HomeMy WebLinkAboutFA-7966_42211_CA_MRP_20210305_8132
Speedway LLC
Speedway Office
500 Speedway Drive
Enon, OH 45323
Telephone 937-864-3000
March 5, 2021
Delivered via electronic mail to sarah.brown@ncdenr.gov
Ms, Sarah Brown
North Carolina Department of Environmental Quality
Fayetteville Regional Office
Division of Waste Management - UST Section
225 Green Street #714 Systel Building
FAyetteville, North Carolina 28301
Re: Groundwater Monitoring Report
Speedway No. 8232
24 Raleigh Street
Angier, Harnett County, North Carolina
NCDEQ Incident No. 8132
Dear Ms. Brown:
Speedway LLC (Speedway) is pleased to provide the attached Groundwater Monitoring Report for
the referenced site. The services outlined in this report were performed by our consultant, ATC
Associates of North Carolina, P.C. (ATC), as directed by the North Carolina Department of
Environmental Quality (NCDEQ), based on a review of the Phase II Limited Site Assessment (LSA)
Report received by the NCDEQ on August 13, 2020.
On February 9, 2021, ATC conducted groundwater monitoring activities at the site for monitoring
wells MW-01, MW-02, MW-03, and a monitoring well previously installed by Engineering Consulting
Services, Ltd identified as MW-05.
Laboratory analytical results indicated that concentrations of benzene were detected greater than its
2L Standard in the groundwater samples collected from monitoring wells MW-01, MW-03, and MW-
05. Concentrations of toluene, ethylbenzene, xylenes, naphthalene, MTBE, isopropylbenzene, n-
propylbenzene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, were detected greater than their
respective 2L Standards in the groundwater samples collected from monitoring wells MW-01 and
MW-03. Concentrations of chemicals of concern were not detected above the laboratory reporting
limit in the groundwater sample collected from monitoring well MW-02. No concentrations of
chemicals of concern were detected at or above the North Carolina Gross Contamination Levels
(GCL) for groundwater. There are no water supply wells in the vicinity.
Based on these results, Speedway recommends the site be considered for closure after a Notice of
Residual Petroleum is filed in the Harnett County Registry.
Ms. Sarah Brown
NCDEQ
March 5, 2021
Page 2
If you have any questions or require additional information, please contact me at 919-516-8069 or
by email at cachiara@speedway.com.
Sincerely,
Speedway LLC
Charles A. Chiara
Environmental Representative
Attachment
cc: ATC Associates of North Carolina, P.C., 2725 East Millbrook Road, Suite 121, Raleigh, NC 27604
Groundwater Monitoring Report
Prepared for:
Speedway LLC
March 5, 2021
Speedway No. 8232
24 South Raleigh Street
Angier, Harnett County, North Carolina
NCDEQ Incident No. 43094
NCDEQ Priority Ranking: Intermediate
ATC Project No. SWDP823204
Groundwater Monitoring Report
Speedway No. 8232
March 5, 2021 ATC Associates of North Carolina, PC ii
Document Information
Prepared for Speedway LLC
Project Name Speedway No. 8232
File Reference SW8232_March 2021_GW Monitoring Report
Job Reference SWDP823205
Date March 05, 2020
Contact Information
ATC Group Services LLC
2725 East Millbrook Road, Suite 121
Raleigh, North Carolina 27604
Telephone: 919.871.0999
www.atcgs.com
Document Control
Version Date Author Author
Initials
Reviewer Reviewer
Initials
Draft 02-24-21 D.T. Hurdle DTH Bob Bolton BB
Final 03-05-21 D.T. Hurdle DTH Bob Bolton BB
Donald T. Hurdle, PG Bob Bolton
Project Manager Senior Project Manager
ATC Group Services, LLC ATC Group Services, LLC
Direct Line +1 757.364.6739 Direct Line +1 803.226.0793
Email: donald.hurdle@atcgs.com Email: bob.bolton@atcgs.com
Groundwater Monitoring Report
Speedway No. 8232
March 5, 2021 ATC Associates of North Carolina, PC iii
Site Information
Site Name: Speedway No. 8232
Site Address: 24 South Raleigh Street
Angier, Harnett County, North Carolina
Facility I.D.: 0-034026 UST Incident Number (if known): 42211
Latitude: 35.507025 Longitude: -78.740953
Source: Speedway IDS
UST Owner: Speedway LLC UST Operator: Speedway LLC
Address: 500 Speedway Drive Address: 500 Speedway Drive
Enon, Ohio 45323 Enon, Ohio 45323
Telephone (919) 516-8069 Telephone (919) 516-8069
Property Property
Owner: Williams Family Heirs LLC Occupant: Speedway LLC
Address: & Wilco Hess LLC c/o Property Tax Address: 500 Speedway Drive
539 South Main Street Enon, Ohio 45323
Findlay, Ohio 45840 Telephone (919) 516-8069
Consultant: ATC Associates of North Carolina, P.C.
Address: 2725 East Millbrook Road, Suite 121
Raleigh, North Carolina 27604
Telephone (919) 871-0999
Analytical
Laboratory: Pace Analytical State Certification No. ENV375/DW21704/BI0041
Address: 12065 Lebanon Road,
Mt. Juliet, Tennessee 37122
Telephone (615) 758-5858
Release Information
Date Discovered: December 4, 2017
Estimated Quantity
Of Release: Unknown
Cause of Release: Water intrusion into the now inactive No. 4 6,000-gallon diesel UST
UST Information: One 10,000-gallon regular unleaded gasoline UST, one 6,000-gallon regular unleaded
gasoline UST, one 6,000-gallon premium unleaded gasoline UST, and two 6,000-gallon
diesel USTs, of which one is inactive.
I, Donald T. Hurdle, a Professional Engineer/Licensed Geologist (circle one) for ATC Associates of North Carolina.
P.C., do certify that the information contained in this report is correct and accurate to the best of my knowledge.
ATC Associates of North Carolina. P.C. is licensed to practice geology/engineering (circle one or both) in North
Carolina. The certification number issued by the North Carolina Board for Licensing of Geologists is C-274. The
certification number issued by the North Carolina Board of Examiners for Engineers and Surveyors is C-1598.
Groundwater Monitoring Report
Speedway No. 8232
March 5, 2021 ATC Associates of North Carolina, PC iv
Executive Summary
ATC Associates of North Carolina, P.C. (ATC), on behalf of Speedway LLC (Speedway), conducted additional risk
assessment activities at Speedway Store No. 8232, as directed by the North Carolina Department of
Environmental Quality (NCDEQ) in a Notice of Regulatory Requirement (NORR) letter dated November 25, 2020.
A groundwater sampling event that included monitoring wells MW-01, MW-02, and MW-03, which were previously
installed by ATC, and an additional well (MW-05) installed previously by Engineering Consulting Services, Ltd was
conducted on February 9, 2021. Concentrations of benzene, were detected greater than its 2L Standard in the
groundwater samples collected from monitoring wells MW-01, MW-03, and MW-05. Concentrations of toluene,
ethylbenzene, xylenes, naphthalene, MTBE, isopropylbenzene, n-propylbenzene, 1,2,4-trimethylbenzene, 1,3,5-
trimethylbenzene, were detected greater than their respective 2L Standards in the groundwater samples collected
from monitoring wells MW-01 and MW-03. Concentrations of chemicals of concern were not detected above the
laboratory reporting limit in the groundwater sample collected from monitoring well MW-02. No concentrations of
chemicals of concern were detected at or above the Gross Contamination Levels (GCL) for groundwater.
No water supply wells were identified within 1,500 feet of the site, and the municipal water source is more than
eight miles from the site. An intermittent stream is located approximately 275 feet west of the site.
Based on chemicals of concern in groundwater being detected at concentrations less than their GCLs, and the
lack of water supply wells in the vicinity, ATC recommends the site be considered for closure after a Notice of
Residual Petroleum (NORP) is filed with the County Registrar.
Groundwater Monitoring Report
Speedway No. 8232
March 5, 2021 ATC Associates of North Carolina, PC v
Table of Contents
Site Information iii
Executive Summary iv
1 Introduction 1
1.1 Site Background 1
1.2 Current Activities 2
2 Subsurface Investigation 3
2.1 Site Geology 3
2.2 Groundwater Elevation 3
2.3 Groundwater Sample Collection and Analysis 3
2.4 Groundwater Analytical Results 3
3 Findings and Conclusions 5
4 Recommendations 6
5 Report Limitations 7
6 References 8
Tables
TABLE 1 UST System Information
TABLE 2 Monitoring Well Construction Information
TABLE 3 Summary of Recent and Historical Groundwater Elevation Measurements
TABLE 4 Summary of Groundwater Analytical Results
Figures
FIGURE 1 Site Location Map
FIGURE 2 Site Map
FIGURE 3 Groundwater Elevation Contour Map
FIGURE 4 Chemical of Concern in Groundwater Map
Appendices
APPENDIX A Notice of Regulatory Requirements
APPENDIX B Laboratory Analytical Report for Groundwater
Groundwater Monitoring Report
Speedway No. 8232
March 5, 2021 ATC Associates of North Carolina, PC 1
1 Introduction
Speedway LLC (Speedway) contracted ATC Group Services LLC (ATC) to perform groundwater monitoring
activities at Speedway No. 8232, located at 24 South Raleigh Street, Angier, Harnett County, North Carolina.
Figure 1 shows the location of the site on part of a United States Geological Survey (USGS) topographic map.
The site is currently an active convenience store with retail fuel sales. Figure 2 depicts the site layout including
the location of relevant site features.
1.1 Site Background
On December 4, 2017, non-passing tank tightness test results were received for the No. 4 diesel underground
storage tank (UST) due to water intrusion. On December 5, 2017, Speedway submitted North Carolina Department
of Environmental Quality (NCDEQ) Form UST-61, which documented the tank test results. The No. 4 diesel UST
was emptied of product on December 1, 2017, with the remaining six inches of sludge and liquids removed on
December 4, 2017. On September 18, 2018, Speedway submitted Form UST-17A that documented non-passing
tank tightness test results for the No. 3 premium unleaded gasoline UST due to water intrusion. On September
27, 2018, Speedway submitted Form UST-17B detailing the non-passing tank tests. On September 19, 2018, a
new riser was installed on the No. 3 premium STP and subsequently tested by CROMPCO, LLC. The tank testing
results indicated that the premium UST passed its tank tightness tests.
On May 10, 2019, Speedway submitted Form UST-61 which documented a 20 to 30-gallon diesel spill that
occurred on May 7, 2019. The spill occurred at Satellite Dispenser No. 12 due to a leaking hose/nozzle. At 1440
hours on May 7, 2019, Speedway contacted ATC requesting emergency response activities at the site. ATC
subsequently contacted HEPACO, and both parties were onsite by 1615 hours. Upon arrival, the diesel had
migrated across the pavement into storm drains both west and east of the dispenser island. These storm drains
both emptied into a ditch with flowing water located southwest of the site and behind McDonalds. The diesel also
migrated across the pavement; through the shared drive with McDonalds; and across the front parking lot stopping
just before the storm drain at the curbing. The local fire department had already responded; applied oil dry to the
pavement; added absorbent pads to the two storm drains; and placed absorbent booms at the culverts in the ditch.
HEPACO swept up all the oil dry; placed it in four drums; and left them onsite for future disposal. Since the South
Raleigh Street entrance to McDonalds was closed due to the spill, the oil dry was removed from their property first.
McDonalds was completely reopened by 1800 hours. HEPACO vacuumed any observed sheen off the water in
the ditch at the culvert on the south side of W. Lillington Street, and later at the culvert/stormwater piping discharge
from Speedway on the north side of W. Lillington Street. The absorbent pads from the storm drains were removed
and drummed for disposal. HEPACO vacuumed out both onsite storm drains prior to flushing them with water and
Microblaze. All rinseate was recovered at the stormwater piping discharge point and later transported to Covanta
in Asheboro, North Carolina for proper disposal. Prior to leaving the site, Microblaze was applied to all impacted
pavement, and the absorbent booms at the culvert openings were replaced. Clean up activities ceased at 2100
hours.
On June 5, 2019, ATC conducted site check activities and oversaw Geological Exploration (GEX) utilize direct
hydraulic push technology to conduct a soil boring (identified as SB-01/TW-01) 10 feet below land surface (bls)
near the diesel UST. Soil sample SB01-2 was placed in laboratory-supplied containers, entered into chain-of-
custody control, placed on ice, and shipped via FedEx to Pace National Laboratories (Pace) [12065 Lebanon
Road, Mt. Juliet, Tennessee 37122, North Carolina Laboratory Certification Number ENV375/DW21704/BI0041,
(615) 758-5858] for benzene, toluene, ethylbenzene, total xylenes (BTEX), methyl tert-butyl ether (MTBE),
naphthalene, and di-isopropyl ether (IPE) analysis by Environmental Protection Agency (EPA) Method 8260D;
total petroleum hydrocarbons (TPH) diesel range organics (DRO) by EPA Method 8015D; TPH gasoline range
organics (GRO) analysis by EPA Method 8015D; semi-volatiles analysis by EPA Method 8270E; and petroleum
hydrocarbon analysis by Massachusetts Department of Environmental Protection (MADEP) Extractable Petroleum
Hydrocarbons (EPH) and Volatile Petroleum Hydrocarbons (VPH). Laboratory analytical results indicated
Groundwater Monitoring Report
Speedway No. 8232
March 5, 2021 ATC Associates of North Carolina, PC 2
concentrations of benzene and naphthalene exceeded their respective Soil-to-Groundwater MSCCs. TPH as
DRO was detected in the sample at 14.6 mg/kg.
A groundwater sample from temporary monitoring well TW-01 was collected; placed in laboratory-supplied
containers; entered into chain-of-custody; placed on ice; and shipped via FedEx to Pace for volatile organics
analysis by EPA Method 602; lead analysis by EPA Method 6010D; semi-volatile organics analysis by EPA Method
625; and MADEP EPH/VPH analysis. Laboratory analytical results indicated concentrations of benzene,
ethylbenzene, total xylenes, naphthalene, MTBE, C11-C22 aromatics, C5-C8 aliphatics, C9-C12 aliphatics, and
C11-C22 aliphatics greater than their respective 2L Standards; however, no analytes were detected greater than
their respective GCLs. Based on the results of the site check activities, the NCDEQ issued a NORR requesting
Limited Site Assessment (LSA) activities be conducted.
On November 18, 2019, ATC oversaw GEX install monitoring well MW-01 on the eastern end of the out-of-service
6,000-gallon diesel UST. During the monitoring well installation activities, ATC collected one soil sample from the
borehole. The collected soil sample was placed in laboratory supplied containers, placed on ice, and delivered
under chain of custody via FedEx to Pace Analytical (Pace) [12065 Lebanon Road, Mt. Juliet, Tennessee 37122,
North Carolina Laboratory Certification Number ENV375/DW21704/BI0041, (615) 758-5858] for BTEX, IPE,
MTBE, and naphthalene analysis by EPA Method 8260B; semi-volatiles by EPA Method 625; EPH by MADEP
method; VPH by MADEP method; and TPH DRO and TPH GRO analysis by EPA Method 8015. Based on the
laboratory analytical results of soil samples collected during the LSA activities, soils contained benzene,
ethylbenzene, total xylenes, naphthalene, C5-C8 aliphatics, C9-C10 aromatics, and 1-methylnaphthalene at
concentrations greater than their respective Soil-to-Groundwater MSCCs. Additionally, concentrations of TPH
DRO and GRO were detected greater than their respective NCDEQ action levels. On November 25, 2019, ATC
collected groundwater samples from monitoring well MW-01. Laboratory analytical results indicated
concentrations of benzene, ethylbenzene, total xylenes, naphthalene, C11-C22 aromatics, and lead greater than
their respective NCDEQ 2L Standards in the groundwater collected from monitoring well MW-01. An intermittent
stream was identified approximately 275 feet west of the site and water supply wells were not identified within
1,500 feet of the site. Based on the results of the LSA, the NCDEQ issued a NORR requesting Phase II LSA
activities be conducted.
An LSA II, including the installation of monitoring wells and soil and groundwater sampling and analysis, was
prepared and submitted to the NCDEQ on August 13, 2020. After reviewing the LSA II Report, the NCDEQ issued
a NORR requesting that further assessment take place and that a groundwater sampling report be completed to
further assess contamination and determine further assessment or corrective action.
1.2 Current Activities
On November 25, 2020, the NCDEQ issued a NORR for an additional monitoring event at the site including
sampling monitoring well MW-05, previously installed by Engineering Consulting Services, LTD in the early 1990’s.
Additionally, monitoring wells MW-01, MW-02 and MW-03 were sampled. The NORR associated with these
activities is attached as Appendix A.
Groundwater Monitoring Report
Speedway No. 8232
March 5, 2021 ATC Associates of North Carolina, PC 3
2 Subsurface Investigation
2.1 Site Geology
According to the Geologic Map of North Carolina (1985) produced by Philip Brown, et al, the referenced site is
located within the Inner Coastal Plain Physiographic Region of North Carolina. More specifically, the site is
underlain by the Cretaceous Middendorf Formation. This formation is identified by sand, sandstone, and mudstone
that can contain iron-cemented concretions. Cross-bedding is common and the beds are laterally discontinuous.
Based on observations made during soil boring activities, the residual soil at the site consists mainly of dark brown
to tan sandy silts and silty sands.
2.2 Groundwater Elevation
The top-of-casing of monitoring well MW-05 was surveyed for vertical elevation by ATC on February 9, 2021, and
tied into the existing monitoring well network. The depth to water measured across the site ranged from 0.98 feet
bls to 3.07 feet bls. Groundwater elevations in surveyed monitoring wells were calculated based on the surveyed
top of casing elevations and the measured depths to groundwater. Groundwater elevation data are summarized
in Table 3.
A groundwater elevation contour map (Figure 3) was prepared based on the depth to water data collected on
February 9, 2021. Based on this map, groundwater at the site flows southward.
2.3 Groundwater Sample Collection and Analysis
On February 9, 2021, groundwater samples were collected from monitoring wells MW-01, MW-02, MW-03, and
MW-05. Monitoring well gauging was performed using an oil/water interface probe prior to collection of
groundwater samples. Free phase product was not observed in any of the monitoring wells.
Groundwater samples were collected from the monitoring wells; placed in laboratory-supplied, preserved
containers; entered into chain-of-custody; placed on ice; and shipped via FedEx to Pace Laboratories in Mt Juliet,
TN for analysis of volatile organics by EPA Method 6200B.
2.4 Groundwater Analytical Results
Results for laboratory analysis of the groundwater samples collected from monitoring wells MW-01, MW-02, MW-
03 and MW-05 are summarized in Table 4 and presented in Figure 4. The following summary of findings is based
on the laboratory analysis of the groundwater samples collected on February 9, 2020:
Concentrations of benzene, were detected greater than its 2L Standard in the groundwater samples
collected from monitoring well MW-01, MW-03, and MW-05;
Concentrations of naphthalene were detected greater than its 2L Standard in the groundwater samples
collected from monitoring well MW-03 and MW-05;
Concentrations of ethylbenzene, total xylenes, n-propyl benzene, isopropyl benzene, 1,2,4,
Trimethylbenzene and 1,2,5, Trimethylbenzene were detected greater than their respective 2L Standards
in the groundwater samples collected from monitoring well MW-01 and MW-03;
Concentrations of toluene and MTBE were detected greater than their respective 2L Standards in the
groundwater samples collected from monitoring well MW-03;
No compounds were detected above the laboratory reporting limit in the groundwater samples collected
from monitoring well MW-02; and
None of the compounds were detected at concentrations greater than its North Carolina Gross
Contaminant Level (GCL).
Groundwater Monitoring Report
Speedway No. 8232
March 5, 2021 ATC Associates of North Carolina, PC 4
A copy of the laboratory analytical report and chain-of-custody documentation is included in Appendix B.
Groundwater Monitoring Report
Speedway No. 8232
March 5, 2021 ATC Associates of North Carolina, PC 5
3 Findings and Conclusions
Based on data collected during the recent groundwater monitoring activities, the following conclusions are made:
> On February 9, 2021, four, two-inch diameter monitoring wells (identified as MW-01, MW-02, MW-03 and MW-
05) were sampled at the site;
> Concentrations of benzene, ethylbenzene, total xylenes, 1,2,4-trimethylbenzene, 1,2,5-trimethylbenzene and
isopropyl benzene were detected greater than their respective 2L Standards in the groundwater samples
collected from monitoring well MW-01;
> No compounds were detected above the laboratory reporting limit in the groundwater samples collected from
monitoring well MW-02;
> Concentrations of benzene, toluene, ethylbenzene, total xylenes, naphthalene, MTBE, n-propyl benzene,
isopropyl benzene, and 1,2,4-trimethylbenzene were detected greater than their respective 2L Standards in
the groundwater samples collected from monitoring well MW-03;
> Concentrations of benzene and naphthalene were detected greater than their respective 2L Standards in the
groundwater samples collected from monitoring well MW-05; and
> None of the compounds were detected at concentrations greater than its North Carolina GCL.
Groundwater Monitoring Report
Speedway No. 8232
March 5, 2021 ATC Associates of North Carolina, PC 6
4 Recommendations
Based on chemicals of concern in groundwater being detected at concentrations less than their respective GCLs
and the lack of water supply wells in area, ATC recommends the incident be considered for closure and the filing
of a Notice of Residual Petroleum (NORP) with the Harnett County Registrar.
Groundwater Monitoring Report
Speedway No. 8232
March 5, 2021 ATC Associates of North Carolina, PC 7
5 Report Limitations
This investigation is intended to be a non-biased assessment of on-site environmental conditions proximate to the
location of the former and/or current UST system. Subsurface investigative and remedial methodologies were
performed in general accordance with applicable state and federal regulatory requirements. The information
presented in this report is based upon site-specific observations, generally accepted geological and environmental
consulting practices, and analytical results for environmental samples collected at the time the field investigation
was performed. The data presented in this report are believed to represent subsurface conditions at the facility;
however, data may not be completely representative of subsurface conditions at every location. ATC assumes no
liability arising from environmental impact to, or from, the site, regardless of the date of impact occurrence or
findings.
Groundwater Monitoring Report
Speedway No. 8232
March 5, 2021 ATC Associates of North Carolina, PC 8
6 References
Allyn, E. A., Bolton, B., and Hurdle, D.T., 2020. Phase II Limited Site Assessment Report, Speedway Store
No. 8232, Angier, Harnett County, North Carolina. ATC Group Services, 87 p.
Brown, P.M. and others. 1985. Geologic Map of North Carolina. North Carolina Geological Survey.
https://ncdenr.maps.arcgis.com/apps/MapSeries/index.html?appid=a8281cbd24b84239b29cd2ca798d4a10
Harnett County Department of Public Utilities, Public Utilities. Harnett County, North Carolina.
http://www.harnett.org/utilities/
North Carolina Department of Environment and Natural Resources, now the North Carolina Department of
Environmental Quality. Surface Water Classification.
https://deq.nc.gov/about/divisions/water-resources/planning/classification-standards/classifications
North Carolina Department of Environment and Natural Resources, now the North Carolina Department of
Environmental Quality. NC Surface Water Classifications On-line Mapping Engine.
https://ncdenr.maps.arcgis.com/apps/webappviewer/index.html?id=6e125ad7628f494694e259c80dd64265
North Carolina Department of Environment and Natural Resources, now the North Carolina Department of
Environmental Quality. July 2008. Guidelines for Assessment and Corrective Action.
North Carolina Department of Environment and Natural Resources, now the North Carolina Department of
Environmental Quality. February 2010. North Carolina Aquifers.
North Carolina Department of Environment and Natural Resources, now the North Carolina Department of
Environmental Quality. 2017. Wellhead Protection Areas https://deq.nc.gov/wellhead-protection
United States Department of Agriculture, Soil Conservation Service. Soil Survey of Harnett County, North
Carolina. https://websoilsurvey.sc.egov.usda.gov.
United States Geological Survey (USGS), 7.5-Minute Series, Angier, North Carolina, Topographic
Quadrangle Map, 2016.
Weathers, T., Bolton, B., and Hurdle, D.T., 2019. Limited Site Assessment Report, Speedway Store No.
8232, Angier, Harnett County, North Carolina. ATC Group Services, 170 p.
Groundwater Monitoring Report
Speedway No. 8232
March 5, 2021
Speedway No. 8232
TABLES
UST ID Number 1, 2, 3, 4, 5 Facility ID Number 0-034026
City State Zip Telephone Number
Enon OH 45323 919-516-8069
City State Zip Telephone Number
Enon OH 45323 919-516-8069
TABLE 1
UST OWNER/OPERATOR AND OTHER RESPONSIBLE PARTY INFORMATION
SPEEDWAY NO. 8232
24 SOUTH RALEIGH STREET
ANGIER, HARNETT COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO. 42211
ATC GROUP SERVICES OF NORTH CAROLINA, P.C. PROJECT NO. SWDP823206
Name of Operator Dates of Operation (MM/DD/YY to MM/DD/YY)
Speedway LLC 09-29-2015 to Current
Street Address
500 Speedway Drive
Name of Owner Dates of Operation
Speedway LLC 09-29-2015 to Current
Street Address
500 Speedway Drive
MW-01 11/18/19 2 0.01 2-12 12 Active
MW-02 07/13/20 2 0.01 2-10 10 Active
MW-03 07/13/20 2 0.01 2-12 12 Active
MW-05 unknown 2 unknown unknown 8.44 Active
NCDEQ INCIDENT NO. 42211
TABLE 2
MONITORING WELL CONSTRUCTION INFORMATION
SPEEDWAY NO. 8232
24 SOUTH RALEIGH STREET
ANGIER, HARNETT COUNTY, NORTH CAROLINA
ATC GROUP SERVICES OF NORTH CAROLINA, P.C. PROJECT NO. SWDP823206
Well ID Date
Installed
Well
Diamenter
(inches)
Screen
Slot Size
(inches)
Screened
interval
(feet)
Total
Depth
(feet)
Status
WELL
I.D. Date
TOC
Elevation
(feet)
Well Depth
(feet)
Depth to
Product
(feet)
Depth to
Groundwater
(feet)
Product
Thickness
(feet)
Groundwater
Elevation
(feet)
11/25/19 287.37 12 -2.95 -284.42
07/14/20 287.37 12 -3.40 -283.97
02/09/21 287.37 12 -2.39 -284.98
07/14/20 288.35 10 -3.95 -284.40
02/09/21 288.35 10 -3.07 -285.28
07/14/20 287.10 12 -3.26 -283.84
02/09/21 287.10 12 -2.29 -284.81
MW-05 02/09/21 285.51 8.44 -0.98 -284.53
Notes:
1. TOC = Top of well casing
MW-02
MW-03
MW-01
TABLE 3
SUMMARY OF RECENT AND HISTORICAL GROUNDWATER ELEVATION MEASUREMENTS
NCDEQ INCIDENT NO. 42211
ANGIER, HARNETT COUNTY, NORTH CAROLINA
24 SOUTH RALEIGH STREET
SPEEDWAY NO. 8232
ATC GROUP SERVICES OF NORTH CAROLINA, P.C. PROJECT NO. SWDP823206
EPA
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1 600 600 500 ---6 20 0.4 70 70 70 400 400 0.02 15 400 700 200 700 10,000 200 ---
5,000 260,000 84,500 85,500 ---6,000 20,000 400 70,000 25,000 30,000 28,500 25,000 50 15,000 NE NE NE NE NE NE ---
11/25/19 426 113 2,590 8,720 11,849 731 < 10 < 10 < 10 NA NA NA NA < 0.01 21.9 < 100,000 < 100,000 < 100,000 302 < 100 331 633
07/14/20 289 <250 1,780 5,330 7,399 <1,250 <250 <250 <250 NA NA NA NA NA NA NA NA NA NA NA NA NA
02/09/21 431 74 2,950 7,940 11,321 <500 <1.00 <1.00 <1.00 136 461 3,080 800 <1.00 NA NA NA NA NA NA NA NA
07/14/20 <1.00 <1.00 <1.00 <3.00 ---<5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <0.0200 <6.00 <100 <100 <100 <100 <100 <100 <100
02/09/21 <1.00 <1.00 <1.00 <3.00 ---<5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <0.0200 NA NA NA NA NA NA NA NA
07/14/20 1,320 3,650 1,500 5,070 11,540 591 51.1 <10.0 23.0 104 338 1,700 401 <0.0200 11.3 9,720 9,660 4,140 <100 <100 467 B 580
02/09/21 984 1,220 682 1,800 4,686 209 39.3 <1.00 20.8 46.7 140 414 90.6 <1.00 NA NA NA NA NA NA NA NA
MW-05 02/09/21 164 12.4 52.3 146 375 76.7 <1.00 <1.00 25.1 24.8 60.5 42.8 10.6 <1.00 NA NA NA NA NA NA NA NA
Notes:
1. Laboratory results concentrations reported in micrograms per liter (µg/L).
2. 2L Standard limits reported in micrograms per liter (µg/L).
3. Italics type denotes concentration equals or exceeds - 2L Standard
4. BOLD/Underline denotes concentration equals or exceeds Gross Contaminant Level (GCL).
5. "<" denotes compound not detected above laboratory method detection limit.
6. J value denotes estimated concentration by the laboratory.
7. NE = Not Established.
8. B = The same analyte found in the associated blank.
9. NA = Not Analyzed.
MW-02
MW-03
MW-01
2L Standard (µg/L)
GCL (µg/L)
TABLE 4
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
SPEEDWAY NO. 8232
24 SOUTH RALEIGH STREET
ANGIER, HARNETT COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO. 42211
ATC GROUP SERVICES OF NORTH CAROLINA, P.C. PROJECT NO. SWDP823206
MADEP Method for VPH MADEP Method for EPH
GW
Sample ID
Sampling
Date
EPA Method 6200B
Groundwater Monitoring Report
Speedway No. 8232
March 5, 2021
Speedway No. 8232
FIGURES
TITLE FIGURE 1 FACILITY ID No. 0-034026
SITE VICINITY MAP
SPEEDWAY No. 8232
24 SOUTH RALEIGH STREET
ANGIER, NORTH CAROLINA 27052
SITE LOCATION
PREP. BY
E. SHELTON
REV. BY
D. HURDLE
SCALE
1" = 2000'
DATE
12-12-2019
PROJECT NO.
SWDP823206
0 2000'4000'
SCALE IN FEET
N
EW
S
2725 East Millbrook, Suite 121
Raleigh, North Carolina 27604
Phone (919) 871-0999 Fax (704) 583-2744
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Groundwater Monitoring Report
Speedway No. 8232
March 5, 2021
Speedway No. 8232
APPENDIX A
NORR
Fayetteville Regional Office | 225 Green Street | Suite 714 | Systel Building | Fayetteville, NC 28301 | (910) 433-3300
November 25, 2020
Email only
Charles Chiara Speedway LLC. 3200 Spring Forest Road, STE 206
Raleigh, NC 27616 Subject: LSA Phase II Report Review Speedway No. 8232 24 South Raleigh Street Angier Harnett County Incident Number: 8132 Risk Classification: Intermediate Ranking: I 115 D Dear Mr. Chiara:
On August 13, 2020, the Division of Waste Management (DWM) received a Phase II Limited Site Assessment (LSA) Report, prepared on your behalf by ATC. The report summarizes soil and groundwater assessment activities conducted at the subject site. The DWM has reviewed and approved the report.
After review of this report, the DWM requests additional risk assessment which should include:
•The installation of one additional horizontal extent monitoring well between the source and thesurface water. If intact, monitoring well MW-5 (installed in 1993) may be used in place of a newwell.
•The collection of groundwater samples from all monitoring wells, analyzed by the appropriatemethod(s) for the constituents relevant to the release.
•The survey of the new monitoring well or monitoring well MW-5 and collection of potentiometricdata for the completion of a potentiometric surface / groundwater elevation and flow map.
The additional risk assessment work should be summarized in a monitoring report. The report should be received by this office no later than February 25, 2021.
Because a release or discharge has been confirmed, a Licensed Geologist or a Professional Engineer,
certified by the State of North Carolina, is required to prepare and certify all reports submitted to the
Department in accordance with 15A NCAC 2L .0103(e) and 2L .0111(b).
Please note that before you sell, transfer, or request a “No Further Action” determination for a property that has not been remediated to below “unrestricted use” standards, you must file a Notice of Residual
State of North Carolina | Environmental Quality | Waste Management
Petroleum ("Notice") with the Register of Deeds in the county where the property is located (NCGS 143B-279.9 and 143B-279.11).
If you have any questions regarding trust fund eligibility or reimbursement from the Commercial Leaking Petroleum Underground Storage Tank Cleanup Fund, please contact the UST Section Trust Fund Branch at (919) 707-8171. If you have any questions regarding the actions that must be taken or the rules mentioned in this letter, please contact Sarah Brown at the address or telephone number listed below.
Sincerely,
Sarah Brown Environmental Specialist II Fayetteville Regional Office
UST Section, Division of Waste Management, NCDEQ
cc: Oliver Tolksdorf Harnett County Environmental Health 307 W Cornelius Harnett Boulevard Lillington, NC 27546 Liz Allyn – ATC (email only)
Fayetteville Regional Office | 225 Green St | #714 Systel Building | Fayetteville, NC 28301 | (910) 433-3300
Groundwater Monitoring Report
Speedway No. 8232
March 5, 2021
Speedway No. 8232
APPENDIX B
LABORATORY ANALYSIS REPORT
GROUNDWATER
ANALYTICAL REPORT
February 24, 2021
Revised Report
ATC Group Services - NC Speedway
Sample Delivery Group:L1315684
Samples Received:02/10/2021
Project Number:SWDP793303
Description:Speedway 8232
Site:0008232 0-034026
Report To:Bob Bolton / Donald Hurdle
7606 Whitehall Executive Ctr Ste 800
Charlotte, NC 28273
Entire Report Reviewed By:
February 24, 2021
[Preliminary Report]
John Hawkins
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Speedway SWDP793303 L1315684 02/24/21 11:56 1 of 30
February 25, 2021
John Hawkins
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Speedway SWDP793303 L1315684 02/25/21 11:42 1 of 30
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
MW-1 L1315684-01 5
MW-2 L1315684-02 7
MW-3 L1315684-03 9
MW-5 L1315684-04 11
Qc: Quality Control Summary 13
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 13
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 23
Gl: Glossary of Terms 26
Al: Accreditations & Locations 27
Sc: Sample Chain of Custody 28
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-1 L1315684-01 GW Brian Buchanon 02/09/21 11:15 02/10/21 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 WG1619889 1 02/12/21 02:51 02/12/21 02:51 JHH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1619446 100 02/10/21 19:56 02/10/21 19:56 JHH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1621611 100 02/18/21 13:38 02/18/21 13:38 JHH Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-2 L1315684-02 GW Brian Buchanon 02/09/21 10:55 02/10/21 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 WG1619889 1 02/12/21 03:11 02/12/21 03:11 JHH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1619446 1 02/10/21 19:36 02/10/21 19:36 JHH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1621611 1 02/18/21 13:17 02/18/21 13:17 JHH Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-3 L1315684-03 GW Brian Buchanon 02/09/21 11:35 02/10/21 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 WG1619889 1 02/12/21 03:31 02/12/21 03:31 JHH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1619446 10 02/10/21 20:17 02/10/21 20:17 JHH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1621611 10 02/18/21 13:58 02/18/21 13:58 JHH Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-5 L1315684-04 GW Brian Buchanon 02/09/21 12:15 02/10/21 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 WG1621124 1 02/13/21 15:26 02/13/21 15:26 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1622526 1 02/22/21 17:08 02/22/21 17:08 BMB Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
John Hawkins
Report Revision History
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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John Hawkins
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1315684
MW-1
Collected date/time: 02/09/21 11:15
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 11.3 50.0 1 02/12/2021 02:51 WG1619889
Acrolein U J4 2.54 50.0 1 02/12/2021 02:51 WG1619889
Acrylonitrile U 0.671 10.0 1 02/12/2021 02:51 WG1619889
Benzene 431 9.41 100 100 02/10/2021 19:56 WG1619446
Bromobenzene U 0.118 1.00 1 02/12/2021 02:51 WG1619889
Bromodichloromethane U 0.136 1.00 1 02/12/2021 02:51 WG1619889
Bromoform U 0.129 1.00 1 02/12/2021 02:51 WG1619889
Bromomethane U 0.605 5.00 1 02/12/2021 02:51 WG1619889
n-Butylbenzene 42.8 0.157 1.00 1 02/12/2021 02:51 WG1619889
sec-Butylbenzene 16.5 0.125 1.00 1 02/12/2021 02:51 WG1619889
tert-Butylbenzene U 0.127 1.00 1 02/12/2021 02:51 WG1619889
Carbon tetrachloride U 0.128 1.00 1 02/12/2021 02:51 WG1619889
Chlorobenzene U 0.116 1.00 1 02/12/2021 02:51 WG1619889
Chlorodibromomethane U 0.140 1.00 1 02/12/2021 02:51 WG1619889
Chloroethane U 0.192 5.00 1 02/12/2021 02:51 WG1619889
Chloroform U 0.111 5.00 1 02/12/2021 02:51 WG1619889
Chloromethane U 0.960 2.50 1 02/12/2021 02:51 WG1619889
2-Chlorotoluene U 0.106 1.00 1 02/12/2021 02:51 WG1619889
4-Chlorotoluene U 0.114 1.00 1 02/12/2021 02:51 WG1619889
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 02/12/2021 02:51 WG1619889
1,2-Dibromoethane U 0.126 1.00 1 02/12/2021 02:51 WG1619889
Dibromomethane U 0.122 1.00 1 02/12/2021 02:51 WG1619889
1,2-Dichlorobenzene U 0.107 1.00 1 02/12/2021 02:51 WG1619889
1,3-Dichlorobenzene U 0.110 1.00 1 02/12/2021 02:51 WG1619889
1,4-Dichlorobenzene U 0.120 1.00 1 02/12/2021 02:51 WG1619889
Dichlorodifluoromethane U 0.374 5.00 1 02/12/2021 02:51 WG1619889
1,1-Dichloroethane U 0.100 1.00 1 02/12/2021 02:51 WG1619889
1,2-Dichloroethane U 0.0819 1.00 1 02/12/2021 02:51 WG1619889
1,1-Dichloroethene U 0.188 1.00 1 02/12/2021 02:51 WG1619889
cis-1,2-Dichloroethene U 0.126 1.00 1 02/12/2021 02:51 WG1619889
trans-1,2-Dichloroethene U 0.149 1.00 1 02/12/2021 02:51 WG1619889
1,2-Dichloropropane U 0.149 1.00 1 02/12/2021 02:51 WG1619889
1,1-Dichloropropene U 0.142 1.00 1 02/12/2021 02:51 WG1619889
1,3-Dichloropropane U 0.110 1.00 1 02/12/2021 02:51 WG1619889
2,2-Dichloropropane U 0.161 1.00 1 02/12/2021 02:51 WG1619889
Di-isopropyl ether U 0.105 1.00 1 02/12/2021 02:51 WG1619889
Ethylbenzene 2950 13.7 100 100 02/10/2021 19:56 WG1619446
Hexachloro-1,3-butadiene U 0.337 1.00 1 02/12/2021 02:51 WG1619889
Isopropylbenzene 136 0.105 1.00 1 02/12/2021 02:51 WG1619889
p-Isopropyltoluene 48.7 0.120 1.00 1 02/12/2021 02:51 WG1619889
2-Butanone (MEK)U 1.19 10.0 1 02/12/2021 02:51 WG1619889
Methylene Chloride U 0.430 5.00 1 02/12/2021 02:51 WG1619889
4-Methyl-2-pentanone (MIBK)U 0.478 10.0 1 02/12/2021 02:51 WG1619889
Methyl tert-butyl ether U 0.101 1.00 1 02/12/2021 02:51 WG1619889
Naphthalene 396 J 100 500 100 02/18/2021 13:38 WG1621611
n-Propylbenzene 461 9.93 100 100 02/10/2021 19:56 WG1619446
Styrene U 0.118 1.00 1 02/12/2021 02:51 WG1619889
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 02/12/2021 02:51 WG1619889
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 02/12/2021 02:51 WG1619889
Tetrachloroethene U 0.300 1.00 1 02/12/2021 02:51 WG1619889
Toluene 74.0 0.278 1.00 1 02/12/2021 02:51 WG1619889
1,2,3-Trichlorobenzene U 0.230 1.00 1 02/12/2021 02:51 WG1619889
1,2,4-Trichlorobenzene U 0.481 1.00 1 02/12/2021 02:51 WG1619889
1,1,1-Trichloroethane U 0.149 1.00 1 02/12/2021 02:51 WG1619889
1,1,2-Trichloroethane U 0.158 1.00 1 02/12/2021 02:51 WG1619889
Trichloroethene U 0.190 1.00 1 02/12/2021 02:51 WG1619889
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Speedway SWDP793303 L1315684 02/25/21 11:42 5 of 30
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1315684
MW-1
Collected date/time: 02/09/21 11:15
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Trichlorofluoromethane U 0.160 5.00 1 02/12/2021 02:51 WG1619889
1,2,3-Trichloropropane U 0.237 2.50 1 02/12/2021 02:51 WG1619889
1,2,4-Trimethylbenzene 3080 32.2 100 100 02/10/2021 19:56 WG1619446
1,3,5-Trimethylbenzene 800 J4 10.4 100 100 02/10/2021 19:56 WG1619446
Vinyl chloride U 0.234 1.00 1 02/12/2021 02:51 WG1619889
o-Xylene 54.1 J 17.4 100 100 02/10/2021 19:56 WG1619446
m&p-Xylenes 7890 43.0 200 100 02/10/2021 19:56 WG1619446
Xylenes, Total 7940 17.4 300 100 02/10/2021 19:56 WG1619446
ethanol U 42.0 100 1 02/12/2021 02:51 WG1619889
3,3-Dimethyl-1-butanol U 4.51 100 1 02/12/2021 02:51 WG1619889
Ethyl tert-butyl ether U 0.101 1.00 1 02/12/2021 02:51 WG1619889
t-Amyl Alcohol 39.2 J 4.90 50.0 1 02/12/2021 02:51 WG1619889
tert-Butyl alcohol U 4.06 5.00 1 02/12/2021 02:51 WG1619889
tert-Butyl Formate U 4.51 20.0 1 02/12/2021 02:51 WG1619889
tert-Amyl Methyl Ether U 0.195 1.00 1 02/12/2021 02:51 WG1619889
(S) Toluene-d8 113 80.0-120 02/10/2021 19:56 WG1619446
(S) Toluene-d8 106 80.0-120 02/12/2021 02:51 WG1619889
(S) Toluene-d8 104 80.0-120 02/18/2021 13:38 WG1621611
(S) 4-Bromofluorobenzene 94.6 77.0-126 02/10/2021 19:56 WG1619446
(S) 4-Bromofluorobenzene 117 77.0-126 02/12/2021 02:51 WG1619889
(S) 4-Bromofluorobenzene 101 77.0-126 02/18/2021 13:38 WG1621611
(S) 1,2-Dichloroethane-d4 110 70.0-130 02/10/2021 19:56 WG1619446
(S) 1,2-Dichloroethane-d4 126 70.0-130 02/12/2021 02:51 WG1619889
(S) 1,2-Dichloroethane-d4 112 70.0-130 02/18/2021 13:38 WG1621611
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Speedway SWDP793303 L1315684 02/24/21 11:56 6 of 30
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Speedway SWDP793303 L1315684 02/25/21 11:42 6 of 30
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1315684
MW-2
Collected date/time: 02/09/21 10:55
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 11.3 50.0 1 02/12/2021 03:11 WG1619889
Acrolein U J4 2.54 50.0 1 02/12/2021 03:11 WG1619889
Acrylonitrile U 0.671 10.0 1 02/12/2021 03:11 WG1619889
Benzene 0.388 J 0.0941 1.00 1 02/10/2021 19:36 WG1619446
Bromobenzene U 0.118 1.00 1 02/12/2021 03:11 WG1619889
Bromodichloromethane U 0.136 1.00 1 02/12/2021 03:11 WG1619889
Bromoform U 0.129 1.00 1 02/12/2021 03:11 WG1619889
Bromomethane U 0.605 5.00 1 02/12/2021 03:11 WG1619889
n-Butylbenzene U 0.157 1.00 1 02/10/2021 19:36 WG1619446
sec-Butylbenzene U 0.125 1.00 1 02/10/2021 19:36 WG1619446
tert-Butylbenzene U 0.127 1.00 1 02/12/2021 03:11 WG1619889
Carbon tetrachloride U 0.128 1.00 1 02/12/2021 03:11 WG1619889
Chlorobenzene U 0.116 1.00 1 02/12/2021 03:11 WG1619889
Chlorodibromomethane U 0.140 1.00 1 02/12/2021 03:11 WG1619889
Chloroethane U 0.192 5.00 1 02/12/2021 03:11 WG1619889
Chloroform U 0.111 5.00 1 02/12/2021 03:11 WG1619889
Chloromethane U 0.960 2.50 1 02/12/2021 03:11 WG1619889
2-Chlorotoluene U 0.106 1.00 1 02/12/2021 03:11 WG1619889
4-Chlorotoluene U 0.114 1.00 1 02/12/2021 03:11 WG1619889
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 02/12/2021 03:11 WG1619889
1,2-Dibromoethane U 0.126 1.00 1 02/12/2021 03:11 WG1619889
Dibromomethane U 0.122 1.00 1 02/12/2021 03:11 WG1619889
1,2-Dichlorobenzene U 0.107 1.00 1 02/12/2021 03:11 WG1619889
1,3-Dichlorobenzene U 0.110 1.00 1 02/12/2021 03:11 WG1619889
1,4-Dichlorobenzene U 0.120 1.00 1 02/12/2021 03:11 WG1619889
Dichlorodifluoromethane U 0.374 5.00 1 02/12/2021 03:11 WG1619889
1,1-Dichloroethane U 0.100 1.00 1 02/12/2021 03:11 WG1619889
1,2-Dichloroethane U 0.0819 1.00 1 02/12/2021 03:11 WG1619889
1,1-Dichloroethene U 0.188 1.00 1 02/12/2021 03:11 WG1619889
cis-1,2-Dichloroethene U 0.126 1.00 1 02/12/2021 03:11 WG1619889
trans-1,2-Dichloroethene U 0.149 1.00 1 02/12/2021 03:11 WG1619889
1,2-Dichloropropane U 0.149 1.00 1 02/12/2021 03:11 WG1619889
1,1-Dichloropropene U 0.142 1.00 1 02/12/2021 03:11 WG1619889
1,3-Dichloropropane U 0.110 1.00 1 02/12/2021 03:11 WG1619889
2,2-Dichloropropane U 0.161 1.00 1 02/12/2021 03:11 WG1619889
Di-isopropyl ether U 0.105 1.00 1 02/12/2021 03:11 WG1619889
Ethylbenzene U 0.137 1.00 1 02/10/2021 19:36 WG1619446
Hexachloro-1,3-butadiene U 0.337 1.00 1 02/12/2021 03:11 WG1619889
Isopropylbenzene U 0.105 1.00 1 02/10/2021 19:36 WG1619446
p-Isopropyltoluene U 0.120 1.00 1 02/10/2021 19:36 WG1619446
2-Butanone (MEK)U 1.19 10.0 1 02/12/2021 03:11 WG1619889
Methylene Chloride U 0.430 5.00 1 02/12/2021 03:11 WG1619889
4-Methyl-2-pentanone (MIBK)U 0.478 10.0 1 02/12/2021 03:11 WG1619889
Methyl tert-butyl ether U 0.101 1.00 1 02/12/2021 03:11 WG1619889
Naphthalene U 1.00 5.00 1 02/18/2021 13:17 WG1621611
n-Propylbenzene U 0.0993 1.00 1 02/10/2021 19:36 WG1619446
Styrene U 0.118 1.00 1 02/12/2021 03:11 WG1619889
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 02/12/2021 03:11 WG1619889
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 02/12/2021 03:11 WG1619889
Tetrachloroethene 0.826 J 0.300 1.00 1 02/12/2021 03:11 WG1619889
Toluene U 0.278 1.00 1 02/12/2021 03:11 WG1619889
1,2,3-Trichlorobenzene U 0.230 1.00 1 02/12/2021 03:11 WG1619889
1,2,4-Trichlorobenzene U 0.481 1.00 1 02/12/2021 03:11 WG1619889
1,1,1-Trichloroethane U 0.149 1.00 1 02/12/2021 03:11 WG1619889
1,1,2-Trichloroethane U 0.158 1.00 1 02/12/2021 03:11 WG1619889
Trichloroethene U 0.190 1.00 1 02/12/2021 03:11 WG1619889
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Speedway SWDP793303 L1315684 02/24/21 11:56 7 of 30
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Speedway SWDP793303 L1315684 02/25/21 11:42 7 of 30
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1315684
MW-2
Collected date/time: 02/09/21 10:55
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Trichlorofluoromethane U 0.160 5.00 1 02/12/2021 03:11 WG1619889
1,2,3-Trichloropropane U 0.237 2.50 1 02/12/2021 03:11 WG1619889
1,2,4-Trimethylbenzene U 0.322 1.00 1 02/10/2021 19:36 WG1619446
1,3,5-Trimethylbenzene U J4 0.104 1.00 1 02/10/2021 19:36 WG1619446
Vinyl chloride U 0.234 1.00 1 02/12/2021 03:11 WG1619889
o-Xylene U 0.174 1.00 1 02/10/2021 19:36 WG1619446
m&p-Xylenes U 0.430 2.00 1 02/10/2021 19:36 WG1619446
Xylenes, Total U 0.174 3.00 1 02/10/2021 19:36 WG1619446
ethanol U 42.0 100 1 02/12/2021 03:11 WG1619889
3,3-Dimethyl-1-butanol U 4.51 100 1 02/12/2021 03:11 WG1619889
Ethyl tert-butyl ether U 0.101 1.00 1 02/12/2021 03:11 WG1619889
t-Amyl Alcohol U 4.90 50.0 1 02/12/2021 03:11 WG1619889
tert-Butyl alcohol U 4.06 5.00 1 02/12/2021 03:11 WG1619889
tert-Butyl Formate U 4.51 20.0 1 02/12/2021 03:11 WG1619889
tert-Amyl Methyl Ether U 0.195 1.00 1 02/12/2021 03:11 WG1619889
(S) Toluene-d8 115 80.0-120 02/10/2021 19:36 WG1619446
(S) Toluene-d8 102 80.0-120 02/12/2021 03:11 WG1619889
(S) Toluene-d8 105 80.0-120 02/18/2021 13:17 WG1621611
(S) 4-Bromofluorobenzene 96.1 77.0-126 02/10/2021 19:36 WG1619446
(S) 4-Bromofluorobenzene 98.9 77.0-126 02/12/2021 03:11 WG1619889
(S) 4-Bromofluorobenzene 100 77.0-126 02/18/2021 13:17 WG1621611
(S) 1,2-Dichloroethane-d4 110 70.0-130 02/10/2021 19:36 WG1619446
(S) 1,2-Dichloroethane-d4 101 70.0-130 02/12/2021 03:11 WG1619889
(S) 1,2-Dichloroethane-d4 108 70.0-130 02/18/2021 13:17 WG1621611
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Speedway SWDP793303 L1315684 02/24/21 11:56 8 of 30
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Speedway SWDP793303 L1315684 02/25/21 11:42 8 of 30
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1315684
MW-3
Collected date/time: 02/09/21 11:35
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 11.3 50.0 1 02/12/2021 03:31 WG1619889
Acrolein U J4 2.54 50.0 1 02/12/2021 03:31 WG1619889
Acrylonitrile U 0.671 10.0 1 02/12/2021 03:31 WG1619889
Benzene 984 0.941 10.0 10 02/10/2021 20:17 WG1619446
Bromobenzene U 0.118 1.00 1 02/12/2021 03:31 WG1619889
Bromodichloromethane U 0.136 1.00 1 02/12/2021 03:31 WG1619889
Bromoform U 0.129 1.00 1 02/12/2021 03:31 WG1619889
Bromomethane U 0.605 5.00 1 02/12/2021 03:31 WG1619889
n-Butylbenzene 14.2 0.157 1.00 1 02/12/2021 03:31 WG1619889
sec-Butylbenzene 6.73 0.125 1.00 1 02/12/2021 03:31 WG1619889
tert-Butylbenzene U 0.127 1.00 1 02/12/2021 03:31 WG1619889
Carbon tetrachloride U 0.128 1.00 1 02/12/2021 03:31 WG1619889
Chlorobenzene U 0.116 1.00 1 02/12/2021 03:31 WG1619889
Chlorodibromomethane U 0.140 1.00 1 02/12/2021 03:31 WG1619889
Chloroethane U 0.192 5.00 1 02/12/2021 03:31 WG1619889
Chloroform U 0.111 5.00 1 02/12/2021 03:31 WG1619889
Chloromethane U 0.960 2.50 1 02/12/2021 03:31 WG1619889
2-Chlorotoluene U 0.106 1.00 1 02/12/2021 03:31 WG1619889
4-Chlorotoluene U 0.114 1.00 1 02/12/2021 03:31 WG1619889
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 02/12/2021 03:31 WG1619889
1,2-Dibromoethane U 0.126 1.00 1 02/12/2021 03:31 WG1619889
Dibromomethane U 0.122 1.00 1 02/12/2021 03:31 WG1619889
1,2-Dichlorobenzene U 0.107 1.00 1 02/12/2021 03:31 WG1619889
1,3-Dichlorobenzene U 0.110 1.00 1 02/12/2021 03:31 WG1619889
1,4-Dichlorobenzene U 0.120 1.00 1 02/12/2021 03:31 WG1619889
Dichlorodifluoromethane U 0.374 5.00 1 02/12/2021 03:31 WG1619889
1,1-Dichloroethane U 0.100 1.00 1 02/12/2021 03:31 WG1619889
1,2-Dichloroethane U 0.0819 1.00 1 02/12/2021 03:31 WG1619889
1,1-Dichloroethene U 0.188 1.00 1 02/12/2021 03:31 WG1619889
cis-1,2-Dichloroethene U 0.126 1.00 1 02/12/2021 03:31 WG1619889
trans-1,2-Dichloroethene U 0.149 1.00 1 02/12/2021 03:31 WG1619889
1,2-Dichloropropane U 0.149 1.00 1 02/12/2021 03:31 WG1619889
1,1-Dichloropropene U 0.142 1.00 1 02/12/2021 03:31 WG1619889
1,3-Dichloropropane U 0.110 1.00 1 02/12/2021 03:31 WG1619889
2,2-Dichloropropane U 0.161 1.00 1 02/12/2021 03:31 WG1619889
Di-isopropyl ether 20.8 0.105 1.00 1 02/12/2021 03:31 WG1619889
Ethylbenzene 682 1.37 10.0 10 02/10/2021 20:17 WG1619446
Hexachloro-1,3-butadiene U 0.337 1.00 1 02/12/2021 03:31 WG1619889
Isopropylbenzene 46.7 0.105 1.00 1 02/12/2021 03:31 WG1619889
p-Isopropyltoluene 2.91 0.120 1.00 1 02/12/2021 03:31 WG1619889
2-Butanone (MEK)U 1.19 10.0 1 02/12/2021 03:31 WG1619889
Methylene Chloride U 0.430 5.00 1 02/12/2021 03:31 WG1619889
4-Methyl-2-pentanone (MIBK)U 0.478 10.0 1 02/12/2021 03:31 WG1619889
Methyl tert-butyl ether 39.3 0.101 1.00 1 02/12/2021 03:31 WG1619889
Naphthalene 209 10.0 50.0 10 02/18/2021 13:58 WG1621611
n-Propylbenzene 140 0.0993 1.00 1 02/12/2021 03:31 WG1619889
Styrene U 0.118 1.00 1 02/12/2021 03:31 WG1619889
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 02/12/2021 03:31 WG1619889
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 02/12/2021 03:31 WG1619889
Tetrachloroethene U 0.300 1.00 1 02/12/2021 03:31 WG1619889
Toluene 1220 2.78 10.0 10 02/10/2021 20:17 WG1619446
1,2,3-Trichlorobenzene U 0.230 1.00 1 02/12/2021 03:31 WG1619889
1,2,4-Trichlorobenzene U 0.481 1.00 1 02/12/2021 03:31 WG1619889
1,1,1-Trichloroethane U 0.149 1.00 1 02/12/2021 03:31 WG1619889
1,1,2-Trichloroethane U 0.158 1.00 1 02/12/2021 03:31 WG1619889
Trichloroethene U 0.190 1.00 1 02/12/2021 03:31 WG1619889
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Speedway SWDP793303 L1315684 02/24/21 11:56 9 of 30
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Speedway SWDP793303 L1315684 02/25/21 11:42 9 of 30
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1315684
MW-3
Collected date/time: 02/09/21 11:35
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Trichlorofluoromethane U 0.160 5.00 1 02/12/2021 03:31 WG1619889
1,2,3-Trichloropropane U 0.237 2.50 1 02/12/2021 03:31 WG1619889
1,2,4-Trimethylbenzene 414 3.22 10.0 10 02/10/2021 20:17 WG1619446
1,3,5-Trimethylbenzene 90.6 0.104 1.00 1 02/12/2021 03:31 WG1619889
Vinyl chloride 1.73 0.234 1.00 1 02/12/2021 03:31 WG1619889
o-Xylene 441 1.74 10.0 10 02/10/2021 20:17 WG1619446
m&p-Xylenes 1360 4.30 20.0 10 02/10/2021 20:17 WG1619446
Xylenes, Total 1800 1.74 30.0 10 02/10/2021 20:17 WG1619446
ethanol U 42.0 100 1 02/12/2021 03:31 WG1619889
3,3-Dimethyl-1-butanol U 4.51 100 1 02/12/2021 03:31 WG1619889
Ethyl tert-butyl ether U 0.101 1.00 1 02/12/2021 03:31 WG1619889
t-Amyl Alcohol 89.7 4.90 50.0 1 02/12/2021 03:31 WG1619889
tert-Butyl alcohol 39.0 4.06 5.00 1 02/12/2021 03:31 WG1619889
tert-Butyl Formate U 4.51 20.0 1 02/12/2021 03:31 WG1619889
tert-Amyl Methyl Ether U 0.195 1.00 1 02/12/2021 03:31 WG1619889
(S) Toluene-d8 112 80.0-120 02/10/2021 20:17 WG1619446
(S) Toluene-d8 99.4 80.0-120 02/12/2021 03:31 WG1619889
(S) Toluene-d8 105 80.0-120 02/18/2021 13:58 WG1621611
(S) 4-Bromofluorobenzene 97.5 77.0-126 02/10/2021 20:17 WG1619446
(S) 4-Bromofluorobenzene 99.4 77.0-126 02/12/2021 03:31 WG1619889
(S) 4-Bromofluorobenzene 103 77.0-126 02/18/2021 13:58 WG1621611
(S) 1,2-Dichloroethane-d4 109 70.0-130 02/10/2021 20:17 WG1619446
(S) 1,2-Dichloroethane-d4 109 70.0-130 02/12/2021 03:31 WG1619889
(S) 1,2-Dichloroethane-d4 110 70.0-130 02/18/2021 13:58 WG1621611
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Speedway SWDP793303 L1315684 02/24/21 11:56 10 of 30
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Speedway SWDP793303 L1315684 02/25/21 11:42 10 of 30
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L1315684
MW-5
Collected date/time: 02/09/21 12:15
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 11.3 50.0 1 02/22/2021 17:08 WG1622526
Acrolein U 2.54 50.0 1 02/22/2021 17:08 WG1622526
Acrylonitrile U 0.671 10.0 1 02/13/2021 15:26 WG1621124
Benzene 164 0.0941 1.00 1 02/13/2021 15:26 WG1621124
Bromobenzene U 0.118 1.00 1 02/13/2021 15:26 WG1621124
Bromodichloromethane U 0.136 1.00 1 02/13/2021 15:26 WG1621124
Bromoform U 0.129 1.00 1 02/13/2021 15:26 WG1621124
Bromomethane U 0.605 5.00 1 02/13/2021 15:26 WG1621124
n-Butylbenzene 3.53 0.157 1.00 1 02/22/2021 17:08 WG1622526
sec-Butylbenzene 4.01 0.125 1.00 1 02/13/2021 15:26 WG1621124
tert-Butylbenzene 0.333 J 0.127 1.00 1 02/13/2021 15:26 WG1621124
Carbon tetrachloride U 0.128 1.00 1 02/13/2021 15:26 WG1621124
Chlorobenzene U 0.116 1.00 1 02/13/2021 15:26 WG1621124
Chlorodibromomethane U 0.140 1.00 1 02/13/2021 15:26 WG1621124
Chloroethane U 0.192 5.00 1 02/13/2021 15:26 WG1621124
Chloroform U 0.111 5.00 1 02/13/2021 15:26 WG1621124
Chloromethane U 0.960 2.50 1 02/13/2021 15:26 WG1621124
2-Chlorotoluene U 0.106 1.00 1 02/13/2021 15:26 WG1621124
4-Chlorotoluene U 0.114 1.00 1 02/13/2021 15:26 WG1621124
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 02/13/2021 15:26 WG1621124
1,2-Dibromoethane U 0.126 1.00 1 02/13/2021 15:26 WG1621124
Dibromomethane U 0.122 1.00 1 02/13/2021 15:26 WG1621124
1,2-Dichlorobenzene U 0.107 1.00 1 02/13/2021 15:26 WG1621124
1,3-Dichlorobenzene U 0.110 1.00 1 02/13/2021 15:26 WG1621124
1,4-Dichlorobenzene U 0.120 1.00 1 02/13/2021 15:26 WG1621124
Dichlorodifluoromethane U 0.374 5.00 1 02/13/2021 15:26 WG1621124
1,1-Dichloroethane U 0.100 1.00 1 02/13/2021 15:26 WG1621124
1,2-Dichloroethane U 0.0819 1.00 1 02/13/2021 15:26 WG1621124
1,1-Dichloroethene U 0.188 1.00 1 02/13/2021 15:26 WG1621124
cis-1,2-Dichloroethene U 0.126 1.00 1 02/13/2021 15:26 WG1621124
trans-1,2-Dichloroethene U 0.149 1.00 1 02/13/2021 15:26 WG1621124
1,2-Dichloropropane U 0.149 1.00 1 02/13/2021 15:26 WG1621124
1,1-Dichloropropene U 0.142 1.00 1 02/13/2021 15:26 WG1621124
1,3-Dichloropropane U 0.110 1.00 1 02/13/2021 15:26 WG1621124
2,2-Dichloropropane U 0.161 1.00 1 02/13/2021 15:26 WG1621124
Di-isopropyl ether 25.1 0.105 1.00 1 02/13/2021 15:26 WG1621124
Ethylbenzene 52.3 0.137 1.00 1 02/13/2021 15:26 WG1621124
Hexachloro-1,3-butadiene U 0.337 1.00 1 02/13/2021 15:26 WG1621124
Isopropylbenzene 24.8 0.105 1.00 1 02/13/2021 15:26 WG1621124
p-Isopropyltoluene 1.53 0.120 1.00 1 02/13/2021 15:26 WG1621124
2-Butanone (MEK)U 1.19 10.0 1 02/22/2021 17:08 WG1622526
Methylene Chloride U 0.430 5.00 1 02/13/2021 15:26 WG1621124
4-Methyl-2-pentanone (MIBK)U 0.478 10.0 1 02/13/2021 15:26 WG1621124
Methyl tert-butyl ether U 0.101 1.00 1 02/13/2021 15:26 WG1621124
Naphthalene 76.7 1.00 5.00 1 02/13/2021 15:26 WG1621124
n-Propylbenzene 60.5 0.0993 1.00 1 02/13/2021 15:26 WG1621124
Styrene U 0.118 1.00 1 02/13/2021 15:26 WG1621124
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 02/13/2021 15:26 WG1621124
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 02/13/2021 15:26 WG1621124
Tetrachloroethene U 0.300 1.00 1 02/13/2021 15:26 WG1621124
Toluene 12.4 0.278 1.00 1 02/13/2021 15:26 WG1621124
1,2,3-Trichlorobenzene U 0.230 1.00 1 02/13/2021 15:26 WG1621124
1,2,4-Trichlorobenzene U 0.481 1.00 1 02/13/2021 15:26 WG1621124
1,1,1-Trichloroethane U 0.149 1.00 1 02/13/2021 15:26 WG1621124
1,1,2-Trichloroethane U 0.158 1.00 1 02/13/2021 15:26 WG1621124
Trichloroethene U 0.190 1.00 1 02/13/2021 15:26 WG1621124
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L1315684
MW-5
Collected date/time: 02/09/21 12:15
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Trichlorofluoromethane U 0.160 5.00 1 02/13/2021 15:26 WG1621124
1,2,3-Trichloropropane U 0.237 2.50 1 02/13/2021 15:26 WG1621124
1,2,4-Trimethylbenzene 42.8 0.322 1.00 1 02/13/2021 15:26 WG1621124
1,3,5-Trimethylbenzene 10.6 0.104 1.00 1 02/13/2021 15:26 WG1621124
Vinyl chloride U 0.234 1.00 1 02/13/2021 15:26 WG1621124
o-Xylene 47.9 0.174 1.00 1 02/13/2021 15:26 WG1621124
m&p-Xylenes 98.5 0.430 2.00 1 02/13/2021 15:26 WG1621124
Xylenes, Total 146 0.174 3.00 1 02/13/2021 15:26 WG1621124
ethanol U 42.0 100 1 02/22/2021 17:08 WG1622526
3,3-Dimethyl-1-butanol U 4.51 100 1 02/13/2021 15:26 WG1621124
Ethyl tert-butyl ether U 0.101 1.00 1 02/13/2021 15:26 WG1621124
t-Amyl Alcohol 5.90 J 4.90 50.0 1 02/13/2021 15:26 WG1621124
tert-Butyl alcohol U 4.06 5.00 1 02/13/2021 15:26 WG1621124
tert-Butyl Formate U 4.51 20.0 1 02/13/2021 15:26 WG1621124
tert-Amyl Methyl Ether U 0.195 1.00 1 02/13/2021 15:26 WG1621124
(S) Toluene-d8 101 80.0-120 02/13/2021 15:26 WG1621124
(S) Toluene-d8 94.3 80.0-120 02/22/2021 17:08 WG1622526
(S) 4-Bromofluorobenzene 97.0 77.0-126 02/13/2021 15:26 WG1621124
(S) 4-Bromofluorobenzene 116 77.0-126 02/22/2021 17:08 WG1622526
(S) 1,2-Dichloroethane-d4 88.4 70.0-130 02/13/2021 15:26 WG1621124
(S) 1,2-Dichloroethane-d4 95.1 70.0-130 02/22/2021 17:08 WG1622526
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1619889
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1315684-01,02,03
Method Blank (MB)
(MB) R3622550-3 02/11/21 22:52
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acetone U 11.3 50.0
Acrolein U 2.54 50.0
Acrylonitrile U 0.671 10.0
Bromobenzene U 0.118 1.00
Bromodichloromethane U 0.136 1.00
Bromoform U 0.129 1.00
Bromomethane U 0.605 5.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
2,2-Dichloropropane U 0.161 1.00
Di-isopropyl ether U 0.105 1.00
Ethanol U 42.0 100
Hexachloro-1,3-butadiene U 0.337 1.00
Isopropylbenzene U 0.105 1.00
p-Isopropyltoluene U 0.120 1.00
2-Butanone (MEK)U 1.19 10.0
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1619889
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1315684-01,02,03
Method Blank (MB)
(MB) R3622550-3 02/11/21 22:52
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Methylene Chloride U 0.430 5.00
4-Methyl-2-pentanone (MIBK)U 0.478 10.0
Methyl tert-butyl ether U 0.101 1.00
n-Propylbenzene U 0.0993 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Trichlorofluoromethane U 0.160 5.00
1,2,3-Trichloropropane U 0.237 2.50
1,3,5-Trimethylbenzene U 0.104 1.00
Vinyl chloride U 0.234 1.00
tert-Amyl Methyl Ether U 0.195 1.00
Ethyl tert-butyl ether U 0.101 1.00
tert-Butyl alcohol U 4.06 5.00
3,3-Dimethyl-1-butanol U 4.51 100
t-Amyl Alcohol U 4.90 50.0
tert-Butyl formate U 4.51 20.0
(S) Toluene-d8 103 80.0-120
(S) 4-Bromofluorobenzene 97.2 77.0-126
(S) 1,2-Dichloroethane-d4 103 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3622550-1 02/11/21 21:51
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acetone 25.0 30.7 123 19.0-160
Acrolein 25.0 40.5 162 10.0-160 J4
Acrylonitrile 25.0 30.9 124 55.0-149
Bromobenzene 5.00 5.18 104 73.0-121
Bromodichloromethane 5.00 5.26 105 75.0-120
Bromoform 5.00 5.40 108 68.0-132
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ATC Group Services - NC Speedway SWDP793303 L1315684 02/25/21 11:42 14 of 30
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1619889
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1315684-01,02,03
Laboratory Control Sample (LCS)
(LCS) R3622550-1 02/11/21 21:51
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Bromomethane 5.00 5.03 101 10.0-160
n-Butylbenzene 5.00 5.42 108 73.0-125
sec-Butylbenzene 5.00 5.40 108 75.0-125
tert-Butylbenzene 5.00 5.23 105 76.0-124
Carbon tetrachloride 5.00 5.92 118 68.0-126
Chlorobenzene 5.00 5.10 102 80.0-121
Chlorodibromomethane 5.00 5.35 107 77.0-125
Chloroethane 5.00 6.12 122 47.0-150
Chloroform 5.00 5.35 107 73.0-120
Chloromethane 5.00 6.79 136 41.0-142
2-Chlorotoluene 5.00 5.69 114 76.0-123
4-Chlorotoluene 5.00 5.20 104 75.0-122
1,2-Dibromo-3-Chloropropane 5.00 4.70 94.0 58.0-134
1,2-Dibromoethane 5.00 5.05 101 80.0-122
Dibromomethane 5.00 5.43 109 80.0-120
1,2-Dichlorobenzene 5.00 5.13 103 79.0-121
1,3-Dichlorobenzene 5.00 5.19 104 79.0-120
1,4-Dichlorobenzene 5.00 5.37 107 79.0-120
Dichlorodifluoromethane 5.00 6.88 138 51.0-149
1,1-Dichloroethane 5.00 5.53 111 70.0-126
1,2-Dichloroethane 5.00 5.50 110 70.0-128
1,1-Dichloroethene 5.00 5.56 111 71.0-124
cis-1,2-Dichloroethene 5.00 5.03 101 73.0-120
trans-1,2-Dichloroethene 5.00 5.17 103 73.0-120
1,2-Dichloropropane 5.00 5.54 111 77.0-125
1,1-Dichloropropene 5.00 5.85 117 74.0-126
1,3-Dichloropropane 5.00 5.59 112 80.0-120
2,2-Dichloropropane 5.00 6.27 125 58.0-130
Di-isopropyl ether 5.00 5.67 113 58.0-138
Hexachloro-1,3-butadiene 5.00 6.05 121 54.0-138
Isopropylbenzene 5.00 4.99 99.8 76.0-127
p-Isopropyltoluene 5.00 5.32 106 76.0-125
2-Butanone (MEK)25.0 32.7 131 44.0-160
Methylene Chloride 5.00 5.02 100 67.0-120
4-Methyl-2-pentanone (MIBK)25.0 30.6 122 68.0-142
Methyl tert-butyl ether 5.00 4.74 94.8 68.0-125
n-Propylbenzene 5.00 5.29 106 77.0-124
Styrene 5.00 4.96 99.2 73.0-130
1,1,1,2-Tetrachloroethane 5.00 4.99 99.8 75.0-125
1,1,2,2-Tetrachloroethane 5.00 5.76 115 65.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Speedway SWDP793303 L1315684 02/25/21 11:42 15 of 30
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1619889
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1315684-01,02,03
Laboratory Control Sample (LCS)
(LCS) R3622550-1 02/11/21 21:51
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Tetrachloroethene 5.00 5.47 109 72.0-132
Toluene 5.00 5.07 101 79.0-120
1,2,3-Trichlorobenzene 5.00 5.12 102 50.0-138
1,2,4-Trichlorobenzene 5.00 4.93 98.6 57.0-137
1,1,1-Trichloroethane 5.00 5.48 110 73.0-124
1,1,2-Trichloroethane 5.00 4.81 96.2 80.0-120
Trichloroethene 5.00 5.27 105 78.0-124
Trichlorofluoromethane 5.00 6.13 123 59.0-147
1,2,3-Trichloropropane 5.00 5.86 117 73.0-130
1,3,5-Trimethylbenzene 5.00 5.22 104 76.0-122
Vinyl chloride 5.00 6.43 129 67.0-131
ethanol 250 357 143 10.0-160
tert-Butyl alcohol 25.0 26.9 108 27.0-160
tert-Amyl Methyl Ether 5.00 4.63 92.6 66.0-125
Ethyl tert-butyl ether 5.00 5.12 102 63.0-138
(S) Toluene-d8 102 80.0-120
(S) 4-Bromofluorobenzene 97.6 77.0-126
(S) 1,2-Dichloroethane-d4 105 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3622550-2 02/11/21 22:11
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
3,3-Dimethyl-1-butanol 100 97.9 97.9 55.0-148
tert-Butyl Formate 100 108 108 10.0-160
(S) Toluene-d8 102 80.0-120
(S) 4-Bromofluorobenzene 98.9 77.0-126
(S) 1,2-Dichloroethane-d4 101 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1621124
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1315684-04
Method Blank (MB)
(MB) R3623236-3 02/13/21 12:45
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acrylonitrile U 0.671 10.0
Benzene U 0.0941 1.00
Bromobenzene U 0.118 1.00
Bromodichloromethane U 0.136 1.00
Bromoform U 0.129 1.00
Bromomethane U 0.605 5.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
2,2-Dichloropropane U 0.161 1.00
Di-isopropyl ether U 0.105 1.00
Ethylbenzene U 0.137 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
Isopropylbenzene U 0.105 1.00
p-Isopropyltoluene U 0.120 1.00
Methylene Chloride U 0.430 5.00
4-Methyl-2-pentanone (MIBK)U 0.478 10.0
Methyl tert-butyl ether U 0.101 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1621124
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1315684-04
Method Blank (MB)
(MB) R3623236-3 02/13/21 12:45
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.0993 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Trichlorofluoromethane U 0.160 5.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,4-Trimethylbenzene U 0.322 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
Vinyl chloride U 0.234 1.00
Xylenes, Total U 0.174 3.00
o-Xylene U 0.174 1.00
m&p-Xylenes U 0.430 2.00
tert-Amyl Methyl Ether U 0.195 1.00
Ethyl tert-butyl ether U 0.101 1.00
tert-Butyl alcohol U 4.06 5.00
3,3-Dimethyl-1-butanol U 4.51 100
t-Amyl Alcohol U 4.90 50.0
tert-Butyl formate U 4.51 20.0
(S) Toluene-d8 102 80.0-120
(S) 4-Bromofluorobenzene 91.9 77.0-126
(S) 1,2-Dichloroethane-d4 86.6 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3623236-1 02/13/21 11:18
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
t-Amyl Alcohol 25.0 13.6 54.4 50.0-160
Acrylonitrile 25.0 20.7 82.8 55.0-149
Benzene 5.00 4.49 89.8 70.0-123
Bromobenzene 5.00 4.29 85.8 73.0-121
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Speedway SWDP793303 L1315684 02/25/21 11:42 18 of 30
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1621124
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1315684-04
Laboratory Control Sample (LCS)
(LCS) R3623236-1 02/13/21 11:18
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Bromodichloromethane 5.00 4.30 86.0 75.0-120
Bromoform 5.00 4.92 98.4 68.0-132
Bromomethane 5.00 4.94 98.8 10.0-160
sec-Butylbenzene 5.00 5.01 100 75.0-125
tert-Butylbenzene 5.00 4.76 95.2 76.0-124
Carbon tetrachloride 5.00 4.56 91.2 68.0-126
Chlorobenzene 5.00 4.89 97.8 80.0-121
Chlorodibromomethane 5.00 5.02 100 77.0-125
Chloroethane 5.00 4.69 93.8 47.0-150
Chloroform 5.00 4.94 98.8 73.0-120
Chloromethane 5.00 3.90 78.0 41.0-142
2-Chlorotoluene 5.00 4.66 93.2 76.0-123
4-Chlorotoluene 5.00 4.50 90.0 75.0-122
1,2-Dibromo-3-Chloropropane 5.00 4.25 85.0 58.0-134
1,2-Dibromoethane 5.00 4.90 98.0 80.0-122
Dibromomethane 5.00 4.75 95.0 80.0-120
1,2-Dichlorobenzene 5.00 5.14 103 79.0-121
1,3-Dichlorobenzene 5.00 4.89 97.8 79.0-120
1,4-Dichlorobenzene 5.00 4.74 94.8 79.0-120
Dichlorodifluoromethane 5.00 4.70 94.0 51.0-149
1,1-Dichloroethane 5.00 4.22 84.4 70.0-126
1,2-Dichloroethane 5.00 4.45 89.0 70.0-128
1,1-Dichloroethene 5.00 5.20 104 71.0-124
cis-1,2-Dichloroethene 5.00 4.58 91.6 73.0-120
trans-1,2-Dichloroethene 5.00 5.27 105 73.0-120
1,2-Dichloropropane 5.00 4.70 94.0 77.0-125
1,1-Dichloropropene 5.00 5.00 100 74.0-126
1,3-Dichloropropane 5.00 4.77 95.4 80.0-120
2,2-Dichloropropane 5.00 4.85 97.0 58.0-130
Di-isopropyl ether 5.00 3.45 69.0 58.0-138
Ethylbenzene 5.00 4.92 98.4 79.0-123
Hexachloro-1,3-butadiene 5.00 5.26 105 54.0-138
Isopropylbenzene 5.00 4.95 99.0 76.0-127
p-Isopropyltoluene 5.00 4.90 98.0 76.0-125
Methylene Chloride 5.00 5.01 100 67.0-120
4-Methyl-2-pentanone (MIBK)25.0 18.4 73.6 68.0-142
Methyl tert-butyl ether 5.00 4.28 85.6 68.0-125
Naphthalene 5.00 4.65 93.0 54.0-135
n-Propylbenzene 5.00 4.66 93.2 77.0-124
Styrene 5.00 4.81 96.2 73.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Speedway SWDP793303 L1315684 02/24/21 11:56 19 of 30
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Speedway SWDP793303 L1315684 02/25/21 11:42 19 of 30
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1621124
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1315684-04
Laboratory Control Sample (LCS)
(LCS) R3623236-1 02/13/21 11:18
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
1,1,1,2-Tetrachloroethane 5.00 4.69 93.8 75.0-125
1,1,2,2-Tetrachloroethane 5.00 4.71 94.2 65.0-130
Tetrachloroethene 5.00 5.53 111 72.0-132
Toluene 5.00 5.06 101 79.0-120
1,2,3-Trichlorobenzene 5.00 4.91 98.2 50.0-138
1,2,4-Trichlorobenzene 5.00 4.57 91.4 57.0-137
1,1,1-Trichloroethane 5.00 4.85 97.0 73.0-124
1,1,2-Trichloroethane 5.00 5.07 101 80.0-120
Trichloroethene 5.00 4.63 92.6 78.0-124
Trichlorofluoromethane 5.00 5.11 102 59.0-147
1,2,3-Trichloropropane 5.00 4.88 97.6 73.0-130
1,2,4-Trimethylbenzene 5.00 4.86 97.2 76.0-121
1,3,5-Trimethylbenzene 5.00 4.81 96.2 76.0-122
Vinyl chloride 5.00 4.51 90.2 67.0-131
Xylenes, Total 15.0 14.5 96.7 79.0-123
o-Xylene 5.00 4.79 95.8 80.0-122
m&p-Xylenes 10.0 9.68 96.8 80.0-122
tert-Butyl alcohol 25.0 17.3 69.2 27.0-160
tert-Amyl Methyl Ether 5.00 4.32 86.4 66.0-125
Ethyl tert-butyl ether 5.00 4.06 81.2 63.0-138
(S) Toluene-d8 99.2 80.0-120
(S) 4-Bromofluorobenzene 91.3 77.0-126
(S) 1,2-Dichloroethane-d4 90.9 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3623236-2 02/13/21 12:02
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
3,3-Dimethyl-1-butanol 100 78.6 78.6 55.0-148
tert-Butyl Formate 100 71.6 71.6 10.0-160
(S) Toluene-d8 100 80.0-120
(S) 4-Bromofluorobenzene 94.3 77.0-126
(S) 1,2-Dichloroethane-d4 87.5 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1621124
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1315684-04
L1316387-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1316387-02 02/13/21 20:51 • (MS) R3623236-4 02/13/21 21:34 • (MSD) R3623236-5 02/13/21 21:56
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Acrylonitrile 250 U 220 240 88.0 96.0 10 21.0-160 8.70 32
Benzene 50.0 658 614 619 0.000 0.000 10 17.0-158 V V 0.811 27
Bromobenzene 50.0 U 35.7 30.7 71.4 61.4 10 30.0-149 15.1 28
Bromodichloromethane 50.0 U 33.4 28.6 66.8 57.2 10 31.0-150 15.5 27
Bromoform 50.0 U 41.4 45.7 82.8 91.4 10 29.0-150 9.87 29
Bromomethane 50.0 U 24.2 19.5 48.4 39.0 10 10.0-160 21.5 38
sec-Butylbenzene 50.0 1.29 27.2 17.8 51.8 33.0 10 33.0-155 J3 41.8 29
tert-Butylbenzene 50.0 2.26 26.8 17.9 49.1 31.3 10 34.0-153 J3 J6 39.8 28
Carbon tetrachloride 50.0 U 19.9 12.6 39.8 25.2 10 23.0-159 J3 44.9 28
Chlorobenzene 50.0 U 35.3 28.9 70.6 57.8 10 33.0-152 19.9 27
Chlorodibromomethane 50.0 U 43.8 42.1 87.6 84.2 10 37.0-149 3.96 27
Chloroethane 50.0 U 20.8 15.4 41.6 30.8 10 10.0-160 29.8 30
Chloroform 50.0 U 36.4 28.3 72.8 56.6 10 29.0-154 25.0 28
Chloromethane 50.0 U 17.9 14.1 35.8 28.2 10 10.0-160 23.7 29
2-Chlorotoluene 50.0 U 31.1 23.6 62.2 47.2 10 32.0-153 27.4 28
4-Chlorotoluene 50.0 U 32.0 24.6 64.0 49.2 10 32.0-150 26.1 28
1,2-Dibromo-3-Chloropropane 50.0 U 46.6 46.8 93.2 93.6 10 22.0-151 0.428 34
1,2-Dibromoethane 50.0 U 47.3 45.6 94.6 91.2 10 34.0-147 3.66 27
Dibromomethane 50.0 U 42.6 40.8 85.2 81.6 10 30.0-151 4.32 27
1,2-Dichlorobenzene 50.0 U 42.0 36.4 84.0 72.8 10 34.0-149 14.3 28
1,3-Dichlorobenzene 50.0 U 37.3 30.8 74.6 61.6 10 36.0-146 19.1 27
1,4-Dichlorobenzene 50.0 U 39.3 32.9 78.6 65.8 10 35.0-142 17.7 27
Dichlorodifluoromethane 50.0 U 8.50 4.74 17.0 9.48 10 10.0-160 J3 J6 56.8 29
1,1-Dichloroethane 50.0 U 24.9 19.6 49.8 39.2 10 25.0-158 23.8 27
1,2-Dichloroethane 50.0 U 37.7 34.8 75.4 69.6 10 29.0-151 8.00 27
1,1-Dichloroethene 50.0 U 19.9 12.5 39.8 25.0 10 11.0-160 J3 45.7 29
cis-1,2-Dichloroethene 50.0 U 30.8 24.4 61.6 48.8 10 10.0-160 23.2 27
trans-1,2-Dichloroethene 50.0 U 26.2 19.0 52.4 38.0 10 17.0-153 J3 31.9 27
1,2-Dichloropropane 50.0 U 34.5 28.6 69.0 57.2 10 30.0-156 18.7 27
1,1-Dichloropropene 50.0 U 21.6 13.3 43.2 26.6 10 25.0-158 J3 47.6 27
1,3-Dichloropropane 50.0 U 45.7 42.7 91.4 85.4 10 38.0-147 6.79 27
2,2-Dichloropropane 50.0 U 23.5 14.6 47.0 29.2 10 24.0-152 J3 46.7 29
Di-isopropyl ether 50.0 U 28.2 24.6 56.4 49.2 10 21.0-160 13.6 28
Ethylbenzene 50.0 31.0 58.3 50.5 54.6 39.0 10 30.0-155 14.3 27
Hexachloro-1,3-butadiene 50.0 U 22.8 15.5 45.6 31.0 10 20.0-154 J3 38.1 34
Isopropylbenzene 50.0 5.23 32.2 24.3 53.9 38.1 10 28.0-157 J3 28.0 27
p-Isopropyltoluene 50.0 U 26.1 18.1 52.2 36.2 10 30.0-154 J3 36.2 29
Methylene Chloride 50.0 U 36.3 31.8 72.6 63.6 10 23.0-144 13.2 28
4-Methyl-2-pentanone (MIBK)250 U 203 209 81.2 83.6 10 29.0-160 2.91 29
Methyl tert-butyl ether 50.0 U 41.9 40.5 83.8 81.0 10 28.0-150 3.40 29
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1621124
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1315684-04
L1316387-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1316387-02 02/13/21 20:51 • (MS) R3623236-4 02/13/21 21:34 • (MSD) R3623236-5 02/13/21 21:56
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Naphthalene 50.0 U 43.8 45.5 87.6 91.0 10 12.0-156 3.81 35
n-Propylbenzene 50.0 9.39 34.8 26.8 50.8 34.8 10 31.0-154 26.0 28
Styrene 50.0 U 36.4 30.2 72.8 60.4 10 33.0-155 18.6 28
1,1,1,2-Tetrachloroethane 50.0 U 36.5 30.0 73.0 60.0 10 36.0-151 19.5 29
1,1,2,2-Tetrachloroethane 50.0 U 49.4 49.9 98.8 99.8 10 33.0-150 1.01 28
Tetrachloroethene 50.0 U 27.1 17.2 54.2 34.4 10 10.0-160 J3 44.7 27
Toluene 50.0 U 32.5 24.8 65.0 49.6 10 26.0-154 26.9 28
1,2,3-Trichlorobenzene 50.0 U 36.7 36.7 73.4 73.4 10 17.0-150 0.000 36
1,2,4-Trichlorobenzene 50.0 U 32.8 31.6 65.6 63.2 10 24.0-150 3.73 33
1,1,1-Trichloroethane 50.0 U 21.7 14.2 43.4 28.4 10 23.0-160 J3 41.8 28
1,1,2-Trichloroethane 50.0 U 49.4 46.4 98.8 92.8 10 35.0-147 6.26 27
Trichloroethene 50.0 U 26.0 17.9 52.0 35.8 10 10.0-160 J3 36.9 25
Trichlorofluoromethane 50.0 U 15.0 8.65 30.0 17.3 10 17.0-160 J3 53.7 31
1,2,3-Trichloropropane 50.0 U 53.7 53.2 107 106 10 34.0-151 0.935 29
1,2,4-Trimethylbenzene 50.0 15.7 47.0 39.0 62.6 46.6 10 26.0-154 18.6 27
1,3,5-Trimethylbenzene 50.0 U 28.7 21.3 57.4 42.6 10 28.0-153 J3 29.6 27
Vinyl chloride 50.0 U 14.2 9.35 28.4 18.7 10 10.0-160 J3 41.2 27
Xylenes, Total 150 U 92.3 71.9 61.5 47.9 10 29.0-154 24.8 28
o-Xylene 50.0 U 32.5 25.1 65.0 50.2 10 45.0-144 25.7 26
m&p-Xylenes 100 U 59.8 46.8 59.8 46.8 10 43.0-146 24.4 26
tert-Butyl alcohol 250 U 156 180 62.4 72.0 10 50.0-150 14.3 20
tert-Amyl Methyl Ether 50.0 14.0 38.7 37.0 49.4 46.0 10 10.0-160 4.49 37
Ethyl tert-butyl ether 50.0 U 36.6 33.8 73.2 67.6 10 10.0-160 7.95 37
(S) Toluene-d8 99.2 100 80.0-120
(S) 4-Bromofluorobenzene 92.1 93.5 77.0-126
(S) 1,2-Dichloroethane-d4 87.7 88.0 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1619446
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1315684-01,02,03
Method Blank (MB)
(MB) R3621538-2 02/10/21 13:48
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Benzene U 0.0941 1.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
Ethylbenzene U 0.137 1.00
Isopropylbenzene U 0.105 1.00
p-Isopropyltoluene U 0.120 1.00
n-Propylbenzene U 0.0993 1.00
Toluene U 0.278 1.00
1,2,4-Trimethylbenzene U 0.322 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
Xylenes, Total U 0.174 3.00
o-Xylene U 0.174 1.00
m&p-Xylenes U 0.430 2.00
(S) Toluene-d8 116 80.0-120
(S) 4-Bromofluorobenzene 98.0 77.0-126
(S) 1,2-Dichloroethane-d4 115 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3621538-1 02/10/21 13:07
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Benzene 5.00 5.28 106 70.0-123
n-Butylbenzene 5.00 5.66 113 73.0-125
sec-Butylbenzene 5.00 6.21 124 75.0-125
Ethylbenzene 5.00 6.01 120 79.0-123
Isopropylbenzene 5.00 5.86 117 76.0-127
p-Isopropyltoluene 5.00 5.98 120 76.0-125
n-Propylbenzene 5.00 6.22 124 77.0-124
Toluene 5.00 5.73 115 79.0-120
1,2,4-Trimethylbenzene 5.00 5.98 120 76.0-121
1,3,5-Trimethylbenzene 5.00 6.37 127 76.0-122 J4
Xylenes, Total 15.0 17.2 115 79.0-123
o-Xylene 5.00 5.60 112 80.0-122
m&p-Xylenes 10.0 11.6 116 80.0-122
(S) Toluene-d8 111 80.0-120
(S) 4-Bromofluorobenzene 98.1 77.0-126
(S) 1,2-Dichloroethane-d4 114 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1621611
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1315684-01,02,03
Method Blank (MB)
(MB) R3623139-3 02/18/21 11:24
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Naphthalene U 1.00 5.00
(S) Toluene-d8 103 80.0-120
(S) 4-Bromofluorobenzene 102 77.0-126
(S) 1,2-Dichloroethane-d4 110 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3623139-1 02/18/21 10:23 • (LCSD) R3623139-2 02/18/21 10:43
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Naphthalene 5.00 4.98 4.64 99.6 92.8 54.0-135 7.07 20
(S) Toluene-d8 102 103 80.0-120
(S) 4-Bromofluorobenzene 101 99.4 77.0-126
(S) 1,2-Dichloroethane-d4 109 111 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1622526
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1315684-04
Method Blank (MB)
(MB) R3624032-2 02/22/21 16:32
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acetone U 11.3 50.0
Acrolein U 2.54 50.0
n-Butylbenzene U 0.157 1.00
Ethanol U 42.0 100
2-Butanone (MEK)U 1.19 10.0
(S) Toluene-d8 113 80.0-120
(S) 4-Bromofluorobenzene 107 77.0-126
(S) 1,2-Dichloroethane-d4 90.8 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3624032-1 02/22/21 15:51
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acetone 25.0 18.9 75.6 19.0-160
Acrolein 25.0 25.3 101 10.0-160
n-Butylbenzene 5.00 4.80 96.0 73.0-125
2-Butanone (MEK)25.0 20.1 80.4 44.0-160
ethanol 250 257 103 10.0-160
(S) Toluene-d8 102 80.0-120
(S) 4-Bromofluorobenzene 103 77.0-126
(S) 1,2-Dichloroethane-d4 91.3 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
Abbreviations and Definitions
Qualifier Description
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN, 37122
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ACCREDITATIONS & LOCATIONS
¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Page 1 of 1
TURN AROUND TIME
STANDARD
Chain-of-Custody-Record
Speedway Project Information
Speedway Store #: C210008232 Facility ID 0-034026
Address:24 S Raleigh Rd
City:Angier State:NC
Phone #:Fax #:
Speedway Proj. Mgr: Charles Chiara **INVOICE TO SPEEDWAY**
AFE #:190260 Work Order #:1104046474
COC ID # 00054623
Lab Information
Lab:Pace Analytical Services (TN)
Consultant:ATC Group Services - Columbia, SC
Project Mgr: Donald Hurdle
Address:
Phone #:Fax #:
Sampler:Brian Buchanan
Shipped:FedExp
Tracking #:TBD
Sample ID Date/Time Sampled Matrix Count Container Type Preservative Analysis to be Performed Method Remarks
MW-01 02/09/2021 11:15am W 3 40 MIL AMBER VIAL HCL Eight Oxygenates 6200B
40 MIL AMBER VIAL HCL 6200B Full LIst 6200B
MW-02 02/09/2021 10:55am W 3 40 MIL AMBER VIAL HCL Eight Oxygenates 6200B
40 MIL AMBER VIAL HCL 6200B Full LIst 6200B
MW-03 02/09/2021 11:35am W 3 40 MIL AMBER VIAL HCL Eight Oxygenates 6200B
40 MIL AMBER VIAL HCL 6200B Full LIst 6200B
MW-05 02/09/2021 12:15pm W 5 40 MIL AMBER VIAL HCL Eight Oxygenates 6200B
40 MIL AMBER VIAL HCL 6200B Full LIst 6200B
Relinquished by:Date Time Received by:Date Time
Relinquished by:Date Time Received by laboratory:Date Time
Special Reporting Requirements:Lab Notes:Temp
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Chain of Custody Analysis to be Performed Chain-of-Custody-Record
COC ID # 54623 Printed: 02/11/2021
Analysis Name: 6200B Full LIst ( Water )
Analysis Description / Method:6200B Full List / 6200B
Container Type / Preservative:40 MIL AMBER VIAL / HCL
Analytes: 1,1,1,2-Tetrachloroethane ug/L, 1,1,1-Trichloroethane ug/L, 1,1,2,2-Tetrachloroethane ug/L, 1,1,2-Trichloroethane ug/L, 1,1-Dichloroethane ug/L, 1,1-Dichloroethene ug/L, 1,1-Dichloropropene ug/L,
1,2,3-Trichlorobenzene ug/L, 1,2,3-Trichloropropane ug/L, 1,2,4-Trichlorobenzene ug/L, 1,2,4-Trimethylbenzene ug/L, 1,2-Dibromo-3-chloropropane ug/L, 1,2-Dibromoethane ug/L, 1,2-Dichlorobenzene ug/L,
1,2-Dichloroethane ug/L, 1,2-Dichloropropane ug/L, 1,3,5-Trimethylbenzene ug/L, 1,3-Dichlorobenzene ug/L, 1,3-Dichloropropane ug/L, 1,4-Dichlorobenzene ug/L, 2,2-Dichloropropane ug/L, 2-Butanone ug/L,
2-Chlorotoluene ug/L, 4-Chlorotoluene ug/L, 4-Methyl-2-pentanone ug/L, Acetone ug/L, Acrolein ug/L, Acrylonitrile ug/L, Benzene ug/L, Bromobenzene ug/L, Bromodichloromethane ug/L, Bromoform ug/L, Bromomethane
ug/L, Carbon tetrachloride ug/L, Chlorobenzene ug/L, Chlorodibromomethane ug/L, Chloroethane ug/L, Chloroform ug/L, Chloromethane ug/L, Dibromomethane ug/L, Dichlorodifluoromethane ug/L, Diisopropyl ether ug/L,
Ethylbenzene ug/L, Hexchloro-1,3-butadiene ug/L, Isopropylbenzene ug/L, Methyl tert butyl ether ug/L, Methylene chloride ug/L, Naphthalene ug/L, Styrene ug/L, Tetrachloroethene ug/L, Toluene ug/L, Total Xylenes ug/L,
Trichloroethene ug/L, Trichlorofluoromethane ug/L, Vinyl chloride ug/L, cis-1,2-Dichloroethene ug/L, m,p-Xylene ug/L, n-Butylbenzene ug/L, n-Propylbenzene ug/L, o-Xylene ug/L, p-Isopropyltoluene ug/L,
sec-Butylbenzene ug/L, tert-Butylbenzene ug/L, trans-1,2-Dichloroethene ug/L
Analysis Name: Eight Oxygenates ( Water )
Analysis Description / Method:Eight oxygenates by 6200B / 6200B
Container Type / Preservative:40 MIL AMBER VIAL / HCL
Analytes: 3,3-Dimethyl-1-butanol ug/L, Diisopropyl ether ug/L, Ethanol ug/L, t-Butyl alcohol ug/L, tert-Amyl alcohol ug/L, tert-Amyl methyl ether ug/L, tert-Butyl ethyl ether ug/L, tert-Butyl formate ug/L
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