WS-8955_44197_CA_MRP_20221031

GROUNDWATER MONITORING REPORT

RAY’S QUICK STOP
7610 NC HIGHWAY 87 S.
SNOW CAMP, ALAMANCE COUNTY, NORTH CAROLINA
GROUNDWATER INCIDENT: 44197 FACILITY ID: 00-0-0000023858 SITE RISK: HIGH LATITUDE: N 35.906644° LONGITUDE: W 79.307045° OCTOBER 31, 2022

FORMER UST OWNER: Ray’s Quick Stop, LLC 7319 Morrow Mill Road Chapel Hill, NC 27516 Phone Number: [phone]

UST OWNER / OPERATOR / PROPERTY OWNER: KNN, LLC 7610 NC Highway 87 S. Snow Camp, NC 27349-9835 Phone Number: [phone]

CONSULTANT:
Paragon Environmental Consultants, Inc. [e-mail] P. O. Box 157 Thomasville, NC 27361-0157 Phone Number: [phone] ANALYTICAL LABORATORY:
Waypoint Analytical, LLC State Certification Number: #402 449 Springbrook Road Charlotte, NC 28224-0543 Phone Number: [phone] RELEASE INFORMATION:
Date Discovered: 5/9/13 Estimated Quantity of Release: Unknown Cause of Release: Unknown Source of Release: Gasoline USTs Size and Contents: Two (2) 8,000 Gallon Gasoline USTs and One (1) 4,000 Gallon Gasoline UST

October 31, 2022

Thomas Ray
Ray’s Quick Stop, LLC 7319 Morrow Mill Road Chapel Hill, NC 27516 Reference: Groundwater Monitoring Report Ray’s Quick Stop 7610 NC Highway 87 S. Snow Camp, Alamance County, North Carolina Groundwater Incident # 44197 Facility ID #00-0-0000023858

Dear Mr. Ray:

In accordance with an approved Task Authorization Form (TAF) dated September 26, 2022
from the North Carolina Department of Environmental Quality (NCDEQ), contained
herein is a Groundwater Monitoring Report for the release which occurred at the above
referenced facility. The field activities for this project consisted of the sampling of seven
existing monitor wells and one supply well with the laboratory analyses of the collected
groundwater samples.

All activities were conducted in accordance with the NCDEQ guidelines and the
requirements of 15A NCAC 2L .0115. Mr. Clifton, if you have any questions regarding
this report, please contact our office.
Sincerely,
Benjamin W. Robinson, L.G.
Paragon Environmental Consultants, Inc.

R22-1326
PARAGON
Environmental Consultants, Inc.
P.O. Box 157 • Thomasville, NC 27361-0157
Business Ph: [phone] • Fax: [phone]
EXECUTIVE SUMMARY

1. Free Product: Free product has not ever been detected in any monitor well, boring, or excavation at the site.

2. Contaminant Mass: The contaminant mass in the soil has been calculated from the data collected during the Limited Site Assessment (LSA) and Comprehensive Site Assessment (CSA), which is the most recent soil data collected at the site. The contaminant mass in the soil was calculated to be approximately 4.37 kilograms (kg). The contaminant mass in the groundwater has been calculated from the data of the groundwater samples collected on October 4, 2022. The current contaminant mass in the groundwater was calculated to be approximately 0.0302 kg. The total contaminant mass in the soil and groundwater has been calculated to be approximately 4.4002 kg. This value is less than the historical maximum contaminant mass of 4.8565 kg, calculated during from data obtained during the CSA activities.

3. Maximum Concentrations of Dissolved Groundwater Contaminants:

Contaminant Result Well ID 2L Standard
C9-C18 Aliphatics 878 ug/L (MW-1) 700 ug/L
C9-C22 Aromatics 424 ug/L (MW-1) 200 ug/L

4. Extent of Dissolved Groundwater Contamination:

The plume of dissolved groundwater contamination is currently at the smallest
extent to date. Historically, the plume has extended from the source area around
the USTs down-gradient towards the intersection of NC Highway 87 and
Greensboro / Chapel Hill Road. The two main contaminants of concern during the
CSA (MTBE and C5-C8 Aliphatics) have decreased to concentrations that are
below the 2L Standards in the two impacted monitor wells. MW-1, which is down-
gradient of the USTs, currently contains the highest contaminant concentrations.
Currently, 2L Violations are only present in MW-1.
5. Maximum Soil Contaminant Concentrations (Collected during the LSA activities in 2013 and during the CSA activities in 2015): Contaminant Result Sample ID Lowest MSCC Benzene 0.014 mg/kg (GP-12) 0.0072 mg/kg n-Butylbenzene 4.88 mg/kg (GP-14) 2.4 mg/kg sec-Butylbenzene 2.46 mg/kg (GP-14) 2.2 mg/kg p-Isopropyltoluene 2.06 mg/kg (GP-14) 0.12 mg/kg Naphthalene 7.28 mg/kg (GP-14) 0.2 mg/kg
1,2,4-Trimethylbenzene 11.7 mg/kg (GP-14) 6.6 mg/kg
MTBE 5.01 mg/kg (GP-12) 0.085 mg/kg
C5-C8 Volatile Aliphatics 74.8 mg/kg (GP-14) 68 mg/kg
C9-C18 Aliphatics (total) 2,650 mg/kg (GP-14) 540 mg/kg
C9-C22 Aromatics (total) 783 mg/kg (GP-14) 31 mg/kg

6. Remedial Action Plan:

There has never been any remedial action plan implemented at this site. However, natural attenuation has been effective at reducing contaminant concentrations at this site. MW-1 contained MTBE at a concentration of 953 micrograms per Liter (ug/L) in 2013. During the most recent sampling event conducted on October 4, 2022, MTBE had decreased to a concentration of 1.3 ug/L. Similar reductions due to natural attenuation have occurred in vertical extent well VEW-1.

7. Impacted Receptors:

During the most recent sampling event conducted on October 4, 2022, the supply
well serving the store building and the Eli Whitney Fire Department was below the
laboratory detection limits for all target compounds by EPA Methods 6200B and
VPH. The other supply wells within 1,000’ of the petroleum release source area
have never been sampled, but are not considered to be at imminent risk of impact.

TABLE OF CONTENTS

Section Page 1.0 Site History and Characterization 1.1 Introduction .................................................................... 1 1.2 Scope of Services ........................................................... 1 2.0 Presentation of Current Site Assessment Information / Comparison to Historical Assessment Information 2.1 Historical Soil Assessment Information ........................ 2 2.2 Groundwater Flow Direction and Gradient ................... 2 2.3 Monitor Well Sampling and Analyses ........................... 3 2.4 Regional / Site Geology and Hydrogeology .................. 3 2.5 Plume Development ....................................................... 4 3.0 Monitored Natural Attenuation 3.1 Natural Source Zone Depletion Status ........................... 5 4.0 Conclusions 4.1 General Summary .......................................................... 5 4.2 Recommendations .......................................................... 6 4.3 Limitations ..................................................................... 6 5.0 Statements and Certification 5.1 Statements ...................................................................... 6 5.2 Certification ................................................................... 7

LIST OF FIGURES Figure 1: Project Location Figure 2: Site Layout, UST Locations, and Monitor Well Locations Figure 3: Soil Concentrations Map Figure 3A: Soil Cross-Sections C to C’ and D to D’ Figure 4: Potentiometric Surface Map (10/4/22) Figure 5: Groundwater Analytical Results Map Figure 6: Shallow Well C9-C18 Aliphatics Isoconcentration Map Figure 6A: C9-C18 Aliphatics Isoconcentration Cross-Section A to A’ Figure 6B: C9-C18 Aliphatics Isoconcentration Cross-Section B to B’ Figure 7: Shallow Well C9-C22 Aromatics Isoconcentration Map Figure 7A: C9-C22 Aromatics Isoconcentration Cross-Section A to A’ Figure 7B: C9-C22 Aromatics Isoconcentration Cross-Section B to B’ Figure 8: Supply Well Locations Map

LIST OF TABLES Table 1: Site History Table 2: Water Supply Well Information Table 3: Summary of Soil Analytical Results Table 4: Summary of Groundwater Analytical Results Table 5: Monitoring Well Information and Groundwater Elevations Table 6: Evaluation of Change in Contaminant Mass Table 6A: Contaminant Mass Calculation Data

APPENDICES Appendix A: Historical Sampling Results Appendix B: Contaminant Concentrations vs. Time Graphs Appendix C: Compilation of Costs / Chronology of Remediation Activities Appendix D: Laboratory Analytical Results
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GROUNDWATER MONITORING REPORT Ray’s Quick Stop 7610 NC Highway 87 S. Snow Camp, North Carolina

1.0 Site History and Characterization

1.1 Introduction

Ray’s Quick Stop, LLC formerly owned and operated a facility located at 7610 NC Highway 87 S. in Snow Camp, NC. This property contains one permanent structure that is used as a convenience store which is referred to as Ray’s Quick Stop. Figure 1 illustrates the location of this facility on the Saxapahaw Quadrangle U.S.G.S. Topographic Map. The site currently contains two (2) 8,000 gallon gasoline USTs and one (1) 4,000 gallon gasoline UST which are used for the retail sale of petroleum. Figure 2 illustrates the site layout of this facility and the location of the USTs. Information regarding the ownership of the regulated USTs which are located at this facility is contained in Table 1. Soil contamination at a maximum level of 1,000 milligrams per kilogram (mg/kg) by EPA Method 5030 was detected adjacent to the gasoline USTs during a Phase II Environmental Site Assessment performed in May of 2013. A Phase I and II Limited Site Assessment was submitted to the DWM on December 12, 2013 for this facility. A Comprehensive Site Assessment (CSA) was prepared by Paragon and submitted to the DWM on February 20, 2020. A Supplement to the CSA was prepared by Paragon and submitted to the DWM on July 16, 2015. The site has been ranked as High Risk based on supply wells in use for consumption. Information about the supply wells is contained in Table 2. During the most recent sampling event conducted on October 4, 2022, the supply well serving the store building and the Eli Whitney Fire Department was below the laboratory detection limits for all target compounds by EPA Methods 6200B and VPH. The other supply wells within 1,000’ of the petroleum release source area have never been sampled, but are not considered to be at imminent risk of impact. 1.2 Scope of Services

Contained herein are the results of a groundwater sampling event as approved by the
NCDEQ in an approved TAF dated September 26, 2022. This Groundwater Monitoring
Report contains documentation concerning the following activities which have been
conducted at this facility:

o Sampling of seven monitor wells and one supply well conducted by Paragon on
October 4, 2022.

o Laboratory analyses of groundwater samples conducted by Waypoint Analytical, LLC of Charlotte, NC.

o The approximate groundwater flow direction and hydraulic gradient at the site calculated by Paragon.

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2.0 Presentation of Current Site Assessment Information / Comparison to Historical Assessment Information 2.1 Historical Soil Assessment Information On July 15, 2013 one Geoprobe® sample point was advanced near the center gasoline UST to obtain soil samples to complete the LSA requirements. One soil sample was collected for analysis from a depth of 15 feet below the land surface. This soil sample was submitted to Meritech, Inc. for analyses by EPA Method 8260 plus MTBE and IPE. The laboratory analytical results showed no petroleum compounds in excess of the lowest Maximum Soil Contaminant Concentrations (MSCCs). Four additional Geoprobe® sample points were advanced at this facility to delineate the soil contamination in the gasoline tank area. One sample was collected from each Geoprobe® point at depth of 7 ½ feet below surface grade to be submitted to Meritech, Inc. for laboratory analyses by EPA Method 8260 plus MTBE and IPE in addition to Volatile Petroleum Hydrocarbons (VPH). Three of the samples showed Method 8260 compounds and VPH fraction classes in excess of the lowest Maximum Soil Contaminant Concentrations (MSCCs). MTBE was detected at levels which ranged in concentration from a minimum of 0.046 mg/kg to the maximum of 5.01 mg/kg which exceeds the lowest MSCC. No further soil delineation was conducted in the directions which were above the lowest MSCCs due to underground utilities and the store building in those directions at Ray’s Quick Stop. Based on the soil assessment at 7610 NC Highway 87 S., it would appear that most of the gasoline impacted soils are situated beneath the northwest ends of the three existing gasoline USTs. The majority of the contaminated soil underneath the three tanks is also located beneath the shallow groundwater table at the project site. Figure 3 illustrates the soil sample locations and the estimated zone of soil contamination at the Ray’s Quick Stop facility. Figure 3A depicts the soil samples and the contaminant levels in cross-sections A to A’ and B to B’. The results for the “Risk-Based” soil samples obtained at the subject property are summarized in Table 3. 2.2 Ground Water Flow Direction and Gradient

In order to estimate the groundwater flow direction in the vicinity of the petroleum release, elevations of the monitor well casings were measured using surveying equipment. Static water levels were obtained from monitor wells MW-1, MW-2, MW-3, MW-4, MW-5, MW-6, and VEW-1 and the data was used to compute a potentiometric surface map. Figure 4 illustrates the current potentiometric surface map as calculated based on the measurements obtained on October 4, 2022 and Table 5 contains the historical groundwater elevation data and monitoring well information. Groundwater data and monitoring well information were also used to estimate the hydraulic gradient at the project site. Using the horizontal distance between the monitor wells and the static water levels, the groundwater was calculated to flow toward the west with a hydraulic gradient of approximately 0.0148 feet per feet.

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2.3 Monitor Well Sampling and Analyses

On October 4, 2022, monitor wells MW-1, MW-2, MW-3, MW-4, MW-5, MW-6, and VEW-1 on the Ray’s Quick Stop property, as well as the supply well that serves the store building and the Eli Whitney Fire Deparment were sampled for analyses utilizing EPA Method 6200B plus MTBE, IPE, EDB, 5 Oxygenates, and Ethanol and MADEP Methods for Volatile Petroleum Hydrocarbons (VPH). Before collecting the samples, the monitor wells were purged by removing a minimum of three well volumes to ensure that the samples were representative of the actual groundwater conditions. The wells were developed using disposable plastic bailers suspended with unused nylon string. The supply wells were purged for a minimum of ten minutes each prior to collection of the samples. Following development of the monitoring wells, groundwater samples were obtained from the disposable bailers. All samples were placed in laboratory supplied glassware, labeled with sample location, analysis to be performed, time, date, and sampler's name. The sample jars were then immediately placed in a cooler and chilled with ice to approximately 4oC in preparation for transportation to the analytical laboratory utilizing EPA approved chain-of-custody procedures. The laboratory analytical results for monitor well MW-1 reported C9-C18 Aliphatics and C9-C22 Aromatics concentrations above the 2L Standards by VPH. C9-C18 Aliphatics were reported at a concentration of 878 micrograms per Liter (ug/L), which exceeds the 2L Standard of 700 ug/L. C9-C22 Aromatics were reported at a concentration of 424 ug/L, which is above the 2L Standard of 200 ug/L. Fifteen other compounds were reported in MW-1 at concentrations above the laboratory detection limits, but below their 2L Standards. The laboratory analytical results for monitor wells MW-2, MW-3, MW-4, MW-5, MW-6, and VEW-1, as well as supply well SW-1 were below the 2L Standards for all compounds according to EPA Method 6200B and VPH. Table 4 summarizes the groundwater analytical results from the sampling event conducted on October 4, 2022. Figure 5 illustrates the groundwater analytical results from the sampling event conducted on October 4, 2022. Figure 6 illustrates the estimated horizontal extent of C9-C18 Aliphatics in the groundwater on an isoconcentration map, and Figures 6A and 6B contain isoconcentration cross-sections for C9-C18 Alpihatics. Figure 7 illustrates the estimated horizontal extent of C9-C22 Aromatics in the groundwater on an isoconcentration map, and Figures 7A and 7B contain isoconcentration cross-sections for C9-C22 Aromatics. The locations of the supply wells are depicted on Figure 8. 2.4 Regional / Site Geology and Hydrogeology The site is situated in the Piedmont Region of the North Carolina Slate Belt. According to the Geological Map of North Carolina local bedrock geology of the region consists of late Proterozoic to Cambrian-aged metamorphosed granitic bedrock. The soils encountered at the project site consisted predominantly of clay with varying amounts of silt. Competent bedrock was encountered at depths ranging between 14 feet and 25 feet below land surface at Ray’s Quick Stop. During the installation of the Type III monitor well, competent bedrock was encountered at a depth of 22 feet below land surface.

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Field observations showed the soils at the site consist of a variety of textural assemblages as noted:

o orange clay with varying silt content

o orange to tan clay with varying silt content

o orange to white clay with varying silt content Groundwater is noted to be flowing predominantly toward the west according to the data collected on October 4, 2022. The average potentiometric surface gradient has been calculated at approximately 0.0148 feet per feet. During the CSA hydrogeological investigation, three single well rising head tests or "slug tests" were performed on MW-3, MW-4, and MW-5 to determine the saturated hydraulic conductivity of the water table aquifer. The method of Bouwer and Rice (Bouwer and Rice, 1989, 1976) was chosen to reduce the slug test data. A computer program developed by the Geraghty & Miller Modeling Group named Aqtesolv was used to estimate the aquifer parameters. Results of the slug tests indicated hydraulic conductivities of 1.386x10-4 feet/minute in MW-3, 2.222x10-4 feet/minute in MW-4, and 3.133x10-4 feet/minute in MW-5. These results are consistent with published values for silt, loess, and silty-sand (Freeze & Cherry, 1979). Slug test data and analyses for the subject site are included as Appendix F. Groundwater flow velocity was determined by averaging the hydraulic conductivity values and assuming an estimated effective porosity of 20 percent for soils at the site. The following equation yields an estimate of average groundwater flow velocity: v = k/n x dh/dl Where v = average groundwater flow velocity k = average hydraulic conductivity = 2.247 x 10-4 ft/min. n = effective porosity = 0.20 dh/dl = groundwater head gradient = 0.0148 ft/ft The average groundwater flow velocity at the Ray’s Quick Stop site has been calculated to be approximately 1.66x10-5 feet per minute which is equal to 8.72 feet per year. 2.5 Plume Development

The two monitor wells (MW-1 and VEW-1) which were contaminated by MTBE and C5-C8 Aliphatics during the CSA activities in 2015 have decreased to MTBE and C5-C8 Aliphatics concentrations that are below the 2L Standards. The laboratory results for VEW-1 is below the 2L Standards for all compounds by EPA Method 6200B and VPH. The laboratory results for MW-1 have indicated an increase in C9-C18 Aliphatics and C9-C22 Aromatics.

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The contaminant mass in the soil has been calculated from the data collected during the Limited Site Assessment (LSA) and Comprehensive Site Assessment (CSA), which is the most recent soil data collected at the site. The contaminant mass in the soil was calculated to be approximately 4.37 kilograms (kg). The contaminant mass in the groundwater has been calculated from the data of the groundwater samples collected on October 4, 2022. The current contaminant mass in the groundwater was calculated to be approximately 0.0302 kg. The total contaminant mass in the soil and groundwater has been calculated to be approximately 4.4002 kg. This value is less than the historical maximum contaminant mass of 4.8565 kg, calculated during from data obtained during the CSA activities. 3.0 Monitored Natural Attenuation 3.1 Natural Source Zone Depletion Status The groundwater contaminant plume has migrated approximately 20 feet down-gradient from the source area at the USTs, appears to be stable, and is possibly contracting due to the decreasing contaminant concentrations. The groundwater concentrations were not significantly elevated in any of the monitor wells during CSA phase of work and have decreased since then. Only two petroleum compounds exceed the 2L Standards according to the most recent groundwater results. The calculated groundwater flow velocity is on par with the general average for sites in this hydrogeologic regime. The significant decrease in contaminant concentrations since the previous sampling event indicates the absence of significant contaminant mass in the source area, as significant contaminant mass in the soil/smear zones would be expected to leach into the groundwater contaminant plume. Natural attenuation has been effective at reducing contaminant concentrations at this site. Tentative plans for the site include monitored natural attenuation due to the small size of the groundwater contaminant plume, the relatively low contaminant concentrations, and the lack of potential receptors immediately downgradient of the contaminant plume. Appendix A contains the historical sampling results for the monitor and supply wells at the subject site. Appendix B contains graphs depicting the MTBE concentrations vs. time. Appendix C contains a compilation of costs and a chronology of remediation activities. Appendix D contains a copy of the laboratory report and the chain-of-custody record for the groundwater samples obtained on October 4, 2022. 4.0 Conclusions

4.1 General Summary

A Groundwater Monitoring event at Ray’s Quick Stop located at 7610 NC Highway 87 S. in Snow Camp, North Carolina has been completed. From a review of all information gathered during this groundwater monitoring project, Paragon Environmental Consultants, Inc. makes the following conclusions:

o Petroleum compounds are present in monitor well MW-1 at concentrations which exceed the 2L Standards based on the analytical results for the October 4, 2022 sampling event.

o The analytical results for the other monitor wells were below the 2L Standards for all petroleum compounds by EPA Method 6200B and VPH.

o The analytical results for supply well SW-1 were below the 2L Standards for all petroleum compounds by EPA Method 6200B and VPH.

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4.2 Recommendations

Since natural attenuation has been effective at reducing the contaminant concentrations at this site, Paragon recommends continuing periodic monitoring of the groundwater. A copy of this monitoring report should be forwarded to the following address:

Winston-Salem Regional Office - UST Section 450 W. Hanes Mill Road – Suite 300 Winston-Salem, NC 27105 4.3 Limitations

This report has been prepared for the exclusive use of Ray’s Quick Stop, LLC for the
specific application to the referenced site located in Alamance County, North Carolina.
The assessment was conducted based on the scope of work and level of effort desired by
the client. Our findings have been developed in accordance with generally accepted
standards in the practice of Groundwater Monitoring Reports in the State of North
Carolina, available information, and our professional judgment. No other warranty is
expressed or implied.
The data presented in this report are indicative of conditions that existed at the precise locations sampled and at the time the samples were collected. Additionally, the data obtained from the samples would be interpreted as meaningful with respect to the parameters indicated in the laboratory reports. No additional information can be logically inferred from this data.

5.0 Statements and Certification 5.1 Statements The monitoring report had an established due date of November 1, 2022. Will this report be submitted after the established due date? No Was any required information from the template missing from this report? No If applicable, will any of the proposed attenuation milestones under the schedule approved in the Corrective Action Plan not be met? Not Applicable, No Corrective Action Plan has been written for this site. Does any known or suspected source zone soil contamination or free product remain outside of the assessed area that could be inhibiting natural attenuation? No Has there been an unexpected increase in contaminant mass sufficient to suggest a potential new release from a separate onsite or offsite source? No
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5.2 Certification I, Benjamin W. Robinson, a Licensed Geologist for Paragon Environmental Consultants, Inc., do certify that the information contained in this report is correct and accurate to the best of my knowledge.
Benjamin W. Robinson, L.G. North Carolina License #2466 Paragon Environmental Consultants, Inc. is licensed to practice geology in North Carolina. The certification number of the corporation is C-300.

FIGURES

TABLES

TABLE 1: SITE HISTORY RAY’S QUICK STOP 7610 NC HIGHWAY 87 S SNOW CAMP, NORTH CAROLINA Former UST Owner: Ray’s Quick Stop, LLC 7319 Morrow Mill Road Chapel Hill, NC 27516 Current UST / Property Owner: KNN, LLC 7610 NC Highway 87 S. Snow Camp, NC 27349

UST Information:

Tank Installation Size Closure UST Tank No Date (Gal) Date Status Contents
T1 Unknown 8,000 Not Applicable Active Gasoline
T2 Unknown 8,000 Not Applicable Active Gasoline
T3 Unknown 4,000 Not Applicable Active Gasoline

M22-1326H
TABLE 2
WATER SUPPLY WELL INFORMATION
1,000' RADIUS
Ray's Quick Stop
Snow Camp, North Carolina
Well
Identification SW-1 SW-2 SW-3 SW-4 SW-5
Owner Name Eli Whitney Fire Dept.Carol Lamm JDS Investments Ent. LLC Curtis F. Davis Angelica L. Lopez
Owner Address 7618 S NC HWY 87 7354 Lindley Mill Road 7609 Pinewild Court 2664 Millbrook Court 3935 G'boro / C H Rd.
Snow Camp, NC 27349 Graham, NC 27253 Raleigh, NC 27615 Haw River, NC 27258 Snow Camp, NC 27349
Telephone #Unknown Unknown Unknown Unknown Unknown
Use of Well Consumption Consumption Consumption Consumption Consumption
Depth of Well Unknown Unknown Unknown Unknown Unknown
Type of Well Unknown Unknown Unknown Unknown Unknown
Well Yield Unknown Unknown Unknown Unknown Unknown
Depth of Casing Unknown Unknown Unknown Unknown Unknown
Well Screen Interval Unknown Unknown Unknown Unknown Unknown
Feet from Source 670'200'280'430'460'
X22-1326C
TABLE 2
WATER SUPPLY WELL INFORMATION
1,000' RADIUS
Ray's Quick Stop
Snow Camp, North Carolina
Well
Identification SW-6 SW-7 SW-8 SW-9 SW-10
Owner Name Eusebia C. Castellanos Walinda F. Lloyd Rogelio Bautista Myron and Lisa Wells William B. George
Owner Address 3946 G'boro / C H Rd.3941 G'boro / C H Rd.7150 Raymon Road 7271 Whitney Road 3960 G'boro/ C H Rd.
Snow Camp, NC 27349 Snow Camp, NC 27349 Graham, NC 27256 Snow Camp, NC 27349 Snow Camp, NC 27349
Telephone #Unknown Unknown Unknown 336-376-6270 Unknown
Use of Well Consumption Consumption Consumption Consumption Consumption
Depth of Well Unknown Unknown Unknown Unknown Unknown
Type of Well Unknown Unknown Unknown Unknown Unknown
Well Yield Unknown Unknown Unknown Unknown Unknown
Depth of Casing Unknown Unknown Unknown Unknown Unknown
Well Screen Interval Unknown Unknown Unknown Unknown Unknown
Feet from Source 520'600'605'695'705'
X22-1326C
TABLE 2
WATER SUPPLY WELL INFORMATION
1,000' RADIUS
Ray's Quick Stop
Snow Camp, North Carolina
Well
Identification SW-11 SW-12 SW-13 SW-14 SW-15
Owner Name Braxton H. Reyna Mariana Cantu Thomas S. Redding III Alejandra S. Gamez Tamara Flick
Owner Address 9505 Pleasant Hill Ch Rd 7136 Raymon Road 1942 Van Thomas Road 7121 Raymon Road 7153 Whitney Road
Liberty, NC 27298 Snow Camp, NC 27349 Pittsboro, NC 27312 Graham, NC 27253 Graham, NC 27253
Telephone #Unknown Unknown Unknown Unknown Unknown
Use of Well Consumption Consumption Consumption Consumption Consumption
Depth of Well Unknown Unknown Unknown Unknown Unknown
Type of Well Unknown Unknown Unknown Unknown Unknown
Well Yield Unknown Unknown Unknown Unknown Unknown
Depth of Casing Unknown Unknown Unknown Unknown Unknown
Well Screen Interval Unknown Unknown Unknown Unknown Unknown
Feet from Source 710'745'795'740'870'
X22-1326C
TABLE 2
WATER SUPPLY WELL INFORMATION
1,000' RADIUS
Ray's Quick Stop
Snow Camp, North Carolina
Well
Identification SW-16 SW-17 SW-18 SW-19 SW-20
Owner Name Ayala J. Jaimes Michele F. Dry C. Barth & R. Cooper Charlotte D. Farrow Carol Lamm
Owner Address 7092 Raymon Road 7143 Whitney Road 7111 Raymon Road 7156 Whitney Road 7354 Lindley Mill Road
Graham, NC 27253 Graham, NC 27253 Graham, NC 27253 Graham, NC 27253 Graham, NC 27253
Telephone #Unknown Unknown Unknown 336-376-6270 Unknown
Use of Well Consumption Consumption Consumption Consumption Consumption
Depth of Well Unknown Unknown Unknown Unknown Unknown
Type of Well Unknown Unknown Unknown Unknown Unknown
Well Yield Unknown Unknown Unknown Unknown Unknown
Depth of Casing Unknown Unknown Unknown Unknown Unknown
Well Screen Interval Unknown Unknown Unknown Unknown Unknown
Feet from Source 852'970'930'950'165'
X22-1326C
TABLE 3
Summary of Soil Analytical Results
Ray's Quick Stop
Snow Camp, North Carolina
Constituent GP-4 GP-11 GP-12 GP-13 GP-14 Lowest MSCCs

Date 7/15/2013 3/11/2015 3/11/2015 3/11/2015 3/11/2015
Method 8260 (mg/kg)
Benzene BDL BDL 0.014 BDL BDL 0.0072
n-Butylbenzene 0.871 BDL BDL BDL 4.88 2.4
sec-Butylbenzene 0.77 BDL BDL BDL 2.46 2.2
Ethylbenzene 1.01 BDL 0.007 BDL 0.596 8
Isopropylbenzene 0.484 BDL BDL BDL 0.57 1.3
4-Isopropyltoluene 0.651 BDL BDL BDL 2.06 0.12
Naphthalene 1.3 BDL 0.009 BDL 7.28 0.2
n-Propylbenzene BDL BDL BDL BDL 1.67 1.4
Toluene BDL BDL BDL BDL BDL 5.4
1,2,4-Trimethylbenzene 6.37 0.006 0.013 BDL 11.7 6.6
1,3,5-Trimethylbenzene 1.63 BDL BDL BDL 4.91 6.6
Xylenes (total)1.165 BDL 0.066 BDL 2.78 6
MTBE BDL 0.046 5.01 0.383 BDL 0.085
IPE BDL BDL 0.028 0.008 BDL 0.32
Lead (mg/kg)
Lead 1.88 N/A N/A N/A N/A 270
Aliphatic Fraction Classes (mg/kg)
C5-C8 Volatile Aliphatics N/A BDL 6.67 BDL 74.8 68
C9-C12 Volatile Aliphatics N/A BDL BDL BDL 2,650 NSE
C9-C18 Extractable Aliphatics N/A N/A N/A N/A N/A NSE
C9-C18 Aliphatics (total)N/A BDL BDL BDL 2,650 540
C19-C36 Extractable Aliphatics N/A N/A N/A N/A N/A NSE
Aromatic Fraction Classes (mg/kg)
C9-C10 Volatile Aromatics N/A BDL BDL BDL 783 NSE
C11-C22 Extractable Aromatics N/A N/A N/A N/A N/A NSE
C9-C22 Aromatics (total)N/A BDL BDL BDL 783 31
BDL= Below Detection Limits
NSE = No Standard Established X22-1326
Constituent MW-1 MW-2 MW-3 MW-4 MW-5 MW-6 VEW-1 SW-1 2L Standard

Date 10/4/2022 10/4/2022 10/4/2022 10/4/2022 10/4/2022 10/4/2022 10/4/2022 10/4/2022
Method 6200B (ug/L)
Benzene 0.47 BDL BDL BDL BDL BDL BDL BDL 1
Toluene 2.2 BDL BDL BDL BDL BDL BDL BDL 600
Ethylbenzene 0.849 BDL BDL BDL BDL BDL BDL BDL 600
Xylenes (total)21 BDL BDL BDL BDL BDL BDL BDL 500
BTEX (total)23.2 BDL BDL BDL BDL BDL BDL BDL NSE
Acetone 16.5 BDL BDL BDL BDL BDL BDL BDL 6,000
n-Butylbenzene 2.11 BDL BDL BDL BDL BDL BDL BDL 70
sec-Butylbenzene 1.5 BDL BDL BDL BDL BDL BDL BDL 70
Isopropylbenzene 0.624 BDL BDL BDL BDL BDL BDL BDL 70
p-Isopropyltolune 2.31 BDL BDL BDL BDL BDL BDL BDL 25
4-Methyl-2-Pentanone (MIBK)6.48 BDL BDL BDL BDL BDL BDL BDL 100
Naphthalene 3.97 BDL BDL BDL BDL BDL BDL BDL 6
n-Propylbenzene 1.09 BDL BDL BDL BDL BDL BDL BDL 70
tert-Butyl Alcohol (TBA)BDL BDL BDL BDL BDL BDL 7.82 BDL 10
Tetrachloroethene (PCE)BDL BDL BDL BDL BDL 0.266 BDL BDL 0.7
1,2,4-Trimethylbenzene 22.5 BDL BDL BDL BDL BDL BDL BDL 400
1,3,5-Trimethylbenzene 11.1 BDL BDL BDL BDL BDL BDL BDL 400
IPE BDL BDL BDL BDL BDL BDL 1.51 BDL 70
MTBE 1.3 BDL BDL BDL BDL BDL 8.82 BDL 20
Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics BDL BDL BDL BDL BDL BDL BDL BDL 400
C9-C12 Volatile Aliphatics 878 BDL BDL BDL BDL BDL BDL BDL NSE
C9-C18 Extractable Aliphatics N/A N/A N/A N/A N/A N/A N/A N/A NSE
C9-C18 Aliphatics (total)878 BDL BDL BDL BDL BDL BDL BDL 700
C19-C36 Extractable Aliphatics N/A N/A N/A N/A N/A N/A N/A N/A 10,000
Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics 424 BDL BDL BDL BDL BDL BDL BDL NSE
C11-C22 Extractable Aromatics N/A N/A N/A N/A N/A N/A N/A N/A NSE
C9-C22 Aromatics (total)424 BDL BDL BDL BDL BDL BDL BDL 200
BDL = Below Detection Limits
N/A = Not Analyzed
NSE = No Standard Established X22-1326A
TABLE 4
Summary of Groundwater Analytical Results
Ray's Quick Stop
Snow Camp, North Carolina
TABLE 5

Monitoring Well Information and Groundwater Elevations
Ray's Quick Stop
Snow Camp, North Carolina
Well Number Top of Casing Elevation Top of Screen Elevation Bottom of Screen Elevation Depth to Water Groundwater Elevation
MW-1 98.30 77.30 62.30 11.74 86.56
MW-2 99.84 95.84 85.84 11.72 88.12
MW-3 100.00 87.00 77.00 12.96 87.04
MW-4 97.94 85.94 75.94 11.56 86.38
MW-5 99.66 91.66 81.66 12.24 87.42
MW-6 97.38 85.38 75.38 10.44 86.94
VEW-1 98.53 61.53 56.53 12.75 85.78
Note: All measurements taken in feet and based on an arbitrary benchmark of 100.00 feet at MW-2; groundwater levels measured on October 4, 2022.
X22-1326B
TABLE 6
Evaluation of Change in Contaminant Mass
Ray's Quick Stop
Snow Camp, North Carolina
Mass Estimates
CSA 10/4/22
Projected Mass Reduction:0%5%
Projected Soil Source Zone Mass:4.37 4.15
Projected Groundwater Zone Mass:0.4865 0.4622
Total Mass:4.8565 4.6137
Change in Contaminant Mass
Measured Mass
Soil Source Zone:4.37 4.37
Groundwater Source Zone:0.4865 0.0302
Removed Mass
Excavated from Soil/Smear:0.00 0.00
Extracted as Vapor/Gas:0.00 0.00
Extracted as Liquid:0.00 0.00
Total Mass Removed:0.00 0.00
Revised Total Mass:4.8565 4.4002
Estimated Reduction Rate:0.00 9.40
Reference Milestone 0%5%
Reference Milestone 4.8565 4.6137
Reduction Progress vs. Milestone 0.00 0.05
All results are reported in kilograms (kg)
NOTE: No CAP has been written for this site.
X22-1326MRC
Milestones
TABLE 6A
Contaminant Mass Calculation Data
Ray's Quick Stop
Snow Camp, North Carolina
Soil Soil Data Soil Data
Area of Soil Contamination (ft²)1,561.22 1,561.22
Average Height of Soil Contamination (ft)6.03 6.03
Volume of Soil Contamination (ft³)9,414.14 9,414.14
Volume of Soil Contamination (m³)266.58 266.58
Average Bulk Density of Soil (kg/m³) *1,430.00 1,430.00
Soil Mass (kg)381,207.16 381,207.16
Average Contaminant Concentration in Soil (mg/kg)11.47 11.47
Contaminant Mass in Soil (mg)4,373,685.01 4,373,685.01
Contaminant Mass in Soil (kg)4.37 4.37
Groundwater Data from CSA Data from 10/4/2022 sampling event
Area of Groundwater Contamination (ft²)2,285.76 337.97
Average Height of Groundwater Contamination (ft)29.69 24.26
Volume of Plume (ft³)67,864.34 8,199.24
Volume of Plume (L)1,921,700.83 232,176.23
Porosity (n) *0.20 0.20
Volume of Water in Plume (L)384,340.17 46,435.25
Average Contaminant Concentration in Plume (ug/L)1,265.75 651.00
Contaminant Mass in Groundwater (ug)486,478,565.95 30,229,344.64
Contaminant Mass in Groundwater (kg)0.4865 0.0302
Extracted Water (L)N/A N/A
Extracted Mass (kg)N/A N/A
* Assumed Values for the Piedmont of NC
NOTE: No CAP has been written for this site.
X22-1326MRC

APPENDIX A

HISTORICAL SAMPLING RESULTS

Constituent SW-1 2L Standard

Date 11/4/13 10/4/22 11/26/13 10/4/22 11/26/13 10/4/22 11/26/13 10/4/22 3/19/15 10/4/22 3/19/15 10/4/22 3/19/15 10/4/22 10/4/22
Method 6200B (ug/L)
Benzene BDL 0.47 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1
Toluene 0.69 2.2 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 600
Ethylbenzene BDL 0.849 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 600
Xylenes (total)1.14 21 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 500
BTEX (total)1.83 23.2 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NSE
Acetone BDL 16.5 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 128 BDL BDL 6,000
2-Butanone (MEK)BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 127 BDL BDL 4,000
n-Butylbenzene BDL 2.11 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 70
sec-Butylbenzene BDL 1.5 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 70
2-Hexanone BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.68 BDL BDL 40
Isopropylbenzene BDL 0.624 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 70
p-Isopropyltolune BDL 2.31 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 25
4-Methyl-2-Pentanone (MIBK)BDL 6.48 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 100
Naphthalene BDL 3.97 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 6
n-Propylbenzene BDL 1.09 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 70
tert-Butyl Alcohol (TBA)N/A BDL N/A BDL N/A BDL N/A BDL N/A BDL N/A BDL N/A 7.82 BDL 10
Tetrachloroethene (PCE)BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.75 0.266 BDL BDL BDL 0.7
1,2,4-Trimethylbenzene BDL 22.5 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 400
1,3,5-Trimethylbenzene BDL 11.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 400
IPE 21.6 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 9.71 1.51 BDL 70
MTBE 953 1.3 BDL BDL BDL BDL 1.54 BDL BDL BDL BDL BDL 610 8.82 BDL 20
Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics 2,490 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1,010 BDL BDL 400
C9-C12 Volatile Aliphatics 275 878 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 139 BDL BDL NSE
C9-C18 Extractable Aliphatics N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A NSE
C9-C18 Aliphatics (total)275 878 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 139 BDL BDL 700
C19-C36 Extractable Aliphatics N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A 10,000
Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics BDL 424 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NSE
C11-C22 Extractable Aromatics N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A NSE
C9-C22 Aromatics (total)BDL 424 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 200
BDL = Below Detection Limits
N/A = Not Analyzed
NSE = No Standard Established X22-1326A
Historical Sampling Results
Ray's Quick Stop
Snow Camp, North Carolina
MW-1 MW-2 MW-3 MW-4 MW-5 MW-6 VEW-1

APPENDIX B

CONTAMINANT CONCENTRATIONS VS.

TIME GRAPHS

0
200
400
600
800
1,000
1,200
CSA Event 10/4/22 EventMTBE Concentration (ug/L)Time
Ray's Quick Stop
MTBE Concentration vs. Time
MW-1
VEW-1

APPENDIX C

COMPILATION OF COSTS / CHRONOLOGY OF REMEDIATION
ACTIVITIES

Compilation of Costs / Chronology of Remediation Activities
Ray's Quick Stop
7610 NC Highway 87 S.
Snow Camp, North Carolina
Date(s)Activity Cost
7/15/13 - 12/12/13 Limited Site Assessment $9,190.00
3/4/15 - 7/16/15 Comprehensive Site Assessment $14,897.50
Total:$24,087.50
X22-1326Costs

APPENDIX D

LABORATORY ANALYTICAL RESULTS

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

10/13/2022
Paragon Environmental Consultants, Inc. Brandon Moore
PO Box 157 Thomasville, NC, 27361
Ref: Analytical Testing
Lab Report Number: 22-278-0022 Client Project Description: Ray's Quick Stop
P-1326
Dear Brandon Moore:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 10/5/2022 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 84
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/22-278-0022
Page 2 of 84
Report Number:
Sample Summary Table
Client Project Description:
22-278-0022
Ray's Quick Stop
P-1326
Lab No Client Sample ID Matrix Date Collected Date Received
10/04/2022 09:50Aqueous 89961 MW-1 10/05/2022 15:31
10/04/2022 08:30Aqueous 89962 MW-2 10/05/2022 15:31
10/04/2022 09:00Aqueous 89963 MW-3 10/05/2022 15:31
10/04/2022 08:15Aqueous 89964 MW-4 10/05/2022 15:31
10/04/2022 08:45Aqueous 89965 MW-5 10/05/2022 15:31
10/04/2022 09:15Aqueous 89966 MW-6 10/05/2022 15:31
10/04/2022 09:35Aqueous 89967 VEW-1 10/05/2022 15:31
10/04/2022 10:00Aqueous 89968 SW-1 10/05/2022 15:31
10/04/2022Aqueous 89969 TRIP BLANK 10/05/2022 15:31
Page 3 of 84
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-278-0022
Report Limit
Project:Ray's Quick Stop
V 89961MW-1
16.5 10/10/2022 19:336200BAcetoneµg/L 1.80
J0.470 10/10/2022 19:336200BBenzeneµg/L 0.180
2.11 10/10/2022 19:336200Bn-Butylbenzene µg/L 0.180
1.50 10/10/2022 19:336200Bsec-Butyl benzene µg/L 0.200
0.849 10/10/2022 19:336200BEthylbenzeneµg/L 0.170
0.624 10/10/2022 19:336200BIsopropylbenzeneµg/L 0.180
2.31 10/10/2022 19:336200B4-Isopropyl toluene µg/L 0.089
1.30 10/10/2022 19:336200BMethyl tert-butyl ether (MTBE)µg/L 0.140
6.48 10/10/2022 19:336200B4-Methyl-2-Pentanone µg/L 0.078
3.97 10/10/2022 19:336200BNaphthaleneµg/L 0.470
1.09 10/10/2022 19:336200Bn-Propylbenzene µg/L 0.190
2.20 10/10/2022 19:336200BTolueneµg/L 0.220
22.5 10/10/2022 19:336200B1,2,4-Trimethylbenzene µg/L 0.190
11.1 10/10/2022 19:336200B1,3,5-Trimethylbenzene µg/L 0.180
9.35 10/10/2022 19:336200Bo-Xylene µg/L 0.210
11.6 10/10/2022 19:336200Bm,p-Xylene µg/L 0.420
21.0 10/10/2022 19:336200BXylene (Total)µg/L 0.210
878 10/07/2022 10:32MADEP-VPH Aliphatic C9-C12 µg/L 25.8
424 10/07/2022 10:32MADEP-VPH Aromatic C9-C10 µg/L 4.02
V 89966MW-6
J0.266 10/06/2022 23:426200BTetrachloroetheneµg/L 0.220
V 89967VEW-1
1.51 10/07/2022 00:056200BDi-Isopropyl Ether (DIPE)µg/L 0.500
8.82 10/07/2022 00:056200BMethyl tert-butyl ether (MTBE)µg/L 0.140
J7.82 10/07/2022 00:056200Btert-Butyl Alcohol (TBA)µg/L 1.60
Page 4 of 84

Client: Paragon Environmental Consultants, Inc. CASE NARRATIVE
Project: Ray's Quick Stop Lab Report Number: 22-278-0022
Date: 10/12/2022
Volatile Organic Compounds - GC/MS Method 6200B Sample 89969 (TRIP BLANK) QC Batch No: V24860/V24859
Many LCS/LCSD analytes have recoveries high out of parameters. No hits detected in the sample and no more vials available fore re-runs. The QC skewing high would give a high bias towards any hits, but there are non
present. No further action taken.
Analyte: 1,1,1-Trichloroethane QC Batch No: V24843/V24970
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: 1,1,1-Trichloroethane QC Batch No: V24860/V24970
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: 1,1,2-Trichloroethane QC Batch No: V24860/V24970 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: 1,1-Dichloroethane QC Batch No: V24860/V24970
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: 1,1-Dichloropropene QC Batch No: V24843/V24970
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: 1,1-Dichloropropene QC Batch No: V24860/V24970
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: 1,2-Dibromoethane QC Batch No: V24843/V24970
Page 5 of 84

Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: 1,2-Dichloroethane
QC Batch No: V24860/V24970 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: 1,2-Dichloropropane
QC Batch No: V24860/V24970 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: 2,2-Dichloropropane
QC Batch No: V24860/V24970 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: 2-Butanone QC Batch No: V24860/V24970 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: Benzene QC Batch No: V24860/V24970 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: Bromochloromethane
QC Batch No: V24843/V24970 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: Bromochloromethane
QC Batch No: V24860/V24970 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: Bromomethane QC Batch No: V24843/V24970 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: Carbon Tetrachloride
Page 6 of 84

QC Batch No: V24843/V24970
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: Carbon Tetrachloride QC Batch No: V24860/V24970
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: Chloroform QC Batch No: V24860/V24970
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: cis-1,2-Dichloroethene QC Batch No: V24860/V24970
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable. Analyte: cis-1,3-Dichloropropene QC Batch No: V24843/V24970
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable. Analyte: cis-1,3-Dichloropropene QC Batch No: V24860/V24970 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: Di isopropyl ether QC Batch No: V24860/V24970 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: Dibromomethane QC Batch No: V24860/V24970 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: Ethyl Tertiary Butyl Ether QC Batch No: V24860/V24970 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Page 7 of 84

Analyte: Hexachlorobutadiene
QC Batch No: V24843/V24970 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: Methyl tert-butyl ether (MTBE)
QC Batch No: V24860/V24970 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: Methylene chloride
QC Batch No: V24860/V24970 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: tert-Amyl alcohol
QC Batch No: V24843/V24970 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: tert-Amyl Methyl Ether QC Batch No: V24860/V24970 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: Toluene QC Batch No: V24860/V24970 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: trans-1,2-Dichloroethene
QC Batch No: V24860/V24970 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: trans-1,3-Dichloropropene
QC Batch No: V24843/V24970 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: trans-1,3-Dichloropropene QC Batch No: V24860/V24970 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: Trichloroethene
Page 8 of 84

QC Batch No: V24843/V24970
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: Trichloroethene QC Batch No: V24860/V24970
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: Vinyl acetate QC Batch No: V24860/V24970
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.

Page 9 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-1
89961 Matrix:
10/4/2022 9:50
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 10/10/22 19:33 6200BMSA
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%10/10/22 19:331 MSA V24973
Surrogate: Dibromofluoromethane 96.8 Limits: 70-130%10/10/22 19:331 MSA V24973
Surrogate: 1,2-Dichloroethane - d4 94.2 Limits: 70-130%10/10/22 19:331 MSA V24973
Surrogate: Toluene-d8 99.2 Limits: 70-130%10/10/22 19:331 MSA V24973
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-1
89961 Matrix:
10/4/2022 9:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24970 10/10/22 09:00
16.5 µg/L 1.80 10.0Acetone 1 10/10/22 19:33 V24973MSA
0.470 J
µg/L 0.180 0.500
Benzene 1 10/10/22 19:33 V24973MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 10/10/22 19:33 V24973MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 10/10/22 19:33 V24973MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 10/10/22 19:33 V24973MSA
<1.50 µg/L 1.50 5.00Bromoform 1 10/10/22 19:33 V24973MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 10/10/22 19:33 V24973MSA
2.11 µg/L 0.180 0.500n-Butylbenzene 1 10/10/22 19:33 V24973MSA
1.50 µg/L 0.200 0.500
sec-Butyl benzene 1 10/10/22 19:33 V24973MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 10/10/22 19:33 V24973MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 10/10/22 19:33 V24973MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 10/10/22 19:33 V24973MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 10/10/22 19:33 V24973MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 10/10/22 19:33 V24973MSA
<0.220 µg/L 0.220 0.500Chloroform 1 10/10/22 19:33 V24973MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 10/10/22 19:33 V24973MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 10/10/22 19:33 V24973MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 10/10/22 19:33 V24973MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 10/10/22 19:33 V24973MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 10/10/22 19:33 V24973MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 10/10/22 19:33 V24973MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 10/10/22 19:33 V24973MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-1
89961 Matrix:
10/4/2022 9:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24970 10/10/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 10/10/22 19:33 V24973MSA
<0.190 µg/L 0.190 0.500
1,3-Dichlorobenzene 1 10/10/22 19:33 V24973MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 10/10/22 19:33 V24973MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 10/10/22 19:33 V24973MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 10/10/22 19:33 V24973MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 10/10/22 19:33 V24973MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 10/10/22 19:33 V24973MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 10/10/22 19:33 V24973MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 10/10/22 19:33 V24973MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 10/10/22 19:33 V24973MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 10/10/22 19:33 V24973MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 10/10/22 19:33 V24973MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 10/10/22 19:33 V24973MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 10/10/22 19:33 V24973MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 10/10/22 19:33 V24973MSA
<42.0 µg/L 42.0 200Ethanol 1 10/10/22 19:33 V24973MSA
0.849 µg/L 0.170 0.500Ethylbenzene 1 10/10/22 19:33 V24973MSA
<0.059 µg/L 0.059 10.0Ethyl Tertiary Butyl Ether (ETBE)1 10/10/22 19:33 V24973MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 10/10/22 19:33 V24973MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 10/10/22 19:33 V24973MSA
0.624 µg/L 0.180 0.500Isopropylbenzene 1 10/10/22 19:33 V24973MSA
2.31 µg/L 0.089 0.5004-Isopropyl toluene 1 10/10/22 19:33 V24973MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-1
89961 Matrix:
10/4/2022 9:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24970 10/10/22 09:00
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 10/10/22 19:33 V24973MSA
1.30 µg/L 0.140 1.00
Methyl tert-butyl ether (MTBE)1 10/10/22 19:33 V24973MSA
6.48 µg/L 0.078 1.004-Methyl-2-Pentanone 1 10/10/22 19:33 V24973MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 10/10/22 19:33 V24973MSA
3.97 µg/L 0.470 1.00Naphthalene 1 10/10/22 19:33 V24973MSA
1.09 µg/L 0.190 0.500n-Propylbenzene 1 10/10/22 19:33 V24973MSA
<0.220 µg/L 0.220 0.500Styrene 1 10/10/22 19:33 V24973MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 10/10/22 19:33 V24973MSA
<0.350 µg/L 0.350 10.0
tert-Butyl formate (TBF)1 10/10/22 19:33 V24973MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 10/10/22 19:33 V24973MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 10/10/22 19:33 V24973MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 10/10/22 19:33 V24973MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 10/10/22 19:33 V24973MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 10/10/22 19:33 V24973MSA
2.20 µg/L 0.220 0.500Toluene 1 10/10/22 19:33 V24973MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 10/10/22 19:33 V24973MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 10/10/22 19:33 V24973MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 10/10/22 19:33 V24973MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 10/10/22 19:33 V24973MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 10/10/22 19:33 V24973MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 10/10/22 19:33 V24973MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 10/10/22 19:33 V24973MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-1
89961 Matrix:
10/4/2022 9:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24970 10/10/22 09:00
22.5 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 10/10/22 19:33 V24973MSA
11.1 µg/L 0.180 0.500
1,3,5-Trimethylbenzene 1 10/10/22 19:33 V24973MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 10/10/22 19:33 V24973MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 10/10/22 19:33 V24973MSA
9.35 µg/L 0.210 0.500o-Xylene 1 10/10/22 19:33 V24973MSA
11.6 µg/L 0.420 1.00m,p-Xylene 1 10/10/22 19:33 V24973MSA
21.0 µg/L 0.210 0.500Xylene (Total)1 10/10/22 19:33 V24973
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%10/10/22 19:331 MSA V24973
Surrogate: Dibromofluoromethane 96.8 Limits: 70-130%10/10/22 19:331 MSA V24973
Surrogate: 1,2-Dichloroethane - d4 94.2 Limits: 70-130%10/10/22 19:331 MSA V24973
Surrogate: Toluene-d8 99.2 Limits: 70-130%10/10/22 19:331 MSA V24973
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-1
89961 Matrix:
10/4/2022 9:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V24827 10/06/22 08:00
<11.5 µg/L 11.5 50.0Aliphatic C5-C8 1 10/07/22 10:32 V24828TBL
878 µg/L 25.8 50.0
Aliphatic C9-C12 1 10/07/22 10:32 V24828TBL
424 µg/L 4.02 50.0Aromatic C9-C10 1 10/07/22 10:32 V24828TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)123 Limits: 70-130%10/07/22 10:321 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)99.3 Limits: 70-130%10/07/22 10:321 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-2
89962 Matrix:
10/4/2022 8:30
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 10/06/22 22:09 6200BANG
Surrogate: 4-Bromofluorobenzene 110 Limits: 70-130%10/06/22 22:091 ANG V24843
Surrogate: Dibromofluoromethane 114 Limits: 70-130%10/06/22 22:091 ANG V24843
Surrogate: 1,2-Dichloroethane - d4 96.4 Limits: 70-130%10/06/22 22:091 ANG V24843
Surrogate: Toluene-d8 99.0 Limits: 70-130%10/06/22 22:091 ANG V24843
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-2
89962 Matrix:
10/4/2022 8:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 10/06/22 22:09 V24843ANG
<0.180 µg/L 0.180 0.500
Benzene 1 10/06/22 22:09 V24843ANG
<0.210 µg/L 0.210 0.500Bromobenzene 1 10/06/22 22:09 V24843ANG
<0.420 µg/L 0.420 1.00Bromochloromethane 1 10/06/22 22:09 V24843ANG
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 10/06/22 22:09 V24843ANG
<1.50 µg/L 1.50 5.00Bromoform 1 10/06/22 22:09 V24843ANG
<0.280 µg/L 0.280 1.00Bromomethane 1 10/06/22 22:09 V24843ANG
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 10/06/22 22:09 V24843ANG
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 10/06/22 22:09 V24843ANG
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 10/06/22 22:09 V24843ANG
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 10/06/22 22:09 V24843ANG
<0.190 µg/L 0.190 0.500Chlorobenzene 1 10/06/22 22:09 V24843ANG
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 10/06/22 22:09 V24843ANG
<0.430 µg/L 0.430 1.00Chloroethane 1 10/06/22 22:09 V24843ANG
<0.220 µg/L 0.220 0.500Chloroform 1 10/06/22 22:09 V24843ANG
<0.220 µg/L 0.220 0.500Chloromethane 1 10/06/22 22:09 V24843ANG
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 10/06/22 22:09 V24843ANG
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 10/06/22 22:09 V24843ANG
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 10/06/22 22:09 V24843ANG
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 10/06/22 22:09 V24843ANG
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 10/06/22 22:09 V24843ANG
<0.230 µg/L 0.230 0.500Dibromomethane 1 10/06/22 22:09 V24843ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-2
89962 Matrix:
10/4/2022 8:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 10/06/22 22:09 V24843ANG
<0.190 µg/L 0.190 0.500
1,3-Dichlorobenzene 1 10/06/22 22:09 V24843ANG
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 10/06/22 22:09 V24843ANG
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 10/06/22 22:09 V24843ANG
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 10/06/22 22:09 V24843ANG
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 10/06/22 22:09 V24843ANG
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 10/06/22 22:09 V24843ANG
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 10/06/22 22:09 V24843ANG
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 10/06/22 22:09 V24843ANG
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 10/06/22 22:09 V24843ANG
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 10/06/22 22:09 V24843ANG
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 10/06/22 22:09 V24843ANG
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 10/06/22 22:09 V24843ANG
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 10/06/22 22:09 V24843ANG
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 10/06/22 22:09 V24843ANG
<42.0 µg/L 42.0 200Ethanol 1 10/06/22 22:09 V24843ANG
<0.170 µg/L 0.170 0.500Ethylbenzene 1 10/06/22 22:09 V24843ANG
<0.059 µg/L 0.059 10.0Ethyl Tertiary Butyl Ether (ETBE)1 10/06/22 22:09 V24843ANG
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 10/06/22 22:09 V24843ANG
<0.380 µg/L 0.380 1.002-Hexanone 1 10/06/22 22:09 V24843ANG
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 10/06/22 22:09 V24843ANG
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 10/06/22 22:09 V24843ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-2
89962 Matrix:
10/4/2022 8:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 10/06/22 22:09 V24843ANG
<0.140 µg/L 0.140 1.00
Methyl tert-butyl ether (MTBE)1 10/06/22 22:09 V24843ANG
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 10/06/22 22:09 V24843ANG
<0.330 µg/L 0.330 2.00Methylene Chloride 1 10/06/22 22:09 V24843ANG
<0.470 µg/L 0.470 1.00Naphthalene 1 10/06/22 22:09 V24843ANG
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 10/06/22 22:09 V24843ANG
<0.220 µg/L 0.220 0.500Styrene 1 10/06/22 22:09 V24843ANG
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 10/06/22 22:09 V24843ANG
<0.350 µg/L 0.350 10.0
tert-Butyl formate (TBF)1 10/06/22 22:09 V24843ANG
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 10/06/22 22:09 V24843ANG
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 10/06/22 22:09 V24843ANG
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 10/06/22 22:09 V24843ANG
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 10/06/22 22:09 V24843ANG
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 10/06/22 22:09 V24843ANG
<0.220 µg/L 0.220 0.500Toluene 1 10/06/22 22:09 V24843ANG
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 10/06/22 22:09 V24843ANG
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 10/06/22 22:09 V24843ANG
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 10/06/22 22:09 V24843ANG
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 10/06/22 22:09 V24843ANG
<0.180 µg/L 0.180 0.500Trichloroethene 1 10/06/22 22:09 V24843ANG
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 10/06/22 22:09 V24843ANG
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 10/06/22 22:09 V24843ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-2
89962 Matrix:
10/4/2022 8:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 10/06/22 22:09 V24843ANG
<0.180 µg/L 0.180 0.500
1,3,5-Trimethylbenzene 1 10/06/22 22:09 V24843ANG
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 10/06/22 22:09 V24843ANG
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 10/06/22 22:09 V24843ANG
<0.210 µg/L 0.210 0.500o-Xylene 1 10/06/22 22:09 V24843ANG
<0.420 µg/L 0.420 1.00m,p-Xylene 1 10/06/22 22:09 V24843ANG
<0.21 µg/L 0.210 0.500Xylene (Total)1 10/06/22 22:09 V24843
Surrogate: 4-Bromofluorobenzene 110 Limits: 70-130%10/06/22 22:091 ANG V24843
Surrogate: Dibromofluoromethane 114 Limits: 70-130%10/06/22 22:091 ANG V24843
Surrogate: 1,2-Dichloroethane - d4 96.4 Limits: 70-130%10/06/22 22:091 ANG V24843
Surrogate: Toluene-d8 99.0 Limits: 70-130%10/06/22 22:091 ANG V24843
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-2
89962 Matrix:
10/4/2022 8:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V24827 10/06/22 08:00
<11.5 µg/L 11.5 50.0Aliphatic C5-C8 1 10/06/22 14:11 V24828TBL
<25.8 µg/L 25.8 50.0
Aliphatic C9-C12 1 10/06/22 14:11 V24828TBL
<4.02 µg/L 4.02 50.0Aromatic C9-C10 1 10/06/22 14:11 V24828TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)93.5 Limits: 70-130%10/06/22 14:111 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)86.4 Limits: 70-130%10/06/22 14:111 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-3
89963 Matrix:
10/4/2022 9:00
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 10/06/22 22:33 6200BANG
Surrogate: 4-Bromofluorobenzene 110 Limits: 70-130%10/06/22 22:331 ANG V24843
Surrogate: Dibromofluoromethane 114 Limits: 70-130%10/06/22 22:331 ANG V24843
Surrogate: 1,2-Dichloroethane - d4 96.0 Limits: 70-130%10/06/22 22:331 ANG V24843
Surrogate: Toluene-d8 97.2 Limits: 70-130%10/06/22 22:331 ANG V24843
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-3
89963 Matrix:
10/4/2022 9:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 10/06/22 22:33 V24843ANG
<0.180 µg/L 0.180 0.500
Benzene 1 10/06/22 22:33 V24843ANG
<0.210 µg/L 0.210 0.500Bromobenzene 1 10/06/22 22:33 V24843ANG
<0.420 µg/L 0.420 1.00Bromochloromethane 1 10/06/22 22:33 V24843ANG
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 10/06/22 22:33 V24843ANG
<1.50 µg/L 1.50 5.00Bromoform 1 10/06/22 22:33 V24843ANG
<0.280 µg/L 0.280 1.00Bromomethane 1 10/06/22 22:33 V24843ANG
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 10/06/22 22:33 V24843ANG
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 10/06/22 22:33 V24843ANG
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 10/06/22 22:33 V24843ANG
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 10/06/22 22:33 V24843ANG
<0.190 µg/L 0.190 0.500Chlorobenzene 1 10/06/22 22:33 V24843ANG
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 10/06/22 22:33 V24843ANG
<0.430 µg/L 0.430 1.00Chloroethane 1 10/06/22 22:33 V24843ANG
<0.220 µg/L 0.220 0.500Chloroform 1 10/06/22 22:33 V24843ANG
<0.220 µg/L 0.220 0.500Chloromethane 1 10/06/22 22:33 V24843ANG
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 10/06/22 22:33 V24843ANG
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 10/06/22 22:33 V24843ANG
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 10/06/22 22:33 V24843ANG
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 10/06/22 22:33 V24843ANG
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 10/06/22 22:33 V24843ANG
<0.230 µg/L 0.230 0.500Dibromomethane 1 10/06/22 22:33 V24843ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-3
89963 Matrix:
10/4/2022 9:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 10/06/22 22:33 V24843ANG
<0.190 µg/L 0.190 0.500
1,3-Dichlorobenzene 1 10/06/22 22:33 V24843ANG
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 10/06/22 22:33 V24843ANG
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 10/06/22 22:33 V24843ANG
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 10/06/22 22:33 V24843ANG
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 10/06/22 22:33 V24843ANG
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 10/06/22 22:33 V24843ANG
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 10/06/22 22:33 V24843ANG
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 10/06/22 22:33 V24843ANG
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 10/06/22 22:33 V24843ANG
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 10/06/22 22:33 V24843ANG
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 10/06/22 22:33 V24843ANG
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 10/06/22 22:33 V24843ANG
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 10/06/22 22:33 V24843ANG
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 10/06/22 22:33 V24843ANG
<42.0 µg/L 42.0 200Ethanol 1 10/06/22 22:33 V24843ANG
<0.170 µg/L 0.170 0.500Ethylbenzene 1 10/06/22 22:33 V24843ANG
<0.059 µg/L 0.059 10.0Ethyl Tertiary Butyl Ether (ETBE)1 10/06/22 22:33 V24843ANG
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 10/06/22 22:33 V24843ANG
<0.380 µg/L 0.380 1.002-Hexanone 1 10/06/22 22:33 V24843ANG
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 10/06/22 22:33 V24843ANG
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 10/06/22 22:33 V24843ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-3
89963 Matrix:
10/4/2022 9:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 10/06/22 22:33 V24843ANG
<0.140 µg/L 0.140 1.00
Methyl tert-butyl ether (MTBE)1 10/06/22 22:33 V24843ANG
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 10/06/22 22:33 V24843ANG
<0.330 µg/L 0.330 2.00Methylene Chloride 1 10/06/22 22:33 V24843ANG
<0.470 µg/L 0.470 1.00Naphthalene 1 10/06/22 22:33 V24843ANG
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 10/06/22 22:33 V24843ANG
<0.220 µg/L 0.220 0.500Styrene 1 10/06/22 22:33 V24843ANG
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 10/06/22 22:33 V24843ANG
<0.350 µg/L 0.350 10.0
tert-Butyl formate (TBF)1 10/06/22 22:33 V24843ANG
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 10/06/22 22:33 V24843ANG
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 10/06/22 22:33 V24843ANG
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 10/06/22 22:33 V24843ANG
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 10/06/22 22:33 V24843ANG
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 10/06/22 22:33 V24843ANG
<0.220 µg/L 0.220 0.500Toluene 1 10/06/22 22:33 V24843ANG
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 10/06/22 22:33 V24843ANG
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 10/06/22 22:33 V24843ANG
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 10/06/22 22:33 V24843ANG
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 10/06/22 22:33 V24843ANG
<0.180 µg/L 0.180 0.500Trichloroethene 1 10/06/22 22:33 V24843ANG
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 10/06/22 22:33 V24843ANG
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 10/06/22 22:33 V24843ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-3
89963 Matrix:
10/4/2022 9:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 10/06/22 22:33 V24843ANG
<0.180 µg/L 0.180 0.500
1,3,5-Trimethylbenzene 1 10/06/22 22:33 V24843ANG
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 10/06/22 22:33 V24843ANG
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 10/06/22 22:33 V24843ANG
<0.210 µg/L 0.210 0.500o-Xylene 1 10/06/22 22:33 V24843ANG
<0.420 µg/L 0.420 1.00m,p-Xylene 1 10/06/22 22:33 V24843ANG
<0.21 µg/L 0.210 0.500Xylene (Total)1 10/06/22 22:33 V24843
Surrogate: 4-Bromofluorobenzene 110 Limits: 70-130%10/06/22 22:331 ANG V24843
Surrogate: Dibromofluoromethane 114 Limits: 70-130%10/06/22 22:331 ANG V24843
Surrogate: 1,2-Dichloroethane - d4 96.0 Limits: 70-130%10/06/22 22:331 ANG V24843
Surrogate: Toluene-d8 97.2 Limits: 70-130%10/06/22 22:331 ANG V24843
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-3
89963 Matrix:
10/4/2022 9:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V24827 10/06/22 08:00
<11.5 µg/L 11.5 50.0Aliphatic C5-C8 1 10/06/22 14:35 V24828TBL
<25.8 µg/L 25.8 50.0
Aliphatic C9-C12 1 10/06/22 14:35 V24828TBL
<4.02 µg/L 4.02 50.0Aromatic C9-C10 1 10/06/22 14:35 V24828TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)83.0 Limits: 70-130%10/06/22 14:351 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)79.7 Limits: 70-130%10/06/22 14:351 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-4
89964 Matrix:
10/4/2022 8:15
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 10/06/22 22:56 6200BANG
Surrogate: 4-Bromofluorobenzene 109 Limits: 70-130%10/06/22 22:561 ANG V24843
Surrogate: Dibromofluoromethane 112 Limits: 70-130%10/06/22 22:561 ANG V24843
Surrogate: 1,2-Dichloroethane - d4 98.4 Limits: 70-130%10/06/22 22:561 ANG V24843
Surrogate: Toluene-d8 98.0 Limits: 70-130%10/06/22 22:561 ANG V24843
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-4
89964 Matrix:
10/4/2022 8:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 10/06/22 22:56 V24843ANG
<0.180 µg/L 0.180 0.500
Benzene 1 10/06/22 22:56 V24843ANG
<0.210 µg/L 0.210 0.500Bromobenzene 1 10/06/22 22:56 V24843ANG
<0.420 µg/L 0.420 1.00Bromochloromethane 1 10/06/22 22:56 V24843ANG
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 10/06/22 22:56 V24843ANG
<1.50 µg/L 1.50 5.00Bromoform 1 10/06/22 22:56 V24843ANG
<0.280 µg/L 0.280 1.00Bromomethane 1 10/06/22 22:56 V24843ANG
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 10/06/22 22:56 V24843ANG
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 10/06/22 22:56 V24843ANG
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 10/06/22 22:56 V24843ANG
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 10/06/22 22:56 V24843ANG
<0.190 µg/L 0.190 0.500Chlorobenzene 1 10/06/22 22:56 V24843ANG
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 10/06/22 22:56 V24843ANG
<0.430 µg/L 0.430 1.00Chloroethane 1 10/06/22 22:56 V24843ANG
<0.220 µg/L 0.220 0.500Chloroform 1 10/06/22 22:56 V24843ANG
<0.220 µg/L 0.220 0.500Chloromethane 1 10/06/22 22:56 V24843ANG
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 10/06/22 22:56 V24843ANG
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 10/06/22 22:56 V24843ANG
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 10/06/22 22:56 V24843ANG
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 10/06/22 22:56 V24843ANG
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 10/06/22 22:56 V24843ANG
<0.230 µg/L 0.230 0.500Dibromomethane 1 10/06/22 22:56 V24843ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-4
89964 Matrix:
10/4/2022 8:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 10/06/22 22:56 V24843ANG
<0.190 µg/L 0.190 0.500
1,3-Dichlorobenzene 1 10/06/22 22:56 V24843ANG
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 10/06/22 22:56 V24843ANG
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 10/06/22 22:56 V24843ANG
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 10/06/22 22:56 V24843ANG
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 10/06/22 22:56 V24843ANG
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 10/06/22 22:56 V24843ANG
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 10/06/22 22:56 V24843ANG
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 10/06/22 22:56 V24843ANG
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 10/06/22 22:56 V24843ANG
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 10/06/22 22:56 V24843ANG
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 10/06/22 22:56 V24843ANG
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 10/06/22 22:56 V24843ANG
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 10/06/22 22:56 V24843ANG
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 10/06/22 22:56 V24843ANG
<42.0 µg/L 42.0 200Ethanol 1 10/06/22 22:56 V24843ANG
<0.170 µg/L 0.170 0.500Ethylbenzene 1 10/06/22 22:56 V24843ANG
<0.059 µg/L 0.059 10.0Ethyl Tertiary Butyl Ether (ETBE)1 10/06/22 22:56 V24843ANG
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 10/06/22 22:56 V24843ANG
<0.380 µg/L 0.380 1.002-Hexanone 1 10/06/22 22:56 V24843ANG
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 10/06/22 22:56 V24843ANG
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 10/06/22 22:56 V24843ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-4
89964 Matrix:
10/4/2022 8:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 10/06/22 22:56 V24843ANG
<0.140 µg/L 0.140 1.00
Methyl tert-butyl ether (MTBE)1 10/06/22 22:56 V24843ANG
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 10/06/22 22:56 V24843ANG
<0.330 µg/L 0.330 2.00Methylene Chloride 1 10/06/22 22:56 V24843ANG
<0.470 µg/L 0.470 1.00Naphthalene 1 10/06/22 22:56 V24843ANG
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 10/06/22 22:56 V24843ANG
<0.220 µg/L 0.220 0.500Styrene 1 10/06/22 22:56 V24843ANG
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 10/06/22 22:56 V24843ANG
<0.350 µg/L 0.350 10.0
tert-Butyl formate (TBF)1 10/06/22 22:56 V24843ANG
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 10/06/22 22:56 V24843ANG
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 10/06/22 22:56 V24843ANG
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 10/06/22 22:56 V24843ANG
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 10/06/22 22:56 V24843ANG
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 10/06/22 22:56 V24843ANG
<0.220 µg/L 0.220 0.500Toluene 1 10/06/22 22:56 V24843ANG
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 10/06/22 22:56 V24843ANG
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 10/06/22 22:56 V24843ANG
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 10/06/22 22:56 V24843ANG
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 10/06/22 22:56 V24843ANG
<0.180 µg/L 0.180 0.500Trichloroethene 1 10/06/22 22:56 V24843ANG
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 10/06/22 22:56 V24843ANG
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 10/06/22 22:56 V24843ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-4
89964 Matrix:
10/4/2022 8:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 10/06/22 22:56 V24843ANG
<0.180 µg/L 0.180 0.500
1,3,5-Trimethylbenzene 1 10/06/22 22:56 V24843ANG
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 10/06/22 22:56 V24843ANG
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 10/06/22 22:56 V24843ANG
<0.210 µg/L 0.210 0.500o-Xylene 1 10/06/22 22:56 V24843ANG
<0.420 µg/L 0.420 1.00m,p-Xylene 1 10/06/22 22:56 V24843ANG
<0.21 µg/L 0.210 0.500Xylene (Total)1 10/06/22 22:56 V24843
Surrogate: 4-Bromofluorobenzene 109 Limits: 70-130%10/06/22 22:561 ANG V24843
Surrogate: Dibromofluoromethane 112 Limits: 70-130%10/06/22 22:561 ANG V24843
Surrogate: 1,2-Dichloroethane - d4 98.4 Limits: 70-130%10/06/22 22:561 ANG V24843
Surrogate: Toluene-d8 98.0 Limits: 70-130%10/06/22 22:561 ANG V24843
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-4
89964 Matrix:
10/4/2022 8:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V24827 10/06/22 08:00
<11.5 µg/L 11.5 50.0Aliphatic C5-C8 1 10/06/22 14:59 V24828TBL
<25.8 µg/L 25.8 50.0
Aliphatic C9-C12 1 10/06/22 14:59 V24828TBL
<4.02 µg/L 4.02 50.0Aromatic C9-C10 1 10/06/22 14:59 V24828TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)96.1 Limits: 70-130%10/06/22 14:591 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)91.9 Limits: 70-130%10/06/22 14:591 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-5
89965 Matrix:
10/4/2022 8:45
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 10/06/22 23:19 6200BANG
Surrogate: 4-Bromofluorobenzene 110 Limits: 70-130%10/06/22 23:191 ANG V24843
Surrogate: Dibromofluoromethane 114 Limits: 70-130%10/06/22 23:191 ANG V24843
Surrogate: 1,2-Dichloroethane - d4 95.8 Limits: 70-130%10/06/22 23:191 ANG V24843
Surrogate: Toluene-d8 100 Limits: 70-130%10/06/22 23:191 ANG V24843
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-5
89965 Matrix:
10/4/2022 8:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 10/06/22 23:19 V24843ANG
<0.180 µg/L 0.180 0.500
Benzene 1 10/06/22 23:19 V24843ANG
<0.210 µg/L 0.210 0.500Bromobenzene 1 10/06/22 23:19 V24843ANG
<0.420 µg/L 0.420 1.00Bromochloromethane 1 10/06/22 23:19 V24843ANG
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 10/06/22 23:19 V24843ANG
<1.50 µg/L 1.50 5.00Bromoform 1 10/06/22 23:19 V24843ANG
<0.280 µg/L 0.280 1.00Bromomethane 1 10/06/22 23:19 V24843ANG
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 10/06/22 23:19 V24843ANG
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 10/06/22 23:19 V24843ANG
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 10/06/22 23:19 V24843ANG
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 10/06/22 23:19 V24843ANG
<0.190 µg/L 0.190 0.500Chlorobenzene 1 10/06/22 23:19 V24843ANG
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 10/06/22 23:19 V24843ANG
<0.430 µg/L 0.430 1.00Chloroethane 1 10/06/22 23:19 V24843ANG
<0.220 µg/L 0.220 0.500Chloroform 1 10/06/22 23:19 V24843ANG
<0.220 µg/L 0.220 0.500Chloromethane 1 10/06/22 23:19 V24843ANG
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 10/06/22 23:19 V24843ANG
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 10/06/22 23:19 V24843ANG
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 10/06/22 23:19 V24843ANG
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 10/06/22 23:19 V24843ANG
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 10/06/22 23:19 V24843ANG
<0.230 µg/L 0.230 0.500Dibromomethane 1 10/06/22 23:19 V24843ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-5
89965 Matrix:
10/4/2022 8:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 10/06/22 23:19 V24843ANG
<0.190 µg/L 0.190 0.500
1,3-Dichlorobenzene 1 10/06/22 23:19 V24843ANG
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 10/06/22 23:19 V24843ANG
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 10/06/22 23:19 V24843ANG
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 10/06/22 23:19 V24843ANG
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 10/06/22 23:19 V24843ANG
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 10/06/22 23:19 V24843ANG
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 10/06/22 23:19 V24843ANG
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 10/06/22 23:19 V24843ANG
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 10/06/22 23:19 V24843ANG
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 10/06/22 23:19 V24843ANG
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 10/06/22 23:19 V24843ANG
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 10/06/22 23:19 V24843ANG
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 10/06/22 23:19 V24843ANG
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 10/06/22 23:19 V24843ANG
<42.0 µg/L 42.0 200Ethanol 1 10/06/22 23:19 V24843ANG
<0.170 µg/L 0.170 0.500Ethylbenzene 1 10/06/22 23:19 V24843ANG
<0.059 µg/L 0.059 10.0Ethyl Tertiary Butyl Ether (ETBE)1 10/06/22 23:19 V24843ANG
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 10/06/22 23:19 V24843ANG
<0.380 µg/L 0.380 1.002-Hexanone 1 10/06/22 23:19 V24843ANG
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 10/06/22 23:19 V24843ANG
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 10/06/22 23:19 V24843ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-5
89965 Matrix:
10/4/2022 8:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 10/06/22 23:19 V24843ANG
<0.140 µg/L 0.140 1.00
Methyl tert-butyl ether (MTBE)1 10/06/22 23:19 V24843ANG
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 10/06/22 23:19 V24843ANG
<0.330 µg/L 0.330 2.00Methylene Chloride 1 10/06/22 23:19 V24843ANG
<0.470 µg/L 0.470 1.00Naphthalene 1 10/06/22 23:19 V24843ANG
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 10/06/22 23:19 V24843ANG
<0.220 µg/L 0.220 0.500Styrene 1 10/06/22 23:19 V24843ANG
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 10/06/22 23:19 V24843ANG
<0.350 µg/L 0.350 10.0
tert-Butyl formate (TBF)1 10/06/22 23:19 V24843ANG
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 10/06/22 23:19 V24843ANG
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 10/06/22 23:19 V24843ANG
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 10/06/22 23:19 V24843ANG
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 10/06/22 23:19 V24843ANG
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 10/06/22 23:19 V24843ANG
<0.220 µg/L 0.220 0.500Toluene 1 10/06/22 23:19 V24843ANG
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 10/06/22 23:19 V24843ANG
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 10/06/22 23:19 V24843ANG
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 10/06/22 23:19 V24843ANG
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 10/06/22 23:19 V24843ANG
<0.180 µg/L 0.180 0.500Trichloroethene 1 10/06/22 23:19 V24843ANG
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 10/06/22 23:19 V24843ANG
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 10/06/22 23:19 V24843ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-5
89965 Matrix:
10/4/2022 8:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 10/06/22 23:19 V24843ANG
<0.180 µg/L 0.180 0.500
1,3,5-Trimethylbenzene 1 10/06/22 23:19 V24843ANG
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 10/06/22 23:19 V24843ANG
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 10/06/22 23:19 V24843ANG
<0.210 µg/L 0.210 0.500o-Xylene 1 10/06/22 23:19 V24843ANG
<0.420 µg/L 0.420 1.00m,p-Xylene 1 10/06/22 23:19 V24843ANG
<0.21 µg/L 0.210 0.500Xylene (Total)1 10/06/22 23:19 V24843
Surrogate: 4-Bromofluorobenzene 110 Limits: 70-130%10/06/22 23:191 ANG V24843
Surrogate: Dibromofluoromethane 114 Limits: 70-130%10/06/22 23:191 ANG V24843
Surrogate: 1,2-Dichloroethane - d4 95.8 Limits: 70-130%10/06/22 23:191 ANG V24843
Surrogate: Toluene-d8 100 Limits: 70-130%10/06/22 23:191 ANG V24843
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-5
89965 Matrix:
10/4/2022 8:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V24827 10/06/22 08:00
<11.5 µg/L 11.5 50.0Aliphatic C5-C8 1 10/06/22 15:22 V24828TBL
<25.8 µg/L 25.8 50.0
Aliphatic C9-C12 1 10/06/22 15:22 V24828TBL
<4.02 µg/L 4.02 50.0Aromatic C9-C10 1 10/06/22 15:22 V24828TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)93.6 Limits: 70-130%10/06/22 15:221 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)82.7 Limits: 70-130%10/06/22 15:221 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-6
89966 Matrix:
10/4/2022 9:15
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 10/06/22 23:42 6200BANG
Surrogate: 4-Bromofluorobenzene 107 Limits: 70-130%10/06/22 23:421 ANG V24843
Surrogate: Dibromofluoromethane 117 Limits: 70-130%10/06/22 23:421 ANG V24843
Surrogate: 1,2-Dichloroethane - d4 98.0 Limits: 70-130%10/06/22 23:421 ANG V24843
Surrogate: Toluene-d8 99.2 Limits: 70-130%10/06/22 23:421 ANG V24843
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-6
89966 Matrix:
10/4/2022 9:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 10/06/22 23:42 V24843ANG
<0.180 µg/L 0.180 0.500
Benzene 1 10/06/22 23:42 V24843ANG
<0.210 µg/L 0.210 0.500Bromobenzene 1 10/06/22 23:42 V24843ANG
<0.420 µg/L 0.420 1.00Bromochloromethane 1 10/06/22 23:42 V24843ANG
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 10/06/22 23:42 V24843ANG
<1.50 µg/L 1.50 5.00Bromoform 1 10/06/22 23:42 V24843ANG
<0.280 µg/L 0.280 1.00Bromomethane 1 10/06/22 23:42 V24843ANG
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 10/06/22 23:42 V24843ANG
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 10/06/22 23:42 V24843ANG
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 10/06/22 23:42 V24843ANG
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 10/06/22 23:42 V24843ANG
<0.190 µg/L 0.190 0.500Chlorobenzene 1 10/06/22 23:42 V24843ANG
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 10/06/22 23:42 V24843ANG
<0.430 µg/L 0.430 1.00Chloroethane 1 10/06/22 23:42 V24843ANG
<0.220 µg/L 0.220 0.500Chloroform 1 10/06/22 23:42 V24843ANG
<0.220 µg/L 0.220 0.500Chloromethane 1 10/06/22 23:42 V24843ANG
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 10/06/22 23:42 V24843ANG
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 10/06/22 23:42 V24843ANG
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 10/06/22 23:42 V24843ANG
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 10/06/22 23:42 V24843ANG
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 10/06/22 23:42 V24843ANG
<0.230 µg/L 0.230 0.500Dibromomethane 1 10/06/22 23:42 V24843ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-6
89966 Matrix:
10/4/2022 9:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 10/06/22 23:42 V24843ANG
<0.190 µg/L 0.190 0.500
1,3-Dichlorobenzene 1 10/06/22 23:42 V24843ANG
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 10/06/22 23:42 V24843ANG
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 10/06/22 23:42 V24843ANG
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 10/06/22 23:42 V24843ANG
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 10/06/22 23:42 V24843ANG
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 10/06/22 23:42 V24843ANG
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 10/06/22 23:42 V24843ANG
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 10/06/22 23:42 V24843ANG
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 10/06/22 23:42 V24843ANG
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 10/06/22 23:42 V24843ANG
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 10/06/22 23:42 V24843ANG
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 10/06/22 23:42 V24843ANG
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 10/06/22 23:42 V24843ANG
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 10/06/22 23:42 V24843ANG
<42.0 µg/L 42.0 200Ethanol 1 10/06/22 23:42 V24843ANG
<0.170 µg/L 0.170 0.500Ethylbenzene 1 10/06/22 23:42 V24843ANG
<0.059 µg/L 0.059 10.0Ethyl Tertiary Butyl Ether (ETBE)1 10/06/22 23:42 V24843ANG
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 10/06/22 23:42 V24843ANG
<0.380 µg/L 0.380 1.002-Hexanone 1 10/06/22 23:42 V24843ANG
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 10/06/22 23:42 V24843ANG
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 10/06/22 23:42 V24843ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 42 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-6
89966 Matrix:
10/4/2022 9:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 10/06/22 23:42 V24843ANG
<0.140 µg/L 0.140 1.00
Methyl tert-butyl ether (MTBE)1 10/06/22 23:42 V24843ANG
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 10/06/22 23:42 V24843ANG
<0.330 µg/L 0.330 2.00Methylene Chloride 1 10/06/22 23:42 V24843ANG
<0.470 µg/L 0.470 1.00Naphthalene 1 10/06/22 23:42 V24843ANG
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 10/06/22 23:42 V24843ANG
<0.220 µg/L 0.220 0.500Styrene 1 10/06/22 23:42 V24843ANG
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 10/06/22 23:42 V24843ANG
<0.350 µg/L 0.350 10.0
tert-Butyl formate (TBF)1 10/06/22 23:42 V24843ANG
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 10/06/22 23:42 V24843ANG
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 10/06/22 23:42 V24843ANG
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 10/06/22 23:42 V24843ANG
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 10/06/22 23:42 V24843ANG
0.266 J µg/L 0.220 0.500Tetrachloroethene 1 10/06/22 23:42 V24843ANG
<0.220 µg/L 0.220 0.500Toluene 1 10/06/22 23:42 V24843ANG
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 10/06/22 23:42 V24843ANG
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 10/06/22 23:42 V24843ANG
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 10/06/22 23:42 V24843ANG
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 10/06/22 23:42 V24843ANG
<0.180 µg/L 0.180 0.500Trichloroethene 1 10/06/22 23:42 V24843ANG
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 10/06/22 23:42 V24843ANG
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 10/06/22 23:42 V24843ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-6
89966 Matrix:
10/4/2022 9:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 10/06/22 23:42 V24843ANG
<0.180 µg/L 0.180 0.500
1,3,5-Trimethylbenzene 1 10/06/22 23:42 V24843ANG
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 10/06/22 23:42 V24843ANG
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 10/06/22 23:42 V24843ANG
<0.210 µg/L 0.210 0.500o-Xylene 1 10/06/22 23:42 V24843ANG
<0.420 µg/L 0.420 1.00m,p-Xylene 1 10/06/22 23:42 V24843ANG
<0.21 µg/L 0.210 0.500Xylene (Total)1 10/06/22 23:42 V24843
Surrogate: 4-Bromofluorobenzene 107 Limits: 70-130%10/06/22 23:421 ANG V24843
Surrogate: Dibromofluoromethane 117 Limits: 70-130%10/06/22 23:421 ANG V24843
Surrogate: 1,2-Dichloroethane - d4 98.0 Limits: 70-130%10/06/22 23:421 ANG V24843
Surrogate: Toluene-d8 99.2 Limits: 70-130%10/06/22 23:421 ANG V24843
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:MW-6
89966 Matrix:
10/4/2022 9:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V24827 10/06/22 08:00
<11.5 µg/L 11.5 50.0Aliphatic C5-C8 1 10/06/22 15:46 V24828TBL
<25.8 µg/L 25.8 50.0
Aliphatic C9-C12 1 10/06/22 15:46 V24828TBL
<4.02 µg/L 4.02 50.0Aromatic C9-C10 1 10/06/22 15:46 V24828TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)94.0 Limits: 70-130%10/06/22 15:461 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)88.8 Limits: 70-130%10/06/22 15:461 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 45 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:VEW-1
89967 Matrix:
10/4/2022 9:35
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 10/07/22 00:05 6200BANG
Surrogate: 4-Bromofluorobenzene 114 Limits: 70-130%10/07/22 00:051 ANG V24843
Surrogate: Dibromofluoromethane 115 Limits: 70-130%10/07/22 00:051 ANG V24843
Surrogate: 1,2-Dichloroethane - d4 92.6 Limits: 70-130%10/07/22 00:051 ANG V24843
Surrogate: Toluene-d8 97.8 Limits: 70-130%10/07/22 00:051 ANG V24843
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 46 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:VEW-1
89967 Matrix:
10/4/2022 9:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 10/07/22 00:05 V24843ANG
<0.180 µg/L 0.180 0.500
Benzene 1 10/07/22 00:05 V24843ANG
<0.210 µg/L 0.210 0.500Bromobenzene 1 10/07/22 00:05 V24843ANG
<0.420 µg/L 0.420 1.00Bromochloromethane 1 10/07/22 00:05 V24843ANG
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 10/07/22 00:05 V24843ANG
<1.50 µg/L 1.50 5.00Bromoform 1 10/07/22 00:05 V24843ANG
<0.280 µg/L 0.280 1.00Bromomethane 1 10/07/22 00:05 V24843ANG
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 10/07/22 00:05 V24843ANG
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 10/07/22 00:05 V24843ANG
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 10/07/22 00:05 V24843ANG
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 10/07/22 00:05 V24843ANG
<0.190 µg/L 0.190 0.500Chlorobenzene 1 10/07/22 00:05 V24843ANG
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 10/07/22 00:05 V24843ANG
<0.430 µg/L 0.430 1.00Chloroethane 1 10/07/22 00:05 V24843ANG
<0.220 µg/L 0.220 0.500Chloroform 1 10/07/22 00:05 V24843ANG
<0.220 µg/L 0.220 0.500Chloromethane 1 10/07/22 00:05 V24843ANG
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 10/07/22 00:05 V24843ANG
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 10/07/22 00:05 V24843ANG
1.51 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 10/07/22 00:05 V24843ANG
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 10/07/22 00:05 V24843ANG
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 10/07/22 00:05 V24843ANG
<0.230 µg/L 0.230 0.500Dibromomethane 1 10/07/22 00:05 V24843ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 47 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:VEW-1
89967 Matrix:
10/4/2022 9:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 10/07/22 00:05 V24843ANG
<0.190 µg/L 0.190 0.500
1,3-Dichlorobenzene 1 10/07/22 00:05 V24843ANG
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 10/07/22 00:05 V24843ANG
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 10/07/22 00:05 V24843ANG
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 10/07/22 00:05 V24843ANG
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 10/07/22 00:05 V24843ANG
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 10/07/22 00:05 V24843ANG
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 10/07/22 00:05 V24843ANG
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 10/07/22 00:05 V24843ANG
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 10/07/22 00:05 V24843ANG
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 10/07/22 00:05 V24843ANG
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 10/07/22 00:05 V24843ANG
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 10/07/22 00:05 V24843ANG
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 10/07/22 00:05 V24843ANG
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 10/07/22 00:05 V24843ANG
<42.0 µg/L 42.0 200Ethanol 1 10/07/22 00:05 V24843ANG
<0.170 µg/L 0.170 0.500Ethylbenzene 1 10/07/22 00:05 V24843ANG
<0.059 µg/L 0.059 10.0Ethyl Tertiary Butyl Ether (ETBE)1 10/07/22 00:05 V24843ANG
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 10/07/22 00:05 V24843ANG
<0.380 µg/L 0.380 1.002-Hexanone 1 10/07/22 00:05 V24843ANG
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 10/07/22 00:05 V24843ANG
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 10/07/22 00:05 V24843ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 48 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:VEW-1
89967 Matrix:
10/4/2022 9:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 10/07/22 00:05 V24843ANG
8.82 µg/L 0.140 1.00
Methyl tert-butyl ether (MTBE)1 10/07/22 00:05 V24843ANG
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 10/07/22 00:05 V24843ANG
<0.330 µg/L 0.330 2.00Methylene Chloride 1 10/07/22 00:05 V24843ANG
<0.470 µg/L 0.470 1.00Naphthalene 1 10/07/22 00:05 V24843ANG
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 10/07/22 00:05 V24843ANG
<0.220 µg/L 0.220 0.500Styrene 1 10/07/22 00:05 V24843ANG
7.82 J µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 10/07/22 00:05 V24843ANG
<0.350 µg/L 0.350 10.0
tert-Butyl formate (TBF)1 10/07/22 00:05 V24843ANG
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 10/07/22 00:05 V24843ANG
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 10/07/22 00:05 V24843ANG
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 10/07/22 00:05 V24843ANG
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 10/07/22 00:05 V24843ANG
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 10/07/22 00:05 V24843ANG
<0.220 µg/L 0.220 0.500Toluene 1 10/07/22 00:05 V24843ANG
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 10/07/22 00:05 V24843ANG
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 10/07/22 00:05 V24843ANG
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 10/07/22 00:05 V24843ANG
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 10/07/22 00:05 V24843ANG
<0.180 µg/L 0.180 0.500Trichloroethene 1 10/07/22 00:05 V24843ANG
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 10/07/22 00:05 V24843ANG
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 10/07/22 00:05 V24843ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 49 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:VEW-1
89967 Matrix:
10/4/2022 9:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 10/07/22 00:05 V24843ANG
<0.180 µg/L 0.180 0.500
1,3,5-Trimethylbenzene 1 10/07/22 00:05 V24843ANG
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 10/07/22 00:05 V24843ANG
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 10/07/22 00:05 V24843ANG
<0.210 µg/L 0.210 0.500o-Xylene 1 10/07/22 00:05 V24843ANG
<0.420 µg/L 0.420 1.00m,p-Xylene 1 10/07/22 00:05 V24843ANG
<0.21 µg/L 0.210 0.500Xylene (Total)1 10/07/22 00:05 V24843
Surrogate: 4-Bromofluorobenzene 114 Limits: 70-130%10/07/22 00:051 ANG V24843
Surrogate: Dibromofluoromethane 115 Limits: 70-130%10/07/22 00:051 ANG V24843
Surrogate: 1,2-Dichloroethane - d4 92.6 Limits: 70-130%10/07/22 00:051 ANG V24843
Surrogate: Toluene-d8 97.8 Limits: 70-130%10/07/22 00:051 ANG V24843
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 50 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:VEW-1
89967 Matrix:
10/4/2022 9:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V24827 10/06/22 08:00
<11.5 µg/L 11.5 50.0Aliphatic C5-C8 1 10/06/22 16:10 V24828TBL
<25.8 µg/L 25.8 50.0
Aliphatic C9-C12 1 10/06/22 16:10 V24828TBL
<4.02 µg/L 4.02 50.0Aromatic C9-C10 1 10/06/22 16:10 V24828TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)82.9 Limits: 70-130%10/06/22 16:101 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)76.1 Limits: 70-130%10/06/22 16:101 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 51 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:SW-1
89968 Matrix:
10/4/2022 10:00
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 10/07/22 00:29 6200BANG
Surrogate: 4-Bromofluorobenzene 111 Limits: 70-130%10/07/22 00:291 ANG V24843
Surrogate: Dibromofluoromethane 117 Limits: 70-130%10/07/22 00:291 ANG V24843
Surrogate: 1,2-Dichloroethane - d4 97.4 Limits: 70-130%10/07/22 00:291 ANG V24843
Surrogate: Toluene-d8 97.2 Limits: 70-130%10/07/22 00:291 ANG V24843
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 52 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:SW-1
89968 Matrix:
10/4/2022 10:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 10/07/22 00:29 V24843ANG
<0.180 µg/L 0.180 0.500
Benzene 1 10/07/22 00:29 V24843ANG
<0.210 µg/L 0.210 0.500Bromobenzene 1 10/07/22 00:29 V24843ANG
<0.420 µg/L 0.420 1.00Bromochloromethane 1 10/07/22 00:29 V24843ANG
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 10/07/22 00:29 V24843ANG
<1.50 µg/L 1.50 5.00Bromoform 1 10/07/22 00:29 V24843ANG
<0.280 µg/L 0.280 1.00Bromomethane 1 10/07/22 00:29 V24843ANG
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 10/07/22 00:29 V24843ANG
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 10/07/22 00:29 V24843ANG
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 10/07/22 00:29 V24843ANG
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 10/07/22 00:29 V24843ANG
<0.190 µg/L 0.190 0.500Chlorobenzene 1 10/07/22 00:29 V24843ANG
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 10/07/22 00:29 V24843ANG
<0.430 µg/L 0.430 1.00Chloroethane 1 10/07/22 00:29 V24843ANG
<0.220 µg/L 0.220 0.500Chloroform 1 10/07/22 00:29 V24843ANG
<0.220 µg/L 0.220 0.500Chloromethane 1 10/07/22 00:29 V24843ANG
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 10/07/22 00:29 V24843ANG
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 10/07/22 00:29 V24843ANG
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 10/07/22 00:29 V24843ANG
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 10/07/22 00:29 V24843ANG
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 10/07/22 00:29 V24843ANG
<0.230 µg/L 0.230 0.500Dibromomethane 1 10/07/22 00:29 V24843ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 53 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:SW-1
89968 Matrix:
10/4/2022 10:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 10/07/22 00:29 V24843ANG
<0.190 µg/L 0.190 0.500
1,3-Dichlorobenzene 1 10/07/22 00:29 V24843ANG
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 10/07/22 00:29 V24843ANG
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 10/07/22 00:29 V24843ANG
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 10/07/22 00:29 V24843ANG
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 10/07/22 00:29 V24843ANG
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 10/07/22 00:29 V24843ANG
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 10/07/22 00:29 V24843ANG
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 10/07/22 00:29 V24843ANG
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 10/07/22 00:29 V24843ANG
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 10/07/22 00:29 V24843ANG
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 10/07/22 00:29 V24843ANG
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 10/07/22 00:29 V24843ANG
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 10/07/22 00:29 V24843ANG
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 10/07/22 00:29 V24843ANG
<42.0 µg/L 42.0 200Ethanol 1 10/07/22 00:29 V24843ANG
<0.170 µg/L 0.170 0.500Ethylbenzene 1 10/07/22 00:29 V24843ANG
<0.059 µg/L 0.059 10.0Ethyl Tertiary Butyl Ether (ETBE)1 10/07/22 00:29 V24843ANG
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 10/07/22 00:29 V24843ANG
<0.380 µg/L 0.380 1.002-Hexanone 1 10/07/22 00:29 V24843ANG
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 10/07/22 00:29 V24843ANG
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 10/07/22 00:29 V24843ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 54 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:SW-1
89968 Matrix:
10/4/2022 10:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 10/07/22 00:29 V24843ANG
<0.140 µg/L 0.140 1.00
Methyl tert-butyl ether (MTBE)1 10/07/22 00:29 V24843ANG
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 10/07/22 00:29 V24843ANG
<0.330 µg/L 0.330 2.00Methylene Chloride 1 10/07/22 00:29 V24843ANG
<0.470 µg/L 0.470 1.00Naphthalene 1 10/07/22 00:29 V24843ANG
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 10/07/22 00:29 V24843ANG
<0.220 µg/L 0.220 0.500Styrene 1 10/07/22 00:29 V24843ANG
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 10/07/22 00:29 V24843ANG
<0.350 µg/L 0.350 10.0
tert-Butyl formate (TBF)1 10/07/22 00:29 V24843ANG
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 10/07/22 00:29 V24843ANG
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 10/07/22 00:29 V24843ANG
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 10/07/22 00:29 V24843ANG
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 10/07/22 00:29 V24843ANG
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 10/07/22 00:29 V24843ANG
<0.220 µg/L 0.220 0.500Toluene 1 10/07/22 00:29 V24843ANG
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 10/07/22 00:29 V24843ANG
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 10/07/22 00:29 V24843ANG
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 10/07/22 00:29 V24843ANG
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 10/07/22 00:29 V24843ANG
<0.180 µg/L 0.180 0.500Trichloroethene 1 10/07/22 00:29 V24843ANG
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 10/07/22 00:29 V24843ANG
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 10/07/22 00:29 V24843ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 55 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:SW-1
89968 Matrix:
10/4/2022 10:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24842 10/06/22 09:00
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 10/07/22 00:29 V24843ANG
<0.180 µg/L 0.180 0.500
1,3,5-Trimethylbenzene 1 10/07/22 00:29 V24843ANG
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 10/07/22 00:29 V24843ANG
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 10/07/22 00:29 V24843ANG
<0.210 µg/L 0.210 0.500o-Xylene 1 10/07/22 00:29 V24843ANG
<0.420 µg/L 0.420 1.00m,p-Xylene 1 10/07/22 00:29 V24843ANG
<0.21 µg/L 0.210 0.500Xylene (Total)1 10/07/22 00:29 V24843
Surrogate: 4-Bromofluorobenzene 111 Limits: 70-130%10/07/22 00:291 ANG V24843
Surrogate: Dibromofluoromethane 117 Limits: 70-130%10/07/22 00:291 ANG V24843
Surrogate: 1,2-Dichloroethane - d4 97.4 Limits: 70-130%10/07/22 00:291 ANG V24843
Surrogate: Toluene-d8 97.2 Limits: 70-130%10/07/22 00:291 ANG V24843
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 56 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:SW-1
89968 Matrix:
10/4/2022 10:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V24827 10/06/22 08:00
<11.5 µg/L 11.5 50.0Aliphatic C5-C8 1 10/06/22 16:34 V24828TBL
<25.8 µg/L 25.8 50.0
Aliphatic C9-C12 1 10/06/22 16:34 V24828TBL
<4.02 µg/L 4.02 50.0Aromatic C9-C10 1 10/06/22 16:34 V24828TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)86.4 Limits: 70-130%10/06/22 16:341 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)81.9 Limits: 70-130%10/06/22 16:341 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 57 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:TRIP BLANK
89969 Matrix:
10/4/2022 0:00
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 10/06/22 12:26 6200BMSA
Surrogate: 4-Bromofluorobenzene 93.0 Limits: 70-130%10/06/22 12:261 MSA V24860
Surrogate: Dibromofluoromethane 95.8 Limits: 70-130%10/06/22 12:261 MSA V24860
Surrogate: 1,2-Dichloroethane - d4 84.6 Limits: 70-130%10/06/22 12:261 MSA V24860
Surrogate: Toluene-d8 77.6 Limits: 70-130%10/06/22 12:261 MSA V24860
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 58 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:TRIP BLANK
89969 Matrix:
10/4/2022 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24859 10/06/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 10/06/22 12:26 V24860MSA
<0.180 µg/L 0.180 0.500
Benzene 1 10/06/22 12:26 V24860MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 10/06/22 12:26 V24860MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 10/06/22 12:26 V24860MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 10/06/22 12:26 V24860MSA
<1.50 µg/L 1.50 5.00Bromoform 1 10/06/22 12:26 V24860MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 10/06/22 12:26 V24860MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 10/06/22 12:26 V24860MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 10/06/22 12:26 V24860MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 10/06/22 12:26 V24860MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 10/06/22 12:26 V24860MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 10/06/22 12:26 V24860MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 10/06/22 12:26 V24860MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 10/06/22 12:26 V24860MSA
<0.220 µg/L 0.220 0.500Chloroform 1 10/06/22 12:26 V24860MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 10/06/22 12:26 V24860MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 10/06/22 12:26 V24860MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 10/06/22 12:26 V24860MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 10/06/22 12:26 V24860MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 10/06/22 12:26 V24860MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 10/06/22 12:26 V24860MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 10/06/22 12:26 V24860MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 59 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:TRIP BLANK
89969 Matrix:
10/4/2022 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24859 10/06/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 10/06/22 12:26 V24860MSA
<0.190 µg/L 0.190 0.500
1,3-Dichlorobenzene 1 10/06/22 12:26 V24860MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 10/06/22 12:26 V24860MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 10/06/22 12:26 V24860MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 10/06/22 12:26 V24860MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 10/06/22 12:26 V24860MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 10/06/22 12:26 V24860MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 10/06/22 12:26 V24860MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 10/06/22 12:26 V24860MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 10/06/22 12:26 V24860MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 10/06/22 12:26 V24860MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 10/06/22 12:26 V24860MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 10/06/22 12:26 V24860MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 10/06/22 12:26 V24860MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 10/06/22 12:26 V24860MSA
<42.0 µg/L 42.0 200Ethanol 1 10/06/22 12:26 V24860MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 10/06/22 12:26 V24860MSA
<0.059 µg/L 0.059 10.0Ethyl Tertiary Butyl Ether (ETBE)1 10/06/22 12:26 V24860MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 10/06/22 12:26 V24860MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 10/06/22 12:26 V24860MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 10/06/22 12:26 V24860MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 10/06/22 12:26 V24860MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 60 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:TRIP BLANK
89969 Matrix:
10/4/2022 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24859 10/06/22 09:00
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 10/06/22 12:26 V24860MSA
<0.140 µg/L 0.140 1.00
Methyl tert-butyl ether (MTBE)1 10/06/22 12:26 V24860MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 10/06/22 12:26 V24860MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 10/06/22 12:26 V24860MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 10/06/22 12:26 V24860MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 10/06/22 12:26 V24860MSA
<0.220 µg/L 0.220 0.500Styrene 1 10/06/22 12:26 V24860MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 10/06/22 12:26 V24860MSA
<0.350 µg/L 0.350 10.0
tert-Butyl formate (TBF)1 10/06/22 12:26 V24860MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 10/06/22 12:26 V24860MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 10/06/22 12:26 V24860MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 10/06/22 12:26 V24860MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 10/06/22 12:26 V24860MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 10/06/22 12:26 V24860MSA
<0.220 µg/L 0.220 0.500Toluene 1 10/06/22 12:26 V24860MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 10/06/22 12:26 V24860MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 10/06/22 12:26 V24860MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 10/06/22 12:26 V24860MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 10/06/22 12:26 V24860MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 10/06/22 12:26 V24860MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 10/06/22 12:26 V24860MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 10/06/22 12:26 V24860MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 61 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:TRIP BLANK
89969 Matrix:
10/4/2022 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V24859 10/06/22 09:00
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 10/06/22 12:26 V24860MSA
<0.180 µg/L 0.180 0.500
1,3,5-Trimethylbenzene 1 10/06/22 12:26 V24860MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 10/06/22 12:26 V24860MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 10/06/22 12:26 V24860MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 10/06/22 12:26 V24860MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 10/06/22 12:26 V24860MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 10/06/22 12:26 V24860
Surrogate: 4-Bromofluorobenzene 93.0 Limits: 70-130%10/06/22 12:261 MSA V24860
Surrogate: Dibromofluoromethane 95.8 Limits: 70-130%10/06/22 12:261 MSA V24860
Surrogate: 1,2-Dichloroethane - d4 84.6 Limits: 70-130%10/06/22 12:261 MSA V24860
Surrogate: Toluene-d8 77.6 Limits: 70-130%10/06/22 12:261 MSA V24860
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 62 of 84
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
22-278-0022
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
P-1326 Received : 10/05/2022
Ray's Quick Stop
Report Date : 10/13/2022
Sample ID :
Lab No :
Sampled:TRIP BLANK
89969 Matrix:
10/4/2022 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V24827 10/06/22 08:00
<11.5 µg/L 11.5 50.0Aliphatic C5-C8 1 10/06/22 13:48 V24828TBL
<25.8 µg/L 25.8 50.0
Aliphatic C9-C12 1 10/06/22 13:48 V24828TBL
<4.02 µg/L 4.02 50.0Aromatic C9-C10 1 10/06/22 13:48 V24828TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)101 Limits: 70-130%10/06/22 13:481 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)79.3 Limits: 70-130%10/06/22 13:481 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 63 of 84
Quality Control Data
22-278-0022Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Ray's Quick Stop
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V24843QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V24842
Associated Lab Samples: 89962, 89963, 89964, 89965, 89966, 89967, 89968
LRB-V24842 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/06/22 21:4610.01.80<1.80µg/LAcetone
10/06/22 21:460.5000.180<0.180µg/LBenzene
10/06/22 21:460.5000.210<0.210µg/LBromobenzene
10/06/22 21:461.000.420<0.420µg/LBromochloromethane
10/06/22 21:460.5000.160<0.160µg/LBromodichloromethane
10/06/22 21:465.001.50<1.50µg/LBromoform
10/06/22 21:461.000.280<0.280µg/LBromomethane
10/06/22 21:460.5000.180<0.180µg/Ln-Butylbenzene
10/06/22 21:460.5000.200<0.200µg/Lsec-Butyl benzene
10/06/22 21:462.000.920<0.920µg/Ltert-Butyl benzene
10/06/22 21:460.5000.180<0.180µg/LCarbon Tetrachloride
10/06/22 21:460.5000.190<0.190µg/LChlorobenzene
10/06/22 21:460.5000.190<0.190µg/LChlorodibromomethane
10/06/22 21:461.000.430<0.430µg/LChloroethane
10/06/22 21:460.5000.220<0.220µg/LChloroform
10/06/22 21:460.5000.220<0.220µg/LChloromethane
10/06/22 21:460.5000.200<0.200µg/L2-Chlorotoluene
10/06/22 21:460.5000.200<0.200µg/L4-Chlorotoluene
10/06/22 21:460.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
10/06/22 21:462.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
10/06/22 21:460.5000.200<0.200µg/L1,2-Dibromoethane
10/06/22 21:460.5000.230<0.230µg/LDibromomethane
10/06/22 21:460.5000.220<0.220µg/L1,2-Dichlorobenzene
10/06/22 21:460.5000.190<0.190µg/L1,3-Dichlorobenzene
10/06/22 21:460.5000.210<0.210µg/L1,4-Dichlorobenzene
10/06/22 21:465.001.20<1.20µg/LDichlorodifluoromethane
10/06/22 21:460.5000.240<0.240µg/L1,1-Dichloroethane
Page 1 of 19Date:10/13/2022 01:44 PM
Page 64 of 84
Quality Control Data
22-278-0022Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Ray's Quick Stop
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V24843QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V24842
Associated Lab Samples: 89962, 89963, 89964, 89965, 89966, 89967, 89968
LRB-V24842 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/06/22 21:460.5000.150<0.150µg/L1,2-Dichloroethane
10/06/22 21:460.5000.150<0.150µg/L1,1-Dichloroethene
10/06/22 21:460.5000.200<0.200µg/Lcis-1,2-Dichloroethene
10/06/22 21:460.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
10/06/22 21:460.5000.190<0.190µg/L1,2-Dichloropropane
10/06/22 21:460.5000.130<0.130µg/L1,3-Dichloropropane
10/06/22 21:462.000.210<0.210µg/L2,2-Dichloropropane
10/06/22 21:460.5000.200<0.200µg/L1,1-Dichloropropene
10/06/22 21:460.5000.210<0.210µg/Lcis-1,3-Dichloropropene
10/06/22 21:460.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
10/06/22 21:4620042.0<42.0µg/LEthanol
10/06/22 21:460.5000.170<0.170µg/LEthylbenzene
10/06/22 21:4610.00.059<0.059µg/LEthyl Tertiary Butyl Ether (ETBE)
10/06/22 21:463.000.350<0.350µg/LHexachlorobutadiene
10/06/22 21:461.000.380<0.380µg/L2-Hexanone
10/06/22 21:460.5000.180<0.180µg/LIsopropylbenzene
10/06/22 21:460.5000.089<0.089µg/L4-Isopropyl toluene
10/06/22 21:465.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
10/06/22 21:461.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
10/06/22 21:461.000.078<0.078µg/L4-Methyl-2-Pentanone
10/06/22 21:462.000.330<0.330µg/LMethylene Chloride
10/06/22 21:461.000.470<0.470µg/LNaphthalene
10/06/22 21:460.5000.190<0.190µg/Ln-Propylbenzene
10/06/22 21:460.5000.220<0.220µg/LStyrene
10/06/22 21:4610.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
10/06/22 21:4610.00.350<0.350µg/Ltert-Butyl formate (TBF)
10/06/22 21:4610.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
Page 2 of 19Date:10/13/2022 01:44 PM
Page 65 of 84
Quality Control Data
22-278-0022Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Ray's Quick Stop
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V24843QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V24842
Associated Lab Samples: 89962, 89963, 89964, 89965, 89966, 89967, 89968
LRB-V24842 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/06/22 21:4610.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
10/06/22 21:460.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
10/06/22 21:460.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
10/06/22 21:460.5000.220<0.220µg/LTetrachloroethene
10/06/22 21:460.5000.220<0.220µg/LToluene
10/06/22 21:460.5000.380<0.380µg/L1,2,3-Trichlorobenzene
10/06/22 21:460.5000.310<0.310µg/L1,2,4-Trichlorobenzene
10/06/22 21:460.5000.160<0.160µg/L1,1,1-Trichloroethane
10/06/22 21:460.5000.096<0.096µg/L1,1,2-Trichloroethane
10/06/22 21:460.5000.180<0.180µg/LTrichloroethene
10/06/22 21:460.5000.180<0.180µg/LTrichlorofluoromethane
10/06/22 21:460.5000.270<0.270µg/L1,2,3-Trichloropropane
10/06/22 21:460.5000.190<0.190µg/L1,2,4-Trimethylbenzene
10/06/22 21:460.5000.180<0.180µg/L1,3,5-Trimethylbenzene
10/06/22 21:465.001.00<1.00µg/LVinyl Acetate
10/06/22 21:460.5000.170<0.170µg/LVinyl Chloride
10/06/22 21:460.5000.210<0.210µg/Lo-Xylene
10/06/22 21:461.000.420<0.420µg/Lm,p-Xylene
10/06/22 21:4610.01.00<1.00µg/L3,3-Dimethyl-1-butanol
10/06/22 21:464-Bromofluorobenzene (S)111 70-130
10/06/22 21:46Dibromofluoromethane (S)117 70-130
10/06/22 21:461,2-Dichloroethane - d4 (S)95.0 70-130
10/06/22 21:46Toluene-d8 (S)96.0 70-130
Page 3 of 19Date:10/13/2022 01:44 PM
Page 66 of 84
Quality Control Data
22-278-0022Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Ray's Quick Stop
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V24843QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V24842
LCS-V24842 LCSD-V24842Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
41.2 10311847.340.0µg/LAcetone 40-160 13.7 20.0
22.3 11211723.420.0µg/LBenzene 70-130 4.8 20.0
23.7 11912424.720.0µg/LBromobenzene 70-130 4.1 20.0
21.2 10610921.820.0µg/LBromodichloromethane 70-130 2.7 20.0
22.5 11311322.520.0µg/LBromoform 70-130 0.0 20.0
20.7 10410621.220.0µg/Ln-Butylbenzene 70-130 2.3 20.0
19.8 99.010220.320.0µg/Lsec-Butyl benzene 70-130 2.4 20.0
20.8 10410420.820.0µg/Ltert-Butyl benzene 70-130 0.0 20.0
21.9 11011322.520.0µg/LChlorobenzene 70-130 2.7 20.0
19.5 97.510420.720.0µg/LChlorodibromomethane 70-130 5.9 20.0
19.3 96.511122.220.0µg/LChloroethane 60-140 13.9 20.0
22.5 11311623.120.0µg/LChloroform 70-130 2.6 20.0
19.6 98.099.519.920.0µg/LChloromethane 60-140 1.5 20.0
19.8 99.010420.720.0µg/L2-Chlorotoluene 70-130 4.4 20.0
20.8 10411122.120.0µg/L4-Chlorotoluene 70-130 6.0 20.0
22.4 11211923.820.0µg/LDi-Isopropyl Ether (DIPE)70-130 6.0 20.0
21.3 10712024.020.0µg/L1,2-Dibromo-3-Chloropropane 70-130 11.9 20.0
23.6 11812224.320.0µg/LDibromomethane 70-130 2.9 20.0
21.9 11011422.820.0µg/L1,2-Dichlorobenzene 70-130 4.0 20.0
23.3 11711923.720.0µg/L1,3-Dichlorobenzene 70-130 1.7 20.0
20.7 10410821.620.0µg/L1,4-Dichlorobenzene 70-130 4.2 20.0
18.2 91.010521.020.0µg/LDichlorodifluoromethane 60-140 14.2 20.0
23.7 11912725.420.0µg/L1,1-Dichloroethane 70-130 6.9 20.0
21.6 10811823.620.0µg/L1,2-Dichloroethane 70-130 8.8 20.0
23.5 11812424.820.0µg/L1,1-Dichloroethene 70-130 5.3 20.0
22.1 11111623.120.0µg/Lcis-1,2-Dichloroethene 70-130 4.4 20.0
Page 4 of 19Date:10/13/2022 01:44 PM
Page 67 of 84
Quality Control Data
22-278-0022Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Ray's Quick Stop
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V24843QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V24842
LCS-V24842 LCSD-V24842Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
22.4 11212024.020.0µg/Ltrans-1,2-Dichloroethene 70-130 6.8 20.0
22.8 11411623.120.0µg/L1,2-Dichloropropane 70-130 1.3 20.0
21.1 10611322.620.0µg/L1,3-Dichloropropane 70-130 6.8 20.0
22.6 11311923.720.0µg/L2,2-Dichloropropane 70-130 4.7 20.0
600 120120601500µg/LEthanol 60-140 0.1 20.0
21.0 10511122.220.0µg/LEthylbenzene 70-130 5.5 20.0
46.9 11712248.840.0µg/LEthyl Tertiary Butyl Ether (ETBE)70-130 3.9 20.0
19.3 96.511523.020.0µg/L2-Hexanone 60-140 17.4 20.0
20.5 10310721.320.0µg/LIsopropylbenzene 70-130 3.8 20.0
21.0 10510721.420.0µg/L4-Isopropyl toluene 70-130 1.8 20.0
19.8 99.083.516.720.0µg/LMethyl Ethyl Ketone (MEK)60-140 16.9 20.0
20.8 10411122.120.0µg/LMethyl tert-butyl ether (MTBE)70-130 6.0 20.0
20.7 10411823.620.0µg/L4-Methyl-2-Pentanone 60-140 13.0 20.0
23.3 11711923.820.0µg/LMethylene Chloride 70-130 2.1 20.0
19.0 95.011122.220.0µg/LNaphthalene 70-130 15.5 20.0
19.8 99.010420.720.0µg/Ln-Propylbenzene 70-130 4.4 20.0
21.1 10611422.720.0µg/LStyrene 70-130 7.3 20.0
38.1 95.211445.740.0µg/Ltert-Butyl Alcohol (TBA)40-140 18.1 20.0
38.9 97.210441.540.0µg/Ltert-Butyl formate (TBF)40-140 6.4 20.0
14.1 70.512424.820.0µg/Ltert-Amyl Alcohol (TAA)40-140 55.0*20.0
43.7 10911746.940.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 7.0 20.0
23.8 11912525.020.0µg/L1,1,1,2-Tetrachloroethane 70-130 4.9 20.0
21.8 10912224.420.0µg/L1,1,2,2-Tetrachloroethane 70-130 11.2 20.0
23.9 12012224.420.0µg/LTetrachloroethene 70-130 2.0 20.0
21.6 10811723.420.0µg/LToluene 70-130 8.0 20.0
23.1 11612725.320.0µg/L1,2,3-Trichlorobenzene 70-130 9.0 20.0
Page 5 of 19* QC Fail Date:10/13/2022 01:44 PM
Page 68 of 84
Quality Control Data
22-278-0022Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Ray's Quick Stop
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V24843QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V24842
LCS-V24842 LCSD-V24842Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.8 10912424.820.0µg/L1,2,4-Trichlorobenzene 70-130 12.8 20.0
20.8 10411623.120.0µg/L1,1,2-Trichloroethane 70-130 10.4 20.0
24.8 124133*26.520.0µg/LTrichloroethene 70-130 6.6 20.0
23.3 11712424.720.0µg/LTrichlorofluoromethane 60-140 5.8 20.0
22.8 11412524.920.0µg/L1,2,3-Trichloropropane 70-130 8.8 20.0
20.7 10410621.120.0µg/L1,2,4-Trimethylbenzene 70-130 1.9 20.0
20.5 10310520.920.0µg/L1,3,5-Trimethylbenzene 70-130 1.9 20.0
22.0 11011422.720.0µg/LVinyl Acetate 60-140 3.1 20.0
21.9 11011623.220.0µg/LVinyl Chloride 60-140 5.7 20.0
20.7 10410921.820.0µg/Lo-Xylene 70-130 5.1 20.0
44.1 11011545.940.0µg/Lm,p-Xylene 70-130 4.0 20.0
14.6 73.078.515.720.0µg/L3,3-Dimethyl-1-butanol 70-130 7.2 20.0
1081094-Bromofluorobenzene (S)70-130
130129Dibromofluoromethane (S)70-130
1001031,2-Dichloroethane - d4 (S)70-130
99.298.8Toluene-d8 (S)70-130
Page 6 of 19* QC Fail Date:10/13/2022 01:44 PM
Page 69 of 84
Quality Control Data
22-278-0022Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Ray's Quick Stop
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V24860QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V24859
Associated Lab Samples: 89969
LRB-V24859 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/06/22 12:0210.01.80<1.80µg/LAcetone
10/06/22 12:020.5000.180<0.180µg/LBenzene
10/06/22 12:020.5000.210<0.210µg/LBromobenzene
10/06/22 12:021.000.420<0.420µg/LBromochloromethane
10/06/22 12:020.5000.160<0.160µg/LBromodichloromethane
10/06/22 12:025.001.50<1.50µg/LBromoform
10/06/22 12:021.000.280<0.280µg/LBromomethane
10/06/22 12:020.5000.180<0.180µg/Ln-Butylbenzene
10/06/22 12:020.5000.200<0.200µg/Lsec-Butyl benzene
10/06/22 12:022.000.920<0.920µg/Ltert-Butyl benzene
10/06/22 12:020.5000.180<0.180µg/LCarbon Tetrachloride
10/06/22 12:020.5000.190<0.190µg/LChlorobenzene
10/06/22 12:020.5000.190<0.190µg/LChlorodibromomethane
10/06/22 12:021.000.430<0.430µg/LChloroethane
10/06/22 12:020.5000.220<0.220µg/LChloroform
10/06/22 12:020.5000.220<0.220µg/LChloromethane
10/06/22 12:020.5000.200<0.200µg/L2-Chlorotoluene
10/06/22 12:020.5000.200<0.200µg/L4-Chlorotoluene
10/06/22 12:020.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
10/06/22 12:022.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
10/06/22 12:020.5000.200<0.200µg/L1,2-Dibromoethane
10/06/22 12:020.5000.230<0.230µg/LDibromomethane
10/06/22 12:020.5000.220<0.220µg/L1,2-Dichlorobenzene
10/06/22 12:020.5000.190<0.190µg/L1,3-Dichlorobenzene
10/06/22 12:020.5000.210<0.210µg/L1,4-Dichlorobenzene
10/06/22 12:025.001.20<1.20µg/LDichlorodifluoromethane
10/06/22 12:020.5000.240<0.240µg/L1,1-Dichloroethane
Page 7 of 19Date:10/13/2022 01:44 PM
Page 70 of 84
Quality Control Data
22-278-0022Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Ray's Quick Stop
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V24860QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V24859
Associated Lab Samples: 89969
LRB-V24859 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/06/22 12:020.5000.150<0.150µg/L1,2-Dichloroethane
10/06/22 12:020.5000.150<0.150µg/L1,1-Dichloroethene
10/06/22 12:020.5000.200<0.200µg/Lcis-1,2-Dichloroethene
10/06/22 12:020.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
10/06/22 12:020.5000.190<0.190µg/L1,2-Dichloropropane
10/06/22 12:020.5000.130<0.130µg/L1,3-Dichloropropane
10/06/22 12:022.000.210<0.210µg/L2,2-Dichloropropane
10/06/22 12:020.5000.200<0.200µg/L1,1-Dichloropropene
10/06/22 12:020.5000.210<0.210µg/Lcis-1,3-Dichloropropene
10/06/22 12:020.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
10/06/22 12:0220042.0<42.0µg/LEthanol
10/06/22 12:020.5000.170<0.170µg/LEthylbenzene
10/06/22 12:0210.00.059<0.059µg/LEthyl Tertiary Butyl Ether (ETBE)
10/06/22 12:023.000.350<0.350µg/LHexachlorobutadiene
10/06/22 12:021.000.380<0.380µg/L2-Hexanone
10/06/22 12:020.5000.180<0.180µg/LIsopropylbenzene
10/06/22 12:020.5000.089<0.089µg/L4-Isopropyl toluene
10/06/22 12:025.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
10/06/22 12:021.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
10/06/22 12:021.000.078<0.078µg/L4-Methyl-2-Pentanone
10/06/22 12:022.000.330<0.330µg/LMethylene Chloride
10/06/22 12:021.000.470<0.470µg/LNaphthalene
10/06/22 12:020.5000.190<0.190µg/Ln-Propylbenzene
10/06/22 12:020.5000.220<0.220µg/LStyrene
10/06/22 12:0210.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
10/06/22 12:0210.00.350<0.350µg/Ltert-Butyl formate (TBF)
10/06/22 12:0210.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
Page 8 of 19Date:10/13/2022 01:44 PM
Page 71 of 84
Quality Control Data
22-278-0022Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Ray's Quick Stop
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V24860QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V24859
Associated Lab Samples: 89969
LRB-V24859 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/06/22 12:0210.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
10/06/22 12:020.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
10/06/22 12:020.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
10/06/22 12:020.5000.220<0.220µg/LTetrachloroethene
10/06/22 12:020.5000.220<0.220µg/LToluene
10/06/22 12:020.5000.380<0.380µg/L1,2,3-Trichlorobenzene
10/06/22 12:020.5000.310<0.310µg/L1,2,4-Trichlorobenzene
10/06/22 12:020.5000.160<0.160µg/L1,1,1-Trichloroethane
10/06/22 12:020.5000.096<0.096µg/L1,1,2-Trichloroethane
10/06/22 12:020.5000.180<0.180µg/LTrichloroethene
10/06/22 12:020.5000.180<0.180µg/LTrichlorofluoromethane
10/06/22 12:020.5000.270<0.270µg/L1,2,3-Trichloropropane
10/06/22 12:020.5000.190<0.190µg/L1,2,4-Trimethylbenzene
10/06/22 12:020.5000.180<0.180µg/L1,3,5-Trimethylbenzene
10/06/22 12:025.001.00<1.00µg/LVinyl Acetate
10/06/22 12:020.5000.170<0.170µg/LVinyl Chloride
10/06/22 12:020.5000.210<0.210µg/Lo-Xylene
10/06/22 12:021.000.420<0.420µg/Lm,p-Xylene
10/06/22 12:0210.01.00<1.00µg/L3,3-Dimethyl-1-butanol
10/06/22 12:024-Bromofluorobenzene (S)91.4 70-130
10/06/22 12:02Dibromofluoromethane (S)95.8 70-130
10/06/22 12:021,2-Dichloroethane - d4 (S)87.6 70-130
10/06/22 12:02Toluene-d8 (S)76.4 70-130
Page 9 of 19Date:10/13/2022 01:44 PM
Page 72 of 84
Quality Control Data
22-278-0022Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Ray's Quick Stop
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V24860QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V24859
LCS-V24859 LCSD-V24859Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
45.7 11411947.440.0µg/LAcetone 40-160 3.6 20.0
27.7 139*145*28.920.0µg/LBenzene 70-130 4.2 20.0
17.1 85.587.017.420.0µg/LBromobenzene 70-130 1.7 20.0
27.5 138*139*27.720.0µg/LBromochloromethane 70-130 0.7 20.0
25.3 12713025.920.0µg/LBromodichloromethane 70-130 2.3 20.0
20.5 10310520.920.0µg/LBromoform 70-130 1.9 20.0
24.8 12412725.420.0µg/LBromomethane 60-140 2.3 20.0
17.9 89.590.018.020.0µg/Ln-Butylbenzene 70-130 0.5 20.0
17.4 87.089.017.820.0µg/Lsec-Butyl benzene 70-130 2.2 20.0
17.5 87.588.517.720.0µg/Ltert-Butyl benzene 70-130 1.1 20.0
26.3 132*139*27.720.0µg/LCarbon Tetrachloride 70-130 5.1 20.0
20.6 10310520.920.0µg/LChlorobenzene 70-130 1.4 20.0
19.8 99.010320.620.0µg/LChlorodibromomethane 70-130 3.9 20.0
24.1 12112925.720.0µg/LChloroethane 60-140 6.4 20.0
26.6 133*137*27.420.0µg/LChloroform 70-130 2.9 20.0
20.1 10110120.220.0µg/LChloromethane 60-140 0.4 20.0
17.9 89.590.518.120.0µg/L2-Chlorotoluene 70-130 1.1 20.0
17.4 87.088.017.620.0µg/L4-Chlorotoluene 70-130 1.1 20.0
25.6 128131*26.120.0µg/LDi-Isopropyl Ether (DIPE)70-130 1.9 20.0
18.6 93.090.518.120.0µg/L1,2-Dibromo-3-Chloropropane 70-130 2.7 20.0
20.7 10410521.020.0µg/L1,2-Dibromoethane 70-130 1.4 20.0
28.3 142*149*29.720.0µg/LDibromomethane 70-130 4.8 20.0
18.7 93.594.518.920.0µg/L1,2-Dichlorobenzene 70-130 1.0 20.0
18.6 93.094.018.820.0µg/L1,3-Dichlorobenzene 70-130 1.0 20.0
18.4 92.093.018.620.0µg/L1,4-Dichlorobenzene 70-130 1.0 20.0
24.7 12412625.120.0µg/LDichlorodifluoromethane 60-140 1.6 20.0
Page 10 of 19* QC Fail Date:10/13/2022 01:44 PM
Page 73 of 84
Quality Control Data
22-278-0022Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Ray's Quick Stop
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V24860QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V24859
LCS-V24859 LCSD-V24859Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
26.0 130137*27.420.0µg/L1,1-Dichloroethane 70-130 5.2 20.0
26.4 132*136*27.120.0µg/L1,2-Dichloroethane 70-130 2.6 20.0
24.5 12312725.320.0µg/L1,1-Dichloroethene 70-130 3.2 20.0
25.4 127134*26.820.0µg/Lcis-1,2-Dichloroethene 70-130 5.3 20.0
25.4 127133*26.520.0µg/Ltrans-1,2-Dichloroethene 70-130 4.2 20.0
27.2 136*142*28.420.0µg/L1,2-Dichloropropane 70-130 4.3 20.0
20.0 10010320.620.0µg/L1,3-Dichloropropane 70-130 2.9 20.0
26.0 130136*27.220.0µg/L2,2-Dichloropropane 70-130 4.5 20.0
27.4 137*146*29.120.0µg/L1,1-Dichloropropene 70-130 6.0 20.0
26.6 133*139*27.720.0µg/Lcis-1,3-Dichloropropene 70-130 4.0 20.0
26.6 133*139*27.720.0µg/Ltrans-1,3-Dichloropropene 70-130 4.0 20.0
456 91.292.2461500µg/LEthanol 60-140 1.0 20.0
20.4 10210521.020.0µg/LEthylbenzene 70-130 2.8 20.0
55.9 140*133*53.140.0µg/LEthyl Tertiary Butyl Ether (ETBE)70-130 5.1 20.0
19.5 97.597.019.420.0µg/LHexachlorobutadiene 70-130 0.5 20.0
15.9 79.583.016.620.0µg/L2-Hexanone 60-140 4.3 20.0
17.8 89.089.017.820.0µg/LIsopropylbenzene 70-130 0.0 20.0
18.2 91.092.018.420.0µg/L4-Isopropyl toluene 70-130 1.0 20.0
26.3 132141*28.120.0µg/LMethyl Ethyl Ketone (MEK)60-140 6.6 20.0
26.1 131*137*27.320.0µg/LMethyl tert-butyl ether (MTBE)70-130 4.4 20.0
23.4 11712524.920.0µg/L4-Methyl-2-Pentanone 60-140 6.2 20.0
25.1 126131*26.120.0µg/LMethylene Chloride 70-130 3.9 20.0
17.2 86.084.516.920.0µg/LNaphthalene 70-130 1.7 20.0
17.7 88.589.517.920.0µg/Ln-Propylbenzene 70-130 1.1 20.0
20.2 10110320.520.0µg/LStyrene 70-130 1.4 20.0
41.6 10410341.140.0µg/Ltert-Butyl Alcohol (TBA)40-140 1.2 20.0
Page 11 of 19* QC Fail Date:10/13/2022 01:44 PM
Page 74 of 84
Quality Control Data
22-278-0022Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Ray's Quick Stop
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V24860QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V24859
LCS-V24859 LCSD-V24859Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
50.9 12713353.040.0µg/Ltert-Butyl formate (TBF)40-140 4.0 20.0
24.6 12313226.320.0µg/Ltert-Amyl Alcohol (TAA)40-140 6.6 20.0
54.7 137143*57.340.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 4.6 20.0
20.8 10410621.220.0µg/L1,1,1,2-Tetrachloroethane 70-130 1.9 20.0
17.3 86.588.017.620.0µg/L1,1,2,2-Tetrachloroethane 70-130 1.7 20.0
20.7 10410520.920.0µg/LTetrachloroethene 70-130 0.9 20.0
27.7 139*145*28.920.0µg/LToluene 70-130 4.2 20.0
19.8 99.010120.120.0µg/L1,2,3-Trichlorobenzene 70-130 1.5 20.0
18.9 94.595.019.020.0µg/L1,2,4-Trichlorobenzene 70-130 0.5 20.0
25.9 130138*27.620.0µg/L1,1,1-Trichloroethane 70-130 6.3 20.0
27.5 138*142*28.320.0µg/L1,1,2-Trichloroethane 70-130 2.8 20.0
26.7 134*138*27.520.0µg/LTrichloroethene 70-130 2.9 20.0
25.7 12913226.420.0µg/LTrichlorofluoromethane 60-140 2.6 20.0
16.9 84.588.017.620.0µg/L1,2,3-Trichloropropane 70-130 4.0 20.0
17.6 88.089.017.820.0µg/L1,2,4-Trimethylbenzene 70-130 1.1 20.0
17.7 88.590.018.020.0µg/L1,3,5-Trimethylbenzene 70-130 1.6 20.0
30.5 153*154*30.820.0µg/LVinyl Acetate 60-140 0.9 20.0
24.8 12412925.720.0µg/LVinyl Chloride 60-140 3.5 20.0
20.1 10110320.520.0µg/Lo-Xylene 70-130 1.9 20.0
43.3 10811044.140.0µg/Lm,p-Xylene 70-130 1.8 20.0
22.9 11511021.920.0µg/L3,3-Dimethyl-1-butanol 70-130 4.4 20.0
92.091.64-Bromofluorobenzene (S)70-130
95.698.2Dibromofluoromethane (S)70-130
87.089.61,2-Dichloroethane - d4 (S)70-130
77.477.6Toluene-d8 (S)70-130
Page 12 of 19* QC Fail Date:10/13/2022 01:44 PM
Page 75 of 84
Quality Control Data
22-278-0022Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Ray's Quick Stop
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V24973QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V24970
Associated Lab Samples: 89961
LRB-V24970 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/10/22 13:1510.01.80<1.80µg/LAcetone
10/10/22 13:150.5000.180<0.180µg/LBenzene
10/10/22 13:150.5000.210<0.210µg/LBromobenzene
10/10/22 13:151.000.420<0.420µg/LBromochloromethane
10/10/22 13:150.5000.160<0.160µg/LBromodichloromethane
10/10/22 13:155.001.50<1.50µg/LBromoform
10/10/22 13:151.000.280<0.280µg/LBromomethane
10/10/22 13:150.5000.180<0.180µg/Ln-Butylbenzene
10/10/22 13:150.5000.200<0.200µg/Lsec-Butyl benzene
10/10/22 13:152.000.920<0.920µg/Ltert-Butyl benzene
10/10/22 13:150.5000.180<0.180µg/LCarbon Tetrachloride
10/10/22 13:150.5000.190<0.190µg/LChlorobenzene
10/10/22 13:150.5000.190<0.190µg/LChlorodibromomethane
10/10/22 13:151.000.430<0.430µg/LChloroethane
10/10/22 13:150.5000.220<0.220µg/LChloroform
10/10/22 13:150.5000.220<0.220µg/LChloromethane
10/10/22 13:150.5000.200<0.200µg/L2-Chlorotoluene
10/10/22 13:150.5000.200<0.200µg/L4-Chlorotoluene
10/10/22 13:150.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
10/10/22 13:152.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
10/10/22 13:150.5000.200<0.200µg/L1,2-Dibromoethane
10/10/22 13:150.5000.230<0.230µg/LDibromomethane
10/10/22 13:150.5000.220<0.220µg/L1,2-Dichlorobenzene
10/10/22 13:150.5000.190<0.190µg/L1,3-Dichlorobenzene
10/10/22 13:150.5000.210<0.210µg/L1,4-Dichlorobenzene
10/10/22 13:155.001.20<1.20µg/LDichlorodifluoromethane
10/10/22 13:150.5000.240<0.240µg/L1,1-Dichloroethane
Page 13 of 19Date:10/13/2022 01:44 PM
Page 76 of 84
Quality Control Data
22-278-0022Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Ray's Quick Stop
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V24973QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V24970
Associated Lab Samples: 89961
LRB-V24970 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/10/22 13:150.5000.150<0.150µg/L1,2-Dichloroethane
10/10/22 13:150.5000.150<0.150µg/L1,1-Dichloroethene
10/10/22 13:150.5000.200<0.200µg/Lcis-1,2-Dichloroethene
10/10/22 13:150.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
10/10/22 13:150.5000.190<0.190µg/L1,2-Dichloropropane
10/10/22 13:150.5000.130<0.130µg/L1,3-Dichloropropane
10/10/22 13:152.000.210<0.210µg/L2,2-Dichloropropane
10/10/22 13:150.5000.200<0.200µg/L1,1-Dichloropropene
10/10/22 13:150.5000.210<0.210µg/Lcis-1,3-Dichloropropene
10/10/22 13:150.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
10/10/22 13:1520042.0<42.0µg/LEthanol
10/10/22 13:150.5000.170<0.170µg/LEthylbenzene
10/10/22 13:1510.00.059<0.059µg/LEthyl Tertiary Butyl Ether (ETBE)
10/10/22 13:153.000.350<0.350µg/LHexachlorobutadiene
10/10/22 13:151.000.380<0.380µg/L2-Hexanone
10/10/22 13:150.5000.180<0.180µg/LIsopropylbenzene
10/10/22 13:150.5000.089<0.089µg/L4-Isopropyl toluene
10/10/22 13:155.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
10/10/22 13:151.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
10/10/22 13:151.000.078<0.078µg/L4-Methyl-2-Pentanone
10/10/22 13:152.000.330<0.330µg/LMethylene Chloride
10/10/22 13:151.000.470<0.470µg/LNaphthalene
10/10/22 13:150.5000.190<0.190µg/Ln-Propylbenzene
10/10/22 13:150.5000.220<0.220µg/LStyrene
10/10/22 13:1510.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
10/10/22 13:1510.00.350<0.350µg/Ltert-Butyl formate (TBF)
10/10/22 13:1510.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
Page 14 of 19Date:10/13/2022 01:44 PM
Page 77 of 84
Quality Control Data
22-278-0022Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Ray's Quick Stop
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V24973QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V24970
Associated Lab Samples: 89961
LRB-V24970 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/10/22 13:1510.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
10/10/22 13:150.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
10/10/22 13:150.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
10/10/22 13:150.5000.220<0.220µg/LTetrachloroethene
10/10/22 13:150.5000.220<0.220µg/LToluene
10/10/22 13:150.5000.380<0.380µg/L1,2,3-Trichlorobenzene
10/10/22 13:150.5000.310<0.310µg/L1,2,4-Trichlorobenzene
10/10/22 13:150.5000.160<0.160µg/L1,1,1-Trichloroethane
10/10/22 13:150.5000.096<0.096µg/L1,1,2-Trichloroethane
10/10/22 13:150.5000.180<0.180µg/LTrichloroethene
10/10/22 13:150.5000.180<0.180µg/LTrichlorofluoromethane
10/10/22 13:150.5000.270<0.270µg/L1,2,3-Trichloropropane
10/10/22 13:150.5000.190<0.190µg/L1,2,4-Trimethylbenzene
10/10/22 13:150.5000.180<0.180µg/L1,3,5-Trimethylbenzene
10/10/22 13:155.001.00<1.00µg/LVinyl Acetate
10/10/22 13:150.5000.170<0.170µg/LVinyl Chloride
10/10/22 13:150.5000.210<0.210µg/Lo-Xylene
10/10/22 13:151.000.420<0.420µg/Lm,p-Xylene
10/10/22 13:1510.01.00<1.00µg/L3,3-Dimethyl-1-butanol
10/10/22 13:154-Bromofluorobenzene (S)99.0 70-130
10/10/22 13:15Dibromofluoromethane (S)95.0 70-130
10/10/22 13:151,2-Dichloroethane - d4 (S)92.8 70-130
10/10/22 13:15Toluene-d8 (S)96.0 70-130
Page 15 of 19Date:10/13/2022 01:44 PM
Page 78 of 84
Quality Control Data
22-278-0022Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Ray's Quick Stop
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V24973QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V24970
LCS-V24970 LCSD-V24970Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
40.7 10210140.440.0µg/LAcetone 40-160 0.7 20.0
20.3 10210420.820.0µg/LBenzene 70-130 2.4 20.0
19.2 96.094.018.820.0µg/LBromobenzene 70-130 2.1 20.0
20.7 10410721.320.0µg/LBromochloromethane 70-130 2.8 20.0
19.8 99.097.519.520.0µg/LBromodichloromethane 70-130 1.5 20.0
19.9 99.597.519.520.0µg/LBromoform 70-130 2.0 20.0
16.4 82.085.017.020.0µg/LBromomethane 60-140 3.5 20.0
19.3 96.598.019.620.0µg/Ln-Butylbenzene 70-130 1.5 20.0
19.2 96.095.019.020.0µg/Lsec-Butyl benzene 70-130 1.0 20.0
19.0 95.096.019.220.0µg/Ltert-Butyl benzene 70-130 1.0 20.0
19.1 95.511723.320.0µg/LCarbon Tetrachloride 70-130 19.8 20.0
20.2 10110220.320.0µg/LChlorobenzene 70-130 0.4 20.0
20.7 10410320.520.0µg/LChlorodibromomethane 70-130 0.9 20.0
16.4 82.085.017.020.0µg/LChloroethane 60-140 3.5 20.0
20.2 10110621.220.0µg/LChloroform 70-130 4.8 20.0
15.1 75.578.015.620.0µg/LChloromethane 60-140 3.2 20.0
19.3 96.597.519.520.0µg/L2-Chlorotoluene 70-130 1.0 20.0
18.8 94.093.518.720.0µg/L4-Chlorotoluene 70-130 0.5 20.0
20.2 10110420.820.0µg/LDi-Isopropyl Ether (DIPE)70-130 2.9 20.0
17.7 88.583.016.620.0µg/L1,2-Dibromo-3-Chloropropane 70-130 6.4 20.0
21.5 10810721.320.0µg/L1,2-Dibromoethane 70-130 0.9 20.0
20.8 10410420.820.0µg/LDibromomethane 70-130 0.0 20.0
19.7 98.510020.020.0µg/L1,2-Dichlorobenzene 70-130 1.5 20.0
20.8 10410420.720.0µg/L1,3-Dichlorobenzene 70-130 0.4 20.0
20.1 10110320.520.0µg/L1,4-Dichlorobenzene 70-130 1.9 20.0
17.1 85.590.518.120.0µg/LDichlorodifluoromethane 60-140 5.6 20.0
Page 16 of 19Date:10/13/2022 01:44 PM
Page 79 of 84
Quality Control Data
22-278-0022Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Ray's Quick Stop
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V24973QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V24970
LCS-V24970 LCSD-V24970Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.8 10410420.720.0µg/L1,1-Dichloroethane 70-130 0.4 20.0
18.5 92.594.018.820.0µg/L1,2-Dichloroethane 70-130 1.6 20.0
18.8 94.098.019.620.0µg/L1,1-Dichloroethene 70-130 4.1 20.0
19.8 99.010020.020.0µg/Lcis-1,2-Dichloroethene 70-130 1.0 20.0
20.0 10010320.620.0µg/Ltrans-1,2-Dichloroethene 70-130 2.9 20.0
20.1 10110420.820.0µg/L1,2-Dichloropropane 70-130 3.4 20.0
20.9 10510120.120.0µg/L1,3-Dichloropropane 70-130 3.9 20.0
19.4 97.096.019.220.0µg/L2,2-Dichloropropane 70-130 1.0 20.0
21.5 10811222.320.0µg/L1,1-Dichloropropene 70-130 3.6 20.0
20.7 10410621.120.0µg/Lcis-1,3-Dichloropropene 70-130 1.9 20.0
20.7 10410621.120.0µg/Ltrans-1,3-Dichloropropene 70-130 1.9 20.0
489 97.896.8484500µg/LEthanol 60-140 1.0 20.0
19.0 95.095.019.020.0µg/LEthylbenzene 70-130 0.0 20.0
43.1 10810943.540.0µg/LEthyl Tertiary Butyl Ether (ETBE)70-130 0.9 20.0
19.5 97.596.019.220.0µg/LHexachlorobutadiene 70-130 1.5 20.0
18.4 92.093.018.620.0µg/L2-Hexanone 60-140 1.0 20.0
19.6 98.098.519.720.0µg/LIsopropylbenzene 70-130 0.5 20.0
20.1 10198.519.720.0µg/L4-Isopropyl toluene 70-130 2.0 20.0
19.3 96.596.519.320.0µg/LMethyl Ethyl Ketone (MEK)60-140 0.0 20.0
20.5 10310220.320.0µg/LMethyl tert-butyl ether (MTBE)70-130 0.9 20.0
19.9 99.597.019.420.0µg/L4-Methyl-2-Pentanone 60-140 2.5 20.0
19.4 97.010120.120.0µg/LMethylene Chloride 70-130 3.5 20.0
18.1 90.587.017.420.0µg/LNaphthalene 70-130 3.9 20.0
18.8 94.094.518.920.0µg/Ln-Propylbenzene 70-130 0.5 20.0
19.7 98.510220.320.0µg/LStyrene 70-130 3.0 20.0
29.0 72.573.229.340.0µg/Ltert-Butyl Alcohol (TBA)40-140 1.0 20.0
Page 17 of 19Date:10/13/2022 01:44 PM
Page 80 of 84
Quality Control Data
22-278-0022Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Ray's Quick Stop
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V24973QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V24970
LCS-V24970 LCSD-V24970Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
43.4 10910441.640.0µg/Ltert-Butyl formate (TBF)40-140 4.2 20.0
22.5 11310220.320.0µg/Ltert-Amyl Alcohol (TAA)40-140 10.2 20.0
41.9 10510541.840.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 0.2 20.0
19.1 95.599.019.820.0µg/L1,1,1,2-Tetrachloroethane 70-130 3.5 20.0
20.1 10196.019.220.0µg/L1,1,2,2-Tetrachloroethane 70-130 4.5 20.0
19.8 99.010220.420.0µg/LTetrachloroethene 70-130 2.9 20.0
19.6 98.010220.420.0µg/LToluene 70-130 4.0 20.0
19.5 97.597.519.520.0µg/L1,2,3-Trichlorobenzene 70-130 0.0 20.0
19.7 98.597.519.520.0µg/L1,2,4-Trichlorobenzene 70-130 1.0 20.0
19.7 98.510120.220.0µg/L1,1,1-Trichloroethane 70-130 2.5 20.0
21.4 10710921.720.0µg/L1,1,2-Trichloroethane 70-130 1.3 20.0
20.4 10210621.120.0µg/LTrichloroethene 70-130 3.3 20.0
17.5 87.594.518.920.0µg/LTrichlorofluoromethane 60-140 7.6 20.0
19.2 96.094.518.920.0µg/L1,2,3-Trichloropropane 70-130 1.5 20.0
19.1 95.595.019.020.0µg/L1,2,4-Trimethylbenzene 70-130 0.5 20.0
19.5 97.597.019.420.0µg/L1,3,5-Trimethylbenzene 70-130 0.5 20.0
22.0 11010821.620.0µg/LVinyl Acetate 60-140 1.8 20.0
18.2 91.096.519.320.0µg/LVinyl Chloride 60-140 5.8 20.0
18.8 94.096.019.220.0µg/Lo-Xylene 70-130 2.1 20.0
39.7 99.210040.040.0µg/Lm,p-Xylene 70-130 0.7 20.0
25.7 12911923.720.0µg/L3,3-Dimethyl-1-butanol 70-130 8.0 20.0
99.897.84-Bromofluorobenzene (S)70-130
98.0100Dibromofluoromethane (S)70-130
93.693.61,2-Dichloroethane - d4 (S)70-130
96.696.2Toluene-d8 (S)70-130
Page 18 of 19Date:10/13/2022 01:44 PM
Page 81 of 84
Quality Control Data
22-278-0022Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Ray's Quick Stop
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V24828QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V24827
Associated Lab Samples: 89961, 89962, 89963, 89964, 89965, 89966, 89967, 89968, 89969
LRB-V24827 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/06/22 13:2450.011.5<11.5µg/LAliphatic C5-C8
10/06/22 13:2450.025.8<25.8µg/LAliphatic C9-C12
10/06/22 13:2450.04.02<4.02µg/LAromatic C9-C10
10/06/22 13:242,5-Dibromotoluene (FID) (S)91.1 70-130
10/06/22 13:242,5-Dibromotoluene (PID) (S)84.7 70-130
LCS-V24827 LCSD-V24827Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
313 104102305300µg/LAliphatic C5-C8 70-130 2.5 50.0
361 120119356300µg/LAliphatic C9-C12 70-130 1.3 50.0
119 119119119100µg/LAromatic C9-C10 70-130 0.0 50.0
94.888.92,5-Dibromotoluene (FID) (S)70-130
85.585.52,5-Dibromotoluene (PID) (S)70-130
Page 19 of 19Date:10/13/2022 01:44 PM
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Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-278-0022
Paragon Environmental Consultants, Inc.
01156
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 0.2C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)?Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:10/05/2022 15:37:30
Special precautions or instructions included?
Comments:
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