94.935 13.49 0.00 0.00 0.00 12.94 82.00 06-5-12 94.935 13.10 0.00 0.00 0.00 13.10 81.84 09-11-12 94.935 14.26 0.00 0.00 0.00 14.26 80.68 12-12-12 94.935 14.58 0.00 0.00 0.00 14.58 80.36 03-12-13 94.935 12.72 0.00 0.00 0.00 12.72 82.22 05-29-13 94.935 11.38 0.00 0.00 0.00 11.38 83.56 09-10-13 94.935 9.65 0.00 0.00 0.00 9.65 85.29 11-6-13 94.935 11.29 0.00 0.00 0.00 11.29 83.65 03-19-14 94.935 8.58 0.00 0.00 0.00 8.58 86.36 06-26-14 94.935 9.39 0.00 0.00 0.00 9.39 85.55 08-22-14 94.935 11.01 0.00 0.00 0.00 11.01 83.93 11-7-14 94.935 12.99 0.00 0.00 0.00 12.99 81.95 03-4-15 94.935 12.11 0.00 0.00 0.00 12.11 82.83 06-25-15 94.935 12.43 0.00 0.00 0.00 12.43 82.51 09-22-15 94.935 14.50 0.00 0.00 0.00 14.50 80.44 12-9-15 94.935 11.53 0.00 0.00 0.00 11.53 83.41 03-2-16 94.935 8.40 0.00 0.00 0.00 8.40 86.54 05-31-16 94.935 9.38 0.00 0.00 0.00 9.38 85.56 09-1-16 94.935 12.14 0.00 0.00 0.00 12.14 82.80 MW-7 09-9-09 94.215 11.61 0.00 0.00 0.00 11.61 82.61 12-3-09 94.215 9.65 0.00 0.00 0.00 9.65 84.57 03-24-10 94.215 7.69 0.00 0.00 0.00 7.69 86.53 06-24-10 94.215 7.55 0.00 0.00 0.00 7.55 86.67 09-8-10 94.215 8.18 0.00 0.00 0.00 8.18 86.04 12-10-10 94.215 10.36 0.00 0.00 0.00 10.36 83.86 03-8-11 94.215 9.94 0.00 0.00 0.00 9.94 84.28 06-30-11 94.215 10.92 0.00 0.00 0.00 10.92 83.30 09-8-11 94.215 12.05 0.00 0.00 0.00 12.05 82.17 12-8-11 94.215 11.64 0.00 0.00 0.00 11.64 82.58 03-13-12 94.215 13.49 0.00 0.00 0.00 10.75 83.47 06-5-12 94.215 10.63 0.00 0.00 0.00 10.63 83.59 09-11-12 94.215 11.33 0.00 0.00 0.00 11.33 82.89 12-12-12 94.215 12.20 0.00 0.00 0.00 12.20 82.02 03-12-13 94.215 NG 0.00 0.00 0.00 0.00 NG 05-29-13 94.215 NG 0.00 0.00 0.00 0.00 NG 09-10-13 94.215 7.57 0.00 0.00 0.00 7.57 86.65 11-6-13 94.215 9.08 0.00 0.00 0.00 9.08 85.14 03-19-14 94.215 6.95 0.00 0.00 0.00 6.95 87.27 Page 2 of 6 TOC Depth Depth Free Free Corrected Corrected Well Date Elevation To To Product Product Depth To Water Number Gauged Groundwater Product Thickness Adjustment Water Elevation (feet)(feet)(feet) (feet) (feet) (feet) (feet) TABLE 2 Union Ridge Road, Burlington, North carolina Groundwater Elevation Data Harold Smith GrocerIncident #12913 MW-7 06-26-14 94.215 7.47 0.00 0.00 0.00 7.47 86.75 08-22-14 94.215 8.70 0.00 0.00 0.00 8.70 85.52 11-7-14 94.215 10.60 0.00 0.00 0.00 10.60 83.62 03-4-15 94.215 9.40 0.00 0.00 0.00 9.40 84.82 06-25-15 94.215 9.96 0.00 0.00 0.00 9.96 84.26 09-22-15 94.215 11.76 0.00 0.00 0.00 11.76 82.46 12-9-15 94.215 9.20 0.00 0.00 0.00 9.20 85.02 03-2-16 94.215 6.88 0.00 0.00 0.00 6.88 87.34 05-31-16 94.215 7.45 0.00 0.00 0.00 7.45 86.77 09-1-16 94.215 9.67 0.00 0.00 0.00 9.67 84.55 MW-8 09-9-09 89.630 NG 0.00 0.00 0.00 0.00 NG 12-3-09 89.630 7.23 0.00 0.00 0.00 7.23 82.40 03-24-10 89.630 5.64 0.00 0.00 0.00 5.64 83.99 06-24-10 89.630 6.13 0.00 0.00 0.00 6.13 83.50 09-8-10 89.630 7.79 0.00 0.00 0.00 7.79 81.84 12-10-10 89.630 9.43 0.00 0.00 0.00 9.43 80.20 03-8-11 89.630 8.39 0.00 0.00 0.00 8.39 81.24 06-30-11 89.630 NG 0.00 0.00 0.00 0.00 NG 09-8-11 89.630 NG 0.00 0.00 0.00 0.00 NG 12-8-11 89.630 NG 0.00 0.00 0.00 0.00 NG 03-13-12 89.630 NG 0.00 0.00 0.00 0.00 NG 06-5-12 89.630 8.80 0.00 0.00 0.00 8.80 80.83 09-11-12 89.630 9.84 0.00 0.00 0.00 9.84 79.79 12-12-12 89.630 10.60 0.00 0.00 0.00 10.60 79.03 03-12-13 89.630 NG 0.00 0.00 0.00 0.00 NG 05-29-13 89.630 NG 0.00 0.00 0.00 0.00 NG 09-10-13 89.630 NG 0.00 0.00 0.00 0.00 NG 11-6-13 89.630 NG 0.00 0.00 0.00 0.00 NG 03-19-14 89.630 NG 0.00 0.00 0.00 0.00 NG 06-26-14 89.630 NG 0.00 0.00 0.00 0.00 NG 08-22-14 89.630 NG 0.00 0.00 0.00 0.00 NG 11-7-14 89.630 NG 0.00 0.00 0.00 0.00 NG 03-4-15 89.630 NG 0.00 0.00 0.00 0.00 NG 06-25-15 89.630 NG 0.00 0.00 0.00 0.00 NG 09-22-15 89.630 NG 0.00 0.00 0.00 0.00 NG 12-9-15 89.630 NG 0.00 0.00 0.00 0.00 NG 03-2-16 89.630 NG 0.00 0.00 0.00 0.00 NG 05-31-16 89.630 NG 0.00 0.00 0.00 0.00 NG 09-1-16 89.630 NG 0.00 0.00 0.00 0.00 NG MW-9 09-9-09 94.770 14.21 0.00 0.00 0.00 14.21 80.56 12-3-09 94.770 12.76 0.00 0.00 0.00 12.76 82.01 03-24-10 94.770 8.91 0.00 0.00 0.00 8.91 85.86 06-24-10 94.770 9.79 0.00 0.00 0.00 9.79 84.98 09-8-10 94.770 11.70 0.00 0.00 0.00 11.70 83.07 12-10-10 94.770 12.89 0.00 0.00 0.00 12.89 81.88 03-8-11 94.770 12.79 0.00 0.00 0.00 12.79 81.98 06-30-11 94.770 NG 0.00 0.00 0.00 0.00 NG 09-8-11 94.770 14.34 0.00 0.00 0.00 14.34 80.43 12-8-11 94.770 14.09 0.00 0.00 0.00 14.09 80.68 03-13-12 94.770 13.49 0.00 0.00 0.00 11.82 82.95 06-5-12 94.770 NG 0.00 0.00 0.00 0.00 NG 09-11-12 94.770 14.15 0.00 0.00 0.00 14.15 80.62 12-12-12 94.770 NG 0.00 0.00 0.00 0.00 NG 03-12-13 94.770 12.60 0.00 0.00 0.00 12.60 82.17 05-29-13 94.770 11.20 0.00 0.00 0.00 11.20 83.57 09-10-13 94.770 9.50 0.00 0.00 0.00 9.50 85.27 11-6-13 94.770 11.16 0.00 0.00 0.00 11.16 83.61 03-19-14 94.770 8.18 0.00 0.00 0.00 8.18 86.59 06-26-14 94.770 9.30 0.00 0.00 0.00 9.30 85.47 08-22-14 94.770 10.88 0.00 0.00 0.00 10.88 83.89 11-7-14 94.770 12.92 0.00 0.00 0.00 12.92 81.85 03-4-15 94.770 12.00 0.00 0.00 0.00 12.00 82.77 06-25-15 94.770 12.27 0.00 0.00 0.00 12.27 82.50 09-22-15 94.770 14.37 0.00 0.00 0.00 14.37 80.40 12-9-15 94.770 11.48 0.00 0.00 0.00 11.48 83.29 03-2-16 94.770 8.28 0.00 0.00 0.00 8.28 86.49 05-31-16 94.770 9.27 0.00 0.00 0.00 9.27 85.50 09-1-16 94.770 11.99 0.00 0.00 0.00 11.99 82.78 MW-10 09-9-09 93.210 13.25 0.00 0.00 0.00 13.25 79.96 12-3-09 93.210 10.51 0.00 0.00 0.00 10.51 82.70 03-24-10 93.210 7.80 0.00 0.00 0.00 7.80 85.41 06-24-10 93.210 8.77 0.00 0.00 0.00 8.77 84.44 09-8-10 93.210 10.74 0.00 0.00 0.00 10.74 82.47 12-10-10 93.210 12.15 0.00 0.00 0.00 12.15 81.06 03-8-11 93.210 11.78 0.00 0.00 0.00 11.78 81.43 06-30-11 93.210 12.29 0.00 0.00 0.00 12.29 80.92 09-8-11 93.210 13.39 0.00 0.00 0.00 13.39 79.82 12-8-11 93.210 12.91 0.00 0.00 0.00 12.91 80.30 03-13-12 93.210 13.49 0.00 0.00 0.00 11.61 81.60 06-5-12 93.210 11.79 0.00 0.00 0.00 11.79 81.42 Page 3 of 6 TOC Depth Depth Free Free Corrected Corrected Well Date Elevation To To Product Product Depth To Water Number Gauged Groundwater Product Thickness Adjustment Water Elevation (feet)(feet)(feet) (feet) (feet) (feet) (feet) TABLE 2 Union Ridge Road, Burlington, North carolina Groundwater Elevation Data Harold Smith GrocerIncident #12913 MW-10 09-11-12 93.210 13.10 0.00 0.00 0.00 13.10 80.11 12-12-12 93.210 13.29 0.00 0.00 0.00 13.29 79.92 03-12-13 93.210 10.93 0.00 0.00 0.00 10.93 82.28 05-29-13 93.210 10.03 0.00 0.00 0.00 10.03 83.18 09-10-13 93.210 8.61 0.00 0.00 0.00 8.61 84.60 11-6-13 93.210 10.11 0.00 0.00 0.00 10.11 83.10 03-19-14 93.210 6.68 0.00 0.00 0.00 6.68 86.53 06-26-14 93.210 8.43 0.00 0.00 0.00 8.43 84.78 08-22-14 93.210 10.00 0.00 0.00 0.00 10.00 83.21 11-7-14 93.210 11.98 0.00 0.00 0.00 11.98 81.23 03-4-15 93.210 10.66 0.00 0.00 0.00 10.66 82.55 06-25-15 93.210 11.35 0.00 0.00 0.00 11.35 81.86 09-22-15 93.210 13.44 0.00 0.00 0.00 13.44 79.77 12-9-15 93.210 10.42 0.00 0.00 0.00 10.42 82.79 03-2-16 93.210 6.95 0.00 0.00 0.00 6.95 86.26 05-31-16 93.210 8.13 0.00 0.00 0.00 8.13 85.08 09-1-16 93.210 11.80 0.00 0.00 0.00 11.80 81.41 11-28-16 93.210 12.07 0.00 0.00 0.00 12.07 81.14 02-28-17 93.210 12.52 0.00 0.00 0.00 12.52 80.69 MW-11 09-9-09 95.840 NG 0.00 0.00 0.00 0.00 NG 12-3-09 95.840 14.05 0.00 0.00 0.00 14.05 81.79 03-24-10 95.840 10.06 0.00 0.00 0.00 10.06 85.78 06-24-10 95.840 10.91 0.00 0.00 0.00 10.91 84.93 09-8-10 95.840 12.77 0.00 0.00 0.00 12.77 83.07 12-10-10 95.840 14.00 0.00 0.00 0.00 14.00 81.84 03-8-11 95.840 13.94 0.00 0.00 0.00 13.94 81.90 06-30-11 95.840 13.92 0.00 0.00 0.00 13.92 81.92 09-8-11 95.840 15.52 0.00 0.00 0.00 15.52 80.32 12-8-11 95.840 15.21 0.00 0.00 0.00 15.21 80.63 03-13-12 95.840 13.49 0.00 0.00 0.00 13.94 81.90 06-5-12 95.840 14.16 0.00 0.00 0.00 14.16 81.68 09-11-12 95.840 15.36 0.00 0.00 0.00 15.36 80.48 12-12-12 95.840 15.60 0.00 0.00 0.00 15.60 80.24 03-12-13 95.840 13.88 0.00 0.00 0.00 13.88 81.96 05-29-13 95.840 12.35 0.00 0.00 0.00 12.35 83.49 09-10-13 95.840 10.64 0.00 0.00 0.00 10.64 85.20 11-6-13 95.840 12.35 0.00 0.00 0.00 12.35 83.49 03-19-14 95.840 9.58 0.00 0.00 0.00 9.58 86.26 06-26-14 95.840 10.41 0.00 0.00 0.00 10.41 85.43 08-22-14 95.840 12.02 0.00 0.00 0.00 12.02 83.82 11-7-14 95.840 14.04 0.00 0.00 0.00 14.04 81.80 03-4-15 95.840 13.21 0.00 0.00 0.00 13.21 82.63 06-25-15 95.840 13.41 0.00 0.00 0.00 13.41 82.43 09-22-15 95.840 15.52 0.00 0.00 0.00 15.52 80.32 12-9-15 95.840 12.59 0.00 0.00 0.00 12.59 83.25 03-2-16 95.840 9.41 0.00 0.00 0.00 9.41 86.43 05-31-16 95.840 10.46 0.00 0.00 0.00 10.46 85.38 09-1-16 95.840 13.14 0.00 0.00 0.00 13.14 82.70 02-28-17 95.840 14.05 0.00 0.00 0.00 14.05 81.79 MW-12 09-9-09 94.270 14.70 0.00 0.00 0.00 14.70 79.57 12-3-09 94.270 13.45 0.00 0.00 0.00 13.45 80.82 03-24-10 94.270 9.50 0.00 0.00 0.00 9.50 84.77 06-24-10 94.270 10.36 0.00 0.00 0.00 10.36 83.91 09-8-10 94.270 12.26 0.00 0.00 0.00 12.26 82.01 12-10-10 94.270 13.43 0.00 0.00 0.00 13.43 80.84 03-8-11 94.270 13.35 0.00 0.00 0.00 13.35 80.92 06-30-11 94.270 13.42 0.00 0.00 0.00 13.42 80.85 09-8-11 94.270 15.05 0.00 0.00 0.00 15.05 79.22 12-8-11 94.270 14.66 0.00 0.00 0.00 14.66 79.61 03-13-12 94.270 13.49 0.00 0.00 0.00 13.43 80.84 06-5-12 94.270 13.58 0.00 0.00 0.00 13.58 80.69 09-11-12 94.270 14.79 0.00 0.00 0.00 14.79 79.48 12-12-12 94.270 15.04 0.00 0.00 0.00 15.04 79.23 03-12-13 94.270 13.24 0.00 0.00 0.00 13.24 81.03 05-29-13 94.270 11.79 0.00 0.00 0.00 11.79 82.48 09-10-13 94.270 10.08 0.00 0.00 0.00 10.08 84.19 11-6-13 94.270 11.73 0.00 0.00 0.00 11.73 82.54 03-19-14 94.270 8.92 0.00 0.00 0.00 8.92 85.35 06-26-14 94.270 9.86 0.00 0.00 0.00 9.86 84.41 08-22-14 94.270 11.43 0.00 0.00 0.00 11.43 82.84 11-7-14 94.270 13.45 0.00 0.00 0.00 13.45 80.82 03-4-15 94.270 12.59 0.00 0.00 0.00 12.59 81.68 06-25-15 94.270 12.82 0.00 0.00 0.00 12.82 81.45 09-22-15 94.270 14.95 0.00 0.00 0.00 14.95 79.32 12-9-15 94.270 12.04 0.00 0.00 0.00 12.04 82.23 03-2-16 94.270 8.84 0.00 0.00 0.00 8.84 85.43 05-31-16 94.270 9.84 0.00 0.00 0.00 9.84 84.43 09-1-16 94.270 12.60 0.00 0.00 0.00 12.60 81.67 11-28-16 94.270 13.38 0.00 0.00 0.00 13.38 80.89 02-28-17 94.270 13.48 0.00 0.00 0.00 13.48 80.79 Page 4 of 6 TOC Depth Depth Free Free Corrected Corrected Well Date Elevation To To Product Product Depth To Water Number Gauged Groundwater Product Thickness Adjustment Water Elevation (feet)(feet)(feet) (feet) (feet) (feet) (feet) TABLE 2 Union Ridge Road, Burlington, North carolina Groundwater Elevation Data Harold Smith GrocerIncident #12913 MW-13 06-24-10 94.805 10.56 0.00 0.00 0.00 10.56 84.25 09-8-10 94.805 9.82 0.00 0.00 0.00 9.82 84.99 12-10-10 94.805 10.93 0.00 0.00 0.00 10.93 83.88 03-8-11 94.805 11.24 0.00 0.00 0.00 11.24 83.57 06-30-11 94.805 10.73 0.00 0.00 0.00 10.73 84.08 09-8-11 94.805 12.51 0.00 0.00 0.00 12.51 82.30 12-8-11 94.805 12.69 0.00 0.00 0.00 12.69 82.12 03-13-12 94.805 13.49 0.00 0.00 0.00 10.48 84.33 06-5-12 94.805 10.28 0.00 0.00 0.00 10.28 84.53 09-11-12 94.805 11.55 0.00 0.00 0.00 11.55 83.26 12-12-12 94.805 13.55 0.00 0.00 0.00 13.55 81.26 03-12-13 94.805 10.33 0.00 0.00 0.00 10.33 84.48 05-29-13 94.805 9.41 0.00 0.00 0.00 9.41 85.40 09-10-13 94.805 7.78 0.00 0.00 0.00 7.78 87.03 11-6-13 94.805 9.36 0.00 0.00 0.00 9.36 85.45 03-19-14 94.805 6.88 0.00 0.00 0.00 6.88 87.93 06-26-14 94.805 7.53 0.00 0.00 0.00 7.53 87.28 08-22-14 94.805 8.60 0.00 0.00 0.00 8.60 86.21 11-7-14 94.805 10.69 0.00 0.00 0.00 10.69 84.12 03-4-15 94.805 9.46 0.00 0.00 0.00 9.46 85.35 06-25-15 94.805 10.11 0.00 0.00 0.00 10.11 84.70 09-22-15 94.805 12.30 0.00 0.00 0.00 12.30 82.51 12-9-15 94.805 8.90 0.00 0.00 0.00 8.90 85.91 03-2-16 94.805 6.54 0.00 0.00 0.00 6.54 88.27 05-31-16 94.805 7.21 0.00 0.00 0.00 7.21 87.60 09-1-16 94.805 9.75 0.00 0.00 0.00 9.75 85.06 02-28-17 94.805 11.09 0.00 0.00 0.00 11.09 83.72 MW-14 03-18-09 94.395 NG 0.00 0.00 0.00 0.00 NG 06-23-09 94.395 NG 0.00 0.00 0.00 0.00 NG 09-9-09 94.395 NG 0.00 0.00 0.00 0.00 NG 12-3-09 94.395 NG 0.00 0.00 0.00 0.00 NG 03-24-10 94.395 NG 0.00 0.00 0.00 0.00 NG 06-24-10 94.395 NG 0.00 0.00 0.00 0.00 NG 09-8-10 94.395 NG 0.00 0.00 0.00 0.00 NG 12-10-10 94.395 NG 0.00 0.00 0.00 0.00 NG 03-8-11 94.395 NG 0.00 0.00 0.00 0.00 NG 06-30-11 94.395 NG 0.00 0.00 0.00 0.00 NG 09-8-11 94.395 NG 0.00 0.00 0.00 0.00 NG 12-8-11 94.395 NG 0.00 0.00 0.00 0.00 NG 03-13-12 94.395 NG 0.00 0.00 0.00 0.00 NG 06-5-12 94.395 NG 0.00 0.00 0.00 0.00 NG 09-11-12 94.395 NG 0.00 0.00 0.00 0.00 NG 12-12-12 94.395 NG 0.00 0.00 0.00 0.00 NG 03-12-13 94.395 NG 0.00 0.00 0.00 0.00 NG 05-29-13 94.395 NG 0.00 0.00 0.00 0.00 NG 09-10-13 94.395 NG 0.00 0.00 0.00 0.00 NG 11-6-13 94.395 NG 0.00 0.00 0.00 0.00 NG 03-19-14 94.395 NG 0.00 0.00 0.00 0.00 NG 06-26-14 94.395 NG 0.00 0.00 0.00 0.00 NG 08-22-14 94.395 NG 0.00 0.00 0.00 0.00 NG 11-7-14 94.395 NG 0.00 0.00 0.00 0.00 NG 03-4-15 94.395 NG 0.00 0.00 0.00 0.00 NG 06-25-15 94.395 NG 0.00 0.00 0.00 0.00 NG 09-22-15 94.395 NG 0.00 0.00 0.00 0.00 NG 12-9-15 94.395 NG 0.00 0.00 0.00 0.00 NG 03-2-16 94.395 NG 0.00 0.00 0.00 0.00 NG 05-31-16 94.395 NG 0.00 0.00 0.00 0.00 NG 09-1-16 94.395 NG 0.00 0.00 0.00 0.00 NG MW-15/03-18-09 93.775 13.77 0.00 0.00 0.00 13.77 80.01 MW-15A 06-23-09 93.775 9.90 0.00 0.00 0.00 9.90 83.88 09-9-09 93.775 11.57 0.00 0.00 0.00 11.57 82.21 12-3-09 93.775 11.24 0.00 0.00 0.00 11.24 82.54 03-24-10 93.775 7.57 0.00 0.00 0.00 7.57 86.21 06-24-10 93.775 8.43 0.00 0.00 0.00 8.43 85.35 09-8-10 93.775 9.67 0.00 0.00 0.00 9.67 84.11 12-10-10 93.775 11.24 0.00 0.00 0.00 11.24 82.54 03-8-11 93.775 11.42 0.00 0.00 0.00 11.42 82.36 06-30-11 94.950 12.47 0.00 0.00 0.00 12.47 82.48 09-8-11 94.950 13.88 0.00 0.00 0.00 13.88 81.07 12-8-11 94.950 13.75 0.00 0.00 0.00 13.75 81.20 03-13-12 94.950 13.49 0.00 0.00 0.00 12.60 82.35 06-5-12 94.950 12.45 0.00 0.00 0.00 12.45 82.50 09-11-12 94.950 13.51 0.00 0.00 0.00 13.51 81.44 12-12-12 94.950 14.08 0.00 0.00 0.00 14.08 80.87 03-12-13 94.950 12.07 0.00 0.00 0.00 12.07 82.88 05-29-13 94.950 8.72 0.00 0.00 0.00 8.72 86.23 09-10-13 94.950 9.17 0.00 0.00 0.00 9.17 85.7811-6-13 94.950 7.94 0.00 0.00 0.00 7.94 87.01 Page 5 of 6 TOC Depth Depth Free Free Corrected Corrected Well Date Elevation To To Product Product Depth To Water Number Gauged Groundwater Product Thickness Adjustment Water Elevation (feet)(feet)(feet) (feet) (feet) (feet) (feet) TABLE 2 Union Ridge Road, Burlington, North carolina Groundwater Elevation Data Harold Smith GrocerIncident #12913 MW-15/03-19-14 94.950 8.33 0.00 0.00 0.00 8.33 86.62 MW-15A 06-26-14 94.950 7.78 0.00 0.00 0.00 7.78 87.17 08-22-14 94.950 9.14 0.00 0.00 0.00 9.14 85.81 11-7-14 94.950 11.24 0.00 0.00 0.00 11.24 83.71 03-4-15 94.950 11.40 0.00 0.00 0.00 11.40 83.55 06-25-15 94.950 10.88 0.00 0.00 0.00 10.88 84.07 09-22-15 94.950 13.81 0.00 0.00 0.00 13.81 81.14 12-9-15 94.950 9.28 0.00 0.00 0.00 9.28 85.67 03-2-16 94.950 8.18 0.00 0.00 0.00 8.18 86.77 05-31-16 94.950 8.88 0.00 0.00 0.00 8.88 86.07 09-1-16 94.950 11.35 0.00 0.00 0.00 11.35 83.60 02-28-17 94.950 12.48 0.00 0.00 0.00 12.48 82.47 *MW-5 depth inaccurate for this event as groundwater was seeping in at time of measurement. Page 6 of 6 PARAMETE UNITS DATE MW-1/ MW-3 MW-4 MW-5 MW-6* MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/ TS-1 NCAC 2L MW-1A MW-15A Groundwater Standard Benzen ug/l 03-14-07 440 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 DNE DNE DNE NS 1 06-06-07 410 <1 <1 <1 3.6 <1 <1 <1 <1 <1 2.4 DNE DNE DNE NS 08-29-07 340 <1 <1 <1 2.6 <1 <1 <1 <1 <1 6.4 DNE DNE DNE NS 12-13-07 200 <1 <1 <1 1.1 <1 <1 <1 <1 <1 9.2 DNE DNE DNE NS 03-14-08 250 <1 <1 <1 24 <1 <1 <1 <1 <1 130 DNE DNE DNE NS 06-18-08 310 <1 <1 <1 NS <1 <1 <1 <1 <1 5.3 DNE DNE DNE NS 09-10-08 <100 <1 <1 <1 11.6 <1 <1 <1 <1 <1 69.5 DNE DNE DNE NS 12-03-08 18 <0.5 <0.5 <0.5 8.7 32 <0.5 <0.5 <0.5 <0.5 41 DNE DNE DNE NS 03-18-09 110 <0.5 1.9 <0.5 <0.5 5.9 <0.5 <0.5 <0.5 <0.5 3.6 <0.5 NS 520 NS 06-23-09 290 <0.5 <0.5 <0.5 <0.5 0.66 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 210 NS 09-09-09 190 <0.5 <0.5 <0.5 <0.5 0.66 NS <0.5 <0.5 NS 5.1 <0.5 NS 910 NS 12-03-09 180 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 7.5 <0.5 NS 440 NS 03-24-10 120 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 55 NS 06-24-10 30 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 98 NS 09-08-10 69.7 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1.1 <0.5 NS 37.5 NS 12-10-10 140 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1.3 <0.5 NS 5.4 NS 03-08-11 120 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 52 NS 06-30-11 18.3 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 77.1 NS 09-08-11 22 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 1.7 <0.5 NS 462 NS 12-09-11 15.4 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 0.61 <0.5 NS 384 NS 03-14-12 20 ND ND ND ND ND NS ND ND ND 0.17J ND NS 290 NS 06-07-12 28 ND ND ND ND ND ND NS ND ND ND ND NS 220 NS 9/11-12/12 30.1 ND ND ND ND ND ND NS ND ND 1.2 ND NS 132 NS 12-12-12 19 ND ND ND ND ND ND NS ND ND 0.81 ND NS 91 NS 03-14-13 20.4 ND ND ND ND NS NS NS ND ND ND ND NS 82.8 NS 05-30-13 0.83 ND ND ND ND NS NS ND ND ND ND ND NS ND NS 09-10-13 5.5 ND ND ND ND ND NS ND ND ND ND ND NS 4.4 NS 11-07-13 0.5 ND ND ND ND ND NS ND ND ND ND ND NS ND NS 03-20-14 0.49 ND ND ND ND ND NS ND ND ND ND ND NS 0.29 NS 06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 08-22-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 11-07-14 0.15 ND ND ND 0.15 ND NS ND ND ND ND ND NS ND NS 03-04-15 ND ND ND ND ND ND NS ND ND ND ND ND NS 1.1 NS 06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 9/22-23/15 1.2 ND ND ND ND ND NS ND ND ND ND ND NS ND NS 12-09-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 03-02-16 22 ND ND ND ND ND NS ND ND ND ND ND NS 0.82 NS 05-31-16 10 ND ND ND ND ND NS ND ND ND ND ND NS ND NS 9/1 - 9/2/16 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 11-28-16 38 NS NS NS NS NS NS NS BRL NS BRL NS NS NS NS 02-28-17 67 NS NS NS NS NS NS NS BRL BRL BRL BRL NS BRL NS Toluen ug/l 03-14-07 2.3 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 600 06-06-07 5200 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 08-29-07 6300 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 12-13-07 3300 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 03-14-08 4400 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 06-18-08 5800 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 09-10-08 1850 <1 <1 <1 <1 <1 2.72 <1 <1 <1 <10 DNE DNE DNE NS 12-03-08 28 <1 <1 <1 <1 140 5.3 <1 <1 <1 <1 DNE DNE DNE NS 03-18-09 3200 <1 <1 <1 <1 50 2.9 <1 <1 <1 <1 <0.5 NS 12000 NS 06-23-09 5700 <1 <1 <1 <1 0.69J 2.9 <1 <1 <1 <1 <1 NS 17000 NS 09-09-09 4300 <1 <1 <1 <1 <1 NS <1 <1 NS <1 <1 NS 25000 NS 12-03-09 3900 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS 30000 NS 03-24-10 3100 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 1600 NS 06-24-10 640 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 6900 NS 09-08-10 1090 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 1630 NS 12-10-10 3100 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 94 NS 03-08-11 1390 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 1940 NS 06-30-11 29.6 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 600 NS 09-08-11 2.1 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 5620 NS 12-09-11 5.9 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 <0.5 <0.5 NS 6820 NS 03-14-12 5.7 ND ND ND ND ND NS ND ND ND ND ND NS 7400 NS 06-07-12 8.2 ND ND ND ND ND ND NS ND ND ND ND NS 6300 NS 9/11-12/12 8.1 ND ND ND ND ND ND NS ND ND ND ND NS 3240 NS 12-12-12 3.3 ND ND ND ND ND ND NS ND ND ND ND NS 3300 NS 03-14-13 5.4 ND ND ND ND NS NS NS ND ND ND ND NS 1860 NS 05-30-13 ND ND ND ND ND NS NS ND ND ND ND ND NS 1.8 NS 09-10-13 7.2 ND ND ND ND ND NS ND ND ND ND ND NS 66.2 NS 11-07-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 03-20-14 0.31 ND ND ND ND ND NS ND ND ND ND ND NS 3 NS 06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 08-22-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 11-07-14 0.12 0.11 ND ND ND ND NS ND ND ND ND ND NS 0.22 NS 03-04-15 ND ND ND ND ND ND NS ND ND ND ND ND NS 58 NS 06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 9/22-23/15 ND ND ND ND ND ND NS ND ND ND ND ND NS 19 NS 12-09-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 03-02-16 1.1 ND ND ND ND ND NS ND ND ND ND ND NS 20 NS 05-31-16 0.65 ND ND ND ND ND NS ND ND ND ND ND NS 1.4 NS 9/1 - 9/2/16 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 11-28-16 2.3 NS NS NS NS NS NS NS BRL NS BRL NS NS NS NS 02-28-17 4.8 NS NS NS NS NS NS NS BRL BRL BRL BRL NS 10 NS Ethylbenzen ug/l 03-14-07 66 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 600 06-06-07 550 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 08-29-07 760 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 12-13-07 620 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 03-14-08 580 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 06-18-08 730 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 09-10-08 228 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 DNE DNE DNE NS 12-03-08 21 <1 <1 <1 <1 11 <1 <1 <1 <1 <1 DNE DNE DNE NS 03-18-09 280 <1 <1 <1 <1 16 <1 <1 <1 <1 <1 6.3 NS 930 NS 06-23-09 870 <1 <1 <1 <1 2.5 <1 <1 <1 <1 <1 <1 NS 3000 NS 09-09-09 830 <1 <1 <1 <1 2.1 NS <1 <1 NS <1 <1 NS 2300 NS 12-03-09 990 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS 2700 NS 03-24-10 720 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 160 NS 06-24-10 250 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 1300 NS 09-08-10 625 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 215 NS 12-10-10 700 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 5.1 NS 03-08-11 307 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 198 NS 06-30-11 19.7 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 140 NS 09-08-11 41.9 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 1550 NS 12-09-11 11.8 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 <0.5 <0.5 NS 1740 NS TABLE 3 Monitoring Well Analytical Results Incident #12913 Harold Smith Grocer Union Ridge Road, Burlington, North Carolina 1 of 4 PARAMETE UNITS DATE MW-1/ MW-3 MW-4 MW-5 MW-6* MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/ TS-1 NCAC 2L MW-1A MW-15A Groundwater Standard TABLE 3 Monitoring Well Analytical Results Incident #12913 Harold Smith Grocer Union Ridge Road, Burlington, North Carolina Ethylbenzen 03-14-12 11 ND ND ND ND ND NS ND ND ND ND ND NS 2200 NS 06-07-12 15 ND ND ND ND ND ND NS ND ND ND ND NS 1900 NS 9/11-12/12 22.5 ND ND ND ND ND ND NS ND ND ND ND NS 1620 NS 12-12-12 21 ND ND ND ND ND ND NS ND ND ND ND NS 1600 NS 03-14-13 13.8 ND ND ND ND NS NS NS ND ND ND ND NS 1440 NS 05-30-13 0.58 ND ND ND ND NS NS ND ND ND ND ND NS 1.7 NS 09-10-13 7.3 ND ND ND ND ND NS ND ND ND ND ND NS 76.8 NS 11-07-13 1.6 ND ND ND ND ND NS ND ND ND ND ND NS 0.88 NS 03-20-14 1.1 ND ND ND ND ND NS ND ND ND ND ND NS 8 NS 06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 08-22-14 0.16 ND ND ND ND ND NS ND ND ND ND ND NS ND NS 11-07-14 ND ND ND ND ND ND NS ND ND ND ND ND NS 0.32 NS 03-04-15 ND ND ND ND ND ND NS ND ND ND ND ND NS 120 NS 06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 9/22-23/15 0.53 ND ND ND ND ND NS ND ND ND ND ND NS 16 NS 12-09-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 03-02-16 3.9 ND ND ND ND ND NS ND ND ND ND ND NS 15 NS 05-31-16 6.3 ND ND ND ND ND NS ND ND ND ND ND NS 4.1 NS 9/1 - 9/2/16 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 11-28-16 13 NS NS NS NS NS NS NS BRL NS BRL NS NS NS NS 02-28-17 38 NS NS NS NS NS NS NS BRL BRL BRL BRL NS 37 NS Total Xylenes ug/l 03-14-07 5700 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 DNE DNE DNE NS 500 06-06-07 7000 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 DNE DNE DNE NS 08-29-07 9600 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 DNE DNE DNE NS 12-13-07 5600 <3 <3 <3 <3 <3 <3 <3 <3 <3 27 DNE DNE DNE NS 03-14-08 6200 <3 <3 <3 <3 <3 <3 <3 <3 <3 16 DNE DNE DNE NS 06-18-08 7800 <3 <3 <3 NS <3 <3 <3 <3 <3 12 DNE DNE DNE NS 09-10-08 2377 <4 <4 <4 <4 <4 <4 <4 <4 <4 <40 DNE DNE DNE NS 12-03-08 610 <3 <3 <3 <3 1810 <3 <3 <3 <3 15 DNE DNE DNE NS 03-18-09 5500 <3 <3 <3 <3 2020 <3 13.6 <3 <3 4.7 2.3 NS 7000 NS 06-23-09 9300 <3 <3 <3 <3 71 <3 <3 <3 <3 <3 <3 NS 22400 NS 09-09-09 8700 <3 <3 <3 <3 30.1 NS <3 <3 NS 3.4 <3 NS 19300 NS 12-03-09 9300 <3 <3 <3 <3 <3 <3 <3 <3 NS 5.8 <3 NS 21200 NS 03-24-10 7800 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 NS 2600 NS 06-24-10 2700 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 NS 11100 NS 09-08-10 5720 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 NS 3790 NS 12-10-10 9700 NS NS <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 0.61 <1.5 NS 162 NS 03-08-11 5700 <1.5 <1.5 <1.5 <1.5 0.66 <1.5 <1.5 <1.5 <1.5 0.82 <1.5 NS 2124 NS 06-30-11 213.2 <1.5 <1.5 <1.5 <1.5 0.66 NS NS <1.5 <1.5 5.8 <1.5 NS 602 NS 09-08-11 42.4 <1.5 <1.5 <1.5 <1.5 0.66 NS NS <1.5 <1.5 11.6 <1.5 NS 3990 NS 12-09-11 48 <1.5 <1.5 <1.5 <1.5 <1.5 NS <1.5 <1.5 <1.5 0.66 <1.5 NS 5680 NS 03-14-12 44 ND ND ND ND ND NS ND ND ND ND ND NS 8300 NS 06-07-12 60 ND ND ND ND ND ND NS ND ND ND ND NS 7400 NS 9/11-12/12 73.9 ND ND ND ND ND ND NS ND ND ND ND NS 5940 NS 12-12-12 28 ND ND ND ND ND ND NS ND ND ND ND NS 7400 NS 03-14-13 44 ND ND ND ND NS NS NS ND ND ND ND NS 5600 NS 05-30-13 1.94 ND ND ND ND NS NS ND ND ND ND ND NS 7.7 NS 09-10-13 83.1 ND ND ND ND ND NS ND ND ND ND ND NS 470 NS 11-07-13 4.5 ND ND ND ND ND NS ND ND ND ND ND NS 3.76 NS 03-20-14 5.6 ND ND ND ND ND NS ND ND ND ND ND NS 32.2 NS 06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 08-22-14 1.13 ND ND ND ND ND NS ND ND ND ND ND NS ND NS 11-07-14 0.27 0.23 ND 0.19 0.22 0.19 NS ND ND ND ND ND NS 1.37 NS 03-04-15 3.2 ND ND ND ND ND NS ND ND ND ND ND NS 570 NS 06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 9/22-23/15 22.3 ND ND ND ND ND NS ND ND ND ND ND NS 250 NS 12-09-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 03-02-16 107 ND ND ND ND ND NS ND ND ND ND ND NS 173 NS 05-31-16 46 ND ND ND ND ND NS ND ND ND ND ND NS 16.3 NS 9/1 - 9/2/16 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 11-28-16 94 NS NS NS NS NS NS NS BRL NS BRL NS NS NS NS 02-28-17 180 NS NS NS NS NS NS NS BRL BRL BRL BRL NS 130 NS TOTAL BTE ug/l 03-14-07 9406 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL DNE DNE DNE NS N/A 06-06-07 13160 BDL BDL BDL 3.6 BDL BDL BDL BDL BDL 2.4 DNE DNE DNE NS 08-29-07 17000 BDL BDL BDL 2.6 BDL BDL BDL BDL BDL 6.4 DNE DNE DNE NS 12-13-07 9720 BDL BDL BDL BDL BDL BDL BDL BDL BDL 36.2 DNE DNE DNE NS 03-14-08 11430 BDL BDL BDL 24 BDL BDL BDL BDL BDL 146 DNE DNE DNE NS 06-18-08 14640 BDL BDL BDL NS BDL BDL BDL BDL BDL 17.3 DNE DNE DNE NS 09-10-08 4455 BDL BDL BDL 11.6 BDL 2.72 BDL BDL BDL 69.5 DNE DNE DNE NS 12-03-08 677 BDL BDL BDL 8.7 1993 5.3 BDL BDL BDL 56 DNE DNE DNE NS 03-18-09 9090 BDL 1.9 BDL BDL 2091.9 2.9 13.6 BDL BDL 8.3 8.6 NS 20450 NS 06-23-09 16160 BDL BDL BDL BDL 74.16 2.9 BDL BDL BDL BDL BDL NS 42610 NS 09-09-09 14020 BDL BDL BDL BDL 32.86 NS BDL BDL NS 8.5 BDL NS 47510 NS 12-03-09 14370 BRL BRL BRL BRL BRL BRL BRL BRL NS 13.3 BRL NS 54340 NS 03-24-10 11740 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS 4415 NS 06-24-10 3620 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS 19398 NS 09-08-10 7504.7 BRL BRL BRL BRL BRL BRL BRL BRL BRL 1.1 BRL NS 5672.5 NS 12-10-10 13640 NS NS BRL BRL BRL BRL BRL BRL BRL 1.91 BRL NS 266.5 NS 03-08-11 7517 ND ND ND ND 0.66 ND ND ND ND 0.82 ND NS 4314 NS 06-30-11 280.8 ND ND ND ND 0.66 NS NS ND ND 5.8 ND NS 1419.1 NS 09-08-11 108.4 ND ND ND ND 0.66 NS NS ND ND 13.3 ND NS 11622 NS 12-09-11 81.1 ND ND ND ND ND NS ND ND ND 1.27 ND NS 14624 NS 03-14-12 80.7 ND ND ND ND ND NS ND ND ND ND ND NS 18190 NS 06-07-12 111.2 ND ND ND ND ND ND NS ND ND ND ND NS 15820 NS 9/11-12/12 134.6 ND ND ND ND ND ND NS ND ND 1.2 ND NS 10932 NS 12-12-12 71.3 ND ND ND ND 0.2 ND NS ND ND 0.81 ND NS 12391 NS 03-14-13 83.6 ND ND ND ND NS NS NS ND ND ND ND NS 8982.8 NS 05-30-13 3.35 ND ND ND ND NS NS ND ND ND ND ND NS 11.2 NS 09-10-13 103.1 ND ND ND ND ND NS ND ND ND ND ND NS 617.4 NS 11-07-13 6.6 ND ND ND ND ND NS ND ND ND ND ND NS 4.64 NS 03-20-14 7.19 ND ND ND ND ND NS ND ND ND ND ND NS 40.49 NS 06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 08-22-14 1.29 ND ND ND ND ND NS ND ND ND ND ND NS ND NS 11-07-14 0.54 0.34 ND 0.19 0.37 0.19 NS ND ND ND ND ND NS 1.91 NS 03-04-15 3.2 ND ND ND ND ND NS ND ND ND ND ND NS 749.1 NS 06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 9/22-23/15 24.03 ND ND ND ND ND NS ND ND ND ND ND NS 285 NS 12-09-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 03-02-16 134 ND ND ND ND ND NS ND ND ND ND ND NS 208.82 NS 05-31-16 62.95 ND ND ND ND ND NS ND ND ND ND ND NS 21.8 NS 9/1 - 9/2/16 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 11-28-16 147.3 NS NS NS NS NS NS NS BRL NS BRL NS NS NS NS 02-28-17 289.8 NS NS NS NS NS NS NS BRL BRL BRL BRL NS 177 NS 2 of 4 PARAMETE UNITS DATE MW-1/ MW-3 MW-4 MW-5 MW-6* MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/ TS-1 NCAC 2L MW-1A MW-15A Groundwater Standard TABLE 3 Monitoring Well Analytical Results Incident #12913 Harold Smith Grocer Union Ridge Road, Burlington, North Carolina Methyl Tertiary ug/l 03-14-07 <50 <5 10 <5 4.3J <5 <5 <5 <5 <5 2.7J DNE DNE DNE NS 20 Butyl Ether 06-06-07 <50 19 7.5 <5 5.9 <5 4.9J <5 <5 <5 4.1J DNE DNE DNE NS (MTBE)08-29-07 <50 73 4.6J <5 7.1 <5 <5 <5 <5 <5 4.1J DNE DNE DNE NS 12-13-07 <50 97 20 <5 8.5 <5 <5 <5 <5 <5 13 DNE DNE DNE NS 03-14-08 <50 10 6.9 <5 16 <5 <5 <5 <5 <5 74 DNE DNE DNE NS 06-18-08 <50 26 27 <5 NS <5 <5 <5 <5 <5 15 DNE DNE DNE NS 09-10-08 <200 2.3 <2 <2 6.39 <2 <2 <2 <2 <2 38.1 DNE DNE DNE NS 12-03-08 <5 2.8J 8.9 <5 9.3 5.1 <5 <5 <5 <5 75 DNE DNE DNE NS 03-18-09 <50 <5 <5 <5 <5 8.2 <5 8.3 <5 <5 25 <0.5 NS <50 NS 06-23-09 <50 <5 5.4 <5 <5 3.3J <5 <5 <5 <5 11 <5 NS <50 NS 09-09-09 <50 <5 7.7 <5 <5 2.6J NS <5 <5 NS 44 <5 NS <200 NS 12-03-09 <50 <5 4J <5 <5 <5 <5 <5 <5 NS 92 <5 NS <200 NS 03-24-10 <50 <5 13 <5 <5 <5 <5 <5 <5 <5 3.3J <5 NS <200 NS 06-24-10 <50 <1 4.2 <1 <1 1.5 <1 <1 <1 <1 13 <1 NS <40 NS 09-08-10 <2.5 <0.5 1.7 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 45.8 <0.5 NS <5 NS 12-10-10 <10 NS NS <1 <1 <1 <1 <1 <1 <1 57 <1 NS <1 NS 03-08-11 <10 <0.5 1.6 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 19.1 <0.5 NS <10 NS 06-30-11 2.7 <0.5 0.83 <0.5 <0.5 <0.5 NS NS 0.51 <0.5 23.8 <0.5 NS <0.5 NS 09-08-11 12.3 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS 0.54 <0.5 54.7 <0.5 NS 2.9 NS 12-09-11 9.2 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 0.52 <0.5 28.5 <0.5 NS <25 NS 03-14-12 9.6 ND 0.5 ND 0.25J ND NS ND 0.84 ND 10 ND NS ND NS 06-07-12 ND ND ND ND ND ND ND NS 1.7 ND 15 ND NS ND NS 9/11-12/12 21.4 ND ND ND ND ND ND NS 2.2 ND 33.8 ND NS ND NS 12-12-12 21 ND ND ND 0.19J ND ND NS 0.32J ND 24 ND NS ND NS 03-14-13 21.3 ND ND ND ND NS NS NS ND ND 8.4 ND NS ND NS 05-30-13 9.4 ND ND ND ND NS NS ND 0.8 ND 2 ND NS 0.61 NS 09-10-13 14.4 ND ND ND ND ND NS ND 2.9 ND 1.9 ND NS ND NS 11-07-13 9.4 ND ND ND ND ND NS ND 2.2 ND 1.2 ND NS ND NS 03-20-14 8.6 ND 0.35 ND 0.16 ND NS 1.1 0.12 ND 1.8 ND NS 0.2 NS 06-26-14 0.25 ND 0.32 ND 0.53 0.24 NS 0.3 3.2 ND 0.66 ND NS ND NS 08-22-14 4.1 ND ND ND ND ND NS 0.25 1.3 ND 0.57 ND NS ND NS 11-07-14 0.79 ND ND ND ND ND NS 1.4 1.5 ND 0.46 ND NS ND NS 03-04-15 4.6 ND ND ND 0.60J ND NS 1.6 ND ND 0.80J ND NS ND NS 06-25-15 3.9 ND ND ND 0.75J ND NS ND 0.67J ND 0.68J ND NS ND NS 9/22-23/15 6.2 ND ND ND 1 ND NS ND ND ND ND ND NS ND NS 12-09-15 1.7 ND ND ND 1.9 ND NS ND ND ND ND ND NS ND NS 03-02-16 8.5 ND ND ND 1.4 ND NS ND ND ND 1.4 ND NS ND NS 05-31-16 16 ND ND ND 1.2 ND NS ND ND 0.72J ND ND NS ND NS 9/1 - 9/2/16 7.1 ND ND ND ND ND NS ND ND ND ND ND NS ND NS 11-28-16 13 NS NS NS NS NS NS NS BRL NS BRL NS NS NS NS 02-28-17 20 NS NS NS NS NS NS NS BRL BRL BRL BRL NS BRL NS Ethylen ug/l 03-14-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 0.02 Dibromid 06-06-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS (EDB)08-29-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 12-13-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 03-14-08 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 06-18-08 <10 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 09-10-08 <2 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 DNE DNE DNE NS 12-03-08 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 03-18-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <0.5 NS <50 NS 06-23-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS <50 NS 09-09-09 <10 <1 <1 <1 <1 <1 NS <1 <1 NS <1 <1 NS <40 NS 12-03-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS <40 NS 03-24-10 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS <40 NS 06-24-10 14 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 28 NS 09-08-10 <2.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS <5 NS 12-10-10 <5 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 3.9 NS 03-08-11 <10 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS <10 NS 06-30-11 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 1.9 NS 09-08-11 <1.2 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 7 NS 12-09-11 <1 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 <0.5 <0.5 NS <25 NS 03-14-12 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 06-07-12 ND ND ND ND ND ND ND NS ND ND ND ND NS ND NS 9/11-12/12 ND ND ND ND ND ND ND NS ND ND ND ND NS ND NS 12-12-12 ND ND ND ND ND ND ND NS ND ND ND ND NS ND NS 03-14-13 ND ND ND ND ND NS NS NS ND ND ND ND NS ND NS 05-30-13 ND ND ND ND ND NS NS ND ND ND ND ND NS ND NS 09-10-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 11-07-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 03-20-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 08-22-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 11-07-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 03-04-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 9/22-23/15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 12-09-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 03-02-16 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 05-31-16 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 9/1 - 9/2/16 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 11-28-16 NS NS NS NS NS NS NS NS BRL NS BRL NS NS NS NS 02-28-17 BRL NS NS NS NS NS NS NS BRL BRL BRL BRL NS BRL NS Isopropyl Ether ug/l 03-14-08 86 <5 3J <5 9.9 <5 <5 <5 <5 <5 270 DNE DNE DNE NS 70 (IPE)06-18-08 <50 <5 13 <5 NS <5 <5 <5 <5 <5 19 DNE DNE DNE NS 09-10-08 <100 <1 <1 <1 9.28 <1 <1 <1 <1 <1 221 DNE DNE DNE NS 12-03-08 15 <5 4.6J <5 6.9 23 <5 8.1 <5 <5 200 DNE DNE DNE NS 03-18-09 <50 <5 <5 <5 <5 19 <5 10 <5 <5 69 <0.5 NS <50 NS 06-23-09 <50 <5 <5 <5 <5 6.2 <5 <5 <5 <5 10 <5 NS <50 NS 09-09-09 <50 <5 3.3J <5 <5 4.9J NS <5 <5 NS 73 <5 NS <200 NS 12-03-09 <50 <5 <5 <5 <5 <5 <5 <5 <5 NS 180 <5 NS <200 NS 03-24-10 <50 <5 5.9 <5 <5 <5 <5 <5 <5 <5 3.2J <5 NS <200 NS 06-24-10 <5 <0.5 1.8 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 12 <0.5 NS <20 NS 09-08-10 2.9 <0.5 0.66 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 35.9 <0.5 NS <5 NS 12-10-10 6 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 49 <0.5 NS 1.3 NS 03-08-11 <10 <0.5 <0.5 <0.5 <0.5 0.56 <0.5 <0.5 0.82 <0.5 24.6 <0.5 NS <10 NS 06-30-11 13 <0.5 <0.5 <0.5 <0.5 0.56 NS NS 1.2 <0.5 29.2 <0.5 NS 2.7 NS 09-08-11 62.2 <0.5 <0.5 <0.5 <0.5 0.56 NS NS 0.73 <0.5 55.2 <0.5 NS 22.5 NS 3 of 4 PARAMETE UNITS DATE MW-1/ MW-3 MW-4 MW-5 MW-6* MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/ TS-1 NCAC 2L MW-1A MW-15A Groundwater Standard TABLE 3 Monitoring Well Analytical Results Incident #12913 Harold Smith Grocer Union Ridge Road, Burlington, North Carolina Isopropyl Ether 12-09-11 40.9 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 29.1 <0.5 NS <25 NS (IPE)03-14-12 47 ND ND ND ND ND NS ND 0.17J ND 11 ND NS ND NS 06-07-12 78 ND ND ND ND ND ND NS 0.52J ND 12 ND NS 15J NS 9/11-12/12 94.8 ND ND ND ND ND ND NS 1.6 ND 29.8 ND NS 13.5 NS 12-12-12 120 ND ND ND 0.16J ND ND NS 1.6 ND 26 ND NS ND NS 03-14-13 112 ND ND ND ND NS NS NS ND ND 10.2 ND NS ND NS 05-30-13 32.5 ND ND ND ND NS NS 3.1 1.5 ND ND ND NS 1.5 NS 09-10-13 80.7 ND ND ND ND ND NS 3.1 6.9 ND ND ND NS 7.2 NS 11-07-13 42.2 ND ND ND ND ND NS ND 3.1 1.9 ND ND NS 0.79 NS 03-20-14 46 ND ND ND 0.2 ND NS ND 3.1 1.9 0.34 ND NS 1.5 NS 06-26-14 ND ND ND ND 1.4 ND NS ND 3.3 3.1 ND ND NS ND NS 08-22-14 11 ND ND ND 0.24 ND NS ND 2.1 3.1 ND ND NS ND NS 11-07-14 2 ND ND ND ND ND NS ND 1.1 ND ND ND NS ND NS 03-04-15 27 ND ND ND ND ND NS ND ND ND 0.5 ND NS ND NS 06-25-15 11 ND ND ND ND ND NS ND 0.59 ND ND ND NS ND NS 9/22-23/15 32 ND ND ND ND ND NS ND ND ND ND ND NS ND NS 12-09-15 6 ND ND ND ND ND NS ND ND 1.9 ND ND NS ND NS 03-02-16 75 ND ND ND ND ND NS ND ND ND 1.1 ND NS ND NS 05-31-16 120 E ND ND ND ND ND NS ND ND 4.5 ND ND NS ND NS 9/1 - 9/2/16 51 ND ND ND ND ND NS ND ND ND ND ND NS ND NS 11-28-16 94 NS NS NS NS NS NS NS BRL NS BRL NS NS NS NS 02-28-17 170 NS NS NS NS NS NS NS BRL BRL BRL BRL NS BRL NS 1,2-Dichloroethan ug/l 03-14-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 0.4 06-06-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 08-29-07 <10 <1 <1 <1 <1 <1 <1 <1 1.4 <1 1.3 DNE DNE DNE NS 12-13-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 1.5 DNE DNE DNE NS 03-14-08 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 31 DNE DNE DNE NS 06-18-08 <10 <1 1.3 <1 NS <1 <1 <1 <1 <1 2.8 DNE DNE DNE NS 09-10-08 <2 <1 <1 <1 <1 <1 <1 <1 <1 <1 29.3 DNE DNE DNE NS 12-03-08 <1 <1 <1 <1 <1 4 <1 0.76J <1 <1 30 DNE DNE DNE NS 03-18-09 <10 <1 <1 <1 <1 2.1 <1 1.5 <1 <1 4.5 <0.5 NS <50 NS 06-23-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 0.69J <1 NS <50 NS 09-09-09 <10 <1 <1 <1 <1 0.64J NS <1 <1 NS 8.6 <1 NS <40 NS 12-03-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 NS 13 <1 NS <40 NS 03-24-10 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS <40 NS 06-24-10 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 2.8 <0.5 <0.5 NS <20 NS 09-08-10 <2.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 6.9 <0.5 NS <5 NS 12-10-10 <5 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 11 <0.5 NS <0.5 NS 03-08-11 <10 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 7.1 <0.5 NS <10 NS 06-30-11 1.1 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 9.1 <0.5 NS 0.58 NS 09-08-11 4.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 10.9 <0.5 NS 4 NS 12-09-11 4.1 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 7.1 <0.5 NS <25 NS 03-14-12 ND ND ND ND ND ND NS ND 0.33J ND 3.6 ND NS ND NS 06-07-12 ND ND ND ND ND ND ND NS ND ND 4 ND NS ND NS 9/11-12/12 13.7 ND ND ND ND ND ND NS 0.67 ND 5.9 ND NS ND NS 12-12-12 15 ND ND ND ND ND ND NS ND ND 0.81 ND NS 4.9 NS 03-14-13 14.2 ND ND ND ND NS NS NS 0.72 ND 3.3 ND NS ND NS 05-30-13 4.2 ND ND ND ND NS NS ND 1.1 ND 0.53 ND NS ND NS 09-10-13 9.2 ND ND ND ND ND NS ND 2.4 ND 0.51 ND NS 0.6 NS 11-07-13 4.1 ND ND ND ND ND NS ND 2.2 ND ND ND NS ND NS 03-20-14 4.8 ND ND ND 0.23 ND NS ND 3.2 ND ND ND NS ND NS 06-26-14 ND ND ND ND 0.32 ND NS ND 1.4 0.63 ND ND NS ND NS 08-22-14 2 ND ND ND ND ND NS ND 1.2 0.84 ND ND NS ND NS 11-07-14 ND ND ND ND ND ND NS ND 0.69 ND ND ND NS ND NS 03-04-15 2.7 ND ND ND ND ND NS ND ND ND ND ND NS ND NS 06-25-15 1.6 ND ND ND ND ND NS ND ND 0.53 ND ND NS ND NS 9/22-23/15 3.7 ND ND ND ND ND NS ND ND ND ND ND NS ND NS 12-09-15 1.2 ND ND ND ND ND NS ND ND 0.61 ND ND NS ND NS 03-02-16 7.3 ND ND ND ND ND NS ND ND 1 ND ND NS ND NS 05-31-16 11 ND ND ND ND ND NS ND ND 1 ND ND NS ND NS 9/1 - 9/2/16 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 11-28-16 7.8 NS NS NS NS NS NS NS BRL NS BRL NS NS NS NS 02-28-17 11 NS NS NS NS NS NS NS BRL BRL BRL BRL NS BRL NS Naphthalen ug/l 03-14-08 470 <1 <1 <1 <1 <1 <1 <1 <1 <1 4.5 DNE DNE DNE NS 6 06-18-08 590 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 09-10-08 136 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 DNE DNE DNE NS 12-03-08 31 <1 <1 <1 <1 <1 <1 <1 <1 <1 3.5 DNE DNE DNE NS 03-18-09 250 <1 1.9 <1 <1 <1 <1 1.6 <1 <1 <1 6.2 NS 490 NS 06-23-09 470 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 950 NS 09-09-09 540 <1 <1 <1 <1 <1 NS <1 <1 NS <1 <1 NS 680 NS 12-03-09 490 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS 750 NS 03-24-10 550 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 220 NS 06-24-10 680 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 580 NS 09-08-10 736 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 NS 255 NS 12-10-10 520 NS NS <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 7.1 NS 03-08-11 337 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 NS 118 NS 06-30-11 54.1 <2 <2 <2 <2 <2 NS NS <2 <2 3 <2 NS 41.6 NS 09-08-11 154 <2 <2 <2 <2 <2 NS NS <2 <2 5.9 <2 NS 395 NS 12-09-11 112 <2 <2 <2 <2 <2 NS <2 <2 <2 <2 <2 NS 504 NS 03-14-12 87 ND ND ND ND ND NS ND ND ND ND ND NS 130J NS 06-07-12 84 ND ND ND ND ND ND NS ND ND ND ND NS 150 NS 9/11-12/12 197 ND ND ND ND ND ND NS ND ND ND ND NS 515 NS 12-12-12 99 ND ND ND ND ND ND NS ND ND ND ND NS 250 NS 03-14-13 84.6 ND ND ND ND NS NS NS ND ND ND ND NS 344 NS 05-30-13 3.4 ND ND ND ND NS NS ND ND ND ND ND NS ND NS 09-10-13 18 ND ND ND ND ND NS ND ND ND ND ND NS 2.3 NS 11-07-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 03-20-14 2.5 ND ND ND ND ND NS ND ND ND ND ND NS ND NS 06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 08-22-14 0.66 ND ND ND ND ND NS ND ND ND ND ND NS ND NS 11-07-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 03-04-15 0.73J ND ND ND ND ND NS ND ND ND ND ND NS 33 NS 06-25-15 0.99J ND ND ND ND ND NS ND ND ND ND ND NS ND NS 9/22-23/15 3.2 ND ND ND ND ND NS ND ND ND ND ND NS 16 NS 12-09-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 03-02-16 47 0.79J ND ND ND ND NS ND ND ND ND ND NS 30 NS 05-31-16 16 ND ND ND ND ND NS ND ND ND ND ND NS 0.92J NS 9/1 - 9/2/16 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS 11-28-16 75 NS NS NS NS NS NS NS BRL NS BRL NS NS NS NS 02-28-17 85 NS NS NS NS NS NS NS BRL BRL BRL BRL NS 11 NS NA=Not Analyzed for Parameter DNE=Did Not Exist Bold Values exceed the NCAC 2L Groundwater Standard J=Estimated Value NS=Not Sampled BDL=Below Detection Limits ND=Not Detected E=Estimated concentration above calibration rangeBRL=Below Reporting Limits 4 of 4 PARAMETER UNITS DATE NCAC 15A:2L 2768B 2774 2760 2773 2755 2761 2779 2765 2765 2765 2800 Groundwater Influent Midfluent Effluent Standard Benzen ug/l 03-24-10 <0.5 NS NS NS NS NS NS 1.7 <0.5 <0.5 NS 06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 09-08-10 NS NS NS <0.5 NS NS NS 1 <0.5 <0.5 NS 12-10-10 NS NS NS <0.5 NS NS NS 0.97 <0.5 <0.5 NS 1 03-08-11 NS NS NS <0.5 NS NS <0.5 1.6 <0.5 <0.5 NS 06-30-11 NS NS NS <0.5 NS NS <0.5 8.4 <0.5 <0.5 NS 09-08-11 NS NS NS <0.5 NS NS <0.5 7.1 <0.5 <0.5 NS 12-09-11 NS NS NS <0.5 NS NS <0.5 3.3 <0.5 <0.5 NS 03-14-12 NS NS NS ND NS NS ND NS NS NS NS 06-07-12 NS NS NS ND NS NS ND NS NS NS NS 9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS 12-12-12 NS NS NS ND NS NS ND ND NS ND NS 03-14-13 ND NS NS ND NS NS ND ND NS ND NS 05-29-13 ND NS NS ND NS NS ND ND NS ND NS 09-10-13 ND NS NS ND NS NS ND ND NS ND NS 11-07-13 ND NS NS ND NS NS ND ND NS ND NS 09-20-14 ND NS NS ND NS NS ND ND ND ND NS 06-26-14 ND NS ND ND NS NS ND 0.33 ND ND NS 08-22-14 ND NS ND ND NS NS ND 0.54 ND ND NS 11-07-14 ND NS ND ND NS NS ND ND ND ND NS 03-04-15 NS NS ND ND NS NS ND ND ND ND NS 06-25-15 ND NS ND ND NS NS ND ND ND ND NS 09-23-15 ND NS ND ND NS NS ND ND ND ND NS 12-09-15 ND NS ND ND NS NS ND ND ND ND NS 02-29-16 ND ND ND ND NS NS ND ND ND ND NS 06-01-16 ND ND ND ND NS NS ND ND ND ND NS 09-02-16 ND ND ND ND NS NS ND ND ND ND NS 11-28-16 BRL BRL NS ND NS NS BRL ND BRL BRL NS 02-28-17 NS NS NS BRL NS NS NS BRL BRL BRL NS Toluen ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS 06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 600 03-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS 09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS 12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS 03-14-12 NS NS NS ND NS NS ND NS NS NS NS 06-07-12 NS NS NS ND NS NS ND NS NS NS NS 9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS 12-12-12 NS NS NS ND NS NS ND ND NS ND NS 03-14-13 ND NS NS ND NS NS ND ND NS ND NS 05-29-13 ND NS NS ND NS NS ND ND NS ND NS 09-10-13 ND NS NS ND NS NS ND ND NS ND NS 11-07-13 ND NS NS ND NS NS ND ND NS ND NS 03-20-14 ND NS NS ND NS NS ND ND ND ND NS 06-26-14 ND NS ND ND NS NS ND ND ND ND NS 08-22-14 ND NS ND ND NS NS ND ND ND ND NS 11-07-14 ND NS ND ND NS NS ND ND ND ND NS 03-04-15 NS NS ND ND NS NS ND ND ND ND NS 06-25-15 ND NS ND ND NS NS ND ND ND ND NS 09-23-15 ND NS ND ND NS NS ND ND ND ND NS 12-09-15 ND NS ND ND NS NS ND ND ND ND NS 02-29-16 ND ND ND ND NS NS ND ND ND ND NS 06-01-16 ND ND ND ND NS NS ND ND ND ND NS 09-02-16 ND ND ND ND NS NS ND ND ND ND NS 11-28-16 BRL BRL NS ND NS NS BRL ND BRL BRL NS 02-28-17 NS NS NS BRL NS NS NS BRL BRL BRL NS Ethylbenzen ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS 06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 600 03-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS 09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS 12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS 03-14-12 NS NS NS ND NS NS ND NS NS NS NS 06-07-12 NS NS NS ND NS NS ND NS NS NS NS 9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS 12-12-12 NS NS NS ND NS NS ND ND NS ND NS 03-14-13 ND NS NS ND NS NS ND ND NS ND NS 05-29-13 ND NS NS ND NS NS ND 0.55 NS ND NS 09-10-13 ND NS NS ND NS NS ND ND NS ND NS 11-07-13 ND NS NS ND NS NS ND ND NS ND NS 03-20-14 ND ND ND ND NS NS ND ND ND ND NS 06-26-14 ND NS ND ND NS NS ND ND ND ND NS 08-22-14 ND NS ND ND NS NS ND 0.26 ND ND NS 11-07-14 ND NS ND ND NS NS ND ND ND ND NS 03-04-15 NS NS ND ND NS NS ND ND ND ND NS 06-25-15 ND NS ND ND NS NS ND ND ND ND NS 09-23-15 ND NS ND ND NS NS ND ND ND ND NS 12-09-15 ND NS ND ND NS NS ND ND ND ND NS 02-29-16 ND ND ND ND NS NS ND ND ND ND NS 06-01-16 ND ND ND ND NS NS ND ND ND ND NS 09-02-16 ND ND ND ND NS NS ND ND ND ND NS 11-28-16 BRL BRL NS ND NS NS BRL ND BRL BRL NS 02-28-17 NS NS NS BRL NS NS NS BRL BRL BRL NS SUPPLY WELL Union Ridge Road, Burlington, North Carolina TABLE 4 Water Supply Well Analytical Results Harold Smith Grocery Incident #12913 Page 1 of 4 PARAMETER UNITS DATE NCAC 15A:2L 2768B 2774 2760 2773 2755 2761 2779 2765 2765 2765 2800 Groundwater Influent Midfluent Effluent Standard SUPPLY WELL Union Ridge Road, Burlington, North Carolina TABLE 4 Water Supply Well Analytical Results Harold Smith Grocery Incident #12913 Total Xylene ug/l 03-24-10 <3 NS NS NS NS NS NS <3 <3 <3 NS 06-24-10 NS NS NS <1.5 NS NS NS <1.5 <1.5 <1.5 NS 09-08-10 NS NS NS <1.5 NS NS NS <1.5 <1.5 <1.5 NS 12-10-10 NS NS NS <1.5 NS NS NS <1.5 <1.5 <1.5 NS 500 03-08-11 NS NS NS <1.5 NS NS <1.5 <1.5 <1.5 <1.5 NS 06-30-11 NS NS NS <1.5 NS NS <1.5 <3 <1.5 <1.5 NS 09-08-11 NS NS NS <1.5 NS NS <1.5 <3 <1.5 <1.5 NS 12-09-11 NS NS NS <1.5 NS NS <1.5 <3 <1.5 <1.5 NS 03-14-12 NS NS NS ND NS NS ND NS NS NS NS 06-07-12 NS NS NS ND NS NS ND NS NS NS NS 9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS 12-12-12 NS NS NS ND NS NS ND ND NS ND NS 03-14-13 ND NS NS ND NS NS ND ND NS ND NS 05-29-13 ND NS NS ND NS NS ND ND NS ND NS 09-10-13 ND NS NS ND NS NS ND ND NS ND NS 11-07-13 ND NS NS ND NS NS ND ND NS ND NS 03-20-14 ND ND ND ND NS NS ND ND ND ND NS 06-26-14 ND NS ND ND NS NS ND ND ND ND NS 08-22-14 ND NS ND ND NS NS ND ND ND ND NS 11-07-14 ND NS ND ND NS NS ND ND ND ND NS 03-04-15 NS NS ND ND NS NS ND ND ND ND NS 06-25-15 ND NS ND ND NS NS ND ND ND ND NS 09-23-15 ND NS ND ND NS NS ND ND ND ND NS 12-09-15 ND NS ND ND NS NS ND ND ND ND NS 02-29-16 ND ND ND ND NS NS ND ND ND ND NS 06-01-16 ND ND ND ND NS NS ND ND ND ND NS 09-02-16 ND ND ND ND NS NS ND ND ND ND NS 11-28-16 BRL BRL NS ND NS NS BRL ND BRL BRL NS 02-28-17 NS NS NS BRL NS NS NS BRL BRL BRL NS TOTAL BTE ug/l 03-24-10 BDL NS NS NS NS NS NS 1.7 BDL BDL NS 06-24-10 NS NS NS BDL NS NS NS BDL BDL BDL NS 09-08-10 NS NS NS BDL NS NS NS 1 BDL BDL NS 12-10-10 NS NS NS BDL NS NS NS 0.97 <0.5 <0.5 NS N/ 03-08-11 NS NS NS BDL NS NS BDL 1.6 BDL BDL NS 06-30-11 NS NS NS BDL NS NS BDL 8.4 BDL BDL NS 09-08-11 NS NS NS BDL NS NS BDL 7.1 BDL BDL NS 12-09-11 NS NS NS BDL NS NS BDL 3.3 BDL BDL NS 03-14-12 NS NS NS ND NS NS ND NS NS NS NS 06-07-12 NS NS NS ND NS NS ND NS NS NS NS 9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS 12-12-12 NS NS NS ND NS NS ND ND NS ND NS 03-14-13 ND NS NS ND NS NS ND ND NS ND NS 05-29-13 ND NS NS ND NS NS ND 0.55 NS ND NS 09-10-13 ND NS NS ND NS NS ND ND NS ND NS 11-07-13 ND NS NS ND NS NS ND ND NS ND NS 03-20-14 ND ND ND ND NS NS ND ND ND ND NS 06-26-14 ND NS ND ND NS NS ND 0.33 ND ND NS 08-22-14 ND NS ND ND NS NS ND 0.8 ND ND NS 11-07-14 ND NS ND ND NS NS ND ND ND ND NS 03-04-15 NS NS ND ND NS NS ND ND ND ND NS 06-25-15 ND NS ND ND NS NS ND ND ND ND NS 09-23-15 ND NS ND ND NS NS ND ND ND ND NS 12-09-15 ND NS ND ND NS NS ND ND ND ND NS 02-29-16 ND ND ND ND NS NS ND ND ND ND NS 06-01-16 ND ND ND ND NS NS ND ND ND ND NS 09-02-16 ND ND ND ND NS NS ND ND ND ND NS 11-28-16 BRL BRL NS ND NS NS BRL ND BRL BRL NS 02-28-17 NS NS NS BRL NS NS NS BRL BRL BRL NS Methyl Tertiary ug/l 03-24-10 22 NS NS NS NS NS NS 98 <5 <5 NS Butyl Ether 06-24-10 NS NS NS <1 NS NS NS <1 <1 <1 NS (MTBE)09-08-10 NS NS NS <1 NS NS NS 84.8 <1 <1 NS 12-10-10 NS NS NS <1 NS NS NS 100 <1 <1 NS 20 03-08-11 NS NS NS <0.5 NS NS <0.5 166 <0.5 <0.5 NS 06-30-11 NS NS NS <0.5 NS NS <0.5 125 <0.5 <0.5 NS 09-08-11 NS NS NS <0.5 NS NS <0.5 136 <0.5 <0.5 NS 12-09-11 NS NS NS <0.5 NS NS <0.5 150 <0.5 <0.5 NS 03-14-12 NS NS NS ND NS NS ND NS NS NS NS 06-07-12 NS NS NS ND NS NS ND NS NS NS NS 9/11-12/2012 NS NS NS ND NS NS ND 149 NS ND NS 12-12-12 NS NS NS ND NS NS ND 140 NS ND NS 03-14-13 ND NS NS ND NS NS ND 157 NS ND NS 05-29-13 ND NS NS ND NS NS ND 150 NS ND NS 09-10-13 ND NS NS ND NS NS ND 128 NS ND NS 11-07-13 ND NS NS ND NS NS ND 117 NS ND NS 03-20-14 ND ND ND 0.81 NS NS ND 140 ND 0.62 NS 06-26-14 ND NS ND 0.23 NS NS ND 120 ND ND NS 08-22-14 ND NS ND 0.18 NS NS ND 120 ND 0.28 NS 11-07-14 ND NS ND ND NS NS ND 130 ND ND NS 03-04-15 NS NS ND 0.79J NS NS ND 80 ND ND NS 06-25-15 ND NS ND 0.57J NS NS ND 57 ND ND NS 09-23-15 ND NS ND ND NS NS ND 70 ND ND NS 12-09-15 ND NS ND 3.1 NS NS ND 53 ND ND NS 02-29-16 ND ND ND 12 NS NS ND 60 ND ND NS 06-01-16 ND ND ND 4.6 NS NS ND 39 ND ND NS 09-02-16 ND ND ND ND NS NS ND 35 ND ND NS 11-28-16 BRL BRL NS 1.2 NS NS BRL 35 BRL BRL NS 02-28-17 NS NS NS 1.8 NS NS NS 29 BRL BRL NS Page 2 of 4 PARAMETER UNITS DATE NCAC 15A:2L 2768B 2774 2760 2773 2755 2761 2779 2765 2765 2765 2800 Groundwater Influent Midfluent Effluent Standard SUPPLY WELL Union Ridge Road, Burlington, North Carolina TABLE 4 Water Supply Well Analytical Results Harold Smith Grocery Incident #12913 Ethylen ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS Dibromid 06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS (EDB)09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 0.02 03-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS 09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS 12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS 03-14-12 NS NS NS ND NS NS ND NS NS NS NS 06-07-12 NS NS NS ND NS NS ND NS NS NS NS 9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS 12-12-12 NS NS NS ND NS NS ND ND NS ND NS 03-14-13 ND NS NS ND NS NS ND ND NS ND NS 05-29-13 ND NS NS ND NS NS ND ND NS ND NS 09-10-13 ND NS NS ND NS NS ND ND NS ND NS 11-07-13 ND NS NS ND NS NS ND ND NS ND NS 03-20-14 ND ND ND ND NS NS ND ND ND ND NS 06-26-14 ND NS ND ND NS NS ND ND ND ND NS 08-22-14 ND NS ND ND NS NS ND ND ND ND NS 11-07-14 ND NS ND ND NS NS ND ND ND ND NS 03-04-15 ND NS ND ND NS NS ND ND ND ND NS 06-25-15 ND NS ND ND NS NS ND ND ND ND NS 09-23-15 ND NS ND ND NS NS ND ND ND ND NS 12-09-15 ND NS ND ND NS NS ND ND ND ND NS 02-29-16 ND ND ND ND NS NS ND ND ND ND NS 06-01-16 ND ND ND ND NS NS ND ND ND ND NS 09-02-16 ND ND ND ND NS NS ND ND ND ND NS 11-28-16 BRL BRL NS ND NS NS BRL ND BRL BRL NS 02-28-17 NS NS NS BRL NS NS NS BRL BRL BRL NS Isopropyl Ether ug/l 03-24-10 11 NS NS NS NS NS NS 130 <5 <5 NS (IPE)06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 09-08-10 NS NS NS <0.5 NS NS NS 104 <0.5 <0.5 NS 12-10-10 NS NS NS <0.5 NS NS NS 150 <0.5 <0.5 NS 70 03-08-11 NS NS NS <0.5 NS NS <0.5 260 <0.5 <0.5 NS 06-30-11 NS NS NS <0.5 NS NS <0.5 191 <0.5 <0.5 NS 09-08-11 NS NS NS <0.5 NS NS <0.5 206 <0.5 NS 12-09-11 NS NS NS <0.5 NS NS <0.5 178 <0.5 <0.5 NS 03-14-12 NS NS NS ND NS NS ND NS NS NS NS 06-07-12 NS NS NS ND NS NS ND NS NS NS NS 9/11-12/2012 NS NS NS ND NS NS ND 149 NS ND NS 12-12-12 NS NS NS ND NS NS ND 150 NS ND NS 03-14-13 ND NS NS ND NS NS ND 159 NS ND NS 05-29-13 ND NS NS ND NS NS ND 168 NS ND NS 09-10-13 ND NS NS 0.96 NS NS ND 183 NS ND NS 11-07-13 ND NS NS 1.96 NS NS ND 138 NS ND NS 03-20-14 ND ND ND 0.67 NS NS ND 140 ND 0.2 NS 06-26-14 ND NS ND ND NS NS ND 160 ND ND NS 08-22-14 ND NS ND ND NS NS ND 150 ND ND NS 11-07-14 ND NS ND ND NS NS ND 160 ND ND NS 03-04-15 NS NS ND ND NS NS ND 100 ND ND NS 06-25-15 ND NS ND ND NS NS ND 68 ND ND NS 09-23-15 ND NS ND ND NS NS ND 74 ND ND NS 12-09-15 ND NS ND 2.2 NS NS ND 75 ND ND NS 02-29-16 ND ND ND 18 NS NS ND 76 ND ND NS 06-01-16 ND ND ND 5.8 NS NS ND 56 ND ND NS 09-02-16 ND ND ND ND NS NS ND 37 ND ND NS 11-28-16 BRL BRL NS 0.79 NS NS BRL 38 BRL BRL NS 02-28-17 NS NS NS 2 NS NS NS 33 BRL BRL NS 1,2- Dichloroethan ug/l 03-24-10 <1 NS NS NS NS NS NS 6.2 <1 <1 NS 06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 09-08-10 NS NS NS <0.5 NS NS NS 15.7 <0.5 <0.5 NS 12-10-10 NS NS NS <0.5 NS NS NS 19 <0.5 <0.5 NS 0.4 03-08-11 NS NS NS <0.5 NS NS <0.5 33.1 <0.5 <0.5 NS 06-30-11 NS NS NS <0.5 NS NS <0.5 28 <0.5 <0.5 NS 09-08-11 NS NS NS <0.5 NS NS <0.5 27.4 <0.5 <0.5 NS 12-09-11 NS NS NS <0.5 NS NS <0.5 26.6 <0.5 <0.5 NS 03-14-12 NS NS NS ND NS NS ND NS NS NS NS 06-07-12 NS NS NS ND NS NS ND NS NS NS NS 9/11-12/2012 NS NS NS ND NS NS ND 20.8 NS ND NS 12-12-12 NS NS NS 0.19J NS NS ND 23 NS ND NS 03-14-13 ND NS NS ND NS NS ND 31.5 NS ND NS 05-29-13 ND NS NS ND NS NS ND 25.9 NS ND NS 09-10-13 ND NS NS ND NS NS ND 25.7 NS ND NS 11-07-13 ND NS NS ND NS NS ND 20.1 NS ND NS 03-20-14 ND ND ND 0.44 NS NS ND 20 ND ND NS 06-26-14 ND NS ND 0.31 NS NS ND 24 ND ND NS 08-22-14 ND NS ND ND NS NS ND 24 ND ND NS 11-07-14 ND NS ND ND NS NS ND 27 ND ND NS 03-04-15 NS NS ND ND NS NS ND 16 ND ND NS 06-25-15 ND NS ND ND NS NS ND 12 ND ND NS 09-23-15 ND NS ND ND NS NS ND 13 ND ND NS 12-09-15 ND NS ND 0.94 NS NS ND 10 ND ND NS 02-29-16 ND ND ND 2 NS NS ND 9.2 ND ND NS 06-01-16 ND ND ND 1 NS NS ND 6.9 ND ND NS 09-02-16 ND ND ND ND NS NS ND 6.4 ND ND NS 11-28-16 BRL BRL NS ND NS NS BRL 6.1 BRL BRL NS 02-28-17 NS NS NS 0.59 NS NS NS 5.2 BRL BRL NS Page 3 of 4 PARAMETER UNITS DATE NCAC 15A:2L 2768B 2774 2760 2773 2755 2761 2779 2765 2765 2765 2800 Groundwater Influent Midfluent Effluent Standard SUPPLY WELL Union Ridge Road, Burlington, North Carolina TABLE 4 Water Supply Well Analytical Results Harold Smith Grocery Incident #12913 1,2-Dichloropropan ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS 06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 0.6 03-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS 09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS 12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS 03-14-12 NS NS NS ND NS NS ND NS NS NS NS 06-07-12 NS NS NS ND NS NS ND NS NS NS NS 9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS 12-12-12 NS NS NS ND NS NS ND ND NS ND NS 03-14-13 ND NS NS ND NS NS ND ND NS ND NS 05-29-13 ND NS NS ND NS NS ND ND NS ND NS 09-10-13 ND NS NS ND NS NS ND ND NS ND NS 11-07-13 ND NS NS ND NS NS ND ND NS ND NS 03-20-14 ND ND ND ND NS NS ND ND ND ND NS 06-26-14 ND NS ND ND NS NS ND ND ND ND NS 08-22-14 ND NS ND ND NS NS ND ND ND ND NS 11-07-14 ND NS ND ND NS NS ND ND ND ND NS 03-04-15 NS NS ND ND NS NS ND ND ND ND NS 06-25-15 ND NS ND ND NS NS ND ND ND ND NS 09-23-15 ND NS ND ND NS NS ND ND ND ND NS 12-09-15 ND NS ND ND NS NS ND ND ND ND NS 02-29-16 ND ND ND ND NS NS ND ND ND ND NS 06-01-16 ND ND ND ND NS NS ND ND ND ND NS 09-02-16 ND ND ND ND NS NS ND ND ND ND NS 11-28-16 BRL BRL NS ND NS NS BRL ND BRL BRL NS 02-28-17 NS NS NS BRL NS NS NS BRL BRL BRL NS Chloroform 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS 06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 03-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 70 06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS 09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS 12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS 03-14-12 NS NS NS ND NS NS ND NS NS NS NS 06-07-12 NS NS NS ND NS NS ND NS NS NS NS 9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS 12-12-12 NS NS NS ND NS NS ND ND NS ND NS 03-14-13 ND NS NS ND NS NS ND ND NS ND NS 05-29-13 ND NS NS ND NS NS ND ND NS ND NS 09-10-13 ND NS NS ND NS NS ND ND NS ND NS 11-07-13 ND NS NS ND NS NS ND ND NS ND NS 03-20-14 ND ND ND ND NS NS ND ND ND ND NS 06-26-14 ND NS ND ND NS NS ND 1.1 ND ND NS 08-22-14 ND NS ND ND NS NS ND ND ND 1.6 NS 11-07-14 ND NS ND ND NS NS ND ND ND ND NS 03-04-15 NS NS ND ND NS NS ND ND ND ND NS 06-25-15 ND NS ND ND NS NS ND ND ND ND NS 09-23-15 ND NS ND ND NS NS ND ND ND ND NS 12-09-15 ND NS ND ND NS NS ND ND ND ND NS 02-29-16 ND ND ND ND NS NS ND ND ND ND NS 06-01-16 ND ND ND ND NS NS ND ND ND ND NS 09-02-16 ND ND ND ND NS NS ND ND ND ND NS 11-28-16 BRL BRL NS ND NS NS BRL ND BRL BRL NS 02-28-17 NS NS NS BRL NS NS NS BRL BRL BRL NS Chloromethan 02-28-17 NS NS NS BRL NS NS NS BRL BRL 0.8 NS 3 BRL=Below reporting limits NA=Not analyzed for this parameter J=Estimated Value NS=Not Sampled Page 4 of 4 APPENDIX A Standard Field Procedures: Revision 10.3 Page 1 Pyramid Environmental & Engineering, P.C. Revision date 11-11-2016 Standard Field Procedures Pyramid Environmental & Engineering, P.C. ________________________________________________________________________ 1.0 Equipment Decontamination Equipment decontamination is essential to assure representative environmental samples are collected and to eliminate the potential for cross contamination between sample points. Pyramid strives to clean all field equipment prior to leaving the office; however, field decontamination is still required on most projects. The procedures for decontamination of water level probes, hand augers, sampling probes and trowels, and other field equipment are listed below. 1.1 EPA Region IV Decontamination Procedures Drilling and soil sampling equipment is decontaminated prior to each use using a pressure washer or steam cleaner. Reusable sampling equipment (hand augers, sampling probes, trowels, split spoon samplers, water sampling equipment, etc.…) are decontaminated using the general procedure described below.  Wash with non-phosphate detergent and water, brush to remove particulate matter.  Rinse with tap water.  Rinse with 10 percent nitric acid solution (only if sampling for metals)  Rinse with deionized water.  Rinse with pesticide-grade isopropyl alcohol.  Rinse with deionized water.  Air-dry as long as possible. The level of decontamination used is appropriate to the analytical parameters selected and the material of the sampling device being used for sampling. For example, if metals analyses are required, then the 10 % nitric acid solution is used for decontamination of stainless steel equipment. Pyramid uses deionized or distilled water for decontamination. Equipment that is not used immediately after decontamination is wrapped in aluminum foil prior to storage. 2.0 Soil Borings & Sampling: 2.1 Soil Borings Soil borings are used by Pyramid to characterize the subsurface at many sites. The borings provide information concerning soil types and density, depth to refusal, depth to bedrock, organic vapors that may be present, and can be used to obtain samples for laboratory analysis. Pyramid conducts borings in several different ways, using hand augers, Direct Push equipment (Geoprobe), sample probes, split-spoon samplers (ASTM D 1586-84), auger drilling, air drilling, and Vibro-Core. The following procedures are used by Pyramid Environmental when performing soil borings: 1. Soil boring locations are chosen, and the utility locating service is called to mark all public utilities. Pyramid also located private utilities at many project sites using Pyramid locating equipment or a private utility locating service. Standard Field Procedures: Revision 10.3 Page 2 Pyramid Environmental & Engineering, P.C. Revision date 11-11-2016 2. Down hole drilling equipment is cleaned prior to use and between borings using pressure washing or steam cleaning. Additional decontamination procedures in section 1.1 are used for quality assurance for sampling tools such as split spoons or Direct-Push Points. 3. Soil borings are advanced using direct-push, drilling rigs, hand augers, or other appropriate means. 4. Soil samples are normally collected at a minimum of 5-foot intervals. Each sample is divided into two parts. Soil samples for laboratory analyses are jarred from the initial sample volume. The remaining soil is stored in a sealed container for headspace analysis with an organic vapor analyzer (OVA). 5. After screening the soil with the field instruments, each soil sample is described by the field geologist and a geologic description is recorded in project documentation. 6. Soils are typically described in the field by the project geologist or soil scientist and are classified according to the Unified Soil Classification System (ASTM D 2488-84). 7. Soil samples selected for laboratory analysis are placed in properly prepared, laboratory supplied containers and immediately packed in a cooler on ice. Sample custody is maintained using standard chain-of-custody procedures through delivery to the analytical laboratory. 8. Soil borings, which are not completed as monitor wells are grouted using a Portland cement, bentonite, or backfilled with soil cuttings. 9. Where appropriate, soil cuttings are spread near the soil boring or well site in most instances. In rare instances, drill cuttings will be containerized and disposed off-site after waste determination has been made. 2.2 Headspace Screening Soil samples are routinely screened for volatile organic compounds (VOCs) which may be an indication of organic or petroleum hydrocarbon contamination. The typical screening procedure includes immediately transferring the soil from the sampling devices to a sealed container (sealed plastic bag). The soil container is filled approximately halfway with soil and sealed. This creates headspace above the soil in which VOCs may accumulate. The container is allowed to stand for 5 to 15 minutes for the VOCs to equilibrate in the headspace of the container. The headspace of the container is then screened using a calibrated organic vapor analyzer (PID or FID). The screening is conducted by cracking the seal only enough to allow insertion of the probe into the headspace so as not to dilute the sample. In most cases where the contaminant of concern includes volatile organics, the highest or “Peak “ field screening result is documented for each sample. The soil samples showing the highest reading from each boring are typically selected for laboratory analysis. Standard Field Procedures: Revision 10.3 Page 3 Pyramid Environmental & Engineering, P.C. Revision date 11-11-2016 2.3 Soil Sample Collection for Laboratory Analysis After the targeted depth has been reached, soil samples are collected using a variety of sampling devices. Soil sample devices used include split-spoons, stainless steel hand augers, stainless steel sampling scoops, and directly from the center of the excavator bucket. The sample technician uses appropriate disposable sampling gloves, which are changed between samples to avoid cross-contamination of samples. Each sampling device is decontaminated prior to use. Only laboratory provided containers are used for sample collection. Samples are collected in accordance with the preservation methods required by the requested analytical method. Samples are handled as little as possible and preserved in the field as specified for the analytical method. The samples are stored and transported to the laboratory in an insulated cooler chilled to approximately 4 degrees C. The samples are labeled with a minimum of the following information: project name or number, sampler name, date collected, sample number, and analysis requested. Sample custody is maintained using standard chain-of-custody procedures through delivery to the analytical laboratory. Notes of the sampling events are recorded in bound field notebooks. 2.4 Sediment Sample Collection for Laboratory Analysis Near surface sediment may be present in a surface water stream or dry intermittent stream bed. Sediment samples are typically soil related samples and may be collected with a variety of sampling tools. Pyramid will use stainless steel samplers which have been decontaminated according to the procedure detailed in section 1.1 of this document. After the sediment samples are collected, the location, depth, conditions, and sample composition are documented in the project records. The samples will be screened in the field to detect volatile organic vapors and visually examined for contamination. Sediment samples will be preserved in laboratory prepared containers in accordance with sample preservation recommendation of the analytical laboratory. Samples are handled as little as possible and preserved in the field as specified for the analytical method. The samples are stored and transported to the laboratory in an insulated cooler chilled to approximately 4 degrees C. The samples are labeled with a minimum of the following information: project name or number, sampler name, date collected, sample number, and analysis requested. Sample custody is maintained using standard chain-of-custody procedures through delivery to the analytical laboratory. Documentation of the sampling events are recorded in bound field notebooks. 3.0 Direct Push Sampling Procedures Direct Push sampling techniques have been used at many sites to collect soil and groundwater samples rapidly and inexpensively. Track mounted direct push rigs can access hard to reach areas and allow borings and monitoring wells to be installed. Pyramid has used this technology to the benefit of our clients at many project sites. For soil sampling, typically, the direct push steel drive tube is decontaminated using a pressure washer, and a new plastic sample liner is inserted in the steel drive tube to collect soil samples. If necessary, the stainless-steel sampling tube is decontaminated using Region IV decontamination procedures presented in section 1.1. The soil samples are collected in new polyethylene sample tubes within the steel drive tube. The soil samples are then extracted from the polyethylene liner and preserved as required for the appropriate laboratory analysis. Standard Field Procedures: Revision 10.3 Page 4 Pyramid Environmental & Engineering, P.C. Revision date 11-11-2016 For Groundwater sampling, a steel probe with a retractable screen section and tubing are driven to depth and the screened section is opened to allow groundwater to enter the tubing. The water samples are withdrawn using new polyethylene tubing with either a decontaminated stainless-steel check ball, or peristaltic pump. The groundwater sample is placed directly into the appropriate laboratory containers and sealed immediately. To prevent cross contamination of samples, new disposable tubing is used for each groundwater sample point. Disposable nitrile gloves are worn by field personnel during development and groundwater sampling, and gloves are changed between samples. Groundwater sampling procedures are detailed more in section 5.0., as appropriate for each analytical method. 4.0 Monitoring Well Installation Groundwater monitoring wells are installed in many subsurface environments; sedimentary, Piedmont saprolite, and mountain terrains to list a few. Formations encountered include unconsolidated and consolidated sediments, saprolitic and weathered rock formations, and bedrock. Groundwater monitoring wells provide a stable sampling point at discrete intervals within the confined or unconfined aquifers. Monitoring wells are installed for a number of reasons, and are typically installed as 1-inch, 2-inch, 4-inch, or 6-inch diameter wells. Construction may be of PVC or other appropriate materials. The following procedures are used by Pyramid when performing borings and monitoring well installations.  If required, monitoring well permits are obtained from the State, County, or City.  Boring and monitoring well locations are chosen, and utilities are marked by the public utility locating company. As needed, the drill locations may also be scanned for utilities using a private utility locating company.  In selecting a drill site, care is taken to avoid overhead power lines, and subsurface utilities whenever possible.  Down hole drilling equipment is decontaminated prior to use and between borings.  Borings are advanced using direct-push, drilling rigs, hand augers, solid-stem augers, hollow-stem augers, air rotary drilling, or air hammer drilling.  Soil samples are normally collected at a minimum of 5-foot intervals. Each sample is divided into two parts. Soil samples for laboratory analyses are jarred from the initial sample volume. The remaining soil is stored in a sealed container for headspace analysis with an organic vapor analyzer (OVA).  After screening the soil with the field instruments, each soil sample is described by the field geologist and a geologic description is recorded in the field notes. Type II monitoring wells are usually installed using 2-inch diameter schedule 40 PVC riser and 2- inch, 0.010-inch machine slotted well screen. The screened interval varies with the purpose of the well, and well details are presented with the boring logs. Type III wells are usually installed as double cased wells to monitor the deeper portions of the aquifer. The first casing is usually a 6-inch diameter casing drilled to bedrock or an appropriate depth within the saprolite. The 6-inch diameter casing is then set and grouted in the borehole. After the cement grout has set for 12 to 24-hours, the borehole is completed to the desired depth using air rotary or an air hammer drilling. The Type III monitor well is usually constructed of 2-inch diameter SCH 40 PVC casing and 2-inch diameter SCH 40 PVC 0.010-inch slotted well screen. Standard Field Procedures: Revision 10.3 Page 5 Pyramid Environmental & Engineering, P.C. Revision date 11-11-2016 In most applications, a sand filter pack of #2 well sand (or appropriately sized well sand) is typically installed to a level of 2 feet above the top of the screen in each well. A minimum 2- foot thick bentonite seal is usually placed on top of the filter pack and hydrated with deionized or distilled water. The remaining annular space of a typical well is backfilled to grade with a Portland cement/bentonite grout. In monitoring wells where the water table is close to surface, the amount of sand above the screen and bentonite will be reduced to allow for a minimum of 2 –3 feet of cement grout in the well bore. At the surface, each well is usually secured with a locking cap and a steel well protector set in a 2 by 2 foot concrete pad. In some cases, stick-up well protectors are used to secure the well and allow the well to be more easily located in wooded or open areas. Each groundwater monitoring well is developed by surging, pumping, or bailing to remove sediment before sampling. Water removed during development is managed according to regulatory standards. 5.0 Water Sampling Procedures Pyramid relies on water sampling as a primary method for assessment of subsurface conditions. Water sampling typically includes sampling groundwater from monitoring wells, supply wells, surface water bodies, waste pits, sumps, etc. The following provides typical sampling procedures for the major sample types. 5.1 Monitoring Wells Prior to sampling each monitor well, depth to product/groundwater and total well depth are measured using a properly decontaminated electric interface probe. This information is recorded in the field record and the volume of the water in the well casing is calculated. To purge stagnant water from each monitor well, five well casing volumes of water are removed from each well, or until the field parameters pH, conductivity, dissolved oxygen, and temperature have stabilized. If the water in the monitoring well is removed until the well is dry, then the well is sampled thereafter. Water removed from wells during purging is managed in accordance with regulatory guidance. Depending on project requirements, temperature, pH, specific conductance, dissolved oxygen, and other parameters may be measured prior to sampling. Groundwater samples are typically collected using a new disposable polyethylene bailer and a new length of nylon cord. To prevent cross contamination of samples between wells, a new disposable bailer is used for each well. A new pair of disposable gloves is worn by field personnel during purging and sampling, and is changed between wells. In the case of small diameter monitoring wells or direct-push water samples, water samples may be collected using a peristaltic pump and new polyethylene tubing. Another method is to use a segment of new polyethylene tubing and a stainless-steel check ball to create a “Tube Bailer”. Groundwater samples selected for laboratory analysis are placed in properly prepared, laboratory supplied containers and immediately preserved in a cooler on ice. Samples are maintained under standard chain-of-custody procedures from sample collection through laboratory analysis. Standard Field Procedures: Revision 10.3 Page 6 Pyramid Environmental & Engineering, P.C. Revision date 11-11-2016 5.2 Water Supply Well Sampling Procedures Prior to sampling each water supply well, the well owner is contacted to provide access to the well. The well owner is interviewed to find the faucet closest to the well for sampling. If there are no faucets located on the well, then water from an outside faucet is usually sampled. If there are no outside faucets available, then the water samples are collected from an inside faucet. The location of the sample is recorded in the field book. The owner is interviewed to see if there is a chlorination system on the well, or if the well has been recently chlorinated. Recent chlorination could affect the laboratory detection limits. In most cases, the samples are preserved using sodium thiosulfate or ascorbic acid to remove the interactions of chlorine, which may be present in the samples. To purge stagnant water from the water supply well system, the faucet is allowed to run on full stream for a minimum of 15 minutes. The aerator is removed from the tap if one is present. Water removed from wells during purging is managed according to regulatory standards. Supply well samples are collected using appropriate laboratory prepared containers for each analysis. The analytical methods selected will vary with the contaminant of interest. To prevent cross contamination of samples between wells, disposable latex gloves are worn by field personnel during purging and sampling and are changed between wells. It is possible that samples may be required at several places within the water supply system. The samples will be collected accordingly and labeled to show the source and location sampled. Supply well samples selected for laboratory analysis are placed in properly prepared, laboratory supplied containers and immediately packed in a cooler on wet ice, and chilled to approximately 4 degrees Celsius. Samples are maintained under strict control using standard chain-of-custody procedures through laboratory analysis. 5.3 Surface Water Sampling Surface water samples are obtained using several techniques including use of sample bailers, sample scoops, from boats, bridges, or actually wading into a stream. Caution should always be used when sampling surface water to ensure that the water collected is representative of the conditions. Since stream or open water sampling is transient, careful documentation of the site conditions is required. In many studies, additional samples from upstream and downstream of the desired sample point are required. Surface water sampling must be planned to reflect the desired conditions during sampling. The general procedures are similar to the supply well sampling procedures detailed above. Prepare the appropriate laboratory prepared containers for each analysis. The analytical methods selected will vary with the contaminant of interest. To prevent cross contamination of samples between samples, disposable latex gloves are worn by field personnel during purging and sampling and are changed between samples. It is possible that samples may be required at several places along the stream to check for influences of up-stream facilities. Standard Field Procedures: Revision 10.3 Page 7 Pyramid Environmental & Engineering, P.C. Revision date 11-11-2016 The samples will be collected accordingly and labeled to show the source and location sampled. Sample will always be collected upstream of the area disturbed by the person sampling the stream. Surface water samples selected for laboratory analysis are placed in properly prepared, laboratory supplied containers and immediately packed in a cooler on ice. Samples are maintained under strict control using standard chain-of-custody procedures through laboratory analysis. 6.0 Quality Assurance / Quality Control The decontamination procedures listed above have been implemented on many sites with excellent results. The procedures are often verified by an appropriate use of the following environmental sample “Blanks”. Trip Blanks The trip blank (or travel blanks) are often used to verify that the sample containers are not impacted during shipping, and verify that the source of the glassware is not the source of contamination. The trip blanks are preserved de-ionized water, collected in the laboratory, and shipped with the sample containers to the site. The trip blank remains in the cooler and is shipped back to the laboratory with the environmental samples. The trip blank is usually analyzed for volatile organics, which correspond to the target analyses. Field Blanks Field Blanks are quality assurance samples which are collected in the field to represent the conditions present at the time the samples are collected. For water samples, the laboratory containers are opened and filled in the field using de-ionized (or distilled) water from a known source. The samples then travel to the laboratory with the other samples for analysis. Equipment Blanks Equipment blanks are used to verify whether the decontamination procedures used for the sample equipment or the new equipment added any contaminants to the sample during collection. If a non-disposable sampling device is used (such as a sampling treir, scoop, hand auger, Teflon bailer, etc…), then the decontamination of the sampling device is usually verified using an equipment blank. The equipment blank is collected using de-ionized (or distilled) water from a known source. The equipment is cleaned, and allowed to dry, the water is poured over or through the equipment, and collected in the appropriate sample containers. The equipment blank samples are preserved with the other environmental samples, and shipped for analyses for the target parameters. Duplicate Samples Duplicate Samples are used to verify the sampling procedures and laboratory analysis variability. The duplicate samples may be collected from waste streams, soil, or groundwater. These samples are collected and sent to the laboratory as a blind sample to have maximum effectiveness. Samples are generally analyzed for the same analytical methods as the actual environmental sample for direct comparison. Duplicate samples may also be split between two different laboratories to provide verification of laboratory detection limits or quality process verification. APPENDIX B This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Case Narrative 03/10/2017 Pyramid Environmental, Inc Mika Trifunovic PO Box 16265 Greensboro, NC 27416-0265 Project: Harold Smith Lab Submittal Date: 03/03/2017 Prism Work Order: 7030063 Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. VP Laboratory Services Reviewed ByAngela D. Overcash Terri W. Cole For Angela D. Overcash Project Manager Data Qualifiers Key Reference: D RPD value outside of the control limits. L1 LCS recovery outside of the QC limits. LCSD recovery within the limits. No further action taken. Method Detection LimitMDL Below Reporting LimitBRL Relative Percent DifferenceRPD *Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 30 Sample Receipt Summary 03/10/2017 Prism Work Order: 7030063 Client Sample ID MatrixLab Sample ID Date Sampled Date Received 7030063-01 02/28/17MW-1A 03/03/17Water 7030063-02 02/28/17MW-10 03/03/17Water 7030063-03 02/28/17MW-11 03/03/17Water 7030063-04 02/28/17MW-12 03/03/17Water 7030063-05 02/28/17MW-13 03/03/17Water 7030063-06 02/28/17MW-15A 03/03/17Water 7030063-07 02/28/17SW 2773 03/03/17Water 7030063-08 02/28/17SW-2765 03/03/17Water 7030063-09 02/28/172765 Mid 03/03/17Water 7030063-10 02/28/172765 Eff 03/03/17Water Samples were received in good condition at 4.6 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 30 Client ID ResultParameterMethod UnitsPrism ID Prism Work Order: 7030063 03/10/2017 Summary of Detections 470 ug/L7030063-01 MW-1A 1,2,4-Trimethylbenzene SM6200 B 11 ug/L7030063-01 MW-1A 1,2-Dichloroethane SM6200 B 120 ug/L7030063-01 MW-1A 1,3,5-Trimethylbenzene SM6200 B 4.9 ug/L7030063-01 MW-1A 4-Isopropyltoluene SM6200 B 67 ug/L7030063-01 MW-1A Benzene SM6200 B 38 ug/L7030063-01 MW-1A Ethylbenzene SM6200 B 170 ug/L7030063-01 MW-1A Isopropyl Ether SM6200 B 13 ug/L7030063-01 MW-1A Isopropylbenzene (Cumene)SM6200 B 77 ug/L7030063-01 MW-1A m,p-Xylenes SM6200 B 20 ug/L7030063-01 MW-1A Methyl-tert-Butyl Ether SM6200 B 85 ug/L7030063-01 MW-1A Naphthalene SM6200 B 7.5 ug/L7030063-01 MW-1A n-Butylbenzene SM6200 B 20 ug/L7030063-01 MW-1A n-Propylbenzene SM6200 B 100 ug/L7030063-01 MW-1A o-Xylene SM6200 B 7.7 ug/L7030063-01 MW-1A sec-Butylbenzene SM6200 B 0.78 ug/L7030063-01 MW-1A Styrene SM6200 B 1.5 ug/L7030063-01 MW-1A tert-Butylbenzene SM6200 B 4.8 ug/L7030063-01 MW-1A Toluene SM6200 B 180 ug/L7030063-01 MW-1A Xylenes, total SM6200 B 0.60 ug/L7030063-05 MW-13 sec-Butylbenzene SM6200 B 35 ug/L7030063-06 MW-15A 1,2,4-Trimethylbenzene SM6200 B 8.8 ug/L7030063-06 MW-15A 1,3,5-Trimethylbenzene SM6200 B 37 ug/L7030063-06 MW-15A Ethylbenzene SM6200 B 3.0 ug/L7030063-06 MW-15A Isopropylbenzene (Cumene)SM6200 B 69 ug/L7030063-06 MW-15A m,p-Xylenes SM6200 B 11 ug/L7030063-06 MW-15A Naphthalene SM6200 B 3.6 ug/L7030063-06 MW-15A n-Propylbenzene SM6200 B 56 ug/L7030063-06 MW-15A o-Xylene SM6200 B 10 ug/L7030063-06 MW-15A Toluene SM6200 B 130 ug/L7030063-06 MW-15A Xylenes, total SM6200 B 0.59 ug/L7030063-07 SW 2773 1,2-Dichloroethane SM6200 B 2.0 ug/L7030063-07 SW 2773 Isopropyl Ether SM6200 B 1.8 ug/L7030063-07 SW 2773 Methyl-tert-Butyl Ether SM6200 B 5.2 ug/L7030063-08 SW-2765 1,2-Dichloroethane SM6200 B 33 ug/L7030063-08 SW-2765 Isopropyl Ether SM6200 B 29 ug/L7030063-08 SW-2765 Methyl-tert-Butyl Ether SM6200 B 0.80 ug/L7030063-10 2765 Eff Chloromethane SM6200 B This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 30 Laboratory Report 03/10/2017 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Sample Matrix: Water Client Sample ID: MW-1A Prism Sample ID: 7030063-01 Prism Work Order: 7030063 Time Collected: 02/28/17 15:10 Time Submitted: 03/03/17 15:15 Volatile Organic Compounds by GC/MS BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.111,1,1,2-Tetrachloroethane BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.0611,1,1-Trichloroethane BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.0361,1,2,2-Tetrachloroethane BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.0661,1,2-Trichloroethane BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.0831,1-Dichloroethane BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.0831,1-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.0511,1-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.401,2,3-Trichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.141,2,3-Trichloropropane BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.131,2,4-Trichlorobenzene 470 SM6200 B P7C0120105.0 3/8/17 21:11 KDMug/L 0.541,2,4-Trimethylbenzene BRL SM6200 B P7C012012.0 3/7/17 19:08 KDMug/L 0.171,2-Dibromo-3-chloropropane BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.0511,2-Dibromoethane BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.0761,2-Dichlorobenzene 11 SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.0661,2-Dichloroethane BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.111,2-Dichloropropane 120 SM6200 B P7C0120105.0 3/8/17 21:11 KDMug/L 0.761,3,5-Trimethylbenzene BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.0541,3-Dichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.0431,3-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.0501,4-Dichlorobenzene BRL SM6200 B P7C012012.0 3/7/17 19:08 KDMug/L 0.112,2-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.0662-Chlorotoluene BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.0504-Chlorotoluene 4.9 SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.0894-Isopropyltoluene BRL SM6200 B P7C01201103/7/17 19:08 KDMug/L 0.31Acetone 67 SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.048Benzene BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.057Bromobenzene BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.14Bromochloromethane BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.062Bromodichloromethane BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.040Bromoform BRL SM6200 B P7C012011.0 3/7/17 19:08 KDMug/L 0.18Bromomethane BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.11Carbon Tetrachloride BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.062Chlorobenzene BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.22Chloroethane BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.076Chloroform BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.079Chloromethane BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.056cis-1,2-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.079cis-1,3-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.081Dibromochloromethane BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.065Dibromomethane BRL SM6200 B P7C012011.0 3/7/17 19:08 KDMug/L 0.11Dichlorodifluoromethane BRL SM6200 B P7C012012003/7/17 19:08 KDMug/L 27Ethanol This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 30 Laboratory Report 03/10/2017 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Sample Matrix: Water Client Sample ID: MW-1A Prism Sample ID: 7030063-01 Prism Work Order: 7030063 Time Collected: 02/28/17 15:10 Time Submitted: 03/03/17 15:15 38 SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.061Ethylbenzene BRL SM6200 B P7C012012.0 3/7/17 19:08 KDMug/L 0.16Hexachlorobutadiene 170 SM6200 B P7C0120105.0 3/8/17 21:11 KDMug/L 0.50Isopropyl Ether 13 SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.054Isopropylbenzene (Cumene) 77 SM6200 B P7C012011.0 3/7/17 19:08 KDMug/L 0.12m,p-Xylenes BRL SM6200 B P7C012011.0 3/7/17 19:08 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL SM6200 B P7C012015.0 3/7/17 19:08 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL SM6200 B P7C012011.0 3/7/17 19:08 KDMug/L 0.078Methyl Isobutyl Ketone BRL SM6200 B P7C012012.0 3/7/17 19:08 KDMug/L 0.083Methylene Chloride 20 SM6200 B P7C012011.0 3/7/17 19:08 KDMug/L 0.042Methyl-tert-Butyl Ether 85 SM6200 B P7C012011.0 3/7/17 19:08 KDMug/L 0.19Naphthalene 7.5 SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.076n-Butylbenzene 20 SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.087n-Propylbenzene 100 SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.044o-Xylene 7.7 SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.076sec-Butylbenzene 0.78 SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.047Styrene 1.5 SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.088tert-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.098Tetrachloroethylene 4.8 SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.044Toluene BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.070trans-1,2-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.12trans-1,3-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.078Trichloroethylene BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.062Trichlorofluoromethane BRL SM6200 B P7C012015.0 3/7/17 19:08 KDMug/L 0.060Vinyl acetate BRL SM6200 B P7C012010.50 3/7/17 19:08 KDMug/L 0.097Vinyl chloride 180 SM6200 B P7C012011.5 3/7/17 19:08 KDMug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-13086 %4-Bromofluorobenzene 70-13089 %Dibromofluoromethane 70-13084 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 30 Laboratory Report 03/10/2017 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Sample Matrix: Water Client Sample ID: MW-10 Prism Sample ID: 7030063-02 Prism Work Order: 7030063 Time Collected: 02/28/17 14:10 Time Submitted: 03/03/17 15:15 Volatile Organic Compounds by GC/MS BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.111,1,1,2-Tetrachloroethane BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.0611,1,1-Trichloroethane BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.0361,1,2,2-Tetrachloroethane BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.0661,1,2-Trichloroethane BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.0831,1-Dichloroethane BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.0831,1-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.0511,1-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.401,2,3-Trichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.141,2,3-Trichloropropane BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.131,2,4-Trichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.0541,2,4-Trimethylbenzene BRL SM6200 B P7C012012.0 3/7/17 19:34 KDMug/L 0.171,2-Dibromo-3-chloropropane BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.0511,2-Dibromoethane BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.0761,2-Dichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.0661,2-Dichloroethane BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.111,2-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.0761,3,5-Trimethylbenzene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.0541,3-Dichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.0431,3-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.0501,4-Dichlorobenzene BRL SM6200 B P7C012012.0 3/7/17 19:34 KDMug/L 0.112,2-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.0662-Chlorotoluene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.0504-Chlorotoluene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.0894-Isopropyltoluene BRL SM6200 B P7C01201103/7/17 19:34 KDMug/L 0.31Acetone BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.048Benzene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.057Bromobenzene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.14Bromochloromethane BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.062Bromodichloromethane BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.040Bromoform BRL SM6200 B P7C012011.0 3/7/17 19:34 KDMug/L 0.18Bromomethane BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.11Carbon Tetrachloride BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.062Chlorobenzene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.22Chloroethane BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.076Chloroform BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.079Chloromethane BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.056cis-1,2-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.079cis-1,3-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.081Dibromochloromethane BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.065Dibromomethane BRL SM6200 B P7C012011.0 3/7/17 19:34 KDMug/L 0.11Dichlorodifluoromethane BRL SM6200 B P7C012012003/7/17 19:34 KDMug/L 27Ethanol This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 30 Laboratory Report 03/10/2017 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Sample Matrix: Water Client Sample ID: MW-10 Prism Sample ID: 7030063-02 Prism Work Order: 7030063 Time Collected: 02/28/17 14:10 Time Submitted: 03/03/17 15:15 BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.061Ethylbenzene BRL SM6200 B P7C012012.0 3/7/17 19:34 KDMug/L 0.16Hexachlorobutadiene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.050Isopropyl Ether BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.054Isopropylbenzene (Cumene) BRL SM6200 B P7C012011.0 3/7/17 19:34 KDMug/L 0.12m,p-Xylenes BRL SM6200 B P7C012011.0 3/7/17 19:34 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL SM6200 B P7C012015.0 3/7/17 19:34 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL SM6200 B P7C012011.0 3/7/17 19:34 KDMug/L 0.078Methyl Isobutyl Ketone BRL SM6200 B P7C012012.0 3/7/17 19:34 KDMug/L 0.083Methylene Chloride BRL SM6200 B P7C012011.0 3/7/17 19:34 KDMug/L 0.042Methyl-tert-Butyl Ether BRL SM6200 B P7C012011.0 3/7/17 19:34 KDMug/L 0.19Naphthalene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.076n-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.087n-Propylbenzene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.044o-Xylene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.076sec-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.047Styrene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.088tert-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.098Tetrachloroethylene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.044Toluene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.070trans-1,2-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.12trans-1,3-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.078Trichloroethylene BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.062Trichlorofluoromethane BRL SM6200 B P7C012015.0 3/7/17 19:34 KDMug/L 0.060Vinyl acetate BRL SM6200 B P7C012010.50 3/7/17 19:34 KDMug/L 0.097Vinyl chloride BRL SM6200 B P7C012011.5 3/7/17 19:34 KDMug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-13092 %4-Bromofluorobenzene 70-13091 %Dibromofluoromethane 70-13084 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 30 Laboratory Report 03/10/2017 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Sample Matrix: Water Client Sample ID: MW-11 Prism Sample ID: 7030063-03 Prism Work Order: 7030063 Time Collected: 02/28/17 14:20 Time Submitted: 03/03/17 15:15 Volatile Organic Compounds by GC/MS BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.111,1,1,2-Tetrachloroethane BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.0611,1,1-Trichloroethane BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.0361,1,2,2-Tetrachloroethane BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.0661,1,2-Trichloroethane BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.0831,1-Dichloroethane BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.0831,1-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.0511,1-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.401,2,3-Trichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.141,2,3-Trichloropropane BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.131,2,4-Trichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.0541,2,4-Trimethylbenzene BRL SM6200 B P7C012012.0 3/7/17 20:00 KDMug/L 0.171,2-Dibromo-3-chloropropane BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.0511,2-Dibromoethane BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.0761,2-Dichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.0661,2-Dichloroethane BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.111,2-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.0761,3,5-Trimethylbenzene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.0541,3-Dichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.0431,3-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.0501,4-Dichlorobenzene BRL SM6200 B P7C012012.0 3/7/17 20:00 KDMug/L 0.112,2-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.0662-Chlorotoluene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.0504-Chlorotoluene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.0894-Isopropyltoluene BRL SM6200 B P7C01201103/7/17 20:00 KDMug/L 0.31Acetone BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.048Benzene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.057Bromobenzene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.14Bromochloromethane BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.062Bromodichloromethane BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.040Bromoform BRL SM6200 B P7C012011.0 3/7/17 20:00 KDMug/L 0.18Bromomethane BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.11Carbon Tetrachloride BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.062Chlorobenzene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.22Chloroethane BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.076Chloroform BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.079Chloromethane BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.056cis-1,2-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.079cis-1,3-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.081Dibromochloromethane BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.065Dibromomethane BRL SM6200 B P7C012011.0 3/7/17 20:00 KDMug/L 0.11Dichlorodifluoromethane BRL SM6200 B P7C012012003/7/17 20:00 KDMug/L 27Ethanol This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 30 Laboratory Report 03/10/2017 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Sample Matrix: Water Client Sample ID: MW-11 Prism Sample ID: 7030063-03 Prism Work Order: 7030063 Time Collected: 02/28/17 14:20 Time Submitted: 03/03/17 15:15 BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.061Ethylbenzene BRL SM6200 B P7C012012.0 3/7/17 20:00 KDMug/L 0.16Hexachlorobutadiene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.050Isopropyl Ether BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.054Isopropylbenzene (Cumene) BRL SM6200 B P7C012011.0 3/7/17 20:00 KDMug/L 0.12m,p-Xylenes BRL SM6200 B P7C012011.0 3/7/17 20:00 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL SM6200 B P7C012015.0 3/7/17 20:00 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL SM6200 B P7C012011.0 3/7/17 20:00 KDMug/L 0.078Methyl Isobutyl Ketone BRL SM6200 B P7C012012.0 3/7/17 20:00 KDMug/L 0.083Methylene Chloride BRL SM6200 B P7C012011.0 3/7/17 20:00 KDMug/L 0.042Methyl-tert-Butyl Ether BRL SM6200 B P7C012011.0 3/7/17 20:00 KDMug/L 0.19Naphthalene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.076n-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.087n-Propylbenzene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.044o-Xylene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.076sec-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.047Styrene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.088tert-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.098Tetrachloroethylene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.044Toluene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.070trans-1,2-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.12trans-1,3-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.078Trichloroethylene BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.062Trichlorofluoromethane BRL SM6200 B P7C012015.0 3/7/17 20:00 KDMug/L 0.060Vinyl acetate BRL SM6200 B P7C012010.50 3/7/17 20:00 KDMug/L 0.097Vinyl chloride BRL SM6200 B P7C012011.5 3/7/17 20:00 KDMug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-13092 %4-Bromofluorobenzene 70-13093 %Dibromofluoromethane 70-13084 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 9 of 30 Laboratory Report 03/10/2017 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Sample Matrix: Water Client Sample ID: MW-12 Prism Sample ID: 7030063-04 Prism Work Order: 7030063 Time Collected: 02/28/17 14:30 Time Submitted: 03/03/17 15:15 Volatile Organic Compounds by GC/MS BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.111,1,1,2-Tetrachloroethane BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.0611,1,1-Trichloroethane BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.0361,1,2,2-Tetrachloroethane BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.0661,1,2-Trichloroethane BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.0831,1-Dichloroethane BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.0831,1-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.0511,1-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.401,2,3-Trichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.141,2,3-Trichloropropane BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.131,2,4-Trichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.0541,2,4-Trimethylbenzene BRL SM6200 B P7C012012.0 3/7/17 20:26 KDMug/L 0.171,2-Dibromo-3-chloropropane BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.0511,2-Dibromoethane BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.0761,2-Dichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.0661,2-Dichloroethane BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.111,2-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.0761,3,5-Trimethylbenzene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.0541,3-Dichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.0431,3-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.0501,4-Dichlorobenzene BRL SM6200 B P7C012012.0 3/7/17 20:26 KDMug/L 0.112,2-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.0662-Chlorotoluene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.0504-Chlorotoluene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.0894-Isopropyltoluene BRL SM6200 B P7C01201103/7/17 20:26 KDMug/L 0.31Acetone BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.048Benzene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.057Bromobenzene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.14Bromochloromethane BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.062Bromodichloromethane BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.040Bromoform BRL SM6200 B P7C012011.0 3/7/17 20:26 KDMug/L 0.18Bromomethane BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.11Carbon Tetrachloride BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.062Chlorobenzene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.22Chloroethane BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.076Chloroform BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.079Chloromethane BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.056cis-1,2-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.079cis-1,3-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.081Dibromochloromethane BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.065Dibromomethane BRL SM6200 B P7C012011.0 3/7/17 20:26 KDMug/L 0.11Dichlorodifluoromethane BRL SM6200 B P7C012012003/7/17 20:26 KDMug/L 27Ethanol This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 30 Laboratory Report 03/10/2017 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Sample Matrix: Water Client Sample ID: MW-12 Prism Sample ID: 7030063-04 Prism Work Order: 7030063 Time Collected: 02/28/17 14:30 Time Submitted: 03/03/17 15:15 BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.061Ethylbenzene BRL SM6200 B P7C012012.0 3/7/17 20:26 KDMug/L 0.16Hexachlorobutadiene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.050Isopropyl Ether BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.054Isopropylbenzene (Cumene) BRL SM6200 B P7C012011.0 3/7/17 20:26 KDMug/L 0.12m,p-Xylenes BRL SM6200 B P7C012011.0 3/7/17 20:26 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL SM6200 B P7C012015.0 3/7/17 20:26 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL SM6200 B P7C012011.0 3/7/17 20:26 KDMug/L 0.078Methyl Isobutyl Ketone BRL SM6200 B P7C012012.0 3/7/17 20:26 KDMug/L 0.083Methylene Chloride BRL SM6200 B P7C012011.0 3/7/17 20:26 KDMug/L 0.042Methyl-tert-Butyl Ether BRL SM6200 B P7C012011.0 3/7/17 20:26 KDMug/L 0.19Naphthalene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.076n-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.087n-Propylbenzene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.044o-Xylene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.076sec-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.047Styrene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.088tert-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.098Tetrachloroethylene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.044Toluene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.070trans-1,2-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.12trans-1,3-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.078Trichloroethylene BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.062Trichlorofluoromethane BRL SM6200 B P7C012015.0 3/7/17 20:26 KDMug/L 0.060Vinyl acetate BRL SM6200 B P7C012010.50 3/7/17 20:26 KDMug/L 0.097Vinyl chloride BRL SM6200 B P7C012011.5 3/7/17 20:26 KDMug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-13093 %4-Bromofluorobenzene 70-13094 %Dibromofluoromethane 70-13085 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 11 of 30 Laboratory Report 03/10/2017 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Sample Matrix: Water Client Sample ID: MW-13 Prism Sample ID: 7030063-05 Prism Work Order: 7030063 Time Collected: 02/28/17 15:00 Time Submitted: 03/03/17 15:15 Volatile Organic Compounds by GC/MS BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.111,1,1,2-Tetrachloroethane BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.0611,1,1-Trichloroethane BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.0361,1,2,2-Tetrachloroethane BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.0661,1,2-Trichloroethane BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.0831,1-Dichloroethane BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.0831,1-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.0511,1-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.401,2,3-Trichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.141,2,3-Trichloropropane BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.131,2,4-Trichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.0541,2,4-Trimethylbenzene BRL SM6200 B P7C012012.0 3/7/17 20:52 KDMug/L 0.171,2-Dibromo-3-chloropropane BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.0511,2-Dibromoethane BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.0761,2-Dichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.0661,2-Dichloroethane BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.111,2-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.0761,3,5-Trimethylbenzene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.0541,3-Dichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.0431,3-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.0501,4-Dichlorobenzene BRL SM6200 B P7C012012.0 3/7/17 20:52 KDMug/L 0.112,2-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.0662-Chlorotoluene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.0504-Chlorotoluene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.0894-Isopropyltoluene BRL SM6200 B P7C01201103/7/17 20:52 KDMug/L 0.31Acetone BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.048Benzene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.057Bromobenzene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.14Bromochloromethane BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.062Bromodichloromethane BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.040Bromoform BRL SM6200 B P7C012011.0 3/7/17 20:52 KDMug/L 0.18Bromomethane BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.11Carbon Tetrachloride BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.062Chlorobenzene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.22Chloroethane BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.076Chloroform BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.079Chloromethane BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.056cis-1,2-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.079cis-1,3-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.081Dibromochloromethane BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.065Dibromomethane BRL SM6200 B P7C012011.0 3/7/17 20:52 KDMug/L 0.11Dichlorodifluoromethane BRL SM6200 B P7C012012003/7/17 20:52 KDMug/L 27Ethanol This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 12 of 30 Laboratory Report 03/10/2017 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Sample Matrix: Water Client Sample ID: MW-13 Prism Sample ID: 7030063-05 Prism Work Order: 7030063 Time Collected: 02/28/17 15:00 Time Submitted: 03/03/17 15:15 BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.061Ethylbenzene BRL SM6200 B P7C012012.0 3/7/17 20:52 KDMug/L 0.16Hexachlorobutadiene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.050Isopropyl Ether BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.054Isopropylbenzene (Cumene) BRL SM6200 B P7C012011.0 3/7/17 20:52 KDMug/L 0.12m,p-Xylenes BRL SM6200 B P7C012011.0 3/7/17 20:52 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL SM6200 B P7C012015.0 3/7/17 20:52 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL SM6200 B P7C012011.0 3/7/17 20:52 KDMug/L 0.078Methyl Isobutyl Ketone BRL SM6200 B P7C012012.0 3/7/17 20:52 KDMug/L 0.083Methylene Chloride BRL SM6200 B P7C012011.0 3/7/17 20:52 KDMug/L 0.042Methyl-tert-Butyl Ether BRL SM6200 B P7C012011.0 3/7/17 20:52 KDMug/L 0.19Naphthalene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.076n-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.087n-Propylbenzene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.044o-Xylene 0.60 SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.076sec-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.047Styrene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.088tert-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.098Tetrachloroethylene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.044Toluene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.070trans-1,2-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.12trans-1,3-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.078Trichloroethylene BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.062Trichlorofluoromethane BRL SM6200 B P7C012015.0 3/7/17 20:52 KDMug/L 0.060Vinyl acetate BRL SM6200 B P7C012010.50 3/7/17 20:52 KDMug/L 0.097Vinyl chloride BRL SM6200 B P7C012011.5 3/7/17 20:52 KDMug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-13095 %4-Bromofluorobenzene 70-13093 %Dibromofluoromethane 70-13087 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 13 of 30 Laboratory Report 03/10/2017 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Sample Matrix: Water Client Sample ID: MW-15A Prism Sample ID: 7030063-06 Prism Work Order: 7030063 Time Collected: 02/28/17 15:20 Time Submitted: 03/03/17 15:15 Volatile Organic Compounds by GC/MS BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.111,1,1,2-Tetrachloroethane BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.0611,1,1-Trichloroethane BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.0361,1,2,2-Tetrachloroethane BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.0661,1,2-Trichloroethane BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.0831,1-Dichloroethane BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.0831,1-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.0511,1-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.401,2,3-Trichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.141,2,3-Trichloropropane BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.131,2,4-Trichlorobenzene 35 SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.0541,2,4-Trimethylbenzene BRL SM6200 B P7C012012.0 3/7/17 23:53 KDMug/L 0.171,2-Dibromo-3-chloropropane BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.0511,2-Dibromoethane BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.0761,2-Dichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.0661,2-Dichloroethane BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.111,2-Dichloropropane 8.8 SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.0761,3,5-Trimethylbenzene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.0541,3-Dichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.0431,3-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.0501,4-Dichlorobenzene BRL SM6200 B P7C012012.0 3/7/17 23:53 KDMug/L 0.112,2-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.0662-Chlorotoluene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.0504-Chlorotoluene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.0894-Isopropyltoluene BRL SM6200 B P7C01201103/7/17 23:53 KDMug/L 0.31Acetone BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.048Benzene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.057Bromobenzene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.14Bromochloromethane BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.062Bromodichloromethane BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.040Bromoform BRL SM6200 B P7C012011.0 3/7/17 23:53 KDMug/L 0.18Bromomethane BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.11Carbon Tetrachloride BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.062Chlorobenzene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.22Chloroethane BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.076Chloroform BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.079Chloromethane BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.056cis-1,2-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.079cis-1,3-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.081Dibromochloromethane BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.065Dibromomethane BRL SM6200 B P7C012011.0 3/7/17 23:53 KDMug/L 0.11Dichlorodifluoromethane BRL SM6200 B P7C012012003/7/17 23:53 KDMug/L 27Ethanol This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 14 of 30 Laboratory Report 03/10/2017 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Sample Matrix: Water Client Sample ID: MW-15A Prism Sample ID: 7030063-06 Prism Work Order: 7030063 Time Collected: 02/28/17 15:20 Time Submitted: 03/03/17 15:15 37 SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.061Ethylbenzene BRL SM6200 B P7C012012.0 3/7/17 23:53 KDMug/L 0.16Hexachlorobutadiene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.050Isopropyl Ether 3.0 SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.054Isopropylbenzene (Cumene) 69 SM6200 B P7C012011.0 3/7/17 23:53 KDMug/L 0.12m,p-Xylenes BRL SM6200 B P7C012011.0 3/7/17 23:53 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL SM6200 B P7C012015.0 3/7/17 23:53 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL SM6200 B P7C012011.0 3/7/17 23:53 KDMug/L 0.078Methyl Isobutyl Ketone BRL SM6200 B P7C012012.0 3/7/17 23:53 KDMug/L 0.083Methylene Chloride BRL SM6200 B P7C012011.0 3/7/17 23:53 KDMug/L 0.042Methyl-tert-Butyl Ether 11 SM6200 B P7C012011.0 3/7/17 23:53 KDMug/L 0.19Naphthalene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.076n-Butylbenzene 3.6 SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.087n-Propylbenzene 56 SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.044o-Xylene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.076sec-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.047Styrene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.088tert-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.098Tetrachloroethylene 10 SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.044Toluene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.070trans-1,2-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.12trans-1,3-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.078Trichloroethylene BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.062Trichlorofluoromethane BRL SM6200 B P7C012015.0 3/7/17 23:53 KDMug/L 0.060Vinyl acetate BRL SM6200 B P7C012010.50 3/7/17 23:53 KDMug/L 0.097Vinyl chloride 130 SM6200 B P7C012011.5 3/7/17 23:53 KDMug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-13093 %4-Bromofluorobenzene 70-13092 %Dibromofluoromethane 70-13085 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 15 of 30 Laboratory Report 03/10/2017 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Sample Matrix: Water Client Sample ID: SW 2773 Prism Sample ID: 7030063-07 Prism Work Order: 7030063 Time Collected: 02/28/17 14:00 Time Submitted: 03/03/17 15:15 Volatile Organic Compounds by GC/MS BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.111,1,1,2-Tetrachloroethane BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.0611,1,1-Trichloroethane BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.0361,1,2,2-Tetrachloroethane BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.0661,1,2-Trichloroethane BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.0831,1-Dichloroethane BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.0831,1-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.0511,1-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.401,2,3-Trichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.141,2,3-Trichloropropane BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.131,2,4-Trichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.0541,2,4-Trimethylbenzene BRL SM6200 B P7C012012.0 3/7/17 21:18 KDMug/L 0.171,2-Dibromo-3-chloropropane BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.0511,2-Dibromoethane BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.0761,2-Dichlorobenzene 0.59 SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.0661,2-Dichloroethane BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.111,2-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.0761,3,5-Trimethylbenzene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.0541,3-Dichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.0431,3-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.0501,4-Dichlorobenzene BRL SM6200 B P7C012012.0 3/7/17 21:18 KDMug/L 0.112,2-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.0662-Chlorotoluene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.0504-Chlorotoluene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.0894-Isopropyltoluene BRL SM6200 B P7C01201103/7/17 21:18 KDMug/L 0.31Acetone BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.048Benzene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.057Bromobenzene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.14Bromochloromethane BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.062Bromodichloromethane BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.040Bromoform BRL SM6200 B P7C012011.0 3/7/17 21:18 KDMug/L 0.18Bromomethane BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.11Carbon Tetrachloride BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.062Chlorobenzene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.22Chloroethane BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.076Chloroform BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.079Chloromethane BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.056cis-1,2-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.079cis-1,3-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.081Dibromochloromethane BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.065Dibromomethane BRL SM6200 B P7C012011.0 3/7/17 21:18 KDMug/L 0.11Dichlorodifluoromethane BRL SM6200 B P7C012012003/7/17 21:18 KDMug/L 27Ethanol This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 16 of 30 Laboratory Report 03/10/2017 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Sample Matrix: Water Client Sample ID: SW 2773 Prism Sample ID: 7030063-07 Prism Work Order: 7030063 Time Collected: 02/28/17 14:00 Time Submitted: 03/03/17 15:15 BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.061Ethylbenzene BRL SM6200 B P7C012012.0 3/7/17 21:18 KDMug/L 0.16Hexachlorobutadiene 2.0 SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.050Isopropyl Ether BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.054Isopropylbenzene (Cumene) BRL SM6200 B P7C012011.0 3/7/17 21:18 KDMug/L 0.12m,p-Xylenes BRL SM6200 B P7C012011.0 3/7/17 21:18 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL SM6200 B P7C012015.0 3/7/17 21:18 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL SM6200 B P7C012011.0 3/7/17 21:18 KDMug/L 0.078Methyl Isobutyl Ketone BRL SM6200 B P7C012012.0 3/7/17 21:18 KDMug/L 0.083Methylene Chloride 1.8 SM6200 B P7C012011.0 3/7/17 21:18 KDMug/L 0.042Methyl-tert-Butyl Ether BRL SM6200 B P7C012011.0 3/7/17 21:18 KDMug/L 0.19Naphthalene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.076n-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.087n-Propylbenzene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.044o-Xylene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.076sec-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.047Styrene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.088tert-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.098Tetrachloroethylene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.044Toluene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.070trans-1,2-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.12trans-1,3-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.078Trichloroethylene BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.062Trichlorofluoromethane BRL SM6200 B P7C012015.0 3/7/17 21:18 KDMug/L 0.060Vinyl acetate BRL SM6200 B P7C012010.50 3/7/17 21:18 KDMug/L 0.097Vinyl chloride BRL SM6200 B P7C012011.5 3/7/17 21:18 KDMug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-13090 %4-Bromofluorobenzene 70-13091 %Dibromofluoromethane 70-13084 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 17 of 30 Laboratory Report 03/10/2017 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Sample Matrix: Water Client Sample ID: SW-2765 Prism Sample ID: 7030063-08 Prism Work Order: 7030063 Time Collected: 02/28/17 13:00 Time Submitted: 03/03/17 15:15 Volatile Organic Compounds by GC/MS BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.111,1,1,2-Tetrachloroethane BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.0611,1,1-Trichloroethane BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.0361,1,2,2-Tetrachloroethane BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.0661,1,2-Trichloroethane BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.0831,1-Dichloroethane BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.0831,1-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.0511,1-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.401,2,3-Trichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.141,2,3-Trichloropropane BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.131,2,4-Trichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.0541,2,4-Trimethylbenzene BRL SM6200 B P7C012012.0 3/7/17 21:44 KDMug/L 0.171,2-Dibromo-3-chloropropane BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.0511,2-Dibromoethane BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.0761,2-Dichlorobenzene 5.2 SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.0661,2-Dichloroethane BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.111,2-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.0761,3,5-Trimethylbenzene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.0541,3-Dichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.0431,3-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.0501,4-Dichlorobenzene BRL SM6200 B P7C012012.0 3/7/17 21:44 KDMug/L 0.112,2-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.0662-Chlorotoluene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.0504-Chlorotoluene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.0894-Isopropyltoluene BRL SM6200 B P7C01201103/7/17 21:44 KDMug/L 0.31Acetone BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.048Benzene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.057Bromobenzene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.14Bromochloromethane BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.062Bromodichloromethane BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.040Bromoform BRL SM6200 B P7C012011.0 3/7/17 21:44 KDMug/L 0.18Bromomethane BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.11Carbon Tetrachloride BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.062Chlorobenzene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.22Chloroethane BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.076Chloroform BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.079Chloromethane BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.056cis-1,2-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.079cis-1,3-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.081Dibromochloromethane BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.065Dibromomethane BRL SM6200 B P7C012011.0 3/7/17 21:44 KDMug/L 0.11Dichlorodifluoromethane BRL SM6200 B P7C012012003/7/17 21:44 KDMug/L 27Ethanol This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 18 of 30 Laboratory Report 03/10/2017 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Sample Matrix: Water Client Sample ID: SW-2765 Prism Sample ID: 7030063-08 Prism Work Order: 7030063 Time Collected: 02/28/17 13:00 Time Submitted: 03/03/17 15:15 BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.061Ethylbenzene BRL SM6200 B P7C012012.0 3/7/17 21:44 KDMug/L 0.16Hexachlorobutadiene 33 SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.050Isopropyl Ether BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.054Isopropylbenzene (Cumene) BRL SM6200 B P7C012011.0 3/7/17 21:44 KDMug/L 0.12m,p-Xylenes BRL SM6200 B P7C012011.0 3/7/17 21:44 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL SM6200 B P7C012015.0 3/7/17 21:44 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL SM6200 B P7C012011.0 3/7/17 21:44 KDMug/L 0.078Methyl Isobutyl Ketone BRL SM6200 B P7C012012.0 3/7/17 21:44 KDMug/L 0.083Methylene Chloride 29 SM6200 B P7C012011.0 3/7/17 21:44 KDMug/L 0.042Methyl-tert-Butyl Ether BRL SM6200 B P7C012011.0 3/7/17 21:44 KDMug/L 0.19Naphthalene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.076n-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.087n-Propylbenzene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.044o-Xylene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.076sec-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.047Styrene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.088tert-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.098Tetrachloroethylene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.044Toluene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.070trans-1,2-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.12trans-1,3-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.078Trichloroethylene BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.062Trichlorofluoromethane BRL SM6200 B P7C012015.0 3/7/17 21:44 KDMug/L 0.060Vinyl acetate BRL SM6200 B P7C012010.50 3/7/17 21:44 KDMug/L 0.097Vinyl chloride BRL SM6200 B P7C012011.5 3/7/17 21:44 KDMug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-13092 %4-Bromofluorobenzene 70-13091 %Dibromofluoromethane 70-13085 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 19 of 30 Laboratory Report 03/10/2017 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Sample Matrix: Water Client Sample ID: 2765 Mid Prism Sample ID: 7030063-09 Prism Work Order: 7030063 Time Collected: 02/28/17 13:10 Time Submitted: 03/03/17 15:15 Volatile Organic Compounds by GC/MS BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.111,1,1,2-Tetrachloroethane BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.0611,1,1-Trichloroethane BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.0361,1,2,2-Tetrachloroethane BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.0661,1,2-Trichloroethane BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.0831,1-Dichloroethane BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.0831,1-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.0511,1-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.401,2,3-Trichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.141,2,3-Trichloropropane BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.131,2,4-Trichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.0541,2,4-Trimethylbenzene BRL SM6200 B P7C012012.0 3/7/17 22:10 KDMug/L 0.171,2-Dibromo-3-chloropropane BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.0511,2-Dibromoethane BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.0761,2-Dichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.0661,2-Dichloroethane BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.111,2-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.0761,3,5-Trimethylbenzene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.0541,3-Dichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.0431,3-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.0501,4-Dichlorobenzene BRL SM6200 B P7C012012.0 3/7/17 22:10 KDMug/L 0.112,2-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.0662-Chlorotoluene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.0504-Chlorotoluene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.0894-Isopropyltoluene BRL SM6200 B P7C01201103/7/17 22:10 KDMug/L 0.31Acetone BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.048Benzene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.057Bromobenzene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.14Bromochloromethane BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.062Bromodichloromethane BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.040Bromoform BRL SM6200 B P7C012011.0 3/7/17 22:10 KDMug/L 0.18Bromomethane BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.11Carbon Tetrachloride BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.062Chlorobenzene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.22Chloroethane BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.076Chloroform BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.079Chloromethane BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.056cis-1,2-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.079cis-1,3-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.081Dibromochloromethane BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.065Dibromomethane BRL SM6200 B P7C012011.0 3/7/17 22:10 KDMug/L 0.11Dichlorodifluoromethane BRL SM6200 B P7C012012003/7/17 22:10 KDMug/L 27Ethanol This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 20 of 30 Laboratory Report 03/10/2017 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Sample Matrix: Water Client Sample ID: 2765 Mid Prism Sample ID: 7030063-09 Prism Work Order: 7030063 Time Collected: 02/28/17 13:10 Time Submitted: 03/03/17 15:15 BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.061Ethylbenzene BRL SM6200 B P7C012012.0 3/7/17 22:10 KDMug/L 0.16Hexachlorobutadiene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.050Isopropyl Ether BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.054Isopropylbenzene (Cumene) BRL SM6200 B P7C012011.0 3/7/17 22:10 KDMug/L 0.12m,p-Xylenes BRL SM6200 B P7C012011.0 3/7/17 22:10 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL SM6200 B P7C012015.0 3/7/17 22:10 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL SM6200 B P7C012011.0 3/7/17 22:10 KDMug/L 0.078Methyl Isobutyl Ketone BRL SM6200 B P7C012012.0 3/7/17 22:10 KDMug/L 0.083Methylene Chloride BRL SM6200 B P7C012011.0 3/7/17 22:10 KDMug/L 0.042Methyl-tert-Butyl Ether BRL SM6200 B P7C012011.0 3/7/17 22:10 KDMug/L 0.19Naphthalene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.076n-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.087n-Propylbenzene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.044o-Xylene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.076sec-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.047Styrene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.088tert-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.098Tetrachloroethylene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.044Toluene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.070trans-1,2-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.12trans-1,3-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.078Trichloroethylene BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.062Trichlorofluoromethane BRL SM6200 B P7C012015.0 3/7/17 22:10 KDMug/L 0.060Vinyl acetate BRL SM6200 B P7C012010.50 3/7/17 22:10 KDMug/L 0.097Vinyl chloride BRL SM6200 B P7C012011.5 3/7/17 22:10 KDMug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-13092 %4-Bromofluorobenzene 70-13092 %Dibromofluoromethane 70-13083 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 21 of 30 Laboratory Report 03/10/2017 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Sample Matrix: Water Client Sample ID: 2765 Eff Prism Sample ID: 7030063-10 Prism Work Order: 7030063 Time Collected: 02/28/17 13:20 Time Submitted: 03/03/17 15:15 Volatile Organic Compounds by GC/MS BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.111,1,1,2-Tetrachloroethane BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.0611,1,1-Trichloroethane BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.0361,1,2,2-Tetrachloroethane BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.0661,1,2-Trichloroethane BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.0831,1-Dichloroethane BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.0831,1-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.0511,1-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.401,2,3-Trichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.141,2,3-Trichloropropane BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.131,2,4-Trichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.0541,2,4-Trimethylbenzene BRL SM6200 B P7C012012.0 3/7/17 22:35 KDMug/L 0.171,2-Dibromo-3-chloropropane BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.0511,2-Dibromoethane BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.0761,2-Dichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.0661,2-Dichloroethane BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.111,2-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.0761,3,5-Trimethylbenzene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.0541,3-Dichlorobenzene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.0431,3-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.0501,4-Dichlorobenzene BRL SM6200 B P7C012012.0 3/7/17 22:35 KDMug/L 0.112,2-Dichloropropane BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.0662-Chlorotoluene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.0504-Chlorotoluene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.0894-Isopropyltoluene BRL SM6200 B P7C01201103/7/17 22:35 KDMug/L 0.31Acetone BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.048Benzene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.057Bromobenzene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.14Bromochloromethane BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.062Bromodichloromethane BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.040Bromoform BRL SM6200 B P7C012011.0 3/7/17 22:35 KDMug/L 0.18Bromomethane BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.11Carbon Tetrachloride BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.062Chlorobenzene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.22Chloroethane BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.076Chloroform 0.80 SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.079Chloromethane BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.056cis-1,2-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.079cis-1,3-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.081Dibromochloromethane BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.065Dibromomethane BRL SM6200 B P7C012011.0 3/7/17 22:35 KDMug/L 0.11Dichlorodifluoromethane BRL SM6200 B P7C012012003/7/17 22:35 KDMug/L 27Ethanol This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 22 of 30 Laboratory Report 03/10/2017 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Sample Matrix: Water Client Sample ID: 2765 Eff Prism Sample ID: 7030063-10 Prism Work Order: 7030063 Time Collected: 02/28/17 13:20 Time Submitted: 03/03/17 15:15 BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.061Ethylbenzene BRL SM6200 B P7C012012.0 3/7/17 22:35 KDMug/L 0.16Hexachlorobutadiene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.050Isopropyl Ether BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.054Isopropylbenzene (Cumene) BRL SM6200 B P7C012011.0 3/7/17 22:35 KDMug/L 0.12m,p-Xylenes BRL SM6200 B P7C012011.0 3/7/17 22:35 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL SM6200 B P7C012015.0 3/7/17 22:35 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL SM6200 B P7C012011.0 3/7/17 22:35 KDMug/L 0.078Methyl Isobutyl Ketone BRL SM6200 B P7C012012.0 3/7/17 22:35 KDMug/L 0.083Methylene Chloride BRL SM6200 B P7C012011.0 3/7/17 22:35 KDMug/L 0.042Methyl-tert-Butyl Ether BRL SM6200 B P7C012011.0 3/7/17 22:35 KDMug/L 0.19Naphthalene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.076n-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.087n-Propylbenzene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.044o-Xylene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.076sec-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.047Styrene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.088tert-Butylbenzene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.098Tetrachloroethylene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.044Toluene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.070trans-1,2-Dichloroethylene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.12trans-1,3-Dichloropropylene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.078Trichloroethylene BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.062Trichlorofluoromethane BRL SM6200 B P7C012015.0 3/7/17 22:35 KDMug/L 0.060Vinyl acetate BRL SM6200 B P7C012010.50 3/7/17 22:35 KDMug/L 0.097Vinyl chloride BRL SM6200 B P7C012011.5 3/7/17 22:35 KDMug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-13091 %4-Bromofluorobenzene 70-13090 %Dibromofluoromethane 70-13084 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 23 of 30 3/10/17 Level II QC Report PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Prism Work Order: 7030063 Time Submitted: 3/3/2017 3:15:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P7C0120 - SM6200 B Blank (P7C0120-BLK1)Prepared & Analyzed: 03/07/17 1,1,1,2-Tetrachloroethane ug/LBRL0.50 1,1,1-Trichloroethane ug/LBRL0.50 1,1,2,2-Tetrachloroethane ug/LBRL0.50 1,1,2-Trichloroethane ug/LBRL0.50 1,1-Dichloroethane ug/LBRL0.50 1,1-Dichloroethylene ug/LBRL0.50 1,1-Dichloropropylene ug/LBRL0.50 1,2,3-Trichlorobenzene ug/LBRL0.50 1,2,3-Trichloropropane ug/LBRL0.50 1,2,4-Trichlorobenzene ug/LBRL0.50 1,2,4-Trimethylbenzene ug/LBRL0.50 1,2-Dibromo-3-chloropropane ug/LBRL2.0 1,2-Dibromoethane ug/LBRL0.50 1,2-Dichlorobenzene ug/LBRL0.50 1,2-Dichloroethane ug/LBRL0.50 1,2-Dichloropropane ug/LBRL0.50 1,3,5-Trimethylbenzene ug/LBRL0.50 1,3-Dichlorobenzene ug/LBRL0.50 1,3-Dichloropropane ug/LBRL0.50 1,4-Dichlorobenzene ug/LBRL0.50 2,2-Dichloropropane ug/LBRL2.0 2-Chlorotoluene ug/LBRL0.50 4-Chlorotoluene ug/LBRL0.50 4-Isopropyltoluene ug/LBRL0.50 Acetone ug/LBRL10 Benzene ug/LBRL0.50 Bromobenzene ug/LBRL0.50 Bromochloromethane ug/LBRL0.50 Bromodichloromethane ug/LBRL0.50 Bromoform ug/LBRL0.50 Bromomethane ug/LBRL1.0 Carbon Tetrachloride ug/LBRL0.50 Chlorobenzene ug/LBRL0.50 Chloroethane ug/LBRL0.50 Chloroform ug/LBRL0.50 Chloromethane ug/LBRL0.50 cis-1,2-Dichloroethylene ug/LBRL0.50 cis-1,3-Dichloropropylene ug/LBRL0.50 Dibromochloromethane ug/LBRL0.50 Dibromomethane ug/LBRL0.50 Dichlorodifluoromethane ug/LBRL1.0 Ethanol ug/LBRL200 Ethylbenzene ug/LBRL0.50 Hexachlorobutadiene ug/LBRL2.0 Isopropyl Ether ug/LBRL0.50 Isopropylbenzene (Cumene)ug/LBRL0.50 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 24 of 30 3/10/17 Level II QC Report PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Prism Work Order: 7030063 Time Submitted: 3/3/2017 3:15:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P7C0120 - SM6200 B Blank (P7C0120-BLK1)Prepared & Analyzed: 03/07/17 m,p-Xylenes ug/LBRL1.0 Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0 Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0 Methyl Isobutyl Ketone ug/LBRL1.0 Methylene Chloride ug/LBRL2.0 Methyl-tert-Butyl Ether ug/LBRL1.0 Naphthalene ug/LBRL1.0 n-Butylbenzene ug/LBRL0.50 n-Propylbenzene ug/LBRL0.50 o-Xylene ug/LBRL0.50 sec-Butylbenzene ug/LBRL0.50 Styrene ug/LBRL0.50 tert-Butylbenzene ug/LBRL0.50 Tetrachloroethylene ug/LBRL0.50 Toluene ug/LBRL0.50 trans-1,2-Dichloroethylene ug/LBRL0.50 trans-1,3-Dichloropropylene ug/LBRL0.50 Trichloroethylene ug/LBRL0.50 Trichlorofluoromethane ug/LBRL0.50 Vinyl acetate ug/LBRL5.0 Vinyl chloride ug/LBRL0.50 Xylenes, total ug/LBRL1.5 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9145.3 ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9346.7 ug/L 50.00 70-130Surrogate: Toluene-d8 8442.0 LCS (P7C0120-BS1)Prepared & Analyzed: 03/07/17 1,1,1,2-Tetrachloroethane ug/L20.3 0.50 20.00 70-130102 1,1,1-Trichloroethane ug/L22.1 0.50 20.00 70-130111 1,1,2,2-Tetrachloroethane ug/L16.6 0.50 20.00 70-13083 1,1,2-Trichloroethane ug/L20.9 0.50 20.00 70-130105 1,1-Dichloroethane ug/L21.7 0.50 20.00 70-130109 1,1-Dichloroethylene ug/L20.8 0.50 20.00 70-130104 1,1-Dichloropropylene ug/L22.1 0.50 20.00 70-130110 1,2,3-Trichlorobenzene ug/L18.1 0.50 20.00 70-13090 1,2,3-Trichloropropane ug/L16.3 0.50 20.00 70-13082 1,2,4-Trichlorobenzene ug/L17.9 0.50 20.00 70-13090 1,2,4-Trimethylbenzene ug/L18.6 0.50 20.00 70-13093 1,2-Dibromo-3-chloropropane ug/L14.5 2.0 20.00 70-13073 1,2-Dibromoethane ug/L18.9 0.50 20.00 70-13095 1,2-Dichlorobenzene ug/L18.4 0.50 20.00 70-13092 1,2-Dichloroethane ug/L21.9 0.50 20.00 70-130110 1,2-Dichloropropane ug/L21.6 0.50 20.00 70-130108 1,3,5-Trimethylbenzene ug/L18.6 0.50 20.00 70-13093 1,3-Dichlorobenzene ug/L18.2 0.50 20.00 70-13091 1,3-Dichloropropane ug/L19.2 0.50 20.00 70-13096 1,4-Dichlorobenzene ug/L17.9 0.50 20.00 70-13090 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 25 of 30 3/10/17 Level II QC Report PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Prism Work Order: 7030063 Time Submitted: 3/3/2017 3:15:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P7C0120 - SM6200 B LCS (P7C0120-BS1)Prepared & Analyzed: 03/07/17 2,2-Dichloropropane ug/L22.5 2.0 20.00 70-130112 2-Chlorotoluene ug/L17.9 0.50 20.00 70-13089 4-Chlorotoluene ug/L18.0 0.50 20.00 70-13090 4-Isopropyltoluene ug/L18.8 0.50 20.00 70-13094 Acetone ug/L29.8 10 40.00 40-16074 Benzene ug/L22.2 0.50 20.00 70-130111 Bromobenzene ug/L17.4 0.50 20.00 70-13087 Bromochloromethane ug/L22.3 0.50 20.00 70-130112 Bromodichloromethane ug/L22.8 0.50 20.00 70-130114 Bromoform ug/L16.6 0.50 20.00 70-13083 Bromomethane ug/L22.5 1.0 20.00 60-140113 Carbon Tetrachloride ug/L19.3 0.50 20.00 70-13097 Chlorobenzene ug/L20.0 0.50 20.00 70-130100 Chloroethane ug/L26.2 0.50 20.00 60-140131 Chloroform ug/L21.8 0.50 20.00 70-130109 Chloromethane ug/L16.4 0.50 20.00 60-14082 cis-1,2-Dichloroethylene ug/L21.9 0.50 20.00 70-130109 cis-1,3-Dichloropropylene ug/L22.1 0.50 20.00 70-130110 Dibromochloromethane ug/L18.2 0.50 20.00 70-13091 Dibromomethane ug/L21.1 0.50 20.00 70-130106 Dichlorodifluoromethane ug/L18.9 1.0 20.00 60-14095 Ethanol ug/L375200 500.0 60-14075 Ethylbenzene ug/L20.6 0.50 20.00 70-130103 Hexachlorobutadiene ug/L18.4 2.0 20.00 70-13092 Isopropyl Ether ug/L22.5 0.50 20.00 70-130113 Isopropylbenzene (Cumene)ug/L19.1 0.50 20.00 70-13095 m,p-Xylenes ug/L41.9 1.0 40.00 70-130105 Methyl Butyl Ketone (2-Hexanone)ug/L16.2 1.0 20.00 60-14081 Methyl Ethyl Ketone (2-Butanone)ug/L17.1 5.0 20.00 60-14085 Methyl Isobutyl Ketone ug/L18.4 1.0 20.00 60-14092 Methylene Chloride ug/L21.1 2.0 20.00 70-130106 Methyl-tert-Butyl Ether ug/L21.1 1.0 20.00 70-130106 Naphthalene ug/L16.5 1.0 20.00 70-13082 n-Butylbenzene ug/L18.8 0.50 20.00 70-13094 n-Propylbenzene ug/L19.1 0.50 20.00 70-13095 o-Xylene ug/L20.2 0.50 20.00 70-130101 sec-Butylbenzene ug/L19.0 0.50 20.00 70-13095 Styrene ug/L20.2 0.50 20.00 70-130101 tert-Butylbenzene ug/L18.3 0.50 20.00 70-13092 Tetrachloroethylene ug/L20.6 0.50 20.00 70-130103 Toluene ug/L22.5 0.50 20.00 70-130113 trans-1,2-Dichloroethylene ug/L21.3 0.50 20.00 70-130106 trans-1,3-Dichloropropylene ug/L21.7 0.50 20.00 70-130108 Trichloroethylene ug/L22.8 0.50 20.00 70-130114 Trichlorofluoromethane ug/L28.9 0.50 20.00 L160-140145 Vinyl acetate ug/L21.8 5.0 20.00 60-140109 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 26 of 30 3/10/17 Level II QC Report PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Prism Work Order: 7030063 Time Submitted: 3/3/2017 3:15:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P7C0120 - SM6200 B LCS (P7C0120-BS1)Prepared & Analyzed: 03/07/17 Vinyl chloride ug/L20.1 0.50 20.00 60-140100 Xylenes, total ug/L62.2 1.5 60.00 70-130104 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9246.0 ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9446.9 ug/L 50.00 70-130Surrogate: Toluene-d8 8743.6 LCS Dup (P7C0120-BSD1)Prepared & Analyzed: 03/07/17 1,1,1,2-Tetrachloroethane ug/L19.6 0.50 20.00 2070-13098 4 1,1,1-Trichloroethane ug/L21.1 0.50 20.00 2070-130106 5 1,1,2,2-Tetrachloroethane ug/L17.5 0.50 20.00 2070-13087 5 1,1,2-Trichloroethane ug/L21.3 0.50 20.00 2070-130106 2 1,1-Dichloroethane ug/L21.0 0.50 20.00 2070-130105 3 1,1-Dichloroethylene ug/L20.2 0.50 20.00 2070-130101 3 1,1-Dichloropropylene ug/L21.2 0.50 20.00 2070-130106 4 1,2,3-Trichlorobenzene ug/L18.3 0.50 20.00 2070-13091 0.9 1,2,3-Trichloropropane ug/L16.9 0.50 20.00 2070-13085 4 1,2,4-Trichlorobenzene ug/L17.8 0.50 20.00 2070-13089 0.7 1,2,4-Trimethylbenzene ug/L17.9 0.50 20.00 2070-13090 4 1,2-Dibromo-3-chloropropane ug/L16.2 2.0 20.00 2070-13081 11 1,2-Dibromoethane ug/L19.4 0.50 20.00 2070-13097 2 1,2-Dichlorobenzene ug/L17.7 0.50 20.00 2070-13089 4 1,2-Dichloroethane ug/L22.0 0.50 20.00 2070-130110 0.6 1,2-Dichloropropane ug/L21.3 0.50 20.00 2070-130106 1 1,3,5-Trimethylbenzene ug/L18.0 0.50 20.00 2070-13090 4 1,3-Dichlorobenzene ug/L17.8 0.50 20.00 2070-13089 2 1,3-Dichloropropane ug/L19.2 0.50 20.00 2070-13096 0.5 1,4-Dichlorobenzene ug/L17.5 0.50 20.00 2070-13088 2 2,2-Dichloropropane ug/L21.6 2.0 20.00 2070-130108 4 2-Chlorotoluene ug/L17.1 0.50 20.00 2070-13086 4 4-Chlorotoluene ug/L17.4 0.50 20.00 2070-13087 3 4-Isopropyltoluene ug/L18.1 0.50 20.00 2070-13090 4 Acetone ug/L35.4 10 40.00 2040-16088 17 Benzene ug/L21.4 0.50 20.00 2070-130107 4 Bromobenzene ug/L17.0 0.50 20.00 2070-13085 3 Bromochloromethane ug/L22.4 0.50 20.00 2070-130112 0.3 Bromodichloromethane ug/L22.4 0.50 20.00 2070-130112 2 Bromoform ug/L17.3 0.50 20.00 2070-13087 4 Bromomethane ug/L20.3 1.0 20.00 2060-140101 10 Carbon Tetrachloride ug/L18.8 0.50 20.00 2070-13094 3 Chlorobenzene ug/L19.3 0.50 20.00 2070-13097 4 Chloroethane ug/L23.9 0.50 20.00 2060-140120 9 Chloroform ug/L21.1 0.50 20.00 2070-130106 3 Chloromethane ug/L15.8 0.50 20.00 2060-14079 4 cis-1,2-Dichloroethylene ug/L21.0 0.50 20.00 2070-130105 4 cis-1,3-Dichloropropylene ug/L21.9 0.50 20.00 2070-130110 0.8 Dibromochloromethane ug/L18.0 0.50 20.00 2070-13090 1 Dibromomethane ug/L21.6 0.50 20.00 2070-130108 2 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 27 of 30 3/10/17 Level II QC Report PO Box 16265 Project: Harold SmithPyramid Environmental, Inc Greensboro, NC 27416-0265 Attn: Mika Trifunovic Prism Work Order: 7030063 Time Submitted: 3/3/2017 3:15:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P7C0120 - SM6200 B LCS Dup (P7C0120-BSD1)Prepared & Analyzed: 03/07/17 Dichlorodifluoromethane ug/L17.3 1.0 20.00 2060-14087 9 Ethanol ug/L520200 500.0 20 D60-140104 32 Ethylbenzene ug/L19.9 0.50 20.00 2070-130100 4 Hexachlorobutadiene ug/L17.7 2.0 20.00 2070-13088 4 Isopropyl Ether ug/L22.1 0.50 20.00 2070-130110 2 Isopropylbenzene (Cumene)ug/L18.0 0.50 20.00 2070-13090 6 m,p-Xylenes ug/L40.5 1.0 40.00 2070-130101 3 Methyl Butyl Ketone (2-Hexanone)ug/L18.5 1.0 20.00 2060-14093 13 Methyl Ethyl Ketone (2-Butanone)ug/L19.7 5.0 20.00 2060-14098 14 Methyl Isobutyl Ketone ug/L20.6 1.0 20.00 2060-140103 11 Methylene Chloride ug/L20.7 2.0 20.00 2070-130103 2 Methyl-tert-Butyl Ether ug/L21.2 1.0 20.00 2070-130106 0.2 Naphthalene ug/L17.5 1.0 20.00 2070-13088 6 n-Butylbenzene ug/L17.9 0.50 20.00 2070-13090 5 n-Propylbenzene ug/L18.2 0.50 20.00 2070-13091 5 o-Xylene ug/L19.5 0.50 20.00 2070-13097 4 sec-Butylbenzene ug/L18.1 0.50 20.00 2070-13090 5 Styrene ug/L19.7 0.50 20.00 2070-13099 3 tert-Butylbenzene ug/L17.6 0.50 20.00 2070-13088 4 Tetrachloroethylene ug/L19.7 0.50 20.00 2070-13098 4 Toluene ug/L21.8 0.50 20.00 2070-130109 3 trans-1,2-Dichloroethylene ug/L20.5 0.50 20.00 2070-130103 4 trans-1,3-Dichloropropylene ug/L22.1 0.50 20.00 2070-130110 2 Trichloroethylene ug/L22.1 0.50 20.00 2070-130111 3 Trichlorofluoromethane ug/L26.3 0.50 20.00 2060-140132 9 Vinyl acetate ug/L23.0 5.0 20.00 2060-140115 5 Vinyl chloride ug/L19.3 0.50 20.00 2060-14096 4 Xylenes, total ug/L60.0 1.5 60.00 2070-130100 4 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9145.7 ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9446.9 ug/L 50.00 70-130Surrogate: Toluene-d8 8643.0 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 28 of 30 Sample Extraction Data Prep Method: SM6200 B Lab Number Batch Date/TimeInitialFinal P7C01207030063-01 03/07/17 8:421010mLmL P7C01207030063-01 03/07/17 8:421010mLmL P7C01207030063-02 03/07/17 8:421010mLmL P7C01207030063-03 03/07/17 8:421010mLmL P7C01207030063-04 03/07/17 8:421010mLmL P7C01207030063-05 03/07/17 8:421010mLmL P7C01207030063-06 03/07/17 8:421010mLmL P7C01207030063-07 03/07/17 8:421010mLmL P7C01207030063-08 03/07/17 8:421010mLmL P7C01207030063-09 03/07/17 8:421010mLmL P7C01207030063-10 03/07/17 8:421010mLmL This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 29 of 30 Page 30 of 30 APPENDIX C P.O. Box 16265 • Greensboro, NC 27416 503 Industrial Ave • Greensboro, NC 27406 Phone (336)335-3174 • Fax (336)691-0648 • Toll Free (866)545-9507 Email: Info@pyramidenvironmental.com www.pyramidenvironmental.com March 29, 2017 Ms. Adrienne Apple 2761 Union Ridge Road Burlington, NC 27217 RE: Supply Well Analytical Results 2765 Union Ridge Road, Burlington, NC NCDEQ Incident #12913 Former Harold Smith Grocery Pyramid Project 2016-339 Dear Ms. Apple: As directed by the NCDEQ and T.A.C., Inc., Pyramid Environmental has continued to collect samples from the Point-of-Entry (POE) treatment system that is connected to the water supply well at 2765 Union Ridge Road. The work is being performed as part of the ongoing assessment of the referenced underground storage tank release. The results of the water analyses are presented below. On February 28, 2017, Pyramid collected influent, mid-fluent, and effluent samples from the POE connected to your supply well. The samples are designated as SW-2765 INF, SW-2765 MID, and SW- 2765 EFF. The groundwater samples were analyzed at a State certified laboratory and the results are attached for your review. The laboratory results indicate that the POE influent (untreated water) contained methyl tert-butyl ether (MTBE) at a concentration of 29 parts per billion (PPB). The current North Carolina drinking water standard for MTBE is 20 PPB. The compound 1,2-Dichloroethane was detected at 5.2 PPB. The current North Carolina drinking water standard for 1,2-Dichloroethane is 0.4 PPB. The compound isopropyl ether (IPE) was detected at 33 PPB. The current North Carolina drinking water standard for IPE is 70 PPB. No other targeted compounds were detected at concentrations that exceeded the laboratory detection limits in the POE influent. The laboratory results of the POE effluent sample (treated water) collected on February 28, 2017 indicate that none of the targeted petroleum compounds were detected at concentrations that exceed the laboratory detection limits. Only chloromethane was detected at a concentration of 0.8 PPB, which is below the 2L Groundwater Standard of 3 PPB. Chloromethane is not a petroleum-related contaminant and its presence is most likely associated with the supply well chlorination. Pyramid will continue to monitor concentrations of chloromethane in the POE system. The POE effectively removed the petroleum contaminants prior to water use. Maintenance of the POE treatment system will continue to be performed on a quarterly basis. If you have any questions, please call Pyramid at (336) 335-3174. Thank you for your cooperation with this project. Sincerely, Project Manager Attachments – Laboratory Report P.O. Box 16265 • Greensboro, NC 27416 503 Industrial Ave • Greensboro, NC 27406 Phone (336)335-3174 • Fax (336)691-0648 • Toll Free (866)545-9507 Email: Info@pyramidenvironmental.com www.pyramidenvironmental.com March 29, 2017 Mr. Ricky Lassiter 2773 Union Ridge Road Burlington, NC 27217 RE: Supply Well Analytical Results 2773 Union Ridge Road, Burlington, NC NCDEQ Incident #12913 Former Harold Smith Grocery Pyramid Project 2016-339 Dear Mr. Lassiter: As directed by the NCDEQ and T.A.C., Inc., Pyramid Environmental has continued to collect samples from your water supply well located at 2773 Union Ridge Road. The work is being performed as part of the ongoing assessment of the referenced underground storage tank release. The results of the water analyses are presented below. On February 28, 2017, Pyramid collected a groundwater sample from your supply well. The sample is designated as SW-2773. The groundwater samples were analyzed at a State certified laboratory and the results are attached for your review. The laboratory results showed the presence of methyl tert-butyl ether (MTBE) at a concentration of 1.8 parts per billion (PPB), isopropyl ether (IPE) at a concentration of 2 PPB, and 1,2-Dichloroethane at a concentration of 0.59 PPB. Respectively the current North Carolina drinking water standard for these compounds are 20 PPB, 70 PPB, and 0.4 PPB. Since the residence is provided with bottled water, the potential for exposure from the detected petroleum compounds is reduced. In the past, Pyramid has requested that the NC DEQ Central Office perform a Health Risk Evaluation (HRE) for this well. Please let us know when you receive the HRE letter from the DEQ regarding your well as they do not always copy us on the HRE letters. T.A.C./Pyramid will continue to monitor the petroleum concentrations for this water supply well on a quarterly basis. If you have any questions, please call Mike Jones (336) 335-3174. Thank you for your cooperation with this project. Sincerely, Project Manager Attachments – Laboratory Report