MO-27698_47019_CA_MRP_20240118

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
January 18, 2024

Mr. Brad Newton
NCDEQ-UST Section
Mooresville Regional Office
610 East Center Ave.
Mooresville, NC 28115

Re: Ground Water Monitoring Report
December 2023
Kingsway #20
2201 Kendrick Road
Gastonia, Gaston County
North Carolina
Facility ID Number: 00-0-0000016201
Incident Number: 47019
GRI Project Number: 5351

Dear Mr. Newton,

Please find enclosed the referenced report for the above-mentioned site.
If you have any questions, please contact Ashleigh Thrash at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Mr. Mark King; Kingsway Enterprises, Inc., file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Ground Water Monitoring Report
December 2023
Kingsway #20
2201 Kendrick Road
Gastonia, Gaston County
North Carolina 28056
Facility ID Number: 00-0-0000016201
Incident Number: 47019
GRI Project Number: 5351

Prepared for:

Mr. Mark King
Kingsway Enterprises, Inc.
407 South Marietta Street
Gastonia, NC 28052

January 18, 2024

Ashleigh Thrash, P.G.
Project Manager
Eric M. Eubanks, P.G.
Report Writer

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 18, 2024 Kingsway #20
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5351
i
EXECUTIVE SUMMARY
Kingsway #20 is located at 2201 Kendrick Road in Gastonia, Gaston County, North Carolina. The site is
currently owned and operated by Kingsway Enterprises, Inc. as a petroleum retail facility. On May 30,
2019, three non-passing UST spill buckets were reported during triennial integrity testing activities. In
response, on March 18, 2020, GRI conducted a site check at the subject site. Three soil borings were
advanced adjacent to the spill buckets and soil samples were collected from the borings. Analytical results
from the soil samples collected during the site check indicated that he RAL and/or soil-to-water MCCs
were exceeded for multiple contaminants. Therefore, an LSA was required. The surrounding properties
are primarily residential. According to the information determined during receptor survey activities
conducted during the LSA in May 2020, two non-potable water supply wells were identified within a 1,500-
foot radius of the site. Public water is available to the subject site and to all surrounding properties. A
pond and creek were identified 1,250 feet south of the site.

A CAP has not yet been developed for the site. One AFVR event and one MMPE event have been
conducted at the site beginning in December 2020. Additionally, a free product skimmer was installed at
the site in March 2022 but was permanently removed during the December 2022 sampling event.

Based on the January 31, 2023, NORR from the NCDEQ, one monitoring well (MW-1) was abandoned at
the site and replaced with recovery well MW-1R on March 24, 2023. MW-1R was installed as a four-inch
well to a total depth of 35 feet BGS with a screened interval of 20 feet. MW-1R was installed in order to
aid in free product recovery at the site.

On December 19, 2023, nine monitoring wells, one recovery well, and one telescoping well were gauged,
purged, and/or sampled. Free product was observed in recovery well MW-1R. There was not enough
water in monitoring wells MW-2, MW-6, or MW-10 to collect a sample. The concentrations of VOCs
reported in the ground water samples collected from MW-3, MW-4, MW-7, and TW-1 exceeded the
MACs. All reported contaminant concentrations were below the GCLs.

Based on this information, the risk classification for the site should remain intermediate risk. GRI
recommends removing free product from MW-1R by conducting an AFVR. A comprehensive ground water
sampling event should be conducted approximately 30 days after the AFVR. The AFVR is tentatively
scheduled for May 2024.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 18, 2024 Kingsway #20
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5351
ii
SITE INFORMATION
1. Site Identification
 Kingsway #20 (Facility ID 00-0-0000016201)
 Incident Number 47019 – Intermediate Risk (I245A)
 Location of Source Area: 2201 Kendrick Road
Gastonia, NC 28056
Gaston County
35.213919°N, 81.133526°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST/AST Owner
Kingsway Enterprises, Inc.
407 S. Marietta Street
Gastonia, NC 28052
[e-mail]
704-718-7437

UST/AST Operator
Kingsway Enterprises, Inc.
407 S. Marietta Street
Gastonia, NC 28052
[e-mail]
704-718-7437

Property Owner
Kingsway Enterprises, Inc.
407 S. Marietta Street
Gastonia, NC 28052
[e-mail]
704-718-7437

Property Occupant
Kingsway Enterprises, Inc.
407 S. Marietta Street
Gastonia, NC 28052
[e-mail]
704-718-7437

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
Waypoint Analytical, LLC
449 Springbrook Rd.
Charlotte, NC 28217
State Certification No. 37735 and
402
704-529-6364
3. Information about Release
 Release was discovered on April 17, 2020
 An unknown amount of product was released from the leaking UST System via non-passing spill
buckets.
 Three 10,000-gallon gasoline USTs and associated pumps and product piping are active at the site.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 18, 2024 Kingsway #20
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5351
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
HERR: HAZMAT Emergency Response and
Remediation, Inc.
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 18, 2024 Kingsway #20
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5351
TABLE OF CONTENTS
EXECUTIVE SUMMARY ....................................................................................................................... i
SITE INFORMATION ............................................................................................................................ ii
ACRONYMS ....................................................................................................................................... iii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................2
3.0 FREE PRODUCT REMOVAL ........................................................................................................4
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................4
5.0 CONCLUSIONS .........................................................................................................................4
6.0 LIMITATIONS ...........................................................................................................................5
7.0 STATEMENTS AND CERTIFICATION ...........................................................................................5

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3A: Site Vicinity Map
Figure 3B: Zoning Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map

TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Receptor Information
Table 4: Adjacent Property Owner Information
Table 5: Well Construction and Gauging Information
Table 6: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: State Correspondence
Appendix B: Land Use Information
Appendix C: Incident Report
Appendix D: Historical Soil Quality Information
Appendix E: Laboratory Analytical Report

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 18, 2024 Kingsway #20
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5351
1
1.0 SITE HISTORY AND CHARACTERIZATION
GRI presents the results of the December 2023 ground water sampling event at the Kingsway #20 site
located at 2201 Kendrick Road in Gastonia, Gaston County, North Carolina. A topographic map showing
the general site location and the surrounding area is included as Figure 1. These activities were conducted
in accordance with GRI Proposal No. 23-450, which was submitted to the NCDEQ on August 15, 2023, and
was approved as Task Authorization No. 47019-09 on August 16, 2023. State correspondence is included
as Appendix A.

The site is currently owned and operated by Kingsway Enterprises, Inc. as a petroleum retail facility and
convenience store. A site check was conducted at the site in March 2020 following failed hydrostatic tests
for the three USTs and confirmed a release. Currently, three 10,000-gallon gasoline USTs are active at the
site. UST owner/operator information and UST system information are included as Table 1 and Table 2,
respectively. The Registered Tank Report is shown below:

The surrounding properties are primarily residential. A copy of the Land Use table is included as Appendix
B. The site contains one building (the store) and is primarily capped with asphalt. The overall topography
at the site is relatively flat with a slight downward slope to the east. Ten Type II monitoring wells (MW-1
through MW-10) and one Type III telescope well (TW-1) were installed at the site during previous ground
water assessment activities. A Site Map showing the locations of the monitoring wells and the structures
on-site is included as Figure 2.

On June 10, 2020, GRI personnel conducted a receptor survey at the site. Two non-potable water supply
wells were identified within 1,500 feet of the site. To date, the water supply wells have not been sampled.
Municipal water is available to the site and surrounding properties. A pond and a creek were identified
1,250 feet south of the site. Receptor information is included in Table 3. Adjacent property owner

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 18, 2024 Kingsway #20
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5351
2
information is included in Table 4. A Site Vicinity Map showing the adjacent properties and a Zoning Map
showing the zoning information are included as Figure 3A and Figure 3B, respectively.

No incidents have been reported on any adjacent properties. A copy of the NCDEQ Incident Report is
included as Appendix C. A map showing the locations of additional incidents in the vicinity of the site is
shown below:

A CAP has not been developed for the site. One AFVR event and one MMPE event have been conducted
at the site along with hand bailing and free product skimming. Approximately 571 gallons of contaminated
ground water and free product have been removed from the site to date. Please note that no projected
attenuation milestones have been established for the site.

Based on this information, the site was classified as intermediate risk. Corrective action should be
performed at the site until free product is no longer present and contaminant concentrations are below
the GCLs.
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
Soil assessment was not conducted during the current scope of work. Historical soil quality information
and soil excavation information is included as Appendix D.

On December 19, 2023, nine Type II monitoring wells (MW-2 through MW-10), one recovery well (MW-
1R) and one telescoping well (TW-1) were gauged, purged, and/or sampled in accordance with the NCDEQ
guidelines. Free product was observed in recovery well MW-1R. Depths to ground water in the Type II
monitoring wells ranged from 21.51 feet to 29.55 feet below TOC. Ground water elevations in the Type II
monitoring wells ranged from 70.70 feet to 77.34 feet. Ground water flow generally converged toward
47019

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 18, 2024 Kingsway #20
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5351
3
the center of the site from the east and west, then diverged to the north and south. The average horizontal
gradient of approximately 0.04 feet per foot. The vertical gradient could not be calculated, as MW-1 had
been abandoned and MW-1R has not been surveyed. Well construction and gauging information is
included in Table 5. A Water Table Surface Map based on the Type II monitoring wells is included as Figure
4. A summary of the current ground water gauging data is shown below:

Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
MW-1R 15 - 35 35 NM 25.78 --- NM
MW-2 13 - 28 28 99.93 26.53 --- 72.80
MW-3 20 - 35 35 99.90 27.82 --- 72.08
MW-4 13 - 28 28 100.39 27.53 --- 72.86
MW-5 16 - 31 31 98.85 21.51 --- 77.34
MW-6 15 - 30 30 101.53 29.55 --- 71.98
MW-7 11 - 26 26 99.97 25.94 --- 74.03
MW-8 15 - 30 30 99.05 28.35 --- 70.70
MW-9 15 - 30 30 99.23 28.19 --- 71.04
MW-10 15 - 30 30 100.49 29.13 --- 71.36
TW-1 45 - 50 50 99.96 29.30 --- 70.66

Ground water samples collected from the monitoring wells were submitted for laboratory analyses using
EPA Method 6200B. Free product was observed in recovery well MW-1R. There was not enough water in
monitoring wells MW-2, MW-6, or MW-10 to collect a sample. The concentrations of VOCs reported in
the ground water samples collected from MW-3, MW-4, MW-7, and TW-1 exceeded the MACs. All
reported contaminant concentrations were below the GCLs. A summary of the analytical results for
ground water samples collected on December 19, 2023, is included in Table 6. A Ground Water Quality
Map based on the December 2023 data is included as Figure 5. A complete report of laboratory analyses
of the ground water samples collected from the monitoring wells during the December 2023 sampling
event is included as Appendix E. A summary of the current BTEX, MTBE, and Naphthalene ground water
analytical data is shown below:

Contaminant
of Concern 
Be
n
z
e
n
e

To
l
u
e
n
e

Et
h
y
l
b
e
n
z
e
n
e

Xy
l
e
n
e
s

MT
B
E

Na
p
h
t
h
a
l
e
n
e

Well
ID
MACs (μg/l) 1 600 600 500 20 6
GCL (μg/l) 5,000 260,000 80,000 50,000 20,000 6,000
MW-1R FP FP FP FP FP FP
MW-2 NS NS NS NS NS NS
MW-3 17.6 2.38 0.279 J 4.21 0.233 J <0.470
MW-4 4,300 136.36 E 2,930 19,100 <14.0 806
MW-5 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
MW-6 NS NS NS NS NS NS
MW-7 7.97 0.572 1.69 6.88 0.664 J <0.470
MW-8 <1.80 <2.20 <1.70 <2.10 <1.40 <4.70

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 18, 2024 Kingsway #20
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5351
4
MW-9 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
MW-10 NS NS NS NS NS NS
TW-1 2.73 <0.220 0.435 J 0.214 J <0.140 <0.470

The site is located in the Kings Mountain Belt within the Piedmont Physiographic Province of North
Carolina. The underlying bedrock is comprised of metamorphosed quartz diorites. The soil mantle that
covers the underlying fractured bedrock in most places provides an intergranular medium through which
the recharge and discharge of water from the fractured rocks commonly occurs. The result is a composite
two-media system which characterizes ground water flow. The top of the system is the water table
surface, which is typically located in the soil or saprolite. The fractured bedrock generally grades
downward into unfractured rock below a depth of approximately 300 feet. Thus, the base of the ground
water system is indistinct. Locally the onsite ground water table has a seasonal high depth to water of
approximately eighteen feet BGS.

A CAP has not yet been developed for the site. Please note that attenuation milestones will be established
in the CAP.
3.0 FREE PRODUCT REMOVAL
Free product has historically been present in monitoring wells MW-1 and MW-4 and is currently present
in recovery well MW-1R. Hand bailing of free product from monitoring well MW-4 was conducted in
October 2020. An AFVR event was conducted on monitoring wells MW-1 and MW-2 in December 2020.
An MMPE was conducted on monitoring wells MW-1, MW-2, and MW-4 in October 2021. A total of
672.35 gallons of fluid have been removed during free product recovery activities. Of the 672.35 gallons,
approximately 114.35 gallons of free product have been removed from the site. The majority of this free
product was removed during the October 2021 MMPE event which resulted in the removal of 101.09
gallons of vaporized free product. A free product skimmer was installed in MW-1 on March 21, 2022. No
free product was recovered using the free product skimmer; therefore, it was permanently removed
during the December 2022 sampling event. Free product recovery should continue at the site until free
product is no longer present.
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
Free product recovery is currently being conducted at the site. Due to the site being in the active
remediation phase, no natural attenuation monitoring plan is currently in place at the site.
5.0 CONCLUSIONS
 On December 19, 2023, nine Type II monitoring wells, one recovery well, and one telescoping well
were gauged, purged, and/or sampled. Recovery well MW-1R contained free product and was not
sampled. There was not enough water in monitoring wells MW-2, MW-6, or MW-10 to collect a
sample. Ground water flow generally converged towards the center of the site from the east and
west, then diverged to the north and south. The horizontal gradient of approximately 0.04 feet
per foot. The vertical gradient could not be calculated.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 18, 2024 Kingsway #20
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5351
5
 The concentrations of VOCs reported in the ground water samples collected from MW-3, MW-4,
MW-7, and TW-1 exceeded the MACs. All reported contaminant concentrations were below the
GCLs.
 Based on this information, the risk classification for the site should remain intermediate risk. GRI
recommends removing free product from MW-1R by conducting an AFVR. A comprehensive
ground water sampling event should be conducted approximately 30 days after the AFVR. The
AFVR is tentatively scheduled for May 2024.
6.0 LIMITATIONS
This report has been prepared for the exclusive use of Kingsway Enterprises, Inc. for specific application
to the referenced site in Gaston County, North Carolina. The assessment was conducted based on the
scope of work and level of effort desired by the NCDEQ and with resources adequate only for that scope
of work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.
7.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. n/a Will this report be submitted after the
established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO
IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain
what was missing and why.
3 If applicable, will any of the proposed attenuation milestones under the schedule approved
in the Corrective Action Plan not be met? (within a reasonable margin of error)
YES NO
IF the answer to question #3 is “NO”, skip to the certification under #8 below.
IF the answer to question #3 is “YES”, please generally describe in this cell the possible reason(s) and
outline proposed remedies. (This should be described in more detail in the report text above.)

N/A
4 Does any known or suspected source zone soil contamination or free product remain
outside of the assessed area that could be inhibiting natural attenuation?
YES NO
5 Has there been an unexpected increase in contaminant mass sufficient to suggest a
potential new release from a separate onsite or offsite source?
YES NO

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 18, 2024 Kingsway #20
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5351
6
IF the answer to either question #4 or #5 is “YES”, generally describe in this cell any actions
recommended to further assess or clean up this known or suspected source. (This should be described
in more detail in the report text above.)

6 Certification:
I, Ashleigh Thrash, a Licensed Geologist for Geological Resources, Inc., do certify that the information
contained in this report is correct and accurate to the best of my knowledge.

Geological Resources, Inc. is licensed to practice engineering and geology in North Carolina. The
certification number of the company or corporation is C-2727/C-127.

FIGURES
SITE LOCATION
Figure 1
Site Location
Kingsway #20
2201 Kendrick Road Gastonia, Gaston
County, NC
Incident No. 47019
GRI Project No. 5351
500 M
2000 FT
Date: 07/16/2020 Location: 35.213919° N -81.133526 W
D
a
d
"J
"J
SITE
3563391879
3563297651
3563298901
3563293972
3563295618
3563287459
3563296931
3563391634
35632983083563295338
3563295534
3563296368
3563390537
3563390432
WSW-2
WSW-1
KENDRICK RDST REGIS DR
KINGS DR
KENNEDY RD
KENTWOOD DR
ERIKA LN
EAGLEBROOK DR
ST ANDREWS LN
WIMBLEDON DR
PATIO LN
SU SAN FARMS RD
STONEYCREEK CT
CLAY CT
MARIA LYNN CT
HOVIS CT
GASTON DAY SCHOOL RD
GLENEAGLES DR
EASTHAMPTON DR
PRINCETON DR
ROXBURGH LN
STABLEVIEW DR LOVE CT
KENDRICK ESTATES DR
EMERALD LN
JORDANVIEW LN
ANGELA CT EPPINETTE CT
LAVER CT
GASTON DAY SCHOOL RD GURE 3A: MAPKINGSWAY #202201 KENDRICK ROADGASTONIA, GASTON COUNTYNORTH CAROLINAINCIDENT NO. 40626GRI NO. 5351
PREPARED BY:GEOLOGICAL RESOURCES, INC.JUNE 9, 2020
³
0 300150Feet
1 inch = 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS
500-FOOT RADIUS
250-FOOT RADIUS
LEGEND
"J Water Supply Well
Streets
CreeksStreams
Ponds
Well Owners and Adjacent Properties
Gaston County NC Parcels
FI SITE VICINITY
SITE
KENDRICK RDST REGIS DR
KINGS DR
KENNEDY RD
KENTWOOD DR
ERIKA LN
EAGLEBROOK DR
ST ANDREWS LN
WIMBLEDON DR
PATIO LN
SU SAN FARMS RD
STONEYCREEK CT
CLAY CT
MARIA LYNN CT
HOVIS CT
GASTON DAY SCHOOL RD
GLENEAGLES DR
EASTHAMPTON DR
PRINCETON DR
ROXBURGH LN
STABLEVIEW DR LOVE CT
KENDRICK ESTATES DR
EMERALD LN
JORDANVIEW LN
ANGELA CT EPPINETTE CT
LAVER CT
GASTON DAY SCHOOL RD
FIGURE 3B: ZONING MAPKINGSWAY #202201 KENDRICK ROADGASTONIA, GASTON COUNTYNORTH CAROLINAINCIDENT NO. 40626GRI NO. 5351
PREPARED BY:GEOLOGICAL RESOURCES, INC.JUNE 9, 2020
³
0 300150Feet
1 inch = 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS
500-FOOT RADIUS
250-FOOT RADIUS
LEGEND
Zoning RS-8CD
Zoning RS-12
Streets
CreeksStreams
Ponds
Rivers
Gaston County NC Parcels

TABLES
UST ID Number 1,2,3 Facility ID Number
Owner or Operator?
Owner
UST ID Number 1,2,3 Facility ID Number
Owner or Operator?
Operator
UST ID Number 1,2,3 Facility ID Number
Owner or Operator?
Owner
UST ID Number 1,2,3 Facility ID Number
Owner or Operator?
Owner
Address Telephone Number
Unknown Unknown
00-0-0000016201
Name of Owner or Operator Dates of Ownership / Operation
Daniel L. Johnson 07/09/1986 - 03/21/2004
00-0-0000016201
TABLE 1
UST OWNER/OPERATOR INFORMATION
KINGSWAY #20 (INCIDENT NO. 47019)
100 Wynnchester Road, Gastonia, NC 28052-0003 Unknown
Name of Owner or Operator Dates of Ownership / Operation
Carolyn W. Johnson 03/21/2004 - 05/08/2018
Address Telephone Number
00-0-0000016201
Name of Owner or Operator Dates of Ownership / Operation
Kingsway Enterprises, Inc. 03/03/2016 - Present
Address Telephone Number
407 S. Marietta St., Gastonia, NC 28052-4331 704-864-0401
Address Telephone Number
407 S. Marietta St., Gastonia, NC 28052-4331 704-864-0401
00-0-0000016201
Name of Owner or Operator Dates of Ownership / Operation
Kingsway Properties, LLC 05/08/2018 - Present
Page 1 of 1
Date: 6/23/2020
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline 10,000 7/9/1986 Single Wall
Steel/FR 8' x 26' 7" Single Wall FRP Current Yes
2 Gasoline 10,000 7/9/1986 Single Wall
Steel/FR 8' x 26' 7" Single Wall FRP Current Yes
3 Gasoline 10,000 7/9/1986 Single Wall
Steel/FR 8' x 26' 7" Single Wall FRP Current Yes
TABLE 2
UST SYSTEM INFORMATION
KINGSWAY #20 (INCIDENT NO. 47019)
UST
ID
No.
Current
or Most
Recent
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
Facility ID #: 0-016201
Page 1 of 1
Date: 01/03/2023 Facility ID #: 0-016201
Well ID Parcel PIN Parcel ID Well Owner Mailing Address Well Location Address
Well Use
(Potable/
Agriculture, etc.)
Public Water
Connected
Distance from
source area of
release
(ft.)
WSW-1 3563-2939-71 149540 Rental Properties, LLC PO BOX 2185, Gastonia, NC 28053-
2105
2070 Kendrick Rd. Gastonia, NC
28056 Non-potable Yes 460 NW
WSW-2 3563-0824-54 149591 Adan W. Moreira-Ferrin and
Karla S. Garcia
2927 Gaston Day School Rd.
Gastonia, NC 28056-7523
2927 Gaston Day School Rd.
Gastonia, NC 28056 Non-potable Yes 1,230 S
Notes:
• Water supply wells are shown on Figure 3A
TABLE 3
WATER SUPPLY WELL INFORMATION
KINGSWAY #20 (INCIDENT NO. 47019)
Page 1 of 1
Date: 01/03/24 Facility ID #: 0-016201
PIN Number Parcel ID No. Property Owner Name Property Owner Address
3563-2976-51 (site) 149544 Kingsway Properties LLC 1910 Kendrick Rd., Gastonia, NC
28052-4331
3563-2983-08 149723 Anna K. Beesley 3908 Saint Regis Dr., Gastonia, NC
28056
3563-2963-68 149722 James F. Jacobs 3904 Saint Regis Dr., Gastonia, NC
28056-8824
3563-2953-38 224057 Thomas W. & Lisa K. Garrett 3900 St Regis Dr., Gastonia, NC
28056
3563-2953-27 223732 Ronald J. & Renee A. Reeger 3604 Eaglebrook Dr., Gastonia, NC
28056
3563-2956-18 149719 D. Patrick & Ann D. Toomey 3600 Eaglebrook Dr., Gastonia, NC
28054-0000
3563-2969-31 149542 James R. II. & Karin A. Norman 502 Ingonish Dr., Gastonia, NC
28056-0000
3563-2989-01 302456 Thomas O. & Kristine A. McFadden 2126 Kendrick Rd., Gastonia, NC
28056
3563-3918-79 149662 Richard L. Massey Life Est.2300 Kendrick Rd., Gastonia, NC
28056
3563-3905-37 149587 Karen Jaeger 3609 Stoneycreek Ct., Gastonia, NC
28056-0000
3563-3916-42 149586 Matthew G. & Michelle L. Gibbons 3601 Stoneycreek Ct., Gastonia, NC
28056-0000
3563-3904-32 149588 Ronald A. & Coleen D. Grenier 3617 Stoneycreek Ct., Gastonia, NC
28056-0000
Note:
• Properties are keyed to Figure 3.
TABLE 4
ADJACENT PROPERTY OWNER INFORMATION
KINGSWAY #20 (INCIDENT NO. 47019)
Page 1 of 1
Date: 01/03/24
Well ID
Date
Installed
(m/dd/yy)
Date Water
Level
Measured
(m/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free Product
Thickness
(ft.)
Ground
Water
Elevation (ft.)
Comments
06/10/20 23.68 0.18 76.47
10/01/20 25.70 0.78 74.97
10/05/20 25.16 0.06 74.89
12/30/20 25.28 0.08 74.79
12/30/20 25.36 ---74.64
03/10/21 23.95 0.17 76.20
10/04/21 26.54 0.28 73.70
10/08/21 26.24 0.22 73.95
12/02/21 27.63 0.12 72.47
05/05/22 27.71 0.01 72.30
06/01/22 27.77 ---72.23 FP during bailing
12/22/22 NM ---NM Dry
06/06/23 25.78 ---NM
12/19/23 28.95 1.50 NM
10/05/20 24.40 ---74.93
12/30/20 24.45 ---74.88
12/30/20 24.72 ---74.61
03/10/21 22.95 ---76.38
10/04/21 25.61 ---73.72
10/08/21 25.88 ---73.45
12/02/21 26.51 ---72.82
05/05/22 26.08 ---73.25
06/01/22 26.05 ---73.28
12/22/22 26.48 ---72.85
06/06/23 25.20 ---74.13
12/19/23 26.53 ---72.80
10/05/20 NM ---NM Well was dry
03/10/21 23.29 ---76.61
12/02/21 26.67 ---73.23
05/05/22 26.41 ---73.49
06/01/22 26.78 ---73.12
12/22/22 27.06 ---72.84
06/06/23 25.85 ---74.05
12/19/23 27.82 ---72.08
10/05/20 26.25 0.56 74.62
12/30/20 26.71 0.82 74.38
12/30/20 26.98 ---73.41
03/10/21 24.49 ---75.90
10/04/21 NM ---NM
10/08/21 27.17 ---73.22
12/02/21 27.49 ---72.90
05/05/22 27.56 ---72.83
06/01/22 27.74 ---72.65
12/22/22 27.77 ---72.62
06/06/23 NM ---NM Dry
12/19/23 27.53 ---72.86
03/10/21 18.59 ---80.26
12/02/21 21.91 ---76.94
05/05/22 21.03 ---77.82
06/01/22 21.06 ---77.79
12/22/22 21.12 ---77.73
06/06/23 20.66 ---78.19
12/19/23 21.51 ---77.34
13 13 - 28
100.39
16 16 - 31 31 98.85
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
KINGSWAY #20 (INCIDENT NO. 47019)
Facility ID # : 0-016201
28
13 13 - 28 28
99.33
20 20 - 35 35 99.90
100.00288 - 28806/10/20MW-1
10/01/20
MW-3 10/02/20
MW-4 10/01/20
MW-5 03/08/21
Abandoned 3/24/23
MW-1R 3/23/2023 15 15 - 35 35 NM
MW-2
Page 1 of 2
Date: 01/03/24
Well ID
Date
Installed
(m/dd/yy)
Date Water
Level
Measured
(m/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free Product
Thickness
(ft.)
Ground
Water
Elevation (ft.)
Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
KINGSWAY #20 (INCIDENT NO. 47019)
Facility ID # : 0-016201
03/10/21 25.80 ---75.73
12/02/21 29.20 ---72.33
05/05/22 29.17 ---72.36
06/01/22 29.10 ---72.43
12/22/22 29.48 ---72.05
06/06/23 28.30 ---73.23
12/19/23 29.55 ---71.98
03/10/21 24.63 ---75.34
12/02/21 NM ---NM Dry
05/05/22 26.04 ---73.93
06/01/22 25.92 ---74.05
12/22/22 NM ---NM Dry
06/06/23 NM ---NM Dry
12/19/23 25.94 ---74.03
03/10/21 22.85 ---76.20
12/02/21 26.92 ---72.13
05/05/22 26.07 ---72.98
06/01/22 26.12 ---72.93
12/22/22 27.99 ---71.06
06/06/23 25.21 ---73.84
12/19/23 28.35 ---70.70
03/10/21 21.98 ---77.25
12/02/21 26.96 ---72.27
05/05/22 25.48 ---73.75
06/01/22 25.69 ---73.54
12/22/22 27.29 ---71.94
06/06/23 24.56 ---74.67
12/19/23 28.19 ---71.04
03/10/21 24.11 ---76.38
12/02/21 28.29 ---72.20
05/05/22 27.50 ---72.99
06/01/22 27.53 ---72.96
12/22/22 NM ---NM Dry
06/06/23 26.59 ---73.90
12/19/23 29.13 ---71.36
10/05/20 26.35 ---73.61
03/10/21 23.73 ---76.23
12/02/21 26.92 ---73.04
05/05/22 26.94 ---73.02
06/01/22 26.97 ---72.99
12/22/22 29.09 ---70.87
06/06/23 26.05 ---73.91
12/19/23 29.30 ---70.66
Notes:
99.96
99.23
15 15 - 30 30 100.49
45 45 - 50 50
15 15 - 30 30
99.97
15 15 - 30 30 99.05
11 11 - 26 26
15 15 - 30 30
TW-1 10/02/20
MW-9 03/09/21
101.53
• Elevation relative to mean sea level.
MW-10 03/09/21
• ft BGS : feet below ground surface.
• NM : Not measured.
MW-8
MW-6 03/08/21
MW-7 03/08/21
03/08/21
Page 2 of 2
Date: 01/03/24 Facility ID # : 0-016201
EPA 6010
Well
ID
Date Sampled
(mm/dd/yy)
1 600 600 500 20 6 40 10 70 3 40 70 25 5 70 0.6 400 400 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 10,000 5,900 3,000 40,000 30,500 11,700 5,000 26,100 600 28,500 24,100 15,000 NE NE NE06/10/20 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP10/05/20 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP03/10/21 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP12/02/21 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP06/01/22 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP12/22/22 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/06/23 1,980 11,400 2,620 16,500 <14.0 726 <190 <160 37.7 J 24.1 J <38.0 156 <8.90 <33.0 398 <9.60 4,030 1,040 NR NR NR NR
12/19/23 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
10/05/20 5,930 56,000 4,750 27,700 <250 412 J <4,000 <4,000 <250 <400 NR <250 <250 <2000 382 J <250 2,820 864 J 25.6 30,800 4,150 J 13,200
10/04/21 4,650 48,000 4,300 27,500 <130 1,050 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
12/02/21 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/01/22 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/22/22 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/06/23 2,460 38,000 5,050 32,100 <14.0 831 253 J <160 46.8 J <22.0 127 172 <8.90 <33.0 447 <9.60 5,470 1,400 NR NR NR NR
12/19/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/05/20 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/10/21 375 54.4 11.8 87.5 <1.3 <1.3 120 <20 <1.3 <2.0 NR 2.1 J <1.3 <10 <1.3 <1.3 <1.3 <1.3 <5.0 878 <35 91.9 J
12/02/21 333 8.4 7.0 9.3 J <1.3 2.2 J 120 <20 <1.3 <2.0 NR 1.5 J <1.3 <10 <1.3 <1.3 <1.3 <1.3 NR NR NR NR
06/01/22 20.3 0.62 J <0.25 <0.50 <0.25 <0.25 11.0 J <4.0 <0.25 <0.40 NR <0.25 <0.25 4.6 B <0.25 <0.25 <0.25 <0.25 NR NR NR NR
12/22/22 127 5.00 2.48 14.9 <0.140 <0.470 18.0 4.07 J 0.623 <0.220 <0.380 2.80 <0.089 <0.330 0.757 <0.096 1.32 0.421 J NR NR NR NR
06/06/23 2.23 <0.220 0.206 J <0.210 <0.140 <0.470 12.3 3.18 J <0.180 0.355 J <0.380 0.428 J <0.089 <0.330 <0.190 <0.096 <0.190 <0.180 NR NR NR NR
12/19/23 17.6 2.38 0.279 J 4.21 0.233 J <0.470 95.4 13.4 <0.180 <0.220 <0.380 0.218 J 0.377 J <0.330 <0.190 <0.096 0.598 0.478 J NR NR NR NR
10/05/20 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP12/02/21 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS06/01/22 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/22/22 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/06/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/19/23 4,300 136.36 E 2,930 19,100 <14.0 806 596 J <160 74.7 <22.0 102 212 31.8 J <33.0 500 <9.60 5,710 1,490 NR NR NR NR
03/10/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 <0.13 <0.20 NR <0.13 <0.13 <1.0 <0.13 <0.13 <0.13 <0.13 <5.0 <35 <35 <35 12/02/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 <0.13 <0.20 NR <0.13 <0.13 <1.0 <0.13 <0.13 <0.13 <0.13 NR NR NR NR06/01/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 <0.13 <0.20 NR <0.13 <0.13 2.0 B <0.13 <0.13 <0.13 <0.13 NR NR NR NR
12/22/22 <0.180 0.384 J <0.170 0.225 J <0.140 <0.470 <1.90 <1.60 <0.180 <0.220 <0.380 <0.180 <0.089 <0.330 <0.190 <0.096 0.234 J <0.180 NR NR NR NR
06/06/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <1.60 <0.180 <0.220 <0.380 <0.180 <0.089 <0.330 <0.190 <0.096 <0.190 <0.180 NR NR NR NR
12/19/23 <0.180 <0.220 <0.170 <0.21 <0.140 <0.470 <1.90 <1.60 <0.180 <0.220 <0.380 <0.180 <0.089 <0.330 <0.190 <0.096 <0.190 <0.180 NR NR NR NR
03/10/21 347 20.6 5.4 13.0 J <1.3 2.6 J 173 <20 <1.3 <2.0 NR 2.8 J <1.3 <10 <1.3 <1.3 1.6 J <1.3 <5.0 266 <35 54.4 J
12/02/21 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/01/22 13.5 <0.13 0.29 J <0.25 <0.13 <0.13 <2.0 3.5 J <0.13 <0.20 NR 1.2 <0.13 2.5 B <0.13 <0.13 <0.13 <0.13 NR NR NR NR
12/22/22 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/06/23 122 6.08 5.26 17.0 J <1.40 17.5 78.6 J 44.9 J <1.80 <2.20 <3.80 15.2 <0.890 <3.30 <1.90 <0.960 10.4 3.04 J NR NR NR NR
12/19/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/10/21 403 150 24.7 142 <1.3 16.7 222 <20 <1.3 <2.0 NR 9.4 <1.3 <10 2.2 J <1.3 19.1 5.2 25.7 372 <35 203
12/02/21 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/01/22 <0.25 <0.25 <0.25 <0.50 <0.25 <0.25 <4.0 <4.0 <0.25 <0.40 NR <0.25 <0.25 5.5 B <0.25 <0.25 <0.25 <0.25 NR NR NR NR
12/22/22 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/06/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/19/23 7.97 0.572 1.69 6.88 0.664 J <0.470 118 173 1.64 <0.220 1.28 7.22 1.72 <0.330 1.61 2.22 1.77 2.40 NR NR NR NR
03/10/21 2.0 <0.13 <0.13 0.27 J 2.6 <0.13 32.0 45.4 <0.13 <0.20 NR 0.51 <0.13 <1.0 <0.13 <0.13 0.43 J <0.13 <5.0 138 <35 55.5 J12/02/21 0.51 3.9 0.94 7.7 2.6 0.69 45.8 61.1 <0.13 <0.20 NR 0.20 J <0.13 <1.0 0.23 J <0.13 3.1 1.3 NR NR NR NR06/01/22 2.0 0.76 0.15 J 1.1 J 4.4 <0.13 3.2 J <2.0 <0.13 1.5 NR <0.13 <0.13 2.2 B <0.13 <0.13 0.23 J 0.13 J NR NR NR NR
12/22/22 9.29 157 29.8 224 2.89 5.22 <1.90 5.90 J 0.556 <0.220 <0.380 1.74 <0.089 <0.330 3.91 <0.096 47.7 15.5 NR NR NR NR
06/06/23 0.994 0.796 0.527 3.08 4.82 1.28 <1.90 <1.60 <0.180 <0.220 <0.380 <0.180 <0.089 <0.330 0.252 J <0.096 2.00 0.603 NR NR NR NR
12/19/23 <1.80 <2.20 <1.70 <2.10 <1.40 <4.70 <19.0 <16.0 <1.80 <2.20 <3.80 <1.80 <0.890 <3.30 <1.90 <0.960 <1.90 <1.80 NR NR NR NR
03/10/21 21.2 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 <0.13 <0.20 NR 0.59 <0.13 <1.0 <0.13 <0.13 <0.13 <0.13 <5.0 <35 <35 <35 12/02/21 3.9 <0.13 <0.13 <0.25 <0.13 <0.13 2.1 J <2.0 <0.13 <0.20 NR 0.36 J <0.13 <1.0 <0.13 <0.13 <0.13 <0.13 NR NR NR NR06/01/22 0.23 J <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 <0.13 <0.20 NR <0.13 <0.13 2.2 B <0.13 <0.13 <0.13 <0.13 NR NR NR NR
12/22/22 0.273 J 0.607 <0.170 1.24 J <0.140 <0.470 <1.90 <1.60 <0.180 <0.220 <0.380 <0.180 <0.089 <0.330 <0.190 <0.096 0.426 J <0.180 NR NR NR NR
06/06/23 <0.180 3.61 1.68 12.3 <0.140 1.06 <1.90 <1.60 <0.180 <0.220 <0.380 <0.180 <0.089 <0.330 0.301 J <0.096 3.84 1.08 NR NR NR NR
12/19/23 <0.180 <0.220 <0.170 <0.21 <0.140 <0.470 <1.90 <1.60 <0.180 <0.220 <0.380 <0.180 <0.089 <0.330 <0.190 <0.096 <0.190 <0.180 NR NR NR NR
03/10/21 64.5 18.2 5.1 18.6 <0.25 <0.25 36.5 <4.0 <0.25 <0.40 NR 1.9 <0.25 <2.0 1.8 <0.25 0.97 J 0.76 J <5.0 154 <35 105
12/02/21 24.9 1.3 0.30 J 11.7 <0.13 0.92 233 28.0 <0.13 <0.20 NR 1.0 <0.13 <1.0 <0.13 <0.13 0.97 1.2 NR NR NR NR
06/01/22 18.0 3.7 2.5 24.8 <0.25 <0.25 <4.0 15.6 J <0.25 1.0 NR 2.1 <0.25 4.6 B 1.6 <0.25 2.0 1.2 NR NR NR NR
12/22/22 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/06/23 <0.180 <0.220 <0.170 0.224 J <0.140 <0.470 18.5 69.8 <0.180 <0.220 <0.380 <0.180 <0.089 <0.330 <0.190 <0.096 0.376 J <0.180 NR NR NR NR
12/19/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/05/20 209 356 59.8 238 <1.3 23.7 43.4 J <20 <1.3 <2.0 NR 3.7 J <1.3 <10 4.2 J <1.3 22.9 4.2 J <10 320 <35 139
03/10/21 205 340 4.7 J 360 <1.3 2.8 J 55.6 J <20 <1.3 <2.0 NR <1.3 <1.3 <10 <1.3 <1.3 14.4 6.1 <5.0 361 <35 238
12/02/21 58.3 73.8 2.7 93.5 0.35 J 1.3 36.3 <4.0 <0.25 <0.40 NR 0.46 J <0.25 <2.0 <0.25 <0.25 7.6 3.2 NR NR NR NR
06/01/22 0.31 J 2.1 1.2 7.0 <0.13 0.94 <2.0 <2.0 0.20 J <0.20 NR 0.17 J <0.13 2.0 B 0.60 <0.13 5.0 1.4 NR NR NR NR
12/22/22 0.415 J 3.02 1.59 9.69 <0.140 2.65 <1.90 2.82 J 0.298 J <0.220 <0.380 0.271 J <0.089 <0.330 1.03 <0.096 9.40 2.64 NR NR NR NR
06/06/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <1.60 <0.180 <0.220 <0.380 <0.180 <0.089 <0.330 <0.190 <0.096 <0.190 <0.180 NR NR NR NR
12/19/23 2.73 <0.220 0.435 J 0.214 J <0.140 <0.470 6.92 J <1.60 <0.180 <0.220 8.76 0.563 <0.089 <0.330 <0.190 <0.096 <0.190 <0.180 NR NR NR NR
03/10/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 <0.13 <0.20 NR 0.59 <0.13 <1.0 <0.13 <0.13 <0.13 <0.13 NR NR NR NR10/04/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
12/02/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 <0.13 <0.20 NR <0.13 <0.13 <1.0 <0.13 <0.13 <0.13 <0.13 NR NR NR NR06/01/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR <0.13 <0.20 NR <0.13 <0.13 2.0 B <0.13 <0.13 <0.13 <0.13 NR NR NR NR
12/22/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 NR NR <0.180 <0.220 <0.380 <0.180 <0.089 <0.330 <0.190 <0.096 <0.190 <0.180 NR NR NR NR
06/06/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <1.60 <0.180 <0.220 <0.380 <0.180 <0.089 <0.330 <0.190 <0.096 <0.190 <0.180 NR NR NR NR
12/19/23 <0.180 <0.220 <0.170 <0.21 <0.140 <0.470 NR NR <0.180 <0.220 <0.380 <0.180 <0.089 <0.330 <0.190 <0.096 <0.190 <0.180 NR NR NR NR
Notes:
• Results reported in micrograms per liter (µg/l).• MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202.• GCL: Gross contamination level.
• Concentrations in bold face type indicate the MAC was below the reported concentration.
• J: Estimated value.• NE: Not established.
• NR: Not Requested.
• FP: Free product.
• *: concentrations prior to initial detection have not been updated
TW-1
Trip Blank
MW-6
MW-7
MW-8
MW-9
MW-10
MW-1
MW-1R
MW-2
MW-3
MW-4
MW-5
C9
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TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
KINGSWAY #20 (INCIDENT NO. 47019)
Analytical Method
→MADEP VPH
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Page 1 of 1

APPENDICES

APPENDIX A
State Correspondence

July 13, 2023 Carolyn Johnson 2603 White Pines Court Monroe, North Carolina 28112

Re: Notice of Regulatory Requirements 15A NCAC 2L .0404 Risk-based Assessment and Corrective Action for Petroleum Underground Storage Tanks Kingsway 20 2201 Kendrick Road, Gastonia Gaston County
Incident Number: 47019 Risk Classification: Intermediate Ranking: I245A
Dear Ms. Johnson:
The Groundwater Monitoring Report received by the UST Section, Division of Waste Management, Mooresville Regional Office on June 28, 2023, has been reviewed. This report will remain in the UST Section’s files. The next groundwater monitoring event should be conducted in December 2023, with the report received no later than January 31,
2024. If you have any questions regarding the actions that must be taken or the rules mentioned in this letter, please contact me at the address or telephone number listed below. Sincerely,
Brad C. Newton, P.G.
Hydrogeologist Mooresville Regional Office UST Section, Division of Waste Management, NCDEQ
cc: Joanna Alley – Geologic Resources, Inc. (via e-mail) Gaston County Health Department
Site Name City / County /Gaston Incident #47019
Resp Pty Name / Contact Incident Mgr Region MORRP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #8
Consultant / Project Mgr /Joanna R Alley
Telephone / Fax Number /Task Authorization Number:9 ChangeOrd:
Project Mgr Email Site Risk / Rank / Abatement:I245A RRA Date:
Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
 Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.
Task #Lab /
SubCode
RO

I
M

A
u
t
h
Proposed
Rate/Price
(Consultant)RO

S
u
p
v
.

Au
t
h
Proposed Task
Subtotal
(Consultant)
Final
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
2.074 1 /well Y $90.00 y $90.00 $90.00 /
2.281 1 /sock Y $30.00 y $30.00 $30.00 /
2.290 1 /sock Y $15.00 y $15.00 $15.00 /
4.031 11 /wells Y $110.00 y $1,210.00 $1,210.00 /
4.090 #240 11 /samples Y $94.00 y $1,034.00 $1,034.00 /
4.090 #272 1 /sample Y $66.00 y $66.00 $66.00 /
4.091 1 /shipment Y $60.00 y $60.00 $60.00 /
6.090 1 /report Y $1,125.00 y $1,125.00 $1,125.00 /
12.050 1 /trip Y $250.00 y $250.00 $250.00 /
12.055 1 /trip Y $50.00 y $50.00 $50.00 /
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
Requested Preapproved
TOTAL:$3,930.00 $3,930.00 TOTAL:
Total Standard Costs (Not Third Party)$3,930.00 $3,930.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty CostsProcess Tracking (Date)
TA Submittal:8/15/23 by:(PM)(Reserved for RO)
RO Review:8/16/23 by:(IM)Joint UST Preapproval Confirmed By:
RO Supv. Review:8/16/23 by:(STF)RP or Designee Receipt Confirmation By:
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable.
3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned.
4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee within a week of approval. The signed pre-approval must be submitted
in the submitted claim. Signature indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to workproceeding. Scope/cost negotiations do not supersede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both theUST Section and RP is not to be modified without written consent by all signatories.
5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full.
DWM/UST ePATA 4/1/2022
Proposed
Units / Type
(Consultant)
Brad Newton
YES23-450 December 2023
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
[e-mail]
Kingsway Enterprises Mark King
Geological Resources, Inc.
Gastonia
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
704-845-4010 (Reserved for Incident Manager)
Kingsway 20
Note:This Electronic Preapproval Task Authorization (ePATA)shall be used to receive preapproval from the UST Section.A proposal,including maps and figures,must be
attached to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If,following completion of this ePATA,
you discover that unexpected tasks must be performed, incurring costs for tasks not originally included with this form,you must complete and submit a separate ePATA requestdesignated as a "Change Order" in the provided space above prior to conducting those tasks.Include a copy of the prior ePATA form for confirmation.Please attach this form to
the cover of the corresponding claim when requesting reimbursement.IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been
completed within 12 months ofthe completion date of the FIRST completed task to remain within the Statute ofLimitations.All ePATAs submitted withina claim areclosed with that
claim,and may not be re-used in a separate submittal,even for costs or tasks that were not originally claimed.Final reimbursement of costs associated with the Total Claimedamount below may be affected by the eligibility status of the site (i.e.,deductibles,apportionment,etc.),and the documentary validation of incurred costs as reasonable and
BCN
RHT
(Initials)
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORMDept of Environmental Quality -Division of Waste Management
08/16/23

APPENDIX B
Land Use Information
Date: 04/08/21 Facility ID # : 0-016201
Map ID No.Land Use Feature Zoning Despription Address
Distance from
Source Area
(feet)
n/a RS-12 Residential 12,000 sq. ft.
lots n/a n/a
n/a RS-8CD Residential 8 Units Per
Acre Conditional District n/a n/a
Note:
• Properties are keyed to Figure 3B.
APPENDIX B
LAND USE INFORMATION
KINGSWAY #20 (INCIDENT NO. 47019)
Page 1 of 1

APPENDIX C
Incident Report
NCDEQ Incident Report
RP/Company
RPAddress 2603 WHITE PINES COURT
RPCity MONROE
Contact CAROLYN JOHNSON
RPState NC
TELEPHONE
IncidentNumber 47019 USTNum MO-27698
IncidentName KINGSWAY 20
FacilID 00-0-0000016201
Address 2201 KENDRICK ROAD
CityTown GASTONIA State
ZipCode
DateOccurred 3 /28/2020
DateReported 4 /28/2020
ConfRisk I
CloseOut
COMMENT
RptType Rcvd Rvwd Appvd
Incident Mgr BCNLongitude-81.133392 Latitude 35.213889
County GASTO
IAR 4/17/2020 5/7/2020 5/7/2020
LSA1 7/24/2020 8/5/2020 8/5/2020
FPRS 12/3/2020 12/10/2020 12/10/2020
free product evaluation
FPRS 2/25/2021 3/15/2021 3/15/2021
CSAS 5/10/2021 5/24/2021 5/24/2021
Thursday, January 4, 2024 Page 1 of 2
MRP 1/11/2022 1/27/2022 1/27/2022
MRP 7/1/2022 7/11/2022 7/11/2022
MRP 1/17/2023 1/31/2023 1/31/2023
MRP 6/28/2023 7/13/2023 7/13/2023
Thursday, January 4, 2024 Page 2 of 2

APPENDIX D
Historical Soil Quality Information
Date: 04/08/21
5030/
8015D
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50 NE NE NE NE NA NA NE NE NE
NE 0.0056 4.3 4.9 4.6 0.091 0.16 68 540 31
NE 18 1,200 1,560 3,129 350 313 939 1,500 469
SB-1-R-3'03/18/20 3 18,100 99.8 1,370 398 2,090 NR NR NR NR NR
SB-2-+-3'03/18/20 3 <4.6 0.0081 0.0183 J 0.0029 J 0.0459 NR NR NR NR NR
SB-3-P-3'03/18/20 3 8.27 0.0281 0.0707 0.0114J 8.27 J NR NR NR NR NR
MW-1 (5')06/10/20 5 NR <0.0016 <0.013 <0.0013 <0.0028 <0.0013 <0.0026 <2.5 <2.5 <2.5
MW-1 (10')06/10/20 10 NR <0.0014 <0.011 <0.0011 <0.0024 <0.0011 <0.0022 <2.2 <2.2 <2.2
MW-1 (15')06/10/20 15 NR <0.0012 <0.0098 <0.00098 <0.0021 <0.00098 <0.0020 <2.3 <2.3 <2.3
SB-6-13'10/01/20 13 NR <0.11 <0.89 <0.089 0.365 J <0.089 4.58 10.3 58.0 67.0
Notes:
• Results reported in mg/kg (milligrams per kilograms)
• ft-BGS: feet below ground surface.
• RAL: Regulatory Action Level.
• MCCs: Maximum Contaminant Concentrations (soils).
• SCLs: Soil Cleanup Levels.
• < : Less than the method detection limit specified in the laboratory report
• NE: Not Established
• NR: Not Requested.
• Concentrations in bold face type indicate the reported concentrations were above the the soil-to-water MCCs
• Concentrations in italic type indicate the reported concentrations were above the residential SCLs.
MADEP VPH
KINGSWAY #20 (INCIDENT NO. 47019)
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS
Soil to Water MCC (mg/kg)
Residential SCLs (mg/kg)
EPA Method 8260B
APPENDIX E
Facility ID #: 00-0-016201
RAL (mg/kg)
Analytical Method 
Page 1 of 1

APPENDIX E
Laboratory Analytical Report

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

1/5/2024
Geological Resources, Inc. Joanna Alley
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-354-0023 Client Project Description: Kingsway #20
GRI #5351
Dear Joanna Alley:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 12/20/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 59
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2024402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Page 1 of 1 00016/23-354-0023
Page 2 of 59
Report Number:
Sample Summary Table
Client Project Description:
23-354-0023
Kingsway #20
GRI #5351
Lab No Client Sample ID Matrix Date Collected Date Received
12/19/2023 11:41Aqueous 92466 MW-3 12/20/2023 16:33
12/19/2023 11:08Aqueous 92467 MW-4 12/20/2023 16:33
12/19/2023 10:05Aqueous 92468 MW-5 12/20/2023 16:33
12/19/2023 10:51Aqueous 92469 MW-7 12/20/2023 16:33
12/19/2023 10:33Aqueous 92470 MW-8 12/20/2023 16:33
12/19/2023 10:15Aqueous 92471 MW-9 12/20/2023 16:33
12/19/2023 12:13Aqueous 92472 TW-1 12/20/2023 16:33
12/19/2023 07:58Aqueous 92473 Trip Blanks 12/20/2023 16:33
Page 3 of 59
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-354-0023
Report Limit
Project:Kingsway #20
V 92466MW-3
17.6 12/29/2023 03:076200BBenzeneµg/L 0.180
0.562 12/29/2023 03:076200BDi-Isopropyl Ether (DIPE)µg/L 0.500
J0.279 12/29/2023 03:076200BEthylbenzeneµg/L 0.170
J0.218 12/29/2023 03:076200BIsopropylbenzeneµg/L 0.180
J0.377 12/29/2023 03:076200B4-Isopropyl toluene µg/L 0.089
J0.233 12/29/2023 03:076200BMethyl tert-butyl ether (MTBE)µg/L 0.140
13.4 12/29/2023 03:076200Btert-Butyl Alcohol (TBA)µg/L 1.60
95.4 12/29/2023 03:076200Btert-Amyl Alcohol (TAA)µg/L 1.90
2.38 12/29/2023 03:076200BTolueneµg/L 0.220
0.598 12/29/2023 03:076200B1,2,4-Trimethylbenzene µg/L 0.190
J0.478 12/29/2023 03:076200B1,3,5-Trimethylbenzene µg/L 0.180
0.820 12/29/2023 03:076200Bo-Xylene µg/L 0.210
3.39 12/29/2023 03:076200Bm,p-Xylene µg/L 0.420
4.21 12/29/2023 03:076200BXylene (Total)µg/L 0.210
V 92467MW-4
J89812/29/2023 10:076200BAcetoneµg/L 180
4300 12/29/2023 10:076200BBenzeneµg/L 18.0
74.7 12/29/2023 10:076200Bn-Butylbenzene µg/L 18.0
J43.6 12/29/2023 10:076200Bsec-Butyl benzene µg/L 20.0
2930 12/29/2023 10:076200BEthylbenzeneµg/L 17.0
102 12/29/2023 10:076200B2-Hexanone µg/L 38.0
212 12/29/2023 10:076200BIsopropylbenzeneµg/L 18.0
J31.8 12/29/2023 10:076200B4-Isopropyl toluene µg/L 8.90
J40112/29/2023 10:076200BMethyl Ethyl Ketone (MEK)µg/L 71.0
806 12/29/2023 10:076200BNaphthaleneµg/L 47.0
500 12/29/2023 10:076200Bn-Propylbenzene µg/L 19.0
J28.0 12/29/2023 10:076200BStyreneµg/L 22.0
J59612/29/2023 10:076200Btert-Amyl Alcohol (TAA)µg/L 190
E136.36 12/29/2023 10:076200BTolueneµg/L 22.0
5710 12/29/2023 10:076200B1,2,4-Trimethylbenzene µg/L 19.0
1490 12/29/2023 10:076200B1,3,5-Trimethylbenzene µg/L 18.0
6410 12/29/2023 10:076200Bo-Xylene µg/L 21.0
12700 12/29/2023 10:076200Bm,p-Xylene µg/L 42.0
19100 12/29/2023 10:076200BXylene (Total)µg/L 21.0
V 92469MW-7
40.7 12/28/2023 02:326200BAcetoneµg/L 1.80
Page 4 of 59
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-354-0023
Report Limit
Project:Kingsway #20
V 92469MW-7
7.97 12/28/2023 02:326200BBenzeneµg/L 0.180
1.64 12/28/2023 02:326200Bn-Butylbenzene µg/L 0.180
1.86 12/28/2023 02:326200Bsec-Butyl benzene µg/L 0.200
0.653 12/28/2023 02:326200BDi-Isopropyl Ether (DIPE)µg/L 0.500
1.69 12/28/2023 02:326200BEthylbenzeneµg/L 0.170
1.28 12/28/2023 02:326200B2-Hexanone µg/L 0.380
7.22 12/28/2023 02:326200BIsopropylbenzeneµg/L 0.180
1.72 12/28/2023 02:326200B4-Isopropyl toluene µg/L 0.089
J0.664 12/28/2023 02:326200BMethyl tert-butyl ether (MTBE)µg/L 0.140
2.46 12/28/2023 02:326200B4-Methyl-2-Pentanone µg/L 0.078
1.61 12/28/2023 02:326200Bn-Propylbenzene µg/L 0.190
173 12/28/2023 02:326200Btert-Butyl Alcohol (TBA)µg/L 1.60
118 12/29/2023 09:426200Btert-Amyl Alcohol (TAA)µg/L 19.0
0.572 12/28/2023 02:326200BTolueneµg/L 0.220
2.22 12/28/2023 02:326200B1,1,2-Trichloroethane µg/L 0.096
1.77 12/28/2023 02:326200B1,2,4-Trimethylbenzene µg/L 0.190
2.40 12/28/2023 02:326200B1,3,5-Trimethylbenzene µg/L 0.180
2.47 12/28/2023 02:326200Bo-Xylene µg/L 0.210
4.41 12/28/2023 02:326200Bm,p-Xylene µg/L 0.420
6.88 12/28/2023 02:326200BXylene (Total)µg/L 0.210
V 92472TW-1
2.73 12/28/2023 03:216200BBenzeneµg/L 0.180
J0.435 12/28/2023 03:216200BEthylbenzeneµg/L 0.170
8.76 12/28/2023 03:216200B2-Hexanone µg/L 0.380
0.563 12/28/2023 03:216200BIsopropylbenzeneµg/L 0.180
J6.92 12/28/2023 03:216200Btert-Amyl Alcohol (TAA)µg/L 1.90
J0.214 12/28/2023 03:216200Bo-Xylene µg/L 0.210
J0.214 12/28/2023 03:216200BXylene (Total)µg/L 0.210
Page 5 of 59

Client: Geological Resources, Inc. CASE NARRATIVE
Project: Kingsway #20 Lab Report Number: 23-354-0023
Date: 1/5/2024
Volatile Organic Compounds - GC/MS Method 6200B Sample 92470 (MW-8) QC Batch No: V41777/V41775
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Sample received has only one vial. Only about half a volume of the vial is liquid.
Analyte: 2-Butanone
QC Batch No: V41839/V41838 CCV recovers low for this compound. All other QC passes within method parameters. All hits below MQL. No
further action taken.
Analyte: 3,3-Dimethyl-1-butanol QC Batch No: V41777/V41838
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Acetone QC Batch No: V41839/V41838
CCV recovers low for this compound. All other QC passes within method parameters. All hits below MQL. No further action taken.
Analyte: Vinyl acetate QC Batch No: V41839/V41838 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias.
LCS/LCSD fails low. A standard at or below the MQL was run and saw recovery.

Page 6 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-3
92466 Matrix:
12/19/2023 11:41
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 12/29/23 03:07 6200BMSA
Surrogate: 4-Bromofluorobenzene 99.0 Limits: 70-130%12/29/23 03:071 MSA V41839
Surrogate: Dibromofluoromethane 95.8 Limits: 70-130%12/29/23 03:071 MSA V41839
Surrogate: 1,2-Dichloroethane - d4 91.6 Limits: 70-130%12/29/23 03:071 MSA V41839
Surrogate: Toluene-d8 102 Limits: 70-130%12/29/23 03:071 MSA V41839
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 7 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-3
92466 Matrix:
12/19/2023 11:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41838 12/28/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 12/29/23 03:07 V41839MSA
17.6 µg/L 0.180 0.500Benzene 1 12/29/23 03:07 V41839MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 12/29/23 03:07 V41839MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 12/29/23 03:07 V41839MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 12/29/23 03:07 V41839MSA
<1.50 µg/L 1.50 5.00Bromoform 1 12/29/23 03:07 V41839MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 12/29/23 03:07 V41839MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 12/29/23 03:07 V41839MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 12/29/23 03:07 V41839MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 12/29/23 03:07 V41839MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 12/29/23 03:07 V41839MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 12/29/23 03:07 V41839MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 12/29/23 03:07 V41839MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 12/29/23 03:07 V41839MSA
<0.220 µg/L 0.220 0.500Chloroform 1 12/29/23 03:07 V41839MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 12/29/23 03:07 V41839MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 12/29/23 03:07 V41839MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 12/29/23 03:07 V41839MSA
0.562 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 12/29/23 03:07 V41839MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 12/29/23 03:07 V41839MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 12/29/23 03:07 V41839MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 12/29/23 03:07 V41839MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 12/29/23 03:07 V41839MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 8 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-3
92466 Matrix:
12/19/2023 11:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41838 12/28/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 12/29/23 03:07 V41839MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 12/29/23 03:07 V41839MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 12/29/23 03:07 V41839MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 12/29/23 03:07 V41839MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 12/29/23 03:07 V41839MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 12/29/23 03:07 V41839MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 12/29/23 03:07 V41839MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 12/29/23 03:07 V41839MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 12/29/23 03:07 V41839MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 12/29/23 03:07 V41839MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 12/29/23 03:07 V41839MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 12/29/23 03:07 V41839MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 12/29/23 03:07 V41839MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 12/29/23 03:07 V41839MSA
<42.0 µg/L 42.0 200Ethanol 1 12/29/23 03:07 V41839MSA
0.279 J µg/L 0.170 0.500Ethylbenzene 1 12/29/23 03:07 V41839MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 12/29/23 03:07 V41839MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 12/29/23 03:07 V41839MSA
0.218 J µg/L 0.180 0.500Isopropylbenzene 1 12/29/23 03:07 V41839MSA
0.377 J µg/L 0.089 0.5004-Isopropyl toluene 1 12/29/23 03:07 V41839MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 12/29/23 03:07 V41839MSA
0.233 J µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 12/29/23 03:07 V41839MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 12/29/23 03:07 V41839MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 9 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-3
92466 Matrix:
12/19/2023 11:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41838 12/28/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 12/29/23 03:07 V41839MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 12/29/23 03:07 V41839MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 12/29/23 03:07 V41839MSA
<0.220 µg/L 0.220 0.500Styrene 1 12/29/23 03:07 V41839MSA
13.4 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 12/29/23 03:07 V41839MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 12/29/23 03:07 V41839MSA
95.4 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 12/29/23 03:07 V41839MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 12/29/23 03:07 V41839MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 12/29/23 03:07 V41839MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 12/29/23 03:07 V41839MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 12/29/23 03:07 V41839MSA
2.38 µg/L 0.220 0.500Toluene 1 12/29/23 03:07 V41839MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 12/29/23 03:07 V41839MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 12/29/23 03:07 V41839MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 12/29/23 03:07 V41839MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 12/29/23 03:07 V41839MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 12/29/23 03:07 V41839MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 12/29/23 03:07 V41839MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 12/29/23 03:07 V41839MSA
0.598 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 12/29/23 03:07 V41839MSA
0.478 J µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 12/29/23 03:07 V41839MSA
<1.00 M µg/L 1.00 5.00Vinyl Acetate 1 12/29/23 03:07 V41839MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 12/29/23 03:07 V41839MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 10 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-3
92466 Matrix:
12/19/2023 11:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41838 12/28/23 14:00
0.820 µg/L 0.210 0.500o-Xylene 1 12/29/23 03:07 V41839MSA
3.39 µg/L 0.420 1.00m,p-Xylene 1 12/29/23 03:07 V41839MSA
4.21 µg/L 0.210 0.500Xylene (Total)1 12/29/23 03:07 V41839
Surrogate: 4-Bromofluorobenzene 99.0 Limits: 70-130%12/29/23 03:071 MSA V41839
Surrogate: Dibromofluoromethane 95.8 Limits: 70-130%12/29/23 03:071 MSA V41839
Surrogate: 1,2-Dichloroethane - d4 91.6 Limits: 70-130%12/29/23 03:071 MSA V41839
Surrogate: Toluene-d8 102 Limits: 70-130%12/29/23 03:071 MSA V41839
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 11 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-4
92467 Matrix:
12/19/2023 11:08
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 12/29/23 10:07 6200BMSA
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%12/29/23 10:07100 MSA V41839
Surrogate: Dibromofluoromethane 95.8 Limits: 70-130%12/29/23 10:07100 MSA V41839
Surrogate: 1,2-Dichloroethane - d4 89.8 Limits: 70-130%12/29/23 10:07100 MSA V41839
Surrogate: Toluene-d8 103 Limits: 70-130%12/29/23 10:07100 MSA V41839
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 12 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-4
92467 Matrix:
12/19/2023 11:08
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41838 12/28/23 14:00
898 J µg/L 180 1000Acetone 100 12/29/23 10:07 V41839MSA
4300 µg/L 18.0 50.0Benzene 100 12/29/23 10:07 V41839MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 12/29/23 10:07 V41839MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 12/29/23 10:07 V41839MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 12/29/23 10:07 V41839MSA
<150 µg/L 150 500Bromoform 100 12/29/23 10:07 V41839MSA
<28.0 µg/L 28.0 100Bromomethane 100 12/29/23 10:07 V41839MSA
74.7 µg/L 18.0 50.0n-Butylbenzene 100 12/29/23 10:07 V41839MSA
43.6 J µg/L 20.0 50.0sec-Butyl benzene 100 12/29/23 10:07 V41839MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 12/29/23 10:07 V41839MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 12/29/23 10:07 V41839MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 12/29/23 10:07 V41839MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 12/29/23 10:07 V41839MSA
<43.0 µg/L 43.0 100Chloroethane 100 12/29/23 10:07 V41839MSA
<22.0 µg/L 22.0 50.0Chloroform 100 12/29/23 10:07 V41839MSA
<22.0 µg/L 22.0 50.0Chloromethane 100 12/29/23 10:07 V41839MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 12/29/23 10:07 V41839MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 12/29/23 10:07 V41839MSA
<50.0 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 12/29/23 10:07 V41839MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 12/29/23 10:07 V41839MSA
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 12/29/23 10:07 V41839MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 12/29/23 10:07 V41839MSA
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 12/29/23 10:07 V41839MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 13 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-4
92467 Matrix:
12/19/2023 11:08
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41838 12/28/23 14:00
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 12/29/23 10:07 V41839MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 12/29/23 10:07 V41839MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 12/29/23 10:07 V41839MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 12/29/23 10:07 V41839MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 12/29/23 10:07 V41839MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 12/29/23 10:07 V41839MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 12/29/23 10:07 V41839MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 12/29/23 10:07 V41839MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 12/29/23 10:07 V41839MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 12/29/23 10:07 V41839MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 12/29/23 10:07 V41839MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 12/29/23 10:07 V41839MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 12/29/23 10:07 V41839MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 12/29/23 10:07 V41839MSA
<4200 µg/L 4200 20000Ethanol 100 12/29/23 10:07 V41839MSA
2930 µg/L 17.0 50.0Ethylbenzene 100 12/29/23 10:07 V41839MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 12/29/23 10:07 V41839MSA
102 µg/L 38.0 1002-Hexanone 100 12/29/23 10:07 V41839MSA
212 µg/L 18.0 50.0Isopropylbenzene 100 12/29/23 10:07 V41839MSA
31.8 J µg/L 8.90 50.04-Isopropyl toluene 100 12/29/23 10:07 V41839MSA
401 J µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 12/29/23 10:07 V41839MSA
<14.0 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 12/29/23 10:07 V41839MSA
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 12/29/23 10:07 V41839MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 14 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-4
92467 Matrix:
12/19/2023 11:08
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41838 12/28/23 14:00
<33.0 µg/L 33.0 200Methylene Chloride 100 12/29/23 10:07 V41839MSA
806 µg/L 47.0 100Naphthalene 100 12/29/23 10:07 V41839MSA
500 µg/L 19.0 50.0n-Propylbenzene 100 12/29/23 10:07 V41839MSA
28.0 J µg/L 22.0 50.0Styrene 100 12/29/23 10:07 V41839MSA
<160 µg/L 160 1000tert-Butyl Alcohol (TBA)100 12/29/23 10:07 V41839MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 12/29/23 10:07 V41839MSA
596 J µg/L 190 1000tert-Amyl Alcohol (TAA)100 12/29/23 10:07 V41839MSA
<28.0 µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 12/29/23 10:07 V41839MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 12/29/23 10:07 V41839MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 12/29/23 10:07 V41839MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 12/29/23 10:07 V41839MSA
136.36 E µg/L 22.0 50.0Toluene 100 12/29/23 10:07 V41839MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 12/29/23 10:07 V41839MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 12/29/23 10:07 V41839MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 12/29/23 10:07 V41839MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 12/29/23 10:07 V41839MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 12/29/23 10:07 V41839MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 12/29/23 10:07 V41839MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 12/29/23 10:07 V41839MSA
5710 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 12/29/23 10:07 V41839MSA
1490 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 12/29/23 10:07 V41839MSA
<100 M µg/L 100 500Vinyl Acetate 100 12/29/23 10:07 V41839MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 12/29/23 10:07 V41839MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 15 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-4
92467 Matrix:
12/19/2023 11:08
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41838 12/28/23 14:00
6410 µg/L 21.0 50.0o-Xylene 100 12/29/23 10:07 V41839MSA
12700 µg/L 42.0 100m,p-Xylene 100 12/29/23 10:07 V41839MSA
19100 µg/L 21.0 50.0Xylene (Total)100 12/29/23 10:07 V41839KCC
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%12/29/23 10:07100 MSA V41839
Surrogate: Dibromofluoromethane 95.8 Limits: 70-130%12/29/23 10:07100 MSA V41839
Surrogate: 1,2-Dichloroethane - d4 89.8 Limits: 70-130%12/29/23 10:07100 MSA V41839
Surrogate: Toluene-d8 103 Limits: 70-130%12/29/23 10:07100 MSA V41839
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 16 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-5
92468 Matrix:
12/19/2023 10:05
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 12/28/23 02:07 6200BMSA
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%12/28/23 02:071 MSA V41777
Surrogate: Dibromofluoromethane 98.6 Limits: 70-130%12/28/23 02:071 MSA V41777
Surrogate: 1,2-Dichloroethane - d4 91.6 Limits: 70-130%12/28/23 02:071 MSA V41777
Surrogate: Toluene-d8 104 Limits: 70-130%12/28/23 02:071 MSA V41777
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 17 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-5
92468 Matrix:
12/19/2023 10:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 12/28/23 02:07 V41777MSA
<0.180 µg/L 0.180 0.500Benzene 1 12/28/23 02:07 V41777MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 12/28/23 02:07 V41777MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 12/28/23 02:07 V41777MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 12/28/23 02:07 V41777MSA
<1.50 µg/L 1.50 5.00Bromoform 1 12/28/23 02:07 V41777MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 12/28/23 02:07 V41777MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 12/28/23 02:07 V41777MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 12/28/23 02:07 V41777MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 12/28/23 02:07 V41777MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 12/28/23 02:07 V41777MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 12/28/23 02:07 V41777MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 12/28/23 02:07 V41777MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 12/28/23 02:07 V41777MSA
<0.220 µg/L 0.220 0.500Chloroform 1 12/28/23 02:07 V41777MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 12/28/23 02:07 V41777MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 12/28/23 02:07 V41777MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 12/28/23 02:07 V41777MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 12/28/23 02:07 V41777MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 12/28/23 02:07 V41777MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 12/28/23 02:07 V41777MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 12/28/23 02:07 V41777MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 12/28/23 02:07 V41777MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 18 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-5
92468 Matrix:
12/19/2023 10:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 12/28/23 02:07 V41777MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 12/28/23 02:07 V41777MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 12/28/23 02:07 V41777MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 12/28/23 02:07 V41777MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 12/28/23 02:07 V41777MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 12/28/23 02:07 V41777MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 12/28/23 02:07 V41777MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 12/28/23 02:07 V41777MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 12/28/23 02:07 V41777MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 12/28/23 02:07 V41777MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 12/28/23 02:07 V41777MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 12/28/23 02:07 V41777MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 12/28/23 02:07 V41777MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 12/28/23 02:07 V41777MSA
<42.0 µg/L 42.0 200Ethanol 1 12/28/23 02:07 V41777MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 12/28/23 02:07 V41777MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 12/28/23 02:07 V41777MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 12/28/23 02:07 V41777MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 12/28/23 02:07 V41777MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 12/28/23 02:07 V41777MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 12/28/23 02:07 V41777MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 12/28/23 02:07 V41777MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 12/28/23 02:07 V41777MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 19 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-5
92468 Matrix:
12/19/2023 10:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 12/28/23 02:07 V41777MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 12/28/23 02:07 V41777MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 12/28/23 02:07 V41777MSA
<0.220 µg/L 0.220 0.500Styrene 1 12/28/23 02:07 V41777MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 12/28/23 02:07 V41777MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 12/28/23 02:07 V41777MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 12/28/23 02:07 V41777MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 12/28/23 02:07 V41777MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 12/28/23 02:07 V41777MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 12/28/23 02:07 V41777MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 12/28/23 02:07 V41777MSA
<0.220 µg/L 0.220 0.500Toluene 1 12/28/23 02:07 V41777MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 12/28/23 02:07 V41777MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 12/28/23 02:07 V41777MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 12/28/23 02:07 V41777MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 12/28/23 02:07 V41777MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 12/28/23 02:07 V41777MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 12/28/23 02:07 V41777MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 12/28/23 02:07 V41777MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 12/28/23 02:07 V41777MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 12/28/23 02:07 V41777MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 12/28/23 02:07 V41777MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 12/28/23 02:07 V41777MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 20 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-5
92468 Matrix:
12/19/2023 10:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00
<0.210 µg/L 0.210 0.500o-Xylene 1 12/28/23 02:07 V41777MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 12/28/23 02:07 V41777MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 12/28/23 02:07 V41777
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%12/28/23 02:071 MSA V41777
Surrogate: Dibromofluoromethane 98.6 Limits: 70-130%12/28/23 02:071 MSA V41777
Surrogate: 1,2-Dichloroethane - d4 91.6 Limits: 70-130%12/28/23 02:071 MSA V41777
Surrogate: Toluene-d8 104 Limits: 70-130%12/28/23 02:071 MSA V41777
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 21 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-7
92469 Matrix:
12/19/2023 10:51
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 12/28/23 02:32 6200BMSA
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%12/28/23 02:321 MSA V41777
Surrogate: Dibromofluoromethane 99.6 Limits: 70-130%12/28/23 02:321 MSA V41777
Surrogate: 1,2-Dichloroethane - d4 93.8 Limits: 70-130%12/28/23 02:321 MSA V41777
Surrogate: Toluene-d8 105 Limits: 70-130%12/28/23 02:321 MSA V41777
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%12/29/23 09:4210 MSA V41839
Surrogate: Dibromofluoromethane 94.6 Limits: 70-130%12/29/23 09:4210 MSA V41839
Surrogate: 1,2-Dichloroethane - d4 90.4 Limits: 70-130%12/29/23 09:4210 MSA V41839
Surrogate: Toluene-d8 104 Limits: 70-130%12/29/23 09:4210 MSA V41839
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 22 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-7
92469 Matrix:
12/19/2023 10:51
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00 V41838 12/28/23 14:00
40.7 µg/L 1.80 10.0Acetone 1 12/28/23 02:32 V41777MSA
7.97 µg/L 0.180 0.500Benzene 1 12/28/23 02:32 V41777MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 12/28/23 02:32 V41777MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 12/28/23 02:32 V41777MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 12/28/23 02:32 V41777MSA
<1.50 µg/L 1.50 5.00Bromoform 1 12/28/23 02:32 V41777MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 12/28/23 02:32 V41777MSA
1.64 µg/L 0.180 0.500n-Butylbenzene 1 12/28/23 02:32 V41777MSA
1.86 µg/L 0.200 0.500sec-Butyl benzene 1 12/28/23 02:32 V41777MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 12/28/23 02:32 V41777MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 12/28/23 02:32 V41777MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 12/28/23 02:32 V41777MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 12/28/23 02:32 V41777MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 12/28/23 02:32 V41777MSA
<0.220 µg/L 0.220 0.500Chloroform 1 12/28/23 02:32 V41777MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 12/28/23 02:32 V41777MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 12/28/23 02:32 V41777MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 12/28/23 02:32 V41777MSA
0.653 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 12/28/23 02:32 V41777MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 12/28/23 02:32 V41777MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 12/28/23 02:32 V41777MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 12/28/23 02:32 V41777MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 12/28/23 02:32 V41777MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 23 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-7
92469 Matrix:
12/19/2023 10:51
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00 V41838 12/28/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 12/28/23 02:32 V41777MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 12/28/23 02:32 V41777MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 12/28/23 02:32 V41777MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 12/28/23 02:32 V41777MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 12/28/23 02:32 V41777MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 12/28/23 02:32 V41777MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 12/28/23 02:32 V41777MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 12/28/23 02:32 V41777MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 12/28/23 02:32 V41777MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 12/28/23 02:32 V41777MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 12/28/23 02:32 V41777MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 12/28/23 02:32 V41777MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 12/28/23 02:32 V41777MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 12/28/23 02:32 V41777MSA
<42.0 µg/L 42.0 200Ethanol 1 12/28/23 02:32 V41777MSA
1.69 µg/L 0.170 0.500Ethylbenzene 1 12/28/23 02:32 V41777MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 12/28/23 02:32 V41777MSA
1.28 µg/L 0.380 1.002-Hexanone 1 12/28/23 02:32 V41777MSA
7.22 µg/L 0.180 0.500Isopropylbenzene 1 12/28/23 02:32 V41777MSA
1.72 µg/L 0.089 0.5004-Isopropyl toluene 1 12/28/23 02:32 V41777MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 12/28/23 02:32 V41777MSA
0.664 J µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 12/28/23 02:32 V41777MSA
2.46 µg/L 0.078 1.004-Methyl-2-Pentanone 1 12/28/23 02:32 V41777MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 24 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-7
92469 Matrix:
12/19/2023 10:51
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00 V41838 12/28/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 12/28/23 02:32 V41777MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 12/28/23 02:32 V41777MSA
1.61 µg/L 0.190 0.500n-Propylbenzene 1 12/28/23 02:32 V41777MSA
<0.220 µg/L 0.220 0.500Styrene 1 12/28/23 02:32 V41777MSA
173 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 12/28/23 02:32 V41777MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 12/28/23 02:32 V41777MSA
118 µg/L 19.0 100tert-Amyl Alcohol (TAA)10 12/29/23 09:42 V41839MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 12/28/23 02:32 V41777MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 12/28/23 02:32 V41777MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 12/28/23 02:32 V41777MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 12/28/23 02:32 V41777MSA
0.572 µg/L 0.220 0.500Toluene 1 12/28/23 02:32 V41777MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 12/28/23 02:32 V41777MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 12/28/23 02:32 V41777MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 12/28/23 02:32 V41777MSA
2.22 µg/L 0.096 0.5001,1,2-Trichloroethane 1 12/28/23 02:32 V41777MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 12/28/23 02:32 V41777MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 12/28/23 02:32 V41777MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 12/28/23 02:32 V41777MSA
1.77 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 12/28/23 02:32 V41777MSA
2.40 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 12/28/23 02:32 V41777MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 12/28/23 02:32 V41777MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 12/28/23 02:32 V41777MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 25 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-7
92469 Matrix:
12/19/2023 10:51
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00 V41838 12/28/23 14:00
2.47 µg/L 0.210 0.500o-Xylene 1 12/28/23 02:32 V41777MSA
4.41 µg/L 0.420 1.00m,p-Xylene 1 12/28/23 02:32 V41777MSA
6.88 µg/L 0.210 0.500Xylene (Total)1 12/28/23 02:32 V41777
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%12/28/23 02:321 MSA V41777
Surrogate: Dibromofluoromethane 99.6 Limits: 70-130%12/28/23 02:321 MSA V41777
Surrogate: 1,2-Dichloroethane - d4 93.8 Limits: 70-130%12/28/23 02:321 MSA V41777
Surrogate: Toluene-d8 105 Limits: 70-130%12/28/23 02:321 MSA V41777
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%12/29/23 09:4210 MSA V41839
Surrogate: Dibromofluoromethane 94.6 Limits: 70-130%12/29/23 09:4210 MSA V41839
Surrogate: 1,2-Dichloroethane - d4 90.4 Limits: 70-130%12/29/23 09:4210 MSA V41839
Surrogate: Toluene-d8 104 Limits: 70-130%12/29/23 09:4210 MSA V41839
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 26 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-8
92470 Matrix:
12/19/2023 10:33
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0 1003,3-Dimethyl-1-butanol 10 12/28/23 07:03 6200BMSA
Surrogate: 4-Bromofluorobenzene 99.2 Limits: 70-130%12/28/23 07:0310 MSA V41777
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%12/28/23 07:0310 MSA V41777
Surrogate: 1,2-Dichloroethane - d4 90.6 Limits: 70-130%12/28/23 07:0310 MSA V41777
Surrogate: Toluene-d8 103 Limits: 70-130%12/28/23 07:0310 MSA V41777
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 27 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-8
92470 Matrix:
12/19/2023 10:33
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00
<18.0 µg/L 18.0 100Acetone 10 12/28/23 07:03 V41777MSA
<1.80 µg/L 1.80 5.00Benzene 10 12/28/23 07:03 V41777MSA
<2.10 µg/L 2.10 5.00Bromobenzene 10 12/28/23 07:03 V41777MSA
<4.20 µg/L 4.20 10.0Bromochloromethane 10 12/28/23 07:03 V41777MSA
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 12/28/23 07:03 V41777MSA
<15.0 µg/L 15.0 50.0Bromoform 10 12/28/23 07:03 V41777MSA
<2.80 µg/L 2.80 10.0Bromomethane 10 12/28/23 07:03 V41777MSA
<1.80 µg/L 1.80 5.00n-Butylbenzene 10 12/28/23 07:03 V41777MSA
<2.00 µg/L 2.00 5.00sec-Butyl benzene 10 12/28/23 07:03 V41777MSA
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 12/28/23 07:03 V41777MSA
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 12/28/23 07:03 V41777MSA
<1.90 µg/L 1.90 5.00Chlorobenzene 10 12/28/23 07:03 V41777MSA
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 12/28/23 07:03 V41777MSA
<4.30 µg/L 4.30 10.0Chloroethane 10 12/28/23 07:03 V41777MSA
<2.20 µg/L 2.20 5.00Chloroform 10 12/28/23 07:03 V41777MSA
<2.20 µg/L 2.20 5.00Chloromethane 10 12/28/23 07:03 V41777MSA
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 12/28/23 07:03 V41777MSA
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 12/28/23 07:03 V41777MSA
<5.00 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 12/28/23 07:03 V41777MSA
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 12/28/23 07:03 V41777MSA
<2.00 µg/L 2.00 5.001,2-Dibromoethane 10 12/28/23 07:03 V41777MSA
<2.30 µg/L 2.30 5.00Dibromomethane 10 12/28/23 07:03 V41777MSA
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 12/28/23 07:03 V41777MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 28 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-8
92470 Matrix:
12/19/2023 10:33
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 12/28/23 07:03 V41777MSA
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 12/28/23 07:03 V41777MSA
<12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 12/28/23 07:03 V41777MSA
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 12/28/23 07:03 V41777MSA
<1.50 µg/L 1.50 5.001,2-Dichloroethane 10 12/28/23 07:03 V41777MSA
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 12/28/23 07:03 V41777MSA
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 12/28/23 07:03 V41777MSA
<1.80 µg/L 1.80 5.00trans-1,2-Dichloroethene 10 12/28/23 07:03 V41777MSA
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 12/28/23 07:03 V41777MSA
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 12/28/23 07:03 V41777MSA
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 12/28/23 07:03 V41777MSA
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 12/28/23 07:03 V41777MSA
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 12/28/23 07:03 V41777MSA
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 12/28/23 07:03 V41777MSA
<420 µg/L 420 2000Ethanol 10 12/28/23 07:03 V41777MSA
<1.70 µg/L 1.70 5.00Ethylbenzene 10 12/28/23 07:03 V41777MSA
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 12/28/23 07:03 V41777MSA
<3.80 µg/L 3.80 10.02-Hexanone 10 12/28/23 07:03 V41777MSA
<1.80 µg/L 1.80 5.00Isopropylbenzene 10 12/28/23 07:03 V41777MSA
<0.890 µg/L 0.890 5.004-Isopropyl toluene 10 12/28/23 07:03 V41777MSA
<7.10 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 12/28/23 07:03 V41777MSA
<1.40 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 12/28/23 07:03 V41777MSA
<0.780 µg/L 0.780 10.04-Methyl-2-Pentanone 10 12/28/23 07:03 V41777MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 29 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-8
92470 Matrix:
12/19/2023 10:33
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00
<3.30 µg/L 3.30 20.0Methylene Chloride 10 12/28/23 07:03 V41777MSA
<4.70 µg/L 4.70 10.0Naphthalene 10 12/28/23 07:03 V41777MSA
<1.90 µg/L 1.90 5.00n-Propylbenzene 10 12/28/23 07:03 V41777MSA
<2.20 µg/L 2.20 5.00Styrene 10 12/28/23 07:03 V41777MSA
<16.0 µg/L 16.0 100tert-Butyl Alcohol (TBA)10 12/28/23 07:03 V41777MSA
<3.50 µg/L 3.50 100tert-Butyl formate (TBF)10 12/28/23 07:03 V41777MSA
<19.0 µg/L 19.0 100tert-Amyl Alcohol (TAA)10 12/28/23 07:03 V41777MSA
<2.80 µg/L 2.80 100tert-Amyl Methyl Ether (TAME)10 12/28/23 07:03 V41777MSA
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 12/28/23 07:03 V41777MSA
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 12/28/23 07:03 V41777MSA
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 12/28/23 07:03 V41777MSA
<2.20 µg/L 2.20 5.00Toluene 10 12/28/23 07:03 V41777MSA
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 12/28/23 07:03 V41777MSA
<3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 12/28/23 07:03 V41777MSA
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 12/28/23 07:03 V41777MSA
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 12/28/23 07:03 V41777MSA
<1.80 µg/L 1.80 5.00Trichloroethene 10 12/28/23 07:03 V41777MSA
<1.80 µg/L 1.80 5.00Trichlorofluoromethane 10 12/28/23 07:03 V41777MSA
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 12/28/23 07:03 V41777MSA
<1.90 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 12/28/23 07:03 V41777MSA
<1.80 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 12/28/23 07:03 V41777MSA
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 12/28/23 07:03 V41777MSA
<1.70 µg/L 1.70 5.00Vinyl Chloride 10 12/28/23 07:03 V41777MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 30 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-8
92470 Matrix:
12/19/2023 10:33
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00
<2.10 µg/L 2.10 5.00o-Xylene 10 12/28/23 07:03 V41777MSA
<4.20 µg/L 4.20 10.0m,p-Xylene 10 12/28/23 07:03 V41777MSA
<2.1 µg/L 2.10 5.00Xylene (Total)10 12/28/23 07:03 V41777
Surrogate: 4-Bromofluorobenzene 99.2 Limits: 70-130%12/28/23 07:0310 MSA V41777
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%12/28/23 07:0310 MSA V41777
Surrogate: 1,2-Dichloroethane - d4 90.6 Limits: 70-130%12/28/23 07:0310 MSA V41777
Surrogate: Toluene-d8 103 Limits: 70-130%12/28/23 07:0310 MSA V41777
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 31 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-9
92471 Matrix:
12/19/2023 10:15
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 12/28/23 02:56 6200BMSA
Surrogate: 4-Bromofluorobenzene 98.6 Limits: 70-130%12/28/23 02:561 MSA V41777
Surrogate: Dibromofluoromethane 97.6 Limits: 70-130%12/28/23 02:561 MSA V41777
Surrogate: 1,2-Dichloroethane - d4 90.6 Limits: 70-130%12/28/23 02:561 MSA V41777
Surrogate: Toluene-d8 105 Limits: 70-130%12/28/23 02:561 MSA V41777
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 32 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-9
92471 Matrix:
12/19/2023 10:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 12/28/23 02:56 V41777MSA
<0.180 µg/L 0.180 0.500Benzene 1 12/28/23 02:56 V41777MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 12/28/23 02:56 V41777MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 12/28/23 02:56 V41777MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 12/28/23 02:56 V41777MSA
<1.50 µg/L 1.50 5.00Bromoform 1 12/28/23 02:56 V41777MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 12/28/23 02:56 V41777MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 12/28/23 02:56 V41777MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 12/28/23 02:56 V41777MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 12/28/23 02:56 V41777MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 12/28/23 02:56 V41777MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 12/28/23 02:56 V41777MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 12/28/23 02:56 V41777MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 12/28/23 02:56 V41777MSA
<0.220 µg/L 0.220 0.500Chloroform 1 12/28/23 02:56 V41777MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 12/28/23 02:56 V41777MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 12/28/23 02:56 V41777MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 12/28/23 02:56 V41777MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 12/28/23 02:56 V41777MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 12/28/23 02:56 V41777MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 12/28/23 02:56 V41777MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 12/28/23 02:56 V41777MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 12/28/23 02:56 V41777MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 33 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-9
92471 Matrix:
12/19/2023 10:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 12/28/23 02:56 V41777MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 12/28/23 02:56 V41777MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 12/28/23 02:56 V41777MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 12/28/23 02:56 V41777MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 12/28/23 02:56 V41777MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 12/28/23 02:56 V41777MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 12/28/23 02:56 V41777MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 12/28/23 02:56 V41777MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 12/28/23 02:56 V41777MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 12/28/23 02:56 V41777MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 12/28/23 02:56 V41777MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 12/28/23 02:56 V41777MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 12/28/23 02:56 V41777MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 12/28/23 02:56 V41777MSA
<42.0 µg/L 42.0 200Ethanol 1 12/28/23 02:56 V41777MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 12/28/23 02:56 V41777MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 12/28/23 02:56 V41777MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 12/28/23 02:56 V41777MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 12/28/23 02:56 V41777MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 12/28/23 02:56 V41777MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 12/28/23 02:56 V41777MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 12/28/23 02:56 V41777MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 12/28/23 02:56 V41777MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 34 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-9
92471 Matrix:
12/19/2023 10:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 12/28/23 02:56 V41777MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 12/28/23 02:56 V41777MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 12/28/23 02:56 V41777MSA
<0.220 µg/L 0.220 0.500Styrene 1 12/28/23 02:56 V41777MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 12/28/23 02:56 V41777MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 12/28/23 02:56 V41777MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 12/28/23 02:56 V41777MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 12/28/23 02:56 V41777MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 12/28/23 02:56 V41777MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 12/28/23 02:56 V41777MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 12/28/23 02:56 V41777MSA
<0.220 µg/L 0.220 0.500Toluene 1 12/28/23 02:56 V41777MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 12/28/23 02:56 V41777MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 12/28/23 02:56 V41777MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 12/28/23 02:56 V41777MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 12/28/23 02:56 V41777MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 12/28/23 02:56 V41777MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 12/28/23 02:56 V41777MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 12/28/23 02:56 V41777MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 12/28/23 02:56 V41777MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 12/28/23 02:56 V41777MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 12/28/23 02:56 V41777MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 12/28/23 02:56 V41777MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 35 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:MW-9
92471 Matrix:
12/19/2023 10:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00
<0.210 µg/L 0.210 0.500o-Xylene 1 12/28/23 02:56 V41777MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 12/28/23 02:56 V41777MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 12/28/23 02:56 V41777
Surrogate: 4-Bromofluorobenzene 98.6 Limits: 70-130%12/28/23 02:561 MSA V41777
Surrogate: Dibromofluoromethane 97.6 Limits: 70-130%12/28/23 02:561 MSA V41777
Surrogate: 1,2-Dichloroethane - d4 90.6 Limits: 70-130%12/28/23 02:561 MSA V41777
Surrogate: Toluene-d8 105 Limits: 70-130%12/28/23 02:561 MSA V41777
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 36 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:TW-1
92472 Matrix:
12/19/2023 12:13
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 12/28/23 03:21 6200BMSA
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%12/28/23 03:211 MSA V41777
Surrogate: Dibromofluoromethane 96.8 Limits: 70-130%12/28/23 03:211 MSA V41777
Surrogate: 1,2-Dichloroethane - d4 89.0 Limits: 70-130%12/28/23 03:211 MSA V41777
Surrogate: Toluene-d8 106 Limits: 70-130%12/28/23 03:211 MSA V41777
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 37 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:TW-1
92472 Matrix:
12/19/2023 12:13
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 12/28/23 03:21 V41777MSA
2.73 µg/L 0.180 0.500Benzene 1 12/28/23 03:21 V41777MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 12/28/23 03:21 V41777MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 12/28/23 03:21 V41777MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 12/28/23 03:21 V41777MSA
<1.50 µg/L 1.50 5.00Bromoform 1 12/28/23 03:21 V41777MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 12/28/23 03:21 V41777MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 12/28/23 03:21 V41777MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 12/28/23 03:21 V41777MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 12/28/23 03:21 V41777MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 12/28/23 03:21 V41777MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 12/28/23 03:21 V41777MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 12/28/23 03:21 V41777MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 12/28/23 03:21 V41777MSA
<0.220 µg/L 0.220 0.500Chloroform 1 12/28/23 03:21 V41777MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 12/28/23 03:21 V41777MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 12/28/23 03:21 V41777MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 12/28/23 03:21 V41777MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 12/28/23 03:21 V41777MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 12/28/23 03:21 V41777MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 12/28/23 03:21 V41777MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 12/28/23 03:21 V41777MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 12/28/23 03:21 V41777MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 38 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:TW-1
92472 Matrix:
12/19/2023 12:13
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 12/28/23 03:21 V41777MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 12/28/23 03:21 V41777MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 12/28/23 03:21 V41777MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 12/28/23 03:21 V41777MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 12/28/23 03:21 V41777MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 12/28/23 03:21 V41777MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 12/28/23 03:21 V41777MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 12/28/23 03:21 V41777MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 12/28/23 03:21 V41777MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 12/28/23 03:21 V41777MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 12/28/23 03:21 V41777MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 12/28/23 03:21 V41777MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 12/28/23 03:21 V41777MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 12/28/23 03:21 V41777MSA
<42.0 µg/L 42.0 200Ethanol 1 12/28/23 03:21 V41777MSA
0.435 J µg/L 0.170 0.500Ethylbenzene 1 12/28/23 03:21 V41777MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 12/28/23 03:21 V41777MSA
8.76 µg/L 0.380 1.002-Hexanone 1 12/28/23 03:21 V41777MSA
0.563 µg/L 0.180 0.500Isopropylbenzene 1 12/28/23 03:21 V41777MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 12/28/23 03:21 V41777MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 12/28/23 03:21 V41777MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 12/28/23 03:21 V41777MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 12/28/23 03:21 V41777MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 39 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:TW-1
92472 Matrix:
12/19/2023 12:13
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 12/28/23 03:21 V41777MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 12/28/23 03:21 V41777MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 12/28/23 03:21 V41777MSA
<0.220 µg/L 0.220 0.500Styrene 1 12/28/23 03:21 V41777MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 12/28/23 03:21 V41777MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 12/28/23 03:21 V41777MSA
6.92 J µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 12/28/23 03:21 V41777MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 12/28/23 03:21 V41777MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 12/28/23 03:21 V41777MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 12/28/23 03:21 V41777MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 12/28/23 03:21 V41777MSA
<0.220 µg/L 0.220 0.500Toluene 1 12/28/23 03:21 V41777MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 12/28/23 03:21 V41777MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 12/28/23 03:21 V41777MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 12/28/23 03:21 V41777MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 12/28/23 03:21 V41777MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 12/28/23 03:21 V41777MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 12/28/23 03:21 V41777MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 12/28/23 03:21 V41777MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 12/28/23 03:21 V41777MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 12/28/23 03:21 V41777MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 12/28/23 03:21 V41777MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 12/28/23 03:21 V41777MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 40 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:TW-1
92472 Matrix:
12/19/2023 12:13
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00
0.214 J µg/L 0.210 0.500o-Xylene 1 12/28/23 03:21 V41777MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 12/28/23 03:21 V41777MSA
0.214 J µg/L 0.210 0.500Xylene (Total)1 12/28/23 03:21 V41777
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%12/28/23 03:211 MSA V41777
Surrogate: Dibromofluoromethane 96.8 Limits: 70-130%12/28/23 03:211 MSA V41777
Surrogate: 1,2-Dichloroethane - d4 89.0 Limits: 70-130%12/28/23 03:211 MSA V41777
Surrogate: Toluene-d8 106 Limits: 70-130%12/28/23 03:211 MSA V41777
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 41 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:Trip Blanks
92473 Matrix:
12/19/2023 7:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 12/28/23 00:04 V41777MSA
<0.180 µg/L 0.180 0.500Benzene 1 12/28/23 00:04 V41777MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 12/28/23 00:04 V41777MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 12/28/23 00:04 V41777MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 12/28/23 00:04 V41777MSA
<1.50 µg/L 1.50 5.00Bromoform 1 12/28/23 00:04 V41777MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 12/28/23 00:04 V41777MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 12/28/23 00:04 V41777MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 12/28/23 00:04 V41777MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 12/28/23 00:04 V41777MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 12/28/23 00:04 V41777MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 12/28/23 00:04 V41777MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 12/28/23 00:04 V41777MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 12/28/23 00:04 V41777MSA
<0.220 µg/L 0.220 0.500Chloroform 1 12/28/23 00:04 V41777MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 12/28/23 00:04 V41777MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 12/28/23 00:04 V41777MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 12/28/23 00:04 V41777MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 12/28/23 00:04 V41777MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 12/28/23 00:04 V41777MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 12/28/23 00:04 V41777MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 12/28/23 00:04 V41777MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 12/28/23 00:04 V41777MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 42 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:Trip Blanks
92473 Matrix:
12/19/2023 7:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 12/28/23 00:04 V41777MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 12/28/23 00:04 V41777MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 12/28/23 00:04 V41777MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 12/28/23 00:04 V41777MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 12/28/23 00:04 V41777MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 12/28/23 00:04 V41777MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 12/28/23 00:04 V41777MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 12/28/23 00:04 V41777MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 12/28/23 00:04 V41777MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 12/28/23 00:04 V41777MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 12/28/23 00:04 V41777MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 12/28/23 00:04 V41777MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 12/28/23 00:04 V41777MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 12/28/23 00:04 V41777MSA
<42.0 µg/L 42.0 200Ethanol 1 12/28/23 00:04 V41777MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 12/28/23 00:04 V41777MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 12/28/23 00:04 V41777MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 12/28/23 00:04 V41777MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 12/28/23 00:04 V41777MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 12/28/23 00:04 V41777MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 12/28/23 00:04 V41777MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 12/28/23 00:04 V41777MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 12/28/23 00:04 V41777MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 43 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:Trip Blanks
92473 Matrix:
12/19/2023 7:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 12/28/23 00:04 V41777MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 12/28/23 00:04 V41777MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 12/28/23 00:04 V41777MSA
<0.220 µg/L 0.220 0.500Styrene 1 12/28/23 00:04 V41777MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 12/28/23 00:04 V41777MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 12/28/23 00:04 V41777MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 12/28/23 00:04 V41777MSA
<0.220 µg/L 0.220 0.500Toluene 1 12/28/23 00:04 V41777MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 12/28/23 00:04 V41777MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 12/28/23 00:04 V41777MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 12/28/23 00:04 V41777MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 12/28/23 00:04 V41777MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 12/28/23 00:04 V41777MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 12/28/23 00:04 V41777MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 12/28/23 00:04 V41777MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 12/28/23 00:04 V41777MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 12/28/23 00:04 V41777MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 12/28/23 00:04 V41777MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 12/28/23 00:04 V41777MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 12/28/23 00:04 V41777MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 12/28/23 00:04 V41777MSA
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 44 of 59
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-354-0023
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5351 Received : 12/20/2023
Kingsway #20
Report Date : 01/05/2024
Sample ID :
Lab No :
Sampled:Trip Blanks
92473 Matrix:
12/19/2023 7:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41775 12/27/23 14:00
<0.21 µg/L 0.210 0.500Xylene (Total)1 12/28/23 00:04 V41777
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%12/28/23 00:041 MSA V41777
Surrogate: Dibromofluoromethane 98.4 Limits: 70-130%12/28/23 00:041 MSA V41777
Surrogate: 1,2-Dichloroethane - d4 89.6 Limits: 70-130%12/28/23 00:041 MSA V41777
Surrogate: Toluene-d8 104 Limits: 70-130%12/28/23 00:041 MSA V41777
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 45 of 59
Quality Control Data
23-354-0023Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #20
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41777QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41775
Associated Lab Samples: 92468, 92469, 92470, 92471, 92472, 92473
LRB-V41775 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/27/23 23:3910.01.80<1.80µg/LAcetone
12/27/23 23:390.5000.180<0.180µg/LBenzene
12/27/23 23:390.5000.210<0.210µg/LBromobenzene
12/27/23 23:391.000.420<0.420µg/LBromochloromethane
12/27/23 23:390.5000.160<0.160µg/LBromodichloromethane
12/27/23 23:395.001.50<1.50µg/LBromoform
12/27/23 23:391.000.280<0.280µg/LBromomethane
12/27/23 23:390.5000.180<0.180µg/Ln-Butylbenzene
12/27/23 23:390.5000.200<0.200µg/Lsec-Butyl benzene
12/27/23 23:392.000.920<0.920µg/Ltert-Butyl benzene
12/27/23 23:390.5000.180<0.180µg/LCarbon Tetrachloride
12/27/23 23:390.5000.190<0.190µg/LChlorobenzene
12/27/23 23:390.5000.190<0.190µg/LChlorodibromomethane
12/27/23 23:391.000.430<0.430µg/LChloroethane
12/27/23 23:390.5000.220<0.220µg/LChloroform
12/27/23 23:390.5000.220<0.220µg/LChloromethane
12/27/23 23:390.5000.200<0.200µg/L2-Chlorotoluene
12/27/23 23:390.5000.200<0.200µg/L4-Chlorotoluene
12/27/23 23:390.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
12/27/23 23:392.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
12/27/23 23:390.5000.200<0.200µg/L1,2-Dibromoethane
12/27/23 23:390.5000.230<0.230µg/LDibromomethane
12/27/23 23:390.5000.220<0.220µg/L1,2-Dichlorobenzene
12/27/23 23:390.5000.190<0.190µg/L1,3-Dichlorobenzene
12/27/23 23:390.5000.210<0.210µg/L1,4-Dichlorobenzene
12/27/23 23:395.001.20<1.20µg/LDichlorodifluoromethane
12/27/23 23:390.5000.240<0.240µg/L1,1-Dichloroethane
Page 1 of 12Date:01/05/2024 03:22 PM
Page 46 of 59
Quality Control Data
23-354-0023Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #20
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41777QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41775
Associated Lab Samples: 92468, 92469, 92470, 92471, 92472, 92473
LRB-V41775 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/27/23 23:390.5000.150<0.150µg/L1,2-Dichloroethane
12/27/23 23:390.5000.150<0.150µg/L1,1-Dichloroethene
12/27/23 23:390.5000.200<0.200µg/Lcis-1,2-Dichloroethene
12/27/23 23:390.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
12/27/23 23:390.5000.190<0.190µg/L1,2-Dichloropropane
12/27/23 23:390.5000.130<0.130µg/L1,3-Dichloropropane
12/27/23 23:392.000.210<0.210µg/L2,2-Dichloropropane
12/27/23 23:390.5000.200<0.200µg/L1,1-Dichloropropene
12/27/23 23:390.5000.210<0.210µg/Lcis-1,3-Dichloropropene
12/27/23 23:390.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
12/27/23 23:3920042.0<42.0µg/LEthanol
12/27/23 23:390.5000.170<0.170µg/LEthylbenzene
12/27/23 23:393.000.350<0.350µg/LHexachlorobutadiene
12/27/23 23:391.000.380<0.380µg/L2-Hexanone
12/27/23 23:390.5000.180<0.180µg/LIsopropylbenzene
12/27/23 23:390.5000.089<0.089µg/L4-Isopropyl toluene
12/27/23 23:395.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
12/27/23 23:391.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
12/27/23 23:391.000.078<0.078µg/L4-Methyl-2-Pentanone
12/27/23 23:392.000.330<0.330µg/LMethylene Chloride
12/27/23 23:391.000.470<0.470µg/LNaphthalene
12/27/23 23:390.5000.190<0.190µg/Ln-Propylbenzene
12/27/23 23:390.5000.220<0.220µg/LStyrene
12/27/23 23:3910.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
12/27/23 23:3910.00.350<0.350µg/Ltert-Butyl formate (TBF)
12/27/23 23:3910.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
12/27/23 23:3910.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 2 of 12Date:01/05/2024 03:22 PM
Page 47 of 59
Quality Control Data
23-354-0023Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #20
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41777QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41775
Associated Lab Samples: 92468, 92469, 92470, 92471, 92472, 92473
LRB-V41775 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/27/23 23:390.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
12/27/23 23:390.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
12/27/23 23:390.5000.220<0.220µg/LTetrachloroethene
12/27/23 23:390.5000.220<0.220µg/LToluene
12/27/23 23:390.5000.380<0.380µg/L1,2,3-Trichlorobenzene
12/27/23 23:390.5000.310<0.310µg/L1,2,4-Trichlorobenzene
12/27/23 23:390.5000.160<0.160µg/L1,1,1-Trichloroethane
12/27/23 23:390.5000.096<0.096µg/L1,1,2-Trichloroethane
12/27/23 23:390.5000.180<0.180µg/LTrichloroethene
12/27/23 23:390.5000.180<0.180µg/LTrichlorofluoromethane
12/27/23 23:390.5000.270<0.270µg/L1,2,3-Trichloropropane
12/27/23 23:390.5000.190<0.190µg/L1,2,4-Trimethylbenzene
12/27/23 23:390.5000.180<0.180µg/L1,3,5-Trimethylbenzene
12/27/23 23:395.001.00<1.00µg/LVinyl Acetate
12/27/23 23:390.5000.170<0.170µg/LVinyl Chloride
12/27/23 23:390.5000.210<0.210µg/Lo-Xylene
12/27/23 23:391.000.420<0.420µg/Lm,p-Xylene
12/27/23 23:3910.01.00<1.00µg/L3,3-Dimethyl-1-butanol
12/27/23 23:394-Bromofluorobenzene (S)99.8 70-130
12/27/23 23:39Dibromofluoromethane (S)97.2 70-130
12/27/23 23:391,2-Dichloroethane - d4 (S)91.2 70-130
12/27/23 23:39Toluene-d8 (S)104 70-130
Page 3 of 12Date:01/05/2024 03:22 PM
Page 48 of 59
Quality Control Data
23-354-0023Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #20
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41777QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41775
LCS-V41775 LCSD-V41775Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
38.0 95.010742.840.0µg/LAcetone 40-160 11.8 20.0
20.0 10010621.120.0µg/LBenzene 70-130 5.3 20.0
23.2 11611823.520.0µg/LBromobenzene 70-130 1.2 20.0
21.0 10510521.020.0µg/LBromochloromethane 70-130 0.0 20.0
19.4 97.010220.420.0µg/LBromodichloromethane 70-130 5.0 20.0
21.6 10811422.720.0µg/LBromoform 70-130 4.9 20.0
20.7 10410220.320.0µg/LBromomethane 60-140 1.9 20.0
23.8 11912525.020.0µg/Ln-Butylbenzene 70-130 4.9 20.0
24.1 12112424.820.0µg/Lsec-Butyl benzene 70-130 2.8 20.0
24.4 12212524.920.0µg/Ltert-Butyl benzene 70-130 2.0 20.0
22.6 11311522.920.0µg/LCarbon Tetrachloride 70-130 1.3 20.0
22.6 11311723.320.0µg/LChlorobenzene 70-130 3.0 20.0
22.3 11211623.220.0µg/LChlorodibromomethane 70-130 3.9 20.0
19.9 99.510220.320.0µg/LChloroethane 60-140 1.9 20.0
20.4 10210621.120.0µg/LChloroform 70-130 3.3 20.0
20.2 10110020.020.0µg/LChloromethane 60-140 0.9 20.0
23.7 11912023.920.0µg/L2-Chlorotoluene 70-130 0.8 20.0
23.3 11711923.720.0µg/L4-Chlorotoluene 70-130 1.7 20.0
18.0 90.094.018.820.0µg/LDi-Isopropyl Ether (DIPE)70-130 4.3 20.0
24.6 12312825.620.0µg/L1,2-Dibromo-3-Chloropropane 70-130 3.9 20.0
22.1 11111623.220.0µg/L1,2-Dibromoethane 70-130 4.8 20.0
20.2 10110420.820.0µg/LDibromomethane 70-130 2.9 20.0
23.8 11912324.520.0µg/L1,2-Dichlorobenzene 70-130 2.8 20.0
23.7 11912124.120.0µg/L1,3-Dichlorobenzene 70-130 1.6 20.0
24.0 12012023.920.0µg/L1,4-Dichlorobenzene 70-130 0.4 20.0
18.1 90.594.018.820.0µg/LDichlorodifluoromethane 60-140 3.7 20.0
Page 4 of 12Date:01/05/2024 03:22 PM
Page 49 of 59
Quality Control Data
23-354-0023Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #20
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41777QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41775
LCS-V41775 LCSD-V41775Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.5 97.510220.320.0µg/L1,1-Dichloroethane 70-130 4.0 20.0
19.1 95.597.519.520.0µg/L1,2-Dichloroethane 70-130 2.0 20.0
20.2 10110821.620.0µg/L1,1-Dichloroethene 70-130 6.6 20.0
18.8 94.099.519.920.0µg/Lcis-1,2-Dichloroethene 70-130 5.6 20.0
19.8 99.010420.820.0µg/Ltrans-1,2-Dichloroethene 70-130 4.9 20.0
19.4 97.098.019.620.0µg/L1,2-Dichloropropane 70-130 1.0 20.0
20.9 10511022.020.0µg/L1,3-Dichloropropane 70-130 5.1 20.0
17.9 89.594.018.820.0µg/L2,2-Dichloropropane 70-130 4.9 20.0
21.4 10711222.320.0µg/L1,1-Dichloropropene 70-130 4.1 20.0
19.0 95.098.519.720.0µg/Lcis-1,3-Dichloropropene 70-130 3.6 20.0
18.8 94.096.519.320.0µg/Ltrans-1,3-Dichloropropene 70-130 2.6 20.0
393 78.688.2441500µg/LEthanol 60-140 11.5 20.0
22.1 11111522.920.0µg/LEthylbenzene 70-130 3.5 20.0
23.7 11912825.620.0µg/LHexachlorobutadiene 70-130 7.7 20.0
19.6 98.010721.320.0µg/L2-Hexanone 60-140 8.3 20.0
24.6 12312725.320.0µg/LIsopropylbenzene 70-130 2.8 20.0
25.1 12612925.820.0µg/L4-Isopropyl toluene 70-130 2.7 20.0
18.7 93.510521.020.0µg/LMethyl Ethyl Ketone (MEK)60-140 11.5 20.0
19.7 98.510020.020.0µg/LMethyl tert-butyl ether (MTBE)70-130 1.5 20.0
17.2 86.090.518.120.0µg/L4-Methyl-2-Pentanone 60-140 5.0 20.0
17.7 88.594.018.820.0µg/LMethylene Chloride 70-130 6.0 20.0
20.9 10511723.320.0µg/LNaphthalene 70-130 10.8 20.0
23.6 11812124.120.0µg/Ln-Propylbenzene 70-130 2.0 20.0
22.3 11211322.620.0µg/LStyrene 70-130 1.3 20.0
41.8 10512148.340.0µg/Ltert-Butyl Alcohol (TBA)40-140 14.4 20.0
23.5 58.755.522.240.0µg/Ltert-Butyl formate (TBF)40-140 5.6 20.0
Page 5 of 12Date:01/05/2024 03:22 PM
Page 50 of 59
Quality Control Data
23-354-0023Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #20
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41777QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41775
LCS-V41775 LCSD-V41775Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
18.5 92.588.017.620.0µg/Ltert-Amyl Alcohol (TAA)40-140 4.9 20.0
43.2 10811144.440.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 2.7 20.0
23.7 11912224.420.0µg/L1,1,1,2-Tetrachloroethane 70-130 2.9 20.0
21.0 10510821.620.0µg/L1,1,2,2-Tetrachloroethane 70-130 2.8 20.0
23.6 11812224.320.0µg/LTetrachloroethene 70-130 2.9 20.0
20.0 10010420.820.0µg/LToluene 70-130 3.9 20.0
21.4 10711923.720.0µg/L1,2,3-Trichlorobenzene 70-130 10.1 20.0
22.6 11312224.320.0µg/L1,2,4-Trichlorobenzene 70-130 7.2 20.0
20.5 10310821.620.0µg/L1,1,1-Trichloroethane 70-130 5.2 20.0
19.8 99.010220.420.0µg/L1,1,2-Trichloroethane 70-130 2.9 20.0
22.0 11011923.820.0µg/LTrichloroethene 70-130 7.8 20.0
23.2 11612024.020.0µg/LTrichlorofluoromethane 60-140 3.3 20.0
22.6 11311322.620.0µg/L1,2,3-Trichloropropane 70-130 0.0 20.0
24.6 12312424.720.0µg/L1,2,4-Trimethylbenzene 70-130 0.4 20.0
24.7 12412625.220.0µg/L1,3,5-Trimethylbenzene 70-130 2.0 20.0
12.6 63.060.012.020.0µg/LVinyl Acetate 60-140 4.8 20.0
21.1 10611022.020.0µg/LVinyl Chloride 60-140 4.1 20.0
22.5 11311522.920.0µg/Lo-Xylene 70-130 1.7 20.0
47.4 11912148.540.0µg/Lm,p-Xylene 70-130 2.2 20.0
17.9 89.570.514.120.0µg/L3,3-Dimethyl-1-butanol 70-130 23.7*20.0
10098.84-Bromofluorobenzene (S)70-130
98.098.2Dibromofluoromethane (S)70-130
91.693.21,2-Dichloroethane - d4 (S)70-130
104105Toluene-d8 (S)70-130
Page 6 of 12* QC Fail Date:01/05/2024 03:22 PM
Page 51 of 59
Quality Control Data
23-354-0023Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #20
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41839QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41838
Associated Lab Samples: 92466, 92467, 92469
LRB-V41838 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/29/23 01:5310.01.80<1.80µg/LAcetone
12/29/23 01:530.5000.180<0.180µg/LBenzene
12/29/23 01:530.5000.210<0.210µg/LBromobenzene
12/29/23 01:531.000.420<0.420µg/LBromochloromethane
12/29/23 01:530.5000.160<0.160µg/LBromodichloromethane
12/29/23 01:535.001.50<1.50µg/LBromoform
12/29/23 01:531.000.280<0.280µg/LBromomethane
12/29/23 01:530.5000.180<0.180µg/Ln-Butylbenzene
12/29/23 01:530.5000.200<0.200µg/Lsec-Butyl benzene
12/29/23 01:532.000.920<0.920µg/Ltert-Butyl benzene
12/29/23 01:530.5000.180<0.180µg/LCarbon Tetrachloride
12/29/23 01:530.5000.190<0.190µg/LChlorobenzene
12/29/23 01:530.5000.190<0.190µg/LChlorodibromomethane
12/29/23 01:531.000.430<0.430µg/LChloroethane
12/29/23 01:530.5000.220<0.220µg/LChloroform
12/29/23 01:530.5000.220<0.220µg/LChloromethane
12/29/23 01:530.5000.200<0.200µg/L2-Chlorotoluene
12/29/23 01:530.5000.200<0.200µg/L4-Chlorotoluene
12/29/23 01:530.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
12/29/23 01:532.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
12/29/23 01:530.5000.200<0.200µg/L1,2-Dibromoethane
12/29/23 01:530.5000.230<0.230µg/LDibromomethane
12/29/23 01:530.5000.220<0.220µg/L1,2-Dichlorobenzene
12/29/23 01:530.5000.190<0.190µg/L1,3-Dichlorobenzene
12/29/23 01:530.5000.210<0.210µg/L1,4-Dichlorobenzene
12/29/23 01:535.001.20<1.20µg/LDichlorodifluoromethane
12/29/23 01:530.5000.240<0.240µg/L1,1-Dichloroethane
Page 7 of 12Date:01/05/2024 03:22 PM
Page 52 of 59
Quality Control Data
23-354-0023Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #20
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41839QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41838
Associated Lab Samples: 92466, 92467, 92469
LRB-V41838 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/29/23 01:530.5000.150<0.150µg/L1,2-Dichloroethane
12/29/23 01:530.5000.150<0.150µg/L1,1-Dichloroethene
12/29/23 01:530.5000.200<0.200µg/Lcis-1,2-Dichloroethene
12/29/23 01:530.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
12/29/23 01:530.5000.190<0.190µg/L1,2-Dichloropropane
12/29/23 01:530.5000.130<0.130µg/L1,3-Dichloropropane
12/29/23 01:532.000.210<0.210µg/L2,2-Dichloropropane
12/29/23 01:530.5000.200<0.200µg/L1,1-Dichloropropene
12/29/23 01:530.5000.210<0.210µg/Lcis-1,3-Dichloropropene
12/29/23 01:530.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
12/29/23 01:5320042.0<42.0µg/LEthanol
12/29/23 01:530.5000.170<0.170µg/LEthylbenzene
12/29/23 01:533.000.350<0.350µg/LHexachlorobutadiene
12/29/23 01:531.000.380<0.380µg/L2-Hexanone
12/29/23 01:530.5000.180<0.180µg/LIsopropylbenzene
12/29/23 01:530.5000.089<0.089µg/L4-Isopropyl toluene
12/29/23 01:535.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
12/29/23 01:531.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
12/29/23 01:531.000.078<0.078µg/L4-Methyl-2-Pentanone
12/29/23 01:532.000.330<0.330µg/LMethylene Chloride
12/29/23 01:531.000.470<0.470µg/LNaphthalene
12/29/23 01:530.5000.190<0.190µg/Ln-Propylbenzene
12/29/23 01:530.5000.220<0.220µg/LStyrene
12/29/23 01:5310.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
12/29/23 01:5310.00.350<0.350µg/Ltert-Butyl formate (TBF)
12/29/23 01:5310.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
12/29/23 01:5310.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 8 of 12Date:01/05/2024 03:22 PM
Page 53 of 59
Quality Control Data
23-354-0023Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #20
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41839QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41838
Associated Lab Samples: 92466, 92467, 92469
LRB-V41838 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/29/23 01:530.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
12/29/23 01:530.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
12/29/23 01:530.5000.220<0.220µg/LTetrachloroethene
12/29/23 01:530.5000.220<0.220µg/LToluene
12/29/23 01:530.5000.380<0.380µg/L1,2,3-Trichlorobenzene
12/29/23 01:530.5000.310<0.310µg/L1,2,4-Trichlorobenzene
12/29/23 01:530.5000.160<0.160µg/L1,1,1-Trichloroethane
12/29/23 01:530.5000.096<0.096µg/L1,1,2-Trichloroethane
12/29/23 01:530.5000.180<0.180µg/LTrichloroethene
12/29/23 01:530.5000.180<0.180µg/LTrichlorofluoromethane
12/29/23 01:530.5000.270<0.270µg/L1,2,3-Trichloropropane
12/29/23 01:530.5000.190<0.190µg/L1,2,4-Trimethylbenzene
12/29/23 01:530.5000.180<0.180µg/L1,3,5-Trimethylbenzene
12/29/23 01:535.001.00<1.00µg/LVinyl Acetate
12/29/23 01:530.5000.170<0.170µg/LVinyl Chloride
12/29/23 01:530.5000.210<0.210µg/Lo-Xylene
12/29/23 01:531.000.420<0.420µg/Lm,p-Xylene
12/29/23 01:5310.01.00<1.00µg/L3,3-Dimethyl-1-butanol
12/29/23 01:534-Bromofluorobenzene (S)99.8 70-130
12/29/23 01:53Dibromofluoromethane (S)94.4 70-130
12/29/23 01:531,2-Dichloroethane - d4 (S)89.4 70-130
12/29/23 01:53Toluene-d8 (S)102 70-130
Page 9 of 12Date:01/05/2024 03:22 PM
Page 54 of 59
Quality Control Data
23-354-0023Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #20
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41839QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41838
LCS-V41838 LCSD-V41838Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
40.4 10198.239.340.0µg/LAcetone 40-160 2.7 20.0
18.9 94.596.019.220.0µg/LBenzene 70-130 1.5 20.0
21.8 10910921.820.0µg/LBromobenzene 70-130 0.0 20.0
19.5 97.596.019.220.0µg/LBromochloromethane 70-130 1.5 20.0
18.4 92.091.018.220.0µg/LBromodichloromethane 70-130 1.0 20.0
20.0 10099.519.920.0µg/LBromoform 70-130 0.5 20.0
17.6 88.090.518.120.0µg/LBromomethane 60-140 2.8 20.0
22.4 11211523.020.0µg/Ln-Butylbenzene 70-130 2.6 20.0
22.4 11211523.020.0µg/Lsec-Butyl benzene 70-130 2.6 20.0
22.6 11311723.320.0µg/Ltert-Butyl benzene 70-130 3.0 20.0
20.5 10310220.420.0µg/LCarbon Tetrachloride 70-130 0.4 20.0
21.3 10710721.420.0µg/LChlorobenzene 70-130 0.4 20.0
20.9 10510520.920.0µg/LChlorodibromomethane 70-130 0.0 20.0
19.0 95.010020.020.0µg/LChloroethane 60-140 5.1 20.0
19.0 95.096.019.220.0µg/LChloroform 70-130 1.0 20.0
17.6 88.093.518.720.0µg/LChloromethane 60-140 6.0 20.0
22.2 11111322.520.0µg/L2-Chlorotoluene 70-130 1.3 20.0
21.9 11011122.220.0µg/L4-Chlorotoluene 70-130 1.3 20.0
17.1 85.586.017.220.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.5 20.0
22.7 11411021.920.0µg/L1,2-Dibromo-3-Chloropropane 70-130 3.5 20.0
20.5 10310521.020.0µg/L1,2-Dibromoethane 70-130 2.4 20.0
18.3 91.591.518.320.0µg/LDibromomethane 70-130 0.0 20.0
22.0 11011222.320.0µg/L1,2-Dichlorobenzene 70-130 1.3 20.0
22.2 11111122.120.0µg/L1,3-Dichlorobenzene 70-130 0.4 20.0
22.3 11211422.720.0µg/L1,4-Dichlorobenzene 70-130 1.7 20.0
15.2 76.078.515.720.0µg/LDichlorodifluoromethane 60-140 3.2 20.0
Page 10 of 12Date:01/05/2024 03:22 PM
Page 55 of 59
Quality Control Data
23-354-0023Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #20
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41839QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41838
LCS-V41838 LCSD-V41838Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
18.5 92.592.518.520.0µg/L1,1-Dichloroethane 70-130 0.0 20.0
17.8 89.087.017.420.0µg/L1,2-Dichloroethane 70-130 2.2 20.0
19.3 96.597.519.520.0µg/L1,1-Dichloroethene 70-130 1.0 20.0
17.8 89.089.017.820.0µg/Lcis-1,2-Dichloroethene 70-130 0.0 20.0
18.8 94.093.518.720.0µg/Ltrans-1,2-Dichloroethene 70-130 0.5 20.0
18.0 90.089.517.920.0µg/L1,2-Dichloropropane 70-130 0.5 20.0
20.2 10110020.020.0µg/L1,3-Dichloropropane 70-130 0.9 20.0
15.4 77.079.015.820.0µg/L2,2-Dichloropropane 70-130 2.5 20.0
19.9 99.510120.120.0µg/L1,1-Dichloropropene 70-130 1.0 20.0
18.0 90.088.517.720.0µg/Lcis-1,3-Dichloropropene 70-130 1.6 20.0
17.5 87.586.517.320.0µg/Ltrans-1,3-Dichloropropene 70-130 1.1 20.0
432 86.485.0425500µg/LEthanol 60-140 1.6 20.0
20.5 10310521.020.0µg/LEthylbenzene 70-130 2.4 20.0
24.1 12111422.720.0µg/LHexachlorobutadiene 70-130 5.9 20.0
20.3 10299.519.920.0µg/L2-Hexanone 60-140 1.9 20.0
22.8 11411823.520.0µg/LIsopropylbenzene 70-130 3.0 20.0
23.4 11712124.120.0µg/L4-Isopropyl toluene 70-130 2.9 20.0
18.9 94.595.519.120.0µg/LMethyl Ethyl Ketone (MEK)60-140 1.0 20.0
18.7 93.591.518.320.0µg/LMethyl tert-butyl ether (MTBE)70-130 2.1 20.0
16.2 81.082.516.520.0µg/L4-Methyl-2-Pentanone 60-140 1.8 20.0
17.0 85.085.517.120.0µg/LMethylene Chloride 70-130 0.5 20.0
21.7 10998.019.620.0µg/LNaphthalene 70-130 10.1 20.0
22.0 11011222.420.0µg/Ln-Propylbenzene 70-130 1.8 20.0
20.9 10510821.620.0µg/LStyrene 70-130 3.2 20.0
43.1 10810140.340.0µg/Ltert-Butyl Alcohol (TBA)40-140 6.7 20.0
20.0 50.052.521.040.0µg/Ltert-Butyl formate (TBF)40-140 4.8 20.0
Page 11 of 12Date:01/05/2024 03:22 PM
Page 56 of 59
Quality Control Data
23-354-0023Report No:
Project Description:
Client ID:Geological Resources, Inc.
Kingsway #20
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41839QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41838
LCS-V41838 LCSD-V41838Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
16.7 83.571.514.320.0µg/Ltert-Amyl Alcohol (TAA)40-140 15.4 20.0
40.6 10299.739.940.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 1.7 20.0
21.6 10811022.020.0µg/L1,1,1,2-Tetrachloroethane 70-130 1.8 20.0
18.7 93.593.518.720.0µg/L1,1,2,2-Tetrachloroethane 70-130 0.0 20.0
21.8 10911322.620.0µg/LTetrachloroethene 70-130 3.6 20.0
18.9 94.594.518.920.0µg/LToluene 70-130 0.0 20.0
21.7 10910220.420.0µg/L1,2,3-Trichlorobenzene 70-130 6.1 20.0
21.8 10910721.320.0µg/L1,2,4-Trichlorobenzene 70-130 2.3 20.0
19.7 98.598.019.620.0µg/L1,1,1-Trichloroethane 70-130 0.5 20.0
18.7 93.593.018.620.0µg/L1,1,2-Trichloroethane 70-130 0.5 20.0
21.8 10911022.020.0µg/LTrichloroethene 70-130 0.9 20.0
21.8 10911122.220.0µg/LTrichlorofluoromethane 60-140 1.8 20.0
20.5 10310821.520.0µg/L1,2,3-Trichloropropane 70-130 4.7 20.0
22.8 11411422.820.0µg/L1,2,4-Trimethylbenzene 70-130 0.0 20.0
23.0 11511723.420.0µg/L1,3,5-Trimethylbenzene 70-130 1.7 20.0
8.80 44.0*48.8*9.7720.0µg/LVinyl Acetate 60-140 10.4 20.0
19.6 98.010220.320.0µg/LVinyl Chloride 60-140 3.5 20.0
20.9 10510721.420.0µg/Lo-Xylene 70-130 2.3 20.0
44.0 11011244.640.0µg/Lm,p-Xylene 70-130 1.3 20.0
16.2 81.080.516.120.0µg/L3,3-Dimethyl-1-butanol 70-130 0.6 20.0
1001014-Bromofluorobenzene (S)70-130
96.295.2Dibromofluoromethane (S)70-130
91.690.01,2-Dichloroethane - d4 (S)70-130
104104Toluene-d8 (S)70-130
Page 12 of 12* QC Fail Date:01/05/2024 03:22 PM
Page 57 of 59
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-354-0023
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 3.8C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:12/20/2023 17:29:13
Special precautions or instructions included?
Comments:
Page 58 of 59
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