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HomeMy WebLinkAbout18045-Seneca Place-IA & SG Confirmation Sampling-Suite HINDOOR AIR AND SUB -SLAB VAPOR SAMPLING REPORT SENECA PLACE BROWNFIELDS SITE SUITE H 5033 SOUTH BOULEVARD CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA BROWNFIELDS PROJECT NO. 18045-14-060 ECS SOUTHEAST, LLP PROJECT 49:11814-B PREPARED FOR: NEW FORUM, LLC/SENECA PLACE PARTNERS, LLC NOVEMBER 15, 2021 i "Setting the Standard for Service" Ceotechnical • Construction Materials • Environmental • Facilities November 15, 2021 Mr. Tyler Steele New Forum, LLC/Seneca Place Partners, LLC 9224 Kings Parade Boulevard, Suite 2101 Charlotte, North Carolina 28273 Reference: Indoor Air and Sub -Slab Vapor Sampling Report Seneca Place Brownfields Site Suite H 5033 South Boulevard Charlotte, Mecklenburg County, North Carolina Brownfields Project No. 18045-14-060 ECS Project No. 49:11814-A Dear Mr. Steele: ECS Southeast, LLP (ECS) has completed the Indoor Air and Sub -Slab Vapor Sampling Report for the above referenced site. This report has been completed at the request of the North Carolina Department of Environmental Quality (NCDEQ) Division of Waste Management (NCDWM) — North Carolina Brownfields Program (NCBP). ECS appreciates the opportunity to provide our environmental consulting services to you on this project. If you have any questions concerning this work plan or this project, please contact us. Sincerely, LLP Scott Youy(g; P.G. Environ ental roject Manager 704-525-5152 syoungl@ecslimited.com Report Certification I, Scott Young, P.G., a Licensed Geol ' certify that the information cods c,Qi9 `°o g< SEAL irlv�zsg 2 19 Lei Roger A. Smith, P.G. Principal Geologist 704-525-5152 rsmith3@ecslimited.com ;S Southeast, LLP (NC Registered Geologist Firm C-553), do rrect and accurate to the best of my knowledge. �o � nP GG A 1812 Center Park Drive. Suite D. Charlotte, NC 28217 • T 704-525-5152 • www.ecslimited.cor ECS Capitol Services. PLLC • ECS Florida. LLC • ECS Mid -Atlantic. LLC • ECS Midwest LLC • ECS Southeast. LLP • ECS Southwest. Li. 5 Indoor Air& Sub -Slab Vapor Sampling Report Seneca Place Brownfields Site, Suite H Charlotte, Mecklenburg County, North Carolina Brownfields Project Number 18045-14-060 ECS Project No. 49:11814-8 November 15, 2021 TABLE OF CONTENTS 1.0 INTRODUCTION.......................................................................................................................................1 2.0 SCOPE OF WORK.....................................................................................................................................1 3.0 LABORATORY ANALYSES......................................................................................................................... 3 4.0 QA/QC..................................................................................................................................................... 3 5.0 CONCLUSIONS AND RECOMENDATIONS................................................................................................3 6.0 QUALIFICATIONS OF REPORT..................................................................................................................4 FIGURES Figure 1— Site Location Map Figure 2—Sample Location Map TABLES Table 1— Summary of Exterior Meteorological Conditions Table 2 — Summary of Indoor Air and Outside Background Analytical Results Table 3 — Summary of Leak Testing Results Table 4 — Summary of Sub -Slab Soil Gas Analytical Results n nnrninil-Ice AppendixA —Sampling Field Notes Appendix B — Indoor Air Survey Form Appendix C — Laboratory Analytical Reports and Chain -of -Custody Forms Appendix D — Historical Sample Results Appendix E — NCDEQ Risk Calculator Output Indoor Air & Sub -Slab Vapor Sampling Report Seneca Place Brownfields Site, Suite H Charlotte, Mecklenburg County, North Carolina Brownfields Project Number 18045-14-060 ECS Project No. 49:11814-B November 15, 2021 1.0 INTRODUCTION The subject property is located at 5033 South Boulevard in Charlotte, Mecklenburg County, North Carolina (Figure 1) and identified by the Mecklenburg County GIS as Parcel Identification Number (PIN) 17105209. The site currently consists of an approximate 36,750-square foot multi -tenant strip shopping center that was constructed in 1985, an approximate 5,700-square foot automotive garage that was constructed in 1984, associated parking areas, and various landscaped areas. Due to previously identified groundwater and associated vapor contaminants at the site, the site was included into the North Carolina Department of Environmental Quality (NCDEQ), Brownfields Program (BP). The Brownfields Agreement (BFA) for the site was finalized in April 2016. The Brownfields Project number for the site is 18045-14-60. The entity, Seneca Place Partners, LLC, intends to conduct plumbing up fits in the various existing suites of the strip shopping center. In accordance with the BFA, the NCDEQ, BP was notified of the intended up fits and the NCDEQ, BP required that a new Environmental Management Plan (EMP) be prepared to address the proposed activities. ECS completed and submitted the EMP (ECS Project No. 49:11814) on July 9, 2020. The new EMP was approved by the NCDEQ, BP on July 10, 2020. The plumping up -fits in Suite H were conducted between January 20 through 29, 2021. 2.0 SCOPE OF WORK On September 16, 2021, ECS collected four indoor air samples and on September 17, 2021, collected four sub -slab soil gas samples inside Suite H. These samples include IA-1 through IA-4 (indoor air) and SG-1 through SG-4 (sub -slab soil gas). Indoor air and sub -slab soil gas sampling were conducted to confirm that vapor intrusion (VI) concerns do not exist in the portions of the building that are to be occupied. The indoor air and sub -slab soil gas sampling were conducted in general accordance with the North Carolina Division of Waste Management's (NCDWM) Vapor Intrusion Guidance document (March 2018, Version 2) and Vapor Sampling Work Plan, Revision 2.0 dated August 6, 2020 and approved by the NCDEQ, Brownfields on August 11, 2020. 2.1 Indoor Air Sampling On September 16, 2021, four indoor air samples (IA-1 through IA-4) were collected at the site as shown at the locations shown on Figure 2. The locations were selected based on accessibility and as proposed in the above referenced approved Work Plan. Prior to conducting the indoor air sampling, ECS completed an Indoor Air Building Survey and Sampling Form that included information concerning the building characteristics, noted potential indoor air contaminant sources, general meteorological conditions, as well as other general observations and conditions that could potentially affect sampling and sample results. Meteorological conditions throughout the sampling event are summarized in Table 1. A copy of the survey form is included in Appendix B. In order to minimize disturbance of the canisters, ECS locked the doors to Suite H after initiating the sampling. All doors and windows remained closed during the sampling, with the exception of when ECS left and returned to complete the sampling. The heating, ventilation, and air conditioning (HVAC) was operating in its normal continuous mode when samples were collected. As noted on the indoor air building Indoor Air & Sub -Slab Vapor Sampling Report Seneca Place Brownfields Site, Suite H Charlotte, Mecklenburg County, North Carolina Brownfields Project Number 18045-14-060 ECS Project No. 49:11814-B November 15, 2021 survey, potential VOC source(s) were observed in the kitchen and dining area of Suite H, consisting of various cleaning products, new furniture, and new carpeting. The samples were collected using individually certified 6-liter (L) Summa canisters equipped with 8-hour flow restrictors. The samples were collected by placing each Summa canister at a height of approximately 5 feet above the floor during sampling. ECS documented the vacuum readings indicated on each canister at initiation and termination of sampling. These readings are included in Table 2 and the field notes included as Appendix A. The sample containers were labeled, placed into protective packaging material and shipped to Con -Test Analytical Laboratory (Con -Test) in East Longmeadow, Massachusetts, to be analyzed for volatile organic compounds (VOCs) by EPA Method TO-15. ECS maintained chain -of -custody (COC) procedures throughout the sample collection and transportation process. ECS collected one duplicate indoor air sample for laboratory analysis by EPA Method TO-15. Sample IA-DUP was a duplicate of indoor air sample IA-1 and was collected jointly with indoor air sample IA-1 via a tee connection in the tubing. Concurrent with the indoor air sampling, one exterior (ambient) upwind air sample (AA-1) was collected for laboratory analysis by EPA Method TO-15. The approximate location of the exterior sample is indicated on Figure 2. 2.2 Sub -Slab Soil Gas Samplin On September 17, 2021, ECS collected four sub -slab soil gas samples from newly installed sub -slab monitoring points (SG-1 through SG-4) at the site as shown at the locations shown on Figure 2. The sub - slab samples were collected by installing new VaporPin° with a new silicon sleeve through the existing concrete slab and allowed to equilibrate for a minimum of 20 minutes, prior to leak testing. New dedicated and disposable polyethylene tubing was then connected from the VaporPin° to a pre -evacuated and pre -cleaned batch certified Summa canister. Prior to collecting the soil gas samples, laboratory grade helium gas was used as a quality assurance/control measure to confirm the integrity of the VaporPin° seal. A plastic container (with an approximate volume of 18 quarts) used as a shroud was placed and sealed over the sampling point and sampling train. The sampling tubing and tracer gas tubing were placed through the container wall via rubber grommets and a shroud was placed over the sample point and sample train leading to the purge valves and sample port. The container was flooded with helium via the hose placed through the container wall. A Model MGD-2000 Multi -Gas Leak detector was connected to the probe tube and three calculated purge volumes were purged with a syringe. The calculated purge volume included the sample train as well as the plumbing of the monitoring point plumbing. Helium samples were collected with a syringe into a tedlar bag, and readings recorded in field notes and provided as Table 3. Additionally, the construction details of the permanent sub -slab soil gas sampling points are included on the sampling field notes. A concentration of less than 10 percent of the helium concentration within the shroud was considered acceptable. Following the helium leak test, sub -slab soil gas samples were collected using 1-liter Summa canisters at an approximate flow rate of 0.2 L/minute over an approximate 5-minute period. ECS documented the vacuum readings indicated on each canister at initiation and termination of sampling. These readings are 2 Indoor Air & Sub -Slab Vapor Sampling Report Seneca Place Brownfields Site, Suite H Charlotte, Mecklenburg County, North Carolina Brownfields Project Number 18045-14-060 ECS Project No. 49:11814-B November 15, 2021 included in Table 4 and the field notes included as Appendix A. The sample containers were labeled, placed into protective packaging material and shipped to Con -Test to be analyzed for VOCs by EPA Method TO-15. ECS maintained COC procedures throughout the sample collection and transportation process. A copy of the COC is included in Appendix C. ECS collected one duplicate sub -slab soil gas sample for laboratory analysis by EPA Method TO-15. Sample SG-DUP was a duplicate of sub -slab soil gas sample SG- 1. 3.0 LABORATORY ANALYSES A summary of the laboratory analytical data for indoor air samples is shown on Table 2. Review of the laboratory analytical report indicated a total of nine compounds in one or more of the samples collected at concentrations greater than their respective Residential Vapor Intrusion Screening Levels (VISLs), with the concentrations of chloroform in sample IA-3 and ethylbenzene, naphthalene, and m&p-xylene in samples IA-1 through IA-4 greater than their respective Non -Residential VISLs. Various additional compounds were detected in one or more of the indoor air samples collected at concentrations greater than the laboratory method reporting limits, but less than their respective VISLs. A summary of the laboratory analytical data for sub -slab soil gas samples is shown on Table 4. Review of the laboratory analytical report indicated concentrations of 1,2-dichloroethane and 1,1,2-trichloroethane in the SG-3 sub -slab sample greater than their respective Residential VISLs, but less than their respective Non -Residential VISLs. Several additional compounds were detected in one or more of the sub -slab soil gas samples collected at concentrations greater than the laboratory method reporting limits, but less than their respective VISLs. The laboratory analytical report is included as Appendix C. 4.0 QA/QC The Summa canisters were individually certified for indoor air samples and batch certified for the soil gas samples. Helium concentrations did not exceed five percent (5%) helium above the shroud concentrations during leak tests for sub -slab samples. During the sampling of sub -slab soil gas, the sample train was closed when the canister vacuum decreased to approximately five inches of mercury (in-Hg). ECS documented the vacuum readings indicated on each canister at initiation and termination of sampling. These readings are included in Tables 2 and 4 and the field notes included as Appendix B. A duplicate indoor air sample (IA-DUP) was collected in conjunction with IA-1 while a duplicate sub -slab soil gas sample (SG-DUP) was collected from SV-1. Results of the duplicate analysis appear consistent with the samples they were collected in conjunction with. 5.0 CONCLUSIONS AND RECOMENDATIONS Based on the laboratory analytical data, petroleum -related VOCs were detected in the indoor air of the portions of the building that were sampled above their respective Non -Residential VISLs. VOCs were not detected in the sub -slab soil gas samples at levels exceeding their respective Non -Residential VISLs. 3 Indoor Air & Sub -Slab Vapor Sampling Report Seneca Place Brownfields Site, Suite H Charlotte, Mecklenburg County, North Carolina Brownfields Project Number 18045-14-060 ECS Project No. 49:11814-B November 15, 2021 The absence of VOCs at concentrations above the Non -Residential VISLs in the sub -slab soil gas samples suggest that the exceedances of VOCs in indoor air samples may be the result of a source or sources other than vapor intrusion of soil gas. The initial driver for the sampling was a concentration of tetra chloroethene (PCE) detected in soil gas sample VMP-2 collected by Hart & Hickman on May 5, 2015. PCE was not detected in the indoor air or sub -slab samples collected at concentrations greater than its VISLs. The locations of the historic soil gas samples are shown on Figure 2 and the analytical results of the soil gas samples are included in Appendix D. As such, the indoor air concentrations leading to the Non - Residential VISL exceedances appear to be attributed to indoor air sources/materials used during construction and not a result of vapors below the building. In addition, in light of the results for the indoor air and sub -slab soil gas samples collected, ECS input the laboratory analytical results of these samples into the NCDEQ Risk Calculator. Based on the results of the NCDEQ Risk Calculator, the concentrations did not exceed the risk thresholds for residential and non- residential uses for any of the samples collected. Output from the results of the NCDEQ Risk Calculator are presented in Appendix E. Based upon the results of this assessment and the above conclusions, ECS recommends no additional sampling at this time. 6.0 QUALIFICATIONS OF REPORT The activities and evaluative approaches used in this assessment are consistent with those normally employed in environmental assessment projects of this type. Our evaluation of site conditions has been based on our understanding of the site project information and the data obtained during our field activities. Environmental sampling performed and reported herein only provides for specific data points scattered throughout the project area in accordance with the prior approved scope of work and work authorization. 4 FIGURES SCALE 1:24 000 1 0.5 D KILON,ETEas 1 2 500 D METERS 100C 201)O 1 0.5 0 1 MILES 1 oC 4 4 1440 zw 3000 40IO 5D30 110w 7D00 mm 900ID 1 DDDU 24al N W * E c+ f9. SINQ , } L_ A 1 mA 4q, C'items A F1 FA LE .1 r ' A $ p�x ` 5 SppIM IIrv- r 1 LF •B, �,rl � NassEi�' SITE LOCATION 4 M1 xYt }.V � 2+j [}+[}� 31, � 4l• O W� J Client: Seneca Place Partners, LLC Project: SENECA PLACE SHOPPING CENTER 5033 SOUTH BOULEVARD CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA Title: USGS TOPOGRAPHIC MAP SCALE AS SHOWN Source: Charlotte West, NC 7.5' Topographic Map, 2019 Charlotte East, NC 7.5' Topographic Map, 2019 Drawn By: Checked By: MSY RAS Approved By: Date: RAS 12/07/20 ECS Project No. 49:11814-B FIGURE 1 i rrt= un EXISTING PARCEL BOUNDARY INDOOR AIR/SUB-SLAB SAMPLE OUTDOOR BACKGROUND I I APPROXIMATE SUITE LOCATION SAMPLE I _ _ _ _ PARTITIONS .VMP1/13 Approximate sub -slab sample collected by Hart & Hickman in 2015. (sample ID / PCE concentration in µg/m3) bold values exceeded Non -Residential Soil gas Screening Level of 3,500 µg/m3 0 0.01251.025 0.05 Miles I I I I I I I Client: SENECA PLACE PARTNERS, LLC Project: SENECA PLACE SHOPPING CENTER 5033 SOUTH BOULEVARD CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA Title: SAMPLE LOCATION MAP SCALE AS SHOWN Source: Charlotte -Mecklenburg County POLARIS GIS Website Drawn By: Checked By: MSY RAS Approved By: Date: RAS 11/8/2021 ECS Project No. 49:11814-B FIGURE 2 TABLES TABLE 1 SUMMARY OF EXTERIOR METEOROLOGICAL CONDITIONS Seneca Place Brownfields Site - Suite H 5033 South Boulevard Charlotte, Mecklenburg County, North Carolina Brownfields Project No.: 18045-14-060 ECS Project No.: 49:11814-B Date Time Temperature (°F) Dew Point (7) Humidity Humidity Wind Wind Speed (mph) Pressure (in Hz0) Amount of Precipitation (in) Condition 9/16/2021 8:52 AM 71 68 90 N 7 29.29 0.0 Light Rain 9/16/2021 9:52 AM 72 68 87 NNE 12 29.30 0.0 Cloudy 9/16/2021 10:52 AM 74 68 82 NNE 6 29.32 0.0 Light Rain 9/16/2021 11:52 AM 75 68 79 NNE 5 29.32 0.0 Light Rain 9/16/2021 12:52 PM 75 69 82 NNE 7 29.31 0.0 Light Rain 9/16/2021 1:52 PM 76 69 79 N 6 29.30 0.0 Light Rain 9/16/2021 2:52 PM 78 69 74 NNE 7 29.29 0.0 Mostly Cloudy 9/16/2021 3:52 PM 80 69 69 NNE 8 29.28 0.0 Mostly Cloudy 9/16/2021 4:52 PM 80 66 62 NE 6 29.27 0.0 Mostly Cloudy 9/16/2021 5:52 PM 80 67 64 NE 5 29.27 0.0 Mostly Cloudy 9/16/2021 6:52 PM 78 67 68 NNW 3 29.28 0.0 Mostly Cloudy 9/16/2021 7:52 PM 76 66 71 N 3 29.29 0.0 Mostl Cloud Notes: Meteorological information obtained from Weather Underground website (https://www.wunderground.com/history/daily/us/nc/charlotte/KCLT/date/2021-9-16) T = degrees Fahrenheit mph = miles per hour in H2O = inches of water in = inches TABLE 2 SUMMARY OF INDOOR AIR AND OUTSIDE BACKGROUND ANALYTICAL RESULTS Seneca Place Brownfields Site - Suite H 5033 South Boulevard Charlotte, Mecklenburg County, North Carolina Brownfields Project No.: 18045-14-060 ECS Project No.: 49:11814-B Volatile Organic Compounds by EPA TO-15 Laboratory Initial Sample Final Sample v c v 2 `o v c r 0 0 Vaccuum Vaccum Vaccum v w a v Sample ID Sample Date no Y c c c Reading Reading Reading o v s N (in Hg) (in Hg) (in Hg) is w o U E o m L ri w L E •: n > n i0 c N 13 c O O N U C 0 3 m ONCW O r O :E u -E E 0 O O O ra LW c H H H0 vNCO mCN 3 :E :EO U> L O u O no na 'rp - - .p V N V>E1 M 0>XNO7 , N ❑ cI 2 Zco c-I '-I E Non -Residential VISL 27,000 16 4,400 2.0 0.53 79 5,300 88 0.47 NS NS 61 4.9 350 1 350 610 180 530 0.36 880 35 1,800 4,400 0.18 NS 4,400 53 53 88 88 IA-1 -30 -29 -5 09/16/21 75 0.77 7.4 0.49 0.39 1.1 1.7 3.3 <0.14 <0.24 720 <1.3 65 0.60 <0.14 2.8 J 35 3.6 2.7 <0.15 <0.24 3.9 3.9 <0.19 20 0.87 J 4.0 0.93 230 74 IA -DU P* -30 -30 -5 09/16/21 16 0.43 1.3 J 0.44 0.27 1.3 2.7 <0.14 0.14 J 20 <1.3 0.36 <0.17 0.35 0.75 J 2.1 J 1.8 0.19 0.12 J 0.085 J <1.0 1.3 <0.19 1.4 0.65 J 0.21 0.055 J 1.2 0.46 IA-2 -30 -29 -6 09/16/21 64 0.75 5.5 0.48 0.42 1.2 1.2 3.5 <0.14 <0.24 670 <1.3 54 0.72 0.80 1.9 J 33 1.2 2.7 <0.15 0.18 J 3.8 3.6 <0.19 18 0.95 J 3.6 0.84 190 62 IA-3 -30 -29 -6 09/16/21 82 0.89 5.5 0.59 0.83 1.2 3.2 3.1 0.72 <0.24 650 28 50 <0.17 <0.14 <4.9 1 15 1.8 1.6 1.6 0.35 4.0 14 1.3 10 0.72 J 2.4 0.50 170 57 IA-4 -30 -30 -5 09/16/21 31 0.92 3.81 0.38 0.29 1.5 1.4 3.4 <0.14 <0.24 760 <1.3 69 0.40 0.85 1.4 J 7.7 0.81 J 1.5 0.46 0.111 3.6 3.3 <0.19 12 0.61 J 2.1 0.36 230 73 AA-1 30 28 6 09/16/21 64 0.81 5.8 0.43 0.30 1.3 1.5 3.5 0.111 <0.24 690 <1.3 65 1 0.6 0.77 1 1.11 1 31.0 0.68 J 2.3 1.2 0.121 2.2 4.1 <0.19 20 0.66 J 3.8 0.74 220 69 Notes. Results presented in micrograms per cubic meter (µg/m3) in Hg = inches of mercury Non -Residential VISL= NCDEQ-DWM Non -Residential Vapor Instrusion Screening Level Indoor Air Level (A) (June 2021) at target risk 1.0E-06 - - IA-DUP is a duplicate sample of the IA-1 record sample 1= Estimated concentration detected between laboratory method detection limit and reporting limit INS = No Standard Established VALUE= concentration greaterthan the laboratory method reporting limit VALUE J= concentration greaterthan the Non -Residential VISL TABLE 3 SUMMARY OF LEAK TESTING RESULTS Seneca Place Brownfields Site - Suite H 5033 South Boulevard Charlotte, Mecklenburg County, North Carolina Brownfields Project No.: 18045-14-060 ECS Project No.: 49:11814-B Sample ID Helium Concentration in Shroud (ppm) Helium Readings from Sample Train (ppm) 1 2 3 SG-1 28,000 2S 0 0 SG-2 19,000 0 0 SG-3 34,000 0 0 SG-4 29,000 0 0 EOOJ Notes. ppm = parts per million TABLE 4 SUMMARY OF SUB -SLAB SOIL GAS ANALYTICAL RESULTS Seneca Place Brownfields Site - Suite H 5033 South Boulevard Charlotte, Mecklenburg County, North Carolina Brownfields Project No.: 18045-14-060 ECS Project No.: 49:11814-B Laboratory Reading Reading M. ex eye ��m� a x�mx m. er lNE/m31 - .NeiS,,—hg Level inaoorE—.—d sun-sbe soeemn¢Eevei lfebruarvzozal - 15 � er.xe e...�a or o ee � aoare m �`ao�x.�o-an a rerma�me No�ae,me„nai msr nmsumu AVAJ II 7 J , • � b • o !��ri�9Y�i�Ti11mmommofI�A1 IL-16 wills! mi off 11 IM 1 lip 44— JO A / I , p i #,j .1 k 1--z' � M�"l 9f Zzl) .� 10 - - i Y V I �i � LV 1 7 k � ol ® I f ------------------ --I ----- V --- --- ` I I I ITI I © jv- { OA 0� q 13,3 )JO �,'D �) .-p )10 I Of f- Amrk dl O (nnivcA,ur(�, C�) CIA 44 4 5 {Ot- N r- 0 V( T � J CS' N r Y P i T F I 3 � r� P ti M 1 c� /_1»=1►IQPAV4=3 INDOOR AIR BUILDING SURVEY and SAMPLING FORM iite Name: M#: ip 'reparer's namclw r mi �"cT. y Date: r-�1y' O1 - 1 'reparer's affiliation: ELS Phone #: 164fl part 1- Occupants ' ,�t� Building Address: �033 �v,ytct �VD �%Tlj Property Contact: Owner / Renter / otber: Contact's Phone: home ( ) work ( ) cell ( ) # of Building occupants: Children under age 13 ff� Children age 13-18 Adults Part 11— Building Characteristics Building type: residential / multi -family residential / office stri mall commercial / industrial Describe building: k 1 UU i \ 0. tCk 'SM.P TI\AL — Year constructed: Sensitive population: day care / nursing home / hospital / school / other (specify): _ Number of floors below grade: —6- (fall basement / crawl space / slab on grade) Number of floors az or above grade: 1 Depth of basement below grade surface: ft. Basement size: ftr Basement floor construction: concrete / dirt / floating / stone / other (specify): Foundation walls: poured con cinder bloc stone / other (specify) Basement sump present? Yes / No Sump pump? Yes No Water in smnp? yes No Type of healing system (circle all that apply): hotaircirculation hot air radiation wood steam radiation meal pump hot water radiation kerosene heater electric baseboard of er(specify): Type of ventilation system (circle all that apply): a av conditiontn mechanical f aflnnom ventilation fans dtvt ua avng uni en range hood fan a t e au m other (specify): e Type(Corte all that apply): Nazural gas electric / fuel el oil /wood /coal /solar /kerosene Are the basement walls or floor sealed with waterproof paint or epoxy comings? Yes / Na Is there a whole house fan? Yes Septic system? Yes / Yes (but not used) r..No Irrigation/pnvate well? Yes / Yes (but no used) No Type of ground cover outside of building: grass wnc / asphalt other (specify) Existing subsurface depressurization (radon) system in place? Yes & active /Passive Sub -slab vapor/moisture barrier in place? Type of barrier: Yes / No Part III - Outside Contaminant Sources Ity� rr Other stationary sources nearby (gas stations, emission stacks, etc.): Neat C) � tQC Heavy vehicular traffic nearby (or other mobile sources): \ F "N SC Part IV -Indoor Contaminant Sources Identify all potential indoor sources found in the building (including attached garages) and crawlspace (if present), the location of the some (floor and room), and whether the item was removed from the building 48 hours prior to indoor air sampling event. Any ventilation implemented after removal of the items should be completed a[ least 24 hours prior to the commencement of the indoor air sampling event. entiajc�: Location(s) Removed storared e storainne E solve- anersphol other house cleaning products SL ' Moth balls Polishes/waxes U JW Insecticides Furniture/floor polish 4a - Nail polish / polish remover Hairspray Cologne /perhme Air fresheners -� Fuel tank (inside buildin) -� stove or fireplace New furniture / upholstery — 4NAWood Hobbies - um, paints, etc. Part V — Miscellaneous Items Do any occupants of the building smoke? Yes Na , How often? Last time someone smoked in the building? J1_ hours / days ago Does the building have an attached garage directly connected to living space? Yes If so, is a car usually parked in the garage? Yes / No Are gas -powered equipment or cans of goaoline/fuels stored in the garage? Yes / No Do the occupants of the building have thew clothes dry cleaned? Yes / No If yes, how often? weekly / monthly / 34 limes a year Do any of the occupants use solvents in work? Yes No If yes, what types of solvents are used? If yes, are their clothes washed at work? Yes / No Have any pesticides/herbicides been applied around the building or in the yard? If so, when and which chemicals? Has there ever been a fire in the building? Yes / No If yes, when? Yes No Has painting or staining been done in the building in the last 6 months? Yes No If yes, when T ItA kokandwhen:? t TN��WLk4 Part VI —Sampling Information Sample Technician: Phone number: ( ) Sample Source: Indoor Air / Crawlspace Air / Sub -Slab / Near Slab Soil Gas / Exterior Soil Gas Sampler Type: Tedlar bag / Sorbent / Stainless Steel Canister / Other (specify): Analytical Method: TO-15 / TO-17 / other: Cert. Laboratory: Sample locations (floor, room): Field [DR _ - Field ID # Field ID # Field M # Were -Instructions for Occupams" followed? Yes /No If not, describe modifications: APPENDIX C con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 September 27, 2021 Scott Young ECS Southeast - Greensboro, NC 4811 Koger Boulevard Greensboro, NC 27407 Project Location: Charlotte, NC Client Job Number: Project Number: 11814B Laboratory Work Order Number: 21I1198 Enclosed are results of analyses for samples received by the laboratory on September 20, 2021. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kerry K. McGee Project Manager QA Officer Katherine Allen Laboratory Manager Daren Damboragian Page 1 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ECS Southeast - Greensboro, NC REPORT DATE: 9/27/2021 4811 Koger Boulevard Greensboro, NC 27407 PURCHASE ORDER NUMBER: ATTN: Scott Young PROJECT NUMBER: 11814B ANALYTICAL SUMMARY WORK ORDER NUMBER: 21I1198 The results of analyses performed on the following samples submitted to Con -Test, a Pace Analytical Laboratory, are found in this report. PROJECT LOCATION: Charlotte, NC FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB SG-1 21I1198-01 Soil Gas EPATO-15 SG-2 21I1198-02 Soil Gas EPATO-15 SG-3 21I1198-03 Soil Gas EPATO-15 SG-4 21I1198-04 Soil Gas EPA TO-15 SG-DUP 21I1198-05 Soil Gas EPATO-15 Page 2 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. EPA TO-15 Qualifications: Laboratory fortified blank/laboratory control sample recovery outside of control limits. Data validation is not affected since all results are "not detected" for all samples in this batch for this compound and bias is on the high side. Analyte & Samples(s) Qualified: Vinyl Acetate B290913-BSI Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this compound is likely to be biased on the low side. Analyte & Samples(s) Qualified: Ethyl Acetate 21I1198-01[SG-1], 21I1198-02[SG-2], 21I1198-03[SG-3], 21I1198-04[SG-4], 21I1198-05[SG-DUP], B290913-BLKI, B290913-BS1 Internal Standard is outside of control criteria for this sample. The analytes being reported for this analytical run are not affected by this I.S. being outside of control criteria. Data validation is not affected. Analyte & Samples(s) Qualified: 1,4-Difluorobenzene (1) 21I1198-01 RE 1 [SG-1 ] Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this compound. Reported result is estimated. Analyte & Samples(s) Qualified: Naphthalene 21I1198-01[SG-1], 21I1198-03[SG-3], 21I1198-04[SG-4], S063579-CCVI Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was 'hot detected" for this compound. Analyte & Samples(s) Qualified: Vinyl Acetate B290913-BS1, 5063579-CCVI Page 3 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 The results of analyses reported only relate to samples submitted to Con -Test, a Pace Analytical Laboratory, for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Tod E. Kopyscinski Laboratory Director Page 4 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Charlotte, NC Date Received: 9/20/2021 Field Sample #: SG-1 Sample ID: 21I1198-01 Sample Matrix: Soil Gas Sampled: 9/17/2021 12:06 Sample Description/Location: Sub Description/Location: Canister ID: 2108 Canister Size: 1 liter Flow Controller ID: 4098 Sample Type: 5 min Work Order: 21I1198 Initial Vacuum(in Hg): -27 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -4.8 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Acetone 71 8.0 4.8 170 19 11 4 9/23/21 21:55 BRF Benzene 0.36 0.20 0.048 1.2 0.64 0.15 4 9/23/21 21:55 BRF Benzyl chloride ND 0.20 0.090 ND 1.0 0.47 4 9/23/21 21:55 BRF Bromodichloromethane ND 0.20 0.073 ND 1.3 0.49 4 9/23/21 21:55 BRF Bromoform ND 0.40 0.072 ND 4.1 0.74 4 9/23/21 21:55 BRF Bromomethane ND 0.20 0.16 ND 0.78 0.63 4 9/23/21 21:55 BRF 1,3-Butadiene ND 0.20 0.14 ND 0.44 0.31 4 9/23/21 21:55 BRF 2-Butanone (MEK) 4.3 8.0 0.66 J 13 24 2.0 4 9/23/21 21:55 BRF Carbon Disulfide 1.1 2.0 0.51 J 3.4 6.2 1.6 4 9/23/21 21:55 BRF Carbon Tetrachloride 0.10 0.20 0.060 J 0.63 1.3 0.38 4 9/23/21 21:55 BRF Chlorobenzene ND 0.20 0.060 ND 0.92 0.27 4 9/23/21 21:55 BRF Chloroethane ND 0.20 0.15 ND 0.53 0.39 4 9/23/21 21:55 BRF Chloroform 0.72 0.20 0.048 3.5 0.98 0.24 4 9/23/21 21:55 BRF Chloromethane ND 0.40 0.082 ND 0.83 0.17 4 9/23/21 21:55 BRF Cyclohexane 4.3 0.20 0.13 15 0.69 0.46 4 9/23/21 21:55 BRF Dibromochloromethane ND 0.20 0.067 ND 1.7 0.57 4 9/23/21 21:55 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.056 ND 1.5 0.43 4 9/23/21 21:55 BRF 1,2-Dichlorobenzene ND 0.20 0.074 ND 1.2 0.44 4 9/23/21 21:55 BRF 1,3-Dichlorobenzene ND 0.20 0.048 ND 1.2 0.29 4 9/23/21 21:55 BRF 1,4-Dichlorobenzene ND 0.20 0.081 ND 1.2 0.49 4 9/23/21 21:55 BRF Dichlorodifluoromethane (Freon 12) 11 0.20 0.061 54 0.99 0.30 4 9/23/21 21:55 BRF 1, 1 -Dichloroethane ND 0.20 0.067 ND 0.81 0.27 4 9/23/21 21:55 BRF 1,2-Dichloroethane ND 0.20 0.073 ND 0.81 0.30 4 9/23/21 21:55 BRF 1, 1 -Dichloroethylene ND 0.20 0.079 ND 0.79 0.31 4 9/23/21 21:55 BRF cis-1,2-Dichloroethylene ND 0.20 0.068 ND 0.79 0.27 4 9/23/21 21:55 BRF trans-1,2-Dichloroethylene ND 0.20 0.070 ND 0.79 0.28 4 9/23/21 21:55 BRF 1,2-Dichloropropane ND 0.20 0.072 ND 0.92 0.33 4 9/23/21 21:55 BRF cis- 1,3 -Dichloropropene ND 0.20 0.093 ND 0.91 0.42 4 9/23/21 21:55 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.062 ND 0.91 0.28 4 9/23/21 21:55 BRF 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.069 ND 1.4 0.48 4 9/23/21 21:55 BRF 1,4-Dioxane ND 2.0 0.14 ND 7.2 0.49 4 9/23/21 21:55 BRF Ethanol 260 60 18 490 110 34 30 9/23/21 22:26 BRF Ethyl Acetate 26 2.0 1.2 L-03 93 7.2 4.3 4 9/23/21 21:55 BRF Ethylbenzene ND 0.20 0.052 ND 0.87 0.22 4 9/23/21 21:55 BRF 4-Ethyltoluene ND 0.20 0.062 ND 0.98 0.30 4 9/23/21 21:55 BRF Heptane ND 0.20 0.082 ND 0.82 0.34 4 9/23/21 21:55 BRF Hexachlorobutadiene ND 0.20 0.11 ND 2.1 1.2 4 9/23/21 21:55 BRF Hexane ND 8.0 0.66 ND 28 2.3 4 9/23/21 21:55 BRF 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 9/23/21 21:55 BRF Isopropanol 18 8.0 1.8 45 20 4.5 4 9/23/21 21:55 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.080 ND 0.72 0.29 4 9/23/21 21:55 BRF Methylene Chloride 3.1 2.0 0.46 11 6.9 1.6 4 9/23/21 21:55 BRF 4-Methyl-2-pentanone (MIBK) 0.48 0.20 0.10 2.0 0.82 0.42 4 9/23/21 21:55 BRF Naphthalene 0.51 0.20 0.13 V-35 2.7 1.0 0.66 4 9/23/21 21:55 BRF Propene ND 8.0 0.67 ND 14 1.2 4 9/23/21 21:55 BRF Styrene ND 0.20 0.063 ND 0.85 0.27 4 9/23/21 21:55 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.061 ND 1.4 0.42 4 9/23/21 21:55 BRF Page 5 of 29 con -test® A Pace Analytical Laboratory Project Location: Charlotte, NC Date Received: 9/20/2021 Field Sample #: SG-1 Sample ID: 21I1198-01 Sample Matrix: Soil Gas Sampled: 9/ 17/2021 12:06 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2108 Canister Size: 1 liter Flow Controller ID: 4098 Sample Type: 5 min Work Order: 21I1198 Initial Vacuum(in Hg): -27 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -4.8 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.20 0.059 ND 1.4 0.40 4 9/23/21 21:55 BRF Tetrahydrofuran 4.7 2.0 0.49 14 5.9 1.5 4 9/23/21 21:55 BRF Toluene 5.0 0.20 0.084 19 0.75 0.32 4 9/23/21 21:55 BRF 1,2,4-Trichlorobenzene ND 0.20 0.14 ND 1.5 1.0 4 9/23/21 21:55 BRF 1, 1, 1 -Trichloroethane ND 0.20 0.092 ND 1.1 0.50 4 9/23/21 21:55 BRF 1,1,2-Trichloroethane ND 0.20 0.080 ND 1.1 0.43 4 9/23/21 21:55 BRF Trichloroethylene ND 0.20 0.074 ND 1.1 0.40 4 9/23/21 21:55 BRF Trichlorofluoromethane (Freon 11) 4.6 0.80 0.080 26 4.5 0.45 4 9/23/21 21:55 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.23 0.80 0.071 J 1.7 6.1 0.54 4 9/23/21 21:55 BRF 1,2,4-Trimethylbenzene ND 0.20 0.059 ND 0.98 0.29 4 9/23/21 21:55 BRF 1,3,5-Trimethylbenzene ND 0.20 0.055 ND 0.98 0.27 4 9/23/21 21:55 BRF Vinyl Acetate ND 4.0 0.37 ND 14 1.3 4 9/23/21 21:55 BRF Vinyl Chloride ND 0.20 0.079 ND 0.51 0.20 4 9/23/21 21:55 BRF m&p-Xylene 21 0.40 0.11 93 1.7 0.48 4 9/23/21 21:55 BRF o-Xylene ND 0.20 0.054 ND 0.87 0.23 4 9/23/21 21:55 BRF Surrogates 4-Bromofluorobenzene (1) 4-Bromofluorobenzene (1) % Recovery % REC Limits 92.5 70-130 98.2 70-130 9/23/21 22:26 9/23/21 21:55 Page 6 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Charlotte, NC Sample Description/Location: Work Order: 2111198 Date Received: 9/20/2021 Sub Description/Location: Initial Vacuum(in Hg): -29 Field Sample #: SG-2 Canister ID: 2230 Final Vacuum(in Hg): -5 Sample ID: 21I1198-02 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.7 Sample Matrix: Soil Gas Flow Controller ID: 4309 Flow Controller Type: Fixed -Orifice Sampled: 9/17/2021 11:28 Sample Type: 5 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 26 8.0 4.8 62 19 11 4 9/23/21 23:26 BRF Benzene 0.67 0.20 0.048 2.1 0.64 0.15 4 9/23/21 23:26 BRF Benzyl chloride ND 0.20 0.090 ND 1.0 0.47 4 9/23/21 23:26 BRF Bromodichloromethane ND 0.20 0.073 ND 1.3 0.49 4 9/23/21 23:26 BRF Bromoform ND 0.40 0.072 ND 4.1 0.74 4 9/23/21 23:26 BRF Bromomethane ND 0.20 0.16 ND 0.78 0.63 4 9/23/21 23:26 BRF 1,3-Butadiene ND 0.20 0.14 ND 0.44 0.31 4 9/23/21 23:26 BRF 2-Butanone (MEK) ND 8.0 0.66 ND 24 2.0 4 9/23/21 23:26 BRF Carbon Disulfide ND 2.0 0.51 ND 6.2 1.6 4 9/23/21 23:26 BRF Carbon Tetrachloride ND 0.20 0.060 ND 1.3 0.38 4 9/23/21 23:26 BRF Chlorobenzene ND 0.20 0.060 ND 0.92 0.27 4 9/23/21 23:26 BRF Chloroethane ND 0.20 0.15 ND 0.53 0.39 4 9/23/21 23:26 BRF Chloroform ND 0.20 0.048 ND 0.98 0.24 4 9/23/21 23:26 BRF Chloromethane ND 0.40 0.082 ND 0.83 0.17 4 9/23/21 23:26 BRF Cyclohexane 8.4 0.20 0.13 29 0.69 0.46 4 9/23/21 23:26 BRF Dibromochloromethane ND 0.20 0.067 ND 1.7 0.57 4 9/23/21 23:26 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.056 ND 1.5 0.43 4 9/23/21 23:26 BRF 1,2-Dichlorobenzene ND 0.20 0.074 ND 1.2 0.44 4 9/23/21 23:26 BRF 1,3-Dichlorobenzene ND 0.20 0.048 ND 1.2 0.29 4 9/23/21 23:26 BRF 1,4-Dichlorobenzene ND 0.20 0.081 ND 1.2 0.49 4 9/23/21 23:26 BRF Dichlorodifluoromethane (Freon 12) 0.92 0.20 0.061 4.5 0.99 0.30 4 9/23/21 23:26 BRF 1,1-Dichloroethane ND 0.20 0.067 ND 0.81 0.27 4 9/23/21 23:26 BRF 1,2-Dichloroethane ND 0.20 0.073 ND 0.81 0.30 4 9/23/21 23:26 BRF 1,1-Dichloroethylene ND 0.20 0.079 ND 0.79 0.31 4 9/23/21 23:26 BRF cis-1,2-Dichloroethylene ND 0.20 0.068 ND 0.79 0.27 4 9/23/21 23:26 BRF trans-1,2-Dichloroethylene ND 0.20 0.070 ND 0.79 0.28 4 9/23/21 23:26 BRF 1,2-Dichloropropane ND 0.20 0.072 ND 0.92 0.33 4 9/23/21 23:26 BRF cis- 1,3 -Dichloropropene ND 0.20 0.093 ND 0.91 0.42 4 9/23/21 23:26 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.062 ND 0.91 0.28 4 9/23/21 23:26 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.069 ND 1.4 0.48 4 9/23/21 23:26 BRF 1,4-Dioxane ND 2.0 0.14 ND 7.2 0.49 4 9/23/21 23:26 BRF Ethanol 81 8.0 2.4 150 15 4.6 4 9/23/21 23:26 BRF Ethyl Acetate ND 2.0 1.2 L-03 ND 7.2 4.3 4 9/23/21 23:26 BRF Ethylbenzene 9.9 0.20 0.052 43 0.87 0.22 4 9/23/21 23:26 BRF 4-Ethyltoluene ND 0.20 0.062 ND 0.98 0.30 4 9/23/21 23:26 BRF Heptane ND 0.20 0.082 ND 0.82 0.34 4 9/23/21 23:26 BRF Hexachlorobutadiene ND 0.20 0.11 ND 2.1 1.2 4 9/23/21 23:26 BRF Hexane ND 8.0 0.66 ND 28 2.3 4 9/23/21 23:26 BRF 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 9/23/21 23:26 BRF Isopropanol ND 8.0 1.8 ND 20 4.5 4 9/23/21 23:26 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.080 ND 0.72 0.29 4 9/23/21 23:26 BRF Methylene Chloride 0.62 2.0 0.46 J 2.2 6.9 1.6 4 9/23/21 23:26 BRF 4-Methyl-2-pentanone (MIBK) ND 0.20 0.10 ND 0.82 0.42 4 9/23/21 23:26 BRF Naphthalene ND 0.20 0.13 ND 1.0 0.66 4 9/23/21 23:26 BRF Propene ND 8.0 0.67 ND 14 1.2 4 9/23/21 23:26 BRF Styrene 0.70 0.20 0.063 3.0 0.85 0.27 4 9/23/21 23:26 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.061 ND 1.4 0.42 4 9/23/21 23:26 BRF Page 7 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Charlotte, NC Sample Description/Location: Work Order: 2111198 Date Received: 9/20/2021 Sub Description/Location: Initial Vacuum(in Hg): -29 Field Sample #: SG-2 Canister ID: 2230 Final Vacuum(in Hg): -5 Sample ID: 21I1198-02 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.7 Sample Matrix: Soil Gas Flow Controller ID: 4309 Flow Controller Type: Fixed -Orifice Sampled: 9/17/2021 11:28 Sample Type: 5 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Tetrachloroethylene ND 0.20 0.059 ND 1.4 0.40 4 9/23/21 23:26 BRF Tetrahydrofuran ND 2.0 0.49 ND 5.9 1.5 4 9/23/21 23:26 BRF Toluene 1.3 0.20 0.084 4.8 0.75 0.32 4 9/23/21 23:26 BRF 1,2,4-Trichlorobenzene ND 0.20 0.14 ND 1.5 1.0 4 9/23/21 23:26 BRF 1, 1, 1 -Trichloroethane ND 0.20 0.092 ND 1.1 0.50 4 9/23/21 23:26 BRF 1,1,2-Trichloroethane ND 0.20 0.080 ND 1.1 0.43 4 9/23/21 23:26 BRF Trichloroethylene ND 0.20 0.074 ND 1.1 0.40 4 9/23/21 23:26 BRF Trichlorofluoromethane (Freon 11) 4.4 0.80 0.080 25 4.5 0.45 4 9/23/21 23:26 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.071 ND 6.1 0.54 4 9/23/21 23:26 BRF 1,2,4-Trimethylbenzene ND 0.20 0.059 ND 0.98 0.29 4 9/23/21 23:26 BRF 1,3,5-Trimethylbenzene ND 0.20 0.055 ND 0.98 0.27 4 9/23/21 23:26 BRF Vinyl Acetate ND 4.0 0.37 ND 14 1.3 4 9/23/21 23:26 BRF Vinyl Chloride ND 0.20 0.079 ND 0.51 0.20 4 9/23/21 23:26 BRF m&p-Xylene 31 0.40 0.11 130 1.7 0.48 4 9/23/21 23:26 BRF o-Xylene 9.1 0.20 0.054 40 0.87 0.23 4 9/23/21 23:26 BRF Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 96.7 70-130 9/23/21 23:26 Page 8 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Charlotte, NC Sample Description/Location: Work Order: 2111198 Date Received: 9/20/2021 Sub Description/Location: Initial Vacuum(in Hg): -21 Field Sample #: SG-3 Canister ID: 2524 Final Vacuum(in Hg): -5 Sample ID: 21I1198-03 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.2 Sample Matrix: Soil Gas Flow Controller ID: 4173 Flow Controller Type: Fixed -Orifice Sampled: 9/17/2021 11:02 Sample Type: 5 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 65 8.0 4.8 150 19 11 4 9/24/21 0:29 BRF Benzene 0.72 0.20 0.048 2.3 0.64 0.15 4 9/24/21 0:29 BRF Benzyl chloride ND 0.20 0.090 ND 1.0 0.47 4 9/24/21 0:29 BRF Bromodichloromethane ND 0.20 0.073 ND 1.3 0.49 4 9/24/21 0:29 BRF Bromoform ND 0.40 0.072 ND 4.1 0.74 4 9/24/21 0:29 BRF Bromomethane ND 0.20 0.16 ND 0.78 0.63 4 9/24/21 0:29 BRF 1,3-Butadiene ND 0.20 0.14 ND 0.44 0.31 4 9/24/21 0:29 BRF 2-Butanone (MEK) 20 8.0 0.66 60 24 2.0 4 9/24/21 0:29 BRF Carbon Disulfide ND 2.0 0.51 ND 6.2 1.6 4 9/24/21 0:29 BRF Carbon Tetrachloride 0.14 0.20 0.060 J 0.88 1.3 0.38 4 9/24/21 0:29 BRF Chlorobenzene ND 0.20 0.060 ND 0.92 0.27 4 9/24/21 0:29 BRF Chloroethane ND 0.20 0.15 ND 0.53 0.39 4 9/24/21 0:29 BRF Chloroform 0.66 0.20 0.048 3.2 0.98 0.24 4 9/24/21 0:29 BRF Chloromethane ND 0.40 0.082 ND 0.83 0.17 4 9/24/21 0:29 BRF Cyclohexane 7.3 0.20 0.13 25 0.69 0.46 4 9/24/21 0:29 BRF Dibromochloromethane ND 0.20 0.067 ND 1.7 0.57 4 9/24/21 0:29 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.056 ND 1.5 0.43 4 9/24/21 0:29 BRF 1,2-Dichlorobenzene ND 0.20 0.074 ND 1.2 0.44 4 9/24/21 0:29 BRF 1,3-Dichlorobenzene ND 0.20 0.048 ND 1.2 0.29 4 9/24/21 0:29 BRF 1,4-Dichlorobenzene ND 0.20 0.081 ND 1.2 0.49 4 9/24/21 0:29 BRF Dichlorodifluoromethane (Freon 12) 0.61 0.20 0.061 3.0 0.99 0.30 4 9/24/21 0:29 BRF 1,1-Dichloroethane ND 0.20 0.067 ND 0.81 0.27 4 9/24/21 0:29 BRF 1,2-Dichloroethane 0.91 0.20 0.073 3.7 0.81 0.30 4 9/24/21 0:29 BRF 1,1-Dichloroethylene ND 0.20 0.079 ND 0.79 0.31 4 9/24/21 0:29 BRF cis-1,2-Dichloroethylene ND 0.20 0.068 ND 0.79 0.27 4 9/24/21 0:29 BRF trans-1,2-Dichloroethylene ND 0.20 0.070 ND 0.79 0.28 4 9/24/21 0:29 BRF 1,2-Dichloropropane ND 0.20 0.072 ND 0.92 0.33 4 9/24/21 0:29 BRF cis- 1,3 -Dichloropropene ND 0.20 0.093 ND 0.91 0.42 4 9/24/21 0:29 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.062 ND 0.91 0.28 4 9/24/21 0:29 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.069 ND 1.4 0.48 4 9/24/21 0:29 BRF 1,4-Dioxane 2.9 2.0 0.14 11 7.2 0.49 4 9/24/21 0:29 BRF Ethanol 380 60 18 710 110 34 30 9/24/21 1:00 BRF Ethyl Acetate 36 2.0 1.2 L-03 130 7.2 4.3 4 9/24/21 0:29 BRF Ethylbenzene 11 0.20 0.052 49 0.87 0.22 4 9/24/21 0:29 BRF 4-Ethyltoluene ND 0.20 0.062 ND 0.98 0.30 4 9/24/21 0:29 BRF Heptane 0.70 0.20 0.082 2.9 0.82 0.34 4 9/24/21 0:29 BRF Hexachlorobutadiene ND 0.20 0.11 ND 2.1 1.2 4 9/24/21 0:29 BRF Hexane ND 8.0 0.66 ND 28 2.3 4 9/24/21 0:29 BRF 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 9/24/21 0:29 BRF Isopropanol 19 8.0 1.8 46 20 4.5 4 9/24/21 0:29 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.080 ND 0.72 0.29 4 9/24/21 0:29 BRF Methylene Chloride 1.9 2.0 0.46 J 6.6 6.9 1.6 4 9/24/21 0:29 BRF 4-Methyl-2-pentanone (MIBK) ND 0.20 0.10 ND 0.82 0.42 4 9/24/21 0:29 BRF Naphthalene 0.44 0.20 0.13 V-35 2.3 1.0 0.66 4 9/24/21 0:29 BRF Propene ND 8.0 0.67 ND 14 1.2 4 9/24/21 0:29 BRF Styrene 2.1 0.20 0.063 9.1 0.85 0.27 4 9/24/21 0:29 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.061 ND 1.4 0.42 4 9/24/21 0:29 BRF Page 9 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Charlotte, NC Sample Description/Location: Work Order: 2111198 Date Received: 9/20/2021 Sub Description/Location: Initial Vacuum(in Hg): -21 Field Sample #: SG-3 Canister ID: 2524 Final Vacuum(in Hg): -5 Sample ID: 21I1198-03 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.2 Sample Matrix: Soil Gas Flow Controller ID: 4173 Flow Controller Type: Fixed -Orifice Sampled: 9/17/2021 11:02 Sample Type: 5 min Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.20 0.059 ND 1.4 0.40 4 9/24/21 0:29 BRF Tetrahydrofuran 15 2.0 0.49 44 5.9 1.5 4 9/24/21 0:29 BRF Toluene 17 0.20 0.084 64 0.75 0.32 4 9/24/21 0:29 BRF 1,2,4-Trichlorobenzene ND 0.20 0.14 ND 1.5 1.0 4 9/24/21 0:29 BRF 1, 1, 1 -Trichloroethane ND 0.20 0.092 ND 1.1 0.50 4 9/24/21 0:29 BRF 1,1,2-Trichloroethane 1.0 0.20 0.080 5.7 1.1 0.43 4 9/24/21 0:29 BRF Trichloroethylene ND 0.20 0.074 ND 1.1 0.40 4 9/24/21 0:29 BRF Trichlorofluoromethane (Freon 11) 2.5 0.80 0.080 14 4.5 0.45 4 9/24/21 0:29 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.071 ND 6.1 0.54 4 9/24/21 0:29 BRF 1,2,4-Trimethylbenzene 0.88 0.20 0.059 4.3 0.98 0.29 4 9/24/21 0:29 BRF 1,3,5-Trimethylbenzene 0.25 0.20 0.055 1.2 0.98 0.27 4 9/24/21 0:29 BRF Vinyl Acetate ND 4.0 0.37 ND 14 1.3 4 9/24/21 0:29 BRF Vinyl Chloride ND 0.20 0.079 ND 0.51 0.20 4 9/24/21 0:29 BRF m&p-Xylene 30 0.40 0.11 130 1.7 0.48 4 9/24/21 0:29 BRF o-Xylene 7.0 0.20 0.054 31 0.87 0.23 4 9/24/21 0:29 BRF Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 97.0 70-130 9/24/21 0:29 4-Bromofluorobenzene (1) 98.5 70-130 9/24/21 1:00 Page 10 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Charlotte, NC Sample Description/Location: Work Order: 2111198 Date Received: 9/20/2021 Sub Description/Location: Initial Vacuum(in Hg): -28 Field Sample #: SG-4 Canister ID: 2542 Final Vacuum(in Hg): -5 Sample ID: 21I1198-04 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.4 Sample Matrix: Soil Gas Flow Controller ID: 4191 Flow Controller Type: Fixed -Orifice Sampled: 9/17/2021 10:26 Sample Type: 5 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 35 8.0 4.8 84 19 11 4 9/24/21 1:59 BRF Benzene 0.34 0.20 0.048 1.1 0.64 0.15 4 9/24/21 1:59 BRF Benzyl chloride ND 0.20 0.090 ND 1.0 0.47 4 9/24/21 1:59 BRF Bromodichloromethane ND 0.20 0.073 ND 1.3 0.49 4 9/24/21 1:59 BRF Bromoform ND 0.20 0.072 ND 2.1 0.74 4 9/24/21 1:59 BRF Bromomethane ND 0.20 0.16 ND 0.78 0.63 4 9/24/21 1:59 BRF 1,3-Butadiene ND 0.20 0.14 ND 0.44 0.31 4 9/24/21 1:59 BRF 2-Butanone (MEK) 4.5 8.0 0.66 J 13 24 2.0 4 9/24/21 1:59 BRF Carbon Disulfide ND 2.0 0.51 ND 6.2 1.6 4 9/24/21 1:59 BRF Carbon Tetrachloride ND 0.20 0.060 ND 1.3 0.38 4 9/24/21 1:59 BRF Chlorobenzene ND 0.20 0.060 ND 0.92 0.27 4 9/24/21 1:59 BRF Chloroethane ND 0.20 0.15 ND 0.53 0.39 4 9/24/21 1:59 BRF Chloroform 0.26 0.20 0.048 1.3 0.98 0.24 4 9/24/21 1:59 BRF Chloromethane ND 0.40 0.082 ND 0.83 0.17 4 9/24/21 1:59 BRF Cyclohexane 4.9 0.20 0.13 17 0.69 0.46 4 9/24/21 1:59 BRF Dibromochloromethane ND 0.20 0.067 ND 1.7 0.57 4 9/24/21 1:59 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.056 ND 1.5 0.43 4 9/24/21 1:59 BRF 1,2-Dichlorobenzene ND 0.20 0.074 ND 1.2 0.44 4 9/24/21 1:59 BRF 1,3-Dichlorobenzene ND 0.20 0.048 ND 1.2 0.29 4 9/24/21 1:59 BRF 1,4-Dichlorobenzene ND 0.20 0.081 ND 1.2 0.49 4 9/24/21 1:59 BRF Dichlorodifluoromethane (Freon 12) 12 0.20 0.061 59 0.99 0.30 4 9/24/21 1:59 BRF 1,1-Dichloroethane ND 0.20 0.067 ND 0.81 0.27 4 9/24/21 1:59 BRF 1,2-Dichloroethane ND 0.20 0.073 ND 0.81 0.30 4 9/24/21 1:59 BRF 1,1-Dichloroethylene ND 0.20 0.079 ND 0.79 0.31 4 9/24/21 1:59 BRF cis-1,2-Dichloroethylene ND 0.20 0.068 ND 0.79 0.27 4 9/24/21 1:59 BRF trans-1,2-Dichloroethylene ND 0.20 0.070 ND 0.79 0.28 4 9/24/21 1:59 BRF 1,2-Dichloropropane ND 0.20 0.072 ND 0.92 0.33 4 9/24/21 1:59 BRF cis- 1,3 -Dichloropropene ND 0.20 0.093 ND 0.91 0.42 4 9/24/21 1:59 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.062 ND 0.91 0.28 4 9/24/21 1:59 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.069 ND 1.4 0.48 4 9/24/21 1:59 BRF 1,4-Dioxane ND 2.0 0.14 ND 7.2 0.49 4 9/24/21 1:59 BRF Ethanol 150 8.0 2.4 290 15 4.6 4 9/24/21 1:59 BRF Ethyl Acetate ND 2.0 1.2 L-03 ND 7.2 4.3 4 9/24/21 1:59 BRF Ethylbenzene 5.6 0.20 0.052 24 0.87 0.22 4 9/24/21 1:59 BRF 4-Ethyltoluene ND 0.20 0.062 ND 0.98 0.30 4 9/24/21 1:59 BRF Heptane ND 0.20 0.082 ND 0.82 0.34 4 9/24/21 1:59 BRF Hexachlorobutadiene ND 0.20 0.11 ND 2.1 1.2 4 9/24/21 1:59 BRF Hexane ND 8.0 0.66 ND 28 2.3 4 9/24/21 1:59 BRF 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 9/24/21 1:59 BRF Isopropanol 3.1 8.0 1.8 J 7.6 20 4.5 4 9/24/21 1:59 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.080 ND 0.72 0.29 4 9/24/21 1:59 BRF Methylene Chloride ND 2.0 0.46 ND 6.9 1.6 4 9/24/21 1:59 BRF 4-Methyl-2-pentanone (MIBK) ND 0.20 0.10 ND 0.82 0.42 4 9/24/21 1:59 BRF Naphthalene 0.32 0.20 0.13 V-35 1.7 1.0 0.66 4 9/24/21 1:59 BRF Propene ND 8.0 0.67 ND 14 1.2 4 9/24/21 1:59 BRF Styrene 0.58 0.20 0.063 2.5 0.85 0.27 4 9/24/21 1:59 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.061 ND 1.4 0.42 4 9/24/21 1:59 BRF Page 11 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Charlotte, NC Sample Description/Location: Work Order: 2111198 Date Received: 9/20/2021 Sub Description/Location: Initial Vacuum(in Hg): -28 Field Sample #: SG-4 Canister ID: 2542 Final Vacuum(in Hg): -5 Sample ID: 21I1198-04 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.4 Sample Matrix: Soil Gas Flow Controller ID: 4191 Flow Controller Type: Fixed -Orifice Sampled: 9/17/2021 10:26 Sample Type: 5 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Tetrachloroethylene 1.7 0.20 0.059 12 1.4 0.40 4 9/24/21 1:59 BRF Tetrahydrofuran ND 2.0 0.49 ND 5.9 1.5 4 9/24/21 1:59 BRF Toluene 1.1 0.20 0.084 4.0 0.75 0.32 4 9/24/21 1:59 BRF 1,2,4-Trichlorobenzene ND 0.20 0.14 ND 1.5 1.0 4 9/24/21 1:59 BRF 1, 1, 1 -Trichloroethane ND 0.20 0.092 ND 1.1 0.50 4 9/24/21 1:59 BRF 1,1,2-Trichloroethane ND 0.20 0.080 ND 1.1 0.43 4 9/24/21 1:59 BRF Trichloroethylene ND 0.20 0.074 ND 1.1 0.40 4 9/24/21 1:59 BRF Trichlorofluoromethane (Freon 11) 140 0.80 0.080 790 4.5 0.45 4 9/24/21 1:59 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.071 ND 6.1 0.54 4 9/24/21 1:59 BRF 1,2,4-Trimethylbenzene ND 0.20 0.059 ND 0.98 0.29 4 9/24/21 1:59 BRF 1,3,5-Trimethylbenzene ND 0.20 0.055 ND 0.98 0.27 4 9/24/21 1:59 BRF Vinyl Acetate ND 4.0 0.37 ND 14 1.3 4 9/24/21 1:59 BRF Vinyl Chloride ND 0.20 0.079 ND 0.51 0.20 4 9/24/21 1:59 BRF m&p-Xylene 21 0.40 0.11 90 1.7 0.48 4 9/24/21 1:59 BRF o-Xylene 7.4 0.20 0.054 32 0.87 0.23 4 9/24/21 1:59 BRF Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 97.8 70-130 9/24/21 1:59 Page 12 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Charlotte, NC Sample Description/Location: Work Order: 2111198 Date Received: 9/20/2021 Sub Description/Location: Initial Vacuum(in Hg): -28 Field Sample #: SGDUP Canister ID: 2240 Final Vacuum(in Hg): -5 Sample ID: 21I1198-05 Canister Size: 1 liter Receipt Vacuum(in Hg): -6.3 Sample Matrix: Soil Gas Flow Controller ID: 4075 Flow Controller Type: Fixed -Orifice Sampled: 9/17/2021 00:00 Sample Type: 5 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 65 8.0 4.8 150 19 11 4 9/24/21 3:00 BRF Benzene 0.20 0.20 0.048 J 0.63 0.64 0.15 4 9/24/21 3:00 BRF Benzyl chloride ND 0.20 0.090 ND 1.0 0.47 4 9/24/21 3:00 BRF Bromodichloromethane ND 0.20 0.073 ND 1.3 0.49 4 9/24/21 3:00 BRF Bromoform ND 0.20 0.072 ND 2.1 0.74 4 9/24/21 3:00 BRF Bromomethane ND 0.20 0.16 ND 0.78 0.63 4 9/24/21 3:00 BRF 1,3-Butadiene ND 0.20 0.14 ND 0.44 0.31 4 9/24/21 3:00 BRF 2-Butanone (MEK) 3.3 8.0 0.66 J 9.8 24 2.0 4 9/24/21 3:00 BRF Carbon Disulfide ND 2.0 0.51 ND 6.2 1.6 4 9/24/21 3:00 BRF Carbon Tetrachloride ND 0.20 0.060 ND 1.3 0.38 4 9/24/21 3:00 BRF Chlorobenzene ND 0.20 0.060 ND 0.92 0.27 4 9/24/21 3:00 BRF Chloroethane ND 0.20 0.15 ND 0.53 0.39 4 9/24/21 3:00 BRF Chloroform 0.63 0.20 0.048 3.1 0.98 0.24 4 9/24/21 3:00 BRF Chloromethane ND 0.40 0.082 ND 0.83 0.17 4 9/24/21 3:00 BRF Cyclohexane ND 0.20 0.13 ND 0.69 0.46 4 9/24/21 3:00 BRF Dibromochloromethane ND 0.20 0.067 ND 1.7 0.57 4 9/24/21 3:00 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.056 ND 1.5 0.43 4 9/24/21 3:00 BRF 1,2-Dichlorobenzene ND 0.20 0.074 ND 1.2 0.44 4 9/24/21 3:00 BRF 1,3-Dichlorobenzene ND 0.20 0.048 ND 1.2 0.29 4 9/24/21 3:00 BRF 1,4-Dichlorobenzene ND 0.20 0.081 ND 1.2 0.49 4 9/24/21 3:00 BRF Dichlorodifluoromethane (Freon 12) 13 0.20 0.061 66 0.99 0.30 4 9/24/21 3:00 BRF 1,1-Dichloroethane ND 0.20 0.067 ND 0.81 0.27 4 9/24/21 3:00 BRF 1,2-Dichloroethane ND 0.20 0.073 ND 0.81 0.30 4 9/24/21 3:00 BRF 1,1-Dichloroethylene ND 0.20 0.079 ND 0.79 0.31 4 9/24/21 3:00 BRF cis-1,2-Dichloroethylene ND 0.20 0.068 ND 0.79 0.27 4 9/24/21 3:00 BRF trans-1,2-Dichloroethylene ND 0.20 0.070 ND 0.79 0.28 4 9/24/21 3:00 BRF 1,2-Dichloropropane ND 0.20 0.072 ND 0.92 0.33 4 9/24/21 3:00 BRF cis- 1,3 -Dichloropropene ND 0.20 0.093 ND 0.91 0.42 4 9/24/21 3:00 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.062 ND 0.91 0.28 4 9/24/21 3:00 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.069 ND 1.4 0.48 4 9/24/21 3:00 BRF 1,4-Dioxane ND 2.0 0.14 ND 7.2 0.49 4 9/24/21 3:00 BRF Ethanol 260 60 18 500 110 34 30 9/24/21 3:31 BRF Ethyl Acetate 1.6 2.0 1.2 L-03, J 5.8 7.2 4.3 4 9/24/21 3:00 BRF Ethylbenzene ND 0.20 0.052 ND 0.87 0.22 4 9/24/21 3:00 BRF 4-Ethyltoluene ND 0.20 0.062 ND 0.98 0.30 4 9/24/21 3:00 BRF Heptane ND 0.20 0.082 ND 0.82 0.34 4 9/24/21 3:00 BRF Hexachlorobutadiene ND 0.20 0.11 ND 2.1 1.2 4 9/24/21 3:00 BRF Hexane ND 8.0 0.66 ND 28 2.3 4 9/24/21 3:00 BRF 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 9/24/21 3:00 BRF Isopropanol 17 8.0 1.8 43 20 4.5 4 9/24/21 3:00 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.080 ND 0.72 0.29 4 9/24/21 3:00 BRF Methylene Chloride 1.7 2.0 0.46 J 5.8 6.9 1.6 4 9/24/21 3:00 BRF 4-Methyl-2-pentanone (MIBK) ND 0.20 0.10 ND 0.82 0.42 4 9/24/21 3:00 BRF Naphthalene ND 0.20 0.13 ND 1.0 0.66 4 9/24/21 3:00 BRF Propene ND 8.0 0.67 ND 14 1.2 4 9/24/21 3:00 BRF Styrene ND 0.20 0.063 ND 0.85 0.27 4 9/24/21 3:00 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.061 ND 1.4 0.42 4 9/24/21 3:00 BRF Page 13 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Charlotte, NC Sample Description/Location: Work Order: 2111198 Date Received: 9/20/2021 Sub Description/Location: Initial Vacuum(in Hg): -28 Field Sample #: SGDUP Canister ID: 2240 Final Vacuum(in Hg): -5 Sample ID: 21I1198-05 Canister Size: 1 liter Receipt Vacuum(in Hg): -6.3 Sample Matrix: Soil Gas Flow Controller ID: 4075 Flow Controller Type: Fixed -Orifice Sampled: 9/17/2021 00:00 Sample Type: 5 min Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.20 0.059 ND 1.4 0.40 4 9/24/21 3:00 BRF Tetrahydrofuran 5.0 2.0 0.49 15 5.9 1.5 4 9/24/21 3:00 BRF Toluene 1.4 0.20 0.084 5.2 0.75 0.32 4 9/24/21 3:00 BRF 1,2,4-Trichlorobenzene ND 0.20 0.14 ND 1.5 1.0 4 9/24/21 3:00 BRF 1, 1, 1 -Trichloroethane ND 0.20 0.092 ND 1.1 0.50 4 9/24/21 3:00 BRF 1,1,2-Trichloroethane ND 0.20 0.080 ND 1.1 0.43 4 9/24/21 3:00 BRF Trichloroethylene ND 0.20 0.074 ND 1.1 0.40 4 9/24/21 3:00 BRF Trichlorofluoromethane (Freon 11) 5.0 0.80 0.080 28 4.5 0.45 4 9/24/21 3:00 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.071 ND 6.1 0.54 4 9/24/21 3:00 BRF 1,2,4-Trimethylbenzene ND 0.20 0.059 ND 0.98 0.29 4 9/24/21 3:00 BRF 1,3,5-Trimethylbenzene ND 0.20 0.055 ND 0.98 0.27 4 9/24/21 3:00 BRF Vinyl Acetate ND 4.0 0.37 ND 14 1.3 4 9/24/21 3:00 BRF Vinyl Chloride ND 0.20 0.079 ND 0.51 0.20 4 9/24/21 3:00 BRF m&p-Xylene 25 0.40 0.11 110 1.7 0.48 4 9/24/21 3:00 BRF o-Xylene 20 0.20 0.054 85 0.87 0.23 4 9/24/21 3:00 BRF Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 90.4 70-130 9/24/21 3:31 4-Bromofluorobenzene (1) 96.7 70-130 9/24/21 3:00 Page 14 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Sample Extraction Data Prep Method: TO-15 Prep -EPA TO-15 Lab Number [Field ID1 Batch Pressure Dilution Pre Dilution Pre-Dil Initial mL Pre-Dil Final mL Default Injection mL Actual Injection mL Date 21I1198-01 [SG-1] B290913 1.5 1 N/A 1000 200 75 09/23/21 2111198-OIRE1 [SG-1] B290913 1.5 1 N/A 1000 200 10 09/23/21 21I1198-02 [SG-2] B290913 1.5 1 N/A 1000 200 75 09/23/21 21I1198-03 [SG-3] B290913 1.5 1 N/A 1000 200 75 09/23/21 21I1198-03RE1 [SG-3] B290913 1.5 1 N/A 1000 200 10 09/23/21 2111198-04 [SG-4] B290913 1.5 1 N/A 1000 200 75 09/23/21 21I1198-05 [SG-DUP] B290913 1.5 1 N/A 1000 200 75 09/23/21 2111198-05RE1 [SG-DUP] B290913 1.5 1 N/A 1000 200 10 09/23/21 Page 15 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua Batch B290913 - TO-15 Prep Blank (B290913-BLKl) Prepared & Analyzed: 09/23/21 Acetone ND 0.80 Benzene ND 0.020 Benzyl chloride ND 0.020 Bromodichloromethane ND 0.020 Bromoform ND 0.020 Bromomethane ND 0.020 113-Butadiene ND 0.020 2-Butanone (MEK) ND 0.80 Carbon Disulfide ND 0.20 Carbon Tetrachloride 0.0068 0.020 J Chlorobenzene ND 0.020 Chloroethane ND 0.020 Chloroform ND 0.020 Chloromethane ND 0.040 Cyclohexane ND 0.020 Dibromochloromethane ND 0.020 1,2-Dibromoethane (EDB) ND 0.020 1,2-Dichlorobenzene ND 0.020 1,3-Dichlorobenzene ND 0.020 114-Dichlorobenzene ND 0.020 Dichlorodifluoromethane (Freon 12) ND 0.020 1,1-Dichloroethane ND 0.020 1,2-Dichloroethane ND 0.020 1,1-Dichloroethylene ND 0.020 cis-1,2-Dichloroethylene ND 0.020 trans-1,2-Dichloroethylene ND 0.020 1,2-Dichloropropane ND 0.020 cis- 1,3 -Dichloropropene ND 0.020 trans- l,3-Dichloropropene ND 0.020 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane ND 0.020 (Freon 114) 114-Dioxane ND 0.20 Ethanol ND 0.80 Ethyl Acetate ND 0.20 L-03 Ethylbenzene 0.0084 0.020 J 4-Ethyltoluene ND 0.020 Heptane ND 0.020 Hexachlorobutadiene ND 0.020 Hexane ND 0.80 2-Hexanone (MBK) ND 0.020 Isopropanol ND 0.80 Methyl tert-Butyl Ether (MTBE) ND 0.020 Methylene Chloride ND 0.20 4-Methyl-2-pentanone (MIBK) ND 0.020 Naphthalene ND 0.020 Propene ND 0.80 Styrene ND 0.020 Page 16 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B290913 - TO-15 Prep Blank (B290913-BLKI) Prepared & Analyzed: 09/23/21 1,1,2,2-Tetrachloroethane ND 0.020 Tetrachloroethylene ND 0.020 Tetrahydrofuran ND 0.20 Toluene ND 0.020 1,2,4-Trichlorobenzene ND 0.020 1, 1, 1 -Trichloroethane ND 0.020 1,1,2-Trichloroethane ND 0.020 Trichloroethylene ND 0.020 Trichlorofluoromethane (Freon 11) ND 0.080 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon ND 0.080 113) 1,2,4-Trimethylbenzene ND 0.020 1,3,5-Trimethylbenzene ND 0.020 Vinyl Acetate ND 0.40 Vinyl Chloride ND 0.020 m&p-Xylene 0.018 0.040 1 o-Xylene 0.0084 0.020 J Surrogate: 4-Bromofluorobenzene (1) LCS (B290913-BSI) 7.58 8.00 94.7 Prepared & Analyzed: 09/23/21 70-130 Acetone 4.79 5.00 95.8 70-130 Benzene 4.62 5.00 92.3 70-130 Benzyl chloride 5.16 5.00 103 70-130 Bromodichloromethane 4.75 5.00 95.0 70-130 Bromoform 5.40 5.00 108 70-130 Bromomethane 5.10 5.00 102 70-130 1,3-Butadiene 4.76 5.00 95.2 70-130 2-Butanone (MEK) 4.74 5.00 94.8 70-130 Carbon Disulfide 5.74 5.00 115 70-130 Carbon Tetrachloride 4.67 5.00 93.4 70-130 Chlorobenzene 4.64 5.00 92.7 70-130 Chloroethane 5.25 5.00 105 70-130 Chloroform 5.00 5.00 100 70-130 Chloromethane 4.75 5.00 95.0 70-130 Cyclohexane 4.43 5.00 88.6 70-130 Dibromochloromethane 4.82 5.00 96.5 70-130 1,2-Dibromoethane (EDB) 4.77 5.00 95.5 70-130 1,2-Dichlorobenzene 5.39 5.00 108 70-130 1,3-Dichlorobenzene 5.34 5.00 107 70-130 1,4-Dichlorobenzene 5.13 5.00 103 70-130 Dichlorodifluoromethane (Freon 12) 5.24 5.00 105 70-130 1,1-Dichloroethane 4.86 5.00 97.1 70-130 1,2-Dichloroethane 4.79 5.00 95.9 70-130 1,1-Dichloroethylene 4.97 5.00 99.3 70-130 cis-1,2-Dichloroethylene 4.90 5.00 97.9 70-130 trans-1,2-Dichloroethylene 4.78 5.00 95.5 70-130 1,2-Dichloropropane 4.55 5.00 91.0 70-130 Page 17 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B290913 - TO-15 Prep LCS (B290913-BS1) Prepared & Analyzed: 09/23/21 cis-1,3-Dichloropropene 5.01 5.00 100 70-130 trans-1,3-Dichloropropene 4.74 5.00 94.8 70-130 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane 4.65 5.00 93.0 70-130 (Freon 114) 1,4-Dioxane 5.16 5.00 103 70-130 Ethanol 6.28 5.00 126 70-130 Ethyl Acetate 3.49 5.00 69.8 * 70-130 L-02 Ethylbenzene 4.89 5.00 97.9 70-130 4-Ethyltoluene 5.22 5.00 104 70-130 Heptane 3.84 5.00 76.7 70-130 Hexachlorobutadiene 5.39 5.00 108 70-130 Hexane 4.86 5.00 97.3 70-130 2-Hexanone (MBK) 5.07 5.00 101 70-130 Isopropanol 4.01 5.00 80.2 70-130 Methyl tert-Butyl Ether (MTBE) 4.70 5.00 93.9 70-130 Methylene Chloride 4.86 5.00 97.2 70-130 4-Methyl-2-pentanone (MIBK) 4.92 5.00 98.5 70-130 Naphthalene 5.64 5.00 113 70-130 Propene 5.04 5.00 101 70-130 Styrene 5.07 5.00 101 70-130 1,1,2,2-Tetrachloroethane 5.05 5.00 101 70-130 Tetrachloroethylene 4.99 5.00 99.7 70-130 Tetrahydrofuran 4.50 5.00 90.0 70-130 Toluene 4.61 5.00 92.1 70-130 1,2,4-Trichlorobenzene 5.67 5.00 113 70-130 1, 1, 1 -Trichloroethane 4.76 5.00 95.2 70-130 1,1,2-Trichloroethane 4.52 5.00 90.5 70-130 Trichloroethylene 5.10 5.00 102 70-130 Trichlorofluoromethane (Freon 11) 5.19 5.00 104 70-130 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 5.97 5.00 119 70-130 113) 1,2,4-Trimethylbenzene 5.07 5.00 101 70-130 1,3,5-Trimethylbenzene 4.86 5.00 97.2 70-130 Vinyl Acetate 6.59 5.00 132 * 70-130 L-01, V-3( Vinyl Chloride 5.37 5.00 107 70-130 m&p-Xylene 9.61 10.0 96.1 70-130 o-Xylene 5.06 5.00 101 70-130 Surrogate: 4-Bromofluorobenzene (1) 8.19 8.00 102 70-130 Page 18 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 ` TEL. 413/525-2332 Note: Blank Subtraction is not performed unless otherwise noted FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. t Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level RL Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference LCS Laboratory Control Sample LCS Dup Duplicate Laboratory Control Sample MS Matrix Spike Sample MS Dup Duplicate Matrix Spike Sample REC Recovery QC Quality Control ppbv Parts per billion volume EPA United States Environmental Protection Agency % REC Percent Recovery ND Not Detected N/A Not Applicable DL Detection Limit NC Not Calculated LFB/LCS Lab Fortified Blank/Lab Control Sample ORP Oxidation -Reduction Potential wet Not dry weight corrected % wt Percent weight Kg Kilogram g Gram mg Milligram µg Microgram ng Nanogram L Liter mL Milliliter µL Microliter m3 Cubic Meter EPH Extractable Petroleum Hydrocarbons VPH Volatile Petroleum Hydrocarbons APH Air Petroleum Hydrocarbons FID Flame Ionization Detector PID Photo Ionization Detector Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). L-01 Laboratory fortified blank/laboratory control sample recovery outside of control limits. Data validation is not affected since all results are "not detected" for all samples in this batch for this compound and bias is on the high side. L-03 Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this compound is likely to be biased on the low side. V-31 Internal Standard is outside of control criteria for this sample. The analytes being reported for this analytical run are not affected by this I.S. being outside of control criteria. Data validation is not affected. V-35 Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this compound. Reported result is estimated. V-36 Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. Page 19 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 TPH Thomas P. Hnitecki RLF Rebecca Faust STATION PDF Management Station KKM Kerry K. McGee BRF Brittany R. Fisk ANALYST Page 20 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Initial Cal Check (S063338-ICV1) Lab File ID: K21A259025.13 Analyzed: 09/16/21 23:09 Bromochloromethane (1) 65004 2.989 65617 2.992 99 60 - 140 -0.0030 +/-0.50 1,4-Difluorobenzene(1) 208463 3.592 200888 3.595 104 60-140 -0.0030 +/-0.50 Chlorobenzene-d5(1) 167501 5.185 162778 5.188 103 60-140 -0.0030 +/-0.50 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Calibration Check (S063579-CCV1) Lab File ID: K21A266004.13 Analyzed: 09/23/21 09:38 Bromochloromethane (1) 56022 2.992 65617 2.992 85 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 171584 3.595 200888 3.595 85 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 145496 5.188 162778 5.188 89 60-140 0.0000 +/-0.50 LCS (B290913-BS1 ) Lab File ID: K21A266005.13 Analyzed: 09/23/21 10:10 Bromochloromethane (1) 56833 2.992 56022 2.992 101 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 180913 3.598 171584 3.595 105 60-140 0.0030 +/-0.50 Chlorobenzene-d5(1) 144330 5.188 145496 5.188 99 60-140 0.0000 +/-0.50 Blank (B290913-BLK1) Lab File ID: K21A266008.13 Analyzed: 09/23/21 12:01 Bromochloromethane (1) 62952 2.992 56022 2.992 112 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 180763 3.598 171584 3.595 105 60-140 0.0030 +/-0.50 Chlorobenzene-d5(1) 155964 5.188 145496 5.188 107 60-140 0.0000 +/-0.50 SG-1 (21I1198-01) Lab File ID: K21A266020.13 Analyzed: 09/23/21 21:55 Bromochloromethane (1) 63518 2.995 56022 2.992 113 60 - 140 0.0030 +/-0.50 1,4-Difluorobenzene(1) 189972 3.598 171584 3.595 ill 60-140 0.0030 +/-0.50 Chlorobenzene-d5(1) 166188 5.188 145496 5.188 114 60-140 0.0000 +/-0.50 SG-1 (21I1198-01RE1) Lab File ID: K2IA266021.13 Analyzed: 09/23/21 22:26 Bromochloromethane (1) 72441 2.992 56022 2.992 129 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 242040 3.598 171584 3.595 141 60-140 0.0030 +/-0.50 Chlorobenzene-d5(1) 201355 5.188 145496 5.188 138 60-140 0.0000 +/-0.50 SG-2 (21I1198-02) Lab File ID: K21A266023.1) Analyzed: 09/23/21 23:26 Bromochloromethane (1) 69927 2.996 56022 2.992 125 60 - 140 0.0040 +/-0.50 1,4-Difluorobenzene(1) 230428 3.598 171584 3.595 134 60-140 0.0030 +/-0.50 Chlorobenzene-d5(1) 194707 5.188 145496 5.188 134 60-140 0.0000 +/-0.50 SG-3 (21I1198-03) Lab File ID: K21A266025.13 Analyzed: 09/24/21 00:29 Bromochloromethane (1) 63330 2.991 56022 2.992 113 60 - 140 -0.0010 +/-0.50 1,4-Difluorobenzene(1) 224321 3.597 171584 3.595 131 60-140 0.0020 +/-0.50 Chlorobenzene-d5(1) 173437 5.187 145496 5.188 119 60-140 -0.0010 +/-0.50 Page 21 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q SG-3 (21I1198-03RE1) Lab File ID: K21A266026.D Analyzed: 09/24/21 01:00 Bromochloromethane (1) 64020 2.996 56022 2.992 114 60 - 140 0.0040 +/-0.50 1,4-Difluorobenzene(1) 198181 3.598 171584 3.595 116 60-140 0.0030 +/-0.50 Chlorobenzene-d5(1) 174214 5.188 145496 5.188 120 60-140 0.0000 +/-0.50 SG4 (21I1198-04) Lab File ID: K21A266028.D Analyzed: 09/24/21 01:59 Bromochloromethane (1) 60670 2.992 56022 2.992 108 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 191255 3.598 171584 3.595 111 60-140 0.0030 +/-0.50 Chlorobenzene-d5(1) 160045 5.188 145496 5.188 110 60-140 0.0000 +/-0.50 SG-DUP (21I1198-05) Lab File ID: K21A266030.D Analyzed: 09/24/21 03:00 Bromochloromethane (1) 57656 2.996 56022 2.992 103 60 - 140 0.0040 +/-0.50 1,4-Difluorobenzene(1) 174239 3.598 171584 3.595 102 60-140 0.0030 +/-0.50 Chlorobenzene-d5(1) 156034 5.188 145496 5.188 107 60-140 0.0000 +/-0.50 SG-DUP (21I1198-05RE1) Lab File ID: K21A26603 LD Analyzed: 09/24/21 03:31 Bromochloromethane (1) 66746 2.996 56022 2.992 119 60 - 140 0.0040 +/-0.50 1,4-Difluorobenzene(1) 216606 3.598 171584 3.595 126 60-140 0.0030 +/-0.50 Chlorobenzene-d5(1) 190388 5.188 145496 5.188 131 60-140 0.0000 +/-0.50 Page 22 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 5063579-CCV 1 COMPOUND TYPE. CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) Acetone A 5.00 5.18 1.044997 1.08246 3.6 30 Benzene A 5.00 5.12 0.6772546 0.6939295 2.5 30 Benzyl chloride A 5.00 5.62 0.4517045 0.5074724 12.3 30 Bromodichloromethane A 5.00 5.36 0.4576082 0.4909549 7.3 30 Bromoform A 5.00 5.86 0.4225807 0.4956287 17.3 30 Bromomethane A 5.00 5.60 0.7358094 0.8248188 12.1 30 1,3-Butadiene A 5.00 5.25 0.6122438 0.643233 5.1 30 2-Butanone(MEK) A 5.00 4.75 1.117205 1.061469 -5.0 30 Carbon Disulfide A 5.00 6.02 1.700674 2.049052 20.5 30 Carbon Tetrachloride A 5.00 5.20 0.4399405 0.4575998 4.0 30 Chlorobenzene A 5.00 5.02 0.6710772 0.673844 0.4 30 Chloroethane A 5.00 5.44 0.4322339 0.4702724 8.8 30 Chloroform A 5.00 5.35 1.383001 1.480675 7.1 30 Chloromethane A 5.00 5.34 0.6957364 0.7428225 6.8 30 Cyclohexane A 5.00 4.97 0.2863864 0.2848284 -0.5 30 Dibromochloromethane A 5.00 5.24 0.5392756 0.565041 4.8 30 1,2-Dibromoethane (EDB) A 5.00 5.08 0.4882235 0.4959477 1.6 30 1,2-Dichlorobenzene A 5.00 5.63 0.5583295 0.6290537 12.7 30 1,3-Dichlorobenzene A 5.00 5.42 0.3904983 0.4236872 8.5 30 1,4-Dichlorobenzene A 5.00 5.28 0.6060934 0.6397647 5.6 30 Dichlorodifluoromethane (Freon 12) A 5.00 5.73 2.131798 2.441955 14.5 30 1,1-Dichloroethane A 5.00 5.32 1.070749 1.138524 6.3 30 1,2-Dichloroethane A 5.00 5.05 0.850621 0.8595195 1.0 30 1,1-Dichloroethylene A 5.00 5.28 1.199799 1.268187 5.7 30 cis-1,2-Dichloroethylene A 5.00 5.07 0.8960317 0.9092999 1.5 30 trans-1,2-Dichloroethylene A 5.00 5.33 0.9105593 0.9705616 6.6 30 1,2-Dichloropropane A 5.00 4.98 0.2471363 0.245981 -0.5 30 cis-1,3-Dichloropropene A 5.00 4.68 0.282988 0.2650783 -6.3 30 trans- l,3-Dichloropropene A 5.00 5.01 0.3201369 0.3209344 0.2 30 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane (Freon 1 A 5.00 5.44 2.193098 2.385434 8.8 30 1,4-Dioxane A 5.00 5.70 0.1252425 0.14268 13.9 30 Ethanol A 5.00 5.64 0.1614241 0.182157 12.8 30 Ethyl Acetate A 5.00 4.96 0.2630812 0.2608118 -0.9 30 Ethylbenzene A 5.00 5.21 1.130441 1.177489 4.2 30 4-Ethyltoluene A 5.00 5.54 1.136131 1.258239 10.7 30 Heptane A 5.00 4.64 0.1870834 0.1737132 -7.1 30 Hexachlorobutadiene A 5.00 5.52 0.353338 0.3902348 10A 30 Hexane L 5.00 5.39 0.5879851 0.6421763 7.9 30 Page 23 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 5063579-CCV 1 COMPOUND TYPE CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) 2-Hexanone (MBK) A 5.00 5.23 0.4582989 0.4791664 4.6 30 Isopropanol A 5.00 5.38 1.230091 1.322995 7.6 30 Methyl tert-Butyl Ether (MTBE) A 5.00 5.11 1.735778 1.775074 2.3 30 Methylene Chloride A 5.00 5.32 0.7520661 0.8004855 6.4 30 4-Methyl-2-pentanone (MI13K) A 5.00 5.24 0.1956749 0.2052779 4.9 30 Naphthalene A 5.00 5.40 0.9756151 1.052873 7.9 30 Propene A 5.00 5.68 0.5977407 0.6789047 13.6 30 Styrene A 5.00 5.53 0.6328158 0.6998515 10.6 30 1,1,2,2-Tetrachloroethane A 5.00 5.34 0.6582366 0.7023368 6.7 30 Tetrachloroethylene A 5.00 5.41 0.3934633 0.4257657 8.2 30 Tetrahydroforan A 5.00 4.92 0.6580954 0.6470601 -1.7 30 Toluene A 5.00 5.04 0.959144 0.9665145 0.8 30 1,2,4-Trichlorobenzene A 5.00 5.65 0.375898 0.4248529 13.0 30 1, 1, 1 -Trichloroethane A 5.00 5.56 0.471714 0.5248042 11.3 30 1,1,2-Trichloroethane A 5.00 4.67 0.3462991 0.3232749 -6.6 30 Trichloroethylene A 5.00 5.70 0.2556787 0.2913931 14.0 30 Trichlorofluoromethane(Freon 11) A 5.00 5.62 1.972353 2.215016 12.3 30 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 11 A 5.00 5.74 1.00369 1.151776 14.8 30 1,2,4-Trimethylbenzene A 5.00 5.41 0.9612681 1.039688 8.2 30 1,3,5-Trimethylbenzene A 5.00 5.41 0.7473243 0.8087645 8.2 30 Vinyl Acetate A 5.00 4.69 0.8051633 0.7551034 -6.2 30 Vinyl Chloride A 5.00 5.55 0.7945618 0.8816536 11.0 30 m&p-Xylene A 10.0 10.3 0.9266552 0.9567108 3.2 30 o-Xylene A 5.00 5.38 0.8546217 0.9186782 7.5 30 # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk * Values outside of QC limits Page 24 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte EPA TO-15 in Air Acetone Benzene Benzyl chloride Bromodichloromethane Bromoform Bromomethane 1,3-Butadiene 2-Butanone (MEK) Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane Cyclohexane Dibromochloromethane 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane (Freon 12) 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethylene cis-1,2-Dichloroethylene trans- l,2-Dichloro ethylene 1,2-Dichloropropane cis- 1,3 -Dichloropropene trans- 1, 3 -Dichloropropene 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) 1,4-Dioxane Ethanol Ethyl Acetate Ethylbenzene 4-Ethyltoluene Heptane Hexachlorobutadiene Hexane 2-Hexanone (MBK) Isopropanol Methyl tart -Butyl Ether (MTBE) Methylene Chloride 4-Methyl-2-pentanone (MIBK) Naphthalene Propene Styrene 1,1,2,2-Tetrachloroethane Certifications AIHA,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA, FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH,VA AIHA,NY,ME,NH AIHA,NJ,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NY,ME,NH AIHA,NJ,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA AIHA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ AIHA,NJ,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA, FL,NJ,NY,ME,NH, VA AIHA AIHA,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH NY,ME,NH AIHA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA Page 25 of 29 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte EPA TO-15 in Air Tetrachloroethylene Tetrahydrofuran Toluene 1,2,4-Trichlorobenzene 1, 1, 1 -Trichloroethane 1,1,2-Trichloroethane Trichloroethylene Trichlorofluoromethane (Freon 11) 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl Chloride m&p-Xylene o-Xylene Certifications AIHA,FL,NJ,NY,ME,NH, VA AIHA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NY,ME,NH AIHA,NJ,NY,ME,NH,VA AIHA,NJ,NY,ME,NH AIHA,NJ,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA, FL,NJ,NY,ME,NH, VA AIHA, FL,NJ,NY,ME,NH, VA Con -Test, a Pace Environmental Laboratory, operates under the following certifications and accreditation: Code Description Number Expires AHIA AIHA-LAP, LLC - ISO17025:2017 100033 03/l/2022 MA Massachusetts DEP M-MA100 06/30/2022 CT Connecticut Department of Publilc Health PH-0165 12/31/2022 NY New York State Department of Health 10899 NELAP 04/l/2022 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2022 RI Rhode Island Department of Health LA000112 12/30/2021 NC North Carolina Div. of Water Quality 652 12/31/2021 NJ New Jersey DEP MA007 NELAP 06/30/2022 FL Florida Department of Health E871027 NELAP 06/30/2022 VT Vermont Department of Health Lead Laboratory LL720741 07/30/2022 ME State of Maine MA00100 06/9/2023 VA Commonwealth of Virginia 460217 12/14/2021 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2022 VT-DW Vermont Department of Health Drinking Water VT-255716 06/12/2022 NC-DW North Carolina Department of Health 25703 07/31/2022 PA Commonwealth of Pennsylvania DEP 68-05812 06/30/2022 MI Dept. of Env, Great Lakes, and Energy 9100 09/6/2022 Page 26 of 29 - � 0 a- CL a,q CD O an o N W V � N J h N LLJ v i7al of ...3 CO 7L 0 in Lab Receipt Pressure Final Pressure Initial Pressure Li C,- t___E ❑ ❑ El C [O �•"-• � A T � Q w X 2 O 0 ,y r- �� M V ,a W .=1 Cr ;M, on a E o �a ZtL �eu cc v „r Qjta74a1 vtQZm- Z Y_ z° a {j (� i L i3 it [a t'1 itEl El ni 5V N NaaLnamo C ra f N AWN 1 E 2 x 0 5 F a❑❑ ' m C " C N C n E � K 3 r� E u U G 0 V .c C J 1� Q V an L, 11 El El c u N W V U V ip QT Q N d cC w V C � u onEl'E -, 3 N U ,Jr El ENJ �V :U'TU d-7 I I �-j 9/22121, 6:48 PM Detailed Tracking TRACK ANOTHER SHIPMENT 987548455539 O ADD NICKNAME Delivered Wednesday, September 22, 2021 at 12:05 pm THIS IS 1 OF 5 PIECES AM, Ah DELIVERED Signed for by: AALINE GET STATUS UPDATES OBTAIN PROOF OF DELIVERY FROM TO Huntersville, NC US East Longmeadow, MA US 5 Piece Shipment TRACKING ID STATUS SHIP DELIVERY HANDLING PIECE SHIPPER CITY, RECIPIENT CITY, DATE DATE UNITS STATE STATE 987548455539 (master) Delivered 9/20/21 9/22/21 0 Huntersville NC EAST LONGMEADOW MA 98754846554D Delivered 9/20/21 9/22121 0 Huntetsvillc NC EAST LONGMEADOW MA 987548456550 Delivered 9/20121 9/22/21 0 Huntersville NC LAST LONG MEADOW MA 987548455561 Delivered 9120/21 9122121 0 Huntersville NC EAST LONGMEADOW €CIA 987548455572 Delivered 9120/21 9/22/21 0 Huntersville NC FAST LONGMEADOW MA Travel i-i dory TIME ZONE Local Scan Time NV https:!lwww.fedex.comlfedextracW?trknbr=987548455539&trkquaI= 12022-987548455539—FDEG Page 28 of 29 OD I Have Not Confirmed Sample Container Numbers With Lab Staff Before caonmwtemst Relinquishing Over Samples .. . . k3b�#= ... R Air Media Sample Receipt Checklist - (Rejection Criteria Listing - Using Acceptance Policy) Any False Statement will be brought to the attention of the Client - State Prue or False Client` Received Byt— Date Time How were the samples In Cooler On Ice No Ice received? In Box Ambient Melted ice Were samples within Temperature Compliance? 2-6'C� Was Custody Seal intact?� W COC R : ? By Gun # Actual Temp - By Blank # Actual Temp - as el�nquished . Are there any loose caps/valves on any samples? Is COC in ink/ Legible? Were Samples Tampered with? Does Chain Agree With Samples? j Did COC Include all Client Analysis Sampler Name I Pertinent Information? Project i ID's —C Collection Dates/Times i Are Sample Labels filled out and legible? _ Are there Rushes? Who was notified? Samples are received within holding time? Proper Media Used? Individually Certified Cans? -F— Are there Trip Blanks?— Is there enough Volume? umma Cans TO-17 Tubes Radiello Pufs/TO-11 s m Tu Tedlar j Page 29 of 29 1 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 September 27, 2021 Scott Young ECS Southeast - Greensboro, NC 4811 Koger Boulevard Greensboro, NC 27407 Project Location: Charlotte, NC Client Job Number: Project Number: 118148 Laboratory Work Order Number: 21I1199 Enclosed are results of analyses for samples received by the laboratory on September 20, 2021. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kerry K. McGee Project Manager QA Officer Katherine Allen Laboratory Manager Daren Damboragian Page 1 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ECS Southeast - Greensboro, NC REPORT DATE: 9/27/2021 4811 Koger Boulevard Greensboro, NC 27407 PURCHASE ORDER NUMBER: ATTN: Scott Young PROJECT NUMBER: 118148 ANALYTICAL SUMMARY WORK ORDER NUMBER: 21I1199 The results of analyses performed on the following samples submitted to Con -Test, a Pace Analytical Laboratory, are found in this report. PROJECT LOCATION: Charlotte, NC FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB IA-1 21I1199-01 Indoor air EPA TO-15 IA-2 21I1199-02 Indoor air EPA TO-15 IA-3 21I1199-03 Indoor air EPA TO-15 IA-4 21I1199-04 Indoor air EPA TO-15 IA-DUP 21I1199-05 Indoor air EPA TO-15 AA-1 21I1199-06 Ambient Air EPATO-15 Page 2 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. Page 3 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 EPA TO-15 Qualifications: Laboratory fortified blank/laboratory control sample recovery outside of control limits. Data validation is not affected since all results are "not detected" for all samples in this batch for this compound and bias is on the high side. Analyte & Samples(s) Qualified: Vinyl Acetate B290913-BSI Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this compound is likely to be biased on the low side. Analyte & Samples(s) Qualified: Ethyl Acetate 21I1199-01[IA-1], 21I1199-02[IA-2], 21I1199-03[IA-3], 21I1199-04[IA-4], 21I1199-05[IA-DUP], 21I1199-06[AA-1], B290913-BLKI, B290913-BSI, B290914-BLKI, B290914-BS1 Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method specified criteria. Reported result is estimated. Analyte & Samples(s) Qualified: 1,2,4-Trichlorobenzene 21I1199-04[IA-4], 21I1199-05[IA-DUP], 21I1199-06[AA-1], B290914-BLKI, B290914-BSI, S063580-CCVI Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound. Analyte & Samples(s) Qualified: Hexachlorobutadiene 21I1199-04[IA-4], 21I1199-05[IA-DUP], 21I1199-06[AA-1], B290914-BLKI, B290914-BSI, S063580-CCVI Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is estimated. Analyte & Samples(s) Qualified: Ethyl Acetate 21I1199-04[IA-4], 21I1199-05[IA-DUP], 21I1199-06[AA-1], B290914-BLKI, B290914-BSI Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this compound. Reported result is estimated. Analyte & Samples(s) Qualified: Naphthalene 21II199-OI[IA-1], 21I1199-02[IA-2], 21II199-03[IA-3], 5063579-CCVI Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. Analyte & Samples(s) Qualified: Vinyl Acetate B290913-BS1, B290914-BSI, 5063579-CCVI, 5063580-CCV1 Page 4 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 The results of analyses reported only relate to samples submitted to Con -Test, a Pace Analytical Laboratory, for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Tod E. Kopyscinski Laboratory Director Page 5 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Charlotte, NC Date Received: 9/20/2021 Field Sample #: IA-1 Sample ID: 21I1199-01 Sample Matrix: Indoor air Sampled: 9/16/2021 18:06 Sample Description/Location: Sub Description/Location: Canister ID: 2157 Canister Size: 6 liter Flow Controller ID: 3215 Sample Type: 8 hr Work Order: 21I1199 Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -6.3 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Acetone 32 1.4 0.84 75 3.3 2.0 0.698 9/24/21 5:36 BRF Benzene 0.24 0.035 0.0084 0.77 0.11 0.027 0.698 9/24/21 5:36 BRF Benzyl chloride ND 0.035 0.016 ND 0.18 0.081 0.698 9/24/21 5:36 BRF Bromodichloromethane ND 0.035 0.013 ND 0.23 0.085 0.698 9/24/21 5:36 BRF Bromoform ND 0.070 0.013 ND 0.72 0.13 0.698 9/24/21 5:36 BRF Bromomethane ND 0.035 0.028 ND 0.14 0.11 0.698 9/24/21 5:36 BRF 1,3-Butadiene ND 0.035 0.024 ND 0.077 0.054 0.698 9/24/21 5:36 BRF 2-Butanone (MEK) 2.5 1.4 0.12 7.4 4.1 0.34 0.698 9/24/21 5:36 BRF Carbon Disulfide ND 0.35 0.089 ND 1.1 0.28 0.698 9/24/21 5:36 BRF Carbon Tetrachloride 0.077 0.035 0.011 0.49 0.22 0.066 0.698 9/24/21 5:36 BRF Chlorobenzene ND 0.035 0.010 ND 0.16 0.048 0.698 9/24/21 5:36 BRF Chloroethane ND 0.035 0.025 ND 0.092 0.067 0.698 9/24/21 5:36 BRF Chloroform 0.080 0.035 0.0084 0.39 0.17 0.041 0.698 9/24/21 5:36 BRF Chloromethane 0.55 0.070 0.014 1.1 0.14 0.030 0.698 9/24/21 5:36 BRF Cyclohexane 0.49 0.035 0.023 1.7 0.12 0.079 0.698 9/24/21 5:36 BRF Dibromochloromethane ND 0.035 0.012 ND 0.30 0.100 0.698 9/24/21 5:36 BRF 1,2-Dibromoethane (EDB) ND 0.035 0.0098 ND 0.27 0.075 0.698 9/24/21 5:36 BRF 1,2-Dichlorobenzene ND 0.035 0.013 ND 0.21 0.078 0.698 9/24/21 5:36 BRF 1,3-Dichlorobenzene ND 0.035 0.0084 ND 0.21 0.051 0.698 9/24/21 5:36 BRF 1,4-Dichlorobenzene ND 0.035 0.014 ND 0.21 0.085 0.698 9/24/21 5:36 BRF Dichlorodifluoromethane (Freon 12) 0.67 0.035 0.011 3.3 0.17 0.053 0.698 9/24/21 5:36 BRF 1, 1 -Dichloroethane ND 0.035 0.012 ND 0.14 0.047 0.698 9/24/21 5:36 BRF 1,2-Dichloroethane ND 0.035 0.013 ND 0.14 0.052 0.698 9/24/21 5:36 BRF 1, 1 -Dichloroethylene ND 0.035 0.014 ND 0.14 0.054 0.698 9/24/21 5:36 BRF cis-1,2-Dichloroethylene ND 0.035 0.012 ND 0.14 0.047 0.698 9/24/21 5:36 BRF trans-1,2-Dichloroethylene ND 0.035 0.012 ND 0.14 0.048 0.698 9/24/21 5:36 BRF 1,2-Dichloropropane ND 0.035 0.013 ND 0.16 0.058 0.698 9/24/21 5:36 BRF cis- 1,3 -Dichloropropene ND 0.035 0.016 ND 0.16 0.073 0.698 9/24/21 5:36 BRF trans- 1, 3 -Dichloropropene ND 0.035 0.011 ND 0.16 0.049 0.698 9/24/21 5:36 BRF 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.012 ND 0.24 0.084 0.698 9/24/21 5:36 BRF 1,4-Dioxane ND 0.35 0.024 ND 1.3 0.085 0.698 9/24/21 5:36 BRF Ethanol 380 20 6.1 720 38 11 10 9/25/21 1:28 BRF Ethyl Acetate ND 0.35 0.21 L-03 ND 1.3 0.75 0.698 9/24/21 5:36 BRF Ethylbenzene 15 0.035 0.0090 65 0.15 0.039 0.698 9/24/21 5:36 BRF 4-Ethyltoluene 0.12 0.035 0.011 0.60 0.17 0.053 0.698 9/24/21 5:36 BRF Heptane ND 0.035 0.014 ND 0.14 0.059 0.698 9/24/21 5:36 BRF Hexachlorobutadiene ND 0.035 0.019 ND 0.37 0.21 0.698 9/24/21 5:36 BRF Hexane 0.78 1.4 0.11 J 2.8 4.9 0.40 0.698 9/24/21 5:36 BRF 2-Hexanone (MBK) ND 0.035 0.018 ND 0.14 0.072 0.698 9/24/21 5:36 BRF Isopropanol 14 1.4 0.32 35 3.4 0.79 0.698 9/24/21 5:36 BRF Methyl tert-Butyl Ether (MTBE) ND 0.035 0.014 ND 0.13 0.050 0.698 9/24/21 5:36 BRF Methylene Chloride 1.0 0.35 0.080 3.6 1.2 0.28 0.698 9/24/21 5:36 BRF 4-Methyl-2-pentanone (MIBK) ND 0.035 0.018 ND 0.14 0.073 0.698 9/24/21 5:36 BRF Naphthalene 0.51 0.035 0.022 V-35 2.7 0.18 0.12 0.698 9/24/21 5:36 BRF Propene ND 1.4 0.12 ND 2.4 0.20 0.698 9/24/21 5:36 BRF Styrene ND 0.035 0.011 ND 0.15 0.047 0.698 9/24/21 5:36 BRF 1,1,2,2-Tetrachloroethane ND 0.035 0.011 ND 0.24 0.073 0.698 9/24/21 5:36 BRF Page 6 of 40 con -test® A Pace Analytical Laboratory Project Location: Charlotte, NC Date Received: 9/20/2021 Field Sample #: IA-1 Sample ID: 21I1199-01 Sample Matrix: Indoor air Sampled: 9/ 16/2021 18:06 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2157 Canister Size: 6 liter Flow Controller ID: 3215 Sample Type: 8 hr Work Order: 21I1199 Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -6.3 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.035 0.010 ND 0.24 0.070 0.698 9/24/21 5:36 BRF Tetrahydrofuran 1.3 0.35 0.086 3.9 1.0 0.25 0.698 9/24/21 5:36 BRF Toluene 1.0 0.035 0.015 3.9 0.13 0.055 0.698 9/24/21 5:36 BRF 1,2,4-Trichlorobenzene ND 0.035 0.024 ND 0.26 0.18 0.698 9/24/21 5:36 BRF 1, 1, 1 -Trichloroethane ND 0.035 0.016 ND 0.19 0.088 0.698 9/24/21 5:36 BRF 1,1,2-Trichloroethane ND 0.035 0.014 ND 0.19 0.076 0.698 9/24/21 5:36 BRF Trichloroethylene ND 0.035 0.013 ND 0.19 0.069 0.698 9/24/21 5:36 BRF Trichlorofluoromethane (Freon 11) 3.6 0.14 0.014 20 0.78 0.078 0.698 9/24/21 5:36 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.11 0.14 0.012 J 0.87 1.1 0.095 0.698 9/24/21 5:36 BRF 1,2,4-Trimethylbenzene 0.81 0.035 0.010 4.0 0.17 0.051 0.698 9/24/21 5:36 BRF 1,3,5-Trimethylbenzene 0.19 0.035 0.0096 0.93 0.17 0.047 0.698 9/24/21 5:36 BRF Vinyl Acetate ND 0.70 0.065 ND 2.5 0.23 0.698 9/24/21 5:36 BRF Vinyl Chloride ND 0.035 0.014 ND 0.089 0.035 0.698 9/24/21 5:36 BRF m&p-Xylene 52 0.070 0.019 230 0.30 0.084 0.698 9/24/21 5:36 BRF o-Xylene 17 0.035 0.0093 74 0.15 0.041 0.698 9/24/21 5:36 BRF Surrogates 4-Bromofluorobenzene (1) 4-Bromofluorobenzene (1) % Recovery % REC Limits 92.7 70-130 97.0 70-130 9/25/21 1:28 9/24/21 5:36 Page 7 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Charlotte, NC Date Received: 9/20/2021 Field Sample #: IA-2 Sample ID: 21I1199-02 Sample Matrix: Indoor air Sampled: 9/16/2021 18:30 Sample Description/Location: Sub Description/Location: Canister ID: 1212 Canister Size: 6 liter Flow Controller ID: 3553 Sample Type: 8 hr Work Order: 21I1199 Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -6 Receipt Vacuum(in Hg): -6.4 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RI MDL Dilution Analyzed Analyst Acetone 27 1.4 0.84 64 3.3 2.0 0.698 9/24/21 6:12 BRF Benzene 0.23 0.035 0.0084 0.75 0.11 0.027 0.698 9/24/21 6:12 BRF Benzyl chloride ND 0.035 0.016 ND 0.18 0.081 0.698 9/24/21 6:12 BRF Bromodichloromethane ND 0.035 0.013 ND 0.23 0.085 0.698 9/24/21 6:12 BRF Bromoform ND 0.070 0.013 ND 0.72 0.13 0.698 9/24/21 6:12 BRF Bromomethane ND 0.035 0.028 ND 0.14 0.11 0.698 9/24/21 6:12 BRF 1,3-Butadiene ND 0.035 0.024 ND 0.077 0.054 0.698 9/24/21 6:12 BRF 2-Butanone (MEK) 1.8 1.4 0.12 5.5 4.1 0.34 0.698 9/24/21 6:12 BRF Carbon Disulfide ND 0.35 0.089 ND 1.1 0.28 0.698 9/24/21 6:12 BRF Carbon Tetrachloride 0.077 0.035 0.011 0.48 0.22 0.066 0.698 9/24/21 6:12 BRF Chlorobenzene ND 0.035 0.010 ND 0.16 0.048 0.698 9/24/21 6:12 BRF Chloroethane ND 0.035 0.025 ND 0.092 0.067 0.698 9/24/21 6:12 BRF Chloroform 0.086 0.035 0.0084 0.42 0.17 0.041 0.698 9/24/21 6:12 BRF Chloromethane 0.57 0.070 0.014 1.2 0.14 0.030 0.698 9/24/21 6:12 BRF Cyclohexane 0.36 0.035 0.023 1.2 0.12 0.079 0.698 9/24/21 6:12 BRF Dibromochloromethane ND 0.035 0.012 ND 0.30 0.100 0.698 9/24/21 6:12 BRF 1,2-Dibromoethane (EDB) ND 0.035 0.0098 ND 0.27 0.075 0.698 9/24/21 6:12 BRF 1,2-Dichlorobenzene ND 0.035 0.013 ND 0.21 0.078 0.698 9/24/21 6:12 BRF 1,3-Dichlorobenzene ND 0.035 0.0084 ND 0.21 0.051 0.698 9/24/21 6:12 BRF 1,4-Dichlorobenzene ND 0.035 0.014 ND 0.21 0.085 0.698 9/24/21 6:12 BRF Dichlorodifluoromethane (Freon 12) 0.70 0.035 0.011 3.5 0.17 0.053 0.698 9/24/21 6:12 BRF 1,1-Dichloroethane ND 0.035 0.012 ND 0.14 0.047 0.698 9/24/21 6:12 BRF 1,2-Dichloroethane ND 0.035 0.013 ND 0.14 0.052 0.698 9/24/21 6:12 BRF 1,1-Dichloroethylene ND 0.035 0.014 ND 0.14 0.054 0.698 9/24/21 6:12 BRF cis-1,2-Dichloroethylene ND 0.035 0.012 ND 0.14 0.047 0.698 9/24/21 6:12 BRF trans-1,2-Dichloroethylene ND 0.035 0.012 ND 0.14 0.048 0.698 9/24/21 6:12 BRF 1,2-Dichloropropane ND 0.035 0.013 ND 0.16 0.058 0.698 9/24/21 6:12 BRF cis- 1,3 -Dichloropropene ND 0.035 0.016 ND 0.16 0.073 0.698 9/24/21 6:12 BRF trans- 1, 3 -Dichloropropene ND 0.035 0.011 ND 0.16 0.049 0.698 9/24/21 6:12 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.012 ND 0.24 0.084 0.698 9/24/21 6:12 BRF 1,4-Dioxane ND 0.35 0.024 ND 1.3 0.085 0.698 9/24/21 6:12 BRF Ethanol 360 20 6.1 670 38 11 10 9/25/21 1:53 BRF Ethyl Acetate ND 0.35 0.21 L-03 ND 1.3 0.75 0.698 9/24/21 6:12 BRF Ethylbenzene 13 0.035 0.0090 54 0.15 0.039 0.698 9/24/21 6:12 BRF 4-Ethyltoluene 0.15 0.035 0.011 0.72 0.17 0.053 0.698 9/24/21 6:12 BRF Heptane 0.19 0.035 0.014 0.80 0.14 0.059 0.698 9/24/21 6:12 BRF Hexachlorobutadiene ND 0.035 0.019 ND 0.37 0.21 0.698 9/24/21 6:12 BRF Hexane 0.53 1.4 0.11 J 1.9 4.9 0.40 0.698 9/24/21 6:12 BRF 2-Hexanone (MBK) ND 0.035 0.018 ND 0.14 0.072 0.698 9/24/21 6:12 BRF Isopropanol 13 1.4 0.32 33 3.4 0.79 0.698 9/24/21 6:12 BRF Methyl tert-Butyl Ether (MTBE) ND 0.035 0.014 ND 0.13 0.050 0.698 9/24/21 6:12 BRF Methylene Chloride 0.35 0.35 0.080 1.2 1.2 0.28 0.698 9/24/21 6:12 BRF 4-Methyl-2-pentanone (MIBK) ND 0.035 0.018 ND 0.14 0.073 0.698 9/24/21 6:12 BRF Naphthalene 0.51 0.035 0.022 V-35 2.7 0.18 0.12 0.698 9/24/21 6:12 BRF Propene ND 1.4 0.12 ND 2.4 0.20 0.698 9/24/21 6:12 BRF Styrene ND 0.035 0.011 ND 0.15 0.047 0.698 9/24/21 6:12 BRF 1,1,2,2-Tetrachloroethane ND 0.035 0.011 ND 0.24 0.073 0.698 9/24/21 6:12 BRF Page 8 of 40 con -test® A Pace Analytical Laboratory Project Location: Charlotte, NC Date Received: 9/20/2021 Field Sample #: IA-2 Sample ID: 21I1199-02 Sample Matrix: Indoor air Sampled: 9/ 16/2021 18:30 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 1212 Canister Size: 6 liter Flow Controller ID: 3553 Sample Type: 8 hr Work Order: 21I1199 Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -6 Receipt Vacuum(in Hg): -6.4 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 0.026 0.035 0.010 J 0.18 0.24 0.070 0.698 9/24/21 6:12 BRF Tetrahydrofuran 1.3 0.35 0.086 3.8 1.0 0.25 0.698 9/24/21 6:12 BRF Toluene 0.96 0.035 0.015 3.6 0.13 0.055 0.698 9/24/21 6:12 BRF 1,2,4-Trichlorobenzene ND 0.035 0.024 ND 0.26 0.18 0.698 9/24/21 6:12 BRF 1, 1, 1 -Trichloroethane ND 0.035 0.016 ND 0.19 0.088 0.698 9/24/21 6:12 BRF 1,1,2-Trichloroethane ND 0.035 0.014 ND 0.19 0.076 0.698 9/24/21 6:12 BRF Trichloroethylene ND 0.035 0.013 ND 0.19 0.069 0.698 9/24/21 6:12 BRF Trichlorofluoromethane (Freon 11) 3.1 0.14 0.014 18 0.78 0.078 0.698 9/24/21 6:12 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.12 0.14 0.012 J 0.95 1.1 0.095 0.698 9/24/21 6:12 BRF 1,2,4-Trimethylbenzene 0.73 0.035 0.010 3.6 0.17 0.051 0.698 9/24/21 6:12 BRF 1,3,5-Trimethylbenzene 0.17 0.035 0.0096 0.84 0.17 0.047 0.698 9/24/21 6:12 BRF Vinyl Acetate ND 0.70 0.065 ND 2.5 0.23 0.698 9/24/21 6:12 BRF Vinyl Chloride ND 0.035 0.014 ND 0.089 0.035 0.698 9/24/21 6:12 BRF m&p-Xylene 44 0.070 0.019 190 0.30 0.084 0.698 9/24/21 6:12 BRF o-Xylene 14 0.035 0.0093 62 0.15 0.041 0.698 9/24/21 6:12 BRF Surrogates 4-Bromofluorobenzene (1) 4-Bromofluorobenzene (1) % Recovery % REC Limits 93.0 70-130 95.4 70-130 9/25/21 1:53 9/24/21 6:12 Page 9 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Charlotte, NC Date Received: 9/20/2021 Field Sample #: IA-3 Sample ID: 21I1199-03 Sample Matrix: Indoor air Sampled: 9/16/2021 18:30 Sample Description/Location: Sub Description/Location: Canister ID: 2223 Canister Size: 6 liter Flow Controller ID: 3571 Sample Type: 8 hr Work Order: 21I1199 Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -6 Receipt Vacuum(in Hg): -5.2 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RI MDL Dilution Analyzed Analyst Acetone 35 1.4 0.84 82 3.3 2.0 0.698 9/24/21 6:50 BRF Benzene 0.28 0.035 0.0084 0.89 0.11 0.027 0.698 9/24/21 6:50 BRF Benzyl chloride ND 0.035 0.016 ND 0.18 0.081 0.698 9/24/21 6:50 BRF Bromodichloromethane ND 0.035 0.013 ND 0.23 0.085 0.698 9/24/21 6:50 BRF Bromoform ND 0.070 0.013 ND 0.72 0.13 0.698 9/24/21 6:50 BRF Bromomethane ND 0.035 0.028 ND 0.14 0.11 0.698 9/24/21 6:50 BRF 1,3-Butadiene ND 0.035 0.024 ND 0.077 0.054 0.698 9/24/21 6:50 BRF 2-Butanone (MEK) 1.9 1.4 0.12 5.5 4.1 0.34 0.698 9/24/21 6:50 BRF Carbon Disulfide ND 0.35 0.089 ND 1.1 0.28 0.698 9/24/21 6:50 BRF Carbon Tetrachloride 0.093 0.035 0.011 0.59 0.22 0.066 0.698 9/24/21 6:50 BRF Chlorobenzene ND 0.035 0.010 ND 0.16 0.048 0.698 9/24/21 6:50 BRF Chloroethane ND 0.035 0.025 ND 0.092 0.067 0.698 9/24/21 6:50 BRF Chloroform 0.17 0.035 0.0084 0.83 0.17 0.041 0.698 9/24/21 6:50 BRF Chloromethane 0.56 0.070 0.014 1.2 0.14 0.030 0.698 9/24/21 6:50 BRF Cyclohexane 0.94 0.035 0.023 3.2 0.12 0.079 0.698 9/24/21 6:50 BRF Dibromochloromethane ND 0.035 0.012 ND 0.30 0.100 0.698 9/24/21 6:50 BRF 1,2-Dibromoethane (EDB) ND 0.035 0.0098 ND 0.27 0.075 0.698 9/24/21 6:50 BRF 1,2-Dichlorobenzene ND 0.035 0.013 ND 0.21 0.078 0.698 9/24/21 6:50 BRF 1,3-Dichlorobenzene ND 0.035 0.0084 ND 0.21 0.051 0.698 9/24/21 6:50 BRF 1,4-Dichlorobenzene ND 0.035 0.014 ND 0.21 0.085 0.698 9/24/21 6:50 BRF Dichlorodifluoromethane (Freon 12) 0.62 0.035 0.011 3.1 0.17 0.053 0.698 9/24/21 6:50 BRF 1,1-Dichloroethane ND 0.035 0.012 ND 0.14 0.047 0.698 9/24/21 6:50 BRF 1,2-Dichloroethane 0.18 0.035 0.013 0.72 0.14 0.052 0.698 9/24/21 6:50 BRF 1,1-Dichloroethylene ND 0.035 0.014 ND 0.14 0.054 0.698 9/24/21 6:50 BRF cis-1,2-Dichloroethylene ND 0.035 0.012 ND 0.14 0.047 0.698 9/24/21 6:50 BRF trans-1,2-Dichloroethylene ND 0.035 0.012 ND 0.14 0.048 0.698 9/24/21 6:50 BRF 1,2-Dichloropropane ND 0.035 0.013 ND 0.16 0.058 0.698 9/24/21 6:50 BRF cis- 1,3 -Dichloropropene ND 0.035 0.016 ND 0.16 0.073 0.698 9/24/21 6:50 BRF trans- 1, 3 -Dichloropropene ND 0.035 0.011 ND 0.16 0.049 0.698 9/24/21 6:50 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.012 ND 0.24 0.084 0.698 9/24/21 6:50 BRF 1,4-Dioxane ND 0.35 0.024 ND 1.3 0.085 0.698 9/24/21 6:50 BRF Ethanol 340 20 6.1 650 38 11 10 9/25/21 2:18 BRF Ethyl Acetate 7.9 0.35 0.21 L-03 28 1.3 0.75 0.698 9/24/21 6:50 BRF Ethylbenzene 11 0.035 0.0090 50 0.15 0.039 0.698 9/24/21 6:50 BRF 4-Ethyltoluene ND 0.035 0.011 ND 0.17 0.053 0.698 9/24/21 6:50 BRF Heptane ND 0.035 0.014 ND 0.14 0.059 0.698 9/24/21 6:50 BRF Hexachlorobutadiene ND 0.035 0.019 ND 0.37 0.21 0.698 9/24/21 6:50 BRF Hexane ND 1.4 0.11 ND 4.9 0.40 0.698 9/24/21 6:50 BRF 2-Hexanone (MBK) ND 0.035 0.018 ND 0.14 0.072 0.698 9/24/21 6:50 BRF Isopropanol 5.9 1.4 0.32 15 3.4 0.79 0.698 9/24/21 6:50 BRF Methyl tert-Butyl Ether (MTBE) ND 0.035 0.014 ND 0.13 0.050 0.698 9/24/21 6:50 BRF Methylene Chloride 0.53 0.35 0.080 1.8 1.2 0.28 0.698 9/24/21 6:50 BRF 4-Methyl-2-pentanone (MIBK) ND 0.035 0.018 ND 0.14 0.073 0.698 9/24/21 6:50 BRF Naphthalene 0.31 0.035 0.022 V-35 1.6 0.18 0.12 0.698 9/24/21 6:50 BRF Propene ND 1.4 0.12 ND 2.4 0.20 0.698 9/24/21 6:50 BRF Styrene 0.37 0.035 0.011 1.6 0.15 0.047 0.698 9/24/21 6:50 BRF 1,1,2,2-Tetrachloroethane ND 0.035 0.011 ND 0.24 0.073 0.698 9/24/21 6:50 BRF Page 10 of 40 con -test® A Pace Analytical Laboratory Project Location: Charlotte, NC Date Received: 9/20/2021 Field Sample #: IA-3 Sample ID: 21I1199-03 Sample Matrix: Indoor air Sampled: 9/ 16/2021 18:30 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2223 Canister Size: 6 liter Flow Controller ID: 3571 Sample Type: 8 hr Work Order: 21I1199 Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -6 Receipt Vacuum(in Hg): -5.2 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 0.051 0.035 0.010 0.35 0.24 0.070 0.698 9/24/21 6:50 BRF Tetrahydrofuran 1.4 0.35 0.086 4.0 1.0 0.25 0.698 9/24/21 6:50 BRF Toluene 3.7 0.035 0.015 14 0.13 0.055 0.698 9/24/21 6:50 BRF 1,2,4-Trichlorobenzene ND 0.035 0.024 ND 0.26 0.18 0.698 9/24/21 6:50 BRF 1, 1, 1 -Trichloroethane ND 0.035 0.016 ND 0.19 0.088 0.698 9/24/21 6:50 BRF 1,1,2-Trichloroethane 0.24 0.035 0.014 1.3 0.19 0.076 0.698 9/24/21 6:50 BRF Trichloroethylene ND 0.035 0.013 ND 0.19 0.069 0.698 9/24/21 6:50 BRF Trichlorofluoromethane (Freon 11) 1.9 0.14 0.014 10 0.78 0.078 0.698 9/24/21 6:50 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.093 0.14 0.012 J 0.72 1.1 0.095 0.698 9/24/21 6:50 BRF 1,2,4-Trimethylbenzene 0.49 0.035 0.010 2.4 0.17 0.051 0.698 9/24/21 6:50 BRF 1,3,5-Trimethylbenzene 0.10 0.035 0.0096 0.50 0.17 0.047 0.698 9/24/21 6:50 BRF Vinyl Acetate ND 0.70 0.065 ND 2.5 0.23 0.698 9/24/21 6:50 BRF Vinyl Chloride ND 0.035 0.014 ND 0.089 0.035 0.698 9/24/21 6:50 BRF m&p-Xylene 40 0.070 0.019 170 0.30 0.084 0.698 9/24/21 6:50 BRF o-Xylene 13 0.035 0.0093 57 0.15 0.041 0.698 9/24/21 6:50 BRF Surrogates 4-Bromofluorobenzene (1) 4-Bromofluorobenzene (1) % Recovery % REC Limits 92.2 70-130 98.8 70-130 9/25/21 2:18 9/24/21 6:50 Page 11 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Charlotte, NC Date Received: 9/20/2021 Field Sample #: IA-4 Sample ID: 21I1199-04 Sample Matrix: Indoor air Sampled: 9/16/2021 17:09 Sample Description/Location: Sub Description/Location: Canister ID: 2154 Canister Size: 6 liter Flow Controller ID: 3241 Sample Type: 8 hr Work Order: 21I1199 Initial Vacuum(in Hg): -30 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -5.1 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Acetone 13 1.4 0.84 31 3.3 2.0 0.698 9/23/21 19:42 BRF Benzene 0.29 0.035 0.0084 0.92 0.11 0.027 0.698 9/23/21 19:42 BRF Benzyl chloride ND 0.035 0.016 ND 0.18 0.081 0.698 9/23/21 19:42 BRF Bromodichloromethane ND 0.035 0.013 ND 0.23 0.085 0.698 9/23/21 19:42 BRF Bromoform ND 0.035 0.013 ND 0.36 0.13 0.698 9/23/21 19:42 BRF Bromomethane ND 0.035 0.028 ND 0.14 0.11 0.698 9/23/21 19:42 BRF 1,3-Butadiene ND 0.035 0.024 ND 0.077 0.054 0.698 9/23/21 19:42 BRF 2-Butanone (MEK) 1.3 1.4 0.12 J 3.8 4.1 0.34 0.698 9/23/21 19:42 BRF Carbon Disulfide ND 0.35 0.089 ND 1.1 0.28 0.698 9/23/21 19:42 BRF Carbon Tetrachloride 0.061 0.035 0.011 0.38 0.22 0.066 0.698 9/23/21 19:42 BRF Chlorobenzene ND 0.035 0.010 ND 0.16 0.048 0.698 9/23/21 19:42 BRF Chloroethane ND 0.035 0.025 ND 0.092 0.067 0.698 9/23/21 19:42 BRF Chloroform 0.060 0.035 0.0084 0.29 0.17 0.041 0.698 9/23/21 19:42 BRF Chloromethane 0.72 0.070 0.014 1.5 0.14 0.030 0.698 9/23/21 19:42 BRF Cyclohexane 0.41 0.035 0.023 1.4 0.12 0.079 0.698 9/23/21 19:42 BRF Dibromochloromethane ND 0.035 0.012 ND 0.30 0.100 0.698 9/23/21 19:42 BRF 1,2-Dibromoethane (EDB) ND 0.035 0.0098 ND 0.27 0.075 0.698 9/23/21 19:42 BRF 1,2-Dichlorobenzene ND 0.035 0.013 ND 0.21 0.078 0.698 9/23/21 19:42 BRF 1,3-Dichlorobenzene ND 0.035 0.0084 ND 0.21 0.051 0.698 9/23/21 19:42 BRF 1,4-Dichlorobenzene ND 0.035 0.014 ND 0.21 0.085 0.698 9/23/21 19:42 BRF Dichlorodifluoromethane (Freon 12) 0.69 0.035 0.011 3.4 0.17 0.053 0.698 9/23/21 19:42 BRF 1,1-Dichloroethane ND 0.035 0.012 ND 0.14 0.047 0.698 9/23/21 19:42 BRF 1,2-Dichloroethane ND 0.035 0.013 ND 0.14 0.052 0.698 9/23/21 19:42 BRF 1,1-Dichloroethylene ND 0.035 0.014 ND 0.14 0.054 0.698 9/23/21 19:42 BRF cis-1,2-Dichloroethylene ND 0.035 0.012 ND 0.14 0.047 0.698 9/23/21 19:42 BRF trans-1,2-Dichloroethylene ND 0.035 0.012 ND 0.14 0.048 0.698 9/23/21 19:42 BRF 1,2-Dichloropropane ND 0.035 0.013 ND 0.16 0.058 0.698 9/23/21 19:42 BRF cis- 1,3 -Dichloropropene ND 0.035 0.016 ND 0.16 0.073 0.698 9/23/21 19:42 BRF trans- 1, 3 -Dichloropropene ND 0.035 0.011 ND 0.16 0.049 0.698 9/23/21 19:42 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.012 ND 0.24 0.084 0.698 9/23/21 19:42 BRF 1,4-Dioxane ND 0.35 0.024 ND 1.3 0.085 0.698 9/23/21 19:42 BRF Ethanol 410 20 6.1 760 38 11 10 9/24/21 6:42 BRF Ethyl Acetate ND 0.35 0.21 L-03, V-34 ND 1.3 0.75 0.698 9/23/21 19:42 BRF Ethylbenzene 16 0.035 0.0090 69 0.15 0.039 0.698 9/23/21 19:42 BRF 4-Ethyltoluene 0.082 0.035 0.011 0.40 0.17 0.053 0.698 9/23/21 19:42 BRF Heptane 0.21 0.035 0.014 0.85 0.14 0.059 0.698 9/23/21 19:42 BRF Hexachlorobutadiene ND 0.035 0.019 V-05 ND 0.37 0.21 0.698 9/23/21 19:42 BRF Hexane 0.41 1.4 0.11 J 1.4 4.9 0.40 0.698 9/23/21 19:42 BRF 2-Hexanone (MBK) ND 0.070 0.018 ND 0.29 0.072 0.698 9/23/21 19:42 BRF Isopropanol 3.1 1.4 0.32 7.7 3.4 0.79 0.698 9/23/21 19:42 BRF Methyl tert-Butyl Ether (MTBE) ND 0.035 0.014 ND 0.13 0.050 0.698 9/23/21 19:42 BRF Methylene Chloride 0.23 0.35 0.080 J 0.81 1.2 0.28 0.698 9/23/21 19:42 BRF 4-Methyl-2-pentanone (MIBK) ND 0.035 0.018 ND 0.14 0.073 0.698 9/23/21 19:42 BRF Naphthalene 0.28 0.035 0.022 1.5 0.18 0.12 0.698 9/23/21 19:42 BRF Propene ND 1.4 0.12 ND 2.4 0.20 0.698 9/23/21 19:42 BRF Styrene 0.11 0.035 0.011 0.46 0.15 0.047 0.698 9/23/21 19:42 BRF 1,1,2,2-Tetrachloroethane ND 0.035 0.011 ND 0.24 0.073 0.698 9/23/21 19:42 BRF Page 12 of 40 con -test® A Pace Analytical Laboratory Project Location: Charlotte, NC Date Received: 9/20/2021 Field Sample #: IA-4 Sample ID: 21I1199-04 Sample Matrix: Indoor air Sampled: 9/ 16/2021 17:09 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2154 Canister Size: 6 liter Flow Controller ID: 3241 Sample Type: 8 hr Work Order: 21I1199 Initial Vacuum(in Hg): -30 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -5.1 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RI MDL Dilution Analyzed Analyst Tetrachloroethylene 0.017 0.035 0.010 J 0.11 0.24 0.070 0.698 9/23/21 19:42 BRF Tetrahydrofuran 1.2 0.35 0.086 3.6 1.0 0.25 0.698 9/23/21 19:42 BRF Toluene 0.89 0.035 0.015 3.3 0.13 0.055 0.698 9/23/21 19:42 BRF 1,2,4-Trichlorobenzene ND 0.070 0.024 V-04 ND 0.52 0.18 0.698 9/23/21 19:42 BRF 1, 1, 1 -Trichloroethane ND 0.035 0.016 ND 0.19 0.088 0.698 9/23/21 19:42 BRF 1,1,2-Trichloroethane ND 0.035 0.014 ND 0.19 0.076 0.698 9/23/21 19:42 BRF Trichloroethylene ND 0.035 0.013 ND 0.19 0.069 0.698 9/23/21 19:42 BRF Trichlorofluoromethane (Freon 11) 2.2 0.14 0.014 12 0.78 0.078 0.698 9/23/21 19:42 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.080 0.14 0.012 J 0.61 1.1 0.095 0.698 9/23/21 19:42 BRF 1,2,4-Trimethylbenzene 0.43 0.035 0.010 2.1 0.17 0.051 0.698 9/23/21 19:42 BRF 1,3,5-Trimethylbenzene 0.073 0.035 0.0096 0.36 0.17 0.047 0.698 9/23/21 19:42 BRF Vinyl Acetate ND 0.70 0.065 ND 2.5 0.23 0.698 9/23/21 19:42 BRF Vinyl Chloride ND 0.035 0.014 ND 0.089 0.035 0.698 9/23/21 19:42 BRF m&p-Xylene 53 0.070 0.019 230 0.30 0.084 0.698 9/23/21 19:42 BRF o-Xylene 17 0.035 0.0093 73 0.15 0.041 0.698 9/23/21 19:42 BRF Surrogates 4-Bromofluorobenzene (1) 4-Bromofluorobenzene (1) % Recovery % REC Limits 93.9 70-130 96.3 70-130 9/24/21 6:42 9/23/21 19:42 Page 13 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Charlotte, NC Date Received: 9/20/2021 Field Sample #: IA-DUP Sample ID: 21I1199-05 Sample Matrix: Indoor air Sampled: 9/16/2021 00:00 Sample Description/Location: Sub Description/Location: Canister ID: 1958 Canister Size: 6 liter Flow Controller ID: 3643 Sample Type: 8 hr Work Order: 21I1199 Initial Vacuum(in Hg): -30 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -6.2 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Acetone 6.8 1.4 0.84 16 3.3 2.0 0.698 9/23/21 20:14 BRF Benzene 0.13 0.035 0.0084 0.43 0.11 0.027 0.698 9/23/21 20:14 BRF Benzyl chloride ND 0.035 0.016 ND 0.18 0.081 0.698 9/23/21 20:14 BRF Bromodichloromethane ND 0.035 0.013 ND 0.23 0.085 0.698 9/23/21 20:14 BRF Bromoform ND 0.035 0.013 ND 0.36 0.13 0.698 9/23/21 20:14 BRF Bromomethane ND 0.035 0.028 ND 0.14 0.11 0.698 9/23/21 20:14 BRF 1,3-Butadiene ND 0.035 0.024 ND 0.077 0.054 0.698 9/23/21 20:14 BRF 2-Butanone (MEK) 0.46 1.4 0.12 J 1.3 4.1 0.34 0.698 9/23/21 20:14 BRF Carbon Disulfide ND 0.35 0.089 ND 1.1 0.28 0.698 9/23/21 20:14 BRF Carbon Tetrachloride 0.070 0.035 0.011 0.44 0.22 0.066 0.698 9/23/21 20:14 BRF Chlorobenzene ND 0.035 0.010 ND 0.16 0.048 0.698 9/23/21 20:14 BRF Chloroethane ND 0.035 0.025 ND 0.092 0.067 0.698 9/23/21 20:14 BRF Chloroform 0.056 0.035 0.0084 0.27 0.17 0.041 0.698 9/23/21 20:14 BRF Chloromethane 0.62 0.070 0.014 1.3 0.14 0.030 0.698 9/23/21 20:14 BRF Cyclohexane ND 0.035 0.023 ND 0.12 0.079 0.698 9/23/21 20:14 BRF Dibromochloromethane ND 0.035 0.012 ND 0.30 0.100 0.698 9/23/21 20:14 BRF 1,2-Dibromoethane (EDB) ND 0.035 0.0098 ND 0.27 0.075 0.698 9/23/21 20:14 BRF 1,2-Dichlorobenzene ND 0.035 0.013 ND 0.21 0.078 0.698 9/23/21 20:14 BRF 1,3-Dichlorobenzene ND 0.035 0.0084 ND 0.21 0.051 0.698 9/23/21 20:14 BRF 1,4-Dichlorobenzene ND 0.035 0.014 ND 0.21 0.085 0.698 9/23/21 20:14 BRF Dichlorodifluoromethane (Freon 12) 0.54 0.035 0.011 2.7 0.17 0.053 0.698 9/23/21 20:14 BRF 1,1-Dichloroethane ND 0.035 0.012 ND 0.14 0.047 0.698 9/23/21 20:14 BRF 1,2-Dichloroethane ND 0.035 0.013 ND 0.14 0.052 0.698 9/23/21 20:14 BRF 1,1-Dichloroethylene ND 0.035 0.014 ND 0.14 0.054 0.698 9/23/21 20:14 BRF cis-1,2-Dichloroethylene ND 0.035 0.012 ND 0.14 0.047 0.698 9/23/21 20:14 BRF trans-1,2-Dichloroethylene ND 0.035 0.012 ND 0.14 0.048 0.698 9/23/21 20:14 BRF 1,2-Dichloropropane ND 0.035 0.013 ND 0.16 0.058 0.698 9/23/21 20:14 BRF cis- 1,3 -Dichloropropene ND 0.035 0.016 ND 0.16 0.073 0.698 9/23/21 20:14 BRF trans- 1, 3 -Dichloropropene ND 0.035 0.011 ND 0.16 0.049 0.698 9/23/21 20:14 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) 0.020 0.035 0.012 J 0.14 0.24 0.084 0.698 9/23/21 20:14 BRF 1,4-Dioxane ND 0.35 0.024 ND 1.3 0.085 0.698 9/23/21 20:14 BRF Ethanol 11 1.4 0.42 20 2.6 0.80 0.698 9/23/21 20:14 BRF Ethyl Acetate ND 0.35 0.21 L-03, V-34 ND 1.3 0.75 0.698 9/23/21 20:14 BRF Ethylbenzene 0.084 0.035 0.0090 0.36 0.15 0.039 0.698 9/23/21 20:14 BRF 4-Ethyltoluene ND 0.035 0.011 ND 0.17 0.053 0.698 9/23/21 20:14 BRF Heptane 0.084 0.035 0.014 0.35 0.14 0.059 0.698 9/23/21 20:14 BRF Hexachlorobutadiene ND 0.035 0.019 V-05 ND 0.37 0.21 0.698 9/23/21 20:14 BRF Hexane 0.21 1.4 0.11 J 0.75 4.9 0.40 0.698 9/23/21 20:14 BRF 2-Hexanone (MBK) ND 0.070 0.018 ND 0.29 0.072 0.698 9/23/21 20:14 BRF Isopropanol 0.86 1.4 0.32 J 2.1 3.4 0.79 0.698 9/23/21 20:14 BRF Methyl tert-Butyl Ether (MTBE) ND 0.035 0.014 ND 0.13 0.050 0.698 9/23/21 20:14 BRF Methylene Chloride 0.51 0.35 0.080 1.8 1.2 0.28 0.698 9/23/21 20:14 BRF 4-Methyl-2-pentanone (MIBK) ND 0.035 0.018 ND 0.14 0.073 0.698 9/23/21 20:14 BRF Naphthalene 0.036 0.035 0.022 0.19 0.18 0.12 0.698 9/23/21 20:14 BRF Propene ND 1.4 0.12 ND 2.4 0.20 0.698 9/23/21 20:14 BRF Styrene 0.028 0.035 0.011 J 0.12 0.15 0.047 0.698 9/23/21 20:14 BRF 1,1,2,2-Tetrachloroethane ND 0.035 0.011 ND 0.24 0.073 0.698 9/23/21 20:14 BRF Page 14 of 40 con -test® A Pace Analytical Laboratory Project Location: Charlotte, NC Date Received: 9/20/2021 Field Sample #: IA-DUP Sample ID: 21I1199-05 Sample Matrix: Indoor air Sampled: 9/ 16/2021 00:00 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 1958 Canister Size: 6 liter Flow Controller ID: 3643 Sample Type: 8 hr Work Order: 21I1199 Initial Vacuum(in Hg): -30 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -6.2 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 0.013 0.035 0.010 J 0.085 0.24 0.070 0.698 9/23/21 20:14 BRF Tetrahydrofuran ND 0.35 0.086 ND 1.0 0.25 0.698 9/23/21 20:14 BRF Toluene 0.35 0.035 0.015 1.3 0.13 0.055 0.698 9/23/21 20:14 BRF 1,2,4-Trichlorobenzene ND 0.070 0.024 V-04 ND 0.52 0.18 0.698 9/23/21 20:14 BRF 1, 1, 1 -Trichloroethane ND 0.035 0.016 ND 0.19 0.088 0.698 9/23/21 20:14 BRF 1,1,2-Trichloroethane ND 0.035 0.014 ND 0.19 0.076 0.698 9/23/21 20:14 BRF Trichloroethylene ND 0.035 0.013 ND 0.19 0.069 0.698 9/23/21 20:14 BRF Trichlorofluoromethane (Freon 11) 0.26 0.14 0.014 1.4 0.78 0.078 0.698 9/23/21 20:14 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.085 0.14 0.012 J 0.65 1.1 0.095 0.698 9/23/21 20:14 BRF 1,2,4-Trimethylbenzene 0.042 0.035 0.010 0.21 0.17 0.051 0.698 9/23/21 20:14 BRF 1,3,5-Trimethylbenzene 0.011 0.035 0.0096 J 0.055 0.17 0.047 0.698 9/23/21 20:14 BRF Vinyl Acetate ND 0.70 0.065 ND 2.5 0.23 0.698 9/23/21 20:14 BRF Vinyl Chloride ND 0.035 0.014 ND 0.089 0.035 0.698 9/23/21 20:14 BRF m&p-Xylene 0.27 0.070 0.019 1.2 0.30 0.084 0.698 9/23/21 20:14 BRF o-Xylene 0.11 0.035 0.0093 0.46 0.15 0.041 0.698 9/23/21 20:14 BRF Surrogates 4-Bromofluorobenzene (1) % Recovery 92.9 % REC Limits 70-130 9/23/21 20:14 Page 15 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Charlotte, NC Date Received: 9/20/2021 Field Sample #: AA-1 Sample ID: 21I1199-06 Sample Matrix: Ambient Air Sampled: 9/16/2021 18:30 Sample Description/Location: Sub Description/Location: Canister ID: 1104 Canister Size: 6 liter Flow Controller ID: 3349 Sample Type: 8 hr Work Order: 21I1199 Initial Vacuum(in Hg): -28 Final Vacuum(in Hg): -6 Receipt Vacuum(in Hg): -6.8 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RI MDL Dilution Analyzed Analyst Acetone 27 1.4 0.84 64 3.3 2.0 0.698 9/23/21 20:47 BRF Benzene 0.25 0.035 0.0084 0.81 0.11 0.027 0.698 9/23/21 20:47 BRF Benzyl chloride ND 0.035 0.016 ND 0.18 0.081 0.698 9/23/21 20:47 BRF Bromodichloromethane ND 0.035 0.013 ND 0.23 0.085 0.698 9/23/21 20:47 BRF Bromoform ND 0.035 0.013 ND 0.36 0.13 0.698 9/23/21 20:47 BRF Bromomethane ND 0.035 0.028 ND 0.14 0.11 0.698 9/23/21 20:47 BRF 1,3-Butadiene ND 0.035 0.024 ND 0.077 0.054 0.698 9/23/21 20:47 BRF 2-Butanone (MEK) 2.0 1.4 0.12 5.8 4.1 0.34 0.698 9/23/21 20:47 BRF Carbon Disulfide ND 0.35 0.089 ND 1.1 0.28 0.698 9/23/21 20:47 BRF Carbon Tetrachloride 0.068 0.035 0.011 0.43 0.22 0.066 0.698 9/23/21 20:47 BRF Chlorobenzene ND 0.035 0.010 ND 0.16 0.048 0.698 9/23/21 20:47 BRF Chloroethane ND 0.035 0.025 ND 0.092 0.067 0.698 9/23/21 20:47 BRF Chloroform 0.062 0.035 0.0084 0.30 0.17 0.041 0.698 9/23/21 20:47 BRF Chloromethane 0.63 0.070 0.014 1.3 0.14 0.030 0.698 9/23/21 20:47 BRF Cyclohexane 0.43 0.035 0.023 1.5 0.12 0.079 0.698 9/23/21 20:47 BRF Dibromochloromethane ND 0.035 0.012 ND 0.30 0.100 0.698 9/23/21 20:47 BRF 1,2-Dibromoethane (EDB) ND 0.035 0.0098 ND 0.27 0.075 0.698 9/23/21 20:47 BRF 1,2-Dichlorobenzene ND 0.035 0.013 ND 0.21 0.078 0.698 9/23/21 20:47 BRF 1,3-Dichlorobenzene ND 0.035 0.0084 ND 0.21 0.051 0.698 9/23/21 20:47 BRF 1,4-Dichlorobenzene ND 0.035 0.014 ND 0.21 0.085 0.698 9/23/21 20:47 BRF Dichlorodifluoromethane (Freon 12) 0.70 0.035 0.011 3.5 0.17 0.053 0.698 9/23/21 20:47 BRF 1,1-Dichloroethane ND 0.035 0.012 ND 0.14 0.047 0.698 9/23/21 20:47 BRF 1,2-Dichloroethane 0.028 0.035 0.013 J 0.11 0.14 0.052 0.698 9/23/21 20:47 BRF 1,1-Dichloroethylene ND 0.035 0.014 ND 0.14 0.054 0.698 9/23/21 20:47 BRF cis-1,2-Dichloroethylene ND 0.035 0.012 ND 0.14 0.047 0.698 9/23/21 20:47 BRF trans-1,2-Dichloroethylene ND 0.035 0.012 ND 0.14 0.048 0.698 9/23/21 20:47 BRF 1,2-Dichloropropane ND 0.035 0.013 ND 0.16 0.058 0.698 9/23/21 20:47 BRF cis- 1,3 -Dichloropropene ND 0.035 0.016 ND 0.16 0.073 0.698 9/23/21 20:47 BRF trans- 1, 3 -Dichloropropene ND 0.035 0.011 ND 0.16 0.049 0.698 9/23/21 20:47 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.012 ND 0.24 0.084 0.698 9/23/21 20:47 BRF 1,4-Dioxane ND 0.35 0.024 ND 1.3 0.085 0.698 9/23/21 20:47 BRF Ethanol 370 20 6.1 690 38 11 10 9/24/21 7:07 BRF Ethyl Acetate ND 0.35 0.21 L-03, V-34 ND 1.3 0.75 0.698 9/23/21 20:47 BRF Ethylbenzene 15 0.035 0.0090 65 0.15 0.039 0.698 9/23/21 20:47 BRF 4-Ethyltoluene 0.13 0.035 0.011 0.62 0.17 0.053 0.698 9/23/21 20:47 BRF Heptane 0.19 0.035 0.014 0.77 0.14 0.059 0.698 9/23/21 20:47 BRF Hexachlorobutadiene ND 0.035 0.019 V-05 ND 0.37 0.21 0.698 9/23/21 20:47 BRF Hexane 0.32 1.4 0.11 J 1.1 4.9 0.40 0.698 9/23/21 20:47 BRF 2-Hexanone (MBK) ND 0.070 0.018 ND 0.29 0.072 0.698 9/23/21 20:47 BRF Isopropanol 13 1.4 0.32 31 3.4 0.79 0.698 9/23/21 20:47 BRF Methyl tert-Butyl Ether (MTBE) ND 0.035 0.014 ND 0.13 0.050 0.698 9/23/21 20:47 BRF Methylene Chloride 0.20 0.35 0.080 J 0.68 1.2 0.28 0.698 9/23/21 20:47 BRF 4-Methyl-2-pentanone (MIBK) ND 0.035 0.018 ND 0.14 0.073 0.698 9/23/21 20:47 BRF Naphthalene 0.43 0.035 0.022 2.3 0.18 0.12 0.698 9/23/21 20:47 BRF Propene ND 1.4 0.12 ND 2.4 0.20 0.698 9/23/21 20:47 BRF Styrene 0.28 0.035 0.011 1.2 0.15 0.047 0.698 9/23/21 20:47 BRF 1,1,2,2-Tetrachloroethane ND 0.035 0.011 ND 0.24 0.073 0.698 9/23/21 20:47 BRF Page 16 of 40 con -test® A Pace Analytical Laboratory Project Location: Charlotte, NC Date Received: 9/20/2021 Field Sample #: AA-1 Sample ID: 21I1199-06 Sample Matrix: Ambient Air Sampled: 9/ 16/2021 18:30 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 1104 Canister Size: 6 liter Flow Controller ID: 3349 Sample Type: 8 hr Work Order: 21I1199 Initial Vacuum(in Hg): -28 Final Vacuum(in Hg): -6 Receipt Vacuum(in Hg): -6.8 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 0.017 0.035 0.010 J 0.12 0.24 0.070 0.698 9/23/21 20:47 BRF Tetrahydrofuran 1.1 0.35 0.086 3.3 1.0 0.25 0.698 9/23/21 20:47 BRF Toluene 1.1 0.035 0.015 4.1 0.13 0.055 0.698 9/23/21 20:47 BRF 1,2,4-Trichlorobenzene ND 0.070 0.024 V-04 ND 0.52 0.18 0.698 9/23/21 20:47 BRF 1, 1, 1 -Trichloroethane ND 0.035 0.016 ND 0.19 0.088 0.698 9/23/21 20:47 BRF 1,1,2-Trichloroethane ND 0.035 0.014 ND 0.19 0.076 0.698 9/23/21 20:47 BRF Trichloroethylene ND 0.035 0.013 ND 0.19 0.069 0.698 9/23/21 20:47 BRF Trichlorofluoromethane (Freon 11) 3.5 0.14 0.014 20 0.78 0.078 0.698 9/23/21 20:47 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.086 0.14 0.012 J 0.66 1.1 0.095 0.698 9/23/21 20:47 BRF 1,2,4-Trimethylbenzene 0.78 0.035 0.010 3.8 0.17 0.051 0.698 9/23/21 20:47 BRF 1,3,5-Trimethylbenzene 0.15 0.035 0.0096 0.74 0.17 0.047 0.698 9/23/21 20:47 BRF Vinyl Acetate ND 0.70 0.065 ND 2.5 0.23 0.698 9/23/21 20:47 BRF Vinyl Chloride ND 0.035 0.014 ND 0.089 0.035 0.698 9/23/21 20:47 BRF m&p-Xylene 50 0.070 0.019 220 0.30 0.084 0.698 9/23/21 20:47 BRF o-Xylene 16 0.035 0.0093 69 0.15 0.041 0.698 9/23/21 20:47 BRF Surrogates 4-Bromofluorobenzene (1) 4-Bromofluorobenzene (1) % Recovery % REC Limits 94.3 70-130 96.6 70-130 9/24/21 7:07 9/23/21 20:47 Page 17 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Sample Extraction Data Prep Method: TO-15 Prep -EPA TO-15 Pre-Dil Pre-Dil Default Actual Pressure Pre Initial Final Injection Injection Lab Number [Field ID] Batch Dilution Dilution mL mL mL mL Date 21III99-OIRE1 [IA-1] B290908 1.5 1 N/A 1000 200 30 09/24/21 21I1199-02RE1 [IA-2] B290908 1.5 1 N/A 1000 200 30 09/24/21 21I1199-03RE1 [IA-3] B290908 1.5 1 N/A 1000 200 30 09/24/21 Prep Method: TO-15 Prep -EPA TO-15 Pre-Dil Pre-Dil Default Actual Pressure Pre Initial Final Injection Injection Lab Number [Field ID] Batch Dilution Dilution mL mL mL mL Date 21I1199-01 [IA-1] B290913 1.5 1 N/A 1000 200 430 09/23/21 21I1199-02 [IA-2] B290913 1.5 1 N/A 1000 200 430 09/23/21 21I1199-03 [IA-3] B290913 1.5 1 N/A 1000 200 430 09/23/21 Prep Method: TO-15 Prep -EPA TO-15 Pre-Dil Pre-Dil Default Actual Pressure Pre Initial Final Injection Injection Lab Number [Field ID] Batch Dilution Dilution mL mL mL mL Date 21I1199-04 [IA-4] B290914 1.5 1 N/A 1000 200 430 09/23/21 21I1199-04RE1 [IA-4] B290914 1.5 1 N/A 1000 200 30 09/23/21 21I1199-05 [IA-DUP] B290914 1.5 1 N/A 1000 200 430 09/23/21 21I1199-06 [AA-1] B290914 1.5 1 N/A 1000 200 430 09/23/21 21I1199-06RE1 [AA-1] B290914 1.5 1 N/A 1000 200 30 09/23/21 Page 18 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD Analyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qual Batch B290908 - TO-15 Prep Blank (B290908-BLK1) Prepared: 09/23/21 Analyzed: 09/24/21 Ethanol ND 0.80 Surrogate: 4-Bromofluorobenzene (1) 7.54 8.00 94.2 70-130 LCS (B290908-BSI) Prepared: 09/23/21 Analyzed: 09/24/21 Ethanol 6.38 5.00 128 70-130 Surrogate: 4-Bromofluorobenzene (1) 7.65 8.00 95.6 70-130 Batch B290913 - TO-15 Prep Blank (B290913-BLK1) Prepared & Analyzed: 09/23/21 Acetone ND 0.80 Benzene ND 0.020 Benzyl chloride ND 0.020 Bromodichloromethane ND 0.020 Bromoform ND 0.020 Bromomethane ND 0.020 1,3-Butadiene ND 0.020 2-Butanone (MEK) ND 0.80 Carbon Disulfide ND 0.20 Carbon Tetrachloride 0.0068 0.020 J Chlorobenzene ND 0.020 Chloroethane ND 0.020 Chloroform ND 0.020 Chloromethane ND 0.040 Cyclohexane ND 0.020 Dibromochloromethane ND 0.020 1,2-Dibromoethane (EDB) ND 0.020 1,2-Dichlorobenzene ND 0.020 1,3-Dichlorobenzene ND 0.020 1,4-Dichlorobenzene ND 0.020 Dichlorodifluoromethane (Freon 12) ND 0.020 1, 1 -Dichloroethane ND 0.020 1,2-Dichloroethane ND 0.020 1,1-Dichloroethylene ND 0.020 cis-1,2-Dichloroethylene ND 0.020 trans-1,2-Dichloroethylene ND 0.020 1,2-Dichloropropane ND 0.020 cis-1,3-Dichloropropene ND 0.020 trans- l,3-Dichloropropene ND 0.020 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane ND 0.020 (Freon 114) 1,4-Dioxane ND 0.20 Ethanol ND 0.80 Ethyl Acetate ND 0.20 L-03 Ethylbenzene 0.0084 0.020 J 4-Ethyltoluene ND 0.020 Heptane ND 0.020 Page 19 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD .nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua Batch B290913 - TO-15 Prep Blank (B290913-BLKI) Prepared & Analyzed: 09/23/21 Hexachlorobutadiene ND 0.020 Hexane ND 0.80 2-Hexanone (MBK) ND 0.020 Isopropanol ND 0.80 Methyl tert-Butyl Ether (MTBE) ND 0.020 Methylene Chloride ND 0.20 4-Methyl-2-pentanone (MIBK) ND 0.020 Naphthalene ND 0.020 Propene ND 0.80 Styrene ND 0.020 1,1,2,2-Tetrachloroethane ND 0.020 Tetrachloroethylene ND 0.020 Tetrahydrofuran ND 0.20 Toluene ND 0.020 1,2,4-Trichlorobenzene ND 0.020 1, 1, 1 -Trichloroethane ND 0.020 1,1,2-Trichloroethane ND 0.020 Trichloroethylene ND 0.020 Trichlorofluoromethane (Freon 11) ND 0.080 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon ND 0.080 113) 1,2,4-Trimethylbenzene ND 0.020 1,3,5-Trimethylbenzene ND 0.020 Vinyl Acetate ND 0.40 Vinyl Chloride ND 0.020 m&p-Xylene 0.018 0.040 1 o-Xylene 0.0084 0.020 J Surrogate: 4-Bromofluorobenzene (1) 7.58 8.00 94.7 70-130 Page 20 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B290913 - TO-15 Prep LCS (B290913-BS1) Prepared & Analyzed: 09/23/21 Acetone 4.79 5.00 95.8 70-130 Benzene 4.62 5.00 92.3 70-130 Benzyl chloride 5.16 5.00 103 70-130 Bromodichloromethane 4.75 5.00 95.0 70-130 Bromoform 5.40 5.00 108 70-130 Bromomethane 5.10 5.00 102 70-130 1,3-Butadiene 4.76 5.00 95.2 70-130 2-Butanone (MEK) 4.74 5.00 94.8 70-130 Carbon Disulfide 5.74 5.00 115 70-130 Carbon Tetrachloride 4.67 5.00 93.4 70-130 Chlorobenzene 4.64 5.00 92.7 70-130 Chloroethane 5.25 5.00 105 70-130 Chloroform 5.00 5.00 100 70-130 Chloromethane 4.75 5.00 95.0 70-130 Cyclohexane 4.43 5.00 88.6 70-130 Dibromochloromethane 4.82 5.00 96.5 70-130 1,2-Dibromoethane (EDB) 4.77 5.00 95.5 70-130 1,2-Dichlorobenzene 5.39 5.00 108 70-130 1,3-Dichlorobenzene 5.34 5.00 107 70-130 1,4-Dichlorobenzene 5.13 5.00 103 70-130 Dichlorodifluoromethane(Freon 12) 5.24 5.00 105 70-130 1,1-Dichloroethane 4.86 5.00 97.1 70-130 1,2-Dichloroethane 4.79 5.00 95.9 70-130 1,1-Dichloroethylene 4.97 5.00 99.3 70-130 cis-1,2-Dichloroethylene 4.90 5.00 97.9 70-130 trans-1,2-Dichloroethylene 4.78 5.00 95.5 70-130 1,2-Dichloropropane 4.55 5.00 91.0 70-130 cis- 1,3 -Dichloropropene 5.01 5.00 100 70-130 trans- 1, 3 -Dichloropropene 4.74 5.00 94.8 70-130 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane 4.65 5.00 93.0 70-130 (Freon 114) 1,4-Dioxane 5.16 5.00 103 70-130 Ethanol 6.28 5.00 126 70-130 Ethyl Acetate 3.49 5.00 69.8 * 70-130 L-03 Ethylbenzene 4.89 5.00 97.9 70-130 4-Ethyltoluene 5.22 5.00 104 70-130 Heptane 3.84 5.00 76.7 70-130 Hexachlorobutadiene 5.39 5.00 108 70-130 Hexane 4.86 5.00 97.3 70-130 2-Hexanone (MBK) 5.07 5.00 101 70-130 Isopropanol 4.01 5.00 80.2 70-130 Methyl tert-Butyl Ether (MTBE) 4.70 5.00 93.9 70-130 Methylene Chloride 4.86 5.00 97.2 70-130 4-Methyl-2-pentanone (MIBK) 4.92 5.00 98.5 70-130 Naphthalene 5.64 5.00 113 70-130 Propene 5.04 5.00 101 70-130 Styrene 5.07 5.00 101 70-130 Page 21 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B290913 - TO-15 Prep LCS (B290913-BS1) Prepared & Analyzed: 09/23/21 1,1,2,2-Tetrachloroethane 5.05 5.00 101 70-130 Tetrachloroethylene 4.99 5.00 99.7 70-130 Tetrahydrofuran 4.50 5.00 90.0 70-130 Toluene 4.61 5.00 92.1 70-130 1,2,4-Trichlorobenzene 5.67 5.00 113 70-130 1, 1, 1 -Trichloroethane 4.76 5.00 95.2 70-130 1,1,2-Trichloroethane 4.52 5.00 90.5 70-130 Trichloroethylene 5.10 5.00 102 70-130 Trichlorofluoromethane (Freon 11) 5.19 5.00 104 70-130 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 5.97 5.00 119 70-130 113) 1,2,4-Trimethylbenzene 5.07 5.00 101 70-130 1,3,5-Trimethylbenzene 4.86 5.00 97.2 70-130 Vinyl Acetate 6.59 5.00 132 * 70-130 L-01, V-3E Vinyl Chloride 5.37 5.00 107 70-130 m&p-Xylene 9.61 10.0 96.1 70-130 o-Xylene 5.06 5.00 101 70-130 Surrogate: 4-BromoJluorobenzene (1) 8.19 8.00 102 70-130 Batch B290914 - TO-15 Prep Blank (B290914-BLK1) Prepared & Analyzed: 09/23/21 Acetone ND 0.80 Benzene ND 0.020 Benzyl chloride ND 0.020 Bromodichloromethane ND 0.020 Bromoform ND 0.020 Bromomethane ND 0.020 1,3-Butadiene ND 0.020 2-Butanone (MEK) ND 0.80 Carbon Disulfide ND 0.20 Carbon Tetrachloride ND 0.020 Chlorobenzene ND 0.020 Chloroethane ND 0.020 Chloroform ND 0.020 Chloromethane ND 0.040 Cyclohexane ND 0.020 Dibromochloromethane ND 0.020 1,2-Dibromoethane (EDB) ND 0.020 1,2-Dichlorobenzene ND 0.020 1,3-Dichlorobenzene ND 0.020 1,4-Dichlorobenzene ND 0.020 Dichlorodifluoromethane (Freon 12) ND 0.020 1,1-Dichloroethane ND 0.020 1,2-Dichloroethane ND 0.020 1,1-Dichloroethylene ND 0.020 cis-1,2-Dichloroethylene ND 0.020 Page 22 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD .nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua Batch B290914 - TO-15 Prep Blank (B290914-BLKI) Prepared & Analyzed: 09/23/21 trans-1,2-Dichloroethylene ND 0.020 1,2-Dichloropropane ND 0.020 cis- 1,3 -Dichloropropene ND 0.020 trans- l,3-Dichloropropene ND 0.020 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane ND 0.020 (Freon 114) 1,4-Dioxane ND 0.20 Ethanol ND 0.80 Ethyl Acetate ND 0.20 L-03, V-34 Ethylbenzene ND 0.020 4-Ethyltoluene ND 0.020 Heptane ND 0.020 Hexachlorobutadiene ND 0.020 V-05 Hexane ND 0.80 2-Hexanone (MBK) ND 0.020 Isopropanol ND 0.80 Methyl tert-Butyl Ether (MTBE) ND 0.020 Methylene Chloride ND 0.20 4-Methyl-2-pentanone (MIBK) ND 0.020 Naphthalene ND 0.020 Propene ND 0.80 Styrene ND 0.020 1,1,2,2-Tetrachloroethane ND 0.020 Tetrachloroethylene ND 0.020 Tetrahydrofuran ND 0.20 Toluene ND 0.020 1,2,4-Trichlorobenzene ND 0.020 V-04 1, 1, 1 -Trichloroethane ND 0.020 1,1,2-Trichloroethane ND 0.020 Tichloroethylene ND 0.020 Trichlorofluoromethane (Freon 11) ND 0.080 1,1,2-Tichloro-1,2,2-trifluoroethane (Freon ND 0.080 113) 1,2,4-Trimethylbenzene ND 0.020 1,3,5-Trimethylbenzene ND 0.020 Vinyl Acetate ND 0.40 Vinyl Chloride ND 0.020 m&p-Xylene ND 0.040 o-Xylene ND 0.020 Surrogate: 4-BromoJluorobenzene (I) 7.58 8.00 94.7 70-130 Page 23 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B290914 - TO-15 Prep LCS (B290914-BS1) Prepared & Analyzed: 09/23/21 Acetone 4.28 5.00 85.7 70-130 Benzene 5.28 5.00 106 70-130 Benzyl chloride 6.50 5.00 130 70-130 Bromodichloromethane 4.83 5.00 96.5 70-130 Bromoform 5.05 5.00 101 70-130 Bromomethane 6.16 5.00 123 70-130 1,3-Butadiene 5.86 5.00 117 70-130 2-Butanone (MEK) 4.38 5.00 87.6 70-130 Carbon Disulfide 6.05 5.00 121 70-130 Carbon Tetrachloride 4.29 5.00 85.8 70-130 Chlorobenzene 4.95 5.00 99.0 70-130 Chloroethane 6.33 5.00 127 70-130 Chloroform 5.15 5.00 103 70-130 Chloromethane 5.45 5.00 109 70-130 Cyclohexane 4.98 5.00 99.7 70-130 Dibromochloromethane 5.00 5.00 99.9 70-130 1,2-Dibromoethane (EDB) 5.07 5.00 101 70-130 1,2-Dichlorobenzene 5.07 5.00 101 70-130 1,3-Dichlorobenzene 5.40 5.00 108 70-130 1,4-Dichlorobenzene 5.19 5.00 104 70-130 Dichlorodifluoromethane(Freon 12) 5.22 5.00 104 70-130 1,1-Dichloroethane 5.26 5.00 105 70-130 1,2-Dichloroethane 4.37 5.00 87.4 70-130 1,1-Dichloroethylene 5.44 5.00 109 70-130 cis-1,2-Dichloroethylene 5.04 5.00 101 70-130 trans-1,2-Dichloroethylene 4.95 5.00 98.9 70-130 1,2-Dichloropropane 4.98 5.00 99.7 70-130 cis- 1,3 -Dichloropropene 5.26 5.00 105 70-130 trans- 1, 3 -Dichloropropene 5.32 5.00 106 70-130 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane 5.54 5.00 111 70-130 (Freon 114) 1,4-Dioxane 5.32 5.00 106 70-130 Ethanol 6.28 5.00 126 70-130 Ethyl Acetate 3.48 5.00 69.5 * 70-130 L-03,V-34 Ethylbenzene 5.15 5.00 103 70-130 4-Ethyltoluene 5.36 5.00 107 70-130 Heptane 4.95 5.00 99.1 70-130 Hexachlorobutadiene 3.70 5.00 74.0 70-130 V-05 Hexane 4.44 5.00 88.8 70-130 2-Hexanone (MBK) 4.95 5.00 99.0 70-130 Isopropanol 3.92 5.00 78.4 70-130 Methyl tert-Butyl Ether (MTBE) 4.85 5.00 97.1 70-130 Methylene Chloride 5.02 5.00 100 70-130 4-Methyl-2-pentanone (MIBK) 5.42 5.00 108 70-130 Naphthalene 5.44 5.00 109 70-130 Propene 5.07 5.00 101 70-130 Styrene 5.50 5.00 110 70-130 Page 24 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD .nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua Batch B290914 - TO-15 Prep LCS (B290914-BS1) Prepared & Analyzed: 09/23/21 1,1,2,2-Tetrachloroethane 5.37 5.00 107 70-130 Tetrachloroethylene 4.52 5.00 90.4 70-130 Tetrahydrofuran 4.29 5.00 85.7 70-130 Toluene 5.14 5.00 103 70-130 1,2,4-Trichlorobenzene 4.88 5.00 97.6 70-130 V-04 1, 1, 1 -Trichloroethane 4.31 5.00 86.2 70-130 1,1,2-Trichloroethane 5.04 5.00 101 70-130 Trichloroethylene 4.98 5.00 99.6 70-130 Trichlorofluoromethane (Freon 11) 5.19 5.00 104 70-130 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 5.99 5.00 120 70-130 113) 1,2,4-Trimethylbenzene 4.97 5.00 99.4 70-130 1,3,5-Trimethylbenzene 5.01 5.00 100 70-130 Vinyl Acetate 6.44 5.00 129 70-130 V-3E Vinyl Chloride 6.28 5.00 126 70-130 m&p-Xylene 10.2 10.0 102 70-130 o-Xylene 5.03 5.00 101 70-130 Surrogate: 4-Bromofluorobenzene (1) 7.61 8.00 95.1 70-130 Page 25 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 ` TEL. 413/525-2332 Note: Blank Subtraction is not performed unless otherwise noted FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. t Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level RL Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference LCS Laboratory Control Sample LCS Dup Duplicate Laboratory Control Sample MS Matrix Spike Sample MS Dup Duplicate Matrix Spike Sample REC Recovery QC Quality Control ppbv Parts per billion volume EPA United States Environmental Protection Agency % REC Percent Recovery ND Not Detected N/A Not Applicable DL Detection Limit NC Not Calculated LFB/LCS Lab Fortified Blank/Lab Control Sample ORP Oxidation -Reduction Potential wet Not dry weight corrected % wt Percent weight Kg Kilogram g Gram mg Milligram µg Microgram ng Nanogram L Liter mL Milliliter µL Microliter m3 Cubic Meter EPH Extractable Petroleum Hydrocarbons VPH Volatile Petroleum Hydrocarbons APH Air Petroleum Hydrocarbons FID Flame Ionization Detector PID Photo Ionization Detector Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). L-01 Laboratory fortified blank/laboratory control sample recovery outside of control limits. Data validation is not affected since all results are "not detected" for all samples in this batch for this compound and bias is on the high side. L-03 Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this compound is likely to be biased on the low side. V-04 Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method specified criteria. Reported result is estimated. V-05 Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound. V-34 Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is estimated. V-35 Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this compound. Reported result is estimated. V-36 Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. Page 26 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 TPH Thomas P. Hnitecki RLF Rebecca Faust STATION PDF Management Station KKM Kerry K. McGee BRF Brittany R. Fisk ANALYST Page 27 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Initial Cal Check (S062606-ICV1) Lab File ID: J21A232023.D Analyzed: 08/21/21 02:04 Bromochloromethane (1) 152325 2.866 150879 2.863 101 60 - 140 0.0030 +/-0.50 1,4-Difluorobenzene(1) 700372 3.471 694423 3.468 101 60-140 0.0030 +/-0.50 Chlorobenzene-d5(1) 652377 5.056 641566 5.057 102 60-140 -0.0010 +/-0.50 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Initial Cal Check (S063338-ICV1) Lab File ID: K21A259025.13 Analyzed: 09/16/21 23:09 Bromochloromethane (1) 65004 2.989 65617 2.992 99 60 - 140 -0.0030 +/-0.50 1,4-Difluorobenzene(1) 208463 3.592 200888 3.595 104 60-140 -0.0030 +/-0.50 Chlorobenzene-d5(1) 167501 5.185 162778 5.188 103 60-140 -0.0030 +/-0.50 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Calibration Check (S063573-CCV1) Lab File ID: J2IA267004.D Analyzed: 09/24/21 09:40 Bromochloromethane (1) 160833 2.863 150879 2.863 107 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 797554 3.468 694423 3.468 115 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 744007 5.053 641566 5.057 116 60-140 -0.0040 +/-0.50 LCS (B290908-BS1 ) Lab File ID: J21A267005.D Analyzed: 09/24/21 10:06 Bromochloromethane (1) 162105 2.86 160833 2.863 101 60 - 140 -0.0030 +/-0.50 1,4-Difluorobenzene(1) 794587 3.468 797554 3.468 100 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 743683 5.053 744007 5.053 100 60-140 0.0000 +/-0.50 Blank (B290908-BLK1) Lab File ID: J21A267008.D Analyzed: 09/24/21 11:37 Bromochloromethane (1) 161497 2.85 160833 2.863 100 60 - 140 -0.0130 +/-0.50 1,4-Difluorobenzene(1) 776970 3.459 797554 3.468 97 60-140 -0.0090 +/-0.50 Chlorobenzene-d5(1) 712481 5.05 744007 5.053 96 60-140 -0.0030 +/-0.50 IA-1 (2111199-01RE1) Lab File ID: J2IA267035.D Analyzed: 09/25/21 01:28 Bromochloromethane (1) 150140 2.85 160833 2.863 93 60 - 140 -0.0130 +/-0.50 1,4-Difluorobenzene(1) 747510 3.458 797554 3.468 94 60-140 -0.0100 +/-0.50 Chlorobenzene-d5(1) 676403 5.05 744007 5.053 91 60-140 -0.0030 +/-0.50 IA-2 (2111199-02RE1) Lab File ID: J2IA267036.13 Analyzed: 09/25/21 01:53 Bromochloromethane (1) 147939 2.85 160833 2.863 92 60 - 140 -0.0130 +/-0.50 1,4-Difluorobenzene(1) 728506 3.459 797554 3.468 91 60-140 -0.0090 +/-0.50 Chlorobenzene-d5(1) 666377 5.051 744007 5.053 90 60-140 -0.0020 +/-0.50 Page 28 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area % Limits RT Diff RT Diff Limit Q IA-3 (2111199-03RE1) Lab File ID: J21A267037.D Analyzed: 09/25/21 02:18 Bromochloromethane (1) 150913 2.85 160833 2.863 94 60 - 140 -0.0130 +/-0.50 1,4-Difluorobenzene(1) 739425 3.462 797554 3.468 93 60-140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 683089 5.051 744007 5.053 92 60-140 -0.0020 +/-0.50 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area % Limits RT Diff RT Diff Limit Q Calibration Check (S063579-CCV1) Lab File ID: K21A266004.13 Analyzed: 09/23/21 09:38 Bromochloromethane (1) 56022 2.992 65617 2.992 85 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 171584 3.595 200888 3.595 85 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 145496 5.188 162778 5.188 89 60-140 0.0000 +/-0.50 LCS (B290913-BS1 ) Lab File ID: K21A266005.13 Analyzed: 09/23/21 10:10 Bromochloromethane (1) 56833 2.992 56022 2.992 101 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 180913 3.598 171584 3.595 105 60-140 0.0030 +/-0.50 Chlorobenzene-d5(1) 144330 5.188 145496 5.188 99 60-140 0.0000 +/-0.50 Blank (B290913-BLK1) Lab File ID: K21A266008.13 Analyzed: 09/23/21 12:01 Bromochloromethane (1) 62952 2.992 56022 2.992 112 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 180763 3.598 171584 3.595 105 60-140 0.0030 +/-0.50 Chlorobenzene-d5(1) 155964 5.188 145496 5.188 107 60-140 0.0000 +/-0.50 IA-1 (2111199-01) Lab File ID: K21A266035.13 Analyzed: 09/24/21 05:36 Bromochloromethane (1) 67373 2.992 56022 2.992 120 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 225007 3.598 171584 3.595 131 60-140 0.0030 +/-0.50 Chlorobenzene-d5(1) 188343 5.188 145496 5.188 129 60-140 0.0000 +/-0.50 IA-2 (2111199-02 ) Lab File ID: K21A266036.13 Analyzed: 09/24/21 06:12 Bromochloromethane (1) 65936 2.992 56022 2.992 118 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 223152 3.598 171584 3.595 130 60-140 0.0030 +/-0.50 Chlorobenzene-d5(1) 187810 5.188 145496 5.188 129 60-140 0.0000 +/-0.50 IA-3 (2111199-03) Lab File ID: K21A266037.1) Analyzed: 09/24/21 06:50 Bromochloromethane (1) 67526 2.992 56022 2.992 121 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 236949 3.595 171584 3.595 138 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 184939 5.188 145496 5.188 127 60-140 0.0000 +/-0.50 INTERNAL STANDARD AREA AND RT SUMMARY EPA TO-15 Reference Reference Area % RT Diff Internal Standard Response RT Response RT Area % Limits 11 RT Diff Limit Q Page 29 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Calibration Check (S063580-CCV1) Lab File ID: J21A266006.D Analyzed: 09/23/21 12:22 Bromochloromethane (1) 170036 2.86 150879 2.863 113 60 - 140 -0.0030 +/-0.50 1,4-Difluorobenzene(1) 840594 3.468 694423 3.468 121 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 777364 5.054 641566 5.057 121 60-140 -0.0030 +/-0.50 LCS (B290914-BS1 ) Lab File ID: J21A266007.D Analyzed: 09/23/21 12:48 Bromochloromethane (1) 174614 2.86 170036 2.86 103 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 855895 3.468 840594 3.468 102 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 797196 5.054 777364 5.054 103 60-140 0.0000 +/-0.50 Blank (B290914-BLK1) Lab File ID: J21A266010.D Analyzed: 09/23/21 14:16 Bromochloromethane (1) 172704 2.85 170036 2.86 102 60 - 140 -0.0100 +/-0.50 1,4-Difluorobenzene(1) 828463 3.459 840594 3.468 99 60-140 -0.0090 +/-0.50 Chlorobenzene-d5(1) 751077 5.05 777364 5.054 97 60-140 -0.0040 +/-0.50 IA-4 (2111199-04 ) Lab File ID: J21A266019.D Analyzed: 09/23/21 19:42 Bromochloromethane (1) 168505 2.85 170036 2.86 99 60 - 140 -0.0100 +/-0.50 1,4-Difluorobenzene(1) 825994 3.462 840594 3.468 98 60-140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 760970 5.05 777364 5.054 98 60-140 -0.0040 +/-0.50 IA-DUP (2111199-05) Lab File ID: J2IA266020.D Analyzed: 09/23/21 20:14 Bromochloromethane (1) 172371 2.85 170036 2.86 101 60 - 140 -0.0100 +/-0.50 1,4-Difluorobenzene(1) 829463 3.462 840594 3.468 99 60-140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 765403 5.053 777364 5.054 98 60-140 -0.0010 +/-0.50 AA-1 (21I1199-06 ) Lab File ID: J2IA266021.D Analyzed: 09/23/21 20:47 Bromochloromethane (1) 172020 2.85 170036 2.86 101 60 - 140 -0.0100 +/-0.50 1,4-Difluorobenzene(1) 832110 3.459 840594 3.468 99 60-140 -0.0090 +/-0.50 Chlorobenzene-d5(1) 762420 5.054 777364 5.054 98 60-140 0.0000 +/-0.50 IA-4 (2111199-04RE1) Lab File ID: J2IA266029.1) Analyzed: 09/24/21 06:42 Bromochloromethane (1) 158486 2.85 170036 2.86 93 60 - 140 -0.0100 +/-0.50 1,4-Difluorobenzene(1) 778316 3.462 840594 3.468 93 60-140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 729916 5.05 777364 5.054 94 60-140 -0.0040 +/-0.50 AA-1 (21I1199-06RE1) Lab File ID: J21A266030.13 Analyzed: 09/24/21 07:07 Bromochloromethane (1) 167906 2.85 170036 2.86 99 60 - 140 -0.0100 +/-0.50 1,4-Difluorobenzene(1) 798557 3.462 840594 3.468 95 60-140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 729258 5.05 777364 5.054 94 60-140 -0.0040 +/-0.50 Page 30 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S063573-CCV 1 COMPOUND TYPE CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) Ethanol A 5.00 6.00 0.1363511 0.1635386 19.9 30 # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk * Values outside of QC limits Page 31 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S063579-CCV 1 COMPOUND TYPE. CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) Acetone A 5.00 5.18 1.044997 1.08246 3.6 30 Benzene A 5.00 5.12 0.6772546 0.6939295 2.5 30 Benzyl chloride A 5.00 5.62 0.4517045 0.5074724 12.3 30 Bromodichloromethane A 5.00 5.36 0.4576082 0.4909549 7.3 30 Bromoform A 5.00 5.86 0.4225807 0.4956287 17.3 30 Bromomethane A 5.00 5.60 0.7358094 0.8248188 12.1 30 1,3-Butadiene A 5.00 5.25 0.6122438 0.643233 5.1 30 2-Butanone(MEK) A 5.00 4.75 1.117205 1.061469 -5.0 30 Carbon Disulfide A 5.00 6.02 1.700674 2.049052 20.5 30 Carbon Tetrachloride A 5.00 5.20 0.4399405 0.4575998 4.0 30 Chlorobenzene A 5.00 5.02 0.6710772 0.673844 0.4 30 Chloroethane A 5.00 5.44 0.4322339 0.4702724 8.8 30 Chloroform A 5.00 5.35 1.383001 1.480675 7.1 30 Chloromethane A 5.00 5.34 0.6957364 0.7428225 6.8 30 Cyclohexane A 5.00 4.97 0.2863864 0.2848284 -0.5 30 Dibromochloromethane A 5.00 5.24 0.5392756 0.565041 4.8 30 1,2-Dibromoethane (EDB) A 5.00 5.08 0.4882235 0.4959477 1.6 30 1,2-Dichlorobenzene A 5.00 5.63 0.5583295 0.6290537 12.7 30 1,3-Dichlorobenzene A 5.00 5.42 0.3904983 0.4236872 8.5 30 1,4-Dichlorobenzene A 5.00 5.28 0.6060934 0.6397647 5.6 30 Dichlorodifluoromethane (Freon 12) A 5.00 5.73 2.131798 2.441955 14.5 30 1,1-Dichloroethane A 5.00 5.32 1.070749 1.138524 6.3 30 1,2-Dichloroethane A 5.00 5.05 0.850621 0.8595195 1.0 30 1,1-Dichloroethylene A 5.00 5.28 1.199799 1.268187 5.7 30 cis-1,2-Dichloroethylene A 5.00 5.07 0.8960317 0.9092999 1.5 30 trans-1,2-Dichloroethylene A 5.00 5.33 0.9105593 0.9705616 6.6 30 1,2-Dichloropropane A 5.00 4.98 0.2471363 0.245981 -0.5 30 cis-1,3-Dichloropropene A 5.00 4.68 0.282988 0.2650783 -6.3 30 trans- l,3-Dichloropropene A 5.00 5.01 0.3201369 0.3209344 0.2 30 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane (Freon 1 A 5.00 5.44 2.193098 2.385434 8.8 30 1,4-Dioxane A 5.00 5.70 0.1252425 0.14268 13.9 30 Ethanol A 5.00 5.64 0.1614241 0.182157 12.8 30 Ethyl Acetate A 5.00 4.96 0.2630812 0.2608118 -0.9 30 Ethylbenzene A 5.00 5.21 1.130441 1.177489 4.2 30 4-Ethyltoluene A 5.00 5.54 1.136131 1.258239 10.7 30 Heptane A 5.00 4.64 0.1870834 0.1737132 -7.1 30 Hexachlorobutadiene A 5.00 5.52 0.353338 0.3902348 10A 30 Hexane L 5.00 5.39 0.5879851 0.6421763 7.9 30 Page 32 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S063579-CCV 1 COMPOUND TYPE CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) 2-Hexanone (MBK) A 5.00 5.23 0.4582989 0.4791664 4.6 30 Isopropanol A 5.00 5.38 1.230091 1.322995 7.6 30 Methyl tert-Butyl Ether (MTBE) A 5.00 5.11 1.735778 1.775074 2.3 30 Methylene Chloride A 5.00 5.32 0.7520661 0.8004855 6.4 30 4-Methyl-2-pentanone (MI13K) A 5.00 5.24 0.1956749 0.2052779 4.9 30 Naphthalene A 5.00 5.40 0.9756151 1.052873 7.9 30 Propene A 5.00 5.68 0.5977407 0.6789047 13.6 30 Styrene A 5.00 5.53 0.6328158 0.6998515 10.6 30 1,1,2,2-Tetrachloroethane A 5.00 5.34 0.6582366 0.7023368 6.7 30 Tetrachloroethylene A 5.00 5.41 0.3934633 0.4257657 8.2 30 Tetrahydroforan A 5.00 4.92 0.6580954 0.6470601 -1.7 30 Toluene A 5.00 5.04 0.959144 0.9665145 0.8 30 1,2,4-Trichlorobenzene A 5.00 5.65 0.375898 0.4248529 13.0 30 1, 1, 1 -Trichloroethane A 5.00 5.56 0.471714 0.5248042 11.3 30 1,1,2-Trichloroethane A 5.00 4.67 0.3462991 0.3232749 -6.6 30 Trichloroethylene A 5.00 5.70 0.2556787 0.2913931 14.0 30 Trichlorofluoromethane(Freon 11) A 5.00 5.62 1.972353 2.215016 12.3 30 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 11 A 5.00 5.74 1.00369 1.151776 14.8 30 1,2,4-Trimethylbenzene A 5.00 5.41 0.9612681 1.039688 8.2 30 1,3,5-Trimethylbenzene A 5.00 5.41 0.7473243 0.8087645 8.2 30 Vinyl Acetate A 5.00 4.69 0.8051633 0.7551034 -6.2 30 Vinyl Chloride A 5.00 5.55 0.7945618 0.8816536 11.0 30 m&p-Xylene A 10.0 10.3 0.9266552 0.9567108 3.2 30 o-Xylene A 5.00 5.38 0.8546217 0.9186782 7.5 30 # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk * Values outside of QC limits Page 33 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S063580-CCV 1 COMPOUND TYPE. CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) Acetone A 5.00 4.50 1.013483 0.9118822 -10.0 30 Benzene A 5.00 5.68 0.5773346 0.6564101 13.7 30 Benzyl chloride A 5.00 6.00 0.5662092 0.6798298 20.1 30 Bromodichloromethane A 5.00 4.79 0.4493554 0.4307183 -4.1 30 Bromoform A 5.00 4.88 0.6972692 0.6812479 -2.3 30 Bromomethane A 5.00 6.07 0.795872 0.966026 21.4 30 1,3-Butadiene A 5.00 6.00 0.4907101 0.5884495 19.9 30 2-Butanone (MEK) A 5.00 4.36 1.40087 1.220447 -12.9 30 Carbon Disulfide A 5.00 6.12 1.998984 2.44639 22.4 30 Carbon Tetrachloride A 5.00 4.28 0.5188025 0.443888 -14.4 30 Chlorobenzene A 5.00 4.94 0.7193 0.7106169 -1.2 30 Chloroethane A 5.00 6.21 0.3795632 0.4713731 24.2 30 Chloroform A 5.00 5.17 1.888134 1.953375 3.5 30 Chloromethane A 5.00 5.41 0.5417118 0.5859936 8.2 30 Cyclohexane A 5.00 5.00 0.265344 0.2652372 -0.04 30 Dibromochloromethane A 5.00 4.93 0.6098379 0.6016826 -1.3 30 1,2-Dibromoethane(EDB) A 5.00 5.10 0.4553549 0.4640503 1.9 30 1,2-Dichlorobenzene A 5.00 4.75 0.757862 0.7204141 -4.9 30 1,3-Dichlorobenzene A 5.00 5.15 0.7367625 0.7588846 3.0 30 1,4-Dichlorobenzene A 5.00 5.03 0.7493582 0.7542063 0.6 30 Dichlorodifluoromethane (Freon 12) A 5.00 5.17 2.185662 2.259832 3.4 30 1,1-Dichloroethane A 5.00 5.04 1.41636 1.427971 0.8 30 1,2-Dichloroethane A 5.00 4.33 1.131436 0.9799619 -13.4 30 1,1-Dichloroethylene A 5.00 5.18 1.038306 1.076619 3.7 30 cis-1,2-Dichloroethylene A 5.00 5.05 1.058854 1.070032 1.1 30 trans-1,2-Dichloroethylene A 5.00 4.95 1.144971 1.132795 -1.1 30 1,2-Dichloropropane A 5.00 4.88 0.2035658 0.1988023 -2.3 30 cis-1,3-Dichloropropene A 5.00 5.17 0.3153762 0.3261065 3.4 30 trans- l,3-Dichloropropene A 5.00 5.01 0.2855395 0.2863423 0.3 30 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane (Freon 1 A 5.00 5.96 2.0897 2.490277 19.2 30 1,4-Dioxane A 5.00 5.34 0.1348394 0.1439477 6.8 30 Ethanol A 5.00 6.04 0.1363511 0.1647275 20.8 30 Ethyl Acetate A 5.00 4.71 0.2996362 0.2820579 -5.9 30 Ethylbenzene A 5.00 5.16 1.068394 1.102999 3.2 30 4-Ethyltoluene A 5.00 5.23 1.191921 1.246821 4.6 30 Heptane A 5.00 4.96 0.1598388 0.1585812 -0.8 30 Hexachlorobutadiene A 5.00 3.47 1.05506 0.7331052 -30.5 30 Hexane L 5.00 4.42 0.7820405 0.6355078 -11.7 30 Page 34 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S063580-CCV 1 COMPOUND TYPE CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) 2-Hexanone (MBK) A 5.00 5.34 0.3105363 0.3317262 6.8 30 Isopropanol A 5.00 4.68 1.087458 1.018278 -6.4 30 Methyl tert-Butyl Ether (MTBE) A 5.00 4.92 2.400388 2.361467 -1.6 30 Methylene Chloride A 5.00 4.88 0.6720844 0.6559458 -2.4 30 4-Methyl-2-pentanone (MI13K) A 5.00 6.02 0.141787 0.1705917 20.3 30 Naphthalene A 5.00 4.73 1.049522 0.9925214 -5.4 30 Propene A 5.00 5.33 0.4575591 0.4877649 6.6 30 Styrene A 5.00 5.31 0.6387272 0.6784693 6.2 30 1,1,2,2-Tetrachloroethane A 5.00 5.31 0.5691929 0.6047 6.2 30 Tetrachloroethylene A 5.00 4.59 0.5934671 0.5451325 -8.1 30 Tetrahydroforan A 5.00 4.49 0.811293 0.7278459 -10.3 30 Toluene A 5.00 5.04 0.8381161 0.8456394 0.9 30 1,2,4-Trichlorobenzene A 5.00 4.52 0.5285083 0.4775544 -9.6 30 1, 1, 1 -Trichloroethane A 5.00 4.41 0.4533588 0.3999648 -11.8 30 1,1,2-Trichloroethane A 5.00 4.91 0.2953724 0.2898822 -1.9 30 Trichloroethylene A 5.00 4.76 0.2950588 0.2806853 4.9 30 Trichlorofluoromethane(Freon 11) A 5.00 5.16 2.216429 2.285276 3.1 30 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 11 A 5.00 5.86 1.637043 1.9179 17.2 30 1,2,4-Trimethylbenzene A 5.00 4.78 1.051818 1.005225 -4.4 30 1,3,5-Trimethylbenzene A 5.00 4.84 1.056033 1.022831 -3.1 30 Vinyl Acetate A 5.00 4.20 1.072956 0.9015879 -16.0 30 Vinyl Chloride A 5.00 6.23 0.6636142 0.8264885 24.5 30 m&p-Xylene A 10.0 10.1 0.8662275 0.8721793 0.7 30 o-Xylene A 5.00 4.92 0.8477905 0.8333579 -1.7 30 # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk * Values outside of QC limits Page 35 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte EPA TO-15 in Air Acetone Benzene Benzyl chloride Bromodichloromethane Bromoform Bromomethane 1,3-Butadiene 2-Butanone (MEK) Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane Cyclohexane Dibromochloromethane 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane (Freon 12) 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethylene cis-1,2-Dichloroethylene trans- l,2-Dichloro ethylene 1,2-Dichloropropane cis- 1,3 -Dichloropropene trans- 1, 3 -Dichloropropene 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) 1,4-Dioxane Ethanol Ethyl Acetate Ethylbenzene 4-Ethyltoluene Heptane Hexachlorobutadiene Hexane 2-Hexanone (MBK) Isopropanol Methyl tart -Butyl Ether (MTBE) Methylene Chloride 4-Methyl-2-pentanone (MIBK) Naphthalene Propene Styrene 1,1,2,2-Tetrachloroethane Certifications AIHA,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA, FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH,VA AIHA,NY,ME,NH AIHA,NJ,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NY,ME,NH AIHA,NJ,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA AIHA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ AIHA,NJ,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA, FL,NJ,NY,ME,NH, VA AIHA AIHA,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH NY,ME,NH AIHA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA Page 36 of 40 con -test® A Pace Analytical Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte EPA TO-15 in Air Tetrachloroethylene Tetrahydrofuran Toluene 1,2,4-Trichlorobenzene 1, 1, 1 -Trichloroethane 1,1,2-Trichloroethane Trichloroethylene Trichlorofluoromethane (Freon 11) 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl Chloride m&p-Xylene o-Xylene Certifications AIHA,FL,NJ,NY,ME,NH, VA AIHA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NY,ME,NH AIHA,NJ,NY,ME,NH,VA AIHA,NJ,NY,ME,NH AIHA,NJ,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA, FL,NJ,NY,ME,NH, VA AIHA, FL,NJ,NY,ME,NH, VA Con -Test, a Pace Environmental Laboratory, operates under the following certifications and accreditation: Code Description Number Expires AHIA AIHA-LAP, LLC - ISO17025:2017 100033 03/l/2022 MA Massachusetts DEP M-MA100 06/30/2022 CT Connecticut Department of Publilc Health PH-0165 12/31/2022 NY New York State Department of Health 10899 NELAP 04/l/2022 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2022 RI Rhode Island Department of Health LA000112 12/30/2021 NC North Carolina Div. of Water Quality 652 12/31/2021 NJ New Jersey DEP MA007 NELAP 06/30/2022 FL Florida Department of Health E871027 NELAP 06/30/2022 VT Vermont Department of Health Lead Laboratory LL720741 07/30/2022 ME State of Maine MA00100 06/9/2023 VA Commonwealth of Virginia 460217 12/14/2021 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2022 VT-DW Vermont Department of Health Drinking Water VT-255716 06/12/2022 NC-DW North Carolina Department of Health 25703 07/31/2022 PA Commonwealth of Pennsylvania DEP 68-05812 06/30/2022 MI Dept. of Env, Great Lakes, and Energy 9100 09/6/2022 Page 37 of 40 c-n M Co A cvi N q S7 p . Ii. N O ti cLab Receipt Pressure an f Final Pressure a Initial Pressure uc 2 ° ltE w f� Q, M M uj O v Ew,t a co n 0 0 Q m l a of e 7 0 > fl w XLu N O1 O M Q 3 Cr U jif an Y u-No u °i •� F rt 9 o N a n V E V U [`7 M N t 0 kn `t in kn ram' uNk &V A �Qn 4 ti V T •R s o X ac. U- € n & 17 0 E � � E u .. Z 055, C o y E a an p ac, d N J Z :9 m c -0 0 U �o V •0 V 0 a a a -° E a a •�, ci cL a 0 U � ,.`�, rj I i M :mil Vk 11 .( ark x (5 v L c Nz a �" � � Ln � o 'oLn a w u z U X O a a- c N z IF N O ❑ ❑ � am ifQ u taa ` nc,mo H E v aL a s E to a c. c N O ❑ ❑ N 0 ° c x 6 a a c a c d _ a ° c � ❑ u ° a n u a, o I� p c rr c, m 3 L m u 3 F V) °n ..J C n o. ❑❑❑ ZE R p w O 1 m ._ m T Af a yea L V V c a a y= N a C 9 El U Ch N R V � N Q] a � ❑ ❑ c E ° Li u V ❑ ❑ ❑ E a e F= E v w DD an >, a .o N > Cr n a (, Page 38 of 40 9122121, 6:48 PM Detailed Tracking TRACK ANOTHER SHIPMENT 987548455539 ADD NICKNAME Delivered Wednesday, September 22, 2021 at 12:05 pm THIS IS 1 OF S PIECES DELIVERED Signed for by: AALINE GET STATUS UPDATES OBTAIN PROOF OF DELIVERY FROM TO Huntersville, NC US East Longmeadow, MA US 5 Piece Shipment TRACKING ID STATUS SHIP DELIVERY HANDLING PIECE SHIPPER CITY, DATE DATE UNITS STATE 967548455539 (master) Delivered 9/20/21 9/22/21 C Hun€ersville NC 98754845554E Delivered 9/20/21 9/22/21 0 Huntersville NC 98754845555D Delivered 9/20/21 9/22/21 0 Huntersville NC 9875,184555�)1 Delivered 9/20/21 9/22/21 0 Huntersville NC 987548455572 Delivered 9120/21 9/22/21 0 Huntersville NC Travel History TIME ZONE Local Scan Time hUps://www.fedex .com/fed extrack/?trkn br=987548455539&trkq ua l=12022-987548455539—F D EG it 0 RECIPIENT CITY, STATE EAST LONGMEADOW MA EAST LONGMEADOW MA EAST LONGMEADOW MA EAST LONGMEADOW MA EAST LONGMEADOW MA O Page 39 of 40 I Have Not Confirmed Sample Container Numbers With Lab Staff Before Relinquishing Over Samples Air Media Sample Receipt Checklist - (Rejection Criteria Listing - Using Acceptance Policy) Any False Statement will be brought to the attention of the Client - State True or False Client Received By Date E Time is -- How were the samples In Cooler On Ice No Ice received? In Box Ambient Melted Ice Were samples within Temperature By Gun # Actual Temp - Compliance? 2-6'C By Blank # Actual Temp - Was Custody Seal Intact? Was COC Relinquished ? Are there any loose caps/valves on any samples? Is COC in ink/ Legible?�Is N7 .. . Were Samples Tampered with? Does Chain Agree With Samples? Did COC Include all Client( Analysis 7 Sampler Name -A. Pertinent Information? Project ID's Collection Dates/Times Are Sample Labels filled out and legible? Are there Rushes? _ �- Samples are received within holding time? Proper Media Used? 7 Are there Trip Blanks? -I-_ Who was notified? Individually Certified Cans? \_LL_ is there enough Volume? f Page 40 of 40 APPENDIX D Table 1 Summary of Subslab Vapor Analytical Data Seneca Place Shopping Center Charlotte, North Carolina H&H Job No. AZA-001 Screening Criteria Former Malone's Pourhouse Former PersonalFormer Touch Dry- Cleaning Baby USA Hook & Tire Sample ID VMP-1 VMP-2 VMP-3 VMP-4 VMP-5 DWM Non -Residential SGSL1 DWM Residential SGSLZ Sample Date 5/5/2015 5/5/2015 5/5/2015 5/5/2015 5/5/2015 Units u /m3 u /m3 u /m3 u /m3 u /m3 u /m3 u /m3 VOCs (TO-15) Acetone 2,720,000 21,600 150 B 76 B 86 B 200 B 330 B Benzene 1,570 120 1.8 1.2 1.7 2.0 2.1 2-Butanone (MEK) 438,000 34,800 21 J 181 14 J 181 191 Carbon Disulfide 61,300 4,870 12 15 11 10 8.7 Chloroform 533 40.7 0.94 J <0.98 0.23 J <0.98 <0.98 Chloromethane 7,880 626 0.74 J <0.83 0.40 J <0.83 0.45 J Cyclohexane 526,000 41,700 <0.69 2.1 <0.69 4.2 2.9 1,4-Dichlorobenzene 1,110 85.1 1.2 J 0.89 J 1.9 1.1 J 0.82 J Dichlorodifluoromethane (Freon 12) 8,760 695 440 B 2.9 B 2.5 B 7.7 B 4.4 B 1,2-Dichloroethane 472 36.0 <0.81 1.8 <0.81 2.0 1.8 Ethanol NS NS 120 19 24 74 180 Ethyl Acetate 6,130 487 7.9 <0.72 2.8 <0.72 <0.72 Ethylbenzene 4,910 374 3.2 4.9 2.0 6.2 11 4-Ethyltoluene NS NS 0.92 J 2.5 1.8 12 50 Heptane NS NS 1.2 4.6 1.1 23 140 Hexane 61,300 4,870 8.5 B, J 680 B 21 B, J 1,900 B 1,500 B 2-Hexanone (MBK) 2,630 209 4.3 <0.82 3.1 <0.82 <0.82 Isopropanol NS NS 26 13 J 8.6 J 16 J 16 J Methylene Chloride 52,600 4,170 1.3 B, J 0.97 B, J 1.2 B, J 1.4 B, J 1.1 B, J 4-Methyl-2-pentanone (MIBK) 263,000 20,900 2.5 <0.82 3.0 19 4.8 Naphthalene 263 20.9 0.96 J 2.1 9.8 2.3 35 Propene 263,000 20,900 5.1 J <14 <14 <14 <14 Styrene 87,600 6,950 5.9 2.0 4.7 1.9 2.0 Tetrachloroethylene 3,500 278 13 6,600 57 31 1,300 Tetrahydrofuran 175,000 13,900 3.6 3.9 1.4 1.9 1.5 Toluene 438,000 34,800 19 20 11 24 24 1, 1, 1 -Trichloroethane 438,000 34,800 <1.1 <1.1 0.83 J <1.1 <1.1 Trichloroethylene 175 13.9 <1.1 0.32 J <1.1 <1.1 <1.1 Trichlorofluoromethane (Freon 11) 61,300 4,870 32 120 120 3.0 J 3.4 J 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 2,630,000 209,000 5.4 J 4.8 J 5.5 J 5.6 J 5.7 J 1,2,4-Trimethylbenzene 613 34.8 4.9 12 17 25 260 1,3,5-Trimethylbenzene NS NS 1.0 4.9 4.2 12 76 Xylene, Total 8,760 695 9.8 43 10.3 38 103 Notes: 1) NC Department of Environment and Natural Resources (DENR) Divison of Waste Management Non -Residential Subslab Soil Gas Screening Levels (June 2014) 2) NC Department of Environment and Natural Resources (DENR) Divison of Waste Management Residential Subslab Soil Gas Screening Levels (June 2014) Only those compounds detected in at least one sample shown above Bold indicates an exceedance of the Non -Residential Subslab Soil Gas Screening Level (SGSL) B = Analyte is found in the associated blank as well as in the sample J = Detected but below the reporting limit (lowest calibration standard); therefore, result is an estimated concentration VOCs = volatile organic compounds NS = screening criteria not specified; µg/m3 = micro grams per cubic meter Table 1 S:WAA-Master Projects\Azalea Management (AZA)\AZA.001 Seneca Place BRIndoor Air Report\Data Table Hart & Hickman, PC APPENDIX E Risk for Individual Pathways r Version Date: June 2021 Basis: May 2021 EPA RSL Table Site ID: Seneca Place Suite H Exposure Unit ID: IA-1 DIRECT CONTACT SOIL AND WATER CALCULATORS Receptor Pathway CarcinogenicRiskHazard Index Risk exceeded? Resident Soil NC NC NC Groundwater Use* NC NC NC Non -Residential Worker Soil NC NC NC Groundwater Use* NC NC NC Construction Worker Soil NC NC NC Recreator/Trespasser Soil NC NC NC Surface Water* NC NC NC VAPOR INTRUSION CALCULATORS Receptor Pathway CarcinogenicRiskHazard Index Risk exceeded? Resident Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air NC NC NC Indoor Air 9.7E-05 4.2E+00 YES Non -Residential Worker Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air NC NC NC Indoor Air 2.2E-05 1.0E+00 NO CONTAMINANT MIGRATION CALCULATORS Pathway Source Target Receptor Concentrations Exceeded? Groundwater Source Soil Exceedence of 2L at Receptor? NC Source Groundwater Exceedence of 2L at Receptor? NC Surface Water Source Soil Exceedence of 2B at Receptor? NC Source Groundwater Exceedence of 2B at Receptor? NC Notes: 1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations. 2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk -based closure. 3. NM = Not Modeled 4. NC = Pathway not calculated North Carolina DEQ Risk Calculator Risk for Individual Pathways r Version Date: June 2021 Basis: May 2021 EPA RSL Table Site ID: Seneca Place Suite H Exposure Unit ID: IA-2 DIRECT CONTACT SOIL AND WATER CALCULATORS Receptor Pathway CarcinogenicRiskHazard Index Risk exceeded? Resident Soil NC NC NC Groundwater Use* NC NC NC Non -Residential Worker Soil NC NC NC Groundwater Use* NC NC NC Construction Worker Soil NC NC NC Recreator/Trespasser Soil NC NC NC Surface Water* NC NC NC VAPOR INTRUSION CALCULATORS Receptor Pathway CarcinogenicRiskHazard Index Risk exceeded? Resident Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air NC NC NC Indoor Air 8.7E-05 3.6E+00 YES Non -Residential Worker Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air NC NC NC Indoor Air 2.0E-05 8.5E-01 NO CONTAMINANT MIGRATION CALCULATORS Pathway Source Target Receptor Concentrations Exceeded? Groundwater Source Soil Exceedence of 2L at Receptor? NC Source Groundwater Exceedence of 2L at Receptor? NC Surface Water Source Soil Exceedence of 2B at Receptor? NC Source Groundwater Exceedence of 2B at Receptor? NC Notes: 1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations. 2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk -based closure. 3. NM = Not Modeled 4. NC = Pathway not calculated North Carolina DEQ Risk Calculator Risk for Individual Pathways r Version Date: June 2021 Basis: May 2021 EPA RSL Table Site ID: Seneca Place Suite H Exposure Unit ID: IA-3 DIRECT CONTACT SOIL AND WATER CALCULATORS Receptor Pathway CarcinogenicRiskHazard Index Risk exceeded? Resident Soil NC NC NC Groundwater Use* NC NC NC Non -Residential Worker Soil NC NC NC Groundwater Use* NC NC NC Construction Worker Soil NC NC NC Recreator/Trespasser Soil NC NC NC Surface Water* NC NC NC VAPOR INTRUSION CALCULATORS Receptor Pathway CarcinogenicRiskHazard Index Risk exceeded? Resident Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air NC NC NC Indoor Air 8.1E-05 3.5E+00 YES Non -Residential Worker Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air NC NC NC Indoor Air 1.9E-05 8.2E-01 NO CONTAMINANT MIGRATION CALCULATORS Pathway Source Target Receptor Concentrations Exceeded? Groundwater Source Soil Exceedence of 2L at Receptor? NC Source Groundwater Exceedence of 2L at Receptor? NC Surface Water Source Soil Exceedence of 2B at Receptor? NC Source Groundwater Exceedence of 2B at Receptor? NC Notes: 1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations. 2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk -based closure. 3. NM = Not Modeled 4. NC = Pathway not calculated North Carolina DEQ Risk Calculator Risk for Individual Pathways r Version Date: June 2021 Basis: May 2021 EPA RSL Table Site ID: Seneca Place Suite H Exposure Unit ID: IA-4 DIRECT CONTACT SOIL AND WATER CALCULATORS Receptor Pathway CarcinogenicRiskHazard Index Risk exceeded? Resident Soil NC NC NC Groundwater Use* NC NC NC Non -Residential Worker Soil NC NC NC Groundwater Use* NC NC NC Construction Worker Soil NC NC NC Recreator/Trespasser Soil NC NC NC Surface Water* NC NC NC VAPOR INTRUSION CALCULATORS Receptor Pathway CarcinogenicRiskHazard Index Risk exceeded? Resident Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air NC NC NC Indoor Air 8.5E-05 3.6E+00 YES Non -Residential Worker Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air NC NC NC Indoor Air 2.0E-05 8.6E-01 NO CONTAMINANT MIGRATION CALCULATORS Pathway Source Target Receptor Concentrations Exceeded? Groundwater Source Soil Exceedence of 2L at Receptor? NC Source Groundwater Exceedence of 2L at Receptor? NC Surface Water Source Soil Exceedence of 2B at Receptor? NC Source Groundwater Exceedence of 2B at Receptor? NC Notes: 1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations. 2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk -based closure. 3. NM = Not Modeled 4. NC = Pathway not calculated North Carolina DEQ Risk Calculator Risk for Individual Pathways r Version Date: June 2021 Basis: May 2021 EPA RSL Table Site ID: Seneca Place Suite H Exposure Unit ID: SG-1 DIRECT CONTACT SOIL AND WATER CALCULATORS Receptor Pathway CarcinogenicRiskHazard Index Risk exceeded? Resident Soil NC NC NC Groundwater Use* NC NC NC Non -Residential Worker Soil NC NC NC Groundwater Use* NC NC NC Construction Worker Soil NC NC NC Recreator/Trespasser Soil NC NC NC Surface Water* NC NC NC VAPOR INTRUSION CALCULATORS Receptor Pathway CarcinogenicRiskHazard Index Risk exceeded? Resident Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air 2.0E-06 1.2E-01 NO Indoor Air NC NC NC Non -Residential Worker Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air 1.5E-07 9.2E-03 NO Indoor Air NC NC NC CONTAMINANT MIGRATION CALCULATORS Pathway Source Target Receptor Concentrations Exceeded? Groundwater Source Soil Exceedence of 2L at Receptor? NC Source Groundwater Exceedence of 2L at Receptor? NC Surface Water Source Soil Exceedence of 2B at Receptor? NC Source Groundwater Exceedence of 2B at Receptor? NC Notes: 1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations. 2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk -based closure. 3. NM = Not Modeled 4. NC = Pathway not calculated North Carolina DEQ Risk Calculator Risk for Individual Pathways r Version Date: June 2021 Basis: May 2021 EPA RSL Table Site ID: Seneca Place Suite H Exposure Unit ID: SG-2 DIRECT CONTACT SOIL AND WATER CALCULATORS Receptor Pathway CarcinogenicRiskHazard Index Risk exceeded? Resident Soil NC NC NC Groundwater Use* NC NC NC Non -Residential Worker Soil NC NC NC Groundwater Use* NC NC NC Construction Worker Soil NC NC NC Recreator/Trespasser Soil NC NC NC Surface Water* NC NC NC VAPOR INTRUSION CALCULATORS Receptor Pathway CarcinogenicRiskHazard Index Risk exceeded? Resident Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air 1.3E-06 5.4E-02 NO Indoor Air NC NC NC Non -Residential Worker Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air 1.0E-07 4.3E-03 NO Indoor Air NC NC NC CONTAMINANT MIGRATION CALCULATORS Pathway Source Target Receptor Concentrations Exceeded? Groundwater Source Soil Exceedence of 2L at Receptor? NC Source Groundwater Exceedence of 2L at Receptor? NC Surface Water Source Soil Exceedence of 2B at Receptor? NC Source Groundwater Exceedence of 2B at Receptor? NC Notes: 1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations. 2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk -based closure. 3. NM = Not Modeled 4. NC = Pathway not calculated North Carolina DEQ Risk Calculator Risk for Individual Pathways r Version Date: June 2021 Basis: May 2021 EPA RSL Table Site ID: Seneca Place Suite H Exposure Unit ID: SG-3 DIRECT CONTACT SOIL AND WATER CALCULATORS Receptor Pathway CarcinogenicRiskHazard Index Risk exceeded? Resident Soil NC NC NC Groundwater Use* NC NC NC Non -Residential Worker Soil NC NC NC Groundwater Use* NC NC NC Construction Worker Soil NC NC NC Recreator/Trespasser Soil NC NC NC Surface Water* NC NC NC VAPOR INTRUSION CALCULATORS Receptor Pathway CarcinogenicRiskHazard Index Risk exceeded? Resident Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air 5.8E-06 9.8E-01 NO Indoor Air NC NC NC Non -Residential Worker Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air 4.4E-07 7.8E-02 NO Indoor Air NC NC NC CONTAMINANT MIGRATION CALCULATORS Pathway Source Target Receptor Concentrations Exceeded? Groundwater Source Soil Exceedence of 2L at Receptor? NC Source Groundwater Exceedence of 2L at Receptor? NC Surface Water Source Soil Exceedence of 2B at Receptor? NC Source Groundwater Exceedence of 2B at Receptor? NC Notes: 1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations. 2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk -based closure. 3. NM = Not Modeled 4. NC = Pathway not calculated North Carolina DEQ Risk Calculator Risk for Individual Pathways r Version Date: June 2021 Basis: May 2021 EPA RSL Table Site ID: Seneca Place Suite H Exposure Unit ID: SG-4 DIRECT CONTACT SOIL AND WATER CALCULATORS Receptor Pathway CarcinogenicRiskHazard Index Risk exceeded? Resident Soil NC NC NC Groundwater Use* NC NC NC Non -Residential Worker Soil NC NC NC Groundwater Use* NC NC NC Construction Worker Soil NC NC NC Recreator/Trespasser Soil NC NC NC Surface Water* NC NC NC VAPOR INTRUSION CALCULATORS Receptor Pathway CarcinogenicRiskHazard Index Risk exceeded? Resident Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air 1.7E-06 7.2E-02 NO Indoor Air NC NC NC Non -Residential Worker Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air 1.3E-07 5.7E-03 NO Indoor Air NC NC NC CONTAMINANT MIGRATION CALCULATORS Pathway Source Target Receptor Concentrations Exceeded? Groundwater Source Soil Exceedence of 2L at Receptor? NC Source Groundwater Exceedence of 2L at Receptor? NC Surface Water Source Soil Exceedence of 2B at Receptor? NC Source Groundwater Exceedence of 2B at Receptor? NC Notes: 1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations. 2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk -based closure. 3. NM = Not Modeled 4. NC = Pathway not calculated North Carolina DEQ Risk Calculator