MO-9227_40741_CA_CAFS_20240227

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
February 27, 2024

Mr. Brad Newton
NCDEQ-UST Section
Mooresville Regional Office
610 East Center Ave.
Mooresville, NC 28115

Re: Corrective Action Feasibility Study – Pilot Study
October 2023 - January 2024
Ganesha Food Mart
1617 North Chester Street
Gastonia, Gaston County
North Carolina
Facility ID Number: 0-00-0000015835
Incident Number: 40741
GRI Project Number: 4457

Dear Mr. Newton,

Please find enclosed the referenced report for the above-mentioned site.
If you have any questions, please contact Rae Brown at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Ganesha Food Mart, file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Corrective Action Feasibility Study – Pilot Study
October 2023 – January 2024
Ganesha Food Mart
1617 North Chester Street
Gastonia, Gaston County
North Carolina
Facility ID Number: 0-00-0000015835
Incident Number: 40741
GRI Project Number: 4457

Prepared for:

Ganesha Food Mart
1617 North Chester Street
Gastonia, North Carolina 28052

February 27, 2024

Rae Troiano Brown, P.G.
Project Manager
Rohit Shetty, P.E.
Report Reviewer

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Feasibility Study – Pilot Study
Prepared on: February 27, 2024 Ganesha Food Mart
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 4457
i
SITE INFORMATION

1. Site Identification
 Ganesha Food Mart (Facility ID 0-00-0000015835)
 Incident Number 40741 – Intermediate Risk (I165A)
 Location of Source Area: 1617 North Chester Street
Gastonia, NC 28075
Gaston County
35.280688°N, 81.188480°W (Topographical Map)

2. Information about Contacts Associated with the Leaking UST System

UST Owner
Janki Khyati, Inc.
1617 North Chester Street
Gastonia, NC 28052
[e-mail]
704-906-9443

UST Operator
Ganesha Food Mart
1617 North Chester Street
Gastonia, NC 28052
[e-mail]
704-906-9443

Property Owner
Janki Khyati, LLC
7676 Orchard Park Circle
Harrisburg, NC 28075
[e-mail]
704-906-9443

Property Occupant
Ganesha Food Mart
1617 North Chester Street
Gastonia, NC 28052
[e-mail]
704-906-9443

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
Waypoint Analytical, LLC
449 Springbrook Road
Charlotte, NC 28217
State Certification No. 402
704-529-6364
3. Information about Release
 1995 (Incident 13392); 2017 (Incident 40741).
 An unknown amount of product was released from the leaking UST System.
 Three 10,000-gallon gasoline, one 6,000-gallon diesel, and one 6,000-gallon kerosene USTs and
associated pumps and product piping are active at the site. In 1995, a release was reported at the
site and assigned Incident No. 13392.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Feasibility Study – Pilot Study
Prepared on: February 27, 2024 Ganesha Food Mart
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 4457
ii
EXECUTIVE SUMMARY
Ganesha Food Mart is located at 1617 North Chester Street in Gastonia, Gaston County, North Carolina.
The site is currently owned by Janki Khyati, LLC and is operated by Ganesha Food Mart as a petroleum
retail facility. Currently, three 10,000-gallon gasoline, one 6,000-gallon diesel, and one 6,000-gallon
kerosene USTs are active at the site.

In 1995, a release was reported at the site, classified as high risk, and assigned Incident No. 13392; Exxon
Mobil was identified as the Responsible Party. In July 2021, an NFA was issued for Incident No. 13392.
Responsibility for the remaining on-site and off-site contamination was assigned to Ganesha Food Mart
(Incident 40741). Clean up goals for Incident 40741 were defined to be less than GCLs because there is
no complete pathway to the surface water body located within 500 feet of the site. The adjoining
properties are commercial properties. According to the information determined during receptor survey
activities, no water supply wells were identified within 1,500 feet of the site. Public water is available to
the site and surrounding properties within a 1,500-foot radius of the site. Therefore, Incident 40741 is
classified as intermediate risk.

The NCDEQ required installation of a passive skimming system at the Site. On September 23, 2020, an
F.A.P. Plus Zero Water Pump System manufactured by Durham Geo Slope Indicator was installed in
monitoring well GMW-3. Per the direction of the NCDEQ, the system was de-activated in April 2021,
reactivated in February 2022, and deactivated in February 2023.

A Feasibility Study was conducted; and, based on the available technologies, site-specific conditions, and
limitations of the other technologies, the NCDEQ approved the ISCO via vertical injection points as the
preferred conceptual remedial approach to eliminate free product and lower contaminant concentrations
in ground water below the GCLs in a time- and cost-effective manner.

Between October 25 and 30, 2023, as part of the pilot test, 33 injection points were installed on-site (Area
A) and 11 injection points were installed off-site (Area B). A total of 3,960 gallons of chemical oxidation
compound (Cool-Ox®) were injected into the injection points within the areas of concern.

As part of the pilot study, ground water samples were collected from select monitoring wells 30- and 60
days subsequent to the injection event; 90-days after injection, a comprehensive sampling event was
conducted. Concentrations of individual BTEX constituents, MTBE, naphthalene, TAA, TBA, EDB, 1,2
dichloroethane, ethanol, 2-hexanone, isopropylbenzene, di-isopropyl ether, n-propylbenzene, styrene,
1,2,4-trimethylbenzene, and/or 1,3,5-trimethylbenzene that exceeded the MACs were reported in GMW-
4 and MW-21. Concentrations of benzene and EDB in MW-21 exceeded the GCLs.

From May 2023 (pre-injection) to January 2024 (post-injection), contaminant mass has decreased 84.5%
in Area A and increased 35.5% in Area B. Please note that the average total contaminant concentrations
in Area B (MW-18 and MW-21) have decreased when compared to December 2021 data but the average
height of the water column has increased in Area B. This increase in water column height (and therefore

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Feasibility Study – Pilot Study
Prepared on: February 27, 2024 Ganesha Food Mart
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 4457
iii
contaminant volume) may be contributing to an increase in overall contaminant mass in this area. The
lack of contaminant mass reduction from the ISCO event is likely because only six of the eleven temporary
wells were successfully installed due to a subsurface impediment.

Based on these data, a ground water sampling event should be conducted in June 2024 to confirm no GCL
violations remain on-site and evaluate any continued effects from the ISCO event off-site. The decision to
conduct additional injection events will be based on an evaluation of the June 2024 ground water quality
data. If a declining trend of contaminant reduction is observed in the off-site area, additional injections
may not be required.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Feasibility Study – Pilot Study
Prepared on: February 27, 2024 Ganesha Food Mart
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 4457
iv
ACRONYMS
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DOT: Department of Transportation
DPT: Direct Push Technology
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
ISCO: In-Situ Chemical Oxidation
ITC: Innovative Technology Committee
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
ROW: Right of way
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Feasibility Study – Pilot Study
Prepared on: February 27, 2024 Ganesha Food Mart
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 4457
TABLE OF CONTENTS
SITE INFORMATION ............................................................................................................................ i
EXECUTIVE SUMMARY ....................................................................................................................... ii
ACRONYMS ....................................................................................................................................... iv
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 ISCO PILOT TEST ......................................................................................................................2
3.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................4
4.0 FREE PRODUCT REMOVAL ........................................................................................................7
5.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................7
6.0 CONCLUSIONS .........................................................................................................................7
7.0 LIMITATIONS ...........................................................................................................................9

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Injectant Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map
Figure 6: Benzene Isoconcentration Map
Figure 7: EDB Isoconcentration Map
Figure 8: Estimated Contaminant Mass Area Map

TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Well Construction and Gauging Information
Table 4: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: State Correspondence
Appendix B: DOT Permit and RTE
Appendix C: Health and Safety Plans and Utility Maps
Appendix D: Well Construction Logs and Permits
Appendix E: Deep Earth Field Injection Sheets
Appendix F: Notice of Intent and Injection Event Record
Appendix G: Laboratory Analytical Report
Appendix H: Contaminant Mass Reduction Calculations

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Feasibility Study – Pilot Study
Prepared on: February 27, 2024 Ganesha Food Mart
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 4457
1
1.0 SITE HISTORY AND CHARACTERIZATION
The Ganesha Food Mart site is located at 1617 North Chester Street in Gastonia, Gaston County, North
Carolina (Figure 1).

The site is currently owned by Janki Khyati, LLC and is operated by Ganesha Food Mart as a petroleum
retail facility and convenience store. Currently, three 10,000-gallon gasoline, one 6,000-gallon diesel, and
one 6,000-gallon kerosene USTs are active at the site. UST owner/operator information and UST system
information are included as Tables 1 and 2, respectively. The Registered Tank Report is shown below:

In 1995, a release was reported at the site, classified as high risk, and assigned Incident No. 13392; Exxon
Mobil was identified as the Responsible Party. In July 2021, an NFA was issued for Incident No. 13392.
Responsibility for the remaining on-site and off-site contamination was assigned to Ganesha Food Mart
(Incident 40741). Clean up goals for Incident 40741 were defined to be less than GCLs because there is
no complete pathway to the surface water body located within 500 feet of the site. The adjoining
properties are commercial properties. According to the information determined during receptor survey
activities, no water supply wells were identified within 1,500 feet of the site. Public water is available to
the site and surrounding properties within a 1,500-foot radius of the site. Therefore, Incident 40741 is
classified as intermediate risk.

Four Type II monitoring wells (GMW-1 through GMW-4) were installed at the site for the Ganesha Food
Mart (Incident 40741) during 2018 Site Check activities. Several Type II monitoring wells (MW-1, MW-
1R/MMPE-3, MW-2, MW-2R/MMPE-1, MW-3 through MW-20, OB-1, and MMPE-2) and one Type III
monitoring well (DW-1) were installed at the site during previous ground water assessment activities
conducted by Exxon (Incident 13392). Ganesha Food Mart obtained permission from Exxon to access

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Feasibility Study – Pilot Study
Prepared on: February 27, 2024 Ganesha Food Mart
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 4457
2
monitoring wells MMPE-2 and MMPE-3. A Site Map showing the locations of the monitoring wells and
the structures on-site has been included as Figure 2.

On June 1, 2020, the NCDEQ determined that a free product skimming system must be installed at
Ganesha Food Mart. On September 23, 2020, GRI installed an F.A.P. Plus Zero Water Pump System
manufactured by Durham Geo Slope Indicator in monitoring well GMW-3. Monthly O&M events were
conducted from October 2020 until the NCDEQ directed de-activating the system in April 2021. Per the
direction of the NCDEQ, the system was de-activated in April 2021 and reactivated in February 2022 and
deactivated in February 2023.

A Feasibility Study was conducted and the NCDEQ approved injection of a chemicaloxidation reagent
(Cool-Ox®) as the preferred remedial strategy to eliminate free product and lower contaminant
concentrations in ground water to below the GCLs in a time- and cost-effective manner. A Pilot Study was
proposed and outlined in the Correction Action Feasibility Study Report (June 2022).

GRI presents the results of the Pilot Study and the subsequent sampling events conducted in November
and December 2023 and January 2024. These activities were conducted in accordance with GRI Proposal
No. 23-393, which was submitted to the NCDEQ on August 23, 2023 and was approved as Task
Authorization No. 40741-22 on August 25, 2023. State correspondence has been included as Appendix
A.
2.0 ISCO PILOT TEST
From October 25 through October 30, 2023, DeepEarth Technologies, Inc. (DeepEarth) and GRI personnel
conducted the ISCO pilot test. Based on previous ground water data, two injection areas were selected.
Copies of RTE and DOT ROW permits are included in Appendix B. Copies of the Health and Safety plans
and subsurface utility location maps are included in Appendix C.

Thirty-three injection points (IP-12 through IP-44) were installed on-site (Area A) to 25 feet BGS. Eleven
injection points (IP-1 through IP-11) were attempted off-site in the DOT ROW at 1626 North Chester Street
(Area B). However, due to auger refusal, only 6 temporary wells (IP-1,3,5,8,9, and 10) were installed to
30 feet BGS. All of the boring locations were pre-cleared using an air knife prior to drilling activities and
installed using DPT. Subsequent to injection, the temporary wells were abandoned. A map showing the
locations of the injections points is included as Figure 3. Well logs and abandonment records are included
in Appendix D.

The volume of Cool-Ox (a patented chemical oxidizer that releases oxygen and micronutrients to catalyze
the biodegradation of petroleum constituents in soil and ground water) delivered to the subsurface per
injection point, ranged from 120 to 360 gallons for the off-site injection points; and 80 gallons for the on-
site injection points. A total of 3,960 gallons of Cool-Ox was injected during the Pilot Study. A summary
of the injection data for the October 2023 ISCO pilot test is listed below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Feasibility Study – Pilot Study
Prepared on: February 27, 2024 Ganesha Food Mart
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 4457
3
Injection
Point Location Total Depth
(feet) Gallons Injected
IP-1
Off-site
Area B
1626 North
Chester Street
30 120
IP-2 Refusal 3’ 0
IP-3 30 120
IP-4 Refusal 3’ 0
IP-5 30 360
IP-6 Refusal 4’ 0
IP-7 Refusal 3’ 0
IP-8 30 120
IP-9 30 240
IP-10 30 360
IP-11 Refusal 4’ 0
IP-12
On-site
Area A
1617 North
Chester Street
25 80
IP-13 25 80
IP-14 25 80
IP-15 25 80
IP-16 25 80
IP-17 25 80
IP-18 25 80
IP-19 25 80
IP-20 25 80
IP-21 25 80
IP-22 25 80
IP-23 25 80
IP-24 25 80
IP-25 25 80
IP-26 25 80
IP-27 25 80
IP-28 25 80
IP-29 25 80
IP-30 25 80
IP-31 25 80
IP-32 25 80
IP-33 25 80
IP-34 25 80
IP-35 25 80
IP-36 25 80
IP-37 25 80
IP-38 25 80
IP-39 25 80
IP-40 25 80
IP-41 25 80
IP-42 25 80
IP-43 25 80
IP-44 25 80

In October 2023, during the injection event, 2,640 gallons and 1,320 gallons of Cool-Ox were injected into
the on-site and off-site areas (Area A and Area B), respectively. Copies of DeepEarth’s Injection Sheets are
included in Appendix E. Copies of the Notice of Intent and Injection Event Record that were filed with the
Underground Injection Control Division are included in Appendix F. A summary of the ISCO injection data
from the October 2023 event is listed below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Feasibility Study – Pilot Study
Prepared on: February 27, 2024 Ganesha Food Mart
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 4457
4

Area
Number of
Injection
Points
Injection
Point Depth
(feet BGS)
Average
Injection
Rate
(gal/min)
Average
Pump
Pressure
(psi)
Average Amount
of Cool-Ox
Injected
(gal/IP)
Average
Amount Cool-
Ox Injected per
foot drilled
(gal/ft BGS)
Amount
Cool-Ox
Injected
On-site 33 25 7 100 80 3.2 2,640
Off-site 6 30 10 150 220 7.3 1,320
Total to Date 3.960

3.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
On November 30, 2023, approximately 30-days post injection, monitoring wells GMW-4 and MW-21 were
gauged, purged, and sampled. Depths to ground water were 15.36 and 25.31 feet below TOC in GMW-4
and MW-21, respectively. Ground water samples were submitted for laboratory analyses using EPA
Method 6200B with oxygenates. Concentrations of individual BTEX constituents, MTBE, naphthalene,
TAA, TBA, chloroform, EDB, 1,2 dichloroethane, ethanol, 2-hexanone, isopropylbenzene, di-isopropyl
ether, n-propylbenzene, styrene, 1,2,4-trimethylbenzene, and/or 1,3,5-trimethylbenzene that exceeded
the MACs as specified in T15A NCAC 2L.0202 were reported in GMW-4 and MW-21. The benzene
concentration reported in GMW-4 exceeded the GCL. Concentrations of benzene and EDB in MW-21
exceeded the GCLs.

On December 26, 2023, approximately 60-days post injection, monitoring wells GMW-4 and MW-21 were
gauged, purged, and sampled. Depths to ground water were 15.49 and 25.04 feet below TOC in GMW-4
and MW-21, respectively. Ground water samples were submitted for laboratory analyses using EPA
Method 6200B with oxygenates. Concentrations of individual BTEX constituents, MTBE, naphthalene,
TAA, TBA, EDB, 1,2 dichloroethane, ethanol, 2-hexanone, isopropylbenzene, di-isopropyl ether, n-
propylbenzene, styrene, 1,2,4-trimethylbenzene, and/or 1,3,5-trimethylbenzene that exceeded the MACs
were reported in GMW-4 and MW-21. The benzene concentration reported in GMW-4 exceeded the GCL.
Concentrations of benzene and EDB in MW-21 exceeded the GCLs.

On January 30, 2024, ten monitoring wells (GMW-1 through GMW-4, MW-6, MW-18, MW-21, MMPE-2,
and MMPE-3) were gauged. No free product was present. Depths to ground water in the Type II
monitoring wells ranged from 13.73 feet to 23.69 feet below TOC. Ground water elevations in the Type
II monitoring wells ranged from 75.16 feet to 86.27 feet. Ground water flow was generally toward the
east. Well construction and gauging information is presented in Table 3. A Water Table Surface Map
based on the January 2024 gauging data is included as Figure 4. A summary of the current ground water
gauging data is shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Feasibility Study – Pilot Study
Prepared on: February 27, 2024 Ganesha Food Mart
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 4457
5
Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth
to
Water
from
Top of
Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
GMW-1 5 - 25 25 100.00 13.73 --- 86.27
GMW-2 5 - 25 25 100.21 13.98 --- 86.23
GMW-3 5 - 25 25 99.94 14.51 --- 85.43
GMW-4 5 - 25 25 100.13 14.11 --- 86.02
MMPE-2 unknown unknown 100.27 14.45 --- 85.82
MMPE-3 unknown unknown 99.84 14.13 --- 85.71
MW-6 unknown unknown 98.83 23.45 --- 75.38
MW-18 unknown unknown 98.62 23.46 --- 75.16
MW-21 unknown unknown 98.88 23.69 --- 75.19

On January 30, 2024, approximately 90-days post injection, ten monitoring wells (GMW-1 through GMW-
4, MW-6, MW-18, MW-21, MMPE-2, and MMPE-3) were purged and sampled. Concentrations of
individual BTEX constituents, MTBE, naphthalene, tert-amyl alcohol (TAA), tert-butyl alcohol (TBA),
chloroform, EDB, 1,2 dichloroethane, ethanol, 2-hexanone, isopropylbenzene, di-isopropyl ether, n-
propylbenzene, styrene, 1,2,4-trimethylbenzene, and/or 1,3,5-trimethylbenzene that exceeded the MACs
were reported in GMW-1 through GMW-4, MW-18, MW-21, and MMPE-2. Concentrations of benzene
and EDB in MW-21 exceeded the GCLs.

A summary of the analytical results for ground water samples is presented in Table 4. A Ground Water
Quality Map based on the January 2024 data is included as Figure 5. Isoconcentration Maps for benzene
and EDB are included as Figures 6 and 7, respectively. Copies of laboratory analyses of the ground water
samples collected from the monitoring wells during post-injection sampling events have been included as
Appendix G. A summary of the current ground water analytical data is shown below:

Contaminant of Concern
Be
n
z
e
n
e

To
l
u
e
n
e

Et
h
y
l
b
e
n
z
e
n
e

Xy
l
e
n
e
s

MT
B
E

Na
p
h
t
h
a
l
e
n
e

Well ID
Date
Collected
(mm/dd/yy)
2L Standard (µg/l) 1 600 600 500 20 6
GCL (µg/l) 5,000 260,000 80,000 50,000 20,000 6,000
GMW-1 01/30/24 3,200 13,700 2,060 11,300 88.5 J 1,130
GMW-2 01/30/24 941 4,030 1,520 7,960 <14.0 601
GMW-3 01/30/24 1,430 8,280 1,940 13,300 39.3 J 720
GMW-4 01/30/24 4,100 8,460 1,220 7,020 81.1 J 266
MMPE-2 01/30/24 81.4 46.7 10.6 156 2.33 4.24

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Feasibility Study – Pilot Study
Prepared on: February 27, 2024 Ganesha Food Mart
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 4457
6
Contaminant of Concern
Be
n
z
e
n
e

To
l
u
e
n
e

Et
h
y
l
b
e
n
z
e
n
e

Xy
l
e
n
e
s

MT
B
E

Na
p
h
t
h
a
l
e
n
e

Well ID
Date
Collected
(mm/dd/yy)
2L Standard (µg/l) 1 600 600 500 20 6
GCL (µg/l) 5,000 260,000 80,000 50,000 20,000 6,000
MMPE-3 01/30/24 <0.180 0.399 J 0.222 J 1.42 J <0.140 <0.470
MW-6 01/30/24 <0.180 <0.220 <0.170 <0.210 <0.140 0.536 J
MW-18 01/30/24 3,170 15,100 2,250 11,500 401 750
MW-21 01/30/24 27,700 38,800 3,740 17,700 248 1,140

The baseline contaminant mass at the site was determined based on the total BTEX, MTBE and
naphthalene concentrations from the December 2021 ground water sampling event as well as the average
historical water column height observed in each area. Overall, contaminant mass at the site has decreased
84%.

From May 2023 (pre-injection) to January 2024 (post-injection), contaminant mass in Area A has
decreased 84.5%. Based on these calculations, the ISCO event was successful at reducing contaminant
concentrations in Area A (on-site). When compared to December 2021 data, contaminant mass in Area A
has decreased 92.3%.

From May 2023 (pre-injection) to January 2024 (post-injection), contaminant mass in Area B has increased
35.5%. The lack of contaminant mass reduction from the ISCO event is likely because only six of the eleven
temporary wells were successfully installed due to a subsurface impediment. When compared to
December 2021 data, contaminant mass in Area B has decreased 10.8%. Please note that the average
total contaminant concentrations in Area B (MW-18 and MW-21) have decreased when compared to
December 2021 data but the average height of the water column has increased in Area B. This increase
in water column height (and therefore contaminant volume) may be contributing to an increase in overall
contaminant mass in this area.

Contaminant mass calculations are included as Appendix H. A map of the contaminant mass areas is
included as Figure 8. A chart depicting the overall trend in contaminant mass is shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Feasibility Study – Pilot Study
Prepared on: February 27, 2024 Ganesha Food Mart
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 4457
7

4.0 FREE PRODUCT REMOVAL
Free product and/or GCL exceedances have only been reported in GMW-1 through GMW-4, MMPE-2,
MW-16, MW-18, and MW-21.

On September 23, 2020, at the direction of NCDEQ, GRI installed a F.A.P. Plus Zero Water Pump System
in monitoring well GMW-3. The system consists of a nitrogen-fed pneumatic bladder pump and a Precise
Positioning System (PPS), a float which identifies the product/water interface. As free product enters
through the PPS, a constant supply of nitrogen gas cycles through the system, feeding the product to a
holding tank. This process continues until the free product is reduced to its minimum allowable thickness.
Per the direction of the NCDEQ, the system was deactivated in April 2021 and reactivated in February
2022 and deactivated in February 2023; the system has been dismantled.
5.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
Currently GCL exceedances exist at the site; therefore, no natural attenuation monitoring plan is currently
in place at the site.
6.0 CONCLUSIONS
 Ganesha Food Mart is located at 1617 North Chester Street in Gastonia, Gaston County, North
Carolina. The site is currently owned by Janki Khyati, LLC and is operated by Ganesha Food Mart
0.00
2.00
4.00
6.00
8.00
10.00
12.00
0
10,000
20,000
30,000
40,000
50,000
60,000
70,000
80,000
90,000
100,000
Wa
t
e
r

C
o
l
u
m
n

H
e
i
g
h
t
s

(
f
t
)
Co
n
t
a
m
i
n
a
n
t

M
a
s
s

(
g
r
a
m
s
)
Time
Total Contaminant Mass vs. Time
Ganesha Food Mart (Incident No. 40741)
Total Contaminant Mass (g)
Water Column Heights (ft)

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Feasibility Study – Pilot Study
Prepared on: February 27, 2024 Ganesha Food Mart
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 4457
8
as a petroleum retail facility. Currently, three 10,000-gallon gasoline, one 6,000-gallon diesel, and
one 6,000-gallon kerosene USTs are active at the site.
 In 1995, a previous release was reported at the site. In July 2021, an NFA was issued for the the
1995 release. Responsibility for the remaining on-site and off-site contamination was assigned to
Ganesha Food Mart (Incident 40741). Clean up goals for the site are defined to be less than GCLs
because there is no complete pathway to the surface water body located within 500 feet of the
site.
 On June 1, 2020, the NCDEQ determined that a free product skimming system must be installed
at Ganesha Food Mart. On September 23, 2020, GRI installed an F.A.P. Plus Zero Water Pump
System manufactured by Durham Geo Slope Indicator in monitoring well GMW-3. Monthly O&M
events were conducted from October 2020 until the NCDEQ directed de-activating the system in
April 2021. Per the direction of the NCDEQ, the system was de-activated in April 2021 and
reactivated in February 2022 and deactivated in February 2023.
 A Feasibility Study was conducted; and, based on the available technologies, site-specific
conditions, and limitations of the other technologies, the NCDEQ approved the ISCO via vertical
injection points as the preferred conceptual remedial approach to eliminate free product and
lower contaminant concentrations in ground water below the GCLs in a time- and cost-effective
manner.
 Thirty-three injection points (IP-12 through IP-44) were installed on-site (Area A) to 25 feet BGS.
Eleven injection points (IP-1 through IP-11) were attempted off-site in the DOT ROW at 1626
North Chester Street (Area B). However, due to auger refusal, only 6 temporary wells (IP-
1,3,5,8,9, and 10) were installed to 30 feet BGS.
 On January 30, 2024, ten monitoring wells (GMW-1 through GMW-4, MW-6, MW-18, MW-21,
MMPE-2, and MMPE-3) were gauged. No free product was present. Concentrations of individual
BTEX constituents, MTBE, naphthalene, TAA, TBA, EDB, 1,2 dichloroethane, ethanol, 2-hexanone,
isopropylbenzene, di-isopropyl ether, n-propylbenzene, styrene, 1,2,4-trimethylbenzene, and/or
1,3,5-trimethylbenzene that exceeded the MACs were reported in GMW-4 and MW-21.
Concentrations of benzene and EDB in MW-21 exceeded the GCLs.
 From May 2023 (pre-injection) to January 2024 (post-injection), contaminant mass in Area A has
decreased 84.5%. Based on these calculations, the ISCO event was successful at reducing
contaminant concentrations in Area A (on-site).
 From May 2023 (pre-injection) to January 2024 (post-injection), contaminant mass in Area B has
increased 35.5%. However, the average total contaminant concentrations in Area B (MW-18 and
MW-21) have decreased when compared to December 2021 data but the average height of the
water column has increased in Area B. This increase in water column height (and therefore
contaminant volume) may be contributing to an increase in overall contaminant mass in this area.
In addition, the lack of contaminant mass reduction from the ISCO event is likely because only six
of the eleven temporary wells were successfully installed due to a subsurface impediment.
 Based on these data, a ground water sampling event should be conducted in June 2024 to confirm
no GCL violations remain on-site and evaluate any continued effects from the ISCO event off-site.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Feasibility Study – Pilot Study
Prepared on: February 27, 2024 Ganesha Food Mart
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 4457
9
The decision to conduct additional injection events will be based on an evaluation of the June
2024 ground water quality data.
7.0 LIMITATIONS
This report has been prepared for the exclusive use of Ganesha Food Mart for specific application to the
referenced site in Gaston County, North Carolina. The assessment was conducted based on the scope of
work and level of effort desired by the NCDEQ and with resources adequate only for that scope of work.
Our findings have been developed in accordance with generally accepted standards of environmental
practices in the State of North Carolina, available information, and our professional judgment. No other
warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.

8.0 STATEMENTS AND CERTIFICATION

1 Enter the date the monitoring report was due. n/a Will this report be submitted after
the established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO
IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain
what was missing and why.
3 If applicable, will any of the proposed attenuation milestones under the schedule
approved in the Corrective Action Plan not be met? (within a reasonable margin of
YES NO
IF the answer to question #3 is “NO”, skip to the certification under #8 below.
IF the answer to question #3 is “YES”, please generally describe in this cell the possible reason(s) and
outline proposed remedies. (This should be described in more detail in the report text above.)

N/A 4 Does any known or suspected source zone soil contamination or free product remain
outside of the assessed area that could be inhibiting natural attenuation?
YES NO
5 Has there been an unexpected increase in contaminant mass sufficient to suggest a
potential new release from a separate onsite or offsite source?
YES NO
IF the answer to either question #4 or #5 is “YES”, generally describe in this cell any actions recommended
to further assess or clean up this known or suspected source. (This should be described in more detail in
the report text above.)

FIGURES
ÁSITE LOCATION
³
FIGURE 1SITE LOCATION MAPGANESHA FOOD MART1617 NORTH CHESTER STREETGASTONIA, GASTON COUNTYNORTH CAROLINAGRI PROJECT NO. 4457
PREPARED BY:GEOLOGICAL RESOURCES, INC.MAY 26, 2017
0 2,0001,000 Feet
1 inch = 2,000 feet
MAP CENTER LOCATION
LATITUDE: 35.280688oN
LONGITUDE: 81.188480oW

TABLES
UST ID Number 1 - 5 Facility ID Number
Owner or Operator?
Owner
UST ID Number 1 - 5 Facility ID Number
Owner or Operator?
Owner
TABLE 1
UST OWNER/OPERATOR INFORMATION
GANESHA FOOD MART
1617 North Chester Street, Gastonia NC 28052 704-906-9443
00-0-0000015835
Dates of Ownership / OperationName of Owner or Operator
Address Telephone Number
Janki Khyati, Inc. 01/31/2006 to Present
Address Telephone Number
NA NA
00-0-0000015835
Name of Owner or Operator Dates of Ownership / Operation
Bradshaw's Enterprises, Inc. 08/01/1981 - 01/31/2006
Page 1 of 1
Date: 05/24/17 00-0-0000015835
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline Gasoline 10,000 05/31/71 Fiberglass 8' x 26.6"Double Wall
Flex Current No
2 Gasoline Gasoline 10,000 05/31/71 Fiberglass 8' x 26.6"Double Wall
Flex Current No
3 Gasoline Gasoline 10,000 05/31/71 Fiberglass 8' x 26.6"Double Wall
Flex Current No
4 Diesel Diesel 6,000 05/31/71 Fiberglass 8' x 16'Double Wall
Flex Current No
5 Kerosene Kerosene 6,000 05/31/71 Fiberglass 8' x 16'Double Wall
Flex Current No
Notes:
Data obtained from the NCDEQ registered tank database.
GANESHA FOOD MART
Facility ID # :
TABLE 2
UST SYSTEM INFORMATION
Capacity
(gallons)
Tank
Dimensions
Status
of
UST
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Construction
Details
Description of
Associated
Product Piping
and
Pumps
Date
Installed
Page 1 of 1
Date: 02/02/2024 Facility ID # : 00-0-0000015835
5/17/2018 14.81 0.00 0.00 NA
3/8/2019 10.73 0.00 0.00 714.25
5/19/2021 11.32 0.00 0.00 713.66
12/1/2021 14.50 0.00 0.00 710.48
7/7/2022 14.16 0.00 0.00 710.82
12/8/2022 15.21 0.00 0.00 709.77
5/18/2023 12.46 0.00 0.00 87.54
1/30/2024 13.73 0.00 0.00 86.27
5/17/2018 14.94 0.00 0.00 709.91
3/8/2019 10.76 0.00 0.00 714.09
12/9/2019 13.94 13.92 0.02 710.93
1/15/2021 11.80 0.00 0.00 713.05
2/11/2021 11.86 0.00 0.00 712.99
3/12/2021 11.30 0.00 0.00 713.55
5/19/2021 11.47 0.00 0.00 713.38
12/1/2021 14.67 14.61 0.06 710.23
2/7/2022 14.55 0.00 0.00 710.30
3/3/2022 14.68 0.00 0.00 710.17
4/18/2022 13.46 0.00 0.00 711.39
5/18/2022 13.65 0.00 0.00 711.20
6/21/2022 14.13 0.00 0.00 710.72
7/7/2022 14.28 0.00 0.00 710.57
8/29/2022 14.89 14.85 0.04 709.99
9/12/2022 15.05 15.01 0.04 709.83
10/13/2022 15.04 0.00 0.00 709.81
12/8/2022 15.35 15.34 0.01 709.51
12/22/2022 14.54 14.53 0.01 710.32
1/9/2023 15.28 0.00 0.00 709.57
2/6/2023 13.47 0.00 0.00 711.38
5/18/2023 12.58 0.00 0.00 87.63 sheen/odor
1/30/2024 13.98 0.00 0.00 86.23
724.85
05/16/18GMW-2 5 5 - 25 25
TABLE 3
WELL CONSTRUCTION AND GAUGING INFORMATION
GANESHA FOOD MART (Incident No. 40741)
Well ID Date Installed
(mm/dd/yy)
Date Water Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft. BGS)
Bottom of Well
(ft. BGS)
Top of Casing
Elevation (ft.)***
Depth to Free
Product**
(ft.)
Depth to Water
from Top of Casing
(ft.)
Free Product
Thickness**
(ft.)
Ground Water
Elevation (ft.)Comments
255 - 25505/16/18GMW-1
724.98
100.00
100.21
Page 1 of 5
Date: 02/02/2024 Facility ID # : 00-0-0000015835
TABLE 3
WELL CONSTRUCTION AND GAUGING INFORMATION
GANESHA FOOD MART (Incident No. 40741)
Well ID Date Installed
(mm/dd/yy)
Date Water Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft. BGS)
Bottom of Well
(ft. BGS)
Top of Casing
Elevation (ft.)***
Depth to Free
Product**
(ft.)
Depth to Water
from Top of Casing
(ft.)
Free Product
Thickness**
(ft.)
Ground Water
Elevation (ft.)Comments
5/17/2018 14.91 14.86 0.05 710.09
3/8/2019 10.88 10.83 0.05 714.12
7/10/2019 12.07 11.59 0.48 713.30
12/9/2019 13.94 13.92 0.02 711.04
3/13/2020 10.97 10.85 0.12 714.09
9/23/2020 12.59 12.31 0.28 712.61
10/14/2020 NM NM NM NM
11/5/2020 NM NM NM NM
12/3/2020 12.91 12.90 0.01 712.06
1/15/2021 12.88 0.00 0.00 712.08
2/11/2021 11.60 0.00 0.00 713.36
3/12/2021 10.89 0.00 0.00 714.07
5/19/2021 11.55 0.00 0.00 713.41
12/1/2021 14.95 14.92 0.03 710.04
2/7/2022 15.02 14.86 0.16 710.08
3/3/2022 14.91 14.81 0.10 710.14
4/18/2022 13.89 13.85 0.04 711.10
5/18/2022 13.89 13.8 0.09 711.15
6/21/2022 14.28 14.15 0.13 710.79
7/7/2022 14.46 14.38 0.08 710.57
8/29/2022 15.01 14.94 0.07 710.01
9/12/2022 15.18 15.07 0.11 709.87
10/13/2022 15.33 15.24 0.09 709.71
12/8/2022 15.66 15.51 0.15 709.43
12/22/2022 15.16 15.15 0.01 709.81
1/9/2023 14.41 0.00 0.00 710.55
2/6/2023 13.73 0.00 0.00 711.23
5/18/2023 13.02 0.00 0.00 86.92 sheen/odor
1/30/2024 14.51 0.00 0.00 85.43
25
724.96
99.94
GMW-3 05/16/18 5 5 - 25
Page 2 of 5
Date: 02/02/2024 Facility ID # : 00-0-0000015835
TABLE 3
WELL CONSTRUCTION AND GAUGING INFORMATION
GANESHA FOOD MART (Incident No. 40741)
Well ID Date Installed
(mm/dd/yy)
Date Water Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft. BGS)
Bottom of Well
(ft. BGS)
Top of Casing
Elevation (ft.)***
Depth to Free
Product**
(ft.)
Depth to Water
from Top of Casing
(ft.)
Free Product
Thickness**
(ft.)
Ground Water
Elevation (ft.)Comments
5/17/2018 14.18 0.00 0.00 710.72
3/8/2019 10.74 0.00 0.00 714.16
7/10/2019 11.88 0.00 0.00 713.02
5/19/2021 11.53 0.00 0.00 713.37
12/1/2021 14.73 14.71 0.02 710.19
2/7/2022 14.79 0.00 0.00 710.11
3/3/2022 14.75 0.00 0.00 710.15
4/18/2022 13.62 0.00 0.00 711.28
5/18/2022 13.75 0.00 0.00 711.15
6/21/2022 14.21 0.00 0.00 710.69
7/7/2022 14.40 0.00 0.00 710.50
8/29/2022 14.99 14.98 0.01 709.92
9/12/2022 15.16 15.11 0.05 709.78
10/13/2022 15.22 15.20 0.02 709.70
12/8/2022 14.92 14.91 0.01 709.99
12/22/2022 14.92 0.00 0.00 709.98
1/9/2023 14.61 14.60 0.01 710.30
2/6/2023 13.61 0.00 0.00 711.29
11/30/2023 15.36 0.00 0.00 84.77
12/26/2023 15.49 0.00 0.00 84.64
1/30/2024 14.11 0.00 0.00 86.02
3/13/2020 16.16 0.00 0.00 NM
12/1/2021 19.75 0.00 0.00 NM
7/7/2022 19.35 0.00 0.00 NM
12/8/2022 19.92 0.00 0.00 NM
5/18/2023 100.50 17.40 0.00 0.00 83.10
5 5 - 25 25
724.90
GMW-4 05/16/18
GMW-5 03/13/20 5 5 - 25 25 NM
100.13
Page 3 of 5
Date: 02/02/2024 Facility ID # : 00-0-0000015835
TABLE 3
WELL CONSTRUCTION AND GAUGING INFORMATION
GANESHA FOOD MART (Incident No. 40741)
Well ID Date Installed
(mm/dd/yy)
Date Water Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft. BGS)
Bottom of Well
(ft. BGS)
Top of Casing
Elevation (ft.)***
Depth to Free
Product**
(ft.)
Depth to Water
from Top of Casing
(ft.)
Free Product
Thickness**
(ft.)
Ground Water
Elevation (ft.)Comments
10/29/2018 16.32 13.91 2.41 709.56
11/2/2018 16.39 0.00 0.00 707.42
3/8/2019 10.26 10.23 0.03 713.58
6/26/2019 12.10 11.50 0.60 712.22 Before AFVR
6/26/2019 18.38 0.00 0.00 705.43 After AFVR
7/10/2019 12.51 0.00 0.00 711.30
11/7/2019 14.10 13.90 0.20 709.88 Before AFVR
11/7/2019 19.01 0.00 0.00 704.80 After AFVR
12/9/2019 14.54 0.00 0.00 709.27
3/13/2020 10.41 0.00 0.00 713.40
1/15/2021 12.45 0.00 0.00 711.36
2/11/2021 12.17 0.00 0.00 711.64
3/12/2021 11.60 0.00 0.00 712.21
5/19/2021 12.18 0.00 0.00 711.63
12/1/2021 NM NM NM NM Well not found
7/7/2022 14.99 0.00 0.00 708.82
12/8/2022 15.92 0.00 0.00 707.89
5/18/2023 13.25 0.00 0.00 87.02
1/30/2024 14.45 0.00 0.00 85.82
3/8/2019 10.56 0.00 0.00 713.26
12/1/2021 NM NM NM NM Well not found
7/7/2022 NM NM NM NM Abandoned
3/8/2019 10.09 0.00 0.00 713.90
12/1/2021 14.28 0.00 0.00 709.71
7/7/2022 NM NM NM NM Abandoned
3/8/2019 10.43 0.00 0.00 729.26
5/19/2021 11.80 0.00 0.00 727.89
12/1/2021 NM NM NM NM Well not found
7/7/2022 14.61 0.00 0.00 725.08
5/18/2023 12.83 0.00 0.00 87.01
1/30/2024 14.13 0.00 0.00 85.71
3/8/2019 10.79 0.00 0.00 728.99
12/1/2021 NM NM NM NM Well not found
7/7/2022 NM NM NM NM Abandoned
12/1/2021 24.87 0.00 0.00 698.43
7/7/2022 24.73 0.00 0.00 698.57
12/8/2022 24.53 0.00 0.00 698.77
5/18/2023 23.63 0.00 0.00 75.20
1/30/2024 23.45 0.00 0.00 75.38
723.30
unknown*MW-6 unknown unknown 25
98.83
739.69
MW-1R/MMPE-3 unknown* unknown unknown 22
99.84
723.81
MMPE-2 unknown* unknown unknown 22
100.27
739.78MW-2R/ MMPE-1 unknown* unknown unknown 24
OB-1 unknown* unknown unknown 25 723.99
unknown* unknown unknown 107 723.82DW-1
Page 4 of 5
Date: 02/02/2024 Facility ID # : 00-0-0000015835
TABLE 3
WELL CONSTRUCTION AND GAUGING INFORMATION
GANESHA FOOD MART (Incident No. 40741)
Well ID Date Installed
(mm/dd/yy)
Date Water Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft. BGS)
Bottom of Well
(ft. BGS)
Top of Casing
Elevation (ft.)***
Depth to Free
Product**
(ft.)
Depth to Water
from Top of Casing
(ft.)
Free Product
Thickness**
(ft.)
Ground Water
Elevation (ft.)Comments
12/1/2021 23.97 0.00 0.00 698.00
7/7/2022 NM NM NM NM Abandoned
12/1/2021 24.54 0.00 0.00 697.92
7/7/2022 NM NM NM NM Abandoned
12/1/2021 25.07 0.00 0.00 NM No TOC data
7/7/2022 25.04 0.00 0.00 NM
12/8/2022 24.66 0.00 0.00 NM
5/18/2023 23.87 0.00 0.00 74.75
1/30/2024 23.46 0.00 0.00 75.16
12/1/2021 16.89 0.00 0.00 697.86
7/7/2022 NM NM NM NM Abandoned
12/1/2021 25.31 0.00 0.00 697.15
7/7/2022 25.27 0.00 0.00 697.19
12/8/2022 25.91 0.00 0.00 697.45
5/18/2023 24.10 0.00 0.00 74.78 sheen/odor
11/30/2023 25.31 0.00 0.00 73.57
12/26/2023 25.04 0.00 0.00 73.84
1/30/2024 23.69 0.00 0.00 75.19
Notes:
• ** : If free product is present in a well, ground water elevation calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.8581].
• ft BGS : feet below ground surface.
• N/A: Not available.
• * : Wells installed by Arcadis; well construction information is unavailable.
• *** : TOC data obtained from Arcadis 2021 GWMR; ; TOC data re-surveyed by GRI 5/18/23 for wells shown.
723.36
unknown*MW-21 unknown unknown 30
98.88
NM
MW-18 unknown* unknown unknown 34
98.62
MW-16 unknown*
MW-17 unknown*
unknown unknown 31 721.97
unknown unknown 34 722.46
unknown unknown 29 714.75MW-19 unknown*
Page 5 of 5
Date:2/21/2024
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 40 10 70 0.02 0.4 4,000 40 70 70 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 40,000 10,000 70,000 50 400 4,000,000 40,000 30,500 70,000 26,100 70,000 28,500 24,100
05/17/18 2,840 9,090 807 7,660 36.7 J 1,030 994 J <200 <13 <13 <13 NR NR 44.8 J 77.3 99.4 249 1,570 362
03/08/19 4,800 13,700 1,750 9,980 99.3 J 3,030 NR NR NR NR NR NR NR NR 134 NR NR NR NR
07/10/19 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/09/19 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/13/20 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/19/21 4,250 14,400 1,730 10,400 <63 1,640 <1000 <1000 <63 <63 <63 NR NR <63 <63 112 J 568 1,410 303
12/01/21 3,890 14,100 1,730 10,800 103 J 1,420 2,860 J 1,190 J <63 <63 <63 <33000 NR 70.0 J 149 J 190 J 391 1,730 446
07/07/22 4,860 16,800 2,270 12,600 104 1,460 2,440 <160 <22.0 <20.0 <15.0 <4200 <38.0 99.2 120 242 658 2,310 497
12/08/22 5,560 22,200 2,550 13,500 98.0 J 2,860 2,980 216 J <22.0 <20.0 <15.0 <4200 <38.0 <18.0 172 278 697 2,450 554
05/18/23 3,820 15,900 2,000 10,300 62.2 J 1,940 3,020 559 J <22.0 21.0 J <15.0 <4200 <38.0 66.9 92.8 175 522 1,730 356
01/30/24 3,200 13,700 2,060 11,300 88.5 J 1,130 2,870 1,060 <22.0 <20.0 <15.0 <4,200 53.1 J 97.3 90 250 439 2,150 498
05/17/18 1,120 5,370 1,640 9,750 43.3 J 1,040 1,140 <200 18.5 J <13 <13 NR NR 116 23.5 J 296 210 2,370 597
03/08/19 1,610 8,610 2,400 12,800 <25 1,190 NR NR NR NR NR NR NR NR 30.9 J NR NR NR NR
07/10/19 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/09/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
03/13/20 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/19/21 2,020 11,700 1,630 10,100 <31 680 5,040 <500 40.6 J <31 <31 NR NR 68.5 J <31 184 288 2,060 512
12/01/21 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
07/07/22 1,750 12,900 2,580 13,100 <14.0 1,020 4,210 <160 27.6 J <20.0 <15.0 <4200 <38.0 122 <50.0 303 453 2,370 593
12/08/22 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
05/18/23 1,260 5,490 1,410 7,980 <140 1,000 4000 J <1600 <220 <200 <150 <42000 <380 <180 <500 231 J <220 2,010 574
01/30/24 941 4,030 1,520 7,960 <14.0 601 2,160 1,100 <22.0 <20.0 <15.0 <4,200 87.8 J 90.2 <50.0 255 158 1,850 557
2L Standard (µg/l)
GCL (µg/l)
GMW-1
GMW-2
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
St
y
r
e
n
e
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
Et
h
a
n
o
l
2-
H
e
x
a
n
o
n
e
1,
2
-
D
i
b
r
o
m
o
e
t
h
a
n
e
(E
D
B
)
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
Di
-
i
s
o
p
r
o
p
y
l

e
t
h
e
r
1,
2
-
D
i
c
h
l
o
r
o
e
t
h
a
n
e
te
r
t
-
B
u
t
y
l

a
l
c
o
h
o
l
(T
B
A
)
Contaminant of Concern
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
To
t
a
l

X
y
l
e
n
e
s
Me
t
h
y
l
-
t
e
r
t
-
b
u
t
y
l

e
t
h
e
r
(M
T
B
E
)
Na
p
h
t
h
a
l
e
n
e
te
r
t
-
A
m
y
l

a
l
c
o
h
o
l
(T
A
A
)
Ch
l
o
r
o
f
o
r
m

(
T
r
i
c
h
l
o
r
o
m
e
t
h
a
n
e
)
Analytical Method SM 6200B / EPA 602
TABLE 4
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
GANESHA FOOD MART (Incident No. 40741)
Facility ID No. 00-0-0000015835
Page 1 of Page6
Date:2/21/2024
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 40 10 70 0.02 0.4 4,000 40 70 70 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 40,000 10,000 70,000 50 400 4,000,000 40,000 30,500 70,000 26,100 70,000 28,500 24,100
2L Standard (µg/l)
GCL (µg/l)
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
St
y
r
e
n
e
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
Et
h
a
n
o
l
2-
H
e
x
a
n
o
n
e
1,
2
-
D
i
b
r
o
m
o
e
t
h
a
n
e
(E
D
B
)
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
Di
-
i
s
o
p
r
o
p
y
l

e
t
h
e
r
1,
2
-
D
i
c
h
l
o
r
o
e
t
h
a
n
e
te
r
t
-
B
u
t
y
l

a
l
c
o
h
o
l
(T
B
A
)
Contaminant of Concern
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
To
t
a
l

X
y
l
e
n
e
s
Me
t
h
y
l
-
t
e
r
t
-
b
u
t
y
l

e
t
h
e
r
(M
T
B
E
)
Na
p
h
t
h
a
l
e
n
e
te
r
t
-
A
m
y
l

a
l
c
o
h
o
l
(T
A
A
)
Ch
l
o
r
o
f
o
r
m

(
T
r
i
c
h
l
o
r
o
m
e
t
h
a
n
e
)
Analytical Method SM 6200B / EPA 602
TABLE 4
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
GANESHA FOOD MART (Incident No. 40741)
Facility ID No. 00-0-0000015835
05/17/18 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
03/08/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
07/10/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
12/09/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
03/13/20 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
05/19/21 9,700 32,500 4,830 27,200 <130 1,010 36,100 <2000 <130 <130 <130 NR NR 216 J <130 688 317 J 5,580 1,510
12/01/21 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
12/08/22 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
05/18/23 8,260 29,300 3,550 18,900 <140 1,220 43,800 3390 J <220 <200 <150 <42000 <380 <180 <500 312 J 274 J 2,870 737
01/30/24 1,430 8,280 1,940 13,300 39.3 J 720 5,610 1,180 <22.0 <20.0 <15.0 <4,200 <38.0 105 <50.0 301 113 2,690 691
05/17/18 7,320 20,500 2,530 14,900 286 731 9,230 <500 <31 <31 <31 NR NR 92.0 J 60.4 J 251 68.4 J 2,090 517
03/08/19 7,920 29,400 4,160 24,100 254 712 NR NR NR NR NR NR NR NR 77.2 J NR NR NR NR
07/10/19 8,160 26,600 3,180 17,200 313 461 NR NR NR NR NR NR NR NR 89.4 J NR NR NR NR
12/09/19 9,240 28,800 2,810 15,800 412 J 398 J NR NR NR NR NR NR NR NR <130 NR NR NR NR
03/13/20 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
05/19/21 8,790 29,500 2,450 16,200 439 J 363 J 20,600 3810 J 202 J <130 <130 NR NR <130 <130 171 J <130 1,550 473 J
12/01/21 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
07/07/22 6,870 17,800 2,010 11,200 190 1,640 14,200 1,570 54.9 <20.0 <15.0 2,410,000 <38.0 71.6 <50.0 180 65.9 1,430 333
12/08/22 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
05/18/23 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
11/30/23 6,570 9,790 2,000 11,400 135 449 9,770 1,230 127 <20.0 <15.0 1,420,000 <38.0 69.7 <50.0 192 33.3 J 1,600 382
12/26/23 6,590 15,800 1,940 10,700 149 435 9,760 1,480 66.0 <20.0 <15.0 1,680,000 <38.0 71.2 <50.0 166 40.9 J 1,310 305
01/30/24 4,100 8,460 1,220 7,020 81.1 J 266 7,100 1,270 117 <20.0 <15.0 843,000 <38.0 37.4 J <50.0 101 22.7 J 813 188
03/13/20 2,020 13,900 1,940 10,600 64.6 J 810 4,450 J 2,810 J <63 <63 <63 NR NR 71.8 J <63 167 J <63 1330 431
12/01/21 1,590 10,300 1,250 8,240 <63 345 3,740 J <1000 <63 <63 <63 <33000 NR <63 <63 101 J <63 1,060 326
07/07/22 2,340 12,800 2,180 12,100 44.6 608 7,010 <1.60 11.4 <0.200 <0.150 50.4 J 57.7 74.7 21.9 194 14.7 1,870 496
12/08/22 940 <0.220 750 4,930 12.7 358 2,860 179 <0.220 <0.200 <0.150 471 24.0 42.6 7.9 66 <0.220 894 219
05/18/23 1,250 7,380 1,570 10,000 39.1 J 490 3,590 1,560 <22.0 <20.0 <15.0 <4200 49.4 J 58 <50.0 156 <22.0 1,590 444
GMW-3
GMW-4
GMW-5
Page 2 of Page6
Date:2/21/2024
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 40 10 70 0.02 0.4 4,000 40 70 70 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 40,000 10,000 70,000 50 400 4,000,000 40,000 30,500 70,000 26,100 70,000 28,500 24,100
2L Standard (µg/l)
GCL (µg/l)
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
St
y
r
e
n
e
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
Et
h
a
n
o
l
2-
H
e
x
a
n
o
n
e
1,
2
-
D
i
b
r
o
m
o
e
t
h
a
n
e
(E
D
B
)
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
Di
-
i
s
o
p
r
o
p
y
l

e
t
h
e
r
1,
2
-
D
i
c
h
l
o
r
o
e
t
h
a
n
e
te
r
t
-
B
u
t
y
l

a
l
c
o
h
o
l
(T
B
A
)
Contaminant of Concern
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
To
t
a
l

X
y
l
e
n
e
s
Me
t
h
y
l
-
t
e
r
t
-
b
u
t
y
l

e
t
h
e
r
(M
T
B
E
)
Na
p
h
t
h
a
l
e
n
e
te
r
t
-
A
m
y
l

a
l
c
o
h
o
l
(T
A
A
)
Ch
l
o
r
o
f
o
r
m

(
T
r
i
c
h
l
o
r
o
m
e
t
h
a
n
e
)
Analytical Method SM 6200B / EPA 602
TABLE 4
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
GANESHA FOOD MART (Incident No. 40741)
Facility ID No. 00-0-0000015835
05/17/18 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/08/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
07/10/19 2.2 10.4 2.2 171 <0.13 12.8 NR NR NR NR NR NR NR NR <0.13 NR NR NR NR
12/09/19 2.6 7.3 1.1 10 <0.13 0.19 J NR NR NR NR NR NR NR NR <0.13 NR NR NR NR
03/13/20 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/19/21 0.99 3.7 0.37 J 1.6 <0.13 <0.13 <2.0 <2.0 <0.13 <0.13 <0.13 NR NR <0.13 <0.13 <0.13 <0.13 0.15 J <0.13
12/01/21 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/07/22 <0.180 0.704 B <0.170 0.822 J <0.140 0.863 J <1.90 <1.60 <0.220 <0.200 <0.150 <42.0 <0.380 <0.180 <0.500 <0.190 <0.220 <0.190 <0.180
12/08/22 0.663 8.76 4.17 34.0 <0.140 23.1 <1.90 <1.60 <0.220 <0.200 <0.150 109 J <0.380 <0.180 <0.500 2.66 0.337 J 40 9
12/08/22 0.663 8.76 4.17 34 <0.140 23.1 <1.90 <1.60 <0.220 <0.200 <0.150 109 J <0.380 <0.180 <0.500 2.66 0.337 J 39.5 8.83
05/18/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <1.60 <0.220 <0.200 <0.150 <42.0 <0.380 <0.180 <0.500 <0.190 <0.220 <0.190 <0.180
01/30/24 81.4 46.7 10.6 156 2.33 4.24 622 34 1.2 <0.200 <0.150 <42.0 <0.380 0.317 J 1.14 0.669 0.964 16 4.9
12/01/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 <0.13 <0.13 <0.13 <65 NR <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
07/07/22 0.216 J 0.993 B 0.252 J 1.38 J <0.140 <0.470 <1.90 <1.60 <0.220 <0.200 <0.150 <42.0 <0.380 <0.180 <0.500 <0.190 <0.220 0.305 J <0.180
12/08/22 <0.180 0.302 J <0.170 <0.210 <0.140 2.40 <1.90 <1.60 <0.220 <0.200 <0.150 <42.0 <0.380 <0.180 <0.500 <0.190 <0.220 0.411 J <0.180
05/18/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <1.60 <0.220 <0.200 <0.150 <42.0 <0.380 <0.180 <0.500 <0.190 <0.220 <0.190 <0.180
01/30/24 <0.180 <0.220 <0.170 <0.210 <0.140 0.536 J <1.90 11 <0.220 <0.200 <0.150 <42.0 <0.380 <0.180 <0.500 <0.190 <0.220 0.493 J <0.180
MW-16 12/01/21 8,060 11,600 1,120 5,110 <63 426 3,860 J <1000 <63 <63 <63 <33000 NR <63 548 <63 140 J 467 127 J
MW-17 12/01/21 4,590 15,400 2,300 9,950 <63 760 <1000 <1000 <63 <63 <63 <33000 NR 78.1 J 185 J 189 J 308 1,270 325
12/01/21 6,590 26,300 3,400 17,400 1,040 1,030 8,350 J <2000 <130 <130 <130 <65000 NR <130 498 J 272 J 251 J 2,140 564
07/07/22 6,210 25,400 3,650 17.6 1,110 1,320 9,670 1,610 <22.0 46.8 J <15.0 <4200 47.3 J 152 417 379 441 2,830 686
12/08/22 3,420 17,100 2,910 14,300 544 1,430 5,800 J 409 <2.20 27.0 <1.50 <420 35.3 132 338 330 426 2,310 598
05/18/23 808 4,700 760 4,190 198 496 2,150 934 J <22.0 <20.0 <15.0 <4200 <38.0 44.1 J 106 85.5 101 798 236
01/30/24 3,170 15,100 2,250 11,500 401 750 6,640 410 J <22.0 23.3 J <15.0 <4,200 <38.0 95.7 229 240 262 1,830 465
MW-19 12/01/21 2,860 15,500 2,030 10,900 779 443 6,240 <1000 93.7 J <63 <63 <33000 NR 73.4 J 266 198 J <63 1,550 420
MMPE-2
MW-6
MW-18
Page 3 of Page6
Date:2/21/2024
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 40 10 70 0.02 0.4 4,000 40 70 70 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 40,000 10,000 70,000 50 400 4,000,000 40,000 30,500 70,000 26,100 70,000 28,500 24,100
2L Standard (µg/l)
GCL (µg/l)
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
St
y
r
e
n
e
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
Et
h
a
n
o
l
2-
H
e
x
a
n
o
n
e
1,
2
-
D
i
b
r
o
m
o
e
t
h
a
n
e
(E
D
B
)
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
Di
-
i
s
o
p
r
o
p
y
l

e
t
h
e
r
1,
2
-
D
i
c
h
l
o
r
o
e
t
h
a
n
e
te
r
t
-
B
u
t
y
l

a
l
c
o
h
o
l
(T
B
A
)
Contaminant of Concern
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
To
t
a
l

X
y
l
e
n
e
s
Me
t
h
y
l
-
t
e
r
t
-
b
u
t
y
l

e
t
h
e
r
(M
T
B
E
)
Na
p
h
t
h
a
l
e
n
e
te
r
t
-
A
m
y
l

a
l
c
o
h
o
l
(T
A
A
)
Ch
l
o
r
o
f
o
r
m

(
T
r
i
c
h
l
o
r
o
m
e
t
h
a
n
e
)
Analytical Method SM 6200B / EPA 602
TABLE 4
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
GANESHA FOOD MART (Incident No. 40741)
Facility ID No. 00-0-0000015835
12/01/21 26,500 34,400 3,220 16,000 298 J 930 7,930 J <2000 <130 317 J 159 J <65000 NR <130 1,520 226 J 408 J 1,690 443 J
07/07/22 28,000 35,400 3,640 17.1 303 1,350 10,100 <160 <22.0 486 134 <4200 73.4 J 130 1,410 308 730 2,410 580
12/08/22 30,300 34,300 3,490 16,300 249 1,190 9,360 271 J <22.0 367 <15.0 <4200 60.6 J <18.0 1620 304 697 2,230 541
05/18/23 24,600 37,600 3,180 17,200 183 1,100 5,450 880 J <22.0 444 108 <4200 42.9 J 118 1,140 299 625 2,470 585
11/30/23 26,400 33,800 3,420 16,900 248 1,130 11,761 E 820 J <22.0 405 133 12,100 J 65.6 J 113 1,400 279 666 2,140 505
12/26/23 26,400 36,300 4,080 19,500 226 1,360 11,100 <160 <22.0 455 163 <4,200 62.1 J 147 1,350 365 824 2,740 672
01/30/24 27,700 38,800 3,740 17,700 248 1,140 13,200 279 J <22.0 353 149 <4,200 <38.0 127 1,460 329 714 2,360 568
05/17/18 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/08/19 221 1,200 268 1,310 17.9 119 NR NR NR NR NR NR NR NR 9.3 J NR NR NR NR
07/10/19 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/09/19 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/13/20 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/19/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 <0.13 <0.13 <0.13 NR NR <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
12/01/21 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/07/22 <0.180 0.545 B <0.170 0.702 J <0.140 1.01 <1.90 <1.60 <0.220 <0.200 <0.150 <42.0 <0.380 <0.180 <0.500 <0.190 <0.220 <0.190 <0.180
05/18/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <1.60 <0.220 <0.200 <0.150 <42.0 <0.380 <0.180 <0.500 <0.190 <0.220 <0.190 <0.180
01/30/24 <0.180 0.399 J 0.222 J 1.42 J <0.140 <0.470 <1.90 <1.60 <0.220 <0.200 <0.150 <42.0 <0.380 <0.180 <0.500 <0.190 <0.220 0.6 0.201 J
05/17/18 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/08/19 <0.13 <0.13 0.38 J 0.52 J <0.13 0.29 J NR NR NR NR NR NR NR NR 0.18 J NR NR NR NR
07/10/19 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/09/19 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/13/20 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/01/21 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-1R/MMPE-3
MW-2R/MMPE-1
MW-21
Page 4 of Page6
Date:2/21/2024
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 40 10 70 0.02 0.4 4,000 40 70 70 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 40,000 10,000 70,000 50 400 4,000,000 40,000 30,500 70,000 26,100 70,000 28,500 24,100
2L Standard (µg/l)
GCL (µg/l)
1,
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Analytical Method SM 6200B / EPA 602
TABLE 4
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
GANESHA FOOD MART (Incident No. 40741)
Facility ID No. 00-0-0000015835
05/17/18 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/08/19 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/10/19 1.8 1.2 0.13 J 1.3 J <0.13 <0.13 NR NR NR NR NR NR NR NR <0.13 NR NR NR NR
12/09/19 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/13/20 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/01/21 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/17/18 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/08/19 28.5 1,060 1,180 2,790 <3.1 680 NR NR NR NR NR NR NR NR 3.5 J NR NR NR NR
07/10/19 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/09/19 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/13/20 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/01/21 10.4 J 377 812 1,590 <3.1 426 <50 <50 <3.1 <3.1 <3.1 <1600 NR 55.9 <3.1 144 6.1 J 637 228
11/30/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 NR NR <0.220 <0.200 <0.150 <42.0 <0.380 <0.180 <0.500 <0.190 <0.220 <0.190 <0.180
12/26/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 NR NR <0.220 <0.200 <0.150 <42.0 <0.380 <0.180 <0.500 <0.190 <0.220 <0.190 <0.180
01/30/24 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 NR NR <0.220 <0.200 <0.150 <42.0 <0.380 <0.180 <0.500 <0.190 <0.220 <0.190 <0.180
DW-1
OB-1
Trip Blank
Page 5 of Page6
Date:2/21/2024
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 40 10 70 0.02 0.4 4,000 40 70 70 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 40,000 10,000 70,000 50 400 4,000,000 40,000 30,500 70,000 26,100 70,000 28,500 24,100
2L Standard (µg/l)
GCL (µg/l)
1,
2
,
4
-
T
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m
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t
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b
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Analytical Method SM 6200B / EPA 602
TABLE 4
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
GANESHA FOOD MART (Incident No. 40741)
Facility ID No. 00-0-0000015835
Notes:
• Results reported in micrograms per liter (µg/l).
• < : Less than the method detection limit specified in the laboratory report.
• 2L Standard specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
• NE: Not Established
• Concentrations in bold face type exceeded the 2L standards.
• Concentrations in italics exceeded the gross contamination levels.
• NS: No sample collected.
• NR: Analysis not requested.
• FP: Free Product.
• J: Estimated concentration.
• Refer to laboratory report for detected constituents that did not
Page 6 of Page6

APPENDICES

APPENDIX A
State Correspondence

June 16, 2023 Janki Dhayti, Inc.
7676 Orchard Park Circle Harrisburg, North Carolina 28075 Attention: Milan Patel
Re: Acknowledgment of Receipt/ Notice of Regulatory Requirements 15A NCAC 2L .407 Ganesha Food Mart 1617 North Chester Street, Gastonia Gaston County Incident Number: 40741 Risk Classification: Intermediate Ranking: I165A
Dear Mr. Patel:
On May 31, 2023, the Division of Waste Management’s Underground Storage Tank Section, Mooresville Regional Office, received the Groundwater Monitoring Report for the above-referenced site. The report has been reviewed and will remain in the UST Section’s files. The next groundwater sampling event should be conducted in November 2023, with the
report received by this office no later than December 31, 2023. If you have any questions regarding the actions that must be taken, or the rules mentioned in this letter, please contact me at the address or telephone number listed below. Sincerely, Brad C. Newton, P.G.
Hydrogeologist Mooresville Regional Office UST Section, Division of Waste Management, NCDEQ
cc: Rae Brown – Geologic Resources, Inc. (via e-mail) Gaston County Health Department
4457 Received JUN 19 2023
August 23, 2023
Janki Dhayti, Inc. 7676 Orchard Park Circle Harrisburg, North Carolina 28075
Attention: Milan Patel
Re: Ganesha Food Mart 1617 North Chester Street, Gastonia
Gaston County Incident Number: 4074 Risk Classification: Intermediate
Dear Mr. Patel:
Your request for additional time to submit the Corrective Action Feasibility Study at the above referenced site has been reviewed by the Underground Storage Tank Section of the Division of Waste Management (the Division), Mooresville Regional Office.  Based on the information your consultant has provided with the request for an extension, the request is hereby granted until February 29, 2024. Failure to submit the report by the extended due date may result in a recommendation for the assessment of civil penalties beginning from the original due date.   
If you have any questions regarding the actions that must be taken, or the rules mentioned in this letter, please contact me at the address or telephone number listed below for the Mooresville Regional Office. 
Sincerely,
Brad C. Newton, P.G. Hydrogeologist Mooresville Regional Office
UST Section, Division of Waste Management, NCDEQ
cc: Rae Brown – Geologic Resources, Inc. (via e-mail) Gaston County Health Department
4457 Received AUG 23 2023

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
August 23, 2023

Mr. Brad Newton
NCDEQ-UST Section
Mooresville Regional Office
610 East Center Ave.
Mooresville, NC 28115 via email: [e-mail]

Re: Proposal #23-393
Post Pilot Study Sampling
Ganesha Food Mart
1617 North Chester Street
Gastonia, Gaston County
North Carolina
Incident Number: 40741
GRI Project Number: 4457

Dear Mr. Newton:

Geological Resources, Inc. (GRI) presents the attached Task Authorization (TA) to complete the ground water
sampling post Pilot Test requested in correspondence dated June 16, 2023.

Based on the available technologies, site-specific conditions, and limitations of the other technologies, GRI
believes that a conceptual remedy consisting of In-Situ Chemical Oxidation (ISCO0) via vertical injection
points is the preferred conceptual remedial alternative to eliminate free product and lower contaminant
concentrations in ground water below the GCLs in a time- and cost-effective manner. Cool-Ox® is the
technology approved by the Innovative Technology Committee as a potentially viable innovative remedial
alternative to be investigated for the above referenced site.
Costs for the recommended ground water sampling 30-, 60-, and 90-days after injecting Cool-Ox® during the
pilot study are included. The injections are scheduled to be completed by October 31; therefore, sampling
events should take place November 30, December 30, and January 30. NCDEQ correspondence dated June
16, 2023, requests a ground water sampling report submitted by December 31, 2023. Please extend this
until February 29, 2024.
During the 30- and 60-day sampling events, ground water samples will be collected from GMW-4 and MW-
21. Samples will be analyzed for natural attenuation parameters (ORP, pH, temperature, DO and ORP) and
submitted for laboratory analyses for volatile organic compounds (VOCs) using SM 6200B. A trip blank will
accompany the lab shipment and will be analyzed by SM 6200B.
During the 90-day sampling event, GMW-1 through GMW-4, MMPE-2, MMPE-3, MW-6, MW-18, and MW-21
will be gauged, purged, and sampled. Natural attenuation parameters (ORP, pH, temperature, DO and ORP)
will also be collected from each well. Collected samples will be submitted for laboratory analyses for volatile
Proposal #23-393
Ganesha Food Mart
Page 2 of 2

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]

organic compounds (VOCs) using SM 6200B. A trip blank will accompany the lab shipment and will be
analyzed by SM 6200B. The results of the sampling event will be presented in a Ground Water Monitoring
Report by February 29, 2024.
ESTIMATED COSTS
Task #
La
b

C
o
d
e
#

Scope of Work Count Rate Units Subtotal
4.031
Cost for Sampling
30-Days: GMW-4 and MW-21
60-Days: GMW-4 and MW-21
90-Days: GMW-1 through GMW-4, MMPE-2,
MMPE-3, MW-6, MW-18, and MW-21 13 $110.00 well $1,430.00
4.090 240
Standard Method 6200B + oxygenates
30-Days: GMW-4 and MW-21
60-Days: GMW-4 and MW-21
90-Days: GMW-1 through GMW-4, MMPE-2,
MMPE-3, MW-6, MW-18, and MW-21 13 $94.00 sample $1,222.00
4.090 272
Standard Method 6200B
30-Days: trip blank
60-Days: trip blank
90-Days: trip blank 3 $66.00 sample $198.00
4.091 shipments: 30-, 60-, 90-day events 3 $60.00 shipment $180.00
6.065 Corrective Action Feasibility Study 1 $2,500.00 report $2,500.00
12.050 Consultant Mobilization: 30-, 60-, 90-day events 3 $250.00 trip $750.00
12.055
Temporary Impact Increase: 30-, 60-, 90-day
events 3 $50.00 trip $150.00
Total $6,430.00

To authorize this scope of work, please sign and return the attached TA. If you have questions or comments,
please do not hesitate to contact me at [phone].

Sincerely,
Geological Resources, Inc.
Rae Troiano Brown, P.G.
Project Manager

Attachments

Site Name City / County /Gaston Incident #40741
Resp Pty Name / Contact Incident Mgr Region MORRP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #21
Consultant / Project Mgr /Rae Troiano Brown
Telephone / Fax Number /Task Authorization Number:22 ChangeOrd:
Project Mgr Email Site Risk / Rank / Abatement:I165A RRA Date:
Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
 Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.
Task #Lab /
SubCode
RO

A
u
t
h
Proposed
Rate/Price
(Consultant)CO

A
u
t
h
Proposed Task
Subtotal
(Consultant)
Final
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
4.031 13 /wells y $110.00 Y $1,430.00 $1,430.00 /
4.090 #240 13 /samples y $94.00 Y $1,222.00 $1,222.00 /
4.090 #272 3 /samples y $66.00 Y $198.00 $198.00 /
4.091 3 /shipments y $60.00 Y $180.00 $180.00 /
6.065 1 /report n $2,500.00 0 $2,500.00 $0.00 /
12.050 3 /trips y $250.00 Y $750.00 $750.00 /
12.055 3 /trips y $50.00 Y $150.00 $150.00 /
6.105 1 /report Y $2,000.00 Y $2,000.00 $2,000.00 /
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
Requested Preapproved
TOTAL:$8,430.00 $5,930.00 TOTAL:
Total Standard Costs (Not Third Party)$8,430.00 $5,930.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty CostsProcess Tracking (Date)
TA Submittal:8/23/23 by:(PM)(Reserved for RO)
RO Review:8/24/23 by:(IM)Joint UST Preapproval Confirmed By:
CO Review:8/24/23 by:(STF)RP or Designee Receipt Confirmation By:
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable.
3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned.
4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee and returned to the Trust Fund within a week of approval. Signature
indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to work proceeding. Scope/costnegotiations do not supersede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both the UST Section and RPis not to be modified without written consent by all signatories.
5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full.
DWM/UST ePATA 4/1/2022
DIRECTED COSTS
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
(Reserved for Incident Manager)
PREAPPROVAL / TASK AUTHORIZATION
Note:This Electronic Preapproval Task Authorization (ePATA)shall be used to receive preapproval from the UST Section.A proposal,including maps and figures,must be
attached to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If,following completion of this ePATA,
you discover that unexpected tasks must be performed, incurring costs for tasks not originally included with this form,you must complete and submit a separate ePATA requestdesignated as a "Change Order" in the provided space above prior to conducting those tasks.Include a copy of the prior ePATA form for confirmation.Please attach this form to
the cover of the corresponding claim when requesting reimbursement.IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been
completed within 12 months ofthe completion date of the FIRST completed task to remain within the Statute ofLimitations.All ePATAs submitted withina claim areclosed with that
claim,and may not be re-used in a separate submittal,even for costs or tasks that were not originally claimed.Final reimbursement of costs associated with the Total Claimedamount below may be affected by the eligibility status of the site (i.e.,deductibles,apportionment,etc.),and the documentary validation of incurred costs as reasonable and
bcn
LP
(Initials)
RTB
Proposed
Units / Type
(Consultant)
Brad Newton
YES23-393 Nov-23
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
[e-mail]
Janki Dhayti
Geological Resources, Inc.
Dept of Environmental Quality - Division of Waste Management
8/26/23
1
Rae Brown
From:Rae Brown
Sent:Wednesday, August 23, 2023 10:49 AM
To:Newton, Brad
Subject:RE: [External] Ganesha (GRI 4457)
There isn’t a 30 day report in the TA; there is a report at the end of the 90 day sampling that summarizes the sampling
events; please add a 30 day sampling event if that is what you would like and I will submit one to meet the deadline

Rae Troiano Brown, P.G.
Project Manager
Geological Resources, Inc.
113 Firetower Road, Suite G
Winterville, NC 28590
Main [phone] Cell [phone]
www.geologicalresourcesinc.com

From: Newton, Brad <[e-mail]>
Sent: Wednesday, August 23, 2023 10:29 AM
To: Rae Brown <[e-mail]>
Subject: RE: [External] Ganesha (GRI 4457)

Rather than submit a summary in mid-November, how about just including that in the 30 day sampling report?

From: Rae Brown <[e-mail]>
Sent: Wednesday, August 23, 2023 10:26 AM
To: Newton, Brad <[e-mail]>
Subject: [External] Ganesha (GRI 4457)

CAUTION: External email. Do not click links or open attachments unless verified. Report suspicious emails with the Report Message
button located on your Outlook menu bar on the Home tab.

Brad,

A ached is the TA for the 30, 60, 90 sampling post pilot study. The June NORR requests sampling in Nov and a report in
Dec. I am reques ng an extension for the sampling report because the 30, 60, 90 sampling post pilot study will make
this redundant.

Thanks for your help,
Rae

Rae Troiano Brown, P.G.
Project Manager
Geological Resources, Inc.
113 Firetower Road, Suite G
Winterville, NC 28590
Main [phone] Cell [phone]
www.geologicalresourcesinc.com

APPENDIX B
DOT Permit and Access Agreement

4457 Received APR 21 2022

APPENDIX C
Health and Safety Plans and Utilities Maps

Treatment Areas
Area A
33 IPs* | 1,200 ft2
VTI: 15 to 25 ft-bgs
Area B
11 IPs* | 400 ft2
VTI: 15 to 30 ft-bgs
*IP locations are subject to change
based upon site conditions and
obstructions.
Fiber Optic
Line
Monitoring Well
Natural Gas
Overhead Electric
Point
Product Line
Sewer
Soil Boring
Underground Electric
Water
Legend
(4457) Ganesha Food Mart 11/7/2023Date
1/13
Fiber Optic
Line
Monitoring Well
Natural Gas
Overhead Electric
Point
Product Line
Sewer
Soil Boring
Underground Electric
Water
Legend
(4457) Ganesha Food Mart 11/7/2023Date
1/12

APPENDIX D
Well Construction Logs and Permits

WELL CONSTRUCTION RECORD
This form can be used for single or multiple wells
Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared) □Irrigation
Non-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip
County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W
6. Is (are) the well(s): □Permanent or □Temporary

7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells:
Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed.
For Internal Use ONLY:
_______________
Matt Steele
4548-A
Geological Resources, Inc.
WI0300497
4
10/26-30/23 IP-12 thru IP-44
Ganesha Food Mart 00-0-0000015835
1617 North Chester Street, Gastonia, NC, 28052
Gaston 3546-64-9362
35.28119770 -81.18818532
4
4
33
25
~15
1.5
Direct Push
15 25 Saturated
NA
NA
15 25 1 Stainless
NA
NA
0 0.25 Asphalt
0.25 1 No soil cuttings generated
Temporary wells to be used for in situ chemical oxidation. After
injection, will be abandoned with granular bentonite.
11/6/23
WELL CONSTRUCTION RECORD
This form can be used for single or multiple wells
Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared) □Irrigation
Non-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip
County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W
6. Is (are) the well(s): □Permanent or □Temporary

7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells:
Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed.
For Internal Use ONLY:
_______________
Matt Steele
4548-A
Geological Resources, Inc.
WI0300497
4
10/25/23 IP-1,3,5,8,9,10
Ganesha Food Mart 00-0-0000015835
1626 North Chester Street, Gastonia, NC, 28052
Gaston 3546-74-2410
35.28117460 -81.18770708
4
4
6
30
~25
1.5
Direct Push
25 30 Saturated
NA
NA
15 30 1 Stainless
NA
NA
0 0.25 Asphalt
0.25 30 No soil cuttings generated
Temporary wells to be used for in situ chemical oxidation. After
injection, temporary wells will be abandoned with granular bentonite.
11/6/23
WELL ABANDONMENT RECORD
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1.Well Contractor Information:
Well Contractor Name (or well owner personally abandoning well on his/her property)
NC Well Contractor Certification Number
Company Name
2.Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) if known
3.Well use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply wells
ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s): (gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
□Neat Cement Grout □Bentonite Chips or Pellets
□Sand Cement Grout □Dry Clay
□Concrete Grout □Drill Cuttings
□Specialty Grout □Gravel
□Bentonite Slurry □Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
7g. Provide a brief description of the abandonment procedure:
8.Certification:
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9.Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
abandoned.
For Internal Use ONLY:
Matthew Steele
4548 A 6
0.2
Geological Resources, Inc.
WI0300497
10 lbs of Bentonite
5 lb concrete
10/25/23
Pour
Wells were used for in situ chemical oxidation
Abandoned with bentonite after injection.Ganesha Food Mart 00-0-000015835
1626 North Chester St., Gastonia NC 28052 11/6/23
Gaston 3456-74-2410
35.28119770 -81.18818532
IP-1,3,5,8,9,10
30
1.5
25
n/a
n/a
15
WELL ABANDONMENT RECORD
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1.Well Contractor Information:
Well Contractor Name (or well owner personally abandoning well on his/her property)
NC Well Contractor Certification Number
Company Name
2.Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) if known
3.Well use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply wells
ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s): (gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
□Neat Cement Grout □Bentonite Chips or Pellets
□Sand Cement Grout □Dry Clay
□Concrete Grout □Drill Cuttings
□Specialty Grout □Gravel
□Bentonite Slurry □Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
7g. Provide a brief description of the abandonment procedure:
8.Certification:
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9.Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
abandoned.
For Internal Use ONLY:
Matthew Steele
4548 A 33
0.4
Geological Resources, Inc.
WI0300497
10 lbs of Bentonite
5 lb concrete
10/26-30/23
Pour
Wells were used for in situ chemical oxidation
Abandoned with bentonite after injection.Ganesha Food Mart 00-0-000015835
1617 North Chester St., Gastonia NC 28052 11/6/23
Gaston 3546-64-9362
35.28119770 -81.18818532
IP-12 thru IP-44
25
1.5
15
n/a
n/a
15

APPENDIX E
Deep Earth Field Injection Sheets

2657 Pilot R1
4,000
Start End From:To:
10/25/2023 IP-6 1000 1004 0 0 1 0 0 0 0IP-1 1006 1043 15 30 1 120 10 8 150
IP-4 1051 1057 0 0 1 0 0 0 0
IP-11 1058 1059 0 0 1 0 0 0 0
IP-8 1101 1133 15 30 1 120 10 8 150
IP-2 1145 1148 0 0 1 0 0 0 0IP-3 1152 1226 15 30 1 120 10 8 150
IP-5 1324 1431 15 30 1 360 10 8 150IP-7 1442 1450 0 0 1 0 0 0 0
IP-10 1452 1602 15 30 1 360 10 8 150
IP-9 1611 1701 15 30 1 240 10 8 150
TOTAL:11 1320
Date IP #
refusal 3 ft
refusal 4 ft
Area B; refusal 4 ft
refusal 3 ft
Gallons
Cool-Ox ® Daily Field Injection Sheet
10/25/2023
Austin, Barry & Anthony
Office:Client Personnel:Client Project #:Site:Ganesha Food Mart DTI Operations Manager:Subcontract #:
DTI Field Crew:
pH Pressure
Gal/cy
Gastonia, NC5
GPM
refusal 3 ft
CommentsTotal IPs
QUOTE:
2657 Pilot R1
4,000
Start End From:To:
10/26/2023 IP-32 850 912 15 25 1 80 7 8 100IP-42 918 942 15 25 1 80 7 8 100
IP-27 947 1010 15 25 1 80 7 8 100
IP-28 1021 1044 15 25 1 80 7 8 100
IP-36 1051 1104 15 25 1 80 7 8 100
IP-34 1109 1128 15 25 1 80 7 8 100IP-39 1138 1157 15 25 1 80 7 8 100
IP-43 1204 1228 15 25 1 80 7 8 100IP-38 1320 1334 15 25 1 80 7 8 100
IP-40 1339 1356 15 25 1 80 7 8 100
IP-44 1359 1411 15 25 1 80 7 8 100IP-35 1416 1434 15 25 1 80 7 8 100
IP-31 1439 1502 15 25 1 80 7 8 100
IP-24 1505 1524 15 25 1 80 7 8 100
IP-26 1536 1559 15 25 1 80 7 8 100
TOTAL:15 1200
GPM
no reaction
no reaction
no reaction
communication with MW-4
no reaction
no reaction
CommentsTotal IPs
QUOTE:
pH Pressure
Gal/cy
Gastonia, NC5 Austin, Barry & Anthony
Office:Client Personnel:Client Project #:Site:Ganesha Food Mart DTI Operations Manager:Subcontract #:
DTI Field Crew:
Cool-Ox ® Daily Field Injection Sheet
10/26/2023
Date IP #
communication with GMW-3; strong odor; product; slight reaction
no reaction
no reaction
slight odor; product
communication GMW-3
Area Ano reaction
no reaction
Gallons
2657 Pilot R1
4,000
Start End From:To:
10/27/2023 IP-30 842 916 15 25 1 80 7 8 100IP-25 925 943 15 25 1 80 7 8 100
IP-20 949 1011 15 25 1 80 7 8 100
IP-22 1018 1043 15 25 1 80 7 8 100
IP-17 1050 1115 15 25 1 80 7 8 100
IP-19 1122 1149 15 25 1 80 7 8 100IP-12 1306 1327 15 25 1 80 7 8 100
IP-14 1334 1358 15 25 1 80 7 8 100
TOTAL:8 640
GPM
communication GMW-2
communication GMW-2; strong odor
CommentsTotal IPs
QUOTE:
pH Pressure
Gal/cy
Gastonia, NC5 Austin, Barry & Anthony
Office:Client Personnel:Client Project #:Site:Ganesha Food Mart DTI Operations Manager:Subcontract #:
DTI Field Crew:
Cool-Ox ® Daily Field Injection Sheet
10/27/2023
Date IP #
no reaction
no reaction
no reaction
communication GMW-3no reaction
no reaction
Gallons
2657 Pilot R1
4,000
Start End From:To:
10/30/2023 IP-13 845 906 15 25 1 80 7 8 100IP-15 912 930 15 25 1 80 7 8 100
IP-18 935 956 15 25 1 80 7 8 100
IP-16 1000 1013 15 25 1 80 7 8 100
IP-21 1021 1122 15 25 1 80 7 8 100
IP-41 1130 1200 15 25 1 80 7 8 100IP-23 1209 1233 15 25 1 80 7 8 100
IP-29 1303 1327 15 25 1 80 7 8 100IP-33 1335 1358 15 25 1 80 7 8 100
IP-37 1406 1438 15 25 1 80 7 8 100
TOTAL:10 800
Date IP #
no reaction
no reaction
no reaction
communication GMW-2; odorno reaction
no reaction
Gallons
Cool-Ox ® Daily Field Injection Sheet
10/30/2023
Austin, Barry & Anthony
Office:Client Personnel:Client Project #:Site:Ganesha Food Mart DTI Operations Manager:Subcontract #:
DTI Field Crew:
pH Pressure
Gal/cy
Gastonia, NC5
GPM
no reaction
no reaction
no reaction
no reaction
CommentsTotal IPs
QUOTE:

“Where Science & Technology Meet”
PO Box 360 | Allegan, MI 49010 - [phone] - [e-mail]

Direct Push Technology Subcontractor Information
The most important requirements are listed below. DeepEarth requires a track mounted rig NOT
a truck mounted rig. DeepEarth also requires the use of 5’ tooling, so the rig must accommodate
that. Preferred 1.5 inch diameter by 5’ Geoprobe rods. If the driller uses AMS Powerprobes rather
than Geoprobe, 5’x 1-5/8” AMS rods are good.

Please provide DPT Subcontractor the following to complete a quote:
- Site location
- Total depth (lithology)
- Number of injection locations
- Number of days (10 hr/day possibly weekends)

What DeepEarth needs:
- Track mounted Geoprobe 7822 or similar (must accommodate 5’ long 1.5” injection
rods)
- 2-man crew (driller/helper)
- Abatement materials (granular bentonite, NOT chips)
- They supply tooling except for end tooling (1’ pressure injector rod)
- All costs (daily, weekend, standby rates, consumables, mob, per-diems)

Please call your DeepEarth representative for further clarification or with any questions.
Once a driller is selected, please notify your DeepEarth representative to schedule a call to
confirm details.

Geological Resources, Inc. Site:Ganesha Food Mart 7/25/2023
113 Firetower Road 1617 North Chester Street
Suite G Gastonia, NC DTI Job #:2657 Pilot R1
Winterville, NC 28590
Attention:Rae Troiano Brown, P.G.Phone:[phone] [e-mail]
Cool-Ox ® remediation of subject site:
Contaminants:BTEXMedia Treated:Soil & GW
20
Total Area A Area B
Vertical Extent (feet bgl):15 to 25 15 to 30
667 444 222
44 33 11
4,000 2,667 1,33380120
Proposed Injection Point Spacing (feet):6 6
Reagent Per Cubic Yard (gal):6 6
Est. On-Site Days to Complete:5
Rate Unit Total
Cool-Ox ®$6.37 gallon 25,480$
Mixing Equipment $2,402 day 12,010$
Labor (3 personnel)$3,326 day 16,630$
Mobilization $6,663 lump sum 6,663$ Materials/Incidentals $3,696 lump sum 3,696$
Lump Sum Price:64,479$
Rate Unit Total
Labor (2 personnel)2,478$ day 12,390$
Mobilization 5,559$ lump sum 5,559$ Materials/Incidentals 1,258$ lump sum 1,258$ Lump Sum Price:29,832$
Conditions of Quote:
1) All quotes shall remain in effect for a period of sixty (60) days only. Expired quotes must be renegotiated.
2) The Client shall:
DTI Field Services Group - Summary Sheet for Cool-Ox ® Application
Chemical Mixing Rates
DPT Injection Rates
b) Arrange for the locating and marking of all underground utilities and structures including GPR. DTI shall not
be liable for any damage to such utilities or structures not clearly identified and revealed to DTI.c) Secure all permits necessary for the legal commencement of work and right of entry to the site.
d) Unless otherwise noted, source and retain DPT subcontractor licensed and legally permitted to perform
Cool-Ox ® into the subsurface as directed by DTI.
DPT rig shall be track mounted and of a size acceptable to DTI.
e) If necessary, arrange for coring of paved surfaces prior to the commencement of work.
f) Pay DTI for all work completed within 30 days of receipt of DTI invoice. For projects in excess of $200,000
a minimum deposit in the amount of 1/3 of the quoted price will be required prior to the commencement
of work to cover a portion of the materials and mobilization costs.
If payment is not received within 30 days of receipt of DTI invoice, a late payment fee of 1.5% per month
will be charged.
g) Notify DTI if any additional on site health and safety training classes are required 30 days prior to job start.
h) Provide copies of all analytical data derived from samples collected prior to (to establish baseline data),
during, and for three years after the completion of the remedial application. This data shall be considered
Cool-Ox ® technology.
3) Assumptions:
a) No work shall be conducted in inclement weather such as lightning storms, freezing conditions, excessive rain or snow. The Stand-by daily rate, if applicable, shall be that rate stated in the work order.
b) All quotes are based upon an eight (8) hour work day.
c) In offering this quote, DTI does not warrant or imply that the site shall be remediated to closure
Cool-Ox ® technology.
d) The Estimated Total Gallons states the maximum amount that could be applied at the above mentioned site.
If the amount of reagent applied is less than the Estimated Total Gallons, a discount in the Lump Sum Price
will not be provided.
4) Site Specific Provisions:
a) This estimate includes all costs for material, labor and equipment for injections.
Changes to the scope may be made in the field by DTI to account for unknowns or changes in the site conditions.
b) If a larger treatment area or additional reagent is required to adequately treat the site, a change order
shall be be executed by the client prior to the initiation of additional work.
5) Ownership of Documents, Patents, and Copyrights:
Client understands and agrees that the primary reason Client is contracting with DTI is to secure the
services and knowledge of DTI to provide Client with in-situ or ex-situ remediation of contaminants
employing technology and application methods developed and provided by DTI. Client further understandsand agrees that in the broadest definition of the term, the “craft” of DTI is providing, developing and
improving the technology for the exclusive commercial or other use of DTI and that all intellectual property
developed in the performance of any and all Work performed by DTI for Client or its clients, including,
without limitation, all drawings, specifications, reports, summaries, samples, photographs, memoranda,
property of DTI.
We at DTI wish to thank you for your consideration of our company as your in-situ chemical oxidation and reduction
remedial contractor. If you have any questions regarding the technology or the information contained in this proposal, please
contact us immediately. If you are in agreement with the proposal and wish to proceed with the project by reserving
a work schedule date, please sign below and return this form to us.
Sincerely,Accepted:
William L. Lundy, Sr. V. P.Name and Title:___________________________
8/23/23
FORMERBUILDING
FORMERDISPENSERISLANDSINSTALLATIONOF USTs ON4/16/83 AND9/23/81
UP LP
TS
UP
UPLP
LP LP
LP
LP
UPLP
LP
LP
LP
LP
LP
LP
LPLP
LP
UPLP
UP
UP
PD
RP
CANOPY
CANOPY
GRASS
TANKFARM(CONCRETE)
GRASS
GRASS
GRASS
GRASS
GRASS
ASPHALT
ASPHALT
RADIO AVE.
U.
S
.

H
I
G
H
W
A
Y

3
2
1
GRASS
GRASS
GR
A
S
S

M
E
D
I
A
N
ASPHALTPARKING
BILLBOARD
BILLBOARD
FR
A
C

T
A
N
K
ASPHALTPARKING
CRE
E
K
HIGH VOLTAGEUTILITY TOWER
REMEDIATIONTRAILER
RECOVERY POINT
FREE PRODUCTSKIMMEREQUIPMENT
RA
I
L
R
O
A
D

T
R
A
C
K
S
HISTORICUST FIELD64'-83'
BLDG
BLDG
BLDG
KIOSK
CAR WASH
BL
D
G
BLDG(Bradshaw'sMarket)
STORAGE
BLDG
INSTALLATIONOF USTs ON4/16/83
HISTORICDISPENSER PUMPS71'-83'
INSTALLATION OFCURRENT USTs ON5/31/71
MW-11
MW-12
MW-13
MW-14
MW-20
MW-19
MW-18
MW-17
MW-16
MW-21
GWM-4
GWM-3
GWM-2
GWM-1
MW-1
MW-7
MW-5
MW-3
MW-2
DW-1
MW1R/MMPE3
MMPE2
OB-1
MW2R/MMPE1
RW-2
RW-1FORMERBUILDING
FORMERDISPENSERISLANDS
MW-4
MW-8
MW-9
MW-10
MW-6
MW-17
Date 09/27/19 03/16/20 09/04/20 03/24/21
B 3,000 4,100 410 43
T 9,600 13,000 200 8.5
E 1,700 2,100 49 4.6
X 6,400 8,100 100 9.1
MTBE <50 <50 <5.0 <0.50
DIPE 180 140 --52
EDB <50 --<5.0 <0.50
Naph 620 670 35 9.0
1,3,5-TMB 280 310 <5.0 <0.50
1,2,4-TMB 1,200 1,300 17 1.3
STY 390 510 6.9 <0.50
1,2-Dich <50 <50 <5.0 1.5
MW-13
Date 09/27/19 03/16/20 09/04/20 03/23/21
B <0.5 <0.5 <0.50 5.9
T <0.5 <0.5 <0.50 2.4
E <0.5 <0.5 <0.50 3.9
X <1.0 <1.0 <1.0 4.7
MTBE 0.6 41 <0.50 5.7
DIPE <0.5 2.4 --0.67
EDB <0.5 --<0.50 <0.50
Naph <0.5 1.4 <0.50 0.75
1,3,5-TMB <0.5 <0.5 <0.50 <0.50
1,2,4-TMB <0.5 <0.5 <0.50 1.1
STY <0.5 <0.5 <0.50 <0.50
1,2-Dich <0.5 <0.5 <0.50 <0.50
MW-16
Date 09/27/19 03/16/20 09/04/20 03/24/21
B 6,400 1,300 2.6 2.0
T 5,900 1,300 2.5 3.2
E 580 130 0.87 0.92
X 3,200 820 5.2 6.3
MTBE 120 <2.5 <0.50 <0.50
DIPE 530 81 --<0.50
EDB 66 --<0.50 <0.50
Naph 270 69 0.78 1.1
1,3,5-TMB 250 92 <0.50 0.56
1,2,4-TMB 840 250 0.94 1.8
STY <25 <25 <0.50 <0.50
1,2-Dich 78 <25 <0.50 <0.50
MW-11
Date 09/27/19 03/16/20 09/04/20 03/23/21
B <0.5 <0.5 <0.50 <0.50
T 33 E <0.5 <0.50 <0.50
E <0.5 <0.5 <0.50 <0.50
X <1.0 <1.0 <1.0 <1.0
MTBE <0.5 <0.5 <0.50 <0.50
DDIPE <0.5 <0.5 --<0.50
EDB <0.5 --<0.50 <0.50
Naph <0.5 <0.5 <0.50 <0.50
1,3,5-TMB <0.5 <0.5 <0.50 <0.50
1,2,4-TMB <0.5 <0.5 <0.50 <0.50
STY <0.5 <0.5 <0.50 <0.50
1,2-Dich <0.5 <0.5 <0.50 <0.50
MW-20
Date 09/27/19 03/16/20 09/04/20 03/23/21
B <0.5 <5.0 <0.50 <0.50
T <0.5 <5.0 <0.50 <0.50
E <0.5 <5.0 <0.50 <0.50
X <1.0 <10 <1.0 <1.0
MTBE 27 <5.0 10 <0.50
DIPE 0.6 <5.0 --<0.50
EDB <0.5 --<0.50 <0.50
Naph <0.5 <5.0 <0.50 <0.50
1,3,5-TMB <0.5 <5.0 <0.50 <0.50
1,2,4-TMB <0.5 <5.0 <0.50 <0.50
STY <0.5 <5.0 <0.50 <0.50
1,2-Dich <0.5 <5.0 <0.50 <0.50
MW-19
Date 09/27/19 03/16/20 09/04/20 03/24/21
B 2,200 2,000 820 580
T 9,900 16,000 7,200 4,200
E 1,800 2,200 960 730
X 8,800 11,000 5,400 3,900
MTBE 210 350 240 170
DIPE <50 74 --54
EDB <50 --<50 <10
Naph 470 450 220 200
1,3,5-TMB 490 520 180 160
1,2,4-TMB 1,800 1,900 710 610
STY <50 <50 <50 58
1,2-Dich <50 <50 <50 <10
LEGEND
B Benzene
T Toluene
E Ethylbenzene
X Total Xylenes
MTBE Methyl tert-butyl Ether
IPE Disopropyl Ether
EDB Ethylene Dibromide
Naph Naphthalene
1,3,5-TMB 1,3,5-Trimethylbenzene
1,2,4-TMB 1,2,4-Trimethylbenzene
STY STYRENE
1,2-Dich 1,2-Dichloroethane
North Carolina Standards
COMPOUND 2B Standards GCL Standards
B 51 5,000
T 11 2,60,000
E 97 84,500
X 670 85,000
MTBE 1,500 20,000
IPE 13,000 70,000
EDB 0.31 50
Naph 330 6,000
1,3,4-TMB 630 25,000
1,2,4-TMB 390 28,500
STY NE 70,000
1,2-Dich 37 400
LNAPL THICKNESS: 0.16
MW-21
Date 01/20/20 03/16/20 09/04/20 03/24/21
B 25,000 26,000 21,000 21,000 E
T 30,000 33,000 25,000 2,3000 E
E 3,100 3,200 1,900 1,700
X 16,000 17,000 10,000 9,800 F1
MTBE 370 260 260 270
DIPE 1,400 1,400 --1,200
EDB ----370 370
Naph 980 830 670 550
1,3,5-TMB 490 520 260 230
1,2,4-TMB 2,000 2,000 1,000 960
STY 760 870 560 490
1,2-Dich <250 <250 <250 120
GMW-1
Date 03/25/21
B 4,200
T 12,000
E 1,500
X 7,200
MTBE 67
DIPE 110
EDB <50
Naph 1,400
1,3,5-TMB 250
1,2,4-TMB 1,200
STY <50
1,2-Dich <50
GMW-2
Date 03/25/21
B 1,100
T 6,700
E 920
X 5,400
MTBE <25
DIPE <25
EDB <25
Naph 400
1,3,5-TMB 250
1,2,4-TMB 950
STY <25
1,2-Dich <25
GMW-3
Date 03/25/21
B 4,500
T 13,000
E 1,700
X 8,600
MTBE 160
DIPE <50
EDB <50
Naph 400
1,3,5-TMB 390
1,2,4-TMB 1,400
STY <50
1,2-Dich <50
GMW-4
Date 03/25/21
B 5,400
T 12,000
E 1,200
X 6,800
MTBE 160
DIPE <50
EDB <50
Naph 190
1,3,5-TMB 160
1,2,4-TMB 640
STY <50
1,2-Dich <50
GMW-5
Date 03/24/21
B 1,800
T 11,000
E 1,800
X 10,000
MTBE 79
DIPE <50
EDB <50
Naph 450
1,3,5-TMB 390
1,2,4-TMB 1,400
STY <50
1,2-Dich <50
GWM-5
MW-18
Date 09/12/18 03/27/19 09/04/20
B 4,800 3,900 2,100
T 26,000 19,000 8,500
E 2,900 2,400 860
X 15,000 13,000 4,500
MTBE 1,500 1,500 590
IPE 500 410 --
EDB <100 <100 <100
Naph 870 730 <100
1,3,5-TMB 600 470 120
1,2,4-TMB 2,400 1,800 440
STY 350 <100 240
1,2-Dich 170 <100 <100
MMPE-2
Date 03/25/21
B 2,000
T 9,700
E 1,600
X 12,000
MTBE <50
DIPE <50
EDB <50
Naph 1,100
1,3,5-TMB 810
1,2,4-TMB 3,000
STY <50
1,2-Dich <50
FIGURE
EXXONMOBIL ENVIRONMENTAL AND PROPERTY SOLUTIONS COMPANY
FORMER EXXONMOBIL FACILITY #44953GASTONIA, NORTH CAROLINA
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MONITORING WELL
RECOVERY WELL
MMPE
OBSERVATION WELL
ABANDONED MONITORING WELL
LNAPL DETECTED
MICROGRAMS PER LITER
NORTH CAROLINAADMINISTRATIVE CODE
NORTH CAROLINA GROSSCONTAMINANT LEVEL
CONCENTRATIONS EXCEEDNCAC 2B STANDARD
CONCENTRATIONS EXCEED NCGCL STANDARDS
CONCENTRATIONS EXCEEDSCALIBRATION RANGE
MS AND/OR MSD RECOVERYEXCEEDS CONTROL LIMITS.
NOT ANALYSED
LEGEND:
GRAPHIC SCALE
DISSOLVED PHASECONCENTRATION MAP
µg/L
SHADED
F1
GCL
NCAC
--
1.UNABLE TO ACCESS THE MONITORING WELL
MW-18 DURING THE MOST RECENT EVENT.
NOTE:
0 60'120'
E
BOLDTreatment Areas
Area A
1,200 ft2
VTI: 15 to 25 ft-bgs
Area B
400 ft2
VTI: 15 to 30 ft-bgs

APPENDIX F
Notice of Intent and Injection Event Record

Submit the original of this form to the Division of Water Resources within 30 days of injection. Form UIC-IER
Attn: UIC Program, 1636 Mail Service Center, Raleigh, NC 27699-1636, Phone No. 919-807-6464 Rev. 3-1-2016
North Carolina Department of Environmental Quality – Division of Water Resources INJECTION EVENT RECORD (IER)
Permit Number_____________________
1. Permit Information
____________________________________
Permittee
_______________________________________ Facility Name
_______________________________________ Facility Address (include County)
2. Injection Contractor Information _______________________________________ Injection Contractor / Company Name Street Address___________________________ _______________________________________ City State Zip Code
(_____) _________________ Area code – Phone number
3. Well Information Number of wells used for injection ___________
Well IDs______________________________ Were any new wells installed during this injection event? Yes No
If yes, please provide the following information: Number of Monitoring Wells _______________ Number of Injection Wells__________________
Type of Well Installed (Check applicable type): Bored Drilled Direct-Push Hand-Augured Other (specify) ________ Please include a copy of the GW-1 form for each well installed.

Were any wells abandoned during this injection event?
Yes No If yes, please provide the following information: Number of Monitoring Wells _______________ Number of Injection Wells__________________ Please include a copy of the GW-30 for each well
abandoned. 4. Injectant Information _______________________________________
Injectant(s) Type (can use separate additional sheets if necessary
Concentration ___________________________ If the injectant is diluted please indicate the source
dilution fluid.____________________________ Total Volume Injected (gal)____________________ Volume Injected per well (gal)_________________ 5. Injection History Injection date(s)_____________________________ Injection number (e.g. 3 of 5)________________
Is this the last injection at this site? Yes No
I DO HEREBY CERTIFY THAT ALL THE
INFORMATION ON THIS FORM IS CORRECT TO THE BEST OF MY KNOWLEDGE AND THAT THE INJECTION WAS PERFORMED WITHIN THE STANDARDS LAID OUT IN THE PERMIT. ____________________________________________________________ SIGNATURE OF INJECTION CONTRACTOR DATE ____________________________________________________________ PRINT NAME OF PERSON PERFORMING THE INJECTION
Ganesha Food Mart
Ganesha Food Mart UST FACID 00-0-0000015835
1617 N Chester St, Gastonia, Gaston
39
IP-1,3,5,8,9,10,and 12-44
X
39
X
Rae Brown/ Geological Resources, Inc performed injection
under the supervision of Deep Earth Technologies, Inc
3502 Hayes Road
Monroe NC 28110
704 845-4010
X
39
Cool-Ox Reagent
See attached
10/25,26,27,30/23
1
X
3,960
0
0
Matt Steele
11/15/23
WI0300497
2657 Pilot R1
4,000
Start End From:To:
10/25/2023 IP-6 1000 1004 0 0 1 0 0 0 0IP-1 1006 1043 15 30 1 120 10 8 150
IP-4 1051 1057 0 0 1 0 0 0 0
IP-11 1058 1059 0 0 1 0 0 0 0
IP-8 1101 1133 15 30 1 120 10 8 150
IP-2 1145 1148 0 0 1 0 0 0 0IP-3 1152 1226 15 30 1 120 10 8 150
IP-5 1324 1431 15 30 1 360 10 8 150IP-7 1442 1450 0 0 1 0 0 0 0
IP-10 1452 1602 15 30 1 360 10 8 150
IP-9 1611 1701 15 30 1 240 10 8 150
TOTAL:11 1320
Date IP #
refusal 3 ft
refusal 4 ft
Area B; refusal 4 ft
refusal 3 ft
Gallons
Cool-Ox ® Daily Field Injection Sheet
10/25/2023
Austin, Barry & Anthony
Office:Client Personnel:Client Project #:Site:Ganesha Food Mart DTI Operations Manager:Subcontract #:
DTI Field Crew:
pH Pressure
Gal/cy
Gastonia, NC5
GPM
refusal 3 ft
CommentsTotal IPs
QUOTE:
2657 Pilot R1
4,000
Start End From:To:
10/26/2023 IP-32 850 912 15 25 1 80 7 8 100IP-42 918 942 15 25 1 80 7 8 100
IP-27 947 1010 15 25 1 80 7 8 100
IP-28 1021 1044 15 25 1 80 7 8 100
IP-36 1051 1104 15 25 1 80 7 8 100
IP-34 1109 1128 15 25 1 80 7 8 100IP-39 1138 1157 15 25 1 80 7 8 100
IP-43 1204 1228 15 25 1 80 7 8 100IP-38 1320 1334 15 25 1 80 7 8 100
IP-40 1339 1356 15 25 1 80 7 8 100
IP-44 1359 1411 15 25 1 80 7 8 100IP-35 1416 1434 15 25 1 80 7 8 100
IP-31 1439 1502 15 25 1 80 7 8 100
IP-24 1505 1524 15 25 1 80 7 8 100
IP-26 1536 1559 15 25 1 80 7 8 100
TOTAL:15 1200
GPM
no reaction
no reaction
no reaction
communication with MW-4
no reaction
no reaction
CommentsTotal IPs
QUOTE:
pH Pressure
Gal/cy
Gastonia, NC5 Austin, Barry & Anthony
Office:Client Personnel:Client Project #:Site:Ganesha Food Mart DTI Operations Manager:Subcontract #:
DTI Field Crew:
Cool-Ox ® Daily Field Injection Sheet
10/26/2023
Date IP #
communication with GMW-3; strong odor; product; slight reaction
no reaction
no reaction
slight odor; product
communication GMW-3
Area Ano reaction
no reaction
Gallons
2657 Pilot R1
4,000
Start End From:To:
10/27/2023 IP-30 842 916 15 25 1 80 7 8 100IP-25 925 943 15 25 1 80 7 8 100
IP-20 949 1011 15 25 1 80 7 8 100
IP-22 1018 1043 15 25 1 80 7 8 100
IP-17 1050 1115 15 25 1 80 7 8 100
IP-19 1122 1149 15 25 1 80 7 8 100IP-12 1306 1327 15 25 1 80 7 8 100
IP-14 1334 1358 15 25 1 80 7 8 100
TOTAL:8 640
GPM
communication GMW-2
communication GMW-2; strong odor
CommentsTotal IPs
QUOTE:
pH Pressure
Gal/cy
Gastonia, NC5 Austin, Barry & Anthony
Office:Client Personnel:Client Project #:Site:Ganesha Food Mart DTI Operations Manager:Subcontract #:
DTI Field Crew:
Cool-Ox ® Daily Field Injection Sheet
10/27/2023
Date IP #
no reaction
no reaction
no reaction
communication GMW-3no reaction
no reaction
Gallons
2657 Pilot R1
4,000
Start End From:To:
10/30/2023 IP-13 845 906 15 25 1 80 7 8 100IP-15 912 930 15 25 1 80 7 8 100
IP-18 935 956 15 25 1 80 7 8 100
IP-16 1000 1013 15 25 1 80 7 8 100
IP-21 1021 1122 15 25 1 80 7 8 100
IP-41 1130 1200 15 25 1 80 7 8 100IP-23 1209 1233 15 25 1 80 7 8 100
IP-29 1303 1327 15 25 1 80 7 8 100IP-33 1335 1358 15 25 1 80 7 8 100
IP-37 1406 1438 15 25 1 80 7 8 100
TOTAL:10 800
Date IP #
no reaction
no reaction
no reaction
communication GMW-2; odorno reaction
no reaction
Gallons
Cool-Ox ® Daily Field Injection Sheet
10/30/2023
Austin, Barry & Anthony
Office:Client Personnel:Client Project #:Site:Ganesha Food Mart DTI Operations Manager:Subcontract #:
DTI Field Crew:
pH Pressure
Gal/cy
Gastonia, NC5
GPM
no reaction
no reaction
no reaction
no reaction
CommentsTotal IPs
QUOTE:
WELL CONSTRUCTION RECORD
This form canbe usedforsingle or multiple wells
FormGW-1 North Carolina Departmentof Environmentand Natural Resources –Division ofWaterResources Revised August 2013
1.Well Contractor Information:
Well ContractorName
NC WellContractor Certification Number
CompanyName
2.Well Construction Permit #:
List all applicable well permits (i.e. County, State, Variance, Injection, etc.)
3.Well Use (check well use):
Water Supply Well:□Agricultural □Municipal/Public□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)□Irrigation
Non-Water Supply Well:□Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier□Aquifer Test □StormwaterDrainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer□Geothermal (Heating/Cooling Return)□Other (explain under #21 Remarks)
4.Date Well(s)Completed:____________Well ID#______________________
5a.Well Location:
Facility/Owner Name Facility ID#(if applicable)

Physical Address,City,and Zip
County Parcel Identification No.(PIN)
5b.Latitudeand Longitudein degrees/minutes/secondsor decimal degrees:(if well field,one lat/long is sufficient)
N W
6.Is (are)the well(s):□Permanent or □Temporary
7.Is this a repair to an existing well:□Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8.Number of wells constructed:
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.
9.Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10.Static water level below topof casing: (ft.)If water level is above casing, use “+”
11.Borehole diameter: (in.)
12.Well construction method: (i.e.auger,rotary,cable,direct push,etc.)
FOR WATER SUPPLY WELLS ONLY:
13a.Yield (gpm) Method oftest:
13b.Disinfection type: Amount:
14.WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15.OUTER CASING (for multi-cased wells)OR LINER(if applicable)FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16.INNER CASING OR TUBING(geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17.SCREENFROMTO DIAMETER SLOTSIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18.GROUT
FROM TO MATERIAL EMPLACEMENT METHOD &AMOUNT
ft.ft.
ft.ft.
ft.ft.
19.SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENTMETHOD
ft.ft.
ft.ft.
20.DRILLING LOG (attach additional sheetsif necessary)FROM TO DESCRIPTION(color,hardness,soil/rock type,grain size,etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21.REMARKS
22.Certification:
Signatureof Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23.Site diagram or additional well details:You may use the back of this page to provide additional well site details or wellconstructiondetails.You may also attach additional pages if necessary.
SUBMITTAL INSTUCTIONS
24a.For All Wells: Submit this form within 30 days of completion of wellconstructiontothefollowing:
Division of Water Resources,Information Processing Unit,1617 Mail Service Center,Raleigh,NC 27699-1617
24b.For Injection Wells ONLY:In addition to sending the form to the address in
24a above,also submit a copy of this form within 30 days of completion of wellconstructiontothefollowing:
Division of Water Resources,Underground Injection Control Program,1636 Mail Service Center,Raleigh,NC 27699-1636
24c.For Water Supply &Injection Wells:
Also submit one copy of this form within 30 days of completion ofwellconstructiontothecountyhealthdepartmentofthecountywhereconstructed.
For Internal UseONLY:
Matt Steele
4548-A
Geological Resources, Inc.
WI0300497
10/25/23 IP-1,3,5,8,9,10
Ganesha Food Mart 00-0-0000015835
1626 North Chester Street, Gastonia, NC, 28052
Gaston 3546-74-2410
35.28117460 -81.18770708
6
30
~25
1.5
Direct Push
25 30 Saturated
NA
NA
15 30 1 Stainless
NA
NA
0 0.25 Asphalt
0.25 30 No soil cuttings generated
Temporary wells to be used for in situ chemical oxidation. After
injection, temporary wells will be abandoned with granular bentonite.
11/6/23
WELL ABANDONMENT RECORD
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name (or well owner personally abandoning well on his/her property)
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) if known
3. Well use (check well use):
Water Supply Well: □Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared) □Irrigation
Non-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control □Geothermal (Closed Loop)□Tracer□Geothermal (Heating/Cooling Return) □Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply wells
ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s): (gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply): □Neat Cement Grout □Bentonite Chips or Pellets
□Sand Cement Grout □Dry Clay
□Concrete Grout □Drill Cuttings □Specialty Grout □Gravel
□Bentonite Slurry □Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
7g. Provide a brief description of the abandonment procedure:
8. Certification:
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
abandoned.
For Internal Use ONLY:
Matthew Steele
4548 A 6
0.2
Geological Resources, Inc.
WI0300497
10 lbs of Bentonite
5 lb concrete
10/25/23
Pour
Wells were used for in situ chemical oxidation
Abandoned with bentonite after injection.Ganesha Food Mart 00-0-000015835
1626 North Chester St., Gastonia NC 28052 11/6/23
Gaston 3456-74-2410
35.28119770 -81.18818532
IP-1,3,5,8,9,10
30
1.5
25
n/a
n/a
15
WELL CONSTRUCTION RECORD
This form canbe usedforsingle or multiple wells
FormGW-1 North Carolina Departmentof Environmentand Natural Resources –Division ofWaterResources Revised August 2013
1.Well Contractor Information:
Well ContractorName
NC WellContractor Certification Number
CompanyName
2.Well Construction Permit #:
List all applicable well permits (i.e. County, State, Variance, Injection, etc.)
3.Well Use (check well use):
Water Supply Well:□Agricultural □Municipal/Public□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)□Irrigation
Non-Water Supply Well:□Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier□Aquifer Test □StormwaterDrainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer□Geothermal (Heating/Cooling Return)□Other (explain under #21 Remarks)
4.Date Well(s)Completed:____________Well ID#______________________
5a.Well Location:
Facility/Owner Name Facility ID#(if applicable)

Physical Address,City,and Zip
County Parcel Identification No.(PIN)
5b.Latitudeand Longitudein degrees/minutes/secondsor decimal degrees:(if well field,one lat/long is sufficient)
N W
6.Is (are)the well(s):□Permanent or □Temporary
7.Is this a repair to an existing well:□Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8.Number of wells constructed:
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.
9.Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10.Static water level below topof casing: (ft.)If water level is above casing, use “+”
11.Borehole diameter: (in.)
12.Well construction method: (i.e.auger,rotary,cable,direct push,etc.)
FOR WATER SUPPLY WELLS ONLY:
13a.Yield (gpm) Method oftest:
13b.Disinfection type:Amount:
14.WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15.OUTER CASING (for multi-cased wells)OR LINER(if applicable)FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16.INNER CASING OR TUBING(geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17.SCREENFROMTO DIAMETER SLOTSIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18.GROUT
FROM TO MATERIAL EMPLACEMENT METHOD &AMOUNT
ft.ft.
ft.ft.
ft.ft.
19.SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENTMETHOD
ft.ft.
ft.ft.
20.DRILLING LOG (attach additional sheetsif necessary)FROM TO DESCRIPTION(color,hardness,soil/rock type,grain size,etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21.REMARKS
22.Certification:
Signatureof Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23.Site diagram or additional well details:You may use the back of this page to provide additional well site details or wellconstructiondetails.You may also attach additional pages if necessary.
SUBMITTAL INSTUCTIONS
24a.For All Wells: Submit this form within 30 days of completion of wellconstructiontothefollowing:
Division of Water Resources,Information Processing Unit,1617 Mail Service Center,Raleigh,NC 27699-1617
24b.For Injection Wells ONLY:In addition to sending the form to the address in
24a above,also submit a copy of this form within 30 days of completion of wellconstructiontothefollowing:
Division of Water Resources,Underground Injection Control Program,1636 Mail Service Center,Raleigh,NC 27699-1636
24c.For Water Supply &Injection Wells:
Also submit one copy of this form within 30 days of completion ofwellconstructiontothecountyhealthdepartmentofthecountywhereconstructed.
For Internal UseONLY:
Matt Steele
4548-A
Geological Resources, Inc.
WI0300497
10/26-30/23 IP-12 thru IP-44
Ganesha Food Mart 00-0-0000015835
1617 North Chester Street, Gastonia, NC, 28052
Gaston 3546-64-9362
35.28119770 -81.18818532
33
25
~15
1.5
Direct Push
15 25 Saturated
NA
NA
15 25 1 Stainless
NA
NA
0 0.25 Asphalt
0.25 1 No soil cuttings generated
Temporary wells to be used for in situ chemical oxidation. After
injection, will be abandoned with granular bentonite.
11/6/23
WELL ABANDONMENT RECORD
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name (or well owner personally abandoning well on his/her property)
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) if known
3. Well use (check well use):
Water Supply Well: □Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared) □Irrigation
Non-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control □Geothermal (Closed Loop)□Tracer□Geothermal (Heating/Cooling Return) □Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply wells
ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s): (gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply): □Neat Cement Grout □Bentonite Chips or Pellets
□Sand Cement Grout □Dry Clay
□Concrete Grout □Drill Cuttings □Specialty Grout □Gravel
□Bentonite Slurry □Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
7g. Provide a brief description of the abandonment procedure:
8. Certification:
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
abandoned.
For Internal Use ONLY:
Matthew Steele
4548 A 33
0.4
Geological Resources, Inc.
WI0300497
10 lbs of Bentonite
5 lb concrete
10/26-30/23
Pour
Wells were used for in situ chemical oxidation
Abandoned with bentonite after injection.Ganesha Food Mart 00-0-000015835
1617 North Chester St., Gastonia NC 28052 11/6/23
Gaston 3546-64-9362
35.28119770 -81.18818532
IP-12 thru IP-44
25
1.5
15
n/a
n/a
15
1
Rae Brown
From:Butcher, Blake L <[e-mail]>
Sent:Tuesday, August 22, 2023 12:14 PM
To:Rae Brown
Subject:RE: [External] FW: Ganesha (GRI 4457) NOI
Hey Rae,

I spoke with my supervisor, and we have decided to treat these two NOI’s as one. The second NOI will be considered
supplemental informa on and will be documented in Laserfiche as such. Please use the NOI tracking number
(WI0300497) in all future correspondence, repor ng forms, and in the subject line of all emails regarding the NOI
tracking number. Please refer to NOI confirma on email for addi onal informa on. Please feel free to contact me if
you have any ques ons regarding this email.

Thank you and have a great a ernoon,

Blake Butcher
Geologist/Hydrogeologist, Underground Injec on Control
NC Division of Water Resources – Groundwater Management Branch
1636 Mail Service Center
Raleigh, NC 27699
Office: 1-919-707-3671
[e-mail]

*At present I am primarily teleworking. The best way to contact me is via email.

From: Rae Brown <[e-mail]>
Sent: Tuesday, August 22, 2023 11:39 AM
To: Butcher, Blake L <[e-mail]>
Subject: RE: [External] FW: Ganesha (GRI 4457) NOI

CAUTION: External email. Do not click links or open attachments unless verified. Report suspicious emails with the Report Message
button located on your Outlook menu bar on the Home tab.

No rush – I just didn’t see an email confirma on so I resent. Good luck with the big permit. I am sure there is a lot to
learn.

Rae

Rae Troiano Brown, P.G.
Project Manager
Geological Resources, Inc.
113 Firetower Road, Suite G
Winterville, NC 28590
Main [phone] Cell [phone]
www.geologicalresourcesinc.com

2
From: Butcher, Blake L <[e-mail]>
Sent: Tuesday, August 22, 2023 11:34 AM
To: Rae Brown <[e-mail]>
Subject: RE: [External] FW: Ganesha (GRI 4457) NOI

Hey Rae,
I apologize, I’ve been working my way through my first big permit since last week. I will process your NOI this a ernoon.
Have a great day,

Blake Butcher
Geologist/Hydrogeologist, Underground Injec on Control
NC Division of Water Resources – Groundwater Management Branch
1636 Mail Service Center
Raleigh, NC 27699
Office: 1-919-707-3671
[e-mail]

*At present I am primarily teleworking. The best way to contact me is via email.

From: Rae Brown <[e-mail]>
Sent: Tuesday, August 22, 2023 11:28 AM
To: Butcher, Blake L <[e-mail]>
Subject: [External] FW: Ganesha (GRI 4457) NOI

CAUTION: External email. Do not click links or open attachments unless verified. Report suspicious emails with the Report Message
button located on your Outlook menu bar on the Home tab.

Hey Blake,

I wanted to be sure that you received this – I am sure you are busy with the upcoming move!

Rae

Rae Troiano Brown, P.G.
Project Manager
Geological Resources, Inc.
113 Firetower Road, Suite G
Winterville, NC 28590
Main [phone] Cell [phone]
www.geologicalresourcesinc.com

From: Rae Brown
Sent: Thursday, August 17, 2023 4:41 PM
To: Butcher, Blake L <[e-mail]>
Subject: Ganesha (GRI 4457) NOI

Hi Blake,

3
This is another NOI for Ganesha, but this NOI is for the off-site property. The injec on is in the DOT ROW. It is s ll the
same UST release (Incident 40741) with Incident Manager Brad Newton (Morrisville RO). Please let me know if you need
addi onal informa on.

Thank you,
Rae

Rae Troiano Brown, P.G.
Project Manager
Geological Resources, Inc.
113 Firetower Road, Suite G
Winterville, NC 28590
Main [phone] Cell [phone]
www.geologicalresourcesinc.com

Email correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third parties by an authorized
state official.
Deemed Permitted GW Remediation NOI Rev. 3-1-2023 Page 1
NC Department of Environmental Quality (DEQ) – Division of Water Resources (DWR)

Print Clearly or Type Information. Illegible Submittals Will Be Returned as Incomplete.
DATE: , 20_23__ NOI TRACKING NO. (To be filled in by DWR)
DIRECTIONS- Submit this NOI only for (1) New deemed ‘permitted by rule’ injection project or (2) If there is going
to be a different permit type (listed above) used for a previously issued NOI.
NOTE- After this NOI is processed and acknowledged, any supplemental or additional injections still meeting the
criteria referenced in Section G below shall be reported using Injection Event Records (IERs) and using the NOI
tracking number provided by DWR.
A. WELL TYPE TO BE CONSTRUCTED OR OPERATED
(1)Air Injection Well……………………………..…. Complete sections B through F, J, M
(2)Aquifer Test Well……………………….……….. Complete sections B through F, J, M
(3)Passive Injection System………………….……... Complete sections B through F, H-M
(4)Small-Scale Injection Operation…………………. Complete sections B through M
(5) X Pilot Test…………………………………………. Complete sections B through M
(6)Tracer Injection Well………………………….…. Complete sections B through M
(7)In-Situ Thermal (IST) Well……………………… Complete sections B through M
NOTIFICATION OF INTENT (NOI) TO CONSTRUCT OR OPERATE INJECTION WELLS
The following are “permitted by rule” and do not require an application to be submitted and an individual permit
be issued when constructed in accordance with the rules of 15A NCAC 02C .0200 (NOTE: This form must be
received at least 14 DAYS prior to injection)
GROUNDWATER (GW) REMEDIATION INJECTION PERMIT TYPES:
(1) IN-SITU GW REMEDIATION PERMIT TYPE (15A NCAC 02C .0225)
In-Situ Passive Injection Systems - In-well delivery systems to diffuse injectants into the subsurface. Examples include
ORC socks, iSOC systems, and other gas infusion methods (Note: Injection Event Records (IER) do not need to be
submitted for replacement of each sock used in ORC systems).
In-Situ Small-Scale Injection Operations – Injection wells located within a land surface area not to exceed 10,000
square feet (SF) for the purpose of soil or groundwater remediation or tracer tests. If area to be treated exceeds 10,000
SF do not use this NOI; an injection Permit application shall be submitted, and a Permit issued per 15A NCAC
02C .0225(f).
In-Situ Pilot Tests - Preliminary studies conducted for the purpose of evaluating the technical feasibility of a
remediation strategy to develop a full-scale remediation plan for future implementation, and where the surface area of
the injection zone wells is located within an area that does not exceed five percent of the land surface above the known
extent of groundwater contamination. Also, if pilot test is going to be conducted on separate groundwater
contaminant plumes do not use this NOI; a Permit application shall be submitted, and a Permit issued as per
15A NCAC 02C .0225(f).
In-Situ Thermal (IST) – IST wells ‘heat’ contaminated groundwater in-situ to enhance remediation.
(2) AIR INJECTION PERMIT TYPE (15A NCAC 02C .0225)
These permit types are used to inject ambient air to enhance treatment of soil or groundwater.
(3) TRACER WELL PERMIT TYPE (15A NCAC 02C .0229)
These permit types are used to inject substances for determining hydrogeologic properties of aquifers.
(4) AQUIFER TEST PERMIT TYPE (15A NCAC 02C .0220)
These permit types are used to inject uncontaminated fluid into an aquifer to determine aquifer hydraulic characteristics.
08/15 WI0300497
Deemed Permitted GW Remediation NOI Rev. 3-1-2023 Page 2
B. STATUS OF WELL OWNER: State Government
C. WELL OWNER(S) – State name of Business/Agency, and Name and Title of person delegated authority to
sign on behalf of the business or agency:
Name(s): GANESHA FOOD MART
Mailing Address: 1716 North Chester Street
City: Gastonia State: NC Zip Code: 28052-9443 County: Gaston
Day Tele No.: 704-906-9443 Cell No.: 704-906-9443
EMAIL Address: [e-mail] Fax No.: N/A
D. PROPERTY OWNER(S) (if different than well owner/applicant)
Name and Title: Milan Patel, owner
Company Name Janki Dhayti, Inc.
Mailing Address: 1716 North Chester Street
City: Gastonia State: NC Zip Code: 28502 County: Gaston
Day Tele No.: 704-906-9443 Cell No.: 704-906-9443
EMAIL Address: [e-mail] Fax No.: N/A
E. PROJECT CONTACT (Typically Environmental Consulting/Engineering Firm)
Name and Title: Rae Troiano Brown, Project Manager
Company Name Geological Resources, Inc.
Mailing Address: 3502 Hayes Road
City: Monroe State: NC Zip Code:28110 County: Union
Day Tele No.: 704-845-4010 Cell No.: 252-227-3005
EMAIL Address: [e-mail] Fax No.: 704-845-4012
F. PHYSICAL LOCATION OF WELL SITE
(1) Facility Name & Address: Ganesha Food Mart, 1617 North Chester Street

City: Gastonia County: Gaston Zip Code: 28052
(2) Geographic Coordinates: Latitude**: o ′ ″ or 35 o. 28119770
Longitude**: o ′ ″ or -81 o. 18818532
Reference Datum: WGS84 Accuracy: <1’
Method of Collection: Mobile GPS Unit
**FOR AIR INJECTION AND AQUIFER TEST WELLS ONLY: A FACILITY SITE MAP WITH PROPERTY
BOUNDARIES MAY BE SUBMITTED IN LIEU OF GEOGRAPHIC COORDINATES.
G. TREATMENT AREA
Land surface area of contaminant plume: 33,485 square feet
Land surface area of inj. well network: 1,600 square feet (< 10,000 ft2 for small-scale injections)
Percent of contaminant plume area to be treated: 4.8 (must be < 5% of plume for pilot test injections)

Deemed Permitted GW Remediation NOI Rev. 3-1-2023 Page 3
H. INJECTION ZONE MAPS – Attach the following to the notification.
(1) Contaminant plume map(s) with isoconcentration lines that show the horizontal extent of the
contaminant plume in soil and groundwater, existing and proposed monitoring wells, and existing and
proposed injection wells; and
(2) Cross-section(s) to the known or projected depth of contamination that show the horizontal and vertical
extent of the contaminant plume in soil and groundwater, changes in lithology, existing and proposed
monitoring wells, and existing and proposed injection wells.
(3) Potentiometric surface map(s) indicating the rate and direction of groundwater movement, plus existing
and proposed wells.

I. DESCRIPTION OF PROPOSED INJECTION ACTIVITIES AT THE SITE – Provide a brief narrative
regarding the cause of the contamination, and purpose, scope, goals of the proposed injection activity:
The contamination at the site is the result of a UST release in 1995. The contaminant plumes are located on the
site of origin (1617 North Chester Street) and 1626 North Chester Street. Prior remedial activities include: 871.5
tons impacted soil remediated by soil thermal treatment (1995), 275 gallons of LNAP recovered by AFVR (1998-
2001), 205 gallons LNAPL recovered in 6 MMPE events (2002 – 2008), Dual phase extraction unit operated
off-site (1626 North Chester Street) for 6 months in 2012, and Air sparge/soil vapor extraction on 1617 North
Chester Street (2012). The incident risk has been reduced to intermediate based on a site conceptual model that
concluded there was no complete contaminant pathway to any receptors in the area. Therefore, cleanup goals
are to remove free product and reduce ground water contamination to less than GCLs. The pilot study area for
the on-site plume is limited to the area around the monitoring wells with the highest GCL violations and Free
Product. The injectant selected was Cool-Ox® because it will initially oxidize petroleum contaminants and then
provide oxygen to enhance the biological degradation.

J. WELL CONSTRUCTION DATA

(1) No. of injection wells: 33 Proposed 0 Existing (provide NC Well
Construction Record (GW-1) for each well)
(2) Appx. injection depths (BLS):______25_________________________________________________
(3) For Proposed wells or Existing wells not having GW-1s, provide well construction details for each
injection well in a diagram or table format. A single diagram or line in a table can be used for
multiple wells with the same construction details. Well construction details shall include the
following (indicate if construction is proposed or as-built):
(a) Well type as permanent, Geoprobe/DPT, or subsurface distribution infiltration gallery
(b) Depth below land surface of casing, each grout type and depth, screen, and sand pack
(c) Well contractor name and certification number

K. INJECTION SUMMARY

NOTE: Only injectants approved by the epidemiology section of the NC Division of Public Health, Department
of Health and Human Services can be injected. Approved injectants can be found online at
http://deq.nc.gov/about/divisions/water-resources/water-resources-permits/wastewater-branch/ground-water-
protection/ground-water-approved-injectants. All other substances must be reviewed by the DHHS prior to use.
Contact the UIC Program for more info if you wish to get approval for a different additive. However, please
note it may take 3 months or longer. If no injectants are to be used use N/A.

Deemed Permitted GW Remediation NOI Rev. 3-1-2023 Page 5
Please send 1 (one) hard color copy of this NOI along with a copy on an attached CD or Flash Drive at least
two (2) weeks prior to injection to:

DWR – UIC Program
1636 Mail Service Center
Raleigh, NC 27699-1636
Telephone: [phone]
BLDG
GRASS
BILLBOARD
ASPHALT
PARKINGGRASS
RADIO AVE.
GRASS
CAR WASH
STORAGE
GRASS
FORMER
BUILDING
KIOSK
FORMERDISPENSER
ISLANDS
INSTALLATION
OF USTs ON
4/16/83 AND
9/23/81
HISTORIC
UST FIELD
64'-83'
LP
GRASS
TANK
FARM
(CONCRETE)
ASPHALT
BLDG
ASPHALT
(Bradshaw's
Market)
HISTORIC
DISPENSER PUMPS
71'-83'
GRASS
BLDG
INSTALLATION OF
CURRENT USTs ON
5/31/71
GRASS
BLDG
ASPHALT
PARKING
CANOPY
INSTALLATION
OF USTs ON
4/16/83
GRASS
HIGH VOLTAGE
UTILITY TOWER
TS
BL
D
G
U.
S
.

H
I
G
H
W
A
Y

3
2
1
GR
A
S
S

M
E
D
I
A
N
CR
E
E
K
RA
I
L
R
O
A
D

T
R
A
C
K
S
Estimated area for pilot
study; 1,600 sq feet; 33
injection points; 6' apart
A
A'
34,022.2 17,140 61,230 FP (sheen)
5/18/23
100,000
10,000
1,000
100
FP
Injection wells will be installed between GWM-1 and GMW-4 to 25' deep at 6' intervals
FORMER
BUILDING
FORMER
DISPENSER
ISLANDS
INSTALLATION
OF USTs ON
4/16/83 AND
9/23/81
UP LP
TS
UP
UPLP
LP LP
LP
LP
UPLP
LP
LP
LP
LP
LP
LP
LP
LP
LP
UPLP
UP
UP
PD
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CANOPY
CANOPY
GRASS
TANK
FARM
(CONCRETE)
GRASS
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ASPHALT
RADIO AVE.
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HIGH VOLTAGE
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REMEDIATION
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RECOVERY POINT
FREE PRODUCT
SKIMMER
EQUIPMENT
RA
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HISTORIC
UST FIELD
64'-83'
BLDG
BLDG
BLDG
KIOSK
CAR WASH
BL
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BLDG
(Bradshaw's
Market)
STORAGE
BLDG
INSTALLATION
OF USTs ON
4/16/83
HISTORIC
DISPENSER PUMPS
71'-83'
INSTALLATION OF
CURRENT USTs ON
5/31/71
MW-11
(697.57)
MW-12
(NL)
MW-13(697.20)
MW-14
(696.57)
MW-20
(696.29)
MW-19
(699.74)
MW-18
(UTA)
MW-16
(699.91)
MW-21(699.76)
GWM-4(713.82)
GWM-3
(713.71)
GWM-2(713.91)
GWM-1
(714.08)
MW-1
MW-7
MW-5
MW-3
MW-2
DW-1
OB-1(713.49)
MW2R/MMPE1
(715.34)RW-2
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MW-9
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MW-17
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(713.26)
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69
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0
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8
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6
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6
FIGURE
EXXONMOBIL ENVIRONMENTAL AND PROPERTY SOLUTIONS COMPANY
FORMER EXXONMOBIL FACILITY #44953
GASTONIA, NORTH CAROLINA
1st SEMI-ANNUAL CORRECTIVE ACTION PLAN MONITORING REPORT - 2021
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POTENTIOMETRIC SURFACE MAP -
MARCH 23, 2021
MONITORING WELL
RECOVERY WELL
MMPE
OBSERVATION WELL
ABANDONED MONITORING WELL
GROUNDWATER ELEVATION
CONTOUR (DASHED WHERE
INFERRED)
GROUNDWATER ELEVATION
(FEET ABOVE MEAN SEA LEVEL)
GROUNDWATER FLOW
DIRECTION
NOT LOCATED
NOT AVAILABLE
UNABLE TO ACCESS
1.MMPE-2 HAD MEASURABLE FREE PRODUCT.
GROUNDWATER ELEVATION SHOWN IS CORRECTED.
NOTE:
LEGEND:
GRAPHIC SCALE
0 60'120'
(714.08)
(NL)
(NA)
(UTA)PARCEL #100048
PARCEL #100050
Estimated area for pilot
study; 1,600 sq feet; 33
injection points; 6' apart
Well ID Well Type
Installation
Method Diameter
Total well
Depth (ft)
Grout
type Screen Sand pack Well driller
TMW - 1 thru 33 Temporary Direct Push 1.5"25 NA NA NA
Justin Radford
NC License
#3270A
Notes:
NA: Not applicable: temporary wells to be abandoned after injection of CoolOx® solution to design depths. Temporary wells to
be abandoned using granualar bentonite only.
1
Rae Brown
From:Butcher, Blake L <[e-mail]>
Sent:Tuesday, August 22, 2023 12:14 PM
To:Rae Brown
Subject:RE: [External] FW: Ganesha (GRI 4457) NOI
Hey Rae,

I spoke with my supervisor, and we have decided to treat these two NOI’s as one. The second NOI will be considered
supplemental informa on and will be documented in Laserfiche as such. Please use the NOI tracking number
(WI0300497) in all future correspondence, repor ng forms, and in the subject line of all emails regarding the NOI
tracking number. Please refer to NOI confirma on email for addi onal informa on. Please feel free to contact me if
you have any ques ons regarding this email.

Thank you and have a great a ernoon,

Blake Butcher
Geologist/Hydrogeologist, Underground Injec on Control
NC Division of Water Resources – Groundwater Management Branch
1636 Mail Service Center
Raleigh, NC 27699
Office: 1-919-707-3671
[e-mail]

*At present I am primarily teleworking. The best way to contact me is via email.

From: Rae Brown <[e-mail]>
Sent: Tuesday, August 22, 2023 11:39 AM
To: Butcher, Blake L <[e-mail]>
Subject: RE: [External] FW: Ganesha (GRI 4457) NOI

CAUTION: External email. Do not click links or open attachments unless verified. Report suspicious emails with the Report Message
button located on your Outlook menu bar on the Home tab.

No rush – I just didn’t see an email confirma on so I resent. Good luck with the big permit. I am sure there is a lot to
learn.

Rae

Rae Troiano Brown, P.G.
Project Manager
Geological Resources, Inc.
113 Firetower Road, Suite G
Winterville, NC 28590
Main [phone] Cell [phone]
www.geologicalresourcesinc.com

2
From: Butcher, Blake L <[e-mail]>
Sent: Tuesday, August 22, 2023 11:34 AM
To: Rae Brown <[e-mail]>
Subject: RE: [External] FW: Ganesha (GRI 4457) NOI

Hey Rae,
I apologize, I’ve been working my way through my first big permit since last week. I will process your NOI this a ernoon.
Have a great day,

Blake Butcher
Geologist/Hydrogeologist, Underground Injec on Control
NC Division of Water Resources – Groundwater Management Branch
1636 Mail Service Center
Raleigh, NC 27699
Office: 1-919-707-3671
[e-mail]

*At present I am primarily teleworking. The best way to contact me is via email.

From: Rae Brown <[e-mail]>
Sent: Tuesday, August 22, 2023 11:28 AM
To: Butcher, Blake L <[e-mail]>
Subject: [External] FW: Ganesha (GRI 4457) NOI

CAUTION: External email. Do not click links or open attachments unless verified. Report suspicious emails with the Report Message
button located on your Outlook menu bar on the Home tab.

Hey Blake,

I wanted to be sure that you received this – I am sure you are busy with the upcoming move!

Rae

Rae Troiano Brown, P.G.
Project Manager
Geological Resources, Inc.
113 Firetower Road, Suite G
Winterville, NC 28590
Main [phone] Cell [phone]
www.geologicalresourcesinc.com

From: Rae Brown
Sent: Thursday, August 17, 2023 4:41 PM
To: Butcher, Blake L <[e-mail]>
Subject: Ganesha (GRI 4457) NOI

Hi Blake,

3
This is another NOI for Ganesha, but this NOI is for the off-site property. The injec on is in the DOT ROW. It is s ll the
same UST release (Incident 40741) with Incident Manager Brad Newton (Morrisville RO). Please let me know if you need
addi onal informa on.

Thank you,
Rae

Rae Troiano Brown, P.G.
Project Manager
Geological Resources, Inc.
113 Firetower Road, Suite G
Winterville, NC 28590
Main [phone] Cell [phone]
www.geologicalresourcesinc.com

Email correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third parties by an authorized
state official.

APPENDIX G
Laboratory Reports

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

1/10/2024
Geological Resources, Inc. Rae Brown
113 West Firetower Road, Suite G Winterville, NC, 28590
Ref: Analytical Testing
Lab Report Number: 23-363-0017 Client Project Description: Ganesha
GRI #4457
Dear Rae Brown:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 12/29/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 36
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2024402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Page 1 of 1 00016/23-363-0017
Page 2 of 36
Report Number:
Sample Summary Table
Client Project Description:
23-363-0017
Ganesha
GRI #4457
Lab No Client Sample ID Matrix Date Collected Date Received
12/26/2023 12:28Aqueous 92887 GMW-4 12/29/2023 11:22
12/26/2023 12:50Aqueous 92888 MW-21 12/29/2023 11:22
12/26/2023 11:45Aqueous 92889 Trip Blank 12/29/2023 11:22
Page 3 of 36
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-363-0017
Report Limit
Project:Ganesha
V 92887GMW-4
J38801/03/2024 19:136200BAcetoneµg/L 180
6590 01/03/2024 19:136200BBenzeneµg/L 18.0
J22.9 01/03/2024 19:136200Bn-Butylbenzene µg/L 18.0
66.0 01/03/2024 19:136200BChloroformµg/L 22.0
1680000 01/08/2024 19:146200BEthanolµg/L 42000
1940 01/03/2024 19:136200BEthylbenzeneµg/L 17.0
71.2 01/03/2024 19:136200BIsopropylbenzeneµg/L 18.0
J23901/03/2024 19:136200BMethyl Ethyl Ketone (MEK)µg/L 71.0
149 01/03/2024 19:136200BMethyl tert-butyl ether (MTBE)µg/L 14.0
435 01/03/2024 19:136200BNaphthaleneµg/L 47.0
166 01/03/2024 19:136200Bn-Propylbenzene µg/L 19.0
J40.9 01/03/2024 19:136200BStyreneµg/L 22.0
1480 01/03/2024 19:136200Btert-Butyl Alcohol (TBA)µg/L 160
9760 01/03/2024 19:136200Btert-Amyl Alcohol (TAA)µg/L 190
15800 01/08/2024 19:146200BTolueneµg/L 220
1310 01/03/2024 19:136200B1,2,4-Trimethylbenzene µg/L 19.0
305 01/03/2024 19:136200B1,3,5-Trimethylbenzene µg/L 18.0
3550 01/03/2024 19:136200Bo-Xylene µg/L 21.0
7110 01/03/2024 19:136200Bm,p-Xylene µg/L 42.0
10700 01/03/2024 19:136200BXylene (Total)µg/L 21.0
V 92888MW-21
26400 01/09/2024 19:576200BBenzeneµg/L 180
J26.1 01/08/2024 16:456200Bn-Butylbenzene µg/L 18.0
1350 01/08/2024 16:456200BDi-Isopropyl Ether (DIPE)µg/L 50.0
455 01/08/2024 16:456200B1,2-Dibromoethane µg/L 20.0
163 01/08/2024 16:456200B1,2-Dichloroethane µg/L 15.0
4080 01/08/2024 16:456200BEthylbenzeneµg/L 17.0
J62.1 01/08/2024 16:456200B2-Hexanone µg/L 38.0
147 01/08/2024 16:456200BIsopropylbenzeneµg/L 18.0
J33501/08/2024 16:456200BMethyl Ethyl Ketone (MEK)µg/L 71.0
226 01/08/2024 16:456200BMethyl tert-butyl ether (MTBE)µg/L 14.0
1360 01/08/2024 16:456200BNaphthaleneµg/L 47.0
365 01/08/2024 16:456200Bn-Propylbenzene µg/L 19.0
824 01/08/2024 16:456200BStyreneµg/L 22.0
11100 01/09/2024 19:576200Btert-Amyl Alcohol (TAA)µg/L 1900
36300 01/09/2024 19:576200BTolueneµg/L 220
Page 4 of 36
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-363-0017
Report Limit
Project:Ganesha
V 92888MW-21
2740 01/08/2024 16:456200B1,2,4-Trimethylbenzene µg/L 19.0
672 01/08/2024 16:456200B1,3,5-Trimethylbenzene µg/L 18.0
6610 01/08/2024 16:456200Bo-Xylene µg/L 21.0
12900 01/08/2024 16:456200Bm,p-Xylene µg/L 42.0
19500 01/08/2024 16:456200BXylene (Total)µg/L 21.0
V 92889Trip Blank
J2.56 01/08/2024 11:246200BMethyl Ethyl Ketone (MEK)µg/L 0.710
Page 5 of 36

Client: Geological Resources, Inc. CASE NARRATIVE
Project: Ganesha Lab Report Number: 23-363-0017
Date: 1/10/2024
Volatile Organic Compounds - GC/MS Method 6200B Analyte: 1,2,3-Trichlorobenzene QC Batch No: V42022/V41953
LCSD fails high. All other QC for this batch passes including the LCS. Data no affected.
Analyte: 1,2,3-Trichlorobenzene QC Batch No: V42078/V41953
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: 2-Butanone QC Batch No: V42095/V41953
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable. All hits below MQL.
Analyte: Acetone
QC Batch No: V41956/V41953 CCV fails low. All other QC passes within method parameters. Data not affected. No further action taken. Analyte: Acetone
QC Batch No: V42095/V41953 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
All hits below MQL. Analyte: 1,2-Dibromo-3-chloropropane QC Batch No: V41956/V41953
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable. Analyte: 1,2-Dibromo-3-chloropropane QC Batch No: V42022/V41953 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable. Analyte: tert-Amyl alcohol QC Batch No: V41956/V41953 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Page 6 of 36

Analyte: tert-Amyl alcohol
QC Batch No: V42022/V41953 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.

Page 7 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-363-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/29/2023
Ganesha
Report Date : 01/10/2024
Sample ID :
Lab No :
Sampled:GMW-4
92887 Matrix:
12/26/2023 12:28
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 01/03/24 19:13 6200BMSA
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%01/03/24 19:13100 MSA V41956
Surrogate: Dibromofluoromethane 93.8 Limits: 70-130%01/03/24 19:13100 MSA V41956
Surrogate: 1,2-Dichloroethane - d4 90.0 Limits: 70-130%01/03/24 19:13100 MSA V41956
Surrogate: Toluene-d8 102 Limits: 70-130%01/03/24 19:13100 MSA V41956
Surrogate: 4-Bromofluorobenzene 97.0 Limits: 70-130%01/08/24 19:141000 MSA V42078
Surrogate: Dibromofluoromethane 101 Limits: 70-130%01/08/24 19:141000 MSA V42078
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%01/08/24 19:141000 MSA V42078
Surrogate: Toluene-d8 95.8 Limits: 70-130%01/08/24 19:141000 MSA V42078
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-363-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/29/2023
Ganesha
Report Date : 01/10/2024
Sample ID :
Lab No :
Sampled:GMW-4
92887 Matrix:
12/26/2023 12:28
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41953 01/03/24 09:00 V42072 01/08/24 09:00
388 J µg/L 180 1000Acetone 100 01/03/24 19:13 V41956MSA
6590 µg/L 18.0 50.0Benzene 100 01/03/24 19:13 V41956MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 01/03/24 19:13 V41956MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 01/03/24 19:13 V41956MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 01/03/24 19:13 V41956MSA
<150 µg/L 150 500Bromoform 100 01/03/24 19:13 V41956MSA
<28.0 µg/L 28.0 100Bromomethane 100 01/03/24 19:13 V41956MSA
22.9 J µg/L 18.0 50.0n-Butylbenzene 100 01/03/24 19:13 V41956MSA
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 01/03/24 19:13 V41956MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 01/03/24 19:13 V41956MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 01/03/24 19:13 V41956MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 01/03/24 19:13 V41956MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 01/03/24 19:13 V41956MSA
<43.0 µg/L 43.0 100Chloroethane 100 01/03/24 19:13 V41956MSA
66.0 µg/L 22.0 50.0Chloroform 100 01/03/24 19:13 V41956MSA
<22.0 µg/L 22.0 50.0Chloromethane 100 01/03/24 19:13 V41956MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 01/03/24 19:13 V41956MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 01/03/24 19:13 V41956MSA
<50.0 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 01/03/24 19:13 V41956MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 01/03/24 19:13 V41956MSA
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 01/03/24 19:13 V41956MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 01/03/24 19:13 V41956MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-363-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/29/2023
Ganesha
Report Date : 01/10/2024
Sample ID :
Lab No :
Sampled:GMW-4
92887 Matrix:
12/26/2023 12:28
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41953 01/03/24 09:00 V42072 01/08/24 09:00
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 01/03/24 19:13 V41956MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 01/03/24 19:13 V41956MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 01/03/24 19:13 V41956MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 01/03/24 19:13 V41956MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 01/03/24 19:13 V41956MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 01/03/24 19:13 V41956MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 01/03/24 19:13 V41956MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 01/03/24 19:13 V41956MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 01/03/24 19:13 V41956MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 01/03/24 19:13 V41956MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 01/03/24 19:13 V41956MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 01/03/24 19:13 V41956MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 01/03/24 19:13 V41956MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 01/03/24 19:13 V41956MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 01/03/24 19:13 V41956MSA
1680000 µg/L 42000 200000Ethanol 1000 01/08/24 19:14 V42078MSA
1940 µg/L 17.0 50.0Ethylbenzene 100 01/03/24 19:13 V41956MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 01/03/24 19:13 V41956MSA
<38.0 µg/L 38.0 1002-Hexanone 100 01/03/24 19:13 V41956MSA
71.2 µg/L 18.0 50.0Isopropylbenzene 100 01/03/24 19:13 V41956MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 01/03/24 19:13 V41956MSA
239 J µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 01/03/24 19:13 V41956MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-363-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/29/2023
Ganesha
Report Date : 01/10/2024
Sample ID :
Lab No :
Sampled:GMW-4
92887 Matrix:
12/26/2023 12:28
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41953 01/03/24 09:00 V42072 01/08/24 09:00
149 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 01/03/24 19:13 V41956MSA
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 01/03/24 19:13 V41956MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 01/03/24 19:13 V41956MSA
435 µg/L 47.0 100Naphthalene 100 01/03/24 19:13 V41956MSA
166 µg/L 19.0 50.0n-Propylbenzene 100 01/03/24 19:13 V41956MSA
40.9 J µg/L 22.0 50.0Styrene 100 01/03/24 19:13 V41956MSA
1480 µg/L 160 1000tert-Butyl Alcohol (TBA)100 01/03/24 19:13 V41956MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 01/03/24 19:13 V41956MSA
9760 µg/L 190 1000tert-Amyl Alcohol (TAA)100 01/03/24 19:13 V41956MSA
<28.0 µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 01/03/24 19:13 V41956MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 01/03/24 19:13 V41956MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 01/03/24 19:13 V41956MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 01/03/24 19:13 V41956MSA
15800 µg/L 220 500Toluene 1000 01/08/24 19:14 V42078MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 01/03/24 19:13 V41956MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 01/03/24 19:13 V41956MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 01/03/24 19:13 V41956MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 01/03/24 19:13 V41956MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 01/03/24 19:13 V41956MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 01/03/24 19:13 V41956MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 01/03/24 19:13 V41956MSA
1310 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 01/03/24 19:13 V41956MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-363-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/29/2023
Ganesha
Report Date : 01/10/2024
Sample ID :
Lab No :
Sampled:GMW-4
92887 Matrix:
12/26/2023 12:28
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V41953 01/03/24 09:00 V42072 01/08/24 09:00
305 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 01/03/24 19:13 V41956MSA
<100 µg/L 100 500Vinyl Acetate 100 01/03/24 19:13 V41956MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 01/03/24 19:13 V41956MSA
3550 µg/L 21.0 50.0o-Xylene 100 01/03/24 19:13 V41956MSA
7110 µg/L 42.0 100m,p-Xylene 100 01/03/24 19:13 V41956MSA
10700 µg/L 21.0 50.0Xylene (Total)100 01/03/24 19:13 V41956
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%01/03/24 19:13100 MSA V41956
Surrogate: Dibromofluoromethane 93.8 Limits: 70-130%01/03/24 19:13100 MSA V41956
Surrogate: 1,2-Dichloroethane - d4 90.0 Limits: 70-130%01/03/24 19:13100 MSA V41956
Surrogate: Toluene-d8 102 Limits: 70-130%01/03/24 19:13100 MSA V41956
Surrogate: 4-Bromofluorobenzene 97.0 Limits: 70-130%01/08/24 19:141000 MSA V42078
Surrogate: Dibromofluoromethane 101 Limits: 70-130%01/08/24 19:141000 MSA V42078
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%01/08/24 19:141000 MSA V42078
Surrogate: Toluene-d8 95.8 Limits: 70-130%01/08/24 19:141000 MSA V42078
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-363-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/29/2023
Ganesha
Report Date : 01/10/2024
Sample ID :
Lab No :
Sampled:MW-21
92888 Matrix:
12/26/2023 12:50
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 01/08/24 16:45 6200BMSA
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%01/08/24 16:45100 MSA V42078
Surrogate: Dibromofluoromethane 99.6 Limits: 70-130%01/08/24 16:45100 MSA V42078
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%01/08/24 16:45100 MSA V42078
Surrogate: Toluene-d8 97.4 Limits: 70-130%01/08/24 16:45100 MSA V42078
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%01/09/24 19:571000 MSA V42095
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%01/09/24 19:571000 MSA V42095
Surrogate: 1,2-Dichloroethane - d4 105 Limits: 70-130%01/09/24 19:571000 MSA V42095
Surrogate: Toluene-d8 107 Limits: 70-130%01/09/24 19:571000 MSA V42095
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-363-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/29/2023
Ganesha
Report Date : 01/10/2024
Sample ID :
Lab No :
Sampled:MW-21
92888 Matrix:
12/26/2023 12:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V42072 01/08/24 09:00 V42094 01/09/24 09:00
<180 µg/L 180 1000Acetone 100 01/08/24 16:45 V42078MSA
26400 µg/L 180 500Benzene 1000 01/09/24 19:57 V42095MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 01/08/24 16:45 V42078MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 01/08/24 16:45 V42078MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 01/08/24 16:45 V42078MSA
<150 µg/L 150 500Bromoform 100 01/08/24 16:45 V42078MSA
<28.0 µg/L 28.0 100Bromomethane 100 01/08/24 16:45 V42078MSA
26.1 J µg/L 18.0 50.0n-Butylbenzene 100 01/08/24 16:45 V42078MSA
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 01/08/24 16:45 V42078MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 01/08/24 16:45 V42078MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 01/08/24 16:45 V42078MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 01/08/24 16:45 V42078MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 01/08/24 16:45 V42078MSA
<43.0 µg/L 43.0 100Chloroethane 100 01/08/24 16:45 V42078MSA
<22.0 µg/L 22.0 50.0Chloroform 100 01/08/24 16:45 V42078MSA
<22.0 µg/L 22.0 50.0Chloromethane 100 01/08/24 16:45 V42078MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 01/08/24 16:45 V42078MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 01/08/24 16:45 V42078MSA
1350 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 01/08/24 16:45 V42078MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 01/08/24 16:45 V42078MSA
455 µg/L 20.0 50.01,2-Dibromoethane 100 01/08/24 16:45 V42078MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 01/08/24 16:45 V42078MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-363-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/29/2023
Ganesha
Report Date : 01/10/2024
Sample ID :
Lab No :
Sampled:MW-21
92888 Matrix:
12/26/2023 12:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V42072 01/08/24 09:00 V42094 01/09/24 09:00
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 01/08/24 16:45 V42078MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 01/08/24 16:45 V42078MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 01/08/24 16:45 V42078MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 01/08/24 16:45 V42078MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 01/08/24 16:45 V42078MSA
163 µg/L 15.0 50.01,2-Dichloroethane 100 01/08/24 16:45 V42078MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 01/08/24 16:45 V42078MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 01/08/24 16:45 V42078MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 01/08/24 16:45 V42078MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 01/08/24 16:45 V42078MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 01/08/24 16:45 V42078MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 01/08/24 16:45 V42078MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 01/08/24 16:45 V42078MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 01/08/24 16:45 V42078MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 01/08/24 16:45 V42078MSA
<4200 µg/L 4200 20000Ethanol 100 01/08/24 16:45 V42078MSA
4080 µg/L 17.0 50.0Ethylbenzene 100 01/08/24 16:45 V42078MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 01/08/24 16:45 V42078MSA
62.1 J µg/L 38.0 1002-Hexanone 100 01/08/24 16:45 V42078MSA
147 µg/L 18.0 50.0Isopropylbenzene 100 01/08/24 16:45 V42078MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 01/08/24 16:45 V42078MSA
335 J µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 01/08/24 16:45 V42078MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-363-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/29/2023
Ganesha
Report Date : 01/10/2024
Sample ID :
Lab No :
Sampled:MW-21
92888 Matrix:
12/26/2023 12:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V42072 01/08/24 09:00 V42094 01/09/24 09:00
226 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 01/08/24 16:45 V42078MSA
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 01/08/24 16:45 V42078MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 01/08/24 16:45 V42078MSA
1360 µg/L 47.0 100Naphthalene 100 01/08/24 16:45 V42078MSA
365 µg/L 19.0 50.0n-Propylbenzene 100 01/08/24 16:45 V42078MSA
824 µg/L 22.0 50.0Styrene 100 01/08/24 16:45 V42078MSA
<160 µg/L 160 1000tert-Butyl Alcohol (TBA)100 01/08/24 16:45 V42078MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 01/08/24 16:45 V42078MSA
11100 µg/L 1900 10000tert-Amyl Alcohol (TAA)1000 01/09/24 19:57 V42095MSA
<28.0 µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 01/08/24 16:45 V42078MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 01/08/24 16:45 V42078MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 01/08/24 16:45 V42078MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 01/08/24 16:45 V42078MSA
36300 µg/L 220 500Toluene 1000 01/09/24 19:57 V42095MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 01/08/24 16:45 V42078MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 01/08/24 16:45 V42078MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 01/08/24 16:45 V42078MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 01/08/24 16:45 V42078MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 01/08/24 16:45 V42078MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 01/08/24 16:45 V42078MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 01/08/24 16:45 V42078MSA
2740 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 01/08/24 16:45 V42078MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-363-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/29/2023
Ganesha
Report Date : 01/10/2024
Sample ID :
Lab No :
Sampled:MW-21
92888 Matrix:
12/26/2023 12:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V42072 01/08/24 09:00 V42094 01/09/24 09:00
672 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 01/08/24 16:45 V42078MSA
<100 µg/L 100 500Vinyl Acetate 100 01/08/24 16:45 V42078MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 01/08/24 16:45 V42078MSA
6610 µg/L 21.0 50.0o-Xylene 100 01/08/24 16:45 V42078MSA
12900 µg/L 42.0 100m,p-Xylene 100 01/08/24 16:45 V42078MSA
19500 µg/L 21.0 50.0Xylene (Total)100 01/08/24 16:45 V42078
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%01/08/24 16:45100 MSA V42078
Surrogate: Dibromofluoromethane 99.6 Limits: 70-130%01/08/24 16:45100 MSA V42078
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%01/08/24 16:45100 MSA V42078
Surrogate: Toluene-d8 97.4 Limits: 70-130%01/08/24 16:45100 MSA V42078
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%01/09/24 19:571000 MSA V42095
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%01/09/24 19:571000 MSA V42095
Surrogate: 1,2-Dichloroethane - d4 105 Limits: 70-130%01/09/24 19:571000 MSA V42095
Surrogate: Toluene-d8 107 Limits: 70-130%01/09/24 19:571000 MSA V42095
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-363-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/29/2023
Ganesha
Report Date : 01/10/2024
Sample ID :
Lab No :
Sampled:Trip Blank
92889 Matrix:
12/26/2023 11:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V42072 01/08/24 09:00
<1.80 µg/L 1.80 10.0Acetone 1 01/08/24 11:24 V42078MSA
<0.180 µg/L 0.180 0.500Benzene 1 01/08/24 11:24 V42078MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 01/08/24 11:24 V42078MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 01/08/24 11:24 V42078MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 01/08/24 11:24 V42078MSA
<1.50 µg/L 1.50 5.00Bromoform 1 01/08/24 11:24 V42078MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 01/08/24 11:24 V42078MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 01/08/24 11:24 V42078MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 01/08/24 11:24 V42078MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 01/08/24 11:24 V42078MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 01/08/24 11:24 V42078MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 01/08/24 11:24 V42078MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 01/08/24 11:24 V42078MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 01/08/24 11:24 V42078MSA
<0.220 µg/L 0.220 0.500Chloroform 1 01/08/24 11:24 V42078MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 01/08/24 11:24 V42078MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 01/08/24 11:24 V42078MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 01/08/24 11:24 V42078MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 01/08/24 11:24 V42078MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 01/08/24 11:24 V42078MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 01/08/24 11:24 V42078MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 01/08/24 11:24 V42078MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-363-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/29/2023
Ganesha
Report Date : 01/10/2024
Sample ID :
Lab No :
Sampled:Trip Blank
92889 Matrix:
12/26/2023 11:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V42072 01/08/24 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 01/08/24 11:24 V42078MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 01/08/24 11:24 V42078MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 01/08/24 11:24 V42078MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 01/08/24 11:24 V42078MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 01/08/24 11:24 V42078MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 01/08/24 11:24 V42078MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 01/08/24 11:24 V42078MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 01/08/24 11:24 V42078MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 01/08/24 11:24 V42078MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 01/08/24 11:24 V42078MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 01/08/24 11:24 V42078MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 01/08/24 11:24 V42078MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 01/08/24 11:24 V42078MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 01/08/24 11:24 V42078MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 01/08/24 11:24 V42078MSA
<42.0 µg/L 42.0 200Ethanol 1 01/08/24 11:24 V42078MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 01/08/24 11:24 V42078MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 01/08/24 11:24 V42078MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 01/08/24 11:24 V42078MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 01/08/24 11:24 V42078MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 01/08/24 11:24 V42078MSA
2.56 J µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 01/08/24 11:24 V42078MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-363-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/29/2023
Ganesha
Report Date : 01/10/2024
Sample ID :
Lab No :
Sampled:Trip Blank
92889 Matrix:
12/26/2023 11:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V42072 01/08/24 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 01/08/24 11:24 V42078MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 01/08/24 11:24 V42078MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 01/08/24 11:24 V42078MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 01/08/24 11:24 V42078MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 01/08/24 11:24 V42078MSA
<0.220 µg/L 0.220 0.500Styrene 1 01/08/24 11:24 V42078MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 01/08/24 11:24 V42078MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 01/08/24 11:24 V42078MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 01/08/24 11:24 V42078MSA
<0.220 µg/L 0.220 0.500Toluene 1 01/08/24 11:24 V42078MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 01/08/24 11:24 V42078MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 01/08/24 11:24 V42078MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 01/08/24 11:24 V42078MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 01/08/24 11:24 V42078MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 01/08/24 11:24 V42078MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 01/08/24 11:24 V42078MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 01/08/24 11:24 V42078MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 01/08/24 11:24 V42078MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 01/08/24 11:24 V42078MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 01/08/24 11:24 V42078MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 01/08/24 11:24 V42078MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 01/08/24 11:24 V42078MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-363-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/29/2023
Ganesha
Report Date : 01/10/2024
Sample ID :
Lab No :
Sampled:Trip Blank
92889 Matrix:
12/26/2023 11:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V42072 01/08/24 09:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 01/08/24 11:24 V42078MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 01/08/24 11:24 V42078
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%01/08/24 11:241 MSA V42078
Surrogate: Dibromofluoromethane 97.8 Limits: 70-130%01/08/24 11:241 MSA V42078
Surrogate: 1,2-Dichloroethane - d4 98.6 Limits: 70-130%01/08/24 11:241 MSA V42078
Surrogate: Toluene-d8 99.0 Limits: 70-130%01/08/24 11:241 MSA V42078
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 36
Quality Control Data
23-363-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41956QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41953
Associated Lab Samples: 92887
LRB-V41953 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/03/24 12:3910.01.80<1.80µg/LAcetone
01/03/24 12:390.5000.180<0.180µg/LBenzene
01/03/24 12:390.5000.210<0.210µg/LBromobenzene
01/03/24 12:391.000.420<0.420µg/LBromochloromethane
01/03/24 12:390.5000.160<0.160µg/LBromodichloromethane
01/03/24 12:395.001.50<1.50µg/LBromoform
01/03/24 12:391.000.280<0.280µg/LBromomethane
01/03/24 12:390.5000.180<0.180µg/Ln-Butylbenzene
01/03/24 12:390.5000.200<0.200µg/Lsec-Butyl benzene
01/03/24 12:392.000.920<0.920µg/Ltert-Butyl benzene
01/03/24 12:390.5000.180<0.180µg/LCarbon Tetrachloride
01/03/24 12:390.5000.190<0.190µg/LChlorobenzene
01/03/24 12:390.5000.190<0.190µg/LChlorodibromomethane
01/03/24 12:391.000.430<0.430µg/LChloroethane
01/03/24 12:390.5000.220<0.220µg/LChloroform
01/03/24 12:390.5000.220<0.220µg/LChloromethane
01/03/24 12:390.5000.200<0.200µg/L2-Chlorotoluene
01/03/24 12:390.5000.200<0.200µg/L4-Chlorotoluene
01/03/24 12:390.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
01/03/24 12:392.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
01/03/24 12:390.5000.200<0.200µg/L1,2-Dibromoethane
01/03/24 12:390.5000.230<0.230µg/LDibromomethane
01/03/24 12:390.5000.220<0.220µg/L1,2-Dichlorobenzene
01/03/24 12:390.5000.190<0.190µg/L1,3-Dichlorobenzene
01/03/24 12:390.5000.210<0.210µg/L1,4-Dichlorobenzene
01/03/24 12:395.001.20<1.20µg/LDichlorodifluoromethane
01/03/24 12:390.5000.240<0.240µg/L1,1-Dichloroethane
Page 1 of 13Date:01/10/2024 04:24 PM
Page 22 of 36
Quality Control Data
23-363-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41956QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41953
Associated Lab Samples: 92887
LRB-V41953 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/03/24 12:390.5000.150<0.150µg/L1,2-Dichloroethane
01/03/24 12:390.5000.150<0.150µg/L1,1-Dichloroethene
01/03/24 12:390.5000.200<0.200µg/Lcis-1,2-Dichloroethene
01/03/24 12:390.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
01/03/24 12:390.5000.190<0.190µg/L1,2-Dichloropropane
01/03/24 12:390.5000.130<0.130µg/L1,3-Dichloropropane
01/03/24 12:392.000.210<0.210µg/L2,2-Dichloropropane
01/03/24 12:390.5000.200<0.200µg/L1,1-Dichloropropene
01/03/24 12:390.5000.210<0.210µg/Lcis-1,3-Dichloropropene
01/03/24 12:390.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
01/03/24 12:390.5000.170<0.170µg/LEthylbenzene
01/03/24 12:393.000.350<0.350µg/LHexachlorobutadiene
01/03/24 12:391.000.380<0.380µg/L2-Hexanone
01/03/24 12:390.5000.180<0.180µg/LIsopropylbenzene
01/03/24 12:390.5000.089<0.089µg/L4-Isopropyl toluene
01/03/24 12:395.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
01/03/24 12:391.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
01/03/24 12:391.000.078<0.078µg/L4-Methyl-2-Pentanone
01/03/24 12:392.000.330<0.330µg/LMethylene Chloride
01/03/24 12:391.000.470<0.470µg/LNaphthalene
01/03/24 12:390.5000.190<0.190µg/Ln-Propylbenzene
01/03/24 12:390.5000.220<0.220µg/LStyrene
01/03/24 12:3910.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
01/03/24 12:3910.00.350<0.350µg/Ltert-Butyl formate (TBF)
01/03/24 12:3910.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
01/03/24 12:3910.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
01/03/24 12:390.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
Page 2 of 13Date:01/10/2024 04:24 PM
Page 23 of 36
Quality Control Data
23-363-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41956QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41953
Associated Lab Samples: 92887
LRB-V41953 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/03/24 12:390.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
01/03/24 12:390.5000.220<0.220µg/LTetrachloroethene
01/03/24 12:390.5000.380<0.380µg/L1,2,3-Trichlorobenzene
01/03/24 12:390.5000.310<0.310µg/L1,2,4-Trichlorobenzene
01/03/24 12:390.5000.160<0.160µg/L1,1,1-Trichloroethane
01/03/24 12:390.5000.096<0.096µg/L1,1,2-Trichloroethane
01/03/24 12:390.5000.180<0.180µg/LTrichloroethene
01/03/24 12:390.5000.180<0.180µg/LTrichlorofluoromethane
01/03/24 12:390.5000.270<0.270µg/L1,2,3-Trichloropropane
01/03/24 12:390.5000.190<0.190µg/L1,2,4-Trimethylbenzene
01/03/24 12:390.5000.180<0.180µg/L1,3,5-Trimethylbenzene
01/03/24 12:395.001.00<1.00µg/LVinyl Acetate
01/03/24 12:390.5000.170<0.170µg/LVinyl Chloride
01/03/24 12:390.5000.210<0.210µg/Lo-Xylene
01/03/24 12:391.000.420<0.420µg/Lm,p-Xylene
01/03/24 12:3910.01.00<1.00µg/L3,3-Dimethyl-1-butanol
01/03/24 12:394-Bromofluorobenzene (S)100 70-130
01/03/24 12:39Dibromofluoromethane (S)97.2 70-130
01/03/24 12:391,2-Dichloroethane - d4 (S)92.0 70-130
01/03/24 12:39Toluene-d8 (S)103 70-130
LCS-V41953 LCSD-V41953Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
41.2 10311044.040.0µg/LAcetone 40-160 6.5 20.0
20.2 10110120.220.0µg/LBenzene 70-130 0.0 20.0
Page 3 of 13Date:01/10/2024 04:24 PM
Page 24 of 36
Quality Control Data
23-363-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41956QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41953
LCS-V41953 LCSD-V41953Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
23.1 11611422.820.0µg/LBromobenzene 70-130 1.3 20.0
21.2 10610320.520.0µg/LBromochloromethane 70-130 3.3 20.0
19.9 99.599.019.820.0µg/LBromodichloromethane 70-130 0.5 20.0
21.9 11010921.720.0µg/LBromoform 70-130 0.9 20.0
16.7 83.575.015.020.0µg/LBromomethane 60-140 10.7 20.0
24.4 12212224.320.0µg/Ln-Butylbenzene 70-130 0.4 20.0
24.4 12212024.020.0µg/Lsec-Butyl benzene 70-130 1.6 20.0
24.3 12211923.820.0µg/Ltert-Butyl benzene 70-130 2.0 20.0
22.2 11111222.320.0µg/LCarbon Tetrachloride 70-130 0.4 20.0
22.7 11411322.620.0µg/LChlorobenzene 70-130 0.4 20.0
22.6 11311122.220.0µg/LChlorodibromomethane 70-130 1.7 20.0
20.2 10111022.020.0µg/LChloroethane 60-140 8.5 20.0
20.0 10010120.220.0µg/LChloroform 70-130 0.9 20.0
18.1 90.589.517.920.0µg/LChloromethane 60-140 1.1 20.0
23.4 11711723.320.0µg/L2-Chlorotoluene 70-130 0.4 20.0
23.3 11711523.020.0µg/L4-Chlorotoluene 70-130 1.2 20.0
18.5 92.592.518.520.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.0 20.0
25.6 128131*26.220.0µg/L1,2-Dibromo-3-Chloropropane 70-130 2.3 20.0
23.0 11511322.620.0µg/L1,2-Dibromoethane 70-130 1.7 20.0
20.3 10210020.020.0µg/LDibromomethane 70-130 1.4 20.0
23.7 11911523.020.0µg/L1,2-Dichlorobenzene 70-130 2.9 20.0
23.3 11711623.120.0µg/L1,3-Dichlorobenzene 70-130 0.8 20.0
23.7 11911923.720.0µg/L1,4-Dichlorobenzene 70-130 0.0 20.0
15.2 76.076.015.220.0µg/LDichlorodifluoromethane 60-140 0.0 20.0
19.7 98.597.019.420.0µg/L1,1-Dichloroethane 70-130 1.5 20.0
19.2 96.097.019.420.0µg/L1,2-Dichloroethane 70-130 1.0 20.0
Page 4 of 13* QC Fail Date:01/10/2024 04:24 PM
Page 25 of 36
Quality Control Data
23-363-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41956QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41953
LCS-V41953 LCSD-V41953Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.6 10310320.620.0µg/L1,1-Dichloroethene 70-130 0.0 20.0
18.9 94.595.519.120.0µg/Lcis-1,2-Dichloroethene 70-130 1.0 20.0
20.4 10299.519.920.0µg/Ltrans-1,2-Dichloroethene 70-130 2.4 20.0
19.2 96.097.019.420.0µg/L1,2-Dichloropropane 70-130 1.0 20.0
21.5 10810821.520.0µg/L1,3-Dichloropropane 70-130 0.0 20.0
20.5 10310621.220.0µg/L2,2-Dichloropropane 70-130 3.3 20.0
21.9 11011021.920.0µg/L1,1-Dichloropropene 70-130 0.0 20.0
20.1 10199.519.920.0µg/Lcis-1,3-Dichloropropene 70-130 1.0 20.0
19.8 99.098.519.720.0µg/Ltrans-1,3-Dichloropropene 70-130 0.5 20.0
22.2 11111022.020.0µg/LEthylbenzene 70-130 0.9 20.0
25.9 13012625.120.0µg/LHexachlorobutadiene 70-130 3.1 20.0
22.0 11011322.520.0µg/L2-Hexanone 60-140 2.2 20.0
24.4 12212124.220.0µg/LIsopropylbenzene 70-130 0.8 20.0
25.4 12712524.920.0µg/L4-Isopropyl toluene 70-130 1.9 20.0
20.0 10010721.320.0µg/LMethyl Ethyl Ketone (MEK)60-140 6.2 20.0
20.1 10110220.420.0µg/LMethyl tert-butyl ether (MTBE)70-130 1.4 20.0
19.1 95.596.019.220.0µg/L4-Methyl-2-Pentanone 60-140 0.5 20.0
18.2 91.089.017.820.0µg/LMethylene Chloride 70-130 2.2 20.0
25.6 12811623.220.0µg/LNaphthalene 70-130 9.8 20.0
23.8 11911723.420.0µg/Ln-Propylbenzene 70-130 1.6 20.0
22.4 11211222.320.0µg/LStyrene 70-130 0.4 20.0
40.8 10211445.440.0µg/Ltert-Butyl Alcohol (TBA)40-140 10.6 20.0
40.4 10110140.340.0µg/Ltert-Butyl formate (TBF)40-140 0.2 20.0
16.5 82.510420.820.0µg/Ltert-Amyl Alcohol (TAA)40-140 23.0*20.0
44.6 11211244.640.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 0.0 20.0
23.4 11711723.320.0µg/L1,1,1,2-Tetrachloroethane 70-130 0.4 20.0
Page 5 of 13* QC Fail Date:01/10/2024 04:24 PM
Page 26 of 36
Quality Control Data
23-363-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41956QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41953
LCS-V41953 LCSD-V41953Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
22.5 11311322.620.0µg/L1,1,2,2-Tetrachloroethane 70-130 0.4 20.0
23.7 11911723.420.0µg/LTetrachloroethene 70-130 1.2 20.0
27.0 135*12525.020.0µg/L1,2,3-Trichlorobenzene 70-130 7.6 20.0
25.8 12911823.620.0µg/L1,2,4-Trichlorobenzene 70-130 8.9 20.0
20.9 10510420.720.0µg/L1,1,1-Trichloroethane 70-130 0.9 20.0
20.6 10310320.620.0µg/L1,1,2-Trichloroethane 70-130 0.0 20.0
21.4 10710721.420.0µg/LTrichloroethene 70-130 0.0 20.0
23.9 12012023.920.0µg/LTrichlorofluoromethane 60-140 0.0 20.0
22.2 11111422.720.0µg/L1,2,3-Trichloropropane 70-130 2.2 20.0
24.5 12312124.220.0µg/L1,2,4-Trimethylbenzene 70-130 1.2 20.0
24.7 12412224.320.0µg/L1,3,5-Trimethylbenzene 70-130 1.6 20.0
19.6 98.011222.320.0µg/LVinyl Acetate 60-140 12.8 20.0
20.6 10310420.720.0µg/LVinyl Chloride 60-140 0.4 20.0
22.7 11411322.520.0µg/Lo-Xylene 70-130 0.8 20.0
47.7 11911947.740.0µg/Lm,p-Xylene 70-130 0.0 20.0
20.7 10410621.120.0µg/L3,3-Dimethyl-1-butanol 70-130 1.9 20.0
1021014-Bromofluorobenzene (S)70-130
96.696.6Dibromofluoromethane (S)70-130
92.492.81,2-Dichloroethane - d4 (S)70-130
103103Toluene-d8 (S)70-130
Page 6 of 13* QC Fail Date:01/10/2024 04:24 PM
Page 27 of 36
Quality Control Data
23-363-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V42078QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V42072
Associated Lab Samples: 92887, 92888, 92889
LRB-V42072 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/08/24 11:0010.01.80<1.80µg/LAcetone
01/08/24 11:000.5000.180<0.180µg/LBenzene
01/08/24 11:000.5000.210<0.210µg/LBromobenzene
01/08/24 11:001.000.420<0.420µg/LBromochloromethane
01/08/24 11:000.5000.160<0.160µg/LBromodichloromethane
01/08/24 11:005.001.50<1.50µg/LBromoform
01/08/24 11:001.000.280<0.280µg/LBromomethane
01/08/24 11:000.5000.180<0.180µg/Ln-Butylbenzene
01/08/24 11:000.5000.200<0.200µg/Lsec-Butyl benzene
01/08/24 11:002.000.920<0.920µg/Ltert-Butyl benzene
01/08/24 11:000.5000.180<0.180µg/LCarbon Tetrachloride
01/08/24 11:000.5000.190<0.190µg/LChlorobenzene
01/08/24 11:000.5000.190<0.190µg/LChlorodibromomethane
01/08/24 11:001.000.430<0.430µg/LChloroethane
01/08/24 11:000.5000.220<0.220µg/LChloroform
01/08/24 11:000.5000.220<0.220µg/LChloromethane
01/08/24 11:000.5000.200<0.200µg/L2-Chlorotoluene
01/08/24 11:000.5000.200<0.200µg/L4-Chlorotoluene
01/08/24 11:000.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
01/08/24 11:002.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
01/08/24 11:000.5000.200<0.200µg/L1,2-Dibromoethane
01/08/24 11:000.5000.230<0.230µg/LDibromomethane
01/08/24 11:000.5000.220<0.220µg/L1,2-Dichlorobenzene
01/08/24 11:000.5000.190<0.190µg/L1,3-Dichlorobenzene
01/08/24 11:000.5000.210<0.210µg/L1,4-Dichlorobenzene
01/08/24 11:005.001.20<1.20µg/LDichlorodifluoromethane
01/08/24 11:000.5000.240<0.240µg/L1,1-Dichloroethane
Page 7 of 13Date:01/10/2024 04:24 PM
Page 28 of 36
Quality Control Data
23-363-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V42078QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V42072
Associated Lab Samples: 92887, 92888, 92889
LRB-V42072 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/08/24 11:000.5000.150<0.150µg/L1,2-Dichloroethane
01/08/24 11:000.5000.150<0.150µg/L1,1-Dichloroethene
01/08/24 11:000.5000.200<0.200µg/Lcis-1,2-Dichloroethene
01/08/24 11:000.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
01/08/24 11:000.5000.190<0.190µg/L1,2-Dichloropropane
01/08/24 11:000.5000.130<0.130µg/L1,3-Dichloropropane
01/08/24 11:002.000.210<0.210µg/L2,2-Dichloropropane
01/08/24 11:000.5000.200<0.200µg/L1,1-Dichloropropene
01/08/24 11:000.5000.210<0.210µg/Lcis-1,3-Dichloropropene
01/08/24 11:000.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
01/08/24 11:0020042.0<42.0µg/LEthanol
01/08/24 11:000.5000.170<0.170µg/LEthylbenzene
01/08/24 11:003.000.350<0.350µg/LHexachlorobutadiene
01/08/24 11:001.000.380<0.380µg/L2-Hexanone
01/08/24 11:000.5000.180<0.180µg/LIsopropylbenzene
01/08/24 11:000.5000.089<0.089µg/L4-Isopropyl toluene
01/08/24 11:005.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
01/08/24 11:001.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
01/08/24 11:001.000.078<0.078µg/L4-Methyl-2-Pentanone
01/08/24 11:002.000.330<0.330µg/LMethylene Chloride
01/08/24 11:001.000.470<0.470µg/LNaphthalene
01/08/24 11:000.5000.190<0.190µg/Ln-Propylbenzene
01/08/24 11:000.5000.220<0.220µg/LStyrene
01/08/24 11:0010.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
01/08/24 11:0010.00.350<0.350µg/Ltert-Butyl formate (TBF)
01/08/24 11:0010.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
01/08/24 11:000.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
Page 8 of 13Date:01/10/2024 04:24 PM
Page 29 of 36
Quality Control Data
23-363-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V42078QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V42072
Associated Lab Samples: 92887, 92888, 92889
LRB-V42072 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/08/24 11:000.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
01/08/24 11:000.5000.220<0.220µg/LTetrachloroethene
01/08/24 11:000.5000.220<0.220µg/LToluene
01/08/24 11:000.5000.380<0.380µg/L1,2,3-Trichlorobenzene
01/08/24 11:000.5000.310<0.310µg/L1,2,4-Trichlorobenzene
01/08/24 11:000.5000.160<0.160µg/L1,1,1-Trichloroethane
01/08/24 11:000.5000.096<0.096µg/L1,1,2-Trichloroethane
01/08/24 11:000.5000.180<0.180µg/LTrichloroethene
01/08/24 11:000.5000.180<0.180µg/LTrichlorofluoromethane
01/08/24 11:000.5000.270<0.270µg/L1,2,3-Trichloropropane
01/08/24 11:000.5000.190<0.190µg/L1,2,4-Trimethylbenzene
01/08/24 11:000.5000.180<0.180µg/L1,3,5-Trimethylbenzene
01/08/24 11:005.001.00<1.00µg/LVinyl Acetate
01/08/24 11:000.5000.170<0.170µg/LVinyl Chloride
01/08/24 11:000.5000.210<0.210µg/Lo-Xylene
01/08/24 11:001.000.420<0.420µg/Lm,p-Xylene
01/08/24 11:0010.01.00<1.00µg/L3,3-Dimethyl-1-butanol
01/08/24 11:004-Bromofluorobenzene (S)104 70-130
01/08/24 11:00Dibromofluoromethane (S)96.2 70-130
01/08/24 11:001,2-Dichloroethane - d4 (S)97.2 70-130
01/08/24 11:00Toluene-d8 (S)99.8 70-130
LCS-V42072Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
135*26.920.0µg/L1,2,3-Trichlorobenzene 70-130
Page 9 of 13* QC Fail Date:01/10/2024 04:24 PM
Page 30 of 36
Quality Control Data
23-363-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V42078QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V42072
LCS-V42072 LCSD-V42072Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
51.9 13013554.140.0µg/LAcetone 40-160 4.1 20.0
20.7 10410520.920.0µg/LBenzene 70-130 0.9 20.0
22.7 11411623.220.0µg/LBromobenzene 70-130 2.1 20.0
20.8 10410521.020.0µg/LBromochloromethane 70-130 0.9 20.0
20.9 10510521.020.0µg/LBromodichloromethane 70-130 0.4 20.0
21.9 11010821.520.0µg/LBromoform 70-130 1.8 20.0
17.1 85.578.015.620.0µg/LBromomethane 60-140 9.1 20.0
23.9 12012324.520.0µg/Ln-Butylbenzene 70-130 2.4 20.0
23.1 11611823.620.0µg/Lsec-Butyl benzene 70-130 2.1 20.0
23.0 11511723.420.0µg/Ltert-Butyl benzene 70-130 1.7 20.0
23.0 11511823.520.0µg/LCarbon Tetrachloride 70-130 2.1 20.0
21.8 10911322.520.0µg/LChlorobenzene 70-130 3.1 20.0
21.9 11011122.220.0µg/LChlorodibromomethane 70-130 1.3 20.0
22.5 11311923.720.0µg/LChloroethane 60-140 5.1 20.0
21.3 10710721.420.0µg/LChloroform 70-130 0.4 20.0
21.0 10510220.420.0µg/LChloromethane 60-140 2.8 20.0
22.7 11411422.720.0µg/L2-Chlorotoluene 70-130 0.0 20.0
22.3 11211523.020.0µg/L4-Chlorotoluene 70-130 3.0 20.0
21.5 10810821.620.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.4 20.0
25.6 12812725.420.0µg/L1,2-Dibromo-3-Chloropropane 70-130 0.7 20.0
22.5 11311422.820.0µg/L1,2-Dibromoethane 70-130 1.3 20.0
20.6 10310520.920.0µg/LDibromomethane 70-130 1.4 20.0
22.6 11311522.920.0µg/L1,2-Dichlorobenzene 70-130 1.3 20.0
22.4 11211322.620.0µg/L1,3-Dichlorobenzene 70-130 0.8 20.0
22.3 11211522.920.0µg/L1,4-Dichlorobenzene 70-130 2.6 20.0
16.9 84.585.017.020.0µg/LDichlorodifluoromethane 60-140 0.5 20.0
Page 10 of 13Date:01/10/2024 04:24 PM
Page 31 of 36
Quality Control Data
23-363-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V42078QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V42072
LCS-V42072 LCSD-V42072Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.1 10610721.320.0µg/L1,1-Dichloroethane 70-130 0.9 20.0
21.1 10610621.120.0µg/L1,2-Dichloroethane 70-130 0.0 20.0
22.5 11311823.620.0µg/L1,1-Dichloroethene 70-130 4.7 20.0
20.3 10210420.820.0µg/Lcis-1,2-Dichloroethene 70-130 2.4 20.0
21.3 10710821.620.0µg/Ltrans-1,2-Dichloroethene 70-130 1.3 20.0
20.1 10110320.520.0µg/L1,2-Dichloropropane 70-130 1.9 20.0
21.4 10710921.720.0µg/L1,3-Dichloropropane 70-130 1.3 20.0
21.6 10811222.420.0µg/L2,2-Dichloropropane 70-130 3.6 20.0
22.5 11311623.120.0µg/L1,1-Dichloropropene 70-130 2.6 20.0
20.2 10110320.520.0µg/Lcis-1,3-Dichloropropene 70-130 1.4 20.0
20.4 10210220.420.0µg/Ltrans-1,3-Dichloropropene 70-130 0.0 20.0
473 94.690.4452500µg/LEthanol 60-140 4.5 20.0
21.7 10911021.920.0µg/LEthylbenzene 70-130 0.9 20.0
24.0 12012424.720.0µg/LHexachlorobutadiene 70-130 2.8 20.0
25.6 12813426.820.0µg/L2-Hexanone 60-140 4.5 20.0
23.1 11611823.620.0µg/LIsopropylbenzene 70-130 2.1 20.0
24.1 12112324.520.0µg/L4-Isopropyl toluene 70-130 1.6 20.0
24.8 12412825.620.0µg/LMethyl Ethyl Ketone (MEK)60-140 3.1 20.0
21.2 10610621.220.0µg/LMethyl tert-butyl ether (MTBE)70-130 0.0 20.0
22.4 11211222.420.0µg/L4-Methyl-2-Pentanone 60-140 0.0 20.0
20.5 10310621.120.0µg/LMethylene Chloride 70-130 2.8 20.0
24.4 12212124.120.0µg/LNaphthalene 70-130 1.2 20.0
22.8 11411623.120.0µg/Ln-Propylbenzene 70-130 1.3 20.0
21.6 10811021.920.0µg/LStyrene 70-130 1.3 20.0
46.6 11711646.440.0µg/Ltert-Butyl Alcohol (TBA)40-140 0.4 20.0
46.4 11611947.540.0µg/Ltert-Butyl formate (TBF)40-140 2.3 20.0
Page 11 of 13Date:01/10/2024 04:24 PM
Page 32 of 36
Quality Control Data
23-363-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V42078QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V42072
LCS-V42072 LCSD-V42072Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
45.6 11411545.940.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 0.6 20.0
22.9 11511723.420.0µg/L1,1,1,2-Tetrachloroethane 70-130 2.1 20.0
22.5 11311322.520.0µg/L1,1,2,2-Tetrachloroethane 70-130 0.0 20.0
22.9 11511422.820.0µg/LTetrachloroethene 70-130 0.4 20.0
20.4 10210420.720.0µg/LToluene 70-130 1.4 20.0
24.3 12212925.720.0µg/L1,2,4-Trichlorobenzene 70-130 5.6 20.0
21.9 11011222.420.0µg/L1,1,1-Trichloroethane 70-130 2.2 20.0
21.0 10510320.620.0µg/L1,1,2-Trichloroethane 70-130 1.9 20.0
21.5 10810821.620.0µg/LTrichloroethene 70-130 0.4 20.0
25.4 12713025.920.0µg/LTrichlorofluoromethane 60-140 1.9 20.0
22.1 11110921.820.0µg/L1,2,3-Trichloropropane 70-130 1.3 20.0
23.0 11511823.620.0µg/L1,2,4-Trimethylbenzene 70-130 2.5 20.0
23.0 11511823.620.0µg/L1,3,5-Trimethylbenzene 70-130 2.5 20.0
20.6 10310120.220.0µg/LVinyl Acetate 60-140 1.9 20.0
22.2 11111021.920.0µg/LVinyl Chloride 60-140 1.3 20.0
22.1 11111021.920.0µg/Lo-Xylene 70-130 0.9 20.0
46.3 11611746.840.0µg/Lm,p-Xylene 70-130 1.0 20.0
16.3 81.579.515.920.0µg/L3,3-Dimethyl-1-butanol 70-130 2.4 20.0
1011014-Bromofluorobenzene (S)70-130
97.697.0Dibromofluoromethane (S)70-130
99.499.61,2-Dichloroethane - d4 (S)70-130
99.2100Toluene-d8 (S)70-130
Page 12 of 13Date:01/10/2024 04:24 PM
Page 33 of 36
Quality Control Data
23-363-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V42095QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V42094
Associated Lab Samples: 92888
LRB-V42094 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/09/24 13:010.5000.180<0.180µg/LBenzene
01/09/24 13:0110.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
01/09/24 13:010.5000.220<0.220µg/LToluene
01/09/24 13:014-Bromofluorobenzene (S)103 70-130
01/09/24 13:01Dibromofluoromethane (S)94.8 70-130
01/09/24 13:011,2-Dichloroethane - d4 (S)97.8 70-130
01/09/24 13:01Toluene-d8 (S)104 70-130
LCS-V42094 LCSD-V42094Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.5 97.510120.120.0µg/LBenzene 70-130 3.0 20.0
19.0 95.011522.920.0µg/Ltert-Amyl Alcohol (TAA)40-140 18.6 20.0
19.4 97.010020.020.0µg/LToluene 70-130 3.0 20.0
1011004-Bromofluorobenzene (S)70-130
96.096.0Dibromofluoromethane (S)70-130
99.01001,2-Dichloroethane - d4 (S)70-130
104102Toluene-d8 (S)70-130
Page 13 of 13Date:01/10/2024 04:24 PM
Page 34 of 36
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-363-0017
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 1.1C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:12/29/2023 13:31:52
Special precautions or instructions included?
Comments:
Page 35 of 36
Page 36 of 36

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

12/12/2023
Geological Resources, Inc. Rae Brown
113 West Firetower Road, Suite G Winterville, NC, 28590
Ref: Analytical Testing
Lab Report Number: 23-335-0008 Client Project Description: Ganesha
GRI #4457
Dear Rae Brown:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 12/1/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 29
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Page 1 of 1 00016/23-335-0008
Page 2 of 29
Report Number:
Sample Summary Table
Client Project Description:
23-335-0008
Ganesha
GRI #4457
Lab No Client Sample ID Matrix Date Collected Date Received
11/30/2023 16:50Aqueous 90659 GMW-4 12/01/2023 11:10
11/30/2023 17:04Aqueous 90660 MW-21 12/01/2023 11:10
11/30/2023 16:05Aqueous 90661 Trip Blank 12/01/2023 11:10
Page 3 of 29
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-335-0008
Report Limit
Project:Ganesha
V 90659GMW-4
6570 12/06/2023 18:596200BBenzeneµg/L 18.0
127 12/06/2023 18:596200BChloroformµg/L 22.0
1420000 12/08/2023 08:146200BEthanolµg/L 42000
2000 12/06/2023 18:596200BEthylbenzeneµg/L 17.0
69.7 12/06/2023 18:596200BIsopropylbenzeneµg/L 18.0
J37112/06/2023 18:596200BMethyl Ethyl Ketone (MEK)µg/L 71.0
135 12/06/2023 18:596200BMethyl tert-butyl ether (MTBE)µg/L 14.0
449 12/06/2023 18:596200BNaphthaleneµg/L 47.0
192 12/06/2023 18:596200Bn-Propylbenzene µg/L 19.0
J33.3 12/06/2023 18:596200BStyreneµg/L 22.0
1230 12/06/2023 18:596200Btert-Butyl Alcohol (TBA)µg/L 160
9770 12/06/2023 18:596200Btert-Amyl Alcohol (TAA)µg/L 190
9790 12/08/2023 08:146200BTolueneµg/L 220
1600 12/06/2023 18:596200B1,2,4-Trimethylbenzene µg/L 19.0
382 12/06/2023 18:596200B1,3,5-Trimethylbenzene µg/L 18.0
3750 12/06/2023 18:596200Bo-Xylene µg/L 21.0
7620 12/06/2023 18:596200Bm,p-Xylene µg/L 42.0
11400 12/06/2023 18:596200BXylene (Total)µg/L 21.0
V 90660MW-21
26400 12/08/2023 06:586200BBenzeneµg/L 180
1400 12/06/2023 19:246200BDi-Isopropyl Ether (DIPE)µg/L 50.0
405 12/06/2023 19:246200B1,2-Dibromoethane µg/L 20.0
133 12/06/2023 19:246200B1,2-Dichloroethane µg/L 15.0
J1210012/06/2023 19:246200BEthanolµg/L 4200
3420 12/06/2023 19:246200BEthylbenzeneµg/L 17.0
J65.6 12/06/2023 19:246200B2-Hexanone µg/L 38.0
113 12/06/2023 19:246200BIsopropylbenzeneµg/L 18.0
248 12/06/2023 19:246200BMethyl tert-butyl ether (MTBE)µg/L 14.0
1130 12/06/2023 19:246200BNaphthaleneµg/L 47.0
279 12/06/2023 19:246200Bn-Propylbenzene µg/L 19.0
666 12/06/2023 19:246200BStyreneµg/L 22.0
J82012/06/2023 19:246200Btert-Butyl Alcohol (TBA)µg/L 160
E1176112/06/2023 19:246200Btert-Amyl Alcohol (TAA)µg/L 190
33800 12/08/2023 06:586200BTolueneµg/L 220
2140 12/06/2023 19:246200B1,2,4-Trimethylbenzene µg/L 19.0
505 12/06/2023 19:246200B1,3,5-Trimethylbenzene µg/L 18.0
Page 4 of 29
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-335-0008
Report Limit
Project:Ganesha
V 90660MW-21
5750 12/06/2023 19:246200Bo-Xylene µg/L 21.0
11100 12/06/2023 19:246200Bm,p-Xylene µg/L 42.0
16900 12/06/2023 19:246200BXylene (Total)µg/L 21.0
Page 5 of 29

Client: Geological Resources, Inc. CASE NARRATIVE
Project: Ganesha Lab Report Number: 23-335-0008
Date: 12/12/2023
Volatile Organic Compounds - GC/MS Method 6200B Analyte: Acetone QC Batch No: V40995/V40994
High LCS/LCSD recovery. CCV recovers within method parameters. Hits estimated high.

Page 6 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-335-0008
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/01/2023
Ganesha
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:GMW-4
90659 Matrix:
11/30/2023 16:50
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 12/06/23 18:59 6200BENM
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%12/06/23 18:59100 ENM V40995
Surrogate: Dibromofluoromethane 97.6 Limits: 70-130%12/06/23 18:59100 ENM V40995
Surrogate: 1,2-Dichloroethane - d4 92.0 Limits: 70-130%12/06/23 18:59100 ENM V40995
Surrogate: Toluene-d8 98.6 Limits: 70-130%12/06/23 18:59100 ENM V40995
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%12/08/23 08:141000 MSA V41035
Surrogate: Dibromofluoromethane 99.6 Limits: 70-130%12/08/23 08:141000 MSA V41035
Surrogate: 1,2-Dichloroethane - d4 94.2 Limits: 70-130%12/08/23 08:141000 MSA V41035
Surrogate: Toluene-d8 103 Limits: 70-130%12/08/23 08:141000 MSA V41035
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 7 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-335-0008
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/01/2023
Ganesha
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:GMW-4
90659 Matrix:
11/30/2023 16:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40994 12/06/23 09:00 V41034 12/07/23 09:00
<180 µg/L 180 1000Acetone 100 12/06/23 18:59 V40995ENM
6570 µg/L 18.0 50.0Benzene 100 12/06/23 18:59 V40995ENM
<21.0 µg/L 21.0 50.0Bromobenzene 100 12/06/23 18:59 V40995ENM
<42.0 µg/L 42.0 100Bromochloromethane 100 12/06/23 18:59 V40995ENM
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 12/06/23 18:59 V40995ENM
<150 µg/L 150 500Bromoform 100 12/06/23 18:59 V40995ENM
<28.0 µg/L 28.0 100Bromomethane 100 12/06/23 18:59 V40995ENM
<18.0 µg/L 18.0 50.0n-Butylbenzene 100 12/06/23 18:59 V40995ENM
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 12/06/23 18:59 V40995ENM
<92.0 µg/L 92.0 200tert-Butyl benzene 100 12/06/23 18:59 V40995ENM
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 12/06/23 18:59 V40995ENM
<19.0 µg/L 19.0 50.0Chlorobenzene 100 12/06/23 18:59 V40995ENM
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 12/06/23 18:59 V40995ENM
<43.0 µg/L 43.0 100Chloroethane 100 12/06/23 18:59 V40995ENM
127 µg/L 22.0 50.0Chloroform 100 12/06/23 18:59 V40995ENM
<22.0 µg/L 22.0 50.0Chloromethane 100 12/06/23 18:59 V40995ENM
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 12/06/23 18:59 V40995ENM
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 12/06/23 18:59 V40995ENM
<50.0 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 12/06/23 18:59 V40995ENM
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 12/06/23 18:59 V40995ENM
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 12/06/23 18:59 V40995ENM
<23.0 µg/L 23.0 50.0Dibromomethane 100 12/06/23 18:59 V40995ENM
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 8 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-335-0008
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/01/2023
Ganesha
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:GMW-4
90659 Matrix:
11/30/2023 16:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40994 12/06/23 09:00 V41034 12/07/23 09:00
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 12/06/23 18:59 V40995ENM
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 12/06/23 18:59 V40995ENM
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 12/06/23 18:59 V40995ENM
<120 µg/L 120 500Dichlorodifluoromethane 100 12/06/23 18:59 V40995ENM
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 12/06/23 18:59 V40995ENM
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 12/06/23 18:59 V40995ENM
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 12/06/23 18:59 V40995ENM
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 12/06/23 18:59 V40995ENM
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 12/06/23 18:59 V40995ENM
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 12/06/23 18:59 V40995ENM
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 12/06/23 18:59 V40995ENM
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 12/06/23 18:59 V40995ENM
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 12/06/23 18:59 V40995ENM
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 12/06/23 18:59 V40995ENM
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 12/06/23 18:59 V40995ENM
1420000 µg/L 42000 200000Ethanol 1000 12/08/23 08:14 V41035MSA
2000 µg/L 17.0 50.0Ethylbenzene 100 12/06/23 18:59 V40995ENM
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 12/06/23 18:59 V40995ENM
<38.0 µg/L 38.0 1002-Hexanone 100 12/06/23 18:59 V40995ENM
69.7 µg/L 18.0 50.0Isopropylbenzene 100 12/06/23 18:59 V40995ENM
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 12/06/23 18:59 V40995ENM
371 J µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 12/06/23 18:59 V40995ENM
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 9 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-335-0008
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/01/2023
Ganesha
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:GMW-4
90659 Matrix:
11/30/2023 16:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40994 12/06/23 09:00 V41034 12/07/23 09:00
135 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 12/06/23 18:59 V40995ENM
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 12/06/23 18:59 V40995ENM
<33.0 µg/L 33.0 200Methylene Chloride 100 12/06/23 18:59 V40995ENM
449 µg/L 47.0 100Naphthalene 100 12/06/23 18:59 V40995ENM
192 µg/L 19.0 50.0n-Propylbenzene 100 12/06/23 18:59 V40995ENM
33.3 J µg/L 22.0 50.0Styrene 100 12/06/23 18:59 V40995ENM
1230 µg/L 160 1000tert-Butyl Alcohol (TBA)100 12/06/23 18:59 V40995ENM
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 12/06/23 18:59 V40995ENM
9770 µg/L 190 1000tert-Amyl Alcohol (TAA)100 12/06/23 18:59 V40995ENM
<28.0 µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 12/06/23 18:59 V40995ENM
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 12/06/23 18:59 V40995ENM
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 12/06/23 18:59 V40995ENM
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 12/06/23 18:59 V40995ENM
9790 µg/L 220 500Toluene 1000 12/08/23 08:14 V41035MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 12/06/23 18:59 V40995ENM
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 12/06/23 18:59 V40995ENM
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 12/06/23 18:59 V40995ENM
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 12/06/23 18:59 V40995ENM
<18.0 µg/L 18.0 50.0Trichloroethene 100 12/06/23 18:59 V40995ENM
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 12/06/23 18:59 V40995ENM
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 12/06/23 18:59 V40995ENM
1600 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 12/06/23 18:59 V40995ENM
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 10 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-335-0008
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/01/2023
Ganesha
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:GMW-4
90659 Matrix:
11/30/2023 16:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40994 12/06/23 09:00 V41034 12/07/23 09:00
382 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 12/06/23 18:59 V40995ENM
<100 µg/L 100 500Vinyl Acetate 100 12/06/23 18:59 V40995ENM
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 12/06/23 18:59 V40995ENM
3750 µg/L 21.0 50.0o-Xylene 100 12/06/23 18:59 V40995ENM
7620 µg/L 42.0 100m,p-Xylene 100 12/06/23 18:59 V40995ENM
11400 µg/L 21.0 50.0Xylene (Total)100 12/06/23 18:59 V40995
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%12/06/23 18:59100 ENM V40995
Surrogate: Dibromofluoromethane 97.6 Limits: 70-130%12/06/23 18:59100 ENM V40995
Surrogate: 1,2-Dichloroethane - d4 92.0 Limits: 70-130%12/06/23 18:59100 ENM V40995
Surrogate: Toluene-d8 98.6 Limits: 70-130%12/06/23 18:59100 ENM V40995
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%12/08/23 08:141000 MSA V41035
Surrogate: Dibromofluoromethane 99.6 Limits: 70-130%12/08/23 08:141000 MSA V41035
Surrogate: 1,2-Dichloroethane - d4 94.2 Limits: 70-130%12/08/23 08:141000 MSA V41035
Surrogate: Toluene-d8 103 Limits: 70-130%12/08/23 08:141000 MSA V41035
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 11 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-335-0008
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/01/2023
Ganesha
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:MW-21
90660 Matrix:
11/30/2023 17:04
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 12/06/23 19:24 6200BENM
Surrogate: 4-Bromofluorobenzene 97.4 Limits: 70-130%12/06/23 19:24100 ENM V40995
Surrogate: Dibromofluoromethane 98.2 Limits: 70-130%12/06/23 19:24100 ENM V40995
Surrogate: 1,2-Dichloroethane - d4 93.6 Limits: 70-130%12/06/23 19:24100 ENM V40995
Surrogate: Toluene-d8 96.4 Limits: 70-130%12/06/23 19:24100 ENM V40995
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%12/08/23 06:581000 MSA V41035
Surrogate: Dibromofluoromethane 97.8 Limits: 70-130%12/08/23 06:581000 MSA V41035
Surrogate: 1,2-Dichloroethane - d4 94.2 Limits: 70-130%12/08/23 06:581000 MSA V41035
Surrogate: Toluene-d8 102 Limits: 70-130%12/08/23 06:581000 MSA V41035
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 12 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-335-0008
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/01/2023
Ganesha
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:MW-21
90660 Matrix:
11/30/2023 17:04
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40994 12/06/23 09:00 V41034 12/07/23 09:00
<180 µg/L 180 1000Acetone 100 12/06/23 19:24 V40995ENM
26400 µg/L 180 500Benzene 1000 12/08/23 06:58 V41035MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 12/06/23 19:24 V40995ENM
<42.0 µg/L 42.0 100Bromochloromethane 100 12/06/23 19:24 V40995ENM
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 12/06/23 19:24 V40995ENM
<150 µg/L 150 500Bromoform 100 12/06/23 19:24 V40995ENM
<28.0 µg/L 28.0 100Bromomethane 100 12/06/23 19:24 V40995ENM
<18.0 µg/L 18.0 50.0n-Butylbenzene 100 12/06/23 19:24 V40995ENM
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 12/06/23 19:24 V40995ENM
<92.0 µg/L 92.0 200tert-Butyl benzene 100 12/06/23 19:24 V40995ENM
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 12/06/23 19:24 V40995ENM
<19.0 µg/L 19.0 50.0Chlorobenzene 100 12/06/23 19:24 V40995ENM
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 12/06/23 19:24 V40995ENM
<43.0 µg/L 43.0 100Chloroethane 100 12/06/23 19:24 V40995ENM
<22.0 µg/L 22.0 50.0Chloroform 100 12/06/23 19:24 V40995ENM
<22.0 µg/L 22.0 50.0Chloromethane 100 12/06/23 19:24 V40995ENM
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 12/06/23 19:24 V40995ENM
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 12/06/23 19:24 V40995ENM
1400 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 12/06/23 19:24 V40995ENM
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 12/06/23 19:24 V40995ENM
405 µg/L 20.0 50.01,2-Dibromoethane 100 12/06/23 19:24 V40995ENM
<23.0 µg/L 23.0 50.0Dibromomethane 100 12/06/23 19:24 V40995ENM
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 13 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-335-0008
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/01/2023
Ganesha
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:MW-21
90660 Matrix:
11/30/2023 17:04
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40994 12/06/23 09:00 V41034 12/07/23 09:00
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 12/06/23 19:24 V40995ENM
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 12/06/23 19:24 V40995ENM
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 12/06/23 19:24 V40995ENM
<120 µg/L 120 500Dichlorodifluoromethane 100 12/06/23 19:24 V40995ENM
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 12/06/23 19:24 V40995ENM
133 µg/L 15.0 50.01,2-Dichloroethane 100 12/06/23 19:24 V40995ENM
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 12/06/23 19:24 V40995ENM
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 12/06/23 19:24 V40995ENM
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 12/06/23 19:24 V40995ENM
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 12/06/23 19:24 V40995ENM
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 12/06/23 19:24 V40995ENM
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 12/06/23 19:24 V40995ENM
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 12/06/23 19:24 V40995ENM
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 12/06/23 19:24 V40995ENM
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 12/06/23 19:24 V40995ENM
12100 J µg/L 4200 20000Ethanol 100 12/06/23 19:24 V40995ENM
3420 µg/L 17.0 50.0Ethylbenzene 100 12/06/23 19:24 V40995ENM
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 12/06/23 19:24 V40995ENM
65.6 J µg/L 38.0 1002-Hexanone 100 12/06/23 19:24 V40995ENM
113 µg/L 18.0 50.0Isopropylbenzene 100 12/06/23 19:24 V40995ENM
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 12/06/23 19:24 V40995ENM
<71.0 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 12/06/23 19:24 V40995ENM
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 14 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-335-0008
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/01/2023
Ganesha
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:MW-21
90660 Matrix:
11/30/2023 17:04
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40994 12/06/23 09:00 V41034 12/07/23 09:00
248 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 12/06/23 19:24 V40995ENM
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 12/06/23 19:24 V40995ENM
<33.0 µg/L 33.0 200Methylene Chloride 100 12/06/23 19:24 V40995ENM
1130 µg/L 47.0 100Naphthalene 100 12/06/23 19:24 V40995ENM
279 µg/L 19.0 50.0n-Propylbenzene 100 12/06/23 19:24 V40995ENM
666 µg/L 22.0 50.0Styrene 100 12/06/23 19:24 V40995ENM
820 J µg/L 160 1000tert-Butyl Alcohol (TBA)100 12/06/23 19:24 V40995ENM
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 12/06/23 19:24 V40995ENM
11761 E µg/L 190 1000tert-Amyl Alcohol (TAA)100 12/06/23 19:24 V40995ENM
<28.0 µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 12/06/23 19:24 V40995ENM
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 12/06/23 19:24 V40995ENM
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 12/06/23 19:24 V40995ENM
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 12/06/23 19:24 V40995ENM
33800 µg/L 220 500Toluene 1000 12/08/23 06:58 V41035MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 12/06/23 19:24 V40995ENM
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 12/06/23 19:24 V40995ENM
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 12/06/23 19:24 V40995ENM
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 12/06/23 19:24 V40995ENM
<18.0 µg/L 18.0 50.0Trichloroethene 100 12/06/23 19:24 V40995ENM
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 12/06/23 19:24 V40995ENM
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 12/06/23 19:24 V40995ENM
2140 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 12/06/23 19:24 V40995ENM
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 15 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-335-0008
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/01/2023
Ganesha
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:MW-21
90660 Matrix:
11/30/2023 17:04
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40994 12/06/23 09:00 V41034 12/07/23 09:00
505 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 12/06/23 19:24 V40995ENM
<100 µg/L 100 500Vinyl Acetate 100 12/06/23 19:24 V40995ENM
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 12/06/23 19:24 V40995ENM
5750 µg/L 21.0 50.0o-Xylene 100 12/06/23 19:24 V40995ENM
11100 µg/L 42.0 100m,p-Xylene 100 12/06/23 19:24 V40995ENM
16900 µg/L 21.0 50.0Xylene (Total)100 12/06/23 19:24 V40995KCC
Surrogate: 4-Bromofluorobenzene 97.4 Limits: 70-130%12/06/23 19:24100 ENM V40995
Surrogate: Dibromofluoromethane 98.2 Limits: 70-130%12/06/23 19:24100 ENM V40995
Surrogate: 1,2-Dichloroethane - d4 93.6 Limits: 70-130%12/06/23 19:24100 ENM V40995
Surrogate: Toluene-d8 96.4 Limits: 70-130%12/06/23 19:24100 ENM V40995
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%12/08/23 06:581000 MSA V41035
Surrogate: Dibromofluoromethane 97.8 Limits: 70-130%12/08/23 06:581000 MSA V41035
Surrogate: 1,2-Dichloroethane - d4 94.2 Limits: 70-130%12/08/23 06:581000 MSA V41035
Surrogate: Toluene-d8 102 Limits: 70-130%12/08/23 06:581000 MSA V41035
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 16 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-335-0008
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/01/2023
Ganesha
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:Trip Blank
90661 Matrix:
11/30/2023 16:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40994 12/06/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 12/06/23 11:09 V40995ENM
<0.180 µg/L 0.180 0.500Benzene 1 12/06/23 11:09 V40995ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 12/06/23 11:09 V40995ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 12/06/23 11:09 V40995ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 12/06/23 11:09 V40995ENM
<1.50 µg/L 1.50 5.00Bromoform 1 12/06/23 11:09 V40995ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 12/06/23 11:09 V40995ENM
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 12/06/23 11:09 V40995ENM
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 12/06/23 11:09 V40995ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 12/06/23 11:09 V40995ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 12/06/23 11:09 V40995ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 12/06/23 11:09 V40995ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 12/06/23 11:09 V40995ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 12/06/23 11:09 V40995ENM
<0.220 µg/L 0.220 0.500Chloroform 1 12/06/23 11:09 V40995ENM
<0.220 µg/L 0.220 0.500Chloromethane 1 12/06/23 11:09 V40995ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 12/06/23 11:09 V40995ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 12/06/23 11:09 V40995ENM
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 12/06/23 11:09 V40995ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 12/06/23 11:09 V40995ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 12/06/23 11:09 V40995ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 12/06/23 11:09 V40995ENM
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 17 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-335-0008
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/01/2023
Ganesha
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:Trip Blank
90661 Matrix:
11/30/2023 16:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40994 12/06/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 12/06/23 11:09 V40995ENM
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 12/06/23 11:09 V40995ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 12/06/23 11:09 V40995ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 12/06/23 11:09 V40995ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 12/06/23 11:09 V40995ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 12/06/23 11:09 V40995ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 12/06/23 11:09 V40995ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 12/06/23 11:09 V40995ENM
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 12/06/23 11:09 V40995ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 12/06/23 11:09 V40995ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 12/06/23 11:09 V40995ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 12/06/23 11:09 V40995ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 12/06/23 11:09 V40995ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 12/06/23 11:09 V40995ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 12/06/23 11:09 V40995ENM
<42.0 µg/L 42.0 200Ethanol 1 12/06/23 11:09 V40995ENM
<0.170 µg/L 0.170 0.500Ethylbenzene 1 12/06/23 11:09 V40995ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 12/06/23 11:09 V40995ENM
<0.380 µg/L 0.380 1.002-Hexanone 1 12/06/23 11:09 V40995ENM
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 12/06/23 11:09 V40995ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 12/06/23 11:09 V40995ENM
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 12/06/23 11:09 V40995ENM
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 18 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-335-0008
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/01/2023
Ganesha
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:Trip Blank
90661 Matrix:
11/30/2023 16:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40994 12/06/23 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 12/06/23 11:09 V40995ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 12/06/23 11:09 V40995ENM
<0.330 µg/L 0.330 2.00Methylene Chloride 1 12/06/23 11:09 V40995ENM
<0.470 µg/L 0.470 1.00Naphthalene 1 12/06/23 11:09 V40995ENM
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 12/06/23 11:09 V40995ENM
<0.220 µg/L 0.220 0.500Styrene 1 12/06/23 11:09 V40995ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 12/06/23 11:09 V40995ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 12/06/23 11:09 V40995ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 12/06/23 11:09 V40995ENM
<0.220 µg/L 0.220 0.500Toluene 1 12/06/23 11:09 V40995ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 12/06/23 11:09 V40995ENM
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 12/06/23 11:09 V40995ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 12/06/23 11:09 V40995ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 12/06/23 11:09 V40995ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 12/06/23 11:09 V40995ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 12/06/23 11:09 V40995ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 12/06/23 11:09 V40995ENM
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 12/06/23 11:09 V40995ENM
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 12/06/23 11:09 V40995ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 12/06/23 11:09 V40995ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 12/06/23 11:09 V40995ENM
<0.210 µg/L 0.210 0.500o-Xylene 1 12/06/23 11:09 V40995ENM
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 19 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-335-0008
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 12/01/2023
Ganesha
Report Date : 12/12/2023
Sample ID :
Lab No :
Sampled:Trip Blank
90661 Matrix:
11/30/2023 16:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40994 12/06/23 09:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 12/06/23 11:09 V40995ENM
<0.21 µg/L 0.210 0.500Xylene (Total)1 12/06/23 11:09 V40995
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%12/06/23 11:091 ENM V40995
Surrogate: Dibromofluoromethane 101 Limits: 70-130%12/06/23 11:091 ENM V40995
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 70-130%12/06/23 11:091 ENM V40995
Surrogate: Toluene-d8 98.6 Limits: 70-130%12/06/23 11:091 ENM V40995
Qualifiers/
Definitions
Result above calibration rangeEDilution FactorDF
Method Quantitation LimitMQLEstimated valueJ
Page 20 of 29
Quality Control Data
23-335-0008Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V40995QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V40994
Associated Lab Samples: 90659, 90660, 90661
LRB-V40994 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/06/23 10:4410.01.80<1.80µg/LAcetone
12/06/23 10:440.5000.180<0.180µg/LBenzene
12/06/23 10:440.5000.210<0.210µg/LBromobenzene
12/06/23 10:441.000.420<0.420µg/LBromochloromethane
12/06/23 10:440.5000.160<0.160µg/LBromodichloromethane
12/06/23 10:445.001.50<1.50µg/LBromoform
12/06/23 10:441.000.280<0.280µg/LBromomethane
12/06/23 10:440.5000.180<0.180µg/Ln-Butylbenzene
12/06/23 10:440.5000.200<0.200µg/Lsec-Butyl benzene
12/06/23 10:442.000.920<0.920µg/Ltert-Butyl benzene
12/06/23 10:440.5000.180<0.180µg/LCarbon Tetrachloride
12/06/23 10:440.5000.190<0.190µg/LChlorobenzene
12/06/23 10:440.5000.190<0.190µg/LChlorodibromomethane
12/06/23 10:441.000.430<0.430µg/LChloroethane
12/06/23 10:440.5000.220<0.220µg/LChloroform
12/06/23 10:440.5000.220<0.220µg/LChloromethane
12/06/23 10:440.5000.200<0.200µg/L2-Chlorotoluene
12/06/23 10:440.5000.200<0.200µg/L4-Chlorotoluene
12/06/23 10:440.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
12/06/23 10:442.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
12/06/23 10:440.5000.200<0.200µg/L1,2-Dibromoethane
12/06/23 10:440.5000.230<0.230µg/LDibromomethane
12/06/23 10:440.5000.220<0.220µg/L1,2-Dichlorobenzene
12/06/23 10:440.5000.190<0.190µg/L1,3-Dichlorobenzene
12/06/23 10:440.5000.210<0.210µg/L1,4-Dichlorobenzene
12/06/23 10:445.001.20<1.20µg/LDichlorodifluoromethane
12/06/23 10:440.5000.240<0.240µg/L1,1-Dichloroethane
Page 1 of 7Date:12/08/2023 05:51 PM
Page 21 of 29
Quality Control Data
23-335-0008Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V40995QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V40994
Associated Lab Samples: 90659, 90660, 90661
LRB-V40994 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/06/23 10:440.5000.150<0.150µg/L1,2-Dichloroethane
12/06/23 10:440.5000.150<0.150µg/L1,1-Dichloroethene
12/06/23 10:440.5000.200<0.200µg/Lcis-1,2-Dichloroethene
12/06/23 10:440.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
12/06/23 10:440.5000.190<0.190µg/L1,2-Dichloropropane
12/06/23 10:440.5000.130<0.130µg/L1,3-Dichloropropane
12/06/23 10:442.000.210<0.210µg/L2,2-Dichloropropane
12/06/23 10:440.5000.200<0.200µg/L1,1-Dichloropropene
12/06/23 10:440.5000.210<0.210µg/Lcis-1,3-Dichloropropene
12/06/23 10:440.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
12/06/23 10:4420042.0<42.0µg/LEthanol
12/06/23 10:440.5000.170<0.170µg/LEthylbenzene
12/06/23 10:443.000.350<0.350µg/LHexachlorobutadiene
12/06/23 10:441.000.380<0.380µg/L2-Hexanone
12/06/23 10:440.5000.180<0.180µg/LIsopropylbenzene
12/06/23 10:440.5000.089<0.089µg/L4-Isopropyl toluene
12/06/23 10:445.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
12/06/23 10:441.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
12/06/23 10:441.000.078<0.078µg/L4-Methyl-2-Pentanone
12/06/23 10:442.000.330<0.330µg/LMethylene Chloride
12/06/23 10:441.000.470<0.470µg/LNaphthalene
12/06/23 10:440.5000.190<0.190µg/Ln-Propylbenzene
12/06/23 10:440.5000.220<0.220µg/LStyrene
12/06/23 10:4410.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
12/06/23 10:4410.00.350<0.350µg/Ltert-Butyl formate (TBF)
12/06/23 10:4410.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
12/06/23 10:4410.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 2 of 7Date:12/08/2023 05:51 PM
Page 22 of 29
Quality Control Data
23-335-0008Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V40995QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V40994
Associated Lab Samples: 90659, 90660, 90661
LRB-V40994 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/06/23 10:440.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
12/06/23 10:440.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
12/06/23 10:440.5000.220<0.220µg/LTetrachloroethene
12/06/23 10:440.5000.220<0.220µg/LToluene
12/06/23 10:440.5000.380<0.380µg/L1,2,3-Trichlorobenzene
12/06/23 10:440.5000.310<0.310µg/L1,2,4-Trichlorobenzene
12/06/23 10:440.5000.160<0.160µg/L1,1,1-Trichloroethane
12/06/23 10:440.5000.096<0.096µg/L1,1,2-Trichloroethane
12/06/23 10:440.5000.180<0.180µg/LTrichloroethene
12/06/23 10:440.5000.180<0.180µg/LTrichlorofluoromethane
12/06/23 10:440.5000.270<0.270µg/L1,2,3-Trichloropropane
12/06/23 10:440.5000.190<0.190µg/L1,2,4-Trimethylbenzene
12/06/23 10:440.5000.180<0.180µg/L1,3,5-Trimethylbenzene
12/06/23 10:445.001.00<1.00µg/LVinyl Acetate
12/06/23 10:440.5000.170<0.170µg/LVinyl Chloride
12/06/23 10:440.5000.210<0.210µg/Lo-Xylene
12/06/23 10:441.000.420<0.420µg/Lm,p-Xylene
12/06/23 10:4410.01.00<1.00µg/L3,3-Dimethyl-1-butanol
12/06/23 10:444-Bromofluorobenzene (S)100 70-130
12/06/23 10:44Dibromofluoromethane (S)98.2 70-130
12/06/23 10:441,2-Dichloroethane - d4 (S)96.2 70-130
12/06/23 10:44Toluene-d8 (S)99.4 70-130
Page 3 of 7Date:12/08/2023 05:51 PM
Page 23 of 29
Quality Control Data
23-335-0008Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V40995QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V40994
LCS-V40994 LCSD-V40994Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
72.4 181*178*71.340.0µg/LAcetone 40-160 1.5 20.0
21.4 10710921.820.0µg/LBenzene 70-130 1.8 20.0
21.1 10610621.220.0µg/LBromobenzene 70-130 0.4 20.0
22.3 11211222.420.0µg/LBromochloromethane 70-130 0.4 20.0
22.0 11011022.020.0µg/LBromodichloromethane 70-130 0.0 20.0
21.0 10510520.920.0µg/LBromoform 70-130 0.4 20.0
20.8 10498.019.620.0µg/LBromomethane 60-140 5.9 20.0
20.6 10310821.620.0µg/Ln-Butylbenzene 70-130 4.7 20.0
20.9 10510721.420.0µg/Lsec-Butyl benzene 70-130 2.3 20.0
21.2 10610721.320.0µg/Ltert-Butyl benzene 70-130 0.4 20.0
21.7 10911222.420.0µg/LCarbon Tetrachloride 70-130 3.1 20.0
21.6 10810821.620.0µg/LChlorobenzene 70-130 0.0 20.0
22.6 11311222.420.0µg/LChlorodibromomethane 70-130 0.8 20.0
25.5 12813526.920.0µg/LChloroethane 60-140 5.3 20.0
21.7 10911122.220.0µg/LChloroform 70-130 2.2 20.0
23.8 11911823.620.0µg/LChloromethane 60-140 0.8 20.0
20.9 10510621.220.0µg/L2-Chlorotoluene 70-130 1.4 20.0
20.8 10410921.820.0µg/L4-Chlorotoluene 70-130 4.6 20.0
22.7 11411322.520.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.8 20.0
23.1 11611723.420.0µg/L1,2-Dibromo-3-Chloropropane 70-130 1.2 20.0
22.0 11010721.420.0µg/L1,2-Dibromoethane 70-130 2.7 20.0
21.8 10911222.320.0µg/LDibromomethane 70-130 2.2 20.0
21.7 10910821.520.0µg/L1,2-Dichlorobenzene 70-130 0.9 20.0
21.3 10711021.920.0µg/L1,3-Dichlorobenzene 70-130 2.7 20.0
21.3 10710921.820.0µg/L1,4-Dichlorobenzene 70-130 2.3 20.0
15.2 76.080.016.020.0µg/LDichlorodifluoromethane 60-140 5.1 20.0
Page 4 of 7* QC Fail Date:12/08/2023 05:51 PM
Page 24 of 29
Quality Control Data
23-335-0008Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V40995QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V40994
LCS-V40994 LCSD-V40994Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
22.6 11311422.820.0µg/L1,1-Dichloroethane 70-130 0.8 20.0
21.8 10911322.520.0µg/L1,2-Dichloroethane 70-130 3.1 20.0
22.3 11211222.320.0µg/L1,1-Dichloroethene 70-130 0.0 20.0
21.6 10810821.620.0µg/Lcis-1,2-Dichloroethene 70-130 0.0 20.0
21.1 10611222.320.0µg/Ltrans-1,2-Dichloroethene 70-130 5.5 20.0
22.2 11111222.320.0µg/L1,2-Dichloropropane 70-130 0.4 20.0
21.3 10710621.220.0µg/L1,3-Dichloropropane 70-130 0.4 20.0
22.5 11311422.820.0µg/L2,2-Dichloropropane 70-130 1.3 20.0
21.8 10911322.520.0µg/L1,1-Dichloropropene 70-130 3.1 20.0
21.8 10910721.420.0µg/Lcis-1,3-Dichloropropene 70-130 1.8 20.0
21.8 10911122.220.0µg/Ltrans-1,3-Dichloropropene 70-130 1.8 20.0
630 126113566500µg/LEthanol 60-140 10.7 20.0
20.6 10310621.220.0µg/LEthylbenzene 70-130 2.8 20.0
20.8 10410621.120.0µg/LHexachlorobutadiene 70-130 1.4 20.0
25.7 12913026.020.0µg/L2-Hexanone 60-140 1.1 20.0
20.9 10510921.720.0µg/LIsopropylbenzene 70-130 3.7 20.0
20.5 10310621.120.0µg/L4-Isopropyl toluene 70-130 2.8 20.0
27.0 13513727.420.0µg/LMethyl Ethyl Ketone (MEK)60-140 1.4 20.0
21.5 10810721.320.0µg/LMethyl tert-butyl ether (MTBE)70-130 0.9 20.0
23.4 11711723.420.0µg/L4-Methyl-2-Pentanone 60-140 0.0 20.0
20.3 10210220.320.0µg/LMethylene Chloride 70-130 0.0 20.0
24.2 12111523.020.0µg/LNaphthalene 70-130 5.0 20.0
21.0 10510821.620.0µg/Ln-Propylbenzene 70-130 2.8 20.0
21.8 10910921.820.0µg/LStyrene 70-130 0.0 20.0
44.4 11111545.940.0µg/Ltert-Butyl Alcohol (TBA)40-140 3.3 20.0
47.2 11811646.440.0µg/Ltert-Butyl formate (TBF)40-140 1.7 20.0
Page 5 of 7Date:12/08/2023 05:51 PM
Page 25 of 29
Quality Control Data
23-335-0008Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V40995QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V40994
LCS-V40994 LCSD-V40994Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.7 10911523.020.0µg/Ltert-Amyl Alcohol (TAA)40-140 5.8 20.0
47.5 11911947.740.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 0.4 20.0
21.8 10910821.620.0µg/L1,1,1,2-Tetrachloroethane 70-130 0.9 20.0
20.9 10510721.420.0µg/L1,1,2,2-Tetrachloroethane 70-130 2.3 20.0
21.3 10711022.020.0µg/LTetrachloroethene 70-130 3.2 20.0
21.4 10711122.220.0µg/LToluene 70-130 3.6 20.0
25.9 13012024.020.0µg/L1,2,3-Trichlorobenzene 70-130 7.6 20.0
22.4 11211021.920.0µg/L1,2,4-Trichlorobenzene 70-130 2.2 20.0
21.7 10911222.320.0µg/L1,1,1-Trichloroethane 70-130 2.7 20.0
21.8 10911022.020.0µg/L1,1,2-Trichloroethane 70-130 0.9 20.0
22.4 11211523.020.0µg/LTrichloroethene 70-130 2.6 20.0
23.3 11712424.820.0µg/LTrichlorofluoromethane 60-140 6.2 20.0
20.0 10010220.320.0µg/L1,2,3-Trichloropropane 70-130 1.4 20.0
20.8 10410821.620.0µg/L1,2,4-Trimethylbenzene 70-130 3.7 20.0
20.5 10310621.220.0µg/L1,3,5-Trimethylbenzene 70-130 3.3 20.0
23.2 11612224.420.0µg/LVinyl Acetate 60-140 5.0 20.0
23.2 11612324.620.0µg/LVinyl Chloride 60-140 5.8 20.0
21.6 10811022.020.0µg/Lo-Xylene 70-130 1.8 20.0
44.1 11011345.240.0µg/Lm,p-Xylene 70-130 2.4 20.0
18.6 93.085.517.120.0µg/L3,3-Dimethyl-1-butanol 70-130 8.4 20.0
98.699.04-Bromofluorobenzene (S)70-130
10099.2Dibromofluoromethane (S)70-130
1021011,2-Dichloroethane - d4 (S)70-130
99.498.6Toluene-d8 (S)70-130
Page 6 of 7Date:12/08/2023 05:51 PM
Page 26 of 29
Quality Control Data
23-335-0008Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V41035QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V41034
Associated Lab Samples: 90659, 90660
LRB-V41034 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/08/23 00:100.5000.180<0.180µg/LBenzene
12/08/23 00:1020042.0<42.0µg/LEthanol
12/08/23 00:1010.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
12/08/23 00:100.5000.220<0.220µg/LToluene
12/08/23 00:104-Bromofluorobenzene (S)105 70-130
12/08/23 00:10Dibromofluoromethane (S)97.8 70-130
12/08/23 00:101,2-Dichloroethane - d4 (S)93.6 70-130
12/08/23 00:10Toluene-d8 (S)100 70-130
LCS-V41034 LCSD-V41034Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.5 10310320.520.0µg/LBenzene 70-130 0.0 20.0
525 105103514500µg/LEthanol 60-140 2.1 20.0
13.6 68.072.014.420.0µg/Ltert-Amyl Alcohol (TAA)40-140 5.7 20.0
19.4 97.010220.420.0µg/LToluene 70-130 5.0 20.0
99.097.24-Bromofluorobenzene (S)70-130
100100Dibromofluoromethane (S)70-130
98.498.61,2-Dichloroethane - d4 (S)70-130
103103Toluene-d8 (S)70-130
Page 7 of 7Date:12/08/2023 05:51 PM
Page 27 of 29
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-335-0008
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 2.6C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:12/01/2023 13:33:55
Special precautions or instructions included?
Comments:
Page 28 of 29
Page 29 of 29

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

2/13/2024
Geological Resources, Inc. Rae Brown
113 West Firetower Road, Suite G Winterville, NC, 28590
Ref: Analytical Testing
Lab Report Number: 24-030-0017 Client Project Description: Ganesha
GRI #4457
Dear Rae Brown:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 1/30/2024 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 73
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2024402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Page 1 of 1 00016/24-030-0017
Page 2 of 73
Report Number:
Sample Summary Table
Client Project Description:
24-030-0017
Ganesha
GRI #4457
Lab No Client Sample ID Matrix Date Collected Date Received
01/30/2024 10:26Aqueous 95552 GMW-1 01/30/2024 14:04
01/30/2024 10:11Aqueous 95553 GMW-2 01/30/2024 14:04
01/30/2024 09:29Aqueous 95554 GMW-3 01/30/2024 14:04
01/30/2024 09:59Aqueous 95555 GMW-4 01/30/2024 14:04
01/30/2024 10:42Aqueous 95556 MMPE-2 01/30/2024 14:04
01/30/2024 10:58Aqueous 95557 MMPE-3 01/30/2024 14:04
01/30/2024 11:52Aqueous 95558 MW-6 01/30/2024 14:04
01/30/2024 11:32Aqueous 95559 MW-18 01/30/2024 14:04
01/30/2024 12:07Aqueous 95560 MW-21 01/30/2024 14:04
01/30/2024 08:25Aqueous 95561 Trip Blank 01/30/2024 14:04
Page 3 of 73
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
24-030-0017
Report Limit
Project:Ganesha
V 95552GMW-1
3200 02/08/2024 05:306200BBenzeneµg/L 18.0
J26.0 02/08/2024 05:306200Bn-Butylbenzene µg/L 18.0
90.0 02/08/2024 05:306200BDi-Isopropyl Ether (DIPE)µg/L 50.0
2060 02/08/2024 05:306200BEthylbenzeneµg/L 17.0
J53.1 02/08/2024 05:306200B2-Hexanone µg/L 38.0
97.3 02/08/2024 05:306200BIsopropylbenzeneµg/L 18.0
J19302/08/2024 05:306200BMethyl Ethyl Ketone (MEK)µg/L 71.0
J88.5 02/08/2024 05:306200BMethyl tert-butyl ether (MTBE)µg/L 14.0
J30.2 02/08/2024 05:306200B4-Methyl-2-Pentanone µg/L 7.80
1130 02/08/2024 05:306200BNaphthaleneµg/L 47.0
250 02/08/2024 05:306200Bn-Propylbenzene µg/L 19.0
439 02/08/2024 05:306200BStyreneµg/L 22.0
1060 02/08/2024 05:306200Btert-Butyl Alcohol (TBA)µg/L 160
2870 02/08/2024 05:306200Btert-Amyl Alcohol (TAA)µg/L 190
13700 02/08/2024 21:136200BTolueneµg/L 220
2150 02/08/2024 05:306200B1,2,4-Trimethylbenzene µg/L 19.0
498 02/08/2024 05:306200B1,3,5-Trimethylbenzene µg/L 18.0
3860 02/08/2024 05:306200Bo-Xylene µg/L 21.0
7460 02/08/2024 05:306200Bm,p-Xylene µg/L 42.0
11300 02/08/2024 05:306200BXylene (Total)µg/L 21.0
V 95553GMW-2
941 02/08/2024 05:556200BBenzeneµg/L 18.0
J43.5 02/08/2024 05:556200Bn-Butylbenzene µg/L 18.0
1520 02/08/2024 05:556200BEthylbenzeneµg/L 17.0
J87.8 02/08/2024 05:556200B2-Hexanone µg/L 38.0
90.2 02/08/2024 05:556200BIsopropylbenzeneµg/L 18.0
J15802/08/2024 05:556200BMethyl Ethyl Ketone (MEK)µg/L 71.0
J45.6 02/08/2024 05:556200B4-Methyl-2-Pentanone µg/L 7.80
601 02/08/2024 05:556200BNaphthaleneµg/L 47.0
255 02/08/2024 05:556200Bn-Propylbenzene µg/L 19.0
158 02/08/2024 05:556200BStyreneµg/L 22.0
1100 02/08/2024 05:556200Btert-Butyl Alcohol (TBA)µg/L 160
2160 02/08/2024 05:556200Btert-Amyl Alcohol (TAA)µg/L 190
4030 02/08/2024 05:556200BTolueneµg/L 22.0
1850 02/08/2024 05:556200B1,2,4-Trimethylbenzene µg/L 19.0
557 02/08/2024 05:556200B1,3,5-Trimethylbenzene µg/L 18.0
Page 4 of 73
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
24-030-0017
Report Limit
Project:Ganesha
V 95553GMW-2
2540 02/08/2024 05:556200Bo-Xylene µg/L 21.0
5420 02/08/2024 05:556200Bm,p-Xylene µg/L 42.0
7960 02/08/2024 05:556200BXylene (Total)µg/L 21.0
V 95554GMW-3
1430 02/08/2024 06:196200BBenzeneµg/L 18.0
J35.0 02/08/2024 06:196200Bn-Butylbenzene µg/L 18.0
J20.4 02/08/2024 06:196200Bsec-Butyl benzene µg/L 20.0
1940 02/08/2024 06:196200BEthylbenzeneµg/L 17.0
105 02/08/2024 06:196200BIsopropylbenzeneµg/L 18.0
J24002/08/2024 06:196200BMethyl Ethyl Ketone (MEK)µg/L 71.0
J39.3 02/08/2024 06:196200BMethyl tert-butyl ether (MTBE)µg/L 14.0
J44.5 02/08/2024 06:196200B4-Methyl-2-Pentanone µg/L 7.80
720 02/08/2024 06:196200BNaphthaleneµg/L 47.0
301 02/08/2024 06:196200Bn-Propylbenzene µg/L 19.0
113 02/08/2024 06:196200BStyreneµg/L 22.0
1180 02/08/2024 06:196200Btert-Butyl Alcohol (TBA)µg/L 160
5610 02/08/2024 06:196200Btert-Amyl Alcohol (TAA)µg/L 190
8280 02/08/2024 06:196200BTolueneµg/L 22.0
2690 02/08/2024 06:196200B1,2,4-Trimethylbenzene µg/L 19.0
691 02/08/2024 06:196200B1,3,5-Trimethylbenzene µg/L 18.0
4630 02/08/2024 06:196200Bo-Xylene µg/L 21.0
8670 02/08/2024 06:196200Bm,p-Xylene µg/L 42.0
13300 02/08/2024 06:196200BXylene (Total)µg/L 21.0
V 95555GMW-4
4100 02/08/2024 06:446200BBenzeneµg/L 18.0
117 02/08/2024 06:446200BChloroformµg/L 22.0
843000 02/09/2024 18:316200BEthanolµg/L 42000
1220 02/08/2024 06:446200BEthylbenzeneµg/L 17.0
J37.4 02/08/2024 06:446200BIsopropylbenzeneµg/L 18.0
J22502/08/2024 06:446200BMethyl Ethyl Ketone (MEK)µg/L 71.0
J81.1 02/08/2024 06:446200BMethyl tert-butyl ether (MTBE)µg/L 14.0
J22.0 02/08/2024 06:446200B4-Methyl-2-Pentanone µg/L 7.80
266 02/08/2024 06:446200BNaphthaleneµg/L 47.0
101 02/08/2024 06:446200Bn-Propylbenzene µg/L 19.0
J22.7 02/08/2024 06:446200BStyreneµg/L 22.0
1270 02/08/2024 06:446200Btert-Butyl Alcohol (TBA)µg/L 160
Page 5 of 73
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
24-030-0017
Report Limit
Project:Ganesha
V 95555GMW-4
7100 02/08/2024 06:446200Btert-Amyl Alcohol (TAA)µg/L 190
8460 02/08/2024 06:446200BTolueneµg/L 22.0
813 02/08/2024 06:446200B1,2,4-Trimethylbenzene µg/L 19.0
188 02/08/2024 06:446200B1,3,5-Trimethylbenzene µg/L 18.0
2320 02/08/2024 06:446200Bo-Xylene µg/L 21.0
4700 02/08/2024 06:446200Bm,p-Xylene µg/L 42.0
7020 02/08/2024 06:446200BXylene (Total)µg/L 21.0
V 95556MMPE-2
81.4 02/08/2024 02:386200BBenzeneµg/L 0.180
1.20 02/08/2024 02:386200BChloroformµg/L 0.220
2.16 02/08/2024 02:386200BChloromethaneµg/L 0.220
1.14 02/08/2024 02:386200BDi-Isopropyl Ether (DIPE)µg/L 0.500
10.6 02/08/2024 02:386200BEthylbenzeneµg/L 0.170
J0.317 02/08/2024 02:386200BIsopropylbenzeneµg/L 0.180
J2.30 02/08/2024 02:386200BMethyl Ethyl Ketone (MEK)µg/L 0.710
2.33 02/08/2024 02:386200BMethyl tert-butyl ether (MTBE)µg/L 0.140
4.24 02/08/2024 02:386200BNaphthaleneµg/L 0.470
0.669 02/08/2024 02:386200Bn-Propylbenzene µg/L 0.190
0.964 02/08/2024 02:386200BStyreneµg/L 0.220
33.5 02/08/2024 02:386200Btert-Butyl Alcohol (TBA)µg/L 1.60
622 02/08/2024 16:186200Btert-Amyl Alcohol (TAA)µg/L 19.0
46.7 02/08/2024 02:386200BTolueneµg/L 0.220
16.0 02/08/2024 02:386200B1,2,4-Trimethylbenzene µg/L 0.190
4.90 02/08/2024 02:386200B1,3,5-Trimethylbenzene µg/L 0.180
60.2 02/08/2024 02:386200Bo-Xylene µg/L 0.210
96.2 02/08/2024 02:386200Bm,p-Xylene µg/L 0.420
156 02/08/2024 02:386200BXylene (Total)µg/L 0.210
V 95557MMPE-3
J0.222 02/08/2024 15:056200BEthylbenzeneµg/L 0.170
J0.846 02/08/2024 15:056200BMethyl Ethyl Ketone (MEK)µg/L 0.710
J0.399 02/08/2024 15:056200BTolueneµg/L 0.220
0.600 02/08/2024 15:056200B1,2,4-Trimethylbenzene µg/L 0.190
J0.201 02/08/2024 15:056200B1,3,5-Trimethylbenzene µg/L 0.180
0.522 02/08/2024 15:056200Bo-Xylene µg/L 0.210
J0.902 02/08/2024 15:056200Bm,p-Xylene µg/L 0.420
Page 6 of 73
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
24-030-0017
Report Limit
Project:Ganesha
V 95557MMPE-3
J1.42 02/08/2024 15:056200BXylene (Total)µg/L 0.210
V 95558MW-6
J0.755 02/08/2024 03:276200BMethyl Ethyl Ketone (MEK)µg/L 0.710
J0.536 02/08/2024 03:276200BNaphthaleneµg/L 0.470
10.5 02/08/2024 03:276200Btert-Butyl Alcohol (TBA)µg/L 1.60
J0.493 02/08/2024 03:276200B1,2,4-Trimethylbenzene µg/L 0.190
V 95559MW-18
3170 02/08/2024 17:576200BBenzeneµg/L 18.0
229 02/08/2024 17:576200BDi-Isopropyl Ether (DIPE)µg/L 50.0
J23.3 02/08/2024 17:576200B1,2-Dibromoethane µg/L 20.0
2250 02/08/2024 17:576200BEthylbenzeneµg/L 17.0
95.7 02/08/2024 17:576200BIsopropylbenzeneµg/L 18.0
401 02/08/2024 17:576200BMethyl tert-butyl ether (MTBE)µg/L 14.0
750 02/08/2024 17:576200BNaphthaleneµg/L 47.0
240 02/08/2024 17:576200Bn-Propylbenzene µg/L 19.0
262 02/08/2024 17:576200BStyreneµg/L 22.0
J41002/08/2024 17:576200Btert-Butyl Alcohol (TBA)µg/L 160
6640 02/08/2024 17:576200Btert-Amyl Alcohol (TAA)µg/L 190
J34.1 02/08/2024 17:576200Btert-Amyl Methyl Ether (TAME)µg/L 28.0
15100 02/09/2024 18:566200BTolueneµg/L 220
1830 02/08/2024 17:576200B1,2,4-Trimethylbenzene µg/L 19.0
465 02/08/2024 17:576200B1,3,5-Trimethylbenzene µg/L 18.0
3950 02/08/2024 17:576200Bo-Xylene µg/L 21.0
7500 02/08/2024 17:576200Bm,p-Xylene µg/L 42.0
11500 02/08/2024 17:576200BXylene (Total)µg/L 21.0
V 95560MW-21
27700 02/09/2024 19:206200BBenzeneµg/L 180
J24.3 02/08/2024 18:216200Bn-Butylbenzene µg/L 18.0
1460 02/08/2024 18:216200BDi-Isopropyl Ether (DIPE)µg/L 50.0
353 02/08/2024 18:216200B1,2-Dibromoethane µg/L 20.0
149 02/08/2024 18:216200B1,2-Dichloroethane µg/L 15.0
3740 02/08/2024 18:216200BEthylbenzeneµg/L 17.0
127 02/08/2024 18:216200BIsopropylbenzeneµg/L 18.0
J26702/08/2024 18:216200BMethyl Ethyl Ketone (MEK)µg/L 71.0
248 02/08/2024 18:216200BMethyl tert-butyl ether (MTBE)µg/L 14.0
Page 7 of 73
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
24-030-0017
Report Limit
Project:Ganesha
V 95560MW-21
1140 02/08/2024 18:216200BNaphthaleneµg/L 47.0
329 02/08/2024 18:216200Bn-Propylbenzene µg/L 19.0
714 02/08/2024 18:216200BStyreneµg/L 22.0
J27902/08/2024 18:216200Btert-Butyl Alcohol (TBA)µg/L 160
13200 02/09/2024 19:206200Btert-Amyl Alcohol (TAA)µg/L 1900
38800 02/09/2024 19:206200BTolueneµg/L 220
2360 02/08/2024 18:216200B1,2,4-Trimethylbenzene µg/L 19.0
568 02/08/2024 18:216200B1,3,5-Trimethylbenzene µg/L 18.0
5940 02/08/2024 18:216200Bo-Xylene µg/L 21.0
11800 02/08/2024 18:216200Bm,p-Xylene µg/L 42.0
17700 02/08/2024 18:216200BXylene (Total)µg/L 21.0
V 95561Trip Blank
J0.380 02/08/2024 13:026200BMethylene Chloride µg/L 0.330
Page 8 of 73

Client: Geological Resources, Inc. CASE NARRATIVE
Project: Ganesha Lab Report Number: 24-030-0017
Date: 2/13/2024
Volatile Organic Compounds - GC/MS Method 6200B Analyte: 3,3-Dimethyl-1-butanol QC Batch No: V43374/V43373
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: 3,3-Dimethyl-1-butanol QC Batch No: V43393/V43373
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Hexachlorobutadiene QC Batch No: V43374/V43373
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: tert-Amyl alcohol QC Batch No: V43494/V43373
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.

Page 9 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:GMW-1
95552 Matrix:
1/30/2024 10:26
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 02/08/24 05:30 6200BMSA
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%02/08/24 05:30100 MSA V43374
Surrogate: Dibromofluoromethane 97.4 Limits: 70-130%02/08/24 05:30100 MSA V43374
Surrogate: 1,2-Dichloroethane - d4 98.8 Limits: 70-130%02/08/24 05:30100 MSA V43374
Surrogate: Toluene-d8 100 Limits: 70-130%02/08/24 05:30100 MSA V43374
Surrogate: 4-Bromofluorobenzene 99.2 Limits: 70-130%02/08/24 21:131000 MSA V43393
Surrogate: Dibromofluoromethane 95.4 Limits: 70-130%02/08/24 21:131000 MSA V43393
Surrogate: 1,2-Dichloroethane - d4 97.6 Limits: 70-130%02/08/24 21:131000 MSA V43393
Surrogate: Toluene-d8 99.4 Limits: 70-130%02/08/24 21:131000 MSA V43393
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:GMW-1
95552 Matrix:
1/30/2024 10:26
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00 V43392 02/08/24 09:00
<180 µg/L 180 1000Acetone 100 02/08/24 05:30 V43374MSA
3200 µg/L 18.0 50.0Benzene 100 02/08/24 05:30 V43374MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 02/08/24 05:30 V43374MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 02/08/24 05:30 V43374MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 02/08/24 05:30 V43374MSA
<150 µg/L 150 500Bromoform 100 02/08/24 05:30 V43374MSA
<28.0 µg/L 28.0 100Bromomethane 100 02/08/24 05:30 V43374MSA
26.0 J µg/L 18.0 50.0n-Butylbenzene 100 02/08/24 05:30 V43374MSA
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 02/08/24 05:30 V43374MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 02/08/24 05:30 V43374MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 02/08/24 05:30 V43374MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 02/08/24 05:30 V43374MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 02/08/24 05:30 V43374MSA
<43.0 µg/L 43.0 100Chloroethane 100 02/08/24 05:30 V43374MSA
<22.0 µg/L 22.0 50.0Chloroform 100 02/08/24 05:30 V43374MSA
<22.0 µg/L 22.0 50.0Chloromethane 100 02/08/24 05:30 V43374MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 02/08/24 05:30 V43374MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 02/08/24 05:30 V43374MSA
90.0 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 02/08/24 05:30 V43374MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 02/08/24 05:30 V43374MSA
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 02/08/24 05:30 V43374MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 02/08/24 05:30 V43374MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:GMW-1
95552 Matrix:
1/30/2024 10:26
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00 V43392 02/08/24 09:00
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 02/08/24 05:30 V43374MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 02/08/24 05:30 V43374MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 02/08/24 05:30 V43374MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 02/08/24 05:30 V43374MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 02/08/24 05:30 V43374MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 02/08/24 05:30 V43374MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 02/08/24 05:30 V43374MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 02/08/24 05:30 V43374MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 02/08/24 05:30 V43374MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 02/08/24 05:30 V43374MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 02/08/24 05:30 V43374MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 02/08/24 05:30 V43374MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 02/08/24 05:30 V43374MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 02/08/24 05:30 V43374MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 02/08/24 05:30 V43374MSA
<4200 µg/L 4200 20000Ethanol 100 02/08/24 05:30 V43374MSA
2060 µg/L 17.0 50.0Ethylbenzene 100 02/08/24 05:30 V43374MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 02/08/24 05:30 V43374MSA
53.1 J µg/L 38.0 1002-Hexanone 100 02/08/24 05:30 V43374MSA
97.3 µg/L 18.0 50.0Isopropylbenzene 100 02/08/24 05:30 V43374MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 02/08/24 05:30 V43374MSA
193 J µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 02/08/24 05:30 V43374MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:GMW-1
95552 Matrix:
1/30/2024 10:26
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00 V43392 02/08/24 09:00
88.5 J µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 02/08/24 05:30 V43374MSA
30.2 J µg/L 7.80 1004-Methyl-2-Pentanone 100 02/08/24 05:30 V43374MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 02/08/24 05:30 V43374MSA
1130 µg/L 47.0 100Naphthalene 100 02/08/24 05:30 V43374MSA
250 µg/L 19.0 50.0n-Propylbenzene 100 02/08/24 05:30 V43374MSA
439 µg/L 22.0 50.0Styrene 100 02/08/24 05:30 V43374MSA
1060 µg/L 160 1000tert-Butyl Alcohol (TBA)100 02/08/24 05:30 V43374MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 02/08/24 05:30 V43374MSA
2870 µg/L 190 1000tert-Amyl Alcohol (TAA)100 02/08/24 05:30 V43374MSA
<28.0 µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 02/08/24 05:30 V43374MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 02/08/24 05:30 V43374MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 02/08/24 05:30 V43374MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 02/08/24 05:30 V43374MSA
13700 µg/L 220 500Toluene 1000 02/08/24 21:13 V43393MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 02/08/24 05:30 V43374MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 02/08/24 05:30 V43374MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 02/08/24 05:30 V43374MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 02/08/24 05:30 V43374MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 02/08/24 05:30 V43374MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 02/08/24 05:30 V43374MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 02/08/24 05:30 V43374MSA
2150 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 02/08/24 05:30 V43374MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:GMW-1
95552 Matrix:
1/30/2024 10:26
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00 V43392 02/08/24 09:00
498 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 02/08/24 05:30 V43374MSA
<100 µg/L 100 500Vinyl Acetate 100 02/08/24 05:30 V43374MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 02/08/24 05:30 V43374MSA
3860 µg/L 21.0 50.0o-Xylene 100 02/08/24 05:30 V43374MSA
7460 µg/L 42.0 100m,p-Xylene 100 02/08/24 05:30 V43374MSA
11300 µg/L 21.0 50.0Xylene (Total)100 02/08/24 05:30 V43374
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%02/08/24 05:30100 MSA V43374
Surrogate: Dibromofluoromethane 97.4 Limits: 70-130%02/08/24 05:30100 MSA V43374
Surrogate: 1,2-Dichloroethane - d4 98.8 Limits: 70-130%02/08/24 05:30100 MSA V43374
Surrogate: Toluene-d8 100 Limits: 70-130%02/08/24 05:30100 MSA V43374
Surrogate: 4-Bromofluorobenzene 99.2 Limits: 70-130%02/08/24 21:131000 MSA V43393
Surrogate: Dibromofluoromethane 95.4 Limits: 70-130%02/08/24 21:131000 MSA V43393
Surrogate: 1,2-Dichloroethane - d4 97.6 Limits: 70-130%02/08/24 21:131000 MSA V43393
Surrogate: Toluene-d8 99.4 Limits: 70-130%02/08/24 21:131000 MSA V43393
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:GMW-2
95553 Matrix:
1/30/2024 10:11
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 02/08/24 05:55 6200BMSA
Surrogate: 4-Bromofluorobenzene 99.8 Limits: 70-130%02/08/24 05:55100 MSA V43374
Surrogate: Dibromofluoromethane 98.8 Limits: 70-130%02/08/24 05:55100 MSA V43374
Surrogate: 1,2-Dichloroethane - d4 98.0 Limits: 70-130%02/08/24 05:55100 MSA V43374
Surrogate: Toluene-d8 100 Limits: 70-130%02/08/24 05:55100 MSA V43374
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:GMW-2
95553 Matrix:
1/30/2024 10:11
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00
<180 µg/L 180 1000Acetone 100 02/08/24 05:55 V43374MSA
941 µg/L 18.0 50.0Benzene 100 02/08/24 05:55 V43374MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 02/08/24 05:55 V43374MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 02/08/24 05:55 V43374MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 02/08/24 05:55 V43374MSA
<150 µg/L 150 500Bromoform 100 02/08/24 05:55 V43374MSA
<28.0 µg/L 28.0 100Bromomethane 100 02/08/24 05:55 V43374MSA
43.5 J µg/L 18.0 50.0n-Butylbenzene 100 02/08/24 05:55 V43374MSA
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 02/08/24 05:55 V43374MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 02/08/24 05:55 V43374MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 02/08/24 05:55 V43374MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 02/08/24 05:55 V43374MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 02/08/24 05:55 V43374MSA
<43.0 µg/L 43.0 100Chloroethane 100 02/08/24 05:55 V43374MSA
<22.0 µg/L 22.0 50.0Chloroform 100 02/08/24 05:55 V43374MSA
<22.0 µg/L 22.0 50.0Chloromethane 100 02/08/24 05:55 V43374MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 02/08/24 05:55 V43374MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 02/08/24 05:55 V43374MSA
<50.0 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 02/08/24 05:55 V43374MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 02/08/24 05:55 V43374MSA
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 02/08/24 05:55 V43374MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 02/08/24 05:55 V43374MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:GMW-2
95553 Matrix:
1/30/2024 10:11
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 02/08/24 05:55 V43374MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 02/08/24 05:55 V43374MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 02/08/24 05:55 V43374MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 02/08/24 05:55 V43374MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 02/08/24 05:55 V43374MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 02/08/24 05:55 V43374MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 02/08/24 05:55 V43374MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 02/08/24 05:55 V43374MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 02/08/24 05:55 V43374MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 02/08/24 05:55 V43374MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 02/08/24 05:55 V43374MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 02/08/24 05:55 V43374MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 02/08/24 05:55 V43374MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 02/08/24 05:55 V43374MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 02/08/24 05:55 V43374MSA
<4200 µg/L 4200 20000Ethanol 100 02/08/24 05:55 V43374MSA
1520 µg/L 17.0 50.0Ethylbenzene 100 02/08/24 05:55 V43374MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 02/08/24 05:55 V43374MSA
87.8 J µg/L 38.0 1002-Hexanone 100 02/08/24 05:55 V43374MSA
90.2 µg/L 18.0 50.0Isopropylbenzene 100 02/08/24 05:55 V43374MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 02/08/24 05:55 V43374MSA
158 J µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 02/08/24 05:55 V43374MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:GMW-2
95553 Matrix:
1/30/2024 10:11
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00
<14.0 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 02/08/24 05:55 V43374MSA
45.6 J µg/L 7.80 1004-Methyl-2-Pentanone 100 02/08/24 05:55 V43374MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 02/08/24 05:55 V43374MSA
601 µg/L 47.0 100Naphthalene 100 02/08/24 05:55 V43374MSA
255 µg/L 19.0 50.0n-Propylbenzene 100 02/08/24 05:55 V43374MSA
158 µg/L 22.0 50.0Styrene 100 02/08/24 05:55 V43374MSA
1100 µg/L 160 1000tert-Butyl Alcohol (TBA)100 02/08/24 05:55 V43374MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 02/08/24 05:55 V43374MSA
2160 µg/L 190 1000tert-Amyl Alcohol (TAA)100 02/08/24 05:55 V43374MSA
<28.0 µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 02/08/24 05:55 V43374MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 02/08/24 05:55 V43374MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 02/08/24 05:55 V43374MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 02/08/24 05:55 V43374MSA
4030 µg/L 22.0 50.0Toluene 100 02/08/24 05:55 V43374MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 02/08/24 05:55 V43374MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 02/08/24 05:55 V43374MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 02/08/24 05:55 V43374MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 02/08/24 05:55 V43374MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 02/08/24 05:55 V43374MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 02/08/24 05:55 V43374MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 02/08/24 05:55 V43374MSA
1850 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 02/08/24 05:55 V43374MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:GMW-2
95553 Matrix:
1/30/2024 10:11
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00
557 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 02/08/24 05:55 V43374MSA
<100 µg/L 100 500Vinyl Acetate 100 02/08/24 05:55 V43374MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 02/08/24 05:55 V43374MSA
2540 µg/L 21.0 50.0o-Xylene 100 02/08/24 05:55 V43374MSA
5420 µg/L 42.0 100m,p-Xylene 100 02/08/24 05:55 V43374MSA
7960 µg/L 21.0 50.0Xylene (Total)100 02/08/24 05:55 V43374
Surrogate: 4-Bromofluorobenzene 99.8 Limits: 70-130%02/08/24 05:55100 MSA V43374
Surrogate: Dibromofluoromethane 98.8 Limits: 70-130%02/08/24 05:55100 MSA V43374
Surrogate: 1,2-Dichloroethane - d4 98.0 Limits: 70-130%02/08/24 05:55100 MSA V43374
Surrogate: Toluene-d8 100 Limits: 70-130%02/08/24 05:55100 MSA V43374
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:GMW-3
95554 Matrix:
1/30/2024 9:29
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 02/08/24 06:19 6200BMSA
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%02/08/24 06:19100 MSA V43374
Surrogate: Dibromofluoromethane 97.6 Limits: 70-130%02/08/24 06:19100 MSA V43374
Surrogate: 1,2-Dichloroethane - d4 98.8 Limits: 70-130%02/08/24 06:19100 MSA V43374
Surrogate: Toluene-d8 99.6 Limits: 70-130%02/08/24 06:19100 MSA V43374
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:GMW-3
95554 Matrix:
1/30/2024 9:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00
<180 µg/L 180 1000Acetone 100 02/08/24 06:19 V43374MSA
1430 µg/L 18.0 50.0Benzene 100 02/08/24 06:19 V43374MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 02/08/24 06:19 V43374MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 02/08/24 06:19 V43374MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 02/08/24 06:19 V43374MSA
<150 µg/L 150 500Bromoform 100 02/08/24 06:19 V43374MSA
<28.0 µg/L 28.0 100Bromomethane 100 02/08/24 06:19 V43374MSA
35.0 J µg/L 18.0 50.0n-Butylbenzene 100 02/08/24 06:19 V43374MSA
20.4 J µg/L 20.0 50.0sec-Butyl benzene 100 02/08/24 06:19 V43374MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 02/08/24 06:19 V43374MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 02/08/24 06:19 V43374MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 02/08/24 06:19 V43374MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 02/08/24 06:19 V43374MSA
<43.0 µg/L 43.0 100Chloroethane 100 02/08/24 06:19 V43374MSA
<22.0 µg/L 22.0 50.0Chloroform 100 02/08/24 06:19 V43374MSA
<22.0 µg/L 22.0 50.0Chloromethane 100 02/08/24 06:19 V43374MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 02/08/24 06:19 V43374MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 02/08/24 06:19 V43374MSA
<50.0 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 02/08/24 06:19 V43374MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 02/08/24 06:19 V43374MSA
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 02/08/24 06:19 V43374MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 02/08/24 06:19 V43374MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:GMW-3
95554 Matrix:
1/30/2024 9:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 02/08/24 06:19 V43374MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 02/08/24 06:19 V43374MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 02/08/24 06:19 V43374MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 02/08/24 06:19 V43374MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 02/08/24 06:19 V43374MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 02/08/24 06:19 V43374MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 02/08/24 06:19 V43374MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 02/08/24 06:19 V43374MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 02/08/24 06:19 V43374MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 02/08/24 06:19 V43374MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 02/08/24 06:19 V43374MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 02/08/24 06:19 V43374MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 02/08/24 06:19 V43374MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 02/08/24 06:19 V43374MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 02/08/24 06:19 V43374MSA
<4200 µg/L 4200 20000Ethanol 100 02/08/24 06:19 V43374MSA
1940 µg/L 17.0 50.0Ethylbenzene 100 02/08/24 06:19 V43374MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 02/08/24 06:19 V43374MSA
<38.0 µg/L 38.0 1002-Hexanone 100 02/08/24 06:19 V43374MSA
105 µg/L 18.0 50.0Isopropylbenzene 100 02/08/24 06:19 V43374MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 02/08/24 06:19 V43374MSA
240 J µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 02/08/24 06:19 V43374MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:GMW-3
95554 Matrix:
1/30/2024 9:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00
39.3 J µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 02/08/24 06:19 V43374MSA
44.5 J µg/L 7.80 1004-Methyl-2-Pentanone 100 02/08/24 06:19 V43374MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 02/08/24 06:19 V43374MSA
720 µg/L 47.0 100Naphthalene 100 02/08/24 06:19 V43374MSA
301 µg/L 19.0 50.0n-Propylbenzene 100 02/08/24 06:19 V43374MSA
113 µg/L 22.0 50.0Styrene 100 02/08/24 06:19 V43374MSA
1180 µg/L 160 1000tert-Butyl Alcohol (TBA)100 02/08/24 06:19 V43374MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 02/08/24 06:19 V43374MSA
5610 µg/L 190 1000tert-Amyl Alcohol (TAA)100 02/08/24 06:19 V43374MSA
<28.0 µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 02/08/24 06:19 V43374MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 02/08/24 06:19 V43374MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 02/08/24 06:19 V43374MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 02/08/24 06:19 V43374MSA
8280 µg/L 22.0 50.0Toluene 100 02/08/24 06:19 V43374MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 02/08/24 06:19 V43374MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 02/08/24 06:19 V43374MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 02/08/24 06:19 V43374MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 02/08/24 06:19 V43374MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 02/08/24 06:19 V43374MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 02/08/24 06:19 V43374MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 02/08/24 06:19 V43374MSA
2690 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 02/08/24 06:19 V43374MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:GMW-3
95554 Matrix:
1/30/2024 9:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00
691 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 02/08/24 06:19 V43374MSA
<100 µg/L 100 500Vinyl Acetate 100 02/08/24 06:19 V43374MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 02/08/24 06:19 V43374MSA
4630 µg/L 21.0 50.0o-Xylene 100 02/08/24 06:19 V43374MSA
8670 µg/L 42.0 100m,p-Xylene 100 02/08/24 06:19 V43374MSA
13300 µg/L 21.0 50.0Xylene (Total)100 02/08/24 06:19 V43374
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%02/08/24 06:19100 MSA V43374
Surrogate: Dibromofluoromethane 97.6 Limits: 70-130%02/08/24 06:19100 MSA V43374
Surrogate: 1,2-Dichloroethane - d4 98.8 Limits: 70-130%02/08/24 06:19100 MSA V43374
Surrogate: Toluene-d8 99.6 Limits: 70-130%02/08/24 06:19100 MSA V43374
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:GMW-4
95555 Matrix:
1/30/2024 9:59
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 02/08/24 06:44 6200BMSA
Surrogate: 4-Bromofluorobenzene 98.4 Limits: 70-130%02/08/24 06:44100 MSA V43374
Surrogate: Dibromofluoromethane 98.4 Limits: 70-130%02/08/24 06:44100 MSA V43374
Surrogate: 1,2-Dichloroethane - d4 99.0 Limits: 70-130%02/08/24 06:44100 MSA V43374
Surrogate: Toluene-d8 100 Limits: 70-130%02/08/24 06:44100 MSA V43374
Surrogate: 4-Bromofluorobenzene 98.0 Limits: 70-130%02/09/24 18:311000 MSA V43494
Surrogate: Dibromofluoromethane 96.0 Limits: 70-130%02/09/24 18:311000 MSA V43494
Surrogate: 1,2-Dichloroethane - d4 97.6 Limits: 70-130%02/09/24 18:311000 MSA V43494
Surrogate: Toluene-d8 99.4 Limits: 70-130%02/09/24 18:311000 MSA V43494
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:GMW-4
95555 Matrix:
1/30/2024 9:59
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00 V43493 02/09/24 09:00
<180 µg/L 180 1000Acetone 100 02/08/24 06:44 V43374MSA
4100 µg/L 18.0 50.0Benzene 100 02/08/24 06:44 V43374MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 02/08/24 06:44 V43374MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 02/08/24 06:44 V43374MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 02/08/24 06:44 V43374MSA
<150 µg/L 150 500Bromoform 100 02/08/24 06:44 V43374MSA
<28.0 µg/L 28.0 100Bromomethane 100 02/08/24 06:44 V43374MSA
<18.0 µg/L 18.0 50.0n-Butylbenzene 100 02/08/24 06:44 V43374MSA
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 02/08/24 06:44 V43374MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 02/08/24 06:44 V43374MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 02/08/24 06:44 V43374MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 02/08/24 06:44 V43374MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 02/08/24 06:44 V43374MSA
<43.0 µg/L 43.0 100Chloroethane 100 02/08/24 06:44 V43374MSA
117 µg/L 22.0 50.0Chloroform 100 02/08/24 06:44 V43374MSA
<22.0 µg/L 22.0 50.0Chloromethane 100 02/08/24 06:44 V43374MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 02/08/24 06:44 V43374MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 02/08/24 06:44 V43374MSA
<50.0 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 02/08/24 06:44 V43374MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 02/08/24 06:44 V43374MSA
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 02/08/24 06:44 V43374MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 02/08/24 06:44 V43374MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:GMW-4
95555 Matrix:
1/30/2024 9:59
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00 V43493 02/09/24 09:00
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 02/08/24 06:44 V43374MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 02/08/24 06:44 V43374MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 02/08/24 06:44 V43374MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 02/08/24 06:44 V43374MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 02/08/24 06:44 V43374MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 02/08/24 06:44 V43374MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 02/08/24 06:44 V43374MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 02/08/24 06:44 V43374MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 02/08/24 06:44 V43374MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 02/08/24 06:44 V43374MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 02/08/24 06:44 V43374MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 02/08/24 06:44 V43374MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 02/08/24 06:44 V43374MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 02/08/24 06:44 V43374MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 02/08/24 06:44 V43374MSA
843000 µg/L 42000 200000Ethanol 1000 02/09/24 18:31 V43494MSA
1220 µg/L 17.0 50.0Ethylbenzene 100 02/08/24 06:44 V43374MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 02/08/24 06:44 V43374MSA
<38.0 µg/L 38.0 1002-Hexanone 100 02/08/24 06:44 V43374MSA
37.4 J µg/L 18.0 50.0Isopropylbenzene 100 02/08/24 06:44 V43374MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 02/08/24 06:44 V43374MSA
225 J µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 02/08/24 06:44 V43374MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:GMW-4
95555 Matrix:
1/30/2024 9:59
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00 V43493 02/09/24 09:00
81.1 J µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 02/08/24 06:44 V43374MSA
22.0 J µg/L 7.80 1004-Methyl-2-Pentanone 100 02/08/24 06:44 V43374MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 02/08/24 06:44 V43374MSA
266 µg/L 47.0 100Naphthalene 100 02/08/24 06:44 V43374MSA
101 µg/L 19.0 50.0n-Propylbenzene 100 02/08/24 06:44 V43374MSA
22.7 J µg/L 22.0 50.0Styrene 100 02/08/24 06:44 V43374MSA
1270 µg/L 160 1000tert-Butyl Alcohol (TBA)100 02/08/24 06:44 V43374MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 02/08/24 06:44 V43374MSA
7100 µg/L 190 1000tert-Amyl Alcohol (TAA)100 02/08/24 06:44 V43374MSA
<28.0 µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 02/08/24 06:44 V43374MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 02/08/24 06:44 V43374MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 02/08/24 06:44 V43374MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 02/08/24 06:44 V43374MSA
8460 µg/L 22.0 50.0Toluene 100 02/08/24 06:44 V43374MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 02/08/24 06:44 V43374MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 02/08/24 06:44 V43374MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 02/08/24 06:44 V43374MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 02/08/24 06:44 V43374MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 02/08/24 06:44 V43374MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 02/08/24 06:44 V43374MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 02/08/24 06:44 V43374MSA
813 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 02/08/24 06:44 V43374MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:GMW-4
95555 Matrix:
1/30/2024 9:59
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00 V43493 02/09/24 09:00
188 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 02/08/24 06:44 V43374MSA
<100 µg/L 100 500Vinyl Acetate 100 02/08/24 06:44 V43374MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 02/08/24 06:44 V43374MSA
2320 µg/L 21.0 50.0o-Xylene 100 02/08/24 06:44 V43374MSA
4700 µg/L 42.0 100m,p-Xylene 100 02/08/24 06:44 V43374MSA
7020 µg/L 21.0 50.0Xylene (Total)100 02/08/24 06:44 V43374
Surrogate: 4-Bromofluorobenzene 98.4 Limits: 70-130%02/08/24 06:44100 MSA V43374
Surrogate: Dibromofluoromethane 98.4 Limits: 70-130%02/08/24 06:44100 MSA V43374
Surrogate: 1,2-Dichloroethane - d4 99.0 Limits: 70-130%02/08/24 06:44100 MSA V43374
Surrogate: Toluene-d8 100 Limits: 70-130%02/08/24 06:44100 MSA V43374
Surrogate: 4-Bromofluorobenzene 98.0 Limits: 70-130%02/09/24 18:311000 MSA V43494
Surrogate: Dibromofluoromethane 96.0 Limits: 70-130%02/09/24 18:311000 MSA V43494
Surrogate: 1,2-Dichloroethane - d4 97.6 Limits: 70-130%02/09/24 18:311000 MSA V43494
Surrogate: Toluene-d8 99.4 Limits: 70-130%02/09/24 18:311000 MSA V43494
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MMPE-2
95556 Matrix:
1/30/2024 10:42
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 02/08/24 02:38 6200BMSA
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%02/08/24 02:381 MSA V43374
Surrogate: Dibromofluoromethane 98.4 Limits: 70-130%02/08/24 02:381 MSA V43374
Surrogate: 1,2-Dichloroethane - d4 99.2 Limits: 70-130%02/08/24 02:381 MSA V43374
Surrogate: Toluene-d8 101 Limits: 70-130%02/08/24 02:381 MSA V43374
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%02/08/24 16:1810 MSA V43393
Surrogate: Dibromofluoromethane 96.6 Limits: 70-130%02/08/24 16:1810 MSA V43393
Surrogate: 1,2-Dichloroethane - d4 95.8 Limits: 70-130%02/08/24 16:1810 MSA V43393
Surrogate: Toluene-d8 100 Limits: 70-130%02/08/24 16:1810 MSA V43393
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MMPE-2
95556 Matrix:
1/30/2024 10:42
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00 V43392 02/08/24 09:00
<1.80 µg/L 1.80 10.0Acetone 1 02/08/24 02:38 V43374MSA
81.4 µg/L 0.180 0.500Benzene 1 02/08/24 02:38 V43374MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 02/08/24 02:38 V43374MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 02/08/24 02:38 V43374MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 02/08/24 02:38 V43374MSA
<1.50 µg/L 1.50 5.00Bromoform 1 02/08/24 02:38 V43374MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 02/08/24 02:38 V43374MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 02/08/24 02:38 V43374MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 02/08/24 02:38 V43374MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 02/08/24 02:38 V43374MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 02/08/24 02:38 V43374MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 02/08/24 02:38 V43374MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 02/08/24 02:38 V43374MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 02/08/24 02:38 V43374MSA
1.20 µg/L 0.220 0.500Chloroform 1 02/08/24 02:38 V43374MSA
2.16 µg/L 0.220 0.500Chloromethane 1 02/08/24 02:38 V43374MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 02/08/24 02:38 V43374MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 02/08/24 02:38 V43374MSA
1.14 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 02/08/24 02:38 V43374MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 02/08/24 02:38 V43374MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 02/08/24 02:38 V43374MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 02/08/24 02:38 V43374MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MMPE-2
95556 Matrix:
1/30/2024 10:42
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00 V43392 02/08/24 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 02/08/24 02:38 V43374MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 02/08/24 02:38 V43374MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 02/08/24 02:38 V43374MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 02/08/24 02:38 V43374MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 02/08/24 02:38 V43374MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 02/08/24 02:38 V43374MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 02/08/24 02:38 V43374MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 02/08/24 02:38 V43374MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 02/08/24 02:38 V43374MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 02/08/24 02:38 V43374MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 02/08/24 02:38 V43374MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 02/08/24 02:38 V43374MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 02/08/24 02:38 V43374MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 02/08/24 02:38 V43374MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 02/08/24 02:38 V43374MSA
<42.0 µg/L 42.0 200Ethanol 1 02/08/24 02:38 V43374MSA
10.6 µg/L 0.170 0.500Ethylbenzene 1 02/08/24 02:38 V43374MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 02/08/24 02:38 V43374MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 02/08/24 02:38 V43374MSA
0.317 J µg/L 0.180 0.500Isopropylbenzene 1 02/08/24 02:38 V43374MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 02/08/24 02:38 V43374MSA
2.30 J µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 02/08/24 02:38 V43374MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MMPE-2
95556 Matrix:
1/30/2024 10:42
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00 V43392 02/08/24 09:00
2.33 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 02/08/24 02:38 V43374MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 02/08/24 02:38 V43374MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 02/08/24 02:38 V43374MSA
4.24 µg/L 0.470 1.00Naphthalene 1 02/08/24 02:38 V43374MSA
0.669 µg/L 0.190 0.500n-Propylbenzene 1 02/08/24 02:38 V43374MSA
0.964 µg/L 0.220 0.500Styrene 1 02/08/24 02:38 V43374MSA
33.5 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 02/08/24 02:38 V43374MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 02/08/24 02:38 V43374MSA
622 µg/L 19.0 100tert-Amyl Alcohol (TAA)10 02/08/24 16:18 V43393MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 02/08/24 02:38 V43374MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 02/08/24 02:38 V43374MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 02/08/24 02:38 V43374MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 02/08/24 02:38 V43374MSA
46.7 µg/L 0.220 0.500Toluene 1 02/08/24 02:38 V43374MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 02/08/24 02:38 V43374MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 02/08/24 02:38 V43374MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 02/08/24 02:38 V43374MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 02/08/24 02:38 V43374MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 02/08/24 02:38 V43374MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 02/08/24 02:38 V43374MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 02/08/24 02:38 V43374MSA
16.0 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 02/08/24 02:38 V43374MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MMPE-2
95556 Matrix:
1/30/2024 10:42
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00 V43392 02/08/24 09:00
4.90 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 02/08/24 02:38 V43374MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 02/08/24 02:38 V43374MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 02/08/24 02:38 V43374MSA
60.2 µg/L 0.210 0.500o-Xylene 1 02/08/24 02:38 V43374MSA
96.2 µg/L 0.420 1.00m,p-Xylene 1 02/08/24 02:38 V43374MSA
156 µg/L 0.210 0.500Xylene (Total)1 02/08/24 02:38 V43374
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%02/08/24 02:381 MSA V43374
Surrogate: Dibromofluoromethane 98.4 Limits: 70-130%02/08/24 02:381 MSA V43374
Surrogate: 1,2-Dichloroethane - d4 99.2 Limits: 70-130%02/08/24 02:381 MSA V43374
Surrogate: Toluene-d8 101 Limits: 70-130%02/08/24 02:381 MSA V43374
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%02/08/24 16:1810 MSA V43393
Surrogate: Dibromofluoromethane 96.6 Limits: 70-130%02/08/24 16:1810 MSA V43393
Surrogate: 1,2-Dichloroethane - d4 95.8 Limits: 70-130%02/08/24 16:1810 MSA V43393
Surrogate: Toluene-d8 100 Limits: 70-130%02/08/24 16:1810 MSA V43393
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MMPE-3
95557 Matrix:
1/30/2024 10:58
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 02/08/24 15:05 6200BMSA
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%02/08/24 15:051 MSA V43393
Surrogate: Dibromofluoromethane 97.0 Limits: 70-130%02/08/24 15:051 MSA V43393
Surrogate: 1,2-Dichloroethane - d4 98.0 Limits: 70-130%02/08/24 15:051 MSA V43393
Surrogate: Toluene-d8 100 Limits: 70-130%02/08/24 15:051 MSA V43393
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MMPE-3
95557 Matrix:
1/30/2024 10:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43392 02/08/24 09:00
<1.80 µg/L 1.80 10.0Acetone 1 02/08/24 15:05 V43393MSA
<0.180 µg/L 0.180 0.500Benzene 1 02/08/24 15:05 V43393MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 02/08/24 15:05 V43393MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 02/08/24 15:05 V43393MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 02/08/24 15:05 V43393MSA
<1.50 µg/L 1.50 5.00Bromoform 1 02/08/24 15:05 V43393MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 02/08/24 15:05 V43393MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 02/08/24 15:05 V43393MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 02/08/24 15:05 V43393MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 02/08/24 15:05 V43393MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 02/08/24 15:05 V43393MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 02/08/24 15:05 V43393MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 02/08/24 15:05 V43393MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 02/08/24 15:05 V43393MSA
<0.220 µg/L 0.220 0.500Chloroform 1 02/08/24 15:05 V43393MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 02/08/24 15:05 V43393MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 02/08/24 15:05 V43393MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 02/08/24 15:05 V43393MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 02/08/24 15:05 V43393MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 02/08/24 15:05 V43393MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 02/08/24 15:05 V43393MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 02/08/24 15:05 V43393MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MMPE-3
95557 Matrix:
1/30/2024 10:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43392 02/08/24 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 02/08/24 15:05 V43393MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 02/08/24 15:05 V43393MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 02/08/24 15:05 V43393MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 02/08/24 15:05 V43393MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 02/08/24 15:05 V43393MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 02/08/24 15:05 V43393MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 02/08/24 15:05 V43393MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 02/08/24 15:05 V43393MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 02/08/24 15:05 V43393MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 02/08/24 15:05 V43393MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 02/08/24 15:05 V43393MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 02/08/24 15:05 V43393MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 02/08/24 15:05 V43393MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 02/08/24 15:05 V43393MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 02/08/24 15:05 V43393MSA
<42.0 µg/L 42.0 200Ethanol 1 02/08/24 15:05 V43393MSA
0.222 J µg/L 0.170 0.500Ethylbenzene 1 02/08/24 15:05 V43393MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 02/08/24 15:05 V43393MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 02/08/24 15:05 V43393MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 02/08/24 15:05 V43393MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 02/08/24 15:05 V43393MSA
0.846 J µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 02/08/24 15:05 V43393MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MMPE-3
95557 Matrix:
1/30/2024 10:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43392 02/08/24 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 02/08/24 15:05 V43393MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 02/08/24 15:05 V43393MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 02/08/24 15:05 V43393MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 02/08/24 15:05 V43393MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 02/08/24 15:05 V43393MSA
<0.220 µg/L 0.220 0.500Styrene 1 02/08/24 15:05 V43393MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 02/08/24 15:05 V43393MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 02/08/24 15:05 V43393MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 02/08/24 15:05 V43393MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 02/08/24 15:05 V43393MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 02/08/24 15:05 V43393MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 02/08/24 15:05 V43393MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 02/08/24 15:05 V43393MSA
0.399 J µg/L 0.220 0.500Toluene 1 02/08/24 15:05 V43393MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 02/08/24 15:05 V43393MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 02/08/24 15:05 V43393MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 02/08/24 15:05 V43393MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 02/08/24 15:05 V43393MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 02/08/24 15:05 V43393MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 02/08/24 15:05 V43393MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 02/08/24 15:05 V43393MSA
0.600 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 02/08/24 15:05 V43393MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MMPE-3
95557 Matrix:
1/30/2024 10:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43392 02/08/24 09:00
0.201 J µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 02/08/24 15:05 V43393MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 02/08/24 15:05 V43393MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 02/08/24 15:05 V43393MSA
0.522 µg/L 0.210 0.500o-Xylene 1 02/08/24 15:05 V43393MSA
0.902 J µg/L 0.420 1.00m,p-Xylene 1 02/08/24 15:05 V43393MSA
1.42 J µg/L 0.210 0.500Xylene (Total)1 02/08/24 15:05 V43393
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%02/08/24 15:051 MSA V43393
Surrogate: Dibromofluoromethane 97.0 Limits: 70-130%02/08/24 15:051 MSA V43393
Surrogate: 1,2-Dichloroethane - d4 98.0 Limits: 70-130%02/08/24 15:051 MSA V43393
Surrogate: Toluene-d8 100 Limits: 70-130%02/08/24 15:051 MSA V43393
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MW-6
95558 Matrix:
1/30/2024 11:52
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 02/08/24 03:27 6200BMSA
Surrogate: 4-Bromofluorobenzene 98.8 Limits: 70-130%02/08/24 03:271 MSA V43374
Surrogate: Dibromofluoromethane 100 Limits: 70-130%02/08/24 03:271 MSA V43374
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 70-130%02/08/24 03:271 MSA V43374
Surrogate: Toluene-d8 99.2 Limits: 70-130%02/08/24 03:271 MSA V43374
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MW-6
95558 Matrix:
1/30/2024 11:52
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00
<1.80 µg/L 1.80 10.0Acetone 1 02/08/24 03:27 V43374MSA
<0.180 µg/L 0.180 0.500Benzene 1 02/08/24 03:27 V43374MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 02/08/24 03:27 V43374MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 02/08/24 03:27 V43374MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 02/08/24 03:27 V43374MSA
<1.50 µg/L 1.50 5.00Bromoform 1 02/08/24 03:27 V43374MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 02/08/24 03:27 V43374MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 02/08/24 03:27 V43374MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 02/08/24 03:27 V43374MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 02/08/24 03:27 V43374MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 02/08/24 03:27 V43374MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 02/08/24 03:27 V43374MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 02/08/24 03:27 V43374MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 02/08/24 03:27 V43374MSA
<0.220 µg/L 0.220 0.500Chloroform 1 02/08/24 03:27 V43374MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 02/08/24 03:27 V43374MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 02/08/24 03:27 V43374MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 02/08/24 03:27 V43374MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 02/08/24 03:27 V43374MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 02/08/24 03:27 V43374MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 02/08/24 03:27 V43374MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 02/08/24 03:27 V43374MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MW-6
95558 Matrix:
1/30/2024 11:52
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 02/08/24 03:27 V43374MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 02/08/24 03:27 V43374MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 02/08/24 03:27 V43374MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 02/08/24 03:27 V43374MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 02/08/24 03:27 V43374MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 02/08/24 03:27 V43374MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 02/08/24 03:27 V43374MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 02/08/24 03:27 V43374MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 02/08/24 03:27 V43374MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 02/08/24 03:27 V43374MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 02/08/24 03:27 V43374MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 02/08/24 03:27 V43374MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 02/08/24 03:27 V43374MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 02/08/24 03:27 V43374MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 02/08/24 03:27 V43374MSA
<42.0 µg/L 42.0 200Ethanol 1 02/08/24 03:27 V43374MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 02/08/24 03:27 V43374MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 02/08/24 03:27 V43374MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 02/08/24 03:27 V43374MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 02/08/24 03:27 V43374MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 02/08/24 03:27 V43374MSA
0.755 J µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 02/08/24 03:27 V43374MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 42 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MW-6
95558 Matrix:
1/30/2024 11:52
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 02/08/24 03:27 V43374MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 02/08/24 03:27 V43374MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 02/08/24 03:27 V43374MSA
0.536 J µg/L 0.470 1.00Naphthalene 1 02/08/24 03:27 V43374MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 02/08/24 03:27 V43374MSA
<0.220 µg/L 0.220 0.500Styrene 1 02/08/24 03:27 V43374MSA
10.5 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 02/08/24 03:27 V43374MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 02/08/24 03:27 V43374MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 02/08/24 03:27 V43374MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 02/08/24 03:27 V43374MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 02/08/24 03:27 V43374MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 02/08/24 03:27 V43374MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 02/08/24 03:27 V43374MSA
<0.220 µg/L 0.220 0.500Toluene 1 02/08/24 03:27 V43374MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 02/08/24 03:27 V43374MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 02/08/24 03:27 V43374MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 02/08/24 03:27 V43374MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 02/08/24 03:27 V43374MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 02/08/24 03:27 V43374MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 02/08/24 03:27 V43374MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 02/08/24 03:27 V43374MSA
0.493 J µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 02/08/24 03:27 V43374MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MW-6
95558 Matrix:
1/30/2024 11:52
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43373 02/07/24 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 02/08/24 03:27 V43374MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 02/08/24 03:27 V43374MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 02/08/24 03:27 V43374MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 02/08/24 03:27 V43374MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 02/08/24 03:27 V43374MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 02/08/24 03:27 V43374
Surrogate: 4-Bromofluorobenzene 98.8 Limits: 70-130%02/08/24 03:271 MSA V43374
Surrogate: Dibromofluoromethane 100 Limits: 70-130%02/08/24 03:271 MSA V43374
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 70-130%02/08/24 03:271 MSA V43374
Surrogate: Toluene-d8 99.2 Limits: 70-130%02/08/24 03:271 MSA V43374
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MW-18
95559 Matrix:
1/30/2024 11:32
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 02/08/24 17:57 6200BMSA
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%02/08/24 17:57100 MSA V43393
Surrogate: Dibromofluoromethane 97.4 Limits: 70-130%02/08/24 17:57100 MSA V43393
Surrogate: 1,2-Dichloroethane - d4 97.0 Limits: 70-130%02/08/24 17:57100 MSA V43393
Surrogate: Toluene-d8 99.4 Limits: 70-130%02/08/24 17:57100 MSA V43393
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%02/09/24 18:561000 MSA V43494
Surrogate: Dibromofluoromethane 96.4 Limits: 70-130%02/09/24 18:561000 MSA V43494
Surrogate: 1,2-Dichloroethane - d4 98.0 Limits: 70-130%02/09/24 18:561000 MSA V43494
Surrogate: Toluene-d8 99.4 Limits: 70-130%02/09/24 18:561000 MSA V43494
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 45 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MW-18
95559 Matrix:
1/30/2024 11:32
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43392 02/08/24 09:00 V43493 02/09/24 09:00
<180 µg/L 180 1000Acetone 100 02/08/24 17:57 V43393MSA
3170 µg/L 18.0 50.0Benzene 100 02/08/24 17:57 V43393MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 02/08/24 17:57 V43393MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 02/08/24 17:57 V43393MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 02/08/24 17:57 V43393MSA
<150 µg/L 150 500Bromoform 100 02/08/24 17:57 V43393MSA
<28.0 µg/L 28.0 100Bromomethane 100 02/08/24 17:57 V43393MSA
<18.0 µg/L 18.0 50.0n-Butylbenzene 100 02/08/24 17:57 V43393MSA
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 02/08/24 17:57 V43393MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 02/08/24 17:57 V43393MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 02/08/24 17:57 V43393MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 02/08/24 17:57 V43393MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 02/08/24 17:57 V43393MSA
<43.0 µg/L 43.0 100Chloroethane 100 02/08/24 17:57 V43393MSA
<22.0 µg/L 22.0 50.0Chloroform 100 02/08/24 17:57 V43393MSA
<22.0 µg/L 22.0 50.0Chloromethane 100 02/08/24 17:57 V43393MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 02/08/24 17:57 V43393MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 02/08/24 17:57 V43393MSA
229 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 02/08/24 17:57 V43393MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 02/08/24 17:57 V43393MSA
23.3 J µg/L 20.0 50.01,2-Dibromoethane 100 02/08/24 17:57 V43393MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 02/08/24 17:57 V43393MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 46 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MW-18
95559 Matrix:
1/30/2024 11:32
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43392 02/08/24 09:00 V43493 02/09/24 09:00
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 02/08/24 17:57 V43393MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 02/08/24 17:57 V43393MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 02/08/24 17:57 V43393MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 02/08/24 17:57 V43393MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 02/08/24 17:57 V43393MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 02/08/24 17:57 V43393MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 02/08/24 17:57 V43393MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 02/08/24 17:57 V43393MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 02/08/24 17:57 V43393MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 02/08/24 17:57 V43393MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 02/08/24 17:57 V43393MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 02/08/24 17:57 V43393MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 02/08/24 17:57 V43393MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 02/08/24 17:57 V43393MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 02/08/24 17:57 V43393MSA
<4200 µg/L 4200 20000Ethanol 100 02/08/24 17:57 V43393MSA
2250 µg/L 17.0 50.0Ethylbenzene 100 02/08/24 17:57 V43393MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 02/08/24 17:57 V43393MSA
<38.0 µg/L 38.0 1002-Hexanone 100 02/08/24 17:57 V43393MSA
95.7 µg/L 18.0 50.0Isopropylbenzene 100 02/08/24 17:57 V43393MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 02/08/24 17:57 V43393MSA
<71.0 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 02/08/24 17:57 V43393MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 47 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MW-18
95559 Matrix:
1/30/2024 11:32
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43392 02/08/24 09:00 V43493 02/09/24 09:00
401 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 02/08/24 17:57 V43393MSA
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 02/08/24 17:57 V43393MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 02/08/24 17:57 V43393MSA
750 µg/L 47.0 100Naphthalene 100 02/08/24 17:57 V43393MSA
240 µg/L 19.0 50.0n-Propylbenzene 100 02/08/24 17:57 V43393MSA
262 µg/L 22.0 50.0Styrene 100 02/08/24 17:57 V43393MSA
410 J µg/L 160 1000tert-Butyl Alcohol (TBA)100 02/08/24 17:57 V43393MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 02/08/24 17:57 V43393MSA
6640 µg/L 190 1000tert-Amyl Alcohol (TAA)100 02/08/24 17:57 V43393MSA
34.1 J µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 02/08/24 17:57 V43393MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 02/08/24 17:57 V43393MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 02/08/24 17:57 V43393MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 02/08/24 17:57 V43393MSA
15100 µg/L 220 500Toluene 1000 02/09/24 18:56 V43494MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 02/08/24 17:57 V43393MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 02/08/24 17:57 V43393MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 02/08/24 17:57 V43393MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 02/08/24 17:57 V43393MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 02/08/24 17:57 V43393MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 02/08/24 17:57 V43393MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 02/08/24 17:57 V43393MSA
1830 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 02/08/24 17:57 V43393MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 48 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MW-18
95559 Matrix:
1/30/2024 11:32
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43392 02/08/24 09:00 V43493 02/09/24 09:00
465 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 02/08/24 17:57 V43393MSA
<100 µg/L 100 500Vinyl Acetate 100 02/08/24 17:57 V43393MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 02/08/24 17:57 V43393MSA
3950 µg/L 21.0 50.0o-Xylene 100 02/08/24 17:57 V43393MSA
7500 µg/L 42.0 100m,p-Xylene 100 02/08/24 17:57 V43393MSA
11500 µg/L 21.0 50.0Xylene (Total)100 02/08/24 17:57 V43393
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%02/08/24 17:57100 MSA V43393
Surrogate: Dibromofluoromethane 97.4 Limits: 70-130%02/08/24 17:57100 MSA V43393
Surrogate: 1,2-Dichloroethane - d4 97.0 Limits: 70-130%02/08/24 17:57100 MSA V43393
Surrogate: Toluene-d8 99.4 Limits: 70-130%02/08/24 17:57100 MSA V43393
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%02/09/24 18:561000 MSA V43494
Surrogate: Dibromofluoromethane 96.4 Limits: 70-130%02/09/24 18:561000 MSA V43494
Surrogate: 1,2-Dichloroethane - d4 98.0 Limits: 70-130%02/09/24 18:561000 MSA V43494
Surrogate: Toluene-d8 99.4 Limits: 70-130%02/09/24 18:561000 MSA V43494
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 49 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MW-21
95560 Matrix:
1/30/2024 12:07
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 02/08/24 18:21 6200BMSA
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%02/08/24 18:21100 MSA V43393
Surrogate: Dibromofluoromethane 95.4 Limits: 70-130%02/08/24 18:21100 MSA V43393
Surrogate: 1,2-Dichloroethane - d4 98.4 Limits: 70-130%02/08/24 18:21100 MSA V43393
Surrogate: Toluene-d8 97.8 Limits: 70-130%02/08/24 18:21100 MSA V43393
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%02/09/24 19:201000 MSA V43494
Surrogate: Dibromofluoromethane 95.4 Limits: 70-130%02/09/24 19:201000 MSA V43494
Surrogate: 1,2-Dichloroethane - d4 97.2 Limits: 70-130%02/09/24 19:201000 MSA V43494
Surrogate: Toluene-d8 99.0 Limits: 70-130%02/09/24 19:201000 MSA V43494
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 50 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MW-21
95560 Matrix:
1/30/2024 12:07
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43392 02/08/24 09:00 V43493 02/09/24 09:00
<180 µg/L 180 1000Acetone 100 02/08/24 18:21 V43393MSA
27700 µg/L 180 500Benzene 1000 02/09/24 19:20 V43494MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 02/08/24 18:21 V43393MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 02/08/24 18:21 V43393MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 02/08/24 18:21 V43393MSA
<150 µg/L 150 500Bromoform 100 02/08/24 18:21 V43393MSA
<28.0 µg/L 28.0 100Bromomethane 100 02/08/24 18:21 V43393MSA
24.3 J µg/L 18.0 50.0n-Butylbenzene 100 02/08/24 18:21 V43393MSA
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 02/08/24 18:21 V43393MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 02/08/24 18:21 V43393MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 02/08/24 18:21 V43393MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 02/08/24 18:21 V43393MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 02/08/24 18:21 V43393MSA
<43.0 µg/L 43.0 100Chloroethane 100 02/08/24 18:21 V43393MSA
<22.0 µg/L 22.0 50.0Chloroform 100 02/08/24 18:21 V43393MSA
<22.0 µg/L 22.0 50.0Chloromethane 100 02/08/24 18:21 V43393MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 02/08/24 18:21 V43393MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 02/08/24 18:21 V43393MSA
1460 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 02/08/24 18:21 V43393MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 02/08/24 18:21 V43393MSA
353 µg/L 20.0 50.01,2-Dibromoethane 100 02/08/24 18:21 V43393MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 02/08/24 18:21 V43393MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 51 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MW-21
95560 Matrix:
1/30/2024 12:07
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43392 02/08/24 09:00 V43493 02/09/24 09:00
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 02/08/24 18:21 V43393MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 02/08/24 18:21 V43393MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 02/08/24 18:21 V43393MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 02/08/24 18:21 V43393MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 02/08/24 18:21 V43393MSA
149 µg/L 15.0 50.01,2-Dichloroethane 100 02/08/24 18:21 V43393MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 02/08/24 18:21 V43393MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 02/08/24 18:21 V43393MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 02/08/24 18:21 V43393MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 02/08/24 18:21 V43393MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 02/08/24 18:21 V43393MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 02/08/24 18:21 V43393MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 02/08/24 18:21 V43393MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 02/08/24 18:21 V43393MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 02/08/24 18:21 V43393MSA
<4200 µg/L 4200 20000Ethanol 100 02/08/24 18:21 V43393MSA
3740 µg/L 17.0 50.0Ethylbenzene 100 02/08/24 18:21 V43393MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 02/08/24 18:21 V43393MSA
<38.0 µg/L 38.0 1002-Hexanone 100 02/08/24 18:21 V43393MSA
127 µg/L 18.0 50.0Isopropylbenzene 100 02/08/24 18:21 V43393MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 02/08/24 18:21 V43393MSA
267 J µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 02/08/24 18:21 V43393MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 52 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MW-21
95560 Matrix:
1/30/2024 12:07
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43392 02/08/24 09:00 V43493 02/09/24 09:00
248 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 02/08/24 18:21 V43393MSA
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 02/08/24 18:21 V43393MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 02/08/24 18:21 V43393MSA
1140 µg/L 47.0 100Naphthalene 100 02/08/24 18:21 V43393MSA
329 µg/L 19.0 50.0n-Propylbenzene 100 02/08/24 18:21 V43393MSA
714 µg/L 22.0 50.0Styrene 100 02/08/24 18:21 V43393MSA
279 J µg/L 160 1000tert-Butyl Alcohol (TBA)100 02/08/24 18:21 V43393MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 02/08/24 18:21 V43393MSA
13200 µg/L 1900 10000tert-Amyl Alcohol (TAA)1000 02/09/24 19:20 V43494MSA
<28.0 µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 02/08/24 18:21 V43393MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 02/08/24 18:21 V43393MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 02/08/24 18:21 V43393MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 02/08/24 18:21 V43393MSA
38800 µg/L 220 500Toluene 1000 02/09/24 19:20 V43494MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 02/08/24 18:21 V43393MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 02/08/24 18:21 V43393MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 02/08/24 18:21 V43393MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 02/08/24 18:21 V43393MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 02/08/24 18:21 V43393MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 02/08/24 18:21 V43393MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 02/08/24 18:21 V43393MSA
2360 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 02/08/24 18:21 V43393MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 53 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:MW-21
95560 Matrix:
1/30/2024 12:07
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43392 02/08/24 09:00 V43493 02/09/24 09:00
568 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 02/08/24 18:21 V43393MSA
<100 µg/L 100 500Vinyl Acetate 100 02/08/24 18:21 V43393MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 02/08/24 18:21 V43393MSA
5940 µg/L 21.0 50.0o-Xylene 100 02/08/24 18:21 V43393MSA
11800 µg/L 42.0 100m,p-Xylene 100 02/08/24 18:21 V43393MSA
17700 µg/L 21.0 50.0Xylene (Total)100 02/08/24 18:21 V43393
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%02/08/24 18:21100 MSA V43393
Surrogate: Dibromofluoromethane 95.4 Limits: 70-130%02/08/24 18:21100 MSA V43393
Surrogate: 1,2-Dichloroethane - d4 98.4 Limits: 70-130%02/08/24 18:21100 MSA V43393
Surrogate: Toluene-d8 97.8 Limits: 70-130%02/08/24 18:21100 MSA V43393
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%02/09/24 19:201000 MSA V43494
Surrogate: Dibromofluoromethane 95.4 Limits: 70-130%02/09/24 19:201000 MSA V43494
Surrogate: 1,2-Dichloroethane - d4 97.2 Limits: 70-130%02/09/24 19:201000 MSA V43494
Surrogate: Toluene-d8 99.0 Limits: 70-130%02/09/24 19:201000 MSA V43494
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 54 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:Trip Blank
95561 Matrix:
1/30/2024 8:25
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43392 02/08/24 09:00
<1.80 µg/L 1.80 10.0Acetone 1 02/08/24 13:02 V43393MSA
<0.180 µg/L 0.180 0.500Benzene 1 02/08/24 13:02 V43393MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 02/08/24 13:02 V43393MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 02/08/24 13:02 V43393MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 02/08/24 13:02 V43393MSA
<1.50 µg/L 1.50 5.00Bromoform 1 02/08/24 13:02 V43393MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 02/08/24 13:02 V43393MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 02/08/24 13:02 V43393MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 02/08/24 13:02 V43393MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 02/08/24 13:02 V43393MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 02/08/24 13:02 V43393MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 02/08/24 13:02 V43393MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 02/08/24 13:02 V43393MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 02/08/24 13:02 V43393MSA
<0.220 µg/L 0.220 0.500Chloroform 1 02/08/24 13:02 V43393MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 02/08/24 13:02 V43393MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 02/08/24 13:02 V43393MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 02/08/24 13:02 V43393MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 02/08/24 13:02 V43393MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 02/08/24 13:02 V43393MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 02/08/24 13:02 V43393MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 02/08/24 13:02 V43393MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 55 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:Trip Blank
95561 Matrix:
1/30/2024 8:25
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43392 02/08/24 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 02/08/24 13:02 V43393MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 02/08/24 13:02 V43393MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 02/08/24 13:02 V43393MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 02/08/24 13:02 V43393MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 02/08/24 13:02 V43393MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 02/08/24 13:02 V43393MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 02/08/24 13:02 V43393MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 02/08/24 13:02 V43393MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 02/08/24 13:02 V43393MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 02/08/24 13:02 V43393MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 02/08/24 13:02 V43393MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 02/08/24 13:02 V43393MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 02/08/24 13:02 V43393MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 02/08/24 13:02 V43393MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 02/08/24 13:02 V43393MSA
<42.0 µg/L 42.0 200Ethanol 1 02/08/24 13:02 V43393MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 02/08/24 13:02 V43393MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 02/08/24 13:02 V43393MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 02/08/24 13:02 V43393MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 02/08/24 13:02 V43393MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 02/08/24 13:02 V43393MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 02/08/24 13:02 V43393MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 56 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:Trip Blank
95561 Matrix:
1/30/2024 8:25
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43392 02/08/24 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 02/08/24 13:02 V43393MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 02/08/24 13:02 V43393MSA
0.380 J µg/L 0.330 2.00Methylene Chloride 1 02/08/24 13:02 V43393MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 02/08/24 13:02 V43393MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 02/08/24 13:02 V43393MSA
<0.220 µg/L 0.220 0.500Styrene 1 02/08/24 13:02 V43393MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 02/08/24 13:02 V43393MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 02/08/24 13:02 V43393MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 02/08/24 13:02 V43393MSA
<0.220 µg/L 0.220 0.500Toluene 1 02/08/24 13:02 V43393MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 02/08/24 13:02 V43393MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 02/08/24 13:02 V43393MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 02/08/24 13:02 V43393MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 02/08/24 13:02 V43393MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 02/08/24 13:02 V43393MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 02/08/24 13:02 V43393MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 02/08/24 13:02 V43393MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 02/08/24 13:02 V43393MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 02/08/24 13:02 V43393MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 02/08/24 13:02 V43393MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 02/08/24 13:02 V43393MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 02/08/24 13:02 V43393MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 57 of 73
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
24-030-0017
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #4457 Received : 01/30/2024
Ganesha
Report Date : 02/13/2024
Sample ID :
Lab No :
Sampled:Trip Blank
95561 Matrix:
1/30/2024 8:25
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V43392 02/08/24 09:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 02/08/24 13:02 V43393MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 02/08/24 13:02 V43393
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%02/08/24 13:021 MSA V43393
Surrogate: Dibromofluoromethane 99.0 Limits: 70-130%02/08/24 13:021 MSA V43393
Surrogate: 1,2-Dichloroethane - d4 98.4 Limits: 70-130%02/08/24 13:021 MSA V43393
Surrogate: Toluene-d8 99.8 Limits: 70-130%02/08/24 13:021 MSA V43393
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 58 of 73
Quality Control Data
24-030-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V43374QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V43373
Associated Lab Samples: 95552, 95553, 95554, 95555, 95556, 95558
LRB-V43373 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/07/24 22:3310.01.80<1.80µg/LAcetone
02/07/24 22:330.5000.180<0.180µg/LBenzene
02/07/24 22:330.5000.210<0.210µg/LBromobenzene
02/07/24 22:331.000.420<0.420µg/LBromochloromethane
02/07/24 22:330.5000.160<0.160µg/LBromodichloromethane
02/07/24 22:335.001.50<1.50µg/LBromoform
02/07/24 22:331.000.280<0.280µg/LBromomethane
02/07/24 22:330.5000.180<0.180µg/Ln-Butylbenzene
02/07/24 22:330.5000.200<0.200µg/Lsec-Butyl benzene
02/07/24 22:332.000.920<0.920µg/Ltert-Butyl benzene
02/07/24 22:330.5000.180<0.180µg/LCarbon Tetrachloride
02/07/24 22:330.5000.190<0.190µg/LChlorobenzene
02/07/24 22:330.5000.190<0.190µg/LChlorodibromomethane
02/07/24 22:331.000.430<0.430µg/LChloroethane
02/07/24 22:330.5000.220<0.220µg/LChloroform
02/07/24 22:330.5000.220<0.220µg/LChloromethane
02/07/24 22:330.5000.200<0.200µg/L2-Chlorotoluene
02/07/24 22:330.5000.200<0.200µg/L4-Chlorotoluene
02/07/24 22:330.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
02/07/24 22:332.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
02/07/24 22:330.5000.200<0.200µg/L1,2-Dibromoethane
02/07/24 22:330.5000.230<0.230µg/LDibromomethane
02/07/24 22:330.5000.220<0.220µg/L1,2-Dichlorobenzene
02/07/24 22:330.5000.190<0.190µg/L1,3-Dichlorobenzene
02/07/24 22:330.5000.210<0.210µg/L1,4-Dichlorobenzene
02/07/24 22:335.001.20<1.20µg/LDichlorodifluoromethane
02/07/24 22:330.5000.240<0.240µg/L1,1-Dichloroethane
Page 1 of 13Date:02/13/2024 01:44 PM
Page 59 of 73
Quality Control Data
24-030-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V43374QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V43373
Associated Lab Samples: 95552, 95553, 95554, 95555, 95556, 95558
LRB-V43373 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/07/24 22:330.5000.150<0.150µg/L1,2-Dichloroethane
02/07/24 22:330.5000.150<0.150µg/L1,1-Dichloroethene
02/07/24 22:330.5000.200<0.200µg/Lcis-1,2-Dichloroethene
02/07/24 22:330.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
02/07/24 22:330.5000.190<0.190µg/L1,2-Dichloropropane
02/07/24 22:330.5000.130<0.130µg/L1,3-Dichloropropane
02/07/24 22:332.000.210<0.210µg/L2,2-Dichloropropane
02/07/24 22:330.5000.200<0.200µg/L1,1-Dichloropropene
02/07/24 22:330.5000.210<0.210µg/Lcis-1,3-Dichloropropene
02/07/24 22:330.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
02/07/24 22:3320042.0<42.0µg/LEthanol
02/07/24 22:330.5000.170<0.170µg/LEthylbenzene
02/07/24 22:333.000.350<0.350µg/LHexachlorobutadiene
02/07/24 22:331.000.380<0.380µg/L2-Hexanone
02/07/24 22:330.5000.180<0.180µg/LIsopropylbenzene
02/07/24 22:330.5000.089<0.089µg/L4-Isopropyl toluene
02/07/24 22:335.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
02/07/24 22:331.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
02/07/24 22:331.000.078<0.078µg/L4-Methyl-2-Pentanone
02/07/24 22:332.000.330<0.330µg/LMethylene Chloride
02/07/24 22:331.000.470<0.470µg/LNaphthalene
02/07/24 22:330.5000.190<0.190µg/Ln-Propylbenzene
02/07/24 22:330.5000.220<0.220µg/LStyrene
02/07/24 22:3310.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
02/07/24 22:3310.00.350<0.350µg/Ltert-Butyl formate (TBF)
02/07/24 22:3310.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
02/07/24 22:3310.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 2 of 13Date:02/13/2024 01:44 PM
Page 60 of 73
Quality Control Data
24-030-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V43374QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V43373
Associated Lab Samples: 95552, 95553, 95554, 95555, 95556, 95558
LRB-V43373 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/07/24 22:330.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
02/07/24 22:330.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
02/07/24 22:330.5000.220<0.220µg/LTetrachloroethene
02/07/24 22:330.5000.220<0.220µg/LToluene
02/07/24 22:330.5000.380<0.380µg/L1,2,3-Trichlorobenzene
02/07/24 22:330.5000.310<0.310µg/L1,2,4-Trichlorobenzene
02/07/24 22:330.5000.160<0.160µg/L1,1,1-Trichloroethane
02/07/24 22:330.5000.096<0.096µg/L1,1,2-Trichloroethane
02/07/24 22:330.5000.180<0.180µg/LTrichloroethene
02/07/24 22:330.5000.180<0.180µg/LTrichlorofluoromethane
02/07/24 22:330.5000.270<0.270µg/L1,2,3-Trichloropropane
02/07/24 22:330.5000.190<0.190µg/L1,2,4-Trimethylbenzene
02/07/24 22:330.5000.180<0.180µg/L1,3,5-Trimethylbenzene
02/07/24 22:335.001.00<1.00µg/LVinyl Acetate
02/07/24 22:330.5000.170<0.170µg/LVinyl Chloride
02/07/24 22:330.5000.210<0.210µg/Lo-Xylene
02/07/24 22:331.000.420<0.420µg/Lm,p-Xylene
02/07/24 22:3310.01.00<1.00µg/L3,3-Dimethyl-1-butanol
02/07/24 22:334-Bromofluorobenzene (S)98.6 70-130
02/07/24 22:33Dibromofluoromethane (S)98.0 70-130
02/07/24 22:331,2-Dichloroethane - d4 (S)96.4 70-130
02/07/24 22:33Toluene-d8 (S)101 70-130
Page 3 of 13Date:02/13/2024 01:44 PM
Page 61 of 73
Quality Control Data
24-030-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V43374QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V43373
LCS-V43373 LCSD-V43373Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
48.5 12113051.940.0µg/LAcetone 40-160 6.7 20.0
20.2 10111422.720.0µg/LBenzene 70-130 11.6 20.0
20.2 10111422.820.0µg/LBromobenzene 70-130 12.0 20.0
20.3 10211122.220.0µg/LBromochloromethane 70-130 8.9 20.0
19.9 99.510921.720.0µg/LBromodichloromethane 70-130 8.6 20.0
21.4 10711222.420.0µg/LBromoform 70-130 4.5 20.0
21.7 10911923.820.0µg/LBromomethane 60-140 9.2 20.0
18.8 94.011021.920.0µg/Ln-Butylbenzene 70-130 15.2 20.0
20.2 10111422.720.0µg/Lsec-Butyl benzene 70-130 11.6 20.0
20.3 10211422.820.0µg/Ltert-Butyl benzene 70-130 11.6 20.0
20.1 10111522.920.0µg/LCarbon Tetrachloride 70-130 13.0 20.0
20.2 10111322.520.0µg/LChlorobenzene 70-130 10.7 20.0
20.5 10311322.520.0µg/LChlorodibromomethane 70-130 9.3 20.0
22.4 11212625.220.0µg/LChloroethane 60-140 11.7 20.0
19.6 98.010721.320.0µg/LChloroform 70-130 8.3 20.0
19.2 96.010821.520.0µg/LChloromethane 60-140 11.3 20.0
20.4 10211523.020.0µg/L2-Chlorotoluene 70-130 11.9 20.0
20.7 10411523.020.0µg/L4-Chlorotoluene 70-130 10.5 20.0
21.3 10711623.220.0µg/LDi-Isopropyl Ether (DIPE)70-130 8.5 20.0
24.8 12413025.920.0µg/L1,2-Dibromo-3-Chloropropane 70-130 4.3 20.0
21.3 10711422.720.0µg/L1,2-Dibromoethane 70-130 6.3 20.0
20.3 10211021.920.0µg/LDibromomethane 70-130 7.5 20.0
19.6 98.011222.320.0µg/L1,2-Dichlorobenzene 70-130 12.8 20.0
19.4 97.010921.820.0µg/L1,3-Dichlorobenzene 70-130 11.6 20.0
19.9 99.511222.320.0µg/L1,4-Dichlorobenzene 70-130 11.3 20.0
21.8 10912324.620.0µg/LDichlorodifluoromethane 60-140 12.0 20.0
Page 4 of 13Date:02/13/2024 01:44 PM
Page 62 of 73
Quality Control Data
24-030-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V43374QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V43373
LCS-V43373 LCSD-V43373Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.6 98.010921.720.0µg/L1,1-Dichloroethane 70-130 10.1 20.0
20.1 10110921.720.0µg/L1,2-Dichloroethane 70-130 7.6 20.0
19.2 96.011021.920.0µg/L1,1-Dichloroethene 70-130 13.1 20.0
19.5 97.510921.720.0µg/Lcis-1,2-Dichloroethene 70-130 10.6 20.0
19.2 96.010721.420.0µg/Ltrans-1,2-Dichloroethene 70-130 10.8 20.0
19.5 97.511021.920.0µg/L1,2-Dichloropropane 70-130 11.5 20.0
20.8 10411122.220.0µg/L1,3-Dichloropropane 70-130 6.5 20.0
19.1 95.510721.420.0µg/L2,2-Dichloropropane 70-130 11.3 20.0
19.8 99.011222.320.0µg/L1,1-Dichloropropene 70-130 11.8 20.0
19.6 98.010821.520.0µg/Lcis-1,3-Dichloropropene 70-130 9.2 20.0
20.2 10111122.120.0µg/Ltrans-1,3-Dichloropropene 70-130 8.9 20.0
668 134125625500µg/LEthanol 60-140 6.6 20.0
19.8 99.011222.420.0µg/LEthylbenzene 70-130 12.3 20.0
19.6 98.012024.020.0µg/LHexachlorobutadiene 70-130 20.1*20.0
25.0 12513226.420.0µg/L2-Hexanone 60-140 5.4 20.0
20.0 10011523.020.0µg/LIsopropylbenzene 70-130 13.9 20.0
19.5 97.511022.020.0µg/L4-Isopropyl toluene 70-130 12.0 20.0
23.7 11912525.020.0µg/LMethyl Ethyl Ketone (MEK)60-140 5.3 20.0
21.9 11011723.320.0µg/LMethyl tert-butyl ether (MTBE)70-130 6.1 20.0
24.1 12112424.720.0µg/L4-Methyl-2-Pentanone 60-140 2.4 20.0
19.8 99.010921.820.0µg/LMethylene Chloride 70-130 9.6 20.0
20.3 10211222.420.0µg/LNaphthalene 70-130 9.8 20.0
20.4 10211823.520.0µg/Ln-Propylbenzene 70-130 14.1 20.0
20.3 10211122.220.0µg/LStyrene 70-130 8.9 20.0
38.6 96.599.239.740.0µg/Ltert-Butyl Alcohol (TBA)40-140 2.8 20.0
45.6 11412048.040.0µg/Ltert-Butyl formate (TBF)40-140 5.1 20.0
Page 5 of 13* QC Fail Date:02/13/2024 01:44 PM
Page 63 of 73
Quality Control Data
24-030-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V43374QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V43373
LCS-V43373 LCSD-V43373Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
24.4 12212625.220.0µg/Ltert-Amyl Alcohol (TAA)40-140 3.2 20.0
47.6 11912851.240.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 7.2 20.0
20.3 10211222.420.0µg/L1,1,1,2-Tetrachloroethane 70-130 9.8 20.0
22.4 11211923.720.0µg/L1,1,2,2-Tetrachloroethane 70-130 5.6 20.0
19.6 98.011222.420.0µg/LTetrachloroethene 70-130 13.3 20.0
19.9 99.511222.320.0µg/LToluene 70-130 11.3 20.0
22.6 11312625.220.0µg/L1,2,3-Trichlorobenzene 70-130 10.8 20.0
20.9 10512024.020.0µg/L1,2,4-Trichlorobenzene 70-130 13.8 20.0
19.3 96.510921.820.0µg/L1,1,1-Trichloroethane 70-130 12.1 20.0
20.2 10110921.820.0µg/L1,1,2-Trichloroethane 70-130 7.6 20.0
19.6 98.011122.220.0µg/LTrichloroethene 70-130 12.4 20.0
18.7 93.510721.420.0µg/LTrichlorofluoromethane 60-140 13.4 20.0
22.6 11311823.520.0µg/L1,2,3-Trichloropropane 70-130 3.9 20.0
19.8 99.011122.120.0µg/L1,2,4-Trimethylbenzene 70-130 10.9 20.0
20.0 10011422.720.0µg/L1,3,5-Trimethylbenzene 70-130 12.6 20.0
21.4 10711322.620.0µg/LVinyl Acetate 60-140 5.4 20.0
18.8 94.010621.120.0µg/LVinyl Chloride 60-140 11.5 20.0
20.3 10211322.620.0µg/Lo-Xylene 70-130 10.7 20.0
42.5 10611947.540.0µg/Lm,p-Xylene 70-130 11.1 20.0
27.6 138*138*27.620.0µg/L3,3-Dimethyl-1-butanol 70-130 0.0 20.0
1001024-Bromofluorobenzene (S)70-130
100101Dibromofluoromethane (S)70-130
1021031,2-Dichloroethane - d4 (S)70-130
99.8101Toluene-d8 (S)70-130
Page 6 of 13* QC Fail Date:02/13/2024 01:44 PM
Page 64 of 73
Quality Control Data
24-030-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V43393QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V43392
Associated Lab Samples: 95552, 95556, 95557, 95559, 95560, 95561
LRB-V43392 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/08/24 12:3810.01.80<1.80µg/LAcetone
02/08/24 12:380.5000.180<0.180µg/LBenzene
02/08/24 12:380.5000.210<0.210µg/LBromobenzene
02/08/24 12:381.000.420<0.420µg/LBromochloromethane
02/08/24 12:380.5000.160<0.160µg/LBromodichloromethane
02/08/24 12:385.001.50<1.50µg/LBromoform
02/08/24 12:381.000.280<0.280µg/LBromomethane
02/08/24 12:380.5000.180<0.180µg/Ln-Butylbenzene
02/08/24 12:380.5000.200<0.200µg/Lsec-Butyl benzene
02/08/24 12:382.000.920<0.920µg/Ltert-Butyl benzene
02/08/24 12:380.5000.180<0.180µg/LCarbon Tetrachloride
02/08/24 12:380.5000.190<0.190µg/LChlorobenzene
02/08/24 12:380.5000.190<0.190µg/LChlorodibromomethane
02/08/24 12:381.000.430<0.430µg/LChloroethane
02/08/24 12:380.5000.220<0.220µg/LChloroform
02/08/24 12:380.5000.220<0.220µg/LChloromethane
02/08/24 12:380.5000.200<0.200µg/L2-Chlorotoluene
02/08/24 12:380.5000.200<0.200µg/L4-Chlorotoluene
02/08/24 12:380.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
02/08/24 12:382.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
02/08/24 12:380.5000.200<0.200µg/L1,2-Dibromoethane
02/08/24 12:380.5000.230<0.230µg/LDibromomethane
02/08/24 12:380.5000.220<0.220µg/L1,2-Dichlorobenzene
02/08/24 12:380.5000.190<0.190µg/L1,3-Dichlorobenzene
02/08/24 12:380.5000.210<0.210µg/L1,4-Dichlorobenzene
02/08/24 12:385.001.20<1.20µg/LDichlorodifluoromethane
02/08/24 12:380.5000.240<0.240µg/L1,1-Dichloroethane
Page 7 of 13Date:02/13/2024 01:44 PM
Page 65 of 73
Quality Control Data
24-030-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V43393QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V43392
Associated Lab Samples: 95552, 95556, 95557, 95559, 95560, 95561
LRB-V43392 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/08/24 12:380.5000.150<0.150µg/L1,2-Dichloroethane
02/08/24 12:380.5000.150<0.150µg/L1,1-Dichloroethene
02/08/24 12:380.5000.200<0.200µg/Lcis-1,2-Dichloroethene
02/08/24 12:380.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
02/08/24 12:380.5000.190<0.190µg/L1,2-Dichloropropane
02/08/24 12:380.5000.130<0.130µg/L1,3-Dichloropropane
02/08/24 12:382.000.210<0.210µg/L2,2-Dichloropropane
02/08/24 12:380.5000.200<0.200µg/L1,1-Dichloropropene
02/08/24 12:380.5000.210<0.210µg/Lcis-1,3-Dichloropropene
02/08/24 12:380.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
02/08/24 12:3820042.0<42.0µg/LEthanol
02/08/24 12:380.5000.170<0.170µg/LEthylbenzene
02/08/24 12:383.000.350<0.350µg/LHexachlorobutadiene
02/08/24 12:381.000.380<0.380µg/L2-Hexanone
02/08/24 12:380.5000.180<0.180µg/LIsopropylbenzene
02/08/24 12:380.5000.089<0.089µg/L4-Isopropyl toluene
02/08/24 12:385.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
02/08/24 12:381.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
02/08/24 12:381.000.078<0.078µg/L4-Methyl-2-Pentanone
02/08/24 12:382.000.330<0.330µg/LMethylene Chloride
02/08/24 12:381.000.470<0.470µg/LNaphthalene
02/08/24 12:380.5000.190<0.190µg/Ln-Propylbenzene
02/08/24 12:380.5000.220<0.220µg/LStyrene
02/08/24 12:3810.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
02/08/24 12:3810.00.350<0.350µg/Ltert-Butyl formate (TBF)
02/08/24 12:3810.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
02/08/24 12:3810.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 8 of 13Date:02/13/2024 01:44 PM
Page 66 of 73
Quality Control Data
24-030-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V43393QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V43392
Associated Lab Samples: 95552, 95556, 95557, 95559, 95560, 95561
LRB-V43392 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/08/24 12:380.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
02/08/24 12:380.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
02/08/24 12:380.5000.220<0.220µg/LTetrachloroethene
02/08/24 12:380.5000.220<0.220µg/LToluene
02/08/24 12:380.5000.380<0.380µg/L1,2,3-Trichlorobenzene
02/08/24 12:380.5000.310<0.310µg/L1,2,4-Trichlorobenzene
02/08/24 12:380.5000.160<0.160µg/L1,1,1-Trichloroethane
02/08/24 12:380.5000.096<0.096µg/L1,1,2-Trichloroethane
02/08/24 12:380.5000.180<0.180µg/LTrichloroethene
02/08/24 12:380.5000.180<0.180µg/LTrichlorofluoromethane
02/08/24 12:380.5000.270<0.270µg/L1,2,3-Trichloropropane
02/08/24 12:380.5000.190<0.190µg/L1,2,4-Trimethylbenzene
02/08/24 12:380.5000.180<0.180µg/L1,3,5-Trimethylbenzene
02/08/24 12:385.001.00<1.00µg/LVinyl Acetate
02/08/24 12:380.5000.170<0.170µg/LVinyl Chloride
02/08/24 12:380.5000.210<0.210µg/Lo-Xylene
02/08/24 12:381.000.420<0.420µg/Lm,p-Xylene
02/08/24 12:3810.01.00<1.00µg/L3,3-Dimethyl-1-butanol
02/08/24 12:384-Bromofluorobenzene (S)99.2 70-130
02/08/24 12:38Dibromofluoromethane (S)98.6 70-130
02/08/24 12:381,2-Dichloroethane - d4 (S)98.6 70-130
02/08/24 12:38Toluene-d8 (S)97.8 70-130
Page 9 of 13Date:02/13/2024 01:44 PM
Page 67 of 73
Quality Control Data
24-030-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V43393QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V43392
LCS-V43392 LCSD-V43392Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
43.8 11010240.640.0µg/LAcetone 40-160 7.5 20.0
20.9 10510320.620.0µg/LBenzene 70-130 1.4 20.0
20.8 10410320.620.0µg/LBromobenzene 70-130 0.9 20.0
20.8 10410320.520.0µg/LBromochloromethane 70-130 1.4 20.0
19.8 99.010120.220.0µg/LBromodichloromethane 70-130 2.0 20.0
19.3 96.598.019.620.0µg/LBromoform 70-130 1.5 20.0
24.2 12113627.120.0µg/LBromomethane 60-140 11.3 20.0
20.2 10110220.420.0µg/Ln-Butylbenzene 70-130 0.9 20.0
20.6 10310420.720.0µg/Lsec-Butyl benzene 70-130 0.4 20.0
20.4 10210320.520.0µg/Ltert-Butyl benzene 70-130 0.4 20.0
20.1 10199.019.820.0µg/LCarbon Tetrachloride 70-130 1.5 20.0
20.9 10510420.820.0µg/LChlorobenzene 70-130 0.4 20.0
20.6 10310320.620.0µg/LChlorodibromomethane 70-130 0.0 20.0
23.0 11513627.220.0µg/LChloroethane 60-140 16.7 20.0
20.6 10310320.520.0µg/LChloroform 70-130 0.4 20.0
20.3 10212124.120.0µg/LChloromethane 60-140 17.1 20.0
20.8 10410521.020.0µg/L2-Chlorotoluene 70-130 0.9 20.0
20.6 10310521.020.0µg/L4-Chlorotoluene 70-130 1.9 20.0
21.5 10810821.620.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.4 20.0
21.1 10611021.920.0µg/L1,2-Dibromo-3-Chloropropane 70-130 3.7 20.0
20.1 10110220.420.0µg/L1,2-Dibromoethane 70-130 1.4 20.0
20.7 10410220.420.0µg/LDibromomethane 70-130 1.4 20.0
21.0 10510721.320.0µg/L1,2-Dichlorobenzene 70-130 1.4 20.0
20.8 10410420.720.0µg/L1,3-Dichlorobenzene 70-130 0.4 20.0
20.7 10410320.620.0µg/L1,4-Dichlorobenzene 70-130 0.4 20.0
22.2 11113025.920.0µg/LDichlorodifluoromethane 60-140 15.3 20.0
Page 10 of 13Date:02/13/2024 01:44 PM
Page 68 of 73
Quality Control Data
24-030-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V43393QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V43392
LCS-V43392 LCSD-V43392Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.6 10310320.620.0µg/L1,1-Dichloroethane 70-130 0.0 20.0
20.2 10199.519.920.0µg/L1,2-Dichloroethane 70-130 1.4 20.0
20.5 10310120.220.0µg/L1,1-Dichloroethene 70-130 1.4 20.0
19.6 98.097.019.420.0µg/Lcis-1,2-Dichloroethene 70-130 1.0 20.0
20.5 10310320.520.0µg/Ltrans-1,2-Dichloroethene 70-130 0.0 20.0
20.8 10410220.320.0µg/L1,2-Dichloropropane 70-130 2.4 20.0
20.3 10210220.420.0µg/L1,3-Dichloropropane 70-130 0.4 20.0
21.6 10810721.420.0µg/L2,2-Dichloropropane 70-130 0.9 20.0
21.2 10610520.920.0µg/L1,1-Dichloropropene 70-130 1.4 20.0
21.0 10510420.820.0µg/Lcis-1,3-Dichloropropene 70-130 0.9 20.0
19.9 99.599.019.820.0µg/Ltrans-1,3-Dichloropropene 70-130 0.5 20.0
475 95.095.0475500µg/LEthanol 60-140 0.0 20.0
20.2 10110220.320.0µg/LEthylbenzene 70-130 0.4 20.0
21.1 10610721.320.0µg/LHexachlorobutadiene 70-130 0.9 20.0
20.8 10410220.420.0µg/L2-Hexanone 60-140 1.9 20.0
20.5 10310320.620.0µg/LIsopropylbenzene 70-130 0.4 20.0
20.3 10210220.320.0µg/L4-Isopropyl toluene 70-130 0.0 20.0
21.0 10599.519.920.0µg/LMethyl Ethyl Ketone (MEK)60-140 5.3 20.0
20.7 10410320.520.0µg/LMethyl tert-butyl ether (MTBE)70-130 0.9 20.0
20.7 10410621.120.0µg/L4-Methyl-2-Pentanone 60-140 1.9 20.0
20.8 10410320.620.0µg/LMethylene Chloride 70-130 0.9 20.0
20.0 10010721.320.0µg/LNaphthalene 70-130 6.2 20.0
20.7 10410420.820.0µg/Ln-Propylbenzene 70-130 0.4 20.0
20.3 10210120.220.0µg/LStyrene 70-130 0.4 20.0
33.7 84.286.034.440.0µg/Ltert-Butyl Alcohol (TBA)40-140 2.0 20.0
46.0 11511545.840.0µg/Ltert-Butyl formate (TBF)40-140 0.4 20.0
Page 11 of 13Date:02/13/2024 01:44 PM
Page 69 of 73
Quality Control Data
24-030-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V43393QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V43392
LCS-V43392 LCSD-V43392Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.3 10292.018.420.0µg/Ltert-Amyl Alcohol (TAA)40-140 9.8 20.0
46.1 11511646.240.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 0.2 20.0
20.4 10210020.020.0µg/L1,1,1,2-Tetrachloroethane 70-130 1.9 20.0
19.7 98.599.019.820.0µg/L1,1,2,2-Tetrachloroethane 70-130 0.5 20.0
20.7 10410320.520.0µg/LTetrachloroethene 70-130 0.9 20.0
20.6 10310320.620.0µg/LToluene 70-130 0.0 20.0
22.0 11012424.820.0µg/L1,2,3-Trichlorobenzene 70-130 11.9 20.0
21.8 10911422.720.0µg/L1,2,4-Trichlorobenzene 70-130 4.0 20.0
20.4 10210120.120.0µg/L1,1,1-Trichloroethane 70-130 1.4 20.0
20.3 10210320.620.0µg/L1,1,2-Trichloroethane 70-130 1.4 20.0
20.5 10310220.320.0µg/LTrichloroethene 70-130 0.9 20.0
20.1 10111322.520.0µg/LTrichlorofluoromethane 60-140 11.2 20.0
19.8 99.098.019.620.0µg/L1,2,3-Trichloropropane 70-130 1.0 20.0
20.0 10010320.520.0µg/L1,2,4-Trimethylbenzene 70-130 2.4 20.0
20.2 10110220.420.0µg/L1,3,5-Trimethylbenzene 70-130 0.9 20.0
20.6 10311422.720.0µg/LVinyl Acetate 60-140 9.6 20.0
19.9 99.511422.720.0µg/LVinyl Chloride 60-140 13.1 20.0
20.8 10410320.620.0µg/Lo-Xylene 70-130 0.9 20.0
43.3 10810843.340.0µg/Lm,p-Xylene 70-130 0.0 20.0
15.2 76.010320.520.0µg/L3,3-Dimethyl-1-butanol 70-130 29.6*20.0
99.299.64-Bromofluorobenzene (S)70-130
96.697.4Dibromofluoromethane (S)70-130
98.898.21,2-Dichloroethane - d4 (S)70-130
10099.4Toluene-d8 (S)70-130
Page 12 of 13* QC Fail Date:02/13/2024 01:44 PM
Page 70 of 73
Quality Control Data
24-030-0017Report No:
Project Description:
Client ID:Geological Resources, Inc.
Ganesha
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V43494QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V43493
Associated Lab Samples: 95555, 95559, 95560
LRB-V43493 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/09/24 14:260.5000.180<0.180µg/LBenzene
02/09/24 14:2620042.0<42.0µg/LEthanol
02/09/24 14:2610.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
02/09/24 14:260.5000.220<0.220µg/LToluene
02/09/24 14:264-Bromofluorobenzene (S)103 70-130
02/09/24 14:26Dibromofluoromethane (S)95.0 70-130
02/09/24 14:261,2-Dichloroethane - d4 (S)92.0 70-130
02/09/24 14:26Toluene-d8 (S)102 70-130
LCS-V43493 LCSD-V43493Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.3 10710821.620.0µg/LBenzene 70-130 1.3 20.0
628 126118590500µg/LEthanol 60-140 6.2 20.0
23.2 11692.518.520.0µg/Ltert-Amyl Alcohol (TAA)40-140 22.5*20.0
21.0 10510721.420.0µg/LToluene 70-130 1.8 20.0
1011024-Bromofluorobenzene (S)70-130
95.894.8Dibromofluoromethane (S)70-130
96.494.21,2-Dichloroethane - d4 (S)70-130
99.4102Toluene-d8 (S)70-130
Page 13 of 13* QC Fail Date:02/13/2024 01:44 PM
Page 71 of 73
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:24-030-0017
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 3.9C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:01/30/2024 17:14:41
Special precautions or instructions included?
Comments:
Page 72 of 73
Page 73 of 73

APPENDIX H
Mass Contaminant Calculations
0.00
2.00
4.00
6.00
8.00
10.00
12.00
0
10,000
20,000
30,000
40,000
50,000
60,000
70,000
80,000
90,000
100,000
Wa
t
e
r

C
o
l
u
m
n

H
e
i
g
h
t
s

(
f
t
)
Co
n
t
a
m
i
n
a
n
t

M
a
s
s

(
g
r
a
m
s
)
Time
Total Contaminant Mass vs. Time
Ganesha Food Mart (Incident No. 40741)
Total Contaminant Mass (g)Water Column Heights (ft)Linear (Total Contaminant Mass (g))
Area ID Well IDs Area (ft²)Average Well
Depth
(ft.)
Average
Depth to
Water
(ft.)
Water Column
Height (ft)Volume (ft³) Volume (L)Effective
Porosity
Effective
Volume (L)
GMW-1
GMW-2
GMW-3
GMW-4
MMPE-2
MMPE-3
MW-18
MW-21
Area Date Well Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Total DTW
Average Water
Column Height
(ft.)
Total Average
Mass (g)Percent Red. To Date Red.
MW-18 6,590 26,300 3,400 17,400 1,040 1,030 55,760.00 25.07
MW-21 26,500 34,400 3,220 16,000 298 J 930 81,050.00 25.31
Avg. 16,545.00 30,350.00 3,310.00 16,700.00 520.00 980.00 68,405.00 25.19
MW-18 3,420 17,100 2,910 14,300 544 1,430 39,704.00 24.66
MW-21 30,300 34,300 3,490 16,300 249 1,190 85,829.00 25.91
Avg. 16,860.00 25,700.00 3,200.00 15,300.00 396.50 1,310.00 62,766.50 25.29
MW-18 808 4,700 760 4,190 198 496 11,152.00 23.87
MW-21 24,600 37,600 3,180 17,200 183 1,100 83,863.00 24.10
Avg. 12,704.00 21,150.00 1,970.00 10,695.00 190.50 798.00 47,507.50 23.99
MW-18 3,170 15,100 2,250 11,500 401 750 33,171.00 23.46
MW-21 27,700 38,800 3,740 17,700 248 1,140 89,328.00 23.69
Avg. 15,435.00 26,950.00 2,995.00 14,600.00 324.50 945.00 61,249.50 23.58
GMW-1 3,890 14,100 1,730 10,800 103 1,420 32043.00 14.50
GMW-2 5,000 260,000 80,000 50,000 20,000 6,000 421000.00 14.67
GMW-3 5,000 260,000 80,000 50,000 20,000 6,000 421000.00 14.95
GMW-4 5,000 260,000 80,000 50,000 20,000 6,000 421000.00 14.73
MMPE-2 0.663 8.76 4.17 34.0 0 23.1 70.69 14.73
MMPE-3 0.00 0.00 0.00 0.00 0.00 0.00 0.00 14.73
Avg. 3148.44 132351.46 40289.03 26805.67 10017.17 3240.52 215852.28 14.72
GMW-1 5,560 22,200 2,550 13,500 98.0 2,860 46768.00 15.21
GMW-2 5,000 260,000 80,000 50,000 20,000 6,000 421000.00 15.35
GMW-3 5,000 260,000 80,000 50,000 20,000 6,000 421000.00 15.66
GMW-4 5,000 260,000 80,000 50,000 20,000 6,000 421000.00 14.92
MMPE-2 0.663 8.76 4.17 34.0 0 23.1 70.69 15.92
MMPE-3 0.00 0.00 0.00 0.00 0.00 0.00 0.00 15.92
Avg. 3426.78 133701.46 40425.70 27255.67 10016.33 3480.52 218306.45 15.50
391,0800.20
12/08/22 6.72 6,297.34 9.5%
Area A 6,871.09 24 13.95 10.05 69,054 1,955,401
12/08/22 8.50 72,236.31 7.3% 7.3%
8.43 7,710.03 -35.5%-10.8%
Area A
12/01/21 9.28 77,961.90 --- ---
6.81 6,960.15 ------
05/18/23 8.02 5,689.17 9.7% 18.3%
9.5%
21,396 605,863 121,173
Area B
12/01/21
01/30/24
APPENDIX
CONTAMINANT MASS CALCULATIONS
GANESHA FOOD MART (Incident No. 40741)
Baseline Event
0.20Area B 2,638.21 32 23.89 8.11
Page 1 of 3
Area ID Well IDs Area (ft²)Average Well
Depth
(ft.)
Average
Depth to
Water
(ft.)
Water Column
Height (ft)Volume (ft³) Volume (L)Effective
Porosity
Effective
Volume (L)
GMW-1
GMW-2
GMW-3
GMW-4
MMPE-2
MMPE-3
MW-18
MW-21
Area Date Well Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Total DTW
Average Water
Column Height
(ft.)
Total Average
Mass (g)Percent Red. To Date Red.
391,0800.20Area A 6,871.09 24 13.95 10.05 69,054 1,955,401
21,396 605,863 121,173
APPENDIX
CONTAMINANT MASS CALCULATIONS
GANESHA FOOD MART (Incident No. 40741)
Baseline Event
0.20Area B 2,638.21 32 23.89 8.11
GMW-1 3,820 15,900 2,000 10,300 62 1,940 34022.20 12.46
GMW-2 1,260 5,490 1,410 7,980 0 1,000 17140.00 12.58
GMW-3 8,260 29,300 3,550 18,900 0 1,220 61230.00 13.02
GMW-4 5,000 260,000 80,000 50,000 20,000 6,000 421000.00 13.02
MMPE-2 0 0 0 0 0 0 0.00 13.25
MMPE-3 0 0 0 0 0 0 0.00 12.83
Avg. 3056.67 51781.67 14493.33 14530.00 3343.70 1693.33 88898.70 12.86
GMW-1 3,200 13,700 2,060 11,300 88.5 1,130 31478.50 13.73
GMW-2 941 4,030 1,520 7,960 0 601 13.98
GMW-3 1,430 8,280 1,940 13,300 39.3 720 14.51
GMW-4 4,100 8,460 1,220 7,020 81.1 266 21147.10 14.11
MMPE-2 81.4 46.7 10.6 156 2.33 4.24 301.27 14.45
MMPE-3 0 0.399 0.222 1.42 0 0 2.04 14.13
Avg. 1625.40 5752.85 1125.14 6622.90 35.21 453.54 15615.04 14.15
01/30/24 9.85 5,984.19 84.5% 92.3%
05/18/23 11.14 38,537.22 46.7% 50.6%
Area A
Page 2 of 3
Area ID Well IDs Area (ft²)Average Well
Depth
(ft.)
Average
Depth to
Water
(ft.)
Water Column
Height (ft)Volume (ft³) Volume (L)Effective
Porosity
Effective
Volume (L)
GMW-1
GMW-2
GMW-3
GMW-4
MMPE-2
MMPE-3
MW-18
MW-21
Area Date Well Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Total DTW
Average Water
Column Height
(ft.)
Total Average
Mass (g)Percent Red. To Date Red.
391,0800.20Area A 6,871.09 24 13.95 10.05 69,054 1,955,401
21,396 605,863 121,173
APPENDIX
CONTAMINANT MASS CALCULATIONS
GANESHA FOOD MART (Incident No. 40741)
Baseline Event
0.20Area B 2,638.21 32 23.89 8.11
Date
Average Water
Column Height
(ft.)
Percent Change To Date
12/01/21 8.05
12/08/22 7.61
05/18/23 9.58
01/30/24 9.14
Notes:
• FP: Free Product
• Area of the contaminant plume is calculated from Figure 6.
• Height of the water column is calculated by subtracting the average depth to water from the average well depth of the referenced monitoring wells
• Volume of the contaminant plume is calculated by multiplying the area of the plume by the average height of the water column during each sampling event
• Effective porosity is assumed based on the sub-surface soil profile obtained from well construction records and soil boring logs
• Total mass was calculated by multiplying the total contaminant concentrations for the sampling event with effective volume
• Contaminant mass cannot be calculated in wells containing FP; therefore, the total contaminant mass is based on the known concentrations in the area for each sampling event.
• When areas couldn’t be sampled, the last known concentrations were used in the calculations.
44,226 43.7%48%
13,694 69.0%84%
Total Contaminant Mass (g)Percent Change Compared to
Previous Event
84,922 ------
78,534 7.5%8%
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