FA-2841_29112_CA_HRE_20230920_WSW3

September 21, 2023 TO: Mike Haseltine
Fayetteville Regional Office NC UST Section RE: Health Risk Evaluation Incident # 29112
5350 Cedar Creek Road Well Sampling Results Fayetteville, NC During this sampling event, one contaminant was detected in the well water. The standards used to determine if the water is suitable for drinking and cooking are the United States Environmental
Protection Agency’s Maximum Contaminant Levels (MCLs) or, if no MCLs exist, North Carolina Groundwater Standards (2L). If the contaminant concentration exceeds the applicable standard for using the water for drinking and cooking, the contaminant concentration is further analyzed to determine if the water is suitable for
other household uses, such as showering, bathing, washing dishes, flushing toilets, and hand washing. The chart below compares the detected contaminant concentration with the applicable standard:
Sample ID Contaminant Concentration (µg/L) MCL (µg/L) 2L (µg/L)
µg/L – Stands for micrograms of contaminant per liter of water and is roughly equivalent to parts per
billion.
* This value is an Interim Maximum Allowable Concentration (IMAC).
RECOMMENDATION: The detected contaminant did not exceed the applicable water standard.
Therefore, no restrictions on the use of this water are recommended at this time.
David Lilley, Environmental Toxicologist
Division of Waste Management, NCDEQ
North Carolina Department of Environmental Quality | Division of Waste Management
Fayetteville Regional Office | 225 Green Street | Suite 714 | Systel Building | Fayetteville,
NC 28301 | (910) 433­3300
September 20, 2023
MEMORANDUM
TO: Dave Lilley, Environmental Toxicologist, Division of Waste Management, 1646 Mail
Service Center, Raleigh, NC 27699-1646
FROM: Mike Haseltine, Fayetteville Regional Office, UST Section, Division of Waste
Management
SUBJECT: Request for Health Risk Evaluation of Water Supply
Tracking ID: 29112
Enclosed please find the analytical results for a water sample collected on June 20, 2023, from potable
water supply well, identified as WSW-3 located at 5350 Cedar Creek Road, Fayetteville, Cumberland
County. Please perform a health risk evaluation and send the evaluation with your recommendation and a
copy of this memo to me. I will then forward the health risk evaluation and recommendation to any well
users.
If you have questions or need additional information, please contact me at the address or telephone number
below. Thank you for your assistance.
Attachment(s): SGS Laboratory Report
07/03/23
Technical Report for
GRI (Geological Resources Inc.)
Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
5426
SGS Job Number: FC7092
Sampling Date: 06/20/23
Report to:
[e-mail]
[e-mail]
[e-mail]
ATTN: Distribution6
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, IL, UT, VT, WA, WI, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc.  4405 Vineland Road  Suite C-15  Orlando, FL 32811  tel: [phone] 
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable unless noted
in the narrative, comments or footnotes.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Orlando, FL 07/03/23
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Automated Report
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Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................8
3.1: FC7092-1: TRIP BLANK .............................................................................................9
3.2: FC7092-2: DW-1 ..........................................................................................................11
3.3: FC7092-3: MW-1 ..........................................................................................................16
3.4: FC7092-4: MW-2 ..........................................................................................................21
3.5: FC7092-5: MW-3 ..........................................................................................................26
3.6: FC7092-6: MW-4 ..........................................................................................................31
3.7: FC7092-7: MW-5 ..........................................................................................................36
3.8: FC7092-8: MW-6 ..........................................................................................................41
3.9: FC7092-9: MW-7 ..........................................................................................................46
3.10: FC7092-10: WSW-1 ...................................................................................................51
3.11: FC7092-11: WSW-14 ..................................................................................................54
3.12: FC7092-12: WSW-3 ...................................................................................................57
Section 4: Misc. Forms ............................................................................................................60
4.1: Chain of Custody ...........................................................................................................61
Section 5: MS Volatiles - QC Data Summaries .....................................................................63
5.1: Method Blank Summary ................................................................................................64
5.2: Blank Spike Summary ...................................................................................................70
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................76
Section 6: GC Volatiles - QC Data Summaries .....................................................................82
6.1: Method Blank Summary ................................................................................................83
6.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................84
6.3: Matrix Spike Summary ..................................................................................................85
6.4: Duplicate Summary .......................................................................................................86
Section 7: General Chemistry - QC Data Summaries ..........................................................87
7.1: Method Blank and Spike Results Summary ..................................................................88
7.2: Duplicate Results Summary ..........................................................................................89
7.3: Matrix Spike Results Summary .....................................................................................90
7.4: Matrix Spike Duplicate Results Summary ....................................................................91
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SGS LabLink@15:15 03-Jul-2023
Sample Summary
GRI (Geological Resources Inc.)
Job No:FC7092
Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Project No: 5426
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FC7092-1 06/20/23 08:58 JB 06/21/23 AQ Trip Blank Water TRIP BLANK
FC7092-2 06/20/23 09:51 JB 06/21/23 AQ Ground Water DW-1
FC7092-3 06/20/23 10:07 JB 06/21/23 AQ Ground Water MW-1
FC7092-4 06/20/23 10:23 JB 06/21/23 AQ Ground Water MW-2
FC7092-5 06/20/23 10:39 JB 06/21/23 AQ Ground Water MW-3
FC7092-6 06/20/23 10:55 JB 06/21/23 AQ Ground Water MW-4
FC7092-7 06/20/23 11:12 JB 06/21/23 AQ Ground Water MW-5
FC7092-8 06/20/23 11:31 JB 06/21/23 AQ Ground Water MW-6
FC7092-9 06/20/23 11:47 JB 06/21/23 AQ Ground Water MW-7
FC7092-10 06/20/23 12:02 JB 06/21/23 AQ Ground Water WSW-1
FC7092-11 06/20/23 12:13 JB 06/21/23 AQ Ground Water WSW-14
FC7092-12 06/20/23 12:22 JB 06/21/23 AQ Ground Water WSW-3
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Summary of Hits Page 1 of 4
Job Number:FC7092
Account:GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Collected:06/20/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FC7092-1 TRIP BLANK
Methylene Chloride a 1.9 J 2.0 1.0 ug/l SM 6200B
Toluene 5.7 0.50 0.13 ug/l SM 6200B
FC7092-2 DW-1
Ethyl Alcohol b 118 100 65 ug/l SM 6200B
Nitrogen, Nitrate 0.24 0.10 mg/l EPA 300/SW846 9056A
Sulfate 11.3 2.0 mg/l EPA 300/SW846 9056A
FC7092-3 MW-1
Benzene 238 5.0 1.3 ug/l SM 6200B
Di-Isopropyl Ether 11.3 5.0 1.3 ug/l SM 6200B
Ethylbenzene 262 5.0 1.3 ug/l SM 6200B
Isopropylbenzene 4.8 J 5.0 1.3 ug/l SM 6200B
Methylene Chloride 12.5 J 20 10 ug/l SM 6200B
Naphthalene 83.9 5.0 1.3 ug/l SM 6200B
n-Propylbenzene 16.3 5.0 1.3 ug/l SM 6200B
Styrene 3.1 J 5.0 1.3 ug/l SM 6200B
Tert-Amyl Alcohol 299 100 20 ug/l SM 6200B
Toluene 1090 13 3.1 ug/l SM 6200B
1,2,4-Trimethylbenzene 215 5.0 1.3 ug/l SM 6200B
1,3,5-Trimethylbenzene 49.8 5.0 1.3 ug/l SM 6200B
m,p-Xylene 976 10 1.3 ug/l SM 6200B
o-Xylene 486 5.0 1.3 ug/l SM 6200B
Methane 695 0.50 0.16 ug/l RSKSOP-147/175
Iron, Ferrous c 0.77 0.50 mg/l SM3500FE B-11
Nitrogen, Nitrate 0.42 0.10 mg/l EPA 300/SW846 9056A
Sulfate 5.1 2.0 mg/l EPA 300/SW846 9056A
FC7092-4 MW-2
Benzene 11.5 0.50 0.13 ug/l SM 6200B
n-Butylbenzene 0.39 J 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 0.35 J 0.50 0.13 ug/l SM 6200B
Di-Isopropyl Ether 1.0 0.50 0.13 ug/l SM 6200B
Ethyl Alcohol d 65.1 J 100 65 ug/l SM 6200B
Ethylbenzene 15.1 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 1.1 0.50 0.13 ug/l SM 6200B
p-Isopropyltoluene 0.66 0.50 0.13 ug/l SM 6200B
Methylene Chloride a 1.0 J 2.0 1.0 ug/l SM 6200B
Naphthalene 10.2 0.50 0.13 ug/l SM 6200B
n-Propylbenzene 2.3 0.50 0.13 ug/l SM 6200B
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Summary of Hits Page 2 of 4
Job Number:FC7092
Account:GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Collected:06/20/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Tert-Amyl Alcohol 16.2 10 2.0 ug/l SM 6200B
Toluene 2.5 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 24.4 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 4.3 0.50 0.13 ug/l SM 6200B
m,p-Xylene 31.7 1.0 0.13 ug/l SM 6200B
o-Xylene 14.5 0.50 0.13 ug/l SM 6200B
Methane 178 0.50 0.16 ug/l RSKSOP-147/175
Iron, Ferrous c 2.3 0.50 mg/l SM3500FE B-11
Nitrogen, Nitrate 0.29 0.10 mg/l EPA 300/SW846 9056A
Sulfate 4.0 2.0 mg/l EPA 300/SW846 9056A
FC7092-5 MW-3
Ethyl Alcohol e 73.2 J 100 65 ug/l SM 6200B
Methane 1.5 0.50 0.16 ug/l RSKSOP-147/175
Nitrogen, Nitrate 0.20 0.10 mg/l EPA 300/SW846 9056A
Sulfate 5.8 2.0 mg/l EPA 300/SW846 9056A
FC7092-6 MW-4
Chloroform 0.51 0.50 0.13 ug/l SM 6200B
Nitrogen, Nitrate 0.73 0.10 mg/l EPA 300/SW846 9056A
Sulfate 7.7 2.0 mg/l EPA 300/SW846 9056A
FC7092-7 MW-5
Benzene 3.5 0.50 0.13 ug/l SM 6200B
n-Butylbenzene 0.36 J 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 0.89 0.50 0.13 ug/l SM 6200B
tert-Butylbenzene 0.23 J 0.50 0.13 ug/l SM 6200B
Di-Isopropyl Ether 0.50 0.50 0.13 ug/l SM 6200B
Ethyl Alcohol e 99.6 J 100 65 ug/l SM 6200B
Ethylbenzene 17.7 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 6.7 0.50 0.13 ug/l SM 6200B
p-Isopropyltoluene 0.89 0.50 0.13 ug/l SM 6200B
Naphthalene 9.2 0.50 0.13 ug/l SM 6200B
n-Propylbenzene 2.8 0.50 0.13 ug/l SM 6200B
Tert-Amyl Alcohol 12.1 10 2.0 ug/l SM 6200B
Toluene 3.6 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 20.3 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 1.9 0.50 0.13 ug/l SM 6200B
m,p-Xylene 17.1 1.0 0.13 ug/l SM 6200B
o-Xylene 12.4 0.50 0.13 ug/l SM 6200B
Xylene (total)29.5 1.5 0.25 ug/l SM 6200B
Methane 275 0.50 0.16 ug/l RSKSOP-147/175
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Summary of Hits Page 3 of 4
Job Number:FC7092
Account:GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Collected:06/20/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Iron, Ferrous c 0.90 0.50 mg/l SM3500FE B-11
FC7092-8 MW-6
Benzene 3.5 0.50 0.13 ug/l SM 6200B
n-Butylbenzene 0.36 J 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 0.92 0.50 0.13 ug/l SM 6200B
tert-Butylbenzene 0.24 J 0.50 0.13 ug/l SM 6200B
Di-Isopropyl Ether 0.52 0.50 0.13 ug/l SM 6200B
Ethylbenzene 18.7 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 6.8 0.50 0.13 ug/l SM 6200B
Naphthalene 9.2 0.50 0.13 ug/l SM 6200B
n-Propylbenzene 3.0 0.50 0.13 ug/l SM 6200B
Tert-Amyl Alcohol 13.9 10 2.0 ug/l SM 6200B
Toluene 3.7 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 20.5 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 2.1 0.50 0.13 ug/l SM 6200B
m,p-Xylene 17.9 1.0 0.13 ug/l SM 6200B
o-Xylene 13.0 0.50 0.13 ug/l SM 6200B
Methane 0.73 0.50 0.16 ug/l RSKSOP-147/175
Nitrogen, Nitrate 0.50 0.10 mg/l EPA 300/SW846 9056A
Sulfate 4.1 2.0 mg/l EPA 300/SW846 9056A
FC7092-9 MW-7
Ethyl Alcohol e 68.2 J 100 65 ug/l SM 6200B
Methane 3.7 0.50 0.16 ug/l RSKSOP-147/175
Nitrogen, Nitrate 0.41 0.10 mg/l EPA 300/SW846 9056A
Sulfate 3.9 2.0 mg/l EPA 300/SW846 9056A
FC7092-10 WSW-1
No hits reported in this sample.
FC7092-11 WSW-14
Ethyl Alcohol e 132 100 65 ug/l SM 6200B
Methyl Chloride 0.21 J 0.50 0.20 ug/l SM 6200B
FC7092-12 WSW-3
Ethyl Alcohol e 82.2 J 100 65 ug/l SM 6200B
(a) Suspected laboratory contaminant.
(b) Associated CCV and BS recovery outside control limits high. Insufficient sample avaliable for re-analysis.
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Summary of Hits Page 4 of 4
Job Number:FC7092
Account:GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Collected:06/20/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
(c) Field analysis required. Received out of hold time and analyzed by request.
(d) Associated BS recovery outside control limits high. Insufficient sample avaliable for re-analysis.
(e) Associated CCV and BS outside control limits high. Insufficient sample available for re-analysis.
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Sample Results
Report of Analysis
Orlando, FL
Section 3
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Report of Analysis Page 1 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FC7092-1 Date Sampled:06/20/23
Matrix:AQ - Trip Blank Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1641.D 1 06/22/23 15:35 AK n/a n/a V3A82
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FC7092-1 Date Sampled:06/20/23
Matrix:AQ - Trip Blank Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride a 1.9 2.0 1.0 ug/l J
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 5.7 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
(a) Suspected laboratory contaminant.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:DW-1
Lab Sample ID:FC7092-2 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1686.D 1 06/27/23 10:56 AK n/a n/a V3A84
Run #2 a 3A1642.D 1 06/22/23 15:59 AK n/a n/a V3A82
Purge Volume
Run #1 5.0 ml
Run #2 5.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:DW-1
Lab Sample ID:FC7092-2 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol b 118 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:DW-1
Lab Sample ID:FC7092-2 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 107%107%70-130%
2037-26-5 Toluene-D8 99%105%70-130%
460-00-4 4-Bromofluorobenzene 100%99%70-130%
(a) Confirmation run.
(b) Associated CCV and BS recovery outside control limits high. Insufficient sample avaliable for re-analysis.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:DW-1
Lab Sample ID:FC7092-2 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:RSKSOP-147/175 Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL83227.D 1 06/26/23 11:03 SS n/a n/a GLL2891
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 21 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane ND 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:DW-1
Lab Sample ID:FC7092-2 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a <0.10 0.10 mg/l 1 07/02/23 13:20 FN SM3500FE B-11
Nitrogen, Nitrate 0.24 0.10 mg/l 1 06/21/23 17:46 JB EPA 300/SW846 9056A
Sulfate 11.3 2.0 mg/l 1 06/21/23 17:46 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
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Client Sample ID:MW-1
Lab Sample ID:FC7092-3 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1643.D 10 06/22/23 16:23 AK n/a n/a V3A82
Run #2 3A1687.D 25 06/27/23 11:20 AK n/a n/a V3A84
Purge Volume
Run #1 5.0 ml
Run #2 5.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 238 5.0 1.3 ug/l
108-86-1 Bromobenzene ND 5.0 1.3 ug/l
74-97-5 Bromochloromethane ND 5.0 1.3 ug/l
75-27-4 Bromodichloromethane ND 5.0 1.3 ug/l
75-25-2 Bromoform ND 5.0 1.3 ug/l
104-51-8 n-Butylbenzene ND 5.0 1.3 ug/l
135-98-8 sec-Butylbenzene ND 5.0 1.3 ug/l
98-06-6 tert-Butylbenzene ND 5.0 1.3 ug/l
56-23-5 Carbon Tetrachloride ND 5.0 1.3 ug/l
108-90-7 Chlorobenzene ND 5.0 1.3 ug/l
75-00-3 Chloroethane ND 5.0 2.0 ug/l
67-66-3 Chloroform ND 5.0 1.3 ug/l
95-49-8 o-Chlorotoluene ND 5.0 1.3 ug/l
106-43-4 p-Chlorotoluene ND 5.0 1.3 ug/l
124-48-1 Dibromochloromethane ND 5.0 1.3 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 2.5 ug/l
106-93-4 1,2-Dibromoethane ND 5.0 1.3 ug/l
75-71-8 Dichlorodifluoromethane ND 5.0 2.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 5.0 1.3 ug/l
541-73-1 1,3-Dichlorobenzene ND 5.0 1.3 ug/l
106-46-7 1,4-Dichlorobenzene ND 5.0 1.3 ug/l
75-34-3 1,1-Dichloroethane ND 5.0 1.3 ug/l
107-06-2 1,2-Dichloroethane ND 5.0 1.3 ug/l
75-35-4 1,1-Dichloroethylene ND 5.0 1.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.3 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.3 ug/l
78-87-5 1,2-Dichloropropane ND 5.0 1.3 ug/l
142-28-9 1,3-Dichloropropane ND 5.0 1.3 ug/l
594-20-7 2,2-Dichloropropane ND 5.0 1.3 ug/l
563-58-6 1,1-Dichloropropene ND 5.0 1.3 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-1
Lab Sample ID:FC7092-3 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 11.3 5.0 1.3 ug/l
64-17-5 Ethyl Alcohol a ND 1000 650 ug/l
100-41-4 Ethylbenzene 262 5.0 1.3 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 5.0 1.3 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 1.3 ug/l
98-82-8 Isopropylbenzene 4.8 5.0 1.3 ug/l J
99-87-6 p-Isopropyltoluene ND 5.0 1.3 ug/l
74-83-9 Methyl Bromide ND 5.0 2.0 ug/l
74-87-3 Methyl Chloride ND 5.0 2.0 ug/l
74-95-3 Methylene Bromide ND 5.0 1.3 ug/l
75-09-2 Methylene Chloride 12.5 20 10 ug/l J
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.3 ug/l
91-20-3 Naphthalene 83.9 5.0 1.3 ug/l
103-65-1 n-Propylbenzene 16.3 5.0 1.3 ug/l
100-42-5 Styrene 3.1 5.0 1.3 ug/l J
75-85-4 Tert-Amyl Alcohol 299 100 20 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 10 2.0 ug/l
75-65-0 Tert-Butyl Alcohol ND 100 20 ug/l
762-75-4 Tert-Butyl Formate ND 100 20 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.3 ug/l
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/l
108-88-3 Toluene 1090 b 13 3.1 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.3 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 5.0 1.3 ug/l
79-00-5 1,1,2-Trichloroethane ND 5.0 1.3 ug/l
79-01-6 Trichloroethylene ND 5.0 1.3 ug/l
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/l
95-63-6 1,2,4-Trimethylbenzene 215 5.0 1.3 ug/l
108-67-8 1,3,5-Trimethylbenzene 49.8 5.0 1.3 ug/l
75-01-4 Vinyl Chloride ND 5.0 1.3 ug/l
m,p-Xylene 976 10 1.3 ug/l
95-47-6 o-Xylene 486 5.0 1.3 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 94%97%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%105%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-1
Lab Sample ID:FC7092-3 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 106%90%70-130%
460-00-4 4-Bromofluorobenzene 102%99%70-130%
(a) Associated BS recovery outside control limits high, sample is ND.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-1
Lab Sample ID:FC7092-3 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:RSKSOP-147/175 Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL83228.D 1 06/26/23 11:19 SS n/a n/a GLL2891
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 21 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane 695 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-1
Lab Sample ID:FC7092-3 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a 0.77 0.50 mg/l 5 07/02/23 13:20 FN SM3500FE B-11
Nitrogen, Nitrate 0.42 0.10 mg/l 1 06/21/23 18:09 JB EPA 300/SW846 9056A
Sulfate 5.1 2.0 mg/l 1 06/21/23 18:09 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
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Client Sample ID:MW-2
Lab Sample ID:FC7092-4 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1644.D 1 06/22/23 16:46 AK n/a n/a V3A82
Run #2 a 3A1688.D 1 06/27/23 11:55 AK n/a n/a V3A84
Purge Volume
Run #1 5.0 ml
Run #2 5.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 11.5 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 0.39 0.50 0.13 ug/l J
135-98-8 sec-Butylbenzene 0.35 0.50 0.13 ug/l J
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-2
Lab Sample ID:FC7092-4 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 1.0 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol b 65.1 100 65 ug/l J
100-41-4 Ethylbenzene 15.1 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 1.1 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene 0.66 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride c 1.0 2.0 1.0 ug/l J
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene 10.2 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 2.3 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol 16.2 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 2.5 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 24.4 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 4.3 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 31.7 1.0 0.13 ug/l
95-47-6 o-Xylene 14.5 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 94%96%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%103%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-2
Lab Sample ID:FC7092-4 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 106%100%70-130%
460-00-4 4-Bromofluorobenzene 105%102%70-130%
(a) Confirmation run.
(b) Associated BS recovery outside control limits high. Insufficient sample avaliable for re-analysis.
(c) Suspected laboratory contaminant.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-2
Lab Sample ID:FC7092-4 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:RSKSOP-147/175 Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL83229.D 1 06/26/23 11:30 SS n/a n/a GLL2891
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 21 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane 178 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 91
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Report of Analysis Page 1 of 1
Client Sample ID:MW-2
Lab Sample ID:FC7092-4 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a 2.3 0.50 mg/l 5 07/02/23 13:20 FN SM3500FE B-11
Nitrogen, Nitrate 0.29 0.10 mg/l 1 06/21/23 18:31 JB EPA 300/SW846 9056A
Sulfate 4.0 2.0 mg/l 1 06/21/23 18:31 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
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Client Sample ID:MW-3
Lab Sample ID:FC7092-5 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1689.D 1 06/27/23 12:18 AK n/a n/a V3A84
Run #2 a 3A1645.D 1 06/22/23 17:10 AK n/a n/a V3A82
Purge Volume
Run #1 5.0 ml
Run #2 5.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-3
Lab Sample ID:FC7092-5 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol b 73.2 100 65 ug/l J
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-3
Lab Sample ID:FC7092-5 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 107%108%70-130%
2037-26-5 Toluene-D8 110%103%70-130%
460-00-4 4-Bromofluorobenzene 100%103%70-130%
(a) Confirmation run.
(b) Associated CCV and BS outside control limits high. Insufficient sample available for re-analysis.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-3
Lab Sample ID:FC7092-5 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:RSKSOP-147/175 Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL83230.D 1 06/26/23 11:40 SS n/a n/a GLL2891
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 21 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane 1.5 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-3
Lab Sample ID:FC7092-5 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a <0.50 0.50 mg/l 5 07/02/23 13:20 FN SM3500FE B-11
Nitrogen, Nitrate 0.20 0.10 mg/l 1 06/21/23 18:54 JB EPA 300/SW846 9056A
Sulfate 5.8 2.0 mg/l 1 06/21/23 18:54 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
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Client Sample ID:MW-4
Lab Sample ID:FC7092-6 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1646.D 1 06/22/23 17:34 AK n/a n/a V3A82
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform 0.51 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-4
Lab Sample ID:FC7092-6 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol a ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-4
Lab Sample ID:FC7092-6 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 105%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
(a) Associated BS recovery outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-4
Lab Sample ID:FC7092-6 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:RSKSOP-147/175 Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL83231.D 1 06/26/23 11:52 SS n/a n/a GLL2891
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 21 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane ND 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-4
Lab Sample ID:FC7092-6 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a <0.10 0.10 mg/l 1 07/02/23 13:20 FN SM3500FE B-11
Nitrogen, Nitrate 0.73 0.10 mg/l 1 06/21/23 19:17 JB EPA 300/SW846 9056A
Sulfate 7.7 2.0 mg/l 1 06/21/23 19:17 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
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Client Sample ID:MW-5
Lab Sample ID:FC7092-7 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1690.D 1 06/27/23 12:42 AK n/a n/a V3A84
Run #2 a 3A1647.D 1 06/22/23 17:58 AK n/a n/a V3A82
Purge Volume
Run #1 5.0 ml
Run #2 5.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 3.5 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 0.36 0.50 0.13 ug/l J
135-98-8 sec-Butylbenzene 0.89 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene 0.23 0.50 0.13 ug/l J
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-5
Lab Sample ID:FC7092-7 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.50 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol b 99.6 100 65 ug/l J
100-41-4 Ethylbenzene 17.7 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 6.7 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene 0.89 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene 9.2 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 2.8 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol 12.1 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 3.6 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 20.3 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 1.9 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 17.1 1.0 0.13 ug/l
95-47-6 o-Xylene 12.4 0.50 0.13 ug/l
1330-20-7 Xylene (total)29.5 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-5
Lab Sample ID:FC7092-7 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 105%116%70-130%
2037-26-5 Toluene-D8 104%102%70-130%
460-00-4 4-Bromofluorobenzene 103%102%70-130%
(a) Confirmation run.
(b) Associated CCV and BS outside control limits high. Insufficient sample available for re-analysis.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-5
Lab Sample ID:FC7092-7 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:RSKSOP-147/175 Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL83232.D 1 06/26/23 12:00 SS n/a n/a GLL2891
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 21 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane 275 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-5
Lab Sample ID:FC7092-7 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a 0.90 0.50 mg/l 5 07/02/23 13:20 FN SM3500FE B-11
Nitrogen, Nitrate <0.10 0.10 mg/l 1 06/21/23 19:39 JB EPA 300/SW846 9056A
Sulfate <2.0 2.0 mg/l 1 06/21/23 19:39 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
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Client Sample ID:MW-6
Lab Sample ID:FC7092-8 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1648.D 1 06/22/23 18:21 AK n/a n/a V3A82
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 3.5 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 0.36 0.50 0.13 ug/l J
135-98-8 sec-Butylbenzene 0.92 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene 0.24 0.50 0.13 ug/l J
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-6
Lab Sample ID:FC7092-8 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.52 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol a ND 100 65 ug/l
100-41-4 Ethylbenzene 18.7 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 6.8 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene 9.2 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 3.0 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol 13.9 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 3.7 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 20.5 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 2.1 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 17.9 1.0 0.13 ug/l
95-47-6 o-Xylene 13.0 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 95%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-6
Lab Sample ID:FC7092-8 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 105%70-130%
(a) Associated BS recovery outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-6
Lab Sample ID:FC7092-8 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:RSKSOP-147/175 Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL83235.D 1 06/26/23 13:46 SS n/a n/a GLL2891
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 21 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane 0.73 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-6
Lab Sample ID:FC7092-8 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a <0.10 0.10 mg/l 1 07/02/23 13:20 FN SM3500FE B-11
Nitrogen, Nitrate 0.50 0.10 mg/l 1 06/21/23 20:02 JB EPA 300/SW846 9056A
Sulfate 4.1 2.0 mg/l 1 06/21/23 20:02 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
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Client Sample ID:MW-7
Lab Sample ID:FC7092-9 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1691.D 1 06/27/23 13:06 AK n/a n/a V3A84
Run #2 a 3A1649.D 1 06/22/23 18:45 AK n/a n/a V3A82
Purge Volume
Run #1 5.0 ml
Run #2 5.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-7
Lab Sample ID:FC7092-9 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol b 68.2 100 65 ug/l J
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-7
Lab Sample ID:FC7092-9 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 103%110%70-130%
2037-26-5 Toluene-D8 101%102%70-130%
460-00-4 4-Bromofluorobenzene 104%104%70-130%
(a) Confirmation run.
(b) Associated CCV and BS outside control limits high. Insufficient sample available for re-analysis.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-7
Lab Sample ID:FC7092-9 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:RSKSOP-147/175 Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL83236.D 1 06/26/23 14:08 SS n/a n/a GLL2891
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 21 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane 3.7 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-7
Lab Sample ID:FC7092-9 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a <0.10 0.10 mg/l 1 07/02/23 13:20 FN SM3500FE B-11
Nitrogen, Nitrate 0.41 0.10 mg/l 1 06/21/23 21:55 JB EPA 300/SW846 9056A
Sulfate 3.9 2.0 mg/l 1 06/21/23 21:55 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
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Client Sample ID:WSW-1
Lab Sample ID:FC7092-10 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1650.D 1 06/22/23 19:09 AK n/a n/a V3A82
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:WSW-1
Lab Sample ID:FC7092-10 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol a ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 112%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:WSW-1
Lab Sample ID:FC7092-10 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 102%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
(a) Associated BS recovery outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:WSW-14
Lab Sample ID:FC7092-11 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1692.D 1 06/27/23 13:30 AK n/a n/a V3A84
Run #2 a 3A1651.D 1 06/22/23 19:33 AK n/a n/a V3A82
Purge Volume
Run #1 5.0 ml
Run #2 5.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:WSW-14
Lab Sample ID:FC7092-11 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol b 132 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride 0.21 0.50 0.20 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:WSW-14
Lab Sample ID:FC7092-11 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 109%115%70-130%
2037-26-5 Toluene-D8 98%102%70-130%
460-00-4 4-Bromofluorobenzene 106%103%70-130%
(a) Confirmation run.
(b) Associated CCV and BS outside control limits high. Insufficient sample available for re-analysis.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:WSW-3
Lab Sample ID:FC7092-12 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3A1693.D 1 06/27/23 13:54 AK n/a n/a V3A84
Run #2 a 3A1652.D 1 06/22/23 19:56 AK n/a n/a V3A82
Purge Volume
Run #1 5.0 ml
Run #2 5.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:WSW-3
Lab Sample ID:FC7092-12 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol b 82.2 100 65 ug/l J
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:WSW-3
Lab Sample ID:FC7092-12 Date Sampled:06/20/23
Matrix:AQ - Ground Water Date Received:06/21/23
Method:SM 6200B Percent Solids:n/a
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 108%116%70-130%
2037-26-5 Toluene-D8 103%102%70-130%
460-00-4 4-Bromofluorobenzene 103%103%70-130%
(a) Confirmation run.
(b) Associated CCV and BS outside control limits high. Insufficient sample available for re-analysis.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
 Chain of Custody
Orlando, FL
Section 4
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Page 1 of 2
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Job Number:FC7092 Client:GRI
Date / Time Received:6/21/2023 9:30:00 AM Delivery Method:FED EX
Project:5426
Airbill #'s:5707 9050 9991
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (4.1);
Cooler 1: (4.0);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230320 pH 10-12 Other: (Specify)pH 1.0 - 12.0 222221
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:-0.1; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:SHAYLAP Date:Date:6/21/2023 9:30:00 AM
FC7092: Chain of Custody
Page 2 of 2
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MS Volatiles
QC Data Summaries
Includes the following where applicable:
 Method Blank Summaries
 Blank Spike Summaries
 Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
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Method Blank Summary Page 1 of 3
Job Number:FC7092
Account:GRINCC GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A82-MB 3A1632.D 1 06/22/23 AK n/a n/a V3A82
The QC reported here applies to the following samples:Method: SM 6200B
FC7092-1, FC7092-3, FC7092-4, FC7092-6, FC7092-8, FC7092-10
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
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Method Blank Summary Page 2 of 3
Job Number:FC7092
Account:GRINCC GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A82-MB 3A1632.D 1 06/22/23 AK n/a n/a V3A82
The QC reported here applies to the following samples:Method: SM 6200B
FC7092-1, FC7092-3, FC7092-4, FC7092-6, FC7092-8, FC7092-10
CAS No.Compound Result RL MDL Units Q
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 99%70-130%
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Method Blank Summary Page 3 of 3
Job Number:FC7092
Account:GRINCC GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A82-MB 3A1632.D 1 06/22/23 AK n/a n/a V3A82
The QC reported here applies to the following samples:Method: SM 6200B
FC7092-1, FC7092-3, FC7092-4, FC7092-6, FC7092-8, FC7092-10
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 105%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
66 of 91
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Method Blank Summary Page 1 of 3
Job Number:FC7092
Account:GRINCC GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A84-MB 3A1685.D 1 06/27/23 AK n/a n/a V3A84
The QC reported here applies to the following samples:Method: SM 6200B
FC7092-2, FC7092-3, FC7092-5, FC7092-7, FC7092-9, FC7092-11, FC7092-12
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
67 of 91
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Method Blank Summary Page 2 of 3
Job Number:FC7092
Account:GRINCC GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A84-MB 3A1685.D 1 06/27/23 AK n/a n/a V3A84
The QC reported here applies to the following samples:Method: SM 6200B
FC7092-2, FC7092-3, FC7092-5, FC7092-7, FC7092-9, FC7092-11, FC7092-12
CAS No.Compound Result RL MDL Units Q
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
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Method Blank Summary Page 3 of 3
Job Number:FC7092
Account:GRINCC GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A84-MB 3A1685.D 1 06/27/23 AK n/a n/a V3A84
The QC reported here applies to the following samples:Method: SM 6200B
FC7092-2, FC7092-3, FC7092-5, FC7092-7, FC7092-9, FC7092-11, FC7092-12
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
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Blank Spike Summary Page 1 of 3
Job Number:FC7092
Account:GRINCC GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A82-BS 3A1630.D 1 06/22/23 AK n/a n/a V3A82
The QC reported here applies to the following samples:Method: SM 6200B
FC7092-1, FC7092-3, FC7092-4, FC7092-6, FC7092-8, FC7092-10
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.1 101 70-130
108-86-1 Bromobenzene 10 10.6 106 70-130
74-97-5 Bromochloromethane 10 9.8 98 70-130
75-27-4 Bromodichloromethane 10 8.7 87 70-130
75-25-2 Bromoform 10 8.2 82 70-130
104-51-8 n-Butylbenzene 10 9.7 97 70-130
135-98-8 sec-Butylbenzene 10 9.1 91 70-130
98-06-6 tert-Butylbenzene 10 9.4 94 70-130
56-23-5 Carbon Tetrachloride 10 9.1 91 70-130
108-90-7 Chlorobenzene 10 9.8 98 70-130
75-00-3 Chloroethane 10 9.5 95 60-140
67-66-3 Chloroform 10 10.1 101 70-130
95-49-8 o-Chlorotoluene 10 9.5 95 70-130
106-43-4 p-Chlorotoluene 10 9.5 95 70-130
124-48-1 Dibromochloromethane 10 9.5 95 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.6 96 70-130
106-93-4 1,2-Dibromoethane 10 9.1 91 70-130
75-71-8 Dichlorodifluoromethane 10 9.9 99 60-140
95-50-1 1,2-Dichlorobenzene 10 10.1 101 70-130
541-73-1 1,3-Dichlorobenzene 10 9.9 99 70-130
106-46-7 1,4-Dichlorobenzene 10 9.9 99 70-130
75-34-3 1,1-Dichloroethane 10 9.6 96 70-130
107-06-2 1,2-Dichloroethane 10 10.0 100 70-130
75-35-4 1,1-Dichloroethylene 10 9.8 98 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.0 100 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.1 101 70-130
78-87-5 1,2-Dichloropropane 10 10.4 104 70-130
142-28-9 1,3-Dichloropropane 10 11.2 112 70-130
594-20-7 2,2-Dichloropropane 10 10.9 109 70-130
563-58-6 1,1-Dichloropropene 10 9.5 95 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.2 92 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.2 92 70-130
108-20-3 Di-Isopropyl Ether 10 9.0 90 70-130
64-17-5 Ethyl Alcohol 500 681 136*70-130
100-41-4 Ethylbenzene 10 9.9 99 70-130
637-92-3 Ethyl Tert Butyl Ether 10 9.2 92 70-130
* = Outside of Control Limits.
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Blank Spike Summary Page 2 of 3
Job Number:FC7092
Account:GRINCC GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A82-BS 3A1630.D 1 06/22/23 AK n/a n/a V3A82
The QC reported here applies to the following samples:Method: SM 6200B
FC7092-1, FC7092-3, FC7092-4, FC7092-6, FC7092-8, FC7092-10
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
87-68-3 Hexachlorobutadiene 10 10.3 103 70-130
98-82-8 Isopropylbenzene 10 9.3 93 70-130
99-87-6 p-Isopropyltoluene 10 9.2 92 70-130
74-83-9 Methyl Bromide 10 10.1 101 60-140
74-87-3 Methyl Chloride 10 10.4 104 60-140
74-95-3 Methylene Bromide 10 10.0 100 70-130
75-09-2 Methylene Chloride 10 10.4 104 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.4 104 70-130
91-20-3 Naphthalene 10 9.2 92 70-130
103-65-1 n-Propylbenzene 10 9.3 93 70-130
100-42-5 Styrene 10 8.9 89 70-130
75-85-4 Tert-Amyl Alcohol 100 82.4 82 70-130
994-05-8 Tert-Amyl Methyl Ether 10 8.7 87 70-130
75-65-0 Tert-Butyl Alcohol 100 91.7 92 70-130
762-75-4 Tert-Butyl Formate 50 55.6 111 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.0 90 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.2 102 70-130
127-18-4 Tetrachloroethylene 10 10.6 106 70-130
108-88-3 Toluene 10 10.5 105 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.3 93 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.1 91 70-130
71-55-6 1,1,1-Trichloroethane 10 10 100 70-130
79-00-5 1,1,2-Trichloroethane 10 10.7 107 70-130
79-01-6 Trichloroethylene 10 9.8 98 70-130
75-69-4 Trichlorofluoromethane 10 8.7 87 60-140
96-18-4 1,2,3-Trichloropropane 10 10.7 107 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.6 96 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.6 96 70-130
75-01-4 Vinyl Chloride 10 10.7 107 60-140
m,p-Xylene 20 18.8 94 70-130
95-47-6 o-Xylene 10 8.7 87 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 97%70-130%
* = Outside of Control Limits.
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Job Number:FC7092
Account:GRINCC GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A82-BS 3A1630.D 1 06/22/23 AK n/a n/a V3A82
The QC reported here applies to the following samples:Method: SM 6200B
FC7092-1, FC7092-3, FC7092-4, FC7092-6, FC7092-8, FC7092-10
CAS No.Surrogate Recoveries BSP Limits
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 105%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
* = Outside of Control Limits.
72 of 91
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Blank Spike Summary Page 1 of 3
Job Number:FC7092
Account:GRINCC GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A84-BS 3A1683.D 1 06/27/23 AK n/a n/a V3A84
The QC reported here applies to the following samples:Method: SM 6200B
FC7092-2, FC7092-3, FC7092-5, FC7092-7, FC7092-9, FC7092-11, FC7092-12
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 11.5 115 70-130
108-86-1 Bromobenzene 10 11.8 118 70-130
74-97-5 Bromochloromethane 10 11.4 114 70-130
75-27-4 Bromodichloromethane 10 10.4 104 70-130
75-25-2 Bromoform 10 10.4 104 70-130
104-51-8 n-Butylbenzene 10 10.6 106 70-130
135-98-8 sec-Butylbenzene 10 10 100 70-130
98-06-6 tert-Butylbenzene 10 10.3 103 70-130
56-23-5 Carbon Tetrachloride 10 10.6 106 70-130
108-90-7 Chlorobenzene 10 11.4 114 70-130
75-00-3 Chloroethane 10 10.3 103 60-140
67-66-3 Chloroform 10 11.7 117 70-130
95-49-8 o-Chlorotoluene 10 10.6 106 70-130
106-43-4 p-Chlorotoluene 10 10.6 106 70-130
124-48-1 Dibromochloromethane 10 11.1 111 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 11.0 110 70-130
106-93-4 1,2-Dibromoethane 10 10.5 105 70-130
75-71-8 Dichlorodifluoromethane 10 11.9 119 60-140
95-50-1 1,2-Dichlorobenzene 10 11.4 114 70-130
541-73-1 1,3-Dichlorobenzene 10 11.2 112 70-130
106-46-7 1,4-Dichlorobenzene 10 11.1 111 70-130
75-34-3 1,1-Dichloroethane 10 11.3 113 70-130
107-06-2 1,2-Dichloroethane 10 11.6 116 70-130
75-35-4 1,1-Dichloroethylene 10 11.1 111 70-130
156-59-2 cis-1,2-Dichloroethylene 10 11.2 112 70-130
156-60-5 trans-1,2-Dichloroethylene 10 11.5 115 70-130
78-87-5 1,2-Dichloropropane 10 11.9 119 70-130
142-28-9 1,3-Dichloropropane 10 12.6 126 70-130
594-20-7 2,2-Dichloropropane 10 12.1 121 70-130
563-58-6 1,1-Dichloropropene 10 10.5 105 70-130
10061-01-5 cis-1,3-Dichloropropene 10 10.9 109 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.3 103 70-130
108-20-3 Di-Isopropyl Ether 10 10.4 104 70-130
64-17-5 Ethyl Alcohol 500 721 144*70-130
100-41-4 Ethylbenzene 10 11.4 114 70-130
637-92-3 Ethyl Tert Butyl Ether 10 10.5 105 70-130
* = Outside of Control Limits.
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Blank Spike Summary Page 2 of 3
Job Number:FC7092
Account:GRINCC GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A84-BS 3A1683.D 1 06/27/23 AK n/a n/a V3A84
The QC reported here applies to the following samples:Method: SM 6200B
FC7092-2, FC7092-3, FC7092-5, FC7092-7, FC7092-9, FC7092-11, FC7092-12
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
87-68-3 Hexachlorobutadiene 10 11.7 117 70-130
98-82-8 Isopropylbenzene 10 10.5 105 70-130
99-87-6 p-Isopropyltoluene 10 10.2 102 70-130
74-83-9 Methyl Bromide 10 10.4 104 60-140
74-87-3 Methyl Chloride 10 11.4 114 60-140
74-95-3 Methylene Bromide 10 11.9 119 70-130
75-09-2 Methylene Chloride 10 12.0 120 70-130
1634-04-4 Methyl Tert Butyl Ether 10 12.2 122 70-130
91-20-3 Naphthalene 10 10.4 104 70-130
103-65-1 n-Propylbenzene 10 10.3 103 70-130
100-42-5 Styrene 10 10.5 105 70-130
75-85-4 Tert-Amyl Alcohol 100 96.1 96 70-130
994-05-8 Tert-Amyl Methyl Ether 10 10.0 100 70-130
75-65-0 Tert-Butyl Alcohol 100 105 105 70-130
762-75-4 Tert-Butyl Formate 50 52.5 105 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.7 107 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 11.7 117 70-130
127-18-4 Tetrachloroethylene 10 11.5 115 70-130
108-88-3 Toluene 10 11.8 118 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.6 106 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.3 103 70-130
71-55-6 1,1,1-Trichloroethane 10 11.5 115 70-130
79-00-5 1,1,2-Trichloroethane 10 12.1 121 70-130
79-01-6 Trichloroethylene 10 11.3 113 70-130
75-69-4 Trichlorofluoromethane 10 9.3 93 60-140
96-18-4 1,2,3-Trichloropropane 10 12.3 123 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.9 109 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.8 108 70-130
75-01-4 Vinyl Chloride 10 11.1 111 60-140
m,p-Xylene 20 21.6 108 70-130
95-47-6 o-Xylene 10 10.3 103 70-130
1330-20-7 Xylene (total)30 31.8 106 70-130
* = Outside of Control Limits.
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Job Number:FC7092
Account:GRINCC GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3A84-BS 3A1683.D 1 06/27/23 AK n/a n/a V3A84
The QC reported here applies to the following samples:Method: SM 6200B
FC7092-2, FC7092-3, FC7092-5, FC7092-7, FC7092-9, FC7092-11, FC7092-12
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
* = Outside of Control Limits.
75 of 91
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2
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2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FC7092
Account:GRINCC GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC6943-5MS 3A1653.D 1 06/22/23 AK n/a n/a V3A82
FC6943-5MSD 3A1654.D 1 06/22/23 AK n/a n/a V3A82
FC6943-5 3A1633.D 1 06/22/23 AK n/a n/a V3A82
The QC reported here applies to the following samples:Method: SM 6200B
FC7092-1, FC7092-3, FC7092-4, FC7092-6, FC7092-8, FC7092-10
FC6943-5 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 0.51 0.5 0.95 88 0.5 0.95 88 0 70-130/20
108-86-1 Bromobenzene ND 0.5 0.44 88 0.5 0.48 96 9 70-130/20
74-97-5 Bromochloromethane ND 0.5 0.42 84 0.5 0.45 90 7 70-130/20
75-27-4 Bromodichloromethane 0.052 0.5 0.44 78 0.5 0.47 84 7 70-130/20
75-25-2 Bromoform 0.018 J 0.5 0.35 66*0.5 0.40 76 13 70-130/20
104-51-8 n-Butylbenzene 0.010 J 0.5 0.42 82 0.5 0.46 90 9 70-130/20
135-98-8 sec-Butylbenzene 0.0086 J 0.5 0.40 78 0.5 0.43 84 7 70-130/20
98-06-6 tert-Butylbenzene ND 0.5 0.41 42*0.5 0.45 50*9 70-130/20
56-23-5 Carbon Tetrachloride ND 0.5 0.43 86 0.5 0.47 94 9 70-130/20
108-90-7 Chlorobenzene ND 0.5 0.42 84 0.5 0.46 92 9 70-130/20
75-00-3 Chloroethane ND 0.5 0.53 106 0.5 0.52 104 2 60-140/20
67-66-3 Chloroform 0.43 0.5 0.91 96 0.5 0.90 94 1 70-130/20
95-49-8 o-Chlorotoluene ND 0.5 0.44 82 0.5 0.48 90 9 70-130/20
106-43-4 p-Chlorotoluene ND 0.5 0.40 73 0.5 0.44 81 10 70-130/20
124-48-1 Dibromochloromethane 0.022 J 0.5 0.40 76 0.5 0.44 84 10 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 0.5 0.41 82 0.5 0.43 86 5 70-130/20
106-93-4 1,2-Dibromoethane ND 0.5 0.36 72 0.5 0.41 82 13 70-130/20
75-71-8 Dichlorodifluoromethane ND 0.5 0.54 108 0.5 0.53 106 2 60-140/20
95-50-1 1,2-Dichlorobenzene ND 0.5 0.42 84 0.5 0.43 86 2 70-130/20
541-73-1 1,3-Dichlorobenzene ND 0.5 0.41 82 0.5 0.45 90 9 70-130/20
106-46-7 1,4-Dichlorobenzene ND 0.5 0.41 82 0.5 0.46 92 11 70-130/20
75-34-3 1,1-Dichloroethane ND 0.5 0.44 88 0.5 0.47 94 7 70-130/20
107-06-2 1,2-Dichloroethane ND 0.5 0.45 90 0.5 0.48 96 6 70-130/20
75-35-4 1,1-Dichloroethylene ND 0.5 0.46 92 0.5 0.50 100 8 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 0.5 0.41 82 0.5 0.46 92 11 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 0.5 0.46 92 0.5 0.50 100 8 70-130/20
78-87-5 1,2-Dichloropropane ND 0.5 0.45 90 0.5 0.50 100 11 70-130/20
142-28-9 1,3-Dichloropropane ND 0.5 0.46 92 0.5 0.51 102 10 70-130/20
594-20-7 2,2-Dichloropropane ND 0.5 0.44 88 0.5 0.46 92 4 70-130/20
563-58-6 1,1-Dichloropropene ND 0.5 0.42 84 0.5 0.46 92 9 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 0.5 0.38 76 0.5 0.42 84 10 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 0.5 0.36 72 0.5 0.39 78 8 70-130/20
108-20-3 Di-Isopropyl Ether 0.0095 J 0.5 0.40 78 0.5 0.45 88 12 70-130/20
64-17-5 Ethyl Alcohol ND 25 34.4 138*25 32.8 131*5 70-130/20
100-41-4 Ethylbenzene 0.66 0.5 1.1 88 0.5 1.1 88 0 70-130/20
637-92-3 Ethyl Tert Butyl Ether ND 0.5 0.39 78 0.5 0.43 86 10 70-130/20
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FC7092
Account:GRINCC GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC6943-5MS 3A1653.D 1 06/22/23 AK n/a n/a V3A82
FC6943-5MSD 3A1654.D 1 06/22/23 AK n/a n/a V3A82
FC6943-5 3A1633.D 1 06/22/23 AK n/a n/a V3A82
The QC reported here applies to the following samples:Method: SM 6200B
FC7092-1, FC7092-3, FC7092-4, FC7092-6, FC7092-8, FC7092-10
FC6943-5 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
87-68-3 Hexachlorobutadiene ND 0.5 0.45 90 0.5 0.50 100 11 70-130/20
98-82-8 Isopropylbenzene 0.048 0.5 0.45 80 0.5 0.50 90 11 70-130/20
99-87-6 p-Isopropyltoluene ND 0.5 0.39 78 0.5 0.43 86 10 70-130/20
74-83-9 Methyl Bromide ND 0.5 0.31 62 0.5 0.38 76 20 60-140/20
74-87-3 Methyl Chloride ND 0.5 0.52 104 0.5 0.53 106 2 60-140/20
74-95-3 Methylene Bromide ND 0.5 0.43 86 0.5 0.47 94 9 70-130/20
75-09-2 Methylene Chloride 0.065 J 0.5 0.50 87 0.5 0.53 93 6 70-130/20
1634-04-4 Methyl Tert Butyl Ether 0.93 0.5 1.5 114 0.5 1.4 94 7 70-130/20
91-20-3 Naphthalene 0.16 0.5 0.59 86 0.5 0.63 94 7 70-130/20
103-65-1 n-Propylbenzene 0.12 0.5 0.53 82 0.5 0.57 90 7 70-130/20
100-42-5 Styrene ND 0.5 0.38 76 0.5 0.43 86 12 70-130/20
75-85-4 Tert-Amyl Alcohol 0.50 5 3.9 68*5 4.6 82 16 70-130/20
994-05-8 Tert-Amyl Methyl Ether 0.15 0.5 0.55 80 0.5 0.60 90 9 70-130/20
75-65-0 Tert-Butyl Alcohol ND 5 3.9 78 5 4.4 88 12 70-130/20
762-75-4 Tert-Butyl Formate ND 2.5 3.1 124 2.5 2.6 104 18 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 0.5 0.38 76 0.5 0.42 84 10 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 0.5 0.42 84 0.5 0.45 90 7 70-130/20
127-18-4 Tetrachloroethylene ND 0.5 0.44 88 0.5 0.48 96 9 70-130/20
108-88-3 Toluene 2.2 0.5 2.4 40* a 0.5 2.3 20* a 4 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 0.5 0.40 80 0.5 0.43 86 7 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 0.5 0.39 78 0.5 0.43 86 10 70-130/20
71-55-6 1,1,1-Trichloroethane ND 0.5 0.46 92 0.5 0.49 98 6 70-130/20
79-00-5 1,1,2-Trichloroethane ND 0.5 0.42 84 0.5 0.45 90 7 70-130/20
79-01-6 Trichloroethylene ND 0.5 0.43 86 0.5 0.47 94 9 70-130/20
75-69-4 Trichlorofluoromethane ND 0.5 0.50 100 0.5 0.48 96 4 60-140/20
96-18-4 1,2,3-Trichloropropane ND 0.5 0.44 88 0.5 0.49 98 11 70-130/20
95-63-6 1,2,4-Trimethylbenzene 1.1 0.5 1.5 80 0.5 1.5 80 0 70-130/20
108-67-8 1,3,5-Trimethylbenzene 0.26 0.5 0.69 86 0.5 0.72 92 4 70-130/20
75-01-4 Vinyl Chloride ND 0.5 0.52 104 0.5 0.53 106 2 60-140/20
m,p-Xylene 2.7 1 3.4 70 1 3.3 60* a 3 70-130/20
95-47-6 o-Xylene 1.3 0.5 1.7 80 0.5 1.6 60* a 6 70-130/20
CAS No.Surrogate Recoveries MS MSD FC6943-5 Limits
1868-53-7 Dibromofluoromethane 100%99%96%70-130%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FC7092
Account:GRINCC GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC6943-5MS 3A1653.D 1 06/22/23 AK n/a n/a V3A82
FC6943-5MSD 3A1654.D 1 06/22/23 AK n/a n/a V3A82
FC6943-5 3A1633.D 1 06/22/23 AK n/a n/a V3A82
The QC reported here applies to the following samples:Method: SM 6200B
FC7092-1, FC7092-3, FC7092-4, FC7092-6, FC7092-8, FC7092-10
CAS No.Surrogate Recoveries MS MSD FC6943-5 Limits
17060-07-0 1,2-Dichloroethane-D4 110%106%103%70-130%
2037-26-5 Toluene-D8 101%101%104%70-130%
460-00-4 4-Bromofluorobenzene 104%102%101%70-130%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FC7092
Account:GRINCC GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC7092-3MS 3A1706.D 25 06/27/23 AK n/a n/a V3A84
FC7092-3MSD 3A1707.D 25 06/27/23 AK n/a n/a V3A84
FC7092-3 3A1687.D 25 06/27/23 AK n/a n/a V3A84
The QC reported here applies to the following samples:Method: SM 6200B
FC7092-2, FC7092-3, FC7092-5, FC7092-7, FC7092-9, FC7092-11, FC7092-12
FC7092-3 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 229 250 485 102 250 480 100 1 70-130/20
108-86-1 Bromobenzene ND 250 256 102 250 277 111 8 70-130/20
74-97-5 Bromochloromethane ND 250 292 117 250 254 102 14 70-130/20
75-27-4 Bromodichloromethane ND 250 233 93 250 218 87 7 70-130/20
75-25-2 Bromoform ND 250 211 84 250 198 79 6 70-130/20
104-51-8 n-Butylbenzene ND 250 252 101 250 265 106 5 70-130/20
135-98-8 sec-Butylbenzene ND 250 235 94 250 247 99 5 70-130/20
98-06-6 tert-Butylbenzene ND 250 250 100 250 257 103 3 70-130/20
56-23-5 Carbon Tetrachloride ND 250 278 111 250 253 101 9 70-130/20
108-90-7 Chlorobenzene ND 250 247 99 250 239 96 3 70-130/20
75-00-3 Chloroethane ND 250 314 126 250 273 109 14 60-140/20
67-66-3 Chloroform ND 250 307 123 250 266 106 14 70-130/20
95-49-8 o-Chlorotoluene ND 250 250 98 250 246 96 2 70-130/20
106-43-4 p-Chlorotoluene ND 250 237 95 250 242 97 2 70-130/20
124-48-1 Dibromochloromethane ND 250 234 94 250 227 91 3 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 250 251 100 250 263 105 5 70-130/20
106-93-4 1,2-Dibromoethane ND 250 227 91 250 221 88 3 70-130/20
75-71-8 Dichlorodifluoromethane ND 250 384 154*250 349 140 10 60-140/20
95-50-1 1,2-Dichlorobenzene ND 250 252 101 250 266 106 5 70-130/20
541-73-1 1,3-Dichlorobenzene ND 250 248 99 250 243 97 2 70-130/20
106-46-7 1,4-Dichlorobenzene ND 250 243 97 250 241 96 1 70-130/20
75-34-3 1,1-Dichloroethane ND 250 296 118 250 265 106 11 70-130/20
107-06-2 1,2-Dichloroethane ND 250 280 112 250 260 104 7 70-130/20
75-35-4 1,1-Dichloroethylene ND 250 308 123 250 276 110 11 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 250 293 117 250 260 104 12 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 250 307 123 250 276 110 11 70-130/20
78-87-5 1,2-Dichloropropane ND 250 269 108 250 251 100 7 70-130/20
142-28-9 1,3-Dichloropropane ND 250 274 110 250 262 105 4 70-130/20
594-20-7 2,2-Dichloropropane ND 250 303 121 250 262 105 15 70-130/20
563-58-6 1,1-Dichloropropene ND 250 260 104 250 252 101 3 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 250 239 96 250 235 94 2 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 250 222 89 250 212 85 5 70-130/20
108-20-3 Di-Isopropyl Ether 10.3 J 250 288 111 250 260 100 10 70-130/20
64-17-5 Ethyl Alcohol ND 12500 20600 165*12500 20100 161*2 70-130/20
100-41-4 Ethylbenzene 243 250 507 106 250 470 91 8 70-130/20
637-92-3 Ethyl Tert Butyl Ether ND 250 271 108 250 244 98 10 70-130/20
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FC7092
Account:GRINCC GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC7092-3MS 3A1706.D 25 06/27/23 AK n/a n/a V3A84
FC7092-3MSD 3A1707.D 25 06/27/23 AK n/a n/a V3A84
FC7092-3 3A1687.D 25 06/27/23 AK n/a n/a V3A84
The QC reported here applies to the following samples:Method: SM 6200B
FC7092-2, FC7092-3, FC7092-5, FC7092-7, FC7092-9, FC7092-11, FC7092-12
FC7092-3 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
87-68-3 Hexachlorobutadiene ND 250 276 110 250 305 122 10 70-130/20
98-82-8 Isopropylbenzene 4.7 J 250 251 99 250 241 95 4 70-130/20
99-87-6 p-Isopropyltoluene ND 250 238 95 250 254 102 7 70-130/20
74-83-9 Methyl Bromide ND 250 161 64 250 177 71 9 60-140/20
74-87-3 Methyl Chloride ND 250 329 132 250 293 117 12 60-140/20
74-95-3 Methylene Bromide ND 250 267 107 250 255 102 5 70-130/20
75-09-2 Methylene Chloride ND 250 304 122 250 273 109 11 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 250 305 122 250 276 110 10 70-130/20
91-20-3 Naphthalene 73.0 250 339 106 250 371 119 9 70-130/20
103-65-1 n-Propylbenzene 14.3 250 255 96 250 270 102 6 70-130/20
100-42-5 Styrene 3.6 J 250 241 95 250 223 88 8 70-130/20
75-85-4 Tert-Amyl Alcohol 247 J 2500 2590 94 2500 2710 99 5 70-130/20
994-05-8 Tert-Amyl Methyl Ether ND 250 228 91 250 220 88 4 70-130/20
75-65-0 Tert-Butyl Alcohol ND 2500 2650 106 2500 2570 103 3 70-130/20
762-75-4 Tert-Butyl Formate ND 1250 1230 98 1250 1190 95 3 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 250 234 94 250 217 87 8 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 250 254 102 250 273 109 7 70-130/20
127-18-4 Tetrachloroethylene ND 250 258 103 250 258 103 0 70-130/20
108-88-3 Toluene 1090 250 1410 128 250 1370 112 3 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 250 246 98 250 267 107 8 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 250 240 96 250 261 104 8 70-130/20
71-55-6 1,1,1-Trichloroethane ND 250 302 121 250 270 108 11 70-130/20
79-00-5 1,1,2-Trichloroethane ND 250 254 102 250 250 100 2 70-130/20
79-01-6 Trichloroethylene ND 250 264 106 250 260 104 2 70-130/20
75-69-4 Trichlorofluoromethane ND 250 289 116 250 261 104 10 60-140/20
96-18-4 1,2,3-Trichloropropane ND 250 270 108 250 267 107 1 70-130/20
95-63-6 1,2,4-Trimethylbenzene 184 250 457 109 250 474 116 4 70-130/20
108-67-8 1,3,5-Trimethylbenzene 43.2 250 300 103 250 297 102 1 70-130/20
75-01-4 Vinyl Chloride ND 250 329 132 250 302 121 9 60-140/20
m,p-Xylene 935 500 1400 93 500 1320 77 6 70-130/20
95-47-6 o-Xylene 466 250 719 101 250 673 83 7 70-130/20
1330-20-7 Xylene (total)1400 750 2120 96 750 1990 79 6 70-130/20
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FC7092
Account:GRINCC GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC7092-3MS 3A1706.D 25 06/27/23 AK n/a n/a V3A84
FC7092-3MSD 3A1707.D 25 06/27/23 AK n/a n/a V3A84
FC7092-3 3A1687.D 25 06/27/23 AK n/a n/a V3A84
The QC reported here applies to the following samples:Method: SM 6200B
FC7092-2, FC7092-3, FC7092-5, FC7092-7, FC7092-9, FC7092-11, FC7092-12
CAS No.Surrogate Recoveries MS MSD FC7092-3 Limits
1868-53-7 Dibromofluoromethane 113%102%97%70-130%
17060-07-0 1,2-Dichloroethane-D4 113%108%105%70-130%
2037-26-5 Toluene-D8 101%102%90%70-130%
460-00-4 4-Bromofluorobenzene 103%110%99%70-130%
* = Outside of Control Limits.
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SGS LabLink@15:16 03-Jul-2023
GC Volatiles
QC Data Summaries
Includes the following where applicable:
 Method Blank Summaries
 Blank Spike Summaries
 Matrix Spike and Duplicate Summaries
Orlando, FL
Section 6
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Method Blank Summary Page 1 of 1
Job Number:FC7092
Account:GRINCC GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLL2891-MB LL83226.D 1 06/26/23 SS n/a n/a GLL2891
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FC7092-2, FC7092-3, FC7092-4, FC7092-5, FC7092-6, FC7092-7, FC7092-8, FC7092-9
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane ND 0.50 0.16 ug/l
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Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FC7092
Account:GRINCC GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLL2891-BS LL83223.D 1 06/26/23 SS n/a n/a GLL2891
GLL2891-BSD LL83224.D 1 06/26/23 SS n/a n/a GLL2891
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FC7092-2, FC7092-3, FC7092-4, FC7092-5, FC7092-6, FC7092-7, FC7092-8, FC7092-9
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
74-82-8 Methane 108 123 114 125 116 2 62-139/30
* = Outside of Control Limits.
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Matrix Spike Summary Page 1 of 1
Job Number:FC7092
Account:GRINCC GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC7133-1MS LL83239.D 1 06/26/23 SS n/a n/a GLL2891
FC7133-1 LL83237.D 1 06/26/23 SS n/a n/a GLL2891
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FC7092-2, FC7092-3, FC7092-4, FC7092-5, FC7092-6, FC7092-7, FC7092-8, FC7092-9
FC7133-1 Spike MS MS
CAS No.Compound ug/l Q ug/l ug/l %Limits
74-82-8 Methane 0.50 U 108 118 109 62-139
* = Outside of Control Limits.
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Duplicate Summary Page 1 of 1
Job Number:FC7092
Account:GRINCC GRI (Geological Resources Inc.)
Project:Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC7133-1DUP LL83238.D 1 06/26/23 SS n/a n/a GLL2891
FC7133-1 LL83237.D 1 06/26/23 SS n/a n/a GLL2891
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FC7092-2, FC7092-3, FC7092-4, FC7092-5, FC7092-6, FC7092-7, FC7092-8, FC7092-9
FC7133-1 DUP
CAS No.Compound ug/l Q ug/l Q RPD Limits
74-82-8 Methane 0.50 U ND nc 30
* = Outside of Control Limits.
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General Chemistry
QC Data Summaries
Includes the following where applicable:
 Method Blank and Blank Spike Summaries
 Duplicate Summaries
 Matrix Spike Summaries
Orlando, FL
Section 7
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METHOD BLANK AND SPIKE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FC7092
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
MB Spike BSP BSP QC
Analyte Batch ID RL Result Units Amount Result %Recov Limits
Chloride GP38886/GN94534 2.0 0.0 mg/l 50 49.5 99.0 90-110%
Iron, Ferrous GN94630 0.10 0.0 mg/l 0.500 0.50 99.7 82-115%
Nitrogen, Nitrate GP38886/GN94534 0.10 0.0 mg/l 2.5 2.72 108.8 90-110%
Sulfate GP38886/GN94534 2.0 0.0 mg/l 50 51.1 102.2 90-110%
Associated Samples:
Batch GN94630: FC7092-2, FC7092-3, FC7092-4, FC7092-5, FC7092-6, FC7092-7, FC7092-8, FC7092-9
Batch GP38886: FC7092-2, FC7092-3, FC7092-4, FC7092-5, FC7092-6, FC7092-7, FC7092-8, FC7092-9
(*) Outside of QC limits
__________________________________________________________________________________________________________________________
Page 1
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DUPLICATE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FC7092
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
QC Original DUP QC
Analyte Batch ID Sample Units Result Result RPD Limits
Iron, Ferrous GN94630 FC7092-2 mg/l 0.0 0.0 0.0 0-31%
Associated Samples:
Batch GN94630: FC7092-2, FC7092-3, FC7092-4, FC7092-5, FC7092-6, FC7092-7, FC7092-8, FC7092-9
(*) Outside of QC limits
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MATRIX SPIKE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FC7092
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
QC Original Spike MS QC
Analyte Batch ID Sample Units Result Amount Result %Rec Limits
Chloride GP38886/GN94534 FC7092-8 mg/l 3.3 50 55.5 104.4 90-110%
Nitrogen, Nitrate GP38886/GN94534 FC7092-8 mg/l 0.50 2.5 3.3 112.0N(a) 90-110%
Sulfate GP38886/GN94534 FC7092-8 mg/l 4.1 50 58.1 108.0 90-110%
Associated Samples:
Batch GP38886: FC7092-2, FC7092-3, FC7092-4, FC7092-5, FC7092-6, FC7092-7, FC7092-8, FC7092-9
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(a) Spike recovery indicates possible matrix interference.
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MATRIX SPIKE DUPLICATE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FC7092
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Economy Foods 2; 5310 Cedar Creek Rd, Fayetteville, NC
QC Original Spike MSD QC
Analyte Batch ID Sample Units Result Amount Result RPD Limit
Chloride GP38886/GN94534 FC7092-8 mg/l 3.3 50 53.9 2.9 15%
Nitrogen, Nitrate GP38886/GN94534 FC7092-8 mg/l 0.50 2.5 3.2 3.1 15%
Sulfate GP38886/GN94534 FC7092-8 mg/l 4.1 50 56.3 3.1 15%
Associated Samples:
Batch GP38886: FC7092-2, FC7092-3, FC7092-4, FC7092-5, FC7092-6, FC7092-7, FC7092-8, FC7092-9
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
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