RA-29680_48803_CA_LSA_20230508

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
May 8, 2023
Mr. Luis Franco
NCDEQ
Compliance Inspector
1646 Mail Service
Raleigh, NC 27699-1646
Re: Phase I Limited Site Assessment Report
Flash market #367
479 West Washington Street
Nashville, Nash County
North Carolina
Facility ID Number: 0-036412
Incident Number: 48803
GRI Project No: 6212
Dear Mr. Franco,
Please find enclosed the referenced report for the above mentioned site.
If you have any questions, please contact Laura Minor at 704-845-4010.
Sincerely,
Geological Resources, Inc.
Leslie Maxtone-Graham
Administrative Assistant
Enclosure
Cc: Mr. Scott Gordon, NC Remediation Manager, file
3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Phase I Limited Site Assessment Report
Flash Market #367
479 West Washington Street
Nashville, Nash County
North Carolina
Facility ID Number: 0-036412
Incident Number: 48803
GRI Project Number: 6212
Prepared for:
Mr. Scott Gordon, NC Remediation Manager
Transit Energy Group
501 River Street, Floor 3
Greenville, SC 29602
May 8, 2023
Project Manager Report Writer

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 8, 2023 Flash Market #367
Project Manager: Laura Minor GRI Project No. 6212
i
EXECUTIVE SUMMARY
The Flash Market #367 site is located at 479 West Washington Street in Nashville, Nash County, North
Carolina. The property operates as a petroleum retail facility and convenience store. The store building is
connected to two restaurants. The site is covered by asphalt, concrete, and grass. There is one 20,000-
gallon regular gasoline UST, one 8,000-gallon premium gasoline UST, one 8,000-gallon diesel UST, and one
2,000-gallon ethanol-free gasoline UST currently in use at the site with ten associated dispenser islands.

On October 14, 2021, two non-passing spill buckets were reported for the 20,000-gallon regular gasoline
and the 8,000-gallon premium gasoline USTs. GRI conducted a site check at the subject site on November
28, 2022. Two soil borings (Reg-SB-3’ and Prem-SB-3’) were advanced to approximately 3 feet BGS within
the vapor recovery ports located adjacent to each of the non-passing spill buckets. The concentrations of
GRO in both samples exceeded the RALs. Site Check results identified a release at the site and an LSA was
required.

On April 18, 2023, one monitoring well (MW-1) was installed in the vicinity of the spill bucket of the 8,000-
gallon premium gasoline UST. A soil sample was collected at 5 feet BGS during the installation of
monitoring well MW-1. All contaminant concentrations in the soil sample were below the MSCCs.

On April 18, 2023, a ground water sample was collected from MW-1. All contaminant concentrations in
the ground water sample collected from MW-1 were below the MACs.

A receptor survey was conducted on April 18, 2023. No water supply wells were identified within a 1,500-
foot radius of the site. Public water is available to the subject site and to all surrounding properties. One
surface water body, Stony Creek, was identified within a 500-foot radius of the site.

The reported soil contaminant concentrations do not exceed the MSCCs. The reported ground water
contaminant concentrations do not exceed the MACs or ten times the 2B standards. Based on the lack of
receptors other than a surface water body, the availability of municipal water to all properties in the area,
and relatively low ground water contaminant concentrations, GRI recommends the site be classified as
Low Risk and the incident closed with an NFA after filing an NRP.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 8, 2023 Flash Market #367
Project Manager: Laura Minor GRI Project No. 6212
ii
SITE INFORMATION
1. Site Identification
 Flash Market #367 (Facility ID 0-036412)
 Incident Number 48803 – (Risk Ranking Undetermined)
 Location of Source Area: 479 West Washington Street
Nashville, NC 27856
Nash County (Figures 1 and 2A)
35.978694°N, 77.973166°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST Owner
Flash Market, LLC (Table 1)
P.O. Box 1477
Greenville, SC 29602
Email Unknown
864-626-5553

UST Operator
Flash Market, LLC
P.O. Box 1477
Greenville, SC 29602
Email Unknown
864-626-5553

Property Owner
Getty Leasing, Inc.
160 Mine Lake Ct., Ste. 200
Raleigh, NC 27615-6417
Email Unknown
Phone No. Unknown

Property Occupant
L&L Food Stores, Inc.
710 East Church St.
Nashville, NC 27856
Email Unknown
252-459-3146

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
Waypoint Analytical, LLC
449 Springbrook Road
Charlotte, NC 28217
State Cert. Nos. 37735 and 402
[phone]
3. Information about Release
 Release was discovered on December 1, 2022
 An unknown amount of product was released from the leaking UST System via two non-passing spill
buckets
 One 20,000-gallon gasoline UST, one 8,000-gallon gasoline UST, one 8,000-gallon diesel UST, and one
2,000-gallon ethanol-free gasoline UST are in use at the site

Certification:

I, Samuel L. McKay, III, a Licensed Geologist for Geological Resources, Inc., do certify that the information
contained in this report is correct and accurate to the best of my knowledge.

Geological Resources, Inc. is licensed to practice geology and engineering in North Carolina. The
certification numbers of the corporation are C-127 and C-2727, respectively.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 8, 2023 Flash Market #367
Project Manager: Laura Minor GRI Project No. 6212
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MSCC: Maximum Soil Contaminant
Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWAP: Source Water Assessment and
Protection
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 8, 2023 Flash Market #367
Project Manager: Laura Minor GRI Project No. 6212
TABLE OF CONTENTS

EXECUTIVE SUMMARY ....................................................................................................................... i
SITE INFORMATION ............................................................................................................................ ii
ACRONYMS ....................................................................................................................................... iii
1. RISK CHARACTERIZATION .....................................................................................................1
2. RECEPTOR INFORMATION .....................................................................................................3
3. SITE GEOLOGY AND HYDROGEOLOGY ...................................................................................4
4. SITE INVESTIGATION .............................................................................................................5
5. CONCLUSIONS AND RECOMMENDATIONS ............................................................................6
6. LIMITATIONS ........................................................................................................................7

FIGURES
Figure 1: Site Location Map
Figure 2A: Site Vicinity Map
Figure 2B: Zoning Map
Figure 3: Site Map
Figure 4: Soil Quality Map
Figure 5: Ground Water Quality Map

TABLES
Table 1: UST Owner/Operator Information
Table 2: UST System Information
Table 3: Land Use Information
Table 4: Receptor Information
Table 5: Adjacent Property Owner Information
Table 6: Well Construction and Gauging Information
Table 7: Summary of Soil Sample Analytical Results
Table 8: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: Nash County Property Cards
Appendix B: Well Construction Record and Subsurface Log
Appendix C: State Correspondence
Appendix D: Laboratory Analytical Report

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 8, 2023 Flash Market #367
Project Manager: Laura Minor GRI Project No. 6212
1
1. RISK CHARACTERIZATION
Limited Site Assessment Risk Classification and Land Use Form
Part I – Groundwater/Surface Water/Vapor Impacts
High Risk
1. Has the release contaminated any water supply well including any well used for non-drinking
purposes? NO

2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the
release? NO

3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars, industrial cooling
water, filling swimming pools) located within 250 feet of the source area of the release?
NO

4. Does ground water within 500 feet of the source area of the release have the potential for future
use (there is no other source of water supply other than the groundwater)? NO

Public water is available to the site and surrounding properties.

5. Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a
confined space or pose any other serious threat to public health, public safety or the
environment?
NO

6. Are there any other factors that would cause the release to pose an imminent danger to public
health, public safety, or the environment? NO
If YES, explain:

Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the release? YES

Stony Creek, a Class C stream, is located approximately 360 feet southeast of the site.

If YES, does the maximum groundwater contaminant concentration exceed the surface water
quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10?
NO
8. Is the source area of the release located within an approved or planned wellhead protection area
as defined in 42 USC 300h-7(e)? NO

9. Is the release located in the Coastal Plain physiographic region as designated on a map entitled
“Geology of North Carolina” published by the Department in 1985? NO

10. If YES, is the source area of the release located in an area in which there is recharge to an
unconfined or semi-confined deeper aquifer that is being used or may be used as a source of
drinking water? N/A

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 8, 2023 Flash Market #367
Project Manager: Laura Minor GRI Project No. 6212
2
If YES, describe.
11. Do the levels of ground water contamination for any contaminant exceed the gross contamination
levels established by the Department? NO

Part II - Land Use
Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary residences (permanent or
temporary)? NO
Explain:
The subject property is an active convenience store and petroleum retail facility.

2. Does the property contain a school, daycare center, hospital, playground, park, recreation area,
church, nursing home, or other place of public assembly? NO
Explain:

The subject property is an active convenience store and petroleum retail facility.

3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or
industrial (e.g., manufacturing, utilities, industrial research and development,
chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial
enterprise, or is the land undeveloped? YES
Explain:

The subject property is an active convenience store and petroleum retail facility.

4. Do children visit the property? YES
Explain:

The site is currently a convenience store and children would likely visit the property.

5. Is access to the property reliably restricted consistent with its use (e.g., by fences, security
personnel or both)? NO
Explain:
The property is easily accessible to pedestrian and vehicular traffic.
6. Do pavement, buildings, or other structures cap the contaminated soil? YES
Explain:
The site is currently covered with grass, concrete, and asphalt.

If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil
will remain capped in the foreseeable future?
The site is expected to remain in operation as an active convenience store and petroleum retail

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 8, 2023 Flash Market #367
Project Manager: Laura Minor GRI Project No. 6212
3
facility for the foreseeable future.
7. What is the zoning status of the property?
According to the Nash County Official Zoning Map, the site is zoned B-1 (Business District).
8. Is the use of the property likely to change in the next 20 years? NO
Explain:

The subject property is currently an active convenience store and petroleum retail facility and
likely remain a convenience store for the foreseeable future.
Property Surrounding Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the release (excludes
property containing source area of the release):

9. What is the distance from the source area of the release to the nearest primary or secondary
residence (permanent or temporary)?

The closest primary residence is 402 Clark Circle located approximately 1,450 feet south-
southeast of the UST basin.

10. What is the distance from the source area of the release to the nearest school, daycare center,
hospital, playground, park, recreation area, church, nursing home or other place of public
assembly?

Stony Creek Environmental Park is located approximately 500 feet south of the UST basin.

11. What is the zoning status of properties in the surrounding area?

According to the Nash County Official Zoning Map, the surrounding areas are zoned Agricultural
(A-1), Business (B-1, B-2), Residential (R-4, R-10), and Office and Institutional (OI).

12. Briefly characterize the use and activities of the land in the surrounding area.

The area surrounding the site is a mixture of commercial, residential, agricultural, undeveloped,
and recreational. Land use information is included in Table 3. A zoning map is included as Figure
2B.

2. RECEPTOR INFORMATION
1. Water Supply Wells:
A receptor survey was conducted on April 18, 2023. No water supply wells were identified within
1,500 feet of the site. A Site Location Map is provided as Figure 1 and a Site Vicinity Map showing
property boundaries for the site and surrounding properties is included as Figure 2A. Receptor
information is provided in Table 4.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 8, 2023 Flash Market #367
Project Manager: Laura Minor GRI Project No. 6212
4
2. Public Water Supplies:
Are public water supplies available within 1,500 feet of the source area of the release? YES
If yes, where is the location of the nearest public water lines and the source(s) of the public water
supply. Explain:
Municipal water is available to the site and the surrounding properties. Water lines run along the
public streets in the area. Public water is supplied by Nash County Public Utilities.

3. Surface Water:
Identify all surface water bodies (e.g., ditch, pond, stream, lake, river) within 1,500 feet of the
source area of the release. This information must be shown on the USGS topographic map.
One surface water body, Stony Creek, was identified within a 500-foot radius of the site. Stony
Creek is a small Class C stream, located approximately 360 feet southeast of the site.

4. Wellhead Protection Areas:
Identify all planned or approved wellhead protection areas in the vicinity of the source area. This
information must be shown on the USGS topographic map. Wellhead protection areas are defined
in 42 USC 300h-7(e).
On May 4, 2023, GRI personnel accessed the NCDEQ SWAP Program’s website to identify wellhead
protection areas in the vicinity of the subject site. The site is not located within a wellhead
protection area.

5. Deep Aquifers in the Coastal Plain Physiographic Region:
The site is not in the Coastal Plain.

6. Subsurface Structures:
No structures with basements were observed in the vicinity of the source area. The water main
and other underground utilities run along West Washington Street and Evans Drive and several
underground utility lines were observed on the property.

7. Property Owners and Occupants:
The names and addresses of the owners of properties adjacent to the site are presented in Table
5. Property boundaries are shown on Figure 2A. Property cards for the adjacent property owners
are attached as Appendix B.

3. SITE GEOLOGY AND HYDROGEOLOGY
According to the 1985 Geologic Map of North Carolina, the site is located in the Eastern Slate Belt. The
bedrock is generally described as metamudstone and meta-argillite, interbedded with metasandstone,
metaconglomerate, and metavolcanic rock. The soil samples collected during well installation activities
were brown and gray silts and clays. The depth to ground water during the April 2023 sampling event was
5.18 feet below the top of well casing. A copy of the well construction record and subsurface log are
included as Appendix C. A Site Map is included as Figure 3. Well construction and gauging information is

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 8, 2023 Flash Market #367
Project Manager: Laura Minor GRI Project No. 6212
5
presented in Table 6.

4. SITE INVESTIGATION
GRI performed a site check during spill bucket replacement activities on November 28, 2022, that included
collection of two soil samples within the vapor recovery ports located adjacent to each of the non-passing
spill buckets associated with the 20,000-gallon regular gasoline and the 8,000-gallon premium gasoline
USTs. The reported concentrations of TPH-GRO in soil samples Reg-SB-3’ and Prem-SB-3’ were above the
RAL. No free product was noted at the site. The soil sampling results confirmed a release at the site and
an LSA was required.

In accordance with the NORR dated January 5, 2023, one Type II monitoring well (MW-1) was installed by
a North Carolina licensed well contractor on April 18, 2023, to assess the identified release at the site.
MW-1 was installed to a total depth of 15 feet BGS with a 10-foot screened interval set to bracket the
water table at the time of installation. Monitoring well MW-1 was installed in the vicinity of the spill bucket
of the 8,000-gallon premium gasoline UST. State correspondence is included in Appendix C.

1. Soil Sampling:
On November 28, 2022, two soil samples (Reg-SB-3’ and Prem-SB-3’) were collected within the vapor
recovery ports located adjacent to each of the non-passing spill buckets associated with the 20,000-
gallon regular gasoline and the 8,000-gallon premium gasoline USTs, respectively. The reported
concentrations of TPH-GRO in soil samples Reg-SB-3’ and Prem-SB-3’ were above the RAL. No free
product was noted at the site.

On April 18, 2023, one soil sample (MW-1-5’) was collected at 5 feet BGS during the installation of
monitoring well MW-1. The soil sample was submitted for analysis of VOCs by EPA Method 8260 and
VPH by the MADEP Method. All contaminant concentrations reported in soil sample MW-1-5’ were
below the MSCCs. A Soil Quality Map is included as Figure 4. A summary of the soil sample analytical
results is presented in Table 7. A copy of the laboratory analytical report from the April 2023 soil
sampling event is included in Appendix D. A summary of the current soil sampling data collected
during the LSA activities is shown below:

Sa
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MT
B
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Na
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Soil to Water MSCC
(mg/kg) 0.0072 5.4 8 6 0.085 0.2
Residential SCLs (mg/kg) 12 1,250 60.3 3,120 156 5.5
MW-1-5’ 5 <0.0007 <0.0008 <0.0007 <0.0006 <0.0007 <0.001

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 8, 2023 Flash Market #367
Project Manager: Laura Minor GRI Project No. 6212
6
2. Ground Water Sampling:
On April 18, 2023, MW-1 was gauged, purged, and sampled in accordance with NCDEQ guidelines.
The ground water sample was submitted for analysis of VOCs by EPA Method 6200B, EDB by EPA
Method 504.1, total lead by EPA Method 3030C and VPH by the MADEP Method. All contaminant
concentrations reported in the ground water sample collected from MW-1 were below the MACs. No
free product was observed at the site. A Ground Water Quality Map is included as Figure 5. A
summary of the ground water analytical data has been included in Table 8. A copy of the laboratory
analytical report has been included as Appendix D. A summary of the current ground water sampling
data is shown below:

Contaminant of
Concern

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Well
ID
MAC (µg/l) 1 600 600 500 20 6
GCL (µg/l) 5,000 260,000 80,000 50,000 20,000 6,000
MW-1 <0.180 <0.220 0.495 J 1.28 0.309 J <0.470

3. Quality Control:
The soil and ground water samples were immediately placed in laboratory-supplied containers after
collection, which were then placed in iced coolers. New disposable bailers were used to sample the
monitoring well and new nitrile gloves were worn during soil and ground water sampling. Samples
were logged using proper chain-of-custody procedures. The samples were transported to a North
Carolina certified laboratory for analysis.

5. CONCLUSIONS AND RECOMMENDATIONS
 The site is an active convenience store and petroleum retail facility. Land use in the area consists
of commercial, residential, agricultural, undeveloped, and recreational properties.
 A receptor survey was conducted on April 18, 2023. No water supply wells were identified within
a 1,500-foot radius of the site. Public water is available to the subject site and to all surrounding
properties.
 One surface water body was identified within a 500-foot radius of the site. Stony Creek, a Class
C/NSW stream, is located approximately 360 feet southeast of the site.
 On April 18, 2023, one monitoring well was installed. A soil sample was collected at 5 feet BGS
during the installation of monitoring well MW-1. All contaminant concentrations reported in soil
sample MW-1-5’ were below the soil-to-water MSCCs.
 On April 18, 2023, a ground water sample was collected from MW-1. All contaminant
concentrations reported in the ground water sample collected from MW-1 were below the MACs.
No free product was observed at the site.
 The reported contaminant concentrations do not exceed the MACs or ten times the 2B standards.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 8, 2023 Flash Market #367
Project Manager: Laura Minor GRI Project No. 6212
7
Based on the lack of receptors other than a surface water body, the availability of municipal water
to all properties in the area, and relatively low ground water contaminant concentrations, GRI
recommends the site be classified as Low Risk and the incident closed with an NFA after filing an
NRP.

6. LIMITATIONS
This report has been prepared for the exclusive use of Transit Energy Group and Mr. Scott Gordon for
specific application to the referenced site in Nash County, North Carolina. The assessment was conducted
based on the scope of work and level of effort specified by NCDEQ and with resources adequate only for
that scope of work. Our findings have been developed in accordance with generally accepted standards
of geology and hydrogeology practices in the State of North Carolina, available information and our
professional judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.

FIGURES
SITE LOCATION
Figure 1
Site Location
Flash Market #367
479 West Washington Street
Nashville, North Carolina
Nash County
Incident No. 48803
GRI Project No. 6212
500 M
2000 FT
Date: 10/13/2022 Location: 35.978694°N -77.973166°W
D
a
d
SITE
310651
029734
001626
310653
039913
001197
045594
310652
039912
US 64
NC 58
ELM ST
ALSTON ST
WASHINGTON ST
CEDAR STBODDIE ST
EAST EVANS DR
VALE ST
DRAKE ST
EVANS DR
WOMBLE RD
WEST NASHVILLE DR
BARNES ST
COLLINS ST
COURT ST
CLARK ST
RICHARDSON AVE
TRIANGLE CT
CLARK CIR
US 64
COLLINS ST
FIGURE 2A: SITE VICINITY MAPFLASH MARKET #367479 WEST WASHINGTON STREETNASHVILLE, NASH COUNTYNORTH CAROLINAINCIDENT NO. 48803GRI PROJECT NO. 6212
PREPARED BY:GEOLOGICAL RESOURCES, INC.APRIL 13, 2023
1,500-FOOT RADIUS
1,000-FOOT RADIUS
500-FOOT RADIUS
250-FOOT RADIUS
³
0 300150
Feet1 inch = 300 feet
1
2
LEGEND
ROADS
USGS_Hydro_Blueline_Streams
USGS_Waterbody
Adjacent Properties
nc_nash_parcels_poly
1 Land Use Code
361.
5
9

ft
SITE
US 64
NC 58
ELM ST
ALSTON ST
WASHINGTON ST
CEDAR STBODDIE ST
EAST EVANS DR
VALE ST
DRAKE ST
EVANS DR
WOMBLE RD
WEST NASHVILLE DR
BARNES ST
COLLINS ST
COURT ST
CLARK ST
RICHARDSON AVE
TRIANGLE CT
CLARK CIR
US 64
COLLINS ST
FIGURE 2B: ZONING MAPFLASH MARKET #367479 WEST WASHINGTON STREETNASHVILLE, NASH COUNTYNORTH CAROLINAINCIDENT NO. 48803GRI PROJECT NO. 6212
PREPARED BY:GEOLOGICAL RESOURCES, INC.APRIL 13, 2023
1,500-FOOT RADIUS
1,000-FOOT RADIUS
500-FOOT RADIUS
250-FOOT RADIUS
³
0 300150
Feet1 inch = 300 feet
1
2
LEGEND
ROADS
USGS_Hydro_Blueline_Streams
USGS_Waterbody
ZONING - A-1
ZONING - R-4
ZONING - OI
ZONING - R-10
ZONING - B-2
ZONING - A-1
ZONING - B-1
nc_nash_parcels_poly
1 Land Use Code

TABLES
UST ID Number Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number Facility ID Number
Owner or Operator?
Owner
UST ID Number Facility ID Number
Owner or Operator?
Owner
Name of Owner or Operator Dates of Ownership / Operation
TABLE 1
UST OWNER/OPERATOR INFORMATION
FLASH MARKET #367 (INCIDENT NO. 48803)
00-0-0000036412
Address Telephone Number
Flash Market, LLC 9/30/2021 - Present
Address Telephone Number
P.O. Box 1477, Greenville, SC 29602 864-626-5553
00-0-0000036412
Name of Owner or Operator Dates of Ownership / Operation
Rosemart Properties, LLC 5/8/2018 - 9/30/2021
Address Telephone Number
710 Church Street, Nashville NC 27856
613 US 158 Bypass, Henderson, NC 27537-6825
00-0-0000036412
Name of Owner or Operator Dates of Ownership / Operation
L & L Stores, Inc. 7/30/2001 - 5/8/2018
Page 1 of 1
Date: 11/28/2022 Facility ID #: 0-036412
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline Gasoline 20,000 7/30/2001 Single wall
Steel/FRP 10' 6" x 31' Double wall Flex Current Yes
2 Gasoline Gasoline 8,000 7/30/2001 Single wall
Steel/FRP 8' x 21' 4" Double wall Flex Current Yes
3 Diesel Diesel 8,000 7/30/2001 Single wall
Steel/FRP 8' x 21' 4" Double wall Flex Current No
4
Ethanol-
free
Gasoline
Kerosene 2,000 7/30/2001 Single wall
Steel/FRP 8' x 5' 4" Double wall Flex Current No
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
TABLE 2
UST SYSTEM INFORMATION
FLASH MARKET #367 (INCIDENT NO. N/A)
INCIDENT NO. PENDING
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Page 1 of 1
Date: 05/05/23 Facility ID # : 0-036412
Map ID No. Land Use Feature Zoning Description Address
Distance from
Source Area
(feet)
n/a A1 Agricultural District n/a n/a
n/a A1 Agricultural District n/a n/a
n/a B-1 Business District n/a n/a
n/a B-2 Central Business District n/a n/a
n/a R-4 High-Density Residential
District n/a n/a
n/a R-10 Medium-Density
Residential District n/a n/a
n/a OI Office and Institutional
District n/a n/a
Note:
• Properties are keyed to Figure 2B.
TABLE 3
LAND USE INFORMATION
FLASH MARKET #367 (INCIDENT NO. 48803)
Page 1 of 1
Facility ID #: 0-036412
Receptor ID
Latitude/
Longitude of Any
Significant Points
Up or Down-
Gradient
Distance from
the source area
of release (ft.)
1 n/a Down ~375' SE
2 n/a Down ~500' S
Notes:
• Receptors are shown on Figure 2A.
• n/a: not applicable.
Stony Creek Environmental Park 455 W Washington St, Nashville, NC 27856 n/a Public Park
TABLE 4
RECEPTOR INFORMATION
FLASH MARKET #367 (INCIDENT NO. 48803)
Date: 05/4/23
Stony Creek Southeast of the site, flowing east n/a Class C Steam, a tributary of the Tar River
Description Location Contact/Phone Number Usage
Page 1 of 1
Date: 04/19/23 Facility ID #: 0-036412
Parcel I.D. Property Owner Name Property Owner Address
039913 (site)
039912
029734 Dixie Place Land LLC P.O. Box 518
Nashville, NC 27856
045594 McDonald's Corporation #11932 P.O. Box 7908
Rocky Mount, NC 27804
310653 PTM LP 5700 Sixth Ave
Altoona, PA 16602
310652 Zaxnash RE, LLC P.O. Box 1139
Watkinsville, GA 30677
310651 Stallings Oil Company 300 S Wesleyan Blvd
Rocky Mount, NC 27804
001626 Town of Nashville P.O. Box 987
Nashville, NC 27856
001197 Tablerock Real Prop Invest LLC P.O. Box 277
Kinston, NC 28502
Note:
• Properties are keyed to Figure 2A.
TABLE 5
ADJACENT PROPERTY OWNER INFORMATION
FLASH MARKET #367 (INCIDENT NO. 48803)
Getty Leasing, Inc.292 Madison Ave, Fl 9
New York, NY 10017
Page 1 of 1
Date: 05/04/23 Facility ID #: 0-036412
Well ID Date Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
MW-1 04/18/23 04/18/23 5 5 - 15 15 NM 5.18 ---NM
Notes:
• ft BGS : feet below ground surface.
• NA: Not available.
• NM: Not measured.
TABLE 6
WELL CONSTRUCTION AND GAUGING INFORMATION
FLASH MARKET #367 (INCIDENT NO. 48803)
Page 1 of 1
Date: 05/3/23 Facility ID #: 0-036412
UVF/EPA
Methods
5030/8015B
Sample ID
Date
Collected
(mm/dd/yy)
Sample
Location
Sample
Depth
(ft-BGS)
50 NE NE NE NE NE NE NA NA NA
NE 0.0072 5.4 8 6 0.085 0.2 68 540 31
NE 12 1,250 60.3 3,120 156 5.5 625 1,500 469
Reg-SB-3'11/28/22 3 1,008 NR NR NR NR NR NR NR NR NR
Prem-SB-3'11/28/22 3 1,500 NR NR NR NR NR NR NR NR NR
MW-1-5'04/18/23 MW-1 5 NR <0.0007 <0.0008 <0.0007 <0.0006 <0.0007 <0.001 <1.45 <5.41 <0.740
Notes:
• Results reported in mg/kg (milligrams per kilograms)
• Trip Blank results reported in ug/l (micrograms per liter)
• ft-BGS: feet below ground surface.
• RAL: Regulatory Action Level.
• MCCs: Maximum Contaminant Concentrations (soils).
• SCLs: Soil Cleanup Levels.
• < : Less than the method detection limit specified in the laboratory report
• Concentrations in bold face type indicate the reported concentrations exceed the soil-to-water MCCs
• Concentrations in red italic type indicate the reported concentrations exceeded the residential SCLs
• NE: Not Established
• NR: Not Requested.
• < : Less than the method detection limit specified in the laboratory report.
Spill Buckets
Contaminant of Concern 
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e
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Residential SCLs (mg/kg)
RAL (mg/kg)
Soil-to-Water MSCCs (mg/kg)
To
t
a
l

X
y
l
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s
MT
B
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Na
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TABLE 7
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS
FLASH MARKET #367 (INCIDENT NO. 48803)
Analytical Method MADEP VPHEPA Method 8260D
Page 1 of 1
Date: 05/04/23 Facility ID #:0-036412
EPA 504.1 EPA 6010
Well
ID
Date Sampled
(mm/dd/yy)
1 600 600 500 20 6 0.02 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 50 15,000 NE NE NE
MW-1 04/18/23 <0.180 <0.220 0.495 J 1.28 0.309 J <0.470 <0.00351 0.313 <11.5 43.3 J 9.47 J
Notes:
• Results reported in micrograms per liter (µg/l).
• MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202.
• < : Less than the method detection limit specified in the laboratory report.• GCL: Gross contamination level.
• J: Estimated value.
• M: Minimum value.
• NE: Not established.
• Refer to laboratory report for other detectable concentrations which did not exceed the MACs.
MADEP VPH
TABLE 8
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
FLASH MARKET #367 (INCIDENT NO. 48803)
EPA 6200B
C9
-
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1
2

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2
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(E
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)
MAC (μg/l)
GCL (μg/l)
Contaminant of Concern
→
Analytical Method
→
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Page 1 of 1

APPENDICES

APPENDIX A
Nash County Property Cards
Parcel:
PIN:
Owner Details:
Description:
Mailing Address:
Address:Municipality:
NBHD:
380114326555
GETTY LEASING INC
ATTN: JOSHUA DICKER
292 MADISON AVE FL 9
479 W WASHINGTON ST NASHVILLE
253
NEW YORK NY 10017 6318
NA64
1Utilities
Value Summary
Appraised Land:Assessed Land
Appraised Building:Assessed Building
Appraised Total:Assessed Total
$742,790.00 $742,790.00
$906,980.00 $906,980.00
$1,649,770.00 $1,649,770.00
Stories:
Card:
Use:
Year Remod.
Total Rooms:
Bedrooms:
Family Room:
Full Bath:Half Bath:
Basement:
Square Feet:
HT/AC:
Fuel:
Attic:
Finished Basement:
Fireplace Pref.:
Fireplace OP/ST:
Basement Gar.:
Grade:
Cond (CDU):
/
Percent Complete:
Primary Residential Card
Type
Land
Eff. Front/Eff. DepthClassification
Profile
Land Use Code:31
LUC Description:31
Ext. Material:
Commercial Card
Year Built
Eff. Yr. Built
Units
Stories
Gross Flr. Area
Grade
AcresCode Description
Other Items
DescriptionCode Year Built Square Ft.
AGRICULTURE
Classification Sub Class/Use Soil type/Acres
2.03Land Acres:
Zoning:
Topography:LEVEL-LOW-
Type:
Year Built:
Recreation Room:
System:-
039913
HIGHWAY BUSINESS
Tax District:
/12 12 S-SQUARE FOOT 2.03
C-Commercial /F UD/0
C-Commercial /HOME/2.03
C-Commercial /A UD/0
Nash County Assessor's OfficeProperty Report Card
5/4/2023 9:08:04 AMPrinted on Page 1 of 2
Nash County Assessor's OfficeProperty Report Card
SKETCHMAP
Sales History
Date Book-Page Grantor Sale Desc Parcels Amount
1 FOOD FRCHSE - 100:FOOD
FRANCHISE 2015 Sq. Ft.
2 FOOD FRCHSE - 100:FOOD
FRANCHISE 1365 Sq. Ft.
3 CONVNCE STOR - 038:CONVENIENCE
STORE 4077 Sq. Ft.
1 OPEN PORCH - 85:OPEN PORCH 116
Sq. Ft.
1 3s BR - 34:3s BR 4956 Sq. Ft.
2 1s FR - 14:1s FR 61300 Sq. Ft.
3 1s FR - 15:1s FR 12400 Sq. Ft.
4 LIGHTS - 83:Lights 1 Sq. Ft.
Sketch
08-JUN-2001 1790--4 0 Valid $0
19-OCT-2009 2484--65 LAND WAYNE J 2 3 + Parcels $0
15-MAR-2018 2925--510 WJL STORES LLC 2 3 + Parcels $5,476,500
14-OCT-2021 3167--583 L & L ROSES LLC 99 Deed Stamps $3,025,000
5/4/2023 9:08:04 AMPrinted on Page 2 of 2
Parcel:
PIN:
Owner Details:
Description:
Mailing Address:
Address:Municipality:
NBHD:
380118326226
GETTY LEASING INC
ATTN: JOSHUA DICKER
292 MADISON AVE FL 9
225 EVANS DR NASHVILLE
253
NEW YORK NY 10017 6318
NA64
1Utilities
Value Summary
Appraised Land:Assessed Land
Appraised Building:Assessed Building
Appraised Total:Assessed Total
$278,170.00 $278,170.00
$220,580.00 $220,580.00
$498,750.00 $498,750.00
Stories:
Card:
Use:
Year Remod.
Total Rooms:
Bedrooms:
Family Room:
Full Bath:Half Bath:
Basement:
Square Feet:
HT/AC:
Fuel:
Attic:
Finished Basement:
Fireplace Pref.:
Fireplace OP/ST:
Basement Gar.:
Grade:
Cond (CDU):
/
Percent Complete:
Primary Residential Card
Type
Land
Eff. Front/Eff. DepthClassification
Profile
Land Use Code:68
LUC Description:68
Ext. Material:
Commercial Card
Year Built
Eff. Yr. Built
Units
Stories
Gross Flr. Area
Grade
AcresCode Description
Other Items
DescriptionCode Year Built Square Ft.
AGRICULTURE
Classification Sub Class/Use Soil type/Acres
1.24Land Acres:
Zoning:
Topography:LEVEL-ABOVE STREET-
Type:
Year Built:
Recreation Room:
System:-
039912
HIGHWAY BUSINESS
Tax District:
/12 12 S-SQUARE FOOT 1.24
C-Commercial /F UD/.1
C-Commercial /A UD/1.26
15 Concrete Paving 2002 5100
Nash County Assessor's OfficeProperty Report Card
5/4/2023 9:11:02 AMPrinted on Page 1 of 2
Nash County Assessor's OfficeProperty Report Card
SKETCHMAP
Sales History
Date Book-Page Grantor Sale Desc Parcels Amount
1 CAR WSH MANL - 074:CAR WASH
MANUAL 1560 Sq. Ft.
2 CAR WSH AUTO - 075:CAR WASH
AUTOMATIC 1260 Sq. Ft.
1 UTILITY ROOM - 91:UTILITY ROOM
900 Sq. Ft.
1 3s BR - 34:3s BR 4956 Sq. Ft.
2 1s FR - 14:1s FR 23800 Sq. Ft.
3 1s FR - 15:1s FR 5100 Sq. Ft.
Sketch
25-FEB-2022 3199--241 L & L ROSES LLC 3 $6 > in Excise Stamps $0
08-JUN-2001 1790--4 0 Valid $0
25-FEB-2022 3199--245 GETTY LEASING INC 3 $6 > in Excise Stamps $0
19-OCT-2009 2484--65 LAND WAYNE J 2 3 + Parcels $0
15-MAR-2018 2925--510 WJL STORES LLC 2 3 + Parcels $5,476,500
5/4/2023 9:11:02 AMPrinted on Page 2 of 2
5/5/23, 1:33 PM Nash County, NC - Tax Search
https://taxdata.nashcountync.gov/Datalets/PrintDatalet.aspx?pin=029734&gsp=PROFILEALL&taxyear=2023&jur=064&ownseq=0&card=1&roll=RE…1/1
PARID: 029734 TAX DISTRICT: NC34
CITYNAME: County TOWNSHIP: Nashville FIRE DISTRICT: NS Gulley
DIXIE PLACE LAND LLC CARL BLACKWOOD
Parcel
PIN 380100332789U
Physical Address
Unit
City
Zip Code -
Descriptive Location NORTH NC 58
Neighborhood 228
Class V-V
Land Use Code 0-0
Acres 11.29
Land Type A-ACREAGE
Frontage Width and Depth - -
Street1/Street2 01-Paved /-
Topo1/Topo2/Topo3 LEVEL-ROLLING-
Util1/Util2/Util3 2-Public Water/3-Public Sewer/-
Restrict1/Restrict2/Restrict3 -/-/-
Legal
Legal Description 11 29 AC, TRACT G PLYLER SPLIT OUT OF 380100253260
AC TRACT G PLYLER
Sub Name
Lot No.
Block
Phase #
Plat Book 33
Plat Page 289
Deed Book/Page 2394 / 596
Owner Details
Owner 1 DIXIE PLACE LAND LLC CARL BLACKWOOD
Owner 2
In Care Of
Mailing Address
City/State/Zip NASHVILLE/NC/27856
# of Dogs
Solid Waste Fee
Parcel:
PIN:
Owner Details:
Description:
Mailing Address:
Address:Municipality:
NBHD:
380114323711
MCDONALDS CORPORATION # 11932
PO BOX 7908
501 W WASHINGTON ST NASHVILLE
253
ROCKY MOUNT NC 27804
NA64
Utilities
Value Summary
Appraised Land:Assessed Land
Appraised Building:Assessed Building
Appraised Total:Assessed Total
$656,530.00 $656,530.00
$772,030.00 $772,030.00
$1,428,560.00 $1,428,560.00
Stories:
Card:
Use:
Year Remod.
Total Rooms:
Bedrooms:
Family Room:
Full Bath:Half Bath:
Basement:
Square Feet:
HT/AC:
Fuel:
Attic:
Finished Basement:
Fireplace Pref.:
Fireplace OP/ST:
Basement Gar.:
Grade:
Cond (CDU):
/
Percent Complete:
Primary Residential Card
Type
Land
Eff. Front/Eff. DepthClassification
Profile
Land Use Code:34
LUC Description:34
Ext. Material:
Commercial Card
Year Built
Eff. Yr. Built
Units
1991
Stories
Gross Flr. Area
Grade
AcresCode Description
Other Items
DescriptionCode Year Built Square Ft.
AGRICULTURE
Classification Sub Class/Use Soil type/Acres
1.57Land Acres:
Zoning:
Topography:--
Type:
Year Built:
Recreation Room:
System:-
045594
HIGHWAY BUSINESS
Tax District:
/12 12 S-SQUARE FOOT 1.57
C-Commercial /A GRB/0
C-Commercial /A WH/0
C-Commercial /HOME/1.57
C-Commercial /A UD/0
Nash County Assessor's OfficeProperty Report Card
5/4/2023 9:13:10 AMPrinted on Page 1 of 2
Nash County Assessor's OfficeProperty Report Card
SKETCHMAP
Sales History
Date Book-Page Grantor Sale Desc Parcels Amount
1 FOOD FRCHSE - 100:FOOD
FRANCHISE 3868 Sq. Ft.
1 1s FR - 14:1s FR 39900 Sq. Ft.
2 1s FR - 15:1s FR 3390 Sq. Ft.
3 3s BR - 32:3s BR 1175 Sq. Ft.
DescriptionCode Year Built Square Ft.
31-DEC-2001 1834--904 6 Conveying Fractional Interest $237,000
5/4/2023 9:13:10 AMPrinted on Page 2 of 2
Parcel:
PIN:
Owner Details:
Description:
Mailing Address:
Address:Municipality:
NBHD:
380114329961
PTM LP
5700 SIXTH AVE
100 EAST EVANS DR NASHVILLE
254
ALTOONA PA 16602
NA64
1Utilities
Value Summary
Appraised Land:Assessed Land
Appraised Building:Assessed Building
Appraised Total:Assessed Total
$835,310.00 $835,310.00
$906,500.00 $906,500.00
$1,741,810.00 $1,741,810.00
Stories:
Card:
Use:
Year Remod.
Total Rooms:
Bedrooms:
Family Room:
Full Bath:Half Bath:
Basement:
Square Feet:
HT/AC:
Fuel:
Attic:
Finished Basement:
Fireplace Pref.:
Fireplace OP/ST:
Basement Gar.:
Grade:
Cond (CDU):
/
Percent Complete:
Primary Residential Card
Type
Land
Eff. Front/Eff. DepthClassification
Profile
Land Use Code:31
LUC Description:31
Ext. Material:
Commercial Card
Year Built
Eff. Yr. Built
Units 1
Stories
Gross Flr. Area
Grade
AcresCode Description
Other Items
DescriptionCode Year Built Square Ft.
AGRICULTURE
Classification Sub Class/Use Soil type/Acres
2.35Land Acres:
Zoning:
Topography:LEVEL-ROLLING-LOW
Type:
Year Built:
Recreation Room:
System:-
310653
HIGHWAY BUSINESS
Tax District:
/12 12 S-SQUARE FOOT 2.35
C-Commercial /A UD/.32
C-Commercial /F WH/.13
C-Commercial /A WH/1.89
Nash County Assessor's OfficeProperty Report Card
5/4/2023 9:14:32 AMPrinted on Page 1 of 2
Nash County Assessor's OfficeProperty Report Card
SKETCHMAP
Sales History
Date Book-Page Grantor Sale Desc Parcels Amount
1 CONVNCE STOR - 038:CONVENIENCE
STORE 6312 Sq. Ft.
1 OPEN PORCH - 85:OPEN PORCH 126
Sq. Ft.
2 OPEN PORCH - 85:OPEN PORCH 216
Sq. Ft.
1 3s BR - 34:3s BR 5890 Sq. Ft.
2 1s FR - 15:1s FR 51500 Sq. Ft.
3 MAS WALL - 19:Masonary Wall 512 Sq.
Ft.
4 1s FR - 18:1s FR 168 Sq. Ft.
5 1s FR - 14:1s FR 944 Sq. Ft.
6 LIGHTS - 83:Lights 1 Sq. Ft.
Sketch
30-SEP-2016 2846--60 STALLINGS OIL COMPANY 99 Deed Stamps $850,000
11-APR-2008 2388--894
5/4/2023 9:14:32 AMPrinted on Page 2 of 2
Parcel:
PIN:
Owner Details:
Description:
Mailing Address:
Address:Municipality:
NBHD:
380114338113
ZAXNASH RE LLC
PO BOX 1139
101 EAST EVANS DR NASHVILLE
254
WATKINSVILLE GA 30677
NA64
Utilities
Value Summary
Appraised Land:Assessed Land
Appraised Building:Assessed Building
Appraised Total:Assessed Total
$617,380.00 $617,380.00
$438,910.00 $438,910.00
$1,056,290.00 $1,056,290.00
Stories:
Card:
Use:
Year Remod.
Total Rooms:
Bedrooms:
Family Room:
Full Bath:Half Bath:
Basement:
Square Feet:
HT/AC:
Fuel:
Attic:
Finished Basement:
Fireplace Pref.:
Fireplace OP/ST:
Basement Gar.:
Grade:
Cond (CDU):
/
Percent Complete:
Primary Residential Card
Type
Land
Eff. Front/Eff. DepthClassification
Profile
Land Use Code:10
LUC Description:10
Ext. Material:
Commercial Card
Year Built
Eff. Yr. Built
Units 1
Stories
Gross Flr. Area
Grade
AcresCode Description
Other Items
DescriptionCode Year Built Square Ft.
AGRICULTURE
Classification Sub Class/Use Soil type/Acres
1.27Land Acres:
Zoning:
Topography:--
Type:
Year Built:
Recreation Room:
System:-
310652
Tax District:
/12 12 S-SQUARE FOOT 1.27
C-Commercial /A WH/1.1
C-Commercial /A NOA/.17
18 Wood Fence 2016 216
Nash County Assessor's OfficeProperty Report Card
5/4/2023 9:13:46 AMPrinted on Page 1 of 2
Nash County Assessor's OfficeProperty Report Card
SKETCHMAP
Sales History
Date Book-Page Grantor Sale Desc Parcels Amount
1 RESTAURANT - 031:RESTAURANT
3587 Sq. Ft.
1 CNPY DRIVE I - CP1:CANOPY-DRIVE
IN 192 Sq. Ft.
2 UTILITY ROOM - 91:UTILITY ROOM 72
Sq. Ft.
3 OPEN PORCH - 85:OPEN PORCH 68
Sq. Ft.
4 OPEN PORCH - 85:OPEN PORCH 45
Sq. Ft.
5 OPEN PORCH - 85:OPEN PORCH 64
Sq. Ft.
1 OP - 11:OP 143 Sq. Ft.
2 MAS WALL - 19:Masonary Wall 342 Sq.
Ft.
3 1s FR - 18:1s FR 216 Sq. Ft.
4 1s FR - 14:1s FR 24900 Sq. Ft.
5 1s FR - 15:1s FR 7050 Sq. Ft.
6 LIGHTS - 83:Lights 1 Sq. Ft.
Sketch
22-MAR-2016 2817--563 STALLINGS OIL COMPANY 99 Deed Stamps $650,000
11-APR-2008 2388--894
5/4/2023 9:13:46 AMPrinted on Page 2 of 2
Parcel:
PIN:
Owner Details:
Description:
Mailing Address:
Address:Municipality:
NBHD:
380114439182
STALLINGS OIL COMPANY
300 S WESLEYAN BLVD

254
ROCKY MOUNT NC 27804
NA64
Utilities
Value Summary
Appraised Land:Assessed Land
Appraised Building:Assessed Building
Appraised Total:Assessed Total
$14,270.00 $14,270.00
$0.00 $0.00
$14,270.00 $14,270.00
Stories:
Card:
Use:
Year Remod.
Total Rooms:
Bedrooms:
Family Room:
Full Bath:Half Bath:
Basement:
Square Feet:
HT/AC:
Fuel:
Attic:
Finished Basement:
Fireplace Pref.:
Fireplace OP/ST:
Basement Gar.:
Grade:
Cond (CDU):
/
Percent Complete:
Primary Residential Card
Type
Land
Eff. Front/Eff. DepthClassification
Profile
Land Use Code:0
LUC Description:0
Ext. Material:
Commercial Card
Year Built
Eff. Yr. Built
Units
Stories
Gross Flr. Area
Grade
AcresCode Description
AGRICULTURE
Classification Sub Class/Use Soil type/Acres
28.82Land Acres:
Zoning:
Topography:--
Type:
Year Built:
Recreation Room:
System:-
310651
HIGHWAY BUSINESS
Tax District:
/49 Wasteland A-ACREAGE 28.82
V-Vacant /A NOA/.02
V-Vacant /F UD/.12
V-Vacant /A UD/.22
V-Vacant /F WH/27.02
V-Vacant /A WH/1.18
V-Vacant /F NUB/.23
Nash County Assessor's OfficeProperty Report Card
5/4/2023 9:15:14 AMPrinted on Page 1 of 2
Nash County Assessor's OfficeProperty Report Card
SKETCHMAP
Sales History
Date Book-Page Grantor Sale Desc Parcels Amount
Other Items
DescriptionCode Year Built Square Ft.
11-APR-2008 2388--894
5/4/2023 9:15:14 AMPrinted on Page 2 of 2
Parcel:
PIN:
Owner Details:
Description:
Mailing Address:
Address:Municipality:
NBHD:
380118311699I
TOWN OF NASHVILLE
PO BOX 987

253
NASHVILLE NC 27856 0987
NA64
1Utilities
Value Summary
Appraised Land:Assessed Land
Appraised Building:Assessed Building
Appraised Total:Assessed Total
$25,340.00 $25,340.00
$43,430.00 $43,430.00
$68,770.00 $68,770.00
Stories:
Card:
Use:
Year Remod.
Total Rooms:
Bedrooms:
Family Room:
Full Bath:Half Bath:
Basement:
Square Feet:
HT/AC:
Fuel:
Attic:
Finished Basement:
Fireplace Pref.:
Fireplace OP/ST:
Basement Gar.:
Grade:
Cond (CDU):
/
Percent Complete:
Primary Residential Card
Type
Land
Eff. Front/Eff. DepthClassification
Profile
Land Use Code:0
LUC Description:0
Ext. Material:
Commercial Card
Year Built
Eff. Yr. Built
Units
Stories
Gross Flr. Area
Grade
AcresCode Description
AGRICULTURE
Classification Sub Class/Use Soil type/Acres
11.52Land Acres:
Zoning:
Topography:LEVEL-ROLLING-LOW
Type:
Year Built:
Recreation Room:
System:-
001626
HIGHWAY BUSINESS
Tax District:
/41 41 A-ACREAGE 11.52
O-Other /A GRB/0
O-Other /F UD/0
O-Other /A UD/0
O-Other /A WH/0
O-Other /F GRB/0
O-Other /F WH/0
O-Other /HOME/11.52
Nash County Assessor's OfficeProperty Report Card
5/4/2023 9:17:09 AMPrinted on Page 1 of 3
Nash County Assessor's OfficeProperty Report Card
SKETCHMAP
Sales History
Date Book-Page Grantor Sale Desc Parcels Amount
1 CH LINK FE - 17:Chain Link Fence 1260
Sq. Ft.
2 CH LINK FE - 17:Chain Link Fence 80
Sq. Ft.
3 CH LINK FE - 17:Chain Link Fence 80
Sq. Ft.
4 SHELTER - 8:Shelter 126 Sq. Ft.
5 SHELTER - 8:Shelter 126 Sq. Ft.
6 SHELTER - 8:Shelter 120 Sq. Ft.
7 SHELTER - 8:Shelter 546 Sq. Ft.
8 CH LINK FE - 17:Chain Link Fence 328
Sq. Ft.
9 TENNIS CT - 16:Tennis Court 7626 Sq.
Ft.
10 CH LINK FE - 17:Chain Link Fence
3570 Sq. Ft.
11 1s FR - 15:1s FR 513 Sq. Ft.
Other Items
DescriptionCode Year Built Square Ft.
17-DEC-2009 2492--249 WJL COMMERCIAL LLC 3 $6 > in Excise Stamps $0
08-JUN-2001 1790--4 2 3 + Parcels $0
19-OCT-2009 2484--80 LAND WAYNE J 2 3 + Parcels $0
5/4/2023 9:17:09 AMPrinted on Page 2 of 3
Nash County Assessor's OfficeProperty Report Card
Ft.
10 CH LINK FE - 17:Chain Link Fence
3570 Sq. Ft.
11 1s FR - 15:1s FR 513 Sq. Ft.
5/4/2023 9:17:09 AMPrinted on Page 3 of 3
Parcel:
PIN:
Owner Details:
Description:
Mailing Address:
Address:Municipality:
NBHD:
380118323348
TABLEROCK REAL PROP INVEST LLC
ATTN JANNIE
PO BOX 277
101 WEST NASHVILLE DR NASHVILLE
253
KINSTON NC 28502
NA64
1Utilities
Value Summary
Appraised Land:Assessed Land
Appraised Building:Assessed Building
Appraised Total:Assessed Total
$443,960.00 $443,960.00
$890,520.00 $890,520.00
$1,334,480.00 $1,334,480.00
Stories:
Card:
Use:
Year Remod.
Total Rooms:
Bedrooms:
Family Room:
Full Bath:Half Bath:
Basement:
Square Feet:
HT/AC:
Fuel:
Attic:
Finished Basement:
Fireplace Pref.:
Fireplace OP/ST:
Basement Gar.:
Grade:
Cond (CDU):
/
Percent Complete:
Primary Residential Card
Type
Land
Eff. Front/Eff. DepthClassification
Profile
Land Use Code:34
LUC Description:34
Ext. Material:
Commercial Card
Year Built
Eff. Yr. Built
Units
2002
Stories
Gross Flr. Area
Grade
AcresCode Description
Other Items
DescriptionCode Year Built Square Ft.
AGRICULTURE
Classification Sub Class/Use Soil type/Acres
1.82Land Acres:
Zoning:
Topography:LEVEL--
Type:
Year Built:
Recreation Room:
System:-
001197
HIGHWAY BUSINESS
Tax District:
/12 12 S-SQUARE FOOT 1.82
C-Commercial /A GRB/0
C-Commercial /A UD/0
C-Commercial /HOME/1.82
Nash County Assessor's OfficeProperty Report Card
5/4/2023 9:12:23 AMPrinted on Page 1 of 2
Nash County Assessor's OfficeProperty Report Card
SKETCHMAP
Sales History
Date Book-Page Grantor Sale Desc Parcels Amount
1 FOOD FRCHSE - 100:FOOD
FRANCHISE 3908 Sq. Ft.
1 TERR - 95:TERR 85 Sq. Ft.
2 TERR - 95:TERR 35 Sq. Ft.
3 TERR - 95:TERR 70 Sq. Ft.
4 TERR - 95:TERR 70 Sq. Ft.
5 TERR - 95:TERR 120 Sq. Ft.
6 TERR - 95:TERR 100 Sq. Ft.
1 1s FR - 15:1s FR 3660 Sq. Ft.
2 1s FR - 14:1s FR 43850 Sq. Ft.
7 CLD STG - 96:CLD STG 3908 Sq. Ft.
3 S MISC BLD - 35S:MISC BUILDING S
2000 Sq. Ft.
4 LIGHTS - 83:Lights 1 Sq. Ft.
Sketch
04-OCT-2002 1895--1059 3 $6 > in Excise Stamps $0
5/4/2023 9:12:23 AMPrinted on Page 2 of 2

APPENDIX B
Well Construction Record and Subsurface Log
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Flash Market #367
6212
4/18/23
Eric Eubanks
Geological Resources, Inc.
Matt Steele
Solid Stem Auger
4548-A
MW-1
6
0 0.5 Asphalt
0.5 4 Clayey Silt
4 11 Silty Clay
11 14 Sandy Silt
14 15 Coarse Sandy Silt
Photo 1: Preclearing Photo 2: Completion
15
Well installed at completion

Brown

Brown Wet
Gray Wet

Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Top of Casing:
Diameter:Depth to Water:
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
Sand
Bentonite
Grout
Screen
Casing
SITE INFORMATION
DRILLING INFORMATION
WELL CONSTRUCTION INFORMATION
DIAGRAM - MONITORING WELL
Sand
Bentonite
Grout Screen
Inner Casing
Outer Casing
Flash Market #367
6212
4/18/23
Eric Eubanks
Geological Resources, Inc.
Matt Steele
Solid Stem Auger
4548-A
MW-1
6 5.18
3 15
1 3
0 1
0 5 2
5 15 2
1
3
15
5
15
WELL CONSTRUCTION RECORD
This form can be used for single or multiple wells
Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared) □Irrigation
Non-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip
County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W
6. Is (are) the well(s): □Permanent or □Temporary

7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells:
Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed.
For Internal Use ONLY:
Matt Steele
4548-A
Geological Resources, Inc.
4/18/23 MW-1
Flash Market #367 0-036412
479 West Washington Street
Nash 380114326555
35.978694 77.973166
1
15
5.18
6
Solid Stem Auger
11 15
0 5 2 Sch 40 PVC
5 15 2 0.010 Sch 40 PVC
0 1 grout pour
1 3 bentonite pour
3 15 #2 Sand Pour
0 0.5 Asphalt
0.5 4 Clayey Silt
4 11 Silty Clay
11 14 Sandy Silt
14 15 Coarse Sandy Silt
4/18/23
4
4
4
_______________

APPENDIX C
State Correspondence
Site Name City / County /Nash Incident #48803
Resp Pty Name / Contact Incident Mgr Region RAL
RP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #
Consultant / Project Mgr /Laura Minor
Telephone / Fax Number /Task Authorization Number:1 ChangeOrd:
Project Mgr Email Site Risk / Rank / Abatement:U RRA Date:
Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
w Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.
3r
d

P
t
y

D
e
d
?
Task #Lab /
SubCode
RO

I
M

A
u
t
h
Proposed
Rate/Price
(Consultant)RO

S
u
p
v
.

Au
t
h
Proposed Task
Subtotal
(Consultant)
Final
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
2.600 1 /site Y $5,761.50 Y $5,761.50 $5,761.50 /
12.055 1 /trip Y $50.00 Y $50.00 $50.00 /
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
Requested Preapproved Claimed3
TOTAL:$5,811.50 $5,811.50 TOTAL:
Total Standard Costs (Not Third Party)$5,811.50 $5,811.50 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty Costs
Process Tracking (Date)
TA Submittal:by:(PM)(Reserved for RO)
RO Review:3/8/23 by:(IM)Joint UST Preapproval Confirmed By:Date1
RO Supv. Review:3/10/23 by:(STF)RP or Designee Receipt Confirmation By:Date 4
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)
2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable.
3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned.
4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee within a week of approval. The signed pre-approval must be submitted
in the submitted claim. Signature indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to work
proceeding. Scope/cost negotiations do not supersede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both the
UST Section and RP is not to be modified without written consent by all signatories.
5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full.
DWM/UST ePATA 4/1/2022
DIRECTED - CAB ONLY
Nashville
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
704-845-4010
(Reserved for Incident Manager)
PREAPPROVAL / TASK AUTHORIZATION
Flash Market 367
Note: This Electronic Preapproval Task Authorization (ePATA) shall be used to receive preapproval from the UST Section. A proposal,including maps and figures,must be
attached to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If, following completion of this ePATA,
you discover that unexpected tasks must be performed, incurring costs for tasks not originally included with this form, you must complete and submit a separate ePATA request
designated as a "Change Order"in the provided space above prior to conducting those tasks. Include a copy of the prior ePATA form for confirmation. Please attach this form to
the cover of the corresponding claim when requesting reimbursement. IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been
completed within 12 monthsof the completion date ofthe FIRSTcompleted taskto remain within the Statute of Limitations. All ePATAs submitted within a claim are closed with that
claim, and may not be re-used in a separate submittal,even for costs or tasks that were not originally claimed. Final reimbursement of costs associated with the Total Claimed
amount below may be affected by the eligibility status of the site (i.e., deductibles, apportionment, etc.), and the documentary validation of incurred costs as reasonable and
necessary expenses per 15A NCAC 2P .0402 and .0404.
LF
MRP
(Initials)
LM
Proposed
Units / Type
(Consultant)
John Maloy
ActiveNO
23-019 February 2023
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
FINAL REIMBURSEMENT
100.00%
[e-mail]
Transit Energy Group
Geological Resources, Inc.
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORM
Dept of Environmental Quality -Division of Waste Management
03/13/2023
3/13/23

APPENDIX D
Laboratory Analytical Report

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

5/2/2023
Geological Resources, Inc. Laura Minor
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-111-0022 Client Project Description: Flash Market #367
GRI #6212
Dear Laura Minor:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 4/21/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 36
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-111-0022
Page 2 of 36
Report Number:
Sample Summary Table
Client Project Description:
23-111-0022
Flash Market #367
GRI #6212
Lab No Client Sample ID Matrix Date Collected Date Received
04/18/2023 13:30Aqueous 94649 MW-1 04/21/2023
04/18/2023 11:40Solids 94650 MW-1 - 5 04/21/2023
Page 3 of 36
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-111-0022
Report Limit
Project:Flash Market #367
V 94649MW-1
0.313 04/25/2023 19:116010DLeadmg/L 0.012
J3.03 04/28/2023 12:386200BAcetoneµg/L 1.80
J0.495 04/28/2023 12:386200BEthylbenzeneµg/L 0.170
J0.309 04/28/2023 12:386200BMethyl tert-butyl ether (MTBE)µg/L 0.140
J0.236 04/28/2023 12:386200Bn-Propylbenzene µg/L 0.190
1.14 04/28/2023 12:386200B1,2,4-Trimethylbenzene µg/L 0.190
J0.355 04/28/2023 12:386200B1,3,5-Trimethylbenzene µg/L 0.180
1.28 04/28/2023 12:386200Bm,p-Xylene µg/L 0.420
1.28 04/28/2023 12:386200BXylene (Total)µg/L 0.210
J43.3 04/24/2023 19:11CALCULATIONAliphatics C9-C12 (Adjusted)µg/L 25.8
J9.47 04/24/2023 19:11CALCULATIONAromatic C9-C10 (Adjusted)µg/L 4.02
54.5 04/24/2023 19:11MADEP-VPH Aliphatic C9-C12 µg/L 25.8
J9.47 04/24/2023 19:11MADEP-VPH Aromatic C9-C10 µg/L 4.02
V 94650MW-1 - 5
0.032 04/25/2023 17:598260DAcetonemg/Kg - dry 0.002
JM0.002 04/25/2023 17:598260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
15.7 04/30/2023 12:30SW-DRYWT Moisture %
Page 4 of 36

Client: Geological Resources, Inc. CASE NARRATIVE
Project: Flash Market #367 Lab Report Number: 23-111-0022
Date: 5/1/2023
EDB and DBCP by Microextraction GC/ECD Method EPA-504.1 Analyte: 1,2-Dibromoethane QC Batch No: V32508/V32463
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Sample 94769 (WSW-Little) Analyte: 1,2-Dibromoethane
QC Batch No: V32508/V32463 Dup was spiked by accident. LCSD reported.
Volatile Organic Compounds - GC/MS Method 6200B
Analyte: 3,3-Dimethyl-1-butanol QC Batch No: V32559/V32558
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: tert-Amyl alcohol QC Batch No: V32559/V32558 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Metals Analysis Method 6010D Sample 94649 (MW-1)
QC Batch No: V32411/V32360 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Volatile Organic Compounds - GC/MS Method 8260D Analyte: 2-Butanone QC Batch No: V32426/V32424
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias.
Page 5 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-111-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6212 Received : 04/21/2023
Flash Market #367
Report Date : 05/02/2023
Sample ID :
Lab No :
Sampled:MW-1
94649 Matrix:
4/18/2023 13:30
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 04/28/23 12:38 6200BMSA
0.313 mg/L 0.012 0.030Lead 5 04/25/23 19:11 6010DJKC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 6 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-111-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6212 Received : 04/21/2023
Flash Market #367
Report Date : 05/02/2023
Sample ID :
Lab No :
Sampled:MW-1
94649 Matrix:
4/18/2023 13:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V32558 04/27/23 14:00
3.03 J µg/L 1.80 10.0Acetone 1 04/28/23 12:38 V32559MSA
<0.180 µg/L 0.180 0.500Benzene 1 04/28/23 12:38 V32559MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 04/28/23 12:38 V32559MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 04/28/23 12:38 V32559MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 04/28/23 12:38 V32559MSA
<1.50 µg/L 1.50 5.00Bromoform 1 04/28/23 12:38 V32559MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 04/28/23 12:38 V32559MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 04/28/23 12:38 V32559MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 04/28/23 12:38 V32559MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 04/28/23 12:38 V32559MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 04/28/23 12:38 V32559MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 04/28/23 12:38 V32559MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 04/28/23 12:38 V32559MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 04/28/23 12:38 V32559MSA
<0.220 µg/L 0.220 0.500Chloroform 1 04/28/23 12:38 V32559MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 04/28/23 12:38 V32559MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 04/28/23 12:38 V32559MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 04/28/23 12:38 V32559MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 04/28/23 12:38 V32559MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 04/28/23 12:38 V32559MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 04/28/23 12:38 V32559MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 04/28/23 12:38 V32559MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 7 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-111-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6212 Received : 04/21/2023
Flash Market #367
Report Date : 05/02/2023
Sample ID :
Lab No :
Sampled:MW-1
94649 Matrix:
4/18/2023 13:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V32558 04/27/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 04/28/23 12:38 V32559MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 04/28/23 12:38 V32559MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 04/28/23 12:38 V32559MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 04/28/23 12:38 V32559MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 04/28/23 12:38 V32559MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 04/28/23 12:38 V32559MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 04/28/23 12:38 V32559MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 04/28/23 12:38 V32559MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 04/28/23 12:38 V32559MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 04/28/23 12:38 V32559MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 04/28/23 12:38 V32559MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 04/28/23 12:38 V32559MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 04/28/23 12:38 V32559MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 04/28/23 12:38 V32559MSA
<42.0 µg/L 42.0 200Ethanol 1 04/28/23 12:38 V32559MSA
0.495 J µg/L 0.170 0.500Ethylbenzene 1 04/28/23 12:38 V32559MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 04/28/23 12:38 V32559MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 04/28/23 12:38 V32559MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 04/28/23 12:38 V32559MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 04/28/23 12:38 V32559MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 04/28/23 12:38 V32559MSA
0.309 J µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 04/28/23 12:38 V32559MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 8 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-111-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6212 Received : 04/21/2023
Flash Market #367
Report Date : 05/02/2023
Sample ID :
Lab No :
Sampled:MW-1
94649 Matrix:
4/18/2023 13:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V32558 04/27/23 14:00
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 04/28/23 12:38 V32559MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 04/28/23 12:38 V32559MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 04/28/23 12:38 V32559MSA
0.236 J µg/L 0.190 0.500n-Propylbenzene 1 04/28/23 12:38 V32559MSA
<0.220 µg/L 0.220 0.500Styrene 1 04/28/23 12:38 V32559MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 04/28/23 12:38 V32559MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 04/28/23 12:38 V32559MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 04/28/23 12:38 V32559MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 04/28/23 12:38 V32559MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 04/28/23 12:38 V32559MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 04/28/23 12:38 V32559MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 04/28/23 12:38 V32559MSA
<0.220 µg/L 0.220 0.500Toluene 1 04/28/23 12:38 V32559MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 04/28/23 12:38 V32559MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 04/28/23 12:38 V32559MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 04/28/23 12:38 V32559MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 04/28/23 12:38 V32559MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 04/28/23 12:38 V32559MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 04/28/23 12:38 V32559MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 04/28/23 12:38 V32559MSA
1.14 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 04/28/23 12:38 V32559MSA
0.355 J µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 04/28/23 12:38 V32559MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 9 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-111-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6212 Received : 04/21/2023
Flash Market #367
Report Date : 05/02/2023
Sample ID :
Lab No :
Sampled:MW-1
94649 Matrix:
4/18/2023 13:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V32558 04/27/23 14:00
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 04/28/23 12:38 V32559MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 04/28/23 12:38 V32559MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 04/28/23 12:38 V32559MSA
1.28 µg/L 0.420 1.00m,p-Xylene 1 04/28/23 12:38 V32559MSA
1.28 µg/L 0.210 0.500Xylene (Total)1 04/28/23 12:38 V32559
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%04/28/23 12:381 MSA V32559
Surrogate: Dibromofluoromethane 99.0 Limits: 70-130%04/28/23 12:381 MSA V32559
Surrogate: 1,2-Dichloroethane - d4 95.2 Limits: 70-130%04/28/23 12:381 MSA V32559
Surrogate: Toluene-d8 100 Limits: 70-130%04/28/23 12:381 MSA V32559
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
EPA-504.1(PREP)
EPA-504.1 Prep Batch(es):V32463 04/27/23 09:37
<0.00351 µg/L 0.00351 0.02131,2-Dibromoethane 1 04/27/23 14:16 V32508AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 10 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-111-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6212 Received : 04/21/2023
Flash Market #367
Report Date : 05/02/2023
Sample ID :
Lab No :
Sampled:MW-1
94649 Matrix:
4/18/2023 13:30
Aqueous
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<11.5 µg/L 11.5 50.0Aliphatic C5-C8 (Adjusted)1 04/24/23 19:11
43.3 J µg/L 25.8 50.0Aliphatics C9-C12 (Adjusted)1 04/24/23 19:11
9.47 J µg/L 4.02 50.0Aromatic C9-C10 (Adjusted)1 04/24/23 19:11
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V32356 04/24/23 08:00
<11.5 µg/L 11.5 50.0Aliphatic C5-C8 1 04/24/23 19:11 V32357TBL
54.5 µg/L 25.8 50.0Aliphatic C9-C12 1 04/24/23 19:11 V32357TBL
9.47 J µg/L 4.02 50.0Aromatic C9-C10 1 04/24/23 19:11 V32357TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)87.6 Limits: 70-130%04/24/23 19:111 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)79.6 Limits: 70-130%04/24/23 19:111 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 11 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-111-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6212 Received : 04/21/2023
Flash Market #367
Report Date : 05/02/2023
Sample ID :
Lab No :
Sampled:MW-1 - 5
94650 Matrix:
4/18/2023 11:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
15.7 %Moisture 1 04/30/23 12:30 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 12 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-111-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6212 Received : 04/21/2023
Flash Market #367
Report Date : 05/02/2023
Sample ID :
Lab No :
Sampled:MW-1 - 5
94650 Matrix:
4/18/2023 11:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32424 04/25/23 08:00
0.032 mg/Kg - dry 0.002 0.023Acetone 1 04/25/23 17:59 V32426TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 04/25/23 17:59 V32426TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 04/25/23 17:59 V32426TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 04/25/23 17:59 V32426TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 04/25/23 17:59 V32426TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 04/25/23 17:59 V32426TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 04/25/23 17:59 V32426TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 04/25/23 17:59 V32426TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 04/25/23 17:59 V32426TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 04/25/23 17:59 V32426TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 04/25/23 17:59 V32426TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 04/25/23 17:59 V32426TBL
<0.0008 mg/Kg - dry 0.0008 0.005Carbon Disulfide 1 04/25/23 17:59 V32426TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 04/25/23 17:59 V32426TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 04/25/23 17:59 V32426TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 04/25/23 17:59 V32426TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 04/25/23 17:59 V32426TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 04/25/23 17:59 V32426TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 04/25/23 17:59 V32426TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 04/25/23 17:59 V32426TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 04/25/23 17:59 V32426TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 04/25/23 17:59 V32426TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 13 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-111-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6212 Received : 04/21/2023
Flash Market #367
Report Date : 05/02/2023
Sample ID :
Lab No :
Sampled:MW-1 - 5
94650 Matrix:
4/18/2023 11:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32424 04/25/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 04/25/23 17:59 V32426TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 04/25/23 17:59 V32426TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 04/25/23 17:59 V32426TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 04/25/23 17:59 V32426TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,3-Dichlorobenzene 1 04/25/23 17:59 V32426TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 04/25/23 17:59 V32426TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 04/25/23 17:59 V32426TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 04/25/23 17:59 V32426TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 04/25/23 17:59 V32426TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 04/25/23 17:59 V32426TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 04/25/23 17:59 V32426TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 04/25/23 17:59 V32426TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 04/25/23 17:59 V32426TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,3-Dichloropropane 1 04/25/23 17:59 V32426TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 04/25/23 17:59 V32426TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 04/25/23 17:59 V32426TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 04/25/23 17:59 V32426TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 04/25/23 17:59 V32426TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 04/25/23 17:59 V32426TBL
<0.0010 mg/Kg - dry 0.0010 0.059Ethyl Tertiary Butyl Ether (ETBE)1 04/25/23 17:59 V32426TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 04/25/23 17:59 V32426TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 04/25/23 17:59 V32426TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 14 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-111-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6212 Received : 04/21/2023
Flash Market #367
Report Date : 05/02/2023
Sample ID :
Lab No :
Sampled:MW-1 - 5
94650 Matrix:
4/18/2023 11:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32424 04/25/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 04/25/23 17:59 V32426TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 04/25/23 17:59 V32426TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 04/25/23 17:59 V32426TBL
0.002 JM mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 04/25/23 17:59 V32426TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 04/25/23 17:59 V32426TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 04/25/23 17:59 V32426TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 04/25/23 17:59 V32426TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 04/25/23 17:59 V32426TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 04/25/23 17:59 V32426TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 04/25/23 17:59 V32426TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 04/25/23 17:59 V32426TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 04/25/23 17:59 V32426TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 04/25/23 17:59 V32426TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 04/25/23 17:59 V32426TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 04/25/23 17:59 V32426TBL
<0.0008 mg/Kg - dry 0.0008 0.0111,2,4-Trichlorobenzene 1 04/25/23 17:59 V32426TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 04/25/23 17:59 V32426TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,1,2-Trichloroethane 1 04/25/23 17:59 V32426TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 04/25/23 17:59 V32426TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 04/25/23 17:59 V32426TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,2,3-Trichloropropane 1 04/25/23 17:59 V32426TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 04/25/23 17:59 V32426TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 15 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-111-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6212 Received : 04/21/2023
Flash Market #367
Report Date : 05/02/2023
Sample ID :
Lab No :
Sampled:MW-1 - 5
94650 Matrix:
4/18/2023 11:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32424 04/25/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 04/25/23 17:59 V32426TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 04/25/23 17:59 V32426TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 04/25/23 17:59 V32426TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 04/25/23 17:59 V32426TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 04/25/23 17:59 V32426TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 04/25/23 17:59 V32426
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%04/25/23 17:591 TBL V32426
Surrogate: Dibromofluoromethane 98.0 Limits: 84-123%04/25/23 17:591 TBL V32426
Surrogate: Toluene-d8 89.8 Limits: 76-129%04/25/23 17:591 TBL V32426
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 16 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-111-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6212 Received : 04/21/2023
Flash Market #367
Report Date : 05/02/2023
Sample ID :
Lab No :
Sampled:MW-1 - 5
94650 Matrix:
4/18/2023 11:40
Solids
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<1.45 mg/Kg - dry 1.45 9.49Aliphatic C5-C8 (Adjusted)1 04/22/23 14:51
<5.41 mg/Kg - dry 5.41 9.49Aliphatics C9-C12 (Adjusted)1 04/22/23 14:51
<0.740 mg/Kg - dry 0.740 9.49Aromatic C9-C10 (Adjusted)100 04/22/23 14:51
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V32301 04/22/23 08:00
<1.45 mg/Kg - dry 1.45 9.49Aliphatic C5-C8 100 04/22/23 14:51 V32302TBL
<5.41 mg/Kg - dry 5.41 9.49Aliphatic C9-C12 100 04/22/23 14:51 V32302TBL
<0.740 mg/Kg - dry 0.740 9.49Aromatic C9-C10 100 04/22/23 14:51 V32302TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)83.9 Limits: 70-130%04/22/23 14:51100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)79.3 Limits: 70-130%04/22/23 14:51100 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Page 17 of 36
Quality Control Data
23-111-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #367
QC Prep Batch Method:
Metals Analysis
6010D
V32411QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V32360
Associated Lab Samples: 94649
LRB-V32360 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
04/25/23 18:090.0060.002<0.002mg/LLead
LCS-V32360Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1070.1070.100mg/LLead 80-120
V 94528-MS-V32360 V 94528-MSD-V32360Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.105 93.00.1040.1000.1000.012mg/LLead 92.0 75-125 0.9 20.0
V 94528-PDS-V32360Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
04/25/23 18:2694.00.241mg/LLead
Page 1 of 17Date:05/02/2023 10:46 AM
Page 18 of 36
Quality Control Data
23-111-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #367
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V32559QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V32558
Associated Lab Samples: 94649
LRB-V32558 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/28/23 05:2110.01.80<1.80µg/LAcetone
04/28/23 05:210.5000.180<0.180µg/LBenzene
04/28/23 05:210.5000.210<0.210µg/LBromobenzene
04/28/23 05:211.000.420<0.420µg/LBromochloromethane
04/28/23 05:210.5000.160<0.160µg/LBromodichloromethane
04/28/23 05:215.001.50<1.50µg/LBromoform
04/28/23 05:211.000.280<0.280µg/LBromomethane
04/28/23 05:210.5000.180<0.180µg/Ln-Butylbenzene
04/28/23 05:210.5000.200<0.200µg/Lsec-Butyl benzene
04/28/23 05:212.000.920<0.920µg/Ltert-Butyl benzene
04/28/23 05:210.5000.180<0.180µg/LCarbon Tetrachloride
04/28/23 05:210.5000.190<0.190µg/LChlorobenzene
04/28/23 05:210.5000.190<0.190µg/LChlorodibromomethane
04/28/23 05:211.000.430<0.430µg/LChloroethane
04/28/23 05:210.5000.220<0.220µg/LChloroform
04/28/23 05:210.5000.220<0.220µg/LChloromethane
04/28/23 05:210.5000.200<0.200µg/L2-Chlorotoluene
04/28/23 05:210.5000.200<0.200µg/L4-Chlorotoluene
04/28/23 05:210.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
04/28/23 05:212.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
04/28/23 05:210.5000.230<0.230µg/LDibromomethane
04/28/23 05:210.5000.220<0.220µg/L1,2-Dichlorobenzene
04/28/23 05:210.5000.190<0.190µg/L1,3-Dichlorobenzene
04/28/23 05:210.5000.210<0.210µg/L1,4-Dichlorobenzene
04/28/23 05:215.001.20<1.20µg/LDichlorodifluoromethane
04/28/23 05:210.5000.240<0.240µg/L1,1-Dichloroethane
04/28/23 05:210.5000.150<0.150µg/L1,2-Dichloroethane
Page 2 of 17Date:05/02/2023 10:46 AM
Page 19 of 36
Quality Control Data
23-111-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #367
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V32559QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V32558
Associated Lab Samples: 94649
LRB-V32558 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/28/23 05:210.5000.150<0.150µg/L1,1-Dichloroethene
04/28/23 05:210.5000.200<0.200µg/Lcis-1,2-Dichloroethene
04/28/23 05:210.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
04/28/23 05:210.5000.190<0.190µg/L1,2-Dichloropropane
04/28/23 05:210.5000.130<0.130µg/L1,3-Dichloropropane
04/28/23 05:212.000.210<0.210µg/L2,2-Dichloropropane
04/28/23 05:210.5000.200<0.200µg/L1,1-Dichloropropene
04/28/23 05:210.5000.210<0.210µg/Lcis-1,3-Dichloropropene
04/28/23 05:210.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
04/28/23 05:2120042.0<42.0µg/LEthanol
04/28/23 05:210.5000.170<0.170µg/LEthylbenzene
04/28/23 05:213.000.350<0.350µg/LHexachlorobutadiene
04/28/23 05:211.000.380<0.380µg/L2-Hexanone
04/28/23 05:210.5000.180<0.180µg/LIsopropylbenzene
04/28/23 05:210.5000.089<0.089µg/L4-Isopropyl toluene
04/28/23 05:215.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
04/28/23 05:211.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
04/28/23 05:211.000.078<0.078µg/L4-Methyl-2-Pentanone
04/28/23 05:212.000.330<0.330µg/LMethylene Chloride
04/28/23 05:211.000.470<0.470µg/LNaphthalene
04/28/23 05:210.5000.190<0.190µg/Ln-Propylbenzene
04/28/23 05:210.5000.220<0.220µg/LStyrene
04/28/23 05:2110.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
04/28/23 05:2110.00.350<0.350µg/Ltert-Butyl formate (TBF)
04/28/23 05:2110.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
04/28/23 05:2110.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
04/28/23 05:210.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
Page 3 of 17Date:05/02/2023 10:46 AM
Page 20 of 36
Quality Control Data
23-111-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #367
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V32559QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V32558
Associated Lab Samples: 94649
LRB-V32558 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/28/23 05:210.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
04/28/23 05:210.5000.220<0.220µg/LTetrachloroethene
04/28/23 05:210.5000.220<0.220µg/LToluene
04/28/23 05:210.5000.380<0.380µg/L1,2,3-Trichlorobenzene
04/28/23 05:210.5000.310<0.310µg/L1,2,4-Trichlorobenzene
04/28/23 05:210.5000.160<0.160µg/L1,1,1-Trichloroethane
04/28/23 05:210.5000.096<0.096µg/L1,1,2-Trichloroethane
04/28/23 05:210.5000.180<0.180µg/LTrichloroethene
04/28/23 05:210.5000.180<0.180µg/LTrichlorofluoromethane
04/28/23 05:210.5000.270<0.270µg/L1,2,3-Trichloropropane
04/28/23 05:210.5000.190<0.190µg/L1,2,4-Trimethylbenzene
04/28/23 05:210.5000.180<0.180µg/L1,3,5-Trimethylbenzene
04/28/23 05:215.001.00<1.00µg/LVinyl Acetate
04/28/23 05:210.5000.170<0.170µg/LVinyl Chloride
04/28/23 05:210.5000.210<0.210µg/Lo-Xylene
04/28/23 05:211.000.420<0.420µg/Lm,p-Xylene
04/28/23 05:2110.01.00<1.00µg/L3,3-Dimethyl-1-butanol
04/28/23 05:214-Bromofluorobenzene (S)101 70-130
04/28/23 05:21Dibromofluoromethane (S)97.8 70-130
04/28/23 05:211,2-Dichloroethane - d4 (S)95.6 70-130
04/28/23 05:21Toluene-d8 (S)100 70-130
LCS-V32558Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
478*95.520.0µg/L3,3-Dimethyl-1-butanol 70-130
Page 4 of 17* QC Fail Date:05/02/2023 10:46 AM
Page 21 of 36
Quality Control Data
23-111-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #367
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V32559QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V32558
LCS-V32558 LCSD-V32558Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
33.9 84.788.735.540.0µg/LAcetone 40-160 4.6 20.0
19.9 99.510220.420.0µg/LBenzene 70-130 2.4 20.0
20.1 10110721.420.0µg/LBromobenzene 70-130 6.2 20.0
19.8 99.010320.520.0µg/LBromochloromethane 70-130 3.4 20.0
19.1 95.510020.020.0µg/LBromodichloromethane 70-130 4.6 20.0
18.3 91.592.018.420.0µg/LBromoform 70-130 0.5 20.0
19.8 99.097.019.420.0µg/LBromomethane 60-140 2.0 20.0
19.3 96.510120.220.0µg/Ln-Butylbenzene 70-130 4.5 20.0
19.2 96.010120.220.0µg/Lsec-Butyl benzene 70-130 5.0 20.0
19.2 96.010320.520.0µg/Ltert-Butyl benzene 70-130 6.5 20.0
19.2 96.099.019.820.0µg/LCarbon Tetrachloride 70-130 3.0 20.0
19.2 96.010120.220.0µg/LChlorobenzene 70-130 5.0 20.0
19.5 97.510220.420.0µg/LChlorodibromomethane 70-130 4.5 20.0
20.8 10411422.720.0µg/LChloroethane 60-140 8.7 20.0
19.6 98.010520.920.0µg/LChloroform 70-130 6.4 20.0
18.0 90.092.018.420.0µg/LChloromethane 60-140 2.1 20.0
19.6 98.010420.720.0µg/L2-Chlorotoluene 70-130 5.4 20.0
19.6 98.010320.520.0µg/L4-Chlorotoluene 70-130 4.4 20.0
19.0 95.098.519.720.0µg/LDi-Isopropyl Ether (DIPE)70-130 3.6 20.0
20.6 10395.019.020.0µg/L1,2-Dibromo-3-Chloropropane 70-130 8.0 20.0
19.2 96.010320.520.0µg/LDibromomethane 70-130 6.5 20.0
19.1 95.598.019.620.0µg/L1,2-Dichlorobenzene 70-130 2.5 20.0
19.7 98.510320.520.0µg/L1,3-Dichlorobenzene 70-130 3.9 20.0
19.0 95.010020.020.0µg/L1,4-Dichlorobenzene 70-130 5.1 20.0
17.7 88.587.517.520.0µg/LDichlorodifluoromethane 60-140 1.1 20.0
19.9 99.510420.820.0µg/L1,1-Dichloroethane 70-130 4.4 20.0
Page 5 of 17Date:05/02/2023 10:46 AM
Page 22 of 36
Quality Control Data
23-111-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #367
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V32559QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V32558
LCS-V32558 LCSD-V32558Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
18.1 90.596.019.220.0µg/L1,2-Dichloroethane 70-130 5.8 20.0
19.4 97.010220.320.0µg/L1,1-Dichloroethene 70-130 4.5 20.0
19.6 98.010120.220.0µg/Lcis-1,2-Dichloroethene 70-130 3.0 20.0
19.8 99.010621.120.0µg/Ltrans-1,2-Dichloroethene 70-130 6.3 20.0
20.0 10010420.720.0µg/L1,2-Dichloropropane 70-130 3.4 20.0
19.3 96.510220.420.0µg/L1,3-Dichloropropane 70-130 5.5 20.0
16.2 81.090.018.020.0µg/L2,2-Dichloropropane 70-130 10.5 20.0
21.0 10510921.720.0µg/L1,1-Dichloropropene 70-130 3.2 20.0
19.6 98.010020.020.0µg/Lcis-1,3-Dichloropropene 70-130 2.0 20.0
18.6 93.096.019.220.0µg/Ltrans-1,3-Dichloropropene 70-130 3.1 20.0
527 10594.6473500µg/LEthanol 60-140 10.8 20.0
19.4 97.010220.420.0µg/LEthylbenzene 70-130 5.0 20.0
19.1 95.594.518.920.0µg/LHexachlorobutadiene 70-130 1.0 20.0
17.6 88.097.019.420.0µg/L2-Hexanone 60-140 9.7 20.0
20.3 10210621.120.0µg/LIsopropylbenzene 70-130 3.8 20.0
19.9 99.510721.420.0µg/L4-Isopropyl toluene 70-130 7.2 20.0
16.4 82.088.017.620.0µg/LMethyl Ethyl Ketone (MEK)60-140 7.0 20.0
19.6 98.010220.320.0µg/LMethyl tert-butyl ether (MTBE)70-130 3.5 20.0
18.4 92.090.518.120.0µg/L4-Methyl-2-Pentanone 60-140 1.6 20.0
19.2 96.098.519.720.0µg/LMethylene Chloride 70-130 2.5 20.0
17.3 86.591.518.320.0µg/LNaphthalene 70-130 5.6 20.0
19.3 96.510420.720.0µg/Ln-Propylbenzene 70-130 7.0 20.0
19.5 97.510420.720.0µg/LStyrene 70-130 5.9 20.0
36.4 91.093.037.240.0µg/Ltert-Butyl Alcohol (TBA)40-140 2.1 20.0
39.0 97.510441.640.0µg/Ltert-Butyl formate (TBF)40-140 6.4 20.0
17.4 87.011422.720.0µg/Ltert-Amyl Alcohol (TAA)40-140 26.4*20.0
Page 6 of 17* QC Fail Date:05/02/2023 10:46 AM
Page 23 of 36
Quality Control Data
23-111-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #367
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V32559QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V32558
LCS-V32558 LCSD-V32558Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
39.9 99.710541.840.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 4.6 20.0
18.7 93.510320.520.0µg/L1,1,1,2-Tetrachloroethane 70-130 9.1 20.0
19.6 98.010420.820.0µg/L1,1,2,2-Tetrachloroethane 70-130 5.9 20.0
19.5 97.510320.520.0µg/LTetrachloroethene 70-130 5.0 20.0
19.4 97.010320.520.0µg/LToluene 70-130 5.5 20.0
20.6 10310921.720.0µg/L1,2,3-Trichlorobenzene 70-130 5.2 20.0
19.1 95.598.019.620.0µg/L1,2,4-Trichlorobenzene 70-130 2.5 20.0
18.6 93.010020.020.0µg/L1,1,1-Trichloroethane 70-130 7.2 20.0
19.4 97.010320.520.0µg/L1,1,2-Trichloroethane 70-130 5.5 20.0
19.7 98.510320.520.0µg/LTrichloroethene 70-130 3.9 20.0
18.3 91.596.519.320.0µg/LTrichlorofluoromethane 60-140 5.3 20.0
19.3 96.599.519.920.0µg/L1,2,3-Trichloropropane 70-130 3.0 20.0
19.8 99.010320.520.0µg/L1,2,4-Trimethylbenzene 70-130 3.4 20.0
20.0 10010621.220.0µg/L1,3,5-Trimethylbenzene 70-130 5.8 20.0
19.0 95.010821.520.0µg/LVinyl Acetate 60-140 12.3 20.0
20.0 10010320.620.0µg/LVinyl Chloride 60-140 2.9 20.0
19.3 96.510220.420.0µg/Lo-Xylene 70-130 5.5 20.0
39.6 99.010441.640.0µg/Lm,p-Xylene 70-130 4.9 20.0
1001014-Bromofluorobenzene (S)70-130
98.498.6Dibromofluoromethane (S)70-130
95.697.21,2-Dichloroethane - d4 (S)70-130
101101Toluene-d8 (S)70-130
Page 7 of 17Date:05/02/2023 10:46 AM
Page 24 of 36
Quality Control Data
23-111-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #367
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32426QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32424
Associated Lab Samples: 94650
LRB-V32424 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/25/23 10:440.0200.002<0.002mg/KgAcetone
04/25/23 10:440.0200.001<0.001mg/KgAcrolein
04/25/23 10:440.0200.0008<0.0008mg/KgAcrylonitrile
04/25/23 10:440.0050.0006<0.0006mg/KgBenzene
04/25/23 10:440.0050.0005<0.0005mg/KgBromobenzene
04/25/23 10:440.0050.0008<0.0008mg/KgBromochloromethane
04/25/23 10:440.0050.001<0.001mg/KgBromodichloromethane
04/25/23 10:440.0050.001<0.001mg/KgBromoform
04/25/23 10:440.0100.001<0.001mg/KgBromomethane
04/25/23 10:440.0050.0005<0.0005mg/Kgn-Butylbenzene
04/25/23 10:440.0050.0006<0.0006mg/Kgsec-Butyl benzene
04/25/23 10:440.0050.0005<0.0005mg/Kgtert-Butyl benzene
04/25/23 10:440.0050.0006<0.0006mg/KgCarbon Disulfide
04/25/23 10:440.0050.001<0.001mg/KgCarbon Tetrachloride
04/25/23 10:440.0050.0007<0.0007mg/KgChlorobenzene
04/25/23 10:440.0050.0009<0.0009mg/KgChlorodibromomethane
04/25/23 10:440.0100.0009<0.0009mg/KgChloroethane
04/25/23 10:440.0050.001<0.001mg/KgChloroform
04/25/23 10:440.0100.0006<0.0006mg/KgChloromethane
04/25/23 10:440.0050.0005<0.0005mg/Kg2-Chlorotoluene
04/25/23 10:440.0050.0004<0.0004mg/Kg4-Chlorotoluene
04/25/23 10:440.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
04/25/23 10:440.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
04/25/23 10:440.0050.0006<0.0006mg/Kg1,2-Dibromoethane
04/25/23 10:440.0050.0006<0.0006mg/KgDibromomethane
04/25/23 10:440.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
04/25/23 10:440.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 8 of 17Date:05/02/2023 10:46 AM
Page 25 of 36
Quality Control Data
23-111-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #367
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32426QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32424
Associated Lab Samples: 94650
LRB-V32424 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/25/23 10:440.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
04/25/23 10:440.0100.001<0.001mg/KgDichlorodifluoromethane
04/25/23 10:440.0050.0008<0.0008mg/Kg1,1-Dichloroethane
04/25/23 10:440.0050.001<0.001mg/Kg1,2-Dichloroethane
04/25/23 10:440.0050.0007<0.0007mg/Kg1,1-Dichloroethene
04/25/23 10:440.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
04/25/23 10:440.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
04/25/23 10:440.0050.0004<0.0004mg/Kg1,2-Dichloropropane
04/25/23 10:440.0050.0006<0.0006mg/Kg1,3-Dichloropropane
04/25/23 10:440.0050.001<0.001mg/Kg2,2-Dichloropropane
04/25/23 10:440.0050.0008<0.0008mg/Kg1,1-Dichloropropene
04/25/23 10:440.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
04/25/23 10:440.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
04/25/23 10:440.0050.0006<0.0006mg/KgEthylbenzene
04/25/23 10:440.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
04/25/23 10:440.0100.0008<0.0008mg/KgHexachlorobutadiene
04/25/23 10:440.0100.0007<0.0007mg/Kgn-Hexane
04/25/23 10:440.0200.0006<0.0006mg/Kg2-Hexanone
04/25/23 10:440.0050.0005<0.0005mg/KgIsopropylbenzene
04/25/23 10:440.0050.001<0.001mg/Kg4-Isopropyl toluene
04/25/23 10:440.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
04/25/23 10:440.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
04/25/23 10:440.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
04/25/23 10:440.0100.0010.002mg/KgMethylene Chloride
04/25/23 10:440.0100.0010<0.0010mg/KgNaphthalene
04/25/23 10:440.0050.0005<0.0005mg/Kgn-Propylbenzene
04/25/23 10:440.0050.001<0.001mg/KgStyrene
Page 9 of 17Date:05/02/2023 10:46 AM
Page 26 of 36
Quality Control Data
23-111-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #367
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32426QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32424
Associated Lab Samples: 94650
LRB-V32424 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/25/23 10:440.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
04/25/23 10:440.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
04/25/23 10:440.0050.0009<0.0009mg/KgTetrachloroethene
04/25/23 10:440.0050.0007<0.0007mg/KgToluene
04/25/23 10:440.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
04/25/23 10:440.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
04/25/23 10:440.0050.001<0.001mg/Kg1,1,1-Trichloroethane
04/25/23 10:440.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
04/25/23 10:440.0050.0009<0.0009mg/KgTrichloroethene
04/25/23 10:440.0100.002<0.002mg/KgTrichlorofluoromethane
04/25/23 10:440.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
04/25/23 10:440.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
04/25/23 10:440.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
04/25/23 10:440.0100.0005<0.0005mg/KgVinyl Acetate
04/25/23 10:440.0100.0005<0.0005mg/KgVinyl Chloride
04/25/23 10:440.0050.0005<0.0005mg/Kgo-Xylene
04/25/23 10:440.0100.001<0.001mg/Kgm,p-Xylene
04/25/23 10:444-Bromofluorobenzene (S)101 70-130
04/25/23 10:44Dibromofluoromethane (S)95.0 84-123
04/25/23 10:44Toluene-d8 (S)91.6 76-129
LCS-V32424 LCSD-V32424Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.080 80.075.60.0750.100mg/KgAcetone 29-198 5.6 20
0.085 85.078.30.0780.100mg/KgAcrolein 70-130 8.2 20
Page 10 of 17Date:05/02/2023 10:46 AM
Page 27 of 36
Quality Control Data
23-111-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #367
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32426QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32424
LCS-V32424 LCSD-V32424Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.102 10296.20.0960.100mg/KgAcrylonitrile 65-134 5.8 20
0.046 92.897.20.0480.050mg/KgBenzene 74-127 4.6 20
0.042 85.083.00.0410.050mg/KgBromobenzene 73-125 2.3 20
0.051 1031060.0520.050mg/KgBromochloromethane 72-134 2.6 20
0.049 98.01010.0500.050mg/KgBromodichloromethane 75-122 3.2 20
0.051 1031020.0510.050mg/KgBromoform 66-135 1.1 20
0.039 78.492.40.0460.050mg/KgBromomethane 20-180 16.3 20
0.041 83.887.20.0430.050mg/Kgn-Butylbenzene 65-135 3.9 20
0.041 83.086.00.0430.050mg/Kgsec-Butyl benzene 66-131 3.5 20
0.040 81.886.40.0430.050mg/Kgtert-Butyl benzene 67-132 5.4 20
0.044 89.896.80.0480.050mg/KgCarbon Disulfide 61-129 7.5 20
0.048 97.81020.0510.050mg/KgCarbon Tetrachloride 64-143 4.5 20
0.046 92.294.00.0470.050mg/KgChlorobenzene 74-118 1.9 20
0.048 96.698.80.0490.050mg/KgChlorodibromomethane 73-122 2.2 20
0.036 72.072.00.0360.050mg/KgChloroethane 33-149 0.0 20
0.047 95.499.60.0490.050mg/KgChloroform 73-127 4.3 20
0.046 93.695.00.0470.050mg/KgChloromethane 45-143 1.4 20
0.041 83.684.60.0420.050mg/Kg2-Chlorotoluene 67-124 1.1 20
0.041 83.684.60.0420.050mg/Kg4-Chlorotoluene 71-126 1.1 20
0.046 92.293.60.0460.050mg/KgDi-Isopropyl Ether (DIPE)59-159 1.5 20
0.054 1091020.0510.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 6.4 20
0.050 1001040.0510.050mg/Kg1,2-Dibromoethane 70-132 3.3 20
0.052 1041060.0530.050mg/KgDibromomethane 74-133 1.8 20
0.044 89.690.60.0450.050mg/Kg1,2-Dichlorobenzene 72-123 1.1 20
0.044 89.088.60.0440.050mg/Kg1,3-Dichlorobenzene 71-120 0.4 20
0.042 85.286.40.0430.050mg/Kg1,4-Dichlorobenzene 71-123 1.3 20
Page 11 of 17Date:05/02/2023 10:46 AM
Page 28 of 36
Quality Control Data
23-111-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #367
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32426QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32424
LCS-V32424 LCSD-V32424Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.044 89.098.00.0490.050mg/KgDichlorodifluoromethane 26-146 9.6 20
0.047 94.899.80.0490.050mg/Kg1,1-Dichloroethane 74-127 5.1 20
0.047 95.295.60.0470.050mg/Kg1,2-Dichloroethane 68-128 0.4 20
0.043 87.893.20.0460.050mg/Kg1,1-Dichloroethene 67-149 5.9 20
0.046 92.096.20.0480.050mg/Kgcis-1,2-Dichloroethene 76-134 4.4 20
0.045 90.095.20.0470.050mg/Kgtrans-1,2-Dichloroethene 73-132 5.6 20
0.049 98.496.80.0480.050mg/Kg1,2-Dichloropropane 73-130 1.6 20
0.047 94.296.20.0480.050mg/Kg1,3-Dichloropropane 75-124 2.1 20
0.045 90.298.40.0490.050mg/Kg2,2-Dichloropropane 50-142 8.6 20
0.047 95.01020.0510.050mg/Kg1,1-Dichloropropene 71-130 7.3 20
0.050 1011030.0510.050mg/Kgcis-1,3-Dichloropropene 71-125 1.3 20
0.052 1051030.0510.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.9 20
0.042 85.691.00.0450.050mg/KgEthylbenzene 74-128 6.1 20
0.094 94.393.70.0930.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.6 20
0.044 89.694.60.0470.050mg/KgHexachlorobutadiene 64-125 5.4 20
0.046 92.81020.0510.050mg/Kgn-Hexane 70-130 9.8 20
0.044 89.085.00.0420.050mg/Kg2-Hexanone 61-157 4.5 20
0.041 83.087.20.0430.050mg/KgIsopropylbenzene 68-126 4.9 20
0.042 85.287.20.0430.050mg/Kg4-Isopropyl toluene 68-129 2.3 20
0.031 62.2*59.2*0.0290.050mg/KgMethyl Ethyl Ketone (MEK)63-149 4.9 20
0.049 99.698.40.0490.050mg/KgMethyl tert-butyl ether (MTBE)70-130 1.2 20
0.055 1111030.0510.050mg/Kg4-Methyl-2-Pentanone 57-162 7.4 20
0.041 82.680.80.0400.050mg/KgMethylene Chloride 74-129 2.2 20
0.050 10195.60.0470.050mg/KgNaphthalene 57-157 5.4 20
0.040 81.884.80.0420.050mg/Kgn-Propylbenzene 67-130 3.6 20
0.045 91.898.20.0490.050mg/KgStyrene 77-121 6.7 20
Page 12 of 17* QC Fail Date:05/02/2023 10:46 AM
Page 29 of 36
Quality Control Data
23-111-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #367
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32426QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32424
LCS-V32424 LCSD-V32424Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.046 92.294.80.0470.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 2.7 20
0.046 92.088.20.0440.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 4.2 20
0.049 98.21040.0520.050mg/KgTetrachloroethene 68-130 6.1 20
0.046 93.298.80.0490.050mg/KgToluene 71-129 5.8 20
0.049 99.498.60.0490.050mg/Kg1,2,3-Trichlorobenzene 68-130 0.8 20
0.049 99.01030.0510.050mg/Kg1,2,4-Trichlorobenzene 66-125 3.7 20
0.046 92.01010.0500.050mg/Kg1,1,1-Trichloroethane 67-131 9.7 20
0.048 96.297.60.0480.050mg/Kg1,1,2-Trichloroethane 70-133 1.4 20
0.048 97.81010.0500.050mg/KgTrichloroethene 75-133 2.8 20
0.036 72.673.20.0360.050mg/KgTrichlorofluoromethane 44-146 0.8 20
0.049 98.290.60.0450.050mg/Kg1,2,3-Trichloropropane 60-137 8.0 20
0.042 84.485.80.0420.050mg/Kg1,2,4-Trimethylbenzene 69-129 1.6 20
0.041 82.884.20.0420.050mg/Kg1,3,5-Trimethylbenzene 69-128 1.6 20
0.053 1071040.0520.050mg/KgVinyl Acetate 60-140 2.2 20
0.047 94.61000.0500.050mg/KgVinyl Chloride 48-147 5.5 20
0.043 86.092.60.0460.050mg/Kgo-Xylene 74-126 7.3 20
0.087 87.292.70.0920.100mg/Kgm,p-Xylene 75-124 6.1 20
1011004-Bromofluorobenzene (S)70-130
96.695.6Dibromofluoromethane (S)84-123
88.491.4Toluene-d8 (S)76-129
Page 13 of 17Date:05/02/2023 10:46 AM
Page 30 of 36
Quality Control Data
23-111-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #367
QC Prep Batch Method:
EDB and DBCP by Microextraction GC/ECD
EPA-504.1
V32508QC Analytical Batch(es):
Analysis Method:
Analysis Description:
EPA-504.1(PREP)
QC Prep:V32463
Associated Lab Samples: 94649
LRB-V32463 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
04/27/23 11:390.02000.00330<0.00330µg/L1,2-Dibromoethane
LCS-V32463 LCSD-V32463Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.425 170*139*0.3480.250µg/L1,2-Dibromoethane 70-130 19.9 20.0
V 94769-DUP-V32463Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 04/27/23 12:57182*0.430< 0.0208µg/L1,2-Dibromoethane
Page 14 of 17* QC Fail Date:05/02/2023 10:46 AM
Page 31 of 36
Quality Control Data
23-111-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #367
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V32302QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V32301
Associated Lab Samples: 94650
LRB-V32301 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/22/23 14:288.001.22<1.22mg/KgAliphatic C5-C8
04/22/23 14:288.004.56<4.56mg/KgAliphatic C9-C12
04/22/23 14:288.000.624<0.624mg/KgAromatic C9-C10
04/22/23 14:282,5-Dibromotoluene (FID) (S)80.0 70-130
04/22/23 14:282,5-Dibromotoluene (PID) (S)76.9 70-130
LCS-V32301 LCSD-V32301Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
34.1 10710935.032.0mg/KgAliphatic C5-C8 70-130 2.6 50
34.5 10810935.032.0mg/KgAliphatic C9-C12 70-130 1.4 50
10.9 10210411.110.7mg/KgAromatic C9-C10 70-130 1.8 50
90.487.52,5-Dibromotoluene (FID) (S)70-130
80.876.32,5-Dibromotoluene (PID) (S)70-130
Page 15 of 17Date:05/02/2023 10:46 AM
Page 32 of 36
Quality Control Data
23-111-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #367
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V32357QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V32356
Associated Lab Samples: 94649
LRB-V32356 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/24/23 14:0550.011.5<11.5µg/LAliphatic C5-C8
04/24/23 14:0550.025.8<25.8µg/LAliphatic C9-C12
04/24/23 14:0550.04.02<4.02µg/LAromatic C9-C10
04/24/23 14:052,5-Dibromotoluene (FID) (S)77.4 70-130
04/24/23 14:052,5-Dibromotoluene (PID) (S)81.7 70-130
LCS-V32356 LCSD-V32356Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
284 94.694.6284300µg/LAliphatic C5-C8 70-130 0.0 50.0
323 108107321300µg/LAliphatic C9-C12 70-130 0.6 50.0
102 102108108100µg/LAromatic C9-C10 70-130 5.7 50.0
79.185.22,5-Dibromotoluene (FID) (S)70-130
79.676.62,5-Dibromotoluene (PID) (S)70-130
Page 16 of 17Date:05/02/2023 10:46 AM
Page 33 of 36
Quality Control Data
23-111-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #367
Dry Weight Determination
SW-DRYWT
V32568QC Analytical Batch:
Analysis Method:
Analysis Description:
V 94818-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 04/30/23 12:305.716.817.8%Moisture
V 95042-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 04/30/23 12:305.918.019.1%Moisture
Page 17 of 17Date:05/02/2023 10:46 AM
Page 34 of 36
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-111-0022
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 2.6C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Danyale Love Date & Time:04/21/2023 15:36:41
Special precautions or instructions included?
Comments:
Page 35 of 36
Page 36 of 36