WS-3891_12913_CA_RMR_20160111

TABLE OF CONTENTS

ACRONYMS ............................................................................................... III
1.0 INTRODUCTION .............................................................................. 1
1.1 SITE INFORMATION ................................................................................................... 1
1.2 ADJOINING PROPERTIES AND POTENTIAL RECEPTORS .............................................. 1
1.3 SITE HYDROLOGY & GEOLOGY ................................................................................ 2
1.4 PREVIOUS REPORTS ................................................................................................. 2
2.0 GROUNDWATER SAMPLING ....................................................... 3
2.1 MONITORING WELL SAMPLING ................................................................................ 3
2.2 POTABLE WATER SUPPLY WELL SAMPLING............................................................. 3
3.0 TREATMENT SYSTEM OPERATIONAL STATUS ................... 4
3.1 SYSTEM OPERATIONS ............................................................................................... 4
3.2 CONTAMINATED SOIL REMOVAL .............................................................................. 5
3.3 SYSTEM UPDATE ...................................................................................................... 6
4.0 SOIL & GROUNDWATER ASSESSMENT ................................... 6
4.1 GROUNDWATER ANALYTICAL RESULTS ................................................................... 6
4.2 SUPPLY WELL ANALYTICAL RESULTS...................................................................... 7
5.0 CONCLUSIONS & RECOMMENDATIONS ................................ 8
6.0 CLOSURE ........................................................................................... 9

Page I
TABLE OF CONTENTS (Continued)

FIGURES:

1. Topographic Map
2. Site Map
3a. Adjoining Properties and Water Supply Wells
3b. Adjoining Properties and Water Supply Wells
4. Potentiometric Surface Map (12/09/2015)
5. MTBE Isoconcentration Map (12/09/2015)
6. 1,2-Dichloroethane Isoconcentration Map (12/09/2015)
7. Remediation System Layout Map (1/16/12)

TABLES:

1. Monitoring Well Construction Details
2. Groundwater Elevation Data
3. Monitoring Well Analytical Results
4. Water Supply Well Analytical Results
5. System Operation Parameters

APPENDICES:

A. Groundwater Laboratory Report & Chain of Custody
B. Supply Well Results Letter (POE)
C. Recent O&M Activities

Page II
ACRONYMS

BLS ................Below Land Surface
BTEX ............Benzene, Toluene, Ethylbenzene, & Xylenes
CFR ................Code of Federal Regulations
COC ...............Chain of Custody
CSA ................Comprehensive Site Assessment
DEQ ...............Department of Environmental Quality
EPH ................Extractable Petroleum Hydrocarbons
GCLs ..............Gross Contaminant Levels
HASP .............Health & Safety Plan
MADEP..........Massachusetts Department of Environmental Protection
MSCC ............Maximum Soil Contaminant Concentration
MTBE ............Methyl Tertiary Butyl Ether
µg/L ................Micrograms per Liter
mg/kg .............Milligrams per kilogram
MW ................Monitoring Well
NCAC ............North Carolina Administrative Code
O&M ..............Operations and Maintenance
OSHA .............Occupational Safety and Health Administration
OVA ...............Organic Vapor Analyzer
PPM ...............Parts Per Million
PID .................Photo-ionization Detector
P&ID ..............Process & Instrumentation Diagram
PVC ................Poly-vinyl Chloride
QA/QC ...........Quality Assurance / Quality Control
SCFM .............Standard Cubic Feet per Minute
SVE ................Soil Vapor Extraction
SW .................Water Supply Well
UST ................Underground Storage Tank
US EPA ..........United States Environmental Protection Agency
VPH................Volatile Petroleum Hydrocarbons

Page III
Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 1 Pyramid Project # 2015-217 01/11/2016
ACTIVE REMEDIATION MONITORING REPORT
Harold Smith Grocery
Burlington, North Carolina

1.0 INTRODUCTION

1.1 Site Information

SITE NAME: Harold Smith Grocery
ADDRESS: 2774 Union Ridge Road
CITY: Burlington, NC
COUNTY: Alamance

CURRENT PROPERTY OWNER: Jessica Alton
CURRENT PROPERTY USE: Inactive Store (used as storage)
OWNER OF USTs: TAC, Inc. (All USTs were removed in 1994)
RESPONSIBLE PARTY: TAC, Inc.
NCDEQ UST FACILITY ID: 0-024148
GROUNDWATER INCIDENT NO.: 12913
SITE RANKING: H755E

UNDERGROUND STORAGE TANKS (USTs)

(gallons)
1 550 Kerosene Removed 8/01/94
2 550 Gasoline Removed 8/01/94
3 550 Gasoline Removed 8/01/94
4 1,000 Gasoline Removed 8/01/94

FIGURES: Figure 1: Topographic Map
Figure 2: Site Map
Figure 3a: Adjoining Properties and Water Supply Wells
Figure 3b: Adjoining Properties and Water Supply Wells

1.2 Adjoining Properties and Potential Receptors

ADJOINING PROPERTY USE: Residential/Agricultural
PUBLIC WATER AVAILABILITY: Unavailable
SUPPLY WELLS WITHIN 1000 FEET: Yes (see Figure 3a/b)
SUPPLY WELLS IMPACTED ABOVE
NCAC 2L STANDARDS: Yes, Supply well at 2765 Union Ridge Rd.
(currently on POE system)
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NEAREST SURFACE WATER: Intermittent Creek – 500-600’ SE
BASEMENTS: None
SUBSURFACE UTILITIES: None near source area

1.3 Site Hydrology & Geology

GEOLOGIC PROVINCE: Carolina Slate Belt
BEDROCK TYPE: Felsic Intrusive Complex
DEPTH TO BEDROCK: 25-38 feet BGS (below ground surface)
CURRENT DEPTH TO WATER TABLE: 7.19 – 12.59 feet BGS (12/9/15)
HISTORIC GW FLUCTUATIONS: Over the past 14 years, the groundwater has
fluctuated in the source area from 5-15 feet BGS
POTENTIOMETRIC GRADIENT: Southeast ~ 0.025 ft. /ft.
HYDRAULIC CONDUCTIVITY (K): 6.17–6.25 x 10-7 ft. /sec.
GROUNDWATER VELOCITY: ~0.4–1.3 feet/year

1.4 Previous Reports

REPORT TITLE

CONSULTANT
DATE OF
REPORT

COMMENTS
Pyramid Environmental 8/30/94 Soil TPH above Action Level
Pyramid Environmental 1/2/95
Pyramid Environmental 9/20/96
Pyramid Environmental 1/30/97 Original CAP report
Pyramid Environmental
Pyramid Environmental 6/7/99
Pyramid Environmental 11/99 to 01/13
Soil Cleanup Report Pyramid Environmental 5/31/2011
Pyramid Environmental
Pyramid Environmental 8/10/15
Pyramid Environmental 12/08/15
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REPORT TITLE

CONSULTANT
DATE OF
REPORT

COMMENTS
Active Remediation
Monitoring Report Pyramid Environmental 1/10/16 Current Report

2.0 GROUNDWATER SAMPLING

2.1 Monitoring Well Sampling

On December 9, 2015, selected monitoring wells at the Harold Smith Site were sampled.

WELLS SAMPLED: MW-1A, MW-3, MW-4, MW-5, MW-6, MW-7, MW-9, MW-10,
MW-11, MW-12, MW-13 and MW-15A
LAB ANALYSES: EPA Method 6200B

FREE PRODUCT: No free product has been observed on this site.

TABLES & GRAPHS: Table 1: Monitoring Well Construction Details
Table 2: Groundwater Elevation Data
Table 3: Monitoring Well Analytical Results

FIGURES: Figure 4: Potentiometric Surface Map
Figure 5: MTBE Concentration Map
Figure 6: 1, 2-Dichloroethane Isoconcentration Map

LABORATORY REPORT & CHAIN-OF-CUSTODY: Appendix A

FIELD PROCEDURES: Field procedures were performed as outlined in the DEQ July 15,
2008 and May 1, 2012 updates publication “Guidelines for
Sampling” under the UST Section.

2.2 Potable Water Supply Well Sampling

SAMPLING DATE: December 9, 2015
WELLS SAMPLED: 2765 INF, 2765 MID, 2765 EFF, 2768B, 2760, 2773, and 2779
The house at 2779 Union Ridge Road no longer uses the supply
well in the front yard, but uses the well located on an adjacent
eastern property. The property at 2768 Union Ridge Road uses the
supply well in the back yard and is automatically switched to the
well in the front yard (2768-A) if the water level gets too low.

LAB ANALYSES: EPA Method 6200B
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TABLES: Table 4: Water Supply Well Analytical Results
FIGURES: Figure 3 a/b: Adjoining Properties and Water Supply Wells.

LABORATORY REPORTS & CHAINS-OF-CUSTODY: Appendix A

FIELD PROCEDURES: Field procedures were performed as outlined in the DEQ July 15,
2008 and May 1, 2012 updates publication “Guidelines for
Sampling” under the UST Section.

*NOTE* Supply wells are named by the address of the residence they serve and not the property
owner. All supply well addresses sampled are on Union Ridge Road. Mr. James McMillan
requested that Pyramid inform him of the POE system analytical results after each sampling. The
well analytical evaluation letter is presented in Appendix B.

3.0 TREATMENT SYSTEM OPERATIONAL STATUS
3.1 System Operations

The air sparging (AS) and soil vapor extraction (SVE) treatment system for the Harold Smith
Grocery site began operation in July 1999 and operated through 2004 when it was shut down.

The system was restarted in February 2005 and the system was operational through October
2005. Repairs were made to the system and the remediation system was officially restarted on
February 8, 2006. The system ran intermittently during the first quarter of 2006, needing minor
repairs. System operation was interrupted by electrical power interruptions (strong storms)
tripping circuit breakers. In August 2006, the system electrical contacts were found to be
completely melted. The electrical components were replaced after pre-approval, and tested. The
motor of the air-sparge compressor would not operate, and the electric motor was found to be
locked up. Pyramid contacted the equipment manufacturer and priced the replacement items
necessary to get the air-sparge system running again. The SVE system continued to run after the
replacement of the circuit breakers.

In March 2007 the rebuilt air sparge motor was put back in service. The restored compressor
operated from March 2007 through June 2008. At this time, the air-sparge compressor needed to
be replaced. The air sparge motor was replaced with a more serviceable model on October 7,
2008. The carbon vanes were changed by Pyramid in February 2010. The air sparge system was
operational during the 1st quarter of 2011. The system ceased operating in March 2011 to allow
for the soil excavation. Since the system operation ceased, DO concentrations dropped and
Pyramid recommended continued air sparging operation to speed site cleanup. In January 2012,
the air sparge system was restarted using the selected remaining air sparge wells.

In 2013, the system was upgraded to include deeper AS wells and a higher pressure compressor.

Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 5 Pyramid Project # 2015-217 01/11/2016
The system was operational for most of the fourth quarter of 2014, with the exception of short
period of time in December when the system was down due a damaged compressor drive belt.
The damaged belt was discovered on 12/12/14 and replaced on 12/19/14 and the system was re-
started. Since restarting the system in December 2014, the system has remained operational. A
summary of the operations and maintenance activities performed from October 2015 through
December 2015 is presented in Appendix C.

3.2 Contaminated Soil Removal

In March 2009, Pyramid collected risk-based soil samples from several soil borings and added
several monitoring wells. The additional assessment was conducted to investigate the soils in the
area of the former pump island, and provide additional monitoring wells to assess the source area
for regulatory incident closure. The highest groundwater concentrations have been in MW-1 and
MW-1A throughout the remediation period. As a result of the additional investigations, an area
approximately 40 feet by 20 feet was identified as containing soil concentrations greater than
Soil-to-Groundwater (STGW) standards. Only the soil boring directly at the location of the
former pump island showed concentrations above residential Maximum Soil Contaminant
Concentrations (MSCCs). The DEQ requested that Pyramid evaluate soil excavation as a way to
help move the site toward regulatory closure. After the excavation plan was preapproved by the
DEQ, Pyramid implemented the excavation plan.

In May 2011, Pyramid supervised the excavation of petroleum contaminated soils at the Harold
Smith site in Burlington, NC. The goal of the soil excavation was to remove volatile petroleum
hydrocarbons from the smear zone (between 5 and 15 feet BLS) to help reduce groundwater
contamination. Based on certified weight tickets, 483.69 tons of petroleum-contaminated soil
was removed. Pyramid requested pre-approval to implement oxygen release compound in
addition to the excavation, but DEQ denied the request. The laboratory results of the post
excavation soil samples collected indicate that all of the contaminated soils above the residential
MSCCs were removed.

The remaining contamination detected at the site was above the STGW MSCCs and well below
the residential standards. The remaining STGW concentrations were located underneath the store
building, along the northern property boundary, and on the eastern edge of the property near
Union Ridge Road. Because of the structures, roads, and utilities, additional soil excavation was
not feasible or recommended.

After the excavation of contaminated soil, Pyramid installed monitoring wells MW-1A and MW-
15A to assess the groundwater in the source area. The latest results of these new wells (MW-1A
and MW-15A) since installation are included in Section 4.0 with past results located in Table 3.
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3.3 System Update

FIGURES: Figure 7: Remediation System Layout Map

To prevent the migration of the contaminant plume, protect nearby supply wells, and speed up
remediation, the current air sparge (AS) and soil vapor extraction (SVE) system was updated in
October 2012. Additional wells were added to the air sparge segment of the remediation system.
Seven deeper air sparge wells were added to surround the existing petroleum contaminant plume.
The additional wells prevent contaminant plume migration and provide additional air flow for
petroleum hydrocarbons volatilization. Along with the AS remediation update, the SVE system
was repaired after it was damaged during the soil excavation in May 2011. A map of the
Remediation System Layout is shown in Figure 7.

4.0 SOIL & GROUNDWATER ASSESSMENT

4.1 Groundwater Analytical Results

The results of the December 9, 2015 sampling event showed that remaining petroleum
contaminants were detected at low concentrations. All of the reported concentrations are listed in
micrograms per liter (µg/L). The concentrations of 1,2-Dichloroethane (1,2-DCA) in MW-1A
(1.2 µg/L), MW-11 (0.61 µg/L), SW-2773 (0.94 µg/L), and SW-2765 (10.0 µg/L) were above the
2L groundwater standard of 0.4 µg/L. The concentrations of targeted compounds for this
sampling event have slightly increased or remained the same in all of the monitoring wells. The
highest concentrations found for this sampling event are shown below. Concentrations above
NCAC 2L groundwater standards are shown in bold and the associated well numbers are shown
in parentheses. All of the reported concentrations are listed in micrograms per liter (µg/L).

• Benzene Not Detected (MW-1A)
• Toluene Not Detected (MW-15A)
• Ethylbenzene Not Detected (MW-15A)
• Total Xylenes Not Detected (MW-15A)
• MTBE 53 µg/L (SW-2765 Influent)
• Isopropyl Ether (IPE) 75 µg/L (SW-2765 Influent)
• 1,2-Dichloroethane 10 µg/L (SW-2765 Influent)
• Naphthalene Not Detected (MW-15A)

Over the past 14 years of groundwater and soil remediation, the general concentration trends
demonstrated in the groundwater monitoring wells have been decreasing and are now
approaching regulatory closure.

The benzene concentrations in MW-1A have decreased from over 8,000 µg/L in 1998 to below
detection limits for the current monitoring period. Benzene concentrations in MW-15A have
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remained at a concentration below detection limits for the last few sampling events from June
through December 2015. The MTBE concentrations in MW-1A have decreased from 610 µg/L in
1999 to 1.7 µg/L for the current monitoring period. Concentrations of 1,2-dichloroethane were
detected in MW-1A, MW-11, and the influent for SW-2765 and remain above the 2L Standard.

As shown in Table 3, the groundwater contaminant concentrations in the source area decreased
significantly after the contaminated soil excavation was performed in May 2001. In planning for
the soil excavation project, Pyramid recommended that the DEQ consider the placement of
oxygen-release compounds in the open excavation to help clean up the site. Since cleanup will
have to be to the NCAC 2L Standards, any remedial process that can help reach regulatory
closure more quickly should be considered by the DEQ. Pyramid’s request was not approved for
Trust Fund reimbursement, and no oxygen-release compounds were used in the excavation. In
the future, the Trust Fund should consider reimbursing the use of oxygen-release compounds
while excavations are open to help reduce the overall costs for petroleum incident closures.
Active soil and groundwater remediation are needed to reduce the remaining petroleum
contaminant concentrations in the groundwater.

4.2 Supply Well Analytical Results

Supply well sampling was conducted on December 9, 2015 as required by the State. Pyramid
sampled four supply wells 2768B, 2760, 2773, and 2779. Influent, mid-fluent and effluent
samples were also collected from the point of entry (POE) treatment system for SW-2765. All
samples were collected using clean, disposable nitrile gloves, preserved in laboratory provided
containers, packed in ice and shipped to Prism Analytical Laboratories for analysis using EPA
Method 6200B.

Groundwater pumped from the supply well at address 2765 (SW-2765) is treated by a Point-of-
Entry (POE) treatment system installed in 2000. The POE system consists of particulate and
carbon filters that remove petroleum from the groundwater. This residential treatment system has
shown effective groundwater treatment since 2000. The laboratory results of treated water
samples collected from the supply well in December 2015 show no detections of petroleum
contaminants.

For the untreated water (influent) from SW-2765, MTBE (53 µg/L), IPE (75 µg/L), and 1,2-
dichloroethane (10 µg/L) were detected above their respective NCAC 2L Groundwater
Standards. No petroleum hydrocarbon concentrations were detected in the treated water (effluent)
showing effective POE treatment. Table 4 shows the recent supply well analytical results. A
copy of the laboratory report and chain-of-custody form is presented in Appendix A.

The supply well samples from SW-2773 showed a concentration of 1,2-Dichloroethane (0.94
µg/L) above the 2L standards. IPE and MTBE were also present, but at concentrations that are
well below the 2L standards. This supply well has shown little to no petroleum impacts in the
past several years. In the March 2015 sample analysis, there was an “Estimated” detection of
trans-1,2-dichloroethene reported by the laboratory. The Prism lab report stated:

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“For sample 5030124-05 with client ID of SW-2773, the initial 6200 was analyzed
undiluted and showed a large hit of Trans-1,2-dichloroethene that was outside of
calibration range. Dilutions of 1:20 and 1:50 were analyzed and the Trans-1,2-
dichloroethene did not duplicate. Vials were checked for accuracy in labeling and were
correct. The initial run is reported with an "E" flag to show an estimated value. “

Basically, the initial detection was not confirmed and was a questionable result. Pyramid
recommended re-sampling the well, which was planned and pre-approved by the Trust Fund.
Since the residence is provided with bottled water at this time, the potential for exposure was
mitigated. Pyramid re-sampled SW-2773 in the June 2015 sampling event. In June 2015, the
trans-1,2-dichloroethene detection of 2.4 µg/L was far below the 2L standard of 100 µg/L. The
current sampling event in December 2015 showed a concentration of 0.51 µg/L. Pyramid will
continue to monitor the trans-1,2-dichloroethene concentrations for this well.

Laboratory analytical results show that there were no other detectable petroleum hydrocarbon
concentrations in the supply well samples collected from wells 2768B, 2760, and 2779.

Pyramid recommends continued POE treatment of supply well 2765, continued sampling of the
closest supply wells (2765 & 2773) on a quarterly basis, and continued sampling of the wells
further from the source area (2761, 2768, 2774, and 2779) on an annual basis. The next quarterly
sampling event will be in March 2016.

5.0 CONCLUSIONS & RECOMMENDATIONS

Pyramid has completed the directed operation & maintenance and groundwater monitoring at the
Harold Smith Grocery. Based on the current groundwater concentrations of MTBE, IPE, and 1,2-
Dichloroethane remaining above the 2L groundwater standard, the site remains high risk. The
remediation goal is to reduce dissolved groundwater contamination below 2L standards to protect
local water supply well users.

• The contaminated soil excavation was completed in May 2011. Contaminated soil
beneath the NC DOT Right-of-Way and under the store building was unable to be
removed. Since petroleum concentrations that exceed the STGW levels remain under the
building and near the roadway, continued soil remediation using the SVE system is
recommended at the site.

• Based on the risk to private well users, Pyramid recommended a new air-sparge system
with deeper air sparge wells to enhance the groundwater cleanup. This new system was
designed, bid, pre-approved, and built from October 2012 through April 2013. The
system was successfully started on April 3, 2013. The new system has shown significant
reductions in the remaining petroleum contaminants.

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• The continued presence of concentrations of petroleum contaminants in monitoring wells
MW-1A, MW-15A, and SW-2765 show that groundwater contamination remains above
regulatory closure levels.

• Continued groundwater remediation and monitoring is recommended for the site. The
next semi-annual sampling of the monitoring wells will be conducted in March 2016.

6.0 CLOSURE

This report is prepared for and made available solely for the use of T.A.C, Inc. and the NCDEQ,
and the contents thereof may not be used or relied upon by any other person without the express
written consent and authorization of Pyramid Environmental & Engineering, P.C. The
observations, conclusions, and recommendations documented in this report are based on site
conditions and information reviewed at the time of the investigation. Pyramid Environmental &
Engineering, P.C. appreciates the opportunity to provide this environmental service.

FIGURES

TABLES
TABLE 1 Monitoring Well Construction Details Harold Smith Grocery Incident #12913
Union Ridge Road, Burlington, North Carolina

WELL INSTALLED DEPTH BEDROCK CASING INTERVAL INTERVAL INTERVAL INTERVAL INTERVAL
MW-1 11/21/94 20’ NBE NA 0-10’ 10-20’ 0-6’ 6-7.5 7.5-20’
MW-1A 6/27/11 24’ NBE NA 0-4’ 4-24’ 0-1’ 1-3’ 3-24’
MW-2 10/11/95 25’ 25’ NA 0-10’ 10-20’ 0-6’ 6-8’ 8-20’
MW-3 10/11/95 22’ NBE NA 0-7’ 7-22’ 0-3’ 3-5’ 5-22’
MW-4 11/8/95 20’ NBE NA 0-5’ 5-20’ 0-2’ 2-4’ 4-20’
MW-5 11/8/95 20’ NBE NA 0-5’ 5-20’ 0-2’ 2-4’ 4-20’
MW-6 1/2/96 53’ 25’ 0-30’ 0-43’ 43-53’ 0-38’ 38-41’ 41-53’
MW-7 1/3/96 13.8’ NBE NA 0-3.8’ 3.8-13.8’ 0-0.5’ 0.5-1.5’ 1.5-13.8’
MW-8 5/6/96 14.3’ 15’ NA 0-4.3’ 4.3-14.3’ 0-1.8’ 1.8-3.3’ 3.3-14.3’
MW-9 5/6/96 15’ NBE NA 0-5’ 5-15’ 0-2.5’ 2.5-4’ 6/4-15’
MW-10 11/30/99 20’ NBE NA 0-5’ 5-20’ 0.5-2’ 2-4’ 4-20’
MW-11 7/25/00

20’ NA NA 0-5’ 5-20’ 0.5-2’ 2-4’ 4-20’
MW-12 11/6/01 30’ NBE NA 0-10’ 10-30’ 0-6’ 6-8’ 8-30’
MW-13 3/5/09 25’ NBE NA 0-5’ 5-25’ 0-1’ 1-3’ 3-25’
MW-14 3/5/09 25’ NBE NA 0-5’ 5-25’ 0-1’ 1-3’ 3-25’
MW-15 3/5/09 25’ 24’ NA 0-5’ 5-25’ 0-1’ 1-3' 3-25’
MW-15A 6/27/11 24’ NBE NA 0-4’ 4-24’ 0-1’ 1-3’ 3-24’
TS-1 12/17/99 15’ NBE NA 0-5’ 5-15’ 0-2’ 2-4’ 4-15’
TS-2 12/17/99 15’ NBE NA 0-5’ 5-15’ 0-2’ 2-4’ 4-15’
TS-3 12/17/99 15’ NBE NA 0-5’ 5-15’ 0-2’ 2-4’ 4-15’
ALL MONITORING WELLS HAVE 2” PVC CASING/RISER AND 2” PVC SCREEN WITH 0.01” SLOTS. OUTER CASING FOR TYPE III WELL IS 6” PVC.
NBE = NO BEDROCK ENCOUNTERED. NA = NOT APPLICABLE. SHADED WELLS ARE CLOSED.
Page 1 of 6
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
MW-1A 06-30-11 94.650 12.24 0.00 0.00 0.00 12.24 82.41
09-8-11 94.650 13.59 0.00 0.00 0.00 13.59 81.06
12-8-11 94.650 13.49 0.00 0.00 0.00 13.49 81.16
03-13-12 94.650 13.49 0.00 0.00 0.00 12.35 82.30
06-5-12 94.650 12.14 0.00 0.00 0.00 12.14 82.51
09-11-12 94.650 13.22 0.00 0.00 0.00 13.22 81.43
12-12-12 94.650 13.85 0.00 0.00 0.00 13.85 80.80
03-12-13 94.650 11.83 0.00 0.00 0.00 11.83 82.82
05-29-13 94.650 10.44 0.00 0.00 0.00 10.44 84.21
09-10-13 94.650 8.96 0.00 0.00 0.00 8.96 85.69
11-6-13 94.650 10.96 0.00 0.00 0.00 10.96 83.69
03-19-14 94.650 8.07 0.00 0.00 0.00 8.07 86.58
06-26-14 94.650 8.72 0.00 0.00 0.00 8.72 85.93
08-22-14 94.650 10.13 0.00 0.00 0.00 10.13 84.52
11-7-14 94.650 12.00 0.00 0.00 0.00 12.00 82.65
03-4-15 94.650 11.21 0.00 0.00 0.00 11.21 83.44
06-25-15 94.650 11.48 0.00 0.00 0.00 11.48 83.17
09-22-15 94.650 13.50 0.00 0.00 0.00 13.50 81.15
12-9-15 94.650 10.67 0.00 0.00 0.00 10.67 83.98
MW-3 09-9-09 93.065 12.03 0.00 0.00 0.00 12.03 81.04
12-3-09 93.065 10.40 0.00 0.00 0.00 10.40 82.67
03-24-10 93.065 7.34 0.00 0.00 0.00 7.34 85.73
06-24-10 93.065 8.07 0.00 0.00 0.00 8.07 85.00
09-8-10 93.065 9.62 0.00 0.00 0.00 9.62 83.45
12-10-10 93.065 10.77 0.00 0.00 0.00 10.77 82.30
03-8-11 93.065 10.60 0.00 0.00 0.00 10.60 82.47
06-30-11 93.065 10.74 0.00 0.00 0.00 10.74 82.33
09-8-11 93.065 12.16 0.00 0.00 0.00 12.16 80.91
12-8-11 93.065 12.06 0.00 0.00 0.00 12.06 81.01
03-13-12 93.065 13.49 0.00 0.00 0.00 10.52 82.55
06-5-12 93.065 10.71 0.00 0.00 0.00 10.71 82.36
09-11-12 93.065 11.79 0.00 0.00 0.00 11.79 81.28
12-12-12 93.065 12.37 0.00 0.00 0.00 12.37 80.70
03-12-13 93.065 10.53 0.00 0.00 0.00 10.53 82.54
05-29-13 93.065 9.04 0.00 0.00 0.00 9.04 84.03
09-10-13 93.065 7.53 0.00 0.00 0.00 7.53 85.54
11-6-13 93.065 8.88 0.00 0.00 0.00 8.88 84.19
03-19-14 93.065 6.69 0.00 0.00 0.00 6.69 86.38
06-26-14 93.065 7.46 0.00 0.00 0.00 7.46 85.61
08-22-14 93.065 8.82 0.00 0.00 0.00 8.82 84.25
11-7-14 93.065 10.84 0.00 0.00 0.00 10.84 82.23
03-4-15 93.065 8.51 0.00 0.00 0.00 8.51 84.56
06-25-15 93.065 10.22 0.00 0.00 0.00 10.22 82.85
09-22-15 93.065 12.35 0.00 0.00 0.00 12.35 80.72
12-9-15 93.065 9.42 0.00 0.00 0.00 9.42 83.65
MW-4 09-9-09 91.470 10.81 0.00 0.00 0.00 10.81 80.66
12-3-09 91.470 9.11 0.00 0.00 0.00 9.11 82.36
03-24-10 91.470 6.10 0.00 0.00 0.00 6.10 85.37
06-24-10 91.470 6.76 0.00 0.00 0.00 6.76 84.71
09-8-10 91.470 8.41 0.00 0.00 0.00 8.41 83.06
12-10-10 91.470 9.55 0.00 0.00 0.00 9.55 81.92
03-8-11 91.470 9.37 0.00 0.00 0.00 9.37 82.10
06-30-11 91.470 9.53 0.00 0.00 0.00 9.53 81.94
09-8-11 91.470 11.12 0.00 0.00 0.00 11.12 80.35
12-8-11 91.470 10.81 0.00 0.00 0.00 10.81 80.66
03-13-12 91.470 13.49 0.00 0.00 0.00 8.58 82.89
06-5-12 91.470 9.50 0.00 0.00 0.00 9.50 81.97
09-11-12 91.470 10.67 0.00 0.00 0.00 10.67 80.80
12-12-12 91.470 11.15 0.00 0.00 0.00 11.15 80.32
03-12-13 91.470 8.84 0.00 0.00 0.00 8.84 82.63
05-29-13 91.470 7.80 0.00 0.00 0.00 7.80 83.67
09-10-13 91.470 6.33 0.00 0.00 0.00 6.33 85.14
11-6-13 91.470 7.70 0.00 0.00 0.00 7.70 83.77
03-19-14 91.470 5.51 0.00 0.00 0.00 5.51 85.96
06-26-14 91.470 6.18 0.00 0.00 0.00 6.18 85.29
08-22-14 91.470 7.58 0.00 0.00 0.00 7.58 83.89
11-7-14 91.470 9.62 0.00 0.00 0.00 9.62 81.85
03-4-15 91.470 7.55 0.00 0.00 0.00 7.55 83.92
06-25-15 91.470 8.97 0.00 0.00 0.00 8.97 82.50
09-22-15 91.470 11.11 0.00 0.00 0.00 11.11 80.36
12-9-15 91.470 8.11 0.00 0.00 0.00 8.11 83.36
TABLE 2
Union Ridge Road, Burlington, North carolina
Groundwater Elevation Data
Harold Smith GroceryIncident #12913
Page 2 of 6
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
09-9-09 95.045 12.81 0.00 0.00 0.00 12.81 82.24
12-3-09 95.045 6.35 0.00 0.00 0.00 6.35 88.70
03-24-10 95.045 6.63 0.00 0.00 0.00 6.63 88.42
06-24-10 95.045 8.25 0.00 0.00 0.00 8.25 86.80
09-8-10 95.045 10.34 0.00 0.00 0.00 10.34 84.71
12-10-10 95.045 9.78 0.00 0.00 0.00 9.78 85.27
03-8-11 95.045 7.20 0.00 0.00 0.00 7.20 87.85
06-30-11 95.045 8.53 0.00 0.00 0.00 8.53 86.52
09-8-11 95.045 12.62 0.00 0.00 0.00 12.62 82.43
12-8-11 95.045 8.74 0.00 0.00 0.00 8.74 86.31
03-13-12 95.045 13.49 0.00 0.00 0.00 10.94 84.11
06-5-12 95.045 10.87 0.00 0.00 0.00 10.87 84.18
09-11-12 95.045 11.98 0.00 0.00 0.00 11.98 83.07
12-12-12 95.045 13.20 0.00 0.00 0.00 13.20 81.85
03-12-13 95.045 7.32 0.00 0.00 0.00 7.32 87.73
05-29-13 95.045 9.38 0.00 0.00 0.00 9.38 85.67
09-10-13 95.045 8.16 0.00 0.00 0.00 8.16 86.89
11-6-13 95.045 9.53 0.00 0.00 0.00 9.53 85.52
03-19-14 95.045 2.87 0.00 0.00 0.00 2.87 92.18
06-26-14 95.045 7.78 0.00 0.00 0.00 7.78 87.27
08-22-14 95.045 9.06 0.00 0.00 0.00 9.06 85.99
11-7-14 95.045 11.16 0.00 0.00 0.00 11.16 83.89
03-4-15 95.045 1.70*0.00 0.00 0.00 1.70*93.35
06-25-15 95.045 10.78 0.00 0.00 0.00 10.78 84.27
09-22-15 95.045 13.05 0.00 0.00 0.00 13.05 82.00
12-9-15 95.045 7.19 0.00 0.00 0.00 7.19 87.86
MW-6 09-9-09 94.935 14.28 0.00 0.00 0.00 14.28 80.66
12-3-09 94.935 12.98 0.00 0.00 0.00 12.98 81.96
03-24-10 94.935 9.07 0.00 0.00 0.00 9.07 85.87
06-24-10 94.935 9.90 0.00 0.00 0.00 9.90 85.04
09-8-10 94.935 11.76 0.00 0.00 0.00 11.76 83.18
12-10-10 94.935 12.91 0.00 0.00 0.00 12.91 82.03
03-8-11 94.935 12.89 0.00 0.00 0.00 12.89 82.05
06-30-11 94.935 12.91 0.00 0.00 0.00 12.91 82.03
09-8-11 94.935 14.50 0.00 0.00 0.00 14.50 80.44
12-8-11 94.935 14.20 0.00 0.00 0.00 14.20 80.74
03-13-12 94.935 13.49 0.00 0.00 0.00 12.94 82.00
06-5-12 94.935 13.10 0.00 0.00 0.00 13.10 81.84
09-11-12 94.935 14.26 0.00 0.00 0.00 14.26 80.68
12-12-12 94.935 14.58 0.00 0.00 0.00 14.58 80.36
03-12-13 94.935 12.72 0.00 0.00 0.00 12.72 82.22
05-29-13 94.935 11.38 0.00 0.00 0.00 11.38 83.56
09-10-13 94.935 9.65 0.00 0.00 0.00 9.65 85.29
11-6-13 94.935 11.29 0.00 0.00 0.00 11.29 83.65
03-19-14 94.935 8.58 0.00 0.00 0.00 8.58 86.36
06-26-14 94.935 9.39 0.00 0.00 0.00 9.39 85.55
08-22-14 94.935 11.01 0.00 0.00 0.00 11.01 83.93
11-7-14 94.935 12.99 0.00 0.00 0.00 12.99 81.95
03-4-15 94.935 12.11 0.00 0.00 0.00 12.11 82.83
06-25-15 94.935 12.43 0.00 0.00 0.00 12.43 82.51
09-22-15 94.935 14.50 0.00 0.00 0.00 14.50 80.44
12-9-15 94.935 11.53 0.00 0.00 0.00 11.53 83.41
MW-7 09-9-09 94.215 11.61 0.00 0.00 0.00 11.61 82.61
12-3-09 94.215 9.65 0.00 0.00 0.00 9.65 84.57
03-24-10 94.215 7.69 0.00 0.00 0.00 7.69 86.53
06-24-10 94.215 7.55 0.00 0.00 0.00 7.55 86.67
09-8-10 94.215 8.18 0.00 0.00 0.00 8.18 86.04
12-10-10 94.215 10.36 0.00 0.00 0.00 10.36 83.86
03-8-11 94.215 9.94 0.00 0.00 0.00 9.94 84.28
06-30-11 94.215 10.92 0.00 0.00 0.00 10.92 83.30
09-8-11 94.215 12.05 0.00 0.00 0.00 12.05 82.17
12-8-11 94.215 11.64 0.00 0.00 0.00 11.64 82.58
03-13-12 94.215 13.49 0.00 0.00 0.00 10.75 83.47
06-5-12 94.215 10.63 0.00 0.00 0.00 10.63 83.59
09-11-12 94.215 11.33 0.00 0.00 0.00 11.33 82.89
12-12-12 94.215 12.20 0.00 0.00 0.00 12.20 82.02
03-12-13 94.215 NG 0.00 0.00 0.00 0.00 NG
05-29-13 94.215 NG 0.00 0.00 0.00 0.00 NG
09-10-13 94.215 7.57 0.00 0.00 0.00 7.57 86.65
11-6-13 94.215 9.08 0.00 0.00 0.00 9.08 85.14
Page 3 of 6
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
06-26-14 94.215 7.47 0.00 0.00 0.00 7.47 86.75
08-22-14 94.215 8.70 0.00 0.00 0.00 8.70 85.52
11-7-14 94.215 10.60 0.00 0.00 0.00 10.60 83.62
03-4-15 94.215 9.40 0.00 0.00 0.00 9.40 84.82
06-25-15 94.215 9.96 0.00 0.00 0.00 9.96 84.26
09-22-15 94.215 11.76 0.00 0.00 0.00 11.76 82.46
12-9-15 94.215 9.20 0.00 0.00 0.00 9.20 85.02
MW-8 09-9-09 89.630 NG 0.00 0.00 0.00 0.00 NG
12-3-09 89.630 7.23 0.00 0.00 0.00 7.23 82.40
03-24-10 89.630 5.64 0.00 0.00 0.00 5.64 83.99
06-24-10 89.630 6.13 0.00 0.00 0.00 6.13 83.50
09-8-10 89.630 7.79 0.00 0.00 0.00 7.79 81.84
12-10-10 89.630 9.43 0.00 0.00 0.00 9.43 80.20
03-8-11 89.630 8.39 0.00 0.00 0.00 8.39 81.24
06-30-11 89.630 NG 0.00 0.00 0.00 0.00 NG
09-8-11 89.630 NG 0.00 0.00 0.00 0.00 NG
12-8-11 89.630 NG 0.00 0.00 0.00 0.00 NG
03-13-12 89.630 NG 0.00 0.00 0.00 0.00 NG
06-5-12 89.630 8.80 0.00 0.00 0.00 8.80 80.83
09-11-12 89.630 9.84 0.00 0.00 0.00 9.84 79.79
12-12-12 89.630 10.60 0.00 0.00 0.00 10.60 79.03
03-12-13 89.630 NG 0.00 0.00 0.00 0.00 NG
05-29-13 89.630 NG 0.00 0.00 0.00 0.00 NG
09-10-13 89.630 NG 0.00 0.00 0.00 0.00 NG
11-6-13 89.630 NG 0.00 0.00 0.00 0.00 NG
03-19-14 89.630 NG 0.00 0.00 0.00 0.00 NG
06-26-14 89.630 NG 0.00 0.00 0.00 0.00 NG
08-22-14 89.630 NG 0.00 0.00 0.00 0.00 NG
11-7-14 89.630 NG 0.00 0.00 0.00 0.00 NG
03-4-15 89.630 NG 0.00 0.00 0.00 0.00 NG
06-25-15 89.630 NG 0.00 0.00 0.00 0.00 NG
09-22-15 89.630 NG 0.00 0.00 0.00 0.00 NG
12-9-15 89.630 NG 0.00 0.00 0.00 0.00 NG
MW-9 09-9-09 94.770 14.21 0.00 0.00 0.00 14.21 80.56
12-3-09 94.770 12.76 0.00 0.00 0.00 12.76 82.01
03-24-10 94.770 8.91 0.00 0.00 0.00 8.91 85.86
06-24-10 94.770 9.79 0.00 0.00 0.00 9.79 84.98
09-8-10 94.770 11.70 0.00 0.00 0.00 11.70 83.07
12-10-10 94.770 12.89 0.00 0.00 0.00 12.89 81.88
03-8-11 94.770 12.79 0.00 0.00 0.00 12.79 81.98
06-30-11 94.770 NG 0.00 0.00 0.00 0.00 NG
09-8-11 94.770 14.34 0.00 0.00 0.00 14.34 80.43
12-8-11 94.770 14.09 0.00 0.00 0.00 14.09 80.68
03-13-12 94.770 13.49 0.00 0.00 0.00 11.82 82.95
06-5-12 94.770 NG 0.00 0.00 0.00 0.00 NG
09-11-12 94.770 14.15 0.00 0.00 0.00 14.15 80.62
12-12-12 94.770 NG 0.00 0.00 0.00 0.00 NG
03-12-13 94.770 12.60 0.00 0.00 0.00 12.60 82.17
05-29-13 94.770 11.20 0.00 0.00 0.00 11.20 83.57
09-10-13 94.770 9.50 0.00 0.00 0.00 9.50 85.27
11-6-13 94.770 11.16 0.00 0.00 0.00 11.16 83.61
03-19-14 94.770 8.18 0.00 0.00 0.00 8.18 86.59
06-26-14 94.770 9.30 0.00 0.00 0.00 9.30 85.47
08-22-14 94.770 10.88 0.00 0.00 0.00 10.88 83.89
11-7-14 94.770 12.92 0.00 0.00 0.00 12.92 81.85
03-4-15 94.770 12.00 0.00 0.00 0.00 12.00 82.77
06-25-15 94.770 12.27 0.00 0.00 0.00 12.27 82.50
09-22-15 94.770 14.37 0.00 0.00 0.00 14.37 80.40
12-9-15 94.770 11.48 0.00 0.00 0.00 11.48 83.29
MW-10 09-9-09 93.210 13.25 0.00 0.00 0.00 13.25 79.96
12-3-09 93.210 10.51 0.00 0.00 0.00 10.51 82.70
03-24-10 93.210 7.80 0.00 0.00 0.00 7.80 85.41
06-24-10 93.210 8.77 0.00 0.00 0.00 8.77 84.44
09-8-10 93.210 10.74 0.00 0.00 0.00 10.74 82.47
12-10-10 93.210 12.15 0.00 0.00 0.00 12.15 81.06
03-8-11 93.210 11.78 0.00 0.00 0.00 11.78 81.43
06-30-11 93.210 12.29 0.00 0.00 0.00 12.29 80.92
09-8-11 93.210 13.39 0.00 0.00 0.00 13.39 79.82
12-8-11 93.210 12.91 0.00 0.00 0.00 12.91 80.30
03-13-12 93.210 13.49 0.00 0.00 0.00 11.61 81.60
Page 4 of 6
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
09-11-12 93.210 13.10 0.00 0.00 0.00 13.10 80.11
12-12-12 93.210 13.29 0.00 0.00 0.00 13.29 79.92
03-12-13 93.210 10.93 0.00 0.00 0.00 10.93 82.28
05-29-13 93.210 10.03 0.00 0.00 0.00 10.03 83.18
09-10-13 93.210 8.61 0.00 0.00 0.00 8.61 84.60
11-6-13 93.210 10.11 0.00 0.00 0.00 10.11 83.10
03-19-14 93.210 6.68 0.00 0.00 0.00 6.68 86.53
06-26-14 93.210 8.43 0.00 0.00 0.00 8.43 84.78
08-22-14 93.210 10.00 0.00 0.00 0.00 10.00 83.21
11-7-14 93.210 11.98 0.00 0.00 0.00 11.98 81.23
03-4-15 93.210 10.66 0.00 0.00 0.00 10.66 82.55
06-25-15 93.210 11.35 0.00 0.00 0.00 11.35 81.86
09-22-15 93.210 13.44 0.00 0.00 0.00 13.44 79.77
12-9-15 93.210 10.42 0.00 0.00 0.00 10.42 82.79
MW-11 09-9-09 95.840 NG 0.00 0.00 0.00 0.00 NG
12-3-09 95.840 14.05 0.00 0.00 0.00 14.05 81.79
03-24-10 95.840 10.06 0.00 0.00 0.00 10.06 85.78
06-24-10 95.840 10.91 0.00 0.00 0.00 10.91 84.93
09-8-10 95.840 12.77 0.00 0.00 0.00 12.77 83.07
12-10-10 95.840 14.00 0.00 0.00 0.00 14.00 81.84
03-8-11 95.840 13.94 0.00 0.00 0.00 13.94 81.90
06-30-11 95.840 13.92 0.00 0.00 0.00 13.92 81.92
09-8-11 95.840 15.52 0.00 0.00 0.00 15.52 80.32
12-8-11 95.840 15.21 0.00 0.00 0.00 15.21 80.63
03-13-12 95.840 13.49 0.00 0.00 0.00 13.94 81.90
06-5-12 95.840 14.16 0.00 0.00 0.00 14.16 81.68
09-11-12 95.840 15.36 0.00 0.00 0.00 15.36 80.48
12-12-12 95.840 15.60 0.00 0.00 0.00 15.60 80.24
03-12-13 95.840 13.88 0.00 0.00 0.00 13.88 81.96
05-29-13 95.840 12.35 0.00 0.00 0.00 12.35 83.49
09-10-13 95.840 10.64 0.00 0.00 0.00 10.64 85.20
11-6-13 95.840 12.35 0.00 0.00 0.00 12.35 83.49
03-19-14 95.840 9.58 0.00 0.00 0.00 9.58 86.26
06-26-14 95.840 10.41 0.00 0.00 0.00 10.41 85.43
08-22-14 95.840 12.02 0.00 0.00 0.00 12.02 83.82
11-7-14 95.840 14.04 0.00 0.00 0.00 14.04 81.80
03-4-15 95.840 13.21 0.00 0.00 0.00 13.21 82.63
06-25-15 95.840 13.41 0.00 0.00 0.00 13.41 82.43
09-22-15 95.840 15.52 0.00 0.00 0.00 15.52 80.32
12-9-15 95.840 12.59 0.00 0.00 0.00 12.59 83.25
MW-12 09-9-09 94.270 14.70 0.00 0.00 0.00 14.70 79.57
12-3-09 94.270 13.45 0.00 0.00 0.00 13.45 80.82
03-24-10 94.270 9.50 0.00 0.00 0.00 9.50 84.77
06-24-10 94.270 10.36 0.00 0.00 0.00 10.36 83.91
09-8-10 94.270 12.26 0.00 0.00 0.00 12.26 82.01
12-10-10 94.270 13.43 0.00 0.00 0.00 13.43 80.84
03-8-11 94.270 13.35 0.00 0.00 0.00 13.35 80.92
06-30-11 94.270 13.42 0.00 0.00 0.00 13.42 80.85
09-8-11 94.270 15.05 0.00 0.00 0.00 15.05 79.22
12-8-11 94.270 14.66 0.00 0.00 0.00 14.66 79.61
03-13-12 94.270 13.49 0.00 0.00 0.00 13.43 80.84
06-5-12 94.270 13.58 0.00 0.00 0.00 13.58 80.69
09-11-12 94.270 14.79 0.00 0.00 0.00 14.79 79.48
12-12-12 94.270 15.04 0.00 0.00 0.00 15.04 79.23
03-12-13 94.270 13.24 0.00 0.00 0.00 13.24 81.03
05-29-13 94.270 11.79 0.00 0.00 0.00 11.79 82.48
09-10-13 94.270 10.08 0.00 0.00 0.00 10.08 84.19
11-6-13 94.270 11.73 0.00 0.00 0.00 11.73 82.54
03-19-14 94.270 8.92 0.00 0.00 0.00 8.92 85.35
06-26-14 94.270 9.86 0.00 0.00 0.00 9.86 84.41
08-22-14 94.270 11.43 0.00 0.00 0.00 11.43 82.84
11-7-14 94.270 13.45 0.00 0.00 0.00 13.45 80.82
03-4-15 94.270 12.59 0.00 0.00 0.00 12.59 81.68
06-25-15 94.270 12.82 0.00 0.00 0.00 12.82 81.45
09-22-15 94.270 14.95 0.00 0.00 0.00 14.95 79.32
12-9-15 94.270 12.04 0.00 0.00 0.00 12.04 82.23
MW-13 03-18-09 94.805 13.58 0.00 0.00 0.00 13.58 81.23
06-23-09 94.805 11.01 0.00 0.00 0.00 11.01 83.80
09-9-09 94.805 12.61 0.00 0.00 0.00 12.61 82.20
12-3-09 94.805 11.26 0.00 0.00 0.00 11.26 83.55
Page 5 of 6
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
06-24-10 94.805 10.56 0.00 0.00 0.00 10.56 84.25
09-8-10 94.805 9.82 0.00 0.00 0.00 9.82 84.99
12-10-10 94.805 10.93 0.00 0.00 0.00 10.93 83.88
03-8-11 94.805 11.24 0.00 0.00 0.00 11.24 83.57
06-30-11 94.805 10.73 0.00 0.00 0.00 10.73 84.08
09-8-11 94.805 12.51 0.00 0.00 0.00 12.51 82.30
12-8-11 94.805 12.69 0.00 0.00 0.00 12.69 82.12
03-13-12 94.805 13.49 0.00 0.00 0.00 10.48 84.33
06-5-12 94.805 10.28 0.00 0.00 0.00 10.28 84.53
09-11-12 94.805 11.55 0.00 0.00 0.00 11.55 83.26
12-12-12 94.805 13.55 0.00 0.00 0.00 13.55 81.26
03-12-13 94.805 10.33 0.00 0.00 0.00 10.33 84.48
05-29-13 94.805 9.41 0.00 0.00 0.00 9.41 85.40
09-10-13 94.805 7.78 0.00 0.00 0.00 7.78 87.03
11-6-13 94.805 9.36 0.00 0.00 0.00 9.36 85.45
03-19-14 94.805 6.88 0.00 0.00 0.00 6.88 87.93
06-26-14 94.805 7.53 0.00 0.00 0.00 7.53 87.28
08-22-14 94.805 8.60 0.00 0.00 0.00 8.60 86.21
11-7-14 94.805 10.69 0.00 0.00 0.00 10.69 84.12
03-4-15 94.805 9.46 0.00 0.00 0.00 9.46 85.35
06-25-15 94.805 10.11 0.00 0.00 0.00 10.11 84.70
09-22-15 94.805 12.30 0.00 0.00 0.00 12.30 82.51
12-9-15 94.805 8.90 0.00 0.00 0.00 8.90 85.91
MW-14 03-18-09 94.395 NG 0.00 0.00 0.00 0.00 NG
06-23-09 94.395 NG 0.00 0.00 0.00 0.00 NG
09-9-09 94.395 NG 0.00 0.00 0.00 0.00 NG
12-3-09 94.395 NG 0.00 0.00 0.00 0.00 NG
03-24-10 94.395 NG 0.00 0.00 0.00 0.00 NG
06-24-10 94.395 NG 0.00 0.00 0.00 0.00 NG
09-8-10 94.395 NG 0.00 0.00 0.00 0.00 NG
12-10-10 94.395 NG 0.00 0.00 0.00 0.00 NG
03-8-11 94.395 NG 0.00 0.00 0.00 0.00 NG
06-30-11 94.395 NG 0.00 0.00 0.00 0.00 NG
09-8-11 94.395 NG 0.00 0.00 0.00 0.00 NG
12-8-11 94.395 NG 0.00 0.00 0.00 0.00 NG
03-13-12 94.395 NG 0.00 0.00 0.00 0.00 NG
06-5-12 94.395 NG 0.00 0.00 0.00 0.00 NG
09-11-12 94.395 NG 0.00 0.00 0.00 0.00 NG
12-12-12 94.395 NG 0.00 0.00 0.00 0.00 NG
03-12-13 94.395 NG 0.00 0.00 0.00 0.00 NG
05-29-13 94.395 NG 0.00 0.00 0.00 0.00 NG
09-10-13 94.395 NG 0.00 0.00 0.00 0.00 NG
11-6-13 94.395 NG 0.00 0.00 0.00 0.00 NG
03-19-14 94.395 NG 0.00 0.00 0.00 0.00 NG
06-26-14 94.395 NG 0.00 0.00 0.00 0.00 NG
08-22-14 94.395 NG 0.00 0.00 0.00 0.00 NG
11-7-14 94.395 NG 0.00 0.00 0.00 0.00 NG
03-4-15 94.395 NG 0.00 0.00 0.00 0.00 NG
06-25-15 94.395 NG 0.00 0.00 0.00 0.00 NG
09-22-15 94.395 NG 0.00 0.00 0.00 0.00 NG
12-9-15 94.395 NG 0.00 0.00 0.00 0.00 NG
MW-15/03-18-09 93.775 13.77 0.00 0.00 0.00 13.77 80.01
MW-15A 06-23-09 93.775 9.90 0.00 0.00 0.00 9.90 83.88
09-9-09 93.775 11.57 0.00 0.00 0.00 11.57 82.21
12-3-09 93.775 11.24 0.00 0.00 0.00 11.24 82.54
03-24-10 93.775 7.57 0.00 0.00 0.00 7.57 86.21
06-24-10 93.775 8.43 0.00 0.00 0.00 8.43 85.35
09-8-10 93.775 9.67 0.00 0.00 0.00 9.67 84.11
12-10-10 93.775 11.24 0.00 0.00 0.00 11.24 82.54
03-8-11 93.775 11.42 0.00 0.00 0.00 11.42 82.36
06-30-11 94.950 12.47 0.00 0.00 0.00 12.47 82.48
09-8-11 94.950 13.88 0.00 0.00 0.00 13.88 81.07
12-8-11 94.950 13.75 0.00 0.00 0.00 13.75 81.20
03-13-12 94.950 13.49 0.00 0.00 0.00 12.60 82.35
06-5-12 94.950 12.45 0.00 0.00 0.00 12.45 82.50
09-11-12 94.950 13.51 0.00 0.00 0.00 13.51 81.44
12-12-12 94.950 14.08 0.00 0.00 0.00 14.08 80.87
03-12-13 94.950 12.07 0.00 0.00 0.00 12.07 82.88
05-29-13 94.950 8.72 0.00 0.00 0.00 8.72 86.23
09-10-13 94.950 9.17 0.00 0.00 0.00 9.17 85.78
Page 6 of 6
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
03-19-14 94.950 8.33 0.00 0.00 0.00 8.33 86.62
MW-15A 06-26-14 94.950 7.78 0.00 0.00 0.00 7.78 87.17
08-22-14 94.950 9.14 0.00 0.00 0.00 9.14 85.81
11-7-14 94.950 11.24 0.00 0.00 0.00 11.24 83.71
03-4-15 94.950 11.40 0.00 0.00 0.00 11.40 83.55
06-25-15 94.950 10.88 0.00 0.00 0.00 10.88 84.07
09-22-15 94.950 13.81 0.00 0.00 0.00 13.81 81.14
12-9-15 94.950 9.28 0.00 0.00 0.00 9.28 85.67
*MW-5 depth inaccurate for this event as groundwater was seeping in at time of measurement.
1 of 4
PARAMETER UNITS DATE MW-1/MW-3 MW-4 MW-5 MW-6*MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/TS-1 NCAC 2L
MW-1A MW-15A Groundwater
Standard
Benzene ug/l 03-14-07 440 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 DNE DNE DNE NS 1
06-06-07 410 <1 <1 <1 3.6 <1 <1 <1 <1 <1 2.4 DNE DNE DNE NS
08-29-07 340 <1 <1 <1 2.6 <1 <1 <1 <1 <1 6.4 DNE DNE DNE NS
12-13-07 200 <1 <1 <1 1.1 <1 <1 <1 <1 <1 9.2 DNE DNE DNE NS03-14-08 250 <1 <1 <1 24 <1 <1 <1 <1 <1 130 DNE DNE DNE NS
06-18-08 310 <1 <1 <1 NS <1 <1 <1 <1 <1 5.3 DNE DNE DNE NS
09-10-08 <100 <1 <1 <1 11.6 <1 <1 <1 <1 <1 69.5 DNE DNE DNE NS
12-03-08 18 <0.5 <0.5 <0.5 8.7 32 <0.5 <0.5 <0.5 <0.5 41 DNE DNE DNE NS
03-18-09 110 <0.5 1.9 <0.5 <0.5 5.9 <0.5 <0.5 <0.5 <0.5 3.6 <0.5 NS 520 NS
06-23-09 290 <0.5 <0.5 <0.5 <0.5 0.66 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 210 NS
09-09-09 190 <0.5 <0.5 <0.5 <0.5 0.66 NS <0.5 <0.5 NS 5.1 <0.5 NS 910 NS
12-03-09 180 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 7.5 <0.5 NS 440 NS
03-24-10 120 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 55 NS
06-24-10 30 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 98 NS
09-08-10 69.7 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1.1 <0.5 NS 37.5 NS
12-10-10 140 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1.3 <0.5 NS 5.4 NS
03-08-11 120 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 52 NS
06-30-11 18.3 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 77.1 NS
09-08-11 22 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 1.7 <0.5 NS 462 NS
12-09-11 15.4 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 0.61 <0.5 NS 384 NS
03-14-12 20 ND ND ND ND ND NS ND ND ND 0.17J ND NS 290 NS06-07-12 28 ND ND ND ND ND ND NS ND ND ND ND NS 220 NS
9/11-12/12 30.1 ND ND ND ND ND ND NS ND ND 1.2 ND NS 132 NS
12-12-12 19 ND ND ND ND ND ND NS ND ND 0.81 ND NS 91 NS
03-14-13 20.4 ND ND ND ND NS NS NS ND ND ND ND NS 82.8 NS
05-30-13 0.83 ND ND ND ND NS NS ND ND ND ND ND NS ND NS
09-10-13 5.5 ND ND ND ND ND NS ND ND ND ND ND NS 4.4 NS
11-07-13 0.5 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-20-14 0.49 ND ND ND ND ND NS ND ND ND ND ND NS 0.29 NS06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 0.15 ND ND ND 0.15 ND NS ND ND ND ND ND NS ND NS
03-04-15 ND ND ND ND ND ND NS ND ND ND ND ND NS 1.1 NS
06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
9/22-23/15 1.2 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
12-09-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
Toluene ug/l 03-14-07 3200 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 600
06-06-07 5200 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
08-29-07 6300 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
12-13-07 3300 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-14-08 4400 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS06-18-08 5800 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
09-10-08 1850 <1 <1 <1 <1 <1 2.72 <1 <1 <1 <10 DNE DNE DNE NS
12-03-08 28 <1 <1 <1 <1 140 5.3 <1 <1 <1 <1 DNE DNE DNE NS
03-18-09 3200 <1 <1 <1 <1 50 2.9 <1 <1 <1 <1 <0.5 NS 12000 NS
06-23-09 5700 <1 <1 <1 <1 0.69J 2.9 <1 <1 <1 <1 <1 NS 17000 NS
09-09-09 4300 <1 <1 <1 <1 <1 NS <1 <1 NS <1 <1 NS 25000 NS
12-03-09 3900 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS 30000 NS
03-24-10 3100 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 1600 NS06-24-10 640 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 6900 NS
09-08-10 1090 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 1630 NS
12-10-10 3100 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 94 NS
03-08-11 1390 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 1940 NS
06-30-11 29.6 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 600 NS
09-08-11 2.1 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 5620 NS
12-09-11 5.9 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 <0.5 <0.5 NS 6820 NS
03-14-12 5.7 ND ND ND ND ND NS ND ND ND ND ND NS 7400 NS
06-07-12 8.2 ND ND ND ND ND ND NS ND ND ND ND NS 6300 NS
9/11-12/12 8.1 ND ND ND ND ND ND NS ND ND ND ND NS 3240 NS
12-12-12 3.3 ND ND ND ND ND ND NS ND ND ND ND NS 3300 NS
03-14-13 5.4 ND ND ND ND NS NS NS ND ND ND ND NS 1860 NS
05-30-13 ND ND ND ND ND NS NS ND ND ND ND ND NS 1.8 NS
09-10-13 7.2 ND ND ND ND ND NS ND ND ND ND ND NS 66.2 NS
11-07-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-20-14 0.31 ND ND ND ND ND NS ND ND ND ND ND NS 3 NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS08-22-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 0.12 0.11 ND ND ND ND NS ND ND ND ND ND NS 0.22 NS
03-04-15 ND ND ND ND ND ND NS ND ND ND ND ND NS 58 NS
06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
9/22-23/15 ND ND ND ND ND ND NS ND ND ND ND ND NS 19 NS
12-09-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
Ethylbenzene ug/l 03-14-07 66 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 600
06-06-07 550 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
08-29-07 760 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
12-13-07 620 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-14-08 580 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
06-18-08 730 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
09-10-08 228 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 DNE DNE DNE NS
12-03-08 21 <1 <1 <1 <1 11 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-18-09 280 <1 <1 <1 <1 16 <1 <1 <1 <1 <1 6.3 NS 930 NS
06-23-09 870 <1 <1 <1 <1 2.5 <1 <1 <1 <1 <1 <1 NS 3000 NS
09-09-09 830 <1 <1 <1 <1 2.1 NS <1 <1 NS <1 <1 NS 2300 NS
12-03-09 990 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS 2700 NS
03-24-10 720 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 160 NS
06-24-10 250 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 1300 NS09-08-10 625 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 215 NS
12-10-10 700 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 5.1 NS
03-08-11 307 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 198 NS
06-30-11 19.7 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 140 NS
09-08-11 41.9 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 1550 NS
12-09-11 11.8 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 <0.5 <0.5 NS 1740 NS
03-14-12 11 ND ND ND ND ND NS ND ND ND ND ND NS 2200 NS
06-07-12 15 ND ND ND ND ND ND NS ND ND ND ND NS 1900 NS9/11-12/12 22.5 ND ND ND ND ND ND NS ND ND ND ND NS 1620 NS
12-12-12 21 ND ND ND ND ND ND NS ND ND ND ND NS 1600 NS
03-14-13 13.8 ND ND ND ND NS NS NS ND ND ND ND NS 1440 NS
05-30-13 0.58 ND ND ND ND NS NS ND ND ND ND ND NS 1.7 NS
09-10-13 7.3 ND ND ND ND ND NS ND ND ND ND ND NS 76.8 NS
11-07-13 1.6 ND ND ND ND ND NS ND ND ND ND ND NS 0.88 NS
03-20-14 1.1 ND ND ND ND ND NS ND ND ND ND ND NS 8 NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 0.16 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 ND ND ND ND ND ND NS ND ND ND ND ND NS 0.32 NS
03-04-15 ND ND ND ND ND ND NS ND ND ND ND ND NS 120 NS
06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
9/22-23/15 0.53 ND ND ND ND ND NS ND ND ND ND ND NS 16 NS
12-09-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
TABLE 3
Monitoring Well Analytical Results
Incident #12913
Harold Smith Grocery
Union Ridge Road, Burlington, North Carolina
2 of 4
PARAMETER UNITS DATE MW-1/MW-3 MW-4 MW-5 MW-6*MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/TS-1 NCAC 2L
MW-1A MW-15A Groundwater
Standard
TABLE 3
Monitoring Well Analytical Results
Incident #12913
Harold Smith Grocery
Union Ridge Road, Burlington, North Carolina
Total Xylenes ug/l 03-14-07 5700 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 DNE DNE DNE NS 500
06-06-07 7000 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 DNE DNE DNE NS
08-29-07 9600 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 DNE DNE DNE NS
12-13-07 5600 <3 <3 <3 <3 <3 <3 <3 <3 <3 27 DNE DNE DNE NS
03-14-08 6200 <3 <3 <3 <3 <3 <3 <3 <3 <3 16 DNE DNE DNE NS
06-18-08 7800 <3 <3 <3 NS <3 <3 <3 <3 <3 12 DNE DNE DNE NS
09-10-08 2377 <4 <4 <4 <4 <4 <4 <4 <4 <4 <40 DNE DNE DNE NS
12-03-08 610 <3 <3 <3 <3 1810 <3 <3 <3 <3 15 DNE DNE DNE NS
03-18-09 5500 <3 <3 <3 <3 2020 <3 13.6 <3 <3 4.7 2.3 NS 7000 NS
06-23-09 9300 <3 <3 <3 <3 71 <3 <3 <3 <3 <3 <3 NS 22400 NS
09-09-09 8700 <3 <3 <3 <3 30.1 NS <3 <3 NS 3.4 <3 NS 19300 NS
12-03-09 9300 <3 <3 <3 <3 <3 <3 <3 <3 NS 5.8 <3 NS 21200 NS
03-24-10 7800 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 NS 2600 NS06-24-10 2700 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 NS 11100 NS
09-08-10 5720 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 NS 3790 NS
12-10-10 9700 NS NS <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 0.61 <1.5 NS 162 NS
03-08-11 5700 <1.5 <1.5 <1.5 <1.5 0.66 <1.5 <1.5 <1.5 <1.5 0.82 <1.5 NS 2124 NS
06-30-11 213.2 <1.5 <1.5 <1.5 <1.5 0.66 NS NS <1.5 <1.5 5.8 <1.5 NS 602 NS
09-08-11 42.4 <1.5 <1.5 <1.5 <1.5 0.66 NS NS <1.5 <1.5 11.6 <1.5 NS 3990 NS
12-09-11 48 <1.5 <1.5 <1.5 <1.5 <1.5 NS <1.5 <1.5 <1.5 0.66 <1.5 NS 5680 NS
03-14-12 44 ND ND ND ND ND NS ND ND ND ND ND NS 8300 NS06-07-12 60 ND ND ND ND ND ND NS ND ND ND ND NS 7400 NS
9/11-12/12 73.9 ND ND ND ND ND ND NS ND ND ND ND NS 5940 NS
12-12-12 28 ND ND ND ND ND ND NS ND ND ND ND NS 7400 NS
03-14-13 44 ND ND ND ND NS NS NS ND ND ND ND NS 5600 NS
05-30-13 1.94 ND ND ND ND NS NS ND ND ND ND ND NS 7.7 NS
09-10-13 83.1 ND ND ND ND ND NS ND ND ND ND ND NS 470 NS
11-07-13 4.5 ND ND ND ND ND NS ND ND ND ND ND NS 3.76 NS
03-20-14 5.6 ND ND ND ND ND NS ND ND ND ND ND NS 32.2 NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 1.13 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 0.27 0.23 ND 0.19 0.22 0.19 NS ND ND ND ND ND NS 1.37 NS
03-04-15 3.2 ND ND ND ND ND NS ND ND ND ND ND NS 570 NS
06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
9/22-23/15 22.3 ND ND ND ND ND NS ND ND ND ND ND NS 250 NS
12-09-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
TOTAL BTEX ug/l 03-14-07 9406 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL DNE DNE DNE NS N/A
06-06-07 13160 BDL BDL BDL 3.6 BDL BDL BDL BDL BDL 2.4 DNE DNE DNE NS
08-29-07 17000 BDL BDL BDL 2.6 BDL BDL BDL BDL BDL 6.4 DNE DNE DNE NS
12-13-07 9720 BDL BDL BDL BDL BDL BDL BDL BDL BDL 36.2 DNE DNE DNE NS
03-14-08 11430 BDL BDL BDL 24 BDL BDL BDL BDL BDL 146 DNE DNE DNE NS06-18-08 14640 BDL BDL BDL NS BDL BDL BDL BDL BDL 17.3 DNE DNE DNE NS
09-10-08 4455 BDL BDL BDL 11.6 BDL 2.72 BDL BDL BDL 69.5 DNE DNE DNE NS
12-03-08 677 BDL BDL BDL 8.7 1993 5.3 BDL BDL BDL 56 DNE DNE DNE NS
03-18-09 9090 BDL 1.9 BDL BDL 2091.9 2.9 13.6 BDL BDL 8.3 8.6 NS 20450 NS
06-23-09 16160 BDL BDL BDL BDL 74.16 2.9 BDL BDL BDL BDL BDL NS 42610 NS
09-09-09 14020 BDL BDL BDL BDL 32.86 NS BDL BDL NS 8.5 BDL NS 47510 NS
12-03-09 14370 BRL BRL BRL BRL BRL BRL BRL BRL NS 13.3 BRL NS 54340 NS
03-24-10 11740 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS 4415 NS
06-24-10 3620 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS 19398 NS
09-08-10 7504.7 BRL BRL BRL BRL BRL BRL BRL BRL BRL 1.1 BRL NS 5672.5 NS
12-10-10 13640 NS NS BRL BRL BRL BRL BRL BRL BRL 1.91 BRL NS 266.5 NS
03-08-11 7517 ND ND ND ND 0.66 ND ND ND ND 0.82 ND NS 4314 NS
06-30-11 280.8 ND ND ND ND 0.66 NS NS ND ND 5.8 ND NS 1419.1 NS
09-08-11 108.4 ND ND ND ND 0.66 NS NS ND ND 13.3 ND NS 11622 NS
12-09-11 81.1 ND ND ND ND ND NS ND ND ND 1.27 ND NS 14624 NS
03-14-12 80.7 ND ND ND ND ND NS ND ND ND ND ND NS 18190 NS
06-07-12 111.2 ND ND ND ND ND ND NS ND ND ND ND NS 15820 NS9/11-12/12 134.6 ND ND ND ND ND ND NS ND ND 1.2 ND NS 10932 NS
12-12-12 71.3 ND ND ND ND 0.2 ND NS ND ND 0.81 ND NS 12391 NS
03-14-13 83.6 ND ND ND ND NS NS NS ND ND ND ND NS 8982.8 NS
05-30-13 3.35 ND ND ND ND NS NS ND ND ND ND ND NS 11.2 NS
09-10-13 103.1 ND ND ND ND ND NS ND ND ND ND ND NS 617.4 NS
11-07-13 6.6 ND ND ND ND ND NS ND ND ND ND ND NS 4.64 NS
03-20-14 7.19 ND ND ND ND ND NS ND ND ND ND ND NS 40.49 NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS08-22-14 1.29 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 0.54 0.34 ND 0.19 0.37 0.19 NS ND ND ND ND ND NS 1.91 NS
03-04-15 3.2 ND ND ND ND ND NS ND ND ND ND ND NS 749.1 NS
06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
9/22-23/15 24.03 ND ND ND ND ND NS ND ND ND ND ND NS 285 NS
12-09-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
Methyl Tertiary ug/l 03-14-07 <50 <5 10 <5 4.3J <5 <5 <5 <5 <5 2.7J DNE DNE DNE NS 20Butyl Ether 06-06-07 <50 19 7.5 <5 5.9 <5 4.9J <5 <5 <5 4.1J DNE DNE DNE NS
(MTBE)08-29-07 <50 73 4.6J <5 7.1 <5 <5 <5 <5 <5 4.1J DNE DNE DNE NS
12-13-07 <50 97 20 <5 8.5 <5 <5 <5 <5 <5 13 DNE DNE DNE NS
03-14-08 <50 10 6.9 <5 16 <5 <5 <5 <5 <5 74 DNE DNE DNE NS
06-18-08 <50 26 27 <5 NS <5 <5 <5 <5 <5 15 DNE DNE DNE NS09-10-08 <200 2.3 <2 <2 6.39 <2 <2 <2 <2 <2 38.1 DNE DNE DNE NS
12-03-08 <5 2.8J 8.9 <5 9.3 5.1 <5 <5 <5 <5 75 DNE DNE DNE NS
03-18-09 <50 <5 <5 <5 <5 8.2 <5 8.3 <5 <5 25 <0.5 NS <50 NS
06-23-09 <50 <5 5.4 <5 <5 3.3J <5 <5 <5 <5 11 <5 NS <50 NS
09-09-09 <50 <5 7.7 <5 <5 2.6J NS <5 <5 NS 44 <5 NS <200 NS
12-03-09 <50 <5 4J <5 <5 <5 <5 <5 <5 NS 92 <5 NS <200 NS
03-24-10 <50 <5 13 <5 <5 <5 <5 <5 <5 <5 3.3J <5 NS <200 NS
06-24-10 <50 <1 4.2 <1 <1 1.5 <1 <1 <1 <1 13 <1 NS <40 NS09-08-10 <2.5 <0.5 1.7 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 45.8 <0.5 NS <5 NS
12-10-10 <10 NS NS <1 <1 <1 <1 <1 <1 <1 57 <1 NS <1 NS
03-08-11 <10 <0.5 1.6 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 19.1 <0.5 NS <10 NS
06-30-11 2.7 <0.5 0.83 <0.5 <0.5 <0.5 NS NS 0.51 <0.5 23.8 <0.5 NS <0.5 NS
09-08-11 12.3 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS 0.54 <0.5 54.7 <0.5 NS 2.9 NS
12-09-11 9.2 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 0.52 <0.5 28.5 <0.5 NS <25 NS
03-14-12 9.6 ND 0.5 ND 0.25J ND NS ND 0.84 ND 10 ND NS ND NS
06-07-12 ND ND ND ND ND ND ND NS 1.7 ND 15 ND NS ND NS
9/11-12/12 21.4 ND ND ND ND ND ND NS 2.2 ND 33.8 ND NS ND NS
12-12-12 21 ND ND ND 0.19J ND ND NS 0.32J ND 24 ND NS ND NS
03-14-13 21.3 ND ND ND ND NS NS NS ND ND 8.4 ND NS ND NS
05-30-13 9.4 ND ND ND ND NS NS ND 0.8 ND 2 ND NS 0.61 NS
09-10-13 14.4 ND ND ND ND ND NS ND 2.9 ND 1.9 ND NS ND NS
11-07-13 9.4 ND ND ND ND ND NS ND 2.2 ND 1.2 ND NS ND NS
03-20-14 8.6 ND 0.35 ND 0.16 ND NS 1.1 0.12 ND 1.8 ND NS 0.2 NS
06-26-14 0.25 ND 0.32 ND 0.53 0.24 NS 0.3 3.2 ND 0.66 ND NS ND NS
08-22-14 4.1 ND ND ND ND ND NS 0.25 1.3 ND 0.57 ND NS ND NS11-07-14 0.79 ND ND ND ND ND NS 1.4 1.5 ND 0.46 ND NS ND NS
03-04-15 4.6 ND ND ND 0.60J ND NS 1.6 ND ND 0.80J ND NS ND NS
06-25-15 3.9 ND ND ND 0.75J ND NS ND 0.67J ND 0.68J ND NS ND NS
9/22-23/15 6.2 ND ND ND 1 ND NS ND ND ND ND ND NS ND NS
12-09-15 1.7 ND ND ND 1.9 ND NS ND ND ND ND ND NS ND NS
3 of 4
PARAMETER UNITS DATE MW-1/MW-3 MW-4 MW-5 MW-6*MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/TS-1 NCAC 2L
MW-1A MW-15A Groundwater
Standard
TABLE 3
Monitoring Well Analytical Results
Incident #12913
Harold Smith Grocery
Union Ridge Road, Burlington, North Carolina
Ethylene ug/l 03-14-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 0.02
Dibromide 06-06-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
(EDB)08-29-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
12-13-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-14-08 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
06-18-08 <10 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
09-10-08 <2 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 DNE DNE DNE NS
12-03-08 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-18-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <0.5 NS <50 NS
06-23-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS <50 NS
09-09-09 <10 <1 <1 <1 <1 <1 NS <1 <1 NS <1 <1 NS <40 NS
12-03-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS <40 NS
03-24-10 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS <40 NS06-24-10 14 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 28 NS
09-08-10 <2.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS <5 NS
12-10-10 <5 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 3.9 NS
03-08-11 <10 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS <10 NS
06-30-11 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 1.9 NS
09-08-11 <1.2 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 7 NS
12-09-11 <1 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 <0.5 <0.5 NS <25 NS
03-14-12 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS06-07-12 ND ND ND ND ND ND ND NS ND ND ND ND NS ND NS
9/11-12/12 ND ND ND ND ND ND ND NS ND ND ND ND NS ND NS
12-12-12 ND ND ND ND ND ND ND NS ND ND ND ND NS ND NS
03-14-13 ND ND ND ND ND NS NS NS ND ND ND ND NS ND NS
05-30-13 ND ND ND ND ND NS NS ND ND ND ND ND NS ND NS
09-10-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-20-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-04-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
9/22-23/15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
12-09-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
Isopropyl Ether ug/l 03-14-08 86 <5 3J <5 9.9 <5 <5 <5 <5 <5 270 DNE DNE DNE NS 70(IPE)06-18-08 <50 <5 13 <5 NS <5 <5 <5 <5 <5 19 DNE DNE DNE NS
09-10-08 <100 <1 <1 <1 9.28 <1 <1 <1 <1 <1 221 DNE DNE DNE NS
12-03-08 15 <5 4.6J <5 6.9 23 <5 8.1 <5 <5 200 DNE DNE DNE NS
03-18-09 <50 <5 <5 <5 <5 19 <5 10 <5 <5 69 <0.5 NS <50 NS06-23-09 <50 <5 <5 <5 <5 6.2 <5 <5 <5 <5 10 <5 NS <50 NS
09-09-09 <50 <5 3.3J <5 <5 4.9J NS <5 <5 NS 73 <5 NS <200 NS
12-03-09 <50 <5 <5 <5 <5 <5 <5 <5 <5 NS 180 <5 NS <200 NS
03-24-10 <50 <5 5.9 <5 <5 <5 <5 <5 <5 <5 3.2J <5 NS <200 NS
06-24-10 <5 <0.5 1.8 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 12 <0.5 NS <20 NS
09-08-10 2.9 <0.5 0.66 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 35.9 <0.5 NS <5 NS
12-10-10 6 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 49 <0.5 NS 1.3 NS
03-08-11 <10 <0.5 <0.5 <0.5 <0.5 0.56 <0.5 <0.5 0.82 <0.5 24.6 <0.5 NS <10 NS
06-30-11 13 <0.5 <0.5 <0.5 <0.5 0.56 NS NS 1.2 <0.5 29.2 <0.5 NS 2.7 NS
09-08-11 62.2 <0.5 <0.5 <0.5 <0.5 0.56 NS NS 0.73 <0.5 55.2 <0.5 NS 22.5 NS
12-09-11 40.9 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 29.1 <0.5 NS <25 NS
03-14-12 47 ND ND ND ND ND NS ND 0.17J ND 11 ND NS ND NS
06-07-12 78 ND ND ND ND ND ND NS 0.52J ND 12 ND NS 15J NS
9/11-12/12 94.8 ND ND ND ND ND ND NS 1.6 ND 29.8 ND NS 13.5 NS
12-12-12 120 ND ND ND 0.16J ND ND NS 1.6 ND 26 ND NS ND NS
03-14-13 112 ND ND ND ND NS NS NS ND ND 10.2 ND NS ND NS
05-30-13 32.5 ND ND ND ND NS NS 3.1 1.5 ND ND ND NS 1.5 NS09-10-13 80.7 ND ND ND ND ND NS 3.1 6.9 ND ND ND NS 7.2 NS
11-07-13 42.2 ND ND ND ND ND NS ND 3.1 1.9 ND ND NS 0.79 NS
03-20-14 46 ND ND ND 0.2 ND NS ND 3.1 1.9 0.34 ND NS 1.5 NS
06-26-14 ND ND ND ND 1.4 ND NS ND 3.3 3.1 ND ND NS ND NS
08-22-14 11 ND ND ND 0.24 ND NS ND 2.1 3.1 ND ND NS ND NS
11-07-14 2 ND ND ND ND ND NS ND 1.1 ND ND ND NS ND NS
03-04-15 27 ND ND ND ND ND NS ND ND ND 0.5 ND NS ND NS
06-25-15 11 ND ND ND ND ND NS ND 0.59 ND ND ND NS ND NS9/22-23/15 32 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
12-09-15 6 ND ND ND ND ND NS ND ND 1.9 ND ND NS ND NS
1,2-Dichloroethane ug/l 03-14-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 0.4
06-06-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
08-29-07 <10 <1 <1 <1 <1 <1 <1 <1 1.4 <1 1.3 DNE DNE DNE NS
12-13-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 1.5 DNE DNE DNE NS
03-14-08 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 31 DNE DNE DNE NS
06-18-08 <10 <1 1.3 <1 NS <1 <1 <1 <1 <1 2.8 DNE DNE DNE NS
09-10-08 <2 <1 <1 <1 <1 <1 <1 <1 <1 <1 29.3 DNE DNE DNE NS
12-03-08 <1 <1 <1 <1 <1 4 <1 0.76J <1 <1 30 DNE DNE DNE NS
03-18-09 <10 <1 <1 <1 <1 2.1 <1 1.5 <1 <1 4.5 <0.5 NS <50 NS
06-23-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 0.69J <1 NS <50 NS09-09-09 <10 <1 <1 <1 <1 0.64J NS <1 <1 NS 8.6 <1 NS <40 NS
12-03-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 NS 13 <1 NS <40 NS
03-24-10 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS <40 NS
06-24-10 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 2.8 <0.5 <0.5 NS <20 NS
09-08-10 <2.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 6.9 <0.5 NS <5 NS
12-10-10 <5 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 11 <0.5 NS <0.5 NS
03-08-11 <10 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 7.1 <0.5 NS <10 NS
06-30-11 1.1 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 9.1 <0.5 NS 0.58 NS09-08-11 4.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 10.9 <0.5 NS 4 NS
12-09-11 4.1 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 7.1 <0.5 NS <25 NS
03-14-12 ND ND ND ND ND ND NS ND 0.33J ND 3.6 ND NS ND NS
06-07-12 ND ND ND ND ND ND ND NS ND ND 4 ND NS ND NS
9/11-12/12 13.7 ND ND ND ND ND ND NS 0.67 ND 5.9 ND NS ND NS
12-12-12 15 ND ND ND ND ND ND NS ND ND 0.81 ND NS 4.9 NS
03-14-13 14.2 ND ND ND ND NS NS NS 0.72 ND 3.3 ND NS ND NS
05-30-13 4.2 ND ND ND ND NS NS ND 1.1 ND 0.53 ND NS ND NS
09-10-13 9.2 ND ND ND ND ND NS ND 2.4 ND 0.51 ND NS 0.6 NS
11-07-13 4.1 ND ND ND ND ND NS ND 2.2 ND ND ND NS ND NS
03-20-14 4.8 ND ND ND 0.23 ND NS ND 3.2 ND ND ND NS ND NS
06-26-14 ND ND ND ND 0.32 ND NS ND 1.4 0.63 ND ND NS ND NS
08-22-14 2 ND ND ND ND ND NS ND 1.2 0.84 ND ND NS ND NS
11-07-14 ND ND ND ND ND ND NS ND 0.69 ND ND ND NS ND NS
03-04-15 2.7 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
06-25-15 1.6 ND ND ND ND ND NS ND ND 0.53 ND ND NS ND NS
9/22-23/15 3.7 ND ND ND ND ND NS ND ND ND ND ND NS ND NS12-09-15 1.2 ND ND ND ND ND NS ND ND 0.61 ND ND NS ND NS
4 of 4
PARAMETER UNITS DATE MW-1/MW-3 MW-4 MW-5 MW-6*MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/TS-1 NCAC 2L
MW-1A MW-15A Groundwater
Standard
TABLE 3
Monitoring Well Analytical Results
Incident #12913
Harold Smith Grocery
Union Ridge Road, Burlington, North Carolina
Naphthalene ug/l 03-14-08 470 <1 <1 <1 <1 <1 <1 <1 <1 <1 4.5 DNE DNE DNE NS 6
06-18-08 590 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
09-10-08 136 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 DNE DNE DNE NS
12-03-08 31 <1 <1 <1 <1 <1 <1 <1 <1 <1 3.5 DNE DNE DNE NS
03-18-09 250 <1 1.9 <1 <1 <1 <1 1.6 <1 <1 <1 6.2 NS 490 NS
06-23-09 470 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 950 NS
09-09-09 540 <1 <1 <1 <1 <1 NS <1 <1 NS <1 <1 NS 680 NS
12-03-09 490 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS 750 NS
03-24-10 550 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 220 NS
06-24-10 680 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 580 NS
09-08-10 736 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 NS 255 NS
12-10-10 520 NS NS <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 7.1 NS
03-08-11 337 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 NS 118 NS06-30-11 54.1 <2 <2 <2 <2 <2 NS NS <2 <2 3 <2 NS 41.6 NS
09-08-11 154 <2 <2 <2 <2 <2 NS NS <2 <2 5.9 <2 NS 395 NS
12-09-11 112 <2 <2 <2 <2 <2 NS <2 <2 <2 <2 <2 NS 504 NS
03-14-12 87 ND ND ND ND ND NS ND ND ND ND ND NS 130J NS
06-07-12 84 ND ND ND ND ND ND NS ND ND ND ND NS 150 NS
9/11-12/12 197 ND ND ND ND ND ND NS ND ND ND ND NS 515 NS
12-12-12 99 ND ND ND ND ND ND NS ND ND ND ND NS 250 NS
03-14-13 84.6 ND ND ND ND NS NS NS ND ND ND ND NS 344 NS05-30-13 3.4 ND ND ND ND NS NS ND ND ND ND ND NS ND NS
09-10-13 18 ND ND ND ND ND NS ND ND ND ND ND NS 2.3 NS
11-07-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-20-14 2.5 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 0.66 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-04-15 0.73J ND ND ND ND ND NS ND ND ND ND ND NS 33 NS
06-25-15 0.99J ND ND ND ND ND NS ND ND ND ND ND NS ND NS
9/22-23/15 3.2 ND ND ND ND ND NS ND ND ND ND ND NS 16 NS
12-09-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
NA=Not Analyzed for Parameter DNE=Did Not Exist Bold Values exceed the NCAC 2L Groundwater StandardNS=Not Sampled BDL=Below Detection Limits ND=Not Detected
Page 1 of 2
PARAMETER UNITS DATE NCAC 15A:2L 2768B 2774 2760 2773 2755 2761 2779 2765 2765 2765 2800 Groundwater
Influent Midfluent Effluent Standard
Benzene ug/l 03-24-10 <0.5 NS NS NS NS NS NS 1.7 <0.5 <0.5 NS06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS09-08-10 NS NS NS <0.5 NS NS NS 1 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS 0.97 <0.5 <0.5 NS 103-08-11 NS NS NS <0.5 NS NS <0.5 1.6 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 8.4 <0.5 <0.5 NS09-08-11 NS NS NS <0.5 NS NS <0.5 7.1 <0.5 <0.5 NS12-09-11 NS NS NS <0.5 NS NS <0.5 3.3 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS12-12-12 NS NS NS ND NS NS ND ND NS ND NS03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND ND NS ND NS09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS09-20-14 ND NS NS ND NS NS ND ND ND ND NS06-26-14 ND NS ND ND NS NS ND 0.33 ND ND NS
08-22-14 ND NS ND ND NS NS ND 0.54 ND ND NS11-07-14 ND NS ND ND NS NS ND ND ND ND NS
03-04-15 NS NS ND ND NS NS ND ND ND ND NS06-25-15 ND NS ND ND NS NS ND ND ND ND NS09-23-15 ND NS ND ND NS NS ND ND ND ND NS
12-09-15 ND NS ND ND NS NS ND ND ND ND NS
Toluene ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 60003-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS12-12-12 NS NS NS ND NS NS ND ND NS ND NS03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND ND NS ND NS09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS03-20-14 ND NS NS ND NS NS ND ND ND ND NS06-26-14 ND NS ND ND NS NS ND ND ND ND NS
08-22-14 ND NS ND ND NS NS ND ND ND ND NS11-07-14 ND NS ND ND NS NS ND ND ND ND NS
03-04-15 NS NS ND ND NS NS ND ND ND ND NS06-25-15 ND NS ND ND NS NS ND ND ND ND NS09-23-15 ND NS ND ND NS NS ND ND ND ND NS
12-09-15 ND NS ND ND NS NS ND ND ND ND NS
Ethylbenzene ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 60003-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND 0.55 NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS
03-20-14 ND ND ND ND NS NS ND ND ND ND NS06-26-14 ND NS ND ND NS NS ND ND ND ND NS
08-22-14 ND NS ND ND NS NS ND 0.26 ND ND NS11-07-14 ND NS ND ND NS NS ND ND ND ND NS03-04-15 NS NS ND ND NS NS ND ND ND ND NS06-25-15 ND NS ND ND NS NS ND ND ND ND NS09-23-15 ND NS ND ND NS NS ND ND ND ND NS
12-09-15 ND NS ND ND NS NS ND ND ND ND NS
Total Xylenes ug/l 03-24-10 <3 NS NS NS NS NS NS <3 <3 <3 NS06-24-10 NS NS NS <1.5 NS NS NS <1.5 <1.5 <1.5 NS09-08-10 NS NS NS <1.5 NS NS NS <1.5 <1.5 <1.5 NS
12-10-10 NS NS NS <1.5 NS NS NS <1.5 <1.5 <1.5 NS 50003-08-11 NS NS NS <1.5 NS NS <1.5 <1.5 <1.5 <1.5 NS06-30-11 NS NS NS <1.5 NS NS <1.5 <3 <1.5 <1.5 NS09-08-11 NS NS NS <1.5 NS NS <1.5 <3 <1.5 <1.5 NS12-09-11 NS NS NS <1.5 NS NS <1.5 <3 <1.5 <1.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS12-12-12 NS NS NS ND NS NS ND ND NS ND NS03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND ND NS ND NS09-10-13 ND NS NS ND NS NS ND ND NS ND NS11-07-13 ND NS NS ND NS NS ND ND NS ND NS03-20-14 ND ND ND ND NS NS ND ND ND ND NS06-26-14 ND NS ND ND NS NS ND ND ND ND NS
08-22-14 ND NS ND ND NS NS ND ND ND ND NS11-07-14 ND NS ND ND NS NS ND ND ND ND NS03-04-15 NS NS ND ND NS NS ND ND ND ND NS06-25-15 ND NS ND ND NS NS ND ND ND ND NS09-23-15 ND NS ND ND NS NS ND ND ND ND NS
12-09-15 ND NS ND ND NS NS ND ND ND ND NS
TOTAL BTEX ug/l 03-24-10 BDL NS NS NS NS NS NS 1.7 BDL BDL NS06-24-10 NS NS NS BDL NS NS NS BDL BDL BDL NS09-08-10 NS NS NS BDL NS NS NS 1 BDL BDL NS
12-10-10 NS NS NS BDL NS NS NS 0.97 <0.5 <0.5 NS N/A03-08-11 NS NS NS BDL NS NS BDL 1.6 BDL BDL NS06-30-11 NS NS NS BDL NS NS BDL 8.4 BDL BDL NS09-08-11 NS NS NS BDL NS NS BDL 7.1 BDL BDL NS12-09-11 NS NS NS BDL NS NS BDL 3.3 BDL BDL NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS12-12-12 NS NS NS ND NS NS ND ND NS ND NS03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND 0.55 NS ND NS09-10-13 ND NS NS ND NS NS ND ND NS ND NS11-07-13 ND NS NS ND NS NS ND ND NS ND NS03-20-14 ND ND ND ND NS NS ND ND ND ND NS06-26-14 ND NS ND ND NS NS ND 0.33 ND ND NS
08-22-14 ND NS ND ND NS NS ND 0.8 ND ND NS11-07-14 ND NS ND ND NS NS ND ND ND ND NS03-04-15 NS NS ND ND NS NS ND ND ND ND NS06-25-15 ND NS ND ND NS NS ND ND ND ND NS09-23-15 ND NS ND ND NS NS ND ND ND ND NS
12-09-15 ND NS ND ND NS NS ND ND ND ND NS
Methyl Tertiary ug/l 03-24-10 22 NS NS NS NS NS NS 98 <5 <5 NSButyl Ether 06-24-10 NS NS NS <1 NS NS NS <1 <1 <1 NS(MTBE)09-08-10 NS NS NS <1 NS NS NS 84.8 <1 <1 NS
12-10-10 NS NS NS <1 NS NS NS 100 <1 <1 NS 2003-08-11 NS NS NS <0.5 NS NS <0.5 166 <0.5 <0.5 NS06-30-11 NS NS NS <0.5 NS NS <0.5 125 <0.5 <0.5 NS09-08-11 NS NS NS <0.5 NS NS <0.5 136 <0.5 <0.5 NS12-09-11 NS NS NS <0.5 NS NS <0.5 150 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS9/11-12/2012 NS NS NS ND NS NS ND 149 NS ND NS12-12-12 NS NS NS ND NS NS ND 140 NS ND NS03-14-13 ND NS NS ND NS NS ND 157 NS ND NS
05-29-13 ND NS NS ND NS NS ND 150 NS ND NS09-10-13 ND NS NS ND NS NS ND 128 NS ND NS11-07-13 ND NS NS ND NS NS ND 117 NS ND NS03-20-14 ND ND ND 0.81 NS NS ND 140 ND 0.62 NS06-26-14 ND NS ND 0.23 NS NS ND 120 ND ND NS
08-22-14 ND NS ND 0.18 NS NS ND 120 ND 0.28 NS11-07-14 ND NS ND ND NS NS ND 130 ND ND NS03-04-15 NS NS ND 0.79J NS NS ND 80 ND ND NS06-25-15 ND NS ND 0.57J NS NS ND 57 ND ND NS09-23-15 ND NS ND ND NS NS ND 70 ND ND NS
12-09-15 ND NS ND 3.1 NS NS ND 53 ND ND NS
SUPPLY WELL
Union Ridge Road, Burlington, North Carolina
TABLE 4
Water Supply Well Analytical Results
Harold Smith GroceryIncident #12913
Page 2 of 2
PARAMETER UNITS DATE NCAC 15A:2L 2768B 2774 2760 2773 2755 2761 2779 2765 2765 2765 2800 Groundwater
Influent Midfluent Effluent Standard
SUPPLY WELL
Union Ridge Road, Burlington, North Carolina
TABLE 4
Water Supply Well Analytical Results
Harold Smith GroceryIncident #12913
Ethylene ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NSDibromide06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS(EDB)09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 0.0203-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS12-12-12 NS NS NS ND NS NS ND ND NS ND NS03-14-13 ND NS NS ND NS NS ND ND NS ND NS05-29-13 ND NS NS ND NS NS ND ND NS ND NS09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS03-20-14 ND ND ND ND NS NS ND ND ND ND NS06-26-14 ND NS ND ND NS NS ND ND ND ND NS08-22-14 ND NS ND ND NS NS ND ND ND ND NS11-07-14 ND NS ND ND NS NS ND ND ND ND NS
03-04-15 ND NS ND ND NS NS ND ND ND ND NS06-25-15 ND NS ND ND NS NS ND ND ND ND NS09-23-15 ND NS ND ND NS NS ND ND ND ND NS12-09-15 ND NS ND ND NS NS ND ND ND ND NS
Isopropyl Ether ug/l 03-24-10 11 NS NS NS NS NS NS 130 <5 <5 NS(IPE)06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS09-08-10 NS NS NS <0.5 NS NS NS 104 <0.5 <0.5 NS12-10-10 NS NS NS <0.5 NS NS NS 150 <0.5 <0.5 NS 7003-08-11 NS NS NS <0.5 NS NS <0.5 260 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 191 <0.5 <0.5 NS09-08-11 NS NS NS <0.5 NS NS <0.5 206 <0.5 NS12-09-11 NS NS NS <0.5 NS NS <0.5 178 <0.5 <0.5 NS03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND 149 NS ND NS12-12-12 NS NS NS ND NS NS ND 150 NS ND NS03-14-13 ND NS NS ND NS NS ND 159 NS ND NS05-29-13 ND NS NS ND NS NS ND 168 NS ND NS09-10-13 ND NS NS 0.96 NS NS ND 183 NS ND NS
11-07-13 ND NS NS 1.96 NS NS ND 138 NS ND NS03-20-14 ND ND ND 0.67 NS NS ND 140 ND 0.2 NS06-26-14 ND NS ND ND NS NS ND 160 ND ND NS08-22-14 ND NS ND ND NS NS ND 150 ND ND NS11-07-14 ND NS ND ND NS NS ND 160 ND ND NS
03-04-15 NS NS ND ND NS NS ND 100 ND ND NS06-25-15 ND NS ND ND NS NS ND 68 ND ND NS09-23-15 ND NS ND ND NS NS ND 74 ND ND NS12-09-15 ND NS ND 2.2 NS NS ND 75 ND ND NS
1,2- Dichloroethane ug/l 03-24-10 <1 NS NS NS NS NS NS 6.2 <1 <1 NS06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS09-08-10 NS NS NS <0.5 NS NS NS 15.7 <0.5 <0.5 NS12-10-10 NS NS NS <0.5 NS NS NS 19 <0.5 <0.5 NS 0.403-08-11 NS NS NS <0.5 NS NS <0.5 33.1 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 28 <0.5 <0.5 NS09-08-11 NS NS NS <0.5 NS NS <0.5 27.4 <0.5 <0.5 NS12-09-11 NS NS NS <0.5 NS NS <0.5 26.6 <0.5 <0.5 NS03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND 20.8 NS ND NS12-12-12 NS NS NS 0.19J NS NS ND 23 NS ND NS03-14-13 ND NS NS ND NS NS ND 31.5 NS ND NS05-29-13 ND NS NS ND NS NS ND 25.9 NS ND NS09-10-13 ND NS NS ND NS NS ND 25.7 NS ND NS
11-07-13 ND NS NS ND NS NS ND 20.1 NS ND NS03-20-14 ND ND ND 0.44 NS NS ND 20 ND ND NS06-26-14 ND NS ND 0.31 NS NS ND 24 ND ND NS08-22-14 ND NS ND ND NS NS ND 24 ND ND NS11-07-14 ND NS ND ND NS NS ND 27 ND ND NS
03-04-15 NS NS ND ND NS NS ND 16 ND ND NS06-25-15 ND NS ND ND NS NS ND 12 ND ND NS09-23-15 ND NS ND ND NS NS ND 13 ND ND NS12-09-15 ND NS ND 0.94 NS NS ND 10 ND ND NS
1,2-Dichloropropane ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 0.603-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS12-12-12 NS NS NS ND NS NS ND ND NS ND NS03-14-13 ND NS NS ND NS NS ND ND NS ND NS05-29-13 ND NS NS ND NS NS ND ND NS ND NS09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS03-20-14 ND ND ND ND NS NS ND ND ND ND NS06-26-14 ND NS ND ND NS NS ND ND ND ND NS08-22-14 ND NS ND ND NS NS ND ND ND ND NS11-07-14 ND NS ND ND NS NS ND ND ND ND NS
03-04-15 NS NS ND ND NS NS ND ND ND ND NS06-25-15 ND NS ND ND NS NS ND ND ND ND NS09-23-15 ND NS ND ND NS NS ND ND ND ND NS12-09-15 ND NS ND ND NS NS ND ND ND ND NS
Chloroform 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS03-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 70
06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS12-12-12 NS NS NS ND NS NS ND ND NS ND NS03-14-13 ND NS NS ND NS NS ND ND NS ND NS05-29-13 ND NS NS ND NS NS ND ND NS ND NS09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS03-20-14 ND ND ND ND NS NS ND ND ND ND NS06-26-14 ND NS ND ND NS NS ND 1.1 ND ND NS08-22-14 ND NS ND ND NS NS ND ND ND 1.6 NS11-07-14 ND NS ND ND NS NS ND ND ND ND NS
03-04-15 NS NS ND ND NS NS ND ND ND ND NS06-25-15 ND NS ND ND NS NS ND ND ND ND NS09-23-15 ND NS ND ND NS NS ND ND ND ND NS12-09-15 ND NS ND ND NS NS ND ND ND ND NS
*Samples 2765 influent & effluent were sampled on 9/25/01 NA=Not analyzed for this parameter J=Estimated Value NS=Not Sampled
TABLE 5 System Operation Parameters
Harold Smith Grocery
Incident #12913 Union Ridge Road, Burlington, North Carolina
DATE: TEMP. (°F) FLOW (SCFM) VACUUM (IN.-H2O) TEMP. (°F) PRESSURE (PSI)
1/6/09 65 120 9 180 15
2/4/09 55 115 9 175 12
3/16/09 55 115 8 170 10
4/2/09 75 115 7 180 10
5/6/09 78 115 8 184 10
6/5/09 70 115 6 175 10
7/6/09 80 115 8 NR 10
8/10/09 78 115 8 NR 10
9/8/09 76 115 8 NR 9
10/5/09 72 115 7 NR 7
11/2/09 70 115 6 NR 5
12/13/09 58 115 7 NR 5
1/6/10 36 115 8 NR 3
2/18/10 42 115 8 NR 12
3/5/10 56 115 7 NR 12
3/31/10 50 115 8 NR 12
5/24/10 70 115 8 NR 14
6/25/10 75 110 7 NR 14
7/27/10 75 110 6 NR 12
8/6/10 90 110 6 NR 12
9/2/10 90 110 6 NR 11
10/1/10 85 115 6 NR 10
11/10/10 50 115 6 NR 12
12/7/10 45 115 6 NR 12
1/6/11 40 110 6 NR 12
2/3/11 45 110 6 NR 12
3/15/11 55 110 6 NR 12
SYSTEM OFF – SOIL EXCAVATION
1/6/12 OFF OFF OFF NR 10
2/10/12 OFF OFF OFF NR 10
3/19/12 OFF OFF OFF NR 10
4/4/12 OFF OFF OFF NR 10
5/3/12 OFF OFF OFF NR 10
6/1/12 OFF OFF OFF NR 9
7/3/12 OFF OFF OFF NR 9
8/3/12 OFF OFF OFF NR 9
9/21/12 OFF OFF OFF NR OFF
10/3/12 OFF OFF OFF NR OFF
11/19/12 OFF OFF OFF NR OFF
12/14/12 OFF OFF OFF NR OFF
1/28/13 OFF OFF OFF NR OFF
2/25/13 OFF OFF OFF NR OFF
3/19/13 OFF OFF OFF NR OFF
TABLE 5 System Operation Parameters
Harold Smith Grocery
Incident #12913 Union Ridge Road, Burlington, North Carolina
DATE: TEMP. (°F) FLOW (SCFM) VACUUM (IN.-H2O) TEMP. (°F) PRESSURE (PSI)
5/30/13 OFF OFF OFF NR OFF
6/19/13 OFF OFF OFF NR OFF
7/9/13 OFF OFF OFF NR OFF
8/9/13 OFF OFF OFF NR OFF
9/15/3 OFF OFF OFF NR OFF
10/22/13 OFF OFF OFF NR OFF
11/5/13 OFF OFF OFF NR OFF
12/12/13 40 110 5 NR 8
1/10/14 50 110 5 NR 8
2/4/14 40 110 5 NR 8
3/1/14 42 110 5 NR 8
3/25/14 50 110 5 NR 8
5/29/14 80 110 5 NR 8
6/9/14 75 110 5 NR 7
6/30/14 90 110 5 NR 8
8/5/14 80 110 5 NR 8
9/3/14 85 110 5 NR 8
9/26/14 70 110 5 NR 8
11/12/14 50 110 5 NR 8
12/12/14 45 110 5 NR 8
1/21/15 50 110 5 NR 8
1/30/15 50 110 5 NR 8
3/11/15 60 110 5 NR 8
4/13/15 70 110 5 NR 8
5/15/15 70 110 5 NR 8
6/4/15 70 110 5 NR 8
6/29/15 85 110 5 NR 8
7/27/15 85 110 5 NR 8
8/26/15 80 110 5 NR 8
9/30/15 80 110 5 NR 8
11/4/15 70 110 4 NR 8
12/2/15 50 110 4 NR 8

* Individual pressure (in psi) and flow (in scfm) at each sparge well. NR = not recorded.
TABLE 5 System Operation Parameters
Harold Smith Grocery
Incident #12913 Union Ridge Road, Burlington, North Carolina
DATE: PRES./ AS-2 PRES./
AS-3 PRES./
AS-4 PRES./
AS-5 PRES./
AS-6 PRES./
AS-7 PRES./
AS-8 PRES./
TABLE 5 System Operation Parameters
Harold Smith Grocery
Incident #12913 Union Ridge Road, Burlington, North Carolina
DATE: PRES./ AS-2 PRES./
AS-3 PRES./
AS-4 PRES./
AS-5 PRES./
AS-6 PRES./
AS-7 PRES./
AS-8 PRES./
Individual pressure (in psi) and flow (in scfm) at each sparge well. NR = not recorded.

APPENDIX A

This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
Case Narrative
12/22/2015
Pyramid Environmental, Inc
Brett Higgins
PO Box 16265
Greensboro, NC 27416-0265
Project: Harold Smith
Lab Submittal Date: 12/14/2015
Prism Work Order: 5120244
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services
Reviewed ByAngela D. Overcash Terri W. Cole For Angela D. Overcash
Project Manager
Data Qualifiers Key Reference:
D RPD value outside of the control limits.
L1 LCS recovery outside of the QC limits. LCSD recovery within the limits. No further action taken.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 54
Sample Receipt Summary
12/22/2015
Prism Work Order: 5120244
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
5120244-01 12/09/15MW-1A 12/14/15Water
5120244-02 12/09/15MW-3 12/14/15Water
5120244-03 12/09/15MW-4 12/14/15Water
5120244-04 12/09/15MW-5 12/14/15Water
5120244-05 12/09/15MW-6 12/14/15Water
5120244-06 12/09/15MW-7 12/14/15Water
5120244-07 12/09/15MW-9 12/14/15Water
5120244-08 12/09/15MW-10 12/14/15Water
5120244-09 12/09/15MW-11 12/14/15Water
5120244-10 12/09/15MW-12 12/14/15Water
5120244-11 12/09/15MW-13 12/14/15Water
5120244-12 12/09/15MW-15A 12/14/15Water
5120244-13 12/09/15SW-2760 12/14/15Water
5120244-14 12/09/15SW-2768B 12/14/15Water
5120244-15 12/09/15SW-2773 12/14/15Water
5120244-16 12/09/15SW-2779 12/14/15Water
5120244-17 12/09/152765 INF 12/14/15Water
5120244-18 12/09/152765 Mid 12/14/15Water
5120244-19 12/09/152765 EFF 12/14/15Water
Samples were received in good condition at 3.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 54
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 5120244
12/22/2015
Summary of Detections
1.2 ug/L5120244-01 MW-1A 1,2-Dichloroethane SM6200 B
6.0 ug/L5120244-01 MW-1A Isopropyl Ether SM6200 B
1.7 ug/L5120244-01 MW-1A Methyl-tert-Butyl Ether SM6200 B
1.9 ug/L5120244-05 MW-6 Methyl-tert-Butyl Ether SM6200 B
0.61 ug/L5120244-09 MW-11 1,2-Dichloroethane SM6200 B
1.9 ug/L5120244-09 MW-11 Isopropyl Ether SM6200 B
0.94 ug/L5120244-15 SW-2773 1,2-Dichloroethane SM6200 B
2.2 ug/L5120244-15 SW-2773 Isopropyl Ether SM6200 B
3.1 ug/L5120244-15 SW-2773 Methyl-tert-Butyl Ether SM6200 B
0.51 ug/L5120244-15 SW-2773 trans-1,2-Dichloroethylene SM6200 B
10 ug/L5120244-17 2765 INF 1,2-Dichloroethane SM6200 B
75 ug/L5120244-17 2765 INF Isopropyl Ether SM6200 B
0.54 ug/L5120244-17 2765 INF Isopropylbenzene (Cumene)SM6200 B
53 ug/L5120244-17 2765 INF Methyl-tert-Butyl Ether SM6200 B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-1A
Prism Sample ID: 5120244-01
Prism Work Order: 5120244
Time Collected: 12/09/15 15:15
Time Submitted: 12/14/15 15:40
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5L027812.0 12/16/15 20:26 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.0761,2-Dichlorobenzene
1.2 SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5L027812.0 12/16/15 20:26 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5L027811012/16/15 20:26 KDMug/L 0.31Acetone
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.048Benzene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.040Bromoform
BRL SM6200 B P5L027811.0 12/16/15 20:26 KDMug/L 0.18Bromomethane
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.22Chloroethane
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.076Chloroform
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.079Chloromethane
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5L027811.0 12/16/15 20:26 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5L0278120012/16/15 20:26 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-1A
Prism Sample ID: 5120244-01
Prism Work Order: 5120244
Time Collected: 12/09/15 15:15
Time Submitted: 12/14/15 15:40
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5L027812.0 12/16/15 20:26 KDMug/L 0.16Hexachlorobutadiene
6.0 SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5L027811.0 12/16/15 20:26 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P5L027811.0 12/16/15 20:26 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5L027815.0 12/16/15 20:26 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5L027811.0 12/16/15 20:26 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5L027812.0 12/16/15 20:26 KDMug/L 0.083Methylene Chloride
1.7 SM6200 B P5L027811.0 12/16/15 20:26 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5L027811.0 12/16/15 20:26 KDMug/L 0.19Naphthalene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.044o-Xylene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.047Styrene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.044Toluene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5L027815.0 12/16/15 20:26 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5L027810.50 12/16/15 20:26 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5L027811.5 12/16/15 20:26 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130113 %4-Bromofluorobenzene
70-130113 %Dibromofluoromethane
70-130112 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-3
Prism Sample ID: 5120244-02
Prism Work Order: 5120244
Time Collected: 12/09/15 14:55
Time Submitted: 12/14/15 15:40
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5L027812.0 12/16/15 20:52 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5L027812.0 12/16/15 20:52 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5L027811012/16/15 20:52 KDMug/L 0.31Acetone
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.048Benzene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.040Bromoform
BRL SM6200 B P5L027811.0 12/16/15 20:52 KDMug/L 0.18Bromomethane
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.22Chloroethane
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.076Chloroform
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.079Chloromethane
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5L027811.0 12/16/15 20:52 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5L0278120012/16/15 20:52 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-3
Prism Sample ID: 5120244-02
Prism Work Order: 5120244
Time Collected: 12/09/15 14:55
Time Submitted: 12/14/15 15:40
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5L027812.0 12/16/15 20:52 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5L027811.0 12/16/15 20:52 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P5L027811.0 12/16/15 20:52 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5L027815.0 12/16/15 20:52 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5L027811.0 12/16/15 20:52 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5L027812.0 12/16/15 20:52 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5L027811.0 12/16/15 20:52 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5L027811.0 12/16/15 20:52 KDMug/L 0.19Naphthalene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.044o-Xylene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.047Styrene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.044Toluene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5L027815.0 12/16/15 20:52 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5L027810.50 12/16/15 20:52 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5L027811.5 12/16/15 20:52 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130115 %4-Bromofluorobenzene
70-130114 %Dibromofluoromethane
70-130112 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-4
Prism Sample ID: 5120244-03
Prism Work Order: 5120244
Time Collected: 12/09/15 14:45
Time Submitted: 12/14/15 15:40
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5L027812.0 12/16/15 21:17 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5L027812.0 12/16/15 21:17 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5L027811012/16/15 21:17 KDMug/L 0.31Acetone
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.048Benzene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.040Bromoform
BRL SM6200 B P5L027811.0 12/16/15 21:17 KDMug/L 0.18Bromomethane
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.22Chloroethane
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.076Chloroform
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.079Chloromethane
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5L027811.0 12/16/15 21:17 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5L0278120012/16/15 21:17 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-4
Prism Sample ID: 5120244-03
Prism Work Order: 5120244
Time Collected: 12/09/15 14:45
Time Submitted: 12/14/15 15:40
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5L027812.0 12/16/15 21:17 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5L027811.0 12/16/15 21:17 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P5L027811.0 12/16/15 21:17 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5L027815.0 12/16/15 21:17 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5L027811.0 12/16/15 21:17 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5L027812.0 12/16/15 21:17 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5L027811.0 12/16/15 21:17 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5L027811.0 12/16/15 21:17 KDMug/L 0.19Naphthalene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.044o-Xylene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.047Styrene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.044Toluene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5L027815.0 12/16/15 21:17 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5L027810.50 12/16/15 21:17 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5L027811.5 12/16/15 21:17 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130111 %4-Bromofluorobenzene
70-130114 %Dibromofluoromethane
70-130113 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-5
Prism Sample ID: 5120244-04
Prism Work Order: 5120244
Time Collected: 12/09/15 15:35
Time Submitted: 12/14/15 15:40
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5L027812.0 12/16/15 21:43 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5L027812.0 12/16/15 21:43 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5L027811012/16/15 21:43 KDMug/L 0.31Acetone
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.048Benzene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.040Bromoform
BRL SM6200 B P5L027811.0 12/16/15 21:43 KDMug/L 0.18Bromomethane
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.22Chloroethane
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.076Chloroform
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.079Chloromethane
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5L027811.0 12/16/15 21:43 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5L0278120012/16/15 21:43 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-5
Prism Sample ID: 5120244-04
Prism Work Order: 5120244
Time Collected: 12/09/15 15:35
Time Submitted: 12/14/15 15:40
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5L027812.0 12/16/15 21:43 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5L027811.0 12/16/15 21:43 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P5L027811.0 12/16/15 21:43 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5L027815.0 12/16/15 21:43 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5L027811.0 12/16/15 21:43 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5L027812.0 12/16/15 21:43 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5L027811.0 12/16/15 21:43 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5L027811.0 12/16/15 21:43 KDMug/L 0.19Naphthalene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.044o-Xylene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.047Styrene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.044Toluene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5L027815.0 12/16/15 21:43 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5L027810.50 12/16/15 21:43 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5L027811.5 12/16/15 21:43 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130114 %4-Bromofluorobenzene
70-130113 %Dibromofluoromethane
70-130114 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-6
Prism Sample ID: 5120244-05
Prism Work Order: 5120244
Time Collected: 12/09/15 15:05
Time Submitted: 12/14/15 15:40
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5L027812.0 12/16/15 22:09 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5L027812.0 12/16/15 22:09 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5L027811012/16/15 22:09 KDMug/L 0.31Acetone
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.048Benzene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.040Bromoform
BRL SM6200 B P5L027811.0 12/16/15 22:09 KDMug/L 0.18Bromomethane
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.22Chloroethane
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.076Chloroform
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.079Chloromethane
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5L027811.0 12/16/15 22:09 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5L0278120012/16/15 22:09 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-6
Prism Sample ID: 5120244-05
Prism Work Order: 5120244
Time Collected: 12/09/15 15:05
Time Submitted: 12/14/15 15:40
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5L027812.0 12/16/15 22:09 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5L027811.0 12/16/15 22:09 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P5L027811.0 12/16/15 22:09 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5L027815.0 12/16/15 22:09 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5L027811.0 12/16/15 22:09 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5L027812.0 12/16/15 22:09 KDMug/L 0.083Methylene Chloride
1.9 SM6200 B P5L027811.0 12/16/15 22:09 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5L027811.0 12/16/15 22:09 KDMug/L 0.19Naphthalene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.044o-Xylene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.047Styrene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.044Toluene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5L027815.0 12/16/15 22:09 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5L027810.50 12/16/15 22:09 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5L027811.5 12/16/15 22:09 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130112 %4-Bromofluorobenzene
70-130115 %Dibromofluoromethane
70-130115 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-7
Prism Sample ID: 5120244-06
Prism Work Order: 5120244
Time Collected: 12/09/15 13:55
Time Submitted: 12/14/15 15:40
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 15:09 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5L028112.0 12/16/15 15:09 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5L028111012/16/15 15:09 KDMug/L 0.31Acetone
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.048Benzene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.040Bromoform
BRL SM6200 B P5L028111.0 12/16/15 15:09 KDMug/L 0.18Bromomethane
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.22Chloroethane
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.076Chloroform
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.079Chloromethane
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5L028111.0 12/16/15 15:09 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5L0281120012/16/15 15:09 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-7
Prism Sample ID: 5120244-06
Prism Work Order: 5120244
Time Collected: 12/09/15 13:55
Time Submitted: 12/14/15 15:40
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 15:09 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5L028111.0 12/16/15 15:09 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P5L028111.0 12/16/15 15:09 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5L028115.0 12/16/15 15:09 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5L028111.0 12/16/15 15:09 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5L028112.0 12/16/15 15:09 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5L028111.0 12/16/15 15:09 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5L028111.0 12/16/15 15:09 KDMug/L 0.19Naphthalene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.044o-Xylene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.047Styrene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.044Toluene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5L028115.0 12/16/15 15:09 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5L028110.50 12/16/15 15:09 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5L028111.5 12/16/15 15:09 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-13099 %Dibromofluoromethane
70-130100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-9
Prism Sample ID: 5120244-07
Prism Work Order: 5120244
Time Collected: 12/09/15 14:35
Time Submitted: 12/14/15 15:40
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 15:35 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5L028112.0 12/16/15 15:35 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5L028111012/16/15 15:35 KDMug/L 0.31Acetone
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.048Benzene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.040Bromoform
BRL SM6200 B P5L028111.0 12/16/15 15:35 KDMug/L 0.18Bromomethane
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.22Chloroethane
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.076Chloroform
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.079Chloromethane
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5L028111.0 12/16/15 15:35 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5L0281120012/16/15 15:35 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-9
Prism Sample ID: 5120244-07
Prism Work Order: 5120244
Time Collected: 12/09/15 14:35
Time Submitted: 12/14/15 15:40
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 15:35 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5L028111.0 12/16/15 15:35 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P5L028111.0 12/16/15 15:35 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5L028115.0 12/16/15 15:35 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5L028111.0 12/16/15 15:35 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5L028112.0 12/16/15 15:35 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5L028111.0 12/16/15 15:35 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5L028111.0 12/16/15 15:35 KDMug/L 0.19Naphthalene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.044o-Xylene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.047Styrene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.044Toluene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5L028115.0 12/16/15 15:35 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5L028110.50 12/16/15 15:35 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5L028111.5 12/16/15 15:35 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13098 %4-Bromofluorobenzene
70-13098 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-10
Prism Sample ID: 5120244-08
Prism Work Order: 5120244
Time Collected: 12/09/15 14:25
Time Submitted: 12/14/15 15:40
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 16:00 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5L028112.0 12/16/15 16:00 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5L028111012/16/15 16:00 KDMug/L 0.31Acetone
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.048Benzene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.040Bromoform
BRL SM6200 B P5L028111.0 12/16/15 16:00 KDMug/L 0.18Bromomethane
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.22Chloroethane
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.076Chloroform
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.079Chloromethane
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5L028111.0 12/16/15 16:00 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5L0281120012/16/15 16:00 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-10
Prism Sample ID: 5120244-08
Prism Work Order: 5120244
Time Collected: 12/09/15 14:25
Time Submitted: 12/14/15 15:40
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 16:00 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5L028111.0 12/16/15 16:00 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P5L028111.0 12/16/15 16:00 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5L028115.0 12/16/15 16:00 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5L028111.0 12/16/15 16:00 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5L028112.0 12/16/15 16:00 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5L028111.0 12/16/15 16:00 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5L028111.0 12/16/15 16:00 KDMug/L 0.19Naphthalene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.044o-Xylene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.047Styrene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.044Toluene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5L028115.0 12/16/15 16:00 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5L028110.50 12/16/15 16:00 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5L028111.5 12/16/15 16:00 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-13099 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-11
Prism Sample ID: 5120244-09
Prism Work Order: 5120244
Time Collected: 12/09/15 14:05
Time Submitted: 12/14/15 15:40
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 16:26 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.0761,2-Dichlorobenzene
0.61 SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5L028112.0 12/16/15 16:26 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5L028111012/16/15 16:26 KDMug/L 0.31Acetone
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.048Benzene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.040Bromoform
BRL SM6200 B P5L028111.0 12/16/15 16:26 KDMug/L 0.18Bromomethane
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.22Chloroethane
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.076Chloroform
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.079Chloromethane
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5L028111.0 12/16/15 16:26 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5L0281120012/16/15 16:26 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-11
Prism Sample ID: 5120244-09
Prism Work Order: 5120244
Time Collected: 12/09/15 14:05
Time Submitted: 12/14/15 15:40
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 16:26 KDMug/L 0.16Hexachlorobutadiene
1.9 SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5L028111.0 12/16/15 16:26 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P5L028111.0 12/16/15 16:26 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5L028115.0 12/16/15 16:26 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5L028111.0 12/16/15 16:26 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5L028112.0 12/16/15 16:26 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5L028111.0 12/16/15 16:26 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5L028111.0 12/16/15 16:26 KDMug/L 0.19Naphthalene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.044o-Xylene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.047Styrene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.044Toluene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5L028115.0 12/16/15 16:26 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5L028110.50 12/16/15 16:26 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5L028111.5 12/16/15 16:26 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-130101 %Dibromofluoromethane
70-130100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-12
Prism Sample ID: 5120244-10
Prism Work Order: 5120244
Time Collected: 12/09/15 14:15
Time Submitted: 12/14/15 15:40
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 16:51 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5L028112.0 12/16/15 16:51 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5L028111012/16/15 16:51 KDMug/L 0.31Acetone
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.048Benzene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.040Bromoform
BRL SM6200 B P5L028111.0 12/16/15 16:51 KDMug/L 0.18Bromomethane
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.22Chloroethane
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.076Chloroform
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.079Chloromethane
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5L028111.0 12/16/15 16:51 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5L0281120012/16/15 16:51 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-12
Prism Sample ID: 5120244-10
Prism Work Order: 5120244
Time Collected: 12/09/15 14:15
Time Submitted: 12/14/15 15:40
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 16:51 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5L028111.0 12/16/15 16:51 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P5L028111.0 12/16/15 16:51 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5L028115.0 12/16/15 16:51 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5L028111.0 12/16/15 16:51 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5L028112.0 12/16/15 16:51 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5L028111.0 12/16/15 16:51 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5L028111.0 12/16/15 16:51 KDMug/L 0.19Naphthalene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.044o-Xylene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.047Styrene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.044Toluene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5L028115.0 12/16/15 16:51 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5L028110.50 12/16/15 16:51 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5L028111.5 12/16/15 16:51 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-130103 %Dibromofluoromethane
70-130101 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-13
Prism Sample ID: 5120244-11
Prism Work Order: 5120244
Time Collected: 12/09/15 13:45
Time Submitted: 12/14/15 15:40
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 17:16 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5L028112.0 12/16/15 17:16 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5L028111012/16/15 17:16 KDMug/L 0.31Acetone
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.048Benzene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.040Bromoform
BRL SM6200 B P5L028111.0 12/16/15 17:16 KDMug/L 0.18Bromomethane
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.22Chloroethane
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.076Chloroform
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.079Chloromethane
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5L028111.0 12/16/15 17:16 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5L0281120012/16/15 17:16 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-13
Prism Sample ID: 5120244-11
Prism Work Order: 5120244
Time Collected: 12/09/15 13:45
Time Submitted: 12/14/15 15:40
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 17:16 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5L028111.0 12/16/15 17:16 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P5L028111.0 12/16/15 17:16 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5L028115.0 12/16/15 17:16 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5L028111.0 12/16/15 17:16 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5L028112.0 12/16/15 17:16 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5L028111.0 12/16/15 17:16 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5L028111.0 12/16/15 17:16 KDMug/L 0.19Naphthalene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.044o-Xylene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.047Styrene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.044Toluene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5L028115.0 12/16/15 17:16 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5L028110.50 12/16/15 17:16 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5L028111.5 12/16/15 17:16 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-130100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-15A
Prism Sample ID: 5120244-12
Prism Work Order: 5120244
Time Collected: 12/09/15 15:25
Time Submitted: 12/14/15 15:40
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 20:39 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5L028112.0 12/16/15 20:39 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5L028111012/16/15 20:39 KDMug/L 0.31Acetone
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.048Benzene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.040Bromoform
BRL SM6200 B P5L028111.0 12/16/15 20:39 KDMug/L 0.18Bromomethane
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.22Chloroethane
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.076Chloroform
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.079Chloromethane
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5L028111.0 12/16/15 20:39 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5L0281120012/16/15 20:39 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-15A
Prism Sample ID: 5120244-12
Prism Work Order: 5120244
Time Collected: 12/09/15 15:25
Time Submitted: 12/14/15 15:40
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 20:39 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5L028111.0 12/16/15 20:39 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P5L028111.0 12/16/15 20:39 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5L028115.0 12/16/15 20:39 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5L028111.0 12/16/15 20:39 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5L028112.0 12/16/15 20:39 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5L028111.0 12/16/15 20:39 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5L028111.0 12/16/15 20:39 KDMug/L 0.19Naphthalene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.044o-Xylene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.047Styrene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.044Toluene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5L028115.0 12/16/15 20:39 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5L028110.50 12/16/15 20:39 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5L028111.5 12/16/15 20:39 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130103 %4-Bromofluorobenzene
70-130103 %Dibromofluoromethane
70-130100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW-2760
Prism Sample ID: 5120244-13
Prism Work Order: 5120244
Time Collected: 12/09/15 13:00
Time Submitted: 12/14/15 15:40
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 17:41 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5L028112.0 12/16/15 17:41 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5L028111012/16/15 17:41 KDMug/L 0.31Acetone
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.048Benzene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.040Bromoform
BRL SM6200 B P5L028111.0 12/16/15 17:41 KDMug/L 0.18Bromomethane
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.22Chloroethane
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.076Chloroform
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.079Chloromethane
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5L028111.0 12/16/15 17:41 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5L0281120012/16/15 17:41 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW-2760
Prism Sample ID: 5120244-13
Prism Work Order: 5120244
Time Collected: 12/09/15 13:00
Time Submitted: 12/14/15 15:40
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 17:41 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5L028111.0 12/16/15 17:41 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P5L028111.0 12/16/15 17:41 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5L028115.0 12/16/15 17:41 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5L028111.0 12/16/15 17:41 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5L028112.0 12/16/15 17:41 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5L028111.0 12/16/15 17:41 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5L028111.0 12/16/15 17:41 KDMug/L 0.19Naphthalene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.044o-Xylene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.047Styrene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.044Toluene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5L028115.0 12/16/15 17:41 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5L028110.50 12/16/15 17:41 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5L028111.5 12/16/15 17:41 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
70-13099 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW-2768B
Prism Sample ID: 5120244-14
Prism Work Order: 5120244
Time Collected: 12/09/15 13:30
Time Submitted: 12/14/15 15:40
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 18:07 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5L028112.0 12/16/15 18:07 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5L028111012/16/15 18:07 KDMug/L 0.31Acetone
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.048Benzene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.040Bromoform
BRL SM6200 B P5L028111.0 12/16/15 18:07 KDMug/L 0.18Bromomethane
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.22Chloroethane
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.076Chloroform
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.079Chloromethane
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5L028111.0 12/16/15 18:07 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5L0281120012/16/15 18:07 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW-2768B
Prism Sample ID: 5120244-14
Prism Work Order: 5120244
Time Collected: 12/09/15 13:30
Time Submitted: 12/14/15 15:40
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 18:07 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5L028111.0 12/16/15 18:07 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P5L028111.0 12/16/15 18:07 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5L028115.0 12/16/15 18:07 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5L028111.0 12/16/15 18:07 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5L028112.0 12/16/15 18:07 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5L028111.0 12/16/15 18:07 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5L028111.0 12/16/15 18:07 KDMug/L 0.19Naphthalene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.044o-Xylene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.047Styrene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.044Toluene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5L028115.0 12/16/15 18:07 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5L028110.50 12/16/15 18:07 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5L028111.5 12/16/15 18:07 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
70-13098 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW-2773
Prism Sample ID: 5120244-15
Prism Work Order: 5120244
Time Collected: 12/09/15 12:20
Time Submitted: 12/14/15 15:40
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 18:32 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.0761,2-Dichlorobenzene
0.94 SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5L028112.0 12/16/15 18:32 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5L028111012/16/15 18:32 KDMug/L 0.31Acetone
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.048Benzene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.040Bromoform
BRL SM6200 B P5L028111.0 12/16/15 18:32 KDMug/L 0.18Bromomethane
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.22Chloroethane
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.076Chloroform
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.079Chloromethane
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5L028111.0 12/16/15 18:32 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5L0281120012/16/15 18:32 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW-2773
Prism Sample ID: 5120244-15
Prism Work Order: 5120244
Time Collected: 12/09/15 12:20
Time Submitted: 12/14/15 15:40
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 18:32 KDMug/L 0.16Hexachlorobutadiene
2.2 SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5L028111.0 12/16/15 18:32 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P5L028111.0 12/16/15 18:32 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5L028115.0 12/16/15 18:32 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5L028111.0 12/16/15 18:32 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5L028112.0 12/16/15 18:32 KDMug/L 0.083Methylene Chloride
3.1 SM6200 B P5L028111.0 12/16/15 18:32 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5L028111.0 12/16/15 18:32 KDMug/L 0.19Naphthalene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.044o-Xylene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.047Styrene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.044Toluene
0.51 SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5L028115.0 12/16/15 18:32 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5L028110.50 12/16/15 18:32 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5L028111.5 12/16/15 18:32 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW-2779
Prism Sample ID: 5120244-16
Prism Work Order: 5120244
Time Collected: 12/09/15 12:40
Time Submitted: 12/14/15 15:40
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 18:57 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5L028112.0 12/16/15 18:57 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5L028111012/16/15 18:57 KDMug/L 0.31Acetone
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.048Benzene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.040Bromoform
BRL SM6200 B P5L028111.0 12/16/15 18:57 KDMug/L 0.18Bromomethane
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.22Chloroethane
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.076Chloroform
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.079Chloromethane
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5L028111.0 12/16/15 18:57 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5L0281120012/16/15 18:57 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW-2779
Prism Sample ID: 5120244-16
Prism Work Order: 5120244
Time Collected: 12/09/15 12:40
Time Submitted: 12/14/15 15:40
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 18:57 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5L028111.0 12/16/15 18:57 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P5L028111.0 12/16/15 18:57 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5L028115.0 12/16/15 18:57 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5L028111.0 12/16/15 18:57 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5L028112.0 12/16/15 18:57 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5L028111.0 12/16/15 18:57 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5L028111.0 12/16/15 18:57 KDMug/L 0.19Naphthalene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.044o-Xylene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.047Styrene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.044Toluene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5L028115.0 12/16/15 18:57 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5L028110.50 12/16/15 18:57 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5L028111.5 12/16/15 18:57 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13099 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765 INF
Prism Sample ID: 5120244-17
Prism Work Order: 5120244
Time Collected: 12/09/15 11:30
Time Submitted: 12/14/15 15:40
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 19:23 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0761,2-Dichlorobenzene
10 SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5L028112.0 12/16/15 19:23 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5L028111012/16/15 19:23 KDMug/L 0.31Acetone
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.048Benzene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.040Bromoform
BRL SM6200 B P5L028111.0 12/16/15 19:23 KDMug/L 0.18Bromomethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.22Chloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.076Chloroform
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.079Chloromethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5L028111.0 12/16/15 19:23 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5L0281120012/16/15 19:23 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765 INF
Prism Sample ID: 5120244-17
Prism Work Order: 5120244
Time Collected: 12/09/15 11:30
Time Submitted: 12/14/15 15:40
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 19:23 KDMug/L 0.16Hexachlorobutadiene
75 SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.050Isopropyl Ether
0.54 SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5L028111.0 12/16/15 19:23 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P5L028111.0 12/16/15 19:23 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5L028115.0 12/16/15 19:23 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5L028111.0 12/16/15 19:23 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5L028112.0 12/16/15 19:23 KDMug/L 0.083Methylene Chloride
53 SM6200 B P5L028111.0 12/16/15 19:23 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5L028111.0 12/16/15 19:23 KDMug/L 0.19Naphthalene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.044o-Xylene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.047Styrene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.044Toluene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5L028115.0 12/16/15 19:23 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5L028111.5 12/16/15 19:23 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-130100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765 Mid
Prism Sample ID: 5120244-18
Prism Work Order: 5120244
Time Collected: 12/09/15 11:40
Time Submitted: 12/14/15 15:40
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 19:48 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5L028112.0 12/16/15 19:48 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5L028111012/16/15 19:48 KDMug/L 0.31Acetone
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.048Benzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.040Bromoform
BRL SM6200 B P5L028111.0 12/16/15 19:48 KDMug/L 0.18Bromomethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.22Chloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.076Chloroform
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.079Chloromethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5L028111.0 12/16/15 19:48 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5L0281120012/16/15 19:48 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765 Mid
Prism Sample ID: 5120244-18
Prism Work Order: 5120244
Time Collected: 12/09/15 11:40
Time Submitted: 12/14/15 15:40
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 19:48 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5L028111.0 12/16/15 19:48 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P5L028111.0 12/16/15 19:48 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5L028115.0 12/16/15 19:48 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5L028111.0 12/16/15 19:48 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5L028112.0 12/16/15 19:48 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5L028111.0 12/16/15 19:48 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5L028111.0 12/16/15 19:48 KDMug/L 0.19Naphthalene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.044o-Xylene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.047Styrene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.044Toluene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5L028115.0 12/16/15 19:48 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5L028111.5 12/16/15 19:48 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765 EFF
Prism Sample ID: 5120244-19
Prism Work Order: 5120244
Time Collected: 12/09/15 11:50
Time Submitted: 12/14/15 15:40
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 20:14 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5L028112.0 12/16/15 20:14 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5L028111012/16/15 20:14 KDMug/L 0.31Acetone
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.048Benzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.040Bromoform
BRL SM6200 B P5L028111.0 12/16/15 20:14 KDMug/L 0.18Bromomethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.22Chloroethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.076Chloroform
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.079Chloromethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5L028111.0 12/16/15 20:14 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5L0281120012/16/15 20:14 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765 EFF
Prism Sample ID: 5120244-19
Prism Work Order: 5120244
Time Collected: 12/09/15 11:50
Time Submitted: 12/14/15 15:40
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 20:14 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5L028111.0 12/16/15 20:14 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P5L028111.0 12/16/15 20:14 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5L028115.0 12/16/15 20:14 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5L028111.0 12/16/15 20:14 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5L028112.0 12/16/15 20:14 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5L028111.0 12/16/15 20:14 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5L028111.0 12/16/15 20:14 KDMug/L 0.19Naphthalene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.044o-Xylene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.047Styrene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.044Toluene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5L028115.0 12/16/15 20:14 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5L028111.5 12/16/15 20:14 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
70-13099 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 41 of 54
12/22/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5120244
Time Submitted: 12/14/2015 3:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5L0278 - SM6200 B
Blank (P5L0278-BLK1)Prepared & Analyzed: 12/16/15
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL0.50
1,2,4-Trichlorobenzene ug/LBRL0.50
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL10
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL0.50
Bromomethane ug/LBRL1.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethanol ug/LBRL200
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 42 of 54
12/22/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5120244
Time Submitted: 12/14/2015 3:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5L0278 - SM6200 B
Blank (P5L0278-BLK1)Prepared & Analyzed: 12/16/15
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL1.0
Methylene Chloride ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL1.0
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL0.50
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Butylbenzene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL5.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 11255.9
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 11155.6
ug/L 50.00 70-130Surrogate: Toluene-d8 10853.8
LCS (P5L0278-BS1)Prepared & Analyzed: 12/16/15
1,1,1,2-Tetrachloroethane ug/L21.5 0.50 20.00 70-130108
1,1,1-Trichloroethane ug/L23.1 0.50 20.00 70-130115
1,1,2,2-Tetrachloroethane ug/L24.0 0.50 20.00 70-130120
1,1,2-Trichloroethane ug/L22.3 0.50 20.00 70-130112
1,1-Dichloroethane ug/L22.7 0.50 20.00 70-130114
1,1-Dichloroethylene ug/L23.1 0.50 20.00 70-130116
1,1-Dichloropropylene ug/L23.8 0.50 20.00 70-130119
1,2,3-Trichlorobenzene ug/L27.1 0.50 20.00 L170-130136
1,2,3-Trichloropropane ug/L22.6 0.50 20.00 70-130113
1,2,4-Trichlorobenzene ug/L24.6 0.50 20.00 70-130123
1,2,4-Trimethylbenzene ug/L22.6 0.50 20.00 70-130113
1,2-Dibromo-3-chloropropane ug/L24.1 2.0 20.00 70-130121
1,2-Dibromoethane ug/L22.9 0.50 20.00 70-130115
1,2-Dichlorobenzene ug/L22.3 0.50 20.00 70-130112
1,2-Dichloroethane ug/L20.6 0.50 20.00 70-130103
1,2-Dichloropropane ug/L22.1 0.50 20.00 70-130111
1,3,5-Trimethylbenzene ug/L23.0 0.50 20.00 70-130115
1,3-Dichlorobenzene ug/L22.6 0.50 20.00 70-130113
1,3-Dichloropropane ug/L22.6 0.50 20.00 70-130113
1,4-Dichlorobenzene ug/L22.1 0.50 20.00 70-130111
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 43 of 54
12/22/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5120244
Time Submitted: 12/14/2015 3:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5L0278 - SM6200 B
LCS (P5L0278-BS1)Prepared & Analyzed: 12/16/15
2,2-Dichloropropane ug/L24.0 2.0 20.00 70-130120
2-Chlorotoluene ug/L22.8 0.50 20.00 70-130114
4-Chlorotoluene ug/L22.4 0.50 20.00 70-130112
4-Isopropyltoluene ug/L23.3 0.50 20.00 70-130117
Acetone ug/L39.9 10 40.00 40-160100
Benzene ug/L21.9 0.50 20.00 70-130109
Bromobenzene ug/L21.5 0.50 20.00 70-130108
Bromochloromethane ug/L23.2 0.50 20.00 70-130116
Bromodichloromethane ug/L22.1 0.50 20.00 70-130111
Bromoform ug/L20.5 0.50 20.00 70-130102
Bromomethane ug/L22.6 1.0 20.00 60-140113
Carbon Tetrachloride ug/L20.6 0.50 20.00 70-130103
Chlorobenzene ug/L21.6 0.50 20.00 70-130108
Chloroethane ug/L22.0 0.50 20.00 60-140110
Chloroform ug/L21.4 0.50 20.00 70-130107
Chloromethane ug/L21.3 0.50 20.00 60-140106
cis-1,2-Dichloroethylene ug/L22.2 0.50 20.00 70-130111
cis-1,3-Dichloropropylene ug/L22.8 0.50 20.00 70-130114
Dibromochloromethane ug/L23.3 0.50 20.00 70-130116
Dibromomethane ug/L22.0 0.50 20.00 70-130110
Dichlorodifluoromethane ug/L23.2 1.0 20.00 60-140116
Ethanol ug/L581200 500.0 60-140116
Ethylbenzene ug/L21.9 0.50 20.00 70-130110
Hexachlorobutadiene ug/L23.1 2.0 20.00 70-130115
Isopropyl Ether ug/L22.4 0.50 20.00 70-130112
Isopropylbenzene (Cumene)ug/L22.8 0.50 20.00 70-130114
m,p-Xylenes ug/L44.3 1.0 40.00 70-130111
Methyl Butyl Ketone (2-Hexanone)ug/L21.9 1.0 20.00 60-140110
Methyl Ethyl Ketone (2-Butanone)ug/L19.1 5.0 20.00 60-14095
Methyl Isobutyl Ketone ug/L22.8 1.0 20.00 60-140114
Methylene Chloride ug/L21.3 2.0 20.00 70-130107
Methyl-tert-Butyl Ether ug/L22.4 1.0 20.00 70-130112
Naphthalene ug/L24.0 1.0 20.00 70-130120
n-Butylbenzene ug/L23.6 0.50 20.00 70-130118
n-Propylbenzene ug/L23.2 0.50 20.00 70-130116
o-Xylene ug/L22.1 0.50 20.00 70-130110
sec-Butylbenzene ug/L23.5 0.50 20.00 70-130117
Styrene ug/L22.2 0.50 20.00 70-130111
tert-Butylbenzene ug/L22.9 0.50 20.00 70-130114
Tetrachloroethylene ug/L22.8 0.50 20.00 70-130114
Toluene ug/L22.3 0.50 20.00 70-130111
trans-1,2-Dichloroethylene ug/L22.8 0.50 20.00 70-130114
trans-1,3-Dichloropropylene ug/L22.7 0.50 20.00 70-130113
Trichloroethylene ug/L21.8 0.50 20.00 70-130109
Trichlorofluoromethane ug/L20.3 0.50 20.00 60-140102
Vinyl acetate ug/L25.3 5.0 20.00 60-140127
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 44 of 54
12/22/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5120244
Time Submitted: 12/14/2015 3:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5L0278 - SM6200 B
LCS (P5L0278-BS1)Prepared & Analyzed: 12/16/15
Vinyl chloride ug/L22.7 0.50 20.00 60-140113
Xylenes, total ug/L66.3 1.5 60.00 70-130111
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10853.8
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10854.2
ug/L 50.00 70-130Surrogate: Toluene-d8 10652.8
LCS Dup (P5L0278-BSD1)Prepared & Analyzed: 12/16/15
1,1,1,2-Tetrachloroethane ug/L22.2 0.50 20.00 2070-130111 3
1,1,1-Trichloroethane ug/L21.2 0.50 20.00 2070-130106 8
1,1,2,2-Tetrachloroethane ug/L23.2 0.50 20.00 2070-130116 3
1,1,2-Trichloroethane ug/L22.5 0.50 20.00 2070-130113 1
1,1-Dichloroethane ug/L21.8 0.50 20.00 2070-130109 4
1,1-Dichloroethylene ug/L22.1 0.50 20.00 2070-130110 5
1,1-Dichloropropylene ug/L23.0 0.50 20.00 2070-130115 4
1,2,3-Trichlorobenzene ug/L21.3 0.50 20.00 20 D70-130106 24
1,2,3-Trichloropropane ug/L23.1 0.50 20.00 2070-130116 2
1,2,4-Trichlorobenzene ug/L22.0 0.50 20.00 2070-130110 11
1,2,4-Trimethylbenzene ug/L21.9 0.50 20.00 2070-130110 3
1,2-Dibromo-3-chloropropane ug/L22.1 2.0 20.00 2070-130110 9
1,2-Dibromoethane ug/L22.7 0.50 20.00 2070-130113 1
1,2-Dichlorobenzene ug/L21.3 0.50 20.00 2070-130106 5
1,2-Dichloroethane ug/L20.3 0.50 20.00 2070-130102 1
1,2-Dichloropropane ug/L21.9 0.50 20.00 2070-130110 0.8
1,3,5-Trimethylbenzene ug/L22.0 0.50 20.00 2070-130110 4
1,3-Dichlorobenzene ug/L21.8 0.50 20.00 2070-130109 4
1,3-Dichloropropane ug/L22.6 0.50 20.00 2070-130113 0.2
1,4-Dichlorobenzene ug/L21.5 0.50 20.00 2070-130108 3
2,2-Dichloropropane ug/L23.0 2.0 20.00 2070-130115 5
2-Chlorotoluene ug/L22.1 0.50 20.00 2070-130110 3
4-Chlorotoluene ug/L21.8 0.50 20.00 2070-130109 3
4-Isopropyltoluene ug/L22.4 0.50 20.00 2070-130112 4
Acetone ug/L45.6 10 40.00 2040-160114 14
Benzene ug/L21.5 0.50 20.00 2070-130107 2
Bromobenzene ug/L23.5 0.50 20.00 2070-130118 9
Bromochloromethane ug/L22.5 0.50 20.00 2070-130112 3
Bromodichloromethane ug/L21.7 0.50 20.00 2070-130109 2
Bromoform ug/L21.6 0.50 20.00 2070-130108 5
Bromomethane ug/L22.2 1.0 20.00 2060-140111 2
Carbon Tetrachloride ug/L20.1 0.50 20.00 2070-130100 3
Chlorobenzene ug/L21.7 0.50 20.00 2070-130109 0.6
Chloroethane ug/L22.0 0.50 20.00 2060-140110 0.3
Chloroform ug/L20.9 0.50 20.00 2070-130104 3
Chloromethane ug/L20.4 0.50 20.00 2060-140102 4
cis-1,2-Dichloroethylene ug/L21.8 0.50 20.00 2070-130109 2
cis-1,3-Dichloropropylene ug/L22.8 0.50 20.00 2070-130114 0.4
Dibromochloromethane ug/L22.6 0.50 20.00 2070-130113 3
Dibromomethane ug/L22.2 0.50 20.00 2070-130111 0.9
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 45 of 54
12/22/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5120244
Time Submitted: 12/14/2015 3:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5L0278 - SM6200 B
LCS Dup (P5L0278-BSD1)Prepared & Analyzed: 12/16/15
Dichlorodifluoromethane ug/L21.4 1.0 20.00 2060-140107 8
Ethanol ug/L570200 500.0 2060-140114 2
Ethylbenzene ug/L21.3 0.50 20.00 2070-130106 3
Hexachlorobutadiene ug/L21.1 2.0 20.00 2070-130105 9
Isopropyl Ether ug/L22.5 0.50 20.00 2070-130113 0.4
Isopropylbenzene (Cumene)ug/L22.3 0.50 20.00 2070-130111 3
m,p-Xylenes ug/L43.6 1.0 40.00 2070-130109 1
Methyl Butyl Ketone (2-Hexanone)ug/L22.2 1.0 20.00 2060-140111 1
Methyl Ethyl Ketone (2-Butanone)ug/L20.7 5.0 20.00 2060-140103 8
Methyl Isobutyl Ketone ug/L22.7 1.0 20.00 2060-140113 0.4
Methylene Chloride ug/L21.5 2.0 20.00 2070-130108 1
Methyl-tert-Butyl Ether ug/L22.8 1.0 20.00 2070-130114 2
Naphthalene ug/L21.8 1.0 20.00 2070-130109 10
n-Butylbenzene ug/L22.5 0.50 20.00 2070-130112 5
n-Propylbenzene ug/L22.0 0.50 20.00 2070-130110 6
o-Xylene ug/L21.6 0.50 20.00 2070-130108 2
sec-Butylbenzene ug/L22.3 0.50 20.00 2070-130112 5
Styrene ug/L21.9 0.50 20.00 2070-130110 1
tert-Butylbenzene ug/L22.5 0.50 20.00 2070-130112 2
Tetrachloroethylene ug/L21.8 0.50 20.00 2070-130109 4
Toluene ug/L21.7 0.50 20.00 2070-130109 2
trans-1,2-Dichloroethylene ug/L21.6 0.50 20.00 2070-130108 5
trans-1,3-Dichloropropylene ug/L23.2 0.50 20.00 2070-130116 2
Trichloroethylene ug/L21.8 0.50 20.00 2070-130109 0.2
Trichlorofluoromethane ug/L19.8 0.50 20.00 2060-14099 2
Vinyl acetate ug/L24.4 5.0 20.00 2060-140122 4
Vinyl chloride ug/L22.2 0.50 20.00 2060-140111 2
Xylenes, total ug/L65.2 1.5 60.00 2070-130109 2
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 11055.0
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10552.6
ug/L 50.00 70-130Surrogate: Toluene-d8 10753.5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 46 of 54
12/22/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5120244
Time Submitted: 12/14/2015 3:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5L0281 - SM6200 B
Blank (P5L0281-BLK1)Prepared & Analyzed: 12/16/15
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL0.50
1,2,4-Trichlorobenzene ug/LBRL0.50
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL10
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL0.50
Bromomethane ug/LBRL1.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethanol ug/LBRL200
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 47 of 54
12/22/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5120244
Time Submitted: 12/14/2015 3:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5L0281 - SM6200 B
Blank (P5L0281-BLK1)Prepared & Analyzed: 12/16/15
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL1.0
Methylene Chloride ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL1.0
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL0.50
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Butylbenzene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL5.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10049.8
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10049.9
ug/L 50.00 70-130Surrogate: Toluene-d8 9849.2
LCS (P5L0281-BS1)Prepared & Analyzed: 12/16/15
1,1,1,2-Tetrachloroethane ug/L21.8 0.50 20.00 70-130109
1,1,1-Trichloroethane ug/L22.1 0.50 20.00 70-130111
1,1,2,2-Tetrachloroethane ug/L21.4 0.50 20.00 70-130107
1,1,2-Trichloroethane ug/L21.0 0.50 20.00 70-130105
1,1-Dichloroethane ug/L21.3 0.50 20.00 70-130107
1,1-Dichloroethylene ug/L20.4 0.50 20.00 70-130102
1,1-Dichloropropylene ug/L20.5 0.50 20.00 70-130102
1,2,3-Trichlorobenzene ug/L22.0 0.50 20.00 70-130110
1,2,3-Trichloropropane ug/L20.7 0.50 20.00 70-130103
1,2,4-Trichlorobenzene ug/L22.7 0.50 20.00 70-130114
1,2,4-Trimethylbenzene ug/L22.8 0.50 20.00 70-130114
1,2-Dibromo-3-chloropropane ug/L21.4 2.0 20.00 70-130107
1,2-Dibromoethane ug/L21.7 0.50 20.00 70-130109
1,2-Dichlorobenzene ug/L21.6 0.50 20.00 70-130108
1,2-Dichloroethane ug/L19.9 0.50 20.00 70-13099
1,2-Dichloropropane ug/L21.4 0.50 20.00 70-130107
1,3,5-Trimethylbenzene ug/L22.9 0.50 20.00 70-130115
1,3-Dichlorobenzene ug/L22.0 0.50 20.00 70-130110
1,3-Dichloropropane ug/L21.1 0.50 20.00 70-130106
1,4-Dichlorobenzene ug/L21.5 0.50 20.00 70-130108
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 48 of 54
12/22/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5120244
Time Submitted: 12/14/2015 3:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5L0281 - SM6200 B
LCS (P5L0281-BS1)Prepared & Analyzed: 12/16/15
2,2-Dichloropropane ug/L23.0 2.0 20.00 70-130115
2-Chlorotoluene ug/L21.9 0.50 20.00 70-130109
4-Chlorotoluene ug/L21.9 0.50 20.00 70-130110
4-Isopropyltoluene ug/L22.8 0.50 20.00 70-130114
Acetone ug/L38.2 10 40.00 40-16095
Benzene ug/L21.8 0.50 20.00 70-130109
Bromobenzene ug/L21.2 0.50 20.00 70-130106
Bromochloromethane ug/L21.2 0.50 20.00 70-130106
Bromodichloromethane ug/L21.0 0.50 20.00 70-130105
Bromoform ug/L21.7 0.50 20.00 70-130109
Bromomethane ug/L20.1 1.0 20.00 60-140100
Carbon Tetrachloride ug/L21.6 0.50 20.00 70-130108
Chlorobenzene ug/L22.1 0.50 20.00 70-130110
Chloroethane ug/L15.1 0.50 20.00 60-14076
Chloroform ug/L21.0 0.50 20.00 70-130105
Chloromethane ug/L21.1 0.50 20.00 60-140105
cis-1,2-Dichloroethylene ug/L21.2 0.50 20.00 70-130106
cis-1,3-Dichloropropylene ug/L21.7 0.50 20.00 70-130109
Dibromochloromethane ug/L21.8 0.50 20.00 70-130109
Dibromomethane ug/L20.6 0.50 20.00 70-130103
Dichlorodifluoromethane ug/L22.4 1.0 20.00 60-140112
Ethanol ug/L603200 500.0 60-140121
Ethylbenzene ug/L22.8 0.50 20.00 70-130114
Hexachlorobutadiene ug/L22.6 2.0 20.00 70-130113
Isopropyl Ether ug/L21.8 0.50 20.00 70-130109
Isopropylbenzene (Cumene)ug/L23.1 0.50 20.00 70-130116
m,p-Xylenes ug/L45.6 1.0 40.00 70-130114
Methyl Butyl Ketone (2-Hexanone)ug/L22.2 1.0 20.00 60-140111
Methyl Ethyl Ketone (2-Butanone)ug/L20.0 5.0 20.00 60-140100
Methyl Isobutyl Ketone ug/L21.7 1.0 20.00 60-140108
Methylene Chloride ug/L20.2 2.0 20.00 70-130101
Methyl-tert-Butyl Ether ug/L21.3 1.0 20.00 70-130107
Naphthalene ug/L22.0 1.0 20.00 70-130110
n-Butylbenzene ug/L22.5 0.50 20.00 70-130113
n-Propylbenzene ug/L23.1 0.50 20.00 70-130116
o-Xylene ug/L22.8 0.50 20.00 70-130114
sec-Butylbenzene ug/L22.3 0.50 20.00 70-130112
Styrene ug/L23.5 0.50 20.00 70-130118
tert-Butylbenzene ug/L22.8 0.50 20.00 70-130114
Tetrachloroethylene ug/L21.1 0.50 20.00 70-130105
Toluene ug/L22.0 0.50 20.00 70-130110
trans-1,2-Dichloroethylene ug/L21.8 0.50 20.00 70-130109
trans-1,3-Dichloropropylene ug/L21.6 0.50 20.00 70-130108
Trichloroethylene ug/L21.9 0.50 20.00 70-130110
Trichlorofluoromethane ug/L21.1 0.50 20.00 60-140105
Vinyl acetate ug/L23.8 5.0 20.00 60-140119
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 49 of 54
12/22/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5120244
Time Submitted: 12/14/2015 3:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5L0281 - SM6200 B
LCS (P5L0281-BS1)Prepared & Analyzed: 12/16/15
Vinyl chloride ug/L20.7 0.50 20.00 60-140103
Xylenes, total ug/L68.4 1.5 60.00 70-130114
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9848.9
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9949.4
ug/L 50.00 70-130Surrogate: Toluene-d8 10150.6
LCS Dup (P5L0281-BSD1)Prepared & Analyzed: 12/16/15
1,1,1,2-Tetrachloroethane ug/L20.9 0.50 20.00 2070-130105 4
1,1,1-Trichloroethane ug/L21.3 0.50 20.00 2070-130106 4
1,1,2,2-Tetrachloroethane ug/L20.5 0.50 20.00 2070-130103 4
1,1,2-Trichloroethane ug/L20.3 0.50 20.00 2070-130102 3
1,1-Dichloroethane ug/L20.7 0.50 20.00 2070-130103 3
1,1-Dichloroethylene ug/L19.8 0.50 20.00 2070-13099 3
1,1-Dichloropropylene ug/L19.8 0.50 20.00 2070-13099 3
1,2,3-Trichlorobenzene ug/L21.6 0.50 20.00 2070-130108 2
1,2,3-Trichloropropane ug/L20.2 0.50 20.00 2070-130101 2
1,2,4-Trichlorobenzene ug/L21.8 0.50 20.00 2070-130109 4
1,2,4-Trimethylbenzene ug/L22.0 0.50 20.00 2070-130110 4
1,2-Dibromo-3-chloropropane ug/L20.0 2.0 20.00 2070-130100 7
1,2-Dibromoethane ug/L21.0 0.50 20.00 2070-130105 3
1,2-Dichlorobenzene ug/L21.0 0.50 20.00 2070-130105 3
1,2-Dichloroethane ug/L19.2 0.50 20.00 2070-13096 3
1,2-Dichloropropane ug/L20.8 0.50 20.00 2070-130104 3
1,3,5-Trimethylbenzene ug/L22.3 0.50 20.00 2070-130112 3
1,3-Dichlorobenzene ug/L21.2 0.50 20.00 2070-130106 3
1,3-Dichloropropane ug/L20.8 0.50 20.00 2070-130104 2
1,4-Dichlorobenzene ug/L21.2 0.50 20.00 2070-130106 2
2,2-Dichloropropane ug/L22.3 2.0 20.00 2070-130111 3
2-Chlorotoluene ug/L21.2 0.50 20.00 2070-130106 3
4-Chlorotoluene ug/L21.4 0.50 20.00 2070-130107 2
4-Isopropyltoluene ug/L22.1 0.50 20.00 2070-130110 3
Acetone ug/L36.0 10 40.00 2040-16090 6
Benzene ug/L21.1 0.50 20.00 2070-130106 3
Bromobenzene ug/L20.9 0.50 20.00 2070-130104 2
Bromochloromethane ug/L21.0 0.50 20.00 2070-130105 0.6
Bromodichloromethane ug/L20.6 0.50 20.00 2070-130103 2
Bromoform ug/L21.1 0.50 20.00 2070-130105 3
Bromomethane ug/L19.5 1.0 20.00 2060-14098 3
Carbon Tetrachloride ug/L20.8 0.50 20.00 2070-130104 4
Chlorobenzene ug/L21.4 0.50 20.00 2070-130107 3
Chloroethane ug/L16.3 0.50 20.00 2060-14082 7
Chloroform ug/L20.3 0.50 20.00 2070-130102 3
Chloromethane ug/L20.7 0.50 20.00 2060-140103 2
cis-1,2-Dichloroethylene ug/L20.5 0.50 20.00 2070-130103 3
cis-1,3-Dichloropropylene ug/L21.3 0.50 20.00 2070-130106 2
Dibromochloromethane ug/L21.2 0.50 20.00 2070-130106 3
Dibromomethane ug/L20.2 0.50 20.00 2070-130101 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 50 of 54
12/22/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5120244
Time Submitted: 12/14/2015 3:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5L0281 - SM6200 B
LCS Dup (P5L0281-BSD1)Prepared & Analyzed: 12/16/15
Dichlorodifluoromethane ug/L21.5 1.0 20.00 2060-140108 4
Ethanol ug/L586200 500.0 2060-140117 3
Ethylbenzene ug/L21.9 0.50 20.00 2070-130110 4
Hexachlorobutadiene ug/L22.0 2.0 20.00 2070-130110 3
Isopropyl Ether ug/L21.2 0.50 20.00 2070-130106 3
Isopropylbenzene (Cumene)ug/L22.5 0.50 20.00 2070-130112 3
m,p-Xylenes ug/L44.2 1.0 40.00 2070-130111 3
Methyl Butyl Ketone (2-Hexanone)ug/L21.4 1.0 20.00 2060-140107 4
Methyl Ethyl Ketone (2-Butanone)ug/L19.5 5.0 20.00 2060-14097 3
Methyl Isobutyl Ketone ug/L21.0 1.0 20.00 2060-140105 3
Methylene Chloride ug/L19.6 2.0 20.00 2070-13098 3
Methyl-tert-Butyl Ether ug/L20.9 1.0 20.00 2070-130104 2
Naphthalene ug/L21.6 1.0 20.00 2070-130108 2
n-Butylbenzene ug/L22.0 0.50 20.00 2070-130110 2
n-Propylbenzene ug/L22.5 0.50 20.00 2070-130112 3
o-Xylene ug/L22.0 0.50 20.00 2070-130110 3
sec-Butylbenzene ug/L21.5 0.50 20.00 2070-130108 3
Styrene ug/L22.4 0.50 20.00 2070-130112 5
tert-Butylbenzene ug/L22.2 0.50 20.00 2070-130111 3
Tetrachloroethylene ug/L19.9 0.50 20.00 2070-130100 6
Toluene ug/L21.4 0.50 20.00 2070-130107 3
trans-1,2-Dichloroethylene ug/L21.1 0.50 20.00 2070-130106 3
trans-1,3-Dichloropropylene ug/L21.2 0.50 20.00 2070-130106 2
Trichloroethylene ug/L21.5 0.50 20.00 2070-130108 2
Trichlorofluoromethane ug/L20.9 0.50 20.00 2060-140104 0.9
Vinyl acetate ug/L22.4 5.0 20.00 2060-140112 6
Vinyl chloride ug/L20.1 0.50 20.00 2060-140101 3
Xylenes, total ug/L66.3 1.5 60.00 2070-130110 3
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9848.9
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9849.2
ug/L 50.00 70-130Surrogate: Toluene-d8 10049.8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 51 of 54
Sample Extraction Data
Prep Method: SM6200 B
Lab Number Batch Date/TimeInitialFinal
P5L02785120244-01 12/16/15 8:551010mLmL
P5L02785120244-02 12/16/15 8:551010mLmL
P5L02785120244-03 12/16/15 8:551010mLmL
P5L02785120244-04 12/16/15 8:551010mLmL
P5L02785120244-05 12/16/15 8:551010mLmL
P5L02815120244-06 12/16/15 9:081010mLmL
P5L02815120244-07 12/16/15 9:081010mLmL
P5L02815120244-08 12/16/15 9:081010mLmL
P5L02815120244-09 12/16/15 9:081010mLmL
P5L02815120244-10 12/16/15 9:081010mLmL
P5L02815120244-11 12/16/15 9:081010mLmL
P5L02815120244-12 12/16/15 9:081010mLmL
P5L02815120244-13 12/16/15 9:081010mLmL
P5L02815120244-14 12/16/15 9:081010mLmL
P5L02815120244-15 12/16/15 9:081010mLmL
P5L02815120244-16 12/16/15 9:081010mLmL
P5L02815120244-17 12/16/15 9:081010mLmL
P5L02815120244-18 12/16/15 9:081010mLmL
P5L02815120244-19 12/16/15 9:081010mLmL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 52 of 54
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APPENDIX B

503 Industrial Ave • Greensboro, NC 27406 Phone [phone] • Fax [phone] • Toll Free [phone]
Email: [e-mail]
January 20, 2015 James McMillan Sent Via email: [e-mail]

RE: Supply Well Analytical Results 2765 Union Ridge Road, Burlington, NC NCDEQ Incident #12913 Former Harold Smith Grocery Pyramid Project 2015-217
Dear Mr. McMillan:

As directed by the NCDENR and T.A.C., Inc., Pyramid Environmental has continued to collect samples
from the Point-of-Entry (POE) treatment system that is connected to your water supply well. The work is
being performed as part of the ongoing assessment of the referenced underground storage tank release.
The results of the water analyses are presented below.

On December 9, 2015, Pyramid collected influent, midfluent, and effluent samples from the POE
connected to your supply well. The samples are designated as SW2765 INF, SW2765 MID, and SW2765
EFF. The groundwater samples were analyzed at a State certified laboratory and the results are attached
for your review. The laboratory results indicate that the POE influent (untreated water) contained methyl
tert-butyl ether (MTBE) at a concentration of 53 parts per billion (PPB). The current North Carolina
drinking water standard for MTBE is 20 PPB. The compound 1,2-dichloroethane was detected at 10 PPB.
The current North Carolina drinking water standard for 1,2-dichloroethane is 0.4 PPB. The compound
isopropyl ether was detected at 75 PPB. The current North Carolina drinking water standard for isopropyl
ether is 70 PPB. No other targeted compounds were detected at concentrations that exceeded the laboratory detection limits in the POE influent. The laboratory results of the POE effluent sample (treated water) collected on December 9, 2015 indicate that none of the targeted petroleum compounds were detected at concentrations that exceed the
laboratory detection limits. The POE worked to remove petroleum contaminants prior to water use.
Maintenance of the POE treatment system will continue to be performed on a quarterly basis.

If you have any questions, please call Pyramid at [phone]. Thank you for your cooperation with
this project.

Sincerely,
Brett S. Higgins
Project Manager
Attachments – Laboratory Report
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765 INF
Prism Sample ID: 5120244-17
Prism Work Order: 5120244
Time Collected: 12/09/15 11:30
Time Submitted: 12/14/15 15:40
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 19:23 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0761,2-Dichlorobenzene
10 SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5L028112.0 12/16/15 19:23 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5L028111012/16/15 19:23 KDMug/L 0.31Acetone
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.048Benzene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.040Bromoform
BRL SM6200 B P5L028111.0 12/16/15 19:23 KDMug/L 0.18Bromomethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.22Chloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.076Chloroform
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.079Chloromethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5L028111.0 12/16/15 19:23 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5L0281120012/16/15 19:23 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765 INF
Prism Sample ID: 5120244-17
Prism Work Order: 5120244
Time Collected: 12/09/15 11:30
Time Submitted: 12/14/15 15:40
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 19:23 KDMug/L 0.16Hexachlorobutadiene
75 SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.050Isopropyl Ether
0.54 SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5L028111.0 12/16/15 19:23 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P5L028111.0 12/16/15 19:23 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5L028115.0 12/16/15 19:23 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5L028111.0 12/16/15 19:23 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5L028112.0 12/16/15 19:23 KDMug/L 0.083Methylene Chloride
53 SM6200 B P5L028111.0 12/16/15 19:23 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5L028111.0 12/16/15 19:23 KDMug/L 0.19Naphthalene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.044o-Xylene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.047Styrene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.044Toluene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5L028115.0 12/16/15 19:23 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5L028110.50 12/16/15 19:23 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5L028111.5 12/16/15 19:23 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-130100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765 Mid
Prism Sample ID: 5120244-18
Prism Work Order: 5120244
Time Collected: 12/09/15 11:40
Time Submitted: 12/14/15 15:40
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 19:48 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5L028112.0 12/16/15 19:48 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5L028111012/16/15 19:48 KDMug/L 0.31Acetone
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.048Benzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.040Bromoform
BRL SM6200 B P5L028111.0 12/16/15 19:48 KDMug/L 0.18Bromomethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.22Chloroethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.076Chloroform
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.079Chloromethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5L028111.0 12/16/15 19:48 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5L0281120012/16/15 19:48 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765 Mid
Prism Sample ID: 5120244-18
Prism Work Order: 5120244
Time Collected: 12/09/15 11:40
Time Submitted: 12/14/15 15:40
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 19:48 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5L028111.0 12/16/15 19:48 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P5L028111.0 12/16/15 19:48 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5L028115.0 12/16/15 19:48 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5L028111.0 12/16/15 19:48 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5L028112.0 12/16/15 19:48 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5L028111.0 12/16/15 19:48 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5L028111.0 12/16/15 19:48 KDMug/L 0.19Naphthalene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.044o-Xylene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.047Styrene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.044Toluene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5L028115.0 12/16/15 19:48 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5L028110.50 12/16/15 19:48 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5L028111.5 12/16/15 19:48 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765 EFF
Prism Sample ID: 5120244-19
Prism Work Order: 5120244
Time Collected: 12/09/15 11:50
Time Submitted: 12/14/15 15:40
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 20:14 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5L028112.0 12/16/15 20:14 KDMug/L 0.112,2-Dichloropropane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5L028111012/16/15 20:14 KDMug/L 0.31Acetone
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.048Benzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.040Bromoform
BRL SM6200 B P5L028111.0 12/16/15 20:14 KDMug/L 0.18Bromomethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.22Chloroethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.076Chloroform
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.079Chloromethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5L028111.0 12/16/15 20:14 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5L0281120012/16/15 20:14 KDMug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 of 54
Laboratory Report
12/22/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765 EFF
Prism Sample ID: 5120244-19
Prism Work Order: 5120244
Time Collected: 12/09/15 11:50
Time Submitted: 12/14/15 15:40
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5L028112.0 12/16/15 20:14 KDMug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5L028111.0 12/16/15 20:14 KDMug/L 0.12m,p-Xylenes
BRL SM6200 B P5L028111.0 12/16/15 20:14 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5L028115.0 12/16/15 20:14 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5L028111.0 12/16/15 20:14 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5L028112.0 12/16/15 20:14 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5L028111.0 12/16/15 20:14 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5L028111.0 12/16/15 20:14 KDMug/L 0.19Naphthalene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.044o-Xylene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.047Styrene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.044Toluene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5L028115.0 12/16/15 20:14 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5L028110.50 12/16/15 20:14 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5L028111.5 12/16/15 20:14 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
70-13099 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 41 of 54

APPENDIX C
Summary of System Installation, Start-up, and Operation Activities
Harold Smith Remediation System
October - December 2015

October Visit:
September 30, 2015 System was operational upon arrival. The technician checked the system
and performed regular operational and maintenance tasks on the system.
The technician then recorded system operational data and measurements.
System was operational at departure.

November 4, 2015 System was not operational at arrival. The technician checked the system
and restarted. The technician performed regular operational and
maintenance tasks on the system. The technician then recorded system
operations data and measurements. System was operational at departure.

December 2, 2015 System was operational upon arrival. The technician checked the system
and performed regular operational and maintenance tasks on the system.
The technician then recorded system operational data and measurements.
System was operational at departure.