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HomeMy WebLinkAboutFA-7966_42211_CA_MRP_20230302_8132 Speedway, LLC 500 Speedway Drive Enon, Ohio 45323 Phone: (937) 864-3000 Groundwater Monitoring Report Speedway Store No. 8232 24 South Raleigh Street Angier, Harnett County, North Carolina Incident No. 8132 Project No. 60689740 March 2, 2023 AECOM ii Speedway 8232 Angier, NC Groundwater Monitoring Report February 2023 Quality Information Prepared by Reviewed by Elizabeth Andrews Environmental Scientist Elizabeth.Andrews@aecom.com Marianne Link, PG Project Manager Marianne.Link@aecom.com Reviewed by Marie Treiber Marie.Treiber@aecom.com Regional Senior Project Manager Prepared for: Speedway, LLC 500 Speedway Drive Enon, Ohio 45323 Phone: (937) 864-3000 Prepared by: AECOM Technical Services of North Carolina, Inc. 5438 Wade Park Blvd, Suite 200 Raleigh, North Carolina 27607 Phone: (919) 461-1100 aecom.com Copyright © 2023 by AECOM All rights reserved. No part of this copyrighted work may be reproduced, distributed, or transmitted in any form or by any means without the prior written permission of AECOM. AECOM iv Speedway 8232 Angier, NC Groundwater Monitoring Report February 2023 Table of Contents Executive Summary ................................................................................................................................................. ES-1 1 Introduction ...................................................................................................................................................... 1-1 2 Site Background Information ............................................................................................................................ 2-1 2.3 Information about the Release .............................................................................................................. 2-1 3 Site History and Characterization..................................................................................................................... 3-1 3.1 Underground Storage Tank Systems .................................................................................................... 3-1 3.2 Aboveground Storage Tank Systems .................................................................................................... 3-1 3.3 Historical Releases ............................................................................................................................... 3-1 3.4 Site Characteristics ............................................................................................................................... 3-1 3.4.1 Zoning/Receptor Information ..................................................................................................... 3-1 3.4.2 Site Geology and Hydrogeology................................................................................................ 3-1 4 Receptor Information ....................................................................................................................................... 4-1 4.1 Water Supply Wells............................................................................................................................... 4-1 4.1.1 Private Water Supply Wells ....................................................................................................... 4-1 4.1.2 Public Water Systems ............................................................................................................... 4-1 4.2 Surface Water ....................................................................................................................................... 4-1 4.3 Wellhead Protection Areas ................................................................................................................... 4-1 5 Groundwater Investigation ............................................................................................................................... 5-1 5.1 Groundwater Gauging .......................................................................................................................... 5-1 5.2 Groundwater Sampling ......................................................................................................................... 5-1 5.3 Groundwater Analytical Results ............................................................................................................ 5-1 6 LNAPL Investigation and Recovery ................................................................................................................. 6-1 7 Discussion ....................................................................................................................................................... 7-1 8 References ...................................................................................................................................................... 8-1 AECOM v Speedway 8232 Angier, NC Groundwater Monitoring Report February 2023 Figures Figure 1: Site Location Map Figure 2: Site Plan Figure 3: Groundwater Elevation Map, November 2022 Figure 4: Contaminants of Concern Concentration Map, November 2022 Tables Table 1: Site History – UST Owner/Operator and Other Responsible Party Information Table 2: Site History – UST System and Other Release Information Table 3: Well Construction and Historical Groundwater Elevations Table 4: Summary of Recent and Historical Groundwater Monitoring Results for Selected Compounds Appendices Appendix A. Groundwater Analytical Report AECOM vi Speedway 8232 Angier, NC Groundwater Monitoring Report February 2023 Acronyms 2L Title 15 NCAC 2L.0202 Groundwater Standard AECOM AECOM Technical Services of North Carolina, Inc. AST aboveground storage tanks ATC ATC Associates of North Carolina, Inc. bgs below ground surface EPA United States Environmental Protection Agency GCL Gross Contamination Levels GIS Geographic Information System HCDPU Harnett County Department of Public Utilities LNAPL light non-aqueous phase liquid LSA Limited Site Assessment MTBE Methyl tert-butyl ether NCDEQ North Carolina Department of Environmental Quality NORR Notice of Regulatory Requirement Pace Pace Analytical Services, LLC Site Speedway Store No. 8232 Speedway Speedway, LLC UST underground storage tank VOC volatile organic constituent ES-1 Speedway 8232 Angier, NC Groundwater Monitoring Report February 2023 Executive Summary As required by the North Carolina Department of Environmental Quality (NCDEQ), AECOM Technical Services of North Carolina, Inc. (AECOM) on behalf of Speedway, LLC (Speedway) has prepared this Groundwater Monitoring Report for Speedway Store No. 8232 (Site), located at 24 South Raleigh Street, Angier, Harnett County, North Carolina. The Site is currently owned by Williams Family Heirs, LLC and operates as an active Speedway gas station and convenience store. This report includes the groundwater sampling conducted in November 2022. In April 2022, an Additional Assessment Report was submitted to NCDEQ by Speedway’s former consultant, ATC Associates of North Carolina, P.C. [(ATC), 2022]. The Additional Assessment Report recommended comprehensive groundwater monitoring events be conducted to determine the stability of the impacted groundwater plume and performing a survey of the monitoring well MW-04. The NCDEQ acknowledged the receipt of the report in a letter dated May 9, 2022. NCDEQ requested the collection and submittal of groundwater samples from all wells exceeding the Title 15 NCAC 2L.0202 Groundwater Standard (2L Standard) and survey all wells to determine the groundwater flow direction. On November 3, 2022, six monitoring wells (MW-01, MW-02, MW-03, MW-04, MW-05 and MW-06) were gauged, purged, and sampled by AECOM field staff. The groundwater samples were analyzed for Volatile Organic Compounds (VOCs) via Environmental Protection Agency (EPA) Method 6200B. Laboratory results indicate the presence of petroleum compounds in several monitoring wells at concentrations that exceed the 2L Standard but not the Gross Contamination Level (GCL). Light non-aqueous phase liquid (LNAPL) has not been detected in any of the wells gauged onsite. AECOM, on behalf of Speedway, recommends continued semi-annual groundwater monitoring events be conducted in May and November 2023 to monitor natural attenuation of the contamination plume. The risk category of the Site should remain “Intermediate” due to the presence of an intermediate stream approximately 275 feet west of the Site. AECOM 1-1 Speedway 8232 Angier, NC Groundwater Monitoring Report February 2023 1 Introduction As required by the North Carolina Department of Environmental Quality (NCDEQ), AECOM Technical Services of North Carolina, Inc. (AECOM) on behalf of Speedway LLC (Speedway) has prepared this Groundwater Monitoring Report for Speedway Store No. 8232 (Site), located at 24 South Raleigh Street, Angier, Harnett County, North Carolina. The Site is currently owned by Williams Family Heirs, LLC and is operated by Speedway, LLC as a petroleum retail facility and convenience store. AECOM 2-1 Speedway 8232 Angier, NC Groundwater Monitoring Report February 2023 2 Site Background Information The following sections provide Site background and contact information. 2.1 Site Identification Date of Incident Report: December 5, 2017 Facility ID: 0-034026 Incident Number: 42211 Site Rank: Intermediate Risk Site Name: Speedway Store No. 8232 Site Street Address: 24 South Raleigh Street City/Town: Angier Zip Code: 27501 County: Harnett Description of Geographical Data Point (e.g., dispenser): dispenser island canopy Location Method (global positioning system, topographical map, other): Google Earth Latitude (decimal degrees): 35.507025° N, Longitude (decimal degrees): -78.740953° W 2.2 Contact Information UST Owner: Speedway, LLC Telephone: (937) 864-3000 Address: 500 Speedway Drive Enon, Ohio 45323 UST Operator: Speedway, LLC Telephone: (937) 864-3000 Address: 500 Speedway Drive Enon, Ohio 45323 Property Owner: Williams Family Heirs, LLC Telephone: Unknown Address: 3602 Hwy264 East Greenville, NC 27858 Property Occupant: Speedway, LLC Telephone: (937) 864-3000 Address: 500 Speedway Drive Enon, Ohio 45323 Consultant: AECOM Address: 5438 Wade Park Boulevard, Suite 200 Raleigh, NC Telephone: (919) 461-1100 Analytical Laboratory: Pace State Certification No. 5342 Address: 9800 Kincey Avenue # 100, Huntersville, NC 28078 Telephone: (704) 875-9092 2.3 Information about the Release Recently, there have been three releases associated with the Site: – On December 4, 2017, water was detected in the Number (No.) 4 diesel UST. Sludge and diesel fluid were removed, and the tank was placed out of service. The release was reported on December AECOM 2-2 Speedway 8232 Angier, NC Groundwater Monitoring Report February 2023 5, 2017 with submittal of the Form UST-61. The No. 4 diesel UST closed in place according to the Underground Storage Tank Closure Report (ATC, 2021). Incident number 42211 was assigned to this release by the NCDEQ. – On September 18, 2018, Speedway submitted a NCDEQ Form UST-17A which documented a failed tank tightness test of the No. 3 premium unleaded gasoline UST. On September 19, 2018, UST No. 3 was repaired and passed its tank tightness tests. Form UST-61 was submitted on May 10, 2019. This incident was included in Incident No. 42211. – On May 7, 2019, a diesel spill occurred at satellite dispenser No. 12 due to a leaking hose/nozzle. On May 10, 2019, Speedway submitted NCDEQ Form UST-61. The Site Check Report (ATC, 2019a) summarizes the emergency response and site check activities performed by Speedway. ATC submitted the Limited Site Assessment (LSA) to the NCDEQ on August 16, 2019. The diesel spill was tracked by NCDEQ under UST No. FA-7992, however, an incident number was not assigned. NCDEQ determined that the releases associated with the No. 4 Diesel UST and the No. 3 Premium Unleaded Gasoline UST would be addressed together under Incident No. 42211. NCDEQ also determined that the releases associated with Incident No. 42211 are commingled with the release associated with Incident No. 8132 that occurred in 1991 and was closed in 1992. Speedway’s former consultant, ATC, submitted a Limited Site Assessment (LSA) on December 23, 2019. Based on the results of the LSA, the NCDEQ issued a Notice of Regulatory Requirement (NORR) on February 5, 2020 requesting a Phase II LSA to be conducted. The LSA Phase II Report (ATC, 2020) was submitted to the NCDEQ on August 13, 2020. After reviewing the LSA Phase II report, the NCDEQ issued a NORR on November 25, 2020 requesting that further assessment be conducted, and a groundwater sampling report be submitted to further assess contamination and determine further assessment or corrective action. A groundwater monitoring report was submitted to NCDEQ on July 2, 2021. Based on the results from the groundwater monitoring report, NCDEQ requested one additional Type II monitoring well to be installed. The field activities were conducted in May 2021. An Additional Assessment Report was submitted to the NCDEQ on April 15, 2022. The NCDEQ acknowledged the receipt of the report in a letter dated May 9, 2022. NCDEQ requested the collection and submittal of groundwater samples from all wells exceeding the Title 15 NCAC 2L.0202 Groundwater Standard (2L Standard) and survey all wells to determine the groundwater flow direction. AECOM 3-1 Speedway 8232 Angier, NC Groundwater Monitoring Report February 2023 3 Site History and Characterization The following sections provide information on the USTs operated at the Site and follows the general outline established in Guidelines for Assessment and Corrective Action for UST Releases (NCDEQ, 2021a) and Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement for UST Releases (NCDEQ, 2021b) using the Comprehensive Tables for Corrective Action Guidelines Tables (NCDEQ, 2022). 3.1 Underground Storage Tank Systems The Site is currently in use as a Speedway gas station and convenience store and operates one 10,000-gallon and one 6, 000-gallon regular unleaded gasoline UST, one 6,000-gallon premium unleaded UST and one 6,000-gallon diesel UST. The current USTs were installed by the Trade Oil Company and are owned by Speedway. UST owner/operator information and UST system information are included in Tables 1 and 2, respectively. According to the Harnett County, North Carolina Geographic Information System (GIS) mapping service, the current property owner of the Site is listed as Williams Family Heirs, LLC. 3.2 Aboveground Storage Tank Systems No aboveground storage tank systems (ASTs) are currently present onsite. Based on available information, no ASTs have historically been present at the Site. 3.3 Historical Releases D.K. Taylor Oil Company, Inc. dba Dennings/Angier Exxon was responsible for Incident No. 8132 which was discovered and reported on June 24, 1991 when gasoline-impacted soil was encountered beneath three (3) 6,000- gallon gasoline USTs during removal activities. The USTs had been in service from 1973 and were removed in 1991 and 1993. The incident was closed on June 3,1992. A former Gulf Station was located north of the Site. A release of unknown quantity from an unknown responsible party was suspected. Records available on the NCDEQ Incident Map indicated that this incident was closed on 4/13/1999 following environmental investigation and corrective action activities performed by Chevron. 3.4 Site Characteristics The location of the Site is shown on a portion of the United States Geological Survey Angier, NC (2022) digital raster graphic file (Figure 1). The Site layout is found on Figure 2. The Site is currently operational and is occupied by a Speedway petroleum retail facility and convenience store. A McDonald’s restaurant is also located onsite, to the south of the convenience store. The Site is located at 24 South Raleigh Street, Angier, North Carolina and is accessed from West Depot Street, located North of the Site, as well as from South Raleigh Street, located East of the Site. Various commercial and residential properties surround the Site. 3.4.1 Zoning/Receptor Information The Site and adjoining properties are currently zoned Residential and business (Harnett County GIS Viewer). The previous consultant, ATC Associates of North Carolina, Inc. (ATC), conducted a receptor survey to identify the presence of water supply wells within a 1,500-foot radius from the Site. The receptor survey is documented in the LSA (ATC, 2019b). 3.4.2 Site Geology and Hydrogeology Site geology was evaluated based on historic and current investigations completed by previous consultants and AECOM. The Site is located within the Inner Coastal Plain Physiographic Region of North Carolina and is underlain AECOM 3-2 Speedway 8232 Angier, NC Groundwater Monitoring Report February 2023 by the Cretaceous Middendorf Formation. The Site is generally underlain by sand, sandstone and mudstone, pale gray to gray in color with orange casts, clay balls and iron-cemented concretions. Crossbedding is common and the beds are laterally discontinuous. Previous investigations show the soil has consisted of mainly dark brown to tan sandy silts and silty sands. Groundwater is encountered on average at approximately 3.24 feet below ground surface (bgs). Based on the results of the November 3, 2022, gauging event, groundwater flow is to the south, which is generally consistent with historical groundwater flow. Well construction and historical groundwater elevations are summarized on Table 3, and a groundwater elevation map (Figure 3) was constructed based on the November 3, 2022, gauging results. The hydraulic gradient, as measured from monitoring well MW-02 to MW-05, is 0.005 ft/ft [(283.99-283.41)/128]. Hydraulic Gradient = Δ𝑦 Δ𝑥 Δy = Change in groundwater elevation from MW-02 to MW-05 Δx = Distance between MW-02 and MW-05 AECOM 4-1 Speedway 8232 Angier, NC Groundwater Monitoring Report February 2023 4 Receptor Information 4.1 Water Supply Wells Speedway’s previous consultant, ATC, conducted a receptor survey as part of the LSA to identify the presence of water supply wells within a 1,500-foot radius from the Site. The receptor survey is cited within the LSA report submitted in December 2019. 4.1.1 Private Water Supply Wells Suspected well structures were identified according to a LSA report submitted in December 2019. Water supply well forms were sent to property owners at the suspect locations. In addition, water supply well forms were sent to all properties within 500 feet of the Site. Based on the completed/returned water supply well surveys, there were no water supply wells identified in the vicinity of the Site. 4.1.2 Public Water Systems Harnett County Department of Public Utilities (HCDPU) is the primary water utility for the area. The public water sources are the Cape Fear River, located approximately eight miles southwest of the Site. Based on currently available information, many properties surrounding the Site receive their municipal water supplies through buried piping that runs beneath the streets and highway easements. 4.2 Surface Water No surface water was observed on the Site. The previous consultant identified a small, intermittent stream approximately 275 feet west of the Site. A stormwater drainage ditch is located approximately 270 feet west of the Site and drains into the Black River, located approximately 1,500 feet northeast of the Site. A small, unnamed creek – a tributary of the Black River – was identified approximately 1,000 feet southwest of the Site. 4.3 Wellhead Protection Areas According to the NCDEQ Well Head Protection website, last updated in December 2022, there are no approved wellhead protection plans located in Harnett County. AECOM 5-1 Speedway 8232 Angier, NC Groundwater Monitoring Report February 2023 5 Groundwater Investigation During the current monitoring period, activities included groundwater gauging and sampling. 5.1 Groundwater Gauging On November 3, 2022, monitoring wells MW-01, MW-02, MW-03, MW-04, MW-05 and MW-06 were gauged for depth to water and depth to light non-aqueous phase liquid (LNAPL), if present. LNAPL was not observed at the Site. Depths to groundwater ranged from 1.96 to 4.25 feet bgs at monitoring wells MW-05 and MW-02, respectively. Depth to water and calculated groundwater elevations for the current and historic gauging events are included on Table 3. 5.2 Groundwater Sampling Prior to the collection of a groundwater sample for laboratory analysis, the depth to liquid or LNAPL was measured using an electronic oil-water interface probe. If no LNAPL was present, the well was purged of at least three well volumes using a dedicated disposable polyethylene bailer attached to nylon rope. Once the wells had been properly purged, groundwater samples were collected from each location using dedicated disposable polyethylene bailers attached to nylon rope. To collect a sample, the bailer was slowly lowered to a depth just beneath the water surface in the well. The bailer was then recovered, and the contents carefully decanted into laboratory-supplied sample containers, properly preserved, and delivered to Pace Analytical Services, LLC (Pace), a North Carolina-certified laboratory. 5.3 Groundwater Analytical Results On November 3, 2022, six monitoring wells MW-01, MW-02, MW-03, MW-04, MW-05 and MW-06 were gauged, purged, and sampled by AECOM field staff. The groundwater samples were analyzed for Volatile Organic Compounds (VOCs) via Environmental Protection Agency (EPA) Method 6200B. Laboratory results indicate the presence of petroleum compounds in several monitoring wells at concentrations that exceed the 2L Standard but not the Gross Contamination Level (GCL). Benzene and naphthalene were reported in monitoring wells MW-01, MW-03, MW-04, MW-05 and MW-06. Ethylbenzene, methyl tert-butyl ether (MTBE) and isopropylbenzene was reported in monitoring well MW-06. Total xylenes were reported in monitoring well MW-01. N-propylbenzene was reported in monitoring wells MW-01, MW-03, MW-05 and MW-06. Recent and historical analytical results are summarized in Table 4. A contaminants of concern concentration map is shown on Figure 4. Laboratory analytical reports are included in Appendix A. 5.4 Monitoring Well Survey On November 3, 2022, six monitoring wells MW-01, MW-02, MW-03, MW-04, MW-05 and MW-06 were surveyed using a Duncan Parnell VRS-GPS unit. The VRS-GPS unit provided elevations with respect to the NAD83 (2011) datum. AECOM 6-1 Speedway 8232 Angier, NC Groundwater Monitoring Report February 2023 6 LNAPL Investigation and Recovery Historically, LNAPL has not been detected at this Site. AECOM 7-1 Speedway 8232 Angier, NC Groundwater Monitoring Report February 2023 7 Discussion Analysis of the groundwater samples collected on November 3, 2022, indicate the presence of petroleum compounds in several monitoring wells at concentrations that exceed the 2L Standard but not the GCL. Based on the results of the groundwater monitoring event: − Constituents detected above the 2L Standard include benzene and naphthalene (MW-01, MW-03, MW-04, MW-05 and MW-06); ethylbenzene, MTBE and isopropylbenzene (MW-06); total xylenes (MW-01); and n- propylbenzene (MW-01, MW-03, MW-05 and MW-06). − The concentrations of petroleum-related constituents have remained the same or decreased in all monitoring wells except for monitoring well MW-05, the furthest downgradient well, which increased but remains well below the GCL. − LNAPL was not detected in any of the wells gauged onsite. − Water level measurements collected from the Site indicate that groundwater flow direction corresponded with historical flow direction, which has been generally towards the south. AECOM, on behalf of Speedway, recommends continued semi-annual groundwater monitoring events be conducted in May and November 2023 to monitor natural attenuation of the contamination plume. If constituents detected in downgradient well MW-05 continue to increase, further delineation may be warranted downgradient of the Site to the south. The risk classification for the Site should remain “Intermediate”. AECOM 8-1 Speedway 8232 Angier, NC Groundwater Monitoring Report February 2023 8 References NCDEQ, 2021a. Guidelines for Assessment and Corrective Action for UST Releases. Effective January 19, 2021. NCDEQ, 2021b. Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement for UST Releases. Change 11, effective May 17, 2021. NCDEQ, 2022. Comprehensive Tables for Corrective Action Guidelines. Effective September 7,2022. ATC, 2019a. Site Check Report, Speedway No. 8232. Prepared for Speedway, LLC by ATC Associates of North Carolina, Inc., July 19, 2019. ATC, 2019b. Limited Site Assessment Report, Speedway No. 8232. Prepared for Speedway, LLC by ATC Associates of North Carolina, Inc., December 23, 2019. ATC, 2020. Phase II Limited Site Assessment Report, Speedway No. 8232. Prepared for Speedway, LLC by ATC Associates of North Carolina, Inc., August 13, 2020 ATC, 2021. Underground Storage Tank Closure Report, Speedway No. 8232. Prepared for Speedway, LLC by ATC Associates of North Carolina, Inc., August 18, 2021 ATC, 2022. Additional Assessment Report, Speedway No. 8232. Prepared for Speedway, LLC by ATC Associates of North Carolina, Inc., April 15, 2022. Figures 2,0002,000 N SITE LOCATION I. DUMITRU FIGURE 1SITE LOCATION MAP Source: Topo USGS 7.5 Minute Topographic Map Quadrangle: Angier, NC Copyright: 2022 National Geographic Society DATE:DRAWN BY:REVIEWED BY:PROJECT NO.:Fil e : C : \ C o n f i d e n t i a l \ A E C O M \ 7 - E l e v e n \ S i t e s F o l d e r s \ N o r t h C a r o l i n a \ 8 2 3 2 A n g i e r \ 8 2 3 2 A n g i e r . d w g L a y o u t : S i t e L o c a t i o n M a p D a t e : 1 4 D e c , 2 0 2 2 X r e f s : 00 SCALE IN FEET: NOTE: ALL MAP FEATURES ARE APPROXIMATE IN SCALE AND LOCATION. DECEMBER 2022 E. ANDREWS Speedway Store #8232 24 South Raleigh Street Angier, North Carolina 60689740 Speedway LLC. © 2022 Microsoft Corporation © 2022 Maxar ©CNES (2022) Distribution Airbus DS MW-02 MW-06 MW-01 MW-02MW-03 MW-05 MW-04 Sign Vents Shed Speedway Store #8232 Canopy & Dispenser Islands McDonald's N C H i g h w a y 5 5 ( R a l e i g h S t r e e t ) W e s t L i l l i n g t o n S t r e e t Canopy & Dispenser Islands Church Drive-Thru Lane Dumpsters Enclosure Storm Sewer Piping Discharge Point Flowing Water In Ditch Diesel Satellite Dispenser Diesel Dispenser Diesel Dispensers Former Kerosene Dispenser Dispenser (TYP) Dispenser (TYP) 4' O Culvert Culvert Culvert 3' O W e s t D e p o t S t r e e t ParkingAlley & Parking SCALE IN FEET: 40 400 DATE:DRAWN BY:REVIEWED BY:PROJECT NO.:C:\ C o n f i d e n t i a l \ A E C O M \ 7 - E l e v e n \ S i t e s F o l d e r s \ N o r t h C a r o l i n a \ 8 2 3 2 A n g i e r \ 8 2 3 2 A n g i e r . d w g , 12 / 1 4 / 2 0 2 2 9 : 1 0 P M , Du m i t r u , I o n u t , PD F 9 9 5 . p c 3 , Us e r 3 2 7 6 7 , 1'- 0 " = 1 ' - 0 " N I. DUMITRUDECEMBER 2022 E. ANDREWS FIGURE 2 SITE PLAN LEGEND NOTE: ALL MAP FEATURES ARE APPROXIMATE IN SCALE AND LOCATION. Speedway Store #8232 24 South Raleigh Street Angier, North Carolina 60689740 Speedway LLC. Former 6,000-Gal. Diesel UST Approximate Property Boundary Fence Product Dispenser Underground Storage Tank Utility Pole / Power Pole Light Post / Traffic Light Catch Basin / Stormwater Inlet Overhead Wire Monitoring Well Storm Sewer Former Product Dispenser Former Underground Storage Tank Stream 6,000-Gal. Diesel UST (Former Kerosene UST) 6,000-Gal. RUL Gasoline UST 6,000-Gal. PUL Gasoline UST 10,000-Gal. RUL Gasoline UST (Closed In Place on 6/7/2021) MW-02 MW-06 MW-01 MW-02MW-03 MW-05 MW-04 Sign Vents Shed Speedway Store #8232 Canopy & Dispenser Islands McDonald's N C H i g h w a y 5 5 ( R a l e i g h S t r e e t ) W e s t L i l l i n g t o n S t r e e t Canopy & Dispenser Islands Church Drive-Thru Lane Dumpsters Enclosure Storm Sewer Piping Discharge Point Flowing Water In Ditch Diesel Satellite Dispenser Diesel Dispenser Diesel Dispensers Former Kerosene Dispenser Dispenser (TYP) Dispenser (TYP) 4' O Culvert Culvert Culvert 3' O W e s t D e p o t S t r e e t ParkingAlley & Parking SCALE IN FEET: 40 400 DATE:DRAWN BY:REVIEWED BY:PROJECT NO.: C: \ U s e r s \ A l e x a n d r u I o n u t . D u m i t \ A E C O M \ C o n v e n i e n c e S t o r e - 7 - E l e v e n \ N o r t h C a r o l i n a \ 8 2 3 2 A n g i e r \ 8 2 3 2 A n g i e r . d w g , 2/1 6 / 2 0 2 3 4 : 0 1 P M , Du m i t r u , I o n u t , PD F 9 9 5 . p c 3 , Us e r 3 2 7 6 7 , 1'- 0 " = 1 ' - 0 " N I. DUMITRUFEBRUARY 2023 E. ANDREWS FIGURE 3GROUNDWATER ELEVATION MAP NOVEMBER 3, 2022 LEGEND 283.71 Groundwater Elevation (Ft) Inferred Groundwater Elevation Contour (Ft) Approximate Groundwater Flow Direction NOTE: ALL MAP FEATURES ARE APPROXIMATE IN SCALE AND LOCATION. Speedway Store #8232 24 South Raleigh Street Angier, North Carolina 60689740 Speedway LLC. Former 6,000-Gal. Diesel UST 283.8 Approximate Property Boundary Fence Product Dispenser Underground Storage Tank Utility Pole / Power Pole Light Post / Traffic Light Catch Basin / Stormwater Inlet Overhead Wire Monitoring Well Storm Sewer Former Product Dispenser Former Underground Storage Tank Stream 6,000-Gal. Diesel UST (Former Kerosene UST) 6,000-Gal. RUL Gasoline UST 6,000-Gal. PUL Gasoline UST 10,000-Gal. RUL Gasoline UST (Closed In Place on 6/7/2021) 283.8 283 . 8 283.71 283.65 283.63 283.41 283.65 283.99 283.6 283.6 283.4 283.4 MW-02 MW-06 MW-01 MW-02MW-03 MW-05 MW-04 Sign Vents Shed Speedway Store #8232 Canopy & Dispenser Islands McDonald's N C H i g h w a y 5 5 ( R a l e i g h S t r e e t ) W e s t L i l l i n g t o n S t r e e t Canopy & Dispenser Islands Church Drive-Thru Lane Dumpsters Enclosure Storm Sewer Piping Discharge Point Flowing Water In Ditch Diesel Satellite Dispenser Diesel Dispenser Diesel Dispensers Former Kerosene Dispenser Dispenser (TYP) Dispenser (TYP) 4' O Culvert Culvert Culvert 3' O W e s t D e p o t S t r e e t ParkingAlley & Parking Former 6,000-Gal. Diesel UST Approximate Property Boundary Fence Product Dispenser Underground Storage Tank Utility Pole / Power Pole Light Post / Traffic Light Catch Basin / Stormwater Inlet Overhead Wire Monitoring Well Storm Sewer Former Product Dispenser Former Underground Storage Tank Stream 6,000-Gal. Diesel UST (Former Kerosene UST) 6,000-Gal. RUL Gasoline UST 6,000-Gal. PUL Gasoline UST 10,000-Gal. RUL Gasoline UST (Closed In Place on 6/7/2021) SCALE IN FEET: 40 400 DATE:DRAWN BY:REVIEWED BY:PROJECT NO.: C: \ U s e r s \ A l e x a n d r u I o n u t . D u m i t \ A E C O M \ C o n v e n i e n c e S t o r e - 7 - E l e v e n \ N o r t h C a r o l i n a \ 8 2 3 2 A n g i e r \ 8 2 3 2 A n g i e r . d w g , 2/1 6 / 2 0 2 3 4 : 0 0 P M , Du m i t r u , I o n u t , PD F 9 9 5 . p c 3 , Us e r 3 2 7 6 7 , 1'- 0 " = 1 ' - 0 " N I. DUMITRUFEBRUARY 2023 E. ANDREWS LEGEND NOTE: ALL MAP FEATURES ARE APPROXIMATE IN SCALE AND LOCATION. Speedway Store #8232 24 South Raleigh Street Angier, North Carolina 60689740 Speedway LLC.FIGURE 4CONTAMINANTS OF CONCERN CONCENTRATION MAP NOVEMBER 3, 2022 All units in µg/L (Micrograms per Liter) < Less Than The Method Detection BOLD Limit Specified In The Laboratory Concentration Exceeds 2L Standard Maximum Allowable Concentration As Specified In T15A NCAC 2L.0202 TABLE NOTES 2L Report GCL Gross Contamination Level Tables UST ID Number 2,3,4,5 Facility ID Number Incident Number 5285 Date Incident Occurred Date Incident Reported Date Incident Closed Incident Number 8132 Date Incident Occurred Date Incident Reported Date Incident Closed Incident Number 42211 Date Incident Occurred Date Incident Reported Date Incident Closed Incident Number FA-7992 (no incident # assigned)Date Incident Occurred Date Incident Reported Date Incident Closed UST 1 (6,000 gallon diesel) was removed from service June 2021 and closed by insitu foam fill on June 7, 2021 TABLE 1 SITE HISTORY - UST OWNER/OPERATOR AND OTHER RESPONSIBLE PARTY INFORMATION SPEEDWAY #8232 ANGIER, NORTH CAROLINA INCIDENT NO. 42211 0-034026 Name of UST Operator Speedway, LLC Address 500 Speedway Drive, Enon, Ohio 45323 Current UST Owner Address Speedway, LLC Name of UST Owner Dates of Ownership Telephone Number September 2015 to Present 937-864-3000 Dates of Operation September 2015 to Present Telephone Number 500 Speedway Drive, Enon, Ohio 45323 937-864-3000 Other Incidents Onsite or Commingled/In Close Proximity Name of Responsible Party for Other Incident Water was detected in the diesel UST on 12/4/2017. Sludge and diesel fuel were removed and the UST was temporarily taken out of service. The release was reported to NDEQ on 12/5/2017. In addition, the #3 Premium Unleaded Gasoline UST failed a tank tightness test. A UST 17B was submitted to NCDEQ on 9/18/2019. A UST-61 was submitted to NCDEQ on 5/10/2019. Surface diesel release involving diesel dispenser #12; very little to no impact to soil; release was closed out without issuing an incident number. 6/24/1991 12/5/2017 Open Incident 5/7/2019 Name of Responsible Party for Other Incident No Incident Number Assigned Name of Responsible Party for Other Incident 4/24/1989 4/24/1989 4/13/1999 Release of unknown quantity from unknown responsible party suspected after site was leased for retail gas facilities for 20 years. Chevron performed environmental investigation and remedial activities. Site closed when groundwater COCs less than GCLs and soil COCs less than Industrial/Commercial/Residential MSCCs. 12/4/2017 Abandoned Gulf Station (Chevron) - Upgradient 6/24/1991 Name of Responsible Party for Other Incident D.K. Taylor Oil Company/Dennings Angier Exxon Gasoline contaminanted soils were encountered beneath three (3) 6000-gallon gasoline USTs at a former Exxon facility during the June 1991 UST closure. 6/3/1992 UST Capacity (gallons)Date Installed Construction Details Tank Demensions Status Associated with release? 5 10,000 8/1/1994 Single Wall Steel/FRP N/A Current No Incident Number Material Released Date of Release 8132 Unknown 6/24/1991 42211 Unknown 12/4/2017 FA-7992 (no incident # assigned) Diesel 5/7/2019 2 Gasoline (Regular Unleaded) Contents Diesel Diesel Gasoline (Regular Unleaded) Gasoline (Premium Unleaded) Single Wall Steel/FRP 6,000 8/1/1994 6,000 8/1/1994 Single Wall Steel/FRP 6,000 8/1/1994 TABLE 2 SITE HISTORY - UST SYSTEM AND OTHER RELEASE INFORMATION SPEEDWAY #8232 INCIDENT NO. 42211 ANGIER, NORTH CAROLINA No N/A Yes Current Current Current NoN/A N/A N/A Removed 06/07/21 Yes1Single Wall/CLAD/FRP Description of Releases Surface diesel release involving diesel dispenser #12; very little to no impact to soil; release was closed out without issuing an incident number. Soil and groundwater contamination discovered and reported in June 1991 during UST closure; closed out on June 3, 1992. 4 3 6,000 8/1/1994 Single Wall Steel/FRP Water detected in diesel UST; failed tank tightness test in December 2017 on the No. 4 diesel UST due to water intrusion. Sludge and diesel fuel were removed and the UST was temporarily taken out of order; additionally, a failed tightness test was reported on the No. 3 premium unleaded gasoline UST. Well ID Date Installed Date Water Level Measured Well Diameter (Inches) Screened Interval (feet bgs) Total Depth (feet bgs) TOC Elevation (feet msl) Depth to Water from TOC (feet bgs) Non-Aqueous Phase Liquid Thickness (inches) Groundwater Elevation (feet bgs) 11/25/2019 2.95 -- 284.37 7/14/2020 3.40 -- 283.92 2/9/2021 2.39 -- 284.93 3/25/2021 2.74 -- 284.58 3/11/2022 3.34 -- 283.98 11/3/2022 3.61 -- 283.71 7/14/2020 3.95 --- 284.29 2/9/2021 3.07 --- 285.17 3/25/2021 3.35 --- 284.89 3/11/2022 3.93 --- 284.31 11/3/2022 4.25 --- 283.99 7/14/2020 3.26 --- 283.79 2/9/2021 2.29 --- 284.76 3/25/2021 2.65 --- 284.40 3/11/2022 3.23 --- 283.82 11/3/2022 3.42 --- 283.63 3/25/2021 1.60 -- 284.41 3/11/2022 2.19 -- 283.82 11/3/2022 2.36 -- 283.65 2/9/2021 0.98 --- 284.39 3/25/2021 1.17 --- 284.20 3/11/2022 1.82 --- 283.55 11/3/2022 1.96 --- 283.41 3/11/2022 3.60 --- 283.89 11/3/2022 3.84 --- 283.65 Notes: Blue highlight = Recent Data TOC = Top of Casing Historical groundwater elevations dated prior to the November 3, 2022 sampling event from Additional Assessment Report , ATC Associates of North Carolina, Dated April 15, 2022 2-10 10 288.24 2-12 12 287.05 Unknown 9 286.01 MW-06 3/10/2022 16 287.49 285.3715 2-12 2 2 TABLE 3 WELL CONSTRUCTION AND HISTORICAL GROUNDWATER ELEVATION SPEEDWAY #8232 INCIDENT NO. 42211 ANGIER, NORTH CAROLINA Unknown 2 2 2 2 msl= mean sea level bgs = below ground surface --- = non-aqueous phase liquid not present in monitoring well 287.32 MW-05 Unknown 2-12 12MW-01 11/18/2019 MW-02 7/13/2020 MW-03 7/13/2020 MW-04 Unknown 1 600 600 500 NE 6 20 70 70 0.4 70 70 70 70 400 400 47 40 10 70 0.7 3 0.02 15 400 700 200 700 10,000 200 --- 5,000 260,000 80,000 50,000 NE 6,000 20,000 30,500 26,100 400 70,000 5,900 8,800 14,750 28,500 24,100 47,000 40,000 10,000 70,000 700 3,000 50 15,000 NE NE NE NE NE NE --- 11/25/19 426 113 2,590 8,720 11,849 731 < 10 NR NR < 10* < 10 NR NR NR NR NR NR NR NR NR NR NR < 0.01 21.9 < 100,000 < 100,000 < 100,000 302 < 100 331 633 07/14/20 289 <250 1,780 5,330 7,399 <1,250 <250 NR NR <250* <250 NR NR NR NR NR <250 <12,500 <1,250 NR NR NR NR NA NA NA NA NA NA NA NA 02/09/21 431 74 2,950 7,940 11,321 <500 <1.00 136 461 <1.00* <1.00 42.8 16.5 <1.00 3,080 800 <1.00 39.2J <5.00 <1.00 <1.00 <1.00 <1.00 NA NA NA NA NA NA NA NA 11/03/22 99.5 8.8 483 744 1,335.3 191 <2.0 32.9 118 <2.0* <2.0 35.8 <2.0 <2.0 535 99.6 NR NR NR <2.0 <2.0 <2.0 <2.0 NA NA NA NA NA NA NA NA 07/14/20 <1.00 <1.00 <1.00 <3.00 --- <5.00 <1.00 <1.00 <1.00 <1.00* <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <50.0 <5.00 <1.00 <1.00 <1.00 <0.0200 <6.00 <100 <100 <100 <100 <100 <100 <100 02/09/21 <1.00 <1.00 <1.00 <3.00 --- <5.00 <1.00 <1.00 <1.00 <1.00* <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <50.0 <5.00 <1.00 0.826J <1.00 <0.0200 NA NA NA NA NA NA NA NA 11/03/22 0.53 <0.50 <0.50 <1.50 0.53 <2.0 2.2 <0.50 <0.50 <0.50* <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NR NR NR <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA NA 07/14/20 1,320 3,650 1,500 5,070 11,540 591 51.1 104 338 <10.0* 23 <10.0 <10.0 <10.0 1,700 401 <10.0 <500 <50.0 <10.0 <10.0 <10.0 <0.0200 11.3 9,720 9,660 4,140 <100 <100 467B 580 02/09/21 984 1,220 682 1,800 4,686 209 39.3 46.7 140 <1.00* 20.8 14.2 6.73 <1.00 414 90.6 <1.00 89.7 39 <1.00 <1.00 <1.00 <1.00 NA NA NA NA NA NA NA NA 11/03/22 569 12.8 381 300 1,262.8 208 17.3 33.4 94.4 <2.5* 12.3 14.7 <2.5 <2.5 227 23.4 NR NR NR <2.5 <2.5 <2.5 <2.5 NA NA NA NA NA NA NA NA 03/25/21 44.5 0.883J 28 17.8 91.183 106 1.32 8.4 1.5 <1.00* <1.00 1.02 1.45 <1.00 117 1.6 <1.00 21.8J <5.00 2.93 1.65 <1.00 <1.00 NA NA NA NA NA NA NA NA 03/11/22 45.6 0.621J 10 7.99 64.211 135 1.02 6.77 1.0 <1.00* <1.00 0.890J 1.4 0.269J 30.1 0.374J <1.00 <50.0 <5.00 2.38 0.789J 0.893J NA NA NA NA NA NA NA NA NA 11/03/22 41.3 1.7 7 9.70 59.70 212 1.10 4.6 1.9 <1.0* <1.0 <1.0 <1.0 <1.0 21.5 1.1 NR NR NR 1.9 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NA 02/09/21 164 12.40 52.3 146 374.7 76.7 <1.00 24.8 60.5 <1.00* 25.1 3.5 4.01 0.333J 42.8 10.6 <1.00 5.90J <5.00 <1.00 <1.00 <1.00 <1.00 NA NA NA NA NA NA NA NA 11/03/22 308 5.6 36.8 16.4 366.8 139 <1.2 28.7 76.7 <1.2* 46.3 4 2.8 <1.2 <1.2 <1.2 NR NR NR <1.2 <1.2 <1.2 <1.2 NA NA NA NA NA NA NA NA 03/11/22 2,560 34.1 1,290 274 4,158.1 434 901 84.9 256 <1.00* 12.8 33.4 14.7 <1.00 404 76.2 3.63 <50.0 <5.00 2.12 <1.00 <1.00 NA NA NA NA NA NA NA NA NA 11/03/22 1,600 24.1 1,130 121 2,875.1 544 181 75.7 243 <6.2* <6.2 35 <6.2 <6.2 155 49.6 NR NR NR <6.2 <6.2 <6.2 <6.2 NA NA NA NA NA NA NA NA Historical Groundwater Analytical Data dated prior to the November 3rd, 2022 sampling event comes from Additional Assessment Report, ATC Associates of North Carolina, Dated April 15, 2022 Notes: Results reported in micrograms per liter (µg/l). 2L = Maximum Allowable Concentration as specified in T15A NCAC 2L.0202. GCL = Gross Contamination Level < = Less than the method detection limit specified in the laboratory report. Bold = reported concentrations exceed the 2L Standard Bold & Italicized = reported concentrations exceed the GCL Blue highlight = Recent Data J = Estimated value. NE = Not established. NR = Not reported. NA = Not Analyzed Refer to laboratory report for other detectable concentrations which did not exceed the 2L Standard. *Laboratory reporting limits were set above 2L Standard --- = not calculated - BTEX constituents not detected above laboratory reporting limits 1, 2 , 4 - T r i m e t h y l b e n z e n e Chemicals of concern (μg/l) TABLE 4 MW-02 te r t - B u t y l - A l c o h o l (T B A ) ci s - 1 , 2 - D i c h l o r o e t h e n e Te t r a c h l o r o e t h e n e SPEEDWAY #8232 ANGIER, HARNETT COUNTY, NORTH CAROLINA INCIDENT NO. 42211 To t a l B T E X Na p h t h a l e n e Me t h y l t e r t - b u t y l e t h e r (M T B E ) 1,2 D i c h l o r o e t h a n e SUMMARY OF RECENT AND HISTORICAL GROUNDWATER MONITORING RESULTS FOR SELECTED COMPOUNDS MW-05 Et h y l t e r t - b u t y l e t h e r Di - i s o p r o p y l e t h e r (D I P E ) Be n z e n e To l u e n e Et h y l b e n z e n e To t a l X y l e n e s Well ID Date Sampled n- B u t y l b e n z e n e se c - B u t y l b e n z e n e te r t - B u t y l b e n z e n e 1, 3 , 5 - T r i m e t h y l b e n z e n e MW-03 MW-04 Is o p r o p y l b e n z e n e n- P r o p y l b e n z e n e MW-06 Page 1 of 1 Un a d j u s t e d T P H 2L (μg/l) GCL (μg/l) C9 - C 1 8 A l i p h a t i c s C1 9 - C 3 6 A l i p h a t i c s C1 1 - C 2 2 A l i p h a t i c s MW-01 Tr i c h l o r o e t h e n e 1, 2 - D i b r o m o e t h a n e (E D B ) Le a d C5 - C 8 A l i p h a t i c s C9 - C 1 2 A l i p h a t i c s C9 - C 1 0 A r o m a t i c s te r t - A m y l - A l c o h o l (T A A ) Appendix A - Groundwater Analytical Report #=CL# November 11, 2022 LIMS USE: FR - MARIANNE LINK LIMS OBJECT ID: 92635033 92635033 Project: Pace Project No.: RE: Marianne Link AECOM 5438 Wade Park Boulevard Suite 200 Raleigh, NC 27607 SPEEDWAY 8232 60689740 Dear Marianne Link: Enclosed are the analytical results for sample(s) received by the laboratory on November 04, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Bonnie Vang bonnie.vang@pacelabs.com Project Manager (704)875-9092 Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 1 of 23 #=CP# CERTIFICATIONS Pace Project No.: Project: 92635033 SPEEDWAY 8232 60689740 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 23 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92635033 SPEEDWAY 8232 60689740 Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 92635033001 MW-01 SM 6200B 63 PASI-CCL 92635033002 MW-02 SM 6200B 63 PASI-CCL 92635033003 MW-03 SM 6200B 63 PASI-CCL 92635033004 MW-04 SM 6200B 63 PASI-CCL 92635033005 MW-05 SM 6200B 63 PASI-CCL 92635033006 MW-06 SM 6200B 63 PASI-CCL PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 23 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635033 SPEEDWAY 8232 60689740 Sample:MW-01 Lab ID:92635033001 Collected:11/03/22 11:15 Received:11/04/22 15:30 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene 99.5 ug/L 11/11/22 16:07 71-43-22.0 4 Bromobenzene ND ug/L 11/11/22 16:07 108-86-12.0 4 Bromochloromethane ND ug/L 11/11/22 16:07 74-97-52.0 4 Bromodichloromethane ND ug/L 11/11/22 16:07 75-27-42.0 4 Bromoform ND ug/L 11/11/22 16:07 75-25-22.0 4 Bromomethane ND ug/L 11/11/22 16:07 74-83-920.0 4 n-Butylbenzene 35.8 ug/L 11/11/22 16:07 104-51-82.0 4 sec-Butylbenzene ND ug/L 11/11/22 16:07 135-98-82.0 4 tert-Butylbenzene ND ug/L 11/11/22 16:07 98-06-62.0 4 Carbon tetrachloride ND ug/L 11/11/22 16:07 56-23-52.0 4 Chlorobenzene ND ug/L 11/11/22 16:07 108-90-72.0 4 Chloroethane ND ug/L 11/11/22 16:07 75-00-34.0 4 Chloroform ND ug/L 11/11/22 16:07 67-66-32.0 4 Chloromethane ND ug/L 11/11/22 16:07 74-87-34.0 4 2-Chlorotoluene ND ug/L 11/11/22 16:07 95-49-82.0 4 4-Chlorotoluene ND ug/L 11/11/22 16:07 106-43-42.0 4 1,2-Dibromo-3-chloropropane ND ug/L 11/11/22 16:07 96-12-84.0 4 Dibromochloromethane ND ug/L 11/11/22 16:07 124-48-12.0 4 1,2-Dibromoethane (EDB)ND ug/L 11/11/22 16:07 106-93-42.0 4 Dibromomethane ND ug/L 11/11/22 16:07 74-95-32.0 4 1,2-Dichlorobenzene ND ug/L 11/11/22 16:07 95-50-12.0 4 1,3-Dichlorobenzene ND ug/L 11/11/22 16:07 541-73-12.0 4 1,4-Dichlorobenzene ND ug/L 11/11/22 16:07 106-46-72.0 4 Dichlorodifluoromethane ND ug/L 11/11/22 16:07 75-71-82.0 4 1,1-Dichloroethane ND ug/L 11/11/22 16:07 75-34-32.0 4 1,2-Dichloroethane ND ug/L 11/11/22 16:07 107-06-22.0 4 1,1-Dichloroethene ND ug/L 11/11/22 16:07 75-35-42.0 4 cis-1,2-Dichloroethene ND ug/L 11/11/22 16:07 156-59-22.0 4 trans-1,2-Dichloroethene ND ug/L 11/11/22 16:07 156-60-52.0 4 1,2-Dichloropropane ND ug/L 11/11/22 16:07 78-87-52.0 4 1,3-Dichloropropane ND ug/L 11/11/22 16:07 142-28-92.0 4 2,2-Dichloropropane ND ug/L 11/11/22 16:07 594-20-72.0 4 1,1-Dichloropropene ND ug/L 11/11/22 16:07 563-58-62.0 4 cis-1,3-Dichloropropene ND ug/L 11/11/22 16:07 10061-01-52.0 4 trans-1,3-Dichloropropene ND ug/L 11/11/22 16:07 10061-02-62.0 4 Diisopropyl ether ND ug/L 11/11/22 16:07 108-20-32.0 4 Ethylbenzene 483 ug/L 11/11/22 16:07 100-41-42.0 4 Hexachloro-1,3-butadiene ND ug/L 11/11/22 16:07 87-68-38.0 4 Isopropylbenzene (Cumene)32.9 ug/L 11/11/22 16:07 98-82-82.0 4 Methylene Chloride ND ug/L 11/11/22 16:07 75-09-28.0 4 Methyl-tert-butyl ether ND ug/L 11/11/22 16:07 1634-04-42.0 4 Naphthalene 191 ug/L 11/11/22 16:07 91-20-38.0 4 n-Propylbenzene 118 ug/L 11/11/22 16:07 103-65-12.0 4 Styrene ND ug/L 11/11/22 16:07 100-42-52.0 4 1,1,1,2-Tetrachloroethane ND ug/L 11/11/22 16:07 630-20-62.0 4 1,1,2,2-Tetrachloroethane ND ug/L 11/11/22 16:07 79-34-52.0 4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 05:44 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 4 of 23 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635033 SPEEDWAY 8232 60689740 Sample:MW-01 Lab ID:92635033001 Collected:11/03/22 11:15 Received:11/04/22 15:30 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Tetrachloroethene ND ug/L 11/11/22 16:07 127-18-42.0 4 Toluene 8.8 ug/L 11/11/22 16:07 108-88-32.0 4 1,2,3-Trichlorobenzene ND ug/L 11/11/22 16:07 87-61-68.0 4 1,2,4-Trichlorobenzene ND ug/L 11/11/22 16:07 120-82-18.0 4 1,1,1-Trichloroethane ND ug/L 11/11/22 16:07 71-55-62.0 4 1,1,2-Trichloroethane ND ug/L 11/11/22 16:07 79-00-52.0 4 Trichloroethene ND ug/L 11/11/22 16:07 79-01-62.0 4 Trichlorofluoromethane ND ug/L 11/11/22 16:07 75-69-44.0 4 1,2,3-Trichloropropane ND ug/L 11/11/22 16:07 96-18-42.0 4 1,2,4-Trimethylbenzene 535 ug/L 11/11/22 16:07 95-63-62.0 4 1,3,5-Trimethylbenzene 99.6 ug/L 11/11/22 16:07 108-67-82.0 4 Vinyl chloride ND ug/L 11/11/22 16:07 75-01-44.0 4 m&p-Xylene 744 ug/L 11/11/22 16:07 179601-23-14.0 4 o-Xylene ND ug/L 11/11/22 16:07 95-47-62.0 4 Surrogates 1,2-Dichloroethane-d4 (S)96 %11/11/22 16:07 17060-07-070-130 4 4-Bromofluorobenzene (S)95 %11/11/22 16:07 460-00-470-130 4 Toluene-d8 (S)99 %11/11/22 16:07 2037-26-570-130 4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 05:44 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 5 of 23 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635033 SPEEDWAY 8232 60689740 Sample:MW-02 Lab ID:92635033002 Collected:11/03/22 10:10 Received:11/04/22 15:30 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene 0.53 ug/L 11/11/22 14:19 71-43-20.50 1 Bromobenzene ND ug/L 11/11/22 14:19 108-86-10.50 1 Bromochloromethane ND ug/L 11/11/22 14:19 74-97-50.50 1 Bromodichloromethane ND ug/L 11/11/22 14:19 75-27-40.50 1 Bromoform ND ug/L 11/11/22 14:19 75-25-20.50 1 Bromomethane ND ug/L 11/11/22 14:19 74-83-95.0 1 n-Butylbenzene ND ug/L 11/11/22 14:19 104-51-80.50 1 sec-Butylbenzene ND ug/L 11/11/22 14:19 135-98-80.50 1 tert-Butylbenzene ND ug/L 11/11/22 14:19 98-06-60.50 1 Carbon tetrachloride ND ug/L 11/11/22 14:19 56-23-50.50 1 Chlorobenzene ND ug/L 11/11/22 14:19 108-90-70.50 1 Chloroethane ND ug/L 11/11/22 14:19 75-00-31.0 1 Chloroform ND ug/L 11/11/22 14:19 67-66-30.50 1 Chloromethane ND ug/L 11/11/22 14:19 74-87-31.0 1 2-Chlorotoluene ND ug/L 11/11/22 14:19 95-49-80.50 1 4-Chlorotoluene ND ug/L 11/11/22 14:19 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 11/11/22 14:19 96-12-81.0 1 Dibromochloromethane ND ug/L 11/11/22 14:19 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 11/11/22 14:19 106-93-40.50 1 Dibromomethane ND ug/L 11/11/22 14:19 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 11/11/22 14:19 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 11/11/22 14:19 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 11/11/22 14:19 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 11/11/22 14:19 75-71-80.50 1 1,1-Dichloroethane ND ug/L 11/11/22 14:19 75-34-30.50 1 1,2-Dichloroethane ND ug/L 11/11/22 14:19 107-06-20.50 1 1,1-Dichloroethene ND ug/L 11/11/22 14:19 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 11/11/22 14:19 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 11/11/22 14:19 156-60-50.50 1 1,2-Dichloropropane ND ug/L 11/11/22 14:19 78-87-50.50 1 1,3-Dichloropropane ND ug/L 11/11/22 14:19 142-28-90.50 1 2,2-Dichloropropane ND ug/L 11/11/22 14:19 594-20-70.50 1 1,1-Dichloropropene ND ug/L 11/11/22 14:19 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 11/11/22 14:19 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 11/11/22 14:19 10061-02-60.50 1 Diisopropyl ether ND ug/L 11/11/22 14:19 108-20-30.50 1 Ethylbenzene ND ug/L 11/11/22 14:19 100-41-40.50 1 Hexachloro-1,3-butadiene ND ug/L 11/11/22 14:19 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 11/11/22 14:19 98-82-80.50 1 Methylene Chloride ND ug/L 11/11/22 14:19 75-09-22.0 1 Methyl-tert-butyl ether 2.2 ug/L 11/11/22 14:19 1634-04-40.50 1 Naphthalene ND ug/L 11/11/22 14:19 91-20-32.0 1 n-Propylbenzene ND ug/L 11/11/22 14:19 103-65-10.50 1 Styrene ND ug/L 11/11/22 14:19 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 11/11/22 14:19 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 11/11/22 14:19 79-34-50.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 05:44 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 6 of 23 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635033 SPEEDWAY 8232 60689740 Sample:MW-02 Lab ID:92635033002 Collected:11/03/22 10:10 Received:11/04/22 15:30 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Tetrachloroethene ND ug/L 11/11/22 14:19 127-18-40.50 1 Toluene ND ug/L 11/11/22 14:19 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 11/11/22 14:19 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 11/11/22 14:19 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 11/11/22 14:19 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 11/11/22 14:19 79-00-50.50 1 Trichloroethene ND ug/L 11/11/22 14:19 79-01-60.50 1 Trichlorofluoromethane ND ug/L 11/11/22 14:19 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 11/11/22 14:19 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 11/11/22 14:19 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 11/11/22 14:19 108-67-80.50 1 Vinyl chloride ND ug/L 11/11/22 14:19 75-01-41.0 1 m&p-Xylene ND ug/L 11/11/22 14:19 179601-23-11.0 1 o-Xylene ND ug/L 11/11/22 14:19 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)98 %11/11/22 14:19 17060-07-070-130 1 4-Bromofluorobenzene (S)98 %11/11/22 14:19 460-00-470-130 1 Toluene-d8 (S)99 %11/11/22 14:19 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 05:44 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 7 of 23 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635033 SPEEDWAY 8232 60689740 Sample:MW-03 Lab ID:92635033003 Collected:11/03/22 11:55 Received:11/04/22 15:30 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene 569 ug/L 11/11/22 16:26 71-43-22.5 5 Bromobenzene ND ug/L 11/11/22 16:26 108-86-12.5 5 Bromochloromethane ND ug/L 11/11/22 16:26 74-97-52.5 5 Bromodichloromethane ND ug/L 11/11/22 16:26 75-27-42.5 5 Bromoform ND ug/L 11/11/22 16:26 75-25-22.5 5 Bromomethane ND ug/L 11/11/22 16:26 74-83-925.0 5 n-Butylbenzene 14.7 ug/L 11/11/22 16:26 104-51-82.5 5 sec-Butylbenzene ND ug/L 11/11/22 16:26 135-98-82.5 5 tert-Butylbenzene ND ug/L 11/11/22 16:26 98-06-62.5 5 Carbon tetrachloride ND ug/L 11/11/22 16:26 56-23-52.5 5 Chlorobenzene ND ug/L 11/11/22 16:26 108-90-72.5 5 Chloroethane ND ug/L 11/11/22 16:26 75-00-35.0 5 Chloroform ND ug/L 11/11/22 16:26 67-66-32.5 5 Chloromethane ND ug/L 11/11/22 16:26 74-87-35.0 5 2-Chlorotoluene ND ug/L 11/11/22 16:26 95-49-82.5 5 4-Chlorotoluene ND ug/L 11/11/22 16:26 106-43-42.5 5 1,2-Dibromo-3-chloropropane ND ug/L 11/11/22 16:26 96-12-85.0 5 Dibromochloromethane ND ug/L 11/11/22 16:26 124-48-12.5 5 1,2-Dibromoethane (EDB)ND ug/L 11/11/22 16:26 106-93-42.5 5 Dibromomethane ND ug/L 11/11/22 16:26 74-95-32.5 5 1,2-Dichlorobenzene ND ug/L 11/11/22 16:26 95-50-12.5 5 1,3-Dichlorobenzene ND ug/L 11/11/22 16:26 541-73-12.5 5 1,4-Dichlorobenzene ND ug/L 11/11/22 16:26 106-46-72.5 5 Dichlorodifluoromethane ND ug/L 11/11/22 16:26 75-71-82.5 5 1,1-Dichloroethane ND ug/L 11/11/22 16:26 75-34-32.5 5 1,2-Dichloroethane ND ug/L 11/11/22 16:26 107-06-22.5 5 1,1-Dichloroethene ND ug/L 11/11/22 16:26 75-35-42.5 5 cis-1,2-Dichloroethene ND ug/L 11/11/22 16:26 156-59-22.5 5 trans-1,2-Dichloroethene ND ug/L 11/11/22 16:26 156-60-52.5 5 1,2-Dichloropropane ND ug/L 11/11/22 16:26 78-87-52.5 5 1,3-Dichloropropane ND ug/L 11/11/22 16:26 142-28-92.5 5 2,2-Dichloropropane ND ug/L 11/11/22 16:26 594-20-72.5 5 1,1-Dichloropropene ND ug/L 11/11/22 16:26 563-58-62.5 5 cis-1,3-Dichloropropene ND ug/L 11/11/22 16:26 10061-01-52.5 5 trans-1,3-Dichloropropene ND ug/L 11/11/22 16:26 10061-02-62.5 5 Diisopropyl ether 12.3 ug/L 11/11/22 16:26 108-20-32.5 5 Ethylbenzene 381 ug/L 11/11/22 16:26 100-41-42.5 5 Hexachloro-1,3-butadiene ND ug/L 11/11/22 16:26 87-68-310.0 5 Isopropylbenzene (Cumene)33.4 ug/L 11/11/22 16:26 98-82-82.5 5 Methylene Chloride ND ug/L 11/11/22 16:26 75-09-210.0 5 Methyl-tert-butyl ether 17.3 ug/L 11/11/22 16:26 1634-04-42.5 5 Naphthalene 208 ug/L 11/11/22 16:26 91-20-310.0 5 n-Propylbenzene 94.4 ug/L 11/11/22 16:26 103-65-12.5 5 Styrene ND ug/L 11/11/22 16:26 100-42-52.5 5 1,1,1,2-Tetrachloroethane ND ug/L 11/11/22 16:26 630-20-62.5 5 1,1,2,2-Tetrachloroethane ND ug/L 11/11/22 16:26 79-34-52.5 5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 05:44 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 8 of 23 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635033 SPEEDWAY 8232 60689740 Sample:MW-03 Lab ID:92635033003 Collected:11/03/22 11:55 Received:11/04/22 15:30 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Tetrachloroethene ND ug/L 11/11/22 16:26 127-18-42.5 5 Toluene 12.8 ug/L 11/11/22 16:26 108-88-32.5 5 1,2,3-Trichlorobenzene ND ug/L 11/11/22 16:26 87-61-610.0 5 1,2,4-Trichlorobenzene ND ug/L 11/11/22 16:26 120-82-110.0 5 1,1,1-Trichloroethane ND ug/L 11/11/22 16:26 71-55-62.5 5 1,1,2-Trichloroethane ND ug/L 11/11/22 16:26 79-00-52.5 5 Trichloroethene ND ug/L 11/11/22 16:26 79-01-62.5 5 Trichlorofluoromethane ND ug/L 11/11/22 16:26 75-69-45.0 5 1,2,3-Trichloropropane ND ug/L 11/11/22 16:26 96-18-42.5 5 1,2,4-Trimethylbenzene 227 ug/L 11/11/22 16:26 95-63-62.5 5 1,3,5-Trimethylbenzene 23.4 ug/L 11/11/22 16:26 108-67-82.5 5 Vinyl chloride ND ug/L 11/11/22 16:26 75-01-45.0 5 m&p-Xylene 294 ug/L 11/11/22 16:26 179601-23-15.0 5 o-Xylene 6.0 ug/L 11/11/22 16:26 95-47-62.5 5 Surrogates 1,2-Dichloroethane-d4 (S)97 %11/11/22 16:26 17060-07-070-130 5 4-Bromofluorobenzene (S)98 %11/11/22 16:26 460-00-470-130 5 Toluene-d8 (S)98 %11/11/22 16:26 2037-26-570-130 5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 05:44 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 9 of 23 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635033 SPEEDWAY 8232 60689740 Sample:MW-04 Lab ID:92635033004 Collected:11/03/22 12:35 Received:11/04/22 15:30 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene 41.3 ug/L 11/11/22 17:20 71-43-21.0 2 Bromobenzene ND ug/L 11/11/22 17:20 108-86-11.0 2 Bromochloromethane ND ug/L 11/11/22 17:20 74-97-51.0 2 Bromodichloromethane ND ug/L 11/11/22 17:20 75-27-41.0 2 Bromoform ND ug/L 11/11/22 17:20 75-25-21.0 2 Bromomethane ND ug/L 11/11/22 17:20 74-83-910.0 2 n-Butylbenzene ND ug/L 11/11/22 17:20 104-51-81.0 2 sec-Butylbenzene ND ug/L 11/11/22 17:20 135-98-81.0 2 tert-Butylbenzene ND ug/L 11/11/22 17:20 98-06-61.0 2 Carbon tetrachloride ND ug/L 11/11/22 17:20 56-23-51.0 2 Chlorobenzene ND ug/L 11/11/22 17:20 108-90-71.0 2 Chloroethane ND ug/L 11/11/22 17:20 75-00-32.0 2 Chloroform ND ug/L 11/11/22 17:20 67-66-31.0 2 Chloromethane ND ug/L 11/11/22 17:20 74-87-32.0 2 2-Chlorotoluene ND ug/L 11/11/22 17:20 95-49-81.0 2 4-Chlorotoluene ND ug/L 11/11/22 17:20 106-43-41.0 2 1,2-Dibromo-3-chloropropane ND ug/L 11/11/22 17:20 96-12-82.0 2 Dibromochloromethane ND ug/L 11/11/22 17:20 124-48-11.0 2 1,2-Dibromoethane (EDB)ND ug/L 11/11/22 17:20 106-93-41.0 2 Dibromomethane ND ug/L 11/11/22 17:20 74-95-31.0 2 1,2-Dichlorobenzene ND ug/L 11/11/22 17:20 95-50-11.0 2 1,3-Dichlorobenzene ND ug/L 11/11/22 17:20 541-73-11.0 2 1,4-Dichlorobenzene ND ug/L 11/11/22 17:20 106-46-71.0 2 Dichlorodifluoromethane ND ug/L 11/11/22 17:20 75-71-81.0 2 1,1-Dichloroethane ND ug/L 11/11/22 17:20 75-34-31.0 2 1,2-Dichloroethane ND ug/L 11/11/22 17:20 107-06-21.0 2 1,1-Dichloroethene ND ug/L 11/11/22 17:20 75-35-41.0 2 cis-1,2-Dichloroethene 1.9 ug/L 11/11/22 17:20 156-59-21.0 2 trans-1,2-Dichloroethene ND ug/L 11/11/22 17:20 156-60-51.0 2 1,2-Dichloropropane ND ug/L 11/11/22 17:20 78-87-51.0 2 1,3-Dichloropropane ND ug/L 11/11/22 17:20 142-28-91.0 2 2,2-Dichloropropane ND ug/L 11/11/22 17:20 594-20-71.0 2 1,1-Dichloropropene ND ug/L 11/11/22 17:20 563-58-61.0 2 cis-1,3-Dichloropropene ND ug/L 11/11/22 17:20 10061-01-51.0 2 trans-1,3-Dichloropropene ND ug/L 11/11/22 17:20 10061-02-61.0 2 Diisopropyl ether ND ug/L 11/11/22 17:20 108-20-31.0 2 Ethylbenzene 7.0 ug/L 11/11/22 17:20 100-41-41.0 2 Hexachloro-1,3-butadiene ND ug/L 11/11/22 17:20 87-68-34.0 2 Isopropylbenzene (Cumene)4.6 ug/L 11/11/22 17:20 98-82-81.0 2 Methylene Chloride ND ug/L 11/11/22 17:20 75-09-24.0 2 Methyl-tert-butyl ether 1.1 ug/L 11/11/22 17:20 1634-04-41.0 2 Naphthalene 212 ug/L 11/11/22 17:20 91-20-34.0 2 n-Propylbenzene 1.9 ug/L 11/11/22 17:20 103-65-11.0 2 Styrene ND ug/L 11/11/22 17:20 100-42-51.0 2 1,1,1,2-Tetrachloroethane ND ug/L 11/11/22 17:20 630-20-61.0 2 1,1,2,2-Tetrachloroethane ND ug/L 11/11/22 17:20 79-34-51.0 2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 05:44 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 10 of 23 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635033 SPEEDWAY 8232 60689740 Sample:MW-04 Lab ID:92635033004 Collected:11/03/22 12:35 Received:11/04/22 15:30 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Tetrachloroethene ND ug/L 11/11/22 17:20 127-18-41.0 2 Toluene 1.7 ug/L 11/11/22 17:20 108-88-31.0 2 1,2,3-Trichlorobenzene ND ug/L 11/11/22 17:20 87-61-64.0 2 1,2,4-Trichlorobenzene ND ug/L 11/11/22 17:20 120-82-14.0 2 1,1,1-Trichloroethane ND ug/L 11/11/22 17:20 71-55-61.0 2 1,1,2-Trichloroethane ND ug/L 11/11/22 17:20 79-00-51.0 2 Trichloroethene ND ug/L 11/11/22 17:20 79-01-61.0 2 Trichlorofluoromethane ND ug/L 11/11/22 17:20 75-69-42.0 2 1,2,3-Trichloropropane ND ug/L 11/11/22 17:20 96-18-41.0 2 1,2,4-Trimethylbenzene 21.5 ug/L 11/11/22 17:20 95-63-61.0 2 1,3,5-Trimethylbenzene 1.1 ug/L 11/11/22 17:20 108-67-81.0 2 Vinyl chloride ND ug/L 11/11/22 17:20 75-01-42.0 2 m&p-Xylene 7.6 ug/L 11/11/22 17:20 179601-23-12.0 2 o-Xylene 2.1 ug/L 11/11/22 17:20 95-47-61.0 2 Surrogates 1,2-Dichloroethane-d4 (S)97 %11/11/22 17:20 17060-07-070-130 2 4-Bromofluorobenzene (S)98 %11/11/22 17:20 460-00-470-130 2 Toluene-d8 (S)100 %11/11/22 17:20 2037-26-570-130 2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 05:44 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 11 of 23 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635033 SPEEDWAY 8232 60689740 Sample:MW-05 Lab ID:92635033005 Collected:11/03/22 13:10 Received:11/04/22 15:30 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene 308 ug/L 11/11/22 17:02 71-43-21.2 2.5 Bromobenzene ND ug/L 11/11/22 17:02 108-86-11.2 2.5 Bromochloromethane ND ug/L 11/11/22 17:02 74-97-51.2 2.5 Bromodichloromethane ND ug/L 11/11/22 17:02 75-27-41.2 2.5 Bromoform ND ug/L 11/11/22 17:02 75-25-21.2 2.5 Bromomethane ND ug/L 11/11/22 17:02 74-83-912.5 2.5 n-Butylbenzene 4.0 ug/L 11/11/22 17:02 104-51-81.2 2.5 sec-Butylbenzene 2.8 ug/L 11/11/22 17:02 135-98-81.2 2.5 tert-Butylbenzene ND ug/L 11/11/22 17:02 98-06-61.2 2.5 Carbon tetrachloride ND ug/L 11/11/22 17:02 56-23-51.2 2.5 Chlorobenzene ND ug/L 11/11/22 17:02 108-90-71.2 2.5 Chloroethane ND ug/L 11/11/22 17:02 75-00-32.5 2.5 Chloroform ND ug/L 11/11/22 17:02 67-66-31.2 2.5 Chloromethane ND ug/L 11/11/22 17:02 74-87-32.5 2.5 2-Chlorotoluene ND ug/L 11/11/22 17:02 95-49-81.2 2.5 4-Chlorotoluene ND ug/L 11/11/22 17:02 106-43-41.2 2.5 1,2-Dibromo-3-chloropropane ND ug/L 11/11/22 17:02 96-12-82.5 2.5 Dibromochloromethane ND ug/L 11/11/22 17:02 124-48-11.2 2.5 1,2-Dibromoethane (EDB)ND ug/L 11/11/22 17:02 106-93-41.2 2.5 Dibromomethane ND ug/L 11/11/22 17:02 74-95-31.2 2.5 1,2-Dichlorobenzene ND ug/L 11/11/22 17:02 95-50-11.2 2.5 1,3-Dichlorobenzene ND ug/L 11/11/22 17:02 541-73-11.2 2.5 1,4-Dichlorobenzene ND ug/L 11/11/22 17:02 106-46-71.2 2.5 Dichlorodifluoromethane ND ug/L 11/11/22 17:02 75-71-81.2 2.5 1,1-Dichloroethane ND ug/L 11/11/22 17:02 75-34-31.2 2.5 1,2-Dichloroethane ND ug/L 11/11/22 17:02 107-06-21.2 2.5 1,1-Dichloroethene ND ug/L 11/11/22 17:02 75-35-41.2 2.5 cis-1,2-Dichloroethene ND ug/L 11/11/22 17:02 156-59-21.2 2.5 trans-1,2-Dichloroethene ND ug/L 11/11/22 17:02 156-60-51.2 2.5 1,2-Dichloropropane ND ug/L 11/11/22 17:02 78-87-51.2 2.5 1,3-Dichloropropane ND ug/L 11/11/22 17:02 142-28-91.2 2.5 2,2-Dichloropropane ND ug/L 11/11/22 17:02 594-20-71.2 2.5 1,1-Dichloropropene ND ug/L 11/11/22 17:02 563-58-61.2 2.5 cis-1,3-Dichloropropene ND ug/L 11/11/22 17:02 10061-01-51.2 2.5 trans-1,3-Dichloropropene ND ug/L 11/11/22 17:02 10061-02-61.2 2.5 Diisopropyl ether 46.3 ug/L 11/11/22 17:02 108-20-31.2 2.5 Ethylbenzene 36.8 ug/L 11/11/22 17:02 100-41-41.2 2.5 Hexachloro-1,3-butadiene ND ug/L 11/11/22 17:02 87-68-35.0 2.5 Isopropylbenzene (Cumene)28.7 ug/L 11/11/22 17:02 98-82-81.2 2.5 Methylene Chloride ND ug/L 11/11/22 17:02 75-09-25.0 2.5 Methyl-tert-butyl ether ND ug/L 11/11/22 17:02 1634-04-41.2 2.5 Naphthalene 139 ug/L 11/11/22 17:02 91-20-35.0 2.5 n-Propylbenzene 76.7 ug/L 11/11/22 17:02 103-65-11.2 2.5 Styrene ND ug/L 11/11/22 17:02 100-42-51.2 2.5 1,1,1,2-Tetrachloroethane ND ug/L 11/11/22 17:02 630-20-61.2 2.5 1,1,2,2-Tetrachloroethane ND ug/L 11/11/22 17:02 79-34-51.2 2.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 05:44 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 12 of 23 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635033 SPEEDWAY 8232 60689740 Sample:MW-05 Lab ID:92635033005 Collected:11/03/22 13:10 Received:11/04/22 15:30 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Tetrachloroethene ND ug/L 11/11/22 17:02 127-18-41.2 2.5 Toluene 5.6 ug/L 11/11/22 17:02 108-88-31.2 2.5 1,2,3-Trichlorobenzene ND ug/L 11/11/22 17:02 87-61-65.0 2.5 1,2,4-Trichlorobenzene ND ug/L 11/11/22 17:02 120-82-15.0 2.5 1,1,1-Trichloroethane ND ug/L 11/11/22 17:02 71-55-61.2 2.5 1,1,2-Trichloroethane ND ug/L 11/11/22 17:02 79-00-51.2 2.5 Trichloroethene ND ug/L 11/11/22 17:02 79-01-61.2 2.5 Trichlorofluoromethane ND ug/L 11/11/22 17:02 75-69-42.5 2.5 1,2,3-Trichloropropane ND ug/L 11/11/22 17:02 96-18-41.2 2.5 1,2,4-Trimethylbenzene ND ug/L 11/11/22 17:02 95-63-61.2 2.5 1,3,5-Trimethylbenzene ND ug/L 11/11/22 17:02 108-67-81.2 2.5 Vinyl chloride ND ug/L 11/11/22 17:02 75-01-42.5 2.5 m&p-Xylene 15.1 ug/L 11/11/22 17:02 179601-23-12.5 2.5 o-Xylene 1.3 ug/L 11/11/22 17:02 95-47-61.2 2.5 Surrogates 1,2-Dichloroethane-d4 (S)98 %11/11/22 17:02 17060-07-070-130 2.5 4-Bromofluorobenzene (S)98 %11/11/22 17:02 460-00-470-130 2.5 Toluene-d8 (S)99 %11/11/22 17:02 2037-26-570-130 2.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 05:44 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 13 of 23 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635033 SPEEDWAY 8232 60689740 Sample:MW-06 Lab ID:92635033006 Collected:11/03/22 10:45 Received:11/04/22 15:30 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene 1600 ug/L 11/11/22 16:44 71-43-26.2 12.5 Bromobenzene ND ug/L 11/11/22 16:44 108-86-16.2 12.5 Bromochloromethane ND ug/L 11/11/22 16:44 74-97-56.2 12.5 Bromodichloromethane ND ug/L 11/11/22 16:44 75-27-46.2 12.5 Bromoform ND ug/L 11/11/22 16:44 75-25-26.2 12.5 Bromomethane ND ug/L 11/11/22 16:44 74-83-962.5 12.5 n-Butylbenzene 35.0 ug/L 11/11/22 16:44 104-51-86.2 12.5 sec-Butylbenzene ND ug/L 11/11/22 16:44 135-98-86.2 12.5 tert-Butylbenzene ND ug/L 11/11/22 16:44 98-06-66.2 12.5 Carbon tetrachloride ND ug/L 11/11/22 16:44 56-23-56.2 12.5 Chlorobenzene ND ug/L 11/11/22 16:44 108-90-76.2 12.5 Chloroethane ND ug/L 11/11/22 16:44 75-00-312.5 12.5 Chloroform ND ug/L 11/11/22 16:44 67-66-36.2 12.5 Chloromethane ND ug/L 11/11/22 16:44 74-87-312.5 12.5 2-Chlorotoluene ND ug/L 11/11/22 16:44 95-49-86.2 12.5 4-Chlorotoluene ND ug/L 11/11/22 16:44 106-43-46.2 12.5 1,2-Dibromo-3-chloropropane ND ug/L 11/11/22 16:44 96-12-812.5 12.5 Dibromochloromethane ND ug/L 11/11/22 16:44 124-48-16.2 12.5 1,2-Dibromoethane (EDB)ND ug/L 11/11/22 16:44 106-93-46.2 12.5 Dibromomethane ND ug/L 11/11/22 16:44 74-95-36.2 12.5 1,2-Dichlorobenzene ND ug/L 11/11/22 16:44 95-50-16.2 12.5 1,3-Dichlorobenzene ND ug/L 11/11/22 16:44 541-73-16.2 12.5 1,4-Dichlorobenzene ND ug/L 11/11/22 16:44 106-46-76.2 12.5 Dichlorodifluoromethane ND ug/L 11/11/22 16:44 75-71-86.2 12.5 1,1-Dichloroethane ND ug/L 11/11/22 16:44 75-34-36.2 12.5 1,2-Dichloroethane ND ug/L 11/11/22 16:44 107-06-26.2 12.5 1,1-Dichloroethene ND ug/L 11/11/22 16:44 75-35-46.2 12.5 cis-1,2-Dichloroethene ND ug/L 11/11/22 16:44 156-59-26.2 12.5 trans-1,2-Dichloroethene ND ug/L 11/11/22 16:44 156-60-56.2 12.5 1,2-Dichloropropane ND ug/L 11/11/22 16:44 78-87-56.2 12.5 1,3-Dichloropropane ND ug/L 11/11/22 16:44 142-28-96.2 12.5 2,2-Dichloropropane ND ug/L 11/11/22 16:44 594-20-76.2 12.5 1,1-Dichloropropene ND ug/L 11/11/22 16:44 563-58-66.2 12.5 cis-1,3-Dichloropropene ND ug/L 11/11/22 16:44 10061-01-56.2 12.5 trans-1,3-Dichloropropene ND ug/L 11/11/22 16:44 10061-02-66.2 12.5 Diisopropyl ether ND ug/L 11/11/22 16:44 108-20-36.2 12.5 Ethylbenzene 1130 ug/L 11/11/22 16:44 100-41-46.2 12.5 Hexachloro-1,3-butadiene ND ug/L 11/11/22 16:44 87-68-325.0 12.5 Isopropylbenzene (Cumene)75.7 ug/L 11/11/22 16:44 98-82-86.2 12.5 Methylene Chloride ND ug/L 11/11/22 16:44 75-09-225.0 12.5 Methyl-tert-butyl ether 181 ug/L 11/11/22 16:44 1634-04-46.2 12.5 Naphthalene 544 ug/L 11/11/22 16:44 91-20-325.0 12.5 n-Propylbenzene 243 ug/L 11/11/22 16:44 103-65-16.2 12.5 Styrene ND ug/L 11/11/22 16:44 100-42-56.2 12.5 1,1,1,2-Tetrachloroethane ND ug/L 11/11/22 16:44 630-20-66.2 12.5 1,1,2,2-Tetrachloroethane ND ug/L 11/11/22 16:44 79-34-56.2 12.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 05:44 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 14 of 23 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635033 SPEEDWAY 8232 60689740 Sample:MW-06 Lab ID:92635033006 Collected:11/03/22 10:45 Received:11/04/22 15:30 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Tetrachloroethene ND ug/L 11/11/22 16:44 127-18-46.2 12.5 Toluene 24.1 ug/L 11/11/22 16:44 108-88-36.2 12.5 1,2,3-Trichlorobenzene ND ug/L 11/11/22 16:44 87-61-625.0 12.5 1,2,4-Trichlorobenzene ND ug/L 11/11/22 16:44 120-82-125.0 12.5 1,1,1-Trichloroethane ND ug/L 11/11/22 16:44 71-55-66.2 12.5 1,1,2-Trichloroethane ND ug/L 11/11/22 16:44 79-00-56.2 12.5 Trichloroethene ND ug/L 11/11/22 16:44 79-01-66.2 12.5 Trichlorofluoromethane ND ug/L 11/11/22 16:44 75-69-412.5 12.5 1,2,3-Trichloropropane ND ug/L 11/11/22 16:44 96-18-46.2 12.5 1,2,4-Trimethylbenzene 155 ug/L 11/11/22 16:44 95-63-66.2 12.5 1,3,5-Trimethylbenzene 49.6 ug/L 11/11/22 16:44 108-67-86.2 12.5 Vinyl chloride ND ug/L 11/11/22 16:44 75-01-412.5 12.5 m&p-Xylene 114 ug/L 11/11/22 16:44 179601-23-112.5 12.5 o-Xylene 7.0 ug/L 11/11/22 16:44 95-47-66.2 12.5 Surrogates 1,2-Dichloroethane-d4 (S)97 %11/11/22 16:44 17060-07-070-130 12.5 4-Bromofluorobenzene (S)96 %11/11/22 16:44 460-00-470-130 12.5 Toluene-d8 (S)99 %11/11/22 16:44 2037-26-570-130 12.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 05:44 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 15 of 23 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92635033 SPEEDWAY 8232 60689740 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 736499 SM 6200B SM 6200B 6200B MSV Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples:92635033001, 92635033002, 92635033003, 92635033004, 92635033005, 92635033006 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3833116 Associated Lab Samples:92635033001, 92635033002, 92635033003, 92635033004, 92635033005, 92635033006 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/11/22 14:01 1,1,1-Trichloroethane ug/L ND 0.50 11/11/22 14:01 1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/11/22 14:01 1,1,2-Trichloroethane ug/L ND 0.50 11/11/22 14:01 1,1-Dichloroethane ug/L ND 0.50 11/11/22 14:01 1,1-Dichloroethene ug/L ND 0.50 11/11/22 14:01 1,1-Dichloropropene ug/L ND 0.50 11/11/22 14:01 1,2,3-Trichlorobenzene ug/L ND 2.0 11/11/22 14:01 1,2,3-Trichloropropane ug/L ND 0.50 11/11/22 14:01 1,2,4-Trichlorobenzene ug/L ND 2.0 11/11/22 14:01 1,2,4-Trimethylbenzene ug/L ND 0.50 11/11/22 14:01 1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/11/22 14:01 1,2-Dibromoethane (EDB)ug/L ND 0.50 11/11/22 14:01 1,2-Dichlorobenzene ug/L ND 0.50 11/11/22 14:01 1,2-Dichloroethane ug/L ND 0.50 11/11/22 14:01 1,2-Dichloropropane ug/L ND 0.50 11/11/22 14:01 1,3,5-Trimethylbenzene ug/L ND 0.50 11/11/22 14:01 1,3-Dichlorobenzene ug/L ND 0.50 11/11/22 14:01 1,3-Dichloropropane ug/L ND 0.50 11/11/22 14:01 1,4-Dichlorobenzene ug/L ND 0.50 11/11/22 14:01 2,2-Dichloropropane ug/L ND 0.50 11/11/22 14:01 2-Chlorotoluene ug/L ND 0.50 11/11/22 14:01 4-Chlorotoluene ug/L ND 0.50 11/11/22 14:01 Benzene ug/L ND 0.50 11/11/22 14:01 Bromobenzene ug/L ND 0.50 11/11/22 14:01 Bromochloromethane ug/L ND 0.50 11/11/22 14:01 Bromodichloromethane ug/L ND 0.50 11/11/22 14:01 Bromoform ug/L ND 0.50 11/11/22 14:01 Bromomethane ug/L ND 5.0 11/11/22 14:01 Carbon tetrachloride ug/L ND 0.50 11/11/22 14:01 Chlorobenzene ug/L ND 0.50 11/11/22 14:01 Chloroethane ug/L ND 1.0 11/11/22 14:01 Chloroform ug/L ND 0.50 11/11/22 14:01 Chloromethane ug/L ND 1.0 11/11/22 14:01 cis-1,2-Dichloroethene ug/L ND 0.50 11/11/22 14:01 cis-1,3-Dichloropropene ug/L ND 0.50 11/11/22 14:01 Dibromochloromethane ug/L ND 0.50 11/11/22 14:01 Dibromomethane ug/L ND 0.50 11/11/22 14:01 Dichlorodifluoromethane ug/L ND 0.50 11/11/22 14:01 Diisopropyl ether ug/L ND 0.50 11/11/22 14:01 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 05:44 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 16 of 23 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92635033 SPEEDWAY 8232 60689740 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3833116 Associated Lab Samples:92635033001, 92635033002, 92635033003, 92635033004, 92635033005, 92635033006 Matrix:Water Analyzed Ethylbenzene ug/L ND 0.50 11/11/22 14:01 Hexachloro-1,3-butadiene ug/L ND 2.0 11/11/22 14:01 Isopropylbenzene (Cumene)ug/L ND 0.50 11/11/22 14:01 m&p-Xylene ug/L ND 1.0 11/11/22 14:01 Methyl-tert-butyl ether ug/L ND 0.50 11/11/22 14:01 Methylene Chloride ug/L ND 2.0 11/11/22 14:01 n-Butylbenzene ug/L ND 0.50 11/11/22 14:01 n-Propylbenzene ug/L ND 0.50 11/11/22 14:01 Naphthalene ug/L ND 2.0 11/11/22 14:01 o-Xylene ug/L ND 0.50 11/11/22 14:01 sec-Butylbenzene ug/L ND 0.50 11/11/22 14:01 Styrene ug/L ND 0.50 11/11/22 14:01 tert-Butylbenzene ug/L ND 0.50 11/11/22 14:01 Tetrachloroethene ug/L ND 0.50 11/11/22 14:01 Toluene ug/L ND 0.50 11/11/22 14:01 trans-1,2-Dichloroethene ug/L ND 0.50 11/11/22 14:01 trans-1,3-Dichloropropene ug/L ND 0.50 11/11/22 14:01 Trichloroethene ug/L ND 0.50 11/11/22 14:01 Trichlorofluoromethane ug/L ND 1.0 11/11/22 14:01 Vinyl chloride ug/L ND 1.0 11/11/22 14:01 1,2-Dichloroethane-d4 (S)%100 70-130 11/11/22 14:01 4-Bromofluorobenzene (S)%98 70-130 11/11/22 14:01 Toluene-d8 (S)%99 70-130 11/11/22 14:01 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3833117LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 48.450 97 60-140 1,1,1-Trichloroethane ug/L 43.050 86 60-140 1,1,2,2-Tetrachloroethane ug/L 48.050 96 60-140 1,1,2-Trichloroethane ug/L 47.550 95 60-140 1,1-Dichloroethane ug/L 42.250 84 60-140 1,1-Dichloroethene ug/L 43.050 86 60-140 1,1-Dichloropropene ug/L 46.850 94 60-140 1,2,3-Trichlorobenzene ug/L 51.050 102 60-140 1,2,3-Trichloropropane ug/L 49.450 99 60-140 1,2,4-Trichlorobenzene ug/L 46.450 93 60-140 1,2,4-Trimethylbenzene ug/L 44.550 89 60-140 1,2-Dibromo-3-chloropropane ug/L 49.050 98 60-140 1,2-Dibromoethane (EDB)ug/L 49.150 98 60-140 1,2-Dichlorobenzene ug/L 47.150 94 60-140 1,2-Dichloroethane ug/L 43.750 87 60-140 1,2-Dichloropropane ug/L 47.650 95 60-140 1,3,5-Trimethylbenzene ug/L 43.550 87 60-140 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 05:44 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 17 of 23 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92635033 SPEEDWAY 8232 60689740 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3833117LABORATORY CONTROL SAMPLE: LCSSpike 1,3-Dichlorobenzene ug/L 46.750 93 60-140 1,3-Dichloropropane ug/L 47.850 96 60-140 1,4-Dichlorobenzene ug/L 45.050 90 60-140 2,2-Dichloropropane ug/L 36.750 73 60-140 2-Chlorotoluene ug/L 43.250 86 60-140 4-Chlorotoluene ug/L 44.550 89 60-140 Benzene ug/L 43.550 87 60-140 Bromobenzene ug/L 46.150 92 60-140 Bromochloromethane ug/L 43.250 86 60-140 Bromodichloromethane ug/L 44.750 89 60-140 Bromoform ug/L 49.850 100 60-140 Bromomethane ug/L 45.750 91 60-140 Carbon tetrachloride ug/L 44.850 90 60-140 Chlorobenzene ug/L 46.050 92 60-140 Chloroethane ug/L 43.650 87 60-140 Chloroform ug/L 42.350 85 60-140 Chloromethane ug/L 45.350 91 60-140 cis-1,2-Dichloroethene ug/L 43.150 86 60-140 cis-1,3-Dichloropropene ug/L 45.450 91 60-140 Dibromochloromethane ug/L 48.150 96 60-140 Dibromomethane ug/L 48.350 97 60-140 Dichlorodifluoromethane ug/L 45.750 91 60-140 Diisopropyl ether ug/L 44.650 89 60-140 Ethylbenzene ug/L 44.650 89 60-140 Hexachloro-1,3-butadiene ug/L 43.350 87 60-140 Isopropylbenzene (Cumene)ug/L 43.850 88 60-140 m&p-Xylene ug/L 89.0100 89 60-140 Methyl-tert-butyl ether ug/L 47.050 94 60-140 Methylene Chloride ug/L 44.750 89 60-140 n-Butylbenzene ug/L 41.950 84 60-140 n-Propylbenzene ug/L 42.550 85 60-140 Naphthalene ug/L 53.950 108 60-140 o-Xylene ug/L 44.850 90 60-140 sec-Butylbenzene ug/L 43.350 87 60-140 Styrene ug/L 45.950 92 60-140 tert-Butylbenzene ug/L 37.350 75 60-140 Tetrachloroethene ug/L 44.450 89 60-140 Toluene ug/L 43.750 87 60-140 trans-1,2-Dichloroethene ug/L 44.050 88 60-140 trans-1,3-Dichloropropene ug/L 46.050 92 60-140 Trichloroethene ug/L 48.550 97 60-140 Trichlorofluoromethane ug/L 42.450 85 60-140 Vinyl chloride ug/L 47.450 95 60-140 1,2-Dichloroethane-d4 (S)%99 70-130 4-Bromofluorobenzene (S)%100 70-130 Toluene-d8 (S)%98 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 05:44 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 18 of 23 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92635033 SPEEDWAY 8232 60689740 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 3833118MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92635033002 3833119 MSD Result MSD % Rec RPD MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 20 114 60-140104 920ND22.8 20.9 1,1,1-Trichloroethane ug/L 20 118 60-140110 720ND23.5 21.9 1,1,2,2-Tetrachloroethane ug/L 20 110 60-140102 720ND22.0 20.4 1,1,2-Trichloroethane ug/L 20 107 60-140104 320ND21.4 20.9 1,1-Dichloroethane ug/L 20 108 60-140102 620ND21.6 20.4 1,1-Dichloroethene ug/L 20 114 60-140112 220ND22.8 22.4 1,1-Dichloropropene ug/L 20 127 60-140121 520ND25.3 24.1 1,2,3-Trichlorobenzene ug/L 20 107 60-140106 020ND21.3 21.2 1,2,3-Trichloropropane ug/L 20 104 60-14094 1020ND20.8 18.8 1,2,4-Trichlorobenzene ug/L 20 108 60-140101 720ND21.7 20.1 1,2,4-Trimethylbenzene ug/L 20 108 60-140104 520ND21.7 20.7 1,2-Dibromo-3-chloropropane ug/L 20 101 60-14096 520ND20.2 19.2 1,2-Dibromoethane (EDB)ug/L 20 110 60-140104 620ND22.0 20.7 1,2-Dichlorobenzene ug/L 20 106 60-140101 520ND21.3 20.2 1,2-Dichloroethane ug/L 20 107 60-140105 220ND21.5 21.0 1,2-Dichloropropane ug/L 20 108 60-140102 620ND21.7 20.3 1,3,5-Trimethylbenzene ug/L 20 114 60-140108 520ND22.7 21.6 1,3-Dichlorobenzene ug/L 20 106 60-140104 220ND21.1 20.8 1,3-Dichloropropane ug/L 20 107 60-140101 620ND21.4 20.2 1,4-Dichlorobenzene ug/L 20 109 60-140100 820ND21.7 20.1 2,2-Dichloropropane ug/L 20 119 60-140113 520ND23.8 22.7 2-Chlorotoluene ug/L 20 101 60-140104 320ND20.2 20.8 4-Chlorotoluene ug/L 20 101 60-140104 320ND20.2 20.8 Benzene ug/L 20 105 60-14099 6200.53 21.5 20.2 Bromobenzene ug/L 20 106 60-140102 320ND21.1 20.4 Bromochloromethane ug/L 20 112 60-140108 420ND22.5 21.7 Bromodichloromethane ug/L 20 110 60-140105 520ND22.0 21.0 Bromoform ug/L 20 114 60-140107 620ND22.8 21.4 Bromomethane ug/L 20 112 60-140106 520ND22.3 21.2 Carbon tetrachloride ug/L 20 117 60-140111 520ND23.4 22.3 Chlorobenzene ug/L 20 110 60-140102 720ND21.9 20.4 Chloroethane ug/L 20 121 60-140116 420ND24.2 23.2 Chloroform ug/L 20 105 60-140104 220ND21.1 20.8 Chloromethane ug/L 20 125 60-140117 720ND25.1 23.5 cis-1,2-Dichloroethene ug/L 20 111 60-140108 320ND22.2 21.5 cis-1,3-Dichloropropene ug/L 20 112 60-140109 220ND22.3 21.8 Dibromochloromethane ug/L 20 113 60-140103 1020ND22.7 20.5 Dibromomethane ug/L 20 108 60-140102 620ND21.6 20.4 Dichlorodifluoromethane ug/L 20 118 60-140111 720ND23.7 22.1 Diisopropyl ether ug/L 20 104 60-140100 420ND20.8 19.9 Ethylbenzene ug/L 20 112 60-140103 820ND22.4 20.7 Hexachloro-1,3-butadiene ug/L 20 121 60-140116 420ND24.1 23.2 Isopropylbenzene (Cumene)ug/L 20 113 60-140103 1020ND22.6 20.5 m&p-Xylene ug/L 40 114 60-140104 940ND45.5 41.6 Methyl-tert-butyl ether ug/L 20 107 60-140103 3202.2 23.7 22.9 Methylene Chloride ug/L 20 92 60-14089 320ND18.4 17.8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 05:44 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 19 of 23 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92635033 SPEEDWAY 8232 60689740 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 3833118MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92635033002 3833119 MSD Result MSD % Rec RPD MSDMS Spike Conc. n-Butylbenzene ug/L 20 117 60-140109 720ND23.5 21.8 n-Propylbenzene ug/L 20 111 60-140107 420ND22.2 21.3 Naphthalene ug/L 20 102 60-140100 220ND20.5 20.0 o-Xylene ug/L 20 113 60-140106 620ND22.6 21.2 sec-Butylbenzene ug/L 20 113 60-140107 620ND22.6 21.3 Styrene ug/L 20 111 60-140100 1020ND22.2 20.1 tert-Butylbenzene ug/L 20 97 60-14094 320ND19.4 18.8 Tetrachloroethene ug/L 20 118 60-140107 1020ND23.6 21.4 Toluene ug/L 20 106 60-140102 420ND21.2 20.3 trans-1,2-Dichloroethene ug/L 20 114 60-140110 420ND22.8 21.9 trans-1,3-Dichloropropene ug/L 20 112 60-140107 420ND22.3 21.5 Trichloroethene ug/L 20 114 60-140111 220ND22.7 22.2 Trichlorofluoromethane ug/L 20 116 60-140109 620ND23.1 21.8 Vinyl chloride ug/L 20 126 60-140121 420ND25.2 24.1 1,2-Dichloroethane-d4 (S)%100 70-130108 4-Bromofluorobenzene (S)%104 70-130101 Toluene-d8 (S)%98 70-130100 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 05:44 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 20 of 23 #=QL# QUALIFIERS Pace Project No.: Project: 92635033 SPEEDWAY 8232 60689740 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 05:44 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 21 of 23 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92635033 SPEEDWAY 8232 60689740 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92635033001 736499MW-01 SM 6200B 92635033002 736499MW-02 SM 6200B 92635033003 736499MW-03 SM 6200B 92635033004 736499MW-04 SM 6200B 92635033005 736499MW-05 SM 6200B 92635033006 736499MW-06 SM 6200B REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 05:44 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 22 of 23 Page 23 of 23