MO-88974_97285_CA_LSA_20240226

Limited Site Assessment Report
A. Site Information
1. Site Identification
sDate ofReport: February26. 2024
sFacility I.D.: ~M'"""~~'A"--_________ UST Incident Number (if known): Pending
ssite Name: 2901 Monroe Road
8 Site Street Address:--=29""'0""'1'""""'M~o"-'n"""'ro~e""R,_.o"'"'a""d"'---------------------
scity/Town: Charlotte Zip Code: 28205 County: Mecklenburg
8 Description of Geographical Data Point (e.g., diesel fill port): Assumed Source Area
sLocation Method (GPS, topographical map, other): _G"'""'-P""-S ____________ _
sLatitude (decimal degrees): N35.204442 Longitude (decimal degrees): W80. 7062302
2. Information about Contacts Associated with the Leaking UST System (Addresses must include
street, city, state, zip code and mailing address, if different).
susT Owner: No Documented UST or ASTs Remaining on the Site at the Time o(the Assessment
Address: Tel.:---------­
susT Operator: No Documented UST or ASTs Remaining on the Site at the Time o(the Assessment
Address: Tel:----------
sproperty Owner: MJP Monroe Road Holdings. LLC
Address: 520 Gervias Street. Columba. SC 29201 Tel: [phone]
sproperty Occupant: _,U."""'n""'o"""c""cu""'p~z""·e""d _____________________ _
Address: _________________ Tel:-----------
sconsultant/Contractor: Harmon Environmental PA
Address: 615 Bruce Thomas Rd. Monroe. NC 28112 Tel: [phone]
s Analytical Laboratory: W aypoint Analytical LLC. State Certification No. -"4'-"0'-='2 __ _
Address: 449 Springbrook Rd. Charlotte. NC 28224 Tel: [phone]
3. Information about Release
8 Date Discovered: _,J.'""a=n:.::::u=ary'"-'-'2""'6"'".-=2""0=24-'---------------------­
sEstimated Quantity of Release: -=U.=n=kn""o""'w"'"'n""-------------------­
scause ofRelease: ____,.U.""'n""kn'""o""'w""n"'-----------------------­
rasource ofRelease (Dispenser/Piping/UST): ----"'U.""n"""kn"'o~w""'n"'-------------
ssizes and contents ofUST system(s) from which the release occurred): _,U."""'n""k""n""o'""w""'n~----
4. Certification (Tize title page must display tlze seal and signature oftlze certifying P.E. or LG. and
tlze name and certification number oftlze company or corporation [See 15A NCAC 2L .0103(e).])
a Professional Engineer/License~r Harmon Environmental. PA,
M · · din this report is correct and accurate to the best of my knowledge.
Limited Site Assessment
2901 Monroe Road, Charlotte, North Carolina
February 26, 2024
1 Harmon Environmental, P A
615 Bruce Thomas Road, Monroe, North Carolina
harmonenv@yahoo. com
B. Site History and Characterization
Present information relevant to site history and characterization, updating information provided in the 20-Day
Report, the Initial Abatement Action Report, and any FP Recovery Reports, using the following outline:
1. Provide UST owner and operator information
s List the names, addresses, telephone numbers, and dates of ownership/operation of all previous
UST owners and operators of the UST system(s). Present in table form (Use Reporting Table
B-2, Site History, UST Owner/Operator and Other Responsible Party Information, from the
Guidelines, Appendix B.).
No tanks were observed on the property at the time o[this assessment (See attached Table B-2).
2. Provide UST information (inclusive of all USTs, currently and historically in place at facility). For each
UST, provide the following information in table form (Use Reporting Table B-1, Site History-UST/AST
System and Other Release Information, from the Guidelines, Appendix B.):
s Tank identification number (keyed to a map showing the locations of all UST systems);
s Last contents of tank;
s Previous contents oftank (if any);
s Capacity of tank in gallons;
s Construction (material and structure);
s Tank dimensions;
s Installation date;
u=~ Description of piping and pump(s) associated with each UST;
s Status ofUST (in use or not in use, closed in place, closed by removal; date oflast use, date of
closure); and
s Indication that a release was or was not associated with the tank or associated piping or pump(s).
Provide discussion to supplement Table B-1 and the UST location map in order to clarify the spatial
and historical relationships among tanks and between tanks and piping and dispensers and a brief
description of all historical compliance issues and releases (indicate incident number).
No tanks were observed on the property at the time o(this assessment (See Attached Table B-1 ).
3. Provide non-UST information.
s List, describe, and indicate location of ASTs and associated piping and pump(s) currently and
historically in place at facility and describe historical releases (indicate incident number). For each
AST, present the information in table form (Use Reporting Table B-1, Site History-UST/AST
System and Other Release Information, from the Guidelines, Appendix B); and
s List, describe, and indicate location and date of spills that have occurred at facility.
No tanks or associated piping was observed on the property at the time o(this assessment.
4. Provide a comprehensive description of the release, including date discovered, cause and source
(including tank identification number and contents), and the relationship of historical UST releases, non­
UST releases, and off-site releases (indicate incident number) to contamination from current release.
On January 26. 2024. Harmon Environmental. PA and MidSouth Environmental. Inc. visited the stie
to collect soil and groundwater samples in the vicinity of a suspected petroleum release. One
temporary monitor well and fOur soil borings were advanced on the site and soil and groundwater
samples were collected The analvtical results associated with these samples are presented in this
report. A 24-Hour Release Report was filed on February 21. 2024.
5. Provide a brief description of site characteristics (including status of facility (active or inactive), land use
of site and surrounding area, water supply, topography, vegetation, surface water, wells, buildings, surface
cover, soil type, depth to and nature of bedrock, depth to groundwater, direction of groundwater flow, etc.)
Limited Site Assessment
2901 Monroe Road, Charlotte, North Carolina
Febrnary 26, 2024
2 Harmon Environmental, P A
615 Broce Thomas Road, Monroe, North Carolina
[e-mail]
,·
The site is located in an established commercial area in Charlotte, North Carolina. The topography o(the
site slopes toward the north. draining toward Briar Creek. The vegetation on site primarily consists of
grass and ornamental shrubbery. Based on the Soil Survey of Mecklenburg County published by the United
States Department of Agriculture. Natural Resource Conservation Service (USDA NRCS) in 2023. the soil
type associated with this region o(Mecklenburg County is the Cecil-Urban land complex (CuB). The depth
to bedrock on site was not determined during this project. The depth to groundwater was determined on
January 27, 2024 as approximately 12.67 feet below grade. The direction of groundwater flow has not
been determined at this time.
6. Summarize initial abatement actions, assessment activities, and corrective actions performed to date and
list all reports previously submitted.
No initial abatment activities have been conducted on this site.
C. Risk Characterization
Submit the following questionnaire in its entirety. Answer all questions completely. Attach additional pages as needed
to fully explain answers. Base answers/explanations on information obtained (or updated from preceding reports)
during the current investigation. Note: Source area means point of release from a UST system.
Limited Site Assessment Risk Classification and Land Use Form
Part I-Groundwater/Surface WaterNapor Impacts
High Risk
1. Has the release contaminated any water supply well including any well used for non-drinking purpo~e ?
YE /NO
2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the relea .
YE 0
3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars, industrial cooling~~
filling swimming pools) located within 250 feet of the source area of the release? YE~
4. Does groundwater within 500 feet of the source area of the release have the potential for future use~
is no other source ofwater supply other than the groundwater)? YE~
5. Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a
confmed space or pose any other serious threat to public health, public safety or the environment? ~
YE~
If yes, describe.
The release area is on an undeveloped property.
6. Are there any other factors that would cause the release to pose an imminent danger to public health~
public safety, or the environment? YE~
If yes, describe.
Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the release? ~0
8.
If YES, does the maximum groundwater contaminant concentration exceed the surface water quality~
standards and criteria found in 15A NCAC 2B .0200 by a factor of 10? YE.,~
Is the source area of the release located within a approved or planned wellhead protection area as defm~
42 USC 300h-7(e)? YE~
If yes, describe.
Limited Site Assessment 3 Harmon Environmental, P A
615 Bruce Thomas Road, Monroe, North Carolina
[e-mail]
2901 Monroe Road, Charlotte, North Carolina
February 26, 2024
9. Is the release located in the Coastal Plain physiographic region as designated on a map entitled "Ge~
of North Carolina" published by the Department in 1985? YE~
If YES, is the source area of the release located in an area in which there is recharge to an unconfmed or
semi-confmed deeper aquifer that is being used or may be used as a source of drinking water? YES/NO
If YES, describe.
10. Do the levels of groundwater contamination for any contaminant exceed the gross contamination le~e~
(see Table 9) established by the Department? YE~
Part II-Land Use
Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary residences (permanent or temporary)? ~
YE~
2.
Describe.
The property is undeveloped
Does the property contain a school, daycare center, hospital, playground, park, recreation area, chur~
nursing home, or other place of public assembly? YE~
Describe.
The property is undeveloped
3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or industrial
(e.g., manufacturing, utilities, industrial research and development, chemical/petroleum bulk storage~
etc.) enterprise, an inactive commercial or industrial enterprise, or is the land undeveloped? YE~
Describe.
The property is undeveloped
YE~ 4. Do children visit the property?
Explain.
The property is undeveloped
Is access to the property reliably restricted consistent with its use (e.g., by fences, security personnel or
both)? YE€)
Explain.
The property is undeveloped
Do pavement, buildings, or other structures cap the contaminated soil?
Describe.
The property is undeveloped with grass. ornamental shrubbery and woods. No structures are present
on the property.
If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil will
remain capped in the foreseeable future?
5. What is the zoning status of the property?
Manufacturing and Logistics (ML-2)
6. Is the use of the property likely to change in the next 20 years?
Explain.
Limited Site Assessment
2901 Monroe Road, Charlotte, North Carolina
February 26, 2024
4 Harmon Environmental, P A
615 Bruce Thomas Road, Monroe, North Carolina
[e-mail]
The property is located within a well established business area on Monroe Road in Charlotte. There
is no indications that this zoning will change in the fOreseeable future.
Property Surrounding Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the release (excludes property
containing source area ofthe release):
1. What is the distance from the source area of the release to the nearest primary or secondary residence
(permanent or temporary)?
The nearest primary residence is the Dora! Apartments approximately I 00 teet ftom the assessed
ro er .
2. What is the distance from the source area of the release to the nearest school, daycare center, hospital,
playground, park, recreation area, church, nursing home or other place of public assembly?
The Chantillv Montessori School is approximately 2.000 feet ftom the assessed property.
3. What is the zoning status of properties in the surrounding area?
General Commercial (CG) and Manufacturing and Logistics (ML-1 and ML-2)
4. Briefly characterize the use and activities of the land in the surrounding area.
The site is located in an established commercial area within the Charlotte city limits.
D. Receptor Information
Determine and describe all potential receptors, including those in the categories listed below. Compile this
information in a table entitled Public and Private Water Supply Well and Other Receptor Information (Complete
Table B-5 from the Guidelines, Appendix B.) in which an identification code is assigned to each potential receptor.
Indicate the locations of each potential receptor, using the identification code, on a potential receptor map. Use
information from all available sources and from site investigations.
1. Water Supply Wells
Determine and describe the location, use, and ownership of public and private water supply wells in the area
within 1,500 feet of the source of the release. Compile this information in Table B-5 and indicate the well
locations on the potential receptor map. Note whether well users are also served by a municipal water supply.
Refer to the instructions for a water supply well survey in Section 2.3 of the Guidelines.
On January 26. 2024. Harmon Environmental. PA personnel visually evaluated properties located within
a 1.500-fOot radius ofthe site. This evaluation consisted oflooking fOr water meters at each property.
Additionally. Harmon Environmental. PA reviewed the Mecklenburg County Registered Well web site fOr
wells within the area surrounding the site. Based on this review. no water supply wells were observed or
documented within 1.500 feet o(the assessed property.
2. Public Water Supplies
Determine the existence and availability of public water supplies within 1,500 feet of the source area of the
release. Compile this information in Table B-5 and indicate the locations of the nearest public water lines and
the source(s) of the public water supply on the potential receptor map.
Based on the locations of the water meters observed during the January 26. 2024 survey. Charlotte­
Mecklenburg municipal water lines appear to be available along the roads throughout the assessed area.
3. Surface Water
Identify all surface water bodies (e.g., ditch, pond, stream, lake, river) located within 1,500 feet of the source
area of the release and indicate distance from source of release in Table B-5 and indicate locations on the
potential receptor map.
Based on the USGS topographic map of the region. Briar Creek is located northwest and north ofthe
assessed property.
Limited Site Assessment
2901 Monroe Road, Charlotte, North Carolina
February 26, 2024
5 Harmon Environmental, P A
615 Bruce Thomas Road, Monroe, North Carolina
[e-mail]
4. Wellhead Protection Areas
Indicate whether or not the UST release source area is located within an approved wellhead protection area.
Refer to Section 2.3 of the Guidelines for instructions on how to access the list of currently approved
wellhead protection plans and generate a map ofUST and wellhead protection area locations. List any
identified wellhead protection area in Table B-5 by PWS ID number and PWS system name and show the
wellhead protection area on the potential receptor map. To document performance of the wellhead protection
area investigation append to the potential receptor map a copy of the map generated using ArciMS Viewer to
show 1) the UST location, 2) the wellhead protection area, and 3) community wells.
Based on the DEO Division o(Environmental Health. Public Water Supply Section web site. the assessed
property does not appear to be located within a documented Wellhead Protection Area.
5. Deep Aquifers in the Coastal Plain Physiographic Region
Indicate if the source area of the release is located in an area in which there is recharge to an unconfined or
semi-confmed deeper aquifer and indicate if that aquifer is being used or may be used as a source of drinking
water, referring to Section 2.3 of the Guidelines. Based on a review of scientific literature on the regional
hydrogeology and well construction records and lithologic logs for deeper wells in the area, identify and
describe the deep aquifers underlying the release. Include information on the depth of the deep aquifer in
relation to the surficial saturated zone, the lithology and hydraulic conductivity of the strata between the
surficial aquifer and the deeper aquifer, and the difference in groundwater head between the surficial aquifer
and the deeper aquifer. Discuss the local and regional usage of the deep aquifer and the draw down from major
pumping influences. Also, specify the distance from the source area of the release to major discharge areas,
such as streams and rivers. Cite all sources and references used for this discussion.
NOTE: This requirement only pertains to releases in the Coastal Plain physiographic region as designated
on a map entitled "Geology of North Carolina" published by the Department in 1985. This map can be
obtained for a fee .from the North Carolina Geologic Survey, 1612 MSC, Raleigh, NC 27699-1612.
The assessed property is not located within the Coastal Plain Physiographic Region.
6. Subsurface Structures
Describe subsurface features, including sewers, utility lines, conduits, basements, vaults, septic tanks,
drainfields, etc., referring to Section 2.3 of the Guidelines. Compile this information in Table B-5 and
indicate the locations on the potential receptor map. Discuss the risk of explosion due to the accumulation of
vapors in confmed space and the threat to public health, public safety or the environment posed by vapors in
the subsurface features.
No subsurface features were observed during the site assessment.
E. Land Use
1. Property Owners and Occupants
Determine the names and addresses of property owners and occupants within or contiguous to the area
containing contamination and all property owners and occupants within or contiguous to the area where the
contamination is expected to migrate. Compile this information in Table B-6 from the Guidelines, Appendix
B, and indicate the property locations on the land use map.
See Attached Table B-6.
2. Sensitive Land Use Features
List features sensitive to impact from the release (schools, daycare centers, nursing homes, hospitals,
playgrounds, parks and recreation areas, churches, camps and other places of assembly) and show the zoning
status of the area within 1500' of the source of the release. Compile this information in Table B-10 from the
Guidelines, Appendix B, and indicate the feature locations on the land use map.
Limited Site Assessment
2901 Monroe Road, Charlotte, North Carolina
February 26, 2024
6 Harmon Environmental, P A
615 Bruce Thomas Road, Monroe, North Carolina
[e-mail]
The Chantilly Montessori School is located approximately 2. 000 feet northeast o(the assessed property.
F. Site Geology and Hydrogeology
Describe the soil and geology encountered at the site. Discuss the effects of soil and geological characteristics on
the migration and attenuation of contaminants. Include information obtained during assessment activities (e.g.,
lithologic descriptions made during drilling, probe surveys, tank closure, etc). If a Phase II investigation is
required include a discussion of groundwater flow direction and hydraulic gradient (vertical and horizontal).
The soil samples collected as the Geoprobe® boring was advanced indicated the presence of_fine sanc!v
silt and fine sandy silty clav to a depth of approximately 20 teet below grade. Temporary monitor well
MW-1 was advanced to a termination depth o(20 teet below grade using Geoprobe® technology.
G. Sampling Results
Phase I Investigation
Responsible parties must perform a Phase I investigation for all releases.
A Phase I investigation includes the installation of one monitoring well in the source area of a release.
Soil samples are to be collected every five feet in the unsaturated zone and should be analyzed in accordance with
the methods specified in Table 5 of the Guidelines, Analytical Methods for Petroleum Contaminated Soil. If the
water table is encountered at 25 feet or greater from the land surface, samples for laboratory analysis should be
collected every 10 feet in the unsaturated zone.
1. Describe all soil sampling performed during the installation of the source well(s) as follows:
s Use tables and maps to illustrate;
s Indicate location of soil samples: from excavation, borehole, geoprobe, etc.;
s Complete Table B-3 from the Guidelines, Appendix B; and
s If multiple source areas have been identified, clearly distinguish the data collected from each source area
in the table.
On January 26. 2024. soil samples were collected continuously ftom the surface o(the ground to the selected
termination depths using Geoprobe® direct push technology. Each soil sample was visually described in
general accordance with the Unified Soil Classification System (USCSJ. Based on the depth o(the water table
on site soil samples were collected (tom the temporary monitor well boring at 4 teet. 8 teet and 12 teet below
grade. Soil samples were collected (tom the four additional Geoprobe® borings (tom a depth of12 teet below
a de.
2. Describe any groundwater sampling from the source area monitoring well(s), as follows:
s Use tables and maps to illustrate;
s Indicate location of groundwater samples/monitoring wells/water supply wells;
s Complete and attach Table B-4 from the Guidelines, Appendix B; and
s If multiple source areas have been identified, clearly distinguish the data collected from each source area
in the table.
Note: If free product is present, do not sample the monitoring well. Report the estimated thickness, type, and
quantity of free product present.
On January 27. 2024 Harmon Environmental. PA personnel collected groundwater samples (tom temporary
monitor well MW-1 in general accordance with DEQ accepted protocols. The location o(this temporary
monitor well is depicted on Figure 2. The analytical results associated with these samples are presented in
Table B-4. No (tee product was observed at the time o(sample collection.
3. Provide monitoring well construction information (Complete and attach Table B-7 from the Guidelines,
Appendix B.).
Limited Site Assessment
2901 Monroe Road, Charlotte, North Carolina
Febrnary 26, 2024
7 Harmon Environmental, PA
615 Brnce Thomas Road, Monroe, North Carolina
[e-mail]
Table B-7 (Attached) presents the construction information for temporary monitor well MW-1.
Phase II Investigation (if required)
A Phase II investigation should only he conducted if the release is from a high risk commercial UST and
the levels of groundwater contamination detected in the source area monitoring well exceed the groundwater
standards or interim standards by a factor of 10.
The Phase II investigation includes the installation of three additional monitoring wells to be installed as
follows: one up gradient of the source of contamination and two downgradient of the source of contamination of
the source but within the area of contamination. The upgradient and downgradient wells must be placed so that
groundwater flow direction can be determined.
1. Describe any groundwater sampling from the monitoring well(s), as follows:
s Use tables and maps to illustrate;
s Indicate location of groundwater samples/monitoring wells/water supply wells;
s Complete and attach Table B-4 from the Guidelines, Appendix B; and
s If multiple source areas have been identified, clearly distinguish the data collected from each source area
in the table.
Note: If free product is present, do not sample the monitoring well. Report the estimated thickness, type, and
quantity of free product present.
2. Provide monitoring well construction information (Complete and attach Table B-7 from the Guidelines,
Appendix B.).
A Phase II Limited Site Assessment was not conducted at this site.
H. Conclusions and Recommendations
Discuss the risk criteria that apply to the release and identify any other site-specific factors related to the
release that may pose a risk to human health and the environment. Also, discuss any site-specific conditions or
possible actions that could result in lowering the level of risk posed by the release.
On January 26. 2024 Harmon Environmental. PA initiated a Phase I Limited Site Assessment at the site. Based
on the depth of the water table on site soil samples were collected from the temporary monitor well boring at
4 feet. 8 feet and 12 feet below grade. Soil samples were collected from the four additional Geoprobe® borings
from a depth of12 feet below grade. Each soil sample was analyzed for volatile organic compounds (VOCs ),
semi-volatile organic compounds (SVOCs). volatile petroleum hydrocarbon compounds (VPH) and extractable
petroleum hydrocarbon compounds (EPH). The analytical results associated with these seven samples are
presented in Table B-3. A groundwater sample wase collected from temporary monitor well MW-1 on January
27. 2024 and analyzed for VOCs. SVOCs. VPH. EPH and lead The analytical results associated with this
sample are summarized on Table B-4. Based on these data. MJP Monroe Road Holdings. LLC would like to
pursue closure o(this site with a Notice o(Residual Petroleum.
I. Free Product Investigation and Recovery (if applicable)
Discuss the status of free product at the site, as follows:
1. If free product is, or has been, present at the site, describe its current and historical status (product
distribution, thickness, recovery activities). Refer to tables in Section K: Table B-7, Monitoring and
Remediation Well Construction Information; and Table B-8A, Free Product Recovery Information; Table B-
8B, Cumulative Volume of Free Product Recovered from Site; and Table B-9, Current and Historical
Groundwater Elevations and Free Product Thickness. Also refer to map( s) showing extent of free product in
Section J;
2. Identify any on-site or off-site effluent discharges, treatment used, effluent quality, permitting actions taken,
and location of such discharges and identify the disposition of recovered free product ( refer to attached
product disposal manifests);
3. Document the performance, total cost, and cost per gallon to date of each method of free product recovery
used at site. Justify why the technology is or was used;
Limited Site Assessment
2901 Monroe Road, Charlotte, North Carolina
February 26, 2024
8 Harmon Environmental, P A
615 Bruce Thomas Road, Monroe, North Carolina
[e-mail]
4. Provide conclusions and recommendations concerning historical, current, and future recovery activities,
including:
""' Any proposal to change the current method of free product recovery to a better or more cost -effective
technology;
""' A justification for continued product recovery, if planned; and
""' Any determination that free product has been eliminated from the site with a recommendation to
reclassify the risk posed by the release, if applicable.
No tree product was observed in conjunction with this assessment.
J. Figures
Provide the following:
1. A topographic map illustrating the area within 1500-foot radius of the UST system, showing:
s Topographic contours;
s Site location;
li3 Buildings;
s Adjacent streets, roads, highways (identified by street names and numbers);
s Surface water bodies;
1e1 Groundwater flow direction (if determined); and
s North arrow and scale.
See Attached Figure I.
2. A site map* and cross-sections illustrating the UST system(s), drawn to scale, showing:
s Buildings and property boundaries;
s Underground utilities, such as sewer lines and other conduits; basements; and vaults;
s Water supply wells, surface water bodies
s Location and orientation of current and former UST(s), pumps, product lines, sumps, etc.;
s Length, diameter and volume of current and former UST(s);
s Type ofmaterial(s) stored in UST(s) (currently and formerly);
s Final limits of each stage of excavation for each excavation on site; and
s North arrow and scale.
See Attached Figure 2.
3. Map(s)* and geological cross-sections, drawn to scale, depicting all soil analytical results obtained to
date, to include:
s Description of soil and bedrock lithology (as determined by investigation to date);
s Location and orientation ofUST(s), pumps, piping, sumps, etc.( current and former);
s Soil sample identification (unique letter and/or numerical code), location, and depth;
li3 Soil sample analytical results;
IE! Final limits of each stage of excavation for each excavation on site; and
s Two geological cross-sections, drawn across the contaminated area and intersecting at right angles,
showing the vertical distribution of the contaminants in the unsaturated zone. (Indicate vertical and
horizontal scale, orientation of each section, location of water table, soil types and lithology, all
borings and sample locations represented by the sections, and soil analytical results for each
represented sample, and show sections as labeled lines on the map.)
See Attached Figure 3.
4. Map(s)* and geological cross-sections, drawn to scale, depicting the groundwater and surface water
analytical results, to include:
s Location and orientation ofUST(s), pumps, piping, sumps, etc.( current and former);
Limited Site Assessment
2901 Monroe Road, Charlotte, North Carolina
February 26, 2024
9 Harmon Environmental, P A
615 Bruce Thomas Road, Monroe, North Carolina
[e-mail]
[eJ Groundwater sample identification (unique letter and/or numerical code referencing monitoring or
water supply well)and location;
13 Surface water sample identification (unique letter and/or numerical code) and location; and
13 Groundwater and surface water sample analytical results and
No geologic cross section or water table map has been prepared in conjunction with this project. See Attached
Fi re 3.
5. Map(s)* depicting groundwater elevations, to include:
~>=~ Potentiometric contour lines (if sufficient data points exist); and
13 Groundwater flow direction
No applicable to this Phase I Limited Site Assessment project.
6. A free product map* depicting thickness and extent of free product**
No applicable. no free-product was observed
7. A potential receptor map that clearly identifies water supply wells (municipal or public/private wells, etc.)
and other potential receptors (surface water bodies, basements, utilities, wellhead protection areas, etc.)
within 1500' of the source of the release.
See Attached Figure 4.
8. A land use map that identifies the following items within 1500' of the source of the release:
13 Features sensitive to impact from the release (schools, daycare centers, nursing homes, hospitals,
playgrounds, parks and recreation areas, churches, camps and other places of assembly):
s Properties within or contiguous to the area containing contamination or within and contiguous to the area
where the contamination is expected to migrate; and
13 Zoning status.
*Note: If possible, use a single base map to prepare site maps using a map scale of I inch= 40 feet (or a
smaller scale for large sites, if necessary). Maps and figures should include conventional symbols, notations,
labeling, legends, scales, and north arrows and should conform to generally accepted practices of map
presentation such as those enumerated in the USGS Geological Survey pamphlet, "Topographic Maps."
**If applicable
See Attached Figure 4.
K. Tables
Provide the following:
1. Site History (Complete Tables B-1 and B-2 from Guidelines, Appendix B);
2. Public and Private Water Supply Well and Other Receptor Information (Complete Table B-5 from
Guidelines, Appendix B);
3. Field Screening Results
4. Summary of Soil Sampling Results (Complete Table B-3 from Guidelines, Appendix B);
5. Summary of Groundwater Sampling and Surface Water Results (Complete Table B-4 from Guidelines,
Appendix B);
6. Monitoring and Remediation Well Construction Information (Complete Table B-7 from Guidelines,
Appendix B);
7. Free Product Recovery Information (Complete Table B-8A from Guidelines, Appendix B)*;
8. Cumulative Volume ofFree Product Recovered from Site (Complete Table B-8B from Guidelines,
Appendix B)*;
Limited Site Assessment
2901 Monroe Road, Charlotte, North Carolina
February 26, 2024
10 Harmon Environmental, P A
615 Bruce Thomas Road, Monroe, North Carolina
[e-mail]
9. Current and Historical Groundwater Elevations and Free Product Thickness (Complete Table B-9 from
Guidelines, Appendix B)*: and
11. Land Use (Complete Table B-10 from Guidelines, Appendix B).
*If applicable
A. Appendices
Provide the following:
Appendix A Site Specific Health and Safety Plan (HASP)
Appendix B Groundwater field measurements (pH, dissolved oxygen, specific conductivity,
Appendix C
AppendixD
AppendixE
AppendixF
Appendix G
AppendixH
Limited Site Assessment
temperature)
Standard procedures (sampling, field equipment decontamination, field screening, etc.)
Soil, water, free product, and sludge disposal manifests and soil treatment permits
Complete chain-of-custody records
Copy of all laboratory analytical records
Geologic logs for borings (related to LSA investigation only)
Monitoring Well Construction Forms (for all wells constructed to date)
11
2901 Monroe Road, Charlotte, North Carolina
February 26, 2024
Harmon Environmental, P A
615 Bruce Thomas Road, Monroe, North Carolina
[e-mail]
Figures
SOURCE: TOPO! 2003 NATIONAL GEOGRAPHIC
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA
704-292-4527
[e-mail]
APPROXIMATE SCALE IN FEET
0 2000
FIGURE 1
SITE LOCATION MAP
2901 MONROE ROAD
CHARLOTTE, NORTH CAROLINA
4000
0 ,-----. ~ I l ~ I WOODED
~~
I B2 I ~(\ I ~ \j $B1 _:j
MONROE ROAD
LEGEND
APPROXIMATE LOCATION OF
PROPERTY BOUNDARIES
APPROXIMATE LOCATION OF
TEMPORARY MONITORING WELL
APPROXIMATE LOCATION OF
SOIL BORING
APPROXIMATE LOCATION OF ON-SITE
VEGETATION APPROXIMATE SCALE IN FEET
I
0 so
I
100
SOURCE: MECKLENBURG COUNTY GIS AND FIELD MEASUREMENTS
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
[phone] PHONE & FAX
FIGURE 2
SITE LAYOUT MAP
2901 MONROE ROAD
CHARLOTTE, NORTH CAROLINA
MW-1(4)
ACETONE
C9 TO C18 ALIPHATICS
C19 TO C36 ALIPHATICS
C9 TO C22 AROMATICS
MW-1(8)
0.079 MG/KG
44.1 (J) MG!KG
55.5 (J) MG!KG
28.9 (J) MG!KG
ACETONE 0.047 MG/KG
METHYLENE CHLORIDE 0.005 (J) MG!KG
C9 TO C18 ALIPHATICS 39.8 (J) MG/KG
C19 TO C36 ALIPHATICS 47.9 (J) MG!KG
MW-1(12)
ACETONE 0.093 MG/KG
N-BUTYLBENZENE 0.024 MG/KG
SEC-BUTYLBENZENE 0.020 MG/KG
TERT-BUTYLBENZENE 0.002 (J) MG/KG
ETHYLBENZENE 0.003 (J) MG/KG
ISOPROPYLBENZENE 0.004 (J) MG/KG
METHYLENE CHLORIDE 0.003 (J) MG/KG
NAPHTHALENE 0.012 MG/KG
N-PROPYLBENZENE 0.006 MG/KG
XYLENES (TOTAL) 0.0009 (J) MG!KG
ACENAPHTHANE 0.677 (J) MG/KG
DIBENZOFURAN 0.623 (J) MG/KG FLUORANTHENE 0.211 (J) MG!KG
FLUORENE 1.22 MG!KG
1-METHYLNAPHTHALENE 2.84 MG/KG
PHENANTHRENE 0.649 (J) MG/KG
PYRENE 0.272 (J) MG/KG
C9 TO C18 ALIPHATICS 963.5 MG/KG
C19 TO C36 ALIPHATICS 190 MG/KG
C9 TO C22 AROMATICS 598.0 MG!KG
MONROE ROAD
LEGEND
APPROXIMATE LOCATION OF
PROPERTY BOUNDARIES
~ APPROXIMATE LOCATION OF
TEMPORARY MONITORING WELL
E9 APPROXIMATE LOCATION OF
SOIL BORING
v~ APPROXIMATE LOCATION OF
ON-SITE VEGETATION
(8) APPROXIMATE DEPTH OF SOIL
SAMPLE
MG/KG MILLIGRAMS PER KILOGRAM
ESTIM~TED CONCENTRATION
(J) BELOW THE ANALYTICAL METHOD
DETECTION LIMIT
TARGET ANALYTE RECOVERY WAS (~) OUTSIDE LABORATORY QUALITY
CONTROL LIMIT
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
[phone] PHONE & FAX
NOTES:
B3(12)
ACETONE 0.042 MG/KG
METHYLENE CHLORIDE 0.007 (J) MG!KG
B4(12)
4.03 MG!KG
2.21 MG/KG
0.264MG/KG
5.00MG/KG
1.65 MG!KG
0.091 (J) MG!KG
43.0MG!KG
4.62 MG!KG
N-BUTYLBENZENE
SEC-BUTYLBENZENE
TERT-BUTYLBENZENE
ETHYLBENZENE
ISOPROPYLBENZENE
4-ISOPROPYL TOLUENE
NAPHTHALENE
N-PROPYLBENZENE
XYLENES (TOTAL)
FLUORENE
1-METHYLNAPHTHALENE
2-METHYLNAPHTHALENE NAPHTHALENE
PHENANTHRENE
0.258 (J) MG/KG
CS TO C8 ALIPHATICS
C9 TO C18 ALIPHATICS
C19 TO C36 ALIPHATICS
C9 TO C22 AROMATICS
B2(12)
NAPHTHALENE
N-PROPYLBENZENE
C9 TO C18 ALIPHATICS
C19 TO C36 ALIPHATICS
C9 TO C22 AROMATICS
B1(12)
4.67 MG/KG
36.6.MG!KG
60.5 MG/KG
11.3 MG/KG
11.3 MG!KG
75.3 MG!KG
4,734MG/KG
792 (J) MG/KG
3,837 MG/KG
0.004 (J) MG!KG
0.001 (J) MG/KG
301 MG/KG
80.8 MG/KG
78.5 MG/KG
ACETONE 0.013 (J) MG/KG
METHYLENE CHLORIDE 0.004 (J) MG!KG
SOIL SAMPLES MW-1(4), MW-1(8, MW-1(12), B1(12), B2(12), B3(12) AND
B4(12) WERE COLLECTED BY HARMON ENVIRONMENTAL, PA
PERSONNEL ON JANUARY 26, 2024 AND ANALYZED BY WAYPOINT
ANALYTICAL,LLC FOR VOLATILE ORGANIC COMPOUNDS BY SW-846
METHOD 8260D FOLLOWING SAMPLE PREPARATION IN ACCORDANCE
WITH SW-846 METHOD 5035, SEMI-VOLATILE ORGANIC COMPOUNDS
BY SW-846 METHOD 8270E BN/A, AND VOLATILE AND EXTRACTABLE
PETROLEUM HYDROCARBON COMPOUNDS BY MASSACHUSETTS
METHODS.
APPROXIMATE SCALE IN FEET
0 50 100
SOURCE: MECKLENBURG COUNTY GIS AND FIELD MEASUREMENTS
FIGURE 3
SITE LAYOUT MAP WITH SOIL ANALYTICAL DATA
2901 MONROE ROAD
CHARLOTTE, NORTH CAROLINA
MW-1
ACETONE
BENZENE
N-BUTYLBENZENE
SEC-BUTYLBENZENE
TERT-BUTYLBENZENE
CHLOROMETHANE
ETHYLBENZENE
ISOPROPYLBENZENE
NAPHTHALENE
N-PROPYLBENZENE
TOLUENE
6.81 ug/L
0.460 (J) ug/L
2.89 ug/L
3.92 ug/L
0. 978 (J) ug/L
0.377 (J) ug/L
1.63 ug/L 3.48 (J) ug/L
25.4 ug/L
4.27 ug/L
0.479 (J) ug/L
0.595 ug/L
8.11 ug/L
6.69 ug/L
49.0 (M) ug/L
25.2 (M) ug/L
11.8 ug/L
I
I
XYLENES (TOTAL)
ACENAPHTHALENE
FLUORENE
1-METHYLNAPHTHALENE
2-METHYLNAPHTHALENE
NAPHTHALENE
PHEANTHRENE C9-C18 ALIPHATICS
C19-C36 ALIPHATICS
C9-C22 AROMATICS
18.3 ug/L
1,688 ug/L
1,090 ug/L
1,479 ug/L ~a I
I
_:j
MONROE ROAD
MG/KG
(J)
(M)
LEGEND
APPROXIMATE LOCATION OF
PROPERTY BOUNDARIES
APPROXIMATE LOCATION OF
TEMPORARY MONITORING WELL
APPROXIMATE LOCATION OF
SOIL BORING
APPROXIMATE LOCATION OF
ON-SITE VEGETATION
MICROGRAMS PER LITER
ESTIMATED CONCENTRATION
BELOW THE ANALYTICAL METHOD
DETECTION LIMIT
TARGETED ANALYTE RECOVERY WAS
OUTSIDE THE QC LIMITS. THESE
RESULTS ARE CONSIDERED A
MINIMUM VALUE DUE TO LOW BIAS
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
[phone] PHONE & FAX
NOTES:
GROUNDWATER SAMPLE MW-1 WAS COLLECTED BY HARMON
ENVIRONMENTAL. PA PERSONNEL ON JANUARY 27,2024 AND
ANALYZED BY WAYPOINT ANALYTICAL LLC FOR VOLATILE ORGANIC
COMPOUNDS BY SW-846 METHOD 8260D, SEMI-VOLATILE ORGANIC
COMPOUNDS BY SW-846 METHOD 8270E BN/A, VOLATILE AND
EXTRACT ABLE PETROLEUM HYDROCARBON COMPOUNDS BY
MASSACHUSETTS METHODS AND LEAD BY METHOD 6010D.
APPROXIMATE SCALE IN FEET
0 50 100
SOURCE: MECKLENBURG COUNTY GIS AND FIELD MEASUREMENTS
FIGURE 4
SITE LAYOUT MAP WITH GROUNDWATER
ANALYTICAL DATA
2901 MONROE ROAD
CHARLOTIE, NORTH CAROLINA
I 1
•
HARMON ENVIRONMENTAL PA
615 BltUCE'lHC»MS ltOAD
MONROE. NOJml CMOUNA
704 29Z..c527
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'MII.OIIEIMD DIJUIG 1HE.IANIMR'f ,_
FKiUIIE 5
ruRAOUNDING PROPEinY USAGE MAP
Z!IOI MONROE ltOAD
awu.arTE. NOJml CAROUNA
Tables
Table B-1: Site History-UST/AST System Information
Revision Date: 2/22/24 Incident Number and Name: Pending/2901 Monroe Road
.. :UST ID ,,
~JmHJer
No Tanks on
the site
.. ~< ~----• -~ t :~-+ Description ~ ,"'!:; ' 'l~ --CoristrucJion: ., Tank '·ofAssp<;iated
-.beta:ils;~*' ·: ,Dimensiolis• Piping an'd
. _' ~' , " · : ~.._,:·.~·~· ·-r~mJ!s ..
Date. Tank
Jnstalled
AppendixB
Reporting Tables
Add additional records as necessa
.. f;~"' ·· : .;;:~, ;..was re1~¢.ase, ·
Date Tanic;.-'Statl!~'of·· ja~soci!lfed, ,, Instan~d:, ,' ::-;·~~T:**;if~;', ~-:W~tp.:·~J:te').sr
•t '~:' ~ At ;~l ~;, ~~: '~ { --zt .,.~ "'?~t:. ;.,
* **
***
Add additional records as necessary
Gasoline (unleaded or leaded), diesel, used oil, waste oil, aviation fuel, etc., or pesticides, non-halogenated or halogenated solvents, etc.
Fiberglass (single-or double-walled), steel (single-or double-walled), steel with FRP (single-or double-walled), steel with liner, other, unknown.
Currently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removal·(specify
date)
Table B-2: Site History-UST Owner and Operator Information
Revision Date: 2/22/24 Incident Number and Name: Pendin /2901 Monroe Road
No Tanks on the Site
Unknown
· Sired ~·aar.ess ''" _.< ' • I - -
-State' '-Zi
Unknown
Street· Addreis ·? · . . '
di·. Stafe
· f~cnr1¥:,w;.~iff11:~etl
"t,~-1('('~ •• ' "
. .._., {l' <1-!~t~:/. t"'":_ ~ ~-~ .
N~e 9f oWn-er:
-~-~". ~~. ~~:·
,f ·,·~. ' •! . _. :~:" -~ ,;
Add additional records as necessary
8260D 8260D 8260D 8260D 8260D 8260D 8260D 8260D 8260D 8260D 8260D 8270E 8270E 8270E 8270E 8270E 8270E 8270E 8270E 8270E EPH&VPH EPH&VPH EPH&VPH VPH/EPH
Sample Date Source Sample IncidentID Collected Area Depth (ft) Phase
MW-1(4) 1/26/2024 4 LSA 0.079 <0.0006 <0.0007 <0.0006 <0.0007 <0.0006 <0.001 <0.001 <0.001 <0.00007 <0.0006 <0.142 <0.146 <0.151 <0.157 <0.130 <0.123 <0.177 <0.256 <0.165 <1.50 44.1(J) 55.5(J) 28.9(J)
MW-1(8) 1/26/2024 8 LSA 0.047 <0.0006 <0.0007 <0.0006 <0.0007 <0.0006 <0.001 0.005(J) <0.001 <0.0007 <0.0006 <0.145 <0.148 <0.153 <0.160 <0.132 <0.125 <0.180 <0.260 <0.167 <0.153 39.8(J) 47.9(J) <17.8MW-1(12) 1/26/2024 12 LSA 0.093 0.024 0.020 0.002(J) 0.003(J) 0.004(J) <0.001 0.003(J) 0.012 0.006 0.0009(J) 0.677(J) 0.623(J) 0.211(J) 1.22 2.84 <0.127 <0.183 0.649(J) 0.272(J) <1.56 963.5 190 598.0B1(12) 1/26/2024 12 LSA 0.013(J) <0.0006 <0.0007 <0.0007 <0.0008 <0.0006 <0.001 0.004(J) <0.001 <0.0007 <0.0007 <0.151 <0.155 <0.160 <0.167 <0.138 <0.130 <0.187 <0.271 <0.174 <1.59 <12.0 <15.9 <18.5B2(12) 1/26/2024 12 LSA <0.003 <0.0006 <0.0007 <0.0006 <0.0007 <0.0006 <0.001 <0.001 0.004(J) 0.001(J) <0.0006 <0.148 <0.152 <0.157 <0.164 <0.135 <0.128 <0.184 <0.266 <0.171 <1.56 301 80.8 78.5
B3(12) 1/26/2024 12 LSA 0.042 <0.0006 <0.0007 <0.0007 <0.0008 <0.0006 <0.001 0.007(J) <0.001 <0.0007 <0.0007 <0.153 <0.157 <0.162 <0.169 <0.140 <0.132 <0.190 <0.274 <0.177 <1.61 <12.2 <16.1 <18.9B4(12) 1/26/2024 12 LSA <0.076 4.03 2.21 0.264 5.00 1.65 0.091(J) <0.047 43.0 4.62 0.258(J) <0.148 <0.152 <0.157 4.67 36.6 60.5 11.3 11.2 <0.171 75.3 4,734 792(J) 3,837
24 2.4 2.2 1.7 8 1.3 0.12 0.023 0.2 1.4 6 20 5.2 330 55 0.054 1.5 0.2 64 210 68 540 # 3114,000 783 1,560 1,560 60.3 1,560 1,560 93.8 5.5 1,560 3,120 930 15.6 625 625 22.8 62.5 5.5 469 469 625 1,560 31,200 469210,000 11,600 23,300 23,300 297 23,300 23,300 1,400 27 23,300 46,700 14,000 233 9,340 9,340 112 934 27 7,000 7,000 93,340 23,300 467,000 7,000
Notes:
Sample Depth presented in feet below ground surfaceResults presented in milligrams per kilogram (mg/kg)OCs = Volatile Organic CompoundsSemi-VOCs = Semi Volatile Organic Compounds
PH = Volatile Petroleum Hydrocarbon EPH = Extractable Petroleum Hydrocarbons# = Considered immobile
Table B-3: Summary of Soil Sampling Results
Revision Date: 2/20/24 Incident Number and Name: Pending/2901 Monroe Rd.
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MSCC = Maximum Soil Contaminant Concentration
Residential MSCC (mg/kg)Industrial/Commerical MSCC (mg/kg)
Soil to Groundwater MSCC (mg/kg)
Analytical Method
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8260D 8260D 8260D 8260D 8260D 8260D 8260D 8260D 8260D 8260D 8260D 8260D 8270E 8270E 8270E 8270E 8270E 8270E EPH&VPH EPH&EPH EPH&VPH
MW-1 1/27/2024 MW-1 LSA 6.81 0.460(J) 2.89 3.92 0.978(J) 0.377(J) 1.63 3.48(J) 25.4 4.27 0.479(J) 0.595 8.11 6.69 49.0(M) 25.2(M) 11.8 18.3 1,688 1,090 1,479
6,000 1 70 70 70 3 600 70 6 70 600 500 80 300 1 30 6 200 700 10,000 200
6,000,000 5,000 6,900 8,500 15,000 3,000 84,500 25,000 6,000 30,000 70,000 85,500 2,120 990 1,000 12,500 6,000 410 NS NS NS
Indicate method detection limit for contaminents when analyzed, but not detected (e.g. <1, 10,42)
List any contaminants detected above the method detective limt
(μg/L) = micrograms per liter
GCL = gross contamination level
NS = No Standard
(J) = Estimated concentration beneath the analytical method detection limit(M) = Targeted analyte recovery was outside the QC Limits. These results should considered minimum diue to a low bias.
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Table B-4: Summary of Groundwater and Surface Water Sampling Results
Revision Date: 2/20/24 Incident Number and Name: Pending/2901 Monroe Rd. Facility ID# None
1-
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Contaminant of Concern →
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GCL (μg/L)
NC 2B Standard or EPA National Criteria (μg/L)
2L Standard (µg/L)
Incident Phase (Closure, 20 Day,
LSA, etc.)
Sample IDDate Collected
(mm/dd/yy)Well or SW ID
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'able B-5 Water Supply Well Information
AppendixB
Reports Format
tate: 2/26/24 Incident Number and Name: Pending/2901 Monroe Road Facility ID#: NA
nclude the following information. The well number (can use tax number), well owner and user names, addresses and telephone numbers, use of the well (potable,
~ricultural, etc.) Well depth, type of well (i.e., drilled, bored), well casing depth, well screen interval and distance of well from the source of the release).
t BGS = feet below ground surface
B-69 April2001
Table B-6
Date: February 26, 2024
<f.. ~~j. .. ~,, " "' . p,·· '1 y 1.''"~ -· T~2c .-arce
·:. Nu!riJJ"et/lviap:ID-·
15901101
15901144
15902124
Property Owners/Occupants
AppendixB
Reporting Tables
I Incident Number and Name: PendingJ2901 Monroe Road Facility ID#: NA
,. ,. ' _, ""'i,. " 'f ... _ . ' " -·· . ' " " " ,, >;c~j!~ "/~ ~~-':: \vr t' , •• " ' . .JL·""'' .~ '.-':f?W11eri?cc~l?ant~N~e .. :<i r'· ·x ~-;,.:·::-.. ·, ··l·;:. ~· $-~ •. ,. :,J 'l •t ·'i; ~ ~;>, "' .,_: ':r.t• 1 · ~ • (Last, FJ.q;t, NJ:l) ' .. ,:... . • l-4ailing-Addres~ ~-l-, ~ "" ; ~...! .... ~,. >(
3205 Freedom Drive, Suite 6000
Mecklenburg County Charlotte, NC 28208
300 Frank W Burr Suite 68
Charlotte Holdings 132 LLC Teaneak, NJ 07666
P.O. Box 320099
Cubesmart LP Alexandria, VA 22320
B-70 April2001
Table B-7 Well Construction Information
Date: Februarv 26 2024 Incident Number and Name: Pending/2901 Monroe Road
~~~4;.··" ,,
"'" ,. • .. ~ ·:Pate~~ ~~~ ' ., · '• Installe-d 1" \f~i't,ro ,J. ~ (mi~d!yy)
TMW-1 1126/24 1/27/24 10 10 to 20 20 NA 12.92
Reference Point for Elevation Measurements Top of Casing of Monitor Well MW-1, Assumed Elevation: I 00.00 ft.
AppendixB
Reporting Tables
Facility ID#: NA
"" -'::~: ~ ,j" h ;:-_;:. ·~
:1 i<,' ,;."!,! ~ Fre~-Prod~ct;~ :~·· \ ·~ ~ :-,, ·'-.-~::~¥: :: "
l?hicihress~k ' :~'rol)ndwat~r.~ ,·
:-~~. (tt~) pif.~* ~ ;-EI~vatiQ~ {ft;) .. -~Co_m-nrents
" ~· ,.!, ~ ·" i ' • " ' ~
None NA
*
** If free product is present in a well, groundwater elevation should be calculated by [Top of Casing Elevation-Depth to Water]+ [free product thickness x 0.8581]
B-71 April2001
Appendix A
Site Specific Health and Safety Plan
Site Specific Health and Safety Plan
~ for
Initial Abatement Activities
at
2901 Monroe Road, Charlotte, North Carolina
January 8, 2024
Prepared By:
Harmon Environmental, P A
615 Bruce Thomas Road
Monroe, North Carolina 28112
704-292-4527
Harmonenvironmental.com
This document is confidential and is to be used by designated project personnel. Reproduction of
this document is strictly prohibited unless approved in writing by Harmon Environmental, P A.
Signatures of Approval
ILL
Project Manager
Corporate Health and Safety Coordinator
Site Health and Safety Manager ' Date
I I
I~
I
Plan Acceptance
I have been permitted the opportunity to read this Health and Safety Plan for Initial Abatement
Activities at 2901 Monroe Road, Charlotte, North Carolina, and have been briefed by the Site
Safety Manager or an appropriately designated alternate on its content. All questions and
comments I have asked or stated regarding this Plan have been satisfactorily addressed. I
understand the contents of this Plan and agree to abide by its requirements.
Each person entering exclusion zones defined in Section 5.4 of this Plan shall sign below.
Table of Contents
Section Title Page No.
1.0 General Information 1
2.0 Project Organization 2
3.0 Site Description 2
4.0 Site Safety Control 2
5.0 Hazard Assessment/Personnel Protection 3
6.0 Decontaminating Procedures 4
7.0 Emergency Procedures 4
Figure Site Layout Map
Appendix A Exposure Limits of Chemical Hazardous
AppendixB Route to Hospital
1.0 General Information
1.1 Site Safety Plan Preparation:
Plan Prepared By: R. Harmon
Date Plan Approved: January 8, 2024
1.2 Site Information:
Site Name: MJP Monroe Road Holdings, LLC
Site Location: 2901 Monroe Road, Charlotte, NC
Site Contact: None
Site Status: Open (X ) Closed ( )
Limited Access ( ) Fenced ( )
Existing Site Information:
Detailed ( ) Sketch ( )
Preliminary (X) None ( )
Facility EPA I.D. No.:N/A
1.3 Hazardous Materials Information:
State/Form of Hazardous Materials:
Gas ( ) Liquid ( )
Groundwater (X) Sludge ( )
Material Hazards:
Corrosive ( )
Toxic ( )
Radioactive ( )
Volatile (X)
Reactive ( )
Unknown()
1.4 Scope of Work:
Soil (X)
Solid ( )
Ignitable ( )
Explosive ( )
Flammable ( )
Observe the installation of soil borings and one Type II monitor well. Collect soil
and groundwater samples for laboratory analysis.
Health and Safety Plan
2901 Monroe Road
Charlotte, NC
January 8, 2024
1 Harmon Environmental, PA
615 Bruce Thomas Road
Monroe, NC 28112
704-292-4527
2.0 Project Organization
Project Manager:
Corporate Health and Safety Coordinator:
Site Health and Safety Manager:
Technical Support:
Harmon Environmental Project No. 951-01
3.0 Site Description
Richard Harmon
Richard Harmon
Richard Harmon
Mid South Environmental, LLC
The site consists of a former service station. The former USTs have reportedly been removed.
There are no structures on the property.
4.0 Site Safety Controls
4.1 Site Map:
See attached figure
4.2 Perimeter Control:
No perimeter control is in place at the site.
4.3 Command Post Area:
The command post will be established outside of the exclusion zone at the subject site. A telephone
will be available at the command post area.
4.4 Exclusion Zones:
During the excavation activities, the exclusion zone shall be defined as a 15-foot radius around the
operating equipment.
4.5 Decontamination Area:
Should decontamination be required, it will be performed on-site.
5. 0 Hazard Assessment/Personnel Protection
5.1 General
Primary routes of potential exposure are through inhalation of dust, ingestion, and skin contact
with impacted soil and/or groundwater. Hazards include the physical hazard associated with
excavation, drilling and well advancement activities. Due to the outdoor location of the project
and expected hazards, moderate health risks are anticipated.
Health and Safety Plan
2901 Monroe Road
Charlotte, NC
January 8, 2024
2 Harmon Environmental, PA
615 Bruce Thomas Road
Monroe, NC 28112
704-292-4527
5.2 Health and Safety Training Requirements
All field personnel (including Subcontractors) must have appropriate hazardous waste site health
and safety training in accordance with OSHA 1910.120 regulations prior to initiating on-site
activities. The Site Safety Manager must have an additional 8 hours of specific site management
training.
5.3 Personnel Protection
General Level of Protection:
A ( ) B ( ) C ( ) D modified ( ) D(X)
LevelD:
For all personnel participating in the excavation and sampling activities, the following equipment
is required as a minimum:
• Chemical resistant outer gloves
• Steel toe and shank boots
• Standard work clothing (long-sleeve shirt and long pants)
• Hard hat and safety glasses.
• Ear protection (when noise levels preclude normal conversation)
5.4 Upgrading and Downgrading of Personnel Protection:
Upgrading and downgrading of personnel protection levels will be implemented if deemed
necessary by the Site Safety Manager. Any upgrades will be based on observed site conditions.
Under no circumstances will downgrading be permitted by any field personnel without the consent
of the Site Safety Manager.
6. 0 Decontamination Procedures
• Boots, boot covers, and gloves will be cleaned with phosphate-free soap and tap
water.
• Disposable coverings and equipment will be cleaned with phosphate-free soap and
tap water, then disposed of as normal trash.
Health and Safety Plan
2901 Monroe Road
Charlotte, NC
January 8, 2024
3 Harmon Environmental, PA
615 Bruce Thomas Road
Monroe, NC 28112
704-292-4527
• Sampling equipment will be cleaned with phosphate-free soap, and tap water,
followed by a distilled water rinse.
7. 0 Emergency Procedure
7.1 Field Communications: Hand signals when distressed; working m noisy
environment; or wearing respirators.
Thumbs up OK
Thumbs Down Not OK
Hands on wrist Exit Exclusion Zone
Hands on Throat Cannot Breathe
7.2 In the Event of Personnel Exposure:
Skin Contact: Flush with water, remove impacted clothing. Secure Medical
Attention
Inhalation:
Ingestion:
Move person away from exclusion zone, administer first aid and
CPR as necessary. Secure medical attention.
Secure medical attention.
Eye Contact: Irrigate with water. Secure medical attention.
7.3 Personnel Injury:
In the event a personnel injury occurs, decontaminate individual if injury is not life
threatening. If decontamination is not feasible, wrap the victim in a blanket,
administer first aid or CPR as necessary, contact the local rescue squad, and
hospital.
All injuries, exposures, or spills are to be documented by the Site Safety Manager
and reported to the Project Manager within 24 hours. Such documentation is to be
kept on file at Harmon Environmental, P A for future reference.
7.4 Heat Stress:
In the event of heat stress, move the victim out of the heat to a cool area on site.
Place the victim in shock position with their feet elevated. Cool the victim by
spraying with water or using wet towels and fanning. Secure medical attention.
Health and Safety Plan
2901 Monroe Road
Charlotte, NC
January 8, 2024
4 Harmon Environmental, PA
615 Bruce Thomas Road
Monroe, NC 28112
704-292-4527
7.5 First Aid Equipment:
A first aid kit is located within the support vehicles on-site. Potable water is available on-site.
7.6 Route to Hospital
See Appendix B
7. 7 Emergency Information:
Service
Ambulance
Fire Department
Police
Hospital (Novant Health Presbyterian Medical Center)
Charlotte Poison Control
North Carolina Department of Environment,
Health and Natural Resources
Region IV EPA
Mid South Environmental
Harmon Environmental, P A
951-0l.H&S
Health and Safety Plan
2901 Monroe Road
Charlotte, NC
January 8, 2024
5
Phone
911
911
911
[phone]
[phone]
(704 663-1699
[phone]
[phone]
[phone]
Harmon Environmental, PA
615 Bruce Thomas Road
Monroe, NC 28112
704-292-4527
A. _),
Figures
,.
Polaris 3G Map-Mecklenburg County, North Carolina
Date Printed: 1/8/2024 1:43:12 PM
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Appendix A
Exposure Limits of Chemical Hazards
CONOCO --GASOLINE,SUPERUNLEADED -GASOLINE,AUTOMOTIVE
MATERIAL SAFETY DATA SHEET
NSN: 9130010550816
Manufacturer's CAGE: 5R396
Part No. Indicator: A
Part Number/Trade Name: GASOLINE,SUPERUNLEADED
====--=====================---=============--============
General Information
===========================================================================
Item Name: GASOLINE,AUTOMOTIVE
Company's Name: CONOCO INC
Company's P. 0. Box: 2197
Company's City: HOUSTON
Company's State: TX
Company's Country: US
Company's Zip Code: 77252
Company's Emerg Ph #: 800-441-3637/800-424-9300(CHEMTREC)
Company's Info Ph #: 713-293-5550
Record No. For S~fety Entry: 031
Tot Safety Entries This Stk#: 044
Status: SE
Date MSDS Prepared: 16NOV92
Safety Data Review Date: 03AUG93
Supply Item Manager: KY
MSDS Serial Number: BRGZJ
Specification Number: ASTM D439
Spec Type, Grade, Class: SPECIAL GRADE
Hazard Characteristic Code: F2
Unit Of Issue: GL
Unit Of Issue Container Qty: 55 GALLONS
Type Of Container: DRUM,18 GAGE
Net Unit Weight: 334.3 LBS
===============================================~==========================
Ingredients/Identity Information
==~-====---==--==================================================~==========
Proprietary: NO
Ingredient: GASOLINE (INGREDIENTS BELOW ARE INCLUDED IN GASOLINE)
Ingredient Sequence Number: 01
Percent: 100
NIOSH (RTECS) Number: LX3300000
OSHA PEL: 300 PPM/500 STEL
ACGIH TLV: 300 PPM/500STEL;9293
Other Recommended Limit: NONE RECOMMENDED
Proprietary: NO
Ingredient: BENZENE (SARA III) (INCLUDED IN GASOLINE)
Ingredient Sequence Number: 02
Percent: 0.1-4.9
NIOSH (RTECS) Number: CY1400000
CAS Number: 71-43-2
OSHA PEL: 1PPM/SSTEL;1910.1028
ACGIH TLV: 10 PPM; A2; 9293
Other Recommended Limit: NONE RECOMMENDED
Proprietary: NO
Ingredient: ETHYL BENZENE (SARA III) (INCLUDED IN GASOLINE)
Ingredient Sequence Number: 03
Percent: 2
NIOSH (RTECS) Number: DA0700000
CAS Number: 100-41-4
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OSHA PEL: 100 PPM/125 STEL
ACGIH TLV: 100 PPM/125STEL 9293
Other Recommended Limit: NONE RECOMMENDED
Proprietary: NO
Ingredient: CUMENE (SARA III) (INCLUDED IN GASOLINE)
Ingredient Sequence Number: 04
Percent: 1
NIOSH (RTECS) Number: GR8575000
CAS Number: 98-82-8
OSHA PEL: S, 50 PPM
ACGIH TLV: S, 50 PPM; 9293
Other Recommended Limit: NONE RECOMMENDED
Proprietary: NO
Ingredient: PSEUDOCUMENE (1,2,4-TRIMETHYLBENZENE) (SARA III) (INCLUDED IN
GASOLINE)
Ingredient Sequence Number: 05
Percent: 2
NIOSH (RTECS) Number: DC3325000
CAS Number: 95-63-6
OSHA PEL: 25 PPM
ACGIH TLV: 25 PPM; 9293
Other Recommended Limit: NONE RECOMMENDED
Proprietary: NO
Ingredient: XYLENES (0-,M-,P-ISOMERS) (SARA III) (INCLUDED IN GASOLINE)
Ingredient Sequence Number: 06
Percent: 12
NIOSH (RTECS) Number: ZE2100000
CAS Number: 1330-20-7
OSHA PEL: 100 PPM/150 STEL
ACGIH TLV: 100 PPM/150STEL;9293
Other Recommended Limit: NONE RECOMMENDED
Proprietary: NO
Ingredient: TOLUENE (SARA III) (INCLUDED IN GASOLINE)
Ingredient Sequence Number: 07
Percent: 15
NIOSH (RTECS) Number: XS5250000
CAS Number: 108-88-3
OSHA PEL: 200 PPM/150 STEL
ACGIH TLV: 50 PPM; 9293
Other Recommended Limit: NONE RECOMMENDED
Proprietary: NO
Ingredient: METHYL TERT-BUTYL ETHER (SARA III) (INCLUDED IN GASOLINE)
Ingredient Sequence Number: 08
Percent: 0-15
NIOSH (RTECS) Number: KN5250000
CAS Number: 1634-04-4
OSHA PEL: NOT ESTABLISHED
ACGIH TLV: NOT ESTABLISHED
Other Recommended Limit: 100 PPM (MFR)
=--~===========================--=----=============--========================
Physical/Chemical Characteristics
==============================-===============================~==-=========
Appearance And Odor: WATER WHITE TO STRAW YELLOW LIQUIED. GASOLINE ODOR.
Boiling Point: 85-437F
Vapor Pressure (MM Hg/70 F); 200-475
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Vapor Density (Air=1): >1
Specific Gravity: 0.7-0.77
Decomposition Temperature: UNKNOWN
Evaporation Rate And Ref: UNKNOWN
Solubility In Water: SLIGHTLY SOLUBLE.
Percent Volatiles By Volume: 100
Corrosion Rate (IPY): UNKNOWN
Autoignition Temperature: 536F
=======================================================----======--======--==
Fire and Explosion Hazard Data
===--===================--=================--==---==--====
Flash Point: <-50F,<-46C
Flash Point Method: TCC
Lower Explosive Limit: <1
Upper Explosive Limit: 8
Extinguishing Media: USE CARBON DIOXIDE, FOAM, OR DRY CHEMICAL. WATER
STREAM MAY BE INEFFECTIVE.
Special Fire Fighting Proc: WEAR FIRE FIGHTING PROTECTIVE EQUIPMENT AND A
FULL FACED SELF CONTAINED BREATHING APPARATUS. COOL FIRE EXPOSED CONTAINERS
WITH WATER SPRAY.
Unusual Fire And Expl Hazrds: VAPORS CAN TRAVEL ALONG GROUND AND FLASHBACK
EXPLOSIVELY. CONTAINERS MAY BURST WITH HEAT OF FIRE. COMBUSTION PRODUCTS
MAY CONTAIN TOXIC CARBON MONOXIDE.
=========================================--=================================
Reactivity Data
~-====================================
Stability: YES
Cond To Avoid (Stability): HIGH HEAT, OPEN FLAMES, UNDUE EXPOSURE TO AIR.
Materials To Avoid: STRONG OXIDIZING AGENTS, HALOGENS, STRONG ACIDS AND
ALKALIES.
Hazardous Decamp Products: CARBON OXIDES AND VARIOUS HYDROCARBONS WHEN
BURNED.
Hazardous Poly Occur: NO
Conditions To Avoid (Poly): NOT APPLICABLE
=========================================--=========--=======================
Health Hazard Data
===============--========================----===========--=============--=====
LD50-LC50 Mixture: LD50 ORAL RAT IS UNKNOWN
Route Of Entry -Inhalation: YES
Route Of Entry -Skin: YES
Route Of Entry -Ingestion: NO
Health Haz Acute And Chronic: ACUTE: IRRITATION, CENTRAL NERVOUS SYSTEM
EFFECTS. GASOLINE IF SWALLOWED, MAY BE ASPIRATED INTO LUNGS, RESULTING IN
PULMONARY EDEMA AND CHEMICAL PNEUMONITIS. CHRONIC: BENZENE IS A CONFIRMED
CARCINOGEN AND MAY PRODUCE BLOOD CHANGES. PROLONGED EXPOSURE TO HIGH
CONCENTRATIONS HAS CAUSED KIDNEY AND LIVER CANCER IN RAT/MICE
Carcinogenicity -NTP: YES
Carcinogenicity -IARC: YES
Carcinogenicity -OSHA: YES
Explanation Carcinogenicity: BENZENE IS A CONFIRMED CARCINOGEN BY NTP,
IARC AND OSHA.
Signs/Symptoms Of Overexp: EYES/SKIN: IRRITATION. INHALATION: HEADACHE,
NAUSEA, WEAKNESS, SEDATION, AND UNCONSCIOUSNESS. INGESTION: IRRITATION OF
GASTROINTESTINAL SYSTEM. ASPIRATION AFTER INGESTION MAY CAUSE LUNG DAMAGE
AND DEATH.
Med Cond Aggravated By Exp: INDIVIDUALS WITH A HISTORY OF SKIN,
RESPIRATORY OR CENTRAL NERVOUS SYSTEM DISORDERS MAY BE AT INCREASED RISK
FROM EXPOSURE.
Emergency/First Aid Proc: EYES: FLUSH WITH PLENTY OF WATER FOR 15 MINUTES.
SEE DOCTOR. SKIN: REMOVE CONTAMINATED CLOTHING AND SHOES. WASH WITH SOAP
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AND WATER. SEE DOCTOR. INHALATION: REMOVE VICTIM TO FRESH AIR. GIVE
OXYGEN/CPR IF NEEDED. SEE DOCTOR. INGESTION: DO NOT INDUCE VOMITING. SEE
DOCTOR IMMEDIATELY. *** NOTE TO PHYSICIAN: ACTIVATED CHARCOAL SLURRY MAY BE
ADMINISTERED ***
=======================~=====m--====--==========---~======================
Precautions for Safe Handling and Use
=======================================-----================~==============
Steps If Matl Released/Spill: ELIMINATE IGNITION SOURCES. VENTILATE AREA.
USE NON-SPARKING TOOLS. WEAR PROPER PROTECTIVE EQUIPMENT. STOP LEAK AND
CONTAIN SPILL. ABSORB IN INERT ABSORBENT AND PLACE INTO APPROPIATE DISPOSAL
CONTAINER AND SEAL. WASH AREA WITH PLENTY OF WATER.
Neutralizing Agent: NOT APPLICABLE
Waste Disposal Method: CONSULT YOUR LOCAL ENVIRONMENTAL OFFICER. DISPOSE
OF IN ACCORDANCE WITH ALL APPLICABLE FEDERAL, STATE AND LOCAL ENVIRONMENTAL
REGULATIONS. BY ITSELF THE LIQUID IS EXPECTED TO BE A RCRA IGNITABLE
HAZARDOUS WASTE.
Precautions-Handling/Storing: STORE IN COOL, DRY, WELL VENTILATED PLACE,
AWAY FROM HEAT, IGNITION SOURCES AND INCOMPATIBLE MATERIALS. KEEP
CONTAINERS CLOSED.
Other Precautions: AVOID BREATHING VAPORS, AND EYE AND SKIN CONTACT. USE
ONLY WITH ADEQUATE VENTILATION. DO NOT SIPHON BY MOUTH. BOND AND GROUND
CONTAINERS DURING TRANSFER. PROTECT CONTAINERS FROM PHYSICAL DAMAGE.
====================--=========---====================
Control Measures
============--======================--====================
Respiratory Protection: NIOSH/MSHA RESPIRATOR WITH ORGANIC VAPOR CARTRIDGE
APPROPIATE FOR EXPOSURE OF CONCERN OR SCBA IF TLV IS EXCEEDED.
Ventilation: SUFFICIENT MECHANICAL (GENERAL) AND/OR LOCAL EXHAUST
VENTILATION. USE EXPLOSION-PROOF EQUIPMENT.
Protective Gloves: NBR, VITON, NITRILE, PVA.
Eye Protection: SAFETY GLASSES WITH SIDE SHIELDS.
Other Protective Equipment: FULL BODY LONG-SLEEVED GARMENTS TO PREVENT
REPEATED OR PROLONGED SKIN CONTACT. EYE WASH STATION AND SAFETY SHOWER.
Work Hygienic Practices: AVOID CONTACT WITH EYES AND SKIN. DO NOT BREATHE
VAPORS. WASH THOROUGHLY AFTER HANDLING. LAUNDER CONTAMINATED CLOTHING.
Suppl. Safety & Health Data: THESE PRECAUTIONS ARE FOR NORMAL USES AND
CONDITIONS. WHERE SPECIAL OR UNUSUAL CONDITIONS EXIST, CONSULT AN
INDUSTRIAL HYGIENIST. RCRA CLASSIFICATION IGNITABLE (D001). EP TOXIC
(U019).
==========-=====================--===--===========--==========--===============
Transportation Data
===========================================================================
Trans Data Review Date: 93215
DOT PSN Code: GTN
DOT Proper Shipping Name: GASOLINE
DOT Class: 3
DOT ID Number: UN1203
DOT Pack Group: II
DOT Label: FLAMMABLE LIQUID
IMO PSN Code: HRV
IMO Proper Shipping Name: GASOLINE
IMO Regulations Page Number: 3141
IMO UN Number: 1203
IMO UN Class: 3.1
IMO Subsidiary Risk Label: -
IATA PSN Code: MUC
IATA UN ID Number: 1203
IATA Proper Shipping Name: GASO~INE
IATA UN Class: 3
IATA Label: FLAMMABLE LIQUID
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AFI PSN Code: MUC
AFI Prop. Shipping Name: GASOLINE
AFI Class: 3
AFI ID Number: UN1203
AFI Pack Group: II
AFI Basic Pac Ref: 7-7
Additional Trans Data: BENZENE REPORTABLE QUANTITY IS 10 POUNDS.
=================================================-~~====~=================
Disposal Data
=================-=========================================================
=-
Label Data
==================================================================--========
Label Required: YES
Technical Review Date: 06AUG93
Label Status: F
Common Name: GASOLINE,SUPERUNLEADED
Signal Word: DANGER!
Acute Health Hazard-Moderate: X
Contact Hazard-Slight: X
Fire Hazard-Severe: X
Reactivity Hazard-None: X
Special Hazard Precautions: ACUTE: IRRITATION, CENTRAL NERVOUS SYSTEM
EFFECTS. GASOLINE IF SWALLOWED, MAY BE ASPIRATED INTO LUNGS, RESULTING IN
PULMONARY EDEMA AND CHEMICAL PNEUMONITIS. CHRONIC: BENZENE IS A CONFIRMED
CARCINOGEN AND MAY PRODUCE BLOOD CHANGES. PROLONGED EXPOSURE TO HIGH
EYES: FLUSH WITH PLENTY OF WATER FOR 15 MINUTES. SEE DOCTOR. SKIN: REMOVE
CONTAMINATED CLOTHING AND SHOES. WASH WITH SOAP AND WATER. SEE DOCTOR.
INHALATION: REMOVE VICTIM TO FRESH AIR. GIVE OXYGEN/CPR IF NEEDED. SEE
DOCTOR. INGESTION: DO NOT INDUCE VOMITING. SEE DOCTOR IMMEDIATELY.
Protect Eye: Y
Protect Skin: Y
Label Name: CONOCO INC
Label P.O. Box: 2197
Label City: HOUSTON
Label State: TX
Label Zip Code: 77252
Label Country: US
Label Emergency Number: 800-441-3637/800-424-9300(CHEMTREC)
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·-
~ONOCO --DIESEL FUEL NO. 2 -DIESEL FUEL
1ATERIAL SAFETY DATA SHEET
~SN: 9140002865296
~anufacturer's CAGE: 15445
?art No. Indicator: A
?art Number/Trade Name: DIESEL FUEL NO. 2
General Information
m--==============
=====================================~===================================
Item Name: DIESEL FUEL
:ompany's Name: CONOCO INC
:ompany's Street: 600 N DAIRY ASHFORD RD RM 3012
~ompany's P. 0. Box: 4784
8ompany's City: HOUSTON
8ompany's State: TX
Company's Country: US
Company's Zip Code: 77210-4784
Company's Emerg Ph #: 713-293-5550/800-424-9300
Company's Info Ph #: 713-293-5550
Record No. For Safety Entry: 029
Tot Safety Entries This Stk#: 093
Status: SMU
Date MSDS Prepared: 14AUG91
Safety Data Review Date: 24JUN92
Supply Item Manager: KY
MSDS Serial Number: BMZTT
Specification Number: VV-F-800
Spec Type, Grade, Class: GRADE DF-2
Hazard Characteristic Code: F4
===========================================================================
Ingredients/Identity Information
===========================================================================
Proprietary: NO
Ingredient: PETROLEUM MID-DISTILLATE (DIESEL MARINE FUEL)
Ingredient Sequence Number: 01
Percent: 100 %
NIOSH (RTECS) Number: 1004302PE
CAS Number: 68476-34-6
OSHA PEL: 5 MG/M3 AS OIL MIST
ACGIH TLV: 5 MG/M3 AS OIL MIST
Other Recommended Limit: NONE SPECIFIED
===============================~====================--=====================
Physical/Chemical Characteristics
===========================================================================
Appearance And Odor: CLEAR OR LIGHT YELLOW LIQUID, AROMATIC ODOR
Boiling Point: 350 -680F
Melting Point: NOT GIVEN
Vapor Pressure (MM Hg/70 F): 1 MMHG
Vapor Density (Air=1): > 1
Specific Gravity: 0.85 -0.93
Decomposition Temperature: NOT GIVEN
Evaporation Rate And Ref: NIL
Solubility In Water: INSOLUBLE
Percent Volatiles By Volume: NIL
Corrosion Rate (IPY): UNKNOWN
==--===--~-================================================~===============
Fire and Explosion Hazard Data
=============================--===============--=================---~========
Flash Point: 130F,54C
Flash Point Method: TCC
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Lower Explosive Limit: 0.4 %
Upper Explosive Limit: 6 %
Extinguishing Media: WATER SPRAY, FOAM, DRY CHEMICAL CAARBON DIOXIDE
Special Fire Fighting Proc: USE WATER TO KEEP FIRE-EXPOSED CONTAINERS
COOL. IF LEAK OR SPILL HAS NOT IGNITIED, USE WATER SPRAY TO DISPERSE THE
VAPORS AND TO PROVIDE PROTECTION.
Unusual Fire And Expl Hazrds: PRODUCTS OF COMBUSTION MAY CONTAIN CARBON
MONOXIDE, CARBON DIOXIDE AND OTHER TOXIC MATERILS. DO NOT ENTER ENCLOSED OR
CONFINED SPACE WITHOUT PROPER PPE.
===~-=========================================--=======--===================
Reactivity Data
===================================--=======================================
Stability: YES
Cond To Avoid (Stability): AVOID HEAT AND FLAME
Materials To Avoid: INCOMATIBLE WITH OXIDIZING MATERIALS.
==========================================================--================
Health Hazard Data
===============--=======================================--========--==========
===================================================--=======================
Precautions for Safe Handling and Use
=============--=====================--=========--===--===========--=====---=--=== ===============--===========================================================
Control Measures
==============================--============--=====--=========================
====================================================--======================
Transportation Data
==============--================================--===========================
=========================================================================--=
Disposal Data
================================================-==========================
==============================================--============================
Label Data
==============================================----=======
Label Required: YES
Technical Review Date: 24JUN92
MFR Label Number: NONE
Label Status: G
Common Name: DIESEL FUEL NO. 2
Chronic Hazard: NO
Signal Word: CAUTION!
Acute Health Hazard-Slight: X
Contact Hazard-Slight: X
Fire Hazard-Slight: X
Reactivity Hazard-None: X
Special Hazard Precautions: STORE IN WELL VENTILATED AREEA. KEEP CONTAINER
TIGHTLY CLOSED. STORE IN ACCORDANCE WITH NATIONAL FIRE PROTECTION ASSN
REGULATIONS. FIRST AID: INHALATION: REMOVE TO FRESH AIR. IF NOT BREATHING,
GIVE ARTIFICIAL RESPIRATION. IF BREATHING IS DIFFICULT, GIVE OXYGEN. CALL A
PHYSICIAN. SKIN: FLUSH SKIN WITH WATER AFTER CONTACT. REMOVE CONTAMINATED
CLOTHING. EYES: IMMEDIATELY FLUSH WITH WATER FOR 15 MINUTES. CALL A
PHYSICIAN. INGESTION: DO NOT INDUCE VOMITING. IMMEDIATELY GIVE TWO GLASSES
OF WATER. NEVER GIVE ANYTHING TO IF UNCONCIOUS. CALL MD
Protect Eye: Y
Protect Skin: Y
Label Name: CONOCO INC
Label Street: 600 N DAIRY ASHFORD RD RM 3012
Label P.O. Box: 4784
Label City: HOUSTON
Label State: TX
Label Zip Code: 77210-4784
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--·g-··----
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.>. "5"" J U.L ..1
Label Country: US
Label Emergency Number: 713-293-5550/800-424-9300
~. I
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AppendixB
Route to Hospital
1/8/24, 2:22PM 2901 Monroe Rd , Charlotte, NC 28205 to Novant Health Presbyterian Medical Center-Google Maps .
G o gle Maps 2901 Monroe Rd, Charlotte, NC 28205 to Novant Health Drive 1.6 miles, 5 min
Presbyterian Medical Center, 200 Hawthorne Ln, Charlotte, NC 28204
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viaE 7th St
Fastest route now due to traff1c
conditions
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viaE 5th St
Smin
1.6 miles
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1.5 miles
6min
1.4 miles
Explore nearby Novant Health Presbyterian
Medical Center
p •••
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https:/ /www.google .com/maps/dir/290 1 +Monroe+Rd, +Charlotte, +NC+ 28205/Novant+Health+Presbyterian+Medicai+Center, + 200+ Hawthorne+Ln, +Ch ... 1 /1
Appendix B
Groundwater Field Measurements
(pH, Dissolved Oxygen, Specific Conductivity,
Temperature)
(!'his Appendix was not used as a part of this Assessment)
Appendix C
Standard Procedures
(Sampling, Field Equipment Decontamination, Field
Screening, etc.)
Typical Standard Procedures
Soil and Groundwater Sampling Activities Associated with Geoprobe® Borings and
Monitor Well Installation
Harmon Environmental, PA routinely retains North Carolina Licensed Well Contractors
to advance Geoprobe® borings and construct monitor wells. Since these services are
provided by a Licensed Professional, the procedures associated with these activities are
not addressed in this summary.
Soil Sample Collection and Screening Activities
As each Geoprobe® sample is recovered from the boring, the liner is opened by the
driller anq delivered to Harmon Environmental, ·p A personnel. Prior to evaluating the
sample, a sample aliquot is stored in a labeled zipper sealed bag in a cooler on ice. Each
zipper seal bag is labeled with a sample designation, time, date, approximate depth and
sampler's initials at the time of collected. Following collection and storage of this
portion of the soil sample, the remaining portion of each sample is visually described and
a second sample aliquot is placed into a zipper sealed bag and screened for the presence
of volatile organic vapor using a Multi-Rae® photoionizing organic vapor detector (PID),
or equivalent, calibrated to an isobutylene standard. New latex gloves, or equivalent, are
typically worn throughout the collection of each sample.
Based on the results of the field screening activities, Harmon Environmental, P A field
personnel selected samples for laboratory analyses. Prior to transferring each selected
sample from the zipper sealed bag into the laboratory supplied glassware, new latex
gloves, or equivalent, are donned, and the laboratory supplied sample bottles are labeled.
Each soil sample is then transferred directly from the original zipper sealed bag directly
into the pre-labeled glassware provided by the laboratory. These samples are then
placed in a cooler on ice pending delivery under chain-of-custody protocol to the
analyzing laboratory.
The depth of each sample, the location of each sample, the time of sample collection, the
field screening results and any deviations from these standard protocols are documented
in the field notes prepared in conjunction with each project.
Groundwater Sample Collection Activities
Prior to collecting groundwater samples, the monitor well is opened and allowed to
equilibrate, if necessary. The water level is than measured to the nearest 0.01 feet from
the highest point at the top of the well casing using an electric depth-to-water probe.
Based on the measured depth to water, the volume of water in the well is calculated and
the well is purged of three well volumes, or until dry. The purging process is completed
using a new disposable bailer and nylon cord. New latex gloves, or equivalent, are worn
throughout the well purging process.
Following completion of the well pp.rging process, groundwater samples are collected by
pouring water directly from the bailer into pre-labeled glassware supplied by the
analyzing laboratory. Samples are collected in order of decreasing volatility. As
collected, the bottles are placed in a cooler on ice pending delivery under chain-of­
custody protocol to the analyzing laboratory.
Each sample bottle is labeled with sample identification information discrete to the
specific event. The time and date of sample collection, any field screening results and any
deviations from these standard protocols are documented in the field notes prepared in
conjunction with each project.
AppendixD
Soil, Water, Free-Product, and Sludge Disposal Manifests
and Soil Treatment Permits
(This Appendix not used as a part of this Assessment)
AppendixE
Completed Chain-of-Custody Records
··~·· GH~IN oF c,usrooy Recafip
: .. -:}·')., .. :· .Ji • r''""" "". . . qyon; ... · ,
' •'
QSC t:INC OSC 1:1 0 1:1 __ _
*CdNJ:AINER TYPE CODE:S: A"' Amber G=Giass
REMARKS
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4-ll 0
C'l C'l
-l'----'"":,-,1 ,-1.
Q)
"01' ~__,......,..-l 11!..,, AI,.,
~-.-.~u.uy a1mo:
Field TI!Ch Feo:
SEE REVERSE FOR
TERMS & CONDil'lONS
ORIGINAL.
AppendixF
Copy of All Laboratory Analytical Records

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

2/9/2024
Harmon Environmental, PA Rick Harmon
615 Bruce Thomas Rd. Monroe, NC, 28112
Ref: Analytical Testing
Lab Report Number: 24-031-0014 Client Project Description: Souther States
Dear Rick Harmon:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 1/31/2024 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 122
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2024402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Page 1 of 1 00016/24-031-0014
Page 2 of 122
Report Number:
Sample Summary Table
Client Project Description:
24-031-0014
Souther States
Lab No Client Sample ID Matrix Date Collected Date Received
01/27/2024 09:30Aqueous 95680 MW-1 01/31/2024 14:30
01/26/2024 09:35Solids 95681 MW-1 (4)01/31/2024 14:30
01/26/2024 09:40Solids 95682 MW-1 (8)01/31/2024 14:30
01/26/2024 09:43Solids 95683 MW-1 (12)01/31/2024 14:30
01/26/2024 10:38Solids 95684 B1 (12)01/31/2024 14:30
01/26/2024 11:00Solids 95685 B2 (12)01/31/2024 14:30
01/26/2024 11:25Solids 95686 B3 (12)01/31/2024 14:30
01/26/2024 11:55Solids 95687 B4 (12)01/31/2024 14:30
Page 3 of 122
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
24-031-0014
Report Limit
Project:Souther States
V 95680MW-1
6.81 02/08/2024 00:198260DAcetoneµg/L 1.80
J0.460 02/08/2024 00:198260DBenzeneµg/L 0.180
2.89 02/08/2024 00:198260Dn-Butylbenzene µg/L 0.185
3.92 02/08/2024 00:198260Dsec-Butyl benzene µg/L 0.200
J0.978 02/08/2024 00:198260Dtert-Butyl benzene µg/L 0.920
J0.377 02/08/2024 00:198260DChloromethaneµg/L 0.220
1.63 02/08/2024 00:198260DEthylbenzeneµg/L 0.170
J3.48 02/08/2024 00:198260DIsopropylbenzeneµg/L 0.180
25.4 02/08/2024 00:198260DNaphthaleneµg/L 0.470
4.27 02/08/2024 00:198260Dn-Propylbenzene µg/L 0.190
J0.479 02/08/2024 00:198260DTolueneµg/L 0.220
0.595 02/08/2024 00:198260Do-Xylene µg/L 0.210
0.595 02/08/2024 00:198260DXylene (Total)µg/L 0.210
8.11 02/06/2024 23:458270EAcenaphtheneµg/L 0.302
6.69 02/06/2024 23:458270EFluoreneµg/L 0.807
M49.0 02/06/2024 23:458270E1-Methylnaphthalene µg/L 1.14
M25.2 02/06/2024 23:458270E2-Methylnaphthalene µg/L 0.666
11.8 02/06/2024 23:458270ENaphthaleneµg/L 0.728
18.3 02/06/2024 23:458270EPhenanthreneµg/L 0.428
1410 02/08/2024 16:24MADEP-EPH Aliphatic C9-C18 µg/L 28.2
1090 02/08/2024 16:24MADEP-EPH Aliphatic C19-C36 µg/L 248
1250 02/08/2024 16:24MADEP-EPH Aromatic C11-C22 µg/L 61.2
278 02/01/2024 17:01MADEP-VPH Aliphatic C9-C12 µg/L 25.8
229 02/01/2024 17:01MADEP-VPH Aromatic C9-C10 µg/L 4.02
V 95681MW-1 (4)
0.079 01/31/2024 22:308260DAcetonemg/Kg - dry 0.002
J44.1 02/07/2024 19:42MADEP-EPH Aliphatic C9-C18 mg/Kg - dry 11.3
J55.5 02/07/2024 19:42MADEP-EPH Aliphatic C19-C36 mg/Kg - dry 15.0
J28.9 02/07/2024 19:42MADEP-EPH Aromatic C11-C22 mg/Kg - dry 17.4
18.8 02/02/2024 11:55SW-DRYWT Moisture %
V 95682MW-1 (8)
0.047 01/31/2024 22:578260DAcetonemg/Kg - dry 0.003
J0.005 01/31/2024 22:578260DMethylene Chloride mg/Kg - dry 0.001
J39.8 02/07/2024 20:19MADEP-EPH Aliphatic C9-C18 mg/Kg - dry 11.5
J47.9 02/07/2024 20:19MADEP-EPH Aliphatic C19-C36 mg/Kg - dry 15.3
Page 4 of 122
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
24-031-0014
Report Limit
Project:Souther States
V 95682MW-1 (8)
20.1 02/02/2024 11:55SW-DRYWT Moisture %
V 95683MW-1 (12)
0.093 02/01/2024 01:408260DAcetonemg/Kg - dry 0.003
0.024 02/01/2024 01:408260Dn-Butylbenzene mg/Kg - dry 0.0006
0.020 02/01/2024 01:408260Dsec-Butyl benzene mg/Kg - dry 0.0007
J0.002 02/01/2024 01:408260Dtert-Butyl benzene mg/Kg - dry 0.0006
J0.003 02/01/2024 01:408260DEthylbenzenemg/Kg - dry 0.0007
J0.004 02/01/2024 01:408260DIsopropylbenzenemg/Kg - dry 0.0006
J0.003 02/01/2024 01:408260DMethylene Chloride mg/Kg - dry 0.001
0.012 02/01/2024 01:408260DNaphthalenemg/Kg - dry 0.001
0.006 02/01/2024 01:408260Dn-Propylbenzene mg/Kg - dry 0.0007
J0.0009 02/01/2024 01:408260Do-Xylene mg/Kg - dry 0.0006
J0.0009 02/01/2024 01:408260DXylene (Total)mg/Kg - dry 0.0006
J0.677 02/06/2024 20:328270EAcenaphthenemg/Kg - dry 0.147
J0.623 02/06/2024 20:328270EDibenzofuranmg/Kg - dry 0.151
J0.211 02/06/2024 20:328270EFluoranthenemg/Kg - dry 0.156
1.22 02/06/2024 20:328270EFluorenemg/Kg - dry 0.163
2.84 02/06/2024 20:328270E1-Methylnaphthalene mg/Kg - dry 0.135
J0.649 02/06/2024 20:328270EPhenanthrenemg/Kg - dry 0.265
J0.272 02/06/2024 20:328270EPyrenemg/Kg - dry 0.170
918 02/08/2024 13:35MADEP-EPH Aliphatic C9-C18 mg/Kg - dry 58.9
190 02/07/2024 20:55MADEP-EPH Aliphatic C19-C36 mg/Kg - dry 15.6
571 02/08/2024 13:35MADEP-EPH Aromatic C11-C22 mg/Kg - dry 90.9
45.5 02/01/2024 00:51MADEP-VPH Aliphatic C9-C12 mg/Kg - dry 5.82
27.0 02/01/2024 00:51MADEP-VPH Aromatic C9-C10 mg/Kg - dry 0.795
21.6 02/02/2024 11:55SW-DRYWT Moisture %
V 95684B1 (12)
J0.013 01/31/2024 23:248260DAcetonemg/Kg - dry 0.003
J0.004 01/31/2024 23:248260DMethylene Chloride mg/Kg - dry 0.001
23.4 02/02/2024 11:55SW-DRYWT Moisture %
V 95685B2 (12)
J0.004 01/31/2024 23:528260DNaphthalenemg/Kg - dry 0.001
J0.001 01/31/2024 23:528260Dn-Propylbenzene mg/Kg - dry 0.0007
301 02/07/2024 22:08MADEP-EPH Aliphatic C9-C18 mg/Kg - dry 11.8
80.8 02/07/2024 22:08MADEP-EPH Aliphatic C19-C36 mg/Kg - dry 15.6
Page 5 of 122
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
24-031-0014
Report Limit
Project:Souther States
V 95685B2 (12)
78.5 02/07/2024 22:08MADEP-EPH Aromatic C11-C22 mg/Kg - dry 18.2
22.0 02/02/2024 11:55SW-DRYWT Moisture %
V 95686B3 (12)
0.042 02/01/2024 00:198260DAcetonemg/Kg - dry 0.003
J0.007 02/01/2024 00:198260DMethylene Chloride mg/Kg - dry 0.001
24.3 02/02/2024 11:55SW-DRYWT Moisture %
V 95687B4 (12)
4.03 02/01/2024 03:028260Dn-Butylbenzene mg/Kg - dry 0.015
2.21 02/01/2024 03:028260Dsec-Butyl benzene mg/Kg - dry 0.017
0.264 02/01/2024 03:028260Dtert-Butyl benzene mg/Kg - dry 0.015
5.00 02/01/2024 03:028260DEthylbenzenemg/Kg - dry 0.018
1.65 02/01/2024 03:028260DIsopropylbenzenemg/Kg - dry 0.014
J0.091 02/01/2024 03:028260D4-Isopropyl toluene mg/Kg - dry 0.041
43.0 02/01/2024 03:298260DNaphthalenemg/Kg - dry 0.317
4.62 02/01/2024 03:028260Dn-Propylbenzene mg/Kg - dry 0.017
0.424 02/01/2024 03:028260D1,3,5-Trimethylbenzene mg/Kg - dry 0.017
0.167 02/01/2024 03:028260Do-Xylene mg/Kg - dry 0.015
J0.090 02/01/2024 03:028260Dm,p-Xylene mg/Kg - dry 0.040
J0.258 02/01/2024 03:028260DXylene (Total)mg/Kg - dry 0.015
4.67 02/06/2024 22:268270EFluorenemg/Kg - dry 0.163
36.6 02/07/2024 14:238270E1-Methylnaphthalene mg/Kg - dry 1.36
60.5 02/07/2024 14:238270E2-Methylnaphthalene mg/Kg - dry 1.28
11.3 02/07/2024 14:238270ENaphthalenemg/Kg - dry 1.84
11.2 02/07/2024 14:238270EPhenanthrenemg/Kg - dry 2.66
4410 02/08/2024 12:58MADEP-EPH Aliphatic C9-C18 mg/Kg - dry 234
J79202/08/2024 12:58MADEP-EPH Aliphatic C19-C36 mg/Kg - dry 311
3620 02/08/2024 12:58MADEP-EPH Aromatic C11-C22 mg/Kg - dry 362
75.3 02/01/2024 01:38MADEP-VPH Aliphatic C5-C8 mg/Kg - dry 7.77
324 02/01/2024 01:38MADEP-VPH Aliphatic C9-C12 mg/Kg - dry 29.2
217 02/01/2024 01:38MADEP-VPH Aromatic C9-C10 mg/Kg - dry 3.99
21.8 02/02/2024 11:55SW-DRYWT Moisture %
Page 6 of 122

Client: Harmon Environmental, PA CASE NARRATIVE
Project: Souther States Lab Report Number: 24-031-0014
Date: 2/8/2024
Massachusetts EPH Method MADEP-EPH Sample 95680 (MW-1) QC Batch No: V43310
Surrogate recovery(s) was flagged as outside QC limits due to high levels of target and/or non-target analytes. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Sample 95687 (B4 (12))
QC Batch No: V43311 Surrogate recovery(s) was flagged as outside QC limits due to high levels of target and/or non-target analytes.
Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Analyte: Aliphatic C9-C18 QC Batch No: V43310/V43206
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias. LCS fails low for this range. All other QC passes within method parameters. No further action taken.
Semivolatile Organic Compounds - GC/MS Method 8270E Analyte: 1-Methylnaphthalene QC Batch No: V43253/V43104 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias.
Analyte: 2-Methylnaphthalene QC Batch No: V43253/V43104
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias.
Analyte: Dibenz(a,h)anthracene QC Batch No: V43253/V43104
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Analyte: Pyridine QC Batch No: V43253/V43104 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Sample 95681 (MW-1 (4)) Analyte: Benzoic Acid QC Batch No: V43256/V43183 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Page 7 of 122

Page 8 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1
95680 Matrix:
1/27/2024 9:30
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.003 mg/L 0.003 0.006Lead 1 02/08/24 05:21 6010DJKC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 9 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1
95680 Matrix:
1/27/2024 9:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V43357 02/07/24 14:00
6.81 µg/L 1.80 5.00Acetone 1 02/08/24 00:19 V43359MSA
<2.00 µg/L 2.00 5.00Acrolein 1 02/08/24 00:19 V43359MSA
<0.230 µg/L 0.230 5.00Acrylonitrile 1 02/08/24 00:19 V43359MSA
0.460 J µg/L 0.180 0.500Benzene 1 02/08/24 00:19 V43359MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 02/08/24 00:19 V43359MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 02/08/24 00:19 V43359MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 02/08/24 00:19 V43359MSA
<1.50 µg/L 1.50 5.00Bromoform 1 02/08/24 00:19 V43359MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 02/08/24 00:19 V43359MSA
2.89 µg/L 0.185 1.00n-Butylbenzene 1 02/08/24 00:19 V43359MSA
3.92 µg/L 0.200 0.500sec-Butyl benzene 1 02/08/24 00:19 V43359MSA
0.978 J µg/L 0.920 2.00tert-Butyl benzene 1 02/08/24 00:19 V43359MSA
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 02/08/24 00:19 V43359MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 02/08/24 00:19 V43359MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 02/08/24 00:19 V43359MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 02/08/24 00:19 V43359MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 02/08/24 00:19 V43359MSA
<0.220 µg/L 0.220 0.500Chloroform 1 02/08/24 00:19 V43359MSA
0.377 J µg/L 0.220 0.500Chloromethane 1 02/08/24 00:19 V43359MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 02/08/24 00:19 V43359MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 02/08/24 00:19 V43359MSA
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 02/08/24 00:19 V43359MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 10 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1
95680 Matrix:
1/27/2024 9:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V43357 02/07/24 14:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 02/08/24 00:19 V43359MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 02/08/24 00:19 V43359MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 02/08/24 00:19 V43359MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 02/08/24 00:19 V43359MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 02/08/24 00:19 V43359MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 02/08/24 00:19 V43359MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 02/08/24 00:19 V43359MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 02/08/24 00:19 V43359MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 02/08/24 00:19 V43359MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 02/08/24 00:19 V43359MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 02/08/24 00:19 V43359MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 02/08/24 00:19 V43359MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 02/08/24 00:19 V43359MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 02/08/24 00:19 V43359MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 02/08/24 00:19 V43359MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 02/08/24 00:19 V43359MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 02/08/24 00:19 V43359MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 02/08/24 00:19 V43359MSA
1.63 µg/L 0.170 0.500Ethylbenzene 1 02/08/24 00:19 V43359MSA
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 02/08/24 00:19 V43359MSA
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 02/08/24 00:19 V43359MSA
<1.30 µg/L 1.30 10.0n-Hexane 1 02/08/24 00:19 V43359MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 11 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1
95680 Matrix:
1/27/2024 9:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V43357 02/07/24 14:00
<0.380 µg/L 0.380 5.002-Hexanone 1 02/08/24 00:19 V43359MSA
3.48 J µg/L 0.180 5.00Isopropylbenzene 1 02/08/24 00:19 V43359MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 02/08/24 00:19 V43359MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 02/08/24 00:19 V43359MSA
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 02/08/24 00:19 V43359MSA
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 02/08/24 00:19 V43359MSA
<0.330 µg/L 0.330 1.00Methylene Chloride 1 02/08/24 00:19 V43359MSA
25.4 µg/L 0.470 1.00Naphthalene 1 02/08/24 00:19 V43359MSA
4.27 µg/L 0.190 0.500n-Propylbenzene 1 02/08/24 00:19 V43359MSA
<0.220 µg/L 0.220 0.500Styrene 1 02/08/24 00:19 V43359MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 02/08/24 00:19 V43359MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 02/08/24 00:19 V43359MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 02/08/24 00:19 V43359MSA
0.479 J µg/L 0.220 0.500Toluene 1 02/08/24 00:19 V43359MSA
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 02/08/24 00:19 V43359MSA
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 02/08/24 00:19 V43359MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 02/08/24 00:19 V43359MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 02/08/24 00:19 V43359MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 02/08/24 00:19 V43359MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 02/08/24 00:19 V43359MSA
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 02/08/24 00:19 V43359MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 02/08/24 00:19 V43359MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 12 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1
95680 Matrix:
1/27/2024 9:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V43357 02/07/24 14:00
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 02/08/24 00:19 V43359MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 02/08/24 00:19 V43359MSA
0.595 µg/L 0.210 0.500o-Xylene 1 02/08/24 00:19 V43359MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 02/08/24 00:19 V43359MSA
0.595 µg/L 0.210 0.500Xylene (Total)1 02/08/24 00:19 V43359
Surrogate: 4-Bromofluorobenzene 101 Limits: 80-124%02/08/24 00:191 MSA V43359
Surrogate: Dibromofluoromethane 98.0 Limits: 75-129%02/08/24 00:191 MSA V43359
Surrogate: 1,2-Dichloroethane - d4 98.6 Limits: 63-136%02/08/24 00:191 MSA V43359
Surrogate: Toluene-d8 100 Limits: 77-123%02/08/24 00:191 MSA V43359
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V43104 02/02/24 10:27
8.11 µg/L 0.302 2.00Acenaphthene 1 02/06/24 23:45 V43253TJW
<0.297 µg/L 0.297 2.00Acenaphthylene 1 02/06/24 23:45 V43253TJW
<2.05 µg/L 2.05 5.00Aniline 1 02/06/24 23:45 V43253TJW
<0.836 µg/L 0.836 2.00Anthracene 1 02/06/24 23:45 V43253TJW
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 02/06/24 23:45 V43253TJW
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 02/06/24 23:45 V43253TJW
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 02/06/24 23:45 V43253TJW
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 02/06/24 23:45 V43253TJW
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 02/06/24 23:45 V43253TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 13 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1
95680 Matrix:
1/27/2024 9:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V43104 02/02/24 10:27
<1.10 µg/L 1.10 10.0Benzoic Acid 1 02/06/24 23:45 V43253TJW
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 02/06/24 23:45 V43253TJW
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 02/06/24 23:45 V43253TJW
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 02/06/24 23:45 V43253TJW
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 02/06/24 23:45 V43253TJW
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 02/06/24 23:45 V43253TJW
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 02/06/24 23:45 V43253TJW
<1.83 µg/L 1.83 5.00Butyl benzyl phthalate 1 02/06/24 23:45 V43253TJW
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 02/06/24 23:45 V43253TJW
<1.33 µg/L 1.33 5.004-Chloroaniline 1 02/06/24 23:45 V43253TJW
<1.83 µg/L 1.83 20.02-Chloronaphthalene 1 02/06/24 23:45 V43253TJW
<0.938 µg/L 0.938 10.02-Chlorophenol 1 02/06/24 23:45 V43253TJW
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 02/06/24 23:45 V43253TJW
<0.405 µg/L 0.405 2.00Chrysene 1 02/06/24 23:45 V43253TJW
<0.434 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 02/06/24 23:45 V43253TJW
<0.856 µg/L 0.856 5.00Dibenzofuran 1 02/06/24 23:45 V43253TJW
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 02/06/24 23:45 V43253TJW
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 02/06/24 23:45 V43253TJW
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 02/06/24 23:45 V43253TJW
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 02/06/24 23:45 V43253TJW
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 02/06/24 23:45 V43253TJW
<0.745 µg/L 0.745 5.00Diethyl phthalate 1 02/06/24 23:45 V43253TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 14 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1
95680 Matrix:
1/27/2024 9:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V43104 02/02/24 10:27
<0.939 µg/L 0.939 5.00Dimethyl phthalate 1 02/06/24 23:45 V43253TJW
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 02/06/24 23:45 V43253TJW
<2.06 µg/L 2.06 5.00Di-n-butyl phthalate 1 02/06/24 23:45 V43253TJW
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 02/06/24 23:45 V43253TJW
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 02/06/24 23:45 V43253TJW
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 02/06/24 23:45 V43253TJW
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 02/06/24 23:45 V43253TJW
<1.65 µg/L 1.65 5.00Di-n-Octyl Phthalate 1 02/06/24 23:45 V43253TJW
<0.250 µg/L 0.250 2.00Fluoranthene 1 02/06/24 23:45 V43253TJW
6.69 µg/L 0.807 2.00Fluorene 1 02/06/24 23:45 V43253TJW
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 02/06/24 23:45 V43253TJW
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 02/06/24 23:45 V43253TJW
<2.05 µg/L 2.05 5.00Hexachlorocyclopentadiene 1 02/06/24 23:45 V43253TJW
<1.76 µg/L 1.76 5.00Hexachloroethane 1 02/06/24 23:45 V43253TJW
<0.477 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 02/06/24 23:45 V43253TJW
<0.444 µg/L 0.444 5.00Isophorone 1 02/06/24 23:45 V43253TJW
49.0 M µg/L 1.14 2.001-Methylnaphthalene 1 02/06/24 23:45 V43253TJW
25.2 M µg/L 0.666 2.002-Methylnaphthalene 1 02/06/24 23:45 V43253TJW
<1.15 µg/L 1.15 5.002-Methylphenol 1 02/06/24 23:45 V43253TJW
<0.880 µg/L 0.880 10.03&4 Methylphenol 1 02/06/24 23:45 V43253TJW
11.8 µg/L 0.728 2.00Naphthalene 1 02/06/24 23:45 V43253TJW
<1.39 µg/L 1.39 5.002-Nitroaniline 1 02/06/24 23:45 V43253TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 15 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1
95680 Matrix:
1/27/2024 9:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V43104 02/02/24 10:27
<1.39 µg/L 1.39 5.003-Nitroaniline 1 02/06/24 23:45 V43253TJW
<1.53 µg/L 1.53 5.004-Nitroaniline 1 02/06/24 23:45 V43253TJW
<0.905 µg/L 0.905 5.00Nitrobenzene 1 02/06/24 23:45 V43253TJW
<0.493 µg/L 0.493 5.002-Nitrophenol 1 02/06/24 23:45 V43253TJW
<1.23 µg/L 1.23 10.04-Nitrophenol 1 02/06/24 23:45 V43253TJW
<0.450 µg/L 0.450 5.00N-Nitrosodimethylamine 1 02/06/24 23:45 V43253TJW
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 02/06/24 23:45 V43253TJW
<0.641 µg/L 0.641 5.00N-Nitroso-di-n-propylamine 1 02/06/24 23:45 V43253TJW
<1.43 µg/L 1.43 5.00Pentachlorophenol 1 02/06/24 23:45 V43253TJW
18.3 µg/L 0.428 2.00Phenanthrene 1 02/06/24 23:45 V43253TJW
<0.651 µg/L 0.651 5.00Phenol 1 02/06/24 23:45 V43253TJW
<0.434 µg/L 0.434 2.00Pyrene 1 02/06/24 23:45 V43253TJW
<1.20 µg/L 1.20 5.00Pyridine 1 02/06/24 23:45 V43253TJW
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 02/06/24 23:45 V43253TJW
<1.31 µg/L 1.31 5.002,4,5-Trichlorophenol 1 02/06/24 23:45 V43253TJW
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 02/06/24 23:45 V43253TJW
8270ESurrogate: Phenol-d5 35.9 Limits: 11-100%02/06/24 23:451 TJW
Surrogate: 2-Fluorobiphenyl 70.2 Limits: 44-119%02/06/24 23:451 TJW V43253
Surrogate: 2-Fluorophenol 48.1 Limits: 19-119%02/06/24 23:451 TJW V43253
Surrogate: Nitrobenzene-d5 61.6 Limits: 44-120%02/06/24 23:451 TJW V43253
Surrogate: 4-Terphenyl-d14 81.4 Limits: 50-134%02/06/24 23:451 TJW V43253
Surrogate: 2,4,6-Tribromophenol 98.2 Limits: 43-140%02/06/24 23:451 TJW V43253
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 16 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1
95680 Matrix:
1/27/2024 9:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V43206 02/06/24 10:48
1410 µg/L 28.2 350Aliphatic C9-C18 1 02/08/24 16:24 V43310NDL
1090 µg/L 248 1000Aliphatic C19-C36 2 02/08/24 16:24 V43310NDL
1250 µg/L 61.2 250Aromatic C11-C22 1 02/08/24 16:24 V43310NDL
MADEP-EPHSurrogate: 2-Bromonaphthalene 45.8 Limits: 40-140%02/08/24 16:241 NDL
MADEP-EPHSurrogate: OTP Surrogate 31.4 *Limits: 40-140%02/08/24 16:241 NDL
Surrogate: 2-Fluorobiphenyl 43.5 Limits: 40-140%02/08/24 16:241 NDL V43310
MADEP-EPHSurrogate: Chlorooctadecane 85.9 Limits: 40-140%02/08/24 16:242 NDL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V43050 01/31/24 08:00
<11.5 µg/L 11.5 50.0Aliphatic C5-C8 1 02/01/24 17:01 V43051TBL
278 µg/L 25.8 50.0Aliphatic C9-C12 1 02/01/24 17:01 V43051TBL
229 µg/L 4.02 50.0Aromatic C9-C10 1 02/01/24 17:01 V43051TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)88.0 Limits: 70-130%02/01/24 17:011 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)104 Limits: 70-130%02/01/24 17:011 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 17 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (4)
95681 Matrix:
1/26/2024 9:35
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.8 %Moisture 1 02/02/24 11:55 SW-DRYWTPEB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 18 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (4)
95681 Matrix:
1/26/2024 9:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
0.079 mg/Kg - dry 0.002 0.024Acetone 1 01/31/24 22:30 V43078TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 01/31/24 22:30 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 01/31/24 22:30 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 01/31/24 22:30 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 01/31/24 22:30 V43078TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 01/31/24 22:30 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 01/31/24 22:30 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 01/31/24 22:30 V43078TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 01/31/24 22:30 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 01/31/24 22:30 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 01/31/24 22:30 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 01/31/24 22:30 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 01/31/24 22:30 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 01/31/24 22:30 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 01/31/24 22:30 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 01/31/24 22:30 V43078TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 01/31/24 22:30 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 01/31/24 22:30 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 01/31/24 22:30 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 01/31/24 22:30 V43078TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 01/31/24 22:30 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 01/31/24 22:30 V43078TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 19 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (4)
95681 Matrix:
1/26/2024 9:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 01/31/24 22:30 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 01/31/24 22:30 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 01/31/24 22:30 V43078TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 01/31/24 22:30 V43078TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 01/31/24 22:30 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 01/31/24 22:30 V43078TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 01/31/24 22:30 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 01/31/24 22:30 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 01/31/24 22:30 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 01/31/24 22:30 V43078TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 01/31/24 22:30 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 01/31/24 22:30 V43078TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 01/31/24 22:30 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 01/31/24 22:30 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 01/31/24 22:30 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 01/31/24 22:30 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 01/31/24 22:30 V43078TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 01/31/24 22:30 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 01/31/24 22:30 V43078TBL
<0.001 mg/Kg - dry 0.001 0.061Ethyl Tertiary Butyl Ether (ETBE)1 01/31/24 22:30 V43078TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 01/31/24 22:30 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 01/31/24 22:30 V43078TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 20 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (4)
95681 Matrix:
1/26/2024 9:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 01/31/24 22:30 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 01/31/24 22:30 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 01/31/24 22:30 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 01/31/24 22:30 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 01/31/24 22:30 V43078TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 01/31/24 22:30 V43078TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 01/31/24 22:30 V43078TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 01/31/24 22:30 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 01/31/24 22:30 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 01/31/24 22:30 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 01/31/24 22:30 V43078TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 01/31/24 22:30 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 01/31/24 22:30 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 01/31/24 22:30 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 01/31/24 22:30 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 01/31/24 22:30 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 01/31/24 22:30 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 01/31/24 22:30 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 01/31/24 22:30 V43078TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 01/31/24 22:30 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 01/31/24 22:30 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 01/31/24 22:30 V43078TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 21 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (4)
95681 Matrix:
1/26/2024 9:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 01/31/24 22:30 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 01/31/24 22:30 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 01/31/24 22:30 V43078TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 01/31/24 22:30 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 01/31/24 22:30 V43078
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%01/31/24 22:301 TBL V43078
Surrogate: Dibromofluoromethane 109 Limits: 84-123%01/31/24 22:301 TBL V43078
Surrogate: Toluene-d8 118 Limits: 76-129%01/31/24 22:301 TBL V43078
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.142 mg/Kg - dry 0.142 0.812Acenaphthene 1 02/06/24 21:18 V43256TJW
<0.129 mg/Kg - dry 0.129 0.812Acenaphthylene 1 02/06/24 21:18 V43256TJW
<0.187 mg/Kg - dry 0.187 0.812Aniline 1 02/06/24 21:18 V43256TJW
<0.176 mg/Kg - dry 0.176 0.812Anthracene 1 02/06/24 21:18 V43256TJW
<0.171 mg/Kg - dry 0.171 0.812Benzo(a)anthracene 1 02/06/24 21:18 V43256TJW
<0.181 mg/Kg - dry 0.181 0.812Benzo(a)pyrene 1 02/06/24 21:18 V43256TJW
<0.179 mg/Kg - dry 0.179 0.812Benzo(b)fluoranthene 1 02/06/24 21:18 V43256TJW
<0.167 mg/Kg - dry 0.167 0.812Benzo(g,h,i)perylene 1 02/06/24 21:18 V43256TJW
<0.168 mg/Kg - dry 0.168 0.812Benzo(k)fluoranthene 1 02/06/24 21:18 V43256TJW
<0.714 mg/Kg - dry 0.714 2.46Benzoic Acid 1 02/06/24 21:18 V43256TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 22 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (4)
95681 Matrix:
1/26/2024 9:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.129 mg/Kg - dry 0.129 0.812Benzyl alcohol 1 02/06/24 21:18 V43256TJW
<0.145 mg/Kg - dry 0.145 0.812Bis(2-Chloroethoxy)methane 1 02/06/24 21:18 V43256TJW
<0.131 mg/Kg - dry 0.131 0.812Bis(2-Chloroethyl)ether 1 02/06/24 21:18 V43256TJW
<0.167 mg/Kg - dry 0.167 0.406Bis(2-Chloroisopropyl)ether 1 02/06/24 21:18 V43256TJW
<0.147 mg/Kg - dry 0.147 0.812Bis(2-ethylhexyl)phthalate 1 02/06/24 21:18 V43256TJW
<0.134 mg/Kg - dry 0.134 0.8124-Bromophenyl phenyl ether 1 02/06/24 21:18 V43256TJW
<0.139 mg/Kg - dry 0.139 0.406Butyl benzyl phthalate 1 02/06/24 21:18 V43256TJW
<0.113 mg/Kg - dry 0.113 0.8124-Chloro-3-methylphenol 1 02/06/24 21:18 V43256TJW
<0.137 mg/Kg - dry 0.137 0.4064-Chloroaniline 1 02/06/24 21:18 V43256TJW
<0.142 mg/Kg - dry 0.142 0.8122-Chloronaphthalene 1 02/06/24 21:18 V43256TJW
<0.120 mg/Kg - dry 0.120 0.8122-Chlorophenol 1 02/06/24 21:18 V43256TJW
<0.155 mg/Kg - dry 0.155 1.234-Chlorophenyl phenyl ether 1 02/06/24 21:18 V43256TJW
<0.174 mg/Kg - dry 0.174 0.812Chrysene 1 02/06/24 21:18 V43256TJW
<0.283 mg/Kg - dry 0.283 0.812Dibenz(a,h)anthracene 1 02/06/24 21:18 V43256TJW
<0.146 mg/Kg - dry 0.146 0.812Dibenzofuran 1 02/06/24 21:18 V43256TJW
<0.116 mg/Kg - dry 0.116 0.8121,2-Dichlorobenzene 1 02/06/24 21:18 V43256TJW
<0.119 mg/Kg - dry 0.119 0.8121,3-Dichlorobenzene 1 02/06/24 21:18 V43256TJW
<0.120 mg/Kg - dry 0.120 0.4061,4-Dichlorobenzene 1 02/06/24 21:18 V43256TJW
<0.181 mg/Kg - dry 0.181 0.8123,3'-Dichlorobenzidine 1 02/06/24 21:18 V43256TJW
<0.117 mg/Kg - dry 0.117 0.8122,4-Dichlorophenol 1 02/06/24 21:18 V43256TJW
<0.221 mg/Kg - dry 0.221 0.812Diethyl phthalate 1 02/06/24 21:18 V43256TJW
<0.214 mg/Kg - dry 0.214 0.812Dimethyl phthalate 1 02/06/24 21:18 V43256TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 23 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (4)
95681 Matrix:
1/26/2024 9:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.133 mg/Kg - dry 0.133 0.4062,4-Dimethylphenol 1 02/06/24 21:18 V43256TJW
<0.131 mg/Kg - dry 0.131 0.812Di-n-butyl phthalate 1 02/06/24 21:18 V43256TJW
<0.295 mg/Kg - dry 0.295 1.854,6-Dinitro-2-methylphenol 1 02/06/24 21:18 V43256TJW
<0.640 mg/Kg - dry 0.640 1.852,4-Dinitrophenol 1 02/06/24 21:18 V43256TJW
<0.118 mg/Kg - dry 0.118 0.8122,4-Dinitrotoluene 1 02/06/24 21:18 V43256TJW
<0.133 mg/Kg - dry 0.133 0.8122,6-Dinitrotoluene 1 02/06/24 21:18 V43256TJW
<0.176 mg/Kg - dry 0.176 0.406Di-n-Octyl Phthalate 1 02/06/24 21:18 V43256TJW
<0.151 mg/Kg - dry 0.151 0.812Fluoranthene 1 02/06/24 21:18 V43256TJW
<0.157 mg/Kg - dry 0.157 0.812Fluorene 1 02/06/24 21:18 V43256TJW
<0.130 mg/Kg - dry 0.130 0.812Hexachlorobenzene 1 02/06/24 21:18 V43256TJW
<0.120 mg/Kg - dry 0.120 0.812Hexachlorobutadiene 1 02/06/24 21:18 V43256TJW
<0.193 mg/Kg - dry 0.193 0.812Hexachlorocyclopentadiene 1 02/06/24 21:18 V43256TJW
<0.097 mg/Kg - dry 0.097 0.812Hexachloroethane 1 02/06/24 21:18 V43256TJW
<0.220 mg/Kg - dry 0.220 0.812Indeno(1,2,3-cd)pyrene 1 02/06/24 21:18 V43256TJW
<0.235 mg/Kg - dry 0.235 0.812Isophorone 1 02/06/24 21:18 V43256TJW
<0.130 mg/Kg - dry 0.130 0.8121-Methylnaphthalene 1 02/06/24 21:18 V43256TJW
<0.123 mg/Kg - dry 0.123 0.8122-Methylnaphthalene 1 02/06/24 21:18 V43256TJW
<0.119 mg/Kg - dry 0.119 0.8122-Methylphenol 1 02/06/24 21:18 V43256TJW
<0.104 mg/Kg - dry 0.104 0.8123&4 Methylphenol 1 02/06/24 21:18 V43256TJW
<0.177 mg/Kg - dry 0.177 0.812Naphthalene 1 02/06/24 21:18 V43256TJW
<0.119 mg/Kg - dry 0.119 0.8122-Nitroaniline 1 02/06/24 21:18 V43256TJW
<0.147 mg/Kg - dry 0.147 0.8123-Nitroaniline 1 02/06/24 21:18 V43256TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 24 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (4)
95681 Matrix:
1/26/2024 9:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.114 mg/Kg - dry 0.114 0.4064-Nitroaniline 1 02/06/24 21:18 V43256TJW
<0.142 mg/Kg - dry 0.142 0.406Nitrobenzene 1 02/06/24 21:18 V43256TJW
<0.109 mg/Kg - dry 0.109 0.8122-Nitrophenol 1 02/06/24 21:18 V43256TJW
<0.144 mg/Kg - dry 0.144 0.8124-Nitrophenol 1 02/06/24 21:18 V43256TJW
<0.323 mg/Kg - dry 0.323 0.812N-Nitrosodimethylamine 1 02/06/24 21:18 V43256TJW
<0.222 mg/Kg - dry 0.222 0.812N-Nitrosodiphenylamine 1 02/06/24 21:18 V43256TJW
<0.145 mg/Kg - dry 0.145 0.812N-Nitroso-di-n-propylamine 1 02/06/24 21:18 V43256TJW
<0.427 mg/Kg - dry 0.427 1.23Pentachlorophenol 1 02/06/24 21:18 V43256TJW
<0.256 mg/Kg - dry 0.256 0.812Phenanthrene 1 02/06/24 21:18 V43256TJW
<0.137 mg/Kg - dry 0.137 0.812Phenol 1 02/06/24 21:18 V43256TJW
<0.165 mg/Kg - dry 0.165 0.812Pyrene 1 02/06/24 21:18 V43256TJW
<0.097 mg/Kg - dry 0.097 0.406Pyridine 1 02/06/24 21:18 V43256TJW
<0.131 mg/Kg - dry 0.131 0.8121,2,4-Trichlorobenzene 1 02/06/24 21:18 V43256TJW
<0.118 mg/Kg - dry 0.118 0.8122,4,5-Trichlorophenol 1 02/06/24 21:18 V43256TJW
<0.118 mg/Kg - dry 0.118 0.8122,4,6-Trichlorophenol 1 02/06/24 21:18 V43256TJW
8270ESurrogate: Phenol-d5 88.3 Limits: 34-121%02/06/24 21:181 TJW
Surrogate: 2-Fluorobiphenyl 88.0 Limits: 44-115%02/06/24 21:181 TJW V43256
Surrogate: 2-Fluorophenol 92.8 Limits: 35-115%02/06/24 21:181 TJW V43256
Surrogate: Nitrobenzene-d5 80.8 Limits: 37-122%02/06/24 21:181 TJW V43256
Surrogate: 4-Terphenyl-d14 84.4 Limits: 54-127%02/06/24 21:181 TJW V43256
Surrogate: 2,4,6-Tribromophenol 87.4 Limits: 39-132%02/06/24 21:181 TJW V43256
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 25 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (4)
95681 Matrix:
1/26/2024 9:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V43116 02/02/24 09:50
44.1 J mg/Kg - dry 11.3 61.3Aliphatic C9-C18 1 02/07/24 19:42 V43311NDL
55.5 J mg/Kg - dry 15.0 61.3Aliphatic C19-C36 1 02/07/24 19:42 V43311NDL
28.9 J mg/Kg - dry 17.4 61.3Aromatic C11-C22 1 02/07/24 19:42 V43311NDL
MADEP-EPHSurrogate: 2-Bromonaphthalene 101 Limits: 40-140%02/07/24 19:421 NDL
MADEP-EPHSurrogate: Chlorooctadecane 76.9 Limits: 40-140%02/07/24 19:421 NDL
MADEP-EPHSurrogate: OTP Surrogate 104 Limits: 40-140%02/07/24 19:421 NDL
Surrogate: 2-Fluorobiphenyl 102 Limits: 40-140%02/07/24 19:421 NDL V43311
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V43048 01/31/24 08:00
<1.50 mg/Kg - dry 1.50 9.85Aliphatic C5-C8 100 01/31/24 22:52 V43049TBL
<5.62 mg/Kg - dry 5.62 9.85Aliphatic C9-C12 100 01/31/24 22:52 V43049TBL
<0.768 mg/Kg - dry 0.768 9.85Aromatic C9-C10 100 01/31/24 22:52 V43049TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)111 Limits: 70-130%01/31/24 22:52100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)112 Limits: 70-130%01/31/24 22:52100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 26 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (8)
95682 Matrix:
1/26/2024 9:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.1 %Moisture 1 02/02/24 11:55 SW-DRYWTPEB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 27 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (8)
95682 Matrix:
1/26/2024 9:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
0.047 mg/Kg - dry 0.003 0.025Acetone 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 01/31/24 22:57 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.025Acrylonitrile 1 01/31/24 22:57 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 01/31/24 22:57 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 01/31/24 22:57 V43078TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 01/31/24 22:57 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 01/31/24 22:57 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 01/31/24 22:57 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 01/31/24 22:57 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 01/31/24 22:57 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 01/31/24 22:57 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 01/31/24 22:57 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 01/31/24 22:57 V43078TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 01/31/24 22:57 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 01/31/24 22:57 V43078TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 28 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (8)
95682 Matrix:
1/26/2024 9:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 01/31/24 22:57 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 01/31/24 22:57 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 01/31/24 22:57 V43078TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 01/31/24 22:57 V43078TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 01/31/24 22:57 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 01/31/24 22:57 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 01/31/24 22:57 V43078TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 01/31/24 22:57 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 01/31/24 22:57 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 01/31/24 22:57 V43078TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 01/31/24 22:57 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 01/31/24 22:57 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 01/31/24 22:57 V43078TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 01/31/24 22:57 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 01/31/24 22:57 V43078TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 29 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (8)
95682 Matrix:
1/26/2024 9:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 01/31/24 22:57 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 01/31/24 22:57 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 01/31/24 22:57 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 01/31/24 22:57 V43078TBL
<0.018 mg/Kg - dry 0.018 0.0254-Methyl-2-Pentanone 1 01/31/24 22:57 V43078TBL
0.005 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 01/31/24 22:57 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 01/31/24 22:57 V43078TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 01/31/24 22:57 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 01/31/24 22:57 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 01/31/24 22:57 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 01/31/24 22:57 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 01/31/24 22:57 V43078TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 01/31/24 22:57 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 01/31/24 22:57 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 01/31/24 22:57 V43078TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 30 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (8)
95682 Matrix:
1/26/2024 9:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 01/31/24 22:57 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 01/31/24 22:57 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 01/31/24 22:57 V43078TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 01/31/24 22:57 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 01/31/24 22:57 V43078
Surrogate: 4-Bromofluorobenzene 94.0 Limits: 70-130%01/31/24 22:571 TBL V43078
Surrogate: Dibromofluoromethane 92.4 Limits: 84-123%01/31/24 22:571 TBL V43078
Surrogate: Toluene-d8 110 Limits: 76-129%01/31/24 22:571 TBL V43078
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.145 mg/Kg - dry 0.145 0.827Acenaphthene 1 02/06/24 22:49 V43256TJW
<0.131 mg/Kg - dry 0.131 0.827Acenaphthylene 1 02/06/24 22:49 V43256TJW
<0.190 mg/Kg - dry 0.190 0.827Aniline 1 02/06/24 22:49 V43256TJW
<0.178 mg/Kg - dry 0.178 0.827Anthracene 1 02/06/24 22:49 V43256TJW
<0.173 mg/Kg - dry 0.173 0.827Benzo(a)anthracene 1 02/06/24 22:49 V43256TJW
<0.183 mg/Kg - dry 0.183 0.827Benzo(a)pyrene 1 02/06/24 22:49 V43256TJW
<0.182 mg/Kg - dry 0.182 0.827Benzo(b)fluoranthene 1 02/06/24 22:49 V43256TJW
<0.170 mg/Kg - dry 0.170 0.827Benzo(g,h,i)perylene 1 02/06/24 22:49 V43256TJW
<0.171 mg/Kg - dry 0.171 0.827Benzo(k)fluoranthene 1 02/06/24 22:49 V43256TJW
<0.725 mg/Kg - dry 0.725 2.50Benzoic Acid 1 02/06/24 22:49 V43256TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 31 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (8)
95682 Matrix:
1/26/2024 9:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.131 mg/Kg - dry 0.131 0.827Benzyl alcohol 1 02/06/24 22:49 V43256TJW
<0.147 mg/Kg - dry 0.147 0.827Bis(2-Chloroethoxy)methane 1 02/06/24 22:49 V43256TJW
<0.133 mg/Kg - dry 0.133 0.827Bis(2-Chloroethyl)ether 1 02/06/24 22:49 V43256TJW
<0.170 mg/Kg - dry 0.170 0.413Bis(2-Chloroisopropyl)ether 1 02/06/24 22:49 V43256TJW
<0.150 mg/Kg - dry 0.150 0.827Bis(2-ethylhexyl)phthalate 1 02/06/24 22:49 V43256TJW
<0.136 mg/Kg - dry 0.136 0.8274-Bromophenyl phenyl ether 1 02/06/24 22:49 V43256TJW
<0.141 mg/Kg - dry 0.141 0.413Butyl benzyl phthalate 1 02/06/24 22:49 V43256TJW
<0.115 mg/Kg - dry 0.115 0.8274-Chloro-3-methylphenol 1 02/06/24 22:49 V43256TJW
<0.140 mg/Kg - dry 0.140 0.4134-Chloroaniline 1 02/06/24 22:49 V43256TJW
<0.145 mg/Kg - dry 0.145 0.8272-Chloronaphthalene 1 02/06/24 22:49 V43256TJW
<0.123 mg/Kg - dry 0.123 0.8272-Chlorophenol 1 02/06/24 22:49 V43256TJW
<0.157 mg/Kg - dry 0.157 1.254-Chlorophenyl phenyl ether 1 02/06/24 22:49 V43256TJW
<0.177 mg/Kg - dry 0.177 0.827Chrysene 1 02/06/24 22:49 V43256TJW
<0.287 mg/Kg - dry 0.287 0.827Dibenz(a,h)anthracene 1 02/06/24 22:49 V43256TJW
<0.148 mg/Kg - dry 0.148 0.827Dibenzofuran 1 02/06/24 22:49 V43256TJW
<0.118 mg/Kg - dry 0.118 0.8271,2-Dichlorobenzene 1 02/06/24 22:49 V43256TJW
<0.121 mg/Kg - dry 0.121 0.8271,3-Dichlorobenzene 1 02/06/24 22:49 V43256TJW
<0.122 mg/Kg - dry 0.122 0.4131,4-Dichlorobenzene 1 02/06/24 22:49 V43256TJW
<0.183 mg/Kg - dry 0.183 0.8273,3'-Dichlorobenzidine 1 02/06/24 22:49 V43256TJW
<0.120 mg/Kg - dry 0.120 0.8272,4-Dichlorophenol 1 02/06/24 22:49 V43256TJW
<0.225 mg/Kg - dry 0.225 0.827Diethyl phthalate 1 02/06/24 22:49 V43256TJW
<0.217 mg/Kg - dry 0.217 0.827Dimethyl phthalate 1 02/06/24 22:49 V43256TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 32 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (8)
95682 Matrix:
1/26/2024 9:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.135 mg/Kg - dry 0.135 0.4132,4-Dimethylphenol 1 02/06/24 22:49 V43256TJW
<0.133 mg/Kg - dry 0.133 0.827Di-n-butyl phthalate 1 02/06/24 22:49 V43256TJW
<0.300 mg/Kg - dry 0.300 1.884,6-Dinitro-2-methylphenol 1 02/06/24 22:49 V43256TJW
<0.650 mg/Kg - dry 0.650 1.882,4-Dinitrophenol 1 02/06/24 22:49 V43256TJW
<0.121 mg/Kg - dry 0.121 0.8272,4-Dinitrotoluene 1 02/06/24 22:49 V43256TJW
<0.135 mg/Kg - dry 0.135 0.8272,6-Dinitrotoluene 1 02/06/24 22:49 V43256TJW
<0.178 mg/Kg - dry 0.178 0.413Di-n-Octyl Phthalate 1 02/06/24 22:49 V43256TJW
<0.153 mg/Kg - dry 0.153 0.827Fluoranthene 1 02/06/24 22:49 V43256TJW
<0.160 mg/Kg - dry 0.160 0.827Fluorene 1 02/06/24 22:49 V43256TJW
<0.132 mg/Kg - dry 0.132 0.827Hexachlorobenzene 1 02/06/24 22:49 V43256TJW
<0.122 mg/Kg - dry 0.122 0.827Hexachlorobutadiene 1 02/06/24 22:49 V43256TJW
<0.196 mg/Kg - dry 0.196 0.827Hexachlorocyclopentadiene 1 02/06/24 22:49 V43256TJW
<0.099 mg/Kg - dry 0.099 0.827Hexachloroethane 1 02/06/24 22:49 V43256TJW
<0.224 mg/Kg - dry 0.224 0.827Indeno(1,2,3-cd)pyrene 1 02/06/24 22:49 V43256TJW
<0.239 mg/Kg - dry 0.239 0.827Isophorone 1 02/06/24 22:49 V43256TJW
<0.132 mg/Kg - dry 0.132 0.8271-Methylnaphthalene 1 02/06/24 22:49 V43256TJW
<0.125 mg/Kg - dry 0.125 0.8272-Methylnaphthalene 1 02/06/24 22:49 V43256TJW
<0.121 mg/Kg - dry 0.121 0.8272-Methylphenol 1 02/06/24 22:49 V43256TJW
<0.106 mg/Kg - dry 0.106 0.8273&4 Methylphenol 1 02/06/24 22:49 V43256TJW
<0.180 mg/Kg - dry 0.180 0.827Naphthalene 1 02/06/24 22:49 V43256TJW
<0.121 mg/Kg - dry 0.121 0.8272-Nitroaniline 1 02/06/24 22:49 V43256TJW
<0.150 mg/Kg - dry 0.150 0.8273-Nitroaniline 1 02/06/24 22:49 V43256TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 33 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (8)
95682 Matrix:
1/26/2024 9:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.116 mg/Kg - dry 0.116 0.4134-Nitroaniline 1 02/06/24 22:49 V43256TJW
<0.145 mg/Kg - dry 0.145 0.413Nitrobenzene 1 02/06/24 22:49 V43256TJW
<0.111 mg/Kg - dry 0.111 0.8272-Nitrophenol 1 02/06/24 22:49 V43256TJW
<0.146 mg/Kg - dry 0.146 0.8274-Nitrophenol 1 02/06/24 22:49 V43256TJW
<0.329 mg/Kg - dry 0.329 0.827N-Nitrosodimethylamine 1 02/06/24 22:49 V43256TJW
<0.226 mg/Kg - dry 0.226 0.827N-Nitrosodiphenylamine 1 02/06/24 22:49 V43256TJW
<0.147 mg/Kg - dry 0.147 0.827N-Nitroso-di-n-propylamine 1 02/06/24 22:49 V43256TJW
<0.434 mg/Kg - dry 0.434 1.25Pentachlorophenol 1 02/06/24 22:49 V43256TJW
<0.260 mg/Kg - dry 0.260 0.827Phenanthrene 1 02/06/24 22:49 V43256TJW
<0.140 mg/Kg - dry 0.140 0.827Phenol 1 02/06/24 22:49 V43256TJW
<0.167 mg/Kg - dry 0.167 0.827Pyrene 1 02/06/24 22:49 V43256TJW
<0.099 mg/Kg - dry 0.099 0.413Pyridine 1 02/06/24 22:49 V43256TJW
<0.133 mg/Kg - dry 0.133 0.8271,2,4-Trichlorobenzene 1 02/06/24 22:49 V43256TJW
<0.120 mg/Kg - dry 0.120 0.8272,4,5-Trichlorophenol 1 02/06/24 22:49 V43256TJW
<0.121 mg/Kg - dry 0.121 0.8272,4,6-Trichlorophenol 1 02/06/24 22:49 V43256TJW
8270ESurrogate: Phenol-d5 82.9 Limits: 34-121%02/06/24 22:491 TJW
Surrogate: 2-Fluorobiphenyl 82.0 Limits: 44-115%02/06/24 22:491 TJW V43256
Surrogate: 2-Fluorophenol 87.4 Limits: 35-115%02/06/24 22:491 TJW V43256
Surrogate: Nitrobenzene-d5 79.6 Limits: 37-122%02/06/24 22:491 TJW V43256
Surrogate: 4-Terphenyl-d14 80.2 Limits: 54-127%02/06/24 22:491 TJW V43256
Surrogate: 2,4,6-Tribromophenol 86.5 Limits: 39-132%02/06/24 22:491 TJW V43256
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 34 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (8)
95682 Matrix:
1/26/2024 9:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V43116 02/02/24 09:50
39.8 J mg/Kg - dry 11.5 62.5Aliphatic C9-C18 1 02/07/24 20:19 V43311NDL
47.9 J mg/Kg - dry 15.3 62.5Aliphatic C19-C36 1 02/07/24 20:19 V43311NDL
<17.8 mg/Kg - dry 17.8 62.5Aromatic C11-C22 1 02/07/24 20:19 V43311NDL
MADEP-EPHSurrogate: 2-Bromonaphthalene 92.0 Limits: 40-140%02/07/24 20:191 NDL
MADEP-EPHSurrogate: Chlorooctadecane 70.2 Limits: 40-140%02/07/24 20:191 NDL
MADEP-EPHSurrogate: OTP Surrogate 91.7 Limits: 40-140%02/07/24 20:191 NDL
Surrogate: 2-Fluorobiphenyl 99.0 Limits: 40-140%02/07/24 20:191 NDL V43311
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V43048 01/31/24 08:00
<1.53 mg/Kg - dry 1.53 10.0Aliphatic C5-C8 100 01/31/24 23:16 V43049TBL
<5.71 mg/Kg - dry 5.71 10.0Aliphatic C9-C12 100 01/31/24 23:16 V43049TBL
<0.780 mg/Kg - dry 0.780 10.0Aromatic C9-C10 100 01/31/24 23:16 V43049TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)115 Limits: 70-130%01/31/24 23:16100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)114 Limits: 70-130%01/31/24 23:16100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 35 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (12)
95683 Matrix:
1/26/2024 9:43
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
21.6 %Moisture 1 02/02/24 11:55 SW-DRYWTPEB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 36 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (12)
95683 Matrix:
1/26/2024 9:43
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
0.093 mg/Kg - dry 0.003 0.025Acetone 1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 02/01/24 01:40 V43078TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 02/01/24 01:40 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 02/01/24 01:40 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 02/01/24 01:40 V43078TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 02/01/24 01:40 V43078TBL
0.024 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 02/01/24 01:40 V43078TBL
0.020 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 02/01/24 01:40 V43078TBL
0.002 J mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 02/01/24 01:40 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 02/01/24 01:40 V43078TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 02/01/24 01:40 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 02/01/24 01:40 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 02/01/24 01:40 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 02/01/24 01:40 V43078TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 02/01/24 01:40 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 02/01/24 01:40 V43078TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 37 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (12)
95683 Matrix:
1/26/2024 9:43
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 02/01/24 01:40 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 02/01/24 01:40 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 02/01/24 01:40 V43078TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 02/01/24 01:40 V43078TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 02/01/24 01:40 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 02/01/24 01:40 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 02/01/24 01:40 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 02/01/24 01:40 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 02/01/24 01:40 V43078TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 02/01/24 01:40 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 02/01/24 01:40 V43078TBL
0.003 J mg/Kg - dry 0.0007 0.006Ethylbenzene 1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.063Ethyl Tertiary Butyl Ether (ETBE)1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 02/01/24 01:40 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 02/01/24 01:40 V43078TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 38 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (12)
95683 Matrix:
1/26/2024 9:43
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 02/01/24 01:40 V43078TBL
0.004 J mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 02/01/24 01:40 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 02/01/24 01:40 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 02/01/24 01:40 V43078TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 02/01/24 01:40 V43078TBL
0.003 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 02/01/24 01:40 V43078TBL
0.012 mg/Kg - dry 0.001 0.012Naphthalene 1 02/01/24 01:40 V43078TBL
0.006 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 02/01/24 01:40 V43078TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 02/01/24 01:40 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 02/01/24 01:40 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 02/01/24 01:40 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 02/01/24 01:40 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 02/01/24 01:40 V43078TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 02/01/24 01:40 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 02/01/24 01:40 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 02/01/24 01:40 V43078TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 39 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (12)
95683 Matrix:
1/26/2024 9:43
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 02/01/24 01:40 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 02/01/24 01:40 V43078TBL
0.0009 J mg/Kg - dry 0.0006 0.006o-Xylene 1 02/01/24 01:40 V43078TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 02/01/24 01:40 V43078TBL
0.0009 J mg/Kg - dry 0.0006 0.006Xylene (Total)1 02/01/24 01:40 V43078
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%02/01/24 01:401 TBL V43078
Surrogate: Dibromofluoromethane 113 Limits: 84-123%02/01/24 01:401 TBL V43078
Surrogate: Toluene-d8 85.7 Limits: 76-129%02/01/24 01:401 TBL V43078
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
0.677 J mg/Kg - dry 0.147 0.841Acenaphthene 1 02/06/24 20:32 V43256TJW
<0.133 mg/Kg - dry 0.133 0.841Acenaphthylene 1 02/06/24 20:32 V43256TJW
<0.193 mg/Kg - dry 0.193 0.841Aniline 1 02/06/24 20:32 V43256TJW
<0.182 mg/Kg - dry 0.182 0.841Anthracene 1 02/06/24 20:32 V43256TJW
<0.177 mg/Kg - dry 0.177 0.841Benzo(a)anthracene 1 02/06/24 20:32 V43256TJW
<0.187 mg/Kg - dry 0.187 0.841Benzo(a)pyrene 1 02/06/24 20:32 V43256TJW
<0.186 mg/Kg - dry 0.186 0.841Benzo(b)fluoranthene 1 02/06/24 20:32 V43256TJW
<0.173 mg/Kg - dry 0.173 0.841Benzo(g,h,i)perylene 1 02/06/24 20:32 V43256TJW
<0.174 mg/Kg - dry 0.174 0.841Benzo(k)fluoranthene 1 02/06/24 20:32 V43256TJW
<0.739 mg/Kg - dry 0.739 2.55Benzoic Acid 1 02/06/24 20:32 V43256TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 40 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (12)
95683 Matrix:
1/26/2024 9:43
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.133 mg/Kg - dry 0.133 0.841Benzyl alcohol 1 02/06/24 20:32 V43256TJW
<0.150 mg/Kg - dry 0.150 0.841Bis(2-Chloroethoxy)methane 1 02/06/24 20:32 V43256TJW
<0.136 mg/Kg - dry 0.136 0.841Bis(2-Chloroethyl)ether 1 02/06/24 20:32 V43256TJW
<0.173 mg/Kg - dry 0.173 0.420Bis(2-Chloroisopropyl)ether 1 02/06/24 20:32 V43256TJW
<0.153 mg/Kg - dry 0.153 0.841Bis(2-ethylhexyl)phthalate 1 02/06/24 20:32 V43256TJW
<0.139 mg/Kg - dry 0.139 0.8414-Bromophenyl phenyl ether 1 02/06/24 20:32 V43256TJW
<0.144 mg/Kg - dry 0.144 0.420Butyl benzyl phthalate 1 02/06/24 20:32 V43256TJW
<0.117 mg/Kg - dry 0.117 0.8414-Chloro-3-methylphenol 1 02/06/24 20:32 V43256TJW
<0.142 mg/Kg - dry 0.142 0.4204-Chloroaniline 1 02/06/24 20:32 V43256TJW
<0.147 mg/Kg - dry 0.147 0.8412-Chloronaphthalene 1 02/06/24 20:32 V43256TJW
<0.125 mg/Kg - dry 0.125 0.8412-Chlorophenol 1 02/06/24 20:32 V43256TJW
<0.160 mg/Kg - dry 0.160 1.284-Chlorophenyl phenyl ether 1 02/06/24 20:32 V43256TJW
<0.181 mg/Kg - dry 0.181 0.841Chrysene 1 02/06/24 20:32 V43256TJW
<0.293 mg/Kg - dry 0.293 0.841Dibenz(a,h)anthracene 1 02/06/24 20:32 V43256TJW
0.623 J mg/Kg - dry 0.151 0.841Dibenzofuran 1 02/06/24 20:32 V43256TJW
<0.120 mg/Kg - dry 0.120 0.8411,2-Dichlorobenzene 1 02/06/24 20:32 V43256TJW
<0.124 mg/Kg - dry 0.124 0.8411,3-Dichlorobenzene 1 02/06/24 20:32 V43256TJW
<0.124 mg/Kg - dry 0.124 0.4201,4-Dichlorobenzene 1 02/06/24 20:32 V43256TJW
<0.187 mg/Kg - dry 0.187 0.8413,3'-Dichlorobenzidine 1 02/06/24 20:32 V43256TJW
<0.122 mg/Kg - dry 0.122 0.8412,4-Dichlorophenol 1 02/06/24 20:32 V43256TJW
<0.229 mg/Kg - dry 0.229 0.841Diethyl phthalate 1 02/06/24 20:32 V43256TJW
<0.221 mg/Kg - dry 0.221 0.841Dimethyl phthalate 1 02/06/24 20:32 V43256TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 41 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (12)
95683 Matrix:
1/26/2024 9:43
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.137 mg/Kg - dry 0.137 0.4202,4-Dimethylphenol 1 02/06/24 20:32 V43256TJW
<0.136 mg/Kg - dry 0.136 0.841Di-n-butyl phthalate 1 02/06/24 20:32 V43256TJW
<0.306 mg/Kg - dry 0.306 1.914,6-Dinitro-2-methylphenol 1 02/06/24 20:32 V43256TJW
<0.663 mg/Kg - dry 0.663 1.912,4-Dinitrophenol 1 02/06/24 20:32 V43256TJW
<0.123 mg/Kg - dry 0.123 0.8412,4-Dinitrotoluene 1 02/06/24 20:32 V43256TJW
<0.137 mg/Kg - dry 0.137 0.8412,6-Dinitrotoluene 1 02/06/24 20:32 V43256TJW
<0.182 mg/Kg - dry 0.182 0.420Di-n-Octyl Phthalate 1 02/06/24 20:32 V43256TJW
0.211 J mg/Kg - dry 0.156 0.841Fluoranthene 1 02/06/24 20:32 V43256TJW
1.22 mg/Kg - dry 0.163 0.841Fluorene 1 02/06/24 20:32 V43256TJW
<0.135 mg/Kg - dry 0.135 0.841Hexachlorobenzene 1 02/06/24 20:32 V43256TJW
<0.124 mg/Kg - dry 0.124 0.841Hexachlorobutadiene 1 02/06/24 20:32 V43256TJW
<0.200 mg/Kg - dry 0.200 0.841Hexachlorocyclopentadiene 1 02/06/24 20:32 V43256TJW
<0.101 mg/Kg - dry 0.101 0.841Hexachloroethane 1 02/06/24 20:32 V43256TJW
<0.228 mg/Kg - dry 0.228 0.841Indeno(1,2,3-cd)pyrene 1 02/06/24 20:32 V43256TJW
<0.243 mg/Kg - dry 0.243 0.841Isophorone 1 02/06/24 20:32 V43256TJW
2.84 mg/Kg - dry 0.135 0.8411-Methylnaphthalene 1 02/06/24 20:32 V43256TJW
<0.127 mg/Kg - dry 0.127 0.8412-Methylnaphthalene 1 02/06/24 20:32 V43256TJW
<0.123 mg/Kg - dry 0.123 0.8412-Methylphenol 1 02/06/24 20:32 V43256TJW
<0.108 mg/Kg - dry 0.108 0.8413&4 Methylphenol 1 02/06/24 20:32 V43256TJW
<0.183 mg/Kg - dry 0.183 0.841Naphthalene 1 02/06/24 20:32 V43256TJW
<0.123 mg/Kg - dry 0.123 0.8412-Nitroaniline 1 02/06/24 20:32 V43256TJW
<0.153 mg/Kg - dry 0.153 0.8413-Nitroaniline 1 02/06/24 20:32 V43256TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 42 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (12)
95683 Matrix:
1/26/2024 9:43
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.119 mg/Kg - dry 0.119 0.4204-Nitroaniline 1 02/06/24 20:32 V43256TJW
<0.147 mg/Kg - dry 0.147 0.420Nitrobenzene 1 02/06/24 20:32 V43256TJW
<0.113 mg/Kg - dry 0.113 0.8412-Nitrophenol 1 02/06/24 20:32 V43256TJW
<0.149 mg/Kg - dry 0.149 0.8414-Nitrophenol 1 02/06/24 20:32 V43256TJW
<0.335 mg/Kg - dry 0.335 0.841N-Nitrosodimethylamine 1 02/06/24 20:32 V43256TJW
<0.230 mg/Kg - dry 0.230 0.841N-Nitrosodiphenylamine 1 02/06/24 20:32 V43256TJW
<0.150 mg/Kg - dry 0.150 0.841N-Nitroso-di-n-propylamine 1 02/06/24 20:32 V43256TJW
<0.442 mg/Kg - dry 0.442 1.28Pentachlorophenol 1 02/06/24 20:32 V43256TJW
0.649 J mg/Kg - dry 0.265 0.841Phenanthrene 1 02/06/24 20:32 V43256TJW
<0.142 mg/Kg - dry 0.142 0.841Phenol 1 02/06/24 20:32 V43256TJW
0.272 J mg/Kg - dry 0.170 0.841Pyrene 1 02/06/24 20:32 V43256TJW
<0.101 mg/Kg - dry 0.101 0.420Pyridine 1 02/06/24 20:32 V43256TJW
<0.136 mg/Kg - dry 0.136 0.8411,2,4-Trichlorobenzene 1 02/06/24 20:32 V43256TJW
<0.122 mg/Kg - dry 0.122 0.8412,4,5-Trichlorophenol 1 02/06/24 20:32 V43256TJW
<0.123 mg/Kg - dry 0.123 0.8412,4,6-Trichlorophenol 1 02/06/24 20:32 V43256TJW
8270ESurrogate: Phenol-d5 85.3 Limits: 34-121%02/06/24 20:321 TJW
Surrogate: 2-Fluorobiphenyl 84.4 Limits: 44-115%02/06/24 20:321 TJW V43256
Surrogate: 2-Fluorophenol 91.9 Limits: 35-115%02/06/24 20:321 TJW V43256
Surrogate: Nitrobenzene-d5 89.2 Limits: 37-122%02/06/24 20:321 TJW V43256
Surrogate: 4-Terphenyl-d14 81.4 Limits: 54-127%02/06/24 20:321 TJW V43256
Surrogate: 2,4,6-Tribromophenol 94.0 Limits: 39-132%02/06/24 20:321 TJW V43256
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 43 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:MW-1 (12)
95683 Matrix:
1/26/2024 9:43
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V43116 02/02/24 09:50
918 mg/Kg - dry 58.9 320Aliphatic C9-C18 5 02/08/24 13:35 V43311NDL
190 mg/Kg - dry 15.6 64.0Aliphatic C19-C36 1 02/07/24 20:55 V43311NDL
571 mg/Kg - dry 90.9 320Aromatic C11-C22 5 02/08/24 13:35 V43311NDL
MADEP-EPHSurrogate: 2-Bromonaphthalene 107 Limits: 40-140%02/07/24 20:551 NDL
MADEP-EPHSurrogate: Chlorooctadecane 56.4 Limits: 40-140%02/07/24 20:551 NDL
MADEP-EPHSurrogate: OTP Surrogate 106 Limits: 40-140%02/07/24 20:551 NDL
Surrogate: 2-Fluorobiphenyl 102 Limits: 40-140%02/07/24 20:551 NDL V43311
MADEP-EPHSurrogate: 2-Bromonaphthalene 60.2 Limits: 40-140%02/08/24 13:355 NDL
MADEP-EPHSurrogate: Chlorooctadecane 59.2 Limits: 40-140%02/08/24 13:355 NDL
MADEP-EPHSurrogate: OTP Surrogate 86.7 Limits: 40-140%02/08/24 13:355 NDL
Surrogate: 2-Fluorobiphenyl 73.4 Limits: 40-140%02/08/24 13:355 NDL V43311
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V43048 01/31/24 08:00
<1.56 mg/Kg - dry 1.56 10.2Aliphatic C5-C8 100 02/01/24 00:51 V43049TBL
45.5 mg/Kg - dry 5.82 10.2Aliphatic C9-C12 100 02/01/24 00:51 V43049TBL
27.0 mg/Kg - dry 0.795 10.2Aromatic C9-C10 100 02/01/24 00:51 V43049TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)92.1 Limits: 70-130%02/01/24 00:51100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)118 Limits: 70-130%02/01/24 00:51100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 44 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B1 (12)
95684 Matrix:
1/26/2024 10:38
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.4 %Moisture 1 02/02/24 11:55 SW-DRYWTPEB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 45 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B1 (12)
95684 Matrix:
1/26/2024 10:38
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
0.013 J mg/Kg - dry 0.003 0.026Acetone 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 01/31/24 23:24 V43078TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 01/31/24 23:24 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 01/31/24 23:24 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 01/31/24 23:24 V43078TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 01/31/24 23:24 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 01/31/24 23:24 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 01/31/24 23:24 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 01/31/24 23:24 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 01/31/24 23:24 V43078TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 01/31/24 23:24 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 01/31/24 23:24 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 01/31/24 23:24 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 01/31/24 23:24 V43078TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 01/31/24 23:24 V43078TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 01/31/24 23:24 V43078TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 46 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B1 (12)
95684 Matrix:
1/26/2024 10:38
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 01/31/24 23:24 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 01/31/24 23:24 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 01/31/24 23:24 V43078TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 01/31/24 23:24 V43078TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 01/31/24 23:24 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 01/31/24 23:24 V43078TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 01/31/24 23:24 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 01/31/24 23:24 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 01/31/24 23:24 V43078TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 01/31/24 23:24 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 01/31/24 23:24 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 01/31/24 23:24 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 01/31/24 23:24 V43078TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 47 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B1 (12)
95684 Matrix:
1/26/2024 10:38
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 01/31/24 23:24 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 01/31/24 23:24 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.026Methyl Ethyl Ketone (MEK)1 01/31/24 23:24 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 01/31/24 23:24 V43078TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 01/31/24 23:24 V43078TBL
0.004 J mg/Kg - dry 0.001 0.013Methylene Chloride 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 01/31/24 23:24 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 01/31/24 23:24 V43078TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 01/31/24 23:24 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 01/31/24 23:24 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 01/31/24 23:24 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 01/31/24 23:24 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 01/31/24 23:24 V43078TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 01/31/24 23:24 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 01/31/24 23:24 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 01/31/24 23:24 V43078TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 48 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B1 (12)
95684 Matrix:
1/26/2024 10:38
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 01/31/24 23:24 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 01/31/24 23:24 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 01/31/24 23:24 V43078TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 01/31/24 23:24 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 01/31/24 23:24 V43078
Surrogate: 4-Bromofluorobenzene 86.7 Limits: 70-130%01/31/24 23:241 TBL V43078
Surrogate: Dibromofluoromethane 86.0 Limits: 84-123%01/31/24 23:241 TBL V43078
Surrogate: Toluene-d8 99.1 Limits: 76-129%01/31/24 23:241 TBL V43078
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.151 mg/Kg - dry 0.151 0.861Acenaphthene 1 02/06/24 19:25 V43256TJW
<0.137 mg/Kg - dry 0.137 0.861Acenaphthylene 1 02/06/24 19:25 V43256TJW
<0.198 mg/Kg - dry 0.198 0.861Aniline 1 02/06/24 19:25 V43256TJW
<0.186 mg/Kg - dry 0.186 0.861Anthracene 1 02/06/24 19:25 V43256TJW
<0.181 mg/Kg - dry 0.181 0.861Benzo(a)anthracene 1 02/06/24 19:25 V43256TJW
<0.191 mg/Kg - dry 0.191 0.861Benzo(a)pyrene 1 02/06/24 19:25 V43256TJW
<0.190 mg/Kg - dry 0.190 0.861Benzo(b)fluoranthene 1 02/06/24 19:25 V43256TJW
<0.177 mg/Kg - dry 0.177 0.861Benzo(g,h,i)perylene 1 02/06/24 19:25 V43256TJW
<0.178 mg/Kg - dry 0.178 0.861Benzo(k)fluoranthene 1 02/06/24 19:25 V43256TJW
<0.757 mg/Kg - dry 0.757 2.61Benzoic Acid 1 02/06/24 19:25 V43256TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 49 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B1 (12)
95684 Matrix:
1/26/2024 10:38
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.137 mg/Kg - dry 0.137 0.861Benzyl alcohol 1 02/06/24 19:25 V43256TJW
<0.154 mg/Kg - dry 0.154 0.861Bis(2-Chloroethoxy)methane 1 02/06/24 19:25 V43256TJW
<0.139 mg/Kg - dry 0.139 0.861Bis(2-Chloroethyl)ether 1 02/06/24 19:25 V43256TJW
<0.177 mg/Kg - dry 0.177 0.430Bis(2-Chloroisopropyl)ether 1 02/06/24 19:25 V43256TJW
<0.156 mg/Kg - dry 0.156 0.861Bis(2-ethylhexyl)phthalate 1 02/06/24 19:25 V43256TJW
<0.142 mg/Kg - dry 0.142 0.8614-Bromophenyl phenyl ether 1 02/06/24 19:25 V43256TJW
<0.147 mg/Kg - dry 0.147 0.430Butyl benzyl phthalate 1 02/06/24 19:25 V43256TJW
<0.120 mg/Kg - dry 0.120 0.8614-Chloro-3-methylphenol 1 02/06/24 19:25 V43256TJW
<0.146 mg/Kg - dry 0.146 0.4304-Chloroaniline 1 02/06/24 19:25 V43256TJW
<0.151 mg/Kg - dry 0.151 0.8612-Chloronaphthalene 1 02/06/24 19:25 V43256TJW
<0.128 mg/Kg - dry 0.128 0.8612-Chlorophenol 1 02/06/24 19:25 V43256TJW
<0.164 mg/Kg - dry 0.164 1.314-Chlorophenyl phenyl ether 1 02/06/24 19:25 V43256TJW
<0.185 mg/Kg - dry 0.185 0.861Chrysene 1 02/06/24 19:25 V43256TJW
<0.300 mg/Kg - dry 0.300 0.861Dibenz(a,h)anthracene 1 02/06/24 19:25 V43256TJW
<0.155 mg/Kg - dry 0.155 0.861Dibenzofuran 1 02/06/24 19:25 V43256TJW
<0.123 mg/Kg - dry 0.123 0.8611,2-Dichlorobenzene 1 02/06/24 19:25 V43256TJW
<0.127 mg/Kg - dry 0.127 0.8611,3-Dichlorobenzene 1 02/06/24 19:25 V43256TJW
<0.127 mg/Kg - dry 0.127 0.4301,4-Dichlorobenzene 1 02/06/24 19:25 V43256TJW
<0.191 mg/Kg - dry 0.191 0.8613,3'-Dichlorobenzidine 1 02/06/24 19:25 V43256TJW
<0.125 mg/Kg - dry 0.125 0.8612,4-Dichlorophenol 1 02/06/24 19:25 V43256TJW
<0.234 mg/Kg - dry 0.234 0.861Diethyl phthalate 1 02/06/24 19:25 V43256TJW
<0.227 mg/Kg - dry 0.227 0.861Dimethyl phthalate 1 02/06/24 19:25 V43256TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 50 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B1 (12)
95684 Matrix:
1/26/2024 10:38
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.140 mg/Kg - dry 0.140 0.4302,4-Dimethylphenol 1 02/06/24 19:25 V43256TJW
<0.139 mg/Kg - dry 0.139 0.861Di-n-butyl phthalate 1 02/06/24 19:25 V43256TJW
<0.313 mg/Kg - dry 0.313 1.964,6-Dinitro-2-methylphenol 1 02/06/24 19:25 V43256TJW
<0.678 mg/Kg - dry 0.678 1.962,4-Dinitrophenol 1 02/06/24 19:25 V43256TJW
<0.126 mg/Kg - dry 0.126 0.8612,4-Dinitrotoluene 1 02/06/24 19:25 V43256TJW
<0.140 mg/Kg - dry 0.140 0.8612,6-Dinitrotoluene 1 02/06/24 19:25 V43256TJW
<0.186 mg/Kg - dry 0.186 0.430Di-n-Octyl Phthalate 1 02/06/24 19:25 V43256TJW
<0.160 mg/Kg - dry 0.160 0.861Fluoranthene 1 02/06/24 19:25 V43256TJW
<0.167 mg/Kg - dry 0.167 0.861Fluorene 1 02/06/24 19:25 V43256TJW
<0.138 mg/Kg - dry 0.138 0.861Hexachlorobenzene 1 02/06/24 19:25 V43256TJW
<0.127 mg/Kg - dry 0.127 0.861Hexachlorobutadiene 1 02/06/24 19:25 V43256TJW
<0.204 mg/Kg - dry 0.204 0.861Hexachlorocyclopentadiene 1 02/06/24 19:25 V43256TJW
<0.103 mg/Kg - dry 0.103 0.861Hexachloroethane 1 02/06/24 19:25 V43256TJW
<0.233 mg/Kg - dry 0.233 0.861Indeno(1,2,3-cd)pyrene 1 02/06/24 19:25 V43256TJW
<0.249 mg/Kg - dry 0.249 0.861Isophorone 1 02/06/24 19:25 V43256TJW
<0.138 mg/Kg - dry 0.138 0.8611-Methylnaphthalene 1 02/06/24 19:25 V43256TJW
<0.130 mg/Kg - dry 0.130 0.8612-Methylnaphthalene 1 02/06/24 19:25 V43256TJW
<0.126 mg/Kg - dry 0.126 0.8612-Methylphenol 1 02/06/24 19:25 V43256TJW
<0.110 mg/Kg - dry 0.110 0.8613&4 Methylphenol 1 02/06/24 19:25 V43256TJW
<0.187 mg/Kg - dry 0.187 0.861Naphthalene 1 02/06/24 19:25 V43256TJW
<0.126 mg/Kg - dry 0.126 0.8612-Nitroaniline 1 02/06/24 19:25 V43256TJW
<0.156 mg/Kg - dry 0.156 0.8613-Nitroaniline 1 02/06/24 19:25 V43256TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 51 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B1 (12)
95684 Matrix:
1/26/2024 10:38
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.121 mg/Kg - dry 0.121 0.4304-Nitroaniline 1 02/06/24 19:25 V43256TJW
<0.151 mg/Kg - dry 0.151 0.430Nitrobenzene 1 02/06/24 19:25 V43256TJW
<0.115 mg/Kg - dry 0.115 0.8612-Nitrophenol 1 02/06/24 19:25 V43256TJW
<0.152 mg/Kg - dry 0.152 0.8614-Nitrophenol 1 02/06/24 19:25 V43256TJW
<0.343 mg/Kg - dry 0.343 0.861N-Nitrosodimethylamine 1 02/06/24 19:25 V43256TJW
<0.236 mg/Kg - dry 0.236 0.861N-Nitrosodiphenylamine 1 02/06/24 19:25 V43256TJW
<0.154 mg/Kg - dry 0.154 0.861N-Nitroso-di-n-propylamine 1 02/06/24 19:25 V43256TJW
<0.453 mg/Kg - dry 0.453 1.31Pentachlorophenol 1 02/06/24 19:25 V43256TJW
<0.271 mg/Kg - dry 0.271 0.861Phenanthrene 1 02/06/24 19:25 V43256TJW
<0.146 mg/Kg - dry 0.146 0.861Phenol 1 02/06/24 19:25 V43256TJW
<0.174 mg/Kg - dry 0.174 0.861Pyrene 1 02/06/24 19:25 V43256TJW
<0.103 mg/Kg - dry 0.103 0.430Pyridine 1 02/06/24 19:25 V43256TJW
<0.139 mg/Kg - dry 0.139 0.8611,2,4-Trichlorobenzene 1 02/06/24 19:25 V43256TJW
<0.125 mg/Kg - dry 0.125 0.8612,4,5-Trichlorophenol 1 02/06/24 19:25 V43256TJW
<0.126 mg/Kg - dry 0.126 0.8612,4,6-Trichlorophenol 1 02/06/24 19:25 V43256TJW
8270ESurrogate: Phenol-d5 88.0 Limits: 34-121%02/06/24 19:251 TJW
Surrogate: 2-Fluorobiphenyl 85.6 Limits: 44-115%02/06/24 19:251 TJW V43256
Surrogate: 2-Fluorophenol 92.2 Limits: 35-115%02/06/24 19:251 TJW V43256
Surrogate: Nitrobenzene-d5 80.8 Limits: 37-122%02/06/24 19:251 TJW V43256
Surrogate: 4-Terphenyl-d14 85.6 Limits: 54-127%02/06/24 19:251 TJW V43256
Surrogate: 2,4,6-Tribromophenol 88.9 Limits: 39-132%02/06/24 19:251 TJW V43256
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 52 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B1 (12)
95684 Matrix:
1/26/2024 10:38
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V43116 02/02/24 09:50
<12.0 mg/Kg - dry 12.0 65.3Aliphatic C9-C18 1 02/07/24 21:31 V43311NDL
<15.9 mg/Kg - dry 15.9 65.3Aliphatic C19-C36 1 02/07/24 21:31 V43311NDL
<18.5 mg/Kg - dry 18.5 65.3Aromatic C11-C22 1 02/07/24 21:31 V43311NDL
MADEP-EPHSurrogate: 2-Bromonaphthalene 95.8 Limits: 40-140%02/07/24 21:311 NDL
MADEP-EPHSurrogate: Chlorooctadecane 73.8 Limits: 40-140%02/07/24 21:311 NDL
MADEP-EPHSurrogate: OTP Surrogate 102 Limits: 40-140%02/07/24 21:311 NDL
Surrogate: 2-Fluorobiphenyl 101 Limits: 40-140%02/07/24 21:311 NDL V43311
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V43048 01/31/24 08:00
<1.59 mg/Kg - dry 1.59 10.4Aliphatic C5-C8 100 01/31/24 23:40 V43049TBL
<5.95 mg/Kg - dry 5.95 10.4Aliphatic C9-C12 100 01/31/24 23:40 V43049TBL
<0.814 mg/Kg - dry 0.814 10.4Aromatic C9-C10 100 01/31/24 23:40 V43049TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)111 Limits: 70-130%01/31/24 23:40100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)113 Limits: 70-130%01/31/24 23:40100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 53 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B2 (12)
95685 Matrix:
1/26/2024 11:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
22.0 %Moisture 1 02/02/24 11:55 SW-DRYWTPEB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 54 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B2 (12)
95685 Matrix:
1/26/2024 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
<0.003 mg/Kg - dry 0.003 0.025Acetone 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 01/31/24 23:52 V43078TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 01/31/24 23:52 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 01/31/24 23:52 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 01/31/24 23:52 V43078TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 01/31/24 23:52 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 01/31/24 23:52 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 01/31/24 23:52 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 01/31/24 23:52 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 01/31/24 23:52 V43078TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 01/31/24 23:52 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 01/31/24 23:52 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 01/31/24 23:52 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 01/31/24 23:52 V43078TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 01/31/24 23:52 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 01/31/24 23:52 V43078TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 55 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B2 (12)
95685 Matrix:
1/26/2024 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 01/31/24 23:52 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 01/31/24 23:52 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 01/31/24 23:52 V43078TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 01/31/24 23:52 V43078TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 01/31/24 23:52 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 01/31/24 23:52 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 01/31/24 23:52 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 01/31/24 23:52 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 01/31/24 23:52 V43078TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 01/31/24 23:52 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 01/31/24 23:52 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.064Ethyl Tertiary Butyl Ether (ETBE)1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 01/31/24 23:52 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 01/31/24 23:52 V43078TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 56 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B2 (12)
95685 Matrix:
1/26/2024 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 01/31/24 23:52 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 01/31/24 23:52 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 01/31/24 23:52 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 01/31/24 23:52 V43078TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 01/31/24 23:52 V43078TBL
0.004 J mg/Kg - dry 0.001 0.012Naphthalene 1 01/31/24 23:52 V43078TBL
0.001 J mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 01/31/24 23:52 V43078TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 01/31/24 23:52 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 01/31/24 23:52 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 01/31/24 23:52 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 01/31/24 23:52 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 01/31/24 23:52 V43078TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 01/31/24 23:52 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 01/31/24 23:52 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 01/31/24 23:52 V43078TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 57 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B2 (12)
95685 Matrix:
1/26/2024 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 01/31/24 23:52 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 01/31/24 23:52 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 01/31/24 23:52 V43078TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 01/31/24 23:52 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 01/31/24 23:52 V43078
Surrogate: 4-Bromofluorobenzene 120 Limits: 70-130%01/31/24 23:521 TBL V43078
Surrogate: Dibromofluoromethane 85.6 Limits: 84-123%01/31/24 23:521 TBL V43078
Surrogate: Toluene-d8 101 Limits: 76-129%01/31/24 23:521 TBL V43078
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.148 mg/Kg - dry 0.148 0.846Acenaphthene 1 02/06/24 23:11 V43256TJW
<0.134 mg/Kg - dry 0.134 0.846Acenaphthylene 1 02/06/24 23:11 V43256TJW
<0.194 mg/Kg - dry 0.194 0.846Aniline 1 02/06/24 23:11 V43256TJW
<0.183 mg/Kg - dry 0.183 0.846Anthracene 1 02/06/24 23:11 V43256TJW
<0.178 mg/Kg - dry 0.178 0.846Benzo(a)anthracene 1 02/06/24 23:11 V43256TJW
<0.188 mg/Kg - dry 0.188 0.846Benzo(a)pyrene 1 02/06/24 23:11 V43256TJW
<0.187 mg/Kg - dry 0.187 0.846Benzo(b)fluoranthene 1 02/06/24 23:11 V43256TJW
<0.174 mg/Kg - dry 0.174 0.846Benzo(g,h,i)perylene 1 02/06/24 23:11 V43256TJW
<0.175 mg/Kg - dry 0.175 0.846Benzo(k)fluoranthene 1 02/06/24 23:11 V43256TJW
<0.743 mg/Kg - dry 0.743 2.56Benzoic Acid 1 02/06/24 23:11 V43256TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 58 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B2 (12)
95685 Matrix:
1/26/2024 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.134 mg/Kg - dry 0.134 0.846Benzyl alcohol 1 02/06/24 23:11 V43256TJW
<0.151 mg/Kg - dry 0.151 0.846Bis(2-Chloroethoxy)methane 1 02/06/24 23:11 V43256TJW
<0.137 mg/Kg - dry 0.137 0.846Bis(2-Chloroethyl)ether 1 02/06/24 23:11 V43256TJW
<0.174 mg/Kg - dry 0.174 0.423Bis(2-Chloroisopropyl)ether 1 02/06/24 23:11 V43256TJW
<0.153 mg/Kg - dry 0.153 0.846Bis(2-ethylhexyl)phthalate 1 02/06/24 23:11 V43256TJW
<0.139 mg/Kg - dry 0.139 0.8464-Bromophenyl phenyl ether 1 02/06/24 23:11 V43256TJW
<0.144 mg/Kg - dry 0.144 0.423Butyl benzyl phthalate 1 02/06/24 23:11 V43256TJW
<0.118 mg/Kg - dry 0.118 0.8464-Chloro-3-methylphenol 1 02/06/24 23:11 V43256TJW
<0.143 mg/Kg - dry 0.143 0.4234-Chloroaniline 1 02/06/24 23:11 V43256TJW
<0.148 mg/Kg - dry 0.148 0.8462-Chloronaphthalene 1 02/06/24 23:11 V43256TJW
<0.125 mg/Kg - dry 0.125 0.8462-Chlorophenol 1 02/06/24 23:11 V43256TJW
<0.161 mg/Kg - dry 0.161 1.284-Chlorophenyl phenyl ether 1 02/06/24 23:11 V43256TJW
<0.182 mg/Kg - dry 0.182 0.846Chrysene 1 02/06/24 23:11 V43256TJW
<0.294 mg/Kg - dry 0.294 0.846Dibenz(a,h)anthracene 1 02/06/24 23:11 V43256TJW
<0.152 mg/Kg - dry 0.152 0.846Dibenzofuran 1 02/06/24 23:11 V43256TJW
<0.121 mg/Kg - dry 0.121 0.8461,2-Dichlorobenzene 1 02/06/24 23:11 V43256TJW
<0.124 mg/Kg - dry 0.124 0.8461,3-Dichlorobenzene 1 02/06/24 23:11 V43256TJW
<0.125 mg/Kg - dry 0.125 0.4231,4-Dichlorobenzene 1 02/06/24 23:11 V43256TJW
<0.188 mg/Kg - dry 0.188 0.8463,3'-Dichlorobenzidine 1 02/06/24 23:11 V43256TJW
<0.122 mg/Kg - dry 0.122 0.8462,4-Dichlorophenol 1 02/06/24 23:11 V43256TJW
<0.230 mg/Kg - dry 0.230 0.846Diethyl phthalate 1 02/06/24 23:11 V43256TJW
<0.223 mg/Kg - dry 0.223 0.846Dimethyl phthalate 1 02/06/24 23:11 V43256TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 59 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B2 (12)
95685 Matrix:
1/26/2024 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.138 mg/Kg - dry 0.138 0.4232,4-Dimethylphenol 1 02/06/24 23:11 V43256TJW
<0.137 mg/Kg - dry 0.137 0.846Di-n-butyl phthalate 1 02/06/24 23:11 V43256TJW
<0.307 mg/Kg - dry 0.307 1.924,6-Dinitro-2-methylphenol 1 02/06/24 23:11 V43256TJW
<0.666 mg/Kg - dry 0.666 1.922,4-Dinitrophenol 1 02/06/24 23:11 V43256TJW
<0.123 mg/Kg - dry 0.123 0.8462,4-Dinitrotoluene 1 02/06/24 23:11 V43256TJW
<0.138 mg/Kg - dry 0.138 0.8462,6-Dinitrotoluene 1 02/06/24 23:11 V43256TJW
<0.183 mg/Kg - dry 0.183 0.423Di-n-Octyl Phthalate 1 02/06/24 23:11 V43256TJW
<0.157 mg/Kg - dry 0.157 0.846Fluoranthene 1 02/06/24 23:11 V43256TJW
<0.164 mg/Kg - dry 0.164 0.846Fluorene 1 02/06/24 23:11 V43256TJW
<0.135 mg/Kg - dry 0.135 0.846Hexachlorobenzene 1 02/06/24 23:11 V43256TJW
<0.125 mg/Kg - dry 0.125 0.846Hexachlorobutadiene 1 02/06/24 23:11 V43256TJW
<0.201 mg/Kg - dry 0.201 0.846Hexachlorocyclopentadiene 1 02/06/24 23:11 V43256TJW
<0.101 mg/Kg - dry 0.101 0.846Hexachloroethane 1 02/06/24 23:11 V43256TJW
<0.229 mg/Kg - dry 0.229 0.846Indeno(1,2,3-cd)pyrene 1 02/06/24 23:11 V43256TJW
<0.244 mg/Kg - dry 0.244 0.846Isophorone 1 02/06/24 23:11 V43256TJW
<0.135 mg/Kg - dry 0.135 0.8461-Methylnaphthalene 1 02/06/24 23:11 V43256TJW
<0.128 mg/Kg - dry 0.128 0.8462-Methylnaphthalene 1 02/06/24 23:11 V43256TJW
<0.124 mg/Kg - dry 0.124 0.8462-Methylphenol 1 02/06/24 23:11 V43256TJW
<0.108 mg/Kg - dry 0.108 0.8463&4 Methylphenol 1 02/06/24 23:11 V43256TJW
<0.184 mg/Kg - dry 0.184 0.846Naphthalene 1 02/06/24 23:11 V43256TJW
<0.123 mg/Kg - dry 0.123 0.8462-Nitroaniline 1 02/06/24 23:11 V43256TJW
<0.153 mg/Kg - dry 0.153 0.8463-Nitroaniline 1 02/06/24 23:11 V43256TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 60 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B2 (12)
95685 Matrix:
1/26/2024 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.119 mg/Kg - dry 0.119 0.4234-Nitroaniline 1 02/06/24 23:11 V43256TJW
<0.148 mg/Kg - dry 0.148 0.423Nitrobenzene 1 02/06/24 23:11 V43256TJW
<0.113 mg/Kg - dry 0.113 0.8462-Nitrophenol 1 02/06/24 23:11 V43256TJW
<0.150 mg/Kg - dry 0.150 0.8464-Nitrophenol 1 02/06/24 23:11 V43256TJW
<0.337 mg/Kg - dry 0.337 0.846N-Nitrosodimethylamine 1 02/06/24 23:11 V43256TJW
<0.232 mg/Kg - dry 0.232 0.846N-Nitrosodiphenylamine 1 02/06/24 23:11 V43256TJW
<0.151 mg/Kg - dry 0.151 0.846N-Nitroso-di-n-propylamine 1 02/06/24 23:11 V43256TJW
<0.444 mg/Kg - dry 0.444 1.28Pentachlorophenol 1 02/06/24 23:11 V43256TJW
<0.266 mg/Kg - dry 0.266 0.846Phenanthrene 1 02/06/24 23:11 V43256TJW
<0.143 mg/Kg - dry 0.143 0.846Phenol 1 02/06/24 23:11 V43256TJW
<0.171 mg/Kg - dry 0.171 0.846Pyrene 1 02/06/24 23:11 V43256TJW
<0.101 mg/Kg - dry 0.101 0.423Pyridine 1 02/06/24 23:11 V43256TJW
<0.137 mg/Kg - dry 0.137 0.8461,2,4-Trichlorobenzene 1 02/06/24 23:11 V43256TJW
<0.123 mg/Kg - dry 0.123 0.8462,4,5-Trichlorophenol 1 02/06/24 23:11 V43256TJW
<0.123 mg/Kg - dry 0.123 0.8462,4,6-Trichlorophenol 1 02/06/24 23:11 V43256TJW
8270ESurrogate: Phenol-d5 84.1 Limits: 34-121%02/06/24 23:111 TJW
Surrogate: 2-Fluorobiphenyl 80.7 Limits: 44-115%02/06/24 23:111 TJW V43256
Surrogate: 2-Fluorophenol 88.9 Limits: 35-115%02/06/24 23:111 TJW V43256
Surrogate: Nitrobenzene-d5 77.7 Limits: 37-122%02/06/24 23:111 TJW V43256
Surrogate: 4-Terphenyl-d14 82.5 Limits: 54-127%02/06/24 23:111 TJW V43256
Surrogate: 2,4,6-Tribromophenol 88.6 Limits: 39-132%02/06/24 23:111 TJW V43256
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 61 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B2 (12)
95685 Matrix:
1/26/2024 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V43116 02/02/24 09:50
301 mg/Kg - dry 11.8 64.0Aliphatic C9-C18 1 02/07/24 22:08 V43311NDL
80.8 mg/Kg - dry 15.6 64.0Aliphatic C19-C36 1 02/07/24 22:08 V43311NDL
78.5 mg/Kg - dry 18.2 64.0Aromatic C11-C22 1 02/07/24 22:08 V43311NDL
MADEP-EPHSurrogate: 2-Bromonaphthalene 100 Limits: 40-140%02/07/24 22:081 NDL
MADEP-EPHSurrogate: Chlorooctadecane 72.8 Limits: 40-140%02/07/24 22:081 NDL
MADEP-EPHSurrogate: OTP Surrogate 108 Limits: 40-140%02/07/24 22:081 NDL
Surrogate: 2-Fluorobiphenyl 106 Limits: 40-140%02/07/24 22:081 NDL V43311
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V43048 01/31/24 08:00
<1.56 mg/Kg - dry 1.56 10.3Aliphatic C5-C8 100 02/01/24 00:04 V43049TBL
<5.85 mg/Kg - dry 5.85 10.3Aliphatic C9-C12 100 02/01/24 00:04 V43049TBL
<0.800 mg/Kg - dry 0.800 10.3Aromatic C9-C10 100 02/01/24 00:04 V43049TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)96.3 Limits: 70-130%02/01/24 00:04100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)111 Limits: 70-130%02/01/24 00:04100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 62 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B3 (12)
95686 Matrix:
1/26/2024 11:25
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
24.3 %Moisture 1 02/02/24 11:55 SW-DRYWTPEB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 63 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B3 (12)
95686 Matrix:
1/26/2024 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
0.042 mg/Kg - dry 0.003 0.026Acetone 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 02/01/24 00:19 V43078TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 02/01/24 00:19 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 02/01/24 00:19 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 02/01/24 00:19 V43078TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 02/01/24 00:19 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 02/01/24 00:19 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 02/01/24 00:19 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 02/01/24 00:19 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 02/01/24 00:19 V43078TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 02/01/24 00:19 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 02/01/24 00:19 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 02/01/24 00:19 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 02/01/24 00:19 V43078TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 02/01/24 00:19 V43078TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 02/01/24 00:19 V43078TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 64 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B3 (12)
95686 Matrix:
1/26/2024 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 02/01/24 00:19 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 02/01/24 00:19 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 02/01/24 00:19 V43078TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 02/01/24 00:19 V43078TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 02/01/24 00:19 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 02/01/24 00:19 V43078TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 02/01/24 00:19 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 02/01/24 00:19 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 02/01/24 00:19 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 02/01/24 00:19 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.066Ethyl Tertiary Butyl Ether (ETBE)1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 02/01/24 00:19 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 02/01/24 00:19 V43078TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 65 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B3 (12)
95686 Matrix:
1/26/2024 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 02/01/24 00:19 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 02/01/24 00:19 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 02/01/24 00:19 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 02/01/24 00:19 V43078TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 02/01/24 00:19 V43078TBL
0.007 J mg/Kg - dry 0.001 0.013Methylene Chloride 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 02/01/24 00:19 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 02/01/24 00:19 V43078TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 02/01/24 00:19 V43078TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 02/01/24 00:19 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 02/01/24 00:19 V43078TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 02/01/24 00:19 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 02/01/24 00:19 V43078TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 02/01/24 00:19 V43078TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 02/01/24 00:19 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 02/01/24 00:19 V43078TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 66 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B3 (12)
95686 Matrix:
1/26/2024 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43077 01/31/24 08:00
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 02/01/24 00:19 V43078TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 02/01/24 00:19 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 02/01/24 00:19 V43078TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 02/01/24 00:19 V43078TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 02/01/24 00:19 V43078
Surrogate: 4-Bromofluorobenzene 110 Limits: 70-130%02/01/24 00:191 TBL V43078
Surrogate: Dibromofluoromethane 114 Limits: 84-123%02/01/24 00:191 TBL V43078
Surrogate: Toluene-d8 87.0 Limits: 76-129%02/01/24 00:191 TBL V43078
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.153 mg/Kg - dry 0.153 0.871Acenaphthene 1 02/06/24 17:54 V43256TJW
<0.138 mg/Kg - dry 0.138 0.871Acenaphthylene 1 02/06/24 17:54 V43256TJW
<0.200 mg/Kg - dry 0.200 0.871Aniline 1 02/06/24 17:54 V43256TJW
<0.188 mg/Kg - dry 0.188 0.871Anthracene 1 02/06/24 17:54 V43256TJW
<0.183 mg/Kg - dry 0.183 0.871Benzo(a)anthracene 1 02/06/24 17:54 V43256TJW
<0.194 mg/Kg - dry 0.194 0.871Benzo(a)pyrene 1 02/06/24 17:54 V43256TJW
<0.192 mg/Kg - dry 0.192 0.871Benzo(b)fluoranthene 1 02/06/24 17:54 V43256TJW
<0.179 mg/Kg - dry 0.179 0.871Benzo(g,h,i)perylene 1 02/06/24 17:54 V43256TJW
<0.180 mg/Kg - dry 0.180 0.871Benzo(k)fluoranthene 1 02/06/24 17:54 V43256TJW
<0.766 mg/Kg - dry 0.766 2.64Benzoic Acid 1 02/06/24 17:54 V43256TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 67 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B3 (12)
95686 Matrix:
1/26/2024 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.138 mg/Kg - dry 0.138 0.871Benzyl alcohol 1 02/06/24 17:54 V43256TJW
<0.155 mg/Kg - dry 0.155 0.871Bis(2-Chloroethoxy)methane 1 02/06/24 17:54 V43256TJW
<0.141 mg/Kg - dry 0.141 0.871Bis(2-Chloroethyl)ether 1 02/06/24 17:54 V43256TJW
<0.179 mg/Kg - dry 0.179 0.435Bis(2-Chloroisopropyl)ether 1 02/06/24 17:54 V43256TJW
<0.158 mg/Kg - dry 0.158 0.871Bis(2-ethylhexyl)phthalate 1 02/06/24 17:54 V43256TJW
<0.143 mg/Kg - dry 0.143 0.8714-Bromophenyl phenyl ether 1 02/06/24 17:54 V43256TJW
<0.149 mg/Kg - dry 0.149 0.435Butyl benzyl phthalate 1 02/06/24 17:54 V43256TJW
<0.122 mg/Kg - dry 0.122 0.8714-Chloro-3-methylphenol 1 02/06/24 17:54 V43256TJW
<0.147 mg/Kg - dry 0.147 0.4354-Chloroaniline 1 02/06/24 17:54 V43256TJW
<0.153 mg/Kg - dry 0.153 0.8712-Chloronaphthalene 1 02/06/24 17:54 V43256TJW
<0.129 mg/Kg - dry 0.129 0.8712-Chlorophenol 1 02/06/24 17:54 V43256TJW
<0.166 mg/Kg - dry 0.166 1.324-Chlorophenyl phenyl ether 1 02/06/24 17:54 V43256TJW
<0.187 mg/Kg - dry 0.187 0.871Chrysene 1 02/06/24 17:54 V43256TJW
<0.303 mg/Kg - dry 0.303 0.871Dibenz(a,h)anthracene 1 02/06/24 17:54 V43256TJW
<0.157 mg/Kg - dry 0.157 0.871Dibenzofuran 1 02/06/24 17:54 V43256TJW
<0.124 mg/Kg - dry 0.124 0.8711,2-Dichlorobenzene 1 02/06/24 17:54 V43256TJW
<0.128 mg/Kg - dry 0.128 0.8711,3-Dichlorobenzene 1 02/06/24 17:54 V43256TJW
<0.128 mg/Kg - dry 0.128 0.4351,4-Dichlorobenzene 1 02/06/24 17:54 V43256TJW
<0.194 mg/Kg - dry 0.194 0.8713,3'-Dichlorobenzidine 1 02/06/24 17:54 V43256TJW
<0.126 mg/Kg - dry 0.126 0.8712,4-Dichlorophenol 1 02/06/24 17:54 V43256TJW
<0.237 mg/Kg - dry 0.237 0.871Diethyl phthalate 1 02/06/24 17:54 V43256TJW
<0.229 mg/Kg - dry 0.229 0.871Dimethyl phthalate 1 02/06/24 17:54 V43256TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 68 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B3 (12)
95686 Matrix:
1/26/2024 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.142 mg/Kg - dry 0.142 0.4352,4-Dimethylphenol 1 02/06/24 17:54 V43256TJW
<0.141 mg/Kg - dry 0.141 0.871Di-n-butyl phthalate 1 02/06/24 17:54 V43256TJW
<0.317 mg/Kg - dry 0.317 1.984,6-Dinitro-2-methylphenol 1 02/06/24 17:54 V43256TJW
<0.686 mg/Kg - dry 0.686 1.982,4-Dinitrophenol 1 02/06/24 17:54 V43256TJW
<0.127 mg/Kg - dry 0.127 0.8712,4-Dinitrotoluene 1 02/06/24 17:54 V43256TJW
<0.142 mg/Kg - dry 0.142 0.8712,6-Dinitrotoluene 1 02/06/24 17:54 V43256TJW
<0.188 mg/Kg - dry 0.188 0.435Di-n-Octyl Phthalate 1 02/06/24 17:54 V43256TJW
<0.162 mg/Kg - dry 0.162 0.871Fluoranthene 1 02/06/24 17:54 V43256TJW
<0.169 mg/Kg - dry 0.169 0.871Fluorene 1 02/06/24 17:54 V43256TJW
<0.140 mg/Kg - dry 0.140 0.871Hexachlorobenzene 1 02/06/24 17:54 V43256TJW
<0.128 mg/Kg - dry 0.128 0.871Hexachlorobutadiene 1 02/06/24 17:54 V43256TJW
<0.207 mg/Kg - dry 0.207 0.871Hexachlorocyclopentadiene 1 02/06/24 17:54 V43256TJW
<0.104 mg/Kg - dry 0.104 0.871Hexachloroethane 1 02/06/24 17:54 V43256TJW
<0.236 mg/Kg - dry 0.236 0.871Indeno(1,2,3-cd)pyrene 1 02/06/24 17:54 V43256TJW
<0.252 mg/Kg - dry 0.252 0.871Isophorone 1 02/06/24 17:54 V43256TJW
<0.140 mg/Kg - dry 0.140 0.8711-Methylnaphthalene 1 02/06/24 17:54 V43256TJW
<0.132 mg/Kg - dry 0.132 0.8712-Methylnaphthalene 1 02/06/24 17:54 V43256TJW
<0.128 mg/Kg - dry 0.128 0.8712-Methylphenol 1 02/06/24 17:54 V43256TJW
<0.112 mg/Kg - dry 0.112 0.8713&4 Methylphenol 1 02/06/24 17:54 V43256TJW
<0.190 mg/Kg - dry 0.190 0.871Naphthalene 1 02/06/24 17:54 V43256TJW
<0.127 mg/Kg - dry 0.127 0.8712-Nitroaniline 1 02/06/24 17:54 V43256TJW
<0.158 mg/Kg - dry 0.158 0.8713-Nitroaniline 1 02/06/24 17:54 V43256TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 69 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B3 (12)
95686 Matrix:
1/26/2024 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.123 mg/Kg - dry 0.123 0.4354-Nitroaniline 1 02/06/24 17:54 V43256TJW
<0.153 mg/Kg - dry 0.153 0.435Nitrobenzene 1 02/06/24 17:54 V43256TJW
<0.117 mg/Kg - dry 0.117 0.8712-Nitrophenol 1 02/06/24 17:54 V43256TJW
<0.154 mg/Kg - dry 0.154 0.8714-Nitrophenol 1 02/06/24 17:54 V43256TJW
<0.347 mg/Kg - dry 0.347 0.871N-Nitrosodimethylamine 1 02/06/24 17:54 V43256TJW
<0.239 mg/Kg - dry 0.239 0.871N-Nitrosodiphenylamine 1 02/06/24 17:54 V43256TJW
<0.155 mg/Kg - dry 0.155 0.871N-Nitroso-di-n-propylamine 1 02/06/24 17:54 V43256TJW
<0.458 mg/Kg - dry 0.458 1.32Pentachlorophenol 1 02/06/24 17:54 V43256TJW
<0.274 mg/Kg - dry 0.274 0.871Phenanthrene 1 02/06/24 17:54 V43256TJW
<0.147 mg/Kg - dry 0.147 0.871Phenol 1 02/06/24 17:54 V43256TJW
<0.177 mg/Kg - dry 0.177 0.871Pyrene 1 02/06/24 17:54 V43256TJW
<0.104 mg/Kg - dry 0.104 0.435Pyridine 1 02/06/24 17:54 V43256TJW
<0.141 mg/Kg - dry 0.141 0.8711,2,4-Trichlorobenzene 1 02/06/24 17:54 V43256TJW
<0.127 mg/Kg - dry 0.127 0.8712,4,5-Trichlorophenol 1 02/06/24 17:54 V43256TJW
<0.127 mg/Kg - dry 0.127 0.8712,4,6-Trichlorophenol 1 02/06/24 17:54 V43256TJW
8270ESurrogate: Phenol-d5 81.4 Limits: 34-121%02/06/24 17:541 TJW
Surrogate: 2-Fluorobiphenyl 81.4 Limits: 44-115%02/06/24 17:541 TJW V43256
Surrogate: 2-Fluorophenol 83.8 Limits: 35-115%02/06/24 17:541 TJW V43256
Surrogate: Nitrobenzene-d5 77.2 Limits: 37-122%02/06/24 17:541 TJW V43256
Surrogate: 4-Terphenyl-d14 79.6 Limits: 54-127%02/06/24 17:541 TJW V43256
Surrogate: 2,4,6-Tribromophenol 76.9 Limits: 39-132%02/06/24 17:541 TJW V43256
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 70 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B3 (12)
95686 Matrix:
1/26/2024 11:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V43116 02/02/24 09:50
<12.2 mg/Kg - dry 12.2 66.3Aliphatic C9-C18 1 02/07/24 22:44 V43311NDL
<16.1 mg/Kg - dry 16.1 66.3Aliphatic C19-C36 1 02/07/24 22:44 V43311NDL
<18.9 mg/Kg - dry 18.9 66.3Aromatic C11-C22 1 02/07/24 22:44 V43311NDL
MADEP-EPHSurrogate: 2-Bromonaphthalene 105 Limits: 40-140%02/07/24 22:441 NDL
MADEP-EPHSurrogate: Chlorooctadecane 77.8 Limits: 40-140%02/07/24 22:441 NDL
MADEP-EPHSurrogate: OTP Surrogate 110 Limits: 40-140%02/07/24 22:441 NDL
Surrogate: 2-Fluorobiphenyl 110 Limits: 40-140%02/07/24 22:441 NDL V43311
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V43048 01/31/24 08:00
<1.61 mg/Kg - dry 1.61 10.6Aliphatic C5-C8 100 02/01/24 00:27 V43049TBL
<6.02 mg/Kg - dry 6.02 10.6Aliphatic C9-C12 100 02/01/24 00:27 V43049TBL
<0.824 mg/Kg - dry 0.824 10.6Aromatic C9-C10 100 02/01/24 00:27 V43049TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)119 Limits: 70-130%02/01/24 00:27100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)130 Limits: 70-130%02/01/24 00:27100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 71 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B4 (12)
95687 Matrix:
1/26/2024 11:55
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
21.8 %Moisture 1 02/02/24 11:55 SW-DRYWTPEB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 72 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B4 (12)
95687 Matrix:
1/26/2024 11:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43079 01/31/24 08:00
<0.076 mg/Kg - dry 0.076 0.639Acetone 50 02/01/24 03:02 V43081TBL
<0.038 mg/Kg - dry 0.038 0.639Acrolein 50 02/01/24 03:02 V43081TBL
<0.024 mg/Kg - dry 0.024 0.639Acrylonitrile 50 02/01/24 03:02 V43081TBL
<0.018 mg/Kg - dry 0.018 0.159Benzene 50 02/01/24 03:02 V43081TBL
<0.015 mg/Kg - dry 0.015 0.159Bromobenzene 50 02/01/24 03:02 V43081TBL
<0.025 mg/Kg - dry 0.025 0.159Bromochloromethane 50 02/01/24 03:02 V43081TBL
<0.038 mg/Kg - dry 0.038 0.159Bromodichloromethane 50 02/01/24 03:02 V43081TBL
<0.032 mg/Kg - dry 0.032 0.159Bromoform 50 02/01/24 03:02 V43081TBL
<0.058 mg/Kg - dry 0.058 0.319Bromomethane 50 02/01/24 03:02 V43081TBL
4.03 mg/Kg - dry 0.015 0.159n-Butylbenzene 50 02/01/24 03:02 V43081TBL
2.21 mg/Kg - dry 0.017 0.159sec-Butyl benzene 50 02/01/24 03:02 V43081TBL
0.264 mg/Kg - dry 0.015 0.159tert-Butyl benzene 50 02/01/24 03:02 V43081TBL
<0.020 mg/Kg - dry 0.020 0.159Carbon Disulfide 50 02/01/24 03:02 V43081TBL
<0.050 mg/Kg - dry 0.050 0.159Carbon Tetrachloride 50 02/01/24 03:02 V43081TBL
<0.021 mg/Kg - dry 0.021 0.159Chlorobenzene 50 02/01/24 03:02 V43081TBL
<0.028 mg/Kg - dry 0.028 0.159Chlorodibromomethane 50 02/01/24 03:02 V43081TBL
<0.028 mg/Kg - dry 0.028 0.319Chloroethane 50 02/01/24 03:02 V43081TBL
<0.033 mg/Kg - dry 0.033 0.159Chloroform 50 02/01/24 03:02 V43081TBL
<0.020 mg/Kg - dry 0.020 0.319Chloromethane 50 02/01/24 03:02 V43081TBL
<0.016 mg/Kg - dry 0.016 0.1592-Chlorotoluene 50 02/01/24 03:02 V43081TBL
<0.012 mg/Kg - dry 0.012 0.1594-Chlorotoluene 50 02/01/24 03:02 V43081TBL
<0.023 mg/Kg - dry 0.023 0.159Di-Isopropyl Ether (DIPE)50 02/01/24 03:02 V43081TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 73 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B4 (12)
95687 Matrix:
1/26/2024 11:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43079 01/31/24 08:00
<0.014 mg/Kg - dry 0.014 0.3191,2-Dibromo-3-Chloropropane 50 02/01/24 03:02 V43081TBL
<0.018 mg/Kg - dry 0.018 0.1591,2-Dibromoethane 50 02/01/24 03:02 V43081TBL
<0.031 mg/Kg - dry 0.031 0.159Dibromomethane 50 02/01/24 03:02 V43081TBL
<0.009 mg/Kg - dry 0.009 0.1591,2-Dichlorobenzene 50 02/01/24 03:02 V43081TBL
<0.012 mg/Kg - dry 0.012 0.1591,3-Dichlorobenzene 50 02/01/24 03:02 V43081TBL
<0.019 mg/Kg - dry 0.019 0.1591,4-Dichlorobenzene 50 02/01/24 03:02 V43081TBL
<0.042 mg/Kg - dry 0.042 0.319Dichlorodifluoromethane 50 02/01/24 03:02 V43081TBL
<0.026 mg/Kg - dry 0.026 0.1591,1-Dichloroethane 50 02/01/24 03:02 V43081TBL
<0.044 mg/Kg - dry 0.044 0.1591,2-Dichloroethane 50 02/01/24 03:02 V43081TBL
<0.023 mg/Kg - dry 0.023 0.1591,1-Dichloroethene 50 02/01/24 03:02 V43081TBL
<0.025 mg/Kg - dry 0.025 0.159cis-1,2-Dichloroethene 50 02/01/24 03:02 V43081TBL
<0.033 mg/Kg - dry 0.033 0.159trans-1,2-Dichloroethene 50 02/01/24 03:02 V43081TBL
<0.014 mg/Kg - dry 0.014 0.1591,2-Dichloropropane 50 02/01/24 03:02 V43081TBL
<0.017 mg/Kg - dry 0.017 0.1591,3-Dichloropropane 50 02/01/24 03:02 V43081TBL
<0.040 mg/Kg - dry 0.040 0.1592,2-Dichloropropane 50 02/01/24 03:02 V43081TBL
<0.024 mg/Kg - dry 0.024 0.1591,1-Dichloropropene 50 02/01/24 03:02 V43081TBL
<0.017 mg/Kg - dry 0.017 0.159cis-1,3-Dichloropropene 50 02/01/24 03:02 V43081TBL
<0.025 mg/Kg - dry 0.025 0.159trans-1,3-Dichloropropene 50 02/01/24 03:02 V43081TBL
5.00 mg/Kg - dry 0.018 0.159Ethylbenzene 50 02/01/24 03:02 V43081TBL
<0.026 mg/Kg - dry 0.026 3.20Ethyl Tertiary Butyl Ether (ETBE)50 02/01/24 03:02 V43081TBL
<0.025 mg/Kg - dry 0.025 0.319Hexachlorobutadiene 50 02/01/24 03:02 V43081TBL
<0.021 mg/Kg - dry 0.021 0.319n-Hexane 50 02/01/24 03:02 V43081TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 74 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B4 (12)
95687 Matrix:
1/26/2024 11:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43079 01/31/24 08:00
<0.019 mg/Kg - dry 0.019 0.6392-Hexanone 50 02/01/24 03:02 V43081TBL
1.65 mg/Kg - dry 0.014 0.159Isopropylbenzene 50 02/01/24 03:02 V43081TBL
0.091 J mg/Kg - dry 0.041 0.1594-Isopropyl toluene 50 02/01/24 03:02 V43081TBL
<0.020 mg/Kg - dry 0.020 0.639Methyl Ethyl Ketone (MEK)50 02/01/24 03:02 V43081TBL
<0.019 mg/Kg - dry 0.019 0.159Methyl tert-butyl ether (MTBE)50 02/01/24 03:02 V43081TBL
<0.479 mg/Kg - dry 0.479 0.6394-Methyl-2-Pentanone 50 02/01/24 03:02 V43081TBL
<0.047 mg/Kg - dry 0.047 0.159Methylene Chloride 50 02/01/24 03:02 V43081TBL
43.0 mg/Kg - dry 0.317 3.20Naphthalene 500 02/01/24 03:29 V43081TBL
4.62 mg/Kg - dry 0.017 0.159n-Propylbenzene 50 02/01/24 03:02 V43081TBL
<0.045 mg/Kg - dry 0.045 0.159Styrene 50 02/01/24 03:02 V43081TBL
<0.033 mg/Kg - dry 0.033 0.1591,1,1,2-Tetrachloroethane 50 02/01/24 03:02 V43081TBL
<0.010 mg/Kg - dry 0.010 0.1591,1,2,2-Tetrachloroethane 50 02/01/24 03:02 V43081TBL
<0.028 mg/Kg - dry 0.028 0.159Tetrachloroethene 50 02/01/24 03:02 V43081TBL
<0.021 mg/Kg - dry 0.021 0.159Toluene 50 02/01/24 03:02 V43081TBL
<0.017 mg/Kg - dry 0.017 0.3191,2,3-Trichlorobenzene 50 02/01/24 03:02 V43081TBL
<0.020 mg/Kg - dry 0.020 0.3191,2,4-Trichlorobenzene 50 02/01/24 03:02 V43081TBL
<0.046 mg/Kg - dry 0.046 0.1591,1,1-Trichloroethane 50 02/01/24 03:02 V43081TBL
<0.015 mg/Kg - dry 0.015 0.1591,1,2-Trichloroethane 50 02/01/24 03:02 V43081TBL
<0.029 mg/Kg - dry 0.029 0.159Trichloroethene 50 02/01/24 03:02 V43081TBL
<0.066 mg/Kg - dry 0.066 0.319Trichlorofluoromethane 50 02/01/24 03:02 V43081TBL
<0.023 mg/Kg - dry 0.023 0.1591,2,3-Trichloropropane 50 02/01/24 03:02 V43081TBL
0.424 mg/Kg - dry 0.017 0.1591,3,5-Trimethylbenzene 50 02/01/24 03:02 V43081TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 75 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B4 (12)
95687 Matrix:
1/26/2024 11:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V43079 01/31/24 08:00
<0.014 mg/Kg - dry 0.014 0.319Vinyl Acetate 50 02/01/24 03:02 V43081TBL
<0.015 mg/Kg - dry 0.015 0.319Vinyl Chloride 50 02/01/24 03:02 V43081TBL
0.167 mg/Kg - dry 0.015 0.159o-Xylene 50 02/01/24 03:02 V43081TBL
0.090 J mg/Kg - dry 0.040 0.319m,p-Xylene 50 02/01/24 03:02 V43081TBL
0.258 J mg/Kg - dry 0.015 0.159Xylene (Total)50 02/01/24 03:02 V43081
Surrogate: 4-Bromofluorobenzene 118 Limits: 70-130%02/01/24 03:0250 TBL V43081
Surrogate: Dibromofluoromethane 97.7 Limits: 70-130%02/01/24 03:0250 TBL V43081
Surrogate: Toluene-d8 85.8 Limits: 76-129%02/01/24 03:0250 TBL V43081
Surrogate: 4-Bromofluorobenzene 89.9 Limits: 70-130%02/01/24 03:29500 TBL V43081
Surrogate: Dibromofluoromethane 84.6 Limits: 70-130%02/01/24 03:29500 TBL V43081
Surrogate: Toluene-d8 107 Limits: 76-129%02/01/24 03:29500 TBL V43081
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.148 mg/Kg - dry 0.148 0.843Acenaphthene 1 02/06/24 22:26 V43256TJW
<0.134 mg/Kg - dry 0.134 0.843Acenaphthylene 1 02/06/24 22:26 V43256TJW
<0.194 mg/Kg - dry 0.194 0.843Aniline 1 02/06/24 22:26 V43256TJW
<0.182 mg/Kg - dry 0.182 0.843Anthracene 1 02/06/24 22:26 V43256TJW
<0.177 mg/Kg - dry 0.177 0.843Benzo(a)anthracene 1 02/06/24 22:26 V43256TJW
<0.187 mg/Kg - dry 0.187 0.843Benzo(a)pyrene 1 02/06/24 22:26 V43256TJW
<0.186 mg/Kg - dry 0.186 0.843Benzo(b)fluoranthene 1 02/06/24 22:26 V43256TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 76 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B4 (12)
95687 Matrix:
1/26/2024 11:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.173 mg/Kg - dry 0.173 0.843Benzo(g,h,i)perylene 1 02/06/24 22:26 V43256TJW
<0.175 mg/Kg - dry 0.175 0.843Benzo(k)fluoranthene 1 02/06/24 22:26 V43256TJW
<0.741 mg/Kg - dry 0.741 2.56Benzoic Acid 1 02/06/24 22:26 V43256TJW
<0.134 mg/Kg - dry 0.134 0.843Benzyl alcohol 1 02/06/24 22:26 V43256TJW
<0.150 mg/Kg - dry 0.150 0.843Bis(2-Chloroethoxy)methane 1 02/06/24 22:26 V43256TJW
<0.136 mg/Kg - dry 0.136 0.843Bis(2-Chloroethyl)ether 1 02/06/24 22:26 V43256TJW
<0.173 mg/Kg - dry 0.173 0.421Bis(2-Chloroisopropyl)ether 1 02/06/24 22:26 V43256TJW
<0.153 mg/Kg - dry 0.153 0.843Bis(2-ethylhexyl)phthalate 1 02/06/24 22:26 V43256TJW
<0.139 mg/Kg - dry 0.139 0.8434-Bromophenyl phenyl ether 1 02/06/24 22:26 V43256TJW
<0.144 mg/Kg - dry 0.144 0.421Butyl benzyl phthalate 1 02/06/24 22:26 V43256TJW
<0.118 mg/Kg - dry 0.118 0.8434-Chloro-3-methylphenol 1 02/06/24 22:26 V43256TJW
<0.143 mg/Kg - dry 0.143 0.4214-Chloroaniline 1 02/06/24 22:26 V43256TJW
<0.148 mg/Kg - dry 0.148 0.8432-Chloronaphthalene 1 02/06/24 22:26 V43256TJW
<0.125 mg/Kg - dry 0.125 0.8432-Chlorophenol 1 02/06/24 22:26 V43256TJW
<0.161 mg/Kg - dry 0.161 1.284-Chlorophenyl phenyl ether 1 02/06/24 22:26 V43256TJW
<0.181 mg/Kg - dry 0.181 0.843Chrysene 1 02/06/24 22:26 V43256TJW
<0.294 mg/Kg - dry 0.294 0.843Dibenz(a,h)anthracene 1 02/06/24 22:26 V43256TJW
<0.152 mg/Kg - dry 0.152 0.843Dibenzofuran 1 02/06/24 22:26 V43256TJW
<0.120 mg/Kg - dry 0.120 0.8431,2-Dichlorobenzene 1 02/06/24 22:26 V43256TJW
<0.124 mg/Kg - dry 0.124 0.8431,3-Dichlorobenzene 1 02/06/24 22:26 V43256TJW
<0.124 mg/Kg - dry 0.124 0.4211,4-Dichlorobenzene 1 02/06/24 22:26 V43256TJW
<0.187 mg/Kg - dry 0.187 0.8433,3'-Dichlorobenzidine 1 02/06/24 22:26 V43256TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 77 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B4 (12)
95687 Matrix:
1/26/2024 11:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.122 mg/Kg - dry 0.122 0.8432,4-Dichlorophenol 1 02/06/24 22:26 V43256TJW
<0.230 mg/Kg - dry 0.230 0.843Diethyl phthalate 1 02/06/24 22:26 V43256TJW
<0.222 mg/Kg - dry 0.222 0.843Dimethyl phthalate 1 02/06/24 22:26 V43256TJW
<0.138 mg/Kg - dry 0.138 0.4212,4-Dimethylphenol 1 02/06/24 22:26 V43256TJW
<0.136 mg/Kg - dry 0.136 0.843Di-n-butyl phthalate 1 02/06/24 22:26 V43256TJW
<0.306 mg/Kg - dry 0.306 1.924,6-Dinitro-2-methylphenol 1 02/06/24 22:26 V43256TJW
<0.664 mg/Kg - dry 0.664 1.922,4-Dinitrophenol 1 02/06/24 22:26 V43256TJW
<0.123 mg/Kg - dry 0.123 0.8432,4-Dinitrotoluene 1 02/06/24 22:26 V43256TJW
<0.138 mg/Kg - dry 0.138 0.8432,6-Dinitrotoluene 1 02/06/24 22:26 V43256TJW
<0.182 mg/Kg - dry 0.182 0.421Di-n-Octyl Phthalate 1 02/06/24 22:26 V43256TJW
<0.157 mg/Kg - dry 0.157 0.843Fluoranthene 1 02/06/24 22:26 V43256TJW
4.67 mg/Kg - dry 0.163 0.843Fluorene 1 02/06/24 22:26 V43256TJW
<0.135 mg/Kg - dry 0.135 0.843Hexachlorobenzene 1 02/06/24 22:26 V43256TJW
<0.124 mg/Kg - dry 0.124 0.843Hexachlorobutadiene 1 02/06/24 22:26 V43256TJW
<0.200 mg/Kg - dry 0.200 0.843Hexachlorocyclopentadiene 1 02/06/24 22:26 V43256TJW
<0.101 mg/Kg - dry 0.101 0.843Hexachloroethane 1 02/06/24 22:26 V43256TJW
<0.228 mg/Kg - dry 0.228 0.843Indeno(1,2,3-cd)pyrene 1 02/06/24 22:26 V43256TJW
<0.244 mg/Kg - dry 0.244 0.843Isophorone 1 02/06/24 22:26 V43256TJW
36.6 mg/Kg - dry 1.36 8.441-Methylnaphthalene 10 02/07/24 14:23 V43256TJW
60.5 mg/Kg - dry 1.28 8.442-Methylnaphthalene 10 02/07/24 14:23 V43256TJW
<0.124 mg/Kg - dry 0.124 0.8432-Methylphenol 1 02/06/24 22:26 V43256TJW
<0.108 mg/Kg - dry 0.108 0.8433&4 Methylphenol 1 02/06/24 22:26 V43256TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 78 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B4 (12)
95687 Matrix:
1/26/2024 11:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
11.3 mg/Kg - dry 1.84 8.44Naphthalene 10 02/07/24 14:23 V43256TJW
<0.123 mg/Kg - dry 0.123 0.8432-Nitroaniline 1 02/06/24 22:26 V43256TJW
<0.153 mg/Kg - dry 0.153 0.8433-Nitroaniline 1 02/06/24 22:26 V43256TJW
<0.119 mg/Kg - dry 0.119 0.4214-Nitroaniline 1 02/06/24 22:26 V43256TJW
<0.148 mg/Kg - dry 0.148 0.421Nitrobenzene 1 02/06/24 22:26 V43256TJW
<0.113 mg/Kg - dry 0.113 0.8432-Nitrophenol 1 02/06/24 22:26 V43256TJW
<0.149 mg/Kg - dry 0.149 0.8434-Nitrophenol 1 02/06/24 22:26 V43256TJW
<0.336 mg/Kg - dry 0.336 0.843N-Nitrosodimethylamine 1 02/06/24 22:26 V43256TJW
<0.231 mg/Kg - dry 0.231 0.843N-Nitrosodiphenylamine 1 02/06/24 22:26 V43256TJW
<0.150 mg/Kg - dry 0.150 0.843N-Nitroso-di-n-propylamine 1 02/06/24 22:26 V43256TJW
<0.443 mg/Kg - dry 0.443 1.28Pentachlorophenol 1 02/06/24 22:26 V43256TJW
11.2 mg/Kg - dry 2.66 8.44Phenanthrene 10 02/07/24 14:23 V43256TJW
<0.143 mg/Kg - dry 0.143 0.843Phenol 1 02/06/24 22:26 V43256TJW
<0.171 mg/Kg - dry 0.171 0.843Pyrene 1 02/06/24 22:26 V43256TJW
<0.101 mg/Kg - dry 0.101 0.421Pyridine 1 02/06/24 22:26 V43256TJW
<0.136 mg/Kg - dry 0.136 0.8431,2,4-Trichlorobenzene 1 02/06/24 22:26 V43256TJW
<0.123 mg/Kg - dry 0.123 0.8432,4,5-Trichlorophenol 1 02/06/24 22:26 V43256TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 79 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B4 (12)
95687 Matrix:
1/26/2024 11:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V43183 02/05/24 09:50
<0.123 mg/Kg - dry 0.123 0.8432,4,6-Trichlorophenol 1 02/06/24 22:26 V43256TJW
8270ESurrogate: Phenol-d5 83.8 Limits: 34-121%02/06/24 22:261 TJW
Surrogate: 2-Fluorobiphenyl 96.4 Limits: 44-115%02/06/24 22:261 TJW V43256
Surrogate: 2-Fluorophenol 85.6 Limits: 35-115%02/06/24 22:261 TJW V43256
Surrogate: Nitrobenzene-d5 122 Limits: 37-122%02/06/24 22:261 TJW V43256
Surrogate: 4-Terphenyl-d14 88.0 Limits: 54-127%02/06/24 22:261 TJW V43256
Surrogate: 2,4,6-Tribromophenol 120 Limits: 39-132%02/06/24 22:261 TJW V43256
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 80 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28112
24-031-0014
00358
Harmon Environmental, PA
615 Bruce Thomas Rd.
Rick Harmon
Monroe
Received : 01/31/2024
Souther States
Report Date : 02/09/2024
Sample ID :
Lab No :
Sampled:B4 (12)
95687 Matrix:
1/26/2024 11:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V43116 02/02/24 09:50
4410 mg/Kg - dry 234 1270Aliphatic C9-C18 20 02/08/24 12:58 V43311NDL
792 J mg/Kg - dry 311 1270Aliphatic C19-C36 20 02/08/24 12:58 V43311NDL
3620 mg/Kg - dry 362 1270Aromatic C11-C22 20 02/08/24 12:58 V43311NDL
MADEP-EPHSurrogate: 2-Bromonaphthalene 144 *Limits: 40-140%02/08/24 12:5820 NDL
MADEP-EPHSurrogate: Chlorooctadecane 68.6 Limits: 40-140%02/08/24 12:5820 NDL
MADEP-EPHSurrogate: OTP Surrogate 111 Limits: 40-140%02/08/24 12:5820 NDL
Surrogate: 2-Fluorobiphenyl 89.9 Limits: 40-140%02/08/24 12:5820 NDL V43311
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V43048 01/31/24 08:00
75.3 mg/Kg - dry 7.77 51.2Aliphatic C5-C8 500 02/01/24 01:38 V43049TBL
324 mg/Kg - dry 29.2 51.2Aliphatic C9-C12 500 02/01/24 01:38 V43049TBL
217 mg/Kg - dry 3.99 51.2Aromatic C9-C10 500 02/01/24 01:38 V43049TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)105 Limits: 70-130%02/01/24 01:38500 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)106 Limits: 70-130%02/01/24 01:38500 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQLMinimum valueM
Page 81 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Metals Analysis
6010D
V43320QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V43106
Associated Lab Samples: 95680
LRB-V43106 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
02/08/24 05:080.0060.003<0.003mg/LLead
LCS-V43106Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
97.00.0970.100mg/LLead 80-120
V 95680-MS-V43106 V 95680-MSD-V43106Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.096 96.00.0980.1000.100< 0.003mg/LLead 98.0 75-125 2.0 20.0
V 95680-PDS-V43106Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
02/08/24 05:261020.256mg/LLead
Page 1 of 39Date:02/09/2024 08:26 AM
Page 82 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43078QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V43077
Associated Lab Samples: 95681, 95682, 95683, 95684, 95685, 95686
LRB-V43077 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/31/24 19:470.0200.002<0.002mg/KgAcetone
01/31/24 19:470.0200.001<0.001mg/KgAcrolein
01/31/24 19:470.0200.0008<0.0008mg/KgAcrylonitrile
01/31/24 19:470.0050.0006<0.0006mg/KgBenzene
01/31/24 19:470.0050.0005<0.0005mg/KgBromobenzene
01/31/24 19:470.0050.0008<0.0008mg/KgBromochloromethane
01/31/24 19:470.0050.001<0.001mg/KgBromodichloromethane
01/31/24 19:470.0050.001<0.001mg/KgBromoform
01/31/24 19:470.0100.001<0.001mg/KgBromomethane
01/31/24 19:470.0050.0005<0.0005mg/Kgn-Butylbenzene
01/31/24 19:470.0050.0006<0.0006mg/Kgsec-Butyl benzene
01/31/24 19:470.0050.0005<0.0005mg/Kgtert-Butyl benzene
01/31/24 19:470.0050.0006<0.0006mg/KgCarbon Disulfide
01/31/24 19:470.0050.001<0.001mg/KgCarbon Tetrachloride
01/31/24 19:470.0050.0007<0.0007mg/KgChlorobenzene
01/31/24 19:470.0050.0009<0.0009mg/KgChlorodibromomethane
01/31/24 19:470.0100.0009<0.0009mg/KgChloroethane
01/31/24 19:470.0050.001<0.001mg/KgChloroform
01/31/24 19:470.0100.0006<0.0006mg/KgChloromethane
01/31/24 19:470.0050.0005<0.0005mg/Kg2-Chlorotoluene
01/31/24 19:470.0050.0004<0.0004mg/Kg4-Chlorotoluene
01/31/24 19:470.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
01/31/24 19:470.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
01/31/24 19:470.0050.0006<0.0006mg/Kg1,2-Dibromoethane
01/31/24 19:470.0050.0006<0.0006mg/KgDibromomethane
01/31/24 19:470.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
01/31/24 19:470.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 2 of 39Date:02/09/2024 08:26 AM
Page 83 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43078QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V43077
Associated Lab Samples: 95681, 95682, 95683, 95684, 95685, 95686
LRB-V43077 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/31/24 19:470.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
01/31/24 19:470.0100.001<0.001mg/KgDichlorodifluoromethane
01/31/24 19:470.0050.0008<0.0008mg/Kg1,1-Dichloroethane
01/31/24 19:470.0050.001<0.001mg/Kg1,2-Dichloroethane
01/31/24 19:470.0050.0007<0.0007mg/Kg1,1-Dichloroethene
01/31/24 19:470.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
01/31/24 19:470.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
01/31/24 19:470.0050.0004<0.0004mg/Kg1,2-Dichloropropane
01/31/24 19:470.0050.0006<0.0006mg/Kg1,3-Dichloropropane
01/31/24 19:470.0050.001<0.001mg/Kg2,2-Dichloropropane
01/31/24 19:470.0050.0008<0.0008mg/Kg1,1-Dichloropropene
01/31/24 19:470.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
01/31/24 19:470.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
01/31/24 19:470.0050.0006<0.0006mg/KgEthylbenzene
01/31/24 19:470.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
01/31/24 19:470.0100.0008<0.0008mg/KgHexachlorobutadiene
01/31/24 19:470.0100.0007<0.0007mg/Kgn-Hexane
01/31/24 19:470.0200.0006<0.0006mg/Kg2-Hexanone
01/31/24 19:470.0050.0005<0.0005mg/KgIsopropylbenzene
01/31/24 19:470.0050.001<0.001mg/Kg4-Isopropyl toluene
01/31/24 19:470.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
01/31/24 19:470.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
01/31/24 19:470.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
01/31/24 19:470.0100.001<0.001mg/KgMethylene Chloride
01/31/24 19:470.0100.0010<0.0010mg/KgNaphthalene
01/31/24 19:470.0050.0005<0.0005mg/Kgn-Propylbenzene
01/31/24 19:470.0050.001<0.001mg/KgStyrene
Page 3 of 39Date:02/09/2024 08:26 AM
Page 84 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43078QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V43077
Associated Lab Samples: 95681, 95682, 95683, 95684, 95685, 95686
LRB-V43077 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/31/24 19:470.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
01/31/24 19:470.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
01/31/24 19:470.0050.0009<0.0009mg/KgTetrachloroethene
01/31/24 19:470.0050.0007<0.0007mg/KgToluene
01/31/24 19:470.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
01/31/24 19:470.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
01/31/24 19:470.0050.001<0.001mg/Kg1,1,1-Trichloroethane
01/31/24 19:470.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
01/31/24 19:470.0050.0009<0.0009mg/KgTrichloroethene
01/31/24 19:470.0100.002<0.002mg/KgTrichlorofluoromethane
01/31/24 19:470.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
01/31/24 19:470.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
01/31/24 19:470.0100.0005<0.0005mg/KgVinyl Acetate
01/31/24 19:470.0100.0005<0.0005mg/KgVinyl Chloride
01/31/24 19:470.0050.0005<0.0005mg/Kgo-Xylene
01/31/24 19:470.0100.001<0.001mg/Kgm,p-Xylene
01/31/24 19:474-Bromofluorobenzene (S)115 70-130
01/31/24 19:47Dibromofluoromethane (S)109 84-123
01/31/24 19:47Toluene-d8 (S)85.2 76-129
LCS-V43077 LCSD-V43077Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.113 1131090.1090.100mg/KgAcetone 29-198 3.6 20
0.130 130131*0.1310.100mg/KgAcrolein 70-130 0.7 20
0.120 1201210.1210.100mg/KgAcrylonitrile 65-134 0.8 20
Page 4 of 39* QC Fail Date:02/09/2024 08:26 AM
Page 85 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43078QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V43077
LCS-V43077 LCSD-V43077Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.051 1021090.0540.050mg/KgBenzene 74-127 7.0 20
0.053 1081100.0550.050mg/KgBromobenzene 73-125 2.5 20
0.057 1141190.0590.050mg/KgBromochloromethane 72-134 4.2 20
0.054 1081130.0560.050mg/KgBromodichloromethane 75-122 4.3 20
0.058 1181200.0600.050mg/KgBromoform 66-135 2.0 20
0.052 1041090.0540.050mg/KgBromomethane 20-180 4.4 20
0.055 1101190.0590.050mg/Kgn-Butylbenzene 65-135 8.0 20
0.050 1011110.0550.050mg/Kgsec-Butyl benzene 66-131 9.0 20
0.050 1011120.0560.050mg/Kgtert-Butyl benzene 67-132 10.1 20
0.052 1041180.0580.050mg/KgCarbon Disulfide 61-129 12.2 20
0.050 1021130.0560.050mg/KgCarbon Tetrachloride 64-143 10.6 20
0.053 1071130.0560.050mg/KgChlorobenzene 74-118 4.9 20
0.057 1141180.0590.050mg/KgChlorodibromomethane 73-122 3.2 20
0.051 1031160.0570.050mg/KgChloroethane 33-149 11.8 20
0.051 1041120.0560.050mg/KgChloroform 73-127 7.7 20
0.051 1041190.0590.050mg/KgChloromethane 45-143 13.8 20
0.050 1021090.0540.050mg/Kg2-Chlorotoluene 67-124 6.6 20
0.050 1021090.0540.050mg/Kg4-Chlorotoluene 71-126 6.6 20
0.053 1071110.0550.050mg/KgDi-Isopropyl Ether (DIPE)59-159 4.0 20
0.056 1131150.0570.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 1.4 20
0.059 1181190.0590.050mg/Kg1,2-Dibromoethane 70-132 1.0 20
0.056 1141170.0580.050mg/KgDibromomethane 74-133 2.4 20
0.054 1101150.0570.050mg/Kg1,2-Dichlorobenzene 72-123 4.4 20
0.053 1061100.0550.050mg/Kg1,3-Dichlorobenzene 71-120 4.0 20
0.052 1041080.0540.050mg/Kg1,4-Dichlorobenzene 71-123 3.7 20
0.060 1201330.0660.050mg/KgDichlorodifluoromethane 26-146 10.1 20
Page 5 of 39Date:02/09/2024 08:26 AM
Page 86 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43078QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V43077
LCS-V43077 LCSD-V43077Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.051 1031120.0550.050mg/Kg1,1-Dichloroethane 74-127 8.0 20
0.054 1081130.0560.050mg/Kg1,2-Dichloroethane 68-128 3.9 20
0.050 1021160.0570.050mg/Kg1,1-Dichloroethene 67-149 12.6 20
0.051 1041110.0550.050mg/Kgcis-1,2-Dichloroethene 76-134 7.0 20
0.051 1041140.0570.050mg/Kgtrans-1,2-Dichloroethene 73-132 9.7 20
0.053 1081130.0560.050mg/Kg1,2-Dichloropropane 73-130 4.8 20
0.056 1131190.0590.050mg/Kg1,3-Dichloropropane 75-124 4.4 20
0.051 1021130.0560.050mg/Kg2,2-Dichloropropane 50-142 9.8 20
0.050 1001130.0560.050mg/Kg1,1-Dichloropropene 71-130 11.6 20
0.056 1131170.0580.050mg/Kgcis-1,3-Dichloropropene 71-125 3.6 20
0.058 1181230.0610.050mg/Kgtrans-1,3-Dichloropropene 68-123 4.1 20
0.051 1031100.0550.050mg/KgEthylbenzene 74-128 7.1 20
0.108 1081110.1110.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 2.7 20
0.053 1061190.0590.050mg/KgHexachlorobutadiene 64-125 11.7 20
0.054 1081210.0600.050mg/Kgn-Hexane 70-130 11.1 20
0.052 1051030.0510.050mg/Kg2-Hexanone 61-157 2.6 20
0.050 1021110.0550.050mg/KgIsopropylbenzene 68-126 8.4 20
0.051 1041130.0560.050mg/Kg4-Isopropyl toluene 68-129 8.6 20
0.043 86.484.80.0420.050mg/KgMethyl Ethyl Ketone (MEK)63-149 1.8 20
0.055 1111130.0560.050mg/KgMethyl tert-butyl ether (MTBE)70-130 1.6 20
0.055 1111090.0540.050mg/Kg4-Methyl-2-Pentanone 57-162 1.6 20
0.050 1001060.0520.050mg/KgMethylene Chloride 74-129 5.0 20
0.058 1181230.0610.050mg/KgNaphthalene 57-157 4.3 20
0.051 1021100.0550.050mg/Kgn-Propylbenzene 67-130 7.5 20
0.056 1121160.0580.050mg/KgStyrene 77-121 3.5 20
0.054 1081150.0570.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 5.9 20
Page 6 of 39Date:02/09/2024 08:26 AM
Page 87 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43078QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V43077
LCS-V43077 LCSD-V43077Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.055 1121110.0550.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 0.7 20
0.050 1011110.0550.050mg/KgTetrachloroethene 68-130 9.2 20
0.051 1021090.0540.050mg/KgToluene 71-129 6.6 20
0.056 1141260.0620.050mg/Kg1,2,3-Trichlorobenzene 68-130 9.8 20
0.057 1141250.0620.050mg/Kg1,2,4-Trichlorobenzene 66-125 8.5 20
0.051 1021140.0560.050mg/Kg1,1,1-Trichloroethane 67-131 10.5 20
0.057 1151200.0590.050mg/Kg1,1,2-Trichloroethane 70-133 4.2 20
0.052 1051130.0560.050mg/KgTrichloroethene 75-133 7.8 20
0.048 97.61100.0540.050mg/KgTrichlorofluoromethane 44-146 11.5 20
0.058 1171180.0580.050mg/Kg1,2,3-Trichloropropane 60-137 0.8 20
0.051 1021110.0550.050mg/Kg1,3,5-Trimethylbenzene 69-128 8.8 20
0.059 1181130.0560.050mg/KgVinyl Acetate 60-140 4.6 20
0.053 1081190.0590.050mg/KgVinyl Chloride 48-147 10.3 20
0.053 1061140.0560.050mg/Kgo-Xylene 74-126 6.9 20
0.105 1051130.1130.100mg/Kgm,p-Xylene 75-124 7.3 20
98.693.04-Bromofluorobenzene (S)70-130
114111Dibromofluoromethane (S)84-123
90.287.8Toluene-d8 (S)76-129
Page 7 of 39Date:02/09/2024 08:26 AM
Page 88 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43081QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V43079
Associated Lab Samples: 95687
LRB-V43079 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/31/24 19:470.0200.002<0.002mg/KgAcetone
01/31/24 19:470.0200.001<0.001mg/KgAcrolein
01/31/24 19:470.0200.0008<0.0008mg/KgAcrylonitrile
01/31/24 19:470.0050.0006<0.0006mg/KgBenzene
01/31/24 19:470.0050.0005<0.0005mg/KgBromobenzene
01/31/24 19:470.0050.0008<0.0008mg/KgBromochloromethane
01/31/24 19:470.0050.001<0.001mg/KgBromodichloromethane
01/31/24 19:470.0050.001<0.001mg/KgBromoform
01/31/24 19:470.0100.001<0.001mg/KgBromomethane
01/31/24 19:470.0050.0005<0.0005mg/Kgn-Butylbenzene
01/31/24 19:470.0050.0006<0.0006mg/Kgsec-Butyl benzene
01/31/24 19:470.0050.0005<0.0005mg/Kgtert-Butyl benzene
01/31/24 19:470.0050.0006<0.0006mg/KgCarbon Disulfide
01/31/24 19:470.0050.001<0.001mg/KgCarbon Tetrachloride
01/31/24 19:470.0050.0007<0.0007mg/KgChlorobenzene
01/31/24 19:470.0050.0009<0.0009mg/KgChlorodibromomethane
01/31/24 19:470.0100.0009<0.0009mg/KgChloroethane
01/31/24 19:470.0050.001<0.001mg/KgChloroform
01/31/24 19:470.0100.0006<0.0006mg/KgChloromethane
01/31/24 19:470.0050.0005<0.0005mg/Kg2-Chlorotoluene
01/31/24 19:470.0050.0004<0.0004mg/Kg4-Chlorotoluene
01/31/24 19:470.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
01/31/24 19:470.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
01/31/24 19:470.0050.0006<0.0006mg/Kg1,2-Dibromoethane
01/31/24 19:470.0050.0010<0.0010mg/KgDibromomethane
01/31/24 19:470.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
01/31/24 19:470.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 8 of 39Date:02/09/2024 08:26 AM
Page 89 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43081QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V43079
Associated Lab Samples: 95687
LRB-V43079 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/31/24 19:470.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
01/31/24 19:470.0100.001<0.001mg/KgDichlorodifluoromethane
01/31/24 19:470.0050.0008<0.0008mg/Kg1,1-Dichloroethane
01/31/24 19:470.0050.001<0.001mg/Kg1,2-Dichloroethane
01/31/24 19:470.0050.0007<0.0007mg/Kg1,1-Dichloroethene
01/31/24 19:470.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
01/31/24 19:470.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
01/31/24 19:470.0050.0004<0.0004mg/Kg1,2-Dichloropropane
01/31/24 19:470.0050.0006<0.0006mg/Kg1,3-Dichloropropane
01/31/24 19:470.0050.001<0.001mg/Kg2,2-Dichloropropane
01/31/24 19:470.0050.0008<0.0008mg/Kg1,1-Dichloropropene
01/31/24 19:470.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
01/31/24 19:470.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
01/31/24 19:470.0050.0006<0.0006mg/KgEthylbenzene
01/31/24 19:470.1000.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
01/31/24 19:470.0100.0008<0.0008mg/KgHexachlorobutadiene
01/31/24 19:470.0100.0007<0.0007mg/Kgn-Hexane
01/31/24 19:470.0200.0006<0.0006mg/Kg2-Hexanone
01/31/24 19:470.0050.0005<0.0005mg/KgIsopropylbenzene
01/31/24 19:470.0050.001<0.001mg/Kg4-Isopropyl toluene
01/31/24 19:470.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
01/31/24 19:470.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
01/31/24 19:470.0050.001<0.001mg/KgMethylene Chloride
01/31/24 19:470.0100.0010<0.0010mg/KgNaphthalene
01/31/24 19:470.0050.0005<0.0005mg/Kgn-Propylbenzene
01/31/24 19:470.0050.001<0.001mg/KgStyrene
01/31/24 19:470.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
Page 9 of 39Date:02/09/2024 08:26 AM
Page 90 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43081QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V43079
Associated Lab Samples: 95687
LRB-V43079 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/31/24 19:470.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
01/31/24 19:470.0050.0009<0.0009mg/KgTetrachloroethene
01/31/24 19:470.0050.0007<0.0007mg/KgToluene
01/31/24 19:470.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
01/31/24 19:470.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
01/31/24 19:470.0050.001<0.001mg/Kg1,1,1-Trichloroethane
01/31/24 19:470.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
01/31/24 19:470.0050.0009<0.0009mg/KgTrichloroethene
01/31/24 19:470.0100.002<0.002mg/KgTrichlorofluoromethane
01/31/24 19:470.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
01/31/24 19:470.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
01/31/24 19:470.0100.0005<0.0005mg/KgVinyl Acetate
01/31/24 19:470.0100.0005<0.0005mg/KgVinyl Chloride
01/31/24 19:470.0050.0005<0.0005mg/Kgo-Xylene
01/31/24 19:470.0100.001<0.001mg/Kgm,p-Xylene
01/31/24 19:474-Bromofluorobenzene (S)115 70-130
01/31/24 19:47Dibromofluoromethane (S)109 70-130
01/31/24 19:47Toluene-d8 (S)85.2 76-129
LCS-V43079 LCSD-V43079Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.113 1131090.1090.100mg/KgAcetone 29-198 3.6 20
0.130 130131*0.1310.100mg/KgAcrolein 70-130 0.7 20
0.120 1201210.1210.100mg/KgAcrylonitrile 65-134 0.8 20
0.051 1021090.0540.050mg/KgBenzene 74-127 7.0 20
Page 10 of 39* QC Fail Date:02/09/2024 08:26 AM
Page 91 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43081QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V43079
LCS-V43079 LCSD-V43079Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.053 1081100.0550.050mg/KgBromobenzene 73-125 2.5 20
0.057 1141190.0590.050mg/KgBromochloromethane 72-134 4.2 20
0.054 1081130.0560.050mg/KgBromodichloromethane 75-122 4.3 20
0.058 1181200.0600.050mg/KgBromoform 66-135 2.0 20
0.052 1041090.0540.050mg/KgBromomethane 20-180 4.4 20
0.055 1101190.0590.050mg/Kgn-Butylbenzene 65-135 8.0 20
0.050 1011110.0550.050mg/Kgsec-Butyl benzene 66-131 9.0 20
0.050 1011120.0560.050mg/Kgtert-Butyl benzene 67-132 10.1 20
0.052 1041180.0580.050mg/KgCarbon Disulfide 61-129 12.2 20
0.050 1021130.0560.050mg/KgCarbon Tetrachloride 64-143 10.6 20
0.053 1071130.0560.050mg/KgChlorobenzene 74-118 4.9 20
0.057 1141180.0590.050mg/KgChlorodibromomethane 73-122 3.2 20
0.051 1031160.0570.050mg/KgChloroethane 33-149 11.8 20
0.051 1041120.0560.050mg/KgChloroform 73-127 7.7 20
0.051 1041190.0590.050mg/KgChloromethane 45-143 13.8 20
0.050 1021090.0540.050mg/Kg2-Chlorotoluene 67-124 6.6 20
0.050 1021090.0540.050mg/Kg4-Chlorotoluene 71-126 6.6 20
0.053 1071110.0550.050mg/KgDi-Isopropyl Ether (DIPE)59-159 4.0 20
0.056 1131150.0570.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 1.4 20
0.059 1181190.0590.050mg/Kg1,2-Dibromoethane 70-132 1.0 20
0.056 1141170.0580.050mg/KgDibromomethane 74-133 2.4 20
0.054 1101150.0570.050mg/Kg1,2-Dichlorobenzene 72-123 4.4 20
0.053 1061100.0550.050mg/Kg1,3-Dichlorobenzene 71-120 4.0 20
0.052 1041080.0540.050mg/Kg1,4-Dichlorobenzene 71-123 3.7 20
0.060 1201330.0660.050mg/KgDichlorodifluoromethane 26-146 10.1 20
0.051 1031120.0550.050mg/Kg1,1-Dichloroethane 74-127 8.0 20
Page 11 of 39Date:02/09/2024 08:26 AM
Page 92 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43081QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V43079
LCS-V43079 LCSD-V43079Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.054 1081130.0560.050mg/Kg1,2-Dichloroethane 68-128 3.9 20
0.050 1021160.0570.050mg/Kg1,1-Dichloroethene 67-149 12.6 20
0.051 1041110.0550.050mg/Kgcis-1,2-Dichloroethene 76-134 7.0 20
0.051 1041140.0570.050mg/Kgtrans-1,2-Dichloroethene 73-132 9.7 20
0.053 1081130.0560.050mg/Kg1,2-Dichloropropane 73-130 4.8 20
0.056 1131190.0590.050mg/Kg1,3-Dichloropropane 75-124 4.4 20
0.051 1021130.0560.050mg/Kg2,2-Dichloropropane 50-142 9.8 20
0.050 1001130.0560.050mg/Kg1,1-Dichloropropene 71-130 11.6 20
0.056 1131170.0580.050mg/Kgcis-1,3-Dichloropropene 71-125 3.6 20
0.058 1181230.0610.050mg/Kgtrans-1,3-Dichloropropene 68-123 4.1 20
0.051 1031100.0550.050mg/KgEthylbenzene 74-128 7.1 20
0.108 1081110.1110.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 2.7 20
0.053 1061190.0590.050mg/KgHexachlorobutadiene 64-125 11.7 20
0.054 1081210.0600.050mg/Kgn-Hexane 70-130 11.1 20
0.052 1051030.0510.050mg/Kg2-Hexanone 61-157 2.6 20
0.050 1021110.0550.050mg/KgIsopropylbenzene 68-126 8.4 20
0.051 1041130.0560.050mg/Kg4-Isopropyl toluene 68-129 8.6 20
0.043 86.484.80.0420.050mg/KgMethyl Ethyl Ketone (MEK)63-149 1.8 20
0.055 1111130.0560.050mg/KgMethyl tert-butyl ether (MTBE)70-130 1.6 20
0.050 1001060.0520.050mg/KgMethylene Chloride 74-129 5.0 20
0.058 1181230.0610.050mg/KgNaphthalene 57-157 4.3 20
0.051 1021100.0550.050mg/Kgn-Propylbenzene 67-130 7.5 20
0.056 1121160.0580.050mg/KgStyrene 77-121 3.5 20
0.054 1081150.0570.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 5.9 20
0.055 1121110.0550.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 0.7 20
0.050 1011110.0550.050mg/KgTetrachloroethene 68-130 9.2 20
Page 12 of 39Date:02/09/2024 08:26 AM
Page 93 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43081QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V43079
LCS-V43079 LCSD-V43079Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.051 1021090.0540.050mg/KgToluene 71-129 6.6 20
0.056 1141260.0620.050mg/Kg1,2,3-Trichlorobenzene 68-130 9.8 20
0.057 1141250.0620.050mg/Kg1,2,4-Trichlorobenzene 66-125 8.5 20
0.051 1021140.0560.050mg/Kg1,1,1-Trichloroethane 67-131 10.5 20
0.057 1151200.0590.050mg/Kg1,1,2-Trichloroethane 70-133 4.2 20
0.052 1051130.0560.050mg/KgTrichloroethene 75-133 7.8 20
0.048 97.61100.0540.050mg/KgTrichlorofluoromethane 44-146 11.5 20
0.058 1171180.0580.050mg/Kg1,2,3-Trichloropropane 60-137 0.8 20
0.051 1021110.0550.050mg/Kg1,3,5-Trimethylbenzene 69-128 8.8 20
0.059 1181130.0560.050mg/KgVinyl Acetate 60-140 4.6 20
0.053 1081190.0590.050mg/KgVinyl Chloride 48-147 10.3 20
0.053 1061140.0560.050mg/Kgo-Xylene 74-126 6.9 20
0.105 1051130.1130.100mg/Kgm,p-Xylene 75-124 7.3 20
98.693.04-Bromofluorobenzene (S)70-130
114111Dibromofluoromethane (S)70-130
90.287.8Toluene-d8 (S)76-129
Page 13 of 39Date:02/09/2024 08:26 AM
Page 94 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43359QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V43357
Associated Lab Samples: 95680
LRB-V43357 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/07/24 23:305.001.80<1.80µg/LAcetone
02/07/24 23:305.002.00<2.00µg/LAcrolein
02/07/24 23:305.000.230<0.230µg/LAcrylonitrile
02/07/24 23:300.5000.180<0.180µg/LBenzene
02/07/24 23:300.5000.210<0.210µg/LBromobenzene
02/07/24 23:301.000.420<0.420µg/LBromochloromethane
02/07/24 23:300.5000.160<0.160µg/LBromodichloromethane
02/07/24 23:305.001.50<1.50µg/LBromoform
02/07/24 23:301.000.280<0.280µg/LBromomethane
02/07/24 23:301.000.185<0.185µg/Ln-Butylbenzene
02/07/24 23:300.5000.200<0.200µg/Lsec-Butyl benzene
02/07/24 23:302.000.920<0.920µg/Ltert-Butyl benzene
02/07/24 23:305.000.150<0.150µg/LCarbon Disulfide
02/07/24 23:300.5000.180<0.180µg/LCarbon Tetrachloride
02/07/24 23:300.5000.190<0.190µg/LChlorobenzene
02/07/24 23:300.5000.190<0.190µg/LChlorodibromomethane
02/07/24 23:301.000.430<0.430µg/LChloroethane
02/07/24 23:300.5000.220<0.220µg/LChloroform
02/07/24 23:300.5000.220<0.220µg/LChloromethane
02/07/24 23:300.5000.200<0.200µg/L2-Chlorotoluene
02/07/24 23:300.5000.200<0.200µg/L4-Chlorotoluene
02/07/24 23:305.000.960<0.960µg/LDi-Isopropyl Ether (DIPE)
02/07/24 23:302.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
02/07/24 23:300.5000.200<0.200µg/L1,2-Dibromoethane
02/07/24 23:300.5000.230<0.230µg/LDibromomethane
02/07/24 23:300.5000.220<0.220µg/L1,2-Dichlorobenzene
02/07/24 23:300.5000.190<0.190µg/L1,3-Dichlorobenzene
Page 14 of 39Date:02/09/2024 08:26 AM
Page 95 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43359QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V43357
Associated Lab Samples: 95680
LRB-V43357 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/07/24 23:300.5000.210<0.210µg/L1,4-Dichlorobenzene
02/07/24 23:305.001.20<1.20µg/LDichlorodifluoromethane
02/07/24 23:300.5000.240<0.240µg/L1,1-Dichloroethane
02/07/24 23:300.5000.150<0.150µg/L1,2-Dichloroethane
02/07/24 23:300.5000.150<0.150µg/L1,1-Dichloroethene
02/07/24 23:300.5000.200<0.200µg/Lcis-1,2-Dichloroethene
02/07/24 23:300.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
02/07/24 23:300.5000.190<0.190µg/L1,2-Dichloropropane
02/07/24 23:300.5000.130<0.130µg/L1,3-Dichloropropane
02/07/24 23:302.000.210<0.210µg/L2,2-Dichloropropane
02/07/24 23:300.5000.200<0.200µg/L1,1-Dichloropropene
02/07/24 23:300.5000.210<0.210µg/Lcis-1,3-Dichloropropene
02/07/24 23:300.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
02/07/24 23:300.5000.170<0.170µg/LEthylbenzene
02/07/24 23:3010.01.80<1.80µg/LEthyl Tertiary Butyl Ether (ETBE)
02/07/24 23:302.000.350<0.350µg/LHexachlorobutadiene
02/07/24 23:3010.01.30<1.30µg/Ln-Hexane
02/07/24 23:305.000.380<0.380µg/L2-Hexanone
02/07/24 23:305.000.180<0.180µg/LIsopropylbenzene
02/07/24 23:300.5000.089<0.089µg/L4-Isopropyl toluene
02/07/24 23:305.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
02/07/24 23:300.5000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
02/07/24 23:305.001.00<1.00µg/L4-Methyl-2-Pentanone
02/07/24 23:301.000.330<0.330µg/LMethylene Chloride
02/07/24 23:301.000.470<0.470µg/LNaphthalene
02/07/24 23:300.5000.190<0.190µg/Ln-Propylbenzene
02/07/24 23:300.5000.220<0.220µg/LStyrene
Page 15 of 39Date:02/09/2024 08:26 AM
Page 96 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43359QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V43357
Associated Lab Samples: 95680
LRB-V43357 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/07/24 23:300.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
02/07/24 23:300.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
02/07/24 23:300.5000.220<0.220µg/LTetrachloroethene
02/07/24 23:300.5000.220<0.220µg/LToluene
02/07/24 23:302.000.380<0.380µg/L1,2,3-Trichlorobenzene
02/07/24 23:301.000.310<0.310µg/L1,2,4-Trichlorobenzene
02/07/24 23:300.5000.160<0.160µg/L1,1,1-Trichloroethane
02/07/24 23:300.5000.096<0.096µg/L1,1,2-Trichloroethane
02/07/24 23:300.5000.180<0.180µg/LTrichloroethene
02/07/24 23:300.5000.180<0.180µg/LTrichlorofluoromethane
02/07/24 23:301.000.270<0.270µg/L1,2,3-Trichloropropane
02/07/24 23:300.5000.180<0.180µg/L1,3,5-Trimethylbenzene
02/07/24 23:302.001.00<1.00µg/LVinyl Acetate
02/07/24 23:300.5000.170<0.170µg/LVinyl Chloride
02/07/24 23:300.5000.210<0.210µg/Lo-Xylene
02/07/24 23:301.000.420<0.420µg/Lm,p-Xylene
02/07/24 23:304-Bromofluorobenzene (S)101 80-124
02/07/24 23:30Dibromofluoromethane (S)98.0 75-129
02/07/24 23:301,2-Dichloroethane - d4 (S)101 63-136
02/07/24 23:30Toluene-d8 (S)99.8 77-123
LCS-V43357 LCSD-V43357Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
39.5 98.798.539.440.0µg/LAcetone 40-166 0.2 20.0
41.0 10310542.040.0µg/LAcrolein 70-130 2.4 20.0
Page 16 of 39Date:02/09/2024 08:26 AM
Page 97 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43359QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V43357
LCS-V43357 LCSD-V43357Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
42.0 10511043.940.0µg/LAcrylonitrile 81-127 4.4 20.0
20.9 10510520.920.0µg/LBenzene 77-128 0.0 20.0
21.9 11010420.720.0µg/LBromobenzene 78-129 5.6 20.0
21.4 10710420.720.0µg/LBromochloromethane 78-135 3.3 20.0
20.5 10310220.320.0µg/LBromodichloromethane 76-138 0.9 20.0
20.3 10298.019.620.0µg/LBromoform 71-135 3.5 20.0
22.0 11011923.720.0µg/LBromomethane 41-168 7.4 20.0
21.3 10710420.720.0µg/Ln-Butylbenzene 68-134 2.8 20.0
21.9 11010521.020.0µg/Lsec-Butyl benzene 71-131 4.1 20.0
22.0 11010520.920.0µg/Ltert-Butyl benzene 70-132 5.1 20.0
22.2 11111022.020.0µg/LCarbon Disulfide 59-135 0.9 20.0
20.6 10310120.220.0µg/LCarbon Tetrachloride 72-142 1.9 20.0
21.5 10810520.920.0µg/LChlorobenzene 78-119 2.8 20.0
21.3 10710520.920.0µg/LChlorodibromomethane 75-134 1.8 20.0
25.1 12612725.320.0µg/LChloroethane 57-142 0.7 20.0
21.1 10610320.520.0µg/LChloroform 77-130 2.8 20.0
21.4 10711222.320.0µg/LChloromethane 47-145 4.1 20.0
22.1 11110521.020.0µg/L2-Chlorotoluene 74-126 5.1 20.0
21.8 10910320.620.0µg/L4-Chlorotoluene 78-129 5.6 20.0
21.8 10910821.520.0µg/LDi-Isopropyl Ether (DIPE)60-154 1.3 20.0
22.3 11211222.320.0µg/L1,2-Dibromo-3-Chloropropane 63-134 0.0 20.0
20.9 10510320.620.0µg/L1,2-Dibromoethane 77-135 1.4 20.0
21.2 10610520.920.0µg/LDibromomethane 76-138 1.4 20.0
22.1 11110621.120.0µg/L1,2-Dichlorobenzene 78-128 4.6 20.0
21.8 10910420.820.0µg/L1,3-Dichlorobenzene 77-125 4.6 20.0
21.8 10910320.620.0µg/L1,4-Dichlorobenzene 75-126 5.6 20.0
Page 17 of 39Date:02/09/2024 08:26 AM
Page 98 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43359QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V43357
LCS-V43357 LCSD-V43357Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
24.2 12112725.420.0µg/LDichlorodifluoromethane 28-163 4.8 20.0
21.0 10510320.520.0µg/L1,1-Dichloroethane 70-130 2.4 20.0
20.2 10110120.220.0µg/L1,2-Dichloroethane 68-131 0.0 20.0
21.3 10710520.920.0µg/L1,1-Dichloroethene 70-154 1.8 20.0
19.8 99.099.019.820.0µg/Lcis-1,2-Dichloroethene 76-141 0.0 20.0
21.0 10510320.520.0µg/Ltrans-1,2-Dichloroethene 76-135 2.4 20.0
21.0 10510320.620.0µg/L1,2-Dichloropropane 77-130 1.9 20.0
21.1 10610420.720.0µg/L1,3-Dichloropropane 76-132 1.9 20.0
19.8 99.095.019.020.0µg/L2,2-Dichloropropane 29-149 4.1 20.0
21.9 11010621.220.0µg/L1,1-Dichloropropene 71-136 3.2 20.0
20.5 10310420.720.0µg/Lcis-1,3-Dichloropropene 65-140 0.9 20.0
20.0 10010120.120.0µg/Ltrans-1,3-Dichloropropene 67-140 0.4 20.0
21.0 10510320.620.0µg/LEthylbenzene 80-127 1.9 20.0
44.5 11111043.940.0µg/LEthyl Tertiary Butyl Ether (ETBE)70-130 1.3 20.0
21.8 10910320.520.0µg/LHexachlorobutadiene 61-134 6.1 20.0
20.2 10110320.620.0µg/Ln-Hexane 70-130 1.9 20.0
20.9 10510320.520.0µg/L2-Hexanone 64-137 1.9 20.0
22.0 11010520.920.0µg/LIsopropylbenzene 70-130 5.1 20.0
21.5 10810220.420.0µg/L4-Isopropyl toluene 69-132 5.2 20.0
19.5 97.598.019.620.0µg/LMethyl Ethyl Ketone (MEK)71-134 0.5 20.0
21.0 10510320.620.0µg/LMethyl tert-butyl ether (MTBE)68-135 1.9 20.0
21.6 10810721.420.0µg/L4-Methyl-2-Pentanone 69-134 0.9 20.0
21.0 10510521.020.0µg/LMethylene Chloride 73-131 0.0 20.0
21.6 10810821.520.0µg/LNaphthalene 64-136 0.4 20.0
22.0 11010520.920.0µg/Ln-Propylbenzene 72-132 5.1 20.0
20.9 10510320.620.0µg/LStyrene 78-129 1.4 20.0
Page 18 of 39Date:02/09/2024 08:26 AM
Page 99 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V43359QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V43357
LCS-V43357 LCSD-V43357Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.5 10810320.520.0µg/L1,1,1,2-Tetrachloroethane 79-134 4.7 20.0
21.6 10899.019.820.0µg/L1,1,2,2-Tetrachloroethane 62-127 8.6 20.0
20.9 10510420.720.0µg/LTetrachloroethene 80-129 0.9 20.0
20.9 10510521.020.0µg/LToluene 76-131 0.4 20.0
24.7 12412525.020.0µg/L1,2,3-Trichlorobenzene 58-144 1.2 20.0
23.2 11611322.620.0µg/L1,2,4-Trichlorobenzene 66-139 2.6 20.0
20.8 10410320.520.0µg/L1,1,1-Trichloroethane 75-135 1.4 20.0
20.8 10410320.620.0µg/L1,1,2-Trichloroethane 70-140 0.9 20.0
21.2 10610120.220.0µg/LTrichloroethene 77-133 4.8 20.0
22.1 11111022.020.0µg/LTrichlorofluoromethane 62-148 0.4 20.0
21.6 10810320.520.0µg/L1,2,3-Trichloropropane 71-127 5.2 20.0
21.4 10710120.220.0µg/L1,3,5-Trimethylbenzene 75-131 5.7 20.0
22.7 11411322.620.0µg/LVinyl Acetate 34-167 0.4 20.0
21.4 10710921.820.0µg/LVinyl Chloride 57-141 1.8 20.0
21.2 10610420.720.0µg/Lo-Xylene 78-128 2.3 20.0
44.6 11210943.740.0µg/Lm,p-Xylene 77-133 2.0 20.0
10198.84-Bromofluorobenzene (S)80-124
96.896.6Dibromofluoromethane (S)75-129
97.499.61,2-Dichloroethane - d4 (S)63-136
10299.6Toluene-d8 (S)77-123
Page 19 of 39Date:02/09/2024 08:26 AM
Page 100 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V43253QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V43104
Associated Lab Samples: 95680
LRB-V43104 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/06/24 16:252.000.302<0.302µg/LAcenaphthene
02/06/24 16:252.000.297<0.297µg/LAcenaphthylene
02/06/24 16:255.002.05<2.05µg/LAniline
02/06/24 16:252.000.836<0.836µg/LAnthracene
02/06/24 16:252.000.637<0.637µg/LBenzo(a)anthracene
02/06/24 16:252.001.02<1.02µg/LBenzo(a)pyrene
02/06/24 16:255.002.49<2.49µg/LBenzo(b)fluoranthene
02/06/24 16:255.001.01<1.01µg/LBenzo(g,h,i)perylene
02/06/24 16:255.001.99<1.99µg/LBenzo(k)fluoranthene
02/06/24 16:2510.01.10<1.10µg/LBenzoic Acid
02/06/24 16:255.000.684<0.684µg/LBenzyl alcohol
02/06/24 16:255.000.468<0.468µg/LBis(2-Chloroethoxy)methane
02/06/24 16:255.001.04<1.04µg/LBis(2-Chloroethyl)ether
02/06/24 16:255.001.08<1.08µg/LBis(2-Chloroisopropyl)ether
02/06/24 16:2510.03.46<3.46µg/LBis(2-ethylhexyl)phthalate
02/06/24 16:255.001.11<1.11µg/L4-Bromophenyl phenyl ether
02/06/24 16:255.001.83<1.83µg/LButyl benzyl phthalate
02/06/24 16:255.001.18<1.18µg/L4-Chloro-3-methylphenol
02/06/24 16:255.001.33<1.33µg/L4-Chloroaniline
02/06/24 16:2520.01.83<1.83µg/L2-Chloronaphthalene
02/06/24 16:2510.00.938<0.938µg/L2-Chlorophenol
02/06/24 16:255.001.71<1.71µg/L4-Chlorophenyl phenyl ether
02/06/24 16:252.000.405<0.405µg/LChrysene
02/06/24 16:252.000.434<0.434µg/LDibenz(a,h)anthracene
02/06/24 16:255.000.856<0.856µg/LDibenzofuran
02/06/24 16:255.002.00<2.00µg/L1,2-Dichlorobenzene
02/06/24 16:255.002.00<2.00µg/L1,3-Dichlorobenzene
Page 20 of 39Date:02/09/2024 08:26 AM
Page 101 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V43253QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V43104
Associated Lab Samples: 95680
LRB-V43104 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/06/24 16:255.002.05<2.05µg/L1,4-Dichlorobenzene
02/06/24 16:255.001.89<1.89µg/L3,3'-Dichlorobenzidine
02/06/24 16:2510.01.46<1.46µg/L2,4-Dichlorophenol
02/06/24 16:255.000.745<0.745µg/LDiethyl phthalate
02/06/24 16:255.000.939<0.939µg/LDimethyl phthalate
02/06/24 16:2520.01.57<1.57µg/L2,4-Dimethylphenol
02/06/24 16:255.002.06<2.06µg/LDi-n-butyl phthalate
02/06/24 16:2510.02.07<2.07µg/L4,6-Dinitro-2-methylphenol
02/06/24 16:2510.01.92<1.92µg/L2,4-Dinitrophenol
02/06/24 16:255.001.11<1.11µg/L2,4-Dinitrotoluene
02/06/24 16:255.000.809<0.809µg/L2,6-Dinitrotoluene
02/06/24 16:255.001.65<1.65µg/LDi-n-Octyl Phthalate
02/06/24 16:252.000.250<0.250µg/LFluoranthene
02/06/24 16:252.000.807<0.807µg/LFluorene
02/06/24 16:255.000.979<0.979µg/LHexachlorobenzene
02/06/24 16:255.002.73<2.73µg/LHexachlorobutadiene
02/06/24 16:255.002.05<2.05µg/LHexachlorocyclopentadiene
02/06/24 16:255.001.76<1.76µg/LHexachloroethane
02/06/24 16:252.000.477<0.477µg/LIndeno(1,2,3-cd)pyrene
02/06/24 16:255.000.444<0.444µg/LIsophorone
02/06/24 16:252.001.14<1.14µg/L1-Methylnaphthalene
02/06/24 16:252.000.666<0.666µg/L2-Methylnaphthalene
02/06/24 16:255.001.15<1.15µg/L2-Methylphenol
02/06/24 16:2510.00.880<0.880µg/L3&4 Methylphenol
02/06/24 16:252.000.728<0.728µg/LNaphthalene
02/06/24 16:255.001.39<1.39µg/L2-Nitroaniline
02/06/24 16:255.001.39<1.39µg/L3-Nitroaniline
Page 21 of 39Date:02/09/2024 08:26 AM
Page 102 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V43253QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V43104
Associated Lab Samples: 95680
LRB-V43104 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/06/24 16:255.001.53<1.53µg/L4-Nitroaniline
02/06/24 16:255.000.905<0.905µg/LNitrobenzene
02/06/24 16:255.000.493<0.493µg/L2-Nitrophenol
02/06/24 16:2510.01.23<1.23µg/L4-Nitrophenol
02/06/24 16:255.000.450<0.450µg/LN-Nitrosodimethylamine
02/06/24 16:255.001.10<1.10µg/LN-Nitrosodiphenylamine
02/06/24 16:255.000.641<0.641µg/LN-Nitroso-di-n-propylamine
02/06/24 16:255.001.43<1.43µg/LPentachlorophenol
02/06/24 16:252.000.428<0.428µg/LPhenanthrene
02/06/24 16:255.000.651<0.651µg/LPhenol
02/06/24 16:252.000.434<0.434µg/LPyrene
02/06/24 16:255.001.20<1.20µg/LPyridine
02/06/24 16:255.002.21<2.21µg/L1,2,4-Trichlorobenzene
02/06/24 16:255.001.31<1.31µg/L2,4,5-Trichlorophenol
02/06/24 16:255.001.32<1.32µg/L2,4,6-Trichlorophenol
02/06/24 16:252-Fluorobiphenyl (S)57.0 44-119
02/06/24 16:252-Fluorophenol (S)33.5 19-119
02/06/24 16:25Nitrobenzene-d5 (S)73.6 44-120
02/06/24 16:254-Terphenyl-d14 (S)75.2 50-134
02/06/24 16:252,4,6-Tribromophenol (S)72.2 43-140
02/06/24 16:25Phenol-d5 (S)24.9 11-100
LCS-V43104 LCSD-V43104Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
32.3 64.670.635.350.0µg/LAcenaphthene 38-117 8.8 20.0
Page 22 of 39Date:02/09/2024 08:26 AM
Page 103 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V43253QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V43104
LCS-V43104 LCSD-V43104Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
31.1 62.267.033.550.0µg/LAcenaphthylene 41-130 7.4 20.0
47.7 95.487.643.850.0µg/LAniline 12-197 8.5 20.0
39.6 79.283.641.850.0µg/LAnthracene 57-123 5.4 20.0
38.9 77.882.441.250.0µg/LBenzo(a)anthracene 58-125 5.7 20.0
42.9 85.888.644.350.0µg/LBenzo(a)pyrene 54-128 3.2 20.0
38.9 77.887.243.650.0µg/LBenzo(b)fluoranthene 53-131 11.3 20.0
32.6 65.270.035.050.0µg/LBenzo(g,h,i)perylene 50-134 7.1 20.0
37.4 74.884.642.350.0µg/LBenzo(k)fluoranthene 53-131 12.2 20.0
14.4 28.834.817.450.0µg/LBenzoic Acid 10-125 18.8 20.0
33.6 67.271.035.550.0µg/LBenzyl alcohol 31-112 5.4 20.0
30.8 61.661.430.750.0µg/LBis(2-Chloroethoxy)methane 48-120 0.3 20.0
29.3 58.661.830.950.0µg/LBis(2-Chloroethyl)ether 43-118 5.3 20.0
28.6 57.261.630.850.0µg/LBis(2-Chloroisopropyl)ether 37-130 7.4 20.0
40.2 80.485.242.650.0µg/LBis(2-ethylhexyl)phthalate 55-135 5.7 20.0
35.9 71.875.037.550.0µg/L4-Bromophenyl phenyl ether 55-124 4.3 20.0
39.6 79.285.442.750.0µg/LButyl benzyl phthalate 53-134 7.5 20.0
26.9 53.856.028.050.0µg/L4-Chloro-3-methylphenol 52-119 4.0 20.0
35.8 71.664.832.450.0µg/L4-Chloroaniline 33-117 9.9 20.0
28.5 57.061.030.550.0µg/L2-Chloronaphthalene 40-116 6.7 20.0
30.9 61.863.831.950.0µg/L2-Chlorophenol 38-117 3.1 20.0
34.0 68.073.436.750.0µg/L4-Chlorophenyl phenyl ether 53-121 7.6 20.0
41.9 83.884.642.350.0µg/LChrysene 59-123 0.9 20.0
46.5 93.067.233.650.0µg/LDibenz(a,h)anthracene 51-134 32.2*20.0
34.7 69.475.637.850.0µg/LDibenzofuran 53-118 8.5 20.0
22.9 45.848.824.450.0µg/L1,2-Dichlorobenzene 32-111 6.3 20.0
22.2 44.447.023.550.0µg/L1,3-Dichlorobenzene 28-110 5.6 20.0
Page 23 of 39* QC Fail Date:02/09/2024 08:26 AM
Page 104 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V43253QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V43104
LCS-V43104 LCSD-V43104Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.5 41.044.222.150.0µg/L1,4-Dichlorobenzene 29-112 7.5 20.0
33.5 67.072.236.150.0µg/L3,3'-Dichlorobenzidine 27-129 7.4 20.0
31.3 62.667.233.650.0µg/L2,4-Dichlorophenol 47-121 7.0 20.0
40.0 80.085.642.850.0µg/LDiethyl phthalate 56-125 6.7 20.0
38.5 77.084.242.150.0µg/LDimethyl phthalate 45-127 8.9 20.0
37.4 74.886.043.050.0µg/L2,4-Dimethylphenol 31-124 13.9 20.0
42.4 84.888.444.250.0µg/LDi-n-butyl phthalate 59-127 4.1 20.0
36.5 73.078.239.150.0µg/L4,6-Dinitro-2-methylphenol 44-137 6.8 20.0
37.5 75.079.639.850.0µg/L2,4-Dinitrophenol 23-143 5.9 20.0
43.8 87.692.046.050.0µg/L2,4-Dinitrotoluene 57-128 4.8 20.0
42.2 84.487.443.750.0µg/L2,6-Dinitrotoluene 57-124 3.4 20.0
43.2 86.493.646.850.0µg/LDi-n-Octyl Phthalate 51-140 8.0 20.0
40.2 80.483.841.950.0µg/LFluoranthene 57-128 4.1 20.0
37.2 74.480.240.150.0µg/LFluorene 52-124 7.5 20.0
39.4 78.885.242.650.0µg/LHexachlorobenzene 53-125 7.8 20.0
23.5 47.039.619.850.0µg/LHexachlorobutadiene 22-124 17.0 20.0
21.0 42.045.022.550.0µg/LHexachlorocyclopentadiene 32-117 6.8 20.0
21.3 42.646.423.250.0µg/LHexachloroethane 21-115 8.5 20.0
32.8 65.670.835.450.0µg/LIndeno(1,2,3-cd)pyrene 52-134 7.6 20.0
29.0 58.063.031.550.0µg/LIsophorone 42-124 8.2 20.0
19.7 39.4*41.420.750.0µg/L1-Methylnaphthalene 41-119 4.9 20.0
19.5 39.0*41.020.550.0µg/L2-Methylnaphthalene 40-121 5.0 20.0
30.2 60.465.832.950.0µg/L2-Methylphenol 30-117 8.5 20.0
26.0 52.056.028.050.0µg/L3&4 Methylphenol 29-110 7.4 20.0
22.3 44.647.823.950.0µg/LNaphthalene 40-121 6.9 20.0
38.7 77.482.641.350.0µg/L2-Nitroaniline 55-127 6.5 20.0
Page 24 of 39* QC Fail Date:02/09/2024 08:26 AM
Page 105 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V43253QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V43104
LCS-V43104 LCSD-V43104Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
38.7 77.482.641.350.0µg/L3-Nitroaniline 41-128 6.5 20.0
37.5 75.079.439.750.0µg/L4-Nitroaniline 45-135 5.6 20.0
27.4 54.861.630.850.0µg/LNitrobenzene 45-121 11.6 20.0
30.0 60.058.429.250.0µg/L2-Nitrophenol 47-123 2.7 20.0
15.7 31.434.617.350.0µg/L4-Nitrophenol 10-105 9.6 20.0
20.1 40.241.820.950.0µg/LN-Nitrosodimethylamine 10-119 3.9 20.0
43.9 87.896.448.250.0µg/LN-Nitrosodiphenylamine 51-123 9.3 20.0
37.7 75.480.440.250.0µg/LN-Nitroso-di-n-propylamine 49-119 6.4 20.0
50.1 10010854.050.0µg/LPentachlorophenol 35-138 7.4 20.0
39.8 79.684.042.050.0µg/LPhenanthrene 59-120 5.3 20.0
13.3 26.628.014.050.0µg/LPhenol 12-58 5.1 20.0
40.5 81.085.242.650.0µg/LPyrene 57-126 5.0 20.0
10.4 20.812.46.2250.0µg/LPyridine 10-80 50.3*20.0
22.0 44.044.422.250.0µg/L1,2,4-Trichlorobenzene 29-126 0.9 20.0
36.3 72.675.437.750.0µg/L2,4,5-Trichlorophenol 53-123 3.7 20.0
34.3 68.675.637.850.0µg/L2,4,6-Trichlorophenol 50-125 9.7 20.0
63.265.62-Fluorobiphenyl (S)44-119
32.241.42-Fluorophenol (S)19-119
56.263.4Nitrobenzene-d5 (S)44-120
78.683.64-Terphenyl-d14 (S)50-134
84.592.52,4,6-Tribromophenol (S)43-140
26.728.4Phenol-d5 (S)11-100
Page 25 of 39* QC Fail Date:02/09/2024 08:26 AM
Page 106 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V43256QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V43183
Associated Lab Samples: 95681, 95682, 95683, 95684, 95685, 95686, 95687
LRB-V43183 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/06/24 17:090.6600.116<0.116mg/KgAcenaphthene
02/06/24 17:090.6600.105<0.105mg/KgAcenaphthylene
02/06/24 17:090.6600.152<0.152mg/KgAniline
02/06/24 17:090.6600.143<0.143mg/KgAnthracene
02/06/24 17:090.6600.139<0.139mg/KgBenzo(a)anthracene
02/06/24 17:090.6600.147<0.147mg/KgBenzo(a)pyrene
02/06/24 17:090.6600.146<0.146mg/KgBenzo(b)fluoranthene
02/06/24 17:090.6600.136<0.136mg/KgBenzo(g,h,i)perylene
02/06/24 17:090.6600.137<0.137mg/KgBenzo(k)fluoranthene
02/06/24 17:092.000.580<0.580mg/KgBenzoic Acid
02/06/24 17:090.6600.105<0.105mg/KgBenzyl alcohol
02/06/24 17:090.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
02/06/24 17:090.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
02/06/24 17:090.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
02/06/24 17:090.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
02/06/24 17:090.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
02/06/24 17:090.3300.113<0.113mg/KgButyl benzyl phthalate
02/06/24 17:090.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
02/06/24 17:090.3300.112<0.112mg/Kg4-Chloroaniline
02/06/24 17:090.6600.116<0.116mg/Kg2-Chloronaphthalene
02/06/24 17:090.6600.098<0.098mg/Kg2-Chlorophenol
02/06/24 17:091.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
02/06/24 17:090.6600.142<0.142mg/KgChrysene
02/06/24 17:090.6600.230<0.230mg/KgDibenz(a,h)anthracene
02/06/24 17:090.6600.119<0.119mg/KgDibenzofuran
02/06/24 17:090.6600.094<0.094mg/Kg1,2-Dichlorobenzene
02/06/24 17:090.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 26 of 39Date:02/09/2024 08:26 AM
Page 107 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V43256QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V43183
Associated Lab Samples: 95681, 95682, 95683, 95684, 95685, 95686, 95687
LRB-V43183 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/06/24 17:090.3300.097<0.097mg/Kg1,4-Dichlorobenzene
02/06/24 17:090.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
02/06/24 17:090.6600.095<0.095mg/Kg2,4-Dichlorophenol
02/06/24 17:090.6600.180<0.180mg/KgDiethyl phthalate
02/06/24 17:090.6600.174<0.174mg/KgDimethyl phthalate
02/06/24 17:090.3300.108<0.108mg/Kg2,4-Dimethylphenol
02/06/24 17:090.6600.107<0.107mg/KgDi-n-butyl phthalate
02/06/24 17:091.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
02/06/24 17:091.500.520<0.520mg/Kg2,4-Dinitrophenol
02/06/24 17:090.6600.096<0.096mg/Kg2,4-Dinitrotoluene
02/06/24 17:090.6600.108<0.108mg/Kg2,6-Dinitrotoluene
02/06/24 17:090.3300.143<0.143mg/KgDi-n-Octyl Phthalate
02/06/24 17:090.6600.123<0.123mg/KgFluoranthene
02/06/24 17:090.6600.128<0.128mg/KgFluorene
02/06/24 17:090.6600.106<0.106mg/KgHexachlorobenzene
02/06/24 17:090.6600.097<0.097mg/KgHexachlorobutadiene
02/06/24 17:090.6600.157<0.157mg/KgHexachlorocyclopentadiene
02/06/24 17:090.6600.079<0.079mg/KgHexachloroethane
02/06/24 17:090.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
02/06/24 17:090.6600.191<0.191mg/KgIsophorone
02/06/24 17:090.6600.106<0.106mg/Kg1-Methylnaphthalene
02/06/24 17:090.6600.100<0.100mg/Kg2-Methylnaphthalene
02/06/24 17:090.6600.097<0.097mg/Kg2-Methylphenol
02/06/24 17:090.6600.084<0.084mg/Kg3&4 Methylphenol
02/06/24 17:090.6600.144<0.144mg/KgNaphthalene
02/06/24 17:090.6600.096<0.096mg/Kg2-Nitroaniline
02/06/24 17:090.6600.120<0.120mg/Kg3-Nitroaniline
Page 27 of 39Date:02/09/2024 08:26 AM
Page 108 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V43256QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V43183
Associated Lab Samples: 95681, 95682, 95683, 95684, 95685, 95686, 95687
LRB-V43183 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/06/24 17:090.3300.093<0.093mg/Kg4-Nitroaniline
02/06/24 17:090.3300.116<0.116mg/KgNitrobenzene
02/06/24 17:090.6600.088<0.088mg/Kg2-Nitrophenol
02/06/24 17:090.6600.117<0.117mg/Kg4-Nitrophenol
02/06/24 17:090.6600.263<0.263mg/KgN-Nitrosodimethylamine
02/06/24 17:090.6600.181<0.181mg/KgN-Nitrosodiphenylamine
02/06/24 17:090.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
02/06/24 17:091.000.347<0.347mg/KgPentachlorophenol
02/06/24 17:090.6600.208<0.208mg/KgPhenanthrene
02/06/24 17:090.6600.112<0.112mg/KgPhenol
02/06/24 17:090.6600.134<0.134mg/KgPyrene
02/06/24 17:090.3300.079<0.079mg/KgPyridine
02/06/24 17:090.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
02/06/24 17:090.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
02/06/24 17:090.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
02/06/24 17:092-Fluorobiphenyl (S)80.2 44-115
02/06/24 17:092-Fluorophenol (S)86.7 35-115
02/06/24 17:09Nitrobenzene-d5 (S)78.4 37-122
02/06/24 17:094-Terphenyl-d14 (S)80.8 54-127
02/06/24 17:092,4,6-Tribromophenol (S)73.8 39-132
02/06/24 17:09Phenol-d5 (S)83.4 34-121
LCS-V43183Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
74.81.251.67mg/KgAcenaphthene 40-123
74.21.241.67mg/KgAcenaphthylene 32-132
Page 28 of 39Date:02/09/2024 08:26 AM
Page 109 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V43256QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V43183
LCS-V43183Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1292.151.67mg/KgAniline 12-197
79.01.321.67mg/KgAnthracene 47-123
76.01.271.67mg/KgBenzo(a)anthracene 49-126
81.41.361.67mg/KgBenzo(a)pyrene 45-129
75.41.261.67mg/KgBenzo(b)fluoranthene 45-132
74.81.251.67mg/KgBenzo(g,h,i)perylene 43-134
72.41.211.67mg/KgBenzo(k)fluoranthene 47-132
46.30.7741.67mg/KgBenzoic Acid 10-83
80.21.341.67mg/KgBenzyl alcohol 29-122
64.61.081.67mg/KgBis(2-Chloroethoxy)methane 36-121
67.01.121.67mg/KgBis(2-Chloroethyl)ether 31-120
71.81.201.67mg/KgBis(2-Chloroisopropyl)ether 33-131
81.41.361.67mg/KgBis(2-ethylhexyl)phthalate 51-133
75.41.261.67mg/Kg4-Bromophenyl phenyl ether 46-124
81.41.361.67mg/KgButyl benzyl phthalate 48-132
66.41.111.67mg/Kg4-Chloro-3-methylphenol 45-122
62.81.051.67mg/Kg4-Chloroaniline 17-106
78.41.311.67mg/Kg2-Chloronaphthalene 41-114
76.61.281.67mg/Kg2-Chlorophenol 34-121
72.41.211.67mg/Kg4-Chlorophenyl phenyl ether 45-121
77.81.301.67mg/KgChrysene 50-124
62.81.051.67mg/KgDibenz(a,h)anthracene 45-134
77.21.291.67mg/KgDibenzofuran 44-120
71.21.191.67mg/Kg1,2-Dichlorobenzene 33-117
68.81.151.67mg/Kg1,3-Dichlorobenzene 30-115
65.81.101.67mg/Kg1,4-Dichlorobenzene 31-115
57.80.9661.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 29 of 39Date:02/09/2024 08:26 AM
Page 110 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V43256QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V43183
LCS-V43183Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
68.81.151.67mg/Kg2,4-Dichlorophenol 40-122
77.21.291.67mg/KgDiethyl phthalate 50-124
77.21.291.67mg/KgDimethyl phthalate 48-124
83.81.401.67mg/Kg2,4-Dimethylphenol 30-127
79.61.331.67mg/KgDi-n-butyl phthalate 51-128
68.81.151.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
60.41.011.67mg/Kg2,4-Dinitrophenol 27-129
85.01.421.67mg/Kg2,4-Dinitrotoluene 48-126
82.61.381.67mg/Kg2,6-Dinitrotoluene 46-124
76.01.271.67mg/KgDi-n-Octyl Phthalate 45-140
76.01.271.67mg/KgFluoranthene 50-127
77.21.291.67mg/KgFluorene 43-125
76.61.281.67mg/KgHexachlorobenzene 45-122
70.61.181.67mg/KgHexachlorobutadiene 32-123
55.80.9321.67mg/KgHexachlorocyclopentadiene 32-117
67.61.131.67mg/KgHexachloroethane 28-117
71.81.201.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
61.61.031.67mg/KgIsophorone 30-122
64.01.071.67mg/Kg1-Methylnaphthalene 40-119
66.41.111.67mg/Kg2-Methylnaphthalene 38-122
79.01.321.67mg/Kg2-Methylphenol 32-122
68.81.151.67mg/Kg3&4 Methylphenol 34-119
62.81.051.67mg/KgNaphthalene 35-123
78.41.311.67mg/Kg2-Nitroaniline 44-127
68.81.151.67mg/Kg3-Nitroaniline 33-119
78.41.311.67mg/Kg4-Nitroaniline 63-147
65.81.101.67mg/KgNitrobenzene 34-122
Page 30 of 39Date:02/09/2024 08:26 AM
Page 111 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V43256QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V43183
LCS-V43183Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
66.41.111.67mg/Kg2-Nitrophenol 36-123
63.41.061.67mg/Kg4-Nitrophenol 30-132
67.01.121.67mg/KgN-Nitrosodimethylamine 10-146
92.81.551.67mg/KgN-Nitrosodiphenylamine 38-127
74.81.251.67mg/KgN-Nitroso-di-n-propylamine 36-120
68.81.151.67mg/KgPentachlorophenol 25-133
76.01.271.67mg/KgPhenanthrene 50-121
75.41.261.67mg/KgPhenol 34-121
80.81.351.67mg/KgPyrene 47-127
47.70.7971.67mg/KgPyridine 10-80
64.61.081.67mg/Kg1,2,4-Trichlorobenzene 34-118
72.41.211.67mg/Kg2,4,5-Trichlorophenol 41-124
74.81.251.67mg/Kg2,4,6-Trichlorophenol 39-126
77.82-Fluorobiphenyl (S)44-115
83.72-Fluorophenol (S)35-115
65.8Nitrobenzene-d5 (S)37-122
78.44-Terphenyl-d14 (S)54-127
82.82,4,6-Tribromophenol (S)39-132
79.8Phenol-d5 (S)34-121
V 95681-MS-V43183 V 95681-MSD-V43183Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.32 79.51.361.671.66<0.116mg/KgAcenaphthene 81.4 40-123 2.9 20
1.31 78.91.351.671.66<0.105mg/KgAcenaphthylene 80.8 32-132 3.0 20
1.99 1202.031.671.66<0.152mg/KgAniline 122 12-197 1.9 20
Page 31 of 39Date:02/09/2024 08:26 AM
Page 112 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V43256QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V43183
V 95681-MS-V43183 V 95681-MSD-V43183Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.48 89.11.501.671.66<0.143mg/KgAnthracene 89.8 47-123 1.3 20
1.33 80.11.391.671.66<0.139mg/KgBenzo(a)anthracene 83.2 49-126 4.4 20
1.57 94.51.631.671.66<0.147mg/KgBenzo(a)pyrene 97.6 45-129 3.7 20
1.42 85.51.491.671.66<0.146mg/KgBenzo(b)fluoranthene 89.2 45-132 4.8 20
1.36 81.91.431.671.66<0.136mg/KgBenzo(g,h,i)perylene 85.6 43-134 5.0 20
1.44 86.71.521.671.66<0.137mg/KgBenzo(k)fluoranthene 91.0 47-132 5.4 20
1.47 88.5*1.511.671.66<0.580mg/KgBenzoic Acid 90.4*10-83 2.6 20
1.41 84.91.461.671.66<0.105mg/KgBenzyl alcohol 87.4 29-122 3.4 20
1.13 68.01.161.671.66<0.118mg/KgBis(2-Chloroethoxy)methane 69.4 36-121 2.6 20
1.17 70.41.191.671.66<0.107mg/KgBis(2-Chloroethyl)ether 71.2 31-120 1.6 20
1.24 74.61.261.671.66<0.136mg/KgBis(2-Chloroisopropyl)ether 75.4 33-131 1.6 20
1.45 87.31.521.671.66<0.120mg/KgBis(2-ethylhexyl)phthalate 91.0 51-133 4.7 20
1.35 81.31.351.671.66<0.109mg/Kg4-Bromophenyl phenyl ether 80.8 46-124 0.0 20
1.45 87.31.561.671.66<0.113mg/KgButyl benzyl phthalate 93.4 48-132 7.3 20
1.19 71.61.221.671.66<0.092mg/Kg4-Chloro-3-methylphenol 73.0 45-122 2.4 20
1.01 60.81.061.671.66<0.112mg/Kg4-Chloroaniline 63.4 17-106 4.8 20
1.38 83.11.391.671.66<0.116mg/Kg2-Chloronaphthalene 83.2 41-114 0.7 20
1.29 77.71.331.671.66<0.098mg/Kg2-Chlorophenol 79.6 34-121 3.0 20
1.26 75.91.291.671.66<0.126mg/Kg4-Chlorophenyl phenyl ether 77.2 45-121 2.3 20
1.39 83.71.471.671.66<0.142mg/KgChrysene 88.0 50-124 5.5 20
1.23 74.01.301.671.66<0.230mg/KgDibenz(a,h)anthracene 77.8 45-134 5.5 20
1.36 81.91.411.671.66<0.119mg/KgDibenzofuran 84.4 44-120 3.6 20
1.23 74.01.241.671.66<0.094mg/Kg1,2-Dichlorobenzene 74.2 33-117 0.8 20
1.22 73.41.231.671.66<0.097mg/Kg1,3-Dichlorobenzene 73.6 30-115 0.8 20
1.16 69.81.151.671.66<0.097mg/Kg1,4-Dichlorobenzene 68.8 31-115 0.8 20
0.804 48.40.8701.671.66<0.147mg/Kg3,3'-Dichlorobenzidine 52.0 22-121 7.8 20
Page 32 of 39* QC Fail Date:02/09/2024 08:26 AM
Page 113 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V43256QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V43183
V 95681-MS-V43183 V 95681-MSD-V43183Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.23 74.01.241.671.66<0.095mg/Kg2,4-Dichlorophenol 74.2 40-122 0.8 20
1.35 81.31.411.671.66<0.180mg/KgDiethyl phthalate 84.4 50-124 4.3 20
1.36 81.91.411.671.66<0.174mg/KgDimethyl phthalate 84.4 48-124 3.6 30
1.60 96.31.621.671.66<0.108mg/Kg2,4-Dimethylphenol 97.0 30-127 1.2 20
1.47 88.51.471.671.66<0.107mg/KgDi-n-butyl phthalate 88.0 51-128 0.0 20
1.30 78.31.321.671.66<0.240mg/Kg4,6-Dinitro-2-methylphenol 79.0 29-132 1.5 20
1.33 80.11.321.671.66<0.520mg/Kg2,4-Dinitrophenol 79.0 27-129 0.7 20
1.44 86.71.511.671.66<0.096mg/Kg2,4-Dinitrotoluene 90.4 48-126 4.7 20
1.45 87.31.521.671.66<0.108mg/Kg2,6-Dinitrotoluene 91.0 46-124 4.7 20
1.54 92.71.621.671.66<0.143mg/KgDi-n-Octyl Phthalate 97.0 45-140 5.0 20
1.38 83.11.421.671.66<0.123mg/KgFluoranthene 85.0 50-127 2.8 20
1.34 80.71.401.671.66<0.128mg/KgFluorene 83.8 43-125 4.3 20
1.38 83.11.411.671.66<0.106mg/KgHexachlorobenzene 84.4 45-122 2.1 20
1.23 74.01.251.671.66<0.097mg/KgHexachlorobutadiene 74.8 32-123 1.6 20
1.01 60.81.031.671.66<0.157mg/KgHexachlorocyclopentadiene 61.6 32-117 1.9 20
1.16 69.81.181.671.66<0.079mg/KgHexachloroethane 70.6 28-117 1.7 20
1.36 81.91.441.671.66<0.179mg/KgIndeno(1,2,3-cd)pyrene 86.2 45-133 5.7 20
1.05 63.21.081.671.66<0.191mg/KgIsophorone 64.6 30-122 2.8 20
1.15 69.21.181.671.66<0.106mg/Kg1-Methylnaphthalene 70.6 40-119 2.5 20
1.19 71.61.201.671.66<0.100mg/Kg2-Methylnaphthalene 71.8 38-122 0.8 20
1.35 81.31.391.671.66<0.097mg/Kg2-Methylphenol 83.2 32-122 2.9 20
1.17 70.41.181.671.66<0.084mg/Kg3&4 Methylphenol 70.6 34-119 0.8 20
1.13 68.01.151.671.66<0.144mg/KgNaphthalene 68.8 35-123 1.7 20
1.39 83.71.441.671.66<0.096mg/Kg2-Nitroaniline 86.2 44-127 3.5 20
1.17 70.41.241.671.66<0.120mg/Kg3-Nitroaniline 74.2 33-119 5.8 20
1.26 75.91.421.671.66<0.093mg/Kg4-Nitroaniline 85.0 63-147 11.9 20
Page 33 of 39Date:02/09/2024 08:26 AM
Page 114 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V43256QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V43183
V 95681-MS-V43183 V 95681-MSD-V43183Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.15 69.21.161.671.66<0.116mg/KgNitrobenzene 69.4 34-122 0.8 20
1.16 69.81.191.671.66<0.088mg/Kg2-Nitrophenol 71.2 32-123 2.5 20
1.19 71.61.261.671.66<0.117mg/Kg4-Nitrophenol 75.4 30-132 5.7 20
1.15 69.21.211.671.66<0.263mg/KgN-Nitrosodimethylamine 72.4 10-146 5.0 30
1.68 1011.701.671.66<0.181mg/KgN-Nitrosodiphenylamine 102 38-127 1.1 20
1.30 78.31.351.671.66<0.118mg/KgN-Nitroso-di-n-propylamine 80.8 36-120 3.7 20
1.49 89.71.481.671.66<0.347mg/KgPentachlorophenol 88.6 25-133 0.6 20
1.43 86.11.451.671.66<0.208mg/KgPhenanthrene 86.8 50-121 1.3 20
1.29 77.71.301.671.66<0.112mg/KgPhenol 77.8 34-121 0.7 20
1.40 84.31.501.671.66<0.134mg/KgPyrene 89.8 47-127 6.8 20
0.863 51.90.8951.671.66<0.079mg/KgPyridine 53.5 10-80 3.6 20
1.13 68.01.141.671.66<0.107mg/Kg1,2,4-Trichlorobenzene 68.2 34-118 0.8 20
1.31 78.91.371.671.66<0.096mg/Kg2,4,5-Trichlorophenol 82.0 41-124 4.4 20
1.31 78.91.351.671.66<0.096mg/Kg2,4,6-Trichlorophenol 80.8 39-126 3.0 20
83.12-Fluorobiphenyl (S)82.6 44-115
90.02-Fluorophenol (S)88.2 35-115
70.4Nitrobenzene-d5 (S)68.8 37-122
83.74-Terphenyl-d14 (S)84.4 54-127
86.72,4,6-Tribromophenol (S)87.6 39-132
84.3Phenol-d5 (S)81.0 34-121
Page 34 of 39Date:02/09/2024 08:26 AM
Page 115 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V43311QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V43116
Associated Lab Samples: 95681, 95682, 95683, 95684, 95685, 95686, 95687
LRB-V43116 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/08/24 15:3150.09.20<9.20mg/KgAliphatic C9-C18
02/08/24 15:3150.012.2<12.2mg/KgAliphatic C19-C36
02/08/24 15:3150.014.2<14.2mg/KgAromatic C11-C22
02/08/24 15:312-Fluorobiphenyl (S)89.0 40-140
02/08/24 15:312-Bromonaphthalene (S)83.0 40-140
02/08/24 15:31Chlorooctadecane (S)74.6 40-140
02/08/24 15:31OTP Surrogate (S)85.7 40-140
LCS-V43116 LCSD-V43116Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
44.3 73.874.344.660.0mg/KgAliphatic C9-C18 40-140 0.6 50
79.7 99.695.576.480.0mg/KgAliphatic C19-C36 40-140 4.2 50
182 107104176170mg/KgAromatic C11-C22 40-140 3.3 50
94.796.22-Fluorobiphenyl (S)40-140
91.794.02-Bromonaphthalene (S)40-140
71.668.8Chlorooctadecane (S)40-140
97.699.2OTP Surrogate (S)40-140
Page 35 of 39Date:02/09/2024 08:26 AM
Page 116 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V43310QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V43206
Associated Lab Samples: 95680
LRB-V43206 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/08/24 16:2435028.287.8µg/LAliphatic C9-C18
02/08/24 16:24500124<124µg/LAliphatic C19-C36
02/08/24 16:2425061.2<61.2µg/LAromatic C11-C22
02/08/24 16:242-Fluorobiphenyl (S)87.2 40-140
02/08/24 16:242-Bromonaphthalene (S)74.0 40-140
02/08/24 16:24Chlorooctadecane (S)77.8 40-140
02/08/24 16:24OTP Surrogate (S)81.8 40-140
LCS-V43206 LCSD-V43206Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
241 40.135.5*213600µg/LAliphatic C9-C18 40-140 12.3 50.0
877 110105841800µg/LAliphatic C19-C36 40-140 4.1 50.0
1660 97.688.815101700µg/LAromatic C11-C22 40-140 9.4 50.0
94.595.02-Fluorobiphenyl (S)40-140
88.789.72-Bromonaphthalene (S)40-140
70.174.2Chlorooctadecane (S)40-140
89.687.6OTP Surrogate (S)40-140
Page 36 of 39* QC Fail Date:02/09/2024 08:26 AM
Page 117 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V43049QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V43048
Associated Lab Samples: 95681, 95682, 95683, 95684, 95685, 95686, 95687
LRB-V43048 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/31/24 22:298.001.22<1.22mg/KgAliphatic C5-C8
01/31/24 22:298.004.56<4.56mg/KgAliphatic C9-C12
01/31/24 22:298.000.624<0.624mg/KgAromatic C9-C10
01/31/24 22:292,5-Dibromotoluene (FID) (S)82.6 70-130
01/31/24 22:292,5-Dibromotoluene (PID) (S)122 70-130
LCS-V43048 LCSD-V43048Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
34.6 10810533.632.0mg/KgAliphatic C5-C8 70-130 2.9 50
36.2 11311035.132.0mg/KgAliphatic C9-C12 70-130 3.0 50
11.6 10810110.810.7mg/KgAromatic C9-C10 70-130 7.1 50
81.991.42,5-Dibromotoluene (FID) (S)70-130
1171072,5-Dibromotoluene (PID) (S)70-130
Page 37 of 39Date:02/09/2024 08:26 AM
Page 118 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V43051QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V43050
Associated Lab Samples: 95680
LRB-V43050 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/31/24 19:4350.011.5<11.5µg/LAliphatic C5-C8
01/31/24 19:4350.025.8<25.8µg/LAliphatic C9-C12
01/31/24 19:4350.04.02<4.02µg/LAromatic C9-C10
01/31/24 19:432,5-Dibromotoluene (FID) (S)86.4 70-130
01/31/24 19:432,5-Dibromotoluene (PID) (S)88.9 70-130
LCS-V43050 LCSD-V43050Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
304 101101303300µg/LAliphatic C5-C8 70-130 0.3 50.0
319 106104313300µg/LAliphatic C9-C12 70-130 1.8 50.0
96.3 96.3111111100µg/LAromatic C9-C10 70-130 14.1 50.0
78.582.82,5-Dibromotoluene (FID) (S)70-130
1021132,5-Dibromotoluene (PID) (S)70-130
Page 38 of 39Date:02/09/2024 08:26 AM
Page 119 of 122
Quality Control Data
24-031-0014Report No:
Project Description:
Client ID:Harmon Environmental, PA
Souther States
Dry Weight Determination
SW-DRYWT
V43120QC Analytical Batch:
Analysis Method:
Analysis Description:
V 95682-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 02/02/24 11:550.420.020.1%Moisture
V 95683-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 02/02/24 11:550.921.421.6%Moisture
Page 39 of 39Date:02/09/2024 08:26 AM
Page 120 of 122
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:24-031-0014
Harmon Environmental, PA
00358
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 3.9C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:01/31/2024 15:03:12
Special precautions or instructions included?
Comments:
Page 121 of 122
Appendix G
Geologic Logs for Borings
BORING/WELL NO.:
PROJECT NAME:
PROJECT NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
4 -
8 -
12 -
16 -
20 -
SAMPLING
METHOD
GEOPROBE
GEOPROBE
GEOPROBE
GEOPROBE
GEOPROBE
MW-1 BORING LOG
2901 MONROE ROAD
951-01
MIDSOUTH ENV., INC.
DON WARREN
GEOPROBE
JANUARY 26, 2024
NOT MEASURED
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
RED SILTY CLAY
RED FINE SANDY CLAY
BROWN AND RED FINE SANDY SILTY CLAY
LIGHT GRAY FINE SANDY CLAY
GRAY, BROWN AND ORANGE SILTY FINE SAND
~-------------------------~
BORING TERMINATED AT 20 FEET
REMARKS/
COMMENTS
0.1 PPM-V
0.3 PPM-V
9.9 PPM-V
11.3 PPM-V
0.6 PPM-V
BORING/WELL NO.:
PROJECT NAME:
PROJEC,T NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
4 -
8 -
12 -
16 -
SAMPLING
METHOD
GEOPROBE
GEOPROBE
GEOPROBE
B1
2901 MONROE ROAD
951-01
MIDSOUTH ENV .• INC.
DON WARREN
GEOPROBE
JANI,.JARY 26, 2024
NOT MEASURED
BORING LOG
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
REMARKS/
COMMENTS
0.0 PPM-V
RED FINE SANDY CLAY
RED AND TAN SPECKLED FINE SANDY SILTY
CLAY
TAN, BLACK AND BROWN MOTTLED SILT
~-------------------------~
0.0 PPM-V
0.0 PPM-V
0.0 PPM-V
BORING TERMINATED AT 16 FEET
BORING/WELL NO.:
PROJECT NAME:
PROJECT NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
4 -
8 -
12 -
16 -
SAMPLING
METHOD
GEOPROBE
GEOPROBE
GEOPROBE
GEOPROBE
B2 BORING LOG
2901 MONROE ROAD
951-01
MIDSOUTH ENV., INC.
DON WARREN
GEOPROBE
JANUARY 26, 2024
NOT MEASURED
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
RED AND BROWN MOTTLED FINE TO
MEDIUM SANDY CLAY
RED FINE SANDY SILTY CLAY
RED FINE SANDY CLAYEY SILT
BROWN FINE SANDY CLAYEY SILT
~-------------------------~
BORING TERMINATED AT 16 FEET
REMARKS/
COMMENTS
0.0 PPM-V
0.0 PPM-V
0.0 PPM-V
0.0 PPM-V
BORING/WELL NO.:
PROJECT NAME:
PROJECT NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
4 -
8 -
12 -
16 -
SAMPLING
METHOD
GEOPROBE
GEOPROBE
GEOPROBE
B3
2901 MONROE ROAD
951-01
MIDSOUTH ENV., INC.
DON WARREN
GEOPROBE
JANUARY 26, 2024
NOT MEASURED
BORING LOG
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
REMARKS/
COMMENTS
RED SILTY CLAY 0.0 PPM-V
0.0 PPM-V
RED FINE SANDY MICACEOUS SILT
0.0 PPM-V
GRAY AND RED MOTTLED SILT 0.0 PPM-V
~-------------------------~
BORING TERMINATED AT 16 FEET
BORING/WELL NO.:
PROJECT NAME:
PROJECT NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
4 -
8 -
12 -
16 -
SAMPLING
METHOD
GEOPROBE
GEOPROBE
GEOPROBE
GEOPROBE
B4 BORING LOG
2901 MONROE ROAD
951-01
MIDSOUTH ENV., INC.
DON WARREN
GEOPROBE
JANUARY 26, 2024
NOT MEASURED
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
TAN AND RED FINE SANDY SILTY CLAY
RED FINE SANDY SILT
BROWN AND GRAY MOTTLED FINE SANDY
SILT
GRAY FINE TO MEDIUM SANDY CLAY
1----------------1
BORING TERMINATED AT 16 FEET
REMARKS/
COMMENTS
0.0 PPM-V
0.0 PPM-V
5.2 PPM-V
5.7 PPM-V
AppendixH
Monitor Well Construction Forms
WELL ABANDONMENT RECORD
1. Well Contractor Information:
Don Warren
Well Contractor Name (or well owner personally abandoning well on his/her property)
3581-A
NC Well Contractor Cenification Number
Mid South Environmental
Company Name
2. Well Construction Permit#: SIP #70003181
List all applicable well construction permits (i.e. UIC, Com1ty, State, Variance, etc.) ifknov.m
3. Well use (check well use):
Water Supply Well:
OAgricultural OMunicipai/Public
OGeothennal (Heating/Cooling Supply) OResidential Water Supply (single)
Olndustrial/Commercial OResidential Water Supply (shared)
Olrrigation
Non-Water Supply Well:
IIMonitoring ORecovery
Injection Well:
OAquifer Recharge OGroundwater Remediation
OAquifer Storage and Recovery OSalinity Barrier
OAquifer Test OStormwater Drainage
OExperimental Technology OSubsidence Control
OGeothermal (Closed Loop) OTracer
OGeothermal (Heating/Cooling Retnrn) OOther (explain under 7g)
4. Date well(s) abandoned: 2/16/2024
Sa. Well location:
MJP Monroe Rd Holdings, LLC
Facility/Owner Name Facility ID# (if applicable)
2901 Monroe Rd, Charlotte, NC 28205
Physical Address, City, and Zip
Mecklenburg
County
11908314
Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one !at/long is sufficient)
35 12' 16.35" N 80 48' 22.63" ------------------
CONSTRUCTION DETAILS OF WELL(Sl BEING ABANDONED
w
Attach well consh71Ction record(s} if available. For multiple injection or non-water supply wells
ONLY vdth the same construction/abandonment, you can submit one form.
Ga. Well ID#: TMW-1 ----------------
Gb. Total well depth: _2_0 ______ (ft.)
Gc. Borehole diameter: ._4_._2_5 _____ ,(in.)
Gd. Water level below ground surface: ________ (ft.)
Ge. Outer casing length (if !mown): _1_0 _______ (ft.)
Gf. Inner casing/tubing length (if !mown): _______ (ft.)
Gg. Screen length (if !mown): _1_0 _________ (ft.)
I For Internal Use ONLY:
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
well construction/depth, only I GW-30 is needed. Indicate TOTAL NUMBER of wells abandoned:_1 _______________ _
7b. Approximate volume of water remaining in well(s): _____ __;(gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:----------------
7d. Amount of disinfectant used:
7 e. Sealing materials used (check all that apply):
0 Neat Cement Grout
0 Sand Cement Grout
0 Concrete Grout
0 Specialty Grout
0 Bentonite Slurry
II Bentonite Chips or Pellets
0 Dry Clay
0 Drill Cuttings
0 Gravel
0 Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
25lbs Bentonite
7g. Provide a brief description of the abandonment procedure:
PVC removed from the ground and borehole filled
bentonite.
8. Certification:
2/18/24
Signature ofCenified Well Contractor or Well Owner Date
By signing this form, I hereby ce1·tify that the wel/(s) was (were) abandoned in
acco1-dance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this reco1-d has been provided to the well o;mer.
9. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
SUBJVIITT AL INSTRUCTIONS
lOa. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
lOb. For Injection Wells: In addition to sending the form to the address in lOa
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of\Vater Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
lOc. For Water Supply & Injection Wells: In addition to sending the form to the
address( es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
abandoned.
FormGW-30 North Carolina Department of Environmental Quality-Division of Water Resources Revised 2-22-2016