WS-3891_12913_CA_RMR_20160505

TABLE OF CONTENTS
1.0 INTRODUCTION .............................................................................. 1
1.1 SITE INFORMATION .................................................................................................. 1 1.2 ADJOINING PROPERTIES AND POTENTIAL RECEPTORS ............................................. 1 1.3 SITE HYDROLOGY & GEOLOGY ............................................................................... 2 1.4 PREVIOUS REPORTS ................................................................................................. 2
2.0 GROUNDWATER SAMPLING....................................................... 3
2.1 MONITORING WELL SAMPLING ................................................................................ 3
2.2 POTABLE WATER SUPPLY WELL SAMPLING ............................................................ 3
3.0 TREATMENT SYSTEM OPERATIONAL STATUS ................... 4
3.1 SYSTEM OPERATIONS .............................................................................................. 4 3.2 CONTAMINATED SOIL REMOVAL ............................................................................. 5 3.3 SYSTEM UPDATE ...................................................................................................... 6
4.0 SOIL & GROUNDWATER ASSESSMENT ................................... 6
4.1 GROUNDWATER ANALYTICAL RESULTS .................................................................. 6 4.2 SUPPLY WELL ANALYTICAL RESULTS ..................................................................... 7
5.0 CONCLUSIONS & RECOMMENDATIONS ................................ 9
6.0 CLOSURE ........................................................................................... 9

Page I
TABLE OF CONTENTS (Continued)
FIGURES:
1. Topographic Map
2. Site Map 3a. Adjoining Properties and Water Supply Wells 3b. Adjoining Properties and Water Supply Wells 4. Potentiometric Surface Map (2/29/2016)
5. MTBE Isoconcentration Map (2/29/2016)
6. 1,2-Dichloroethane Isoconcentration Map (2/29/2016) 7. Remediation System Layout Map (1/16/12) TABLES:
1. Monitoring Well Construction Details 2. Groundwater Elevation Data 3. Monitoring Well Analytical Results 4. Water Supply Well Analytical Results
5. System Operation Parameters
APPENDICES: A. Groundwater Laboratory Report & Chain of Custody
B. Supply Well Results Letter (POE)
C. Recent O&M Activities D. Supply Well Sampling Data from Lassiter SW

Page II
ACRONYMS

BLS ................Below Land Surface
BTEX ............Benzene, Toluene, Ethylbenzene, & Xylenes
CFR ................Code of Federal Regulations
COC ...............Chain of Custody
CSA ................Comprehensive Site Assessment
DEQ ...............Department of Environmental Quality
EPH ................Extractable Petroleum Hydrocarbons
GCLs ..............Gross Contaminant Levels
HASP .............Health & Safety Plan
MADEP..........Massachusetts Department of Environmental Protection
MSCC ............Maximum Soil Contaminant Concentration
MTBE ............Methyl Tertiary Butyl Ether
µg/L ................Micrograms per Liter
mg/kg .............Milligrams per kilogram
MW ................Monitoring Well
NCAC ............North Carolina Administrative Code
O&M ..............Operations and Maintenance
OSHA .............Occupational Safety and Health Administration
OVA ...............Organic Vapor Analyzer
PPM................Parts Per Million
PID .................Photo-ionization Detector
P&ID ..............Process & Instrumentation Diagram
PVC ................Poly-vinyl Chloride
QA/QC ...........Quality Assurance / Quality Control
SCFM .............Standard Cubic Feet per Minute
SVE ................Soil Vapor Extraction
SW..................Water Supply Well
UST ................Underground Storage Tank
US EPA ..........United States Environmental Protection Agency
VPH................Volatile Petroleum Hydrocarbons

Page III
Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 1 Pyramid Project # 2016-004 04/20/2016
ACTIVE REMEDIATION MONITORING REPORT Harold Smith Grocery
Burlington, North Carolina
1.0 INTRODUCTION
1.1 Site Information SITE NAME: Harold Smith Grocery ADDRESS: 2774 Union Ridge Road CITY: Burlington, NC
COUNTY: Alamance
CURRENT PROPERTY OWNER: Jessica Alton CURRENT PROPERTY USE: Inactive Store (used as storage) OWNER OF USTs: TAC, Inc. (All USTs were removed in 1994) RESPONSIBLE PARTY: TAC, Inc.
NCDEQ UST FACILITY ID: 0-024148
GROUNDWATER INCIDENT NO.: 12913 SITE RANKING: H755E UNDERGROUND STORAGE TANKS (USTs)
(gallons)
1 550 Kerosene Removed 8/01/94
2 550 Gasoline Removed 8/01/94
3 550 Gasoline Removed 8/01/94
4 1,000 Gasoline Removed 8/01/94
FIGURES: Figure 1: Topographic Map
Figure 2: Site Map Figure 3a: Adjoining Properties and Water Supply Wells Figure 3b: Adjoining Properties and Water Supply Wells
1.2 Adjoining Properties and Potential Receptors ADJOINING PROPERTY USE: Residential/Agricultural PUBLIC WATER AVAILABILITY: Unavailable
SUPPLY WELLS (SW) WITHIN 1000 FEET: Yes (see Figure 3a/b)
SW IMPACTED ABOVE NCAC 2L STANDARDS: Yes, SW 2765 Union Ridge Rd. ( POE system ) Yes, SW 2773 Union Ridge Rd. (Bottled Water) NEAREST SURFACE WATER: Intermittent Creek – 500-600’ SE
BASEMENTS: None
SUBSURFACE UTILITIES: None near source area
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1.3 Site Hydrology & Geology GEOLOGIC PROVINCE: Carolina Slate Belt
BEDROCK TYPE: Felsic Intrusive Complex
DEPTH TO BEDROCK: 25-38 feet BGS (below ground surface) CURRENT DEPTH TO WATER TABLE: 4.93 – 9.41 feet BGS (2/29/16) HISTORIC GW FLUCTUATIONS: Over the past 15 years, the groundwater has fluctuated in the source area from 5-15 feet BGS
POTENTIOMETRIC GRADIENT: Southeast ~ 0.025 ft. /ft.
HYDRAULIC CONDUCTIVITY (K): 6.17–6.25 x 10-7 ft. /sec. GROUNDWATER VELOCITY: ~0.4–1.3 feet/year
1.4 Previous Reports
REPORT TITLE CONSULTANT DATE OF REPORT COMMENTS
Pyramid Environmental 9/20/96
Pyramid Environmental 1/30/97 Original CAP report
Pyramid Environmental
Pyramid Environmental 11/99 to 01/13 Received by NCDEQ
Soil Cleanup Report Pyramid Environmental 5/31/2011 Received by NCDEQ
Active Rem. Mon. Report Pyramid Environmental Received by NCDEQ
Active Rem. Mon. Report Pyramid Environmental 8/10/15 Received by NCDEQ
Active Rem. Mon. Report Pyramid Environmental 12/08/15 Received by NCDEQ
Active Rem. Mon. Report Pyramid Environmental 1/10/16 Received by NCDEQ
Active Rem. Mon. Report Pyramid Environmental 5/04/16 Current Report

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2.0 GROUNDWATER SAMPLING
2.1 Monitoring Well Sampling On March 2, 2016, selected monitoring wells at the Harold Smith Site were sampled. WELLS SAMPLED: MW-1A, MW-3, MW-4, MW-5, MW-6, MW-7, MW-9, MW-10,
MW-11, MW-12, MW-13 and MW-15A LAB ANALYSES: EPA Method 6200B FREE PRODUCT: No free product has been observed on this site.
TABLES & GRAPHS: Table 1: Monitoring Well Construction Details Table 2: Groundwater Elevation Data Table 3: Monitoring Well Analytical Results FIGURES: Figure 4: Potentiometric Surface Map Figure 5: MTBE Concentration Map Figure 6: 1, 2-Dichloroethane Isoconcentration Map LABORATORY REPORT & CHAIN-OF-CUSTODY: Appendix A
FIELD PROCEDURES: Field procedures were performed as outlined in the DEQ July 15, 2008 and May 1, 2012 updates publication “Guidelines for Sampling” under the UST Section.

2.2 Potable Water Supply Well Sampling SAMPLING DATE: February 29, 2016 WELLS SAMPLED: 2765 INF, 2765 MID, 2765 EFF, 2768B, 2760, 2773, 2774, and 2779
The house at 2779 Union Ridge Road no longer uses the supply well in the front yard, but uses the well located on an adjacent eastern property. The property at 2768 Union Ridge Road uses the supply well in the back yard and is automatically switched to the well in the front yard (2768-A) if the water level gets too low.
LAB ANALYSES: EPA Method 6200B TABLES: Table 4: Water Supply Well Analytical Results FIGURES: Figure 3 a/b: Adjoining Properties and Water Supply Wells.
LABORATORY REPORTS & CHAINS-OF-CUSTODY: Appendix A
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FIELD PROCEDURES: Field procedures were performed as outlined in the DEQ July 15,
2008 and May 1, 2012 updates publication “Guidelines for Sampling” under the UST Section. *NOTE* Supply wells are named by the address of the residence they serve and not the property
owner. All supply well addresses sampled are on Union Ridge Road. Mr. James McMillan
requested that Pyramid inform him of the POE system analytical results after each sampling. The well analytical evaluation letter is presented in Appendix B.
3.0 TREATMENT SYSTEM OPERATIONAL STATUS
3.1 System Operations The air sparging (AS) and soil vapor extraction (SVE) treatment system for the Harold Smith Grocery site began operation in July 1999 and operated through 2004 when it was shut down. The system was restarted in February 2005 and the system was operational through October
2005. Repairs were made to the system and the remediation system was officially restarted on
February 8, 2006. The system ran intermittently during the first quarter of 2006, needing minor repairs. System operation was interrupted by electrical power interruptions (strong storms) tripping circuit breakers. In August 2006, the system electrical contacts were found to be completely melted. The electrical components were replaced after pre-approval, and tested. The
motor of the air-sparge compressor would not operate, and the electric motor was found to be
locked up. Pyramid contacted the equipment manufacturer and priced the replacement items necessary to get the air-sparge system running again. The SVE system continued to run after the replacement of the circuit breakers.
In March 2007 the rebuilt air sparge motor was put back in service. The restored compressor
operated from March 2007 through June 2008. At this time, the air-sparge compressor needed to be replaced. The air sparge motor was replaced with a more serviceable model on October 7, 2008. The carbon vanes were changed by Pyramid in February 2010. The air sparge system was operational during the 1st quarter of 2011. The system ceased operating in March 2011 to allow
for the soil excavation. Since the system operation ceased, DO concentrations dropped and
Pyramid recommended continued air sparging operation to speed site cleanup. In January 2012, the air sparge system was restarted using the selected remaining air sparge wells. In 2013, the system was upgraded to include deeper AS wells and a higher pressure compressor.
The system was operational for most of the fourth quarter of 2014, with the exception of short
period of time in December when the system was down due a damaged compressor drive belt. The damaged belt was discovered on 12/12/14 and replaced on 12/19/14 and the system was re-started.
Since the compressor drive belt was repaired, the system performed optimally in 2015 with few
interruptions in operation. In January 2016, the system was down when the technician performed the monthly O&M visit. The technician reset the system and it was operational upon departure. In February 2016, the
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system was down again. The technician tried to reset the system, but the operation failed. A
damaged electric drive motor was causing the power to trip. On February 23, 2016, a preapproval was sent to the DEQ requesting equipment, labor, and mileage to replace the electric drive motor. The preapproval was returned on February 25, 2016 and the work to replace the electric drive motor is scheduled for April of 2016.

A summary of the operations and maintenance activities performed from January through March 2016 is presented in Appendix C.
3.2 Contaminated Soil Removal In March 2009, Pyramid collected risk-based soil samples from several soil borings and added several monitoring wells. The additional assessment was conducted to investigate the soils in the
area of the former pump island and provide additional monitoring wells to assess the source area
for regulatory incident closure. The highest groundwater concentrations have been in MW-1 and MW-1A throughout the remediation period. As a result of the additional investigations, an area approximately 40 feet by 20 feet was identified as containing soil concentrations greater than Soil-to-Groundwater (STGW) standards. Only the soil boring directly at the location of the
former pump island showed concentrations above residential Maximum Soil Contaminant
Concentrations (MSCCs). The DEQ requested that Pyramid evaluate soil excavation as a way to help move the site toward regulatory closure. After the excavation plan was preapproved by the DEQ, Pyramid implemented the excavation plan.
In May 2011, Pyramid supervised the excavation of petroleum contaminated soils at the Harold
Smith site in Burlington, NC. The goal of the soil excavation was to remove volatile petroleum hydrocarbons from the smear zone (between 5 and 15 feet BLS) to help reduce groundwater contamination. Based on certified weight tickets, 483.69 tons of petroleum-contaminated soil was removed. Pyramid requested pre-approval to implement oxygen release compound in
addition to the excavation, but DEQ denied the request. The laboratory results of the post
excavation soil samples collected indicate that all of the contaminated soils above the residential MSCCs were removed. The remaining contamination detected at the site was above the STGW MSCCs and well below
the residential standards. The remaining STGW concentrations were located underneath the store
building, along the northern property boundary, and on the eastern edge of the property near Union Ridge Road. Because of the structures, roads, and utilities, additional soil excavation was not feasible or recommended.
After the excavation of contaminated soil, Pyramid installed monitoring wells MW-1A and MW-15A to assess the groundwater in the source area. The latest results of these new wells (MW-1A and MW-15A) since installation are included in Section 4.0 with past results located in Table 3.
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3.3 System Update

FIGURES: Figure 7: Remediation System Layout Map To prevent the migration of the contaminant plume, protect nearby supply wells, and speed up remediation, the current air sparge (AS) and soil vapor extraction (SVE) system was updated in October 2012. Additional wells were added to the air sparge segment of the remediation system.
Seven deeper air sparge wells were added to surround the existing petroleum contaminant plume. The additional wells prevent contaminant plume migration and provide additional air flow for petroleum hydrocarbons volatilization. Along with the AS remediation update, the SVE system was repaired after it was damaged during the soil excavation in May 2011. A map of the Remediation System Layout is shown in Figure 7.

4.0 SOIL & GROUNDWATER ASSESSMENT
4.1 Groundwater Analytical Results The results of the February 29 and March 2, 2016 sampling events showed that remaining
petroleum contaminants were detected at low concentrations. All of the reported concentrations
are listed in micrograms per liter (µg/L). The detected concentration of benzene in MW-1A (22 µg/L) exceed the 2L groundwater standard of 1.0 µg/L. This is the highest concentration of benzene detected in MW-1A since March 2013. The detected concentrations of 1,2-Dichloroethane (1,2-DCA) in MW-1A (7.3 µg/L), SW-2773 (2 µg/L), and SW-2765 (9.2 µg/L) also exceed the 2L groundwater standard of 0.4 µg/L. The concentrations of targeted compounds
for this sampling event have slightly increased in all of the monitoring wells. The highest concentrations found for this sampling event are shown below. Concentrations above NCAC 2L groundwater standards are shown in bold and the associated well numbers are shown in parentheses. All of the reported concentrations are listed in micrograms per liter (µg/L).
• Benzene 22 µg/L (MW-1A)
• Toluene 20 µg/L (MW-15A)
• Ethylbenzene 15 µg/L (MW-15A)
• Total Xylenes 173 µg/L (MW-15A)
• MTBE 60 µg/L (SW-2765 Influent)
• Isopropyl Ether (IPE) 76 µg/L (SW-2765 Influent)
• 1,2-Dichloroethane 9.2 µg/L (SW-2765 Influent)
• Naphthalene 47 µg/L (MW-1A)
Over the past 17 years of groundwater and soil remediation, the general concentration trends
demonstrated in the groundwater monitoring wells have been decreasing and are now approaching regulatory closure. The benzene concentration in MW-1A has decreased from over 8,000 µg/L in 1998 to 22 µg/L
for the current monitoring period. The benzene concentration in MW-1A has been below or
slightly above 1.0 µg/L since November 2013; however, the March 2016 sampling event showed
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a concentration of 22 µg/L. This may be due to the remediation system (Air-Sparging) being
down at the present time. The MTBE concentration in MW-1A has decreased from 610 µg/L in 1999 to 8.5 µg/L for the current monitoring period. The monitoring well samples from MW-1A also showed a concentration of 1,2-Dichloropropane (1.5 µg/L) above the 2L Standard of 0.6 µg/L. In previous sampling events, 1,2-Dichloropropane had not been detected at a
concentration above the laboratory detection limits. Pyramid will continue to monitor the 1,2-
Dichloropropane concentrations for this well. Concentrations of 1,2-dichloroethane were detected in MW-1A, SW-2773, and the influent for SW-2765 and remain above the 2L Standard.

As shown in Table 3, the groundwater contaminant concentrations in the source area decreased significantly after the contaminated soil excavation was performed in May 2001. In planning for the soil excavation project, Pyramid recommended that the DEQ consider the placement of oxygen-release compounds in the open excavation to help clean up the site. Since cleanup will
have to be to stringent the NCAC 2L Standards, any remedial process that can help reach
regulatory closure more quickly should be considered by the DEQ. Pyramid’s request was not approved for Trust Fund reimbursement, and no oxygen-release compounds were used in the excavation. In the future, the Trust Fund should consider reimbursing the use of oxygen-release compounds while excavations are open to help reduce the overall costs for petroleum incident
closures. Active soil and groundwater remediation are needed to reduce the remaining petroleum
contaminant concentrations in the groundwater.
4.2 Supply Well Analytical Results Supply well sampling was conducted on February 29, 2016 as required by the State. Pyramid sampled six supply wells 2765, 2768B, 2760, 2774, 2773, and 2779. Influent, mid-fluent and effluent samples were collected from the point of entry (POE) treatment system for SW-2765.
All samples were collected using clean, disposable nitrile gloves, preserved in laboratory
provided containers, packed in ice and shipped to Prism Analytical Laboratories for analysis using EPA Method 6200B. Supply Well SW-2765 – POE System Groundwater pumped from the supply well at address 2765 (SW-2765) is treated by a Point-of-Entry (POE) treatment system installed in 2000. The POE system consists of particulate and carbon filters that remove petroleum from the groundwater. This residential treatment system has shown effective groundwater treatment since 2000. The laboratory results of treated water samples collected from the supply well in February 2016 show no detections of petroleum
contaminants. For the untreated water (influent) from SW-2765, MTBE (60 µg/L), IPE (76 µg/L), and 1,2-dichloroethane (9.2 µg/L) were detected above their respective NCAC 2L Groundwater Standards. No petroleum hydrocarbon concentrations were detected in the treated water (effluent) showing effective POE treatment. Table 4 shows the recent supply well analytical
results. A copy of the laboratory report and chain-of-custody form is presented in Appendix A.

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Supply Well SW-2773, Mr. Lassiter The most recent supply well sampling at the Lassiter residence (SW2773) showed several detections of petroleum contaminants. The following paragraphs describe the two supply well sample analyses conducted in February and April 2016. The initial samples were collected in late February and reported in late March. The February lab
results showed a concentration of (2.0 µg/L) of the compound 1,2-Dichloroethane (1,2-DCA). At a concentration above the NCAC 2L Groundwater Standard of 0.4 µg/L. Two other petroleum compounds, Isopropyl Ether (IPE) and Methyl Tert-Butyl ether (MTBE) were also detected at concentrations below the 2L standards. This supply well has shown few petroleum impacts in the past several years.
Based on this initial detection, Pyramid sampled the supply well again on April 20, 2016. Confirmation sampling was warranted and the results were similar to the initial results. The laboratory report for the April 20, 2016 sampling of SW2773 is presented in Appendix D. Results from the April groundwater analyses for SW2773 showed a 1,2-DCA concentration of
1.2 µg/L which is still above the NCAC 2L Groundwater Standard. The confirmation sample also showed concentration of the petroleum compounds IPE and MTBE at concentrations below the 2L standards.
A comparison of the detections in SW2773 with those detected in untreated water from SW2765,
indicate that similar compounds were detected; however, the concentrations in SW2765 influent were higher. The Lassiter residence is on bottled water at this time and has been using the account regularly.
Since the residence is provided with bottled water at this time, the potential for exposure was
mitigated. Pyramid requests that the NC DEQ request a Health Risk Evaluation (HRE) from the central office for this well. TAC/Pyramid will continue to monitor the petroleum concentrations for this water supply well.

Supply Wells 2765B, 2774, 2760, & 2779 Laboratory analytical results show that there were no other detectable petroleum hydrocarbon concentrations in the supply well samples collected from wells 2768B, 2774, 2760, and 2779.

Supply Well Recommendations Pyramid recommends continued POE treatment of supply well 2765, continued sampling of the closest supply wells (2765 & 2773) on a quarterly basis, and continued sampling of the wells further from the source area (2761, 2768, 2774, and 2779) on an annual basis. The next quarterly
sampling event will be in June 2016.

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5.0 CONCLUSIONS & RECOMMENDATIONS
Pyramid has completed the directed operation & maintenance and groundwater monitoring at the
Harold Smith Grocery. Based on the current groundwater concentrations of benzene, MTBE,
IPE, and 1,2-Dichloroethane remaining above the 2L groundwater standard, the site remains high risk. The remediation goal is to reduce dissolved groundwater contamination below 2L standards to protect local water supply well users.
• The contaminated soil excavation was completed in May 2011. Contaminated soil beneath the NC DOT Right-of-Way and under the store building was unable to be removed. Since petroleum concentrations that exceed the STGW levels remain under the building and near the roadway, continued soil remediation using the SVE system is
recommended at the site.

• Based on the risk to private well users, Pyramid recommended a new air-sparge system with deeper air sparge wells to enhance the groundwater cleanup. This new system was designed, bid, pre-approved, and built from October 2012 through April 2013. The
system was successfully started on April 3, 2013. The new system has shown significant
reductions in the remaining petroleum contaminants.
• The most recent supply well sampling showed petroleum contamination in two of the
closest downgradient water supply wells. One of the wells is on a POE treatment system,
and the other residence is supplied with bottled water. The petroleum concentrations in the local water supply wells will continue to be monitored.
• The continued presence of concentrations of petroleum contaminants in monitoring wells
MW-1A, MW-15A, and SW-2765 show that groundwater contamination remains above regulatory closure levels.
• Continued groundwater remediation and monitoring is recommended for the Harold
Smith site. The next sampling of the monitoring wells will be conducted in June 2016.
6.0 CLOSURE
This report is prepared for and made available solely for the use of T.A.C, Inc. and the NCDEQ, and the contents thereof may not be used or relied upon by any other person without the express written consent and authorization of Pyramid Environmental & Engineering, P.C. The observations, conclusions, and recommendations documented in this report are based on site
conditions and information reviewed at the time of the investigation. Pyramid Environmental & Engineering, P.C. appreciates the opportunity to provide this environmental service.

FIGURES

TABLES

TABLE 1 Monitoring Well Construction Details Harold Smith Grocery Incident #12913 Union Ridge Road, Burlington, North Carolina
WELL INSTALLED DEPTH BEDROCK CASING INTERVAL INTERVAL INTERVAL INTERVAL INTERVAL
MW-1 11/21/94 20’ NBE NA 0-10’ 10-20’ 0-6’ 6-7.5 7.5-20’
MW-1A 6/27/11 24’ NBE NA 0-4’ 4-24’ 0-1’ 1-3’ 3-24’
MW-2 10/11/95 25’ 25’ NA 0-10’ 10-20’ 0-6’ 6-8’ 8-20’
MW-3 10/11/95 22’ NBE NA 0-7’ 7-22’ 0-3’ 3-5’ 5-22’
MW-4 11/8/95 20’ NBE NA 0-5’ 5-20’ 0-2’ 2-4’ 4-20’
MW-5 11/8/95 20’ NBE NA 0-5’ 5-20’ 0-2’ 2-4’ 4-20’
MW-6 1/2/96 53’ 25’ 0-30’ 0-43’ 43-53’ 0-38’ 38-41’ 41-53’
MW-7 1/3/96 13.8’ NBE NA 0-3.8’ 3.8-13.8’ 0-0.5’ 0.5-1.5’ 1.5-13.8’
MW-8 5/6/96 14.3’ 15’ NA 0-4.3’ 4.3-14.3’ 0-1.8’ 1.8-3.3’ 3.3-14.3’
MW-9 5/6/96 15’ NBE NA 0-5’ 5-15’ 0-2.5’ 2.5-4’ 6/4-15’
MW-10 11/30/99 20’ NBE NA 0-5’ 5-20’ 0.5-2’ 2-4’ 4-20’
MW-11 7/25/00 20’ NA NA 0-5’ 5-20’ 0.5-2’ 2-4’ 4-20’
MW-12 11/6/01 30’ NBE NA 0-10’ 10-30’ 0-6’ 6-8’ 8-30’
MW-13 3/5/09 25’ NBE NA 0-5’ 5-25’ 0-1’ 1-3’ 3-25’
MW-14 3/5/09 25’ NBE NA 0-5’ 5-25’ 0-1’ 1-3’ 3-25’
MW-15 3/5/09 25’ 24’ NA 0-5’ 5-25’ 0-1’ 1-3' 3-25’
MW-15A 6/27/11 24’ NBE NA 0-4’ 4-24’ 0-1’ 1-3’ 3-24’
TS-1 12/17/99 15’ NBE NA 0-5’ 5-15’ 0-2’ 2-4’ 4-15’
TS-2 12/17/99 15’ NBE NA 0-5’ 5-15’ 0-2’ 2-4’ 4-15’
TS-3 12/17/99 15’ NBE NA 0-5’ 5-15’ 0-2’ 2-4’ 4-15’
ALL MONITORING WELLS HAVE 2” PVC CASING/RISER AND 2” PVC SCREEN WITH 0.01” SLOTS. OUTER CASING FOR TYPE III WELL IS 6” PVC. NBE = NO BEDROCK ENCOUNTERED. NA = NOT APPLICABLE. SHADED WELLS ARE CLOSED.
Page 1 of 6
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
MW-1A 06-30-11 94.650 12.24 0.00 0.00 0.00 12.24 82.41
09-8-11 94.650 13.59 0.00 0.00 0.00 13.59 81.06
12-8-11 94.650 13.49 0.00 0.00 0.00 13.49 81.16
03-13-12 94.650 13.49 0.00 0.00 0.00 12.35 82.30
06-5-12 94.650 12.14 0.00 0.00 0.00 12.14 82.51
09-11-12 94.650 13.22 0.00 0.00 0.00 13.22 81.43
12-12-12 94.650 13.85 0.00 0.00 0.00 13.85 80.80
03-12-13 94.650 11.83 0.00 0.00 0.00 11.83 82.82
05-29-13 94.650 10.44 0.00 0.00 0.00 10.44 84.21
09-10-13 94.650 8.96 0.00 0.00 0.00 8.96 85.69
11-6-13 94.650 10.96 0.00 0.00 0.00 10.96 83.69
03-19-14 94.650 8.07 0.00 0.00 0.00 8.07 86.58
06-26-14 94.650 8.72 0.00 0.00 0.00 8.72 85.93
08-22-14 94.650 10.13 0.00 0.00 0.00 10.13 84.52
11-7-14 94.650 12.00 0.00 0.00 0.00 12.00 82.65
03-4-15 94.650 11.21 0.00 0.00 0.00 11.21 83.44
06-25-15 94.650 11.48 0.00 0.00 0.00 11.48 83.17
09-22-15 94.650 13.50 0.00 0.00 0.00 13.50 81.15
12-9-15 94.650 10.67 0.00 0.00 0.00 10.67 83.98
03-2-16 94.650 7.96 0.00 0.00 0.00 7.96 86.69
MW-3 09-9-09 93.065 12.03 0.00 0.00 0.00 12.03 81.04
12-3-09 93.065 10.40 0.00 0.00 0.00 10.40 82.67
03-24-10 93.065 7.34 0.00 0.00 0.00 7.34 85.73
06-24-10 93.065 8.07 0.00 0.00 0.00 8.07 85.00
09-8-10 93.065 9.62 0.00 0.00 0.00 9.62 83.45
12-10-10 93.065 10.77 0.00 0.00 0.00 10.77 82.30
03-8-11 93.065 10.60 0.00 0.00 0.00 10.60 82.47
06-30-11 93.065 10.74 0.00 0.00 0.00 10.74 82.33
09-8-11 93.065 12.16 0.00 0.00 0.00 12.16 80.91
12-8-11 93.065 12.06 0.00 0.00 0.00 12.06 81.01
03-13-12 93.065 13.49 0.00 0.00 0.00 10.52 82.55
06-5-12 93.065 10.71 0.00 0.00 0.00 10.71 82.36
09-11-12 93.065 11.79 0.00 0.00 0.00 11.79 81.28
12-12-12 93.065 12.37 0.00 0.00 0.00 12.37 80.70
03-12-13 93.065 10.53 0.00 0.00 0.00 10.53 82.54
05-29-13 93.065 9.04 0.00 0.00 0.00 9.04 84.03
09-10-13 93.065 7.53 0.00 0.00 0.00 7.53 85.54
11-6-13 93.065 8.88 0.00 0.00 0.00 8.88 84.19
03-19-14 93.065 6.69 0.00 0.00 0.00 6.69 86.38
06-26-14 93.065 7.46 0.00 0.00 0.00 7.46 85.61
08-22-14 93.065 8.82 0.00 0.00 0.00 8.82 84.25
11-7-14 93.065 10.84 0.00 0.00 0.00 10.84 82.23
03-4-15 93.065 8.51 0.00 0.00 0.00 8.51 84.56
06-25-15 93.065 10.22 0.00 0.00 0.00 10.22 82.85
09-22-15 93.065 12.35 0.00 0.00 0.00 12.35 80.72
12-9-15 93.065 9.42 0.00 0.00 0.00 9.42 83.65
03-2-16 93.065 6.54 0.00 0.00 0.00 6.54 86.53
MW-4 09-9-09 91.470 10.81 0.00 0.00 0.00 10.81 80.66
12-3-09 91.470 9.11 0.00 0.00 0.00 9.11 82.36
03-24-10 91.470 6.10 0.00 0.00 0.00 6.10 85.37
06-24-10 91.470 6.76 0.00 0.00 0.00 6.76 84.71
09-8-10 91.470 8.41 0.00 0.00 0.00 8.41 83.06
12-10-10 91.470 9.55 0.00 0.00 0.00 9.55 81.92
03-8-11 91.470 9.37 0.00 0.00 0.00 9.37 82.10
06-30-11 91.470 9.53 0.00 0.00 0.00 9.53 81.94
09-8-11 91.470 11.12 0.00 0.00 0.00 11.12 80.35
12-8-11 91.470 10.81 0.00 0.00 0.00 10.81 80.66
03-13-12 91.470 13.49 0.00 0.00 0.00 8.58 82.89
06-5-12 91.470 9.50 0.00 0.00 0.00 9.50 81.97
09-11-12 91.470 10.67 0.00 0.00 0.00 10.67 80.80
12-12-12 91.470 11.15 0.00 0.00 0.00 11.15 80.32
03-12-13 91.470 8.84 0.00 0.00 0.00 8.84 82.63
05-29-13 91.470 7.80 0.00 0.00 0.00 7.80 83.67
09-10-13 91.470 6.33 0.00 0.00 0.00 6.33 85.14
11-6-13 91.470 7.70 0.00 0.00 0.00 7.70 83.77
03-19-14 91.470 5.51 0.00 0.00 0.00 5.51 85.96
06-26-14 91.470 6.18 0.00 0.00 0.00 6.18 85.29
08-22-14 91.470 7.58 0.00 0.00 0.00 7.58 83.89
11-7-14 91.470 9.62 0.00 0.00 0.00 9.62 81.85
03-4-15 91.470 7.55 0.00 0.00 0.00 7.55 83.92
06-25-15 91.470 8.97 0.00 0.00 0.00 8.97 82.50
09-22-15 91.470 11.11 0.00 0.00 0.00 11.11 80.36
12-9-15 91.470 8.11 0.00 0.00 0.00 8.11 83.36
03-2-16 91.470 5.29 0.00 0.00 0.00 5.29 86.18
TABLE 2
Union Ridge Road, Burlington, North carolina
Groundwater Elevation Data
Harold Smith GroceryIncident #12913
Page 2 of 6
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
09-9-09 95.045 12.81 0.00 0.00 0.00 12.81 82.24
12-3-09 95.045 6.35 0.00 0.00 0.00 6.35 88.70
03-24-10 95.045 6.63 0.00 0.00 0.00 6.63 88.42
06-24-10 95.045 8.25 0.00 0.00 0.00 8.25 86.80
09-8-10 95.045 10.34 0.00 0.00 0.00 10.34 84.71
12-10-10 95.045 9.78 0.00 0.00 0.00 9.78 85.27
03-8-11 95.045 7.20 0.00 0.00 0.00 7.20 87.85
06-30-11 95.045 8.53 0.00 0.00 0.00 8.53 86.52
09-8-11 95.045 12.62 0.00 0.00 0.00 12.62 82.43
12-8-11 95.045 8.74 0.00 0.00 0.00 8.74 86.31
03-13-12 95.045 13.49 0.00 0.00 0.00 10.94 84.11
06-5-12 95.045 10.87 0.00 0.00 0.00 10.87 84.18
09-11-12 95.045 11.98 0.00 0.00 0.00 11.98 83.07
12-12-12 95.045 13.20 0.00 0.00 0.00 13.20 81.85
03-12-13 95.045 7.32 0.00 0.00 0.00 7.32 87.73
05-29-13 95.045 9.38 0.00 0.00 0.00 9.38 85.67
09-10-13 95.045 8.16 0.00 0.00 0.00 8.16 86.89
11-6-13 95.045 9.53 0.00 0.00 0.00 9.53 85.52
03-19-14 95.045 2.87 0.00 0.00 0.00 2.87 92.18
06-26-14 95.045 7.78 0.00 0.00 0.00 7.78 87.27
08-22-14 95.045 9.06 0.00 0.00 0.00 9.06 85.99
11-7-14 95.045 11.16 0.00 0.00 0.00 11.16 83.89
03-4-15 95.045 1.70*0.00 0.00 0.00 1.70*93.35
06-25-15 95.045 10.78 0.00 0.00 0.00 10.78 84.27
09-22-15 95.045 13.05 0.00 0.00 0.00 13.05 82.00
12-9-15 95.045 7.19 0.00 0.00 0.00 7.19 87.86
03-2-16 95.045 4.93 0.00 0.00 0.00 4.93 90.12
MW-6 09-9-09 94.935 14.28 0.00 0.00 0.00 14.28 80.66
12-3-09 94.935 12.98 0.00 0.00 0.00 12.98 81.96
03-24-10 94.935 9.07 0.00 0.00 0.00 9.07 85.87
06-24-10 94.935 9.90 0.00 0.00 0.00 9.90 85.04
09-8-10 94.935 11.76 0.00 0.00 0.00 11.76 83.18
12-10-10 94.935 12.91 0.00 0.00 0.00 12.91 82.03
03-8-11 94.935 12.89 0.00 0.00 0.00 12.89 82.05
06-30-11 94.935 12.91 0.00 0.00 0.00 12.91 82.03
09-8-11 94.935 14.50 0.00 0.00 0.00 14.50 80.44
12-8-11 94.935 14.20 0.00 0.00 0.00 14.20 80.74
03-13-12 94.935 13.49 0.00 0.00 0.00 12.94 82.00
06-5-12 94.935 13.10 0.00 0.00 0.00 13.10 81.84
09-11-12 94.935 14.26 0.00 0.00 0.00 14.26 80.68
12-12-12 94.935 14.58 0.00 0.00 0.00 14.58 80.36
03-12-13 94.935 12.72 0.00 0.00 0.00 12.72 82.22
05-29-13 94.935 11.38 0.00 0.00 0.00 11.38 83.56
09-10-13 94.935 9.65 0.00 0.00 0.00 9.65 85.29
11-6-13 94.935 11.29 0.00 0.00 0.00 11.29 83.65
03-19-14 94.935 8.58 0.00 0.00 0.00 8.58 86.36
06-26-14 94.935 9.39 0.00 0.00 0.00 9.39 85.55
08-22-14 94.935 11.01 0.00 0.00 0.00 11.01 83.93
11-7-14 94.935 12.99 0.00 0.00 0.00 12.99 81.95
03-4-15 94.935 12.11 0.00 0.00 0.00 12.11 82.83
06-25-15 94.935 12.43 0.00 0.00 0.00 12.43 82.51
09-22-15 94.935 14.50 0.00 0.00 0.00 14.50 80.44
12-9-15 94.935 11.53 0.00 0.00 0.00 11.53 83.41
03-2-16 94.935 8.40 0.00 0.00 0.00 8.40 86.54
MW-7 09-9-09 94.215 11.61 0.00 0.00 0.00 11.61 82.61
12-3-09 94.215 9.65 0.00 0.00 0.00 9.65 84.57
03-24-10 94.215 7.69 0.00 0.00 0.00 7.69 86.53
06-24-10 94.215 7.55 0.00 0.00 0.00 7.55 86.67
09-8-10 94.215 8.18 0.00 0.00 0.00 8.18 86.04
12-10-10 94.215 10.36 0.00 0.00 0.00 10.36 83.86
03-8-11 94.215 9.94 0.00 0.00 0.00 9.94 84.28
06-30-11 94.215 10.92 0.00 0.00 0.00 10.92 83.30
09-8-11 94.215 12.05 0.00 0.00 0.00 12.05 82.17
12-8-11 94.215 11.64 0.00 0.00 0.00 11.64 82.58
03-13-12 94.215 13.49 0.00 0.00 0.00 10.75 83.47
06-5-12 94.215 10.63 0.00 0.00 0.00 10.63 83.59
09-11-12 94.215 11.33 0.00 0.00 0.00 11.33 82.89
12-12-12 94.215 12.20 0.00 0.00 0.00 12.20 82.02
03-12-13 94.215 NG 0.00 0.00 0.00 0.00 NG
05-29-13 94.215 NG 0.00 0.00 0.00 0.00 NG
09-10-13 94.215 7.57 0.00 0.00 0.00 7.57 86.65
11-6-13 94.215 9.08 0.00 0.00 0.00 9.08 85.14
Page 3 of 6
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
06-26-14 94.215 7.47 0.00 0.00 0.00 7.47 86.75
08-22-14 94.215 8.70 0.00 0.00 0.00 8.70 85.52
11-7-14 94.215 10.60 0.00 0.00 0.00 10.60 83.62
03-4-15 94.215 9.40 0.00 0.00 0.00 9.40 84.82
06-25-15 94.215 9.96 0.00 0.00 0.00 9.96 84.26
09-22-15 94.215 11.76 0.00 0.00 0.00 11.76 82.46
12-9-15 94.215 9.20 0.00 0.00 0.00 9.20 85.02
03-2-16 94.215 6.88 0.00 0.00 0.00 6.88 87.34
MW-8 09-9-09 89.630 NG 0.00 0.00 0.00 0.00 NG
12-3-09 89.630 7.23 0.00 0.00 0.00 7.23 82.40
03-24-10 89.630 5.64 0.00 0.00 0.00 5.64 83.99
06-24-10 89.630 6.13 0.00 0.00 0.00 6.13 83.50
09-8-10 89.630 7.79 0.00 0.00 0.00 7.79 81.84
12-10-10 89.630 9.43 0.00 0.00 0.00 9.43 80.20
03-8-11 89.630 8.39 0.00 0.00 0.00 8.39 81.24
06-30-11 89.630 NG 0.00 0.00 0.00 0.00 NG
09-8-11 89.630 NG 0.00 0.00 0.00 0.00 NG
12-8-11 89.630 NG 0.00 0.00 0.00 0.00 NG
03-13-12 89.630 NG 0.00 0.00 0.00 0.00 NG
06-5-12 89.630 8.80 0.00 0.00 0.00 8.80 80.83
09-11-12 89.630 9.84 0.00 0.00 0.00 9.84 79.79
12-12-12 89.630 10.60 0.00 0.00 0.00 10.60 79.03
03-12-13 89.630 NG 0.00 0.00 0.00 0.00 NG
05-29-13 89.630 NG 0.00 0.00 0.00 0.00 NG
09-10-13 89.630 NG 0.00 0.00 0.00 0.00 NG
11-6-13 89.630 NG 0.00 0.00 0.00 0.00 NG
03-19-14 89.630 NG 0.00 0.00 0.00 0.00 NG
06-26-14 89.630 NG 0.00 0.00 0.00 0.00 NG
08-22-14 89.630 NG 0.00 0.00 0.00 0.00 NG
11-7-14 89.630 NG 0.00 0.00 0.00 0.00 NG
03-4-15 89.630 NG 0.00 0.00 0.00 0.00 NG
06-25-15 89.630 NG 0.00 0.00 0.00 0.00 NG
09-22-15 89.630 NG 0.00 0.00 0.00 0.00 NG
12-9-15 89.630 NG 0.00 0.00 0.00 0.00 NG
03-2-16 89.630 NG 0.00 0.00 0.00 0.00 NG
MW-9 09-9-09 94.770 14.21 0.00 0.00 0.00 14.21 80.56
12-3-09 94.770 12.76 0.00 0.00 0.00 12.76 82.01
03-24-10 94.770 8.91 0.00 0.00 0.00 8.91 85.86
06-24-10 94.770 9.79 0.00 0.00 0.00 9.79 84.98
09-8-10 94.770 11.70 0.00 0.00 0.00 11.70 83.07
12-10-10 94.770 12.89 0.00 0.00 0.00 12.89 81.88
03-8-11 94.770 12.79 0.00 0.00 0.00 12.79 81.98
06-30-11 94.770 NG 0.00 0.00 0.00 0.00 NG
09-8-11 94.770 14.34 0.00 0.00 0.00 14.34 80.43
12-8-11 94.770 14.09 0.00 0.00 0.00 14.09 80.68
03-13-12 94.770 13.49 0.00 0.00 0.00 11.82 82.95
06-5-12 94.770 NG 0.00 0.00 0.00 0.00 NG
09-11-12 94.770 14.15 0.00 0.00 0.00 14.15 80.62
12-12-12 94.770 NG 0.00 0.00 0.00 0.00 NG
03-12-13 94.770 12.60 0.00 0.00 0.00 12.60 82.17
05-29-13 94.770 11.20 0.00 0.00 0.00 11.20 83.57
09-10-13 94.770 9.50 0.00 0.00 0.00 9.50 85.27
11-6-13 94.770 11.16 0.00 0.00 0.00 11.16 83.61
03-19-14 94.770 8.18 0.00 0.00 0.00 8.18 86.59
06-26-14 94.770 9.30 0.00 0.00 0.00 9.30 85.47
08-22-14 94.770 10.88 0.00 0.00 0.00 10.88 83.89
11-7-14 94.770 12.92 0.00 0.00 0.00 12.92 81.85
03-4-15 94.770 12.00 0.00 0.00 0.00 12.00 82.77
06-25-15 94.770 12.27 0.00 0.00 0.00 12.27 82.50
09-22-15 94.770 14.37 0.00 0.00 0.00 14.37 80.40
12-9-15 94.770 11.48 0.00 0.00 0.00 11.48 83.29
03-2-16 94.770 8.28 0.00 0.00 0.00 8.28 86.49
MW-10 09-9-09 93.210 13.25 0.00 0.00 0.00 13.25 79.96
12-3-09 93.210 10.51 0.00 0.00 0.00 10.51 82.70
03-24-10 93.210 7.80 0.00 0.00 0.00 7.80 85.41
06-24-10 93.210 8.77 0.00 0.00 0.00 8.77 84.44
09-8-10 93.210 10.74 0.00 0.00 0.00 10.74 82.47
12-10-10 93.210 12.15 0.00 0.00 0.00 12.15 81.06
03-8-11 93.210 11.78 0.00 0.00 0.00 11.78 81.43
06-30-11 93.210 12.29 0.00 0.00 0.00 12.29 80.92
09-8-11 93.210 13.39 0.00 0.00 0.00 13.39 79.82
12-8-11 93.210 12.91 0.00 0.00 0.00 12.91 80.30
03-13-12 93.210 13.49 0.00 0.00 0.00 11.61 81.60
Page 4 of 6
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
09-11-12 93.210 13.10 0.00 0.00 0.00 13.10 80.11
12-12-12 93.210 13.29 0.00 0.00 0.00 13.29 79.92
03-12-13 93.210 10.93 0.00 0.00 0.00 10.93 82.28
05-29-13 93.210 10.03 0.00 0.00 0.00 10.03 83.18
09-10-13 93.210 8.61 0.00 0.00 0.00 8.61 84.60
11-6-13 93.210 10.11 0.00 0.00 0.00 10.11 83.10
03-19-14 93.210 6.68 0.00 0.00 0.00 6.68 86.53
06-26-14 93.210 8.43 0.00 0.00 0.00 8.43 84.78
08-22-14 93.210 10.00 0.00 0.00 0.00 10.00 83.21
11-7-14 93.210 11.98 0.00 0.00 0.00 11.98 81.23
03-4-15 93.210 10.66 0.00 0.00 0.00 10.66 82.55
06-25-15 93.210 11.35 0.00 0.00 0.00 11.35 81.86
09-22-15 93.210 13.44 0.00 0.00 0.00 13.44 79.77
12-9-15 93.210 10.42 0.00 0.00 0.00 10.42 82.79
03-2-16 93.210 6.95 0.00 0.00 0.00 6.95 86.26
MW-11 09-9-09 95.840 NG 0.00 0.00 0.00 0.00 NG
12-3-09 95.840 14.05 0.00 0.00 0.00 14.05 81.79
03-24-10 95.840 10.06 0.00 0.00 0.00 10.06 85.78
06-24-10 95.840 10.91 0.00 0.00 0.00 10.91 84.93
09-8-10 95.840 12.77 0.00 0.00 0.00 12.77 83.07
12-10-10 95.840 14.00 0.00 0.00 0.00 14.00 81.84
03-8-11 95.840 13.94 0.00 0.00 0.00 13.94 81.90
06-30-11 95.840 13.92 0.00 0.00 0.00 13.92 81.92
09-8-11 95.840 15.52 0.00 0.00 0.00 15.52 80.32
12-8-11 95.840 15.21 0.00 0.00 0.00 15.21 80.63
03-13-12 95.840 13.49 0.00 0.00 0.00 13.94 81.90
06-5-12 95.840 14.16 0.00 0.00 0.00 14.16 81.68
09-11-12 95.840 15.36 0.00 0.00 0.00 15.36 80.48
12-12-12 95.840 15.60 0.00 0.00 0.00 15.60 80.24
03-12-13 95.840 13.88 0.00 0.00 0.00 13.88 81.96
05-29-13 95.840 12.35 0.00 0.00 0.00 12.35 83.49
09-10-13 95.840 10.64 0.00 0.00 0.00 10.64 85.20
11-6-13 95.840 12.35 0.00 0.00 0.00 12.35 83.49
03-19-14 95.840 9.58 0.00 0.00 0.00 9.58 86.26
06-26-14 95.840 10.41 0.00 0.00 0.00 10.41 85.43
08-22-14 95.840 12.02 0.00 0.00 0.00 12.02 83.82
11-7-14 95.840 14.04 0.00 0.00 0.00 14.04 81.80
03-4-15 95.840 13.21 0.00 0.00 0.00 13.21 82.63
06-25-15 95.840 13.41 0.00 0.00 0.00 13.41 82.43
09-22-15 95.840 15.52 0.00 0.00 0.00 15.52 80.32
12-9-15 95.840 12.59 0.00 0.00 0.00 12.59 83.25
03-2-16 95.840 9.41 0.00 0.00 0.00 9.41 86.43
MW-12 09-9-09 94.270 14.70 0.00 0.00 0.00 14.70 79.57
12-3-09 94.270 13.45 0.00 0.00 0.00 13.45 80.82
03-24-10 94.270 9.50 0.00 0.00 0.00 9.50 84.77
06-24-10 94.270 10.36 0.00 0.00 0.00 10.36 83.91
09-8-10 94.270 12.26 0.00 0.00 0.00 12.26 82.01
12-10-10 94.270 13.43 0.00 0.00 0.00 13.43 80.84
03-8-11 94.270 13.35 0.00 0.00 0.00 13.35 80.92
06-30-11 94.270 13.42 0.00 0.00 0.00 13.42 80.85
09-8-11 94.270 15.05 0.00 0.00 0.00 15.05 79.22
12-8-11 94.270 14.66 0.00 0.00 0.00 14.66 79.61
03-13-12 94.270 13.49 0.00 0.00 0.00 13.43 80.84
06-5-12 94.270 13.58 0.00 0.00 0.00 13.58 80.69
09-11-12 94.270 14.79 0.00 0.00 0.00 14.79 79.48
12-12-12 94.270 15.04 0.00 0.00 0.00 15.04 79.23
03-12-13 94.270 13.24 0.00 0.00 0.00 13.24 81.03
05-29-13 94.270 11.79 0.00 0.00 0.00 11.79 82.48
09-10-13 94.270 10.08 0.00 0.00 0.00 10.08 84.19
11-6-13 94.270 11.73 0.00 0.00 0.00 11.73 82.54
03-19-14 94.270 8.92 0.00 0.00 0.00 8.92 85.35
06-26-14 94.270 9.86 0.00 0.00 0.00 9.86 84.41
08-22-14 94.270 11.43 0.00 0.00 0.00 11.43 82.84
11-7-14 94.270 13.45 0.00 0.00 0.00 13.45 80.82
03-4-15 94.270 12.59 0.00 0.00 0.00 12.59 81.68
06-25-15 94.270 12.82 0.00 0.00 0.00 12.82 81.45
09-22-15 94.270 14.95 0.00 0.00 0.00 14.95 79.32
12-9-15 94.270 12.04 0.00 0.00 0.00 12.04 82.23
03-2-16 94.270 8.84 0.00 0.00 0.00 8.84 85.43
MW-13 03-18-09 94.805 13.58 0.00 0.00 0.00 13.58 81.23
06-23-09 94.805 11.01 0.00 0.00 0.00 11.01 83.80
09-9-09 94.805 12.61 0.00 0.00 0.00 12.61 82.20
12-3-09 94.805 11.26 0.00 0.00 0.00 11.26 83.55
Page 5 of 6
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
06-24-10 94.805 10.56 0.00 0.00 0.00 10.56 84.25
09-8-10 94.805 9.82 0.00 0.00 0.00 9.82 84.99
12-10-10 94.805 10.93 0.00 0.00 0.00 10.93 83.88
03-8-11 94.805 11.24 0.00 0.00 0.00 11.24 83.57
06-30-11 94.805 10.73 0.00 0.00 0.00 10.73 84.08
09-8-11 94.805 12.51 0.00 0.00 0.00 12.51 82.30
12-8-11 94.805 12.69 0.00 0.00 0.00 12.69 82.12
03-13-12 94.805 13.49 0.00 0.00 0.00 10.48 84.33
06-5-12 94.805 10.28 0.00 0.00 0.00 10.28 84.53
09-11-12 94.805 11.55 0.00 0.00 0.00 11.55 83.26
12-12-12 94.805 13.55 0.00 0.00 0.00 13.55 81.26
03-12-13 94.805 10.33 0.00 0.00 0.00 10.33 84.48
05-29-13 94.805 9.41 0.00 0.00 0.00 9.41 85.40
09-10-13 94.805 7.78 0.00 0.00 0.00 7.78 87.03
11-6-13 94.805 9.36 0.00 0.00 0.00 9.36 85.45
03-19-14 94.805 6.88 0.00 0.00 0.00 6.88 87.93
06-26-14 94.805 7.53 0.00 0.00 0.00 7.53 87.28
08-22-14 94.805 8.60 0.00 0.00 0.00 8.60 86.21
11-7-14 94.805 10.69 0.00 0.00 0.00 10.69 84.12
03-4-15 94.805 9.46 0.00 0.00 0.00 9.46 85.35
06-25-15 94.805 10.11 0.00 0.00 0.00 10.11 84.70
09-22-15 94.805 12.30 0.00 0.00 0.00 12.30 82.51
12-9-15 94.805 8.90 0.00 0.00 0.00 8.90 85.91
03-2-16 94.805 6.54 0.00 0.00 0.00 6.54 88.27
MW-14 03-18-09 94.395 NG 0.00 0.00 0.00 0.00 NG
06-23-09 94.395 NG 0.00 0.00 0.00 0.00 NG
09-9-09 94.395 NG 0.00 0.00 0.00 0.00 NG
12-3-09 94.395 NG 0.00 0.00 0.00 0.00 NG
03-24-10 94.395 NG 0.00 0.00 0.00 0.00 NG
06-24-10 94.395 NG 0.00 0.00 0.00 0.00 NG
09-8-10 94.395 NG 0.00 0.00 0.00 0.00 NG
12-10-10 94.395 NG 0.00 0.00 0.00 0.00 NG
03-8-11 94.395 NG 0.00 0.00 0.00 0.00 NG
06-30-11 94.395 NG 0.00 0.00 0.00 0.00 NG
09-8-11 94.395 NG 0.00 0.00 0.00 0.00 NG
12-8-11 94.395 NG 0.00 0.00 0.00 0.00 NG
03-13-12 94.395 NG 0.00 0.00 0.00 0.00 NG
06-5-12 94.395 NG 0.00 0.00 0.00 0.00 NG
09-11-12 94.395 NG 0.00 0.00 0.00 0.00 NG
12-12-12 94.395 NG 0.00 0.00 0.00 0.00 NG
03-12-13 94.395 NG 0.00 0.00 0.00 0.00 NG
05-29-13 94.395 NG 0.00 0.00 0.00 0.00 NG
09-10-13 94.395 NG 0.00 0.00 0.00 0.00 NG
11-6-13 94.395 NG 0.00 0.00 0.00 0.00 NG
03-19-14 94.395 NG 0.00 0.00 0.00 0.00 NG
06-26-14 94.395 NG 0.00 0.00 0.00 0.00 NG
08-22-14 94.395 NG 0.00 0.00 0.00 0.00 NG
11-7-14 94.395 NG 0.00 0.00 0.00 0.00 NG
03-4-15 94.395 NG 0.00 0.00 0.00 0.00 NG
06-25-15 94.395 NG 0.00 0.00 0.00 0.00 NG
09-22-15 94.395 NG 0.00 0.00 0.00 0.00 NG
12-9-15 94.395 NG 0.00 0.00 0.00 0.00 NG
03-2-16 94.395 NG 0.00 0.00 0.00 0.00 NG
MW-15/03-18-09 93.775 13.77 0.00 0.00 0.00 13.77 80.01
MW-15A 06-23-09 93.775 9.90 0.00 0.00 0.00 9.90 83.88
09-9-09 93.775 11.57 0.00 0.00 0.00 11.57 82.21
12-3-09 93.775 11.24 0.00 0.00 0.00 11.24 82.54
03-24-10 93.775 7.57 0.00 0.00 0.00 7.57 86.21
06-24-10 93.775 8.43 0.00 0.00 0.00 8.43 85.35
09-8-10 93.775 9.67 0.00 0.00 0.00 9.67 84.11
12-10-10 93.775 11.24 0.00 0.00 0.00 11.24 82.54
03-8-11 93.775 11.42 0.00 0.00 0.00 11.42 82.36
06-30-11 94.950 12.47 0.00 0.00 0.00 12.47 82.48
09-8-11 94.950 13.88 0.00 0.00 0.00 13.88 81.07
12-8-11 94.950 13.75 0.00 0.00 0.00 13.75 81.20
03-13-12 94.950 13.49 0.00 0.00 0.00 12.60 82.35
06-5-12 94.950 12.45 0.00 0.00 0.00 12.45 82.50
09-11-12 94.950 13.51 0.00 0.00 0.00 13.51 81.44
12-12-12 94.950 14.08 0.00 0.00 0.00 14.08 80.87
03-12-13 94.950 12.07 0.00 0.00 0.00 12.07 82.88
05-29-13 94.950 8.72 0.00 0.00 0.00 8.72 86.23
09-10-13 94.950 9.17 0.00 0.00 0.00 9.17 85.78
Page 6 of 6
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
03-19-14 94.950 8.33 0.00 0.00 0.00 8.33 86.62
MW-15A 06-26-14 94.950 7.78 0.00 0.00 0.00 7.78 87.17
08-22-14 94.950 9.14 0.00 0.00 0.00 9.14 85.81
11-7-14 94.950 11.24 0.00 0.00 0.00 11.24 83.71
03-4-15 94.950 11.40 0.00 0.00 0.00 11.40 83.55
06-25-15 94.950 10.88 0.00 0.00 0.00 10.88 84.07
09-22-15 94.950 13.81 0.00 0.00 0.00 13.81 81.14
12-9-15 94.950 9.28 0.00 0.00 0.00 9.28 85.67
03-2-16 94.950 8.18 0.00 0.00 0.00 8.18 86.77
*MW-5 depth inaccurate for this event as groundwater was seeping in at time of measurement.
1 of 4
PARAMETER UNITS DATE MW-1/MW-3 MW-4 MW-5 MW-6*MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/TS-1 NCAC 2L
MW-1A MW-15A Groundwater
Standard
Benzene ug/l 03-14-07 440 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 DNE DNE DNE NS 1
06-06-07 410 <1 <1 <1 3.6 <1 <1 <1 <1 <1 2.4 DNE DNE DNE NS
08-29-07 340 <1 <1 <1 2.6 <1 <1 <1 <1 <1 6.4 DNE DNE DNE NS12-13-07 200 <1 <1 <1 1.1 <1 <1 <1 <1 <1 9.2 DNE DNE DNE NS03-14-08 250 <1 <1 <1 24 <1 <1 <1 <1 <1 130 DNE DNE DNE NS
06-18-08 310 <1 <1 <1 NS <1 <1 <1 <1 <1 5.3 DNE DNE DNE NS
09-10-08 <100 <1 <1 <1 11.6 <1 <1 <1 <1 <1 69.5 DNE DNE DNE NS
12-03-08 18 <0.5 <0.5 <0.5 8.7 32 <0.5 <0.5 <0.5 <0.5 41 DNE DNE DNE NS03-18-09 110 <0.5 1.9 <0.5 <0.5 5.9 <0.5 <0.5 <0.5 <0.5 3.6 <0.5 NS 520 NS06-23-09 290 <0.5 <0.5 <0.5 <0.5 0.66 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 210 NS
09-09-09 190 <0.5 <0.5 <0.5 <0.5 0.66 NS <0.5 <0.5 NS 5.1 <0.5 NS 910 NS
12-03-09 180 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 7.5 <0.5 NS 440 NS
03-24-10 120 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 55 NS06-24-10 30 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 98 NS09-08-10 69.7 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1.1 <0.5 NS 37.5 NS
12-10-10 140 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1.3 <0.5 NS 5.4 NS
03-08-11 120 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 52 NS
06-30-11 18.3 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 77.1 NS09-08-11 22 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 1.7 <0.5 NS 462 NS12-09-11 15.4 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 0.61 <0.5 NS 384 NS
03-14-12 20 ND ND ND ND ND NS ND ND ND 0.17J ND NS 290 NS
06-07-12 28 ND ND ND ND ND ND NS ND ND ND ND NS 220 NS
9/11-12/12 30.1 ND ND ND ND ND ND NS ND ND 1.2 ND NS 132 NS12-12-12 19 ND ND ND ND ND ND NS ND ND 0.81 ND NS 91 NS03-14-13 20.4 ND ND ND ND NS NS NS ND ND ND ND NS 82.8 NS
05-30-13 0.83 ND ND ND ND NS NS ND ND ND ND ND NS ND NS
09-10-13 5.5 ND ND ND ND ND NS ND ND ND ND ND NS 4.4 NS
11-07-13 0.5 ND ND ND ND ND NS ND ND ND ND ND NS ND NS03-20-14 0.49 ND ND ND ND ND NS ND ND ND ND ND NS 0.29 NS06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 0.15 ND ND ND 0.15 ND NS ND ND ND ND ND NS ND NS
03-04-15 ND ND ND ND ND ND NS ND ND ND ND ND NS 1.1 NS06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS9/22-23/15 1.2 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
12-09-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-02-16 22 ND ND ND ND ND NS ND ND ND ND ND NS 0.82 NS
Toluene ug/l 03-14-07 3200 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 600
06-06-07 5200 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS08-29-07 6300 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS12-13-07 3300 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-14-08 4400 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
06-18-08 5800 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
09-10-08 1850 <1 <1 <1 <1 <1 2.72 <1 <1 <1 <10 DNE DNE DNE NS12-03-08 28 <1 <1 <1 <1 140 5.3 <1 <1 <1 <1 DNE DNE DNE NS03-18-09 3200 <1 <1 <1 <1 50 2.9 <1 <1 <1 <1 <0.5 NS 12000 NS
06-23-09 5700 <1 <1 <1 <1 0.69J 2.9 <1 <1 <1 <1 <1 NS 17000 NS
09-09-09 4300 <1 <1 <1 <1 <1 NS <1 <1 NS <1 <1 NS 25000 NS
12-03-09 3900 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS 30000 NS03-24-10 3100 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 1600 NS06-24-10 640 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 6900 NS
09-08-10 1090 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 1630 NS
12-10-10 3100 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 94 NS
03-08-11 1390 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 1940 NS06-30-11 29.6 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 600 NS09-08-11 2.1 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 5620 NS
12-09-11 5.9 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 <0.5 <0.5 NS 6820 NS
03-14-12 5.7 ND ND ND ND ND NS ND ND ND ND ND NS 7400 NS
06-07-12 8.2 ND ND ND ND ND ND NS ND ND ND ND NS 6300 NS9/11-12/12 8.1 ND ND ND ND ND ND NS ND ND ND ND NS 3240 NS12-12-12 3.3 ND ND ND ND ND ND NS ND ND ND ND NS 3300 NS
03-14-13 5.4 ND ND ND ND NS NS NS ND ND ND ND NS 1860 NS
05-30-13 ND ND ND ND ND NS NS ND ND ND ND ND NS 1.8 NS
09-10-13 7.2 ND ND ND ND ND NS ND ND ND ND ND NS 66.2 NS11-07-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS03-20-14 0.31 ND ND ND ND ND NS ND ND ND ND ND NS 3 NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 0.12 0.11 ND ND ND ND NS ND ND ND ND ND NS 0.22 NS03-04-15 ND ND ND ND ND ND NS ND ND ND ND ND NS 58 NS06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
9/22-23/15 ND ND ND ND ND ND NS ND ND ND ND ND NS 19 NS
12-09-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-02-16 1.1 ND ND ND ND ND NS ND ND ND ND ND NS 20 NS
Ethylbenzene ug/l 03-14-07 66 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 60006-06-07 550 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS08-29-07 760 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
12-13-07 620 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-14-08 580 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
06-18-08 730 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS09-10-08 228 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 DNE DNE DNE NS12-03-08 21 <1 <1 <1 <1 11 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-18-09 280 <1 <1 <1 <1 16 <1 <1 <1 <1 <1 6.3 NS 930 NS
06-23-09 870 <1 <1 <1 <1 2.5 <1 <1 <1 <1 <1 <1 NS 3000 NS
09-09-09 830 <1 <1 <1 <1 2.1 NS <1 <1 NS <1 <1 NS 2300 NS12-03-09 990 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS 2700 NS03-24-10 720 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 160 NS
06-24-10 250 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 1300 NS
09-08-10 625 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 215 NS
12-10-10 700 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 5.1 NS03-08-11 307 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 198 NS06-30-11 19.7 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 140 NS
09-08-11 41.9 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 1550 NS
12-09-11 11.8 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 <0.5 <0.5 NS 1740 NS
03-14-12 11 ND ND ND ND ND NS ND ND ND ND ND NS 2200 NS06-07-12 15 ND ND ND ND ND ND NS ND ND ND ND NS 1900 NS9/11-12/12 22.5 ND ND ND ND ND ND NS ND ND ND ND NS 1620 NS
12-12-12 21 ND ND ND ND ND ND NS ND ND ND ND NS 1600 NS
03-14-13 13.8 ND ND ND ND NS NS NS ND ND ND ND NS 1440 NS
05-30-13 0.58 ND ND ND ND NS NS ND ND ND ND ND NS 1.7 NS09-10-13 7.3 ND ND ND ND ND NS ND ND ND ND ND NS 76.8 NS11-07-13 1.6 ND ND ND ND ND NS ND ND ND ND ND NS 0.88 NS
03-20-14 1.1 ND ND ND ND ND NS ND ND ND ND ND NS 8 NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 0.16 ND ND ND ND ND NS ND ND ND ND ND NS ND NS11-07-14 ND ND ND ND ND ND NS ND ND ND ND ND NS 0.32 NS03-04-15 ND ND ND ND ND ND NS ND ND ND ND ND NS 120 NS
06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
9/22-23/15 0.53 ND ND ND ND ND NS ND ND ND ND ND NS 16 NS
12-09-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS03-02-16 3.9 ND ND ND ND ND NS ND ND ND ND ND NS 15 NS
TABLE 3
Monitoring Well Analytical Results
Incident #12913Harold Smith Grocery
Union Ridge Road, Burlington, North Carolina
2 of 4
PARAMETER UNITS DATE MW-1/MW-3 MW-4 MW-5 MW-6*MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/TS-1 NCAC 2L
MW-1A MW-15A Groundwater
Standard
TABLE 3
Monitoring Well Analytical Results
Incident #12913Harold Smith Grocery
Union Ridge Road, Burlington, North Carolina
Total Xylenes ug/l 03-14-07 5700 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 DNE DNE DNE NS 500
06-06-07 7000 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 DNE DNE DNE NS
08-29-07 9600 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 DNE DNE DNE NS12-13-07 5600 <3 <3 <3 <3 <3 <3 <3 <3 <3 27 DNE DNE DNE NS03-14-08 6200 <3 <3 <3 <3 <3 <3 <3 <3 <3 16 DNE DNE DNE NS
06-18-08 7800 <3 <3 <3 NS <3 <3 <3 <3 <3 12 DNE DNE DNE NS
09-10-08 2377 <4 <4 <4 <4 <4 <4 <4 <4 <4 <40 DNE DNE DNE NS
12-03-08 610 <3 <3 <3 <3 1810 <3 <3 <3 <3 15 DNE DNE DNE NS03-18-09 5500 <3 <3 <3 <3 2020 <3 13.6 <3 <3 4.7 2.3 NS 7000 NS06-23-09 9300 <3 <3 <3 <3 71 <3 <3 <3 <3 <3 <3 NS 22400 NS
09-09-09 8700 <3 <3 <3 <3 30.1 NS <3 <3 NS 3.4 <3 NS 19300 NS
12-03-09 9300 <3 <3 <3 <3 <3 <3 <3 <3 NS 5.8 <3 NS 21200 NS
03-24-10 7800 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 NS 2600 NS06-24-10 2700 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 NS 11100 NS09-08-10 5720 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 NS 3790 NS
12-10-10 9700 NS NS <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 0.61 <1.5 NS 162 NS
03-08-11 5700 <1.5 <1.5 <1.5 <1.5 0.66 <1.5 <1.5 <1.5 <1.5 0.82 <1.5 NS 2124 NS
06-30-11 213.2 <1.5 <1.5 <1.5 <1.5 0.66 NS NS <1.5 <1.5 5.8 <1.5 NS 602 NS09-08-11 42.4 <1.5 <1.5 <1.5 <1.5 0.66 NS NS <1.5 <1.5 11.6 <1.5 NS 3990 NS12-09-11 48 <1.5 <1.5 <1.5 <1.5 <1.5 NS <1.5 <1.5 <1.5 0.66 <1.5 NS 5680 NS
03-14-12 44 ND ND ND ND ND NS ND ND ND ND ND NS 8300 NS
06-07-12 60 ND ND ND ND ND ND NS ND ND ND ND NS 7400 NS
9/11-12/12 73.9 ND ND ND ND ND ND NS ND ND ND ND NS 5940 NS12-12-12 28 ND ND ND ND ND ND NS ND ND ND ND NS 7400 NS03-14-13 44 ND ND ND ND NS NS NS ND ND ND ND NS 5600 NS
05-30-13 1.94 ND ND ND ND NS NS ND ND ND ND ND NS 7.7 NS
09-10-13 83.1 ND ND ND ND ND NS ND ND ND ND ND NS 470 NS
11-07-13 4.5 ND ND ND ND ND NS ND ND ND ND ND NS 3.76 NS03-20-14 5.6 ND ND ND ND ND NS ND ND ND ND ND NS 32.2 NS06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 1.13 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 0.27 0.23 ND 0.19 0.22 0.19 NS ND ND ND ND ND NS 1.37 NS
03-04-15 3.2 ND ND ND ND ND NS ND ND ND ND ND NS 570 NS06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS9/22-23/15 22.3 ND ND ND ND ND NS ND ND ND ND ND NS 250 NS
12-09-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-02-16 107 ND ND ND ND ND NS ND ND ND ND ND NS 173 NS
TOTAL BTEX ug/l 03-14-07 9406 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL DNE DNE DNE NS N/A
06-06-07 13160 BDL BDL BDL 3.6 BDL BDL BDL BDL BDL 2.4 DNE DNE DNE NS08-29-07 17000 BDL BDL BDL 2.6 BDL BDL BDL BDL BDL 6.4 DNE DNE DNE NS12-13-07 9720 BDL BDL BDL BDL BDL BDL BDL BDL BDL 36.2 DNE DNE DNE NS
03-14-08 11430 BDL BDL BDL 24 BDL BDL BDL BDL BDL 146 DNE DNE DNE NS
06-18-08 14640 BDL BDL BDL NS BDL BDL BDL BDL BDL 17.3 DNE DNE DNE NS
09-10-08 4455 BDL BDL BDL 11.6 BDL 2.72 BDL BDL BDL 69.5 DNE DNE DNE NS12-03-08 677 BDL BDL BDL 8.7 1993 5.3 BDL BDL BDL 56 DNE DNE DNE NS03-18-09 9090 BDL 1.9 BDL BDL 2091.9 2.9 13.6 BDL BDL 8.3 8.6 NS 20450 NS
06-23-09 16160 BDL BDL BDL BDL 74.16 2.9 BDL BDL BDL BDL BDL NS 42610 NS
09-09-09 14020 BDL BDL BDL BDL 32.86 NS BDL BDL NS 8.5 BDL NS 47510 NS
12-03-09 14370 BRL BRL BRL BRL BRL BRL BRL BRL NS 13.3 BRL NS 54340 NS03-24-10 11740 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS 4415 NS06-24-10 3620 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS 19398 NS
09-08-10 7504.7 BRL BRL BRL BRL BRL BRL BRL BRL BRL 1.1 BRL NS 5672.5 NS
12-10-10 13640 NS NS BRL BRL BRL BRL BRL BRL BRL 1.91 BRL NS 266.5 NS
03-08-11 7517 ND ND ND ND 0.66 ND ND ND ND 0.82 ND NS 4314 NS06-30-11 280.8 ND ND ND ND 0.66 NS NS ND ND 5.8 ND NS 1419.1 NS09-08-11 108.4 ND ND ND ND 0.66 NS NS ND ND 13.3 ND NS 11622 NS
12-09-11 81.1 ND ND ND ND ND NS ND ND ND 1.27 ND NS 14624 NS
03-14-12 80.7 ND ND ND ND ND NS ND ND ND ND ND NS 18190 NS
06-07-12 111.2 ND ND ND ND ND ND NS ND ND ND ND NS 15820 NS9/11-12/12 134.6 ND ND ND ND ND ND NS ND ND 1.2 ND NS 10932 NS12-12-12 71.3 ND ND ND ND 0.2 ND NS ND ND 0.81 ND NS 12391 NS
03-14-13 83.6 ND ND ND ND NS NS NS ND ND ND ND NS 8982.8 NS
05-30-13 3.35 ND ND ND ND NS NS ND ND ND ND ND NS 11.2 NS
09-10-13 103.1 ND ND ND ND ND NS ND ND ND ND ND NS 617.4 NS11-07-13 6.6 ND ND ND ND ND NS ND ND ND ND ND NS 4.64 NS03-20-14 7.19 ND ND ND ND ND NS ND ND ND ND ND NS 40.49 NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 1.29 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 0.54 0.34 ND 0.19 0.37 0.19 NS ND ND ND ND ND NS 1.91 NS03-04-15 3.2 ND ND ND ND ND NS ND ND ND ND ND NS 749.1 NS06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
9/22-23/15 24.03 ND ND ND ND ND NS ND ND ND ND ND NS 285 NS
12-09-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-02-16 134 ND ND ND ND ND NS ND ND ND ND ND NS 208.82 NS
Methyl Tertiary ug/l 03-14-07 <50 <5 10 <5 4.3J <5 <5 <5 <5 <5 2.7J DNE DNE DNE NS 20Butyl Ether 06-06-07 <50 19 7.5 <5 5.9 <5 4.9J <5 <5 <5 4.1J DNE DNE DNE NS
(MTBE)08-29-07 <50 73 4.6J <5 7.1 <5 <5 <5 <5 <5 4.1J DNE DNE DNE NS
12-13-07 <50 97 20 <5 8.5 <5 <5 <5 <5 <5 13 DNE DNE DNE NS
03-14-08 <50 10 6.9 <5 16 <5 <5 <5 <5 <5 74 DNE DNE DNE NS
06-18-08 <50 26 27 <5 NS <5 <5 <5 <5 <5 15 DNE DNE DNE NS09-10-08 <200 2.3 <2 <2 6.39 <2 <2 <2 <2 <2 38.1 DNE DNE DNE NS
12-03-08 <5 2.8J 8.9 <5 9.3 5.1 <5 <5 <5 <5 75 DNE DNE DNE NS
03-18-09 <50 <5 <5 <5 <5 8.2 <5 8.3 <5 <5 25 <0.5 NS <50 NS
06-23-09 <50 <5 5.4 <5 <5 3.3J <5 <5 <5 <5 11 <5 NS <50 NS
09-09-09 <50 <5 7.7 <5 <5 2.6J NS <5 <5 NS 44 <5 NS <200 NS12-03-09 <50 <5 4J <5 <5 <5 <5 <5 <5 NS 92 <5 NS <200 NS
03-24-10 <50 <5 13 <5 <5 <5 <5 <5 <5 <5 3.3J <5 NS <200 NS
06-24-10 <50 <1 4.2 <1 <1 1.5 <1 <1 <1 <1 13 <1 NS <40 NS
09-08-10 <2.5 <0.5 1.7 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 45.8 <0.5 NS <5 NS
12-10-10 <10 NS NS <1 <1 <1 <1 <1 <1 <1 57 <1 NS <1 NS03-08-11 <10 <0.5 1.6 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 19.1 <0.5 NS <10 NS
06-30-11 2.7 <0.5 0.83 <0.5 <0.5 <0.5 NS NS 0.51 <0.5 23.8 <0.5 NS <0.5 NS
09-08-11 12.3 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS 0.54 <0.5 54.7 <0.5 NS 2.9 NS
12-09-11 9.2 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 0.52 <0.5 28.5 <0.5 NS <25 NS
03-14-12 9.6 ND 0.5 ND 0.25J ND NS ND 0.84 ND 10 ND NS ND NS06-07-12 ND ND ND ND ND ND ND NS 1.7 ND 15 ND NS ND NS
9/11-12/12 21.4 ND ND ND ND ND ND NS 2.2 ND 33.8 ND NS ND NS
12-12-12 21 ND ND ND 0.19J ND ND NS 0.32J ND 24 ND NS ND NS
03-14-13 21.3 ND ND ND ND NS NS NS ND ND 8.4 ND NS ND NS
05-30-13 9.4 ND ND ND ND NS NS ND 0.8 ND 2 ND NS 0.61 NS09-10-13 14.4 ND ND ND ND ND NS ND 2.9 ND 1.9 ND NS ND NS
11-07-13 9.4 ND ND ND ND ND NS ND 2.2 ND 1.2 ND NS ND NS
03-20-14 8.6 ND 0.35 ND 0.16 ND NS 1.1 0.12 ND 1.8 ND NS 0.2 NS
06-26-14 0.25 ND 0.32 ND 0.53 0.24 NS 0.3 3.2 ND 0.66 ND NS ND NS
08-22-14 4.1 ND ND ND ND ND NS 0.25 1.3 ND 0.57 ND NS ND NS11-07-14 0.79 ND ND ND ND ND NS 1.4 1.5 ND 0.46 ND NS ND NS
03-04-15 4.6 ND ND ND 0.60J ND NS 1.6 ND ND 0.80J ND NS ND NS
06-25-15 3.9 ND ND ND 0.75J ND NS ND 0.67J ND 0.68J ND NS ND NS
9/22-23/15 6.2 ND ND ND 1 ND NS ND ND ND ND ND NS ND NS
12-09-15 1.7 ND ND ND 1.9 ND NS ND ND ND ND ND NS ND NS03-02-16 8.5 ND ND ND 1.4 ND NS ND ND ND 1.4 ND NS ND NS
3 of 4
PARAMETER UNITS DATE MW-1/MW-3 MW-4 MW-5 MW-6*MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/TS-1 NCAC 2L
MW-1A MW-15A Groundwater
Standard
TABLE 3
Monitoring Well Analytical Results
Incident #12913Harold Smith Grocery
Union Ridge Road, Burlington, North Carolina
Ethylene ug/l 03-14-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 0.02Dibromide06-06-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS(EDB)08-29-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS12-13-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS03-14-08 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
06-18-08 <10 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
09-10-08 <2 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 DNE DNE DNE NS
12-03-08 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS03-18-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <0.5 NS <50 NS06-23-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS <50 NS
09-09-09 <10 <1 <1 <1 <1 <1 NS <1 <1 NS <1 <1 NS <40 NS
12-03-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS <40 NS
03-24-10 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS <40 NS06-24-10 14 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 28 NS09-08-10 <2.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS <5 NS
12-10-10 <5 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 3.9 NS
03-08-11 <10 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS <10 NS
06-30-11 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 1.9 NS09-08-11 <1.2 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 7 NS12-09-11 <1 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 <0.5 <0.5 NS <25 NS
03-14-12 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
06-07-12 ND ND ND ND ND ND ND NS ND ND ND ND NS ND NS
9/11-12/12 ND ND ND ND ND ND ND NS ND ND ND ND NS ND NS12-12-12 ND ND ND ND ND ND ND NS ND ND ND ND NS ND NS03-14-13 ND ND ND ND ND NS NS NS ND ND ND ND NS ND NS
05-30-13 ND ND ND ND ND NS NS ND ND ND ND ND NS ND NS
09-10-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS03-20-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-04-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS9/22-23/15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
12-09-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-02-16 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
Isopropyl Ether ug/l 03-14-08 86 <5 3J <5 9.9 <5 <5 <5 <5 <5 270 DNE DNE DNE NS 70(IPE)06-18-08 <50 <5 13 <5 NS <5 <5 <5 <5 <5 19 DNE DNE DNE NS09-10-08 <100 <1 <1 <1 9.28 <1 <1 <1 <1 <1 221 DNE DNE DNE NS12-03-08 15 <5 4.6J <5 6.9 23 <5 8.1 <5 <5 200 DNE DNE DNE NS
03-18-09 <50 <5 <5 <5 <5 19 <5 10 <5 <5 69 <0.5 NS <50 NS
06-23-09 <50 <5 <5 <5 <5 6.2 <5 <5 <5 <5 10 <5 NS <50 NS
09-09-09 <50 <5 3.3J <5 <5 4.9J NS <5 <5 NS 73 <5 NS <200 NS12-03-09 <50 <5 <5 <5 <5 <5 <5 <5 <5 NS 180 <5 NS <200 NS03-24-10 <50 <5 5.9 <5 <5 <5 <5 <5 <5 <5 3.2J <5 NS <200 NS
06-24-10 <5 <0.5 1.8 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 12 <0.5 NS <20 NS
09-08-10 2.9 <0.5 0.66 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 35.9 <0.5 NS <5 NS
12-10-10 6 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 49 <0.5 NS 1.3 NS03-08-11 <10 <0.5 <0.5 <0.5 <0.5 0.56 <0.5 <0.5 0.82 <0.5 24.6 <0.5 NS <10 NS06-30-11 13 <0.5 <0.5 <0.5 <0.5 0.56 NS NS 1.2 <0.5 29.2 <0.5 NS 2.7 NS
09-08-11 62.2 <0.5 <0.5 <0.5 <0.5 0.56 NS NS 0.73 <0.5 55.2 <0.5 NS 22.5 NS
12-09-11 40.9 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 29.1 <0.5 NS <25 NS
03-14-12 47 ND ND ND ND ND NS ND 0.17J ND 11 ND NS ND NS06-07-12 78 ND ND ND ND ND ND NS 0.52J ND 12 ND NS 15J NS9/11-12/12 94.8 ND ND ND ND ND ND NS 1.6 ND 29.8 ND NS 13.5 NS
12-12-12 120 ND ND ND 0.16J ND ND NS 1.6 ND 26 ND NS ND NS
03-14-13 112 ND ND ND ND NS NS NS ND ND 10.2 ND NS ND NS
05-30-13 32.5 ND ND ND ND NS NS 3.1 1.5 ND ND ND NS 1.5 NS09-10-13 80.7 ND ND ND ND ND NS 3.1 6.9 ND ND ND NS 7.2 NS11-07-13 42.2 ND ND ND ND ND NS ND 3.1 1.9 ND ND NS 0.79 NS
03-20-14 46 ND ND ND 0.2 ND NS ND 3.1 1.9 0.34 ND NS 1.5 NS
06-26-14 ND ND ND ND 1.4 ND NS ND 3.3 3.1 ND ND NS ND NS
08-22-14 11 ND ND ND 0.24 ND NS ND 2.1 3.1 ND ND NS ND NS11-07-14 2 ND ND ND ND ND NS ND 1.1 ND ND ND NS ND NS03-04-15 27 ND ND ND ND ND NS ND ND ND 0.5 ND NS ND NS
06-25-15 11 ND ND ND ND ND NS ND 0.59 ND ND ND NS ND NS
9/22-23/15 32 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
12-09-15 6 ND ND ND ND ND NS ND ND 1.9 ND ND NS ND NS03-02-16 75 ND ND ND ND ND NS ND ND ND 1.1 ND NS ND NS
1,2-Dichloroethane ug/l 03-14-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 0.4
06-06-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
08-29-07 <10 <1 <1 <1 <1 <1 <1 <1 1.4 <1 1.3 DNE DNE DNE NS
12-13-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 1.5 DNE DNE DNE NS
03-14-08 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 31 DNE DNE DNE NS06-18-08 <10 <1 1.3 <1 NS <1 <1 <1 <1 <1 2.8 DNE DNE DNE NS
09-10-08 <2 <1 <1 <1 <1 <1 <1 <1 <1 <1 29.3 DNE DNE DNE NS
12-03-08 <1 <1 <1 <1 <1 4 <1 0.76J <1 <1 30 DNE DNE DNE NS
03-18-09 <10 <1 <1 <1 <1 2.1 <1 1.5 <1 <1 4.5 <0.5 NS <50 NS
06-23-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 0.69J <1 NS <50 NS09-09-09 <10 <1 <1 <1 <1 0.64J NS <1 <1 NS 8.6 <1 NS <40 NS
12-03-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 NS 13 <1 NS <40 NS
03-24-10 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS <40 NS
06-24-10 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 2.8 <0.5 <0.5 NS <20 NS
09-08-10 <2.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 6.9 <0.5 NS <5 NS12-10-10 <5 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 11 <0.5 NS <0.5 NS
03-08-11 <10 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 7.1 <0.5 NS <10 NS
06-30-11 1.1 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 9.1 <0.5 NS 0.58 NS
09-08-11 4.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 10.9 <0.5 NS 4 NS
12-09-11 4.1 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 7.1 <0.5 NS <25 NS03-14-12 ND ND ND ND ND ND NS ND 0.33J ND 3.6 ND NS ND NS
06-07-12 ND ND ND ND ND ND ND NS ND ND 4 ND NS ND NS
9/11-12/12 13.7 ND ND ND ND ND ND NS 0.67 ND 5.9 ND NS ND NS
12-12-12 15 ND ND ND ND ND ND NS ND ND 0.81 ND NS 4.9 NS
03-14-13 14.2 ND ND ND ND NS NS NS 0.72 ND 3.3 ND NS ND NS05-30-13 4.2 ND ND ND ND NS NS ND 1.1 ND 0.53 ND NS ND NS
09-10-13 9.2 ND ND ND ND ND NS ND 2.4 ND 0.51 ND NS 0.6 NS
11-07-13 4.1 ND ND ND ND ND NS ND 2.2 ND ND ND NS ND NS
03-20-14 4.8 ND ND ND 0.23 ND NS ND 3.2 ND ND ND NS ND NS
06-26-14 ND ND ND ND 0.32 ND NS ND 1.4 0.63 ND ND NS ND NS08-22-14 2 ND ND ND ND ND NS ND 1.2 0.84 ND ND NS ND NS
11-07-14 ND ND ND ND ND ND NS ND 0.69 ND ND ND NS ND NS
03-04-15 2.7 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
06-25-15 1.6 ND ND ND ND ND NS ND ND 0.53 ND ND NS ND NS
9/22-23/15 3.7 ND ND ND ND ND NS ND ND ND ND ND NS ND NS12-09-15 1.2 ND ND ND ND ND NS ND ND 0.61 ND ND NS ND NS
03-02-16 7.3 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
4 of 4
PARAMETER UNITS DATE MW-1/MW-3 MW-4 MW-5 MW-6*MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/TS-1 NCAC 2L
MW-1A MW-15A Groundwater
Standard
TABLE 3
Monitoring Well Analytical Results
Incident #12913Harold Smith Grocery
Union Ridge Road, Burlington, North Carolina
Naphthalene ug/l 03-14-08 470 <1 <1 <1 <1 <1 <1 <1 <1 <1 4.5 DNE DNE DNE NS 6
06-18-08 590 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
09-10-08 136 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 DNE DNE DNE NS12-03-08 31 <1 <1 <1 <1 <1 <1 <1 <1 <1 3.5 DNE DNE DNE NS03-18-09 250 <1 1.9 <1 <1 <1 <1 1.6 <1 <1 <1 6.2 NS 490 NS
06-23-09 470 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 950 NS
09-09-09 540 <1 <1 <1 <1 <1 NS <1 <1 NS <1 <1 NS 680 NS
12-03-09 490 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS 750 NS03-24-10 550 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 220 NS06-24-10 680 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 580 NS
09-08-10 736 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 NS 255 NS
12-10-10 520 NS NS <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 7.1 NS
03-08-11 337 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 NS 118 NS06-30-11 54.1 <2 <2 <2 <2 <2 NS NS <2 <2 3 <2 NS 41.6 NS09-08-11 154 <2 <2 <2 <2 <2 NS NS <2 <2 5.9 <2 NS 395 NS
12-09-11 112 <2 <2 <2 <2 <2 NS <2 <2 <2 <2 <2 NS 504 NS
03-14-12 87 ND ND ND ND ND NS ND ND ND ND ND NS 130J NS
06-07-12 84 ND ND ND ND ND ND NS ND ND ND ND NS 150 NS9/11-12/12 197 ND ND ND ND ND ND NS ND ND ND ND NS 515 NS12-12-12 99 ND ND ND ND ND ND NS ND ND ND ND NS 250 NS
03-14-13 84.6 ND ND ND ND NS NS NS ND ND ND ND NS 344 NS
05-30-13 3.4 ND ND ND ND NS NS ND ND ND ND ND NS ND NS
09-10-13 18 ND ND ND ND ND NS ND ND ND ND ND NS 2.3 NS11-07-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS03-20-14 2.5 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 0.66 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS03-04-15 0.73J ND ND ND ND ND NS ND ND ND ND ND NS 33 NS06-25-15 0.99J ND ND ND ND ND NS ND ND ND ND ND NS ND NS
9/22-23/15 3.2 ND ND ND ND ND NS ND ND ND ND ND NS 16 NS
12-09-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-02-16 47 0.79J ND ND ND ND NS ND ND ND ND ND NS 30 NS
NA=Not Analyzed for Parameter DNE=Did Not Exist Bold Values exceed the NCAC 2L Groundwater Standard J=Estimated ValueNS=Not Sampled BDL=Below Detection Limits ND=Not Detected
Page 1 of 2
PARAMETER UNITS DATE NCAC 15A:2L 2768B 2774 2760 2773 2755 2761 2779 2765 2765 2765 2800 Groundwater
Influent Midfluent Effluent Standard
Benzene ug/l 03-24-10 <0.5 NS NS NS NS NS NS 1.7 <0.5 <0.5 NS06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS09-08-10 NS NS NS <0.5 NS NS NS 1 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS 0.97 <0.5 <0.5 NS 103-08-11 NS NS NS <0.5 NS NS <0.5 1.6 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 8.4 <0.5 <0.5 NS09-08-11 NS NS NS <0.5 NS NS <0.5 7.1 <0.5 <0.5 NS12-09-11 NS NS NS <0.5 NS NS <0.5 3.3 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS12-12-12 NS NS NS ND NS NS ND ND NS ND NS03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND ND NS ND NS09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS09-20-14 ND NS NS ND NS NS ND ND ND ND NS06-26-14 ND NS ND ND NS NS ND 0.33 ND ND NS
08-22-14 ND NS ND ND NS NS ND 0.54 ND ND NS11-07-14 ND NS ND ND NS NS ND ND ND ND NS
03-04-15 NS NS ND ND NS NS ND ND ND ND NS06-25-15 ND NS ND ND NS NS ND ND ND ND NS09-23-15 ND NS ND ND NS NS ND ND ND ND NS
12-09-15 ND NS ND ND NS NS ND ND ND ND NS02-29-16 ND ND ND ND NS NS ND ND ND ND NS
Toluene ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 600
03-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS05-29-13 ND NS NS ND NS NS ND ND NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS11-07-13 ND NS NS ND NS NS ND ND NS ND NS03-20-14 ND NS NS ND NS NS ND ND ND ND NS
06-26-14 ND NS ND ND NS NS ND ND ND ND NS08-22-14 ND NS ND ND NS NS ND ND ND ND NS
11-07-14 ND NS ND ND NS NS ND ND ND ND NS03-04-15 NS NS ND ND NS NS ND ND ND ND NS06-25-15 ND NS ND ND NS NS ND ND ND ND NS
09-23-15 ND NS ND ND NS NS ND ND ND ND NS12-09-15 ND NS ND ND NS NS ND ND ND ND NS
02-29-16 ND ND ND ND NS NS ND ND ND ND NS
Ethylbenzene ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS
06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 60003-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND 0.55 NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS
03-20-14 ND ND ND ND NS NS ND ND ND ND NS06-26-14 ND NS ND ND NS NS ND ND ND ND NS08-22-14 ND NS ND ND NS NS ND 0.26 ND ND NS11-07-14 ND NS ND ND NS NS ND ND ND ND NS03-04-15 NS NS ND ND NS NS ND ND ND ND NS
06-25-15 ND NS ND ND NS NS ND ND ND ND NS09-23-15 ND NS ND ND NS NS ND ND ND ND NS12-09-15 ND NS ND ND NS NS ND ND ND ND NS02-29-16 ND ND ND ND NS NS ND ND ND ND NS
Total Xylenes ug/l 03-24-10 <3 NS NS NS NS NS NS <3 <3 <3 NS06-24-10 NS NS NS <1.5 NS NS NS <1.5 <1.5 <1.5 NS09-08-10 NS NS NS <1.5 NS NS NS <1.5 <1.5 <1.5 NS12-10-10 NS NS NS <1.5 NS NS NS <1.5 <1.5 <1.5 NS 50003-08-11 NS NS NS <1.5 NS NS <1.5 <1.5 <1.5 <1.5 NS
06-30-11 NS NS NS <1.5 NS NS <1.5 <3 <1.5 <1.5 NS09-08-11 NS NS NS <1.5 NS NS <1.5 <3 <1.5 <1.5 NS12-09-11 NS NS NS <1.5 NS NS <1.5 <3 <1.5 <1.5 NS03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS12-12-12 NS NS NS ND NS NS ND ND NS ND NS03-14-13 ND NS NS ND NS NS ND ND NS ND NS05-29-13 ND NS NS ND NS NS ND ND NS ND NS09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS03-20-14 ND ND ND ND NS NS ND ND ND ND NS06-26-14 ND NS ND ND NS NS ND ND ND ND NS08-22-14 ND NS ND ND NS NS ND ND ND ND NS11-07-14 ND NS ND ND NS NS ND ND ND ND NS
03-04-15 NS NS ND ND NS NS ND ND ND ND NS06-25-15 ND NS ND ND NS NS ND ND ND ND NS09-23-15 ND NS ND ND NS NS ND ND ND ND NS12-09-15 ND NS ND ND NS NS ND ND ND ND NS02-29-16 ND ND ND ND NS NS ND ND ND ND NS
TOTAL BTEX ug/l 03-24-10 BDL NS NS NS NS NS NS 1.7 BDL BDL NS06-24-10 NS NS NS BDL NS NS NS BDL BDL BDL NS09-08-10 NS NS NS BDL NS NS NS 1 BDL BDL NS12-10-10 NS NS NS BDL NS NS NS 0.97 <0.5 <0.5 NS N/A
03-08-11 NS NS NS BDL NS NS BDL 1.6 BDL BDL NS06-30-11 NS NS NS BDL NS NS BDL 8.4 BDL BDL NS09-08-11 NS NS NS BDL NS NS BDL 7.1 BDL BDL NS12-09-11 NS NS NS BDL NS NS BDL 3.3 BDL BDL NS03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS12-12-12 NS NS NS ND NS NS ND ND NS ND NS03-14-13 ND NS NS ND NS NS ND ND NS ND NS05-29-13 ND NS NS ND NS NS ND 0.55 NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS11-07-13 ND NS NS ND NS NS ND ND NS ND NS03-20-14 ND ND ND ND NS NS ND ND ND ND NS06-26-14 ND NS ND ND NS NS ND 0.33 ND ND NS08-22-14 ND NS ND ND NS NS ND 0.8 ND ND NS
11-07-14 ND NS ND ND NS NS ND ND ND ND NS03-04-15 NS NS ND ND NS NS ND ND ND ND NS06-25-15 ND NS ND ND NS NS ND ND ND ND NS09-23-15 ND NS ND ND NS NS ND ND ND ND NS12-09-15 ND NS ND ND NS NS ND ND ND ND NS
02-29-16 ND ND ND ND NS NS ND ND ND ND NS
Methyl Tertiary ug/l 03-24-10 22 NS NS NS NS NS NS 98 <5 <5 NSButyl Ether 06-24-10 NS NS NS <1 NS NS NS <1 <1 <1 NS(MTBE)09-08-10 NS NS NS <1 NS NS NS 84.8 <1 <1 NS
12-10-10 NS NS NS <1 NS NS NS 100 <1 <1 NS 2003-08-11 NS NS NS <0.5 NS NS <0.5 166 <0.5 <0.5 NS06-30-11 NS NS NS <0.5 NS NS <0.5 125 <0.5 <0.5 NS09-08-11 NS NS NS <0.5 NS NS <0.5 136 <0.5 <0.5 NS12-09-11 NS NS NS <0.5 NS NS <0.5 150 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS9/11-12/2012 NS NS NS ND NS NS ND 149 NS ND NS12-12-12 NS NS NS ND NS NS ND 140 NS ND NS03-14-13 ND NS NS ND NS NS ND 157 NS ND NS
05-29-13 ND NS NS ND NS NS ND 150 NS ND NS09-10-13 ND NS NS ND NS NS ND 128 NS ND NS11-07-13 ND NS NS ND NS NS ND 117 NS ND NS03-20-14 ND ND ND 0.81 NS NS ND 140 ND 0.62 NS06-26-14 ND NS ND 0.23 NS NS ND 120 ND ND NS
08-22-14 ND NS ND 0.18 NS NS ND 120 ND 0.28 NS11-07-14 ND NS ND ND NS NS ND 130 ND ND NS03-04-15 NS NS ND 0.79J NS NS ND 80 ND ND NS06-25-15 ND NS ND 0.57J NS NS ND 57 ND ND NS09-23-15 ND NS ND ND NS NS ND 70 ND ND NS
12-09-15 ND NS ND 3.1 NS NS ND 53 ND ND NS02-29-16 ND ND ND 12 NS NS ND 60 ND ND NS
SUPPLY WELL
Union Ridge Road, Burlington, North Carolina
TABLE 4
Water Supply Well Analytical Results
Harold Smith GroceryIncident #12913
Page 2 of 2
PARAMETER UNITS DATE NCAC 15A:2L 2768B 2774 2760 2773 2755 2761 2779 2765 2765 2765 2800 Groundwater
Influent Midfluent Effluent Standard
SUPPLY WELL
Union Ridge Road, Burlington, North Carolina
TABLE 4
Water Supply Well Analytical Results
Harold Smith GroceryIncident #12913
Ethylene ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NSDibromide06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS(EDB)09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 0.0203-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS12-12-12 NS NS NS ND NS NS ND ND NS ND NS03-14-13 ND NS NS ND NS NS ND ND NS ND NS05-29-13 ND NS NS ND NS NS ND ND NS ND NS09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS03-20-14 ND ND ND ND NS NS ND ND ND ND NS06-26-14 ND NS ND ND NS NS ND ND ND ND NS08-22-14 ND NS ND ND NS NS ND ND ND ND NS11-07-14 ND NS ND ND NS NS ND ND ND ND NS
03-04-15 ND NS ND ND NS NS ND ND ND ND NS06-25-15 ND NS ND ND NS NS ND ND ND ND NS09-23-15 ND NS ND ND NS NS ND ND ND ND NS12-09-15 ND NS ND ND NS NS ND ND ND ND NS02-29-16 ND ND ND ND NS NS ND ND ND ND NS
Isopropyl Ether ug/l 03-24-10 11 NS NS NS NS NS NS 130 <5 <5 NS(IPE)06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS09-08-10 NS NS NS <0.5 NS NS NS 104 <0.5 <0.5 NS12-10-10 NS NS NS <0.5 NS NS NS 150 <0.5 <0.5 NS 70
03-08-11 NS NS NS <0.5 NS NS <0.5 260 <0.5 <0.5 NS06-30-11 NS NS NS <0.5 NS NS <0.5 191 <0.5 <0.5 NS09-08-11 NS NS NS <0.5 NS NS <0.5 206 <0.5 NS12-09-11 NS NS NS <0.5 NS NS <0.5 178 <0.5 <0.5 NS03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS9/11-12/2012 NS NS NS ND NS NS ND 149 NS ND NS12-12-12 NS NS NS ND NS NS ND 150 NS ND NS03-14-13 ND NS NS ND NS NS ND 159 NS ND NS05-29-13 ND NS NS ND NS NS ND 168 NS ND NS
09-10-13 ND NS NS 0.96 NS NS ND 183 NS ND NS11-07-13 ND NS NS 1.96 NS NS ND 138 NS ND NS03-20-14 ND ND ND 0.67 NS NS ND 140 ND 0.2 NS06-26-14 ND NS ND ND NS NS ND 160 ND ND NS08-22-14 ND NS ND ND NS NS ND 150 ND ND NS
11-07-14 ND NS ND ND NS NS ND 160 ND ND NS03-04-15 NS NS ND ND NS NS ND 100 ND ND NS06-25-15 ND NS ND ND NS NS ND 68 ND ND NS09-23-15 ND NS ND ND NS NS ND 74 ND ND NS12-09-15 ND NS ND 2.2 NS NS ND 75 ND ND NS
02-29-16 ND ND ND 18 NS NS ND 76 ND ND NS
1,2- Dichloroethane ug/l 03-24-10 <1 NS NS NS NS NS NS 6.2 <1 <1 NS06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS09-08-10 NS NS NS <0.5 NS NS NS 15.7 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS 19 <0.5 <0.5 NS 0.403-08-11 NS NS NS <0.5 NS NS <0.5 33.1 <0.5 <0.5 NS06-30-11 NS NS NS <0.5 NS NS <0.5 28 <0.5 <0.5 NS09-08-11 NS NS NS <0.5 NS NS <0.5 27.4 <0.5 <0.5 NS12-09-11 NS NS NS <0.5 NS NS <0.5 26.6 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS9/11-12/2012 NS NS NS ND NS NS ND 20.8 NS ND NS12-12-12 NS NS NS 0.19J NS NS ND 23 NS ND NS03-14-13 ND NS NS ND NS NS ND 31.5 NS ND NS
05-29-13 ND NS NS ND NS NS ND 25.9 NS ND NS09-10-13 ND NS NS ND NS NS ND 25.7 NS ND NS11-07-13 ND NS NS ND NS NS ND 20.1 NS ND NS03-20-14 ND ND ND 0.44 NS NS ND 20 ND ND NS06-26-14 ND NS ND 0.31 NS NS ND 24 ND ND NS
08-22-14 ND NS ND ND NS NS ND 24 ND ND NS11-07-14 ND NS ND ND NS NS ND 27 ND ND NS03-04-15 NS NS ND ND NS NS ND 16 ND ND NS06-25-15 ND NS ND ND NS NS ND 12 ND ND NS09-23-15 ND NS ND ND NS NS ND 13 ND ND NS
12-09-15 ND NS ND 0.94 NS NS ND 10 ND ND NS02-29-16 ND ND ND 2 NS NS ND 9.2 ND ND NS
1,2-Dichloropropane ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 0.603-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS05-29-13 ND NS NS ND NS NS ND ND NS ND NS09-10-13 ND NS NS ND NS NS ND ND NS ND NS11-07-13 ND NS NS ND NS NS ND ND NS ND NS03-20-14 ND ND ND ND NS NS ND ND ND ND NS
06-26-14 ND NS ND ND NS NS ND ND ND ND NS08-22-14 ND NS ND ND NS NS ND ND ND ND NS11-07-14 ND NS ND ND NS NS ND ND ND ND NS03-04-15 NS NS ND ND NS NS ND ND ND ND NS06-25-15 ND NS ND ND NS NS ND ND ND ND NS
09-23-15 ND NS ND ND NS NS ND ND ND ND NS12-09-15 ND NS ND ND NS NS ND ND ND ND NS02-29-16 ND ND ND ND NS NS ND ND ND ND NS
Chloroform 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS
06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS03-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 7006-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS03-14-13 ND NS NS ND NS NS ND ND NS ND NS05-29-13 ND NS NS ND NS NS ND ND NS ND NS09-10-13 ND NS NS ND NS NS ND ND NS ND NS11-07-13 ND NS NS ND NS NS ND ND NS ND NS
03-20-14 ND ND ND ND NS NS ND ND ND ND NS06-26-14 ND NS ND ND NS NS ND 1.1 ND ND NS08-22-14 ND NS ND ND NS NS ND ND ND 1.6 NS11-07-14 ND NS ND ND NS NS ND ND ND ND NS03-04-15 NS NS ND ND NS NS ND ND ND ND NS
06-25-15 ND NS ND ND NS NS ND ND ND ND NS09-23-15 ND NS ND ND NS NS ND ND ND ND NS12-09-15 ND NS ND ND NS NS ND ND ND ND NS02-29-16 ND ND ND ND NS NS ND ND ND ND NS
*Samples 2765 influent & effluent were sampled on 9/25/01 NA=Not analyzed for this parameter J=Estimated Value NS=Not Sampled
TABLE 5 System Operation Parameters Harold Smith Grocery Incident #12913 Union Ridge Road, Burlington, North Carolina
DATE: TEMP. (°F) FLOW (SCFM) VACUUM (IN.-H2O) TEMP. (°F) PRESSURE (PSI)
1/6/09 65 120 9 180 15
2/4/09 55 115 9 175 12
3/16/09 55 115 8 170 10 4/2/09 75 115 7 180 10
5/6/09 78 115 8 184 10
6/5/09 70 115 6 175 10
7/6/09 80 115 8 NR 10
8/10/09 78 115 8 NR 10
9/8/09 76 115 8 NR 9
10/5/09 72 115 7 NR 7
11/2/09 70 115 6 NR 5
12/13/09 58 115 7 NR 5
1/6/10 36 115 8 NR 3
2/18/10 42 115 8 NR 12
3/5/10 56 115 7 NR 12
3/31/10 50 115 8 NR 12
5/24/10 70 115 8 NR 14
6/25/10 75 110 7 NR 14
7/27/10 75 110 6 NR 12
8/6/10 90 110 6 NR 12
9/2/10 90 110 6 NR 11
10/1/10 85 115 6 NR 10
11/10/10 50 115 6 NR 12
12/7/10 45 115 6 NR 12
1/6/11 40 110 6 NR 12
2/3/11 45 110 6 NR 12
3/15/11 55 110 6 NR 12
SYSTEM OFF – SOIL EXCAVATION
1/6/12 OFF OFF OFF NR 10
2/10/12 OFF OFF OFF NR 10
3/19/12 OFF OFF OFF NR 10
4/4/12 OFF OFF OFF NR 10
5/3/12 OFF OFF OFF NR 10
6/1/12 OFF OFF OFF NR 9
7/3/12 OFF OFF OFF NR 9
8/3/12 OFF OFF OFF NR 9
9/21/12 OFF OFF OFF NR OFF
10/3/12 OFF OFF OFF NR OFF
11/19/12 OFF OFF OFF NR OFF
12/14/12 OFF OFF OFF NR OFF
1/28/13 OFF OFF OFF NR OFF
2/25/13 OFF OFF OFF NR OFF
3/19/13 OFF OFF OFF NR OFF
TABLE 5 System Operation Parameters Harold Smith Grocery Incident #12913 Union Ridge Road, Burlington, North Carolina
DATE: TEMP. (°F) FLOW (SCFM) VACUUM (IN.-H2O) TEMP. (°F) PRESSURE (PSI)
5/30/13 OFF OFF OFF NR OFF
6/19/13 OFF OFF OFF NR OFF
7/9/13 OFF OFF OFF NR OFF
8/9/13 OFF OFF OFF NR OFF
9/15/3 OFF OFF OFF NR OFF
10/22/13 OFF OFF OFF NR OFF
11/5/13 OFF OFF OFF NR OFF
12/12/13 40 110 5 NR 8
1/10/14 50 110 5 NR 8
2/4/14 40 110 5 NR 8
3/1/14 42 110 5 NR 8
3/25/14 50 110 5 NR 8
5/29/14 80 110 5 NR 8
6/9/14 75 110 5 NR 7
6/30/14 90 110 5 NR 8
8/5/14 80 110 5 NR 8
9/3/14 85 110 5 NR 8
9/26/14 70 110 5 NR 8
11/12/14 50 110 5 NR 8
12/12/14 45 110 5 NR 8
1/21/15 50 110 5 NR 8
1/30/15 50 110 5 NR 8
3/11/15 60 110 5 NR 8
4/13/15 70 110 5 NR 8
5/15/15 70 110 5 NR 8
6/4/15 70 110 5 NR 8
6/29/15 85 110 5 NR 8
7/27/15 85 110 5 NR 8
8/26/15 80 110 5 NR 8
9/30/15 80 110 5 NR 8
11/4/15 70 110 4 NR 8
12/2/15 50 110 4 NR 8
1/27/16 45 110 4 NR 15
2/17/16 50 110 4 NR 15
3/23/16 70 110 4 NR 10

* Individual pressure (in psi) and flow (in scfm) at each sparge well. NR = not recorded.
TABLE 5 System Operation Parameters Harold Smith Grocery Incident #12913 Union Ridge Road, Burlington, North Carolina
DATE: PRES./ AS-2 PRES./
AS-3 PRES./
AS-4 PRES./
AS-5 PRES./
AS-6 PRES./
AS-7 PRES./
AS-8 PRES./
TABLE 5 System Operation Parameters Harold Smith Grocery Incident #12913 Union Ridge Road, Burlington, North Carolina
DATE: PRES./ AS-2 PRES./
AS-3 PRES./
AS-4 PRES./
AS-5 PRES./
AS-6 PRES./
AS-7 PRES./
AS-8 PRES./
Individual pressure (in psi) and flow (in scfm) at each sparge well. NR = not recorded.

APPENDIX A

This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
Case Narrative
03/15/2016
Pyramid Environmental, Inc
Brett Higgins
PO Box 16265
Greensboro, NC 27416-0265
Project: Harold Smith
Lab Submittal Date: 03/04/2016
Prism Work Order: 6030100
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services
Reviewed ByAngela D. Overcash Terri W. Cole For Angela D. Overcash
Project Manager
Data Qualifiers Key Reference:
CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L1 LCS recovery outside of the QC limits. LCSD recovery within the limits. No further action taken.
L2 LCSD recovery outside of the QC limits. LCS recovery within the limits. No further action taken.
LH High LCS recovery. Analyte not detected in the sample(s). No further action taken.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 56
Sample Receipt Summary
03/15/2016
Prism Work Order: 6030100
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
6030100-01 02/29/162765 EFF 03/04/16Water
6030100-02 02/29/162765 Mid 03/04/16Water
6030100-03 02/29/162765 INF 03/04/16Water
6030100-04 02/29/16SW 2773 03/04/16Water
6030100-05 02/29/16SW 2779 03/04/16Water
6030100-06 02/29/16SW 2768B 03/04/16Water
6030100-07 02/29/16SW 2760 03/04/16Water
6030100-08 02/29/16SW 2774 03/04/16Water
6030100-09 03/02/16MW-1A 03/04/16Water
6030100-10 03/02/16MW-3 03/04/16Water
6030100-11 03/02/16MW-4 03/04/16Water
6030100-12 03/02/16MW-5 03/04/16Water
6030100-13 03/02/16MW-6 03/04/16Water
6030100-14 03/02/16MW-7 03/04/16Water
6030100-15 03/02/16MW-9 03/04/16Water
6030100-16 03/02/16MW-10 03/04/16Water
6030100-17 03/02/16MW-11 03/04/16Water
6030100-18 03/02/16MW-12 03/04/16Water
6030100-19 03/02/16MW-13 03/04/16Water
6030100-20 03/02/16MW-15A 03/04/16Water
Samples were received in good condition at 1.8 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 56
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 6030100
03/15/2016
Summary of Detections
9.2 ug/L6030100-03 2765 INF 1,2-Dichloroethane SM6200 B
76 ug/L6030100-03 2765 INF Isopropyl Ether SM6200 B
60 ug/L6030100-03 2765 INF Methyl-tert-Butyl Ether SM6200 B
2.0 ug/L6030100-04 SW 2773 1,2-Dichloroethane SM6200 B
18 ug/L6030100-04 SW 2773 Isopropyl Ether SM6200 B
12 ug/L6030100-04 SW 2773 Methyl-tert-Butyl Ether SM6200 B
1.1 ug/L6030100-04 SW 2773 trans-1,2-Dichloroethylene SM6200 B
83 ug/L6030100-09 MW-1A 1,2,4-Trimethylbenzene SM6200 B
7.3 ug/L6030100-09 MW-1A 1,2-Dichloroethane SM6200 B
1.5 ug/L6030100-09 MW-1A 1,2-Dichloropropane SM6200 B
3.2 ug/L6030100-09 MW-1A 1,3,5-Trimethylbenzene SM6200 B
0.89 ug/L6030100-09 MW-1A 4-Isopropyltoluene SM6200 B
22 ug/L6030100-09 MW-1A Benzene SM6200 B
3.9 ug/L6030100-09 MW-1A Ethylbenzene SM6200 B
75 ug/L6030100-09 MW-1A Isopropyl Ether SM6200 B
3.2 ug/L6030100-09 MW-1A Isopropylbenzene (Cumene)SM6200 B
40 ug/L6030100-09 MW-1A m,p-Xylenes SM6200 B
8.5 ug/L6030100-09 MW-1A Methyl-tert-Butyl Ether SM6200 B
47 ug/L6030100-09 MW-1A Naphthalene SM6200 B
5.0 ug/L6030100-09 MW-1A n-Butylbenzene SM6200 B
2.7 ug/L6030100-09 MW-1A n-Propylbenzene SM6200 B
67 ug/L6030100-09 MW-1A o-Xylene SM6200 B
2.1 ug/L6030100-09 MW-1A sec-Butylbenzene SM6200 B
0.63 ug/L6030100-09 MW-1A tert-Butylbenzene SM6200 B
1.1 ug/L6030100-09 MW-1A Toluene SM6200 B
110 ug/L6030100-09 MW-1A Xylenes, total SM6200 B
0.79 J ug/L6030100-10 MW-3 Naphthalene SM6200 B
1.4 ug/L6030100-13 MW-6 Methyl-tert-Butyl Ether SM6200 B
1.1 ug/L6030100-18 MW-12 Isopropyl Ether SM6200 B
1.4 ug/L6030100-18 MW-12 Methyl-tert-Butyl Ether SM6200 B
11 ug/L6030100-20 MW-15A 1,2,4-Trimethylbenzene SM6200 B
0.98 ug/L6030100-20 MW-15A 1,3,5-Trimethylbenzene SM6200 B
0.83 ug/L6030100-20 MW-15A 4-Isopropyltoluene SM6200 B
0.82 ug/L6030100-20 MW-15A Benzene SM6200 B
15 ug/L6030100-20 MW-15A Ethylbenzene SM6200 B
0.98 ug/L6030100-20 MW-15A Isopropylbenzene (Cumene)SM6200 B
97 ug/L6030100-20 MW-15A m,p-Xylenes SM6200 B
30 ug/L6030100-20 MW-15A Naphthalene SM6200 B
0.75 ug/L6030100-20 MW-15A n-Propylbenzene SM6200 B
76 ug/L6030100-20 MW-15A o-Xylene SM6200 B
20 ug/L6030100-20 MW-15A Toluene SM6200 B
170 ug/L6030100-20 MW-15A Xylenes, total SM6200 B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765 EFF
Prism Sample ID: 6030100-01
Prism Work Order: 6030100
Time Collected: 02/29/16 13:15
Time Submitted: 03/04/16 14:30
Volatile Organic Compounds by GC/MS
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 16:09 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P6C021212.0 3/11/16 16:09 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P6C02121103/11/16 16:09 KDMug/L 0.31Acetone
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.048Benzene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.057Bromobenzene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.040Bromoform
BRL SM6200 B P6C021211.0 3/11/16 16:09 KDMug/L 0.18Bromomethane
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.22Chloroethane
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.076Chloroform
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMCCVug/L 0.079Chloromethane
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.065Dibromomethane
BRL SM6200 B P6C021211.0 3/11/16 16:09 KDMCCVug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P6C021212003/11/16 16:09 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765 EFF
Prism Sample ID: 6030100-01
Prism Work Order: 6030100
Time Collected: 02/29/16 13:15
Time Submitted: 03/04/16 14:30
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 16:09 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P6C021211.0 3/11/16 16:09 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P6C021211.0 3/11/16 16:09 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P6C021215.0 3/11/16 16:09 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P6C021211.0 3/11/16 16:09 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P6C021212.0 3/11/16 16:09 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P6C021211.0 3/11/16 16:09 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P6C021211.0 3/11/16 16:09 KDMug/L 0.19Naphthalene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.044o-Xylene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.047Styrene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.044Toluene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P6C021215.0 3/11/16 16:09 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P6C021210.50 3/11/16 16:09 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P6C021211.5 3/11/16 16:09 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
70-13099 %Dibromofluoromethane
70-13096 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765 Mid
Prism Sample ID: 6030100-02
Prism Work Order: 6030100
Time Collected: 02/29/16 13:25
Time Submitted: 03/04/16 14:30
Volatile Organic Compounds by GC/MS
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 16:43 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P6C021212.0 3/11/16 16:43 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P6C02121103/11/16 16:43 KDMug/L 0.31Acetone
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.048Benzene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.057Bromobenzene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.040Bromoform
BRL SM6200 B P6C021211.0 3/11/16 16:43 KDMug/L 0.18Bromomethane
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.22Chloroethane
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.076Chloroform
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMCCVug/L 0.079Chloromethane
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.065Dibromomethane
BRL SM6200 B P6C021211.0 3/11/16 16:43 KDMCCVug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P6C021212003/11/16 16:43 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765 Mid
Prism Sample ID: 6030100-02
Prism Work Order: 6030100
Time Collected: 02/29/16 13:25
Time Submitted: 03/04/16 14:30
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 16:43 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P6C021211.0 3/11/16 16:43 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P6C021211.0 3/11/16 16:43 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P6C021215.0 3/11/16 16:43 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P6C021211.0 3/11/16 16:43 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P6C021212.0 3/11/16 16:43 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P6C021211.0 3/11/16 16:43 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P6C021211.0 3/11/16 16:43 KDMug/L 0.19Naphthalene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.044o-Xylene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.047Styrene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.044Toluene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P6C021215.0 3/11/16 16:43 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P6C021210.50 3/11/16 16:43 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P6C021211.5 3/11/16 16:43 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
70-13097 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765 INF
Prism Sample ID: 6030100-03
Prism Work Order: 6030100
Time Collected: 02/29/16 13:35
Time Submitted: 03/04/16 14:30
Volatile Organic Compounds by GC/MS
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 17:17 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.0761,2-Dichlorobenzene
9.2 SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P6C021212.0 3/11/16 17:17 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P6C02121103/11/16 17:17 KDMug/L 0.31Acetone
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.048Benzene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.057Bromobenzene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.040Bromoform
BRL SM6200 B P6C021211.0 3/11/16 17:17 KDMug/L 0.18Bromomethane
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.22Chloroethane
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.076Chloroform
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMCCVug/L 0.079Chloromethane
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.065Dibromomethane
BRL SM6200 B P6C021211.0 3/11/16 17:17 KDMCCVug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P6C021212003/11/16 17:17 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765 INF
Prism Sample ID: 6030100-03
Prism Work Order: 6030100
Time Collected: 02/29/16 13:35
Time Submitted: 03/04/16 14:30
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 17:17 KDMug/L 0.16Hexachlorobutadiene
76 SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P6C021211.0 3/11/16 17:17 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P6C021211.0 3/11/16 17:17 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P6C021215.0 3/11/16 17:17 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P6C021211.0 3/11/16 17:17 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P6C021212.0 3/11/16 17:17 KDMug/L 0.083Methylene Chloride
60 SM6200 B P6C021211.0 3/11/16 17:17 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P6C021211.0 3/11/16 17:17 KDMug/L 0.19Naphthalene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.044o-Xylene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.047Styrene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.044Toluene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P6C021215.0 3/11/16 17:17 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P6C021210.50 3/11/16 17:17 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P6C021211.5 3/11/16 17:17 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
70-13098 %Dibromofluoromethane
70-13096 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW 2773
Prism Sample ID: 6030100-04
Prism Work Order: 6030100
Time Collected: 02/29/16 14:05
Time Submitted: 03/04/16 14:30
Volatile Organic Compounds by GC/MS
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 17:51 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.0761,2-Dichlorobenzene
2.0 SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P6C021212.0 3/11/16 17:51 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P6C02121103/11/16 17:51 KDMug/L 0.31Acetone
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.048Benzene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.057Bromobenzene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.040Bromoform
BRL SM6200 B P6C021211.0 3/11/16 17:51 KDMug/L 0.18Bromomethane
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.22Chloroethane
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.076Chloroform
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMCCVug/L 0.079Chloromethane
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.065Dibromomethane
BRL SM6200 B P6C021211.0 3/11/16 17:51 KDMCCVug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P6C021212003/11/16 17:51 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW 2773
Prism Sample ID: 6030100-04
Prism Work Order: 6030100
Time Collected: 02/29/16 14:05
Time Submitted: 03/04/16 14:30
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 17:51 KDMug/L 0.16Hexachlorobutadiene
18 SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P6C021211.0 3/11/16 17:51 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P6C021211.0 3/11/16 17:51 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P6C021215.0 3/11/16 17:51 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P6C021211.0 3/11/16 17:51 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P6C021212.0 3/11/16 17:51 KDMug/L 0.083Methylene Chloride
12 SM6200 B P6C021211.0 3/11/16 17:51 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P6C021211.0 3/11/16 17:51 KDMug/L 0.19Naphthalene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.044o-Xylene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.047Styrene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.044Toluene
1.1 SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P6C021215.0 3/11/16 17:51 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P6C021210.50 3/11/16 17:51 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P6C021211.5 3/11/16 17:51 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW 2779
Prism Sample ID: 6030100-05
Prism Work Order: 6030100
Time Collected: 02/29/16 14:35
Time Submitted: 03/04/16 14:30
Volatile Organic Compounds by GC/MS
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 18:26 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P6C021212.0 3/11/16 18:26 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P6C02121103/11/16 18:26 KDMug/L 0.31Acetone
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.048Benzene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.057Bromobenzene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.040Bromoform
BRL SM6200 B P6C021211.0 3/11/16 18:26 KDMug/L 0.18Bromomethane
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.22Chloroethane
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.076Chloroform
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMCCVug/L 0.079Chloromethane
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.065Dibromomethane
BRL SM6200 B P6C021211.0 3/11/16 18:26 KDMCCVug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P6C021212003/11/16 18:26 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW 2779
Prism Sample ID: 6030100-05
Prism Work Order: 6030100
Time Collected: 02/29/16 14:35
Time Submitted: 03/04/16 14:30
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 18:26 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P6C021211.0 3/11/16 18:26 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P6C021211.0 3/11/16 18:26 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P6C021215.0 3/11/16 18:26 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P6C021211.0 3/11/16 18:26 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P6C021212.0 3/11/16 18:26 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P6C021211.0 3/11/16 18:26 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P6C021211.0 3/11/16 18:26 KDMug/L 0.19Naphthalene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.044o-Xylene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.047Styrene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.044Toluene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P6C021215.0 3/11/16 18:26 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P6C021210.50 3/11/16 18:26 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P6C021211.5 3/11/16 18:26 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13096 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW 2768B
Prism Sample ID: 6030100-06
Prism Work Order: 6030100
Time Collected: 02/29/16 14:55
Time Submitted: 03/04/16 14:30
Volatile Organic Compounds by GC/MS
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 19:00 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P6C021212.0 3/11/16 19:00 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P6C02121103/11/16 19:00 KDMug/L 0.31Acetone
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.048Benzene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.057Bromobenzene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.040Bromoform
BRL SM6200 B P6C021211.0 3/11/16 19:00 KDMug/L 0.18Bromomethane
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.22Chloroethane
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.076Chloroform
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMCCVug/L 0.079Chloromethane
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.065Dibromomethane
BRL SM6200 B P6C021211.0 3/11/16 19:00 KDMCCVug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P6C021212003/11/16 19:00 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW 2768B
Prism Sample ID: 6030100-06
Prism Work Order: 6030100
Time Collected: 02/29/16 14:55
Time Submitted: 03/04/16 14:30
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 19:00 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P6C021211.0 3/11/16 19:00 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P6C021211.0 3/11/16 19:00 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P6C021215.0 3/11/16 19:00 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P6C021211.0 3/11/16 19:00 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P6C021212.0 3/11/16 19:00 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P6C021211.0 3/11/16 19:00 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P6C021211.0 3/11/16 19:00 KDMug/L 0.19Naphthalene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.044o-Xylene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.047Styrene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.044Toluene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P6C021215.0 3/11/16 19:00 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P6C021210.50 3/11/16 19:00 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P6C021211.5 3/11/16 19:00 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
70-130101 %Dibromofluoromethane
70-13096 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW 2760
Prism Sample ID: 6030100-07
Prism Work Order: 6030100
Time Collected: 02/29/16 15:15
Time Submitted: 03/04/16 14:30
Volatile Organic Compounds by GC/MS
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 19:34 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P6C021212.0 3/11/16 19:34 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P6C02121103/11/16 19:34 KDMug/L 0.31Acetone
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.048Benzene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.057Bromobenzene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.040Bromoform
BRL SM6200 B P6C021211.0 3/11/16 19:34 KDMug/L 0.18Bromomethane
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.22Chloroethane
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.076Chloroform
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMCCVug/L 0.079Chloromethane
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.065Dibromomethane
BRL SM6200 B P6C021211.0 3/11/16 19:34 KDMCCVug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P6C021212003/11/16 19:34 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW 2760
Prism Sample ID: 6030100-07
Prism Work Order: 6030100
Time Collected: 02/29/16 15:15
Time Submitted: 03/04/16 14:30
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 19:34 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P6C021211.0 3/11/16 19:34 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P6C021211.0 3/11/16 19:34 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P6C021215.0 3/11/16 19:34 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P6C021211.0 3/11/16 19:34 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P6C021212.0 3/11/16 19:34 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P6C021211.0 3/11/16 19:34 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P6C021211.0 3/11/16 19:34 KDMug/L 0.19Naphthalene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.044o-Xylene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.047Styrene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.044Toluene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P6C021215.0 3/11/16 19:34 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P6C021210.50 3/11/16 19:34 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P6C021211.5 3/11/16 19:34 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13096 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW 2774
Prism Sample ID: 6030100-08
Prism Work Order: 6030100
Time Collected: 02/29/16 15:35
Time Submitted: 03/04/16 14:30
Volatile Organic Compounds by GC/MS
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 20:08 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P6C021212.0 3/11/16 20:08 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P6C02121103/11/16 20:08 KDMug/L 0.31Acetone
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.048Benzene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.057Bromobenzene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.040Bromoform
BRL SM6200 B P6C021211.0 3/11/16 20:08 KDMug/L 0.18Bromomethane
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.22Chloroethane
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.076Chloroform
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMCCVug/L 0.079Chloromethane
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.065Dibromomethane
BRL SM6200 B P6C021211.0 3/11/16 20:08 KDMCCVug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P6C021212003/11/16 20:08 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW 2774
Prism Sample ID: 6030100-08
Prism Work Order: 6030100
Time Collected: 02/29/16 15:35
Time Submitted: 03/04/16 14:30
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 20:08 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P6C021211.0 3/11/16 20:08 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P6C021211.0 3/11/16 20:08 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P6C021215.0 3/11/16 20:08 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P6C021211.0 3/11/16 20:08 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P6C021212.0 3/11/16 20:08 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P6C021211.0 3/11/16 20:08 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P6C021211.0 3/11/16 20:08 KDMug/L 0.19Naphthalene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.044o-Xylene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.047Styrene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.044Toluene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P6C021215.0 3/11/16 20:08 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P6C021210.50 3/11/16 20:08 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P6C021211.5 3/11/16 20:08 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
70-13098 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-1A
Prism Sample ID: 6030100-09
Prism Work Order: 6030100
Time Collected: 03/02/16 14:40
Time Submitted: 03/04/16 14:30
Volatile Organic Compounds by GC/MS
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.131,2,4-Trichlorobenzene
83 SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 20:42 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.0761,2-Dichlorobenzene
7.3 SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.0661,2-Dichloroethane
1.5 SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.111,2-Dichloropropane
3.2 SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P6C021212.0 3/11/16 20:42 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.0504-Chlorotoluene
0.89 SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P6C02121103/11/16 20:42 KDMug/L 0.31Acetone
22 SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.048Benzene
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.057Bromobenzene
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.040Bromoform
BRL SM6200 B P6C021211.0 3/11/16 20:42 KDMug/L 0.18Bromomethane
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.22Chloroethane
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.076Chloroform
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMCCVug/L 0.079Chloromethane
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.065Dibromomethane
BRL SM6200 B P6C021211.0 3/11/16 20:42 KDMCCVug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P6C021212003/11/16 20:42 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-1A
Prism Sample ID: 6030100-09
Prism Work Order: 6030100
Time Collected: 03/02/16 14:40
Time Submitted: 03/04/16 14:30
3.9 SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 20:42 KDMug/L 0.16Hexachlorobutadiene
75 SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.050Isopropyl Ether
3.2 SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.054Isopropylbenzene (Cumene)
40 SM6200 B P6C021211.0 3/11/16 20:42 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P6C021211.0 3/11/16 20:42 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P6C021215.0 3/11/16 20:42 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P6C021211.0 3/11/16 20:42 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P6C021212.0 3/11/16 20:42 KDMug/L 0.083Methylene Chloride
8.5 SM6200 B P6C021211.0 3/11/16 20:42 KDMug/L 0.042Methyl-tert-Butyl Ether
47 SM6200 B P6C021211.0 3/11/16 20:42 KDMug/L 0.19Naphthalene
5.0 SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.076n-Butylbenzene
2.7 SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.087n-Propylbenzene
67 SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.044o-Xylene
2.1 SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.047Styrene
0.63 SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.098Tetrachloroethylene
1.1 SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.044Toluene
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P6C021215.0 3/11/16 20:42 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P6C021210.50 3/11/16 20:42 KDMug/L 0.097Vinyl chloride
110 SM6200 B P6C021211.5 3/11/16 20:42 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13095 %4-Bromofluorobenzene
70-13095 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-3
Prism Sample ID: 6030100-10
Prism Work Order: 6030100
Time Collected: 03/02/16 14:00
Time Submitted: 03/04/16 14:30
Volatile Organic Compounds by GC/MS
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 21:16 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P6C021212.0 3/11/16 21:16 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P6C02121103/11/16 21:16 KDMug/L 0.31Acetone
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.048Benzene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.057Bromobenzene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.040Bromoform
BRL SM6200 B P6C021211.0 3/11/16 21:16 KDMug/L 0.18Bromomethane
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.22Chloroethane
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.076Chloroform
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMCCVug/L 0.079Chloromethane
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.065Dibromomethane
BRL SM6200 B P6C021211.0 3/11/16 21:16 KDMCCVug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P6C021212003/11/16 21:16 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-3
Prism Sample ID: 6030100-10
Prism Work Order: 6030100
Time Collected: 03/02/16 14:00
Time Submitted: 03/04/16 14:30
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 21:16 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P6C021211.0 3/11/16 21:16 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P6C021211.0 3/11/16 21:16 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P6C021215.0 3/11/16 21:16 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P6C021211.0 3/11/16 21:16 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P6C021212.0 3/11/16 21:16 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P6C021211.0 3/11/16 21:16 KDMug/L 0.042Methyl-tert-Butyl Ether
0.79 SM6200 B P6C021211.0 3/11/16 21:16 KDMJug/L 0.19Naphthalene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.044o-Xylene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.047Styrene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.044Toluene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P6C021215.0 3/11/16 21:16 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P6C021210.50 3/11/16 21:16 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P6C021211.5 3/11/16 21:16 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130103 %4-Bromofluorobenzene
70-13099 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-4
Prism Sample ID: 6030100-11
Prism Work Order: 6030100
Time Collected: 03/02/16 13:50
Time Submitted: 03/04/16 14:30
Volatile Organic Compounds by GC/MS
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 21:50 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P6C021212.0 3/11/16 21:50 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P6C02121103/11/16 21:50 KDMug/L 0.31Acetone
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.048Benzene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.057Bromobenzene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.040Bromoform
BRL SM6200 B P6C021211.0 3/11/16 21:50 KDMug/L 0.18Bromomethane
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.22Chloroethane
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.076Chloroform
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMCCVug/L 0.079Chloromethane
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.065Dibromomethane
BRL SM6200 B P6C021211.0 3/11/16 21:50 KDMCCVug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P6C021212003/11/16 21:50 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-4
Prism Sample ID: 6030100-11
Prism Work Order: 6030100
Time Collected: 03/02/16 13:50
Time Submitted: 03/04/16 14:30
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 21:50 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P6C021211.0 3/11/16 21:50 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P6C021211.0 3/11/16 21:50 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P6C021215.0 3/11/16 21:50 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P6C021211.0 3/11/16 21:50 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P6C021212.0 3/11/16 21:50 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P6C021211.0 3/11/16 21:50 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P6C021211.0 3/11/16 21:50 KDMug/L 0.19Naphthalene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.044o-Xylene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.047Styrene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.044Toluene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P6C021215.0 3/11/16 21:50 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P6C021210.50 3/11/16 21:50 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P6C021211.5 3/11/16 21:50 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
70-13098 %Dibromofluoromethane
70-13096 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-5
Prism Sample ID: 6030100-12
Prism Work Order: 6030100
Time Collected: 03/02/16 14:20
Time Submitted: 03/04/16 14:30
Volatile Organic Compounds by GC/MS
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 22:24 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P6C021212.0 3/11/16 22:24 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P6C02121103/11/16 22:24 KDMug/L 0.31Acetone
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.048Benzene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.057Bromobenzene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.040Bromoform
BRL SM6200 B P6C021211.0 3/11/16 22:24 KDMug/L 0.18Bromomethane
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.22Chloroethane
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.076Chloroform
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMCCVug/L 0.079Chloromethane
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.065Dibromomethane
BRL SM6200 B P6C021211.0 3/11/16 22:24 KDMCCVug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P6C021212003/11/16 22:24 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-5
Prism Sample ID: 6030100-12
Prism Work Order: 6030100
Time Collected: 03/02/16 14:20
Time Submitted: 03/04/16 14:30
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 22:24 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P6C021211.0 3/11/16 22:24 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P6C021211.0 3/11/16 22:24 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P6C021215.0 3/11/16 22:24 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P6C021211.0 3/11/16 22:24 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P6C021212.0 3/11/16 22:24 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P6C021211.0 3/11/16 22:24 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P6C021211.0 3/11/16 22:24 KDMug/L 0.19Naphthalene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.044o-Xylene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.047Styrene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.044Toluene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P6C021215.0 3/11/16 22:24 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P6C021210.50 3/11/16 22:24 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P6C021211.5 3/11/16 22:24 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-6
Prism Sample ID: 6030100-13
Prism Work Order: 6030100
Time Collected: 03/02/16 14:50
Time Submitted: 03/04/16 14:30
Volatile Organic Compounds by GC/MS
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 22:58 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P6C021212.0 3/11/16 22:58 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P6C02121103/11/16 22:58 KDMug/L 0.31Acetone
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.048Benzene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.057Bromobenzene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.040Bromoform
BRL SM6200 B P6C021211.0 3/11/16 22:58 KDMug/L 0.18Bromomethane
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.22Chloroethane
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.076Chloroform
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMCCVug/L 0.079Chloromethane
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.065Dibromomethane
BRL SM6200 B P6C021211.0 3/11/16 22:58 KDMCCVug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P6C021212003/11/16 22:58 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-6
Prism Sample ID: 6030100-13
Prism Work Order: 6030100
Time Collected: 03/02/16 14:50
Time Submitted: 03/04/16 14:30
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 22:58 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P6C021211.0 3/11/16 22:58 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P6C021211.0 3/11/16 22:58 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P6C021215.0 3/11/16 22:58 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P6C021211.0 3/11/16 22:58 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P6C021212.0 3/11/16 22:58 KDMug/L 0.083Methylene Chloride
1.4 SM6200 B P6C021211.0 3/11/16 22:58 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P6C021211.0 3/11/16 22:58 KDMug/L 0.19Naphthalene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.044o-Xylene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.047Styrene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.044Toluene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P6C021215.0 3/11/16 22:58 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P6C021210.50 3/11/16 22:58 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P6C021211.5 3/11/16 22:58 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-130101 %Dibromofluoromethane
70-13096 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-7
Prism Sample ID: 6030100-14
Prism Work Order: 6030100
Time Collected: 03/02/16 14:10
Time Submitted: 03/04/16 14:30
Volatile Organic Compounds by GC/MS
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 23:32 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P6C021212.0 3/11/16 23:32 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P6C02121103/11/16 23:32 KDMug/L 0.31Acetone
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.048Benzene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.057Bromobenzene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.040Bromoform
BRL SM6200 B P6C021211.0 3/11/16 23:32 KDMug/L 0.18Bromomethane
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.22Chloroethane
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.076Chloroform
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMCCVug/L 0.079Chloromethane
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.065Dibromomethane
BRL SM6200 B P6C021211.0 3/11/16 23:32 KDMCCVug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P6C021212003/11/16 23:32 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-7
Prism Sample ID: 6030100-14
Prism Work Order: 6030100
Time Collected: 03/02/16 14:10
Time Submitted: 03/04/16 14:30
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P6C021212.0 3/11/16 23:32 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P6C021211.0 3/11/16 23:32 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P6C021211.0 3/11/16 23:32 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P6C021215.0 3/11/16 23:32 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P6C021211.0 3/11/16 23:32 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P6C021212.0 3/11/16 23:32 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P6C021211.0 3/11/16 23:32 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P6C021211.0 3/11/16 23:32 KDMug/L 0.19Naphthalene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.044o-Xylene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.047Styrene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.044Toluene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P6C021215.0 3/11/16 23:32 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P6C021210.50 3/11/16 23:32 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P6C021211.5 3/11/16 23:32 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
70-13099 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-9
Prism Sample ID: 6030100-15
Prism Work Order: 6030100
Time Collected: 03/02/16 13:30
Time Submitted: 03/04/16 14:30
Volatile Organic Compounds by GC/MS
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P6C021212.0 3/12/16 0:06 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P6C021212.0 3/12/16 0:06 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P6C02121103/12/16 0:06 KDMug/L 0.31Acetone
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.048Benzene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.057Bromobenzene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.040Bromoform
BRL SM6200 B P6C021211.0 3/12/16 0:06 KDMug/L 0.18Bromomethane
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.22Chloroethane
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.076Chloroform
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMCCVug/L 0.079Chloromethane
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.065Dibromomethane
BRL SM6200 B P6C021211.0 3/12/16 0:06 KDMCCVug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P6C021212003/12/16 0:06 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-9
Prism Sample ID: 6030100-15
Prism Work Order: 6030100
Time Collected: 03/02/16 13:30
Time Submitted: 03/04/16 14:30
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P6C021212.0 3/12/16 0:06 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P6C021211.0 3/12/16 0:06 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P6C021211.0 3/12/16 0:06 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P6C021215.0 3/12/16 0:06 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P6C021211.0 3/12/16 0:06 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P6C021212.0 3/12/16 0:06 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P6C021211.0 3/12/16 0:06 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P6C021211.0 3/12/16 0:06 KDMug/L 0.19Naphthalene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.044o-Xylene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.047Styrene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.044Toluene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P6C021215.0 3/12/16 0:06 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P6C021210.50 3/12/16 0:06 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P6C021211.5 3/12/16 0:06 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13096 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-10
Prism Sample ID: 6030100-16
Prism Work Order: 6030100
Time Collected: 03/02/16 13:40
Time Submitted: 03/04/16 14:30
Volatile Organic Compounds by GC/MS
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P6C021212.0 3/12/16 0:40 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P6C021212.0 3/12/16 0:40 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P6C02121103/12/16 0:40 KDMug/L 0.31Acetone
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.048Benzene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.057Bromobenzene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.040Bromoform
BRL SM6200 B P6C021211.0 3/12/16 0:40 KDMug/L 0.18Bromomethane
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.22Chloroethane
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.076Chloroform
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMCCVug/L 0.079Chloromethane
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.065Dibromomethane
BRL SM6200 B P6C021211.0 3/12/16 0:40 KDMCCVug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P6C021212003/12/16 0:40 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-10
Prism Sample ID: 6030100-16
Prism Work Order: 6030100
Time Collected: 03/02/16 13:40
Time Submitted: 03/04/16 14:30
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P6C021212.0 3/12/16 0:40 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P6C021211.0 3/12/16 0:40 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P6C021211.0 3/12/16 0:40 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P6C021215.0 3/12/16 0:40 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P6C021211.0 3/12/16 0:40 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P6C021212.0 3/12/16 0:40 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P6C021211.0 3/12/16 0:40 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P6C021211.0 3/12/16 0:40 KDMug/L 0.19Naphthalene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.044o-Xylene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.047Styrene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.044Toluene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P6C021215.0 3/12/16 0:40 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P6C021210.50 3/12/16 0:40 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P6C021211.5 3/12/16 0:40 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-13098 %Dibromofluoromethane
70-13096 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-11
Prism Sample ID: 6030100-17
Prism Work Order: 6030100
Time Collected: 03/02/16 13:10
Time Submitted: 03/04/16 14:30
Volatile Organic Compounds by GC/MS
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P6C024012.0 3/14/16 18:51 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P6C024012.0 3/14/16 18:51 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P6C02401103/14/16 18:51 KDMug/L 0.31Acetone
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.048Benzene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.057Bromobenzene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.040Bromoform
BRL SM6200 B P6C024011.0 3/14/16 18:51 KDMug/L 0.18Bromomethane
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.22Chloroethane
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.076Chloroform
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.079Chloromethane
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.065Dibromomethane
BRL SM6200 B P6C024011.0 3/14/16 18:51 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P6C024012003/14/16 18:51 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-11
Prism Sample ID: 6030100-17
Prism Work Order: 6030100
Time Collected: 03/02/16 13:10
Time Submitted: 03/04/16 14:30
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P6C024012.0 3/14/16 18:51 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P6C024011.0 3/14/16 18:51 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P6C024011.0 3/14/16 18:51 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P6C024015.0 3/14/16 18:51 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P6C024011.0 3/14/16 18:51 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P6C024012.0 3/14/16 18:51 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P6C024011.0 3/14/16 18:51 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P6C024011.0 3/14/16 18:51 KDMug/L 0.19Naphthalene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.044o-Xylene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.047Styrene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.044Toluene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P6C024015.0 3/14/16 18:51 KDMCCVug/L 0.060Vinyl acetate
BRL SM6200 B P6C024010.50 3/14/16 18:51 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P6C024011.5 3/14/16 18:51 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13095 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-12
Prism Sample ID: 6030100-18
Prism Work Order: 6030100
Time Collected: 03/02/16 13:20
Time Submitted: 03/04/16 14:30
Volatile Organic Compounds by GC/MS
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P6C024012.0 3/14/16 19:25 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P6C024012.0 3/14/16 19:25 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P6C02401103/14/16 19:25 KDMug/L 0.31Acetone
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.048Benzene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.057Bromobenzene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.040Bromoform
BRL SM6200 B P6C024011.0 3/14/16 19:25 KDMug/L 0.18Bromomethane
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.22Chloroethane
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.076Chloroform
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.079Chloromethane
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.065Dibromomethane
BRL SM6200 B P6C024011.0 3/14/16 19:25 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P6C024012003/14/16 19:25 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-12
Prism Sample ID: 6030100-18
Prism Work Order: 6030100
Time Collected: 03/02/16 13:20
Time Submitted: 03/04/16 14:30
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P6C024012.0 3/14/16 19:25 KDMug/L 0.16Hexachlorobutadiene
1.1 SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P6C024011.0 3/14/16 19:25 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P6C024011.0 3/14/16 19:25 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P6C024015.0 3/14/16 19:25 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P6C024011.0 3/14/16 19:25 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P6C024012.0 3/14/16 19:25 KDMug/L 0.083Methylene Chloride
1.4 SM6200 B P6C024011.0 3/14/16 19:25 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P6C024011.0 3/14/16 19:25 KDMug/L 0.19Naphthalene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.044o-Xylene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.047Styrene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.044Toluene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P6C024015.0 3/14/16 19:25 KDMCCVug/L 0.060Vinyl acetate
BRL SM6200 B P6C024010.50 3/14/16 19:25 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P6C024011.5 3/14/16 19:25 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
70-130102 %Dibromofluoromethane
70-13094 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-13
Prism Sample ID: 6030100-19
Prism Work Order: 6030100
Time Collected: 03/02/16 15:00
Time Submitted: 03/04/16 14:30
Volatile Organic Compounds by GC/MS
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P6C024012.0 3/14/16 19:59 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P6C024012.0 3/14/16 19:59 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P6C02401103/14/16 19:59 KDMug/L 0.31Acetone
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.048Benzene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.057Bromobenzene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.040Bromoform
BRL SM6200 B P6C024011.0 3/14/16 19:59 KDMug/L 0.18Bromomethane
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.22Chloroethane
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.076Chloroform
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.079Chloromethane
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.065Dibromomethane
BRL SM6200 B P6C024011.0 3/14/16 19:59 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P6C024012003/14/16 19:59 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-13
Prism Sample ID: 6030100-19
Prism Work Order: 6030100
Time Collected: 03/02/16 15:00
Time Submitted: 03/04/16 14:30
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P6C024012.0 3/14/16 19:59 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P6C024011.0 3/14/16 19:59 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P6C024011.0 3/14/16 19:59 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P6C024015.0 3/14/16 19:59 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P6C024011.0 3/14/16 19:59 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P6C024012.0 3/14/16 19:59 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P6C024011.0 3/14/16 19:59 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P6C024011.0 3/14/16 19:59 KDMug/L 0.19Naphthalene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.044o-Xylene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.047Styrene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.044Toluene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P6C024015.0 3/14/16 19:59 KDMCCVug/L 0.060Vinyl acetate
BRL SM6200 B P6C024010.50 3/14/16 19:59 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P6C024011.5 3/14/16 19:59 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13095 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 41 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-15A
Prism Sample ID: 6030100-20
Prism Work Order: 6030100
Time Collected: 03/02/16 14:30
Time Submitted: 03/04/16 14:30
Volatile Organic Compounds by GC/MS
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.131,2,4-Trichlorobenzene
11 SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P6C024012.0 3/14/16 23:23 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.111,2-Dichloropropane
0.98 SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P6C024012.0 3/14/16 23:23 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.0504-Chlorotoluene
0.83 SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P6C02401103/14/16 23:23 KDMug/L 0.31Acetone
0.82 SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.048Benzene
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.057Bromobenzene
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.040Bromoform
BRL SM6200 B P6C024011.0 3/14/16 23:23 KDMug/L 0.18Bromomethane
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.22Chloroethane
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.076Chloroform
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.079Chloromethane
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.065Dibromomethane
BRL SM6200 B P6C024011.0 3/14/16 23:23 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P6C024012003/14/16 23:23 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 42 of 56
Laboratory Report
03/15/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-15A
Prism Sample ID: 6030100-20
Prism Work Order: 6030100
Time Collected: 03/02/16 14:30
Time Submitted: 03/04/16 14:30
15 SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P6C024012.0 3/14/16 23:23 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.050Isopropyl Ether
0.98 SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.054Isopropylbenzene (Cumene)
97 SM6200 B P6C024011.0 3/14/16 23:23 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P6C024011.0 3/14/16 23:23 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P6C024015.0 3/14/16 23:23 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P6C024011.0 3/14/16 23:23 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P6C024012.0 3/14/16 23:23 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P6C024011.0 3/14/16 23:23 KDMug/L 0.042Methyl-tert-Butyl Ether
30 SM6200 B P6C024011.0 3/14/16 23:23 KDMug/L 0.19Naphthalene
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.076n-Butylbenzene
0.75 SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.087n-Propylbenzene
76 SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.044o-Xylene
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.047Styrene
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.098Tetrachloroethylene
20 SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.044Toluene
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P6C024015.0 3/14/16 23:23 KDMCCVug/L 0.060Vinyl acetate
BRL SM6200 B P6C024010.50 3/14/16 23:23 KDMug/L 0.097Vinyl chloride
170 SM6200 B P6C024011.5 3/14/16 23:23 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
70-13097 %Dibromofluoromethane
70-13095 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 43 of 56
3/15/16
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 6030100
Time Submitted: 3/4/2016 2:30:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6C0212 - SM6200 B
Blank (P6C0212-BLK1)Prepared & Analyzed: 03/11/16
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL0.50
1,2,4-Trichlorobenzene ug/LBRL0.50
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL10
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL0.50
Bromomethane ug/LBRL1.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethanol ug/LBRL200
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 44 of 56
3/15/16
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 6030100
Time Submitted: 3/4/2016 2:30:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6C0212 - SM6200 B
Blank (P6C0212-BLK1)Prepared & Analyzed: 03/11/16
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL1.0
Methylene Chloride ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL1.0
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL0.50
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Butylbenzene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL5.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10150.6
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9849.2
ug/L 50.00 70-130Surrogate: Toluene-d8 9748.7
LCS (P6C0212-BS1)Prepared & Analyzed: 03/11/16
1,1,1,2-Tetrachloroethane ug/L18.6 0.50 20.00 70-13093
1,1,1-Trichloroethane ug/L20.0 0.50 20.00 70-130100
1,1,2,2-Tetrachloroethane ug/L19.9 0.50 20.00 70-130100
1,1,2-Trichloroethane ug/L21.8 0.50 20.00 70-130109
1,1-Dichloroethane ug/L22.1 0.50 20.00 70-130110
1,1-Dichloroethylene ug/L23.6 0.50 20.00 70-130118
1,1-Dichloropropylene ug/L20.2 0.50 20.00 70-130101
1,2,3-Trichlorobenzene ug/L19.6 0.50 20.00 70-13098
1,2,3-Trichloropropane ug/L18.2 0.50 20.00 70-13091
1,2,4-Trichlorobenzene ug/L20.2 0.50 20.00 70-130101
1,2,4-Trimethylbenzene ug/L21.0 0.50 20.00 70-130105
1,2-Dibromo-3-chloropropane ug/L18.4 2.0 20.00 70-13092
1,2-Dibromoethane ug/L18.3 0.50 20.00 70-13091
1,2-Dichlorobenzene ug/L19.9 0.50 20.00 70-13099
1,2-Dichloroethane ug/L21.1 0.50 20.00 70-130106
1,2-Dichloropropane ug/L19.8 0.50 20.00 70-13099
1,3,5-Trimethylbenzene ug/L21.2 0.50 20.00 70-130106
1,3-Dichlorobenzene ug/L20.3 0.50 20.00 70-130102
1,3-Dichloropropane ug/L20.5 0.50 20.00 70-130102
1,4-Dichlorobenzene ug/L19.8 0.50 20.00 70-13099
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 45 of 56
3/15/16
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 6030100
Time Submitted: 3/4/2016 2:30:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6C0212 - SM6200 B
LCS (P6C0212-BS1)Prepared & Analyzed: 03/11/16
2,2-Dichloropropane ug/L25.6 2.0 20.00 70-130128
2-Chlorotoluene ug/L20.6 0.50 20.00 70-130103
4-Chlorotoluene ug/L20.6 0.50 20.00 70-130103
4-Isopropyltoluene ug/L21.0 0.50 20.00 70-130105
Acetone ug/L40.6 10 40.00 40-160101
Benzene ug/L22.1 0.50 20.00 70-130110
Bromobenzene ug/L20.0 0.50 20.00 70-130100
Bromochloromethane ug/L20.1 0.50 20.00 70-130101
Bromodichloromethane ug/L20.7 0.50 20.00 70-130104
Bromoform ug/L17.9 0.50 20.00 70-13090
Bromomethane ug/L24.9 1.0 20.00 60-140125
Carbon Tetrachloride ug/L20.0 0.50 20.00 70-130100
Chlorobenzene ug/L20.9 0.50 20.00 70-130105
Chloroethane ug/L25.2 0.50 20.00 60-140126
Chloroform ug/L20.7 0.50 20.00 70-130104
Chloromethane ug/L29.4 0.50 20.00 LH60-140147
cis-1,2-Dichloroethylene ug/L21.2 0.50 20.00 70-130106
cis-1,3-Dichloropropylene ug/L20.2 0.50 20.00 70-130101
Dibromochloromethane ug/L18.2 0.50 20.00 70-13091
Dibromomethane ug/L19.6 0.50 20.00 70-13098
Dichlorodifluoromethane ug/L34.9 1.0 20.00 LH60-140174
Ethanol ug/L545200 500.0 60-140109
Ethylbenzene ug/L21.4 0.50 20.00 70-130107
Hexachlorobutadiene ug/L21.4 2.0 20.00 70-130107
Isopropyl Ether ug/L22.3 0.50 20.00 70-130112
Isopropylbenzene (Cumene)ug/L21.2 0.50 20.00 70-130106
m,p-Xylenes ug/L43.1 1.0 40.00 70-130108
Methyl Butyl Ketone (2-Hexanone)ug/L18.8 1.0 20.00 60-14094
Methyl Ethyl Ketone (2-Butanone)ug/L20.1 5.0 20.00 60-140100
Methyl Isobutyl Ketone ug/L19.6 1.0 20.00 60-14098
Methylene Chloride ug/L20.9 2.0 20.00 70-130104
Methyl-tert-Butyl Ether ug/L21.9 1.0 20.00 70-130110
Naphthalene ug/L19.0 1.0 20.00 70-13095
n-Butylbenzene ug/L21.2 0.50 20.00 70-130106
n-Propylbenzene ug/L21.0 0.50 20.00 70-130105
o-Xylene ug/L21.0 0.50 20.00 70-130105
sec-Butylbenzene ug/L21.5 0.50 20.00 70-130107
Styrene ug/L21.4 0.50 20.00 70-130107
tert-Butylbenzene ug/L21.1 0.50 20.00 70-130105
Tetrachloroethylene ug/L21.6 0.50 20.00 70-130108
Toluene ug/L21.9 0.50 20.00 70-130109
trans-1,2-Dichloroethylene ug/L22.7 0.50 20.00 70-130114
trans-1,3-Dichloropropylene ug/L19.6 0.50 20.00 70-13098
Trichloroethylene ug/L20.1 0.50 20.00 70-130100
Trichlorofluoromethane ug/L23.1 0.50 20.00 60-140116
Vinyl acetate ug/L27.8 5.0 20.00 60-140139
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 46 of 56
3/15/16
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 6030100
Time Submitted: 3/4/2016 2:30:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6C0212 - SM6200 B
LCS (P6C0212-BS1)Prepared & Analyzed: 03/11/16
Vinyl chloride ug/L27.8 0.50 20.00 60-140139
Xylenes, total ug/L64.1 1.5 60.00 70-130107
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9848.9
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9949.5
ug/L 50.00 70-130Surrogate: Toluene-d8 9748.6
LCS Dup (P6C0212-BSD1)Prepared & Analyzed: 03/11/16
1,1,1,2-Tetrachloroethane ug/L18.7 0.50 20.00 2070-13093 0.4
1,1,1-Trichloroethane ug/L19.8 0.50 20.00 2070-13099 0.6
1,1,2,2-Tetrachloroethane ug/L19.7 0.50 20.00 2070-13098 1
1,1,2-Trichloroethane ug/L21.0 0.50 20.00 2070-130105 4
1,1-Dichloroethane ug/L21.6 0.50 20.00 2070-130108 2
1,1-Dichloroethylene ug/L23.0 0.50 20.00 2070-130115 2
1,1-Dichloropropylene ug/L20.0 0.50 20.00 2070-130100 0.7
1,2,3-Trichlorobenzene ug/L19.6 0.50 20.00 2070-13098 0.2
1,2,3-Trichloropropane ug/L17.7 0.50 20.00 2070-13088 3
1,2,4-Trichlorobenzene ug/L19.3 0.50 20.00 2070-13096 4
1,2,4-Trimethylbenzene ug/L20.3 0.50 20.00 2070-130101 4
1,2-Dibromo-3-chloropropane ug/L19.2 2.0 20.00 2070-13096 4
1,2-Dibromoethane ug/L18.8 0.50 20.00 2070-13094 3
1,2-Dichlorobenzene ug/L19.6 0.50 20.00 2070-13098 1
1,2-Dichloroethane ug/L21.0 0.50 20.00 2070-130105 0.6
1,2-Dichloropropane ug/L19.4 0.50 20.00 2070-13097 2
1,3,5-Trimethylbenzene ug/L20.8 0.50 20.00 2070-130104 2
1,3-Dichlorobenzene ug/L19.8 0.50 20.00 2070-13099 2
1,3-Dichloropropane ug/L20.5 0.50 20.00 2070-130103 0.3
1,4-Dichlorobenzene ug/L19.4 0.50 20.00 2070-13097 3
2,2-Dichloropropane ug/L25.2 2.0 20.00 2070-130126 2
2-Chlorotoluene ug/L20.2 0.50 20.00 2070-130101 2
4-Chlorotoluene ug/L19.9 0.50 20.00 2070-13099 4
4-Isopropyltoluene ug/L20.4 0.50 20.00 2070-130102 3
Acetone ug/L43.2 10 40.00 2040-160108 6
Benzene ug/L21.6 0.50 20.00 2070-130108 2
Bromobenzene ug/L19.8 0.50 20.00 2070-13099 0.9
Bromochloromethane ug/L20.2 0.50 20.00 2070-130101 0.2
Bromodichloromethane ug/L20.1 0.50 20.00 2070-130101 3
Bromoform ug/L17.8 0.50 20.00 2070-13089 0.6
Bromomethane ug/L25.1 1.0 20.00 2060-140126 0.8
Carbon Tetrachloride ug/L19.4 0.50 20.00 2070-13097 3
Chlorobenzene ug/L20.5 0.50 20.00 2070-130103 2
Chloroethane ug/L24.4 0.50 20.00 2060-140122 3
Chloroform ug/L20.1 0.50 20.00 2070-130101 3
Chloromethane ug/L28.8 0.50 20.00 20 LH60-140144 2
cis-1,2-Dichloroethylene ug/L20.6 0.50 20.00 2070-130103 3
cis-1,3-Dichloropropylene ug/L20.0 0.50 20.00 2070-130100 0.7
Dibromochloromethane ug/L18.4 0.50 20.00 2070-13092 1
Dibromomethane ug/L19.2 0.50 20.00 2070-13096 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 47 of 56
3/15/16
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 6030100
Time Submitted: 3/4/2016 2:30:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6C0212 - SM6200 B
LCS Dup (P6C0212-BSD1)Prepared & Analyzed: 03/11/16
Dichlorodifluoromethane ug/L34.2 1.0 20.00 20 LH60-140171 2
Ethanol ug/L561200 500.0 2060-140112 3
Ethylbenzene ug/L21.1 0.50 20.00 2070-130105 1
Hexachlorobutadiene ug/L19.8 2.0 20.00 2070-13099 7
Isopropyl Ether ug/L22.0 0.50 20.00 2070-130110 1
Isopropylbenzene (Cumene)ug/L20.8 0.50 20.00 2070-130104 2
m,p-Xylenes ug/L42.4 1.0 40.00 2070-130106 2
Methyl Butyl Ketone (2-Hexanone)ug/L19.3 1.0 20.00 2060-14096 2
Methyl Ethyl Ketone (2-Butanone)ug/L19.6 5.0 20.00 2060-14098 3
Methyl Isobutyl Ketone ug/L20.0 1.0 20.00 2060-140100 2
Methylene Chloride ug/L20.8 2.0 20.00 2070-130104 0.4
Methyl-tert-Butyl Ether ug/L21.8 1.0 20.00 2070-130109 0.4
Naphthalene ug/L18.9 1.0 20.00 2070-13094 0.4
n-Butylbenzene ug/L20.5 0.50 20.00 2070-130103 3
n-Propylbenzene ug/L20.4 0.50 20.00 2070-130102 3
o-Xylene ug/L21.1 0.50 20.00 2070-130106 0.5
sec-Butylbenzene ug/L21.0 0.50 20.00 2070-130105 2
Styrene ug/L21.1 0.50 20.00 2070-130106 1
tert-Butylbenzene ug/L20.6 0.50 20.00 2070-130103 2
Tetrachloroethylene ug/L21.4 0.50 20.00 2070-130107 1
Toluene ug/L21.5 0.50 20.00 2070-130108 2
trans-1,2-Dichloroethylene ug/L21.9 0.50 20.00 2070-130109 4
trans-1,3-Dichloropropylene ug/L19.6 0.50 20.00 2070-13098 0.2
Trichloroethylene ug/L19.9 0.50 20.00 2070-130100 0.7
Trichlorofluoromethane ug/L22.5 0.50 20.00 2060-140113 3
Vinyl acetate ug/L29.2 5.0 20.00 20 L260-140146 5
Vinyl chloride ug/L27.1 0.50 20.00 2060-140135 3
Xylenes, total ug/L63.5 1.5 60.00 2070-130106 0.9
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9849.0
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9949.6
ug/L 50.00 70-130Surrogate: Toluene-d8 9848.8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 48 of 56
3/15/16
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 6030100
Time Submitted: 3/4/2016 2:30:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6C0240 - SM6200 B
Blank (P6C0240-BLK1)Prepared & Analyzed: 03/14/16
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL0.50
1,2,4-Trichlorobenzene ug/LBRL0.50
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL10
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL0.50
Bromomethane ug/LBRL1.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethanol ug/LBRL200
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 49 of 56
3/15/16
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 6030100
Time Submitted: 3/4/2016 2:30:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6C0240 - SM6200 B
Blank (P6C0240-BLK1)Prepared & Analyzed: 03/14/16
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL1.0
Methylene Chloride ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL1.0
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL0.50
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Butylbenzene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL5.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10150.5
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10150.4
ug/L 50.00 70-130Surrogate: Toluene-d8 9447.2
LCS (P6C0240-BS1)Prepared & Analyzed: 03/14/16
1,1,1,2-Tetrachloroethane ug/L20.0 0.50 20.00 70-130100
1,1,1-Trichloroethane ug/L21.0 0.50 20.00 70-130105
1,1,2,2-Tetrachloroethane ug/L20.7 0.50 20.00 70-130103
1,1,2-Trichloroethane ug/L23.4 0.50 20.00 70-130117
1,1-Dichloroethane ug/L22.7 0.50 20.00 70-130114
1,1-Dichloroethylene ug/L24.3 0.50 20.00 70-130122
1,1-Dichloropropylene ug/L21.3 0.50 20.00 70-130107
1,2,3-Trichlorobenzene ug/L20.8 0.50 20.00 70-130104
1,2,3-Trichloropropane ug/L18.7 0.50 20.00 70-13093
1,2,4-Trichlorobenzene ug/L21.2 0.50 20.00 70-130106
1,2,4-Trimethylbenzene ug/L21.5 0.50 20.00 70-130108
1,2-Dibromo-3-chloropropane ug/L19.9 2.0 20.00 70-13099
1,2-Dibromoethane ug/L19.4 0.50 20.00 70-13097
1,2-Dichlorobenzene ug/L20.5 0.50 20.00 70-130102
1,2-Dichloroethane ug/L23.2 0.50 20.00 70-130116
1,2-Dichloropropane ug/L21.4 0.50 20.00 70-130107
1,3,5-Trimethylbenzene ug/L21.9 0.50 20.00 70-130110
1,3-Dichlorobenzene ug/L20.9 0.50 20.00 70-130104
1,3-Dichloropropane ug/L21.5 0.50 20.00 70-130108
1,4-Dichlorobenzene ug/L20.6 0.50 20.00 70-130103
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 50 of 56
3/15/16
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 6030100
Time Submitted: 3/4/2016 2:30:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6C0240 - SM6200 B
LCS (P6C0240-BS1)Prepared & Analyzed: 03/14/16
2,2-Dichloropropane ug/L27.5 2.0 20.00 LH70-130138
2-Chlorotoluene ug/L21.4 0.50 20.00 70-130107
4-Chlorotoluene ug/L21.2 0.50 20.00 70-130106
4-Isopropyltoluene ug/L21.7 0.50 20.00 70-130108
Acetone ug/L45.0 10 40.00 40-160113
Benzene ug/L23.5 0.50 20.00 70-130117
Bromobenzene ug/L21.0 0.50 20.00 70-130105
Bromochloromethane ug/L21.0 0.50 20.00 70-130105
Bromodichloromethane ug/L21.8 0.50 20.00 70-130109
Bromoform ug/L19.1 0.50 20.00 70-13095
Bromomethane ug/L24.8 1.0 20.00 60-140124
Carbon Tetrachloride ug/L21.3 0.50 20.00 70-130106
Chlorobenzene ug/L21.2 0.50 20.00 70-130106
Chloroethane ug/L24.4 0.50 20.00 60-140122
Chloroform ug/L21.8 0.50 20.00 70-130109
Chloromethane ug/L29.6 0.50 20.00 60-140148
cis-1,2-Dichloroethylene ug/L21.8 0.50 20.00 70-130109
cis-1,3-Dichloropropylene ug/L21.3 0.50 20.00 70-130107
Dibromochloromethane ug/L19.8 0.50 20.00 70-13099
Dibromomethane ug/L21.2 0.50 20.00 70-130106
Dichlorodifluoromethane ug/L35.8 1.0 20.00 LH60-140179
Ethanol ug/L555200 500.0 60-140111
Ethylbenzene ug/L22.3 0.50 20.00 70-130111
Hexachlorobutadiene ug/L21.6 2.0 20.00 70-130108
Isopropyl Ether ug/L24.2 0.50 20.00 70-130121
Isopropylbenzene (Cumene)ug/L21.9 0.50 20.00 70-130110
m,p-Xylenes ug/L44.6 1.0 40.00 70-130111
Methyl Butyl Ketone (2-Hexanone)ug/L20.8 1.0 20.00 60-140104
Methyl Ethyl Ketone (2-Butanone)ug/L22.1 5.0 20.00 60-140111
Methyl Isobutyl Ketone ug/L22.2 1.0 20.00 60-140111
Methylene Chloride ug/L21.7 2.0 20.00 70-130108
Methyl-tert-Butyl Ether ug/L24.1 1.0 20.00 70-130121
Naphthalene ug/L19.6 1.0 20.00 70-13098
n-Butylbenzene ug/L21.8 0.50 20.00 70-130109
n-Propylbenzene ug/L21.7 0.50 20.00 70-130108
o-Xylene ug/L22.0 0.50 20.00 70-130110
sec-Butylbenzene ug/L22.1 0.50 20.00 70-130110
Styrene ug/L22.2 0.50 20.00 70-130111
tert-Butylbenzene ug/L21.8 0.50 20.00 70-130109
Tetrachloroethylene ug/L22.2 0.50 20.00 70-130111
Toluene ug/L23.5 0.50 20.00 70-130117
trans-1,2-Dichloroethylene ug/L23.7 0.50 20.00 70-130119
trans-1,3-Dichloropropylene ug/L21.2 0.50 20.00 70-130106
Trichloroethylene ug/L21.3 0.50 20.00 70-130107
Trichlorofluoromethane ug/L23.4 0.50 20.00 60-140117
Vinyl acetate ug/L30.3 5.0 20.00 LH60-140151
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 51 of 56
3/15/16
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 6030100
Time Submitted: 3/4/2016 2:30:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6C0240 - SM6200 B
LCS (P6C0240-BS1)Prepared & Analyzed: 03/14/16
Vinyl chloride ug/L28.4 0.50 20.00 L160-140142
Xylenes, total ug/L66.6 1.5 60.00 70-130111
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9949.6
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9848.9
ug/L 50.00 70-130Surrogate: Toluene-d8 9447.0
LCS Dup (P6C0240-BSD1)Prepared & Analyzed: 03/14/16
1,1,1,2-Tetrachloroethane ug/L19.5 0.50 20.00 2070-13098 3
1,1,1-Trichloroethane ug/L21.6 0.50 20.00 2070-130108 3
1,1,2,2-Tetrachloroethane ug/L20.6 0.50 20.00 2070-130103 0.7
1,1,2-Trichloroethane ug/L23.0 0.50 20.00 2070-130115 2
1,1-Dichloroethane ug/L21.9 0.50 20.00 2070-130109 4
1,1-Dichloroethylene ug/L23.8 0.50 20.00 2070-130119 2
1,1-Dichloropropylene ug/L21.5 0.50 20.00 2070-130108 0.8
1,2,3-Trichlorobenzene ug/L20.3 0.50 20.00 2070-130101 2
1,2,3-Trichloropropane ug/L18.7 0.50 20.00 2070-13093 0.1
1,2,4-Trichlorobenzene ug/L20.5 0.50 20.00 2070-130103 3
1,2,4-Trimethylbenzene ug/L21.3 0.50 20.00 2070-130106 1
1,2-Dibromo-3-chloropropane ug/L20.1 2.0 20.00 2070-130100 0.9
1,2-Dibromoethane ug/L19.3 0.50 20.00 2070-13096 0.4
1,2-Dichlorobenzene ug/L20.4 0.50 20.00 2070-130102 0.3
1,2-Dichloroethane ug/L22.8 0.50 20.00 2070-130114 1
1,2-Dichloropropane ug/L21.0 0.50 20.00 2070-130105 2
1,3,5-Trimethylbenzene ug/L21.7 0.50 20.00 2070-130108 1
1,3-Dichlorobenzene ug/L20.5 0.50 20.00 2070-130102 2
1,3-Dichloropropane ug/L21.0 0.50 20.00 2070-130105 2
1,4-Dichlorobenzene ug/L20.3 0.50 20.00 2070-130101 2
2,2-Dichloropropane ug/L26.4 2.0 20.00 20 LH70-130132 4
2-Chlorotoluene ug/L21.2 0.50 20.00 2070-130106 0.7
4-Chlorotoluene ug/L20.9 0.50 20.00 2070-130105 1
4-Isopropyltoluene ug/L21.4 0.50 20.00 2070-130107 1
Acetone ug/L43.7 10 40.00 2040-160109 3
Benzene ug/L23.0 0.50 20.00 2070-130115 2
Bromobenzene ug/L21.0 0.50 20.00 2070-130105 0.05
Bromochloromethane ug/L21.0 0.50 20.00 2070-130105 0.1
Bromodichloromethane ug/L21.4 0.50 20.00 2070-130107 2
Bromoform ug/L18.7 0.50 20.00 2070-13093 2
Bromomethane ug/L25.2 1.0 20.00 2060-140126 2
Carbon Tetrachloride ug/L21.1 0.50 20.00 2070-130105 0.9
Chlorobenzene ug/L21.3 0.50 20.00 2070-130107 0.3
Chloroethane ug/L23.8 0.50 20.00 2060-140119 2
Chloroform ug/L21.4 0.50 20.00 2070-130107 2
Chloromethane ug/L29.5 0.50 20.00 2060-140147 0.3
cis-1,2-Dichloroethylene ug/L21.4 0.50 20.00 2070-130107 2
cis-1,3-Dichloropropylene ug/L21.5 0.50 20.00 2070-130108 0.8
Dibromochloromethane ug/L19.0 0.50 20.00 2070-13095 4
Dibromomethane ug/L20.7 0.50 20.00 2070-130104 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 52 of 56
3/15/16
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 6030100
Time Submitted: 3/4/2016 2:30:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6C0240 - SM6200 B
LCS Dup (P6C0240-BSD1)Prepared & Analyzed: 03/14/16
Dichlorodifluoromethane ug/L36.4 1.0 20.00 20 LH60-140182 1
Ethanol ug/L528200 500.0 2060-140106 5
Ethylbenzene ug/L21.6 0.50 20.00 2070-130108 3
Hexachlorobutadiene ug/L22.1 2.0 20.00 2070-130110 2
Isopropyl Ether ug/L23.4 0.50 20.00 2070-130117 4
Isopropylbenzene (Cumene)ug/L21.7 0.50 20.00 2070-130108 1
m,p-Xylenes ug/L43.8 1.0 40.00 2070-130110 2
Methyl Butyl Ketone (2-Hexanone)ug/L20.2 1.0 20.00 2060-140101 3
Methyl Ethyl Ketone (2-Butanone)ug/L21.5 5.0 20.00 2060-140107 3
Methyl Isobutyl Ketone ug/L21.5 1.0 20.00 2060-140108 3
Methylene Chloride ug/L21.0 2.0 20.00 2070-130105 3
Methyl-tert-Butyl Ether ug/L23.6 1.0 20.00 2070-130118 2
Naphthalene ug/L19.4 1.0 20.00 2070-13097 1
n-Butylbenzene ug/L21.7 0.50 20.00 2070-130108 0.6
n-Propylbenzene ug/L21.6 0.50 20.00 2070-130108 0.4
o-Xylene ug/L21.5 0.50 20.00 2070-130107 2
sec-Butylbenzene ug/L22.1 0.50 20.00 2070-130111 0.09
Styrene ug/L21.9 0.50 20.00 2070-130109 2
tert-Butylbenzene ug/L21.7 0.50 20.00 2070-130109 0.3
Tetrachloroethylene ug/L22.2 0.50 20.00 2070-130111 0.2
Toluene ug/L23.0 0.50 20.00 2070-130115 2
trans-1,2-Dichloroethylene ug/L22.8 0.50 20.00 2070-130114 4
trans-1,3-Dichloropropylene ug/L21.3 0.50 20.00 2070-130107 0.4
Trichloroethylene ug/L20.7 0.50 20.00 2070-130104 3
Trichlorofluoromethane ug/L22.8 0.50 20.00 2060-140114 3
Vinyl acetate ug/L28.4 5.0 20.00 20 LH60-140142 6
Vinyl chloride ug/L27.2 0.50 20.00 2060-140136 4
Xylenes, total ug/L65.3 1.5 60.00 2070-130109 2
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10150.5
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9748.4
ug/L 50.00 70-130Surrogate: Toluene-d8 9547.3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 53 of 56
Sample Extraction Data
Prep Method: SM6200 B
Lab Number Batch Date/TimeInitialFinal
P6C02126030100-01 03/11/16 9:191010mLmL
P6C02126030100-02 03/11/16 9:191010mLmL
P6C02126030100-03 03/11/16 9:191010mLmL
P6C02126030100-04 03/11/16 9:191010mLmL
P6C02126030100-05 03/11/16 9:191010mLmL
P6C02126030100-06 03/11/16 9:191010mLmL
P6C02126030100-07 03/11/16 9:191010mLmL
P6C02126030100-08 03/11/16 9:191010mLmL
P6C02126030100-09 03/11/16 9:191010mLmL
P6C02126030100-10 03/11/16 9:191010mLmL
P6C02126030100-11 03/11/16 9:191010mLmL
P6C02126030100-12 03/11/16 9:191010mLmL
P6C02126030100-13 03/11/16 9:191010mLmL
P6C02126030100-14 03/11/16 9:191010mLmL
P6C02126030100-15 03/11/16 9:191010mLmL
P6C02126030100-16 03/11/16 9:191010mLmL
P6C02406030100-17 03/14/16 8:261010mLmL
P6C02406030100-18 03/14/16 8:261010mLmL
P6C02406030100-19 03/14/16 8:261010mLmL
P6C02406030100-20 03/14/16 8:261010mLmL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 54 of 56
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APPENDIX B

503 Industrial Ave • Greensboro, NC 27406 Phone [phone] • Fax [phone] • Toll Free [phone] Email: [e-mail]
April 20, 2016 James McMillan Sent Via email: [e-mail] RE: Supply Well Analytical Results 2765 Union Ridge Road, Burlington, NC NCDEQ Incident #12913 Former Harold Smith Grocery Pyramid Project 2016-004 Dear Mr. McMillan:
As directed by the NCDENR and T.A.C., Inc., Pyramid Environmental has continued to collect samples from the Point-of-Entry (POE) treatment system that is connected to your water supply well. The work is being performed as part of the ongoing assessment of the referenced underground storage tank release. The results of the water analyses are presented below. On February 29, 2016, Pyramid collected influent, midfluent, and effluent samples from the POE connected to your supply well. The samples are designated as SW2765 INF, SW2765 MID, and SW2765 EFF. The groundwater samples were analyzed at a State certified laboratory and the results are attached for your review. The laboratory results indicate that the POE influent (untreated water) contained methyl tert-butyl ether (MTBE) at a concentration of 60 parts per billion (PPB). The current North Carolina drinking water standard for MTBE is 20 PPB. The compound 1,2-dichloroethane was detected at 9.2
PPB. The current North Carolina drinking water standard for 1,2-dichloroethane is 0.4 PPB. The compound isopropyl ether was detected at 76 PPB. The current North Carolina drinking water standard for isopropyl ether is 70 PPB. No other targeted compounds were detected at concentrations that exceeded
the laboratory detection limits in the POE influent. The laboratory results of the POE effluent sample (treated water) collected on February 29, 2016 indicate
that none of the targeted petroleum compounds were detected at concentrations that exceed the laboratory detection limits. The POE worked to remove petroleum contaminants prior to water use. Maintenance of the POE treatment system will continue to be performed on a quarterly basis. If you have any questions, please call Pyramid at [phone]. Thank you for your cooperation with this project. Sincerely,
Brett S. Higgins Project Manager
Attachments – Laboratory Report

APPENDIX C

Summary of System Installation, Start-up, and Operation Activities
Harold Smith Remediation System
January - March 2016

January 27, 2016 System was not operational at arrival. The technician checked the system and restarted. The technician performed regular operational and maintenance tasks on the system. The technician then recorded system operations data and measurements. System was operational at departure.
February 16, 2016 System was not operational at arrival. The technician checked the system and attempted to restart. The system would not restart due to a damaged electric drive motor. The technician performed other regular operational and maintenance tasks on the system. The technician then recorded system
operations data and measurements. System was not operational at departure. March 23, 2016 System was not operational at arrival. The system was down due to a
damaged electric drive motor. The work to replace the motor is scheduled
for April 2016. The technician performed other regular operational and maintenance tasks on the system. The technician then recorded system operations data and measurements. System was not operational at departure.

APPENDIX D

#=CL#
April 26, 2016
LIMS USE: FR - BRETT HIGGINS
LIMS OBJECT ID: 92294913
92294913
Project:
Pace Project No.:
RE:
Mr. Brett Higgins
Pyramid Environmental
P.O. Box 16265
503 Industrial Avenue
Greensboro, NC 27416
HAROLD SMITH
Dear Mr. Higgins:
Enclosed are the analytical results for sample(s) received by the laboratory on April 22, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 14
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92294913
HAROLD SMITH
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 14
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92294913
HAROLD SMITH
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92294913001 SW 2773 SM 6200B 63 PASI-CNB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 14
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92294913
HAROLD SMITH
Sample:SW 2773 Lab ID:92294913001 Collected:04/20/16 10:00 Received:04/22/16 10:57 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 04/26/16 02:57 71-43-20.50 1
Bromobenzene ND ug/L 04/26/16 02:57 108-86-10.50 1
Bromochloromethane ND ug/L 04/26/16 02:57 74-97-50.50 1
Bromodichloromethane ND ug/L 04/26/16 02:57 75-27-40.50 1
Bromoform ND ug/L 04/26/16 02:57 75-25-20.50 1
Bromomethane ND ug/L 04/26/16 02:57 74-83-95.0 1
n-Butylbenzene ND ug/L 04/26/16 02:57 104-51-80.50 1
sec-Butylbenzene ND ug/L 04/26/16 02:57 135-98-80.50 1
tert-Butylbenzene ND ug/L 04/26/16 02:57 98-06-60.50 1
Carbon tetrachloride ND ug/L 04/26/16 02:57 56-23-50.50 1
Chlorobenzene ND ug/L 04/26/16 02:57 108-90-70.50 1
Chloroethane ND ug/L 04/26/16 02:57 75-00-31.0 1
Chloroform ND ug/L 04/26/16 02:57 67-66-30.50 1
Chloromethane ND ug/L 04/26/16 02:57 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/26/16 02:57 95-49-80.50 1
4-Chlorotoluene ND ug/L 04/26/16 02:57 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 04/26/16 02:57 96-12-81.0 1
Dibromochloromethane ND ug/L 04/26/16 02:57 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 04/26/16 02:57 106-93-40.50 1
Dibromomethane ND ug/L 04/26/16 02:57 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 04/26/16 02:57 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 04/26/16 02:57 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 04/26/16 02:57 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 04/26/16 02:57 75-71-80.50 1
1,1-Dichloroethane ND ug/L 04/26/16 02:57 75-34-30.50 1
1,2-Dichloroethane 1.2 ug/L 04/26/16 02:57 107-06-20.50 1
1,1-Dichloroethene ND ug/L 04/26/16 02:57 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 04/26/16 02:57 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 04/26/16 02:57 156-60-50.50 1
1,2-Dichloropropane ND ug/L 04/26/16 02:57 78-87-50.50 1
1,3-Dichloropropane ND ug/L 04/26/16 02:57 142-28-90.50 1
2,2-Dichloropropane ND ug/L 04/26/16 02:57 594-20-70.50 1
1,1-Dichloropropene ND ug/L 04/26/16 02:57 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 04/26/16 02:57 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 04/26/16 02:57 10061-02-60.50 1
Diisopropyl ether 8.2 ug/L 04/26/16 02:57 108-20-30.50 1
Ethylbenzene ND ug/L 04/26/16 02:57 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 04/26/16 02:57 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 04/26/16 02:57 98-82-80.50 1
Methylene Chloride ND ug/L 04/26/16 02:57 75-09-22.0 1
Methyl-tert-butyl ether 5.9 ug/L 04/26/16 02:57 1634-04-40.50 1
Naphthalene ND ug/L 04/26/16 02:57 91-20-32.0 1
n-Propylbenzene ND ug/L 04/26/16 02:57 103-65-10.50 1
Styrene ND ug/L 04/26/16 02:57 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 04/26/16 02:57 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 04/26/16 02:57 79-34-50.50 1
Tetrachloroethene ND ug/L 04/26/16 02:57 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/26/2016 02:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 14
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92294913
HAROLD SMITH
Sample:SW 2773 Lab ID:92294913001 Collected:04/20/16 10:00 Received:04/22/16 10:57 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 04/26/16 02:57 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 04/26/16 02:57 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 04/26/16 02:57 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 04/26/16 02:57 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 04/26/16 02:57 79-00-50.50 1
Trichloroethene ND ug/L 04/26/16 02:57 79-01-60.50 1
Trichlorofluoromethane ND ug/L 04/26/16 02:57 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/26/16 02:57 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 04/26/16 02:57 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 04/26/16 02:57 108-67-80.50 1
Vinyl chloride ND ug/L 04/26/16 02:57 75-01-41.0 1
m&p-Xylene ND ug/L 04/26/16 02:57 179601-23-11.0 1
o-Xylene ND ug/L 04/26/16 02:57 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %04/26/16 02:57 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %04/26/16 02:57 460-00-470-130 1
Toluene-d8 (S)99 %04/26/16 02:57 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/26/2016 02:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 14
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92294913
HAROLD SMITH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/36560
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92294913001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1719026
Associated Lab Samples:92294913001
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 04/25/16 23:49
1,1,1-Trichloroethane ug/L ND 0.50 04/25/16 23:49
1,1,2,2-Tetrachloroethane ug/L ND 0.50 04/25/16 23:49
1,1,2-Trichloroethane ug/L ND 0.50 04/25/16 23:49
1,1-Dichloroethane ug/L ND 0.50 04/25/16 23:49
1,1-Dichloroethene ug/L ND 0.50 04/25/16 23:49
1,1-Dichloropropene ug/L ND 0.50 04/25/16 23:49
1,2,3-Trichlorobenzene ug/L ND 2.0 04/25/16 23:49
1,2,3-Trichloropropane ug/L ND 0.50 04/25/16 23:49
1,2,4-Trichlorobenzene ug/L ND 2.0 04/25/16 23:49
1,2,4-Trimethylbenzene ug/L ND 0.50 04/25/16 23:49
1,2-Dibromo-3-chloropropane ug/L ND 1.0 04/25/16 23:49
1,2-Dibromoethane (EDB)ug/L ND 0.50 04/25/16 23:49
1,2-Dichlorobenzene ug/L ND 0.50 04/25/16 23:49
1,2-Dichloroethane ug/L ND 0.50 04/25/16 23:49
1,2-Dichloropropane ug/L ND 0.50 04/25/16 23:49
1,3,5-Trimethylbenzene ug/L ND 0.50 04/25/16 23:49
1,3-Dichlorobenzene ug/L ND 0.50 04/25/16 23:49
1,3-Dichloropropane ug/L ND 0.50 04/25/16 23:49
1,4-Dichlorobenzene ug/L ND 0.50 04/25/16 23:49
2,2-Dichloropropane ug/L ND 0.50 04/25/16 23:49
2-Chlorotoluene ug/L ND 0.50 04/25/16 23:49
4-Chlorotoluene ug/L ND 0.50 04/25/16 23:49
Benzene ug/L ND 0.50 04/25/16 23:49
Bromobenzene ug/L ND 0.50 04/25/16 23:49
Bromochloromethane ug/L ND 0.50 04/25/16 23:49
Bromodichloromethane ug/L ND 0.50 04/25/16 23:49
Bromoform ug/L ND 0.50 04/25/16 23:49
Bromomethane ug/L ND 5.0 04/25/16 23:49
Carbon tetrachloride ug/L ND 0.50 04/25/16 23:49
Chlorobenzene ug/L ND 0.50 04/25/16 23:49
Chloroethane ug/L ND 1.0 04/25/16 23:49
Chloroform ug/L ND 0.50 04/25/16 23:49
Chloromethane ug/L ND 1.0 04/25/16 23:49
cis-1,2-Dichloroethene ug/L ND 0.50 04/25/16 23:49
cis-1,3-Dichloropropene ug/L ND 0.50 04/25/16 23:49
Dibromochloromethane ug/L ND 0.50 04/25/16 23:49
Dibromomethane ug/L ND 0.50 04/25/16 23:49
Dichlorodifluoromethane ug/L ND 0.50 04/25/16 23:49
Diisopropyl ether ug/L ND 0.50 04/25/16 23:49
Ethylbenzene ug/L ND 0.50 04/25/16 23:49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/26/2016 02:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 14
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92294913
HAROLD SMITH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1719026
Associated Lab Samples:92294913001
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 04/25/16 23:49
Isopropylbenzene (Cumene)ug/L ND 0.50 04/25/16 23:49
m&p-Xylene ug/L ND 1.0 04/25/16 23:49
Methyl-tert-butyl ether ug/L ND 0.50 04/25/16 23:49
Methylene Chloride ug/L ND 2.0 04/25/16 23:49
n-Butylbenzene ug/L ND 0.50 04/25/16 23:49
n-Propylbenzene ug/L ND 0.50 04/25/16 23:49
Naphthalene ug/L ND 2.0 04/25/16 23:49
o-Xylene ug/L ND 0.50 04/25/16 23:49
sec-Butylbenzene ug/L ND 0.50 04/25/16 23:49
Styrene ug/L ND 0.50 04/25/16 23:49
tert-Butylbenzene ug/L ND 0.50 04/25/16 23:49
Tetrachloroethene ug/L ND 0.50 04/25/16 23:49
Toluene ug/L ND 0.50 04/25/16 23:49
trans-1,2-Dichloroethene ug/L ND 0.50 04/25/16 23:49
trans-1,3-Dichloropropene ug/L ND 0.50 04/25/16 23:49
Trichloroethene ug/L ND 0.50 04/25/16 23:49
Trichlorofluoromethane ug/L ND 1.0 04/25/16 23:49
Vinyl chloride ug/L ND 1.0 04/25/16 23:49
1,2-Dichloroethane-d4 (S)%100 70-130 04/25/16 23:49
4-Bromofluorobenzene (S)%99 70-130 04/25/16 23:49
Toluene-d8 (S)%100 70-130 04/25/16 23:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1719027LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 54.650 109 60-140
1,1,1-Trichloroethane ug/L 54.650 109 60-140
1,1,2,2-Tetrachloroethane ug/L 54.350 109 60-140
1,1,2-Trichloroethane ug/L 55.150 110 60-140
1,1-Dichloroethane ug/L 54.850 110 60-140
1,1-Dichloroethene ug/L 58.250 116 60-140
1,1-Dichloropropene ug/L 54.550 109 60-140
1,2,3-Trichlorobenzene ug/L 60.350 121 60-140
1,2,3-Trichloropropane ug/L 55.750 111 60-140
1,2,4-Trichlorobenzene ug/L 58.250 116 60-140
1,2,4-Trimethylbenzene ug/L 53.750 107 60-140
1,2-Dibromo-3-chloropropane ug/L 52.950 106 60-140
1,2-Dibromoethane (EDB)ug/L 57.050 114 60-140
1,2-Dichlorobenzene ug/L 54.950 110 60-140
1,2-Dichloroethane ug/L 47.850 96 60-140
1,2-Dichloropropane ug/L 55.250 110 60-140
1,3,5-Trimethylbenzene ug/L 53.650 107 60-140
1,3-Dichlorobenzene ug/L 57.550 115 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/26/2016 02:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 14
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92294913
HAROLD SMITH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1719027LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 52.650 105 60-140
1,4-Dichlorobenzene ug/L 51.250 102 60-140
2,2-Dichloropropane ug/L 54.450 109 60-140
2-Chlorotoluene ug/L 54.350 109 60-140
4-Chlorotoluene ug/L 52.550 105 60-140
Benzene ug/L 54.350 109 60-140
Bromobenzene ug/L 52.350 105 60-140
Bromochloromethane ug/L 61.550 123 60-140
Bromodichloromethane ug/L 57.550 115 60-140
Bromoform ug/L 54.750 109 60-140
Bromomethane ug/L 51.950 104 60-140
Carbon tetrachloride ug/L 56.150 112 60-140
Chlorobenzene ug/L 54.550 109 60-140
Chloroethane ug/L 57.850 116 60-140
Chloroform ug/L 53.850 108 60-140
Chloromethane ug/L 40.750 81 60-140
cis-1,2-Dichloroethene ug/L 54.050 108 60-140
cis-1,3-Dichloropropene ug/L 55.850 112 60-140
Dibromochloromethane ug/L 57.950 116 60-140
Dibromomethane ug/L 55.950 112 60-140
Dichlorodifluoromethane ug/L 53.950 108 60-140
Diisopropyl ether ug/L 54.750 109 60-140
Ethylbenzene ug/L 53.850 108 60-140
Hexachloro-1,3-butadiene ug/L 58.250 116 60-140
Isopropylbenzene (Cumene)ug/L 53.450 107 60-140
m&p-Xylene ug/L 107100 107 60-140
Methyl-tert-butyl ether ug/L 54.850 110 60-140
Methylene Chloride ug/L 55.350 111 60-140
n-Butylbenzene ug/L 56.550 113 60-140
n-Propylbenzene ug/L 50.950 102 60-140
Naphthalene ug/L 58.850 118 60-140
o-Xylene ug/L 52.650 105 60-140
sec-Butylbenzene ug/L 52.650 105 60-140
Styrene ug/L 55.050 110 60-140
tert-Butylbenzene ug/L 44.050 88 60-140
Tetrachloroethene ug/L 51.950 104 60-140
Toluene ug/L 55.450 111 60-140
trans-1,2-Dichloroethene ug/L 54.450 109 60-140
trans-1,3-Dichloropropene ug/L 55.650 111 60-140
Trichloroethene ug/L 53.950 108 60-140
Trichlorofluoromethane ug/L 60.450 121 60-140
Vinyl chloride ug/L 63.350 127 60-140
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/26/2016 02:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 14
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92294913
HAROLD SMITH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1719028MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92294940001
1719029
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 102 60-140106 420ND20.4 21.1
1,1,1-Trichloroethane ug/L 20 113 60-140114 120ND22.6 22.8
1,1,2,2-Tetrachloroethane ug/L 20 102 60-140103 120ND20.4 20.6
1,1,2-Trichloroethane ug/L 20 109 60-140114 420ND21.9 22.8
1,1-Dichloroethane ug/L 20 109 60-140110 120ND21.9 22.1
1,1-Dichloroethene ug/L 20 118 60-140120 220ND23.5 23.9
1,1-Dichloropropene ug/L 20 114 60-140117 220ND22.9 23.4
1,2,3-Trichlorobenzene ug/L 20 103 60-140104 120ND20.5 20.8
1,2,3-Trichloropropane ug/L 20 103 60-140100 320ND20.5 20.0
1,2,4-Trichlorobenzene ug/L 20 98 60-14099 120ND19.5 19.7
1,2,4-Trimethylbenzene ug/L 20 104 60-140108 320ND20.8 21.5
1,2-Dibromo-3-chloropropane ug/L 20 98 60-140102 320ND19.7 20.3
1,2-Dibromoethane (EDB)ug/L 20 108 60-140112 320ND21.6 22.4
1,2-Dichlorobenzene ug/L 20 106 60-140106 120ND21.1 21.2
1,2-Dichloroethane ug/L 20 95 60-14097 220ND19.0 19.4
1,2-Dichloropropane ug/L 20 109 60-140116 620ND21.9 23.1
1,3,5-Trimethylbenzene ug/L 20 105 60-140109 420ND21.0 21.9
1,3-Dichlorobenzene ug/L 20 109 60-140112 320ND21.8 22.4
1,3-Dichloropropane ug/L 20 99 60-140103 420ND19.8 20.6
1,4-Dichlorobenzene ug/L 20 99 60-140101 220ND19.9 20.2
2,2-Dichloropropane ug/L 20 100 60-140104 420ND19.9 20.7
2-Chlorotoluene ug/L 20 109 60-140112 220ND21.8 22.4
4-Chlorotoluene ug/L 20 102 60-140109 720ND20.3 21.9
Benzene ug/L 20 112 60-140113 120ND22.4 22.5
Bromobenzene ug/L 20 105 60-140108 320ND21.1 21.6
Bromochloromethane ug/L 20 115 60-140115 020ND23.0 23.1
Bromodichloromethane ug/L 20 110 60-140110 020ND22.0 22.1
Bromoform ug/L 20 101 60-140104 320ND20.2 20.8
Bromomethane ug/L M1205260-14071 3020ND10.5 14.2
Carbon tetrachloride ug/L 20 117 60-140120 320ND23.3 24.0
Chlorobenzene ug/L 20 102 60-140105 220ND20.4 20.9
Chloroethane ug/L 20 116 60-140123 620ND23.1 24.5
Chloroform ug/L 20 106 60-140112 620ND21.1 22.4
Chloromethane ug/L 20 92 60-14095 320ND18.3 18.9
cis-1,2-Dichloroethene ug/L 20 110 60-140114 420ND22.0 22.8
cis-1,3-Dichloropropene ug/L 20 105 60-140111 620ND21.0 22.2
Dibromochloromethane ug/L 20 106 60-140108 220ND21.1 21.6
Dibromomethane ug/L 20 108 60-140111 320ND21.6 22.2
Dichlorodifluoromethane ug/L 20 107 60-140108 120ND21.3 21.6
Diisopropyl ether ug/L 20 108 60-140112 420ND21.8 22.6
Ethylbenzene ug/L 20 104 60-140106 220ND20.7 21.1
Hexachloro-1,3-butadiene ug/L 20 88 60-14099 1220ND17.5 19.8
Isopropylbenzene (Cumene)ug/L 20 102 60-140102 020ND20.4 20.5
m&p-Xylene ug/L 40 102 60-140104 240ND40.9 41.8
Methyl-tert-butyl ether ug/L 20 109 60-140110 120ND21.7 22.0
Methylene Chloride ug/L 20 110 60-140110 120ND22.0 21.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/26/2016 02:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 14
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92294913
HAROLD SMITH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1719028MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92294940001
1719029
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 101 60-140102 120ND20.2 20.4
n-Propylbenzene ug/L 20 104 60-140104 020ND20.7 20.7
Naphthalene ug/L 20 101 60-140104 320ND20.2 20.8
o-Xylene ug/L 20 102 60-140101 120ND20.4 20.1
sec-Butylbenzene ug/L 20 103 60-140106 320ND20.6 21.2
Styrene ug/L 20 100 60-140101 120ND20.0 20.2
tert-Butylbenzene ug/L 20 91 60-14092 120ND18.2 18.3
Tetrachloroethene ug/L 20 99 60-140102 320ND19.9 20.5
Toluene ug/L 20 111 60-140112 020ND22.3 22.3
trans-1,2-Dichloroethene ug/L 20 109 60-140112 320ND21.8 22.4
trans-1,3-Dichloropropene ug/L 20 102 60-140104 220ND20.4 20.7
Trichloroethene ug/L 20 107 60-140111 420ND21.4 22.3
Trichlorofluoromethane ug/L 20 126 60-140126 020ND25.3 25.3
Vinyl chloride ug/L 20 127 60-140125 220ND25.4 25.0
1,2-Dichloroethane-d4 (S)%97 70-13096
4-Bromofluorobenzene (S)%98 70-13096
Toluene-d8 (S)%102 70-130102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/26/2016 02:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 14
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92294913
HAROLD SMITH
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/26/2016 02:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 14
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92294913
HAROLD SMITH
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92294913001 MSV/36560SW 2773 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/26/2016 02:51 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 14
Page 13 of 14
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