WS-3891_12913_CA_RMR_20150521

503 Industrial Ave • Greensboro, NC 27406 Phone [phone] • Fax [phone] • Toll Free [phone] Email: [e-mail]

May 21, 2015

Mr. Michael Rogers
NC Department of Environment, & Natural Resources
Winston-Salem Regional Office 450 W. Hanes Mill Road, Suite 300
Winston-Salem, NC 27105

RE: 1st Quarter 2015 Active Remediation Monitoring Report
Harold Smith Grocery, Burlington, North Carolina Incident # 12913 Pyramid Job #2014-238
Mr. Rogers:
Pyramid Environmental & Engineering, P.C. has completed the Active Remediation Monitoring
Report for the above referenced site. This report was written to summarize the sampling events
and system maintenance for the 1st quarter of 2015.

Please review the enclosed monitoring report. If you have any questions concerning this report, please call [phone].

Sincerely,

Brett S. Higgins
Project Manager
Copy: Mr. Tom Berry, T.A.C., Inc.

TABLE OF CONTENTS

1.0 INTRODUCTION .............................................................................. 1
1.1 SITE INFORMATION ................................................................................................... 1
1.2 ADJOINING PROPERTIES AND POTENTIAL RECEPTORS .............................................. 1
1.3 SITE HYDROLOGY & GEOLOGY ................................................................................ 2
1.4 PREVIOUS REPORTS ................................................................................................. 2
2.0 GROUNDWATER SAMPLING ....................................................... 3
2.1 MONITORING WELL SAMPLING ................................................................................ 3
2.2 POTABLE WATER SUPPLY WELL SAMPLING............................................................. 3
3.0 SYSTEM OPERATIONAL STATUS .............................................. 4
3.1 SYSTEM OPERATIONS ............................................................................................... 4
3.2 CONTAMINATED SOIL REMOVAL .............................................................................. 5
3.3 SYSTEM UPDATE ...................................................................................................... 5
4.0 SOIL & GROUNDWATER ASSESSMENT ................................... 6
4.1 GROUNDWATER ANALYTICAL RESULTS ................................................................... 6
4.2 SUPPLY WELL ANALYTICAL RESULTS...................................................................... 7
5.0 CONCLUSIONS & RECOMMENDATIONS ................................ 8
6.0 CLOSURE ........................................................................................... 8

Page I
TABLE OF CONTENTS (Continued)

FIGURES:

1. Topographic Map
2. Site Map
3a. Adjoining Properties and Water Supply Wells
3b. Adjoining Properties and Water Supply Wells
4. Potentiometric Surface Map (3/04/15)
5. MTBE Concentration Map (3/04/15)
6. 1,2-Dichloroethane Isoconcentration Map (3/04/15)
7. Remediation System Layout Map (1/16/12)

TABLES:

1. Monitoring Well Construction Details
2. Groundwater Elevation Data
3. Monitoring Well Analytical Results
4. Water Supply Well Analytical Results
5. System Operation Parameters

APPENDICES:

A. Groundwater Laboratory Report & Chain of Custody
B. Supply Well Results Letter (POE)
C. Recent O&M Activities

Page II

ACRONYMS

BLS ................Below Land Surface
BTEX ............Benzene, Toluene, Ethylbenzene, & Xylenes
CFR ................Code of Federal Regulations
COC ...............Chain of Custody
CSA ................Comprehensive Site Assessment
DENR .............Department of Environment and Natural Resources
EPH ................Extractable Petroleum Hydrocarbons
GCLs ..............Gross Contaminant Levels
HASP .............Health & Safety Plan
MADEP..........Massachusetts Department of Environmental Protection
MSCC ............Maximum Soil Contaminant Concentration
MTBE ............Methyl Tertiary Butyl Ether
µg/L ................Micrograms per Liter
mg/kg .............Milligrams per kilogram
MW ................Monitoring Well
NCAC ............North Carolina Administrative Code
O&M ..............Operations and Maintenance
OSHA .............Occupational Safety and Health Administration
OVA ...............Organic Vapor Analyzer
PPM ...............Parts Per Million
PID .................Photo-ionization Detector
P&ID ..............Process & Instrumentation Diagram
PVC ................Poly-vinyl Chloride
QA/QC ...........Quality Assurance / Quality Control
SCFM .............Standard Cubic Feet per Minute
SVE ................Soil Vapor Extraction
SW .................Water Supply Well
UST ................Underground Storage Tank
US EPA ..........United States Environmental Protection Agency
VPH................Volatile Petroleum Hydrocarbons

Page III
Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 1 Pyramid Project # 2014-238 05/21/15
ACTIVE REMEDIATION MONITORING REPORT
Harold Smith Grocery
Burlington, North Carolina

1.0 INTRODUCTION

1.1 Site Information

SITE NAME: Harold Smith Grocery
ADDRESS: 2774 Union Ridge Road
CITY: Burlington, NC
COUNTY: Alamance

CURRENT PROPERTY OWNER: Jessica Alton
CURRENT PROPERTY USE: Inactive Store (used as storage)
OWNER OF USTs: TAC, Inc. (All USTs were removed in 1994)
RESPONSIBLE PARTY: TAC, Inc.
NCDENR UST FACILITY ID: 0-024148
GROUNDWATER INCIDENT NO.: 12913
SITE RANKING: H755E

UNDERGROUND STORAGE TANKS (USTs)

(gallons)
1 550 Kerosene Removed 8/01/94
2 550 Gasoline Removed 8/01/94
3 550 Gasoline Removed 8/01/94
4 1,000 Gasoline Removed 8/01/94

FIGURES: Figure 1: Topographic Map
Figure 2: Site Map
Figure 3a: Adjoining Properties and Water Supply Wells
Figure 3b: Adjoining Properties and Water Supply Wells

1.2 Adjoining Properties and Potential Receptors

ADJOINING PROPERTY USE: Residential/Agricultural
PUBLIC WATER AVAILABILITY: Unavailable
SUPPLY WELLS WITHIN 1000 FEET: Yes (see Figure 3a/b)
SUPPLY WELLS IMPACTED ABOVE
NCAC 2L STANDARDS: Yes, Supply well at 2765 Union Ridge Rd.
(currently on POE system)
Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 2 Pyramid Project # 2014-238 05/21/15

NEAREST SURFACE WATER: Intermittent Creek – 500-600’ SE
BASEMENTS: None
SUBSURFACE UTILITIES: None near source area

1.3 Site Hydrology & Geology

GEOLOGIC PROVINCE: Carolina Slate Belt
BEDROCK TYPE: Felsic Intrusive Complex
DEPTH TO BEDROCK: 25-38 feet BGS (below ground surface)
CURRENT DEPTH TO WATER TABLE: 1.70-13.21 feet BGS (3/4/2015)
HISTORIC GW FLUCTUATIONS: Over the past 14 years, the groundwater has
fluctuated in the source area from 5-15 feet BGS
POTENTIOMETRIC GRADIENT: Southeast ~ 0.025 ft. /ft.
HYDRAULIC CONDUCTIVITY (K): 6.17–6.25 x 10-7 ft. /sec.
GROUNDWATER VELOCITY: ~0.4–1.3 feet/year

1.4 Previous Reports

REPORT TITLE

CONSULTANT
DATE OF
REPORT

COMMENTS

Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 3 Pyramid Project # 2014-238 05/21/15
2.0 GROUNDWATER SAMPLING

2.1 Monitoring Well Sampling

On March 4th and 5th, 2015, selected monitoring wells at the Harold Smith Site were sampled.

WELLS SAMPLED: MW-1A, MW-3, MW-4, MW-5, MW-6, MW-7, MW-9, MW-10,
MW-11, MW-12, MW-13 and MW-15A
LAB ANALYSES: EPA Method 6200B

FREE PRODUCT: No free product has been observed on this site.

TABLES & GRAPHS: Table 1: Monitoring Well Construction Details
Table 2: Groundwater Elevation Data
Table 3: Monitoring Well Analytical Results

FIGURES: Figure 4: Potentiometric Surface Map
Figure 5: MTBE Concentration Map
Figure 6: 1, 2-Dichloroethane Isoconcentration Map

LABORATORY REPORTS & CHAINS-OF-CUSTODY: Appendix A

FIELD PROCEDURES: Field procedures were performed as outlined in the DENR July 15,
2008 and May 1, 2012 updates publication “Guidelines for
Sampling” under the UST Section.

2.2 Potable Water Supply Well Sampling

SAMPLING DATE: March 4-5, 2015
WELLS SAMPLED: 2765 INF, 2765 MID, 2765 EFF, 2760, 2773, and 2779
The house at 2779 Union Ridge Road no longer uses the supply
well in the front yard, but uses the well located on an adjacent
eastern property. The property at 2768 Union Ridge Road uses the
supply well in the back yard and is automatically switched to the
well in the front yard (2768-A) if the water level gets too low.

LAB ANALYSES: EPA Method 6200B

TABLES: Table 4: Water Supply Well Analytical Results
FIGURES: Figure 3 a/b: Adjoining Properties and Water Supply Wells.

LABORATORY REPORTS & CHAINS-OF-CUSTODY: Appendix A

Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 4 Pyramid Project # 2014-238 05/21/15
FIELD PROCEDURES: Field procedures were performed as outlined in the DENR July 15,
2008 and May 1, 2012 updates publication “Guidelines for
Sampling” under the UST Section.

*NOTE* Supply wells are named by the address of the residence they serve and not the property
owner. All supply well addresses sampled are on Union Ridge Road. Mr. James McMillan
requested that Pyramid alert him of the system analytical results after each sampling. That letter
is presented in Appendix B.

3.0 SYSTEM OPERATIONAL STATUS
3.1 System Operations

The air sparging (AS) and soil vapor extraction (SVE) treatment system for the Harold Smith
Grocery site began operation in July 1999 through 2004 when it was shut down.

The system was restarted in February 2005 and the system was operational through October
2005. Repairs were made to the system and the remediation system was officially restarted on
February 8, 2006. The system ran intermittently during the first quarter of 2006, needing minor
repairs. System operation was interrupted by electrical power interruptions (strong storms)
tripping circuit breakers. In August 2006, the system electrical contacts were found to be
completely melted. The electrical components were replaced after pre-approval, and tested. The
motor of the air-sparge compressor would not operate, and the electric motor was found to be
locked up. Pyramid contacted the equipment manufacturer and priced the replacement items
necessary to get the air-sparge system running again. The SVE system continued to run after the
replacement of the circuit breakers.

In March 2007 the rebuilt air sparge motor was put back in service. The restored compressor
operated from March 2007 through June 2008. At this time, the air-sparge compressor needed to
be replaced. The air sparge motor was replaced with a more serviceable model on October 7,
2008. The carbon vanes were changed by Pyramid in February 2010. The air sparge system was
operational during the 1st quarter of 2011. The system ceased operating in March 2011 to allow
for the soil excavation. Since the system operation ceased, DO concentrations dropped and
Pyramid recommended continued air sparging operation to speed site cleanup. In January 2012,
the air sparge system was restarted using the selected remaining air sparge wells.

In 2013, the system was upgraded to include deeper AS wells and a higher pressure compressor.

The system was operational for most of the fourth quarter of 2014, with the exception of two to
three weeks in December when the system was down due a damaged compressor drive belt. The
damaged belt was discovered on 12/12/14 and replaced on 12/19/14 and the system was re-
started. Since restarting the system in December 2014, the system has remained operational. A
summary of the operations and maintenance activities performed from January 2015 through
March 2015 is presented in Appendix C.
Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 5 Pyramid Project # 2014-238 05/21/15
3.2 Contaminated Soil Removal

In March 2009, Pyramid collected risk-based soil samples from several soil borings and added
several monitoring wells. The additional assessment was to investigate the soils in the area of the
former pump island, and provide additional monitoring wells to assess the source area for
regulatory incident closure. The highest groundwater concentrations have been in MW-1
throughout the remediation period. As a result of the additional investigations, an area
approximately 40 feet by 20 feet was identified as containing soil concentrations greater than
Soil-to-Groundwater (STGW) standards. Only the soil boring directly at the location of the
former pump island showed concentrations above residential Maximum Soil Contaminant
Concentrations (MSCCs). The DENR requested that Pyramid evaluate soil excavation as a way
to help move the site toward regulatory closure. After the excavation plan was preapproved by
the DENR, Pyramid implemented the excavation plan.

In May 2011, Pyramid supervised the excavation of petroleum contaminated soils at the Harold
Smith site in Burlington, NC. The goal of the soil excavation was to remove volatile petroleum
hydrocarbons from the smear zone (between 5 and 15 feet BLS) to help reduce groundwater
contamination. Based on certified weight tickets, 483.69 tons of petroleum-contaminated soil
was removed. The laboratory results of the post excavation soil samples collected indicate that all
of the contaminated soils above the residential MSCCs were removed.

The remaining contamination detected at the site was above the STGW MSCCs and well below
the residential standards. The remaining STGW concentrations were located underneath the store
building, along the northern property boundary, and on the eastern edge of the property near
Union Ridge Road. Because of the structures, roads, and utilities, additional soil excavation was
not feasible or recommended.

After the excavation of contaminated soil, Pyramid installed replacement monitoring wells for
MW-1 and MW-15 to assess the groundwater in the source area. The latest results of these new
wells since (MW-1A and MW-15A) are included in Section 4.0 with past results located in
Table 3.

3.3 System Update

FIGURES: Figure 7: Remediation System Layout Map

To prevent the migration of the contaminant plume, protect nearby supply wells, and speed up
remediation, the current air sparge (AS) and soil vapor extraction (SVE) system was updated in
October 2012. Additional wells were added to the air sparge segment of the remediation system.
Seven deeper air sparge wells were added to surround the existing petroleum contaminant plume.
The additional wells prevent contaminant plume migration and provide additional air flow for
petroleum hydrocarbons volatilization. Along with the AS remediation update, the soil vapor
extraction system was repaired due to the damage the system incurred during soil excavation in
May 2011. A map of the Remediation System Layout is shown in Figure 7.

Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 6 Pyramid Project # 2014-238 05/21/15
4.0 SOIL & GROUNDWATER ASSESSMENT

4.1 Groundwater Analytical Results

The results of the March 4-5, 2015 sampling event showed that remaining petroleum
contaminants were detected at low concentrations. All of the reported concentrations are listed in
micrograms per liter (µg/L). The concentration of 1,2-Dichloroethane in MW-1A was above the
2L groundwater standards. The concentrations of targeted compounds for this sampling event
have decreased or remained the same in all of the monitoring wells. The exception is MW15-A,
which showed increases in benzene (1.1 µg/L), toluene (58 µg/L), ethylbenzene (120 µg/L),
xylenes (570 µg/L), and naphthalene (33 µg/L). The highest concentrations found for this
sampling event are shown below. The MW concentrations above NCAC 2L groundwater
standards are shown in bold and the associated well numbers are shown in parentheses. All of the
reported concentrations are listed in micrograms per liter (µg/L)

• Benzene 1.1 µg/L (MW-15A)
• Toluene 58 µg/L (MW-15A)
• Ethylbenzene 120 µg/L (MW-15A)
• Total Xylenes 570 µg/L (MW-15A)
• MTBE 4.6 µg/L (MW-1A)
• 1,2-Dichloroethane 2.7 µg/L (MW-1A)
• Naphthalene 33 µg/L (MW-15A)

Over the past 14 years of groundwater and soil remediation, the general concentration trends
demonstrated in the groundwater monitoring wells have been decreasing and are now
approaching regulatory closure.

The benzene concentrations in MW-1A have decreased from over 8,000 µg/L in 1998 to below
detectable levels for the current monitoring period. Benzene concentrations in MW-15A (1.1
µg/L) increased from a concentration below detection limits in the November 2014 sampling
event. MTBE concentrations in MW-1A have decreased from 610 µg/L in 1999 to 4.6 µg/L for
the current monitoring period. Concentrations of 1,2-dichloroethane were detected in MW-1A
remain above the 2L Standard.

In planning for the soil excavation project, Pyramid recommended that the DENR consider the
placement of oxygen-release compounds in the excavation to help clean up the site. Since
cleanup will have to be to the NCAC 2L Standards, any remedial process that can help reach
regulatory closure more quickly should be considered by the DENR. Pyramid’s request was not
approved for Trust Fund reimbursement, and no oxygen-release compounds were used in the
excavation. In the future, the Trust Fund should consider reimbursing the use of oxygen-release
compounds while excavations are open to help reduce the overall costs for petroleum incident
closures.

Active soil and groundwater remediation are needed to reduce the petroleum contaminant
concentrations in the groundwater.
Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 7 Pyramid Project # 2014-238 05/21/15
4.2 Supply Well Analytical Results

Supply well sampling was conducted on March 4-5, 2015 as required by the State. Pyramid
sampled four supply wells 2765, 2760, 2773, and 2779. Samples were also collected from the
point of entry (POE) treatment system, 2765 mid-fluent and 2765 effluent. Samples were
collected in laboratory provided containers using clean, disposable nitrile gloves, packed in ice
and shipped to Prism Analytical Laboratories for analysis using EPA Method 6200B.

Groundwater pumped from the supply well at address 2765 (SW-2765) is treated by a Point-of-
Entry (POE) treatment system installed in 2000. The POE system consists of particulate and
carbon filters that remove petroleum from the groundwater. This residential treatment system has
shown effective groundwater treatment since 2000. The laboratory results of treated water
samples collected from the supply well in March 2015 show no detections of petroleum
contaminants.

For the untreated water from SW-2765, MTBE (80 µg/L), IPE (100 µg/L) and 1,2-dichloroethane
(16 µg/L) were detected above their respective NCAC 2L Groundwater Standards. No petroleum
hydrocarbon concentrations were detected in the effluent (treated water) showing effective POE
treatment. Table 4 shows the recent supply well analytical results. A copy of the laboratory
report and chain-of-custody form is presented in Appendix A.

The supply well samples from SW-2773 showed no petroleum contaminants above the 2L
standards. This supply well has shown no petroleum impacts in the past several year. In the
March sample analysis, there was an “Estimated” detection of trans-1,2-dichloroethene reported
by the laboratory. The Prism lab report stated:

“For sample 5030124-05 with client ID of SW-2773, the initial 6200 was analyzed
undiluted and showed a large hit of Trans-1,2-dichloroethene that was outside of
calibration range. Dilutions of 1:20 and 1:50 were analyzed and the Trans-1,2-
dichloroethene did not duplicate. Vials were checked for accuracy in labeling and were
correct. The initial run is reported with an "E" flag to show an estimated value. “

Basically the initial detection was not confirmed and is suspect. Pyramid recommends re-
sampling the well in June which was planned and pre-approved by the Trust Fund. The results
will be reported to the DENR in the next quarterly report. Since the residence is provided with
bottled water at this time, the potential for exposure is mitigated. Pyramid plans to re-sample
SW-2773 in June 2015.

Laboratory analytical results show that there were no detectable petroleum hydrocarbon
concentrations in the supply well samples collected from wells 2760, 2773 and 2779.

Pyramid recommends continued POE treatment of supply well 2765, continued sampling of the
closest supply wells (2765 & 2773) on a quarterly basis, and continued sampling of the wells
further from the source area (2761, 2768, 2774, and 2779) on an annual basis. The next quarterly
sampling event will be in June 2015.

Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 8 Pyramid Project # 2014-238 05/21/15
5.0 CONCLUSIONS & RECOMMENDATIONS

Pyramid has completed the directed operation & maintenance and groundwater monitoring at the
Harold Smith Grocery. Based on the current groundwater concentrations of MTBE, IPE, and 1,2-
Dichloroethane remaining above the 2L groundwater standard, the site remains high risk. The
remediation goal is to reduce dissolved groundwater contamination below 2L standards to protect
local water supply well users.

• The soil excavation was completed in May 2011. Contaminated soil beneath the NC DOT
Right of Way and under the store building was unable to be removed. Because of the
petroleum concentrations remain above STGW levels under the building and near the
roadway, continued soil remediation using the SVE system is recommended.

• Based on the risk to private well users, Pyramid recommended a new air-sparge system
with deeper air sparge wells to enhance the groundwater cleanup. This new system was
designed, bid, pre-approved, and built from October 2012 through April 2013. The
system was successfully started on April 3, 2013. The new system has shown significant
reductions in the remaining petroleum contaminants.

• The continued presence of concentrations of petroleum contaminants (SW-2765) show
that groundwater contamination remains above regulatory closure levels. Pyramid also
recommends continued quarterly sampling of the high-risk supply wells surrounding the
Harold Smith site. The next quarterly sampling of the supply wells will be in June 2015.

• Continued groundwater remediation and monitoring is recommended for the site. The
next semi-annual sampling of the monitoring wells will be conducted in June 2015.

6.0 CLOSURE

This report is prepared for and made available solely for the use of T.A.C, Inc. and the
NCDENR, and the contents thereof may not be used or relied upon by any other person without
the express written consent and authorization of Pyramid Environmental & Engineering, P.C.
The observations, conclusions, and recommendations documented in this report are based on site
conditions and information reviewed at the time of the investigation. Pyramid Environmental &
Engineering, P.C. appreciates the opportunity to provide this environmental service.

FIGURES

TABLES
TABLE 1
Monitoring Well Construction Details Harold Smith Grocery Incident #12913
Union Ridge Road, Burlington, North Carolina

MONITORING WELL DATE INSTALLED WELL DEPTH DEPTH TO BEDROCK OUTER CASING RISER INTERVAL SCREEN INTERVAL GROUT INTERVAL BENTONITE INTERVAL SAND INTERVAL
MW-1 11/21/94 20’ NBE NA 0-10’ 10-20’ 0-6’ 6-7.5 7.5-20’
MW-1A 6/27/11 24’ NBE NA 0-4’ 4-24’ 0-1’ 1-3’ 3-24’
MW-2 10/11/95 25’ 25’ NA 0-10’ 10-20’ 0-6’ 6-8’ 8-20’
MW-3 10/11/95 22’ NBE NA 0-7’ 7-22’ 0-3’ 3-5’ 5-22’
MW-4 11/8/95 20’ NBE NA 0-5’ 5-20’ 0-2’ 2-4’ 4-20’
MW-5 11/8/95 20’ NBE NA 0-5’ 5-20’ 0-2’ 2-4’ 4-20’
MW-6 1/2/96 53’ 25’ 0-30’ 0-43’ 43-53’ 0-38’ 38-41’ 41-53’
MW-7 1/3/96 13.8’ NBE NA 0-3.8’ 3.8-13.8’ 0-0.5’ 0.5-1.5’ 1.5-13.8’
MW-8 5/6/96 14.3’ 15’ NA 0-4.3’ 4.3-14.3’ 0-1.8’ 1.8-3.3’ 3.3-14.3’
MW-9 5/6/96 15’ NBE NA 0-5’ 5-15’ 0-2.5’ 2.5-4’ 6/4-15’
MW-10 11/30/99 20’ NBE NA 0-5’ 5-20’ 0.5-2’ 2-4’ 4-20’
MW-11 7/25/00 20’ NA NA 0-5’ 5-20’ 0.5-2’ 2-4’ 4-20’
MW-12 11/6/01 30’ NBE NA 0-10’ 10-30’ 0-6’ 6-8’ 8-30’
MW-13 3/5/09 25’ NBE NA 0-5’ 5-25’ 0-1’ 1-3’ 3-25’
MW-14 3/5/09 25’ NBE NA 0-5’ 5-25’ 0-1’ 1-3’ 3-25’
MW-15 3/5/09 25’ 24’ NA 0-5’ 5-25’ 0-1’ 1-3' 3-25’
MW-15A 6/27/11 24’ NBE NA 0-4’ 4-24’ 0-1’ 1-3’ 3-24’
TS-1 12/17/99 15’ NBE NA 0-5’ 5-15’ 0-2’ 2-4’ 4-15’
TS-2 12/17/99 15’ NBE NA 0-5’ 5-15’ 0-2’ 2-4’ 4-15’
TS-3 12/17/99 15’ NBE NA 0-5’ 5-15’ 0-2’ 2-4’ 4-15’
ALL MONITORING WELLS HAVE 2” PVC CASING/RISER AND 2” PVC SCREEN WITH 0.01” SLOTS. OUTER CASING FOR TYPE III WELL IS 6” PVC.
NBE = NO BEDROCK ENCOUNTERED. NA = NOT APPLICABLE. SHADED WELLS ARE CLOSED.
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
(feet)(feet)(feet) (feet) (feet) (feet) (feet)
MW-1A installed 06-30-11 94.650 12.24 0.00 0.00 0.00 12.24 82.41
09-8-11 94.650 13.59 0.00 0.00 0.00 13.59 81.06
12-8-11 94.650 13.49 0.00 0.00 0.00 13.49 81.16
03-13-12 94.650 13.49 0.00 0.00 0.00 12.35 82.30
06-5-12 94.650 12.14 0.00 0.00 0.00 12.14 82.51
09-11-12 94.650 13.22 0.00 0.00 0.00 13.22 81.43
12-12-12 94.650 13.85 0.00 0.00 0.00 13.85 80.80
03-12-13 94.650 11.83 0.00 0.00 0.00 11.83 82.82
05-29-13 94.650 10.44 0.00 0.00 0.00 10.44 84.21
09-10-13 94.650 8.96 0.00 0.00 0.00 8.96 85.69
11-6-13 94.650 10.96 0.00 0.00 0.00 10.96 83.69
03-19-14 94.650 8.07 0.00 0.00 0.00 8.07 86.58
06-26-14 94.650 8.72 0.00 0.00 0.00 8.72 85.93
08-22-14 94.650 10.13 0.00 0.00 0.00 10.13 84.52
11-7-14 94.650 12.00 0.00 0.00 0.00 12.00 82.65
03-4-15 94.650 11.21 0.00 0.00 0.00 11.21 83.44
MW-3 09-9-09 93.065 12.03 0.00 0.00 0.00 12.03 81.04
12-3-09 93.065 10.40 0.00 0.00 0.00 10.40 82.67
03-24-10 93.065 7.34 0.00 0.00 0.00 7.34 85.73
06-24-10 93.065 8.07 0.00 0.00 0.00 8.07 85.00
09-8-10 93.065 9.62 0.00 0.00 0.00 9.62 83.45
12-10-10 93.065 10.77 0.00 0.00 0.00 10.77 82.30
03-8-11 93.065 10.60 0.00 0.00 0.00 10.60 82.47
06-30-11 93.065 10.74 0.00 0.00 0.00 10.74 82.33
09-8-11 93.065 12.16 0.00 0.00 0.00 12.16 80.91
12-8-11 93.065 12.06 0.00 0.00 0.00 12.06 81.01
03-13-12 93.065 13.49 0.00 0.00 0.00 10.52 82.55
06-5-12 93.065 10.71 0.00 0.00 0.00 10.71 82.36
09-11-12 93.065 11.79 0.00 0.00 0.00 11.79 81.28
12-12-12 93.065 12.37 0.00 0.00 0.00 12.37 80.70
03-12-13 93.065 10.53 0.00 0.00 0.00 10.53 82.54
05-29-13 93.065 9.04 0.00 0.00 0.00 9.04 84.03
09-10-13 93.065 7.53 0.00 0.00 0.00 7.53 85.54
11-6-13 93.065 8.88 0.00 0.00 0.00 8.88 84.19
03-19-14 93.065 6.69 0.00 0.00 0.00 6.69 86.38
06-26-14 93.065 7.46 0.00 0.00 0.00 7.46 85.61
08-22-14 93.065 8.82 0.00 0.00 0.00 8.82 84.25
11-7-14 93.065 10.84 0.00 0.00 0.00 10.84 82.23
03-4-15 93.065 8.51 0.00 0.00 0.00 8.51 84.56
MW-4 09-9-09 91.470 10.81 0.00 0.00 0.00 10.81 80.66
12-3-09 91.470 9.11 0.00 0.00 0.00 9.11 82.36
03-24-10 91.470 6.10 0.00 0.00 0.00 6.10 85.37
06-24-10 91.470 6.76 0.00 0.00 0.00 6.76 84.71
09-8-10 91.470 8.41 0.00 0.00 0.00 8.41 83.06
12-10-10 91.470 9.55 0.00 0.00 0.00 9.55 81.92
03-8-11 91.470 9.37 0.00 0.00 0.00 9.37 82.10
06-30-11 91.470 9.53 0.00 0.00 0.00 9.53 81.94
09-8-11 91.470 11.12 0.00 0.00 0.00 11.12 80.35
12-8-11 91.470 10.81 0.00 0.00 0.00 10.81 80.66
03-13-12 91.470 13.49 0.00 0.00 0.00 8.58 82.89
06-5-12 91.470 9.50 0.00 0.00 0.00 9.50 81.97
09-11-12 91.470 10.67 0.00 0.00 0.00 10.67 80.80
12-12-12 91.470 11.15 0.00 0.00 0.00 11.15 80.32
03-12-13 91.470 8.84 0.00 0.00 0.00 8.84 82.63
05-29-13 91.470 7.80 0.00 0.00 0.00 7.80 83.67
09-10-13 91.470 6.33 0.00 0.00 0.00 6.33 85.14
11-6-13 91.470 7.70 0.00 0.00 0.00 7.70 83.77
03-19-14 91.470 5.51 0.00 0.00 0.00 5.51 85.96
06-26-14 91.470 6.18 0.00 0.00 0.00 6.18 85.29
08-22-14 91.470 7.58 0.00 0.00 0.00 7.58 83.89
11-7-14 91.470 9.62 0.00 0.00 0.00 9.62 81.85
03-4-15 91.470 7.55 0.00 0.00 0.00 7.55 83.92
MW-5 09-9-09 95.045 12.81 0.00 0.00 0.00 12.81 82.24
12-3-09 95.045 6.35 0.00 0.00 0.00 6.35 88.70
03-24-10 95.045 6.63 0.00 0.00 0.00 6.63 88.42
06-24-10 95.045 8.25 0.00 0.00 0.00 8.25 86.80
09-8-10 95.045 10.34 0.00 0.00 0.00 10.34 84.71
12-10-10 95.045 9.78 0.00 0.00 0.00 9.78 85.27
03-8-11 95.045 7.20 0.00 0.00 0.00 7.20 87.85
06-30-11 95.045 8.53 0.00 0.00 0.00 8.53 86.52
09-8-11 95.045 12.62 0.00 0.00 0.00 12.62 82.43
12-8-11 95.045 8.74 0.00 0.00 0.00 8.74 86.31
03-13-12 95.045 13.49 0.00 0.00 0.00 10.94 84.11
06-5-12 95.045 10.87 0.00 0.00 0.00 10.87 84.18
09-11-12 95.045 11.98 0.00 0.00 0.00 11.98 83.07
12-12-12 95.045 13.20 0.00 0.00 0.00 13.20 81.85
03-12-13 95.045 7.32 0.00 0.00 0.00 7.32 87.73
05-29-13 95.045 9.38 0.00 0.00 0.00 9.38 85.67
09-10-13 95.045 8.16 0.00 0.00 0.00 8.16 86.89
11-6-13 95.045 9.53 0.00 0.00 0.00 9.53 85.52
03-19-14 95.045 2.87 0.00 0.00 0.00 2.87 92.18
06-26-14 95.045 7.78 0.00 0.00 0.00 7.78 87.27
08-22-14 95.045 9.06 0.00 0.00 0.00 9.06 85.99
11-7-14 95.045 11.16 0.00 0.00 0.00 11.16 83.89
03-4-15 95.045 1.70*0.00 0.00 0.00 1.70* 93.35
TABLE 2
Union Ridge Road, Burlington, North carolina
Groundwater Elevation Data
Harold Smith GrocerIncident #12913
Page 1 of 4
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
(feet)(feet)(feet) (feet) (feet) (feet) (feet)
TABLE 2
Union Ridge Road, Burlington, North carolina
Groundwater Elevation Data
Harold Smith GrocerIncident #12913
MW-6*09-9-09 94.935 14.28 0.00 0.00 0.00 14.28 80.66
12-3-09 94.935 12.98 0.00 0.00 0.00 12.98 81.96
03-24-10 94.935 9.07 0.00 0.00 0.00 9.07 85.87
06-24-10 94.935 9.90 0.00 0.00 0.00 9.90 85.04
09-8-10 94.935 11.76 0.00 0.00 0.00 11.76 83.18
12-10-10 94.935 12.91 0.00 0.00 0.00 12.91 82.03
03-8-11 94.935 12.89 0.00 0.00 0.00 12.89 82.05
06-30-11 94.935 12.91 0.00 0.00 0.00 12.91 82.03
09-8-11 94.935 14.50 0.00 0.00 0.00 14.50 80.44
12-8-11 94.935 14.20 0.00 0.00 0.00 14.20 80.74
03-13-12 94.935 13.49 0.00 0.00 0.00 12.94 82.00
06-5-12 94.935 13.10 0.00 0.00 0.00 13.10 81.84
09-11-12 94.935 14.26 0.00 0.00 0.00 14.26 80.68
12-12-12 94.935 14.58 0.00 0.00 0.00 14.58 80.36
03-12-13 94.935 12.72 0.00 0.00 0.00 12.72 82.22
05-29-13 94.935 11.38 0.00 0.00 0.00 11.38 83.56
09-10-13 94.935 9.65 0.00 0.00 0.00 9.65 85.29
11-6-13 94.935 11.29 0.00 0.00 0.00 11.29 83.65
03-19-14 94.935 8.58 0.00 0.00 0.00 8.58 86.36
06-26-14 94.935 9.39 0.00 0.00 0.00 9.39 85.55
08-22-14 94.935 11.01 0.00 0.00 0.00 11.01 83.93
11-7-14 94.935 12.99 0.00 0.00 0.00 12.99 81.95
03-4-15 94.935 12.11 0.00 0.00 0.00 12.11 82.83
MW-7 09-9-09 94.215 11.61 0.00 0.00 0.00 11.61 82.61
12-3-09 94.215 9.65 0.00 0.00 0.00 9.65 84.57
03-24-10 94.215 7.69 0.00 0.00 0.00 7.69 86.53
06-24-10 94.215 7.55 0.00 0.00 0.00 7.55 86.67
09-8-10 94.215 8.18 0.00 0.00 0.00 8.18 86.04
12-10-10 94.215 10.36 0.00 0.00 0.00 10.36 83.86
03-8-11 94.215 9.94 0.00 0.00 0.00 9.94 84.28
06-30-11 94.215 10.92 0.00 0.00 0.00 10.92 83.30
09-8-11 94.215 12.05 0.00 0.00 0.00 12.05 82.17
12-8-11 94.215 11.64 0.00 0.00 0.00 11.64 82.58
03-13-12 94.215 13.49 0.00 0.00 0.00 10.75 83.47
06-5-12 94.215 10.63 0.00 0.00 0.00 10.63 83.59
09-11-12 94.215 11.33 0.00 0.00 0.00 11.33 82.89
12-12-12 94.215 12.20 0.00 0.00 0.00 12.20 82.02
03-12-13 94.215 NG 0.00 0.00 0.00 0.00 NG
05-29-13 94.215 NG 0.00 0.00 0.00 0.00 NG
09-10-13 94.215 7.57 0.00 0.00 0.00 7.57 86.65
11-6-13 94.215 9.08 0.00 0.00 0.00 9.08 85.14
03-19-14 94.215 6.95 0.00 0.00 0.00 6.95 87.27
06-26-14 94.215 7.47 0.00 0.00 0.00 7.47 86.75
08-22-14 94.215 8.70 0.00 0.00 0.00 8.70 85.52
11-7-14 94.215 10.60 0.00 0.00 0.00 10.60 83.62
03-4-15 94.215 9.40 0.00 0.00 0.00 9.40 84.82
MW-8 09-9-09 89.630 NG 0.00 0.00 0.00 0.00 NG
12-3-09 89.630 7.23 0.00 0.00 0.00 7.23 82.40
03-24-10 89.630 5.64 0.00 0.00 0.00 5.64 83.99
06-24-10 89.630 6.13 0.00 0.00 0.00 6.13 83.50
09-8-10 89.630 7.79 0.00 0.00 0.00 7.79 81.84
12-10-10 89.630 9.43 0.00 0.00 0.00 9.43 80.20
03-8-11 89.630 8.39 0.00 0.00 0.00 8.39 81.24
06-30-11 89.630 NG 0.00 0.00 0.00 0.00 NG
09-8-11 89.630 NG 0.00 0.00 0.00 0.00 NG
12-8-11 89.630 NG 0.00 0.00 0.00 0.00 NG
03-13-12 89.630 NG 0.00 0.00 0.00 0.00 NG
06-5-12 89.630 8.80 0.00 0.00 0.00 8.80 80.83
09-11-12 89.630 9.84 0.00 0.00 0.00 9.84 79.79
12-12-12 89.630 10.60 0.00 0.00 0.00 10.60 79.03
03-12-13 89.630 NG 0.00 0.00 0.00 0.00 NG
05-29-13 89.630 NG 0.00 0.00 0.00 0.00 NG
09-10-13 89.630 NG 0.00 0.00 0.00 0.00 NG
11-6-13 89.630 NG 0.00 0.00 0.00 0.00 NG
03-19-14 89.630 NG 0.00 0.00 0.00 0.00 NG
06-26-14 89.630 NG 0.00 0.00 0.00 0.00 NG
08-22-14 89.630 NG 0.00 0.00 0.00 0.00 NG
11-7-14 89.630 NG 0.00 0.00 0.00 0.00 NG
03-4-15 89.630 NG 0.00 0.00 0.00 0.00 NG
MW-9 09-9-09 94.770 14.21 0.00 0.00 0.00 14.21 80.56
12-3-09 94.770 12.76 0.00 0.00 0.00 12.76 82.01
03-24-10 94.770 8.91 0.00 0.00 0.00 8.91 85.86
06-24-10 94.770 9.79 0.00 0.00 0.00 9.79 84.98
09-8-10 94.770 11.70 0.00 0.00 0.00 11.70 83.07
12-10-10 94.770 12.89 0.00 0.00 0.00 12.89 81.88
03-8-11 94.770 12.79 0.00 0.00 0.00 12.79 81.98
06-30-11 94.770 NG 0.00 0.00 0.00 0.00 NG
09-8-11 94.770 14.34 0.00 0.00 0.00 14.34 80.43
12-8-11 94.770 14.09 0.00 0.00 0.00 14.09 80.68
03-13-12 94.770 13.49 0.00 0.00 0.00 11.82 82.95
06-5-12 94.770 NG 0.00 0.00 0.00 0.00 NG
09-11-12 94.770 14.15 0.00 0.00 0.00 14.15 80.62
12-12-12 94.770 NG 0.00 0.00 0.00 0.00 NG
03-12-13 94.770 12.60 0.00 0.00 0.00 12.60 82.17
05-29-13 94.770 11.20 0.00 0.00 0.00 11.20 83.57
09-10-13 94.770 9.50 0.00 0.00 0.00 9.50 85.27
11-6-13 94.770 11.16 0.00 0.00 0.00 11.16 83.61
03-19-14 94.770 8.18 0.00 0.00 0.00 8.18 86.59
06-26-14 94.770 9.30 0.00 0.00 0.00 9.30 85.47
08-22-14 94.770 10.88 0.00 0.00 0.00 10.88 83.89
11-7-14 94.770 12.92 0.00 0.00 0.00 12.92 81.85
03-4-15 94.770 12.00 0.00 0.00 0.00 12.00 82.77
Page 2 of 4
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
(feet)(feet)(feet) (feet) (feet) (feet) (feet)
TABLE 2
Union Ridge Road, Burlington, North carolina
Groundwater Elevation Data
Harold Smith GrocerIncident #12913
MW-10 09-9-09 93.210 13.25 0.00 0.00 0.00 13.25 79.96
12-3-09 93.210 10.51 0.00 0.00 0.00 10.51 82.70
03-24-10 93.210 7.80 0.00 0.00 0.00 7.80 85.41
06-24-10 93.210 8.77 0.00 0.00 0.00 8.77 84.44
09-8-10 93.210 10.74 0.00 0.00 0.00 10.74 82.47
12-10-10 93.210 12.15 0.00 0.00 0.00 12.15 81.06
03-8-11 93.210 11.78 0.00 0.00 0.00 11.78 81.43
06-30-11 93.210 12.29 0.00 0.00 0.00 12.29 80.92
09-8-11 93.210 13.39 0.00 0.00 0.00 13.39 79.82
12-8-11 93.210 12.91 0.00 0.00 0.00 12.91 80.30
03-13-12 93.210 13.49 0.00 0.00 0.00 11.61 81.60
06-5-12 93.210 11.79 0.00 0.00 0.00 11.79 81.42
09-11-12 93.210 13.10 0.00 0.00 0.00 13.10 80.11
12-12-12 93.210 13.29 0.00 0.00 0.00 13.29 79.92
03-12-13 93.210 10.93 0.00 0.00 0.00 10.93 82.28
05-29-13 93.210 10.03 0.00 0.00 0.00 10.03 83.18
09-10-13 93.210 8.61 0.00 0.00 0.00 8.61 84.60
11-6-13 93.210 10.11 0.00 0.00 0.00 10.11 83.10
03-19-14 93.210 6.68 0.00 0.00 0.00 6.68 86.53
06-26-14 93.210 8.43 0.00 0.00 0.00 8.43 84.78
08-22-14 93.210 10.00 0.00 0.00 0.00 10.00 83.21
11-7-14 93.210 11.98 0.00 0.00 0.00 11.98 81.23
03-4-15 93.210 10.66 0.00 0.00 0.00 10.66 82.55
MW-11 09-9-09 95.840 NG 0.00 0.00 0.00 0.00 NG
12-3-09 95.840 14.05 0.00 0.00 0.00 14.05 81.79
03-24-10 95.840 10.06 0.00 0.00 0.00 10.06 85.78
06-24-10 95.840 10.91 0.00 0.00 0.00 10.91 84.93
09-8-10 95.840 12.77 0.00 0.00 0.00 12.77 83.07
12-10-10 95.840 14.00 0.00 0.00 0.00 14.00 81.84
03-8-11 95.840 13.94 0.00 0.00 0.00 13.94 81.90
06-30-11 95.840 13.92 0.00 0.00 0.00 13.92 81.92
09-8-11 95.840 15.52 0.00 0.00 0.00 15.52 80.32
12-8-11 95.840 15.21 0.00 0.00 0.00 15.21 80.63
03-13-12 95.840 13.49 0.00 0.00 0.00 13.94 81.90
06-5-12 95.840 14.16 0.00 0.00 0.00 14.16 81.68
09-11-12 95.840 15.36 0.00 0.00 0.00 15.36 80.48
12-12-12 95.840 15.60 0.00 0.00 0.00 15.60 80.24
03-12-13 95.840 13.88 0.00 0.00 0.00 13.88 81.96
05-29-13 95.840 12.35 0.00 0.00 0.00 12.35 83.49
09-10-13 95.840 10.64 0.00 0.00 0.00 10.64 85.20
11-6-13 95.840 12.35 0.00 0.00 0.00 12.35 83.49
03-19-14 95.840 9.58 0.00 0.00 0.00 9.58 86.26
06-26-14 95.840 10.41 0.00 0.00 0.00 10.41 85.43
08-22-14 95.840 12.02 0.00 0.00 0.00 12.02 83.82
11-7-14 95.840 14.04 0.00 0.00 0.00 14.04 81.80
03-4-15 95.840 13.21 0.00 0.00 0.00 13.21 82.63
MW-12 09-9-09 94.270 14.70 0.00 0.00 0.00 14.70 79.57
12-3-09 94.270 13.45 0.00 0.00 0.00 13.45 80.82
03-24-10 94.270 9.50 0.00 0.00 0.00 9.50 84.77
06-24-10 94.270 10.36 0.00 0.00 0.00 10.36 83.91
09-8-10 94.270 12.26 0.00 0.00 0.00 12.26 82.01
12-10-10 94.270 13.43 0.00 0.00 0.00 13.43 80.84
03-8-11 94.270 13.35 0.00 0.00 0.00 13.35 80.92
06-30-11 94.270 13.42 0.00 0.00 0.00 13.42 80.85
09-8-11 94.270 15.05 0.00 0.00 0.00 15.05 79.22
12-8-11 94.270 14.66 0.00 0.00 0.00 14.66 79.61
03-13-12 94.270 13.49 0.00 0.00 0.00 13.43 80.84
06-5-12 94.270 13.58 0.00 0.00 0.00 13.58 80.69
09-11-12 94.270 14.79 0.00 0.00 0.00 14.79 79.48
12-12-12 94.270 15.04 0.00 0.00 0.00 15.04 79.23
03-12-13 94.270 13.24 0.00 0.00 0.00 13.24 81.03
05-29-13 94.270 11.79 0.00 0.00 0.00 11.79 82.48
09-10-13 94.270 10.08 0.00 0.00 0.00 10.08 84.19
11-6-13 94.270 11.73 0.00 0.00 0.00 11.73 82.54
03-19-14 94.270 8.92 0.00 0.00 0.00 8.92 85.35
06-26-14 94.270 9.86 0.00 0.00 0.00 9.86 84.41
08-22-14 94.270 11.43 0.00 0.00 0.00 11.43 82.84
11-7-14 94.270 13.45 0.00 0.00 0.00 13.45 80.82
03-4-15 94.270 12.59 0.00 0.00 0.00 12.59 81.68
MW-13 03-18-09 94.805 13.58 0.00 0.00 0.00 13.58 81.23
06-23-09 94.805 11.01 0.00 0.00 0.00 11.01 83.80
09-9-09 94.805 12.61 0.00 0.00 0.00 12.61 82.20
12-3-09 94.805 11.26 0.00 0.00 0.00 11.26 83.55
03-24-10 94.805 7.92 0.00 0.00 0.00 7.92 86.89
06-24-10 94.805 10.56 0.00 0.00 0.00 10.56 84.25
09-8-10 94.805 9.82 0.00 0.00 0.00 9.82 84.99
12-10-10 94.805 10.93 0.00 0.00 0.00 10.93 83.88
03-8-11 94.805 11.24 0.00 0.00 0.00 11.24 83.57
06-30-11 94.805 10.73 0.00 0.00 0.00 10.73 84.08
09-8-11 94.805 12.51 0.00 0.00 0.00 12.51 82.30
12-8-11 94.805 12.69 0.00 0.00 0.00 12.69 82.12
03-13-12 94.805 13.49 0.00 0.00 0.00 10.48 84.33
06-5-12 94.805 10.28 0.00 0.00 0.00 10.28 84.53
09-11-12 94.805 11.55 0.00 0.00 0.00 11.55 83.26
12-12-12 94.805 13.55 0.00 0.00 0.00 13.55 81.26
03-12-13 94.805 10.33 0.00 0.00 0.00 10.33 84.48
05-29-13 94.805 9.41 0.00 0.00 0.00 9.41 85.40
09-10-13 94.805 7.78 0.00 0.00 0.00 7.78 87.03
11-6-13 94.805 9.36 0.00 0.00 0.00 9.36 85.45
03-19-14 94.805 6.88 0.00 0.00 0.00 6.88 87.93
06-26-14 94.805 7.53 0.00 0.00 0.00 7.53 87.28
08-22-14 94.805 8.60 0.00 0.00 0.00 8.60 86.21
11-7-14 94.805 10.69 0.00 0.00 0.00 10.69 84.12
03-4-15 94.805 9.46 0.00 0.00 0.00 9.46 85.35
Page 3 of 4
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
(feet)(feet)(feet) (feet) (feet) (feet) (feet)
TABLE 2
Union Ridge Road, Burlington, North carolina
Groundwater Elevation Data
Harold Smith GrocerIncident #12913
MW-14 03-18-09 94.395 NG 0.00 0.00 0.00 0.00 NG
06-23-09 94.395 NG 0.00 0.00 0.00 0.00 NG
09-9-09 94.395 NG 0.00 0.00 0.00 0.00 NG
12-3-09 94.395 NG 0.00 0.00 0.00 0.00 NG
03-24-10 94.395 NG 0.00 0.00 0.00 0.00 NG
06-24-10 94.395 NG 0.00 0.00 0.00 0.00 NG
09-8-10 94.395 NG 0.00 0.00 0.00 0.00 NG
12-10-10 94.395 NG 0.00 0.00 0.00 0.00 NG
03-8-11 94.395 NG 0.00 0.00 0.00 0.00 NG
06-30-11 94.395 NG 0.00 0.00 0.00 0.00 NG
09-8-11 94.395 NG 0.00 0.00 0.00 0.00 NG
12-8-11 94.395 NG 0.00 0.00 0.00 0.00 NG
03-13-12 94.395 NG 0.00 0.00 0.00 0.00 NG
06-5-12 94.395 NG 0.00 0.00 0.00 0.00 NG
09-11-12 94.395 NG 0.00 0.00 0.00 0.00 NG
12-12-12 94.395 NG 0.00 0.00 0.00 0.00 NG
03-12-13 94.395 NG 0.00 0.00 0.00 0.00 NG
05-29-13 94.395 NG 0.00 0.00 0.00 0.00 NG
09-10-13 94.395 NG 0.00 0.00 0.00 0.00 NG
11-6-13 94.395 NG 0.00 0.00 0.00 0.00 NG
03-19-14 94.395 NG 0.00 0.00 0.00 0.00 NG
06-26-14 94.395 NG 0.00 0.00 0.00 0.00 NG
08-22-14 94.395 NG 0.00 0.00 0.00 0.00 NG
11-7-14 94.395 NG 0.00 0.00 0.00 0.00 NG
03-4-15 94.395 NG 0.00 0.00 0.00 0.00 NG
MW-15/03-18-09 93.775 13.77 0.00 0.00 0.00 13.77 80.01
MW-15A 06-23-09 93.775 9.90 0.00 0.00 0.00 9.90 83.88
09-9-09 93.775 11.57 0.00 0.00 0.00 11.57 82.21
12-3-09 93.775 11.24 0.00 0.00 0.00 11.24 82.54
03-24-10 93.775 7.57 0.00 0.00 0.00 7.57 86.21
06-24-10 93.775 8.43 0.00 0.00 0.00 8.43 85.35
09-8-10 93.775 9.67 0.00 0.00 0.00 9.67 84.11
12-10-10 93.775 11.24 0.00 0.00 0.00 11.24 82.54
03-8-11 93.775 11.42 0.00 0.00 0.00 11.42 82.36
06-30-11 94.950 12.47 0.00 0.00 0.00 12.47 82.48
09-8-11 94.950 13.88 0.00 0.00 0.00 13.88 81.07
12-8-11 94.950 13.75 0.00 0.00 0.00 13.75 81.20
03-13-12 94.950 13.49 0.00 0.00 0.00 12.60 82.35
06-5-12 94.950 12.45 0.00 0.00 0.00 12.45 82.50
09-11-12 94.950 13.51 0.00 0.00 0.00 13.51 81.44
12-12-12 94.950 14.08 0.00 0.00 0.00 14.08 80.87
03-12-13 94.950 12.07 0.00 0.00 0.00 12.07 82.88
05-29-13 94.950 8.72 0.00 0.00 0.00 8.72 86.23
09-10-13 94.950 9.17 0.00 0.00 0.00 9.17 85.78
11-6-13 94.950 7.94 0.00 0.00 0.00 7.94 87.01
03-19-14 94.950 8.33 0.00 0.00 0.00 8.33 86.62
06-26-14 94.950 7.78 0.00 0.00 0.00 7.78 87.17
08-22-14 94.950 9.14 0.00 0.00 0.00 9.14 85.81
11-7-14 94.950 11.24 0.00 0.00 0.00 11.24 83.71
03-4-15 94.950 11.40 0.00 0.00 0.00 11.40 83.55
*MW-5 depth inaccurate for this event as groundwater was seeping in at time of measurement.
Page 4 of 4
PARAMETE UNITS DATE MW-1/ MW-3 MW-4 MW-5 MW-6* MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/ TS-1 NCAC 2L
MW-1A MW-15A Groundwater
Standard
Benzene ug/l 03-14-07 440 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 DNE DNE DNE NS 1
06-06-07 410 <1 <1 <1 3.6 <1 <1 <1 <1 <1 2.4 DNE DNE DNE NS
08-29-07 340 <1 <1 <1 2.6 <1 <1 <1 <1 <1 6.4 DNE DNE DNE NS
12-13-07 200 <1 <1 <1 1.1 <1 <1 <1 <1 <1 9.2 DNE DNE DNE NS
03-14-08 250 <1 <1 <1 24 <1 <1 <1 <1 <1 130 DNE DNE DNE NS
06-18-08 310 <1 <1 <1 NS <1 <1 <1 <1 <1 5.3 DNE DNE DNE NS
09-10-08 <100 <1 <1 <1 11.6 <1 <1 <1 <1 <1 69.5 DNE DNE DNE NS
12-03-08 18 <0.5 <0.5 <0.5 8.7 32 <0.5 <0.5 <0.5 <0.5 41 DNE DNE DNE NS
03-18-09 110 <0.5 1.9 <0.5 <0.5 5.9 <0.5 <0.5 <0.5 <0.5 3.6 <0.5 NS 520 NS
06-23-09 290 <0.5 <0.5 <0.5 <0.5 0.66 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 210 NS
09-09-09 190 <0.5 <0.5 <0.5 <0.5 0.66 NS <0.5 <0.5 NS 5.1 <0.5 NS 910 NS
12-03-09 180 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 7.5 <0.5 NS 440 NS
03-24-10 120 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 55 NS
06-24-10 30 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 98 NS
09-08-10 69.7 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1.1 <0.5 NS 37.5 NS
12-10-10 140 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1.3 <0.5 NS 5.4 NS
03-08-11 120 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 52 NS
06-30-11 18.3 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 77.1 NS
09-08-11 22 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 1.7 <0.5 NS 462 NS
12-09-11 15.4 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 0.61 <0.5 NS 384 NS
03-14-12 20 ND ND ND ND ND NS ND ND ND 0.17J ND NS 290 NS
06-07-12 28 ND ND ND ND ND ND NS ND ND ND ND NS 220 NS
9/11-12/12 30.1 ND ND ND ND ND ND NS ND ND 1.2 ND NS 132 NS
12-12-12 19 ND ND ND ND ND ND NS ND ND 0.81 ND NS 91 NS
03-14-13 20.4 ND ND ND ND NS NS NS ND ND ND ND NS 82.8 NS
05-30-13 0.83 ND ND ND ND NS NS ND ND ND ND ND NS ND NS
09-10-13 5.5 ND ND ND ND ND NS ND ND ND ND ND NS 4.4 NS
11-07-13 0.5 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-20-14 0.49 ND ND ND ND ND NS ND ND ND ND ND NS 0.29 NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 0.15 ND ND ND 0.15 ND NS ND ND ND ND ND NS ND NS
03-04-15 ND ND ND ND ND ND NS ND ND ND ND ND NS 1.1 NS
Toluen ug/l 03-14-07 3200 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 600
06-06-07 5200 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
08-29-07 6300 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
12-13-07 3300 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-14-08 4400 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
06-18-08 5800 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
09-10-08 1850 <1 <1 <1 <1 <1 2.72 <1 <1 <1 <10 DNE DNE DNE NS
12-03-08 28 <1 <1 <1 <1 140 5.3 <1 <1 <1 <1 DNE DNE DNE NS
03-18-09 3200 <1 <1 <1 <1 50 2.9 <1 <1 <1 <1 <0.5 NS 12000 NS
06-23-09 5700 <1 <1 <1 <1 0.69J 2.9 <1 <1 <1 <1 <1 NS 17000 NS
09-09-09 4300 <1 <1 <1 <1 <1 NS <1 <1 NS <1 <1 NS 25000 NS
12-03-09 3900 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS 30000 NS
03-24-10 3100 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 1600 NS
06-24-10 640 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 6900 NS
09-08-10 1090 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 1630 NS
12-10-10 3100 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 94 NS
03-08-11 1390 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 1940 NS
06-30-11 29.6 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 600 NS
09-08-11 2.1 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 5620 NS
12-09-11 5.9 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 <0.5 <0.5 NS 6820 NS
03-14-12 5.7 ND ND ND ND ND NS ND ND ND ND ND NS 7400 NS
06-07-12 8.2 ND ND ND ND ND ND NS ND ND ND ND NS 6300 NS
9/11-12/12 8.1 ND ND ND ND ND ND NS ND ND ND ND NS 3240 NS
12-12-12 3.3 ND ND ND ND ND ND NS ND ND ND ND NS 3300 NS
03-14-13 5.4 ND ND ND ND NS NS NS ND ND ND ND NS 1860 NS
05-30-13 ND ND ND ND ND NS NS ND ND ND ND ND NS 1.8 NS
09-10-13 7.2 ND ND ND ND ND NS ND ND ND ND ND NS 66.2 NS
11-07-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-20-14 0.31 ND ND ND ND ND NS ND ND ND ND ND NS 3 NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 0.12 0.11 ND ND ND ND NS ND ND ND ND ND NS 0.22 NS
03-04-15 ND ND ND ND ND ND NS ND ND ND ND ND NS 58 NS
Ethylbenzene ug/l 03-14-07 66 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 600
06-06-07 550 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
08-29-07 760 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
12-13-07 620 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-14-08 580 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
06-18-08 730 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
09-10-08 228 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 DNE DNE DNE NS
12-03-08 21 <1 <1 <1 <1 11 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-18-09 280 <1 <1 <1 <1 16 <1 <1 <1 <1 <1 6.3 NS 930 NS
06-23-09 870 <1 <1 <1 <1 2.5 <1 <1 <1 <1 <1 <1 NS 3000 NS
09-09-09 830 <1 <1 <1 <1 2.1 NS <1 <1 NS <1 <1 NS 2300 NS
12-03-09 990 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS 2700 NS
03-24-10 720 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 160 NS
06-24-10 250 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 1300 NS
09-08-10 625 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 215 NS
12-10-10 700 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 5.1 NS
03-08-11 307 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 198 NS
06-30-11 19.7 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 140 NS
09-08-11 41.9 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 1550 NS
12-09-11 11.8 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 <0.5 <0.5 NS 1740 NS
03-14-12 11 ND ND ND ND ND NS ND ND ND ND ND NS 2200 NS
06-07-12 15 ND ND ND ND ND ND NS ND ND ND ND NS 1900 NS
9/11-12/12 22.5 ND ND ND ND ND ND NS ND ND ND ND NS 1620 NS
12-12-12 21 ND ND ND ND ND ND NS ND ND ND ND NS 1600 NS
03-14-13 13.8 ND ND ND ND NS NS NS ND ND ND ND NS 1440 NS
05-30-13 0.58 ND ND ND ND NS NS ND ND ND ND ND NS 1.7 NS
09-10-13 7.3 ND ND ND ND ND NS ND ND ND ND ND NS 76.8 NS
11-07-13 1.6 ND ND ND ND ND NS ND ND ND ND ND NS 0.88 NS
03-20-14 1.1 ND ND ND ND ND NS ND ND ND ND ND NS 8 NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 0.16 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 ND ND ND ND ND ND NS ND ND ND ND ND NS 0.32 NS
03-04-15 ND ND ND ND ND ND NS ND ND ND ND ND NS 120 NS
TABLE 3
Monitoring Well Analytical Result
Incident #1291
Harold Smith Grocer
Union Ridge Road, Burlington, North Carolin
1 of 4
PARAMETE UNITS DATE MW-1/ MW-3 MW-4 MW-5 MW-6* MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/ TS-1 NCAC 2L
MW-1A MW-15A Groundwater
Standard
TABLE 3
Monitoring Well Analytical Result
Incident #1291
Harold Smith Grocer
Union Ridge Road, Burlington, North Carolin
Total Xylene ug/l 03-14-07 5700 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 DNE DNE DNE NS 500.0
06-06-07 7000 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 DNE DNE DNE NS
08-29-07 9600 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 DNE DNE DNE NS
12-13-07 5600 <3 <3 <3 <3 <3 <3 <3 <3 <3 27 DNE DNE DNE NS
03-14-08 6200 <3 <3 <3 <3 <3 <3 <3 <3 <3 16 DNE DNE DNE NS
06-18-08 7800 <3 <3 <3 NS <3 <3 <3 <3 <3 12 DNE DNE DNE NS
09-10-08 2377 <4 <4 <4 <4 <4 <4 <4 <4 <4 <40 DNE DNE DNE NS
12-03-08 610 <3 <3 <3 <3 1810 <3 <3 <3 <3 15 DNE DNE DNE NS
03-18-09 5500 <3 <3 <3 <3 2020 <3 13.6 <3 <3 4.7 2.3 NS 7000 NS
06-23-09 9300 <3 <3 <3 <3 71 <3 <3 <3 <3 <3 <3 NS 22400 NS
09-09-09 8700 <3 <3 <3 <3 30.1 NS <3 <3 NS 3.4 <3 NS 19300 NS
12-03-09 9300 <3 <3 <3 <3 <3 <3 <3 <3 NS 5.8 <3 NS 21200 NS
03-24-10 7800 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 NS 2600 NS
06-24-10 2700 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 NS 11100 NS
09-08-10 5720 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 NS 3790 NS
12-10-10 9700 NS NS <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 0.61 <1.5 NS 162 NS
03-08-11 5700 <1.5 <1.5 <1.5 <1.5 0.66 <1.5 <1.5 <1.5 <1.5 0.82 <1.5 NS 2124 NS
06-30-11 213.2 <1.5 <1.5 <1.5 <1.5 0.66 NS NS <1.5 <1.5 5.8 <1.5 NS 602 NS
09-08-11 42.4 <1.5 <1.5 <1.5 <1.5 0.66 NS NS <1.5 <1.5 11.6 <1.5 NS 3990 NS
12-09-11 48 <1.5 <1.5 <1.5 <1.5 <1.5 NS <1.5 <1.5 <1.5 0.66 <1.5 NS 5680 NS
03-14-12 44 ND ND ND ND ND NS ND ND ND ND ND NS 8300 NS
06-07-12 60 ND ND ND ND ND ND NS ND ND ND ND NS 7400 NS
9/11-12/12 73.9 ND ND ND ND ND ND NS ND ND ND ND NS 5940 NS
12-12-12 28 ND ND ND ND ND ND NS ND ND ND ND NS 7400 NS
03-14-13 44 ND ND ND ND NS NS NS ND ND ND ND NS 5600 NS
05-30-13 1.94 ND ND ND ND NS NS ND ND ND ND ND NS 7.7 NS
09-10-13 83.1 ND ND ND ND ND NS ND ND ND ND ND NS 470 NS
11-07-13 4.5 ND ND ND ND ND NS ND ND ND ND ND NS 3.76 NS
03-20-14 5.6 ND ND ND ND ND NS ND ND ND ND ND NS 32.2 NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 1.13 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 0.27 0.23 ND 0.19 0.22 0.19 NS ND ND ND ND ND NS 1.37 NS
03-04-15 3.2 ND ND ND ND ND NS ND ND ND ND ND NS 570 NS
TOTAL BTE ug/l 03-14-07 9406 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL DNE DNE DNE NS N/
06-06-07 13160 BDL BDL BDL 3.6 BDL BDL BDL BDL BDL 2.4 DNE DNE DNE NS
08-29-07 17000 BDL BDL BDL 2.6 BDL BDL BDL BDL BDL 6.4 DNE DNE DNE NS
12-13-07 9720 BDL BDL BDL BDL BDL BDL BDL BDL BDL 36.2 DNE DNE DNE NS
03-14-08 11430 BDL BDL BDL 24 BDL BDL BDL BDL BDL 146 DNE DNE DNE NS
06-18-08 14640 BDL BDL BDL NS BDL BDL BDL BDL BDL 17.3 DNE DNE DNE NS
09-10-08 4455 BDL BDL BDL 11.6 BDL 2.72 BDL BDL BDL 69.5 DNE DNE DNE NS
12-03-08 677 BDL BDL BDL 8.7 1993 5.3 BDL BDL BDL 56 DNE DNE DNE NS
03-18-09 9090 BDL 1.9 BDL BDL 2091.9 2.9 13.6 BDL BDL 8.3 8.6 NS 20450 NS
06-23-09 16160 BDL BDL BDL BDL 74.16 2.9 BDL BDL BDL BDL BDL NS 42610 NS
09-09-09 14020 BDL BDL BDL BDL 32.86 NS BDL BDL NS 8.5 BDL NS 47510 NS
12-03-09 14370 BRL BRL BRL BRL BRL BRL BRL BRL NS 13.3 BRL NS 54340 NS
03-24-10 11740 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS 4415 NS
06-24-10 3620 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS 19398 NS
09-08-10 7504.7 BRL BRL BRL BRL BRL BRL BRL BRL BRL 1.1 BRL NS 5672.5 NS
12-10-10 13640 NS NS BRL BRL BRL BRL BRL BRL BRL 1.91 BRL NS 266.5 NS
03-08-11 7517 ND ND ND ND 0.66 ND ND ND ND 0.82 ND NS 4314 NS
06-30-11 280.8 ND ND ND ND 0.66 NS NS ND ND 5.8 ND NS 1419.1 NS
09-08-11 108.4 ND ND ND ND 0.66 NS NS ND ND 13.3 ND NS 11622 NS
12-09-11 81.1 ND ND ND ND ND NS ND ND ND 1.27 ND NS 14624 NS
03-14-12 80.7 ND ND ND ND ND NS ND ND ND ND ND NS 18190 NS
06-07-12 111.2 ND ND ND ND ND ND NS ND ND ND ND NS 15820 NS
9/11-12/12 134.6 ND ND ND ND ND ND NS ND ND 1.2 ND NS 10932 NS
12-12-12 71.3 ND ND ND ND 0.2 ND NS ND ND 0.81 ND NS 12391 NS
03-14-13 83.6 ND ND ND ND NS NS NS ND ND ND ND NS 8982.8 NS
05-30-13 3.35 ND ND ND ND NS NS ND ND ND ND ND NS 11.2 NS
09-10-13 103.1 ND ND ND ND ND NS ND ND ND ND ND NS 617.4 NS
11-07-13 6.6 ND ND ND ND ND NS ND ND ND ND ND NS 4.64 NS
03-20-14 7.19 ND ND ND ND ND NS ND ND ND ND ND NS 40.49 NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 1.29 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 0.54 0.34 ND 0.19 0.37 0.19 NS ND ND ND ND ND NS 1.91 NS
03-04-15 3.2 ND ND ND ND ND NS ND ND ND ND ND NS 749.1 NS
Methyl Tertiary ug/l 03-14-07 <50 <5 10 <5 4.3J <5 <5 <5 <5 <5 2.7J DNE DNE DNE NS 20.0
Butyl Ether 06-06-07 <50 19 7.5 <5 5.9 <5 4.9J <5 <5 <5 4.1J DNE DNE DNE NS
(MTBE)08-29-07 <50 73 4.6J <5 7.1 <5 <5 <5 <5 <5 4.1J DNE DNE DNE NS
12-13-07 <50 97 20 <5 8.5 <5 <5 <5 <5 <5 13 DNE DNE DNE NS
03-14-08 <50 10 6.9 <5 16 <5 <5 <5 <5 <5 74 DNE DNE DNE NS
06-18-08 <50 26 27 <5 NS <5 <5 <5 <5 <5 15 DNE DNE DNE NS
09-10-08 <200 2.3 <2 <2 6.39 <2 <2 <2 <2 <2 38.1 DNE DNE DNE NS
12-03-08 <5 2.8J 8.9 <5 9.3 5.1 <5 <5 <5 <5 75 DNE DNE DNE NS
03-18-09 <50 <5 <5 <5 <5 8.2 <5 8.3 <5 <5 25 <0.5 NS <50 NS
06-23-09 <50 <5 5.4 <5 <5 3.3J <5 <5 <5 <5 11 <5 NS <50 NS
09-09-09 <50 <5 7.7 <5 <5 2.6J NS <5 <5 NS 44 <5 NS <200 NS
12-03-09 <50 <5 4J <5 <5 <5 <5 <5 <5 NS 92 <5 NS <200 NS
03-24-10 <50 <5 13 <5 <5 <5 <5 <5 <5 <5 3.3J <5 NS <200 NS
06-24-10 <50 <1 4.2 <1 <1 1.5 <1 <1 <1 <1 13 <1 NS <40 NS
09-08-10 <2.5 <0.5 1.7 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 45.8 <0.5 NS <5 NS
12-10-10 <10 NS NS <1 <1 <1 <1 <1 <1 <1 57 <1 NS <1 NS
03-08-11 <10 <0.5 1.6 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 19.1 <0.5 NS <10 NS
06-30-11 2.7 <0.5 0.83 <0.5 <0.5 <0.5 NS NS 0.51 <0.5 23.8 <0.5 NS <0.5 NS
09-08-11 12.3 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS 0.54 <0.5 54.7 <0.5 NS 2.9 NS
12-09-11 9.2 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 0.52 <0.5 28.5 <0.5 NS <25 NS
03-14-12 9.6 ND 0.5 ND 0.25J ND NS ND 0.84 ND 10 ND NS ND NS
06-07-12 ND ND ND ND ND ND ND NS 1.7 ND 15 ND NS ND NS
9/11-12/12 21.4 ND ND ND ND ND ND NS 2.2 ND 33.8 ND NS ND NS
12-12-12 21 ND ND ND 0.19J ND ND NS 0.32J ND 24 ND NS ND NS
03-14-13 21.3 ND ND ND ND NS NS NS ND ND 8.4 ND NS ND NS
05-30-13 9.4 ND ND ND ND NS NS ND 0.8 ND 2 ND NS 0.61 NS
09-10-13 14.4 ND ND ND ND ND NS ND 2.9 ND 1.9 ND NS ND NS
11-07-13 9.4 ND ND ND ND ND NS ND 2.2 ND 1.2 ND NS ND NS
03-20-14 8.6 ND 0.35 ND 0.16 ND NS 1.1 0.12 ND 1.8 ND NS 0.2 NS
06-26-14 0.25 ND 0.32 ND 0.53 0.24 NS 0.3 3.2 ND 0.66 ND NS ND NS
08-22-14 4.1 ND ND ND ND ND NS 0.25 1.3 ND 0.57 ND NS ND NS
11-07-14 0.79 ND ND ND ND ND NS 1.4 1.5 ND 0.46 ND NS ND NS
03-04-15 4.6 ND ND ND 0.60J ND NS 1.6 ND ND 0.80J ND NS ND NS
2 of 4
PARAMETE UNITS DATE MW-1/ MW-3 MW-4 MW-5 MW-6* MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/ TS-1 NCAC 2L
MW-1A MW-15A Groundwater
Standard
TABLE 3
Monitoring Well Analytical Result
Incident #1291
Harold Smith Grocer
Union Ridge Road, Burlington, North Carolin
Ethylene ug/l 03-14-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 0.0200
Dibromid 06-06-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
(EDB)08-29-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
12-13-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-14-08 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
06-18-08 <10 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
09-10-08 <2 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 DNE DNE DNE NS
12-03-08 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-18-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <0.5 NS <50 NS
06-23-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS <50 NS
09-09-09 <10 <1 <1 <1 <1 <1 NS <1 <1 NS <1 <1 NS <40 NS
12-03-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS <40 NS
03-24-10 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS <40 NS
06-24-10 14 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 28 NS
09-08-10 <2.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS <5 NS
12-10-10 <5 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 3.9 NS
03-08-11 <10 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS <10 NS
06-30-11 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 1.9 NS
09-08-11 <1.2 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 7 NS
12-09-11 <1 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 <0.5 <0.5 NS <25 NS
03-14-12 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
06-07-12 ND ND ND ND ND ND ND NS ND ND ND ND NS ND NS
9/11-12/12 ND ND ND ND ND ND ND NS ND ND ND ND NS ND NS
12-12-12 ND ND ND ND ND ND ND NS ND ND ND ND NS ND NS
03-14-13 ND ND ND ND ND NS NS NS ND ND ND ND NS ND NS
05-30-13 ND ND ND ND ND NS NS ND ND ND ND ND NS ND NS
09-10-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-20-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-04-15 NA NA NA NA NA NA NS NA NA NA NA NA NS NA NS
Isopropyl Ethe ug/l 03-14-08 86 <5 3J <5 9.9 <5 <5 <5 <5 <5 270 DNE DNE DNE NS 70.0
(IPE)06-18-08 <50 <5 13 <5 NS <5 <5 <5 <5 <5 19 DNE DNE DNE NS
09-10-08 <100 <1 <1 <1 9.28 <1 <1 <1 <1 <1 221 DNE DNE DNE NS
12-03-08 15 <5 4.6J <5 6.9 23 <5 8.1 <5 <5 200 DNE DNE DNE NS
03-18-09 <50 <5 <5 <5 <5 19 <5 10 <5 <5 69 <0.5 NS <50 NS
06-23-09 <50 <5 <5 <5 <5 6.2 <5 <5 <5 <5 10 <5 NS <50 NS
09-09-09 <50 <5 3.3J <5 <5 4.9J NS <5 <5 NS 73 <5 NS <200 NS
12-03-09 <50 <5 <5 <5 <5 <5 <5 <5 <5 NS 180 <5 NS <200 NS
03-24-10 <50 <5 5.9 <5 <5 <5 <5 <5 <5 <5 3.2J <5 NS <200 NS
06-24-10 <5 <0.5 1.8 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 12 <0.5 NS <20 NS
09-08-10 2.9 <0.5 0.66 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 35.9 <0.5 NS <5 NS
12-10-10 6 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 49 <0.5 NS 1.3 NS
03-08-11 <10 <0.5 <0.5 <0.5 <0.5 0.56 <0.5 <0.5 0.82 <0.5 24.6 <0.5 NS <10 NS
06-30-11 13 <0.5 <0.5 <0.5 <0.5 0.56 NS NS 1.2 <0.5 29.2 <0.5 NS 2.7 NS
09-08-11 62.2 <0.5 <0.5 <0.5 <0.5 0.56 NS NS 0.73 <0.5 55.2 <0.5 NS 22.5 NS
12-09-11 40.9 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 29.1 <0.5 NS <25 NS
03-14-12 47 ND ND ND ND ND NS ND 0.17J ND 11 ND NS ND NS
06-07-12 78 ND ND ND ND ND ND NS 0.52J ND 12 ND NS 15J NS
9/11-12/12 94.8 ND ND ND ND ND ND NS 1.6 ND 29.8 ND NS 13.5 NS
12-12-12 120 ND ND ND 0.16J ND ND NS 1.6 ND 26 ND NS ND NS
03-14-13 112 ND ND ND ND NS NS NS ND ND 10.2 ND NS ND NS
05-30-13 32.5 ND ND ND ND NS NS 3.1 1.5 ND ND ND NS 1.5 NS
09-10-13 80.7 ND ND ND ND ND NS 3.1 6.9 ND ND ND NS 7.2 NS
11-07-13 42.2 ND ND ND ND ND NS ND 3.1 1.9 ND ND NS 0.79 NS
03-20-14 46 ND ND ND 0.2 ND NS ND 3.1 1.9 0.34 ND NS 1.5 NS
06-26-14 ND ND ND ND 1.4 ND NS ND 3.3 3.1 ND ND NS ND NS
08-22-14 11 ND ND ND 0.24 ND NS ND 2.1 3.1 ND ND NS ND NS
11-07-14 2 ND ND ND ND ND NS ND 1.1 ND ND ND NS ND NS
03-04-15 27 ND ND ND ND ND NS ND ND ND 0.5 ND NS ND NS
1,2-Dichloroethane ug/l 03-14-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 0.4
06-06-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
08-29-07 <10 <1 <1 <1 <1 <1 <1 <1 1.4 <1 1.3 DNE DNE DNE NS
12-13-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 1.5 DNE DNE DNE NS
03-14-08 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 31 DNE DNE DNE NS
06-18-08 <10 <1 1.3 <1 NS <1 <1 <1 <1 <1 2.8 DNE DNE DNE NS
09-10-08 <2 <1 <1 <1 <1 <1 <1 <1 <1 <1 29.3 DNE DNE DNE NS
12-03-08 <1 <1 <1 <1 <1 4 <1 0.76J <1 <1 30 DNE DNE DNE NS
03-18-09 <10 <1 <1 <1 <1 2.1 <1 1.5 <1 <1 4.5 <0.5 NS <50 NS
06-23-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 0.69J <1 NS <50 NS
09-09-09 <10 <1 <1 <1 <1 0.64J NS <1 <1 NS 8.6 <1 NS <40 NS
12-03-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 NS 13 <1 NS <40 NS
03-24-10 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS <40 NS
06-24-10 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 2.8 <0.5 <0.5 NS <20 NS
09-08-10 <2.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 6.9 <0.5 NS <5 NS
12-10-10 <5 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 11 <0.5 NS <0.5 NS
03-08-11 <10 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 7.1 <0.5 NS <10 NS
06-30-11 1.1 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 9.1 <0.5 NS 0.58 NS
09-08-11 4.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 10.9 <0.5 NS 4 NS
12-09-11 4.1 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 7.1 <0.5 NS <25 NS
03-14-12 ND ND ND ND ND ND NS ND 0.33J ND 3.6 ND NS ND NS
06-07-12 ND ND ND ND ND ND ND NS ND ND 4 ND NS ND NS
9/11-12/12 13.7 ND ND ND ND ND ND NS 0.67 ND 5.9 ND NS ND NS
12-12-12 15 ND ND ND ND ND ND NS ND ND 0.81 ND NS 4.9 NS
03-14-13 14.2 ND ND ND ND NS NS NS 0.72 ND 3.3 ND NS ND NS
05-30-13 4.2 ND ND ND ND NS NS ND 1.1 ND 0.53 ND NS ND NS
09-10-13 9.2 ND ND ND ND ND NS ND 2.4 ND 0.51 ND NS 0.6 NS
11-07-13 4.1 ND ND ND ND ND NS ND 2.2 ND ND ND NS ND NS
03-20-14 4.8 ND ND ND 0.23 ND NS ND 3.2 ND ND ND NS ND NS
06-26-14 ND ND ND ND 0.32 ND NS ND 1.4 0.63 ND ND NS ND NS
08-22-14 2 ND ND ND ND ND NS ND 1.2 0.84 ND ND NS ND NS
11-07-14 ND ND ND ND ND ND NS ND 0.69 ND ND ND NS ND NS
03-04-15 2.7 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
3 of 4
PARAMETE UNITS DATE MW-1/ MW-3 MW-4 MW-5 MW-6* MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/ TS-1 NCAC 2L
MW-1A MW-15A Groundwater
Standard
TABLE 3
Monitoring Well Analytical Result
Incident #1291
Harold Smith Grocer
Union Ridge Road, Burlington, North Carolin
Naphthalene ug/l 03-14-08 470 <1 <1 <1 <1 <1 <1 <1 <1 <1 4.5 DNE DNE DNE NS 6
06-18-08 590 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
09-10-08 136 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 DNE DNE DNE NS
12-03-08 31 <1 <1 <1 <1 <1 <1 <1 <1 <1 3.5 DNE DNE DNE NS
03-18-09 250 <1 1.9 <1 <1 <1 <1 1.6 <1 <1 <1 6.2 NS 490 NS
06-23-09 470 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 950 NS
09-09-09 540 <1 <1 <1 <1 <1 NS <1 <1 NS <1 <1 NS 680 NS
12-03-09 490 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS 750 NS
03-24-10 550 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 220 NS
06-24-10 680 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 580 NS
09-08-10 736 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 NS 255 NS
12-10-10 520 NS NS <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 7.1 NS
03-08-11 337 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 NS 118 NS
06-30-11 54.1 <2 <2 <2 <2 <2 NS NS <2 <2 3 <2 NS 41.6 NS
09-08-11 154 <2 <2 <2 <2 <2 NS NS <2 <2 5.9 <2 NS 395 NS
12-09-11 112 <2 <2 <2 <2 <2 NS <2 <2 <2 <2 <2 NS 504 NS
03-14-12 87 ND ND ND ND ND NS ND ND ND ND ND NS 130J NS
06-07-12 84 ND ND ND ND ND ND NS ND ND ND ND NS 150 NS
9/11-12/12 197 ND ND ND ND ND ND NS ND ND ND ND NS 515 NS
12-12-12 99 ND ND ND ND ND ND NS ND ND ND ND NS 250 NS
03-14-13 84.6 ND ND ND ND NS NS NS ND ND ND ND NS 344 NS
05-30-13 3.4 ND ND ND ND NS NS ND ND ND ND ND NS ND NS
09-10-13 18 ND ND ND ND ND NS ND ND ND ND ND NS 2.3 NS
11-07-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-20-14 2.5 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
06-26-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
08-22-14 0.66 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
03-04-15 0.73J ND ND ND ND ND NS ND ND ND ND ND NS 33 NS
NA=Not Analyzed for Parameter DNE=Did Not Exist Bold Values exceed the NCAC 2L Groundwater StandardNS=Not Sampled BDL=Below Detection Limits ND=Not Detected
4 of 4
PARAMETER UNITS DATE NCAC 15A:2L
2768B 2774 2760 2773 2755 2761 2779 2765 2765 2765 2800 Groundwater
Influent Midfluent Effluent Standard
Benzene ug/l 03-24-10 <0.5 NS NS NS NS NS NS 1.7 <0.5 <0.5 NS
06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
09-08-10 NS NS NS <0.5 NS NS NS 1 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS 0.97 <0.5 <0.5 NS 1
03-08-11 NS NS NS <0.5 NS NS <0.5 1.6 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 8.4 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 7.1 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 3.3 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND ND NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS
09-20-14 ND NS NS ND NS NS ND ND ND ND NS
06-26-14 ND NS ND ND NS NS ND 0.33 ND ND NS
08-22-14 ND NS ND ND NS NS ND 0.54 ND ND NS
11-07-14 ND NS ND ND NS NS ND ND ND ND NS
03-04-15 NS NS ND ND NS NS ND ND ND ND NS
Toluene ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS
06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 600
03-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND ND NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS
03-20-14 ND NS NS ND NS NS ND ND ND ND NS
06-26-14 ND NS ND ND NS NS ND ND ND ND NS
08-22-14 ND NS ND ND NS NS ND ND ND ND NS
11-07-14 ND NS ND ND NS NS ND ND ND ND NS
03-04-15 NS NS ND ND NS NS ND ND ND ND NS
Ethylbenzene ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS
06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 600
03-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND 0.55 NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS
03-20-14 ND ND ND ND NS NS ND ND ND ND NS
06-26-14 ND NS ND ND NS NS ND ND ND ND NS
08-22-14 ND NS ND ND NS NS ND 0.26 ND ND NS
11-07-14 ND NS ND ND NS NS ND ND ND ND NS
03-04-15 NS NS ND ND NS NS ND ND ND ND NS
Total Xylenes ug/l 03-24-10 <3 NS NS NS NS NS NS <3 <3 <3 NS
06-24-10 NS NS NS <1.5 NS NS NS <1.5 <1.5 <1.5 NS
09-08-10 NS NS NS <1.5 NS NS NS <1.5 <1.5 <1.5 NS
12-10-10 NS NS NS <1.5 NS NS NS <1.5 <1.5 <1.5 NS 500
03-08-11 NS NS NS <1.5 NS NS <1.5 <1.5 <1.5 <1.5 NS
06-30-11 NS NS NS <1.5 NS NS <1.5 <3 <1.5 <1.5 NS
09-08-11 NS NS NS <1.5 NS NS <1.5 <3 <1.5 <1.5 NS
12-09-11 NS NS NS <1.5 NS NS <1.5 <3 <1.5 <1.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND ND NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS
03-20-14 ND ND ND ND NS NS ND ND ND ND NS
06-26-14 ND NS ND ND NS NS ND ND ND ND NS
08-22-14 ND NS ND ND NS NS ND ND ND ND NS
11-07-14 ND NS ND ND NS NS ND ND ND ND NS
03-04-15 NS NS ND ND NS NS ND ND ND ND NS
TOTAL BTEX ug/l 03-24-10 BDL NS NS NS NS NS NS 1.7 BDL BDL NS
06-24-10 NS NS NS BDL NS NS NS BDL BDL BDL NS
09-08-10 NS NS NS BDL NS NS NS 1 BDL BDL NS
12-10-10 NS NS NS BDL NS NS NS 0.97 <0.5 <0.5 NS N/A
03-08-11 NS NS NS BDL NS NS BDL 1.6 BDL BDL NS
06-30-11 NS NS NS BDL NS NS BDL 8.4 BDL BDL NS
09-08-11 NS NS NS BDL NS NS BDL 7.1 BDL BDL NS
12-09-11 NS NS NS BDL NS NS BDL 3.3 BDL BDL NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND 0.55 NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS
03-20-14 ND ND ND ND NS NS ND ND ND ND NS
06-26-14 ND NS ND ND NS NS ND 0.33 ND ND NS
08-22-14 ND NS ND ND NS NS ND 0.8 ND ND NS
11-07-14 ND NS ND ND NS NS ND ND ND ND NS
03-04-15 NS NS ND ND NS NS ND ND ND ND NS
Methyl Tertiary ug/l 03-24-10 22 NS NS NS NS NS NS 98 <5 <5 NS
Butyl Ether 06-24-10 NS NS NS <1 NS NS NS <1 <1 <1 NS
(MTBE)09-08-10 NS NS NS <1 NS NS NS 84.8 <1 <1 NS
12-10-10 NS NS NS <1 NS NS NS 100 <1 <1 NS 20
03-08-11 NS NS NS <0.5 NS NS <0.5 166 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 125 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 136 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 150 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND 149 NS ND NS
12-12-12 NS NS NS ND NS NS ND 140 NS ND NS
03-14-13 ND NS NS ND NS NS ND 157 NS ND NS
05-29-13 ND NS NS ND NS NS ND 150 NS ND NS
09-10-13 ND NS NS ND NS NS ND 128 NS ND NS
11-07-13 ND NS NS ND NS NS ND 117 NS ND NS
03-20-14 ND ND ND 0.81 NS NS ND 140 ND 0.62 NS
06-26-14 ND NS ND 0.23 NS NS ND 120 ND ND NS
08-22-14 ND NS ND 0.18 NS NS ND 120 ND 0.28 NS
11-07-14 ND NS ND ND NS NS ND 130 ND ND NS
03-04-15 NS NS ND 0.79J NS NS ND 80 ND ND NS
SUPPLY WELL
Union Ridge Road, Burlington, North Carolina
TABLE 4
Water Supply Well Analytical Results
Harold Smith Grocery
Incident #12913
Page 1 of 2
PARAMETER UNITS DATE NCAC 15A:2L
2768B 2774 2760 2773 2755 2761 2779 2765 2765 2765 2800 Groundwater
Influent Midfluent Effluent Standard
SUPPLY WELL
Union Ridge Road, Burlington, North Carolina
TABLE 4
Water Supply Well Analytical Results
Harold Smith Grocery
Incident #12913
Ethylene ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS
Dibromide 06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
(EDB)09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 0.02
03-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND ND NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS
03-20-14 ND ND ND ND NS NS ND ND ND ND NS
06-26-14 ND NS ND ND NS NS ND ND ND ND NS
08-22-14 ND NS ND ND NS NS ND ND ND ND NS
11-07-14 ND NS ND ND NS NS ND ND ND ND NS
03-04-15 NS NS NA NA NS NS NA NA NA NA NS
Isopropyl Ether ug/l 03-24-10 11 NS NS NS NS NS NS 130 <5 <5 NS
(IPE)06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
09-08-10 NS NS NS <0.5 NS NS NS 104 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS 150 <0.5 <0.5 NS 70
03-08-11 NS NS NS <0.5 NS NS <0.5 260 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 191 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 206 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 178 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND 149 NS ND NS
12-12-12 NS NS NS ND NS NS ND 150 NS ND NS
03-14-13 ND NS NS ND NS NS ND 159 NS ND NS
05-29-13 ND NS NS ND NS NS ND 168 NS ND NS
09-10-13 ND NS NS 0.96 NS NS ND 183 NS ND NS
11-07-13 ND NS NS 1.96 NS NS ND 138 NS ND NS
03-20-14 ND ND ND 0.67 NS NS ND 140 ND 0.2 NS
06-26-14 ND NS ND ND NS NS ND 160 ND ND NS
08-22-14 ND NS ND ND NS NS ND 150 ND ND NS
11-07-14 ND NS ND ND NS NS ND 160 ND ND NS
03-04-15 NS NS ND ND NS NS ND 100 ND ND NS
1,2- Dichloroethane ug/l 03-24-10 <1 NS NS NS NS NS NS 6.2 <1 <1 NS
06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
09-08-10 NS NS NS <0.5 NS NS NS 15.7 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS 19 <0.5 <0.5 NS 0.4
03-08-11 NS NS NS <0.5 NS NS <0.5 33.1 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 28 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 27.4 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 26.6 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND 20.8 NS ND NS
12-12-12 NS NS NS 0.19J NS NS ND 23 NS ND NS
03-14-13 ND NS NS ND NS NS ND 31.5 NS ND NS
05-29-13 ND NS NS ND NS NS ND 25.9 NS ND NS
09-10-13 ND NS NS ND NS NS ND 25.7 NS ND NS
11-07-13 ND NS NS ND NS NS ND 20.1 NS ND NS
03-20-14 ND ND ND 0.44 NS NS ND 20 ND ND NS
06-26-14 ND NS ND 0.31 NS NS ND 24 ND ND NS
08-22-14 ND NS ND ND NS NS ND 24 ND ND NS
11-07-14 ND NS ND ND NS NS ND 27 ND ND NS
03-04-15 NS NS ND ND NS NS ND 16 ND ND NS
1,2-Dichloropropane ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS
06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 0.6
03-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND ND NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS
03-20-14 ND ND ND ND NS NS ND ND ND ND NS
06-26-14 ND NS ND ND NS NS ND ND ND ND NS
08-22-14 ND NS ND ND NS NS ND ND ND ND NS
11-07-14 ND NS ND ND NS NS ND ND ND ND NS
03-04-15 NS NS ND ND NS NS ND ND ND ND NS
Chloroform 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS
06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
03-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 70
06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND ND NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS
03-20-14 ND ND ND ND NS NS ND ND ND ND NS
06-26-14 ND NS ND ND NS NS ND 1.1 ND ND NS
08-22-14 ND NS ND ND NS NS ND ND ND 1.6 NS
11-07-14 ND NS ND ND NS NS ND ND ND ND NS
03-04-15 NS NS ND ND NS NS ND ND ND ND NS
*Samples 2765 influent & effluent were sampled on 9/25/01 NA=Not analyzed for this parameter J=Estimated Value NS=Not Sampled
Page 2 of 2
TABLE 5 System Operation Parameters
Harold Smith Grocery
Incident #12913
Union Ridge Road, Burlington, North Carolina
DATE:
SVE TEMP. (°F)
SVE FLOW (SCFM)
SVE VACUUM (IN.-H2O)
SPARGE TEMP. (°F)
SPARGE PRESSURE (PSI)
1/6/09 65 120 9 180 15
2/4/09 55 115 9 175 12
3/16/09 55 115 8 170 10
4/2/09 75 115 7 180 10
5/6/09 78 115 8 184 10
6/5/09 70 115 6 175 10
7/6/09 80 115 8 NR 10
8/10/09 78 115 8 NR 10
9/8/09 76 115 8 NR 9
10/5/09 72 115 7 NR 7
11/2/09 70 115 6 NR 5
12/13/09 58 115 7 NR 5
1/6/10 36 115 8 NR 3
2/18/10 42 115 8 NR 12
3/5/10 56 115 7 NR 12
3/31/10 50 115 8 NR 12
5/24/10 70 115 8 NR 14
6/25/10 75 110 7 NR 14
7/27/10 75 110 6 NR 12
8/6/10 90 110 6 NR 12
9/2/10 90 110 6 NR 11
10/1/10 85 115 6 NR 10
11/10/10 50 115 6 NR 12
12/7/10 45 115 6 NR 12
1/6/11 40 110 6 NR 12
2/3/11 45 110 6 NR 12
3/15/11 55 110 6 NR 12
SYSTEM OFF – SOIL EXCAVATION
1/6/12 OFF OFF OFF NR 10
2/10/12 OFF OFF OFF NR 10
3/19/12 OFF OFF OFF NR 10
4/4/12 OFF OFF OFF NR 10
5/3/12 OFF OFF OFF NR 10
6/1/12 OFF OFF OFF NR 9
7/3/12 OFF OFF OFF NR 9
8/3/12 OFF OFF OFF NR 9
9/21/12 OFF OFF OFF NR OFF
10/3/12 OFF OFF OFF NR OFF
11/19/12 OFF OFF OFF NR OFF
12/14/12 OFF OFF OFF NR OFF
1/28/13 OFF OFF OFF NR OFF
2/25/13 OFF OFF OFF NR OFF
3/19/13 OFF OFF OFF NR OFF
TABLE 5 System Operation Parameters
Harold Smith Grocery
Incident #12913
Union Ridge Road, Burlington, North Carolina
DATE:
SVE TEMP. (°F)
SVE FLOW (SCFM)
SVE VACUUM (IN.-H2O)
SPARGE TEMP. (°F)
SPARGE PRESSURE (PSI)
5/30/13 OFF OFF OFF NR OFF
6/19/13 OFF OFF OFF NR OFF
7/9/13 OFF OFF OFF NR OFF
8/9/13 OFF OFF OFF NR OFF
9/15/3 OFF OFF OFF NR OFF
10/22/13 OFF OFF OFF NR OFF
11/5/13 OFF OFF OFF NR OFF
12/12/13 40 110 5 NR 8
1/10/14 50 110 5 NR 8
2/4/14 40 110 5 NR 8
3/1/14 42 110 5 NR 8
3/25/14 50 110 5 NR 8
5/29/14 80 110 5 NR 8
6/9/14 75 110 5 NR 7
6/30/14 90 110 5 NR 8
8/5/14 80 110 5 NR 8
9/3/14 85 110 5 NR 8
9/26/14 70 110 5 NR 8
11/12/14 50 110 5 NR 8
12/12/14 45 110 5 NR 8
1/21/15 50 110 5 NR 8
1/30/15 50 110 5 NR 8
3/11/15 60 110 5 NR 8

* Individual pressure (in psi) and flow (in scfm) at each sparge well. NR = not recorded.
TABLE 5 System Operation Parameters
Harold Smith Grocery
Incident #12913
Union Ridge Road, Burlington, North Carolina
DATE: AS-1 PRES./
FLOW*
AS-2 PRES./
FLOW*
AS-3 PRES./
FLOW*
AS-4 PRES./
FLOW*
AS-5 PRES./
FLOW*
AS-6 PRES./
FLOW*
AS-7 PRES./
FLOW*
AS-8 PRES./
FLOW*
7/6/09 8/.05 8/.05 8/.05 8/.05 8/.05 8/0.5 8/0 8/0.5
8/10/09 8/.05 8/.05 8/.05 8/.05 8/.05 8/0.5 8/0 8/0.5
9/8/09 7/.05 7/.05 7/.05 7/.05 7/.05 7/.05 7/0 7/.05
10/5/09 5/0.5 5/0.5 5/0.5 5/0.5 5/0.5 5/0 5/.05
11/2/09 4/0.5 4/0.5 4/0.5 4/0.5 4/0.5 4/0.5 4/0 4/0.5
12/13/09 4/0.5 4/0.5 4/0.5 4/0 4/0.5 4/0.5 4/0 4/0.5
1/6/10 3/0.5 3/0.5 3/0 3/0 3/0.5 3/0.5 3/0 3/0
2/18/10 11/3 11/3 11/3 11/3 11/3 11/2 11/0 11/3
3/5/10 11/3 11/2 11/3 11/2 11/3 11/3 11/0 11/3
3/31/10 11/3 11/3 11/3 11/3 11/3 11/3 11/0 11/3
5/24/10 13/4 13/3 13/4 13/4 13/3 13/3 13/0 13/3
6/25/10 13/3 13/3 13/3 13/3 13/3 12/0 13/0 12/3
7/27/10 11/3 11/3 11/3 11/3 11/3 11/3 11/0 11/3
8/6/10 11/3 11/3 10/3 10/3 11/3 11/3 11/0 11/3
9/2/10 10/3 10/2 10/3 10/2 10/2 10/3 10/0 10/2
10/1/10 10/3 10/2 10/2 10/2 10/2 10/2 10/0 10/2
11/10/10 11/3 11/3 11/3 11/2 11/3 11/3 11/0 11/2
12/2/10 11/3 11/3 11/2 11/3 11/3 11/3 11/0 11/2
1/6/11 11/3 11/3 11/2 11/2 11/3 11/2 11/0 11/2
2/3/11 11/3 11/2 11/3 11/2 11/3 11/2 11/0 11/2
3/15/11 11/2 11/3 11/2 11/2 11/3 11/2 11/0 11/2
SYSTEM OFF AFTER SOIL EXCAVATION
1/6/12 8/1 8/0 OFF OFF 8/0 8/1 OFF OFF
2/10/12 10/1 10/0 OFF OFF 10/1 10/1 OFF OFF
3/19/12 8/1 8/1 OFF OFF 8/0 8/0 OFF OFF
4/4/12 8/1 8/1 OFF OFF 8/0 8/0 OFF OFF
5/3/12 8/1 8/1 OFF OFF 8/1 8/0 OFF OFF
6/1/12 8/1 8/1 OFF OFF 8/0 8/0 OFF OFF
7/3/12 8/1 8/1 OFF OFF 8/1 8/1 OFF OFF
8/3/12 8/1 8/1 OFF OFF 8/1 8/1 OFF OFF
9/21/12 8/1 8/1 OFF OFF 8/1 8/1 OFF OFF
10/3/12 OFF OFF OFF OFF OFF OFF OFF OFF
11/19/12 OFF OFF OFF OFF OFF OFF OFF OFF
12/14/12 OFF OFF OFF OFF OFF OFF OFF OFF
1/28/13 OFF OFF OFF OFF OFF OFF OFF OFF
2/25/13 OFF OFF OFF OFF OFF OFF OFF OFF
3/19/13 OFF OFF OFF OFF OFF OFF OFF OFF
NEW SYSTEM INSTALLED AND OPERATIONAL
5/30/13 1/.5 9/2 9/2 1/.5 9/2 9/2 5/1 -
6/19/13 1/.5 9/2 9/2 1/.5 9/2 9/2 5/1 -
7/9/13 1/.5 9/2 9/2 1/.5 9/2 9/2 5/1 -
8/9/13 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
9/15/3 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
10/22/13 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
11/5/13 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
12/12/13 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
1/10/14 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
2/4/14 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
3/1/14 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
TABLE 5 System Operation Parameters
Harold Smith Grocery
Incident #12913
Union Ridge Road, Burlington, North Carolina
DATE: AS-1 PRES./
FLOW*
AS-2 PRES./
FLOW*
AS-3 PRES./
FLOW*
AS-4 PRES./
FLOW*
AS-5 PRES./
FLOW*
AS-6 PRES./
FLOW*
AS-7 PRES./
FLOW*
AS-8 PRES./
FLOW*
3/25/14 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
5/29/14 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
6/9/14 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
6/30/14 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
8/5/14 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
9/3/14 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
9/26/14 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
11/12/14 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
12/12/14 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
1/21/15 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
1/30/15 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
3/11/15 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -

Individual pressure (in psi) and flow (in scfm) at each sparge well. NR = not recorded.

APPENDIX A

This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
Case Narrative
03/24/2015
Pyramid Environmental, Inc
Brett Higgins
PO Box 16265
Greensboro, NC 27416-0265
Project: Harold Smith
Lab Submittal Date: 03/06/2015
Prism Work Order: 5030124
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
For sample 5030124-05 with client ID of SW-2773, the initial 6200 was analyzed undiluted and showed a
large hit of Trans-1,2-dichloroethene that was outside of calibration range. Dilutions of 1:20 and 1:50 were
analyzed and the Trans-1,2-dichloroethene did not duplicate. Vials were checked for accuracy in labeling
and were correct. The initial run is reported with an "E" flag to show an estimated value.
Narrative Notes:
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services
Reviewed ByAngela D. Overcash Terri W. Cole For Angela D. Overcash
Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 56
Data Qualifiers Key Reference:
E Estimated concentration above the calibration range
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
M Matrix spike outside of the control limits.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 56
Sample Receipt Summary
03/24/2015
Prism Work Order: 5030124
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
5030124-01 03/04/15MW-9 03/06/15Water
5030124-02 03/04/15MW-10 03/06/15Water
5030124-03 03/04/15MW-11 03/06/15Water
5030124-04 03/04/15MW-12 03/06/15Water
5030124-05 03/04/15SW-2773 03/06/15Water
5030124-06 03/04/15SW-2779 03/06/15Water
5030124-07 03/04/152765INF 03/06/15Water
5030124-08 03/04/152765MID 03/06/15Water
5030124-09 03/04/152765EFF 03/06/15Water
5030124-10 03/05/15MW-1A 03/06/15Water
5030124-11 03/05/15MW-3 03/06/15Water
5030124-12 03/05/15MW-4 03/06/15Water
5030124-13 03/05/15MW-5 03/06/15Water
5030124-14 03/05/15MW-6 03/06/15Water
5030124-15 03/05/15MW-7 03/06/15Water
5030124-16 03/05/15MW-13 03/06/15Water
5030124-17 03/05/15MW-15A 03/06/15Water
5030124-18 03/05/15SW-2760 03/06/15Water
Samples were received in good condition at 4.4 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 56
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 5030124
03/24/2015
Summary of Detections
1.6 ug/L5030124-01 MW-9 Methyl-tert-Butyl Ether SM6200 B
0.50 ug/L5030124-04 MW-12 Isopropyl Ether SM6200 B
0.80 J ug/L5030124-04 MW-12 Methyl-tert-Butyl Ether SM6200 B
0.79 J ug/L5030124-05 SW-2773 Methyl-tert-Butyl Ether SM6200 B
240 E ug/L5030124-05 SW-2773 trans-1,2-Dichloroethylene SM6200 B
15 ug/L5030124-07 2765INF 1,2-Dichloroethane SM6200 B
100 ug/L5030124-07 2765INF Isopropyl Ether SM6200 B
0.63 ug/L5030124-07 2765INF Isopropylbenzene (Cumene)SM6200 B
80 ug/L5030124-07 2765INF Methyl-tert-Butyl Ether SM6200 B
0.98 ug/L5030124-07 2765INF sec-Butylbenzene SM6200 B
5.8 ug/L5030124-10 MW-1A 1,2,4-Trimethylbenzene SM6200 B
2.7 ug/L5030124-10 MW-1A 1,2-Dichloroethane SM6200 B
2.5 ug/L5030124-10 MW-1A 1,3,5-Trimethylbenzene SM6200 B
27 ug/L5030124-10 MW-1A Isopropyl Ether SM6200 B
2.0 ug/L5030124-10 MW-1A m,p-Xylenes SM6200 B
4.6 ug/L5030124-10 MW-1A Methyl-tert-Butyl Ether SM6200 B
0.73 J ug/L5030124-10 MW-1A Naphthalene SM6200 B
1.2 ug/L5030124-10 MW-1A o-Xylene SM6200 B
3.2 ug/L5030124-10 MW-1A Xylenes, total SM6200 B
15 ug/L5030124-12 MW-4 Acetone SM6200 B
0.63 J ug/L5030124-12 MW-4 Methyl Isobutyl Ketone SM6200 B
0.60 J ug/L5030124-14 MW-6 Methyl-tert-Butyl Ether SM6200 B
140 ug/L5030124-17 MW-15A 1,2,4-Trimethylbenzene SM6200 B
42 ug/L5030124-17 MW-15A 1,3,5-Trimethylbenzene SM6200 B
2.0 ug/L5030124-17 MW-15A 4-Isopropyltoluene SM6200 B
1.1 ug/L5030124-17 MW-15A Benzene SM6200 B
120 ug/L5030124-17 MW-15A Ethylbenzene SM6200 B
9.5 ug/L5030124-17 MW-15A Isopropylbenzene (Cumene)SM6200 B
380 ug/L5030124-17 MW-15A m,p-Xylenes SM6200 B
33 ug/L5030124-17 MW-15A Naphthalene SM6200 B
2.3 ug/L5030124-17 MW-15A n-Butylbenzene SM6200 B
17 ug/L5030124-17 MW-15A n-Propylbenzene SM6200 B
190 ug/L5030124-17 MW-15A o-Xylene SM6200 B
1.6 ug/L5030124-17 MW-15A sec-Butylbenzene SM6200 B
2.6 ug/L5030124-17 MW-15A Styrene SM6200 B
58 ug/L5030124-17 MW-15A Toluene SM6200 B
570 ug/L5030124-17 MW-15A Xylenes, total SM6200 B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-9
Prism Sample ID: 5030124-01
Prism Work Order: 5030124
Time Collected: 03/04/15 14:20
Time Submitted: 03/06/15 15:45
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 17:41 VHLug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.111,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5C016512.0 3/9/15 17:41 VHLug/L 0.112,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.0662-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.0504-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5C01651103/9/15 17:41 VHLug/L 0.31Acetone
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.048Benzene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.057Bromobenzene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.14Bromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.062Bromodichloromethane
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.040Bromoform
BRL SM6200 B P5C016511.0 3/9/15 17:41 VHLug/L 0.18Bromomethane
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.062Chlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.22Chloroethane
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.076Chloroform
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.079Chloromethane
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.081Dibromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.065Dibromomethane
BRL SM6200 B P5C016511.0 3/9/15 17:41 VHLug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5C016512003/9/15 17:41 VHLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-9
Prism Sample ID: 5030124-01
Prism Work Order: 5030124
Time Collected: 03/04/15 14:20
Time Submitted: 03/06/15 15:45
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.061Ethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 17:41 VHLug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.050Isopropyl Ether
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5C016511.0 3/9/15 17:41 VHLug/L 0.12m,p-Xylenes
BRL SM6200 B P5C016511.0 3/9/15 17:41 VHLug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5C016515.0 3/9/15 17:41 VHLug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5C016511.0 3/9/15 17:41 VHLug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5C016512.0 3/9/15 17:41 VHLug/L 0.083Methylene Chloride
1.6 SM6200 B P5C016511.0 3/9/15 17:41 VHLug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5C016511.0 3/9/15 17:41 VHLug/L 0.19Naphthalene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.076n-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.087n-Propylbenzene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.044o-Xylene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.076sec-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.047Styrene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.088tert-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.098Tetrachloroethylene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.044Toluene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.078Trichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5C016515.0 3/9/15 17:41 VHLug/L 0.060Vinyl acetate
BRL SM6200 B P5C016510.50 3/9/15 17:41 VHLug/L 0.097Vinyl chloride
BRL SM6200 B P5C016511.5 3/9/15 17:41 VHLug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130111 %4-Bromofluorobenzene
70-130104 %Dibromofluoromethane
70-130109 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-10
Prism Sample ID: 5030124-02
Prism Work Order: 5030124
Time Collected: 03/04/15 14:30
Time Submitted: 03/06/15 15:45
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 18:07 VHLug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.111,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5C016512.0 3/9/15 18:07 VHLug/L 0.112,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.0662-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.0504-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5C01651103/9/15 18:07 VHLug/L 0.31Acetone
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.048Benzene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.057Bromobenzene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.14Bromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.062Bromodichloromethane
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.040Bromoform
BRL SM6200 B P5C016511.0 3/9/15 18:07 VHLug/L 0.18Bromomethane
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.062Chlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.22Chloroethane
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.076Chloroform
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.079Chloromethane
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.081Dibromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.065Dibromomethane
BRL SM6200 B P5C016511.0 3/9/15 18:07 VHLug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5C016512003/9/15 18:07 VHLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-10
Prism Sample ID: 5030124-02
Prism Work Order: 5030124
Time Collected: 03/04/15 14:30
Time Submitted: 03/06/15 15:45
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.061Ethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 18:07 VHLug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.050Isopropyl Ether
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5C016511.0 3/9/15 18:07 VHLug/L 0.12m,p-Xylenes
BRL SM6200 B P5C016511.0 3/9/15 18:07 VHLug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5C016515.0 3/9/15 18:07 VHLug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5C016511.0 3/9/15 18:07 VHLug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5C016512.0 3/9/15 18:07 VHLug/L 0.083Methylene Chloride
BRL SM6200 B P5C016511.0 3/9/15 18:07 VHLug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5C016511.0 3/9/15 18:07 VHLug/L 0.19Naphthalene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.076n-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.087n-Propylbenzene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.044o-Xylene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.076sec-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.047Styrene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.088tert-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.098Tetrachloroethylene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.044Toluene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.078Trichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5C016515.0 3/9/15 18:07 VHLug/L 0.060Vinyl acetate
BRL SM6200 B P5C016510.50 3/9/15 18:07 VHLug/L 0.097Vinyl chloride
BRL SM6200 B P5C016511.5 3/9/15 18:07 VHLug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130110 %4-Bromofluorobenzene
70-130104 %Dibromofluoromethane
70-130110 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-11
Prism Sample ID: 5030124-03
Prism Work Order: 5030124
Time Collected: 03/04/15 14:40
Time Submitted: 03/06/15 15:45
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 18:33 VHLug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.111,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5C016512.0 3/9/15 18:33 VHLug/L 0.112,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.0662-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.0504-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5C01651103/9/15 18:33 VHLug/L 0.31Acetone
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.048Benzene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.057Bromobenzene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.14Bromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.062Bromodichloromethane
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.040Bromoform
BRL SM6200 B P5C016511.0 3/9/15 18:33 VHLug/L 0.18Bromomethane
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.062Chlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.22Chloroethane
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.076Chloroform
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.079Chloromethane
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.081Dibromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.065Dibromomethane
BRL SM6200 B P5C016511.0 3/9/15 18:33 VHLug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5C016512003/9/15 18:33 VHLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-11
Prism Sample ID: 5030124-03
Prism Work Order: 5030124
Time Collected: 03/04/15 14:40
Time Submitted: 03/06/15 15:45
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.061Ethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 18:33 VHLug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.050Isopropyl Ether
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5C016511.0 3/9/15 18:33 VHLug/L 0.12m,p-Xylenes
BRL SM6200 B P5C016511.0 3/9/15 18:33 VHLug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5C016515.0 3/9/15 18:33 VHLug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5C016511.0 3/9/15 18:33 VHLug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5C016512.0 3/9/15 18:33 VHLug/L 0.083Methylene Chloride
BRL SM6200 B P5C016511.0 3/9/15 18:33 VHLug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5C016511.0 3/9/15 18:33 VHLug/L 0.19Naphthalene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.076n-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.087n-Propylbenzene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.044o-Xylene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.076sec-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.047Styrene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.088tert-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.098Tetrachloroethylene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.044Toluene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.078Trichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5C016515.0 3/9/15 18:33 VHLug/L 0.060Vinyl acetate
BRL SM6200 B P5C016510.50 3/9/15 18:33 VHLug/L 0.097Vinyl chloride
BRL SM6200 B P5C016511.5 3/9/15 18:33 VHLug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130109 %4-Bromofluorobenzene
70-130105 %Dibromofluoromethane
70-130110 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-12
Prism Sample ID: 5030124-04
Prism Work Order: 5030124
Time Collected: 03/04/15 14:50
Time Submitted: 03/06/15 15:45
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 18:59 VHLug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.111,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5C016512.0 3/9/15 18:59 VHLug/L 0.112,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.0662-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.0504-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5C01651103/9/15 18:59 VHLug/L 0.31Acetone
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.048Benzene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.057Bromobenzene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.14Bromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.062Bromodichloromethane
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.040Bromoform
BRL SM6200 B P5C016511.0 3/9/15 18:59 VHLug/L 0.18Bromomethane
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.062Chlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.22Chloroethane
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.076Chloroform
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.079Chloromethane
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.081Dibromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.065Dibromomethane
BRL SM6200 B P5C016511.0 3/9/15 18:59 VHLug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5C016512003/9/15 18:59 VHLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-12
Prism Sample ID: 5030124-04
Prism Work Order: 5030124
Time Collected: 03/04/15 14:50
Time Submitted: 03/06/15 15:45
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.061Ethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 18:59 VHLug/L 0.16Hexachlorobutadiene
0.50 SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.050Isopropyl Ether
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5C016511.0 3/9/15 18:59 VHLug/L 0.12m,p-Xylenes
BRL SM6200 B P5C016511.0 3/9/15 18:59 VHLug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5C016515.0 3/9/15 18:59 VHLug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5C016511.0 3/9/15 18:59 VHLug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5C016512.0 3/9/15 18:59 VHLug/L 0.083Methylene Chloride
0.80 SM6200 B P5C016511.0 3/9/15 18:59 VHLJug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5C016511.0 3/9/15 18:59 VHLug/L 0.19Naphthalene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.076n-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.087n-Propylbenzene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.044o-Xylene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.076sec-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.047Styrene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.088tert-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.098Tetrachloroethylene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.044Toluene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.078Trichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5C016515.0 3/9/15 18:59 VHLug/L 0.060Vinyl acetate
BRL SM6200 B P5C016510.50 3/9/15 18:59 VHLug/L 0.097Vinyl chloride
BRL SM6200 B P5C016511.5 3/9/15 18:59 VHLug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130109 %4-Bromofluorobenzene
70-130108 %Dibromofluoromethane
70-130108 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW-2773
Prism Sample ID: 5030124-05
Prism Work Order: 5030124
Time Collected: 03/04/15 13:40
Time Submitted: 03/06/15 15:45
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 19:25 VHLug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.111,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5C016512.0 3/9/15 19:25 VHLug/L 0.112,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.0662-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.0504-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5C01651103/9/15 19:25 VHLug/L 0.31Acetone
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.048Benzene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.057Bromobenzene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.14Bromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.062Bromodichloromethane
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.040Bromoform
BRL SM6200 B P5C016511.0 3/9/15 19:25 VHLug/L 0.18Bromomethane
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.062Chlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.22Chloroethane
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.076Chloroform
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.079Chloromethane
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.081Dibromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.065Dibromomethane
BRL SM6200 B P5C016511.0 3/9/15 19:25 VHLug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5C016512003/9/15 19:25 VHLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW-2773
Prism Sample ID: 5030124-05
Prism Work Order: 5030124
Time Collected: 03/04/15 13:40
Time Submitted: 03/06/15 15:45
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.061Ethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 19:25 VHLug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.050Isopropyl Ether
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5C016511.0 3/9/15 19:25 VHLug/L 0.12m,p-Xylenes
BRL SM6200 B P5C016511.0 3/9/15 19:25 VHLug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5C016515.0 3/9/15 19:25 VHLug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5C016511.0 3/9/15 19:25 VHLug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5C016512.0 3/9/15 19:25 VHLug/L 0.083Methylene Chloride
0.79 SM6200 B P5C016511.0 3/9/15 19:25 VHLJug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5C016511.0 3/9/15 19:25 VHLug/L 0.19Naphthalene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.076n-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.087n-Propylbenzene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.044o-Xylene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.076sec-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.047Styrene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.088tert-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.098Tetrachloroethylene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.044Toluene
240 SM6200 B P5C016510.50 3/9/15 19:25 VHLEug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.078Trichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5C016515.0 3/9/15 19:25 VHLug/L 0.060Vinyl acetate
BRL SM6200 B P5C016510.50 3/9/15 19:25 VHLug/L 0.097Vinyl chloride
BRL SM6200 B P5C016511.5 3/9/15 19:25 VHLug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130115 %4-Bromofluorobenzene
70-130106 %Dibromofluoromethane
70-130107 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW-2779
Prism Sample ID: 5030124-06
Prism Work Order: 5030124
Time Collected: 03/04/15 13:50
Time Submitted: 03/06/15 15:45
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 19:51 VHLug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.111,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5C016512.0 3/9/15 19:51 VHLug/L 0.112,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.0662-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.0504-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5C01651103/9/15 19:51 VHLug/L 0.31Acetone
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.048Benzene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.057Bromobenzene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.14Bromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.062Bromodichloromethane
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.040Bromoform
BRL SM6200 B P5C016511.0 3/9/15 19:51 VHLug/L 0.18Bromomethane
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.062Chlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.22Chloroethane
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.076Chloroform
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.079Chloromethane
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.081Dibromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.065Dibromomethane
BRL SM6200 B P5C016511.0 3/9/15 19:51 VHLug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5C016512003/9/15 19:51 VHLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW-2779
Prism Sample ID: 5030124-06
Prism Work Order: 5030124
Time Collected: 03/04/15 13:50
Time Submitted: 03/06/15 15:45
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.061Ethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 19:51 VHLug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.050Isopropyl Ether
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5C016511.0 3/9/15 19:51 VHLug/L 0.12m,p-Xylenes
BRL SM6200 B P5C016511.0 3/9/15 19:51 VHLug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5C016515.0 3/9/15 19:51 VHLug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5C016511.0 3/9/15 19:51 VHLug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5C016512.0 3/9/15 19:51 VHLug/L 0.083Methylene Chloride
BRL SM6200 B P5C016511.0 3/9/15 19:51 VHLug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5C016511.0 3/9/15 19:51 VHLug/L 0.19Naphthalene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.076n-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.087n-Propylbenzene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.044o-Xylene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.076sec-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.047Styrene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.088tert-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.098Tetrachloroethylene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.044Toluene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.078Trichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5C016515.0 3/9/15 19:51 VHLug/L 0.060Vinyl acetate
BRL SM6200 B P5C016510.50 3/9/15 19:51 VHLug/L 0.097Vinyl chloride
BRL SM6200 B P5C016511.5 3/9/15 19:51 VHLug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130108 %4-Bromofluorobenzene
70-130103 %Dibromofluoromethane
70-130106 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765INF
Prism Sample ID: 5030124-07
Prism Work Order: 5030124
Time Collected: 03/04/15 13:00
Time Submitted: 03/06/15 15:45
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 23:46 VHLug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0761,2-Dichlorobenzene
15 SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.111,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5C016512.0 3/9/15 23:46 VHLug/L 0.112,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0662-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0504-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5C01651103/9/15 23:46 VHLug/L 0.31Acetone
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.048Benzene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.057Bromobenzene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.14Bromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.062Bromodichloromethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.040Bromoform
BRL SM6200 B P5C016511.0 3/9/15 23:46 VHLug/L 0.18Bromomethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.062Chlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.22Chloroethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.076Chloroform
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.079Chloromethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.081Dibromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.065Dibromomethane
BRL SM6200 B P5C016511.0 3/9/15 23:46 VHLug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5C016512003/9/15 23:46 VHLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765INF
Prism Sample ID: 5030124-07
Prism Work Order: 5030124
Time Collected: 03/04/15 13:00
Time Submitted: 03/06/15 15:45
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.061Ethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 23:46 VHLug/L 0.16Hexachlorobutadiene
100 SM6200 B P5C0165100503/9/15 23:46 VHLug/L 5.0Isopropyl Ether
0.63 SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5C016511.0 3/9/15 23:46 VHLug/L 0.12m,p-Xylenes
BRL SM6200 B P5C016511.0 3/9/15 23:46 VHLug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5C016515.0 3/9/15 23:46 VHLug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5C016511.0 3/9/15 23:46 VHLug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5C016512.0 3/9/15 23:46 VHLug/L 0.083Methylene Chloride
80 SM6200 B P5C016511.0 3/9/15 23:46 VHLug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5C016511.0 3/9/15 23:46 VHLug/L 0.19Naphthalene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.076n-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.087n-Propylbenzene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.044o-Xylene
0.98 SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.076sec-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.047Styrene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.088tert-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.098Tetrachloroethylene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.044Toluene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.078Trichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5C016515.0 3/9/15 23:46 VHLug/L 0.060Vinyl acetate
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.097Vinyl chloride
BRL SM6200 B P5C016511.5 3/9/15 23:46 VHLug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130104 %4-Bromofluorobenzene
70-130103 %Dibromofluoromethane
70-130104 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765MID
Prism Sample ID: 5030124-08
Prism Work Order: 5030124
Time Collected: 03/04/15 13:10
Time Submitted: 03/06/15 15:45
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 20:18 VHLug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.111,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5C016512.0 3/9/15 20:18 VHLug/L 0.112,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0662-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0504-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5C01651103/9/15 20:18 VHLug/L 0.31Acetone
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.048Benzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.057Bromobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.14Bromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.062Bromodichloromethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.040Bromoform
BRL SM6200 B P5C016511.0 3/9/15 20:18 VHLug/L 0.18Bromomethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.062Chlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.22Chloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.076Chloroform
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.079Chloromethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.081Dibromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.065Dibromomethane
BRL SM6200 B P5C016511.0 3/9/15 20:18 VHLug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5C016512003/9/15 20:18 VHLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765MID
Prism Sample ID: 5030124-08
Prism Work Order: 5030124
Time Collected: 03/04/15 13:10
Time Submitted: 03/06/15 15:45
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.061Ethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 20:18 VHLug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.050Isopropyl Ether
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5C016511.0 3/9/15 20:18 VHLug/L 0.12m,p-Xylenes
BRL SM6200 B P5C016511.0 3/9/15 20:18 VHLug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5C016515.0 3/9/15 20:18 VHLug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5C016511.0 3/9/15 20:18 VHLug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5C016512.0 3/9/15 20:18 VHLug/L 0.083Methylene Chloride
BRL SM6200 B P5C016511.0 3/9/15 20:18 VHLug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5C016511.0 3/9/15 20:18 VHLug/L 0.19Naphthalene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.076n-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.087n-Propylbenzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.044o-Xylene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.076sec-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.047Styrene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.088tert-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.098Tetrachloroethylene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.044Toluene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.078Trichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5C016515.0 3/9/15 20:18 VHLug/L 0.060Vinyl acetate
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.097Vinyl chloride
BRL SM6200 B P5C016511.5 3/9/15 20:18 VHLug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130110 %4-Bromofluorobenzene
70-130108 %Dibromofluoromethane
70-130106 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765EFF
Prism Sample ID: 5030124-09
Prism Work Order: 5030124
Time Collected: 03/04/15 13:20
Time Submitted: 03/06/15 15:45
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 20:44 VHLug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.111,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5C016512.0 3/9/15 20:44 VHLug/L 0.112,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0662-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0504-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5C01651103/9/15 20:44 VHLug/L 0.31Acetone
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.048Benzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.057Bromobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.14Bromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.062Bromodichloromethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.040Bromoform
BRL SM6200 B P5C016511.0 3/9/15 20:44 VHLug/L 0.18Bromomethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.062Chlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.22Chloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.076Chloroform
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.079Chloromethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.081Dibromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.065Dibromomethane
BRL SM6200 B P5C016511.0 3/9/15 20:44 VHLug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5C016512003/9/15 20:44 VHLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765EFF
Prism Sample ID: 5030124-09
Prism Work Order: 5030124
Time Collected: 03/04/15 13:20
Time Submitted: 03/06/15 15:45
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.061Ethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 20:44 VHLug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.050Isopropyl Ether
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5C016511.0 3/9/15 20:44 VHLug/L 0.12m,p-Xylenes
BRL SM6200 B P5C016511.0 3/9/15 20:44 VHLug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5C016515.0 3/9/15 20:44 VHLug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5C016511.0 3/9/15 20:44 VHLug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5C016512.0 3/9/15 20:44 VHLug/L 0.083Methylene Chloride
BRL SM6200 B P5C016511.0 3/9/15 20:44 VHLug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5C016511.0 3/9/15 20:44 VHLug/L 0.19Naphthalene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.076n-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.087n-Propylbenzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.044o-Xylene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.076sec-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.047Styrene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.088tert-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.098Tetrachloroethylene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.044Toluene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.078Trichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5C016515.0 3/9/15 20:44 VHLug/L 0.060Vinyl acetate
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.097Vinyl chloride
BRL SM6200 B P5C016511.5 3/9/15 20:44 VHLug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130109 %4-Bromofluorobenzene
70-130107 %Dibromofluoromethane
70-130108 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-1A
Prism Sample ID: 5030124-10
Prism Work Order: 5030124
Time Collected: 03/05/15 15:15
Time Submitted: 03/06/15 15:45
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.131,2,4-Trichlorobenzene
5.8 SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 21:10 VHLug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.0761,2-Dichlorobenzene
2.7 SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.111,2-Dichloropropane
2.5 SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5C016512.0 3/9/15 21:10 VHLug/L 0.112,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.0662-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.0504-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5C01651103/9/15 21:10 VHLug/L 0.31Acetone
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.048Benzene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.057Bromobenzene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.14Bromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.062Bromodichloromethane
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.040Bromoform
BRL SM6200 B P5C016511.0 3/9/15 21:10 VHLug/L 0.18Bromomethane
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.062Chlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.22Chloroethane
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.076Chloroform
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.079Chloromethane
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.081Dibromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.065Dibromomethane
BRL SM6200 B P5C016511.0 3/9/15 21:10 VHLug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5C016512003/9/15 21:10 VHLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-1A
Prism Sample ID: 5030124-10
Prism Work Order: 5030124
Time Collected: 03/05/15 15:15
Time Submitted: 03/06/15 15:45
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.061Ethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 21:10 VHLug/L 0.16Hexachlorobutadiene
27 SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.050Isopropyl Ether
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.054Isopropylbenzene (Cumene)
2.0 SM6200 B P5C016511.0 3/9/15 21:10 VHLug/L 0.12m,p-Xylenes
BRL SM6200 B P5C016511.0 3/9/15 21:10 VHLug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5C016515.0 3/9/15 21:10 VHLug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5C016511.0 3/9/15 21:10 VHLug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5C016512.0 3/9/15 21:10 VHLug/L 0.083Methylene Chloride
4.6 SM6200 B P5C016511.0 3/9/15 21:10 VHLug/L 0.042Methyl-tert-Butyl Ether
0.73 SM6200 B P5C016511.0 3/9/15 21:10 VHLJug/L 0.19Naphthalene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.076n-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.087n-Propylbenzene
1.2 SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.044o-Xylene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.076sec-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.047Styrene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.088tert-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.098Tetrachloroethylene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.044Toluene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.078Trichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5C016515.0 3/9/15 21:10 VHLug/L 0.060Vinyl acetate
BRL SM6200 B P5C016510.50 3/9/15 21:10 VHLug/L 0.097Vinyl chloride
3.2 SM6200 B P5C016511.5 3/9/15 21:10 VHLug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130105 %4-Bromofluorobenzene
70-130107 %Dibromofluoromethane
70-130107 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-3
Prism Sample ID: 5030124-11
Prism Work Order: 5030124
Time Collected: 03/05/15 13:45
Time Submitted: 03/06/15 15:45
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 21:36 VHLug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.111,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5C016512.0 3/9/15 21:36 VHLug/L 0.112,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.0662-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.0504-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5C01651103/9/15 21:36 VHLug/L 0.31Acetone
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.048Benzene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.057Bromobenzene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.14Bromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.062Bromodichloromethane
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.040Bromoform
BRL SM6200 B P5C016511.0 3/9/15 21:36 VHLug/L 0.18Bromomethane
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.062Chlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.22Chloroethane
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.076Chloroform
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.079Chloromethane
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.081Dibromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.065Dibromomethane
BRL SM6200 B P5C016511.0 3/9/15 21:36 VHLug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5C016512003/9/15 21:36 VHLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-3
Prism Sample ID: 5030124-11
Prism Work Order: 5030124
Time Collected: 03/05/15 13:45
Time Submitted: 03/06/15 15:45
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.061Ethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 21:36 VHLug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.050Isopropyl Ether
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5C016511.0 3/9/15 21:36 VHLug/L 0.12m,p-Xylenes
BRL SM6200 B P5C016511.0 3/9/15 21:36 VHLug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5C016515.0 3/9/15 21:36 VHLug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5C016511.0 3/9/15 21:36 VHLug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5C016512.0 3/9/15 21:36 VHLug/L 0.083Methylene Chloride
BRL SM6200 B P5C016511.0 3/9/15 21:36 VHLug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5C016511.0 3/9/15 21:36 VHLug/L 0.19Naphthalene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.076n-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.087n-Propylbenzene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.044o-Xylene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.076sec-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.047Styrene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.088tert-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.098Tetrachloroethylene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.044Toluene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.078Trichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5C016515.0 3/9/15 21:36 VHLug/L 0.060Vinyl acetate
BRL SM6200 B P5C016510.50 3/9/15 21:36 VHLug/L 0.097Vinyl chloride
BRL SM6200 B P5C016511.5 3/9/15 21:36 VHLug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130107 %4-Bromofluorobenzene
70-130108 %Dibromofluoromethane
70-130106 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-4
Prism Sample ID: 5030124-12
Prism Work Order: 5030124
Time Collected: 03/05/15 13:55
Time Submitted: 03/06/15 15:45
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 22:02 VHLug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.111,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5C016512.0 3/9/15 22:02 VHLug/L 0.112,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.0662-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.0504-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.0894-Isopropyltoluene
15 SM6200 B P5C01651103/9/15 22:02 VHLug/L 0.31Acetone
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.048Benzene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.057Bromobenzene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.14Bromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.062Bromodichloromethane
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.040Bromoform
BRL SM6200 B P5C016511.0 3/9/15 22:02 VHLug/L 0.18Bromomethane
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.062Chlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.22Chloroethane
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.076Chloroform
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.079Chloromethane
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.081Dibromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.065Dibromomethane
BRL SM6200 B P5C016511.0 3/9/15 22:02 VHLug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5C016512003/9/15 22:02 VHLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-4
Prism Sample ID: 5030124-12
Prism Work Order: 5030124
Time Collected: 03/05/15 13:55
Time Submitted: 03/06/15 15:45
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.061Ethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 22:02 VHLug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.050Isopropyl Ether
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5C016511.0 3/9/15 22:02 VHLug/L 0.12m,p-Xylenes
BRL SM6200 B P5C016511.0 3/9/15 22:02 VHLug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5C016515.0 3/9/15 22:02 VHLug/L 0.24Methyl Ethyl Ketone (2-Butanone)
0.63 SM6200 B P5C016511.0 3/9/15 22:02 VHLJug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5C016512.0 3/9/15 22:02 VHLug/L 0.083Methylene Chloride
BRL SM6200 B P5C016511.0 3/9/15 22:02 VHLug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5C016511.0 3/9/15 22:02 VHLug/L 0.19Naphthalene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.076n-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.087n-Propylbenzene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.044o-Xylene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.076sec-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.047Styrene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.088tert-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.098Tetrachloroethylene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.044Toluene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.078Trichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5C016515.0 3/9/15 22:02 VHLug/L 0.060Vinyl acetate
BRL SM6200 B P5C016510.50 3/9/15 22:02 VHLug/L 0.097Vinyl chloride
BRL SM6200 B P5C016511.5 3/9/15 22:02 VHLug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130113 %4-Bromofluorobenzene
70-130106 %Dibromofluoromethane
70-130107 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-5
Prism Sample ID: 5030124-13
Prism Work Order: 5030124
Time Collected: 03/05/15 14:35
Time Submitted: 03/06/15 15:45
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5C019012.0 3/10/15 16:23 VHLug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.111,2-Dichloropropane
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5C019012.0 3/10/15 16:23 VHLug/L 0.112,2-Dichloropropane
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.0662-Chlorotoluene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.0504-Chlorotoluene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5C01901103/10/15 16:23 VHLug/L 0.31Acetone
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.048Benzene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.057Bromobenzene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.14Bromochloromethane
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.062Bromodichloromethane
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.040Bromoform
BRL SM6200 B P5C019011.0 3/10/15 16:23 VHLug/L 0.18Bromomethane
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.062Chlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.22Chloroethane
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.076Chloroform
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.079Chloromethane
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.081Dibromochloromethane
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.065Dibromomethane
BRL SM6200 B P5C019011.0 3/10/15 16:23 VHLug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5C019012003/10/15 16:23 VHLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-5
Prism Sample ID: 5030124-13
Prism Work Order: 5030124
Time Collected: 03/05/15 14:35
Time Submitted: 03/06/15 15:45
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.061Ethylbenzene
BRL SM6200 B P5C019012.0 3/10/15 16:23 VHLug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.050Isopropyl Ether
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5C019011.0 3/10/15 16:23 VHLug/L 0.12m,p-Xylenes
BRL SM6200 B P5C019011.0 3/10/15 16:23 VHLug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5C019015.0 3/10/15 16:23 VHLug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5C019011.0 3/10/15 16:23 VHLug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5C019012.0 3/10/15 16:23 VHLug/L 0.083Methylene Chloride
BRL SM6200 B P5C019011.0 3/10/15 16:23 VHLug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5C019011.0 3/10/15 16:23 VHLug/L 0.19Naphthalene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.076n-Butylbenzene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.087n-Propylbenzene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.044o-Xylene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.076sec-Butylbenzene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.047Styrene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.088tert-Butylbenzene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.098Tetrachloroethylene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.044Toluene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.078Trichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5C019015.0 3/10/15 16:23 VHLug/L 0.060Vinyl acetate
BRL SM6200 B P5C019010.50 3/10/15 16:23 VHLug/L 0.097Vinyl chloride
BRL SM6200 B P5C019011.5 3/10/15 16:23 VHLug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130110 %4-Bromofluorobenzene
70-130108 %Dibromofluoromethane
70-130109 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-6
Prism Sample ID: 5030124-14
Prism Work Order: 5030124
Time Collected: 03/05/15 15:25
Time Submitted: 03/06/15 15:45
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5C019012.0 3/10/15 16:49 VHLug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.111,2-Dichloropropane
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5C019012.0 3/10/15 16:49 VHLug/L 0.112,2-Dichloropropane
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.0662-Chlorotoluene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.0504-Chlorotoluene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5C01901103/10/15 16:49 VHLug/L 0.31Acetone
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.048Benzene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.057Bromobenzene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.14Bromochloromethane
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.062Bromodichloromethane
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.040Bromoform
BRL SM6200 B P5C019011.0 3/10/15 16:49 VHLug/L 0.18Bromomethane
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.062Chlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.22Chloroethane
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.076Chloroform
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.079Chloromethane
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.081Dibromochloromethane
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.065Dibromomethane
BRL SM6200 B P5C019011.0 3/10/15 16:49 VHLug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5C019012003/10/15 16:49 VHLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-6
Prism Sample ID: 5030124-14
Prism Work Order: 5030124
Time Collected: 03/05/15 15:25
Time Submitted: 03/06/15 15:45
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.061Ethylbenzene
BRL SM6200 B P5C019012.0 3/10/15 16:49 VHLug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.050Isopropyl Ether
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5C019011.0 3/10/15 16:49 VHLug/L 0.12m,p-Xylenes
BRL SM6200 B P5C019011.0 3/10/15 16:49 VHLug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5C019015.0 3/10/15 16:49 VHLug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5C019011.0 3/10/15 16:49 VHLug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5C019012.0 3/10/15 16:49 VHLug/L 0.083Methylene Chloride
0.60 SM6200 B P5C019011.0 3/10/15 16:49 VHLJug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5C019011.0 3/10/15 16:49 VHLug/L 0.19Naphthalene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.076n-Butylbenzene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.087n-Propylbenzene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.044o-Xylene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.076sec-Butylbenzene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.047Styrene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.088tert-Butylbenzene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.098Tetrachloroethylene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.044Toluene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.078Trichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5C019015.0 3/10/15 16:49 VHLug/L 0.060Vinyl acetate
BRL SM6200 B P5C019010.50 3/10/15 16:49 VHLug/L 0.097Vinyl chloride
BRL SM6200 B P5C019011.5 3/10/15 16:49 VHLug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130108 %4-Bromofluorobenzene
70-130107 %Dibromofluoromethane
70-130105 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-7
Prism Sample ID: 5030124-15
Prism Work Order: 5030124
Time Collected: 03/05/15 14:25
Time Submitted: 03/06/15 15:45
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5C019012.0 3/10/15 17:15 VHLug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.111,2-Dichloropropane
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5C019012.0 3/10/15 17:15 VHLug/L 0.112,2-Dichloropropane
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.0662-Chlorotoluene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.0504-Chlorotoluene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5C01901103/10/15 17:15 VHLug/L 0.31Acetone
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.048Benzene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.057Bromobenzene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.14Bromochloromethane
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.062Bromodichloromethane
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.040Bromoform
BRL SM6200 B P5C019011.0 3/10/15 17:15 VHLug/L 0.18Bromomethane
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.062Chlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.22Chloroethane
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.076Chloroform
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.079Chloromethane
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.081Dibromochloromethane
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.065Dibromomethane
BRL SM6200 B P5C019011.0 3/10/15 17:15 VHLug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5C019012003/10/15 17:15 VHLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-7
Prism Sample ID: 5030124-15
Prism Work Order: 5030124
Time Collected: 03/05/15 14:25
Time Submitted: 03/06/15 15:45
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.061Ethylbenzene
BRL SM6200 B P5C019012.0 3/10/15 17:15 VHLug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.050Isopropyl Ether
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5C019011.0 3/10/15 17:15 VHLug/L 0.12m,p-Xylenes
BRL SM6200 B P5C019011.0 3/10/15 17:15 VHLug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5C019015.0 3/10/15 17:15 VHLug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5C019011.0 3/10/15 17:15 VHLug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5C019012.0 3/10/15 17:15 VHLug/L 0.083Methylene Chloride
BRL SM6200 B P5C019011.0 3/10/15 17:15 VHLug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5C019011.0 3/10/15 17:15 VHLug/L 0.19Naphthalene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.076n-Butylbenzene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.087n-Propylbenzene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.044o-Xylene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.076sec-Butylbenzene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.047Styrene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.088tert-Butylbenzene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.098Tetrachloroethylene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.044Toluene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.078Trichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5C019015.0 3/10/15 17:15 VHLug/L 0.060Vinyl acetate
BRL SM6200 B P5C019010.50 3/10/15 17:15 VHLug/L 0.097Vinyl chloride
BRL SM6200 B P5C019011.5 3/10/15 17:15 VHLug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130109 %4-Bromofluorobenzene
70-130111 %Dibromofluoromethane
70-130107 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-13
Prism Sample ID: 5030124-16
Prism Work Order: 5030124
Time Collected: 03/05/15 14:15
Time Submitted: 03/06/15 15:45
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5C019012.0 3/10/15 17:42 VHLug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.111,2-Dichloropropane
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5C019012.0 3/10/15 17:42 VHLug/L 0.112,2-Dichloropropane
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.0662-Chlorotoluene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.0504-Chlorotoluene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5C01901103/10/15 17:42 VHLug/L 0.31Acetone
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.048Benzene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.057Bromobenzene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.14Bromochloromethane
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.062Bromodichloromethane
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.040Bromoform
BRL SM6200 B P5C019011.0 3/10/15 17:42 VHLug/L 0.18Bromomethane
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.062Chlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.22Chloroethane
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.076Chloroform
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.079Chloromethane
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.081Dibromochloromethane
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.065Dibromomethane
BRL SM6200 B P5C019011.0 3/10/15 17:42 VHLug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5C019012003/10/15 17:42 VHLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-13
Prism Sample ID: 5030124-16
Prism Work Order: 5030124
Time Collected: 03/05/15 14:15
Time Submitted: 03/06/15 15:45
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.061Ethylbenzene
BRL SM6200 B P5C019012.0 3/10/15 17:42 VHLug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.050Isopropyl Ether
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5C019011.0 3/10/15 17:42 VHLug/L 0.12m,p-Xylenes
BRL SM6200 B P5C019011.0 3/10/15 17:42 VHLug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5C019015.0 3/10/15 17:42 VHLug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5C019011.0 3/10/15 17:42 VHLug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5C019012.0 3/10/15 17:42 VHLug/L 0.083Methylene Chloride
BRL SM6200 B P5C019011.0 3/10/15 17:42 VHLug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5C019011.0 3/10/15 17:42 VHLug/L 0.19Naphthalene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.076n-Butylbenzene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.087n-Propylbenzene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.044o-Xylene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.076sec-Butylbenzene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.047Styrene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.088tert-Butylbenzene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.098Tetrachloroethylene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.044Toluene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.078Trichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5C019015.0 3/10/15 17:42 VHLug/L 0.060Vinyl acetate
BRL SM6200 B P5C019010.50 3/10/15 17:42 VHLug/L 0.097Vinyl chloride
BRL SM6200 B P5C019011.5 3/10/15 17:42 VHLug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130115 %4-Bromofluorobenzene
70-130107 %Dibromofluoromethane
70-130109 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-15A
Prism Sample ID: 5030124-17
Prism Work Order: 5030124
Time Collected: 03/05/15 15:05
Time Submitted: 03/06/15 15:45
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.131,2,4-Trichlorobenzene
140 SM6200 B P5C0190100503/10/15 19:26 VHLug/L 5.41,2,4-Trimethylbenzene
BRL SM6200 B P5C019012.0 3/10/15 19:00 VHLug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.111,2-Dichloropropane
42 SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5C019012.0 3/10/15 19:00 VHLug/L 0.112,2-Dichloropropane
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.0662-Chlorotoluene
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.0504-Chlorotoluene
2.0 SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5C01901103/10/15 19:00 VHLug/L 0.31Acetone
1.1 SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.048Benzene
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.057Bromobenzene
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.14Bromochloromethane
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.062Bromodichloromethane
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.040Bromoform
BRL SM6200 B P5C019011.0 3/10/15 19:00 VHLug/L 0.18Bromomethane
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.062Chlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.22Chloroethane
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.076Chloroform
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.079Chloromethane
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.081Dibromochloromethane
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.065Dibromomethane
BRL SM6200 B P5C019011.0 3/10/15 19:00 VHLug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5C019012003/10/15 19:00 VHLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: MW-15A
Prism Sample ID: 5030124-17
Prism Work Order: 5030124
Time Collected: 03/05/15 15:05
Time Submitted: 03/06/15 15:45
120 SM6200 B P5C0190100503/10/15 19:26 VHLug/L 6.1Ethylbenzene
BRL SM6200 B P5C019012.0 3/10/15 19:00 VHLug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.050Isopropyl Ether
9.5 SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.054Isopropylbenzene (Cumene)
380 SM6200 B P5C01901001003/10/15 19:26 VHLug/L 12m,p-Xylenes
BRL SM6200 B P5C019011.0 3/10/15 19:00 VHLug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5C019015.0 3/10/15 19:00 VHLug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5C019011.0 3/10/15 19:00 VHLug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5C019012.0 3/10/15 19:00 VHLug/L 0.083Methylene Chloride
BRL SM6200 B P5C019011.0 3/10/15 19:00 VHLug/L 0.042Methyl-tert-Butyl Ether
33 SM6200 B P5C019011.0 3/10/15 19:00 VHLug/L 0.19Naphthalene
2.3 SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.076n-Butylbenzene
17 SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.087n-Propylbenzene
190 SM6200 B P5C0190100503/10/15 19:26 VHLug/L 4.4o-Xylene
1.6 SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.076sec-Butylbenzene
2.6 SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.047Styrene
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.088tert-Butylbenzene
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.098Tetrachloroethylene
58 SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.044Toluene
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.078Trichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5C019015.0 3/10/15 19:00 VHLug/L 0.060Vinyl acetate
BRL SM6200 B P5C019010.50 3/10/15 19:00 VHLug/L 0.097Vinyl chloride
570 SM6200 B P5C01901001503/10/15 19:26 VHLug/L 15Xylenes, total
Surrogate Recovery Control Limits
70-130107 %4-Bromofluorobenzene
70-130101 %Dibromofluoromethane
70-130107 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW-2760
Prism Sample ID: 5030124-18
Prism Work Order: 5030124
Time Collected: 03/05/15 13:25
Time Submitted: 03/06/15 15:45
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5C019012.0 3/10/15 18:08 VHLug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.111,2-Dichloropropane
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5C019012.0 3/10/15 18:08 VHLug/L 0.112,2-Dichloropropane
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.0662-Chlorotoluene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.0504-Chlorotoluene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5C01901103/10/15 18:08 VHLug/L 0.31Acetone
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.048Benzene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.057Bromobenzene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.14Bromochloromethane
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.062Bromodichloromethane
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.040Bromoform
BRL SM6200 B P5C019011.0 3/10/15 18:08 VHLug/L 0.18Bromomethane
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.062Chlorobenzene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.22Chloroethane
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.076Chloroform
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.079Chloromethane
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.081Dibromochloromethane
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.065Dibromomethane
BRL SM6200 B P5C019011.0 3/10/15 18:08 VHLug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5C019012003/10/15 18:08 VHLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: SW-2760
Prism Sample ID: 5030124-18
Prism Work Order: 5030124
Time Collected: 03/05/15 13:25
Time Submitted: 03/06/15 15:45
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.061Ethylbenzene
BRL SM6200 B P5C019012.0 3/10/15 18:08 VHLug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.050Isopropyl Ether
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5C019011.0 3/10/15 18:08 VHLug/L 0.12m,p-Xylenes
BRL SM6200 B P5C019011.0 3/10/15 18:08 VHLug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5C019015.0 3/10/15 18:08 VHLug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5C019011.0 3/10/15 18:08 VHLug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5C019012.0 3/10/15 18:08 VHLug/L 0.083Methylene Chloride
BRL SM6200 B P5C019011.0 3/10/15 18:08 VHLug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5C019011.0 3/10/15 18:08 VHLug/L 0.19Naphthalene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.076n-Butylbenzene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.087n-Propylbenzene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.044o-Xylene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.076sec-Butylbenzene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.047Styrene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.088tert-Butylbenzene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.098Tetrachloroethylene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.044Toluene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.078Trichloroethylene
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5C019015.0 3/10/15 18:08 VHLug/L 0.060Vinyl acetate
BRL SM6200 B P5C019010.50 3/10/15 18:08 VHLug/L 0.097Vinyl chloride
BRL SM6200 B P5C019011.5 3/10/15 18:08 VHLug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130114 %4-Bromofluorobenzene
70-130109 %Dibromofluoromethane
70-130110 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 of 56
3/24/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5030124
Time Submitted: 3/6/2015 3:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0165 - SM6200 B
Blank (P5C0165-BLK1)Prepared & Analyzed: 03/09/15
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL0.50
1,2,4-Trichlorobenzene ug/LBRL0.50
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL10
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL0.50
Bromomethane ug/LBRL1.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethanol ug/LBRL200
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 41 of 56
3/24/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5030124
Time Submitted: 3/6/2015 3:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0165 - SM6200 B
Blank (P5C0165-BLK1)Prepared & Analyzed: 03/09/15
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL1.0
Methylene Chloride ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL1.0
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL0.50
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Butylbenzene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL5.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10753.7
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10954.3
ug/L 50.00 70-130Surrogate: Toluene-d8 10954.7
LCS (P5C0165-BS1)Prepared & Analyzed: 03/09/15
1,1,1,2-Tetrachloroethane ug/L18.4 0.50 20.00 70-13092
1,1,1-Trichloroethane ug/L18.0 0.50 20.00 70-13090
1,1,2,2-Tetrachloroethane ug/L18.4 0.50 20.00 70-13092
1,1,2-Trichloroethane ug/L16.4 0.50 20.00 70-13082
1,1-Dichloroethane ug/L17.3 0.50 20.00 70-13086
1,1-Dichloroethylene ug/L18.5 0.50 20.00 70-13093
1,1-Dichloropropylene ug/L18.6 0.50 20.00 70-13093
1,2,3-Trichlorobenzene ug/L20.3 0.50 20.00 70-130101
1,2,3-Trichloropropane ug/L19.3 0.50 20.00 70-13096
1,2,4-Trichlorobenzene ug/L19.8 0.50 20.00 70-13099
1,2,4-Trimethylbenzene ug/L19.2 0.50 20.00 70-13096
1,2-Dibromo-3-chloropropane ug/L19.4 2.0 20.00 70-13097
1,2-Dibromoethane ug/L19.3 0.50 20.00 70-13097
1,2-Dichlorobenzene ug/L19.0 0.50 20.00 70-13095
1,2-Dichloroethane ug/L17.3 0.50 20.00 70-13086
1,2-Dichloropropane ug/L15.9 0.50 20.00 70-13080
1,3,5-Trimethylbenzene ug/L19.3 0.50 20.00 70-13097
1,3-Dichlorobenzene ug/L18.8 0.50 20.00 70-13094
1,3-Dichloropropane ug/L18.7 0.50 20.00 70-13094
1,4-Dichlorobenzene ug/L18.6 0.50 20.00 70-13093
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 42 of 56
3/24/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5030124
Time Submitted: 3/6/2015 3:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0165 - SM6200 B
LCS (P5C0165-BS1)Prepared & Analyzed: 03/09/15
2,2-Dichloropropane ug/L18.8 2.0 20.00 70-13094
2-Chlorotoluene ug/L18.9 0.50 20.00 70-13094
4-Chlorotoluene ug/L18.6 0.50 20.00 70-13093
4-Isopropyltoluene ug/L17.4 0.50 20.00 70-13087
Acetone ug/L36.8 10 40.00 40-16092
Benzene ug/L17.4 0.50 20.00 70-13087
Bromobenzene ug/L18.5 0.50 20.00 70-13092
Bromochloromethane ug/L17.3 0.50 20.00 70-13087
Bromodichloromethane ug/L15.8 0.50 20.00 70-13079
Bromoform ug/L19.0 0.50 20.00 70-13095
Bromomethane ug/L20.3 1.0 20.00 60-140102
Carbon Tetrachloride ug/L18.7 0.50 20.00 70-13094
Chlorobenzene ug/L18.2 0.50 20.00 70-13091
Chloroethane ug/L17.7 0.50 20.00 60-14088
Chloroform ug/L16.1 0.50 20.00 70-13081
Chloromethane ug/L17.3 0.50 20.00 60-14086
cis-1,2-Dichloroethylene ug/L17.8 0.50 20.00 70-13089
cis-1,3-Dichloropropylene ug/L17.0 0.50 20.00 70-13085
Dibromochloromethane ug/L17.8 0.50 20.00 70-13089
Dibromomethane ug/L16.8 0.50 20.00 70-13084
Dichlorodifluoromethane ug/L18.6 1.0 20.00 60-14093
Ethanol ug/L408200 500.0 60-14082
Ethylbenzene ug/L18.4 0.50 20.00 70-13092
Hexachlorobutadiene ug/L19.8 2.0 20.00 70-13099
Isopropyl Ether ug/L15.5 0.50 20.00 70-13078
Isopropylbenzene (Cumene)ug/L19.4 0.50 20.00 70-13097
m,p-Xylenes ug/L39.6 1.0 40.00 70-13099
Methyl Butyl Ketone (2-Hexanone)ug/L18.5 1.0 20.00 60-14093
Methyl Ethyl Ketone (2-Butanone)ug/L17.6 5.0 20.00 60-14088
Methyl Isobutyl Ketone ug/L15.6 1.0 20.00 60-14078
Methylene Chloride ug/L17.0 2.0 20.00 70-13085
Methyl-tert-Butyl Ether ug/L17.9 1.0 20.00 70-13089
Naphthalene ug/L20.7 1.0 20.00 70-130103
n-Butylbenzene ug/L17.3 0.50 20.00 70-13086
n-Propylbenzene ug/L18.9 0.50 20.00 70-13094
o-Xylene ug/L19.0 0.50 20.00 70-13095
sec-Butylbenzene ug/L16.8 0.50 20.00 70-13084
Styrene ug/L19.3 0.50 20.00 70-13096
tert-Butylbenzene ug/L19.1 0.50 20.00 70-13096
Tetrachloroethylene ug/L19.7 0.50 20.00 70-13099
Toluene ug/L16.0 0.50 20.00 70-13080
trans-1,2-Dichloroethylene ug/L17.4 0.50 20.00 70-13087
trans-1,3-Dichloropropylene ug/L16.8 0.50 20.00 70-13084
Trichloroethylene ug/L17.0 0.50 20.00 70-13085
Trichlorofluoromethane ug/L19.9 0.50 20.00 60-14099
Vinyl acetate ug/L19.8 5.0 20.00 60-14099
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 43 of 56
3/24/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5030124
Time Submitted: 3/6/2015 3:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0165 - SM6200 B
LCS (P5C0165-BS1)Prepared & Analyzed: 03/09/15
Vinyl chloride ug/L17.8 0.50 20.00 60-14089
Xylenes, total ug/L58.7 1.5 60.00 70-13098
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10251.0
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10150.4
ug/L 50.00 70-130Surrogate: Toluene-d8 10552.5
LCS Dup (P5C0165-BSD1)Prepared & Analyzed: 03/09/15
1,1,1,2-Tetrachloroethane ug/L18.5 0.50 20.00 2070-13092 0.3
1,1,1-Trichloroethane ug/L18.4 0.50 20.00 2070-13092 2
1,1,2,2-Tetrachloroethane ug/L18.3 0.50 20.00 2070-13091 1
1,1,2-Trichloroethane ug/L16.4 0.50 20.00 2070-13082 0
1,1-Dichloroethane ug/L17.5 0.50 20.00 2070-13088 1
1,1-Dichloroethylene ug/L18.6 0.50 20.00 2070-13093 0.4
1,1-Dichloropropylene ug/L19.2 0.50 20.00 2070-13096 3
1,2,3-Trichlorobenzene ug/L22.5 0.50 20.00 2070-130112 10
1,2,3-Trichloropropane ug/L18.7 0.50 20.00 2070-13093 3
1,2,4-Trichlorobenzene ug/L21.4 0.50 20.00 2070-130107 7
1,2,4-Trimethylbenzene ug/L19.8 0.50 20.00 2070-13099 3
1,2-Dibromo-3-chloropropane ug/L19.6 2.0 20.00 2070-13098 0.6
1,2-Dibromoethane ug/L19.0 0.50 20.00 2070-13095 2
1,2-Dichlorobenzene ug/L19.5 0.50 20.00 2070-13098 3
1,2-Dichloroethane ug/L17.6 0.50 20.00 2070-13088 2
1,2-Dichloropropane ug/L16.5 0.50 20.00 2070-13083 4
1,3,5-Trimethylbenzene ug/L19.5 0.50 20.00 2070-13098 1
1,3-Dichlorobenzene ug/L19.5 0.50 20.00 2070-13098 4
1,3-Dichloropropane ug/L18.9 0.50 20.00 2070-13094 0.7
1,4-Dichlorobenzene ug/L19.3 0.50 20.00 2070-13096 3
2,2-Dichloropropane ug/L18.5 2.0 20.00 2070-13093 2
2-Chlorotoluene ug/L18.9 0.50 20.00 2070-13095 0.2
4-Chlorotoluene ug/L18.8 0.50 20.00 2070-13094 0.9
4-Isopropyltoluene ug/L18.0 0.50 20.00 2070-13090 4
Acetone ug/L35.9 10 40.00 2040-16090 3
Benzene ug/L18.0 0.50 20.00 2070-13090 3
Bromobenzene ug/L18.5 0.50 20.00 2070-13092 0.2
Bromochloromethane ug/L17.3 0.50 20.00 2070-13087 0.2
Bromodichloromethane ug/L16.0 0.50 20.00 2070-13080 1
Bromoform ug/L18.8 0.50 20.00 2070-13094 1
Bromomethane ug/L19.8 1.0 20.00 2060-14099 3
Carbon Tetrachloride ug/L18.7 0.50 20.00 2070-13094 0.05
Chlorobenzene ug/L18.7 0.50 20.00 2070-13093 3
Chloroethane ug/L18.0 0.50 20.00 2060-14090 2
Chloroform ug/L15.8 0.50 20.00 2070-13079 2
Chloromethane ug/L15.3 0.50 20.00 2060-14077 12
cis-1,2-Dichloroethylene ug/L18.1 0.50 20.00 2070-13090 1
cis-1,3-Dichloropropylene ug/L17.1 0.50 20.00 2070-13086 0.6
Dibromochloromethane ug/L18.0 0.50 20.00 2070-13090 1
Dibromomethane ug/L17.0 0.50 20.00 2070-13085 1
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 44 of 56
3/24/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5030124
Time Submitted: 3/6/2015 3:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0165 - SM6200 B
LCS Dup (P5C0165-BSD1)Prepared & Analyzed: 03/09/15
Dichlorodifluoromethane ug/L17.5 1.0 20.00 2060-14088 6
Ethanol ug/L352200 500.0 2060-14070 15
Ethylbenzene ug/L18.7 0.50 20.00 2070-13094 2
Hexachlorobutadiene ug/L20.1 2.0 20.00 2070-130101 2
Isopropyl Ether ug/L15.8 0.50 20.00 2070-13079 2
Isopropylbenzene (Cumene)ug/L19.6 0.50 20.00 2070-13098 1
m,p-Xylenes ug/L40.1 1.0 40.00 2070-130100 1
Methyl Butyl Ketone (2-Hexanone)ug/L18.8 1.0 20.00 2060-14094 1
Methyl Ethyl Ketone (2-Butanone)ug/L16.0 5.0 20.00 2060-14080 10
Methyl Isobutyl Ketone ug/L15.7 1.0 20.00 2060-14079 1
Methylene Chloride ug/L17.2 2.0 20.00 2070-13086 0.9
Methyl-tert-Butyl Ether ug/L18.2 1.0 20.00 2070-13091 2
Naphthalene ug/L22.2 1.0 20.00 2070-130111 7
n-Butylbenzene ug/L17.7 0.50 20.00 2070-13088 2
n-Propylbenzene ug/L19.4 0.50 20.00 2070-13097 3
o-Xylene ug/L19.2 0.50 20.00 2070-13096 0.7
sec-Butylbenzene ug/L17.3 0.50 20.00 2070-13086 3
Styrene ug/L19.6 0.50 20.00 2070-13098 1
tert-Butylbenzene ug/L19.3 0.50 20.00 2070-13097 1
Tetrachloroethylene ug/L20.0 0.50 20.00 2070-130100 2
Toluene ug/L16.2 0.50 20.00 2070-13081 1
trans-1,2-Dichloroethylene ug/L17.8 0.50 20.00 2070-13089 2
trans-1,3-Dichloropropylene ug/L17.2 0.50 20.00 2070-13086 2
Trichloroethylene ug/L17.0 0.50 20.00 2070-13085 0.2
Trichlorofluoromethane ug/L20.5 0.50 20.00 2060-140102 3
Vinyl acetate ug/L19.8 5.0 20.00 2060-14099 0.1
Vinyl chloride ug/L17.6 0.50 20.00 2060-14088 1
Xylenes, total ug/L59.2 1.5 60.00 2070-13099 0.9
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10552.7
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10451.9
ug/L 50.00 70-130Surrogate: Toluene-d8 10854.2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 45 of 56
3/24/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5030124
Time Submitted: 3/6/2015 3:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0190 - SM6200 B
Blank (P5C0190-BLK1)Prepared & Analyzed: 03/10/15
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL0.50
1,2,4-Trichlorobenzene ug/LBRL0.50
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL10
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL0.50
Bromomethane ug/LBRL1.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethanol ug/LBRL200
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 46 of 56
3/24/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5030124
Time Submitted: 3/6/2015 3:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0190 - SM6200 B
Blank (P5C0190-BLK1)Prepared & Analyzed: 03/10/15
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL1.0
Methylene Chloride ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL1.0
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL0.50
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Butylbenzene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL5.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10753.7
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10954.4
ug/L 50.00 70-130Surrogate: Toluene-d8 10853.8
LCS (P5C0190-BS1)Prepared & Analyzed: 03/10/15
1,1,1,2-Tetrachloroethane ug/L16.7 0.50 20.00 70-13084
1,1,1-Trichloroethane ug/L17.1 0.50 20.00 70-13086
1,1,2,2-Tetrachloroethane ug/L16.1 0.50 20.00 70-13081
1,1,2-Trichloroethane ug/L15.0 0.50 20.00 70-13075
1,1-Dichloroethane ug/L16.4 0.50 20.00 70-13082
1,1-Dichloroethylene ug/L17.8 0.50 20.00 70-13089
1,1-Dichloropropylene ug/L17.9 0.50 20.00 70-13090
1,2,3-Trichlorobenzene ug/L16.3 0.50 20.00 70-13082
1,2,3-Trichloropropane ug/L17.5 0.50 20.00 70-13087
1,2,4-Trichlorobenzene ug/L16.9 0.50 20.00 70-13084
1,2,4-Trimethylbenzene ug/L18.2 0.50 20.00 70-13091
1,2-Dibromo-3-chloropropane ug/L18.0 2.0 20.00 70-13090
1,2-Dibromoethane ug/L17.1 0.50 20.00 70-13085
1,2-Dichlorobenzene ug/L17.4 0.50 20.00 70-13087
1,2-Dichloroethane ug/L15.8 0.50 20.00 70-13079
1,2-Dichloropropane ug/L15.6 0.50 20.00 70-13078
1,3,5-Trimethylbenzene ug/L18.0 0.50 20.00 70-13090
1,3-Dichlorobenzene ug/L17.6 0.50 20.00 70-13088
1,3-Dichloropropane ug/L17.3 0.50 20.00 70-13087
1,4-Dichlorobenzene ug/L17.5 0.50 20.00 70-13088
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 47 of 56
3/24/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5030124
Time Submitted: 3/6/2015 3:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0190 - SM6200 B
LCS (P5C0190-BS1)Prepared & Analyzed: 03/10/15
2,2-Dichloropropane ug/L17.8 2.0 20.00 70-13089
2-Chlorotoluene ug/L17.4 0.50 20.00 70-13087
4-Chlorotoluene ug/L17.0 0.50 20.00 70-13085
4-Isopropyltoluene ug/L16.3 0.50 20.00 70-13082
Acetone ug/L32.6 10 40.00 40-16081
Benzene ug/L16.9 0.50 20.00 70-13085
Bromobenzene ug/L16.9 0.50 20.00 70-13084
Bromochloromethane ug/L16.3 0.50 20.00 70-13081
Bromodichloromethane ug/L14.9 0.50 20.00 70-13074
Bromoform ug/L16.4 0.50 20.00 70-13082
Bromomethane ug/L19.3 1.0 20.00 60-14096
Carbon Tetrachloride ug/L17.5 0.50 20.00 70-13088
Chlorobenzene ug/L16.9 0.50 20.00 70-13085
Chloroethane ug/L16.7 0.50 20.00 60-14084
Chloroform ug/L14.6 0.50 20.00 70-13073
Chloromethane ug/L14.9 0.50 20.00 60-14074
cis-1,2-Dichloroethylene ug/L17.3 0.50 20.00 70-13086
cis-1,3-Dichloropropylene ug/L16.1 0.50 20.00 70-13081
Dibromochloromethane ug/L16.3 0.50 20.00 70-13081
Dibromomethane ug/L15.2 0.50 20.00 70-13076
Dichlorodifluoromethane ug/L17.6 1.0 20.00 60-14088
Ethanol ug/L305200 500.0 60-14061
Ethylbenzene ug/L17.1 0.50 20.00 70-13086
Hexachlorobutadiene ug/L17.2 2.0 20.00 70-13086
Isopropyl Ether ug/L14.8 0.50 20.00 70-13074
Isopropylbenzene (Cumene)ug/L17.7 0.50 20.00 70-13089
m,p-Xylenes ug/L36.8 1.0 40.00 70-13092
Methyl Butyl Ketone (2-Hexanone)ug/L16.3 1.0 20.00 60-14081
Methyl Ethyl Ketone (2-Butanone)ug/L16.5 5.0 20.00 60-14082
Methyl Isobutyl Ketone ug/L14.3 1.0 20.00 60-14072
Methylene Chloride ug/L16.6 2.0 20.00 70-13083
Methyl-tert-Butyl Ether ug/L16.6 1.0 20.00 70-13083
Naphthalene ug/L16.6 1.0 20.00 70-13083
n-Butylbenzene ug/L16.4 0.50 20.00 70-13082
n-Propylbenzene ug/L18.0 0.50 20.00 70-13090
o-Xylene ug/L17.5 0.50 20.00 70-13088
sec-Butylbenzene ug/L16.2 0.50 20.00 70-13081
Styrene ug/L17.8 0.50 20.00 70-13089
tert-Butylbenzene ug/L17.6 0.50 20.00 70-13088
Tetrachloroethylene ug/L18.3 0.50 20.00 70-13091
Toluene ug/L15.3 0.50 20.00 70-13076
trans-1,2-Dichloroethylene ug/L17.0 0.50 20.00 70-13085
trans-1,3-Dichloropropylene ug/L15.5 0.50 20.00 70-13078
Trichloroethylene ug/L16.0 0.50 20.00 70-13080
Trichlorofluoromethane ug/L20.0 0.50 20.00 60-140100
Vinyl acetate ug/L18.6 5.0 20.00 60-14093
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 48 of 56
3/24/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5030124
Time Submitted: 3/6/2015 3:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0190 - SM6200 B
LCS (P5C0190-BS1)Prepared & Analyzed: 03/10/15
Vinyl chloride ug/L17.0 0.50 20.00 60-14085
Xylenes, total ug/L54.3 1.5 60.00 70-13091
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10452.0
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10351.7
ug/L 50.00 70-130Surrogate: Toluene-d8 10552.6
LCS Dup (P5C0190-BSD1)Prepared & Analyzed: 03/10/15
1,1,1,2-Tetrachloroethane ug/L18.3 0.50 20.00 2070-13092 9
1,1,1-Trichloroethane ug/L18.1 0.50 20.00 2070-13090 6
1,1,2,2-Tetrachloroethane ug/L17.2 0.50 20.00 2070-13086 6
1,1,2-Trichloroethane ug/L15.9 0.50 20.00 2070-13080 6
1,1-Dichloroethane ug/L17.7 0.50 20.00 2070-13088 7
1,1-Dichloroethylene ug/L18.9 0.50 20.00 2070-13095 6
1,1-Dichloropropylene ug/L19.3 0.50 20.00 2070-13097 8
1,2,3-Trichlorobenzene ug/L18.6 0.50 20.00 2070-13093 13
1,2,3-Trichloropropane ug/L18.5 0.50 20.00 2070-13092 6
1,2,4-Trichlorobenzene ug/L19.9 0.50 20.00 2070-13099 16
1,2,4-Trimethylbenzene ug/L19.2 0.50 20.00 2070-13096 5
1,2-Dibromo-3-chloropropane ug/L20.1 2.0 20.00 2070-130100 11
1,2-Dibromoethane ug/L18.4 0.50 20.00 2070-13092 8
1,2-Dichlorobenzene ug/L18.9 0.50 20.00 2070-13094 8
1,2-Dichloroethane ug/L17.0 0.50 20.00 2070-13085 7
1,2-Dichloropropane ug/L16.3 0.50 20.00 2070-13081 5
1,3,5-Trimethylbenzene ug/L19.5 0.50 20.00 2070-13097 8
1,3-Dichlorobenzene ug/L18.8 0.50 20.00 2070-13094 6
1,3-Dichloropropane ug/L18.8 0.50 20.00 2070-13094 8
1,4-Dichlorobenzene ug/L18.7 0.50 20.00 2070-13094 7
2,2-Dichloropropane ug/L18.3 2.0 20.00 2070-13092 3
2-Chlorotoluene ug/L18.7 0.50 20.00 2070-13094 7
4-Chlorotoluene ug/L18.5 0.50 20.00 2070-13093 8
4-Isopropyltoluene ug/L17.6 0.50 20.00 2070-13088 8
Acetone ug/L34.8 10 40.00 2040-16087 7
Benzene ug/L18.1 0.50 20.00 2070-13090 6
Bromobenzene ug/L18.0 0.50 20.00 2070-13090 7
Bromochloromethane ug/L17.0 0.50 20.00 2070-13085 4
Bromodichloromethane ug/L15.9 0.50 20.00 2070-13080 7
Bromoform ug/L18.0 0.50 20.00 2070-13090 9
Bromomethane ug/L21.0 1.0 20.00 2060-140105 9
Carbon Tetrachloride ug/L19.0 0.50 20.00 2070-13095 8
Chlorobenzene ug/L18.6 0.50 20.00 2070-13093 10
Chloroethane ug/L17.8 0.50 20.00 2060-14089 6
Chloroform ug/L15.7 0.50 20.00 2070-13079 7
Chloromethane ug/L16.0 0.50 20.00 2060-14080 7
cis-1,2-Dichloroethylene ug/L18.4 0.50 20.00 2070-13092 6
cis-1,3-Dichloropropylene ug/L16.9 0.50 20.00 2070-13084 5
Dibromochloromethane ug/L17.4 0.50 20.00 2070-13087 7
Dibromomethane ug/L16.4 0.50 20.00 2070-13082 8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 49 of 56
3/24/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5030124
Time Submitted: 3/6/2015 3:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0190 - SM6200 B
LCS Dup (P5C0190-BSD1)Prepared & Analyzed: 03/10/15
Dichlorodifluoromethane ug/L18.9 1.0 20.00 2060-14094 7
Ethanol ug/L317200 500.0 2060-14063 4
Ethylbenzene ug/L18.7 0.50 20.00 2070-13094 9
Hexachlorobutadiene ug/L19.2 2.0 20.00 2070-13096 10
Isopropyl Ether ug/L15.9 0.50 20.00 2070-13080 7
Isopropylbenzene (Cumene)ug/L19.3 0.50 20.00 2070-13097 9
m,p-Xylenes ug/L40.6 1.0 40.00 2070-130102 10
Methyl Butyl Ketone (2-Hexanone)ug/L17.2 1.0 20.00 2060-14086 6
Methyl Ethyl Ketone (2-Butanone)ug/L16.3 5.0 20.00 2060-14081 1
Methyl Isobutyl Ketone ug/L14.8 1.0 20.00 2060-14074 3
Methylene Chloride ug/L17.4 2.0 20.00 2070-13087 5
Methyl-tert-Butyl Ether ug/L17.8 1.0 20.00 2070-13089 7
Naphthalene ug/L19.3 1.0 20.00 2070-13096 15
n-Butylbenzene ug/L17.6 0.50 20.00 2070-13088 7
n-Propylbenzene ug/L19.3 0.50 20.00 2070-13096 7
o-Xylene ug/L19.2 0.50 20.00 2070-13096 9
sec-Butylbenzene ug/L17.6 0.50 20.00 2070-13088 8
Styrene ug/L19.5 0.50 20.00 2070-13098 9
tert-Butylbenzene ug/L19.3 0.50 20.00 2070-13097 9
Tetrachloroethylene ug/L19.6 0.50 20.00 2070-13098 7
Toluene ug/L16.4 0.50 20.00 2070-13082 7
trans-1,2-Dichloroethylene ug/L18.3 0.50 20.00 2070-13092 8
trans-1,3-Dichloropropylene ug/L16.6 0.50 20.00 2070-13083 7
Trichloroethylene ug/L17.4 0.50 20.00 2070-13087 8
Trichlorofluoromethane ug/L21.1 0.50 20.00 2060-140106 6
Vinyl acetate ug/L19.8 5.0 20.00 2060-14099 6
Vinyl chloride ug/L18.1 0.50 20.00 2060-14090 6
Xylenes, total ug/L59.9 1.5 60.00 2070-130100 10
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10351.5
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10150.7
ug/L 50.00 70-130Surrogate: Toluene-d8 10753.4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 50 of 56
3/24/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5030124
Time Submitted: 3/6/2015 3:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0190 - SM6200 B
Matrix Spike (P5C0190-MS1)Prepared: 03/10/15 Analyzed: 03/11/15 Source: 5030124-13
1,1,1,2-Tetrachloroethane ug/L1865.0 200.0 BRL 70-13093
1,1,1-Trichloroethane ug/L1955.0 200.0 BRL 70-13097
1,1,2,2-Tetrachloroethane ug/L1745.0 200.0 BRL 70-13087
1,1,2-Trichloroethane ug/L1625.0 200.0 BRL 70-13081
1,1-Dichloroethane ug/L1905.0 200.0 BRL 70-13095
1,1-Dichloroethylene ug/L2055.0 200.0 BRL 70-130102
1,1-Dichloropropylene ug/L2085.0 200.0 BRL 70-130104
1,2,3-Trichlorobenzene ug/L2215.0 200.0 BRL 70-130110
1,2,3-Trichloropropane ug/L1765.0 200.0 BRL 70-13088
1,2,4-Trichlorobenzene ug/L2015.0 200.0 BRL 70-130101
1,2,4-Trimethylbenzene ug/L2025.0 200.0 BRL 70-130101
1,2-Dibromo-3-chloropropane ug/L18420 200.0 BRL 70-13092
1,2-Dibromoethane ug/L1855.0 200.0 BRL 70-13093
1,2-Dichlorobenzene ug/L1935.0 200.0 BRL 70-13096
1,2-Dichloroethane ug/L1805.0 200.0 BRL 70-13090
1,2-Dichloropropane ug/L1765.0 200.0 BRL 70-13088
1,3,5-Trimethylbenzene ug/L2015.0 200.0 BRL 70-130101
1,3-Dichlorobenzene ug/L1955.0 200.0 BRL 70-13098
1,3-Dichloropropane ug/L1925.0 200.0 BRL 70-13096
1,4-Dichlorobenzene ug/L1925.0 200.0 BRL 70-13096
2,2-Dichloropropane ug/L15120 200.0 BRL 70-13076
2-Chlorotoluene ug/L1945.0 200.0 BRL 70-13097
4-Chlorotoluene ug/L1945.0 200.0 BRL 70-13097
4-Isopropyltoluene ug/L1845.0 200.0 BRL 70-13092
Acetone ug/L362100 400.0 BRL 40-16090
Benzene ug/L1935.0 200.0 BRL 70-13097
Bromobenzene ug/L1935.0 200.0 BRL 70-13097
Bromochloromethane ug/L1765.0 200.0 BRL 70-13088
Bromodichloromethane ug/L1665.0 200.0 BRL 70-13083
Bromoform ug/L1715.0 200.0 BRL 70-13086
Bromomethane ug/L18510 200.0 BRL 60-14092
Carbon Tetrachloride ug/L2045.0 200.0 BRL 70-130102
Chlorobenzene ug/L1875.0 200.0 BRL 70-13093
Chloroethane ug/L1845.0 200.0 BRL 60-14092
Chloroform ug/L1685.0 200.0 BRL 70-13084
Chloromethane ug/L1715.0 200.0 BRL 60-14085
cis-1,2-Dichloroethylene ug/L1905.0 200.0 BRL 70-13095
cis-1,3-Dichloropropylene ug/L1595.0 200.0 BRL 70-13080
Dibromochloromethane ug/L1725.0 200.0 BRL 70-13086
Dibromomethane ug/L1685.0 200.0 BRL 70-13084
Dichlorodifluoromethane ug/L20810 200.0 BRL 60-140104
Ethanol ug/L25602000 5000 BRL M60-14051
Ethylbenzene ug/L1935.0 200.0 BRL 70-13097
Hexachlorobutadiene ug/L19320 200.0 BRL 70-13096
Isopropyl Ether ug/L1675.0 200.0 BRL 70-13084
Isopropylbenzene (Cumene)ug/L2045.0 200.0 BRL 70-130102
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 51 of 56
3/24/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5030124
Time Submitted: 3/6/2015 3:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0190 - SM6200 B
Matrix Spike (P5C0190-MS1)Prepared: 03/10/15 Analyzed: 03/11/15 Source: 5030124-13
m,p-Xylenes ug/L41610 400.0 BRL 70-130104
Methyl Butyl Ketone (2-Hexanone)ug/L16810 200.0 BRL 60-14084
Methyl Ethyl Ketone (2-Butanone)ug/L17750 200.0 BRL 60-14088
Methyl Isobutyl Ketone ug/L15210 200.0 BRL 60-14076
Methylene Chloride ug/L18820 200.0 BRL 70-13094
Methyl-tert-Butyl Ether ug/L17910 200.0 BRL 70-13090
Naphthalene ug/L19210 200.0 BRL 70-13096
n-Butylbenzene ug/L1905.0 200.0 BRL 70-13095
n-Propylbenzene ug/L2035.0 200.0 BRL 70-130102
o-Xylene ug/L1945.0 200.0 BRL 70-13097
sec-Butylbenzene ug/L1835.0 200.0 BRL 70-13091
Styrene ug/L1975.0 200.0 BRL 70-13098
tert-Butylbenzene ug/L2025.0 200.0 BRL 70-130101
Tetrachloroethylene ug/L2035.0 200.0 BRL 70-130101
Toluene ug/L1745.0 200.0 BRL 70-13087
trans-1,2-Dichloroethylene ug/L1895.0 200.0 BRL 70-13094
trans-1,3-Dichloropropylene ug/L1635.0 200.0 BRL 70-13082
Trichloroethylene ug/L1835.0 200.0 BRL 70-13092
Trichlorofluoromethane ug/L2225.0 200.0 BRL 60-140111
Vinyl acetate ug/L21250 200.0 BRL 60-140106
Vinyl chloride ug/L1945.0 200.0 BRL 60-14097
Xylenes, total ug/L61015 600.0 BRL 70-130102
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10251.0
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9848.9
ug/L 50.00 70-130Surrogate: Toluene-d8 10552.5
Matrix Spike Dup (P5C0190-MSD1)Prepared: 03/10/15 Analyzed: 03/11/15 Source: 5030124-13
1,1,1,2-Tetrachloroethane ug/L1745.0 200.0 BRL 2070-13087 7
1,1,1-Trichloroethane ug/L1735.0 200.0 BRL 2070-13087 12
1,1,2,2-Tetrachloroethane ug/L1595.0 200.0 BRL 2070-13080 9
1,1,2-Trichloroethane ug/L1535.0 200.0 BRL 2070-13076 6
1,1-Dichloroethane ug/L1725.0 200.0 BRL 2070-13086 10
1,1-Dichloroethylene ug/L1865.0 200.0 BRL 2070-13093 9
1,1-Dichloropropylene ug/L1895.0 200.0 BRL 2070-13095 10
1,2,3-Trichlorobenzene ug/L1895.0 200.0 BRL 2070-13094 16
1,2,3-Trichloropropane ug/L1685.0 200.0 BRL 2070-13084 5
1,2,4-Trichlorobenzene ug/L1755.0 200.0 BRL 2070-13087 14
1,2,4-Trimethylbenzene ug/L1825.0 200.0 BRL 2070-13091 11
1,2-Dibromo-3-chloropropane ug/L16920 200.0 BRL 2070-13084 8
1,2-Dibromoethane ug/L1725.0 200.0 BRL 2070-13086 8
1,2-Dichlorobenzene ug/L1755.0 200.0 BRL 2070-13088 10
1,2-Dichloroethane ug/L1635.0 200.0 BRL 2070-13082 10
1,2-Dichloropropane ug/L1585.0 200.0 BRL 2070-13079 11
1,3,5-Trimethylbenzene ug/L1835.0 200.0 BRL 2070-13091 10
1,3-Dichlorobenzene ug/L1785.0 200.0 BRL 2070-13089 9
1,3-Dichloropropane ug/L1725.0 200.0 BRL 2070-13086 11
1,4-Dichlorobenzene ug/L1755.0 200.0 BRL 2070-13087 9
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 52 of 56
3/24/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5030124
Time Submitted: 3/6/2015 3:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0190 - SM6200 B
Matrix Spike Dup (P5C0190-MSD1)Prepared: 03/10/15 Analyzed: 03/11/15 Source: 5030124-13
2,2-Dichloropropane ug/L13420 200.0 BRL 20 M70-13067 12
2-Chlorotoluene ug/L1785.0 200.0 BRL 2070-13089 9
4-Chlorotoluene ug/L1755.0 200.0 BRL 2070-13087 11
4-Isopropyltoluene ug/L1645.0 200.0 BRL 2070-13082 12
Acetone ug/L336100 400.0 BRL 2040-16084 7
Benzene ug/L1765.0 200.0 BRL 2070-13088 9
Bromobenzene ug/L1735.0 200.0 BRL 2070-13087 11
Bromochloromethane ug/L1655.0 200.0 BRL 2070-13082 7
Bromodichloromethane ug/L1535.0 200.0 BRL 2070-13076 8
Bromoform ug/L1685.0 200.0 BRL 2070-13084 2
Bromomethane ug/L18610 200.0 BRL 2060-14093 1
Carbon Tetrachloride ug/L1845.0 200.0 BRL 2070-13092 10
Chlorobenzene ug/L1765.0 200.0 BRL 2070-13088 6
Chloroethane ug/L1795.0 200.0 BRL 2060-14089 3
Chloroform ug/L1505.0 200.0 BRL 2070-13075 11
Chloromethane ug/L1545.0 200.0 BRL 2060-14077 10
cis-1,2-Dichloroethylene ug/L1785.0 200.0 BRL 2070-13089 7
cis-1,3-Dichloropropylene ug/L1505.0 200.0 BRL 2070-13075 6
Dibromochloromethane ug/L1565.0 200.0 BRL 2070-13078 10
Dibromomethane ug/L1565.0 200.0 BRL 2070-13078 7
Dichlorodifluoromethane ug/L18510 200.0 BRL 2060-14093 12
Ethanol ug/L27502000 5000 BRL 20 M60-14055 7
Ethylbenzene ug/L1785.0 200.0 BRL 2070-13089 9
Hexachlorobutadiene ug/L17920 200.0 BRL 2070-13090 7
Isopropyl Ether ug/L1545.0 200.0 BRL 2070-13077 8
Isopropylbenzene (Cumene)ug/L1845.0 200.0 BRL 2070-13092 11
m,p-Xylenes ug/L38110 400.0 BRL 2070-13095 9
Methyl Butyl Ketone (2-Hexanone)ug/L15910 200.0 BRL 2060-14079 6
Methyl Ethyl Ketone (2-Butanone)ug/L16150 200.0 BRL 2060-14081 9
Methyl Isobutyl Ketone ug/L13710 200.0 BRL 2060-14069 10
Methylene Chloride ug/L17520 200.0 BRL 2070-13087 8
Methyl-tert-Butyl Ether ug/L16610 200.0 BRL 2070-13083 8
Naphthalene ug/L18010 200.0 BRL 2070-13090 6
n-Butylbenzene ug/L1665.0 200.0 BRL 2170-13083 13
n-Propylbenzene ug/L1835.0 200.0 BRL 1870-13092 10
o-Xylene ug/L1785.0 200.0 BRL 2070-13089 9
sec-Butylbenzene ug/L1665.0 200.0 BRL 2070-13083 10
Styrene ug/L1825.0 200.0 BRL 2070-13091 8
tert-Butylbenzene ug/L1825.0 200.0 BRL 2070-13091 10
Tetrachloroethylene ug/L1865.0 200.0 BRL 2070-13093 8
Toluene ug/L1575.0 200.0 BRL 2070-13078 11
trans-1,2-Dichloroethylene ug/L1735.0 200.0 BRL 2070-13087 8
trans-1,3-Dichloropropylene ug/L1505.0 200.0 BRL 2070-13075 9
Trichloroethylene ug/L1755.0 200.0 BRL 2070-13088 4
Trichlorofluoromethane ug/L2065.0 200.0 BRL 2060-140103 7
Vinyl acetate ug/L18850 200.0 BRL 2060-14094 12
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 53 of 56
3/24/15
Level II QC Report
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Prism Work Order: 5030124
Time Submitted: 3/6/2015 3:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0190 - SM6200 B
Matrix Spike Dup (P5C0190-MSD1)Prepared: 03/10/15 Analyzed: 03/11/15 Source: 5030124-13
Vinyl chloride ug/L1805.0 200.0 BRL 2060-14090 7
Xylenes, total ug/L55915 600.0 BRL 2070-13093 9
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10451.8
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10251.0
ug/L 50.00 70-130Surrogate: Toluene-d8 10753.5
Sample Extraction Data
Prep Method: SM6200 B
Lab Number Batch Date/TimeInitialFinal
P5C01655030124-01 03/09/15 10:561010mLmL
P5C01655030124-02 03/09/15 10:561010mLmL
P5C01655030124-03 03/09/15 10:561010mLmL
P5C01655030124-04 03/09/15 10:561010mLmL
P5C01655030124-05 03/09/15 10:561010mLmL
P5C01655030124-06 03/09/15 10:561010mLmL
P5C01655030124-07 03/09/15 10:561010mLmL
P5C01655030124-08 03/09/15 10:561010mLmL
P5C01655030124-09 03/09/15 10:561010mLmL
P5C01655030124-10 03/09/15 10:561010mLmL
P5C01655030124-11 03/09/15 10:561010mLmL
P5C01655030124-12 03/09/15 10:561010mLmL
P5C01905030124-13 03/10/15 10:491010mLmL
P5C01905030124-14 03/10/15 10:491010mLmL
P5C01905030124-15 03/10/15 10:491010mLmL
P5C01905030124-16 03/10/15 10:491010mLmL
P5C01905030124-17 03/10/15 10:491010mLmL
P5C01905030124-17 03/10/15 10:491010mLmL
P5C01905030124-18 03/10/15 10:491010mLmL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 54 of 56
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APPENDIX B

503 Industrial Ave • Greensboro, NC 27406 Phone [phone] • Fax [phone] • Toll Free [phone]
Email: [e-mail]
May 21, 2015 James McMillan Sent Via email: [e-mail]

RE: Supply Well Analytical Results 2765 Union Ridge Road, Burlington, NC NCDENR Incident #12913 Former Harold Smith Grocery Pyramid Project 2014-238
Dear Mr. McMillan:

As directed by the NCDENR and T.A.C., Inc., Pyramid Environmental has continued to collect samples
from the Point-of-Entry (POE) treatment system that is connected to your water supply well. The work is
being performed as part of the ongoing assessment of the referenced underground storage tank release.
The results of the water analyses are presented below.

On March 4, 2015, Pyramid collected influent and effluent samples from the POE connected to your
supply well. The samples are designated as SW2765 INF and SW2765 EFF. The groundwater samples
were analyzed at a State certified laboratory and the results are attached for your review. The laboratory
results indicate that the POE influent (untreated water) contained methyl tert-butyl ether (MTBE) at a
concentration of 80 parts per billion (PPB). The current North Carolina drinking water standard for
MTBE is 20 PPB. The compound IPE was detected at 100 PPB. The current North Carolina drinking
water standard for IPE is 70 PPB. The compound 1,2-dichloroethane was detected at 16 PPB. The current
North Carolina drinking water standard for 1,2-dichloroethane is 0.4 PPB. No other targeted compounds
were detected at concentrations that exceeded the laboratory detection limits in the POE influent. The laboratory results of the POE effluent sample (treated water) collected on March 4, 2015 indicate that none of the targeted petroleum compounds were detected at concentrations that exceed the laboratory detection limits. The POE worked to remove petroleum contaminants prior to water use.
Maintenance of the POE treatment system will continue to be performed on a quarterly basis.

If you have any questions, please call Pyramid at [phone]. Thank you for your cooperation with
this project.

Sincerely,
Brett S. Higgins
Project Manager

Attachments – Laboratory Report
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765INF
Prism Sample ID: 5030124-07
Prism Work Order: 5030124
Time Collected: 03/04/15 13:00
Time Submitted: 03/06/15 15:45
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 23:46 VHLug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0761,2-Dichlorobenzene
15 SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.111,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5C016512.0 3/9/15 23:46 VHLug/L 0.112,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0662-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0504-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5C01651103/9/15 23:46 VHLug/L 0.31Acetone
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.048Benzene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.057Bromobenzene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.14Bromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.062Bromodichloromethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.040Bromoform
BRL SM6200 B P5C016511.0 3/9/15 23:46 VHLug/L 0.18Bromomethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.062Chlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.22Chloroethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.076Chloroform
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.079Chloromethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.081Dibromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.065Dibromomethane
BRL SM6200 B P5C016511.0 3/9/15 23:46 VHLug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5C016512003/9/15 23:46 VHLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765INF
Prism Sample ID: 5030124-07
Prism Work Order: 5030124
Time Collected: 03/04/15 13:00
Time Submitted: 03/06/15 15:45
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.061Ethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 23:46 VHLug/L 0.16Hexachlorobutadiene
100 SM6200 B P5C0165100503/9/15 23:46 VHLug/L 5.0Isopropyl Ether
0.63 SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5C016511.0 3/9/15 23:46 VHLug/L 0.12m,p-Xylenes
BRL SM6200 B P5C016511.0 3/9/15 23:46 VHLug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5C016515.0 3/9/15 23:46 VHLug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5C016511.0 3/9/15 23:46 VHLug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5C016512.0 3/9/15 23:46 VHLug/L 0.083Methylene Chloride
80 SM6200 B P5C016511.0 3/9/15 23:46 VHLug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5C016511.0 3/9/15 23:46 VHLug/L 0.19Naphthalene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.076n-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.087n-Propylbenzene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.044o-Xylene
0.98 SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.076sec-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.047Styrene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.088tert-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.098Tetrachloroethylene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.044Toluene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.078Trichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5C016515.0 3/9/15 23:46 VHLug/L 0.060Vinyl acetate
BRL SM6200 B P5C016510.50 3/9/15 23:46 VHLug/L 0.097Vinyl chloride
BRL SM6200 B P5C016511.5 3/9/15 23:46 VHLug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130104 %4-Bromofluorobenzene
70-130103 %Dibromofluoromethane
70-130104 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765MID
Prism Sample ID: 5030124-08
Prism Work Order: 5030124
Time Collected: 03/04/15 13:10
Time Submitted: 03/06/15 15:45
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 20:18 VHLug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.111,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5C016512.0 3/9/15 20:18 VHLug/L 0.112,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0662-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0504-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5C01651103/9/15 20:18 VHLug/L 0.31Acetone
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.048Benzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.057Bromobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.14Bromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.062Bromodichloromethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.040Bromoform
BRL SM6200 B P5C016511.0 3/9/15 20:18 VHLug/L 0.18Bromomethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.062Chlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.22Chloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.076Chloroform
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.079Chloromethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.081Dibromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.065Dibromomethane
BRL SM6200 B P5C016511.0 3/9/15 20:18 VHLug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5C016512003/9/15 20:18 VHLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765MID
Prism Sample ID: 5030124-08
Prism Work Order: 5030124
Time Collected: 03/04/15 13:10
Time Submitted: 03/06/15 15:45
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.061Ethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 20:18 VHLug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.050Isopropyl Ether
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5C016511.0 3/9/15 20:18 VHLug/L 0.12m,p-Xylenes
BRL SM6200 B P5C016511.0 3/9/15 20:18 VHLug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5C016515.0 3/9/15 20:18 VHLug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5C016511.0 3/9/15 20:18 VHLug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5C016512.0 3/9/15 20:18 VHLug/L 0.083Methylene Chloride
BRL SM6200 B P5C016511.0 3/9/15 20:18 VHLug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5C016511.0 3/9/15 20:18 VHLug/L 0.19Naphthalene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.076n-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.087n-Propylbenzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.044o-Xylene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.076sec-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.047Styrene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.088tert-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.098Tetrachloroethylene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.044Toluene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.078Trichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5C016515.0 3/9/15 20:18 VHLug/L 0.060Vinyl acetate
BRL SM6200 B P5C016510.50 3/9/15 20:18 VHLug/L 0.097Vinyl chloride
BRL SM6200 B P5C016511.5 3/9/15 20:18 VHLug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130110 %4-Bromofluorobenzene
70-130108 %Dibromofluoromethane
70-130106 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765EFF
Prism Sample ID: 5030124-09
Prism Work Order: 5030124
Time Collected: 03/04/15 13:20
Time Submitted: 03/06/15 15:45
Volatile Organic Compounds by GC/MS
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.111,1,1,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0611,1,1-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0361,1,2,2-Tetrachloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0661,1,2-Trichloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0831,1-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0831,1-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0511,1-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.401,2,3-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.141,2,3-Trichloropropane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.131,2,4-Trichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0541,2,4-Trimethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 20:44 VHLug/L 0.171,2-Dibromo-3-chloropropane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0511,2-Dibromoethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0761,2-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0661,2-Dichloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.111,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0761,3,5-Trimethylbenzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0541,3-Dichlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0431,3-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0501,4-Dichlorobenzene
BRL SM6200 B P5C016512.0 3/9/15 20:44 VHLug/L 0.112,2-Dichloropropane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0662-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0504-Chlorotoluene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.0894-Isopropyltoluene
BRL SM6200 B P5C01651103/9/15 20:44 VHLug/L 0.31Acetone
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.048Benzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.057Bromobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.14Bromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.062Bromodichloromethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.040Bromoform
BRL SM6200 B P5C016511.0 3/9/15 20:44 VHLug/L 0.18Bromomethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.11Carbon Tetrachloride
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.062Chlorobenzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.22Chloroethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.076Chloroform
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.079Chloromethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.056cis-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.079cis-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.081Dibromochloromethane
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.065Dibromomethane
BRL SM6200 B P5C016511.0 3/9/15 20:44 VHLug/L 0.11Dichlorodifluoromethane
BRL SM6200 B P5C016512003/9/15 20:44 VHLug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 56
Laboratory Report
03/24/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
PO Box 16265
Project: Harold SmithPyramid Environmental, Inc
Greensboro, NC 27416-0265
Attn: Brett Higgins
Sample Matrix: Water
Client Sample ID: 2765EFF
Prism Sample ID: 5030124-09
Prism Work Order: 5030124
Time Collected: 03/04/15 13:20
Time Submitted: 03/06/15 15:45
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.061Ethylbenzene
BRL SM6200 B P5C016512.0 3/9/15 20:44 VHLug/L 0.16Hexachlorobutadiene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.050Isopropyl Ether
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.054Isopropylbenzene (Cumene)
BRL SM6200 B P5C016511.0 3/9/15 20:44 VHLug/L 0.12m,p-Xylenes
BRL SM6200 B P5C016511.0 3/9/15 20:44 VHLug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL SM6200 B P5C016515.0 3/9/15 20:44 VHLug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL SM6200 B P5C016511.0 3/9/15 20:44 VHLug/L 0.078Methyl Isobutyl Ketone
BRL SM6200 B P5C016512.0 3/9/15 20:44 VHLug/L 0.083Methylene Chloride
BRL SM6200 B P5C016511.0 3/9/15 20:44 VHLug/L 0.042Methyl-tert-Butyl Ether
BRL SM6200 B P5C016511.0 3/9/15 20:44 VHLug/L 0.19Naphthalene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.076n-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.087n-Propylbenzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.044o-Xylene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.076sec-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.047Styrene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.088tert-Butylbenzene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.098Tetrachloroethylene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.044Toluene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.070trans-1,2-Dichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.12trans-1,3-Dichloropropylene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.078Trichloroethylene
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.062Trichlorofluoromethane
BRL SM6200 B P5C016515.0 3/9/15 20:44 VHLug/L 0.060Vinyl acetate
BRL SM6200 B P5C016510.50 3/9/15 20:44 VHLug/L 0.097Vinyl chloride
BRL SM6200 B P5C016511.5 3/9/15 20:44 VHLug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130109 %4-Bromofluorobenzene
70-130107 %Dibromofluoromethane
70-130108 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 56

APPENDIX C
Summary of System Installation, Start-up, and Operation Activities
Harold Smith Remediation System
January - March 2015

January 21, 2015 System was operational at arrival. The technician checked the system and
performed regular operational and maintenance tasks on the system. The
technician then recorded system operational data and measurements.
System was operational at departure.

February Visit:
January 30, 2015 System was operational at arrival. The technician checked the system,
performed regular operational and maintenance tasks, and recorded system
operations data and measurements. System was operational at departure.

March 11, 2015 System was not operational at arrival. The technician checked the system
and restarted. The technician performed regular operational and
maintenance tasks on the system. The technician then recorded system
operations data and measurements. System was operational at departure.