WS-3891_12913_CA_RMR_20151208

TABLE OF CONTENTS

1.0 INTRODUCTION .............................................................................. 1
1.1 SITE INFORMATION ................................................................................................... 1
1.2 ADJOINING PROPERTIES AND POTENTIAL RECEPTORS .............................................. 1
1.3 SITE HYDROLOGY & GEOLOGY ................................................................................ 2
1.4 PREVIOUS REPORTS ................................................................................................. 2
2.0 GROUNDWATER SAMPLING ....................................................... 3
2.1 MONITORING WELL SAMPLING ................................................................................ 3
2.2 POTABLE WATER SUPPLY WELL SAMPLING............................................................. 3
3.0 SYSTEM OPERATIONAL STATUS .............................................. 4
3.1 SYSTEM OPERATIONS ............................................................................................... 4
3.2 CONTAMINATED SOIL REMOVAL .............................................................................. 5
3.3 SYSTEM UPDATE ...................................................................................................... 5
4.0 SOIL & GROUNDWATER ASSESSMENT ................................... 6
4.1 GROUNDWATER ANALYTICAL RESULTS ................................................................... 6
4.2 SUPPLY WELL ANALYTICAL RESULTS...................................................................... 7
5.0 CONCLUSIONS & RECOMMENDATIONS ................................ 8
6.0 CLOSURE ........................................................................................... 8

Page I
TABLE OF CONTENTS (Continued)

FIGURES:

1. Topographic Map
2. Site Map
3a. Adjoining Properties and Water Supply Wells
3b. Adjoining Properties and Water Supply Wells
4. Potentiometric Surface Map (9/22/15)
5. MTBE Isoconcentration Map (9/22 – 9/23/15)
6. 1,2-Dichloroethane Isoconcentration Map (9/22 – 9/23/15)
7. Remediation System Layout Map (1/16/12)

TABLES:

1. Monitoring Well Construction Details
2. Groundwater Elevation Data
3. Monitoring Well Analytical Results
4. Water Supply Well Analytical Results
5. System Operation Parameters

APPENDICES:

A. Groundwater Laboratory Report & Chain of Custody
B. Supply Well Results Letter (POE)
C. Recent O&M Activities

Page II
ACRONYMS

BLS ................Below Land Surface
BTEX ............Benzene, Toluene, Ethylbenzene, & Xylenes
CFR ................Code of Federal Regulations
COC ...............Chain of Custody
CSA ................Comprehensive Site Assessment
DEQ ...............Department of Environmental Quality
EPH ................Extractable Petroleum Hydrocarbons
GCLs ..............Gross Contaminant Levels
HASP .............Health & Safety Plan
MADEP..........Massachusetts Department of Environmental Protection
MSCC ............Maximum Soil Contaminant Concentration
MTBE ............Methyl Tertiary Butyl Ether
µg/L ................Micrograms per Liter
mg/kg .............Milligrams per kilogram
MW ................Monitoring Well
NCAC ............North Carolina Administrative Code
O&M ..............Operations and Maintenance
OSHA .............Occupational Safety and Health Administration
OVA ...............Organic Vapor Analyzer
PPM ...............Parts Per Million
PID .................Photo-ionization Detector
P&ID ..............Process & Instrumentation Diagram
PVC ................Poly-vinyl Chloride
QA/QC ...........Quality Assurance / Quality Control
SCFM .............Standard Cubic Feet per Minute
SVE ................Soil Vapor Extraction
SW .................Water Supply Well
UST ................Underground Storage Tank
US EPA ..........United States Environmental Protection Agency
VPH................Volatile Petroleum Hydrocarbons

Page III
Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 1 Pyramid Project # 2015-160 12/08/15
ACTIVE REMEDIATION MONITORING REPORT
Harold Smith Grocery
Burlington, North Carolina

1.0 INTRODUCTION

1.1 Site Information

SITE NAME: Harold Smith Grocery
ADDRESS: 2774 Union Ridge Road
CITY: Burlington, NC
COUNTY: Alamance

CURRENT PROPERTY OWNER: Jessica Alton
CURRENT PROPERTY USE: Inactive Store (used as storage)
OWNER OF USTs: TAC, Inc. (All USTs were removed in 1994)
RESPONSIBLE PARTY: TAC, Inc.
NCDEQ UST FACILITY ID: 0-024148
GROUNDWATER INCIDENT NO.: 12913
SITE RANKING: H755E

UNDERGROUND STORAGE TANKS (USTs)

(gallons)
1 550 Kerosene Removed 8/01/94
2 550 Gasoline Removed 8/01/94
3 550 Gasoline Removed 8/01/94
4 1,000 Gasoline Removed 8/01/94

FIGURES: Figure 1: Topographic Map
Figure 2: Site Map
Figure 3a: Adjoining Properties and Water Supply Wells
Figure 3b: Adjoining Properties and Water Supply Wells

1.2 Adjoining Properties and Potential Receptors

ADJOINING PROPERTY USE: Residential/Agricultural
PUBLIC WATER AVAILABILITY: Unavailable
SUPPLY WELLS WITHIN 1000 FEET: Yes (see Figure 3a/b)
SUPPLY WELLS IMPACTED ABOVE
NCAC 2L STANDARDS: Yes, Supply well at 2765 Union Ridge Rd.
(currently on POE system)
Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 2 Pyramid Project # 2015-160 12/08/15
NEAREST SURFACE WATER: Intermittent Creek – 500-600’ SE
BASEMENTS: None
SUBSURFACE UTILITIES: None near source area

1.3 Site Hydrology & Geology

GEOLOGIC PROVINCE: Carolina Slate Belt
BEDROCK TYPE: Felsic Intrusive Complex
DEPTH TO BEDROCK: 25-38 feet BGS (below ground surface)
CURRENT DEPTH TO WATER TABLE: 11.11 – 15.52 feet BGS (9/22/15)
HISTORIC GW FLUCTUATIONS: Over the past 14 years, the groundwater has
fluctuated in the source area from 5-15 feet BGS
POTENTIOMETRIC GRADIENT: Southeast ~ 0.025 ft. /ft.
HYDRAULIC CONDUCTIVITY (K): 6.17–6.25 x 10-7 ft. /sec.
GROUNDWATER VELOCITY: ~0.4–1.3 feet/year

1.4 Previous Reports

REPORT TITLE

CONSULTANT
DATE OF
REPORT

COMMENTS
Pyramid Environmental 8/30/94 Soil TPH above Action Level
Pyramid Environmental 1/2/95
Pyramid Environmental 9/20/96
Pyramid Environmental 1/30/97 Original CAP report
Pyramid Environmental
Pyramid Environmental 6/7/99
Pyramid Environmental 11/99 to 01/13
Soil Cleanup Report Pyramid Environmental 5/31/2011
Pyramid Environmental
Pyramid Environmental 8/10/15
Pyramid Environmental 12/08/15 Current Report
Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 3 Pyramid Project # 2015-160 12/08/15
2.0 GROUNDWATER SAMPLING

2.1 Monitoring Well Sampling

On September 22-23, 2015, selected monitoring wells at the Harold Smith Site were sampled.

WELLS SAMPLED: MW-1A, MW-3, MW-4, MW-5, MW-6, MW-7, MW-9, MW-10,
MW-11, MW-12, MW-13 and MW-15A
LAB ANALYSES: EPA Method 6200B

FREE PRODUCT: No free product has been observed on this site.

TABLES & GRAPHS: Table 1: Monitoring Well Construction Details
Table 2: Groundwater Elevation Data
Table 3: Monitoring Well Analytical Results

FIGURES: Figure 4: Potentiometric Surface Map
Figure 5: MTBE Concentration Map
Figure 6: 1, 2-Dichloroethane Isoconcentration Map

LABORATORY REPORTS & CHAINS-OF-CUSTODY: Appendix A

FIELD PROCEDURES: Field procedures were performed as outlined in the DEQ July 15,
2008 and May 1, 2012 updates publication “Guidelines for
Sampling” under the UST Section.

2.2 Potable Water Supply Well Sampling

SAMPLING DATE: September 23, 2015
WELLS SAMPLED: 2765 INF, 2765 MID, 2765 EFF, 2768B, 2760, 2773, and 2779
The house at 2779 Union Ridge Road no longer uses the supply
well in the front yard, but uses the well located on an adjacent
eastern property. The property at 2768 Union Ridge Road uses the
supply well in the back yard and is automatically switched to the
well in the front yard (2768-A) if the water level gets too low.

LAB ANALYSES: EPA Method 6200B

TABLES: Table 4: Water Supply Well Analytical Results
FIGURES: Figure 3 a/b: Adjoining Properties and Water Supply Wells.

LABORATORY REPORTS & CHAINS-OF-CUSTODY: Appendix A

Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 4 Pyramid Project # 2015-160 12/08/15
FIELD PROCEDURES: Field procedures were performed as outlined in the DEQ July 15,
2008 and May 1, 2012 updates publication “Guidelines for
Sampling” under the UST Section.

*NOTE* Supply wells are named by the address of the residence they serve and not the property
owner. All supply well addresses sampled are on Union Ridge Road. Mr. James McMillan
requested that Pyramid inform him of the POE system analytical results after each sampling. The
well analytical evaluation letter is presented in Appendix B.

3.0 SYSTEM OPERATIONAL STATUS
3.1 System Operations

The air sparging (AS) and soil vapor extraction (SVE) treatment system for the Harold Smith
Grocery site began operation in July 1999 and operated through 2004 when it was shut down.

The system was restarted in February 2005 and the system was operational through October
2005. Repairs were made to the system and the remediation system was officially restarted on
February 8, 2006. The system ran intermittently during the first quarter of 2006, needing minor
repairs. System operation was interrupted by electrical power interruptions (strong storms)
tripping circuit breakers. In August 2006, the system electrical contacts were found to be
completely melted. The electrical components were replaced after pre-approval, and tested. The
motor of the air-sparge compressor would not operate, and the electric motor was found to be
locked up. Pyramid contacted the equipment manufacturer and priced the replacement items
necessary to get the air-sparge system running again. The SVE system continued to run after the
replacement of the circuit breakers.

In March 2007 the rebuilt air sparge motor was put back in service. The restored compressor
operated from March 2007 through June 2008. At this time, the air-sparge compressor needed to
be replaced. The air sparge motor was replaced with a more serviceable model on October 7,
2008. The carbon vanes were changed by Pyramid in February 2010. The air sparge system was
operational during the 1st quarter of 2011. The system ceased operating in March 2011 to allow
for the soil excavation. Since the system operation ceased, DO concentrations dropped and
Pyramid recommended continued air sparging operation to speed site cleanup. In January 2012,
the air sparge system was restarted using the selected remaining air sparge wells.

In 2013, the system was upgraded to include deeper AS wells and a higher pressure compressor.

The system was operational for most of the fourth quarter of 2014, with the exception of two to
three weeks in December when the system was down due a damaged compressor drive belt. The
damaged belt was discovered on 12/12/14 and replaced on 12/19/14 and the system was re-
started. Since restarting the system in December 2014, the system has remained operational. A
summary of the operations and maintenance activities performed from July 2015 through
September 2015 is presented in Appendix C.
Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 5 Pyramid Project # 2015-160 12/08/15
3.2 Contaminated Soil Removal

In March 2009, Pyramid collected risk-based soil samples from several soil borings and added
several monitoring wells. The additional assessment was conducted to investigate the soils in the
area of the former pump island, and provide additional monitoring wells to assess the source area
for regulatory incident closure. The highest groundwater concentrations have been in MW-1 and
MW-1A throughout the remediation period. As a result of the additional investigations, an area
approximately 40 feet by 20 feet was identified as containing soil concentrations greater than
Soil-to-Groundwater (STGW) standards. Only the soil boring directly at the location of the
former pump island showed concentrations above residential Maximum Soil Contaminant
Concentrations (MSCCs). The DENR requested that Pyramid evaluate soil excavation as a way
to help move the site toward regulatory closure. After the excavation plan was preapproved by
the DENR, Pyramid implemented the excavation plan.

In May 2011, Pyramid supervised the excavation of petroleum contaminated soils at the Harold
Smith site in Burlington, NC. The goal of the soil excavation was to remove volatile petroleum
hydrocarbons from the smear zone (between 5 and 15 feet BLS) to help reduce groundwater
contamination. Based on certified weight tickets, 483.69 tons of petroleum-contaminated soil
was removed. Pyramid requested pre-approval to implement oxygen release compound in
addition to the excavation, but DENR denied the request. The laboratory results of the post
excavation soil samples collected indicate that all of the contaminated soils above the residential
MSCCs were removed.

The remaining contamination detected at the site was above the STGW MSCCs and well below
the residential standards. The remaining STGW concentrations were located underneath the store
building, along the northern property boundary, and on the eastern edge of the property near
Union Ridge Road. Because of the structures, roads, and utilities, additional soil excavation was
not feasible or recommended.

After the excavation of contaminated soil, Pyramid installed monitoring wells MW-1A and MW-
15A to assess the groundwater in the source area. The latest results of these new wells (MW-1A
and MW-15A) since installation are included in Section 4.0 with past results located in Table 3.

3.3 System Update

FIGURES: Figure 7: Remediation System Layout Map

To prevent the migration of the contaminant plume, protect nearby supply wells, and speed up
remediation, the current air sparge (AS) and soil vapor extraction (SVE) system was updated in
October 2012. Additional wells were added to the air sparge segment of the remediation system.
Seven deeper air sparge wells were added to surround the existing petroleum contaminant plume.
The additional wells prevent contaminant plume migration and provide additional air flow for
petroleum hydrocarbons volatilization. Along with the AS remediation update, the soil vapor
extraction system was repaired after it was damaged during the soil excavation in May 2011. A
map of the Remediation System Layout is shown in Figure 7.
Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 6 Pyramid Project # 2015-160 12/08/15
4.0 SOIL & GROUNDWATER ASSESSMENT

4.1 Groundwater Analytical Results

The results of the September 22-23, 2015 sampling event showed that remaining petroleum
contaminants were detected at low concentrations. All of the reported concentrations are listed in
micrograms per liter (µg/L). The concentrations of 1,2-Dichloroethane (1,2-DCA) in MW-1A
(3.7 µg/L) and SW-2765 (13.0 µg/L) were above the 2L groundwater standard of 0.4 µg/L. The
concentrations of targeted compounds for this sampling event have slightly increased or
remained the same in all of the monitoring wells. The highest concentrations found for this
sampling event are shown below. Concentrations above NCAC 2L groundwater standards are
shown in bold and the associated well numbers are shown in parentheses. All of the reported
concentrations are listed in micrograms per liter (µg/L).

• Benzene 1.2 µg/L (MW-1A)
• Toluene Not Detected (MW-15A)
• Ethylbenzene Not Detected (MW-15A)
• Total Xylenes 250 µg/L (MW-15A)
• MTBE 70 µg/L (SW-2765 Influent)
• Isopropyl Ether (IPE) 74 µg/L (SW-2765 Influent)
• 1,2-Dichloroethane 13 µg/L (SW-2765 Influent)
• Naphthalene 16 µg/L (MW-15A)

Over the past 14 years of groundwater and soil remediation, the general concentration trends
demonstrated in the groundwater monitoring wells have been decreasing and are now
approaching regulatory closure.

The benzene concentrations in MW-1A have decreased from over 8,000 µg/L in 1998 to 1.2
µg/L for the current monitoring period. Benzene concentrations in MW-15A have remained at a
concentration below detection limits for the last two sampling events in June and September
2015. MTBE concentrations in MW-1A have decreased from 610 µg/L in 1999 to 6.2 µg/L for
the current monitoring period. Concentrations of 1,2-dichloroethane were detected in MW-1A
and SW-2765 and remain above the 2L Standard.

In planning for the soil excavation project, Pyramid recommended that the DEQ consider the
placement of oxygen-release compounds in the excavation to help clean up the site. Since
cleanup will have to be to the NCAC 2L Standards, any remedial process that can help reach
regulatory closure more quickly should be considered by the DEQ. Pyramid’s request was not
approved for Trust Fund reimbursement, and no oxygen-release compounds were used in the
excavation. In the future, the Trust Fund should consider reimbursing the use of oxygen-release
compounds while excavations are open to help reduce the overall costs for petroleum incident
closures. Active soil and groundwater remediation are needed to reduce the remaining petroleum
contaminant concentrations in the groundwater.

Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 7 Pyramid Project # 2015-160 12/08/15
4.2 Supply Well Analytical Results

Supply well sampling was conducted on September 22-23, 2015 as required by the State.
Pyramid sampled five supply wells 2765, 2768B, 2760, 2773, and 2779. Samples were also
collected from the point of entry (POE) treatment system, 2765 mid-fluent and 2765 effluent.
Samples were collected in laboratory provided containers using clean, disposable nitrile gloves,
packed in ice and shipped to Prism Analytical Laboratories for analysis using EPA Method
6200B.

Groundwater pumped from the supply well at address 2765 (SW-2765) is treated by a Point-of-
Entry (POE) treatment system installed in 2000. The POE system consists of particulate and
carbon filters that remove petroleum from the groundwater. This residential treatment system has
shown effective groundwater treatment since 2000. The laboratory results of treated water
samples collected from the supply well in September 2015 show no detections of petroleum
contaminants.

For the untreated water from SW-2765, MTBE (70 µg/L), IPE (74 µg/L), and 1,2-dichloroethane
(13 µg/L) were detected above their respective NCAC 2L Groundwater Standards. No petroleum
hydrocarbon concentrations were detected in the effluent (treated water) showing effective POE
treatment. Table 4 shows the recent supply well analytical results. A copy of the laboratory
report and chain-of-custody form is presented in Appendix A.

The supply well samples from SW-2773 showed no petroleum contaminants above the 2L
standards. This supply well has shown no petroleum impacts in the past several years. In the
March 2015 sample analysis, there was an “Estimated” detection of trans-1,2-dichloroethene
reported by the laboratory. The Prism lab report stated:

“For sample 5030124-05 with client ID of SW-2773, the initial 6200 was analyzed
undiluted and showed a large hit of Trans-1,2-dichloroethene that was outside of
calibration range. Dilutions of 1:20 and 1:50 were analyzed and the Trans-1,2-
dichloroethene did not duplicate. Vials were checked for accuracy in labeling and were
correct. The initial run is reported with an "E" flag to show an estimated value. “

Basically, the initial detection was not confirmed and was a questionable result. Pyramid
recommended re-sampling the well, which was planned and pre-approved by the Trust Fund.
Since the residence is provided with bottled water at this time, the potential for exposure was
mitigated. Pyramid re-sampled SW-2773 in the June 2015 sampling event. In June 2015, the
trans-1,2-dichloroethene detection of 2.4 µg/L was far below the 2L standard of 100 µg/L. The
current sampling event in September 2015 also showed a concentration of 2.4 µg/L. Pyramid will
continue to monitor the trans-1,2-dichloroethene concentrations for this well.

Laboratory analytical results show that there were no other detectable petroleum hydrocarbon
concentrations in the supply well samples collected from wells 2768B, 2760, 2773 and 2779.

Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 8 Pyramid Project # 2015-160 12/08/15
Pyramid recommends continued POE treatment of supply well 2765, continued sampling of the
closest supply wells (2765 & 2773) on a quarterly basis, and continued sampling of the wells
further from the source area (2761, 2768, 2774, and 2779) on an annual basis. The next quarterly
sampling event will be in December 2015.

5.0 CONCLUSIONS & RECOMMENDATIONS

Pyramid has completed the directed operation & maintenance and groundwater monitoring at the
Harold Smith Grocery. Based on the current groundwater concentrations of MTBE, Naphthalene,
IPE, and 1,2-Dichloroethane remaining above the 2L groundwater standard, the site remains high
risk. The remediation goal is to reduce dissolved groundwater contamination below 2L standards
to protect local water supply well users.

• The soil excavation was completed in May 2011. Contaminated soil beneath the NC DOT
Right-of-Way and under the store building was unable to be removed. Because of the
petroleum concentrations remain above STGW levels under the building and near the
roadway, continued soil remediation using the SVE system is recommended.

• Based on the risk to private well users, Pyramid recommended a new air-sparge system
with deeper air sparge wells to enhance the groundwater cleanup. This new system was
designed, bid, pre-approved, and built from October 2012 through April 2013. The
system was successfully started on April 3, 2013. The new system has shown significant
reductions in the remaining petroleum contaminants.

• The continued presence of concentrations of petroleum contaminants (MW-1A, MW-
15A, and SW-2765) show that groundwater contamination remains above regulatory
closure levels.

• Continued groundwater remediation and monitoring is recommended for the site. The
next semi-annual sampling of the monitoring wells will be conducted in December 2015.

6.0 CLOSURE

This report is prepared for and made available solely for the use of T.A.C, Inc. and the NCDEQ,
and the contents thereof may not be used or relied upon by any other person without the express
written consent and authorization of Pyramid Environmental & Engineering, P.C. The
observations, conclusions, and recommendations documented in this report are based on site
conditions and information reviewed at the time of the investigation. Pyramid Environmental &
Engineering, P.C. appreciates the opportunity to provide this environmental service.

FIGURES

TABLES
TABLE 1 Monitoring Well Construction Details Harold Smith Grocery Incident #12913
Union Ridge Road, Burlington, North Carolina

WELL INSTALLED DEPTH BEDROCK CASING INTERVAL INTERVAL INTERVAL INTERVAL INTERVAL
MW-1 11/21/94 20’ NBE NA 0-10’ 10-20’ 0-6’ 6-7.5 7.5-20’
MW-1A 6/27/11 24’ NBE NA 0-4’ 4-24’ 0-1’ 1-3’ 3-24’
MW-2 10/11/95 25’ 25’ NA 0-10’ 10-20’ 0-6’ 6-8’ 8-20’
MW-3 10/11/95 22’ NBE NA 0-7’ 7-22’ 0-3’ 3-5’ 5-22’
MW-4 11/8/95 20’ NBE NA 0-5’ 5-20’ 0-2’ 2-4’ 4-20’
MW-5 11/8/95 20’ NBE NA 0-5’ 5-20’ 0-2’ 2-4’ 4-20’
MW-6 1/2/96 53’ 25’ 0-30’ 0-43’ 43-53’ 0-38’ 38-41’ 41-53’
MW-7 1/3/96 13.8’ NBE NA 0-3.8’ 3.8-13.8’ 0-0.5’ 0.5-1.5’ 1.5-13.8’
MW-8 5/6/96 14.3’ 15’ NA 0-4.3’ 4.3-14.3’ 0-1.8’ 1.8-3.3’ 3.3-14.3’
MW-9 5/6/96 15’ NBE NA 0-5’ 5-15’ 0-2.5’ 2.5-4’ 6/4-15’
MW-10 11/30/99 20’ NBE NA 0-5’ 5-20’ 0.5-2’ 2-4’ 4-20’
MW-11 7/25/00

20’ NA NA 0-5’ 5-20’ 0.5-2’ 2-4’ 4-20’
MW-12 11/6/01 30’ NBE NA 0-10’ 10-30’ 0-6’ 6-8’ 8-30’
MW-13 3/5/09 25’ NBE NA 0-5’ 5-25’ 0-1’ 1-3’ 3-25’
MW-14 3/5/09 25’ NBE NA 0-5’ 5-25’ 0-1’ 1-3’ 3-25’
MW-15 3/5/09 25’ 24’ NA 0-5’ 5-25’ 0-1’ 1-3' 3-25’
MW-15A 6/27/11 24’ NBE NA 0-4’ 4-24’ 0-1’ 1-3’ 3-24’
TS-1 12/17/99 15’ NBE NA 0-5’ 5-15’ 0-2’ 2-4’ 4-15’
TS-2 12/17/99 15’ NBE NA 0-5’ 5-15’ 0-2’ 2-4’ 4-15’
TS-3 12/17/99 15’ NBE NA 0-5’ 5-15’ 0-2’ 2-4’ 4-15’
ALL MONITORING WELLS HAVE 2” PVC CASING/RISER AND 2” PVC SCREEN WITH 0.01” SLOTS. OUTER CASING FOR TYPE III WELL IS 6” PVC.
NBE = NO BEDROCK ENCOUNTERED. NA = NOT APPLICABLE. SHADED WELLS ARE CLOSED.
Page 1 of 6
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
MW-1A installed 06-30-11 94.650 12.24 0.00 0.00 0.00 12.24 82.41
09-8-11 94.650 13.59 0.00 0.00 0.00 13.59 81.06
12-8-11 94.650 13.49 0.00 0.00 0.00 13.49 81.16
03-13-12 94.650 13.49 0.00 0.00 0.00 12.35 82.30
06-5-12 94.650 12.14 0.00 0.00 0.00 12.14 82.51
09-11-12 94.650 13.22 0.00 0.00 0.00 13.22 81.43
12-12-12 94.650 13.85 0.00 0.00 0.00 13.85 80.80
03-12-13 94.650 11.83 0.00 0.00 0.00 11.83 82.82
05-29-13 94.650 10.44 0.00 0.00 0.00 10.44 84.21
09-10-13 94.650 8.96 0.00 0.00 0.00 8.96 85.69
11-6-13 94.650 10.96 0.00 0.00 0.00 10.96 83.69
03-19-14 94.650 8.07 0.00 0.00 0.00 8.07 86.58
06-26-14 94.650 8.72 0.00 0.00 0.00 8.72 85.93
08-22-14 94.650 10.13 0.00 0.00 0.00 10.13 84.52
11-7-14 94.650 12.00 0.00 0.00 0.00 12.00 82.65
03-4-15 94.650 11.21 0.00 0.00 0.00 11.21 83.44
06-25-15 94.650 11.48 0.00 0.00 0.00 11.48 83.17
09-22-15 94.650 13.50 0.00 0.00 0.00 13.50 81.15
MW-3 09-9-09 93.065 12.03 0.00 0.00 0.00 12.03 81.04
12-3-09 93.065 10.40 0.00 0.00 0.00 10.40 82.67
03-24-10 93.065 7.34 0.00 0.00 0.00 7.34 85.73
06-24-10 93.065 8.07 0.00 0.00 0.00 8.07 85.00
09-8-10 93.065 9.62 0.00 0.00 0.00 9.62 83.45
12-10-10 93.065 10.77 0.00 0.00 0.00 10.77 82.30
03-8-11 93.065 10.60 0.00 0.00 0.00 10.60 82.47
06-30-11 93.065 10.74 0.00 0.00 0.00 10.74 82.33
09-8-11 93.065 12.16 0.00 0.00 0.00 12.16 80.91
12-8-11 93.065 12.06 0.00 0.00 0.00 12.06 81.01
03-13-12 93.065 13.49 0.00 0.00 0.00 10.52 82.55
06-5-12 93.065 10.71 0.00 0.00 0.00 10.71 82.36
09-11-12 93.065 11.79 0.00 0.00 0.00 11.79 81.28
12-12-12 93.065 12.37 0.00 0.00 0.00 12.37 80.70
03-12-13 93.065 10.53 0.00 0.00 0.00 10.53 82.54
05-29-13 93.065 9.04 0.00 0.00 0.00 9.04 84.03
09-10-13 93.065 7.53 0.00 0.00 0.00 7.53 85.54
11-6-13 93.065 8.88 0.00 0.00 0.00 8.88 84.19
03-19-14 93.065 6.69 0.00 0.00 0.00 6.69 86.38
06-26-14 93.065 7.46 0.00 0.00 0.00 7.46 85.61
08-22-14 93.065 8.82 0.00 0.00 0.00 8.82 84.25
11-7-14 93.065 10.84 0.00 0.00 0.00 10.84 82.23
03-4-15 93.065 8.51 0.00 0.00 0.00 8.51 84.56
06-25-15 93.065 10.22 0.00 0.00 0.00 10.22 82.85
09-22-15 93.065 12.35 0.00 0.00 0.00 12.35 80.72
MW-4 09-9-09 91.470 10.81 0.00 0.00 0.00 10.81 80.66
12-3-09 91.470 9.11 0.00 0.00 0.00 9.11 82.36
03-24-10 91.470 6.10 0.00 0.00 0.00 6.10 85.37
06-24-10 91.470 6.76 0.00 0.00 0.00 6.76 84.71
09-8-10 91.470 8.41 0.00 0.00 0.00 8.41 83.06
12-10-10 91.470 9.55 0.00 0.00 0.00 9.55 81.92
03-8-11 91.470 9.37 0.00 0.00 0.00 9.37 82.10
06-30-11 91.470 9.53 0.00 0.00 0.00 9.53 81.94
09-8-11 91.470 11.12 0.00 0.00 0.00 11.12 80.35
12-8-11 91.470 10.81 0.00 0.00 0.00 10.81 80.66
03-13-12 91.470 13.49 0.00 0.00 0.00 8.58 82.89
06-5-12 91.470 9.50 0.00 0.00 0.00 9.50 81.97
09-11-12 91.470 10.67 0.00 0.00 0.00 10.67 80.80
12-12-12 91.470 11.15 0.00 0.00 0.00 11.15 80.32
03-12-13 91.470 8.84 0.00 0.00 0.00 8.84 82.63
05-29-13 91.470 7.80 0.00 0.00 0.00 7.80 83.67
09-10-13 91.470 6.33 0.00 0.00 0.00 6.33 85.14
11-6-13 91.470 7.70 0.00 0.00 0.00 7.70 83.77
03-19-14 91.470 5.51 0.00 0.00 0.00 5.51 85.96
06-26-14 91.470 6.18 0.00 0.00 0.00 6.18 85.29
08-22-14 91.470 7.58 0.00 0.00 0.00 7.58 83.89
11-7-14 91.470 9.62 0.00 0.00 0.00 9.62 81.85
03-4-15 91.470 7.55 0.00 0.00 0.00 7.55 83.92
06-25-15 91.470 8.97 0.00 0.00 0.00 8.97 82.50
09-22-15 91.470 11.11 0.00 0.00 0.00 11.11 80.36
TABLE 2
Union Ridge Road, Burlington, North carolina
Groundwater Elevation Data
Harold Smith GroceryIncident #12913
Page 2 of 6
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
09-9-09 95.045 12.81 0.00 0.00 0.00 12.81 82.24
12-3-09 95.045 6.35 0.00 0.00 0.00 6.35 88.70
03-24-10 95.045 6.63 0.00 0.00 0.00 6.63 88.42
06-24-10 95.045 8.25 0.00 0.00 0.00 8.25 86.80
09-8-10 95.045 10.34 0.00 0.00 0.00 10.34 84.71
12-10-10 95.045 9.78 0.00 0.00 0.00 9.78 85.27
03-8-11 95.045 7.20 0.00 0.00 0.00 7.20 87.85
06-30-11 95.045 8.53 0.00 0.00 0.00 8.53 86.52
09-8-11 95.045 12.62 0.00 0.00 0.00 12.62 82.43
12-8-11 95.045 8.74 0.00 0.00 0.00 8.74 86.31
03-13-12 95.045 13.49 0.00 0.00 0.00 10.94 84.11
06-5-12 95.045 10.87 0.00 0.00 0.00 10.87 84.18
09-11-12 95.045 11.98 0.00 0.00 0.00 11.98 83.07
12-12-12 95.045 13.20 0.00 0.00 0.00 13.20 81.85
03-12-13 95.045 7.32 0.00 0.00 0.00 7.32 87.73
05-29-13 95.045 9.38 0.00 0.00 0.00 9.38 85.67
09-10-13 95.045 8.16 0.00 0.00 0.00 8.16 86.89
11-6-13 95.045 9.53 0.00 0.00 0.00 9.53 85.52
03-19-14 95.045 2.87 0.00 0.00 0.00 2.87 92.18
06-26-14 95.045 7.78 0.00 0.00 0.00 7.78 87.27
08-22-14 95.045 9.06 0.00 0.00 0.00 9.06 85.99
11-7-14 95.045 11.16 0.00 0.00 0.00 11.16 83.89
03-4-15 95.045 1.70*0.00 0.00 0.00 1.70*93.35
06-25-15 95.045 10.78 0.00 0.00 0.00 10.78 84.27
09-22-15 95.045 13.05 0.00 0.00 0.00 13.05 82.00
MW-6*09-9-09 94.935 14.28 0.00 0.00 0.00 14.28 80.66
12-3-09 94.935 12.98 0.00 0.00 0.00 12.98 81.96
03-24-10 94.935 9.07 0.00 0.00 0.00 9.07 85.87
06-24-10 94.935 9.90 0.00 0.00 0.00 9.90 85.04
09-8-10 94.935 11.76 0.00 0.00 0.00 11.76 83.18
12-10-10 94.935 12.91 0.00 0.00 0.00 12.91 82.03
03-8-11 94.935 12.89 0.00 0.00 0.00 12.89 82.05
06-30-11 94.935 12.91 0.00 0.00 0.00 12.91 82.03
09-8-11 94.935 14.50 0.00 0.00 0.00 14.50 80.44
12-8-11 94.935 14.20 0.00 0.00 0.00 14.20 80.74
03-13-12 94.935 13.49 0.00 0.00 0.00 12.94 82.00
06-5-12 94.935 13.10 0.00 0.00 0.00 13.10 81.84
09-11-12 94.935 14.26 0.00 0.00 0.00 14.26 80.68
12-12-12 94.935 14.58 0.00 0.00 0.00 14.58 80.36
03-12-13 94.935 12.72 0.00 0.00 0.00 12.72 82.22
05-29-13 94.935 11.38 0.00 0.00 0.00 11.38 83.56
09-10-13 94.935 9.65 0.00 0.00 0.00 9.65 85.29
11-6-13 94.935 11.29 0.00 0.00 0.00 11.29 83.65
03-19-14 94.935 8.58 0.00 0.00 0.00 8.58 86.36
06-26-14 94.935 9.39 0.00 0.00 0.00 9.39 85.55
08-22-14 94.935 11.01 0.00 0.00 0.00 11.01 83.93
11-7-14 94.935 12.99 0.00 0.00 0.00 12.99 81.95
03-4-15 94.935 12.11 0.00 0.00 0.00 12.11 82.83
06-25-15 94.935 12.43 0.00 0.00 0.00 12.43 82.51
09-22-15 94.935 14.50 0.00 0.00 0.00 14.50 80.44
MW-7 09-9-09 94.215 11.61 0.00 0.00 0.00 11.61 82.61
12-3-09 94.215 9.65 0.00 0.00 0.00 9.65 84.57
03-24-10 94.215 7.69 0.00 0.00 0.00 7.69 86.53
06-24-10 94.215 7.55 0.00 0.00 0.00 7.55 86.67
09-8-10 94.215 8.18 0.00 0.00 0.00 8.18 86.04
12-10-10 94.215 10.36 0.00 0.00 0.00 10.36 83.86
03-8-11 94.215 9.94 0.00 0.00 0.00 9.94 84.28
06-30-11 94.215 10.92 0.00 0.00 0.00 10.92 83.30
09-8-11 94.215 12.05 0.00 0.00 0.00 12.05 82.17
12-8-11 94.215 11.64 0.00 0.00 0.00 11.64 82.58
03-13-12 94.215 13.49 0.00 0.00 0.00 10.75 83.47
06-5-12 94.215 10.63 0.00 0.00 0.00 10.63 83.59
09-11-12 94.215 11.33 0.00 0.00 0.00 11.33 82.89
12-12-12 94.215 12.20 0.00 0.00 0.00 12.20 82.02
03-12-13 94.215 NG 0.00 0.00 0.00 0.00 NG
05-29-13 94.215 NG 0.00 0.00 0.00 0.00 NG
09-10-13 94.215 7.57 0.00 0.00 0.00 7.57 86.65
11-6-13 94.215 9.08 0.00 0.00 0.00 9.08 85.14
Page 3 of 6
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
06-26-14 94.215 7.47 0.00 0.00 0.00 7.47 86.75
08-22-14 94.215 8.70 0.00 0.00 0.00 8.70 85.52
11-7-14 94.215 10.60 0.00 0.00 0.00 10.60 83.62
03-4-15 94.215 9.40 0.00 0.00 0.00 9.40 84.82
06-25-15 94.215 9.96 0.00 0.00 0.00 9.96 84.26
09-22-15 94.215 11.76 0.00 0.00 0.00 11.76 82.46
MW-8 09-9-09 89.630 NG 0.00 0.00 0.00 0.00 NG
12-3-09 89.630 7.23 0.00 0.00 0.00 7.23 82.40
03-24-10 89.630 5.64 0.00 0.00 0.00 5.64 83.99
06-24-10 89.630 6.13 0.00 0.00 0.00 6.13 83.50
09-8-10 89.630 7.79 0.00 0.00 0.00 7.79 81.84
12-10-10 89.630 9.43 0.00 0.00 0.00 9.43 80.20
03-8-11 89.630 8.39 0.00 0.00 0.00 8.39 81.24
06-30-11 89.630 NG 0.00 0.00 0.00 0.00 NG
09-8-11 89.630 NG 0.00 0.00 0.00 0.00 NG
12-8-11 89.630 NG 0.00 0.00 0.00 0.00 NG
03-13-12 89.630 NG 0.00 0.00 0.00 0.00 NG
06-5-12 89.630 8.80 0.00 0.00 0.00 8.80 80.83
09-11-12 89.630 9.84 0.00 0.00 0.00 9.84 79.79
12-12-12 89.630 10.60 0.00 0.00 0.00 10.60 79.03
03-12-13 89.630 NG 0.00 0.00 0.00 0.00 NG
05-29-13 89.630 NG 0.00 0.00 0.00 0.00 NG
09-10-13 89.630 NG 0.00 0.00 0.00 0.00 NG
11-6-13 89.630 NG 0.00 0.00 0.00 0.00 NG
03-19-14 89.630 NG 0.00 0.00 0.00 0.00 NG
06-26-14 89.630 NG 0.00 0.00 0.00 0.00 NG
08-22-14 89.630 NG 0.00 0.00 0.00 0.00 NG
11-7-14 89.630 NG 0.00 0.00 0.00 0.00 NG
03-4-15 89.630 NG 0.00 0.00 0.00 0.00 NG
06-25-15 89.630 NG 0.00 0.00 0.00 0.00 NG
09-22-15 89.630 NG 0.00 0.00 0.00 0.00 NG
MW-9 09-9-09 94.770 14.21 0.00 0.00 0.00 14.21 80.56
12-3-09 94.770 12.76 0.00 0.00 0.00 12.76 82.01
03-24-10 94.770 8.91 0.00 0.00 0.00 8.91 85.86
06-24-10 94.770 9.79 0.00 0.00 0.00 9.79 84.98
09-8-10 94.770 11.70 0.00 0.00 0.00 11.70 83.07
12-10-10 94.770 12.89 0.00 0.00 0.00 12.89 81.88
03-8-11 94.770 12.79 0.00 0.00 0.00 12.79 81.98
06-30-11 94.770 NG 0.00 0.00 0.00 0.00 NG
09-8-11 94.770 14.34 0.00 0.00 0.00 14.34 80.43
12-8-11 94.770 14.09 0.00 0.00 0.00 14.09 80.68
03-13-12 94.770 13.49 0.00 0.00 0.00 11.82 82.95
06-5-12 94.770 NG 0.00 0.00 0.00 0.00 NG
09-11-12 94.770 14.15 0.00 0.00 0.00 14.15 80.62
12-12-12 94.770 NG 0.00 0.00 0.00 0.00 NG
03-12-13 94.770 12.60 0.00 0.00 0.00 12.60 82.17
05-29-13 94.770 11.20 0.00 0.00 0.00 11.20 83.57
09-10-13 94.770 9.50 0.00 0.00 0.00 9.50 85.27
11-6-13 94.770 11.16 0.00 0.00 0.00 11.16 83.61
03-19-14 94.770 8.18 0.00 0.00 0.00 8.18 86.59
06-26-14 94.770 9.30 0.00 0.00 0.00 9.30 85.47
08-22-14 94.770 10.88 0.00 0.00 0.00 10.88 83.89
11-7-14 94.770 12.92 0.00 0.00 0.00 12.92 81.85
03-4-15 94.770 12.00 0.00 0.00 0.00 12.00 82.77
06-25-15 94.770 12.27 0.00 0.00 0.00 12.27 82.50
09-22-15 94.770 14.37 0.00 0.00 0.00 14.37 80.40
MW-10 09-9-09 93.210 13.25 0.00 0.00 0.00 13.25 79.96
12-3-09 93.210 10.51 0.00 0.00 0.00 10.51 82.70
03-24-10 93.210 7.80 0.00 0.00 0.00 7.80 85.41
06-24-10 93.210 8.77 0.00 0.00 0.00 8.77 84.44
09-8-10 93.210 10.74 0.00 0.00 0.00 10.74 82.47
12-10-10 93.210 12.15 0.00 0.00 0.00 12.15 81.06
03-8-11 93.210 11.78 0.00 0.00 0.00 11.78 81.43
06-30-11 93.210 12.29 0.00 0.00 0.00 12.29 80.92
09-8-11 93.210 13.39 0.00 0.00 0.00 13.39 79.82
12-8-11 93.210 12.91 0.00 0.00 0.00 12.91 80.30
03-13-12 93.210 13.49 0.00 0.00 0.00 11.61 81.60
Page 4 of 6
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
09-11-12 93.210 13.10 0.00 0.00 0.00 13.10 80.11
12-12-12 93.210 13.29 0.00 0.00 0.00 13.29 79.92
03-12-13 93.210 10.93 0.00 0.00 0.00 10.93 82.28
05-29-13 93.210 10.03 0.00 0.00 0.00 10.03 83.18
09-10-13 93.210 8.61 0.00 0.00 0.00 8.61 84.60
11-6-13 93.210 10.11 0.00 0.00 0.00 10.11 83.10
03-19-14 93.210 6.68 0.00 0.00 0.00 6.68 86.53
06-26-14 93.210 8.43 0.00 0.00 0.00 8.43 84.78
08-22-14 93.210 10.00 0.00 0.00 0.00 10.00 83.21
11-7-14 93.210 11.98 0.00 0.00 0.00 11.98 81.23
03-4-15 93.210 10.66 0.00 0.00 0.00 10.66 82.55
06-25-15 93.210 11.35 0.00 0.00 0.00 11.35 81.86
09-22-15 93.210 13.44 0.00 0.00 0.00 13.44 79.77
MW-11 09-9-09 95.840 NG 0.00 0.00 0.00 0.00 NG
12-3-09 95.840 14.05 0.00 0.00 0.00 14.05 81.79
03-24-10 95.840 10.06 0.00 0.00 0.00 10.06 85.78
06-24-10 95.840 10.91 0.00 0.00 0.00 10.91 84.93
09-8-10 95.840 12.77 0.00 0.00 0.00 12.77 83.07
12-10-10 95.840 14.00 0.00 0.00 0.00 14.00 81.84
03-8-11 95.840 13.94 0.00 0.00 0.00 13.94 81.90
06-30-11 95.840 13.92 0.00 0.00 0.00 13.92 81.92
09-8-11 95.840 15.52 0.00 0.00 0.00 15.52 80.32
12-8-11 95.840 15.21 0.00 0.00 0.00 15.21 80.63
03-13-12 95.840 13.49 0.00 0.00 0.00 13.94 81.90
06-5-12 95.840 14.16 0.00 0.00 0.00 14.16 81.68
09-11-12 95.840 15.36 0.00 0.00 0.00 15.36 80.48
12-12-12 95.840 15.60 0.00 0.00 0.00 15.60 80.24
03-12-13 95.840 13.88 0.00 0.00 0.00 13.88 81.96
05-29-13 95.840 12.35 0.00 0.00 0.00 12.35 83.49
09-10-13 95.840 10.64 0.00 0.00 0.00 10.64 85.20
11-6-13 95.840 12.35 0.00 0.00 0.00 12.35 83.49
03-19-14 95.840 9.58 0.00 0.00 0.00 9.58 86.26
06-26-14 95.840 10.41 0.00 0.00 0.00 10.41 85.43
08-22-14 95.840 12.02 0.00 0.00 0.00 12.02 83.82
11-7-14 95.840 14.04 0.00 0.00 0.00 14.04 81.80
03-4-15 95.840 13.21 0.00 0.00 0.00 13.21 82.63
06-25-15 95.840 13.41 0.00 0.00 0.00 13.41 82.43
09-22-15 95.840 15.52 0.00 0.00 0.00 15.52 80.32
MW-12 09-9-09 94.270 14.70 0.00 0.00 0.00 14.70 79.57
12-3-09 94.270 13.45 0.00 0.00 0.00 13.45 80.82
03-24-10 94.270 9.50 0.00 0.00 0.00 9.50 84.77
06-24-10 94.270 10.36 0.00 0.00 0.00 10.36 83.91
09-8-10 94.270 12.26 0.00 0.00 0.00 12.26 82.01
12-10-10 94.270 13.43 0.00 0.00 0.00 13.43 80.84
03-8-11 94.270 13.35 0.00 0.00 0.00 13.35 80.92
06-30-11 94.270 13.42 0.00 0.00 0.00 13.42 80.85
09-8-11 94.270 15.05 0.00 0.00 0.00 15.05 79.22
12-8-11 94.270 14.66 0.00 0.00 0.00 14.66 79.61
03-13-12 94.270 13.49 0.00 0.00 0.00 13.43 80.84
06-5-12 94.270 13.58 0.00 0.00 0.00 13.58 80.69
09-11-12 94.270 14.79 0.00 0.00 0.00 14.79 79.48
12-12-12 94.270 15.04 0.00 0.00 0.00 15.04 79.23
03-12-13 94.270 13.24 0.00 0.00 0.00 13.24 81.03
05-29-13 94.270 11.79 0.00 0.00 0.00 11.79 82.48
09-10-13 94.270 10.08 0.00 0.00 0.00 10.08 84.19
11-6-13 94.270 11.73 0.00 0.00 0.00 11.73 82.54
03-19-14 94.270 8.92 0.00 0.00 0.00 8.92 85.35
06-26-14 94.270 9.86 0.00 0.00 0.00 9.86 84.41
08-22-14 94.270 11.43 0.00 0.00 0.00 11.43 82.84
11-7-14 94.270 13.45 0.00 0.00 0.00 13.45 80.82
03-4-15 94.270 12.59 0.00 0.00 0.00 12.59 81.68
06-25-15 94.270 12.82 0.00 0.00 0.00 12.82 81.45
09-22-15 94.270 14.95 0.00 0.00 0.00 14.95 79.32
MW-13 03-18-09 94.805 13.58 0.00 0.00 0.00 13.58 81.23
06-23-09 94.805 11.01 0.00 0.00 0.00 11.01 83.80
09-9-09 94.805 12.61 0.00 0.00 0.00 12.61 82.20
12-3-09 94.805 11.26 0.00 0.00 0.00 11.26 83.55
Page 5 of 6
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
06-24-10 94.805 10.56 0.00 0.00 0.00 10.56 84.25
09-8-10 94.805 9.82 0.00 0.00 0.00 9.82 84.99
12-10-10 94.805 10.93 0.00 0.00 0.00 10.93 83.88
03-8-11 94.805 11.24 0.00 0.00 0.00 11.24 83.57
06-30-11 94.805 10.73 0.00 0.00 0.00 10.73 84.08
09-8-11 94.805 12.51 0.00 0.00 0.00 12.51 82.30
12-8-11 94.805 12.69 0.00 0.00 0.00 12.69 82.12
03-13-12 94.805 13.49 0.00 0.00 0.00 10.48 84.33
06-5-12 94.805 10.28 0.00 0.00 0.00 10.28 84.53
09-11-12 94.805 11.55 0.00 0.00 0.00 11.55 83.26
12-12-12 94.805 13.55 0.00 0.00 0.00 13.55 81.26
03-12-13 94.805 10.33 0.00 0.00 0.00 10.33 84.48
05-29-13 94.805 9.41 0.00 0.00 0.00 9.41 85.40
09-10-13 94.805 7.78 0.00 0.00 0.00 7.78 87.03
11-6-13 94.805 9.36 0.00 0.00 0.00 9.36 85.45
03-19-14 94.805 6.88 0.00 0.00 0.00 6.88 87.93
06-26-14 94.805 7.53 0.00 0.00 0.00 7.53 87.28
08-22-14 94.805 8.60 0.00 0.00 0.00 8.60 86.21
11-7-14 94.805 10.69 0.00 0.00 0.00 10.69 84.12
03-4-15 94.805 9.46 0.00 0.00 0.00 9.46 85.35
06-25-15 94.805 10.11 0.00 0.00 0.00 10.11 84.70
09-22-15 94.805 12.30 0.00 0.00 0.00 12.30 82.51
MW-14 03-18-09 94.395 NG 0.00 0.00 0.00 0.00 NG
06-23-09 94.395 NG 0.00 0.00 0.00 0.00 NG
09-9-09 94.395 NG 0.00 0.00 0.00 0.00 NG
12-3-09 94.395 NG 0.00 0.00 0.00 0.00 NG
03-24-10 94.395 NG 0.00 0.00 0.00 0.00 NG
06-24-10 94.395 NG 0.00 0.00 0.00 0.00 NG
09-8-10 94.395 NG 0.00 0.00 0.00 0.00 NG
12-10-10 94.395 NG 0.00 0.00 0.00 0.00 NG
03-8-11 94.395 NG 0.00 0.00 0.00 0.00 NG
06-30-11 94.395 NG 0.00 0.00 0.00 0.00 NG
09-8-11 94.395 NG 0.00 0.00 0.00 0.00 NG
12-8-11 94.395 NG 0.00 0.00 0.00 0.00 NG
03-13-12 94.395 NG 0.00 0.00 0.00 0.00 NG
06-5-12 94.395 NG 0.00 0.00 0.00 0.00 NG
09-11-12 94.395 NG 0.00 0.00 0.00 0.00 NG
12-12-12 94.395 NG 0.00 0.00 0.00 0.00 NG
03-12-13 94.395 NG 0.00 0.00 0.00 0.00 NG
05-29-13 94.395 NG 0.00 0.00 0.00 0.00 NG
09-10-13 94.395 NG 0.00 0.00 0.00 0.00 NG
11-6-13 94.395 NG 0.00 0.00 0.00 0.00 NG
03-19-14 94.395 NG 0.00 0.00 0.00 0.00 NG
06-26-14 94.395 NG 0.00 0.00 0.00 0.00 NG
08-22-14 94.395 NG 0.00 0.00 0.00 0.00 NG
11-7-14 94.395 NG 0.00 0.00 0.00 0.00 NG
03-4-15 94.395 NG 0.00 0.00 0.00 0.00 NG
06-25-15 94.395 NG 0.00 0.00 0.00 0.00 NG
09-22-15 94.395 NG 0.00 0.00 0.00 0.00 NG
MW-15/03-18-09 93.775 13.77 0.00 0.00 0.00 13.77 80.01
MW-15A 06-23-09 93.775 9.90 0.00 0.00 0.00 9.90 83.88
09-9-09 93.775 11.57 0.00 0.00 0.00 11.57 82.21
12-3-09 93.775 11.24 0.00 0.00 0.00 11.24 82.54
03-24-10 93.775 7.57 0.00 0.00 0.00 7.57 86.21
06-24-10 93.775 8.43 0.00 0.00 0.00 8.43 85.35
09-8-10 93.775 9.67 0.00 0.00 0.00 9.67 84.11
12-10-10 93.775 11.24 0.00 0.00 0.00 11.24 82.54
03-8-11 93.775 11.42 0.00 0.00 0.00 11.42 82.36
06-30-11 94.950 12.47 0.00 0.00 0.00 12.47 82.48
09-8-11 94.950 13.88 0.00 0.00 0.00 13.88 81.07
12-8-11 94.950 13.75 0.00 0.00 0.00 13.75 81.20
03-13-12 94.950 13.49 0.00 0.00 0.00 12.60 82.35
06-5-12 94.950 12.45 0.00 0.00 0.00 12.45 82.50
09-11-12 94.950 13.51 0.00 0.00 0.00 13.51 81.44
12-12-12 94.950 14.08 0.00 0.00 0.00 14.08 80.87
03-12-13 94.950 12.07 0.00 0.00 0.00 12.07 82.88
05-29-13 94.950 8.72 0.00 0.00 0.00 8.72 86.23
09-10-13 94.950 9.17 0.00 0.00 0.00 9.17 85.78
Page 6 of 6
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
03-19-14 94.950 8.33 0.00 0.00 0.00 8.33 86.62
MW-15A 06-26-14 94.950 7.78 0.00 0.00 0.00 7.78 87.17
08-22-14 94.950 9.14 0.00 0.00 0.00 9.14 85.81
11-7-14 94.950 11.24 0.00 0.00 0.00 11.24 83.71
03-4-15 94.950 11.40 0.00 0.00 0.00 11.40 83.55
06-25-15 94.950 10.88 0.00 0.00 0.00 10.88 84.07
09-22-15 94.950 13.81 0.00 0.00 0.00 13.81 81.14
*MW-5 depth inaccurate for this event as groundwater was seeping in at time of measurement.
1 of 4
PARAMETER UNITS DATE MW-1/MW-3 MW-4 MW-5 MW-6*MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/TS-1 NCAC 2L
MW-1A MW-15A Groundwater
Standard
Benzene ug/l 03-14-07 440 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 DNE DNE DNE NS 1
06-06-07 410 <1 <1 <1 3.6 <1 <1 <1 <1 <1 2.4 DNE DNE DNE NS
08-29-07 340 <1 <1 <1 2.6 <1 <1 <1 <1 <1 6.4 DNE DNE DNE NS
12-13-07 200 <1 <1 <1 1.1 <1 <1 <1 <1 <1 9.2 DNE DNE DNE NS03-14-08 250 <1 <1 <1 24 <1 <1 <1 <1 <1 130 DNE DNE DNE NS
06-18-08 310 <1 <1 <1 NS <1 <1 <1 <1 <1 5.3 DNE DNE DNE NS
09-10-08 <100 <1 <1 <1 11.6 <1 <1 <1 <1 <1 69.5 DNE DNE DNE NS
12-03-08 18 <0.5 <0.5 <0.5 8.7 32 <0.5 <0.5 <0.5 <0.5 41 DNE DNE DNE NS
03-18-09 110 <0.5 1.9 <0.5 <0.5 5.9 <0.5 <0.5 <0.5 <0.5 3.6 <0.5 NS 520 NS
06-23-09 290 <0.5 <0.5 <0.5 <0.5 0.66 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 210 NS
09-09-09 190 <0.5 <0.5 <0.5 <0.5 0.66 NS <0.5 <0.5 NS 5.1 <0.5 NS 910 NS
12-03-09 180 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 7.5 <0.5 NS 440 NS
03-24-10 120 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 55 NS
06-24-10 30 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 98 NS
09-08-10 69.7 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1.1 <0.5 NS 37.5 NS
12-10-10 140 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1.3 <0.5 NS 5.4 NS
03-08-11 120 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 52 NS
06-30-11 18.3 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 77.1 NS
09-08-11 22 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 1.7 <0.5 NS 462 NS
12-09-11 15.4 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 0.61 <0.5 NS 384 NS
03-14-12 20 ND ND ND ND ND NS ND ND ND 0.17J ND NS 290 NS06-07-12 28 ND ND ND ND ND ND NS ND ND ND ND NS 220 NS
9/11-12/12 30.1 ND ND ND ND ND ND NS ND ND 1.2 ND NS 132 NS
12-12-12 19 ND ND ND ND ND ND NS ND ND 0.81 ND NS 91 NS
03-14-13 20.4 ND ND ND ND NS NS NS ND ND ND ND NS 82.8 NS
05-30-13 0.83 ND ND ND ND NS NS ND ND ND ND ND NS ND NS
09-10-13 5.5 ND ND ND ND ND NS ND ND ND ND ND NS 4.4 NS
11-07-13 0.5 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-20-14 0.49 ND ND ND ND ND NS ND ND ND ND ND NS 0.29 NS06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 0.15 ND ND ND 0.15 ND NS ND ND ND ND ND NS ND NS
03-04-15 ND ND ND ND ND ND NS ND ND ND ND ND NS 1.1 NS
06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
9/22-23/15 1.2 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
Toluene ug/l 03-14-07 3200 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 600
06-06-07 5200 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
08-29-07 6300 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
12-13-07 3300 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-14-08 4400 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
06-18-08 5800 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS09-10-08 1850 <1 <1 <1 <1 <1 2.72 <1 <1 <1 <10 DNE DNE DNE NS
12-03-08 28 <1 <1 <1 <1 140 5.3 <1 <1 <1 <1 DNE DNE DNE NS
03-18-09 3200 <1 <1 <1 <1 50 2.9 <1 <1 <1 <1 <0.5 NS 12000 NS
06-23-09 5700 <1 <1 <1 <1 0.69J 2.9 <1 <1 <1 <1 <1 NS 17000 NS
09-09-09 4300 <1 <1 <1 <1 <1 NS <1 <1 NS <1 <1 NS 25000 NS
12-03-09 3900 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS 30000 NS
03-24-10 3100 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 1600 NS
06-24-10 640 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 6900 NS09-08-10 1090 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 1630 NS
12-10-10 3100 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 94 NS
03-08-11 1390 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 1940 NS
06-30-11 29.6 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 600 NS
09-08-11 2.1 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 5620 NS
12-09-11 5.9 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 <0.5 <0.5 NS 6820 NS
03-14-12 5.7 ND ND ND ND ND NS ND ND ND ND ND NS 7400 NS
06-07-12 8.2 ND ND ND ND ND ND NS ND ND ND ND NS 6300 NS
9/11-12/12 8.1 ND ND ND ND ND ND NS ND ND ND ND NS 3240 NS
12-12-12 3.3 ND ND ND ND ND ND NS ND ND ND ND NS 3300 NS
03-14-13 5.4 ND ND ND ND NS NS NS ND ND ND ND NS 1860 NS
05-30-13 ND ND ND ND ND NS NS ND ND ND ND ND NS 1.8 NS
09-10-13 7.2 ND ND ND ND ND NS ND ND ND ND ND NS 66.2 NS
11-07-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-20-14 0.31 ND ND ND ND ND NS ND ND ND ND ND NS 3 NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS11-07-14 0.12 0.11 ND ND ND ND NS ND ND ND ND ND NS 0.22 NS
03-04-15 ND ND ND ND ND ND NS ND ND ND ND ND NS 58 NS
06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
9/22-23/15 ND ND ND ND ND ND NS ND ND ND ND ND NS 19 NS
Ethylbenzene ug/l 03-14-07 66 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 600
06-06-07 550 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
08-29-07 760 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
12-13-07 620 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-14-08 580 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
06-18-08 730 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
09-10-08 228 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 DNE DNE DNE NS
12-03-08 21 <1 <1 <1 <1 11 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-18-09 280 <1 <1 <1 <1 16 <1 <1 <1 <1 <1 6.3 NS 930 NS
06-23-09 870 <1 <1 <1 <1 2.5 <1 <1 <1 <1 <1 <1 NS 3000 NS
09-09-09 830 <1 <1 <1 <1 2.1 NS <1 <1 NS <1 <1 NS 2300 NS
12-03-09 990 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS 2700 NS
03-24-10 720 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 160 NS
06-24-10 250 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 1300 NS
09-08-10 625 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 215 NS
12-10-10 700 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 5.1 NS03-08-11 307 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 198 NS
06-30-11 19.7 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 140 NS
09-08-11 41.9 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 1550 NS
12-09-11 11.8 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 <0.5 <0.5 NS 1740 NS
03-14-12 11 ND ND ND ND ND NS ND ND ND ND ND NS 2200 NS
06-07-12 15 ND ND ND ND ND ND NS ND ND ND ND NS 1900 NS
9/11-12/12 22.5 ND ND ND ND ND ND NS ND ND ND ND NS 1620 NS
12-12-12 21 ND ND ND ND ND ND NS ND ND ND ND NS 1600 NS03-14-13 13.8 ND ND ND ND NS NS NS ND ND ND ND NS 1440 NS
05-30-13 0.58 ND ND ND ND NS NS ND ND ND ND ND NS 1.7 NS
09-10-13 7.3 ND ND ND ND ND NS ND ND ND ND ND NS 76.8 NS
11-07-13 1.6 ND ND ND ND ND NS ND ND ND ND ND NS 0.88 NS
03-20-14 1.1 ND ND ND ND ND NS ND ND ND ND ND NS 8 NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 0.16 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 ND ND ND ND ND ND NS ND ND ND ND ND NS 0.32 NS
03-04-15 ND ND ND ND ND ND NS ND ND ND ND ND NS 120 NS
06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
9/22-23/15 0.53 ND ND ND ND ND NS ND ND ND ND ND NS 16 NS
TABLE 3
Monitoring Well Analytical Results
Incident #12913
Harold Smith Grocery
Union Ridge Road, Burlington, North Carolina
2 of 4
PARAMETER UNITS DATE MW-1/MW-3 MW-4 MW-5 MW-6*MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/TS-1 NCAC 2L
MW-1A MW-15A Groundwater
Standard
TABLE 3
Monitoring Well Analytical Results
Incident #12913
Harold Smith Grocery
Union Ridge Road, Burlington, North Carolina
Total Xylenes ug/l 03-14-07 5700 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 DNE DNE DNE NS 500
06-06-07 7000 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 DNE DNE DNE NS
08-29-07 9600 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 DNE DNE DNE NS
12-13-07 5600 <3 <3 <3 <3 <3 <3 <3 <3 <3 27 DNE DNE DNE NS
03-14-08 6200 <3 <3 <3 <3 <3 <3 <3 <3 <3 16 DNE DNE DNE NS
06-18-08 7800 <3 <3 <3 NS <3 <3 <3 <3 <3 12 DNE DNE DNE NS
09-10-08 2377 <4 <4 <4 <4 <4 <4 <4 <4 <4 <40 DNE DNE DNE NS
12-03-08 610 <3 <3 <3 <3 1810 <3 <3 <3 <3 15 DNE DNE DNE NS
03-18-09 5500 <3 <3 <3 <3 2020 <3 13.6 <3 <3 4.7 2.3 NS 7000 NS
06-23-09 9300 <3 <3 <3 <3 71 <3 <3 <3 <3 <3 <3 NS 22400 NS
09-09-09 8700 <3 <3 <3 <3 30.1 NS <3 <3 NS 3.4 <3 NS 19300 NS
12-03-09 9300 <3 <3 <3 <3 <3 <3 <3 <3 NS 5.8 <3 NS 21200 NS
03-24-10 7800 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 NS 2600 NS06-24-10 2700 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 NS 11100 NS
09-08-10 5720 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 NS 3790 NS
12-10-10 9700 NS NS <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 0.61 <1.5 NS 162 NS
03-08-11 5700 <1.5 <1.5 <1.5 <1.5 0.66 <1.5 <1.5 <1.5 <1.5 0.82 <1.5 NS 2124 NS
06-30-11 213.2 <1.5 <1.5 <1.5 <1.5 0.66 NS NS <1.5 <1.5 5.8 <1.5 NS 602 NS
09-08-11 42.4 <1.5 <1.5 <1.5 <1.5 0.66 NS NS <1.5 <1.5 11.6 <1.5 NS 3990 NS
12-09-11 48 <1.5 <1.5 <1.5 <1.5 <1.5 NS <1.5 <1.5 <1.5 0.66 <1.5 NS 5680 NS
03-14-12 44 ND ND ND ND ND NS ND ND ND ND ND NS 8300 NS06-07-12 60 ND ND ND ND ND ND NS ND ND ND ND NS 7400 NS
9/11-12/12 73.9 ND ND ND ND ND ND NS ND ND ND ND NS 5940 NS
12-12-12 28 ND ND ND ND ND ND NS ND ND ND ND NS 7400 NS
03-14-13 44 ND ND ND ND NS NS NS ND ND ND ND NS 5600 NS
05-30-13 1.94 ND ND ND ND NS NS ND ND ND ND ND NS 7.7 NS
09-10-13 83.1 ND ND ND ND ND NS ND ND ND ND ND NS 470 NS
11-07-13 4.5 ND ND ND ND ND NS ND ND ND ND ND NS 3.76 NS
03-20-14 5.6 ND ND ND ND ND NS ND ND ND ND ND NS 32.2 NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 1.13 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 0.27 0.23 ND 0.19 0.22 0.19 NS ND ND ND ND ND NS 1.37 NS
03-04-15 3.2 ND ND ND ND ND NS ND ND ND ND ND NS 570 NS
06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
9/22-23/15 22.3 ND ND ND ND ND NS ND ND ND ND ND NS 250 NS
TOTAL BTEX ug/l 03-14-07 9406 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL DNE DNE DNE NS N/A
06-06-07 13160 BDL BDL BDL 3.6 BDL BDL BDL BDL BDL 2.4 DNE DNE DNE NS
08-29-07 17000 BDL BDL BDL 2.6 BDL BDL BDL BDL BDL 6.4 DNE DNE DNE NS
12-13-07 9720 BDL BDL BDL BDL BDL BDL BDL BDL BDL 36.2 DNE DNE DNE NS
03-14-08 11430 BDL BDL BDL 24 BDL BDL BDL BDL BDL 146 DNE DNE DNE NS
06-18-08 14640 BDL BDL BDL NS BDL BDL BDL BDL BDL 17.3 DNE DNE DNE NS09-10-08 4455 BDL BDL BDL 11.6 BDL 2.72 BDL BDL BDL 69.5 DNE DNE DNE NS
12-03-08 677 BDL BDL BDL 8.7 1993 5.3 BDL BDL BDL 56 DNE DNE DNE NS
03-18-09 9090 BDL 1.9 BDL BDL 2091.9 2.9 13.6 BDL BDL 8.3 8.6 NS 20450 NS
06-23-09 16160 BDL BDL BDL BDL 74.16 2.9 BDL BDL BDL BDL BDL NS 42610 NS
09-09-09 14020 BDL BDL BDL BDL 32.86 NS BDL BDL NS 8.5 BDL NS 47510 NS
12-03-09 14370 BRL BRL BRL BRL BRL BRL BRL BRL NS 13.3 BRL NS 54340 NS
03-24-10 11740 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS 4415 NS
06-24-10 3620 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS 19398 NS
09-08-10 7504.7 BRL BRL BRL BRL BRL BRL BRL BRL BRL 1.1 BRL NS 5672.5 NS
12-10-10 13640 NS NS BRL BRL BRL BRL BRL BRL BRL 1.91 BRL NS 266.5 NS
03-08-11 7517 ND ND ND ND 0.66 ND ND ND ND 0.82 ND NS 4314 NS
06-30-11 280.8 ND ND ND ND 0.66 NS NS ND ND 5.8 ND NS 1419.1 NS
09-08-11 108.4 ND ND ND ND 0.66 NS NS ND ND 13.3 ND NS 11622 NS
12-09-11 81.1 ND ND ND ND ND NS ND ND ND 1.27 ND NS 14624 NS
03-14-12 80.7 ND ND ND ND ND NS ND ND ND ND ND NS 18190 NS
06-07-12 111.2 ND ND ND ND ND ND NS ND ND ND ND NS 15820 NS
9/11-12/12 134.6 ND ND ND ND ND ND NS ND ND 1.2 ND NS 10932 NS12-12-12 71.3 ND ND ND ND 0.2 ND NS ND ND 0.81 ND NS 12391 NS
03-14-13 83.6 ND ND ND ND NS NS NS ND ND ND ND NS 8982.8 NS
05-30-13 3.35 ND ND ND ND NS NS ND ND ND ND ND NS 11.2 NS
09-10-13 103.1 ND ND ND ND ND NS ND ND ND ND ND NS 617.4 NS
11-07-13 6.6 ND ND ND ND ND NS ND ND ND ND ND NS 4.64 NS
03-20-14 7.19 ND ND ND ND ND NS ND ND ND ND ND NS 40.49 NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 1.29 ND ND ND ND ND NS ND ND ND ND ND NS ND NS11-07-14 0.54 0.34 ND 0.19 0.37 0.19 NS ND ND ND ND ND NS 1.91 NS
03-04-15 3.2 ND ND ND ND ND NS ND ND ND ND ND NS 749.1 NS
06-25-15 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
9/22-23/15 24.03 ND ND ND ND ND NS ND ND ND ND ND NS 285 NS
Methyl Tertiary ug/l 03-14-07 <50 <5 10 <5 4.3J <5 <5 <5 <5 <5 2.7J DNE DNE DNE NS 20Butyl Ether 06-06-07 <50 19 7.5 <5 5.9 <5 4.9J <5 <5 <5 4.1J DNE DNE DNE NS(MTBE)08-29-07 <50 73 4.6J <5 7.1 <5 <5 <5 <5 <5 4.1J DNE DNE DNE NS
12-13-07 <50 97 20 <5 8.5 <5 <5 <5 <5 <5 13 DNE DNE DNE NS
03-14-08 <50 10 6.9 <5 16 <5 <5 <5 <5 <5 74 DNE DNE DNE NS
06-18-08 <50 26 27 <5 NS <5 <5 <5 <5 <5 15 DNE DNE DNE NS
09-10-08 <200 2.3 <2 <2 6.39 <2 <2 <2 <2 <2 38.1 DNE DNE DNE NS
12-03-08 <5 2.8J 8.9 <5 9.3 5.1 <5 <5 <5 <5 75 DNE DNE DNE NS03-18-09 <50 <5 <5 <5 <5 8.2 <5 8.3 <5 <5 25 <0.5 NS <50 NS
06-23-09 <50 <5 5.4 <5 <5 3.3J <5 <5 <5 <5 11 <5 NS <50 NS
09-09-09 <50 <5 7.7 <5 <5 2.6J NS <5 <5 NS 44 <5 NS <200 NS
12-03-09 <50 <5 4J <5 <5 <5 <5 <5 <5 NS 92 <5 NS <200 NS
03-24-10 <50 <5 13 <5 <5 <5 <5 <5 <5 <5 3.3J <5 NS <200 NS
06-24-10 <50 <1 4.2 <1 <1 1.5 <1 <1 <1 <1 13 <1 NS <40 NS
09-08-10 <2.5 <0.5 1.7 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 45.8 <0.5 NS <5 NS
12-10-10 <10 NS NS <1 <1 <1 <1 <1 <1 <1 57 <1 NS <1 NS03-08-11 <10 <0.5 1.6 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 19.1 <0.5 NS <10 NS
06-30-11 2.7 <0.5 0.83 <0.5 <0.5 <0.5 NS NS 0.51 <0.5 23.8 <0.5 NS <0.5 NS
09-08-11 12.3 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS 0.54 <0.5 54.7 <0.5 NS 2.9 NS
12-09-11 9.2 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 0.52 <0.5 28.5 <0.5 NS <25 NS
03-14-12 9.6 ND 0.5 ND 0.25J ND NS ND 0.84 ND 10 ND NS ND NS
06-07-12 ND ND ND ND ND ND ND NS 1.7 ND 15 ND NS ND NS
9/11-12/12 21.4 ND ND ND ND ND ND NS 2.2 ND 33.8 ND NS ND NS
12-12-12 21 ND ND ND 0.19J ND ND NS 0.32J ND 24 ND NS ND NS
03-14-13 21.3 ND ND ND ND NS NS NS ND ND 8.4 ND NS ND NS
05-30-13 9.4 ND ND ND ND NS NS ND 0.8 ND 2 ND NS 0.61 NS
09-10-13 14.4 ND ND ND ND ND NS ND 2.9 ND 1.9 ND NS ND NS
11-07-13 9.4 ND ND ND ND ND NS ND 2.2 ND 1.2 ND NS ND NS
03-20-14 8.6 ND 0.35 ND 0.16 ND NS 1.1 0.12 ND 1.8 ND NS 0.2 NS
06-26-14 0.25 ND 0.32 ND 0.53 0.24 NS 0.3 3.2 ND 0.66 ND NS ND NS
08-22-14 4.1 ND ND ND ND ND NS 0.25 1.3 ND 0.57 ND NS ND NS
11-07-14 0.79 ND ND ND ND ND NS 1.4 1.5 ND 0.46 ND NS ND NS
03-04-15 4.6 ND ND ND 0.60J ND NS 1.6 ND ND 0.80J ND NS ND NS06-25-15 3.9 ND ND ND 0.75J ND NS ND 0.67J ND 0.68J ND NS ND NS
9/22-23/15 6.2 ND ND ND 1 ND NS ND ND ND ND ND NS ND NS
3 of 4
PARAMETER UNITS DATE MW-1/MW-3 MW-4 MW-5 MW-6*MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/TS-1 NCAC 2L
MW-1A MW-15A Groundwater
Standard
TABLE 3
Monitoring Well Analytical Results
Incident #12913
Harold Smith Grocery
Union Ridge Road, Burlington, North Carolina
Ethylene ug/l 03-14-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 0.02
Dibromide 06-06-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
(EDB)08-29-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
12-13-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-14-08 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
06-18-08 <10 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
09-10-08 <2 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 DNE DNE DNE NS
12-03-08 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-18-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <0.5 NS <50 NS
06-23-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS <50 NS
09-09-09 <10 <1 <1 <1 <1 <1 NS <1 <1 NS <1 <1 NS <40 NS
12-03-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS <40 NS
03-24-10 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS <40 NS06-24-10 14 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 28 NS
09-08-10 <2.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS <5 NS
12-10-10 <5 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 3.9 NS
03-08-11 <10 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS <10 NS
06-30-11 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 1.9 NS
09-08-11 <1.2 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 7 NS
12-09-11 <1 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 <0.5 <0.5 NS <25 NS
03-14-12 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS06-07-12 ND ND ND ND ND ND ND NS ND ND ND ND NS ND NS
9/11-12/12 ND ND ND ND ND ND ND NS ND ND ND ND NS ND NS
12-12-12 ND ND ND ND ND ND ND NS ND ND ND ND NS ND NS
03-14-13 ND ND ND ND ND NS NS NS ND ND ND ND NS ND NS
05-30-13 ND ND ND ND ND NS NS ND ND ND ND ND NS ND NS
09-10-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-20-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-04-15 NA NA NA NA NA NA NS NA NA NA NA NA NS NA NS
06-25-15 NA NA NA NA NA NA NS NA NA NA NA NA NS NA NS
9/22-23/15 NA NA NA NA NA NA NS NA NA NA NA NA NS NA NS
Isopropyl Ether ug/l 03-14-08 86 <5 3J <5 9.9 <5 <5 <5 <5 <5 270 DNE DNE DNE NS 70(IPE)06-18-08 <50 <5 13 <5 NS <5 <5 <5 <5 <5 19 DNE DNE DNE NS
09-10-08 <100 <1 <1 <1 9.28 <1 <1 <1 <1 <1 221 DNE DNE DNE NS
12-03-08 15 <5 4.6J <5 6.9 23 <5 8.1 <5 <5 200 DNE DNE DNE NS
03-18-09 <50 <5 <5 <5 <5 19 <5 10 <5 <5 69 <0.5 NS <50 NS
06-23-09 <50 <5 <5 <5 <5 6.2 <5 <5 <5 <5 10 <5 NS <50 NS09-09-09 <50 <5 3.3J <5 <5 4.9J NS <5 <5 NS 73 <5 NS <200 NS
12-03-09 <50 <5 <5 <5 <5 <5 <5 <5 <5 NS 180 <5 NS <200 NS
03-24-10 <50 <5 5.9 <5 <5 <5 <5 <5 <5 <5 3.2J <5 NS <200 NS
06-24-10 <5 <0.5 1.8 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 12 <0.5 NS <20 NS
09-08-10 2.9 <0.5 0.66 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 35.9 <0.5 NS <5 NS
12-10-10 6 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 49 <0.5 NS 1.3 NS
03-08-11 <10 <0.5 <0.5 <0.5 <0.5 0.56 <0.5 <0.5 0.82 <0.5 24.6 <0.5 NS <10 NS
06-30-11 13 <0.5 <0.5 <0.5 <0.5 0.56 NS NS 1.2 <0.5 29.2 <0.5 NS 2.7 NS
09-08-11 62.2 <0.5 <0.5 <0.5 <0.5 0.56 NS NS 0.73 <0.5 55.2 <0.5 NS 22.5 NS
12-09-11 40.9 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 29.1 <0.5 NS <25 NS
03-14-12 47 ND ND ND ND ND NS ND 0.17J ND 11 ND NS ND NS
06-07-12 78 ND ND ND ND ND ND NS 0.52J ND 12 ND NS 15J NS
9/11-12/12 94.8 ND ND ND ND ND ND NS 1.6 ND 29.8 ND NS 13.5 NS
12-12-12 120 ND ND ND 0.16J ND ND NS 1.6 ND 26 ND NS ND NS
03-14-13 112 ND ND ND ND NS NS NS ND ND 10.2 ND NS ND NS
05-30-13 32.5 ND ND ND ND NS NS 3.1 1.5 ND ND ND NS 1.5 NS
09-10-13 80.7 ND ND ND ND ND NS 3.1 6.9 ND ND ND NS 7.2 NS11-07-13 42.2 ND ND ND ND ND NS ND 3.1 1.9 ND ND NS 0.79 NS
03-20-14 46 ND ND ND 0.2 ND NS ND 3.1 1.9 0.34 ND NS 1.5 NS
06-26-14 ND ND ND ND 1.4 ND NS ND 3.3 3.1 ND ND NS ND NS
08-22-14 11 ND ND ND 0.24 ND NS ND 2.1 3.1 ND ND NS ND NS
11-07-14 2 ND ND ND ND ND NS ND 1.1 ND ND ND NS ND NS
03-04-15 27 ND ND ND ND ND NS ND ND ND 0.5 ND NS ND NS
06-25-15 11 ND ND ND ND ND NS ND 0.59 ND ND ND NS ND NS
9/22-23/15 32 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
1,2-Dichloroethane ug/l 03-14-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 0.4
06-06-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
08-29-07 <10 <1 <1 <1 <1 <1 <1 <1 1.4 <1 1.3 DNE DNE DNE NS
12-13-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 1.5 DNE DNE DNE NS
03-14-08 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 31 DNE DNE DNE NS
06-18-08 <10 <1 1.3 <1 NS <1 <1 <1 <1 <1 2.8 DNE DNE DNE NS
09-10-08 <2 <1 <1 <1 <1 <1 <1 <1 <1 <1 29.3 DNE DNE DNE NS
12-03-08 <1 <1 <1 <1 <1 4 <1 0.76J <1 <1 30 DNE DNE DNE NS
03-18-09 <10 <1 <1 <1 <1 2.1 <1 1.5 <1 <1 4.5 <0.5 NS <50 NS
06-23-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 0.69J <1 NS <50 NS
09-09-09 <10 <1 <1 <1 <1 0.64J NS <1 <1 NS 8.6 <1 NS <40 NS
12-03-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 NS 13 <1 NS <40 NS03-24-10 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS <40 NS
06-24-10 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 2.8 <0.5 <0.5 NS <20 NS
09-08-10 <2.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 6.9 <0.5 NS <5 NS
12-10-10 <5 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 11 <0.5 NS <0.5 NS
03-08-11 <10 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 7.1 <0.5 NS <10 NS
06-30-11 1.1 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 9.1 <0.5 NS 0.58 NS
09-08-11 4.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 10.9 <0.5 NS 4 NS
12-09-11 4.1 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 7.1 <0.5 NS <25 NS03-14-12 ND ND ND ND ND ND NS ND 0.33J ND 3.6 ND NS ND NS
06-07-12 ND ND ND ND ND ND ND NS ND ND 4 ND NS ND NS
9/11-12/12 13.7 ND ND ND ND ND ND NS 0.67 ND 5.9 ND NS ND NS
12-12-12 15 ND ND ND ND ND ND NS ND ND 0.81 ND NS 4.9 NS
03-14-13 14.2 ND ND ND ND NS NS NS 0.72 ND 3.3 ND NS ND NS
05-30-13 4.2 ND ND ND ND NS NS ND 1.1 ND 0.53 ND NS ND NS
09-10-13 9.2 ND ND ND ND ND NS ND 2.4 ND 0.51 ND NS 0.6 NS
11-07-13 4.1 ND ND ND ND ND NS ND 2.2 ND ND ND NS ND NS
03-20-14 4.8 ND ND ND 0.23 ND NS ND 3.2 ND ND ND NS ND NS
06-26-14 ND ND ND ND 0.32 ND NS ND 1.4 0.63 ND ND NS ND NS
08-22-14 2 ND ND ND ND ND NS ND 1.2 0.84 ND ND NS ND NS
11-07-14 ND ND ND ND ND ND NS ND 0.69 ND ND ND NS ND NS
03-04-15 2.7 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
06-25-15 1.6 ND ND ND ND ND NS ND ND 0.53 ND ND NS ND NS
9/22-23/15 3.7 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
4 of 4
PARAMETER UNITS DATE MW-1/MW-3 MW-4 MW-5 MW-6*MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/TS-1 NCAC 2L
MW-1A MW-15A Groundwater
Standard
TABLE 3
Monitoring Well Analytical Results
Incident #12913
Harold Smith Grocery
Union Ridge Road, Burlington, North Carolina
Naphthalene ug/l 03-14-08 470 <1 <1 <1 <1 <1 <1 <1 <1 <1 4.5 DNE DNE DNE NS 6
06-18-08 590 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
09-10-08 136 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 DNE DNE DNE NS
12-03-08 31 <1 <1 <1 <1 <1 <1 <1 <1 <1 3.5 DNE DNE DNE NS
03-18-09 250 <1 1.9 <1 <1 <1 <1 1.6 <1 <1 <1 6.2 NS 490 NS
06-23-09 470 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 950 NS
09-09-09 540 <1 <1 <1 <1 <1 NS <1 <1 NS <1 <1 NS 680 NS
12-03-09 490 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS 750 NS
03-24-10 550 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 220 NS
06-24-10 680 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 580 NS
09-08-10 736 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 NS 255 NS
12-10-10 520 NS NS <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 7.1 NS
03-08-11 337 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 NS 118 NS06-30-11 54.1 <2 <2 <2 <2 <2 NS NS <2 <2 3 <2 NS 41.6 NS
09-08-11 154 <2 <2 <2 <2 <2 NS NS <2 <2 5.9 <2 NS 395 NS
12-09-11 112 <2 <2 <2 <2 <2 NS <2 <2 <2 <2 <2 NS 504 NS
03-14-12 87 ND ND ND ND ND NS ND ND ND ND ND NS 130J NS
06-07-12 84 ND ND ND ND ND ND NS ND ND ND ND NS 150 NS
9/11-12/12 197 ND ND ND ND ND ND NS ND ND ND ND NS 515 NS
12-12-12 99 ND ND ND ND ND ND NS ND ND ND ND NS 250 NS
03-14-13 84.6 ND ND ND ND NS NS NS ND ND ND ND NS 344 NS05-30-13 3.4 ND ND ND ND NS NS ND ND ND ND ND NS ND NS
09-10-13 18 ND ND ND ND ND NS ND ND ND ND ND NS 2.3 NS
11-07-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-20-14 2.5 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 0.66 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-04-15 0.73J ND ND ND ND ND NS ND ND ND ND ND NS 33 NS
06-25-15 0.99J ND ND ND ND ND NS ND ND ND ND ND NS ND NS
9/22-23/15 3.2 ND ND ND ND ND NS ND ND ND ND ND NS 16 NS
NA=Not Analyzed for Parameter DNE=Did Not Exist Bold Values exceed the NCAC 2L Groundwater StandardNS=Not Sampled BDL=Below Detection Limits ND=Not Detected
Page 1 of 2
PARAMETER UNITS DATE NCAC 15A:2L
2768B 2774 2760 2773 2755 2761 2779 2765 2765 2765 2800 Groundwater
Influent Midfluent Effluent Standard
Benzene ug/l 03-24-10 <0.5 NS NS NS NS NS NS 1.7 <0.5 <0.5 NS
06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
09-08-10 NS NS NS <0.5 NS NS NS 1 <0.5 <0.5 NS12-10-10 NS NS NS <0.5 NS NS NS 0.97 <0.5 <0.5 NS 1
03-08-11 NS NS NS <0.5 NS NS <0.5 1.6 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 8.4 <0.5 <0.5 NS09-08-11 NS NS NS <0.5 NS NS <0.5 7.1 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 3.3 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND ND NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS11-07-13 ND NS NS ND NS NS ND ND NS ND NS
09-20-14 ND NS NS ND NS NS ND ND ND ND NS
06-26-14 ND NS ND ND NS NS ND 0.33 ND ND NS08-22-14 ND NS ND ND NS NS ND 0.54 ND ND NS11-07-14 ND NS ND ND NS NS ND ND ND ND NS
03-04-15 NS NS ND ND NS NS ND ND ND ND NS06-25-15 ND NS ND ND NS NS ND ND ND ND NS09-23-15 ND NS ND ND NS NS ND ND ND ND NS
Toluene ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 60003-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS05-29-13 ND NS NS ND NS NS ND ND NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS03-20-14 ND NS NS ND NS NS ND ND ND ND NS
06-26-14 ND NS ND ND NS NS ND ND ND ND NS
08-22-14 ND NS ND ND NS NS ND ND ND ND NS11-07-14 ND NS ND ND NS NS ND ND ND ND NS03-04-15 NS NS ND ND NS NS ND ND ND ND NS
06-25-15 ND NS ND ND NS NS ND ND ND ND NS09-23-15 ND NS ND ND NS NS ND ND ND ND NS
Ethylbenzene ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 600
03-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND 0.55 NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS03-20-14 ND ND ND ND NS NS ND ND ND ND NS
06-26-14 ND NS ND ND NS NS ND ND ND ND NS
08-22-14 ND NS ND ND NS NS ND 0.26 ND ND NS11-07-14 ND NS ND ND NS NS ND ND ND ND NS
03-04-15 NS NS ND ND NS NS ND ND ND ND NS
06-25-15 ND NS ND ND NS NS ND ND ND ND NS09-23-15 ND NS ND ND NS NS ND ND ND ND NS
Total Xylenes ug/l 03-24-10 <3 NS NS NS NS NS NS <3 <3 <3 NS06-24-10 NS NS NS <1.5 NS NS NS <1.5 <1.5 <1.5 NS
09-08-10 NS NS NS <1.5 NS NS NS <1.5 <1.5 <1.5 NS
12-10-10 NS NS NS <1.5 NS NS NS <1.5 <1.5 <1.5 NS 50003-08-11 NS NS NS <1.5 NS NS <1.5 <1.5 <1.5 <1.5 NS06-30-11 NS NS NS <1.5 NS NS <1.5 <3 <1.5 <1.5 NS
09-08-11 NS NS NS <1.5 NS NS <1.5 <3 <1.5 <1.5 NS12-09-11 NS NS NS <1.5 NS NS <1.5 <3 <1.5 <1.5 NS03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND ND NS ND NS09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS
03-20-14 ND ND ND ND NS NS ND ND ND ND NS06-26-14 ND NS ND ND NS NS ND ND ND ND NS
08-22-14 ND NS ND ND NS NS ND ND ND ND NS
11-07-14 ND NS ND ND NS NS ND ND ND ND NS03-04-15 NS NS ND ND NS NS ND ND ND ND NS
06-25-15 ND NS ND ND NS NS ND ND ND ND NS
09-23-15 ND NS ND ND NS NS ND ND ND ND NS
TOTAL BTEX ug/l 03-24-10 BDL NS NS NS NS NS NS 1.7 BDL BDL NS
06-24-10 NS NS NS BDL NS NS NS BDL BDL BDL NS09-08-10 NS NS NS BDL NS NS NS 1 BDL BDL NS
12-10-10 NS NS NS BDL NS NS NS 0.97 <0.5 <0.5 NS N/A
03-08-11 NS NS NS BDL NS NS BDL 1.6 BDL BDL NS06-30-11 NS NS NS BDL NS NS BDL 8.4 BDL BDL NS09-08-11 NS NS NS BDL NS NS BDL 7.1 BDL BDL NS
12-09-11 NS NS NS BDL NS NS BDL 3.3 BDL BDL NS03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS12-12-12 NS NS NS ND NS NS ND ND NS ND NS03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND 0.55 NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS11-07-13 ND NS NS ND NS NS ND ND NS ND NS
03-20-14 ND ND ND ND NS NS ND ND ND ND NS
06-26-14 ND NS ND ND NS NS ND 0.33 ND ND NS08-22-14 ND NS ND ND NS NS ND 0.8 ND ND NS
11-07-14 ND NS ND ND NS NS ND ND ND ND NS
03-04-15 NS NS ND ND NS NS ND ND ND ND NS06-25-15 ND NS ND ND NS NS ND ND ND ND NS
09-23-15 ND NS ND ND NS NS ND ND ND ND NS
Methyl Tertiary ug/l 03-24-10 22 NS NS NS NS NS NS 98 <5 <5 NS
Butyl Ether 06-24-10 NS NS NS <1 NS NS NS <1 <1 <1 NS
(MTBE)09-08-10 NS NS NS <1 NS NS NS 84.8 <1 <1 NS12-10-10 NS NS NS <1 NS NS NS 100 <1 <1 NS 20
03-08-11 NS NS NS <0.5 NS NS <0.5 166 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 125 <0.5 <0.5 NS09-08-11 NS NS NS <0.5 NS NS <0.5 136 <0.5 <0.5 NS12-09-11 NS NS NS <0.5 NS NS <0.5 150 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS9/11-12/2012 NS NS NS ND NS NS ND 149 NS ND NS
12-12-12 NS NS NS ND NS NS ND 140 NS ND NS03-14-13 ND NS NS ND NS NS ND 157 NS ND NS05-29-13 ND NS NS ND NS NS ND 150 NS ND NS
09-10-13 ND NS NS ND NS NS ND 128 NS ND NS
11-07-13 ND NS NS ND NS NS ND 117 NS ND NS03-20-14 ND ND ND 0.81 NS NS ND 140 ND 0.62 NS
06-26-14 ND NS ND 0.23 NS NS ND 120 ND ND NS
08-22-14 ND NS ND 0.18 NS NS ND 120 ND 0.28 NS11-07-14 ND NS ND ND NS NS ND 130 ND ND NS
03-04-15 NS NS ND 0.79J NS NS ND 80 ND ND NS
06-25-15 ND NS ND 0.57J NS NS ND 57 ND ND NS09-23-15 ND NS ND ND NS NS ND 70 ND ND NS
SUPPLY WELL
Union Ridge Road, Burlington, North Carolina
TABLE 4
Water Supply Well Analytical Results
Harold Smith Grocery
Incident #12913
Page 2 of 2
PARAMETER UNITS DATE NCAC 15A:2L
2768B 2774 2760 2773 2755 2761 2779 2765 2765 2765 2800 Groundwater
Influent Midfluent Effluent Standard
SUPPLY WELL
Union Ridge Road, Burlington, North Carolina
TABLE 4
Water Supply Well Analytical Results
Harold Smith Grocery
Incident #12913
Ethylene ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS
Dibromide 06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
(EDB)09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 0.02
03-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND ND NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS11-07-13 ND NS NS ND NS NS ND ND NS ND NS03-20-14 ND ND ND ND NS NS ND ND ND ND NS
06-26-14 ND NS ND ND NS NS ND ND ND ND NS08-22-14 ND NS ND ND NS NS ND ND ND ND NS11-07-14 ND NS ND ND NS NS ND ND ND ND NS
03-04-15 NS NS NA NA NS NS NA NA NA NA NS06-25-15 NA NS NA NA NS NS NA NA NA NA NS09-23-15 NA NS NA NA NS NS NA NA NA NA NS
Isopropyl Ether ug/l 03-24-10 11 NS NS NS NS NS NS 130 <5 <5 NS(IPE)06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
09-08-10 NS NS NS <0.5 NS NS NS 104 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS 150 <0.5 <0.5 NS 7003-08-11 NS NS NS <0.5 NS NS <0.5 260 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 191 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 206 <0.5 NS12-09-11 NS NS NS <0.5 NS NS <0.5 178 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS9/11-12/2012 NS NS NS ND NS NS ND 149 NS ND NS
12-12-12 NS NS NS ND NS NS ND 150 NS ND NS
03-14-13 ND NS NS ND NS NS ND 159 NS ND NS05-29-13 ND NS NS ND NS NS ND 168 NS ND NS
09-10-13 ND NS NS 0.96 NS NS ND 183 NS ND NS
11-07-13 ND NS NS 1.96 NS NS ND 138 NS ND NS03-20-14 ND ND ND 0.67 NS NS ND 140 ND 0.2 NS06-26-14 ND NS ND ND NS NS ND 160 ND ND NS
08-22-14 ND NS ND ND NS NS ND 150 ND ND NS11-07-14 ND NS ND ND NS NS ND 160 ND ND NS03-04-15 NS NS ND ND NS NS ND 100 ND ND NS
06-25-15 ND NS ND ND NS NS ND 68 ND ND NS09-23-15 ND NS ND ND NS NS ND 74 ND ND NS
1,2- Dichloroethane ug/l 03-24-10 <1 NS NS NS NS NS NS 6.2 <1 <1 NS
06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS09-08-10 NS NS NS <0.5 NS NS NS 15.7 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS 19 <0.5 <0.5 NS 0.4
03-08-11 NS NS NS <0.5 NS NS <0.5 33.1 <0.5 <0.5 NS06-30-11 NS NS NS <0.5 NS NS <0.5 28 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 27.4 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 26.6 <0.5 <0.5 NS03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND 20.8 NS ND NS12-12-12 NS NS NS 0.19J NS NS ND 23 NS ND NS
03-14-13 ND NS NS ND NS NS ND 31.5 NS ND NS
05-29-13 ND NS NS ND NS NS ND 25.9 NS ND NS09-10-13 ND NS NS ND NS NS ND 25.7 NS ND NS
11-07-13 ND NS NS ND NS NS ND 20.1 NS ND NS
03-20-14 ND ND ND 0.44 NS NS ND 20 ND ND NS06-26-14 ND NS ND 0.31 NS NS ND 24 ND ND NS08-22-14 ND NS ND ND NS NS ND 24 ND ND NS
11-07-14 ND NS ND ND NS NS ND 27 ND ND NS03-04-15 NS NS ND ND NS NS ND 16 ND ND NS06-25-15 ND NS ND ND NS NS ND 12 ND ND NS
09-23-15 ND NS ND ND NS NS ND 13 ND ND NS
1,2-Dichloropropane ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS
06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 0.6
03-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND ND NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS11-07-13 ND NS NS ND NS NS ND ND NS ND NS
03-20-14 ND ND ND ND NS NS ND ND ND ND NS
06-26-14 ND NS ND ND NS NS ND ND ND ND NS08-22-14 ND NS ND ND NS NS ND ND ND ND NS11-07-14 ND NS ND ND NS NS ND ND ND ND NS
03-04-15 NS NS ND ND NS NS ND ND ND ND NS06-25-15 ND NS ND ND NS NS ND ND ND ND NS09-23-15 ND NS ND ND NS NS ND ND ND ND NS
Chloroform 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS03-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 70
06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS05-29-13 ND NS NS ND NS NS ND ND NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS03-20-14 ND ND ND ND NS NS ND ND ND ND NS
06-26-14 ND NS ND ND NS NS ND 1.1 ND ND NS
08-22-14 ND NS ND ND NS NS ND ND ND 1.6 NS11-07-14 ND NS ND ND NS NS ND ND ND ND NS03-04-15 NS NS ND ND NS NS ND ND ND ND NS
06-25-15 ND NS ND ND NS NS ND ND ND ND NS09-23-15 ND NS ND ND NS NS ND ND ND ND NS
TABLE 5 System Operation Parameters
Harold Smith Grocery
Incident #12913 Union Ridge Road, Burlington, North Carolina
DATE: TEMP. (°F) FLOW (SCFM) VACUUM (IN.-H2O) TEMP. (°F) PRESSURE (PSI)
1/6/09 65 120 9 180 15
2/4/09 55 115 9 175 12
3/16/09 55 115 8 170 10
4/2/09 75 115 7 180 10
5/6/09 78 115 8 184 10
6/5/09 70 115 6 175 10
7/6/09 80 115 8 NR 10
8/10/09 78 115 8 NR 10
9/8/09 76 115 8 NR 9
10/5/09 72 115 7 NR 7
11/2/09 70 115 6 NR 5
12/13/09 58 115 7 NR 5
1/6/10 36 115 8 NR 3
2/18/10 42 115 8 NR 12
3/5/10 56 115 7 NR 12
3/31/10 50 115 8 NR 12
5/24/10 70 115 8 NR 14
6/25/10 75 110 7 NR 14
7/27/10 75 110 6 NR 12
8/6/10 90 110 6 NR 12
9/2/10 90 110 6 NR 11
10/1/10 85 115 6 NR 10
11/10/10 50 115 6 NR 12
12/7/10 45 115 6 NR 12
1/6/11 40 110 6 NR 12
2/3/11 45 110 6 NR 12
3/15/11 55 110 6 NR 12
SYSTEM OFF – SOIL EXCAVATION
1/6/12 OFF OFF OFF NR 10
2/10/12 OFF OFF OFF NR 10
3/19/12 OFF OFF OFF NR 10
4/4/12 OFF OFF OFF NR 10
5/3/12 OFF OFF OFF NR 10
6/1/12 OFF OFF OFF NR 9
7/3/12 OFF OFF OFF NR 9
8/3/12 OFF OFF OFF NR 9
9/21/12 OFF OFF OFF NR OFF
10/3/12 OFF OFF OFF NR OFF
11/19/12 OFF OFF OFF NR OFF
12/14/12 OFF OFF OFF NR OFF
1/28/13 OFF OFF OFF NR OFF
2/25/13 OFF OFF OFF NR OFF
3/19/13 OFF OFF OFF NR OFF
TABLE 5 System Operation Parameters
Harold Smith Grocery
Incident #12913 Union Ridge Road, Burlington, North Carolina
DATE: TEMP. (°F) FLOW (SCFM) VACUUM (IN.-H2O) TEMP. (°F) PRESSURE (PSI)
5/30/13 OFF OFF OFF NR OFF
6/19/13 OFF OFF OFF NR OFF
7/9/13 OFF OFF OFF NR OFF
8/9/13 OFF OFF OFF NR OFF
9/15/3 OFF OFF OFF NR OFF
10/22/13 OFF OFF OFF NR OFF
11/5/13 OFF OFF OFF NR OFF
12/12/13 40 110 5 NR 8
1/10/14 50 110 5 NR 8
2/4/14 40 110 5 NR 8
3/1/14 42 110 5 NR 8
3/25/14 50 110 5 NR 8
5/29/14 80 110 5 NR 8
6/9/14 75 110 5 NR 7
6/30/14 90 110 5 NR 8
8/5/14 80 110 5 NR 8
9/3/14 85 110 5 NR 8
9/26/14 70 110 5 NR 8
11/12/14 50 110 5 NR 8
12/12/14 45 110 5 NR 8
1/21/15 50 110 5 NR 8
1/30/15 50 110 5 NR 8
3/11/15 60 110 5 NR 8
4/13/15 70 110 5 NR 8
5/15/15 70 110 5 NR 8
6/4/15 70 110 5 NR 8
6/29/15 85 110 5 NR 8
7/27/15 85 110 5 NR 8
8/26/15 80 110 5 NR 8

* Individual pressure (in psi) and flow (in scfm) at each sparge well. NR = not recorded.
TABLE 5 System Operation Parameters
Harold Smith Grocery
Incident #12913 Union Ridge Road, Burlington, North Carolina
DATE: PRES./ AS-2 PRES./
AS-3 PRES./
AS-4 PRES./
AS-5 PRES./
AS-6 PRES./
AS-7 PRES./
AS-8 PRES./
TABLE 5 System Operation Parameters
Harold Smith Grocery
Incident #12913 Union Ridge Road, Burlington, North Carolina
DATE: PRES./ AS-2 PRES./
AS-3 PRES./
AS-4 PRES./
AS-5 PRES./
AS-6 PRES./
AS-7 PRES./
AS-8 PRES./
Individual pressure (in psi) and flow (in scfm) at each sparge well. NR = not recorded.

APPENDIX A

This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
Case Narrative
10/09/2015
Pyramid Environmental, Inc
Brett Higgins
PO Box 16265
Greensboro, NC 27416-0265
Project: Harold Smith
Lab Submittal Date: 09/24/2015
Prism Work Order: 5090446
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services
Reviewed ByAngela D. Overcash Robbi A. Jones For Angela D. Overcash
President/Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 55
Data Qualifiers Key Reference:
A CCV result below the control limit. Analyte not detected down to the MDL.
Aa LCS & LCSD result are above the control limits. CCV recovery within the limits. Standard issue is believed to be the
case. No further action taken.
CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken.
CVL CCV result is below the control limits. LCS recovery within the limits. Analyte not detected in the sample. No further
action taken.
H Compound reported with possible high bias. LCS recovery above the QC limit.
L Parameter reported with possible low bias. LCS recovery below the QC limit.
L1 LCS recovery outside of the QC limits. LCSD recovery within the limits. No further action taken.
L2 LCSD recovery outside of the QC limits. LCS recovery within the limits. No further action taken.
LCD2 LCS/LCSD RPD Value outside of the control limits. LCS and LCSD Values within the control limits.
LH High LCS recovery. Analyte not detected in the sample(s). No further action taken.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 55
Sample Receipt Summary
10/09/2015
Prism Work Order: 5090446
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
5090446-01 09/22/15MW3 09/24/15Water
5090446-02 09/22/15MW4 09/24/15Water
5090446-03 09/22/15MW7 09/24/15Water
5090446-04 09/22/15MW9 09/24/15Water
5090446-05 09/22/15MW10 09/24/15Water
5090446-06 09/22/15MW11 09/24/15Water
5090446-07 09/22/15MW12 09/24/15Water
5090446-08 09/22/15MW13 09/24/15Water
5090446-09 09/23/15MW1A 09/24/15Water
5090446-10 09/23/15MW5 09/24/15Water
5090446-11 09/23/15MW6 09/24/15Water
5090446-12 09/23/15MW15A 09/24/15Water
5090446-13 09/23/152760 09/24/15Water
5090446-14 09/23/152768B 09/24/15Water
5090446-15 09/23/152779 09/24/15Water
5090446-16 09/23/152773 09/24/15Water
5090446-17 09/23/152765I 09/24/15Water
5090446-18 09/23/152765M 09/24/15Water
5090446-19 09/23/152765E 09/24/15Water
Samples were received in good condition at 1.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 55
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 5090446
10/09/2015
Summary of Detections
42 ug/L5090446-09 MW1A 1,2,4-Trimethylbenzene SM6200 B
3.7 ug/L5090446-09 MW1A 1,2-Dichloroethane SM6200 B
18 ug/L5090446-09 MW1A 1,3,5-Trimethylbenzene SM6200 B
1.2 ug/L5090446-09 MW1A Benzene SM6200 B
0.53 ug/L5090446-09 MW1A Ethylbenzene SM6200 B
32 ug/L5090446-09 MW1A Isopropyl Ether SM6200 B
0.52 ug/L5090446-09 MW1A Isopropylbenzene (Cumene)SM6200 B
13 ug/L5090446-09 MW1A m,p-Xylenes SM6200 B
6.2 ug/L5090446-09 MW1A Methyl-tert-Butyl Ether SM6200 B
3.2 ug/L5090446-09 MW1A Naphthalene SM6200 B
0.80 ug/L5090446-09 MW1A n-Propylbenzene SM6200 B
9.3 ug/L5090446-09 MW1A o-Xylene SM6200 B
22 ug/L5090446-09 MW1A Xylenes, total SM6200 B
1.0 ug/L5090446-11 MW6 Methyl-tert-Butyl Ether SM6200 B
50 ug/L5090446-12 MW15A 1,2,4-Trimethylbenzene SM6200 B
19 ug/L5090446-12 MW15A 1,3,5-Trimethylbenzene SM6200 B
0.80 ug/L5090446-12 MW15A 4-Isopropyltoluene SM6200 B
16 ug/L5090446-12 MW15A Ethylbenzene SM6200 B
2.7 ug/L5090446-12 MW15A Isopropylbenzene (Cumene)SM6200 B
130 ug/L5090446-12 MW15A m,p-Xylenes SM6200 B
16 ug/L5090446-12 MW15A Naphthalene SM6200 B
1.0 ug/L5090446-12 MW15A n-Butylbenzene SM6200 B
2.4 ug/L5090446-12 MW15A n-Propylbenzene SM6200 B
120 ug/L5090446-12 MW15A o-Xylene SM6200 B
0.52 ug/L5090446-12 MW15A Styrene SM6200 B
19 ug/L5090446-12 MW15A Toluene SM6200 B
250 ug/L5090446-12 MW15A Xylenes, total SM6200 B
2.4 ug/L5090446-16 2773 trans-1,2-Dichloroethylene SM6200 B
13 ug/L5090446-17 2765I 1,2-Dichloroethane SM6200 B
74 ug/L5090446-17 2765I Isopropyl Ether SM6200 B
0.56 H ug/L5090446-17 2765I Isopropylbenzene (Cumene)SM6200 B
70 ug/L5090446-17 2765I Methyl-tert-Butyl Ether SM6200 B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW3
Prism Sample ID: 5090446-01
Prism Work Order: 5090446
Time Collected: 09/22/15 12:35
Time Submitted: 09/24/15 16:10
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5J001112.0 9/30/15 19:15 CGPug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.111,2-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5J001112.0 9/30/15 19:15 CGPCCVug/L 0.112,2-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.0662-Chlorotoluene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.0504-Chlorotoluene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5J00111109/30/15 19:15 CGPug/L 0.31Acetone
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.048Benzene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.057Bromobenzene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.14Bromochloromethane
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.062Bromodichloromethane
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.040Bromoform
BRL SM6200 B P5J001111.0 9/30/15 19:15 CGPug/L 0.18Bromomethane
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.062Chlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.22Chloroethane
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.076Chloroform
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.079Chloromethane
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.081Dibromochloromethane
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.065Dibromomethane
BRL SM6200 B P5J001111.0 9/30/15 19:15 CGPug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5J001112009/30/15 19:15 CGPug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW3
Prism Sample ID: 5090446-01
Prism Work Order: 5090446
Time Collected: 09/22/15 12:35
Time Submitted: 09/24/15 16:10
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.061Ethylbenzene
BRL SM6200 B P5J001112.0 9/30/15 19:15 CGPug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.050Isopropyl Ether
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5J001111.0 9/30/15 19:15 CGPug/L 0.12m,p-Xylenes
BRL SM6200 B P5J001111.0 9/30/15 19:15 CGPug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5J001115.0 9/30/15 19:15 CGPug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5J001111.0 9/30/15 19:15 CGPug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5J001112.0 9/30/15 19:15 CGPug/L 0.083Methylene Chloride
BRL SM6200 B P5J001111.0 9/30/15 19:15 CGPug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5J001111.0 9/30/15 19:15 CGPug/L 0.19Naphthalene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.076n-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.087n-Propylbenzene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.044o-Xylene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.076sec-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.047Styrene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.088tert-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.098Tetrachloroethylene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.044Toluene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.078Trichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5J001115.0 9/30/15 19:15 CGPAug/L 0.060Vinyl acetate
BRL SM6200 B P5J001110.50 9/30/15 19:15 CGPug/L 0.097Vinyl chloride
BRL SM6200 B P5J001111.5 9/30/15 19:15 CGPug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13095 %4-Bromofluorobenzene
70-130101 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW4
Prism Sample ID: 5090446-02
Prism Work Order: 5090446
Time Collected: 09/22/15 11:30
Time Submitted: 09/24/15 16:10
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5J001112.0 9/30/15 19:49 CGPug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.111,2-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5J001112.0 9/30/15 19:49 CGPCCVug/L 0.112,2-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.0662-Chlorotoluene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.0504-Chlorotoluene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5J00111109/30/15 19:49 CGPug/L 0.31Acetone
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.048Benzene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.057Bromobenzene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.14Bromochloromethane
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.062Bromodichloromethane
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.040Bromoform
BRL SM6200 B P5J001111.0 9/30/15 19:49 CGPug/L 0.18Bromomethane
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.062Chlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.22Chloroethane
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.076Chloroform
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.079Chloromethane
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.081Dibromochloromethane
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.065Dibromomethane
BRL SM6200 B P5J001111.0 9/30/15 19:49 CGPug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5J001112009/30/15 19:49 CGPug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW4
Prism Sample ID: 5090446-02
Prism Work Order: 5090446
Time Collected: 09/22/15 11:30
Time Submitted: 09/24/15 16:10
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.061Ethylbenzene
BRL SM6200 B P5J001112.0 9/30/15 19:49 CGPug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.050Isopropyl Ether
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5J001111.0 9/30/15 19:49 CGPug/L 0.12m,p-Xylenes
BRL SM6200 B P5J001111.0 9/30/15 19:49 CGPug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5J001115.0 9/30/15 19:49 CGPug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5J001111.0 9/30/15 19:49 CGPug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5J001112.0 9/30/15 19:49 CGPug/L 0.083Methylene Chloride
BRL SM6200 B P5J001111.0 9/30/15 19:49 CGPug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5J001111.0 9/30/15 19:49 CGPug/L 0.19Naphthalene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.076n-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.087n-Propylbenzene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.044o-Xylene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.076sec-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.047Styrene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.088tert-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.098Tetrachloroethylene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.044Toluene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.078Trichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5J001115.0 9/30/15 19:49 CGPAug/L 0.060Vinyl acetate
BRL SM6200 B P5J001110.50 9/30/15 19:49 CGPug/L 0.097Vinyl chloride
BRL SM6200 B P5J001111.5 9/30/15 19:49 CGPug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13097 %4-Bromofluorobenzene
70-13099 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW7
Prism Sample ID: 5090446-03
Prism Work Order: 5090446
Time Collected: 09/22/15 12:00
Time Submitted: 09/24/15 16:10
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5J001112.0 9/30/15 20:24 CGPug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.111,2-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5J001112.0 9/30/15 20:24 CGPCCVug/L 0.112,2-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.0662-Chlorotoluene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.0504-Chlorotoluene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5J00111109/30/15 20:24 CGPug/L 0.31Acetone
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.048Benzene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.057Bromobenzene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.14Bromochloromethane
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.062Bromodichloromethane
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.040Bromoform
BRL SM6200 B P5J001111.0 9/30/15 20:24 CGPug/L 0.18Bromomethane
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.062Chlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.22Chloroethane
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.076Chloroform
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.079Chloromethane
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.081Dibromochloromethane
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.065Dibromomethane
BRL SM6200 B P5J001111.0 9/30/15 20:24 CGPug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5J001112009/30/15 20:24 CGPug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW7
Prism Sample ID: 5090446-03
Prism Work Order: 5090446
Time Collected: 09/22/15 12:00
Time Submitted: 09/24/15 16:10
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.061Ethylbenzene
BRL SM6200 B P5J001112.0 9/30/15 20:24 CGPug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.050Isopropyl Ether
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5J001111.0 9/30/15 20:24 CGPug/L 0.12m,p-Xylenes
BRL SM6200 B P5J001111.0 9/30/15 20:24 CGPug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5J001115.0 9/30/15 20:24 CGPug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5J001111.0 9/30/15 20:24 CGPug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5J001112.0 9/30/15 20:24 CGPug/L 0.083Methylene Chloride
BRL SM6200 B P5J001111.0 9/30/15 20:24 CGPug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5J001111.0 9/30/15 20:24 CGPug/L 0.19Naphthalene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.076n-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.087n-Propylbenzene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.044o-Xylene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.076sec-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.047Styrene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.088tert-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.098Tetrachloroethylene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.044Toluene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.078Trichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5J001115.0 9/30/15 20:24 CGPAug/L 0.060Vinyl acetate
BRL SM6200 B P5J001110.50 9/30/15 20:24 CGPug/L 0.097Vinyl chloride
BRL SM6200 B P5J001111.5 9/30/15 20:24 CGPug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13094 %4-Bromofluorobenzene
70-130101 %Dibromofluoromethane
70-13096 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW9
Prism Sample ID: 5090446-04
Prism Work Order: 5090446
Time Collected: 09/22/15 14:00
Time Submitted: 09/24/15 16:10
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5J001112.0 9/30/15 20:58 CGPug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.111,2-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5J001112.0 9/30/15 20:58 CGPCCVug/L 0.112,2-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.0662-Chlorotoluene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.0504-Chlorotoluene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5J00111109/30/15 20:58 CGPug/L 0.31Acetone
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.048Benzene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.057Bromobenzene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.14Bromochloromethane
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.062Bromodichloromethane
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.040Bromoform
BRL SM6200 B P5J001111.0 9/30/15 20:58 CGPug/L 0.18Bromomethane
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.062Chlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.22Chloroethane
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.076Chloroform
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.079Chloromethane
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.081Dibromochloromethane
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.065Dibromomethane
BRL SM6200 B P5J001111.0 9/30/15 20:58 CGPug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5J001112009/30/15 20:58 CGPug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW9
Prism Sample ID: 5090446-04
Prism Work Order: 5090446
Time Collected: 09/22/15 14:00
Time Submitted: 09/24/15 16:10
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.061Ethylbenzene
BRL SM6200 B P5J001112.0 9/30/15 20:58 CGPug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.050Isopropyl Ether
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5J001111.0 9/30/15 20:58 CGPug/L 0.12m,p-Xylenes
BRL SM6200 B P5J001111.0 9/30/15 20:58 CGPug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5J001115.0 9/30/15 20:58 CGPug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5J001111.0 9/30/15 20:58 CGPug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5J001112.0 9/30/15 20:58 CGPug/L 0.083Methylene Chloride
BRL SM6200 B P5J001111.0 9/30/15 20:58 CGPug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5J001111.0 9/30/15 20:58 CGPug/L 0.19Naphthalene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.076n-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.087n-Propylbenzene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.044o-Xylene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.076sec-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.047Styrene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.088tert-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.098Tetrachloroethylene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.044Toluene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.078Trichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5J001115.0 9/30/15 20:58 CGPAug/L 0.060Vinyl acetate
BRL SM6200 B P5J001110.50 9/30/15 20:58 CGPug/L 0.097Vinyl chloride
BRL SM6200 B P5J001111.5 9/30/15 20:58 CGPug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13092 %4-Bromofluorobenzene
70-130104 %Dibromofluoromethane
70-13095 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW10
Prism Sample ID: 5090446-05
Prism Work Order: 5090446
Time Collected: 09/22/15 13:30
Time Submitted: 09/24/15 16:10
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5J001112.0 9/30/15 21:32 CGPug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.111,2-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5J001112.0 9/30/15 21:32 CGPCCVug/L 0.112,2-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.0662-Chlorotoluene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.0504-Chlorotoluene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5J00111109/30/15 21:32 CGPug/L 0.31Acetone
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.048Benzene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.057Bromobenzene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.14Bromochloromethane
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.062Bromodichloromethane
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.040Bromoform
BRL SM6200 B P5J001111.0 9/30/15 21:32 CGPug/L 0.18Bromomethane
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.062Chlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.22Chloroethane
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.076Chloroform
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.079Chloromethane
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.081Dibromochloromethane
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.065Dibromomethane
BRL SM6200 B P5J001111.0 9/30/15 21:32 CGPug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5J001112009/30/15 21:32 CGPug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW10
Prism Sample ID: 5090446-05
Prism Work Order: 5090446
Time Collected: 09/22/15 13:30
Time Submitted: 09/24/15 16:10
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.061Ethylbenzene
BRL SM6200 B P5J001112.0 9/30/15 21:32 CGPug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.050Isopropyl Ether
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5J001111.0 9/30/15 21:32 CGPug/L 0.12m,p-Xylenes
BRL SM6200 B P5J001111.0 9/30/15 21:32 CGPug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5J001115.0 9/30/15 21:32 CGPug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5J001111.0 9/30/15 21:32 CGPug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5J001112.0 9/30/15 21:32 CGPug/L 0.083Methylene Chloride
BRL SM6200 B P5J001111.0 9/30/15 21:32 CGPug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5J001111.0 9/30/15 21:32 CGPug/L 0.19Naphthalene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.076n-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.087n-Propylbenzene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.044o-Xylene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.076sec-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.047Styrene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.088tert-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.098Tetrachloroethylene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.044Toluene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.078Trichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5J001115.0 9/30/15 21:32 CGPAug/L 0.060Vinyl acetate
BRL SM6200 B P5J001110.50 9/30/15 21:32 CGPug/L 0.097Vinyl chloride
BRL SM6200 B P5J001111.5 9/30/15 21:32 CGPug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13093 %4-Bromofluorobenzene
70-130105 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW11
Prism Sample ID: 5090446-06
Prism Work Order: 5090446
Time Collected: 09/22/15 15:00
Time Submitted: 09/24/15 16:10
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5J001112.0 9/30/15 22:06 CGPug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.111,2-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5J001112.0 9/30/15 22:06 CGPCCVug/L 0.112,2-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.0662-Chlorotoluene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.0504-Chlorotoluene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5J00111109/30/15 22:06 CGPug/L 0.31Acetone
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.048Benzene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.057Bromobenzene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.14Bromochloromethane
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.062Bromodichloromethane
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.040Bromoform
BRL SM6200 B P5J001111.0 9/30/15 22:06 CGPug/L 0.18Bromomethane
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.062Chlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.22Chloroethane
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.076Chloroform
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.079Chloromethane
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.081Dibromochloromethane
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.065Dibromomethane
BRL SM6200 B P5J001111.0 9/30/15 22:06 CGPug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5J001112009/30/15 22:06 CGPug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW11
Prism Sample ID: 5090446-06
Prism Work Order: 5090446
Time Collected: 09/22/15 15:00
Time Submitted: 09/24/15 16:10
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.061Ethylbenzene
BRL SM6200 B P5J001112.0 9/30/15 22:06 CGPug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.050Isopropyl Ether
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5J001111.0 9/30/15 22:06 CGPug/L 0.12m,p-Xylenes
BRL SM6200 B P5J001111.0 9/30/15 22:06 CGPug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5J001115.0 9/30/15 22:06 CGPug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5J001111.0 9/30/15 22:06 CGPug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5J001112.0 9/30/15 22:06 CGPug/L 0.083Methylene Chloride
BRL SM6200 B P5J001111.0 9/30/15 22:06 CGPug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5J001111.0 9/30/15 22:06 CGPug/L 0.19Naphthalene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.076n-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.087n-Propylbenzene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.044o-Xylene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.076sec-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.047Styrene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.088tert-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.098Tetrachloroethylene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.044Toluene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.078Trichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5J001115.0 9/30/15 22:06 CGPAug/L 0.060Vinyl acetate
BRL SM6200 B P5J001110.50 9/30/15 22:06 CGPug/L 0.097Vinyl chloride
BRL SM6200 B P5J001111.5 9/30/15 22:06 CGPug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13094 %4-Bromofluorobenzene
70-130102 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW12
Prism Sample ID: 5090446-07
Prism Work Order: 5090446
Time Collected: 09/22/15 15:30
Time Submitted: 09/24/15 16:10
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5J001112.0 9/30/15 22:40 CGPug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.111,2-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5J001112.0 9/30/15 22:40 CGPCCVug/L 0.112,2-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.0662-Chlorotoluene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.0504-Chlorotoluene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5J00111109/30/15 22:40 CGPug/L 0.31Acetone
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.048Benzene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.057Bromobenzene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.14Bromochloromethane
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.062Bromodichloromethane
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.040Bromoform
BRL SM6200 B P5J001111.0 9/30/15 22:40 CGPug/L 0.18Bromomethane
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.062Chlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.22Chloroethane
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.076Chloroform
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.079Chloromethane
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.081Dibromochloromethane
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.065Dibromomethane
BRL SM6200 B P5J001111.0 9/30/15 22:40 CGPug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5J001112009/30/15 22:40 CGPug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW12
Prism Sample ID: 5090446-07
Prism Work Order: 5090446
Time Collected: 09/22/15 15:30
Time Submitted: 09/24/15 16:10
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.061Ethylbenzene
BRL SM6200 B P5J001112.0 9/30/15 22:40 CGPug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.050Isopropyl Ether
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5J001111.0 9/30/15 22:40 CGPug/L 0.12m,p-Xylenes
BRL SM6200 B P5J001111.0 9/30/15 22:40 CGPug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5J001115.0 9/30/15 22:40 CGPug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5J001111.0 9/30/15 22:40 CGPug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5J001112.0 9/30/15 22:40 CGPug/L 0.083Methylene Chloride
BRL SM6200 B P5J001111.0 9/30/15 22:40 CGPug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5J001111.0 9/30/15 22:40 CGPug/L 0.19Naphthalene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.076n-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.087n-Propylbenzene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.044o-Xylene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.076sec-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.047Styrene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.088tert-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.098Tetrachloroethylene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.044Toluene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.078Trichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5J001115.0 9/30/15 22:40 CGPAug/L 0.060Vinyl acetate
BRL SM6200 B P5J001110.50 9/30/15 22:40 CGPug/L 0.097Vinyl chloride
BRL SM6200 B P5J001111.5 9/30/15 22:40 CGPug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13093 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-130100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW13
Prism Sample ID: 5090446-08
Prism Work Order: 5090446
Time Collected: 09/22/15 13:00
Time Submitted: 09/24/15 16:10
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5J001112.0 9/30/15 23:14 CGPug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.111,2-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5J001112.0 9/30/15 23:14 CGPCCVug/L 0.112,2-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.0662-Chlorotoluene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.0504-Chlorotoluene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5J00111109/30/15 23:14 CGPug/L 0.31Acetone
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.048Benzene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.057Bromobenzene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.14Bromochloromethane
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.062Bromodichloromethane
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.040Bromoform
BRL SM6200 B P5J001111.0 9/30/15 23:14 CGPug/L 0.18Bromomethane
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.062Chlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.22Chloroethane
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.076Chloroform
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.079Chloromethane
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.081Dibromochloromethane
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.065Dibromomethane
BRL SM6200 B P5J001111.0 9/30/15 23:14 CGPug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5J001112009/30/15 23:14 CGPug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW13
Prism Sample ID: 5090446-08
Prism Work Order: 5090446
Time Collected: 09/22/15 13:00
Time Submitted: 09/24/15 16:10
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.061Ethylbenzene
BRL SM6200 B P5J001112.0 9/30/15 23:14 CGPug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.050Isopropyl Ether
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5J001111.0 9/30/15 23:14 CGPug/L 0.12m,p-Xylenes
BRL SM6200 B P5J001111.0 9/30/15 23:14 CGPug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5J001115.0 9/30/15 23:14 CGPug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5J001111.0 9/30/15 23:14 CGPug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5J001112.0 9/30/15 23:14 CGPug/L 0.083Methylene Chloride
BRL SM6200 B P5J001111.0 9/30/15 23:14 CGPug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5J001111.0 9/30/15 23:14 CGPug/L 0.19Naphthalene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.076n-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.087n-Propylbenzene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.044o-Xylene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.076sec-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.047Styrene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.088tert-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.098Tetrachloroethylene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.044Toluene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.078Trichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5J001115.0 9/30/15 23:14 CGPAug/L 0.060Vinyl acetate
BRL SM6200 B P5J001110.50 9/30/15 23:14 CGPug/L 0.097Vinyl chloride
BRL SM6200 B P5J001111.5 9/30/15 23:14 CGPug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13097 %4-Bromofluorobenzene
70-130101 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW1A
Prism Sample ID: 5090446-09
Prism Work Order: 5090446
Time Collected: 09/23/15 12:05
Time Submitted: 09/24/15 16:10
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.131,2,4-Trichlorobenzene
42 SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5J001112.0 9/30/15 23:48 CGPug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.0761,2-Dichlorobenzene
3.7 SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.111,2-Dichloropropane
18 SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5J001112.0 9/30/15 23:48 CGPCCVug/L 0.112,2-Dichloropropane
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.0662-Chlorotoluene
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.0504-Chlorotoluene
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5J00111109/30/15 23:48 CGPug/L 0.31Acetone
1.2 SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.048Benzene
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.057Bromobenzene
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.14Bromochloromethane
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.062Bromodichloromethane
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.040Bromoform
BRL SM6200 B P5J001111.0 9/30/15 23:48 CGPug/L 0.18Bromomethane
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.062Chlorobenzene
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.22Chloroethane
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.076Chloroform
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.079Chloromethane
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.081Dibromochloromethane
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.065Dibromomethane
BRL SM6200 B P5J001111.0 9/30/15 23:48 CGPug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5J001112009/30/15 23:48 CGPug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW1A
Prism Sample ID: 5090446-09
Prism Work Order: 5090446
Time Collected: 09/23/15 12:05
Time Submitted: 09/24/15 16:10
0.53 SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.061Ethylbenzene
BRL SM6200 B P5J001112.0 9/30/15 23:48 CGPug/L 0.16Hexachlorobutadiene
32 SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.050Isopropyl Ether
0.52 SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.054Isopropylbenzene (Cumene)
13 SM6200 B P5J001111.0 9/30/15 23:48 CGPug/L 0.12m,p-Xylenes
BRL SM6200 B P5J001111.0 9/30/15 23:48 CGPug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5J001115.0 9/30/15 23:48 CGPug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5J001111.0 9/30/15 23:48 CGPug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5J001112.0 9/30/15 23:48 CGPug/L 0.083Methylene Chloride
6.2 SM6200 B P5J001111.0 9/30/15 23:48 CGPug/L 0.042Methyl-tert-Butyl Ether
3.2 SM6200 B P5J001111.0 9/30/15 23:48 CGPug/L 0.19Naphthalene
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.076n-Butylbenzene
0.80 SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.087n-Propylbenzene
9.3 SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.044o-Xylene
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.076sec-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.047Styrene
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.088tert-Butylbenzene
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.098Tetrachloroethylene
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.044Toluene
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.078Trichloroethylene
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5J001115.0 9/30/15 23:48 CGPAug/L 0.060Vinyl acetate
BRL SM6200 B P5J001110.50 9/30/15 23:48 CGPug/L 0.097Vinyl chloride
22 SM6200 B P5J001111.5 9/30/15 23:48 CGPug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13094 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW5
Prism Sample ID: 5090446-10
Prism Work Order: 5090446
Time Collected: 09/23/15 10:30
Time Submitted: 09/24/15 16:10
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5J001112.0 10/1/15 0:23 CGPug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.111,2-Dichloropropane
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5J001112.0 10/1/15 0:23 CGPCCVug/L 0.112,2-Dichloropropane
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.0662-Chlorotoluene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.0504-Chlorotoluene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5J001111010/1/15 0:23 CGPug/L 0.31Acetone
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.048Benzene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.057Bromobenzene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.14Bromochloromethane
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.062Bromodichloromethane
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.040Bromoform
BRL SM6200 B P5J001111.0 10/1/15 0:23 CGPug/L 0.18Bromomethane
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.062Chlorobenzene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.22Chloroethane
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.076Chloroform
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.079Chloromethane
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.081Dibromochloromethane
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.065Dibromomethane
BRL SM6200 B P5J001111.0 10/1/15 0:23 CGPug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5J0011120010/1/15 0:23 CGPug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW5
Prism Sample ID: 5090446-10
Prism Work Order: 5090446
Time Collected: 09/23/15 10:30
Time Submitted: 09/24/15 16:10
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.061Ethylbenzene
BRL SM6200 B P5J001112.0 10/1/15 0:23 CGPug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.050Isopropyl Ether
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5J001111.0 10/1/15 0:23 CGPug/L 0.12m,p-Xylenes
BRL SM6200 B P5J001111.0 10/1/15 0:23 CGPug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5J001115.0 10/1/15 0:23 CGPug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5J001111.0 10/1/15 0:23 CGPug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5J001112.0 10/1/15 0:23 CGPug/L 0.083Methylene Chloride
BRL SM6200 B P5J001111.0 10/1/15 0:23 CGPug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5J001111.0 10/1/15 0:23 CGPug/L 0.19Naphthalene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.076n-Butylbenzene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.087n-Propylbenzene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.044o-Xylene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.076sec-Butylbenzene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.047Styrene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.088tert-Butylbenzene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.098Tetrachloroethylene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.044Toluene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.078Trichloroethylene
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5J001115.0 10/1/15 0:23 CGPAug/L 0.060Vinyl acetate
BRL SM6200 B P5J001110.50 10/1/15 0:23 CGPug/L 0.097Vinyl chloride
BRL SM6200 B P5J001111.5 10/1/15 0:23 CGPug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13095 %4-Bromofluorobenzene
70-130101 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW6
Prism Sample ID: 5090446-11
Prism Work Order: 5090446
Time Collected: 09/23/15 10:00
Time Submitted: 09/24/15 16:10
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5J001112.0 10/1/15 0:57 CGPug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.111,2-Dichloropropane
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5J001112.0 10/1/15 0:57 CGPCCVug/L 0.112,2-Dichloropropane
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.0662-Chlorotoluene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.0504-Chlorotoluene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5J001111010/1/15 0:57 CGPug/L 0.31Acetone
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.048Benzene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.057Bromobenzene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.14Bromochloromethane
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.062Bromodichloromethane
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.040Bromoform
BRL SM6200 B P5J001111.0 10/1/15 0:57 CGPug/L 0.18Bromomethane
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.062Chlorobenzene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.22Chloroethane
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.076Chloroform
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.079Chloromethane
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.081Dibromochloromethane
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.065Dibromomethane
BRL SM6200 B P5J001111.0 10/1/15 0:57 CGPug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5J0011120010/1/15 0:57 CGPug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW6
Prism Sample ID: 5090446-11
Prism Work Order: 5090446
Time Collected: 09/23/15 10:00
Time Submitted: 09/24/15 16:10
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.061Ethylbenzene
BRL SM6200 B P5J001112.0 10/1/15 0:57 CGPug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.050Isopropyl Ether
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5J001111.0 10/1/15 0:57 CGPug/L 0.12m,p-Xylenes
BRL SM6200 B P5J001111.0 10/1/15 0:57 CGPug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5J001115.0 10/1/15 0:57 CGPug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5J001111.0 10/1/15 0:57 CGPug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5J001112.0 10/1/15 0:57 CGPug/L 0.083Methylene Chloride
1.0 SM6200 B P5J001111.0 10/1/15 0:57 CGPug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5J001111.0 10/1/15 0:57 CGPug/L 0.19Naphthalene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.076n-Butylbenzene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.087n-Propylbenzene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.044o-Xylene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.076sec-Butylbenzene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.047Styrene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.088tert-Butylbenzene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.098Tetrachloroethylene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.044Toluene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.078Trichloroethylene
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5J001115.0 10/1/15 0:57 CGPAug/L 0.060Vinyl acetate
BRL SM6200 B P5J001110.50 10/1/15 0:57 CGPug/L 0.097Vinyl chloride
BRL SM6200 B P5J001111.5 10/1/15 0:57 CGPug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13094 %4-Bromofluorobenzene
70-13099 %Dibromofluoromethane
70-130100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW15A
Prism Sample ID: 5090446-12
Prism Work Order: 5090446
Time Collected: 09/23/15 11:00
Time Submitted: 09/24/15 16:10
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.131,2,4-Trichlorobenzene
50 SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5J001112.0 10/1/15 1:31 CGPug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.111,2-Dichloropropane
19 SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5J001112.0 10/1/15 1:31 CGPCCVug/L 0.112,2-Dichloropropane
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.0662-Chlorotoluene
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.0504-Chlorotoluene
0.80 SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5J001111010/1/15 1:31 CGPug/L 0.31Acetone
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.048Benzene
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.057Bromobenzene
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.14Bromochloromethane
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.062Bromodichloromethane
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.040Bromoform
BRL SM6200 B P5J001111.0 10/1/15 1:31 CGPug/L 0.18Bromomethane
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.062Chlorobenzene
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.22Chloroethane
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.076Chloroform
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.079Chloromethane
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.081Dibromochloromethane
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.065Dibromomethane
BRL SM6200 B P5J001111.0 10/1/15 1:31 CGPug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5J0011120010/1/15 1:31 CGPug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW15A
Prism Sample ID: 5090446-12
Prism Work Order: 5090446
Time Collected: 09/23/15 11:00
Time Submitted: 09/24/15 16:10
16 SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.061Ethylbenzene
BRL SM6200 B P5J001112.0 10/1/15 1:31 CGPug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.050Isopropyl Ether
2.7 SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.054Isopropylbenzene (Cumene)
130 SM6200 B P5J001111.0 10/1/15 1:31 CGPug/L 0.12m,p-Xylenes
BRL SM6200 B P5J001111.0 10/1/15 1:31 CGPug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5J001115.0 10/1/15 1:31 CGPug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5J001111.0 10/1/15 1:31 CGPug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5J001112.0 10/1/15 1:31 CGPug/L 0.083Methylene Chloride
BRL SM6200 B P5J001111.0 10/1/15 1:31 CGPug/L 0.042Methyl-tert-Butyl Ether
16 SM6200 B P5J001111.0 10/1/15 1:31 CGPug/L 0.19Naphthalene
1.0 SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.076n-Butylbenzene
2.4 SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.087n-Propylbenzene
120 SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.044o-Xylene
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.076sec-Butylbenzene
0.52 SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.047Styrene
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.088tert-Butylbenzene
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.098Tetrachloroethylene
19 SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.044Toluene
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.078Trichloroethylene
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5J001115.0 10/1/15 1:31 CGPAug/L 0.060Vinyl acetate
BRL SM6200 B P5J001110.50 10/1/15 1:31 CGPug/L 0.097Vinyl chloride
250 SM6200 B P5J001111.5 10/1/15 1:31 CGPug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13095 %4-Bromofluorobenzene
70-13098 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2760
Prism Sample ID: 5090446-13
Prism Work Order: 5090446
Time Collected: 09/23/15 12:50
Time Submitted: 09/24/15 16:10
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5J012612.0 10/2/15 14:05 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5J012612.0 10/2/15 14:05 KDMCCVug/L 0.112,2-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5J012611010/2/15 14:05 KDMug/L 0.31Acetone
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.048Benzene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.040Bromoform
BRL SM6200 B P5J012611.0 10/2/15 14:05 KDMug/L 0.18Bromomethane
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.22Chloroethane
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.076Chloroform
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.079Chloromethane
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5J012611.0 10/2/15 14:05 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5J0126120010/2/15 14:05 KDMCVLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2760
Prism Sample ID: 5090446-13
Prism Work Order: 5090446
Time Collected: 09/23/15 12:50
Time Submitted: 09/24/15 16:10
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5J012612.0 10/2/15 14:05 KDMCCVug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5J012611.0 10/2/15 14:05 KDMCCVug/L 0.12m,p-Xylenes
BRL SM6200 B P5J012611.0 10/2/15 14:05 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5J012615.0 10/2/15 14:05 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5J012611.0 10/2/15 14:05 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5J012612.0 10/2/15 14:05 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5J012611.0 10/2/15 14:05 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5J012611.0 10/2/15 14:05 KDMug/L 0.19Naphthalene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.044o-Xylene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.047Styrene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.044Toluene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5J012615.0 10/2/15 14:05 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5J012610.50 10/2/15 14:05 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5J012611.5 10/2/15 14:05 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13095 %4-Bromofluorobenzene
70-130108 %Dibromofluoromethane
70-130102 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2768B
Prism Sample ID: 5090446-14
Prism Work Order: 5090446
Time Collected: 09/23/15 13:40
Time Submitted: 09/24/15 16:10
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5J012612.0 10/2/15 14:39 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5J012612.0 10/2/15 14:39 KDMCCVug/L 0.112,2-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5J012611010/2/15 14:39 KDMug/L 0.31Acetone
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.048Benzene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.040Bromoform
BRL SM6200 B P5J012611.0 10/2/15 14:39 KDMug/L 0.18Bromomethane
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.22Chloroethane
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.076Chloroform
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.079Chloromethane
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5J012611.0 10/2/15 14:39 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5J0126120010/2/15 14:39 KDMCVLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2768B
Prism Sample ID: 5090446-14
Prism Work Order: 5090446
Time Collected: 09/23/15 13:40
Time Submitted: 09/24/15 16:10
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5J012612.0 10/2/15 14:39 KDMCCVug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5J012611.0 10/2/15 14:39 KDMCCVug/L 0.12m,p-Xylenes
BRL SM6200 B P5J012611.0 10/2/15 14:39 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5J012615.0 10/2/15 14:39 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5J012611.0 10/2/15 14:39 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5J012612.0 10/2/15 14:39 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5J012611.0 10/2/15 14:39 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5J012611.0 10/2/15 14:39 KDMug/L 0.19Naphthalene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.044o-Xylene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.047Styrene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.044Toluene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5J012615.0 10/2/15 14:39 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5J012610.50 10/2/15 14:39 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5J012611.5 10/2/15 14:39 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13095 %4-Bromofluorobenzene
70-130106 %Dibromofluoromethane
70-130102 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2779
Prism Sample ID: 5090446-15
Prism Work Order: 5090446
Time Collected: 09/23/15 14:15
Time Submitted: 09/24/15 16:10
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5J012612.0 10/2/15 15:13 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5J012612.0 10/2/15 15:13 KDMCCVug/L 0.112,2-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5J012611010/2/15 15:13 KDMug/L 0.31Acetone
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.048Benzene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.040Bromoform
BRL SM6200 B P5J012611.0 10/2/15 15:13 KDMug/L 0.18Bromomethane
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.22Chloroethane
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.076Chloroform
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.079Chloromethane
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5J012611.0 10/2/15 15:13 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5J0126120010/2/15 15:13 KDMCVLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2779
Prism Sample ID: 5090446-15
Prism Work Order: 5090446
Time Collected: 09/23/15 14:15
Time Submitted: 09/24/15 16:10
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5J012612.0 10/2/15 15:13 KDMCCVug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5J012611.0 10/2/15 15:13 KDMCCVug/L 0.12m,p-Xylenes
BRL SM6200 B P5J012611.0 10/2/15 15:13 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5J012615.0 10/2/15 15:13 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5J012611.0 10/2/15 15:13 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5J012612.0 10/2/15 15:13 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5J012611.0 10/2/15 15:13 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5J012611.0 10/2/15 15:13 KDMug/L 0.19Naphthalene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.044o-Xylene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.047Styrene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.044Toluene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5J012615.0 10/2/15 15:13 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5J012610.50 10/2/15 15:13 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5J012611.5 10/2/15 15:13 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13096 %4-Bromofluorobenzene
70-130107 %Dibromofluoromethane
70-130103 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2773
Prism Sample ID: 5090446-16
Prism Work Order: 5090446
Time Collected: 09/23/15 14:45
Time Submitted: 09/24/15 16:10
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5J012612.0 10/2/15 15:47 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5J012612.0 10/2/15 15:47 KDMCCVug/L 0.112,2-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5J012611010/2/15 15:47 KDMug/L 0.31Acetone
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.048Benzene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.040Bromoform
BRL SM6200 B P5J012611.0 10/2/15 15:47 KDMug/L 0.18Bromomethane
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.22Chloroethane
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.076Chloroform
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.079Chloromethane
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5J012611.0 10/2/15 15:47 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5J0126120010/2/15 15:47 KDMCVLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2773
Prism Sample ID: 5090446-16
Prism Work Order: 5090446
Time Collected: 09/23/15 14:45
Time Submitted: 09/24/15 16:10
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5J012612.0 10/2/15 15:47 KDMCCVug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5J012611.0 10/2/15 15:47 KDMCCVug/L 0.12m,p-Xylenes
BRL SM6200 B P5J012611.0 10/2/15 15:47 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5J012615.0 10/2/15 15:47 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5J012611.0 10/2/15 15:47 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5J012612.0 10/2/15 15:47 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5J012611.0 10/2/15 15:47 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5J012611.0 10/2/15 15:47 KDMug/L 0.19Naphthalene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.044o-Xylene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.047Styrene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.044Toluene
2.4 SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5J012615.0 10/2/15 15:47 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5J012610.50 10/2/15 15:47 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5J012611.5 10/2/15 15:47 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13095 %4-Bromofluorobenzene
70-130104 %Dibromofluoromethane
70-130102 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765I
Prism Sample ID: 5090446-17
Prism Work Order: 5090446
Time Collected: 09/23/15 15:15
Time Submitted: 09/24/15 16:10
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5J012612.0 10/2/15 16:22 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0761,2-Dichlorobenzene
13 SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5J012612.0 10/2/15 16:22 KDMCCVug/L 0.112,2-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5J012611010/2/15 16:22 KDMug/L 0.31Acetone
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.048Benzene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.040Bromoform
BRL SM6200 B P5J012611.0 10/2/15 16:22 KDMug/L 0.18Bromomethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.22Chloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.076Chloroform
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.079Chloromethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5J012611.0 10/2/15 16:22 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5J0126120010/2/15 16:22 KDMCVLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765I
Prism Sample ID: 5090446-17
Prism Work Order: 5090446
Time Collected: 09/23/15 15:15
Time Submitted: 09/24/15 16:10
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5J012612.0 10/2/15 16:22 KDMCCVug/L 0.16Hexachlorobutadiene
74 SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.050Isopropyl Ether
0.56 SM6200 B P5J012610.50 10/2/15 16:22 KDMHug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5J012611.0 10/2/15 16:22 KDMCCVug/L 0.12m,p-Xylenes
BRL SM6200 B P5J012611.0 10/2/15 16:22 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5J012615.0 10/2/15 16:22 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5J012611.0 10/2/15 16:22 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5J012612.0 10/2/15 16:22 KDMug/L 0.083Methylene Chloride
70 SM6200 B P5J012611.0 10/2/15 16:22 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5J012611.0 10/2/15 16:22 KDMug/L 0.19Naphthalene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.044o-Xylene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.047Styrene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.044Toluene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5J012615.0 10/2/15 16:22 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5J012611.5 10/2/15 16:22 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13095 %4-Bromofluorobenzene
70-130102 %Dibromofluoromethane
70-130100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765M
Prism Sample ID: 5090446-18
Prism Work Order: 5090446
Time Collected: 09/23/15 15:25
Time Submitted: 09/24/15 16:10
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5J012612.0 10/2/15 16:56 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5J012612.0 10/2/15 16:56 KDMCCVug/L 0.112,2-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5J012611010/2/15 16:56 KDMug/L 0.31Acetone
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.048Benzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.040Bromoform
BRL SM6200 B P5J012611.0 10/2/15 16:56 KDMug/L 0.18Bromomethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.22Chloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.076Chloroform
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.079Chloromethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5J012611.0 10/2/15 16:56 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5J0126120010/2/15 16:56 KDMCVLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765M
Prism Sample ID: 5090446-18
Prism Work Order: 5090446
Time Collected: 09/23/15 15:25
Time Submitted: 09/24/15 16:10
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5J012612.0 10/2/15 16:56 KDMCCVug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5J012611.0 10/2/15 16:56 KDMCCVug/L 0.12m,p-Xylenes
BRL SM6200 B P5J012611.0 10/2/15 16:56 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5J012615.0 10/2/15 16:56 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5J012611.0 10/2/15 16:56 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5J012612.0 10/2/15 16:56 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5J012611.0 10/2/15 16:56 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5J012611.0 10/2/15 16:56 KDMug/L 0.19Naphthalene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.044o-Xylene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.047Styrene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.044Toluene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5J012615.0 10/2/15 16:56 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5J012611.5 10/2/15 16:56 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13094 %4-Bromofluorobenzene
70-130110 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765E
Prism Sample ID: 5090446-19
Prism Work Order: 5090446
Time Collected: 09/23/15 15:45
Time Submitted: 09/24/15 16:10
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5J012612.0 10/2/15 17:30 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5J012612.0 10/2/15 17:30 KDMCCVug/L 0.112,2-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5J012611010/2/15 17:30 KDMug/L 0.31Acetone
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.048Benzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.040Bromoform
BRL SM6200 B P5J012611.0 10/2/15 17:30 KDMug/L 0.18Bromomethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.22Chloroethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.076Chloroform
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.079Chloromethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5J012611.0 10/2/15 17:30 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5J0126120010/2/15 17:30 KDMCVLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 41 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765E
Prism Sample ID: 5090446-19
Prism Work Order: 5090446
Time Collected: 09/23/15 15:45
Time Submitted: 09/24/15 16:10
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5J012612.0 10/2/15 17:30 KDMCCVug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5J012611.0 10/2/15 17:30 KDMCCVug/L 0.12m,p-Xylenes
BRL SM6200 B P5J012611.0 10/2/15 17:30 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5J012615.0 10/2/15 17:30 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5J012611.0 10/2/15 17:30 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5J012612.0 10/2/15 17:30 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5J012611.0 10/2/15 17:30 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5J012611.0 10/2/15 17:30 KDMug/L 0.19Naphthalene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.044o-Xylene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.047Styrene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.044Toluene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5J012615.0 10/2/15 17:30 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5J012611.5 10/2/15 17:30 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13097 %4-Bromofluorobenzene
70-130106 %Dibromofluoromethane
70-130103 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 42 of 55
10/9/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5090446
Time Submitted: 9/24/2015 4:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5J0011 - SM6200 B
Blank (P5J0011-BLK1)Prepared & Analyzed: 09/30/15
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL0.50
1,2,4-Trichlorobenzene ug/LBRL0.50
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL10
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL0.50
Bromomethane ug/LBRL1.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethanol ug/LBRL200
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 43 of 55
10/9/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5090446
Time Submitted: 9/24/2015 4:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5J0011 - SM6200 B
Blank (P5J0011-BLK1)Prepared & Analyzed: 09/30/15
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL1.0
Methylene Chloride ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL1.0
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL0.50
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Butylbenzene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL5.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9547.6
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10049.8
ug/L 50.00 70-130Surrogate: Toluene-d8 10049.8
LCS (P5J0011-BS1)Prepared & Analyzed: 09/30/15
1,1,1,2-Tetrachloroethane ug/L22.7 0.50 20.00 70-130114
1,1,1-Trichloroethane ug/L25.8 0.50 20.00 70-130129
1,1,2,2-Tetrachloroethane ug/L18.2 0.50 20.00 70-13091
1,1,2-Trichloroethane ug/L21.2 0.50 20.00 70-130106
1,1-Dichloroethane ug/L24.6 0.50 20.00 70-130123
1,1-Dichloroethylene ug/L25.0 0.50 20.00 70-130125
1,1-Dichloropropylene ug/L23.9 0.50 20.00 70-130120
1,2,3-Trichlorobenzene ug/L24.4 0.50 20.00 70-130122
1,2,3-Trichloropropane ug/L20.2 0.50 20.00 70-130101
1,2,4-Trichlorobenzene ug/L24.8 0.50 20.00 70-130124
1,2,4-Trimethylbenzene ug/L26.0 0.50 20.00 70-130130
1,2-Dibromo-3-chloropropane ug/L21.7 2.0 20.00 70-130109
1,2-Dibromoethane ug/L22.4 0.50 20.00 70-130112
1,2-Dichlorobenzene ug/L24.4 0.50 20.00 70-130122
1,2-Dichloroethane ug/L22.5 0.50 20.00 70-130113
1,2-Dichloropropane ug/L20.4 0.50 20.00 70-130102
1,3,5-Trimethylbenzene ug/L26.3 0.50 20.00 LH70-130132
1,3-Dichlorobenzene ug/L24.6 0.50 20.00 70-130123
1,3-Dichloropropane ug/L22.4 0.50 20.00 70-130112
1,4-Dichlorobenzene ug/L24.0 0.50 20.00 70-130120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 44 of 55
10/9/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5090446
Time Submitted: 9/24/2015 4:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5J0011 - SM6200 B
LCS (P5J0011-BS1)Prepared & Analyzed: 09/30/15
2,2-Dichloropropane ug/L32.7 2.0 20.00 LH70-130163
2-Chlorotoluene ug/L24.1 0.50 20.00 70-130120
4-Chlorotoluene ug/L24.6 0.50 20.00 70-130123
4-Isopropyltoluene ug/L23.1 0.50 20.00 70-130116
Acetone ug/L37.6 10 40.00 40-16094
Benzene ug/L23.9 0.50 20.00 70-130120
Bromobenzene ug/L21.6 0.50 20.00 70-130108
Bromochloromethane ug/L19.8 0.50 20.00 70-13099
Bromodichloromethane ug/L22.0 0.50 20.00 70-130110
Bromoform ug/L21.1 0.50 20.00 70-130105
Bromomethane ug/L19.6 1.0 20.00 60-14098
Carbon Tetrachloride ug/L25.2 0.50 20.00 70-130126
Chlorobenzene ug/L24.8 0.50 20.00 70-130124
Chloroethane ug/L21.4 0.50 20.00 60-140107
Chloroform ug/L22.1 0.50 20.00 70-130110
Chloromethane ug/L24.1 0.50 20.00 60-140120
cis-1,2-Dichloroethylene ug/L23.0 0.50 20.00 70-130115
cis-1,3-Dichloropropylene ug/L24.0 0.50 20.00 70-130120
Dibromochloromethane ug/L20.5 0.50 20.00 70-130103
Dibromomethane ug/L22.3 0.50 20.00 70-130112
Dichlorodifluoromethane ug/L29.5 1.0 20.00 LH60-140148
Ethanol ug/L420200 500.0 60-14084
Ethylbenzene ug/L26.2 0.50 20.00 L270-130131
Hexachlorobutadiene ug/L28.3 2.0 20.00 LH70-130142
Isopropyl Ether ug/L19.8 0.50 20.00 70-13099
Isopropylbenzene (Cumene)ug/L28.1 0.50 20.00 Aa70-130140
m,p-Xylenes ug/L54.3 1.0 40.00 Aa70-130136
Methyl Butyl Ketone (2-Hexanone)ug/L20.3 1.0 20.00 60-140102
Methyl Ethyl Ketone (2-Butanone)ug/L16.0 5.0 20.00 60-14080
Methyl Isobutyl Ketone ug/L18.4 1.0 20.00 60-14092
Methylene Chloride ug/L19.3 2.0 20.00 70-13096
Methyl-tert-Butyl Ether ug/L23.7 1.0 20.00 70-130118
Naphthalene ug/L21.6 1.0 20.00 70-130108
n-Butylbenzene ug/L24.8 0.50 20.00 70-130124
n-Propylbenzene ug/L24.5 0.50 20.00 70-130122
o-Xylene ug/L25.5 0.50 20.00 70-130128
sec-Butylbenzene ug/L25.6 0.50 20.00 70-130128
Styrene ug/L25.8 0.50 20.00 70-130129
tert-Butylbenzene ug/L22.8 0.50 20.00 70-130114
Tetrachloroethylene ug/L25.9 0.50 20.00 70-130129
Toluene ug/L25.1 0.50 20.00 70-130126
trans-1,2-Dichloroethylene ug/L23.0 0.50 20.00 70-130115
trans-1,3-Dichloropropylene ug/L21.7 0.50 20.00 70-130108
Trichloroethylene ug/L26.7 0.50 20.00 LH70-130133
Trichlorofluoromethane ug/L25.5 0.50 20.00 60-140128
Vinyl acetate ug/L6.21 5.0 20.00 L60-14031
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 45 of 55
10/9/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5090446
Time Submitted: 9/24/2015 4:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5J0011 - SM6200 B
LCS (P5J0011-BS1)Prepared & Analyzed: 09/30/15
Vinyl chloride ug/L22.2 0.50 20.00 60-140111
Xylenes, total ug/L79.8 1.5 60.00 Aa70-130133
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9647.8
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9447.0
ug/L 50.00 70-130Surrogate: Toluene-d8 10150.5
LCS Dup (P5J0011-BSD1)Prepared & Analyzed: 09/30/15
1,1,1,2-Tetrachloroethane ug/L23.2 0.50 20.00 2070-130116 2
1,1,1-Trichloroethane ug/L26.1 0.50 20.00 2070-130130 1
1,1,2,2-Tetrachloroethane ug/L18.7 0.50 20.00 2070-13094 3
1,1,2-Trichloroethane ug/L20.5 0.50 20.00 2070-130103 3
1,1-Dichloroethane ug/L24.1 0.50 20.00 2070-130120 2
1,1-Dichloroethylene ug/L25.0 0.50 20.00 2070-130125 0.2
1,1-Dichloropropylene ug/L24.0 0.50 20.00 2070-130120 0.5
1,2,3-Trichlorobenzene ug/L24.7 0.50 20.00 2070-130123 1
1,2,3-Trichloropropane ug/L20.9 0.50 20.00 2070-130104 4
1,2,4-Trichlorobenzene ug/L25.2 0.50 20.00 2070-130126 2
1,2,4-Trimethylbenzene ug/L26.3 0.50 20.00 20 L270-130131 1
1,2-Dibromo-3-chloropropane ug/L22.6 2.0 20.00 2070-130113 4
1,2-Dibromoethane ug/L21.7 0.50 20.00 2070-130108 3
1,2-Dichlorobenzene ug/L24.5 0.50 20.00 2070-130122 0.6
1,2-Dichloroethane ug/L22.4 0.50 20.00 2070-130112 0.6
1,2-Dichloropropane ug/L20.5 0.50 20.00 2070-130102 0.2
1,3,5-Trimethylbenzene ug/L26.8 0.50 20.00 20 LH70-130134 2
1,3-Dichlorobenzene ug/L25.2 0.50 20.00 2070-130126 2
1,3-Dichloropropane ug/L22.9 0.50 20.00 2070-130114 2
1,4-Dichlorobenzene ug/L24.4 0.50 20.00 2070-130122 2
2,2-Dichloropropane ug/L32.8 2.0 20.00 20 LH70-130164 0.3
2-Chlorotoluene ug/L24.5 0.50 20.00 2070-130123 2
4-Chlorotoluene ug/L24.6 0.50 20.00 2070-130123 0.1
4-Isopropyltoluene ug/L23.9 0.50 20.00 2070-130120 3
Acetone ug/L39.1 10 40.00 2040-16098 4
Benzene ug/L23.5 0.50 20.00 2070-130117 2
Bromobenzene ug/L21.8 0.50 20.00 2070-130109 1
Bromochloromethane ug/L20.1 0.50 20.00 2070-130100 1
Bromodichloromethane ug/L21.1 0.50 20.00 2070-130106 4
Bromoform ug/L20.8 0.50 20.00 2070-130104 1
Bromomethane ug/L20.1 1.0 20.00 2060-140101 3
Carbon Tetrachloride ug/L26.2 0.50 20.00 20 L270-130131 4
Chlorobenzene ug/L24.7 0.50 20.00 2070-130123 0.5
Chloroethane ug/L21.4 0.50 20.00 2060-140107 0.2
Chloroform ug/L21.6 0.50 20.00 2070-130108 2
Chloromethane ug/L23.2 0.50 20.00 2060-140116 4
cis-1,2-Dichloroethylene ug/L23.0 0.50 20.00 2070-130115 0.09
cis-1,3-Dichloropropylene ug/L23.8 0.50 20.00 2070-130119 0.6
Dibromochloromethane ug/L20.3 0.50 20.00 2070-130101 1
Dibromomethane ug/L21.9 0.50 20.00 2070-130110 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 46 of 55
10/9/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5090446
Time Submitted: 9/24/2015 4:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5J0011 - SM6200 B
LCS Dup (P5J0011-BSD1)Prepared & Analyzed: 09/30/15
Dichlorodifluoromethane ug/L29.0 1.0 20.00 20 LH60-140145 2
Ethanol ug/L434200 500.0 2060-14087 3
Ethylbenzene ug/L25.6 0.50 20.00 2070-130128 2
Hexachlorobutadiene ug/L28.8 2.0 20.00 20 LH70-130144 2
Isopropyl Ether ug/L19.5 0.50 20.00 2070-13097 1
Isopropylbenzene (Cumene)ug/L28.6 0.50 20.00 20 Aa70-130143 2
m,p-Xylenes ug/L53.0 1.0 40.00 20 Aa70-130133 2
Methyl Butyl Ketone (2-Hexanone)ug/L18.4 1.0 20.00 2060-14092 10
Methyl Ethyl Ketone (2-Butanone)ug/L16.5 5.0 20.00 2060-14083 4
Methyl Isobutyl Ketone ug/L18.4 1.0 20.00 2060-14092 0.3
Methylene Chloride ug/L19.9 2.0 20.00 2070-13099 3
Methyl-tert-Butyl Ether ug/L23.8 1.0 20.00 2070-130119 0.4
Naphthalene ug/L21.9 1.0 20.00 2070-130110 2
n-Butylbenzene ug/L24.7 0.50 20.00 2070-130124 0.3
n-Propylbenzene ug/L25.1 0.50 20.00 2070-130126 3
o-Xylene ug/L25.4 0.50 20.00 2070-130127 0.4
sec-Butylbenzene ug/L26.6 0.50 20.00 20 L270-130133 4
Styrene ug/L25.0 0.50 20.00 2070-130125 3
tert-Butylbenzene ug/L23.2 0.50 20.00 2070-130116 2
Tetrachloroethylene ug/L26.6 0.50 20.00 20 L270-130133 3
Toluene ug/L24.6 0.50 20.00 2070-130123 2
trans-1,2-Dichloroethylene ug/L23.2 0.50 20.00 2070-130116 0.9
trans-1,3-Dichloropropylene ug/L21.6 0.50 20.00 2070-130108 0.4
Trichloroethylene ug/L26.9 0.50 20.00 20 LH70-130135 1
Trichlorofluoromethane ug/L25.8 0.50 20.00 2060-140129 1
Vinyl acetate ug/L6.14 5.0 20.00 20 L60-14031 1
Vinyl chloride ug/L22.4 0.50 20.00 2060-140112 0.7
Xylenes, total ug/L78.4 1.5 60.00 20 Aa70-130131 2
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9647.8
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9748.6
ug/L 50.00 70-130Surrogate: Toluene-d8 9949.6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 47 of 55
10/9/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5090446
Time Submitted: 9/24/2015 4:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5J0126 - SM6200 B
Blank (P5J0126-BLK1)Prepared & Analyzed: 10/02/15
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL0.50
1,2,4-Trichlorobenzene ug/LBRL0.50
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL10
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL0.50
Bromomethane ug/LBRL1.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethanol ug/LBRL200
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 48 of 55
10/9/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5090446
Time Submitted: 9/24/2015 4:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5J0126 - SM6200 B
Blank (P5J0126-BLK1)Prepared & Analyzed: 10/02/15
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL1.0
Methylene Chloride ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL1.0
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL0.50
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Butylbenzene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL5.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9848.9
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10451.8
ug/L 50.00 70-130Surrogate: Toluene-d8 10351.4
LCS (P5J0126-BS1)Prepared & Analyzed: 10/02/15
1,1,1,2-Tetrachloroethane ug/L24.6 0.50 20.00 70-130123
1,1,1-Trichloroethane ug/L27.1 0.50 20.00 L170-130136
1,1,2,2-Tetrachloroethane ug/L22.8 0.50 20.00 70-130114
1,1,2-Trichloroethane ug/L22.3 0.50 20.00 70-130112
1,1-Dichloroethane ug/L24.9 0.50 20.00 70-130125
1,1-Dichloroethylene ug/L25.1 0.50 20.00 70-130126
1,1-Dichloropropylene ug/L25.0 0.50 20.00 70-130125
1,2,3-Trichlorobenzene ug/L25.7 0.50 20.00 70-130129
1,2,3-Trichloropropane ug/L20.9 0.50 20.00 70-130104
1,2,4-Trichlorobenzene ug/L25.7 0.50 20.00 70-130128
1,2,4-Trimethylbenzene ug/L27.4 0.50 20.00 L170-130137
1,2-Dibromo-3-chloropropane ug/L21.1 2.0 20.00 70-130105
1,2-Dibromoethane ug/L23.4 0.50 20.00 70-130117
1,2-Dichlorobenzene ug/L25.3 0.50 20.00 70-130126
1,2-Dichloroethane ug/L23.2 0.50 20.00 70-130116
1,2-Dichloropropane ug/L21.0 0.50 20.00 70-130105
1,3,5-Trimethylbenzene ug/L27.8 0.50 20.00 L170-130139
1,3-Dichlorobenzene ug/L26.4 0.50 20.00 L170-130132
1,3-Dichloropropane ug/L23.7 0.50 20.00 70-130119
1,4-Dichlorobenzene ug/L25.7 0.50 20.00 70-130128
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 49 of 55
10/9/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5090446
Time Submitted: 9/24/2015 4:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5J0126 - SM6200 B
LCS (P5J0126-BS1)Prepared & Analyzed: 10/02/15
2,2-Dichloropropane ug/L30.4 2.0 20.00 L170-130152
2-Chlorotoluene ug/L25.4 0.50 20.00 70-130127
4-Chlorotoluene ug/L25.6 0.50 20.00 70-130128
4-Isopropyltoluene ug/L24.3 0.50 20.00 70-130121
Acetone ug/L40.9 10 40.00 40-160102
Benzene ug/L24.4 0.50 20.00 70-130122
Bromobenzene ug/L23.1 0.50 20.00 70-130116
Bromochloromethane ug/L20.3 0.50 20.00 70-130101
Bromodichloromethane ug/L22.8 0.50 20.00 70-130114
Bromoform ug/L24.2 0.50 20.00 70-130121
Bromomethane ug/L26.5 1.0 20.00 60-140132
Carbon Tetrachloride ug/L28.5 0.50 20.00 L170-130142
Chlorobenzene ug/L26.7 0.50 20.00 L170-130134
Chloroethane ug/L21.6 0.50 20.00 60-140108
Chloroform ug/L22.5 0.50 20.00 70-130113
Chloromethane ug/L19.3 0.50 20.00 60-14097
cis-1,2-Dichloroethylene ug/L24.4 0.50 20.00 70-130122
cis-1,3-Dichloropropylene ug/L24.8 0.50 20.00 70-130124
Dibromochloromethane ug/L22.8 0.50 20.00 70-130114
Dibromomethane ug/L22.1 0.50 20.00 70-130110
Dichlorodifluoromethane ug/L20.7 1.0 20.00 60-140103
Ethanol ug/L438200 500.0 60-14088
Ethylbenzene ug/L27.8 0.50 20.00 L170-130139
Hexachlorobutadiene ug/L28.8 2.0 20.00 LH70-130144
Isopropyl Ether ug/L19.6 0.50 20.00 70-13098
Isopropylbenzene (Cumene)ug/L29.8 0.50 20.00 Aa70-130149
m,p-Xylenes ug/L57.5 1.0 40.00 L170-130144
Methyl Butyl Ketone (2-Hexanone)ug/L18.7 1.0 20.00 60-14094
Methyl Ethyl Ketone (2-Butanone)ug/L17.2 5.0 20.00 60-14086
Methyl Isobutyl Ketone ug/L18.5 1.0 20.00 60-14093
Methylene Chloride ug/L20.5 2.0 20.00 70-130103
Methyl-tert-Butyl Ether ug/L23.6 1.0 20.00 70-130118
Naphthalene ug/L21.9 1.0 20.00 70-130109
n-Butylbenzene ug/L25.0 0.50 20.00 70-130125
n-Propylbenzene ug/L26.0 0.50 20.00 70-130130
o-Xylene ug/L27.7 0.50 20.00 L170-130139
sec-Butylbenzene ug/L27.7 0.50 20.00 L170-130139
Styrene ug/L27.0 0.50 20.00 L170-130135
tert-Butylbenzene ug/L23.9 0.50 20.00 70-130119
Tetrachloroethylene ug/L27.5 0.50 20.00 L170-130138
Toluene ug/L25.7 0.50 20.00 70-130129
trans-1,2-Dichloroethylene ug/L23.4 0.50 20.00 70-130117
trans-1,3-Dichloropropylene ug/L21.8 0.50 20.00 70-130109
Trichloroethylene ug/L25.2 0.50 20.00 70-130126
Trichlorofluoromethane ug/L27.5 0.50 20.00 60-140137
Vinyl acetate ug/L20.9 5.0 20.00 60-140105
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 50 of 55
10/9/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5090446
Time Submitted: 9/24/2015 4:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5J0126 - SM6200 B
LCS (P5J0126-BS1)Prepared & Analyzed: 10/02/15
Vinyl chloride ug/L22.0 0.50 20.00 60-140110
Xylenes, total ug/L85.3 1.5 60.00 L170-130142
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9446.8
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9949.6
ug/L 50.00 70-130Surrogate: Toluene-d8 10250.9
LCS Dup (P5J0126-BSD1)Prepared & Analyzed: 10/02/15
1,1,1,2-Tetrachloroethane ug/L22.6 0.50 20.00 2070-130113 9
1,1,1-Trichloroethane ug/L23.4 0.50 20.00 2070-130117 15
1,1,2,2-Tetrachloroethane ug/L20.5 0.50 20.00 2070-130103 11
1,1,2-Trichloroethane ug/L20.3 0.50 20.00 2070-130102 9
1,1-Dichloroethane ug/L21.9 0.50 20.00 2070-130110 13
1,1-Dichloroethylene ug/L22.5 0.50 20.00 2070-130112 11
1,1-Dichloropropylene ug/L21.9 0.50 20.00 2070-130110 13
1,2,3-Trichlorobenzene ug/L23.2 0.50 20.00 2070-130116 10
1,2,3-Trichloropropane ug/L19.8 0.50 20.00 2070-13099 5
1,2,4-Trichlorobenzene ug/L23.0 0.50 20.00 2070-130115 11
1,2,4-Trimethylbenzene ug/L24.3 0.50 20.00 2070-130121 12
1,2-Dibromo-3-chloropropane ug/L22.5 2.0 20.00 2070-130112 7
1,2-Dibromoethane ug/L21.8 0.50 20.00 2070-130109 7
1,2-Dichlorobenzene ug/L23.1 0.50 20.00 2070-130116 9
1,2-Dichloroethane ug/L21.2 0.50 20.00 2070-130106 9
1,2-Dichloropropane ug/L18.6 0.50 20.00 2070-13093 12
1,3,5-Trimethylbenzene ug/L25.1 0.50 20.00 2070-130126 10
1,3-Dichlorobenzene ug/L23.9 0.50 20.00 2070-130119 10
1,3-Dichloropropane ug/L21.7 0.50 20.00 2070-130109 9
1,4-Dichlorobenzene ug/L23.2 0.50 20.00 2070-130116 10
2,2-Dichloropropane ug/L25.6 2.0 20.00 2070-130128 17
2-Chlorotoluene ug/L22.7 0.50 20.00 2070-130114 11
4-Chlorotoluene ug/L23.2 0.50 20.00 2070-130116 10
4-Isopropyltoluene ug/L22.0 0.50 20.00 2070-130110 10
Acetone ug/L37.3 10 40.00 2040-16093 9
Benzene ug/L21.2 0.50 20.00 2070-130106 14
Bromobenzene ug/L20.3 0.50 20.00 2070-130102 13
Bromochloromethane ug/L18.2 0.50 20.00 2070-13091 11
Bromodichloromethane ug/L20.4 0.50 20.00 2070-130102 11
Bromoform ug/L21.9 0.50 20.00 2070-130110 10
Bromomethane ug/L22.3 1.0 20.00 2060-140111 17
Carbon Tetrachloride ug/L25.3 0.50 20.00 2070-130127 12
Chlorobenzene ug/L24.0 0.50 20.00 2070-130120 11
Chloroethane ug/L18.6 0.50 20.00 2060-14093 15
Chloroform ug/L19.8 0.50 20.00 2070-13099 13
Chloromethane ug/L17.0 0.50 20.00 2060-14085 13
cis-1,2-Dichloroethylene ug/L21.4 0.50 20.00 2070-130107 13
cis-1,3-Dichloropropylene ug/L21.9 0.50 20.00 2070-130110 12
Dibromochloromethane ug/L20.7 0.50 20.00 2070-130104 10
Dibromomethane ug/L20.4 0.50 20.00 2070-130102 8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 51 of 55
10/9/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5090446
Time Submitted: 9/24/2015 4:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5J0126 - SM6200 B
LCS Dup (P5J0126-BSD1)Prepared & Analyzed: 10/02/15
Dichlorodifluoromethane ug/L18.0 1.0 20.00 2060-14090 14
Ethanol ug/L364200 500.0 2060-14073 19
Ethylbenzene ug/L24.5 0.50 20.00 2070-130123 12
Hexachlorobutadiene ug/L26.2 2.0 20.00 20 LH70-130131 9
Isopropyl Ether ug/L18.0 0.50 20.00 2070-13090 9
Isopropylbenzene (Cumene)ug/L26.6 0.50 20.00 20 Aa70-130133 11
m,p-Xylenes ug/L51.7 1.0 40.00 2070-130129 11
Methyl Butyl Ketone (2-Hexanone)ug/L17.7 1.0 20.00 2060-14088 6
Methyl Ethyl Ketone (2-Butanone)ug/L13.9 5.0 20.00 20 LCD260-14070 21
Methyl Isobutyl Ketone ug/L17.5 1.0 20.00 2060-14087 6
Methylene Chloride ug/L18.3 2.0 20.00 2070-13092 11
Methyl-tert-Butyl Ether ug/L21.7 1.0 20.00 2070-130108 8
Naphthalene ug/L20.8 1.0 20.00 2070-130104 5
n-Butylbenzene ug/L23.0 0.50 20.00 2070-130115 9
n-Propylbenzene ug/L23.4 0.50 20.00 2070-130117 10
o-Xylene ug/L24.4 0.50 20.00 2070-130122 13
sec-Butylbenzene ug/L24.7 0.50 20.00 2070-130124 12
Styrene ug/L24.7 0.50 20.00 2070-130124 9
tert-Butylbenzene ug/L21.5 0.50 20.00 2070-130108 10
Tetrachloroethylene ug/L25.3 0.50 20.00 2070-130126 8
Toluene ug/L22.6 0.50 20.00 2070-130113 13
trans-1,2-Dichloroethylene ug/L20.8 0.50 20.00 2070-130104 12
trans-1,3-Dichloropropylene ug/L19.4 0.50 20.00 2070-13097 12
Trichloroethylene ug/L21.8 0.50 20.00 2070-130109 15
Trichlorofluoromethane ug/L24.1 0.50 20.00 2060-140120 13
Vinyl acetate ug/L19.8 5.0 20.00 2060-14099 6
Vinyl chloride ug/L19.6 0.50 20.00 2060-14098 11
Xylenes, total ug/L76.1 1.5 60.00 2070-130127 11
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9547.7
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10050.0
ug/L 50.00 70-130Surrogate: Toluene-d8 10451.8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 52 of 55
Sample Extraction Data
Prep Method: SM6200 B
Lab Number Batch Date/TimeInitialFinal
P5J00115090446-01 09/30/15 11:461010mLmL
P5J00115090446-02 09/30/15 11:461010mLmL
P5J00115090446-03 09/30/15 11:461010mLmL
P5J00115090446-04 09/30/15 11:461010mLmL
P5J00115090446-05 09/30/15 11:461010mLmL
P5J00115090446-06 09/30/15 11:461010mLmL
P5J00115090446-07 09/30/15 11:461010mLmL
P5J00115090446-08 09/30/15 11:461010mLmL
P5J00115090446-09 09/30/15 11:461010mLmL
P5J00115090446-10 09/30/15 11:461010mLmL
P5J00115090446-11 09/30/15 11:461010mLmL
P5J00115090446-12 09/30/15 11:461010mLmL
P5J01265090446-13 10/02/15 10:231010mLmL
P5J01265090446-14 10/02/15 10:231010mLmL
P5J01265090446-15 10/02/15 10:231010mLmL
P5J01265090446-16 10/02/15 10:231010mLmL
P5J01265090446-17 10/02/15 10:231010mLmL
P5J01265090446-18 10/02/15 10:231010mLmL
P5J01265090446-19 10/02/15 10:231010mLmL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 53 of 55
Pa
g
e

5
4

o
f

5
5
Pa
g
e

5
5

o
f

5
5

APPENDIX B

503 Industrial Ave • Greensboro, NC 27406 Phone [phone] • Fax [phone] • Toll Free [phone]
Email: [e-mail]
December 11, 2015 James McMillan Sent Via email: [e-mail]

RE: Supply Well Analytical Results 2765 Union Ridge Road, Burlington, NC NCDEQ Incident #12913 Former Harold Smith Grocery Pyramid Project 2015-160
Dear Mr. McMillan:

As directed by the NCDENR and T.A.C., Inc., Pyramid Environmental has continued to collect samples
from the Point-of-Entry (POE) treatment system that is connected to your water supply well. The work is
being performed as part of the ongoing assessment of the referenced underground storage tank release.
The results of the water analyses are presented below.

On September 23, 2015, Pyramid collected influent, midfluent, and effluent samples from the POE
connected to your supply well. The samples are designated as SW2765 INF, SW2765 MID, and SW2765
EFF. The groundwater samples were analyzed at a State certified laboratory and the results are attached
for your review. The laboratory results indicate that the POE influent (untreated water) contained methyl
tert-butyl ether (MTBE) at a concentration of 70 parts per billion (PPB). The current North Carolina
drinking water standard for MTBE is 20 PPB. The compound 1,2-dichloroethane was detected at 13 PPB.
The current North Carolina drinking water standard for 1,2-dichloroethane is 0.4 PPB. The compound
isopropyl ether was detected at 74 PPB. The current North Carolina drinking water standard for isopropyl
ether is 70 PPB. No other targeted compounds were detected at concentrations that exceeded the laboratory detection limits in the POE influent. The laboratory results of the POE effluent sample (treated water) collected on September 23, 2015 indicate that none of the targeted petroleum compounds were detected at concentrations that exceed the
laboratory detection limits. The POE worked to remove petroleum contaminants prior to water use.
Maintenance of the POE treatment system will continue to be performed on a quarterly basis.

If you have any questions, please call Pyramid at [phone]. Thank you for your cooperation with
this project.

Sincerely,
Brett S. Higgins
Project Manager
Attachments – Laboratory Report
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765I
Prism Sample ID: 5090446-17
Prism Work Order: 5090446
Time Collected: 09/23/15 15:15
Time Submitted: 09/24/15 16:10
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5J012612.0 10/2/15 16:22 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0761,2-Dichlorobenzene
13 SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5J012612.0 10/2/15 16:22 KDMCCVug/L 0.112,2-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5J012611010/2/15 16:22 KDMug/L 0.31Acetone
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.048Benzene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.040Bromoform
BRL SM6200 B P5J012611.0 10/2/15 16:22 KDMug/L 0.18Bromomethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.22Chloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.076Chloroform
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.079Chloromethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5J012611.0 10/2/15 16:22 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5J0126120010/2/15 16:22 KDMCVLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765I
Prism Sample ID: 5090446-17
Prism Work Order: 5090446
Time Collected: 09/23/15 15:15
Time Submitted: 09/24/15 16:10
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5J012612.0 10/2/15 16:22 KDMCCVug/L 0.16Hexachlorobutadiene
74 SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.050Isopropyl Ether
0.56 SM6200 B P5J012610.50 10/2/15 16:22 KDMHug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5J012611.0 10/2/15 16:22 KDMCCVug/L 0.12m,p-Xylenes
BRL SM6200 B P5J012611.0 10/2/15 16:22 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5J012615.0 10/2/15 16:22 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5J012611.0 10/2/15 16:22 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5J012612.0 10/2/15 16:22 KDMug/L 0.083Methylene Chloride
70 SM6200 B P5J012611.0 10/2/15 16:22 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5J012611.0 10/2/15 16:22 KDMug/L 0.19Naphthalene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.044o-Xylene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.047Styrene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.044Toluene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5J012615.0 10/2/15 16:22 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5J012610.50 10/2/15 16:22 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5J012611.5 10/2/15 16:22 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13095 %4-Bromofluorobenzene
70-130102 %Dibromofluoromethane
70-130100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765M
Prism Sample ID: 5090446-18
Prism Work Order: 5090446
Time Collected: 09/23/15 15:25
Time Submitted: 09/24/15 16:10
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5J012612.0 10/2/15 16:56 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5J012612.0 10/2/15 16:56 KDMCCVug/L 0.112,2-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5J012611010/2/15 16:56 KDMug/L 0.31Acetone
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.048Benzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.040Bromoform
BRL SM6200 B P5J012611.0 10/2/15 16:56 KDMug/L 0.18Bromomethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.22Chloroethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.076Chloroform
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.079Chloromethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5J012611.0 10/2/15 16:56 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5J0126120010/2/15 16:56 KDMCVLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765M
Prism Sample ID: 5090446-18
Prism Work Order: 5090446
Time Collected: 09/23/15 15:25
Time Submitted: 09/24/15 16:10
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5J012612.0 10/2/15 16:56 KDMCCVug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5J012611.0 10/2/15 16:56 KDMCCVug/L 0.12m,p-Xylenes
BRL SM6200 B P5J012611.0 10/2/15 16:56 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5J012615.0 10/2/15 16:56 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5J012611.0 10/2/15 16:56 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5J012612.0 10/2/15 16:56 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5J012611.0 10/2/15 16:56 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5J012611.0 10/2/15 16:56 KDMug/L 0.19Naphthalene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.044o-Xylene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.047Styrene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.044Toluene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5J012615.0 10/2/15 16:56 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5J012610.50 10/2/15 16:56 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5J012611.5 10/2/15 16:56 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13094 %4-Bromofluorobenzene
70-130110 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765E
Prism Sample ID: 5090446-19
Prism Work Order: 5090446
Time Collected: 09/23/15 15:45
Time Submitted: 09/24/15 16:10
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5J012612.0 10/2/15 17:30 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.111,2-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5J012612.0 10/2/15 17:30 KDMCCVug/L 0.112,2-Dichloropropane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0662-Chlorotoluene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0504-Chlorotoluene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5J012611010/2/15 17:30 KDMug/L 0.31Acetone
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.048Benzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.057Bromobenzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.14Bromochloromethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.062Bromodichloromethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.040Bromoform
BRL SM6200 B P5J012611.0 10/2/15 17:30 KDMug/L 0.18Bromomethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.062Chlorobenzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.22Chloroethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.076Chloroform
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.079Chloromethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.081Dibromochloromethane
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.065Dibromomethane
BRL SM6200 B P5J012611.0 10/2/15 17:30 KDMug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5J0126120010/2/15 17:30 KDMCVLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 41 of 55
Laboratory Report
10/09/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765E
Prism Sample ID: 5090446-19
Prism Work Order: 5090446
Time Collected: 09/23/15 15:45
Time Submitted: 09/24/15 16:10
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.061Ethylbenzene
BRL SM6200 B P5J012612.0 10/2/15 17:30 KDMCCVug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.050Isopropyl Ether
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5J012611.0 10/2/15 17:30 KDMCCVug/L 0.12m,p-Xylenes
BRL SM6200 B P5J012611.0 10/2/15 17:30 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5J012615.0 10/2/15 17:30 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5J012611.0 10/2/15 17:30 KDMug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5J012612.0 10/2/15 17:30 KDMug/L 0.083Methylene Chloride
BRL SM6200 B P5J012611.0 10/2/15 17:30 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5J012611.0 10/2/15 17:30 KDMug/L 0.19Naphthalene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.076n-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.087n-Propylbenzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.044o-Xylene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.076sec-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.047Styrene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.088tert-Butylbenzene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.098Tetrachloroethylene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.044Toluene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.078Trichloroethylene
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5J012615.0 10/2/15 17:30 KDMug/L 0.060Vinyl acetate
BRL SM6200 B P5J012610.50 10/2/15 17:30 KDMug/L 0.097Vinyl chloride
BRL SM6200 B P5J012611.5 10/2/15 17:30 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13097 %4-Bromofluorobenzene
70-130106 %Dibromofluoromethane
70-130103 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 42 of 55

APPENDIX C
Summary of System Installation, Start-up, and Operation Activities
Harold Smith Remediation System
July - September 2015

July Visit:
June 29, 2015 System was operational upon arrival. The technician checked the system
and performed regular operational and maintenance tasks on the system.
The technician then recorded system operational data and measurements.
System was operational at departure.

August Visit:
July 27, 2015 System was not operational at arrival. The technician checked the system
and restarted. The technician performed regular operational and
maintenance tasks on the system. The technician then recorded system
operations data and measurements. System was operational at departure.

September Visit:
August 26, 2015 System was not operational at arrival. The technician checked the system
and restarted. The technician performed regular operational and
maintenance tasks on the system. The technician then recorded system
operations data and measurements. System was operational at departure.