WS-8938_44182_CA_MRP_20221122

Sample OE1 OE2 OE3 OE4 OE5 OE6 OE7 OE8 OE9 OE10 OE11 OE12Sample Depth (feet bgs)22 14 13 15 15 13 13 11 12 18 9 10DateEPA 8260 b (ppm)Benzene BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL 5.61 6.33 0.0056 164N-Butylbenzene 2.27 BQL BQL BQL BQL BQL BQL BQL BQL 4.18 16.4 18.6 4.3 16,350Sec-Butylbenzene 1.04 BQL BQL BQL BQL BQL BQL BQL BQL 2.17J 7.60 8.88 3.3 16,350Ethylbenzene 2.16 BQL BQL BQL BQL BQL BQL BQL BQL 17.3 125 150 4.9 40,000I-Propylbenzene 0.951 BQL BQL BQL BQL BQL BQL BQL BQL 3.90 18.0 21.8 1.7 40,880p-Isopropyltoluene 0.597 0.001 J BQL BQL BQL BQL 0.001J BQL BQL 0.966J 3.29J 4.03 0.12 4,000Methyl Tert-butyl Ether (MTBE)BQL BQL BQL BQL BQL BQL 0.039 0.004J BQL BQL BQL BQL 0.091 3,100Naphthalene13.60 0.176 BQL 0.002J BQL 0.004J 0.033 0.003J 0.003J 13.5 46.2 54.2 0.16 8,176N-Propylbenzene 4.14 BQL BQL BQL BQL BQL BQL BQL BQL 14.9 63.9 77.8 1.7 16,350Toluene 1.06 BQL BQL BQL BQL BQL 0.002J 0.001J BQL 17.7 273 384 4.3 32,0001,2,4-Trimethylbenzene 37.60 0.018 BQL BQL BQL BQL 0.004J 0.004J BQL 101 414 476 8.5 20,4401,3,5-Trimethylbenzene 11.10 0.005 BQL BQL BQL BQL 0.002J 0.002J BQL 29.3 120 156 8.3 20,440Xylenes (Total)18.00 0.001J BQL BQL BQL BQL 0.002J 0.001J BQL 108 729 935 4.6 81,760remaining compounds BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL na naMADEP VPH (ppm)
C5-C8 Aliphatics 3838 BQL BQL BQL BQL BQL BQL BQL BQL 229 1880 1660 68 24,528
C9-C12 Aliphatics 365 BQL BQL BQL BQL BQL BQL BQL BQL 869 4590 4000 540 40,000
C9-C10 Aromatics 190 BQL BQL BQL BQL BQL BQL BQL BQL 390 1900 1620 31 12,264
Soil-to-GW
MSCC
Industrial/Commercial
Cleanup Levels7/15/13 7/18/13
Sample OE1 OE2 OE3 OE4 OE5 OE6 OE7 OE8 OE9 OE10 OE11 OE12Sample Depth (feet bgs)22 14 13 15 15 13 13 11 12 18 9 10
Date
EPA 8260 b (ppm)
Benzene BQLBQLBQLBQLBQLBQLBQLBQLBQLBQL5.61 6.33 0.0056 18 164
N-Butylbenzene 2.27 BQLBQLBQLBQLBQLBQLBQLBQL4.18 16.4 18.6 4.3 626 16,350Sec-Butylbenzene 1.04 BQLBQLBQLBQLBQLBQLBQLBQL2.17J 7.60 8.88 3.3 626 16,350
Ethylbenzene 2.16 BQLBQLBQLBQLBQLBQLBQLBQL17.3 125 150 4.9 1560 40,000
I-Propylbenzene 0.951 BQLBQLBQLBQLBQLBQLBQLBQL3.90 18.0 21.8 1.7 1564 40,880
p-Isopropyltoluene 0.597 0.001 J BQL BQL BQL BQL 0.001J BQL BQL 0.966J 3.29J 4.03 0.12 100 4,000
Methyl Tert-butyl Ether (MTBE)BQL BQL BQL BQL BQL BQL 0.039 0.004J BQL BQL BQL BQL 0.091 350 3,100
Naphthalene 13.60 0.176 BQL 0.002J BQL 0.004J 0.033 0.003J 0.003J 13.5 46.2 54.2 0.16 313 8,176
N-Propylbenzene 4.14 BQLBQLBQLBQLBQLBQLBQLBQL14.9 63.9 77.8 1.7 626 16,350Toluene 1.06 BQL BQL BQL BQL BQL 0.002J 0.001J BQL 17.7 273 384 4.3 1200 32,0001,2,4-Trimethylbenzene 37.60 0.018 BQL BQL BQL BQL 0.004J 0.004J BQL 101 414 476 8.5 782 20,440
1,3,5-Trimethylbenzene 11.10 0.005 BQL BQL BQL BQL 0.002J 0.002J BQL 29.3 120 156 8.3 782 20,440
Xylenes (Total)18.00 0.001J BQL BQL BQL BQL 0.002J 0.001J BQL 108 729 935 4.6 3129 81,760
remaining compounds BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQL na na na
MADEP VPH (ppm)
C5-C8 Aliphatics 3838 BQLBQLBQLBQLBQLBQLBQLBQL229 1880 1660 68 939 24,528
C9-C12 Aliphatics 365 BQLBQLBQLBQLBQLBQLBQLBQL869 4590 4000 540 1,500 40,000
C9-C10 Aromatics 190 BQLBQLBQLBQLBQLBQLBQLBQL390 1900 1620 31 469 12,264
Soil-to-GW
MSCC
Industrial/Commercial
Cleanup Levels7/15/13 7/18/13
Residential
Soil Cleanup
Levels
Sample OE1 OE2 OE3 OE4 OE5 OE6 OE7 OE8 OE9 OE10 OE11 OE12
Sample Depth (feet bgs)22 14 13 15 15 13 13 11 12 18 9 10
Date
EPA 8260 b (ppm)
Benzene BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL 5.61 6.33 0.0056 164
N-Butylbenzene 2.27 BQL BQL BQL BQL BQL BQL BQL BQL 4.18 16.4 18.6 4.3 16,350
Sec-Butylbenzene 1.04 BQL BQL BQL BQL BQL BQL BQL BQL 2.17J 7.60 8.88 3.3 16,350
Ethylbenzene 2.16 BQL BQL BQL BQL BQL BQL BQL BQL 17.3 125 150 4.9 40,000
I-Propylbenzene 0.951 BQL BQL BQL BQL BQL BQL BQL BQL 3.90 18.0 21.8 1.7 40,880
p-Isopropyltoluene 0.597 0.001 J BQL BQL BQL BQL 0.001J BQL BQL 0.966J 3.29J 4.03 0.12 4,000
Methyl Tert-butyl Ether (MTBE)BQL BQL BQL BQL BQL BQL 0.039 0.004J BQL BQL BQL BQL 0.091 3,100
Naphthalene 13.60 0.176 BQL 0.002J BQL 0.004J 0.033 0.003J 0.003J 13.5 46.2 54.2 0.16 8,176
N-Propylbenzene 4.14 BQL BQL BQL BQL BQL BQL BQL BQL 14.9 63.9 77.8 1.7 16,350Toluene 1.06 BQL BQL BQL BQL BQL 0.002J 0.001J BQL 17.7 273 384 4.3 32,0001,2,4-Trimethylbenzene 37.60 0.018 BQL BQL BQL BQL 0.004J 0.004J BQL 101 414 476 8.5 20,4401,3,5-Trimethylbenzene 11.10 0.005 BQL BQL BQL BQL 0.002J 0.002J BQL 29.3 120 156 8.3 20,440Xylenes (Total)18.00 0.001J BQL BQL BQL BQL 0.002J 0.001J BQL 108 729 935 4.6 81,760remaining compounds BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL na naMADEP VPH (ppm)C5-C8 Aliphatics 3838 BQL BQL BQL BQL BQL BQL BQL BQL 229 1880 1660 68 24,528C9-C12 Aliphatics 365 BQL BQL BQL BQL BQL BQL BQL BQL 869 4590 4000 540 40,000C9-C10 Aromatics 190 BQL BQL BQL BQL BQL BQL BQL BQL 390 1900 1620 31 12,264
Soil-to-GW
MSCC
Industrial/Commercial
Cleanup Levels7/15/13 7/18/13
Sample OE1 OE2 OE3 OE4 OE5 OE6 OE7 OE8 OE9 OE10 OE11 OE12
Sample Depth (feet bgs)22 14 13 15 15 13 13 11 12 18 9 10
Date
EPA 8260 b (ppm)
Benzene BQLBQLBQLBQLBQLBQLBQLBQLBQLBQL5.61 6.33 0.0056 18 164N-Butylbenzene 2.27 BQLBQLBQLBQLBQLBQLBQLBQL4.18 16.4 18.6 4.3 626 16,350
Sec-Butylbenzene 1.04 BQLBQLBQLBQLBQLBQLBQLBQL2.17J 7.60 8.88 3.3 626 16,350
Ethylbenzene 2.16 BQLBQLBQLBQLBQLBQLBQLBQL17.3 125 150 4.9 1560 40,000
I-Propylbenzene 0.951 BQLBQLBQLBQLBQLBQLBQLBQL3.90 18.0 21.8 1.7 1564 40,880
p-Isopropyltoluene 0.597 0.001 J BQL BQL BQL BQL 0.001J BQL BQL 0.966J 3.29J 4.03 0.12 100 4,000
Methyl Tert-butyl Ether (MTBE)BQL BQL BQL BQL BQL BQL 0.039 0.004J BQL BQL BQL BQL 0.091 350 3,100
Naphthalene 13.60 0.176 BQL 0.002J BQL 0.004J 0.033 0.003J 0.003J 13.5 46.2 54.2 0.16 313 8,176N-Propylbenzene 4.14 BQLBQLBQLBQLBQLBQLBQLBQL14.9 63.9 77.8 1.7 626 16,350Toluene 1.06 BQL BQL BQL BQL BQL 0.002J 0.001J BQL 17.7 273 384 4.3 1200 32,000
1,2,4-Trimethylbenzene 37.60 0.018 BQL BQL BQL BQL 0.004J 0.004J BQL 101 414 476 8.5 782 20,440
1,3,5-Trimethylbenzene 11.10 0.005 BQL BQL BQL BQL 0.002J 0.002J BQL 29.3 120 156 8.3 782 20,440
Xylenes (Total)18.00 0.001J BQL BQL BQL BQL 0.002J 0.001J BQL 108 729 935 4.6 3129 81,760
remaining compounds BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQL na na na
MADEP VPH (ppm)
C5-C8 Aliphatics 3838 BQLBQLBQLBQLBQLBQLBQLBQL229 1880 1660 68 939 24,528
C9-C12 Aliphatics 365 BQLBQLBQLBQLBQLBQLBQLBQL869 4590 4000 540 1,500 40,000
C9-C10 Aromatics 190 BQLBQLBQLBQLBQLBQLBQLBQL390 1900 1620 31 469 12,264
Soil-to-GW
MSCC
Industrial/Commercial
Cleanup Levels7/15/13 7/18/13
Residential
Soil Cleanup
Levels
#=CL#
November 11, 2022
LIMS USE: FR - MATT (AP)
LIMS OBJECT ID: 92633465
92633465
Project:
Pace Project No.:
RE:
Matt Scheidt (AP)
Northwest Geoscience
P.O. Box 6418
High Point, NC 27262
Konnoak Texaco #13-111
Dear Matt (AP):
Enclosed are the analytical results for sample(s) received by the laboratory on October 28, 2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stephanie Knott
[e-mail]
Project Manager
704-977-0981
Enclosures
cc:Barry Nelson
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 1 of 53
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 2 of 53
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Lab ID Sample ID Matrix Date Collected Date Received
92633465001 MW-1 Water 10/26/22 10:00 10/28/22 10:10
92633465002 MW-2 Water 10/27/22 10:00 10/28/22 10:10
92633465003 MW-3 Water 10/27/22 10:30 10/28/22 10:10
92633465004 MW-4 Water 10/27/22 11:00 10/28/22 10:10
92633465005 MW-5 Water 10/27/22 11:30 10/28/22 10:10
92633465006 MW-6 Water 10/26/22 10:30 10/28/22 10:10
92633465007 MW-7 Water 10/26/22 11:00 10/28/22 10:10
92633465008 MW-8 Water 10/27/22 12:00 10/28/22 10:10
92633465009 MW-9 Water 10/27/22 12:30 10/28/22 10:10
92633465010 MW-10 Water 10/26/22 11:30 10/28/22 10:10
92633465011 MW-11 Water 10/27/22 13:00 10/28/22 10:10
92633465012 MW-12 Water 10/27/22 13:30 10/28/22 10:10
92633465013 MW-14 Water 10/26/22 12:00 10/28/22 10:10
92633465014 MW-15 Water 10/26/22 12:30 10/28/22 10:10
92633465015 TW-1 Water 10/26/22 13:00 10/28/22 10:10
92633465016 DW-1 Water 10/26/22 13:30 10/28/22 10:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 3 of 53
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92633465001 MW-1 SM 6200B 69 PASI-CSAS
92633465002 MW-2 SM 6200B 69 PASI-CSAS
92633465003 MW-3 SM 6200B 69 PASI-CSAS
92633465004 MW-4 SM 6200B 69 PASI-CSAS
92633465005 MW-5 SM 6200B 69 PASI-CSAS
92633465006 MW-6 SM 6200B 69 PASI-CSAS
92633465007 MW-7 SM 6200B 69 PASI-CSAS
92633465008 MW-8 SM 6200B 69 PASI-CSAS
92633465009 MW-9 SM 6200B 69 PASI-CSAS
92633465010 MW-10 SM 6200B 69 PASI-CSAS
92633465011 MW-11 SM 6200B 69 PASI-CSAS
92633465012 MW-12 SM 6200B 69 PASI-CSAS
92633465013 MW-14 SM 6200B 69 PASI-CSAS
92633465014 MW-15 SM 6200B 69 PASI-CSAS
92633465015 TW-1 SM 6200B 69 PASI-CSAS
92633465016 DW-1 SM 6200B 69 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 4 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-1 Lab ID:92633465001 Collected:10/26/22 10:00 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/09/22 16:01 75-85-4500050
tert-Amylmethyl ether ND ug/L 11/09/22 16:01 994-05-850050
Benzene 6020 ug/L 11/09/22 16:01 71-43-225.0 50
Bromobenzene ND ug/L 11/09/22 16:01 108-86-125.0 50
Bromochloromethane ND ug/L 11/09/22 16:01 74-97-525.0 50
Bromodichloromethane ND ug/L 11/09/22 16:01 75-27-425.0 50
Bromoform ND ug/L 11/09/22 16:01 75-25-225.0 50
Bromomethane ND ug/L 11/09/22 16:01 74-83-925050
tert-Butyl Alcohol ND ug/L 11/09/22 16:01 75-65-0250050
n-Butylbenzene ND ug/L 11/09/22 16:01 104-51-825.0 50
sec-Butylbenzene ND ug/L 11/09/22 16:01 135-98-825.0 50
tert-Butylbenzene ND ug/L 11/09/22 16:01 98-06-625.0 50
tert-Butyl Formate ND ug/L 11/09/22 16:01 762-75-4250050
Carbon tetrachloride ND ug/L 11/09/22 16:01 56-23-525.0 50
Chlorobenzene ND ug/L 11/09/22 16:01 108-90-725.0 50
Chloroethane ND ug/L 11/09/22 16:01 75-00-350.0 50
Chloroform ND ug/L 11/09/22 16:01 67-66-325.0 50
Chloromethane ND ug/L 11/09/22 16:01 74-87-350.0 50
2-Chlorotoluene ND ug/L 11/09/22 16:01 95-49-825.0 50
4-Chlorotoluene ND ug/L 11/09/22 16:01 106-43-425.0 50
1,2-Dibromo-3-chloropropane ND ug/L 11/09/22 16:01 96-12-850.0 50
Dibromochloromethane ND ug/L 11/09/22 16:01 124-48-125.0 50
1,2-Dibromoethane (EDB)ND ug/L 11/09/22 16:01 106-93-425.0 50
Dibromomethane ND ug/L 11/09/22 16:01 74-95-325.0 50
1,2-Dichlorobenzene ND ug/L 11/09/22 16:01 95-50-125.0 50
1,3-Dichlorobenzene ND ug/L 11/09/22 16:01 541-73-125.0 50
1,4-Dichlorobenzene ND ug/L 11/09/22 16:01 106-46-725.0 50
Dichlorodifluoromethane ND ug/L 11/09/22 16:01 75-71-825.0 50
1,1-Dichloroethane ND ug/L 11/09/22 16:01 75-34-325.0 50
1,2-Dichloroethane ND ug/L 11/09/22 16:01 107-06-225.0 50
1,1-Dichloroethene ND ug/L 11/09/22 16:01 75-35-425.0 50
cis-1,2-Dichloroethene ND ug/L 11/09/22 16:01 156-59-225.0 50
trans-1,2-Dichloroethene ND ug/L 11/09/22 16:01 156-60-525.0 50
1,2-Dichloropropane ND ug/L 11/09/22 16:01 78-87-525.0 50
1,3-Dichloropropane ND ug/L 11/09/22 16:01 142-28-925.0 50
2,2-Dichloropropane ND ug/L 11/09/22 16:01 594-20-725.0 50
1,1-Dichloropropene ND ug/L 11/09/22 16:01 563-58-625.0 50
cis-1,3-Dichloropropene ND ug/L 11/09/22 16:01 10061-01-525.0 50
trans-1,3-Dichloropropene ND ug/L 11/09/22 16:01 10061-02-625.0 50
Diisopropyl ether ND ug/L 11/09/22 16:01 108-20-325.0 50
Ethanol ND ug/L 11/09/22 16:01 64-17-51000050
Ethylbenzene 5310 ug/L 11/09/22 16:01 100-41-425.0 50
Ethyl-tert-butyl ether ND ug/L 11/09/22 16:01 637-92-350050
Hexachloro-1,3-butadiene ND ug/L 11/09/22 16:01 87-68-310050
Isopropylbenzene (Cumene)236 ug/L 11/09/22 16:01 98-82-825.0 50
Methylene Chloride ND ug/L 11/09/22 16:01 75-09-210050
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 5 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-1 Lab ID:92633465001 Collected:10/26/22 10:00 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether 41.7 ug/L 11/09/22 16:01 1634-04-425.0 50
Naphthalene 628 ug/L 11/09/22 16:01 91-20-310050
n-Propylbenzene ND ug/L 11/09/22 16:01 103-65-125.0 50
Styrene ND ug/L 11/09/22 16:01 100-42-525.0 50
1,1,1,2-Tetrachloroethane ND ug/L 11/09/22 16:01 630-20-625.0 50
1,1,2,2-Tetrachloroethane ND ug/L 11/09/22 16:01 79-34-525.0 50
Tetrachloroethene ND ug/L 11/09/22 16:01 127-18-425.0 50
Toluene 80700 ug/L 11/10/22 11:08 108-88-3 H1,H5250500
1,2,3-Trichlorobenzene ND ug/L 11/09/22 16:01 87-61-610050
1,2,4-Trichlorobenzene ND ug/L 11/09/22 16:01 120-82-110050
1,1,1-Trichloroethane ND ug/L 11/09/22 16:01 71-55-625.0 50
1,1,2-Trichloroethane ND ug/L 11/09/22 16:01 79-00-525.0 50
Trichloroethene ND ug/L 11/09/22 16:01 79-01-625.0 50
Trichlorofluoromethane ND ug/L 11/09/22 16:01 75-69-450.0 50
1,2,3-Trichloropropane ND ug/L 11/09/22 16:01 96-18-425.0 50
1,2,4-Trimethylbenzene 4230 ug/L 11/09/22 16:01 95-63-625.0 50
1,3,5-Trimethylbenzene ND ug/L 11/09/22 16:01 108-67-825.0 50
Vinyl chloride ND ug/L 11/09/22 16:01 75-01-450.0 50
m&p-Xylene 17300 ug/L 11/09/22 16:01 179601-23-150.0 50
o-Xylene 8850 ug/L 11/09/22 16:01 95-47-625.0 50
Surrogates
1,2-Dichloroethane-d4 (S)88 %11/09/22 16:01 17060-07-070-130 50
4-Bromofluorobenzene (S)95 %11/09/22 16:01 460-00-470-130 50
Toluene-d8 (S)98 %11/09/22 16:01 2037-26-570-130 50
Sample:MW-2 Lab ID:92633465002 Collected:10/27/22 10:00 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/10/22 16:22 75-85-4200020
tert-Amylmethyl ether ND ug/L 11/10/22 16:22 994-05-820020
Benzene 95.1 ug/L 11/10/22 16:22 71-43-210.0 20
Bromobenzene ND ug/L 11/10/22 16:22 108-86-110.0 20
Bromochloromethane ND ug/L 11/10/22 16:22 74-97-510.0 20
Bromodichloromethane ND ug/L 11/10/22 16:22 75-27-410.0 20
Bromoform ND ug/L 11/10/22 16:22 75-25-210.0 20
Bromomethane ND ug/L 11/10/22 16:22 74-83-910020
tert-Butyl Alcohol ND ug/L 11/10/22 16:22 75-65-0100020
n-Butylbenzene ND ug/L 11/10/22 16:22 104-51-810.0 20
sec-Butylbenzene ND ug/L 11/10/22 16:22 135-98-810.0 20
tert-Butylbenzene ND ug/L 11/10/22 16:22 98-06-610.0 20
tert-Butyl Formate ND ug/L 11/10/22 16:22 762-75-4100020
Carbon tetrachloride ND ug/L 11/10/22 16:22 56-23-510.0 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 6 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-2 Lab ID:92633465002 Collected:10/27/22 10:00 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Chlorobenzene ND ug/L 11/10/22 16:22 108-90-710.0 20
Chloroethane ND ug/L 11/10/22 16:22 75-00-320.0 20
Chloroform ND ug/L 11/10/22 16:22 67-66-310.0 20
Chloromethane ND ug/L 11/10/22 16:22 74-87-320.0 20
2-Chlorotoluene ND ug/L 11/10/22 16:22 95-49-810.0 20
4-Chlorotoluene ND ug/L 11/10/22 16:22 106-43-410.0 20
1,2-Dibromo-3-chloropropane ND ug/L 11/10/22 16:22 96-12-820.0 20
Dibromochloromethane ND ug/L 11/10/22 16:22 124-48-110.0 20
1,2-Dibromoethane (EDB)ND ug/L 11/10/22 16:22 106-93-410.0 20
Dibromomethane ND ug/L 11/10/22 16:22 74-95-310.0 20
1,2-Dichlorobenzene ND ug/L 11/10/22 16:22 95-50-110.0 20
1,3-Dichlorobenzene ND ug/L 11/10/22 16:22 541-73-110.0 20
1,4-Dichlorobenzene ND ug/L 11/10/22 16:22 106-46-710.0 20
Dichlorodifluoromethane ND ug/L 11/10/22 16:22 75-71-810.0 20
1,1-Dichloroethane ND ug/L 11/10/22 16:22 75-34-310.0 20
1,2-Dichloroethane ND ug/L 11/10/22 16:22 107-06-210.0 20
1,1-Dichloroethene ND ug/L 11/10/22 16:22 75-35-410.0 20
cis-1,2-Dichloroethene ND ug/L 11/10/22 16:22 156-59-210.0 20
trans-1,2-Dichloroethene ND ug/L 11/10/22 16:22 156-60-510.0 20
1,2-Dichloropropane ND ug/L 11/10/22 16:22 78-87-510.0 20
1,3-Dichloropropane ND ug/L 11/10/22 16:22 142-28-910.0 20
2,2-Dichloropropane ND ug/L 11/10/22 16:22 594-20-710.0 20
1,1-Dichloropropene ND ug/L 11/10/22 16:22 563-58-610.0 20
cis-1,3-Dichloropropene ND ug/L 11/10/22 16:22 10061-01-510.0 20
trans-1,3-Dichloropropene ND ug/L 11/10/22 16:22 10061-02-610.0 20
Diisopropyl ether ND ug/L 11/10/22 16:22 108-20-310.0 20
Ethanol ND ug/L 11/10/22 16:22 64-17-5400020
Ethylbenzene 1480 ug/L 11/10/22 16:22 100-41-410.0 20
Ethyl-tert-butyl ether ND ug/L 11/10/22 16:22 637-92-320020
Hexachloro-1,3-butadiene ND ug/L 11/10/22 16:22 87-68-340.0 20
Isopropylbenzene (Cumene)143 ug/L 11/10/22 16:22 98-82-810.0 20
Methylene Chloride ND ug/L 11/10/22 16:22 75-09-240.0 20
Methyl-tert-butyl ether ND ug/L 11/10/22 16:22 1634-04-410.0 20
Naphthalene 953 ug/L 11/10/22 16:22 91-20-340.0 20
n-Propylbenzene 324 ug/L 11/10/22 16:22 103-65-110.0 20
Styrene ND ug/L 11/10/22 16:22 100-42-510.0 20
1,1,1,2-Tetrachloroethane ND ug/L 11/10/22 16:22 630-20-610.0 20
1,1,2,2-Tetrachloroethane ND ug/L 11/10/22 16:22 79-34-510.0 20
Tetrachloroethene ND ug/L 11/10/22 16:22 127-18-410.0 20
Toluene 2820 ug/L 11/10/22 16:22 108-88-310.0 20
1,2,3-Trichlorobenzene ND ug/L 11/10/22 16:22 87-61-640.0 20
1,2,4-Trichlorobenzene ND ug/L 11/10/22 16:22 120-82-140.0 20
1,1,1-Trichloroethane ND ug/L 11/10/22 16:22 71-55-610.0 20
1,1,2-Trichloroethane ND ug/L 11/10/22 16:22 79-00-510.0 20
Trichloroethene ND ug/L 11/10/22 16:22 79-01-610.0 20
Trichlorofluoromethane ND ug/L 11/10/22 16:22 75-69-420.0 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 7 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-2 Lab ID:92633465002 Collected:10/27/22 10:00 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,2,3-Trichloropropane ND ug/L 11/10/22 16:22 96-18-410.0 20
1,2,4-Trimethylbenzene 3280 ug/L 11/10/22 16:22 95-63-610.0 20
1,3,5-Trimethylbenzene 1060 ug/L 11/10/22 16:22 108-67-810.0 20
Vinyl chloride ND ug/L 11/10/22 16:22 75-01-420.0 20
m&p-Xylene 6230 ug/L 11/10/22 16:22 179601-23-120.0 20
o-Xylene 3900 ug/L 11/10/22 16:22 95-47-610.0 20
Surrogates
1,2-Dichloroethane-d4 (S)85 %11/10/22 16:22 17060-07-070-130 20
4-Bromofluorobenzene (S)93 %11/10/22 16:22 460-00-470-130 20
Toluene-d8 (S)103 %11/10/22 16:22 2037-26-570-130 20
Sample:MW-3 Lab ID:92633465003 Collected:10/27/22 10:30 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/10/22 14:34 75-85-41001
tert-Amylmethyl ether ND ug/L 11/10/22 14:34 994-05-810.0 1
Benzene ND ug/L 11/10/22 14:34 71-43-20.50 1
Bromobenzene ND ug/L 11/10/22 14:34 108-86-10.50 1
Bromochloromethane ND ug/L 11/10/22 14:34 74-97-50.50 1
Bromodichloromethane ND ug/L 11/10/22 14:34 75-27-40.50 1
Bromoform ND ug/L 11/10/22 14:34 75-25-20.50 1
Bromomethane ND ug/L 11/10/22 14:34 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 11/10/22 14:34 75-65-050.0 1
n-Butylbenzene ND ug/L 11/10/22 14:34 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/10/22 14:34 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/10/22 14:34 98-06-60.50 1
tert-Butyl Formate ND ug/L 11/10/22 14:34 762-75-450.0 1
Carbon tetrachloride ND ug/L 11/10/22 14:34 56-23-50.50 1
Chlorobenzene ND ug/L 11/10/22 14:34 108-90-70.50 1
Chloroethane ND ug/L 11/10/22 14:34 75-00-31.0 1
Chloroform ND ug/L 11/10/22 14:34 67-66-30.50 1
Chloromethane ND ug/L 11/10/22 14:34 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/10/22 14:34 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/10/22 14:34 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/10/22 14:34 96-12-81.0 1
Dibromochloromethane ND ug/L 11/10/22 14:34 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/10/22 14:34 106-93-40.50 1
Dibromomethane ND ug/L 11/10/22 14:34 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/10/22 14:34 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/10/22 14:34 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/10/22 14:34 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/10/22 14:34 75-71-80.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 8 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-3 Lab ID:92633465003 Collected:10/27/22 10:30 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1-Dichloroethane ND ug/L 11/10/22 14:34 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/10/22 14:34 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/10/22 14:34 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/10/22 14:34 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/10/22 14:34 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/10/22 14:34 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/10/22 14:34 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/10/22 14:34 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/10/22 14:34 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/10/22 14:34 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/10/22 14:34 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/10/22 14:34 108-20-30.50 1
Ethanol ND ug/L 11/10/22 14:34 64-17-52001
Ethylbenzene ND ug/L 11/10/22 14:34 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 11/10/22 14:34 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 11/10/22 14:34 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/10/22 14:34 98-82-80.50 1
Methylene Chloride ND ug/L 11/10/22 14:34 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/10/22 14:34 1634-04-40.50 1
Naphthalene ND ug/L 11/10/22 14:34 91-20-32.0 1
n-Propylbenzene ND ug/L 11/10/22 14:34 103-65-10.50 1
Styrene ND ug/L 11/10/22 14:34 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/10/22 14:34 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/10/22 14:34 79-34-50.50 1
Tetrachloroethene ND ug/L 11/10/22 14:34 127-18-40.50 1
Toluene 1.3 ug/L 11/10/22 14:34 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/10/22 14:34 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/10/22 14:34 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/10/22 14:34 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/10/22 14:34 79-00-50.50 1
Trichloroethene ND ug/L 11/10/22 14:34 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/10/22 14:34 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/10/22 14:34 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/10/22 14:34 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/10/22 14:34 108-67-80.50 1
Vinyl chloride ND ug/L 11/10/22 14:34 75-01-41.0 1
m&p-Xylene 1.3 ug/L 11/10/22 14:34 179601-23-11.0 1
o-Xylene 0.71 ug/L 11/10/22 14:34 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)90 %11/10/22 14:34 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %11/10/22 14:34 460-00-470-130 1
Toluene-d8 (S)102 %11/10/22 14:34 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 9 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-4 Lab ID:92633465004 Collected:10/27/22 11:00 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/10/22 14:52 75-85-41001
tert-Amylmethyl ether ND ug/L 11/10/22 14:52 994-05-810.0 1
Benzene ND ug/L 11/10/22 14:52 71-43-20.50 1
Bromobenzene ND ug/L 11/10/22 14:52 108-86-10.50 1
Bromochloromethane ND ug/L 11/10/22 14:52 74-97-50.50 1
Bromodichloromethane ND ug/L 11/10/22 14:52 75-27-40.50 1
Bromoform ND ug/L 11/10/22 14:52 75-25-20.50 1
Bromomethane ND ug/L 11/10/22 14:52 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 11/10/22 14:52 75-65-050.0 1
n-Butylbenzene ND ug/L 11/10/22 14:52 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/10/22 14:52 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/10/22 14:52 98-06-60.50 1
tert-Butyl Formate ND ug/L 11/10/22 14:52 762-75-450.0 1
Carbon tetrachloride ND ug/L 11/10/22 14:52 56-23-50.50 1
Chlorobenzene ND ug/L 11/10/22 14:52 108-90-70.50 1
Chloroethane ND ug/L 11/10/22 14:52 75-00-31.0 1
Chloroform ND ug/L 11/10/22 14:52 67-66-30.50 1
Chloromethane ND ug/L 11/10/22 14:52 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/10/22 14:52 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/10/22 14:52 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/10/22 14:52 96-12-81.0 1
Dibromochloromethane ND ug/L 11/10/22 14:52 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/10/22 14:52 106-93-40.50 1
Dibromomethane ND ug/L 11/10/22 14:52 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/10/22 14:52 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/10/22 14:52 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/10/22 14:52 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/10/22 14:52 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/10/22 14:52 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/10/22 14:52 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/10/22 14:52 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/10/22 14:52 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/10/22 14:52 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/10/22 14:52 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/10/22 14:52 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/10/22 14:52 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/10/22 14:52 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/10/22 14:52 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/10/22 14:52 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/10/22 14:52 108-20-30.50 1
Ethanol ND ug/L 11/10/22 14:52 64-17-52001
Ethylbenzene ND ug/L 11/10/22 14:52 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 11/10/22 14:52 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 11/10/22 14:52 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/10/22 14:52 98-82-80.50 1
Methylene Chloride ND ug/L 11/10/22 14:52 75-09-22.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 10 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-4 Lab ID:92633465004 Collected:10/27/22 11:00 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether 7.5 ug/L 11/10/22 14:52 1634-04-40.50 1
Naphthalene ND ug/L 11/10/22 14:52 91-20-32.0 1
n-Propylbenzene ND ug/L 11/10/22 14:52 103-65-10.50 1
Styrene ND ug/L 11/10/22 14:52 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/10/22 14:52 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/10/22 14:52 79-34-50.50 1
Tetrachloroethene ND ug/L 11/10/22 14:52 127-18-40.50 1
Toluene ND ug/L 11/10/22 14:52 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/10/22 14:52 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/10/22 14:52 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/10/22 14:52 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/10/22 14:52 79-00-50.50 1
Trichloroethene ND ug/L 11/10/22 14:52 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/10/22 14:52 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/10/22 14:52 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/10/22 14:52 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/10/22 14:52 108-67-80.50 1
Vinyl chloride ND ug/L 11/10/22 14:52 75-01-41.0 1
m&p-Xylene ND ug/L 11/10/22 14:52 179601-23-11.0 1
o-Xylene ND ug/L 11/10/22 14:52 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)88 %11/10/22 14:52 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %11/10/22 14:52 460-00-470-130 1
Toluene-d8 (S)100 %11/10/22 14:52 2037-26-570-130 1
Sample:MW-5 Lab ID:92633465005 Collected:10/27/22 11:30 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/10/22 17:16 75-85-440000400
tert-Amylmethyl ether ND ug/L 11/10/22 17:16 994-05-84000400
Benzene 3110 ug/L 11/10/22 17:16 71-43-2200400
Bromobenzene ND ug/L 11/10/22 17:16 108-86-1200400
Bromochloromethane ND ug/L 11/10/22 17:16 74-97-5200400
Bromodichloromethane ND ug/L 11/10/22 17:16 75-27-4200400
Bromoform ND ug/L 11/10/22 17:16 75-25-2200400
Bromomethane ND ug/L 11/10/22 17:16 74-83-92000400
tert-Butyl Alcohol ND ug/L 11/10/22 17:16 75-65-020000400
n-Butylbenzene ND ug/L 11/10/22 17:16 104-51-8200400
sec-Butylbenzene ND ug/L 11/10/22 17:16 135-98-8200400
tert-Butylbenzene ND ug/L 11/10/22 17:16 98-06-6200400
tert-Butyl Formate ND ug/L 11/10/22 17:16 762-75-420000400
Carbon tetrachloride ND ug/L 11/10/22 17:16 56-23-5200400
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 11 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-5 Lab ID:92633465005 Collected:10/27/22 11:30 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Chlorobenzene ND ug/L 11/10/22 17:16 108-90-7200400
Chloroethane ND ug/L 11/10/22 17:16 75-00-3400400
Chloroform ND ug/L 11/10/22 17:16 67-66-3200400
Chloromethane ND ug/L 11/10/22 17:16 74-87-3400400
2-Chlorotoluene ND ug/L 11/10/22 17:16 95-49-8200400
4-Chlorotoluene ND ug/L 11/10/22 17:16 106-43-4200400
1,2-Dibromo-3-chloropropane ND ug/L 11/10/22 17:16 96-12-8400400
Dibromochloromethane ND ug/L 11/10/22 17:16 124-48-1200400
1,2-Dibromoethane (EDB)ND ug/L 11/10/22 17:16 106-93-4200400
Dibromomethane ND ug/L 11/10/22 17:16 74-95-3200400
1,2-Dichlorobenzene ND ug/L 11/10/22 17:16 95-50-1200400
1,3-Dichlorobenzene ND ug/L 11/10/22 17:16 541-73-1200400
1,4-Dichlorobenzene ND ug/L 11/10/22 17:16 106-46-7200400
Dichlorodifluoromethane ND ug/L 11/10/22 17:16 75-71-8200400
1,1-Dichloroethane ND ug/L 11/10/22 17:16 75-34-3200400
1,2-Dichloroethane ND ug/L 11/10/22 17:16 107-06-2200400
1,1-Dichloroethene ND ug/L 11/10/22 17:16 75-35-4200400
cis-1,2-Dichloroethene ND ug/L 11/10/22 17:16 156-59-2200400
trans-1,2-Dichloroethene ND ug/L 11/10/22 17:16 156-60-5200400
1,2-Dichloropropane ND ug/L 11/10/22 17:16 78-87-5200400
1,3-Dichloropropane ND ug/L 11/10/22 17:16 142-28-9200400
2,2-Dichloropropane ND ug/L 11/10/22 17:16 594-20-7200400
1,1-Dichloropropene ND ug/L 11/10/22 17:16 563-58-6200400
cis-1,3-Dichloropropene ND ug/L 11/10/22 17:16 10061-01-5200400
trans-1,3-Dichloropropene ND ug/L 11/10/22 17:16 10061-02-6200400
Diisopropyl ether ND ug/L 11/10/22 17:16 108-20-3200400
Ethanol ND ug/L 11/10/22 17:16 64-17-580000400
Ethylbenzene 4020 ug/L 11/10/22 17:16 100-41-4200400
Ethyl-tert-butyl ether ND ug/L 11/10/22 17:16 637-92-34000400
Hexachloro-1,3-butadiene ND ug/L 11/10/22 17:16 87-68-3800400
Isopropylbenzene (Cumene)ND ug/L 11/10/22 17:16 98-82-8200400
Methylene Chloride ND ug/L 11/10/22 17:16 75-09-2800400
Methyl-tert-butyl ether ND ug/L 11/10/22 17:16 1634-04-4200400
Naphthalene 846 ug/L 11/10/22 17:16 91-20-3800400
n-Propylbenzene 347 ug/L 11/10/22 17:16 103-65-1200400
Styrene ND ug/L 11/10/22 17:16 100-42-5200400
1,1,1,2-Tetrachloroethane ND ug/L 11/10/22 17:16 630-20-6200400
1,1,2,2-Tetrachloroethane ND ug/L 11/10/22 17:16 79-34-5200400
Tetrachloroethene ND ug/L 11/10/22 17:16 127-18-4200400
Toluene 45400 ug/L 11/10/22 17:16 108-88-3200400
1,2,3-Trichlorobenzene ND ug/L 11/10/22 17:16 87-61-6800400
1,2,4-Trichlorobenzene ND ug/L 11/10/22 17:16 120-82-1800400
1,1,1-Trichloroethane ND ug/L 11/10/22 17:16 71-55-6200400
1,1,2-Trichloroethane ND ug/L 11/10/22 17:16 79-00-5200400
Trichloroethene ND ug/L 11/10/22 17:16 79-01-6200400
Trichlorofluoromethane ND ug/L 11/10/22 17:16 75-69-4400400
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 12 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-5 Lab ID:92633465005 Collected:10/27/22 11:30 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,2,3-Trichloropropane ND ug/L 11/10/22 17:16 96-18-4200400
1,2,4-Trimethylbenzene 3190 ug/L 11/10/22 17:16 95-63-6200400
1,3,5-Trimethylbenzene 773 ug/L 11/10/22 17:16 108-67-8200400
Vinyl chloride ND ug/L 11/10/22 17:16 75-01-4400400
m&p-Xylene 14400 ug/L 11/10/22 17:16 179601-23-1400400
o-Xylene 7370 ug/L 11/10/22 17:16 95-47-6200400
Surrogates
1,2-Dichloroethane-d4 (S)86 %11/10/22 17:16 17060-07-070-130 400
4-Bromofluorobenzene (S)96 %11/10/22 17:16 460-00-470-130 400
Toluene-d8 (S)101 %11/10/22 17:16 2037-26-570-130 400
Sample:MW-6 Lab ID:92633465006 Collected:10/26/22 10:30 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/09/22 17:31 75-85-412500125
tert-Amylmethyl ether ND ug/L 11/09/22 17:31 994-05-81250125
Benzene 280 ug/L 11/09/22 17:31 71-43-262.5 125
Bromobenzene ND ug/L 11/09/22 17:31 108-86-162.5 125
Bromochloromethane ND ug/L 11/09/22 17:31 74-97-562.5 125
Bromodichloromethane ND ug/L 11/09/22 17:31 75-27-462.5 125
Bromoform ND ug/L 11/09/22 17:31 75-25-262.5 125
Bromomethane ND ug/L 11/09/22 17:31 74-83-9625125
tert-Butyl Alcohol ND ug/L 11/09/22 17:31 75-65-06250125
n-Butylbenzene ND ug/L 11/09/22 17:31 104-51-862.5 125
sec-Butylbenzene ND ug/L 11/09/22 17:31 135-98-862.5 125
tert-Butylbenzene ND ug/L 11/09/22 17:31 98-06-662.5 125
tert-Butyl Formate ND ug/L 11/09/22 17:31 762-75-46250125
Carbon tetrachloride ND ug/L 11/09/22 17:31 56-23-562.5 125
Chlorobenzene ND ug/L 11/09/22 17:31 108-90-762.5 125
Chloroethane ND ug/L 11/09/22 17:31 75-00-3125125
Chloroform ND ug/L 11/09/22 17:31 67-66-362.5 125
Chloromethane ND ug/L 11/09/22 17:31 74-87-3125125
2-Chlorotoluene ND ug/L 11/09/22 17:31 95-49-862.5 125
4-Chlorotoluene ND ug/L 11/09/22 17:31 106-43-462.5 125
1,2-Dibromo-3-chloropropane ND ug/L 11/09/22 17:31 96-12-8125125
Dibromochloromethane ND ug/L 11/09/22 17:31 124-48-162.5 125
1,2-Dibromoethane (EDB)ND ug/L 11/09/22 17:31 106-93-462.5 125
Dibromomethane ND ug/L 11/09/22 17:31 74-95-362.5 125
1,2-Dichlorobenzene ND ug/L 11/09/22 17:31 95-50-162.5 125
1,3-Dichlorobenzene ND ug/L 11/09/22 17:31 541-73-162.5 125
1,4-Dichlorobenzene ND ug/L 11/09/22 17:31 106-46-762.5 125
Dichlorodifluoromethane ND ug/L 11/09/22 17:31 75-71-862.5 125
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 13 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-6 Lab ID:92633465006 Collected:10/26/22 10:30 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1-Dichloroethane ND ug/L 11/09/22 17:31 75-34-362.5 125
1,2-Dichloroethane ND ug/L 11/09/22 17:31 107-06-262.5 125
1,1-Dichloroethene ND ug/L 11/09/22 17:31 75-35-462.5 125
cis-1,2-Dichloroethene ND ug/L 11/09/22 17:31 156-59-262.5 125
trans-1,2-Dichloroethene ND ug/L 11/09/22 17:31 156-60-562.5 125
1,2-Dichloropropane ND ug/L 11/09/22 17:31 78-87-562.5 125
1,3-Dichloropropane ND ug/L 11/09/22 17:31 142-28-962.5 125
2,2-Dichloropropane ND ug/L 11/09/22 17:31 594-20-762.5 125
1,1-Dichloropropene ND ug/L 11/09/22 17:31 563-58-662.5 125
cis-1,3-Dichloropropene ND ug/L 11/09/22 17:31 10061-01-562.5 125
trans-1,3-Dichloropropene ND ug/L 11/09/22 17:31 10061-02-662.5 125
Diisopropyl ether ND ug/L 11/09/22 17:31 108-20-362.5 125
Ethanol ND ug/L 11/09/22 17:31 64-17-525000125
Ethylbenzene 4050 ug/L 11/09/22 17:31 100-41-462.5 125
Ethyl-tert-butyl ether ND ug/L 11/09/22 17:31 637-92-31250125
Hexachloro-1,3-butadiene ND ug/L 11/09/22 17:31 87-68-3250125
Isopropylbenzene (Cumene)141 ug/L 11/09/22 17:31 98-82-862.5 125
Methylene Chloride ND ug/L 11/09/22 17:31 75-09-2250125
Methyl-tert-butyl ether ND ug/L 11/09/22 17:31 1634-04-462.5 125
Naphthalene 681 ug/L 11/09/22 17:31 91-20-3250125
n-Propylbenzene 385 ug/L 11/09/22 17:31 103-65-162.5 125
Styrene ND ug/L 11/09/22 17:31 100-42-562.5 125
1,1,1,2-Tetrachloroethane ND ug/L 11/09/22 17:31 630-20-662.5 125
1,1,2,2-Tetrachloroethane ND ug/L 11/09/22 17:31 79-34-562.5 125
Tetrachloroethene ND ug/L 11/09/22 17:31 127-18-462.5 125
Toluene 24000 ug/L 11/09/22 17:31 108-88-362.5 125
1,2,3-Trichlorobenzene ND ug/L 11/09/22 17:31 87-61-6250125
1,2,4-Trichlorobenzene ND ug/L 11/09/22 17:31 120-82-1250125
1,1,1-Trichloroethane ND ug/L 11/09/22 17:31 71-55-662.5 125
1,1,2-Trichloroethane ND ug/L 11/09/22 17:31 79-00-562.5 125
Trichloroethene ND ug/L 11/09/22 17:31 79-01-662.5 125
Trichlorofluoromethane ND ug/L 11/09/22 17:31 75-69-4125125
1,2,3-Trichloropropane ND ug/L 11/09/22 17:31 96-18-462.5 125
1,2,4-Trimethylbenzene 3120 ug/L 11/09/22 17:31 95-63-662.5 125
1,3,5-Trimethylbenzene 789 ug/L 11/09/22 17:31 108-67-862.5 125
Vinyl chloride ND ug/L 11/09/22 17:31 75-01-4125125
m&p-Xylene 14200 ug/L 11/09/22 17:31 179601-23-1125125
o-Xylene 7400 ug/L 11/09/22 17:31 95-47-662.5 125
Surrogates
1,2-Dichloroethane-d4 (S)84 %11/09/22 17:31 17060-07-070-130 125
4-Bromofluorobenzene (S)94 %11/09/22 17:31 460-00-470-130 125
Toluene-d8 (S)102 %11/09/22 17:31 2037-26-570-130 125
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 14 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-7 Lab ID:92633465007 Collected:10/26/22 11:00 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/09/22 17:13 75-85-410000100
tert-Amylmethyl ether ND ug/L 11/09/22 17:13 994-05-81000100
Benzene ND ug/L 11/09/22 17:13 71-43-250.0 100
Bromobenzene ND ug/L 11/09/22 17:13 108-86-150.0 100
Bromochloromethane ND ug/L 11/09/22 17:13 74-97-550.0 100
Bromodichloromethane ND ug/L 11/09/22 17:13 75-27-450.0 100
Bromoform ND ug/L 11/09/22 17:13 75-25-250.0 100
Bromomethane ND ug/L 11/09/22 17:13 74-83-9500100
tert-Butyl Alcohol ND ug/L 11/09/22 17:13 75-65-05000100
n-Butylbenzene 57.2 ug/L 11/09/22 17:13 104-51-850.0 100
sec-Butylbenzene ND ug/L 11/09/22 17:13 135-98-850.0 100
tert-Butylbenzene ND ug/L 11/09/22 17:13 98-06-650.0 100
tert-Butyl Formate ND ug/L 11/09/22 17:13 762-75-45000100
Carbon tetrachloride ND ug/L 11/09/22 17:13 56-23-550.0 100
Chlorobenzene ND ug/L 11/09/22 17:13 108-90-750.0 100
Chloroethane ND ug/L 11/09/22 17:13 75-00-3100100
Chloroform ND ug/L 11/09/22 17:13 67-66-350.0 100
Chloromethane ND ug/L 11/09/22 17:13 74-87-3100100
2-Chlorotoluene ND ug/L 11/09/22 17:13 95-49-850.0 100
4-Chlorotoluene ND ug/L 11/09/22 17:13 106-43-450.0 100
1,2-Dibromo-3-chloropropane ND ug/L 11/09/22 17:13 96-12-8100100
Dibromochloromethane ND ug/L 11/09/22 17:13 124-48-150.0 100
1,2-Dibromoethane (EDB)ND ug/L 11/09/22 17:13 106-93-450.0 100
Dibromomethane ND ug/L 11/09/22 17:13 74-95-350.0 100
1,2-Dichlorobenzene ND ug/L 11/09/22 17:13 95-50-150.0 100
1,3-Dichlorobenzene ND ug/L 11/09/22 17:13 541-73-150.0 100
1,4-Dichlorobenzene ND ug/L 11/09/22 17:13 106-46-750.0 100
Dichlorodifluoromethane ND ug/L 11/09/22 17:13 75-71-850.0 100
1,1-Dichloroethane ND ug/L 11/09/22 17:13 75-34-350.0 100
1,2-Dichloroethane ND ug/L 11/09/22 17:13 107-06-250.0 100
1,1-Dichloroethene ND ug/L 11/09/22 17:13 75-35-450.0 100
cis-1,2-Dichloroethene ND ug/L 11/09/22 17:13 156-59-250.0 100
trans-1,2-Dichloroethene ND ug/L 11/09/22 17:13 156-60-550.0 100
1,2-Dichloropropane ND ug/L 11/09/22 17:13 78-87-550.0 100
1,3-Dichloropropane ND ug/L 11/09/22 17:13 142-28-950.0 100
2,2-Dichloropropane ND ug/L 11/09/22 17:13 594-20-750.0 100
1,1-Dichloropropene ND ug/L 11/09/22 17:13 563-58-650.0 100
cis-1,3-Dichloropropene ND ug/L 11/09/22 17:13 10061-01-550.0 100
trans-1,3-Dichloropropene ND ug/L 11/09/22 17:13 10061-02-650.0 100
Diisopropyl ether ND ug/L 11/09/22 17:13 108-20-350.0 100
Ethanol ND ug/L 11/09/22 17:13 64-17-520000100
Ethylbenzene 2910 ug/L 11/09/22 17:13 100-41-450.0 100
Ethyl-tert-butyl ether ND ug/L 11/09/22 17:13 637-92-31000100
Hexachloro-1,3-butadiene ND ug/L 11/09/22 17:13 87-68-3200100
Isopropylbenzene (Cumene)116 ug/L 11/09/22 17:13 98-82-850.0 100
Methylene Chloride ND ug/L 11/09/22 17:13 75-09-2200100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 15 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-7 Lab ID:92633465007 Collected:10/26/22 11:00 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether ND ug/L 11/09/22 17:13 1634-04-450.0 100
Naphthalene 414 ug/L 11/09/22 17:13 91-20-3200100
n-Propylbenzene ND ug/L 11/09/22 17:13 103-65-150.0 100
Styrene ND ug/L 11/09/22 17:13 100-42-550.0 100
1,1,1,2-Tetrachloroethane ND ug/L 11/09/22 17:13 630-20-650.0 100
1,1,2,2-Tetrachloroethane ND ug/L 11/09/22 17:13 79-34-550.0 100
Tetrachloroethene ND ug/L 11/09/22 17:13 127-18-450.0 100
Toluene 24300 ug/L 11/10/22 10:50 108-88-3 H1100200
1,2,3-Trichlorobenzene ND ug/L 11/09/22 17:13 87-61-6200100
1,2,4-Trichlorobenzene ND ug/L 11/09/22 17:13 120-82-1200100
1,1,1-Trichloroethane ND ug/L 11/09/22 17:13 71-55-650.0 100
1,1,2-Trichloroethane ND ug/L 11/09/22 17:13 79-00-550.0 100
Trichloroethene ND ug/L 11/09/22 17:13 79-01-650.0 100
Trichlorofluoromethane ND ug/L 11/09/22 17:13 75-69-4100100
1,2,3-Trichloropropane ND ug/L 11/09/22 17:13 96-18-450.0 100
1,2,4-Trimethylbenzene 2390 ug/L 11/09/22 17:13 95-63-650.0 100
1,3,5-Trimethylbenzene 1350 ug/L 11/09/22 17:13 108-67-850.0 100
Vinyl chloride ND ug/L 11/09/22 17:13 75-01-4100100
m&p-Xylene 9780 ug/L 11/09/22 17:13 179601-23-1100100
o-Xylene 5150 ug/L 11/09/22 17:13 95-47-650.0 100
Surrogates
1,2-Dichloroethane-d4 (S)88 %11/09/22 17:13 17060-07-070-130 100
4-Bromofluorobenzene (S)95 %11/09/22 17:13 460-00-470-130 100
Toluene-d8 (S)97 %11/09/22 17:13 2037-26-570-130 100
Sample:MW-8 Lab ID:92633465008 Collected:10/27/22 12:00 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/11/22 15:26 75-85-4 H12002
tert-Amylmethyl ether ND ug/L 11/11/22 15:26 994-05-8 H120.0 2
Benzene 31.0 ug/L 11/11/22 15:26 71-43-2 H11.0 2
Bromobenzene ND ug/L 11/11/22 15:26 108-86-1 H11.0 2
Bromochloromethane ND ug/L 11/11/22 15:26 74-97-5 H11.0 2
Bromodichloromethane ND ug/L 11/11/22 15:26 75-27-4 H11.0 2
Bromoform ND ug/L 11/11/22 15:26 75-25-2 H11.0 2
Bromomethane ND ug/L 11/11/22 15:26 74-83-9 H110.0 2
tert-Butyl Alcohol ND ug/L 11/11/22 15:26 75-65-0 H11002
n-Butylbenzene ND ug/L 11/11/22 15:26 104-51-8 H11.0 2
sec-Butylbenzene ND ug/L 11/11/22 15:26 135-98-8 H11.0 2
tert-Butylbenzene ND ug/L 11/11/22 15:26 98-06-6 H11.0 2
tert-Butyl Formate ND ug/L 11/11/22 15:26 762-75-4 H11002
Carbon tetrachloride ND ug/L 11/11/22 15:26 56-23-5 H11.0 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 16 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-8 Lab ID:92633465008 Collected:10/27/22 12:00 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Chlorobenzene ND ug/L 11/11/22 15:26 108-90-7 H11.0 2
Chloroethane ND ug/L 11/11/22 15:26 75-00-3 H12.0 2
Chloroform ND ug/L 11/11/22 15:26 67-66-3 H11.0 2
Chloromethane ND ug/L 11/11/22 15:26 74-87-3 H12.0 2
2-Chlorotoluene ND ug/L 11/11/22 15:26 95-49-8 H11.0 2
4-Chlorotoluene ND ug/L 11/11/22 15:26 106-43-4 H11.0 2
1,2-Dibromo-3-chloropropane ND ug/L 11/11/22 15:26 96-12-8 H12.0 2
Dibromochloromethane ND ug/L 11/11/22 15:26 124-48-1 H11.0 2
1,2-Dibromoethane (EDB)ND ug/L 11/11/22 15:26 106-93-4 H11.0 2
Dibromomethane ND ug/L 11/11/22 15:26 74-95-3 H11.0 2
1,2-Dichlorobenzene ND ug/L 11/11/22 15:26 95-50-1 H11.0 2
1,3-Dichlorobenzene ND ug/L 11/11/22 15:26 541-73-1 H11.0 2
1,4-Dichlorobenzene ND ug/L 11/11/22 15:26 106-46-7 H11.0 2
Dichlorodifluoromethane ND ug/L 11/11/22 15:26 75-71-8 H11.0 2
1,1-Dichloroethane ND ug/L 11/11/22 15:26 75-34-3 H11.0 2
1,2-Dichloroethane ND ug/L 11/11/22 15:26 107-06-2 H11.0 2
1,1-Dichloroethene ND ug/L 11/11/22 15:26 75-35-4 H11.0 2
cis-1,2-Dichloroethene ND ug/L 11/11/22 15:26 156-59-2 H11.0 2
trans-1,2-Dichloroethene ND ug/L 11/11/22 15:26 156-60-5 H11.0 2
1,2-Dichloropropane ND ug/L 11/11/22 15:26 78-87-5 H11.0 2
1,3-Dichloropropane ND ug/L 11/11/22 15:26 142-28-9 H11.0 2
2,2-Dichloropropane ND ug/L 11/11/22 15:26 594-20-7 H11.0 2
1,1-Dichloropropene ND ug/L 11/11/22 15:26 563-58-6 H11.0 2
cis-1,3-Dichloropropene ND ug/L 11/11/22 15:26 10061-01-5 H11.0 2
trans-1,3-Dichloropropene ND ug/L 11/11/22 15:26 10061-02-6 H11.0 2
Diisopropyl ether ND ug/L 11/11/22 15:26 108-20-3 H11.0 2
Ethanol ND ug/L 11/11/22 15:26 64-17-5 H14002
Ethylbenzene 36.7 ug/L 11/11/22 15:26 100-41-4 H11.0 2
Ethyl-tert-butyl ether ND ug/L 11/11/22 15:26 637-92-3 H120.0 2
Hexachloro-1,3-butadiene ND ug/L 11/11/22 15:26 87-68-3 H14.0 2
Isopropylbenzene (Cumene)3.6 ug/L 11/11/22 15:26 98-82-8 H11.0 2
Methylene Chloride ND ug/L 11/11/22 15:26 75-09-2 H14.0 2
Methyl-tert-butyl ether 4.1 ug/L 11/11/22 15:26 1634-04-4 H11.0 2
Naphthalene 11.5 ug/L 11/11/22 15:26 91-20-3 H14.0 2
n-Propylbenzene 5.2 ug/L 11/11/22 15:26 103-65-1 H11.0 2
Styrene ND ug/L 11/11/22 15:26 100-42-5 H11.0 2
1,1,1,2-Tetrachloroethane ND ug/L 11/11/22 15:26 630-20-6 H11.0 2
1,1,2,2-Tetrachloroethane ND ug/L 11/11/22 15:26 79-34-5 H11.0 2
Tetrachloroethene ND ug/L 11/11/22 15:26 127-18-4 H11.0 2
Toluene 297 ug/L 11/11/22 15:26 108-88-3 H11.0 2
1,2,3-Trichlorobenzene ND ug/L 11/11/22 15:26 87-61-6 H14.0 2
1,2,4-Trichlorobenzene ND ug/L 11/11/22 15:26 120-82-1 H14.0 2
1,1,1-Trichloroethane ND ug/L 11/11/22 15:26 71-55-6 H11.0 2
1,1,2-Trichloroethane ND ug/L 11/11/22 15:26 79-00-5 H11.0 2
Trichloroethene ND ug/L 11/11/22 15:26 79-01-6 H11.0 2
Trichlorofluoromethane ND ug/L 11/11/22 15:26 75-69-4 H12.0 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 17 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-8 Lab ID:92633465008 Collected:10/27/22 12:00 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,2,3-Trichloropropane ND ug/L 11/11/22 15:26 96-18-4 H11.0 2
1,2,4-Trimethylbenzene 57.7 ug/L 11/11/22 15:26 95-63-6 H11.0 2
1,3,5-Trimethylbenzene 18.6 ug/L 11/11/22 15:26 108-67-8 H11.0 2
Vinyl chloride ND ug/L 11/11/22 15:26 75-01-4 H12.0 2
m&p-Xylene 201 ug/L 11/11/22 15:26 179601-23-1 H12.0 2
o-Xylene 80.7 ug/L 11/11/22 15:26 95-47-6 H11.0 2
Surrogates
1,2-Dichloroethane-d4 (S)100 %11/11/22 15:26 17060-07-0 H570-130 2
4-Bromofluorobenzene (S)102 %11/11/22 15:26 460-00-470-130 2
Toluene-d8 (S)100 %11/11/22 15:26 2037-26-570-130 2
Sample:MW-9 Lab ID:92633465009 Collected:10/27/22 12:30 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/10/22 15:10 75-85-41001
tert-Amylmethyl ether ND ug/L 11/10/22 15:10 994-05-810.0 1
Benzene ND ug/L 11/10/22 15:10 71-43-20.50 1
Bromobenzene ND ug/L 11/10/22 15:10 108-86-10.50 1
Bromochloromethane ND ug/L 11/10/22 15:10 74-97-50.50 1
Bromodichloromethane ND ug/L 11/10/22 15:10 75-27-40.50 1
Bromoform ND ug/L 11/10/22 15:10 75-25-20.50 1
Bromomethane ND ug/L 11/10/22 15:10 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 11/10/22 15:10 75-65-050.0 1
n-Butylbenzene ND ug/L 11/10/22 15:10 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/10/22 15:10 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/10/22 15:10 98-06-60.50 1
tert-Butyl Formate ND ug/L 11/10/22 15:10 762-75-450.0 1
Carbon tetrachloride ND ug/L 11/10/22 15:10 56-23-50.50 1
Chlorobenzene ND ug/L 11/10/22 15:10 108-90-70.50 1
Chloroethane ND ug/L 11/10/22 15:10 75-00-31.0 1
Chloroform ND ug/L 11/10/22 15:10 67-66-30.50 1
Chloromethane ND ug/L 11/10/22 15:10 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/10/22 15:10 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/10/22 15:10 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/10/22 15:10 96-12-81.0 1
Dibromochloromethane ND ug/L 11/10/22 15:10 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/10/22 15:10 106-93-40.50 1
Dibromomethane ND ug/L 11/10/22 15:10 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/10/22 15:10 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/10/22 15:10 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/10/22 15:10 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/10/22 15:10 75-71-80.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 18 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-9 Lab ID:92633465009 Collected:10/27/22 12:30 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1-Dichloroethane ND ug/L 11/10/22 15:10 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/10/22 15:10 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/10/22 15:10 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/10/22 15:10 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/10/22 15:10 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/10/22 15:10 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/10/22 15:10 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/10/22 15:10 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/10/22 15:10 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/10/22 15:10 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/10/22 15:10 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/10/22 15:10 108-20-30.50 1
Ethanol ND ug/L 11/10/22 15:10 64-17-52001
Ethylbenzene ND ug/L 11/10/22 15:10 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 11/10/22 15:10 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 11/10/22 15:10 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/10/22 15:10 98-82-80.50 1
Methylene Chloride ND ug/L 11/10/22 15:10 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/10/22 15:10 1634-04-40.50 1
Naphthalene ND ug/L 11/10/22 15:10 91-20-32.0 1
n-Propylbenzene ND ug/L 11/10/22 15:10 103-65-10.50 1
Styrene ND ug/L 11/10/22 15:10 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/10/22 15:10 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/10/22 15:10 79-34-50.50 1
Tetrachloroethene ND ug/L 11/10/22 15:10 127-18-40.50 1
Toluene ND ug/L 11/10/22 15:10 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/10/22 15:10 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/10/22 15:10 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/10/22 15:10 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/10/22 15:10 79-00-50.50 1
Trichloroethene ND ug/L 11/10/22 15:10 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/10/22 15:10 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/10/22 15:10 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/10/22 15:10 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/10/22 15:10 108-67-80.50 1
Vinyl chloride ND ug/L 11/10/22 15:10 75-01-41.0 1
m&p-Xylene ND ug/L 11/10/22 15:10 179601-23-11.0 1
o-Xylene ND ug/L 11/10/22 15:10 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)88 %11/10/22 15:10 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %11/10/22 15:10 460-00-470-130 1
Toluene-d8 (S)102 %11/10/22 15:10 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 19 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-10 Lab ID:92633465010 Collected:10/26/22 11:30 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/09/22 16:37 75-85-41001
tert-Amylmethyl ether ND ug/L 11/09/22 16:37 994-05-810.0 1
Benzene ND ug/L 11/09/22 16:37 71-43-20.50 1
Bromobenzene ND ug/L 11/09/22 16:37 108-86-10.50 1
Bromochloromethane ND ug/L 11/09/22 16:37 74-97-50.50 1
Bromodichloromethane ND ug/L 11/09/22 16:37 75-27-40.50 1
Bromoform ND ug/L 11/09/22 16:37 75-25-20.50 1
Bromomethane ND ug/L 11/09/22 16:37 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 11/09/22 16:37 75-65-050.0 1
n-Butylbenzene ND ug/L 11/09/22 16:37 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/09/22 16:37 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/09/22 16:37 98-06-60.50 1
tert-Butyl Formate ND ug/L 11/09/22 16:37 762-75-450.0 1
Carbon tetrachloride ND ug/L 11/09/22 16:37 56-23-50.50 1
Chlorobenzene ND ug/L 11/09/22 16:37 108-90-70.50 1
Chloroethane ND ug/L 11/09/22 16:37 75-00-31.0 1
Chloroform ND ug/L 11/09/22 16:37 67-66-30.50 1
Chloromethane ND ug/L 11/09/22 16:37 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/09/22 16:37 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/09/22 16:37 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/09/22 16:37 96-12-81.0 1
Dibromochloromethane ND ug/L 11/09/22 16:37 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/09/22 16:37 106-93-40.50 1
Dibromomethane ND ug/L 11/09/22 16:37 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/09/22 16:37 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/09/22 16:37 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/09/22 16:37 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/09/22 16:37 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/09/22 16:37 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/09/22 16:37 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/09/22 16:37 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/09/22 16:37 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/09/22 16:37 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/09/22 16:37 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/09/22 16:37 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/09/22 16:37 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/09/22 16:37 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/09/22 16:37 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/09/22 16:37 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/09/22 16:37 108-20-30.50 1
Ethanol ND ug/L 11/09/22 16:37 64-17-52001
Ethylbenzene ND ug/L 11/09/22 16:37 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 11/09/22 16:37 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 11/09/22 16:37 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/09/22 16:37 98-82-80.50 1
Methylene Chloride ND ug/L 11/09/22 16:37 75-09-22.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 20 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-10 Lab ID:92633465010 Collected:10/26/22 11:30 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether 0.68 ug/L 11/09/22 16:37 1634-04-40.50 1
Naphthalene ND ug/L 11/09/22 16:37 91-20-32.0 1
n-Propylbenzene ND ug/L 11/09/22 16:37 103-65-10.50 1
Styrene ND ug/L 11/09/22 16:37 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/09/22 16:37 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/09/22 16:37 79-34-50.50 1
Tetrachloroethene ND ug/L 11/09/22 16:37 127-18-40.50 1
Toluene ND ug/L 11/09/22 16:37 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/09/22 16:37 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/09/22 16:37 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/09/22 16:37 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/09/22 16:37 79-00-50.50 1
Trichloroethene ND ug/L 11/09/22 16:37 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/09/22 16:37 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/09/22 16:37 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/09/22 16:37 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/09/22 16:37 108-67-80.50 1
Vinyl chloride ND ug/L 11/09/22 16:37 75-01-41.0 1
m&p-Xylene ND ug/L 11/09/22 16:37 179601-23-11.0 1
o-Xylene ND ug/L 11/09/22 16:37 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)88 %11/09/22 16:37 17060-07-070-130 1
4-Bromofluorobenzene (S)94 %11/09/22 16:37 460-00-470-130 1
Toluene-d8 (S)100 %11/09/22 16:37 2037-26-570-130 1
Sample:MW-11 Lab ID:92633465011 Collected:10/27/22 13:00 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/10/22 16:04 75-85-4250025
tert-Amylmethyl ether ND ug/L 11/10/22 16:04 994-05-825025
Benzene ND ug/L 11/10/22 16:04 71-43-212.5 25
Bromobenzene ND ug/L 11/10/22 16:04 108-86-112.5 25
Bromochloromethane ND ug/L 11/10/22 16:04 74-97-512.5 25
Bromodichloromethane ND ug/L 11/10/22 16:04 75-27-412.5 25
Bromoform ND ug/L 11/10/22 16:04 75-25-212.5 25
Bromomethane ND ug/L 11/10/22 16:04 74-83-912525
tert-Butyl Alcohol ND ug/L 11/10/22 16:04 75-65-0125025
n-Butylbenzene ND ug/L 11/10/22 16:04 104-51-812.5 25
sec-Butylbenzene ND ug/L 11/10/22 16:04 135-98-812.5 25
tert-Butylbenzene ND ug/L 11/10/22 16:04 98-06-612.5 25
tert-Butyl Formate ND ug/L 11/10/22 16:04 762-75-4125025
Carbon tetrachloride ND ug/L 11/10/22 16:04 56-23-512.5 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 21 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-11 Lab ID:92633465011 Collected:10/27/22 13:00 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Chlorobenzene ND ug/L 11/10/22 16:04 108-90-712.5 25
Chloroethane ND ug/L 11/10/22 16:04 75-00-325.0 25
Chloroform ND ug/L 11/10/22 16:04 67-66-312.5 25
Chloromethane ND ug/L 11/10/22 16:04 74-87-325.0 25
2-Chlorotoluene ND ug/L 11/10/22 16:04 95-49-812.5 25
4-Chlorotoluene ND ug/L 11/10/22 16:04 106-43-412.5 25
1,2-Dibromo-3-chloropropane ND ug/L 11/10/22 16:04 96-12-825.0 25
Dibromochloromethane ND ug/L 11/10/22 16:04 124-48-112.5 25
1,2-Dibromoethane (EDB)ND ug/L 11/10/22 16:04 106-93-412.5 25
Dibromomethane ND ug/L 11/10/22 16:04 74-95-312.5 25
1,2-Dichlorobenzene ND ug/L 11/10/22 16:04 95-50-112.5 25
1,3-Dichlorobenzene ND ug/L 11/10/22 16:04 541-73-112.5 25
1,4-Dichlorobenzene ND ug/L 11/10/22 16:04 106-46-712.5 25
Dichlorodifluoromethane ND ug/L 11/10/22 16:04 75-71-812.5 25
1,1-Dichloroethane ND ug/L 11/10/22 16:04 75-34-312.5 25
1,2-Dichloroethane ND ug/L 11/10/22 16:04 107-06-212.5 25
1,1-Dichloroethene ND ug/L 11/10/22 16:04 75-35-412.5 25
cis-1,2-Dichloroethene ND ug/L 11/10/22 16:04 156-59-212.5 25
trans-1,2-Dichloroethene ND ug/L 11/10/22 16:04 156-60-512.5 25
1,2-Dichloropropane ND ug/L 11/10/22 16:04 78-87-512.5 25
1,3-Dichloropropane ND ug/L 11/10/22 16:04 142-28-912.5 25
2,2-Dichloropropane ND ug/L 11/10/22 16:04 594-20-712.5 25
1,1-Dichloropropene ND ug/L 11/10/22 16:04 563-58-612.5 25
cis-1,3-Dichloropropene ND ug/L 11/10/22 16:04 10061-01-512.5 25
trans-1,3-Dichloropropene ND ug/L 11/10/22 16:04 10061-02-612.5 25
Diisopropyl ether ND ug/L 11/10/22 16:04 108-20-312.5 25
Ethanol ND ug/L 11/10/22 16:04 64-17-5500025
Ethylbenzene 349 ug/L 11/10/22 16:04 100-41-412.5 25
Ethyl-tert-butyl ether ND ug/L 11/10/22 16:04 637-92-325025
Hexachloro-1,3-butadiene ND ug/L 11/10/22 16:04 87-68-350.0 25
Isopropylbenzene (Cumene)119 ug/L 11/10/22 16:04 98-82-812.5 25
Methylene Chloride ND ug/L 11/10/22 16:04 75-09-250.0 25
Methyl-tert-butyl ether 73.3 ug/L 11/10/22 16:04 1634-04-412.5 25
Naphthalene 586 ug/L 11/10/22 16:04 91-20-350.0 25
n-Propylbenzene 311 ug/L 11/10/22 16:04 103-65-112.5 25
Styrene ND ug/L 11/10/22 16:04 100-42-512.5 25
1,1,1,2-Tetrachloroethane ND ug/L 11/10/22 16:04 630-20-612.5 25
1,1,2,2-Tetrachloroethane ND ug/L 11/10/22 16:04 79-34-512.5 25
Tetrachloroethene ND ug/L 11/10/22 16:04 127-18-412.5 25
Toluene 70.6 ug/L 11/10/22 16:04 108-88-312.5 25
1,2,3-Trichlorobenzene ND ug/L 11/10/22 16:04 87-61-650.0 25
1,2,4-Trichlorobenzene ND ug/L 11/10/22 16:04 120-82-150.0 25
1,1,1-Trichloroethane ND ug/L 11/10/22 16:04 71-55-612.5 25
1,1,2-Trichloroethane ND ug/L 11/10/22 16:04 79-00-512.5 25
Trichloroethene ND ug/L 11/10/22 16:04 79-01-612.5 25
Trichlorofluoromethane ND ug/L 11/10/22 16:04 75-69-425.0 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 22 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-11 Lab ID:92633465011 Collected:10/27/22 13:00 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,2,3-Trichloropropane ND ug/L 11/10/22 16:04 96-18-412.5 25
1,2,4-Trimethylbenzene 4140 ug/L 11/10/22 16:04 95-63-612.5 25
1,3,5-Trimethylbenzene 1160 ug/L 11/10/22 16:04 108-67-812.5 25
Vinyl chloride ND ug/L 11/10/22 16:04 75-01-425.0 25
m&p-Xylene 3870 ug/L 11/10/22 16:04 179601-23-125.0 25
o-Xylene 1530 ug/L 11/10/22 16:04 95-47-612.5 25
Surrogates
1,2-Dichloroethane-d4 (S)85 %11/10/22 16:04 17060-07-070-130 25
4-Bromofluorobenzene (S)94 %11/10/22 16:04 460-00-470-130 25
Toluene-d8 (S)104 %11/10/22 16:04 2037-26-570-130 25
Sample:MW-12 Lab ID:92633465012 Collected:10/27/22 13:30 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/10/22 15:46 75-85-4125012.5
tert-Amylmethyl ether ND ug/L 11/10/22 15:46 994-05-812512.5
Benzene ND ug/L 11/10/22 15:46 71-43-26.2 12.5
Bromobenzene ND ug/L 11/10/22 15:46 108-86-16.2 12.5
Bromochloromethane ND ug/L 11/10/22 15:46 74-97-56.2 12.5
Bromodichloromethane ND ug/L 11/10/22 15:46 75-27-46.2 12.5
Bromoform ND ug/L 11/10/22 15:46 75-25-26.2 12.5
Bromomethane ND ug/L 11/10/22 15:46 74-83-962.5 12.5
tert-Butyl Alcohol ND ug/L 11/10/22 15:46 75-65-062512.5
n-Butylbenzene ND ug/L 11/10/22 15:46 104-51-86.2 12.5
sec-Butylbenzene ND ug/L 11/10/22 15:46 135-98-86.2 12.5
tert-Butylbenzene ND ug/L 11/10/22 15:46 98-06-66.2 12.5
tert-Butyl Formate ND ug/L 11/10/22 15:46 762-75-462512.5
Carbon tetrachloride ND ug/L 11/10/22 15:46 56-23-56.2 12.5
Chlorobenzene ND ug/L 11/10/22 15:46 108-90-76.2 12.5
Chloroethane ND ug/L 11/10/22 15:46 75-00-312.5 12.5
Chloroform ND ug/L 11/10/22 15:46 67-66-36.2 12.5
Chloromethane ND ug/L 11/10/22 15:46 74-87-312.5 12.5
2-Chlorotoluene ND ug/L 11/10/22 15:46 95-49-86.2 12.5
4-Chlorotoluene ND ug/L 11/10/22 15:46 106-43-46.2 12.5
1,2-Dibromo-3-chloropropane ND ug/L 11/10/22 15:46 96-12-812.5 12.5
Dibromochloromethane ND ug/L 11/10/22 15:46 124-48-16.2 12.5
1,2-Dibromoethane (EDB)ND ug/L 11/10/22 15:46 106-93-46.2 12.5
Dibromomethane ND ug/L 11/10/22 15:46 74-95-36.2 12.5
1,2-Dichlorobenzene ND ug/L 11/10/22 15:46 95-50-16.2 12.5
1,3-Dichlorobenzene ND ug/L 11/10/22 15:46 541-73-16.2 12.5
1,4-Dichlorobenzene ND ug/L 11/10/22 15:46 106-46-76.2 12.5
Dichlorodifluoromethane ND ug/L 11/10/22 15:46 75-71-86.2 12.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 23 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-12 Lab ID:92633465012 Collected:10/27/22 13:30 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1-Dichloroethane ND ug/L 11/10/22 15:46 75-34-36.2 12.5
1,2-Dichloroethane ND ug/L 11/10/22 15:46 107-06-26.2 12.5
1,1-Dichloroethene ND ug/L 11/10/22 15:46 75-35-46.2 12.5
cis-1,2-Dichloroethene ND ug/L 11/10/22 15:46 156-59-26.2 12.5
trans-1,2-Dichloroethene ND ug/L 11/10/22 15:46 156-60-56.2 12.5
1,2-Dichloropropane ND ug/L 11/10/22 15:46 78-87-56.2 12.5
1,3-Dichloropropane ND ug/L 11/10/22 15:46 142-28-96.2 12.5
2,2-Dichloropropane ND ug/L 11/10/22 15:46 594-20-76.2 12.5
1,1-Dichloropropene ND ug/L 11/10/22 15:46 563-58-66.2 12.5
cis-1,3-Dichloropropene ND ug/L 11/10/22 15:46 10061-01-56.2 12.5
trans-1,3-Dichloropropene ND ug/L 11/10/22 15:46 10061-02-66.2 12.5
Diisopropyl ether ND ug/L 11/10/22 15:46 108-20-36.2 12.5
Ethanol ND ug/L 11/10/22 15:46 64-17-5250012.5
Ethylbenzene 961 ug/L 11/10/22 15:46 100-41-46.2 12.5
Ethyl-tert-butyl ether ND ug/L 11/10/22 15:46 637-92-312512.5
Hexachloro-1,3-butadiene ND ug/L 11/10/22 15:46 87-68-325.0 12.5
Isopropylbenzene (Cumene)57.8 ug/L 11/10/22 15:46 98-82-86.2 12.5
Methylene Chloride ND ug/L 11/10/22 15:46 75-09-225.0 12.5
Methyl-tert-butyl ether 50.2 ug/L 11/10/22 15:46 1634-04-46.2 12.5
Naphthalene 388 ug/L 11/10/22 15:46 91-20-325.0 12.5
n-Propylbenzene ND ug/L 11/10/22 15:46 103-65-16.2 12.5
Styrene ND ug/L 11/10/22 15:46 100-42-56.2 12.5
1,1,1,2-Tetrachloroethane ND ug/L 11/10/22 15:46 630-20-66.2 12.5
1,1,2,2-Tetrachloroethane ND ug/L 11/10/22 15:46 79-34-56.2 12.5
Tetrachloroethene ND ug/L 11/10/22 15:46 127-18-46.2 12.5
Toluene 294 ug/L 11/10/22 15:46 108-88-36.2 12.5
1,2,3-Trichlorobenzene ND ug/L 11/10/22 15:46 87-61-625.0 12.5
1,2,4-Trichlorobenzene ND ug/L 11/10/22 15:46 120-82-125.0 12.5
1,1,1-Trichloroethane ND ug/L 11/10/22 15:46 71-55-66.2 12.5
1,1,2-Trichloroethane ND ug/L 11/10/22 15:46 79-00-56.2 12.5
Trichloroethene ND ug/L 11/10/22 15:46 79-01-66.2 12.5
Trichlorofluoromethane ND ug/L 11/10/22 15:46 75-69-412.5 12.5
1,2,3-Trichloropropane ND ug/L 11/10/22 15:46 96-18-46.2 12.5
1,2,4-Trimethylbenzene 1450 ug/L 11/10/22 15:46 95-63-66.2 12.5
1,3,5-Trimethylbenzene ND ug/L 11/10/22 15:46 108-67-86.2 12.5
Vinyl chloride ND ug/L 11/10/22 15:46 75-01-412.5 12.5
m&p-Xylene 5000 ug/L 11/10/22 15:46 179601-23-112.5 12.5
o-Xylene 2540 ug/L 11/11/22 13:56 95-47-6 H1,H510.0 20
Surrogates
1,2-Dichloroethane-d4 (S)84 %11/10/22 15:46 17060-07-070-130 12.5
4-Bromofluorobenzene (S)94 %11/10/22 15:46 460-00-470-130 12.5
Toluene-d8 (S)107 %11/10/22 15:46 2037-26-570-130 12.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 24 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-14 Lab ID:92633465013 Collected:10/26/22 12:00 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/09/22 17:49 75-85-440000400
tert-Amylmethyl ether ND ug/L 11/09/22 17:49 994-05-84000400
Benzene 5590 ug/L 11/09/22 17:49 71-43-2200400
Bromobenzene ND ug/L 11/09/22 17:49 108-86-1200400
Bromochloromethane ND ug/L 11/09/22 17:49 74-97-5200400
Bromodichloromethane ND ug/L 11/09/22 17:49 75-27-4200400
Bromoform ND ug/L 11/09/22 17:49 75-25-2200400
Bromomethane ND ug/L 11/09/22 17:49 74-83-92000400
tert-Butyl Alcohol ND ug/L 11/09/22 17:49 75-65-020000400
n-Butylbenzene ND ug/L 11/09/22 17:49 104-51-8200400
sec-Butylbenzene ND ug/L 11/09/22 17:49 135-98-8200400
tert-Butylbenzene ND ug/L 11/09/22 17:49 98-06-6200400
tert-Butyl Formate ND ug/L 11/09/22 17:49 762-75-420000400
Carbon tetrachloride ND ug/L 11/09/22 17:49 56-23-5200400
Chlorobenzene ND ug/L 11/09/22 17:49 108-90-7200400
Chloroethane ND ug/L 11/09/22 17:49 75-00-3400400
Chloroform ND ug/L 11/09/22 17:49 67-66-3200400
Chloromethane ND ug/L 11/09/22 17:49 74-87-3400400
2-Chlorotoluene ND ug/L 11/09/22 17:49 95-49-8200400
4-Chlorotoluene ND ug/L 11/09/22 17:49 106-43-4200400
1,2-Dibromo-3-chloropropane ND ug/L 11/09/22 17:49 96-12-8400400
Dibromochloromethane ND ug/L 11/09/22 17:49 124-48-1200400
1,2-Dibromoethane (EDB)ND ug/L 11/09/22 17:49 106-93-4200400
Dibromomethane ND ug/L 11/09/22 17:49 74-95-3200400
1,2-Dichlorobenzene ND ug/L 11/09/22 17:49 95-50-1200400
1,3-Dichlorobenzene ND ug/L 11/09/22 17:49 541-73-1200400
1,4-Dichlorobenzene ND ug/L 11/09/22 17:49 106-46-7200400
Dichlorodifluoromethane ND ug/L 11/09/22 17:49 75-71-8200400
1,1-Dichloroethane ND ug/L 11/09/22 17:49 75-34-3200400
1,2-Dichloroethane ND ug/L 11/09/22 17:49 107-06-2200400
1,1-Dichloroethene ND ug/L 11/09/22 17:49 75-35-4200400
cis-1,2-Dichloroethene ND ug/L 11/09/22 17:49 156-59-2200400
trans-1,2-Dichloroethene ND ug/L 11/09/22 17:49 156-60-5200400
1,2-Dichloropropane ND ug/L 11/09/22 17:49 78-87-5200400
1,3-Dichloropropane ND ug/L 11/09/22 17:49 142-28-9200400
2,2-Dichloropropane ND ug/L 11/09/22 17:49 594-20-7200400
1,1-Dichloropropene ND ug/L 11/09/22 17:49 563-58-6200400
cis-1,3-Dichloropropene ND ug/L 11/09/22 17:49 10061-01-5200400
trans-1,3-Dichloropropene ND ug/L 11/09/22 17:49 10061-02-6200400
Diisopropyl ether ND ug/L 11/09/22 17:49 108-20-3200400
Ethanol ND ug/L 11/09/22 17:49 64-17-580000400
Ethylbenzene 4730 ug/L 11/09/22 17:49 100-41-4200400
Ethyl-tert-butyl ether ND ug/L 11/09/22 17:49 637-92-34000400
Hexachloro-1,3-butadiene ND ug/L 11/09/22 17:49 87-68-3800400
Isopropylbenzene (Cumene)ND ug/L 11/09/22 17:49 98-82-8200400
Methylene Chloride ND ug/L 11/09/22 17:49 75-09-2800400
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 25 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-14 Lab ID:92633465013 Collected:10/26/22 12:00 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether ND ug/L 11/09/22 17:49 1634-04-4200400
Naphthalene ND ug/L 11/09/22 17:49 91-20-3800400
n-Propylbenzene 378 ug/L 11/09/22 17:49 103-65-1200400
Styrene ND ug/L 11/09/22 17:49 100-42-5200400
1,1,1,2-Tetrachloroethane ND ug/L 11/09/22 17:49 630-20-6200400
1,1,2,2-Tetrachloroethane ND ug/L 11/09/22 17:49 79-34-5200400
Tetrachloroethene ND ug/L 11/09/22 17:49 127-18-4200400
Toluene 67500 ug/L 11/09/22 17:49 108-88-3200400
1,2,3-Trichlorobenzene ND ug/L 11/09/22 17:49 87-61-6800400
1,2,4-Trichlorobenzene ND ug/L 11/09/22 17:49 120-82-1800400
1,1,1-Trichloroethane ND ug/L 11/09/22 17:49 71-55-6200400
1,1,2-Trichloroethane ND ug/L 11/09/22 17:49 79-00-5200400
Trichloroethene ND ug/L 11/09/22 17:49 79-01-6200400
Trichlorofluoromethane ND ug/L 11/09/22 17:49 75-69-4400400
1,2,3-Trichloropropane ND ug/L 11/09/22 17:49 96-18-4200400
1,2,4-Trimethylbenzene 3180 ug/L 11/09/22 17:49 95-63-6200400
1,3,5-Trimethylbenzene 658 ug/L 11/09/22 17:49 108-67-8200400
Vinyl chloride ND ug/L 11/09/22 17:49 75-01-4400400
m&p-Xylene 16400 ug/L 11/09/22 17:49 179601-23-1400400
o-Xylene 8520 ug/L 11/09/22 17:49 95-47-6200400
Surrogates
1,2-Dichloroethane-d4 (S)84 %11/09/22 17:49 17060-07-070-130 400
4-Bromofluorobenzene (S)94 %11/09/22 17:49 460-00-470-130 400
Toluene-d8 (S)100 %11/09/22 17:49 2037-26-570-130 400
Sample:MW-15 Lab ID:92633465014 Collected:10/26/22 12:30 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/09/22 18:07 75-85-450000500
tert-Amylmethyl ether ND ug/L 11/09/22 18:07 994-05-85000500
Benzene 4930 ug/L 11/09/22 18:07 71-43-2250500
Bromobenzene ND ug/L 11/09/22 18:07 108-86-1250500
Bromochloromethane ND ug/L 11/09/22 18:07 74-97-5250500
Bromodichloromethane ND ug/L 11/09/22 18:07 75-27-4250500
Bromoform ND ug/L 11/09/22 18:07 75-25-2250500
Bromomethane ND ug/L 11/09/22 18:07 74-83-92500500
tert-Butyl Alcohol ND ug/L 11/09/22 18:07 75-65-025000500
n-Butylbenzene 489 ug/L 11/09/22 18:07 104-51-8250500
sec-Butylbenzene ND ug/L 11/09/22 18:07 135-98-8250500
tert-Butylbenzene ND ug/L 11/09/22 18:07 98-06-6250500
tert-Butyl Formate ND ug/L 11/09/22 18:07 762-75-425000500
Carbon tetrachloride ND ug/L 11/09/22 18:07 56-23-5250500
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 26 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-15 Lab ID:92633465014 Collected:10/26/22 12:30 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Chlorobenzene ND ug/L 11/09/22 18:07 108-90-7250500
Chloroethane ND ug/L 11/09/22 18:07 75-00-3500500
Chloroform ND ug/L 11/09/22 18:07 67-66-3250500
Chloromethane ND ug/L 11/09/22 18:07 74-87-3500500
2-Chlorotoluene ND ug/L 11/09/22 18:07 95-49-8250500
4-Chlorotoluene ND ug/L 11/09/22 18:07 106-43-4250500
1,2-Dibromo-3-chloropropane ND ug/L 11/09/22 18:07 96-12-8500500
Dibromochloromethane ND ug/L 11/09/22 18:07 124-48-1250500
1,2-Dibromoethane (EDB)ND ug/L 11/09/22 18:07 106-93-4250500
Dibromomethane ND ug/L 11/09/22 18:07 74-95-3250500
1,2-Dichlorobenzene ND ug/L 11/09/22 18:07 95-50-1250500
1,3-Dichlorobenzene ND ug/L 11/09/22 18:07 541-73-1250500
1,4-Dichlorobenzene ND ug/L 11/09/22 18:07 106-46-7250500
Dichlorodifluoromethane ND ug/L 11/09/22 18:07 75-71-8250500
1,1-Dichloroethane ND ug/L 11/09/22 18:07 75-34-3250500
1,2-Dichloroethane ND ug/L 11/09/22 18:07 107-06-2250500
1,1-Dichloroethene ND ug/L 11/09/22 18:07 75-35-4250500
cis-1,2-Dichloroethene ND ug/L 11/09/22 18:07 156-59-2250500
trans-1,2-Dichloroethene ND ug/L 11/09/22 18:07 156-60-5250500
1,2-Dichloropropane ND ug/L 11/09/22 18:07 78-87-5250500
1,3-Dichloropropane ND ug/L 11/09/22 18:07 142-28-9250500
2,2-Dichloropropane ND ug/L 11/09/22 18:07 594-20-7250500
1,1-Dichloropropene ND ug/L 11/09/22 18:07 563-58-6250500
cis-1,3-Dichloropropene ND ug/L 11/09/22 18:07 10061-01-5250500
trans-1,3-Dichloropropene ND ug/L 11/09/22 18:07 10061-02-6250500
Diisopropyl ether ND ug/L 11/09/22 18:07 108-20-3250500
Ethanol ND ug/L 11/09/22 18:07 64-17-5100000500
Ethylbenzene 10400 ug/L 11/09/22 18:07 100-41-4250500
Ethyl-tert-butyl ether ND ug/L 11/09/22 18:07 637-92-35000500
Hexachloro-1,3-butadiene ND ug/L 11/09/22 18:07 87-68-31000500
Isopropylbenzene (Cumene)752 ug/L 11/09/22 18:07 98-82-8250500
Methylene Chloride ND ug/L 11/09/22 18:07 75-09-21000500
Methyl-tert-butyl ether ND ug/L 11/09/22 18:07 1634-04-4250500
Naphthalene 1820 ug/L 11/09/22 18:07 91-20-31000500
n-Propylbenzene 2550 ug/L 11/09/22 18:07 103-65-1250500
Styrene ND ug/L 11/09/22 18:07 100-42-5250500
1,1,1,2-Tetrachloroethane ND ug/L 11/09/22 18:07 630-20-6250500
1,1,2,2-Tetrachloroethane ND ug/L 11/09/22 18:07 79-34-5250500
Tetrachloroethene ND ug/L 11/09/22 18:07 127-18-4250500
Toluene 86300 ug/L 11/09/22 18:07 108-88-3250500
1,2,3-Trichlorobenzene ND ug/L 11/09/22 18:07 87-61-61000500
1,2,4-Trichlorobenzene ND ug/L 11/09/22 18:07 120-82-11000500
1,1,1-Trichloroethane ND ug/L 11/09/22 18:07 71-55-6250500
1,1,2-Trichloroethane ND ug/L 11/09/22 18:07 79-00-5250500
Trichloroethene ND ug/L 11/09/22 18:07 79-01-6250500
Trichlorofluoromethane ND ug/L 11/09/22 18:07 75-69-4500500
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 27 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:MW-15 Lab ID:92633465014 Collected:10/26/22 12:30 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,2,3-Trichloropropane ND ug/L 11/09/22 18:07 96-18-4250500
1,2,4-Trimethylbenzene 15200 ug/L 11/09/22 18:07 95-63-6250500
1,3,5-Trimethylbenzene 4330 ug/L 11/09/22 18:07 108-67-8250500
Vinyl chloride ND ug/L 11/09/22 18:07 75-01-4500500
m&p-Xylene 36600 ug/L 11/09/22 18:07 179601-23-1500500
o-Xylene 17200 ug/L 11/09/22 18:07 95-47-6250500
Surrogates
1,2-Dichloroethane-d4 (S)86 %11/09/22 18:07 17060-07-070-130 500
4-Bromofluorobenzene (S)94 %11/09/22 18:07 460-00-470-130 500
Toluene-d8 (S)99 %11/09/22 18:07 2037-26-570-130 500
Sample:TW-1 Lab ID:92633465015 Collected:10/26/22 13:00 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/09/22 16:19 75-85-41001
tert-Amylmethyl ether ND ug/L 11/09/22 16:19 994-05-810.0 1
Benzene ND ug/L 11/09/22 16:19 71-43-20.50 1
Bromobenzene ND ug/L 11/09/22 16:19 108-86-10.50 1
Bromochloromethane ND ug/L 11/09/22 16:19 74-97-50.50 1
Bromodichloromethane ND ug/L 11/09/22 16:19 75-27-40.50 1
Bromoform ND ug/L 11/09/22 16:19 75-25-20.50 1
Bromomethane ND ug/L 11/09/22 16:19 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 11/09/22 16:19 75-65-050.0 1
n-Butylbenzene ND ug/L 11/09/22 16:19 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/09/22 16:19 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/09/22 16:19 98-06-60.50 1
tert-Butyl Formate ND ug/L 11/09/22 16:19 762-75-450.0 1
Carbon tetrachloride ND ug/L 11/09/22 16:19 56-23-50.50 1
Chlorobenzene ND ug/L 11/09/22 16:19 108-90-70.50 1
Chloroethane ND ug/L 11/09/22 16:19 75-00-31.0 1
Chloroform ND ug/L 11/09/22 16:19 67-66-30.50 1
Chloromethane ND ug/L 11/09/22 16:19 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/09/22 16:19 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/09/22 16:19 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/09/22 16:19 96-12-81.0 1
Dibromochloromethane ND ug/L 11/09/22 16:19 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/09/22 16:19 106-93-40.50 1
Dibromomethane ND ug/L 11/09/22 16:19 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/09/22 16:19 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/09/22 16:19 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/09/22 16:19 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/09/22 16:19 75-71-80.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 28 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:TW-1 Lab ID:92633465015 Collected:10/26/22 13:00 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1-Dichloroethane ND ug/L 11/09/22 16:19 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/09/22 16:19 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/09/22 16:19 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/09/22 16:19 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/09/22 16:19 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/09/22 16:19 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/09/22 16:19 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/09/22 16:19 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/09/22 16:19 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/09/22 16:19 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/09/22 16:19 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/09/22 16:19 108-20-30.50 1
Ethanol ND ug/L 11/09/22 16:19 64-17-52001
Ethylbenzene ND ug/L 11/09/22 16:19 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 11/09/22 16:19 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 11/09/22 16:19 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/09/22 16:19 98-82-80.50 1
Methylene Chloride ND ug/L 11/09/22 16:19 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/09/22 16:19 1634-04-40.50 1
Naphthalene ND ug/L 11/09/22 16:19 91-20-32.0 1
n-Propylbenzene ND ug/L 11/09/22 16:19 103-65-10.50 1
Styrene ND ug/L 11/09/22 16:19 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/09/22 16:19 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/09/22 16:19 79-34-50.50 1
Tetrachloroethene ND ug/L 11/09/22 16:19 127-18-40.50 1
Toluene 0.76 ug/L 11/10/22 10:31 108-88-3 H10.50 1
1,2,3-Trichlorobenzene ND ug/L 11/09/22 16:19 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/09/22 16:19 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/09/22 16:19 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/09/22 16:19 79-00-50.50 1
Trichloroethene ND ug/L 11/09/22 16:19 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/09/22 16:19 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/09/22 16:19 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/09/22 16:19 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/09/22 16:19 108-67-80.50 1
Vinyl chloride ND ug/L 11/09/22 16:19 75-01-41.0 1
m&p-Xylene 1.0 ug/L 11/09/22 16:19 179601-23-11.0 1
o-Xylene 0.63 ug/L 11/09/22 16:19 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)90 %11/09/22 16:19 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %11/09/22 16:19 460-00-470-130 1
Toluene-d8 (S)101 %11/09/22 16:19 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 29 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:DW-1 Lab ID:92633465016 Collected:10/26/22 13:30 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/09/22 16:55 75-85-41001
tert-Amylmethyl ether ND ug/L 11/09/22 16:55 994-05-810.0 1
Benzene ND ug/L 11/09/22 16:55 71-43-20.50 1
Bromobenzene ND ug/L 11/09/22 16:55 108-86-10.50 1
Bromochloromethane ND ug/L 11/09/22 16:55 74-97-50.50 1
Bromodichloromethane ND ug/L 11/09/22 16:55 75-27-40.50 1
Bromoform ND ug/L 11/09/22 16:55 75-25-20.50 1
Bromomethane ND ug/L 11/09/22 16:55 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 11/09/22 16:55 75-65-050.0 1
n-Butylbenzene ND ug/L 11/09/22 16:55 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/09/22 16:55 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/09/22 16:55 98-06-60.50 1
tert-Butyl Formate ND ug/L 11/09/22 16:55 762-75-450.0 1
Carbon tetrachloride ND ug/L 11/09/22 16:55 56-23-50.50 1
Chlorobenzene ND ug/L 11/09/22 16:55 108-90-70.50 1
Chloroethane ND ug/L 11/09/22 16:55 75-00-31.0 1
Chloroform 7.7 ug/L 11/09/22 16:55 67-66-30.50 1
Chloromethane ND ug/L 11/09/22 16:55 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/09/22 16:55 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/09/22 16:55 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/09/22 16:55 96-12-81.0 1
Dibromochloromethane ND ug/L 11/09/22 16:55 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/09/22 16:55 106-93-40.50 1
Dibromomethane ND ug/L 11/09/22 16:55 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/09/22 16:55 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/09/22 16:55 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/09/22 16:55 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/09/22 16:55 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/09/22 16:55 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/09/22 16:55 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/09/22 16:55 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/09/22 16:55 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/09/22 16:55 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/09/22 16:55 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/09/22 16:55 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/09/22 16:55 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/09/22 16:55 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/09/22 16:55 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/09/22 16:55 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/09/22 16:55 108-20-30.50 1
Ethanol ND ug/L 11/09/22 16:55 64-17-52001
Ethylbenzene ND ug/L 11/09/22 16:55 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 11/09/22 16:55 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 11/09/22 16:55 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/09/22 16:55 98-82-80.50 1
Methylene Chloride ND ug/L 11/09/22 16:55 75-09-22.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 30 of 53
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Sample:DW-1 Lab ID:92633465016 Collected:10/26/22 13:30 Received:10/28/22 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether ND ug/L 11/09/22 16:55 1634-04-40.50 1
Naphthalene ND ug/L 11/09/22 16:55 91-20-32.0 1
n-Propylbenzene ND ug/L 11/09/22 16:55 103-65-10.50 1
Styrene ND ug/L 11/09/22 16:55 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/09/22 16:55 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/09/22 16:55 79-34-50.50 1
Tetrachloroethene ND ug/L 11/09/22 16:55 127-18-40.50 1
Toluene 0.63 ug/L 11/09/22 16:55 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/09/22 16:55 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/09/22 16:55 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/09/22 16:55 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/09/22 16:55 79-00-50.50 1
Trichloroethene ND ug/L 11/09/22 16:55 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/09/22 16:55 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/09/22 16:55 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/09/22 16:55 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/09/22 16:55 108-67-80.50 1
Vinyl chloride ND ug/L 11/09/22 16:55 75-01-41.0 1
m&p-Xylene ND ug/L 11/09/22 16:55 179601-23-11.0 1
o-Xylene ND ug/L 11/09/22 16:55 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)89 %11/09/22 16:55 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %11/09/22 16:55 460-00-470-130 1
Toluene-d8 (S)104 %11/09/22 16:55 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 31 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
735800
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92633465001, 92633465006, 92633465007, 92633465010, 92633465013, 92633465014, 92633465015,
92633465016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3829385
Associated Lab Samples:92633465001, 92633465006, 92633465007, 92633465010, 92633465013, 92633465014, 92633465015,
92633465016
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/09/22 12:07
1,1,1-Trichloroethane ug/L ND 0.50 11/09/22 12:07
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/09/22 12:07
1,1,2-Trichloroethane ug/L ND 0.50 11/09/22 12:07
1,1-Dichloroethane ug/L ND 0.50 11/09/22 12:07
1,1-Dichloroethene ug/L ND 0.50 11/09/22 12:07
1,1-Dichloropropene ug/L ND 0.50 11/09/22 12:07
1,2,3-Trichlorobenzene ug/L ND 2.0 11/09/22 12:07
1,2,3-Trichloropropane ug/L ND 0.50 11/09/22 12:07
1,2,4-Trichlorobenzene ug/L ND 2.0 11/09/22 12:07
1,2,4-Trimethylbenzene ug/L ND 0.50 11/09/22 12:07
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/09/22 12:07
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/09/22 12:07
1,2-Dichlorobenzene ug/L ND 0.50 11/09/22 12:07
1,2-Dichloroethane ug/L ND 0.50 11/09/22 12:07
1,2-Dichloropropane ug/L ND 0.50 11/09/22 12:07
1,3,5-Trimethylbenzene ug/L ND 0.50 11/09/22 12:07
1,3-Dichlorobenzene ug/L ND 0.50 11/09/22 12:07
1,3-Dichloropropane ug/L ND 0.50 11/09/22 12:07
1,4-Dichlorobenzene ug/L ND 0.50 11/09/22 12:07
2,2-Dichloropropane ug/L ND 0.50 11/09/22 12:07
2-Chlorotoluene ug/L ND 0.50 11/09/22 12:07
4-Chlorotoluene ug/L ND 0.50 11/09/22 12:07
Benzene ug/L ND 0.50 11/09/22 12:07
Bromobenzene ug/L ND 0.50 11/09/22 12:07
Bromochloromethane ug/L ND 0.50 11/09/22 12:07
Bromodichloromethane ug/L ND 0.50 11/09/22 12:07
Bromoform ug/L ND 0.50 11/09/22 12:07
Bromomethane ug/L ND 5.0 11/09/22 12:07
Carbon tetrachloride ug/L ND 0.50 11/09/22 12:07
Chlorobenzene ug/L ND 0.50 11/09/22 12:07
Chloroethane ug/L ND 1.0 11/09/22 12:07
Chloroform ug/L ND 0.50 11/09/22 12:07
Chloromethane ug/L ND 1.0 11/09/22 12:07
cis-1,2-Dichloroethene ug/L ND 0.50 11/09/22 12:07
cis-1,3-Dichloropropene ug/L ND 0.50 11/09/22 12:07
Dibromochloromethane ug/L ND 0.50 11/09/22 12:07
Dibromomethane ug/L ND 0.50 11/09/22 12:07
Dichlorodifluoromethane ug/L ND 0.50 11/09/22 12:07
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 32 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3829385
Associated Lab Samples:92633465001, 92633465006, 92633465007, 92633465010, 92633465013, 92633465014, 92633465015,
92633465016
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 0.50 11/09/22 12:07
Ethanol ug/L ND 200 11/09/22 12:07
Ethyl-tert-butyl ether ug/L ND 10.0 11/09/22 12:07
Ethylbenzene ug/L ND 0.50 11/09/22 12:07
Hexachloro-1,3-butadiene ug/L ND 2.0 11/09/22 12:07
Isopropylbenzene (Cumene)ug/L ND 0.50 11/09/22 12:07
m&p-Xylene ug/L ND 1.0 11/09/22 12:07
Methyl-tert-butyl ether ug/L ND 0.50 11/09/22 12:07
Methylene Chloride ug/L ND 2.0 11/09/22 12:07
n-Butylbenzene ug/L ND 0.50 11/09/22 12:07
n-Propylbenzene ug/L ND 0.50 11/09/22 12:07
Naphthalene ug/L ND 2.0 11/09/22 12:07
o-Xylene ug/L ND 0.50 11/09/22 12:07
sec-Butylbenzene ug/L ND 0.50 11/09/22 12:07
Styrene ug/L ND 0.50 11/09/22 12:07
tert-Amyl Alcohol ug/L ND 100 11/09/22 12:07
tert-Amylmethyl ether ug/L ND 10.0 11/09/22 12:07
tert-Butyl Alcohol ug/L ND 50.0 11/09/22 12:07
tert-Butyl Formate ug/L ND 50.0 11/09/22 12:07
tert-Butylbenzene ug/L ND 0.50 11/09/22 12:07
Tetrachloroethene ug/L ND 0.50 11/09/22 12:07
Toluene ug/L ND 0.50 11/09/22 12:07
trans-1,2-Dichloroethene ug/L ND 0.50 11/09/22 12:07
trans-1,3-Dichloropropene ug/L ND 0.50 11/09/22 12:07
Trichloroethene ug/L ND 0.50 11/09/22 12:07
Trichlorofluoromethane ug/L ND 1.0 11/09/22 12:07
Vinyl chloride ug/L ND 1.0 11/09/22 12:07
1,2-Dichloroethane-d4 (S)%88 70-130 11/09/22 12:07
4-Bromofluorobenzene (S)%96 70-130 11/09/22 12:07
Toluene-d8 (S)%102 70-130 11/09/22 12:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3829386LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.450 111 60-140
1,1,1-Trichloroethane ug/L 50.750 101 60-140
1,1,2,2-Tetrachloroethane ug/L 54.850 110 60-140
1,1,2-Trichloroethane ug/L 54.850 110 60-140
1,1-Dichloroethane ug/L 49.850 100 60-140
1,1-Dichloroethene ug/L 50.750 101 60-140
1,1-Dichloropropene ug/L 52.450 105 60-140
1,2,3-Trichlorobenzene ug/L 53.550 107 60-140
1,2,3-Trichloropropane ug/L 52.050 104 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 33 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3829386LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 55.250 110 60-140
1,2,4-Trimethylbenzene ug/L 53.750 107 60-140
1,2-Dibromo-3-chloropropane ug/L 50.750 101 60-140
1,2-Dibromoethane (EDB)ug/L 58.450 117 60-140
1,2-Dichlorobenzene ug/L 53.550 107 60-140
1,2-Dichloroethane ug/L 47.650 95 60-140
1,2-Dichloropropane ug/L 54.850 110 60-140
1,3,5-Trimethylbenzene ug/L 53.550 107 60-140
1,3-Dichlorobenzene ug/L 54.450 109 60-140
1,3-Dichloropropane ug/L 54.850 110 60-140
1,4-Dichlorobenzene ug/L 51.450 103 60-140
2,2-Dichloropropane ug/L 50.850 102 60-140
2-Chlorotoluene ug/L 50.850 102 60-140
4-Chlorotoluene ug/L 50.850 102 60-140
Benzene ug/L 51.850 104 60-140
Bromobenzene ug/L 52.950 106 60-140
Bromochloromethane ug/L 54.850 110 60-140
Bromodichloromethane ug/L 47.650 95 60-140
Bromoform ug/L 54.850 110 60-140
Bromomethane ug/L 32.550 65 60-140
Carbon tetrachloride ug/L 52.450 105 60-140
Chlorobenzene ug/L 56.050 112 60-140
Chloroethane ug/L 35.350 71 60-140
Chloroform ug/L 50.450 101 60-140
Chloromethane ug/L 49.550 99 60-140
cis-1,2-Dichloroethene ug/L 51.150 102 60-140
cis-1,3-Dichloropropene ug/L 53.050 106 60-140
Dibromochloromethane ug/L 55.750 111 60-140
Dibromomethane ug/L 56.350 113 60-140
Dichlorodifluoromethane ug/L 52.350 105 60-140
Diisopropyl ether ug/L 50.050 100 60-140
Ethanol ug/L 18902000 95 60-140
Ethyl-tert-butyl ether ug/L 100100 100 60-140
Ethylbenzene ug/L 55.250 110 60-140
Hexachloro-1,3-butadiene ug/L 54.850 110 60-140
Isopropylbenzene (Cumene)ug/L 55.250 110 60-140
m&p-Xylene ug/L 113100 113 60-140
Methyl-tert-butyl ether ug/L 54.750 109 60-140
Methylene Chloride ug/L 50.850 102 60-140
n-Butylbenzene ug/L 54.250 108 60-140
n-Propylbenzene ug/L 53.350 107 60-140
Naphthalene ug/L 54.350 109 60-140
o-Xylene ug/L 55.750 111 60-140
sec-Butylbenzene ug/L 53.150 106 60-140
Styrene ug/L 55.450 111 60-140
tert-Amyl Alcohol ug/L 10401000 104 60-140
tert-Amylmethyl ether ug/L 108100 108 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 34 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3829386LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butyl Alcohol ug/L 483500 97 60-140
tert-Butyl Formate ug/L 423400 106 60-140
tert-Butylbenzene ug/L 45.350 91 60-140
Tetrachloroethene ug/L 56.750 113 60-140
Toluene ug/L 53.650 107 60-140
trans-1,2-Dichloroethene ug/L 52.050 104 60-140
trans-1,3-Dichloropropene ug/L 52.050 104 60-140
Trichloroethene ug/L 57.350 115 60-140
Trichlorofluoromethane ug/L 45.150 90 60-140
Vinyl chloride ug/L 54.550 109 60-140
1,2-Dichloroethane-d4 (S)%86 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3829389MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92633087005
3829390
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 250 103 60-140102 1 30250ND257255
1,1,1-Trichloroethane ug/L 250 95 60-14095 0 30250ND237238
1,1,2,2-Tetrachloroethane ug/L 250 99 60-140100 1 30250ND247250
1,1,2-Trichloroethane ug/L 250 100 60-140103 3 30250ND250258
1,1-Dichloroethane ug/L 250 93 60-14096 3 30250ND234240
1,1-Dichloroethene ug/L 250 100 60-140101 1 30250ND249253
1,1-Dichloropropene ug/L 250 103 60-140102 1 30250ND258255
1,2,3-Trichlorobenzene ug/L 250 91 60-140100 10 30250ND228251
1,2,3-Trichloropropane ug/L 250 95 60-14095 0 30250ND237236
1,2,4-Trichlorobenzene ug/L 250 98 60-140105 6 30250ND246261
1,2,4-Trimethylbenzene ug/L 250 103 60-140109 2 30250451708724
1,2-Dibromo-3-
chloropropane ug/L 250 89 60-14093 4 30250ND223232
1,2-Dibromoethane (EDB)ug/L 250 102 60-140107 5 30250ND260273
1,2-Dichlorobenzene ug/L 250 97 60-140100 4 30250ND242251
1,2-Dichloroethane ug/L 250 87 60-14087 0 3025010.1 228 228
1,2-Dichloropropane ug/L 250 101 60-140105 4 30250ND251263
1,3,5-Trimethylbenzene ug/L 250 105 60-140107 2 3025030.0 291 298
1,3-Dichlorobenzene ug/L 250 99 60-140103 4 30250ND248257
1,3-Dichloropropane ug/L 250 102 60-140101 0 30250ND254254
1,4-Dichlorobenzene ug/L 250 97 60-14097 1 30250ND241243
2,2-Dichloropropane ug/L 250 95 60-14095 1 30250ND236238
2-Chlorotoluene ug/L 250 91 60-140104 13 30250ND228261
4-Chlorotoluene ug/L 250 91 60-140104 13 30250ND228261
Benzene ug/L 250 87 60-14092 1 3025094511601170
Bromobenzene ug/L 250 97 60-140102 5 30250ND242254
Bromochloromethane ug/L 250 103 60-140106 3 30250ND257264
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 35 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3829389MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92633087005
3829390
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromodichloromethane ug/L 250 88 60-14091 3 30250ND220227
Bromoform ug/L 250 96 60-14099 3 30250ND240247
Bromomethane ug/L 250 71 60-14072 1 30250ND179180
Carbon tetrachloride ug/L 250 102 60-140104 2 30250ND254261
Chlorobenzene ug/L 250 103 60-140106 3 30250ND258265
Chloroethane ug/L 250 84 60-14085 1 30250ND210212
Chloroform ug/L 250 97 60-140100 3 30250ND246253
Chloromethane ug/L 250 94 60-14096 2 30250ND235239
cis-1,2-Dichloroethene ug/L 250 97 60-14099 1 3025090.8 332 337
cis-1,3-Dichloropropene ug/L 250 94 60-14099 6 30250ND235249
Dibromochloromethane ug/L 250 99 60-140101 1 30250ND248252
Dibromomethane ug/L 250 101 60-140105 3 30250ND254262
Dichlorodifluoromethane ug/L 250 89 60-14088 1 30250ND223219
Diisopropyl ether ug/L 250 90 60-14091 1 30250ND226228
Ethanol ug/L 10000 92 60-14091 2 3010000ND92109070
Ethyl-tert-butyl ether ug/L 500 92 60-14092 0 30500ND459461
Ethylbenzene ug/L 250 104 60-140106 1 30250198458464
Hexachloro-1,3-butadiene ug/L 250 105 60-140112 6 30250ND262279
Isopropylbenzene
(Cumene)ug/L 250 106 60-140107 1 3025039.4 304 306
m&p-Xylene ug/L 500 111 60-140105 1 30500146020101980
Methyl-tert-butyl ether ug/L 250 100 60-140101 2 30250ND249253
Methylene Chloride ug/L 250 125 60-140116 7 30250ND312291
n-Butylbenzene ug/L 250 108 60-140112 4 30250ND269279
n-Propylbenzene ug/L 250 102 60-140107 4 3025042.5 297 309
Naphthalene ug/L 250 105 60-140112 4 30250227488507
o-Xylene ug/L 250 108 60-140108 0 30250576846847
sec-Butylbenzene ug/L 250 104 60-140108 4 30250ND261271
Styrene ug/L 250 102 60-140103 2 30250ND254259
tert-Amyl Alcohol ug/L 5000 105 60-140108 2 305000ND52605380
tert-Amylmethyl ether ug/L 500 95 60-14098 3 30500ND474491
tert-Butyl Alcohol ug/L 2500 89 60-14088 2 302500ND22302200
tert-Butyl Formate ug/L 2000 85 60-14085 0 302000ND17001700
tert-Butylbenzene ug/L 250 86 60-14093 7 30250ND216232
Tetrachloroethene ug/L 250 121 60-140128 1 30250212024202440
Toluene ug/L 250 98 60-140101 3 3025021.7 267 275
trans-1,2-Dichloroethene ug/L 250 101 60-140101 0 30250ND253251
trans-1,3-Dichloropropene ug/L 250 93 60-14097 4 30250ND233243
Trichloroethene ug/L 250 108 60-140113 3 3025095.4 366 377
Trichlorofluoromethane ug/L 250 92 60-14095 3 30250ND231238
Vinyl chloride ug/L 250 99 60-140102 2 30250ND249254
1,2-Dichloroethane-d4 (S)%88 70-13085
4-Bromofluorobenzene (S)%96 70-13096
Toluene-d8 (S)%96 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 36 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
736156
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92633465002, 92633465003, 92633465004, 92633465005, 92633465009, 92633465011, 92633465012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3831176
Associated Lab Samples:92633465002, 92633465003, 92633465004, 92633465005, 92633465009, 92633465011, 92633465012
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/10/22 10:22
1,1,1-Trichloroethane ug/L ND 0.50 11/10/22 10:22
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/10/22 10:22
1,1,2-Trichloroethane ug/L ND 0.50 11/10/22 10:22
1,1-Dichloroethane ug/L ND 0.50 11/10/22 10:22
1,1-Dichloroethene ug/L ND 0.50 11/10/22 10:22
1,1-Dichloropropene ug/L ND 0.50 11/10/22 10:22
1,2,3-Trichlorobenzene ug/L ND 2.0 11/10/22 10:22
1,2,3-Trichloropropane ug/L ND 0.50 11/10/22 10:22
1,2,4-Trichlorobenzene ug/L ND 2.0 11/10/22 10:22
1,2,4-Trimethylbenzene ug/L ND 0.50 11/10/22 10:22
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/10/22 10:22
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/10/22 10:22
1,2-Dichlorobenzene ug/L ND 0.50 11/10/22 10:22
1,2-Dichloroethane ug/L ND 0.50 11/10/22 10:22
1,2-Dichloropropane ug/L ND 0.50 11/10/22 10:22
1,3,5-Trimethylbenzene ug/L ND 0.50 11/10/22 10:22
1,3-Dichlorobenzene ug/L ND 0.50 11/10/22 10:22
1,3-Dichloropropane ug/L ND 0.50 11/10/22 10:22
1,4-Dichlorobenzene ug/L ND 0.50 11/10/22 10:22
2,2-Dichloropropane ug/L ND 0.50 11/10/22 10:22
2-Chlorotoluene ug/L ND 0.50 11/10/22 10:22
4-Chlorotoluene ug/L ND 0.50 11/10/22 10:22
Benzene ug/L ND 0.50 11/10/22 10:22
Bromobenzene ug/L ND 0.50 11/10/22 10:22
Bromochloromethane ug/L ND 0.50 11/10/22 10:22
Bromodichloromethane ug/L ND 0.50 11/10/22 10:22
Bromoform ug/L ND 0.50 11/10/22 10:22
Bromomethane ug/L ND 5.0 11/10/22 10:22
Carbon tetrachloride ug/L ND 0.50 11/10/22 10:22
Chlorobenzene ug/L ND 0.50 11/10/22 10:22
Chloroethane ug/L ND 1.0 11/10/22 10:22
Chloroform ug/L ND 0.50 11/10/22 10:22
Chloromethane ug/L ND 1.0 11/10/22 10:22
cis-1,2-Dichloroethene ug/L ND 0.50 11/10/22 10:22
cis-1,3-Dichloropropene ug/L ND 0.50 11/10/22 10:22
Dibromochloromethane ug/L ND 0.50 11/10/22 10:22
Dibromomethane ug/L ND 0.50 11/10/22 10:22
Dichlorodifluoromethane ug/L ND 0.50 11/10/22 10:22
Diisopropyl ether ug/L ND 0.50 11/10/22 10:22
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 37 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3831176
Associated Lab Samples:92633465002, 92633465003, 92633465004, 92633465005, 92633465009, 92633465011, 92633465012
Matrix:Water
Analyzed
Ethanol ug/L ND 200 11/10/22 10:22
Ethyl-tert-butyl ether ug/L ND 10.0 11/10/22 10:22
Ethylbenzene ug/L ND 0.50 11/10/22 10:22
Hexachloro-1,3-butadiene ug/L ND 2.0 11/10/22 10:22
Isopropylbenzene (Cumene)ug/L ND 0.50 11/10/22 10:22
m&p-Xylene ug/L ND 1.0 11/10/22 10:22
Methyl-tert-butyl ether ug/L ND 0.50 11/10/22 10:22
Methylene Chloride ug/L ND 2.0 11/10/22 10:22
n-Butylbenzene ug/L ND 0.50 11/10/22 10:22
n-Propylbenzene ug/L ND 0.50 11/10/22 10:22
Naphthalene ug/L ND 2.0 11/10/22 10:22
o-Xylene ug/L ND 0.50 11/10/22 10:22
sec-Butylbenzene ug/L ND 0.50 11/10/22 10:22
Styrene ug/L ND 0.50 11/10/22 10:22
tert-Amyl Alcohol ug/L ND 100 11/10/22 10:22
tert-Amylmethyl ether ug/L ND 10.0 11/10/22 10:22
tert-Butyl Alcohol ug/L ND 50.0 11/10/22 10:22
tert-Butyl Formate ug/L ND 50.0 11/10/22 10:22
tert-Butylbenzene ug/L ND 0.50 11/10/22 10:22
Tetrachloroethene ug/L ND 0.50 11/10/22 10:22
Toluene ug/L ND 0.50 11/10/22 10:22
trans-1,2-Dichloroethene ug/L ND 0.50 11/10/22 10:22
trans-1,3-Dichloropropene ug/L ND 0.50 11/10/22 10:22
Trichloroethene ug/L ND 0.50 11/10/22 10:22
Trichlorofluoromethane ug/L ND 1.0 11/10/22 10:22
Vinyl chloride ug/L ND 1.0 11/10/22 10:22
1,2-Dichloroethane-d4 (S)%90 70-130 11/10/22 10:22
4-Bromofluorobenzene (S)%98 70-130 11/10/22 10:22
Toluene-d8 (S)%102 70-130 11/10/22 10:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3831177LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 54.550 109 60-140
1,1,1-Trichloroethane ug/L 52.850 106 60-140
1,1,2,2-Tetrachloroethane ug/L 53.150 106 60-140
1,1,2-Trichloroethane ug/L 53.750 107 60-140
1,1-Dichloroethane ug/L 51.750 103 60-140
1,1-Dichloroethene ug/L 52.850 106 60-140
1,1-Dichloropropene ug/L 55.750 111 60-140
1,2,3-Trichlorobenzene ug/L 54.650 109 60-140
1,2,3-Trichloropropane ug/L 48.950 98 60-140
1,2,4-Trichlorobenzene ug/L 55.850 112 60-140
1,2,4-Trimethylbenzene ug/L 55.050 110 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 38 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3831177LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 51.850 104 60-140
1,2-Dibromoethane (EDB)ug/L 57.250 114 60-140
1,2-Dichlorobenzene ug/L 53.650 107 60-140
1,2-Dichloroethane ug/L 49.350 99 60-140
1,2-Dichloropropane ug/L 53.750 107 60-140
1,3,5-Trimethylbenzene ug/L 53.950 108 60-140
1,3-Dichlorobenzene ug/L 55.250 110 60-140
1,3-Dichloropropane ug/L 54.750 109 60-140
1,4-Dichlorobenzene ug/L 52.050 104 60-140
2,2-Dichloropropane ug/L 52.750 105 60-140
2-Chlorotoluene ug/L 55.650 111 60-140
4-Chlorotoluene ug/L 55.650 111 60-140
Benzene ug/L 49.850 100 60-140
Bromobenzene ug/L 53.450 107 60-140
Bromochloromethane ug/L 56.850 114 60-140
Bromodichloromethane ug/L 47.450 95 60-140
Bromoform ug/L 54.150 108 60-140
Bromomethane ug/L 38.950 78 60-140
Carbon tetrachloride ug/L 52.650 105 60-140
Chlorobenzene ug/L 55.550 111 60-140
Chloroethane ug/L 36.150 72 60-140
Chloroform ug/L 53.150 106 60-140
Chloromethane ug/L 52.650 105 60-140
cis-1,2-Dichloroethene ug/L 52.150 104 60-140
cis-1,3-Dichloropropene ug/L 52.550 105 60-140
Dibromochloromethane ug/L 54.550 109 60-140
Dibromomethane ug/L 55.450 111 60-140
Dichlorodifluoromethane ug/L 57.550 115 60-140
Diisopropyl ether ug/L 51.050 102 60-140
Ethanol ug/L 20102000 100 60-140
Ethyl-tert-butyl ether ug/L 103100 103 60-140
Ethylbenzene ug/L 54.850 110 60-140
Hexachloro-1,3-butadiene ug/L 57.250 114 60-140
Isopropylbenzene (Cumene)ug/L 55.650 111 60-140
m&p-Xylene ug/L 115100 115 60-140
Methyl-tert-butyl ether ug/L 55.750 111 60-140
Methylene Chloride ug/L 49.950 100 60-140
n-Butylbenzene ug/L 54.550 109 60-140
n-Propylbenzene ug/L 55.150 110 60-140
Naphthalene ug/L 55.450 111 60-140
o-Xylene ug/L 56.150 112 60-140
sec-Butylbenzene ug/L 54.850 110 60-140
Styrene ug/L 55.450 111 60-140
tert-Amyl Alcohol ug/L 10501000 105 60-140
tert-Amylmethyl ether ug/L 106100 106 60-140
tert-Butyl Alcohol ug/L 498500 100 60-140
tert-Butyl Formate ug/L 434400 108 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 39 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3831177LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 47.250 94 60-140
Tetrachloroethene ug/L 55.050 110 60-140
Toluene ug/L 51.450 103 60-140
trans-1,2-Dichloroethene ug/L 54.350 109 60-140
trans-1,3-Dichloropropene ug/L 52.250 104 60-140
Trichloroethene ug/L 55.950 112 60-140
Trichlorofluoromethane ug/L 46.950 94 60-140
Vinyl chloride ug/L 57.250 114 60-140
1,2-Dichloroethane-d4 (S)%90 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3831178MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92634677005
3831179
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 100 124 60-140117 6 30100ND124117
1,1,1-Trichloroethane ug/L 100 115 60-140107 7 30100ND115107
1,1,2,2-Tetrachloroethane ug/L 100 115 60-140111 4 30100ND115111
1,1,2-Trichloroethane ug/L 100 129 60-140119 8 30100ND129119
1,1-Dichloroethane ug/L 100 118 60-140105 12 30100ND118105
1,1-Dichloroethene ug/L 100 119 60-140111 7 30100ND119111
1,1-Dichloropropene ug/L 100 121 60-140115 5 30100ND121115
1,2,3-Trichlorobenzene ug/L 100 116 60-140112 4 30100ND116112
1,2,3-Trichloropropane ug/L 100 106 60-140105 1 30100ND106105
1,2,4-Trichlorobenzene ug/L 100 121 60-140116 4 30100ND121116
1,2,4-Trimethylbenzene ug/L 100 106 60-140111 1 30100758864868
1,2-Dibromo-3-
chloropropane ug/L 100 109 60-140107 2 30100ND109107
1,2-Dibromoethane (EDB)ug/L 100 125 60-140118 6 30100ND125118
1,2-Dichlorobenzene ug/L 100 118 60-140113 4 30100ND118113
1,2-Dichloroethane ug/L 100 105 60-140100 4 30100ND105100
1,2-Dichloropropane ug/L 100 124 60-140116 6 30100ND124116
1,3,5-Trimethylbenzene ug/L 100 132 60-140124 2 30100327459451
1,3-Dichlorobenzene ug/L 100 123 60-140115 7 30100ND123115
1,3-Dichloropropane ug/L 100 120 60-140113 6 30100ND120113
1,4-Dichlorobenzene ug/L 100 114 60-140112 2 30100ND114112
2,2-Dichloropropane ug/L 100 109 60-140101 7 30100ND109101
2-Chlorotoluene ug/L 100 129 60-140109 16 30100ND129109
4-Chlorotoluene ug/L 100 129 60-140109 17 30100ND129109
Benzene ug/L 100 116 60-140112 3 3010050.0 166 162
Bromobenzene ug/L 100 122 60-140112 8 30100ND122112
Bromochloromethane ug/L 100 123 60-140116 6 30100ND123116
Bromodichloromethane ug/L 100 111 60-140101 9 30100ND111101
Bromoform ug/L 100 116 60-140110 5 30100ND116110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 40 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3831178MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92634677005
3831179
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromomethane ug/L 100 78 60-14078 0 30100ND77.7 77.8
Carbon tetrachloride ug/L 100 120 60-140112 7 30100ND120112
Chlorobenzene ug/L 100 126 60-140120 5 30100ND126120
Chloroethane ug/L 100 104 60-14098 5 30100ND10498.2
Chloroform ug/L 100 116 60-140109 6 301007.2 123 117
Chloromethane ug/L 100 108 60-140103 5 30100ND108103
cis-1,2-Dichloroethene ug/L 100 115 60-140109 6 30100ND115109
cis-1,3-Dichloropropene ug/L 100 117 60-140109 7 30100ND117109
Dibromochloromethane ug/L 100 120 60-140114 5 30100ND120114
Dibromomethane ug/L 100 124 60-140116 7 30100ND124116
Dichlorodifluoromethane ug/L 100 105 60-14097 8 30100ND10596.8
Diisopropyl ether ug/L 100 110 60-140102 6 3010025.1 135 127
Ethanol ug/L 4000 103 60-140103 1 304000ND41304110
Ethyl-tert-butyl ether ug/L 200 111 60-140103 8 30200ND222205
Ethylbenzene ug/L 100 124 60-140118 5 301004.9 129 123
Hexachloro-1,3-butadiene ug/L 100 128 60-140123 3 30100ND128123
Isopropylbenzene
(Cumene)ug/L 100 123 60-140116 5 301005.5 129 122
m&p-Xylene ug/L 200 123 60-140137 2 30200121014601480
Methyl-tert-butyl ether ug/L 100 121 60-140116 4 30100ND121116
Methylene Chloride ug/L 100 108 60-140104 4 30100ND108104
n-Butylbenzene ug/L 100 138 60-140126 9 30100ND138126
n-Propylbenzene ug/L 100 121 60-140114 6 301006.1 127 120
Naphthalene ug/L 100 114 60-140115 0 3010020.9 135 136
o-Xylene ug/L 100 118 60-140128 1 30100640758768
sec-Butylbenzene ug/L 100 126 60-140119 5 30100ND126119
Styrene ug/L 100 121 60-140120 0 30100ND121120
tert-Amyl Alcohol ug/L 2000 113 60-140112 0 302000ND22602250
tert-Amylmethyl ether ug/L 200 122 60-140115 5 30200ND244231
tert-Butyl Alcohol ug/L 1000 111 60-140110 1 301000ND11101100
tert-Butyl Formate ug/L 800 77 60-14070 9 30800ND614561
tert-Butylbenzene ug/L 100 107 60-140100 6 30100ND107100
Tetrachloroethene ug/L 100 126 60-140120 5 30100ND126120
Toluene ug/L 100 122 60-140112 7 3010020.6 143 133
trans-1,2-Dichloroethene ug/L 100 119 60-140110 8 30100ND119110
trans-1,3-Dichloropropene ug/L 100 116 60-140109 6 30100ND116109
Trichloroethene ug/L 100 131 60-140123 6 30100ND131123
Trichlorofluoromethane ug/L 100 109 60-140101 8 30100ND109101
Vinyl chloride ug/L 100 117 60-140110 7 30100ND117110
1,2-Dichloroethane-d4 (S)%85 70-13085
4-Bromofluorobenzene (S)%95 70-13096
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 41 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
736556
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92633465008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3833366
Associated Lab Samples:92633465008
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/11/22 15:08
1,1,1-Trichloroethane ug/L ND 0.50 11/11/22 15:08
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/11/22 15:08
1,1,2-Trichloroethane ug/L ND 0.50 11/11/22 15:08
1,1-Dichloroethane ug/L ND 0.50 11/11/22 15:08
1,1-Dichloroethene ug/L ND 0.50 11/11/22 15:08
1,1-Dichloropropene ug/L ND 0.50 11/11/22 15:08
1,2,3-Trichlorobenzene ug/L ND 2.0 11/11/22 15:08
1,2,3-Trichloropropane ug/L ND 0.50 11/11/22 15:08
1,2,4-Trichlorobenzene ug/L ND 2.0 11/11/22 15:08
1,2,4-Trimethylbenzene ug/L ND 0.50 11/11/22 15:08
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/11/22 15:08
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/11/22 15:08
1,2-Dichlorobenzene ug/L ND 0.50 11/11/22 15:08
1,2-Dichloroethane ug/L ND 0.50 11/11/22 15:08
1,2-Dichloropropane ug/L ND 0.50 11/11/22 15:08
1,3,5-Trimethylbenzene ug/L ND 0.50 11/11/22 15:08
1,3-Dichlorobenzene ug/L ND 0.50 11/11/22 15:08
1,3-Dichloropropane ug/L ND 0.50 11/11/22 15:08
1,4-Dichlorobenzene ug/L ND 0.50 11/11/22 15:08
2,2-Dichloropropane ug/L ND 0.50 11/11/22 15:08
2-Chlorotoluene ug/L ND 0.50 11/11/22 15:08
4-Chlorotoluene ug/L ND 0.50 11/11/22 15:08
Benzene ug/L ND 0.50 11/11/22 15:08
Bromobenzene ug/L ND 0.50 11/11/22 15:08
Bromochloromethane ug/L ND 0.50 11/11/22 15:08
Bromodichloromethane ug/L ND 0.50 11/11/22 15:08
Bromoform ug/L ND 0.50 11/11/22 15:08
Bromomethane ug/L ND 5.0 11/11/22 15:08
Carbon tetrachloride ug/L ND 0.50 11/11/22 15:08
Chlorobenzene ug/L ND 0.50 11/11/22 15:08
Chloroethane ug/L ND 1.0 11/11/22 15:08
Chloroform ug/L ND 0.50 11/11/22 15:08
Chloromethane ug/L ND 1.0 11/11/22 15:08
cis-1,2-Dichloroethene ug/L ND 0.50 11/11/22 15:08
cis-1,3-Dichloropropene ug/L ND 0.50 11/11/22 15:08
Dibromochloromethane ug/L ND 0.50 11/11/22 15:08
Dibromomethane ug/L ND 0.50 11/11/22 15:08
Dichlorodifluoromethane ug/L ND 0.50 11/11/22 15:08
Diisopropyl ether ug/L ND 0.50 11/11/22 15:08
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
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Kernersville, NC 27284
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Page 42 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3833366
Associated Lab Samples:92633465008
Matrix:Water
Analyzed
Ethanol ug/L ND 200 11/11/22 15:08
Ethyl-tert-butyl ether ug/L ND 10.0 11/11/22 15:08
Ethylbenzene ug/L ND 0.50 11/11/22 15:08
Hexachloro-1,3-butadiene ug/L ND 2.0 11/11/22 15:08
Isopropylbenzene (Cumene)ug/L ND 0.50 11/11/22 15:08
m&p-Xylene ug/L ND 1.0 11/11/22 15:08
Methyl-tert-butyl ether ug/L ND 0.50 11/11/22 15:08
Methylene Chloride ug/L ND 2.0 11/11/22 15:08
n-Butylbenzene ug/L ND 0.50 11/11/22 15:08
n-Propylbenzene ug/L ND 0.50 11/11/22 15:08
Naphthalene ug/L ND 2.0 11/11/22 15:08
o-Xylene ug/L ND 0.50 11/11/22 15:08
sec-Butylbenzene ug/L ND 0.50 11/11/22 15:08
Styrene ug/L ND 0.50 11/11/22 15:08
tert-Amyl Alcohol ug/L ND 100 11/11/22 15:08
tert-Amylmethyl ether ug/L ND 10.0 11/11/22 15:08
tert-Butyl Alcohol ug/L ND 50.0 11/11/22 15:08
tert-Butyl Formate ug/L ND 50.0 11/11/22 15:08
tert-Butylbenzene ug/L ND 0.50 11/11/22 15:08
Tetrachloroethene ug/L ND 0.50 11/11/22 15:08
Toluene ug/L ND 0.50 11/11/22 15:08
trans-1,2-Dichloroethene ug/L ND 0.50 11/11/22 15:08
trans-1,3-Dichloropropene ug/L ND 0.50 11/11/22 15:08
Trichloroethene ug/L ND 0.50 11/11/22 15:08
Trichlorofluoromethane ug/L ND 1.0 11/11/22 15:08
Vinyl chloride ug/L ND 1.0 11/11/22 15:08
1,2-Dichloroethane-d4 (S)%100 70-130 11/11/22 15:08
4-Bromofluorobenzene (S)%102 70-130 11/11/22 15:08
Toluene-d8 (S)%101 70-130 11/11/22 15:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3833367LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.150 100 60-140
1,1,1-Trichloroethane ug/L 51.050 102 60-140
1,1,2,2-Tetrachloroethane ug/L 49.650 99 60-140
1,1,2-Trichloroethane ug/L 49.050 98 60-140
1,1-Dichloroethane ug/L 47.050 94 60-140
1,1-Dichloroethene ug/L 49.650 99 60-140
1,1-Dichloropropene ug/L 55.750 111 60-140
1,2,3-Trichlorobenzene ug/L 51.550 103 60-140
1,2,3-Trichloropropane ug/L 46.650 93 60-140
1,2,4-Trichlorobenzene ug/L 48.950 98 60-140
1,2,4-Trimethylbenzene ug/L 48.250 96 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 43 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3833367LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 48.850 98 60-140
1,2-Dibromoethane (EDB)ug/L 50.350 101 60-140
1,2-Dichlorobenzene ug/L 48.850 98 60-140
1,2-Dichloroethane ug/L 48.350 97 60-140
1,2-Dichloropropane ug/L 48.050 96 60-140
1,3,5-Trimethylbenzene ug/L 50.350 101 60-140
1,3-Dichlorobenzene ug/L 49.250 98 60-140
1,3-Dichloropropane ug/L 48.550 97 60-140
1,4-Dichlorobenzene ug/L 47.650 95 60-140
2,2-Dichloropropane ug/L 50.450 101 60-140
2-Chlorotoluene ug/L 49.150 98 60-140
4-Chlorotoluene ug/L 49.150 98 60-140
Benzene ug/L 46.150 92 60-140
Bromobenzene ug/L 48.450 97 60-140
Bromochloromethane ug/L 49.750 99 60-140
Bromodichloromethane ug/L 49.250 98 60-140
Bromoform ug/L 53.550 107 60-140
Bromomethane ug/L 47.950 96 60-140
Carbon tetrachloride ug/L 50.050 100 60-140
Chlorobenzene ug/L 48.650 97 60-140
Chloroethane ug/L 44.150 88 60-140
Chloroform ug/L 47.850 96 60-140
Chloromethane ug/L 56.250 112 60-140
cis-1,2-Dichloroethene ug/L 49.150 98 60-140
cis-1,3-Dichloropropene ug/L 50.550 101 60-140
Dibromochloromethane ug/L 51.250 102 60-140
Dibromomethane ug/L 48.750 97 60-140
Dichlorodifluoromethane ug/L 50.150 100 60-140
Diisopropyl ether ug/L 49.450 99 60-140
Ethanol ug/L 18702000 94 60-140
Ethyl-tert-butyl ether ug/L 95.3100 95 60-140
Ethylbenzene ug/L 47.950 96 60-140
Hexachloro-1,3-butadiene ug/L 51.450 103 60-140
Isopropylbenzene (Cumene)ug/L 48.750 97 60-140
m&p-Xylene ug/L 98.5100 98 60-140
Methyl-tert-butyl ether ug/L 50.250 100 60-140
Methylene Chloride ug/L 48.650 97 60-140
n-Butylbenzene ug/L 50.550 101 60-140
n-Propylbenzene ug/L 48.950 98 60-140
Naphthalene ug/L 50.050 100 60-140
o-Xylene ug/L 50.250 100 60-140
sec-Butylbenzene ug/L 48.050 96 60-140
Styrene ug/L 50.350 101 60-140
tert-Amyl Alcohol ug/L 9881000 99 60-140
tert-Amylmethyl ether ug/L 97.5100 98 60-140
tert-Butyl Alcohol ug/L 504500 101 60-140
tert-Butyl Formate ug/L 407400 102 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 44 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3833367LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 43.050 86 60-140
Tetrachloroethene ug/L 50.150 100 60-140
Toluene ug/L 47.650 95 60-140
trans-1,2-Dichloroethene ug/L 50.550 101 60-140
trans-1,3-Dichloropropene ug/L 50.850 102 60-140
Trichloroethene ug/L 50.750 101 60-140
Trichlorofluoromethane ug/L 45.050 90 60-140
Vinyl chloride ug/L 54.650 109 60-140
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3833368MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92635052001
3833369
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 5000 109 60-140113 3 305000ND54705660
1,1,1-Trichloroethane ug/L 5000 113 60-140113 0 305000ND56605630
1,1,2,2-Tetrachloroethane ug/L 5000 103 60-140109 6 305000ND51505460
1,1,2-Trichloroethane ug/L 5000 105 60-140108 4 305000ND52305410
1,1-Dichloroethane ug/L 5000 106 60-140106 1 305000ND52905320
1,1-Dichloroethene ug/L 5000 116 60-140113 3 305000ND58205650
1,1-Dichloropropene ug/L 5000 123 60-140124 1 305000ND61606220
1,2,3-Trichlorobenzene ug/L 5000 99 60-140112 12 305000ND49705600
1,2,3-Trichloropropane ug/L 5000 96 60-140106 10 305000ND47805290
1,2,4-Trichlorobenzene ug/L 5000 103 60-140109 6 305000ND51305440
1,2,4-Trimethylbenzene ug/L 5000 111 60-140115 3 305000182073507570
1,2-Dibromo-3-
chloropropane ug/L 5000 99 60-140109 9 305000ND49705430
1,2-Dibromoethane (EDB)ug/L 5000 107 60-140111 4 305000ND53505550
1,2-Dichlorobenzene ug/L 5000 106 60-140110 4 305000ND52905490
1,2-Dichloroethane ug/L 5000 108 60-140104 3 305000ND53905210
1,2-Dichloropropane ug/L 5000 104 60-140105 1 305000ND52105270
1,3,5-Trimethylbenzene ug/L 5000 112 60-140117 4 30500045260706320
1,3-Dichlorobenzene ug/L 5000 108 60-140112 4 305000ND54005600
1,3-Dichloropropane ug/L 5000 103 60-140108 4 305000ND51405380
1,4-Dichlorobenzene ug/L 5000 104 60-140108 4 305000ND52205420
2,2-Dichloropropane ug/L 5000 111 60-140109 2 305000ND55505470
2-Chlorotoluene ug/L 5000 109 60-14098 10 305000ND54504920
4-Chlorotoluene ug/L 5000 109 60-14098 10 305000ND54504920
Benzene ug/L 5000 108 60-140114 2 305000137001910019400
Bromobenzene ug/L 5000 108 60-140109 1 305000ND53905460
Bromochloromethane ug/L 5000 107 60-140111 3 305000ND53605530
Bromodichloromethane ug/L 5000 106 60-140109 3 305000ND52805430
Bromoform ug/L 5000 108 60-140112 4 305000ND54005600
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 45 of 53
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3833368MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92635052001
3833369
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromomethane ug/L 5000 103 60-140107 3 305000ND51505330
Carbon tetrachloride ug/L 5000 114 60-140118 3 305000ND56905890
Chlorobenzene ug/L 5000 107 60-140111 3 305000ND53705530
Chloroethane ug/L 5000 121 60-140121 0 305000ND60706070
Chloroform ug/L 5000 108 60-140102 5 305000ND53805100
Chloromethane ug/L 5000 128 60-140124 3 305000ND64206210
cis-1,2-Dichloroethene ug/L 5000 109 60-140108 1 305000ND54405400
cis-1,3-Dichloropropene ug/L 5000 108 60-140111 2 305000ND54105530
Dibromochloromethane ug/L 5000 106 60-140107 1 305000ND53005370
Dibromomethane ug/L 5000 103 60-140106 3 305000ND51705320
Dichlorodifluoromethane ug/L 5000 121 60-140118 2 305000ND60505910
Diisopropyl ether ug/L 5000 107 60-140109 1 305000203073907460
Ethanol ug/L 200000 102 60-140104 1 30200000ND205000208000
Ethyl-tert-butyl ether ug/L 10000 100 60-140101 0 3010000ND1000010100
Ethylbenzene ug/L 5000 109 60-140114 3 305000280082608470
Hexachloro-1,3-butadiene ug/L 5000 111 60-140116 4 305000ND55505790
Isopropylbenzene
(Cumene)ug/L 5000 107 60-140111 3 30500097.4J 5430 5620
m&p-Xylene ug/L 10000 112 60-140115 1 3010000110002230022500
Methyl-tert-butyl ether ug/L 5000 103 60-140105 2 30500048256205740
Methylene Chloride ug/L 5000 96 60-14099 3 305000ND48104930
n-Butylbenzene ug/L 5000 110 60-140114 4 305000ND54905720
n-Propylbenzene ug/L 5000 110 60-140115 4 30500025057706010
Naphthalene ug/L 5000 104 60-140112 7 305000475J56706090
o-Xylene ug/L 5000 110 60-140117 3 30500052701080011100
sec-Butylbenzene ug/L 5000 112 60-140115 2 305000ND56005730
Styrene ug/L 5000 109 60-140112 2 305000ND54705600
tert-Amyl Alcohol ug/L 100000 101 60-140110 9 30100000ND101000110000
tert-Amylmethyl ether ug/L 10000 105 60-140110 4 3010000ND1050011000
tert-Butyl Alcohol ug/L 50000 94 60-140105 11 3050000ND4710052700
tert-Butyl Formate ug/L 40000 103 60-140105 2 3040000ND4100041900
tert-Butylbenzene ug/L 5000 98 60-140100 2 305000ND49205020
Tetrachloroethene ug/L 5000 111 60-140114 3 305000ND55505710
Toluene ug/L 5000 110 60-140124 2 305000373004290043500
trans-1,2-Dichloroethene ug/L 5000 116 60-140111 4 305000ND57805560
trans-1,3-Dichloropropene ug/L 5000 106 60-140111 5 305000ND52805530
Trichloroethene ug/L 5000 112 60-140117 4 305000ND56105860
Trichlorofluoromethane ug/L 5000 116 60-140116 1 305000ND58105780
Vinyl chloride ug/L 5000 127 60-140126 1 305000ND63606300
1,2-Dichloroethane-d4 (S)%99 70-13094
4-Bromofluorobenzene (S)%100 70-13099
Toluene-d8 (S)%99 70-130100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
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1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 46 of 53
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analysis conducted outside the EPA method holding time.H1
Reanalysis conducted in excess of EPA method holding time. Results confirm original analysis performed in hold time.H5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
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1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 47 of 53
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92633465
Konnoak Texaco #13-111
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92633465001 735800MW-1 SM 6200B
92633465002 736156MW-2 SM 6200B
92633465003 736156MW-3 SM 6200B
92633465004 736156MW-4 SM 6200B
92633465005 736156MW-5 SM 6200B
92633465006 735800MW-6 SM 6200B
92633465007 735800MW-7 SM 6200B
92633465008 736556MW-8 SM 6200B
92633465009 736156MW-9 SM 6200B
92633465010 735800MW-10 SM 6200B
92633465011 736156MW-11 SM 6200B
92633465012 736156MW-12 SM 6200B
92633465013 735800MW-14 SM 6200B
92633465014 735800MW-15 SM 6200B
92633465015 735800TW-1 SM 6200B
92633465016 735800DW-1 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/11/2022 04:47 PM
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1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 48 of 53
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