WS-3891_12913_CA_RMR_20140324

March 24, 2014

Mr. Waddell Watters NC Department of Environment, & Natural Resources
Winston-Salem Regional Office
585 Waughtown Street
Winston-Salem, NC 27107
RE: 1st Quarter 2014 Active Remediation Monitoring Report Harold Smith Grocery, Burlington, North Carolina Incident # 12913

Mr. Watters:
Pyramid Environmental & Engineering, P.C. has completed the Active Remediation Monitoring
Report for the above referenced site. This report was written to summarize the sampling events
and system maintenance for the 1st quarter of 2014.
Please review the enclosed monitoring report. If you have any questions concerning this report,
please call [phone].

Sincerely,

James Cooper Jr., PE Project Engineer

Copy: Mr. Tom Berry, T.A.C., Inc.

P.O. Box 16265 • Greensboro, NC 27416 503 Industrial Ave • Greensboro, NC 27406 Phone [phone] • Fax [phone] • Toll Free [phone] Email: [e-mail] www.pyramidenvironmental.com

TABLE OF CONTENTS

1.0 INTRODUCTION .............................................................................. 1
1.1 SITE INFORMATION ................................................................................................... 1
1.2 ADJOINING PROPERTIES AND POTENTIAL RECEPTORS .............................................. 2
1.3 SITE HYDROLOGY & GEOLOGY ................................................................................ 2
1.4 PREVIOUS REPORTS ................................................................................................. 2
2.0 GROUNDWATER SAMPLING ....................................................... 3
2.1 MONITORING WELL SAMPLING ................................................................................ 3
2.2 POTABLE WATER SUPPLY WELL SAMPLING............................................................. 4
3.0 SYSTEM OPERATIONAL STATUS .............................................. 4
3.1 SYSTEM OPERATIONS ............................................................................................... 4
3.2 CONTAMINATED SOIL REMOVAL .............................................................................. 5
3.3 SYSTEM UPDATE ...................................................................................................... 6
4.0 SOIL & GROUNDWATER ASSESSMENT ................................... 6
4.1 GROUNDWATER ANALYTICAL RESULTS ................................................................... 6
4.2 SUPPLY WELL ANALYTICAL RESULTS...................................................................... 7
5.0 CONCLUSIONS & RECOMMENDATIONS ................................ 7
6.0 CLOSURE ........................................................................................... 8

Page I
TABLE OF CONTENTS (Cont’d)

FIGURES:

1. Topographic Map
2. Site Map
3a. Adjoining Properties and Water Supply Wells
3b. Adjoining Properties and Water Supply Wells
4. Potentiometric Surface Map (3/19/14)
5. BTEX Concentration Map (3/20/14)
6. 1,2-Dichloroethane Isoconcentration Map (3/20/14)

TABLES:

1. Monitoring Well Construction Details
2. Groundwater Elevation Data
3. Monitoring Well Analytical Results
4. Field Measurements – Monitoring Wells
5. Water Supply Well Analytical Results
6. System Operation Parameters

APPENDICES:

A. Groundwater Laboratory Report & Chain of Custody
B. Supply Well Results Letters
C. Recent O&M Activities

Page II
ACTIVE REMEDIATION MONITORING REPORT
Harold Smith Grocery
Burlington, North Carolina

1.0 INTRODUCTION

1.1 Site Information

SITE NAME: Harold Smith Grocery
ADDRESS: 2774 Union Ridge Road
CITY: Burlington, NC
COUNTY: Alamance

CURRENT PROPERTY OWNER: Jessica Alton
CURRENT PROPERTY USE: Inactive Store (used as storage)
OWNER OF USTs: TAC, Inc.
RESPONSIBLE PARTY: TAC, Inc.
NCDENR UST FACILITY ID: 0-024148
GROUNDWATER INCIDENT NO.: 12913
SITE RANKING: H755E

UNDERGROUND STORAGE TANKS (USTs)

(gallons)
1 550 Kerosene Removed 8/01/94
2 550 Gasoline Removed 8/01/94
3 550 Gasoline Removed 8/01/94
4 1,000 Gasoline Removed 8/01/94

FIGURES: Figure 1: Topographic Map
Figure 2: Site Map
Figure 3a: Adjoining Properties and Water Supply Wells
Figure 3b: Adjoining Properties and Water Supply Wells

Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 1 Pyramid Project # 2013-263 4/23/2014
1.2 Adjoining Properties and Potential Receptors

ADJOINING PROPERTY USE: Residential/Agricultural
PUBLIC WATER AVAILABILITY: Unavailable
SUPPLY WELLS WITHIN 1000 FEET: Yes (see Figure 3a/b)
SUPPLY WELLS IMPACTED ABOVE
NCAC 2L STANDARDS: Yes, Supply well at 2765 Union Ridge Rd.
(currently on POE system)

NEAREST SURFACE WATER: Intermittent Creek – 500-600’ SE
BASEMENTS: None
SUBSURFACE UTILITIES: None near source area

1.3 Site Hydrology & Geology

GEOLOGIC PROVINCE: Carolina Slate Belt
BEDROCK TYPE: Felsic Intrusive Complex
DEPTH TO BEDROCK: 25-38 feet BGS (below ground surface)
CURRENT DEPTH TO WATER TABLE: 2.87-9.58 feet BGS (3/19/14)
HISTORIC GW FLUCTUATIONS: Over the past 14 years, the groundwater has
fluctuated in the source area from 5-15 feet BGS
POTENTIOMETRIC GRADIENT: Southeast ~ 0.025 ft. /ft.
HYDRAULIC CONDUCTIVITY (K): 6.17–6.25 x 10-7 ft. /sec.
GROUNDWATER VELOCITY: ~0.4–1.3 feet/year

1.4 Previous Reports

REPORT TITLE

CONSULTANT
DATE OF
REPORT

COMMENTS
Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 2 Pyramid Project # 2013-263 4/23/2014
Soil Cleanup Report Pyramid Environmental 5/31/2011 Received by
NCDENR
Active Remediation
Monitoring Report
Pyramid Environmental 4/8/2013-
2/20/14
Received by
NCDENR
Active Remediation
Monitoring Report
Pyramid Environmental 4/23/14 Current Report

2.0 GROUNDWATER SAMPLING

2.1 Monitoring Well Sampling

SAMPLING DATE: March 20, 2014
WELLS SAMPLED: MW-1A, MW-3, MW-4, MW-5, MW-6, MW-7, MW-9, MW-10,
MW-11, MW-12, MW-13 and MW-15A
LAB ANALYSES: EPA Method 6200B
FIELD ANALYSES: Dissolved oxygen (DO), Temperature, pH, Conductivity,
ORP, Turbidity
FREE PRODUCT: No free product has been observed on this site.

TABLES & GRAPHS: Table 1: Monitoring Well Construction Details
Table 2: Groundwater Elevation Data
Table 3: Monitoring Well Analytical Results
Table 4: Field Measurements – Monitoring Wells

FIGURES: Figure 4: Potentiometric Surface Map
Figure 5: BTEX Concentration Map
Figure 6: 1, 2-Dichloroethane Isoconcentration Map

LABORATORY REPORTS & CHAINS-OF-CUSTODY: Appendix A

FIELD PROCEDURES: Field procedures were performed as outlined in the DENR July 15,
2008 and May 1, 2012 updates publication “Guidelines for
Sampling” under the UST Section.
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2.2 Potable Water Supply Well Sampling

SAMPLING DATE: March 20, 2014
WELLS SAMPLED: 2765 INF, 2765 MID, 2765 EFF, 2760, 2773, 2774, 2779, 2768B
The house at 2779 Union Ridge Road no longer uses the supply
well in the front yard, but uses the well located on an adjacent
eastern property. The property at 2768 Union Ridge Road uses the
supply well in the back yard and is automatically switched to the
well in the front yard (2768-A) if the water level gets too low.

LAB ANALYSES: EPA Method 6200B

TABLES: Table 5: Water Supply Well Analytical Results
FIGURES: Figure 3 a/b: Adjoining Properties and Water Supply Wells.

LABORATORY REPORTS & CHAINS-OF-CUSTODY: Appendix A

FIELD PROCEDURES: Field procedures were performed as outlined in the DENR July 15,
2008 and May 1, 2012 updates publication “Guidelines for
Sampling” under the UST section.

NOTES: Supply wells are named by the address of the residence they serve and not the
property owner. All supply well addresses sampled are on Union Ridge Road.
Letters are shown in Appendix B.
3.0 SYSTEM OPERATIONAL STATUS

3.1 System Operations

The air sparging (AS) and soil vapor extraction (SVE) treatment system for the Harold Smith
Grocery site began operation in July 1999. Various system operation parameters (e.g., SVE
system vacuum and flow, pressure and flow for each of the AS wells, etc.) were recorded during
system operation & maintenance visits. These parameters are summarized in Table 6 with
system operation updates in Appendix C.

The system was restarted in February 2005 and the system was operational through October
2005. Repairs were made to the system and the remediation system was officially restarted on
February 8, 2006. The system ran intermittently during the first quarter of 2006, needing minor
repairs. System operation was interrupted by electrical power interruptions (strong storms)
tripping circuit breakers. These difficulties were resolved and the system was fully operational
during the June and July site visits. In August 2006, the system electrical contacts were found to
be completely melted. The electrical components were replaced after pre-approval, and tested.
The motor of the air-sparge compressor would not operate, and the electric motor was found to
be locked up. Pyramid contacted the equipment manufacturer and priced the replacement items
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necessary to get the air-sparge system running again. The SVE system continued to run after the
replacement of the circuit breakers.

In March 2007 the rebuilt air sparge motor was put back in service. The restored compressor
operated from March 2007 through June 2008. At this time, the air-sparge compressor needed to
be replaced. The air sparge motor was replaced with a more serviceable model on October 7,
2008. The carbon vanes were changed by Pyramid in February 2010. The air sparge system was
operational during the 1st quarter of 2011. The system ceased operating in March 2011 to allow
for the soil excavation. Since the system operation ceased, DO concentrations dropped and
Pyramid recommended continued air sparging operation to speed site cleanup. In January 2012,
the air sparge system was restarted using the selected remaining air sparge wells.

3.2 Contaminated Soil Removal

In March 2009, Pyramid collected risk-based soil samples from several soil borings and added
several monitoring wells. The additional assessment was to investigate the soils in the area of the
former pump island, and provide additional monitoring wells to assess the areas near the source
for incident closure. The highest groundwater concentrations have been in MW-1 throughout the
remediation period. As a result of the additional investigations, an area approximately 40 feet by
20 feet was identified as containing soil concentrations greater than Soil-to-Groundwater
(STGW) standards. Only the soil boring directly at the location of the former pump island
showed concentrations above residential MSCCs. The DENR requested Pyramid to evaluate soil
excavation as a way to help move the site toward regulatory closure. After the excavation plan
was preapproved by the DENR, Pyramid implemented the excavation plan.

In May 2011, Pyramid supervised the excavation of petroleum contaminated soils at the Harold
Smith site in Burlington, NC. The goal of the soil excavation was to remove volatile petroleum
hydrocarbons from the smear zone (between 5 and 15 feet BLS) to help reduce groundwater
contamination. Based on certified weight tickets, 483.69 tons of petroleum-contaminated soil
was removed. The laboratory results of the post excavation soil samples collected indicate that all
of the contaminated soils above the residential MSCCs were removed.

The remaining contamination detected at the site was above the STGW MSCCs and well below
the residential standards. The remaining STGW concentrations were located underneath the store
building, along the northern property boundary, and on the eastern edge of the property near
Union Ridge Road. Because of the structures, roads, and utilities, additional soil excavation was
not feasible or recommended.

After the excavation of contaminated soil, Pyramid installed replacement monitoring wells for
MW-1 and MW-15 to assess the groundwater in the source area. The latest results of these new
wells since (MW-1A and MW-15A) are included in Section 4.0 with past results located in
Table 3.

Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 5 Pyramid Project # 2013-263 4/23/2014
3.3 System Update

To prevent the migration of the contaminant plume, protect nearby supply wells, and speed up
Remediation, the current air sparge (AS) and soil vapor extraction (SVE) system was updated in
October 2012. Additional wells were added to the air sparge segment of the remediation system.
Seven additional air sparge wells were added to surround the existing petroleum contaminant
plume. The additional wells prevent contaminant plume migration and provide additional air
flow for petroleum hydrocarbons volatilization. Along with the AS remediation update, the soil
vapor extraction system was repaired due to the damage the system incurred during soil
excavation in May 2011.
4.0 SOIL & GROUNDWATER ASSESSMENT

4.1 Groundwater Analytical Results

The results of the March 20, 2014 sampling event showed that MW-1A, and MW-10 had
contaminant concentrations above the 2L groundwater standards. The highest concentrations
found for this sampling event are shown below. The MW concentrations above NCAC 2L
groundwater standards are shown in bold and the associated well number is shown in
parentheses(concentrations in micrograms per liter):

• Benzene 0.49 µg/L (MW-1A)
• 1,2-Dichloroethane: 4.8 µg/L (MW-1A)
• BTEX 40.49 µg/L (MW-15A)
• MTBE 140 µg/L (SW-2765)
• IPE 42.2 µg/L (MW-1A)

Over the past 14 years of groundwater and soil remediation, the general concentration trends
demonstrated in the groundwater monitoring wells have been decreasing and are now
approaching regulatory closure.

The benzene concentrations in MW-1A have decreased from over 8,000 µg/L in 1998 to 0.49
µg/L for the current monitoring period. MTBE concentrations in MW-1A have decreased from
610 µg/L in 1999 to 8.6 µg/L for the current monitoring period. Concentrations of 1,2-
dichloroethane were detected in MW-1A and MW-10 above the 2L Standard. The groundwater
concentrations detected after the system update completed in October 2012 are significantly
lower, indicating effective groundwater treatment.

In planning for the soil excavation project, Pyramid recommended that the DENR consider the
placement of oxygen-release compounds in the excavation to help clean up the site. Since
cleanup will have to be to the NCAC 2L Standards, any remedial process that can help reach
regulatory closure more quickly should be considered by the DENR. Pyramid’s request was not
approved for Trust Fund reimbursement, and no oxygen-release compounds were used in the
excavation. In the future, the Trust Fund should consider reimbursing the use of oxygen-release
compounds while excavations are open to help reduce the overall costs for petroleum incident
Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 6 Pyramid Project # 2013-263 4/23/2014
closures. Pyramid implemented several successful oxygen release compound projects at Federal
Trust Fund sites.

Table 4 shows the measured dissolved oxygen (DO) concentrations for the monitoring wells.
Pyramid supervised the reinstallation of the air sparge system with additional air sparge wells
near MW-1A and MW-15A to remediate the remaining petroleum contamination at this high-risk
site. The DO concentrations have increased dramatically since the new air sparge system was
placed into service in April 2013, and the petroleum hydrocarbon concentrations have shown a
rapid reduction. The continued operation and maintenance will continue to reduce the petroleum
contaminant concentrations in the groundwater.

4.2 Supply Well Analytical Results

Supply well sampling was conducted on March 20, 2014 as required by the State. Pyramid
sampled six supply wells 2765, 2760, 2773, 2774, 2779, 2768B. Samples were also collected
from the 2765 mid-fluent and 2765 effluent flows. Samples were collected in laboratory provided
containers using clean, disposable nitrile gloves, packed in ice and shipped to Con-test Analytical
Laboratories for analysis using EPA Method 6200B.

The supply well at address 2765 (SW-2765) was supplied with a Point-of-Entry (POE) treatment
system in 2000. The system has treated the residential potable water for the property through
particulate and carbon treatment since 2000.

Bottled water is being provided to Lassiter (2773). Laboratory analytical results show that there
were no detectable petroleum hydrocarbon concentrations in any of the supply well samples for
2768, 2774, 2760, 2773 and 2779. For the well at 2765, MTBE (140 µg/L), IPE (140 µg/L) and
1,2-Dichloroethane (20 µg/L) were detected above the 2L Groundwater Standard in the influent.
MTBE (0.62µg/L) and IPE (.2 µg/L), both well below the 2L Groundwater Standard, were
detected in the effluent. No benzene was detected in the supply well at 2765 Union Ridge Road
prior to the POE in the past year. Table 5 shows the recent supply well analytical results. A copy
of the laboratory report and chain-of-custody form is presented as Appendix A. Pyramid
recommends continuing sampling all of the supply wells surrounding Harold Smith in June 2014.

5.0 CONCLUSIONS & RECOMMENDATIONS

On behalf of TAC, Inc., Pyramid completed the recent groundwater sampling and air sparge
system operation and maintenance. Based on the current groundwater concentration of 1,2-
Dichloroethane being above the 2L groundwater standard, and the presence of private water
supply wells in the area, the site remains high risk. The remediation goal is to reduce dissolved
groundwater contamination below 2L standards to protect local water supply well users.

• Based on the risk to private well users, Pyramid recommended a new air-sparge system
with deeper air sparge wells to enhance the groundwater cleanup. This new system was
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designed, bid, pre-approved, and built from October 2012 through April 2013. The
system was successfully started on April 3, 2013. The new system has shown significant
reductions in petroleum contaminants.

• The soil excavation was completed in May 2011. Contaminated soil beneath the NC DOT
Right of Way and under the store building was unable to be removed. Because of the
petroleum concentrations remain above STGW levels under the building and near the
roadway, continued soil remediation using the SVE system is recommended.

• Continued groundwater sampling is recommended for the site. The next quarterly
sampling of the monitoring wells will be conducted in June 2014, with a quarterly report
to follow in July 2014.

• The continued presence of concentrations of petroleum contaminants (SW-2765) show
that groundwater contamination remains above regulatory closure levels. Pyramid also
recommends sampling of all of the supply wells surrounding the Harold Smith site. The
next quarterly sampling of the selected supply wells will be in June 2014.

6.0 CLOSURE

This report is prepared for and made available solely for the use of T.A.C, Inc. and the
NCDENR, and the contents thereof may not be used or relied upon by any other person without
the express written consent and authorization of Pyramid Environmental & Engineering, P.C.
The observations, conclusions, and recommendations documented in this report are based on site
conditions and information reviewed at the time of the investigation. Pyramid Environmental &
Engineering, P.C. appreciates the opportunity to provide this environmental service.
Active Remediation Monitoring Report - Harold Smith Grocery, Burlington, NC 8 Pyramid Project # 2013-263 4/23/2014

FIGURES

TABLES

TABLE 1
Monitoring Well Construction Details Harold Smith Grocery Incident #12913
Union Ridge Road, Burlington, North Carolina

MONITORING WELL DATE INSTALLED WELL DEPTH DEPTH TO BEDROCK OUTER CASING RISER INTERVAL SCREEN INTERVAL GROUT INTERVAL BENTONITE INTERVAL SAND INTERVAL
MW-1 11/21/94 20’ NBE NA 0-10’ 10-20’ 0-6’ 6-7.5 7.5-20’
MW-1A 6/27/11 24’ NBE NA 0-4’ 4-24’ 0-1’ 1-3’ 3-24’
MW-2 10/11/95 25’ 25’ NA 0-10’ 10-20’ 0-6’ 6-8’ 8-20’
MW-3 10/11/95 22’ NBE NA 0-7’ 7-22’ 0-3’ 3-5’ 5-22’
MW-4 11/8/95 20’ NBE NA 0-5’ 5-20’ 0-2’ 2-4’ 4-20’
MW-5 11/8/95 20’ NBE NA 0-5’ 5-20’ 0-2’ 2-4’ 4-20’
MW-6 1/2/96 53’ 25’ 0-30’ 0-43’ 43-53’ 0-38’ 38-41’ 41-53’
MW-7 1/3/96 13.8’ NBE NA 0-3.8’ 3.8-13.8’ 0-0.5’ 0.5-1.5’ 1.5-13.8’
MW-8 5/6/96 14.3’ 15’ NA 0-4.3’ 4.3-14.3’ 0-1.8’ 1.8-3.3’ 3.3-14.3’
MW-9 5/6/96 15’ NBE NA 0-5’ 5-15’ 0-2.5’ 2.5-4’ 6/4-15’
MW-10 11/30/99 20’ NBE NA 0-5’ 5-20’ 0.5-2’ 2-4’ 4-20’
MW-11 7/25/00 20’ NA NA 0-5’ 5-20’ 0.5-2’ 2-4’ 4-20’
MW-12 11/6/01 30’ NBE NA 0-10’ 10-30’ 0-6’ 6-8’ 8-30’
MW-13 3/5/09 25’ NBE NA 0-5’ 5-25’ 0-1’ 1-3’ 3-25’
MW-14 3/5/09 25’ NBE NA 0-5’ 5-25’ 0-1’ 1-3’ 3-25’
MW-15 3/5/09 25’ 24’ NA 0-5’ 5-25’ 0-1’ 1-3' 3-25’
MW-15A 6/27/11 24’ NBE NA 0-4’ 4-24’ 0-1’ 1-3’ 3-24’
TS-1 12/17/99 15’ NBE NA 0-5’ 5-15’ 0-2’ 2-4’ 4-15’
TS-2 12/17/99 15’ NBE NA 0-5’ 5-15’ 0-2’ 2-4’ 4-15’
TS-3 12/17/99 15’ NBE NA 0-5’ 5-15’ 0-2’ 2-4’ 4-15’
ALL MONITORING WELLS HAVE 2” PVC CASING/RISER AND 2” PVC SCREEN WITH 0.01” SLOTS. OUTER CASING FOR TYPE III WELL IS 6” PVC.
NBE = NO BEDROCK ENCOUNTERED. NA = NOT APPLICABLE. SHADED WELLS ARE CLOSED.
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
(feet)(feet)(feet) (feet) (feet) (feet) (feet)
MW-1A installed 06-30-11 94.650 12.24 0.00 0.00 0.00 12.24 82.41
09-8-11 94.650 13.59 0.00 0.00 0.00 13.59 81.06
12-8-11 94.650 13.49 0.00 0.00 0.00 13.49 81.16
03-13-12 94.650 13.49 0.00 0.00 0.00 12.35 82.30
06-5-12 94.650 12.14 0.00 0.00 0.00 12.14 82.51
09-11-12 94.650 13.22 0.00 0.00 0.00 13.22 81.43
12-12-12 94.650 13.85 0.00 0.00 0.00 13.85 80.80
03-12-13 94.650 11.83 0.00 0.00 0.00 11.83 82.82
05-29-13 94.650 10.44 0.00 0.00 0.00 10.44 84.21
09-10-13 94.650 8.96 0.00 0.00 0.00 8.96 85.69
11-6-13 94.650 10.96 0.00 0.00 0.00 10.96 83.69
03-19-14 94.650 8.07 0.00 0.00 0.00 8.07 86.58
MW-3 09-9-09 93.065 12.03 0.00 0.00 0.00 12.03 81.04
12-3-09 93.065 10.40 0.00 0.00 0.00 10.40 82.67
03-24-10 93.065 7.34 0.00 0.00 0.00 7.34 85.73
06-24-10 93.065 8.07 0.00 0.00 0.00 8.07 85.00
09-8-10 93.065 9.62 0.00 0.00 0.00 9.62 83.45
12-10-10 93.065 10.77 0.00 0.00 0.00 10.77 82.30
03-8-11 93.065 10.60 0.00 0.00 0.00 10.60 82.47
06-30-11 93.065 10.74 0.00 0.00 0.00 10.74 82.33
09-8-11 93.065 12.16 0.00 0.00 0.00 12.16 80.91
12-8-11 93.065 12.06 0.00 0.00 0.00 12.06 81.01
03-13-12 93.065 13.49 0.00 0.00 0.00 10.52 82.55
06-5-12 93.065 10.71 0.00 0.00 0.00 10.71 82.36
09-11-12 93.065 11.79 0.00 0.00 0.00 11.79 81.28
12-12-12 93.065 12.37 0.00 0.00 0.00 12.37 80.70
03-12-13 93.065 10.53 0.00 0.00 0.00 10.53 82.54
05-29-13 93.065 9.04 0.00 0.00 0.00 9.04 84.03
09-10-13 93.065 7.53 0.00 0.00 0.00 7.53 85.54
11-6-13 93.065 8.88 0.00 0.00 0.00 8.88 84.19
03-19-14 93.065 6.69 0.00 0.00 0.00 6.69 86.38
MW-4 09-9-09 91.470 10.81 0.00 0.00 0.00 10.81 80.66
12-3-09 91.470 9.11 0.00 0.00 0.00 9.11 82.36
03-24-10 91.470 6.10 0.00 0.00 0.00 6.10 85.37
06-24-10 91.470 6.76 0.00 0.00 0.00 6.76 84.71
09-8-10 91.470 8.41 0.00 0.00 0.00 8.41 83.06
12-10-10 91.470 9.55 0.00 0.00 0.00 9.55 81.92
03-8-11 91.470 9.37 0.00 0.00 0.00 9.37 82.10
06-30-11 91.470 9.53 0.00 0.00 0.00 9.53 81.94
09-8-11 91.470 11.12 0.00 0.00 0.00 11.12 80.35
12-8-11 91.470 10.81 0.00 0.00 0.00 10.81 80.66
03-13-12 91.470 13.49 0.00 0.00 0.00 8.58 82.89
06-5-12 91.470 9.50 0.00 0.00 0.00 9.50 81.97
09-11-12 91.470 10.67 0.00 0.00 0.00 10.67 80.80
12-12-12 91.470 11.15 0.00 0.00 0.00 11.15 80.32
03-12-13 91.470 8.84 0.00 0.00 0.00 8.84 82.63
05-29-13 91.470 7.80 0.00 0.00 0.00 7.80 83.67
09-10-13 91.470 6.33 0.00 0.00 0.00 6.33 85.14
11-6-13 91.470 7.70 0.00 0.00 0.00 7.70 83.77
03-19-14 91.470 5.51 0.00 0.00 0.00 5.51 85.96
MW-5 09-9-09 95.045 12.81 0.00 0.00 0.00 12.81 82.24
12-3-09 95.045 6.35 0.00 0.00 0.00 6.35 88.70
03-24-10 95.045 6.63 0.00 0.00 0.00 6.63 88.42
06-24-10 95.045 8.25 0.00 0.00 0.00 8.25 86.80
09-8-10 95.045 10.34 0.00 0.00 0.00 10.34 84.71
12-10-10 95.045 9.78 0.00 0.00 0.00 9.78 85.27
03-8-11 95.045 7.20 0.00 0.00 0.00 7.20 87.85
06-30-11 95.045 8.53 0.00 0.00 0.00 8.53 86.52
09-8-11 95.045 12.62 0.00 0.00 0.00 12.62 82.43
12-8-11 95.045 8.74 0.00 0.00 0.00 8.74 86.31
03-13-12 95.045 13.49 0.00 0.00 0.00 10.94 84.11
06-5-12 95.045 10.87 0.00 0.00 0.00 10.87 84.18
09-11-12 95.045 11.98 0.00 0.00 0.00 11.98 83.07
12-12-12 95.045 13.20 0.00 0.00 0.00 13.20 81.85
03-12-13 95.045 7.32 0.00 0.00 0.00 7.32 87.73
05-29-13 95.045 9.38 0.00 0.00 0.00 9.38 85.67
09-10-13 95.045 8.16 0.00 0.00 0.00 8.16 86.89
11-6-13 95.045 9.53 0.00 0.00 0.00 9.53 85.52
03-19-14 95.045 2.87 0.00 0.00 0.00 2.87 92.18
MW-6*09-9-09 94.935 14.28 0.00 0.00 0.00 14.28 80.66
12-3-09 94.935 12.98 0.00 0.00 0.00 12.98 81.96
03-24-10 94.935 9.07 0.00 0.00 0.00 9.07 85.87
06-24-10 94.935 9.90 0.00 0.00 0.00 9.90 85.04
09-8-10 94.935 11.76 0.00 0.00 0.00 11.76 83.18
12-10-10 94.935 12.91 0.00 0.00 0.00 12.91 82.03
03-8-11 94.935 12.89 0.00 0.00 0.00 12.89 82.05
06-30-11 94.935 12.91 0.00 0.00 0.00 12.91 82.03
09-8-11 94.935 14.50 0.00 0.00 0.00 14.50 80.44
12-8-11 94.935 14.20 0.00 0.00 0.00 14.20 80.74
03-13-12 94.935 13.49 0.00 0.00 0.00 12.94 82.00
06-5-12 94.935 13.10 0.00 0.00 0.00 13.10 81.84
09-11-12 94.935 14.26 0.00 0.00 0.00 14.26 80.68
12-12-12 94.935 14.58 0.00 0.00 0.00 14.58 80.36
03-12-13 94.935 12.72 0.00 0.00 0.00 12.72 82.22
05-29-13 94.935 11.38 0.00 0.00 0.00 11.38 83.56
09-10-13 94.935 9.65 0.00 0.00 0.00 9.65 85.29
11-6-13 94.935 11.29 0.00 0.00 0.00 11.29 83.65
03-19-14 94.935 8.58 0.00 0.00 0.00 8.58 86.36
TABLE 2
Union Ridge Road, Burlington, North carolina
Groundwater Elevation Data
Harold Smith GroceryIncident #12913
Page 1 of 3
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
(feet)(feet)(feet) (feet) (feet) (feet) (feet)
TABLE 2
Union Ridge Road, Burlington, North carolina
Groundwater Elevation Data
Harold Smith GroceryIncident #12913
MW-7 09-9-09 94.215 11.61 0.00 0.00 0.00 11.61 82.61
12-3-09 94.215 9.65 0.00 0.00 0.00 9.65 84.57
03-24-10 94.215 7.69 0.00 0.00 0.00 7.69 86.53
06-24-10 94.215 7.55 0.00 0.00 0.00 7.55 86.67
09-8-10 94.215 8.18 0.00 0.00 0.00 8.18 86.04
12-10-10 94.215 10.36 0.00 0.00 0.00 10.36 83.86
03-8-11 94.215 9.94 0.00 0.00 0.00 9.94 84.28
06-30-11 94.215 10.92 0.00 0.00 0.00 10.92 83.30
09-8-11 94.215 12.05 0.00 0.00 0.00 12.05 82.17
12-8-11 94.215 11.64 0.00 0.00 0.00 11.64 82.58
03-13-12 94.215 13.49 0.00 0.00 0.00 10.75 83.47
06-5-12 94.215 10.63 0.00 0.00 0.00 10.63 83.59
09-11-12 94.215 11.33 0.00 0.00 0.00 11.33 82.89
12-12-12 94.215 12.20 0.00 0.00 0.00 12.20 82.02
03-12-13 94.215 NG 0.00 0.00 0.00 0.00 NG
05-29-13 94.215 NG 0.00 0.00 0.00 0.00 NG
09-10-13 94.215 7.57 0.00 0.00 0.00 7.57 86.65
11-6-13 94.215 9.08 0.00 0.00 0.00 7.57 86.65
03-19-14 94.215 6.95 0.00 0.00 0.00 7.57 86.65
MW-8 09-9-09 89.630 NG 0.00 0.00 0.00 0.00 NG
12-3-09 89.630 7.23 0.00 0.00 0.00 7.23 82.40
03-24-10 89.630 5.64 0.00 0.00 0.00 5.64 83.99
06-24-10 89.630 6.13 0.00 0.00 0.00 6.13 83.50
09-8-10 89.630 7.79 0.00 0.00 0.00 7.79 81.84
12-10-10 89.630 9.43 0.00 0.00 0.00 9.43 80.20
03-8-11 89.630 8.39 0.00 0.00 0.00 8.39 81.24
06-30-11 89.630 NG 0.00 0.00 0.00 0.00 NG
09-8-11 89.630 NG 0.00 0.00 0.00 0.00 NG
12-8-11 89.630 NG 0.00 0.00 0.00 0.00 NG
03-13-12 89.630 NG 0.00 0.00 0.00 0.00 NG
06-5-12 89.630 8.80 0.00 0.00 0.00 8.80 80.83
09-11-12 89.630 9.84 0.00 0.00 0.00 9.84 79.79
12-12-12 89.630 10.60 0.00 0.00 0.00 10.60 79.03
03-12-13 89.630 NG 0.00 0.00 0.00 0.00 NG
05-29-13 89.630 NG 0.00 0.00 0.00 0.00 NG
09-10-13 89.630 NG 0.00 0.00 0.00 0.00 NG
11-6-13 89.630 NG 0.00 0.00 0.00 0.00 NG
03-19-14 89.630 NG 0.00 0.00 0.00 0.00 NG
MW-9 09-9-09 94.770 14.21 0.00 0.00 0.00 14.21 80.56
12-3-09 94.770 12.76 0.00 0.00 0.00 12.76 82.01
03-24-10 94.770 8.91 0.00 0.00 0.00 8.91 85.86
06-24-10 94.770 9.79 0.00 0.00 0.00 9.79 84.98
09-8-10 94.770 11.70 0.00 0.00 0.00 11.70 83.07
12-10-10 94.770 12.89 0.00 0.00 0.00 12.89 81.88
03-8-11 94.770 12.79 0.00 0.00 0.00 12.79 81.98
06-30-11 94.770 NG 0.00 0.00 0.00 0.00 NG
09-8-11 94.770 14.34 0.00 0.00 0.00 14.34 80.43
12-8-11 94.770 14.09 0.00 0.00 0.00 14.09 80.68
03-13-12 94.770 13.49 0.00 0.00 0.00 11.82 82.95
06-5-12 94.770 NG 0.00 0.00 0.00 0.00 NG
09-11-12 94.770 14.15 0.00 0.00 0.00 14.15 80.62
12-12-12 94.770 NG 0.00 0.00 0.00 0.00 NG
03-12-13 94.770 12.60 0.00 0.00 0.00 12.60 82.17
05-29-13 94.770 11.20 0.00 0.00 0.00 11.20 83.57
09-10-13 94.770 9.50 0.00 0.00 0.00 9.50 85.27
11-6-13 94.770 11.16 0.00 0.00 0.00 11.16 83.61
03-19-14 94.770 8.18 0.00 0.00 0.00 8.18 86.59
MW-10 09-9-09 93.210 13.25 0.00 0.00 0.00 13.25 79.96
12-3-09 93.210 10.51 0.00 0.00 0.00 10.51 82.70
03-24-10 93.210 7.80 0.00 0.00 0.00 7.80 85.41
06-24-10 93.210 8.77 0.00 0.00 0.00 8.77 84.44
09-8-10 93.210 10.74 0.00 0.00 0.00 10.74 82.47
12-10-10 93.210 12.15 0.00 0.00 0.00 12.15 81.06
03-8-11 93.210 11.78 0.00 0.00 0.00 11.78 81.43
06-30-11 93.210 12.29 0.00 0.00 0.00 12.29 80.92
09-8-11 93.210 13.39 0.00 0.00 0.00 13.39 79.82
12-8-11 93.210 12.91 0.00 0.00 0.00 12.91 80.30
03-13-12 93.210 13.49 0.00 0.00 0.00 11.61 81.60
06-5-12 93.210 11.79 0.00 0.00 0.00 11.79 81.42
09-11-12 93.210 13.10 0.00 0.00 0.00 13.10 80.11
12-12-12 93.210 13.29 0.00 0.00 0.00 13.29 79.92
03-12-13 93.210 10.93 0.00 0.00 0.00 10.93 82.28
05-29-13 93.210 10.03 0.00 0.00 0.00 10.03 83.18
09-10-13 93.210 8.61 0.00 0.00 0.00 8.61 84.60
11-6-13 93.210 10.11 0.00 0.00 0.00 10.11 83.10
03-19-14 93.210 6.68 0.00 0.00 0.00 6.68 86.53
MW-11 09-9-09 95.840 NG 0.00 0.00 0.00 0.00 NG
12-3-09 95.840 14.05 0.00 0.00 0.00 14.05 81.79
03-24-10 95.840 10.06 0.00 0.00 0.00 10.06 85.78
06-24-10 95.840 10.91 0.00 0.00 0.00 10.91 84.93
09-8-10 95.840 12.77 0.00 0.00 0.00 12.77 83.07
12-10-10 95.840 14.00 0.00 0.00 0.00 14.00 81.84
03-8-11 95.840 13.94 0.00 0.00 0.00 13.94 81.90
06-30-11 95.840 13.92 0.00 0.00 0.00 13.92 81.92
09-8-11 95.840 15.52 0.00 0.00 0.00 15.52 80.32
12-8-11 95.840 15.21 0.00 0.00 0.00 15.21 80.63
03-13-12 95.840 13.49 0.00 0.00 0.00 13.94 81.90
06-5-12 95.840 14.16 0.00 0.00 0.00 14.16 81.68
09-11-12 95.840 15.36 0.00 0.00 0.00 15.36 80.48
12-12-12 95.840 15.60 0.00 0.00 0.00 15.60 80.24
03-12-13 95.840 13.88 0.00 0.00 0.00 13.88 81.96
05-29-13 95.840 12.35 0.00 0.00 0.00 12.35 83.49
09-10-13 95.840 10.64 0.00 0.00 0.00 10.64 85.20
11-6-13 95.840 12.35 0.00 0.00 0.00 12.35 83.49
03-19-14 95.840 9.58 0.00 0.00 0.00 9.58 86.26
Page 2 of 3
TOC Depth Depth Free Free Corrected Corrected
Well Date Elevation To To Product Product Depth To Water
Number Gauged Groundwater Product Thickness Adjustment Water Elevation
(feet)(feet)(feet) (feet) (feet) (feet) (feet)
TABLE 2
Union Ridge Road, Burlington, North carolina
Groundwater Elevation Data
Harold Smith GroceryIncident #12913
MW-12 09-9-09 94.270 14.70 0.00 0.00 0.00 14.70 79.57
12-3-09 94.270 13.45 0.00 0.00 0.00 13.45 80.82
03-24-10 94.270 9.50 0.00 0.00 0.00 9.50 84.77
06-24-10 94.270 10.36 0.00 0.00 0.00 10.36 83.91
09-8-10 94.270 12.26 0.00 0.00 0.00 12.26 82.01
12-10-10 94.270 13.43 0.00 0.00 0.00 13.43 80.84
03-8-11 94.270 13.35 0.00 0.00 0.00 13.35 80.92
06-30-11 94.270 13.42 0.00 0.00 0.00 13.42 80.85
09-8-11 94.270 15.05 0.00 0.00 0.00 15.05 79.22
12-8-11 94.270 14.66 0.00 0.00 0.00 14.66 79.61
03-13-12 94.270 13.49 0.00 0.00 0.00 13.43 80.84
06-5-12 94.270 13.58 0.00 0.00 0.00 13.58 80.69
09-11-12 94.270 14.79 0.00 0.00 0.00 14.79 79.48
12-12-12 94.270 15.04 0.00 0.00 0.00 15.04 79.23
03-12-13 94.270 13.24 0.00 0.00 0.00 13.24 81.03
05-29-13 94.270 11.79 0.00 0.00 0.00 11.79 82.48
09-10-13 94.270 10.08 0.00 0.00 0.00 10.08 84.19
11-6-13 94.270 11.73 0.00 0.00 0.00 11.73 82.54
03-19-14 94.270 8.92 0.00 0.00 0.00 8.92 85.35
MW-13 03-18-09 94.805 13.58 0.00 0.00 0.00 13.58 81.23
06-23-09 94.805 11.01 0.00 0.00 0.00 11.01 83.80
09-9-09 94.805 12.61 0.00 0.00 0.00 12.61 82.20
12-3-09 94.805 11.26 0.00 0.00 0.00 11.26 83.55
03-24-10 94.805 7.92 0.00 0.00 0.00 7.92 86.89
06-24-10 94.805 10.56 0.00 0.00 0.00 10.56 84.25
09-8-10 94.805 9.82 0.00 0.00 0.00 9.82 84.99
12-10-10 94.805 10.93 0.00 0.00 0.00 10.93 83.88
03-8-11 94.805 11.24 0.00 0.00 0.00 11.24 83.57
06-30-11 94.805 10.73 0.00 0.00 0.00 10.73 84.08
09-8-11 94.805 12.51 0.00 0.00 0.00 12.51 82.30
12-8-11 94.805 12.69 0.00 0.00 0.00 12.69 82.12
03-13-12 94.805 13.49 0.00 0.00 0.00 10.48 84.33
06-5-12 94.805 10.28 0.00 0.00 0.00 10.28 84.53
09-11-12 94.805 11.55 0.00 0.00 0.00 11.55 83.26
12-12-12 94.805 13.55 0.00 0.00 0.00 13.55 81.26
03-12-13 94.805 10.33 0.00 0.00 0.00 10.33 84.48
05-29-13 94.805 9.41 0.00 0.00 0.00 9.41 85.40
09-10-13 94.805 7.78 0.00 0.00 0.00 7.78 87.03
11-6-13 94.805 9.36 0.00 0.00 0.00 9.36 85.45
03-19-14 94.805 6.88 0.00 0.00 0.00 6.88 87.93
MW-14 03-18-09 94.395 NG 0.00 0.00 0.00 0.00 NG
06-23-09 94.395 NG 0.00 0.00 0.00 0.00 NG
09-9-09 94.395 NG 0.00 0.00 0.00 0.00 NG
12-3-09 94.395 NG 0.00 0.00 0.00 0.00 NG
03-24-10 94.395 NG 0.00 0.00 0.00 0.00 NG
06-24-10 94.395 NG 0.00 0.00 0.00 0.00 NG
09-8-10 94.395 NG 0.00 0.00 0.00 0.00 NG
12-10-10 94.395 NG 0.00 0.00 0.00 0.00 NG
03-8-11 94.395 NG 0.00 0.00 0.00 0.00 NG
06-30-11 94.395 NG 0.00 0.00 0.00 0.00 NG
09-8-11 94.395 NG 0.00 0.00 0.00 0.00 NG
12-8-11 94.395 NG 0.00 0.00 0.00 0.00 NG
03-13-12 94.395 NG 0.00 0.00 0.00 0.00 NG
06-5-12 94.395 NG 0.00 0.00 0.00 0.00 NG
09-11-12 94.395 NG 0.00 0.00 0.00 0.00 NG
12-12-12 94.395 NG 0.00 0.00 0.00 0.00 NG
03-12-13 94.395 NG 0.00 0.00 0.00 0.00 NG
05-29-13 94.395 NG 0.00 0.00 0.00 0.00 NG
09-10-13 94.395 NG 0.00 0.00 0.00 0.00 NG
11-6-13 94.395 NG 0.00 0.00 0.00 0.00 NG
03-19-14 94.395 NG 0.00 0.00 0.00 0.00 NG
MW-15/03-18-09 93.775 13.77 0.00 0.00 0.00 13.77 80.01
MW-15A 06-23-09 93.775 9.90 0.00 0.00 0.00 9.90 83.88
09-9-09 93.775 11.57 0.00 0.00 0.00 11.57 82.21
12-3-09 93.775 11.24 0.00 0.00 0.00 11.24 82.54
03-24-10 93.775 7.57 0.00 0.00 0.00 7.57 86.21
06-24-10 93.775 8.43 0.00 0.00 0.00 8.43 85.35
09-8-10 93.775 9.67 0.00 0.00 0.00 9.67 84.11
12-10-10 93.775 11.24 0.00 0.00 0.00 11.24 82.54
03-8-11 93.775 11.42 0.00 0.00 0.00 11.42 82.36
06-30-11 94.950 12.47 0.00 0.00 0.00 12.47 82.48
09-8-11 94.950 13.88 0.00 0.00 0.00 13.88 81.07
12-8-11 94.950 13.75 0.00 0.00 0.00 13.75 81.20
03-13-12 94.950 13.49 0.00 0.00 0.00 12.60 82.35
06-5-12 94.950 12.45 0.00 0.00 0.00 12.45 82.50
09-11-12 94.950 13.51 0.00 0.00 0.00 13.51 81.44
12-12-12 94.950 14.08 0.00 0.00 0.00 14.08 80.87
03-12-13 94.950 12.07 0.00 0.00 0.00 12.07 82.88
05-29-13 94.950 8.72 0.00 0.00 0.00 8.72 86.23
09-10-13 94.950 9.17 0.00 0.00 0.00 9.17 85.78
11-6-13 94.950 7.94 0.00 0.00 0.00 7.94 87.01
03-19-14 94.950 8.33 0.00 0.00 0.00 8.33 86.62
Page 3 of 3
PARAMETER UNITS DATE MW-1/ MW-3 MW-4 MW-5 MW-6* MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/ TS-1 NCAC 2L
MW-1A MW-15A Groundwater
Standard
Benzene ug/l 03-14-07 440 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 DNE DNE DNE NS 1
06-06-07 410 <1 <1 <1 3.6 <1 <1 <1 <1 <1 2.4 DNE DNE DNE NS
08-29-07 340 <1 <1 <1 2.6 <1 <1 <1 <1 <1 6.4 DNE DNE DNE NS
12-13-07 200 <1 <1 <1 1.1 <1 <1 <1 <1 <1 9.2 DNE DNE DNE NS
03-14-08 250 <1 <1 <1 24 <1 <1 <1 <1 <1 130 DNE DNE DNE NS
06-18-08 310 <1 <1 <1 NS <1 <1 <1 <1 <1 5.3 DNE DNE DNE NS
09-10-08 <100 <1 <1 <1 11.6 <1 <1 <1 <1 <1 69.5 DNE DNE DNE NS
12-03-08 18 <0.5 <0.5 <0.5 8.7 32 <0.5 <0.5 <0.5 <0.5 41 DNE DNE DNE NS
03-18-09 110 <0.5 1.9 <0.5 <0.5 5.9 <0.5 <0.5 <0.5 <0.5 3.6 <0.5 NS 520 NS
06-23-09 290 <0.5 <0.5 <0.5 <0.5 0.66 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 210 NS
09-09-09 190 <0.5 <0.5 <0.5 <0.5 0.66 NS <0.5 <0.5 NS 5.1 <0.5 NS 910 NS
12-03-09 180 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 7.5 <0.5 NS 440 NS
03-24-10 120 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 55 NS
06-24-10 30 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 98 NS
09-08-10 69.7 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1.1 <0.5 NS 37.5 NS
12-10-10 140 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1.3 <0.5 NS 5.4 NS
03-08-11 120 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 52 NS
06-30-11 18.3 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 77.1 NS
09-08-11 22 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 1.7 <0.5 NS 462 NS
12-09-11 15.4 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 0.61 <0.5 NS 384 NS
03-14-12 20 ND ND ND ND ND NS ND ND ND 0.17J ND NS 290 NS
06-07-12 28 ND ND ND ND ND ND NS ND ND ND ND NS 220 NS
9/11-12/12 30.1 ND ND ND ND ND ND NS ND ND 1.2 ND NS 132 NS
12-12-12 19 ND ND ND ND ND ND NS ND ND 0.81 ND NS 91 NS
03-14-13 20.4 ND ND ND ND NS NS NS ND ND ND ND NS 82.8 NS
05-30-13 0.83 ND ND ND ND NS NS ND ND ND ND ND NS ND NS
09-10-13 5.5 ND ND ND ND ND NS ND ND ND ND ND NS 4.4 NS
11-07-13 0.5 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
09-20-14 0.49 ND ND ND ND ND NS ND ND ND ND ND NS 0.29 NS
Toluene ug/l 03-14-07 3200 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 600
06-06-07 5200 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
08-29-07 6300 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
12-13-07 3300 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-14-08 4400 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
06-18-08 5800 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
09-10-08 1850 <1 <1 <1 <1 <1 2.72 <1 <1 <1 <10 DNE DNE DNE NS
12-03-08 28 <1 <1 <1 <1 140 5.3 <1 <1 <1 <1 DNE DNE DNE NS
03-18-09 3200 <1 <1 <1 <1 50 2.9 <1 <1 <1 <1 <0.5 NS 12000 NS
06-23-09 5700 <1 <1 <1 <1 0.69J 2.9 <1 <1 <1 <1 <1 NS 17000 NS
09-09-09 4300 <1 <1 <1 <1 <1 NS <1 <1 NS <1 <1 NS 25000 NS
12-03-09 3900 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS 30000 NS
03-24-10 3100 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 1600 NS
06-24-10 640 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 6900 NS
09-08-10 1090 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 1630 NS
12-10-10 3100 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 94 NS
03-08-11 1390 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 1940 NS
06-30-11 29.6 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 600 NS
09-08-11 2.1 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 5620 NS
12-09-11 5.9 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 <0.5 <0.5 NS 6820 NS
03-14-12 5.7 ND ND ND ND ND NS ND ND ND ND ND NS 7400 NS
06-07-12 8.2 ND ND ND ND ND ND NS ND ND ND ND NS 6300 NS
9/11-12/12 8.1 ND ND ND ND ND ND NS ND ND ND ND NS 3240 NS
12-12-12 3.3 ND ND ND ND ND ND NS ND ND ND ND NS 3300 NS
03-14-13 5.4 ND ND ND ND NS NS NS ND ND ND ND NS 1860 NS
05-30-13 ND ND ND ND ND NS NS ND ND ND ND ND NS 1.8 NS
09-10-13 7.2 ND ND ND ND ND NS ND ND ND ND ND NS 66.2 NS
11-07-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
09-20-14 0.31 ND ND ND ND ND NS ND ND ND ND ND NS 3 NS
Ethylbenzene ug/l 03-14-07 66 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 600
06-06-07 550 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
08-29-07 760 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
12-13-07 620 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-14-08 580 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
06-18-08 730 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
09-10-08 228 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 DNE DNE DNE NS
12-03-08 21 <1 <1 <1 <1 11 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-18-09 280 <1 <1 <1 <1 16 <1 <1 <1 <1 <1 6.3 NS 930 NS
06-23-09 870 <1 <1 <1 <1 2.5 <1 <1 <1 <1 <1 <1 NS 3000 NS
09-09-09 830 <1 <1 <1 <1 2.1 NS <1 <1 NS <1 <1 NS 2300 NS
12-03-09 990 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS 2700 NS
03-24-10 720 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 160 NS
06-24-10 250 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 1300 NS
09-08-10 625 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 215 NS
12-10-10 700 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 5.1 NS
03-08-11 307 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 198 NS
06-30-11 19.7 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 140 NS
09-08-11 41.9 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 1550 NS
12-09-11 11.8 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 <0.5 <0.5 NS 1740 NS
03-14-12 11 ND ND ND ND ND NS ND ND ND ND ND NS 2200 NS
06-07-12 15 ND ND ND ND ND ND NS ND ND ND ND NS 1900 NS
9/11-12/12 22.5 ND ND ND ND ND ND NS ND ND ND ND NS 1620 NS
12-12-12 21 ND ND ND ND ND ND NS ND ND ND ND NS 1600 NS
03-14-13 13.8 ND ND ND ND NS NS NS ND ND ND ND NS 1440 NS
05-30-13 0.58 ND ND ND ND NS NS ND ND ND ND ND NS 1.7 NS
09-10-13 7.3 ND ND ND ND ND NS ND ND ND ND ND NS 76.8 NS
11-07-13 1.6 ND ND ND ND ND NS ND ND ND ND ND NS 0.88 NS
09-20-14 1.1 ND ND ND ND ND NS ND ND ND ND ND NS 8 NS
Total Xylenes ug/l 03-14-07 5700 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 DNE DNE DNE NS 500.0
06-06-07 7000 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 DNE DNE DNE NS
08-29-07 9600 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 DNE DNE DNE NS
12-13-07 5600 <3 <3 <3 <3 <3 <3 <3 <3 <3 27 DNE DNE DNE NS
03-14-08 6200 <3 <3 <3 <3 <3 <3 <3 <3 <3 16 DNE DNE DNE NS
06-18-08 7800 <3 <3 <3 NS <3 <3 <3 <3 <3 12 DNE DNE DNE NS
09-10-08 2377 <4 <4 <4 <4 <4 <4 <4 <4 <4 <40 DNE DNE DNE NS
12-03-08 610 <3 <3 <3 <3 1810 <3 <3 <3 <3 15 DNE DNE DNE NS
03-18-09 5500 <3 <3 <3 <3 2020 <3 13.6 <3 <3 4.7 2.3 NS 7000 NS
06-23-09 9300 <3 <3 <3 <3 71 <3 <3 <3 <3 <3 <3 NS 22400 NS
09-09-09 8700 <3 <3 <3 <3 30.1 NS <3 <3 NS 3.4 <3 NS 19300 NS
12-03-09 9300 <3 <3 <3 <3 <3 <3 <3 <3 NS 5.8 <3 NS 21200 NS
03-24-10 7800 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 NS 2600 NS
06-24-10 2700 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 NS 11100 NS
09-08-10 5720 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 NS 3790 NS
12-10-10 9700 NS NS <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <1.5 0.61 <1.5 NS 162 NS
03-08-11 5700 <1.5 <1.5 <1.5 <1.5 0.66 <1.5 <1.5 <1.5 <1.5 0.82 <1.5 NS 2124 NS
06-30-11 213.2 <1.5 <1.5 <1.5 <1.5 0.66 NS NS <1.5 <1.5 5.8 <1.5 NS 602 NS
09-08-11 42.4 <1.5 <1.5 <1.5 <1.5 0.66 NS NS <1.5 <1.5 11.6 <1.5 NS 3990 NS
12-09-11 48 <1.5 <1.5 <1.5 <1.5 <1.5 NS <1.5 <1.5 <1.5 0.66 <1.5 NS 5680 NS
03-14-12 44 ND ND ND ND ND NS ND ND ND ND ND NS 8300 NS
06-07-12 60 ND ND ND ND ND ND NS ND ND ND ND NS 7400 NS
9/11-12/12 73.9 ND ND ND ND ND ND NS ND ND ND ND NS 5940 NS
12-12-12 28 ND ND ND ND ND ND NS ND ND ND ND NS 7400 NS
03-14-13 44 ND ND ND ND NS NS NS ND ND ND ND NS 5600 NS
05-30-13 1.94 ND ND ND ND NS NS ND ND ND ND ND NS 7.7 NS
09-10-13 83.1 ND ND ND ND ND NS ND ND ND ND ND NS 470 NS
11-07-13 4.5 ND ND ND ND ND NS ND ND ND ND ND NS 3.76 NS
09-20-14 5.6 ND ND ND ND ND NS ND ND ND ND ND NS 32.2 NS
TABLE 3
Monitoring Well Analytical Results
Incident #12913
Harold Smith Grocer
Union Ridge Road, Burlington, North Carolina
PARAMETER UNITS DATE MW-1/ MW-3 MW-4 MW-5 MW-6* MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/ TS-1 NCAC 2L
MW-1A MW-15A Groundwater
Standard
TABLE 3
Monitoring Well Analytical Results
Incident #12913
Harold Smith Grocer
Union Ridge Road, Burlington, North Carolina
TOTAL BTE ug/l 03-14-07 9406 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL DNE DNE DNE NS N/A
06-06-07 13160 BDL BDL BDL 3.6 BDL BDL BDL BDL BDL 2.4 DNE DNE DNE NS
08-29-07 17000 BDL BDL BDL 2.6 BDL BDL BDL BDL BDL 6.4 DNE DNE DNE NS
12-13-07 9720 BDL BDL BDL BDL BDL BDL BDL BDL BDL 36.2 DNE DNE DNE NS
03-14-08 11430 BDL BDL BDL 24 BDL BDL BDL BDL BDL 146 DNE DNE DNE NS
06-18-08 14640 BDL BDL BDL NS BDL BDL BDL BDL BDL 17.3 DNE DNE DNE NS
09-10-08 4455 BDL BDL BDL 11.6 BDL 2.72 BDL BDL BDL 69.5 DNE DNE DNE NS
12-03-08 677 BDL BDL BDL 8.7 1993 5.3 BDL BDL BDL 56 DNE DNE DNE NS
03-18-09 9090 BDL 1.9 BDL BDL 2091.9 2.9 13.6 BDL BDL 8.3 8.6 NS 20450 NS
06-23-09 16160 BDL BDL BDL BDL 74.16 2.9 BDL BDL BDL BDL BDL NS 42610 NS
09-09-09 14020 BDL BDL BDL BDL 32.86 NS BDL BDL NS 8.5 BDL NS 47510 NS
12-03-09 14370 BRL BRL BRL BRL BRL BRL BRL BRL NS 13.3 BRL NS 54340 NS
03-24-10 11740 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS 4415 NS
06-24-10 3620 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS 19398 NS
09-08-10 7504.7 BRL BRL BRL BRL BRL BRL BRL BRL BRL 1.1 BRL NS 5672.5 NS
12-10-10 13640 NS NS BRL BRL BRL BRL BRL BRL BRL 1.91 BRL NS 266.5 NS
03-08-11 7517 ND ND ND ND 0.66 ND ND ND ND 0.82 ND NS 4314 NS
06-30-11 280.8 ND ND ND ND 0.66 NS NS ND ND 5.8 ND NS 1419.1 NS
09-08-11 108.4 ND ND ND ND 0.66 NS NS ND ND 13.3 ND NS 11622 NS
12-09-11 81.1 ND ND ND ND ND NS ND ND ND 1.27 ND NS 14624 NS
03-14-12 80.7 ND ND ND ND ND NS ND ND ND ND ND NS 18190 NS
06-07-12 111.2 ND ND ND ND ND ND NS ND ND ND ND NS 15820 NS
9/11-12/12 134.6 ND ND ND ND ND ND NS ND ND 1.2 ND NS 10932 NS
12-12-12 71.3 ND ND ND ND 0.2 ND NS ND ND 0.81 ND NS 12391 NS
03-14-13 83.6 ND ND ND ND NS NS NS ND ND ND ND NS 8982.8 NS
05-30-13 3.35 ND ND ND ND NS NS ND ND ND ND ND NS 11.2 NS
09-10-13 103.1 ND ND ND ND ND NS ND ND ND ND ND NS 617.4 NS
11-07-13 6.6 ND ND ND ND ND NS ND ND ND ND ND NS 4.64 NS
09-20-14 7.19 ND ND ND ND ND NS ND ND ND ND ND NS 40.49 NS
Methyl Tertiary ug/l 03-14-07 <50 <5 10 <5 4.3J <5 <5 <5 <5 <5 2.7J DNE DNE DNE NS 20.0
Butyl Ether 06-06-07 <50 19 7.5 <5 5.9 <5 4.9J <5 <5 <5 4.1J DNE DNE DNE NS
(MTBE)08-29-07 <50 73 4.6J <5 7.1 <5 <5 <5 <5 <5 4.1J DNE DNE DNE NS
12-13-07 <50 97 20 <5 8.5 <5 <5 <5 <5 <5 13 DNE DNE DNE NS
03-14-08 <50 10 6.9 <5 16 <5 <5 <5 <5 <5 74 DNE DNE DNE NS
06-18-08 <50 26 27 <5 NS <5 <5 <5 <5 <5 15 DNE DNE DNE NS
09-10-08 <200 2.3 <2 <2 6.39 <2 <2 <2 <2 <2 38.1 DNE DNE DNE NS
12-03-08 <5 2.8J 8.9 <5 9.3 5.1 <5 <5 <5 <5 75 DNE DNE DNE NS
03-18-09 <50 <5 <5 <5 <5 8.2 <5 8.3 <5 <5 25 <0.5 NS <50 NS
06-23-09 <50 <5 5.4 <5 <5 3.3J <5 <5 <5 <5 11 <5 NS <50 NS
09-09-09 <50 <5 7.7 <5 <5 2.6J NS <5 <5 NS 44 <5 NS <200 NS
12-03-09 <50 <5 4J <5 <5 <5 <5 <5 <5 NS 92 <5 NS <200 NS
03-24-10 <50 <5 13 <5 <5 <5 <5 <5 <5 <5 3.3J <5 NS <200 NS
06-24-10 <50 <1 4.2 <1 <1 1.5 <1 <1 <1 <1 13 <1 NS <40 NS
09-08-10 <2.5 <0.5 1.7 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 45.8 <0.5 NS <5 NS
12-10-10 <10 NS NS <1 <1 <1 <1 <1 <1 <1 57 <1 NS <1 NS
03-08-11 <10 <0.5 1.6 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 19.1 <0.5 NS <10 NS
06-30-11 2.7 <0.5 0.83 <0.5 <0.5 <0.5 NS NS 0.51 <0.5 23.8 <0.5 NS <0.5 NS
09-08-11 12.3 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS 0.54 <0.5 54.7 <0.5 NS 2.9 NS
12-09-11 9.2 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 0.52 <0.5 28.5 <0.5 NS <25 NS
03-14-12 9.6 ND 0.5 ND 0.25J ND NS ND 0.84 ND 10 ND NS ND NS
06-07-12 ND ND ND ND ND ND ND NS 1.7 ND 15 ND NS ND NS
9/11-12/12 21.4 ND ND ND ND ND ND NS 2.2 ND 33.8 ND NS ND NS
12-12-12 21 ND ND ND 0.19J ND ND NS 0.32J ND 24 ND NS ND NS
03-14-13 21.3 ND ND ND ND NS NS NS ND ND 8.4 ND NS ND NS
05-30-13 9.4 ND ND ND ND NS NS ND 0.8 ND 2 ND NS 0.61 NS
09-10-13 14.4 ND ND ND ND ND NS ND 2.9 ND 1.9 ND NS ND NS
11-07-13 9.4 ND ND ND ND ND NS ND 2.2 ND 1.2 ND NS ND NS
09-20-14 8.6 ND 0.35 ND 0.16 ND NS 1.1 0.12 ND 1.8 ND NS 0.2 NS
Ethylene ug/l 03-14-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 0.0200
Dibromide 06-06-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
(EDB)08-29-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
12-13-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-14-08 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
06-18-08 <10 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
09-10-08 <2 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 DNE DNE DNE NS
12-03-08 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
03-18-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <0.5 NS <50 NS
06-23-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS <50 NS
09-09-09 <10 <1 <1 <1 <1 <1 NS <1 <1 NS <1 <1 NS <40 NS
12-03-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS <40 NS
03-24-10 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS <40 NS
06-24-10 14 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 28 NS
09-08-10 <2.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS <5 NS
12-10-10 <5 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS 3.9 NS
03-08-11 <10 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS <10 NS
06-30-11 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 1.9 NS
09-08-11 <1.2 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 7 NS
12-09-11 <1 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 <0.5 <0.5 NS <25 NS
03-14-12 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
06-07-12 ND ND ND ND ND ND ND NS ND ND ND ND NS ND NS
9/11-12/12 ND ND ND ND ND ND ND NS ND ND ND ND NS ND NS
12-12-12 ND ND ND ND ND ND ND NS ND ND ND ND NS ND NS
03-14-13 ND ND ND ND ND NS NS NS ND ND ND ND NS ND NS
05-30-13 ND ND ND ND ND NS NS ND ND ND ND ND NS ND NS
09-10-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
11-07-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
09-20-14 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
PARAMETER UNITS DATE MW-1/ MW-3 MW-4 MW-5 MW-6* MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15/ TS-1 NCAC 2L
MW-1A MW-15A Groundwater
Standard
TABLE 3
Monitoring Well Analytical Results
Incident #12913
Harold Smith Grocer
Union Ridge Road, Burlington, North Carolina
Isopropyl Ether ug/l 03-14-08 86 <5 3J <5 9.9 <5 <5 <5 <5 <5 270 DNE DNE DNE NS 70.0
(IPE)06-18-08 <50 <5 13 <5 NS <5 <5 <5 <5 <5 19 DNE DNE DNE NS
09-10-08 <100 <1 <1 <1 9.28 <1 <1 <1 <1 <1 221 DNE DNE DNE NS
12-03-08 15 <5 4.6J <5 6.9 23 <5 8.1 <5 <5 200 DNE DNE DNE NS
03-18-09 <50 <5 <5 <5 <5 19 <5 10 <5 <5 69 <0.5 NS <50 NS
06-23-09 <50 <5 <5 <5 <5 6.2 <5 <5 <5 <5 10 <5 NS <50 NS
09-09-09 <50 <5 3.3J <5 <5 4.9J NS <5 <5 NS 73 <5 NS <200 NS
12-03-09 <50 <5 <5 <5 <5 <5 <5 <5 <5 NS 180 <5 NS <200 NS
03-24-10 <50 <5 5.9 <5 <5 <5 <5 <5 <5 <5 3.2J <5 NS <200 NS
06-24-10 <5 <0.5 1.8 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 12 <0.5 NS <20 NS
09-08-10 2.9 <0.5 0.66 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 35.9 <0.5 NS <5 NS
12-10-10 6 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 49 <0.5 NS 1.3 NS
03-08-11 <10 <0.5 <0.5 <0.5 <0.5 0.56 <0.5 <0.5 0.82 <0.5 24.6 <0.5 NS <10 NS
06-30-11 13 <0.5 <0.5 <0.5 <0.5 0.56 NS NS 1.2 <0.5 29.2 <0.5 NS 2.7 NS
09-08-11 62.2 <0.5 <0.5 <0.5 <0.5 0.56 NS NS 0.73 <0.5 55.2 <0.5 NS 22.5 NS
12-09-11 40.9 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 29.1 <0.5 NS <25 NS
03-14-12 47 ND ND ND ND ND NS ND 0.17J ND 11 ND NS ND NS
06-07-12 78 ND ND ND ND ND ND NS 0.52J ND 12 ND NS 15J NS
9/11-12/12 94.8 ND ND ND ND ND ND NS 1.6 ND 29.8 ND NS 13.5 NS
12-12-12 120 ND ND ND 0.16J ND ND NS 1.6 ND 26 ND NS ND NS
03-14-13 112 ND ND ND ND NS NS NS ND ND 10.2 ND NS ND NS
05-30-13 32.5 ND ND ND ND NS NS 3.1 1.5 ND ND ND NS 1.5 NS
09-10-13 80.7 ND ND ND ND ND NS 3.1 6.9 ND ND ND NS 7.2 NS
11-07-13 42.2 ND ND ND ND ND NS ND 3.1 1.9 ND ND NS 0.79 NS
09-20-14 46 ND ND ND 0.2 ND NS ND 3.1 1.9 0.34 ND NS 1.5 NS
1,2-Dichloroethane ug/l 03-14-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS 0.4
06-06-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
08-29-07 <10 <1 <1 <1 <1 <1 <1 <1 1.4 <1 1.3 DNE DNE DNE NS
12-13-07 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 1.5 DNE DNE DNE NS
03-14-08 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 31 DNE DNE DNE NS
06-18-08 <10 <1 1.3 <1 NS <1 <1 <1 <1 <1 2.8 DNE DNE DNE NS
09-10-08 <2 <1 <1 <1 <1 <1 <1 <1 <1 <1 29.3 DNE DNE DNE NS
12-03-08 <1 <1 <1 <1 <1 4 <1 0.76J <1 <1 30 DNE DNE DNE NS
03-18-09 <10 <1 <1 <1 <1 2.1 <1 1.5 <1 <1 4.5 <0.5 NS <50 NS
06-23-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 0.69J <1 NS <50 NS
09-09-09 <10 <1 <1 <1 <1 0.64J NS <1 <1 NS 8.6 <1 NS <40 NS
12-03-09 <10 <1 <1 <1 <1 <1 <1 <1 <1 NS 13 <1 NS <40 NS
03-24-10 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS <40 NS
06-24-10 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 2.8 <0.5 <0.5 NS <20 NS
09-08-10 <2.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 6.9 <0.5 NS <5 NS
12-10-10 <5 NS NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 11 <0.5 NS <0.5 NS
03-08-11 <10 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 7.1 <0.5 NS <10 NS
06-30-11 1.1 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 9.1 <0.5 NS 0.58 NS
09-08-11 4.5 <0.5 <0.5 <0.5 <0.5 <0.5 NS NS <0.5 <0.5 10.9 <0.5 NS 4 NS
12-09-11 4.1 <0.5 <0.5 <0.5 <0.5 <0.5 NS <0.5 <0.5 <0.5 7.1 <0.5 NS <25 NS
03-14-12 ND ND ND ND ND ND NS ND 0.33J ND 3.6 ND NS ND NS
06-07-12 ND ND ND ND ND ND ND NS ND ND 4 ND NS ND NS
9/11-12/12 13.7 ND ND ND ND ND ND NS 0.67 ND 5.9 ND NS ND NS
12-12-12 15 ND ND ND ND ND ND NS ND ND 0.81 ND NS 4.9 NS
03-14-13 14.2 ND ND ND ND NS NS NS 0.72 ND 3.3 ND NS ND NS
05-30-13 4.2 ND ND ND ND NS NS ND 1.1 ND 0.53 ND NS ND NS
09-10-13 9.2 ND ND ND ND ND NS ND 2.4 ND 0.51 ND NS 0.6 NS
11-07-13 4.1 ND ND ND ND ND NS ND 2.2 ND ND ND NS ND NS
09-20-14 4.8 ND ND ND 0.23 ND NS ND 3.2 ND ND ND NS ND NS
Naphthalene ug/l 03-14-08 470 <1 <1 <1 <1 <1 <1 <1 <1 <1 4.5 DNE DNE DNE NS 6
06-18-08 590 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 DNE DNE DNE NS
09-10-08 136 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 DNE DNE DNE NS
12-03-08 31 <1 <1 <1 <1 <1 <1 <1 <1 <1 3.5 DNE DNE DNE NS
03-18-09 250 <1 1.9 <1 <1 <1 <1 1.6 <1 <1 <1 6.2 NS 490 NS
06-23-09 470 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 950 NS
09-09-09 540 <1 <1 <1 <1 <1 NS <1 <1 NS <1 <1 NS 680 NS
12-03-09 490 <1 <1 <1 <1 <1 <1 <1 <1 NS <1 <1 NS 750 NS
03-24-10 550 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 220 NS
06-24-10 680 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 580 NS
09-08-10 736 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 NS 255 NS
12-10-10 520 NS NS <1 <1 <1 <1 <1 <1 <1 <1 <1 NS 7.1 NS
03-08-11 337 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 NS 118 NS
06-30-11 54.1 <2 <2 <2 <2 <2 NS NS <2 <2 3 <2 NS 41.6 NS
09-08-11 154 <2 <2 <2 <2 <2 NS NS <2 <2 5.9 <2 NS 395 NS
12-09-11 112 <2 <2 <2 <2 <2 NS <2 <2 <2 <2 <2 NS 504 NS
03-14-12 87 ND ND ND ND ND NS ND ND ND ND ND NS 130J NS
06-07-12 84 ND ND ND ND ND ND NS ND ND ND ND NS 150 NS
9/11-12/12 197 ND ND ND ND ND ND NS ND ND ND ND NS 515 NS
12-12-12 99 ND ND ND ND ND ND NS ND ND ND ND NS 250 NS
03-14-13 84.6 ND ND ND ND NS NS NS ND ND ND ND NS 344 NS
05-30-13 3.4 ND ND ND ND NS NS ND ND ND ND ND NS ND NS
09-10-13 18 ND ND ND ND ND NS ND ND ND ND ND NS 2.3 NS
11-07-13 ND ND ND ND ND ND NS ND ND ND ND ND NS ND NS
09-20-14 2.5 ND ND ND ND ND NS ND ND ND ND ND NS ND NS
NA=Not Analyzed for Parameter DNE=Did Not Exist Bold Values exceed the NCAC 2L Groundwater StandardNS=Not Sampled BDL=Below Detection Limits
Parameter Date MW-1 MW-3 MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15
DO (mg/l)9/9/2009 6.19 7.09 7.2 7.67 6.21 5.83 NR NR 5.81 NR 6.92 3.96 NR 6.71
3/24/2010 7.45 4.79 2.72 8.02 7.1 5.11 2.52 7.06 1.53 4.31 5.21 9.75 NR 6.63
6/24/2010 1.07 1.96 3.21 1.39 1.24 2.16 1.8 4.09 2.25 2.19 2.26 7.9 NR 2.91
9/7/2010 1.36 1.2 3.3 8.48 1.75 6.42 1.82 2.55 9.08 2.43 2.28 8.99 NR 8.14
12/10/2010 6.31 4.56 7.22 4.41 5 9.09 6.21 NR 8.46 7.48 6.4 10.88 NR 7.83
3/8/2011 1.23 1.78 1.59 1.44 1.62 3.04 1.25 NR 1.95 1.59 0.85 1.8 NR 1.63
6/30/2011 1.77 10.54 3.59 2.3 2.24 3.21 NR NR 2.77 4.97 5.02 2.85 NR 1.85
9/8/2011 1.79 1.74 2.45 1.63 4.96 NR NR NR 1.74 2.76 1.82 2.96 NR 2.67
12/9/2011 1.57 4.53 5 2.92 1.51 NR NR NR 2.62 2.14 1.5 2 NR 1.41
3/13/2012 1.82 3.02 3.23 1.94 3.49 NR NR NR 3.31 4.54 2.99 8.15 NR 1.68
6/7/2012 3.31 4.45 3.19 1.96 2.18 NR 1.63 NR 1.69 3.85 1.8 4.32 NR 1.58
9/11/2012 1.77 2.37 3.15 2.64 2.49 NR 2.19 NR 3.31 3.35 2.07 2.98 NR 1.63
5/30/2013 6.82 7.3 13.88 2.94 5.2 NR NR NR 7.53 NR 6.19 13.98 NR 11.76
9-10/11-13 2.96 2.42 2.53 2.32 2.22 6.93 NR 3.05 3.88 2.95 3.76 4.39 NR 3.06
11/7/2013 7.67 3.34 3.86 3.25 2.74 3.51 NR 3.37 5.54 3.85 5.58 3.2 NR 8.96
9/19/2014 11.43 4.29 11.09 5.53 5.8 7.32 NR NR 5.67 7.57 3.32 12.08 NR 4.03
Temperature (°C)9/9/2009 20.2 18.8 19.6 18.9 18.3 19.6 NR NR 17.1 NR 17.2 18.4 NR 20.9
6/24/2010 19.92 18.81 18.97 19 18.55 19.41 21.19 19.51 18.07 18.75 17.81 19.93 NR 20.81
9/7/2010 22.02 21.43 21.94 20.19 19.97 23 23.51 20.18 18.51 19.55 18.9 19.9 NR 22.79
12/10/2010 18.3 17.9 18 18.8 17.8 16.7 17.4 NR 16.8 16.9 16.9 17.4 NR 17.9
6/30/2011 19.98 17.34 19.07 18.45 18.91 20.42 NR NR 17.05 18.03 16.19 17.75 NR 19.28
9/8/2011 20.32 19.23 19.89 19.14 19.85 NR NR NR 18.32 19.42 18.26 20.38 NR 20.37
12/9/2011 16.88 16.49 15.67 18.34 18.32 NR NR NR 18.28 17.48 17 17.99 NR 17.83
3/13/2012 18.42 17.98 17.26 18.08 18.28 NR NR NR 17.57 17.44 17.07 17.32 NR 18.15
6/7/2012 18.23 17.99 18.01 18.89 18.8 NR 17.3 NR 16.52 16.74 16.05 18.68 NR 18.12
9/11/2012 21.27 20.39 20.51 22.15 20.31 NR 21.1 NR 18.98 18.73 17.9 21.93 NR 21.74
5/30/2013 21.2 17.64 18.41 18.07 18.01 NR NR NR 17.43 NR 19.03 17.71 NR 18.34
9-10,11,13 21.74 23.57 23.58 22.87 23.27 24.03 NR 23.55 20.12 22.34 22.83 22.55 NR 22.89
11/7/2013 19.91 21.14 20.9 20.58 20.09 21.67 NR 20.9 18.87 20.35 20.09 20.07 NR 20.49
9/19/2014 14.36 17.45 17.53 12.07 15.73 13.33 NR NR 14.18 14.24 15.59 14.07 NR 14.01
pH 9/9/2009 7.31 7.16 6.74 6.65 6.85 7.13 NR NR 6.02 NR 5.9 7.62 NR 7.29
6/24/2010 5 6.39 6.14 5.52 6.38 6.9 5.89 5.87 5.44 5.93 5.1 7.74 NR 6.31
9/7/2010 5.87 5.95 5.75 4.94 6.63 6.63 5.34 5.12 5.13 5.64 4.83 7.1 NR 6.14
12/10/2010 7.45 7.24 7.02 6.41 8.15 7.77 7.06 NR 6.7 7.17 5.72 7.83 NR 7.8
6/30/2011 6.24 6.4 6.13 5.43 6.43 6.65 NR NR 5.24 6.05 4.89 6.75 NR 6.89
9/8/2011 6.25 6.27 6.01 5.66 6.65 NR NR NR 5.39 5.82 5.08 6.88 NR 6.4
12/9/2011 6.3 6.4 6.43 4.84 6.69 NR NR NR 5.66 5.81 4.8 6.74 NR 6.23
3/13/2012 6.35 6.21 6.13 5.15 6.75 NR NR NR 5.63 6 4.54 6.81 NR 6.24
6/7/2012 6.21 5.54 5.54 5.06 6.53 NR 5.35 NR 5.33 5.77 4.37 6.26 NR 5.98
9/11/2012 6.1 6.1 6.15 5.61 6.6 NR 6.17 NR 5.37 5.53 4.96 5.93 NR 6.23
5/30/2013 6.1 6.22 6.07 5.66 6.6 NR NR NR 6.82 NR 6.61 6.54 NR 7.73
9-10/11-13 6.79 6.52 6.6 5 7.06 6.84 NR 5.84 5.37 6.2 4.69 6.49 NR 6.68
11/7/2013 7.5 6.82 6.77 5.31 7.13 7.17 NR 5.7 5.38 5.98 5.02 6.81 NR 7.85
9/19/2014 7.23 5.67 6.85 5.7 7.64 7.16 NR NR 5.23 6.38 4.77 7.07 NR 6.9
TABLE 4
Field Measurements - Monitoring Wells
Harold Smith Grocery, Incident #12913
Union Ridge Road, Burlington, North Carolina
Page 1 of 2
Parameter Date MW-1 MW-3 MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15
TABLE 4
Field Measurements - Monitoring Wells
Harold Smith Grocery, Incident #12913
Union Ridge Road, Burlington, North Carolina
Conductivity 9/9/2009 23.2 19.5 24.3 5.4 50.5 65.1 NR NR 5.5 NR 3.6 22.5 NR 24.8
(m-ohms)6/24/2010 0.013 0.141 0.214 0.072 0.455 0.403 0.263 0.062 0.048 0.207 0.038 0.222 NR 0.198
(m-ohms) 9/7/2010 0.181 0.147 0.215 0.042 0.477 0.423 0.225 0.06 0.048 0.126 0.032 0.189 NR 0.232
12/10/2010 19.2 15.1 21.6 4.9 45.2 59.5 18.4 NR 6 15.3 3.1 18.7 NR 24
6/30/2011 1.18 0.375 0.404 0.179 0.944 DNE DNE NR 0.116 0.528 0.75 0.416 NR 1.1
9/8/2011 1.22 0.374 0.503 0.178 1.03 NR NR NR 0.126 0.474 0.071 0.427 NR 1.25
12/9/2011 1.34 0.131 0.141 0.046 0.455 NR NR NR 0.057 0.146 0.031 0.181 NR 0.611
3/13/2012 1.15 0.117 0.261 0.046 0.458 NR NR NR 0.062 0.166 0.033 0.14 NR 0.669
6/7/2012 1.19 0.136 0.19 0.048 0.447 NR 0.132 NR 0.064 0.238 0.034 0.165 NR 0.67
9/11/2012 1.11 0.144 0.228 0.065 0.451 NR 0.148 NR 0.06 0.201 0.035 0.164 NR 0.619
5/30/2013 0.577 0.158 0.13 0.053 0.376 NR NR NR 0.074 NR 0.192 0.164 NR 0.535
9-10/11-13 0.813 0.215 0.19 0.041 0.45 0.343 NR 0.075 0.055 0.16 0.215 0.217 NR 0.532
11/7/2013 0.503 0.223 0.146 0.052 0.468 0.38 NR 0.068 0.056 0.119 0.17 0.235 NR 0.339
9/19/2014 0.937 0.122 0.358 0.079 0.461 0.318 NR NR 0.139 0.12 0.131 0.29 NR 0.455
ORP 9/9/2009 -204 48 70 56 31 -235 NR NR 58 NR 62 176 NR -198
6/24/2010 -111 73 119 129 130 -80 40 105 138 36 184 105 NR -20
9/7/2010 -78 99 101 209 75 -80 -60 188 202 171 212 81 NR -72
12/10/2010 -94 202 211 152 15 222 -18 NR 140 88 217 129 NR -66
6/30/2011 6 37 103 173 137 -25 NR NR 200 163 219 7 NR -51
9/8/2011 -69 99 134 178 124 NR NR NR 96 176 173 -16 NR -78
12/9/2011 -52 126 113 250 145 NR NR NR 86 85 200 -42 NR -54
3/13/2012 -14 210 203 260 228 NR NR NR 169 208 250 219 NR -47
6/7/2012 -65 184 143 471 159 NR 103 NR 88 95 235 168 NR -39
9/11/2012 -62 28 -6 354 216 NR 12 NR 231 176 173 268 NR -83
5/30/2013 30 59 64 85 83 NR NR NR 65 NR 96 62 NR 73
9-10/11-13 89 9 -55 128 4 -14 NR 83 127 75 179 95 NR 27
11/7/2013 -6 56 -20 101 -26 110 NR 91 140 97 175 34 NR 0.36
9/19/2014 122 135 144 142 118 144 NR NR 185 158 195 142 NR 132
Turbidity 9/9/2009 -5 -5 -5 -5 -5 -5 NR NR -5 NR -5 -5 NR -5
(NTU)6/24/2010 0 0 0 135 299 0 63.7 0.06 0 0.242 146 0 NR 0
9/7/2010 22.6 0 800 334 7.4 12.8 43.3 404 800 172 270 0 NR 0
12/10/2010 -5 -5 -5 -5 839 897 -5 NR -5 957 -5 -5 NR -5
6/30/2011 0 0 800 25.8 17.2 260 NR NR 411 94.8 301 0 NR 800
9/8/2011 0 559 800 96 134 NR NR NR 579 178 672 0 NR 0
12/9/2011 331 800 133 64 2 NR NR NR 156 98 635 800 NR 800
3/13/2012 553 614 800+ 65 267 NR NR NR 366 125 403 800+ NR 800+
6/7/2012 800+ 767 298 63 84 NR 284 NR 249 46 246 800+ NR 800+
9/11/2012 416 800+ 155 56 90 NR 80 NR 516 126 239 800+ NR 800+
5/30/2013 800+ 800 800 160 195 NR NR NR 0 NR 325 800+ NR 0
9-10/11-13 0 0 195 126 28.8 382 NR 94.1 363 232 177 0 NR 0
11/7/2013 0 0 255 67 35.1 217 NR 62.8 388 151 258 0 NR 0
9/19/2014 800+ 471 350 122 92 424 NR NR 212 208 231 800+ NR 342
nm = No measurement NR= Not Recorded d = well dry.
nt = well not tested.nle = well no longer exists. DNE=did not exist
Page 2 of 2
PARAMETER UNITS DATE NCAC 15A:2L
2768B 2774 2760 2773 2755 2761 2779 2765 2765 2765 2800 Groundwate
Influent Midfluent Effluent Standard
Benzen ug/l 03-24-10 <0.5 NS NS NS NS NS NS 1.7 <0.5 <0.5 NS
06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
09-08-10 NS NS NS <0.5 NS NS NS 1 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS 0.97 <0.5 <0.5 NS 1
03-08-11 NS NS NS <0.5 NS NS <0.5 1.6 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 8.4 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 7.1 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 3.3 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND ND NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS
09-20-14 ND NS NS ND NS NS ND ND ND ND NS
Toluen ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS
06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 600
03-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND ND NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS
09-20-14 ND NS NS ND NS NS ND ND ND ND NS
Ethylbenzen ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS
06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 600
03-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND 0.55 NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS
09-20-14 ND ND ND ND NS NS ND ND ND ND NS
Total Xylene ug/l 03-24-10 <3 NS NS NS NS NS NS <3 <3 <3 NS
06-24-10 NS NS NS <1.5 NS NS NS <1.5 <1.5 <1.5 NS
09-08-10 NS NS NS <1.5 NS NS NS <1.5 <1.5 <1.5 NS
12-10-10 NS NS NS <1.5 NS NS NS <1.5 <1.5 <1.5 NS 500
03-08-11 NS NS NS <1.5 NS NS <1.5 <1.5 <1.5 <1.5 NS
06-30-11 NS NS NS <1.5 NS NS <1.5 <3 <1.5 <1.5 NS
09-08-11 NS NS NS <1.5 NS NS <1.5 <3 <1.5 <1.5 NS
12-09-11 NS NS NS <1.5 NS NS <1.5 <3 <1.5 <1.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND ND NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS
09-20-14 ND ND ND ND NS NS ND ND ND ND NS
TOTAL BTE ug/l 03-24-10 BDL NS NS NS NS NS NS 1.7 BDL BDL NS
06-24-10 NS NS NS BDL NS NS NS BDL BDL BDL NS
09-08-10 NS NS NS BDL NS NS NS 1 BDL BDL NS
12-10-10 NS NS NS BDL NS NS NS 0.97 <0.5 <0.5 NS N/
03-08-11 NS NS NS BDL NS NS BDL 1.6 BDL BDL NS
06-30-11 NS NS NS BDL NS NS BDL 8.4 BDL BDL NS
09-08-11 NS NS NS BDL NS NS BDL 7.1 BDL BDL NS
12-09-11 NS NS NS BDL NS NS BDL 3.3 BDL BDL NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND 0.55 NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS
09-20-14 ND ND ND ND NS NS ND ND ND ND NS
SUPPLY WELL
Union Ridge Road, Burlington, North Carolina
TABLE 5
Water Supply Well Analytical Results
Harold Smith Grocer
Incident #12913
Page 1 of 2
PARAMETER UNITS DATE NCAC 15A:2L
2768B 2774 2760 2773 2755 2761 2779 2765 2765 2765 2800 Groundwate
Influent Midfluent Effluent Standard
SUPPLY WELL
Union Ridge Road, Burlington, North Carolina
TABLE 5
Water Supply Well Analytical Results
Harold Smith Grocer
Incident #12913
Methyl Tertiar ug/l 03-24-10 22 NS NS NS NS NS NS 98 <5 <5 NS
Butyl Ethe 06-24-10 NS NS NS <1 NS NS NS <1 <1 <1 NS
(MTBE)09-08-10 NS NS NS <1 NS NS NS 84.8 <1 <1 NS
12-10-10 NS NS NS <1 NS NS NS 100 <1 <1 NS 20
03-08-11 NS NS NS <0.5 NS NS <0.5 166 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 125 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 136 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 150 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND 149 NS ND NS
12-12-12 NS NS NS ND NS NS ND 140 NS ND NS
03-14-13 ND NS NS ND NS NS ND 157 NS ND NS
05-29-13 ND NS NS ND NS NS ND 150 NS ND NS
09-10-13 ND NS NS ND NS NS ND 128 NS ND NS
11-07-13 ND NS NS ND NS NS ND 117 NS ND NS
09-20-14 ND ND ND 0.81 NS NS ND 140 ND 0.62 NS
Ethylen ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS
Dibromid 06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
(EDB)09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 0.02
03-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND ND NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS
09-20-14 ND ND ND ND NS NS ND ND ND ND NS
Isopropyl Ethe ug/l 03-24-10 11 NS NS NS NS NS NS 130 <5 <5 NS
(IPE)06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
09-08-10 NS NS NS <0.5 NS NS NS 104 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS 150 <0.5 <0.5 NS 70
03-08-11 NS NS NS <0.5 NS NS <0.5 260 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 191 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 206 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 178 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND 149 NS ND NS
12-12-12 NS NS NS ND NS NS ND 150 NS ND NS
03-14-13 ND NS NS ND NS NS ND 159 NS ND NS
05-29-13 ND NS NS ND NS NS ND 168 NS ND NS
09-10-13 ND NS NS 0.96 NS NS ND 183 NS ND NS
11-07-13 ND NS NS 1.96 NS NS ND 138 NS ND NS
09-20-14 ND ND ND 0.67 NS NS ND 140 ND 0.2 NS
1,2- Dichloroethan ug/l 03-24-10 <1 NS NS NS NS NS NS 6.2 <1 <1 NS
06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
09-08-10 NS NS NS <0.5 NS NS NS 15.7 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS 19 <0.5 <0.5 NS 0.4
03-08-11 NS NS NS <0.5 NS NS <0.5 33.1 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 28 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 27.4 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 26.6 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND 20.8 NS ND NS
12-12-12 NS NS NS 0.19J NS NS ND 23 NS ND NS
03-14-13 ND NS NS ND NS NS ND 31.5 NS ND NS
05-29-13 ND NS NS ND NS NS ND 25.9 NS ND NS
09-10-13 ND NS NS ND NS NS ND 25.7 NS ND NS
11-07-13 ND NS NS ND NS NS ND 20.1 NS ND NS
09-20-14 ND ND ND 0.44 NS NS ND 20 ND ND NS
1,2-Dichloropropan ug/l 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS
06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS 0.6
03-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS
06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND ND NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS
09-20-14 ND ND ND ND NS NS ND ND ND ND NS
Chloroform 03-24-10 <1 NS NS NS NS NS NS <1 <1 <1 NS
06-24-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
09-08-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
12-10-10 NS NS NS <0.5 NS NS NS <0.5 <0.5 <0.5 NS
03-08-11 NS NS NS <0.5 NS NS <0.5 <0.5 <0.5 <0.5 NS 70
06-30-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
09-08-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
12-09-11 NS NS NS <0.5 NS NS <0.5 <1 <0.5 <0.5 NS
03-14-12 NS NS NS ND NS NS ND NS NS NS NS
06-07-12 NS NS NS ND NS NS ND NS NS NS NS
9/11-12/2012 NS NS NS ND NS NS ND ND NS ND NS
12-12-12 NS NS NS ND NS NS ND ND NS ND NS
03-14-13 ND NS NS ND NS NS ND ND NS ND NS
05-29-13 ND NS NS ND NS NS ND ND NS ND NS
09-10-13 ND NS NS ND NS NS ND ND NS ND NS
11-07-13 ND NS NS ND NS NS ND ND NS ND NS
09-20-14 ND ND ND ND NS NS ND ND ND ND NS
*Samples 2765 influent & effluent were sampled on 9/25/01 NA=Not analyzed for this parameter J=Estimated Value NS=Not Sampled
Page 2 of 2
TABLE 6 System Operation Parameters
Harold Smith Grocery
Incident #12913
Union Ridge Road, Burlington, North Carolina
DATE:
SVE TEMP. (°F)
SVE FLOW (SCFM)
SVE VACUUM (IN.-H2O)
SPARGE TEMP. (°F)
SPARGE PRESSURE (PSI)
1/6/09 65 120 9 180 15
2/4/09 55 115 9 175 12
3/16/09 55 115 8 170 10
4/2/09 75 115 7 180 10
5/6/09 78 115 8 184 10
6/5/09 70 115 6 175 10
7/6/09 80 115 8 NR 10
8/10/09 78 115 8 NR 10
9/8/09 76 115 8 NR 9
10/5/09 72 115 7 NR 7
11/2/09 70 115 6 NR 5
12/13/09 58 115 7 NR 5
1/6/10 36 115 8 NR 3
2/18/10 42 115 8 NR 12
3/5/10 56 115 7 NR 12
3/31/10 50 115 8 NR 12
5/24/10 70 115 8 NR 14
6/25/10 75 110 7 NR 14
7/27/10 75 110 6 NR 12
8/6/10 90 110 6 NR 12
9/2/10 90 110 6 NR 11
10/1/10 85 115 6 NR 10
11/10/10 50 115 6 NR 12
12/7/10 45 115 6 NR 12
1/6/11 40 110 6 NR 12
2/3/11 45 110 6 NR 12
3/15/11 55 110 6 NR 12
SYSTEM OFF – SOIL EXCAVATION
1/6/12 OFF OFF OFF NR 10
2/10/12 OFF OFF OFF NR 10
3/19/12 OFF OFF OFF NR 10
4/4/12 OFF OFF OFF NR 10
5/3/12 OFF OFF OFF NR 10
6/1/12 OFF OFF OFF NR 9
7/3/12 OFF OFF OFF NR 9
8/3/12 OFF OFF OFF NR 9
9/21/12 OFF OFF OFF NR OFF
10/3/12 OFF OFF OFF NR OFF
11/19/12 OFF OFF OFF NR OFF
12/14/12 OFF OFF OFF NR OFF
1/28/13 OFF OFF OFF NR OFF
2/25/13 OFF OFF OFF NR OFF
3/19/13 OFF OFF OFF NR OFF
TABLE 6 System Operation Parameters
Harold Smith Grocery
Incident #12913
Union Ridge Road, Burlington, North Carolina
5/30/13 OFF OFF OFF NR OFF
6/19/13 OFF OFF OFF NR OFF
7/9/13 OFF OFF OFF NR OFF
8/9/13 OFF OFF OFF NR OFF
9/15/3 OFF OFF OFF NR OFF
10/22/13 OFF OFF OFF NR OFF
11/5/13 OFF OFF OFF NR OFF
12/12/13 40 - 5 NR 8
1/10/14 50 - 5 NR 8
2/4/14 40 - 5 NR 8
3/1/14 42 - 5 NR 8

* Individual pressure (in psi) and flow (in scfm) at each sparge well. NR = not recorded.
TABLE 6 System Operation Parameters
Harold Smith Grocery
Incident #12913
Union Ridge Road, Burlington, North Carolina

DATE: AS-1 PRES./ FLOW*
AS-2 PRES./ FLOW*
AS-3 PRES./ FLOW*
AS-4 PRES./ FLOW*
AS-5 PRES./ FLOW*
AS-6 PRES./ FLOW*
AS-7 PRES./ FLOW*
AS-8 PRES./ FLOW*
7/6/09 8/.05 8/.05 8/.05 8/.05 8/.05 8/0.5 8/0 8/0.5
8/10/09 8/.05 8/.05 8/.05 8/.05 8/.05 8/0.5 8/0 8/0.5
9/8/09 7/.05 7/.05 7/.05 7/.05 7/.05 7/.05 7/0 7/.05
10/5/09 5/0.5 5/0.5 5/0.5 5/0.5 5/0.5 5/0 5/.05
11/2/09 4/0.5 4/0.5 4/0.5 4/0.5 4/0.5 4/0.5 4/0 4/0.5
12/13/09 4/0.5 4/0.5 4/0.5 4/0 4/0.5 4/0.5 4/0 4/0.5
1/6/10 3/0.5 3/0.5 3/0 3/0 3/0.5 3/0.5 3/0 3/0
2/18/10 11/3 11/3 11/3 11/3 11/3 11/2 11/0 11/3
3/5/10 11/3 11/2 11/3 11/2 11/3 11/3 11/0 11/3
3/31/10 11/3 11/3 11/3 11/3 11/3 11/3 11/0 11/3
5/24/10 13/4 13/3 13/4 13/4 13/3 13/3 13/0 13/3
6/25/10 13/3 13/3 13/3 13/3 13/3 12/0 13/0 12/3
7/27/10 11/3 11/3 11/3 11/3 11/3 11/3 11/0 11/3
8/6/10 11/3 11/3 10/3 10/3 11/3 11/3 11/0 11/3
9/2/10 10/3 10/2 10/3 10/2 10/2 10/3 10/0 10/2
10/1/10 10/3 10/2 10/2 10/2 10/2 10/2 10/0 10/2
11/10/10 11/3 11/3 11/3 11/2 11/3 11/3 11/0 11/2
12/2/10 11/3 11/3 11/2 11/3 11/3 11/3 11/0 11/2
1/6/11 11/3 11/3 11/2 11/2 11/3 11/2 11/0 11/2
2/3/11 11/3 11/2 11/3 11/2 11/3 11/2 11/0 11/2
3/15/11 11/2 11/3 11/2 11/2 11/3 11/2 11/0 11/2
SYSTEM OFF AFTER SOIL EXCAVATION
1/6/12 8/1 8/0 OFF OFF 8/0 8/1 OFF OFF
2/10/12 10/1 10/0 OFF OFF 10/1 10/1 OFF OFF
3/19/12 8/1 8/1 OFF OFF 8/0 8/0 OFF OFF
4/4/12 8/1 8/1 OFF OFF 8/0 8/0 OFF OFF
5/3/12 8/1 8/1 OFF OFF 8/1 8/0 OFF OFF
6/1/12 8/1 8/1 OFF OFF 8/0 8/0 OFF OFF
7/3/12 8/1 8/1 OFF OFF 8/1 8/1 OFF OFF
8/3/12 8/1 8/1 OFF OFF 8/1 8/1 OFF OFF
9/21/12 8/1 8/1 OFF OFF 8/1 8/1 OFF OFF
10/3/12 OFF OFF OFF OFF OFF OFF OFF OFF
11/19/12 OFF OFF OFF OFF OFF OFF OFF OFF
12/14/12 OFF OFF OFF OFF OFF OFF OFF OFF
1/28/13 OFF OFF OFF OFF OFF OFF OFF OFF
2/25/13 OFF OFF OFF OFF OFF OFF OFF OFF
3/19/13 OFF OFF OFF OFF OFF OFF OFF OFF
NEW SYSTEM INSTALLED AND OPERATIONAL
5/30/13 1/.5 9/2 9/2 1/.5 9/2 9/2 5/1 -
6/19/13 1/.5 9/2 9/2 1/.5 9/2 9/2 5/1 -
7/9/13 1/.5 9/2 9/2 1/.5 9/2 9/2 5/1 -
8/9/13 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
9/15/3 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
10/22/13 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
11/5/13 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
12/12/13 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
1/10/14 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
2/4/14 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -
TABLE 6 System Operation Parameters
Harold Smith Grocery
Incident #12913
Union Ridge Road, Burlington, North Carolina
3/1/14 1/.5 10/2 10/2 1/.5 10/2 10/2 5/1 -

Individual pressure (in psi) and flow (in scfm) at each sparge well. NR = not recorded.

APPENDIX A

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
April 1, 2014
Mika Trisunovic
Pyramid Environmental & Engineering, PC
PO Box 16265
Greensboro, NC 27416
Project Location: Harold South
Client Job Number:
Project Number: 2013-263
Laboratory Work Order Number: 14C0693
Enclosed are results of analyses for samples received by the laboratory on March 21, 2014. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
Lisa A. Worthington
Project Manager
Page 1 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
4/1/2014Pyramid Environmental & Engineering, PC
PO Box 16265
Greensboro, NC 27416
ATTN: Mika Trisunovic
2013-263
14C0693
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Harold South
2013-263
MW-1A 14C0693-01 Ground Water SM18-20 6200B
MW-3 14C0693-02 Ground Water SM18-20 6200B
MW-4 14C0693-03 Ground Water SM18-20 6200B
MW-5 14C0693-04 Ground Water SM18-20 6200B
MW-6 14C0693-05 Ground Water SM18-20 6200B
MW-7 14C0693-06 Ground Water SM18-20 6200B
MW-9 14C0693-07 Ground Water SM18-20 6200B
MW-10 14C0693-08 Ground Water SM18-20 6200B
MW-11 14C0693-09 Ground Water SM18-20 6200B
MW-12 14C0693-10 Ground Water SM18-20 6200B
MW-13 14C0693-11 Ground Water SM18-20 6200B
MW-15 14C0693-12 Ground Water SM18-20 6200B
SW 2773 14C0693-13 Drinking Water SM18-20 6200B
SW 2760 14C0693-14 Drinking Water SM18-20 6200B
SW 2774 14C0693-15 Drinking Water SM18-20 6200B
SW 2768B 14C0693-16 Drinking Water SM18-20 6200B
SW 2779 14C0693-17 Drinking Water SM18-20 6200B
SW 2765 INF 14C0693-18 Drinking Water SM18-20 6200B
SW 2765 EFF 14C0693-19 Drinking Water SM18-20 6200B
SW 2765 MID 14C0693-20 Drinking Water SM18-20 6200B
Page 2 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
SM18-20 6200B
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
1,2,3-Trichlorobenzene, 1,2,4-Trichlorobenzene, 2,2-Dichloropropane, Ethanol, Naphthalene
14C0693-01[MW-1A], 14C0693-02[MW-3], 14C0693-03[MW-4], 14C0693-04[MW-5], 14C0693-05[MW-6], 14C0693-06[MW-7], 14C0693-07[MW-9],
14C0693-08[MW-10], 14C0693-09[MW-11], 14C0693-10[MW-12], 14C0693-11[MW-13], 14C0693-12[MW-15], 14C0693-13[SW 2773], 14C0693-14[SW 2760],
14C0693-15[SW 2774], 14C0693-16[SW 2768B], 14C0693-17[SW 2779], 14C0693-18[SW 2765 INF], 14C0693-19[SW 2765 EFF], 14C0693-20[SW 2765 MID],
B092577-BLK1, B092577-BS1, B092577-BSD1, B092651-BLK1, B092651-BS1, B092651-BSD1
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
Bromoform, trans-1,3-Dichloropropene, Vinyl Acetate
B092577-BS1
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
outside of control limits. Reduced precision anticipated for any reported result for this compound.
Analyte & Samples(s) Qualified:
Ethanol
B092651-BS1
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.
Analyte & Samples(s) Qualified:
Ethanol
14C0693-01[MW-1A], 14C0693-18[SW 2765 INF], 14C0693-20[SW 2765 MID], B092651-BLK1, B092651-BS1, B092651-BSD1
Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may be associated with reported
result.
Analyte & Samples(s) Qualified:
Ethanol
14C0693-01[MW-1A], 14C0693-02[MW-3], 14C0693-03[MW-4], 14C0693-04[MW-5], 14C0693-05[MW-6], 14C0693-06[MW-7], 14C0693-07[MW-9],
14C0693-08[MW-10], 14C0693-09[MW-11], 14C0693-10[MW-12], 14C0693-11[MW-13], 14C0693-12[MW-15], 14C0693-13[SW 2773], 14C0693-14[SW 2760],
14C0693-15[SW 2774], 14C0693-16[SW 2768B], 14C0693-17[SW 2779], 14C0693-18[SW 2765 INF], 14C0693-19[SW 2765 EFF], 14C0693-20[SW 2765 MID],
B092577-BLK1, B092577-BS1, B092577-BSD1, B092651-BLK1, B092651-BS1, B092651-BSD1
Page 3 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Michael A. Erickson
Laboratory Director
Page 4 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-01
Field Sample #: MW-1A
Sample Matrix: Ground Water
Sampled: 3/20/2014 14:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/27/14 15:29 LBDµg/L4.7 3/27/14SM18-20 6200B1Acetone
0.49 0.50 3/27/14 15:29 LBDµg/L0.079 3/27/14SM18-20 6200B1JBenzene
ND 0.50 3/27/14 15:29 LBDµg/L0.044 3/27/14SM18-20 6200B1Bromobenzene
ND 0.50 3/27/14 15:29 LBDµg/L0.22 3/27/14SM18-20 6200B1Bromochloromethane
ND 0.50 3/27/14 15:29 LBDµg/L0.088 3/27/14SM18-20 6200B1Bromodichloromethane
ND 0.50 3/27/14 15:29 LBDµg/L0.21 3/27/14SM18-20 6200B1Bromoform
ND 1.0 3/27/14 15:29 LBDµg/L0.94 3/27/14SM18-20 6200B1Bromomethane
ND 5.0 3/27/14 15:29 LBDµg/L2.4 3/27/14SM18-20 6200B12-Butanone (MEK)
0.29 2.0 3/27/14 15:29 LBDµg/L0.054 3/27/14SM18-20 6200B1Jn-Butylbenzene
0.11 0.50 3/27/14 15:29 LBDµg/L0.084 3/27/14SM18-20 6200B1Jsec-Butylbenzene
ND 0.50 3/27/14 15:29 LBDµg/L0.096 3/27/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 3/27/14 15:29 LBDµg/L0.10 3/27/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 3/27/14 15:29 LBDµg/L0.12 3/27/14SM18-20 6200B1Chlorobenzene
ND 50 3/27/14 15:29 LBDµg/L28 3/27/14SM18-20 6200B1R-05, V-16Ethanol
ND 0.50 3/27/14 15:29 LBDµg/L0.054 3/27/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 3/27/14 15:29 LBDµg/L0.16 3/27/14SM18-20 6200B1Chloroethane
ND 0.50 3/27/14 15:29 LBDµg/L0.14 3/27/14SM18-20 6200B1Chloroform
ND 0.50 3/27/14 15:29 LBDµg/L0.32 3/27/14SM18-20 6200B1Chloromethane
ND 0.50 3/27/14 15:29 LBDµg/L0.070 3/27/14SM18-20 6200B12-Chlorotoluene
ND 0.50 3/27/14 15:29 LBDµg/L0.074 3/27/14SM18-20 6200B14-Chlorotoluene
ND 0.50 3/27/14 15:29 LBDµg/L0.089 3/27/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/27/14 15:29 LBDµg/L0.076 3/27/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 3/27/14 15:29 LBDµg/L0.079 3/27/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 3/27/14 15:29 LBDµg/L0.046 3/27/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 3/27/14 15:29 LBDµg/L0.12 3/27/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/27/14 15:29 LBDµg/L0.16 3/27/14SM18-20 6200B11,1-Dichloroethane
4.8 0.50 3/27/14 15:29 LBDµg/L0.19 3/27/14SM18-20 6200B11,2-Dichloroethane
ND 1.0 3/27/14 15:29 LBDµg/L0.21 3/27/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 3/27/14 15:29 LBDµg/L0.15 3/27/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/27/14 15:29 LBDµg/L0.15 3/27/14SM18-20 6200B1trans-1,2-Dichloroethylene
0.39 0.50 3/27/14 15:29 LBDµg/L0.11 3/27/14SM18-20 6200B1J1,2-Dichloropropane
ND 0.50 3/27/14 15:29 LBDµg/L0.099 3/27/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 3/27/14 15:29 LBDµg/L0.072 3/27/14SM18-20 6200B12,2-Dichloropropane
ND 0.50 3/27/14 15:29 LBDµg/L0.13 3/27/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 3/27/14 15:29 LBDµg/L0.062 3/27/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 3/27/14 15:29 LBDµg/L0.056 3/27/14SM18-20 6200B1trans-1,3-Dichloropropene
46 0.50 3/27/14 15:29 LBDµg/L0.18 3/27/14SM18-20 6200B1Diisopropyl Ether (DIPE)
1.1 0.50 3/27/14 15:29 LBDµg/L0.092 3/27/14SM18-20 6200B1Ethylbenzene
ND 5.0 3/27/14 15:29 LBDµg/L1.5 3/27/14SM18-20 6200B12-Hexanone (MBK)
0.25 0.50 3/27/14 15:29 LBDµg/L0.11 3/27/14SM18-20 6200B1JIsopropylbenzene (Cumene)
0.15 0.50 3/27/14 15:29 LBDµg/L0.12 3/27/14SM18-20 6200B1Jp-Isopropyltoluene (p-Cymene)
8.6 0.50 3/27/14 15:29 LBDµg/L0.090 3/27/14SM18-20 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/27/14 15:29 LBDµg/L3.2 3/27/14SM18-20 6200B1Methylene Chloride
ND 5.0 3/27/14 15:29 LBDµg/L1.5 3/27/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 5 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-01
Field Sample #: MW-1A
Sample Matrix: Ground Water
Sampled: 3/20/2014 14:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
2.5 2.0 3/27/14 15:29 LBDµg/L0.12 3/27/14SM18-20 6200B1L-04Naphthalene
0.44 0.50 3/27/14 15:29 LBDµg/L0.094 3/27/14SM18-20 6200B1Jn-Propylbenzene
0.12 0.50 3/27/14 15:29 LBDµg/L0.12 3/27/14SM18-20 6200B1JStyrene
ND 0.50 3/27/14 15:29 LBDµg/L0.12 3/27/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 1.0 3/27/14 15:29 LBDµg/L0.080 3/27/14SM18-20 6200B1Tetrachloroethylene
0.31 0.50 3/27/14 15:29 LBDµg/L0.090 3/27/14SM18-20 6200B1JToluene
ND 2.0 3/27/14 15:29 LBDµg/L0.14 3/27/14SM18-20 6200B1L-041,2,3-Trichlorobenzene
ND 1.0 3/27/14 15:29 LBDµg/L0.12 3/27/14SM18-20 6200B1L-041,2,4-Trichlorobenzene
ND 0.50 3/27/14 15:29 LBDµg/L0.094 3/27/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 3/27/14 15:29 LBDµg/L0.12 3/27/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 3/27/14 15:29 LBDµg/L0.077 3/27/14SM18-20 6200B1Trichloroethylene
ND 0.50 3/27/14 15:29 LBDµg/L0.15 3/27/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/27/14 15:29 LBDµg/L0.12 3/27/14SM18-20 6200B11,2,3-Trichloropropane
9.9 0.50 3/27/14 15:29 LBDµg/L0.18 3/27/14SM18-20 6200B11,2,4-Trimethylbenzene
3.8 0.50 3/27/14 15:29 LBDµg/L0.10 3/27/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 3/27/14 15:29 LBDµg/L1.3 3/27/14SM18-20 6200B1Vinyl Acetate
ND 0.50 3/27/14 15:29 LBDµg/L0.13 3/27/14SM18-20 6200B1Vinyl Chloride
2.7 1.0 3/27/14 15:29 LBDµg/L0.18 3/27/14SM18-20 6200B1m+p Xylene
2.9 0.50 3/27/14 15:29 LBDµg/L0.11 3/27/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 85.8 3/27/14 15:2970-130
Toluene-d8 102 3/27/14 15:2970-130
4-Bromofluorobenzene 99.8 3/27/14 15:2970-130
Page 6 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-02
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 3/20/2014 13:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/27/14 3:04 LBDµg/L4.7 3/26/14SM18-20 6200B1Acetone
ND 0.50 3/27/14 3:04 LBDµg/L0.079 3/26/14SM18-20 6200B1Benzene
ND 0.50 3/27/14 3:04 LBDµg/L0.044 3/26/14SM18-20 6200B1Bromobenzene
ND 0.50 3/27/14 3:04 LBDµg/L0.22 3/26/14SM18-20 6200B1Bromochloromethane
ND 0.50 3/27/14 3:04 LBDµg/L0.088 3/26/14SM18-20 6200B1Bromodichloromethane
ND 0.50 3/27/14 3:04 LBDµg/L0.21 3/26/14SM18-20 6200B1Bromoform
ND 1.0 3/27/14 3:04 LBDµg/L0.94 3/26/14SM18-20 6200B1Bromomethane
ND 5.0 3/27/14 3:04 LBDµg/L2.4 3/26/14SM18-20 6200B12-Butanone (MEK)
ND 2.0 3/27/14 3:04 LBDµg/L0.054 3/26/14SM18-20 6200B1n-Butylbenzene
ND 0.50 3/27/14 3:04 LBDµg/L0.084 3/26/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 3/27/14 3:04 LBDµg/L0.096 3/26/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 3/27/14 3:04 LBDµg/L0.10 3/26/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 3/27/14 3:04 LBDµg/L0.12 3/26/14SM18-20 6200B1Chlorobenzene
ND 50 3/27/14 3:04 LBDµg/L28 3/26/14SM18-20 6200B1L-04, V-16Ethanol
ND 0.50 3/27/14 3:04 LBDµg/L0.054 3/26/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 3/27/14 3:04 LBDµg/L0.16 3/26/14SM18-20 6200B1Chloroethane
ND 0.50 3/27/14 3:04 LBDµg/L0.14 3/26/14SM18-20 6200B1Chloroform
ND 0.50 3/27/14 3:04 LBDµg/L0.32 3/26/14SM18-20 6200B1Chloromethane
ND 0.50 3/27/14 3:04 LBDµg/L0.070 3/26/14SM18-20 6200B12-Chlorotoluene
ND 0.50 3/27/14 3:04 LBDµg/L0.074 3/26/14SM18-20 6200B14-Chlorotoluene
ND 0.50 3/27/14 3:04 LBDµg/L0.089 3/26/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/27/14 3:04 LBDµg/L0.076 3/26/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 3/27/14 3:04 LBDµg/L0.079 3/26/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 3/27/14 3:04 LBDµg/L0.046 3/26/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 3/27/14 3:04 LBDµg/L0.12 3/26/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/27/14 3:04 LBDµg/L0.16 3/26/14SM18-20 6200B11,1-Dichloroethane
ND 0.50 3/27/14 3:04 LBDµg/L0.19 3/26/14SM18-20 6200B11,2-Dichloroethane
ND 1.0 3/27/14 3:04 LBDµg/L0.21 3/26/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 3/27/14 3:04 LBDµg/L0.15 3/26/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/27/14 3:04 LBDµg/L0.15 3/26/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/27/14 3:04 LBDµg/L0.11 3/26/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 3/27/14 3:04 LBDµg/L0.099 3/26/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 3/27/14 3:04 LBDµg/L0.072 3/26/14SM18-20 6200B1L-042,2-Dichloropropane
ND 0.50 3/27/14 3:04 LBDµg/L0.13 3/26/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 3/27/14 3:04 LBDµg/L0.062 3/26/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 3/27/14 3:04 LBDµg/L0.056 3/26/14SM18-20 6200B1trans-1,3-Dichloropropene
ND 0.50 3/27/14 3:04 LBDµg/L0.18 3/26/14SM18-20 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/27/14 3:04 LBDµg/L0.092 3/26/14SM18-20 6200B1Ethylbenzene
ND 5.0 3/27/14 3:04 LBDµg/L1.5 3/26/14SM18-20 6200B12-Hexanone (MBK)
ND 0.50 3/27/14 3:04 LBDµg/L0.11 3/26/14SM18-20 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/27/14 3:04 LBDµg/L0.12 3/26/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/27/14 3:04 LBDµg/L0.090 3/26/14SM18-20 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/27/14 3:04 LBDµg/L3.2 3/26/14SM18-20 6200B1Methylene Chloride
ND 5.0 3/27/14 3:04 LBDµg/L1.5 3/26/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 7 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-02
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 3/20/2014 13:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/27/14 3:04 LBDµg/L0.12 3/26/14SM18-20 6200B1L-04Naphthalene
ND 0.50 3/27/14 3:04 LBDµg/L0.094 3/26/14SM18-20 6200B1n-Propylbenzene
ND 0.50 3/27/14 3:04 LBDµg/L0.12 3/26/14SM18-20 6200B1Styrene
ND 0.50 3/27/14 3:04 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 1.0 3/27/14 3:04 LBDµg/L0.080 3/26/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 3/27/14 3:04 LBDµg/L0.090 3/26/14SM18-20 6200B1Toluene
ND 2.0 3/27/14 3:04 LBDµg/L0.14 3/26/14SM18-20 6200B1L-041,2,3-Trichlorobenzene
ND 1.0 3/27/14 3:04 LBDµg/L0.12 3/26/14SM18-20 6200B1L-041,2,4-Trichlorobenzene
ND 0.50 3/27/14 3:04 LBDµg/L0.094 3/26/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 3/27/14 3:04 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 3/27/14 3:04 LBDµg/L0.077 3/26/14SM18-20 6200B1Trichloroethylene
ND 0.50 3/27/14 3:04 LBDµg/L0.15 3/26/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/27/14 3:04 LBDµg/L0.12 3/26/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 3/27/14 3:04 LBDµg/L0.18 3/26/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 3/27/14 3:04 LBDµg/L0.10 3/26/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 3/27/14 3:04 LBDµg/L1.3 3/26/14SM18-20 6200B1Vinyl Acetate
ND 0.50 3/27/14 3:04 LBDµg/L0.13 3/26/14SM18-20 6200B1Vinyl Chloride
ND 1.0 3/27/14 3:04 LBDµg/L0.18 3/26/14SM18-20 6200B1m+p Xylene
ND 0.50 3/27/14 3:04 LBDµg/L0.11 3/26/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 85.3 3/27/14 3:0470-130
Toluene-d8 100 3/27/14 3:0470-130
4-Bromofluorobenzene 98.7 3/27/14 3:0470-130
Page 8 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-03
Field Sample #: MW-4
Sample Matrix: Ground Water
Sampled: 3/20/2014 13:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/27/14 3:34 LBDµg/L4.7 3/26/14SM18-20 6200B1Acetone
ND 0.50 3/27/14 3:34 LBDµg/L0.079 3/26/14SM18-20 6200B1Benzene
ND 0.50 3/27/14 3:34 LBDµg/L0.044 3/26/14SM18-20 6200B1Bromobenzene
ND 0.50 3/27/14 3:34 LBDµg/L0.22 3/26/14SM18-20 6200B1Bromochloromethane
ND 0.50 3/27/14 3:34 LBDµg/L0.088 3/26/14SM18-20 6200B1Bromodichloromethane
ND 0.50 3/27/14 3:34 LBDµg/L0.21 3/26/14SM18-20 6200B1Bromoform
ND 1.0 3/27/14 3:34 LBDµg/L0.94 3/26/14SM18-20 6200B1Bromomethane
ND 5.0 3/27/14 3:34 LBDµg/L2.4 3/26/14SM18-20 6200B12-Butanone (MEK)
ND 2.0 3/27/14 3:34 LBDµg/L0.054 3/26/14SM18-20 6200B1n-Butylbenzene
ND 0.50 3/27/14 3:34 LBDµg/L0.084 3/26/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 3/27/14 3:34 LBDµg/L0.096 3/26/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 3/27/14 3:34 LBDµg/L0.10 3/26/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 3/27/14 3:34 LBDµg/L0.12 3/26/14SM18-20 6200B1Chlorobenzene
ND 50 3/27/14 3:34 LBDµg/L28 3/26/14SM18-20 6200B1L-04, V-16Ethanol
ND 0.50 3/27/14 3:34 LBDµg/L0.054 3/26/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 3/27/14 3:34 LBDµg/L0.16 3/26/14SM18-20 6200B1Chloroethane
ND 0.50 3/27/14 3:34 LBDµg/L0.14 3/26/14SM18-20 6200B1Chloroform
ND 0.50 3/27/14 3:34 LBDµg/L0.32 3/26/14SM18-20 6200B1Chloromethane
ND 0.50 3/27/14 3:34 LBDµg/L0.070 3/26/14SM18-20 6200B12-Chlorotoluene
ND 0.50 3/27/14 3:34 LBDµg/L0.074 3/26/14SM18-20 6200B14-Chlorotoluene
ND 0.50 3/27/14 3:34 LBDµg/L0.089 3/26/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/27/14 3:34 LBDµg/L0.076 3/26/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 3/27/14 3:34 LBDµg/L0.079 3/26/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 3/27/14 3:34 LBDµg/L0.046 3/26/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 3/27/14 3:34 LBDµg/L0.12 3/26/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/27/14 3:34 LBDµg/L0.16 3/26/14SM18-20 6200B11,1-Dichloroethane
ND 0.50 3/27/14 3:34 LBDµg/L0.19 3/26/14SM18-20 6200B11,2-Dichloroethane
ND 1.0 3/27/14 3:34 LBDµg/L0.21 3/26/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 3/27/14 3:34 LBDµg/L0.15 3/26/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/27/14 3:34 LBDµg/L0.15 3/26/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/27/14 3:34 LBDµg/L0.11 3/26/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 3/27/14 3:34 LBDµg/L0.099 3/26/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 3/27/14 3:34 LBDµg/L0.072 3/26/14SM18-20 6200B1L-042,2-Dichloropropane
ND 0.50 3/27/14 3:34 LBDµg/L0.13 3/26/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 3/27/14 3:34 LBDµg/L0.062 3/26/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 3/27/14 3:34 LBDµg/L0.056 3/26/14SM18-20 6200B1trans-1,3-Dichloropropene
ND 0.50 3/27/14 3:34 LBDµg/L0.18 3/26/14SM18-20 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/27/14 3:34 LBDµg/L0.092 3/26/14SM18-20 6200B1Ethylbenzene
ND 5.0 3/27/14 3:34 LBDµg/L1.5 3/26/14SM18-20 6200B12-Hexanone (MBK)
ND 0.50 3/27/14 3:34 LBDµg/L0.11 3/26/14SM18-20 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/27/14 3:34 LBDµg/L0.12 3/26/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
0.35 0.50 3/27/14 3:34 LBDµg/L0.090 3/26/14SM18-20 6200B1JMethyl tert-Butyl Ether (MTBE)
ND 5.0 3/27/14 3:34 LBDµg/L3.2 3/26/14SM18-20 6200B1Methylene Chloride
ND 5.0 3/27/14 3:34 LBDµg/L1.5 3/26/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 9 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-03
Field Sample #: MW-4
Sample Matrix: Ground Water
Sampled: 3/20/2014 13:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/27/14 3:34 LBDµg/L0.12 3/26/14SM18-20 6200B1L-04Naphthalene
ND 0.50 3/27/14 3:34 LBDµg/L0.094 3/26/14SM18-20 6200B1n-Propylbenzene
ND 0.50 3/27/14 3:34 LBDµg/L0.12 3/26/14SM18-20 6200B1Styrene
ND 0.50 3/27/14 3:34 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 1.0 3/27/14 3:34 LBDµg/L0.080 3/26/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 3/27/14 3:34 LBDµg/L0.090 3/26/14SM18-20 6200B1Toluene
ND 2.0 3/27/14 3:34 LBDµg/L0.14 3/26/14SM18-20 6200B1L-041,2,3-Trichlorobenzene
ND 1.0 3/27/14 3:34 LBDµg/L0.12 3/26/14SM18-20 6200B1L-041,2,4-Trichlorobenzene
ND 0.50 3/27/14 3:34 LBDµg/L0.094 3/26/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 3/27/14 3:34 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 3/27/14 3:34 LBDµg/L0.077 3/26/14SM18-20 6200B1Trichloroethylene
ND 0.50 3/27/14 3:34 LBDµg/L0.15 3/26/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/27/14 3:34 LBDµg/L0.12 3/26/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 3/27/14 3:34 LBDµg/L0.18 3/26/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 3/27/14 3:34 LBDµg/L0.10 3/26/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 3/27/14 3:34 LBDµg/L1.3 3/26/14SM18-20 6200B1Vinyl Acetate
ND 0.50 3/27/14 3:34 LBDµg/L0.13 3/26/14SM18-20 6200B1Vinyl Chloride
ND 1.0 3/27/14 3:34 LBDµg/L0.18 3/26/14SM18-20 6200B1m+p Xylene
ND 0.50 3/27/14 3:34 LBDµg/L0.11 3/26/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 84.3 3/27/14 3:3470-130
Toluene-d8 101 3/27/14 3:3470-130
4-Bromofluorobenzene 99.8 3/27/14 3:3470-130
Page 10 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-04
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 3/20/2014 14:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/27/14 4:05 LBDµg/L4.7 3/26/14SM18-20 6200B1Acetone
ND 0.50 3/27/14 4:05 LBDµg/L0.079 3/26/14SM18-20 6200B1Benzene
ND 0.50 3/27/14 4:05 LBDµg/L0.044 3/26/14SM18-20 6200B1Bromobenzene
ND 0.50 3/27/14 4:05 LBDµg/L0.22 3/26/14SM18-20 6200B1Bromochloromethane
ND 0.50 3/27/14 4:05 LBDµg/L0.088 3/26/14SM18-20 6200B1Bromodichloromethane
ND 0.50 3/27/14 4:05 LBDµg/L0.21 3/26/14SM18-20 6200B1Bromoform
ND 1.0 3/27/14 4:05 LBDµg/L0.94 3/26/14SM18-20 6200B1Bromomethane
ND 5.0 3/27/14 4:05 LBDµg/L2.4 3/26/14SM18-20 6200B12-Butanone (MEK)
ND 2.0 3/27/14 4:05 LBDµg/L0.054 3/26/14SM18-20 6200B1n-Butylbenzene
ND 0.50 3/27/14 4:05 LBDµg/L0.084 3/26/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 3/27/14 4:05 LBDµg/L0.096 3/26/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 3/27/14 4:05 LBDµg/L0.10 3/26/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 3/27/14 4:05 LBDµg/L0.12 3/26/14SM18-20 6200B1Chlorobenzene
ND 50 3/27/14 4:05 LBDµg/L28 3/26/14SM18-20 6200B1L-04, V-16Ethanol
ND 0.50 3/27/14 4:05 LBDµg/L0.054 3/26/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 3/27/14 4:05 LBDµg/L0.16 3/26/14SM18-20 6200B1Chloroethane
ND 0.50 3/27/14 4:05 LBDµg/L0.14 3/26/14SM18-20 6200B1Chloroform
ND 0.50 3/27/14 4:05 LBDµg/L0.32 3/26/14SM18-20 6200B1Chloromethane
ND 0.50 3/27/14 4:05 LBDµg/L0.070 3/26/14SM18-20 6200B12-Chlorotoluene
ND 0.50 3/27/14 4:05 LBDµg/L0.074 3/26/14SM18-20 6200B14-Chlorotoluene
ND 0.50 3/27/14 4:05 LBDµg/L0.089 3/26/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/27/14 4:05 LBDµg/L0.076 3/26/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 3/27/14 4:05 LBDµg/L0.079 3/26/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 3/27/14 4:05 LBDµg/L0.046 3/26/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 3/27/14 4:05 LBDµg/L0.12 3/26/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/27/14 4:05 LBDµg/L0.16 3/26/14SM18-20 6200B11,1-Dichloroethane
ND 0.50 3/27/14 4:05 LBDµg/L0.19 3/26/14SM18-20 6200B11,2-Dichloroethane
ND 1.0 3/27/14 4:05 LBDµg/L0.21 3/26/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 3/27/14 4:05 LBDµg/L0.15 3/26/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/27/14 4:05 LBDµg/L0.15 3/26/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/27/14 4:05 LBDµg/L0.11 3/26/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 3/27/14 4:05 LBDµg/L0.099 3/26/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 3/27/14 4:05 LBDµg/L0.072 3/26/14SM18-20 6200B1L-042,2-Dichloropropane
ND 0.50 3/27/14 4:05 LBDµg/L0.13 3/26/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 3/27/14 4:05 LBDµg/L0.062 3/26/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 3/27/14 4:05 LBDµg/L0.056 3/26/14SM18-20 6200B1trans-1,3-Dichloropropene
ND 0.50 3/27/14 4:05 LBDµg/L0.18 3/26/14SM18-20 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/27/14 4:05 LBDµg/L0.092 3/26/14SM18-20 6200B1Ethylbenzene
ND 5.0 3/27/14 4:05 LBDµg/L1.5 3/26/14SM18-20 6200B12-Hexanone (MBK)
ND 0.50 3/27/14 4:05 LBDµg/L0.11 3/26/14SM18-20 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/27/14 4:05 LBDµg/L0.12 3/26/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/27/14 4:05 LBDµg/L0.090 3/26/14SM18-20 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/27/14 4:05 LBDµg/L3.2 3/26/14SM18-20 6200B1Methylene Chloride
ND 5.0 3/27/14 4:05 LBDµg/L1.5 3/26/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 11 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-04
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 3/20/2014 14:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/27/14 4:05 LBDµg/L0.12 3/26/14SM18-20 6200B1L-04Naphthalene
ND 0.50 3/27/14 4:05 LBDµg/L0.094 3/26/14SM18-20 6200B1n-Propylbenzene
ND 0.50 3/27/14 4:05 LBDµg/L0.12 3/26/14SM18-20 6200B1Styrene
ND 0.50 3/27/14 4:05 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 1.0 3/27/14 4:05 LBDµg/L0.080 3/26/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 3/27/14 4:05 LBDµg/L0.090 3/26/14SM18-20 6200B1Toluene
ND 2.0 3/27/14 4:05 LBDµg/L0.14 3/26/14SM18-20 6200B1L-041,2,3-Trichlorobenzene
ND 1.0 3/27/14 4:05 LBDµg/L0.12 3/26/14SM18-20 6200B1L-041,2,4-Trichlorobenzene
ND 0.50 3/27/14 4:05 LBDµg/L0.094 3/26/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 3/27/14 4:05 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 3/27/14 4:05 LBDµg/L0.077 3/26/14SM18-20 6200B1Trichloroethylene
ND 0.50 3/27/14 4:05 LBDµg/L0.15 3/26/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/27/14 4:05 LBDµg/L0.12 3/26/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 3/27/14 4:05 LBDµg/L0.18 3/26/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 3/27/14 4:05 LBDµg/L0.10 3/26/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 3/27/14 4:05 LBDµg/L1.3 3/26/14SM18-20 6200B1Vinyl Acetate
ND 0.50 3/27/14 4:05 LBDµg/L0.13 3/26/14SM18-20 6200B1Vinyl Chloride
ND 1.0 3/27/14 4:05 LBDµg/L0.18 3/26/14SM18-20 6200B1m+p Xylene
ND 0.50 3/27/14 4:05 LBDµg/L0.11 3/26/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 86.5 3/27/14 4:0570-130
Toluene-d8 99.4 3/27/14 4:0570-130
4-Bromofluorobenzene 99.0 3/27/14 4:0570-130
Page 12 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-05
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 3/20/2014 15:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/27/14 4:36 LBDµg/L4.7 3/26/14SM18-20 6200B1Acetone
ND 0.50 3/27/14 4:36 LBDµg/L0.079 3/26/14SM18-20 6200B1Benzene
ND 0.50 3/27/14 4:36 LBDµg/L0.044 3/26/14SM18-20 6200B1Bromobenzene
ND 0.50 3/27/14 4:36 LBDµg/L0.22 3/26/14SM18-20 6200B1Bromochloromethane
ND 0.50 3/27/14 4:36 LBDµg/L0.088 3/26/14SM18-20 6200B1Bromodichloromethane
ND 0.50 3/27/14 4:36 LBDµg/L0.21 3/26/14SM18-20 6200B1Bromoform
ND 1.0 3/27/14 4:36 LBDµg/L0.94 3/26/14SM18-20 6200B1Bromomethane
ND 5.0 3/27/14 4:36 LBDµg/L2.4 3/26/14SM18-20 6200B12-Butanone (MEK)
ND 2.0 3/27/14 4:36 LBDµg/L0.054 3/26/14SM18-20 6200B1n-Butylbenzene
ND 0.50 3/27/14 4:36 LBDµg/L0.084 3/26/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 3/27/14 4:36 LBDµg/L0.096 3/26/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 3/27/14 4:36 LBDµg/L0.10 3/26/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 3/27/14 4:36 LBDµg/L0.12 3/26/14SM18-20 6200B1Chlorobenzene
ND 50 3/27/14 4:36 LBDµg/L28 3/26/14SM18-20 6200B1L-04, V-16Ethanol
ND 0.50 3/27/14 4:36 LBDµg/L0.054 3/26/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 3/27/14 4:36 LBDµg/L0.16 3/26/14SM18-20 6200B1Chloroethane
ND 0.50 3/27/14 4:36 LBDµg/L0.14 3/26/14SM18-20 6200B1Chloroform
ND 0.50 3/27/14 4:36 LBDµg/L0.32 3/26/14SM18-20 6200B1Chloromethane
ND 0.50 3/27/14 4:36 LBDµg/L0.070 3/26/14SM18-20 6200B12-Chlorotoluene
ND 0.50 3/27/14 4:36 LBDµg/L0.074 3/26/14SM18-20 6200B14-Chlorotoluene
ND 0.50 3/27/14 4:36 LBDµg/L0.089 3/26/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/27/14 4:36 LBDµg/L0.076 3/26/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 3/27/14 4:36 LBDµg/L0.079 3/26/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 3/27/14 4:36 LBDµg/L0.046 3/26/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 3/27/14 4:36 LBDµg/L0.12 3/26/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
0.23 0.50 3/27/14 4:36 LBDµg/L0.16 3/26/14SM18-20 6200B1J1,1-Dichloroethane
ND 0.50 3/27/14 4:36 LBDµg/L0.19 3/26/14SM18-20 6200B11,2-Dichloroethane
ND 1.0 3/27/14 4:36 LBDµg/L0.21 3/26/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 3/27/14 4:36 LBDµg/L0.15 3/26/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/27/14 4:36 LBDµg/L0.15 3/26/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/27/14 4:36 LBDµg/L0.11 3/26/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 3/27/14 4:36 LBDµg/L0.099 3/26/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 3/27/14 4:36 LBDµg/L0.072 3/26/14SM18-20 6200B1L-042,2-Dichloropropane
ND 0.50 3/27/14 4:36 LBDµg/L0.13 3/26/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 3/27/14 4:36 LBDµg/L0.062 3/26/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 3/27/14 4:36 LBDµg/L0.056 3/26/14SM18-20 6200B1trans-1,3-Dichloropropene
0.20 0.50 3/27/14 4:36 LBDµg/L0.18 3/26/14SM18-20 6200B1JDiisopropyl Ether (DIPE)
ND 0.50 3/27/14 4:36 LBDµg/L0.092 3/26/14SM18-20 6200B1Ethylbenzene
ND 5.0 3/27/14 4:36 LBDµg/L1.5 3/26/14SM18-20 6200B12-Hexanone (MBK)
ND 0.50 3/27/14 4:36 LBDµg/L0.11 3/26/14SM18-20 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/27/14 4:36 LBDµg/L0.12 3/26/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
0.16 0.50 3/27/14 4:36 LBDµg/L0.090 3/26/14SM18-20 6200B1JMethyl tert-Butyl Ether (MTBE)
ND 5.0 3/27/14 4:36 LBDµg/L3.2 3/26/14SM18-20 6200B1Methylene Chloride
ND 5.0 3/27/14 4:36 LBDµg/L1.5 3/26/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 13 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-05
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 3/20/2014 15:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/27/14 4:36 LBDµg/L0.12 3/26/14SM18-20 6200B1L-04Naphthalene
ND 0.50 3/27/14 4:36 LBDµg/L0.094 3/26/14SM18-20 6200B1n-Propylbenzene
ND 0.50 3/27/14 4:36 LBDµg/L0.12 3/26/14SM18-20 6200B1Styrene
ND 0.50 3/27/14 4:36 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 1.0 3/27/14 4:36 LBDµg/L0.080 3/26/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 3/27/14 4:36 LBDµg/L0.090 3/26/14SM18-20 6200B1Toluene
ND 2.0 3/27/14 4:36 LBDµg/L0.14 3/26/14SM18-20 6200B1L-041,2,3-Trichlorobenzene
ND 1.0 3/27/14 4:36 LBDµg/L0.12 3/26/14SM18-20 6200B1L-041,2,4-Trichlorobenzene
ND 0.50 3/27/14 4:36 LBDµg/L0.094 3/26/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 3/27/14 4:36 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 3/27/14 4:36 LBDµg/L0.077 3/26/14SM18-20 6200B1Trichloroethylene
ND 0.50 3/27/14 4:36 LBDµg/L0.15 3/26/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/27/14 4:36 LBDµg/L0.12 3/26/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 3/27/14 4:36 LBDµg/L0.18 3/26/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 3/27/14 4:36 LBDµg/L0.10 3/26/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 3/27/14 4:36 LBDµg/L1.3 3/26/14SM18-20 6200B1Vinyl Acetate
ND 0.50 3/27/14 4:36 LBDµg/L0.13 3/26/14SM18-20 6200B1Vinyl Chloride
ND 1.0 3/27/14 4:36 LBDµg/L0.18 3/26/14SM18-20 6200B1m+p Xylene
ND 0.50 3/27/14 4:36 LBDµg/L0.11 3/26/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 86.8 3/27/14 4:3670-130
Toluene-d8 99.1 3/27/14 4:3670-130
4-Bromofluorobenzene 99.2 3/27/14 4:3670-130
Page 14 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-06
Field Sample #: MW-7
Sample Matrix: Ground Water
Sampled: 3/20/2014 15:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/27/14 5:07 LBDµg/L4.7 3/26/14SM18-20 6200B1Acetone
ND 0.50 3/27/14 5:07 LBDµg/L0.079 3/26/14SM18-20 6200B1Benzene
ND 0.50 3/27/14 5:07 LBDµg/L0.044 3/26/14SM18-20 6200B1Bromobenzene
ND 0.50 3/27/14 5:07 LBDµg/L0.22 3/26/14SM18-20 6200B1Bromochloromethane
ND 0.50 3/27/14 5:07 LBDµg/L0.088 3/26/14SM18-20 6200B1Bromodichloromethane
ND 0.50 3/27/14 5:07 LBDµg/L0.21 3/26/14SM18-20 6200B1Bromoform
ND 1.0 3/27/14 5:07 LBDµg/L0.94 3/26/14SM18-20 6200B1Bromomethane
ND 5.0 3/27/14 5:07 LBDµg/L2.4 3/26/14SM18-20 6200B12-Butanone (MEK)
ND 2.0 3/27/14 5:07 LBDµg/L0.054 3/26/14SM18-20 6200B1n-Butylbenzene
ND 0.50 3/27/14 5:07 LBDµg/L0.084 3/26/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 3/27/14 5:07 LBDµg/L0.096 3/26/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 3/27/14 5:07 LBDµg/L0.10 3/26/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 3/27/14 5:07 LBDµg/L0.12 3/26/14SM18-20 6200B1Chlorobenzene
ND 50 3/27/14 5:07 LBDµg/L28 3/26/14SM18-20 6200B1L-04, V-16Ethanol
ND 0.50 3/27/14 5:07 LBDµg/L0.054 3/26/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 3/27/14 5:07 LBDµg/L0.16 3/26/14SM18-20 6200B1Chloroethane
ND 0.50 3/27/14 5:07 LBDµg/L0.14 3/26/14SM18-20 6200B1Chloroform
ND 0.50 3/27/14 5:07 LBDµg/L0.32 3/26/14SM18-20 6200B1Chloromethane
ND 0.50 3/27/14 5:07 LBDµg/L0.070 3/26/14SM18-20 6200B12-Chlorotoluene
ND 0.50 3/27/14 5:07 LBDµg/L0.074 3/26/14SM18-20 6200B14-Chlorotoluene
ND 0.50 3/27/14 5:07 LBDµg/L0.089 3/26/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/27/14 5:07 LBDµg/L0.076 3/26/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 3/27/14 5:07 LBDµg/L0.079 3/26/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 3/27/14 5:07 LBDµg/L0.046 3/26/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 3/27/14 5:07 LBDµg/L0.12 3/26/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/27/14 5:07 LBDµg/L0.16 3/26/14SM18-20 6200B11,1-Dichloroethane
ND 0.50 3/27/14 5:07 LBDµg/L0.19 3/26/14SM18-20 6200B11,2-Dichloroethane
ND 1.0 3/27/14 5:07 LBDµg/L0.21 3/26/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 3/27/14 5:07 LBDµg/L0.15 3/26/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/27/14 5:07 LBDµg/L0.15 3/26/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/27/14 5:07 LBDµg/L0.11 3/26/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 3/27/14 5:07 LBDµg/L0.099 3/26/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 3/27/14 5:07 LBDµg/L0.072 3/26/14SM18-20 6200B1L-042,2-Dichloropropane
ND 0.50 3/27/14 5:07 LBDµg/L0.13 3/26/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 3/27/14 5:07 LBDµg/L0.062 3/26/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 3/27/14 5:07 LBDµg/L0.056 3/26/14SM18-20 6200B1trans-1,3-Dichloropropene
ND 0.50 3/27/14 5:07 LBDµg/L0.18 3/26/14SM18-20 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/27/14 5:07 LBDµg/L0.092 3/26/14SM18-20 6200B1Ethylbenzene
ND 5.0 3/27/14 5:07 LBDµg/L1.5 3/26/14SM18-20 6200B12-Hexanone (MBK)
ND 0.50 3/27/14 5:07 LBDµg/L0.11 3/26/14SM18-20 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/27/14 5:07 LBDµg/L0.12 3/26/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/27/14 5:07 LBDµg/L0.090 3/26/14SM18-20 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/27/14 5:07 LBDµg/L3.2 3/26/14SM18-20 6200B1Methylene Chloride
ND 5.0 3/27/14 5:07 LBDµg/L1.5 3/26/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 15 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-06
Field Sample #: MW-7
Sample Matrix: Ground Water
Sampled: 3/20/2014 15:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/27/14 5:07 LBDµg/L0.12 3/26/14SM18-20 6200B1L-04Naphthalene
ND 0.50 3/27/14 5:07 LBDµg/L0.094 3/26/14SM18-20 6200B1n-Propylbenzene
ND 0.50 3/27/14 5:07 LBDµg/L0.12 3/26/14SM18-20 6200B1Styrene
ND 0.50 3/27/14 5:07 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 1.0 3/27/14 5:07 LBDµg/L0.080 3/26/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 3/27/14 5:07 LBDµg/L0.090 3/26/14SM18-20 6200B1Toluene
ND 2.0 3/27/14 5:07 LBDµg/L0.14 3/26/14SM18-20 6200B1L-041,2,3-Trichlorobenzene
ND 1.0 3/27/14 5:07 LBDµg/L0.12 3/26/14SM18-20 6200B1L-041,2,4-Trichlorobenzene
ND 0.50 3/27/14 5:07 LBDµg/L0.094 3/26/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 3/27/14 5:07 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 3/27/14 5:07 LBDµg/L0.077 3/26/14SM18-20 6200B1Trichloroethylene
ND 0.50 3/27/14 5:07 LBDµg/L0.15 3/26/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/27/14 5:07 LBDµg/L0.12 3/26/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 3/27/14 5:07 LBDµg/L0.18 3/26/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 3/27/14 5:07 LBDµg/L0.10 3/26/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 3/27/14 5:07 LBDµg/L1.3 3/26/14SM18-20 6200B1Vinyl Acetate
ND 0.50 3/27/14 5:07 LBDµg/L0.13 3/26/14SM18-20 6200B1Vinyl Chloride
ND 1.0 3/27/14 5:07 LBDµg/L0.18 3/26/14SM18-20 6200B1m+p Xylene
ND 0.50 3/27/14 5:07 LBDµg/L0.11 3/26/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 85.1 3/27/14 5:0770-130
Toluene-d8 98.1 3/27/14 5:0770-130
4-Bromofluorobenzene 99.3 3/27/14 5:0770-130
Page 16 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-07
Field Sample #: MW-9
Sample Matrix: Ground Water
Sampled: 3/20/2014 15:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/27/14 5:38 LBDµg/L4.7 3/26/14SM18-20 6200B1Acetone
ND 0.50 3/27/14 5:38 LBDµg/L0.079 3/26/14SM18-20 6200B1Benzene
ND 0.50 3/27/14 5:38 LBDµg/L0.044 3/26/14SM18-20 6200B1Bromobenzene
ND 0.50 3/27/14 5:38 LBDµg/L0.22 3/26/14SM18-20 6200B1Bromochloromethane
ND 0.50 3/27/14 5:38 LBDµg/L0.088 3/26/14SM18-20 6200B1Bromodichloromethane
ND 0.50 3/27/14 5:38 LBDµg/L0.21 3/26/14SM18-20 6200B1Bromoform
ND 1.0 3/27/14 5:38 LBDµg/L0.94 3/26/14SM18-20 6200B1Bromomethane
ND 5.0 3/27/14 5:38 LBDµg/L2.4 3/26/14SM18-20 6200B12-Butanone (MEK)
ND 2.0 3/27/14 5:38 LBDµg/L0.054 3/26/14SM18-20 6200B1n-Butylbenzene
ND 0.50 3/27/14 5:38 LBDµg/L0.084 3/26/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 3/27/14 5:38 LBDµg/L0.096 3/26/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 3/27/14 5:38 LBDµg/L0.10 3/26/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 3/27/14 5:38 LBDµg/L0.12 3/26/14SM18-20 6200B1Chlorobenzene
ND 50 3/27/14 5:38 LBDµg/L28 3/26/14SM18-20 6200B1L-04, V-16Ethanol
ND 0.50 3/27/14 5:38 LBDµg/L0.054 3/26/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 3/27/14 5:38 LBDµg/L0.16 3/26/14SM18-20 6200B1Chloroethane
ND 0.50 3/27/14 5:38 LBDµg/L0.14 3/26/14SM18-20 6200B1Chloroform
ND 0.50 3/27/14 5:38 LBDµg/L0.32 3/26/14SM18-20 6200B1Chloromethane
ND 0.50 3/27/14 5:38 LBDµg/L0.070 3/26/14SM18-20 6200B12-Chlorotoluene
ND 0.50 3/27/14 5:38 LBDµg/L0.074 3/26/14SM18-20 6200B14-Chlorotoluene
ND 0.50 3/27/14 5:38 LBDµg/L0.089 3/26/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/27/14 5:38 LBDµg/L0.076 3/26/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 3/27/14 5:38 LBDµg/L0.079 3/26/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 3/27/14 5:38 LBDµg/L0.046 3/26/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 3/27/14 5:38 LBDµg/L0.12 3/26/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/27/14 5:38 LBDµg/L0.16 3/26/14SM18-20 6200B11,1-Dichloroethane
ND 0.50 3/27/14 5:38 LBDµg/L0.19 3/26/14SM18-20 6200B11,2-Dichloroethane
ND 1.0 3/27/14 5:38 LBDµg/L0.21 3/26/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 3/27/14 5:38 LBDµg/L0.15 3/26/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/27/14 5:38 LBDµg/L0.15 3/26/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/27/14 5:38 LBDµg/L0.11 3/26/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 3/27/14 5:38 LBDµg/L0.099 3/26/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 3/27/14 5:38 LBDµg/L0.072 3/26/14SM18-20 6200B1L-042,2-Dichloropropane
ND 0.50 3/27/14 5:38 LBDµg/L0.13 3/26/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 3/27/14 5:38 LBDµg/L0.062 3/26/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 3/27/14 5:38 LBDµg/L0.056 3/26/14SM18-20 6200B1trans-1,3-Dichloropropene
ND 0.50 3/27/14 5:38 LBDµg/L0.18 3/26/14SM18-20 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/27/14 5:38 LBDµg/L0.092 3/26/14SM18-20 6200B1Ethylbenzene
ND 5.0 3/27/14 5:38 LBDµg/L1.5 3/26/14SM18-20 6200B12-Hexanone (MBK)
ND 0.50 3/27/14 5:38 LBDµg/L0.11 3/26/14SM18-20 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/27/14 5:38 LBDµg/L0.12 3/26/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
1.1 0.50 3/27/14 5:38 LBDµg/L0.090 3/26/14SM18-20 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/27/14 5:38 LBDµg/L3.2 3/26/14SM18-20 6200B1Methylene Chloride
ND 5.0 3/27/14 5:38 LBDµg/L1.5 3/26/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 17 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-07
Field Sample #: MW-9
Sample Matrix: Ground Water
Sampled: 3/20/2014 15:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/27/14 5:38 LBDµg/L0.12 3/26/14SM18-20 6200B1L-04Naphthalene
ND 0.50 3/27/14 5:38 LBDµg/L0.094 3/26/14SM18-20 6200B1n-Propylbenzene
ND 0.50 3/27/14 5:38 LBDµg/L0.12 3/26/14SM18-20 6200B1Styrene
ND 0.50 3/27/14 5:38 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 1.0 3/27/14 5:38 LBDµg/L0.080 3/26/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 3/27/14 5:38 LBDµg/L0.090 3/26/14SM18-20 6200B1Toluene
ND 2.0 3/27/14 5:38 LBDµg/L0.14 3/26/14SM18-20 6200B1L-041,2,3-Trichlorobenzene
ND 1.0 3/27/14 5:38 LBDµg/L0.12 3/26/14SM18-20 6200B1L-041,2,4-Trichlorobenzene
ND 0.50 3/27/14 5:38 LBDµg/L0.094 3/26/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 3/27/14 5:38 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 3/27/14 5:38 LBDµg/L0.077 3/26/14SM18-20 6200B1Trichloroethylene
ND 0.50 3/27/14 5:38 LBDµg/L0.15 3/26/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/27/14 5:38 LBDµg/L0.12 3/26/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 3/27/14 5:38 LBDµg/L0.18 3/26/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 3/27/14 5:38 LBDµg/L0.10 3/26/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 3/27/14 5:38 LBDµg/L1.3 3/26/14SM18-20 6200B1Vinyl Acetate
ND 0.50 3/27/14 5:38 LBDµg/L0.13 3/26/14SM18-20 6200B1Vinyl Chloride
ND 1.0 3/27/14 5:38 LBDµg/L0.18 3/26/14SM18-20 6200B1m+p Xylene
ND 0.50 3/27/14 5:38 LBDµg/L0.11 3/26/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 86.0 3/27/14 5:3870-130
Toluene-d8 100 3/27/14 5:3870-130
4-Bromofluorobenzene 98.3 3/27/14 5:3870-130
Page 18 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-08
Field Sample #: MW-10
Sample Matrix: Ground Water
Sampled: 3/20/2014 15:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/27/14 6:09 LBDµg/L4.7 3/26/14SM18-20 6200B1Acetone
ND 0.50 3/27/14 6:09 LBDµg/L0.079 3/26/14SM18-20 6200B1Benzene
ND 0.50 3/27/14 6:09 LBDµg/L0.044 3/26/14SM18-20 6200B1Bromobenzene
ND 0.50 3/27/14 6:09 LBDµg/L0.22 3/26/14SM18-20 6200B1Bromochloromethane
ND 0.50 3/27/14 6:09 LBDµg/L0.088 3/26/14SM18-20 6200B1Bromodichloromethane
ND 0.50 3/27/14 6:09 LBDµg/L0.21 3/26/14SM18-20 6200B1Bromoform
ND 1.0 3/27/14 6:09 LBDµg/L0.94 3/26/14SM18-20 6200B1Bromomethane
ND 5.0 3/27/14 6:09 LBDµg/L2.4 3/26/14SM18-20 6200B12-Butanone (MEK)
ND 2.0 3/27/14 6:09 LBDµg/L0.054 3/26/14SM18-20 6200B1n-Butylbenzene
ND 0.50 3/27/14 6:09 LBDµg/L0.084 3/26/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 3/27/14 6:09 LBDµg/L0.096 3/26/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 3/27/14 6:09 LBDµg/L0.10 3/26/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 3/27/14 6:09 LBDµg/L0.12 3/26/14SM18-20 6200B1Chlorobenzene
ND 50 3/27/14 6:09 LBDµg/L28 3/26/14SM18-20 6200B1L-04, V-16Ethanol
ND 0.50 3/27/14 6:09 LBDµg/L0.054 3/26/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 3/27/14 6:09 LBDµg/L0.16 3/26/14SM18-20 6200B1Chloroethane
ND 0.50 3/27/14 6:09 LBDµg/L0.14 3/26/14SM18-20 6200B1Chloroform
ND 0.50 3/27/14 6:09 LBDµg/L0.32 3/26/14SM18-20 6200B1Chloromethane
ND 0.50 3/27/14 6:09 LBDµg/L0.070 3/26/14SM18-20 6200B12-Chlorotoluene
ND 0.50 3/27/14 6:09 LBDµg/L0.074 3/26/14SM18-20 6200B14-Chlorotoluene
ND 0.50 3/27/14 6:09 LBDµg/L0.089 3/26/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/27/14 6:09 LBDµg/L0.076 3/26/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 3/27/14 6:09 LBDµg/L0.079 3/26/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 3/27/14 6:09 LBDµg/L0.046 3/26/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 3/27/14 6:09 LBDµg/L0.12 3/26/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/27/14 6:09 LBDµg/L0.16 3/26/14SM18-20 6200B11,1-Dichloroethane
ND 0.50 3/27/14 6:09 LBDµg/L0.19 3/26/14SM18-20 6200B11,2-Dichloroethane
ND 1.0 3/27/14 6:09 LBDµg/L0.21 3/26/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 3/27/14 6:09 LBDµg/L0.15 3/26/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/27/14 6:09 LBDµg/L0.15 3/26/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/27/14 6:09 LBDµg/L0.11 3/26/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 3/27/14 6:09 LBDµg/L0.099 3/26/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 3/27/14 6:09 LBDµg/L0.072 3/26/14SM18-20 6200B1L-042,2-Dichloropropane
ND 0.50 3/27/14 6:09 LBDµg/L0.13 3/26/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 3/27/14 6:09 LBDµg/L0.062 3/26/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 3/27/14 6:09 LBDµg/L0.056 3/26/14SM18-20 6200B1trans-1,3-Dichloropropene
ND 0.50 3/27/14 6:09 LBDµg/L0.18 3/26/14SM18-20 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/27/14 6:09 LBDµg/L0.092 3/26/14SM18-20 6200B1Ethylbenzene
ND 5.0 3/27/14 6:09 LBDµg/L1.5 3/26/14SM18-20 6200B12-Hexanone (MBK)
ND 0.50 3/27/14 6:09 LBDµg/L0.11 3/26/14SM18-20 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/27/14 6:09 LBDµg/L0.12 3/26/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
0.12 0.50 3/27/14 6:09 LBDµg/L0.090 3/26/14SM18-20 6200B1JMethyl tert-Butyl Ether (MTBE)
ND 5.0 3/27/14 6:09 LBDµg/L3.2 3/26/14SM18-20 6200B1Methylene Chloride
ND 5.0 3/27/14 6:09 LBDµg/L1.5 3/26/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 19 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-08
Field Sample #: MW-10
Sample Matrix: Ground Water
Sampled: 3/20/2014 15:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/27/14 6:09 LBDµg/L0.12 3/26/14SM18-20 6200B1L-04Naphthalene
ND 0.50 3/27/14 6:09 LBDµg/L0.094 3/26/14SM18-20 6200B1n-Propylbenzene
ND 0.50 3/27/14 6:09 LBDµg/L0.12 3/26/14SM18-20 6200B1Styrene
ND 0.50 3/27/14 6:09 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 1.0 3/27/14 6:09 LBDµg/L0.080 3/26/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 3/27/14 6:09 LBDµg/L0.090 3/26/14SM18-20 6200B1Toluene
ND 2.0 3/27/14 6:09 LBDµg/L0.14 3/26/14SM18-20 6200B1L-041,2,3-Trichlorobenzene
ND 1.0 3/27/14 6:09 LBDµg/L0.12 3/26/14SM18-20 6200B1L-041,2,4-Trichlorobenzene
ND 0.50 3/27/14 6:09 LBDµg/L0.094 3/26/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 3/27/14 6:09 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 3/27/14 6:09 LBDµg/L0.077 3/26/14SM18-20 6200B1Trichloroethylene
ND 0.50 3/27/14 6:09 LBDµg/L0.15 3/26/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/27/14 6:09 LBDµg/L0.12 3/26/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 3/27/14 6:09 LBDµg/L0.18 3/26/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 3/27/14 6:09 LBDµg/L0.10 3/26/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 3/27/14 6:09 LBDµg/L1.3 3/26/14SM18-20 6200B1Vinyl Acetate
ND 0.50 3/27/14 6:09 LBDµg/L0.13 3/26/14SM18-20 6200B1Vinyl Chloride
ND 1.0 3/27/14 6:09 LBDµg/L0.18 3/26/14SM18-20 6200B1m+p Xylene
ND 0.50 3/27/14 6:09 LBDµg/L0.11 3/26/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 86.6 3/27/14 6:0970-130
Toluene-d8 99.2 3/27/14 6:0970-130
4-Bromofluorobenzene 97.9 3/27/14 6:0970-130
Page 20 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-09
Field Sample #: MW-11
Sample Matrix: Ground Water
Sampled: 3/20/2014 16:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/27/14 6:40 LBDµg/L4.7 3/26/14SM18-20 6200B1Acetone
ND 0.50 3/27/14 6:40 LBDµg/L0.079 3/26/14SM18-20 6200B1Benzene
ND 0.50 3/27/14 6:40 LBDµg/L0.044 3/26/14SM18-20 6200B1Bromobenzene
ND 0.50 3/27/14 6:40 LBDµg/L0.22 3/26/14SM18-20 6200B1Bromochloromethane
ND 0.50 3/27/14 6:40 LBDµg/L0.088 3/26/14SM18-20 6200B1Bromodichloromethane
ND 0.50 3/27/14 6:40 LBDµg/L0.21 3/26/14SM18-20 6200B1Bromoform
ND 1.0 3/27/14 6:40 LBDµg/L0.94 3/26/14SM18-20 6200B1Bromomethane
ND 5.0 3/27/14 6:40 LBDµg/L2.4 3/26/14SM18-20 6200B12-Butanone (MEK)
ND 2.0 3/27/14 6:40 LBDµg/L0.054 3/26/14SM18-20 6200B1n-Butylbenzene
ND 0.50 3/27/14 6:40 LBDµg/L0.084 3/26/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 3/27/14 6:40 LBDµg/L0.096 3/26/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 3/27/14 6:40 LBDµg/L0.10 3/26/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 3/27/14 6:40 LBDµg/L0.12 3/26/14SM18-20 6200B1Chlorobenzene
ND 50 3/27/14 6:40 LBDµg/L28 3/26/14SM18-20 6200B1L-04, V-16Ethanol
ND 0.50 3/27/14 6:40 LBDµg/L0.054 3/26/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 3/27/14 6:40 LBDµg/L0.16 3/26/14SM18-20 6200B1Chloroethane
ND 0.50 3/27/14 6:40 LBDµg/L0.14 3/26/14SM18-20 6200B1Chloroform
ND 0.50 3/27/14 6:40 LBDµg/L0.32 3/26/14SM18-20 6200B1Chloromethane
ND 0.50 3/27/14 6:40 LBDµg/L0.070 3/26/14SM18-20 6200B12-Chlorotoluene
ND 0.50 3/27/14 6:40 LBDµg/L0.074 3/26/14SM18-20 6200B14-Chlorotoluene
ND 0.50 3/27/14 6:40 LBDµg/L0.089 3/26/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/27/14 6:40 LBDµg/L0.076 3/26/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 3/27/14 6:40 LBDµg/L0.079 3/26/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 3/27/14 6:40 LBDµg/L0.046 3/26/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 3/27/14 6:40 LBDµg/L0.12 3/26/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/27/14 6:40 LBDµg/L0.16 3/26/14SM18-20 6200B11,1-Dichloroethane
ND 0.50 3/27/14 6:40 LBDµg/L0.19 3/26/14SM18-20 6200B11,2-Dichloroethane
ND 1.0 3/27/14 6:40 LBDµg/L0.21 3/26/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 3/27/14 6:40 LBDµg/L0.15 3/26/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/27/14 6:40 LBDµg/L0.15 3/26/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/27/14 6:40 LBDµg/L0.11 3/26/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 3/27/14 6:40 LBDµg/L0.099 3/26/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 3/27/14 6:40 LBDµg/L0.072 3/26/14SM18-20 6200B1L-042,2-Dichloropropane
ND 0.50 3/27/14 6:40 LBDµg/L0.13 3/26/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 3/27/14 6:40 LBDµg/L0.062 3/26/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 3/27/14 6:40 LBDµg/L0.056 3/26/14SM18-20 6200B1trans-1,3-Dichloropropene
ND 0.50 3/27/14 6:40 LBDµg/L0.18 3/26/14SM18-20 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/27/14 6:40 LBDµg/L0.092 3/26/14SM18-20 6200B1Ethylbenzene
ND 5.0 3/27/14 6:40 LBDµg/L1.5 3/26/14SM18-20 6200B12-Hexanone (MBK)
ND 0.50 3/27/14 6:40 LBDµg/L0.11 3/26/14SM18-20 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/27/14 6:40 LBDµg/L0.12 3/26/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/27/14 6:40 LBDµg/L0.090 3/26/14SM18-20 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/27/14 6:40 LBDµg/L3.2 3/26/14SM18-20 6200B1Methylene Chloride
ND 5.0 3/27/14 6:40 LBDµg/L1.5 3/26/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 21 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-09
Field Sample #: MW-11
Sample Matrix: Ground Water
Sampled: 3/20/2014 16:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/27/14 6:40 LBDµg/L0.12 3/26/14SM18-20 6200B1L-04Naphthalene
ND 0.50 3/27/14 6:40 LBDµg/L0.094 3/26/14SM18-20 6200B1n-Propylbenzene
ND 0.50 3/27/14 6:40 LBDµg/L0.12 3/26/14SM18-20 6200B1Styrene
ND 0.50 3/27/14 6:40 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 1.0 3/27/14 6:40 LBDµg/L0.080 3/26/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 3/27/14 6:40 LBDµg/L0.090 3/26/14SM18-20 6200B1Toluene
ND 2.0 3/27/14 6:40 LBDµg/L0.14 3/26/14SM18-20 6200B1L-041,2,3-Trichlorobenzene
ND 1.0 3/27/14 6:40 LBDµg/L0.12 3/26/14SM18-20 6200B1L-041,2,4-Trichlorobenzene
ND 0.50 3/27/14 6:40 LBDµg/L0.094 3/26/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 3/27/14 6:40 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 3/27/14 6:40 LBDµg/L0.077 3/26/14SM18-20 6200B1Trichloroethylene
ND 0.50 3/27/14 6:40 LBDµg/L0.15 3/26/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/27/14 6:40 LBDµg/L0.12 3/26/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 3/27/14 6:40 LBDµg/L0.18 3/26/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 3/27/14 6:40 LBDµg/L0.10 3/26/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 3/27/14 6:40 LBDµg/L1.3 3/26/14SM18-20 6200B1Vinyl Acetate
ND 0.50 3/27/14 6:40 LBDµg/L0.13 3/26/14SM18-20 6200B1Vinyl Chloride
ND 1.0 3/27/14 6:40 LBDµg/L0.18 3/26/14SM18-20 6200B1m+p Xylene
ND 0.50 3/27/14 6:40 LBDµg/L0.11 3/26/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 86.2 3/27/14 6:4070-130
Toluene-d8 99.2 3/27/14 6:4070-130
4-Bromofluorobenzene 97.6 3/27/14 6:4070-130
Page 22 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-10
Field Sample #: MW-12
Sample Matrix: Ground Water
Sampled: 3/20/2014 16:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/27/14 7:11 LBDµg/L4.7 3/26/14SM18-20 6200B1Acetone
ND 0.50 3/27/14 7:11 LBDµg/L0.079 3/26/14SM18-20 6200B1Benzene
ND 0.50 3/27/14 7:11 LBDµg/L0.044 3/26/14SM18-20 6200B1Bromobenzene
ND 0.50 3/27/14 7:11 LBDµg/L0.22 3/26/14SM18-20 6200B1Bromochloromethane
ND 0.50 3/27/14 7:11 LBDµg/L0.088 3/26/14SM18-20 6200B1Bromodichloromethane
ND 0.50 3/27/14 7:11 LBDµg/L0.21 3/26/14SM18-20 6200B1Bromoform
ND 1.0 3/27/14 7:11 LBDµg/L0.94 3/26/14SM18-20 6200B1Bromomethane
ND 5.0 3/27/14 7:11 LBDµg/L2.4 3/26/14SM18-20 6200B12-Butanone (MEK)
ND 2.0 3/27/14 7:11 LBDµg/L0.054 3/26/14SM18-20 6200B1n-Butylbenzene
ND 0.50 3/27/14 7:11 LBDµg/L0.084 3/26/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 3/27/14 7:11 LBDµg/L0.096 3/26/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 3/27/14 7:11 LBDµg/L0.10 3/26/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 3/27/14 7:11 LBDµg/L0.12 3/26/14SM18-20 6200B1Chlorobenzene
ND 50 3/27/14 7:11 LBDµg/L28 3/26/14SM18-20 6200B1L-04, V-16Ethanol
ND 0.50 3/27/14 7:11 LBDµg/L0.054 3/26/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 3/27/14 7:11 LBDµg/L0.16 3/26/14SM18-20 6200B1Chloroethane
ND 0.50 3/27/14 7:11 LBDµg/L0.14 3/26/14SM18-20 6200B1Chloroform
ND 0.50 3/27/14 7:11 LBDµg/L0.32 3/26/14SM18-20 6200B1Chloromethane
ND 0.50 3/27/14 7:11 LBDµg/L0.070 3/26/14SM18-20 6200B12-Chlorotoluene
ND 0.50 3/27/14 7:11 LBDµg/L0.074 3/26/14SM18-20 6200B14-Chlorotoluene
ND 0.50 3/27/14 7:11 LBDµg/L0.089 3/26/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/27/14 7:11 LBDµg/L0.076 3/26/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 3/27/14 7:11 LBDµg/L0.079 3/26/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 3/27/14 7:11 LBDµg/L0.046 3/26/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 3/27/14 7:11 LBDµg/L0.12 3/26/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/27/14 7:11 LBDµg/L0.16 3/26/14SM18-20 6200B11,1-Dichloroethane
ND 0.50 3/27/14 7:11 LBDµg/L0.19 3/26/14SM18-20 6200B11,2-Dichloroethane
ND 1.0 3/27/14 7:11 LBDµg/L0.21 3/26/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 3/27/14 7:11 LBDµg/L0.15 3/26/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/27/14 7:11 LBDµg/L0.15 3/26/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/27/14 7:11 LBDµg/L0.11 3/26/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 3/27/14 7:11 LBDµg/L0.099 3/26/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 3/27/14 7:11 LBDµg/L0.072 3/26/14SM18-20 6200B1L-042,2-Dichloropropane
ND 0.50 3/27/14 7:11 LBDµg/L0.13 3/26/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 3/27/14 7:11 LBDµg/L0.062 3/26/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 3/27/14 7:11 LBDµg/L0.056 3/26/14SM18-20 6200B1trans-1,3-Dichloropropene
0.34 0.50 3/27/14 7:11 LBDµg/L0.18 3/26/14SM18-20 6200B1JDiisopropyl Ether (DIPE)
ND 0.50 3/27/14 7:11 LBDµg/L0.092 3/26/14SM18-20 6200B1Ethylbenzene
ND 5.0 3/27/14 7:11 LBDµg/L1.5 3/26/14SM18-20 6200B12-Hexanone (MBK)
ND 0.50 3/27/14 7:11 LBDµg/L0.11 3/26/14SM18-20 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/27/14 7:11 LBDµg/L0.12 3/26/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
1.8 0.50 3/27/14 7:11 LBDµg/L0.090 3/26/14SM18-20 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/27/14 7:11 LBDµg/L3.2 3/26/14SM18-20 6200B1Methylene Chloride
ND 5.0 3/27/14 7:11 LBDµg/L1.5 3/26/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 23 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-10
Field Sample #: MW-12
Sample Matrix: Ground Water
Sampled: 3/20/2014 16:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/27/14 7:11 LBDµg/L0.12 3/26/14SM18-20 6200B1L-04Naphthalene
ND 0.50 3/27/14 7:11 LBDµg/L0.094 3/26/14SM18-20 6200B1n-Propylbenzene
ND 0.50 3/27/14 7:11 LBDµg/L0.12 3/26/14SM18-20 6200B1Styrene
ND 0.50 3/27/14 7:11 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 1.0 3/27/14 7:11 LBDµg/L0.080 3/26/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 3/27/14 7:11 LBDµg/L0.090 3/26/14SM18-20 6200B1Toluene
ND 2.0 3/27/14 7:11 LBDµg/L0.14 3/26/14SM18-20 6200B1L-041,2,3-Trichlorobenzene
ND 1.0 3/27/14 7:11 LBDµg/L0.12 3/26/14SM18-20 6200B1L-041,2,4-Trichlorobenzene
ND 0.50 3/27/14 7:11 LBDµg/L0.094 3/26/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 3/27/14 7:11 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 3/27/14 7:11 LBDµg/L0.077 3/26/14SM18-20 6200B1Trichloroethylene
ND 0.50 3/27/14 7:11 LBDµg/L0.15 3/26/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/27/14 7:11 LBDµg/L0.12 3/26/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 3/27/14 7:11 LBDµg/L0.18 3/26/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 3/27/14 7:11 LBDµg/L0.10 3/26/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 3/27/14 7:11 LBDµg/L1.3 3/26/14SM18-20 6200B1Vinyl Acetate
ND 0.50 3/27/14 7:11 LBDµg/L0.13 3/26/14SM18-20 6200B1Vinyl Chloride
ND 1.0 3/27/14 7:11 LBDµg/L0.18 3/26/14SM18-20 6200B1m+p Xylene
ND 0.50 3/27/14 7:11 LBDµg/L0.11 3/26/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 85.9 3/27/14 7:1170-130
Toluene-d8 99.8 3/27/14 7:1170-130
4-Bromofluorobenzene 98.3 3/27/14 7:1170-130
Page 24 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-11
Field Sample #: MW-13
Sample Matrix: Ground Water
Sampled: 3/20/2014 15:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/27/14 7:42 LBDµg/L4.7 3/26/14SM18-20 6200B1Acetone
ND 0.50 3/27/14 7:42 LBDµg/L0.079 3/26/14SM18-20 6200B1Benzene
ND 0.50 3/27/14 7:42 LBDµg/L0.044 3/26/14SM18-20 6200B1Bromobenzene
ND 0.50 3/27/14 7:42 LBDµg/L0.22 3/26/14SM18-20 6200B1Bromochloromethane
ND 0.50 3/27/14 7:42 LBDµg/L0.088 3/26/14SM18-20 6200B1Bromodichloromethane
ND 0.50 3/27/14 7:42 LBDµg/L0.21 3/26/14SM18-20 6200B1Bromoform
ND 1.0 3/27/14 7:42 LBDµg/L0.94 3/26/14SM18-20 6200B1Bromomethane
ND 5.0 3/27/14 7:42 LBDµg/L2.4 3/26/14SM18-20 6200B12-Butanone (MEK)
ND 2.0 3/27/14 7:42 LBDµg/L0.054 3/26/14SM18-20 6200B1n-Butylbenzene
0.14 0.50 3/27/14 7:42 LBDµg/L0.084 3/26/14SM18-20 6200B1Jsec-Butylbenzene
ND 0.50 3/27/14 7:42 LBDµg/L0.096 3/26/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 3/27/14 7:42 LBDµg/L0.10 3/26/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 3/27/14 7:42 LBDµg/L0.12 3/26/14SM18-20 6200B1Chlorobenzene
ND 50 3/27/14 7:42 LBDµg/L28 3/26/14SM18-20 6200B1L-04, V-16Ethanol
ND 0.50 3/27/14 7:42 LBDµg/L0.054 3/26/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 3/27/14 7:42 LBDµg/L0.16 3/26/14SM18-20 6200B1Chloroethane
ND 0.50 3/27/14 7:42 LBDµg/L0.14 3/26/14SM18-20 6200B1Chloroform
ND 0.50 3/27/14 7:42 LBDµg/L0.32 3/26/14SM18-20 6200B1Chloromethane
ND 0.50 3/27/14 7:42 LBDµg/L0.070 3/26/14SM18-20 6200B12-Chlorotoluene
ND 0.50 3/27/14 7:42 LBDµg/L0.074 3/26/14SM18-20 6200B14-Chlorotoluene
ND 0.50 3/27/14 7:42 LBDµg/L0.089 3/26/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/27/14 7:42 LBDµg/L0.076 3/26/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 3/27/14 7:42 LBDµg/L0.079 3/26/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 3/27/14 7:42 LBDµg/L0.046 3/26/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 3/27/14 7:42 LBDµg/L0.12 3/26/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/27/14 7:42 LBDµg/L0.16 3/26/14SM18-20 6200B11,1-Dichloroethane
ND 0.50 3/27/14 7:42 LBDµg/L0.19 3/26/14SM18-20 6200B11,2-Dichloroethane
ND 1.0 3/27/14 7:42 LBDµg/L0.21 3/26/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 3/27/14 7:42 LBDµg/L0.15 3/26/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/27/14 7:42 LBDµg/L0.15 3/26/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/27/14 7:42 LBDµg/L0.11 3/26/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 3/27/14 7:42 LBDµg/L0.099 3/26/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 3/27/14 7:42 LBDµg/L0.072 3/26/14SM18-20 6200B1L-042,2-Dichloropropane
ND 0.50 3/27/14 7:42 LBDµg/L0.13 3/26/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 3/27/14 7:42 LBDµg/L0.062 3/26/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 3/27/14 7:42 LBDµg/L0.056 3/26/14SM18-20 6200B1trans-1,3-Dichloropropene
ND 0.50 3/27/14 7:42 LBDµg/L0.18 3/26/14SM18-20 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/27/14 7:42 LBDµg/L0.092 3/26/14SM18-20 6200B1Ethylbenzene
ND 5.0 3/27/14 7:42 LBDµg/L1.5 3/26/14SM18-20 6200B12-Hexanone (MBK)
0.12 0.50 3/27/14 7:42 LBDµg/L0.11 3/26/14SM18-20 6200B1JIsopropylbenzene (Cumene)
ND 0.50 3/27/14 7:42 LBDµg/L0.12 3/26/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/27/14 7:42 LBDµg/L0.090 3/26/14SM18-20 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/27/14 7:42 LBDµg/L3.2 3/26/14SM18-20 6200B1Methylene Chloride
ND 5.0 3/27/14 7:42 LBDµg/L1.5 3/26/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 25 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-11
Field Sample #: MW-13
Sample Matrix: Ground Water
Sampled: 3/20/2014 15:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/27/14 7:42 LBDµg/L0.12 3/26/14SM18-20 6200B1L-04Naphthalene
0.15 0.50 3/27/14 7:42 LBDµg/L0.094 3/26/14SM18-20 6200B1Jn-Propylbenzene
ND 0.50 3/27/14 7:42 LBDµg/L0.12 3/26/14SM18-20 6200B1Styrene
ND 0.50 3/27/14 7:42 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 1.0 3/27/14 7:42 LBDµg/L0.080 3/26/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 3/27/14 7:42 LBDµg/L0.090 3/26/14SM18-20 6200B1Toluene
ND 2.0 3/27/14 7:42 LBDµg/L0.14 3/26/14SM18-20 6200B1L-041,2,3-Trichlorobenzene
ND 1.0 3/27/14 7:42 LBDµg/L0.12 3/26/14SM18-20 6200B1L-041,2,4-Trichlorobenzene
ND 0.50 3/27/14 7:42 LBDµg/L0.094 3/26/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 3/27/14 7:42 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 3/27/14 7:42 LBDµg/L0.077 3/26/14SM18-20 6200B1Trichloroethylene
ND 0.50 3/27/14 7:42 LBDµg/L0.15 3/26/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/27/14 7:42 LBDµg/L0.12 3/26/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 3/27/14 7:42 LBDµg/L0.18 3/26/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 3/27/14 7:42 LBDµg/L0.10 3/26/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 3/27/14 7:42 LBDµg/L1.3 3/26/14SM18-20 6200B1Vinyl Acetate
ND 0.50 3/27/14 7:42 LBDµg/L0.13 3/26/14SM18-20 6200B1Vinyl Chloride
ND 1.0 3/27/14 7:42 LBDµg/L0.18 3/26/14SM18-20 6200B1m+p Xylene
ND 0.50 3/27/14 7:42 LBDµg/L0.11 3/26/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 88.0 3/27/14 7:4270-130
Toluene-d8 101 3/27/14 7:4270-130
4-Bromofluorobenzene 99.8 3/27/14 7:4270-130
Page 26 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-12
Field Sample #: MW-15
Sample Matrix: Ground Water
Sampled: 3/20/2014 15:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/27/14 8:13 LBDµg/L4.7 3/26/14SM18-20 6200B1Acetone
0.29 0.50 3/27/14 8:13 LBDµg/L0.079 3/26/14SM18-20 6200B1JBenzene
ND 0.50 3/27/14 8:13 LBDµg/L0.044 3/26/14SM18-20 6200B1Bromobenzene
ND 0.50 3/27/14 8:13 LBDµg/L0.22 3/26/14SM18-20 6200B1Bromochloromethane
ND 0.50 3/27/14 8:13 LBDµg/L0.088 3/26/14SM18-20 6200B1Bromodichloromethane
ND 0.50 3/27/14 8:13 LBDµg/L0.21 3/26/14SM18-20 6200B1Bromoform
ND 1.0 3/27/14 8:13 LBDµg/L0.94 3/26/14SM18-20 6200B1Bromomethane
ND 5.0 3/27/14 8:13 LBDµg/L2.4 3/26/14SM18-20 6200B12-Butanone (MEK)
0.12 2.0 3/27/14 8:13 LBDµg/L0.054 3/26/14SM18-20 6200B1Jn-Butylbenzene
ND 0.50 3/27/14 8:13 LBDµg/L0.084 3/26/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 3/27/14 8:13 LBDµg/L0.096 3/26/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 3/27/14 8:13 LBDµg/L0.10 3/26/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 3/27/14 8:13 LBDµg/L0.12 3/26/14SM18-20 6200B1Chlorobenzene
ND 50 3/27/14 8:13 LBDµg/L28 3/26/14SM18-20 6200B1L-04, V-16Ethanol
ND 0.50 3/27/14 8:13 LBDµg/L0.054 3/26/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 3/27/14 8:13 LBDµg/L0.16 3/26/14SM18-20 6200B1Chloroethane
ND 0.50 3/27/14 8:13 LBDµg/L0.14 3/26/14SM18-20 6200B1Chloroform
ND 0.50 3/27/14 8:13 LBDµg/L0.32 3/26/14SM18-20 6200B1Chloromethane
ND 0.50 3/27/14 8:13 LBDµg/L0.070 3/26/14SM18-20 6200B12-Chlorotoluene
ND 0.50 3/27/14 8:13 LBDµg/L0.074 3/26/14SM18-20 6200B14-Chlorotoluene
ND 0.50 3/27/14 8:13 LBDµg/L0.089 3/26/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/27/14 8:13 LBDµg/L0.076 3/26/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 3/27/14 8:13 LBDµg/L0.079 3/26/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 3/27/14 8:13 LBDµg/L0.046 3/26/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 3/27/14 8:13 LBDµg/L0.12 3/26/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/27/14 8:13 LBDµg/L0.16 3/26/14SM18-20 6200B11,1-Dichloroethane
ND 0.50 3/27/14 8:13 LBDµg/L0.19 3/26/14SM18-20 6200B11,2-Dichloroethane
ND 1.0 3/27/14 8:13 LBDµg/L0.21 3/26/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 3/27/14 8:13 LBDµg/L0.15 3/26/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/27/14 8:13 LBDµg/L0.15 3/26/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/27/14 8:13 LBDµg/L0.11 3/26/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 3/27/14 8:13 LBDµg/L0.099 3/26/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 3/27/14 8:13 LBDµg/L0.072 3/26/14SM18-20 6200B1L-042,2-Dichloropropane
ND 0.50 3/27/14 8:13 LBDµg/L0.13 3/26/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 3/27/14 8:13 LBDµg/L0.062 3/26/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 3/27/14 8:13 LBDµg/L0.056 3/26/14SM18-20 6200B1trans-1,3-Dichloropropene
1.5 0.50 3/27/14 8:13 LBDµg/L0.18 3/26/14SM18-20 6200B1Diisopropyl Ether (DIPE)
8.0 0.50 3/27/14 8:13 LBDµg/L0.092 3/26/14SM18-20 6200B1Ethylbenzene
ND 5.0 3/27/14 8:13 LBDµg/L1.5 3/26/14SM18-20 6200B12-Hexanone (MBK)
0.40 0.50 3/27/14 8:13 LBDµg/L0.11 3/26/14SM18-20 6200B1JIsopropylbenzene (Cumene)
ND 0.50 3/27/14 8:13 LBDµg/L0.12 3/26/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
0.20 0.50 3/27/14 8:13 LBDµg/L0.090 3/26/14SM18-20 6200B1JMethyl tert-Butyl Ether (MTBE)
ND 5.0 3/27/14 8:13 LBDµg/L3.2 3/26/14SM18-20 6200B1Methylene Chloride
ND 5.0 3/27/14 8:13 LBDµg/L1.5 3/26/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 27 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-12
Field Sample #: MW-15
Sample Matrix: Ground Water
Sampled: 3/20/2014 15:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/27/14 8:13 LBDµg/L0.12 3/26/14SM18-20 6200B1L-04Naphthalene
0.67 0.50 3/27/14 8:13 LBDµg/L0.094 3/26/14SM18-20 6200B1n-Propylbenzene
0.53 0.50 3/27/14 8:13 LBDµg/L0.12 3/26/14SM18-20 6200B1Styrene
ND 0.50 3/27/14 8:13 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 1.0 3/27/14 8:13 LBDµg/L0.080 3/26/14SM18-20 6200B1Tetrachloroethylene
3.0 0.50 3/27/14 8:13 LBDµg/L0.090 3/26/14SM18-20 6200B1Toluene
ND 2.0 3/27/14 8:13 LBDµg/L0.14 3/26/14SM18-20 6200B1L-041,2,3-Trichlorobenzene
ND 1.0 3/27/14 8:13 LBDµg/L0.12 3/26/14SM18-20 6200B1L-041,2,4-Trichlorobenzene
ND 0.50 3/27/14 8:13 LBDµg/L0.094 3/26/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 3/27/14 8:13 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 3/27/14 8:13 LBDµg/L0.077 3/26/14SM18-20 6200B1Trichloroethylene
ND 0.50 3/27/14 8:13 LBDµg/L0.15 3/26/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/27/14 8:13 LBDµg/L0.12 3/26/14SM18-20 6200B11,2,3-Trichloropropane
7.7 0.50 3/27/14 8:13 LBDµg/L0.18 3/26/14SM18-20 6200B11,2,4-Trimethylbenzene
2.2 0.50 3/27/14 8:13 LBDµg/L0.10 3/26/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 3/27/14 8:13 LBDµg/L1.3 3/26/14SM18-20 6200B1Vinyl Acetate
ND 0.50 3/27/14 8:13 LBDµg/L0.13 3/26/14SM18-20 6200B1Vinyl Chloride
23 1.0 3/27/14 8:13 LBDµg/L0.18 3/26/14SM18-20 6200B1m+p Xylene
9.2 0.50 3/27/14 8:13 LBDµg/L0.11 3/26/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 86.0 3/27/14 8:1370-130
Toluene-d8 100 3/27/14 8:1370-130
4-Bromofluorobenzene 101 3/27/14 8:1370-130
Page 28 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-13
Field Sample #: SW 2773
Sample Matrix: Drinking Water
Sampled: 3/20/2014 14:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/27/14 8:43 LBDµg/L4.7 3/26/14SM18-20 6200B1Acetone
ND 0.50 3/27/14 8:43 LBDµg/L0.079 3/26/14SM18-20 6200B1Benzene
ND 0.50 3/27/14 8:43 LBDµg/L0.044 3/26/14SM18-20 6200B1Bromobenzene
ND 0.50 3/27/14 8:43 LBDµg/L0.22 3/26/14SM18-20 6200B1Bromochloromethane
ND 0.50 3/27/14 8:43 LBDµg/L0.088 3/26/14SM18-20 6200B1Bromodichloromethane
ND 0.50 3/27/14 8:43 LBDµg/L0.21 3/26/14SM18-20 6200B1Bromoform
ND 1.0 3/27/14 8:43 LBDµg/L0.94 3/26/14SM18-20 6200B1Bromomethane
ND 5.0 3/27/14 8:43 LBDµg/L2.4 3/26/14SM18-20 6200B12-Butanone (MEK)
ND 2.0 3/27/14 8:43 LBDµg/L0.054 3/26/14SM18-20 6200B1n-Butylbenzene
ND 0.50 3/27/14 8:43 LBDµg/L0.084 3/26/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 3/27/14 8:43 LBDµg/L0.096 3/26/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 3/27/14 8:43 LBDµg/L0.10 3/26/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 3/27/14 8:43 LBDµg/L0.12 3/26/14SM18-20 6200B1Chlorobenzene
ND 50 3/27/14 8:43 LBDµg/L28 3/26/14SM18-20 6200B1L-04, V-16Ethanol
ND 0.50 3/27/14 8:43 LBDµg/L0.054 3/26/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 3/27/14 8:43 LBDµg/L0.16 3/26/14SM18-20 6200B1Chloroethane
ND 0.50 3/27/14 8:43 LBDµg/L0.14 3/26/14SM18-20 6200B1Chloroform
ND 0.50 3/27/14 8:43 LBDµg/L0.32 3/26/14SM18-20 6200B1Chloromethane
ND 0.50 3/27/14 8:43 LBDµg/L0.070 3/26/14SM18-20 6200B12-Chlorotoluene
ND 0.50 3/27/14 8:43 LBDµg/L0.074 3/26/14SM18-20 6200B14-Chlorotoluene
ND 0.50 3/27/14 8:43 LBDµg/L0.089 3/26/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/27/14 8:43 LBDµg/L0.076 3/26/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 3/27/14 8:43 LBDµg/L0.079 3/26/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 3/27/14 8:43 LBDµg/L0.046 3/26/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 3/27/14 8:43 LBDµg/L0.12 3/26/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/27/14 8:43 LBDµg/L0.16 3/26/14SM18-20 6200B11,1-Dichloroethane
0.44 0.50 3/27/14 8:43 LBDµg/L0.19 3/26/14SM18-20 6200B1J1,2-Dichloroethane
ND 1.0 3/27/14 8:43 LBDµg/L0.21 3/26/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 3/27/14 8:43 LBDµg/L0.15 3/26/14SM18-20 6200B1cis-1,2-Dichloroethylene
1.1 0.50 3/27/14 8:43 LBDµg/L0.15 3/26/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/27/14 8:43 LBDµg/L0.11 3/26/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 3/27/14 8:43 LBDµg/L0.099 3/26/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 3/27/14 8:43 LBDµg/L0.072 3/26/14SM18-20 6200B1L-042,2-Dichloropropane
ND 0.50 3/27/14 8:43 LBDµg/L0.13 3/26/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 3/27/14 8:43 LBDµg/L0.062 3/26/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 3/27/14 8:43 LBDµg/L0.056 3/26/14SM18-20 6200B1trans-1,3-Dichloropropene
0.67 0.50 3/27/14 8:43 LBDµg/L0.18 3/26/14SM18-20 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/27/14 8:43 LBDµg/L0.092 3/26/14SM18-20 6200B1Ethylbenzene
ND 5.0 3/27/14 8:43 LBDµg/L1.5 3/26/14SM18-20 6200B12-Hexanone (MBK)
ND 0.50 3/27/14 8:43 LBDµg/L0.11 3/26/14SM18-20 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/27/14 8:43 LBDµg/L0.12 3/26/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
0.81 0.50 3/27/14 8:43 LBDµg/L0.090 3/26/14SM18-20 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/27/14 8:43 LBDµg/L3.2 3/26/14SM18-20 6200B1Methylene Chloride
ND 5.0 3/27/14 8:43 LBDµg/L1.5 3/26/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 29 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-13
Field Sample #: SW 2773
Sample Matrix: Drinking Water
Sampled: 3/20/2014 14:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/27/14 8:43 LBDµg/L0.12 3/26/14SM18-20 6200B1L-04Naphthalene
ND 0.50 3/27/14 8:43 LBDµg/L0.094 3/26/14SM18-20 6200B1n-Propylbenzene
ND 0.50 3/27/14 8:43 LBDµg/L0.12 3/26/14SM18-20 6200B1Styrene
ND 0.50 3/27/14 8:43 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 1.0 3/27/14 8:43 LBDµg/L0.080 3/26/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 3/27/14 8:43 LBDµg/L0.090 3/26/14SM18-20 6200B1Toluene
ND 2.0 3/27/14 8:43 LBDµg/L0.14 3/26/14SM18-20 6200B1L-041,2,3-Trichlorobenzene
ND 1.0 3/27/14 8:43 LBDµg/L0.12 3/26/14SM18-20 6200B1L-041,2,4-Trichlorobenzene
ND 0.50 3/27/14 8:43 LBDµg/L0.094 3/26/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 3/27/14 8:43 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 3/27/14 8:43 LBDµg/L0.077 3/26/14SM18-20 6200B1Trichloroethylene
ND 0.50 3/27/14 8:43 LBDµg/L0.15 3/26/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/27/14 8:43 LBDµg/L0.12 3/26/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 3/27/14 8:43 LBDµg/L0.18 3/26/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 3/27/14 8:43 LBDµg/L0.10 3/26/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 3/27/14 8:43 LBDµg/L1.3 3/26/14SM18-20 6200B1Vinyl Acetate
ND 0.50 3/27/14 8:43 LBDµg/L0.13 3/26/14SM18-20 6200B1Vinyl Chloride
ND 1.0 3/27/14 8:43 LBDµg/L0.18 3/26/14SM18-20 6200B1m+p Xylene
ND 0.50 3/27/14 8:43 LBDµg/L0.11 3/26/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 86.8 3/27/14 8:4370-130
Toluene-d8 98.8 3/27/14 8:4370-130
4-Bromofluorobenzene 98.1 3/27/14 8:4370-130
Page 30 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-14
Field Sample #: SW 2760
Sample Matrix: Drinking Water
Sampled: 3/20/2014 14:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/27/14 9:14 LBDµg/L4.7 3/26/14SM18-20 6200B1Acetone
ND 0.50 3/27/14 9:14 LBDµg/L0.079 3/26/14SM18-20 6200B1Benzene
ND 0.50 3/27/14 9:14 LBDµg/L0.044 3/26/14SM18-20 6200B1Bromobenzene
ND 0.50 3/27/14 9:14 LBDµg/L0.22 3/26/14SM18-20 6200B1Bromochloromethane
ND 0.50 3/27/14 9:14 LBDµg/L0.088 3/26/14SM18-20 6200B1Bromodichloromethane
ND 0.50 3/27/14 9:14 LBDµg/L0.21 3/26/14SM18-20 6200B1Bromoform
ND 1.0 3/27/14 9:14 LBDµg/L0.94 3/26/14SM18-20 6200B1Bromomethane
ND 5.0 3/27/14 9:14 LBDµg/L2.4 3/26/14SM18-20 6200B12-Butanone (MEK)
ND 2.0 3/27/14 9:14 LBDµg/L0.054 3/26/14SM18-20 6200B1n-Butylbenzene
ND 0.50 3/27/14 9:14 LBDµg/L0.084 3/26/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 3/27/14 9:14 LBDµg/L0.096 3/26/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 3/27/14 9:14 LBDµg/L0.10 3/26/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 3/27/14 9:14 LBDµg/L0.12 3/26/14SM18-20 6200B1Chlorobenzene
ND 50 3/27/14 9:14 LBDµg/L28 3/26/14SM18-20 6200B1L-04, V-16Ethanol
ND 0.50 3/27/14 9:14 LBDµg/L0.054 3/26/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 3/27/14 9:14 LBDµg/L0.16 3/26/14SM18-20 6200B1Chloroethane
ND 0.50 3/27/14 9:14 LBDµg/L0.14 3/26/14SM18-20 6200B1Chloroform
ND 0.50 3/27/14 9:14 LBDµg/L0.32 3/26/14SM18-20 6200B1Chloromethane
ND 0.50 3/27/14 9:14 LBDµg/L0.070 3/26/14SM18-20 6200B12-Chlorotoluene
ND 0.50 3/27/14 9:14 LBDµg/L0.074 3/26/14SM18-20 6200B14-Chlorotoluene
ND 0.50 3/27/14 9:14 LBDµg/L0.089 3/26/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/27/14 9:14 LBDµg/L0.076 3/26/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 3/27/14 9:14 LBDµg/L0.079 3/26/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 3/27/14 9:14 LBDµg/L0.046 3/26/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 3/27/14 9:14 LBDµg/L0.12 3/26/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/27/14 9:14 LBDµg/L0.16 3/26/14SM18-20 6200B11,1-Dichloroethane
ND 0.50 3/27/14 9:14 LBDµg/L0.19 3/26/14SM18-20 6200B11,2-Dichloroethane
ND 1.0 3/27/14 9:14 LBDµg/L0.21 3/26/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 3/27/14 9:14 LBDµg/L0.15 3/26/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/27/14 9:14 LBDµg/L0.15 3/26/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/27/14 9:14 LBDµg/L0.11 3/26/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 3/27/14 9:14 LBDµg/L0.099 3/26/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 3/27/14 9:14 LBDµg/L0.072 3/26/14SM18-20 6200B1L-042,2-Dichloropropane
ND 0.50 3/27/14 9:14 LBDµg/L0.13 3/26/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 3/27/14 9:14 LBDµg/L0.062 3/26/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 3/27/14 9:14 LBDµg/L0.056 3/26/14SM18-20 6200B1trans-1,3-Dichloropropene
ND 0.50 3/27/14 9:14 LBDµg/L0.18 3/26/14SM18-20 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/27/14 9:14 LBDµg/L0.092 3/26/14SM18-20 6200B1Ethylbenzene
ND 5.0 3/27/14 9:14 LBDµg/L1.5 3/26/14SM18-20 6200B12-Hexanone (MBK)
ND 0.50 3/27/14 9:14 LBDµg/L0.11 3/26/14SM18-20 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/27/14 9:14 LBDµg/L0.12 3/26/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/27/14 9:14 LBDµg/L0.090 3/26/14SM18-20 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/27/14 9:14 LBDµg/L3.2 3/26/14SM18-20 6200B1Methylene Chloride
ND 5.0 3/27/14 9:14 LBDµg/L1.5 3/26/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 31 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-14
Field Sample #: SW 2760
Sample Matrix: Drinking Water
Sampled: 3/20/2014 14:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/27/14 9:14 LBDµg/L0.12 3/26/14SM18-20 6200B1L-04Naphthalene
ND 0.50 3/27/14 9:14 LBDµg/L0.094 3/26/14SM18-20 6200B1n-Propylbenzene
ND 0.50 3/27/14 9:14 LBDµg/L0.12 3/26/14SM18-20 6200B1Styrene
ND 0.50 3/27/14 9:14 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 1.0 3/27/14 9:14 LBDµg/L0.080 3/26/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 3/27/14 9:14 LBDµg/L0.090 3/26/14SM18-20 6200B1Toluene
ND 2.0 3/27/14 9:14 LBDµg/L0.14 3/26/14SM18-20 6200B1L-041,2,3-Trichlorobenzene
ND 1.0 3/27/14 9:14 LBDµg/L0.12 3/26/14SM18-20 6200B1L-041,2,4-Trichlorobenzene
ND 0.50 3/27/14 9:14 LBDµg/L0.094 3/26/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 3/27/14 9:14 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 3/27/14 9:14 LBDµg/L0.077 3/26/14SM18-20 6200B1Trichloroethylene
ND 0.50 3/27/14 9:14 LBDµg/L0.15 3/26/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/27/14 9:14 LBDµg/L0.12 3/26/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 3/27/14 9:14 LBDµg/L0.18 3/26/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 3/27/14 9:14 LBDµg/L0.10 3/26/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 3/27/14 9:14 LBDµg/L1.3 3/26/14SM18-20 6200B1Vinyl Acetate
ND 0.50 3/27/14 9:14 LBDµg/L0.13 3/26/14SM18-20 6200B1Vinyl Chloride
ND 1.0 3/27/14 9:14 LBDµg/L0.18 3/26/14SM18-20 6200B1m+p Xylene
ND 0.50 3/27/14 9:14 LBDµg/L0.11 3/26/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 87.2 3/27/14 9:1470-130
Toluene-d8 99.7 3/27/14 9:1470-130
4-Bromofluorobenzene 99.8 3/27/14 9:1470-130
Page 32 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-15
Field Sample #: SW 2774
Sample Matrix: Drinking Water
Sampled: 3/20/2014 14:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/27/14 9:45 LBDµg/L4.7 3/26/14SM18-20 6200B1Acetone
ND 0.50 3/27/14 9:45 LBDµg/L0.079 3/26/14SM18-20 6200B1Benzene
ND 0.50 3/27/14 9:45 LBDµg/L0.044 3/26/14SM18-20 6200B1Bromobenzene
ND 0.50 3/27/14 9:45 LBDµg/L0.22 3/26/14SM18-20 6200B1Bromochloromethane
ND 0.50 3/27/14 9:45 LBDµg/L0.088 3/26/14SM18-20 6200B1Bromodichloromethane
ND 0.50 3/27/14 9:45 LBDµg/L0.21 3/26/14SM18-20 6200B1Bromoform
ND 1.0 3/27/14 9:45 LBDµg/L0.94 3/26/14SM18-20 6200B1Bromomethane
ND 5.0 3/27/14 9:45 LBDµg/L2.4 3/26/14SM18-20 6200B12-Butanone (MEK)
ND 2.0 3/27/14 9:45 LBDµg/L0.054 3/26/14SM18-20 6200B1n-Butylbenzene
ND 0.50 3/27/14 9:45 LBDµg/L0.084 3/26/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 3/27/14 9:45 LBDµg/L0.096 3/26/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 3/27/14 9:45 LBDµg/L0.10 3/26/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 3/27/14 9:45 LBDµg/L0.12 3/26/14SM18-20 6200B1Chlorobenzene
ND 50 3/27/14 9:45 LBDµg/L28 3/26/14SM18-20 6200B1L-04, V-16Ethanol
ND 0.50 3/27/14 9:45 LBDµg/L0.054 3/26/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 3/27/14 9:45 LBDµg/L0.16 3/26/14SM18-20 6200B1Chloroethane
ND 0.50 3/27/14 9:45 LBDµg/L0.14 3/26/14SM18-20 6200B1Chloroform
ND 0.50 3/27/14 9:45 LBDµg/L0.32 3/26/14SM18-20 6200B1Chloromethane
ND 0.50 3/27/14 9:45 LBDµg/L0.070 3/26/14SM18-20 6200B12-Chlorotoluene
ND 0.50 3/27/14 9:45 LBDµg/L0.074 3/26/14SM18-20 6200B14-Chlorotoluene
ND 0.50 3/27/14 9:45 LBDµg/L0.089 3/26/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/27/14 9:45 LBDµg/L0.076 3/26/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 3/27/14 9:45 LBDµg/L0.079 3/26/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 3/27/14 9:45 LBDµg/L0.046 3/26/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 3/27/14 9:45 LBDµg/L0.12 3/26/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/27/14 9:45 LBDµg/L0.16 3/26/14SM18-20 6200B11,1-Dichloroethane
ND 0.50 3/27/14 9:45 LBDµg/L0.19 3/26/14SM18-20 6200B11,2-Dichloroethane
ND 1.0 3/27/14 9:45 LBDµg/L0.21 3/26/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 3/27/14 9:45 LBDµg/L0.15 3/26/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/27/14 9:45 LBDµg/L0.15 3/26/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/27/14 9:45 LBDµg/L0.11 3/26/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 3/27/14 9:45 LBDµg/L0.099 3/26/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 3/27/14 9:45 LBDµg/L0.072 3/26/14SM18-20 6200B1L-042,2-Dichloropropane
ND 0.50 3/27/14 9:45 LBDµg/L0.13 3/26/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 3/27/14 9:45 LBDµg/L0.062 3/26/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 3/27/14 9:45 LBDµg/L0.056 3/26/14SM18-20 6200B1trans-1,3-Dichloropropene
ND 0.50 3/27/14 9:45 LBDµg/L0.18 3/26/14SM18-20 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/27/14 9:45 LBDµg/L0.092 3/26/14SM18-20 6200B1Ethylbenzene
ND 5.0 3/27/14 9:45 LBDµg/L1.5 3/26/14SM18-20 6200B12-Hexanone (MBK)
ND 0.50 3/27/14 9:45 LBDµg/L0.11 3/26/14SM18-20 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/27/14 9:45 LBDµg/L0.12 3/26/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/27/14 9:45 LBDµg/L0.090 3/26/14SM18-20 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/27/14 9:45 LBDµg/L3.2 3/26/14SM18-20 6200B1Methylene Chloride
ND 5.0 3/27/14 9:45 LBDµg/L1.5 3/26/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 33 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-15
Field Sample #: SW 2774
Sample Matrix: Drinking Water
Sampled: 3/20/2014 14:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/27/14 9:45 LBDµg/L0.12 3/26/14SM18-20 6200B1L-04Naphthalene
ND 0.50 3/27/14 9:45 LBDµg/L0.094 3/26/14SM18-20 6200B1n-Propylbenzene
ND 0.50 3/27/14 9:45 LBDµg/L0.12 3/26/14SM18-20 6200B1Styrene
ND 0.50 3/27/14 9:45 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 1.0 3/27/14 9:45 LBDµg/L0.080 3/26/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 3/27/14 9:45 LBDµg/L0.090 3/26/14SM18-20 6200B1Toluene
ND 2.0 3/27/14 9:45 LBDµg/L0.14 3/26/14SM18-20 6200B1L-041,2,3-Trichlorobenzene
ND 1.0 3/27/14 9:45 LBDµg/L0.12 3/26/14SM18-20 6200B1L-041,2,4-Trichlorobenzene
ND 0.50 3/27/14 9:45 LBDµg/L0.094 3/26/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 3/27/14 9:45 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 3/27/14 9:45 LBDµg/L0.077 3/26/14SM18-20 6200B1Trichloroethylene
ND 0.50 3/27/14 9:45 LBDµg/L0.15 3/26/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/27/14 9:45 LBDµg/L0.12 3/26/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 3/27/14 9:45 LBDµg/L0.18 3/26/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 3/27/14 9:45 LBDµg/L0.10 3/26/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 3/27/14 9:45 LBDµg/L1.3 3/26/14SM18-20 6200B1Vinyl Acetate
ND 0.50 3/27/14 9:45 LBDµg/L0.13 3/26/14SM18-20 6200B1Vinyl Chloride
ND 1.0 3/27/14 9:45 LBDµg/L0.18 3/26/14SM18-20 6200B1m+p Xylene
ND 0.50 3/27/14 9:45 LBDµg/L0.11 3/26/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 88.2 3/27/14 9:4570-130
Toluene-d8 98.6 3/27/14 9:4570-130
4-Bromofluorobenzene 97.9 3/27/14 9:4570-130
Page 34 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-16
Field Sample #: SW 2768B
Sample Matrix: Drinking Water
Sampled: 3/20/2014 13:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/27/14 10:16 LBDµg/L4.7 3/26/14SM18-20 6200B1Acetone
ND 0.50 3/27/14 10:16 LBDµg/L0.079 3/26/14SM18-20 6200B1Benzene
ND 0.50 3/27/14 10:16 LBDµg/L0.044 3/26/14SM18-20 6200B1Bromobenzene
ND 0.50 3/27/14 10:16 LBDµg/L0.22 3/26/14SM18-20 6200B1Bromochloromethane
ND 0.50 3/27/14 10:16 LBDµg/L0.088 3/26/14SM18-20 6200B1Bromodichloromethane
ND 0.50 3/27/14 10:16 LBDµg/L0.21 3/26/14SM18-20 6200B1Bromoform
ND 1.0 3/27/14 10:16 LBDµg/L0.94 3/26/14SM18-20 6200B1Bromomethane
ND 5.0 3/27/14 10:16 LBDµg/L2.4 3/26/14SM18-20 6200B12-Butanone (MEK)
ND 2.0 3/27/14 10:16 LBDµg/L0.054 3/26/14SM18-20 6200B1n-Butylbenzene
ND 0.50 3/27/14 10:16 LBDµg/L0.084 3/26/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 3/27/14 10:16 LBDµg/L0.096 3/26/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 3/27/14 10:16 LBDµg/L0.10 3/26/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 3/27/14 10:16 LBDµg/L0.12 3/26/14SM18-20 6200B1Chlorobenzene
ND 50 3/27/14 10:16 LBDµg/L28 3/26/14SM18-20 6200B1L-04, V-16Ethanol
ND 0.50 3/27/14 10:16 LBDµg/L0.054 3/26/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 3/27/14 10:16 LBDµg/L0.16 3/26/14SM18-20 6200B1Chloroethane
ND 0.50 3/27/14 10:16 LBDµg/L0.14 3/26/14SM18-20 6200B1Chloroform
ND 0.50 3/27/14 10:16 LBDµg/L0.32 3/26/14SM18-20 6200B1Chloromethane
ND 0.50 3/27/14 10:16 LBDµg/L0.070 3/26/14SM18-20 6200B12-Chlorotoluene
ND 0.50 3/27/14 10:16 LBDµg/L0.074 3/26/14SM18-20 6200B14-Chlorotoluene
ND 0.50 3/27/14 10:16 LBDµg/L0.089 3/26/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/27/14 10:16 LBDµg/L0.076 3/26/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 3/27/14 10:16 LBDµg/L0.079 3/26/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 3/27/14 10:16 LBDµg/L0.046 3/26/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 3/27/14 10:16 LBDµg/L0.12 3/26/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/27/14 10:16 LBDµg/L0.16 3/26/14SM18-20 6200B11,1-Dichloroethane
ND 0.50 3/27/14 10:16 LBDµg/L0.19 3/26/14SM18-20 6200B11,2-Dichloroethane
ND 1.0 3/27/14 10:16 LBDµg/L0.21 3/26/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 3/27/14 10:16 LBDµg/L0.15 3/26/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/27/14 10:16 LBDµg/L0.15 3/26/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/27/14 10:16 LBDµg/L0.11 3/26/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 3/27/14 10:16 LBDµg/L0.099 3/26/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 3/27/14 10:16 LBDµg/L0.072 3/26/14SM18-20 6200B1L-042,2-Dichloropropane
ND 0.50 3/27/14 10:16 LBDµg/L0.13 3/26/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 3/27/14 10:16 LBDµg/L0.062 3/26/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 3/27/14 10:16 LBDµg/L0.056 3/26/14SM18-20 6200B1trans-1,3-Dichloropropene
ND 0.50 3/27/14 10:16 LBDµg/L0.18 3/26/14SM18-20 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/27/14 10:16 LBDµg/L0.092 3/26/14SM18-20 6200B1Ethylbenzene
ND 5.0 3/27/14 10:16 LBDµg/L1.5 3/26/14SM18-20 6200B12-Hexanone (MBK)
ND 0.50 3/27/14 10:16 LBDµg/L0.11 3/26/14SM18-20 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/27/14 10:16 LBDµg/L0.12 3/26/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/27/14 10:16 LBDµg/L0.090 3/26/14SM18-20 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/27/14 10:16 LBDµg/L3.2 3/26/14SM18-20 6200B1Methylene Chloride
ND 5.0 3/27/14 10:16 LBDµg/L1.5 3/26/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 35 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-16
Field Sample #: SW 2768B
Sample Matrix: Drinking Water
Sampled: 3/20/2014 13:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/27/14 10:16 LBDµg/L0.12 3/26/14SM18-20 6200B1L-04Naphthalene
ND 0.50 3/27/14 10:16 LBDµg/L0.094 3/26/14SM18-20 6200B1n-Propylbenzene
ND 0.50 3/27/14 10:16 LBDµg/L0.12 3/26/14SM18-20 6200B1Styrene
ND 0.50 3/27/14 10:16 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 1.0 3/27/14 10:16 LBDµg/L0.080 3/26/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 3/27/14 10:16 LBDµg/L0.090 3/26/14SM18-20 6200B1Toluene
ND 2.0 3/27/14 10:16 LBDµg/L0.14 3/26/14SM18-20 6200B1L-041,2,3-Trichlorobenzene
ND 1.0 3/27/14 10:16 LBDµg/L0.12 3/26/14SM18-20 6200B1L-041,2,4-Trichlorobenzene
ND 0.50 3/27/14 10:16 LBDµg/L0.094 3/26/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 3/27/14 10:16 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 3/27/14 10:16 LBDµg/L0.077 3/26/14SM18-20 6200B1Trichloroethylene
ND 0.50 3/27/14 10:16 LBDµg/L0.15 3/26/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/27/14 10:16 LBDµg/L0.12 3/26/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 3/27/14 10:16 LBDµg/L0.18 3/26/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 3/27/14 10:16 LBDµg/L0.10 3/26/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 3/27/14 10:16 LBDµg/L1.3 3/26/14SM18-20 6200B1Vinyl Acetate
ND 0.50 3/27/14 10:16 LBDµg/L0.13 3/26/14SM18-20 6200B1Vinyl Chloride
ND 1.0 3/27/14 10:16 LBDµg/L0.18 3/26/14SM18-20 6200B1m+p Xylene
ND 0.50 3/27/14 10:16 LBDµg/L0.11 3/26/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 87.4 3/27/14 10:1670-130
Toluene-d8 100 3/27/14 10:1670-130
4-Bromofluorobenzene 98.7 3/27/14 10:1670-130
Page 36 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-17
Field Sample #: SW 2779
Sample Matrix: Drinking Water
Sampled: 3/20/2014 13:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/27/14 10:47 LBDµg/L4.7 3/26/14SM18-20 6200B1Acetone
ND 0.50 3/27/14 10:47 LBDµg/L0.079 3/26/14SM18-20 6200B1Benzene
ND 0.50 3/27/14 10:47 LBDµg/L0.044 3/26/14SM18-20 6200B1Bromobenzene
ND 0.50 3/27/14 10:47 LBDµg/L0.22 3/26/14SM18-20 6200B1Bromochloromethane
ND 0.50 3/27/14 10:47 LBDµg/L0.088 3/26/14SM18-20 6200B1Bromodichloromethane
ND 0.50 3/27/14 10:47 LBDµg/L0.21 3/26/14SM18-20 6200B1Bromoform
ND 1.0 3/27/14 10:47 LBDµg/L0.94 3/26/14SM18-20 6200B1Bromomethane
ND 5.0 3/27/14 10:47 LBDµg/L2.4 3/26/14SM18-20 6200B12-Butanone (MEK)
ND 2.0 3/27/14 10:47 LBDµg/L0.054 3/26/14SM18-20 6200B1n-Butylbenzene
ND 0.50 3/27/14 10:47 LBDµg/L0.084 3/26/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 3/27/14 10:47 LBDµg/L0.096 3/26/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 3/27/14 10:47 LBDµg/L0.10 3/26/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 3/27/14 10:47 LBDµg/L0.12 3/26/14SM18-20 6200B1Chlorobenzene
ND 50 3/27/14 10:47 LBDµg/L28 3/26/14SM18-20 6200B1L-04, V-16Ethanol
ND 0.50 3/27/14 10:47 LBDµg/L0.054 3/26/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 3/27/14 10:47 LBDµg/L0.16 3/26/14SM18-20 6200B1Chloroethane
ND 0.50 3/27/14 10:47 LBDµg/L0.14 3/26/14SM18-20 6200B1Chloroform
ND 0.50 3/27/14 10:47 LBDµg/L0.32 3/26/14SM18-20 6200B1Chloromethane
ND 0.50 3/27/14 10:47 LBDµg/L0.070 3/26/14SM18-20 6200B12-Chlorotoluene
ND 0.50 3/27/14 10:47 LBDµg/L0.074 3/26/14SM18-20 6200B14-Chlorotoluene
ND 0.50 3/27/14 10:47 LBDµg/L0.089 3/26/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/27/14 10:47 LBDµg/L0.076 3/26/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 3/27/14 10:47 LBDµg/L0.079 3/26/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 3/27/14 10:47 LBDµg/L0.046 3/26/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 3/27/14 10:47 LBDµg/L0.12 3/26/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/27/14 10:47 LBDµg/L0.16 3/26/14SM18-20 6200B11,1-Dichloroethane
ND 0.50 3/27/14 10:47 LBDµg/L0.19 3/26/14SM18-20 6200B11,2-Dichloroethane
ND 1.0 3/27/14 10:47 LBDµg/L0.21 3/26/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 3/27/14 10:47 LBDµg/L0.15 3/26/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/27/14 10:47 LBDµg/L0.15 3/26/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/27/14 10:47 LBDµg/L0.11 3/26/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 3/27/14 10:47 LBDµg/L0.099 3/26/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 3/27/14 10:47 LBDµg/L0.072 3/26/14SM18-20 6200B1L-042,2-Dichloropropane
ND 0.50 3/27/14 10:47 LBDµg/L0.13 3/26/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 3/27/14 10:47 LBDµg/L0.062 3/26/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 3/27/14 10:47 LBDµg/L0.056 3/26/14SM18-20 6200B1trans-1,3-Dichloropropene
ND 0.50 3/27/14 10:47 LBDµg/L0.18 3/26/14SM18-20 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/27/14 10:47 LBDµg/L0.092 3/26/14SM18-20 6200B1Ethylbenzene
ND 5.0 3/27/14 10:47 LBDµg/L1.5 3/26/14SM18-20 6200B12-Hexanone (MBK)
ND 0.50 3/27/14 10:47 LBDµg/L0.11 3/26/14SM18-20 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/27/14 10:47 LBDµg/L0.12 3/26/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/27/14 10:47 LBDµg/L0.090 3/26/14SM18-20 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/27/14 10:47 LBDµg/L3.2 3/26/14SM18-20 6200B1Methylene Chloride
ND 5.0 3/27/14 10:47 LBDµg/L1.5 3/26/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 37 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-17
Field Sample #: SW 2779
Sample Matrix: Drinking Water
Sampled: 3/20/2014 13:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/27/14 10:47 LBDµg/L0.12 3/26/14SM18-20 6200B1L-04Naphthalene
ND 0.50 3/27/14 10:47 LBDµg/L0.094 3/26/14SM18-20 6200B1n-Propylbenzene
ND 0.50 3/27/14 10:47 LBDµg/L0.12 3/26/14SM18-20 6200B1Styrene
ND 0.50 3/27/14 10:47 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 1.0 3/27/14 10:47 LBDµg/L0.080 3/26/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 3/27/14 10:47 LBDµg/L0.090 3/26/14SM18-20 6200B1Toluene
ND 2.0 3/27/14 10:47 LBDµg/L0.14 3/26/14SM18-20 6200B1L-041,2,3-Trichlorobenzene
ND 1.0 3/27/14 10:47 LBDµg/L0.12 3/26/14SM18-20 6200B1L-041,2,4-Trichlorobenzene
ND 0.50 3/27/14 10:47 LBDµg/L0.094 3/26/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 3/27/14 10:47 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 3/27/14 10:47 LBDµg/L0.077 3/26/14SM18-20 6200B1Trichloroethylene
ND 0.50 3/27/14 10:47 LBDµg/L0.15 3/26/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/27/14 10:47 LBDµg/L0.12 3/26/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 3/27/14 10:47 LBDµg/L0.18 3/26/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 3/27/14 10:47 LBDµg/L0.10 3/26/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 3/27/14 10:47 LBDµg/L1.3 3/26/14SM18-20 6200B1Vinyl Acetate
ND 0.50 3/27/14 10:47 LBDµg/L0.13 3/26/14SM18-20 6200B1Vinyl Chloride
ND 1.0 3/27/14 10:47 LBDµg/L0.18 3/26/14SM18-20 6200B1m+p Xylene
ND 0.50 3/27/14 10:47 LBDµg/L0.11 3/26/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 86.9 3/27/14 10:4770-130
Toluene-d8 99.8 3/27/14 10:4770-130
4-Bromofluorobenzene 96.6 3/27/14 10:4770-130
Page 38 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-18
Field Sample #: SW 2765 INF
Sample Matrix: Drinking Water
Sampled: 3/20/2014 14:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/27/14 16:00 LBDµg/L4.7 3/27/14SM18-20 6200B1Acetone
ND 0.50 3/27/14 16:00 LBDµg/L0.079 3/27/14SM18-20 6200B1Benzene
ND 0.50 3/27/14 16:00 LBDµg/L0.044 3/27/14SM18-20 6200B1Bromobenzene
ND 0.50 3/27/14 16:00 LBDµg/L0.22 3/27/14SM18-20 6200B1Bromochloromethane
ND 0.50 3/27/14 16:00 LBDµg/L0.088 3/27/14SM18-20 6200B1Bromodichloromethane
ND 0.50 3/27/14 16:00 LBDµg/L0.21 3/27/14SM18-20 6200B1Bromoform
ND 1.0 3/27/14 16:00 LBDµg/L0.94 3/27/14SM18-20 6200B1Bromomethane
ND 5.0 3/27/14 16:00 LBDµg/L2.4 3/27/14SM18-20 6200B12-Butanone (MEK)
ND 2.0 3/27/14 16:00 LBDµg/L0.054 3/27/14SM18-20 6200B1n-Butylbenzene
0.11 0.50 3/27/14 16:00 LBDµg/L0.084 3/27/14SM18-20 6200B1Jsec-Butylbenzene
ND 0.50 3/27/14 16:00 LBDµg/L0.096 3/27/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 3/27/14 16:00 LBDµg/L0.10 3/27/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 3/27/14 16:00 LBDµg/L0.12 3/27/14SM18-20 6200B1Chlorobenzene
ND 50 3/27/14 16:00 LBDµg/L28 3/27/14SM18-20 6200B1R-05, V-16Ethanol
ND 0.50 3/27/14 16:00 LBDµg/L0.054 3/27/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 3/27/14 16:00 LBDµg/L0.16 3/27/14SM18-20 6200B1Chloroethane
ND 0.50 3/27/14 16:00 LBDµg/L0.14 3/27/14SM18-20 6200B1Chloroform
ND 0.50 3/27/14 16:00 LBDµg/L0.32 3/27/14SM18-20 6200B1Chloromethane
ND 0.50 3/27/14 16:00 LBDµg/L0.070 3/27/14SM18-20 6200B12-Chlorotoluene
ND 0.50 3/27/14 16:00 LBDµg/L0.074 3/27/14SM18-20 6200B14-Chlorotoluene
ND 0.50 3/27/14 16:00 LBDµg/L0.089 3/27/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/27/14 16:00 LBDµg/L0.076 3/27/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 3/27/14 16:00 LBDµg/L0.079 3/27/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 3/27/14 16:00 LBDµg/L0.046 3/27/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 3/27/14 16:00 LBDµg/L0.12 3/27/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/27/14 16:00 LBDµg/L0.16 3/27/14SM18-20 6200B11,1-Dichloroethane
20 0.50 3/27/14 16:00 LBDµg/L0.19 3/27/14SM18-20 6200B11,2-Dichloroethane
ND 1.0 3/27/14 16:00 LBDµg/L0.21 3/27/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 3/27/14 16:00 LBDµg/L0.15 3/27/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/27/14 16:00 LBDµg/L0.15 3/27/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/27/14 16:00 LBDµg/L0.11 3/27/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 3/27/14 16:00 LBDµg/L0.099 3/27/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 3/27/14 16:00 LBDµg/L0.072 3/27/14SM18-20 6200B12,2-Dichloropropane
ND 0.50 3/27/14 16:00 LBDµg/L0.13 3/27/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 3/27/14 16:00 LBDµg/L0.062 3/27/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 3/27/14 16:00 LBDµg/L0.056 3/27/14SM18-20 6200B1trans-1,3-Dichloropropene
140 0.50 3/27/14 16:00 LBDµg/L0.18 3/27/14SM18-20 6200B1Diisopropyl Ether (DIPE)
0.12 0.50 3/27/14 16:00 LBDµg/L0.092 3/27/14SM18-20 6200B1JEthylbenzene
ND 5.0 3/27/14 16:00 LBDµg/L1.5 3/27/14SM18-20 6200B12-Hexanone (MBK)
0.25 0.50 3/27/14 16:00 LBDµg/L0.11 3/27/14SM18-20 6200B1JIsopropylbenzene (Cumene)
ND 0.50 3/27/14 16:00 LBDµg/L0.12 3/27/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
100 0.50 3/27/14 16:00 LBDµg/L0.090 3/27/14SM18-20 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/27/14 16:00 LBDµg/L3.2 3/27/14SM18-20 6200B1Methylene Chloride
ND 5.0 3/27/14 16:00 LBDµg/L1.5 3/27/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 39 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-18
Field Sample #: SW 2765 INF
Sample Matrix: Drinking Water
Sampled: 3/20/2014 14:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/27/14 16:00 LBDµg/L0.12 3/27/14SM18-20 6200B1L-04Naphthalene
ND 0.50 3/27/14 16:00 LBDµg/L0.094 3/27/14SM18-20 6200B1n-Propylbenzene
ND 0.50 3/27/14 16:00 LBDµg/L0.12 3/27/14SM18-20 6200B1Styrene
ND 0.50 3/27/14 16:00 LBDµg/L0.12 3/27/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 1.0 3/27/14 16:00 LBDµg/L0.080 3/27/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 3/27/14 16:00 LBDµg/L0.090 3/27/14SM18-20 6200B1Toluene
ND 2.0 3/27/14 16:00 LBDµg/L0.14 3/27/14SM18-20 6200B1L-041,2,3-Trichlorobenzene
ND 1.0 3/27/14 16:00 LBDµg/L0.12 3/27/14SM18-20 6200B1L-041,2,4-Trichlorobenzene
ND 0.50 3/27/14 16:00 LBDµg/L0.094 3/27/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 3/27/14 16:00 LBDµg/L0.12 3/27/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 3/27/14 16:00 LBDµg/L0.077 3/27/14SM18-20 6200B1Trichloroethylene
ND 0.50 3/27/14 16:00 LBDµg/L0.15 3/27/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/27/14 16:00 LBDµg/L0.12 3/27/14SM18-20 6200B11,2,3-Trichloropropane
0.21 0.50 3/27/14 16:00 LBDµg/L0.18 3/27/14SM18-20 6200B1J1,2,4-Trimethylbenzene
ND 0.50 3/27/14 16:00 LBDµg/L0.10 3/27/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 3/27/14 16:00 LBDµg/L1.3 3/27/14SM18-20 6200B1Vinyl Acetate
ND 0.50 3/27/14 16:00 LBDµg/L0.13 3/27/14SM18-20 6200B1Vinyl Chloride
ND 1.0 3/27/14 16:00 LBDµg/L0.18 3/27/14SM18-20 6200B1m+p Xylene
ND 0.50 3/27/14 16:00 LBDµg/L0.11 3/27/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 85.0 3/27/14 16:0070-130
Toluene-d8 102 3/27/14 16:0070-130
4-Bromofluorobenzene 99.5 3/27/14 16:0070-130
Page 40 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-19
Field Sample #: SW 2765 EFF
Sample Matrix: Drinking Water
Sampled: 3/20/2014 15:01
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/27/14 11:18 LBDµg/L4.7 3/26/14SM18-20 6200B1Acetone
ND 0.50 3/27/14 11:18 LBDµg/L0.079 3/26/14SM18-20 6200B1Benzene
ND 0.50 3/27/14 11:18 LBDµg/L0.044 3/26/14SM18-20 6200B1Bromobenzene
ND 0.50 3/27/14 11:18 LBDµg/L0.22 3/26/14SM18-20 6200B1Bromochloromethane
ND 0.50 3/27/14 11:18 LBDµg/L0.088 3/26/14SM18-20 6200B1Bromodichloromethane
ND 0.50 3/27/14 11:18 LBDµg/L0.21 3/26/14SM18-20 6200B1Bromoform
ND 1.0 3/27/14 11:18 LBDµg/L0.94 3/26/14SM18-20 6200B1Bromomethane
ND 5.0 3/27/14 11:18 LBDµg/L2.4 3/26/14SM18-20 6200B12-Butanone (MEK)
ND 2.0 3/27/14 11:18 LBDµg/L0.054 3/26/14SM18-20 6200B1n-Butylbenzene
ND 0.50 3/27/14 11:18 LBDµg/L0.084 3/26/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 3/27/14 11:18 LBDµg/L0.096 3/26/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 3/27/14 11:18 LBDµg/L0.10 3/26/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 3/27/14 11:18 LBDµg/L0.12 3/26/14SM18-20 6200B1Chlorobenzene
ND 50 3/27/14 11:18 LBDµg/L28 3/26/14SM18-20 6200B1L-04, V-16Ethanol
ND 0.50 3/27/14 11:18 LBDµg/L0.054 3/26/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 3/27/14 11:18 LBDµg/L0.16 3/26/14SM18-20 6200B1Chloroethane
ND 0.50 3/27/14 11:18 LBDµg/L0.14 3/26/14SM18-20 6200B1Chloroform
ND 0.50 3/27/14 11:18 LBDµg/L0.32 3/26/14SM18-20 6200B1Chloromethane
ND 0.50 3/27/14 11:18 LBDµg/L0.070 3/26/14SM18-20 6200B12-Chlorotoluene
ND 0.50 3/27/14 11:18 LBDµg/L0.074 3/26/14SM18-20 6200B14-Chlorotoluene
ND 0.50 3/27/14 11:18 LBDµg/L0.089 3/26/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/27/14 11:18 LBDµg/L0.076 3/26/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 3/27/14 11:18 LBDµg/L0.079 3/26/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 3/27/14 11:18 LBDµg/L0.046 3/26/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 3/27/14 11:18 LBDµg/L0.12 3/26/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/27/14 11:18 LBDµg/L0.16 3/26/14SM18-20 6200B11,1-Dichloroethane
ND 0.50 3/27/14 11:18 LBDµg/L0.19 3/26/14SM18-20 6200B11,2-Dichloroethane
ND 1.0 3/27/14 11:18 LBDµg/L0.21 3/26/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 3/27/14 11:18 LBDµg/L0.15 3/26/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/27/14 11:18 LBDµg/L0.15 3/26/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/27/14 11:18 LBDµg/L0.11 3/26/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 3/27/14 11:18 LBDµg/L0.099 3/26/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 3/27/14 11:18 LBDµg/L0.072 3/26/14SM18-20 6200B1L-042,2-Dichloropropane
ND 0.50 3/27/14 11:18 LBDµg/L0.13 3/26/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 3/27/14 11:18 LBDµg/L0.062 3/26/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 3/27/14 11:18 LBDµg/L0.056 3/26/14SM18-20 6200B1trans-1,3-Dichloropropene
0.20 0.50 3/27/14 11:18 LBDµg/L0.18 3/26/14SM18-20 6200B1JDiisopropyl Ether (DIPE)
ND 0.50 3/27/14 11:18 LBDµg/L0.092 3/26/14SM18-20 6200B1Ethylbenzene
ND 5.0 3/27/14 11:18 LBDµg/L1.5 3/26/14SM18-20 6200B12-Hexanone (MBK)
ND 0.50 3/27/14 11:18 LBDµg/L0.11 3/26/14SM18-20 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/27/14 11:18 LBDµg/L0.12 3/26/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
0.62 0.50 3/27/14 11:18 LBDµg/L0.090 3/26/14SM18-20 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/27/14 11:18 LBDµg/L3.2 3/26/14SM18-20 6200B1Methylene Chloride
ND 5.0 3/27/14 11:18 LBDµg/L1.5 3/26/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 41 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-19
Field Sample #: SW 2765 EFF
Sample Matrix: Drinking Water
Sampled: 3/20/2014 15:01
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/27/14 11:18 LBDµg/L0.12 3/26/14SM18-20 6200B1L-04Naphthalene
ND 0.50 3/27/14 11:18 LBDµg/L0.094 3/26/14SM18-20 6200B1n-Propylbenzene
ND 0.50 3/27/14 11:18 LBDµg/L0.12 3/26/14SM18-20 6200B1Styrene
ND 0.50 3/27/14 11:18 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 1.0 3/27/14 11:18 LBDµg/L0.080 3/26/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 3/27/14 11:18 LBDµg/L0.090 3/26/14SM18-20 6200B1Toluene
ND 2.0 3/27/14 11:18 LBDµg/L0.14 3/26/14SM18-20 6200B1L-041,2,3-Trichlorobenzene
ND 1.0 3/27/14 11:18 LBDµg/L0.12 3/26/14SM18-20 6200B1L-041,2,4-Trichlorobenzene
ND 0.50 3/27/14 11:18 LBDµg/L0.094 3/26/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 3/27/14 11:18 LBDµg/L0.12 3/26/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 3/27/14 11:18 LBDµg/L0.077 3/26/14SM18-20 6200B1Trichloroethylene
ND 0.50 3/27/14 11:18 LBDµg/L0.15 3/26/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/27/14 11:18 LBDµg/L0.12 3/26/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 3/27/14 11:18 LBDµg/L0.18 3/26/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 3/27/14 11:18 LBDµg/L0.10 3/26/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 3/27/14 11:18 LBDµg/L1.3 3/26/14SM18-20 6200B1Vinyl Acetate
ND 0.50 3/27/14 11:18 LBDµg/L0.13 3/26/14SM18-20 6200B1Vinyl Chloride
ND 1.0 3/27/14 11:18 LBDµg/L0.18 3/26/14SM18-20 6200B1m+p Xylene
ND 0.50 3/27/14 11:18 LBDµg/L0.11 3/26/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 86.8 3/27/14 11:1870-130
Toluene-d8 98.9 3/27/14 11:1870-130
4-Bromofluorobenzene 96.8 3/27/14 11:1870-130
Page 42 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-20
Field Sample #: SW 2765 MID
Sample Matrix: Drinking Water
Sampled: 3/20/2014 14:51
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/27/14 14:58 LBDµg/L4.7 3/27/14SM18-20 6200B1Acetone
ND 0.50 3/27/14 14:58 LBDµg/L0.079 3/27/14SM18-20 6200B1Benzene
ND 0.50 3/27/14 14:58 LBDµg/L0.044 3/27/14SM18-20 6200B1Bromobenzene
ND 0.50 3/27/14 14:58 LBDµg/L0.22 3/27/14SM18-20 6200B1Bromochloromethane
ND 0.50 3/27/14 14:58 LBDµg/L0.088 3/27/14SM18-20 6200B1Bromodichloromethane
ND 0.50 3/27/14 14:58 LBDµg/L0.21 3/27/14SM18-20 6200B1Bromoform
ND 1.0 3/27/14 14:58 LBDµg/L0.94 3/27/14SM18-20 6200B1Bromomethane
ND 5.0 3/27/14 14:58 LBDµg/L2.4 3/27/14SM18-20 6200B12-Butanone (MEK)
ND 2.0 3/27/14 14:58 LBDµg/L0.054 3/27/14SM18-20 6200B1n-Butylbenzene
ND 0.50 3/27/14 14:58 LBDµg/L0.084 3/27/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 3/27/14 14:58 LBDµg/L0.096 3/27/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 3/27/14 14:58 LBDµg/L0.10 3/27/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 3/27/14 14:58 LBDµg/L0.12 3/27/14SM18-20 6200B1Chlorobenzene
ND 50 3/27/14 14:58 LBDµg/L28 3/27/14SM18-20 6200B1R-05, V-16Ethanol
ND 0.50 3/27/14 14:58 LBDµg/L0.054 3/27/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 3/27/14 14:58 LBDµg/L0.16 3/27/14SM18-20 6200B1Chloroethane
ND 0.50 3/27/14 14:58 LBDµg/L0.14 3/27/14SM18-20 6200B1Chloroform
ND 0.50 3/27/14 14:58 LBDµg/L0.32 3/27/14SM18-20 6200B1Chloromethane
ND 0.50 3/27/14 14:58 LBDµg/L0.070 3/27/14SM18-20 6200B12-Chlorotoluene
ND 0.50 3/27/14 14:58 LBDµg/L0.074 3/27/14SM18-20 6200B14-Chlorotoluene
ND 0.50 3/27/14 14:58 LBDµg/L0.089 3/27/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/27/14 14:58 LBDµg/L0.076 3/27/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 3/27/14 14:58 LBDµg/L0.079 3/27/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 3/27/14 14:58 LBDµg/L0.046 3/27/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 3/27/14 14:58 LBDµg/L0.12 3/27/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/27/14 14:58 LBDµg/L0.16 3/27/14SM18-20 6200B11,1-Dichloroethane
ND 0.50 3/27/14 14:58 LBDµg/L0.19 3/27/14SM18-20 6200B11,2-Dichloroethane
ND 1.0 3/27/14 14:58 LBDµg/L0.21 3/27/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 3/27/14 14:58 LBDµg/L0.15 3/27/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/27/14 14:58 LBDµg/L0.15 3/27/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/27/14 14:58 LBDµg/L0.11 3/27/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 3/27/14 14:58 LBDµg/L0.099 3/27/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 3/27/14 14:58 LBDµg/L0.072 3/27/14SM18-20 6200B12,2-Dichloropropane
ND 0.50 3/27/14 14:58 LBDµg/L0.13 3/27/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 3/27/14 14:58 LBDµg/L0.062 3/27/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 3/27/14 14:58 LBDµg/L0.056 3/27/14SM18-20 6200B1trans-1,3-Dichloropropene
ND 0.50 3/27/14 14:58 LBDµg/L0.18 3/27/14SM18-20 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/27/14 14:58 LBDµg/L0.092 3/27/14SM18-20 6200B1Ethylbenzene
ND 5.0 3/27/14 14:58 LBDµg/L1.5 3/27/14SM18-20 6200B12-Hexanone (MBK)
ND 0.50 3/27/14 14:58 LBDµg/L0.11 3/27/14SM18-20 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/27/14 14:58 LBDµg/L0.12 3/27/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/27/14 14:58 LBDµg/L0.090 3/27/14SM18-20 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/27/14 14:58 LBDµg/L3.2 3/27/14SM18-20 6200B1Methylene Chloride
ND 5.0 3/27/14 14:58 LBDµg/L1.5 3/27/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 43 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/21/2014
Work Order: 14C0693Sample Description:Project Location: Harold South
Sample ID: 14C0693-20
Field Sample #: SW 2765 MID
Sample Matrix: Drinking Water
Sampled: 3/20/2014 14:51
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.0 3/27/14 14:58 LBDµg/L0.12 3/27/14SM18-20 6200B1L-04Naphthalene
ND 0.50 3/27/14 14:58 LBDµg/L0.094 3/27/14SM18-20 6200B1n-Propylbenzene
ND 0.50 3/27/14 14:58 LBDµg/L0.12 3/27/14SM18-20 6200B1Styrene
ND 0.50 3/27/14 14:58 LBDµg/L0.12 3/27/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 1.0 3/27/14 14:58 LBDµg/L0.080 3/27/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 3/27/14 14:58 LBDµg/L0.090 3/27/14SM18-20 6200B1Toluene
ND 2.0 3/27/14 14:58 LBDµg/L0.14 3/27/14SM18-20 6200B1L-041,2,3-Trichlorobenzene
ND 1.0 3/27/14 14:58 LBDµg/L0.12 3/27/14SM18-20 6200B1L-041,2,4-Trichlorobenzene
ND 0.50 3/27/14 14:58 LBDµg/L0.094 3/27/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 3/27/14 14:58 LBDµg/L0.12 3/27/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 3/27/14 14:58 LBDµg/L0.077 3/27/14SM18-20 6200B1Trichloroethylene
ND 0.50 3/27/14 14:58 LBDµg/L0.15 3/27/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/27/14 14:58 LBDµg/L0.12 3/27/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 3/27/14 14:58 LBDµg/L0.18 3/27/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 3/27/14 14:58 LBDµg/L0.10 3/27/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 3/27/14 14:58 LBDµg/L1.3 3/27/14SM18-20 6200B1Vinyl Acetate
ND 0.50 3/27/14 14:58 LBDµg/L0.13 3/27/14SM18-20 6200B1Vinyl Chloride
ND 1.0 3/27/14 14:58 LBDµg/L0.18 3/27/14SM18-20 6200B1m+p Xylene
ND 0.50 3/27/14 14:58 LBDµg/L0.11 3/27/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 88.2 3/27/14 14:5870-130
Toluene-d8 99.0 3/27/14 14:5870-130
4-Bromofluorobenzene 98.4 3/27/14 14:5870-130
Page 44 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 5030B-SM18-20 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B092577 03/26/1455.0014C0693-02 [MW-3]
B092577 03/26/1455.0014C0693-03 [MW-4]
B092577 03/26/1455.0014C0693-04 [MW-5]
B092577 03/26/1455.0014C0693-05 [MW-6]
B092577 03/26/1455.0014C0693-06 [MW-7]
B092577 03/26/1455.0014C0693-07 [MW-9]
B092577 03/26/1455.0014C0693-08 [MW-10]
B092577 03/26/1455.0014C0693-09 [MW-11]
B092577 03/26/1455.0014C0693-10 [MW-12]
B092577 03/26/1455.0014C0693-11 [MW-13]
B092577 03/26/1455.0014C0693-12 [MW-15]
B092577 03/26/1455.0014C0693-13 [SW 2773]
B092577 03/26/1455.0014C0693-14 [SW 2760]
B092577 03/26/1455.0014C0693-15 [SW 2774]
B092577 03/26/1455.0014C0693-16 [SW 2768B]
B092577 03/26/1455.0014C0693-17 [SW 2779]
B092577 03/26/1455.0014C0693-19 [SW 2765 EFF]
Prep Method: SW-846 5030B-SM18-20 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B092651 03/27/1455.0014C0693-01 [MW-1A]
B092651 03/27/1455.0014C0693-18 [SW 2765 INF]
B092651 03/27/1455.0014C0693-20 [SW 2765 MID]
Page 45 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B092577 - SW-846 5030B
Blank (B092577-BLK1) Prepared: 03/26/14 Analyzed: 03/27/14
Acetone µg/L50ND
Benzene µg/L0.50ND
Bromobenzene µg/L0.50ND
Bromochloromethane µg/L0.50ND
Bromodichloromethane µg/L0.50ND
Bromoform µg/L0.50ND
Bromomethane µg/L1.0ND
2-Butanone (MEK)µg/L5.0ND
n-Butylbenzene µg/L0.50ND
sec-Butylbenzene µg/L0.50ND
tert-Butylbenzene µg/L0.50ND
Carbon Tetrachloride µg/L0.50ND
Chlorobenzene µg/L0.50ND
Ethanol µg/L50 L-04, V-16ND
Chlorodibromomethane µg/L0.50ND
Chloroethane µg/L0.50ND
Chloroform µg/L0.50ND
Chloromethane µg/L0.50ND
2-Chlorotoluene µg/L0.50ND
4-Chlorotoluene µg/L0.50ND
1,2-Dibromoethane (EDB)µg/L0.50ND
1,2-Dichlorobenzene µg/L0.50ND
1,3-Dichlorobenzene µg/L0.50ND
1,4-Dichlorobenzene µg/L0.50ND
Dichlorodifluoromethane (Freon 12)µg/L0.50ND
1,1-Dichloroethane µg/L0.50ND
1,2-Dichloroethane µg/L0.50ND
1,1-Dichloroethylene µg/L0.50ND
cis-1,2-Dichloroethylene µg/L0.50ND
trans-1,2-Dichloroethylene µg/L0.50ND
1,2-Dichloropropane µg/L0.50ND
1,3-Dichloropropane µg/L0.50ND
2,2-Dichloropropane µg/L0.50 L-04ND
1,1-Dichloropropene µg/L0.50ND
cis-1,3-Dichloropropene µg/L0.50ND
trans-1,3-Dichloropropene µg/L0.50ND
Diisopropyl Ether (DIPE)µg/L0.50ND
Ethylbenzene µg/L0.50ND
2-Hexanone (MBK)µg/L5.0ND
Isopropylbenzene (Cumene)µg/L0.50ND
p-Isopropyltoluene (p-Cymene)µg/L0.50ND
Methyl tert-Butyl Ether (MTBE)µg/L0.50ND
Methylene Chloride µg/L5.0ND
4-Methyl-2-pentanone (MIBK)µg/L5.0ND
Naphthalene µg/L0.50 L-04ND
n-Propylbenzene µg/L0.50ND
Styrene µg/L0.50ND
1,1,2,2-Tetrachloroethane µg/L0.50ND
Tetrachloroethylene µg/L0.50ND
Toluene µg/L0.50ND
1,2,3-Trichlorobenzene µg/L0.50 L-04ND
1,2,4-Trichlorobenzene µg/L0.50 L-04ND
Page 46 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B092577 - SW-846 5030B
Blank (B092577-BLK1) Prepared: 03/26/14 Analyzed: 03/27/14
1,1,1-Trichloroethane µg/L0.50ND
1,1,2-Trichloroethane µg/L0.50ND
Trichloroethylene µg/L0.50ND
Trichlorofluoromethane (Freon 11)µg/L0.50ND
1,2,3-Trichloropropane µg/L0.50ND
1,2,4-Trimethylbenzene µg/L0.50ND
1,3,5-Trimethylbenzene µg/L0.50ND
Vinyl Acetate µg/L5.0ND
Vinyl Chloride µg/L0.50ND
m+p Xylene µg/L1.0ND
o-Xylene µg/L0.50ND
µg/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 84.921.2
µg/L 25.0 70-130Surrogate: Toluene-d8 99.925.0
µg/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10025.1
LCS (B092577-BS1) Prepared: 03/26/14 Analyzed: 03/27/14
Acetone µg/L50 100 70-13072.0 †72.0
Benzene µg/L0.50 10.0 70-13011011.0
Bromobenzene µg/L0.50 10.0 70-13099.49.94
Bromochloromethane µg/L0.50 10.0 70-13011411.4
Bromodichloromethane µg/L0.50 10.0 70-13080.08.00
Bromoform µg/L0.50 10.0 L-0770-13066.0 *6.60
Bromomethane µg/L1.0 10.0 60-140112 †11.2
2-Butanone (MEK)µg/L5.0 100 70-13095.8 †95.8
n-Butylbenzene µg/L0.50 10.0 70-13093.79.37
sec-Butylbenzene µg/L0.50 10.0 70-13011211.2
tert-Butylbenzene µg/L0.50 10.0 70-13010510.5
Carbon Tetrachloride µg/L0.50 10.0 70-13079.37.93
Chlorobenzene µg/L0.50 10.0 70-13011111.1
Ethanol µg/L50 100 L-04, V-1670-13058.5 *58.5
Chlorodibromomethane µg/L0.50 10.0 70-13071.57.15
Chloroethane µg/L0.50 10.0 60-14073.17.31
Chloroform µg/L0.50 10.0 70-13099.29.92
Chloromethane µg/L0.50 10.0 60-14097.7 †9.77
2-Chlorotoluene µg/L0.50 10.0 70-13010310.3
4-Chlorotoluene µg/L0.50 10.0 70-13010210.2
1,2-Dibromoethane (EDB)µg/L0.50 10.0 70-13010310.3
1,2-Dichlorobenzene µg/L0.50 10.0 70-13010410.4
1,3-Dichlorobenzene µg/L0.50 10.0 70-13010410.4
1,4-Dichlorobenzene µg/L0.50 10.0 70-13099.49.94
Dichlorodifluoromethane (Freon 12)µg/L0.50 10.0 60-140138 †13.8
1,1-Dichloroethane µg/L0.50 10.0 70-13010310.3
1,2-Dichloroethane µg/L0.50 10.0 70-13089.08.90
1,1-Dichloroethylene µg/L0.50 10.0 70-13081.48.14
cis-1,2-Dichloroethylene µg/L0.50 10.0 70-13098.99.89
trans-1,2-Dichloroethylene µg/L0.50 10.0 70-13010410.4
1,2-Dichloropropane µg/L0.50 10.0 70-13010310.3
1,3-Dichloropropane µg/L0.50 10.0 70-13010410.4
2,2-Dichloropropane µg/L0.50 10.0 L-0470-13066.5 *†6.65
1,1-Dichloropropene µg/L0.50 10.0 70-13010010.0
cis-1,3-Dichloropropene µg/L0.50 10.0 70-13082.88.28
trans-1,3-Dichloropropene µg/L0.50 10.0 L-0770-13067.9 *6.79
Page 47 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B092577 - SW-846 5030B
LCS (B092577-BS1) Prepared: 03/26/14 Analyzed: 03/27/14
Diisopropyl Ether (DIPE)µg/L0.50 10.0 70-13099.39.93
Ethylbenzene µg/L0.50 10.0 70-13011011.0
2-Hexanone (MBK)µg/L5.0 100 70-13093.1 †93.1
Isopropylbenzene (Cumene)µg/L0.50 10.0 70-13011311.3
p-Isopropyltoluene (p-Cymene)µg/L0.50 10.0 70-13010510.5
Methyl tert-Butyl Ether (MTBE)µg/L0.50 10.0 70-13084.48.44
Methylene Chloride µg/L5.0 10.0 70-13094.99.49
4-Methyl-2-pentanone (MIBK)µg/L5.0 100 70-13094.0 †94.0
Naphthalene µg/L0.50 10.0 L-0470-13053.9 *†5.39
n-Propylbenzene µg/L0.50 10.0 70-13011111.1
Styrene µg/L0.50 10.0 70-13011011.0
1,1,2,2-Tetrachloroethane µg/L0.50 10.0 70-13098.69.86
Tetrachloroethylene µg/L0.50 10.0 70-13011411.4
Toluene µg/L0.50 10.0 70-13010710.7
1,2,3-Trichlorobenzene µg/L0.50 10.0 L-0470-13065.5 *6.55
1,2,4-Trichlorobenzene µg/L0.50 10.0 L-0470-13061.9 *6.19
1,1,1-Trichloroethane µg/L0.50 10.0 70-13082.48.24
1,1,2-Trichloroethane µg/L0.50 10.0 70-13010810.8
Trichloroethylene µg/L0.50 10.0 70-13011611.6
Trichlorofluoromethane (Freon 11)µg/L0.50 10.0 70-13087.58.75
1,2,3-Trichloropropane µg/L0.50 10.0 70-13010110.1
1,2,4-Trimethylbenzene µg/L0.50 10.0 70-13010010.0
1,3,5-Trimethylbenzene µg/L0.50 10.0 70-13010710.7
Vinyl Acetate µg/L5.0 100 L-0770-13067.8 *67.8
Vinyl Chloride µg/L0.50 10.0 60-14094.3 †9.43
m+p Xylene µg/L1.0 20.0 70-13010821.6
o-Xylene µg/L0.50 10.0 70-13010210.2
µg/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 81.620.4
µg/L 25.0 70-130Surrogate: Toluene-d8 10225.6
µg/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10526.3
LCS Dup (B092577-BSD1) Prepared: 03/26/14 Analyzed: 03/27/14
Acetone µg/L50 100 2570-13073.7 2.31 †73.7
Benzene µg/L0.50 10.0 2570-130112 2.4311.2
Bromobenzene µg/L0.50 10.0 2570-130101 1.7910.1
Bromochloromethane µg/L0.50 10.0 2570-130114 0.26211.4
Bromodichloromethane µg/L0.50 10.0 2570-13083.5 4.288.35
Bromoform µg/L0.50 10.0 2570-13071.8 8.427.18
Bromomethane µg/L1.0 10.0 2560-140104 6.58 †10.4
2-Butanone (MEK)µg/L5.0 100 2570-130100 4.33 †100
n-Butylbenzene µg/L0.50 10.0 2570-13093.9 0.2139.39
sec-Butylbenzene µg/L0.50 10.0 2570-130110 0.90111.0
tert-Butylbenzene µg/L0.50 10.0 2570-130105 0.38110.5
Carbon Tetrachloride µg/L0.50 10.0 2570-13079.1 0.2537.91
Chlorobenzene µg/L0.50 10.0 2570-130112 1.4311.2
Ethanol µg/L50 100 25 L-04, V-1670-13068.0 15.0*68.0
Chlorodibromomethane µg/L0.50 10.0 2570-13075.3 5.187.53
Chloroethane µg/L0.50 10.0 2560-14072.0 1.527.20
Chloroform µg/L0.50 10.0 2570-130101 2.1910.1
Chloromethane µg/L0.50 10.0 2560-14099.5 1.83 †9.95
2-Chlorotoluene µg/L0.50 10.0 2570-130104 1.4510.4
4-Chlorotoluene µg/L0.50 10.0 2570-130103 0.097510.3
Page 48 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B092577 - SW-846 5030B
LCS Dup (B092577-BSD1) Prepared: 03/26/14 Analyzed: 03/27/14
1,2-Dibromoethane (EDB)µg/L0.50 10.0 2570-130107 4.2810.7
1,2-Dichlorobenzene µg/L0.50 10.0 2570-130105 1.5310.5
1,3-Dichlorobenzene µg/L0.50 10.0 2570-130105 1.0510.5
1,4-Dichlorobenzene µg/L0.50 10.0 2570-130100 1.1010.0
Dichlorodifluoromethane (Freon 12)µg/L0.50 10.0 2560-140130 5.90 †13.0
1,1-Dichloroethane µg/L0.50 10.0 2570-130105 1.7310.5
1,2-Dichloroethane µg/L0.50 10.0 2570-13091.0 2.229.10
1,1-Dichloroethylene µg/L0.50 10.0 2570-13079.7 2.117.97
cis-1,2-Dichloroethylene µg/L0.50 10.0 2570-130100 1.2110.0
trans-1,2-Dichloroethylene µg/L0.50 10.0 2570-130103 1.0610.3
1,2-Dichloropropane µg/L0.50 10.0 2570-130106 3.5410.6
1,3-Dichloropropane µg/L0.50 10.0 2570-130105 1.0610.5
2,2-Dichloropropane µg/L0.50 10.0 25 L-0470-13066.8 0.450*†6.68
1,1-Dichloropropene µg/L0.50 10.0 2570-13097.1 3.049.71
cis-1,3-Dichloropropene µg/L0.50 10.0 2570-13087.4 5.418.74
trans-1,3-Dichloropropene µg/L0.50 10.0 2570-13071.2 4.747.12
Diisopropyl Ether (DIPE)µg/L0.50 10.0 2570-130102 2.7810.2
Ethylbenzene µg/L0.50 10.0 2570-130109 0.45810.9
2-Hexanone (MBK)µg/L5.0 100 2570-13095.9 3.00 †95.9
Isopropylbenzene (Cumene)µg/L0.50 10.0 2570-130112 0.35611.2
p-Isopropyltoluene (p-Cymene)µg/L0.50 10.0 2570-130104 1.1510.4
Methyl tert-Butyl Ether (MTBE)µg/L0.50 10.0 2570-13089.9 6.318.99
Methylene Chloride µg/L5.0 10.0 2570-13098.0 3.219.80
4-Methyl-2-pentanone (MIBK)µg/L5.0 100 2570-13097.6 3.81 †97.6
Naphthalene µg/L0.50 10.0 25 L-0470-13059.0 9.03*†5.90
n-Propylbenzene µg/L0.50 10.0 2570-130111 0.27111.1
Styrene µg/L0.50 10.0 2570-130113 2.2411.3
1,1,2,2-Tetrachloroethane µg/L0.50 10.0 2570-130106 7.5210.6
Tetrachloroethylene µg/L0.50 10.0 2570-130111 3.0311.1
Toluene µg/L0.50 10.0 2570-130108 0.55810.8
1,2,3-Trichlorobenzene µg/L0.50 10.0 25 L-0470-13068.5 4.48*6.85
1,2,4-Trichlorobenzene µg/L0.50 10.0 25 L-0470-13063.7 2.87*6.37
1,1,1-Trichloroethane µg/L0.50 10.0 2570-13083.2 0.9668.32
1,1,2-Trichloroethane µg/L0.50 10.0 2570-130110 1.6511.0
Trichloroethylene µg/L0.50 10.0 2570-130113 3.2311.3
Trichlorofluoromethane (Freon 11)µg/L0.50 10.0 2570-13081.3 7.358.13
1,2,3-Trichloropropane µg/L0.50 10.0 2570-130104 2.5410.4
1,2,4-Trimethylbenzene µg/L0.50 10.0 2570-130101 0.99110.1
1,3,5-Trimethylbenzene µg/L0.50 10.0 2570-130108 0.92810.8
Vinyl Acetate µg/L5.0 100 2570-13081.8 18.781.8
Vinyl Chloride µg/L0.50 10.0 2560-14092.3 2.14 †9.23
m+p Xylene µg/L1.0 20.0 2570-130108 0.13921.6
o-Xylene µg/L0.50 10.0 2570-130105 2.5110.5
µg/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 81.820.5
µg/L 25.0 70-130Surrogate: Toluene-d8 10125.4
µg/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10626.4
Page 49 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B092651 - SW-846 5030B
Blank (B092651-BLK1) Prepared & Analyzed: 03/27/14
Acetone µg/L50ND
Benzene µg/L0.50ND
Bromobenzene µg/L0.50ND
Bromochloromethane µg/L0.50ND
Bromodichloromethane µg/L0.50ND
Bromoform µg/L0.50ND
Bromomethane µg/L1.0ND
2-Butanone (MEK)µg/L5.0ND
n-Butylbenzene µg/L0.50ND
sec-Butylbenzene µg/L0.50ND
tert-Butylbenzene µg/L0.50ND
Carbon Tetrachloride µg/L0.50ND
Chlorobenzene µg/L0.50ND
Ethanol µg/L50 R-05, V-16ND
Chlorodibromomethane µg/L0.50ND
Chloroethane µg/L0.50ND
Chloroform µg/L0.50ND
Chloromethane µg/L0.50ND
2-Chlorotoluene µg/L0.50ND
4-Chlorotoluene µg/L0.50ND
1,2-Dibromoethane (EDB)µg/L0.50ND
1,2-Dichlorobenzene µg/L0.50ND
1,3-Dichlorobenzene µg/L0.50ND
1,4-Dichlorobenzene µg/L0.50ND
Dichlorodifluoromethane (Freon 12)µg/L0.50ND
1,1-Dichloroethane µg/L0.50ND
1,2-Dichloroethane µg/L0.50ND
1,1-Dichloroethylene µg/L0.50ND
cis-1,2-Dichloroethylene µg/L0.50ND
trans-1,2-Dichloroethylene µg/L0.50ND
1,2-Dichloropropane µg/L0.50ND
1,3-Dichloropropane µg/L0.50ND
2,2-Dichloropropane µg/L0.50ND
1,1-Dichloropropene µg/L0.50ND
cis-1,3-Dichloropropene µg/L0.50ND
trans-1,3-Dichloropropene µg/L0.50ND
Diisopropyl Ether (DIPE)µg/L0.50ND
Ethylbenzene µg/L0.50ND
2-Hexanone (MBK)µg/L5.0ND
Isopropylbenzene (Cumene)µg/L0.50ND
p-Isopropyltoluene (p-Cymene)µg/L0.50ND
Methyl tert-Butyl Ether (MTBE)µg/L0.50ND
Methylene Chloride µg/L5.0ND
4-Methyl-2-pentanone (MIBK)µg/L5.0ND
Naphthalene µg/L0.50 L-04ND
n-Propylbenzene µg/L0.50ND
Styrene µg/L0.50ND
1,1,2,2-Tetrachloroethane µg/L0.50ND
Tetrachloroethylene µg/L0.50ND
Toluene µg/L0.50ND
1,2,3-Trichlorobenzene µg/L0.50 L-04ND
1,2,4-Trichlorobenzene µg/L0.50 L-04ND
Page 50 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B092651 - SW-846 5030B
Blank (B092651-BLK1) Prepared & Analyzed: 03/27/14
1,1,1-Trichloroethane µg/L0.50ND
1,1,2-Trichloroethane µg/L0.50ND
Trichloroethylene µg/L0.50ND
Trichlorofluoromethane (Freon 11)µg/L0.50ND
1,2,3-Trichloropropane µg/L0.50ND
1,2,4-Trimethylbenzene µg/L0.50ND
1,3,5-Trimethylbenzene µg/L0.50ND
Vinyl Acetate µg/L5.0ND
Vinyl Chloride µg/L0.50ND
m+p Xylene µg/L1.0ND
o-Xylene µg/L0.50ND
µg/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 87.521.9
µg/L 25.0 70-130Surrogate: Toluene-d8 99.825.0
µg/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 97.024.2
LCS (B092651-BS1) Prepared & Analyzed: 03/27/14
Acetone µg/L50 100 70-13071.0 †71.0
Benzene µg/L0.50 10.0 70-13011611.6
Bromobenzene µg/L0.50 10.0 70-13010310.3
Bromochloromethane µg/L0.50 10.0 70-13011811.8
Bromodichloromethane µg/L0.50 10.0 70-13087.48.74
Bromoform µg/L0.50 10.0 70-13070.97.09
Bromomethane µg/L1.0 10.0 60-140104 †10.4
2-Butanone (MEK)µg/L5.0 100 70-13095.1 †95.1
n-Butylbenzene µg/L0.50 10.0 70-13010010.0
sec-Butylbenzene µg/L0.50 10.0 70-13011711.7
tert-Butylbenzene µg/L0.50 10.0 70-13010910.9
Carbon Tetrachloride µg/L0.50 10.0 70-13086.78.67
Chlorobenzene µg/L0.50 10.0 70-13011411.4
Ethanol µg/L50 100 L-07A, R-05, V-1670-13060.7 *60.7
Chlorodibromomethane µg/L0.50 10.0 70-13077.67.76
Chloroethane µg/L0.50 10.0 60-14077.77.77
Chloroform µg/L0.50 10.0 70-13010510.5
Chloromethane µg/L0.50 10.0 60-140103 †10.3
2-Chlorotoluene µg/L0.50 10.0 70-13010710.7
4-Chlorotoluene µg/L0.50 10.0 70-13010710.7
1,2-Dibromoethane (EDB)µg/L0.50 10.0 70-13010510.5
1,2-Dichlorobenzene µg/L0.50 10.0 70-13010610.6
1,3-Dichlorobenzene µg/L0.50 10.0 70-13010710.7
1,4-Dichlorobenzene µg/L0.50 10.0 70-13010310.3
Dichlorodifluoromethane (Freon 12)µg/L0.50 10.0 60-140130 †13.0
1,1-Dichloroethane µg/L0.50 10.0 70-13010810.8
1,2-Dichloroethane µg/L0.50 10.0 70-13092.69.26
1,1-Dichloroethylene µg/L0.50 10.0 70-13086.88.68
cis-1,2-Dichloroethylene µg/L0.50 10.0 70-13010510.5
trans-1,2-Dichloroethylene µg/L0.50 10.0 70-13011011.0
1,2-Dichloropropane µg/L0.50 10.0 70-13010710.7
1,3-Dichloropropane µg/L0.50 10.0 70-13010510.5
2,2-Dichloropropane µg/L0.50 10.0 70-13094.5 †9.45
1,1-Dichloropropene µg/L0.50 10.0 70-13010610.6
cis-1,3-Dichloropropene µg/L0.50 10.0 70-13092.59.25
trans-1,3-Dichloropropene µg/L0.50 10.0 70-13072.57.25
Page 51 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B092651 - SW-846 5030B
LCS (B092651-BS1) Prepared & Analyzed: 03/27/14
Diisopropyl Ether (DIPE)µg/L0.50 10.0 70-13010510.5
Ethylbenzene µg/L0.50 10.0 70-13011111.1
2-Hexanone (MBK)µg/L5.0 100 70-13090.6 †90.6
Isopropylbenzene (Cumene)µg/L0.50 10.0 70-13011611.6
p-Isopropyltoluene (p-Cymene)µg/L0.50 10.0 70-13011211.2
Methyl tert-Butyl Ether (MTBE)µg/L0.50 10.0 70-13087.78.77
Methylene Chloride µg/L5.0 10.0 70-13011011.0
4-Methyl-2-pentanone (MIBK)µg/L5.0 100 70-13094.1 †94.1
Naphthalene µg/L0.50 10.0 L-0470-13048.0 *†4.80
n-Propylbenzene µg/L0.50 10.0 70-13011811.8
Styrene µg/L0.50 10.0 70-13011311.3
1,1,2,2-Tetrachloroethane µg/L0.50 10.0 70-13010810.8
Tetrachloroethylene µg/L0.50 10.0 70-13011511.5
Toluene µg/L0.50 10.0 70-13011011.0
1,2,3-Trichlorobenzene µg/L0.50 10.0 L-0470-13056.8 *5.68
1,2,4-Trichlorobenzene µg/L0.50 10.0 L-0470-13057.9 *5.79
1,1,1-Trichloroethane µg/L0.50 10.0 70-13088.18.81
1,1,2-Trichloroethane µg/L0.50 10.0 70-13011011.0
Trichloroethylene µg/L0.50 10.0 70-13011311.3
Trichlorofluoromethane (Freon 11)µg/L0.50 10.0 70-13094.29.42
1,2,3-Trichloropropane µg/L0.50 10.0 70-13010210.2
1,2,4-Trimethylbenzene µg/L0.50 10.0 70-13010510.5
1,3,5-Trimethylbenzene µg/L0.50 10.0 70-13011211.2
Vinyl Acetate µg/L5.0 100 70-130105105
Vinyl Chloride µg/L0.50 10.0 60-14097.1 †9.71
m+p Xylene µg/L1.0 20.0 70-13011222.4
o-Xylene µg/L0.50 10.0 70-13010610.6
µg/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 84.621.2
µg/L 25.0 70-130Surrogate: Toluene-d8 10225.6
µg/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10626.4
LCS Dup (B092651-BSD1) Prepared & Analyzed: 03/27/14
Acetone µg/L50 100 2570-13088.8 22.3 †88.8
Benzene µg/L0.50 10.0 2570-130115 0.51911.5
Bromobenzene µg/L0.50 10.0 2570-130104 1.1610.4
Bromochloromethane µg/L0.50 10.0 2570-130117 1.4511.7
Bromodichloromethane µg/L0.50 10.0 2570-13086.1 1.508.61
Bromoform µg/L0.50 10.0 2570-13070.2 0.9927.02
Bromomethane µg/L1.0 10.0 2560-140122 16.2 †12.2
2-Butanone (MEK)µg/L5.0 100 2570-13096.6 1.53 †96.6
n-Butylbenzene µg/L0.50 10.0 2570-130102 2.0710.2
sec-Butylbenzene µg/L0.50 10.0 2570-130118 0.85411.8
tert-Butylbenzene µg/L0.50 10.0 2570-130110 1.3711.0
Carbon Tetrachloride µg/L0.50 10.0 2570-13084.8 2.228.48
Chlorobenzene µg/L0.50 10.0 2570-130116 1.3911.6
Ethanol µg/L50 100 25 R-05, V-1670-13084.5 32.8 *84.5
Chlorodibromomethane µg/L0.50 10.0 2570-13077.6 0.007.76
Chloroethane µg/L0.50 10.0 2560-14092.1 17.09.21
Chloroform µg/L0.50 10.0 2570-130105 0.38110.5
Chloromethane µg/L0.50 10.0 2560-140109 6.03 †10.9
2-Chlorotoluene µg/L0.50 10.0 2570-130109 1.2010.9
4-Chlorotoluene µg/L0.50 10.0 2570-130107 0.37510.7
Page 52 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B092651 - SW-846 5030B
LCS Dup (B092651-BSD1) Prepared & Analyzed: 03/27/14
1,2-Dibromoethane (EDB)µg/L0.50 10.0 2570-130108 2.2510.8
1,2-Dichlorobenzene µg/L0.50 10.0 2570-130108 1.5910.8
1,3-Dichlorobenzene µg/L0.50 10.0 2570-130110 1.9411.0
1,4-Dichlorobenzene µg/L0.50 10.0 2570-130104 1.4510.4
Dichlorodifluoromethane (Freon 12)µg/L0.50 10.0 2560-140131 0.306 †13.1
1,1-Dichloroethane µg/L0.50 10.0 2570-13096.9 11.29.69
1,2-Dichloroethane µg/L0.50 10.0 2570-13093.0 0.4319.30
1,1-Dichloroethylene µg/L0.50 10.0 2570-130103 16.710.3
cis-1,2-Dichloroethylene µg/L0.50 10.0 2570-130108 2.2610.8
trans-1,2-Dichloroethylene µg/L0.50 10.0 2570-13096.0 13.39.60
1,2-Dichloropropane µg/L0.50 10.0 2570-130106 0.37610.6
1,3-Dichloropropane µg/L0.50 10.0 2570-130105 0.19110.5
2,2-Dichloropropane µg/L0.50 10.0 2570-13092.4 2.25 †9.24
1,1-Dichloropropene µg/L0.50 10.0 2570-130106 0.28410.6
cis-1,3-Dichloropropene µg/L0.50 10.0 2570-13091.9 0.6519.19
trans-1,3-Dichloropropene µg/L0.50 10.0 2570-13073.3 1.107.33
Diisopropyl Ether (DIPE)µg/L0.50 10.0 2570-130108 2.9010.8
Ethylbenzene µg/L0.50 10.0 2570-130113 1.8711.3
2-Hexanone (MBK)µg/L5.0 100 2570-13090.5 0.0663 †90.5
Isopropylbenzene (Cumene)µg/L0.50 10.0 2570-130117 0.94311.7
p-Isopropyltoluene (p-Cymene)µg/L0.50 10.0 2570-130111 0.17911.1
Methyl tert-Butyl Ether (MTBE)µg/L0.50 10.0 2570-13081.7 7.088.17
Methylene Chloride µg/L5.0 10.0 2570-13089.1 21.38.91
4-Methyl-2-pentanone (MIBK)µg/L5.0 100 2570-13094.0 0.106 †94.0
Naphthalene µg/L0.50 10.0 25 L-0470-13052.4 8.76*†5.24
n-Propylbenzene µg/L0.50 10.0 2570-130118 0.25311.8
Styrene µg/L0.50 10.0 2570-130113 0.53111.3
1,1,2,2-Tetrachloroethane µg/L0.50 10.0 2570-130108 0.55510.8
Tetrachloroethylene µg/L0.50 10.0 2570-130118 2.6511.8
Toluene µg/L0.50 10.0 2570-130113 2.8611.3
1,2,3-Trichlorobenzene µg/L0.50 10.0 25 L-0470-13065.3 13.9*6.53
1,2,4-Trichlorobenzene µg/L0.50 10.0 25 L-0470-13062.5 7.64*6.25
1,1,1-Trichloroethane µg/L0.50 10.0 2570-13088.5 0.4538.85
1,1,2-Trichloroethane µg/L0.50 10.0 2570-130110 0.63611.0
Trichloroethylene µg/L0.50 10.0 2570-130115 1.6611.5
Trichlorofluoromethane (Freon 11)µg/L0.50 10.0 2570-130102 7.9510.2
1,2,3-Trichloropropane µg/L0.50 10.0 2570-130101 0.59210.1
1,2,4-Trimethylbenzene µg/L0.50 10.0 2570-130106 1.1410.6
1,3,5-Trimethylbenzene µg/L0.50 10.0 2570-130113 0.62211.3
Vinyl Acetate µg/L5.0 100 2570-130103 2.32103
Vinyl Chloride µg/L0.50 10.0 2560-140107 9.42 †10.7
m+p Xylene µg/L1.0 20.0 2570-130113 0.53422.6
o-Xylene µg/L0.50 10.0 2570-130107 0.94310.7
µg/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 83.821.0
µg/L 25.0 70-130Surrogate: Toluene-d8 10225.6
µg/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10626.5
Page 53 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
†Wide recovery limits established for difficult compound.
‡Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-04
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD outside of control limits. Reduced precision anticipated for any reported result for
this compound.
L-07A
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any
reported value for this compound.
R-05
Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may
be associated with reported result.
V-16
Page 54 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM18-20 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCEthanol
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
Page 55 of 60 14C0693_1 Contest_Final 04 01 14 0534
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM18-20 6200B in Water
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLCAIHA 02/1/2016
M-MA100Massachusetts DEPMA 06/30/2014
PH-0567Connecticut Department of Publilc HealthCT 09/30/2015
10899 NELAPNew York State Department of HealthNY 04/1/2014
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2015
LAO00112Rhode Island Department of HealthRI 12/30/2014
652North Carolina Div. of Water QualityNC 12/31/2014
MA007 NELAPNew Jersey DEPNJ 06/30/2014
E871027 NELAPFlorida Department of HealthFL 06/30/2014
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2014
C2065State of Washington Department of EcologyWA 02/23/2015
2011028State of MaineME 06/9/2015
460217Commonwealth of VirginiaVA 12/14/2014
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2014
Page 56 of 60 14C0693_1 Contest_Final 04 01 14 0534
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Page 59 of 60 14C0693_1 Contest_Final 04 01 14 0534
Page 60 of 60 14C0693_1 Contest_Final 04 01 14 0534

APPENDIX B

Summary of System Installation, Start-up, and Operation Activities
Harold Smith Remediation System
January 2014 – March 2014

January 10, 2014 System was down due to a power disruption. The technician checked reset
and restarted the system. The technician then performed regularly
operational and maintenance tasks on the system and recorded
measurements.

February 4, 2012 System was operational at arrival. The technician checked the system and
performed regularly operational and maintenance tasking on the system.
The technician then recorded measurements.

March 1, 2014 System was operational at arrival. The technician checked the system and
performed regularly operational and maintenance tasking on the system.
The technician then recorded measurements.

APPENDIX C

April 14, 2014

James McMillan
Sent Via email: [e-mail]

RE: Supply Well Analytical Results 2765 Union Ridge Road, Burlington, NC
NCDENR Incident #12913 Former Harold Smith Grocery
Pyramid Project 2013-263

Dear Mr. McMillan:
As directed by the NCDENR and T.A.C., Inc., Pyramid Environmental has continued to collect
samples from the Point-of-Entry (POE) treatment system that is connected to the water supply
well at the above referenced property. The work is being performed as part of the ongoing
assessment of the referenced nearby underground storage tank release. Groundwater cleanup is
ongoing at the site. The results of these analyses are presented below.

On March 20, 2014, Pyramid collected influent and effluent samples from the POE connected to
your supply well. The samples are designated as SW2765 INF and SW2765 EFF. The
groundwater samples were analyzed at a State certified laboratory and the results are attached for
your review. The laboratory results indicate that the POE influent untreated watercontained
methyl tert-butyl ether (MTBE) at a concentration of 100 parts per billion (PPB). The current
North Carolina drinking water standard for MTBE is 20 PPB. The compound IPE was detected at
140 PPB. The current North Carolina drinking water standard for IPE is 70 PPB. The compound
1,2-dichloroethane was detected at 20 PPB. The current North Carolina drinking water standard
for 1,2-dichloroethane is 0.4 PPB. No of the other targeted compounds were detected at
concentrations that exceeded the laboratory detection limits in the POE influent.

The laboratory results of the POE effluent sample treated water collected on March 20, 2014
indicate that two of the targeted petroleum compounds were detected at concentrations that
exceed the laboratory detection limits. The laboratory results indicate that the POE effluent
contained methyl tert-butyl ether (MTBE) at a concentration of 0.62 parts per billion (PPB). The
compound IPE was detected at 0.2 PPB.

The POE worked to remove petroleum contaminants under North Carolina Drinking Water
Standard levels prior to water use. Continued maintenance of the POE treatment system will
continue to be performed on a quarterly basis.

P.O. Box 16265 • Greensboro, NC 27416
503 Industrial Ave • Greensboro, NC 27406 Phone [phone] • Fax [phone] • Toll Free [phone]
Email: [e-mail] www.pyramidenvironmental.com

If you have any questions, please call Pyramid at [phone]. Thank you for your
cooperation with this project.

Sincerely,
James Cooper Jr., PE
Project Engineer

Attachments – Laboratory Report