MO-8808_40318_CA_CAPR_20240130

CORRECTIVE ACTION
PERFORMANCE REPORT

TERRELL BAIT SHOP
7970 NC HIGHWAY 150
TERRELL, CATAWBA COUNTY, NORTH CAROLINA
FACILITY ID #00-0-00000218

Prepared For:
United Oil of the Carolinas
Post Office Box 68
Gastonia, North Carolina 28053

BLE Project Number J22-17256-07

January 30, 2024

January 30, 2024

Mr. Lewis Efird
United Oil of the Carolinas
Post Office Box 68
Gastonia, North Carolina 28053

Subject: Corrective Action Performance Report
Terrell Bait Shop, Incident 40318
7970 NC Highway 150
Terrell, Catawba County, North Carolina 28682
Facility ID #00-0-00000218
BLE Project No. J22-17256-07

Dear Mr. Efird:

Bunnell-Lammons Engineering, Inc. (BLE) has completed a Corrective Action Performance Report
(CAPR) in association with the former Terrell Bait Shop facility in Terrell, North Carolina (herein referred
to as “Site”). The purpose of the CAPR is to document the effectiveness of the soil and groundwater
remediation system in operation at the Site.

The CAPR was prepared in general accordance with the North Carolina Department of Environmental
Quality (NCDEQ) NCDEQ Underground Storage Tank (UST) Section Corrective Action Guidelines dated
January 19, 2021, and BLE Proposal No. P23-1962 dated October 18, 2023.

BLE appreciates the opportunity to assist United Oil of the Carolinas with this project. If you have any
questions regarding this report, please feel free to contact David R. Loftis at 828-277-0100.

Sincerely,

BUNNELL-LAMMONS ENGINEERING, INC.
NC FIRM REGISTRATION # C-1538

Kelsey Cahill David R. Loftis, P.E.
Environmental Scientist Senior Engineer
Licensed, North Carolina No. 028345

Corrective Action Performance Report January 30, 2024
Terrell Bait Shop, Terrell, Catawba County, North Carolina BLE Project No. J22-17256-07

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TABLE OF CONTENTS

1.0 INTRODUCTION.......................................................................................................................... 1
1.1 Site Identification ............................................................................................................................. 1
1.2 Information about Contacts Associated with the Leaking UST System .......................................... 1
1.3 Information about Release ............................................................................................................... 1
2.0 EXECUTIVE SUMMARY ........................................................................................................... 2
3.0 SITE HISTORY AND CHARACTERISTICS ............................................................................ 3
3.1 Property Information ........................................................................................................................ 3
3.2 Site History ...................................................................................................................................... 3
3.3 UST Information .............................................................................................................................. 3
3.4 Non-UST Information ...................................................................................................................... 3
3.5 Release Description ......................................................................................................................... 3
3.6 Site Characteristics........................................................................................................................... 3
3.7 Geology/Hydrogeology.................................................................................................................... 4
4.0 REMEDIATION SYSTEM OPERATION ................................................................................. 5
4.1 Equipment Operation Data .............................................................................................................. 5
4.2 Mass Removal by Soil Vapor Extraction ......................................................................................... 5
5.0 CONCLUSIONS ............................................................................................................................ 7

Appendices

Appendix A Supplementary Groundwater Report
Appendix B Figures
Appendix C Tables
Appendix D Laboratory Analytical Report

Corrective Action Performance Report January 30, 2024
Terrell Bait Shop, Terrell, Catawba County, North Carolina BLE Project No. J22-17256-07

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2.0 EXECUTIVE SUMMARY
The CAPR should be reviewed in conjunction with the Monitoring Report prepared by Mr. Richard Kelly,
P.G. with Southeastern Geological Services and received by BLE on January 7, 2024 – included in
Appendix A

The Site is located at the intersection of Sherrills Ford Road at NC Highway 150 in Terrell, Catawba
County, North Carolina and was formerly operated as a retail fueling station from 1978 until May 2014. In
2014, soil and groundwater petroleum impacts were discovered as a result of releases from a 3,000-gallon
diesel UST, 4,000-gallon gasoline UST, and a 12,000-gallon gasoline UST. The release led to significant
groundwater impacts north of the Site with free product thicknesses ranging from 3.98 feet to 4.89 feet.

An air sparge (AS) and soil vapor extraction system (SVE) utilizing three AS wells and two SVE wells is
currently being employed to remove free product and reduce the dissolved petroleum concentrations to
below Gross Contamination Levels (GCLs). The remediation system was activated on February 7, 2018
and deactivated, according to Mr. Kelly, sometime around August 2019. The system was reactivated on
March 11, 2022. The CAPR documents the operation and performance of the remediation system from
June 28, 2023 to December 31, 2023. Both the SVE system and AS system operated approximately 100%
of the available run time.

During the groundwater sampling event summarized in the Monitoring Report, groundwater samples were
collected and analyzed from 10 monitoring wells. Free product was not detected in the monitoring wells
and is considered to have been eliminated from the Site. No Gross Contamination Level (GCL) violations
were identified during the current sampling event. Several petroleum compounds, including benzene,
naphthalene, and 1,2,4-trimethylbenzene, were identified in groundwater samples collected from one or
more monitoring wells at concentrations in exceedance of the North Carolina Groundwater Quality
Standards (2L Standards).

During the operational period discussed as part of this CAPR (June 28, 2023 to December 31, 2023),
approximately 1,083 pounds of petroleum hydrocarbons (9.64 pounds as benzene) were removed from the
soil and groundwater via the SVE system. A review of the benzene mass in groundwater data indicates that
approximately 0.57 pounds of benzene have been removed from just groundwater between June 2023 to
December 2023.

A review of the historical groundwater data indicates that the groundwater remediation system is effectively
reducing the groundwater petroleum impacts. BLE recommends that the operation of the remediation
system be continued.

Corrective Action Performance Report January 30, 2024
Terrell Bait Shop, Terrell, Catawba County, North Carolina BLE Project No. J22-17256-07

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3.0 SITE HISTORY AND CHARACTERISTICS
3.1 Property Information

The Site is located at the intersection of Sherrills Ford Road at NC Highway 150 in Terrell, Catawba
County, North Carolina. The location of the Site is noted on Figures 1 and 2, in Appendix B. Figure 3,
Appendix B depicts the approximate location of the former UST system and the monitoring and
remediation wells.

The Site is a 0.28-acre parcel that is part of a 36-acre tract owned by Mr. Charles Connor.

3.2 Site History

A retail fueling station formerly operated on the subject property from 1978 until May 2014, when the UST
system components were permanently removed. A release of petroleum products leading to soil and
groundwater impacts was documented from the UST system.

3.3 UST Information

UST I.D.
Number Product Capacity
(gallons) Date Installed Date
Closed
Associated with
Suspected
Release?
1 Gasoline 4,000 8/18/78 5/7/14 No
2 Diesel 3,000 8/18/78 5/7/14 Yes
3 Gasoline 4,000 8/18/78 5/7/14 Yes
4 Gasoline 12,000 10/31/98 5/7/14 Yes

No USTs are currently located on the Site.

3.4 Non-UST Information

No above-ground storage tanks (ASTs) are located or were located at the Site.

3.5 Release Description

As noted in Section 3.2, a release was documented from a former UST system in May 2014. Petroleum-
impacted soil was documented in association with two (2) gasoline USTs (4,000 gallons and 12,000 gallons)
and one (1) 3,000-gallon diesel UST.

3.6 Site Characteristics

• Land Use of the Site: The Site is currently vacant and does not have a usage. The convenience
store structure has been demolished and only the soil and groundwater remediation system resides
on-Site.

• Land Use of Surrounding Area: The surrounding area is a mix of light commercial and residential.

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• Topography: The surface topography generally slopes to the northeast.

• Vegetation/Surface Cover: The Site’s surface includes concrete and asphalt pavement west and
south of the former convenience store structure and grass/weeds north and east of the former
convenience store structure.

• Surface Water: No surface water features were identified within 1,000 feet of the release area.

• Wells: There are six active water supply wells within 1,000 feet of the release area.

• Buildings: No buildings are currently on-Site.

• Depth to Nature of Bedrock: A soil boring has been completed to 70 feet below grade (BG) and
bedrock was not encountered.

3.7 Geology/Hydrogeology

The Site is divided between the Charlotte Belts and Kings Mountain with the upper three to seven feet of
silty clay overburden before transitioning to saprolite. Bedrock has not been encountered at the Site, but
according, to Mr. Richard Kelly, Geologist with Southern Geological Services, in the March 28, 2019
Corrective Action Performance Report (CAPR), the depth to bedrock is likely around 75 to 80 feet BG.
Mr. Kelly further noted in the CAPR that the depth to bedrock at the Terrell Shell incident, located south
of NC Highway 150, was around 85 feet BG.

The Site slopes to the northeast toward Beaverdam Creek; however, no surface water bodies are present
within 1,000 feet of the release area. The depth to groundwater at the site is approximately 40 feet BG and
is documented to generally flow to the north.

The Site is generally surrounded by properties utilized for light commercial and residential purposes.
Specifically, the adjacent property to the south-southeast is operated as a United States Postal Service office
and Terrell Camping Center, a recreational vehicles dealership.

Based on a 2018 updated receptor survey performed by Southern Geological Services, there are six active
water supply wells within 1,000 feet of the release area. Five of the active water supply well wells are
located upgradient of the Site and the remaining well is located downgradient of the Site and approximately
950 feet from the release area.

Corrective Action Performance Report January 30, 2024
Terrell Bait Shop, Terrell, Catawba County, North Carolina BLE Project No. J22-17256-07

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4.0 REMEDIATION SYSTEM OPERATION
The petroleum-impacted soil and groundwater are currently being remediated using AS and SVE. The
remediation system is comprised of three AS wells that receive compressed air from a 3 horsepower (HP)
air compressor and two SVE wells that supply influent air to a Roots-style blower driven by a 5 HP motor.
The remediation system primarily focuses on reduction in contaminant concentrations in the vicinity of
monitoring wells MW-2, MW-10 and MW-16, as this area has historically exhibited the greatest degree of
petroleum impacts. On January 3, 2018, and prior to beginning remedial actions, the free product thickness
in MW-2, MW-10, and MW-16 measured 3.98 feet, 4.89 feet, and 4.85 feet, respectively.

4.1 Equipment Operation Data

Table 1, Appendix C summarizes the operational data collected during a portion of July to December
2023. During the period, the SVE and AS systems each operated 100% consistently with generally no
down time.

4.2 Mass Removal by Soil Vapor Extraction

On September 28, 2023 and December 13, 2023, samples were collected from the emission stream from
the soil vapor extraction system and analyzed for benzene, toluene, ethylbenzene, total xylenes (BTEX),
methyl tert-butyl ether (MTBE), and total petroleum hydrocarbons (TPH) by Method 18. The results of the
emission sampling is summarized in Table 1 and the laboratory report is included in Appendix D.

Using the emission sampling data, BLE estimated the total mass of BTEX (150 pounds), MTBE (0.04
pounds), and TPH GRO (1,083 pounds) removed by the system during the operational period herein. The
results are summarized in Table 2.

4.3 Total Gallons of Water Treated

The remediation system treats an unspecified volume of petroleum-impacted groundwater within the
unconfined aquifer using AS and SVE techniques. The benzene isoconcentration data generated by
Southeastern Geological Services from May 2023 and December 2023 was utilized to estimate the
reduction in benzene from the Site’s groundwater. The analysis is summarized in Table 3, Appendix C
and indicates that the benzene mass was reduced by approximately 0.57 pounds from May 2023 to
December 2023.

The change in benzene mass was estimated using the following method and assumptions:

• The surface area between the isoconcentration contour lines prepared by Southeastern Geologic
were estimated by GIS Methods.
• The surface area for each isoconcentration interval was multiplied by the estimated depth of
contamination (assumed to be 25 feet). Assuming an estimated porosity of 0.30, the total volume
of groundwater between each isoconcentration line is calculated.
• The average compound concentration within an isoconcentration interval is calculated. For
example, if the isoconcentration interval is between the 1 microgram per liter (g/L)
isoconcentration line and the 5,000 g/L isoconcentration line the average compound concentration
for the isoconcentration interval would be 2,500 g/L.

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• The average compound concentration within an interval is multiplied by the total volume of
groundwater within the same interval, resulting in the contaminant mass within the isoconcentration
interval.
• The contamination masses within each isoconcentration interval are added together to obtain the
total contaminant mass in the unconfined aquifer.
• For this report, the total benzene mass based on the laboratory analytical results from the current
sampling event was compared to the total benzene mass based on the laboratory analytical results
from the prior sampling event to determine the change in total benzene mass.

Corrective Action Performance Report January 30, 2024
Terrell Bait Shop, Terrell, Catawba County, North Carolina BLE Project No. J22-17256-07

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5.0 CONCLUSIONS
From July 28, 2023, to December 31, 2023, the SVE and AS systems operated approximately 100% of the
available run time.

The emissions data from the SVE system indicated that approximately 1,082.56 pounds of petroleum
hydrocarbons (9.64 pounds as benzene) was removed from the soil and groundwater via the SVE system
from June 2023 to December 2023. A review of the benzene mass in groundwater data indicates that
approximately 0.57 pounds of benzene has been removed from groundwater from May 2023 to December
2023.

The most recent groundwater sampling event did not identify free product in the Site’s monitoring wells.
Additionally, no monitoring wells exhibited a GCL exceedance of petroleum compounds. A review of the
historical groundwater data indicates that the groundwater remediation system has significantly reduced the
groundwater petroleum impacts. BLE recommends that the operation of the remediation system be
continued.

Appendix A

Supplementary
Groundwater
Report

A summary follows:
MW-1: benzene at standard / TEX/MTBE < standard,
MW-2: benzene & naphthalene > standard but < GCL / TEX/MTBE < standard,
MW-4: BTEX/MTBE non detect,
MW-6: benzene & naphthalene > standard but < GCL / TEX/MTBE < standard,
MW-7: BTEX/MTBE non detect,
MW-8: BTEX/MTBE non detect,
MW-10: naphthalene > standard but < GCL / TEX < standard (B < 2.5 ppb),
MW-11: BTEX/MTBE non-detect,
MW-12: benzene and naphthalene at standard / TEX/MTBE < standard, and
MW-16: benzene and naphthalene > standard but < GCL / TEX/MTBE < standard.
A comparison with the last sampling event follows.
MW-1: minor changes: benzene increase / xylenes and MTBE decrease,
MW-2: BTEX/MTBE decrease,
MW-4: remain non-detect,
MW-6: BTEX/MTBE minor increases,
MW-7: BTEX/MTBE remain non-detect,
MW-8: BTEX/MTBE remain non-detect,
MW-10: minor changes: toluene and ethylbenzene decrease and xylenes increase,
MW-11: BTEX/MTBE remain non-detect,
MW-12: insignificant changes: BTEX increase and MTBE decrease,
MW-16: BTEX/MTBE significant decreases..
1.3 Sampling Protocol
The monitor wells were sampled with new, disposable bailers after purging three well casing
volumes. The samples were placed in laboratory provided vials, fixed with a chain of custody,
and placed on ice for immediate delivery to PACE Analytical.
B. FREE PRODUCT
Free product was initially present in MWs 2, 10, and 16. The product has been removed, none
has been present since December 2018.
C. SOIL REMEDIATION – not applicable
D. GROUNDWATER REMEDIATION
The AS/SVE system was activated on March 11, 2022. It is maintained by Bunnell Lammons
Engineering (BLE). Mr. David Loftis of BLE prepared the Corrective Action Performance
Report for this period
E. CONCUSIONS
The plume has been restricted to a narrow band that follows the MWs 2-10-16-12 line; the
contaminant levels have been greatly reduced in the plume. Since activating the system,
contaminant concentrations in this band have had significant decreases noted in single sampling
events. MW-10 had a large decrease from the 12-21 event to the 6-22 event. MWs 2 and 12 had
large decreases from the 6-22 event to the 11-22 event. These large decreases have held. This
sampling event showed a similar such drop in the MW-16 concentrations.
The following show an overall positive trend: (1) consistent low contaminant levels in MW-1
after initial high levels, (2) free product has been eliminated, (3) sharp contaminant decreases in
MWs 2, 10, 12, and 16, (4) steady decrease in contaminant levels to non detect in MW-7, a step
out well to the north-northwest, and (5) decrease in contaminant levels in MW-6, thus narrowing
the plume.
F. FIGURES
USGS Topographic Map
Site Map
Groundwater Flow Map
Benzene Iso-Concentration Map
Toluene Iso-Concentration Map
Ethylbenzene Iso-Concentration Map
Xylenes Iso-Concentration Map
MTBE Iso-Concentration Map
G. TABLES
Table B-4 Summary of Groundwater Sampling Results
Table 1 Historical Groundwater Sampling
Table B-7 Well Construction Information
H. APPENDICES
Contaminant Level Graphs: MWs 1, 2, 6, 10, 12, and 16 / linear & logarithmic scales
Laboratory Analysis/Chain of Custody
Table B-4: Summary of Groundwater and Surface Water Sampling Results
Revision Date: 12-27-18 Incident Number and Name: Terrell Bait Shop Facility ID#:
Analytical Method (e.g., VOC by SM6000B) or
Field Measurement (FM)6200B 6200B 6200B` 6200B 6200B 6200B 6200B 6200B 6200B 504.1
Contaminant of Concern/ Field
Measurement
Benzene
Toluene
Ethylbenzene
Xylenes
MTBE
IPE
Naphthalene
1,2
DCE
EDB
EDB
Well or
SW ID
Date
Collected
Sample
ID
Incident
Phase
MW-1 12-14-23 MW-1 Monitor 1 <1 <1 2 4 1 <2 <1 <1
MW-2 “ MW-2 “3 18 4 63 4 13 12 <1 <1
MW-4 “ MW-4 “ <1 <1 <1 <2 <1 <1 <2 <1 <1
MW-6 “ MW-6 “26 18 13 89 9 4 26 <1 <1
MW-7 “ MW-7 “ <1 <1 <1 <2 <1 <1 <2 <1 <1
Minimum Reporting Limit (ug/l)
2L Standard (ug/l)1 600 600 500 20 70 6 0.4 0.02 0.02
GCL (ug/l)5000 260000 84500 85500 20000 70000 6000 400 50 50
NC 2B Standard or EPA National Criteria
(ug/l)
Results must be reported in ug/l ug/l =micrograms per liter GCL = gross contamination level Rounded to Whole Numbers
NOT SAMPLED: MWs 3, 5, 9, 13, 14, 15, VMW-1 & VMW-2
Table B-4: Summary of Groundwater and Surface Water Sampling Results
Revision Date: 12-27-18 Incident Number and Name: Terrell Bait Shop Facility ID#:
Analytical Method (e.g., VOC by SM6000B) or
Field Measurement (FM)6200B 6200B 6200B 6200B` 6200B` 6200B 6200B 6200B 6200B
Contaminant of Concern/ Field Measurement
n-Butlybenzene
Sec-
Butylbenzene
Tert-
Butylbenzene
Isopropyl
benzene
n-Propylbenzene
Styrene
1,2,4
Trimethyl
benzene
1,3,5
Trimethyl
benzene
TCE
Well or
SW ID
Date
Collected
Sample
ID
Incident
Phase
MW-1 12-14-23 MW-1 Monitor <1 <1 <1 <1 <1 <1 3 <1 <1
MW-2 “ MW-2 “ <1 <1 <1 <1 1 <1 45 15 <1
MW-4 “ MW-4 “ <1 <1 <1 <1 <1 <1 <1 <1 <1
MW-6 “ MW-6 <1 <1 <1 4 3 <1 32 8 <1
MW-7 MW-7 <1 <1 <1 <1 <1 <1 <1 <1 <1
Minimum Reporting Limit (ug/l)
2L Standard (ug/l)70 70 70 70 70 70 400 400 15
GCL (ug/l)6900 8500 15000 25000 30000 70000 28500 25000 15000
NC 2B Standard or EPA National Criteria
(ug/l)
Results must be reported in ug/l ug/l =micrograms per liter GCL = gross contamination level Rounded to Whole Numbers
Table B-4: Summary of Groundwater and Surface Water Sampling Results
Revision Date: 12-27-18 Incident Number and Name: Terrell Bait Shop Facility ID#:
Analytical Method (e.g., VOC by SM6000B) or
Field Measurement (FM)6200B 6200B 6200B` 6200B 6200B 6200B 6200B 6200B 6200B 504.1
Contaminant of Concern/ Field
Measurement
Benzene
Toluene
Ethylbenzene
Xylenes
MTBE
IPE
Naphthalene
1,2
DCE
EDB
EDB
Well or
SW ID
Date
Collected
Sample
ID
Incident
Phase
MW-8 12-14-23 MW-8 Monitor <1 <1 <1 <2 <1 <1 <2 <1 <1
MW-10 “ MW-10 “ <2.5 4 3 179 <2.5 <2.5 70 <2.5 <2.5
MW-11 “ MW-11 “ <1 <1 <1 <2 <1 <1 <2 <1 <1
MW-12 “ MW-12 “1 4 1 12 <1 <1 6 <1 <1
MW-16 “ MW-16 “2 10 4 33 <1 <1 18 <1 <1
Minimum Reporting Limit (ug/l)
2L Standard (ug/l)1 600 600 500 20 70 6 0.4 0.02 0.02
GCL (ug/l)5000 260000 84500 85500 20000 70000 6000 400 50 50
NC 2B Standard or EPA National Criteria
(ug/l)
Results must be reported in ug/l ug/l =micrograms per liter GCL = gross contamination level Rounded to Whole Numbers
NOT SAMPLED: MWs 3, 5, 9, 13, 14, 15, VMW-1 & VMW-24
Table B-4: Summary of Groundwater and Surface Water Sampling Results
Revision Date: 12-27-18 Incident Number and Name: Terrell Bait Shop Facility ID#:
Analytical Method (e.g., VOC by SM6000B) or
Field Measurement (FM)6200B 6200B 6200B 6200B` 6200B` 6200B 6200B 6200B 6200B
Contaminant of Concern/ Field Measurement
n-Butlybenzene
Sec-
Butylbenzene
Tert-
Butylbenzene
Isopropyl
benzene
n-Propylbenzene
Styrene
1,2,4
Trimethyl
benzene
1,3,5
Trimethyl
benzene
TCE
Well or
SW ID
Date
Collected
Sample
ID
Incident
Phase
MW-8 12-14-23 MW-8 Monitor <1 <1 <1 <1 <1 <1 <1 <1 <1
MW-10 “ MW-10 “ <1 <1 <1 10 41 <1 437 134 <1
MW-11 “ MW-11 “ <1 <1 <1 <1 <1 <1 <1 <1 <1
MW-12 “ MW-12 <1 <1 <1 <1 1 <1 12 3 <1
MW-16 MW-16 <1 <1 <1 <1 3 <1 36 9 <1
Minimum Reporting Limit (ug/l)
2L Standard (ug/l)70 70 70 70 70 70 400 400 15
GCL (ug/l)6900 8500 15000 25000 30000 70000 28500 25000 15000
NC 2B Standard or EPA National Criteria
(ug/l)
Results must be reported in ug/l ug/l =micrograms per liter GCL = gross contamination
TABLE 1: HISTORICAL GROUNDWATER SAMPLING
Benzene Toluene Ethtlb.Xylenes MTBE
Standard 1 600 600 500 20
GCL 5000 260000 84500 85500 20000
MW-1 10/16/2014 2820 21900 2830 15100 1230
10/17/2017 1120 8460 868 5520 387
5/31/2018 124 147 196 889 244
12/10/2018 7 10 1 133 112
6/12/2019 <1 <1 <1 <2 <1
12/16/2019 9 90 29 193 23
6/16/2020 <1 10 11 406 21
12/21/2020 <3 31 34 837 60
7/4/2021 1 5 <1 445 45
12/7/2021 8 9 5 28 2
6/3/2022 1 23 63 1269 42
11/14/2022 <1 2 <1 281 9
5/31/2023 <1 <1 <1 10 8
12/14/2023 1 <1 <1 2 4
MW-2 10/16/2014 FP
10/17/2017 FP
5/31/2018 FP
12/10/2018 no product
6/12/2019 no product
12/16/2019 10800 23500 2430 12850 1080
6/16/2020 8930 27400 3240 19020 762
12/21/2020 5780 18900 1630 9090 376
7/4/2021 7010 21700 2200 11080 98
12/7/2021 3370 12100 1420 8160 <62
6/3/2022 16500 15800 1670 9960 291
11/14/2022 57 672 240 1798 73
5/31/2023 6 38 14 172 13
12/14/2023 3 18 4 63 4
Benzene Toluene Ethtlb.Xylenes MTBE
Standard 1 600 600 500 20
GCL 5000 260000 84500 85500 20000
MW-3 10/16/2014 <1 <1 <1 <2 <1
10/17/2017 <1 <1 <1 <2 <1
5/31/2018 <1 <1 <1 <2 <1
12/10/2018 <1 <1 <1 <2 <1
6/12/2019 <1 <1 <1 <2 <1
12/16/2019 <1 <1 <1 <2 <1
6/16/2020 <1 <1 <1 <2 <1
12/21/2020 <1 <1 <1 <2 <1
12/7/2021 <1 <1 <1 <2 <1
6/3/2022 <1 <1 <1 <2 <1
11/14/2022 <1 <1 <1 <2 <1
5/31/2023 <1 <1 <1 <2 <1
12/14/2023 discontinue sampling
MW-4 10/16/2014 <1 <1 <1 <2 <1
10/17/2017 <1 <1 <1 <2 <1
5/31/2018 <1 <1 <1 <2 <1
12/10/2018 <1 <1 <1 <2 <1
6/12/2019 <1 <1 <1 <2 <1
12/16/2019 <1 <1 <1 <2 <1
6/16/2020 <1 <1 <1 <2 <1
12/21/2020 <1 <1 <1 <2 <1
7/4/2021 <1 <1 <1 <2 <1
12/7/2021 <1 <1 <1 <2 <1
6/3/2022 <1 <1 <1 <2 <1
11/14/2022 <1 <1 <1 <2 <1
5/31/2023 <1 <1 <1 <2 <1
12/14/2023 <1 <1 `<1 <2 <1
MW-5 10/16/2014 <1 <1 <1 <2 <1
10/17/2017 <1 <1 <1 <2 <1
5/31/2018 <1 <1 <1 <2 <1
12/10/2018 <1 <1 <1 <2 <1
6/12/2019 <1 <1 <1 <2 <1
12/16/2019 <1 <1 <1 <2 <1
6/16/2020 <1 <1 <1 <2 <1
12/21/2020 <1 <1 <1 <2 <1
7/4/2021 <1 <1 <1 <2 <1
12/7/2021 <1 <1 <1 <2 <1
6/3/2022 <1 <1 <1 <2 <1
11/14/2022 <1 <1 <1 <2 <1
5/31/2023 <1 <1 <1 <2 <1
12/14/2023 discontinue sampling
Benzene Toluene Ethtlb.Xylenes MTBE
Standard 1 600 600 500 20
GCL 5000 260000 84500 85500 20000
MW-6 4/9/2015 236 376 35 160 839
10/17/2017 4560 9420 363 4000 877
5/31/2018 6710 12500 753 4570 1290
12/10/2018 1770 1910 166 1093 831
6/12/2019 1600 2990 322 1661 683
12/16/2019 3660 6000 503 2670 761
6/16/2020 1500 4670 581 2750 298
12/21/2020 1620 5060 601 2780 246
7/4/2021 4070 14700 1530 8600 602
12/7/2021 1830 9360 1080 6400 359
6/3/2022 <1 <1 <1 <2 <1
11/14/2022 127 254 31 252 123
5/31/2023 4 10 2 14 8
12/14/2023 26 18 13 89 9
MW-7 4/9/2017 18 18 <1 <2 256
10/17/2017 86 104 12 57 173
5/31/2018 <2 517 56 172 227
12/10/2018 206 558 44 230 158
6/12/2019 275 342 32 173 336
12/16/2019 <1 <1 <1 <2 15
6/16/2020 <1 <1 <1 <2 <1
12/21/2020 <1 <1 <1 <2 <1
7/4/2021 <1 <1 <1 <2 <1
12/7/2021 <1 1 <1 <2 <1
6/3/2022 <1 <1 <1 <2 <1
11/14/2022 <1 <1 <1 <2 <1
5/31/2023 <1 <1 <1 <2 <1
12/14/2023 <1 <1 <1 <2 <1
Benzene Toluene Ethtlb.Xylenes MTBE
Standard 1 600 600 500 20
GCL 5000 260000 84500 85500 20000
MW-8 4/9/2017 <1 <1 <1 <2 87
10/17/2017 <1 <1 <1 <2 24
5/31/2018 <1 <1 <1 <2 <1
12/10/2018 <1 <1 <1 <2 <1
6/12/2019 <1 <1 <1 <2 <1
12/16/2019 <1 <1 <1 <2 <1
6/16/2020 <1 <1 <1 <2 <1
12/21/2020 <1 <1 <1 <2 <1
7/4/2021 <1 <1 <1 <2 <1
12/7/2021 <1 <1 <1 <2 <1
6/3/2022 <1 <1 <1 <2 <1
11/14/2022 <1 <1 <1 <2 <1
5/31/2023 <1 <1 <1 <2 <1
12/14/2023 <1 <1 <1 <2 <1
MW-9 7/30/2015 2 10 4 11 <1
10/17/2017 <1 <1 <1 <2 60
5/31/2018 <1 <1 <1 <2 <1
12/10/2018 <1 <1 <1 <2 <1
6/12/2019 <1 <1 <1 <2 <1
12/16/2019 <1 <1 <1 <2 <1
6/16/2020 <1 <1 <1 <2 <1
12/21/2020 <1 <1 <1 <2 <1
7/4/2021 <1 <1 <1 <2 <1
12/7/2021 <1 <1 <1 <2 <1
6/3/2022 <1 <1 <1 <2 <1
11/14/2022 <1 <1 <1 <2 <1
5/31/2023 <1 <1 <1 <2 <1
12/14/2023 discontinue sampling
MW-10 10/17/2017 FP
5/31/2018 FP
12/10/2018 FP
6/12/2019 no product
12/16/2019 15600 49600 4150 19280 464
6/16/2020 10500 73900 19900 108100 743
12/21/2020 5490 23100 3240 17580 435
7/4/2021 8180 31000 4460 25110 203
12/7/2021 13800 78100 22300 138700 <1000
6/3/2022 233 983 145 1115 73
11/14/2022 27 599 364 2177 <5
5/31/2023 1 9 11 128 <1
12/14/2023 <2.5 4 3 179 <1
Benzene Toluene Ethtlb.Xylenes MTBE
Standard 1 600 600 500 20
GCL 5000 260000 84500 85500 20000
MW-11 7/30/2017 <1 1 <1 <2 143
10/17/2017 35 30 <1 3 <1
5/31/2018 1 2 <1 <2 <1
12/10/2018 23 8 <1 2 <1
6/12/2019 <1 <1 <1 <2 <1
12/16/2019 <1 <1 <1 <2 <1
6/16/2020 <1 <1 <1 <2 <1
12/21/2020 <1 <1 <1 <2 <1
7/4/2021 <1 <1 <1 <2 <1
12/7/2021 <1 1 <1 <2 <1
6/3/2022 <1 <1 <1 <2 <1
11/14/2022 <1 <1 <1 <2 <1
5/31/2023 <1 <1 <1 <2 <1
12/14/2023 <1 <1 <1 <2 ,1
MW-12 7/30/2017 118 258 24 92 8
10/17/2017 10600 27000 1720 9710 235
5/31/2018 2740 6310 253 2360 435
12/10/2018 964 3260 134 1656 245
6/12/2019 3280 9690 522 3890 264
12/16/2019 5800 24900 1800 12230 400
6/16/2020 5680 18500 1400 8120 412
12/21/2020 5090 18800 1420 7970 419
7/4/2021 6900 29100 2290 12520 422
12/7/2021 9090 32500 2410 13530 507
6/3/2022 2450 6380 415 3150 248
11/14/2022 4 9 <1 8 14
5/31/2023 <1 <1 <1 <2 1
12/14/2023 1 4 1 12 <1
Benzene Toluene Ethtlb.Xylenes MTBE
Standard 1 600 600 500 20
GCL 5000 260000 84500 85500 20000
MW-13 10/26/2015 <1 <1 <1 <2 <1
10/17/2017 <1 <1 <1 <2 <1
5/31/2018 <1 <1 <1 <2 <1
12/10/2018 <1 <1 <1 <2 <1
6/12/2019 discontinue sampling
10/26/2015 <1 <1 <1 <2 <1
10/17/2017 <1 <1 <1 <2 <1
MW-14 12/10/2018 <1 <1 <1 <2 <1
12/10/2018 <1 <1 <1 <2 <1
6/12/2019 discontinue sampling
MW-15 10/26/2015 <1 <1 <1 <2 <1
10/17/2017 <1 <1 <1 <2 <1
5/31/2018 <1 <1 <1 <2 <1
12/10/2018 <1 <1 <1 <2 <1
6/12/2019 <1 <1 <1 <2 <1
12/16/2019 <1 <1 <1 <2 <1
6/16/2020 <1 <1 <1 <2 <1
12/21/2020 <1 <1 <1 <2 <1
7/4/2021 <1 <1 <1 <2 <1
12/7/2021 <1 <1 <1 <2 <1
6/3/2022 <1 <1 <1 <2 <1
11/14/2022 <1 <1 <1 <2 <1
5/31/2023 <1 <1 <1 <2 <1
12/14/2023 discontinue sampling
MW-16 10/26/2017 FP
10/17/2017 FP
5/31/2018 FP
12/10/2018 FP
6/12/2019 no product
12/16/2019 9530 29600 3410 17610 308
6/16/2020 7940 28300 2820 14350 <125
12/21/2020 8780 25800 1720 8920 <100
7/4/2021 12800 37600 3300 16730 103
12/7/2021 15900 64800 9460 53500 <500
6/3/2022 3350 19100 2570 14750 165
11/14/2022 1210 16200 7320 43200 <500
5/31/2023 1640 8240 1650 8940 <25
12/14/2023 2 10 4 33 <1
Benzene Toluene Ethtlb.Xylenes MTBE
1 600 600 500 20
5000 260000 84500 85500 20000
Standard
GCL 10/26/2015 <1 <1 <1 <2 <1
10/17/2017 <1 <1 <1 <2 <1
VMW-1 5/31/2018 <1 <1 <1 <2 <1
12/10/2018 <1 <1 <1 <2 <1
6/12/2019 <1 <1 <1 <2 <1
12/16/2019 <1 <1 <1 <2 <1
6/16/2020 <1 <1 <1 <2 <1
12/21/2020 <1 <1 <1 <2 <1
7/4/2021 <1 <1 <1 <2 <1
12/7/2021 <1 <1 <1 <2 <1
6/3/2022 <1 <1 <1 <2 <1
11/14/2022 <1 <1 <1 <2 <1
5/31/2023 <1 <1 <1 <2 <1
12/14/2023 discontinue sampling
VMW-2 6/16/2020 <1 <1 <1 <2 <1
12/21/2020 <1 <1 <1 <2 <1
7/4/2021 <1 <1 <1 <2 <1
12/7/2021 <1 <1 <1 <2 <1
6/3/2022 <1 <1 <1 <2 <1
11/14/2022 <1 <1 <1 <2 <1
5/31/2023 <1 <1 <1 <2 <1
12/14/2023 discontinue sampling
Table B-7: Monitoring and Remediation Well Construction Information
Revision Date: 12-10-18 Incident Number and Name: Terrell Bait Shop Facility ID#:
Well
ID
Date
Installed
(m/dd/yy)
Date
Water
Level
Measured
(m/dd/yy)
Well
Casing
Diameter
(in.)
Well
Casing
Depth
(ft.
BGS)
Screened
Interval
(x to y
ft. BGS)
Depth
of Well
(ft.
BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water
from Top
of Casing
(ft.)
Free
Product
Thickness
**(ft.)
Groundwater
Elevation*
(ft.)
Latitude/
Longitude
(decimal
degrees)***
1 10-14-14 12-13-23 2 34 34-49 49 100.97 40.51 0 60.46 35.589343
80.977701
2 10-14-14 “ 2 34 34-49 49 100.50 40.52 0 59.98 35.589422
80.977766
3 10-18-14 “ 2 34 34-49 49 100.00 35.589486
80.977894
4 10-27-14 “ 2 34 34-49 49 98.31 38.58 0 59.73 35.589525
80.977496
5 10-27-14 “ 2 33 33-48 49 95.61 35.589692
80.777452
6 4-5-15 “ 2 34 34-49 49 99.19 39.27 0 59.92 35.589490
80.977791
7 4-5-15 “ 2 34 34-49 49 98.84 39.14 0 59.70 35.589557
80.977819
8 4-6-15 “ 2 34 34-49 49 98.29 38.91 0 59.38 35.589598
80.977821
9 7-29-15 “ 2 34 34-49 49 99.04 35.589551
80.977856
10 7-15-15 “ 2 34 34-49 49 98.89 38.95 0 59.94 35.589502
80.977659
11 7-29-15 “ 2 34 34-49 49 98.28 39.03 0 59.25 35.589594
80.977753
12 7-15-15 “ 2 34 34-49 49 98.04 38.64 0 59.40 35.589569
80.977621
Ft BGS = feet below ground surface
* Reference Point for Elevation MeasurementsMW-3 , Assumed Elevation: 100.00 ft.
** If free product is present in a well, groundwater elevation is calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.8581]
***The location must be sufficiently accurate and precise to allow easy recovery of lost or damaged wells.
Table B-7: Monitoring and Remediation Well Construction Information
Revision Date: 12-10-18 Incident Number and Name: Terrell Bait Shop Facility ID#: 021875
Well ID
Date
Installed
(m/dd/yy)
Date
Water
Level
Measured
(m/dd/yy)
Well
Casing
Diameter
(in.)
Well
Casing
Depth
(ft.
BGS)
Screened
Interval
(x to y
ft. BGS)
Depth
of Well
(ft.
BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water
from Top
of Casing
(ft.)
Free
Product
Thickness
**(ft.)
Groundwater
Elevation*
(ft.)
Latitude/
Longitude
(decimal
degrees)***
MW-13 10-24-15 12-13-23 2 34 68-70 70 98.78 38.59 35.589343
80.977702
MW-14 10-24-15 “ 2 34 34-49 49 98.11 37.70 35.589250
80.977579
MW-15 10-25-15 “ 2 32 32-47 47 96.30 36.26 30.589344
80.977339
MW-16 10-25-15 “ 2 34 34-49 49 98.60 38.90 0 59.70 35.589557
80.977584
VMW-1 4-25-15 “ 2 68 68-70 70 100.93 35.89343
80.977702
VMW-2 6-14-20 2 75 73-75 75 35.589422
80.977766
TS-8 2 35.589250
80.977579
TS-11 35.589344
80.977339
Ft BGS = feet below ground surface
* Reference Point for Elevation MeasurementsMW-3 , Assumed Elevation: 100.00 ft.
** If free product is present in a well, groundwater elevation is calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.8581]
***The location must be sufficiently accurate and precise to allow easy recovery of lost or damaged wells.
0
5000
10000
15000
20000
25000
10
/
1
6
/
2
0
1
4
10
/
1
7
/
2
0
1
7
5/
3
1
/
2
0
1
8
12
/
1
0
/
2
0
1
8
6/
1
2
/
2
0
1
9
12
/
1
6
/
2
0
1
9
6/
1
6
/
2
0
2
0
12
/
2
1
/
2
0
2
0
7/
4
/
2
0
2
1
12
/
7
/
2
0
2
1
6/
3
/
2
0
2
2
11
/
1
4
/
2
0
2
2
5/
3
1
/
2
0
2
3
12
/
1
3
/
2
0
2
3
MW-1
MW-1
B T E X MTBE
1
10
100
1000
10000
100000
10
/
1
6
/
2
0
1
4
10
/
1
7
/
2
0
1
7
5/
3
1
/
2
0
1
8
12
/
1
0
/
2
0
1
8
6/
1
2
/
2
0
1
9
12
/
1
6
/
2
0
1
9
6/
1
6
/
2
0
2
0
12
/
2
1
/
2
0
2
0
7/
4
/
2
0
2
1
12
/
7
/
2
0
2
1
6/
3
/
2
0
2
2
11
/
1
4
/
2
0
2
2
5/
3
1
/
2
0
2
3
12
/
1
3
/
2
0
2
3
MW-1
MW-1
B T E X MTBE
0
5000
10000
15000
20000
25000
30000
10
/
2
9
/
2
0
1
7
10
/
1
7
/
2
0
1
7
5/
3
1
/
2
0
1
8
12
/
1
0
/
2
0
1
8
6/
1
2
/
2
0
1
9
12
/
1
6
/
2
0
1
9
6/
1
6
/
2
0
2
0
12
/
2
1
/
2
0
2
0
7/
4
/
2
0
2
1
12
/
7
/
2
0
2
1
6/
3
/
2
0
2
2
11
/
1
4
/
2
0
2
2
5/
3
1
/
2
0
2
3
12
/
1
3
/
2
0
2
3
MW-2
MW-2
B T E X MTBE
1
10
100
1000
10000
100000
10
/
2
9
/
2
0
1
7
10
/
1
7
/
2
0
1
7
5/
3
1
/
2
0
1
8
12
/
1
0
/
2
0
1
8
6/
1
2
/
2
0
1
9
12
/
1
6
/
2
0
1
9
6/
1
6
/
2
0
2
0
12
/
2
1
/
2
0
2
0
7/
4
/
2
0
2
1
12
/
7
/
2
0
2
1
6/
3
/
2
0
2
2
11
/
1
4
/
2
0
2
2
5/
3
1
/
2
0
2
3
12
/
1
3
/
2
0
2
3
MW-2
MW-2
B T E X MTBE
0
2000
4000
6000
8000
10000
12000
14000
16000
4/
9
/
2
0
1
5
10
/
1
7
/
2
0
1
7
5/
3
1
/
2
0
1
8
12
/
1
0
/
2
0
1
8
6/
1
2
/
2
0
1
9
12
/
1
6
/
2
0
1
9
6/
1
6
/
2
0
2
0
12
/
2
1
/
2
0
2
0
7/
4
/
2
0
2
1
12
/
7
/
2
0
2
1
6/
3
/
2
0
2
2
11
/
1
4
/
2
0
2
2
5/
3
1
/
2
0
2
3
12
/
1
3
/
2
0
2
3
MW-6
MW-6
B T E X MTBE
1
10
100
1000
10000
100000
4/
9
/
2
0
1
5
10
/
1
7
/
2
0
1
7
5/
3
1
/
2
0
1
8
12
/
1
0
/
2
0
1
8
6/
1
2
/
2
0
1
9
12
/
1
6
/
2
0
1
9
6/
1
6
/
2
0
2
0
12
/
2
1
/
2
0
2
0
7/
4
/
2
0
2
1
12
/
7
/
2
0
2
1
6/
3
/
2
0
2
2
11
/
1
4
/
2
0
2
2
5/
3
1
/
2
0
2
3
12
/
1
3
/
2
0
2
3
MW-6
MW-6
B T E X MTBE
0
100
200
300
400
500
600
4/
9
/
2
0
1
7
10
/
1
7
/
2
0
1
7
5/
3
1
/
2
0
1
8
12
/
1
0
/
2
0
1
8
6/
1
2
/
2
0
1
9
12
/
1
6
/
2
0
1
9
6/
1
6
/
2
0
2
0
12
/
2
1
/
2
0
2
0
7/
4
/
2
0
2
1
12
/
7
/
2
0
2
1
6/
3
/
2
0
2
2
11
/
1
4
/
2
0
2
2
5/
3
1
/
2
0
2
3
12
/
1
3
/
2
0
2
3
MW-7
MW-7
B T E X MTBE
1
10
100
1000
4/
9
/
2
0
1
7
10
/
1
7
/
2
0
1
7
5/
3
1
/
2
0
1
8
12
/
1
0
/
2
0
1
8
6/
1
2
/
2
0
1
9
12
/
1
6
/
2
0
1
9
6/
1
6
/
2
0
2
0
12
/
2
1
/
2
0
2
0
7/
4
/
2
0
2
1
12
/
7
/
2
0
2
1
6/
3
/
2
0
2
2
11
/
1
4
/
2
0
2
2
5/
3
1
/
2
0
2
3
12
/
1
3
/
2
0
2
3
MW-7
MW-7
B T E X MTBE
0
20000
40000
60000
80000
100000
120000
140000
160000
7/
3
0
/
2
0
1
7
10
/
1
7
/
2
0
1
7
5/
3
1
/
2
0
1
8
12
/
1
6
/
2
0
2
0
6/
1
6
/
2
0
2
0
12
/
2
1
/
2
0
2
0
7/
4
/
2
0
2
1
12
/
7
/
2
0
2
1
6/
3
/
2
0
2
2
11
/
1
4
/
2
0
2
2
5/
3
1
/
2
0
2
3
12
/
1
3
/
2
0
2
3
MW-10
MW-10
B T E X MTBE
1
10
100
1000
10000
100000
1000000
7/
3
0
/
2
0
1
7
10
/
1
7
/
2
0
1
7
5/
3
1
/
2
0
1
8
12
/
1
6
/
2
0
2
0
6/
1
6
/
2
0
2
0
12
/
2
1
/
2
0
2
0
7/
4
/
2
0
2
1
12
/
7
/
2
0
2
1
6/
3
/
2
0
2
2
11
/
1
4
/
2
0
2
2
5/
3
1
/
2
0
2
3
12
/
1
3
/
2
0
2
3
MW-10
MW-10
B T E X MTBE
0
20
40
60
80
100
120
140
160
7/
3
0
/
2
0
1
7
10
/
1
7
/
2
0
1
7
5/
3
1
/
2
0
1
8
12
/
1
0
/
2
0
1
8
6/
1
2
/
2
0
1
9
12
/
1
6
/
2
0
1
9
6/
1
6
/
2
0
2
0
12
/
7
/
2
0
2
1
6/
3
/
2
0
2
2
11
/
1
4
/
2
0
2
2
5/
3
1
/
2
0
2
2
12
/
1
3
/
2
0
2
3
MW-11
MW-11
B T E X MTBE
1
10
100
1000
7/
3
0
/
2
0
1
7
10
/
1
7
/
2
0
1
7
5/
3
1
/
2
0
1
8
12
/
1
0
/
2
0
1
8
6/
1
2
/
2
0
1
9
12
/
1
6
/
2
0
1
9
6/
1
6
/
2
0
2
0
12
/
7
/
2
0
2
1
6/
3
/
2
0
2
2
11
/
1
4
/
2
0
2
2
5/
3
1
/
2
0
2
2
12
/
1
3
/
2
0
2
3
MW-11
MW-11
B T E X MTBE
0
5000
10000
15000
20000
25000
30000
35000
7/
3
0
/
2
0
1
7
10
/
1
7
/
2
0
1
7
5/
3
1
/
2
0
1
8
12
/
1
0
/
2
0
1
8
6/
1
2
/
2
0
1
9
12
/
1
6
/
2
0
1
9
6/
1
6
/
2
0
2
0
12
/
2
1
/
2
0
2
0
7/
4
/
2
0
2
1
12
/
7
/
2
0
2
1
6/
3
/
2
0
2
2
11
/
1
4
/
2
0
2
2
5/
3
1
/
2
0
2
3
12
/
1
3
/
2
0
2
3
MW-12
MW-12
B T E X MTBE
1
10
100
1000
10000
100000
7/
3
0
/
2
0
1
7
10
/
1
7
/
2
0
1
7
5/
3
1
/
2
0
1
8
12
/
1
0
/
2
0
1
8
6/
1
2
/
2
0
1
9
12
/
1
6
/
2
0
1
9
6/
1
6
/
2
0
2
0
12
/
2
1
/
2
0
2
0
7/
4
/
2
0
2
1
12
/
7
/
2
0
2
1
6/
3
/
2
0
2
2
11
/
1
4
/
2
0
2
2
5/
3
1
/
2
0
2
3
12
/
1
3
/
2
0
2
3
MW-12
MW-12
B T E X MTBE
0
10000
20000
30000
40000
50000
60000
70000
10
/
2
6
/
2
0
1
7
10
/
1
7
/
2
0
1
7
5/
3
1
/
2
0
1
8
12
/
1
6
/
2
0
2
0
6/
1
6
/
2
0
2
0
12
/
2
1
/
2
0
2
0
7/
4
/
2
0
2
1
12
/
7
/
2
0
2
1
6/
3
/
2
0
2
2
11
/
1
4
/
2
0
2
2
5/
3
1
/
2
0
2
3
12
/
1
3
/
2
0
2
3
MW-16
MW-16
B T E X MTBE
1
10
100
1000
10000
100000
10
/
2
6
/
2
0
1
7
10
/
1
7
/
2
0
1
7
5/
3
1
/
2
0
1
8
12
/
1
6
/
2
0
2
0
6/
1
6
/
2
0
2
0
12
/
2
1
/
2
0
2
0
7/
4
/
2
0
2
1
12
/
7
/
2
0
2
1
6/
3
/
2
0
2
2
11
/
1
4
/
2
0
2
2
5/
3
1
/
2
0
2
3
12
/
1
3
/
2
0
2
3
MW-16
MW-16
B T E X MTBE
#=CL#
December 22, 2023
LIMS USE: FR - RICHARD KELLY
LIMS OBJECT ID: 92703972
92703972
Project:
Pace Project No.:
RE:
Mr. Richard Kelly
SE Geologic
301 Windsor Dr.
Shelby, NC 28150
TERRELL BAIT SHOP
Dear Mr. Kelly:
Enclosed are the analytical results for sample(s) received by the laboratory on December 14, 2023. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
704-977-0942
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 37
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 37
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92703972001 MW-1 SM 6200B 63 PASI-CSAS
92703972002 MW-2 SM 6200B 63 PASI-CSAS
92703972003 MW-4 SM 6200B 63 PASI-CSAS
92703972004 MW-6 SM 6200B 63 PASI-CSAS
92703972005 MW-7 SM 6200B 63 PASI-CSAS
92703972006 MW-8 SM 6200B 63 PASI-CSAS
92703972007 MW-10 SM 6200B 63 PASI-CSAS
92703972008 MW-11 SM 6200B 63 PASI-CSAS
92703972009 MW-12 SM 6200B 63 PASI-CSAS
92703972010 MW-16 SM 6200B 63 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Sample:MW-1 Lab ID:92703972001 Collected:12/14/23 11:45 Received:12/14/23 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 1.2 ug/L 12/19/23 01:18 71-43-20.50 1
Bromobenzene ND ug/L 12/19/23 01:18 108-86-10.50 1
Bromochloromethane ND ug/L 12/19/23 01:18 74-97-50.50 1
Bromodichloromethane ND ug/L 12/19/23 01:18 75-27-40.50 1
Bromoform ND ug/L 12/19/23 01:18 75-25-20.50 1
Bromomethane ND ug/L 12/19/23 01:18 74-83-95.0 1
n-Butylbenzene ND ug/L 12/19/23 01:18 104-51-80.50 1
sec-Butylbenzene ND ug/L 12/19/23 01:18 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/19/23 01:18 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/19/23 01:18 56-23-50.50 1
Chlorobenzene ND ug/L 12/19/23 01:18 108-90-70.50 1
Chloroethane ND ug/L 12/19/23 01:18 75-00-31.0 1
Chloroform ND ug/L 12/19/23 01:18 67-66-30.50 1
Chloromethane 1.9 ug/L 12/19/23 01:18 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/19/23 01:18 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/19/23 01:18 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/19/23 01:18 96-12-81.0 1
Dibromochloromethane ND ug/L 12/19/23 01:18 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/19/23 01:18 106-93-40.50 1
Dibromomethane ND ug/L 12/19/23 01:18 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/19/23 01:18 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/19/23 01:18 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/19/23 01:18 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/19/23 01:18 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/19/23 01:18 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/19/23 01:18 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/19/23 01:18 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/19/23 01:18 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/19/23 01:18 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/19/23 01:18 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/19/23 01:18 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/19/23 01:18 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/19/23 01:18 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/19/23 01:18 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/19/23 01:18 10061-02-60.50 1
Diisopropyl ether 0.63 ug/L 12/19/23 01:18 108-20-30.50 1
Ethylbenzene ND ug/L 12/19/23 01:18 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/19/23 01:18 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 12/19/23 01:18 98-82-80.50 1
Methylene Chloride ND ug/L 12/19/23 01:18 75-09-22.0 1
Methyl-tert-butyl ether 4.2 ug/L 12/19/23 01:18 1634-04-40.50 1
Naphthalene ND ug/L 12/19/23 01:18 91-20-32.0 1
n-Propylbenzene ND ug/L 12/19/23 01:18 103-65-10.50 1
Styrene ND ug/L 12/19/23 01:18 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/19/23 01:18 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/19/23 01:18 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Sample:MW-1 Lab ID:92703972001 Collected:12/14/23 11:45 Received:12/14/23 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 12/19/23 01:18 127-18-40.50 1
Toluene ND ug/L 12/19/23 01:18 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/19/23 01:18 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/19/23 01:18 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/19/23 01:18 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/19/23 01:18 79-00-50.50 1
Trichloroethene ND ug/L 12/19/23 01:18 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/19/23 01:18 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/19/23 01:18 96-18-40.50 1
1,2,4-Trimethylbenzene 2.5 ug/L 12/19/23 01:18 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/19/23 01:18 108-67-80.50 1
Vinyl chloride ND ug/L 12/19/23 01:18 75-01-41.0 1
m&p-Xylene 1.6 ug/L 12/19/23 01:18 179601-23-11.0 1
o-Xylene 0.68 ug/L 12/19/23 01:18 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)121 %12/19/23 01:18 17060-07-070-130 1
4-Bromofluorobenzene (S)102 %12/19/23 01:18 460-00-470-130 1
Toluene-d8 (S)100 %12/19/23 01:18 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Sample:MW-2 Lab ID:92703972002 Collected:12/14/23 11:45 Received:12/14/23 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 2.8 ug/L 12/19/23 05:16 71-43-21.2 2.5
Bromobenzene ND ug/L 12/19/23 05:16 108-86-11.2 2.5
Bromochloromethane ND ug/L 12/19/23 05:16 74-97-51.2 2.5
Bromodichloromethane ND ug/L 12/19/23 05:16 75-27-41.2 2.5
Bromoform ND ug/L 12/19/23 05:16 75-25-21.2 2.5
Bromomethane ND ug/L 12/19/23 05:16 74-83-912.5 2.5
n-Butylbenzene ND ug/L 12/19/23 05:16 104-51-81.2 2.5
sec-Butylbenzene ND ug/L 12/19/23 05:16 135-98-81.2 2.5
tert-Butylbenzene ND ug/L 12/19/23 05:16 98-06-61.2 2.5
Carbon tetrachloride ND ug/L 12/19/23 05:16 56-23-51.2 2.5
Chlorobenzene ND ug/L 12/19/23 05:16 108-90-71.2 2.5
Chloroethane ND ug/L 12/19/23 05:16 75-00-32.5 2.5
Chloroform ND ug/L 12/19/23 05:16 67-66-31.2 2.5
Chloromethane ND ug/L 12/19/23 05:16 74-87-32.5 2.5
2-Chlorotoluene ND ug/L 12/19/23 05:16 95-49-81.2 2.5
4-Chlorotoluene ND ug/L 12/19/23 05:16 106-43-41.2 2.5
1,2-Dibromo-3-chloropropane ND ug/L 12/19/23 05:16 96-12-82.5 2.5
Dibromochloromethane ND ug/L 12/19/23 05:16 124-48-11.2 2.5
1,2-Dibromoethane (EDB)ND ug/L 12/19/23 05:16 106-93-41.2 2.5
Dibromomethane ND ug/L 12/19/23 05:16 74-95-31.2 2.5
1,2-Dichlorobenzene ND ug/L 12/19/23 05:16 95-50-11.2 2.5
1,3-Dichlorobenzene ND ug/L 12/19/23 05:16 541-73-11.2 2.5
1,4-Dichlorobenzene ND ug/L 12/19/23 05:16 106-46-71.2 2.5
Dichlorodifluoromethane ND ug/L 12/19/23 05:16 75-71-81.2 2.5
1,1-Dichloroethane ND ug/L 12/19/23 05:16 75-34-31.2 2.5
1,2-Dichloroethane ND ug/L 12/19/23 05:16 107-06-21.2 2.5
1,1-Dichloroethene ND ug/L 12/19/23 05:16 75-35-41.2 2.5
cis-1,2-Dichloroethene ND ug/L 12/19/23 05:16 156-59-21.2 2.5
trans-1,2-Dichloroethene ND ug/L 12/19/23 05:16 156-60-51.2 2.5
1,2-Dichloropropane ND ug/L 12/19/23 05:16 78-87-51.2 2.5
1,3-Dichloropropane ND ug/L 12/19/23 05:16 142-28-91.2 2.5
2,2-Dichloropropane ND ug/L 12/19/23 05:16 594-20-71.2 2.5
1,1-Dichloropropene ND ug/L 12/19/23 05:16 563-58-61.2 2.5
cis-1,3-Dichloropropene ND ug/L 12/19/23 05:16 10061-01-51.2 2.5
trans-1,3-Dichloropropene ND ug/L 12/19/23 05:16 10061-02-61.2 2.5
Diisopropyl ether 12.5 ug/L 12/19/23 05:16 108-20-31.2 2.5
Ethylbenzene 4.0 ug/L 12/19/23 05:16 100-41-41.2 2.5
Hexachloro-1,3-butadiene ND ug/L 12/19/23 05:16 87-68-35.0 2.5
Isopropylbenzene (Cumene)ND ug/L 12/19/23 05:16 98-82-81.2 2.5
Methylene Chloride ND ug/L 12/19/23 05:16 75-09-25.0 2.5
Methyl-tert-butyl ether 3.5 ug/L 12/19/23 05:16 1634-04-41.2 2.5
Naphthalene 12.0 ug/L 12/19/23 05:16 91-20-35.0 2.5
n-Propylbenzene 1.4 ug/L 12/19/23 05:16 103-65-11.2 2.5
Styrene ND ug/L 12/19/23 05:16 100-42-51.2 2.5
1,1,1,2-Tetrachloroethane ND ug/L 12/19/23 05:16 630-20-61.2 2.5
1,1,2,2-Tetrachloroethane ND ug/L 12/19/23 05:16 79-34-51.2 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Sample:MW-2 Lab ID:92703972002 Collected:12/14/23 11:45 Received:12/14/23 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 12/19/23 05:16 127-18-41.2 2.5
Toluene 17.6 ug/L 12/19/23 05:16 108-88-31.2 2.5
1,2,3-Trichlorobenzene ND ug/L 12/19/23 05:16 87-61-65.0 2.5
1,2,4-Trichlorobenzene ND ug/L 12/19/23 05:16 120-82-15.0 2.5
1,1,1-Trichloroethane ND ug/L 12/19/23 05:16 71-55-61.2 2.5
1,1,2-Trichloroethane ND ug/L 12/19/23 05:16 79-00-51.2 2.5
Trichloroethene ND ug/L 12/19/23 05:16 79-01-61.2 2.5
Trichlorofluoromethane ND ug/L 12/19/23 05:16 75-69-42.5 2.5
1,2,3-Trichloropropane ND ug/L 12/19/23 05:16 96-18-41.2 2.5
1,2,4-Trimethylbenzene 45.4 ug/L 12/19/23 05:16 95-63-61.2 2.5
1,3,5-Trimethylbenzene 14.5 ug/L 12/19/23 05:16 108-67-81.2 2.5
Vinyl chloride ND ug/L 12/19/23 05:16 75-01-42.5 2.5
m&p-Xylene 35.1 ug/L 12/19/23 05:16 179601-23-12.5 2.5
o-Xylene 28.0 ug/L 12/19/23 05:16 95-47-61.2 2.5
Surrogates
1,2-Dichloroethane-d4 (S)119 %12/19/23 05:16 17060-07-070-130 2.5
4-Bromofluorobenzene (S)104 %12/19/23 05:16 460-00-470-130 2.5
Toluene-d8 (S)104 %12/19/23 05:16 2037-26-570-130 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Sample:MW-4 Lab ID:92703972003 Collected:12/14/23 11:45 Received:12/14/23 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/19/23 01:37 71-43-20.50 1
Bromobenzene ND ug/L 12/19/23 01:37 108-86-10.50 1
Bromochloromethane ND ug/L 12/19/23 01:37 74-97-50.50 1
Bromodichloromethane ND ug/L 12/19/23 01:37 75-27-40.50 1
Bromoform ND ug/L 12/19/23 01:37 75-25-20.50 1
Bromomethane ND ug/L 12/19/23 01:37 74-83-95.0 1
n-Butylbenzene ND ug/L 12/19/23 01:37 104-51-80.50 1
sec-Butylbenzene ND ug/L 12/19/23 01:37 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/19/23 01:37 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/19/23 01:37 56-23-50.50 1
Chlorobenzene ND ug/L 12/19/23 01:37 108-90-70.50 1
Chloroethane ND ug/L 12/19/23 01:37 75-00-31.0 1
Chloroform ND ug/L 12/19/23 01:37 67-66-30.50 1
Chloromethane ND ug/L 12/19/23 01:37 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/19/23 01:37 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/19/23 01:37 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/19/23 01:37 96-12-81.0 1
Dibromochloromethane ND ug/L 12/19/23 01:37 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/19/23 01:37 106-93-40.50 1
Dibromomethane ND ug/L 12/19/23 01:37 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/19/23 01:37 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/19/23 01:37 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/19/23 01:37 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/19/23 01:37 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/19/23 01:37 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/19/23 01:37 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/19/23 01:37 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/19/23 01:37 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/19/23 01:37 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/19/23 01:37 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/19/23 01:37 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/19/23 01:37 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/19/23 01:37 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/19/23 01:37 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/19/23 01:37 10061-02-60.50 1
Diisopropyl ether ND ug/L 12/19/23 01:37 108-20-30.50 1
Ethylbenzene ND ug/L 12/19/23 01:37 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/19/23 01:37 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 12/19/23 01:37 98-82-80.50 1
Methylene Chloride ND ug/L 12/19/23 01:37 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 12/19/23 01:37 1634-04-40.50 1
Naphthalene ND ug/L 12/19/23 01:37 91-20-32.0 1
n-Propylbenzene ND ug/L 12/19/23 01:37 103-65-10.50 1
Styrene ND ug/L 12/19/23 01:37 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/19/23 01:37 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/19/23 01:37 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Sample:MW-4 Lab ID:92703972003 Collected:12/14/23 11:45 Received:12/14/23 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 12/19/23 01:37 127-18-40.50 1
Toluene ND ug/L 12/19/23 01:37 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/19/23 01:37 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/19/23 01:37 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/19/23 01:37 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/19/23 01:37 79-00-50.50 1
Trichloroethene ND ug/L 12/19/23 01:37 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/19/23 01:37 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/19/23 01:37 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/19/23 01:37 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/19/23 01:37 108-67-80.50 1
Vinyl chloride ND ug/L 12/19/23 01:37 75-01-41.0 1
m&p-Xylene ND ug/L 12/19/23 01:37 179601-23-11.0 1
o-Xylene ND ug/L 12/19/23 01:37 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)122 %12/19/23 01:37 17060-07-070-130 1
4-Bromofluorobenzene (S)102 %12/19/23 01:37 460-00-470-130 1
Toluene-d8 (S)100 %12/19/23 01:37 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Sample:MW-6 Lab ID:92703972004 Collected:12/14/23 11:45 Received:12/14/23 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 26.0 ug/L 12/19/23 03:08 71-43-21.0 2
Bromobenzene ND ug/L 12/19/23 03:08 108-86-11.0 2
Bromochloromethane ND ug/L 12/19/23 03:08 74-97-51.0 2
Bromodichloromethane ND ug/L 12/19/23 03:08 75-27-41.0 2
Bromoform ND ug/L 12/19/23 03:08 75-25-21.0 2
Bromomethane ND ug/L 12/19/23 03:08 74-83-910.0 2
n-Butylbenzene ND ug/L 12/19/23 03:08 104-51-81.0 2
sec-Butylbenzene ND ug/L 12/19/23 03:08 135-98-81.0 2
tert-Butylbenzene ND ug/L 12/19/23 03:08 98-06-61.0 2
Carbon tetrachloride ND ug/L 12/19/23 03:08 56-23-51.0 2
Chlorobenzene ND ug/L 12/19/23 03:08 108-90-71.0 2
Chloroethane ND ug/L 12/19/23 03:08 75-00-32.0 2
Chloroform ND ug/L 12/19/23 03:08 67-66-31.0 2
Chloromethane ND ug/L 12/19/23 03:08 74-87-32.0 2
2-Chlorotoluene ND ug/L 12/19/23 03:08 95-49-81.0 2
4-Chlorotoluene ND ug/L 12/19/23 03:08 106-43-41.0 2
1,2-Dibromo-3-chloropropane ND ug/L 12/19/23 03:08 96-12-82.0 2
Dibromochloromethane ND ug/L 12/19/23 03:08 124-48-11.0 2
1,2-Dibromoethane (EDB)ND ug/L 12/19/23 03:08 106-93-41.0 2
Dibromomethane ND ug/L 12/19/23 03:08 74-95-31.0 2
1,2-Dichlorobenzene ND ug/L 12/19/23 03:08 95-50-11.0 2
1,3-Dichlorobenzene ND ug/L 12/19/23 03:08 541-73-11.0 2
1,4-Dichlorobenzene ND ug/L 12/19/23 03:08 106-46-71.0 2
Dichlorodifluoromethane ND ug/L 12/19/23 03:08 75-71-81.0 2
1,1-Dichloroethane ND ug/L 12/19/23 03:08 75-34-31.0 2
1,2-Dichloroethane ND ug/L 12/19/23 03:08 107-06-21.0 2
1,1-Dichloroethene ND ug/L 12/19/23 03:08 75-35-41.0 2
cis-1,2-Dichloroethene ND ug/L 12/19/23 03:08 156-59-21.0 2
trans-1,2-Dichloroethene ND ug/L 12/19/23 03:08 156-60-51.0 2
1,2-Dichloropropane ND ug/L 12/19/23 03:08 78-87-51.0 2
1,3-Dichloropropane ND ug/L 12/19/23 03:08 142-28-91.0 2
2,2-Dichloropropane ND ug/L 12/19/23 03:08 594-20-71.0 2
1,1-Dichloropropene ND ug/L 12/19/23 03:08 563-58-61.0 2
cis-1,3-Dichloropropene ND ug/L 12/19/23 03:08 10061-01-51.0 2
trans-1,3-Dichloropropene ND ug/L 12/19/23 03:08 10061-02-61.0 2
Diisopropyl ether 4.2 ug/L 12/19/23 03:08 108-20-31.0 2
Ethylbenzene 12.9 ug/L 12/19/23 03:08 100-41-41.0 2
Hexachloro-1,3-butadiene ND ug/L 12/19/23 03:08 87-68-34.0 2
Isopropylbenzene (Cumene)3.9 ug/L 12/19/23 03:08 98-82-81.0 2
Methylene Chloride ND ug/L 12/19/23 03:08 75-09-24.0 2
Methyl-tert-butyl ether 9.8 ug/L 12/19/23 03:08 1634-04-41.0 2
Naphthalene 26.1 ug/L 12/19/23 03:08 91-20-34.0 2
n-Propylbenzene 3.2 ug/L 12/19/23 03:08 103-65-11.0 2
Styrene ND ug/L 12/19/23 03:08 100-42-51.0 2
1,1,1,2-Tetrachloroethane ND ug/L 12/19/23 03:08 630-20-61.0 2
1,1,2,2-Tetrachloroethane ND ug/L 12/19/23 03:08 79-34-51.0 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Sample:MW-6 Lab ID:92703972004 Collected:12/14/23 11:45 Received:12/14/23 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 12/19/23 03:08 127-18-41.0 2
Toluene 18.0 ug/L 12/19/23 03:08 108-88-31.0 2
1,2,3-Trichlorobenzene ND ug/L 12/19/23 03:08 87-61-64.0 2
1,2,4-Trichlorobenzene ND ug/L 12/19/23 03:08 120-82-14.0 2
1,1,1-Trichloroethane ND ug/L 12/19/23 03:08 71-55-61.0 2
1,1,2-Trichloroethane ND ug/L 12/19/23 03:08 79-00-51.0 2
Trichloroethene ND ug/L 12/19/23 03:08 79-01-61.0 2
Trichlorofluoromethane ND ug/L 12/19/23 03:08 75-69-42.0 2
1,2,3-Trichloropropane ND ug/L 12/19/23 03:08 96-18-41.0 2
1,2,4-Trimethylbenzene 31.8 ug/L 12/19/23 03:08 95-63-61.0 2
1,3,5-Trimethylbenzene 7.5 ug/L 12/19/23 03:08 108-67-81.0 2
Vinyl chloride ND ug/L 12/19/23 03:08 75-01-42.0 2
m&p-Xylene 60.9 ug/L 12/19/23 03:08 179601-23-12.0 2
o-Xylene 28.0 ug/L 12/19/23 03:08 95-47-61.0 2
Surrogates
1,2-Dichloroethane-d4 (S)120 %12/19/23 03:08 17060-07-0 D370-130 2
4-Bromofluorobenzene (S)108 %12/19/23 03:08 460-00-470-130 2
Toluene-d8 (S)102 %12/19/23 03:08 2037-26-570-130 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Sample:MW-7 Lab ID:92703972005 Collected:12/14/23 11:45 Received:12/14/23 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/19/23 01:55 71-43-20.50 1
Bromobenzene ND ug/L 12/19/23 01:55 108-86-10.50 1
Bromochloromethane ND ug/L 12/19/23 01:55 74-97-50.50 1
Bromodichloromethane ND ug/L 12/19/23 01:55 75-27-40.50 1
Bromoform ND ug/L 12/19/23 01:55 75-25-20.50 1
Bromomethane ND ug/L 12/19/23 01:55 74-83-95.0 1
n-Butylbenzene ND ug/L 12/19/23 01:55 104-51-80.50 1
sec-Butylbenzene ND ug/L 12/19/23 01:55 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/19/23 01:55 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/19/23 01:55 56-23-50.50 1
Chlorobenzene ND ug/L 12/19/23 01:55 108-90-70.50 1
Chloroethane ND ug/L 12/19/23 01:55 75-00-31.0 1
Chloroform ND ug/L 12/19/23 01:55 67-66-30.50 1
Chloromethane 1.6 ug/L 12/19/23 01:55 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/19/23 01:55 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/19/23 01:55 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/19/23 01:55 96-12-81.0 1
Dibromochloromethane ND ug/L 12/19/23 01:55 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/19/23 01:55 106-93-40.50 1
Dibromomethane ND ug/L 12/19/23 01:55 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/19/23 01:55 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/19/23 01:55 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/19/23 01:55 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/19/23 01:55 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/19/23 01:55 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/19/23 01:55 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/19/23 01:55 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/19/23 01:55 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/19/23 01:55 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/19/23 01:55 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/19/23 01:55 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/19/23 01:55 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/19/23 01:55 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/19/23 01:55 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/19/23 01:55 10061-02-60.50 1
Diisopropyl ether ND ug/L 12/19/23 01:55 108-20-30.50 1
Ethylbenzene ND ug/L 12/19/23 01:55 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/19/23 01:55 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 12/19/23 01:55 98-82-80.50 1
Methylene Chloride ND ug/L 12/19/23 01:55 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 12/19/23 01:55 1634-04-40.50 1
Naphthalene ND ug/L 12/19/23 01:55 91-20-32.0 1
n-Propylbenzene ND ug/L 12/19/23 01:55 103-65-10.50 1
Styrene ND ug/L 12/19/23 01:55 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/19/23 01:55 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/19/23 01:55 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Sample:MW-7 Lab ID:92703972005 Collected:12/14/23 11:45 Received:12/14/23 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 12/19/23 01:55 127-18-40.50 1
Toluene ND ug/L 12/19/23 01:55 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/19/23 01:55 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/19/23 01:55 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/19/23 01:55 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/19/23 01:55 79-00-50.50 1
Trichloroethene ND ug/L 12/19/23 01:55 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/19/23 01:55 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/19/23 01:55 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/19/23 01:55 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/19/23 01:55 108-67-80.50 1
Vinyl chloride ND ug/L 12/19/23 01:55 75-01-41.0 1
m&p-Xylene ND ug/L 12/19/23 01:55 179601-23-11.0 1
o-Xylene ND ug/L 12/19/23 01:55 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)121 %12/19/23 01:55 17060-07-070-130 1
4-Bromofluorobenzene (S)102 %12/19/23 01:55 460-00-470-130 1
Toluene-d8 (S)100 %12/19/23 01:55 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Sample:MW-8 Lab ID:92703972006 Collected:12/14/23 11:45 Received:12/14/23 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/19/23 02:13 71-43-20.50 1
Bromobenzene ND ug/L 12/19/23 02:13 108-86-10.50 1
Bromochloromethane ND ug/L 12/19/23 02:13 74-97-50.50 1
Bromodichloromethane ND ug/L 12/19/23 02:13 75-27-40.50 1
Bromoform ND ug/L 12/19/23 02:13 75-25-20.50 1
Bromomethane ND ug/L 12/19/23 02:13 74-83-95.0 1
n-Butylbenzene ND ug/L 12/19/23 02:13 104-51-80.50 1
sec-Butylbenzene ND ug/L 12/19/23 02:13 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/19/23 02:13 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/19/23 02:13 56-23-50.50 1
Chlorobenzene ND ug/L 12/19/23 02:13 108-90-70.50 1
Chloroethane ND ug/L 12/19/23 02:13 75-00-31.0 1
Chloroform ND ug/L 12/19/23 02:13 67-66-30.50 1
Chloromethane ND ug/L 12/19/23 02:13 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/19/23 02:13 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/19/23 02:13 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/19/23 02:13 96-12-81.0 1
Dibromochloromethane ND ug/L 12/19/23 02:13 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/19/23 02:13 106-93-40.50 1
Dibromomethane ND ug/L 12/19/23 02:13 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/19/23 02:13 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/19/23 02:13 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/19/23 02:13 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/19/23 02:13 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/19/23 02:13 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/19/23 02:13 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/19/23 02:13 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/19/23 02:13 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/19/23 02:13 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/19/23 02:13 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/19/23 02:13 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/19/23 02:13 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/19/23 02:13 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/19/23 02:13 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/19/23 02:13 10061-02-60.50 1
Diisopropyl ether ND ug/L 12/19/23 02:13 108-20-30.50 1
Ethylbenzene ND ug/L 12/19/23 02:13 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/19/23 02:13 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 12/19/23 02:13 98-82-80.50 1
Methylene Chloride ND ug/L 12/19/23 02:13 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 12/19/23 02:13 1634-04-40.50 1
Naphthalene ND ug/L 12/19/23 02:13 91-20-32.0 1
n-Propylbenzene ND ug/L 12/19/23 02:13 103-65-10.50 1
Styrene ND ug/L 12/19/23 02:13 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/19/23 02:13 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/19/23 02:13 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Sample:MW-8 Lab ID:92703972006 Collected:12/14/23 11:45 Received:12/14/23 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 12/19/23 02:13 127-18-40.50 1
Toluene ND ug/L 12/19/23 02:13 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/19/23 02:13 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/19/23 02:13 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/19/23 02:13 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/19/23 02:13 79-00-50.50 1
Trichloroethene ND ug/L 12/19/23 02:13 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/19/23 02:13 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/19/23 02:13 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/19/23 02:13 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/19/23 02:13 108-67-80.50 1
Vinyl chloride ND ug/L 12/19/23 02:13 75-01-41.0 1
m&p-Xylene ND ug/L 12/19/23 02:13 179601-23-11.0 1
o-Xylene ND ug/L 12/19/23 02:13 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)121 %12/19/23 02:13 17060-07-070-130 1
4-Bromofluorobenzene (S)102 %12/19/23 02:13 460-00-470-130 1
Toluene-d8 (S)101 %12/19/23 02:13 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Sample:MW-10 Lab ID:92703972007 Collected:12/14/23 11:45 Received:12/14/23 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/20/23 20:50 71-43-22.5 5
Bromobenzene ND ug/L 12/20/23 20:50 108-86-12.5 5
Bromochloromethane ND ug/L 12/20/23 20:50 74-97-52.5 5
Bromodichloromethane ND ug/L 12/20/23 20:50 75-27-42.5 5
Bromoform ND ug/L 12/20/23 20:50 75-25-22.5 5
Bromomethane ND ug/L 12/20/23 20:50 74-83-925.0 5
n-Butylbenzene ND ug/L 12/20/23 20:50 104-51-82.5 5
sec-Butylbenzene ND ug/L 12/20/23 20:50 135-98-82.5 5
tert-Butylbenzene ND ug/L 12/20/23 20:50 98-06-62.5 5
Carbon tetrachloride ND ug/L 12/20/23 20:50 56-23-52.5 5
Chlorobenzene ND ug/L 12/20/23 20:50 108-90-72.5 5
Chloroethane ND ug/L 12/20/23 20:50 75-00-35.0 5
Chloroform ND ug/L 12/20/23 20:50 67-66-32.5 5
Chloromethane ND ug/L 12/20/23 20:50 74-87-35.0 5
2-Chlorotoluene ND ug/L 12/20/23 20:50 95-49-82.5 5
4-Chlorotoluene ND ug/L 12/20/23 20:50 106-43-42.5 5
1,2-Dibromo-3-chloropropane ND ug/L 12/20/23 20:50 96-12-85.0 5
Dibromochloromethane ND ug/L 12/20/23 20:50 124-48-12.5 5
1,2-Dibromoethane (EDB)ND ug/L 12/20/23 20:50 106-93-42.5 5
Dibromomethane ND ug/L 12/20/23 20:50 74-95-32.5 5
1,2-Dichlorobenzene ND ug/L 12/20/23 20:50 95-50-12.5 5
1,3-Dichlorobenzene ND ug/L 12/20/23 20:50 541-73-12.5 5
1,4-Dichlorobenzene ND ug/L 12/20/23 20:50 106-46-72.5 5
Dichlorodifluoromethane ND ug/L 12/20/23 20:50 75-71-82.5 5
1,1-Dichloroethane ND ug/L 12/20/23 20:50 75-34-32.5 5
1,2-Dichloroethane ND ug/L 12/20/23 20:50 107-06-22.5 5
1,1-Dichloroethene ND ug/L 12/20/23 20:50 75-35-42.5 5
cis-1,2-Dichloroethene ND ug/L 12/20/23 20:50 156-59-22.5 5
trans-1,2-Dichloroethene ND ug/L 12/20/23 20:50 156-60-52.5 5
1,2-Dichloropropane ND ug/L 12/20/23 20:50 78-87-52.5 5
1,3-Dichloropropane ND ug/L 12/20/23 20:50 142-28-92.5 5
2,2-Dichloropropane ND ug/L 12/20/23 20:50 594-20-72.5 5
1,1-Dichloropropene ND ug/L 12/20/23 20:50 563-58-62.5 5
cis-1,3-Dichloropropene ND ug/L 12/20/23 20:50 10061-01-52.5 5
trans-1,3-Dichloropropene ND ug/L 12/20/23 20:50 10061-02-62.5 5
Diisopropyl ether ND ug/L 12/20/23 20:50 108-20-32.5 5
Ethylbenzene 2.6 ug/L 12/20/23 20:50 100-41-42.5 5
Hexachloro-1,3-butadiene ND ug/L 12/20/23 20:50 87-68-310.0 5
Isopropylbenzene (Cumene)10.2 ug/L 12/20/23 20:50 98-82-82.5 5
Methylene Chloride ND ug/L 12/20/23 20:50 75-09-210.0 5
Methyl-tert-butyl ether ND ug/L 12/20/23 20:50 1634-04-42.5 5
Naphthalene 69.9 ug/L 12/20/23 20:50 91-20-310.0 5
n-Propylbenzene 40.7 ug/L 12/20/23 20:50 103-65-12.5 5
Styrene ND ug/L 12/20/23 20:50 100-42-52.5 5
1,1,1,2-Tetrachloroethane ND ug/L 12/20/23 20:50 630-20-62.5 5
1,1,2,2-Tetrachloroethane ND ug/L 12/20/23 20:50 79-34-52.5 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Sample:MW-10 Lab ID:92703972007 Collected:12/14/23 11:45 Received:12/14/23 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 12/20/23 20:50 127-18-42.5 5
Toluene 3.6 ug/L 12/20/23 20:50 108-88-32.5 5
1,2,3-Trichlorobenzene ND ug/L 12/20/23 20:50 87-61-610.0 5
1,2,4-Trichlorobenzene ND ug/L 12/20/23 20:50 120-82-110.0 5
1,1,1-Trichloroethane ND ug/L 12/20/23 20:50 71-55-62.5 5
1,1,2-Trichloroethane ND ug/L 12/20/23 20:50 79-00-52.5 5
Trichloroethene ND ug/L 12/20/23 20:50 79-01-62.5 5
Trichlorofluoromethane ND ug/L 12/20/23 20:50 75-69-45.0 5
1,2,3-Trichloropropane ND ug/L 12/20/23 20:50 96-18-42.5 5
1,2,4-Trimethylbenzene 437 ug/L 12/20/23 20:50 95-63-62.5 5
1,3,5-Trimethylbenzene 134 ug/L 12/20/23 20:50 108-67-82.5 5
Vinyl chloride ND ug/L 12/20/23 20:50 75-01-45.0 5
m&p-Xylene 130 ug/L 12/20/23 20:50 179601-23-15.0 5
o-Xylene 49.3 ug/L 12/20/23 20:50 95-47-62.5 5
Surrogates
1,2-Dichloroethane-d4 (S)120 %12/20/23 20:50 17060-07-070-130 5
4-Bromofluorobenzene (S)105 %12/20/23 20:50 460-00-470-130 5
Toluene-d8 (S)101 %12/20/23 20:50 2037-26-570-130 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Sample:MW-11 Lab ID:92703972008 Collected:12/14/23 11:45 Received:12/14/23 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/19/23 02:32 71-43-20.50 1
Bromobenzene ND ug/L 12/19/23 02:32 108-86-10.50 1
Bromochloromethane ND ug/L 12/19/23 02:32 74-97-50.50 1
Bromodichloromethane ND ug/L 12/19/23 02:32 75-27-40.50 1
Bromoform ND ug/L 12/19/23 02:32 75-25-20.50 1
Bromomethane ND ug/L 12/19/23 02:32 74-83-95.0 1
n-Butylbenzene ND ug/L 12/19/23 02:32 104-51-80.50 1
sec-Butylbenzene ND ug/L 12/19/23 02:32 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/19/23 02:32 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/19/23 02:32 56-23-50.50 1
Chlorobenzene ND ug/L 12/19/23 02:32 108-90-70.50 1
Chloroethane ND ug/L 12/19/23 02:32 75-00-31.0 1
Chloroform ND ug/L 12/19/23 02:32 67-66-30.50 1
Chloromethane ND ug/L 12/19/23 02:32 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/19/23 02:32 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/19/23 02:32 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/19/23 02:32 96-12-81.0 1
Dibromochloromethane ND ug/L 12/19/23 02:32 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/19/23 02:32 106-93-40.50 1
Dibromomethane ND ug/L 12/19/23 02:32 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/19/23 02:32 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/19/23 02:32 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/19/23 02:32 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/19/23 02:32 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/19/23 02:32 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/19/23 02:32 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/19/23 02:32 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/19/23 02:32 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/19/23 02:32 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/19/23 02:32 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/19/23 02:32 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/19/23 02:32 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/19/23 02:32 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/19/23 02:32 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/19/23 02:32 10061-02-60.50 1
Diisopropyl ether ND ug/L 12/19/23 02:32 108-20-30.50 1
Ethylbenzene ND ug/L 12/19/23 02:32 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/19/23 02:32 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 12/19/23 02:32 98-82-80.50 1
Methylene Chloride ND ug/L 12/19/23 02:32 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 12/19/23 02:32 1634-04-40.50 1
Naphthalene ND ug/L 12/19/23 02:32 91-20-32.0 1
n-Propylbenzene ND ug/L 12/19/23 02:32 103-65-10.50 1
Styrene ND ug/L 12/19/23 02:32 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/19/23 02:32 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/19/23 02:32 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Sample:MW-11 Lab ID:92703972008 Collected:12/14/23 11:45 Received:12/14/23 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 12/19/23 02:32 127-18-40.50 1
Toluene ND ug/L 12/19/23 02:32 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/19/23 02:32 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/19/23 02:32 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/19/23 02:32 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/19/23 02:32 79-00-50.50 1
Trichloroethene ND ug/L 12/19/23 02:32 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/19/23 02:32 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/19/23 02:32 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/19/23 02:32 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/19/23 02:32 108-67-80.50 1
Vinyl chloride ND ug/L 12/19/23 02:32 75-01-41.0 1
m&p-Xylene ND ug/L 12/19/23 02:32 179601-23-11.0 1
o-Xylene ND ug/L 12/19/23 02:32 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)120 %12/19/23 02:32 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %12/19/23 02:32 460-00-470-130 1
Toluene-d8 (S)99 %12/19/23 02:32 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Sample:MW-12 Lab ID:92703972009 Collected:12/14/23 11:45 Received:12/14/23 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 0.56 ug/L 12/20/23 18:06 71-43-20.50 1
Bromobenzene ND ug/L 12/20/23 18:06 108-86-10.50 1
Bromochloromethane ND ug/L 12/20/23 18:06 74-97-50.50 1
Bromodichloromethane ND ug/L 12/20/23 18:06 75-27-40.50 1
Bromoform ND ug/L 12/20/23 18:06 75-25-20.50 1
Bromomethane ND ug/L 12/20/23 18:06 74-83-95.0 1
n-Butylbenzene ND ug/L 12/20/23 18:06 104-51-80.50 1
sec-Butylbenzene ND ug/L 12/20/23 18:06 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/20/23 18:06 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/20/23 18:06 56-23-50.50 1
Chlorobenzene ND ug/L 12/20/23 18:06 108-90-70.50 1
Chloroethane ND ug/L 12/20/23 18:06 75-00-31.0 1
Chloroform ND ug/L 12/20/23 18:06 67-66-30.50 1
Chloromethane ND ug/L 12/20/23 18:06 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/20/23 18:06 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/20/23 18:06 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/20/23 18:06 96-12-81.0 1
Dibromochloromethane ND ug/L 12/20/23 18:06 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/20/23 18:06 106-93-40.50 1
Dibromomethane ND ug/L 12/20/23 18:06 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/20/23 18:06 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/20/23 18:06 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/20/23 18:06 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/20/23 18:06 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/20/23 18:06 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/20/23 18:06 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/20/23 18:06 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/20/23 18:06 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/20/23 18:06 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/20/23 18:06 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/20/23 18:06 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/20/23 18:06 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/20/23 18:06 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/20/23 18:06 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/20/23 18:06 10061-02-60.50 1
Diisopropyl ether ND ug/L 12/20/23 18:06 108-20-30.50 1
Ethylbenzene 1.3 ug/L 12/20/23 18:06 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/20/23 18:06 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 12/20/23 18:06 98-82-80.50 1
Methylene Chloride ND ug/L 12/20/23 18:06 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 12/20/23 18:06 1634-04-40.50 1
Naphthalene 5.6 ug/L 12/20/23 18:06 91-20-32.0 1
n-Propylbenzene 1.1 ug/L 12/20/23 18:06 103-65-10.50 1
Styrene ND ug/L 12/20/23 18:06 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/20/23 18:06 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/20/23 18:06 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Sample:MW-12 Lab ID:92703972009 Collected:12/14/23 11:45 Received:12/14/23 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 12/20/23 18:06 127-18-40.50 1
Toluene 3.7 ug/L 12/20/23 18:06 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/20/23 18:06 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/20/23 18:06 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/20/23 18:06 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/20/23 18:06 79-00-50.50 1
Trichloroethene ND ug/L 12/20/23 18:06 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/20/23 18:06 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/20/23 18:06 96-18-40.50 1
1,2,4-Trimethylbenzene 12.4 ug/L 12/20/23 18:06 95-63-60.50 1
1,3,5-Trimethylbenzene 2.9 ug/L 12/20/23 18:06 108-67-80.50 1
Vinyl chloride ND ug/L 12/20/23 18:06 75-01-41.0 1
m&p-Xylene 7.6 ug/L 12/20/23 18:06 179601-23-11.0 1
o-Xylene 4.1 ug/L 12/20/23 18:06 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)122 %12/20/23 18:06 17060-07-070-130 1
4-Bromofluorobenzene (S)106 %12/20/23 18:06 460-00-470-130 1
Toluene-d8 (S)101 %12/20/23 18:06 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Sample:MW-16 Lab ID:92703972010 Collected:12/14/23 11:45 Received:12/14/23 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 1.5 ug/L 12/20/23 18:42 71-43-20.50 1
Bromobenzene ND ug/L 12/20/23 18:42 108-86-10.50 1
Bromochloromethane ND ug/L 12/20/23 18:42 74-97-50.50 1
Bromodichloromethane ND ug/L 12/20/23 18:42 75-27-40.50 1
Bromoform ND ug/L 12/20/23 18:42 75-25-20.50 1
Bromomethane ND ug/L 12/20/23 18:42 74-83-95.0 1
n-Butylbenzene ND ug/L 12/20/23 18:42 104-51-80.50 1
sec-Butylbenzene ND ug/L 12/20/23 18:42 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/20/23 18:42 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/20/23 18:42 56-23-50.50 1
Chlorobenzene ND ug/L 12/20/23 18:42 108-90-70.50 1
Chloroethane ND ug/L 12/20/23 18:42 75-00-31.0 1
Chloroform ND ug/L 12/20/23 18:42 67-66-30.50 1
Chloromethane ND ug/L 12/20/23 18:42 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/20/23 18:42 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/20/23 18:42 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/20/23 18:42 96-12-81.0 1
Dibromochloromethane ND ug/L 12/20/23 18:42 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/20/23 18:42 106-93-40.50 1
Dibromomethane ND ug/L 12/20/23 18:42 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/20/23 18:42 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/20/23 18:42 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/20/23 18:42 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/20/23 18:42 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/20/23 18:42 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/20/23 18:42 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/20/23 18:42 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/20/23 18:42 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/20/23 18:42 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/20/23 18:42 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/20/23 18:42 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/20/23 18:42 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/20/23 18:42 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/20/23 18:42 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/20/23 18:42 10061-02-60.50 1
Diisopropyl ether 1.3 ug/L 12/20/23 18:42 108-20-30.50 1
Ethylbenzene 3.5 ug/L 12/20/23 18:42 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/20/23 18:42 87-68-32.0 1
Isopropylbenzene (Cumene)0.62 ug/L 12/20/23 18:42 98-82-80.50 1
Methylene Chloride ND ug/L 12/20/23 18:42 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 12/20/23 18:42 1634-04-40.50 1
Naphthalene 18.0 ug/L 12/20/23 18:42 91-20-32.0 1
n-Propylbenzene 3.0 ug/L 12/20/23 18:42 103-65-10.50 1
Styrene ND ug/L 12/20/23 18:42 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/20/23 18:42 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/20/23 18:42 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 22 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Sample:MW-16 Lab ID:92703972010 Collected:12/14/23 11:45 Received:12/14/23 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 12/20/23 18:42 127-18-40.50 1
Toluene 9.8 ug/L 12/20/23 18:42 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/20/23 18:42 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/20/23 18:42 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/20/23 18:42 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/20/23 18:42 79-00-50.50 1
Trichloroethene ND ug/L 12/20/23 18:42 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/20/23 18:42 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/20/23 18:42 96-18-40.50 1
1,2,4-Trimethylbenzene 35.8 ug/L 12/20/23 18:42 95-63-60.50 1
1,3,5-Trimethylbenzene 8.5 ug/L 12/20/23 18:42 108-67-80.50 1
Vinyl chloride ND ug/L 12/20/23 18:42 75-01-41.0 1
m&p-Xylene 21.5 ug/L 12/20/23 18:42 179601-23-11.0 1
o-Xylene 11.6 ug/L 12/20/23 18:42 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)121 %12/20/23 18:42 17060-07-070-130 1
4-Bromofluorobenzene (S)106 %12/20/23 18:42 460-00-470-130 1
Toluene-d8 (S)101 %12/20/23 18:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
820288
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92703972001, 92703972002, 92703972003, 92703972004, 92703972005, 92703972006, 92703972008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4245856
Associated Lab Samples:92703972001, 92703972002, 92703972003, 92703972004, 92703972005, 92703972006, 92703972008
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 12/18/23 22:34
1,1,1-Trichloroethane ug/L ND 0.50 12/18/23 22:34
1,1,2,2-Tetrachloroethane ug/L ND 0.50 12/18/23 22:34
1,1,2-Trichloroethane ug/L ND 0.50 12/18/23 22:34
1,1-Dichloroethane ug/L ND 0.50 12/18/23 22:34
1,1-Dichloroethene ug/L ND 0.50 12/18/23 22:34
1,1-Dichloropropene ug/L ND 0.50 12/18/23 22:34
1,2,3-Trichlorobenzene ug/L ND 2.0 12/18/23 22:34
1,2,3-Trichloropropane ug/L ND 0.50 12/18/23 22:34
1,2,4-Trichlorobenzene ug/L ND 2.0 12/18/23 22:34
1,2,4-Trimethylbenzene ug/L ND 0.50 12/18/23 22:34
1,2-Dibromo-3-chloropropane ug/L ND 1.0 12/18/23 22:34
1,2-Dibromoethane (EDB)ug/L ND 0.50 12/18/23 22:34
1,2-Dichlorobenzene ug/L ND 0.50 12/18/23 22:34
1,2-Dichloroethane ug/L ND 0.50 12/18/23 22:34
1,2-Dichloropropane ug/L ND 0.50 12/18/23 22:34
1,3,5-Trimethylbenzene ug/L ND 0.50 12/18/23 22:34
1,3-Dichlorobenzene ug/L ND 0.50 12/18/23 22:34
1,3-Dichloropropane ug/L ND 0.50 12/18/23 22:34
1,4-Dichlorobenzene ug/L ND 0.50 12/18/23 22:34
2,2-Dichloropropane ug/L ND 0.50 12/18/23 22:34
2-Chlorotoluene ug/L ND 0.50 12/18/23 22:34
4-Chlorotoluene ug/L ND 0.50 12/18/23 22:34
Benzene ug/L ND 0.50 12/18/23 22:34
Bromobenzene ug/L ND 0.50 12/18/23 22:34
Bromochloromethane ug/L ND 0.50 12/18/23 22:34
Bromodichloromethane ug/L ND 0.50 12/18/23 22:34
Bromoform ug/L ND 0.50 12/18/23 22:34
Bromomethane ug/L ND 5.0 12/18/23 22:34
Carbon tetrachloride ug/L ND 0.50 12/18/23 22:34
Chlorobenzene ug/L ND 0.50 12/18/23 22:34
Chloroethane ug/L ND 1.0 12/18/23 22:34
Chloroform ug/L ND 0.50 12/18/23 22:34
Chloromethane ug/L ND 1.0 12/18/23 22:34
cis-1,2-Dichloroethene ug/L ND 0.50 12/18/23 22:34
cis-1,3-Dichloropropene ug/L ND 0.50 12/18/23 22:34
Dibromochloromethane ug/L ND 0.50 12/18/23 22:34
Dibromomethane ug/L ND 0.50 12/18/23 22:34
Dichlorodifluoromethane ug/L ND 0.50 12/18/23 22:34
Diisopropyl ether ug/L ND 0.50 12/18/23 22:34
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4245856
Associated Lab Samples:92703972001, 92703972002, 92703972003, 92703972004, 92703972005, 92703972006, 92703972008
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 12/18/23 22:34
Hexachloro-1,3-butadiene ug/L ND 2.0 12/18/23 22:34
Isopropylbenzene (Cumene)ug/L ND 0.50 12/18/23 22:34
m&p-Xylene ug/L ND 1.0 12/18/23 22:34
Methyl-tert-butyl ether ug/L ND 0.50 12/18/23 22:34
Methylene Chloride ug/L ND 2.0 12/18/23 22:34
n-Butylbenzene ug/L ND 0.50 12/18/23 22:34
n-Propylbenzene ug/L ND 0.50 12/18/23 22:34
Naphthalene ug/L ND 2.0 12/18/23 22:34
o-Xylene ug/L ND 0.50 12/18/23 22:34
sec-Butylbenzene ug/L ND 0.50 12/18/23 22:34
Styrene ug/L ND 0.50 12/18/23 22:34
tert-Butylbenzene ug/L ND 0.50 12/18/23 22:34
Tetrachloroethene ug/L ND 0.50 12/18/23 22:34
Toluene ug/L ND 0.50 12/18/23 22:34
trans-1,2-Dichloroethene ug/L ND 0.50 12/18/23 22:34
trans-1,3-Dichloropropene ug/L ND 0.50 12/18/23 22:34
Trichloroethene ug/L ND 0.50 12/18/23 22:34
Trichlorofluoromethane ug/L ND 1.0 12/18/23 22:34
Vinyl chloride ug/L ND 1.0 12/18/23 22:34
1,2-Dichloroethane-d4 (S)%121 70-130 12/18/23 22:34
4-Bromofluorobenzene (S)%104 70-130 12/18/23 22:34
Toluene-d8 (S)%100 70-130 12/18/23 22:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4245857LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 20.420 102 60-140
1,1,1-Trichloroethane ug/L 23.620 118 60-140
1,1,2,2-Tetrachloroethane ug/L 22.720 114 60-140
1,1,2-Trichloroethane ug/L 22.220 111 60-140
1,1-Dichloroethane ug/L 25.320 127 60-140
1,1-Dichloroethene ug/L 24.120 120 60-140
1,1-Dichloropropene ug/L 26.820 134 60-140
1,2,3-Trichlorobenzene ug/L 18.220 91 60-140
1,2,3-Trichloropropane ug/L 21.820 109 60-140
1,2,4-Trichlorobenzene ug/L 18.020 90 60-140
1,2,4-Trimethylbenzene ug/L 22.520 112 60-140
1,2-Dibromo-3-chloropropane ug/L 20.220 101 60-140
1,2-Dibromoethane (EDB)ug/L 22.320 111 60-140
1,2-Dichlorobenzene ug/L 21.220 106 60-140
1,2-Dichloroethane ug/L 25.720 128 60-140
1,2-Dichloropropane ug/L 23.620 118 60-140
1,3,5-Trimethylbenzene ug/L 22.520 113 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4245857LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 21.120 106 60-140
1,3-Dichloropropane ug/L 22.320 112 60-140
1,4-Dichlorobenzene ug/L 20.520 102 60-140
2,2-Dichloropropane ug/L 21.620 108 60-140
2-Chlorotoluene ug/L 22.920 115 60-140
4-Chlorotoluene ug/L 23.420 117 60-140
Benzene ug/L 22.220 111 60-140
Bromobenzene ug/L 20.820 104 60-140
Bromochloromethane ug/L 24.020 120 60-140
Bromodichloromethane ug/L 21.720 108 60-140
Bromoform ug/L 17.920 90 60-140
Bromomethane ug/L 17.920 89 60-140
Carbon tetrachloride ug/L 20.020 100 60-140
Chlorobenzene ug/L 20.820 104 60-140
Chloroethane ug/L 23.420 117 60-140
Chloroform ug/L 24.120 121 60-140
Chloromethane ug/L 23.020 115 60-140
cis-1,2-Dichloroethene ug/L 25.920 130 60-140
cis-1,3-Dichloropropene ug/L 21.620 108 60-140
Dibromochloromethane ug/L 20.320 101 60-140
Dibromomethane ug/L 19.020 95 60-140
Dichlorodifluoromethane ug/L 19.320 97 60-140
Diisopropyl ether ug/L 25.020 125 60-140
Ethylbenzene ug/L 21.220 106 60-140
Hexachloro-1,3-butadiene ug/L 17.220 86 60-140
Isopropylbenzene (Cumene)ug/L 21.120 106 60-140
m&p-Xylene ug/L 43.240 108 60-140
Methyl-tert-butyl ether ug/L 23.320 116 60-140
Methylene Chloride ug/L 24.720 124 60-140
n-Butylbenzene ug/L 22.720 113 60-140
n-Propylbenzene ug/L 22.320 112 60-140
Naphthalene ug/L 20.220 101 60-140
o-Xylene ug/L 20.720 104 60-140
sec-Butylbenzene ug/L 22.020 110 60-140
Styrene ug/L 21.720 109 60-140
tert-Butylbenzene ug/L 17.420 87 60-140
Tetrachloroethene ug/L 18.220 91 60-140
Toluene ug/L 20.620 103 60-140
trans-1,2-Dichloroethene ug/L 26.420 132 60-140
trans-1,3-Dichloropropene ug/L 21.420 107 60-140
Trichloroethene ug/L 20.320 101 60-140
Trichlorofluoromethane ug/L 20.320 101 60-140
Vinyl chloride ug/L 20.820 104 60-140
1,2-Dichloroethane-d4 (S)%121 70-130
4-Bromofluorobenzene (S)%106 70-130
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4245858MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92704135001
4245859
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 127 60-140115 1020ND25.4 22.9
1,1,1-Trichloroethane ug/L M12015460-140137 1120ND30.8 27.5
1,1,2,2-Tetrachloroethane ug/L 20 134 60-140127 620ND26.9 25.3
1,1,2-Trichloroethane ug/L 20 133 60-140124 720ND26.6 24.8
1,1-Dichloroethane ug/L M12016260-140146 1020ND32.4 29.1
1,1-Dichloroethene ug/L M12015960-140141 1220ND31.9 28.2
1,1-Dichloropropene ug/L M12017860-140159 1120ND35.6 31.8
1,2,3-Trichlorobenzene ug/L 20 113 60-14097 1420ND22.5 19.5
1,2,3-Trichloropropane ug/L 20 130 60-140122 620ND26.1 24.5
1,2,4-Trichlorobenzene ug/L 20 113 60-140101 1120ND22.6 20.2
1,2,4-Trimethylbenzene ug/L M12014260-140130 920ND28.4 26.1
1,2-Dibromo-3-chloropropane ug/L 20 115 60-140106 820ND22.9 21.2
1,2-Dibromoethane (EDB)ug/L 20 133 60-140123 720ND26.5 24.7
1,2-Dichlorobenzene ug/L 20 128 60-140119 720ND25.6 23.8
1,2-Dichloroethane ug/L M12015560-140140 1020ND31.1 28.0
1,2-Dichloropropane ug/L M12014860-140134 1020ND29.5 26.9
1,3,5-Trimethylbenzene ug/L M12014260-140130 920ND28.4 25.9
1,3-Dichlorobenzene ug/L 20 128 60-140120 720ND25.7 23.9
1,3-Dichloropropane ug/L 20 134 60-140124 720ND26.7 24.9
1,4-Dichlorobenzene ug/L 20 125 60-140116 720ND25.0 23.3
2,2-Dichloropropane ug/L M12015460-140137 1120ND30.8 27.5
2-Chlorotoluene ug/L M12014160-140131 820ND28.3 26.2
4-Chlorotoluene ug/L M12014260-140132 820ND28.4 26.3
Benzene ug/L 20 140 60-140127 1020ND28.1 25.3
Bromobenzene ug/L 20 123 60-140114 720ND24.6 22.8
Bromochloromethane ug/L M12014660-140133 1020ND29.3 26.6
Bromodichloromethane ug/L 20 133 60-140121 920ND26.6 24.2
Bromoform ug/L 20 108 60-140101 620ND21.6 20.2
Bromomethane ug/L 20 105 60-14099 520ND21.0 19.9
Carbon tetrachloride ug/L 20 132 60-140117 1220ND26.4 23.5
Chlorobenzene ug/L 20 130 60-140119 820ND25.9 23.8
Chloroethane ug/L M12014760-140131 1120ND29.4 26.3
Chloroform ug/L M12015260-140132 1420ND30.5 26.4
Chloromethane ug/L 20 140 60-140126 1020ND28.0 25.3
cis-1,2-Dichloroethene ug/L M12016060-140145 1020ND32.0 29.0
cis-1,3-Dichloropropene ug/L 20 136 60-140123 1020ND27.2 24.6
Dibromochloromethane ug/L 20 123 60-140113 820ND24.7 22.7
Dibromomethane ug/L 20 112 60-140105 720ND22.5 21.0
Dichlorodifluoromethane ug/L 20 114 60-140101 1320ND22.8 20.1
Diisopropyl ether ug/L M12015460-140140 920ND30.7 28.1
Ethylbenzene ug/L 20 134 60-140123 920ND26.8 24.6
Hexachloro-1,3-butadiene ug/L 20 126 60-140110 1320ND25.2 22.1
Isopropylbenzene (Cumene)ug/L 20 137 60-140124 1020ND27.3 24.8
m&p-Xylene ug/L 40 137 60-140125 940ND54.8 49.8
Methyl-tert-butyl ether ug/L 20 140 60-140129 820ND28.0 25.8
Methylene Chloride ug/L M12015160-140134 1220ND30.2 26.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4245858MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92704135001
4245859
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L M12015760-140141 1120ND31.4 28.2
n-Propylbenzene ug/L M12014360-140131 920ND28.7 26.2
Naphthalene ug/L 20 115 60-140105 920ND23.0 21.0
o-Xylene ug/L 20 132 60-140120 1020ND26.3 23.9
sec-Butylbenzene ug/L M12014460-140130 1020ND28.9 26.0
Styrene ug/L 20 135 60-140124 920ND27.1 24.7
tert-Butylbenzene ug/L 20 111 60-140101 920ND22.2 20.3
Tetrachloroethene ug/L 20 119 60-140109 1020ND23.9 21.7
Toluene ug/L 20 131 60-140119 920ND26.1 23.8
trans-1,2-Dichloroethene ug/L M12017360-140153 1220ND34.5 30.7
trans-1,3-Dichloropropene ug/L 20 133 60-140122 920ND26.6 24.4
Trichloroethene ug/L 20 130 60-140118 1020ND26.0 23.6
Trichlorofluoromethane ug/L 20 133 60-140119 1120ND26.6 23.7
Vinyl chloride ug/L 20 132 60-140118 1120ND26.5 23.7
1,2-Dichloroethane-d4 (S)%120 70-130119
4-Bromofluorobenzene (S)%107 70-130106
Toluene-d8 (S)%101 70-130102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
820540
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92703972007, 92703972009, 92703972010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4247144
Associated Lab Samples:92703972007, 92703972009, 92703972010
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 12/20/23 13:33
1,1,1-Trichloroethane ug/L ND 0.50 12/20/23 13:33
1,1,2,2-Tetrachloroethane ug/L ND 0.50 12/20/23 13:33
1,1,2-Trichloroethane ug/L ND 0.50 12/20/23 13:33
1,1-Dichloroethane ug/L ND 0.50 12/20/23 13:33
1,1-Dichloroethene ug/L ND 0.50 12/20/23 13:33
1,1-Dichloropropene ug/L ND 0.50 12/20/23 13:33
1,2,3-Trichlorobenzene ug/L ND 2.0 12/20/23 13:33
1,2,3-Trichloropropane ug/L ND 0.50 12/20/23 13:33
1,2,4-Trichlorobenzene ug/L ND 2.0 12/20/23 13:33
1,2,4-Trimethylbenzene ug/L ND 0.50 12/20/23 13:33
1,2-Dibromo-3-chloropropane ug/L ND 1.0 12/20/23 13:33
1,2-Dibromoethane (EDB)ug/L ND 0.50 12/20/23 13:33
1,2-Dichlorobenzene ug/L ND 0.50 12/20/23 13:33
1,2-Dichloroethane ug/L ND 0.50 12/20/23 13:33
1,2-Dichloropropane ug/L ND 0.50 12/20/23 13:33
1,3,5-Trimethylbenzene ug/L ND 0.50 12/20/23 13:33
1,3-Dichlorobenzene ug/L ND 0.50 12/20/23 13:33
1,3-Dichloropropane ug/L ND 0.50 12/20/23 13:33
1,4-Dichlorobenzene ug/L ND 0.50 12/20/23 13:33
2,2-Dichloropropane ug/L ND 0.50 12/20/23 13:33
2-Chlorotoluene ug/L ND 0.50 12/20/23 13:33
4-Chlorotoluene ug/L ND 0.50 12/20/23 13:33
Benzene ug/L ND 0.50 12/20/23 13:33
Bromobenzene ug/L ND 0.50 12/20/23 13:33
Bromochloromethane ug/L ND 0.50 12/20/23 13:33
Bromodichloromethane ug/L ND 0.50 12/20/23 13:33
Bromoform ug/L ND 0.50 12/20/23 13:33
Bromomethane ug/L ND 5.0 12/20/23 13:33
Carbon tetrachloride ug/L ND 0.50 12/20/23 13:33
Chlorobenzene ug/L ND 0.50 12/20/23 13:33
Chloroethane ug/L ND 1.0 12/20/23 13:33
Chloroform ug/L ND 0.50 12/20/23 13:33
Chloromethane ug/L ND 1.0 12/20/23 13:33
cis-1,2-Dichloroethene ug/L ND 0.50 12/20/23 13:33
cis-1,3-Dichloropropene ug/L ND 0.50 12/20/23 13:33
Dibromochloromethane ug/L ND 0.50 12/20/23 13:33
Dibromomethane ug/L ND 0.50 12/20/23 13:33
Dichlorodifluoromethane ug/L ND 0.50 12/20/23 13:33
Diisopropyl ether ug/L ND 0.50 12/20/23 13:33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4247144
Associated Lab Samples:92703972007, 92703972009, 92703972010
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 12/20/23 13:33
Hexachloro-1,3-butadiene ug/L ND 2.0 12/20/23 13:33
Isopropylbenzene (Cumene)ug/L ND 0.50 12/20/23 13:33
m&p-Xylene ug/L ND 1.0 12/20/23 13:33
Methyl-tert-butyl ether ug/L ND 0.50 12/20/23 13:33
Methylene Chloride ug/L ND 2.0 12/20/23 13:33
n-Butylbenzene ug/L ND 0.50 12/20/23 13:33
n-Propylbenzene ug/L ND 0.50 12/20/23 13:33
Naphthalene ug/L ND 2.0 12/20/23 13:33
o-Xylene ug/L ND 0.50 12/20/23 13:33
sec-Butylbenzene ug/L ND 0.50 12/20/23 13:33
Styrene ug/L ND 0.50 12/20/23 13:33
tert-Butylbenzene ug/L ND 0.50 12/20/23 13:33
Tetrachloroethene ug/L ND 0.50 12/20/23 13:33
Toluene ug/L ND 0.50 12/20/23 13:33
trans-1,2-Dichloroethene ug/L ND 0.50 12/20/23 13:33
trans-1,3-Dichloropropene ug/L ND 0.50 12/20/23 13:33
Trichloroethene ug/L ND 0.50 12/20/23 13:33
Trichlorofluoromethane ug/L ND 1.0 12/20/23 13:33
Vinyl chloride ug/L ND 1.0 12/20/23 13:33
1,2-Dichloroethane-d4 (S)%119 70-130 12/20/23 13:33
4-Bromofluorobenzene (S)%103 70-130 12/20/23 13:33
Toluene-d8 (S)%100 70-130 12/20/23 13:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4247145LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 19.620 98 60-140
1,1,1-Trichloroethane ug/L 22.820 114 60-140
1,1,2,2-Tetrachloroethane ug/L 22.720 113 60-140
1,1,2-Trichloroethane ug/L 22.020 110 60-140
1,1-Dichloroethane ug/L 25.120 125 60-140
1,1-Dichloroethene ug/L 23.720 119 60-140
1,1-Dichloropropene ug/L 26.120 130 60-140
1,2,3-Trichlorobenzene ug/L 18.920 94 60-140
1,2,3-Trichloropropane ug/L 21.720 108 60-140
1,2,4-Trichlorobenzene ug/L 18.020 90 60-140
1,2,4-Trimethylbenzene ug/L 22.520 112 60-140
1,2-Dibromo-3-chloropropane ug/L 19.920 99 60-140
1,2-Dibromoethane (EDB)ug/L 21.820 109 60-140
1,2-Dichlorobenzene ug/L 20.820 104 60-140
1,2-Dichloroethane ug/L 24.720 123 60-140
1,2-Dichloropropane ug/L 23.120 115 60-140
1,3,5-Trimethylbenzene ug/L 22.320 111 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 30 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4247145LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 20.620 103 60-140
1,3-Dichloropropane ug/L 21.920 110 60-140
1,4-Dichlorobenzene ug/L 20.620 103 60-140
2,2-Dichloropropane ug/L 22.320 112 60-140
2-Chlorotoluene ug/L 22.520 113 60-140
4-Chlorotoluene ug/L 23.220 116 60-140
Benzene ug/L 22.120 110 60-140
Bromobenzene ug/L 20.320 102 60-140
Bromochloromethane ug/L 22.820 114 60-140
Bromodichloromethane ug/L 21.420 107 60-140
Bromoform ug/L 17.920 90 60-140
Bromomethane ug/L 15.920 79 60-140
Carbon tetrachloride ug/L 19.720 98 60-140
Chlorobenzene ug/L 20.220 101 60-140
Chloroethane ug/L 22.920 114 60-140
Chloroform ug/L 23.820 119 60-140
Chloromethane ug/L 24.420 122 60-140
cis-1,2-Dichloroethene ug/L 24.820 124 60-140
cis-1,3-Dichloropropene ug/L 21.320 107 60-140
Dibromochloromethane ug/L 19.920 100 60-140
Dibromomethane ug/L 18.720 93 60-140
Dichlorodifluoromethane ug/L 20.720 103 60-140
Diisopropyl ether ug/L 24.420 122 60-140
Ethylbenzene ug/L 20.820 104 60-140
Hexachloro-1,3-butadiene ug/L 17.820 89 60-140
Isopropylbenzene (Cumene)ug/L 20.620 103 60-140
m&p-Xylene ug/L 42.740 107 60-140
Methyl-tert-butyl ether ug/L 22.820 114 60-140
Methylene Chloride ug/L 23.620 118 60-140
n-Butylbenzene ug/L 23.120 115 60-140
n-Propylbenzene ug/L 22.120 110 60-140
Naphthalene ug/L 19.920 99 60-140
o-Xylene ug/L 20.220 101 60-140
sec-Butylbenzene ug/L 21.720 108 60-140
Styrene ug/L 21.020 105 60-140
tert-Butylbenzene ug/L 16.820 84 60-140
Tetrachloroethene ug/L 17.720 89 60-140
Toluene ug/L 20.520 102 60-140
trans-1,2-Dichloroethene ug/L 26.120 131 60-140
trans-1,3-Dichloropropene ug/L 21.220 106 60-140
Trichloroethene ug/L 19.820 99 60-140
Trichlorofluoromethane ug/L 19.420 97 60-140
Vinyl chloride ug/L 21.220 106 60-140
1,2-Dichloroethane-d4 (S)%117 70-130
4-Bromofluorobenzene (S)%106 70-130
Toluene-d8 (S)%103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4247146MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92704235004
4247147
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 114 60-140138 1920ND22.9 27.6
1,1,1-Trichloroethane ug/L M12013960-140164 1620ND27.8 32.7
1,1,2,2-Tetrachloroethane ug/L M12012860-140153 1820ND25.6 30.6
1,1,2-Trichloroethane ug/L M12013060-140151 1520ND26.0 30.3
1,1-Dichloroethane ug/L M12015260-140177 1520ND30.3 35.3
1,1-Dichloroethene ug/L M12013660-140161 1720ND27.1 32.2
1,1-Dichloropropene ug/L M12015960-140187 1620ND31.7 37.4
1,2,3-Trichlorobenzene ug/L 20 104 60-140118 1320ND20.8 23.6
1,2,3-Trichloropropane ug/L M12012460-140146 1720ND24.8 29.3
1,2,4-Trichlorobenzene ug/L 20 105 60-140121 1420ND21.1 24.3
1,2,4-Trimethylbenzene ug/L M12013060-140154 1720ND25.9 30.8
1,2-Dibromo-3-chloropropane ug/L 20 112 60-140132 1720ND22.4 26.5
1,2-Dibromoethane (EDB)ug/L M12012560-140150 1820ND24.9 30.0
1,2-Dichlorobenzene ug/L 20 118 60-140138 1520ND23.6 27.6
1,2-Dichloroethane ug/L M12014560-140168 1520ND28.9 33.6
1,2-Dichloropropane ug/L M12014060-140164 1620ND28.0 32.9
1,3,5-Trimethylbenzene ug/L M12012760-140150 1720ND25.5 30.1
1,3-Dichlorobenzene ug/L 20 118 60-140139 1620ND23.5 27.7
1,3-Dichloropropane ug/L M12012760-140152 1720ND25.4 30.3
1,4-Dichlorobenzene ug/L 20 116 60-140136 1620ND23.2 27.2
2,2-Dichloropropane ug/L M12013760-140164 1820ND27.5 32.8
2-Chlorotoluene ug/L M12013260-140153 1520ND26.5 30.7
4-Chlorotoluene ug/L M12013260-140155 1620ND26.3 31.0
Benzene ug/L M12013260-140154 1520ND26.4 30.8
Bromobenzene ug/L 20 115 60-140137 1720ND23.1 27.4
Bromochloromethane ug/L M12013660-140159 1520ND27.3 31.8
Bromodichloromethane ug/L M12012660-140148 1620ND25.2 29.6
Bromoform ug/L 20 102 60-140122 1820ND20.4 24.3
Bromomethane ug/L 20 75 60-14087 1520ND15.1 17.5
Carbon tetrachloride ug/L 20 119 60-140140 1620ND23.8 28.0
Chlorobenzene ug/L M12011960-140141 1720ND23.7 28.1
Chloroethane ug/L 20 113 60-140128 1220ND22.7 25.6
Chloroform ug/L M12013760-140169 2020ND27.5 33.7
Chloromethane ug/L 20 99 60-140115 1520ND19.8 23.0
cis-1,2-Dichloroethene ug/L M12015360-140174 1320ND30.5 34.9
cis-1,3-Dichloropropene ug/L M12012660-140147 1520ND25.2 29.4
Dibromochloromethane ug/L 20 115 60-140138 1920ND22.9 27.7
Dibromomethane ug/L 20 111 60-140126 1320ND22.2 25.3
Dichlorodifluoromethane ug/L M1204660-14056 1820ND9.3 11.2
Diisopropyl ether ug/L M12014960-140175 1620ND29.9 35.1
Ethylbenzene ug/L M12012260-140146 1820ND24.4 29.2
Hexachloro-1,3-butadiene ug/L 20 106 60-140130 2020ND21.3 26.1
Isopropylbenzene (Cumene)ug/L M12012360-140147 1820ND24.6 29.4
m&p-Xylene ug/L M14012360-140147 1840ND49.4 58.9
Methyl-tert-butyl ether ug/L M12013460-140157 1520ND26.8 31.3
Methylene Chloride ug/L M12014260-140163 1420ND28.4 32.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4247146MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92704235004
4247147
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L M12013560-140162 1820ND27.0 32.5
n-Propylbenzene ug/L M12012960-140152 1720ND25.7 30.5
Naphthalene ug/L 20 111 60-140130 1520ND22.3 25.9
o-Xylene ug/L M12011860-140142 1920ND23.5 28.3
sec-Butylbenzene ug/L M12012860-140153 1720ND25.7 30.6
Styrene ug/L M12012460-140148 1820ND24.7 29.7
tert-Butylbenzene ug/L 20 100 60-140120 1820ND20.0 24.0
Tetrachloroethene ug/L 20 105 60-140126 1820ND21.0 25.1
Toluene ug/L M12012360-140143 1520ND24.5 28.6
trans-1,2-Dichloroethene ug/L M12015860-140185 1620ND31.6 36.9
trans-1,3-Dichloropropene ug/L M12012760-140150 1720ND25.4 30.0
Trichloroethene ug/L 20 119 60-140139 1520ND23.8 27.8
Trichlorofluoromethane ug/L 20 103 60-140124 1820ND20.6 24.8
Vinyl chloride ug/L 20 97 60-140115 1720ND19.3 22.9
1,2-Dichloroethane-d4 (S)%117 70-130117
4-Bromofluorobenzene (S)%106 70-130108
Toluene-d8 (S)%103 70-130103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 37
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
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Huntersville, NC 28078
[phone]
Page 34 of 37
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92703972
TERRELL BAIT SHOP
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92703972001 820288MW-1 SM 6200B
92703972002 820288MW-2 SM 6200B
92703972003 820288MW-4 SM 6200B
92703972004 820288MW-6 SM 6200B
92703972005 820288MW-7 SM 6200B
92703972006 820288MW-8 SM 6200B
92703972007 820540MW-10 SM 6200B
92703972008 820288MW-11 SM 6200B
92703972009 820540MW-12 SM 6200B
92703972010 820540MW-16 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2023 03:32 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 37
Page 36 of 37
Page 37 of 37

Appendix B

Figures

LEGEND
Site
1
FIGUREDrawing Path: X:\GIS\Asheville Projects\Terrell Bait Shop\Figures.mxd plotted by kelsey.cahill 07-19-2022
REFERENCE:ESRI WORLD STREET BASEMAP
SITE LOCATION MAPTERRELL BAIT SHOP7970 NC 150, TERRELLCATAWBA COUNTY, NORTH CAROLINA
500 0 500 1,000250
APPROXIMATE SCALE IN FEET
DATE:
JOB NO:CHECKED:
DRAWN:
APPROVED:DRLKLC
DRL J22-17256-017-19-22
!
LEGEND
Site
2
FIGUREDrawing Path: X:\GIS\Asheville Projects\Terrell Bait Shop\Figures.mxd plotted by kelsey.cahill 07-19-2022
REFERENCE:NGMDB.USGS.GOV/TOPOVIEWLAKE NORMAN NORTH, NC QUADRANGLE - 2019
USGS TOPOGRAPHIC MAPTERRELL BAIT SHOP7970 NC 150, TERRELLCATAWBA COUNTY, NORTH CAROLINA
500 0 500 1,000250
APPROXIMATE SCALE IN FEET
DATE:
JOB NO:CHECKED:
DRAWN:
APPROVED:DRLKLC
DRL J22-17256-017-19-22
!
@A
@A
@A
@A
@A
@A
@A
@A
@A
@A
@A
@A
@A
@A
@A
@A
@A
@A
@A
@A
@A
@A
@A
@A
@A@AAS-2
AS-1MW-3
TS-8
MW-1
MW-2
MW-4
MW-5
MW-6
MW-7
MW-8
MW-9
SVE-2
SVE-1
DMW-1
MW-17
MW-16
MW-18
TS-11
MW-10
MW-11
MW-12
MW-13
MW-14
MW-15
LEGEND
@A Air Sparge Well
@A Groundwater Monitoring Well
@A Soil Vapor Extraction Well
Approximate Former UST LocationsSite
3
FIGUREDrawing Path: X:\GIS\Asheville Projects\Terrell Bait Shop\Aerial.mxd plotted by kelsey.cahill 07-19-2022
REFERENCE:NCONEMAP.GOV - 2018 AERIAL PHOTOGRAPHNOTES:BUILDING IS NO LONGER PRESENT ON-SITE
SITE MAPTERRELL BAIT SHOP7970 NC 150, TERRELLCATAWBA COUNTY, NORTH CAROLINA
30 0 30 6015
APPROXIMATE SCALE IN FEET
DATE:
JOB NO:CHECKED:
DRAWN:
APPROVED:DRLKLC
DRL J22-17256-017-19-22
!

Appendix C

Tables
Manifold
Pressure
(psi)
Well Head
Pressure
(psi)
Flow
(SCFM)
Manifold
Pressure
(psi)
Well Head
Pressure
(psi)
Flow
(SCFM)
Manifold
Pressure
(psi)
Well Head
Pressure
(psi)
Flow
(SCFM)
7/28/2023 19549.30 On NA 9,513.0 On NA 49 not checked 7.0 52 not checked 7.0 50 not checked 7.0
Stopped compressor, checked oil level - added oil back to max line.
Restarted air compressor. Confirmed automatic bowl drain valve is
working. Checked moisture K/O drum - no water. **6/28/2023 -
added condensate drain hose from manifold piping to condensate catch
bucket to stop oil smear flow meters - (working)
8/11/2023 19884.18 On 100%9,848.0 On 100%50 not checked 7.5 53 not checked 7.0 51 not checked 7.0 Confirmed tank condensate trap drain is working. Confirmed automatic
bowl drain valve is working. Checked moisture K/O drum - no water.
8/30/2023 20337.59 On 99%10,301.0 On 99%53 not checked 7.0 54 not checked 7.0 54 not checked 7.0 Confirmed tank condensate trap drain is working. Confirmed automatic
bowl drain valve is working. Checked moisture K/O drum - no water.
Checked SVE blower gearbox oil leve, greased drive-end bearings
9/16/2023 20745.33 On 100%10,710.0 Off 100%53 not checked 7.5 52 not checked 7.0 52 not checked 7.0 Confirmed tank condensate trap drain is working. Confirmed automatic
bowl drain valve is working. Checked moisture K/O drum - no water.
9/26/2023 20985.32 On 100%10,950.0 On 100%54 not checked 7.0 56 not checked 7.0 56 not checked 7.0 Confirmed tank condensate trap drain is working. Confirmed automatic
bowl drain valve is working. Checked moisture K/O drum - no water.
9/28/2023 21033.27 On 100%10,950.0 On 0%55 not checked 7.0 56 not checked 7.0 56 not checked 7.0 Collected 1 liter tedlar bag sample of SVE blower exhaust - sample
timie 1115
10/23/2023 21634.08 On 100%11,599.0 On 108%53 not checked 7.0 53 not checked 7.5 52 not checked 8.0
Removed air flow meters for AS-1, 2, 3 - cleaned (not showing oil as
before due to adding drain hose from manifold piping to catch bucket).
No water in SVE moisture separator drum. Compressor service due.
11/9/2023 22044.19 On 101%12,009.0 On 100%53 not checked 7.5 51 not checked 7.5 52 not checked 8.0
Compressor temperature at 203 deg, used compressed air to blow off
air/oil cooler until service scheduled. No water in moisture separator
K/O drum. Compressor service due.
11/28/2023 22497.53 On 99%12,462.0 On 99%57 not checked 7.0 54 not checked 7.5 56 not checked 8.0
Water in moisture separator drum approximately 1 inches from high
level float. Pressure regulator stuck bleeding air, removed and cleaned
stem and seat - regulator seals. Increased vacuum to try and fill last 1
inch of water to test system shutdown, draining and restart -
unsuccessful. Compressor service due.
12/13/2023 22858.21 On 100%12,823.0 On 100%53 not checked 7.0 54 not checked 7.5 54 not checked 7.5 Water in moisture separator drum at Low level. Took flow, temp and
%RH at blower exhaust - collected one Tedlar bag air sample (SVE-1
@ 1220). Compressor Service past due.
12/23/2023 23101.03 On 101%13,065.0 On 101%56 not checked 7.5 55 not checked 7.5 57 not checked 8.0
Water in moisture separator drum above high level float. Issue with
low level float, need to remove float tree and check float. Shut down
SVE system and allowed moisture separator to drain; restarted SVE
system. Compressor service past due.
12/31/2023 23295.03 On 101%13,259.0 On 101%57 not checked 7.5 54 not checked 7.0 58 not checked 8.0
Water in moisture separator drum above high level float. Issue with
low level float, need to remove float tree and check float. Shut down
SVE system and allowed moisture separator to drain; restarted SVE
system. Compressor service past due.Total 100%100%
Notes:
psi = pounds per square inch
SCFM = standard cubic feet per minute
- = no data
* Adjusted runtime was prepared as a result of the PLC timer reporting incorrect values
TABLE 1
System Operational Data
7970 NC Highway 150
Terrell, Catawba County, North Carolina
BLE Project No. J22-17256-01
Sparge Well AS-2 Sparge Well AS-3Air
Compressor
Run Time
(hours)
Air Sparge
On/Off CommentsDate
SVE %
Run Since
Previous
Visit
Air Sparge %
Run Since
Previous Visit
Sparge Well AS-1
SVE
On/Off
SVE Run
Time
(hours)
Adjusted
SVE
Timer
(hours)*
1 of 1
STACK DATA
Sample ID Date
Collected
SVE Effluent 09/28/23 2,310 21,100 6,160 25,420 <7.21 272,000
SVE Effluent 12/13/23 17,300 104,000 30,500 97,300 <72.1 1,930,000
AVERAGE 9,805.0 62,550.0 18,330.0 61,360.0 39.7 1,101,000
DRY STANDARD CUBIC FEET PER MINUTE (DSCFM) AIR FLOW CALCULATIONS (Qstd)
Vacuum Velocity Pipe ID Temp Temp Rel Humid Water Qstd
(in-Hg)(ft/min)(in)(°F)(°K)(%/100)Vapor (%)(DSCFM)
09/28/23 3.2 3,573 2 91.9 306 0.416 0.0133 73.6
12/13/23 3.5-4.0 2,070 2 77.6 298 0.391 0.0079 44.0
AVERAGE 58.8
MASS REMOVAL RATE AND TOTAL MASS REMOVED
Start Date 06/28/23 18,830 hours
End Date 12/31/23 23,295 hours
% Run 100%
Total Run Time (hrs)4,466
Analyte
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
To
t
a
l

X
y
l
e
n
e
s
MT
B
E
TP
H
-
G
R
O
Mass Removal Rate (kg/hr)9.79E-04 6.25E-03 1.83E-03 6.13E-03 3.96E-06 1.10E-01
Total Mass Removed (kg)4.37E+00 2.79E+01 8.18E+00 2.74E+01 1.77E-02 4.91E+02
Total Mass Removed (lbs)9.64 61.50 18.02 60.33 0.04 1,082.56
NOTES:
µg/m3 = Micrograms per cubic meter
Qstd = Flow at dry standard cubic feet per minute (DSCFM)
Vacuum = The level of vacuum being applied should be recorded from the vacuum truck tank (inches of Hg)
Velocity = The rate at which air flows is measured at the blower discharge piping (anemometer or pitot tube)
Pipe ID = The inside diameter of the blower discharge piping (from the vacuum truck)
Temperature = The temperature of the air stream exiting the blower discharge piping (dry bulb temp., in deg.°F)
Relative humidity = The % relative humidity of the air stream exiting the blower discharge piping
Water Vapor in % = Pounds of water per pound of dry air, derived from the Psychrometric chart (temp Vs relative humidity)
MT
B
E
TP
H
-
G
R
O
Date
TABLE 2
Analytical Method
Contaminant of Concern
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
To
t
a
l

X
y
l
e
n
e
s
Mass Removal Via Vapor
7970 NC Highway 150
Terrell, Catawba County, North Carolina
BLE Project No. J22-17256-01
EPA Method 18 Target Compounds
(mg/m3)
Date
1.0 - 5,000 5,000 - 10,000 10,000 1.0 - 5,000 5,000 - 10,000 10,000
3,774 2,013 1,121 94,350 50,325 28,025
1.0 - 5,000 5,000 - 10,000 10,000 1.0 - 10 10 - 100 100 - 1,000
4,154 356 342 103,850 8,900 8,550
1.0 - 1,000 1,000 1.0 - 1,000 1,000
2,587 240 64,675 6,000
1.0 - 1,000 1,000 1.0 - 1,000 1,000
1,883 307 47,075 7,675
1.0 - 26 1.0 - 26
2,387 59,675
Date Total Mass
(kg)
Total Mass
(lbs)
2,500 7,500 10,000
2.00 3.21 2.38
2,500 7,500 10,000
2.21 0.57 0.73
500 1,000
0.27 0.05
500 1,000
0.20 0.07
13
0.01
Notes:
0.01 0.01December 2023
May 2023 0.27 0.58
November 2022 0.33 0.72
Surface Area between Contours (ft2)Area (ft2) x Depth of Contamination* (ft) = Volume (ft3)
Between Contours
December 2021
June 2022
Volume (ft3) Between Contours x Average
Contamination Concentration (mg/L) x 30%
Porosity
November 2022
May 2023
December 2023
December 2021 7.59 16.73
June 2022 3.50 7.71
TABLE 3
Contaminant Mass Estimate as Benzene
7970 NC Highway 150
Terrell, Catawba County, North Carolina
BLE Project No. J22-17256-01

Appendix D

Laboratory Analytical Report

#=CL#
December 21, 2023
LIMS USE: FR - DAVID LOFTIS, PE
LIMS OBJECT ID: 92703549
92703549
Project:
Pace Project No.:
RE:
David R. Loftis, PE
Bunnell Lammons Engineering
30 Park Ridge Drive
Fletcher, NC 28732
TERRELL BAIT SHOP / 17526-01
Dear David Loftis, PE:
Enclosed are the analytical results for sample(s) received by the laboratory on December 13, 2023. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
704-977-0943
Enclosures
cc:Jennipher Von Stauffenberg, Bunnell-Lammons
Engineering
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 10
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92703549
TERRELL BAIT SHOP / 17526-01
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 10
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92703549
TERRELL BAIT SHOP / 17526-01
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92703549001 SVE-1 Method 18 Air MeOH & EtOH 8 PANDAH, MNP,
SDS
PAN = Pace National - Mt. Juliet
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 10
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92703549
TERRELL BAIT SHOP / 17526-01
Sample:SVE-1 Lab ID:92703549001 Collected:12/13/23 12:20 Received:12/13/23 13:12 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: Method 18 Air MeOH & EtOH Preparation Method: M18-Mod
Pace National - Mt. Juliet
VOA (MS) M18-Mod
Benzene 17300 ug/m3 12/15/23 03:54 71-43-212/15/23 03:5463.9 100
Toluene 104000 ug/m3 12/20/23 21:37 108-88-3 H112/20/23 21:37942500
Ethylbenzene 30500 ug/m3 12/15/23 03:54 100-41-412/15/23 03:5486.7 100
m&p-Xylene 59400 ug/m3 12/19/23 17:33 179601-23-1 H112/19/23 17:33173100
o-Xylene 37900 ug/m3 12/15/23 03:54 95-47-612/15/23 03:5486.7 100
Methyl-tert-butyl ether ND ug/m3 12/15/23 03:54 1634-04-412/15/23 03:5472.1 100
Gasoline Range Organics 1930000 ug/m3 12/19/23 17:33 8006-61-9 H112/19/23 17:3382600100
Surrogates
4-Bromofluorobenzene (S)99.4 %12/15/23 03:54 460-00-412/15/23 03:5460.0-140 100
4-Bromofluorobenzene (S)103 %12/19/23 17:33 460-00-412/19/23 17:3360.0-140 100
4-Bromofluorobenzene (S)104 %12/20/23 21:37 460-00-412/20/23 21:3760.0-140 500
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/21/2023 10:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 10
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92703549
TERRELL BAIT SHOP / 17526-01
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2189603
M18-Mod/TO-15
Method 18 Air MeOH & EtOH
VOA (MS) M18-Mod
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92703549001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R4014136-3
Associated Lab Samples:92703549001
Matrix:Air
Analyzed
Benzene ug/m3 ND 0.639 12/14/23 15:17
Ethylbenzene ug/m3 ND 0.867 12/14/23 15:17
o-Xylene ug/m3 ND 0.867 12/14/23 15:17
Methyl-tert-butyl ether ug/m3 ND 0.721 12/14/23 15:17
4-Bromofluorobenzene (S)%95 60.0-140 12/14/23 15:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R4014136-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R4014136-2
Benzene ug/m3 13.412.0 112 70.0-13011413.6 1.18 25
Ethylbenzene ug/m3 19.016.3 117 70.0-13011618.9 0.458 25
o-Xylene ug/m3 18.816.3 116 70.0-13011418.5 1.63 25
Methyl-tert-butyl ether ug/m3 15.313.5 113 70.0-13011315.3 0.236 25
4-Bromofluorobenzene (S)%97.4 60.0-14097.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/21/2023 10:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 10
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92703549
TERRELL BAIT SHOP / 17526-01
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2192042
M18-Mod/TO-15
Method 18 Air MeOH & EtOH
VOA (MS) M18-Mod
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92703549001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R4014253-3
Associated Lab Samples:92703549001
Matrix:Air
Analyzed
m&p-Xylene ug/m3 ND 1.73 12/19/23 10:01
Gasoline Range Organics ug/m3 ND 826 12/19/23 10:01
4-Bromofluorobenzene (S)%99.6 60.0-140 12/19/23 10:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R4014253-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R4014253-2
m&p-Xylene ug/m3 33.632.5 103 70.0-13010534.2 1.79 25
Gasoline Range Organics ug/m3 847777 109 70.0-130109847 0.00 25
4-Bromofluorobenzene (S)%103 60.0-140103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/21/2023 10:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 10
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92703549
TERRELL BAIT SHOP / 17526-01
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2193017
M18-Mod/TO-15
Method 18 Air MeOH & EtOH
VOA (MS) M18-Mod
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92703549001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R4015131-2
Associated Lab Samples:92703549001
Matrix:Air
Analyzed
Toluene ug/m3 ND 1.88 12/20/23 09:50
4-Bromofluorobenzene (S)%101 60.0-140 12/20/23 09:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R4015131-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R4015131-3
Toluene ug/m3 14.814.1 105 70.0-13010414.7 0.255 25
4-Bromofluorobenzene (S)%103 60.0-14099.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/21/2023 10:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 10
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92703549
TERRELL BAIT SHOP / 17526-01
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analysis conducted outside the recognized method holding time.H1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/21/2023 10:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 10
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92703549
TERRELL BAIT SHOP / 17526-01
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92703549001 2189603 2189603SVE-1 M18-Mod Method 18 Air MeOH &
EtOH
92703549001 2192042 2192042SVE-1 M18-Mod Method 18 Air MeOH &
EtOH
92703549001 2193017 2193017SVE-1 M18-Mod Method 18 Air MeOH &
EtOH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/21/2023 10:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 10
Page 10 of 10