MO-8561_40099_CA_MRP_20240104

January 5, 2024

Johanna Moats
AP / AR Coordinator

Enclosure

Cc: Mr. Matthew Redmond; Raymer Oil Company, file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Geological Resources, Inc.
Sincerely,
please contact Ashleigh Thrash at 704-845-4010.
Please find enclosed the referenced report for the above-mentioned site. If you have any questions, Dear Mr. Newton,
GRI Project Number: 5398
Incident Number: 40099
Facility ID Number: 00-0-0000036548
North Carolina
Newton, Catawba County
2443 NC Highway 10 West
Fast Track #145 October - December 2023
Re: Ground Water Monitoring Report
Mooresville, North Carolina 28115
610 East Center Ave.
Mooresville Regional Office
NCDEQ-UST Section
Mr. Brad Newton

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone] Engineering
Certification: C-2727 • Geology Certification: C-127

Ground Water Monitoring Report
October - December 2023
Fast Track #145
2443 NC Highway 10 West
Newton, Catawba County
North Carolina
Facility ID Number: 00-0-0000036548
Incident Number: 40099
GRI Project Number: 5398

Prepared for:

Mr. Matthew Redmond
Raymer Oil Company
P.O. Box 327
Troutman, North Carolina 28166

January 4, 2024

Eric M. Eubanks, P.G.
Report Writer
Ashleigh Thrash, P.G.
Project Manager

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 4, 2024 Fast Track #145
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5398
i
SITE INFORMATION
1. Site Identification
 Fast Track #145 (Facility ID 00-0-0000036548)
 Incident Number 40099 – Intermediate Risk (I125D)
 Location of Source Area: 2443 NC Highway 10 West
Newton, NC 28658
Catawba County
35.644579°N, 81.268800°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST Owner
Fast Track Inc.
P.O. Box 410
Wilkesboro, NC 28697
Email Unknown
336-838-4000

UST Operator
Raymer Brothers, Inc.
P.O. Box 327
Troutman, NC 28166
[e-mail]
704-873-7285

Property Owner
KLR Real Estate, LLC.
589 North Main Street
Troutman, NC 28166
Email Unknown
Phone No. Unknown

Property Occupant
Valero/Fast Phil’s #145
2443 NC Highway 10 West
Newton, NC 28658
Email Unknown
828-466-0161

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
Waypoint Analytical
4449 Springbrook Road
Charlotte, NC 28217
State Certification No.
37735/402
704-529-6364
3. Information about Release
 Release was discovered on July 5, 2012
 An unknown amount of product was released from the leaking UST System
 Currently, one 12,000-gallon gasoline UST, one 8,000-gallon gasoline UST, and one 5,000-gallon
diesel UST and associated pumps and product piping are active at the site.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 4, 2024 Fast Track #145
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5398
ii
EXECUTIVE SUMMARY
Fast Track #145 is located at 2443 NC Highway 10 West in Newton, Catawba County, North Carolina. The
site is currently owned by KLR Real Estate, LLC. and is operated by Raymer Brothers, Inc. as a petroleum
retail facility. In May 2020, Raymer Oil Company became the responsible party for incident 40099. A
release was discovered during a Phase II ESA conducted in July 2012. Currently, one 12,000-gallon gasoline
UST, one 8,000-gallon gasoline UST, and one 5,000-gallon diesel UST and associated pumps and product
piping are active at the site. The adjoining properties are a mixture of residential and commercial
properties. According to the information determined during 2012 receptor survey activities, six active
potable water supply wells were identified within a 1,000- foot radius of the site. Public water is available
to the site and surrounding properties within a 1,500-foot radius of the site.

The November 2014 CAP submitted by Paragon Environmental Consultants, Inc. proposed connecting the
residences with potable water supply wells to municipal water and reducing contaminant concentrations
to below GCLs at the site using MMPE events in combination with a dual-phase extraction and air sparging
system. In accordance with the March 2021 remediation system design, an AS/SVE system was installed
at the site and started on March 17, 2023. Additionally, several MMPE events have been conducted at
the site.

O&M site visits were conducted on October 30, November 21, and December 11, 2023. Hour meter,
system vacuum, pressure, air flow, temperature, AS well pressure, and SVE well vacuum readings were
collected during each site visit.

On December 11, 2023, ten Type II monitoring wells were gauged, purged, and sampled. Free product
was not observed during the December 2023 gauging activities. The concentrations of benzene, toluene,
ethylbenzene, xylenes, MTBE, naphthalene, 2-hexanone, isopropylbenzene, n-propylbenzene, styrene,
1,2,4-trimethylbenzene, and/or 1,3,5-trimethylbenzene reported in the ground water samples collected
from MW-1, MW-3, MW-4, MW-6, MW-8, MW-9, MW-14, MW-15, and MW-17 exceeded the MACs. The
concentrations of benzene, toluene, ethylbenzene, xylenes, and/or naphthalene reported in the ground
water samples collected from MW-1, MW-4, MW-6, MW-8, MW-14, and MW-17 exceeded 10 times the
2B Standards. The concentrations of benzene reported in the ground water samples collected from MW-
4 and MW-6 exceeded the GCL.

Calculations based on the December 2023 ground water sampling event indicate that the contaminant
mass has decreased by 7.1%, 86.8%, and 87.9% in Areas 1, 2, and 3, respectively, when compared to the
baseline sampling event. The overall contaminant mass at the site has decreased by approximately 24.5%
from the baseline event to the December 2023 sampling event.

Based on this information, the risk classification for the site should remain Intermediate. GRI recommends
the continued operation of the remediation system until contaminant concentrations have been reduced
to below 10 times the 2B Standards.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 4, 2024 Fast Track #145
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5398
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
PRM: Product Recovery Management, Inc.
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 4, 2024 Fast Track #145
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5398
TABLE OF CONTENTS
SITE INFORMATION ............................................................................................................................ i
EXECUTIVE SUMMARY ....................................................................................................................... ii
ACRONYMS ....................................................................................................................................... iii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................3
3.0 FREE PRODUCT REMOVAL ........................................................................................................4
4.0 REMEDIATION SYSTEM ............................................................................................................4
5.0 AIR SAMPLING.........................................................................................................................5
6.0 GROUND WATER REMEDIATION ..............................................................................................6
7.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................8
8.0 CONCLUSIONS .........................................................................................................................8
9.0 LIMITATIONS ...........................................................................................................................8
10.0 STATEMENTS AND CERTIFICATION ...........................................................................................9

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Site Vicinity Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map
Figure 6: Benzene Isoconcentration Map
Figure 7: Toluene Isoconcentration Map
Figure 8: Ethylbenzene Isoconcentration Map
Figure 9: Xylenes Isoconcentration Map
Figure 10: Naphthalene Isoconcentration Map
Figure 11: Remediation Well Location Map
Figure 12: Estimated Contaminant Mass Area Map

TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Water Supply Well Information
Table 4: Adjacent Property Owner Information
Table 5: Well Construction and Gauging Information
Table 6: Summary of Ground Water Sample Analytical Results
Table 7: Summary of Remediation System O&M Visits
Table 8: Summary of Air Analytical Results

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 4, 2024 Fast Track #145
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5398

APPENDICES
Appendix A: State Correspondence
Appendix B: Land Use Information
Appendix C: Incident Reports
Appendix D: Historical Soil Quality Information
Appendix E: Laboratory Analytical Reports
Appendix F: O&M Field Data Sheets
Appendix G: Overall Remediation Costs
Appendix H: Contaminant Mass Calculations

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 4, 2024 Fast Track #145
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5398
1
1.0 SITE HISTORY AND CHARACTERIZATION
GRI presents the results of the October through December 2023 O&M activities and the December 2023
ground water sampling event at the Fast Track #145 site, located at 2443 NC Highway 10 West in Newton,
Catawba County, North Carolina. These activities were conducted in accordance with GRI Proposal No.
23-634, which was submitted to the NCDEQ on September 28, 2023, and approved as Task Authorization
No. 40099-25 on September 29, 2023. A topographical map showing the location of the site is included as
Figure 1. State correspondence is included as Appendix A.

The site is currently owned by KLR Real Estate, LLC and is operated by Raymer Brothers, Inc. as a petroleum
retail facility. In May 2020, Raymer Oil Company became the responsible party for Incident 40099. A
release was discovered during a Phase II ESA conducted in July 2012. Currently, one 12,000-gallon gasoline
UST, one 8,000-gallon gasoline UST, and one 5,000-gallon diesel UST and associated pumps and product
piping are active at the site. UST owner/operator information and UST system information are included
in Tables 1 and 2, respectively. The Registered Tank Report is shown below:

The site and surrounding area are a mixture of residential and commercial properties. A copy of the Land
Use table is included as Appendix B. The site contains one building (the store) and is primarily capped
with concrete and asphalt. The overall topography at the site is relatively flat; the eastern portion of the
site slopes eastward towards an unnamed creek, located approximately 250 feet east of the source area.
Seventeen Type II monitoring wells (MW-1 through MW-17) were installed at the site during previous
ground water assessment activities. A Site Map showing the locations of the monitoring wells and the
structures on-site is included as Figure 2.

A receptor survey was conducted at the site by Paragon Environmental Consultants, Inc. (Paragon) in July
2012. Fourteen water supply wells were identified within a 1,000-foot radius of the site. Six of the fourteen
water supply wells (WSW-3, WSW-4, WSW-7, WSW-11, WSW-12, and WSW-14) identified were
determined to be active potable wells. According to available information, the six residences with potable
water supply wells were connected to municipal water and as a result, the site’s risk classification was

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 4, 2024 Fast Track #145
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5398
2
lowered by the NCDEQ to Intermediate in January 2016. Municipal water is available to the site and
surrounding properties. Two branches of an unknown tributary are located within a 500-foot radius of the
site. Water supply well information is included in Table 3. Adjacent property owner information is
included in Table 4. A Site Vicinity Map showing the adjacent properties and a Zoning Map showing the
zoning information are included as Figures 3A and 3B, respectively.

Please note that the historical information contained in this report was obtained under the supervision of
the previous consultants. Although GRI cannot verify the accuracy of the information obtained by
previous consultants, for the purpose of this report it is assumed to be correct, and any inferences or
interpretations made by GRI based on data that may be incorrect are not the responsibility of GRI. Please
refer to earlier submittals for additional information regarding previous assessment activities.

One additional incident (Incident No. 22431) was reported on the site. Based on the NCDEQ Incident
Report, it does not appear that this incident was assessed. One incident (Incident No. 10359) was
reported on an adjacent property. These incidents have both been closed. Copies of the NCDEQ Incident
Reports are included as Appendix C. A map showing the locations of additional incidents in the vicinity of
the site is shown below:

On November 18, 2014, Paragon submitted a CAP that proposed to reduce contaminant concentrations
using MMPE events in combination with dual-phase extraction and air sparging system. To date, several
MMPE events have been conducted at the site. No projected milestones were established in the CAP. In
March 2021, GRI submitted a remediation system design to implement the 2014 CAP. In accordance with
40099
22431
10359

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 4, 2024 Fast Track #145
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5398
3
the system design, an AS/SVE remediation system was installed at the site and was started on March 17,
2023. The remediation system is currently in operation.

Based on the presence of surface water and contaminant concentrations exceeding 10 times the 2B
standards, the risk classification should remain intermediate risk.
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
Soil assessment was not conducted during the current scope of work. Historical soil quality information
from previous consultants is included as Appendix D.

On December 11, 2023, ten Type II monitoring wells (MW-1, MW-3, MW-4, MW-6, MW-8, MW-9, MW-
10, MW-14, MW-15, and MW-17) were gauged, purged, and sampled. A surface water sample was not
collected from the creek adjacent to the site because the water was stagnant from recent rainfall and was
not a representative sample of typical surface water conditions in the creek. Free product was not
observed during the December 2023 gauging activities. Depths to ground water in the Type II monitoring
wells ranged from 2.02 feet to 32.05 feet below TOC. Ground water elevations in the Type II monitoring
wells relative to an arbitrary datum of 100.00 feet ranged from 52.82 feet to 74.36 feet. Ground water
flow between MW-14 and MW-15 was generally to the east with an average horizontal gradient of
approximately 0.06 feet per foot. The vertical gradient was not calculated. Well construction and gauging
information is included in Table 5. A Water Table Surface Map based on the Type II monitoring wells is
included as Figure 4. A summary of the current ground water gauging data is shown below:

Well ID
Screened
Interval (x
to y ft. BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
MW-1 25-45 45 97.81 32.05 --- 65.76
MW-3 19-39 39 100.00 25.64 --- 74.36
MW-4 4-19 19 66.37 8.01 --- 58.36
MW-6 16-36 36 100.50 27.76 --- 72.74
MW-8 17-37 37 98.64 25.63 --- 73.01
MW-9 3-13 13 55.86 2.02 --- 53.84
MW-10 3-13 13 58.47 3.43 --- 55.04
MW-14 16-36 36 98.93 28.06 --- 70.87
MW-15 4-14 14 55.44 2.62 --- 52.82
MW-17 10-35 35 97.75 27.97 --- 69.78

Ground water samples collected from the monitoring wells were submitted for laboratory analyses of
VOCs by EPA Method 6200B. The concentrations of benzene, toluene, ethylbenzene, xylenes, MTBE,
naphthalene, 2-hexanone, isopropylbenzene, n-propylbenzene, styrene, 1,2,4-trimethylbenzene, and/or
1,3,5-trimethylbenzene reported in the ground water samples collected from MW-1, MW-3, MW-4, MW-
6, MW-8, MW-9, MW-14, MW-15, and MW-17 exceeded the MACs. The concentrations of benzene,
toluene, ethylbenzene, xylenes, and/or naphthalene reported in the ground water samples collected from

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 4, 2024 Fast Track #145
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5398
4
MW-1, MW-4, MW-6, MW-8, MW-14, and MW-17 exceeded 10 times the 2B Standards. The
concentrations of benzene reported in the ground water samples collected from MW-4 and MW-6
exceeded the GCL. A summary of the analytical results for ground water samples collected on December
11, 2023, is included in Table 6. A Ground Water Quality Map based on the December 2023 data is
included as Figure 5. Isoconcentration maps for all contaminants that exceeded 10 times the 2B Standards
are included as Figure 6 through Figure 10. A telescoping well has not been installed at the site; therefore,
cross sections have not been included. A complete report of laboratory analyses of the ground water
samples collected from the monitoring wells during the December 2023 sampling event is included in
Appendix E. A summary of the current ground water analytical data is shown below:

Contaminant of Concern 
Be
n
z
e
n
e

To
l
u
e
n
e

Et
h
y
l
b
e
n
z
e
n
e

Xy
l
e
n
e
s

MT
B
E

Na
p
h
t
h
a
l
e
n
e

Well ID
MACs (µg/l) 1 600 600 500 20 6
GCL (µg/l) 5,000 260,000 80,000 50,000 20,000 6,000
10 x 2B Standard (µg/l) 510 110 1,300 6,700 15,000 120
MW-1 3,380 6,810 832 4,290 <14.0 302
MW-3 17.3 1.65 0.608 4.13 0.413 J 4.57
MW-4 6,770 1,470 2,900 4,140 91.7 J 655
MW-6 10,200 39,500 3,280 15,500 <14.0 824
MW-8 <1.80 21.8 12.7 94.7 <1.40 466
MW-9 17.1 2.57 5.77 0.752 0.733 J 2.26
MW-10 <0.180 <0.220 <0.170 <0.210 0.459 J <0.470
MW-14 241 1,130 158 759 <0.140 <0.470
MW-15 179 12.1 20.3 17.9 J 5.42 J <4.70
MW-17 2.90 J 24.3 9.27 59.2 <1.40 239

A laboratory supplied trip blank was submitted with the ground water samples for analysis of VOCS by
EPA Method 6200B. No detectable concentrations of requested method constituents were reported in
the trip blank.

The site is in the Piedmont Physiographic Province of North Carolina. The seasonal high water table at the
site was observed in June 2021 and had a depth to water of approximately twenty to twenty-four feet
BGS.
3.0 FREE PRODUCT REMOVAL
Free product has not been historically observed at the subject site. Multiple MMPEs have been conducted
since the CAP was developed in November 2014. The goal of the MMPEs was to reduce contaminant
concentrations in ground water.
4.0 REMEDIATION SYSTEM
In accordance with the 2014 CAP and 2021 system design, an AS/SVE system was installed at the site and
activated on March 17, 2023. The system installation included the connection of a total of seven AS wells

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 4, 2024 Fast Track #145
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5398
5
and seven SVE wells throughout the contaminant plume. A map showing the locations of the remediation
wells is included as Figure 11.

O&M site visits were conducted on October 30, November 21, and December 11, 2023. Hour meter,
system vacuum, pressure, air flow, temperature, AS well pressure, and SVE well vacuum readings were
collected during the site visits and SVE exhaust air samples were collected monthly and submitted for
laboratory analysis of BTEX.

The SVE system operated for a total of 936 hours and the system vacuum ranged from 69.91 to 70.10
inches of water during the current quarter of O&M (October through December 2023). The AS system
operated for a total of 986 hours during the reporting period with system pressures ranging from 16.45
to 18.53 PSI. Please refer to the individual O&M data sheets for additional system measurements. System
flows were adjusted as needed. The general condition of the system was also noted. Work conducted
during the site visits along with hour meter readings is summarized in Table 7. O&M field data sheets are
included as Appendix F.
5.0 AIR SAMPLING
Air samples were collected from the exhaust of the SVE system on November 21 and December 11, 2023.
An air sample was also collected on October 30, 2023, and submitted to Waypoint Analytical; however, it
was necessary for Waypoint to subcontract the sample to a different laboratory for analyzation. GRI was
informed that the sample would not be received by the subcontracted laboratory within the hold time.
Brad Newton of NCDEQ was informed of this on November 3, 2023, and it was determined that the sample
should not be analyzed. A summary of the analytical results for air samples collected during the current
quarter of system operation is presented in Table 8. Complete reports of laboratory analyses are included
as Appendix E. A summary of air sampling results during the current quarter is shown below:
Sample Date Benzene Toluene Ethylbenzene Xylenes Total
BTEX TRPH
10/30/23 NM NM NM NM NM NM
11/21/23 <3.1 <2.6 <2.3 <6.9 <14.9 <31
12/11/23 <3.1 <2.6 <2.3 <6.9 <14.9 <31

Overall, remediation and monitoring activities from CAP implementation through the current quarter
have cost $282,276.79. A breakdown of current quarter’s costs is included as Appendix G and summarized
below:
Claim
Number
Task
Code Task Code Description Cost Claim Amount
(claim has
not been
submitted)
4.031 Cost for Sampling Wells $1,661.00
$14,916.19
4.090 Cost for Analytical $1,877.00
6.090 Ground Water Monitoring Report $2,250.00
7.201 Cost for Scheduled Maintenance $728.19
7.260 Cost for Remediation Operating Expenses
(assumed, pending receipt of all power bills) $6,600.00
12.050 Consultant Travel $1,500.00
12.055 Temporary Impact Increase $300.00
Total Cost Since System Installation $282,276.79

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 4, 2024 Fast Track #145
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5398
6
6.0 GROUND WATER REMEDIATION
The baseline contaminant mass at the site was determined based on the total BTEX, MTBE, and
naphthalene concentrations reported in the January 2014 CSA as well as the maximum historical water
column height observed in each area. The contaminant plume was divided into three areas (Areas 1
through 3) based on the benzene concentrations during the July 2020 ground water sampling event. A
map showing the estimated contaminant mass areas is included as Figure 12.

Available historical data for the site was reviewed in order to develop a strategy for measuring
remediation progress against an established baseline for the contaminant plume. To calculate
contaminant mass present at the site, the following three avenues of contaminant migration/source were
evaluated as well as the data required for each source. The calculations were revised to estimate the
influence of fluctuations in ground water elevation.

1. Contamination present in ground water: the November 2012 and March 2013 ground water
sampling data and total BTEX, MTBE, and naphthalene constituents were used to determine the
baseline contaminant mass in each area. Area #1 had approximately 76,258.29 grams of
contaminant mass; Area #2 had approximately 102,686.65 grams of contaminant mass and Area
#3 had approximately 1,428.39 grams of contaminant mass.

Calculations based on the December 2023 ground water sampling event indicate that the
contaminant mass has decreased by 7.1%, 86.8%, and 87.9% in Areas 1, 2, and 3, respectively,
when compared to the baseline sampling event. The contaminant concentrations in Area 1
through Area 3 have generally decreased over time; however, additional monitoring is necessary
to determine the effect of the remediation system on the contaminant plume. The overall
contaminant mass at the site has decreased by approximately 53.1% from the baseline event to
the December 2023 sampling event. Contaminant mass calculations are included as Appendix H.
A chart depicting the overall trend in contaminant mass and the changes in average water column
depth over time is shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 4, 2024 Fast Track #145
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5398
7

2. Contamination due to leaching effect from unsaturated soils: soil quality data from the former
source areas as well as from the vicinity of the above referenced source area monitoring wells is
not available. Therefore, it is not possible at this point to factor in the effect of this potential on-
going source of ground water contamination. If soil sampling is deemed necessary for the
calculation of any secondary source inputs, they will be proposed at a later date.
3. Contamination input due to the presence of free product: free product has not been historically
observed at the subject site.

Monitoring Plan:
Based on the Intermediate site risk ranking, the following monitoring plan is recommended:
 Conduct a comprehensive ground water sampling event that includes wells MW-1, MW-3, MW-
4, MW-6, MW-8 through MW-10, MW-14, MW-15, and MW-17 on a quarterly basis for the initial
year of operation to monitor the effect of the remediation system. Following the initial year of
operation, any wells with contaminant concentrations exceeding 10 times the 2B Standard should
be sampled on a semi-annual basis and a comprehensive sampling event for the above listed wells
should be conducted on an annual basis.
 Conduct soil sampling on an as-needed basis.
Performance Monitoring:
 The remediation system appears to have been effective at reducing ground water contaminant
concentration in the targeted wells; however, additional monitoring is necessary to establish a
trend for the remedial efforts. Please note that milestones were not established in the CAP.
 The remediation system should remain running for the next quarter of operation.
0.00
2.00
4.00
6.00
8.00
10.00
12.00
14.00
16.00
18.00
30,000
80,000
130,000
180,000
230,000
280,000
Av
e
r
a
g
e

W
a
t
e
r

C
o
l
u
m
n

H
e
i
g
h
t

(
f
t
)
Co
n
t
a
m
i
n
a
n
t

M
a
s
s

(
g
r
a
m
s
)
Time
Total Contaminant Mass vs. Time
Fast Track #145 (Incident No. 40099)
Contaminant Mass (grams)Water Column Height (ft)Linear (Contaminant Mass (grams))

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 4, 2024 Fast Track #145
Project Manager: Ashleigh Thrash, P.G. GRI Project No. 5398
8
7.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
Due to the site being in the active remediation phase, no natural attenuation monitoring plan is currently
in place at the site.
8.0 CONCLUSIONS
 O&M site visits were conducted on October 30, November 21, and December 11, 2023. Hour
meter, system vacuum, pressure, air flow, temperature, AS well pressure, and SVE well vacuum
readings were collected during each site visit.
 On December 11, 2023, ten Type II monitoring wells (MW-1, MW-3, MW-4, MW-6, MW-8, MW-
9, MW-10, MW-14, MW-15, and MW-17) were gauged, purged, and sampled. A surface water
sample was not collected from the creek adjacent to the site because the water was stagnant and
was not a representative sample of typical surface water conditions in the creek. Free product
was not observed during the December 2023 gauging activities. Ground water flow was generally
to the east with a horizontal gradient of approximately 0.06 feet per foot. The vertical gradient
was not calculated.
 The concentrations of benzene, toluene, ethylbenzene, xylenes, MTBE, naphthalene, 2-hexanone,
isopropylbenzene, n-propylbenzene, styrene, 1,2,4-trimethylbenzene, and/or 1,3,5-
trimethylbenzene reported in the ground water samples collected from MW-1, MW-3, MW-4,
MW-6, MW-8, MW-9, MW-14, MW-15, and MW-17 exceeded the MACs. The concentrations of
benzene, toluene, ethylbenzene, xylenes, and/or naphthalene reported in the ground water
samples collected from MW-1, MW-4, MW-6, MW-8, MW-14, and MW-17 exceeded 10 times the
2B Standards. The concentrations of benzene reported in the ground water samples collected
from MW-4 and MW-6 exceeded the GCL.
 Calculations based on the December 2023 ground water sampling event indicate that the
contaminant mass has decreased by 7.1%, 86.8%, and 87.9% in Areas 1, 2, and 3, respectively,
when compared to the baseline sampling event. The overall contaminant mass at the site has
decreased by approximately 53.1% from the baseline event to the December 2023 sampling
event.
 Based on this information, the risk classification for the site should remain Intermediate risk. GRI
recommends the continued operation of the remediation system until contaminant
concentrations have been reduced to below 10 times the 2B Standards.
9.0 LIMITATIONS
This report has been prepared for the exclusive use of Raymer Oil Company and the NCDEQ for specific
application to the referenced site in Catawba County, North Carolina. The assessment was conducted
based on the scope of work and level of effort desired by the NCDEQ and with resources adequate only
for that scope of work. Our findings have been developed in accordance with generally accepted
standards of environmental practices in the State of North Carolina, available information, and our
professional judgment. No other warranty is expressed or implied.

The data that is presented in this report is indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would

FIGURES
SITE LOCATION
Figure 1
Site Location
Fast Track #145
2443 NC Highway 10 West Newton,
Catawba County, NC
Incident No. 40099
GRI Project No. 5398
500 M
2000 FT
Date: 07/19/2020 Location: 35.644579°N -81.268800°W
D
a
d
"J
"J
"J
"J
"J
"J
"J
"J
"J
"J
"J
"J
"J
"J
SITE
362911678025
362911571253
362911564459
362911670179
362907573779
362911672327
362911661942
362907576636
362911565735
362911566946
362907682129
362911576481
362907577597
362911577137
362907586014
362907672635
362911562820
362907670524
WSW-6
WSW-9
WSW-5
WSW-7
WSW-8
WSW-4
WSW-3
WSW-2
WSW-1
WSW-14
WSW-13
WSW-12
WSW-11
WSW-10
Unknown Tributary
Unknown Tributary
Unknown Tributary
NC 10 HWYSTARTOWN RD
NOTTINGHAM DR
STAR DR
KENSINGTON CIRORCHARD ST
DOVE ST
POOVEY ST
STONEHENGE ST
ISHMAL AVE
KNIGHTBRIDGE DR
CAMBRIDGE ST
JERRY AVE
HALLPOINT LN
LITTLE JOHN TRRADER ST
DOVE ST
TRACK #1452443 NC HIGHWAY 10 WESTNEWTON, CATAWBA COUNTYNORTH CAROLINAINCIDENT NO. 40099GRI NO. 5398
PREPARED BY:GEOLOGICAL RESOURCES, INC.AUGUST 13, 2020
1,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS
³
0 300150Feet1 inch = 300 feet
500-FOOT RADIUS
LEGEND
"J Water Supply Well
Catawba County_RoadCenterlines
Catawba County_Streams
Well Owners and Adjacent Properties
Catawba County_Parcels
FIGURE 3A: SITE VICINITY MAP
FAST
S
S
S
S
S
S
S
S
S
S
S
S

TABLES
UST ID Number 1A, 1B, 1C Facility ID Number
Owner or Operator?
Operator
UST ID Number 1A, 1B, 1C Facility ID Number
Owner or Operator?
Owner
UST ID Number 1A, 1B, 1C Facility ID Number
Owner or Operator?
Operator
Telephone Number
00-0-0000036548
Name of Owner or Operator Dates of Ownership / Operation
Address Telephone Number
00-0-0000036548
1-336-766-9801
P.O. Box 410, Wilkesboro, NC 28697 1-336-766-9801
00-0-0000036548
Name of Owner or Operator Dates of Ownership / Operation
Raymer Brothers, Inc. 03/05/2019 - Current
Address
Fast Track Inc. 11/02/2002 - 03/05/2019
Name of Owner or Operator Dates of Ownership / Operation
Address
Fast Track Inc. 11/02/2002 - Current
P.O. Box 410, Wilkesboro, NC 28697
P.O. Box 327, Troutman, NC 28166 1-704-873-7285
Telephone Number
TABLE 1
UST OWNER/OPERATOR INFORMATION
FAST TRACK #145 (INCIDENT NO. 40099)
Page 1 of 1
Date: 07/15/21 Facility ID # : 00-0-0000036548
Was Release
Associated
with UST
System?
(Yes / No)
1A Gasoline NA 12,000 11/1/2002 Double Wall Steel 8' x 32' Other Current Yes
1B Gasoline NA 8,000 11/1/2002 Double Wall Steel 8' x 21' 4" Other Current Yes
1C Diesel NA 5,000 11/1/2002 Double Wall Steel 8' x 13' 6" Other Current Yes
TABLE 2
UST SYSTEM INFORMATION
FAST TRACK #145 (INCIDENT NO. 40099)
Status
of
UST
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Page 1 of 1
Facility ID # : 00-0-0000036548
Well ID. Parcel ID No. Well Owner Mailing Address Well Address
Well Use
(Potable / Non-
Potable
etc.)
Connected to
Municipal Water
Yes/No
Distance from
source area of
release
(ft.)
WSW-1 36291167-2327 Rollin Acres, LLC 2421 W NC Highway 10
Newton, NC 28658
2421 W NC Highway 10
Newton, NC 28658
Abandoned
12/10/2015 Unknown ~240'
WSW-2 36291157-7137 Jerry & Michael Houser 2120 Peeler Road
Vale, NC 28168
3907 Startown Road
Newton, NC 28658
Unknown
Inactive Unknown ~250'
WSW-3 36290767-2635 Glenda R. Mathis &
Terry Robinson
5905 Old Shelby
Vale, NC 28168
2420 W NC Highway 10
Newton, NC 28658
Unknown
Inactive
Reportedly
Connected ~425'
WSW-4 36291157-6481 Startown Tire Center, Inc.2466 W NC Highway 10
Newton, NC 28658
3867 Startown Road
Newton, NC 28658
Unknown
Inactive
Reportedly
Connected ~430'
WSW-5 36290757-6636 Jessie White & John Arrowood 4646 River Run Circle
Hickory, NC 28602
2433 Poovey Street
Newton, NC 28658
Unknown
Inactive Unknown ~500'
WSW-6 36291167-8025 Jeanne F. Davis & Brian McCurdy 4133 Wild Partridge Road
Charlotte, NC 28226
2393 W NC Highway 10
Newton, NC 28658
Unknown
Inactive Unknown ~540'
WSW-7 36291156-5735 Dale & Diane Caldwell P.O. Box 562
Hudson, NC 28638
2511 W NC Highway 10
Newton, NC 28658
Unknown
Inactive
Reportedly
Connected ~620'
WSW-8 36291156-4459 Jacqueline Yoder 3991 Startown Road
Newton, NC 28658
3967 Startown Road
Newton, NC 28658
Unknown
Inactive Unknown ~680'
WSW-9 36291157-1253 Gena E. Poovey & Noah S.
Lindemann
117 Rest Street
Gaffney, SC 29340
2506 W NC Highway 10
Newton, NC 28658
Unknown
Inactive Unknown ~700'
WSW-10 36291156-2820 Cody and Kendra Beal 3265 Water Plant Road
Maiden, NC 28650
2541 W NC Highway 10
Newton, NC 28658 Unknown Unknown ~750'
WSW-11 36290757-3779 Kenneth & Peggy Bissette 2465 Poovey Street
Newton, NC 28658
2465 Poovey Street
Newton, NC 28658
Unknown
Inactive
Reportedly
Connected ~825'
WSW-12 36290758-6014 Shannon M. Mincer 2454 Poovey Street
Newton, NC 28658
2454 Poovey Street
Newton, NC 28658
Unknown
Inactive
Reportedly
Connected ~900'
WSW-13 36290768-2129 Integra Colorado Springs, LLC &
Mark S. Judd
P.O. Box 167
Hennepin, IL 61327
3802 Startown Road
Newton, NC 28658 Unknown Unknown ~900'
WSW-14 36290757-3779 Kenneth & Peggy Bissette 2465 Poovey Street
Newton, NC 28685
2465 Poovey Street
Newton, NC 28658
Unknown
Inactive
Reportedly
Connected ~950'
Note:
• Water supply well information was obtained from the 2012 LSA report submitted by a previous consultant.
• Water supply wells are keyed to Figure 3.
TABLE 3
WATER SUPPLY WELL INFORMATION
FAST TRACK #145 (INCIDENT NO. 40099)
Date: 12/20/23
Page 1 of 1
Date: 12/20/23 Facility ID # : 00-0-0000036548
Parcel Number Owner Name Address
362911670179 (Site) KLR Real Estate, LLC 589 North Main Street
Troutman, NC 28166
362911672327 Rollin Acres, LLC 2421 West NC 10 Highway
Newton, NC 28658
362911661942 Bonnie Jo Bumgarner 3938 Startown Road
Newton, NC 28658
362911566946 Dale & Diane Cynthia Caldwell
Revocable Trust
P.O. Box 562
Hudson, NC 28638
362911577137 Jerry & Michael Houser 2120 Peeler Road
Vale, NC 28168
362911576481 Startown Tire Center, Inc.2466 West NC 10 Highway
Newton, NC 28658
362907577597 Stephen Paul Herzig Revocable
Living Trust
16137 Connor Court
Los Gatos, CA 95032
362907670524 Barakah Investments NC, LLC 419 Commons Park Lane
Tucker, GA 30084
362907672635 Glenda R Mathis & Terry M Robinson 5905 Old Shelby Road
Vale, NC 28168
Note:
• Properties are keyed to Figure 3.
TABLE 4
ADJACENT PROPERTY OWNER INFORMATION
FAST TRACK #145 (INCIDENT NO. 40099)
Page 1 of 1
Date: 12/20/23
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free Product
Thickness
(ft.)
Ground
Water
Elevation (ft.)
Comments
07/02/20 23.86 ---73.95 LSA
06/08/21 23.34 ---74.47
02/14/22 25.66 ---72.15 Slight odor
11/10/22 26.79 ---71.02
06/12/23 30.77 ---67.04
09/21/23 32.55 ---65.26
12/11/23 32.05 ---65.76 Odor
07/02/20 NM NM NM
06/08/21 NM NM NM
07/02/20 21.05 ---78.95 LSA
06/08/21 20.15 ---79.85
02/14/22 23.69 ---76.31
11/10/22 25.24 ---74.76
06/12/23 24.28 ---75.72
09/21/23 25.85 ---74.15
12/11/23 25.64 ---74.36 Odor
07/02/20 NM NM NM Not Found
06/08/21 NM NM NM Not Found
02/14/22 6.96 ---59.41 Slight odor
11/10/22 NM NM NM
06/12/23 NM NM NM Not Found
09/21/23 NM NM NM Not Found
12/11/23 8.01 ---58.36 Odor
07/02/20 NM NM NM
06/08/21 NM NM NM
07/02/20 22.46 ---78.04 CSA
06/08/21 21.53 ---78.97
02/14/22 24.96 ---75.54
11/10/22 26.61 ---73.89
06/12/23 26.36 ---74.14
09/21/23 27.11 ---73.39
12/11/23 27.76 ---72.74 Odor
07/02/20 NM NM NM
06/08/21 NM NM NM
07/02/20 25.02 ---73.62 CSA
06/08/21 24.47 ---74.17
02/14/22 27.23 ---71.41 Sheen/odor
11/10/22 29.58 ---69.06
06/12/23 NM NM NM Dry
09/21/23 NM NM NM Dry
12/11/23 25.63 ---73.01 Odor
07/02/20 1.91 ---53.95 CSA
06/08/21 NM NM NM Not Found
02/14/22 1.54 ---54.32
11/10/22 1.76 ---54.10
06/12/23 NM NM NM Not Found
09/21/23 NM NM NM Not Found
12/11/23 2.02 ---53.84
07/02/20 NM NM NM Not Found
06/08/21 NM NM NM Not Found
02/14/22 2.21 ---56.26
11/10/22 1.90 ---56.57
06/12/23 NM NM NM Not Found
09/21/23 NM NM NM Not Found
12/11/23 3.43 ---55.04
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
FAST TRACK #145 (INCIDENT NO. 40099)
Facility ID # : 00-0-0000036548
19 - 39
17 - 37
Unknown Unknown
19
17
Unknown
MW-5
MW-7
11/01/12
03/08/13
Unknown
101.78
39
37
36 100.5003/08/13
13 58.473 3 - 13
81.39
MW-6 16 16 - 36
MW-8 03/11/13
MW-9 03/11/13
17 17 - 37 37 98.64
3 3 - 13 13 55.86
MW-10 03/11/13
MW-1 11/01/12 25 25 - 45 45 97.81
MW-3 11/01/12
MW-4 11/01/12
19 19 - 39 39 100.00
4 4 - 19 19 66.37
99.11MW-2
Page 1 of 2
Date: 12/20/23
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free Product
Thickness
(ft.)
Ground
Water
Elevation (ft.)
Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
FAST TRACK #145 (INCIDENT NO. 40099)
Facility ID # : 00-0-0000036548
07/02/20 NM NM NM
06/08/21 NM NM NM
07/02/20 NM NM NM
06/08/21 NM NM NM
07/02/20 NM NM NM
06/08/21 NM NM NM
07/02/20 23.06 ---75.87 CSA
06/08/21 22.33 ---76.60
02/14/22 25.99 ---72.94
11/10/22 27.73 ---71.20
06/12/23 26.48 ---72.45
09/21/23 27.27 ---71.66
12/11/23 28.06 ---70.87 Odor
07/02/20 NM NM NM Not Found
06/08/21 NM NM NM Not Found
02/14/22 2.35 ---53.09
11/10/22 2.48 ---52.96
06/12/23 NM NM NM Not Found
09/21/23 NM NM NM Not Found
12/11/23 2.62 ---52.82 Odor
07/02/20 NM NM NM
06/08/21 NM NM NM
07/02/20 23.79 ---73.96
06/08/21 NM NM NM Not Accessible
02/14/22 NM NM NM Not Accessible
11/10/22 NM NM NM
06/12/23 NM NM NM Not Found
09/21/23 25.65 ---72.10
12/11/23 27.97 ---69.78 Odor
Notes:
MW-16 05/24/13
4 - 14
17 - 37
12 - 32
4
17
12
4
03/11/13
4 - 14
MW-11
05/23/13
05/23/13
MW-12
32
14 53.00
63.07
101.31
102.97MW-13
16 16 - 36 36 98.93
• ft BGS : feet below ground surface.
97.75
MW-15 05/24/13
MW-17 Unknown
4
14
37
• NM : Not measured.
• Elevation relative to an arbitrary datum of 100.00 feet.
4 - 14 14 55.44
10 10 - 35 35
MW-14 05/24/13
Page 2 of 2
Facility ID # : 00-0-0000036548
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 70 70 400 400
510 110 1,300 6,700 15,000 120 39 2,500 800 3,900 2,150
5,000 260,000 80,000 50,000 20,000 6,000 5,900 30,500 26,100 28,500 24,100
10/23/19 642 11,700 2,350 11,920 134 615 <50.0 86.0 259 1,760 502
07/02/20 2,560 6,180 1,790 7,230 <25 362 <25 42.3 J 161 1,200 294
06/08/21 104 1,970 1,260 6,030 25.5 257 12.2 J 42.4 J 155 1,290 313
02/14/22 2,250 11,500 2,000 10,600 <63 421 <63 <63 190 J 1,470 509
11/10/22 1,750 3,370 1,420 4,880 40.1 493 30.6 82.5 209 1,090 308
06/12/23 1,840 4,550 486 3,770 <14.0 969 24.7 J 26.9 J 90.9 1,510 340
09/21/23 828 1,700 232 1,380 <14.0 940 <18.0 <18.0 <19.0 258 59.4
12/11/23 3,380 6,810 832 4,290 <14.0 302 <18.0 20.9 J 58.4 517 125
07/02/20 NS NS NS NS NS NS NS NS NS NS NS
06/08/21 NS NS NS NS NS NS NS NS NS NS NS
10/23/19 90.6 3.74 35.5 3.41 <0.500 13.2 15.9 15.5 18.4 11.8 6.86
07/02/20 23.2 0.76 5.8 1.7 <0.13 6.5 4.1 6.0 4.2 0.86 0.94
06/08/21 25.3 0.41 J 8.8 0.44 J <0.13 6.1 6.0 12.3 6.2 0.27 J <0.13
02/14/22 26.1 <0.13 1.3 <0.25 <0.13 6.6 8.5 9.5 6.5 0.14 J <0.13
11/10/22 39.7 0.621 1.89 0.706 J 1.62 9.23 11.6 7.91 7.89 0.363 J <0.180
06/12/23 34.6 3.76 1.81 10.6 1.10 11.3 10.6 6.96 6.80 1.81 1.58
09/21/23 29.4 3.07 1.24 9.36 <0.140 6.80 10.4 5.54 4.26 1.18 1.65
12/11/23 17.3 1.65 0.608 4.13 0.413 J 4.57 7.29 3.66 3.02 0.511 0.525
10/23/19 4,130 1,730 3,080 5,220 56.0 781 <50.0 111 320 1,540 412
07/02/20 NS NS NS NS NS NS NS NS NS NS NS
06/08/21 NS NS NS NS NS NS NS NS NS NS NS
02/14/22 1,940 1,250 2,580 4,460 <13 551 <13 74.9 213 1,110 311
11/10/22 NS NS NS NS NS NS NS NS NS NS NS
06/12/23 NS NS NS NS NS NS NS NS NS NS NS
09/21/23 NS NS NS NS NS NS NS NS NS NS NS
12/11/23 6,770 1,470 2,900 4,140 91.7 J 655 <18.0 100 288 1,220 335
07/02/20 NS NS NS NS NS NS NS NS NS NS NS
06/08/21 NS NS NS NS NS NS NS NS NS NS NS
10/23/19 12,200 27,200 2,630 15,240 <100 766 <100 106 310 2,350 678
07/02/20 12,900 43,700 2,910 14,700 <130 509 <130 <130 261 J 1,570 482 J
06/08/21 8,110 21,200 1,670 8,560 <63 274 <63 <63 195 J 1,310 397
02/14/22 11,200 44,000 3,300 17,800 <130 662 <130 <130 319 J 2,280 708
11/10/22 9,380 33,100 2,790 14,000 <14.0 698 51.2 134 412 2,700 743
06/12/23 8,850 23,100 1,940 10,900 <14.0 588 44.6 J 92.3 290 2,070 601
09/21/23 8,790 28,100 2,640 14,300 <14.0 730 34.9 J 99.8 315 2,560 687
12/11/23 10,200 39,500 3,280 15,500 <14.0 824 23.5 J 106 311 2,270 568
MW-7 07/02/20 NS NS NS NS NS NS NS NS NS NS NS
10/23/19 8,400 24,700 3,900 21,660 <50.0 1,170 <50.0 157 453 3,310 959
07/02/20 5,650 33,800 3,090 16,300 <130 635 <130 <130 274 J 1,870 543
06/08/21 8,620 36,500 3,270 18,100 <130 512 <130 <130 286 J 1,970 576
02/14/22 3,840 68,800 E 14,500 81,200 <130 8,460 1,280 1,300 5,390 37,600 11,100
11/10/22 4,010 39,100 3,620 17,900 <14.0 771 34.9 J 137 399 2,860 733
06/12/23 NS NS NS NS NS NS NS NS NS NS NS
09/21/23 NS NS NS NS NS NS NS NS NS NS NS
12/11/23 <1.80 21.8 12.7 94.7 <1.40 466 2.23 J <1.80 3.99 J 82.2 17.2
07/02/20 51.0 1.9 2.3 <0.50 <0.25 2.5 0.87 J 3.1 0.57 J <0.25 <0.25
06/08/21 NS NS NS NS NS NS NS NS NS NS NS
02/14/22 0.95 J <0.63 <0.63 <1.3 <0.63 0.74 J <0.63 <0.63 <0.63 0.79 J <0.63
11/10/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.180 <0.190 <0.190 <0.180
06/12/23 NS NS NS NS NS NS NS NS NS NS NS
09/21/23 NS NS NS NS NS NS NS NS NS NS NS
12/11/23 17.1 2.57 5.77 0.752 0.733 J 2.26 0.436 J 1.67 1.27 <0.190 <0.180
10/23/19 <0.500 <0.500 <0.500 <1.500 3.42 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500
07/02/20 NS NS NS NS NS NS NS NS NS NS NS
06/08/21 NS NS NS NS NS NS NS NS NS NS NS
02/14/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
11/10/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.180 <0.190 <0.190 <0.180
06/12/23 NS NS NS NS NS NS NS NS NS NS NS
09/21/23 NS NS NS NS NS NS NS NS NS NS NS
12/11/23 <0.180 <0.220 <0.170 <0.210 0.459 J <0.470 <0.180 <0.180 <0.190 <0.190 <0.180
MW-5
EPA Method 6200B
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
1,
2
,
4
-
Tr
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1,
3
,
5
-
Tr
i
m
e
t
h
y
l
b
e
n
z
e
n
e
MW-2
MW-1
MW-3
MW-4
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
FAST TRACK #145 (INCIDENT NO. 40099)
To
t
a
l

X
y
l
e
n
e
s
MT
B
E
n-
B
u
t
y
l
b
e
n
z
e
n
e
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
Date: 12/20/23
Analytical Method
→
MACs (μg/l)
GCL (μg/l)
Contaminant of Concern
→
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
10 x 2B Standards (µg/l)
Na
p
h
t
h
a
l
e
n
e
MW-6
MW-8
MW-9
MW-10
Page 1 of 2
Facility ID # : 00-0-0000036548
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 70 70 400 400
510 110 1,300 6,700 15,000 120 39 2,500 800 3,900 2,150
5,000 260,000 80,000 50,000 20,000 6,000 5,900 30,500 26,100 28,500 24,100
EPA Method 6200B
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
1,
2
,
4
-
Tr
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1,
3
,
5
-
Tr
i
m
e
t
h
y
l
b
e
n
z
e
n
e
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
FAST TRACK #145 (INCIDENT NO. 40099)
To
t
a
l

X
y
l
e
n
e
s
MT
B
E
n-
B
u
t
y
l
b
e
n
z
e
n
e
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
Date: 12/20/23
Analytical Method
→
MACs (μg/l)
GCL (μg/l)
Contaminant of Concern
→
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
10 x 2B Standards (µg/l)
Na
p
h
t
h
a
l
e
n
e
07/02/20 NS NS NS NS NS NS NS NS NS NS NS
06/08/21 NS NS NS NS NS NS NS NS NS NS NS
07/02/20 NS NS NS NS NS NS NS NS NS NS NS
06/08/21 NS NS NS NS NS NS NS NS NS NS NS
07/02/20 NS NS NS NS NS NS NS NS NS NS NS
06/08/21 NS NS NS NS NS NS NS NS NS NS NS
10/23/19 <0.500 <0.500 <0.500 <1.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500
07/02/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
06/08/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
02/14/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
11/10/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.180 <0.190 <0.190 <0.180
06/12/23 22.5 57.0 7.00 51.4 <0.140 <0.470 <0.180 0.562 1.13 9.88 5.67
09/21/23 133 193 32.7 235 <0.140 <0.470 2.79 2.07 3.94 55.7 23.1
12/11/23 241 1,130 158 759 <0.140 <0.470 1.91 5.82 14.1 164 47.5
10/23/19 <0.500 <0.500 <0.500 <1.500 2.45 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500
07/02/20 NS NS NS NS NS NS NS NS NS NS NS
06/08/21 NS NS NS NS NS NS NS NS NS NS NS
02/14/22 10.3 0.56 1.3 1.5 1.5 0.90 <0.13 0.81 0.15 J 0.20 J <0.13
11/10/22 0.529 <0.220 <0.170 <0.210 0.792 J <0.470 <0.180 0.206 J <0.190 <0.190 <0.180
06/12/23 NS NS NS NS NS NS NS NS NS NS NS
09/21/23 NS NS NS NS NS NS NS NS NS NS NS
12/11/23 179 12.1 20.3 17.9 J 5.42 J <4.70 <1.80 6.81 <1.90 3.03 J 2.14 J
07/02/20 NS NS NS NS NS NS NS NS NS NS NS
06/08/21 NS NS NS NS NS NS NS NS NS NS NS
10/23/19 99.7 356 44.9 204.9 <5.00 12.7 <5.00 <5.00 6.40 37.5 8.30
07/02/20 2,590 8,080 1,430 6,540 <25 250 <25 37.4 J 142 965 256
06/08/21 NS NS NS NS NS NS NS NS NS NS NS
02/14/22 NS NS NS NS NS NS NS NS NS NS NS
11/10/22 NS NS NS NS NS NS NS NS NS NS NS
06/12/23 NS NS NS NS NS NS NS NS NS NS NS
09/21/23 <18.0 107 137 1,360 <14.0 902 <18.0 22.1 J 88.3 1,140 255
12/11/23 2.90 J 24.3 9.27 59.2 <1.40 239 <1.80 <1.80 6.16 127 28.4
10/23/19 3.53 0.600 0.500 <1.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500
07/02/20
06/08/21
02/14/22
11/10/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.180 <0.190 <0.190 <0.180
06/12/23
09/21/23
12/11/23
10/23/19 49 17.7 13.4 15.46 <0.500 7.37 <0.500 2.40 2.17 2.69 2.24
07/02/20
06/08/21
07/02/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
06/08/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
02/14/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
11/10/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.180 <0.190 <0.190 <0.180
06/12/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.180 <0.190 <0.190 <0.180
09/21/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.180 <0.190 <0.190 <0.180
12/11/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.180 <0.190 <0.190 <0.180
Notes:
• 2B Standards: North Carolina Surface Water Standards for Class C waters specified in T15A NCAC 2B.0200.
• October 23, 2019 laboratory results from the Groundwater Monitoring Report by Paragon Environmental Consultants, Inc. dated November 4, 2019.
• GCL: Gross contamination level.
• NE: Standard not established.
• < : Less than the method detection limit specified in the laboratory report.
• NS: Not sampled.
Dry
Dry
Dry
MW-16
Dry
• For other compounds reported which did not exceed the MACs, refer to the laboratory reports.
Creek Sample #2
• Other compounds exceeding the MACs: 6/8/21 - methylene chloride in MW-8.
MW-14
MW-15
MW-17
TRIP BLANK
• Other compounds exceeding the MAC: 12/11/23 - 2-hexanone and/or styrene in MW-1, MW-4, and MW-6.
Creek Sample #1
Not Sampled - Stagnant Water
Dry
Dry
Dry
• Other compounds exceeding the MAC: 11/10/22 - styrene and p-isopropyltoluene in MW-8.
• Other compounds exceeding the MACs: 2/14/22 - methylene chloride in MW-1, MW-6, and MW-8 and p-isopropyltoluene and styrene in MW-8.
MW-11
MW-12
MW-13
• Concentrations in italics indicate the GCLs were below the reported concentrations.
• Concentrations in bold face type indicate the MACs were below the reported concentrations.
• J: Estimated value.
• Results reported in µg/l (micrograms per liter)
• MAC: Maximum Allowable Concenration as specified in T15A NCAC 2L.0202.
Page 2 of 2
Facility ID # : 00-0-0000036548
SVE AS SVE AS
10/30/23 08:30-11:05 Scheduled 2.58 Collected system readings, checked oil levels, adjusted
flows and collected air sample 4,295 4,155 4,297 4,157
11/21/23 10:00-12:45 Scheduled 2.75 Collected system readings, checked oil levels, adjusted
flows and collected air sample 4,751 4,661 4,753 4,663
12/11/23 07:30-10:00 Scheduled 2.50 Collected system readings, checked oil levels, adjusted
flows and collected air sample 5,229 5,139 5,231 5,141
7.83 Total Operational Hours SVE: 936 AS: 986
Note:
TABLE 7
SUMMARY OF REMEDIATION SYSTEM O&M VISITS
FAST TRACK #145 (INCIDENT NO. 40099)
Date: 12/20/23
• Operation and Maintenance (hrs.) includes only time spent onsite.
Hour Meter Reading
Upon Departure
Hour Meter Reading
Upon Arrival Date
(mm/dd/yy)Site
Purpose of
Maintenance Visit
(Scheduled or
Unscheduled)
O&M
(hrs.)Description of Maintance Activities
Total (hrs)
Facility ID # : 00-0-0000036548
Benzene Toluene Ethylbenzene Xylenes Total BTEX TRPH
04/10/23 <3.1 <2.3 <2.3 <6.9 <14.6 NR
05/04/23 <3.1 <2.3 <2.3 <6.9 <14.6 <31
05/11/23 <3.1 <2.3 <2.3 <6.9 <14.6 55
06/12/23 <3.1 <2.3 <2.3 <6.9 <14.6 <31
07/17/23 <3.1 <2.6 <2.3 <6.9 <14.9 34
08/21/23 <3.1 <2.6 <2.3 <6.9 <14.9 <31
09/19/23 <3.1 <2.6 <2.3 <6.9 <14.9 <31
10/30/23 NM NM NM NM NM NM
11/21/23 <3.1 <2.6 <2.3 <6.9 <14.9 <31
12/11/23 <3.1 <2.6 <2.3 <6.9 <14.9 <31
Notes:
• Results reported in ppmv (parts per million volume).
• *Air samples collected from the exhaust of the vacuum blower may be named differently in the lab report.
• <: Less than the method detection limit specified in the laboratory report.
• NR: Not Reported.
• TRPH is based on benzene.
SVE EXHAUST*
TABLE 8
SUMMARY OF AIR ANALYTICAL RESULTS
FAST TRACK #145 (INCIDENT NO. 40099)
Date: 12/20/23
Well No.Sample Date
(mm/dd/yy)
EPA METHOD 18
Parge 1 of 1

APPENDICES

APPENDIX A
State Correspondence

July 17, 2023
Raymer Oil Company 589 North Main Street Troutman, North Carolina 28166
Attention: Matthew Redmond Re: Fast Track #145 2443 NC Highway 10 West, Newton Catawba County Incident Number: 40099 Risk Classification: Intermediate Ranking: I125D Dear Mr. Redmond: On June 30, 2023, the Underground Storage Tank Section of the Division of Waste Management, Mooresville
Regional Office, received the Corrective Action Performance Report for the above-referenced site. This information has been reviewed and will remain in the UST Section’s files. Per the NORR dated March 28, 2022, sampling should be conducted on a quarterly basis for the first year of system operation. The next sampling event should therefore be
conducted September 2023, with the CAPR received by this office no later than October 31, 2023. If monitoring wells MW-4 and MW-17 cannot be located and/or accessed during the September 2023 groundwater sampling event, they must be replaced prior to the December 2023 groundwater sampling event.
If you have any questions regarding the actions that must be taken, or the rules mentioned in this letter, please contact me at the address or telephone number listed below for the Mooresville Regional Office. Sincerely, Brad C. Newton, P.G. Hydrogeologist
Mooresville Regional Office UST Section, Division of Waste Management, NCDEQ
cc: Joanna Alley – Geologic Resources, Inc. (via e-mail) Catawba County Health Department
Site Name City / County /Catawba Incident #40099
Resp Pty Name / Contact Incident Mgr Region MORRP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #24
Consultant / Project Mgr /Joanna R Alley
Telephone / Fax Number /Task Authorization Number:25 ChangeOrd:
Project Mgr Email Site Risk / Rank / Abatement:I125D RRA Date:
Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
 Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.
Task #Lab /
SubCode
RO

A
u
t
h
Proposed
Rate/Price
(Consultant)CO

A
u
t
h
Proposed Task
Subtotal
(Consultant)
Final
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
4.031 10 /wells y $110.00 Y $1,100.00 $1,100.00 /
4.051 1 /sample pt.y $50.00 Y $50.00 $50.00 /
4.090 #272 12 /samples y $66.00 Y $792.00 $792.00 /
4.090 #880 3 /samples y $151.00 Y $453.00 $453.00 /
4.091 3 /shipments y $60.00 Y $180.00 $180.00 /
6.090 1 /report y $1,125.00 Y $1,125.00 $1,125.00 /
7.201 15 /hours y $93.00 Y $1,395.00 $1,395.00 /
7.250 1 /system y $2,000.00 Y $2,000.00 $2,000.00 /
7.260 3 /systems y $1,100.00 Y $3,300.00 $3,300.00 /
12.050 3 /trips y $250.00 Y $750.00 $750.00 /
12.055 3 /trips y $50.00 Y $150.00 $150.00 /
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
Requested Preapproved
TOTAL:$11,295.00 $11,295.00 TOTAL:
Total Standard Costs (Not Third Party)$11,295.00 $11,295.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty CostsProcess Tracking (Date)
TA Submittal:9/28/23 by:(PM)(Reserved for RO)
RO Review:9/28/23 by:(IM)Joint UST Preapproval Confirmed By:
CO Review:9/29/23 by:(STF)RP or Designee Receipt Confirmation By:
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable.
3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned.
4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee and returned to the Trust Fund within a week of approval. Signature
indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to work proceeding. Scope/costnegotiations do not supersede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both the UST Section and RPis not to be modified without written consent by all signatories.
5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full.
DWM/UST ePATA 4/1/2022
Proposed
Units / Type
(Consultant)
Brad Newton
YES23-634 Oct-Dec 2023
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
[e-mail]
Raymer Oil Company Matthew Redmond
Geological Resources, Inc.
Newton
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
704-845-4010 (Reserved for Incident Manager)
Fast Track 145
Note:This Electronic Preapproval Task Authorization (ePATA)shall be used to receive preapproval from the UST Section.A proposal,including maps and figures,must be
attached to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If,following completion of this ePATA,
you discover that unexpected tasks must be performed, incurring costs for tasks not originally included with this form,you must complete and submit a separate ePATA requestdesignated as a "Change Order" in the provided space above prior to conducting those tasks.Include a copy of the prior ePATA form for confirmation.Please attach this form to
the cover of the corresponding claim when requesting reimbursement.IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been
completed within 12 months ofthe completion date of the FIRST completed task to remain within the Statute ofLimitations.All ePATAs submitted withina claim areclosed with that
claim,and may not be re-used in a separate submittal,even for costs or tasks that were not originally claimed.Final reimbursement of costs associated with the Total Claimedamount below may be affected by the eligibility status of the site (i.e.,deductibles,apportionment,etc.),and the documentary validation of incurred costs as reasonable and
bcn
LP
(Initials)
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORMDept of Environmental Quality - Division of Waste Management
09/29/23
5398 Received OCT 02 2023
1
Eric Eubanks
From:Joanna Alley
Sent:Thursday, December 21, 2023 9:35 AM
To:Eric Eubanks
Subject:FW: [External] Fast Track 145 Air Sample

Best Regards,
Joanna Alley, P.E.
Project Manager
Geological Resources, Inc.
2021 Winner of the Union County Chamber Excellence In Business Award
3502 Hayes Road | Monroe, NC 28110 | website | facebook |
704-845-4010-office | 704-698-1244-direct | 704-845-4012-fax

From: Newton, Brad <[e-mail]>
Sent: Friday, November 3, 2023 3:36 PM
To: Joanna Alley <[e-mail]>
Subject: RE: [External] Fast Track 145 Air Sample

Skip it. Just make a note in the report.

Brad C. Newton, P.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Qualty
UST Section, Mooresville Regional Office
[phone] (Office)
)828) 572-3041 (Cell)
[e-mail]

Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115

E-mail correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed
to third par es

Branch’s Underground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust Branch’s Above Ground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
https://deq.nc.gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-maps File Review Procedures: https://deq.nc.gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
2
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
https://deq.nc.gov/about/divisions/waste-management/laserfiche

Document Submi al & UST File Names for Laserfiche Policies:
https://files.nc.gov/ncdeq/Waste%20Management/DWM/UST/WhatsNew/Final-Electronic-Document-Submittal-Policy.pdf
https://files.nc.gov/ncdeq/Waste%20Management/DWM/UST/Corrective%20Action/UST%20file%20names%20for%20Laserfiche.d
ocx

From: Joanna Alley <[e-mail]>
Sent: Friday, November 3, 2023 3:35 PM
To: Newton, Brad <[e-mail]>
Subject: [External] Fast Track 145 Air Sample

CAUTION: External email. Do not click links or open attachments unless verified. Report suspicious emails with the Report Message
button located on your Outlook menu bar on the Home tab.

Hey Brad,

The lab has to sub out the air sample and the ab they sub to does not do Saturday delivery so it will be out of hold. Do
you want me to run it anyways or skip the month?

Best Regards,
Joanna Alley, P.E.
Project Manager
Geological Resources, Inc.
2021 Winner of the Union County Chamber Excellence In Business Award
3502 Hayes Road | Monroe, NC 28110 | website | facebook |
704-845-4010-office | 704-698-1244-direct | 704-845-4012-fax

Email correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third parties by an authorized
state official.

APPENDIX B
Land Use Information
Date: 06/29/23 Facility ID # : 00-0-0000036548
Map ID No. Land Use Feature Zoning Description Address
Distance from
Source Area
(feet)
1 Fresenius Kedney Care
Newton PD-SC Doctor's Office 3802 Startown Road
Newton, NC 28658 ~990
2 St. Paul Lutheran Church R-20 Church 3761 Startown Road
Newton, NC 28658 ~1,095
n/a B-2 Business n/a n/a
n/a PD-SC Planned Development
Shopping Center n/a n/a
n/a R-20 Residential n/a n/a
n/a R-20A Residential n/a n/a
Note:
• Properties are keyed to Figure 3B.
APPENDIX B
LAND USE INFORMATION
FAST TRACK #145 (INCIDENT NO. 40099)
Page 1 of 1

APPENDIX C
Incident Reports
NCDEQ Incident Report
RP/Company FAST TRACK, INC.
RPAddress P.O. BOX 410
RPCity WILKESBORO
Contact J.C. FAW
RPState NC
TELEPHONE
IncidentNumber 40099 USTNum MO-8561
IncidentName FAST TRACK #145
FacilID 00-0-0000036548
Address 2443 WEST NC 10 HIGHWAY
CityTown NEWTON State NC
ZipCode 28658-
DateOccurred 7 /5 /2012
DateReported 8 /9 /2012
ConfRisk I
CloseOut
COMMENT
RptType Rcvd Rvwd Appvd
Incident Mgr BCNLongitude-81.268361 Latitude 35.644438
County CATAW
LSA2 12/3/2012 12/20/2012 12/20/2012
CSAS 1/14/2014 2/20/2014 2/20/2014
CAP 11/24/2014 12/15/2014
MRPI 5/31/2016 6/2/2016 6/2/2016
RMR 5/15/2017 6/2/2017 6/2/2017
Wednesday, December 20, 2023 Page 1 of 2
RMR 11/9/2017 11/29/2017 11/29/2017
RMR 5/24/2018 6/6/2018 6/6/2018
RMR 12/3/2018 12/17/2018 12/17/2018
RMR 5/30/2019 6/10/2019 6/10/2019
RMR 9/1/2020 9/9/2020 9/9/2020
MRP 7/20/2021 7/28/2021 7/28/2021
MRP 11/29/2022 12/15/2022 12/15/2022
CAPR 7/3/2023 7/17/2023 7/17/2023
CAPR 10/20/2023 11/2/2023 11/2/2023
Wednesday, December 20, 2023 Page 2 of 2
NCDEQ Incident Report
RP/Company PETROLEUM WORLD, INC.
RPAddress 681 NC 120 HWY
RPCity MOORESBORO
Contact DEBBIE SAILORS
RPState NC
TELEPHONE
IncidentNumber 10359 USTNum MO-3817
IncidentName QUICK STOP #76
FacilID 00-0-0000007821
Address 2442 NC HIGHWAY 10 WEST
CityTown NEWTON State NC
ZipCode 28658-
DateOccurred 2 /10/1993
DateReported 5 /31/1995
ConfRisk L
CloseOut 8/29/2016
COMMENT
WSW-1 REPORTEDLY ABANDONED PRIOR TO CONSTRUCTION OF CAR WASH ON THAT PROPERTY. NO
DOCUMENTATION PROVIDED.
RptType Rcvd Rvwd Appvd
Incident Mgr BCNLongitude-81.268775 Latitude 35.645419
County CATAW
CSA 3/1/1996 5/30/1996
CAP 12/27/1996 9/11/1997 9/11/1997
RMR 9/9/2002 9/25/2002 9/24/2002
RMR 3/3/2003 3/21/2003 3/21/2003
RMR 8/29/2003 9/17/2003 9/17/2003
Thursday, June 29, 2023 Page 1 of 3
RMR 3/3/2004 4/8/2004 4/8/2004
RMR 8/31/2004 9/10/2004 9/15/2004
RMR 8/23/2007 9/7/2007 9/7/2007
RMR 2/15/2008 3/4/2008 3/4/2008
RMR 8/7/2008 8/14/2008 8/14/2008
RMR 1/29/2009 2/16/2009 2/16/2009
RMR 7/15/2009 7/22/2009 7/22/2009
RMR 2/1/2010 2/18/2010 2/18/2010
RMR 7/20/2010 8/5/2010 8/5/2010
RMR 2/1/2011 2/15/2011 2/15/2011
Thursday, June 29, 2023 Page 2 of 3
RMR 8/1/2011 8/15/2011 8/15/2011
RMR 1/30/2012 2/17/2012 2/17/2012
RMR 8/8/2012 8/31/2012 8/31/2012
RMR 2/6/2013 2/22/2013 2/22/2013
RMR 2/3/2014 3/7/2014 3/7/2014
RMR 8/5/2014 8/22/2014 8/22/2014
RMR 1/30/2015 2/24/2015 2/24/2015
RMR 7/24/2015 8/18/2015 8/18/2015
DR 8/26/2016 8/29/2016 8/29/2016
PN 10/12/2016
Thursday, June 29, 2023 Page 3 of 3
NCDEQ Incident Information
RP/Company ROAM K. JARRETT Contact ROAM K. JARRETT
RPAddress 3910 STARTOWN-LINCOLNTON
RPCity NEWTON
RPZipCode 28658-
RPState NC
TELEPHONE [phone]
IncidentNumber 22431
IncidentName STARTOWN SERVICE (J.C. FAW PROP.)
Address 3910 STARTOWN-LINCOLNTON HWY.
CityTown NEWTON State NC
County CATAWZipCode28658-
Lattitude 35.644553 Longitude -81.268736
COMMENT
3 GAS UST'S CLOSED 8/15/91. REPORT NEVER SUBMITTED. 10 PPM DETECTED UNDER ONE TANK. THEY WANT TO DO
ADD. SOIL SAMPLES AND RUN RISK-BASED. WE NEED SAMPLES UNDER LINES AND DISPENSER TOO.
DateOccurred 8 /15/1991
DateReported 9 /25/2000
CloseOut 2/2/2004
FacilID 00-0-000000704 USTNum MO-6009
Mgr FTF
Conf Risk L
Site Priority
Thursday, June 29, 2023 Page 1 of 1

APPENDIX D
Historical Soil Quality Information

APPENDIX E
Laboratory Analytical Reports

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

12/8/2023
Geological Resources, Inc. Joanna Alley
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-325-0031 Client Project Description: Fast Track #145
GRI #5398
Dear Joanna Alley:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 11/21/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 13
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Page 1 of 1 00016/23-325-0031
Page 2 of 13
Report Number:
Sample Summary Table
Client Project Description:
23-325-0031
Fast Track #145
GRI #5398
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
11/21/2023 10:35Air 90010 Air 11/21/2023 SUBCONTRACT AES
AES: Analytical Environmental Services, Inc., Atlanta, GA
Page 3 of 13
November 30, 2023
LABORATORY REPORT NUMBER
PROJECT ID
Primary Data Review By
Project Manager, AES
2311O68
Danyale Love
Waypoint Analytical
449 Springbrook Road
Charlotte NC 28217
23-325-0031
Chris Pafford Project Manager, Access
Analytical
Ashley Amick
PLEASE NOTE:
-Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc.
(AES Inc), 3080 Presidential Drive, Atlanta, GA 30340.
-AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab #
FL-E87582, NELAP certified laboratory # E87582
- AIHA-LAP,LLC Laboratory ID:100671 for Industrial Hygiene samples (Organics, Metals, PCM
Asbestos, Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental
Microbiology (Fungal) Direct Examination.
- Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a
representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be
directed
Secondary Data Review By
ATTENTION
DATE
CLIENT
ANALYTICAL REPORT
Page 1 of 8Page 4 of 13
Page 2 of 8Page 5 of 13
Analytical Results
for
30-Nov-23Date:
Workorder:
Client Reference:
Qual Date Analyzed
/Analyst
Reportin
gLimit
(ug)
Concentration
Total
(ug)
(mg/m3) (ppm)
Analyte
2311O68
Waypoint Analytical
23-325-0031
Front
(ug)
Back
(ug)
Test
Method
11/21/2023Lab ID:90010 Tedlar Bag 1Air Vol.(L):Media:Client ID:2311O68-001A Date Sampled:
<3.1<10Benzene <10 10 EPA1811/28/2023 BHI<10 <10
<2.3<10Ethylbenzene <10 10 EPA1811/28/2023 BHI<10 <10
<4.6<20m,p-Xylene <20 20 EPA1811/28/2023 BHI<20 <20
<2.3<10o-Xylene <10 10 EPA1811/28/2023 BHI<10 <10
<2.6<10Toluene <10 10 EPA1811/28/2023 BHI<10 <10
<250TPH (Gasoline) <250 250 SW8015BM11/28/2023 BHI<250 <250
<31<100TRPH (Based on Benzene) <100 100 EPA1811/28/2023 BHI<100 <100
89 Surr:1,4 Difluorobenzene 89 0 SW8015BM11/28/2023 BHI88.654
Qualifiers:
< Less than the indicated Reporting Limit
H Holding time for preparation or analysis
B Analyte detected in the associated Method Blank
(a) Analysis indicates possible breakthrough; back section result is greater than % of the front section result.10
Page 3 of 8Page 6 of 13
1. Client Name:AES Work Order Number:
2. Carrier: FedEx UPS USPS Client Courier Other
Yes No N/A
3.
4.
5.
6.
7.
8.
9.
10.
11.If no TAT indicated, proceeded with standard TAT per Terms & Conditions.
12.
13.Comments:
I certify that I have completed sections 1-13 (dated initials).
Yes No N/A
14.
15.
16.
17.
19.
21.
22.
23.
24.
25.
26.Comments:
I certify that I have completed sections 14-26 (dated initials).
Yes No N/A
27.
28.
29.
*Note: Certain analyses require chemical preservation but must be checked in the laboratory and not upon Sample Receipt such as Coliforms, VOCs and Oil & Grease/TPH.
This also excludes metals by EPA 200.7, 200.8 and 245.1 which will be verified between 16 and 24 hours after preservation.
I certify that I have completed sections 27-29(dated initials).
SAMPLE/COOLER RECEIPT CHECKLIST
Details Comments
Shipping container/cooler received in good condition?damaged leaking other
Cooler temperature(s) within limits of 0-6϶͍΀^ĞĞŝƚĞŵϭ2ĨŽƌƚĞŵƉĞƌĂƚƵƌĞƌĞĐŽƌĚŝŶŐƐ͘΁
Custody seals present on shipping container?
Custody seals intact on shipping container?
Chain of Custody (COC) present?
Chain of Custody signed, dated, and timed when relinquished and received?
Sampler name and/or signature on COC?
Were all samples received within holding time?
TAT marked on the COC?
Cooler 1 Temperature ϶ŽŽůĞƌϮdĞŵƉĞƌĂƚƵƌĞ϶ŽŽůĞƌϯdĞŵƉĞƌĂƚƵƌĞ϶ŽŽůĞƌϰdĞŵƉĞƌĂƚƵƌĞ϶
Cooler 5 Temperature ϶ŽŽůĞƌϲdĞŵƉĞƌĂƚƵƌĞ϶ŽŽůĞƌϳdĞŵƉĞƌĂƚƵƌĞ϶ŽŽůĞƌϴdĞŵƉĞƌĂƚƵƌĞ϶
Details Comments
Were sample containers intact upon receipt?
Temperature blanks present?
Custody seals present on sample containers?
Custody seals intact on sample containers?
18.Do sample container labels match the COC?incomplete info illegible
no label other
Are analyses requested indicated on the COC?
20.Were all of the samples listed on the COC received?samples received but not listed on COC
samples listed on COC not received
Was the sample collection date/time noted?
Did we receive sufficient sample volume for indicated analyses?
Were samples received in appropriate containers?
Were VOA samples received without headspace (< 1/4" bubble)?
Were trip blanks submitted?listed on COC not listed on COC
This section only applies to samples where pH can be checked at
Sample Receipt. Details Comments
Have containers needing chemical preservation been checked?*
Containers meet preservation guidelines?
Was pH adjusted at Sample Receipt?
Checklist 7.24.23 Rev 4
Access Analytical, Inc 2311O68
✔
Ambient
CP2 11/22/23
LE 11/22/23
LE 11/22/23
Clear Save as
Locked
Page 4 of 8Page 7 of 13
30-Nov-23Date:Analytical Environmental Services, Inc
Client:
Dates ReportLab Order:
Project Name:
Lab Sample ID Client Sample ID Test NameCollection Date Matrix TCLP Date Prep Date Analysis Date
2311O68
23-325-0031
Waypoint Analytical
2311O68-001A 90010 11/21/2023 10:35:00AM Air Aromatic Volatiles in Air 11/24/2023 8:45:00AM 11/28/2023
2311O68-001A 90010 11/21/2023 10:35:00AM Air GASOLINE RANGE ORGANICS 11/24/2023 8:45:00AM 11/28/2023
Page 5 of 8Page 8 of 13
30-Nov-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name
ANALYTICAL QC SUMMARY REPORT
23-325-0031
2311O68
Waypoint Analytical
367326
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID: Analysis Date: Seq No:TestCode:367326MBLK11/28/2023Aromatic Volatiles in Air EPA18
Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 11/24/2023 532331MB-367326
12645063
Benzene 10BRL
Ethylbenzene 10BRL
m,p-Xylene 20BRL
o-Xylene 10BRL
Toluene 10BRL
TRPH (Based on Benzene) 100BRL
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID: Analysis Date: Seq No:TestCode:367326MBLK11/28/20238015M SW8015CM
Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 11/24/2023 532332MB-367326
12645175
TPH (Gasoline)250BRL
Surr: 1,4 Difluorobenzene 081.62 100.0 81.6 67.1 119
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID: Analysis Date: Seq No:TestCode:367326LCS11/28/2023Aromatic Volatiles in Air EPA18
Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 11/24/2023 532331LCS-367326
12645064
Benzene 10108.2 100.0 108 82.3 119
Ethylbenzene 10115.2 100.0 115 83.7 126
m,p-Xylene 20222.9 200.0 111 81.3 124
o-Xylene 10106.7 100.0 107 78.4 123
Toluene 10109.8 100.0 110 82 124
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID: Analysis Date: Seq No:TestCode:367326LCS11/28/20238015M SW8015CM
Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 11/24/2023 532332LCS-367326-2
12645176
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit
Page 6 of 8Page 9 of 13
30-Nov-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name
ANALYTICAL QC SUMMARY REPORT
23-325-0031
2311O68
Waypoint Analytical
367326
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID: Analysis Date: Seq No:TestCode:367326LCS11/28/20238015M SW8015CM
Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 11/24/2023 532332LCS-367326-2
12645176
TPH (Gasoline)2501113 1000 111 75.1 120
Surr: 1,4 Difluorobenzene 099.76 100.0 99.8 67.1 119
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID: Analysis Date: Seq No:TestCode:367326LCSD11/28/2023Aromatic Volatiles in Air EPA18
Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 11/24/2023 532331LCSD-367326
12645065
Benzene 10104.8 15100.0 105 82.3 119 108.2 3.25
Ethylbenzene 10112.6 15100.0 113 83.7 126 115.2 2.22
m,p-Xylene 20218.1 15200.0 109 81.3 124 222.9 2.17
o-Xylene 10104.4 15100.0 104 78.4 123 106.7 2.22
Toluene 10107.2 15100.0 107 82 124 109.8 2.39
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID: Analysis Date: Seq No:TestCode:367326LCSD11/28/20238015M SW8015CM
Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 11/24/2023 532332LCSD-367326-2
12645178
TPH (Gasoline)2501120 27.71000 112 75.1 120 0 0
Surr: 1,4 Difluorobenzene 098.56 0100.0 98.6 67.1 119 0 0
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit
Page 7 of 8Page 10 of 13

End of Report
Page 8 of 8Page 11 of 13
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-325-0031
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:NA
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:11/21/2023 14:43:34
Special precautions or instructions included?
Comments:
Page 12 of 13
Page 13 of 13

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

12/19/2023
Geological Resources, Inc. Joanna Alley
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-345-0025 Client Project Description: Fast Track #145
GRI #5398
Dear Joanna Alley:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 12/11/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 73
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Page 1 of 1 00016/23-345-0025
Page 2 of 73
Report Number:
Sample Summary Table
Client Project Description:
23-345-0025
Fast Track #145
GRI #5398
Lab No Client Sample ID Matrix Date Collected Date Received
12/11/2023 11:50Aqueous 91547 MW-1 12/11/2023 16:14
12/11/2023 11:20Aqueous 91548 MW-3 12/11/2023 16:14
12/11/2023 10:55Aqueous 91549 MW-4 12/11/2023 16:14
12/11/2023 11:29Aqueous 91550 MW-6 12/11/2023 16:14
12/11/2023 11:41Aqueous 91551 MW-8 12/11/2023 16:14
12/11/2023 10:25Aqueous 91552 MW-9 12/11/2023 16:14
12/11/2023 10:15Aqueous 91553 MW-10 12/11/2023 16:14
12/11/2023 11:02Aqueous 91554 MW-14 12/11/2023 16:14
12/11/2023 10:40Aqueous 91555 MW-15 12/11/2023 16:14
12/11/2023 11:10Aqueous 91556 MW-17 12/11/2023 16:14
12/11/2023 10:00Aqueous 91557 Trip Blank 12/11/2023 16:14
Page 3 of 73
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-345-0025
Report Limit
Project:Fast Track #145
V 91547MW-1
J26912/13/2023 05:066200BAcetoneµg/L 180
3380 12/13/2023 05:066200BBenzeneµg/L 18.0
832 12/13/2023 05:066200BEthylbenzeneµg/L 17.0
190 12/13/2023 05:066200B2-Hexanone µg/L 38.0
J20.9 12/13/2023 05:066200BIsopropylbenzeneµg/L 18.0
J20812/13/2023 05:066200BMethyl Ethyl Ketone (MEK)µg/L 71.0
J48.5 12/13/2023 05:066200B4-Methyl-2-Pentanone µg/L 7.80
302 12/13/2023 05:066200BNaphthaleneµg/L 47.0
58.4 12/13/2023 05:066200Bn-Propylbenzene µg/L 19.0
J24.0 12/13/2023 05:066200BStyreneµg/L 22.0
6810 12/13/2023 05:066200BTolueneµg/L 22.0
517 12/13/2023 05:066200B1,2,4-Trimethylbenzene µg/L 19.0
125 12/13/2023 05:066200B1,3,5-Trimethylbenzene µg/L 18.0
1500 12/13/2023 05:066200Bo-Xylene µg/L 21.0
2790 12/13/2023 05:066200Bm,p-Xylene µg/L 42.0
4290 12/13/2023 05:066200BXylene (Total)µg/L 21.0
V 91548MW-3
17.3 12/13/2023 00:086200BBenzeneµg/L 0.180
7.29 12/13/2023 00:086200Bn-Butylbenzene µg/L 0.180
3.77 12/13/2023 00:086200Bsec-Butyl benzene µg/L 0.200
0.608 12/13/2023 00:086200BEthylbenzeneµg/L 0.170
3.66 12/13/2023 00:086200BIsopropylbenzeneµg/L 0.180
1.98 12/13/2023 00:086200B4-Isopropyl toluene µg/L 0.089
J0.413 12/13/2023 00:086200BMethyl tert-butyl ether (MTBE)µg/L 0.140
4.57 12/13/2023 00:086200BNaphthaleneµg/L 0.470
3.02 12/13/2023 00:086200Bn-Propylbenzene µg/L 0.190
1.65 12/13/2023 00:086200BTolueneµg/L 0.220
0.511 12/13/2023 00:086200B1,2,4-Trimethylbenzene µg/L 0.190
0.525 12/13/2023 00:086200B1,3,5-Trimethylbenzene µg/L 0.180
2.07 12/13/2023 00:086200Bo-Xylene µg/L 0.210
2.06 12/13/2023 00:086200Bm,p-Xylene µg/L 0.420
4.13 12/13/2023 00:086200BXylene (Total)µg/L 0.210
V 91549MW-4
6770 12/13/2023 05:316200BBenzeneµg/L 18.0
2900 12/13/2023 05:316200BEthylbenzeneµg/L 17.0
J66.1 12/13/2023 05:316200B2-Hexanone µg/L 38.0
Page 4 of 73
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-345-0025
Report Limit
Project:Fast Track #145
V 91549MW-4
100 12/13/2023 05:316200BIsopropylbenzeneµg/L 18.0
J11512/13/2023 05:316200BMethyl Ethyl Ketone (MEK)µg/L 71.0
J91.7 12/13/2023 05:316200BMethyl tert-butyl ether (MTBE)µg/L 14.0
J43.5 12/13/2023 05:316200B4-Methyl-2-Pentanone µg/L 7.80
655 12/13/2023 05:316200BNaphthaleneµg/L 47.0
288 12/13/2023 05:316200Bn-Propylbenzene µg/L 19.0
1470 12/13/2023 05:316200BTolueneµg/L 22.0
1220 12/13/2023 05:316200B1,2,4-Trimethylbenzene µg/L 19.0
335 12/13/2023 05:316200B1,3,5-Trimethylbenzene µg/L 18.0
1700 12/13/2023 05:316200Bo-Xylene µg/L 21.0
2440 12/13/2023 05:316200Bm,p-Xylene µg/L 42.0
4140 12/13/2023 05:316200BXylene (Total)µg/L 21.0
V 91550MW-6
10200 12/14/2023 20:286200BBenzeneµg/L 180
J23.5 12/13/2023 05:556200Bn-Butylbenzene µg/L 18.0
J27.3 12/13/2023 05:556200BChloroformµg/L 22.0
3280 12/13/2023 05:556200BEthylbenzeneµg/L 17.0
213 12/13/2023 05:556200B2-Hexanone µg/L 38.0
106 12/13/2023 05:556200BIsopropylbenzeneµg/L 18.0
522 12/13/2023 05:556200BMethyl Ethyl Ketone (MEK)µg/L 71.0
824 12/13/2023 05:556200BNaphthaleneµg/L 47.0
311 12/13/2023 05:556200Bn-Propylbenzene µg/L 19.0
88.8 12/13/2023 05:556200BStyreneµg/L 22.0
39500 12/14/2023 20:286200BTolueneµg/L 220
2270 12/13/2023 05:556200B1,2,4-Trimethylbenzene µg/L 19.0
568 12/13/2023 05:556200B1,3,5-Trimethylbenzene µg/L 18.0
4540 12/13/2023 05:556200Bo-Xylene µg/L 21.0
11000 12/13/2023 05:556200Bm,p-Xylene µg/L 42.0
15500 12/13/2023 05:556200BXylene (Total)µg/L 21.0
V 91551MW-8
J2.23 12/18/2023 20:536200Bn-Butylbenzene µg/L 1.80
12.7 12/18/2023 20:536200BEthylbenzeneµg/L 1.70
466 12/18/2023 20:536200BNaphthaleneµg/L 4.70
J3.99 12/18/2023 20:536200Bn-Propylbenzene µg/L 1.90
21.8 12/18/2023 20:536200BTolueneµg/L 2.20
82.2 12/18/2023 20:536200B1,2,4-Trimethylbenzene µg/L 1.90
Page 5 of 73
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-345-0025
Report Limit
Project:Fast Track #145
V 91551MW-8
17.2 12/18/2023 20:536200B1,3,5-Trimethylbenzene µg/L 1.80
70.2 12/18/2023 20:536200Bo-Xylene µg/L 2.10
24.5 12/18/2023 20:536200Bm,p-Xylene µg/L 4.20
94.7 12/18/2023 20:536200BXylene (Total)µg/L 2.10
V 91552MW-9
17.1 12/13/2023 00:336200BBenzeneµg/L 0.180
J0.436 12/13/2023 00:336200Bn-Butylbenzene µg/L 0.180
0.545 12/13/2023 00:336200Bsec-Butyl benzene µg/L 0.200
2.29 12/13/2023 00:336200BDi-Isopropyl Ether (DIPE)µg/L 0.500
5.77 12/13/2023 00:336200BEthylbenzeneµg/L 0.170
4.93 12/13/2023 00:336200B2-Hexanone µg/L 0.380
1.67 12/13/2023 00:336200BIsopropylbenzeneµg/L 0.180
5.29 12/13/2023 00:336200BMethyl Ethyl Ketone (MEK)µg/L 0.710
J0.733 12/13/2023 00:336200BMethyl tert-butyl ether (MTBE)µg/L 0.140
2.26 12/13/2023 00:336200BNaphthaleneµg/L 0.470
1.27 12/13/2023 00:336200Bn-Propylbenzene µg/L 0.190
2.57 12/13/2023 00:336200BTolueneµg/L 0.220
0.752 12/13/2023 00:336200Bo-Xylene µg/L 0.210
0.752 12/13/2023 00:336200BXylene (Total)µg/L 0.210
V 91553MW-10
J2.06 12/13/2023 00:586200BAcetoneµg/L 1.80
1.77 12/13/2023 00:586200B2-Hexanone µg/L 0.380
J2.48 12/13/2023 00:586200BMethyl Ethyl Ketone (MEK)µg/L 0.710
J0.459 12/13/2023 00:586200BMethyl tert-butyl ether (MTBE)µg/L 0.140
V 91554MW-14
241 12/18/2023 22:366200BBenzeneµg/L 18.0
1.91 12/14/2023 12:246200Bn-Butylbenzene µg/L 0.180
1.22 12/14/2023 12:246200Bsec-Butyl benzene µg/L 0.200
158 12/18/2023 22:366200BEthylbenzeneµg/L 17.0
5.82 12/14/2023 12:246200BIsopropylbenzeneµg/L 0.180
0.795 12/14/2023 12:246200B4-Isopropyl toluene µg/L 0.089
14.1 12/14/2023 12:246200Bn-Propylbenzene µg/L 0.190
1130 12/18/2023 22:366200BTolueneµg/L 22.0
164 12/18/2023 22:366200B1,2,4-Trimethylbenzene µg/L 19.0
47.5 12/14/2023 12:246200B1,3,5-Trimethylbenzene µg/L 0.180
Page 6 of 73
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-345-0025
Report Limit
Project:Fast Track #145
V 91554MW-14
242 12/18/2023 22:366200Bo-Xylene µg/L 21.0
517 12/18/2023 22:366200Bm,p-Xylene µg/L 42.0
759 12/18/2023 22:366200BXylene (Total)µg/L 21.0
V 91555MW-15
179 12/14/2023 17:306200BBenzeneµg/L 1.80
20.3 12/14/2023 17:306200BEthylbenzeneµg/L 1.70
6.81 12/14/2023 17:306200BIsopropylbenzeneµg/L 1.80
J5.42 12/14/2023 17:306200BMethyl tert-butyl ether (MTBE)µg/L 1.40
12.1 12/14/2023 17:306200BTolueneµg/L 2.20
J3.03 12/14/2023 17:306200B1,2,4-Trimethylbenzene µg/L 1.90
J2.14 12/14/2023 17:306200B1,3,5-Trimethylbenzene µg/L 1.80
J3.10 12/14/2023 17:306200Bo-Xylene µg/L 2.10
14.8 12/14/2023 17:306200Bm,p-Xylene µg/L 4.20
J17.9 12/14/2023 17:306200BXylene (Total)µg/L 2.10
V 91556MW-17
J2.90 12/14/2023 17:556200BBenzeneµg/L 1.80
9.27 12/14/2023 17:556200BEthylbenzeneµg/L 1.70
239 12/14/2023 17:556200BNaphthaleneµg/L 4.70
6.16 12/14/2023 17:556200Bn-Propylbenzene µg/L 1.90
24.3 12/14/2023 17:556200BTolueneµg/L 2.20
127 12/14/2023 17:556200B1,2,4-Trimethylbenzene µg/L 1.90
28.4 12/14/2023 17:556200B1,3,5-Trimethylbenzene µg/L 1.80
27.2 12/14/2023 17:556200Bo-Xylene µg/L 2.10
32.0 12/14/2023 17:556200Bm,p-Xylene µg/L 4.20
59.2 12/14/2023 17:556200BXylene (Total)µg/L 2.10
Page 7 of 73

Client: Geological Resources, Inc. CASE NARRATIVE
Project: Fast Track #145 Lab Report Number: 23-345-0025
Date: 12/19/2023
Volatile Organic Compounds - GC/MS Method 6200B Analyte: 2-Butanone QC Batch No: V41230/V41227
LCS/LCSD fails high for this batch. Hits estimated high.
Analyte: Acetone QC Batch No: V41230/V41227
LCS/LCSD fails high for this batch. Hits estimated high.
Analyte: Chloroethane QC Batch No: V41230/V41227
LCS/LCSD fails high for this batch. Hits estimated high.
Analyte: Chloromethane QC Batch No: V41230/V41227
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: Di isopropyl ether QC Batch No: V41230/V41227 LCS/LCSD fails high for this batch. Hits estimated high.
Analyte: Vinyl chloride QC Batch No: V41230/V41227
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Page 8 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-1
91547 Matrix:
12/11/2023 11:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00
269 J µg/L 180 1000Acetone 100 12/13/23 05:06 V41230MSA
3380 µg/L 18.0 50.0Benzene 100 12/13/23 05:06 V41230MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 12/13/23 05:06 V41230MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 12/13/23 05:06 V41230MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 12/13/23 05:06 V41230MSA
<150 µg/L 150 500Bromoform 100 12/13/23 05:06 V41230MSA
<28.0 µg/L 28.0 100Bromomethane 100 12/13/23 05:06 V41230MSA
<18.0 µg/L 18.0 50.0n-Butylbenzene 100 12/13/23 05:06 V41230MSA
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 12/13/23 05:06 V41230MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 12/13/23 05:06 V41230MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 12/13/23 05:06 V41230MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 12/13/23 05:06 V41230MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 12/13/23 05:06 V41230MSA
<43.0 µg/L 43.0 100Chloroethane 100 12/13/23 05:06 V41230MSA
<22.0 µg/L 22.0 50.0Chloroform 100 12/13/23 05:06 V41230MSA
<22.0 µg/L 22.0 50.0Chloromethane 100 12/13/23 05:06 V41230MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 12/13/23 05:06 V41230MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 12/13/23 05:06 V41230MSA
<50.0 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 12/13/23 05:06 V41230MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 12/13/23 05:06 V41230MSA
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 12/13/23 05:06 V41230MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 12/13/23 05:06 V41230MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-1
91547 Matrix:
12/11/2023 11:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 12/13/23 05:06 V41230MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 12/13/23 05:06 V41230MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 12/13/23 05:06 V41230MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 12/13/23 05:06 V41230MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 12/13/23 05:06 V41230MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 12/13/23 05:06 V41230MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 12/13/23 05:06 V41230MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 12/13/23 05:06 V41230MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 12/13/23 05:06 V41230MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 12/13/23 05:06 V41230MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 12/13/23 05:06 V41230MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 12/13/23 05:06 V41230MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 12/13/23 05:06 V41230MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 12/13/23 05:06 V41230MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 12/13/23 05:06 V41230MSA
<4200 µg/L 4200 20000Ethanol 100 12/13/23 05:06 V41230MSA
832 µg/L 17.0 50.0Ethylbenzene 100 12/13/23 05:06 V41230MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 12/13/23 05:06 V41230MSA
190 µg/L 38.0 1002-Hexanone 100 12/13/23 05:06 V41230MSA
20.9 J µg/L 18.0 50.0Isopropylbenzene 100 12/13/23 05:06 V41230MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 12/13/23 05:06 V41230MSA
208 J µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 12/13/23 05:06 V41230MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-1
91547 Matrix:
12/11/2023 11:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00
<14.0 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 12/13/23 05:06 V41230MSA
48.5 J µg/L 7.80 1004-Methyl-2-Pentanone 100 12/13/23 05:06 V41230MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 12/13/23 05:06 V41230MSA
302 µg/L 47.0 100Naphthalene 100 12/13/23 05:06 V41230MSA
58.4 µg/L 19.0 50.0n-Propylbenzene 100 12/13/23 05:06 V41230MSA
24.0 J µg/L 22.0 50.0Styrene 100 12/13/23 05:06 V41230MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 12/13/23 05:06 V41230MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 12/13/23 05:06 V41230MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 12/13/23 05:06 V41230MSA
6810 µg/L 22.0 50.0Toluene 100 12/13/23 05:06 V41230MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 12/13/23 05:06 V41230MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 12/13/23 05:06 V41230MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 12/13/23 05:06 V41230MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 12/13/23 05:06 V41230MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 12/13/23 05:06 V41230MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 12/13/23 05:06 V41230MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 12/13/23 05:06 V41230MSA
517 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 12/13/23 05:06 V41230MSA
125 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 12/13/23 05:06 V41230MSA
<100 µg/L 100 500Vinyl Acetate 100 12/13/23 05:06 V41230MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 12/13/23 05:06 V41230MSA
1500 µg/L 21.0 50.0o-Xylene 100 12/13/23 05:06 V41230MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-1
91547 Matrix:
12/11/2023 11:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00
2790 µg/L 42.0 100m,p-Xylene 100 12/13/23 05:06 V41230MSA
4290 µg/L 21.0 50.0Xylene (Total)100 12/13/23 05:06 V41230
Surrogate: 4-Bromofluorobenzene 95.8 Limits: 70-130%12/13/23 05:06100 MSA V41230
Surrogate: Dibromofluoromethane 95.6 Limits: 70-130%12/13/23 05:06100 MSA V41230
Surrogate: 1,2-Dichloroethane - d4 89.0 Limits: 70-130%12/13/23 05:06100 MSA V41230
Surrogate: Toluene-d8 92.0 Limits: 70-130%12/13/23 05:06100 MSA V41230
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-3
91548 Matrix:
12/11/2023 11:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 12/13/23 00:08 V41230MSA
17.3 µg/L 0.180 0.500Benzene 1 12/13/23 00:08 V41230MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 12/13/23 00:08 V41230MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 12/13/23 00:08 V41230MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 12/13/23 00:08 V41230MSA
<1.50 µg/L 1.50 5.00Bromoform 1 12/13/23 00:08 V41230MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 12/13/23 00:08 V41230MSA
7.29 µg/L 0.180 0.500n-Butylbenzene 1 12/13/23 00:08 V41230MSA
3.77 µg/L 0.200 0.500sec-Butyl benzene 1 12/13/23 00:08 V41230MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 12/13/23 00:08 V41230MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 12/13/23 00:08 V41230MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 12/13/23 00:08 V41230MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 12/13/23 00:08 V41230MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 12/13/23 00:08 V41230MSA
<0.220 µg/L 0.220 0.500Chloroform 1 12/13/23 00:08 V41230MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 12/13/23 00:08 V41230MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 12/13/23 00:08 V41230MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 12/13/23 00:08 V41230MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 12/13/23 00:08 V41230MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 12/13/23 00:08 V41230MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 12/13/23 00:08 V41230MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 12/13/23 00:08 V41230MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-3
91548 Matrix:
12/11/2023 11:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 12/13/23 00:08 V41230MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 12/13/23 00:08 V41230MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 12/13/23 00:08 V41230MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 12/13/23 00:08 V41230MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 12/13/23 00:08 V41230MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 12/13/23 00:08 V41230MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 12/13/23 00:08 V41230MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 12/13/23 00:08 V41230MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 12/13/23 00:08 V41230MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 12/13/23 00:08 V41230MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 12/13/23 00:08 V41230MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 12/13/23 00:08 V41230MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 12/13/23 00:08 V41230MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 12/13/23 00:08 V41230MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 12/13/23 00:08 V41230MSA
<42.0 µg/L 42.0 200Ethanol 1 12/13/23 00:08 V41230MSA
0.608 µg/L 0.170 0.500Ethylbenzene 1 12/13/23 00:08 V41230MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 12/13/23 00:08 V41230MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 12/13/23 00:08 V41230MSA
3.66 µg/L 0.180 0.500Isopropylbenzene 1 12/13/23 00:08 V41230MSA
1.98 µg/L 0.089 0.5004-Isopropyl toluene 1 12/13/23 00:08 V41230MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 12/13/23 00:08 V41230MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-3
91548 Matrix:
12/11/2023 11:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00
0.413 J µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 12/13/23 00:08 V41230MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 12/13/23 00:08 V41230MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 12/13/23 00:08 V41230MSA
4.57 µg/L 0.470 1.00Naphthalene 1 12/13/23 00:08 V41230MSA
3.02 µg/L 0.190 0.500n-Propylbenzene 1 12/13/23 00:08 V41230MSA
<0.220 µg/L 0.220 0.500Styrene 1 12/13/23 00:08 V41230MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 12/13/23 00:08 V41230MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 12/13/23 00:08 V41230MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 12/13/23 00:08 V41230MSA
1.65 µg/L 0.220 0.500Toluene 1 12/13/23 00:08 V41230MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 12/13/23 00:08 V41230MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 12/13/23 00:08 V41230MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 12/13/23 00:08 V41230MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 12/13/23 00:08 V41230MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 12/13/23 00:08 V41230MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 12/13/23 00:08 V41230MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 12/13/23 00:08 V41230MSA
0.511 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 12/13/23 00:08 V41230MSA
0.525 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 12/13/23 00:08 V41230MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 12/13/23 00:08 V41230MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 12/13/23 00:08 V41230MSA
2.07 µg/L 0.210 0.500o-Xylene 1 12/13/23 00:08 V41230MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-3
91548 Matrix:
12/11/2023 11:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00
2.06 µg/L 0.420 1.00m,p-Xylene 1 12/13/23 00:08 V41230MSA
4.13 µg/L 0.210 0.500Xylene (Total)1 12/13/23 00:08 V41230
Surrogate: 4-Bromofluorobenzene 96.0 Limits: 70-130%12/13/23 00:081 MSA V41230
Surrogate: Dibromofluoromethane 96.0 Limits: 70-130%12/13/23 00:081 MSA V41230
Surrogate: 1,2-Dichloroethane - d4 90.2 Limits: 70-130%12/13/23 00:081 MSA V41230
Surrogate: Toluene-d8 93.2 Limits: 70-130%12/13/23 00:081 MSA V41230
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-4
91549 Matrix:
12/11/2023 10:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00
<180 µg/L 180 1000Acetone 100 12/13/23 05:31 V41230MSA
6770 µg/L 18.0 50.0Benzene 100 12/13/23 05:31 V41230MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 12/13/23 05:31 V41230MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 12/13/23 05:31 V41230MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 12/13/23 05:31 V41230MSA
<150 µg/L 150 500Bromoform 100 12/13/23 05:31 V41230MSA
<28.0 µg/L 28.0 100Bromomethane 100 12/13/23 05:31 V41230MSA
<18.0 µg/L 18.0 50.0n-Butylbenzene 100 12/13/23 05:31 V41230MSA
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 12/13/23 05:31 V41230MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 12/13/23 05:31 V41230MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 12/13/23 05:31 V41230MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 12/13/23 05:31 V41230MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 12/13/23 05:31 V41230MSA
<43.0 µg/L 43.0 100Chloroethane 100 12/13/23 05:31 V41230MSA
<22.0 µg/L 22.0 50.0Chloroform 100 12/13/23 05:31 V41230MSA
<22.0 µg/L 22.0 50.0Chloromethane 100 12/13/23 05:31 V41230MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 12/13/23 05:31 V41230MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 12/13/23 05:31 V41230MSA
<50.0 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 12/13/23 05:31 V41230MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 12/13/23 05:31 V41230MSA
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 12/13/23 05:31 V41230MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 12/13/23 05:31 V41230MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-4
91549 Matrix:
12/11/2023 10:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 12/13/23 05:31 V41230MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 12/13/23 05:31 V41230MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 12/13/23 05:31 V41230MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 12/13/23 05:31 V41230MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 12/13/23 05:31 V41230MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 12/13/23 05:31 V41230MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 12/13/23 05:31 V41230MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 12/13/23 05:31 V41230MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 12/13/23 05:31 V41230MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 12/13/23 05:31 V41230MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 12/13/23 05:31 V41230MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 12/13/23 05:31 V41230MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 12/13/23 05:31 V41230MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 12/13/23 05:31 V41230MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 12/13/23 05:31 V41230MSA
<4200 µg/L 4200 20000Ethanol 100 12/13/23 05:31 V41230MSA
2900 µg/L 17.0 50.0Ethylbenzene 100 12/13/23 05:31 V41230MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 12/13/23 05:31 V41230MSA
66.1 J µg/L 38.0 1002-Hexanone 100 12/13/23 05:31 V41230MSA
100 µg/L 18.0 50.0Isopropylbenzene 100 12/13/23 05:31 V41230MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 12/13/23 05:31 V41230MSA
115 J µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 12/13/23 05:31 V41230MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-4
91549 Matrix:
12/11/2023 10:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00
91.7 J µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 12/13/23 05:31 V41230MSA
43.5 J µg/L 7.80 1004-Methyl-2-Pentanone 100 12/13/23 05:31 V41230MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 12/13/23 05:31 V41230MSA
655 µg/L 47.0 100Naphthalene 100 12/13/23 05:31 V41230MSA
288 µg/L 19.0 50.0n-Propylbenzene 100 12/13/23 05:31 V41230MSA
<22.0 µg/L 22.0 50.0Styrene 100 12/13/23 05:31 V41230MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 12/13/23 05:31 V41230MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 12/13/23 05:31 V41230MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 12/13/23 05:31 V41230MSA
1470 µg/L 22.0 50.0Toluene 100 12/13/23 05:31 V41230MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 12/13/23 05:31 V41230MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 12/13/23 05:31 V41230MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 12/13/23 05:31 V41230MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 12/13/23 05:31 V41230MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 12/13/23 05:31 V41230MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 12/13/23 05:31 V41230MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 12/13/23 05:31 V41230MSA
1220 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 12/13/23 05:31 V41230MSA
335 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 12/13/23 05:31 V41230MSA
<100 µg/L 100 500Vinyl Acetate 100 12/13/23 05:31 V41230MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 12/13/23 05:31 V41230MSA
1700 µg/L 21.0 50.0o-Xylene 100 12/13/23 05:31 V41230MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-4
91549 Matrix:
12/11/2023 10:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00
2440 µg/L 42.0 100m,p-Xylene 100 12/13/23 05:31 V41230MSA
4140 µg/L 21.0 50.0Xylene (Total)100 12/13/23 05:31 V41230
Surrogate: 4-Bromofluorobenzene 95.4 Limits: 70-130%12/13/23 05:31100 MSA V41230
Surrogate: Dibromofluoromethane 96.0 Limits: 70-130%12/13/23 05:31100 MSA V41230
Surrogate: 1,2-Dichloroethane - d4 89.2 Limits: 70-130%12/13/23 05:31100 MSA V41230
Surrogate: Toluene-d8 92.6 Limits: 70-130%12/13/23 05:31100 MSA V41230
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-6
91550 Matrix:
12/11/2023 11:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00 V41367 12/14/23 09:00
<180 µg/L 180 1000Acetone 100 12/13/23 05:55 V41230MSA
10200 µg/L 180 500Benzene 1000 12/14/23 20:28 V41368MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 12/13/23 05:55 V41230MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 12/13/23 05:55 V41230MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 12/13/23 05:55 V41230MSA
<150 µg/L 150 500Bromoform 100 12/13/23 05:55 V41230MSA
<28.0 µg/L 28.0 100Bromomethane 100 12/13/23 05:55 V41230MSA
23.5 J µg/L 18.0 50.0n-Butylbenzene 100 12/13/23 05:55 V41230MSA
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 12/13/23 05:55 V41230MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 12/13/23 05:55 V41230MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 12/13/23 05:55 V41230MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 12/13/23 05:55 V41230MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 12/13/23 05:55 V41230MSA
<43.0 µg/L 43.0 100Chloroethane 100 12/13/23 05:55 V41230MSA
27.3 J µg/L 22.0 50.0Chloroform 100 12/13/23 05:55 V41230MSA
<22.0 µg/L 22.0 50.0Chloromethane 100 12/13/23 05:55 V41230MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 12/13/23 05:55 V41230MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 12/13/23 05:55 V41230MSA
<50.0 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 12/13/23 05:55 V41230MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 12/13/23 05:55 V41230MSA
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 12/13/23 05:55 V41230MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 12/13/23 05:55 V41230MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-6
91550 Matrix:
12/11/2023 11:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00 V41367 12/14/23 09:00
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 12/13/23 05:55 V41230MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 12/13/23 05:55 V41230MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 12/13/23 05:55 V41230MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 12/13/23 05:55 V41230MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 12/13/23 05:55 V41230MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 12/13/23 05:55 V41230MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 12/13/23 05:55 V41230MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 12/13/23 05:55 V41230MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 12/13/23 05:55 V41230MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 12/13/23 05:55 V41230MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 12/13/23 05:55 V41230MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 12/13/23 05:55 V41230MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 12/13/23 05:55 V41230MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 12/13/23 05:55 V41230MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 12/13/23 05:55 V41230MSA
<4200 µg/L 4200 20000Ethanol 100 12/13/23 05:55 V41230MSA
3280 µg/L 17.0 50.0Ethylbenzene 100 12/13/23 05:55 V41230MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 12/13/23 05:55 V41230MSA
213 µg/L 38.0 1002-Hexanone 100 12/13/23 05:55 V41230MSA
106 µg/L 18.0 50.0Isopropylbenzene 100 12/13/23 05:55 V41230MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 12/13/23 05:55 V41230MSA
522 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 12/13/23 05:55 V41230MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-6
91550 Matrix:
12/11/2023 11:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00 V41367 12/14/23 09:00
<14.0 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 12/13/23 05:55 V41230MSA
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 12/13/23 05:55 V41230MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 12/13/23 05:55 V41230MSA
824 µg/L 47.0 100Naphthalene 100 12/13/23 05:55 V41230MSA
311 µg/L 19.0 50.0n-Propylbenzene 100 12/13/23 05:55 V41230MSA
88.8 µg/L 22.0 50.0Styrene 100 12/13/23 05:55 V41230MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 12/13/23 05:55 V41230MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 12/13/23 05:55 V41230MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 12/13/23 05:55 V41230MSA
39500 µg/L 220 500Toluene 1000 12/14/23 20:28 V41368MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 12/13/23 05:55 V41230MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 12/13/23 05:55 V41230MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 12/13/23 05:55 V41230MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 12/13/23 05:55 V41230MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 12/13/23 05:55 V41230MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 12/13/23 05:55 V41230MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 12/13/23 05:55 V41230MSA
2270 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 12/13/23 05:55 V41230MSA
568 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 12/13/23 05:55 V41230MSA
<100 µg/L 100 500Vinyl Acetate 100 12/13/23 05:55 V41230MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 12/13/23 05:55 V41230MSA
4540 µg/L 21.0 50.0o-Xylene 100 12/13/23 05:55 V41230MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-6
91550 Matrix:
12/11/2023 11:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00 V41367 12/14/23 09:00
11000 µg/L 42.0 100m,p-Xylene 100 12/13/23 05:55 V41230MSA
15500 µg/L 21.0 50.0Xylene (Total)100 12/13/23 05:55 V41230
Surrogate: 4-Bromofluorobenzene 95.8 Limits: 70-130%12/13/23 05:55100 MSA V41230
Surrogate: Dibromofluoromethane 94.2 Limits: 70-130%12/13/23 05:55100 MSA V41230
Surrogate: 1,2-Dichloroethane - d4 89.4 Limits: 70-130%12/13/23 05:55100 MSA V41230
Surrogate: Toluene-d8 90.6 Limits: 70-130%12/13/23 05:55100 MSA V41230
Surrogate: 4-Bromofluorobenzene 105 Limits: 70-130%12/14/23 20:281000 MSA V41368
Surrogate: Dibromofluoromethane 97.0 Limits: 70-130%12/14/23 20:281000 MSA V41368
Surrogate: 1,2-Dichloroethane - d4 88.0 Limits: 70-130%12/14/23 20:281000 MSA V41368
Surrogate: Toluene-d8 101 Limits: 70-130%12/14/23 20:281000 MSA V41368
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-8
91551 Matrix:
12/11/2023 11:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41520 12/18/23 09:00
<18.0 µg/L 18.0 100Acetone 10 12/18/23 20:53 V41522ENM
<1.80 µg/L 1.80 5.00Benzene 10 12/18/23 20:53 V41522ENM
<2.10 µg/L 2.10 5.00Bromobenzene 10 12/18/23 20:53 V41522ENM
<4.20 µg/L 4.20 10.0Bromochloromethane 10 12/18/23 20:53 V41522ENM
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 12/18/23 20:53 V41522ENM
<15.0 µg/L 15.0 50.0Bromoform 10 12/18/23 20:53 V41522ENM
<2.80 µg/L 2.80 10.0Bromomethane 10 12/18/23 20:53 V41522ENM
2.23 J µg/L 1.80 5.00n-Butylbenzene 10 12/18/23 20:53 V41522ENM
<2.00 µg/L 2.00 5.00sec-Butyl benzene 10 12/18/23 20:53 V41522ENM
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 12/18/23 20:53 V41522ENM
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 12/18/23 20:53 V41522ENM
<1.90 µg/L 1.90 5.00Chlorobenzene 10 12/18/23 20:53 V41522ENM
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 12/18/23 20:53 V41522ENM
<4.30 µg/L 4.30 10.0Chloroethane 10 12/18/23 20:53 V41522ENM
<2.20 µg/L 2.20 5.00Chloroform 10 12/18/23 20:53 V41522ENM
<2.20 µg/L 2.20 5.00Chloromethane 10 12/18/23 20:53 V41522ENM
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 12/18/23 20:53 V41522ENM
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 12/18/23 20:53 V41522ENM
<5.00 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 12/18/23 20:53 V41522ENM
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 12/18/23 20:53 V41522ENM
<2.00 µg/L 2.00 5.001,2-Dibromoethane 10 12/18/23 20:53 V41522ENM
<2.30 µg/L 2.30 5.00Dibromomethane 10 12/18/23 20:53 V41522ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-8
91551 Matrix:
12/11/2023 11:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41520 12/18/23 09:00
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 12/18/23 20:53 V41522ENM
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 12/18/23 20:53 V41522ENM
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 12/18/23 20:53 V41522ENM
<12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 12/18/23 20:53 V41522ENM
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 12/18/23 20:53 V41522ENM
<1.50 µg/L 1.50 5.001,2-Dichloroethane 10 12/18/23 20:53 V41522ENM
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 12/18/23 20:53 V41522ENM
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 12/18/23 20:53 V41522ENM
<1.80 µg/L 1.80 5.00trans-1,2-Dichloroethene 10 12/18/23 20:53 V41522ENM
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 12/18/23 20:53 V41522ENM
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 12/18/23 20:53 V41522ENM
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 12/18/23 20:53 V41522ENM
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 12/18/23 20:53 V41522ENM
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 12/18/23 20:53 V41522ENM
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 12/18/23 20:53 V41522ENM
<420 µg/L 420 2000Ethanol 10 12/18/23 20:53 V41522ENM
12.7 µg/L 1.70 5.00Ethylbenzene 10 12/18/23 20:53 V41522ENM
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 12/18/23 20:53 V41522ENM
<3.80 µg/L 3.80 10.02-Hexanone 10 12/18/23 20:53 V41522ENM
<1.80 µg/L 1.80 5.00Isopropylbenzene 10 12/18/23 20:53 V41522ENM
<0.890 µg/L 0.890 5.004-Isopropyl toluene 10 12/18/23 20:53 V41522ENM
<7.10 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 12/18/23 20:53 V41522ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-8
91551 Matrix:
12/11/2023 11:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41520 12/18/23 09:00
<1.40 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 12/18/23 20:53 V41522ENM
<0.780 µg/L 0.780 10.04-Methyl-2-Pentanone 10 12/18/23 20:53 V41522ENM
<3.30 µg/L 3.30 20.0Methylene Chloride 10 12/18/23 20:53 V41522ENM
466 µg/L 4.70 10.0Naphthalene 10 12/18/23 20:53 V41522ENM
3.99 J µg/L 1.90 5.00n-Propylbenzene 10 12/18/23 20:53 V41522ENM
<2.20 µg/L 2.20 5.00Styrene 10 12/18/23 20:53 V41522ENM
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 12/18/23 20:53 V41522ENM
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 12/18/23 20:53 V41522ENM
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 12/18/23 20:53 V41522ENM
21.8 µg/L 2.20 5.00Toluene 10 12/18/23 20:53 V41522ENM
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 12/18/23 20:53 V41522ENM
<3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 12/18/23 20:53 V41522ENM
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 12/18/23 20:53 V41522ENM
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 12/18/23 20:53 V41522ENM
<1.80 µg/L 1.80 5.00Trichloroethene 10 12/18/23 20:53 V41522ENM
<1.80 µg/L 1.80 5.00Trichlorofluoromethane 10 12/18/23 20:53 V41522ENM
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 12/18/23 20:53 V41522ENM
82.2 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 12/18/23 20:53 V41522ENM
17.2 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 12/18/23 20:53 V41522ENM
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 12/18/23 20:53 V41522ENM
<1.70 µg/L 1.70 5.00Vinyl Chloride 10 12/18/23 20:53 V41522ENM
70.2 µg/L 2.10 5.00o-Xylene 10 12/18/23 20:53 V41522ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-8
91551 Matrix:
12/11/2023 11:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41520 12/18/23 09:00
24.5 µg/L 4.20 10.0m,p-Xylene 10 12/18/23 20:53 V41522ENM
94.7 µg/L 2.10 5.00Xylene (Total)10 12/18/23 20:53 V41522
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%12/18/23 20:5310 ENM V41522
Surrogate: Dibromofluoromethane 97.8 Limits: 70-130%12/18/23 20:5310 ENM V41522
Surrogate: 1,2-Dichloroethane - d4 88.6 Limits: 70-130%12/18/23 20:5310 ENM V41522
Surrogate: Toluene-d8 98.8 Limits: 70-130%12/18/23 20:5310 ENM V41522
Surrogate: 4-Bromofluorobenzene 95.0 Limits: 70-130%12/13/23 06:20100 MSA V41230
Surrogate: Dibromofluoromethane 95.6 Limits: 70-130%12/13/23 06:20100 MSA V41230
Surrogate: 1,2-Dichloroethane - d4 88.6 Limits: 70-130%12/13/23 06:20100 MSA V41230
Surrogate: Toluene-d8 93.2 Limits: 70-130%12/13/23 06:20100 MSA V41230
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-9
91552 Matrix:
12/11/2023 10:25
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 12/13/23 00:33 V41230MSA
17.1 µg/L 0.180 0.500Benzene 1 12/13/23 00:33 V41230MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 12/13/23 00:33 V41230MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 12/13/23 00:33 V41230MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 12/13/23 00:33 V41230MSA
<1.50 µg/L 1.50 5.00Bromoform 1 12/13/23 00:33 V41230MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 12/13/23 00:33 V41230MSA
0.436 J µg/L 0.180 0.500n-Butylbenzene 1 12/13/23 00:33 V41230MSA
0.545 µg/L 0.200 0.500sec-Butyl benzene 1 12/13/23 00:33 V41230MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 12/13/23 00:33 V41230MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 12/13/23 00:33 V41230MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 12/13/23 00:33 V41230MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 12/13/23 00:33 V41230MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 12/13/23 00:33 V41230MSA
<0.220 µg/L 0.220 0.500Chloroform 1 12/13/23 00:33 V41230MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 12/13/23 00:33 V41230MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 12/13/23 00:33 V41230MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 12/13/23 00:33 V41230MSA
2.29 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 12/13/23 00:33 V41230MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 12/13/23 00:33 V41230MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 12/13/23 00:33 V41230MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 12/13/23 00:33 V41230MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-9
91552 Matrix:
12/11/2023 10:25
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 12/13/23 00:33 V41230MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 12/13/23 00:33 V41230MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 12/13/23 00:33 V41230MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 12/13/23 00:33 V41230MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 12/13/23 00:33 V41230MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 12/13/23 00:33 V41230MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 12/13/23 00:33 V41230MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 12/13/23 00:33 V41230MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 12/13/23 00:33 V41230MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 12/13/23 00:33 V41230MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 12/13/23 00:33 V41230MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 12/13/23 00:33 V41230MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 12/13/23 00:33 V41230MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 12/13/23 00:33 V41230MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 12/13/23 00:33 V41230MSA
<42.0 µg/L 42.0 200Ethanol 1 12/13/23 00:33 V41230MSA
5.77 µg/L 0.170 0.500Ethylbenzene 1 12/13/23 00:33 V41230MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 12/13/23 00:33 V41230MSA
4.93 µg/L 0.380 1.002-Hexanone 1 12/13/23 00:33 V41230MSA
1.67 µg/L 0.180 0.500Isopropylbenzene 1 12/13/23 00:33 V41230MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 12/13/23 00:33 V41230MSA
5.29 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 12/13/23 00:33 V41230MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-9
91552 Matrix:
12/11/2023 10:25
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00
0.733 J µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 12/13/23 00:33 V41230MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 12/13/23 00:33 V41230MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 12/13/23 00:33 V41230MSA
2.26 µg/L 0.470 1.00Naphthalene 1 12/13/23 00:33 V41230MSA
1.27 µg/L 0.190 0.500n-Propylbenzene 1 12/13/23 00:33 V41230MSA
<0.220 µg/L 0.220 0.500Styrene 1 12/13/23 00:33 V41230MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 12/13/23 00:33 V41230MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 12/13/23 00:33 V41230MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 12/13/23 00:33 V41230MSA
2.57 µg/L 0.220 0.500Toluene 1 12/13/23 00:33 V41230MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 12/13/23 00:33 V41230MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 12/13/23 00:33 V41230MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 12/13/23 00:33 V41230MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 12/13/23 00:33 V41230MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 12/13/23 00:33 V41230MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 12/13/23 00:33 V41230MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 12/13/23 00:33 V41230MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 12/13/23 00:33 V41230MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 12/13/23 00:33 V41230MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 12/13/23 00:33 V41230MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 12/13/23 00:33 V41230MSA
0.752 µg/L 0.210 0.500o-Xylene 1 12/13/23 00:33 V41230MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-9
91552 Matrix:
12/11/2023 10:25
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 12/13/23 00:33 V41230MSA
0.752 µg/L 0.210 0.500Xylene (Total)1 12/13/23 00:33 V41230
Surrogate: 4-Bromofluorobenzene 96.0 Limits: 70-130%12/13/23 00:331 MSA V41230
Surrogate: Dibromofluoromethane 95.4 Limits: 70-130%12/13/23 00:331 MSA V41230
Surrogate: 1,2-Dichloroethane - d4 87.6 Limits: 70-130%12/13/23 00:331 MSA V41230
Surrogate: Toluene-d8 94.2 Limits: 70-130%12/13/23 00:331 MSA V41230
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-10
91553 Matrix:
12/11/2023 10:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00
2.06 J µg/L 1.80 10.0Acetone 1 12/13/23 00:58 V41230MSA
<0.180 µg/L 0.180 0.500Benzene 1 12/13/23 00:58 V41230MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 12/13/23 00:58 V41230MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 12/13/23 00:58 V41230MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 12/13/23 00:58 V41230MSA
<1.50 µg/L 1.50 5.00Bromoform 1 12/13/23 00:58 V41230MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 12/13/23 00:58 V41230MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 12/13/23 00:58 V41230MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 12/13/23 00:58 V41230MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 12/13/23 00:58 V41230MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 12/13/23 00:58 V41230MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 12/13/23 00:58 V41230MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 12/13/23 00:58 V41230MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 12/13/23 00:58 V41230MSA
<0.220 µg/L 0.220 0.500Chloroform 1 12/13/23 00:58 V41230MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 12/13/23 00:58 V41230MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 12/13/23 00:58 V41230MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 12/13/23 00:58 V41230MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 12/13/23 00:58 V41230MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 12/13/23 00:58 V41230MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 12/13/23 00:58 V41230MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 12/13/23 00:58 V41230MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-10
91553 Matrix:
12/11/2023 10:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 12/13/23 00:58 V41230MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 12/13/23 00:58 V41230MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 12/13/23 00:58 V41230MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 12/13/23 00:58 V41230MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 12/13/23 00:58 V41230MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 12/13/23 00:58 V41230MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 12/13/23 00:58 V41230MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 12/13/23 00:58 V41230MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 12/13/23 00:58 V41230MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 12/13/23 00:58 V41230MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 12/13/23 00:58 V41230MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 12/13/23 00:58 V41230MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 12/13/23 00:58 V41230MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 12/13/23 00:58 V41230MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 12/13/23 00:58 V41230MSA
<42.0 µg/L 42.0 200Ethanol 1 12/13/23 00:58 V41230MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 12/13/23 00:58 V41230MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 12/13/23 00:58 V41230MSA
1.77 µg/L 0.380 1.002-Hexanone 1 12/13/23 00:58 V41230MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 12/13/23 00:58 V41230MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 12/13/23 00:58 V41230MSA
2.48 J µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 12/13/23 00:58 V41230MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-10
91553 Matrix:
12/11/2023 10:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00
0.459 J µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 12/13/23 00:58 V41230MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 12/13/23 00:58 V41230MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 12/13/23 00:58 V41230MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 12/13/23 00:58 V41230MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 12/13/23 00:58 V41230MSA
<0.220 µg/L 0.220 0.500Styrene 1 12/13/23 00:58 V41230MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 12/13/23 00:58 V41230MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 12/13/23 00:58 V41230MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 12/13/23 00:58 V41230MSA
<0.220 µg/L 0.220 0.500Toluene 1 12/13/23 00:58 V41230MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 12/13/23 00:58 V41230MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 12/13/23 00:58 V41230MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 12/13/23 00:58 V41230MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 12/13/23 00:58 V41230MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 12/13/23 00:58 V41230MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 12/13/23 00:58 V41230MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 12/13/23 00:58 V41230MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 12/13/23 00:58 V41230MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 12/13/23 00:58 V41230MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 12/13/23 00:58 V41230MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 12/13/23 00:58 V41230MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 12/13/23 00:58 V41230MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-10
91553 Matrix:
12/11/2023 10:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41227 12/12/23 14:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 12/13/23 00:58 V41230MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 12/13/23 00:58 V41230
Surrogate: 4-Bromofluorobenzene 94.0 Limits: 70-130%12/13/23 00:581 MSA V41230
Surrogate: Dibromofluoromethane 96.2 Limits: 70-130%12/13/23 00:581 MSA V41230
Surrogate: 1,2-Dichloroethane - d4 90.4 Limits: 70-130%12/13/23 00:581 MSA V41230
Surrogate: Toluene-d8 92.8 Limits: 70-130%12/13/23 00:581 MSA V41230
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-14
91554 Matrix:
12/11/2023 11:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41367 12/14/23 09:00 V41520 12/18/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 12/14/23 12:24 V41368MSA
241 µg/L 18.0 50.0Benzene 100 12/18/23 22:36 V41522ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 12/14/23 12:24 V41368MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 12/14/23 12:24 V41368MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 12/14/23 12:24 V41368MSA
<1.50 µg/L 1.50 5.00Bromoform 1 12/14/23 12:24 V41368MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 12/14/23 12:24 V41368MSA
1.91 µg/L 0.180 0.500n-Butylbenzene 1 12/14/23 12:24 V41368MSA
1.22 µg/L 0.200 0.500sec-Butyl benzene 1 12/14/23 12:24 V41368MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 12/14/23 12:24 V41368MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 12/14/23 12:24 V41368MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 12/14/23 12:24 V41368MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 12/14/23 12:24 V41368MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 12/14/23 12:24 V41368MSA
<0.220 µg/L 0.220 0.500Chloroform 1 12/14/23 12:24 V41368MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 12/14/23 12:24 V41368MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 12/14/23 12:24 V41368MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 12/14/23 12:24 V41368MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 12/14/23 12:24 V41368MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 12/14/23 12:24 V41368MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 12/14/23 12:24 V41368MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 12/14/23 12:24 V41368MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-14
91554 Matrix:
12/11/2023 11:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41367 12/14/23 09:00 V41520 12/18/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 12/14/23 12:24 V41368MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 12/14/23 12:24 V41368MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 12/14/23 12:24 V41368MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 12/14/23 12:24 V41368MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 12/14/23 12:24 V41368MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 12/14/23 12:24 V41368MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 12/14/23 12:24 V41368MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 12/14/23 12:24 V41368MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 12/14/23 12:24 V41368MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 12/14/23 12:24 V41368MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 12/14/23 12:24 V41368MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 12/14/23 12:24 V41368MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 12/14/23 12:24 V41368MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 12/14/23 12:24 V41368MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 12/14/23 12:24 V41368MSA
<42.0 µg/L 42.0 200Ethanol 1 12/14/23 12:24 V41368MSA
158 µg/L 17.0 50.0Ethylbenzene 100 12/18/23 22:36 V41522ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 12/14/23 12:24 V41368MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 12/14/23 12:24 V41368MSA
5.82 µg/L 0.180 0.500Isopropylbenzene 1 12/14/23 12:24 V41368MSA
0.795 µg/L 0.089 0.5004-Isopropyl toluene 1 12/14/23 12:24 V41368MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 12/14/23 12:24 V41368MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-14
91554 Matrix:
12/11/2023 11:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41367 12/14/23 09:00 V41520 12/18/23 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 12/14/23 12:24 V41368MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 12/14/23 12:24 V41368MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 12/14/23 12:24 V41368MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 12/14/23 12:24 V41368MSA
14.1 µg/L 0.190 0.500n-Propylbenzene 1 12/14/23 12:24 V41368MSA
<0.220 µg/L 0.220 0.500Styrene 1 12/14/23 12:24 V41368MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 12/14/23 12:24 V41368MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 12/14/23 12:24 V41368MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 12/14/23 12:24 V41368MSA
1130 µg/L 22.0 50.0Toluene 100 12/18/23 22:36 V41522ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 12/14/23 12:24 V41368MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 12/14/23 12:24 V41368MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 12/14/23 12:24 V41368MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 12/14/23 12:24 V41368MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 12/14/23 12:24 V41368MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 12/14/23 12:24 V41368MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 12/14/23 12:24 V41368MSA
164 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 12/18/23 22:36 V41522ENM
47.5 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 12/14/23 12:24 V41368MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 12/14/23 12:24 V41368MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 12/14/23 12:24 V41368MSA
242 µg/L 21.0 50.0o-Xylene 100 12/18/23 22:36 V41522ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-14
91554 Matrix:
12/11/2023 11:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41367 12/14/23 09:00 V41520 12/18/23 09:00
517 µg/L 42.0 100m,p-Xylene 100 12/18/23 22:36 V41522ENM
759 µg/L 21.0 50.0Xylene (Total)100 12/18/23 22:36 V41522
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%12/14/23 12:241 MSA V41368
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%12/14/23 12:241 MSA V41368
Surrogate: 1,2-Dichloroethane - d4 96.6 Limits: 70-130%12/14/23 12:241 MSA V41368
Surrogate: Toluene-d8 101 Limits: 70-130%12/14/23 12:241 MSA V41368
Surrogate: 4-Bromofluorobenzene 106 Limits: 70-130%12/18/23 22:36100 ENM V41522
Surrogate: Dibromofluoromethane 97.6 Limits: 70-130%12/18/23 22:36100 ENM V41522
Surrogate: 1,2-Dichloroethane - d4 89.8 Limits: 70-130%12/18/23 22:36100 ENM V41522
Surrogate: Toluene-d8 97.4 Limits: 70-130%12/18/23 22:36100 ENM V41522
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-15
91555 Matrix:
12/11/2023 10:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41367 12/14/23 09:00
<18.0 µg/L 18.0 100Acetone 10 12/14/23 17:30 V41368MSA
179 µg/L 1.80 5.00Benzene 10 12/14/23 17:30 V41368MSA
<2.10 µg/L 2.10 5.00Bromobenzene 10 12/14/23 17:30 V41368MSA
<4.20 µg/L 4.20 10.0Bromochloromethane 10 12/14/23 17:30 V41368MSA
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 12/14/23 17:30 V41368MSA
<15.0 µg/L 15.0 50.0Bromoform 10 12/14/23 17:30 V41368MSA
<2.80 µg/L 2.80 10.0Bromomethane 10 12/14/23 17:30 V41368MSA
<1.80 µg/L 1.80 5.00n-Butylbenzene 10 12/14/23 17:30 V41368MSA
<2.00 µg/L 2.00 5.00sec-Butyl benzene 10 12/14/23 17:30 V41368MSA
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 12/14/23 17:30 V41368MSA
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 12/14/23 17:30 V41368MSA
<1.90 µg/L 1.90 5.00Chlorobenzene 10 12/14/23 17:30 V41368MSA
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 12/14/23 17:30 V41368MSA
<4.30 µg/L 4.30 10.0Chloroethane 10 12/14/23 17:30 V41368MSA
<2.20 µg/L 2.20 5.00Chloroform 10 12/14/23 17:30 V41368MSA
<2.20 µg/L 2.20 5.00Chloromethane 10 12/14/23 17:30 V41368MSA
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 12/14/23 17:30 V41368MSA
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 12/14/23 17:30 V41368MSA
<5.00 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 12/14/23 17:30 V41368MSA
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 12/14/23 17:30 V41368MSA
<2.00 µg/L 2.00 5.001,2-Dibromoethane 10 12/14/23 17:30 V41368MSA
<2.30 µg/L 2.30 5.00Dibromomethane 10 12/14/23 17:30 V41368MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-15
91555 Matrix:
12/11/2023 10:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41367 12/14/23 09:00
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 12/14/23 17:30 V41368MSA
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 12/14/23 17:30 V41368MSA
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 12/14/23 17:30 V41368MSA
<12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 12/14/23 17:30 V41368MSA
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 12/14/23 17:30 V41368MSA
<1.50 µg/L 1.50 5.001,2-Dichloroethane 10 12/14/23 17:30 V41368MSA
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 12/14/23 17:30 V41368MSA
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 12/14/23 17:30 V41368MSA
<1.80 µg/L 1.80 5.00trans-1,2-Dichloroethene 10 12/14/23 17:30 V41368MSA
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 12/14/23 17:30 V41368MSA
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 12/14/23 17:30 V41368MSA
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 12/14/23 17:30 V41368MSA
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 12/14/23 17:30 V41368MSA
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 12/14/23 17:30 V41368MSA
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 12/14/23 17:30 V41368MSA
<420 µg/L 420 2000Ethanol 10 12/14/23 17:30 V41368MSA
20.3 µg/L 1.70 5.00Ethylbenzene 10 12/14/23 17:30 V41368MSA
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 12/14/23 17:30 V41368MSA
<3.80 µg/L 3.80 10.02-Hexanone 10 12/14/23 17:30 V41368MSA
6.81 µg/L 1.80 5.00Isopropylbenzene 10 12/14/23 17:30 V41368MSA
<0.890 µg/L 0.890 5.004-Isopropyl toluene 10 12/14/23 17:30 V41368MSA
<7.10 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 12/14/23 17:30 V41368MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 42 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-15
91555 Matrix:
12/11/2023 10:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41367 12/14/23 09:00
5.42 J µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 12/14/23 17:30 V41368MSA
<0.780 µg/L 0.780 10.04-Methyl-2-Pentanone 10 12/14/23 17:30 V41368MSA
<3.30 µg/L 3.30 20.0Methylene Chloride 10 12/14/23 17:30 V41368MSA
<4.70 µg/L 4.70 10.0Naphthalene 10 12/14/23 17:30 V41368MSA
<1.90 µg/L 1.90 5.00n-Propylbenzene 10 12/14/23 17:30 V41368MSA
<2.20 µg/L 2.20 5.00Styrene 10 12/14/23 17:30 V41368MSA
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 12/14/23 17:30 V41368MSA
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 12/14/23 17:30 V41368MSA
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 12/14/23 17:30 V41368MSA
12.1 µg/L 2.20 5.00Toluene 10 12/14/23 17:30 V41368MSA
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 12/14/23 17:30 V41368MSA
<3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 12/14/23 17:30 V41368MSA
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 12/14/23 17:30 V41368MSA
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 12/14/23 17:30 V41368MSA
<1.80 µg/L 1.80 5.00Trichloroethene 10 12/14/23 17:30 V41368MSA
<1.80 µg/L 1.80 5.00Trichlorofluoromethane 10 12/14/23 17:30 V41368MSA
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 12/14/23 17:30 V41368MSA
3.03 J µg/L 1.90 5.001,2,4-Trimethylbenzene 10 12/14/23 17:30 V41368MSA
2.14 J µg/L 1.80 5.001,3,5-Trimethylbenzene 10 12/14/23 17:30 V41368MSA
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 12/14/23 17:30 V41368MSA
<1.70 µg/L 1.70 5.00Vinyl Chloride 10 12/14/23 17:30 V41368MSA
3.10 J µg/L 2.10 5.00o-Xylene 10 12/14/23 17:30 V41368MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-15
91555 Matrix:
12/11/2023 10:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41367 12/14/23 09:00
14.8 µg/L 4.20 10.0m,p-Xylene 10 12/14/23 17:30 V41368MSA
17.9 J µg/L 2.10 5.00Xylene (Total)10 12/14/23 17:30 V41368
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%12/14/23 17:3010 MSA V41368
Surrogate: Dibromofluoromethane 100 Limits: 70-130%12/14/23 17:3010 MSA V41368
Surrogate: 1,2-Dichloroethane - d4 93.0 Limits: 70-130%12/14/23 17:3010 MSA V41368
Surrogate: Toluene-d8 98.6 Limits: 70-130%12/14/23 17:3010 MSA V41368
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-17
91556 Matrix:
12/11/2023 11:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41367 12/14/23 09:00
<18.0 µg/L 18.0 100Acetone 10 12/14/23 17:55 V41368MSA
2.90 J µg/L 1.80 5.00Benzene 10 12/14/23 17:55 V41368MSA
<2.10 µg/L 2.10 5.00Bromobenzene 10 12/14/23 17:55 V41368MSA
<4.20 µg/L 4.20 10.0Bromochloromethane 10 12/14/23 17:55 V41368MSA
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 12/14/23 17:55 V41368MSA
<15.0 µg/L 15.0 50.0Bromoform 10 12/14/23 17:55 V41368MSA
<2.80 µg/L 2.80 10.0Bromomethane 10 12/14/23 17:55 V41368MSA
<1.80 µg/L 1.80 5.00n-Butylbenzene 10 12/14/23 17:55 V41368MSA
<2.00 µg/L 2.00 5.00sec-Butyl benzene 10 12/14/23 17:55 V41368MSA
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 12/14/23 17:55 V41368MSA
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 12/14/23 17:55 V41368MSA
<1.90 µg/L 1.90 5.00Chlorobenzene 10 12/14/23 17:55 V41368MSA
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 12/14/23 17:55 V41368MSA
<4.30 µg/L 4.30 10.0Chloroethane 10 12/14/23 17:55 V41368MSA
<2.20 µg/L 2.20 5.00Chloroform 10 12/14/23 17:55 V41368MSA
<2.20 µg/L 2.20 5.00Chloromethane 10 12/14/23 17:55 V41368MSA
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 12/14/23 17:55 V41368MSA
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 12/14/23 17:55 V41368MSA
<5.00 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 12/14/23 17:55 V41368MSA
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 12/14/23 17:55 V41368MSA
<2.00 µg/L 2.00 5.001,2-Dibromoethane 10 12/14/23 17:55 V41368MSA
<2.30 µg/L 2.30 5.00Dibromomethane 10 12/14/23 17:55 V41368MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 45 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-17
91556 Matrix:
12/11/2023 11:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41367 12/14/23 09:00
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 12/14/23 17:55 V41368MSA
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 12/14/23 17:55 V41368MSA
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 12/14/23 17:55 V41368MSA
<12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 12/14/23 17:55 V41368MSA
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 12/14/23 17:55 V41368MSA
<1.50 µg/L 1.50 5.001,2-Dichloroethane 10 12/14/23 17:55 V41368MSA
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 12/14/23 17:55 V41368MSA
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 12/14/23 17:55 V41368MSA
<1.80 µg/L 1.80 5.00trans-1,2-Dichloroethene 10 12/14/23 17:55 V41368MSA
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 12/14/23 17:55 V41368MSA
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 12/14/23 17:55 V41368MSA
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 12/14/23 17:55 V41368MSA
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 12/14/23 17:55 V41368MSA
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 12/14/23 17:55 V41368MSA
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 12/14/23 17:55 V41368MSA
<420 µg/L 420 2000Ethanol 10 12/14/23 17:55 V41368MSA
9.27 µg/L 1.70 5.00Ethylbenzene 10 12/14/23 17:55 V41368MSA
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 12/14/23 17:55 V41368MSA
<3.80 µg/L 3.80 10.02-Hexanone 10 12/14/23 17:55 V41368MSA
<1.80 µg/L 1.80 5.00Isopropylbenzene 10 12/14/23 17:55 V41368MSA
<0.890 µg/L 0.890 5.004-Isopropyl toluene 10 12/14/23 17:55 V41368MSA
<7.10 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 12/14/23 17:55 V41368MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 46 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-17
91556 Matrix:
12/11/2023 11:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41367 12/14/23 09:00
<1.40 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 12/14/23 17:55 V41368MSA
<0.780 µg/L 0.780 10.04-Methyl-2-Pentanone 10 12/14/23 17:55 V41368MSA
<3.30 µg/L 3.30 20.0Methylene Chloride 10 12/14/23 17:55 V41368MSA
239 µg/L 4.70 10.0Naphthalene 10 12/14/23 17:55 V41368MSA
6.16 µg/L 1.90 5.00n-Propylbenzene 10 12/14/23 17:55 V41368MSA
<2.20 µg/L 2.20 5.00Styrene 10 12/14/23 17:55 V41368MSA
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 12/14/23 17:55 V41368MSA
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 12/14/23 17:55 V41368MSA
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 12/14/23 17:55 V41368MSA
24.3 µg/L 2.20 5.00Toluene 10 12/14/23 17:55 V41368MSA
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 12/14/23 17:55 V41368MSA
<3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 12/14/23 17:55 V41368MSA
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 12/14/23 17:55 V41368MSA
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 12/14/23 17:55 V41368MSA
<1.80 µg/L 1.80 5.00Trichloroethene 10 12/14/23 17:55 V41368MSA
<1.80 µg/L 1.80 5.00Trichlorofluoromethane 10 12/14/23 17:55 V41368MSA
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 12/14/23 17:55 V41368MSA
127 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 12/14/23 17:55 V41368MSA
28.4 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 12/14/23 17:55 V41368MSA
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 12/14/23 17:55 V41368MSA
<1.70 µg/L 1.70 5.00Vinyl Chloride 10 12/14/23 17:55 V41368MSA
27.2 µg/L 2.10 5.00o-Xylene 10 12/14/23 17:55 V41368MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 47 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:MW-17
91556 Matrix:
12/11/2023 11:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41367 12/14/23 09:00
32.0 µg/L 4.20 10.0m,p-Xylene 10 12/14/23 17:55 V41368MSA
59.2 µg/L 2.10 5.00Xylene (Total)10 12/14/23 17:55 V41368
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%12/14/23 17:5510 MSA V41368
Surrogate: Dibromofluoromethane 94.8 Limits: 70-130%12/14/23 17:5510 MSA V41368
Surrogate: 1,2-Dichloroethane - d4 86.6 Limits: 70-130%12/14/23 17:5510 MSA V41368
Surrogate: Toluene-d8 100 Limits: 70-130%12/14/23 17:5510 MSA V41368
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 48 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:Trip Blank
91557 Matrix:
12/11/2023 10:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41367 12/14/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 12/14/23 11:59 V41368MSA
<0.180 µg/L 0.180 0.500Benzene 1 12/14/23 11:59 V41368MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 12/14/23 11:59 V41368MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 12/14/23 11:59 V41368MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 12/14/23 11:59 V41368MSA
<1.50 µg/L 1.50 5.00Bromoform 1 12/14/23 11:59 V41368MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 12/14/23 11:59 V41368MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 12/14/23 11:59 V41368MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 12/14/23 11:59 V41368MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 12/14/23 11:59 V41368MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 12/14/23 11:59 V41368MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 12/14/23 11:59 V41368MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 12/14/23 11:59 V41368MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 12/14/23 11:59 V41368MSA
<0.220 µg/L 0.220 0.500Chloroform 1 12/14/23 11:59 V41368MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 12/14/23 11:59 V41368MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 12/14/23 11:59 V41368MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 12/14/23 11:59 V41368MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 12/14/23 11:59 V41368MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 12/14/23 11:59 V41368MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 12/14/23 11:59 V41368MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 12/14/23 11:59 V41368MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 49 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:Trip Blank
91557 Matrix:
12/11/2023 10:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41367 12/14/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 12/14/23 11:59 V41368MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 12/14/23 11:59 V41368MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 12/14/23 11:59 V41368MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 12/14/23 11:59 V41368MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 12/14/23 11:59 V41368MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 12/14/23 11:59 V41368MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 12/14/23 11:59 V41368MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 12/14/23 11:59 V41368MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 12/14/23 11:59 V41368MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 12/14/23 11:59 V41368MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 12/14/23 11:59 V41368MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 12/14/23 11:59 V41368MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 12/14/23 11:59 V41368MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 12/14/23 11:59 V41368MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 12/14/23 11:59 V41368MSA
<42.0 µg/L 42.0 200Ethanol 1 12/14/23 11:59 V41368MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 12/14/23 11:59 V41368MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 12/14/23 11:59 V41368MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 12/14/23 11:59 V41368MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 12/14/23 11:59 V41368MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 12/14/23 11:59 V41368MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 12/14/23 11:59 V41368MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 50 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:Trip Blank
91557 Matrix:
12/11/2023 10:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41367 12/14/23 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 12/14/23 11:59 V41368MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 12/14/23 11:59 V41368MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 12/14/23 11:59 V41368MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 12/14/23 11:59 V41368MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 12/14/23 11:59 V41368MSA
<0.220 µg/L 0.220 0.500Styrene 1 12/14/23 11:59 V41368MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 12/14/23 11:59 V41368MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 12/14/23 11:59 V41368MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 12/14/23 11:59 V41368MSA
<0.220 µg/L 0.220 0.500Toluene 1 12/14/23 11:59 V41368MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 12/14/23 11:59 V41368MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 12/14/23 11:59 V41368MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 12/14/23 11:59 V41368MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 12/14/23 11:59 V41368MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 12/14/23 11:59 V41368MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 12/14/23 11:59 V41368MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 12/14/23 11:59 V41368MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 12/14/23 11:59 V41368MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 12/14/23 11:59 V41368MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 12/14/23 11:59 V41368MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 12/14/23 11:59 V41368MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 12/14/23 11:59 V41368MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 51 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-345-0025
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #5398 Received : 12/11/2023
Fast Track #145
Report Date : 12/19/2023
Sample ID :
Lab No :
Sampled:Trip Blank
91557 Matrix:
12/11/2023 10:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41367 12/14/23 09:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 12/14/23 11:59 V41368MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 12/14/23 11:59 V41368
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%12/14/23 11:591 MSA V41368
Surrogate: Dibromofluoromethane 98.0 Limits: 70-130%12/14/23 11:591 MSA V41368
Surrogate: 1,2-Dichloroethane - d4 91.2 Limits: 70-130%12/14/23 11:591 MSA V41368
Surrogate: Toluene-d8 99.4 Limits: 70-130%12/14/23 11:591 MSA V41368
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 52 of 73
Quality Control Data
23-345-0025Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Track #145
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41230QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41227
Associated Lab Samples: 91547, 91548, 91549, 91550, 91552, 91553
LRB-V41227 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/12/23 22:0510.01.80<1.80µg/LAcetone
12/12/23 22:050.5000.180<0.180µg/LBenzene
12/12/23 22:050.5000.210<0.210µg/LBromobenzene
12/12/23 22:051.000.420<0.420µg/LBromochloromethane
12/12/23 22:050.5000.160<0.160µg/LBromodichloromethane
12/12/23 22:055.001.50<1.50µg/LBromoform
12/12/23 22:051.000.280<0.280µg/LBromomethane
12/12/23 22:050.5000.180<0.180µg/Ln-Butylbenzene
12/12/23 22:050.5000.200<0.200µg/Lsec-Butyl benzene
12/12/23 22:052.000.920<0.920µg/Ltert-Butyl benzene
12/12/23 22:050.5000.180<0.180µg/LCarbon Tetrachloride
12/12/23 22:050.5000.190<0.190µg/LChlorobenzene
12/12/23 22:050.5000.190<0.190µg/LChlorodibromomethane
12/12/23 22:051.000.430<0.430µg/LChloroethane
12/12/23 22:050.5000.220<0.220µg/LChloroform
12/12/23 22:050.5000.220<0.220µg/LChloromethane
12/12/23 22:050.5000.200<0.200µg/L2-Chlorotoluene
12/12/23 22:050.5000.200<0.200µg/L4-Chlorotoluene
12/12/23 22:050.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
12/12/23 22:052.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
12/12/23 22:050.5000.200<0.200µg/L1,2-Dibromoethane
12/12/23 22:050.5000.230<0.230µg/LDibromomethane
12/12/23 22:050.5000.220<0.220µg/L1,2-Dichlorobenzene
12/12/23 22:050.5000.190<0.190µg/L1,3-Dichlorobenzene
12/12/23 22:050.5000.210<0.210µg/L1,4-Dichlorobenzene
12/12/23 22:055.001.20<1.20µg/LDichlorodifluoromethane
12/12/23 22:050.5000.240<0.240µg/L1,1-Dichloroethane
Page 1 of 18Date:12/19/2023 04:18 PM
Page 53 of 73
Quality Control Data
23-345-0025Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Track #145
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41230QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41227
Associated Lab Samples: 91547, 91548, 91549, 91550, 91552, 91553
LRB-V41227 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/12/23 22:050.5000.150<0.150µg/L1,2-Dichloroethane
12/12/23 22:050.5000.150<0.150µg/L1,1-Dichloroethene
12/12/23 22:050.5000.200<0.200µg/Lcis-1,2-Dichloroethene
12/12/23 22:050.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
12/12/23 22:050.5000.190<0.190µg/L1,2-Dichloropropane
12/12/23 22:050.5000.130<0.130µg/L1,3-Dichloropropane
12/12/23 22:052.000.210<0.210µg/L2,2-Dichloropropane
12/12/23 22:050.5000.200<0.200µg/L1,1-Dichloropropene
12/12/23 22:050.5000.210<0.210µg/Lcis-1,3-Dichloropropene
12/12/23 22:050.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
12/12/23 22:0520042.0<42.0µg/LEthanol
12/12/23 22:050.5000.170<0.170µg/LEthylbenzene
12/12/23 22:053.000.350<0.350µg/LHexachlorobutadiene
12/12/23 22:051.000.380<0.380µg/L2-Hexanone
12/12/23 22:050.5000.180<0.180µg/LIsopropylbenzene
12/12/23 22:050.5000.089<0.089µg/L4-Isopropyl toluene
12/12/23 22:055.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
12/12/23 22:051.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
12/12/23 22:051.000.078<0.078µg/L4-Methyl-2-Pentanone
12/12/23 22:052.000.330<0.330µg/LMethylene Chloride
12/12/23 22:051.000.470<0.470µg/LNaphthalene
12/12/23 22:050.5000.190<0.190µg/Ln-Propylbenzene
12/12/23 22:050.5000.220<0.220µg/LStyrene
12/12/23 22:050.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
12/12/23 22:050.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
12/12/23 22:050.5000.220<0.220µg/LTetrachloroethene
12/12/23 22:050.5000.220<0.220µg/LToluene
Page 2 of 18Date:12/19/2023 04:18 PM
Page 54 of 73
Quality Control Data
23-345-0025Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Track #145
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41230QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41227
Associated Lab Samples: 91547, 91548, 91549, 91550, 91552, 91553
LRB-V41227 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/12/23 22:050.5000.380<0.380µg/L1,2,3-Trichlorobenzene
12/12/23 22:050.5000.310<0.310µg/L1,2,4-Trichlorobenzene
12/12/23 22:050.5000.160<0.160µg/L1,1,1-Trichloroethane
12/12/23 22:050.5000.096<0.096µg/L1,1,2-Trichloroethane
12/12/23 22:050.5000.180<0.180µg/LTrichloroethene
12/12/23 22:050.5000.180<0.180µg/LTrichlorofluoromethane
12/12/23 22:050.5000.270<0.270µg/L1,2,3-Trichloropropane
12/12/23 22:050.5000.190<0.190µg/L1,2,4-Trimethylbenzene
12/12/23 22:050.5000.180<0.180µg/L1,3,5-Trimethylbenzene
12/12/23 22:055.001.00<1.00µg/LVinyl Acetate
12/12/23 22:050.5000.170<0.170µg/LVinyl Chloride
12/12/23 22:050.5000.210<0.210µg/Lo-Xylene
12/12/23 22:051.000.420<0.420µg/Lm,p-Xylene
12/12/23 22:054-Bromofluorobenzene (S)95.0 70-130
12/12/23 22:05Dibromofluoromethane (S)96.4 70-130
12/12/23 22:051,2-Dichloroethane - d4 (S)93.6 70-130
12/12/23 22:05Toluene-d8 (S)92.4 70-130
LCS-V41227 LCSD-V41227Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
70.5 176*174*69.740.0µg/LAcetone 40-160 1.1 20.0
23.3 11711923.720.0µg/LBenzene 70-130 1.7 20.0
20.8 10410520.920.0µg/LBromobenzene 70-130 0.4 20.0
23.0 11511422.820.0µg/LBromochloromethane 70-130 0.8 20.0
22.1 11111222.420.0µg/LBromodichloromethane 70-130 1.3 20.0
Page 3 of 18* QC Fail Date:12/19/2023 04:18 PM
Page 55 of 73
Quality Control Data
23-345-0025Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Track #145
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41230QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41227
LCS-V41227 LCSD-V41227Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.2 10110220.320.0µg/LBromoform 70-130 0.4 20.0
22.9 11511422.720.0µg/LBromomethane 60-140 0.8 20.0
19.9 99.510120.220.0µg/Ln-Butylbenzene 70-130 1.4 20.0
20.5 10310521.020.0µg/Lsec-Butyl benzene 70-130 2.4 20.0
20.7 10410521.020.0µg/Ltert-Butyl benzene 70-130 1.4 20.0
19.7 98.598.519.720.0µg/LCarbon Tetrachloride 70-130 0.0 20.0
22.2 11111122.220.0µg/LChlorobenzene 70-130 0.0 20.0
21.8 10910921.820.0µg/LChlorodibromomethane 70-130 0.0 20.0
32.8 164*169*33.820.0µg/LChloroethane 60-140 3.0 20.0
22.2 11111122.220.0µg/LChloroform 70-130 0.0 20.0
27.6 138141*28.220.0µg/LChloromethane 60-140 2.1 20.0
20.4 10210520.920.0µg/L2-Chlorotoluene 70-130 2.4 20.0
20.8 10410621.120.0µg/L4-Chlorotoluene 70-130 1.4 20.0
26.4 132*133*26.620.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.7 20.0
23.4 11711422.720.0µg/L1,2-Dibromo-3-Chloropropane 70-130 3.0 20.0
21.9 11011322.520.0µg/L1,2-Dibromoethane 70-130 2.7 20.0
23.0 11511422.820.0µg/LDibromomethane 70-130 0.8 20.0
21.7 10910921.720.0µg/L1,2-Dichlorobenzene 70-130 0.0 20.0
21.3 10711021.920.0µg/L1,3-Dichlorobenzene 70-130 2.7 20.0
21.7 10911021.920.0µg/L1,4-Dichlorobenzene 70-130 0.9 20.0
15.9 79.581.016.220.0µg/LDichlorodifluoromethane 60-140 1.8 20.0
23.3 11711923.720.0µg/L1,1-Dichloroethane 70-130 1.7 20.0
21.3 10710521.020.0µg/L1,2-Dichloroethane 70-130 1.4 20.0
22.2 11111322.520.0µg/L1,1-Dichloroethene 70-130 1.3 20.0
22.7 11411522.920.0µg/Lcis-1,2-Dichloroethene 70-130 0.8 20.0
22.5 11311623.220.0µg/Ltrans-1,2-Dichloroethene 70-130 3.0 20.0
Page 4 of 18* QC Fail Date:12/19/2023 04:18 PM
Page 56 of 73
Quality Control Data
23-345-0025Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Track #145
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41230QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41227
LCS-V41227 LCSD-V41227Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
24.2 12112324.620.0µg/L1,2-Dichloropropane 70-130 1.6 20.0
21.5 10810821.620.0µg/L1,3-Dichloropropane 70-130 0.4 20.0
18.1 90.592.018.420.0µg/L2,2-Dichloropropane 70-130 1.6 20.0
22.5 11311823.520.0µg/L1,1-Dichloropropene 70-130 4.3 20.0
22.4 11211222.420.0µg/Lcis-1,3-Dichloropropene 70-130 0.0 20.0
21.8 10911021.920.0µg/Ltrans-1,3-Dichloropropene 70-130 0.4 20.0
636 127118588500µg/LEthanol 60-140 7.8 20.0
20.8 10410621.120.0µg/LEthylbenzene 70-130 1.4 20.0
17.7 88.591.018.220.0µg/LHexachlorobutadiene 70-130 2.7 20.0
27.5 13813927.720.0µg/L2-Hexanone 60-140 0.7 20.0
20.7 10410621.220.0µg/LIsopropylbenzene 70-130 2.3 20.0
20.2 10110320.620.0µg/L4-Isopropyl toluene 70-130 1.9 20.0
28.5 143*143*28.620.0µg/LMethyl Ethyl Ketone (MEK)60-140 0.3 20.0
22.4 11211222.420.0µg/LMethyl tert-butyl ether (MTBE)70-130 0.0 20.0
27.5 13813927.720.0µg/L4-Methyl-2-Pentanone 60-140 0.7 20.0
22.1 11111222.420.0µg/LMethylene Chloride 70-130 1.3 20.0
23.0 11511923.720.0µg/LNaphthalene 70-130 2.9 20.0
20.7 10410621.220.0µg/Ln-Propylbenzene 70-130 2.3 20.0
21.8 10911222.420.0µg/LStyrene 70-130 2.7 20.0
21.4 10710921.720.0µg/L1,1,1,2-Tetrachloroethane 70-130 1.3 20.0
19.6 98.010020.020.0µg/L1,1,2,2-Tetrachloroethane 70-130 2.0 20.0
21.6 10811122.120.0µg/LTetrachloroethene 70-130 2.2 20.0
23.1 11611723.320.0µg/LToluene 70-130 0.8 20.0
24.5 12312524.920.0µg/L1,2,3-Trichlorobenzene 70-130 1.6 20.0
20.9 10510821.620.0µg/L1,2,4-Trichlorobenzene 70-130 3.2 20.0
20.8 10410520.920.0µg/L1,1,1-Trichloroethane 70-130 0.4 20.0
Page 5 of 18* QC Fail Date:12/19/2023 04:18 PM
Page 57 of 73
Quality Control Data
23-345-0025Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Track #145
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41230QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41227
LCS-V41227 LCSD-V41227Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
23.1 11611623.220.0µg/L1,1,2-Trichloroethane 70-130 0.4 20.0
25.8 12913025.920.0µg/LTrichloroethene 70-130 0.3 20.0
22.9 11511422.720.0µg/LTrichlorofluoromethane 60-140 0.8 20.0
20.2 10110120.120.0µg/L1,2,3-Trichloropropane 70-130 0.4 20.0
20.4 10210320.620.0µg/L1,2,4-Trimethylbenzene 70-130 0.9 20.0
20.2 10110420.720.0µg/L1,3,5-Trimethylbenzene 70-130 2.4 20.0
15.6 78.078.015.620.0µg/LVinyl Acetate 60-140 0.0 20.0
27.8 139143*28.520.0µg/LVinyl Chloride 60-140 2.4 20.0
21.3 10710921.820.0µg/Lo-Xylene 70-130 2.3 20.0
43.1 10810943.740.0µg/Lm,p-Xylene 70-130 1.3 20.0
96.695.84-Bromofluorobenzene (S)70-130
96.496.2Dibromofluoromethane (S)70-130
92.292.21,2-Dichloroethane - d4 (S)70-130
93.492.8Toluene-d8 (S)70-130
Page 6 of 18* QC Fail Date:12/19/2023 04:18 PM
Page 58 of 73
Quality Control Data
23-345-0025Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Track #145
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41368QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41367
Associated Lab Samples: 91550, 91554, 91555, 91556, 91557
LRB-V41367 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/14/23 11:3310.01.80<1.80µg/LAcetone
12/14/23 11:330.5000.180<0.180µg/LBenzene
12/14/23 11:330.5000.210<0.210µg/LBromobenzene
12/14/23 11:331.000.420<0.420µg/LBromochloromethane
12/14/23 11:330.5000.160<0.160µg/LBromodichloromethane
12/14/23 11:335.001.50<1.50µg/LBromoform
12/14/23 11:331.000.280<0.280µg/LBromomethane
12/14/23 11:330.5000.180<0.180µg/Ln-Butylbenzene
12/14/23 11:330.5000.200<0.200µg/Lsec-Butyl benzene
12/14/23 11:332.000.920<0.920µg/Ltert-Butyl benzene
12/14/23 11:330.5000.180<0.180µg/LCarbon Tetrachloride
12/14/23 11:330.5000.190<0.190µg/LChlorobenzene
12/14/23 11:330.5000.190<0.190µg/LChlorodibromomethane
12/14/23 11:331.000.430<0.430µg/LChloroethane
12/14/23 11:330.5000.220<0.220µg/LChloroform
12/14/23 11:330.5000.220<0.220µg/LChloromethane
12/14/23 11:330.5000.200<0.200µg/L2-Chlorotoluene
12/14/23 11:330.5000.200<0.200µg/L4-Chlorotoluene
12/14/23 11:330.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
12/14/23 11:332.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
12/14/23 11:330.5000.200<0.200µg/L1,2-Dibromoethane
12/14/23 11:330.5000.230<0.230µg/LDibromomethane
12/14/23 11:330.5000.220<0.220µg/L1,2-Dichlorobenzene
12/14/23 11:330.5000.190<0.190µg/L1,3-Dichlorobenzene
12/14/23 11:330.5000.210<0.210µg/L1,4-Dichlorobenzene
12/14/23 11:335.001.20<1.20µg/LDichlorodifluoromethane
12/14/23 11:330.5000.240<0.240µg/L1,1-Dichloroethane
Page 7 of 18Date:12/19/2023 04:18 PM
Page 59 of 73
Quality Control Data
23-345-0025Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Track #145
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41368QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41367
Associated Lab Samples: 91550, 91554, 91555, 91556, 91557
LRB-V41367 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/14/23 11:330.5000.150<0.150µg/L1,2-Dichloroethane
12/14/23 11:330.5000.150<0.150µg/L1,1-Dichloroethene
12/14/23 11:330.5000.200<0.200µg/Lcis-1,2-Dichloroethene
12/14/23 11:330.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
12/14/23 11:330.5000.190<0.190µg/L1,2-Dichloropropane
12/14/23 11:330.5000.130<0.130µg/L1,3-Dichloropropane
12/14/23 11:332.000.210<0.210µg/L2,2-Dichloropropane
12/14/23 11:330.5000.200<0.200µg/L1,1-Dichloropropene
12/14/23 11:330.5000.210<0.210µg/Lcis-1,3-Dichloropropene
12/14/23 11:330.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
12/14/23 11:3320042.0<42.0µg/LEthanol
12/14/23 11:330.5000.170<0.170µg/LEthylbenzene
12/14/23 11:333.000.350<0.350µg/LHexachlorobutadiene
12/14/23 11:331.000.380<0.380µg/L2-Hexanone
12/14/23 11:330.5000.180<0.180µg/LIsopropylbenzene
12/14/23 11:330.5000.089<0.089µg/L4-Isopropyl toluene
12/14/23 11:335.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
12/14/23 11:331.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
12/14/23 11:331.000.078<0.078µg/L4-Methyl-2-Pentanone
12/14/23 11:332.000.330<0.330µg/LMethylene Chloride
12/14/23 11:331.000.470<0.470µg/LNaphthalene
12/14/23 11:330.5000.190<0.190µg/Ln-Propylbenzene
12/14/23 11:330.5000.220<0.220µg/LStyrene
12/14/23 11:330.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
12/14/23 11:330.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
12/14/23 11:330.5000.220<0.220µg/LTetrachloroethene
12/14/23 11:330.5000.220<0.220µg/LToluene
Page 8 of 18Date:12/19/2023 04:18 PM
Page 60 of 73
Quality Control Data
23-345-0025Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Track #145
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41368QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41367
Associated Lab Samples: 91550, 91554, 91555, 91556, 91557
LRB-V41367 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/14/23 11:330.5000.380<0.380µg/L1,2,3-Trichlorobenzene
12/14/23 11:330.5000.310<0.310µg/L1,2,4-Trichlorobenzene
12/14/23 11:330.5000.160<0.160µg/L1,1,1-Trichloroethane
12/14/23 11:330.5000.096<0.096µg/L1,1,2-Trichloroethane
12/14/23 11:330.5000.180<0.180µg/LTrichloroethene
12/14/23 11:330.5000.180<0.180µg/LTrichlorofluoromethane
12/14/23 11:330.5000.270<0.270µg/L1,2,3-Trichloropropane
12/14/23 11:330.5000.190<0.190µg/L1,2,4-Trimethylbenzene
12/14/23 11:330.5000.180<0.180µg/L1,3,5-Trimethylbenzene
12/14/23 11:335.001.00<1.00µg/LVinyl Acetate
12/14/23 11:330.5000.170<0.170µg/LVinyl Chloride
12/14/23 11:330.5000.210<0.210µg/Lo-Xylene
12/14/23 11:331.000.420<0.420µg/Lm,p-Xylene
12/14/23 11:334-Bromofluorobenzene (S)102 70-130
12/14/23 11:33Dibromofluoromethane (S)97.6 70-130
12/14/23 11:331,2-Dichloroethane - d4 (S)88.6 70-130
12/14/23 11:33Toluene-d8 (S)99.8 70-130
LCS-V41367 LCSD-V41367Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
43.7 10911445.640.0µg/LAcetone 40-160 4.2 20.0
20.1 10110521.020.0µg/LBenzene 70-130 4.3 20.0
20.6 10310521.020.0µg/LBromobenzene 70-130 1.9 20.0
20.6 10310420.820.0µg/LBromochloromethane 70-130 0.9 20.0
19.9 99.510120.120.0µg/LBromodichloromethane 70-130 1.0 20.0
Page 9 of 18Date:12/19/2023 04:18 PM
Page 61 of 73
Quality Control Data
23-345-0025Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Track #145
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41368QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41367
LCS-V41367 LCSD-V41367Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.9 10510521.020.0µg/LBromoform 70-130 0.4 20.0
17.5 87.595.019.020.0µg/LBromomethane 60-140 8.2 20.0
21.2 10611022.020.0µg/Ln-Butylbenzene 70-130 3.7 20.0
20.3 10210320.620.0µg/Lsec-Butyl benzene 70-130 1.4 20.0
19.7 98.510220.320.0µg/Ltert-Butyl benzene 70-130 3.0 20.0
20.2 10110520.920.0µg/LCarbon Tetrachloride 70-130 3.4 20.0
20.6 10310621.220.0µg/LChlorobenzene 70-130 2.8 20.0
21.2 10611222.320.0µg/LChlorodibromomethane 70-130 5.0 20.0
20.6 10310120.220.0µg/LChloroethane 60-140 1.9 20.0
20.3 10210120.220.0µg/LChloroform 70-130 0.4 20.0
20.0 10011122.220.0µg/LChloromethane 60-140 10.4 20.0
20.6 10310420.720.0µg/L2-Chlorotoluene 70-130 0.4 20.0
20.4 10210520.920.0µg/L4-Chlorotoluene 70-130 2.4 20.0
20.4 10210520.920.0µg/LDi-Isopropyl Ether (DIPE)70-130 2.4 20.0
22.3 112136*27.120.0µg/L1,2-Dibromo-3-Chloropropane 70-130 19.4 20.0
20.8 10410921.820.0µg/L1,2-Dibromoethane 70-130 4.6 20.0
19.4 97.097.519.520.0µg/LDibromomethane 70-130 0.5 20.0
21.1 10610921.720.0µg/L1,2-Dichlorobenzene 70-130 2.8 20.0
21.2 10610621.220.0µg/L1,3-Dichlorobenzene 70-130 0.0 20.0
19.7 98.510320.520.0µg/L1,4-Dichlorobenzene 70-130 3.9 20.0
16.2 81.082.016.420.0µg/LDichlorodifluoromethane 60-140 1.2 20.0
19.9 99.510320.520.0µg/L1,1-Dichloroethane 70-130 2.9 20.0
19.7 98.510320.520.0µg/L1,2-Dichloroethane 70-130 3.9 20.0
19.8 99.010120.120.0µg/L1,1-Dichloroethene 70-130 1.5 20.0
20.1 10110120.120.0µg/Lcis-1,2-Dichloroethene 70-130 0.0 20.0
20.5 10310420.720.0µg/Ltrans-1,2-Dichloroethene 70-130 0.9 20.0
Page 10 of 18* QC Fail Date:12/19/2023 04:18 PM
Page 62 of 73
Quality Control Data
23-345-0025Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Track #145
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41368QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41367
LCS-V41367 LCSD-V41367Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.7 10410621.120.0µg/L1,2-Dichloropropane 70-130 1.9 20.0
20.3 10210821.520.0µg/L1,3-Dichloropropane 70-130 5.7 20.0
19.1 95.510721.420.0µg/L2,2-Dichloropropane 70-130 11.3 20.0
21.6 10811222.420.0µg/L1,1-Dichloropropene 70-130 3.6 20.0
19.5 97.510420.720.0µg/Lcis-1,3-Dichloropropene 70-130 5.9 20.0
19.3 96.510320.620.0µg/Ltrans-1,3-Dichloropropene 70-130 6.5 20.0
499 99.8110549500µg/LEthanol 60-140 9.5 20.0
18.9 94.598.519.720.0µg/LEthylbenzene 70-130 4.1 20.0
21.8 10910721.320.0µg/LHexachlorobutadiene 70-130 2.3 20.0
20.1 10110320.520.0µg/L2-Hexanone 60-140 1.9 20.0
20.6 10310420.820.0µg/LIsopropylbenzene 70-130 0.9 20.0
20.8 10410521.020.0µg/L4-Isopropyl toluene 70-130 0.9 20.0
21.8 10911523.020.0µg/LMethyl Ethyl Ketone (MEK)60-140 5.3 20.0
20.5 10310320.620.0µg/LMethyl tert-butyl ether (MTBE)70-130 0.4 20.0
20.3 10210521.020.0µg/L4-Methyl-2-Pentanone 60-140 3.3 20.0
19.9 99.510320.520.0µg/LMethylene Chloride 70-130 2.9 20.0
21.7 10911021.920.0µg/LNaphthalene 70-130 0.9 20.0
20.0 10010120.120.0µg/Ln-Propylbenzene 70-130 0.4 20.0
20.0 10010721.320.0µg/LStyrene 70-130 6.2 20.0
21.4 10711422.720.0µg/L1,1,1,2-Tetrachloroethane 70-130 5.8 20.0
19.8 99.010721.320.0µg/L1,1,2,2-Tetrachloroethane 70-130 7.2 20.0
19.9 99.510420.720.0µg/LTetrachloroethene 70-130 3.9 20.0
20.3 10210420.720.0µg/LToluene 70-130 1.9 20.0
20.1 10111322.620.0µg/L1,2,3-Trichlorobenzene 70-130 11.7 20.0
19.4 97.010220.320.0µg/L1,2,4-Trichlorobenzene 70-130 4.5 20.0
20.1 10110621.120.0µg/L1,1,1-Trichloroethane 70-130 4.8 20.0
Page 11 of 18Date:12/19/2023 04:18 PM
Page 63 of 73
Quality Control Data
23-345-0025Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Track #145
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41368QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41367
LCS-V41367 LCSD-V41367Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.9 10510921.820.0µg/L1,1,2-Trichloroethane 70-130 4.2 20.0
21.2 10610821.520.0µg/LTrichloroethene 70-130 1.4 20.0
19.0 95.097.019.420.0µg/LTrichlorofluoromethane 60-140 2.0 20.0
20.8 10495.519.120.0µg/L1,2,3-Trichloropropane 70-130 8.5 20.0
20.4 10210420.820.0µg/L1,2,4-Trimethylbenzene 70-130 1.9 20.0
20.3 10210420.720.0µg/L1,3,5-Trimethylbenzene 70-130 1.9 20.0
22.7 11412825.620.0µg/LVinyl Acetate 60-140 12.0 20.0
21.3 10710921.720.0µg/LVinyl Chloride 60-140 1.8 20.0
20.2 10110621.120.0µg/Lo-Xylene 70-130 4.3 20.0
41.4 10410642.440.0µg/Lm,p-Xylene 70-130 2.3 20.0
99.097.64-Bromofluorobenzene (S)70-130
10199.6Dibromofluoromethane (S)70-130
95.696.01,2-Dichloroethane - d4 (S)70-130
99.699.2Toluene-d8 (S)70-130
Page 12 of 18Date:12/19/2023 04:18 PM
Page 64 of 73
Quality Control Data
23-345-0025Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Track #145
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41522QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41520
Associated Lab Samples: 91551, 91554
LRB-V41520 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/18/23 14:3110.01.80<1.80µg/LAcetone
12/18/23 14:310.5000.180<0.180µg/LBenzene
12/18/23 14:310.5000.210<0.210µg/LBromobenzene
12/18/23 14:311.000.420<0.420µg/LBromochloromethane
12/18/23 14:310.5000.160<0.160µg/LBromodichloromethane
12/18/23 14:315.001.50<1.50µg/LBromoform
12/18/23 14:311.000.280<0.280µg/LBromomethane
12/18/23 14:310.5000.180<0.180µg/Ln-Butylbenzene
12/18/23 14:310.5000.200<0.200µg/Lsec-Butyl benzene
12/18/23 14:312.000.920<0.920µg/Ltert-Butyl benzene
12/18/23 14:310.5000.180<0.180µg/LCarbon Tetrachloride
12/18/23 14:310.5000.190<0.190µg/LChlorobenzene
12/18/23 14:310.5000.190<0.190µg/LChlorodibromomethane
12/18/23 14:311.000.430<0.430µg/LChloroethane
12/18/23 14:310.5000.220<0.220µg/LChloroform
12/18/23 14:310.5000.220<0.220µg/LChloromethane
12/18/23 14:310.5000.200<0.200µg/L2-Chlorotoluene
12/18/23 14:310.5000.200<0.200µg/L4-Chlorotoluene
12/18/23 14:310.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
12/18/23 14:312.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
12/18/23 14:310.5000.200<0.200µg/L1,2-Dibromoethane
12/18/23 14:310.5000.230<0.230µg/LDibromomethane
12/18/23 14:310.5000.220<0.220µg/L1,2-Dichlorobenzene
12/18/23 14:310.5000.190<0.190µg/L1,3-Dichlorobenzene
12/18/23 14:310.5000.210<0.210µg/L1,4-Dichlorobenzene
12/18/23 14:315.001.20<1.20µg/LDichlorodifluoromethane
12/18/23 14:310.5000.240<0.240µg/L1,1-Dichloroethane
Page 13 of 18Date:12/19/2023 04:18 PM
Page 65 of 73
Quality Control Data
23-345-0025Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Track #145
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41522QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41520
Associated Lab Samples: 91551, 91554
LRB-V41520 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/18/23 14:310.5000.150<0.150µg/L1,2-Dichloroethane
12/18/23 14:310.5000.150<0.150µg/L1,1-Dichloroethene
12/18/23 14:310.5000.200<0.200µg/Lcis-1,2-Dichloroethene
12/18/23 14:310.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
12/18/23 14:310.5000.190<0.190µg/L1,2-Dichloropropane
12/18/23 14:310.5000.130<0.130µg/L1,3-Dichloropropane
12/18/23 14:312.000.210<0.210µg/L2,2-Dichloropropane
12/18/23 14:310.5000.200<0.200µg/L1,1-Dichloropropene
12/18/23 14:310.5000.210<0.210µg/Lcis-1,3-Dichloropropene
12/18/23 14:310.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
12/18/23 14:3120042.0<42.0µg/LEthanol
12/18/23 14:310.5000.170<0.170µg/LEthylbenzene
12/18/23 14:313.000.350<0.350µg/LHexachlorobutadiene
12/18/23 14:311.000.380<0.380µg/L2-Hexanone
12/18/23 14:310.5000.180<0.180µg/LIsopropylbenzene
12/18/23 14:310.5000.089<0.089µg/L4-Isopropyl toluene
12/18/23 14:315.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
12/18/23 14:311.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
12/18/23 14:311.000.078<0.078µg/L4-Methyl-2-Pentanone
12/18/23 14:312.000.330<0.330µg/LMethylene Chloride
12/18/23 14:311.000.470<0.470µg/LNaphthalene
12/18/23 14:310.5000.190<0.190µg/Ln-Propylbenzene
12/18/23 14:310.5000.220<0.220µg/LStyrene
12/18/23 14:310.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
12/18/23 14:310.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
12/18/23 14:310.5000.220<0.220µg/LTetrachloroethene
12/18/23 14:310.5000.220<0.220µg/LToluene
Page 14 of 18Date:12/19/2023 04:18 PM
Page 66 of 73
Quality Control Data
23-345-0025Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Track #145
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41522QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41520
Associated Lab Samples: 91551, 91554
LRB-V41520 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/18/23 14:310.5000.380<0.380µg/L1,2,3-Trichlorobenzene
12/18/23 14:310.5000.310<0.310µg/L1,2,4-Trichlorobenzene
12/18/23 14:310.5000.160<0.160µg/L1,1,1-Trichloroethane
12/18/23 14:310.5000.096<0.096µg/L1,1,2-Trichloroethane
12/18/23 14:310.5000.180<0.180µg/LTrichloroethene
12/18/23 14:310.5000.180<0.180µg/LTrichlorofluoromethane
12/18/23 14:310.5000.270<0.270µg/L1,2,3-Trichloropropane
12/18/23 14:310.5000.190<0.190µg/L1,2,4-Trimethylbenzene
12/18/23 14:310.5000.180<0.180µg/L1,3,5-Trimethylbenzene
12/18/23 14:315.001.00<1.00µg/LVinyl Acetate
12/18/23 14:310.5000.170<0.170µg/LVinyl Chloride
12/18/23 14:310.5000.210<0.210µg/Lo-Xylene
12/18/23 14:311.000.420<0.420µg/Lm,p-Xylene
12/18/23 14:314-Bromofluorobenzene (S)100 70-130
12/18/23 14:31Dibromofluoromethane (S)97.0 70-130
12/18/23 14:311,2-Dichloroethane - d4 (S)91.0 70-130
12/18/23 14:31Toluene-d8 (S)99.0 70-130
LCS-V41520 LCSD-V41520Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
50.0 12511144.340.0µg/LAcetone 40-160 12.0 20.0
19.2 96.010120.220.0µg/LBenzene 70-130 5.0 20.0
19.6 98.098.519.720.0µg/LBromobenzene 70-130 0.5 20.0
20.2 10110521.020.0µg/LBromochloromethane 70-130 3.8 20.0
19.7 98.510220.420.0µg/LBromodichloromethane 70-130 3.4 20.0
Page 15 of 18Date:12/19/2023 04:18 PM
Page 67 of 73
Quality Control Data
23-345-0025Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Track #145
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41522QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41520
LCS-V41520 LCSD-V41520Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.0 10510420.720.0µg/LBromoform 70-130 1.4 20.0
17.9 89.592.518.520.0µg/LBromomethane 60-140 3.2 20.0
20.5 10310721.420.0µg/Ln-Butylbenzene 70-130 4.2 20.0
19.5 97.510120.220.0µg/Lsec-Butyl benzene 70-130 3.5 20.0
18.7 93.598.519.720.0µg/Ltert-Butyl benzene 70-130 5.2 20.0
19.5 97.510520.920.0µg/LCarbon Tetrachloride 70-130 6.9 20.0
19.9 99.510420.820.0µg/LChlorobenzene 70-130 4.4 20.0
20.8 10410320.520.0µg/LChlorodibromomethane 70-130 1.4 20.0
19.8 99.010220.420.0µg/LChloroethane 60-140 2.9 20.0
19.3 96.510120.120.0µg/LChloroform 70-130 4.0 20.0
19.2 96.010120.120.0µg/LChloromethane 60-140 4.5 20.0
19.2 96.010120.220.0µg/L2-Chlorotoluene 70-130 5.0 20.0
19.4 97.010120.120.0µg/L4-Chlorotoluene 70-130 3.5 20.0
19.3 96.510120.120.0µg/LDi-Isopropyl Ether (DIPE)70-130 4.0 20.0
24.6 12312825.520.0µg/L1,2-Dibromo-3-Chloropropane 70-130 3.5 20.0
20.8 10410020.020.0µg/L1,2-Dibromoethane 70-130 3.9 20.0
19.1 95.597.519.520.0µg/LDibromomethane 70-130 2.0 20.0
21.1 10610320.520.0µg/L1,2-Dichlorobenzene 70-130 2.8 20.0
20.5 10310520.920.0µg/L1,3-Dichlorobenzene 70-130 1.9 20.0
19.1 95.598.519.720.0µg/L1,4-Dichlorobenzene 70-130 3.0 20.0
15.0 75.078.015.620.0µg/LDichlorodifluoromethane 60-140 3.9 20.0
19.4 97.010120.120.0µg/L1,1-Dichloroethane 70-130 3.5 20.0
19.1 95.593.018.620.0µg/L1,2-Dichloroethane 70-130 2.6 20.0
19.6 98.010420.820.0µg/L1,1-Dichloroethene 70-130 5.9 20.0
18.9 94.599.519.920.0µg/Lcis-1,2-Dichloroethene 70-130 5.1 20.0
19.1 95.510521.020.0µg/Ltrans-1,2-Dichloroethene 70-130 9.4 20.0
Page 16 of 18Date:12/19/2023 04:18 PM
Page 68 of 73
Quality Control Data
23-345-0025Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Track #145
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41522QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41520
LCS-V41520 LCSD-V41520Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.0 10010320.620.0µg/L1,2-Dichloropropane 70-130 2.9 20.0
20.8 10410020.020.0µg/L1,3-Dichloropropane 70-130 3.9 20.0
19.6 98.010520.920.0µg/L2,2-Dichloropropane 70-130 6.4 20.0
21.4 10711022.020.0µg/L1,1-Dichloropropene 70-130 2.7 20.0
19.4 97.099.519.920.0µg/Lcis-1,3-Dichloropropene 70-130 2.5 20.0
19.2 96.010420.720.0µg/Ltrans-1,3-Dichloropropene 70-130 7.5 20.0
492 98.485.6428500µg/LEthanol 60-140 13.9 20.0
18.1 90.596.019.220.0µg/LEthylbenzene 70-130 5.8 20.0
21.6 10811122.120.0µg/LHexachlorobutadiene 70-130 2.2 20.0
21.9 11010921.820.0µg/L2-Hexanone 60-140 0.4 20.0
19.4 97.010220.320.0µg/LIsopropylbenzene 70-130 4.5 20.0
20.1 10110320.620.0µg/L4-Isopropyl toluene 70-130 2.4 20.0
26.4 13213326.520.0µg/LMethyl Ethyl Ketone (MEK)60-140 0.3 20.0
20.6 10310320.520.0µg/LMethyl tert-butyl ether (MTBE)70-130 0.4 20.0
20.5 10310220.320.0µg/L4-Methyl-2-Pentanone 60-140 0.9 20.0
18.0 90.095.019.020.0µg/LMethylene Chloride 70-130 5.4 20.0
23.1 11611623.120.0µg/LNaphthalene 70-130 0.0 20.0
19.0 95.099.519.920.0µg/Ln-Propylbenzene 70-130 4.6 20.0
19.1 95.510120.120.0µg/LStyrene 70-130 5.1 20.0
20.7 10410120.220.0µg/L1,1,1,2-Tetrachloroethane 70-130 2.4 20.0
19.7 98.510420.820.0µg/L1,1,2,2-Tetrachloroethane 70-130 5.4 20.0
19.8 99.010821.520.0µg/LTetrachloroethene 70-130 8.2 20.0
19.3 96.510120.120.0µg/LToluene 70-130 4.0 20.0
22.1 11112124.220.0µg/L1,2,3-Trichlorobenzene 70-130 9.0 20.0
20.7 10410621.120.0µg/L1,2,4-Trichlorobenzene 70-130 1.9 20.0
19.8 99.010420.820.0µg/L1,1,1-Trichloroethane 70-130 4.9 20.0
Page 17 of 18Date:12/19/2023 04:18 PM
Page 69 of 73
Quality Control Data
23-345-0025Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Track #145
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41522QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41520
LCS-V41520 LCSD-V41520Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.9 99.510520.920.0µg/L1,1,2-Trichloroethane 70-130 4.9 20.0
19.9 99.510420.820.0µg/LTrichloroethene 70-130 4.4 20.0
20.0 10010220.320.0µg/LTrichlorofluoromethane 60-140 1.4 20.0
20.8 10490.518.120.0µg/L1,2,3-Trichloropropane 70-130 13.8 20.0
19.4 97.099.519.920.0µg/L1,2,4-Trimethylbenzene 70-130 2.5 20.0
19.5 97.599.519.920.0µg/L1,3,5-Trimethylbenzene 70-130 2.0 20.0
23.2 11612424.720.0µg/LVinyl Acetate 60-140 6.2 20.0
20.6 10310621.220.0µg/LVinyl Chloride 60-140 2.8 20.0
19.3 96.598.019.620.0µg/Lo-Xylene 70-130 1.5 20.0
38.9 97.210240.740.0µg/Lm,p-Xylene 70-130 4.5 20.0
97.296.44-Bromofluorobenzene (S)70-130
101100Dibromofluoromethane (S)70-130
95.296.21,2-Dichloroethane - d4 (S)70-130
98.699.0Toluene-d8 (S)70-130
Page 18 of 18Date:12/19/2023 04:18 PM
Page 70 of 73
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-345-0025
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 4.1C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:12/11/2023 17:31:51
Special precautions or instructions included?
Comments:
Page 71 of 73
Page 72 of 73
Page 73 of 73

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

12/20/2023
Geological Resources, Inc. Joanna Alley
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-345-0024 Client Project Description: Fast Track #145
GRI #5398
Dear Joanna Alley:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 12/11/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 12
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Page 1 of 1 00016/23-345-0024
Page 2 of 12
Report Number:
Sample Summary Table
Client Project Description:
23-345-0024
Fast Track #145
GRI #5398
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
12/11/2023 07:55Air 91546 AIR 12/11/2023 16:14 SUBCONTRACT AES
AES: Analytical Environmental Services, Inc., Atlanta, GA
Page 3 of 12
December 15, 2023
LABORATORY REPORT NUMBER
PROJECT ID
Primary Data Review By
Project Manager, AES
2312C04
Terri W Cole
Waypoint Analytical
449 Springbrook Road
Charlotte NC 28217
23-345-0024
Chris Pafford Project Manager, Access
Analytical
Ashley Amick
PLEASE NOTE:
-Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc.
(AES Inc), 3080 Presidential Drive, Atlanta, GA 30340.
-AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab #
FL-E87582, NELAP certified laboratory # E87582
- AIHA-LAP,LLC Laboratory ID:100671 for Industrial Hygiene samples (Organics, Metals, PCM
Asbestos, Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental
Microbiology (Fungal) Direct Examination.
- Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a
representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be
directed
Secondary Data Review By
ATTENTION
DATE
CLIENT
ANALYTICAL REPORT
Page 1 of 7Page 4 of 12
Page 2 of 7Page 5 of 12
Analytical Results
for
18-Dec-23Date:
Workorder:
Client Reference:
Qual Date Analyzed
/Analyst
Reportin
gLimit
(ug)
Concentration
Total
(ug)
(mg/m3) (ppm)
Analyte
2312C04
Waypoint Analytical
23-345-0024
Front
(ug)
Back
(ug)
Test
Method
12/11/2023Lab ID:91546 Tedlar Bag 1Air Vol.(L):Media:Client ID:2312C04-001A Date Sampled:
<3.1<10Benzene <10 10 EPA1812/14/2023 BHI<10 <10
<2.3<10Ethylbenzene <10 10 EPA1812/14/2023 BHI<10 <10
<4.6<20m,p-Xylene <20 20 EPA1812/14/2023 BHI<20 <20
<2.3<10o-Xylene <10 10 EPA1812/14/2023 BHI<10 <10
<2.6<10Toluene <10 10 EPA1812/14/2023 BHI<10 <10
<250TPH (Gasoline) <250 250 SW8015BM12/14/2023 BHI<250 <250
<31<100TRPH (Based on Benzene) <100 100 EPA1812/14/2023 BHI<100 <100
93 Surr:1,4 Difluorobenzene 93 0 SW8015BM12/14/2023 BHI92.744
Qualifiers:
< Less than the indicated Reporting Limit
H Holding time for preparation or analysis
B Analyte detected in the associated Method Blank
(a) Analysis indicates possible breakthrough; back section result is greater than % of the front section result.10
Page 3 of 7Page 6 of 12



 

 !" !#$%
&
'
(
)
*
+
,

-./
/0
12034

/
/2/454

%
46789:;<=7:>?:767>?@78"ABC:D7 8:;"E 7FGFH7ID?:D7;E;:;?C JK7 !" !#$&
'
(
)
+


%
&
'
(
46789:;<=7:>?:767>?@78"ABC:D7 8:;"E 7FLGMN7ID?:D7;E;:;?C JK7 !" !#$)
*
+
O!":P7Q9:?;E7?E?C=  79RS;978>A;8?C7B9 9@?:;"E7TS:7AS :7T78>8UD7;E7:>7C?T"9?:"9=7?ED7E":7SB"E7V?ABC7W8;B:7 S8>7? 7Q"C;<"9A X7YZQ 7?ED7Z;C7[7\9? #]^_K7]>; 7?C "7`8CSD 7A:?C 7T=7a^$7MbbKcX7MbbKd7?ED7MLeKF7f>;8>7f;CC7T7@9;<;D7T:fE7FN7?ED7ML7>"S9 7?<:97B9 9@?:;"EK6789:;<=7:>?:767>?@78"ABC:D7 8:;"E 7McGMgID?:D7;E;:;?C JK7V$h^ia#QZZiaW7WaQa6^]7Q_aQji6V]k:?;C Q"AAE: 22l0
m00nl0o 

l
l2
p4q34.,r(stuvwxyyvz{y|v}~v€ v{y|‚y ƒ{„ yv y…€ †z‡ˆ‰Š‹4Œ4
424422l0
o4Œ4
4
0422l0
o
.4Œpq24o
.4Œ4l1
1
3 4
0no
2

m4l
o
4
240n3lo/
/
o/2
stvvvvvvvvvvvvvt€€Žy v v y|‚y ƒ{„ yvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvstvvvvvvvvvvvvvt€€Žy v‘v y|‚y ƒ{„ yvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvstvvvvvvvvvvvvvt€€Žy v’v y|‚y ƒ{„ yvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvst'/2
stvvvvvvvvvvvvvt€€Žy v“v y|‚y ƒ{„ yvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvstvvvvvvvvvvvvvt€€Žy v”v y|‚y ƒ{„ yvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvstvvvvvvvvvvvvvt€€Žy v•v y|‚y ƒ{„ yvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvstk:?;C Q"AAE: 4
20
4
0202o/2

424o4Œ4
4244
20
4o4Œ4
4
04
20
4o*
–4
20

4
0o 02.l



Œ44 40
o,

.4
2440no 4
240n44
2440n
44
200
mo–30n4..04
2n.0


Œ44o4
240n
222
0
4o—
4
240n3
42
0p˜m&™qo2
44o 44]>; 7 8:;"E7"EC=7?BBC; 7:"7 ?ABC 7f>97B_78?E7T78>8UD7?:7V?ABC7W8;B:K77 k:?;C Q"AAE: š
n0
4l00
24n
00oO
424n
l4o
42š
›4

2œ02o04)
&
%œn&šžžŸ  ¡š¢£¤¥¦§ž£¤¨¡©¢ž ª«¬ª­®¯°±²³´µ¶·¸¹º»¼½»¼½¼¾¿Àº»¼½»¼½¼¾¿Àº»¼½»¼½¼¾ÁÂÃÄÅÆ ÇÄÈÃÆÄÉÊËÌÍÃÎPage 4 of 7Page 7 of 12
15-Dec-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name
ANALYTICAL QC SUMMARY REPORT
23-345-0024
2312C04
Waypoint Analytical
368149
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID: Analysis Date: Seq No:TestCode:368149MBLK12/14/2023Aromatic Volatiles in Air EPA18
Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 12/12/2023 533580MB-368149
12680566
Benzene 10BRL
Ethylbenzene 10BRL
m,p-Xylene 20BRL
o-Xylene 10BRL
Toluene 10BRL
TRPH (Based on Benzene) 100BRL
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID: Analysis Date: Seq No:TestCode:368149MBLK12/14/20238015M SW8015CM
Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 12/12/2023 533581MB-368149
12680784
TPH (Gasoline)250BRL
Surr: 1,4 Difluorobenzene 097.37 100.0 97.4 66 121
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID: Analysis Date: Seq No:TestCode:368149LCS 12/14/2023Aromatic Volatiles in Air EPA18
Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 12/12/2023 533580LCS-368149
12680567
Benzene 10111.7 100.0 112 83.7 128
Ethylbenzene 10121.6 100.0 122 85 135
m,p-Xylene 20235.8 200.0 118 85 131
o-Xylene 10113.2 100.0 113 81.9 128
Toluene 10115.3 100.0 115 85 130
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID: Analysis Date: Seq No:TestCode:368149LCS 12/14/20238015M SW8015CM
Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 12/12/2023 533581LCS-368149-2
12680785
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit
Page 5 of 7Page 8 of 12
15-Dec-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name
ANALYTICAL QC SUMMARY REPORT
23-345-0024
2312C04
Waypoint Analytical
368149
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID: Analysis Date: Seq No:TestCode:368149LCS12/14/20238015M SW8015CM
Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 12/12/2023 533581LCS-368149-2
12680785
TPH (Gasoline)2501133 1000 113 84.6 125
Surr: 1,4 Difluorobenzene 0100.0 100.0 100 66 121
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID: Analysis Date: Seq No:TestCode:368149LCSD 12/14/2023Aromatic Volatiles in Air EPA18
Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 12/12/2023 533580LCSD-368149
12680568
Benzene 10115.8 15100.0 116 83.7 128 111.7 3.65
Ethylbenzene 10125.8 15100.0 126 85 135 121.6 3.41
m,p-Xylene 20244.0 15200.0 122 85 131 235.8 3.41
o-Xylene 10117.1 15100.0 117 81.9 128 113.2 3.35
Toluene 10119.5 15100.0 119 85 130 115.3 3.54
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID: Analysis Date: Seq No:TestCode:368149LCSD 12/14/20238015M SW8015CM
Units: Prep Date:Sample ID: Client ID:Run No:ug, Total 12/12/2023 533581LCSD-368149-2
12680786
TPH (Gasoline)2501144 201000 114 84.6 125 1133 1.04
Surr: 1,4 Difluorobenzene 0102.1 0100.0 102 66 121 100.0 0
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit
Page 6 of 7Page 9 of 12

End of Report
Page 7 of 7Page 10 of 12
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-345-0024
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 4.1C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:12/11/2023 17:27:06
Special precautions or instructions included?
Comments:
Page 11 of 12
Page 12 of 12

APPENDIX F
O&M Field Data Sheets

APPENDIX G
Overall Remediation Costs
Date: 10/19/23 Facility ID #: 0-031674
Claim Number Task Code Task Code Description Cost Claim Amount
3.101 Supervision of Field Work $5,037.50
3.113 Installation of 2-inch Well $13,500.00
3.114 Installation of 4-inch Well $7,980.00
3.118 Temporary Impact Increase $2,015.00
3.397 Temporary Impact Increase $100.00
3.398 Cost for Drill Rig Mobization $350.00
3.500 Driller Per Diem $1,354.00
4.031 Cost for Sampling Wells $1,331.00
4.051 Cost for Sampling Surface Water $50.00
4.090 Cost for Analytical $1,594.00
6.090 Ground Water Monitoring Report $2,250.00
7.040 Cost for SVE System $58,234.75
7.060 Cost for Air Sparge System $58,234.75
7.081 Remediation System Installation Inspection $5,208.00
7.100 Cost for Installation of Remediation System $99,025.00
7.201 Cost for Scheduled Maintenance $3,324.75
7.250 Cost for Remediation Supplies and Equipment $296.77
7.260 Cost for Remediation Operating Expenses
(assumed, pending receipt of all power bills)$1,422.08
8.055 Injection Notice of Intent $500.00
12.030 Overnight Lodging $453.00
12.050 Consultant Travel $4,250.00
12.055 Temporary Impact Increase $850.00
4.031 Cost for Sampling Wells $1,661.00
4.090 Cost for Analytical $1,877.00
6.090 Ground Water Monitoring Report $2,250.00
7.201 Cost for Scheduled Maintenance $728.19
7.260 Cost for Remediation Operating Expenses
(assumed, pending receipt of all power bills)$6,600.00
12.050 Consultant Travel $1,500.00
12.055 Temporary Impact Increase $300.00
$282,276.79Total Cost Since System Installation
APPENDIX G
OVERALL REMEDIATION COSTS (TO DATE)
FAST TRACK #145 (INCIDENT NO. 40099)
211 $267,360.60
(claim has not
been
submitted)
$14,916.19
Page 1 of 1

APPENDIX H
Contaminant Mass Calculations
Area ID Well ID Area
(ft²)
Average Well
Depth
(ft.)
Average
Depth to
Water
(ft.)
Water Column
Height
(ft)
Volume
(ft³)
Volume
(L)
Effective
Porosity
Effective
Volume
(L)
MW-1
MW-6
MW-4
MW-8
MW-9
MW-15
3 MW-3 79,994 39 26.36 12.64 1,011,126 28,631,858 5,726,372
Area Date Well Benzene
(μg/L)
Toluene
(μg/L)
Ethylbenzene
(μg/L)
Xylenes
(μg/L)
MTBE
(μg/L)
Naphthalene
(μg/L)
Total
(μg/L)
DTW
(ft.)
Average Water
Column Height
(ft.)
Total Average Mass
(g)Percent Red. To Date Red.
MW-1 13500.00 9640.00 1670.00 6570.00 225.00 409.00 32014.00 27.96
MW-6 504.00 25500.00 3510.00 15260.00 0.00 504.00 45278.00 27.98
Avg.7002.00 17570.00 2590.00 10915.00 112.50 456.50 38646.00 27.97
MW-1 2560.00 6180.00 1790.00 7230.00 0.00 362.00 18122.00 23.86
MW-6 12900.00 43700.00 2910.00 14700.00 0.00 509.00 74719.00 22.46
Avg.7730.00 24940.00 2350.00 10965.00 0.00 435.50 46420.50 23.16
MW-1 104.00 1970.00 1260.00 6030.00 25.50 257.00 9646.50 23.34
MW-6 8110.00 21200.00 1670.00 8560.00 0.00 274.00 39814.00 21.53
Avg.4107.00 11585.00 1465.00 7295.00 12.75 265.50 24730.25 22.44
MW-1 2250 11500 2000 10600 0.00 421 26771.00 25.66
MW-6 11200 44000 3300 17800 0.00 662 38481.00 24.96
Avg.6725.00 27750.00 2650.00 14200.00 0.00 541.50 32626.00 25.31
MW-1 1750 3370 1420 4880 40.10 493 11953.10 26.79
MW-6 9380 33100 2790 14000 0.00 698 29984.00 26.61
Avg.5565.00 18235.00 2105.00 9440.00 20.05 595.50 20968.55 26.70
MW-1 1840 4550 486 3770 0.00 969 10646.00 30.77
MW-6 8850 23100 1940 10900 0.00 588 44790.00 24.28
Avg.5345.00 13825.00 1213.00 7335.00 0.00 778.50 27718.00 27.53
MW-1 828.00 1,700.00 232.00 1,380.00 0.00 940.00 5080.00 32.55
MW-6 8790.00 28100.00 2640.00 14300.00 0.00 730 53830.00 27.11
Avg.4809.00 14900.00 1436.00 7840.00 0.00 835.00 29,455.00 29.83
MW-1 3380 6810 832 4290 0 302 15614.00 32.05
MW-6 10200 39500 3280 15500 0 824 69304.00 27.76
Avg. 6790.00 23155.00 2056.00 9895.00 0.00 563.00 42,459.00 29.91
Area 1
-43.1%7.1%
APPENDIX H
CONTAMINANT MASS CALCULATIONS
FAST TRACK #145 (INCIDENT NO. 40099)
76,258.29 ------
18.07
-66.2%
25.7%
2
-66.2%
Baseline Event
1 27,807 40.5 27.97 1,973,252
02/14/22
07/02/20 126,762.37
-2.3%15.19 78,046.43 -10.9%
-24.3%12.98 56,637.0606/12/23
12/11/23 10.60 70,843.85
12.53
44.5% 7.7%
17.34
40.2%
70,355.48
11/13/12 -
03/12/13
9.9715.032536,642
06/08/21
11/10/22 13.80 45,569.99 41.6%
2,068,966365,325 10,344,830 0.20
12.53 348,424 9,866,259
09/21/23 10.67 49,494.26 12.6% 35.1%
Area ID Well ID Area
(ft²)
Average Well
Depth
(ft.)
Average
Depth to
Water
(ft.)
Water Column
Height
(ft)
Volume
(ft³)
Volume
(L)
Effective
Porosity
Effective
Volume
(L)
MW-1
MW-6
MW-4
MW-8
MW-9
MW-15
3 MW-3 79,994 39 26.36 12.64 1,011,126 28,631,858 5,726,372
Area Date Well Benzene
(μg/L)
Toluene
(μg/L)
Ethylbenzene
(μg/L)
Xylenes
(μg/L)
MTBE
(μg/L)
Naphthalene
(μg/L)
Total
(μg/L)
DTW
(ft.)
Average Water
Column Height
(ft.)
Total Average Mass
(g)Percent Red. To Date Red.
APPENDIX H
CONTAMINANT MASS CALCULATIONS
FAST TRACK #145 (INCIDENT NO. 40099)
2
Baseline Event
1 27,807 40.5 27.97 1,973,252
9.9715.032536,642 2,068,966365,325 10,344,830 0.20
12.53 348,424 9,866,259
MW-8 9540.00 21300.00 3030.00 14120.00 0.00 336.00 48326.00 28.41
MW-9 1200.00 18.90 13.40 29.16 5.31 39.10 1305.87 1.65
Avg.5370.00 10659.45 1521.70 7074.58 2.66 187.55 49631.87 15.03
MW-8 5650.00 33800.00 3090.00 16300.00 0.00 635.00 59475.00 25.02
MW-9 51.00 1.90 2.30 0.00 0.00 2.50 57.70 1.91
Avg.2850.50 16900.95 1546.15 8150.00 0.00 318.75 29766.35 13.47
MW-8 8620.00 36500.00 3270.00 18100.00 0.00 512.00 67002.00 24.47
MW-9 51.00 1.90 2.30 0.00 0.00 2.50 57.70 1.91
Avg.4335.50 18250.95 1636.15 9050.00 0.00 257.25 33529.85 13.19
MW-4 1940.00 1250.00 2580.00 4460.00 0.00 551.00 10781.00 6.96
MW-8 3840.00 68800.00 14500.00 81200.00 0.00 8460.00 176800.00 27.23
MW-9 0.00 0.00 0.00 0.00 0.00 0.74 0.74 1.54
MW-15 10.30 0.56 1.30 1.50 1.50 0.90 16.06 2.35
Avg.1447.58 17512.64 4270.33 21415.38 0.38 2253.16 46899.45 9.52
MW-4 NM NM NM NM NM NM NM NM
MW-8 4010.00 39100.00 3620.00 17900.00 0.00 771.00 65401.00 29.58
MW-9 0.00 0.00 0.00 0.00 0.00 0.00 0.00 1.76
MW-15 0.53 0.00 0.00 0.00 0.79 0.00 1.32 2.48
Avg.1336.84 13033.33 1206.67 5966.67 0.26 257.00 21800.77 11.27
MW-4 NM NM NM NM NM NM NM NM
MW-8 NM NM NM NM NM NM NM NM
MW-9 NM NM NM NM NM NM NM NM
MW-15 NM NM NM NM NM NM NM NM
Avg.NM NM NM NM NM NM NM NM
MW-4 NM NM NM NM NM NM NM NM
MW-8 NM NM NM NM NM NM NM NM
MW-9 NM NM NM NM NM NM NM NM
MW-15 NM NM NM NM NM NM NM NM
Avg.NM NM NM NM NM NM NM NM
MW-4 6770 1470 2900 4140 91.7 655 16026.70 8.01
MW-8 0 21.8 12.7 94.7 0 466 595.20 25.63
MW-9 17.1 2.57 5.77 0.752 0.733 2.26 29.19 2.02
MW-15 179 12.1 20.3 17.9 5.42 0 234.72 2.62
Avg. 1741.53 376.62 734.69 1063.34 24.46 280.82 4221.45 9.57
Area 2
12/11/23 15.43 13,517.17 78.2% 86.8%
03/12/13 102,686.65 --- ---9.97
71,252.7111.54
-46.7%
11/10/22 13.73 62,100.51 58.8% 39.5%
30.6%
06/08/21 82,175.0011.81
39.5%
-83.3%
30.6%
06/12/23 62,100.51 0.0%13.73
-15.3%
07/02/20
09/21/23 13.73 62,100.51 0.0% 39.5%
15.48 150,659.6302/14/22
20.0%
Area ID Well ID Area
(ft²)
Average Well
Depth
(ft.)
Average
Depth to
Water
(ft.)
Water Column
Height
(ft)
Volume
(ft³)
Volume
(L)
Effective
Porosity
Effective
Volume
(L)
MW-1
MW-6
MW-4
MW-8
MW-9
MW-15
3 MW-3 79,994 39 26.36 12.64 1,011,126 28,631,858 5,726,372
Area Date Well Benzene
(μg/L)
Toluene
(μg/L)
Ethylbenzene
(μg/L)
Xylenes
(μg/L)
MTBE
(μg/L)
Naphthalene
(μg/L)
Total
(μg/L)
DTW
(ft.)
Average Water
Column Height
(ft.)
Total Average Mass
(g)Percent Red. To Date Red.
APPENDIX H
CONTAMINANT MASS CALCULATIONS
FAST TRACK #145 (INCIDENT NO. 40099)
2
Baseline Event
1 27,807 40.5 27.97 1,973,252
9.9715.032536,642 2,068,966365,325 10,344,830 0.20
12.53 348,424 9,866,259
11/13/12 164.00 20.00 23.50 36.50 2.38 3.06 249.44 26.36 12.64 1,428.39 ------
07/02/20 23.20 0.76 5.80 1.70 0.00 6.50 37.96 21.05 17.95 308.69 78.4%78.4%
06/08/21 25.30 0.41 8.80 0.44 0.00 6.10 41.05 20.15 18.85 350.56 -13.6%75.5%
02/14/22 26.1 0 1.3 0 0 6.6 34.00 23.69 15.31 235.82 32.7% 83.5%
11/10/22 39.7 0.621 1.89 0.706 1.62 9.23 53.77 25.24 13.76 335.17 -42.1%76.5%
06/12/23 34.6 3.76 1.81 10.6 1.1 11.3 63.17 24.28 14.72 421.26 -25.7%70.5%
09/21/23 29.40 3.07 1.24 9.36 0.00 6.8 49.87 25.58 13.42 303.20 28.0% 78.8%
12/11/23 17.3 1.65 0.608 4.13 0.413 4.57 28.67 25.64 13.36 173.53 42.8% 87.9%
Date
Average Water
Column Height
(ft.)
11/13/12 11.71
07/02/20 15.61
06/08/21 16.24
02/14/22 15.33
11/10/22 13.76
06/12/23 13.81
09/21/23 13.42
12/11/23 13.13
Notes:
• Area of the contaminant plume is calculated from Figure #6
• The January 2014 CSA report ground water data was used to create the baseline event for the purposes of this calculation. Ground water samples were collected on 11/13/12 and 3/12/13.
• Height of the water column is calculated by subtracting the average depth to water from the average well depth of the referenced monitoring wells
• Volume of the contaminant plume is calculated by multiplying the area of the plume by the average height of the water column during each sampling event
• Effective porosity is assumed based on the sub-surface soil profile obtained from well construction records and soil boring logs
• Total mass was calculated by multiplying the total contaminant concentrations for the sampling event with effective volume
• When areas couldn’t be sampled, the last known concentrations were used in the calculations.
• Monitoring wells MW-4 and MW-15 were not included in the baseline sampling event and are not included in the baseline water column height.
Area 3 MW-3
84,535 24.5%53.1%
---
119,159 -10.3%33.9%
-10.0% -10.0%
-26.9%-49.8%228,942
15.2%
108,006 52.8%40.1%
152,881 22.9%
198,324
Total Contaminant Mass
(g)Percent Reduction To Date
111,898 6.1%38.0%
Percent Reduction Compared
to Previous Event
---180,373