FA-7752_42035_CA_MRP_20230530

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
May 31, 2023

Mr. Mike Haseltine
NCDEQ-UST Section
Wilmington Regional Office
127 Cardinal Drive Extension
Wilmington, NC 28405

Re: Ground Water Monitoring Report
May 2023
J Mart
5654 NC Highway 87 South
Sanford, Lee County
North Carolina
Facility ID Number: 00-0-0000024866
Incident Number: 42035
GRI Project Number: 4238

Dear Mr. Haseltine,

Please find enclosed the referenced report for the abovementioned site.
If you have any questions, please contact William Regenthal at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Ms. Jackie Stillwell, file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127

Ground Water Monitoring Report
May 2023
J Mart
5654 NC Highway 87 South
Sanford, Lee County
North Carolina
Facility ID Number: 00-0-000024866
Incident Number: 42035
GRI Project Number: 4238

Prepared for:

Ms. Jackie Stillwell
6406 Cabin Branch Drive
Durham, North Carolina 27712

May 30, 2023

William Regenthal, P. G.
Project Manager
Blake Butcher
Staff Scientist

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: May 30, 2023 J Mart
Project Manager: William Regenthal, P. G. GRI Project No. 4238
i
SITE INFORMATION
1. Site Identification
 J Mart (Facility ID 00-0-000024866)
 Incident Number 42035 – High Risk (H210D)
 Location of Source Area: 5654 NC Highway 87 South
Sanford, NC 27824
Lee County
35.407950°N, 79.115805°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST Owner
Ms. Jackie Stillwell
6406 Cabin Branch Drive
Durham, NC 27712
[e-mail]
919-477-3603

UST Operator
Jack and Marie Stillwell
4203 NC Highway 87 South
Sanford, NC 27332
[e-mail]
919-477-3603

Property Owner
Ms. Marie B. Stillwell (heirs)
6406 Cabin Branch Drive
Durham, NC 27712
[e-mail]
919-477-3603

Property Occupant
Lee County Online Sales &
Rewards Center
5654 US Highway 87 South
Sanford, NC 27330
Email Unknown
919-498-0094
Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
SGS - North America, Inc.
4405 Vineland Road, Suite C-15
Orlando, FL 32811
State Certification No. 573
407-425-6700
3. Information about Release
 A release was confirmed on November 16, 2016
 An unknown amount of product was released from the leaking UST System
 One 6,000-gallon gasoline and two 4,000-gallon gasoline USTs were removed from the site in
November 2016

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: May 30, 2023 J Mart
Project Manager: William Regenthal, P. G. GRI Project No. 4238
ii
EXECUTIVE SUMMARY
J Mart is located at 5654 NC Highway 87 South in Sanford, Lee County, North Carolina. The site is currently
owned by Ms. Marie Stillwell heirs and is operated by Lee County Online Sales & Reward Center as an
internet cafe. One 6,000-gallon gasoline and two 4,000-gallon gasoline USTs were removed from the site
between November 15 and 16, 2016. A release was reported to NCDEQ on November 29, 2016, upon
receipt of the laboratory report for soil samples collected during the November 2016 UST closure
activities. The adjoining properties are a mixture of general business, agricultural, and residential
properties. According to the information determined during receptor survey activities, seven potable
water supply wells are located within 1,000 feet of the site. One potable water supply well (WSW-1) was
identified within a 250-foot radius of the site. Municipal water is not available to the site or surrounding
properties.

A CSA was completed in February 2018. A CAP has not been developed for this incident.

On May 8, 2023, twenty Type II monitoring wells (MW-1 through MW-20), one Type III monitoring well
(TW-1) and one water supply well (WSW-1) were gauged, purged and/or sampled in accordance with
NCDEQ guidelines. Free product was not measured during the May 2023 sampling and gauging event.
Concentrations of individual BTEX constituents, MTBE, naphthalene, 1,2-dichloroethane, n-
propylbenzene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, TAA, TBA and/or methylene chloride
that exceeded the MACs were reported in the ground water samples collected from MW-1, MW-3, MW-
4, MW-13, MW-18, MW-20, and TW-1. A concentration of benzene that exceeded the GCL was reported
in the ground water sample collected from MW-4.

Based on the above information, the site risk classification should remain as high. The contaminant plume
is reasonably defined for this incident. A CAP for site remediation should be prepared. In preparation for
the CAP activities, a pilot study for the injection of petroleum hydrocarbon reducing compounds (CoolOx®,
PetroFix®, ORC or other like compounds) should be conducted in the vicinity MW-3 and MW-4. Once the
pilot study is completed, a feasibility study for the implementation of a CAP can be completed. In the
interim, semi-annual ground water sampling activities should continue at the site. The next sampling
event is tentatively scheduled for November 2023.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: May 30, 2023 J Mart
Project Manager: William Regenthal, P. G. GRI Project No. 4238
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
HERR: HAZMAT Emergency Response and
Remediation, Inc.
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
ORC: Oxygen Releasing Compound
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: May 30, 2023 J Mart
Project Manager: William Regenthal, P. G. GRI Project No. 4238

TABLE OF CONTENTS
SITE INFORMATION ............................................................................................................................ i
EXECUTIVE SUMMARY ....................................................................................................................... ii
ACRONYMS ....................................................................................................................................... iii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................2
3.0 FREE PRODUCT REMOVAL ........................................................................................................4
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................4
5.0 CONCLUSIONS .........................................................................................................................5
6.0 LIMITATIONS ...........................................................................................................................5
7.0 STATEMENTS AND CERTIFICATION ...........................................................................................5

FIGURES
Figure 1: Site Location Map
Figure 2: Site Vicinity Map
Figure 3: Site Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map
Figure 6: Benzene Isoconcentration Map
Figure 7: MTBE Isoconcentration Map
Figure 8: Estimated Contaminant Mass Map
Figure 9: A-A’ Cross Section Map
Figure 10: B-B’ Cross Section Map

TABLES
Table 1: UST Owner/Operator Information
Table 2: UST System Information
Table 3: Water Supply Well Information
Table 4: Adjacent Property Owner Information
Table 5: Well Construction and Gauging Information
Table 6: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: State Correspondence
Appendix B: Laboratory Reports – Ground Water Samples
Appendix C: Contaminant Mass Calculations

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: May 30, 2023 J Mart
Project Manager: William Regenthal, P. G. GRI Project No. 4238
1
1.0 SITE HISTORY AND CHARACTERIZATION
GRI presents the results of the May 2023 ground water sampling event at the J Mart site; located at 5654
NC Highway 87 South in Sanford, Lee County, North Carolina (Figure 1). These activities were conducted
in accordance with GRI Proposal No. 23-252, which was submitted to NCDEQ on April 24, 2023, and was
approved as Task Authorization No. 42035-10 on April 25, 2023. State correspondence has been included
as Appendix A.

The site is currently owned by Ms. Marie Stillwell heirs and is operated by Lee County Online Sales &
Reward Center as an internet cafe. According to available information, one 6,000-gallon gasoline and two
4,000-gallon gasoline USTs were removed from the site on November 15, 2016. UST owner/operator
information and UST system information are included as Tables 1 and 2, respectively. The Registered
Tank Report is shown below:

The site and surrounding area are a mixture of general business, agricultural, and residential properties.
The site contains one building and is primarily capped with concrete. The overall topography at the site
generally slopes toward the southwest. The closest surface water body is the Upper Little River Tributary
which is located approximately 1,050 feet west of the site. Twenty Type II monitoring wells (MW-1
through MW-20) and one Type III monitoring well (TW-1) were installed at the site during previous ground
water assessment and corrective action activities.

In March 2017, GRI personnel conducted a receptor survey at the site. Twelve water supply wells were
identified within a 1,500-foot radius of the site. Seven potable water supply wells were identified within
a 1,000-foot radius of the site. One potable water supply well (WSW-1) was identified within a 250-foot
radius of the site. Municipal water is not available to the site and surrounding properties. Water supply
well owner information is included as Table 3. Adjacent property owner information is presented in Table
4. A Site Vicinity Map showing the adjacent properties has been included as Figure 2. A Site Map showing
the locations of the monitoring wells and the structures on-site has been included as Figure 3.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: May 30, 2023 J Mart
Project Manager: William Regenthal, P. G. GRI Project No. 4238
2
A CSA was completed in February 2019. To date, a CAP has not been developed for this incident.
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
On May 8, 2023, twenty Type II monitoring wells (MW-1 through MW-20), one Type III monitoring well
(TW-1) and one water supply well (WSW-1) were gauged, purged and/or sampled. Depths to ground
water in the Type II monitoring wells ranged from 11.76 feet to 24.63 feet below TOC. Well construction
and gauging information is presented in Table 5. Ground water elevations in the Type II monitoring wells
relative to a temporary benchmark with an assumed datum of 100.00 feet ranged from 67.44 to 81.54
feet. Based on this information, ground water flow direction is generally toward the southwest. The
horizontal hydraulic gradient across the site was approximately 0.05 feet per foot. The vertical hydraulic
gradient between paired wells MW-4/TW-1 was approximately 0.02 feet per foot downward. A Water
Table Surface Map is included as Figure 4. A summary of the current ground water gauging data is shown
below:

Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
MW-1 25 – 45 45 100.00 19.61 --- 80.39
MW-2 20 – 40 40 101.00 21.22 --- 79.78
MW-3 20 – 40 40 99.88 19.60 --- 80.28
MW-4 20 – 40 40 99.86 21.34 --- 78.52
MW-5 20 – 40 40 98.48 20.91 --- 77.57
MW-6 20 – 40 40 103.52 24.63 --- 78.89
MW-7 20 - 40 40 103.73 23.12 --- 80.61
MW-8 20 – 40 40 97.42 20.89 --- 76.53
MW-9 20 – 40 40 101.80 20.26 --- 81.54
MW-10 20 – 40 40 100.37 19.75 --- 80.62
MW-11 20 - 40 40 97.59 20.71 --- 76.88
MW-12 20 - 40 40 92.77 17.99 --- 74.78
MW-13 20 – 40 40 96.99 20.38 --- 76.61
MW-14 20 - 40 40 99.82 22.41 --- 77.41
MW-15 15 - 35 35 88.42 17.32 --- 71.10
MW-16 15 – 35 35 84.19 13.35 --- 70.84
MW-17 15 - 35 35 85.39 11.76 --- 73.63
MW-18 15 - 35 35 90.71 20.30 --- 70.41
MW-19 10 -25 25 86.86 19.42 --- 67.44
MW-20 10 - 25 25 87.97 18.71 --- 69.26
TW-1 55 - 60 60 99.76 21.98 --- 77.78

Ground water samples collected from the monitoring and water supply wells were submitted for
laboratory analyses of VOCs plus oxygenates using EPA Method 6200B. Natural attenuation samples
(nitrate, sulfate, ferrous iron and methane) and field parameters (dissolved oxygen, oxidation reduction
potential, temperature, pH and conductivity) were collected for MW-1 through MW-5, MW-9, MW-10,
MW-13, MW-14, MW-15, MW-18, MW_19 and MW-20. Concentrations of individual BTEX constituents,

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: May 30, 2023 J Mart
Project Manager: William Regenthal, P. G. GRI Project No. 4238
3
MTBE, naphthalene, 1,2-dichloroethane, n-propylbenzene, 1,2,4-trimethylbenzene, 1,3,5-
trimethylbenzene, TAA, TBA and/or methylene chloride that exceeded the MACs were reported in the
ground water samples collected from MW-1, MW-3, MW-4, MW-13, MW-18, MW-20, and TW-1. The
concentration of benzene reported in the ground water sample collected from MW-4 exceeded the GCL.
A summary of the analytical results for ground water samples collected on July 28, 2022, is presented in
Table 6. A summary of natural attenuation parameter results is presented in Table 6A. A Ground Water
Quality Map based on the May 2023 data is included as Figure 5. Contaminant specific isoconcentration
maps for benzene and MTBE have been included as Figures 6 and 7, respectively. A complete report of
laboratory analyses of the ground water samples collected from the monitoring wells during the May 2023
sampling event has been included as Appendix B. A summary of the current ground water analytical data
is shown below:

Contaminant
of Concern 
Be
n
z
e
n
e

To
l
u
e
n
e

Et
h
y
l
b
e
n
z
e
n
e

Xy
l
e
n
e
s

MT
B
E

Na
p
h
t
h
a
l
e
n
e

Well
ID
MACs (µg/l) 1 600 600 500 20 6
GCL (µg/l) 5,000 260,000 80,000 50,000 20,000 6,000
MW-1 1.7 2.4 1.1 7.2 0.23 J 0.25 J
MW-2 0.67 0.51 0.22 J 1.4 J <0.13 <0.13
MW-3 957 18.4 359 830 196 107
MW-4 5,930 4,220 2,460 13,200 1,830 698
MW-5 <0.13 <0.13 <0.13 <0.25 1.8 <0.13
MW-6 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13
MW-7 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13
MW-8 0.47 J <0.13 0.20 J 0.60 J 0.54 <0.13
MW-9 0.19 J <0.13 <0.13 0.40 J <0.13 <0.13
MW-10 0.16 J <0.13 0.13 J 0.36 J <0.13 <0.13
MW-11 0.13 J <0.13 <0.13 <0.25 <0.13 <0.13
MW-12 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13
MW-13 <0.63 <0.63 <0.63 <1.3 198 <0.63
MW-14 <0.13 <0.13 <0.13 <0.25 2.9 <0.13
MW-15 <0.13 <0.13 <0.13 <0.25 0.31 J <0.13
MW-16 <0.13 <0.13 <0.13 <0.25 0.52 <0.13
MW-17 <0.13 <0.13 <0.13 <0.25 0.21 J <0.13
MW-18 <0.13 <0.13 <0.13 <0.25 37.3 <0.13
MW-19 <0.13 <0.13 <0.13 <0.25 3.1 <0.13
MW-20 <0.13 <0.13 <0.13 <0.25 82.1 <0.13
TW-1 168 <0.63 <0.13 <0.25 <0.13 <0.63
WSW-1 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13

The baseline contaminant mass at the site was determined based on the total BTEX, MTBE, and
naphthalene concentrations from the May 2017 ground water sampling event, as well as the maximum
historical water column height observed in each area. The contaminant plume was divided into two areas
(Areas 1 and 2) based on the benzene and MTBE concentrations during the May 2017 ground water
sampling event. The total contaminant mass at the site has decreased by 67.3% since May 2017.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: May 30, 2023 J Mart
Project Manager: William Regenthal, P. G. GRI Project No. 4238
4
Contaminant mass calculations have been included as Appendix C. A map of the contaminant mass areas
has been included as Figure 8. A chart depicting the overall trend in contaminant mass is shown below:

The site is in the Piedmont Physiographic Province of North Carolina. The water table has a seasonal high
depth to water of approximately 11 to 25 feet BGS. Since a CAP has not been developed for the site,
remediation milestones have not been established for the site. Cross sections depicting the subsurface
at the site based on past well drilling activities are included as Figures 9 and 10.
3.0 FREE PRODUCT REMOVAL
Free product has not been observed at the site. On May 18, 2021, an AFVR was conducted on MW-3 and
MW_4. Of the total liquids extracted during the May 18, 2021, AFVR, no measurable free product was
removed. Based on mass-removal calculations, an additional 0.16 pounds or 0.03 gallons of vapor phase
hydrocarbons were removed during this event. The May 2021 AFVR event was the first AFVR event
conducted at the site, and only AFVR conducted to-date.
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
No natural attenuation monitoring plan is currently in place at the site.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: May 30, 2023 J Mart
Project Manager: William Regenthal, P. G. GRI Project No. 4238
5
5.0 CONCLUSIONS
 On May 8, 2023, twenty Type II monitoring wells, one Type III monitoring well, and one water
supply well were gauged, purged and/or sampled. Ground water flow direction is generally
toward the southwest. The horizontal hydraulic gradient across the site was approximately 0.05
feet per foot. The vertical hydraulic gradient between paired wells MW-4/TW-1 was
approximately 0.02 feet per foot downward.
 Concentrations of individual BTEX constituents, MTBE, naphthalene, 1,2-dichloroethane, n-
propylbenzene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, TAA, TBA and/or methylene
chloride that exceeded the MACs were reported in the ground water samples collected from MW-
1, MW-3, MW-4, MW-13, MW-18, MW-20 and TW-1. A concentration of benzene that exceeded
the GCL was reported in the ground water sample collected from MW-4.
 Contaminant mass at the site decreased by approximately 67.3% since the May 2017 ground
water sampling event.
 Based on the above information, the site risk classification should remain as high. The
contaminant plume is reasonably defined for this incident. A CAP for site remediation should be
prepared. In preparation for the CAP activities, a pilot study for the injection of petroleum
hydrocarbon reducing compounds (CoolOx®, PetroFix®, ORC or other like compounds) should be
conducted in the vicinity MW-3 and MW-4. Once the pilot study is completed, a feasibility study
for the implementation of a CAP can be completed. In the interim, semi-annual ground water
sampling activities should continue at the site. The next sampling event is tentatively scheduled
for November 2023.
6.0 LIMITATIONS
This report has been prepared for the exclusive use of Ms. Jackie Stillwell for specific application to the
referenced site in Lee County, North Carolina. The assessment was conducted based on the scope of work
and level of effort desired by NCDEQ and with resources adequate only for that scope of work. Our
findings have been developed in accordance with generally accepted standards of environmental
practices in the State of North Carolina, available information, and our professional judgment. No other
warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.
7.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. N/A Will this report be submitted after the
established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO

FIGURES
Copyright (C) 2009 MyTopo
SCALE 1:24000
0 1000 2000 3000 4000 5000
FEET
Declination
MN 8.81° W
MN
Location: 035.4079500° N 079.1158050° WDate: 07/11/17
Scale: 1 inch = 2,000 ft.
Copyright (C) 2009 MyTopo
Figure 1
J Mart
5654 NC Highway 87 S Sanford, Lee, NC
Incident No. 42035
GRI Project No. 4238
SITE LOCATION
!
WSW-1
"JWSW-2
"J
WSW-3
"J
WSW-4
"J
WSW-5
"J
WSW-6
"J
WSW-7
"J
WSW-8
"J
WSW-9
"J
WSW-10
"J
WSW-11
"J
WSW-12
"J
LAKETRACE
UPPERLITTLE
RIVERTRIBUTARY
LAKETRACETRIBUTARY
UPPERLITTLERIVERTRIBUTARY
9660-53-0622-00
9660-42-2929-00
9660-53-8165-00
9660-53-4332-00
9660-53-7655-00
9660-54-9401-00
9660-54-0748-00
9660-53-2103-00
9660-54-6354-00
9660-44-9400-00
9660-52-6235-00
9660-52-6661-00
9660-54-6513-00
9660-52-5965-00
9660-54-2296-00
LAKEVIEW DR
TRACEWAY NORTH
TOPSIDE RD
UPPER DECK
NC 87 HWY
INDIAN TRL
EMORY PNT
WINSTEAD RD
SAW TIMBER
FIGURE 2SITE VICINITY MAPJ MART5654 N.C. HIGHWAY 87 SOUTHSANFORD, LEE COUNTY,NORTH CAROLINAINCIDENT NO. 42035GRI PROJECT NO. 4238
PREPARED BY:GEOLOGICAL RESOURCES, INC.MARCH 23, 2017
0 300 600150Feet
SCALE: 1 INCH = 300 FEET
³
NOTE:THIS MAP IS BASED ON DATA FROM THELEE COUNTY GIS OF NC.
SITE
Legend
Subject Parcel
Parcel Boundary
Street Centerline
Stream or Creek Line
250-FT RADIUS
500-FT RADIUS
1,000-FT RADIUS
1,500-FT RADIUS
Parcel ID Number9660-53-4332-00
Water Supply Well"J

TABLES
UST ID Number 1 - 3 Facility ID Number
Owner or Operator?
Owner
TABLE 1
UST OWNER/OPERATOR INFORMATION
J MART (INCIDENT NO. 42035)
6406 Cabin Branch Drive, Durham, NC 27712 919-541-0326
0-0024866
Dates of Ownership / OperationName of Owner or Operator
Address Telephone Number
Jack and Marie Stillwell 4/26/1983 - 11/15/16
Page 1 of 1
Date: 8/23/2019 Facility ID #: 0-0024866
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline Gasoline 6,000 4/26/83 Single Wall Steel 8' x 16'Steel Removed
(11/15/16)Unknown
2 Gasoline Gasoline 4,000 4/26/83 Single Wall Steel 64" x 24'Steel Removed
(11/15/16)Unknown
3 Gasoline Gasoline 4,000 4/26/83 Single Wall Steel 64" x 24'Steel Removed
(11/15/16)Unknown
J MART (INCIDENT NO. 42035)
TABLE 2
UST SYSTEM INFORMATION
Capacity
(gallons)
Tank
Dimensions
Status
of
UST
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Construction
Details
Description of
Associated
Product Piping
and
Pumps
Date
Installed
Page 1 of 1
Well
No. PIN Well Owner Mailing Address Well Location Address Public Water
Connected
Well Use
(Potable/ Agriculture,
etc.)
Well
Depth
(ft BGS)
Type
of
Well
(Drilled/
Bored)
Well
Casing
Depth
(ft.
BGS)
Well
Screen
Interval
(x to y
ft. BGS)
Approximate
Distance
from
Source
Area of
Release (ft.)
WSW-1 966053433200 Marie B. Stillwell 6406 Cabin Branch Drive
Durham, NC 27712
5654 NC Highway 87 South
Sanford, NC 27332 No Active
Potable UK UK UK UK Onsite
WSW-2 966053210300 Eugene Laster Thomas 5740 NC Highway 87 South
Sanford, NC 27332
5680 NC Highway 87 South
Sanford, NC 27332 No Active
Potable UK UK UK UK ~420' SW
WSW-3 966052596500 Quinton Kelly & Irene
Thomas
5740 NC Highway 87 South
Sanford, NC 27332
5740 NC Highway 87 South
Sanford, NC 27332 No Active
Potable UK Bored UK UK ~450' S
WSW-4 966052666100 Eugene L. Thomas 5808 NC Highway 87 South
Sanford, NC 27332
5808 NC Highway 87 South
Sanford, NC 27332 No Active
Potable 85 Bored UK UK ~780' S
WSW-5 966052623500 Carson Cooper Winstead 125 Winstead Road
Sanford, NC 27332
108 Winstead Road
Sanford, NC 27332 No Active
Potable UK Bored UK UK ~1,230 S
WSW-6 966053765500 Escalante Carolina Trace
LLC
8108 Southpark Way
Littleton, CO 80120
5615 NC Highway 87 South
Sanford, NC 27332 No Active
Non-Potable UK UK UK UK ~390' NE
WSW-7 966054940100 Alyce M. Clark 10 Emory Point
Sanford, NC 27332
10 Emory Point
Sanford, NC 27332 No Active
Potable UK Bored UK UK ~450' NE
WSW-8 966054635400 Mona B. McNeill 5485 NC Highway 87 South
Sanford, NC 27332
5485 NC Highway 87 South
Sanford, NC 27332 No Active
Potable UK UK UK UK ~900 N
WSW-9 966054651300 John L. & Beverly M.
Leslie
5441 South Highway 87
Sanford, NC 27332
5441 South Highway 87
Sanford, NC 27332 No Active
Potable UK Bored UK UK ~1,170 N
WSW-10 966054229600 Daniel R. & Connie S.
Dinkins
5466 NC Highway 87 South
Sanford, NC 27332
5466 NC Highway 87 South
Sanford, NC 27332 No Active
Potable UK UK UK UK ~870' N
WSW-11 966044940000 Mark & Susan Smith 5368 NC Highway 87 South
Sanford, NC 27332
5368 NC Highway 87 South
Sanford, NC 27332 No Active
Potable UK UK UK UK ~1,180' NW
WSW-12 966054074800 Hazel C. Bullard 5360 NC Highway 87 South
Sanford, NC 27332
5360 NC Highway 87 South
Sanford, NC 27332 No Active
Potable UK UK UK UK ~1,400 NW
Notes:
• Water supply wells are shown on Figure 2
• Ft. BGS : Feet below ground surface
• UK: Unknown
TABLE 3
WATER SUPPLY WELL INFORMATION
J MART (INCIDENT NO. 42035)
Date: 07/07/17 Facility ID #: 0-0024866
Page 1 of 1
Date: 8/23/19 Facility ID #: 0-0024866
966053433200 (site)Marie B. Stillwell 6406 Cabin Branch Drive
Durham, NC 27712
966053062200 Kenneth L. Clark Sr.632 Barington Place
Matthews, NC 28105
966042292900 Eugene Laster Thomas 5740 Highway 87 South
Sanford, NC 27332
966053816500
966053765500
Note:
• Properties are keyed to Figure 2.
Escalante Carolina Trace LLC 8101 Southpark Way
Littleton, CO 80120
TABLE 4
ADJACENT PROPERTY OWNER INFORMATION
J MART (INCIDENT NO. 42035)
Pin Number Property Owner Name Mailing Address
Page 1 of 1
Date: 05/19/23
Well ID Date Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water from
Top of
Casing
(ft)
Free Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
Comments
03/13/17 29.12 ---70.88
01/24/18 27.96 ---72.04
08/14/19 20.79 ---79.21
05/26/20 20.05 ---79.95
10/27/20 20.36 ---79.64
06/29/21 17.54 ---82.46
01/25/22 22.56 ---77.44
07/28/22 21.81 ---78.19
12/20/22 24.39 ---75.61
05/08/23 19.61 ---80.39
05/04/17 22.96 ---78.04
01/24/18 28.73 ---72.27
08/14/19 21.34 ---79.66
05/26/20 20.69 ---80.31
10/27/20 20.94 ---80.06
06/29/21 18.01 ---82.99
01/25/22 22.14 ---78.86
07/28/22 22.46 ---78.54
12/20/22 25.01 ---75.99
05/08/23 21.22 ---79.78
05/04/17 21.25 ---78.63
01/24/18 26.74 ---73.14
08/14/19 19.47 ---80.41
05/26/20 17.98 ---81.90
10/27/20 19.12 ---80.76
05/18/21 16.48 ---83.40 Before AFVR
05/18/21 22.54 ---77.34 After AFVR
06/29/21 16.62 ---83.26
01/25/22 20.27 ---79.61
07/28/22 20.64 ---79.24
12/20/22 23.23 ---76.65
5/8/2023 19.60 ---80.28
05/04/17 23.42 ---76.44
01/24/18 29.33 ---70.53
08/14/19 22.00 ---77.86
05/26/20 20.86 ---79.00
10/27/20 21.24 ---78.62
05/18/21 18.12 ---81.74 Before AFVR
05/18/21 22.30 ---77.56 After AFVR
06/29/21 18.42 ---81.44
01/25/22 22.59 ---77.27
07/28/22 22.92 ---76.94
12/20/22 25.32 ---74.54
05/08/23 21.34 ---78.52
01/24/18 30.09 ---68.39
08/14/19 23.16 ---75.32
05/26/20 20.89 ---77.59
10/27/20 21.52 ---76.96
12/20/22 25.77 ---72.71
05/08/23 20.91 ---77.57
01/24/18 33.71 ---69.81
08/14/19 26.62 ---76.90
05/26/20 24.72 ---78.80
10/27/20 25.60 ---77.92
05/08/23 24.63 ---78.89
01/24/18 30.12 ---73.61
08/14/19 23.43 ---80.30
05/26/20 20.03 ---83.70
10/27/20 23.09 ---80.64
05/08/23 23.12 ---80.61
01/24/18 21.03 ---76.39
08/14/19 22.28 ---75.14
05/26/20 20.55 ---76.87
10/27/20 21.24 ---76.18
05/08/23 20.89 ---76.53
01/24/18 27.24 ---74.56
08/14/19 20.09 ---81.71
05/26/20 18.79 ---83.01
10/27/20 19.84 ---81.96
05/08/23 20.26 ---81.54
01/24/18 26.82 ---73.55
08/14/19 19.83 ---80.54
05/26/20 18.96 ---81.41
10/27/20 19.32 ---81.05
05/08/23 19.75 ---80.62
01/24/18 27.98 ---69.61
08/14/19 21.60 ---75.99
05/26/20 19.86 ---77.73
10/27/20 20.66 ---76.93
05/08/23 20.71 ---76.88
05/02/18 23.38 ---69.39
08/14/19 20.25 ---72.52
05/26/20 14.21 ---78.56
10/27/20 18.52 ---74.25
05/08/23 17.99 ---74.78
103.52
MW-7 12/12/17 20 20-40 40 103.73
MW-8
MW-9
12/12/17
01/23/18
20 20-40 40 97.42
20 20-40 40 101.80
100.004525-452503/13/17MW-1
101.004020-402004/26/17MW-2
99.884020-402004/27/17MW-3
99.864020-402004/26/17MW-4
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
J MART (INCIDENT NO. 42035)
Facility ID # : 0-0024866
MW-5 12/12/17 20 20-40 40 98.48
MW-6 12/12/17 20 20-40 40
MW-10 01/23/18
MW-11 01/23/18 20 20-40 40 97.59
20 20-40 40 92.77
20 20-40 40 100.37
MW-12 05/02/18
Page 1 of 2
Date: 05/19/23
Well ID Date Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water from
Top of
Casing
(ft)
Free Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
J MART (INCIDENT NO. 42035)
Facility ID # : 0-0024866
05/02/18 25.85 ---71.14
08/14/19 22.98 ---74.01
05/26/20 18.29 ---78.70
10/27/20 21.63 ---75.36
06/29/21 18.53 ---78.46
01/25/22 22.34 ---74.65
07/28/22 23.13 ---73.86
12/20/22 25.35 ---71.64
05/08/23 20.38 ---76.61
05/02/18 28.06 ---71.76
08/14/19 24.86 ---74.96
05/26/20 21.05 ---78.77
10/27/20 23.74 ---76.08
06/29/21 19.45 ---80.37
01/25/22 24.13 ---75.69
07/28/22 25.21 ---74.61
12/20/22 27.32 ---72.50
05/08/23 22.41 ---77.41
11/28/18 20.02 ---68.40
08/14/19 20.22 ---68.20
05/26/20 15.09 ---73.33
10/27/20 18.29 ---70.13
05/08/23 17.32 ---71.10
11/28/18 15.05 ---69.14
08/14/19 15.35 ---68.84
05/26/20 13.27 ---70.92
10/27/20 14.02 ---70.17
05/08/23 13.35 ---70.84
11/28/18 13.10 ---72.29
08/14/19 13.42 ---71.97
05/26/20 11.05 ---74.34
10/27/20 12.09 ---73.30
05/08/23 11.76 ---73.63
11/28/18 24.17 ---66.54
08/14/19 23.33 ---67.38
05/26/20 19.70 ---71.01
10/27/20 22.07 ---68.64
12/20/22 25.44 ---65.27
05/08/23 20.30 ---70.41
08/14/19 24.43 ---62.43
05/26/20 20.25 ---66.61
10/27/20 21.60 ---65.26
12/20/22 24.48 ---62.38
05/08/23 19.42 ---67.44
08/14/19 24.22 ---63.75
05/26/20 19.09 ---68.88
10/27/20 20.72 ---67.25
05/08/23 18.71 ---69.26
01/24/18 30.28 ---69.48
08/14/19 23.35 ---76.41
05/26/20 20.02 ---79.74
10/27/20 22.32 ---77.44
12/20/22 25.58 ---74.18
05/08/23 21.98 ---77.78
Notes:
96.994020-402005/02/18MW-13
MW-14 99.824020-402005/02/18
• NM: Not Measured.
• ft BGS : feet below ground surface.
• *: Reference point for elevation measurements, assumed elevation 100.00 ft.
15 15-35 35 88.42
15 15-35
87.97
15-35 35
10 10-25 25
MW-15 11/27/18
MW-16 11/27/18
MW-17 11/27/18
TW-1 01/23/18 55 55-60 60 99.76
35 84.19
15 15-35 35 90.71
85.39
10 10-25 25 86.86
MW-18 11/27/18
MW-19 08/14/19
MW-20 08/14/19
15
Page 2 of 2
Date: 05/19/23
EPA 504.1 SW846
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 400 400 40 10 0.02 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 70,000 26,100 28,500 24,100 40,000 10,000 50 15,000 NE NE NE
03/13/17 260 1,260 257 1,300 21.4 79.5 <1.3 13.4 2.4 J 63.1 413 106 NR NR 0.38 9.5 518 J 311 E 1,410
01/24/18 143 105 13.2 67.9 5.0 <0.13 <0.13 0.45 J 0.94 0.97 2.7 1.8 NR NR NR NR NR NR NR
08/14/19 442 181 96.2 492 138 19.7 2.2 J 3.9 J 8.4 13.5 105 32.0 NR NR NR NR NR NR NR
05/26/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
10/27/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
06/29/21 4,060 529 846 2,220 352 198 NR NR 40.4 J NR NR NR NR NR NR NR NR NR NR
01/25/22 1.4 <0.13 0.22 J <0.25 0.31 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
07/28/22 0.229 J <0.220 <0.170 <0.21 <0.140 <0.470 <0.150 <0.180 <0.500 <0.190 <0.190 <0.180 NR NR NR NR NR NR NR
12/20/22 0.22 J <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/08/23 1.7 2.4 1.1 7.2 0.23 J 0.25 J <0.13 <0.13 <0.13 <0.13 1.2 0.79 2.9 J <2.0 NR NR NR NR NR
05/04/17 0.73 0.54 <0.13 1.6 0.50 0.20 J <0.13 <0.13 <0.13 <0.13 <0.13 0.16 J NR NR 0.043 55.3 <35 <35 <35
01/24/18 0.14 J <0.13 <0.13 0.36 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
08/14/19 2.2 0.16 J <0.13 2.7 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 0.21 J 0.20 J NR NR NR NR NR NR NR
05/26/20 4.5 0.27 J <0.13 7.0 <0.13 <0.13 <0.13 0.15 J <0.13 0.20 J 0.54 0.39 J NR NR NR NR NR NR NR
10/27/20 7.6 0.25 J 0.21 J 11.6 <0.13 <0.13 <0.13 0.24 J <0.13 0.39 J 0.93 0.86 NR NR NR NR NR NR NR
06/29/21 0.28 J <0.13 <0.13 0.26 J <0.13 <0.13 NR NR <0.13 <0.13 NR NR NR NR NR NR NR NR NR
01/25/22 0.25 J <0.13 0.15 J 0.38 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
07/28/22 <0.180 <0.220 <0.170 <0.21 <0.140 <0.470 <0.150 <0.180 <0.500 <0.190 <0.190 <0.180 NR NR NR NR NR NR NR
12/20/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/08/23 0.67 0.51 0.22 J 1.4 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 0.17 J <0.13 <2.0 <2.0 NR NR NR NR NR
05/04/17 7,520 365 2,240 8,050 2,270 676 36.7 76.6 47.5 235 1,930 412 NR NR 1.8 16.3 9,490 3,560 6,540
01/24/18 4,220 92.9 539 1,630 1,310 373 24.1 J 63.3 31.8 J 106 557 121 NR NR NR NR NR NR NR
08/14/19 5,040 426 2,380 8,380 1,140 602 <25 79.8 J 29.9 J 255 2,000 499 NR NR NR NR NR NR NR
05/26/20 4,470 268 2,130 7,700 1,060 675 18.5 J 63.5 24.8 J 220 1,810 443 NR NR NR NR NR NR NR
10/27/20 4,370 307 2,300 9,520 920 682 16.7 J 64.2 23.5 J 221 1,930 476 NR NR NR NR NR NR NR
05/18/21 3,940 2,160 2,310 11,900 713 661 NR NR 19.1 J NR NR NR NR NR NR NR NR NR NR
06/29/21 3,110 2,100 1,600 7,030 645 541 NR NR 15.5 J NR NR NR NR NR NR NR NR NR NR
01/25/22 1,310 38.9 J 245 794 261 90.7 <13 20.7 J <13 30.7 J 234 63.9 NR NR NR NR NR NR NR
07/28/22 1,560 106 429 1,540 253 121 <1.50 31.7 7.33 69.2 466 136 NR NR NR NR NR NR NR
12/20/22 820 39.9 97.1 200 126 24.2 <3.1 13.2 4.5 J 19.2 40.3 13.7 NR NR NR NR NR NR NR
05/08/23 957 18.4 359 830 196 107 <1.3 23.3 6.5 47.6 255 85.7 515 198 NR NR NR NR NR
MAC (µg/l)
GCL (µg/l)
To
l
u
e
n
e
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
MT
B
E
Na
p
h
t
h
a
l
e
n
e
1,
2
-
D
i
c
h
l
o
r
o
e
t
h
a
n
e
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
EPA Method 6200B
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
J MART (INCIDENT NO. 42035)
Facility ID # : 0-0024866
Is
o
p
r
o
p
y
l
b
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n
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Di
-
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C9
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1
0

A
r
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a
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c
s
Xy
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e
n
e
s
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
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n
z
e
n
e
MADEP Method VPH Analytical Method 
Contaminant of Concern

Et
h
y
l
b
e
n
z
e
n
e
Le
a
d
C5
-
C
8

A
l
i
p
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a
t
i
c
s
C9
-
C
1
2

A
l
i
p
h
a
t
i
c
s
1,
2
-
D
i
b
r
o
m
o
e
t
h
a
n
e
(E
D
B
)
te
r
t
-
A
m
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l

a
l
c
o
h
o
l
(T
A
A
)
te
r
t
-
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u
t
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l

a
l
c
o
h
o
l
(T
B
A
)
MW-1
MW-2
MW-3
Page 1 of 6
Date: 05/19/23
EPA 504.1 SW846
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 400 400 40 10 0.02 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 70,000 26,100 28,500 24,100 40,000 10,000 50 15,000 NE NE NE
MAC (µg/l)
GCL (µg/l)
To
l
u
e
n
e
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
MT
B
E
Na
p
h
t
h
a
l
e
n
e
1,
2
-
D
i
c
h
l
o
r
o
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t
h
a
n
e
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
EPA Method 6200B
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
J MART (INCIDENT NO. 42035)
Facility ID # : 0-0024866
Is
o
p
r
o
p
y
l
b
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n
z
e
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Di
-
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0

A
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Xy
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s
1,
2
,
4
-
T
r
i
m
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t
h
y
l
b
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n
z
e
n
e
MADEP Method VPH Analytical Method 
Contaminant of Concern

Et
h
y
l
b
e
n
z
e
n
e
Le
a
d
C5
-
C
8

A
l
i
p
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a
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s
C9
-
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1
2

A
l
i
p
h
a
t
i
c
s
1,
2
-
D
i
b
r
o
m
o
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t
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a
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(E
D
B
)
te
r
t
-
A
m
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l

a
l
c
o
h
o
l
(T
A
A
)
te
r
t
-
B
u
t
y
l

a
l
c
o
h
o
l
(T
B
A
)
05/04/17 17,000 2,350 3,370 18,500 12,500 1,050 70.0 77.6 169 260 2,420 588 NR NR 39.1 74.4 25,800 5,980 7,650
01/24/18 17,200 895 2,340 8,850 19,100 941 90.2 88.7 277 260 1,900 571 NR NR NR NR NR NR NR
08/14/19 10,300 8,790 3,620 19,300 4,020 817 38.3 J 84.6 J 75.1 J 301 2,700 688 NR NR NR NR NR NR NR
05/26/20 8,690 15,600 3,630 19,800 2,150 713 <31 69.7 J 47.7 J 271 2,470 639 NR NR NR NR NR NR NR
10/27/20 9,780 21,900 4,230 22,900 2,120 607 <63 67.5 J <63 301 2,390 637 NR NR NR NR NR NR NR
05/18/21 7,820 25,000 3,640 21,200 1,240 844 NR NR <130 NR NR NR NR NR NR NR NR NR NR
06/29/21 8,650 20,100 3,730 20,100 3,340 792 NR NR 63.1 J NR NR NR NR NR NR NR NR NR NR
01/25/22 17,500 1,620 3,550 15,100 13,300 831 <130 <130 314 J 287 J 2,450 648 NR NR NR NR NR NR NR
07/28/22 16,500 3,830 3,930 17,500 11,100 1,090 <15.0 116 235 399 3,140 787 NR NR NR NR NR NR NR
12/20/22 15,700 646 2,770 9,120 9,530 682 78.5 J 79.9 J 265 274 2,140 535 NR NR NR NR NR NR NR
05/08/23 5,930 4,220 2,460 13,200 1,830 698 <25 57.0 J 53.5 J 204 1,820 476 5,010 <400 NR NR NR NR NR
01/24/18 10.5 <1.3 <1.3 <2.5 632 <1.3 <1.3 1.4 J 1.5 J <1.3 1.4 J <1.3 NR NR 0.19 56.4 <35 <35 49.9 J
08/14/19 <1.3 <1.3 <1.3 <2.5 245 <1.3 <1.3 <1.3 <1.3 <1.3 4.3 J 1.4 J NR NR NR NR NR NR NR
05/26/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
10/27/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
12/20/22 6.1 <0.13 <0.13 <0.25 382 0.38 J 0.26 J 0.64 1.2 0.15 J 1.1 <0.13 NR NR NR NR NR NR NR
05/08/23 <0.13 <0.13 <0.13 <0.25 1.8 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <2.0 NR NR NR NR NR
01/24/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR <0.010 177 <35 <35 <35
08/14/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/26/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
10/27/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/08/23 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <2.0 NR NR NR NR NR
01/24/18 <0.13 <0.13 <0.13 <0.26 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR <0.0098 22.8 <35 <35 <35
08/14/19 <0.13 <0.13 <0.13 <0.27 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/26/20 <0.13 <0.13 <0.13 <0.28 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
10/27/20 <0.13 <0.13 <0.13 <0.29 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/08/23 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <2.0 NR NR NR NR NR
01/24/18 <0.13 <0.13 <0.13 <0.25 6.0 <0.13 0.51 <0.13 0.31 J <0.13 <0.13 <0.13 NR NR <0.0099 146 <35 <35 <35
08/14/19 <0.13 0.13 J <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 0.80 0.35 J NR NR NR NR NR NR NR
05/26/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 0.16 J NR NR NR NR NR NR NR
10/27/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 1.0 0.49 J NR NR NR NR NR NR NR
05/08/23 0.47 J <0.13 0.20 J 0.60 J 0.54 <0.13 <0.13 <0.13 <0.13 <0.13 0.14 J <0.13 <2.0 8.7 J NR NR NR NR NR
MW-5
MW-4
MW-6
MW-7
MW-8
Page 2 of 6
Date: 05/19/23
EPA 504.1 SW846
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 400 400 40 10 0.02 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 70,000 26,100 28,500 24,100 40,000 10,000 50 15,000 NE NE NE
MAC (µg/l)
GCL (µg/l)
To
l
u
e
n
e
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
MT
B
E
Na
p
h
t
h
a
l
e
n
e
1,
2
-
D
i
c
h
l
o
r
o
e
t
h
a
n
e
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
EPA Method 6200B
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
J MART (INCIDENT NO. 42035)
Facility ID # : 0-0024866
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
Di
-
i
s
o
p
r
o
p
y
l

e
t
h
e
r
Be
n
z
e
n
e
C9
-
C
1
0

A
r
o
m
a
t
i
c
s
Xy
l
e
n
e
s
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
MADEP Method VPH Analytical Method 
Contaminant of Concern

Et
h
y
l
b
e
n
z
e
n
e
Le
a
d
C5
-
C
8

A
l
i
p
h
a
t
i
c
s
C9
-
C
1
2

A
l
i
p
h
a
t
i
c
s
1,
2
-
D
i
b
r
o
m
o
e
t
h
a
n
e
(E
D
B
)
te
r
t
-
A
m
y
l

a
l
c
o
h
o
l
(T
A
A
)
te
r
t
-
B
u
t
y
l

a
l
c
o
h
o
l
(T
B
A
)
01/24/18 0.36 J 1.2 0.24 J 0.85 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR <0.0095 529 52.9 J <35 <35
08/14/19 <0.13 0.20 J <0.13 <0.25 <0.13 0.29 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/26/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
10/27/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/08/23 0.19 J <0.13 <0.13 0.40 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <2.0 NR NR NR NR NR
01/24/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR 0.030 535 <35 <35 <35
08/14/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/26/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
10/27/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/08/23 0.16 J <0.13 0.13 J 0.36 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <2.0 NR NR NR NR NR
01/24/18 0.34 J 0.98 0.17 J 0.52 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR 0.20 267 <35 <35 <35
08/14/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/26/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
10/27/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/08/23 0.13 J <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <2.0 NR NR NR NR NR
05/02/18 2.2 1.1 0.45 J 3.9 570 21.1 6.2 23.3 12.3 3.2 1.4 <0.13 NR NR 0.038 NR <35 60.7 J 183
08/14/19 <0.13 <0.13 <0.13 <0.25 0.20 J <0.13 <0.13 0.91 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/26/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
10/27/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/08/23 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <2.0 NR NR NR NR NR
05/02/18 0.49 J <0.13 <0.13 <0.25 234 <0.13 <0.13 <0.13 0.42 J <0.13 <0.13 <0.13 NR NR 0.12 NR <35 <35 <35
08/14/19 <0.63 <0.63 <0.63 <1.3 172 <0.63 <0.63 <0.63 <0.63 <0.63 <0.63 <0.63 NR NR NR NR NR NR NR
05/26/20 <0.13 <0.13 <0.13 <0.25 16.7 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
10/27/20 <0.13 <0.13 <0.13 <0.25 33.2 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
06/29/21 <0.63 <0.63 <0.63 <1.3 135 <0.63 NR NR <0.63 NR NR NR NR NR NR NR NR NR NR
01/25/22 <3.1 <3.1 <3.1 <6.3 737 <3.1 <3.1 <3.1 <3.1 <3.1 <3.1 <3.1 NR NR NR NR NR NR NR
07/28/22 0.288 J <0.220 <0.170 0.889 J 543 <0.470 <0.150 <0.180 1.28 <0.190 0.227 J <0.180 NR NR NR NR NR NR NR
12/20/22 <0.13 <0.13 <0.13 <0.25 720 <0.13 <0.13 <0.13 1.6 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/08/23 <0.63 <0.63 <0.63 <1.3 198 <0.63 <0.63 <0.63 <0.63 <0.63 <0.63 <0.63 <10 <10 NR NR NR NR NR
MW-9
MW-10
MW-11
MW-12
MW-13
Page 3 of 6
Date: 05/19/23
EPA 504.1 SW846
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 400 400 40 10 0.02 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 70,000 26,100 28,500 24,100 40,000 10,000 50 15,000 NE NE NE
MAC (µg/l)
GCL (µg/l)
To
l
u
e
n
e
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
MT
B
E
Na
p
h
t
h
a
l
e
n
e
1,
2
-
D
i
c
h
l
o
r
o
e
t
h
a
n
e
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
EPA Method 6200B
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
J MART (INCIDENT NO. 42035)
Facility ID # : 0-0024866
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
Di
-
i
s
o
p
r
o
p
y
l

e
t
h
e
r
Be
n
z
e
n
e
C9
-
C
1
0

A
r
o
m
a
t
i
c
s
Xy
l
e
n
e
s
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
MADEP Method VPH Analytical Method 
Contaminant of Concern

Et
h
y
l
b
e
n
z
e
n
e
Le
a
d
C5
-
C
8

A
l
i
p
h
a
t
i
c
s
C9
-
C
1
2

A
l
i
p
h
a
t
i
c
s
1,
2
-
D
i
b
r
o
m
o
e
t
h
a
n
e
(E
D
B
)
te
r
t
-
A
m
y
l

a
l
c
o
h
o
l
(T
A
A
)
te
r
t
-
B
u
t
y
l

a
l
c
o
h
o
l
(T
B
A
)
05/02/18 <0.13 <0.13 <0.13 <0.25 14.9 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR <0.0093 NR <35 <35 <35
08/14/19 <0.13 <0.13 <0.13 <0.25 21.8 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/26/20 <0.13 <0.13 <0.13 <0.25 28.6 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
10/27/20 <0.13 0.16 J 0.16 J 0.84 J 33.0 <0.13 <0.13 <0.13 <0.13 <0.13 0.61 0.14 J NR NR NR NR NR NR NR
06/29/21 0.18 J 0.86 0.14 J 0.37 J 8.2 <0.13 NR NR <0.13 NR NR NR NR NR NR NR NR NR NR
01/25/22 <0.13 <0.13 <0.13 <0.25 8.5 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
07/28/22 0.738 0.354 J 0.434 J 2.04 5.24 <0.470 <0.150 <0.180 <0.500 <0.190 0.392 J <0.180 NR NR NR NR NR NR NR
12/20/22 <0.13 <0.13 <0.13 <0.25 1.3 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/08/23 <0.13 <0.13 <0.13 <0.25 2.9 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <2.0 NR NR NR NR NR
11/28/18 51.5 0.72 J <0.63 194 10.7 101 <0.63 18.2 0.69 J 2.6 21.1 <0.63 NR NR 0.10 NR 579 128 239
08/14/19 <0.13 <0.13 <0.13 <0.25 0.57 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/26/20 <0.13 <0.13 <0.13 <0.25 0.41 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
10/27/20 <0.13 <0.13 <0.13 <0.25 0.58 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/08/23 <0.13 <0.13 <0.13 <0.25 0.31 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <2.0 NR NR NR NR NR
11/28/18 <0.13 <0.13 <0.13 <0.25 1.5 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR <0.0092 NR <35 <35 <35
08/14/19 <0.13 <0.13 <0.13 <0.25 0.37 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/26/20 <0.13 <0.13 <0.13 <0.25 0.36 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
10/27/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/08/23 <0.13 <0.13 <0.13 <0.25 0.52 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <2.0 NR NR NR NR NR
11/28/18 <0.13 <0.13 <0.13 <0.25 0.39 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR <0.0092 NR <35 <35 <35
08/14/19 <0.13 <0.13 <0.13 <0.25 0.38 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/26/20 <0.13 <0.13 <0.13 <0.25 0.32 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
10/27/20 <0.13 <0.13 <0.13 <0.25 0.45 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/08/23 <0.13 <0.13 <0.13 <0.25 0.21 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <2.0 NR NR NR NR NR
11/28/18 30.5 <0.13 <0.13 30.6 288 3.8 <0.13 0.75 2.5 0.61 4.2 <0.13 NR NR 0.024 NR <35 <35 <35
08/14/19 <0.13 <0.13 <0.13 <0.25 77.3 <0.13 <0.13 <0.13 0.75 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/26/20 <0.13 <0.13 <0.13 <0.25 17.6 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
10/27/20 <0.13 <0.13 <0.13 <0.25 23.1 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
12/20/22 1.2 <0.13 <0.13 0.80 J 260 <0.13 <0.13 <0.13 1.4 <0.13 0.13 J <0.13 NR NR NR NR NR NR NR
05/08/23 <0.13 <0.13 <0.13 <0.25 37.3 <0.13 <0.13 <0.13 0.14 J <0.13 <0.13 <0.13 <2.0 <2.0 NR NR NR NR NR
MW-16
MW-17
MW-15
MW-14
MW-18
Page 4 of 6
Date: 05/19/23
EPA 504.1 SW846
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 400 400 40 10 0.02 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 70,000 26,100 28,500 24,100 40,000 10,000 50 15,000 NE NE NE
MAC (µg/l)
GCL (µg/l)
To
l
u
e
n
e
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
MT
B
E
Na
p
h
t
h
a
l
e
n
e
1,
2
-
D
i
c
h
l
o
r
o
e
t
h
a
n
e
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
EPA Method 6200B
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
J MART (INCIDENT NO. 42035)
Facility ID # : 0-0024866
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
Di
-
i
s
o
p
r
o
p
y
l

e
t
h
e
r
Be
n
z
e
n
e
C9
-
C
1
0

A
r
o
m
a
t
i
c
s
Xy
l
e
n
e
s
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
MADEP Method VPH Analytical Method 
Contaminant of Concern

Et
h
y
l
b
e
n
z
e
n
e
Le
a
d
C5
-
C
8

A
l
i
p
h
a
t
i
c
s
C9
-
C
1
2

A
l
i
p
h
a
t
i
c
s
1,
2
-
D
i
b
r
o
m
o
e
t
h
a
n
e
(E
D
B
)
te
r
t
-
A
m
y
l

a
l
c
o
h
o
l
(T
A
A
)
te
r
t
-
B
u
t
y
l

a
l
c
o
h
o
l
(T
B
A
)
08/14/19 0.14 J 0.17 J <0.13 <0.25 15.7 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/26/20 <0.13 <0.13 <0.13 <0.25 11.4 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
10/27/20 <0.13 <0.13 <0.13 <0.25 24.3 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
12/20/22 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/08/23 <0.13 <0.13 <0.13 <0.25 3.1 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <2.0 NR NR NR NR NR
08/14/19 <0.13 <0.13 <0.13 <0.25 31.7 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/26/20 <0.13 <0.13 <0.13 <0.25 13.5 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
10/27/20 <0.13 <0.13 <0.13 <0.25 15.7 <0.13 <0.13 <0.13 <0.13 <0.13 0.19 J <0.13 NR NR NR NR NR NR NR
05/08/23 <0.13 <0.13 <0.13 <0.25 82.1 <0.13 <0.13 <0.13 0.20 J <0.13 <0.13 <0.13 <2.0 <2.0 NR NR NR NR <35
01/24/18 20.5 1.1 0.40 J 5.3 28.2 4.1 0.35 J 0.43 J 0.61 0.21 J 1.1 <0.13 NR NR 0.019 <5.0 <35 <35 NR
08/14/19 <0.13 <0.13 <0.13 <0.25 8.7 <0.13 <0.13 <0.13 0.24 J <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/26/20 <0.13 <0.13 <0.13 <0.25 16.4 0.14 J 0.25 J <0.13 0.30 J <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
10/27/20 <0.13 <0.13 <0.13 <0.25 24.8 <0.13 0.25 J <0.13 0.87 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
12/20/22 493 <2.5 <2.5 <5.0 354 3.5 J 4.8 J 4.5 J 9.7 J <2.5 4.9 J <2.5 NR NR NR NR NR NR NR
05/08/23 168 <0.63 <0.13 <0.25 <0.13 <0.63 2.7 1.7 J 6.9 <0.63 1.6 J <0.63 815 176 NR NR NR NR <35
01/24/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR <0.0099 <5.0 <35 <35 NR
05/26/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
10/27/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
06/29/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR <0.13 NR NR NR NR NR NR NR NR NR NR
01/25/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
07/28/22 <0.180 <0.220 <0.170 <0.21 <0.140 <0.470 <0.150 <0.180 <0.500 <0.190 <0.190 <0.180 NR NR NR NR NR NR NR
12/20/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
05/08/23 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <2.0 NR NR NR NR NR
WSW-2 12/20/22 <0.13 <0.13 <0.13 <0.25 5.3 <0.13 <0.13 <0.13 0.20 J <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
MW-19
MW-20
TW-1
WSW-1
Page 5 of 6
Date: 05/19/23
EPA 504.1 SW846
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 400 400 40 10 0.02 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 70,000 26,100 28,500 24,100 40,000 10,000 50 15,000 NE NE NE
MAC (µg/l)
GCL (µg/l)
To
l
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1,
3
,
5
-
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MT
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EPA Method 6200B
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
J MART (INCIDENT NO. 42035)
Facility ID # : 0-0024866
Is
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4
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MADEP Method VPH Analytical Method 
Contaminant of Concern

Et
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Le
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C5
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8

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(E
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(T
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A
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-
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a
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(T
B
A
)
01/25/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
07/28/22 <0.180 <0.220 <0.170 <0.21 <0.140 <0.470 <0.150 <0.180 <0.500 <0.190 <0.190 <0.180 NR NR NR NR NR NR NR
05/08/23 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
Notes:
• Results reported in micrograms per liter (µg/l).
• < : Less than the method detection limit specified in the laboratory report.
• MAC: Maximum allowable concentrations as specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
• NE: Not Established.
• NR: Not Requested.
• A concentration of methylene chloride (6.5 J µg/l in MW-13) that exceeded the MAC was reported in the ground water sample collected on May 8, 2023.
• Concentrations in bold face type indicate the MACs were below the reported concentrations.
• Concentrations in italics indicate the GCLs were below the reported concentrations.
• For other compounds reported which did not exceed the MACs, refer to the laboratory reports.
Trip Blank
Page 6 of 6
Well No.
Sampled
Date
(mm/dd/
yy)
DO
(mg/L)pH Temp.Conductivity ORP Methane
(μg/L)
Nitrate
(μg/L)
Sulfate
(μg/L)
Ferrous
Iron
(μg/L)
MW-1 05/08/23 2.14 6.59 20.10 31 102.3 4.0 130 <2,000 7,500
MW-2 05/08/23 2.22 5.95 20.02 9 207.2 0.32 J 830 <2,000 550
MW-3 05/08/23 1.75 6.33 20.01 267 48.8 212 <100 <2,000 6,300
MW-4 05/08/23 2.08 6.38 19.88 254 6.1 141 <100 <2,000 11,200
MW-5 05/08/23 2.07 5.17 18.16 54 235.6 2.5 <100 2,000 <500
MW-9 05/08/23 2.15 5.40 18.46 104 88.3 <0.16 610 25,400 1,600
MW-10 05/08/23 2.02 5.71 19.46 62 138.8 0.29 J 570 <2,000 5,200
MW-13 05/08/23 2.04 5.33 16.51 51 241.4 <0.16 <100 <2,000 510
MW-14 05/08/23 1.87 5.36 17.21 69 234.3 4.5 <100 <2,000 <500
MW-15 05/08/23 2.04 5.57 17.96 89 210.2 <0.16 1,600 2,400 1,300
MW-18 05/08/23 1.84 5.79 17.26 61 210.6 <0.16 290 <2,000 <100
MW-19 05/08/23 1.90 5.17 16.83 40 244.6 <0.16 <100 <2,000 <100
MW-20 05/08/23 1.91 5.62 17.83 97 220.1 <0.16 680 <2,000 <500
Notes:
TABLE 6A
SUMMARY OF NATURAL ATTENUATION PARAMETER RESULTS
J Mart (INCIDENT NO. 42035)
Date: 05/19/23 Facility ID # : 00-0-000024866
• NR: Not requested.
• FP: Free Product.
• NS: Not sampled; Low sample volume prohibited parameters being collected.
• Analyses for nitrate and sulfate by Method SW846/9056; analyses for methane by Method RSK 175; analyses for ferrous iron by EPA Method SM
3500 Fe-D. Field measurements of dissolved oxygen, temperature, pH and ORP were collected during sampling using a field meter.
• <: Less than the method detection limit specified in the laboratory report.
• J: Estimated concentration.

APPENDICES

APPENDIX A
State Correspondence
4238 Received APR 26 2023

APPENDIX B
Laboratory Report – Ground Water Samples

05/19/23
Technical Report for
GRI (Geological Resources Inc.)
J Mart; 5654 NC Hwy 87 S, Sanford, NC
4238
SGS Job Number: FC5906
Sampling Date: 05/08/23
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]
ATTN: Joanna Alley
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, IL, UT, VT, WA, WI, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc.  4405 Vineland Road  Suite C-15  Orlando, FL 32811  tel: [phone]  fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Orlando, FL 05/19/23
e-Hardcopy 2.0
Automated Report
154
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 154
FC5906
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................4
Section 2: Summary of Hits ....................................................................................................6
Section 3: Sample Results ........................................................................................................11
3.1: FC5906-1: MW-1 ..........................................................................................................12
3.2: FC5906-2: TRIP BLANK .............................................................................................17
3.3: FC5906-3: MW-2 ..........................................................................................................19
3.4: FC5906-4: MW-3 ..........................................................................................................24
3.5: FC5906-5: MW-4 ..........................................................................................................29
3.6: FC5906-6: MW-9 ..........................................................................................................34
3.7: FC5906-7: MW-10 ........................................................................................................39
3.8: FC5906-8: TW-1 ...........................................................................................................44
3.9: FC5906-9: MW-11 ........................................................................................................46
3.10: FC5906-10: MW-8 ......................................................................................................49
3.11: FC5906-11: WSW-1 ....................................................................................................52
3.12: FC5906-12: MW-7 ......................................................................................................55
3.13: FC5906-13: MW-6 ......................................................................................................58
3.14: FC5906-14: MW-17 ....................................................................................................61
3.15: FC5906-15: MW-16 ....................................................................................................64
3.16: FC5906-16: MW-12 ....................................................................................................67
3.17: FC5906-17: MW-5 ......................................................................................................70
3.18: FC5906-18: MW-15 ....................................................................................................75
3.19: FC5906-19: MW-20 ....................................................................................................80
3.20: FC5906-20: MW-18 ....................................................................................................85
3.21: FC5906-21: MW-19 ....................................................................................................90
3.22: FC5906-22: MW-13 ....................................................................................................95
3.23: FC5906-23: MW-14 ....................................................................................................100
Section 4: Misc. Forms ............................................................................................................105
4.1: Chain of Custody ...........................................................................................................106
Section 5: MS Volatiles - QC Data Summaries .....................................................................109
5.1: Method Blank Summary ................................................................................................110
5.2: Blank Spike Summary ...................................................................................................119
5.3: Matrix Spike Summary ..................................................................................................128
5.4: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................131
Section 6: GC Volatiles - QC Data Summaries .....................................................................137
6.1: Method Blank Summary ................................................................................................138
6.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................141
6.3: Matrix Spike Summary ..................................................................................................144
6.4: Duplicate Summary .......................................................................................................147
Section 7: General Chemistry - QC Data Summaries ..........................................................150
7.1: Method Blank and Spike Results Summary ..................................................................151
7.2: Duplicate Results Summary ..........................................................................................152
7.3: Matrix Spike Results Summary .....................................................................................153
1
2
3
4
5
6
7
2 of 154
FC5906
Table of Contents
-2-
Sections:
7.4: Matrix Spike Duplicate Results Summary ....................................................................154
1
2
3
4
5
6
7
3 of 154
FC5906
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FC5906
J Mart; 5654 NC Hwy 87 S, Sanford, NC
Project No: 4238
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FC5906-1 05/08/23 09:22 JB 05/09/23 AQ Ground Water MW-1
FC5906-2 05/08/23 07:53 JB 05/09/23 AQ Trip Blank Water TRIP BLANK
FC5906-3 05/08/23 09:42 JB 05/09/23 AQ Ground Water MW-2
FC5906-4 05/08/23 10:05 JB 05/09/23 AQ Ground Water MW-3
FC5906-5 05/08/23 10:26 JB 05/09/23 AQ Ground Water MW-4
FC5906-6 05/08/23 10:44 JB 05/09/23 AQ Ground Water MW-9
FC5906-7 05/08/23 11:03 JB 05/09/23 AQ Ground Water MW-10
FC5906-8 05/08/23 11:19 JB 05/09/23 AQ Ground Water TW-1
FC5906-9 05/08/23 11:33 JB 05/09/23 AQ Ground Water MW-11
FC5906-10 05/08/23 11:45 JB 05/09/23 AQ Ground Water MW-8
FC5906-11 05/08/23 11:52 JB 05/09/23 AQ Ground Water WSW-1
FC5906-12 05/08/23 12:10 JB 05/09/23 AQ Ground Water MW-7
4 of 154
FC5906
1
SGS North America Inc.
Sample Summary
(continued)
GRI (Geological Resources Inc.)
Job No:FC5906
J Mart; 5654 NC Hwy 87 S, Sanford, NC
Project No: 4238
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FC5906-13 05/08/23 12:27 JB 05/09/23 AQ Ground Water MW-6
FC5906-14 05/08/23 12:42 JB 05/09/23 AQ Ground Water MW-17
FC5906-15 05/08/23 12:56 JB 05/09/23 AQ Ground Water MW-16
FC5906-16 05/08/23 13:09 JB 05/09/23 AQ Ground Water MW-12
FC5906-17 05/08/23 13:28 JB 05/09/23 AQ Ground Water MW-5
FC5906-18 05/08/23 13:46 JB 05/09/23 AQ Ground Water MW-15
FC5906-19 05/08/23 14:02 JB 05/09/23 AQ Ground Water MW-20
FC5906-20 05/08/23 14:21 JB 05/09/23 AQ Ground Water MW-18
FC5906-21 05/08/23 14:39 JB 05/09/23 AQ Ground Water MW-19
FC5906-22 05/08/23 14:57 JB 05/09/23 AQ Ground Water MW-13
FC5906-23 05/08/23 15:12 JB 05/09/23 AQ Ground Water MW-14
5 of 154
FC5906
1
Summary of Hits Page 1 of 5
Job Number:FC5906
Account:GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Collected:05/08/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FC5906-1 MW-1
Benzene 1.7 0.50 0.13 ug/l SM 6200B
Ethylbenzene 1.1 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 0.23 J 0.50 0.13 ug/l SM 6200B
Naphthalene 0.25 J 0.50 0.13 ug/l SM 6200B
Tert-Amyl Alcohol 2.9 J 10 2.0 ug/l SM 6200B
Toluene 2.4 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 1.2 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.79 0.50 0.13 ug/l SM 6200B
m,p-Xylene 4.3 1.0 0.13 ug/l SM 6200B
o-Xylene 2.9 0.50 0.13 ug/l SM 6200B
Xylene (total)7.2 1.5 0.25 ug/l SM 6200B
Methane 4.0 0.50 0.16 ug/l RSKSOP-147/175
Iron, Ferrous a 7.5 1.0 mg/l SM3500FE B-11
Nitrogen, Nitrate 0.13 0.10 mg/l EPA 300/SW846 9056A
FC5906-2 TRIP BLANK
Methyl Chloride 0.20 J 0.50 0.20 ug/l SM 6200B
FC5906-3 MW-2
Benzene 0.67 0.50 0.13 ug/l SM 6200B
Ethylbenzene 0.22 J 0.50 0.13 ug/l SM 6200B
Toluene 0.51 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.17 J 0.50 0.13 ug/l SM 6200B
m,p-Xylene 0.87 J 1.0 0.13 ug/l SM 6200B
o-Xylene 0.56 0.50 0.13 ug/l SM 6200B
Xylene (total)1.4 J 1.5 0.25 ug/l SM 6200B
Methane 0.32 J 0.50 0.16 ug/l RSKSOP-147/175
Iron, Ferrous a 0.55 0.50 mg/l SM3500FE B-11
Nitrogen, Nitrate 0.83 0.10 mg/l EPA 300/SW846 9056A
FC5906-4 MW-3
Benzene 957 5.0 1.3 ug/l SM 6200B
n-Butylbenzene 8.6 5.0 1.3 ug/l SM 6200B
sec-Butylbenzene 5.3 5.0 1.3 ug/l SM 6200B
Di-Isopropyl Ether 6.5 5.0 1.3 ug/l SM 6200B
Ethylbenzene 359 5.0 1.3 ug/l SM 6200B
Isopropylbenzene 23.3 5.0 1.3 ug/l SM 6200B
p-Isopropyltoluene 2.7 J 5.0 1.3 ug/l SM 6200B
Methyl Tert Butyl Ether 196 5.0 1.3 ug/l SM 6200B
Naphthalene 107 5.0 1.3 ug/l SM 6200B
6 of 154
FC5906
2
Summary of Hits Page 2 of 5
Job Number:FC5906
Account:GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Collected:05/08/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
n-Propylbenzene 47.6 5.0 1.3 ug/l SM 6200B
Tert-Amyl Alcohol 515 100 20 ug/l SM 6200B
Tert-Butyl Alcohol 198 100 20 ug/l SM 6200B
Toluene 18.4 5.0 1.3 ug/l SM 6200B
1,2,4-Trimethylbenzene 255 5.0 1.3 ug/l SM 6200B
1,3,5-Trimethylbenzene 85.7 5.0 1.3 ug/l SM 6200B
m,p-Xylene 730 10 1.3 ug/l SM 6200B
o-Xylene 100 5.0 1.3 ug/l SM 6200B
Xylene (total)830 15 2.5 ug/l SM 6200B
Methane 212 0.50 0.16 ug/l RSKSOP-147/175
Iron, Ferrous a 6.3 2.5 mg/l SM3500FE B-11
FC5906-5 MW-4
Benzene 5930 100 25 ug/l SM 6200B
Di-Isopropyl Ether 53.5 J 100 25 ug/l SM 6200B
Ethylbenzene 2460 100 25 ug/l SM 6200B
Isopropylbenzene 57.0 J 100 25 ug/l SM 6200B
Methyl Tert Butyl Ether 1830 100 25 ug/l SM 6200B
Naphthalene 698 100 25 ug/l SM 6200B
n-Propylbenzene 204 100 25 ug/l SM 6200B
Tert-Amyl Alcohol 5010 2000 400 ug/l SM 6200B
Toluene 4220 100 25 ug/l SM 6200B
1,2,4-Trimethylbenzene 1820 100 25 ug/l SM 6200B
1,3,5-Trimethylbenzene 476 100 25 ug/l SM 6200B
m,p-Xylene 8660 200 25 ug/l SM 6200B
o-Xylene 4510 100 25 ug/l SM 6200B
Xylene (total)13200 300 50 ug/l SM 6200B
Methane 141 0.50 0.16 ug/l RSKSOP-147/175
Iron, Ferrous a 11.2 2.5 mg/l SM3500FE B-11
FC5906-6 MW-9
Benzene 0.19 J 0.50 0.13 ug/l SM 6200B
m,p-Xylene 0.40 J 1.0 0.13 ug/l SM 6200B
Iron, Ferrous a 1.6 1.0 mg/l SM3500FE B-11
Nitrogen, Nitrate 0.61 0.10 mg/l EPA 300/SW846 9056A
Sulfate 25.4 2.0 mg/l EPA 300/SW846 9056A
FC5906-7 MW-10
Benzene 0.16 J 0.50 0.13 ug/l SM 6200B
Ethylbenzene 0.13 J 0.50 0.13 ug/l SM 6200B
m,p-Xylene 0.36 J 1.0 0.13 ug/l SM 6200B
Methane 0.29 J 0.50 0.16 ug/l RSKSOP-147/175
7 of 154
FC5906
2
Summary of Hits Page 3 of 5
Job Number:FC5906
Account:GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Collected:05/08/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Iron, Ferrous a 5.2 1.0 mg/l SM3500FE B-11
Nitrogen, Nitrate 0.57 0.10 mg/l EPA 300/SW846 9056A
FC5906-8 TW-1
Benzene 168 2.5 0.63 ug/l SM 6200B
1,2-Dichloroethane 2.7 2.5 0.63 ug/l SM 6200B
Di-Isopropyl Ether 6.9 2.5 0.63 ug/l SM 6200B
Isopropylbenzene 1.7 J 2.5 0.63 ug/l SM 6200B
Tert-Amyl Alcohol 815 50 10 ug/l SM 6200B
Tert-Amyl Methyl Ether 2.1 J 5.0 1.0 ug/l SM 6200B
Tert-Butyl Alcohol b 176 50 10 ug/l SM 6200B
1,2,4-Trimethylbenzene 1.6 J 2.5 0.63 ug/l SM 6200B
FC5906-9 MW-11
Benzene 0.13 J 0.50 0.13 ug/l SM 6200B
FC5906-10 MW-8
Benzene 0.47 J 0.50 0.13 ug/l SM 6200B
Ethylbenzene 0.20 J 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 0.54 0.50 0.13 ug/l SM 6200B
Tert-Butyl Alcohol 8.7 J 10 2.0 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.14 J 0.50 0.13 ug/l SM 6200B
m,p-Xylene 0.60 J 1.0 0.13 ug/l SM 6200B
FC5906-11 WSW-1
No hits reported in this sample.
FC5906-12 MW-7
Chloroform 0.19 J 0.50 0.13 ug/l SM 6200B
FC5906-13 MW-6
Chloroform 7.1 0.50 0.13 ug/l SM 6200B
FC5906-14 MW-17
Methyl Tert Butyl Ether 0.21 J 0.50 0.13 ug/l SM 6200B
8 of 154
FC5906
2
Summary of Hits Page 4 of 5
Job Number:FC5906
Account:GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Collected:05/08/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FC5906-15 MW-16
Methyl Tert Butyl Ether 0.52 0.50 0.13 ug/l SM 6200B
FC5906-16 MW-12
No hits reported in this sample.
FC5906-17 MW-5
Methyl Tert Butyl Ether 1.8 0.50 0.13 ug/l SM 6200B
Methane 2.5 0.50 0.16 ug/l RSKSOP-147/175
Sulfate 2.0 2.0 mg/l EPA 300/SW846 9056A
FC5906-18 MW-15
Methyl Tert Butyl Ether 0.31 J 0.50 0.13 ug/l SM 6200B
Iron, Ferrous a 1.3 1.0 mg/l SM3500FE B-11
Nitrogen, Nitrate 1.6 0.10 mg/l EPA 300/SW846 9056A
Sulfate 2.4 2.0 mg/l EPA 300/SW846 9056A
FC5906-19 MW-20
Di-Isopropyl Ether 0.20 J 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 82.1 0.50 0.13 ug/l SM 6200B
Nitrogen, Nitrate 0.68 0.10 mg/l EPA 300/SW846 9056A
FC5906-20 MW-18
Di-Isopropyl Ether 0.14 J 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 37.3 0.50 0.13 ug/l SM 6200B
Nitrogen, Nitrate 0.29 0.10 mg/l EPA 300/SW846 9056A
FC5906-21 MW-19
Methyl Tert Butyl Ether 3.1 0.50 0.13 ug/l SM 6200B
FC5906-22 MW-13
Methylene Chloride 6.5 J 10 5.0 ug/l SM 6200B
Methyl Tert Butyl Ether 198 2.5 0.63 ug/l SM 6200B
Iron, Ferrous a 0.51 0.50 mg/l SM3500FE B-11
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Summary of Hits Page 5 of 5
Job Number:FC5906
Account:GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Collected:05/08/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FC5906-23 MW-14
Chloroform 0.87 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 2.9 0.50 0.13 ug/l SM 6200B
Methane 4.5 0.50 0.16 ug/l RSKSOP-147/175
(a) Field analysis required. Received out of hold time and analyzed by request.
(b) Associated ECV outside of control limits high. No sample available for re-analysis.
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Sample Results
Report of Analysis
Orlando, FL
Section 3
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Report of Analysis Page 1 of 3
Client Sample ID:MW-1
Lab Sample ID:FC5906-1 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1077.D 1 05/11/23 15:59 TD n/a n/a V3A53
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1.7 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-1
Lab Sample ID:FC5906-1 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene 1.1 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.23 0.50 0.13 ug/l J
91-20-3 Naphthalene 0.25 0.50 0.13 ug/l J
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol 2.9 10 2.0 ug/l J
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol a ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate a ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 2.4 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 1.2 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.79 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 4.3 1.0 0.13 ug/l
95-47-6 o-Xylene 2.9 0.50 0.13 ug/l
1330-20-7 Xylene (total)7.2 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-1
Lab Sample ID:FC5906-1 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-1
Lab Sample ID:FC5906-1 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:RSKSOP-147/175 Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL82408.D 1 05/15/23 15:49 SS n/a n/a GLL2863
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 24 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane 4.0 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-1
Lab Sample ID:FC5906-1 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a 7.5 1.0 mg/l 10 05/10/23 10:40 ST SM3500FE B-11
Nitrogen, Nitrate 0.13 0.10 mg/l 1 05/09/23 15:55 JB EPA 300/SW846 9056A
Sulfate <2.0 2.0 mg/l 1 05/09/23 15:55 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
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Report of Analysis Page 1 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FC5906-2 Date Sampled:05/08/23
Matrix:AQ - Trip Blank Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1090.D 1 05/12/23 11:35 TD n/a n/a V3A54
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FC5906-2 Date Sampled:05/08/23
Matrix:AQ - Trip Blank Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride 0.20 0.50 0.20 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 102%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
(a) Associated BS recovery outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:MW-2
Lab Sample ID:FC5906-3 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E112363.D 1 05/12/23 12:01 TD n/a n/a VE2709
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.67 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-2
Lab Sample ID:FC5906-3 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene 0.22 0.50 0.13 ug/l J
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride b ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate c ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 0.51 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane b ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.17 0.50 0.13 ug/l J
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 0.87 1.0 0.13 ug/l J
95-47-6 o-Xylene 0.56 0.50 0.13 ug/l
1330-20-7 Xylene (total)1.4 1.5 0.25 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-2
Lab Sample ID:FC5906-3 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 92%70-130%
460-00-4 4-Bromofluorobenzene 93%70-130%
(a) Associated ICV, CCV, and BS recovery outside control limits high, sample ND.
(b) Associated CCV and BS outside control limits high, sample is ND.
(c) Associated BS recovery outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-2
Lab Sample ID:FC5906-3 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:RSKSOP-147/175 Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL82409.D 1 05/15/23 15:58 SS n/a n/a GLL2863
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 24 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane 0.32 0.50 0.16 ug/l J
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-2
Lab Sample ID:FC5906-3 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a 0.55 0.50 mg/l 5 05/10/23 10:40 ST SM3500FE B-11
Nitrogen, Nitrate 0.83 0.10 mg/l 1 05/09/23 17:01 JB EPA 300/SW846 9056A
Sulfate <2.0 2.0 mg/l 1 05/09/23 17:01 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
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Client Sample ID:MW-3
Lab Sample ID:FC5906-4 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E112371.D 10 05/12/23 15:39 TD n/a n/a VE2709
Run #2 3A1073.D 50 05/11/23 14:21 TD n/a n/a V3A53
Purge Volume
Run #1 5.0 ml
Run #2 5.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 957 5.0 1.3 ug/l
108-86-1 Bromobenzene ND 5.0 1.3 ug/l
74-97-5 Bromochloromethane ND 5.0 1.3 ug/l
75-27-4 Bromodichloromethane ND 5.0 1.3 ug/l
75-25-2 Bromoform ND 5.0 1.3 ug/l
104-51-8 n-Butylbenzene 8.6 5.0 1.3 ug/l
135-98-8 sec-Butylbenzene 5.3 5.0 1.3 ug/l
98-06-6 tert-Butylbenzene ND 5.0 1.3 ug/l
56-23-5 Carbon Tetrachloride ND 5.0 1.3 ug/l
108-90-7 Chlorobenzene ND 5.0 1.3 ug/l
75-00-3 Chloroethane ND 5.0 2.0 ug/l
67-66-3 Chloroform ND 5.0 1.3 ug/l
95-49-8 o-Chlorotoluene ND 5.0 1.3 ug/l
106-43-4 p-Chlorotoluene ND 5.0 1.3 ug/l
124-48-1 Dibromochloromethane ND 5.0 1.3 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 2.5 ug/l
106-93-4 1,2-Dibromoethane ND 5.0 1.3 ug/l
75-71-8 Dichlorodifluoromethane a ND 5.0 2.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 5.0 1.3 ug/l
541-73-1 1,3-Dichlorobenzene ND 5.0 1.3 ug/l
106-46-7 1,4-Dichlorobenzene ND 5.0 1.3 ug/l
75-34-3 1,1-Dichloroethane ND 5.0 1.3 ug/l
107-06-2 1,2-Dichloroethane ND 5.0 1.3 ug/l
75-35-4 1,1-Dichloroethylene ND 5.0 1.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.3 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.3 ug/l
78-87-5 1,2-Dichloropropane ND 5.0 1.3 ug/l
142-28-9 1,3-Dichloropropane ND 5.0 1.3 ug/l
594-20-7 2,2-Dichloropropane ND 5.0 1.3 ug/l
563-58-6 1,1-Dichloropropene ND 5.0 1.3 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-3
Lab Sample ID:FC5906-4 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 6.5 5.0 1.3 ug/l
100-41-4 Ethylbenzene 359 5.0 1.3 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 5.0 1.3 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 1.3 ug/l
98-82-8 Isopropylbenzene 23.3 5.0 1.3 ug/l
99-87-6 p-Isopropyltoluene 2.7 5.0 1.3 ug/l J
74-83-9 Methyl Bromide ND 5.0 2.0 ug/l
74-87-3 Methyl Chloride b ND 5.0 2.0 ug/l
74-95-3 Methylene Bromide ND 5.0 1.3 ug/l
75-09-2 Methylene Chloride ND 20 10 ug/l
1634-04-4 Methyl Tert Butyl Ether 196 5.0 1.3 ug/l
91-20-3 Naphthalene 107 5.0 1.3 ug/l
103-65-1 n-Propylbenzene 47.6 5.0 1.3 ug/l
100-42-5 Styrene ND 5.0 1.3 ug/l
75-85-4 Tert-Amyl Alcohol 515 100 20 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 10 2.0 ug/l
75-65-0 Tert-Butyl Alcohol 198 100 20 ug/l
762-75-4 Tert-Butyl Formate c ND 100 20 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.3 ug/l
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/l
108-88-3 Toluene 18.4 5.0 1.3 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.3 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 5.0 1.3 ug/l
79-00-5 1,1,2-Trichloroethane ND 5.0 1.3 ug/l
79-01-6 Trichloroethylene ND 5.0 1.3 ug/l
75-69-4 Trichlorofluoromethane b ND 5.0 2.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/l
95-63-6 1,2,4-Trimethylbenzene 255 5.0 1.3 ug/l
108-67-8 1,3,5-Trimethylbenzene 85.7 5.0 1.3 ug/l
75-01-4 Vinyl Chloride ND 5.0 1.3 ug/l
m,p-Xylene 730 10 1.3 ug/l
95-47-6 o-Xylene 100 5.0 1.3 ug/l
1330-20-7 Xylene (total)830 15 2.5 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 111%106%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-3
Lab Sample ID:FC5906-4 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 91%100%70-130%
460-00-4 4-Bromofluorobenzene 90%96%70-130%
(a) Associated ICV, CCV, and BS recovery outside control limits high, sample ND.
(b) Associated CCV and BS outside control limits high, sample is ND.
(c) Associated BS recovery outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-3
Lab Sample ID:FC5906-4 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:RSKSOP-147/175 Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL82410.D 1 05/15/23 16:05 SS n/a n/a GLL2863
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 24 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane 212 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-3
Lab Sample ID:FC5906-4 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a 6.3 2.5 mg/l 25 05/10/23 10:40 ST SM3500FE B-11
Nitrogen, Nitrate <0.10 0.10 mg/l 1 05/09/23 17:23 JB EPA 300/SW846 9056A
Sulfate <2.0 2.0 mg/l 1 05/09/23 17:23 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
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Report of Analysis Page 1 of 3
Client Sample ID:MW-4
Lab Sample ID:FC5906-5 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1074.D 200 05/11/23 14:46 TD n/a n/a V3A53
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 5930 100 25 ug/l
108-86-1 Bromobenzene ND 100 25 ug/l
74-97-5 Bromochloromethane ND 100 25 ug/l
75-27-4 Bromodichloromethane ND 100 25 ug/l
75-25-2 Bromoform ND 100 25 ug/l
104-51-8 n-Butylbenzene ND 100 25 ug/l
135-98-8 sec-Butylbenzene ND 100 25 ug/l
98-06-6 tert-Butylbenzene ND 100 25 ug/l
56-23-5 Carbon Tetrachloride ND 100 25 ug/l
108-90-7 Chlorobenzene ND 100 25 ug/l
75-00-3 Chloroethane ND 100 40 ug/l
67-66-3 Chloroform ND 100 25 ug/l
95-49-8 o-Chlorotoluene ND 100 25 ug/l
106-43-4 p-Chlorotoluene ND 100 25 ug/l
124-48-1 Dibromochloromethane ND 100 25 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 100 49 ug/l
106-93-4 1,2-Dibromoethane ND 100 25 ug/l
75-71-8 Dichlorodifluoromethane ND 100 40 ug/l
95-50-1 1,2-Dichlorobenzene ND 100 25 ug/l
541-73-1 1,3-Dichlorobenzene ND 100 25 ug/l
106-46-7 1,4-Dichlorobenzene ND 100 25 ug/l
75-34-3 1,1-Dichloroethane ND 100 25 ug/l
107-06-2 1,2-Dichloroethane ND 100 25 ug/l
75-35-4 1,1-Dichloroethylene ND 100 25 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 100 25 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 100 25 ug/l
78-87-5 1,2-Dichloropropane ND 100 25 ug/l
142-28-9 1,3-Dichloropropane ND 100 25 ug/l
594-20-7 2,2-Dichloropropane ND 100 25 ug/l
563-58-6 1,1-Dichloropropene ND 100 25 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 100 25 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 100 25 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-4
Lab Sample ID:FC5906-5 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 53.5 100 25 ug/l J
100-41-4 Ethylbenzene 2460 100 25 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 100 25 ug/l
87-68-3 Hexachlorobutadiene ND 100 25 ug/l
98-82-8 Isopropylbenzene 57.0 100 25 ug/l J
99-87-6 p-Isopropyltoluene ND 100 25 ug/l
74-83-9 Methyl Bromide ND 100 40 ug/l
74-87-3 Methyl Chloride ND 100 40 ug/l
74-95-3 Methylene Bromide ND 100 25 ug/l
75-09-2 Methylene Chloride ND 400 200 ug/l
1634-04-4 Methyl Tert Butyl Ether 1830 100 25 ug/l
91-20-3 Naphthalene 698 100 25 ug/l
103-65-1 n-Propylbenzene 204 100 25 ug/l
100-42-5 Styrene ND 100 25 ug/l
75-85-4 Tert-Amyl Alcohol 5010 2000 400 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 200 40 ug/l
75-65-0 Tert-Butyl Alcohol a ND 2000 400 ug/l
762-75-4 Tert-Butyl Formate a ND 2000 400 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 100 25 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 100 25 ug/l
127-18-4 Tetrachloroethylene ND 100 25 ug/l
108-88-3 Toluene 4220 100 25 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 100 25 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 100 25 ug/l
71-55-6 1,1,1-Trichloroethane ND 100 25 ug/l
79-00-5 1,1,2-Trichloroethane ND 100 25 ug/l
79-01-6 Trichloroethylene ND 100 25 ug/l
75-69-4 Trichlorofluoromethane ND 100 40 ug/l
96-18-4 1,2,3-Trichloropropane ND 100 25 ug/l
95-63-6 1,2,4-Trimethylbenzene 1820 100 25 ug/l
108-67-8 1,3,5-Trimethylbenzene 476 100 25 ug/l
75-01-4 Vinyl Chloride ND 100 25 ug/l
m,p-Xylene 8660 200 25 ug/l
95-47-6 o-Xylene 4510 100 25 ug/l
1330-20-7 Xylene (total)13200 300 50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-4
Lab Sample ID:FC5906-5 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-4
Lab Sample ID:FC5906-5 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:RSKSOP-147/175 Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL82422.D 1 05/16/23 10:34 SS n/a n/a GLL2864
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 24 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane 141 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-4
Lab Sample ID:FC5906-5 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a 11.2 2.5 mg/l 25 05/10/23 10:40 ST SM3500FE B-11
Nitrogen, Nitrate <0.10 0.10 mg/l 1 05/09/23 17:45 JB EPA 300/SW846 9056A
Sulfate <2.0 2.0 mg/l 1 05/09/23 17:45 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
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Report of Analysis Page 1 of 3
Client Sample ID:MW-9
Lab Sample ID:FC5906-6 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E112364.D 1 05/12/23 12:28 TD n/a n/a VE2709
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.19 0.50 0.13 ug/l J
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-9
Lab Sample ID:FC5906-6 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride b ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate c ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane b ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 0.40 1.0 0.13 ug/l J
95-47-6 o-Xylene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 92%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-9
Lab Sample ID:FC5906-6 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 91%70-130%
(a) Associated ICV, CCV, and BS recovery outside control limits high, sample ND.
(b) Associated CCV and BS outside control limits high, sample is ND.
(c) Associated BS recovery outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-9
Lab Sample ID:FC5906-6 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:RSKSOP-147/175 Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL82451.D 1 05/18/23 08:44 JR n/a n/a GLL2865
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 22 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane ND 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-9
Lab Sample ID:FC5906-6 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a 1.6 1.0 mg/l 10 05/10/23 10:40 ST SM3500FE B-11
Nitrogen, Nitrate 0.61 0.10 mg/l 1 05/09/23 18:07 JB EPA 300/SW846 9056A
Sulfate 25.4 2.0 mg/l 1 05/09/23 18:07 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
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Client Sample ID:MW-10
Lab Sample ID:FC5906-7 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E112365.D 1 05/12/23 12:55 TD n/a n/a VE2709
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.16 0.50 0.13 ug/l J
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-10
Lab Sample ID:FC5906-7 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene 0.13 0.50 0.13 ug/l J
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride b ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate c ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane b ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 0.36 1.0 0.13 ug/l J
95-47-6 o-Xylene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
2037-26-5 Toluene-D8 92%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-10
Lab Sample ID:FC5906-7 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 92%70-130%
(a) Associated ICV, CCV, and BS recovery outside control limits high, sample ND.
(b) Associated CCV and BS outside control limits high, sample is ND.
(c) Associated BS recovery outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-10
Lab Sample ID:FC5906-7 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:RSKSOP-147/175 Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL82424.D 1 05/16/23 10:49 SS n/a n/a GLL2864
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 24 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane 0.29 0.50 0.16 ug/l J
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-10
Lab Sample ID:FC5906-7 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a 5.2 1.0 mg/l 10 05/10/23 10:40 ST SM3500FE B-11
Nitrogen, Nitrate 0.57 0.10 mg/l 1 05/09/23 18:29 JB EPA 300/SW846 9056A
Sulfate <2.0 2.0 mg/l 1 05/09/23 18:29 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
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Report of Analysis Page 1 of 2
Client Sample ID:TW-1
Lab Sample ID:FC5906-8 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1079.D 5 05/11/23 16:48 TD n/a n/a V3A53
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 168 2.5 0.63 ug/l
108-86-1 Bromobenzene ND 2.5 0.63 ug/l
74-97-5 Bromochloromethane ND 2.5 0.63 ug/l
75-27-4 Bromodichloromethane ND 2.5 0.63 ug/l
75-25-2 Bromoform ND 2.5 0.63 ug/l
104-51-8 n-Butylbenzene ND 2.5 0.63 ug/l
135-98-8 sec-Butylbenzene ND 2.5 0.63 ug/l
98-06-6 tert-Butylbenzene ND 2.5 0.63 ug/l
56-23-5 Carbon Tetrachloride ND 2.5 0.63 ug/l
108-90-7 Chlorobenzene ND 2.5 0.63 ug/l
75-00-3 Chloroethane ND 2.5 1.0 ug/l
67-66-3 Chloroform ND 2.5 0.63 ug/l
95-49-8 o-Chlorotoluene ND 2.5 0.63 ug/l
106-43-4 p-Chlorotoluene ND 2.5 0.63 ug/l
124-48-1 Dibromochloromethane ND 2.5 0.63 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 2.5 1.2 ug/l
106-93-4 1,2-Dibromoethane ND 2.5 0.63 ug/l
75-71-8 Dichlorodifluoromethane ND 2.5 1.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 2.5 0.63 ug/l
541-73-1 1,3-Dichlorobenzene ND 2.5 0.63 ug/l
106-46-7 1,4-Dichlorobenzene ND 2.5 0.63 ug/l
75-34-3 1,1-Dichloroethane ND 2.5 0.63 ug/l
107-06-2 1,2-Dichloroethane 2.7 2.5 0.63 ug/l
75-35-4 1,1-Dichloroethylene ND 2.5 0.63 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.5 0.63 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.5 0.63 ug/l
78-87-5 1,2-Dichloropropane ND 2.5 0.63 ug/l
142-28-9 1,3-Dichloropropane ND 2.5 0.63 ug/l
594-20-7 2,2-Dichloropropane ND 2.5 0.63 ug/l
563-58-6 1,1-Dichloropropene ND 2.5 0.63 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 2.5 0.63 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 2.5 0.63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:TW-1
Lab Sample ID:FC5906-8 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 6.9 2.5 0.63 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 2.5 0.63 ug/l
87-68-3 Hexachlorobutadiene ND 2.5 0.63 ug/l
98-82-8 Isopropylbenzene 1.7 2.5 0.63 ug/l J
99-87-6 p-Isopropyltoluene ND 2.5 0.63 ug/l
74-83-9 Methyl Bromide ND 2.5 1.0 ug/l
74-87-3 Methyl Chloride ND 2.5 1.0 ug/l
74-95-3 Methylene Bromide ND 2.5 0.63 ug/l
75-09-2 Methylene Chloride ND 10 5.0 ug/l
91-20-3 Naphthalene ND 2.5 0.63 ug/l
103-65-1 n-Propylbenzene ND 2.5 0.63 ug/l
100-42-5 Styrene ND 2.5 0.63 ug/l
75-85-4 Tert-Amyl Alcohol 815 50 10 ug/l
994-05-8 Tert-Amyl Methyl Ether 2.1 5.0 1.0 ug/l J
75-65-0 Tert-Butyl Alcohol a 176 50 10 ug/l
762-75-4 Tert-Butyl Formate b ND 50 10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 0.63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 2.5 0.63 ug/l
127-18-4 Tetrachloroethylene ND 2.5 0.63 ug/l
108-88-3 Toluene ND 2.5 0.63 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.5 0.63 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.5 0.63 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.5 0.63 ug/l
79-00-5 1,1,2-Trichloroethane ND 2.5 0.63 ug/l
79-01-6 Trichloroethylene ND 2.5 0.63 ug/l
75-69-4 Trichlorofluoromethane ND 2.5 1.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.5 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene 1.6 2.5 0.63 ug/l J
108-67-8 1,3,5-Trimethylbenzene ND 2.5 0.63 ug/l
75-01-4 Vinyl Chloride ND 2.5 0.63 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 102%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
(a) Associated ECV outside of control limits high. No sample available for re-analysis.
(b) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-11
Lab Sample ID:FC5906-9 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E112366.D 1 05/12/23 13:22 TD n/a n/a VE2709
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.13 0.50 0.13 ug/l J
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-11
Lab Sample ID:FC5906-9 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride b ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate c ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane b ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%70-130%
17060-07-0 1,2-Dichloroethane-D4 110%70-130%
2037-26-5 Toluene-D8 93%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-11
Lab Sample ID:FC5906-9 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 92%70-130%
(a) Associated ICV, CCV, and BS recovery outside control limits high, sample ND.
(b) Associated CCV and BS outside control limits high, sample is ND.
(c) Associated BS recovery outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:MW-8
Lab Sample ID:FC5906-10 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E112367.D 1 05/12/23 13:49 TD n/a n/a VE2709
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.47 0.50 0.13 ug/l J
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-8
Lab Sample ID:FC5906-10 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene 0.20 0.50 0.13 ug/l J
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride b ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.54 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol 8.7 10 2.0 ug/l J
762-75-4 Tert-Butyl Formate c ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane b ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.14 0.50 0.13 ug/l J
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 0.60 1.0 0.13 ug/l J
95-47-6 o-Xylene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
2037-26-5 Toluene-D8 92%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-8
Lab Sample ID:FC5906-10 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 92%70-130%
(a) Associated ICV, CCV, and BS recovery outside control limits high, sample ND.
(b) Associated CCV and BS outside control limits high, sample is ND.
(c) Associated BS recovery outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:WSW-1
Lab Sample ID:FC5906-11 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E112369.D 1 05/12/23 14:44 TD n/a n/a VE2709
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:WSW-1
Lab Sample ID:FC5906-11 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride b ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate b ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane c ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%70-130%
2037-26-5 Toluene-D8 92%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:WSW-1
Lab Sample ID:FC5906-11 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 95%70-130%
(a) Associated ICV, CCV, and BS recovery outside control limits high, sample ND.
(b) Associated BS recovery outside control limits high, sample is ND.
(c) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:MW-7
Lab Sample ID:FC5906-12 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E112370.D 1 05/12/23 15:12 TD n/a n/a VE2709
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform 0.19 0.50 0.13 ug/l J
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-7
Lab Sample ID:FC5906-12 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride b ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate c ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane b ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%70-130%
17060-07-0 1,2-Dichloroethane-D4 110%70-130%
2037-26-5 Toluene-D8 91%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-7
Lab Sample ID:FC5906-12 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 93%70-130%
(a) Associated ICV, CCV, and BS recovery outside control limits high, sample ND.
(b) Associated CCV and BS outside control limits high, sample is ND.
(c) Associated BS recovery outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
57 of 154
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SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-6
Lab Sample ID:FC5906-13 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1095.D 1 05/12/23 13:36 TD n/a n/a V3A54
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform 7.1 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-6
Lab Sample ID:FC5906-13 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol a ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate a ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-6
Lab Sample ID:FC5906-13 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 103%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
(a) Associated BS recovery outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
60 of 154
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Report of Analysis Page 1 of 3
Client Sample ID:MW-17
Lab Sample ID:FC5906-14 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1096.D 1 05/12/23 14:00 TD n/a n/a V3A54
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-17
Lab Sample ID:FC5906-14 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.21 0.50 0.13 ug/l J
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol a ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate a ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-17
Lab Sample ID:FC5906-14 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 102%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
(a) Associated BS recovery outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
63 of 154
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Report of Analysis Page 1 of 3
Client Sample ID:MW-16
Lab Sample ID:FC5906-15 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1097.D 1 05/12/23 14:24 TD n/a n/a V3A54
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-16
Lab Sample ID:FC5906-15 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.52 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol a ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate a ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-16
Lab Sample ID:FC5906-15 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 103%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
(a) Associated BS recovery outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
66 of 154
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Report of Analysis Page 1 of 3
Client Sample ID:MW-12
Lab Sample ID:FC5906-16 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1098.D 1 05/12/23 14:48 TD n/a n/a V3A54
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-12
Lab Sample ID:FC5906-16 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol a ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate a ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-12
Lab Sample ID:FC5906-16 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 103%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
(a) Associated BS recovery outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-5
Lab Sample ID:FC5906-17 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1099.D 1 05/12/23 15:12 TD n/a n/a V3A54
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-5
Lab Sample ID:FC5906-17 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 1.8 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol a ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate a ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-5
Lab Sample ID:FC5906-17 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 102%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
(a) Associated BS recovery outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
72 of 154
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Report of Analysis Page 1 of 1
Client Sample ID:MW-5
Lab Sample ID:FC5906-17 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:RSKSOP-147/175 Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL82425.D 1 05/16/23 10:58 SS n/a n/a GLL2864
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 24 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane 2.5 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-5
Lab Sample ID:FC5906-17 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a <0.50 0.50 mg/l 5 05/10/23 10:40 ST SM3500FE B-11
Nitrogen, Nitrate <0.10 0.10 mg/l 1 05/09/23 18:51 JB EPA 300/SW846 9056A
Sulfate 2.0 2.0 mg/l 1 05/09/23 18:51 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
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Client Sample ID:MW-15
Lab Sample ID:FC5906-18 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1100.D 1 05/12/23 15:36 TD n/a n/a V3A54
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-15
Lab Sample ID:FC5906-18 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.31 0.50 0.13 ug/l J
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol a ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate a ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-15
Lab Sample ID:FC5906-18 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 102%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
(a) Associated BS recovery outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-15
Lab Sample ID:FC5906-18 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:RSKSOP-147/175 Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL82452.D 1 05/18/23 08:52 JR n/a n/a GLL2865
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 22 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane ND 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-15
Lab Sample ID:FC5906-18 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a 1.3 1.0 mg/l 10 05/10/23 10:40 ST SM3500FE B-11
Nitrogen, Nitrate 1.6 0.10 mg/l 1 05/09/23 19:57 JB EPA 300/SW846 9056A
Sulfate 2.4 2.0 mg/l 1 05/09/23 19:57 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
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Client Sample ID:MW-20
Lab Sample ID:FC5906-19 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1092.D 1 05/12/23 12:23 TD n/a n/a V3A54
Run #2 E112368.D 1 05/12/23 14:17 TD n/a n/a VE2709
Purge Volume
Run #1 5.0 ml
Run #2 5.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-20
Lab Sample ID:FC5906-19 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.20 0.50 0.13 ug/l J
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 82.1 b 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol a ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate a ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%106%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%109%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-20
Lab Sample ID:FC5906-19 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 102%92%70-130%
460-00-4 4-Bromofluorobenzene 99%92%70-130%
(a) Associated BS recovery outside control limits high, sample is ND.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-20
Lab Sample ID:FC5906-19 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:RSKSOP-147/175 Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL82429.D 1 05/16/23 11:29 SS n/a n/a GLL2864
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 24 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane ND 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-20
Lab Sample ID:FC5906-19 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a <0.50 0.50 mg/l 5 05/10/23 10:40 ST SM3500FE B-11
Nitrogen, Nitrate 0.68 0.10 mg/l 1 05/09/23 20:19 JB EPA 300/SW846 9056A
Sulfate <2.0 2.0 mg/l 1 05/09/23 20:19 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
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Client Sample ID:MW-18
Lab Sample ID:FC5906-20 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1093.D 1 05/12/23 12:47 TD n/a n/a V3A54
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-18
Lab Sample ID:FC5906-20 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.14 0.50 0.13 ug/l J
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 37.3 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol a ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate a ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-18
Lab Sample ID:FC5906-20 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 103%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
(a) Associated BS recovery outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
87 of 154
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Report of Analysis Page 1 of 1
Client Sample ID:MW-18
Lab Sample ID:FC5906-20 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:RSKSOP-147/175 Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL82430.D 1 05/16/23 11:36 SS n/a n/a GLL2864
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 24 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane ND 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
88 of 154
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Report of Analysis Page 1 of 1
Client Sample ID:MW-18
Lab Sample ID:FC5906-20 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a <0.10 0.10 mg/l 1 05/10/23 10:40 ST SM3500FE B-11
Nitrogen, Nitrate 0.29 0.10 mg/l 1 05/09/23 20:41 JB EPA 300/SW846 9056A
Sulfate <2.0 2.0 mg/l 1 05/09/23 20:41 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
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Client Sample ID:MW-19
Lab Sample ID:FC5906-21 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1080.D 1 05/11/23 17:12 TD n/a n/a V3A53
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-19
Lab Sample ID:FC5906-21 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 3.1 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol a ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate a ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-19
Lab Sample ID:FC5906-21 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-19
Lab Sample ID:FC5906-21 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:RSKSOP-147/175 Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL82431.D 1 05/16/23 12:32 SS n/a n/a GLL2864
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 24 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane ND 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
93 of 154
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Report of Analysis Page 1 of 1
Client Sample ID:MW-19
Lab Sample ID:FC5906-21 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a <0.10 0.10 mg/l 1 05/10/23 10:40 ST SM3500FE B-11
Nitrogen, Nitrate <0.10 0.10 mg/l 1 05/09/23 21:04 JB EPA 300/SW846 9056A
Sulfate <2.0 2.0 mg/l 1 05/09/23 21:04 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
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Report of Analysis Page 1 of 3
Client Sample ID:MW-13
Lab Sample ID:FC5906-22 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1076.D 5 05/11/23 15:34 TD n/a n/a V3A53
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 2.5 0.63 ug/l
108-86-1 Bromobenzene ND 2.5 0.63 ug/l
74-97-5 Bromochloromethane ND 2.5 0.63 ug/l
75-27-4 Bromodichloromethane ND 2.5 0.63 ug/l
75-25-2 Bromoform ND 2.5 0.63 ug/l
104-51-8 n-Butylbenzene ND 2.5 0.63 ug/l
135-98-8 sec-Butylbenzene ND 2.5 0.63 ug/l
98-06-6 tert-Butylbenzene ND 2.5 0.63 ug/l
56-23-5 Carbon Tetrachloride ND 2.5 0.63 ug/l
108-90-7 Chlorobenzene ND 2.5 0.63 ug/l
75-00-3 Chloroethane ND 2.5 1.0 ug/l
67-66-3 Chloroform ND 2.5 0.63 ug/l
95-49-8 o-Chlorotoluene ND 2.5 0.63 ug/l
106-43-4 p-Chlorotoluene ND 2.5 0.63 ug/l
124-48-1 Dibromochloromethane ND 2.5 0.63 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 2.5 1.2 ug/l
106-93-4 1,2-Dibromoethane ND 2.5 0.63 ug/l
75-71-8 Dichlorodifluoromethane ND 2.5 1.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 2.5 0.63 ug/l
541-73-1 1,3-Dichlorobenzene ND 2.5 0.63 ug/l
106-46-7 1,4-Dichlorobenzene ND 2.5 0.63 ug/l
75-34-3 1,1-Dichloroethane ND 2.5 0.63 ug/l
107-06-2 1,2-Dichloroethane ND 2.5 0.63 ug/l
75-35-4 1,1-Dichloroethylene ND 2.5 0.63 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.5 0.63 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.5 0.63 ug/l
78-87-5 1,2-Dichloropropane ND 2.5 0.63 ug/l
142-28-9 1,3-Dichloropropane ND 2.5 0.63 ug/l
594-20-7 2,2-Dichloropropane ND 2.5 0.63 ug/l
563-58-6 1,1-Dichloropropene ND 2.5 0.63 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 2.5 0.63 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 2.5 0.63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-13
Lab Sample ID:FC5906-22 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 2.5 0.63 ug/l
100-41-4 Ethylbenzene ND 2.5 0.63 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 2.5 0.63 ug/l
87-68-3 Hexachlorobutadiene ND 2.5 0.63 ug/l
98-82-8 Isopropylbenzene ND 2.5 0.63 ug/l
99-87-6 p-Isopropyltoluene ND 2.5 0.63 ug/l
74-83-9 Methyl Bromide ND 2.5 1.0 ug/l
74-87-3 Methyl Chloride ND 2.5 1.0 ug/l
74-95-3 Methylene Bromide ND 2.5 0.63 ug/l
75-09-2 Methylene Chloride 6.5 10 5.0 ug/l J
1634-04-4 Methyl Tert Butyl Ether 198 2.5 0.63 ug/l
91-20-3 Naphthalene ND 2.5 0.63 ug/l
103-65-1 n-Propylbenzene ND 2.5 0.63 ug/l
100-42-5 Styrene ND 2.5 0.63 ug/l
75-85-4 Tert-Amyl Alcohol ND 50 10 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 5.0 1.0 ug/l
75-65-0 Tert-Butyl Alcohol a ND 50 10 ug/l
762-75-4 Tert-Butyl Formate a ND 50 10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 0.63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 2.5 0.63 ug/l
127-18-4 Tetrachloroethylene ND 2.5 0.63 ug/l
108-88-3 Toluene ND 2.5 0.63 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.5 0.63 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.5 0.63 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.5 0.63 ug/l
79-00-5 1,1,2-Trichloroethane ND 2.5 0.63 ug/l
79-01-6 Trichloroethylene ND 2.5 0.63 ug/l
75-69-4 Trichlorofluoromethane ND 2.5 1.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.5 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 2.5 0.63 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 2.5 0.63 ug/l
75-01-4 Vinyl Chloride ND 2.5 0.63 ug/l
m,p-Xylene ND 5.0 0.63 ug/l
95-47-6 o-Xylene ND 2.5 0.63 ug/l
1330-20-7 Xylene (total)ND 7.5 1.3 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-13
Lab Sample ID:FC5906-22 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-13
Lab Sample ID:FC5906-22 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:RSKSOP-147/175 Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL82432.D 1 05/16/23 12:39 SS n/a n/a GLL2864
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 24 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane ND 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-13
Lab Sample ID:FC5906-22 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a 0.51 0.50 mg/l 5 05/10/23 10:40 ST SM3500FE B-11
Nitrogen, Nitrate <0.10 0.10 mg/l 1 05/09/23 21:26 JB EPA 300/SW846 9056A
Sulfate <2.0 2.0 mg/l 1 05/09/23 21:26 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
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Report of Analysis Page 1 of 3
Client Sample ID:MW-14
Lab Sample ID:FC5906-23 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1094.D 1 05/12/23 13:12 TD n/a n/a V3A54
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform 0.87 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-14
Lab Sample ID:FC5906-23 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 2.9 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol a ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate a ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-14
Lab Sample ID:FC5906-23 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:SM 6200B Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 103%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
(a) Associated BS recovery outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-14
Lab Sample ID:FC5906-23 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Method:RSKSOP-147/175 Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL82433.D 1 05/16/23 13:03 SS n/a n/a GLL2864
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 24 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane 4.5 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-14
Lab Sample ID:FC5906-23 Date Sampled:05/08/23
Matrix:AQ - Ground Water Date Received:05/09/23
Percent Solids:n/a
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a <0.50 0.50 mg/l 5 05/10/23 10:40 ST SM3500FE B-11
Nitrogen, Nitrate <0.10 0.10 mg/l 1 05/09/23 21:48 JB EPA 300/SW846 9056A
Sulfate <2.0 2.0 mg/l 1 05/09/23 21:48 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
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Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
 Chain of Custody
Orlando, FL
Section 4
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FC5906: Chain of Custody
Page 1 of 3
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FC5906: Chain of Custody
Page 2 of 3
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Job Number:FC5906 Client:GRI
Date / Time Received:5/9/2023 9:30:00 AM Delivery Method:FED EX
Project:4238
Airbill #'s:5707 9050 8940
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (2.3);
Cooler 1: (2.2);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230320 pH 10-12 25BDH07 Other: (Specify)pH 1.0 - 12.0 222221
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:-0.1; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:SHAYLAP Date:Date:5/9/2023 9:30:00 AM
FC5906: Chain of Custody
Page 3 of 3
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MS Volatiles
QC Data Summaries
Includes the following where applicable:
 Method Blank Summaries
 Blank Spike Summaries
 Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
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Method Blank Summary Page 1 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A53-MB 3A1072.D 1 05/11/23 TD n/a n/a V3A53
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-1, FC5906-4, FC5906-5, FC5906-8, FC5906-21, FC5906-22
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
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Method Blank Summary Page 2 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A53-MB 3A1072.D 1 05/11/23 TD n/a n/a V3A53
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-1, FC5906-4, FC5906-5, FC5906-8, FC5906-21, FC5906-22
CAS No.Compound Result RL MDL Units Q
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 103%70-130%
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Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A53-MB 3A1072.D 1 05/11/23 TD n/a n/a V3A53
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-1, FC5906-4, FC5906-5, FC5906-8, FC5906-21, FC5906-22
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
112 of 154
FC5906
5
5.
1
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Method Blank Summary Page 1 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A54-MB 3A1089.D 1 05/12/23 TD n/a n/a V3A54
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-2, FC5906-13, FC5906-14, FC5906-15, FC5906-16, FC5906-17, FC5906-18, FC5906-19, FC5906-20, FC5906-
23
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
113 of 154
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Method Blank Summary Page 2 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A54-MB 3A1089.D 1 05/12/23 TD n/a n/a V3A54
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-2, FC5906-13, FC5906-14, FC5906-15, FC5906-16, FC5906-17, FC5906-18, FC5906-19, FC5906-20, FC5906-
23
CAS No.Compound Result RL MDL Units Q
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 101%70-130%
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Method Blank Summary Page 3 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A54-MB 3A1089.D 1 05/12/23 TD n/a n/a V3A54
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-2, FC5906-13, FC5906-14, FC5906-15, FC5906-16, FC5906-17, FC5906-18, FC5906-19, FC5906-20, FC5906-
23
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 102%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
115 of 154
FC5906
5
5.
1
.
2
Method Blank Summary Page 1 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2709-MB E112362.D 1 05/12/23 TD n/a n/a VE2709
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-3, FC5906-4, FC5906-6, FC5906-7, FC5906-9, FC5906-10, FC5906-11, FC5906-12, FC5906-19
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
116 of 154
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Method Blank Summary Page 2 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2709-MB E112362.D 1 05/12/23 TD n/a n/a VE2709
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-3, FC5906-4, FC5906-6, FC5906-7, FC5906-9, FC5906-10, FC5906-11, FC5906-12, FC5906-19
CAS No.Compound Result RL MDL Units Q
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 103%70-130%
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Method Blank Summary Page 3 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2709-MB E112362.D 1 05/12/23 TD n/a n/a VE2709
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-3, FC5906-4, FC5906-6, FC5906-7, FC5906-9, FC5906-10, FC5906-11, FC5906-12, FC5906-19
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 94%70-130%
460-00-4 4-Bromofluorobenzene 94%70-130%
118 of 154
FC5906
5
5.
1
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3
Blank Spike Summary Page 1 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A53-BS 3A1070.D 1 05/11/23 TD n/a n/a V3A53
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-1, FC5906-4, FC5906-5, FC5906-8, FC5906-21, FC5906-22
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.1 101 70-130
108-86-1 Bromobenzene 10 9.3 93 70-130
74-97-5 Bromochloromethane 10 9.5 95 70-130
75-27-4 Bromodichloromethane 10 10.2 102 70-130
75-25-2 Bromoform 10 11.0 110 70-130
104-51-8 n-Butylbenzene 10 8.9 89 70-130
135-98-8 sec-Butylbenzene 10 9.4 94 70-130
98-06-6 tert-Butylbenzene 10 8.7 87 70-130
56-23-5 Carbon Tetrachloride 10 9.9 99 70-130
108-90-7 Chlorobenzene 10 9.7 97 70-130
75-00-3 Chloroethane 10 7.6 76 60-140
67-66-3 Chloroform 10 9.8 98 70-130
95-49-8 o-Chlorotoluene 10 9.7 97 70-130
106-43-4 p-Chlorotoluene 10 9.6 96 70-130
124-48-1 Dibromochloromethane 10 8.6 86 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.1 91 70-130
106-93-4 1,2-Dibromoethane 10 8.7 87 70-130
75-71-8 Dichlorodifluoromethane 10 10.1 101 60-140
95-50-1 1,2-Dichlorobenzene 10 9.7 97 70-130
541-73-1 1,3-Dichlorobenzene 10 9.8 98 70-130
106-46-7 1,4-Dichlorobenzene 10 9.5 95 70-130
75-34-3 1,1-Dichloroethane 10 9.8 98 70-130
107-06-2 1,2-Dichloroethane 10 9.6 96 70-130
75-35-4 1,1-Dichloroethylene 10 9.6 96 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.4 94 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.6 96 70-130
78-87-5 1,2-Dichloropropane 10 9.9 99 70-130
142-28-9 1,3-Dichloropropane 10 9.6 96 70-130
594-20-7 2,2-Dichloropropane 10 10.0 100 70-130
563-58-6 1,1-Dichloropropene 10 10.3 103 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.4 94 70-130
10061-02-6 trans-1,3-Dichloropropene 10 8.8 88 70-130
108-20-3 Di-Isopropyl Ether 10 9.0 90 70-130
100-41-4 Ethylbenzene 10 9.8 98 70-130
637-92-3 Ethyl Tert Butyl Ether 10 8.7 87 70-130
87-68-3 Hexachlorobutadiene 10 9.7 97 70-130
* = Outside of Control Limits.
119 of 154
FC5906
5
5.
2
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1
Blank Spike Summary Page 2 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A53-BS 3A1070.D 1 05/11/23 TD n/a n/a V3A53
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-1, FC5906-4, FC5906-5, FC5906-8, FC5906-21, FC5906-22
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
98-82-8 Isopropylbenzene 10 8.9 89 70-130
99-87-6 p-Isopropyltoluene 10 8.7 87 70-130
74-83-9 Methyl Bromide 10 8.8 88 60-140
74-87-3 Methyl Chloride 10 10.4 104 60-140
74-95-3 Methylene Bromide 10 9.6 96 70-130
75-09-2 Methylene Chloride 10 8.3 83 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.8 98 70-130
91-20-3 Naphthalene 10 8.6 86 70-130
103-65-1 n-Propylbenzene 10 9.8 98 70-130
100-42-5 Styrene 10 8.4 84 70-130
75-85-4 Tert-Amyl Alcohol 100 90.6 91 70-130
994-05-8 Tert-Amyl Methyl Ether 10 8.3 83 70-130
75-65-0 Tert-Butyl Alcohol 100 125 125 70-130
762-75-4 Tert-Butyl Formate 50 88.2 176*70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.0 90 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.3 93 70-130
127-18-4 Tetrachloroethylene 10 9.8 98 70-130
108-88-3 Toluene 10 9.7 97 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.3 103 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.0 100 70-130
71-55-6 1,1,1-Trichloroethane 10 10.1 101 70-130
79-00-5 1,1,2-Trichloroethane 10 9.8 98 70-130
79-01-6 Trichloroethylene 10 10.0 100 70-130
75-69-4 Trichlorofluoromethane 10 9.7 97 60-140
96-18-4 1,2,3-Trichloropropane 10 9.9 99 70-130
95-63-6 1,2,4-Trimethylbenzene 10 8.9 89 70-130
108-67-8 1,3,5-Trimethylbenzene 10 8.9 89 70-130
75-01-4 Vinyl Chloride 10 9.2 92 60-140
m,p-Xylene 20 20.0 100 70-130
95-47-6 o-Xylene 10 8.7 87 70-130
1330-20-7 Xylene (total)30 28.7 96 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%70-130%
* = Outside of Control Limits.
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FC5906
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Blank Spike Summary Page 3 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A53-BS 3A1070.D 1 05/11/23 TD n/a n/a V3A53
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-1, FC5906-4, FC5906-5, FC5906-8, FC5906-21, FC5906-22
CAS No.Surrogate Recoveries BSP Limits
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
* = Outside of Control Limits.
121 of 154
FC5906
5
5.
2
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1
Blank Spike Summary Page 1 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A54-BS 3A1087.D 1 05/12/23 TD n/a n/a V3A54
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-2, FC5906-13, FC5906-14, FC5906-15, FC5906-16, FC5906-17, FC5906-18, FC5906-19, FC5906-20, FC5906-
23
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.2 102 70-130
108-86-1 Bromobenzene 10 10.7 107 70-130
74-97-5 Bromochloromethane 10 9.6 96 70-130
75-27-4 Bromodichloromethane 10 10.5 105 70-130
75-25-2 Bromoform 10 12.7 127 70-130
104-51-8 n-Butylbenzene 10 9.5 95 70-130
135-98-8 sec-Butylbenzene 10 9.2 92 70-130
98-06-6 tert-Butylbenzene 10 9.2 92 70-130
56-23-5 Carbon Tetrachloride 10 10.4 104 70-130
108-90-7 Chlorobenzene 10 10.0 100 70-130
75-00-3 Chloroethane 10 7.8 78 60-140
67-66-3 Chloroform 10 10.2 102 70-130
95-49-8 o-Chlorotoluene 10 10.4 104 70-130
106-43-4 p-Chlorotoluene 10 10.6 106 70-130
124-48-1 Dibromochloromethane 10 10.3 103 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 12.3 123 70-130
106-93-4 1,2-Dibromoethane 10 9.6 96 70-130
75-71-8 Dichlorodifluoromethane 10 15.0 150*60-140
95-50-1 1,2-Dichlorobenzene 10 10.6 106 70-130
541-73-1 1,3-Dichlorobenzene 10 10.3 103 70-130
106-46-7 1,4-Dichlorobenzene 10 10.2 102 70-130
75-34-3 1,1-Dichloroethane 10 9.8 98 70-130
107-06-2 1,2-Dichloroethane 10 9.7 97 70-130
75-35-4 1,1-Dichloroethylene 10 9.9 99 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.5 95 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.9 99 70-130
78-87-5 1,2-Dichloropropane 10 10.5 105 70-130
142-28-9 1,3-Dichloropropane 10 11.1 111 70-130
594-20-7 2,2-Dichloropropane 10 10.7 107 70-130
563-58-6 1,1-Dichloropropene 10 10.6 106 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.7 97 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.1 91 70-130
108-20-3 Di-Isopropyl Ether 10 9.6 96 70-130
100-41-4 Ethylbenzene 10 10.1 101 70-130
637-92-3 Ethyl Tert Butyl Ether 10 9.5 95 70-130
87-68-3 Hexachlorobutadiene 10 10.2 102 70-130
* = Outside of Control Limits.
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Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A54-BS 3A1087.D 1 05/12/23 TD n/a n/a V3A54
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-2, FC5906-13, FC5906-14, FC5906-15, FC5906-16, FC5906-17, FC5906-18, FC5906-19, FC5906-20, FC5906-
23
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
98-82-8 Isopropylbenzene 10 9.2 92 70-130
99-87-6 p-Isopropyltoluene 10 8.9 89 70-130
74-83-9 Methyl Bromide 10 11.1 111 60-140
74-87-3 Methyl Chloride 10 12.4 124 60-140
74-95-3 Methylene Bromide 10 10 100 70-130
75-09-2 Methylene Chloride 10 8.7 87 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.8 108 70-130
91-20-3 Naphthalene 10 10.9 109 70-130
103-65-1 n-Propylbenzene 10 10.4 104 70-130
100-42-5 Styrene 10 9.1 91 70-130
75-85-4 Tert-Amyl Alcohol 100 112 112 70-130
994-05-8 Tert-Amyl Methyl Ether 10 9.1 91 70-130
75-65-0 Tert-Butyl Alcohol 100 137 137*70-130
762-75-4 Tert-Butyl Formate 50 89.4 179*70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.8 98 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 11.0 110 70-130
127-18-4 Tetrachloroethylene 10 9.9 99 70-130
108-88-3 Toluene 10 10.1 101 70-130
87-61-6 1,2,3-Trichlorobenzene 10 11.9 119 70-130
120-82-1 1,2,4-Trichlorobenzene 10 11.1 111 70-130
71-55-6 1,1,1-Trichloroethane 10 10.3 103 70-130
79-00-5 1,1,2-Trichloroethane 10 10.7 107 70-130
79-01-6 Trichloroethylene 10 9.9 99 70-130
75-69-4 Trichlorofluoromethane 10 11.1 111 60-140
96-18-4 1,2,3-Trichloropropane 10 12.3 123 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.6 96 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.6 96 70-130
75-01-4 Vinyl Chloride 10 10.1 101 60-140
m,p-Xylene 20 21.0 105 70-130
95-47-6 o-Xylene 10 9.2 92 70-130
1330-20-7 Xylene (total)30 30.3 101 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 99%70-130%
* = Outside of Control Limits.
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Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A54-BS 3A1087.D 1 05/12/23 TD n/a n/a V3A54
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-2, FC5906-13, FC5906-14, FC5906-15, FC5906-16, FC5906-17, FC5906-18, FC5906-19, FC5906-20, FC5906-
23
CAS No.Surrogate Recoveries BSP Limits
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 102%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
* = Outside of Control Limits.
124 of 154
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5.
2
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Blank Spike Summary Page 1 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2709-BS a E112360.D 1 05/12/23 TD n/a n/a VE2709
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-3, FC5906-4, FC5906-6, FC5906-7, FC5906-9, FC5906-10, FC5906-11, FC5906-12, FC5906-19
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.6 106 70-130
108-86-1 Bromobenzene 10 10.8 108 70-130
74-97-5 Bromochloromethane 10 11.3 113 70-130
75-27-4 Bromodichloromethane 10 10.6 106 70-130
75-25-2 Bromoform 10 9.7 97 70-130
104-51-8 n-Butylbenzene 10 10.4 104 70-130
135-98-8 sec-Butylbenzene 10 9.4 94 70-130
98-06-6 tert-Butylbenzene 10 9.5 95 70-130
56-23-5 Carbon Tetrachloride 10 11.9 119 70-130
108-90-7 Chlorobenzene 10 10.3 103 70-130
75-00-3 Chloroethane 10 12.8 128 60-140
67-66-3 Chloroform 10 11.2 112 70-130
95-49-8 o-Chlorotoluene 10 9.4 94 70-130
106-43-4 p-Chlorotoluene 10 9.4 94 70-130
124-48-1 Dibromochloromethane 10 10.5 105 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.9 89 70-130
106-93-4 1,2-Dibromoethane 10 10.5 105 70-130
75-71-8 Dichlorodifluoromethane 10 27.9 279*60-140
95-50-1 1,2-Dichlorobenzene 10 10.1 101 70-130
541-73-1 1,3-Dichlorobenzene 10 10.0 100 70-130
106-46-7 1,4-Dichlorobenzene 10 9.8 98 70-130
75-34-3 1,1-Dichloroethane 10 10.3 103 70-130
107-06-2 1,2-Dichloroethane 10 11.3 113 70-130
75-35-4 1,1-Dichloroethylene 10 11.7 117 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.6 106 70-130
156-60-5 trans-1,2-Dichloroethylene 10 11.4 114 70-130
78-87-5 1,2-Dichloropropane 10 10.9 109 70-130
142-28-9 1,3-Dichloropropane 10 10.7 107 70-130
594-20-7 2,2-Dichloropropane 10 12.7 127 70-130
563-58-6 1,1-Dichloropropene 10 11.0 110 70-130
10061-01-5 cis-1,3-Dichloropropene 10 10.3 103 70-130
10061-02-6 trans-1,3-Dichloropropene 10 8.7 87 70-130
108-20-3 Di-Isopropyl Ether 10 10.5 105 70-130
100-41-4 Ethylbenzene 10 10.4 104 70-130
637-92-3 Ethyl Tert Butyl Ether 10 10.9 109 70-130
87-68-3 Hexachlorobutadiene 10 10.4 104 70-130
* = Outside of Control Limits.
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Blank Spike Summary Page 2 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2709-BS a E112360.D 1 05/12/23 TD n/a n/a VE2709
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-3, FC5906-4, FC5906-6, FC5906-7, FC5906-9, FC5906-10, FC5906-11, FC5906-12, FC5906-19
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
98-82-8 Isopropylbenzene 10 10.4 104 70-130
99-87-6 p-Isopropyltoluene 10 9.7 97 70-130
74-83-9 Methyl Bromide 10 12.0 120 60-140
74-87-3 Methyl Chloride 10 17.9 179*60-140
74-95-3 Methylene Bromide 10 11.3 113 70-130
75-09-2 Methylene Chloride 10 11.5 115 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.6 106 70-130
91-20-3 Naphthalene 10 9.8 98 70-130
103-65-1 n-Propylbenzene 10 9.7 97 70-130
100-42-5 Styrene 10 10.5 105 70-130
75-85-4 Tert-Amyl Alcohol 100 84.2 84 70-130
994-05-8 Tert-Amyl Methyl Ether 10 10.2 102 70-130
75-65-0 Tert-Butyl Alcohol 100 103 103 70-130
762-75-4 Tert-Butyl Formate 50 99.6 199*70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.9 109 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.3 93 70-130
127-18-4 Tetrachloroethylene 10 11.2 112 70-130
108-88-3 Toluene 10 9.7 97 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.6 106 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.4 104 70-130
71-55-6 1,1,1-Trichloroethane 10 11.4 114 70-130
79-00-5 1,1,2-Trichloroethane 10 10.0 100 70-130
79-01-6 Trichloroethylene 10 10.9 109 70-130
75-69-4 Trichlorofluoromethane 10 15.1 151*60-140
96-18-4 1,2,3-Trichloropropane 10 10.4 104 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.7 97 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.7 97 70-130
75-01-4 Vinyl Chloride 10 14.0 140 60-140
m,p-Xylene 20 20.6 103 70-130
95-47-6 o-Xylene 10 10.0 100 70-130
1330-20-7 Xylene (total)30 30.7 102 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101%70-130%
* = Outside of Control Limits.
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Blank Spike Summary Page 3 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2709-BS a E112360.D 1 05/12/23 TD n/a n/a VE2709
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-3, FC5906-4, FC5906-6, FC5906-7, FC5906-9, FC5906-10, FC5906-11, FC5906-12, FC5906-19
CAS No.Surrogate Recoveries BSP Limits
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 92%70-130%
(a) No MSD available for this run.
* = Outside of Control Limits.
127 of 154
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5.
2
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Matrix Spike Summary Page 1 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC5906-4MS E112372.D 25 05/12/23 TD n/a n/a VE2709
FC5906-4 E112371.D 10 05/12/23 TD n/a n/a VE2709
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-3, FC5906-4, FC5906-6, FC5906-7, FC5906-9, FC5906-10, FC5906-11, FC5906-12, FC5906-19
FC5906-4 Spike MS MS
CAS No.Compound ug/l Q ug/l ug/l %Limits
71-43-2 Benzene 957 250 1350 157* a 70-130
108-86-1 Bromobenzene ND 250 279 112 70-130
74-97-5 Bromochloromethane ND 250 301 120 70-130
75-27-4 Bromodichloromethane ND 250 285 114 70-130
75-25-2 Bromoform ND 250 246 98 70-130
104-51-8 n-Butylbenzene 8.6 250 300 117 70-130
135-98-8 sec-Butylbenzene 5.3 250 257 101 70-130
98-06-6 tert-Butylbenzene ND 250 258 103 70-130
56-23-5 Carbon Tetrachloride ND 250 318 127 70-130
108-90-7 Chlorobenzene ND 250 271 108 70-130
75-00-3 Chloroethane ND 250 322 129 60-140
67-66-3 Chloroform ND 250 316 126 70-130
95-49-8 o-Chlorotoluene ND 250 264 106 70-130
106-43-4 p-Chlorotoluene ND 250 249 100 70-130
124-48-1 Dibromochloromethane ND 250 264 106 70-130
96-12-8 1,2-Dibromo-3-chloropropane ND 250 233 93 70-130
106-93-4 1,2-Dibromoethane ND 250 275 110 70-130
75-71-8 Dichlorodifluoromethane ND 250 772 309*60-140
95-50-1 1,2-Dichlorobenzene ND 250 269 108 70-130
541-73-1 1,3-Dichlorobenzene ND 250 261 104 70-130
106-46-7 1,4-Dichlorobenzene ND 250 270 108 70-130
75-34-3 1,1-Dichloroethane ND 250 281 112 70-130
107-06-2 1,2-Dichloroethane ND 250 318 127 70-130
75-35-4 1,1-Dichloroethylene ND 250 321 128 70-130
156-59-2 cis-1,2-Dichloroethylene ND 250 298 119 70-130
156-60-5 trans-1,2-Dichloroethylene ND 250 302 121 70-130
78-87-5 1,2-Dichloropropane ND 250 307 123 70-130
142-28-9 1,3-Dichloropropane ND 250 277 111 70-130
594-20-7 2,2-Dichloropropane ND 250 354 142*70-130
563-58-6 1,1-Dichloropropene ND 250 318 127 70-130
10061-01-5 cis-1,3-Dichloropropene ND 250 288 115 70-130
10061-02-6 trans-1,3-Dichloropropene ND 250 227 91 70-130
108-20-3 Di-Isopropyl Ether 6.5 250 296 116 70-130
100-41-4 Ethylbenzene 359 250 684 130 70-130
637-92-3 Ethyl Tert Butyl Ether ND 250 285 114 70-130
87-68-3 Hexachlorobutadiene ND 250 292 117 70-130
* = Outside of Control Limits.
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Matrix Spike Summary Page 2 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC5906-4MS E112372.D 25 05/12/23 TD n/a n/a VE2709
FC5906-4 E112371.D 10 05/12/23 TD n/a n/a VE2709
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-3, FC5906-4, FC5906-6, FC5906-7, FC5906-9, FC5906-10, FC5906-11, FC5906-12, FC5906-19
FC5906-4 Spike MS MS
CAS No.Compound ug/l Q ug/l ug/l %Limits
98-82-8 Isopropylbenzene 23.3 250 311 115 70-130
99-87-6 p-Isopropyltoluene 2.7 J 250 266 105 70-130
74-83-9 Methyl Bromide ND 250 330 132 60-140
74-87-3 Methyl Chloride ND 250 523 209*60-140
74-95-3 Methylene Bromide ND 250 317 127 70-130
75-09-2 Methylene Chloride ND 250 362 145*70-130
1634-04-4 Methyl Tert Butyl Ether 196 250 499 121 70-130
91-20-3 Naphthalene 107 250 379 109 70-130
103-65-1 n-Propylbenzene 47.6 250 312 106 70-130
100-42-5 Styrene ND 250 285 114 70-130
75-85-4 Tert-Amyl Alcohol 515 2500 3050 101 70-130
994-05-8 Tert-Amyl Methyl Ether ND 250 276 110 70-130
75-65-0 Tert-Butyl Alcohol 198 2500 3430 129 70-130
762-75-4 Tert-Butyl Formate ND 1250 2930 234*70-130
630-20-6 1,1,1,2-Tetrachloroethane ND 250 277 111 70-130
79-34-5 1,1,2,2-Tetrachloroethane ND 250 246 98 70-130
127-18-4 Tetrachloroethylene ND 250 304 122 70-130
108-88-3 Toluene 18.4 250 286 107 70-130
87-61-6 1,2,3-Trichlorobenzene ND 250 278 111 70-130
120-82-1 1,2,4-Trichlorobenzene ND 250 284 114 70-130
71-55-6 1,1,1-Trichloroethane ND 250 328 131*70-130
79-00-5 1,1,2-Trichloroethane ND 250 260 104 70-130
79-01-6 Trichloroethylene ND 250 317 127 70-130
75-69-4 Trichlorofluoromethane ND 250 393 157*60-140
96-18-4 1,2,3-Trichloropropane ND 250 277 111 70-130
95-63-6 1,2,4-Trimethylbenzene 255 250 543 115 70-130
108-67-8 1,3,5-Trimethylbenzene 85.7 250 357 109 70-130
75-01-4 Vinyl Chloride ND 250 356 142*60-140
m,p-Xylene 730 500 1380 130 70-130
95-47-6 o-Xylene 100 250 378 111 70-130
1330-20-7 Xylene (total)830 750 1760 124 70-130
CAS No.Surrogate Recoveries MS FC5906-4 Limits
1868-53-7 Dibromofluoromethane 105%103%70-130%
* = Outside of Control Limits.
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Matrix Spike Summary Page 3 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC5906-4MS E112372.D 25 05/12/23 TD n/a n/a VE2709
FC5906-4 E112371.D 10 05/12/23 TD n/a n/a VE2709
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-3, FC5906-4, FC5906-6, FC5906-7, FC5906-9, FC5906-10, FC5906-11, FC5906-12, FC5906-19
CAS No.Surrogate Recoveries MS FC5906-4 Limits
17060-07-0 1,2-Dichloroethane-D4 112%111%70-130%
2037-26-5 Toluene-D8 93%91%70-130%
460-00-4 4-Bromofluorobenzene 92%90%70-130%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC5906-5MS 3A1081.D 200 05/11/23 TD n/a n/a V3A53
FC5906-5MSD 3A1082.D 200 05/11/23 TD n/a n/a V3A53
FC5906-5 3A1074.D 200 05/11/23 TD n/a n/a V3A53
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-1, FC5906-4, FC5906-5, FC5906-8, FC5906-21, FC5906-22
FC5906-5 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 5930 2000 8070 107 2000 8040 106 0 70-130/20
108-86-1 Bromobenzene ND 2000 2010 101 2000 2080 104 3 70-130/20
74-97-5 Bromochloromethane ND 2000 2080 104 2000 2080 104 0 70-130/20
75-27-4 Bromodichloromethane ND 2000 2170 109 2000 2180 109 0 70-130/20
75-25-2 Bromoform ND 2000 2230 112 2000 2360 118 6 70-130/20
104-51-8 n-Butylbenzene ND 2000 1980 99 2000 2090 105 5 70-130/20
135-98-8 sec-Butylbenzene ND 2000 1830 92 2000 1950 98 6 70-130/20
98-06-6 tert-Butylbenzene ND 2000 1780 89 2000 1910 96 7 70-130/20
56-23-5 Carbon Tetrachloride ND 2000 2170 109 2000 2190 110 1 70-130/20
108-90-7 Chlorobenzene ND 2000 2020 101 2000 2080 104 3 70-130/20
75-00-3 Chloroethane ND 2000 1490 75 2000 1600 80 7 60-140/20
67-66-3 Chloroform ND 2000 2250 113 2000 2180 109 3 70-130/20
95-49-8 o-Chlorotoluene ND 2000 2050 103 2000 2160 108 5 70-130/20
106-43-4 p-Chlorotoluene ND 2000 1950 98 2000 2070 104 6 70-130/20
124-48-1 Dibromochloromethane ND 2000 1880 94 2000 1920 96 2 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 2000 2090 105 2000 2190 110 5 70-130/20
106-93-4 1,2-Dibromoethane ND 2000 1910 96 2000 1960 98 3 70-130/20
75-71-8 Dichlorodifluoromethane ND 2000 2730 137 2000 3230 162*17 60-140/20
95-50-1 1,2-Dichlorobenzene ND 2000 1990 100 2000 2090 105 5 70-130/20
541-73-1 1,3-Dichlorobenzene ND 2000 1970 99 2000 2060 103 4 70-130/20
106-46-7 1,4-Dichlorobenzene ND 2000 1980 99 2000 2010 101 2 70-130/20
75-34-3 1,1-Dichloroethane ND 2000 2090 105 2000 2080 104 0 70-130/20
107-06-2 1,2-Dichloroethane ND 2000 2100 105 2000 2120 106 1 70-130/20
75-35-4 1,1-Dichloroethylene ND 2000 2130 107 2000 2130 107 0 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 2000 1990 100 2000 2020 101 1 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 2000 2110 106 2000 2140 107 1 70-130/20
78-87-5 1,2-Dichloropropane ND 2000 2250 113 2000 2250 113 0 70-130/20
142-28-9 1,3-Dichloropropane ND 2000 2180 109 2000 2220 111 2 70-130/20
594-20-7 2,2-Dichloropropane ND 2000 2180 109 2000 2170 109 0 70-130/20
563-58-6 1,1-Dichloropropene ND 2000 2290 115 2000 2290 115 0 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 2000 2020 101 2000 2060 103 2 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 2000 1740 87 2000 1800 90 3 70-130/20
108-20-3 Di-Isopropyl Ether 53.5 J 2000 2010 98 2000 2090 102 4 70-130/20
100-41-4 Ethylbenzene 2460 2000 4530 104 2000 4630 109 2 70-130/20
637-92-3 Ethyl Tert Butyl Ether ND 2000 1920 96 2000 2000 100 4 70-130/20
87-68-3 Hexachlorobutadiene ND 2000 2040 102 2000 2180 109 7 70-130/20
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC5906-5MS 3A1081.D 200 05/11/23 TD n/a n/a V3A53
FC5906-5MSD 3A1082.D 200 05/11/23 TD n/a n/a V3A53
FC5906-5 3A1074.D 200 05/11/23 TD n/a n/a V3A53
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-1, FC5906-4, FC5906-5, FC5906-8, FC5906-21, FC5906-22
FC5906-5 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
98-82-8 Isopropylbenzene 57.0 J 2000 1930 94 2000 2000 97 4 70-130/20
99-87-6 p-Isopropyltoluene ND 2000 1760 88 2000 1860 93 6 70-130/20
74-83-9 Methyl Bromide ND 2000 1540 77 2000 1860 93 19 60-140/20
74-87-3 Methyl Chloride ND 2000 2330 117 2000 2690 135 14 60-140/20
74-95-3 Methylene Bromide ND 2000 2120 106 2000 2140 107 1 70-130/20
75-09-2 Methylene Chloride ND 2000 2000 100 2000 1980 99 1 70-130/20
1634-04-4 Methyl Tert Butyl Ether 1830 2000 4230 120 2000 4300 124 2 70-130/20
91-20-3 Naphthalene 698 2000 2720 101 2000 2900 110 6 70-130/20
103-65-1 n-Propylbenzene 204 2000 2220 101 2000 2340 107 5 70-130/20
100-42-5 Styrene ND 2000 1810 91 2000 1880 94 4 70-130/20
75-85-4 Tert-Amyl Alcohol 5010 20000 28500 117 20000 30500 127 7 70-130/20
994-05-8 Tert-Amyl Methyl Ether ND 2000 1900 95 2000 1970 99 4 70-130/20
75-65-0 Tert-Butyl Alcohol ND 20000 28600 143*20000 32000 160*11 70-130/20
762-75-4 Tert-Butyl Formate ND 10000 21800 218*10000 24700 247*12 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 2000 1880 94 2000 1940 97 3 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 2000 1970 99 2000 2060 103 4 70-130/20
127-18-4 Tetrachloroethylene ND 2000 2060 103 2000 2110 106 2 70-130/20
108-88-3 Toluene 4220 2000 6110 95 2000 6200 99 1 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 2000 2150 108 2000 2260 113 5 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 2000 2120 106 2000 2250 113 6 70-130/20
71-55-6 1,1,1-Trichloroethane ND 2000 2200 110 2000 2210 111 0 70-130/20
79-00-5 1,1,2-Trichloroethane ND 2000 2070 104 2000 2120 106 2 70-130/20
79-01-6 Trichloroethylene ND 2000 2170 109 2000 2170 109 0 70-130/20
75-69-4 Trichlorofluoromethane ND 2000 2040 102 2000 2330 117 13 60-140/20
96-18-4 1,2,3-Trichloropropane ND 2000 2220 111 2000 2320 116 4 70-130/20
95-63-6 1,2,4-Trimethylbenzene 1820 2000 3750 97 2000 3920 105 4 70-130/20
108-67-8 1,3,5-Trimethylbenzene 476 2000 2380 95 2000 2490 101 5 70-130/20
75-01-4 Vinyl Chloride ND 2000 1910 96 2000 2140 107 11 60-140/20
m,p-Xylene 8660 4000 12800 104 4000 12800 104 0 70-130/20
95-47-6 o-Xylene 4510 2000 6320 91 2000 6450 97 2 70-130/20
1330-20-7 Xylene (total)13200 6000 19100 98 6000 19300 102 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FC5906-5 Limits
1868-53-7 Dibromofluoromethane 102%100%100%70-130%
* = Outside of Control Limits.
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4
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Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC5906-5MS 3A1081.D 200 05/11/23 TD n/a n/a V3A53
FC5906-5MSD 3A1082.D 200 05/11/23 TD n/a n/a V3A53
FC5906-5 3A1074.D 200 05/11/23 TD n/a n/a V3A53
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-1, FC5906-4, FC5906-5, FC5906-8, FC5906-21, FC5906-22
CAS No.Surrogate Recoveries MS MSD FC5906-5 Limits
17060-07-0 1,2-Dichloroethane-D4 107%103%105%70-130%
2037-26-5 Toluene-D8 99%100%99%70-130%
460-00-4 4-Bromofluorobenzene 96%97%98%70-130%
* = Outside of Control Limits.
133 of 154
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5
5.
4
.
1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC5906-23MS 3A1102.D 10 05/12/23 TD n/a n/a V3A54
FC5906-23MSD 3A1103.D 10 05/12/23 TD n/a n/a V3A54
FC5906-23 3A1094.D 1 05/12/23 TD n/a n/a V3A54
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-2, FC5906-13, FC5906-14, FC5906-15, FC5906-16, FC5906-17, FC5906-18, FC5906-19, FC5906-20, FC5906-
23
FC5906-23 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 100 99.4 99 100 96.7 97 3 70-130/20
108-86-1 Bromobenzene ND 100 95.9 96 100 94.0 94 2 70-130/20
74-97-5 Bromochloromethane ND 100 90.0 90 100 89.3 89 1 70-130/20
75-27-4 Bromodichloromethane ND 100 97.2 97 100 95.4 95 2 70-130/20
75-25-2 Bromoform ND 100 106 106 100 104 104 2 70-130/20
104-51-8 n-Butylbenzene ND 100 82.6 83 100 81.8 82 1 70-130/20
135-98-8 sec-Butylbenzene ND 100 82.8 83 100 81.7 82 1 70-130/20
98-06-6 tert-Butylbenzene ND 100 82.0 82 100 81.4 81 1 70-130/20
56-23-5 Carbon Tetrachloride ND 100 98.8 99 100 98.6 99 0 70-130/20
108-90-7 Chlorobenzene ND 100 93.4 93 100 91.7 92 2 70-130/20
75-00-3 Chloroethane ND 100 61.8 62 100 72.7 73 16 60-140/20
67-66-3 Chloroform 0.87 100 99.4 99 100 97.4 97 2 70-130/20
95-49-8 o-Chlorotoluene ND 100 94.9 95 100 93.1 93 2 70-130/20
106-43-4 p-Chlorotoluene ND 100 94.2 94 100 91.2 91 3 70-130/20
124-48-1 Dibromochloromethane ND 100 84.0 84 100 83.9 84 0 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 100 105 105 100 101 101 4 70-130/20
106-93-4 1,2-Dibromoethane ND 100 83.8 84 100 82.6 83 1 70-130/20
75-71-8 Dichlorodifluoromethane ND 100 121 121 100 141 141*15 60-140/20
95-50-1 1,2-Dichlorobenzene ND 100 92.0 92 100 91.7 92 0 70-130/20
541-73-1 1,3-Dichlorobenzene ND 100 92.0 92 100 89.6 90 3 70-130/20
106-46-7 1,4-Dichlorobenzene ND 100 91.6 92 100 89.8 90 2 70-130/20
75-34-3 1,1-Dichloroethane ND 100 94.7 95 100 93.0 93 2 70-130/20
107-06-2 1,2-Dichloroethane ND 100 93.9 94 100 90.4 90 4 70-130/20
75-35-4 1,1-Dichloroethylene ND 100 98.0 98 100 95.6 96 2 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 100 88.8 89 100 88.4 88 0 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 100 96.3 96 100 93.5 94 3 70-130/20
78-87-5 1,2-Dichloropropane ND 100 99.8 100 100 98.5 99 1 70-130/20
142-28-9 1,3-Dichloropropane ND 100 96.6 97 100 95.8 96 1 70-130/20
594-20-7 2,2-Dichloropropane ND 100 102 102 100 98.9 99 3 70-130/20
563-58-6 1,1-Dichloropropene ND 100 103 103 100 101 101 2 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 100 88.7 89 100 86.0 86 3 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 100 78.0 78 100 77.0 77 1 70-130/20
108-20-3 Di-Isopropyl Ether ND 100 88.2 88 100 86.7 87 2 70-130/20
100-41-4 Ethylbenzene ND 100 95.4 95 100 92.2 92 3 70-130/20
637-92-3 Ethyl Tert Butyl Ether ND 100 86.4 86 100 85.7 86 1 70-130/20
87-68-3 Hexachlorobutadiene ND 100 85.5 86 100 85.5 86 0 70-130/20
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC5906-23MS 3A1102.D 10 05/12/23 TD n/a n/a V3A54
FC5906-23MSD 3A1103.D 10 05/12/23 TD n/a n/a V3A54
FC5906-23 3A1094.D 1 05/12/23 TD n/a n/a V3A54
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-2, FC5906-13, FC5906-14, FC5906-15, FC5906-16, FC5906-17, FC5906-18, FC5906-19, FC5906-20, FC5906-
23
FC5906-23 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
98-82-8 Isopropylbenzene ND 100 82.0 82 100 80.2 80 2 70-130/20
99-87-6 p-Isopropyltoluene ND 100 78.1 78 100 76.9 77 2 70-130/20
74-83-9 Methyl Bromide ND 100 88.1 88 100 102 102 15 60-140/20
74-87-3 Methyl Chloride ND 100 103 103 100 121 121 16 60-140/20
74-95-3 Methylene Bromide ND 100 92.0 92 100 91.4 91 1 70-130/20
75-09-2 Methylene Chloride ND 100 86.6 87 100 92.7 93 7 70-130/20
1634-04-4 Methyl Tert Butyl Ether 2.9 100 97.1 94 100 99.5 97 2 70-130/20
91-20-3 Naphthalene ND 100 83.5 84 100 83.7 84 0 70-130/20
103-65-1 n-Propylbenzene ND 100 94.9 95 100 93.4 93 2 70-130/20
100-42-5 Styrene ND 100 79.3 79 100 77.5 78 2 70-130/20
75-85-4 Tert-Amyl Alcohol ND 1000 1050 105 1000 991 99 6 70-130/20
994-05-8 Tert-Amyl Methyl Ether ND 100 80.4 80 100 79.7 80 1 70-130/20
75-65-0 Tert-Butyl Alcohol ND 1000 1360 136*1000 1390 139*2 70-130/20
762-75-4 Tert-Butyl Formate ND 500 944 189*500 1100 220*15 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 100 88.0 88 100 86.5 87 2 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 100 95.6 96 100 93.5 94 2 70-130/20
127-18-4 Tetrachloroethylene ND 100 96.1 96 100 93.2 93 3 70-130/20
108-88-3 Toluene ND 100 95.0 95 100 93.0 93 2 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 100 94.4 94 100 95.5 96 1 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 100 88.8 89 100 89.1 89 0 70-130/20
71-55-6 1,1,1-Trichloroethane ND 100 104 104 100 99.9 100 4 70-130/20
79-00-5 1,1,2-Trichloroethane ND 100 92.9 93 100 93.1 93 0 70-130/20
79-01-6 Trichloroethylene ND 100 97.9 98 100 94.8 95 3 70-130/20
75-69-4 Trichlorofluoromethane ND 100 91.8 92 100 107 107 15 60-140/20
96-18-4 1,2,3-Trichloropropane ND 100 113 113 100 108 108 5 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 100 86.0 86 100 83.8 84 3 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 100 86.3 86 100 84.8 85 2 70-130/20
75-01-4 Vinyl Chloride ND 100 82.2 82 100 97.2 97 17 60-140/20
m,p-Xylene ND 200 193 97 200 189 95 2 70-130/20
95-47-6 o-Xylene ND 100 81.8 82 100 79.8 80 2 70-130/20
1330-20-7 Xylene (total)ND 300 275 92 300 269 90 2 70-130/20
CAS No.Surrogate Recoveries MS MSD FC5906-23 Limits
1868-53-7 Dibromofluoromethane 100%100%101%70-130%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC5906-23MS 3A1102.D 10 05/12/23 TD n/a n/a V3A54
FC5906-23MSD 3A1103.D 10 05/12/23 TD n/a n/a V3A54
FC5906-23 3A1094.D 1 05/12/23 TD n/a n/a V3A54
The QC reported here applies to the following samples:Method: SM 6200B
FC5906-2, FC5906-13, FC5906-14, FC5906-15, FC5906-16, FC5906-17, FC5906-18, FC5906-19, FC5906-20, FC5906-
23
CAS No.Surrogate Recoveries MS MSD FC5906-23 Limits
17060-07-0 1,2-Dichloroethane-D4 101%102%103%70-130%
2037-26-5 Toluene-D8 100%100%103%70-130%
460-00-4 4-Bromofluorobenzene 97%99%101%70-130%
* = Outside of Control Limits.
136 of 154
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4
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2
SGS North America Inc.
GC Volatiles
QC Data Summaries
Includes the following where applicable:
 Method Blank Summaries
 Blank Spike Summaries
 Matrix Spike and Duplicate Summaries
Orlando, FL
Section 6
137 of 154
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6
Method Blank Summary Page 1 of 1
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLL2863-MB LL82387.D 1 05/15/23 SS n/a n/a GLL2863
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FC5906-1, FC5906-3, FC5906-4
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane ND 0.50 0.16 ug/l
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6.
1
.
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Method Blank Summary Page 1 of 1
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLL2864-MB LL82420.D 1 05/16/23 SS n/a n/a GLL2864
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FC5906-5, FC5906-7, FC5906-17, FC5906-19, FC5906-20, FC5906-21, FC5906-22, FC5906-23
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane ND 0.50 0.16 ug/l
139 of 154
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6.
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Method Blank Summary Page 1 of 1
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLL2865-MB LL82459.D 1 05/18/23 JR n/a n/a GLL2865
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FC5906-6, FC5906-18
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane ND 0.50 0.16 ug/l
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Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLL2863-BS LL82384.D 1 05/15/23 SS n/a n/a GLL2863
GLL2863-BSD LL82385.D 1 05/15/23 SS n/a n/a GLL2863
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FC5906-1, FC5906-3, FC5906-4
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
74-82-8 Methane 108 110 102 113 105 3 62-139/30
* = Outside of Control Limits.
141 of 154
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6
6.
2
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1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLL2864-BS LL82417.D 1 05/16/23 SS n/a n/a GLL2864
GLL2864-BSD LL82418.D 1 05/16/23 SS n/a n/a GLL2864
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FC5906-5, FC5906-7, FC5906-17, FC5906-19, FC5906-20, FC5906-21, FC5906-22, FC5906-23
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
74-82-8 Methane 108 111 103 115 106 4 62-139/30
* = Outside of Control Limits.
142 of 154
FC5906
6
6.
2
.
2
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLL2865-BS LL82448.D 1 05/18/23 JR n/a n/a GLL2865
GLL2865-BSD LL82449.D 1 05/18/23 JR n/a n/a GLL2865
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FC5906-6, FC5906-18
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
74-82-8 Methane 108 109 101 112 104 3 62-139/30
* = Outside of Control Limits.
143 of 154
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6
6.
2
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3
Matrix Spike Summary Page 1 of 1
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC5891-3MS LL82397.D 20 05/15/23 SS n/a n/a GLL2863
FC5891-3 LL82389.D 1 05/15/23 SS n/a n/a GLL2863
FC5891-3 LL82393.D 20 05/15/23 SS n/a n/a GLL2863
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FC5906-1, FC5906-3, FC5906-4
FC5891-3 Spike MS MS
CAS No.Compound ug/l Q ug/l ug/l %Limits
74-82-8 Methane 3370 a 2160 5510 99 62-139
(a) Result is from Run #2.
* = Outside of Control Limits.
144 of 154
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6
6.
3
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Matrix Spike Summary Page 1 of 1
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC5924-1MS LL82440.D 1 05/16/23 SS n/a n/a GLL2864
FC5924-1 LL82434.D 1 05/16/23 SS n/a n/a GLL2864
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FC5906-5, FC5906-7, FC5906-17, FC5906-19, FC5906-20, FC5906-21, FC5906-22, FC5906-23
FC5924-1 Spike MS MS
CAS No.Compound ug/l Q ug/l ug/l %Limits
74-82-8 Methane 255 108 381 117 62-139
* = Outside of Control Limits.
145 of 154
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3
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Matrix Spike Summary Page 1 of 1
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC5909-16MS LL82478.D 1 05/18/23 JR n/a n/a GLL2865
FC5909-16 LL82463.D 1 05/18/23 JR n/a n/a GLL2865
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FC5906-6, FC5906-18
FC5909-16 Spike MS MS
CAS No.Compound ug/l Q ug/l ug/l %Limits
74-82-8 Methane 0.67 108 113 104 62-139
* = Outside of Control Limits.
146 of 154
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3
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Duplicate Summary Page 1 of 1
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC5891-3DUP LL82396.D 20 05/15/23 SS n/a n/a GLL2863
FC5891-3 LL82389.D 1 05/15/23 SS n/a n/a GLL2863
FC5891-3 LL82393.D 20 05/15/23 SS n/a n/a GLL2863
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FC5906-1, FC5906-3, FC5906-4
FC5891-3 DUP
CAS No.Compound ug/l Q ug/l Q RPD Limits
74-82-8 Methane 3370 a 4250 23 30
(a) Result is from Run #2.
* = Outside of Control Limits.
147 of 154
FC5906
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6.
4
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Duplicate Summary Page 1 of 1
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC5924-1DUP LL82437.D 1 05/16/23 SS n/a n/a GLL2864
FC5924-1 LL82434.D 1 05/16/23 SS n/a n/a GLL2864
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FC5906-5, FC5906-7, FC5906-17, FC5906-19, FC5906-20, FC5906-21, FC5906-22, FC5906-23
FC5924-1 DUP
CAS No.Compound ug/l Q ug/l Q RPD Limits
74-82-8 Methane 255 300 16 30
* = Outside of Control Limits.
148 of 154
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6.
4
.
2
Duplicate Summary Page 1 of 1
Job Number:FC5906
Account:GRINCC GRI (Geological Resources Inc.)
Project:J Mart; 5654 NC Hwy 87 S, Sanford, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC5909-8DUP LL82472.D 1 05/18/23 JR n/a n/a GLL2865
FC5909-8 LL82454.D 1 05/18/23 JR n/a n/a GLL2865
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FC5906-6, FC5906-18
FC5909-8 DUP
CAS No.Compound ug/l Q ug/l Q RPD Limits
74-82-8 Methane 728 894 20 30
* = Outside of Control Limits.
149 of 154
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6
6.
4
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3
SGS North America Inc.
General Chemistry
QC Data Summaries
Includes the following where applicable:
 Method Blank and Blank Spike Summaries
 Duplicate Summaries
 Matrix Spike Summaries
Orlando, FL
Section 7
150 of 154
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METHOD BLANK AND SPIKE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FC5906
Account: GRINCC - GRI (Geological Resources Inc.)
Project: J Mart; 5654 NC Hwy 87 S, Sanford, NC
MB Spike BSP BSP QC
Analyte Batch ID RL Result Units Amount Result %Recov Limits
Chloride GP38725/GN94144 2.0 0.0 mg/l 50 49.6 99.2 90-110%
Iron, Ferrous GN94148 0.10 0.0 mg/l 0.500 0.51 102.1 82-115%
Nitrogen, Nitrate GP38725/GN94144 0.10 0.0 mg/l 2.5 2.65 106.0 90-110%
Nitrogen, Nitrite GP38725/GN94144 0.10 0.0 mg/l 2.5 2.63 105.2 90-110%
Sulfate GP38725/GN94144 2.0 0.0 mg/l 50 48.7 97.4 90-110%
Associated Samples:
Batch GN94148: FC5906-1, FC5906-3, FC5906-4, FC5906-5, FC5906-6, FC5906-7, FC5906-17, FC5906-18, FC5906-19, FC5906-20,
FC5906-21, FC5906-22, FC5906-23
Batch GP38725: FC5906-1, FC5906-3, FC5906-4, FC5906-5, FC5906-6, FC5906-7, FC5906-17, FC5906-18, FC5906-19, FC5906-20,
FC5906-21, FC5906-22, FC5906-23
(*) Outside of QC limits
__________________________________________________________________________________________________________________________
Page 1
151 of 154
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DUPLICATE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FC5906
Account: GRINCC - GRI (Geological Resources Inc.)
Project: J Mart; 5654 NC Hwy 87 S, Sanford, NC
QC Original DUP QC
Analyte Batch ID Sample Units Result Result RPD Limits
Iron, Ferrous GN94148 FC5906-21 mg/l 0.0 0.0 73.5(a) 0-31%
Iron, Ferrous GN94148 FC5906-20 mg/l 0.070 0.054 25.4 0-31%
Associated Samples:
Batch GN94148: FC5906-1, FC5906-3, FC5906-4, FC5906-5, FC5906-6, FC5906-7, FC5906-17, FC5906-18, FC5906-19, FC5906-20,
FC5906-21, FC5906-22, FC5906-23
(*) Outside of QC limits
(a) RPD acceptable due to low duplicate and sample concentrations.
__________________________________________________________________________________________________________________________
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FC5906
7
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MATRIX SPIKE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FC5906
Account: GRINCC - GRI (Geological Resources Inc.)
Project: J Mart; 5654 NC Hwy 87 S, Sanford, NC
QC Original Spike MS QC
Analyte Batch ID Sample Units Result Amount Result %Rec Limits
Chloride GP38725/GN94144 FC5906-1 mg/l 4.5 50 52.9 96.8 90-110%
Nitrogen, Nitrate GP38725/GN94144 FC5906-1 mg/l 0.13 2.5 2.4 90.8 90-110%
Nitrogen, Nitrite GP38725/GN94144 FC5906-1 mg/l 0.0 2.5 2.5 100.0 90-110%
Sulfate GP38725/GN94144 FC5906-1 mg/l 0.0 50 47.3 94.6 90-110%
Associated Samples:
Batch GP38725: FC5906-1, FC5906-3, FC5906-4, FC5906-5, FC5906-6, FC5906-7, FC5906-17, FC5906-18, FC5906-19, FC5906-20,
FC5906-21, FC5906-22, FC5906-23
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
__________________________________________________________________________________________________________________________
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FC5906
7
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MATRIX SPIKE DUPLICATE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FC5906
Account: GRINCC - GRI (Geological Resources Inc.)
Project: J Mart; 5654 NC Hwy 87 S, Sanford, NC
QC Original Spike MSD QC
Analyte Batch ID Sample Units Result Amount Result RPD Limit
Chloride GP38725/GN94144 FC5906-1 mg/l 4.5 50 52.9 0.0 15%
Nitrogen, Nitrate GP38725/GN94144 FC5906-1 mg/l 0.13 2.5 2.4 0.0 15%
Nitrogen, Nitrite GP38725/GN94144 FC5906-1 mg/l 0.0 2.5 2.5 0.0 15%
Sulfate GP38725/GN94144 FC5906-1 mg/l 0.0 50 47.2 0.2 15%
Associated Samples:
Batch GP38725: FC5906-1, FC5906-3, FC5906-4, FC5906-5, FC5906-6, FC5906-7, FC5906-17, FC5906-18, FC5906-19, FC5906-20,
FC5906-21, FC5906-22, FC5906-23
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
__________________________________________________________________________________________________________________________
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7
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APPENDIX C
Contaminant Mass Calculations

Area ID Well IDs Area (ft²)
Average Well
Depth
(ft.)
Average
Depth to
Water
(ft.)
Water Column
Height (ft)Volume (ft³)Volume (L)Effective
Porosity
Effective
Volume (L)
MW-3
MW-4
MW-1
MW-2
MW-5
MW-13
MW-14
MW-18
MW-20
Area Date Well Benzene
(μ/L)
Toluene
(μ/L)
Ethylbenzene
(μ/L)
Xylenes
(μ/L)
MTBE
(μ/L)
Naphthalene
(μ/L)
Total
(μ/L)
DTW
(ft.)
Average Water
Column Height
(ft.)
Total Average
Mass (g)Percent Red.To Date Red.
MW-3 7,520.00 365.00 2,240.00 8,050.00 2,270.00 676.00 21,121.00 21.25
MW-4 17,000.00 2,350.00 3,370.00 18,500.00 12,500.00 1,050.00 54,770.00 23.42
Avg.12,260.00 1,357.50 2,805.00 13,275.00 7,385.00 863.00 37,945.50 22.34
MW-3 4,220.00 92.90 539.00 1,630.00 1,310.00 373.00 8,164.90 26.74
MW-4 17,200.00 895.00 2,340.00 8,850.00 19,100.00 941.00 49,326.00 29.33
Avg.10,710.00 493.95 1,439.50 5,240.00 10,205.00 657.00 28,745.5 28.04
MW-3 5,040.00 426.00 2,380.00 8,380.00 1,140.00 602.00 17,968.00 19.47
MW-4 10,300.00 8,790.00 3,620.00 19,300.00 4,020.00 817.00 46,847.00 22.00
Avg.7,670.00 4,608.00 3,000.00 13,840.00 2,580.00 709.50 32,407.5 20.74
MW-3 4,470.00 268.00 2,130.00 7,700.00 1,060.00 675.00 16,303.00 17.98
MW-4 8,690.00 15,600.00 3,630.00 19,800.00 2,150.00 713.00 50,583.00 20.86
Avg.6,580.00 7,934.00 2,880.00 13,750.00 1,605.00 694.00 33,443.0 19.42
MW-3 4,370.00 307.00 2,300.00 9,520.00 920.00 682.00 18,099.00 19.12
MW-4 9,780.00 21,900.00 4,230.00 22,900.00 2,120.00 607.00 61,537.00 21.24
Avg.7,075.00 11,103.50 3,265.00 16,210.00 1,520.00 644.50 39,818.0 20.18
MW-3 3,110.00 2,160.00 2,310.00 11,900.00 713.00 661.00 20,854.0 16.62
MW-4 8,650.00 20,100 .00 3,730.00 20,100.00 3,340.00 792.00 36,612.0 18.42
Avg.5,880.00 2,160.00 3,020.00 16,000.00 2,026.50 726.50 28,733.0 17.52
MW-3 1310 38.9 J 245 794 261 90.7 2,700.7 20.27
MW-4 17500 1620 3550 15,100 13300 831 51,901.0 22.59
Avg.9,405.00 1,620.00 1,897.50 7,947.00 6,780.50 460.85 27,300.9 21.43
MW-3 1560 106 429 1540 253 121 4,009.0 20.64
MW-4 16500 3830 3930 17,500 11100 1090 53,950.0 22.92
Avg.9,030.00 1,968.00 2,179.50 9,520.00 5,676.50 605.50 28,979.5 21.78
MW-3 820.00 39.90 97.10 200.00 126.00 24.20 1,307.2 23.23
MW-4 15,700.00 646.00 2,770.00 9,120.00 9,530.00 682.00 38,448.0 25.32
Avg.8,260.00 342.95 1,433.55 4,660.00 4,828.00 353.10 19,877.6 24.28
MW-3 957 18.4 359 830 196 107 2,467.4 19.60
MW-4 5,930 4,220 2,460 13,200 1,830 698 28,338.0 21.34
Avg.3,443.50 2,119.20 1,409.50 7,015.00 1,013.00 402.50 15,402.7 20.47
MW-1 260.00 1,260.00 257.00 1,300.00 21.40 79.50 3,177.90 29.12
MW-2 0.73 0.54 0.00 1.60 0.50 0.20 3.57 22.96
MW-5 ---------------------
MW-13 ------------------------
MW-14 ------------------------
MW-18 ------------------------
MW-20 ------------------------
Avg.130.37 630.27 128.50 650.80 10.95 39.85 1,591 26.04
MW-1 143.00 105.00 13.20 67.90 5.00 0.00 334 27.96
MW-2 0.14 0.00 0.00 0.36 0.00 0.00 1 28.73
MW-5 10.50 0.00 0.00 0.00 632.00 0.00 643 30.09
MW-13 0.49 0.00 0.00 0.00 234.00 0.00 234 25.85
MW-14 0.00 0.00 0.00 0.00 14.90 0.00 15 28.06
MW-18 30.50 0.00 0.00 30.60 288.00 3.80 353 24.17
MW-20 ------------------------
Avg.30.77 17.50 2.20 16.48 195.65 0.63 263 27.48
12/20/22
4381.65
1,832.28
85%
05/26/20
40.8%53.4%
-17.7%
10.38 266.35
---
85%
-4.1%
18.57 3227.56 21.5%
3.6%
11.82
5024.23 -14.7%
---
APPENDIX C
CONTAMINANT MASS CALCULATIONS
J MART (INCIDENT NO. 42035)
613,23321,65619.271,124.11 122,647
0.20
37.86
40 22.33
26.042 10,741,631379,33822.0517,206.9 2,148,326
18.2%
24.4%
------4267.37
48.7%48.7%
-10.2%-2.7%
6.9%-81.5%3974.67
2189.62
15.73 1989.95
11/28/18
05/04/17
01/24/18
4112.10
17.67
11.97
20.58
19.27
22.4806/29/21
08/14/19
11/09/20 19.82
01/25/22
Area 1
05/08/23 19.53 1915.08 3.8%55.1%
21.2%
Area 2
07/28/22 18.22 3361.45
05/04/17
Area ID Well IDs Area (ft²)
Average Well
Depth
(ft.)
Average
Depth to
Water
(ft.)
Water Column
Height (ft)Volume (ft³)Volume (L)Effective
Porosity
Effective
Volume (L)
MW-3
MW-4
MW-1
MW-2
MW-5
MW-13
MW-14
MW-18
MW-20
Area Date Well Benzene
(μ/L)
Toluene
(μ/L)
Ethylbenzene
(μ/L)
Xylenes
(μ/L)
MTBE
(μ/L)
Naphthalene
(μ/L)
Total
(μ/L)
DTW
(ft.)
Average Water
Column Height
(ft.)
Total Average
Mass (g)Percent Red.To Date Red.
APPENDIX C
CONTAMINANT MASS CALCULATIONS
J MART (INCIDENT NO. 42035)
613,23321,65619.271,124.11 122,647
0.20
37.86
40 22.33
26.042 10,741,631379,33822.0517,206.9 2,148,326
MW-1 442.00 181.00 96.20 492.00 138.00 19.70 1368.90 20.79
MW-2 2.20 0.16 0.00 2.70 0.00 0.00 5.06 21.34
MW-5 0.00 0.00 0.00 0.00 245.00 0.00 245.00 23.16
MW-13 0.00 0.00 0.00 0.00 172.00 0.00 172.00 22.98
MW-14 0.00 0.00 0.00 0.00 21.80 0.00 21.80 24.86
MW-18 0.00 0.00 0.00 0.00 77.30 0.00 77.30 23.33
MW-20 0.00 0.00 0.00 0.00 31.70 0.00 31.70 24.22
Avg.63.46 25.88 13.74 70.67 97.97 2.81 274.54 22.95
MW-1 0.00 0.00 0.00 0.00 0.00 0.00 0.00 20.05
MW-2 4.50 0.27 0.00 7.00 0.00 0.00 11.77 20.69
MW-5 0.00 0.00 0.00 0.00 0.00 0.00 0.00 20.89
MW-13 0.00 0.00 0.00 0.00 16.70 0.00 16.70 18.29
MW-14 0.00 0.00 0.00 0.00 28.60 0.00 28.60 21.05
MW-18 0.00 0.00 0.00 0.00 17.60 0.00 17.60 19.70
MW-20 0.00 0.00 0.00 0.00 13.50 0.00 13.50 19.09
Avg.0.64 0.04 0.00 1.00 10.91 0.00 12.60 19.97
MW-1 0.00 0.00 0.00 0.00 0.00 0.00 0.00 20.36
MW-2 7.6 0.25 0.21 11.6 0.00 0.00 19.66 20.94
MW-5 0.00 0.00 0.00 0.00 0.00 0.00 0.00 21.52
MW-13 0.00 0.00 0.00 0.00 33.2 0.00 33.20 21.63
MW-14 0.00 0.16 0.16 0.84 33 0.00 34.16 23.74
MW-18 0.00 0.00 0.00 0.00 23.1 0.00 23.10 22.07
MW-20 0.00 0.00 0.00 0.00 15.7 0.00 15.70 20.72
Avg.1.09 0.06 0.05 1.78 15.00 0.00 17.97 21.57
MW-1 4,060 529 846 2220 352 198 8,205.00 17.54
MW-2 0 0 0 0 0 0 0.00 18.01
MW-5 ------------------------
MW-13 0 0 0 0 135 0 135.00 18.53
MW-14 0.18 0.860 0.14 0.37 8.2 0 9.06 19.45
MW-18 ------------------------
MW-20 ------------------------
Avg.1,015.05 132.47 211.54 555.09 123.80 49.50 2,087.27 18.38
05/26/20
08/14/19
-116%
21.96
-13783.5%
98%
14.91
99%
78%
94.5%
-49.7%
16.29 28.54
398.78
19.48 3,961.75
11/09/20
17.89
-29.9%
Area 2
(Cont.)
06/29/21
Area ID Well IDs Area (ft²)
Average Well
Depth
(ft.)
Average
Depth to
Water
(ft.)
Water Column
Height (ft)Volume (ft³)Volume (L)Effective
Porosity
Effective
Volume (L)
MW-3
MW-4
MW-1
MW-2
MW-5
MW-13
MW-14
MW-18
MW-20
Area Date Well Benzene
(μ/L)
Toluene
(μ/L)
Ethylbenzene
(μ/L)
Xylenes
(μ/L)
MTBE
(μ/L)
Naphthalene
(μ/L)
Total
(μ/L)
DTW
(ft.)
Average Water
Column Height
(ft.)
Total Average
Mass (g)Percent Red.To Date Red.
APPENDIX C
CONTAMINANT MASS CALCULATIONS
J MART (INCIDENT NO. 42035)
613,23321,65619.271,124.11 122,647
0.20
37.86
40 22.33
26.042 10,741,631379,33822.0517,206.9 2,148,326
MW-1 1.4 0 0.22 0 0.31 0 1.93 22.56
MW-2 0 0 0 0 0 0 0.00 22.14
MW-5 ------------------0.00 ---
MW-13 0 0 0 0 737 0 737.00 22.34
MW-14 0 0 0 0 8.5 0 8.50 24.13
MW-18 ------------------0.00 ---
MW-20 ------------------0.00 ---
Avg.0.35 0.00 0.06 0.00 186.45 0.00 106.78 22.79
MW-1 0.229 0 0 0 0 0 0.23 21.81
MW-2 0 0 0 0 0 0 0.00 22.46
MW-5 ------------------0.00 ---
MW-13 0.288 0 0 0.889 543 0 544.18 23.13
MW-14 0.738 0.354 0.434 2.04 5.24 0 8.81 25.21
MW-18 ------------------0.00 ---
MW-20 ------------------0.00 ---
Avg.0.31 0.09 0.11 0.73 137.06 0.00 79.03 23.15
MW-1 0.22 0.00 0.00 0.00 0.00 0.00 0.22 24.39
MW-2 0.00 0.00 0.00 0.00 0.00 0.00 0.00 25.01
MW-5 6.10 0.00 0.00 0.00 382.00 0.38 388.48 25.77
MW-13 0.00 0.00 0.00 0.00 720.00 0.00 720.00 25.35
MW-14 0.00 0.00 0.00 0.00 1.30 0.00 1.30 27.32
MW-18 1.20 0.00 0.00 0.80 260.00 0.00 262.00 25.44
MW-20 ------------------------
Avg.1.25 0.00 0.00 0.13 227.22 0.06 228.67 25.55
MW-1 1.70 2.40 1.10 7.20 0.23 0.25 12.88 19.61
MW-2 0.67 0.51 0.22 1.40 0.00 0.00 2.80 21.22
MW-5 0 0 0 0 1.80 0 1.80 20.91
MW-13 0 0 0 0.00 198.00 0 198.00 20.38
MW-14 0 0 0 0 2.90 0 2.90 22.41
MW-18 0 0 0 0 37.30 0 37.30 20.30
MW-20 0 0 0 0 82.10 0.00 82.10 18.71
Avg.1.19 1.46 0.66 2.87 46.05 0.08 48.25 20.51
Date Percent Reduction To Date
05/04/17
01/24/18;
05/02/18;
11/28/18
07/30/19
05/26/20
11/09/20
06/29/21
01/25/22
07/28/22
12/20/22
05/08/23
Notes:
• Baseline contaminant mass was calculated using the maximum water column observed as well as the maximum historical dissolved phase contaminant concentrations.
• Height of the water column is calculated by subtracting the average depth to water from the average well depth of the referenced monitoring wells
• Volume of the contaminant plume is calculated by multiplying the area of the plume by the average height of the water column during each sampling event
• Effective porosity is assumed based on the sub-surface soil profile obtained from well construction records and soil boring logs
• Total mass was calculated by multiplying the total contaminant concentrations for the sampling event with effective volume
14.02 2,264 34.8%62.9%
-0.7%
01/25/22
16.46 3,475 -2.7%43.0%
-78.1%
Total Contaminant Mass (g)Percent Reduction Compared
to Previous Event
27.8%94%
12.31 274.38 -142.2%12/20/22 85%
113.27
---6,100
2,456
07/28/22
14.74
11.17
Average Water Column
Height
(ft.)
60%
---
60%
18.44 1,997 11.8%67.3%
-14.7%5,05318.06 17.2%
15.07
16.82 3,384 58.1%44.5%
-32.4%20.98 8,074 -59.8%
14.71
4,37317.09
19.24 27.8%4,404
28.3%
05/08/23 17.35 81.61 70.3%96%
Area 2
(Cont.)
156.78 96.0%91%