FA-1722_29035_CA_MRP_20230511

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
May 11, 2023

Mr. Ken Currie
NCDEQ-UST Section
Fayetteville Regional Office
Systel Building
225 Green Street, Suite 714
Fayetteville, NC 28301-5043

Re: Free Product Recovery and
Ground Water Monitoring Report
January - March 2023
Stone’s Fast Save
119 East Main Street
Rowland, Robeson County
North Carolina
Facility ID Number: 0-00-0000019036
Incident Number: 29035
GRI Project Number: 2796

Dear Mr. Currie,

Please find attached the referenced report for the abovementioned site.
If you have any questions, please contact Laura Minor at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Mr. Richard W. Stone, file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Free Product Recovery and
Ground Water Monitoring Report
January – March 2023
Stone’s Fast Save
119 East Main Street
Rowland, Robeson County
North Carolina
Facility ID Number: 0-00-0000019036
Incident Number: 29035
GRI Project Number: 2796

Prepared for:

Mr. Richard Wayne Stone
407 East Church Street
Rowland, North Carolina 28383

May 11, 2023

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: May 11, 2023 Stone’s Fast Save
Project Manager: Laura Minor GRI Project No. 2796
i
SITE INFORMATION
1. Site Identification
 Stone’s Fast Save (Facility ID 0-00-0000019036)
 Incident Number 29035 – Intermediate Risk (I170D)
 Location of Source Area: 119 East Main Street
Rowland, NC 28314
Robeson County
34.536869 °N, 79.291500 °W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST/AST Owner
Richard Wayne Stone
407 East Church Street
Rowland, North Carolina 28383
Email: Unknown
910-422-3735

UST/AST Operator
Richard Wayne Stone
407 East Church Street
Rowland, North Carolina 28383
Email: Unknown
910-422-3735

Property Owner
Richard Wayne Stone
407 East Church Street
Rowland, North Carolina 28383
Email: Unknown
910-422-3735

Property Occupant
Richard Wayne Stone
407 East Church Street
Rowland, North Carolina 28383
Email: Unknown
910-422-3735

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
Waypoint Analytical
449 Springbrook Road
Charlotte, NC 28217
704-529-6364

3. Information about Release
 Release was discovered in October 2002
 An unknown amount of product was released from the leaking UST System
 One 10,000-gallon compartmentalized gasoline UST, one 15,000-gallon gasoline UST, and one
20,000-gallon compartmentalized UST containing kerosene and diesel, and associated pumps and
product piping are active at the site
 One 1,000-gallon kerosene and one 2,000-gallon diesel USTs were removed in December 1981.
One 4,000-gallon kerosene, one 4,000-gallon diesel, two 4,000-gallon gasoline and one 10,000-
gallon gasoline USTs were removed in October 2002

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: May 11, 2023 Stone’s Fast Save
Project Manager: Laura Minor GRI Project No. 2796
ii
EXECUTIVE SUMMARY
Stone’s Fast Save is located at 119 East Main Street in Rowland, Robeson County, North Carolina. Seven
USTs of various sizes and contents were removed in 1981 and 2002. Currently, one 15,000-gallon gasoline
UST, one 10,000-gallon compartmentalized gasoline UST, and one 20,000-gallon compartmentalized
kerosene and diesel UST are currently in use on site. The adjoining properties are a mixture of residential
and commercial/industrial properties. Nineteen Type II monitoring wells (MW-1 through MW-19) and
one Type III monitoring well (TW-1) were installed at the site during previous ground water assessment
and corrective action activities. According to the information determined during receptor survey
activities, four currently inactive water supply wells were identified within 1,000 feet of the site. Public
water is available to the site and all surrounding properties within a 1,500-foot radius of the site.

Free product has been documented at the site since at least 2003. Free product recovery has been
conducted intermittently since that time until the most current event in March 2023. Historical activities
include MMPEs, AFVRs, hand bailing, and utilization of absorbent socks. Depths to water and free product
thicknesses in MW-4 and MW-5 were gauged monthly from January to March 2023. Free product was
measured in MW-5 in January and February 2023. New absorbent socks were placed in MW-5 after each
gauging and hand bailing event. During the gauging period, free product thickness ranged from 0.01 to
0.02 feet. An estimated total of 0.09 gallons of liquid free product was hand bailed from MW-5 between
January and February 2023.

Site monitoring wells were gauged and/or sampled on March 28, 2023. During the sampling event, free
product was measured in monitoring well MW-13. Concentrations of benzene, toluene, ethylbenzene,
xylenes, MTBE, naphthalene, tert-Amyl alcohol (TAA), tert-Amyl methyl ether (TAME), tert-Butyl alcohol
(TBA), 2-Hexanone, isopropylbenzene, n-propylbenzene, 1,2,4-trimethylbenzene, and/or 1,3,5-
trimethylbenzene that exceeded the MACs were reported in the ground water samples collected from
MW-1 through MW-12, MW-14 and MW-17 through MW-19. The reported concentration of benzene
exceeded the GCL in the ground water sample collected from MW-5.

Contaminant mass calculations were completed for the March 2023 ground water sampling event. Since
2013, contaminant mass has decreased 14.8% at the site.

Based on this information, the risk classification for the site should remain intermediate risk. Based on
the persistence of free product and ground water contaminants exceeding the GCLs, GRI recommends a
feasibility study be conducted to evaluate potential site remediation options. In the interim, free product
recovery and semi-annual ground water monitoring (including natural attenuation parameters) should
continue at the site. The next sampling event is tentatively scheduled for December 2023.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: May 11, 2023 Stone’s Fast Save
Project Manager: Laura Minor GRI Project No. 2796

iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LEL: Lower Explosive Limit
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
PID: Photo Ionization Detector
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: May 11, 2023 Stone’s Fast Save
Project Manager: Laura Minor GRI Project No. 2796

TABLE OF CONTENTS
SITE INFORMATION ............................................................................................................................ i
EXECUTIVE SUMMARY ....................................................................................................................... ii
ACRONYMS ....................................................................................................................................... iii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................2
3.0 FREE PRODUCT REMOVAL ........................................................................................................5
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................6
5.0 CONCLUSIONS .........................................................................................................................6
6.0 LIMITATIONS ...........................................................................................................................7
7.0 STATEMENTS AND CERTIFICATION ...........................................................................................8

FIGURES
Figure 1: Site Location Map
Figure 2: Site Vicinity Map
Figure 3: Site Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map
Figure 6: Benzene Isoconcentration Map
Figure 7: Toluene Isoconcentration Map
Figure 8: Ethylbenzene Isoconcentration Map
Figure 9: Xylenes Isoconcentration Map
Figure 10: MTBE Isoconcentration Map
Figure 11: Naphthalene Isoconcentration Map
Figure 12: Cross Section A-A’
Figure 13: Cross Section B-B’
Figure 14: Area of Concern Map

TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Water Supply Well Information
Table 4: Adjacent Property Owner Information
Table 5: Well Construction and Gauging Information
Table 6: Summary of Ground Water Sample Analytical Results

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: May 11, 2023 Stone’s Fast Save
Project Manager: Laura Minor GRI Project No. 2796

Table 7: Free Product Recovery Results
Table 8: Free Product Recovery Event Information
Table 9: Free Product Recovery Cost Summary

APPENDICES
Appendix A: State Correspondence
Appendix B: Notice of Residual Petroleum
Appendix C: Laboratory Analytical Report
Appendix D: Contaminant Mass Calculations

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: May 11, 2023 Stone’s Fast Save
Project Manager: Laura Minor GRI Project No. 2796

1
1.0 SITE HISTORY AND CHARACTERIZATION
GRI presents the results of the January through March 2023 free product recovery activities and the March
2023 ground water sampling event at the Stone’s Fast Save site; located at 119 East Main Street in
Rowland, Robeson County, North Carolina. A topographic map showing the general site location and the
surrounding area is included as Figure 1. These activities were conducted in accordance with GRI Proposal
No. 22-754, which was submitted to the NCDEQ on January 17, 2023 and was approved as Task
Authorization No. 29035-21 on January 25, 2023. State correspondence is included as Appendix A.

The site is currently owned and operated by Ricky Stone as a petroleum retail facility. A site check was
conducted in 2009 following a release from a spill bucket at the north end of the 15,000-gallon UST.
Currently, one 15,000-gallon gasoline UST, one 10,000-gallon compartmentalized gasoline UST, and one
20,000-gallon compartmentalized kerosene and diesel UST are currently in use on site. UST
owner/operator information and UST system information are included as Table 1 and Table 2,
respectively. The Registered Tank Report is shown below:

The site and surrounding area is a mixture of residential and commercial/industrial properties. The site
contains one building and a fuel canopy and is primarily capped with concrete and asphalt. The overall

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: May 11, 2023 Stone’s Fast Save
Project Manager: Laura Minor GRI Project No. 2796

2
topography at the site is relatively flat. A total of eight water supply wells were identified within a 1,500-
foot distance from the source area. Four water supply wells (WSW-2, WSW-3, WSW-4, and WSW-7) are
located within 1,000-feet of the source area but are inactive. Water supply well information is
summarized in Table 3. No surface water bodies were identified within a 500-foot radius of the site.
Municipal water is available to the site and all of the properties within 1,000 feet of the source area. The
site is located within the designated Wellhead Protection Area for the Town of Rowland. Adjacent
property owner information is presented in Table 4. A Site Vicinity Map showing the adjacent properties
and previously identified water supply wells is included as Figure 2.

According to available information, one 4,000-gallon kerosene, one 4,000-gallon diesel, two 4,000-gallon
gasoline, one 10,000-gallon gasoline, one 2,000-gallon diesel and one 1,000-gallon kerosene USTs were
reportedly in use in the past but have since been removed. Nineteen (19) Type II monitoring wells (MW-
1 through MW-19) and one Type III monitoring well (TW-1) were installed at the site during previous
ground water assessment and corrective action activities. Free product has been documented at the site
since at least 2003. Free product recovery has been conducted intermittently since that time. A CAP has
not yet been established since the contaminant plume has not been fully defined.

Please note that a Notice of Residual Petroleum was filed for the site on May 2, 2023 at the Robeson
County Register of Deeds Office. A copy of the filed NRP is included as Appendix B.

Although GRI cannot verify the accuracy of information obtained from previous reports prepared by other
consultants, for the purposes of this report, it is assumed to be correct. Please refer to previous submittals
for further historical information regarding the site.
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
On March 28, 2023, nineteen Type II monitoring wells (MW-1 through MW-19) and one telescoping well
(TW-1) were gauged, purged and/or sampled in accordance with the NCDEQ Guidelines. Free product
was observed in monitoring well MW-13; therefore, it was not sampled. Depths to ground water in the
Type II monitoring wells ranged from 6.49 feet to 8.81 feet. Ground water elevations in the Type II
monitoring wells ranged from 139.29 feet to 141.11 feet. The site topography is relatively flat, but ground
water flow was generally to the west, with a topographic low in the area of MW-2. The average horizontal
gradient across the site was approximately 0.009 feet per foot. The vertical gradient calculated for paired
wells MW-12/TW-1 was approximately 0.026 feet per foot in the downward direction. Well construction
and gauging information is presented in Table 5. A Site Map showing the locations of the monitoring wells
and the structures on-site is included as Figure 3. A Water Table Surface Map based on the Type II
monitoring wells is included as Figure 4. A summary of the current ground water gauging data is shown
below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: May 11, 2023 Stone’s Fast Save
Project Manager: Laura Minor GRI Project No. 2796

3
Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
MW-1 9 – 19 19 148.80 8.81 --- 139.99
MW-2 5 - 20 20 148.05 8.31 --- 139.74
MW-3 5 - 20 20 148.55 7.55 --- 141.00
MW-4 5 - 20 20 148.46 7.81 --- 140.65
MW-5 5 - 20 20 148.04 7.44 --- 140.60
MW-6 7 – 17 16.51 148.22 7.59 --- 140.63
MW-7 7 – 17 17 149.00 7.98 --- 141.02
MW-8 7 – 17 17 148.53 7.46 --- 141.07
MW-9 7 – 17 17 148.41 7.70 --- 140.71
MW-10 7 – 17 17 148.12 7.37 --- 140.75
MW-11 7 – 17 17 147.98 7.49 --- 140.49
MW-12 5 – 15 15 148.06 7.29 --- 140.77
MW-13 5 – 15 15 148.49 7.65 0.03 140.87
MW-14 5 – 15 15 148.33 7.63 --- 140.70
MW-15 5 – 20 20 147.60 6.49 --- 141.11
MW-16 5 – 20 20 147.62 6.67 --- 140.95
MW-17 5 – 20 20 149.14 8.38 --- 140.76
MW-18 7 – 17 17 147.21 7.92 --- 139.29
MW-19 7 – 17 17 148.00 8.66 --- 139.34
TW-1 40 – 45 45 148.23 8.37 --- 139.86

Ground water samples collected from the monitoring wells were submitted for laboratory analyses using
EPA Method 6200B. Concentrations of benzene, toluene, ethylbenzene, xylenes, MTBE, naphthalene,
tert-Amyl alcohol (TAA), tert-Amyl methyl ether (TAME), tert-Butyl alcohol (TBA), 2-Hexanone,
isopropylbenzene, n-propylbenzene, 1,2,4-trimethylbenzene, and/or 1,3,5-trimethylbenzene that
exceeded the MACs were reported in the ground water samples collected from MW-1 through MW-12,
MW-14 and MW-17 through MW-19. The reported concentration of benzene exceeded the GCL in the
ground water sample collected from MW-5. A summary of the analytical results for ground water samples
collected on March 28, 2023 is presented in Table 6. A Ground Water Quality Map based on the March
2023 data is included as Figure 5. Isoconcentration maps for benzene, toluene, ethylbenzene, xylenes,
MTBE, and naphthalene are included as Figures 6 through 11, respectively. Cross-sections A-A’ and B-B’
are included as Figures 12 and 13, respectively. A complete report of laboratory analyses of the ground
water samples collected from the monitoring wells during the March 2023 sampling event is included as
Appendix C. A summary of the current ground water analytical data is shown below:

Contaminant
of Concern 
Be
n
z
e
n
e

To
l
u
e
n
e

Et
h
y
l
b
e
n
z
e
n
e

Xy
l
e
n
e
s

MT
B
E

Na
p
h
t
h
a
l
e
n
e

Well
ID
MACs (mg/l) 1 600 600 500 20 6
GCL (mg/l) 5,000 260,000 80,000 50,000 20,000 6,000
MW-1 3,960 109 3,330 236 J 1,110 1,190
MW-2 14.5 2.67 1,020 884 <0.140 476

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: May 11, 2023 Stone’s Fast Save
Project Manager: Laura Minor GRI Project No. 2796

4
Contaminant
of Concern 
Be
n
z
e
n
e

To
l
u
e
n
e

Et
h
y
l
b
e
n
z
e
n
e

Xy
l
e
n
e
s

MT
B
E

Na
p
h
t
h
a
l
e
n
e

Well
ID
MACs (mg/l) 1 600 600 500 20 6
GCL (mg/l) 5,000 260,000 80,000 50,000 20,000 6,000
MW-3 25.6 <0.220 18.8 5.77 28.6 38.4
MW-4 884 94.7 1,560 1,690 265 1,540
MW-5 8,260 11,400 2,270 9,010 3,240 854
MW-6 0.591 1.06 2.46 6.46 <0.140 8.19
MW-7 950 563 1,040 2,030 273 482
MW-8 581 409 1,830 4,130 <14.0 1,080
MW-9 1,190 3,530 877 4,440 20.9 482
MW-10 5.95 0.731 68.1 18.5 0.358 J 58.6
MW-11 <1.80 63.3 1,750 4,030 <1.40 424
MW-12 967 2,070 702 4,030 323 393
MW-13 FP FP FP FP FP FP
MW-14 593 1,680 1,410 4,840 76.5 862
MW-15 <0.180 <0.220 0.529 1.17 J <0.140 1.19
MW-16 <0.180 <0.220 0.726 1.47 J 0.216 J 2.62
MW-17 0.514 <0.220 30.0 4.02 <0.140 51.0
MW-18 446 544 1300 3,160 53.7 324
MW-19 255 2,580 978 3,590 <1.40 346
TW-1 <0.180 0.422 J 0.385 J 1.96 <0.140 2.74

Since the site is ranked intermediate, the baseline contaminant mass was only calculated for the area of
concern, which includes the former USTs and monitoring wells MW-1, MW-4, MW-5 and MW-13. These
wells currently or formerly contained free product or contaminant concentrations which exceed the GCLs.
The total BTEX, MTBE, and naphthalene concentrations from the January 2013 ground water sampling
event, as well as the maximum historical water column height observed in the area of concern, was used
to establish the baseline contaminant mass. The contaminant mass has decreased by approximately
15.2% compared to the December 2020 sampling event. Overall, contaminant mass at the site has
decreased 14.8% since January 2013. Please note that calculated values represent a conservative
estimate of contaminant mass because GCL values were used for wells containing free product.
Contaminant mass calculations are included as Appendix D. A map of the contaminant mass area of
concern is included as Figure 14. A chart depicting the overall trend in contaminant mass is shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: May 11, 2023 Stone’s Fast Save
Project Manager: Laura Minor GRI Project No. 2796

5

The site is located in the Coastal Plain Physiographic Province of North Carolina. The water table has a
seasonal high depth to water of approximately five to six feet below ground surface (bgs). The seasonal
low depth to water is approximately 12 to 15 feet bgs.

Please note that while free product removal events have continued, a CAP has not been established at
the site; therefore, a baseline contaminant mass for the entire site prior to CAP implementation has not
been established at the site. Please note that milestones would be established in the CAP.
3.0 FREE PRODUCT REMOVAL
Free product has historically been present in monitoring wells MW-1, MW-4, MW-5, and MW-12.
Currently, free product is present in MW-13. Depths to water and free product thicknesses in MW-4 and
MW-5 were gauged monthly from January to March 2023. Free product was measured in MW-5 in
January and February 2023. During the gauging period, free product ranged from 0.01 to 0.02 feet.

Subsequent to gauging the wells, free product was removed from MW-5 by hand bailing in January and
February 2023 and containerized in a drum, which was stored on-site. New absorbent socks were installed
in monitoring well MW-5 monthly. An estimated total of 0.09 gallons of liquid free product was removed

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: May 11, 2023 Stone’s Fast Save
Project Manager: Laura Minor GRI Project No. 2796

6
from MW-5 between January and February 2023. The drum used to store the recovered free product
remains on-site, as it has capacity to store free product and socks for future recovery events. A summary
of free product recovery data is included as Tables 7 through 9. Free product recovery should continue
at the site until free product is no longer present.
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
AFVR events have historically been conducted at the site and free product recovery using hand bailing and
absorbent socks is currently being used as the primary method of corrective action. Due to the site being
in the active assessment and free product recovery phase, no natural attenuation monitoring plan is
currently in place at the site.
5.0 CONCLUSIONS
 Depths to water and free product thicknesses in MW-4 and MW-5 were gauged monthly from
January to March 2023. Free product was measured in MW-5 in January and February 2023.
During the gauging period, free product ranged from 0.01 to 0.02 feet. An estimated total of 0.09
gallons of liquid free product was removed from MW-5 by hand bailing between January and
February 2023.
 On March 28, 2023, nineteen Type II monitoring wells (MW-1 through MW-19) and one
telescoping well (TW-1) were gauged, purged and/or sampled. Free product was observed in
monitoring well MW-13; therefore, it was not sampled. The site topography is relatively flat, but
ground water flow was generally to the west, with a topographic low in the area of MW-2. The
average horizontal gradient across the site was approximately 0.009 feet per foot. The vertical
gradient calculated for paired wells MW-12/TW-1 was approximately 0.026 feet per foot in the
downward direction.
 Concentrations of benzene, toluene, ethylbenzene, xylenes, MTBE, naphthalene, tert-Amyl
alcohol (TAA), tert-Amyl methyl ether (TAME), tert-Butyl alcohol (TBA), 2-Hexanone,
isopropylbenzene, n-propylbenzene, 1,2,4-trimethylbenzene, and/or 1,3,5-trimethylbenzene that
exceeded the MACs were reported in the ground water samples collected from MW-1 through
MW-12, MW-14 and MW-17 through MW-19. The reported concentration of benzene exceeded
the GCL in the ground water sample collected from MW-5.
 Based on this information, the risk classification for the site should remain intermediate risk.
Based on the persistence of free product and ground water contaminants exceeding the GCLs,
GRI recommends a feasibility study be conducted to evaluate potential site remediation options.
In the interim, free product recovery and semi-annual ground water monitoring (including natural
attenuation parameters) should continue at the site. The next sampling event is tentatively
scheduled for December 2023.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: May 11, 2023 Stone’s Fast Save
Project Manager: Laura Minor GRI Project No. 2796

7
6.0 LIMITATIONS
This report has been prepared for the exclusive use of Mr. Ricky Stone and NCDEQ for specific application
to the referenced site in Robeson County, North Carolina. The assessment was conducted based on the
scope of work and level of effort desired by the NCDEQ and with resources adequate only for that scope
of work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that is presented in this report is indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from this data.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: May 11, 2023 Stone’s Fast Save
Project Manager: Laura Minor GRI Project No. 2796

8
7.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. n/a Will this report be submitted after the
established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO
IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain
what was missing and why.
3 If applicable, will any of the proposed attenuation milestones under the schedule approved
in the Corrective Action Plan not be met? (within a reasonable margin of error)
YES NO
IF the answer to question #3 is “NO”, skip to the certification under #8 below.
IF the answer to question #3 is “YES”, please generally describe in this cell the possible reason(s) and
outline proposed remedies. (This should be described in more detail in the report text above.)

N/A
4 Does any known or suspected source zone soil contamination or free product remain
outside of the assessed area that could be inhibiting natural attenuation?
YES NO
5 Has there been an unexpected increase in contaminant mass sufficient to suggest a
potential new release from a separate onsite or offsite source?
YES NO
IF the answer to either question #4 or #5 is “YES”, generally describe in this cell any actions
recommended to further assess or clean up this known or suspected source. (This should be described
in more detail in the report text above.)

6 Certification:
I, Samuel L. McKay, III, a Licensed Geologist for Geological Resources, Inc., do certify that the information
contained in this report is correct and accurate to the best of my knowledge.

Geological Resources, Inc. is licensed to practice engineering and geology in North Carolina. The
certification number of the company or corporation is C-2727/C-127.

FIGURES
"J
"J
"J
"J
"J
"J
"J
"JIncident
MILL ST
MAIN ST
CHAPEL ST
BOND ST
HICKORY ST
CHURCH ST
PEACH ST
WATSON ST
ASH ST
CANAL ST
WARD ST
PINE ST
CEDAR ST
MCCALLUM ST
MARTIN LUTHER KING ST
JACKSON ST
WARD RD
CHERRY ST
RAILROAD ST
MCCORMICK ST
COOLEY ST
NC130 HWY
BOSTIC ST
PEACH ST
RAILROAD ST
RAILROAD ST
JACKSON ST
RAILROAD ST
RAILROAD ST
MCCORMICK ST
WSW-8
WSW-7
WSW-6
WSW-5
WSW-4
WSW-3
WSW-2
WSW-1
9218254756
9218257577
9218352774
9218264415
9218264566
9218262299
9218262544
9218261587
9218262684
9218261376
9218260481
9218261319
9218261348
9218350490
9218367652
9218279016
9218267310
9218255926
9218262627
9218263713
9218261754
9218260443
9218261650
ELM ST
ELM ST
BROWN ST
SOUTHSIDE ST
FIGURE 2: SITE VICINITY MAPSTONES FAST SAVE119 EAST MAIN STREETROWLAND, ROBESON COUNTYNORTH CAROLINAINCIDENT NO. 29035GRI PROJECT NO. 2796
PREPARED BY:GEOLOGICAL RESOURCES, INC.MARCH 19, 2010
Source: Robeson County GIS Website
³
0 300150Feet1 inch = 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS
NOTE:Receptor survey was conducted as part of activtiesrelated to Incident No. 29579
LEGEND
"J Water Supply Well
StreetCenterlinesSep28
Well Owners and Adjacent Properties
ParcelsNov15_2005
9218262684 PIN Number
500-FOOT RADIUS

TABLES
UST ID Number A1, A2A, A2B, A3A, A3B Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number A1, A2A, A2B, A3A, A3B Facility ID Number
Owner or Operator?
Owner/Operator
TABLE 1
UST OWNER/OPERATOR INFORMATION
STONE'S FAST SAVE (INCIDENT NO. 29035)
00-0-019036
00-0-019036
Name of Owner or Operator Dates of Ownership / Operation
Name of Owner or Operator Dates of Ownership / Operation
Shiva Real Estate, LLC 12/23/2020 - present
Address Telephone Number
6569 Wade Stedman Road, Wade, NC 28395 910-644-5155
Richard Wayne Stone 6/14/1991 - 12/23/2020
Address Telephone Number
407 E. Church St, Rowland, NC 28383 910-422-3735
Page 1 of 1
Date: 08/18/22
Was Release
Associated
with UST
System?
(Yes / No)
1 Kerosene Kerosene 1,000 05/08/78 Single Wall Steel 5.3' x 6'Single Wall Steel Removed
12/01/81 Unknown
2 Gasoline Gasoline 4,000 05/10/71 Single Wall Steel
FRP 5.3' x 24'Single Wall Steel
FRP
Removed
10/30/02 Unknown
3 Gasoline Gasoline 4,000 05/10/71 Single Wall Steel
FRP 5.3' x 24'Single Wall Steel
FRP
Removed
10/30/02 Unknown
4 Kerosene Kerosene 4,000 05/10/71 Single Wall Steel
FRP 5.3' x 24'Single Wall Steel
FRP
Removed
10/30/02 Unknown
5 Gasoline Gasoline 10,000 05/10/71 Single Wall Steel
FRP 8' x 27'Single Wall Steel
FRP
Removed
10/30/02 Unknown
6 Diesel Diesel 2,000 05/08/76 Single Wall Steel 5.3' x 12'Single Wall Steel Removed
12/01/81 Unknown
7 Diesel Diesel 4,000 04/10/92 Single Wall Steel 5.3' x 24'Single Wall Steel
FRP
Removed
10/30/02 Unknown
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
TABLE 2
UST SYSTEM INFORMATION
STONE'S FAST SAVE (INCIDENT NO. 29035)
Facility ID #: 0-019036
UST
ID
No.
Current
or Most
Recent
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Tank
Dimensions
Current
or Most
Recent
Contents
Page 1 of 1
Well ID.Map No.Well Owner Address
Well Use
(Potable / Non-
Potable
etc.)
Municpal Water?
Well
Depth
(ft. BGS)
Type of Well
(Drilled/
Bored)
Well
Casing
Depth
(ft. BGS)
Well Screen
Interval
(x to y ft.
BGS)
Distance from source
area of release
(ft.)
WSW-1 921825757700 Sorn W. Beach 402 E Jackson St.
Rowland, NC 28383 Inactive Unknown 30-40 Cased Unknown Unknown ~1,220 SE
WSW-2 921825475600 Crawford Farms, Inc.P.O. Box 317
Lenox GA, 31637-0317 Inactive Unknown 30-40 Cased Unknown Unknown ~900 S
WSW-3 921825592600 Glinston A. Watts, Jr.208 Hwy 301 S
Dillon, SC 29536 Inactive Unknown 30-40 Cased Unknown Unknown ~675 SE
WSW-4 921827901600 Lillie McRae P.O. Box 201
Rowland NC 28383-0201 Inactive Unknown Unknown Unknown Unknown Unknown ~790 NE
WSW-5 921835049000 Allen J. McCall Love 502 E Jackson St.
Rowland NC 28383 Inactive Unknown Unknown Unknown Unknown Unknown ~1,470 SE
WSW-6 921835277400 Virginia L. Thompson P.O. Box 292
Rowland, NC 28383-0292 Inactive Yes Unknown Unknown Unknown Unknown ~1,360 SE
WSW-7 921826731000 VL Investments, LLC c/o Vonta Leach 5409 White Oak Dr.
Lumberton, NC 28358 Inactive Yes Unknown Unknown Unknown Unknown ~520 SE
WSW-8 921836765200 VL Investments, LLC P.O. Box 913
Rowland, NC 28383-0913 Inactive Yes Unknown Unknown Unknown Unknown ~1,480 E
Notes:
• Water supply wells are keyed to Figure 2.
• Ft. BGS : Feet below ground surface
TABLE 3
WATER SUPPLY WELL INFORMATION
STONE'S FAST SAVE (INCIDENT NO. 29035)
Date: 08/18/22 Facility ID # : 0-019036
Page 1 of 1
Date: 08/18/22 Facility ID # : 0-019036
921826254400
(Subject Site)
921826158700
921826268400
921826371300
921826165000
921826262700
921826175400
921826229900
921826137600
921826441500 Phase Two Properties 1990 North Roberts Avenue Road
Lumberton, NC 28385
921826456600 Southeastern Medical Center P.O. Box 1408
Lumberton, NC 28358
921826131900 VL Investments c/o Vonta Leach 300 Grande Oak Boulevard West
Lumberton, NC 28358
921826048100 Novus Ordo Seclorum LLC 1300 Pennsylvania Ave, STE 190-303
Washington, DC 20004
921826134800 Nagmuldin Saleh 112 S. Bond Street
Rowland, NC 28383
Note:
• Properties are keyed to Figure 2.
Shiva Real Estate LLC P.O. Box 69
Rowland, NC 28383
TABLE 4
ADJACENT PROPERTY OWNER INFORMATION
STONE'S FAST SAVE (INCIDENT NO. 29035)
Parcel Number Owner Name Address
Page 1 of 1
Date: 04/21/23
07/31/09 11.03 0.67 138.34
10/13/09 11.92 0.68 137.46
02/14/11 8.41 1.53 141.70 Before MMPE
02/18/11 5.22 ---143.58 After MMPE
03/30/11 7.55 ---141.25
08/01/11 9.85 0.33 139.23
09/02/11 11.16 0.04 137.67
09/29/11 12.02 0.02 136.80
11/02/11 12.39 ---136.41
05/07/12 9.01 0.45 140.18 Before MMPE
05/11/12 9.96 ---138.84 After MMPE
06/11/12 7.20 0.04 141.63
12/10/12 11.01 ---137.79 Before MMPE
12/14/12 9.72 ---139.08 After MMPE
01/14/13 7.92 ---140.88
12/02/13 10.74 ---138.06
06/09/14 8.59 ---140.21
09/27/16 7.49 ---141.31 Before AFVR
09/27/16 10.21 ---138.59 After AFVR
10/24/16 7.17 ---141.63
04/25/17 6.76 ---142.04
10/25/17 8.36 ---140.44
10/02/19 11.91 ---136.89 Before AFVR
10/02/19 12.87 ---135.93 After AFVR
11/06/19 12.90 ---135.90
12/23/20 7.36 ---141.44
03/28/23 8.81 ---139.99
10/13/09 11.69 ---136.36
03/30/11 7.06 ---140.99
08/01/11 9.88 ---138.17
12/10/12 11.43 ---136.62
01/14/13 8.23 ---139.82
12/02/13 11.02 ---137.03
06/09/14 8.98 ---139.07
11/06/19 13.17 ---134.88
12/23/20 7.64 ---140.41
03/28/23 8.31 ---139.74
10/13/09 11.09 ---137.46
03/30/11 7.14 ---141.41
08/01/11 9.35 ---139.20
12/10/12 10.85 ---137.70
01/14/13 7.57 ---140.98
12/02/13 10.35 ---138.20
06/09/14 8.21 ---140.34
10/24/16 6.85 ---141.70
11/06/19 12.64 ---135.91
12/23/20 6.98 ---141.57
03/28/23 7.55 ---141.00
10/13/09 12.15 1.19 137.33
02/14/11 7.51 0.91 141.73 Before MMPE
02/18/11 7.34 ---141.12 After MMPE
03/30/11 7.11 ---141.35
08/01/11 9.37 0.10 139.18
09/02/11 10.89 0.09 137.65
09/29/11 11.73 0.03 136.76
11/02/11 12.26 0.26 136.42
12/10/12 10.87 0.02 137.61 Before MMPE
12/14/12 10.48 ---137.98 After MMPE
01/14/13 7.56 ---140.90
12/02/13 10.38 ---138.08
06/09/14 8.26 ---140.20
10/24/16 6.65 ---141.81
11/06/19 12.63 0.04 135.86
10/26/20 7.36 ---141.10
11/30/20 6.80 ---141.66
12/23/20 6.97 ---141.49
01/30/23 6.35 ---142.11
02/24/23 7.11 ---141.35
03/28/23 7.81 ---140.65
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
STONE'S FAST SAVE (INCIDENT NO. 29035)
Facility ID # : 0-019036
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft. BGS)
Bottom of
Well
(ft. BGS)
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Groundwater
Elevation
(ft.)
Comments
148.05205-20512/10/03MW-2
148.80199-19908/26/03MW-1
148.46205-20512/10/03MW-4
148.55205-20512/10/03MW-3
Page 1 of 4
Date: 04/21/23
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
STONE'S FAST SAVE (INCIDENT NO. 29035)
Facility ID # : 0-019036
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft. BGS)
Bottom of
Well
(ft. BGS)
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Groundwater
Elevation
(ft.)
Comments
10/13/09 11.14 0.53 137.35
02/14/11 6.19 0.13 141.96 Before MMPE
02/18/11 8.14 ---139.90 After MMPE
03/30/11 7.71 1.16 141.33
08/01/11 10.48 1.98 139.26
09/02/11 10.64 0.28 137.64
09/29/11 11.70 0.45 136.73
11/02/11 11.70 0.01 136.35
05/07/12 7.77 1.03 141.15 Before MMPE
05/11/12 9.10 ---138.94 After MMPE
06/11/12 6.54 0.13 141.61
12/10/12 10.51 ---137.53 Before MMPE
12/14/12 10.81 ---137.23 After MMPE
01/14/13 7.23 0.03 140.84
12/02/13 11.05 1.18 138.00
05/06/14 10.32 5.02 142.03 Before AFVR
05/06/14 10.45 ---137.59 After AFVR
06/09/14 8.72 0.90 140.09
09/27/16 8.13 0.62 140.44 Before AFVR
09/27/16 10.66 ---137.38 After AFVR
10/24/16 8.43 2.43 141.70
01/24/17 7.57 1.16 141.47
02/27/17 7.72 0.25 140.53
03/27/17 7.27 ---140.77
04/25/17 6.07 ---141.97
08/21/17 9.75 0.44 138.67
09/26/17 7.47 ---140.57
10/25/17 7.74 ---140.30
10/02/19 11.17 0.07 136.93 Before AFVR
10/02/19 12.60 ---135.44 After AFVR
11/06/19 12.86 0.77 135.84
10/26/20 6.60 0.63 141.98
11/30/20 6.65 0.17 141.54
12/23/20 6.70 0.01 141.35
01/30/23 6.04 0.01 142.01
02/24/23 6.79 0.02 141.27
03/28/23 7.44 ---140.60
03/26/10 6.07 ---142.15
01/14/13 6.87 ---141.35
12/02/13 9.74 ---138.48
06/09/14 7.61 ---140.61
11/06/19 12.24 ---135.98
12/23/20 6.49 ---141.73
03/28/23 7.59 ---140.63
03/26/10 7.08 ---141.92
08/01/11 9.78 ---139.22
12/10/12 11.33 ---137.67
01/14/13 8.02 ---140.98
12/02/13 10.84 ---138.16
06/09/14 8.76 ---140.24
10/24/16 7.41 ---141.59
10/02/19 12.10 ---136.90 OBS well
10/02/19 13.13 ---135.87 OBS well
11/06/19 13.07 ---135.93
12/23/20 7.52 ---141.48
03/28/23 7.98 ---141.02
03/26/10 6.63 ---141.90
01/14/13 7.53 ---141.00
12/02/13 10.36 ---138.17
06/09/14 8.27 ---140.26
10/24/16 6.90 ---141.63
11/06/19 12.59 ---135.94
12/23/20 7.00 ---141.53
03/28/23 7.46 ---141.07
03/26/10 6.64 ---141.77
01/14/13 7.64 ---140.77
12/02/13 10.44 ---137.97
06/09/14 8.34 ---140.07
10/24/16 6.96 ---141.45
04/25/17 6.41 ---142.00
10/25/17 8.03 ---140.38
11/06/19 12.56 ---135.85
12/23/20 7.00 ---141.41
03/28/23 7.70 ---140.71
MW-5
MW-6 148.2216.517-17703/25/10
148.04205-20512/10/03
MW-9
7 7-17 17 148.53
149.00177-17703/25/10
03/25/10MW-8
MW-7
03/25/10 7 7-17 17 148.41
Page 2 of 4
Date: 04/21/23
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
STONE'S FAST SAVE (INCIDENT NO. 29035)
Facility ID # : 0-019036
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft. BGS)
Bottom of
Well
(ft. BGS)
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Groundwater
Elevation
(ft.)
Comments
03/26/10 6.93 ---141.19
01/14/13 8.32 ---139.80
12/02/13 11.01 ---137.11
06/09/14 8.41 ---139.71
11/06/19 11.83 ---136.29
12/23/20 7.26 ---140.86
03/28/23 7.37 ---140.75
03/26/10 6.38 ---141.60
01/14/13 7.47 ---140.51
12/02/13 10.51 ---137.47
06/09/14 7.97 ---140.01
10/24/16 6.63 ---141.35
04/25/17 6.21 ---141.77
10/25/17 7.81 ---140.17
11/06/19 12.13 ---135.85
12/23/20 6.72 ---141.26
03/28/23 7.49 ---140.49
03/30/11 6.78 ---141.28
08/01/11 8.92 ---139.14
12/10/12 10.58 0.10 137.57
12/14/12 8.00 ---140.06
01/14/13 7.25 ---140.81
12/02/13 8.27 ---139.79 Obstructed
06/09/14 7.91 ---140.15
10/24/16 6.54 ---141.52
04/25/17 5.99 ---142.07
10/25/17 7.72 ---140.34
10/02/19 10.83 ---137.23 OBS Well
10/02/19 9.79 ---138.27 OBS Well
11/06/19 DRY DRY DRY
12/23/20 6.98 ---141.08
03/28/23 7.29 ---140.77
03/30/11 7.08 ---141.41
01/14/13 7.54 ---140.95
12/02/13 10.35 ---138.14
06/09/14 8.24 ---140.25
09/27/16 7.95 ---140.54 Before AFVR
09/27/16 9.96 ---138.53 After AFVR
10/24/16 6.87 ---141.62
04/25/17 6.32 ---142.17
08/21/17 9.69 ---138.80
09/26/17 7.65 ---140.84
10/25/17 8.09 ---140.40
10/02/19 11.56 ---136.93 Before AFVR
10/02/19 12.38 ---136.11 After AFVR
11/06/19 12.53 ---135.96
12/23/20 7.01 ---141.48
03/28/23 7.65 0.03 140.87
03/30/11 7.07 ---141.26
08/01/11 9.20 ---139.13
12/10/12 10.79 ---137.54
01/14/13 7.54 ---140.79
12/02/13 10.31 ---138.02
05/06/14 6.54 ---141.79 Before AFVR
05/06/14 9.69 ---138.64 After AFVR
06/09/14 8.19 ---140.14
10/24/16 6.81 ---141.52
11/06/19 DRY DRY DRY
12/23/20 6.96 ---141.37
03/28/23 7.63 ---140.70
12/02/13 9.12 ---138.48
06/09/14 7.04 ---140.56
11/06/19 11.63 ---135.97
12/23/20 5.97 ---141.63
03/28/23 6.49 ---141.11
12/02/13 9.43 ---138.19
06/09/14 7.31 ---140.31
11/06/19 11.72 ---135.90
12/23/20 6.08 ---141.54
03/28/23 6.67 ---140.95
12/02/13 11.34 ---137.80
06/09/14 8.93 ---140.21
11/06/19 13.12 ---136.02
12/23/20 7.60 ---141.54
03/28/23 8.39 ---140.75
10/02/19 10.98 ---136.23
11/06/19 11.82 ---135.39
12/23/20 6.88 ---140.33
03/28/23 7.92 ---139.29
MW-10 177-17703/25/10 148.12
147.98177-17703/25/10MW-11
02/07/11 5 5-15 15 148.06MW-12
148.49155-1502/07/11MW-13
02/07/11 5 5-15 15 148.33MW-14
5
147.60
147.62MW-16
MW-15
5-205
5 5-20 20
2011/20/13
11/20/13
149.14
147.21177-17710/02/19MW-18
MW-17 205-20511/20/13
Page 3 of 4
Date: 04/21/23
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
STONE'S FAST SAVE (INCIDENT NO. 29035)
Facility ID # : 0-019036
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft. BGS)
Bottom of
Well
(ft. BGS)
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Groundwater
Elevation
(ft.)
Comments
10/02/19 11.65 ---136.35
11/06/19 12.52 ---135.48
12/23/20 7.50 ---140.50
03/28/23 8.66 ---139.34
12/03/13 11.66 ---136.57
06/09/14 8.94 ---139.29
10/24/16 7.50 ---140.73
11/06/19 13.00 ---135.23
12/23/20 7.59 ---140.64
03/28/23 8.37 ---139.86
Notes:
• * : Reference point for elevation measurements; Assumed elevation is 150.00 feet
• ** : If free product is present in a well, groundwater elevation calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.8581].
• ft BGS : feet below ground surface.
• Well construction information and top-of-casing elevation prior to March 26, 2010, is reproduced from the report entitled 'Limited Site Assessment Report',
dated February 4, 2004, prepared by Fuss & O'Nell, Inc.
TW-1
MW-19 7 7-17 17 148.00
148.234540-454012/03/13
10/02/19
Page 4 of 4
Date: 04/21/23
EPA
Method
6010B
1 600 600 500 20 6 40 128 10 70 70 40 70 70 25 100 70 70 400 400 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 10,000 5,900 8,800 40,000 30,500 70,000 11,700 100,000 26,100 70,000 28,500 24,100 15,000 NE NE NE
01/14/13 1,970 2,370 914 4,090 1,530 731 ******42.3 ***146 *1,640 465 NR NR NR NR
12/02/13 1,310 1,020 434 1,220 1,750 253 ******21.3 J ***78.6 *595 166 NR NR NR NR
06/09/14 5,100 1,180 2,350 2,880 3,730 698 ******71.3 J ***228 *1,180 323 NR NR NR NR
10/24/16 3,590 2,740 1,050 2,020 6,600 485 ******39.7 J ***127 *616 193 NR NR NR NR
04/25/17 4,890 119 3,120 903 3,200 1,160 ******NR ***NR *NR NR NR NR NR NR
10/25/17 2,400 356 1,170 604 1,970 556 ******NR ***NR *NR NR NR NR NR NR
10/02/19 2,690 142 1,380 294 1,570 557 ******NR ***NR *NR NR NR NR NR NR
11/06/19 3,370 2,350 531 1,110 3,570 310 ******NR ***NR *NR NR NR NR NR NR
12/23/20 4,900 192 3,460 760 2,230 1,480 ******88.7 ***401 *366 121 NR NR NR NR
03/28/23 3,960 109 3,330 236 J 1,110 1,190 801 J 208 J 1,060 30.0 J <20.0 <38.0 145 <50.0 <8.90 <7.80 407 <22.0 49.7 J 45.0 J NR NR NR NR
01/14/13 264 69.6 1,260 2,330 7.0 629 ******33.6 ***125 *1,280 303 NR NR NR NR
12/02/13 156 62.3 491 1,750 21.6 289 ******28.6 ***109 *829 205 NR NR NR NR
06/09/14 246 95.0 930 2,900 14.3 415 ******47.1 ***161 *1,260 302 NR NR NR NR
11/06/19 33.5 55.8 949 2,820 <3.1 591 ******NR ***NR *NR NR NR NR NR NR
12/23/20 22.7 J 15.0 J 1,270 1,390 <6.3 703 ******37.9 ***188 *1,120 274 NR NR NR NR
03/28/23 14.5 2.67 1,020 884 <0.140 476 6.56 J <0.280 2.04 J 25.1 6.32 0.425 J 54.0 <0.500 4.91 <0.078 115 1.32 992 309 NR NR NR NR
01/14/13 14.5 2.67 1020 884 <0.140 476 6.56 J <0.280 2.04 J 25.1 6.32 0.425 J 54.0 <0.500 4.91 <0.078 115 1.32 992 309 NR NR NR NR
12/02/13 68.8 11.2 171 266 656 294 ******14.8 ***38.5 *266 75.4 NR NR NR NR
06/09/14 55.4 17.2 249 425 599 329 ******20.3 ***54.0 *416 116 NR NR NR NR
11/06/19 161 0.76 J 59.2 4.4 J 81.2 109 ******NR ***NR *NR NR NR NR NR NR
12/23/20 108 1.6 J 254 121 181 302 ******10.9 ***37.3 *236 68.4 NR NR NR NR
03/28/23 25.6 <0.220 18.8 5.77 28.6 38.4 81.4 1.31 J 61.5 0.349 J 0.534 <0.380 1.73 <0.500 0.848 <0.078 2.32 <0.220 20.6 0.947 NR NR NR NR
01/14/13 1,780 534 2,520 5,310 343 1,700 ******118 ***475 *5,000 1,030 NR NR NR NR
12/02/13 908 130 1,900 2,320 557 1,530 ******127 ***531 *5,620 1,030 NR NR NR NR
06/09/14 1,400 163 2,530 3,130 177 1,330 ******135 ***584 *4,580 1,060 NR NR NR NR
10/24/16 898 108 3,190 4,450 95.9 2,380 ******289 ***1,350 *7,970 2,650 NR NR NR NR
11/06/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
12/23/20 474 71.2 2,140 1,830 <13 1,500 ******64.8 ***367 *3,270 766 NR NR NR NR
03/28/23 884 94.7 1,560 1,690 265 1,540 2,090 64.0 J <160 63.1 27.3 J 99.6 J 112 <50.0 22.1 J 63.2 J 359 <22.0 2,880 811 NR NR NR NR
01/14/13 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
12/02/13 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
06/09/14 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
10/24/16 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
04/25/17 9,950 13,500 6,360 30,300 5,400 3,180 ******NR ***NR *NR NR NR NR NR NR
10/25/17 6,790 10,500 1,750 7,910 5,480 706 ******NR ***NR *NR NR NR NR NR NR
10/02/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
11/06/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
12/23/20 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
03/28/23 8,260 11,400 2,270 9,010 3,240 854 3,690 588 477 30.6 20.9 <3.80 108 22.6 12.6 <0.780 335 14.7 3,430 862 NR NR NR NR
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
STONE'S FAST SAVE (INCIDENT NO. 29035)
Facility ID#: 0-019036
Analytical Method à EPA Methods 6200B and 602 MADEP Method VPH
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Well ID Date Collected
(mm/dd/yy)1,
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Contaminant of Concern à
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MW-5
MW-4
MW-3
GCL (mg/l)
Page 1 of 4
Date: 04/21/23
EPA
Method
6010B
1 600 600 500 20 6 40 128 10 70 70 40 70 70 25 100 70 70 400 400 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 10,000 5,900 8,800 40,000 30,500 70,000 11,700 100,000 26,100 70,000 28,500 24,100 15,000 NE NE NE
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
STONE'S FAST SAVE (INCIDENT NO. 29035)
Facility ID#: 0-019036
Analytical Method à EPA Methods 6200B and 602 MADEP Method VPH
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C9

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Well ID Date Collected
(mm/dd/yy)1,
3
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5
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Contaminant of Concern à
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(T
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GCL (mg/l)
01/14/13 142 4.7 8.3 1.3 J 2.5 29.5 ******2.6 ***3.4 *2.4 <0.10 NR NR NR NR
12/02/13 38.5 0.64 2.1 0.39 J 1.1 39.6 ******0.60 ***0.65 *1.1 <0.10 NR NR NR NR
06/09/14 175 2.2 22.9 0.79 J 3.4 89.3 ******3.3 ***4.9 *4.6 <0.10 NR NR NR NR
11/06/19 160 14.1 11.5 7.1 J 4.6 38.4 ******NR ***NR *NR NR NR NR NR NR
12/23/20 144 4.5 15.0 2.9 J 6.2 81.1 ******2.5 ***6.8 *1.0 J <0.63 NR NR NR NR
03/28/23 0.591 1.06 2.46 6.46 <0.140 8.19 2.35 J <0.280 4.97 J <0.180 <0.200 <0.380 <0.180 <0.500 <0.089 <0.078 0.543 <0.220 7.47 1.97 NR NR NR NR
01/14/13 2,200 2,900 1,590 3,850 2,000 608 ******57.6 ***214 *1,140 262 NR NR NR NR
12/02/13 1,470 2,370 1,240 4,190 1,140 518 ******58.5 ***194 *1,060 250 NR NR NR NR
06/09/14 1,830 3,580 1,530 5,200 1,380 492 ******60.7 ***239 *1,210 313 NR NR NR NR
10/24/16 1,270 236 1,120 414 921 157 ******88.2 ***328 *81.9 24.6 J NR NR NR NR
11/06/19 1,140 403 773 684 603 256 ******NR ***NR *NR NR NR NR NR NR
12/23/20 1,290 1,290 756 1,620 617 330 ******29.9 ***122 *329 105 NR NR NR NR
03/28/23 950 563 1,040 2,030 273 482 282 19.7 J 45.3 J 16.2 9.10 <3.80 46.8 8.70 3.47 J <0.780 132 3.62 J 739 179 NR NR NR NR
01/14/13 2,620 2,770 302 8,490 1,320 1,180 ******<10 ***30.9 J *2,630 938 NR NR NR NR
12/02/13 1,380 1,310 803 3,490 680 329 ******29.7 ***94.3 *1,050 315 NR NR NR NR
06/09/14 3,750 6,450 2,080 10,400 1,130 789 ******66.6 J ***231 *2,870 872 NR NR NR NR
10/24/16 1,940 1,850 3,030 8,300 341 1,410 ******201 ***704 *3,420 1,760 NR NR NR NR
11/06/19 720 294 816 1,320 67.8 198 ******NR ***NR *NR NR NR NR NR NR
12/23/20 1,370 1,560 2,440 6,480 <6.3 1,310 ******45.4 ***152 *3,360 1,010 NR NR NR NR
03/28/23 581 409 1,830 4,130 <14.0 1,080 <190 <28.0 <160 <18.0 <20.0 <38.0 69.5 <50.0 <8.90 <7.80 174 <22.0 2,700 725 NR NR NR NR
01/14/13 1,350 3,180 597 2,960 330 201 ******16.5 J ***53.6 *490 133 NR NR NR NR
12/02/13 3,210 7,030 1,530 7,450 633 564 ******46.4 J ***159 *1,450 390 NR NR NR NR
06/09/14 2,180 6,570 1,520 7,850 289 446 ******56.8 J ***215 *1,420 387 NR NR NR NR
10/24/16 2,990 8,360 1,810 9,140 190 585 ******54.8 J ***205 *1,720 489 NR NR NR NR
04/25/17 1,980 7,370 1,340 6,400 104 549 ******NR ***NR *NR NR NR NR NR NR
10/25/17 2,860 8,320 2,040 10,400 158 1,180 ******NR ***NR *NR NR NR NR NR NR
11/06/19 3,390 7,160 1,100 4,830 76.1 J 341 ******NR ***NR *NR NR NR NR NR NR
12/23/20 1,370 4,240 984 4,950 <13 511 ******23.3 J ***95.2 *1,010 273 NR NR NR NR
03/28/23 1,190 3,530 877 4,440 20.9 482 669 <2.80 <16.0 10.5 4.66 J 3.80 J 30.9 <5.00 2.76 J 8.40 J 76.6 9.73 948 269 NR NR NR NR
01/14/13 178 76.6 294 869 10.2 195 ******19.8 ***72.2 *750 189 NR NR NR NR
12/02/13 378 151 831 2,230 21.1 J 459 ******54.1 ***221 *1,600 499 NR NR NR NR
06/09/14 <5.0 287 1,090 5,000 <5.0 146 ******44.6 ***137 *871 260 NR NR NR NR
11/06/19 115 17.2 656 589 <2.5 487 ******NR ***NR *NR NR NR NR NR NR
12/23/20 24.3 2.9 229 145 <0.63 200 ******21.7 ***115 *319 178 NR NR NR NR
03/28/23 5.95 0.731 68.1 18.5 0.358 J 58.6 <1.90 <0.280 2.87 J 3.07 1.95 <0.380 8.97 <0.500 1.26 <0.078 30.0 <0.220 54.9 52.0 NR NR NR NR
MW-10
MW-9
MW-8
MW-7
MW-6
Page 2 of 4
Date: 04/21/23
EPA
Method
6010B
1 600 600 500 20 6 40 128 10 70 70 40 70 70 25 100 70 70 400 400 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 10,000 5,900 8,800 40,000 30,500 70,000 11,700 100,000 26,100 70,000 28,500 24,100 15,000 NE NE NE
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
STONE'S FAST SAVE (INCIDENT NO. 29035)
Facility ID#: 0-019036
Analytical Method à EPA Methods 6200B and 602 MADEP Method VPH
C9

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8

Al
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p
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a
t
i
cs
C9

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2
2

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Well ID Date Collected
(mm/dd/yy)1,
3
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5
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Tr
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GCL (mg/l)
01/14/13 <20 1,280 3,930 18,400 <20 785 ******153 ***478 *4,210 1,150 NR NR NR NR
12/02/13 33.0 J 1,050 3,490 16,900 10.8 J 591 ******139 ***407 *2,950 869 NR NR NR NR
06/09/14 1,210 482 3,020 7,480 73.8 J 1,510 ******211 ***930 *5,460 1,720 NR NR NR NR
10/24/16 18.7 J 572 3,200 11,800 <6.3 542 ******137 ***391 *2,690 841 NR NR NR NR
04/25/17 <25 571 3,370 12,700 <25 618 ******NR ***NR *NR NR NR NR NR NR
10/25/17 <13 398 3,340 12,000 <13 1,020 ******NR ***NR *NR NR NR NR NR NR
11/06/19 39.5 J 293 2,920 9,780 <13 481 ******NR ***NR *NR NR NR NR NR NR
12/23/20 <6.3 102 1,660 3,850 <6.3 415 ******72.9 ***262 *1,400 458 NR NR NR NR
03/28/23 <1.80 63.3 1,750 4,030 <1.40 424 <19.0 <2.80 <16.0 7.00 5.18 <3.80 89.0 <5.00 5.38 <0.780 177 <2.20 1,390 446 NR NR NR NR
01/14/13 5,160 9,740 2,120 12,700 2,270 1,530 ******82.5 ***297 *3,880 818 NR NR NR NR
12/02/13 NS NS NS NS NS NS ******NS ***NS *NS NS NR NR NR NR
06/09/14 2,260 5,380 2,480 11,300 530 953 ******82.4 J ***313 *2,890 707 NR NR NR NR
10/24/16 1,540 2,420 1,920 7,450 331 2,060 ******244 ***1,130 *3,300 2,330 NR NR NR NR
04/25/17 1,270 2,960 1,170 7,590 255 890 ******NR ***NR *NR NR NR NR NR NR
10/25/17 1,280 2,940 1,200 7,630 273 939 ******NR ***NR *NR NR NR NR NR NR
11/06/19 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/23/20 458 1,090 657 4,230 83.8 434 ******10.4 J ***36.0 *995 336 NR NR NR NR
03/28/23 967 2,070 702 4,030 323 393 2,210 49.9 J 856 21.2 3.46 J 43.6 21.8 <5.00 <0.890 17.8 46.1 8.26 818 248 NR NR NR NR
01/14/13 10,500 15,600 2,350 13,100 4,110 1,070 ******77.1 ***253 *3,100 695 NR NR NR NR
12/02/13 7,710 8,780 1,560 5,620 5,680 667 ******60.1 J ***224 *1,270 584 NR NR NR NR
06/09/14 11,000 14,400 1,830 9,660 6,940 572 ******52.7 J ***169 *1,680 492 NR NR NR NR
10/24/16 5,020 7,880 1,690 8,030 1,420 930 ******96.7 J ***418 *3,140 1,030 NR NR NR NR
04/25/17 12,200 12,400 1,810 13,100 1,530 872 ******NR ***NR *NR NR NR NR NR NR
10/25/17 9,140 12,200 2,230 10,800 1,290 998 ******NR ***NR *NR NR NR NR NR NR
10/02/19 7,420 10,500 2,300 7,360 1,010 793 ******NR ***NR *NR NR NR NR NR NR
11/06/19 3,480 2,900 952 2,690 583 429 ******NR ***NR *NR NR NR NR NR NR
12/23/20 6,220 10,400 2,130 10,600 449 1,140 ******57.4 J ***246 *2,920 924 NR NR NR NR
03/28/23 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
01/14/13 3,630 6,970 1,950 8,560 1,440 848 ******60.2 ***214 *2,260 506 NR NR NR NR
12/02/13 5,430 8,870 2,040 10,400 3,180 713 ******65.2 J ***232 *2,100 489 NR NR NR NR
06/09/14 3,910 7,810 1,950 9,760 3,350 590 ******61.9 J ***235 *1,910 471 NR NR NR NR
10/24/16 175 716 672 2,810 28.5 431 ******42.8 ***141 *1,170 330 NR NR NR NR
11/06/19 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/23/20 1,860 4,690 1,710 6,940 202 829 ******59.7 ***289 *2,350 637 NR NR NR NR
03/28/23 593 1,680 1,410 4,840 76.5 862 367 <2.80 <16.0 23.9 14.0 <3.80 84.4 <5.00 9.56 <0.780 279 10.1 2,190 612 NR NR NR NR
12/02/13 3.7 0.11 J 3.0 0.39 J 4.8 184 ******6.0 ***6.4 *45.5 3.9 NR NR NR NR
06/09/14 1.7 J <0.50 0.61 J <1.0 1.6 J 125 ******2.9 ***2.7 *13.6 <0.50 NR NR NR NR
11/06/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 ******NR ***NR *NR NR NR NR NR NR
12/23/20 <0.13 <0.13 <0.13 <0.25 <0.13 0.57 ******<0.13 ***<0.13 *<0.13 <0.13 NR NR NR NR
03/28/23 <0.180 <0.220 0.529 1.17 J <0.140 1.19 7.07 J <0.280 9.94 J <0.180 <0.200 <0.380 <0.180 <0.500 <0.089 <0.078 <0.190 <0.220 0.630 <0.180 NR NR NR NR
MW-11
MW-15
MW-14
MW-13
MW-12
Page 3 of 4
Date: 04/21/23
EPA
Method
6010B
1 600 600 500 20 6 40 128 10 70 70 40 70 70 25 100 70 70 400 400 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 10,000 5,900 8,800 40,000 30,500 70,000 11,700 100,000 26,100 70,000 28,500 24,100 15,000 NE NE NE
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
STONE'S FAST SAVE (INCIDENT NO. 29035)
Facility ID#: 0-019036
Analytical Method à EPA Methods 6200B and 602 MADEP Method VPH
C9

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Well ID Date Collected
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-
Am
y
l

al
c
o
h
o
l
(T
A
A
)
GCL (mg/l)
12/02/13 17.7 0.13 J 47.9 4.6 42.7 13.0 ******3.9 ***9.6 *15.0 10.3 NR NR NR NR
06/09/14 49.1 0.16 J 49.1 7.0 48.2 23.6 ******6.6 ***15.2 *22.5 18.4 NR NR NR NR
11/06/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 ******NR ***NR *NR NR NR NR NR NR
12/23/20 2.6 <0.13 2.4 0.37 J 4.8 5.3 ******0.86 ***3.2 *3.0 2.3 NR NR NR NR
03/28/23 <0.180 <0.220 0.726 1.47 J 0.216 J 2.62 <1.90 <0.280 2.70 J <0.180 <0.200 <0.380 <0.180 <0.500 <0.089 <0.078 0.245 J <0.220 0.717 0.271 J NR NR NR NR
12/02/13 182 95.7 189 477 2.2 J 154 ******22.2 ***73.5 *249 102 NR NR NR NR
06/09/14 41.8 8.1 325 324 2.4 265 ******41.9 ***180 *649 247 NR NR NR NR
11/06/19 6.1 0.27 J 22.2 1.2 J <0.13 46.6 ******NR ***NR *NR NR NR NR NR NR
12/23/20 1.4 <0.25 74.1 5.0 <0.25 89.9 ******16.5 ***69.5 *30.2 5.4 NR NR NR NR
03/28/23 0.514 <0.220 30.0 4.02 <0.140 51.0 <1.90 <0.280 2.46 J 4.41 3.64 <0.380 11.2 <0.500 2.63 <0.078 34.0 <0.220 14.7 4.77 NR NR NR NR
11/06/19 679 5,410 1,400 4,460 87.7 J 146 ******NR ***NR *NR NR NR NR NR NR
12/23/20 327 253 378 1,440 12.5 73.5 ******15.0 ***42.7 *377 130 NR NR NR NR
03/28/23 446 544 1,300 3,160 53.7 324 408 2.99 J <16.0 5.75 7.70 <3.80 63.5 <5.00 5.05 <0.780 131 3.05 J 942 323 NR NR NR NR
11/06/19 1,140 8,930 1,630 5,420 <25 165 ******NR ***NR *NR NR NR NR NR NR
12/23/20 214 1,930 613 2,430 <6.3 129 ******43.8 ***146 *1,400 466 NR NR NR NR
03/28/23 255 2,580 978 3,590 <1.40 346 201 <2.80 <16.0 18.0 9.48 <3.80 108 <5.00 9.33 <0.780 206 <2.20 2,490 689 NR NR NR NR
12/03/13 0.53 1.2 0.58 2.4 0.41 J 0.44 J ******<0.10 ***0.13 J *0.65 0.19 J NR NR NR NR
06/09/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 ******<0.10 ***<0.10 *<0.10 <0.10 NR NR NR NR
10/24/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 ******<0.13 ***<0.13 *<0.13 <0.13 NR NR NR NR
11/06/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 ******NR ***NR *NR NR NR NR NR NR
12/23/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 ******<0.13 ***<0.13 *<0.13 <0.13 NR NR NR NR
03/28/23 <0.180 0.422 J 0.385 J 1.96 <0.140 2.74 <1.90 <0.280 <1.60 <0.180 <0.200 <0.380 <0.180 <0.500 <0.089 <0.078 0.226 J <0.220 3.78 0.920 NR NR NR NR
12/23/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 ******<0.13 ***<0.13 *<0.13 <0.13 NR NR NR NR
03/28/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 NR NR NR <0.180 <0.200 <0.380 <0.180 <0.500 <0.089 <0.078 <0.190 <0.220 <0.190 <0.180 NR NR NR NR
Notes:
• Results reported in µg/l (micrograms per liter).
• < : Less than the method detection limit specified in the laboratory report.
• MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
• Concentrations in bold face type exceeded the MAC.
• Concentrations in bold face and italics type exceeded GCL
• NE: Not established.
• NS: Not sampled
• J: Estimated concentration.
• The MACs were below the concentrations of o-dichlorobenzene, p-dichlorobenzene and IPE in MW-5 during the 04/25/17 sampling event.
• The MAC was below the concentration of TAA in MW-1, MW-3, MW-6, MW-7, MW-9, MW-12, MW-13, MW-14, MW-18, AND MW-19 during the 12/23/20 sampling event.
• The MACs were below the concentrations of TAME in MW-1 and MW-13, TBA in MW-6, and 1,2-DCA in MW-18 during the 12/23/20 sampling event.
• Refer to laboratory report for other compounds detected at concentrations below the MACs.
• * Concentrations prior to the initial detection have not been updated.
MW-16
Trip Blank
TW-1
MW-19
MW-18
MW-17
Page 4 of 4
Date: 04/21/23
Method of Measurement:
Well ID Product Type
(gas, diesel, etc.)
Date of
Recovery
(mm/dd/yy)
Free Product
Recovery
Method*
Casing
Diameter
(inches)
Product Thickness
before Recovery
(feet)
Product Thickness
after Recovery
(feet)
Amount of Liquid
Recovered
(gallons)
Amount of
Product
Recovered
(gallons)
MW-1 2 1.53 -
MW-4 2 0.91 -
MW-5 2 0.13 -
MW-1 2 0.45 -
MW-5 2 1.03 -
MW-1 2 0.00 -
MW-4 2 0.02 -
MW-5 2 0.00 -
MW-12 2 0.10 -
MW-5 2 5.02 -
MW-14 2 0.00 -
MW-1 2 0.00 -
MW-5 2 0.62 -
MW-13 2 0.00 -
MW-5 Gasoline, diesel
and kerosene 01/24/17 Hand Bailing 2 1.16 -0.75 0.75
MW-5 Gasoline, diesel
and kerosene 02/27/17 Hand Bailing 2 0.25 -0.58 0.58
MW-5 Gasoline, diesel
and kerosene 03/27/17 Hand Bailing 2 0.00 -0.15 0.15
MW-5 Gasoline, diesel
and kerosene 08/21/17 Hand Bailing 2 0.44 -2.00 0.50
MW-5 Gasoline, diesel
and kerosene 09/26/17 Absorbent
Sock 2 0.00 -0.15 0.15
MW-5 Gasoline, diesel
and kerosene 10/25/17 Absorbent
Sock 2 0.00 -0.00 0
MW-1 2 0.00 -
MW-5 2 0.07 -
MW-13 2 0.00 -
MW-5 Gasoline, diesel
and kerosene 10/26/20
Hand Bailing/
Absorbent
Sock
2 0.63 -1.00 0.25
MW-5 Gasoline, diesel
and kerosene 11/30/20
Hand Bailing/
Absorbent
Sock
2 0.17 -0.50 0.25
MW-5 Gasoline, diesel
and kerosene 12/23/20
Hand Bailing/
Absorbent
Sock
2 0.01 -1.00 0.30
MW-4 2 0.00 -
MW-5 2 0.01 -
MW-4 2 0.00 -
MW-5 2 0.02 -
MW-4 2 0.00 -
MW-5 2 0.00 -
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Liquid Recovered (gallons) includes Total liquids (Water and Free Product) as indicated on Disposal Manifest, field notes and in absorbent socks.
• Amount of Product Recovered (in gallons) includes only the volume of free product in the tanker at the end of the event (based on Disposal Manifest
and/or Field Notes), and recovered by hand bailing and in absorbent socks
• NM: Not measured.
0.00
0.02
0.07
Hand Bailing/
Absorbent
Sock
Hand Bailing/
Absorbent
Sock
Hand Bailing/
Absorbent
Sock
0.00
0.02
0.07Gasoline, diesel
and kerosene
Gasoline, diesel
and kerosene
Gasoline, diesel
and kerosene
01/30/23
03/28/23
02/24/23
Gasoline, diesel
and kerosene
02/14/11 to
02/18/11 MMPE 9,982 101
TABLE 7
FREE PRODUCT RECOVERY RESULTS
STONE'S FAST SAVE (INCIDENT NO. 29035)
Facility ID#: 0-019036
Interface probe at top-of-casing
Gasoline, diesel
and kerosene
12/10/12 to
12/14/12 MMPE 8,340 15
Gasoline, diesel
and kerosene
05/07/12 to
05/11/12 MMPE 9,340 42
Gasoline, diesel
and kerosene 09/27/16 AFVR 1,628 4
Gasoline, diesel
and kerosene 05/06/14 AFVR 1,512 0
Gasoline, diesel
and kerosene 10/02/19 AFVR 1,060 0
Page 1 of 1
Date: 04/21/23
MW-1
MW-4
MW-5
MW-1
MW-5
MW-1
MW-4
MW-5
MW-12
MW-5
MW-14
MW-1
MW-5
MW-13
MW-5 01/24/17 Hand Bailing ------------0.75 0.75 0.75
MW-5 02/27/17 Hand Bailing ------------0.58 0.58 0.58
MW-5 03/27/17 Hand Bailing ------------0.15 0.15 0.15
MW-5 08/21/17 Hand Bailing ------------2.00 0.50 0.50
MW-5 09/26/17 Absorbent Sock ------------0.15 0.15 0.15
MW-5 10/25/17 Absorbent Sock ------------0.00 0.00 0.00
MW-1
MW-5
MW-13
MW-5 10/26/20 Hand Bailing ------------1.00 0.25 0.25
MW-5 11/30/20 Hand Bailing ------------0.50 0.25 0.25
MW-5 12/23/20 Hand Bailing ------------1.00 0.30 0.30
MW-4 ------------
MW-5 ------------
MW-4 ------------
MW-5 ------------
MW-4 ------------
MW-5 ------------
1,650.05 31,868.13 164.93 1,814.98
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Vaporized Product (in gallons) is based on Vapor Emissions Summary Sheet, = lbs emitted/6.25
• Amount of Liquid Recovered includes Total liquids (Water and Free Product) as indicated on Disposal Manifest, field notes and in absorbent socks
• Amount of Product Recovered as Liquid includes only the volume of free product in the tanker at the end of the event (based on Disposal
Manifest and/or Field Notes), and recovered by hand bailing and in absorbent socks
• Total Amount of Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Total Fluids Removed = Amount of Vaporized Product + Amount of Liquid Recovered
• Information regarding historical free product recovery activities is not available.
• NM: not measured
0.00
0.02
0.07
0.00
0.02
0.07
TABLE 8
FREE PRODUCT RECOVERY EVENT INFORMATION
STONE'S FAST SAVE (INCIDENT NO. 29035)
Facility ID #: 0-019036
Well ID Date
(mm/dd/yy)
Product Recovery
Method*
Average
Effluent
Velocity
(ft/min)
Average
Effluent
Temperature
(°F)
Average
Effluent
Concentration
(ppm)
Amount of
Vaporized
Product
(gallons)
Amount of
Liquid
Recovered
(gallons)
Amount of
Product
Recovered as
Liquid (gallons)
Total Amount
of Product
Recovered
(gallons)
1,559.24
05/07/12 to
05/11/12 MMPE 2,717 96.00 49,875 82.29 9,340 42 124.29
02/14/11 to
02/18/11 MMPE 2,718.18 92.73 88,727.27 1,458.24 9,982 101
81.28 8,340 15 96.28
05/06/14 AFVR 2,070.05 176.30 3,124.10 1.65 1,512 0 1.65
12/10/12 to
12/14/12 MMPE 3,700 70.7 26,600
1,628 4 4.98
10/02/19 AFVR 1,178.00 93.40 1,513.10 25.61 1,060
09/27/16 AFVR 1,756.95 174.95 2,011.79 0.98
0 25.61
Totals
SUMMARY OF FLUID REMOVAL
Summary Total Fluids Removed (in gallons)Total Product Removed (in gallons)
Hand Bailing
Hand Bailing
Hand Bailing
03/28/23
02/24/23
01/30/23
0.00
0.02
0.07
Current Event 0.09 0.09
Total to Date 33,518.18 1,814.98
Page 1 of 1
Date: 04/21/23
Wells Included in Event Product Recovery
Method*
Date of Event
(mm/dd/yy)
Total Amount of
Vapor Phase and
Liquids Recovered
(gallons)
Cost of Free
Product Recovery
Event
Cost Per Gallon
Recovered
MW-1, MW-4, MW-5 MMPE 02/14/11 to
02/18/11 11,440.24 $11,821.50 $1.03
MW-1, MW-5 MMPE 05/7/12 to
05/11/12 9,422.29 $11,292.00 $1.20
MW-1, MW-4, MW-5,
MW-12 MMPE 12/10/12 to
12/14/12 8,421.28 $11,613.00 $1.38
MW-5, MW-14 AFVR 05/19/14 1,513.65 $1,828.80 $1.21
MW-1, MW-5, MW-13 AFVR 09/27/16 1,628.98 $2,891.50 $1.78
MW-5 Hand Bailing January -
March 2017 1.48 $1,605.00 $1,084.46
MW-5 Hand Bailing &
Absorbent Socks
August-
October 2017 2.15 $1,495.00 $695.35
MW-1, MW-5, MW-13 AFVR 10/02/19 1,085.61 $3,010.00 $2.77
MW-5 Hand Bailing &
Absorbent Socks
October-
December
2020
2.50 $981.27 $392.51
MW-4 and MW-5 Hand Bailing &
Absorbent Socks
January -
March 2023 0.09 $1,540.00 $17,111.11
33,518.27 $48,078.07 $1.43
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE) and absorbent socks.
• Cost of Free Product Recovery Event includes supervision, travel, mileage, per diem, and subcontractor costs
TABLE 9
FREE PRODUCT RECOVERY COST SUMMARY
STONE'S FAST SAVE (INCIDENT NO. 29035)
Facility ID #: 0-019036
Comments
TOTAL (to date)
Page 1 of 1

APPENDICES

APPENDIX A
State Correspondence

October 24, 2022

Mr. Richard Wayne Stone 407 East Church Street
Rowland, NC 28383

Re: Notice of Regulatory Requirements
15A NCAC 2L .0407(d) Risk-based Assessment and Corrective Action for Petroleum
Underground Storage Tanks
Stone’s Fast Save
119 East Main Street
Rowland, Robeson County
Incident Number: 29035
Risk Classification: Intermediate
Ranking: I-220-A
Dear Mr. Stone,
The requested soil delineation data reported in the Soil Cleanup Plan format was received by was
approved by the Fayetteville Regional Office on September 19, 2022. This office requests the following:

• Continue free product recovery using absorbent sock materials supplemented with
hand bailing while on-site, as necessary,
• Gauge and/or sample all investigation monitoring wells (not done since December 2020),
• Submit a Monitoring Report (MRP) within 90 days of receipt of this letter. The MRP should also
elaborate on a remedial strategy can include targeted soil excavation, mechanical technology,
chemical injection, or a combination thereof. The goal of the remedial strategy should be to
suggest a remedial method that will most cost effectively treat both free product and reduce
groundwater GCLs. This incident must proceed towards a Corrective Action Plan.
• Lastly, ownership of this petroleum impacted parcel was transferred as evidenced by a deed
recorded on 1/5/2021 (Bk: 2263, Pg: 681-687). A Notice of Residual Petroleum was required
by N.C.G.S. 143B-279.9 and 143B-279.11, prior to conveyance and has not been completed.
Please record a Notice of Residual Petroleum as soon as possible.
If you have questions regarding the information contained in this letter, please contact me at the
Fayetteville Regional Office address below or at [phone].
Sincerely,

Kenneth E. Currie, Hydrogeologist
Fayetteville Regional Office
UST Section, Division of Waste Management

c: Mrs. Laura Minor, Geological Resources, Inc. (email copy) Mr. Rohit Shetty, P.E., Geological Resources, Inc. (email copy)
Mr. William Regenthal, P.G., Geological Resources, Inc. (email copy)
FAY/UST Electronic File #29035
2796 Received OCT 2022

APPENDIX B
Notice of Residual Petroleum

APPENDIX C
Laboratory Analytical Report

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

4/12/2023
Geological Resources, Inc. Laura Minor
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-088-0022 Client Project Description: Stone's Fast Save
GRI #2796
Dear Laura Minor:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 3/29/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 142
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-088-0022
Page 2 of 142
Report Number:
Sample Summary Table
Client Project Description:
23-088-0022
Stone's Fast Save
GRI #2796
Lab No Client Sample ID Matrix Date Collected Date Received
03/28/2023 08:40Aqueous 92521 Trip Blank 03/29/2023
03/28/2023 09:42Aqueous 92522 TW-1 03/29/2023
03/28/2023 09:57Aqueous 92523 MW-19 03/29/2023
03/28/2023 10:11Aqueous 92524 MW-18 03/29/2023
03/28/2023 10:23Aqueous 92525 MW-10 03/29/2023
03/28/2023 10:35Aqueous 92526 MW-11 03/29/2023
03/28/2023 10:46Aqueous 92527 MW-17 03/29/2023
03/28/2023 10:58Aqueous 92528 MW-16 03/29/2023
03/28/2023 11:10Aqueous 92529 MW-15 03/29/2023
03/28/2023 11:21Aqueous 92530 MW-14 03/29/2023
03/28/2023 11:33Aqueous 92531 MW-12 03/29/2023
03/28/2023 11:45Aqueous 92532 MW-9 03/29/2023
03/28/2023 11:57Aqueous 92533 MW-8 03/29/2023
03/28/2023 12:08Aqueous 92534 MW-7 03/29/2023
03/28/2023 12:22Aqueous 92535 MW-6 03/29/2023
03/28/2023 12:36Aqueous 92536 MW-4 03/29/2023
03/28/2023 12:49Aqueous 92537 MW-3 03/29/2023
03/28/2023 13:02Aqueous 92538 MW-2 03/29/2023
03/28/2023 13:16Aqueous 92539 MW-1 03/29/2023
03/28/2023 13:28Aqueous 92540 MW-5 03/29/2023
Page 3 of 142
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-088-0022
Report Limit
Project:Stone's Fast Save
V 92522TW-1
J0.385 04/10/2023 22:526200BEthylbenzeneµg/L 0.170
2.74 04/10/2023 22:526200BNaphthaleneµg/L 0.470
J0.226 04/10/2023 22:526200Bn-Propylbenzene µg/L 0.190
J0.422 04/10/2023 22:526200BTolueneµg/L 0.220
3.78 04/10/2023 22:526200B1,2,4-Trimethylbenzene µg/L 0.190
0.920 04/10/2023 22:526200B1,3,5-Trimethylbenzene µg/L 0.180
0.695 04/10/2023 22:526200Bo-Xylene µg/L 0.210
1.26 04/10/2023 22:526200Bm,p-Xylene µg/L 0.420
1.96 04/10/2023 22:526200BXylene (Total)µg/L 0.210
V 92523MW-19
255 04/06/2023 04:206200BBenzeneµg/L 1.80
18.0 04/06/2023 04:206200Bn-Butylbenzene µg/L 1.80
9.48 04/06/2023 04:206200Bsec-Butyl benzene µg/L 2.00
978 04/06/2023 04:206200BEthylbenzeneµg/L 1.70
108 04/06/2023 04:206200BIsopropylbenzeneµg/L 1.80
9.33 04/06/2023 04:206200B4-Isopropyl toluene µg/L 0.890
346 04/06/2023 04:206200BNaphthaleneµg/L 4.70
206 04/06/2023 04:206200Bn-Propylbenzene µg/L 1.90
201 04/06/2023 04:206200Btert-Amyl Alcohol (TAA)µg/L 19.0
2580 04/11/2023 00:546200BTolueneµg/L 22.0
2490 04/11/2023 00:546200B1,2,4-Trimethylbenzene µg/L 19.0
689 04/06/2023 04:206200B1,3,5-Trimethylbenzene µg/L 1.80
523 04/06/2023 04:206200Bo-Xylene µg/L 2.10
3070 04/11/2023 00:546200Bm,p-Xylene µg/L 42.0
3590 04/06/2023 04:206200BXylene (Total)µg/L 2.10
V 92524MW-18
446 04/06/2023 04:456200BBenzeneµg/L 1.80
5.75 04/06/2023 04:456200Bn-Butylbenzene µg/L 1.80
7.70 04/06/2023 04:456200Bsec-Butyl benzene µg/L 2.00
1300 04/11/2023 01:186200BEthylbenzeneµg/L 17.0
63.5 04/06/2023 04:456200BIsopropylbenzeneµg/L 1.80
5.05 04/06/2023 04:456200B4-Isopropyl toluene µg/L 0.890
53.7 04/06/2023 04:456200BMethyl tert-butyl ether (MTBE)µg/L 1.40
324 04/06/2023 04:456200BNaphthaleneµg/L 4.70
131 04/06/2023 04:456200Bn-Propylbenzene µg/L 1.90
J3.05 04/06/2023 04:456200BStyreneµg/L 2.20
Page 4 of 142
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-088-0022
Report Limit
Project:Stone's Fast Save
V 92524MW-18
408 04/06/2023 04:456200Btert-Amyl Alcohol (TAA)µg/L 19.0
J2.99 04/06/2023 04:456200Btert-Amyl Methyl Ether (TAME)µg/L 2.80
544 04/06/2023 04:456200BTolueneµg/L 2.20
942 04/06/2023 04:456200B1,2,4-Trimethylbenzene µg/L 1.90
323 04/06/2023 04:456200B1,3,5-Trimethylbenzene µg/L 1.80
32.1 04/06/2023 04:456200Bo-Xylene µg/L 2.10
3130 04/11/2023 01:186200Bm,p-Xylene µg/L 42.0
3160 04/06/2023 04:456200BXylene (Total)µg/L 2.10
V 92525MW-10
5.95 04/06/2023 00:406200BBenzeneµg/L 0.180
3.07 04/06/2023 00:406200Bn-Butylbenzene µg/L 0.180
1.95 04/06/2023 00:406200Bsec-Butyl benzene µg/L 0.200
68.1 04/06/2023 00:406200BEthylbenzeneµg/L 0.170
8.97 04/06/2023 00:406200BIsopropylbenzeneµg/L 0.180
1.26 04/06/2023 00:406200B4-Isopropyl toluene µg/L 0.089
J0.358 04/06/2023 00:406200BMethyl tert-butyl ether (MTBE)µg/L 0.140
58.6 04/06/2023 00:406200BNaphthaleneµg/L 0.470
30.0 04/06/2023 00:406200Bn-Propylbenzene µg/L 0.190
J2.87 04/06/2023 00:406200Btert-Butyl Alcohol (TBA)µg/L 1.60
0.731 04/06/2023 00:406200BTolueneµg/L 0.220
54.9 04/06/2023 00:406200B1,2,4-Trimethylbenzene µg/L 0.190
52.0 04/06/2023 00:406200B1,3,5-Trimethylbenzene µg/L 0.180
3.37 04/06/2023 00:406200Bo-Xylene µg/L 0.210
15.1 04/06/2023 00:406200Bm,p-Xylene µg/L 0.420
18.5 04/06/2023 00:406200BXylene (Total)µg/L 0.210
V 92526MW-11
7.00 04/06/2023 05:096200Bn-Butylbenzene µg/L 1.80
5.18 04/06/2023 05:096200Bsec-Butyl benzene µg/L 2.00
1750 04/11/2023 01:436200BEthylbenzeneµg/L 17.0
89.0 04/06/2023 05:096200BIsopropylbenzeneµg/L 1.80
5.38 04/06/2023 05:096200B4-Isopropyl toluene µg/L 0.890
424 04/06/2023 05:096200BNaphthaleneµg/L 4.70
177 04/06/2023 05:096200Bn-Propylbenzene µg/L 1.90
63.3 04/06/2023 05:096200BTolueneµg/L 2.20
1390 04/11/2023 01:436200B1,2,4-Trimethylbenzene µg/L 19.0
446 04/06/2023 05:096200B1,3,5-Trimethylbenzene µg/L 1.80
Page 5 of 142
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-088-0022
Report Limit
Project:Stone's Fast Save
V 92526MW-11
997 04/11/2023 01:436200Bo-Xylene µg/L 21.0
3030 04/11/2023 01:436200Bm,p-Xylene µg/L 42.0
4030 04/11/2023 01:436200BXylene (Total)µg/L 21.0
V 92527MW-17
0.514 04/06/2023 01:056200BBenzeneµg/L 0.180
4.41 04/06/2023 01:056200Bn-Butylbenzene µg/L 0.180
3.64 04/06/2023 01:056200Bsec-Butyl benzene µg/L 0.200
30.0 04/06/2023 01:056200BEthylbenzeneµg/L 0.170
11.2 04/06/2023 01:056200BIsopropylbenzeneµg/L 0.180
2.63 04/06/2023 01:056200B4-Isopropyl toluene µg/L 0.089
51.0 04/06/2023 01:056200BNaphthaleneµg/L 0.470
34.0 04/06/2023 01:056200Bn-Propylbenzene µg/L 0.190
J2.46 04/06/2023 01:056200Btert-Butyl Alcohol (TBA)µg/L 1.60
14.7 04/06/2023 01:056200B1,2,4-Trimethylbenzene µg/L 0.190
4.77 04/06/2023 01:056200B1,3,5-Trimethylbenzene µg/L 0.180
1.42 04/06/2023 01:056200Bo-Xylene µg/L 0.210
2.60 04/06/2023 01:056200Bm,p-Xylene µg/L 0.420
4.02 04/06/2023 01:056200BXylene (Total)µg/L 0.210
V 92528MW-16
0.726 04/06/2023 01:296200BEthylbenzeneµg/L 0.170
J0.216 04/06/2023 01:296200BMethyl tert-butyl ether (MTBE)µg/L 0.140
2.62 04/06/2023 01:296200BNaphthaleneµg/L 0.470
J0.245 04/06/2023 01:296200Bn-Propylbenzene µg/L 0.190
J2.70 04/06/2023 01:296200Btert-Butyl Alcohol (TBA)µg/L 1.60
0.717 04/06/2023 01:296200B1,2,4-Trimethylbenzene µg/L 0.190
J0.271 04/06/2023 01:296200B1,3,5-Trimethylbenzene µg/L 0.180
J0.323 04/06/2023 01:296200Bo-Xylene µg/L 0.210
1.15 04/06/2023 01:296200Bm,p-Xylene µg/L 0.420
J1.47 04/06/2023 01:296200BXylene (Total)µg/L 0.210
V 92529MW-15
0.529 04/06/2023 01:546200BEthylbenzeneµg/L 0.170
1.19 04/06/2023 01:546200BNaphthaleneµg/L 0.470
J9.94 04/06/2023 01:546200Btert-Butyl Alcohol (TBA)µg/L 1.60
J7.07 04/06/2023 01:546200Btert-Amyl Alcohol (TAA)µg/L 1.90
0.630 04/06/2023 01:546200B1,2,4-Trimethylbenzene µg/L 0.190
Page 6 of 142
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-088-0022
Report Limit
Project:Stone's Fast Save
V 92529MW-15
J0.264 04/06/2023 01:546200Bo-Xylene µg/L 0.210
J0.902 04/06/2023 01:546200Bm,p-Xylene µg/L 0.420
J1.17 04/06/2023 01:546200BXylene (Total)µg/L 0.210
V 92530MW-14
593 04/06/2023 05:346200BBenzeneµg/L 1.80
23.9 04/06/2023 05:346200Bn-Butylbenzene µg/L 1.80
14.0 04/06/2023 05:346200Bsec-Butyl benzene µg/L 2.00
1410 04/11/2023 02:076200BEthylbenzeneµg/L 17.0
84.4 04/06/2023 05:346200BIsopropylbenzeneµg/L 1.80
9.56 04/06/2023 05:346200B4-Isopropyl toluene µg/L 0.890
76.5 04/06/2023 05:346200BMethyl tert-butyl ether (MTBE)µg/L 1.40
862 04/06/2023 05:346200BNaphthaleneµg/L 4.70
279 04/06/2023 05:346200Bn-Propylbenzene µg/L 1.90
10.1 04/06/2023 05:346200BStyreneµg/L 2.20
367 04/06/2023 05:346200Btert-Amyl Alcohol (TAA)µg/L 19.0
1680 04/11/2023 02:076200BTolueneµg/L 22.0
2190 04/11/2023 02:076200B1,2,4-Trimethylbenzene µg/L 19.0
612 04/06/2023 05:346200B1,3,5-Trimethylbenzene µg/L 1.80
1560 04/11/2023 02:076200Bo-Xylene µg/L 21.0
3280 04/11/2023 02:076200Bm,p-Xylene µg/L 42.0
4840 04/11/2023 02:076200BXylene (Total)µg/L 21.0
V 92531MW-12
967 04/06/2023 05:586200BBenzeneµg/L 1.80
21.2 04/06/2023 05:586200Bn-Butylbenzene µg/L 1.80
J3.46 04/06/2023 05:586200Bsec-Butyl benzene µg/L 2.00
702 04/06/2023 05:586200BEthylbenzeneµg/L 1.70
43.6 04/06/2023 05:586200B2-Hexanone µg/L 3.80
21.8 04/06/2023 05:586200BIsopropylbenzeneµg/L 1.80
J37.5 04/06/2023 05:586200BMethyl Ethyl Ketone (MEK)µg/L 7.10
323 04/06/2023 05:586200BMethyl tert-butyl ether (MTBE)µg/L 1.40
17.8 04/06/2023 05:586200B4-Methyl-2-Pentanone µg/L 0.780
393 04/06/2023 05:586200BNaphthaleneµg/L 4.70
46.1 04/06/2023 05:586200Bn-Propylbenzene µg/L 1.90
8.26 04/06/2023 05:586200BStyreneµg/L 2.20
856 04/06/2023 05:586200Btert-Butyl Alcohol (TBA)µg/L 16.0
2210 04/11/2023 02:316200Btert-Amyl Alcohol (TAA)µg/L 190
Page 7 of 142
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-088-0022
Report Limit
Project:Stone's Fast Save
V 92531MW-12
J49.9 04/06/2023 05:586200Btert-Amyl Methyl Ether (TAME)µg/L 2.80
2070 04/11/2023 02:316200BTolueneµg/L 22.0
818 04/06/2023 05:586200B1,2,4-Trimethylbenzene µg/L 1.90
248 04/06/2023 05:586200B1,3,5-Trimethylbenzene µg/L 1.80
1400 04/11/2023 02:316200Bo-Xylene µg/L 21.0
2630 04/11/2023 02:316200Bm,p-Xylene µg/L 42.0
4030 04/11/2023 02:316200BXylene (Total)µg/L 21.0
V 92532MW-9
1190 04/11/2023 02:566200BBenzeneµg/L 18.0
10.5 04/06/2023 06:236200Bn-Butylbenzene µg/L 1.80
J4.66 04/06/2023 06:236200Bsec-Butyl benzene µg/L 2.00
877 04/06/2023 06:236200BEthylbenzeneµg/L 1.70
J3.80 04/06/2023 06:236200B2-Hexanone µg/L 3.80
30.9 04/06/2023 06:236200BIsopropylbenzeneµg/L 1.80
J2.76 04/06/2023 06:236200B4-Isopropyl toluene µg/L 0.890
20.9 04/06/2023 06:236200BMethyl tert-butyl ether (MTBE)µg/L 1.40
J8.40 04/06/2023 06:236200B4-Methyl-2-Pentanone µg/L 0.780
482 04/06/2023 06:236200BNaphthaleneµg/L 4.70
76.6 04/06/2023 06:236200Bn-Propylbenzene µg/L 1.90
9.73 04/06/2023 06:236200BStyreneµg/L 2.20
669 04/06/2023 06:236200Btert-Amyl Alcohol (TAA)µg/L 19.0
3530 04/11/2023 02:566200BTolueneµg/L 22.0
948 04/06/2023 06:236200B1,2,4-Trimethylbenzene µg/L 1.90
269 04/06/2023 06:236200B1,3,5-Trimethylbenzene µg/L 1.80
1450 04/11/2023 02:566200Bo-Xylene µg/L 21.0
2990 04/11/2023 02:566200Bm,p-Xylene µg/L 42.0
4440 04/11/2023 02:566200BXylene (Total)µg/L 21.0
V 92533MW-8
581 04/06/2023 19:306200BBenzeneµg/L 18.0
1830 04/06/2023 19:306200BEthylbenzeneµg/L 17.0
69.5 04/06/2023 19:306200BIsopropylbenzeneµg/L 18.0
J18604/06/2023 19:306200BMethyl Ethyl Ketone (MEK)µg/L 71.0
1080 04/06/2023 19:306200BNaphthaleneµg/L 47.0
174 04/06/2023 19:306200Bn-Propylbenzene µg/L 19.0
409 04/06/2023 19:306200BTolueneµg/L 22.0
2700 04/06/2023 19:306200B1,2,4-Trimethylbenzene µg/L 19.0
Page 8 of 142
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-088-0022
Report Limit
Project:Stone's Fast Save
V 92533MW-8
725 04/06/2023 19:306200B1,3,5-Trimethylbenzene µg/L 18.0
388 04/06/2023 19:306200Bo-Xylene µg/L 21.0
3740 04/06/2023 19:306200Bm,p-Xylene µg/L 42.0
4130 04/06/2023 19:306200BXylene (Total)µg/L 21.0
V 92534MW-7
950 04/06/2023 06:196200BBenzeneµg/L 1.80
16.2 04/06/2023 06:196200Bn-Butylbenzene µg/L 1.80
9.10 04/06/2023 06:196200Bsec-Butyl benzene µg/L 2.00
8.70 04/06/2023 06:196200BDi-Isopropyl Ether (DIPE)µg/L 5.00
1040 04/11/2023 04:096200BEthylbenzeneµg/L 17.0
46.8 04/06/2023 06:196200BIsopropylbenzeneµg/L 1.80
J3.47 04/06/2023 06:196200B4-Isopropyl toluene µg/L 0.890
273 04/06/2023 06:196200BMethyl tert-butyl ether (MTBE)µg/L 1.40
482 04/06/2023 06:196200BNaphthaleneµg/L 4.70
132 04/06/2023 06:196200Bn-Propylbenzene µg/L 1.90
J3.62 04/06/2023 06:196200BStyreneµg/L 2.20
J45.3 04/06/2023 06:196200Btert-Butyl Alcohol (TBA)µg/L 16.0
282 04/06/2023 06:196200Btert-Amyl Alcohol (TAA)µg/L 19.0
J19.7 04/06/2023 06:196200Btert-Amyl Methyl Ether (TAME)µg/L 2.80
563 04/06/2023 06:196200BTolueneµg/L 2.20
739 04/06/2023 06:196200B1,2,4-Trimethylbenzene µg/L 1.90
179 04/06/2023 06:196200B1,3,5-Trimethylbenzene µg/L 1.80
248 04/06/2023 06:196200Bo-Xylene µg/L 2.10
1780 04/06/2023 06:196200Bm,p-Xylene µg/L 4.20
2030 04/06/2023 06:196200BXylene (Total)µg/L 2.10
V 92535MW-6
0.591 04/06/2023 01:476200BBenzeneµg/L 0.180
2.46 04/06/2023 01:476200BEthylbenzeneµg/L 0.170
8.19 04/06/2023 01:476200BNaphthaleneµg/L 0.470
0.543 04/06/2023 01:476200Bn-Propylbenzene µg/L 0.190
J4.97 04/06/2023 01:476200Btert-Butyl Alcohol (TBA)µg/L 1.60
J2.35 04/06/2023 01:476200Btert-Amyl Alcohol (TAA)µg/L 1.90
1.06 04/06/2023 01:476200BTolueneµg/L 0.220
7.47 04/06/2023 01:476200B1,2,4-Trimethylbenzene µg/L 0.190
1.97 04/06/2023 01:476200B1,3,5-Trimethylbenzene µg/L 0.180
1.10 04/06/2023 01:476200Bo-Xylene µg/L 0.210
Page 9 of 142
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-088-0022
Report Limit
Project:Stone's Fast Save
V 92535MW-6
5.36 04/06/2023 01:476200Bm,p-Xylene µg/L 0.420
6.46 04/06/2023 01:476200BXylene (Total)µg/L 0.210
V 92536MW-4
884 04/06/2023 19:556200BBenzeneµg/L 18.0
63.1 04/06/2023 19:556200Bn-Butylbenzene µg/L 18.0
J27.3 04/06/2023 19:556200Bsec-Butyl benzene µg/L 20.0
1560 04/06/2023 19:556200BEthylbenzeneµg/L 17.0
J99.6 04/06/2023 19:556200B2-Hexanone µg/L 38.0
112 04/06/2023 19:556200BIsopropylbenzeneµg/L 18.0
J22.1 04/06/2023 19:556200B4-Isopropyl toluene µg/L 8.90
265 04/06/2023 19:556200BMethyl tert-butyl ether (MTBE)µg/L 14.0
J63.2 04/06/2023 19:556200B4-Methyl-2-Pentanone µg/L 7.80
1540 04/06/2023 19:556200BNaphthaleneµg/L 47.0
359 04/06/2023 19:556200Bn-Propylbenzene µg/L 19.0
2090 04/06/2023 19:556200Btert-Amyl Alcohol (TAA)µg/L 190
J64.0 04/06/2023 19:556200Btert-Amyl Methyl Ether (TAME)µg/L 28.0
94.7 04/06/2023 19:556200BTolueneµg/L 22.0
2880 04/06/2023 19:556200B1,2,4-Trimethylbenzene µg/L 19.0
811 04/06/2023 19:556200B1,3,5-Trimethylbenzene µg/L 18.0
62.6 04/06/2023 19:556200Bo-Xylene µg/L 21.0
1630 04/06/2023 19:556200Bm,p-Xylene µg/L 42.0
1690 04/06/2023 19:556200BXylene (Total)µg/L 21.0
V 92537MW-3
25.6 04/06/2023 02:156200BBenzeneµg/L 0.180
J0.349 04/06/2023 02:156200Bn-Butylbenzene µg/L 0.180
0.534 04/06/2023 02:156200Bsec-Butyl benzene µg/L 0.200
18.8 04/06/2023 02:156200BEthylbenzeneµg/L 0.170
1.73 04/06/2023 02:156200BIsopropylbenzeneµg/L 0.180
0.848 04/06/2023 02:156200B4-Isopropyl toluene µg/L 0.089
28.6 04/06/2023 02:156200BMethyl tert-butyl ether (MTBE)µg/L 0.140
38.4 04/06/2023 02:156200BNaphthaleneµg/L 0.470
2.32 04/06/2023 02:156200Bn-Propylbenzene µg/L 0.190
61.5 04/06/2023 02:156200Btert-Butyl Alcohol (TBA)µg/L 1.60
81.4 04/06/2023 02:156200Btert-Amyl Alcohol (TAA)µg/L 1.90
J1.31 04/06/2023 02:156200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
20.6 04/06/2023 02:156200B1,2,4-Trimethylbenzene µg/L 0.190
Page 10 of 142
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-088-0022
Report Limit
Project:Stone's Fast Save
V 92537MW-3
0.947 04/06/2023 02:156200B1,3,5-Trimethylbenzene µg/L 0.180
4.35 04/06/2023 02:156200Bo-Xylene µg/L 0.210
1.42 04/06/2023 02:156200Bm,p-Xylene µg/L 0.420
5.77 04/06/2023 02:156200BXylene (Total)µg/L 0.210
V 92538MW-2
14.5 04/06/2023 05:526200BBenzeneµg/L 0.180
25.1 04/06/2023 05:526200Bn-Butylbenzene µg/L 0.180
6.32 04/06/2023 05:526200Bsec-Butyl benzene µg/L 0.200
1020 04/11/2023 03:456200BEthylbenzeneµg/L 17.0
J0.425 04/06/2023 05:526200B2-Hexanone µg/L 0.380
54.0 04/06/2023 05:526200BIsopropylbenzeneµg/L 0.180
4.91 04/06/2023 05:526200B4-Isopropyl toluene µg/L 0.089
476 04/11/2023 03:456200BNaphthaleneµg/L 47.0
115 04/11/2023 03:456200Bn-Propylbenzene µg/L 19.0
1.32 04/06/2023 05:526200BStyreneµg/L 0.220
J2.04 04/06/2023 05:526200Btert-Butyl Alcohol (TBA)µg/L 1.60
J6.56 04/06/2023 05:526200Btert-Amyl Alcohol (TAA)µg/L 1.90
2.67 04/06/2023 05:526200BTolueneµg/L 0.220
992 04/11/2023 03:456200B1,2,4-Trimethylbenzene µg/L 19.0
309 04/11/2023 03:456200B1,3,5-Trimethylbenzene µg/L 18.0
252 04/11/2023 03:456200Bo-Xylene µg/L 21.0
632 04/11/2023 03:456200Bm,p-Xylene µg/L 42.0
884 04/11/2023 03:456200BXylene (Total)µg/L 21.0
V 92539MW-1
3960 04/06/2023 21:086200BBenzeneµg/L 18.0
J30.0 04/06/2023 21:086200Bn-Butylbenzene µg/L 18.0
3330 04/06/2023 21:086200BEthylbenzeneµg/L 17.0
145 04/06/2023 21:086200BIsopropylbenzeneµg/L 18.0
1110 04/06/2023 21:086200BMethyl tert-butyl ether (MTBE)µg/L 14.0
1190 04/06/2023 21:086200BNaphthaleneµg/L 47.0
407 04/06/2023 21:086200Bn-Propylbenzene µg/L 19.0
1060 04/06/2023 21:086200Btert-Butyl Alcohol (TBA)µg/L 160
J80104/06/2023 21:086200Btert-Amyl Alcohol (TAA)µg/L 190
J20804/06/2023 21:086200Btert-Amyl Methyl Ether (TAME)µg/L 28.0
109 04/06/2023 21:086200BTolueneµg/L 22.0
J49.7 04/06/2023 21:086200B1,2,4-Trimethylbenzene µg/L 19.0
Page 11 of 142
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-088-0022
Report Limit
Project:Stone's Fast Save
V 92539MW-1
J45.0 04/06/2023 21:086200B1,3,5-Trimethylbenzene µg/L 18.0
J27.4 04/06/2023 21:086200Bo-Xylene µg/L 21.0
209 04/06/2023 21:086200Bm,p-Xylene µg/L 42.0
J23604/06/2023 21:086200BXylene (Total)µg/L 21.0
V 92540MW-5
8260 04/11/2023 04:346200BBenzeneµg/L 18.0
30.6 04/06/2023 06:476200Bn-Butylbenzene µg/L 1.80
20.9 04/06/2023 06:476200Bsec-Butyl benzene µg/L 2.00
22.6 04/06/2023 06:476200BDi-Isopropyl Ether (DIPE)µg/L 5.00
2270 04/11/2023 04:346200BEthylbenzeneµg/L 17.0
108 04/06/2023 06:476200BIsopropylbenzeneµg/L 1.80
12.6 04/06/2023 06:476200B4-Isopropyl toluene µg/L 0.890
3240 04/11/2023 04:346200BMethyl tert-butyl ether (MTBE)µg/L 14.0
854 04/06/2023 06:476200BNaphthaleneµg/L 4.70
335 04/06/2023 06:476200Bn-Propylbenzene µg/L 1.90
14.7 04/06/2023 06:476200BStyreneµg/L 2.20
477 04/06/2023 06:476200Btert-Butyl Alcohol (TBA)µg/L 16.0
3690 04/11/2023 04:346200Btert-Amyl Alcohol (TAA)µg/L 190
588 04/06/2023 06:476200Btert-Amyl Methyl Ether (TAME)µg/L 2.80
11400 04/12/2023 09:066200BTolueneµg/L 220
3430 04/11/2023 04:346200B1,2,4-Trimethylbenzene µg/L 19.0
862 04/06/2023 06:476200B1,3,5-Trimethylbenzene µg/L 1.80
1990 04/11/2023 04:346200Bo-Xylene µg/L 21.0
7020 04/11/2023 04:346200Bm,p-Xylene µg/L 42.0
9010 04/11/2023 04:346200BXylene (Total)µg/L 21.0
Page 12 of 142

Client: Geological Resources, Inc. CASE NARRATIVE
Project: Stone's Fast Save Lab Report Number: 23-088-0022
Date: 4/12/2023
Volatile Organic Compounds - GC/MS Method 6200B Analyte: 1,2,3-Trichlorobenzene QC Batch No: V31761/V31710
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: 1,2,4-Trichlorobenzene QC Batch No: V31761/V31710
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: 2-Hexanone QC Batch No: V31711/V31710
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: 4-Methyl-2-pentanone QC Batch No: V31711/V31710
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Analyte: Acetone QC Batch No: V31711/V31710
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: 1,2-Dibromo-3-chloropropane QC Batch No: V31711/V31710
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Analyte: 1,2-Dibromo-3-chloropropane QC Batch No: V31761/V31710
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable. Analyte: Ethanol QC Batch No: V31711/V31710 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Ethanol QC Batch No: V31761/V31710 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Page 13 of 142

Sample 92533 (MW-8)
QC Batch No: V31761/V31760 Sample originally run within hold. Dilution ran out of hold and confirms data
Sample 92536 (MW-4)
QC Batch No: V31761/V31760 Sample originally run within hold. Dilution ran out of hold and confirms data
Sample 92539 (MW-1)
QC Batch No: V31761/V31760 Sample originally run within hold. Dilution ran out of hold and confirms data
Analyte: 3,3-Dimethyl-1-butanol
QC Batch No: V31711/V31860 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: 3,3-Dimethyl-1-butanol
QC Batch No: V31711/V31860 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: 3,3-Dimethyl-1-butanol QC Batch No: V31761/V31860 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: 3,3-Dimethyl-1-butanol QC Batch No: V31866/V31860 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Analyte: tert-Amyl alcohol
QC Batch No: V31711/V31860 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: tert-Amyl alcohol QC Batch No: V31717/V31860 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Analyte: tert-Butyl alcohol
QC Batch No: V31920/V31860 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Page 14 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:Trip Blank
92521 Matrix:
3/28/2023 8:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 04/05/23 23:51 V31711MSA
<0.180 µg/L 0.180 0.500Benzene 1 04/05/23 23:51 V31711MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 04/05/23 23:51 V31711MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 04/05/23 23:51 V31711MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 04/05/23 23:51 V31711MSA
<1.50 µg/L 1.50 5.00Bromoform 1 04/05/23 23:51 V31711MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 04/05/23 23:51 V31711MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 04/05/23 23:51 V31711MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 04/05/23 23:51 V31711MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 04/05/23 23:51 V31711MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 04/05/23 23:51 V31711MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 04/05/23 23:51 V31711MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 04/05/23 23:51 V31711MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 04/05/23 23:51 V31711MSA
<0.220 µg/L 0.220 0.500Chloroform 1 04/05/23 23:51 V31711MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 04/05/23 23:51 V31711MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 04/05/23 23:51 V31711MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 04/05/23 23:51 V31711MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 04/05/23 23:51 V31711MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 04/05/23 23:51 V31711MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 04/05/23 23:51 V31711MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 04/05/23 23:51 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:Trip Blank
92521 Matrix:
3/28/2023 8:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 04/05/23 23:51 V31711MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 04/05/23 23:51 V31711MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 04/05/23 23:51 V31711MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 04/05/23 23:51 V31711MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 04/05/23 23:51 V31711MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 04/05/23 23:51 V31711MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 04/05/23 23:51 V31711MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 04/05/23 23:51 V31711MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 04/05/23 23:51 V31711MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 04/05/23 23:51 V31711MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 04/05/23 23:51 V31711MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 04/05/23 23:51 V31711MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 04/05/23 23:51 V31711MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 04/05/23 23:51 V31711MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 04/05/23 23:51 V31711MSA
<42.0 µg/L 42.0 200Ethanol 1 04/05/23 23:51 V31711MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 04/05/23 23:51 V31711MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 04/05/23 23:51 V31711MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 04/05/23 23:51 V31711MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 04/05/23 23:51 V31711MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 04/05/23 23:51 V31711MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 04/05/23 23:51 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:Trip Blank
92521 Matrix:
3/28/2023 8:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 04/05/23 23:51 V31711MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 04/05/23 23:51 V31711MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 04/05/23 23:51 V31711MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 04/05/23 23:51 V31711MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 04/05/23 23:51 V31711MSA
<0.220 µg/L 0.220 0.500Styrene 1 04/05/23 23:51 V31711MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 04/05/23 23:51 V31711MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 04/05/23 23:51 V31711MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 04/05/23 23:51 V31711MSA
<0.220 µg/L 0.220 0.500Toluene 1 04/05/23 23:51 V31711MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 04/05/23 23:51 V31711MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 04/05/23 23:51 V31711MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 04/05/23 23:51 V31711MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 04/05/23 23:51 V31711MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 04/05/23 23:51 V31711MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 04/05/23 23:51 V31711MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 04/05/23 23:51 V31711MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 04/05/23 23:51 V31711MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 04/05/23 23:51 V31711MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 04/05/23 23:51 V31711MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 04/05/23 23:51 V31711MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 04/05/23 23:51 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:Trip Blank
92521 Matrix:
3/28/2023 8:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 04/05/23 23:51 V31711MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 04/05/23 23:51 V31711
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%04/05/23 23:511 MSA V31711
Surrogate: Dibromofluoromethane 103 Limits: 70-130%04/05/23 23:511 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 105 Limits: 70-130%04/05/23 23:511 MSA V31711
Surrogate: Toluene-d8 101 Limits: 70-130%04/05/23 23:511 MSA V31711
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:TW-1
92522 Matrix:
3/28/2023 9:42
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 04/10/23 22:52 6200BMSA
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%04/06/23 03:071 MSA V31711
Surrogate: Dibromofluoromethane 101 Limits: 70-130%04/06/23 03:071 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%04/06/23 03:071 MSA V31711
Surrogate: Toluene-d8 100 Limits: 70-130%04/06/23 03:071 MSA V31711
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%04/10/23 22:521 MSA V31866
Surrogate: Dibromofluoromethane 100 Limits: 70-130%04/10/23 22:521 MSA V31866
Surrogate: 1,2-Dichloroethane - d4 98.6 Limits: 70-130%04/10/23 22:521 MSA V31866
Surrogate: Toluene-d8 101 Limits: 70-130%04/10/23 22:521 MSA V31866
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:TW-1
92522 Matrix:
3/28/2023 9:42
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31860 04/10/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 04/10/23 22:52 V31866MSA
<0.180 µg/L 0.180 0.500Benzene 1 04/10/23 22:52 V31866MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 04/10/23 22:52 V31866MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 04/10/23 22:52 V31866MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 04/10/23 22:52 V31866MSA
<1.50 µg/L 1.50 5.00Bromoform 1 04/10/23 22:52 V31866MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 04/10/23 22:52 V31866MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 04/10/23 22:52 V31866MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 04/10/23 22:52 V31866MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 04/10/23 22:52 V31866MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 04/10/23 22:52 V31866MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 04/10/23 22:52 V31866MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 04/10/23 22:52 V31866MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 04/10/23 22:52 V31866MSA
<0.220 µg/L 0.220 0.500Chloroform 1 04/10/23 22:52 V31866MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 04/10/23 22:52 V31866MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 04/10/23 22:52 V31866MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 04/10/23 22:52 V31866MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 04/10/23 22:52 V31866MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 04/10/23 22:52 V31866MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 04/10/23 22:52 V31866MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 04/10/23 22:52 V31866MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:TW-1
92522 Matrix:
3/28/2023 9:42
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31860 04/10/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 04/10/23 22:52 V31866MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 04/10/23 22:52 V31866MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 04/10/23 22:52 V31866MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 04/10/23 22:52 V31866MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 04/10/23 22:52 V31866MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 04/10/23 22:52 V31866MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 04/10/23 22:52 V31866MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 04/10/23 22:52 V31866MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 04/10/23 22:52 V31866MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 04/10/23 22:52 V31866MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 04/10/23 22:52 V31866MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 04/10/23 22:52 V31866MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 04/10/23 22:52 V31866MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 04/10/23 22:52 V31866MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 04/10/23 22:52 V31866MSA
<42.0 µg/L 42.0 200Ethanol 1 04/10/23 22:52 V31866MSA
0.385 J µg/L 0.170 0.500Ethylbenzene 1 04/10/23 22:52 V31866MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 04/10/23 22:52 V31866MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 04/10/23 22:52 V31866MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 04/10/23 22:52 V31866MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 04/10/23 22:52 V31866MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 04/10/23 22:52 V31866MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:TW-1
92522 Matrix:
3/28/2023 9:42
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31860 04/10/23 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 04/10/23 22:52 V31866MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 04/10/23 22:52 V31866MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 04/10/23 22:52 V31866MSA
2.74 µg/L 0.470 1.00Naphthalene 1 04/10/23 22:52 V31866MSA
0.226 J µg/L 0.190 0.500n-Propylbenzene 1 04/10/23 22:52 V31866MSA
<0.220 µg/L 0.220 0.500Styrene 1 04/10/23 22:52 V31866MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 04/10/23 22:52 V31866MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 04/10/23 22:52 V31866MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 04/10/23 22:52 V31866MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 04/10/23 22:52 V31866MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 04/10/23 22:52 V31866MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 04/10/23 22:52 V31866MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 04/10/23 22:52 V31866MSA
0.422 J µg/L 0.220 0.500Toluene 1 04/10/23 22:52 V31866MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 04/10/23 22:52 V31866MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 04/10/23 22:52 V31866MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 04/10/23 22:52 V31866MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 04/10/23 22:52 V31866MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 04/10/23 22:52 V31866MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 04/10/23 22:52 V31866MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 04/10/23 22:52 V31866MSA
3.78 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 04/10/23 22:52 V31866MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:TW-1
92522 Matrix:
3/28/2023 9:42
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31860 04/10/23 09:00
0.920 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 04/10/23 22:52 V31866MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 04/10/23 22:52 V31866MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 04/10/23 22:52 V31866MSA
0.695 µg/L 0.210 0.500o-Xylene 1 04/10/23 22:52 V31866MSA
1.26 µg/L 0.420 1.00m,p-Xylene 1 04/10/23 22:52 V31866MSA
1.96 µg/L 0.210 0.500Xylene (Total)1 04/10/23 22:52 V31866
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%04/06/23 03:071 MSA V31711
Surrogate: Dibromofluoromethane 101 Limits: 70-130%04/06/23 03:071 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%04/06/23 03:071 MSA V31711
Surrogate: Toluene-d8 100 Limits: 70-130%04/06/23 03:071 MSA V31711
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%04/10/23 22:521 MSA V31866
Surrogate: Dibromofluoromethane 100 Limits: 70-130%04/10/23 22:521 MSA V31866
Surrogate: 1,2-Dichloroethane - d4 98.6 Limits: 70-130%04/10/23 22:521 MSA V31866
Surrogate: Toluene-d8 101 Limits: 70-130%04/10/23 22:521 MSA V31866
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-19
92523 Matrix:
3/28/2023 9:57
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0 1003,3-Dimethyl-1-butanol 10 04/06/23 04:20 6200BMSA
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%04/06/23 04:2010 MSA V31711
Surrogate: Dibromofluoromethane 100 Limits: 70-130%04/06/23 04:2010 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%04/06/23 04:2010 MSA V31711
Surrogate: Toluene-d8 99.4 Limits: 70-130%04/06/23 04:2010 MSA V31711
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%04/11/23 00:54100 MSA V31866
Surrogate: Dibromofluoromethane 102 Limits: 70-130%04/11/23 00:54100 MSA V31866
Surrogate: 1,2-Dichloroethane - d4 99.6 Limits: 70-130%04/11/23 00:54100 MSA V31866
Surrogate: Toluene-d8 101 Limits: 70-130%04/11/23 00:54100 MSA V31866
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-19
92523 Matrix:
3/28/2023 9:57
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
<18.0 µg/L 18.0 100Acetone 10 04/06/23 04:20 V31711MSA
255 µg/L 1.80 5.00Benzene 10 04/06/23 04:20 V31711MSA
<2.10 µg/L 2.10 5.00Bromobenzene 10 04/06/23 04:20 V31711MSA
<4.20 µg/L 4.20 10.0Bromochloromethane 10 04/06/23 04:20 V31711MSA
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 04/06/23 04:20 V31711MSA
<15.0 µg/L 15.0 50.0Bromoform 10 04/06/23 04:20 V31711MSA
<2.80 µg/L 2.80 10.0Bromomethane 10 04/06/23 04:20 V31711MSA
18.0 µg/L 1.80 5.00n-Butylbenzene 10 04/06/23 04:20 V31711MSA
9.48 µg/L 2.00 5.00sec-Butyl benzene 10 04/06/23 04:20 V31711MSA
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 04/06/23 04:20 V31711MSA
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 04/06/23 04:20 V31711MSA
<1.90 µg/L 1.90 5.00Chlorobenzene 10 04/06/23 04:20 V31711MSA
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 04/06/23 04:20 V31711MSA
<4.30 µg/L 4.30 10.0Chloroethane 10 04/06/23 04:20 V31711MSA
<2.20 µg/L 2.20 5.00Chloroform 10 04/06/23 04:20 V31711MSA
<2.20 µg/L 2.20 5.00Chloromethane 10 04/06/23 04:20 V31711MSA
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 04/06/23 04:20 V31711MSA
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 04/06/23 04:20 V31711MSA
<5.00 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 04/06/23 04:20 V31711MSA
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 04/06/23 04:20 V31711MSA
<2.00 µg/L 2.00 5.001,2-Dibromoethane 10 04/06/23 04:20 V31711MSA
<2.30 µg/L 2.30 5.00Dibromomethane 10 04/06/23 04:20 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-19
92523 Matrix:
3/28/2023 9:57
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 04/06/23 04:20 V31711MSA
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 04/06/23 04:20 V31711MSA
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 04/06/23 04:20 V31711MSA
<12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 04/06/23 04:20 V31711MSA
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 04/06/23 04:20 V31711MSA
<1.50 µg/L 1.50 5.001,2-Dichloroethane 10 04/06/23 04:20 V31711MSA
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 04/06/23 04:20 V31711MSA
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 04/06/23 04:20 V31711MSA
<1.80 µg/L 1.80 5.00trans-1,2-Dichloroethene 10 04/06/23 04:20 V31711MSA
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 04/06/23 04:20 V31711MSA
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 04/06/23 04:20 V31711MSA
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 04/06/23 04:20 V31711MSA
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 04/06/23 04:20 V31711MSA
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 04/06/23 04:20 V31711MSA
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 04/06/23 04:20 V31711MSA
<420 µg/L 420 2000Ethanol 10 04/06/23 04:20 V31711MSA
978 µg/L 1.70 5.00Ethylbenzene 10 04/06/23 04:20 V31711MSA
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 04/06/23 04:20 V31711MSA
<3.80 µg/L 3.80 10.02-Hexanone 10 04/06/23 04:20 V31711MSA
108 µg/L 1.80 5.00Isopropylbenzene 10 04/06/23 04:20 V31711MSA
9.33 µg/L 0.890 5.004-Isopropyl toluene 10 04/06/23 04:20 V31711MSA
<7.10 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 04/06/23 04:20 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-19
92523 Matrix:
3/28/2023 9:57
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
<1.40 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 04/06/23 04:20 V31711MSA
<0.780 µg/L 0.780 10.04-Methyl-2-Pentanone 10 04/06/23 04:20 V31711MSA
<3.30 µg/L 3.30 20.0Methylene Chloride 10 04/06/23 04:20 V31711MSA
346 µg/L 4.70 10.0Naphthalene 10 04/06/23 04:20 V31711MSA
206 µg/L 1.90 5.00n-Propylbenzene 10 04/06/23 04:20 V31711MSA
<2.20 µg/L 2.20 5.00Styrene 10 04/06/23 04:20 V31711MSA
<16.0 µg/L 16.0 100tert-Butyl Alcohol (TBA)10 04/06/23 04:20 V31711MSA
<3.50 µg/L 3.50 100tert-Butyl formate (TBF)10 04/06/23 04:20 V31711MSA
201 µg/L 19.0 100tert-Amyl Alcohol (TAA)10 04/06/23 04:20 V31711MSA
<2.80 µg/L 2.80 100tert-Amyl Methyl Ether (TAME)10 04/06/23 04:20 V31711MSA
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 04/06/23 04:20 V31711MSA
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 04/06/23 04:20 V31711MSA
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 04/06/23 04:20 V31711MSA
2580 µg/L 22.0 50.0Toluene 100 04/11/23 00:54 V31866MSA
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 04/06/23 04:20 V31711MSA
<3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 04/06/23 04:20 V31711MSA
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 04/06/23 04:20 V31711MSA
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 04/06/23 04:20 V31711MSA
<1.80 µg/L 1.80 5.00Trichloroethene 10 04/06/23 04:20 V31711MSA
<1.80 µg/L 1.80 5.00Trichlorofluoromethane 10 04/06/23 04:20 V31711MSA
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 04/06/23 04:20 V31711MSA
2490 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 04/11/23 00:54 V31866MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-19
92523 Matrix:
3/28/2023 9:57
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
689 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 04/06/23 04:20 V31711MSA
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 04/06/23 04:20 V31711MSA
<1.70 µg/L 1.70 5.00Vinyl Chloride 10 04/06/23 04:20 V31711MSA
523 µg/L 2.10 5.00o-Xylene 10 04/06/23 04:20 V31711MSA
3070 µg/L 42.0 100m,p-Xylene 100 04/11/23 00:54 V31866MSA
3590 µg/L 2.10 5.00Xylene (Total)10 04/06/23 04:20 V31866
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%04/06/23 04:2010 MSA V31711
Surrogate: Dibromofluoromethane 100 Limits: 70-130%04/06/23 04:2010 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%04/06/23 04:2010 MSA V31711
Surrogate: Toluene-d8 99.4 Limits: 70-130%04/06/23 04:2010 MSA V31711
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%04/11/23 00:54100 MSA V31866
Surrogate: Dibromofluoromethane 102 Limits: 70-130%04/11/23 00:54100 MSA V31866
Surrogate: 1,2-Dichloroethane - d4 99.6 Limits: 70-130%04/11/23 00:54100 MSA V31866
Surrogate: Toluene-d8 101 Limits: 70-130%04/11/23 00:54100 MSA V31866
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-18
92524 Matrix:
3/28/2023 10:11
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0 1003,3-Dimethyl-1-butanol 10 04/06/23 04:45 6200BMSA
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%04/06/23 04:4510 MSA V31711
Surrogate: Dibromofluoromethane 99.8 Limits: 70-130%04/06/23 04:4510 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%04/06/23 04:4510 MSA V31711
Surrogate: Toluene-d8 98.2 Limits: 70-130%04/06/23 04:4510 MSA V31711
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%04/11/23 01:18100 MSA V31866
Surrogate: Dibromofluoromethane 101 Limits: 70-130%04/11/23 01:18100 MSA V31866
Surrogate: 1,2-Dichloroethane - d4 97.2 Limits: 70-130%04/11/23 01:18100 MSA V31866
Surrogate: Toluene-d8 101 Limits: 70-130%04/11/23 01:18100 MSA V31866
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-18
92524 Matrix:
3/28/2023 10:11
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
<18.0 µg/L 18.0 100Acetone 10 04/06/23 04:45 V31711MSA
446 µg/L 1.80 5.00Benzene 10 04/06/23 04:45 V31711MSA
<2.10 µg/L 2.10 5.00Bromobenzene 10 04/06/23 04:45 V31711MSA
<4.20 µg/L 4.20 10.0Bromochloromethane 10 04/06/23 04:45 V31711MSA
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 04/06/23 04:45 V31711MSA
<15.0 µg/L 15.0 50.0Bromoform 10 04/06/23 04:45 V31711MSA
<2.80 µg/L 2.80 10.0Bromomethane 10 04/06/23 04:45 V31711MSA
5.75 µg/L 1.80 5.00n-Butylbenzene 10 04/06/23 04:45 V31711MSA
7.70 µg/L 2.00 5.00sec-Butyl benzene 10 04/06/23 04:45 V31711MSA
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 04/06/23 04:45 V31711MSA
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 04/06/23 04:45 V31711MSA
<1.90 µg/L 1.90 5.00Chlorobenzene 10 04/06/23 04:45 V31711MSA
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 04/06/23 04:45 V31711MSA
<4.30 µg/L 4.30 10.0Chloroethane 10 04/06/23 04:45 V31711MSA
<2.20 µg/L 2.20 5.00Chloroform 10 04/06/23 04:45 V31711MSA
<2.20 µg/L 2.20 5.00Chloromethane 10 04/06/23 04:45 V31711MSA
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 04/06/23 04:45 V31711MSA
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 04/06/23 04:45 V31711MSA
<5.00 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 04/06/23 04:45 V31711MSA
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 04/06/23 04:45 V31711MSA
<2.00 µg/L 2.00 5.001,2-Dibromoethane 10 04/06/23 04:45 V31711MSA
<2.30 µg/L 2.30 5.00Dibromomethane 10 04/06/23 04:45 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-18
92524 Matrix:
3/28/2023 10:11
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 04/06/23 04:45 V31711MSA
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 04/06/23 04:45 V31711MSA
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 04/06/23 04:45 V31711MSA
<12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 04/06/23 04:45 V31711MSA
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 04/06/23 04:45 V31711MSA
<1.50 µg/L 1.50 5.001,2-Dichloroethane 10 04/06/23 04:45 V31711MSA
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 04/06/23 04:45 V31711MSA
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 04/06/23 04:45 V31711MSA
<1.80 µg/L 1.80 5.00trans-1,2-Dichloroethene 10 04/06/23 04:45 V31711MSA
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 04/06/23 04:45 V31711MSA
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 04/06/23 04:45 V31711MSA
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 04/06/23 04:45 V31711MSA
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 04/06/23 04:45 V31711MSA
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 04/06/23 04:45 V31711MSA
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 04/06/23 04:45 V31711MSA
<420 µg/L 420 2000Ethanol 10 04/06/23 04:45 V31711MSA
1300 µg/L 17.0 50.0Ethylbenzene 100 04/11/23 01:18 V31866MSA
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 04/06/23 04:45 V31711MSA
<3.80 µg/L 3.80 10.02-Hexanone 10 04/06/23 04:45 V31711MSA
63.5 µg/L 1.80 5.00Isopropylbenzene 10 04/06/23 04:45 V31711MSA
5.05 µg/L 0.890 5.004-Isopropyl toluene 10 04/06/23 04:45 V31711MSA
<7.10 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 04/06/23 04:45 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-18
92524 Matrix:
3/28/2023 10:11
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
53.7 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 04/06/23 04:45 V31711MSA
<0.780 µg/L 0.780 10.04-Methyl-2-Pentanone 10 04/06/23 04:45 V31711MSA
<3.30 µg/L 3.30 20.0Methylene Chloride 10 04/06/23 04:45 V31711MSA
324 µg/L 4.70 10.0Naphthalene 10 04/06/23 04:45 V31711MSA
131 µg/L 1.90 5.00n-Propylbenzene 10 04/06/23 04:45 V31711MSA
3.05 J µg/L 2.20 5.00Styrene 10 04/06/23 04:45 V31711MSA
<16.0 µg/L 16.0 100tert-Butyl Alcohol (TBA)10 04/06/23 04:45 V31711MSA
<3.50 µg/L 3.50 100tert-Butyl formate (TBF)10 04/06/23 04:45 V31711MSA
408 µg/L 19.0 100tert-Amyl Alcohol (TAA)10 04/06/23 04:45 V31711MSA
2.99 J µg/L 2.80 100tert-Amyl Methyl Ether (TAME)10 04/06/23 04:45 V31711MSA
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 04/06/23 04:45 V31711MSA
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 04/06/23 04:45 V31711MSA
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 04/06/23 04:45 V31711MSA
544 µg/L 2.20 5.00Toluene 10 04/06/23 04:45 V31711MSA
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 04/06/23 04:45 V31711MSA
<3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 04/06/23 04:45 V31711MSA
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 04/06/23 04:45 V31711MSA
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 04/06/23 04:45 V31711MSA
<1.80 µg/L 1.80 5.00Trichloroethene 10 04/06/23 04:45 V31711MSA
<1.80 µg/L 1.80 5.00Trichlorofluoromethane 10 04/06/23 04:45 V31711MSA
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 04/06/23 04:45 V31711MSA
942 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 04/06/23 04:45 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-18
92524 Matrix:
3/28/2023 10:11
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
323 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 04/06/23 04:45 V31711MSA
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 04/06/23 04:45 V31711MSA
<1.70 µg/L 1.70 5.00Vinyl Chloride 10 04/06/23 04:45 V31711MSA
32.1 µg/L 2.10 5.00o-Xylene 10 04/06/23 04:45 V31711MSA
3130 µg/L 42.0 100m,p-Xylene 100 04/11/23 01:18 V31866MSA
3160 µg/L 2.10 5.00Xylene (Total)10 04/06/23 04:45 V31866
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%04/06/23 04:4510 MSA V31711
Surrogate: Dibromofluoromethane 99.8 Limits: 70-130%04/06/23 04:4510 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%04/06/23 04:4510 MSA V31711
Surrogate: Toluene-d8 98.2 Limits: 70-130%04/06/23 04:4510 MSA V31711
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%04/11/23 01:18100 MSA V31866
Surrogate: Dibromofluoromethane 101 Limits: 70-130%04/11/23 01:18100 MSA V31866
Surrogate: 1,2-Dichloroethane - d4 97.2 Limits: 70-130%04/11/23 01:18100 MSA V31866
Surrogate: Toluene-d8 101 Limits: 70-130%04/11/23 01:18100 MSA V31866
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-10
92525 Matrix:
3/28/2023 10:23
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 04/06/23 00:40 6200BMSA
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%04/06/23 00:401 MSA V31711
Surrogate: Dibromofluoromethane 100 Limits: 70-130%04/06/23 00:401 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%04/06/23 00:401 MSA V31711
Surrogate: Toluene-d8 99.0 Limits: 70-130%04/06/23 00:401 MSA V31711
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-10
92525 Matrix:
3/28/2023 10:23
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 04/06/23 00:40 V31711MSA
5.95 µg/L 0.180 0.500Benzene 1 04/06/23 00:40 V31711MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 04/06/23 00:40 V31711MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 04/06/23 00:40 V31711MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 04/06/23 00:40 V31711MSA
<1.50 µg/L 1.50 5.00Bromoform 1 04/06/23 00:40 V31711MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 04/06/23 00:40 V31711MSA
3.07 µg/L 0.180 0.500n-Butylbenzene 1 04/06/23 00:40 V31711MSA
1.95 µg/L 0.200 0.500sec-Butyl benzene 1 04/06/23 00:40 V31711MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 04/06/23 00:40 V31711MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 04/06/23 00:40 V31711MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 04/06/23 00:40 V31711MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 04/06/23 00:40 V31711MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 04/06/23 00:40 V31711MSA
<0.220 µg/L 0.220 0.500Chloroform 1 04/06/23 00:40 V31711MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 04/06/23 00:40 V31711MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 04/06/23 00:40 V31711MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 04/06/23 00:40 V31711MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 04/06/23 00:40 V31711MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 04/06/23 00:40 V31711MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 04/06/23 00:40 V31711MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 04/06/23 00:40 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-10
92525 Matrix:
3/28/2023 10:23
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 04/06/23 00:40 V31711MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 04/06/23 00:40 V31711MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 04/06/23 00:40 V31711MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 04/06/23 00:40 V31711MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 04/06/23 00:40 V31711MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 04/06/23 00:40 V31711MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 04/06/23 00:40 V31711MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 04/06/23 00:40 V31711MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 04/06/23 00:40 V31711MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 04/06/23 00:40 V31711MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 04/06/23 00:40 V31711MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 04/06/23 00:40 V31711MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 04/06/23 00:40 V31711MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 04/06/23 00:40 V31711MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 04/06/23 00:40 V31711MSA
<42.0 µg/L 42.0 200Ethanol 1 04/06/23 00:40 V31711MSA
68.1 µg/L 0.170 0.500Ethylbenzene 1 04/06/23 00:40 V31711MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 04/06/23 00:40 V31711MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 04/06/23 00:40 V31711MSA
8.97 µg/L 0.180 0.500Isopropylbenzene 1 04/06/23 00:40 V31711MSA
1.26 µg/L 0.089 0.5004-Isopropyl toluene 1 04/06/23 00:40 V31711MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 04/06/23 00:40 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-10
92525 Matrix:
3/28/2023 10:23
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00
0.358 J µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 04/06/23 00:40 V31711MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 04/06/23 00:40 V31711MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 04/06/23 00:40 V31711MSA
58.6 µg/L 0.470 1.00Naphthalene 1 04/06/23 00:40 V31711MSA
30.0 µg/L 0.190 0.500n-Propylbenzene 1 04/06/23 00:40 V31711MSA
<0.220 µg/L 0.220 0.500Styrene 1 04/06/23 00:40 V31711MSA
2.87 J µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 04/06/23 00:40 V31711MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 04/06/23 00:40 V31711MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 04/06/23 00:40 V31711MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 04/06/23 00:40 V31711MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 04/06/23 00:40 V31711MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 04/06/23 00:40 V31711MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 04/06/23 00:40 V31711MSA
0.731 µg/L 0.220 0.500Toluene 1 04/06/23 00:40 V31711MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 04/06/23 00:40 V31711MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 04/06/23 00:40 V31711MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 04/06/23 00:40 V31711MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 04/06/23 00:40 V31711MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 04/06/23 00:40 V31711MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 04/06/23 00:40 V31711MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 04/06/23 00:40 V31711MSA
54.9 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 04/06/23 00:40 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-10
92525 Matrix:
3/28/2023 10:23
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00
52.0 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 04/06/23 00:40 V31711MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 04/06/23 00:40 V31711MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 04/06/23 00:40 V31711MSA
3.37 µg/L 0.210 0.500o-Xylene 1 04/06/23 00:40 V31711MSA
15.1 µg/L 0.420 1.00m,p-Xylene 1 04/06/23 00:40 V31711MSA
18.5 µg/L 0.210 0.500Xylene (Total)1 04/06/23 00:40 V31711
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%04/06/23 00:401 MSA V31711
Surrogate: Dibromofluoromethane 100 Limits: 70-130%04/06/23 00:401 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%04/06/23 00:401 MSA V31711
Surrogate: Toluene-d8 99.0 Limits: 70-130%04/06/23 00:401 MSA V31711
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-11
92526 Matrix:
3/28/2023 10:35
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0 1003,3-Dimethyl-1-butanol 10 04/06/23 05:09 6200BMSA
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%04/06/23 05:0910 MSA V31711
Surrogate: Dibromofluoromethane 101 Limits: 70-130%04/06/23 05:0910 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%04/06/23 05:0910 MSA V31711
Surrogate: Toluene-d8 98.8 Limits: 70-130%04/06/23 05:0910 MSA V31711
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%04/11/23 01:43100 MSA V31866
Surrogate: Dibromofluoromethane 102 Limits: 70-130%04/11/23 01:43100 MSA V31866
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%04/11/23 01:43100 MSA V31866
Surrogate: Toluene-d8 101 Limits: 70-130%04/11/23 01:43100 MSA V31866
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-11
92526 Matrix:
3/28/2023 10:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
<18.0 µg/L 18.0 100Acetone 10 04/06/23 05:09 V31711MSA
<1.80 µg/L 1.80 5.00Benzene 10 04/06/23 05:09 V31711MSA
<2.10 µg/L 2.10 5.00Bromobenzene 10 04/06/23 05:09 V31711MSA
<4.20 µg/L 4.20 10.0Bromochloromethane 10 04/06/23 05:09 V31711MSA
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 04/06/23 05:09 V31711MSA
<15.0 µg/L 15.0 50.0Bromoform 10 04/06/23 05:09 V31711MSA
<2.80 µg/L 2.80 10.0Bromomethane 10 04/06/23 05:09 V31711MSA
7.00 µg/L 1.80 5.00n-Butylbenzene 10 04/06/23 05:09 V31711MSA
5.18 µg/L 2.00 5.00sec-Butyl benzene 10 04/06/23 05:09 V31711MSA
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 04/06/23 05:09 V31711MSA
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 04/06/23 05:09 V31711MSA
<1.90 µg/L 1.90 5.00Chlorobenzene 10 04/06/23 05:09 V31711MSA
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 04/06/23 05:09 V31711MSA
<4.30 µg/L 4.30 10.0Chloroethane 10 04/06/23 05:09 V31711MSA
<2.20 µg/L 2.20 5.00Chloroform 10 04/06/23 05:09 V31711MSA
<2.20 µg/L 2.20 5.00Chloromethane 10 04/06/23 05:09 V31711MSA
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 04/06/23 05:09 V31711MSA
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 04/06/23 05:09 V31711MSA
<5.00 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 04/06/23 05:09 V31711MSA
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 04/06/23 05:09 V31711MSA
<2.00 µg/L 2.00 5.001,2-Dibromoethane 10 04/06/23 05:09 V31711MSA
<2.30 µg/L 2.30 5.00Dibromomethane 10 04/06/23 05:09 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-11
92526 Matrix:
3/28/2023 10:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 04/06/23 05:09 V31711MSA
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 04/06/23 05:09 V31711MSA
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 04/06/23 05:09 V31711MSA
<12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 04/06/23 05:09 V31711MSA
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 04/06/23 05:09 V31711MSA
<1.50 µg/L 1.50 5.001,2-Dichloroethane 10 04/06/23 05:09 V31711MSA
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 04/06/23 05:09 V31711MSA
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 04/06/23 05:09 V31711MSA
<1.80 µg/L 1.80 5.00trans-1,2-Dichloroethene 10 04/06/23 05:09 V31711MSA
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 04/06/23 05:09 V31711MSA
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 04/06/23 05:09 V31711MSA
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 04/06/23 05:09 V31711MSA
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 04/06/23 05:09 V31711MSA
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 04/06/23 05:09 V31711MSA
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 04/06/23 05:09 V31711MSA
<420 µg/L 420 2000Ethanol 10 04/06/23 05:09 V31711MSA
1750 µg/L 17.0 50.0Ethylbenzene 100 04/11/23 01:43 V31866MSA
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 04/06/23 05:09 V31711MSA
<3.80 µg/L 3.80 10.02-Hexanone 10 04/06/23 05:09 V31711MSA
89.0 µg/L 1.80 5.00Isopropylbenzene 10 04/06/23 05:09 V31711MSA
5.38 µg/L 0.890 5.004-Isopropyl toluene 10 04/06/23 05:09 V31711MSA
<7.10 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 04/06/23 05:09 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-11
92526 Matrix:
3/28/2023 10:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
<1.40 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 04/06/23 05:09 V31711MSA
<0.780 µg/L 0.780 10.04-Methyl-2-Pentanone 10 04/06/23 05:09 V31711MSA
<3.30 µg/L 3.30 20.0Methylene Chloride 10 04/06/23 05:09 V31711MSA
424 µg/L 4.70 10.0Naphthalene 10 04/06/23 05:09 V31711MSA
177 µg/L 1.90 5.00n-Propylbenzene 10 04/06/23 05:09 V31711MSA
<2.20 µg/L 2.20 5.00Styrene 10 04/06/23 05:09 V31711MSA
<16.0 µg/L 16.0 100tert-Butyl Alcohol (TBA)10 04/06/23 05:09 V31711MSA
<3.50 µg/L 3.50 100tert-Butyl formate (TBF)10 04/06/23 05:09 V31711MSA
<19.0 µg/L 19.0 100tert-Amyl Alcohol (TAA)10 04/06/23 05:09 V31711MSA
<2.80 µg/L 2.80 100tert-Amyl Methyl Ether (TAME)10 04/06/23 05:09 V31711MSA
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 04/06/23 05:09 V31711MSA
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 04/06/23 05:09 V31711MSA
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 04/06/23 05:09 V31711MSA
63.3 µg/L 2.20 5.00Toluene 10 04/06/23 05:09 V31711MSA
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 04/06/23 05:09 V31711MSA
<3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 04/06/23 05:09 V31711MSA
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 04/06/23 05:09 V31711MSA
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 04/06/23 05:09 V31711MSA
<1.80 µg/L 1.80 5.00Trichloroethene 10 04/06/23 05:09 V31711MSA
<1.80 µg/L 1.80 5.00Trichlorofluoromethane 10 04/06/23 05:09 V31711MSA
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 04/06/23 05:09 V31711MSA
1390 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 04/11/23 01:43 V31866MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 42 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-11
92526 Matrix:
3/28/2023 10:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
446 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 04/06/23 05:09 V31711MSA
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 04/06/23 05:09 V31711MSA
<1.70 µg/L 1.70 5.00Vinyl Chloride 10 04/06/23 05:09 V31711MSA
997 µg/L 21.0 50.0o-Xylene 100 04/11/23 01:43 V31866MSA
3030 µg/L 42.0 100m,p-Xylene 100 04/11/23 01:43 V31866MSA
4030 µg/L 21.0 50.0Xylene (Total)100 04/11/23 01:43 V31866
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%04/06/23 05:0910 MSA V31711
Surrogate: Dibromofluoromethane 101 Limits: 70-130%04/06/23 05:0910 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%04/06/23 05:0910 MSA V31711
Surrogate: Toluene-d8 98.8 Limits: 70-130%04/06/23 05:0910 MSA V31711
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%04/11/23 01:43100 MSA V31866
Surrogate: Dibromofluoromethane 102 Limits: 70-130%04/11/23 01:43100 MSA V31866
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%04/11/23 01:43100 MSA V31866
Surrogate: Toluene-d8 101 Limits: 70-130%04/11/23 01:43100 MSA V31866
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-17
92527 Matrix:
3/28/2023 10:46
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 04/06/23 01:05 6200BMSA
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%04/06/23 01:051 MSA V31711
Surrogate: Dibromofluoromethane 100 Limits: 70-130%04/06/23 01:051 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%04/06/23 01:051 MSA V31711
Surrogate: Toluene-d8 99.4 Limits: 70-130%04/06/23 01:051 MSA V31711
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-17
92527 Matrix:
3/28/2023 10:46
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 04/06/23 01:05 V31711MSA
0.514 µg/L 0.180 0.500Benzene 1 04/06/23 01:05 V31711MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 04/06/23 01:05 V31711MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 04/06/23 01:05 V31711MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 04/06/23 01:05 V31711MSA
<1.50 µg/L 1.50 5.00Bromoform 1 04/06/23 01:05 V31711MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 04/06/23 01:05 V31711MSA
4.41 µg/L 0.180 0.500n-Butylbenzene 1 04/06/23 01:05 V31711MSA
3.64 µg/L 0.200 0.500sec-Butyl benzene 1 04/06/23 01:05 V31711MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 04/06/23 01:05 V31711MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 04/06/23 01:05 V31711MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 04/06/23 01:05 V31711MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 04/06/23 01:05 V31711MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 04/06/23 01:05 V31711MSA
<0.220 µg/L 0.220 0.500Chloroform 1 04/06/23 01:05 V31711MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 04/06/23 01:05 V31711MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 04/06/23 01:05 V31711MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 04/06/23 01:05 V31711MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 04/06/23 01:05 V31711MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 04/06/23 01:05 V31711MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 04/06/23 01:05 V31711MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 04/06/23 01:05 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 45 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-17
92527 Matrix:
3/28/2023 10:46
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 04/06/23 01:05 V31711MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 04/06/23 01:05 V31711MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 04/06/23 01:05 V31711MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 04/06/23 01:05 V31711MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 04/06/23 01:05 V31711MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 04/06/23 01:05 V31711MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 04/06/23 01:05 V31711MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 04/06/23 01:05 V31711MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 04/06/23 01:05 V31711MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 04/06/23 01:05 V31711MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 04/06/23 01:05 V31711MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 04/06/23 01:05 V31711MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 04/06/23 01:05 V31711MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 04/06/23 01:05 V31711MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 04/06/23 01:05 V31711MSA
<42.0 µg/L 42.0 200Ethanol 1 04/06/23 01:05 V31711MSA
30.0 µg/L 0.170 0.500Ethylbenzene 1 04/06/23 01:05 V31711MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 04/06/23 01:05 V31711MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 04/06/23 01:05 V31711MSA
11.2 µg/L 0.180 0.500Isopropylbenzene 1 04/06/23 01:05 V31711MSA
2.63 µg/L 0.089 0.5004-Isopropyl toluene 1 04/06/23 01:05 V31711MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 04/06/23 01:05 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 46 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-17
92527 Matrix:
3/28/2023 10:46
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 04/06/23 01:05 V31711MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 04/06/23 01:05 V31711MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 04/06/23 01:05 V31711MSA
51.0 µg/L 0.470 1.00Naphthalene 1 04/06/23 01:05 V31711MSA
34.0 µg/L 0.190 0.500n-Propylbenzene 1 04/06/23 01:05 V31711MSA
<0.220 µg/L 0.220 0.500Styrene 1 04/06/23 01:05 V31711MSA
2.46 J µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 04/06/23 01:05 V31711MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 04/06/23 01:05 V31711MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 04/06/23 01:05 V31711MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 04/06/23 01:05 V31711MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 04/06/23 01:05 V31711MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 04/06/23 01:05 V31711MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 04/06/23 01:05 V31711MSA
<0.220 µg/L 0.220 0.500Toluene 1 04/06/23 01:05 V31711MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 04/06/23 01:05 V31711MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 04/06/23 01:05 V31711MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 04/06/23 01:05 V31711MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 04/06/23 01:05 V31711MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 04/06/23 01:05 V31711MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 04/06/23 01:05 V31711MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 04/06/23 01:05 V31711MSA
14.7 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 04/06/23 01:05 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 47 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-17
92527 Matrix:
3/28/2023 10:46
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00
4.77 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 04/06/23 01:05 V31711MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 04/06/23 01:05 V31711MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 04/06/23 01:05 V31711MSA
1.42 µg/L 0.210 0.500o-Xylene 1 04/06/23 01:05 V31711MSA
2.60 µg/L 0.420 1.00m,p-Xylene 1 04/06/23 01:05 V31711MSA
4.02 µg/L 0.210 0.500Xylene (Total)1 04/06/23 01:05 V31711
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%04/06/23 01:051 MSA V31711
Surrogate: Dibromofluoromethane 100 Limits: 70-130%04/06/23 01:051 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%04/06/23 01:051 MSA V31711
Surrogate: Toluene-d8 99.4 Limits: 70-130%04/06/23 01:051 MSA V31711
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 48 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-16
92528 Matrix:
3/28/2023 10:58
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 04/06/23 01:29 6200BMSA
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%04/06/23 01:291 MSA V31711
Surrogate: Dibromofluoromethane 103 Limits: 70-130%04/06/23 01:291 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%04/06/23 01:291 MSA V31711
Surrogate: Toluene-d8 99.2 Limits: 70-130%04/06/23 01:291 MSA V31711
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 49 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-16
92528 Matrix:
3/28/2023 10:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 04/06/23 01:29 V31711MSA
<0.180 µg/L 0.180 0.500Benzene 1 04/06/23 01:29 V31711MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 04/06/23 01:29 V31711MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 04/06/23 01:29 V31711MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 04/06/23 01:29 V31711MSA
<1.50 µg/L 1.50 5.00Bromoform 1 04/06/23 01:29 V31711MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 04/06/23 01:29 V31711MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 04/06/23 01:29 V31711MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 04/06/23 01:29 V31711MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 04/06/23 01:29 V31711MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 04/06/23 01:29 V31711MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 04/06/23 01:29 V31711MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 04/06/23 01:29 V31711MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 04/06/23 01:29 V31711MSA
<0.220 µg/L 0.220 0.500Chloroform 1 04/06/23 01:29 V31711MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 04/06/23 01:29 V31711MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 04/06/23 01:29 V31711MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 04/06/23 01:29 V31711MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 04/06/23 01:29 V31711MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 04/06/23 01:29 V31711MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 04/06/23 01:29 V31711MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 04/06/23 01:29 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 50 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-16
92528 Matrix:
3/28/2023 10:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 04/06/23 01:29 V31711MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 04/06/23 01:29 V31711MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 04/06/23 01:29 V31711MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 04/06/23 01:29 V31711MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 04/06/23 01:29 V31711MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 04/06/23 01:29 V31711MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 04/06/23 01:29 V31711MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 04/06/23 01:29 V31711MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 04/06/23 01:29 V31711MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 04/06/23 01:29 V31711MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 04/06/23 01:29 V31711MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 04/06/23 01:29 V31711MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 04/06/23 01:29 V31711MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 04/06/23 01:29 V31711MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 04/06/23 01:29 V31711MSA
<42.0 µg/L 42.0 200Ethanol 1 04/06/23 01:29 V31711MSA
0.726 µg/L 0.170 0.500Ethylbenzene 1 04/06/23 01:29 V31711MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 04/06/23 01:29 V31711MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 04/06/23 01:29 V31711MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 04/06/23 01:29 V31711MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 04/06/23 01:29 V31711MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 04/06/23 01:29 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 51 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-16
92528 Matrix:
3/28/2023 10:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00
0.216 J µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 04/06/23 01:29 V31711MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 04/06/23 01:29 V31711MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 04/06/23 01:29 V31711MSA
2.62 µg/L 0.470 1.00Naphthalene 1 04/06/23 01:29 V31711MSA
0.245 J µg/L 0.190 0.500n-Propylbenzene 1 04/06/23 01:29 V31711MSA
<0.220 µg/L 0.220 0.500Styrene 1 04/06/23 01:29 V31711MSA
2.70 J µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 04/06/23 01:29 V31711MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 04/06/23 01:29 V31711MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 04/06/23 01:29 V31711MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 04/06/23 01:29 V31711MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 04/06/23 01:29 V31711MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 04/06/23 01:29 V31711MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 04/06/23 01:29 V31711MSA
<0.220 µg/L 0.220 0.500Toluene 1 04/06/23 01:29 V31711MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 04/06/23 01:29 V31711MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 04/06/23 01:29 V31711MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 04/06/23 01:29 V31711MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 04/06/23 01:29 V31711MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 04/06/23 01:29 V31711MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 04/06/23 01:29 V31711MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 04/06/23 01:29 V31711MSA
0.717 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 04/06/23 01:29 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 52 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-16
92528 Matrix:
3/28/2023 10:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00
0.271 J µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 04/06/23 01:29 V31711MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 04/06/23 01:29 V31711MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 04/06/23 01:29 V31711MSA
0.323 J µg/L 0.210 0.500o-Xylene 1 04/06/23 01:29 V31711MSA
1.15 µg/L 0.420 1.00m,p-Xylene 1 04/06/23 01:29 V31711MSA
1.47 J µg/L 0.210 0.500Xylene (Total)1 04/06/23 01:29 V31711
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%04/06/23 01:291 MSA V31711
Surrogate: Dibromofluoromethane 103 Limits: 70-130%04/06/23 01:291 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%04/06/23 01:291 MSA V31711
Surrogate: Toluene-d8 99.2 Limits: 70-130%04/06/23 01:291 MSA V31711
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 53 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-15
92529 Matrix:
3/28/2023 11:10
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 04/06/23 01:54 6200BMSA
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%04/06/23 01:541 MSA V31711
Surrogate: Dibromofluoromethane 101 Limits: 70-130%04/06/23 01:541 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%04/06/23 01:541 MSA V31711
Surrogate: Toluene-d8 98.2 Limits: 70-130%04/06/23 01:541 MSA V31711
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 54 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-15
92529 Matrix:
3/28/2023 11:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 04/06/23 01:54 V31711MSA
<0.180 µg/L 0.180 0.500Benzene 1 04/06/23 01:54 V31711MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 04/06/23 01:54 V31711MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 04/06/23 01:54 V31711MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 04/06/23 01:54 V31711MSA
<1.50 µg/L 1.50 5.00Bromoform 1 04/06/23 01:54 V31711MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 04/06/23 01:54 V31711MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 04/06/23 01:54 V31711MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 04/06/23 01:54 V31711MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 04/06/23 01:54 V31711MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 04/06/23 01:54 V31711MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 04/06/23 01:54 V31711MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 04/06/23 01:54 V31711MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 04/06/23 01:54 V31711MSA
<0.220 µg/L 0.220 0.500Chloroform 1 04/06/23 01:54 V31711MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 04/06/23 01:54 V31711MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 04/06/23 01:54 V31711MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 04/06/23 01:54 V31711MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 04/06/23 01:54 V31711MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 04/06/23 01:54 V31711MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 04/06/23 01:54 V31711MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 04/06/23 01:54 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 55 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-15
92529 Matrix:
3/28/2023 11:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 04/06/23 01:54 V31711MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 04/06/23 01:54 V31711MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 04/06/23 01:54 V31711MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 04/06/23 01:54 V31711MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 04/06/23 01:54 V31711MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 04/06/23 01:54 V31711MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 04/06/23 01:54 V31711MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 04/06/23 01:54 V31711MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 04/06/23 01:54 V31711MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 04/06/23 01:54 V31711MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 04/06/23 01:54 V31711MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 04/06/23 01:54 V31711MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 04/06/23 01:54 V31711MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 04/06/23 01:54 V31711MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 04/06/23 01:54 V31711MSA
<42.0 µg/L 42.0 200Ethanol 1 04/06/23 01:54 V31711MSA
0.529 µg/L 0.170 0.500Ethylbenzene 1 04/06/23 01:54 V31711MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 04/06/23 01:54 V31711MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 04/06/23 01:54 V31711MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 04/06/23 01:54 V31711MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 04/06/23 01:54 V31711MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 04/06/23 01:54 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 56 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-15
92529 Matrix:
3/28/2023 11:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 04/06/23 01:54 V31711MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 04/06/23 01:54 V31711MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 04/06/23 01:54 V31711MSA
1.19 µg/L 0.470 1.00Naphthalene 1 04/06/23 01:54 V31711MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 04/06/23 01:54 V31711MSA
<0.220 µg/L 0.220 0.500Styrene 1 04/06/23 01:54 V31711MSA
9.94 J µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 04/06/23 01:54 V31711MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 04/06/23 01:54 V31711MSA
7.07 J µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 04/06/23 01:54 V31711MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 04/06/23 01:54 V31711MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 04/06/23 01:54 V31711MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 04/06/23 01:54 V31711MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 04/06/23 01:54 V31711MSA
<0.220 µg/L 0.220 0.500Toluene 1 04/06/23 01:54 V31711MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 04/06/23 01:54 V31711MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 04/06/23 01:54 V31711MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 04/06/23 01:54 V31711MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 04/06/23 01:54 V31711MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 04/06/23 01:54 V31711MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 04/06/23 01:54 V31711MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 04/06/23 01:54 V31711MSA
0.630 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 04/06/23 01:54 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 57 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-15
92529 Matrix:
3/28/2023 11:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 04/06/23 01:54 V31711MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 04/06/23 01:54 V31711MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 04/06/23 01:54 V31711MSA
0.264 J µg/L 0.210 0.500o-Xylene 1 04/06/23 01:54 V31711MSA
0.902 J µg/L 0.420 1.00m,p-Xylene 1 04/06/23 01:54 V31711MSA
1.17 J µg/L 0.210 0.500Xylene (Total)1 04/06/23 01:54 V31711
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%04/06/23 01:541 MSA V31711
Surrogate: Dibromofluoromethane 101 Limits: 70-130%04/06/23 01:541 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%04/06/23 01:541 MSA V31711
Surrogate: Toluene-d8 98.2 Limits: 70-130%04/06/23 01:541 MSA V31711
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 58 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-14
92530 Matrix:
3/28/2023 11:21
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0 1003,3-Dimethyl-1-butanol 10 04/06/23 05:34 6200BMSA
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%04/06/23 05:3410 MSA V31711
Surrogate: Dibromofluoromethane 100 Limits: 70-130%04/06/23 05:3410 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%04/06/23 05:3410 MSA V31711
Surrogate: Toluene-d8 97.8 Limits: 70-130%04/06/23 05:3410 MSA V31711
Surrogate: 4-Bromofluorobenzene 99.0 Limits: 70-130%04/11/23 02:07100 MSA V31866
Surrogate: Dibromofluoromethane 100 Limits: 70-130%04/11/23 02:07100 MSA V31866
Surrogate: 1,2-Dichloroethane - d4 97.8 Limits: 70-130%04/11/23 02:07100 MSA V31866
Surrogate: Toluene-d8 101 Limits: 70-130%04/11/23 02:07100 MSA V31866
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 59 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-14
92530 Matrix:
3/28/2023 11:21
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
<18.0 µg/L 18.0 100Acetone 10 04/06/23 05:34 V31711MSA
593 µg/L 1.80 5.00Benzene 10 04/06/23 05:34 V31711MSA
<2.10 µg/L 2.10 5.00Bromobenzene 10 04/06/23 05:34 V31711MSA
<4.20 µg/L 4.20 10.0Bromochloromethane 10 04/06/23 05:34 V31711MSA
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 04/06/23 05:34 V31711MSA
<15.0 µg/L 15.0 50.0Bromoform 10 04/06/23 05:34 V31711MSA
<2.80 µg/L 2.80 10.0Bromomethane 10 04/06/23 05:34 V31711MSA
23.9 µg/L 1.80 5.00n-Butylbenzene 10 04/06/23 05:34 V31711MSA
14.0 µg/L 2.00 5.00sec-Butyl benzene 10 04/06/23 05:34 V31711MSA
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 04/06/23 05:34 V31711MSA
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 04/06/23 05:34 V31711MSA
<1.90 µg/L 1.90 5.00Chlorobenzene 10 04/06/23 05:34 V31711MSA
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 04/06/23 05:34 V31711MSA
<4.30 µg/L 4.30 10.0Chloroethane 10 04/06/23 05:34 V31711MSA
<2.20 µg/L 2.20 5.00Chloroform 10 04/06/23 05:34 V31711MSA
<2.20 µg/L 2.20 5.00Chloromethane 10 04/06/23 05:34 V31711MSA
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 04/06/23 05:34 V31711MSA
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 04/06/23 05:34 V31711MSA
<5.00 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 04/06/23 05:34 V31711MSA
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 04/06/23 05:34 V31711MSA
<2.00 µg/L 2.00 5.001,2-Dibromoethane 10 04/06/23 05:34 V31711MSA
<2.30 µg/L 2.30 5.00Dibromomethane 10 04/06/23 05:34 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 60 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-14
92530 Matrix:
3/28/2023 11:21
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 04/06/23 05:34 V31711MSA
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 04/06/23 05:34 V31711MSA
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 04/06/23 05:34 V31711MSA
<12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 04/06/23 05:34 V31711MSA
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 04/06/23 05:34 V31711MSA
<1.50 µg/L 1.50 5.001,2-Dichloroethane 10 04/06/23 05:34 V31711MSA
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 04/06/23 05:34 V31711MSA
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 04/06/23 05:34 V31711MSA
<1.80 µg/L 1.80 5.00trans-1,2-Dichloroethene 10 04/06/23 05:34 V31711MSA
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 04/06/23 05:34 V31711MSA
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 04/06/23 05:34 V31711MSA
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 04/06/23 05:34 V31711MSA
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 04/06/23 05:34 V31711MSA
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 04/06/23 05:34 V31711MSA
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 04/06/23 05:34 V31711MSA
<420 µg/L 420 2000Ethanol 10 04/06/23 05:34 V31711MSA
1410 µg/L 17.0 50.0Ethylbenzene 100 04/11/23 02:07 V31866MSA
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 04/06/23 05:34 V31711MSA
<3.80 µg/L 3.80 10.02-Hexanone 10 04/06/23 05:34 V31711MSA
84.4 µg/L 1.80 5.00Isopropylbenzene 10 04/06/23 05:34 V31711MSA
9.56 µg/L 0.890 5.004-Isopropyl toluene 10 04/06/23 05:34 V31711MSA
<7.10 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 04/06/23 05:34 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 61 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-14
92530 Matrix:
3/28/2023 11:21
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
76.5 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 04/06/23 05:34 V31711MSA
<0.780 µg/L 0.780 10.04-Methyl-2-Pentanone 10 04/06/23 05:34 V31711MSA
<3.30 µg/L 3.30 20.0Methylene Chloride 10 04/06/23 05:34 V31711MSA
862 µg/L 4.70 10.0Naphthalene 10 04/06/23 05:34 V31711MSA
279 µg/L 1.90 5.00n-Propylbenzene 10 04/06/23 05:34 V31711MSA
10.1 µg/L 2.20 5.00Styrene 10 04/06/23 05:34 V31711MSA
<16.0 µg/L 16.0 100tert-Butyl Alcohol (TBA)10 04/06/23 05:34 V31711MSA
<3.50 µg/L 3.50 100tert-Butyl formate (TBF)10 04/06/23 05:34 V31711MSA
367 µg/L 19.0 100tert-Amyl Alcohol (TAA)10 04/06/23 05:34 V31711MSA
<2.80 µg/L 2.80 100tert-Amyl Methyl Ether (TAME)10 04/06/23 05:34 V31711MSA
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 04/06/23 05:34 V31711MSA
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 04/06/23 05:34 V31711MSA
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 04/06/23 05:34 V31711MSA
1680 µg/L 22.0 50.0Toluene 100 04/11/23 02:07 V31866MSA
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 04/06/23 05:34 V31711MSA
<3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 04/06/23 05:34 V31711MSA
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 04/06/23 05:34 V31711MSA
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 04/06/23 05:34 V31711MSA
<1.80 µg/L 1.80 5.00Trichloroethene 10 04/06/23 05:34 V31711MSA
<1.80 µg/L 1.80 5.00Trichlorofluoromethane 10 04/06/23 05:34 V31711MSA
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 04/06/23 05:34 V31711MSA
2190 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 04/11/23 02:07 V31866MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 62 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-14
92530 Matrix:
3/28/2023 11:21
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
612 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 04/06/23 05:34 V31711MSA
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 04/06/23 05:34 V31711MSA
<1.70 µg/L 1.70 5.00Vinyl Chloride 10 04/06/23 05:34 V31711MSA
1560 µg/L 21.0 50.0o-Xylene 100 04/11/23 02:07 V31866MSA
3280 µg/L 42.0 100m,p-Xylene 100 04/11/23 02:07 V31866MSA
4840 µg/L 21.0 50.0Xylene (Total)100 04/11/23 02:07 V31866
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%04/06/23 05:3410 MSA V31711
Surrogate: Dibromofluoromethane 100 Limits: 70-130%04/06/23 05:3410 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%04/06/23 05:3410 MSA V31711
Surrogate: Toluene-d8 97.8 Limits: 70-130%04/06/23 05:3410 MSA V31711
Surrogate: 4-Bromofluorobenzene 99.0 Limits: 70-130%04/11/23 02:07100 MSA V31866
Surrogate: Dibromofluoromethane 100 Limits: 70-130%04/11/23 02:07100 MSA V31866
Surrogate: 1,2-Dichloroethane - d4 97.8 Limits: 70-130%04/11/23 02:07100 MSA V31866
Surrogate: Toluene-d8 101 Limits: 70-130%04/11/23 02:07100 MSA V31866
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 63 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-12
92531 Matrix:
3/28/2023 11:33
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0 1003,3-Dimethyl-1-butanol 10 04/06/23 05:58 6200BMSA
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%04/06/23 05:5810 MSA V31711
Surrogate: Dibromofluoromethane 101 Limits: 70-130%04/06/23 05:5810 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%04/06/23 05:5810 MSA V31711
Surrogate: Toluene-d8 98.2 Limits: 70-130%04/06/23 05:5810 MSA V31711
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%04/11/23 02:31100 MSA V31866
Surrogate: Dibromofluoromethane 102 Limits: 70-130%04/11/23 02:31100 MSA V31866
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%04/11/23 02:31100 MSA V31866
Surrogate: Toluene-d8 101 Limits: 70-130%04/11/23 02:31100 MSA V31866
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 64 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-12
92531 Matrix:
3/28/2023 11:33
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
<18.0 µg/L 18.0 100Acetone 10 04/06/23 05:58 V31711MSA
967 µg/L 1.80 5.00Benzene 10 04/06/23 05:58 V31711MSA
<2.10 µg/L 2.10 5.00Bromobenzene 10 04/06/23 05:58 V31711MSA
<4.20 µg/L 4.20 10.0Bromochloromethane 10 04/06/23 05:58 V31711MSA
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 04/06/23 05:58 V31711MSA
<15.0 µg/L 15.0 50.0Bromoform 10 04/06/23 05:58 V31711MSA
<2.80 µg/L 2.80 10.0Bromomethane 10 04/06/23 05:58 V31711MSA
21.2 µg/L 1.80 5.00n-Butylbenzene 10 04/06/23 05:58 V31711MSA
3.46 J µg/L 2.00 5.00sec-Butyl benzene 10 04/06/23 05:58 V31711MSA
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 04/06/23 05:58 V31711MSA
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 04/06/23 05:58 V31711MSA
<1.90 µg/L 1.90 5.00Chlorobenzene 10 04/06/23 05:58 V31711MSA
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 04/06/23 05:58 V31711MSA
<4.30 µg/L 4.30 10.0Chloroethane 10 04/06/23 05:58 V31711MSA
<2.20 µg/L 2.20 5.00Chloroform 10 04/06/23 05:58 V31711MSA
<2.20 µg/L 2.20 5.00Chloromethane 10 04/06/23 05:58 V31711MSA
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 04/06/23 05:58 V31711MSA
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 04/06/23 05:58 V31711MSA
<5.00 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 04/06/23 05:58 V31711MSA
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 04/06/23 05:58 V31711MSA
<2.00 µg/L 2.00 5.001,2-Dibromoethane 10 04/06/23 05:58 V31711MSA
<2.30 µg/L 2.30 5.00Dibromomethane 10 04/06/23 05:58 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 65 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-12
92531 Matrix:
3/28/2023 11:33
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 04/06/23 05:58 V31711MSA
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 04/06/23 05:58 V31711MSA
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 04/06/23 05:58 V31711MSA
<12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 04/06/23 05:58 V31711MSA
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 04/06/23 05:58 V31711MSA
<1.50 µg/L 1.50 5.001,2-Dichloroethane 10 04/06/23 05:58 V31711MSA
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 04/06/23 05:58 V31711MSA
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 04/06/23 05:58 V31711MSA
<1.80 µg/L 1.80 5.00trans-1,2-Dichloroethene 10 04/06/23 05:58 V31711MSA
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 04/06/23 05:58 V31711MSA
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 04/06/23 05:58 V31711MSA
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 04/06/23 05:58 V31711MSA
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 04/06/23 05:58 V31711MSA
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 04/06/23 05:58 V31711MSA
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 04/06/23 05:58 V31711MSA
<420 µg/L 420 2000Ethanol 10 04/06/23 05:58 V31711MSA
702 µg/L 1.70 5.00Ethylbenzene 10 04/06/23 05:58 V31711MSA
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 04/06/23 05:58 V31711MSA
43.6 µg/L 3.80 10.02-Hexanone 10 04/06/23 05:58 V31711MSA
21.8 µg/L 1.80 5.00Isopropylbenzene 10 04/06/23 05:58 V31711MSA
<0.890 µg/L 0.890 5.004-Isopropyl toluene 10 04/06/23 05:58 V31711MSA
37.5 J µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 04/06/23 05:58 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 66 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-12
92531 Matrix:
3/28/2023 11:33
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
323 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 04/06/23 05:58 V31711MSA
17.8 µg/L 0.780 10.04-Methyl-2-Pentanone 10 04/06/23 05:58 V31711MSA
<3.30 µg/L 3.30 20.0Methylene Chloride 10 04/06/23 05:58 V31711MSA
393 µg/L 4.70 10.0Naphthalene 10 04/06/23 05:58 V31711MSA
46.1 µg/L 1.90 5.00n-Propylbenzene 10 04/06/23 05:58 V31711MSA
8.26 µg/L 2.20 5.00Styrene 10 04/06/23 05:58 V31711MSA
856 µg/L 16.0 100tert-Butyl Alcohol (TBA)10 04/06/23 05:58 V31711MSA
<3.50 µg/L 3.50 100tert-Butyl formate (TBF)10 04/06/23 05:58 V31711MSA
2210 µg/L 190 1000tert-Amyl Alcohol (TAA)100 04/11/23 02:31 V31866MSA
49.9 J µg/L 2.80 100tert-Amyl Methyl Ether (TAME)10 04/06/23 05:58 V31711MSA
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 04/06/23 05:58 V31711MSA
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 04/06/23 05:58 V31711MSA
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 04/06/23 05:58 V31711MSA
2070 µg/L 22.0 50.0Toluene 100 04/11/23 02:31 V31866MSA
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 04/06/23 05:58 V31711MSA
<3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 04/06/23 05:58 V31711MSA
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 04/06/23 05:58 V31711MSA
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 04/06/23 05:58 V31711MSA
<1.80 µg/L 1.80 5.00Trichloroethene 10 04/06/23 05:58 V31711MSA
<1.80 µg/L 1.80 5.00Trichlorofluoromethane 10 04/06/23 05:58 V31711MSA
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 04/06/23 05:58 V31711MSA
818 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 04/06/23 05:58 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 67 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-12
92531 Matrix:
3/28/2023 11:33
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
248 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 04/06/23 05:58 V31711MSA
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 04/06/23 05:58 V31711MSA
<1.70 µg/L 1.70 5.00Vinyl Chloride 10 04/06/23 05:58 V31711MSA
1400 µg/L 21.0 50.0o-Xylene 100 04/11/23 02:31 V31866MSA
2630 µg/L 42.0 100m,p-Xylene 100 04/11/23 02:31 V31866MSA
4030 µg/L 21.0 50.0Xylene (Total)100 04/11/23 02:31 V31866
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%04/06/23 05:5810 MSA V31711
Surrogate: Dibromofluoromethane 101 Limits: 70-130%04/06/23 05:5810 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%04/06/23 05:5810 MSA V31711
Surrogate: Toluene-d8 98.2 Limits: 70-130%04/06/23 05:5810 MSA V31711
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%04/11/23 02:31100 MSA V31866
Surrogate: Dibromofluoromethane 102 Limits: 70-130%04/11/23 02:31100 MSA V31866
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%04/11/23 02:31100 MSA V31866
Surrogate: Toluene-d8 101 Limits: 70-130%04/11/23 02:31100 MSA V31866
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 68 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-9
92532 Matrix:
3/28/2023 11:45
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0 1003,3-Dimethyl-1-butanol 10 04/06/23 06:23 6200BMSA
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%04/06/23 06:2310 MSA V31711
Surrogate: Dibromofluoromethane 98.6 Limits: 70-130%04/06/23 06:2310 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%04/06/23 06:2310 MSA V31711
Surrogate: Toluene-d8 98.2 Limits: 70-130%04/06/23 06:2310 MSA V31711
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%04/11/23 02:56100 MSA V31866
Surrogate: Dibromofluoromethane 100 Limits: 70-130%04/11/23 02:56100 MSA V31866
Surrogate: 1,2-Dichloroethane - d4 99.2 Limits: 70-130%04/11/23 02:56100 MSA V31866
Surrogate: Toluene-d8 102 Limits: 70-130%04/11/23 02:56100 MSA V31866
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 69 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-9
92532 Matrix:
3/28/2023 11:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
<18.0 µg/L 18.0 100Acetone 10 04/06/23 06:23 V31711MSA
1190 µg/L 18.0 50.0Benzene 100 04/11/23 02:56 V31866MSA
<2.10 µg/L 2.10 5.00Bromobenzene 10 04/06/23 06:23 V31711MSA
<4.20 µg/L 4.20 10.0Bromochloromethane 10 04/06/23 06:23 V31711MSA
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 04/06/23 06:23 V31711MSA
<15.0 µg/L 15.0 50.0Bromoform 10 04/06/23 06:23 V31711MSA
<2.80 µg/L 2.80 10.0Bromomethane 10 04/06/23 06:23 V31711MSA
10.5 µg/L 1.80 5.00n-Butylbenzene 10 04/06/23 06:23 V31711MSA
4.66 J µg/L 2.00 5.00sec-Butyl benzene 10 04/06/23 06:23 V31711MSA
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 04/06/23 06:23 V31711MSA
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 04/06/23 06:23 V31711MSA
<1.90 µg/L 1.90 5.00Chlorobenzene 10 04/06/23 06:23 V31711MSA
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 04/06/23 06:23 V31711MSA
<4.30 µg/L 4.30 10.0Chloroethane 10 04/06/23 06:23 V31711MSA
<2.20 µg/L 2.20 5.00Chloroform 10 04/06/23 06:23 V31711MSA
<2.20 µg/L 2.20 5.00Chloromethane 10 04/06/23 06:23 V31711MSA
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 04/06/23 06:23 V31711MSA
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 04/06/23 06:23 V31711MSA
<5.00 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 04/06/23 06:23 V31711MSA
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 04/06/23 06:23 V31711MSA
<2.00 µg/L 2.00 5.001,2-Dibromoethane 10 04/06/23 06:23 V31711MSA
<2.30 µg/L 2.30 5.00Dibromomethane 10 04/06/23 06:23 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 70 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-9
92532 Matrix:
3/28/2023 11:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 04/06/23 06:23 V31711MSA
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 04/06/23 06:23 V31711MSA
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 04/06/23 06:23 V31711MSA
<12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 04/06/23 06:23 V31711MSA
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 04/06/23 06:23 V31711MSA
<1.50 µg/L 1.50 5.001,2-Dichloroethane 10 04/06/23 06:23 V31711MSA
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 04/06/23 06:23 V31711MSA
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 04/06/23 06:23 V31711MSA
<1.80 µg/L 1.80 5.00trans-1,2-Dichloroethene 10 04/06/23 06:23 V31711MSA
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 04/06/23 06:23 V31711MSA
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 04/06/23 06:23 V31711MSA
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 04/06/23 06:23 V31711MSA
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 04/06/23 06:23 V31711MSA
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 04/06/23 06:23 V31711MSA
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 04/06/23 06:23 V31711MSA
<420 µg/L 420 2000Ethanol 10 04/06/23 06:23 V31711MSA
877 µg/L 1.70 5.00Ethylbenzene 10 04/06/23 06:23 V31711MSA
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 04/06/23 06:23 V31711MSA
3.80 J µg/L 3.80 10.02-Hexanone 10 04/06/23 06:23 V31711MSA
30.9 µg/L 1.80 5.00Isopropylbenzene 10 04/06/23 06:23 V31711MSA
2.76 J µg/L 0.890 5.004-Isopropyl toluene 10 04/06/23 06:23 V31711MSA
<7.10 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 04/06/23 06:23 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 71 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-9
92532 Matrix:
3/28/2023 11:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
20.9 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 04/06/23 06:23 V31711MSA
8.40 J µg/L 0.780 10.04-Methyl-2-Pentanone 10 04/06/23 06:23 V31711MSA
<3.30 µg/L 3.30 20.0Methylene Chloride 10 04/06/23 06:23 V31711MSA
482 µg/L 4.70 10.0Naphthalene 10 04/06/23 06:23 V31711MSA
76.6 µg/L 1.90 5.00n-Propylbenzene 10 04/06/23 06:23 V31711MSA
9.73 µg/L 2.20 5.00Styrene 10 04/06/23 06:23 V31711MSA
<16.0 µg/L 16.0 100tert-Butyl Alcohol (TBA)10 04/06/23 06:23 V31711MSA
<3.50 µg/L 3.50 100tert-Butyl formate (TBF)10 04/06/23 06:23 V31711MSA
669 µg/L 19.0 100tert-Amyl Alcohol (TAA)10 04/06/23 06:23 V31711MSA
<2.80 µg/L 2.80 100tert-Amyl Methyl Ether (TAME)10 04/06/23 06:23 V31711MSA
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 04/06/23 06:23 V31711MSA
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 04/06/23 06:23 V31711MSA
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 04/06/23 06:23 V31711MSA
3530 µg/L 22.0 50.0Toluene 100 04/11/23 02:56 V31866MSA
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 04/06/23 06:23 V31711MSA
<3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 04/06/23 06:23 V31711MSA
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 04/06/23 06:23 V31711MSA
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 04/06/23 06:23 V31711MSA
<1.80 µg/L 1.80 5.00Trichloroethene 10 04/06/23 06:23 V31711MSA
<1.80 µg/L 1.80 5.00Trichlorofluoromethane 10 04/06/23 06:23 V31711MSA
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 04/06/23 06:23 V31711MSA
948 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 04/06/23 06:23 V31711MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 72 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-9
92532 Matrix:
3/28/2023 11:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31710 04/05/23 09:00 V31860 04/10/23 09:00
269 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 04/06/23 06:23 V31711MSA
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 04/06/23 06:23 V31711MSA
<1.70 µg/L 1.70 5.00Vinyl Chloride 10 04/06/23 06:23 V31711MSA
1450 µg/L 21.0 50.0o-Xylene 100 04/11/23 02:56 V31866MSA
2990 µg/L 42.0 100m,p-Xylene 100 04/11/23 02:56 V31866MSA
4440 µg/L 21.0 50.0Xylene (Total)100 04/11/23 02:56 V31866
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%04/06/23 06:2310 MSA V31711
Surrogate: Dibromofluoromethane 98.6 Limits: 70-130%04/06/23 06:2310 MSA V31711
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%04/06/23 06:2310 MSA V31711
Surrogate: Toluene-d8 98.2 Limits: 70-130%04/06/23 06:2310 MSA V31711
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%04/11/23 02:56100 MSA V31866
Surrogate: Dibromofluoromethane 100 Limits: 70-130%04/11/23 02:56100 MSA V31866
Surrogate: 1,2-Dichloroethane - d4 99.2 Limits: 70-130%04/11/23 02:56100 MSA V31866
Surrogate: Toluene-d8 102 Limits: 70-130%04/11/23 02:56100 MSA V31866
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 73 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-8
92533 Matrix:
3/28/2023 11:57
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 04/06/23 19:30 6200BMSA
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%04/06/23 19:30100 MSA V31761
Surrogate: Dibromofluoromethane 100 Limits: 70-130%04/06/23 19:30100 MSA V31761
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%04/06/23 19:30100 MSA V31761
Surrogate: Toluene-d8 99.2 Limits: 70-130%04/06/23 19:30100 MSA V31761
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 74 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-8
92533 Matrix:
3/28/2023 11:57
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31760 04/06/23 09:00
<180 µg/L 180 1000Acetone 100 04/06/23 19:30 V31761MSA
581 µg/L 18.0 50.0Benzene 100 04/06/23 19:30 V31761MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 04/06/23 19:30 V31761MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 04/06/23 19:30 V31761MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 04/06/23 19:30 V31761MSA
<150 µg/L 150 500Bromoform 100 04/06/23 19:30 V31761MSA
<28.0 µg/L 28.0 100Bromomethane 100 04/06/23 19:30 V31761MSA
<18.0 µg/L 18.0 50.0n-Butylbenzene 100 04/06/23 19:30 V31761MSA
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 04/06/23 19:30 V31761MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 04/06/23 19:30 V31761MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 04/06/23 19:30 V31761MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 04/06/23 19:30 V31761MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 04/06/23 19:30 V31761MSA
<43.0 µg/L 43.0 100Chloroethane 100 04/06/23 19:30 V31761MSA
<22.0 µg/L 22.0 50.0Chloroform 100 04/06/23 19:30 V31761MSA
<22.0 µg/L 22.0 50.0Chloromethane 100 04/06/23 19:30 V31761MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 04/06/23 19:30 V31761MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 04/06/23 19:30 V31761MSA
<50.0 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 04/06/23 19:30 V31761MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 04/06/23 19:30 V31761MSA
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 04/06/23 19:30 V31761MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 04/06/23 19:30 V31761MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 75 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-8
92533 Matrix:
3/28/2023 11:57
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31760 04/06/23 09:00
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 04/06/23 19:30 V31761MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 04/06/23 19:30 V31761MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 04/06/23 19:30 V31761MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 04/06/23 19:30 V31761MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 04/06/23 19:30 V31761MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 04/06/23 19:30 V31761MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 04/06/23 19:30 V31761MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 04/06/23 19:30 V31761MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 04/06/23 19:30 V31761MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 04/06/23 19:30 V31761MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 04/06/23 19:30 V31761MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 04/06/23 19:30 V31761MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 04/06/23 19:30 V31761MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 04/06/23 19:30 V31761MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 04/06/23 19:30 V31761MSA
<4200 µg/L 4200 20000Ethanol 100 04/06/23 19:30 V31761MSA
1830 µg/L 17.0 50.0Ethylbenzene 100 04/06/23 19:30 V31761MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 04/06/23 19:30 V31761MSA
<38.0 µg/L 38.0 1002-Hexanone 100 04/06/23 19:30 V31761MSA
69.5 µg/L 18.0 50.0Isopropylbenzene 100 04/06/23 19:30 V31761MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 04/06/23 19:30 V31761MSA
186 J µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 04/06/23 19:30 V31761MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 76 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-8
92533 Matrix:
3/28/2023 11:57
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31760 04/06/23 09:00
<14.0 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 04/06/23 19:30 V31761MSA
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 04/06/23 19:30 V31761MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 04/06/23 19:30 V31761MSA
1080 µg/L 47.0 100Naphthalene 100 04/06/23 19:30 V31761MSA
174 µg/L 19.0 50.0n-Propylbenzene 100 04/06/23 19:30 V31761MSA
<22.0 µg/L 22.0 50.0Styrene 100 04/06/23 19:30 V31761MSA
<160 µg/L 160 1000tert-Butyl Alcohol (TBA)100 04/06/23 19:30 V31761MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 04/06/23 19:30 V31761MSA
<190 µg/L 190 1000tert-Amyl Alcohol (TAA)100 04/06/23 19:30 V31761MSA
<28.0 µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 04/06/23 19:30 V31761MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 04/06/23 19:30 V31761MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 04/06/23 19:30 V31761MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 04/06/23 19:30 V31761MSA
409 µg/L 22.0 50.0Toluene 100 04/06/23 19:30 V31761MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 04/06/23 19:30 V31761MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 04/06/23 19:30 V31761MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 04/06/23 19:30 V31761MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 04/06/23 19:30 V31761MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 04/06/23 19:30 V31761MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 04/06/23 19:30 V31761MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 04/06/23 19:30 V31761MSA
2700 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 04/06/23 19:30 V31761MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 77 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-8
92533 Matrix:
3/28/2023 11:57
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31760 04/06/23 09:00
725 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 04/06/23 19:30 V31761MSA
<100 µg/L 100 500Vinyl Acetate 100 04/06/23 19:30 V31761MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 04/06/23 19:30 V31761MSA
388 µg/L 21.0 50.0o-Xylene 100 04/06/23 19:30 V31761MSA
3740 µg/L 42.0 100m,p-Xylene 100 04/06/23 19:30 V31761MSA
4130 µg/L 21.0 50.0Xylene (Total)100 04/06/23 19:30 V31761
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%04/06/23 19:30100 MSA V31761
Surrogate: Dibromofluoromethane 100 Limits: 70-130%04/06/23 19:30100 MSA V31761
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%04/06/23 19:30100 MSA V31761
Surrogate: Toluene-d8 99.2 Limits: 70-130%04/06/23 19:30100 MSA V31761
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 78 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-7
92534 Matrix:
3/28/2023 12:08
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0 1003,3-Dimethyl-1-butanol 10 04/06/23 06:19 6200BMSA
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%04/06/23 06:1910 MSA V31717
Surrogate: Dibromofluoromethane 96.6 Limits: 70-130%04/06/23 06:1910 MSA V31717
Surrogate: 1,2-Dichloroethane - d4 94.2 Limits: 70-130%04/06/23 06:1910 MSA V31717
Surrogate: Toluene-d8 98.0 Limits: 70-130%04/06/23 06:1910 MSA V31717
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%04/11/23 04:09100 MSA V31866
Surrogate: Dibromofluoromethane 102 Limits: 70-130%04/11/23 04:09100 MSA V31866
Surrogate: 1,2-Dichloroethane - d4 98.6 Limits: 70-130%04/11/23 04:09100 MSA V31866
Surrogate: Toluene-d8 101 Limits: 70-130%04/11/23 04:09100 MSA V31866
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 79 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-7
92534 Matrix:
3/28/2023 12:08
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31715 04/05/23 09:00 V31860 04/10/23 09:00
<18.0 µg/L 18.0 100Acetone 10 04/06/23 06:19 V31717MSA
950 µg/L 1.80 5.00Benzene 10 04/06/23 06:19 V31717MSA
<2.10 µg/L 2.10 5.00Bromobenzene 10 04/06/23 06:19 V31717MSA
<4.20 µg/L 4.20 10.0Bromochloromethane 10 04/06/23 06:19 V31717MSA
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 04/06/23 06:19 V31717MSA
<15.0 µg/L 15.0 50.0Bromoform 10 04/06/23 06:19 V31717MSA
<2.80 µg/L 2.80 10.0Bromomethane 10 04/06/23 06:19 V31717MSA
16.2 µg/L 1.80 5.00n-Butylbenzene 10 04/06/23 06:19 V31717MSA
9.10 µg/L 2.00 5.00sec-Butyl benzene 10 04/06/23 06:19 V31717MSA
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 04/06/23 06:19 V31717MSA
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 04/06/23 06:19 V31717MSA
<1.90 µg/L 1.90 5.00Chlorobenzene 10 04/06/23 06:19 V31717MSA
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 04/06/23 06:19 V31717MSA
<4.30 µg/L 4.30 10.0Chloroethane 10 04/06/23 06:19 V31717MSA
<2.20 µg/L 2.20 5.00Chloroform 10 04/06/23 06:19 V31717MSA
<2.20 µg/L 2.20 5.00Chloromethane 10 04/06/23 06:19 V31717MSA
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 04/06/23 06:19 V31717MSA
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 04/06/23 06:19 V31717MSA
8.70 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 04/06/23 06:19 V31717MSA
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 04/06/23 06:19 V31717MSA
<2.00 µg/L 2.00 5.001,2-Dibromoethane 10 04/06/23 06:19 V31717MSA
<2.30 µg/L 2.30 5.00Dibromomethane 10 04/06/23 06:19 V31717MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 80 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-7
92534 Matrix:
3/28/2023 12:08
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31715 04/05/23 09:00 V31860 04/10/23 09:00
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 04/06/23 06:19 V31717MSA
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 04/06/23 06:19 V31717MSA
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 04/06/23 06:19 V31717MSA
<12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 04/06/23 06:19 V31717MSA
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 04/06/23 06:19 V31717MSA
<1.50 µg/L 1.50 5.001,2-Dichloroethane 10 04/06/23 06:19 V31717MSA
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 04/06/23 06:19 V31717MSA
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 04/06/23 06:19 V31717MSA
<1.80 µg/L 1.80 5.00trans-1,2-Dichloroethene 10 04/06/23 06:19 V31717MSA
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 04/06/23 06:19 V31717MSA
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 04/06/23 06:19 V31717MSA
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 04/06/23 06:19 V31717MSA
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 04/06/23 06:19 V31717MSA
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 04/06/23 06:19 V31717MSA
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 04/06/23 06:19 V31717MSA
<420 µg/L 420 2000Ethanol 10 04/06/23 06:19 V31717MSA
1040 µg/L 17.0 50.0Ethylbenzene 100 04/11/23 04:09 V31866MSA
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 04/06/23 06:19 V31717MSA
<3.80 µg/L 3.80 10.02-Hexanone 10 04/06/23 06:19 V31717MSA
46.8 µg/L 1.80 5.00Isopropylbenzene 10 04/06/23 06:19 V31717MSA
3.47 J µg/L 0.890 5.004-Isopropyl toluene 10 04/06/23 06:19 V31717MSA
<7.10 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 04/06/23 06:19 V31717MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 81 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-7
92534 Matrix:
3/28/2023 12:08
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31715 04/05/23 09:00 V31860 04/10/23 09:00
273 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 04/06/23 06:19 V31717MSA
<0.780 µg/L 0.780 10.04-Methyl-2-Pentanone 10 04/06/23 06:19 V31717MSA
<3.30 µg/L 3.30 20.0Methylene Chloride 10 04/06/23 06:19 V31717MSA
482 µg/L 4.70 10.0Naphthalene 10 04/06/23 06:19 V31717MSA
132 µg/L 1.90 5.00n-Propylbenzene 10 04/06/23 06:19 V31717MSA
3.62 J µg/L 2.20 5.00Styrene 10 04/06/23 06:19 V31717MSA
45.3 J µg/L 16.0 100tert-Butyl Alcohol (TBA)10 04/06/23 06:19 V31717MSA
<3.50 µg/L 3.50 100tert-Butyl formate (TBF)10 04/06/23 06:19 V31717MSA
282 µg/L 19.0 100tert-Amyl Alcohol (TAA)10 04/06/23 06:19 V31717MSA
19.7 J µg/L 2.80 100tert-Amyl Methyl Ether (TAME)10 04/06/23 06:19 V31717MSA
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 04/06/23 06:19 V31717MSA
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 04/06/23 06:19 V31717MSA
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 04/06/23 06:19 V31717MSA
563 µg/L 2.20 5.00Toluene 10 04/06/23 06:19 V31717MSA
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 04/06/23 06:19 V31717MSA
<3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 04/06/23 06:19 V31717MSA
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 04/06/23 06:19 V31717MSA
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 04/06/23 06:19 V31717MSA
<1.80 µg/L 1.80 5.00Trichloroethene 10 04/06/23 06:19 V31717MSA
<1.80 µg/L 1.80 5.00Trichlorofluoromethane 10 04/06/23 06:19 V31717MSA
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 04/06/23 06:19 V31717MSA
739 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 04/06/23 06:19 V31717MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 82 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-7
92534 Matrix:
3/28/2023 12:08
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31715 04/05/23 09:00 V31860 04/10/23 09:00
179 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 04/06/23 06:19 V31717MSA
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 04/06/23 06:19 V31717MSA
<1.70 µg/L 1.70 5.00Vinyl Chloride 10 04/06/23 06:19 V31717MSA
248 µg/L 2.10 5.00o-Xylene 10 04/06/23 06:19 V31717MSA
1780 µg/L 4.20 10.0m,p-Xylene 10 04/06/23 06:19 V31717MSA
2030 µg/L 2.10 5.00Xylene (Total)10 04/06/23 06:19 V31717
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%04/06/23 06:1910 MSA V31717
Surrogate: Dibromofluoromethane 96.6 Limits: 70-130%04/06/23 06:1910 MSA V31717
Surrogate: 1,2-Dichloroethane - d4 94.2 Limits: 70-130%04/06/23 06:1910 MSA V31717
Surrogate: Toluene-d8 98.0 Limits: 70-130%04/06/23 06:1910 MSA V31717
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%04/11/23 04:09100 MSA V31866
Surrogate: Dibromofluoromethane 102 Limits: 70-130%04/11/23 04:09100 MSA V31866
Surrogate: 1,2-Dichloroethane - d4 98.6 Limits: 70-130%04/11/23 04:09100 MSA V31866
Surrogate: Toluene-d8 101 Limits: 70-130%04/11/23 04:09100 MSA V31866
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 83 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-6
92535 Matrix:
3/28/2023 12:22
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 04/06/23 01:47 6200BMSA
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%04/06/23 01:471 MSA V31717
Surrogate: Dibromofluoromethane 97.8 Limits: 70-130%04/06/23 01:471 MSA V31717
Surrogate: 1,2-Dichloroethane - d4 92.6 Limits: 70-130%04/06/23 01:471 MSA V31717
Surrogate: Toluene-d8 97.8 Limits: 70-130%04/06/23 01:471 MSA V31717
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 84 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-6
92535 Matrix:
3/28/2023 12:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31715 04/05/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 04/06/23 01:47 V31717MSA
0.591 µg/L 0.180 0.500Benzene 1 04/06/23 01:47 V31717MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 04/06/23 01:47 V31717MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 04/06/23 01:47 V31717MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 04/06/23 01:47 V31717MSA
<1.50 µg/L 1.50 5.00Bromoform 1 04/06/23 01:47 V31717MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 04/06/23 01:47 V31717MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 04/06/23 01:47 V31717MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 04/06/23 01:47 V31717MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 04/06/23 01:47 V31717MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 04/06/23 01:47 V31717MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 04/06/23 01:47 V31717MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 04/06/23 01:47 V31717MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 04/06/23 01:47 V31717MSA
<0.220 µg/L 0.220 0.500Chloroform 1 04/06/23 01:47 V31717MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 04/06/23 01:47 V31717MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 04/06/23 01:47 V31717MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 04/06/23 01:47 V31717MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 04/06/23 01:47 V31717MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 04/06/23 01:47 V31717MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 04/06/23 01:47 V31717MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 04/06/23 01:47 V31717MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 85 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-6
92535 Matrix:
3/28/2023 12:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31715 04/05/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 04/06/23 01:47 V31717MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 04/06/23 01:47 V31717MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 04/06/23 01:47 V31717MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 04/06/23 01:47 V31717MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 04/06/23 01:47 V31717MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 04/06/23 01:47 V31717MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 04/06/23 01:47 V31717MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 04/06/23 01:47 V31717MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 04/06/23 01:47 V31717MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 04/06/23 01:47 V31717MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 04/06/23 01:47 V31717MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 04/06/23 01:47 V31717MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 04/06/23 01:47 V31717MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 04/06/23 01:47 V31717MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 04/06/23 01:47 V31717MSA
<42.0 µg/L 42.0 200Ethanol 1 04/06/23 01:47 V31717MSA
2.46 µg/L 0.170 0.500Ethylbenzene 1 04/06/23 01:47 V31717MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 04/06/23 01:47 V31717MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 04/06/23 01:47 V31717MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 04/06/23 01:47 V31717MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 04/06/23 01:47 V31717MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 04/06/23 01:47 V31717MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 86 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-6
92535 Matrix:
3/28/2023 12:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31715 04/05/23 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 04/06/23 01:47 V31717MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 04/06/23 01:47 V31717MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 04/06/23 01:47 V31717MSA
8.19 µg/L 0.470 1.00Naphthalene 1 04/06/23 01:47 V31717MSA
0.543 µg/L 0.190 0.500n-Propylbenzene 1 04/06/23 01:47 V31717MSA
<0.220 µg/L 0.220 0.500Styrene 1 04/06/23 01:47 V31717MSA
4.97 J µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 04/06/23 01:47 V31717MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 04/06/23 01:47 V31717MSA
2.35 J µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 04/06/23 01:47 V31717MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 04/06/23 01:47 V31717MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 04/06/23 01:47 V31717MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 04/06/23 01:47 V31717MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 04/06/23 01:47 V31717MSA
1.06 µg/L 0.220 0.500Toluene 1 04/06/23 01:47 V31717MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 04/06/23 01:47 V31717MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 04/06/23 01:47 V31717MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 04/06/23 01:47 V31717MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 04/06/23 01:47 V31717MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 04/06/23 01:47 V31717MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 04/06/23 01:47 V31717MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 04/06/23 01:47 V31717MSA
7.47 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 04/06/23 01:47 V31717MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 87 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-6
92535 Matrix:
3/28/2023 12:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31715 04/05/23 09:00
1.97 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 04/06/23 01:47 V31717MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 04/06/23 01:47 V31717MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 04/06/23 01:47 V31717MSA
1.10 µg/L 0.210 0.500o-Xylene 1 04/06/23 01:47 V31717MSA
5.36 µg/L 0.420 1.00m,p-Xylene 1 04/06/23 01:47 V31717MSA
6.46 µg/L 0.210 0.500Xylene (Total)1 04/06/23 01:47 V31717
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%04/06/23 01:471 MSA V31717
Surrogate: Dibromofluoromethane 97.8 Limits: 70-130%04/06/23 01:471 MSA V31717
Surrogate: 1,2-Dichloroethane - d4 92.6 Limits: 70-130%04/06/23 01:471 MSA V31717
Surrogate: Toluene-d8 97.8 Limits: 70-130%04/06/23 01:471 MSA V31717
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 88 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-4
92536 Matrix:
3/28/2023 12:36
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 04/06/23 19:55 6200BMSA
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%04/06/23 19:55100 MSA V31761
Surrogate: Dibromofluoromethane 101 Limits: 70-130%04/06/23 19:55100 MSA V31761
Surrogate: 1,2-Dichloroethane - d4 107 Limits: 70-130%04/06/23 19:55100 MSA V31761
Surrogate: Toluene-d8 99.4 Limits: 70-130%04/06/23 19:55100 MSA V31761
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 89 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-4
92536 Matrix:
3/28/2023 12:36
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31760 04/06/23 09:00
<180 µg/L 180 1000Acetone 100 04/06/23 19:55 V31761MSA
884 µg/L 18.0 50.0Benzene 100 04/06/23 19:55 V31761MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 04/06/23 19:55 V31761MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 04/06/23 19:55 V31761MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 04/06/23 19:55 V31761MSA
<150 µg/L 150 500Bromoform 100 04/06/23 19:55 V31761MSA
<28.0 µg/L 28.0 100Bromomethane 100 04/06/23 19:55 V31761MSA
63.1 µg/L 18.0 50.0n-Butylbenzene 100 04/06/23 19:55 V31761MSA
27.3 J µg/L 20.0 50.0sec-Butyl benzene 100 04/06/23 19:55 V31761MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 04/06/23 19:55 V31761MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 04/06/23 19:55 V31761MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 04/06/23 19:55 V31761MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 04/06/23 19:55 V31761MSA
<43.0 µg/L 43.0 100Chloroethane 100 04/06/23 19:55 V31761MSA
<22.0 µg/L 22.0 50.0Chloroform 100 04/06/23 19:55 V31761MSA
<22.0 µg/L 22.0 50.0Chloromethane 100 04/06/23 19:55 V31761MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 04/06/23 19:55 V31761MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 04/06/23 19:55 V31761MSA
<50.0 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 04/06/23 19:55 V31761MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 04/06/23 19:55 V31761MSA
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 04/06/23 19:55 V31761MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 04/06/23 19:55 V31761MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 90 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-4
92536 Matrix:
3/28/2023 12:36
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31760 04/06/23 09:00
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 04/06/23 19:55 V31761MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 04/06/23 19:55 V31761MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 04/06/23 19:55 V31761MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 04/06/23 19:55 V31761MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 04/06/23 19:55 V31761MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 04/06/23 19:55 V31761MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 04/06/23 19:55 V31761MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 04/06/23 19:55 V31761MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 04/06/23 19:55 V31761MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 04/06/23 19:55 V31761MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 04/06/23 19:55 V31761MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 04/06/23 19:55 V31761MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 04/06/23 19:55 V31761MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 04/06/23 19:55 V31761MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 04/06/23 19:55 V31761MSA
<4200 µg/L 4200 20000Ethanol 100 04/06/23 19:55 V31761MSA
1560 µg/L 17.0 50.0Ethylbenzene 100 04/06/23 19:55 V31761MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 04/06/23 19:55 V31761MSA
99.6 J µg/L 38.0 1002-Hexanone 100 04/06/23 19:55 V31761MSA
112 µg/L 18.0 50.0Isopropylbenzene 100 04/06/23 19:55 V31761MSA
22.1 J µg/L 8.90 50.04-Isopropyl toluene 100 04/06/23 19:55 V31761MSA
<71.0 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 04/06/23 19:55 V31761MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 91 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-4
92536 Matrix:
3/28/2023 12:36
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31760 04/06/23 09:00
265 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 04/06/23 19:55 V31761MSA
63.2 J µg/L 7.80 1004-Methyl-2-Pentanone 100 04/06/23 19:55 V31761MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 04/06/23 19:55 V31761MSA
1540 µg/L 47.0 100Naphthalene 100 04/06/23 19:55 V31761MSA
359 µg/L 19.0 50.0n-Propylbenzene 100 04/06/23 19:55 V31761MSA
<22.0 µg/L 22.0 50.0Styrene 100 04/06/23 19:55 V31761MSA
<160 µg/L 160 1000tert-Butyl Alcohol (TBA)100 04/06/23 19:55 V31761MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 04/06/23 19:55 V31761MSA
2090 µg/L 190 1000tert-Amyl Alcohol (TAA)100 04/06/23 19:55 V31761MSA
64.0 J µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 04/06/23 19:55 V31761MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 04/06/23 19:55 V31761MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 04/06/23 19:55 V31761MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 04/06/23 19:55 V31761MSA
94.7 µg/L 22.0 50.0Toluene 100 04/06/23 19:55 V31761MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 04/06/23 19:55 V31761MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 04/06/23 19:55 V31761MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 04/06/23 19:55 V31761MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 04/06/23 19:55 V31761MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 04/06/23 19:55 V31761MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 04/06/23 19:55 V31761MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 04/06/23 19:55 V31761MSA
2880 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 04/06/23 19:55 V31761MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 92 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-4
92536 Matrix:
3/28/2023 12:36
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31760 04/06/23 09:00
811 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 04/06/23 19:55 V31761MSA
<100 µg/L 100 500Vinyl Acetate 100 04/06/23 19:55 V31761MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 04/06/23 19:55 V31761MSA
62.6 µg/L 21.0 50.0o-Xylene 100 04/06/23 19:55 V31761MSA
1630 µg/L 42.0 100m,p-Xylene 100 04/06/23 19:55 V31761MSA
1690 µg/L 21.0 50.0Xylene (Total)100 04/06/23 19:55 V31761
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%04/06/23 19:55100 MSA V31761
Surrogate: Dibromofluoromethane 101 Limits: 70-130%04/06/23 19:55100 MSA V31761
Surrogate: 1,2-Dichloroethane - d4 107 Limits: 70-130%04/06/23 19:55100 MSA V31761
Surrogate: Toluene-d8 99.4 Limits: 70-130%04/06/23 19:55100 MSA V31761
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 93 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-3
92537 Matrix:
3/28/2023 12:49
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 04/06/23 02:15 6200BMSA
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%04/06/23 02:151 MSA V31717
Surrogate: Dibromofluoromethane 96.8 Limits: 70-130%04/06/23 02:151 MSA V31717
Surrogate: 1,2-Dichloroethane - d4 92.8 Limits: 70-130%04/06/23 02:151 MSA V31717
Surrogate: Toluene-d8 97.6 Limits: 70-130%04/06/23 02:151 MSA V31717
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 94 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-3
92537 Matrix:
3/28/2023 12:49
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31715 04/05/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 04/06/23 02:15 V31717MSA
25.6 µg/L 0.180 0.500Benzene 1 04/06/23 02:15 V31717MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 04/06/23 02:15 V31717MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 04/06/23 02:15 V31717MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 04/06/23 02:15 V31717MSA
<1.50 µg/L 1.50 5.00Bromoform 1 04/06/23 02:15 V31717MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 04/06/23 02:15 V31717MSA
0.349 J µg/L 0.180 0.500n-Butylbenzene 1 04/06/23 02:15 V31717MSA
0.534 µg/L 0.200 0.500sec-Butyl benzene 1 04/06/23 02:15 V31717MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 04/06/23 02:15 V31717MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 04/06/23 02:15 V31717MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 04/06/23 02:15 V31717MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 04/06/23 02:15 V31717MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 04/06/23 02:15 V31717MSA
<0.220 µg/L 0.220 0.500Chloroform 1 04/06/23 02:15 V31717MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 04/06/23 02:15 V31717MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 04/06/23 02:15 V31717MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 04/06/23 02:15 V31717MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 04/06/23 02:15 V31717MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 04/06/23 02:15 V31717MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 04/06/23 02:15 V31717MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 04/06/23 02:15 V31717MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 95 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-3
92537 Matrix:
3/28/2023 12:49
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31715 04/05/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 04/06/23 02:15 V31717MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 04/06/23 02:15 V31717MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 04/06/23 02:15 V31717MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 04/06/23 02:15 V31717MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 04/06/23 02:15 V31717MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 04/06/23 02:15 V31717MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 04/06/23 02:15 V31717MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 04/06/23 02:15 V31717MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 04/06/23 02:15 V31717MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 04/06/23 02:15 V31717MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 04/06/23 02:15 V31717MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 04/06/23 02:15 V31717MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 04/06/23 02:15 V31717MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 04/06/23 02:15 V31717MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 04/06/23 02:15 V31717MSA
<42.0 µg/L 42.0 200Ethanol 1 04/06/23 02:15 V31717MSA
18.8 µg/L 0.170 0.500Ethylbenzene 1 04/06/23 02:15 V31717MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 04/06/23 02:15 V31717MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 04/06/23 02:15 V31717MSA
1.73 µg/L 0.180 0.500Isopropylbenzene 1 04/06/23 02:15 V31717MSA
0.848 µg/L 0.089 0.5004-Isopropyl toluene 1 04/06/23 02:15 V31717MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 04/06/23 02:15 V31717MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 96 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-3
92537 Matrix:
3/28/2023 12:49
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31715 04/05/23 09:00
28.6 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 04/06/23 02:15 V31717MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 04/06/23 02:15 V31717MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 04/06/23 02:15 V31717MSA
38.4 µg/L 0.470 1.00Naphthalene 1 04/06/23 02:15 V31717MSA
2.32 µg/L 0.190 0.500n-Propylbenzene 1 04/06/23 02:15 V31717MSA
<0.220 µg/L 0.220 0.500Styrene 1 04/06/23 02:15 V31717MSA
61.5 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 04/06/23 02:15 V31717MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 04/06/23 02:15 V31717MSA
81.4 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 04/06/23 02:15 V31717MSA
1.31 J µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 04/06/23 02:15 V31717MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 04/06/23 02:15 V31717MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 04/06/23 02:15 V31717MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 04/06/23 02:15 V31717MSA
<0.220 µg/L 0.220 0.500Toluene 1 04/06/23 02:15 V31717MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 04/06/23 02:15 V31717MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 04/06/23 02:15 V31717MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 04/06/23 02:15 V31717MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 04/06/23 02:15 V31717MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 04/06/23 02:15 V31717MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 04/06/23 02:15 V31717MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 04/06/23 02:15 V31717MSA
20.6 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 04/06/23 02:15 V31717MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 97 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-3
92537 Matrix:
3/28/2023 12:49
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31715 04/05/23 09:00
0.947 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 04/06/23 02:15 V31717MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 04/06/23 02:15 V31717MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 04/06/23 02:15 V31717MSA
4.35 µg/L 0.210 0.500o-Xylene 1 04/06/23 02:15 V31717MSA
1.42 µg/L 0.420 1.00m,p-Xylene 1 04/06/23 02:15 V31717MSA
5.77 µg/L 0.210 0.500Xylene (Total)1 04/06/23 02:15 V31717
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%04/06/23 02:151 MSA V31717
Surrogate: Dibromofluoromethane 96.8 Limits: 70-130%04/06/23 02:151 MSA V31717
Surrogate: 1,2-Dichloroethane - d4 92.8 Limits: 70-130%04/06/23 02:151 MSA V31717
Surrogate: Toluene-d8 97.6 Limits: 70-130%04/06/23 02:151 MSA V31717
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 98 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-2
92538 Matrix:
3/28/2023 13:02
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 04/06/23 05:52 6200BMSA
Surrogate: 4-Bromofluorobenzene 106 Limits: 70-130%04/06/23 05:521 MSA V31717
Surrogate: Dibromofluoromethane 97.8 Limits: 70-130%04/06/23 05:521 MSA V31717
Surrogate: 1,2-Dichloroethane - d4 93.2 Limits: 70-130%04/06/23 05:521 MSA V31717
Surrogate: Toluene-d8 97.0 Limits: 70-130%04/06/23 05:521 MSA V31717
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%04/11/23 03:45100 MSA V31866
Surrogate: Dibromofluoromethane 100 Limits: 70-130%04/11/23 03:45100 MSA V31866
Surrogate: 1,2-Dichloroethane - d4 98.0 Limits: 70-130%04/11/23 03:45100 MSA V31866
Surrogate: Toluene-d8 101 Limits: 70-130%04/11/23 03:45100 MSA V31866
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 99 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-2
92538 Matrix:
3/28/2023 13:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31715 04/05/23 09:00 V31860 04/10/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 04/06/23 05:52 V31717MSA
14.5 µg/L 0.180 0.500Benzene 1 04/06/23 05:52 V31717MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 04/06/23 05:52 V31717MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 04/06/23 05:52 V31717MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 04/06/23 05:52 V31717MSA
<1.50 µg/L 1.50 5.00Bromoform 1 04/06/23 05:52 V31717MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 04/06/23 05:52 V31717MSA
25.1 µg/L 0.180 0.500n-Butylbenzene 1 04/06/23 05:52 V31717MSA
6.32 µg/L 0.200 0.500sec-Butyl benzene 1 04/06/23 05:52 V31717MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 04/06/23 05:52 V31717MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 04/06/23 05:52 V31717MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 04/06/23 05:52 V31717MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 04/06/23 05:52 V31717MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 04/06/23 05:52 V31717MSA
<0.220 µg/L 0.220 0.500Chloroform 1 04/06/23 05:52 V31717MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 04/06/23 05:52 V31717MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 04/06/23 05:52 V31717MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 04/06/23 05:52 V31717MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 04/06/23 05:52 V31717MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 04/06/23 05:52 V31717MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 04/06/23 05:52 V31717MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 04/06/23 05:52 V31717MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 100 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-2
92538 Matrix:
3/28/2023 13:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31715 04/05/23 09:00 V31860 04/10/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 04/06/23 05:52 V31717MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 04/06/23 05:52 V31717MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 04/06/23 05:52 V31717MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 04/06/23 05:52 V31717MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 04/06/23 05:52 V31717MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 04/06/23 05:52 V31717MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 04/06/23 05:52 V31717MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 04/06/23 05:52 V31717MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 04/06/23 05:52 V31717MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 04/06/23 05:52 V31717MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 04/06/23 05:52 V31717MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 04/06/23 05:52 V31717MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 04/06/23 05:52 V31717MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 04/06/23 05:52 V31717MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 04/06/23 05:52 V31717MSA
<42.0 µg/L 42.0 200Ethanol 1 04/06/23 05:52 V31717MSA
1020 µg/L 17.0 50.0Ethylbenzene 100 04/11/23 03:45 V31866MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 04/06/23 05:52 V31717MSA
0.425 J µg/L 0.380 1.002-Hexanone 1 04/06/23 05:52 V31717MSA
54.0 µg/L 0.180 0.500Isopropylbenzene 1 04/06/23 05:52 V31717MSA
4.91 µg/L 0.089 0.5004-Isopropyl toluene 1 04/06/23 05:52 V31717MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 04/06/23 05:52 V31717MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 101 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-2
92538 Matrix:
3/28/2023 13:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31715 04/05/23 09:00 V31860 04/10/23 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 04/06/23 05:52 V31717MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 04/06/23 05:52 V31717MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 04/06/23 05:52 V31717MSA
476 µg/L 47.0 100Naphthalene 100 04/11/23 03:45 V31866MSA
115 µg/L 19.0 50.0n-Propylbenzene 100 04/11/23 03:45 V31866MSA
1.32 µg/L 0.220 0.500Styrene 1 04/06/23 05:52 V31717MSA
2.04 J µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 04/06/23 05:52 V31717MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 04/06/23 05:52 V31717MSA
6.56 J µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 04/06/23 05:52 V31717MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 04/06/23 05:52 V31717MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 04/06/23 05:52 V31717MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 04/06/23 05:52 V31717MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 04/06/23 05:52 V31717MSA
2.67 µg/L 0.220 0.500Toluene 1 04/06/23 05:52 V31717MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 04/06/23 05:52 V31717MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 04/06/23 05:52 V31717MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 04/06/23 05:52 V31717MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 04/06/23 05:52 V31717MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 04/06/23 05:52 V31717MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 04/06/23 05:52 V31717MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 04/06/23 05:52 V31717MSA
992 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 04/11/23 03:45 V31866MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 102 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-2
92538 Matrix:
3/28/2023 13:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31715 04/05/23 09:00 V31860 04/10/23 09:00
309 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 04/11/23 03:45 V31866MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 04/06/23 05:52 V31717MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 04/06/23 05:52 V31717MSA
252 µg/L 21.0 50.0o-Xylene 100 04/11/23 03:45 V31866MSA
632 µg/L 42.0 100m,p-Xylene 100 04/11/23 03:45 V31866MSA
884 µg/L 21.0 50.0Xylene (Total)100 04/11/23 03:45 V31866
Surrogate: 4-Bromofluorobenzene 106 Limits: 70-130%04/06/23 05:521 MSA V31717
Surrogate: Dibromofluoromethane 97.8 Limits: 70-130%04/06/23 05:521 MSA V31717
Surrogate: 1,2-Dichloroethane - d4 93.2 Limits: 70-130%04/06/23 05:521 MSA V31717
Surrogate: Toluene-d8 97.0 Limits: 70-130%04/06/23 05:521 MSA V31717
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%04/11/23 03:45100 MSA V31866
Surrogate: Dibromofluoromethane 100 Limits: 70-130%04/11/23 03:45100 MSA V31866
Surrogate: 1,2-Dichloroethane - d4 98.0 Limits: 70-130%04/11/23 03:45100 MSA V31866
Surrogate: Toluene-d8 101 Limits: 70-130%04/11/23 03:45100 MSA V31866
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 103 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-1
92539 Matrix:
3/28/2023 13:16
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 04/06/23 21:08 6200BMSA
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%04/06/23 21:08100 MSA V31761
Surrogate: Dibromofluoromethane 103 Limits: 70-130%04/06/23 21:08100 MSA V31761
Surrogate: 1,2-Dichloroethane - d4 107 Limits: 70-130%04/06/23 21:08100 MSA V31761
Surrogate: Toluene-d8 99.4 Limits: 70-130%04/06/23 21:08100 MSA V31761
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 104 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-1
92539 Matrix:
3/28/2023 13:16
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31760 04/06/23 09:00
<180 µg/L 180 1000Acetone 100 04/06/23 21:08 V31761MSA
3960 µg/L 18.0 50.0Benzene 100 04/06/23 21:08 V31761MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 04/06/23 21:08 V31761MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 04/06/23 21:08 V31761MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 04/06/23 21:08 V31761MSA
<150 µg/L 150 500Bromoform 100 04/06/23 21:08 V31761MSA
<28.0 µg/L 28.0 100Bromomethane 100 04/06/23 21:08 V31761MSA
30.0 J µg/L 18.0 50.0n-Butylbenzene 100 04/06/23 21:08 V31761MSA
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 04/06/23 21:08 V31761MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 04/06/23 21:08 V31761MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 04/06/23 21:08 V31761MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 04/06/23 21:08 V31761MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 04/06/23 21:08 V31761MSA
<43.0 µg/L 43.0 100Chloroethane 100 04/06/23 21:08 V31761MSA
<22.0 µg/L 22.0 50.0Chloroform 100 04/06/23 21:08 V31761MSA
<22.0 µg/L 22.0 50.0Chloromethane 100 04/06/23 21:08 V31761MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 04/06/23 21:08 V31761MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 04/06/23 21:08 V31761MSA
<50.0 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 04/06/23 21:08 V31761MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 04/06/23 21:08 V31761MSA
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 04/06/23 21:08 V31761MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 04/06/23 21:08 V31761MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 105 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-1
92539 Matrix:
3/28/2023 13:16
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31760 04/06/23 09:00
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 04/06/23 21:08 V31761MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 04/06/23 21:08 V31761MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 04/06/23 21:08 V31761MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 04/06/23 21:08 V31761MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 04/06/23 21:08 V31761MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 04/06/23 21:08 V31761MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 04/06/23 21:08 V31761MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 04/06/23 21:08 V31761MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 04/06/23 21:08 V31761MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 04/06/23 21:08 V31761MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 04/06/23 21:08 V31761MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 04/06/23 21:08 V31761MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 04/06/23 21:08 V31761MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 04/06/23 21:08 V31761MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 04/06/23 21:08 V31761MSA
<4200 µg/L 4200 20000Ethanol 100 04/06/23 21:08 V31761MSA
3330 µg/L 17.0 50.0Ethylbenzene 100 04/06/23 21:08 V31761MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 04/06/23 21:08 V31761MSA
<38.0 µg/L 38.0 1002-Hexanone 100 04/06/23 21:08 V31761MSA
145 µg/L 18.0 50.0Isopropylbenzene 100 04/06/23 21:08 V31761MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 04/06/23 21:08 V31761MSA
<71.0 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 04/06/23 21:08 V31761MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 106 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-1
92539 Matrix:
3/28/2023 13:16
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31760 04/06/23 09:00
1110 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 04/06/23 21:08 V31761MSA
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 04/06/23 21:08 V31761MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 04/06/23 21:08 V31761MSA
1190 µg/L 47.0 100Naphthalene 100 04/06/23 21:08 V31761MSA
407 µg/L 19.0 50.0n-Propylbenzene 100 04/06/23 21:08 V31761MSA
<22.0 µg/L 22.0 50.0Styrene 100 04/06/23 21:08 V31761MSA
1060 µg/L 160 1000tert-Butyl Alcohol (TBA)100 04/06/23 21:08 V31761MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 04/06/23 21:08 V31761MSA
801 J µg/L 190 1000tert-Amyl Alcohol (TAA)100 04/06/23 21:08 V31761MSA
208 J µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 04/06/23 21:08 V31761MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 04/06/23 21:08 V31761MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 04/06/23 21:08 V31761MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 04/06/23 21:08 V31761MSA
109 µg/L 22.0 50.0Toluene 100 04/06/23 21:08 V31761MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 04/06/23 21:08 V31761MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 04/06/23 21:08 V31761MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 04/06/23 21:08 V31761MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 04/06/23 21:08 V31761MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 04/06/23 21:08 V31761MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 04/06/23 21:08 V31761MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 04/06/23 21:08 V31761MSA
49.7 J µg/L 19.0 50.01,2,4-Trimethylbenzene 100 04/06/23 21:08 V31761MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 107 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-1
92539 Matrix:
3/28/2023 13:16
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31760 04/06/23 09:00
45.0 J µg/L 18.0 50.01,3,5-Trimethylbenzene 100 04/06/23 21:08 V31761MSA
<100 µg/L 100 500Vinyl Acetate 100 04/06/23 21:08 V31761MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 04/06/23 21:08 V31761MSA
27.4 J µg/L 21.0 50.0o-Xylene 100 04/06/23 21:08 V31761MSA
209 µg/L 42.0 100m,p-Xylene 100 04/06/23 21:08 V31761MSA
236 J µg/L 21.0 50.0Xylene (Total)100 04/06/23 21:08 V31761
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%04/06/23 21:08100 MSA V31761
Surrogate: Dibromofluoromethane 103 Limits: 70-130%04/06/23 21:08100 MSA V31761
Surrogate: 1,2-Dichloroethane - d4 107 Limits: 70-130%04/06/23 21:08100 MSA V31761
Surrogate: Toluene-d8 99.4 Limits: 70-130%04/06/23 21:08100 MSA V31761
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 108 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-5
92540 Matrix:
3/28/2023 13:28
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0 1003,3-Dimethyl-1-butanol 10 04/06/23 06:47 6200BMSA
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%04/06/23 06:4710 MSA V31717
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%04/06/23 06:4710 MSA V31717
Surrogate: 1,2-Dichloroethane - d4 93.2 Limits: 70-130%04/06/23 06:4710 MSA V31717
Surrogate: Toluene-d8 96.8 Limits: 70-130%04/06/23 06:4710 MSA V31717
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%04/11/23 04:34100 MSA V31866
Surrogate: Dibromofluoromethane 98.6 Limits: 70-130%04/11/23 04:34100 MSA V31866
Surrogate: 1,2-Dichloroethane - d4 99.8 Limits: 70-130%04/11/23 04:34100 MSA V31866
Surrogate: Toluene-d8 101 Limits: 70-130%04/11/23 04:34100 MSA V31866
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%04/12/23 09:061000 TBL V31920
Surrogate: Dibromofluoromethane 98.0 Limits: 70-130%04/12/23 09:061000 TBL V31920
Surrogate: 1,2-Dichloroethane - d4 95.4 Limits: 70-130%04/12/23 09:061000 TBL V31920
Surrogate: Toluene-d8 101 Limits: 70-130%04/12/23 09:061000 TBL V31920
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 109 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-5
92540 Matrix:
3/28/2023 13:28
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31715 04/05/23 09:00 V31860 04/10/23 09:00
V31919 04/11/23 08:00
<18.0 µg/L 18.0 100Acetone 10 04/06/23 06:47 V31717MSA
8260 µg/L 18.0 50.0Benzene 100 04/11/23 04:34 V31866MSA
<2.10 µg/L 2.10 5.00Bromobenzene 10 04/06/23 06:47 V31717MSA
<4.20 µg/L 4.20 10.0Bromochloromethane 10 04/06/23 06:47 V31717MSA
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 04/06/23 06:47 V31717MSA
<15.0 µg/L 15.0 50.0Bromoform 10 04/06/23 06:47 V31717MSA
<2.80 µg/L 2.80 10.0Bromomethane 10 04/06/23 06:47 V31717MSA
30.6 µg/L 1.80 5.00n-Butylbenzene 10 04/06/23 06:47 V31717MSA
20.9 µg/L 2.00 5.00sec-Butyl benzene 10 04/06/23 06:47 V31717MSA
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 04/06/23 06:47 V31717MSA
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 04/06/23 06:47 V31717MSA
<1.90 µg/L 1.90 5.00Chlorobenzene 10 04/06/23 06:47 V31717MSA
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 04/06/23 06:47 V31717MSA
<4.30 µg/L 4.30 10.0Chloroethane 10 04/06/23 06:47 V31717MSA
<2.20 µg/L 2.20 5.00Chloroform 10 04/06/23 06:47 V31717MSA
<2.20 µg/L 2.20 5.00Chloromethane 10 04/06/23 06:47 V31717MSA
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 04/06/23 06:47 V31717MSA
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 04/06/23 06:47 V31717MSA
22.6 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 04/06/23 06:47 V31717MSA
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 04/06/23 06:47 V31717MSA
<2.00 µg/L 2.00 5.001,2-Dibromoethane 10 04/06/23 06:47 V31717MSA
<2.30 µg/L 2.30 5.00Dibromomethane 10 04/06/23 06:47 V31717MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 110 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-5
92540 Matrix:
3/28/2023 13:28
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31715 04/05/23 09:00 V31860 04/10/23 09:00
V31919 04/11/23 08:00
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 04/06/23 06:47 V31717MSA
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 04/06/23 06:47 V31717MSA
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 04/06/23 06:47 V31717MSA
<12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 04/06/23 06:47 V31717MSA
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 04/06/23 06:47 V31717MSA
<1.50 µg/L 1.50 5.001,2-Dichloroethane 10 04/06/23 06:47 V31717MSA
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 04/06/23 06:47 V31717MSA
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 04/06/23 06:47 V31717MSA
<1.80 µg/L 1.80 5.00trans-1,2-Dichloroethene 10 04/06/23 06:47 V31717MSA
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 04/06/23 06:47 V31717MSA
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 04/06/23 06:47 V31717MSA
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 04/06/23 06:47 V31717MSA
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 04/06/23 06:47 V31717MSA
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 04/06/23 06:47 V31717MSA
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 04/06/23 06:47 V31717MSA
<420 µg/L 420 2000Ethanol 10 04/06/23 06:47 V31717MSA
2270 µg/L 17.0 50.0Ethylbenzene 100 04/11/23 04:34 V31866MSA
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 04/06/23 06:47 V31717MSA
<3.80 µg/L 3.80 10.02-Hexanone 10 04/06/23 06:47 V31717MSA
108 µg/L 1.80 5.00Isopropylbenzene 10 04/06/23 06:47 V31717MSA
12.6 µg/L 0.890 5.004-Isopropyl toluene 10 04/06/23 06:47 V31717MSA
<7.10 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 04/06/23 06:47 V31717MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 111 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-5
92540 Matrix:
3/28/2023 13:28
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31715 04/05/23 09:00 V31860 04/10/23 09:00
V31919 04/11/23 08:00
3240 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 04/11/23 04:34 V31866MSA
<0.780 µg/L 0.780 10.04-Methyl-2-Pentanone 10 04/06/23 06:47 V31717MSA
<3.30 µg/L 3.30 20.0Methylene Chloride 10 04/06/23 06:47 V31717MSA
854 µg/L 4.70 10.0Naphthalene 10 04/06/23 06:47 V31717MSA
335 µg/L 1.90 5.00n-Propylbenzene 10 04/06/23 06:47 V31717MSA
14.7 µg/L 2.20 5.00Styrene 10 04/06/23 06:47 V31717MSA
477 µg/L 16.0 100tert-Butyl Alcohol (TBA)10 04/06/23 06:47 V31717MSA
<3.50 µg/L 3.50 100tert-Butyl formate (TBF)10 04/06/23 06:47 V31717MSA
3690 µg/L 190 1000tert-Amyl Alcohol (TAA)100 04/11/23 04:34 V31866MSA
588 µg/L 2.80 100tert-Amyl Methyl Ether (TAME)10 04/06/23 06:47 V31717MSA
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 04/06/23 06:47 V31717MSA
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 04/06/23 06:47 V31717MSA
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 04/06/23 06:47 V31717MSA
11400 µg/L 220 500Toluene 1000 04/12/23 09:06 V31920TBL
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 04/06/23 06:47 V31717MSA
<3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 04/06/23 06:47 V31717MSA
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 04/06/23 06:47 V31717MSA
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 04/06/23 06:47 V31717MSA
<1.80 µg/L 1.80 5.00Trichloroethene 10 04/06/23 06:47 V31717MSA
<1.80 µg/L 1.80 5.00Trichlorofluoromethane 10 04/06/23 06:47 V31717MSA
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 04/06/23 06:47 V31717MSA
3430 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 04/11/23 04:34 V31866MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 112 of 142
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-088-0022
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #2796 Received : 03/29/2023
Stone's Fast Save
Report Date : 04/12/2023
Sample ID :
Lab No :
Sampled:MW-5
92540 Matrix:
3/28/2023 13:28
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V31715 04/05/23 09:00 V31860 04/10/23 09:00
V31919 04/11/23 08:00
862 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 04/06/23 06:47 V31717MSA
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 04/06/23 06:47 V31717MSA
<1.70 µg/L 1.70 5.00Vinyl Chloride 10 04/06/23 06:47 V31717MSA
1990 µg/L 21.0 50.0o-Xylene 100 04/11/23 04:34 V31866MSA
7020 µg/L 42.0 100m,p-Xylene 100 04/11/23 04:34 V31866MSA
9010 µg/L 21.0 50.0Xylene (Total)100 04/11/23 04:34 V31866
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%04/06/23 06:4710 MSA V31717
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%04/06/23 06:4710 MSA V31717
Surrogate: 1,2-Dichloroethane - d4 93.2 Limits: 70-130%04/06/23 06:4710 MSA V31717
Surrogate: Toluene-d8 96.8 Limits: 70-130%04/06/23 06:4710 MSA V31717
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%04/11/23 04:34100 MSA V31866
Surrogate: Dibromofluoromethane 98.6 Limits: 70-130%04/11/23 04:34100 MSA V31866
Surrogate: 1,2-Dichloroethane - d4 99.8 Limits: 70-130%04/11/23 04:34100 MSA V31866
Surrogate: Toluene-d8 101 Limits: 70-130%04/11/23 04:34100 MSA V31866
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%04/12/23 09:061000 TBL V31920
Surrogate: Dibromofluoromethane 98.0 Limits: 70-130%04/12/23 09:061000 TBL V31920
Surrogate: 1,2-Dichloroethane - d4 95.4 Limits: 70-130%04/12/23 09:061000 TBL V31920
Surrogate: Toluene-d8 101 Limits: 70-130%04/12/23 09:061000 TBL V31920
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 113 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31711QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31710
Associated Lab Samples: 92521, 92523, 92524, 92525, 92526, 92527, 92528, 92529, 92530, 92531, 92532
LRB-V31710 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/05/23 23:2710.01.80<1.80µg/LAcetone
04/05/23 23:270.5000.180<0.180µg/LBenzene
04/05/23 23:270.5000.210<0.210µg/LBromobenzene
04/05/23 23:271.000.420<0.420µg/LBromochloromethane
04/05/23 23:270.5000.160<0.160µg/LBromodichloromethane
04/05/23 23:275.001.50<1.50µg/LBromoform
04/05/23 23:271.000.280<0.280µg/LBromomethane
04/05/23 23:270.5000.180<0.180µg/Ln-Butylbenzene
04/05/23 23:270.5000.200<0.200µg/Lsec-Butyl benzene
04/05/23 23:272.000.920<0.920µg/Ltert-Butyl benzene
04/05/23 23:270.5000.180<0.180µg/LCarbon Tetrachloride
04/05/23 23:270.5000.190<0.190µg/LChlorobenzene
04/05/23 23:270.5000.190<0.190µg/LChlorodibromomethane
04/05/23 23:271.000.430<0.430µg/LChloroethane
04/05/23 23:270.5000.220<0.220µg/LChloroform
04/05/23 23:270.5000.220<0.220µg/LChloromethane
04/05/23 23:270.5000.200<0.200µg/L2-Chlorotoluene
04/05/23 23:270.5000.200<0.200µg/L4-Chlorotoluene
04/05/23 23:270.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
04/05/23 23:272.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
04/05/23 23:270.5000.200<0.200µg/L1,2-Dibromoethane
04/05/23 23:270.5000.230<0.230µg/LDibromomethane
04/05/23 23:270.5000.220<0.220µg/L1,2-Dichlorobenzene
04/05/23 23:270.5000.190<0.190µg/L1,3-Dichlorobenzene
04/05/23 23:270.5000.210<0.210µg/L1,4-Dichlorobenzene
04/05/23 23:275.001.20<1.20µg/LDichlorodifluoromethane
04/05/23 23:270.5000.240<0.240µg/L1,1-Dichloroethane
Page 1 of 25Date:04/12/2023 05:12 PM
Page 114 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31711QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31710
Associated Lab Samples: 92521, 92523, 92524, 92525, 92526, 92527, 92528, 92529, 92530, 92531, 92532
LRB-V31710 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/05/23 23:270.5000.150<0.150µg/L1,2-Dichloroethane
04/05/23 23:270.5000.150<0.150µg/L1,1-Dichloroethene
04/05/23 23:270.5000.200<0.200µg/Lcis-1,2-Dichloroethene
04/05/23 23:270.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
04/05/23 23:270.5000.190<0.190µg/L1,2-Dichloropropane
04/05/23 23:270.5000.130<0.130µg/L1,3-Dichloropropane
04/05/23 23:272.000.210<0.210µg/L2,2-Dichloropropane
04/05/23 23:270.5000.200<0.200µg/L1,1-Dichloropropene
04/05/23 23:270.5000.210<0.210µg/Lcis-1,3-Dichloropropene
04/05/23 23:270.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
04/05/23 23:2720042.0<42.0µg/LEthanol
04/05/23 23:270.5000.170<0.170µg/LEthylbenzene
04/05/23 23:273.000.350<0.350µg/LHexachlorobutadiene
04/05/23 23:271.000.380<0.380µg/L2-Hexanone
04/05/23 23:270.5000.180<0.180µg/LIsopropylbenzene
04/05/23 23:270.5000.089<0.089µg/L4-Isopropyl toluene
04/05/23 23:275.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
04/05/23 23:271.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
04/05/23 23:271.000.078<0.078µg/L4-Methyl-2-Pentanone
04/05/23 23:272.000.330<0.330µg/LMethylene Chloride
04/05/23 23:271.000.470<0.470µg/LNaphthalene
04/05/23 23:270.5000.190<0.190µg/Ln-Propylbenzene
04/05/23 23:270.5000.220<0.220µg/LStyrene
04/05/23 23:2710.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
04/05/23 23:2710.00.350<0.350µg/Ltert-Butyl formate (TBF)
04/05/23 23:2710.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
04/05/23 23:2710.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 2 of 25Date:04/12/2023 05:12 PM
Page 115 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31711QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31710
Associated Lab Samples: 92521, 92523, 92524, 92525, 92526, 92527, 92528, 92529, 92530, 92531, 92532
LRB-V31710 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/05/23 23:270.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
04/05/23 23:270.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
04/05/23 23:270.5000.220<0.220µg/LTetrachloroethene
04/05/23 23:270.5000.220<0.220µg/LToluene
04/05/23 23:270.5000.380<0.380µg/L1,2,3-Trichlorobenzene
04/05/23 23:270.5000.310<0.310µg/L1,2,4-Trichlorobenzene
04/05/23 23:270.5000.160<0.160µg/L1,1,1-Trichloroethane
04/05/23 23:270.5000.096<0.096µg/L1,1,2-Trichloroethane
04/05/23 23:270.5000.180<0.180µg/LTrichloroethene
04/05/23 23:270.5000.180<0.180µg/LTrichlorofluoromethane
04/05/23 23:270.5000.270<0.270µg/L1,2,3-Trichloropropane
04/05/23 23:270.5000.190<0.190µg/L1,2,4-Trimethylbenzene
04/05/23 23:270.5000.180<0.180µg/L1,3,5-Trimethylbenzene
04/05/23 23:275.001.00<1.00µg/LVinyl Acetate
04/05/23 23:270.5000.170<0.170µg/LVinyl Chloride
04/05/23 23:270.5000.210<0.210µg/Lo-Xylene
04/05/23 23:271.000.420<0.420µg/Lm,p-Xylene
04/05/23 23:2710.01.00<1.00µg/L3,3-Dimethyl-1-butanol
04/05/23 23:274-Bromofluorobenzene (S)102 70-130
04/05/23 23:27Dibromofluoromethane (S)101 70-130
04/05/23 23:271,2-Dichloroethane - d4 (S)104 70-130
04/05/23 23:27Toluene-d8 (S)98.6 70-130
Page 3 of 25Date:04/12/2023 05:12 PM
Page 116 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31711QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31710
LCS-V31710 LCSD-V31710Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
32.1 80.259.723.940.0µg/LAcetone 40-160 29.2*20.0
20.1 10197.519.520.0µg/LBenzene 70-130 3.0 20.0
20.6 10310020.020.0µg/LBromobenzene 70-130 2.9 20.0
20.6 10310120.120.0µg/LBromochloromethane 70-130 2.4 20.0
19.9 99.594.018.820.0µg/LBromodichloromethane 70-130 5.6 20.0
22.7 11496.019.220.0µg/LBromoform 70-130 16.7 20.0
22.4 11211122.220.0µg/LBromomethane 60-140 0.8 20.0
20.4 10210120.120.0µg/Ln-Butylbenzene 70-130 1.4 20.0
20.1 10110120.220.0µg/Lsec-Butyl benzene 70-130 0.4 20.0
20.2 10110120.120.0µg/Ltert-Butyl benzene 70-130 0.4 20.0
20.0 10096.519.320.0µg/LCarbon Tetrachloride 70-130 3.5 20.0
19.7 98.596.519.320.0µg/LChlorobenzene 70-130 2.0 20.0
22.0 11010220.420.0µg/LChlorodibromomethane 70-130 7.5 20.0
19.7 98.510120.220.0µg/LChloroethane 60-140 2.5 20.0
20.1 10197.519.520.0µg/LChloroform 70-130 3.0 20.0
18.4 92.094.518.920.0µg/LChloromethane 60-140 2.6 20.0
19.9 99.599.019.820.0µg/L2-Chlorotoluene 70-130 0.5 20.0
20.5 10310120.220.0µg/L4-Chlorotoluene 70-130 1.4 20.0
19.6 98.093.518.720.0µg/LDi-Isopropyl Ether (DIPE)70-130 4.6 20.0
25.3 12710220.320.0µg/L1,2-Dibromo-3-Chloropropane 70-130 21.9*20.0
21.0 10593.518.720.0µg/L1,2-Dibromoethane 70-130 11.5 20.0
21.0 10591.018.220.0µg/LDibromomethane 70-130 14.2 20.0
20.7 10410020.020.0µg/L1,2-Dichlorobenzene 70-130 3.4 20.0
20.4 10210220.420.0µg/L1,3-Dichlorobenzene 70-130 0.0 20.0
20.3 10298.519.720.0µg/L1,4-Dichlorobenzene 70-130 3.0 20.0
18.4 92.095.019.020.0µg/LDichlorodifluoromethane 60-140 3.2 20.0
Page 4 of 25* QC Fail Date:04/12/2023 05:12 PM
Page 117 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31711QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31710
LCS-V31710 LCSD-V31710Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.8 99.099.019.820.0µg/L1,1-Dichloroethane 70-130 0.0 20.0
20.6 10394.018.820.0µg/L1,2-Dichloroethane 70-130 9.1 20.0
19.6 98.096.519.320.0µg/L1,1-Dichloroethene 70-130 1.5 20.0
19.6 98.093.018.620.0µg/Lcis-1,2-Dichloroethene 70-130 5.2 20.0
19.7 98.597.519.520.0µg/Ltrans-1,2-Dichloroethene 70-130 1.0 20.0
19.3 96.595.519.120.0µg/L1,2-Dichloropropane 70-130 1.0 20.0
20.2 10192.018.420.0µg/L1,3-Dichloropropane 70-130 9.3 20.0
18.8 94.095.019.020.0µg/L2,2-Dichloropropane 70-130 1.0 20.0
20.5 10310220.320.0µg/L1,1-Dichloropropene 70-130 0.9 20.0
20.2 10194.518.920.0µg/Lcis-1,3-Dichloropropene 70-130 6.6 20.0
21.4 10795.019.020.0µg/Ltrans-1,3-Dichloropropene 70-130 11.8 20.0
577 11588.8444500µg/LEthanol 60-140 26.0*20.0
19.7 98.597.519.520.0µg/LEthylbenzene 70-130 1.0 20.0
20.6 10399.019.820.0µg/LHexachlorobutadiene 70-130 3.9 20.0
22.1 11184.016.820.0µg/L2-Hexanone 60-140 27.2*20.0
20.5 10310320.520.0µg/LIsopropylbenzene 70-130 0.0 20.0
20.3 10210220.320.0µg/L4-Isopropyl toluene 70-130 0.0 20.0
20.4 10292.018.420.0µg/LMethyl Ethyl Ketone (MEK)60-140 10.3 20.0
21.6 10895.519.120.0µg/LMethyl tert-butyl ether (MTBE)70-130 12.2 20.0
22.9 11582.516.520.0µg/L4-Methyl-2-Pentanone 60-140 32.4*20.0
18.5 92.592.518.520.0µg/LMethylene Chloride 70-130 0.0 20.0
24.3 12210320.620.0µg/LNaphthalene 70-130 16.4 20.0
19.7 98.510020.020.0µg/Ln-Propylbenzene 70-130 1.5 20.0
21.1 10610120.220.0µg/LStyrene 70-130 4.3 20.0
50.4 12610843.340.0µg/Ltert-Butyl Alcohol (TBA)40-140 15.1 20.0
45.0 11394.237.740.0µg/Ltert-Butyl formate (TBF)40-140 17.6 20.0
Page 5 of 25* QC Fail Date:04/12/2023 05:12 PM
Page 118 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31711QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31710
LCS-V31710 LCSD-V31710Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
24.1 12188.517.720.0µg/Ltert-Amyl Alcohol (TAA)40-140 30.6*20.0
43.1 10896.738.740.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 10.7 20.0
20.7 10410120.220.0µg/L1,1,1,2-Tetrachloroethane 70-130 2.4 20.0
22.1 11195.019.020.0µg/L1,1,2,2-Tetrachloroethane 70-130 15.0 20.0
20.5 10310220.420.0µg/LTetrachloroethene 70-130 0.4 20.0
19.9 99.597.519.520.0µg/LToluene 70-130 2.0 20.0
24.4 12211022.020.0µg/L1,2,3-Trichlorobenzene 70-130 10.3 20.0
22.3 11210621.220.0µg/L1,2,4-Trichlorobenzene 70-130 5.0 20.0
20.0 10098.519.720.0µg/L1,1,1-Trichloroethane 70-130 1.5 20.0
21.3 10796.519.320.0µg/L1,1,2-Trichloroethane 70-130 9.8 20.0
19.5 97.596.519.320.0µg/LTrichloroethene 70-130 1.0 20.0
18.8 94.098.519.720.0µg/LTrichlorofluoromethane 60-140 4.6 20.0
22.2 11197.019.420.0µg/L1,2,3-Trichloropropane 70-130 13.4 20.0
20.8 10410220.420.0µg/L1,2,4-Trimethylbenzene 70-130 1.9 20.0
20.1 10110120.220.0µg/L1,3,5-Trimethylbenzene 70-130 0.4 20.0
22.2 11196.519.320.0µg/LVinyl Acetate 60-140 13.9 20.0
19.8 99.010320.520.0µg/LVinyl Chloride 60-140 3.4 20.0
20.0 10098.519.720.0µg/Lo-Xylene 70-130 1.5 20.0
41.9 10510240.640.0µg/Lm,p-Xylene 70-130 3.1 20.0
28.8 144*10721.320.0µg/L3,3-Dimethyl-1-butanol 70-130 29.9*20.0
97.81004-Bromofluorobenzene (S)70-130
10098.4Dibromofluoromethane (S)70-130
10699.81,2-Dichloroethane - d4 (S)70-130
99.699.4Toluene-d8 (S)70-130
Page 6 of 25* QC Fail Date:04/12/2023 05:12 PM
Page 119 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31717QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31715
Associated Lab Samples: 92534, 92535, 92537, 92538, 92540
LRB-V31715 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/06/23 00:2610.01.80<1.80µg/LAcetone
04/06/23 00:260.5000.180<0.180µg/LBenzene
04/06/23 00:260.5000.210<0.210µg/LBromobenzene
04/06/23 00:261.000.420<0.420µg/LBromochloromethane
04/06/23 00:260.5000.160<0.160µg/LBromodichloromethane
04/06/23 00:265.001.50<1.50µg/LBromoform
04/06/23 00:261.000.280<0.280µg/LBromomethane
04/06/23 00:260.5000.180<0.180µg/Ln-Butylbenzene
04/06/23 00:260.5000.200<0.200µg/Lsec-Butyl benzene
04/06/23 00:262.000.920<0.920µg/Ltert-Butyl benzene
04/06/23 00:260.5000.180<0.180µg/LCarbon Tetrachloride
04/06/23 00:260.5000.190<0.190µg/LChlorobenzene
04/06/23 00:260.5000.190<0.190µg/LChlorodibromomethane
04/06/23 00:261.000.430<0.430µg/LChloroethane
04/06/23 00:260.5000.220<0.220µg/LChloroform
04/06/23 00:260.5000.220<0.220µg/LChloromethane
04/06/23 00:260.5000.200<0.200µg/L2-Chlorotoluene
04/06/23 00:260.5000.200<0.200µg/L4-Chlorotoluene
04/06/23 00:260.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
04/06/23 00:262.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
04/06/23 00:260.5000.200<0.200µg/L1,2-Dibromoethane
04/06/23 00:260.5000.230<0.230µg/LDibromomethane
04/06/23 00:260.5000.220<0.220µg/L1,2-Dichlorobenzene
04/06/23 00:260.5000.190<0.190µg/L1,3-Dichlorobenzene
04/06/23 00:260.5000.210<0.210µg/L1,4-Dichlorobenzene
04/06/23 00:265.001.20<1.20µg/LDichlorodifluoromethane
04/06/23 00:260.5000.240<0.240µg/L1,1-Dichloroethane
Page 7 of 25Date:04/12/2023 05:12 PM
Page 120 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31717QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31715
Associated Lab Samples: 92534, 92535, 92537, 92538, 92540
LRB-V31715 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/06/23 00:260.5000.150<0.150µg/L1,2-Dichloroethane
04/06/23 00:260.5000.150<0.150µg/L1,1-Dichloroethene
04/06/23 00:260.5000.200<0.200µg/Lcis-1,2-Dichloroethene
04/06/23 00:260.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
04/06/23 00:260.5000.190<0.190µg/L1,2-Dichloropropane
04/06/23 00:260.5000.130<0.130µg/L1,3-Dichloropropane
04/06/23 00:262.000.210<0.210µg/L2,2-Dichloropropane
04/06/23 00:260.5000.200<0.200µg/L1,1-Dichloropropene
04/06/23 00:260.5000.210<0.210µg/Lcis-1,3-Dichloropropene
04/06/23 00:260.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
04/06/23 00:2620042.0<42.0µg/LEthanol
04/06/23 00:260.5000.170<0.170µg/LEthylbenzene
04/06/23 00:263.000.350<0.350µg/LHexachlorobutadiene
04/06/23 00:261.000.380<0.380µg/L2-Hexanone
04/06/23 00:260.5000.180<0.180µg/LIsopropylbenzene
04/06/23 00:260.5000.089<0.089µg/L4-Isopropyl toluene
04/06/23 00:265.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
04/06/23 00:261.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
04/06/23 00:261.000.078<0.078µg/L4-Methyl-2-Pentanone
04/06/23 00:262.000.330<0.330µg/LMethylene Chloride
04/06/23 00:261.000.470<0.470µg/LNaphthalene
04/06/23 00:260.5000.190<0.190µg/Ln-Propylbenzene
04/06/23 00:260.5000.220<0.220µg/LStyrene
04/06/23 00:2610.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
04/06/23 00:2610.00.350<0.350µg/Ltert-Butyl formate (TBF)
04/06/23 00:2610.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
04/06/23 00:2610.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 8 of 25Date:04/12/2023 05:12 PM
Page 121 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31717QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31715
Associated Lab Samples: 92534, 92535, 92537, 92538, 92540
LRB-V31715 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/06/23 00:260.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
04/06/23 00:260.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
04/06/23 00:260.5000.220<0.220µg/LTetrachloroethene
04/06/23 00:260.5000.220<0.220µg/LToluene
04/06/23 00:260.5000.380<0.380µg/L1,2,3-Trichlorobenzene
04/06/23 00:260.5000.310<0.310µg/L1,2,4-Trichlorobenzene
04/06/23 00:260.5000.160<0.160µg/L1,1,1-Trichloroethane
04/06/23 00:260.5000.096<0.096µg/L1,1,2-Trichloroethane
04/06/23 00:260.5000.180<0.180µg/LTrichloroethene
04/06/23 00:260.5000.180<0.180µg/LTrichlorofluoromethane
04/06/23 00:260.5000.270<0.270µg/L1,2,3-Trichloropropane
04/06/23 00:260.5000.190<0.190µg/L1,2,4-Trimethylbenzene
04/06/23 00:260.5000.180<0.180µg/L1,3,5-Trimethylbenzene
04/06/23 00:265.001.00<1.00µg/LVinyl Acetate
04/06/23 00:260.5000.170<0.170µg/LVinyl Chloride
04/06/23 00:260.5000.210<0.210µg/Lo-Xylene
04/06/23 00:261.000.420<0.420µg/Lm,p-Xylene
04/06/23 00:2610.01.00<1.00µg/L3,3-Dimethyl-1-butanol
04/06/23 00:264-Bromofluorobenzene (S)103 70-130
04/06/23 00:26Dibromofluoromethane (S)97.4 70-130
04/06/23 00:261,2-Dichloroethane - d4 (S)92.6 70-130
04/06/23 00:26Toluene-d8 (S)98.4 70-130
Page 9 of 25Date:04/12/2023 05:12 PM
Page 122 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31717QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31715
LCS-V31715 LCSD-V31715Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
30.8 77.079.531.840.0µg/LAcetone 40-160 3.1 20.0
21.4 10710120.120.0µg/LBenzene 70-130 6.2 20.0
22.0 11010621.220.0µg/LBromobenzene 70-130 3.7 20.0
22.0 11010521.020.0µg/LBromochloromethane 70-130 4.6 20.0
19.5 97.593.018.620.0µg/LBromodichloromethane 70-130 4.7 20.0
20.6 10310120.220.0µg/LBromoform 70-130 1.9 20.0
20.2 10196.019.220.0µg/LBromomethane 60-140 5.0 20.0
21.1 10610020.020.0µg/Ln-Butylbenzene 70-130 5.3 20.0
20.6 10397.019.420.0µg/Lsec-Butyl benzene 70-130 6.0 20.0
20.6 10398.019.620.0µg/Ltert-Butyl benzene 70-130 4.9 20.0
19.8 99.094.018.820.0µg/LCarbon Tetrachloride 70-130 5.1 20.0
20.9 10510020.020.0µg/LChlorobenzene 70-130 4.4 20.0
19.4 97.095.519.120.0µg/LChlorodibromomethane 70-130 1.5 20.0
19.0 95.094.018.820.0µg/LChloroethane 60-140 1.0 20.0
20.4 10296.519.320.0µg/LChloroform 70-130 5.5 20.0
18.6 93.087.017.420.0µg/LChloromethane 60-140 6.6 20.0
21.7 10910320.620.0µg/L2-Chlorotoluene 70-130 5.2 20.0
22.1 11110320.520.0µg/L4-Chlorotoluene 70-130 7.5 20.0
20.8 10410220.420.0µg/LDi-Isopropyl Ether (DIPE)70-130 1.9 20.0
20.2 10110921.820.0µg/L1,2-Dibromo-3-Chloropropane 70-130 7.6 20.0
20.9 10598.019.620.0µg/L1,2-Dibromoethane 70-130 6.4 20.0
20.5 10395.019.020.0µg/LDibromomethane 70-130 7.5 20.0
22.3 11210721.320.0µg/L1,2-Dichlorobenzene 70-130 4.5 20.0
21.8 10910420.720.0µg/L1,3-Dichlorobenzene 70-130 5.1 20.0
21.2 10610320.520.0µg/L1,4-Dichlorobenzene 70-130 3.3 20.0
15.8 79.073.514.720.0µg/LDichlorodifluoromethane 60-140 7.2 20.0
Page 10 of 25Date:04/12/2023 05:12 PM
Page 123 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31717QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31715
LCS-V31715 LCSD-V31715Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.9 10599.019.820.0µg/L1,1-Dichloroethane 70-130 5.4 20.0
19.3 96.593.018.620.0µg/L1,2-Dichloroethane 70-130 3.6 20.0
18.7 93.590.018.020.0µg/L1,1-Dichloroethene 70-130 3.8 20.0
21.0 10597.519.520.0µg/Lcis-1,2-Dichloroethene 70-130 7.4 20.0
19.9 99.595.019.020.0µg/Ltrans-1,2-Dichloroethene 70-130 4.6 20.0
22.0 11010320.520.0µg/L1,2-Dichloropropane 70-130 7.0 20.0
21.0 10510621.120.0µg/L1,3-Dichloropropane 70-130 0.4 20.0
19.7 98.590.518.120.0µg/L2,2-Dichloropropane 70-130 8.4 20.0
22.2 11110520.920.0µg/L1,1-Dichloropropene 70-130 6.0 20.0
20.7 10410320.520.0µg/Lcis-1,3-Dichloropropene 70-130 0.9 20.0
21.6 10810521.020.0µg/Ltrans-1,3-Dichloropropene 70-130 2.8 20.0
506 10194.4472500µg/LEthanol 60-140 6.9 20.0
20.0 10095.519.120.0µg/LEthylbenzene 70-130 4.6 20.0
20.2 10197.019.420.0µg/LHexachlorobutadiene 70-130 4.0 20.0
19.7 98.593.018.620.0µg/L2-Hexanone 60-140 5.7 20.0
21.4 10710320.520.0µg/LIsopropylbenzene 70-130 4.2 20.0
21.1 10699.019.820.0µg/L4-Isopropyl toluene 70-130 6.3 20.0
17.9 89.585.517.120.0µg/LMethyl Ethyl Ketone (MEK)60-140 4.5 20.0
20.5 10310220.320.0µg/LMethyl tert-butyl ether (MTBE)70-130 0.9 20.0
20.3 10210521.020.0µg/L4-Methyl-2-Pentanone 60-140 3.3 20.0
20.0 10094.518.920.0µg/LMethylene Chloride 70-130 5.6 20.0
20.5 10310220.420.0µg/LNaphthalene 70-130 0.4 20.0
21.3 10710320.620.0µg/Ln-Propylbenzene 70-130 3.3 20.0
21.4 10710320.520.0µg/LStyrene 70-130 4.2 20.0
38.9 97.295.738.340.0µg/Ltert-Butyl Alcohol (TBA)40-140 1.5 20.0
41.5 10410943.440.0µg/Ltert-Butyl formate (TBF)40-140 4.4 20.0
Page 11 of 25Date:04/12/2023 05:12 PM
Page 124 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31717QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31715
LCS-V31715 LCSD-V31715Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.9 99.564.512.920.0µg/Ltert-Amyl Alcohol (TAA)40-140 42.6*20.0
42.7 10710843.040.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 0.7 20.0
21.8 10910320.620.0µg/L1,1,1,2-Tetrachloroethane 70-130 5.6 20.0
21.6 10810621.120.0µg/L1,1,2,2-Tetrachloroethane 70-130 2.3 20.0
20.6 10393.518.720.0µg/LTetrachloroethene 70-130 9.6 20.0
21.4 10710220.420.0µg/LToluene 70-130 4.7 20.0
21.7 10910320.620.0µg/L1,2,3-Trichlorobenzene 70-130 5.2 20.0
19.0 95.093.518.720.0µg/L1,2,4-Trichlorobenzene 70-130 1.5 20.0
20.3 10296.019.220.0µg/L1,1,1-Trichloroethane 70-130 5.5 20.0
22.3 11210921.720.0µg/L1,1,2-Trichloroethane 70-130 2.7 20.0
21.6 10897.019.420.0µg/LTrichloroethene 70-130 10.7 20.0
17.5 87.584.516.920.0µg/LTrichlorofluoromethane 60-140 3.4 20.0
21.0 10599.019.820.0µg/L1,2,3-Trichloropropane 70-130 5.8 20.0
21.0 10510120.220.0µg/L1,2,4-Trimethylbenzene 70-130 3.8 20.0
21.3 10710420.820.0µg/L1,3,5-Trimethylbenzene 70-130 2.3 20.0
22.4 11211823.520.0µg/LVinyl Acetate 60-140 4.7 20.0
19.6 98.090.018.020.0µg/LVinyl Chloride 60-140 8.5 20.0
20.3 10298.519.720.0µg/Lo-Xylene 70-130 3.0 20.0
43.1 10810441.440.0µg/Lm,p-Xylene 70-130 4.0 20.0
15.9 79.580.016.020.0µg/L3,3-Dimethyl-1-butanol 70-130 0.6 20.0
1031044-Bromofluorobenzene (S)70-130
95.298.2Dibromofluoromethane (S)70-130
93.692.21,2-Dichloroethane - d4 (S)70-130
98.498.6Toluene-d8 (S)70-130
Page 12 of 25* QC Fail Date:04/12/2023 05:12 PM
Page 125 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31761QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31760
Associated Lab Samples: 92533, 92536, 92539
LRB-V31760 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/06/23 15:5010.01.80<1.80µg/LAcetone
04/06/23 15:500.5000.180<0.180µg/LBenzene
04/06/23 15:500.5000.210<0.210µg/LBromobenzene
04/06/23 15:501.000.420<0.420µg/LBromochloromethane
04/06/23 15:500.5000.160<0.160µg/LBromodichloromethane
04/06/23 15:505.001.50<1.50µg/LBromoform
04/06/23 15:501.000.280<0.280µg/LBromomethane
04/06/23 15:500.5000.180<0.180µg/Ln-Butylbenzene
04/06/23 15:500.5000.200<0.200µg/Lsec-Butyl benzene
04/06/23 15:502.000.920<0.920µg/Ltert-Butyl benzene
04/06/23 15:500.5000.180<0.180µg/LCarbon Tetrachloride
04/06/23 15:500.5000.190<0.190µg/LChlorobenzene
04/06/23 15:500.5000.190<0.190µg/LChlorodibromomethane
04/06/23 15:501.000.430<0.430µg/LChloroethane
04/06/23 15:500.5000.220<0.220µg/LChloroform
04/06/23 15:500.5000.220<0.220µg/LChloromethane
04/06/23 15:500.5000.200<0.200µg/L2-Chlorotoluene
04/06/23 15:500.5000.200<0.200µg/L4-Chlorotoluene
04/06/23 15:500.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
04/06/23 15:502.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
04/06/23 15:500.5000.200<0.200µg/L1,2-Dibromoethane
04/06/23 15:500.5000.230<0.230µg/LDibromomethane
04/06/23 15:500.5000.220<0.220µg/L1,2-Dichlorobenzene
04/06/23 15:500.5000.190<0.190µg/L1,3-Dichlorobenzene
04/06/23 15:500.5000.210<0.210µg/L1,4-Dichlorobenzene
04/06/23 15:505.001.20<1.20µg/LDichlorodifluoromethane
04/06/23 15:500.5000.240<0.240µg/L1,1-Dichloroethane
Page 13 of 25Date:04/12/2023 05:12 PM
Page 126 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31761QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31760
Associated Lab Samples: 92533, 92536, 92539
LRB-V31760 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/06/23 15:500.5000.150<0.150µg/L1,2-Dichloroethane
04/06/23 15:500.5000.150<0.150µg/L1,1-Dichloroethene
04/06/23 15:500.5000.200<0.200µg/Lcis-1,2-Dichloroethene
04/06/23 15:500.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
04/06/23 15:500.5000.190<0.190µg/L1,2-Dichloropropane
04/06/23 15:500.5000.130<0.130µg/L1,3-Dichloropropane
04/06/23 15:502.000.210<0.210µg/L2,2-Dichloropropane
04/06/23 15:500.5000.200<0.200µg/L1,1-Dichloropropene
04/06/23 15:500.5000.210<0.210µg/Lcis-1,3-Dichloropropene
04/06/23 15:500.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
04/06/23 15:5020042.0<42.0µg/LEthanol
04/06/23 15:500.5000.170<0.170µg/LEthylbenzene
04/06/23 15:503.000.350<0.350µg/LHexachlorobutadiene
04/06/23 15:501.000.380<0.380µg/L2-Hexanone
04/06/23 15:500.5000.180<0.180µg/LIsopropylbenzene
04/06/23 15:500.5000.089<0.089µg/L4-Isopropyl toluene
04/06/23 15:505.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
04/06/23 15:501.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
04/06/23 15:501.000.078<0.078µg/L4-Methyl-2-Pentanone
04/06/23 15:502.000.330<0.330µg/LMethylene Chloride
04/06/23 15:501.000.470<0.470µg/LNaphthalene
04/06/23 15:500.5000.190<0.190µg/Ln-Propylbenzene
04/06/23 15:500.5000.220<0.220µg/LStyrene
04/06/23 15:5010.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
04/06/23 15:5010.00.350<0.350µg/Ltert-Butyl formate (TBF)
04/06/23 15:5010.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
04/06/23 15:5010.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 14 of 25Date:04/12/2023 05:12 PM
Page 127 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31761QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31760
Associated Lab Samples: 92533, 92536, 92539
LRB-V31760 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/06/23 15:500.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
04/06/23 15:500.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
04/06/23 15:500.5000.220<0.220µg/LTetrachloroethene
04/06/23 15:500.5000.220<0.220µg/LToluene
04/06/23 15:500.5000.380<0.380µg/L1,2,3-Trichlorobenzene
04/06/23 15:500.5000.310<0.310µg/L1,2,4-Trichlorobenzene
04/06/23 15:500.5000.160<0.160µg/L1,1,1-Trichloroethane
04/06/23 15:500.5000.096<0.096µg/L1,1,2-Trichloroethane
04/06/23 15:500.5000.180<0.180µg/LTrichloroethene
04/06/23 15:500.5000.180<0.180µg/LTrichlorofluoromethane
04/06/23 15:500.5000.270<0.270µg/L1,2,3-Trichloropropane
04/06/23 15:500.5000.190<0.190µg/L1,2,4-Trimethylbenzene
04/06/23 15:500.5000.180<0.180µg/L1,3,5-Trimethylbenzene
04/06/23 15:505.001.00<1.00µg/LVinyl Acetate
04/06/23 15:500.5000.170<0.170µg/LVinyl Chloride
04/06/23 15:500.5000.210<0.210µg/Lo-Xylene
04/06/23 15:501.000.420<0.420µg/Lm,p-Xylene
04/06/23 15:5010.01.00<1.00µg/L3,3-Dimethyl-1-butanol
04/06/23 15:504-Bromofluorobenzene (S)103 70-130
04/06/23 15:50Dibromofluoromethane (S)102 70-130
04/06/23 15:501,2-Dichloroethane - d4 (S)104 70-130
04/06/23 15:50Toluene-d8 (S)99.4 70-130
Page 15 of 25Date:04/12/2023 05:12 PM
Page 128 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31761QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31760
LCS-V31760 LCSD-V31760Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
35.9 89.782.533.040.0µg/LAcetone 40-160 8.4 20.0
19.8 99.010120.120.0µg/LBenzene 70-130 1.5 20.0
21.0 10510520.920.0µg/LBromobenzene 70-130 0.4 20.0
21.1 10610520.920.0µg/LBromochloromethane 70-130 0.9 20.0
20.1 10110220.320.0µg/LBromodichloromethane 70-130 0.9 20.0
23.9 12011823.520.0µg/LBromoform 70-130 1.6 20.0
23.1 11611523.020.0µg/LBromomethane 60-140 0.4 20.0
20.5 10310521.020.0µg/Ln-Butylbenzene 70-130 2.4 20.0
20.2 10110220.420.0µg/Lsec-Butyl benzene 70-130 0.9 20.0
20.5 10310220.320.0µg/Ltert-Butyl benzene 70-130 0.9 20.0
20.7 10410420.820.0µg/LCarbon Tetrachloride 70-130 0.4 20.0
20.1 10110420.720.0µg/LChlorobenzene 70-130 2.9 20.0
23.4 11711322.520.0µg/LChlorodibromomethane 70-130 3.9 20.0
20.7 10410621.220.0µg/LChloroethane 60-140 2.3 20.0
20.4 10210320.620.0µg/LChloroform 70-130 0.9 20.0
20.0 10010520.920.0µg/LChloromethane 60-140 4.4 20.0
20.2 10110220.320.0µg/L2-Chlorotoluene 70-130 0.4 20.0
20.5 10310320.520.0µg/L4-Chlorotoluene 70-130 0.0 20.0
19.4 97.098.019.620.0µg/LDi-Isopropyl Ether (DIPE)70-130 1.0 20.0
28.2 141*140*28.020.0µg/L1,2-Dibromo-3-Chloropropane 70-130 0.7 20.0
22.6 11311021.920.0µg/L1,2-Dibromoethane 70-130 3.1 20.0
21.5 10810521.020.0µg/LDibromomethane 70-130 2.3 20.0
21.2 10610420.720.0µg/L1,2-Dichlorobenzene 70-130 2.3 20.0
21.0 10510520.920.0µg/L1,3-Dichlorobenzene 70-130 0.4 20.0
20.3 10210420.720.0µg/L1,4-Dichlorobenzene 70-130 1.9 20.0
23.3 11712224.420.0µg/LDichlorodifluoromethane 60-140 4.6 20.0
Page 16 of 25* QC Fail Date:04/12/2023 05:12 PM
Page 129 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31761QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31760
LCS-V31760 LCSD-V31760Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.0 10010120.220.0µg/L1,1-Dichloroethane 70-130 0.9 20.0
21.6 10810721.320.0µg/L1,2-Dichloroethane 70-130 1.3 20.0
22.6 11311122.220.0µg/L1,1-Dichloroethene 70-130 1.7 20.0
19.5 97.597.519.520.0µg/Lcis-1,2-Dichloroethene 70-130 0.0 20.0
19.9 99.510020.020.0µg/Ltrans-1,2-Dichloroethene 70-130 0.5 20.0
19.3 96.597.019.420.0µg/L1,2-Dichloropropane 70-130 0.5 20.0
21.2 10610621.220.0µg/L1,3-Dichloropropane 70-130 0.0 20.0
19.8 99.098.019.620.0µg/L2,2-Dichloropropane 70-130 1.0 20.0
20.7 10410320.620.0µg/L1,1-Dichloropropene 70-130 0.4 20.0
21.0 10510420.820.0µg/Lcis-1,3-Dichloropropene 70-130 0.9 20.0
21.8 10910921.720.0µg/Ltrans-1,3-Dichloropropene 70-130 0.4 20.0
743 149*132662500µg/LEthanol 60-140 11.5 20.0
20.1 10110120.220.0µg/LEthylbenzene 70-130 0.4 20.0
23.1 11611723.420.0µg/LHexachlorobutadiene 70-130 1.2 20.0
25.5 12811823.620.0µg/L2-Hexanone 60-140 7.7 20.0
20.8 10410521.020.0µg/LIsopropylbenzene 70-130 0.9 20.0
20.6 10310420.820.0µg/L4-Isopropyl toluene 70-130 0.9 20.0
23.3 11710821.620.0µg/LMethyl Ethyl Ketone (MEK)60-140 7.5 20.0
23.2 11611222.320.0µg/LMethyl tert-butyl ether (MTBE)70-130 3.9 20.0
25.1 12611623.220.0µg/L4-Methyl-2-Pentanone 60-140 7.8 20.0
18.5 92.593.518.720.0µg/LMethylene Chloride 70-130 1.0 20.0
25.7 12912825.520.0µg/LNaphthalene 70-130 0.7 20.0
19.8 99.010220.320.0µg/Ln-Propylbenzene 70-130 2.4 20.0
21.2 10610420.720.0µg/LStyrene 70-130 2.3 20.0
51.1 12813453.740.0µg/Ltert-Butyl Alcohol (TBA)40-140 4.9 20.0
46.4 11611545.840.0µg/Ltert-Butyl formate (TBF)40-140 1.3 20.0
Page 17 of 25* QC Fail Date:04/12/2023 05:12 PM
Page 130 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31761QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31760
LCS-V31760 LCSD-V31760Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
24.5 12312525.020.0µg/Ltert-Amyl Alcohol (TAA)40-140 2.0 20.0
44.9 11211044.140.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 1.7 20.0
22.5 11310921.820.0µg/L1,1,1,2-Tetrachloroethane 70-130 3.1 20.0
23.6 11811723.420.0µg/L1,1,2,2-Tetrachloroethane 70-130 0.8 20.0
20.8 10410621.220.0µg/LTetrachloroethene 70-130 1.9 20.0
20.3 10210320.520.0µg/LToluene 70-130 0.9 20.0
27.3 137*140*27.920.0µg/L1,2,3-Trichlorobenzene 70-130 2.1 20.0
26.2 131*131*26.120.0µg/L1,2,4-Trichlorobenzene 70-130 0.3 20.0
20.2 10110320.520.0µg/L1,1,1-Trichloroethane 70-130 1.4 20.0
22.8 11411222.420.0µg/L1,1,2-Trichloroethane 70-130 1.7 20.0
19.7 98.510220.420.0µg/LTrichloroethene 70-130 3.4 20.0
22.7 11410821.520.0µg/LTrichlorofluoromethane 60-140 5.4 20.0
23.9 12011723.320.0µg/L1,2,3-Trichloropropane 70-130 2.5 20.0
21.0 10510520.920.0µg/L1,2,4-Trimethylbenzene 70-130 0.4 20.0
20.8 10410420.720.0µg/L1,3,5-Trimethylbenzene 70-130 0.4 20.0
23.6 11812023.920.0µg/LVinyl Acetate 60-140 1.2 20.0
22.9 11511322.520.0µg/LVinyl Chloride 60-140 1.7 20.0
20.4 10210520.920.0µg/Lo-Xylene 70-130 2.4 20.0
42.7 10710642.540.0µg/Lm,p-Xylene 70-130 0.4 20.0
36.7 184*176*35.220.0µg/L3,3-Dimethyl-1-butanol 70-130 4.1 20.0
1001024-Bromofluorobenzene (S)70-130
102101Dibromofluoromethane (S)70-130
1081071,2-Dichloroethane - d4 (S)70-130
100100Toluene-d8 (S)70-130
Page 18 of 25* QC Fail Date:04/12/2023 05:12 PM
Page 131 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31866QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31860
Associated Lab Samples: 92522, 92523, 92524, 92526, 92530, 92531, 92532, 92534, 92538, 92540
LRB-V31860 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/10/23 22:2710.01.80<1.80µg/LAcetone
04/10/23 22:270.5000.180<0.180µg/LBenzene
04/10/23 22:270.5000.210<0.210µg/LBromobenzene
04/10/23 22:271.000.420<0.420µg/LBromochloromethane
04/10/23 22:270.5000.160<0.160µg/LBromodichloromethane
04/10/23 22:275.001.50<1.50µg/LBromoform
04/10/23 22:271.000.280<0.280µg/LBromomethane
04/10/23 22:270.5000.180<0.180µg/Ln-Butylbenzene
04/10/23 22:270.5000.200<0.200µg/Lsec-Butyl benzene
04/10/23 22:272.000.920<0.920µg/Ltert-Butyl benzene
04/10/23 22:270.5000.180<0.180µg/LCarbon Tetrachloride
04/10/23 22:270.5000.190<0.190µg/LChlorobenzene
04/10/23 22:270.5000.190<0.190µg/LChlorodibromomethane
04/10/23 22:271.000.430<0.430µg/LChloroethane
04/10/23 22:270.5000.220<0.220µg/LChloroform
04/10/23 22:270.5000.220<0.220µg/LChloromethane
04/10/23 22:270.5000.200<0.200µg/L2-Chlorotoluene
04/10/23 22:270.5000.200<0.200µg/L4-Chlorotoluene
04/10/23 22:270.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
04/10/23 22:272.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
04/10/23 22:270.5000.200<0.200µg/L1,2-Dibromoethane
04/10/23 22:270.5000.230<0.230µg/LDibromomethane
04/10/23 22:270.5000.220<0.220µg/L1,2-Dichlorobenzene
04/10/23 22:270.5000.190<0.190µg/L1,3-Dichlorobenzene
04/10/23 22:270.5000.210<0.210µg/L1,4-Dichlorobenzene
04/10/23 22:275.001.20<1.20µg/LDichlorodifluoromethane
04/10/23 22:270.5000.240<0.240µg/L1,1-Dichloroethane
Page 19 of 25Date:04/12/2023 05:12 PM
Page 132 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31866QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31860
Associated Lab Samples: 92522, 92523, 92524, 92526, 92530, 92531, 92532, 92534, 92538, 92540
LRB-V31860 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/10/23 22:270.5000.150<0.150µg/L1,2-Dichloroethane
04/10/23 22:270.5000.150<0.150µg/L1,1-Dichloroethene
04/10/23 22:270.5000.200<0.200µg/Lcis-1,2-Dichloroethene
04/10/23 22:270.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
04/10/23 22:270.5000.190<0.190µg/L1,2-Dichloropropane
04/10/23 22:270.5000.130<0.130µg/L1,3-Dichloropropane
04/10/23 22:272.000.210<0.210µg/L2,2-Dichloropropane
04/10/23 22:270.5000.200<0.200µg/L1,1-Dichloropropene
04/10/23 22:270.5000.210<0.210µg/Lcis-1,3-Dichloropropene
04/10/23 22:270.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
04/10/23 22:2720042.0<42.0µg/LEthanol
04/10/23 22:270.5000.170<0.170µg/LEthylbenzene
04/10/23 22:273.000.350<0.350µg/LHexachlorobutadiene
04/10/23 22:271.000.380<0.380µg/L2-Hexanone
04/10/23 22:270.5000.180<0.180µg/LIsopropylbenzene
04/10/23 22:270.5000.089<0.089µg/L4-Isopropyl toluene
04/10/23 22:275.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
04/10/23 22:271.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
04/10/23 22:271.000.078<0.078µg/L4-Methyl-2-Pentanone
04/10/23 22:272.000.330<0.330µg/LMethylene Chloride
04/10/23 22:271.000.470<0.470µg/LNaphthalene
04/10/23 22:270.5000.190<0.190µg/Ln-Propylbenzene
04/10/23 22:270.5000.220<0.220µg/LStyrene
04/10/23 22:2710.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
04/10/23 22:2710.00.350<0.350µg/Ltert-Butyl formate (TBF)
04/10/23 22:2710.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
04/10/23 22:2710.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 20 of 25Date:04/12/2023 05:12 PM
Page 133 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31866QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31860
Associated Lab Samples: 92522, 92523, 92524, 92526, 92530, 92531, 92532, 92534, 92538, 92540
LRB-V31860 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/10/23 22:270.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
04/10/23 22:270.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
04/10/23 22:270.5000.220<0.220µg/LTetrachloroethene
04/10/23 22:270.5000.220<0.220µg/LToluene
04/10/23 22:270.5000.380<0.380µg/L1,2,3-Trichlorobenzene
04/10/23 22:270.5000.310<0.310µg/L1,2,4-Trichlorobenzene
04/10/23 22:270.5000.160<0.160µg/L1,1,1-Trichloroethane
04/10/23 22:270.5000.096<0.096µg/L1,1,2-Trichloroethane
04/10/23 22:270.5000.180<0.180µg/LTrichloroethene
04/10/23 22:270.5000.180<0.180µg/LTrichlorofluoromethane
04/10/23 22:270.5000.270<0.270µg/L1,2,3-Trichloropropane
04/10/23 22:270.5000.190<0.190µg/L1,2,4-Trimethylbenzene
04/10/23 22:270.5000.180<0.180µg/L1,3,5-Trimethylbenzene
04/10/23 22:275.001.00<1.00µg/LVinyl Acetate
04/10/23 22:270.5000.170<0.170µg/LVinyl Chloride
04/10/23 22:270.5000.210<0.210µg/Lo-Xylene
04/10/23 22:271.000.420<0.420µg/Lm,p-Xylene
04/10/23 22:2710.01.00<1.00µg/L3,3-Dimethyl-1-butanol
04/10/23 22:274-Bromofluorobenzene (S)103 70-130
04/10/23 22:27Dibromofluoromethane (S)101 70-130
04/10/23 22:271,2-Dichloroethane - d4 (S)99.2 70-130
04/10/23 22:27Toluene-d8 (S)100 70-130
Page 21 of 25Date:04/12/2023 05:12 PM
Page 134 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31866QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31860
LCS-V31860 LCSD-V31860Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
30.6 76.571.228.540.0µg/LAcetone 40-160 7.1 20.0
20.5 10399.519.920.0µg/LBenzene 70-130 2.9 20.0
21.2 10610320.520.0µg/LBromobenzene 70-130 3.3 20.0
21.3 10710020.020.0µg/LBromochloromethane 70-130 6.2 20.0
20.2 10198.519.720.0µg/LBromodichloromethane 70-130 2.5 20.0
21.0 10599.519.920.0µg/LBromoform 70-130 5.3 20.0
21.9 11010520.920.0µg/LBromomethane 60-140 4.6 20.0
21.1 10698.519.720.0µg/Ln-Butylbenzene 70-130 6.8 20.0
20.4 10296.019.220.0µg/Lsec-Butyl benzene 70-130 6.0 20.0
20.6 10396.019.220.0µg/Ltert-Butyl benzene 70-130 7.0 20.0
20.6 10397.019.420.0µg/LCarbon Tetrachloride 70-130 6.0 20.0
21.2 10610220.420.0µg/LChlorobenzene 70-130 3.8 20.0
21.0 10510120.120.0µg/LChlorodibromomethane 70-130 4.3 20.0
20.7 10498.519.720.0µg/LChloroethane 60-140 4.9 20.0
20.7 10410020.020.0µg/LChloroform 70-130 3.4 20.0
21.1 10698.019.620.0µg/LChloromethane 60-140 7.3 20.0
20.3 10298.519.720.0µg/L2-Chlorotoluene 70-130 3.0 20.0
20.5 10398.519.720.0µg/L4-Chlorotoluene 70-130 3.9 20.0
20.0 10096.019.220.0µg/LDi-Isopropyl Ether (DIPE)70-130 4.0 20.0
23.5 11810521.020.0µg/L1,2-Dibromo-3-Chloropropane 70-130 11.2 20.0
20.7 10497.019.420.0µg/L1,2-Dibromoethane 70-130 6.4 20.0
20.7 10496.519.320.0µg/LDibromomethane 70-130 7.0 20.0
21.1 10610220.420.0µg/L1,2-Dichlorobenzene 70-130 3.3 20.0
20.4 10210120.220.0µg/L1,3-Dichlorobenzene 70-130 0.9 20.0
20.6 10399.019.820.0µg/L1,4-Dichlorobenzene 70-130 3.9 20.0
19.0 95.089.017.820.0µg/LDichlorodifluoromethane 60-140 6.5 20.0
Page 22 of 25Date:04/12/2023 05:12 PM
Page 135 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31866QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31860
LCS-V31860 LCSD-V31860Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.0 10510220.320.0µg/L1,1-Dichloroethane 70-130 3.3 20.0
19.8 99.096.019.220.0µg/L1,2-Dichloroethane 70-130 3.0 20.0
21.0 10510020.020.0µg/L1,1-Dichloroethene 70-130 4.8 20.0
20.3 10299.019.820.0µg/Lcis-1,2-Dichloroethene 70-130 2.4 20.0
20.4 10293.518.720.0µg/Ltrans-1,2-Dichloroethene 70-130 8.6 20.0
20.4 10298.519.720.0µg/L1,2-Dichloropropane 70-130 3.4 20.0
20.6 10399.519.920.0µg/L1,3-Dichloropropane 70-130 3.4 20.0
21.6 10896.019.220.0µg/L2,2-Dichloropropane 70-130 11.7 20.0
21.9 11099.019.820.0µg/L1,1-Dichloropropene 70-130 10.0 20.0
20.3 10299.519.920.0µg/Lcis-1,3-Dichloropropene 70-130 1.9 20.0
20.9 10598.019.620.0µg/Ltrans-1,3-Dichloropropene 70-130 6.4 20.0
484 96.886.8434500µg/LEthanol 60-140 10.8 20.0
20.2 10197.019.420.0µg/LEthylbenzene 70-130 4.0 20.0
21.3 10797.019.420.0µg/LHexachlorobutadiene 70-130 9.3 20.0
21.0 10590.518.120.0µg/L2-Hexanone 60-140 14.8 20.0
20.8 10499.519.920.0µg/LIsopropylbenzene 70-130 4.4 20.0
21.3 10710220.420.0µg/L4-Isopropyl toluene 70-130 4.3 20.0
17.8 89.078.515.720.0µg/LMethyl Ethyl Ketone (MEK)60-140 12.5 20.0
20.7 10410020.020.0µg/LMethyl tert-butyl ether (MTBE)70-130 3.4 20.0
20.2 10197.019.420.0µg/L4-Methyl-2-Pentanone 60-140 4.0 20.0
20.1 10196.519.320.0µg/LMethylene Chloride 70-130 4.0 20.0
21.4 10710120.220.0µg/LNaphthalene 70-130 5.7 20.0
20.7 10497.519.520.0µg/Ln-Propylbenzene 70-130 5.9 20.0
20.4 10210120.120.0µg/LStyrene 70-130 1.4 20.0
46.2 11610140.540.0µg/Ltert-Butyl Alcohol (TBA)40-140 13.1 20.0
40.8 10210240.640.0µg/Ltert-Butyl formate (TBF)40-140 0.4 20.0
Page 23 of 25Date:04/12/2023 05:12 PM
Page 136 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31866QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31860
LCS-V31860 LCSD-V31860Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.8 10496.519.320.0µg/Ltert-Amyl Alcohol (TAA)40-140 7.4 20.0
41.7 10499.739.940.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 4.4 20.0
20.7 10410220.420.0µg/L1,1,1,2-Tetrachloroethane 70-130 1.4 20.0
20.7 10499.019.820.0µg/L1,1,2,2-Tetrachloroethane 70-130 4.4 20.0
20.6 10397.019.420.0µg/LTetrachloroethene 70-130 6.0 20.0
20.4 10297.519.520.0µg/LToluene 70-130 4.5 20.0
22.7 11410821.520.0µg/L1,2,3-Trichlorobenzene 70-130 5.4 20.0
23.3 11710721.420.0µg/L1,2,4-Trichlorobenzene 70-130 8.5 20.0
21.1 10610220.320.0µg/L1,1,1-Trichloroethane 70-130 3.8 20.0
19.5 97.596.019.220.0µg/L1,1,2-Trichloroethane 70-130 1.5 20.0
20.8 10497.019.420.0µg/LTrichloroethene 70-130 6.9 20.0
20.2 10194.518.920.0µg/LTrichlorofluoromethane 60-140 6.6 20.0
21.4 10790.518.120.0µg/L1,2,3-Trichloropropane 70-130 16.7 20.0
20.6 10399.019.820.0µg/L1,2,4-Trimethylbenzene 70-130 3.9 20.0
21.0 10510220.320.0µg/L1,3,5-Trimethylbenzene 70-130 3.3 20.0
20.5 10310220.320.0µg/LVinyl Acetate 60-140 0.9 20.0
20.6 10397.519.520.0µg/LVinyl Chloride 60-140 5.4 20.0
20.3 10298.019.620.0µg/Lo-Xylene 70-130 3.5 20.0
41.7 10499.239.740.0µg/Lm,p-Xylene 70-130 4.9 20.0
19.6 98.080.016.020.0µg/L3,3-Dimethyl-1-butanol 70-130 20.2*20.0
99.499.04-Bromofluorobenzene (S)70-130
10299.2Dibromofluoromethane (S)70-130
1021001,2-Dichloroethane - d4 (S)70-130
101101Toluene-d8 (S)70-130
Page 24 of 25* QC Fail Date:04/12/2023 05:12 PM
Page 137 of 142
Quality Control Data
23-088-0022Report No:
Project Description:
Client ID:Geological Resources, Inc.
Stone's Fast Save
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V31920QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V31919
Associated Lab Samples: 92540
LRB-V31919 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/12/23 01:460.5000.220<0.220µg/LToluene
04/12/23 01:464-Bromofluorobenzene (S)103 70-130
04/12/23 01:46Dibromofluoromethane (S)100 70-130
04/12/23 01:461,2-Dichloroethane - d4 (S)93.6 70-130
04/12/23 01:46Toluene-d8 (S)101 70-130
LCS-V31919 LCSD-V31919Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.0 10010020.020.0µg/LToluene 70-130 0.0 20.0
10199.04-Bromofluorobenzene (S)70-130
97.8101Dibromofluoromethane (S)70-130
98.097.81,2-Dichloroethane - d4 (S)70-130
100101Toluene-d8 (S)70-130
Page 25 of 25Date:04/12/2023 05:12 PM
Page 138 of 142
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-088-0022
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 1.6C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Danyale Love Date & Time:03/29/2023 15:29:36
Special precautions or instructions included?
Comments:
Page 139 of 142
Page 140 of 142
Page 141 of 142
Page 142 of 142

APPENDIX D
Contaminant Mass Calculations

Area ID Well ID Area
(ft²)
Average Well
Depth
(ft.)
Average
Depth to
Water
(ft.)
Water
Column
Height
(ft)
Volume
(ft³)
Volume
(L)
Effective
Porosity
Effective
Volume
(L)
MW-1
MW-4
MW-5
MW-13
Area Date Well Benzene
(μ/L)
Toluene
(μ/L)
Ethylbenzene
(μ/L)
Xylenes
(μ/L)
MTBE
(μ/L)
Naphthalene
(μ/L)
Total
(μ/L)
DTW
(ft.)
Average Water
Column Height
(ft.)
Total Average Mass
(g)Percent Red. To Date Red.
MW-1 4,900 2,370 914 4,090 1,530 731 14535.00 7.92
MW-4 1,780 534 2,520 5,310 343 1,700 12187.00 7.56
MW-5 5,000 260,000 84,500 85,500 20,000 6,000 461000.00 7.23
MW-13 10,500 15,600 2,350 13,100 4,110 1,070 46730.00 7.54
Avg. 5545.00 69626.00 22571.00 27000.00 6495.75 2375.25 133613.00 7.56
MW-1 1,310 1,020 434 1,220 1,750 253 5987.00 10.74
MW-4 908 130 1,900 2,320 557 1,530 7345.00 10.38
MW-5 5,000 260,000 84,500 85,500 20,000 6,000 461000.00 11.05
MW-13 7,710 8,780 1,560 5,620 5,680 667 30017.00 10.35
Avg. 3732.00 67482.50 22098.50 23665.00 6996.75 2112.50 126087.25 10.63
MW-1 5,100 1,180 2,350 2,880 3,730 698 15938.00 8.59
MW-4 1,400 163 2,530 3,130 177 1,330 8730.00 8.26
MW-5 5,000 260,000 84,500 85,500 20,000 6,000 461000.00 8.72
MW-13 11,000 14,400 1,830 9,660 6,940 572 44402.00 8.24
Avg. 5625.00 68935.75 22802.50 25292.50 7711.75 2150.00 132517.50 8.45
MW-1 3,590 2,740 1,050 2,020 6,600 485 16485.00 7.17
MW-4 898 108 3,190 4,450 95.9 2,380 11121.90 6.65
MW-5 5,000 260,000 84,500 85,500 20,000 6,000 461000.00 8.43
MW-13 5,020 7,880 1,690 8,030 1,420 930 24970.00 6.87
Avg. 3627.00 67682.00 22607.50 25000.00 7028.98 2448.75 128394.23 7.28
MW-1 3,370 2,350 531 1,110 3,570 310 11241.00 12.90
MW-4 5,000 260,000 84,500 85,500 20,000 6,000 461000.00 12.63
MW-5 5,000 260,000 84,500 85,500 20,000 6,000 461000.00 12.86
MW-13 3,480 2,900 952 2,690 583 429 11034.00 12.53
Avg. 4212.50 131312.50 42620.75 43700.00 11038.25 3184.75 236068.75 12.73
MW-1 4,900 192 3,460 760 2,230 1,480 13022.00 7.36
MW-4 474 71.2 2,140 1,830 0 1,500 6015.20 6.97
MW-5 5,000 260,000 84,500 85,500 20,000 6,000 461000.00 6.70
MW-13 6,220 10,400 2,130 10,600 449 1,140 30939.00 7.01
Avg. 4148.50 67665.80 23057.50 24672.50 5669.75 2530.00 127744.05 7.01
MW-1 3,960 109 3,330 236 1,110 1,190 9935.00 8.81
MW-4 884 94.7 1,560 1,690 265 1,540 6033.70 7.81
MW-5 8,260 11,400 2,270 9,010 3,240 854 34180.00 7.44
MW-13 5,000 260,000 80,000 50,000 20000 6,000 421000.00 7.65
Avg. 4526.00 67900.93 21790.00 15234.00 6153.75 2396.00 117787.18 7.93
Date
Average Water
Column Height
(ft.)
01/14/13 10.94
12/02/13 7.87
06/09/14 10.05
10/24/16 11.22
11/06/19 5.77
12/23/20 11.49
03/28/23 10.57
Notes:
• FP: Free Product
• Area of the contaminant plume is calculated from Figure # 14
• Height of the water column is calculated by subtracting the average depth to water from the average well depth of the referenced monitoring wells
• Volume of the contaminant plume is calculated by multiplying the area of the plume by the average height of the water column during each sampling event
• Effective porosity is assumed based on the sub-surface soil profile obtained from well construction records and soil boring logs
• Total mass was calculated by multiplying the total contaminant concentrations for the sampling event with effective volume
• Contaminant mass cannot be calculated in wells containing FP; therefore, the GCLs were used for calculating the contaminant mass
• When areas couldn’t be sampled, the last known concentrations were used in the calculations.
03/28/23 10.57 13,752.59 15.2% 14.8%
Baseline Event
1 1,950.0 18.5 7.56 10.94 21,333 604,082 0.20 120,816
01/14/13
06/09/14
11/06/19
16,138.96
14,704.15
15,042.61
10.05
Area 1
--- ---
12/02/13 7.87 10,958.59 32.1% 32.1%
10.94
-34.2%8.9%
10/24/16 11.22 15,909.16 -8.2%1.4%
5.4% 6.8%
12/23/20 11.49 16,209.50 -7.8% -0.4%
5.77
Total Contaminant Mass
(g)
Percent Reduction Compared
to Previous Event Percent Reduction To Date
16,138.96 --- ---
10,958.59 32.1% 32.1%
14,704.15 -34.2%8.9%
15,909.16 -8.2%1.4%
15,042.61 5.4% 6.8%
13,752.59 15.2%14.8%
16,209.50 -7.8% -0.4%
APPENDIX D
MASS CALCULATIONS
STONE'S FAST SAVE (INCIDENT NO. 29035)