AS-29559_48692_CA_MRP_20230607

GROUNDWATER MONITORING
REPORT

For The FCE-1426
5445 Asheville Highway Hendersonville, North Carolina 28791 Facility ID 00-0-0000036632

PROJECT # SEI-1332

PREPARED FOR: Southeast Energy, LLC. 7014 A.C. Skinner Parkway, Ste 290 Jacksonville, FL 23356
PREPARED BY:
Singleton Environmental, Inc.
PO Box 604
Fletcher, NC 28732
[phone] February 24, 2023

Singleton Environmental, Inc

GROUNDWATER MONITORING REPORT
June 7, 2023 Site Name: FCE-1426 5445 Asheville Highway Hendersonville, NC 28791
Incident Number: 48692 Facility ID Number: 00-0-0000036632 UST Responsible Party: First Coast Energy, LLC. Attn: Kevin Kusmerik 7014 A.C. Skinner Parkway, Ste 290
Jacksonville, FL 23356 Telephone: [phone] Consultant / Contractor: Singleton Environmental, Inc.
PO Box 2012
Enka, NC 28728 Telephone: [phone] Date Release Discovered: September 23, 2022
Estimated Quantity of Release: Unknown/unquantified Cause/Source of Release: Regular UST #2 Spill Bucket.

Latitude: 35.3950° North
Longitude: -82.5055° West
Signature and Seal of Certifying Professional Engineer: I, Christopher D. Singleton, a Professional Geologist, do certify that the information contained in this report is correct and accurate to the best of my knowledge.

____________________________________
Christopher D. Singleton, P.G. #1928 Singleton Environmental, Inc. is licensed to practice geology in North Carolina. The corporate license number is C-443.

Table of Contents
Introduction ................................................................................................................................1
Site History…......................…………......................................... .................................................1 Initial Abatement Activities…......................…………......................................... .........................1 Risk Characterization…......................…………......................................... ..................................2 Receptor Information…......................…………......................................... ..................................2
Site Geology and Hydrogeology…......................…………......................................... ..................2
Sampling Results…......................…………......................................... .........................................3
Soil……………………………………………………………………………………………3 Groundwater …......................…………......................................... ........................................4 Conclusions & Recommendations…..................…………......................................... ...................4 Tables Table 1. Soil Analytical Table 2. Groundwater Analytical
Table 3. Monitoring Well Data Figures Figure 1. USGS Topo Map
Figure 2. Site Map Figure 3. Groundwater Map Figure 4. Water Supply Wells Figure 5. Groundwater Concentrations Appendices
Appendix A: Field Notes Appendix B: Laboratory Analytical Reports and Chain-of-Custody Documentation

Introduction This report presents the results of the May 2023 Groundwater Monitoring (GMR) event conducted for the FCE-1426 located at 5445 Asheville Highway in Hendersonville, North Carolina. This GMR was required by the North Carolina Department of Environment Quality
(NCDEQ). The location of the site is indicated on a USGS topographic map in Figure 1. Figure
2 presents a site map that shows the sample locations. Site History The following table summarizes information about the USTs at the site:

Tank No. Volume (gallons)
Contents (i.e., gasoline, diesel, kerosene,
heating oil,
Use (resale, heating building, distribution, farm or residential, etc.)
Date last used
Indicate whether UST has been removed or closed in place
Date of permanent closure
(if applicable)
Was a release detected from this UST system? If yes, give date.
Ownership of Tank: First Coast Energy, LLC. Attn: Kevin Kusmerik 7014 A.C. Skinner Parkway, Ste 290
Jacksonville, FL 23356
Telephone: [phone] Initial Abatement Activities A Site Check was completed on September 27, 2022, by Singleton Environmental, Inc. (SEI). The Site Check discovered elevated benzene and naphthalene in the groundwater at SB-1 near
the regular #2 spill bucket in Figure 2. Mr. Kevin Kusmerik with Southeast Energy, LLC.
contracted SEI to complete the Phase II Limited Site Assessment required by NCDEQ.
On November 7, 2022, SEI mobilized to the site to install a monitoring well at the SB-1 location. A soil and groundwater sample from the SB-1 location were collected and submitted for risk-based analysis.

On January 10, 2023, SEI mobilized to the site to install three additional monitoring wells (MW-2, MW-3, and MW-4). Soil and groundwater samples were collected from each location. On May 12, 2023, SEI mobilized to the site to collect groundwater samples from the four
monitoring wells and a stream sample from the adjacent tributary to Mud Creek. Risk Characterization
Based on these risk classification guidelines, the property meets the criteria for high risk due to the benzene and toluene exceeding 10 times (10 X) the NCAC 2B surface water standards. Receptor Information
SEI personnel completed a water supply well survey near the site on November 8, 2022, by
searching surrounding properties for wells and water meter connections within 1,500 feet of the site. The following bullets summarize other receptor information regarding this site:

• Public water supply is available in the vicinity of the site from municipal water supplies.
• The site is not located in a wellhead protection area.
• Two water supply wells are located within 1,500 feet from the source area. They are located over 900 feet to the northwest and upgradient from the site (Figure 3).
• Mud Creek is located approximately 1,800 feet to the southwest. A seasonal creek borders the eastern property boundary at the site. The property containing the release is zoned commercial. The surrounding properties contain
commercial and residential development. Site Geology and Hydrogeology
According to the Geologic Map of North Carolina (1985), the local geology consists of Henderson Gneiss which is located to the southeast of the Brevard Fault Zone inside the Chauga Belt. A soil boring log is included in Appendix B. On November 7, 2022, monitoring well MW-1 was advanced to a depth of 15 feet. On January 10, 2023, monitoring wells MW-2, MW-3,
and MW-4 were advanced to depths of 15 feet. Each monitoring well was installed with 10 feet of PVC screen and 5 feet of solid PVC riser. The depths to groundwater on January 11, 2023, ranged from 4.78 ft/bgs in MW-1 to 7.63 ft/bgs in MW-2. On January 11, 2023, all monitoring wells were surveyed to determine the groundwater flow direction at the site. Groundwater flows
to the south-southwest from the source area toward Mud Creek (Figure 3).

Sampling Results Soil On November 7, 2022, SEI collected additional samples from the SB-1 location at a depth of 5.5
ft-bgs just above the groundwater surface. Soil sample MW-1-Soil was submitted for laboratory
analysis of volatile organic compounds (VOCs) by EPA Method 8260 and volatile petroleum hydrocarbons (VPH) by MADEP method. Analytical results from MW-1-Soil detected concentrations of benzene and naphthalene above the soil-to-groundwater MSCCs. None of the compounds detected exceeded the residential or
commercial MSCCs. On January 10, 2023, SEI collected soil samples during the installation of monitoring wells MW-2, MW-3, and MW-4 at depths ranging from 5.0 ft/bgs to 6.0 ft/bgs just above the groundwater
surface. Soil samples MW-2-Soil, MW-3-Soil, and MW-4-Soil were submitted for laboratory
analysis of VOCs by EPA Method 8260 and VPH by MADEP method. Analytical results from soil sample MW-2-Soil detected concentrations of benzene and naphthalene above the soil-to-groundwater MSCCs. None of the compounds detected exceeded the residential or commercial MSCCs.
Analytical results from soil samples MW-3-Soil and MW-4-Soil did not detect any concentrations exceeding the soil-to-groundwater MSCCs.
Refer to Table 1 for a summary of the concentration levels. Groundwater On November 7, 2022, monitoring well MW-1 was installed in the location of SB-1 in the Site Check Report. MW-1 was installed to a depth of 15 ft-bgs. On November 8, 2022, a sample
was collected and submitted for laboratory analysis of volatile organic compounds (VOCs) by EPA Method 6200B. Analytical results from MW-1 detected concentrations of benzene, naphthalene, and total
xylenes exceeding the NCAC 2L MSCCs. None of the compounds detected exceeded the gross
contamination MSCCs.
On January 10, 2023, monitoring wells MW-2, MW-3, and MW-4 were installed at the site. Monitoring wells MW-2 and MW-4 were installed in the assumed downgradient location and MW-3 was installed in the assumed upgradient location. All three monitoring wells were
installed to a depth of 15 ft-bgs. On January 11, 2023, a sample was collected from monitoring wells MW-1 through MW-4 and submitted for laboratory analysis of VOCs by EPA Method 6200B and VPH by MADEP Method.

Each monitoring well sample was collected using a new clear PVC bailer after three well volumes were purged, and the wells had almost recharged.

On February 9, 2023, SEI collected a surface water sample (SW-1) from the seasonal stream
bordering the southeastern side of the property. The sample was analyzed for VOCs by EPA Method 6200B and VPH by MADEP Method. Analytical results from SW-1 did not detect any concentrations above the minimum laboratory
detection levels. On May 12, 2023, SEI collected groundwater samples from monitoring wells MW-1 through MW-4. Each monitoring well sample was collected using a new clear PVC bailer after three well
volumes were purged, and the wells had almost recharged (Field Notes are in Appendix A). A
surface water sample was also collected from the Mud Creek tributary. The samples were analyzed for VOCs by EPA Method 6200B. Laboratory analysis detected concentrations exceeding the NCAC 2L and NCAC 10 X 2B
standards in MW-1, MW-2, and MW-4. None of the compounds detected exceeded the NCAC 2L gross concentrations. Laboratory analysis did not detect any compounds above the NCAC 2L or 10 X 2B standards in MW-3.

Laboratory analysis did not detect any compounds exceeding the NCAC 2B surface water standards in SW-1. Refer to Table 2 for a summary of the groundwater and surface water concentration levels.
Conclusions and Recommendations

The results of this investigation indicate the soil and groundwater located at the FCE-1426
located at 5445 Asheville Highway in Hendersonville, North Carolina, contains compounds in the soil exceeding the soil-to-groundwater MSCCs and groundwater exceeding the NCAC 2L MSCCs and 10 x 2B surface water standards; however, none of the compounds exceed the residential or gross MSCCs.
The concentration levels in monitoring wells MW-1, MW-2, and MW-4 all increased during the last quarter. Concentrations were detected in surface water sample SW-1; however, they were below the 2B surface water standards.

Based on the information provided in this Groundwater Monitoring Report, NCDEQ will
determine the next course of action at the site.

TABLES
Aliphati
c (C5-
C8)
Apliphat
ic (C9-
C12)
Aromati
c (C9-
C10)
1,2,4-
Trimeth
ylbenze
ne
1,3,5-
Trimeth
ylbenze
ne
Benzen
e
Chlorof
orm
Ethylbe
nzene
Isoprop
ylbenze
ne
(Cumen
e)
Naphth
alene Toluene Xylene
(Total)
n-
Butylbe
nzene
n-
Propylb
enzene
p-
Isoprop
yltoluen
e
Collected Depth (ppm)mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
MW-1-Soil 11/7/2022 5.5 281 N/A N/A N/A 0.16 0.11 0.1 ND 0.25 0.047 0.23 0.017 0.14 0.079 0.079 ND
MW-2-SOIL 01/10/2023 41 20 17 1.8 0.61 0.33 ND 2.8 0.35 1.6 0.040 2.8 ND 1.2 ND
MW-3-SOIL 01/10/2023 ND ND ND ND ND ND 0.012 ND ND ND ND ND ND ND ND
MW-4-SOIL 01/10/2023 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.032
68 540 31 8.5 8.3 0.0056 0.37 4.9 1.7 0.16 4.3 6 2.4 1.7 0.12
625 1560 469 782 782 18 20 1560 1560 313 1200 3120 782 626 100
9340 23300 7000 20400 20400 164 180 40000 40900 8180 32000 46700 11600 16400 4000
Bold data above the 2L Class GA Standard
EPA 8260MADEP VPHAnalytical Method
Sample ID
Constituent of Concern
Soil to Groundwater MSCC
Table # 1
Summary of Analytical Results - Solid Samples
FCE 1426
Aliphati
c (C5-
C8)
Apliphat
ic (C9-
C12)
Aromati
c (C9-
C10)
1,2,4-
Trimeth
ylbenze
ne
1,3,5-
Trimeth
ylbenze
ne
Benzen
e
Diisopro
pyl
ether
Ethylbe
nzene
Isoprop
ylbenze
ne
(Cumen
e)
Methyl-
tert-
butyl
ether
Naphth
alene Toluene m&p-
Xylene
n-
Propylb
enzene
o-
Xylene
Collected Depth ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L
5/12/2023 N/A N/A N/A 2840 624 3260 43.4 4310 115 156 928 5510 15500 349 4110
01/11/2023 7100 9500 5400 1970 538 297 10.6 1460 91.8 ND 710 260 2330 270 150
11/8/2022 N/A N/A N/A 184 46.5 319 ND 495 18.2 12.1 122 198 690.6 46.9 N/A
5/12/2023 N/A N/A N/A 2780 655 2940 ND 4230 112 128 928 4710 15200 340 3800
01/11/2023 8200 4400 2200 343 92.9 2450 66.2 1170 53.6 672 302 444 1200 122 255
5/12/2023 N/A N/A N/A 0.53 ND ND ND 1.9 ND ND ND ND ND 0.52 ND
01/11/2023 ND ND 25 2.3 1.2 ND ND 2.7 ND ND ND ND 2.5 ND ND
5/12/2023 N/A N/A N/A 2220 432 3240 32.5 3080 97.9 77.9 903 85.1 4250 318 38
01/11/2023 1300 1400 1200 329 66.0 453 17.6 345 17.6 28.9 103 8.5 688 43.4 10.4
5/12/2023 N/A N/A N/A 0.62 ND ND ND ND ND ND ND 7.5 ND ND ND
2/9/2023 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
N/A N/A N/A 400 400 1 70 600 70 20 6 600 500 70 500
N/A N/A N/A 28500 25000 5000 70000 84500 25000 20000 6000 260000 50000 30000 50000
N/A N/A N/A N/A N/A 51 N/A N/A N/A N/A N/A 11 N/A N/A N/A
N/A N/A N/A N/A N/A 510 N/A N/A N/A N/A N/A 110 N/A N/A N/A
Bold data above the MSCC (Soil to Groundwater)
Sample ID
Constituent of Concern
2L Class GA Standards
MW-1
MW-2
MW-3
MW-4
SW-1
EPA Method 6200BMADEP VPH
2
Analytical Method
MW Number Date
5/12/2023 7.23 91.58
5/12/2023 7.59 92.41
5/12/2023 5.65 93.99
5/12/2023 8.03 91.971/11/2023
Table 3
Groundwater Flow Mapping Elevation Details
FCE-1426
Hendersonville, NC
5445 Asheville Hwy
MW-4 (Screen 5 to 10')
MW-3 (Screen 5 to 10')
MW-2 (Screen 5 to 10')
MW-1 (Screen 5 to 10')98.81
100.00
99.64
100.00

FIGURES
SKYLAND QUADRANGLE
NORTH CAROLINA 7.5 MINUTE SERIES (TOPOGRAPHIC)
Figure 1
USGS Topographic Map
Singleton Environmental, Inc
FCE-1426
MW-3
MW-1
MW-4
MW-2
SW-1
Singleton Environmental, Inc
FCE-1426
MW-3/93.99'
MW-1/91.58'
MW-4/91.97'
MW-2/92.41'
SW-1
94'
92'
Singleton Environmental, Inc
FCE-1426
WSW-1
WSW-2
Singleton Environmental, Inc
FCE-1426
MW-3
MW-1
MW-4
MW-2
SW-1
VOCs Exceeding 2L and 10 x 2B

APPENDIX A
Field Notes

APPENDIX B
Laboratory Analytical Reports and Chain-of-Custody Documentation
#=CL#
May 23, 2023
LIMS USE: FR - CHRIS SINGLETON
LIMS OBJECT ID: 92667495
92667495
Project:
Pace Project No.:
RE:
Chris Singleton
Singleton Environmental
105 Charlotte Highway
Asheville, NC 28803
FCE-1426
Dear Chris Singleton:
Enclosed are the analytical results for sample(s) received by the laboratory on May 16, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 28
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92667495
FCE-1426
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 28
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92667495
FCE-1426
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92667495001 MW-1 SM 6200B 63 PASI-CSAS
92667495002 MW-2 SM 6200B 63 PASI-CSAS
92667495003 MW-3 SM 6200B 63 PASI-CSAS
92667495004 MW-4 SM 6200B 63 PASI-CSAS
92667495005 SW-1 SM 6200B 63 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667495
FCE-1426
Sample:MW-1 Lab ID:92667495001 Collected:05/12/23 09:00 Received:05/16/23 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 3260 ug/L 05/22/23 21:17 71-43-225.0 50
Bromobenzene ND ug/L 05/22/23 21:17 108-86-125.0 50
Bromochloromethane ND ug/L 05/22/23 21:17 74-97-525.0 50
Bromodichloromethane ND ug/L 05/22/23 21:17 75-27-425.0 50
Bromoform ND ug/L 05/22/23 21:17 75-25-225.0 50
Bromomethane ND ug/L 05/22/23 21:17 74-83-925050
n-Butylbenzene ND ug/L 05/22/23 21:17 104-51-825.0 50
sec-Butylbenzene ND ug/L 05/22/23 21:17 135-98-825.0 50
tert-Butylbenzene ND ug/L 05/22/23 21:17 98-06-625.0 50
Carbon tetrachloride ND ug/L 05/22/23 21:17 56-23-525.0 50
Chlorobenzene ND ug/L 05/22/23 21:17 108-90-725.0 50
Chloroethane ND ug/L 05/22/23 21:17 75-00-3 L150.0 50
Chloroform ND ug/L 05/22/23 21:17 67-66-325.0 50
Chloromethane ND ug/L 05/22/23 21:17 74-87-3 L150.0 50
2-Chlorotoluene ND ug/L 05/22/23 21:17 95-49-825.0 50
4-Chlorotoluene ND ug/L 05/22/23 21:17 106-43-425.0 50
1,2-Dibromo-3-chloropropane ND ug/L 05/22/23 21:17 96-12-850.0 50
Dibromochloromethane ND ug/L 05/22/23 21:17 124-48-125.0 50
1,2-Dibromoethane (EDB)ND ug/L 05/22/23 21:17 106-93-425.0 50
Dibromomethane ND ug/L 05/22/23 21:17 74-95-325.0 50
1,2-Dichlorobenzene ND ug/L 05/22/23 21:17 95-50-125.0 50
1,3-Dichlorobenzene ND ug/L 05/22/23 21:17 541-73-125.0 50
1,4-Dichlorobenzene ND ug/L 05/22/23 21:17 106-46-725.0 50
Dichlorodifluoromethane ND ug/L 05/22/23 21:17 75-71-8 IH,L125.0 50
1,1-Dichloroethane ND ug/L 05/22/23 21:17 75-34-325.0 50
1,2-Dichloroethane ND ug/L 05/22/23 21:17 107-06-225.0 50
1,1-Dichloroethene ND ug/L 05/22/23 21:17 75-35-425.0 50
cis-1,2-Dichloroethene ND ug/L 05/22/23 21:17 156-59-225.0 50
trans-1,2-Dichloroethene ND ug/L 05/22/23 21:17 156-60-525.0 50
1,2-Dichloropropane ND ug/L 05/22/23 21:17 78-87-525.0 50
1,3-Dichloropropane ND ug/L 05/22/23 21:17 142-28-925.0 50
2,2-Dichloropropane ND ug/L 05/22/23 21:17 594-20-725.0 50
1,1-Dichloropropene ND ug/L 05/22/23 21:17 563-58-625.0 50
cis-1,3-Dichloropropene ND ug/L 05/22/23 21:17 10061-01-525.0 50
trans-1,3-Dichloropropene ND ug/L 05/22/23 21:17 10061-02-625.0 50
Diisopropyl ether 43.4 ug/L 05/22/23 21:17 108-20-325.0 50
Ethylbenzene 4310 ug/L 05/22/23 21:17 100-41-425.0 50
Hexachloro-1,3-butadiene ND ug/L 05/22/23 21:17 87-68-310050
Isopropylbenzene (Cumene)115 ug/L 05/22/23 21:17 98-82-825.0 50
Methylene Chloride ND ug/L 05/22/23 21:17 75-09-210050
Methyl-tert-butyl ether 156 ug/L 05/22/23 21:17 1634-04-425.0 50
Naphthalene 928 ug/L 05/22/23 21:17 91-20-310050
n-Propylbenzene 349 ug/L 05/22/23 21:17 103-65-125.0 50
Styrene ND ug/L 05/22/23 21:17 100-42-525.0 50
1,1,1,2-Tetrachloroethane ND ug/L 05/22/23 21:17 630-20-625.0 50
1,1,2,2-Tetrachloroethane ND ug/L 05/22/23 21:17 79-34-525.0 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 01:41 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667495
FCE-1426
Sample:MW-1 Lab ID:92667495001 Collected:05/12/23 09:00 Received:05/16/23 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 05/22/23 21:17 127-18-425.0 50
Toluene 5510 ug/L 05/22/23 21:17 108-88-325.0 50
1,2,3-Trichlorobenzene ND ug/L 05/22/23 21:17 87-61-610050
1,2,4-Trichlorobenzene ND ug/L 05/22/23 21:17 120-82-110050
1,1,1-Trichloroethane ND ug/L 05/22/23 21:17 71-55-625.0 50
1,1,2-Trichloroethane ND ug/L 05/22/23 21:17 79-00-525.0 50
Trichloroethene ND ug/L 05/22/23 21:17 79-01-625.0 50
Trichlorofluoromethane ND ug/L 05/22/23 21:17 75-69-450.0 50
1,2,3-Trichloropropane ND ug/L 05/22/23 21:17 96-18-425.0 50
1,2,4-Trimethylbenzene 2840 ug/L 05/22/23 21:17 95-63-625.0 50
1,3,5-Trimethylbenzene 624 ug/L 05/22/23 21:17 108-67-825.0 50
Vinyl chloride ND ug/L 05/22/23 21:17 75-01-450.0 50
m&p-Xylene 15500 ug/L 05/22/23 21:17 179601-23-150.0 50
o-Xylene 4110 ug/L 05/22/23 21:17 95-47-625.0 50
Surrogates
1,2-Dichloroethane-d4 (S)120 %05/22/23 21:17 17060-07-070-130 50
4-Bromofluorobenzene (S)99 %05/22/23 21:17 460-00-470-130 50
Toluene-d8 (S)102 %05/22/23 21:17 2037-26-570-130 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 01:41 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667495
FCE-1426
Sample:MW-2 Lab ID:92667495002 Collected:05/12/23 09:45 Received:05/16/23 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 2940 ug/L 05/22/23 21:34 71-43-225.0 50
Bromobenzene ND ug/L 05/22/23 21:34 108-86-125.0 50
Bromochloromethane ND ug/L 05/22/23 21:34 74-97-525.0 50
Bromodichloromethane ND ug/L 05/22/23 21:34 75-27-425.0 50
Bromoform ND ug/L 05/22/23 21:34 75-25-225.0 50
Bromomethane ND ug/L 05/22/23 21:34 74-83-925050
n-Butylbenzene ND ug/L 05/22/23 21:34 104-51-825.0 50
sec-Butylbenzene ND ug/L 05/22/23 21:34 135-98-825.0 50
tert-Butylbenzene ND ug/L 05/22/23 21:34 98-06-625.0 50
Carbon tetrachloride ND ug/L 05/22/23 21:34 56-23-525.0 50
Chlorobenzene ND ug/L 05/22/23 21:34 108-90-725.0 50
Chloroethane ND ug/L 05/22/23 21:34 75-00-3 L150.0 50
Chloroform ND ug/L 05/22/23 21:34 67-66-325.0 50
Chloromethane ND ug/L 05/22/23 21:34 74-87-3 L150.0 50
2-Chlorotoluene ND ug/L 05/22/23 21:34 95-49-825.0 50
4-Chlorotoluene ND ug/L 05/22/23 21:34 106-43-425.0 50
1,2-Dibromo-3-chloropropane ND ug/L 05/22/23 21:34 96-12-850.0 50
Dibromochloromethane ND ug/L 05/22/23 21:34 124-48-125.0 50
1,2-Dibromoethane (EDB)ND ug/L 05/22/23 21:34 106-93-425.0 50
Dibromomethane ND ug/L 05/22/23 21:34 74-95-325.0 50
1,2-Dichlorobenzene ND ug/L 05/22/23 21:34 95-50-125.0 50
1,3-Dichlorobenzene ND ug/L 05/22/23 21:34 541-73-125.0 50
1,4-Dichlorobenzene ND ug/L 05/22/23 21:34 106-46-725.0 50
Dichlorodifluoromethane ND ug/L 05/22/23 21:34 75-71-8 IH,L125.0 50
1,1-Dichloroethane ND ug/L 05/22/23 21:34 75-34-325.0 50
1,2-Dichloroethane ND ug/L 05/22/23 21:34 107-06-225.0 50
1,1-Dichloroethene ND ug/L 05/22/23 21:34 75-35-425.0 50
cis-1,2-Dichloroethene ND ug/L 05/22/23 21:34 156-59-225.0 50
trans-1,2-Dichloroethene ND ug/L 05/22/23 21:34 156-60-525.0 50
1,2-Dichloropropane ND ug/L 05/22/23 21:34 78-87-525.0 50
1,3-Dichloropropane ND ug/L 05/22/23 21:34 142-28-925.0 50
2,2-Dichloropropane ND ug/L 05/22/23 21:34 594-20-725.0 50
1,1-Dichloropropene ND ug/L 05/22/23 21:34 563-58-625.0 50
cis-1,3-Dichloropropene ND ug/L 05/22/23 21:34 10061-01-525.0 50
trans-1,3-Dichloropropene ND ug/L 05/22/23 21:34 10061-02-625.0 50
Diisopropyl ether ND ug/L 05/22/23 21:34 108-20-325.0 50
Ethylbenzene 4230 ug/L 05/22/23 21:34 100-41-425.0 50
Hexachloro-1,3-butadiene ND ug/L 05/22/23 21:34 87-68-310050
Isopropylbenzene (Cumene)112 ug/L 05/22/23 21:34 98-82-825.0 50
Methylene Chloride ND ug/L 05/22/23 21:34 75-09-210050
Methyl-tert-butyl ether 128 ug/L 05/22/23 21:34 1634-04-425.0 50
Naphthalene 928 ug/L 05/22/23 21:34 91-20-310050
n-Propylbenzene 340 ug/L 05/22/23 21:34 103-65-125.0 50
Styrene ND ug/L 05/22/23 21:34 100-42-525.0 50
1,1,1,2-Tetrachloroethane ND ug/L 05/22/23 21:34 630-20-625.0 50
1,1,2,2-Tetrachloroethane ND ug/L 05/22/23 21:34 79-34-525.0 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 01:41 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667495
FCE-1426
Sample:MW-2 Lab ID:92667495002 Collected:05/12/23 09:45 Received:05/16/23 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 05/22/23 21:34 127-18-425.0 50
Toluene 4710 ug/L 05/22/23 21:34 108-88-325.0 50
1,2,3-Trichlorobenzene ND ug/L 05/22/23 21:34 87-61-610050
1,2,4-Trichlorobenzene ND ug/L 05/22/23 21:34 120-82-110050
1,1,1-Trichloroethane ND ug/L 05/22/23 21:34 71-55-625.0 50
1,1,2-Trichloroethane ND ug/L 05/22/23 21:34 79-00-525.0 50
Trichloroethene ND ug/L 05/22/23 21:34 79-01-625.0 50
Trichlorofluoromethane ND ug/L 05/22/23 21:34 75-69-450.0 50
1,2,3-Trichloropropane ND ug/L 05/22/23 21:34 96-18-425.0 50
1,2,4-Trimethylbenzene 2780 ug/L 05/22/23 21:34 95-63-625.0 50
1,3,5-Trimethylbenzene 655 ug/L 05/22/23 21:34 108-67-825.0 50
Vinyl chloride ND ug/L 05/22/23 21:34 75-01-450.0 50
m&p-Xylene 15200 ug/L 05/22/23 21:34 179601-23-150.0 50
o-Xylene 3800 ug/L 05/22/23 21:34 95-47-625.0 50
Surrogates
1,2-Dichloroethane-d4 (S)119 %05/22/23 21:34 17060-07-070-130 50
4-Bromofluorobenzene (S)98 %05/22/23 21:34 460-00-470-130 50
Toluene-d8 (S)101 %05/22/23 21:34 2037-26-570-130 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 01:41 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667495
FCE-1426
Sample:MW-3 Lab ID:92667495003 Collected:05/12/23 10:15 Received:05/16/23 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 05/21/23 15:59 71-43-20.50 1
Bromobenzene ND ug/L 05/21/23 15:59 108-86-10.50 1
Bromochloromethane ND ug/L 05/21/23 15:59 74-97-50.50 1
Bromodichloromethane ND ug/L 05/21/23 15:59 75-27-40.50 1
Bromoform ND ug/L 05/21/23 15:59 75-25-20.50 1
Bromomethane ND ug/L 05/21/23 15:59 74-83-95.0 1
n-Butylbenzene ND ug/L 05/21/23 15:59 104-51-80.50 1
sec-Butylbenzene ND ug/L 05/21/23 15:59 135-98-80.50 1
tert-Butylbenzene ND ug/L 05/21/23 15:59 98-06-60.50 1
Carbon tetrachloride ND ug/L 05/21/23 15:59 56-23-50.50 1
Chlorobenzene ND ug/L 05/21/23 15:59 108-90-70.50 1
Chloroethane ND ug/L 05/21/23 15:59 75-00-3 L11.0 1
Chloroform ND ug/L 05/21/23 15:59 67-66-30.50 1
Chloromethane ND ug/L 05/21/23 15:59 74-87-31.0 1
2-Chlorotoluene ND ug/L 05/21/23 15:59 95-49-80.50 1
4-Chlorotoluene ND ug/L 05/21/23 15:59 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 05/21/23 15:59 96-12-81.0 1
Dibromochloromethane ND ug/L 05/21/23 15:59 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 05/21/23 15:59 106-93-40.50 1
Dibromomethane ND ug/L 05/21/23 15:59 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 05/21/23 15:59 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 05/21/23 15:59 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 05/21/23 15:59 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 05/21/23 15:59 75-71-8 IH0.50 1
1,1-Dichloroethane ND ug/L 05/21/23 15:59 75-34-30.50 1
1,2-Dichloroethane ND ug/L 05/21/23 15:59 107-06-20.50 1
1,1-Dichloroethene ND ug/L 05/21/23 15:59 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 05/21/23 15:59 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 05/21/23 15:59 156-60-50.50 1
1,2-Dichloropropane ND ug/L 05/21/23 15:59 78-87-50.50 1
1,3-Dichloropropane ND ug/L 05/21/23 15:59 142-28-90.50 1
2,2-Dichloropropane ND ug/L 05/21/23 15:59 594-20-70.50 1
1,1-Dichloropropene ND ug/L 05/21/23 15:59 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 05/21/23 15:59 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 05/21/23 15:59 10061-02-60.50 1
Diisopropyl ether ND ug/L 05/21/23 15:59 108-20-30.50 1
Ethylbenzene 1.9 ug/L 05/21/23 15:59 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 05/21/23 15:59 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 05/21/23 15:59 98-82-80.50 1
Methylene Chloride ND ug/L 05/21/23 15:59 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 05/21/23 15:59 1634-04-40.50 1
Naphthalene ND ug/L 05/21/23 15:59 91-20-32.0 1
n-Propylbenzene 0.52 ug/L 05/21/23 15:59 103-65-10.50 1
Styrene ND ug/L 05/21/23 15:59 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 05/21/23 15:59 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 05/21/23 15:59 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 01:41 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667495
FCE-1426
Sample:MW-3 Lab ID:92667495003 Collected:05/12/23 10:15 Received:05/16/23 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 05/21/23 15:59 127-18-40.50 1
Toluene ND ug/L 05/21/23 15:59 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 05/21/23 15:59 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 05/21/23 15:59 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 05/21/23 15:59 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 05/21/23 15:59 79-00-50.50 1
Trichloroethene ND ug/L 05/21/23 15:59 79-01-60.50 1
Trichlorofluoromethane ND ug/L 05/21/23 15:59 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/21/23 15:59 96-18-40.50 1
1,2,4-Trimethylbenzene 0.53 ug/L 05/21/23 15:59 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 05/21/23 15:59 108-67-80.50 1
Vinyl chloride ND ug/L 05/21/23 15:59 75-01-41.0 1
m&p-Xylene ND ug/L 05/21/23 15:59 179601-23-11.0 1
o-Xylene ND ug/L 05/21/23 15:59 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)123 %05/21/23 15:59 17060-07-070-130 1
4-Bromofluorobenzene (S)95 %05/21/23 15:59 460-00-470-130 1
Toluene-d8 (S)102 %05/21/23 15:59 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 01:41 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667495
FCE-1426
Sample:MW-4 Lab ID:92667495004 Collected:05/12/23 10:40 Received:05/16/23 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 3240 ug/L 05/22/23 21:52 71-43-212.5 25
Bromobenzene ND ug/L 05/22/23 21:52 108-86-112.5 25
Bromochloromethane ND ug/L 05/22/23 21:52 74-97-512.5 25
Bromodichloromethane ND ug/L 05/22/23 21:52 75-27-412.5 25
Bromoform ND ug/L 05/22/23 21:52 75-25-212.5 25
Bromomethane ND ug/L 05/22/23 21:52 74-83-912525
n-Butylbenzene ND ug/L 05/22/23 21:52 104-51-812.5 25
sec-Butylbenzene ND ug/L 05/22/23 21:52 135-98-812.5 25
tert-Butylbenzene ND ug/L 05/22/23 21:52 98-06-612.5 25
Carbon tetrachloride ND ug/L 05/22/23 21:52 56-23-512.5 25
Chlorobenzene ND ug/L 05/22/23 21:52 108-90-712.5 25
Chloroethane ND ug/L 05/22/23 21:52 75-00-3 L125.0 25
Chloroform ND ug/L 05/22/23 21:52 67-66-312.5 25
Chloromethane ND ug/L 05/22/23 21:52 74-87-3 L125.0 25
2-Chlorotoluene ND ug/L 05/22/23 21:52 95-49-812.5 25
4-Chlorotoluene ND ug/L 05/22/23 21:52 106-43-412.5 25
1,2-Dibromo-3-chloropropane ND ug/L 05/22/23 21:52 96-12-825.0 25
Dibromochloromethane ND ug/L 05/22/23 21:52 124-48-112.5 25
1,2-Dibromoethane (EDB)ND ug/L 05/22/23 21:52 106-93-412.5 25
Dibromomethane ND ug/L 05/22/23 21:52 74-95-312.5 25
1,2-Dichlorobenzene ND ug/L 05/22/23 21:52 95-50-112.5 25
1,3-Dichlorobenzene ND ug/L 05/22/23 21:52 541-73-112.5 25
1,4-Dichlorobenzene ND ug/L 05/22/23 21:52 106-46-712.5 25
Dichlorodifluoromethane ND ug/L 05/22/23 21:52 75-71-8 IH,L112.5 25
1,1-Dichloroethane ND ug/L 05/22/23 21:52 75-34-312.5 25
1,2-Dichloroethane ND ug/L 05/22/23 21:52 107-06-212.5 25
1,1-Dichloroethene ND ug/L 05/22/23 21:52 75-35-412.5 25
cis-1,2-Dichloroethene ND ug/L 05/22/23 21:52 156-59-212.5 25
trans-1,2-Dichloroethene ND ug/L 05/22/23 21:52 156-60-512.5 25
1,2-Dichloropropane ND ug/L 05/22/23 21:52 78-87-512.5 25
1,3-Dichloropropane ND ug/L 05/22/23 21:52 142-28-912.5 25
2,2-Dichloropropane ND ug/L 05/22/23 21:52 594-20-712.5 25
1,1-Dichloropropene ND ug/L 05/22/23 21:52 563-58-612.5 25
cis-1,3-Dichloropropene ND ug/L 05/22/23 21:52 10061-01-512.5 25
trans-1,3-Dichloropropene ND ug/L 05/22/23 21:52 10061-02-612.5 25
Diisopropyl ether 32.5 ug/L 05/22/23 21:52 108-20-312.5 25
Ethylbenzene 3080 ug/L 05/22/23 21:52 100-41-412.5 25
Hexachloro-1,3-butadiene ND ug/L 05/22/23 21:52 87-68-350.0 25
Isopropylbenzene (Cumene)97.9 ug/L 05/22/23 21:52 98-82-812.5 25
Methylene Chloride ND ug/L 05/22/23 21:52 75-09-250.0 25
Methyl-tert-butyl ether 77.9 ug/L 05/22/23 21:52 1634-04-412.5 25
Naphthalene 903 ug/L 05/22/23 21:52 91-20-350.0 25
n-Propylbenzene 318 ug/L 05/22/23 21:52 103-65-112.5 25
Styrene ND ug/L 05/22/23 21:52 100-42-512.5 25
1,1,1,2-Tetrachloroethane ND ug/L 05/22/23 21:52 630-20-612.5 25
1,1,2,2-Tetrachloroethane ND ug/L 05/22/23 21:52 79-34-512.5 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 01:41 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667495
FCE-1426
Sample:MW-4 Lab ID:92667495004 Collected:05/12/23 10:40 Received:05/16/23 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 05/22/23 21:52 127-18-412.5 25
Toluene 85.1 ug/L 05/22/23 21:52 108-88-312.5 25
1,2,3-Trichlorobenzene ND ug/L 05/22/23 21:52 87-61-650.0 25
1,2,4-Trichlorobenzene ND ug/L 05/22/23 21:52 120-82-150.0 25
1,1,1-Trichloroethane ND ug/L 05/22/23 21:52 71-55-612.5 25
1,1,2-Trichloroethane ND ug/L 05/22/23 21:52 79-00-512.5 25
Trichloroethene ND ug/L 05/22/23 21:52 79-01-612.5 25
Trichlorofluoromethane ND ug/L 05/22/23 21:52 75-69-425.0 25
1,2,3-Trichloropropane ND ug/L 05/22/23 21:52 96-18-412.5 25
1,2,4-Trimethylbenzene 2220 ug/L 05/22/23 21:52 95-63-612.5 25
1,3,5-Trimethylbenzene 432 ug/L 05/22/23 21:52 108-67-812.5 25
Vinyl chloride ND ug/L 05/22/23 21:52 75-01-425.0 25
m&p-Xylene 4250 ug/L 05/22/23 21:52 179601-23-125.0 25
o-Xylene 38.0 ug/L 05/22/23 21:52 95-47-612.5 25
Surrogates
1,2-Dichloroethane-d4 (S)118 %05/22/23 21:52 17060-07-070-130 25
4-Bromofluorobenzene (S)99 %05/22/23 21:52 460-00-470-130 25
Toluene-d8 (S)101 %05/22/23 21:52 2037-26-570-130 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 01:41 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667495
FCE-1426
Sample:SW-1 Lab ID:92667495005 Collected:05/12/23 11:00 Received:05/16/23 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 05/21/23 16:17 71-43-20.50 1
Bromobenzene ND ug/L 05/21/23 16:17 108-86-10.50 1
Bromochloromethane ND ug/L 05/21/23 16:17 74-97-50.50 1
Bromodichloromethane ND ug/L 05/21/23 16:17 75-27-40.50 1
Bromoform ND ug/L 05/21/23 16:17 75-25-20.50 1
Bromomethane ND ug/L 05/21/23 16:17 74-83-95.0 1
n-Butylbenzene ND ug/L 05/21/23 16:17 104-51-80.50 1
sec-Butylbenzene ND ug/L 05/21/23 16:17 135-98-80.50 1
tert-Butylbenzene ND ug/L 05/21/23 16:17 98-06-60.50 1
Carbon tetrachloride ND ug/L 05/21/23 16:17 56-23-50.50 1
Chlorobenzene ND ug/L 05/21/23 16:17 108-90-70.50 1
Chloroethane ND ug/L 05/21/23 16:17 75-00-3 L11.0 1
Chloroform ND ug/L 05/21/23 16:17 67-66-30.50 1
Chloromethane ND ug/L 05/21/23 16:17 74-87-31.0 1
2-Chlorotoluene ND ug/L 05/21/23 16:17 95-49-80.50 1
4-Chlorotoluene ND ug/L 05/21/23 16:17 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 05/21/23 16:17 96-12-81.0 1
Dibromochloromethane ND ug/L 05/21/23 16:17 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 05/21/23 16:17 106-93-40.50 1
Dibromomethane ND ug/L 05/21/23 16:17 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 05/21/23 16:17 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 05/21/23 16:17 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 05/21/23 16:17 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 05/21/23 16:17 75-71-8 IH0.50 1
1,1-Dichloroethane ND ug/L 05/21/23 16:17 75-34-30.50 1
1,2-Dichloroethane ND ug/L 05/21/23 16:17 107-06-20.50 1
1,1-Dichloroethene ND ug/L 05/21/23 16:17 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 05/21/23 16:17 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 05/21/23 16:17 156-60-50.50 1
1,2-Dichloropropane ND ug/L 05/21/23 16:17 78-87-50.50 1
1,3-Dichloropropane ND ug/L 05/21/23 16:17 142-28-90.50 1
2,2-Dichloropropane ND ug/L 05/21/23 16:17 594-20-70.50 1
1,1-Dichloropropene ND ug/L 05/21/23 16:17 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 05/21/23 16:17 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 05/21/23 16:17 10061-02-60.50 1
Diisopropyl ether ND ug/L 05/21/23 16:17 108-20-30.50 1
Ethylbenzene ND ug/L 05/21/23 16:17 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 05/21/23 16:17 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 05/21/23 16:17 98-82-80.50 1
Methylene Chloride ND ug/L 05/21/23 16:17 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 05/21/23 16:17 1634-04-40.50 1
Naphthalene ND ug/L 05/21/23 16:17 91-20-32.0 1
n-Propylbenzene ND ug/L 05/21/23 16:17 103-65-10.50 1
Styrene ND ug/L 05/21/23 16:17 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 05/21/23 16:17 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 05/21/23 16:17 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 01:41 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667495
FCE-1426
Sample:SW-1 Lab ID:92667495005 Collected:05/12/23 11:00 Received:05/16/23 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 05/21/23 16:17 127-18-40.50 1
Toluene 7.5 ug/L 05/21/23 16:17 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 05/21/23 16:17 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 05/21/23 16:17 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 05/21/23 16:17 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 05/21/23 16:17 79-00-50.50 1
Trichloroethene ND ug/L 05/21/23 16:17 79-01-60.50 1
Trichlorofluoromethane ND ug/L 05/21/23 16:17 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/21/23 16:17 96-18-40.50 1
1,2,4-Trimethylbenzene 0.62 ug/L 05/21/23 16:17 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 05/21/23 16:17 108-67-80.50 1
Vinyl chloride ND ug/L 05/21/23 16:17 75-01-41.0 1
m&p-Xylene ND ug/L 05/21/23 16:17 179601-23-11.0 1
o-Xylene ND ug/L 05/21/23 16:17 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)122 %05/21/23 16:17 17060-07-070-130 1
4-Bromofluorobenzene (S)95 %05/21/23 16:17 460-00-470-130 1
Toluene-d8 (S)103 %05/21/23 16:17 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 01:41 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667495
FCE-1426
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
775917
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92667495003, 92667495005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4026083
Associated Lab Samples:92667495003, 92667495005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 05/21/23 13:55
1,1,1-Trichloroethane ug/L ND 0.50 05/21/23 13:55
1,1,2,2-Tetrachloroethane ug/L ND 0.50 05/21/23 13:55
1,1,2-Trichloroethane ug/L ND 0.50 05/21/23 13:55
1,1-Dichloroethane ug/L ND 0.50 05/21/23 13:55
1,1-Dichloroethene ug/L ND 0.50 05/21/23 13:55
1,1-Dichloropropene ug/L ND 0.50 05/21/23 13:55
1,2,3-Trichlorobenzene ug/L ND 2.0 05/21/23 13:55
1,2,3-Trichloropropane ug/L ND 0.50 05/21/23 13:55
1,2,4-Trichlorobenzene ug/L ND 2.0 05/21/23 13:55
1,2,4-Trimethylbenzene ug/L ND 0.50 05/21/23 13:55
1,2-Dibromo-3-chloropropane ug/L ND 1.0 05/21/23 13:55
1,2-Dibromoethane (EDB)ug/L ND 0.50 05/21/23 13:55
1,2-Dichlorobenzene ug/L ND 0.50 05/21/23 13:55
1,2-Dichloroethane ug/L ND 0.50 05/21/23 13:55
1,2-Dichloropropane ug/L ND 0.50 05/21/23 13:55
1,3,5-Trimethylbenzene ug/L ND 0.50 05/21/23 13:55
1,3-Dichlorobenzene ug/L ND 0.50 05/21/23 13:55
1,3-Dichloropropane ug/L ND 0.50 05/21/23 13:55
1,4-Dichlorobenzene ug/L ND 0.50 05/21/23 13:55
2,2-Dichloropropane ug/L ND 0.50 05/21/23 13:55
2-Chlorotoluene ug/L ND 0.50 05/21/23 13:55
4-Chlorotoluene ug/L ND 0.50 05/21/23 13:55
Benzene ug/L ND 0.50 05/21/23 13:55
Bromobenzene ug/L ND 0.50 05/21/23 13:55
Bromochloromethane ug/L ND 0.50 05/21/23 13:55
Bromodichloromethane ug/L ND 0.50 05/21/23 13:55
Bromoform ug/L ND 0.50 05/21/23 13:55
Bromomethane ug/L ND 5.0 05/21/23 13:55
Carbon tetrachloride ug/L ND 0.50 05/21/23 13:55
Chlorobenzene ug/L ND 0.50 05/21/23 13:55
Chloroethane ug/L ND 1.0 05/21/23 13:55
Chloroform ug/L ND 0.50 05/21/23 13:55
Chloromethane ug/L ND 1.0 05/21/23 13:55
cis-1,2-Dichloroethene ug/L ND 0.50 05/21/23 13:55
cis-1,3-Dichloropropene ug/L ND 0.50 05/21/23 13:55
Dibromochloromethane ug/L ND 0.50 05/21/23 13:55
Dibromomethane ug/L ND 0.50 05/21/23 13:55
Dichlorodifluoromethane ug/L ND 0.50 IH05/21/23 13:55
Diisopropyl ether ug/L ND 0.50 05/21/23 13:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 01:41 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667495
FCE-1426
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4026083
Associated Lab Samples:92667495003, 92667495005
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 05/21/23 13:55
Hexachloro-1,3-butadiene ug/L ND 2.0 05/21/23 13:55
Isopropylbenzene (Cumene)ug/L ND 0.50 05/21/23 13:55
m&p-Xylene ug/L ND 1.0 05/21/23 13:55
Methyl-tert-butyl ether ug/L ND 0.50 05/21/23 13:55
Methylene Chloride ug/L ND 2.0 05/21/23 13:55
n-Butylbenzene ug/L ND 0.50 05/21/23 13:55
n-Propylbenzene ug/L ND 0.50 05/21/23 13:55
Naphthalene ug/L ND 2.0 05/21/23 13:55
o-Xylene ug/L ND 0.50 05/21/23 13:55
sec-Butylbenzene ug/L ND 0.50 05/21/23 13:55
Styrene ug/L ND 0.50 05/21/23 13:55
tert-Butylbenzene ug/L ND 0.50 05/21/23 13:55
Tetrachloroethene ug/L ND 0.50 05/21/23 13:55
Toluene ug/L ND 0.50 05/21/23 13:55
trans-1,2-Dichloroethene ug/L ND 0.50 05/21/23 13:55
trans-1,3-Dichloropropene ug/L ND 0.50 05/21/23 13:55
Trichloroethene ug/L ND 0.50 05/21/23 13:55
Trichlorofluoromethane ug/L ND 1.0 05/21/23 13:55
Vinyl chloride ug/L ND 1.0 05/21/23 13:55
1,2-Dichloroethane-d4 (S)%123 70-130 05/21/23 13:55
4-Bromofluorobenzene (S)%97 70-130 05/21/23 13:55
Toluene-d8 (S)%103 70-130 05/21/23 13:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4026084LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 20.920 105 60-140
1,1,1-Trichloroethane ug/L 23.020 115 60-140
1,1,2,2-Tetrachloroethane ug/L 22.820 114 60-140
1,1,2-Trichloroethane ug/L 21.420 107 60-140
1,1-Dichloroethane ug/L 25.520 127 60-140
1,1-Dichloroethene ug/L 25.120 126 60-140
1,1-Dichloropropene ug/L 26.320 131 60-140
1,2,3-Trichlorobenzene ug/L 18.420 92 60-140
1,2,3-Trichloropropane ug/L 21.820 109 60-140
1,2,4-Trichlorobenzene ug/L 19.020 95 60-140
1,2,4-Trimethylbenzene ug/L 22.120 110 60-140
1,2-Dibromo-3-chloropropane ug/L 17.320 86 60-140
1,2-Dibromoethane (EDB)ug/L 21.720 109 60-140
1,2-Dichlorobenzene ug/L 21.120 106 60-140
1,2-Dichloroethane ug/L 23.720 119 60-140
1,2-Dichloropropane ug/L 23.820 119 60-140
1,3,5-Trimethylbenzene ug/L 22.820 114 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 01:41 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667495
FCE-1426
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4026084LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 21.620 108 60-140
1,3-Dichloropropane ug/L 22.320 112 60-140
1,4-Dichlorobenzene ug/L 20.920 105 60-140
2,2-Dichloropropane ug/L 24.520 122 60-140
2-Chlorotoluene ug/L 23.120 115 60-140
4-Chlorotoluene ug/L 23.020 115 60-140
Benzene ug/L 22.720 113 60-140
Bromobenzene ug/L 21.020 105 60-140
Bromochloromethane ug/L 22.520 112 60-140
Bromodichloromethane ug/L 20.420 102 60-140
Bromoform ug/L 16.220 81 60-140
Bromomethane ug/L 24.920 124 60-140
Carbon tetrachloride ug/L 19.820 99 60-140
Chlorobenzene ug/L 21.820 109 60-140
Chloroethane ug/L 35.6 L12017860-140
Chloroform ug/L 24.820 124 60-140
Chloromethane ug/L 23.120 116 60-140
cis-1,2-Dichloroethene ug/L 24.420 122 60-140
cis-1,3-Dichloropropene ug/L 21.320 106 60-140
Dibromochloromethane ug/L 19.320 96 60-140
Dibromomethane ug/L 19.420 97 60-140
Dichlorodifluoromethane ug/L 26.2 IH2013160-140
Diisopropyl ether ug/L 22.820 114 60-140
Ethylbenzene ug/L 21.820 109 60-140
Hexachloro-1,3-butadiene ug/L 19.820 99 60-140
Isopropylbenzene (Cumene)ug/L 21.420 107 60-140
m&p-Xylene ug/L 43.040 108 60-140
Methyl-tert-butyl ether ug/L 21.120 105 60-140
Methylene Chloride ug/L 22.820 114 60-140
n-Butylbenzene ug/L 24.120 121 60-140
n-Propylbenzene ug/L 23.220 116 60-140
Naphthalene ug/L 21.120 106 60-140
o-Xylene ug/L 21.020 105 60-140
sec-Butylbenzene ug/L 22.620 113 60-140
Styrene ug/L 21.620 108 60-140
tert-Butylbenzene ug/L 17.920 89 60-140
Tetrachloroethene ug/L 19.020 95 60-140
Toluene ug/L 20.820 104 60-140
trans-1,2-Dichloroethene ug/L 25.620 128 60-140
trans-1,3-Dichloropropene ug/L 20.220 101 60-140
Trichloroethene ug/L 21.420 107 60-140
Trichlorofluoromethane ug/L 23.420 117 60-140
Vinyl chloride ug/L 19.520 97 60-140
1,2-Dichloroethane-d4 (S)%115 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 01:41 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667495
FCE-1426
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4026085MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667617004
4026086
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 140 60-140124 1220<0.31 28.0 24.9
1,1,1-Trichloroethane ug/L M12016360-140142 1320<0.33 32.6 28.5
1,1,2,2-Tetrachloroethane ug/L M12015060-140135 1120<0.22 30.1 27.0
1,1,2-Trichloroethane ug/L M12014460-140127 1220<0.32 28.8 25.4
1,1-Dichloroethane ug/L M12017960-140155 1420<0.37 35.8 31.0
1,1-Dichloroethene ug/L M12018160-140158 1320<0.35 36.1 31.6
1,1-Dichloropropene ug/L M12018860-140167 1220<0.43 37.6 33.4
1,2,3-Trichlorobenzene ug/L 20 114 60-140107 620<0.81 22.8 21.5
1,2,3-Trichloropropane ug/L M12014360-140130 1020<0.26 28.6 25.9
1,2,4-Trichlorobenzene ug/L 20 119 60-140111 720<0.64 23.9 22.2
1,2,4-Trimethylbenzene ug/L M12014560-140133 820<0.50 28.9 26.7
1,2-Dibromo-3-chloropropane ug/L 20 113 60-140106 720<0.34 22.7 21.1
1,2-Dibromoethane (EDB)ug/L M12014560-140131 1120<0.27 29.0 26.1
1,2-Dichlorobenzene ug/L 20 137 60-140126 820<0.34 27.3 25.2
1,2-Dichloroethane ug/L M12016560-140144 1420<0.32 33.0 28.7
1,2-Dichloropropane ug/L M12016360-140143 1420<0.36 32.7 28.5
1,3,5-Trimethylbenzene ug/L M12014860-140134 1020<0.33 29.6 26.8
1,3-Dichlorobenzene ug/L M12014160-140130 820<0.34 28.2 25.9
1,3-Dichloropropane ug/L M12015060-140134 1120<0.28 30.1 26.9
1,4-Dichlorobenzene ug/L 20 135 60-140123 920<0.33 26.9 24.5
2,2-Dichloropropane ug/L M12017560-140151 1520<0.39 35.1 30.3
2-Chlorotoluene ug/L M12015260-140141 720<0.32 30.4 28.3
4-Chlorotoluene ug/L M12015360-140140 920<0.32 30.6 28.0
Benzene ug/L M12015660-140137 1320<0.34 31.2 27.4
Bromobenzene ug/L 20 137 60-140126 820<0.29 27.4 25.2
Bromochloromethane ug/L M12015460-140132 1520<0.47 30.8 26.4
Bromodichloromethane ug/L 20 139 60-140120 1520<0.31 27.8 24.0
Bromoform ug/L 20 107 60-14096 1120<0.34 21.5 19.3
Bromomethane ug/L M12016460-140145 1320<1.7 32.9 29.0
Carbon tetrachloride ug/L 20 138 60-140121 1320<0.33 27.6 24.2
Chlorobenzene ug/L M12014460-140132 920<0.28 28.9 26.4
Chloroethane ug/L M02026160-140231 1220<0.65 52.1 46.3
Chloroform ug/L M12016460-140143 1420<0.43 32.9 28.5
Chloromethane ug/L M12019560-140177 1020<0.54 39.0 35.4
cis-1,2-Dichloroethene ug/L M12017160-140150 1320<0.38 34.1 30.0
cis-1,3-Dichloropropene ug/L 20 139 60-140123 1320<0.36 27.9 24.5
Dibromochloromethane ug/L 20 131 60-140115 1320<0.36 26.3 23.0
Dibromomethane ug/L 20 132 60-140114 1520<0.39 26.4 22.7
Dichlorodifluoromethane ug/L IH,M12026660-140238 1120<0.35 53.2 47.7
Diisopropyl ether ug/L M12015860-140138 1320<0.31 31.6 27.7
Ethylbenzene ug/L M12014860-140134 1020<0.30 29.5 26.8
Hexachloro-1,3-butadiene ug/L 20 126 60-140116 920<1.5 25.3 23.2
Isopropylbenzene (Cumene)ug/L M12014460-140129 1120<0.33 28.8 25.8
m&p-Xylene ug/L M14014660-140130 1140<0.71 58.4 52.0
Methyl-tert-butyl ether ug/L M12014360-140128 1120<0.42 29.1 26.0
Methylene Chloride ug/L M12015160-140135 1220<2.0 30.3 27.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 01:41 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 17 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667495
FCE-1426
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4026085MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667617004
4026086
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L M12015760-140142 1020<0.49 31.5 28.5
n-Propylbenzene ug/L M12015660-140142 1020<0.34 31.2 28.3
Naphthalene ug/L 20 134 60-140126 620<0.64 26.9 25.3
o-Xylene ug/L 20 140 60-140127 920<0.34 28.0 25.5
sec-Butylbenzene ug/L M12014960-140135 1020<0.40 29.9 27.1
Styrene ug/L M12014460-140130 1120<0.29 28.9 25.9
tert-Butylbenzene ug/L 20 122 60-140111 920<0.32 24.4 22.3
Tetrachloroethene ug/L 20 131 60-140118 1020<0.29 26.2 23.7
Toluene ug/L M12014160-140125 1220<0.24 28.2 25.0
trans-1,2-Dichloroethene ug/L M12018160-140160 1320<0.40 36.3 32.0
trans-1,3-Dichloropropene ug/L 20 138 60-140119 1520<0.36 27.6 23.9
Trichloroethene ug/L M12014860-140132 1220<0.38 29.6 26.3
Trichlorofluoromethane ug/L M12017960-140155 1420<0.30 35.8 31.0
Vinyl chloride ug/L M12016460-140143 1320<0.39 32.8 28.7
1,2-Dichloroethane-d4 (S)%120 70-130118
4-Bromofluorobenzene (S)%100 70-130100
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 01:41 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 18 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667495
FCE-1426
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
776133
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92667495001, 92667495002, 92667495004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4026974
Associated Lab Samples:92667495001, 92667495002, 92667495004
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 05/22/23 15:19
1,1,1-Trichloroethane ug/L ND 0.50 05/22/23 15:19
1,1,2,2-Tetrachloroethane ug/L ND 0.50 05/22/23 15:19
1,1,2-Trichloroethane ug/L ND 0.50 05/22/23 15:19
1,1-Dichloroethane ug/L ND 0.50 05/22/23 15:19
1,1-Dichloroethene ug/L ND 0.50 05/22/23 15:19
1,1-Dichloropropene ug/L ND 0.50 05/22/23 15:19
1,2,3-Trichlorobenzene ug/L ND 2.0 05/22/23 15:19
1,2,3-Trichloropropane ug/L ND 0.50 05/22/23 15:19
1,2,4-Trichlorobenzene ug/L ND 2.0 05/22/23 15:19
1,2,4-Trimethylbenzene ug/L ND 0.50 05/22/23 15:19
1,2-Dibromo-3-chloropropane ug/L ND 1.0 05/22/23 15:19
1,2-Dibromoethane (EDB)ug/L ND 0.50 05/22/23 15:19
1,2-Dichlorobenzene ug/L ND 0.50 05/22/23 15:19
1,2-Dichloroethane ug/L ND 0.50 05/22/23 15:19
1,2-Dichloropropane ug/L ND 0.50 05/22/23 15:19
1,3,5-Trimethylbenzene ug/L ND 0.50 05/22/23 15:19
1,3-Dichlorobenzene ug/L ND 0.50 05/22/23 15:19
1,3-Dichloropropane ug/L ND 0.50 05/22/23 15:19
1,4-Dichlorobenzene ug/L ND 0.50 05/22/23 15:19
2,2-Dichloropropane ug/L ND 0.50 05/22/23 15:19
2-Chlorotoluene ug/L ND 0.50 05/22/23 15:19
4-Chlorotoluene ug/L ND 0.50 05/22/23 15:19
Benzene ug/L ND 0.50 05/22/23 15:19
Bromobenzene ug/L ND 0.50 05/22/23 15:19
Bromochloromethane ug/L ND 0.50 05/22/23 15:19
Bromodichloromethane ug/L ND 0.50 05/22/23 15:19
Bromoform ug/L ND 0.50 05/22/23 15:19
Bromomethane ug/L ND 5.0 05/22/23 15:19
Carbon tetrachloride ug/L ND 0.50 05/22/23 15:19
Chlorobenzene ug/L ND 0.50 05/22/23 15:19
Chloroethane ug/L ND 1.0 05/22/23 15:19
Chloroform ug/L ND 0.50 05/22/23 15:19
Chloromethane ug/L ND 1.0 05/22/23 15:19
cis-1,2-Dichloroethene ug/L ND 0.50 05/22/23 15:19
cis-1,3-Dichloropropene ug/L ND 0.50 05/22/23 15:19
Dibromochloromethane ug/L ND 0.50 05/22/23 15:19
Dibromomethane ug/L ND 0.50 05/22/23 15:19
Dichlorodifluoromethane ug/L ND 0.50 IH05/22/23 15:19
Diisopropyl ether ug/L ND 0.50 05/22/23 15:19
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 01:41 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667495
FCE-1426
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4026974
Associated Lab Samples:92667495001, 92667495002, 92667495004
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 05/22/23 15:19
Hexachloro-1,3-butadiene ug/L ND 2.0 05/22/23 15:19
Isopropylbenzene (Cumene)ug/L ND 0.50 05/22/23 15:19
m&p-Xylene ug/L ND 1.0 05/22/23 15:19
Methyl-tert-butyl ether ug/L ND 0.50 05/22/23 15:19
Methylene Chloride ug/L ND 2.0 05/22/23 15:19
n-Butylbenzene ug/L ND 0.50 05/22/23 15:19
n-Propylbenzene ug/L ND 0.50 05/22/23 15:19
Naphthalene ug/L ND 2.0 05/22/23 15:19
o-Xylene ug/L ND 0.50 05/22/23 15:19
sec-Butylbenzene ug/L ND 0.50 05/22/23 15:19
Styrene ug/L ND 0.50 05/22/23 15:19
tert-Butylbenzene ug/L ND 0.50 05/22/23 15:19
Tetrachloroethene ug/L ND 0.50 05/22/23 15:19
Toluene ug/L ND 0.50 05/22/23 15:19
trans-1,2-Dichloroethene ug/L ND 0.50 05/22/23 15:19
trans-1,3-Dichloropropene ug/L ND 0.50 05/22/23 15:19
Trichloroethene ug/L ND 0.50 05/22/23 15:19
Trichlorofluoromethane ug/L ND 1.0 05/22/23 15:19
Vinyl chloride ug/L ND 1.0 05/22/23 15:19
1,2-Dichloroethane-d4 (S)%119 70-130 05/22/23 15:19
4-Bromofluorobenzene (S)%97 70-130 05/22/23 15:19
Toluene-d8 (S)%104 70-130 05/22/23 15:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4026975LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 20.720 104 60-140
1,1,1-Trichloroethane ug/L 22.720 113 60-140
1,1,2,2-Tetrachloroethane ug/L 22.120 110 60-140
1,1,2-Trichloroethane ug/L 20.620 103 60-140
1,1-Dichloroethane ug/L 25.020 125 60-140
1,1-Dichloroethene ug/L 24.920 124 60-140
1,1-Dichloropropene ug/L 25.720 129 60-140
1,2,3-Trichlorobenzene ug/L 18.920 95 60-140
1,2,3-Trichloropropane ug/L 21.320 106 60-140
1,2,4-Trichlorobenzene ug/L 19.120 95 60-140
1,2,4-Trimethylbenzene ug/L 21.620 108 60-140
1,2-Dibromo-3-chloropropane ug/L 18.920 94 60-140
1,2-Dibromoethane (EDB)ug/L 21.220 106 60-140
1,2-Dichlorobenzene ug/L 19.720 98 60-140
1,2-Dichloroethane ug/L 23.820 119 60-140
1,2-Dichloropropane ug/L 23.220 116 60-140
1,3,5-Trimethylbenzene ug/L 22.120 111 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 01:41 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 20 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667495
FCE-1426
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4026975LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 20.820 104 60-140
1,3-Dichloropropane ug/L 22.020 110 60-140
1,4-Dichlorobenzene ug/L 20.020 100 60-140
2,2-Dichloropropane ug/L 24.320 121 60-140
2-Chlorotoluene ug/L 21.920 110 60-140
4-Chlorotoluene ug/L 22.220 111 60-140
Benzene ug/L 22.320 112 60-140
Bromobenzene ug/L 20.120 100 60-140
Bromochloromethane ug/L 21.820 109 60-140
Bromodichloromethane ug/L 20.820 104 60-140
Bromoform ug/L 17.820 89 60-140
Bromomethane ug/L 25.320 126 60-140
Carbon tetrachloride ug/L 19.320 97 60-140
Chlorobenzene ug/L 21.120 106 60-140
Chloroethane ug/L 36.1 L12018060-140
Chloroform ug/L 24.220 121 60-140
Chloromethane ug/L 28.6 L12014360-140
cis-1,2-Dichloroethene ug/L 24.320 122 60-140
cis-1,3-Dichloropropene ug/L 21.320 107 60-140
Dibromochloromethane ug/L 20.620 103 60-140
Dibromomethane ug/L 18.820 94 60-140
Dichlorodifluoromethane ug/L 36.4 IH,L12018260-140
Diisopropyl ether ug/L 22.520 112 60-140
Ethylbenzene ug/L 21.220 106 60-140
Hexachloro-1,3-butadiene ug/L 21.420 107 60-140
Isopropylbenzene (Cumene)ug/L 20.420 102 60-140
m&p-Xylene ug/L 42.540 106 60-140
Methyl-tert-butyl ether ug/L 20.820 104 60-140
Methylene Chloride ug/L 22.320 111 60-140
n-Butylbenzene ug/L 23.620 118 60-140
n-Propylbenzene ug/L 22.220 111 60-140
Naphthalene ug/L 21.520 107 60-140
o-Xylene ug/L 21.020 105 60-140
sec-Butylbenzene ug/L 21.420 107 60-140
Styrene ug/L 21.520 107 60-140
tert-Butylbenzene ug/L 17.420 87 60-140
Tetrachloroethene ug/L 18.820 94 60-140
Toluene ug/L 22.420 112 60-140
trans-1,2-Dichloroethene ug/L 25.820 129 60-140
trans-1,3-Dichloropropene ug/L 20.120 100 60-140
Trichloroethene ug/L 21.120 105 60-140
Trichlorofluoromethane ug/L 23.620 118 60-140
Vinyl chloride ug/L 22.120 111 60-140
1,2-Dichloroethane-d4 (S)%116 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 01:41 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667495
FCE-1426
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4026976MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667432002
4026977
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 137 60-140136 120ND27.5 27.2
1,1,1-Trichloroethane ug/L M12015960-140158 020ND31.7 31.7
1,1,2,2-Tetrachloroethane ug/L M12014960-140151 220ND29.8 30.3
1,1,2-Trichloroethane ug/L 20 138 60-140139 120ND27.6 27.8
1,1-Dichloroethane ug/L M12017660-140174 120ND35.2 34.8
1,1-Dichloroethene ug/L M12017360-140171 220ND34.6 34.1
1,1-Dichloropropene ug/L M12018560-140182 120ND36.9 36.5
1,2,3-Trichlorobenzene ug/L 20 119 60-140123 320ND23.8 24.6
1,2,3-Trichloropropane ug/L M12014360-140145 120ND28.6 28.9
1,2,4-Trichlorobenzene ug/L 20 129 60-140129 020ND25.8 25.9
1,2,4-Trimethylbenzene ug/L M12015260-140150 220ND30.4 29.9
1,2-Dibromo-3-chloropropane ug/L 20 117 60-140120 320ND23.3 24.0
1,2-Dibromoethane (EDB)ug/L M12014260-140144 220ND28.3 28.8
1,2-Dichlorobenzene ug/L 20 137 60-140137 120ND27.5 27.3
1,2-Dichloroethane ug/L M12016360-140166 220ND32.5 33.2
1,2-Dichloropropane ug/L M12015860-140157 120ND31.6 31.4
1,3,5-Trimethylbenzene ug/L M12015360-140150 2200.67 31.2 30.6
1,3-Dichlorobenzene ug/L M12014360-140140 220ND28.5 27.9
1,3-Dichloropropane ug/L M12014860-140148 020ND29.5 29.7
1,4-Dichlorobenzene ug/L 20 136 60-140134 120ND27.1 26.8
2,2-Dichloropropane ug/L M12017560-140173 120ND34.9 34.6
2-Chlorotoluene ug/L M12015760-140154 220ND31.4 30.9
4-Chlorotoluene ug/L M12015460-140152 120ND30.9 30.5
Benzene ug/L M12015360-140150 1203.1 33.6 33.1
Bromobenzene ug/L 20 137 60-140136 120ND27.5 27.2
Bromochloromethane ug/L M12015160-140149 120ND30.1 29.8
Bromodichloromethane ug/L 20 133 60-140133 020ND26.6 26.7
Bromoform ug/L 20 103 60-140105 120ND20.7 21.0
Bromomethane ug/L M12015060-140147 320ND30.0 29.3
Carbon tetrachloride ug/L 20 132 60-140130 120ND26.3 26.0
Chlorobenzene ug/L M12014460-140142 120ND28.8 28.4
Chloroethane ug/L M02023560-140230 220ND47.1 46.0
Chloroform ug/L M12016860-140166 120ND33.5 33.1
Chloromethane ug/L M02019060-140190 020ND38.0 37.9
cis-1,2-Dichloroethene ug/L M12017160-140166 320ND34.2 33.3
cis-1,3-Dichloropropene ug/L 20 135 60-140137 220ND27.0 27.5
Dibromochloromethane ug/L 20 127 60-140128 020ND25.5 25.6
Dibromomethane ug/L 20 124 60-140125 120ND24.7 25.0
Dichlorodifluoromethane ug/L IH,M02022860-140227 020ND45.6 45.4
Diisopropyl ether ug/L M12015960-140159 0201.2 33.1 32.9
Ethylbenzene ug/L M12014860-140146 220ND29.6 29.1
Hexachloro-1,3-butadiene ug/L 20 134 60-140135 020ND26.8 27.0
Isopropylbenzene (Cumene)ug/L M12014860-140143 420ND29.7 28.6
m&p-Xylene ug/L M14014660-140144 2402.1 60.5 59.6
Methyl-tert-butyl ether ug/L M12014660-140150 22014.5 43.7 44.5
Methylene Chloride ug/L M12015360-140150 220ND30.7 30.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 01:41 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667495
FCE-1426
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4026976MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667432002
4026977
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L M12016960-140164 320ND33.8 32.7
n-Propylbenzene ug/L M12015660-140154 120ND31.2 30.8
Naphthalene ug/L M12014860-140157 5208.9 38.6 40.4
o-Xylene ug/L M12014260-140142 0203.0 31.4 31.4
sec-Butylbenzene ug/L M12015460-140153 120ND30.7 30.5
Styrene ug/L M12014460-140145 120ND28.7 28.9
tert-Butylbenzene ug/L 20 124 60-140120 320ND24.7 24.0
Tetrachloroethene ug/L 20 127 60-140127 020ND25.4 25.5
Toluene ug/L M12014160-140135 4201.1 29.3 28.1
trans-1,2-Dichloroethene ug/L M12018260-140180 120ND36.4 36.0
trans-1,3-Dichloropropene ug/L 20 135 60-140135 020ND27.0 27.1
Trichloroethene ug/L M12014160-140142 020ND28.3 28.4
Trichlorofluoromethane ug/L M12016460-140162 120ND32.8 32.4
Vinyl chloride ug/L M12015360-140150 220ND30.7 30.1
1,2-Dichloroethane-d4 (S)%119 70-130119
4-Bromofluorobenzene (S)%102 70-130103
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 01:41 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 28
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92667495
FCE-1426
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 01:41 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 24 of 28
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92667495
FCE-1426
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92667495001 776133MW-1 SM 6200B
92667495002 776133MW-2 SM 6200B
92667495003 775917MW-3 SM 6200B
92667495004 776133MW-4 SM 6200B
92667495005 775917SW-1 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 01:41 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 28
Page 26 of 28
Page 27 of 28
Page 28 of 28