Loading...
HomeMy WebLinkAbout24007_Wrights Exective Sales II_Import Soil Rpt_20220825REPORT OF IMPORT SOIL SAMPLING ASSESSMENT REVISION NUMBER: 0.0 WRIGHT'S EXECUTIVE SALES II 721 AND 723 RIGSBEE AVENUE; 620 AND 616 FOSTER STREET; AND 0.06 ACRE UNNAMED ALLEY (PIN 0822-20-41-6111) DURHAM, DURHAM COUNTY, NORTH CAROLINA BROWNFIELDS PROJECT ID. 24007-20-032 ECS PROJECT NO. 49:10039-B PREPARED FOR GEERHOUSE OWNER, LLC August 25, 2022 Report Certification I, Scott M. Werley, P.G., a Licensed Geologist for ECS Southeast, LLP (NC Registered Geologist Firm C-SS3), do certify that the information contained herein is correct and accurate to the best of my knowledge. O s N SSA } n 2354 'LOG. Scott M. Werler, P.G. NC License No. 2354 SILcZ2 ECS SOUTHEAST, LLP "Setting the Standard for Service" Geotechnical • Construction Materials • Environmental • Facilities RC Registered Engineering Firm F NC Registered Geologists Firm C-553-553 SC Registered Engineering Firm 3239 Ms. Holly Samaha-Smith August 25, 2022 North Carolina Department of Environmental Quality Division of Waste Management Brownfields Program 1646 Mail Service Center Raleigh, North Carolina 27699-1646 Reference: Report of Import Soil Sampling Assessment Wright's Executive Sales 721 and 723 Rigsbee Avenue; 620 and 616 Foster Street; and 0.06 Acre Unnamed Alley (PIN 0822-90-41-6111) Durham, Durham County, North Carolina Brownfields Project No. 24007-20-032 ECS Project No. 49:10039-B Dear Ms. Samaha-Smith: ECS Southeast, LLP (ECS) is pleased to present the results of our Import Soil Sampling Assessment for the above -referenced site. ECS's services were provided in accordance with the Wright's Executive Sales Brownfields Import Soil Sampling Workplan Revision No. 2.0 dated May 27, 2022 and approved on June 7, 2022. This environmental assessment was performed at the request of the North Carolina Department of Environmental Quality (NCDEQ) Division of Waste Management (DWM) Brownfields Program (the Program). ECS appreciates the opportunity to work with the Program. If there are questions regarding this report, or a need for further information, please contact us. Respectfully submitted, ECS SOUTHEAST, LLP r Samantha M. Szakasits, G.I.T. Environmental Staff Project Manager sszakasits@ecslimited.com 919-616-2679 Scott M. WerleV, P.G. Principal Geologist swerlev@ecslimited.com �7�L•1�:iiQ'F �I: cc: Mr. John Sunter, Geerhouse Owner, LLC, 1805 71h Street NW Suite 800, Washington, D.C. 20001 ECS Capitol Services, PLLC • ECS Florida, LLC • ECS Mid -Atlantic, LLC • ECS Midwest, LLC • ECS Southeast, LLP • ECS Southwest, LLP www.ecslimited.com Report of Import Soil Sampling Assessment Wright's Executive Sales Brownfield Project No. 24007-20-032 ECS Project No. 49:10039-B TABLE OF CONTENTS 1.0 SITE BACKGROUND & PROJECT INFORMATION...............................................................1 2.0 SCOPE OF SERVICES..........................................................................................................1 3.0 LABORATORY ANALYTICAL RESULTS................................................................................4 4.0 QUALITY ASSURANCE/QUALITY CONTROL.......................................................................4 5.0 INVESTIGATION DERIVED WASTE.....................................................................................4 6.0 FINDINGS & CONCLUSIONS..............................................................................................5 7.0 QUALIFICATIONS OF REPORT...........................................................................................5 FIGURES Figure 1 Site Topographic Location Map Figure 2 Brownfield Parcel Location Map Figure 3 Borrow Source Site Location Map Figure 4 Previous Imported Fill Placement and Sample Location Map Figure 5 Borrow Source Sample Location Map TABLES Table 1 Summary of Import Soil Analytical Results — Borrow Source Area Table 2 Summary of Import Soil Analytical Results — Brownfields Receiving Site APPENDICES Appendix A Photo Documentation Log Appendix B Soil Boring Logs Appendix C Laboratory Analytical Data and Chain of Custody (COC) Records Report of Import Soil Sampling Assessment Wright's Executive Sales Brownfield Project No. 24007-20-032 ECS Project No. 49:10039-B 1.0 SITE BACKGROUND & PROJECT INFORMATION The subject brownfields site (Brownfields Project Number 24007-20-032), known as Wright's Executive Sales II, currently consists of two parcels and a total of 2.371 acres of land (see Figures 1 and 2). It is in a commercial area of Durham just to the south of W. Geer St. and west of Foster St. The Subject Site was occupied by three buildings associated with Acme Plumbing and Heating offices and storage, a stand- alone yoga studio, Motorco Music Hall, and The Mothership, which was a creative space to share, make, and collaborate on artistic projects. The Subject Site is currently identified by the Durham County Online GIS Database with the following Parcel Identification Numbers (PINS) and street addresses: • 620 Foster St. 0822-90-31-8262; 1.91 acres • 616 Foster St. 0821-99-29-7413; 0.461 acres The property is currently planned to be redeveloped with a mixed multi -family residential, commercial/retail, and/or restaurant complex. In order to accomplish redevelopment, it has been estimated that the brownfields site will require an estimated additional 1,200 cubic yards of imported fill material, with an estimated 1,400 cubic yards of imported fill material already imported and placed onsite and utilized as utility trench/corridor backfill. Correspondence with the North Carolina Department of Environmental Quality (NCDEQ) Brownfields Program (the Program) on April 13, 2022 has indicated that a total of three (3) representative composite soil characterization samples would be required to be collected from the borrow source to support the additional import of an estimated 1,200 cubic yards. This approach would satisfy the April 19, 2021 Program approved Environmental Management Plan (EMP) required sampling frequency of one representative composite sample per every approximate 500 cubic yards. Further, four (4) representative composite soil characterization samples were requested to be collected from the four sections of utility trenches/corridors where an approximate 1,400 cubic yards of imported soil has already been placed prior to Program approval. The soil samples were to be collected as 5-point representative composite samples. Additionally, further Program correspondence on May 13, 2022, requested five (5) background soil samples to be collected on the subject site and analyzed for pesticides and herbicides in an effort to determine if the risk has increased due to the already imported soils to the subject property. The background pesticide/herbicide soil samples were to be collected as grab samples in accordance with Section B.4 of the NCDEQ, Inactive Hazardous Sites Program Guidelines for Assessment and Cleanup (July 2021). The above described scope of work has been performed in accordance with the workplan approved on June 7, 2022, in an effort to satisfy the import soil assessment activities to be performed as required by the April 19, 2021 Program approved EMP. The data obtained from executing this import soil assessment is intended for regulatory use by the Brownfields Program only. 2.0 SCOPE OF SERVICES The objective of this assessment is to maintain the liability protections offered by the Program by characterizing the soil quality being imported to the site. The borrow source property is an approximate 1-acre property located at 7315 Lebanon Road in Mebane, North Carolina as illustrated on Figure 3, and 1 Report of Import Soil Sampling Assessment Wright's Executive Sales Brownfield Project No. 24007-20-032 ECS Project No. 49:10039-B the approximate location of the imported soils already placed on the brownfields site has been illustrated on Figure 4. The borrow source property is reportedly undergoing residential redevelopment. A review of historical aerial photography on Google Earth indicates that the borrow source property was used for agricultural purposes from at least December 1985 through April 1998. By October 2005 the property appears to be undeveloped wooded land, and it maintains this land use through at least April 2021. Land use prior to 1985 is unknown; however, is likely to have been undeveloped wooded land and/or used for agricultural purposes. No additional information on prior land use history of the borrow source was able to be obtained for inclusion in this assessment. Import soil assessment activities were conducted by ECS and initiated on June 14, 2022 and consisted of the collection and laboratory analysis of eleven (11) soil samples. Three (3) representative composite soil samples from the area of the borrow source where additional soil is slated to be sourced for import to the site, three (3) representative composite soil samples from the utility trenches/corridors where imported soil has already been placed, and five (5) background soil grab samples from the subject brownfields property. A photographic log documenting the field sampling activities is provided in Appendix A. 2.1 Soil Assessment Activities On June 14, 2022, ECS mobilized to the borrow source property to collect three (3) representative composite soil samples (SP-1 through SP-3) from the soils currently stockpiled. The stockpile was flagged off in approximate 500 cubic yard cells, and subsequently one 5-point representative composite soil sample was collected from each cell. The approximate location of the stockpile and sample locations are illustrated on Figure 5. On June 17, 2022 and June 20, 2022, ECS mobilized to the subject brownfields property to collect three (3) representative composite soil samples (UT-1, UT-3, and UT-4) from each of the three (3) areas of utility trenches/corridors where imported soil was previously placed at the site. ECS was unable to collect a sample from the northeastern -most utility trench/corridor identified as Area 2. According to Mr. John Hyzak of Clancy & Theys, the imported soil originally placed in Area 2 was relocated and redistributed between the utility trenches/corridors identified as Area 3 and Area 4. Five (5) background samples (BG- 1 through BG-5) were also collected at the subject site in an effort to determine if the risk has increased due the already imported soils to the subject property. The locations of the representative composite soil samples and background samples are illustrated on Figure 4. On July 13, 2022, ECS remobilized to the borrow source property to resample and collected three (3) composite samples (SPR-1 through SPR-3) from the stockpiled soils. The stockpile remained flagged off in approximate 500 cubic yard cells, and subsequently one 5-point representative composite soil sample was collected from each cell. Soils samples for the characterization of soil already imported to the site were collected utilizing a stainless -steel hand auger, and soils collected from stockpiled soils on the borrow source property were collected utilizing a shovel. The hand auger and shovel were decontaminated upon arrival at each respective site, between each representative composite soil sample area, and prior to departure from the site. Decontamination was conducted with scrub bushes and a municipal water/Alconox mix, followed by a municipal water rinse. 2 Report of Import Soil Sampling Assessment Wright's Executive Sales Brownfield Project No. 24007-20-032 ECS Project No. 49:10039-B Field screening was conducted with a photoionization detector (PID) calibrated in the field on the day of assessment per manufacturer's guidelines. ECS personnel observed the soil from each boring and noted the color and texture of the soil. Additional field indicators such as soil staining and distinguishable odors were also noted if present during observation. See soil boring logs included in Appendix B. 2.2 Soil Sample Collection Soil samples were collected by ECS personnel wearing new disposable powder free nitrile gloves exchanged between each sample interval. The representative composite samples were comprised of five individual grab soil samples collected in duplicate re -sealable bags. One of the two duplicate aliquots was screened using a PID for volatile vapors and then considered to be ineligible for sampling. The individual grab soil sample with the highest PID reading, from the unopened re -sealable bag was appropriately packaged and submitted to Pace Analytical Services, LLC (Pace), a North Carolina certified laboratory (NC Certification No. 375), located in Huntersville, NC to be analyzed for volatile organic compounds (VOCs) using EPA Method 8260. Subsequently, it was then mixed with the other four aliquots and one representative composite soil sample was containerized and submitted for North Carolina certified laboratory analysis for semivolatile organic compounds (SVOCs) by EPA Method 8270, total metals regulated under the Resource Conservation and Recovery Act (RCRA metals) using EPA Method 6020/7471, hexavalent chromium (Cr VI) by EPA Method 7199, organochlorine pesticides by EPA Method 8081, organophosphorus pesticides by EPA Method 8141, and chlorinated herbicides by EPA Method 8151. The five background soil samples were collected into laboratory supplied/preserved containers and submitted for the above listed pesticide and herbicide analyses only. The three soil samples (SPR-1 through SPR-3) collected on July 13, 2022 were submitted to Pace to be analyzed for organophosphorus pesticides by EPA Method 8141 and chlorinated herbicides by EPA Method 8151 only to serve as replacements for the "out of hold" analyses for soil samples SP-1 through SP-3. Four duplicate soil samples (DUP-1, DUP-2, DUP-3, and DUP-4) were collected as duplicates of SP-2, UT-4, UT-3, and SPR-2, respectively. Each duplicate was submitted for the same soil analyses as listed above. ECS maintained chain of custody (COC) procedures throughout the sample collection and transportation process. A copy of the analytical laboratory reports along with accompanying COC documentation is included in Appendix C. 2.3 Deviation from Approved Work Plan A total of eleven (11) soil samples were collected as opposed to the twelve (12) soil samples originally proposed in the approved work plan. Three (3) representative composite soil samples were collected from the utility trenches/corridors, identified as Area 1, Area 3, and Area 4, where imported soil has already been placed. ECS was unable to collect a sample from the northeastern -most utility trench/corridor identified as Area 2. According to Mr. Hyzak of Clancy & Theys, the imported soil originally placed in Area 2 was relocated and redistributed between the utility trenches/corridors identified as Area 3 and Area 4 (Figure 4). Two additional duplicate samples (DUP-3 and DUP-4) were collected to support the two additional mobilizations to each respective site location determined necessary to complete the sampling activities. 3 Report of Import Soil Sampling Assessment Wright's Executive Sales Brownfield Project No. 24007-20-032 ECS Project No. 49:10039-B 3.0 LABORATORY ANALYTICAL RESULTS 3.1 Soil Analytical Results The soil samples collected at Mebane import source area on June 14, 2022 (SP-1 through SP-3) and the subject brownfields property on June 17, 2022 and June 20, 2022 (UT-1, UT-3, UT-4, and BG-1 through BG-5) were analyzed for VOCs, SVOCs, pesticides, herbicides, and RCRA metals including Cr VI, respectively. Laboratory analysis of soil samples collected from the import source (SP-1 through SP-3) and the subject brownfields property (UT-1, UT-3, UT-4, and BG-1 through BG-5) did not detect VOCs, SVOCs, pesticides, or herbicides above their respective Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs). Laboratory analysis of soil samples UT-1, UT-3, UT-4, and SP-1 through SP-3 detected barium, chromium (III), lead, and mercury at concentrations above their laboratory reporting limits but below their respective PSRGs. Cr VI was detected in soil samples SP-1 through SP-3 and UT-1 at an estimated concentration above the Residential Health Based PSRG, but below the Protection of Water and Industrial/Commercial Health Based PSRGs. Laboratory analysis of soil samples UT-1, UT-3, UT-4, and SP-1 through SP-3 detected arsenic at concentrations ranging from 0.72 mg/kg to 3.65 mg/kg, which are above the Residential Health Based PSRG and/or Industrial/Commercial Health Based PSRG, but below the Protection of Groundwater PSRG. Laboratory analytical results for import borrow source area are summarized on Table 1 and subject Brownfields receiving property results are summarized on Table 2. A copy of the analytical laboratory reports along with accompanying COC documentation is included in Appendix C. 4.0 QUALITY ASSURANCE/QUALITY CONTROL In accordance with the Brownfields approved work plan, sample duplicates were collected and submitted for soil to support QA/QC of this assessment. The duplicates, identified as DUP-1 through DUP-4, were submitted for the same media and laboratory analyses as the samples they duplicated. Following sample collection, the sample containers were labeled and maintained under COC until delivered to Pace Analytical Services, LLC in Raleigh, NC by local courier. A COC document was utilized throughout the collection and transportation of the samples. A level II QA/QC package was reported by the laboratory. Review of the duplicate sample data presented herein has not affected the interpretation of the assessment's results. 5.0 INVESTIGATION DERIVED WASTE The investigative derived waste (IDW) generated from this assessment was managed in accordance with the NCDEQ, Inactive Hazardous Sites Program Guidelines for Assessment and Cleanup (January202O). Soil IDW was placed back down its respective borehole at the same approximate depth it was recovered from or spread at the surface near each respective borehole from which it was derived. 21 Report of Import Soil Sampling Assessment Wright's Executive Sales Brownfield Project No. 24007-20-032 ECS Project No. 49:10039-B 6.0 FINDINGS & CONCLUSIONS Laboratory analysis of soil samples collected from the import borrow source and the subject Brownfields receiving property did not detect VOCs, SVOCs, pesticides, or herbicides above their respective PSRGs. Cr VI was detected in soil samples SP-1 through SP-3 and UT-1 at an estimated concentration above the Residential Health Based PSRG, but below the Protection of Water and Industrial/Commercial Health Based PSRGs. Laboratory analysis of all samples of the imported soil detected arsenic at concentrations above one or more of its respective PSRGs; however, according to Dragun and Chekiri's Elements in North American Soils, Second Edition, naturally occurring concentrations of arsenic range from 1.0 mg/kg to 18 mg/kg with a mean concentration of 2.07 mg/kg. It is the opinion of ECS that arsenic is a naturally occurring compound found in soils in this region. Laboratory analysis of soil samples UT-1, UT-3, UT-4, and SP-1 through SP-3 detected barium, chromium (III), lead, and mercury at concentrations above their laboratory reporting limits but below their respective PSRGs. Based on the laboratory results of the soil samples collected, ECS recommends submitted this report to the NC Brownfields project manager for approval of the import borrow source located at 7315 Lebanon Road in Mebane, North Carolina to be utilized at the Wrights Executive Sales Brownfields Property. ECS also recommends revising current EMP to include the most recent analytical results collected from the subject brownfields property. 7.0 QUALIFICATIONS OF REPORT The activities and evaluative approaches used in this environmental assessment are consistent with those normally employed in environmental assessment projects of this type. Our evaluation of site conditions has been based on our understanding of the site project information determined during previous environmental assessments and the data obtained during our field activities. This report was prepared for the express use of the North Carolina Brownfields Program. Use of this report by other individuals or companies implies their acceptance of the General Conditions of Service of the original contract. 5 FIGURES _ ' • �� J 1110� } Mir L 9 -, Mf 6qk p PM r WWppd%6 W.OrAo _ y f %L r2 APPROXIMATE BROWNFIELD•••• BOUNDARY NORTHWESTSOURCE: FIGURE 1 USGS TOPOGRAPHIC MAP SITE TOPOGRAPHIC LOCATION MAP •.Executive Sales 11 SOUTHWEST DURHAM, NC (BOTTOM) Brownfields Project Number 24007-20-032 .• . 1 .-Ave;1 & 616 Foster St. 111 Durham, Durham County,•Carolina CONTOUR INVERVAL = 1 • - .- 4911 • SOURCE: ECS Southeast, LLP Phase I ESA, December 6, 2019 APPROXIMATE SCALE: 100 FT. NL I I FIGURE 2 wF BROWNFIELD PARCEL LOCATION MAP s' Wright's Executive Sales II Brownfields Project Number 24007-20-032 721 & 723 Rigsbee Ave; 620 & 616 Foster St. Durham, Durham County, North Carolina TM ECS Project Number: 49-10039-B LEGEND APPROXIMATE AREA OF BORROW SOURCE LOCATED AT 7315 LEBANON ROAD, MEBANE, NORTH CAROLINA See Figure 5 �I SOURCE:" FIGURE 3 BORROW SOURCE SITE LOCATION M]St. Google Earth Aerial s Imagery Dated 2020 Wright's Executive Sales II Brownfields Project Number 24007-2 NOT TO SCALE 721 & 723 Rigsbee Ave; 620 & 616 FosDurham, Durham County, North Caro TM ECS Project Number: 49-10039-B } UT-1 (Area 1) 60'long x 5'wide x 6'deep -22CY URIC Wr --' AREA 2 • x I � BG-1 - d BG-3 r6 0 ti — � UT-3 (Area 3) �: 4501ong x 5'wide x 5'deep BG-4 4 ��• -450CY � BG-5 it * r Lb -�---- ni }_ — UT-4 (Area 4) - Ft 450'long x 10'wide x 5'deep f -890CY LEGEND SITE PROPERTY BOUNDARY IMPORTED SOIL ALREADY PLACED ONSITE WITHIN THE BROWNFIELDS PROPERTY BACKGROUND SAMPLES NOTES: 1.) Samples were composited from five grab sample locations depicted with an " " in each respective Area. SOURCE: " FIGURE 4 ECS Southeast, LLP -*F PREVIOUS IMPORTED FILL PLACEMENT AND Phase I ESA, December 6, 2019 S SAMPLE LOCATION MAP Report of Environmental Assessment Rev.0.0, Wright's Executive Sales II December 18, 2020 Brownfields Project Number 24007-20-032 721 & 723 Rigsbee Ave; 620 & 616 Foster St. APPROXIMATE SCALE: Durham, Durham County, North Carolina 50 FT. TM ECS Project Number: 49-10039-B 9r ■ " ■ iL ■ I 'r LEGEND APPROXIMATE AREA OF BORROW SOURCE LOCATED AT 7315 LEBANON ROAD, MEBANE, NORTH CAROLINA X APPROXIMATE SOIL SAMPLE LOCATION NOTES: ■ 1.) Samples were composited from five grab sample locations depicted with an " " in each respective cell. SOURCE: �"L - FIGURE 5 w F BORROW SOURCE SAMPLE LOCATION MAP Google Earth Aerial S Imagery Dated 2020 Wright's Executive Sales II Brownfields Project Number 24007-20-032 NOT TO SCALE 721 & 723 Rigsbee Ave; 620 & 616 Foster St. gE1Durham, Durham County, North Carolina TM r I ECS Project Number: 49-10039-B TABLES TABLE 1: SUMMARY OF IMPORT SOIL ANALYTICAL RESULTS - BORROW SOURCE AREA Wrights Executive Sales Brownfields Program Site No. 24007-20-032 721 and 723 Rigsbee Avenue; 620 and 616 Foster Street, Durham, Durham County, North Carolina ECS Project No. 49:10039-B Comparison Criteria Sample Identification SP-1 SPR-1 SP-2 SPR-2 SP-3 SPR-3 DUP-1 DUP-4 IHSB Protection of Groundwater PSRG IHSB Residential Health Based PSRG IHSB Industrial/Commercial Health Based PSRG Sample Date 6/14/2022 7/13/2022 6/14/2022 7/13/2022 6/14/2022 7/13/2022 6/14/2022 7/13/2022 Sample Depth (feet) 0-2 0-2 0-2 0-2 0-2 0-2 0-2 0-2 EPA Method 8260 (VOCs) 2-Butanone (MEK) 0.060J NA 0.0991 0.10J NA 0.071J NA 17 5,500 40,000 Styrene 0.0068J NA 0.011 0.012 0.0074J NA 1.5 1,200 7,300 EPA Method 8270 (SVOCs) No EPA Method 8270 Compounds Reported Above Laboratory Method Detection Limits EPA Method 8081 (GCS Pesticides) No EPA Method 8081 Compounds Reported Above Laboratory Method Detection Limits EPA Method 8141 (OP Pesticides) No EPA Method 8141 Compounds Reported Above Laboratory Method Detection Limits EPA Method 8151 (GC Herbicides) No EPA Method 8151 Compounds Reported Above Laboratory Method Detection Limits EPA Method 602013/747113 (RCRA 8-Metals) & EPA Method 7199 (Cr VI) Arsenic 2.65 3.65 NA 2.10 NA 2.28 NA 5.8 0.68 3.0 Barium 84.8 83.2 NA 78.9 NA 84.7 NA 580 3,100 47,000 Cadmium <0.12 NA <0.13 NA <0.12 NA <0.12 NA 3.0 1.4 20 Chromium (III) as Total 71.5 NiA 38.2 NA 29.6 NA 78.2 NA 360,000 23,000 350,000 Chromium (VI) 0.967J NA 1.21J NA 0.824.1 NA 1.04J NA 3.8 0.31 6.5 Lead 6.47 NA 7.45 NA 8.97 NA 7.56 NA 250 400 800 Selenium <0.12 NA <0.13 NA <0.12 NA <0.12 NA 2.1 78 1,200 Silver <0.12 NA <0.13 NA <0.12 NA <0.12 NA 3.4 78 1,200 Mercury 0.027 NA 0.013J NA 0.018 0.046 NA 1.0 2.3 9.7 Notes: mg/Kg = milligrams per kilogram = ppm (parts per million) <0.0088 = Less than the Method Detection Limit (MDL) as shown on the associated analytical report NS denotes no published standard Soil sample results are compared to the NCDEQ PSRGs dated July 2022 J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit IHSB = Inactive Hazardous Sites Branch PSRG = Preliminary Soil Remediation Goal NA = Not Analyzed Bold concentration on sample result indicates and exceedance of the Protection of Groundwater PSRG Underlined concentration on sample result indicates and exceedance of the Residential Health Based PSRG Italicized concentration on sample result indicates and exceedance of the Industrial/Commercial Health Based PSRG SP-1 through SP-3 were resampled and submitted for EPA Method 8141 and 8151 only on 7/13/2022 to replace "out of hold" samples collected 6/14/2022 DUP-1 is a duplicate of SP-2 collected on 6/14/2022 DUP-4 is a duplicate of resampled SP-2R collected on 7/13/2022 TABLE 2: SUMMARY OF IMPORT SOIL ANALYTICAL RESULTS - BROWNFIELDS RECEIVING SITE Wrights Executive Sales Brownfields Program Site No. 24007-20-032 721 and 723 Rigsbee Avenue; 620 and 616 Foster Street, Durham, Durham County, North Carolina ECS Project No. 49:10039-B Comparison Criteria Sample Identification UT-1 UT-4 DUP-2 UT-3 DUP-3 BG-1 BG-2 BG-3 BG-4 BG-5 IHSB Protection of Groundwater PSRG IHSB Residential Health Based PSRG IHSB Industrial/Commercial Health Based PSRG Sample Date 6/17/2022 6/17/2022 6/17/2022 6/20/2022 6/20/2022 6/17/2022 6/17/2022 6/17/2022 6/17/2022 6/17/2022 Sample Depth (feet) 0-5' 0-5' 0-5' 0-5' 0-5' 0-5' 0-5' 0-5' 0-5' 0-5' EPA Method 8260 (VOCs) 2-Butanone (MEK) 0.044J 0.040J 0.041J 0.046J 0.053J NA NA NA NA NA 17 5,500 40,000 Styrene <0.0019 <0.0016 <0.0015 <0.0018 <0.0018 NA NA NA NA NA 1.5 1,200 7,300 EPA Method 8270 (SVOCs) Fluoranthene <1.4 <0.13 <0.13 <0.13 0.27J NA NA NA NA NA 670 480 6,000 Phenanthrene <1.3 <0.12 <0.13 <0.13 0.22J NA NA NA NA NA INS NS NS Pyrene <1.7 <0.15 <0.16 <0.16 0.191 NA NA NA NA NA 440 360 4,500 EPA Method 8081 (GCS Pesticides) No EPA Method 8081 Compounds Reported Above Laboratory Method Detection Limits EPA Method 8141 (OP Pesticides) No EPA Method 8141 Compounds Reported Above Laboratory Method Detection Limits EPA Method 8151 (OP Herbicides) No EPA Method 8151 Compounds Reported Above Laboratory Method Detection Limits EPA Method 6020/7471 (RCRA 8-Metals) & EPA Method 7199 (Cr VI) Arsenic 0.72 1.37 1.84 1.97 2.05 NA NA NA NA NA 5.8 0.68 3.0 Barium 39.7 107 123 162 128 NA NA NA NA NA 580 3,100 47,000 Cadmium <0.12 <0.10 <0.10 <0.10 <0.091 NA NA NA NA NA 3.0 1.4 20 Chromium (III) as Total 11.2 24.7 28.3 41.1 32.4 NA NA NA NA NA 360,000 23,000 350,000 Chromium (VI) <0.32 <0.297 <0.281 <0.293 <0.285 NA NA NA NA NA 3.8 0.31 6.5 Lead 9.86 14.0 14.6 12.1 13.0 NA NA NA NA NA 250 400 800 Selenium <0.12 <0.10 <0.10 <0.10 <0.091 NA NA NA NA NA 2.1 78 1,200 Silver <0.12 <0.10 <0.10 <0.10 <0.091 NA NA NA NA NA 3.4 78 1,200 Mercury 0.025 0.047 0.019 0.039 0.030 NA NA NA NA NA 1.0 2.3 9.7 Notes: mg/Kg = milligrams per kilogram = ppm (parts per million) <0.0088 = Less than the Method Detection Limit (MDL) as shown on the associated analytical report INS denotes no published standard Soil sample results are compared to the NCDEQ PSRGs dated July 2022 J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit IHSB = Inactive Hazardous Sites Branch PSRG = Preliminary Soil Remediation Goal NA = Not Analyzed Bold conentration on sample result indicates and exceedance of the Protection of Groundwater PSRG Underlined conentration on sample result indicates and exceedance of the Residential Health Based PSRG Italicized concentration on sample result indicates and exceedance of the Industrial/Commercial Health Based PSRG DUP-2 is a dupilcate of UT-4 collected on 6/17/2022 DUP-3 is a dupilcate of UT-3 collected on 6/20/2022 APPENDIX A PHOTO DOCUMENTATION LOG - P s Photo 1— View of the current site conditions of the borrow source located at 7315 Lebanon Road, Mebane, NC. Photo 2 — View of the proposed import borrow source stockpile location. Wright's Executive Sales II Brownfields Project Number 24007-20-032 Photo Documentation 721 & 723 Rigsbee Ave; 620 & 616 Foster St. Durham, Durham County, North Carolina ECS Project Number: 49-10039-B i as :4'•" ,�, jr e Photo 5 — A mini -excavator was utilized to dig through the 1- to 1.5-foot-thick layer of gravel placed over the imported soil placed in Areas 3 and 4. Tl V Photo 6 — Typical view of the hand auger boring and sample collection activities performed at the subject site. Wright's Executive Sales II Photo Documentation rf! a Brownfields Project Number 24007-20-032 721 & 723 Rigsbee Ave; 620 & 616 Foster St. Durham, Durham County, North Carolina ECS Project Number: 49-10039-B �s. d Photo 7 — View of utility trench/corridor identified as Area 2 with no observable imported fill. F. 1 r - 14, ill 771 Nk i r Photo 8 — Additional view of the utility trench/corridor identified as Area 2. Photo Documentation Wright's Executive Sales II Brownfields Project Number 24007-20-032 721 & 723 Rigsbee Ave; 620 & 616 Foster St. Durham, Durham County, North Carolina ECS Project Number: 49-10039-B APPENDIX B SOIL BORING LOGS Project Name: Wright's Executive Sales Sheet: 1 of 1 Boring No: BG-1 Client: Geerhouse Partners, LLC Project No.: 10039-B 721 and 723 Rigsbee Avenue; 620 and 616 Site Location: Driller: Drill Rig: Hand Auger Foster Street, Raleigh, NC Latitude/Longitude: U0 c i m 16 E j J Depth/Elevation v Q Soil Classification Description Q E a, Q 12 a n E 0.0 BG-1 0.0 END OF DRILLING AT 2.0 FT 5 -5 10 -10 15 -15 20 -20 25 -25 30 SZ WL (First Encountered) Boring Started: Jun 17 2022 1 WL (Completion) Boring Completed: Jun 17 2022 Remarks: Logged By: Austin Deans, Emery Lovekamp Principal Engineer/ Scott M. Werley Responsible PG: Project Name: Wright's Executive Sales Sheet: 1 of 1 Boring No: BG-2 Client: Geerhouse Partners, LLC Project No.: 10039-B 721 and 723 Rigsbee Avenue; 620 and 616 Site Location: Driller: Drill Rig: Hand Auger Foster Street, Raleigh, NC Latitude/Longitude: U0 c i m 16 E j J Depth/Elevation v Q Soil Classification Description Q E a, Q 12 a n E 0.0 10.6 BG-2 60.5 20.2 END OF DRILLING AT 4.0 FT 5 -5 10 -10 15 -15 20 -20 25 -25 30 SZ WL (First Encountered) Boring Started: Jun 17 2022 1 WL (Completion) Boring Completed: Jun 17 2022 Remarks: Logged By: Austin Deans, Emery Lovekamp Principal Engineer/ Scott M. Werley Responsible PG: Project Name: Wright's Executive Sales Sheet: 1 of 1 Boring No: BG-3 Client: Geerhouse Partners, LLC Project No.: 10039-B 721 and 723 Rigsbee Avenue; 620 and 616 Site Location: Driller: Drill Rig: Hand Auger Foster Street, Raleigh, NC Latitude/Longitude: U0 c i m 16 E j J Depth/Elevation v Q Soil Classification Description Q E a, Q 12 a n E 1.6 3.0 BG-3 4.7 END OF DRILLING AT 3.0 FT 5 -5 10 -10 15 -15 20 -20 25 -25 30 SZ WL (First Encountered) Boring Started: Jun 17 2022 1 WL (Completion) Boring Completed: Jun 17 2022 Remarks: Logged By: Austin Deans, Emery Lovekamp Principal Engineer/ Scott M. Werley Responsible PG: Project Name: Wright's Executive Sales Sheet: 1 of 1 Boring No: BG-4 Client: Geerhouse Partners, LLC Project No.: 10039-B 721 and 723 Rigsbee Avenue; 620 and 616 Site Location: Driller: Drill Rig: Hand Auger Foster Street, Raleigh, NC Latitude/Longitude: U0 c i m 16 E j J Depth/Elevation v Q Soil Classification Description Q E a, Q 12 a n E 0.0 0.0 BG-4 0.0 0.0 END OF DRILLING AT 4.0 FT 5 -5 10 -10 15 -15 20 -20 25 -25 30 SZ WL (First Encountered) Boring Started: Jun 17 2022 1 WL (Completion) Boring Completed: Jun 17 2022 Remarks: Logged By: Austin Deans, Emery Lovekamp Principal Engineer/ Scott M. Werley Responsible PG: Project Name: Wright's Executive Sales Sheet: 1 of 1 Boring No: BG-5 Client: Geerhouse Partners, LLC Project No.: 10039-B 721 and 723 Rigsbee Avenue; 620 and 616 Site Location: Driller: Drill Rig: Hand Auger Foster Street, Raleigh, NC Latitude/Longitude: U0 c i m 16 E j J Depth/Elevation v Q Soil Classification Description Q E a, Q 12 a n E 0.0 0.0 0.0 BG-5 0.0 0.0 5 -5 END OF DRILLING AT 5.0 FT 10 -10 15 -15 20 -20 25 -25 30 SZ WL (First Encountered) Boring Started: Jun 17 2022 1 WL (Completion) Boring Completed: Jun 17 2022 Remarks: Logged By: Austin Deans, Emery Lovekamp Principal Engineer/ Scott M. Werley Responsible PG: Project Name: Wright's Executive Sales Sheet: 1 of 1 Boring No: UT-1 Client: Geerhouse Partners, LLC Project No.: 10039-B 721 and 723 Rigsbee Avenue; 620 and 616 Site Location: Driller: Drill Rig: Hand Auger Foster Street, Raleigh, NC Latitude/Longitude: c _� 16 E j J Depth/Elevation v Q Soil Classification Description Q E a, Q 12 a n E 4.3 2.1 UT-1 2.5 3.8 END OF DRILLING AT 4.0 FT 5 -5 10 -10 15 -15 20 -20 25 -25 30 SZ WL (First Encountered) Boring Started: Jun 17 2022 1 WL (Completion) Boring Completed: Jun 17 2022 Remarks: Logged By: Austin Deans, Emery Lovekamp Principal Engineer/ Scott M. Werley Responsible PG: Project Name: Wright's Executive Sales Sheet: 1 of 1 Boring No: UT-3A Client: Geerhouse Partners, LLC Project No.: 10039-B 721 and 723 Rigsbee Avenue; 620 and 616 Site Location: Driller: Drill Rig: Hand Auger Foster Street, Raleigh, NC Latitude/Longitude: c _� 16 E j J Depth/Elevation v Q Soil Classification Description Q E a, Q 12 a n E 0.0 0.0 UT-3A 0.0 0.0 END OF DRILLING AT 4.0 FT 5 -5 10 -10 15 -15 20 -20 25 -25 30 SZ WL (First Encountered) Boring Started: Jun 20 2022 1 WL (Completion) Boring Completed: Jun 20 2022 Remarks: Logged By: Austin Deans, Emery Lovekamp Principal Engineer/ Scott M. Werley Responsible PG: Project Name: Wright's Executive Sales Sheet: 1 of 1 Boring No: UT-36 Client: Geerhouse Partners, LLC Project No.: 10039-B 721 and 723 Rigsbee Avenue; 620 and 616 Site Location: Driller: Drill Rig: Hand Auger Foster Street, Raleigh, NC Latitude/Longitude: c _� 16 E j J Depth/Elevation v Q Soil Classification Description Q E a, Q 12 a n E 0.0 0.0 UT-3 B 0.0 0.0 END OF DRILLING AT 4.0 FT 5 -5 10 -10 15 -15 20 -20 25 -25 30 SZ WL (First Encountered) Boring Started: Jun 20 2022 1 WL (Completion) Boring Completed: Jun 20 2022 Remarks: Logged By: Austin Deans, Emery Lovekamp Principal Engineer/ Scott M. Werley Responsible PG: Project Name: Wright's Executive Sales Sheet: 1 of 1 Boring No: UT-3C Client: Geerhouse Partners, LLC Project No.: 10039-B 721 and 723 Rigsbee Avenue; 620 and 616 Site Location: Driller: Drill Rig: Hand Auger Foster Street, Raleigh, NC Latitude/Longitude: c _� 16 E j J Depth/Elevation v Q Soil Classification Description Q E a, Q 12 a n E 0.0 0.0 UT-3C 0.0 0.0 END OF DRILLING AT 4.0 FT 5 -5 10 -10 15 -15 20 -20 25 -25 30 SZ WL (First Encountered) Boring Started: Jun 20 2022 1 WL (Completion) Boring Completed: Jun 20 2022 Remarks: Logged By: Austin Deans, Emery Lovekamp Principal Engineer/ Scott M. Werley Responsible PG: Project Name: Wright's Executive Sales Sheet: 1 of 1 Boring No: UT-311) Client: Geerhouse Partners, LLC Project No.: 10039-B 721 and 723 Rigsbee Avenue; 620 and 616 Site Location: Driller: Drill Rig: Hand Auger Foster Street, Raleigh, NC Latitude/Longitude: c _� 16 E j J Depth/Elevation v Q Soil Classification Description Q E a, Q 12 a n E 0.0 0.0 UT-3D 0.0 0.0 END OF DRILLING AT 4.0 FT 5 -5 10 -10 15 -15 20 -20 25 -25 30 SZ WL (First Encountered) Boring Started: Jun 20 2022 1 WL (Completion) Boring Completed: Jun 20 2022 Remarks: Logged By: Austin Deans, Emery Lovekamp Principal Engineer/ Scott M. Werley Responsible PG: Project Name: Wright's Executive Sales Sheet: 1 of 1 Boring No: UT-3F Client: Geerhouse Partners, LLC Project No.: 10039-B 721 and 723 Rigsbee Avenue; 620 and 616 Site Location: Driller: Drill Rig: Hand Auger Foster Street, Raleigh, NC Latitude/Longitude: c _� 16 E j J Depth/Elevation v Q Soil Classification Description Q E a, Q 12 a n E 0.0 0.0 UT-3F 0.0 0.0 END OF DRILLING AT 4.0 FT 5 -5 10 -10 15 -15 20 -20 25 -25 30 SZ WL (First Encountered) Boring Started: Jun 20 2022 1 WL (Completion) Boring Completed: Jun 20 2022 Remarks: Logged By: Austin Deans, Emery Lovekamp Principal Engineer/ Scott M. Werley Responsible PG: Project Name: Wright's Executive Sales Sheet: 1 of 1 Boring No: UT-4A Client: Geerhouse Partners, LLC Project No.: 10039-B 721 and 723 Rigsbee Avenue; 620 and 616 Site Location: Driller: Drill Rig: Hand Auger Foster Street, Raleigh, NC Latitude/Longitude: c _� 16 E j J Depth/Elevation v Q Soil Classification Description Q E a, Q 12 a n E 0.4 2.3 UT-4A 2.5 3.7 END OF DRILLING AT 4.0 FT 5 -5 10 -10 15 -15 20 -20 25 -25 30 SZ WL (First Encountered) Boring Started: Jun 17 2022 1 WL (Completion) Boring Completed: Jun 17 2022 Remarks: Logged By: Austin Deans, Emery Lovekamp Principal Engineer/ Scott M. Werley Responsible PG: Project Name: Wright's Executive Sales Sheet: 1 of 1 Boring No: UT-46 Client: Geerhouse Partners, LLC Project No.: 10039-B 721 and 723 Rigsbee Avenue; 620 and 616 Site Location: Driller: Drill Rig: Hand Auger Foster Street, Raleigh, NC Latitude/Longitude: c _� 16 E j J Depth/Elevation v Q Soil Classification Description Q E a, Q 12 a n E 0.0 0.3 UT-4B 2.3 1.0 END OF DRILLING AT 4.0 FT 5 -5 10 -10 15 -15 20 -20 25 -25 30 SZ WL (First Encountered) Boring Started: Jun 17 2022 1 WL (Completion) Boring Completed: Jun 17 2022 Remarks: Logged By: Austin Deans, Emery Lovekamp Principal Engineer/ Scott M. Werley Responsible PG: Project Name: Wright's Executive Sales Sheet: 1 of 1 Boring No: UT-4C Client: Geerhouse Partners, LLC Project No.: 10039-B 721 and 723 Rigsbee Avenue; 620 and 616 Site Location: Driller: Drill Rig: Hand Auger Foster Street, Raleigh, NC Latitude/Longitude: c _� 16 E j J Depth/Elevation v Q Soil Classification Description Q E a, Q 12 a n E 0.0 0.1 UT-4C 3.1 0.3 END OF DRILLING AT 4.0 FT 5 -5 10 -10 15 -15 20 -20 25 -25 30 SZ WL (First Encountered) Boring Started: Jun 17 2022 1 WL (Completion) Boring Completed: Jun 17 2022 Remarks: Logged By: Austin Deans, Emery Lovekamp Principal Engineer/ Scott M. Werley Responsible PG: Project Name: Wright's Executive Sales Sheet: 1 of 1 Boring No: UT-411) Client: Geerhouse Partners, LLC Project No.: 10039-B 721 and 723 Rigsbee Avenue; 620 and 616 Site Location: Driller: Drill Rig: Hand Auger Foster Street, Raleigh, NC Latitude/Longitude: c _� 16 E j J Depth/Elevation v Q Soil Classification Description Q E a, Q 12 a n E 0.0 0.0 UT-4D 0.0 0.0 END OF DRILLING AT 4.0 FT 5 -5 10 -10 15 -15 20 -20 25 -25 30 SZ WL (First Encountered) Boring Started: Jun 17 2022 1 WL (Completion) Boring Completed: Jun 17 2022 Remarks: Logged By: Austin Deans, Emery Lovekamp Principal Engineer/ Scott M. Werley Responsible PG: Project Name: Wright's Executive Sales Sheet: 1 of 1 Boring No: UT-4E Client: Geerhouse Partners, LLC Project No.: 10039-B 721 and 723 Rigsbee Avenue; 620 and 616 Site Location: Driller: Drill Rig: Hand Auger Foster Street, Raleigh, NC Latitude/Longitude: c _� 16 E j J Depth/Elevation v Q Soil Classification Description Q E a, Q 12 a n E 0.0 0.0 UT-4E 0.0 5.4 END OF DRILLING AT 4.0 FT 5 -5 10 -10 15 -15 20 -20 25 -25 30 SZ WL (First Encountered) Boring Started: Jun 17 2022 1 WL (Completion) Boring Completed: Jun 17 2022 Remarks: Logged By: Austin Deans, Emery Lovekamp Principal Engineer/ Scott M. Werley Responsible PG: APPENDIX C LABORATORY ANALYTICAL DATA AND CHAIN OF CUSTODY (COC) RECORDS leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 July 21, 2022 Ron Navarro ECS Raleigh 5260 Greens Dairy Road Raleigh, NC 27616 RE: Project: Wright's Executive Sales Pace Project No.: 92610504 Dear Ron Navarro: Enclosed are the analytical results for sample(s) received by the laboratory on June 17, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Gulf Coast • Pace National - Mt. Juliet • Pace Analytical Services - Charlotte Revised to include MDL's and J Flags per client request 07/21/22. If you have any questions concerning this report, please feel free to contact me. Sincerely, cL,+1,1- Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures cc: ECS Southeast Reporting, ECS Southeast REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 64 lacieAnalyfica(' www,pacelabs.com Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Wright's Executive Sales Pace Project No.: 92610504 Pace Analytical Services National 12065 Lebanon Road, Mt. Juliet, TN 37122 Alabama Certification #: 40660 Alaska Certification 17-026 Arizona Certification #: AZ0612 Arkansas Certification #: 88-0469 California Certification #: 2932 Canada Certification #: 1461.01 Colorado Certification #: TN00003 Connecticut Certification #: PH-0197 DOD Certification: #1461.01 EPA# TN00003 Florida Certification #: E87487 Georgia DW Certification #: 923 Georgia Certification: NELAP Idaho Certification #: TN00003 Illinois Certification #: 200008 Indiana Certification #: C-TN-01 Iowa Certification #: 364 Kansas Certification #: E-10277 Kentucky UST Certification #: 16 Kentucky Certification #: 90010 Louisiana Certification #: A130792 Louisiana DW Certification #: LA180010 Maine Certification #: TN0002 Maryland Certification #: 324 Massachusetts Certification #: M-TNO03 Michigan Certification #: 9958 Minnesota Certification #: 047-999-395 Mississippi Certification #: TN00003 Missouri Certification #: 340 Montana Certification M CERT0086 Nebraska Certification #: NE-OS-15-05 Pace Analytical Gulf Coast 7979 Innovation Park Drive, Baton Rouge, LA 70820 Arkansas Certification #: 88-0655 DoD ELAP Certification M 6429-01 Florida Certification #: E87854 Illinois Certification #: 004585 Kansas Certification #: E-10354 Louisiana/LELAP Certification #: 01955 North Carolina Certification M 618 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 CERTIFICATIONS Nevada Certification #: TN-03-2002-34 New Hampshire Certification #: 2975 New Jersey Certification #: TNO02 New Mexico DW Certification New York Certification #: 11742 North Carolina Aquatic Toxicity Certification #: 41 North Carolina Drinking Water Certification #: 21704 North Carolina Environmental Certificate #: 375 North Dakota Certification #: R-140 Ohio VAP Certification #: CL0069 Oklahoma Certification #: 9915 Oregon Certification #: TN200002 Pennsylvania Certification #: 68-02979 Rhode Island Certification #: LA000356 South Carolina Certification #: 84004 South Dakota Certification Tennessee DW/Chem/Micro Certification #: 2006 Texas Certification #: T 104704245-17-14 Texas Mold Certification #: LAB0152 USDA Soil Permit #: P330-15-00234 Utah Certification #: TN00003 Virginia Certification #: VT2006 Vermont Dept. of Health: ID# VT-2006 Virginia Certification #: 460132 Washington Certification #: C847 West Virginia Certification #: 233 Wisconsin Certification #: 998093910 Wyoming UST Certification #: via A21LA 2926.01 A21-A-ISO 17025 Certification #: 1461.01 A21-A-ISO 17025 Certification #: 1461.02 AIHA-LAP/LLC EMLAP Certification #:100789 North Dakota Certification #: R-195 Oklahoma Certification #: 2019-101 South Carolina Certification #: 73006001 Texas Certification #: T104704178-19-11 USDA Soil Permit # P330-19-00209 Virginia Certification #: 460215 Washington Certification #: C929 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: Wright's Executive Sales Pace Project No.: 92610504 Lab ID Sample ID Matrix Date Collected Date Received 92610504001 SP-1 Solid 06/14/22 08:55 06/17/22 10:44 92610504002 SP-2 Solid 06/14/22 09:15 06/17/22 10:44 92610504003 SP-3 Solid 06/14/22 09:40 06/17/22 10:44 92610504004 DUP-1 Solid 06/14/22 00:00 06/17/22 10:44 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: Wright's Executive Sales 92610504 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92610504001 SP-1 EPA 8141B JMB 27 PAN EPA 8151 HMH 11 PAN EPA 8081 B BAJ 24 PASI-C EPA 6020E LWZ 7 GCLA EPA 7471 B LWZ, TDM 1 GCLA EPA 8270E BPJ 75 PASI-C EPA 8260D LMB 70 PASI-C SW-846 KDF 1 PASI-C SM 2540G CMK 1 PAN EPA 7199 ERP 1 PAN 92610504002 SP-2 EPA 8141B JMB 27 PAN EPA 8151 CCW 11 PAN EPA 8081 B BAJ 24 PASI-C EPA 6020E LWZ 7 GCLA EPA 7471 B LWZ, TDM 1 GCLA EPA 8270E BPJ 75 PASI-C EPA 8260D LMB 70 PASI-C SW-846 KDF 1 PASI-C SM 2540G CMK 1 PAN EPA 7199 ERP 1 PAN 92610504003 SP-3 EPA 8141B JMB 27 PAN EPA 8151 CCW 11 PAN EPA 8081 B BAJ 24 PASI-C EPA 6020E LWZ 7 GCLA EPA 7471 B LWZ, TDM 1 GCLA EPA 8270E BPJ 75 PASI-C EPA 8260D LMB 70 PASI-C SW-846 KDF 1 PASI-C SM 2540G CMK 1 PAN EPA 7199 ERP 1 PAN 92610504004 DUP-1 EPA 8141B JMB 27 PAN EPA 8151 CCW 11 PAN EPA 8081 B BAJ 24 PASI-C EPA 6020E LWZ 7 GCLA EPA 7471 B LWZ, TDM 1 GCLA EPA 8270E BPJ 75 PASI-C EPA 8260D LMB 70 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Wright's Executive Sales Pace Project No.: 92610504 Analytes Lab ID Sample ID Method Analysts Reported Laboratory SW-846 KDF 1 PASI-C SM 2540G CMK 1 PAN EPA 7199 ERP 1 PAN GCLA = Pace Analytical Gulf Coast PAN = Pace National - Mt. Juliet PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: SP-1 Lab ID: 92610504001 Collected: 06/14/22 08:55 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual OP Pesticides 8141 B Analytical Method: EPA 8141 B Preparation Method: 3546 Pace National - Mt. Juliet Azinphos, methyl (Guthion) ND mg/kg 0.148 0.0469 1 07/11/22 07:27 07/12/22 03:41 86-50-0 H3 Bolstar ND mg/kg 0.148 0.0220 1 07/11/22 07:27 07/12/22 03:41 35400-43-2 H3 Chlorpyrifos ND mg/kg 0.148 0.0232 1 07/11/22 07:27 07/12/22 03:41 2921-88-2 H3 Coumaphos ND mg/kg 0.148 0.0358 1 07/11/22 07:27 07/12/22 03:41 56-72-4 H3 Total Demeton ND mg/kg 0.103 0.00862 1 07/11/22 07:27 07/12/22 03:41 8065-48-3 H3 Diazinon ND mg/kg 0.148 0.0332 1 07/11/22 07:27 07/12/22 03:41 333-41-5 H3 Dichlorvos ND mg/kg 0.148 0.0443 1 07/11/22 07:27 07/12/22 03:41 62-73-7 H3 Dimethoate ND mg/kg 0.148 0.0493 1 07/11/22 07:27 07/12/22 03:41 60-51-5 H3 Disulfoton ND mg/kg 0.148 0.0375 1 07/11/22 07:27 07/12/22 03:41 298-04-4 H3 EPN (ENT) ND mg/kg 0.148 0.0407 1 07/11/22 07:27 07/12/22 03:41 2104-64-5 H3 Ethoprop ND mg/kg 0.148 0.0174 1 07/11/22 07:27 07/12/22 03:41 13194-48-4 H3 Parathion (Ethyl parathion) ND mg/kg 0.148 0.0242 1 07/11/22 07:27 07/12/22 03:41 56-38-2 H3 Fensulfothion ND mg/kg 0.148 0.0521 1 07/11/22 07:27 07/12/22 03:41 115-90-2 H3 Fenthion ND mg/kg 0.148 0.0196 1 07/11/22 07:27 07/12/22 03:41 55-38-9 H3 Malathion ND mg/kg 0.148 0.0264 1 07/11/22 07:27 07/12/22 03:41 121-75-5 H3 Merphos ND mg/kg 0.148 0.0342 1 07/11/22 07:27 07/12/22 03:41 150-50-5 H3 Methyl parathion ND mg/kg 0.148 0.0299 1 07/11/22 07:27 07/12/22 03:41 298-00-0 H3 Mevinphos ND mg/kg 0.148 0.0339 1 07/11/22 07:27 07/12/22 03:41 7786-34-7 H3 Naled ND mg/kg 0.148 0.0708 1 07/11/22 07:27 07/12/22 03:41 300-76-5 H3 Phorate ND mg/kg 0.148 0.0310 1 07/11/22 07:27 07/12/22 03:41 298-02-2 H3 Ronnel ND mg/kg 0.148 0.0220 1 07/11/22 07:27 07/12/22 03:41 299-84-3 H3 Stirophos (Tetrachlorvinphos) ND mg/kg 0.148 0.0263 1 07/11/22 07:27 07/12/22 03:41 22248-79-9 H3 Sulfotepp (ThiodiphosphoricAc ND mg/kg 0.148 0.0145 1 07/11/22 07:27 07/12/22 03:41 3689-24-5 H3 TEPP ND mg/kg 1.48 0.232 1 07/11/22 07:27 07/12/22 03:41 107-49-3 H3 Tokuthion (Prothiofos) ND mg/kg 0.148 0.0221 1 07/11/22 07:27 07/12/22 03:41 34643-46-4 H3 Trichloronate ND mg/kg 0.148 0.0297 1 07/11/22 07:27 07/12/22 03:41 327-98-0 H3 Surrogates Triphenylphosphate (S) 74.8 % 36.0-121 1 07/11/22 07:27 07/12/22 03:41 115-86-6 Chlorinated Herb. (GC) 8151 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND mg/kg 0.103 0.0104 1 07/13/22 10:13 07/15/22 02:29 94-75-7 H3 Dalapon ND mg/kg 0.103 0.0167 1 07/13/22 10:13 07/15/22 02:29 127-20-8 H3 2,4-DB ND mg/kg 0.103 0.0438 1 07/13/22 10:13 07/15/22 02:29 94-82-6 H3 Dicamba ND mg/kg 0.103 0.0232 1 07/13/22 10:13 07/15/22 02:29 1918-00-9 H3 Dichloroprop ND mg/kg 0.103 0.0361 1 07/13/22 10:13 07/15/22 02:29 15165-67-0 H3 Dinoseb ND mg/kg 0.103 0.0103 1 07/13/22 10:13 07/15/22 02:29 88-85-7 H3 MCPA ND mg/kg 9.59 0.654 1 07/13/22 10:13 07/15/22 02:29 94-74-6 H3 MCPP ND mg/kg 9.59 0.541 1 07/13/22 10:13 07/15/22 02:29 7085-19-0 H3 2,4,5-T ND mg/kg 0.103 0.0126 1 07/13/22 10:13 07/15/22 02:29 93-76-5 H3 2,4,5-TP (Silvex) ND mg/kg 0.103 0.0158 1 07/13/22 10:13 07/15/22 02:29 93-72-1 H3 Surrogates 2,4-DCAA (S) 56.3 % 22.0-132 1 07/13/22 10:13 07/15/22 02:29 19719-28-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: SP-1 Lab ID: 92610504001 Collected: 06/14/22 08:55 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 B Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Aldrin ND mg/kg 0.0025 0.0010 1 06/22/22 16:23 06/27/22 12:58 309-00-2 alpha-BHC ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 12:58 319-84-6 beta-BHC ND mg/kg 0.0025 0.0012 1 06/22/22 16:23 06/27/22 12:58 319-85-7 delta-BHC ND mg/kg 0.0025 0.0013 1 06/22/22 16:23 06/27/22 12:58 319-86-8 gamma-BHC (Lindane) ND mg/kg 0.0025 0.0010 1 06/22/22 16:23 06/27/22 12:58 58-89-9 Chlordane (Technical) ND mg/kg 0.013 0.011 1 06/22/22 16:23 06/27/22 12:58 57-74-9 4,4'-DDD ND mg/kg 0.0025 0.0012 1 06/22/22 16:23 06/27/22 12:58 72-54-8 4,4'-DDE ND mg/kg 0.0025 0.0012 1 06/22/22 16:23 06/27/22 12:58 72-55-9 4,4'-DDT ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 12:58 50-29-3 Dieldrin ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 12:58 60-57-1 Endosulfan I ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 12:58 959-98-8 Endosulfan 11 ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 12:58 33213-65-9 Endosulfan sulfate ND mg/kg 0.0025 0.0014 1 06/22/22 16:23 06/27/22 12:58 1031-07-8 Endrin ND mg/kg 0.0025 0.0012 1 06/22/22 16:23 06/27/22 12:58 72-20-8 Endrin aldehyde ND mg/kg 0.0025 0.0017 1 06/22/22 16:23 06/27/22 12:58 7421-93-4 Endrin ketone ND mg/kg 0.0025 0.0014 1 06/22/22 16:23 06/27/22 12:58 53494-70-5 Heptachlor ND mg/kg 0.0025 0.0012 1 06/22/22 16:23 06/27/22 12:58 76-44-8 Heptachlor epoxide ND mg/kg 0.0025 0.0010 1 06/22/22 16:23 06/27/22 12:58 1024-57-3 Hexachlorobenzene ND mg/kg 0.0025 0.0010 1 06/22/22 16:23 06/27/22 12:58 118-74-1 Methoxychlor ND mg/kg 0.0063 0.0031 1 06/22/22 16:23 06/27/22 12:58 72-43-5 Mirex ND mg/kg 0.0063 0.0028 1 06/22/22 16:23 06/27/22 12:58 2385-85-5 Toxaphene ND mg/kg 0.0089 0.0068 1 06/22/22 16:23 06/27/22 12:58 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 47 % 10-133 1 06/22/22 16:23 06/27/22 12:58 877-09-8 Decachlorobiphenyl (S) 48 % 10-146 1 06/22/22 16:23 06/27/22 12:58 2051-24-3 EPA 6020B Analytical Method: EPA 6020E Preparation Method: EPA 3050B Pace Analytical Gulf Coast Arsenic 2.15 mg/kg 0.49 0.12 10 06/26/22 09:00 06/29/22 20:55 7440-38-2 Arsenic 2.65 mg/kg 0.49 0.12 10 06/22/22 09:30 06/22/22 20:23 7440-38-2 Barium 84.8 mg/kg 0.49 0.12 10 06/22/22 09:30 06/22/22 20:23 7440-39-3 Barium 84.2 mg/kg 0.49 0.12 10 06/26/22 09:00 06/29/22 20:55 7440-39-3 Cadmium ND mg/kg 0.49 0.12 10 06/26/22 09:00 06/29/22 20:55 7440-43-9 Cadmium ND mg/kg 0.49 0.12 10 06/22/22 09:30 06/22/22 20:23 7440-43-9 Chromium 84.6 mg/kg 0.49 0.12 10 06/26/22 09:00 06/29/22 20:55 7440-47-3 Chromium 71.5 mg/kg 0.49 0.12 10 06/22/22 09:30 06/22/22 20:23 7440-47-3 Lead 7.32 mg/kg 0.49 0.12 10 06/26/22 09:00 06/29/22 20:55 7439-92-1 Lead 6.47 mg/kg 0.49 0.12 10 06/22/22 09:30 06/22/22 20:23 7439-92-1 Selenium ND mg/kg 0.49 0.12 10 06/22/22 09:30 06/22/22 20:23 7782-49-2 Selenium ND mg/kg 0.49 0.12 10 06/26/22 09:00 06/29/22 20:55 7782-49-2 Silver ND mg/kg 0.49 0.12 10 06/26/22 09:00 06/29/22 20:55 7440-22-4 Silver ND mg/kg 0.49 0.12 10 06/22/22 09:30 06/22/22 20:23 7440-22-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: SP-1 Lab ID: 92610504001 Collected: 06/14/22 08:55 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual EPA 7471 B Analytical Method: EPA 7471 B Preparation Method: METHOD Pace Analytical Gulf Coast Mercury 0.027 mg/kg 0.014 0.0055 1 06/22/2214:45 06/23/2211:42 7439-97-6 Mercury 0.048 mg/kg 0.014 0.0056 1 06/26/2212:15 06/27/2212:50 7439-97-6 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 14:33 83-32-9 Acenaphthylene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 14:33 208-96-8 Aniline ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 14:33 62-53-3 Anthracene ND mg/kg 0.41 0.13 1 06/23/22 07:43 06/29/22 14:33 120-12-7 Benzo(a)anthracene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 14:33 56-55-3 Benzo(a)pyrene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 14:33 50-32-8 Benzo(b)fluoranthene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 14:33 205-99-2 Benzo(g,h,i)perylene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 14:33 191-24-2 Benzo(k)fluoranthene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 14:33 207-08-9 Benzoic Acid ND mg/kg 2.1 0.88 1 06/23/22 07:43 06/29/22 14:33 65-85-0 Benzyl alcohol ND mg/kg 0.82 0.31 1 06/23/22 07:43 06/29/22 14:33 100-51-6 4-Bromophenylphenyl ether ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 14:33 101-55-3 Butylbenzylphthalate ND mg/kg 0.41 0.17 1 06/23/22 07:43 06/29/22 14:33 85-68-7 4-Chloro-3-methyl phenol ND mg/kg 0.82 0.29 1 06/23/22 07:43 06/29/22 14:33 59-50-7 4-Chloroaniline ND mg/kg 0.82 0.32 1 06/23/22 07:43 06/29/22 14:33 106-47-8 bis(2-Chloroethoxy)methane ND mg/kg 0.41 0.17 1 06/23/22 07:43 06/29/22 14:33 111-91-1 bis(2-Chloroethyl) ether ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 14:33 111-44-4 2-Chloronaphthalene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 14:33 91-58-7 2-Chlorophenol ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 14:33 95-57-8 4-Chlorophenylphenyl ether ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 14:33 7005-72-3 Chrysene ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 14:33 218-01-9 Dibenz(a,h)anthracene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 14:33 53-70-3 Dibenzofuran ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 14:33 132-64-9 1,2-Dichlorobenzene ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 14:33 95-50-1 1,3-Dichlorobenzene ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 14:33 541-73-1 1,4-Dichlorobenzene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 14:33 106-46-7 3,3'-Dichlorobenzidine ND mg/kg 0.82 0.28 1 06/23/22 07:43 06/29/22 14:33 91-94-1 2,4-Dichlorophenol ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 14:33 120-83-2 Diethylphthalate ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 14:33 84-66-2 2,4-Dimethylphenol ND mg/kg 0.41 0.17 1 06/23/22 07:43 06/29/22 14:33 105-67-9 Dimethylphthalate ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 14:33 131-11-3 Di-n-butylphthalate ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 14:33 84-74-2 4,6-Dinitro-2-methyl phenol ND mg/kg 0.82 0.38 1 06/23/22 07:43 06/29/22 14:33 534-52-1 2,4-Dinitrophenol ND mg/kg 2.1 1.3 1 06/23/22 07:43 06/29/22 14:33 51-28-5 2,4-Dinitrotoluene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 14:33 121-14-2 2,6-Dinitrotoluene ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 14:33 606-20-2 Di-n-octylphthalate ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 14:33 117-84-0 bis(2- Ethyl hexyl)phthalate ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 14:33 117-81-7 Fluoranthene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 14:33 206-44-0 REPORT OF LABORATORY ANALYSIS IL This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: SP-1 Lab ID: 92610504001 Collected: 06/14/22 08:55 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Fluorene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 14:33 86-73-7 Hexachloro-1,3-butadiene ND mg/kg 0.41 0.18 1 06/23/22 07:43 06/29/22 14:33 87-68-3 Hexachlorobenzene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 14:33 118-74-1 Hexachlorocyclopentadiene ND mg/kg 0.41 0.24 1 06/23/22 07:43 06/29/22 14:33 77-47-4 v2 Hexachloroethane ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 14:33 67-72-1 Indeno(1,2,3-cd)pyrene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 14:33 193-39-5 Isophorone ND mg/kg 0.41 0.18 1 06/23/22 07:43 06/29/22 14:33 78-59-1 1-Methylnaphthalene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 14:33 90-12-0 2-Methylnaphthalene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 14:33 91-57-6 2-Methylphenol(o-Cresol) ND mg/kg 0.41 0.17 1 06/23/22 07:43 06/29/22 14:33 95-48-7 3&4-Methyl phenol (m&p Cresol) ND mg/kg 0.41 0.17 1 06/23/22 07:43 06/29/22 14:33 15831-10-4 Naphthalene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 14:33 91-20-3 2-Nitroaniline ND mg/kg 2.1 0.34 1 06/23/22 07:43 06/29/22 14:33 88-74-4 3-Nitroaniline ND mg/kg 2.1 0.32 1 06/23/22 07:43 06/29/22 14:33 99-09-2 4-Nitroaniline ND mg/kg 0.82 0.31 1 06/23/22 07:43 06/29/22 14:33 100-01-6 Nitrobenzene ND mg/kg 0.41 0.19 1 06/23/22 07:43 06/29/22 14:33 98-95-3 2-Nitrophenol ND mg/kg 0.41 0.18 1 06/23/22 07:43 06/29/22 14:33 88-75-5 4-Nitrophenol ND mg/kg 2.1 0.79 1 06/23/22 07:43 06/29/22 14:33 100-02-7 N-Nitrosodimethylamine ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 14:33 62-75-9 N-Nitroso-di-n-propylamine ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 14:33 621-64-7 N-Nitrosodiphenylamine ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 14:33 86-30-6 2,2'-Oxybis(1-chloropropane) ND mg/kg 0.41 0.20 1 06/23/22 07:43 06/29/22 14:33 108-60-1 Pentachlorophenol ND mg/kg 0.82 0.40 1 06/23/22 07:43 06/29/22 14:33 87-86-5 Phenanthrene ND mg/kg 0.41 0.13 1 06/23/22 07:43 06/29/22 14:33 85-01-8 Phenol ND mg/kg 0.41 0.18 1 06/23/22 07:43 06/29/22 14:33 108-95-2 Pyrene ND mg/kg 0.41 0.17 1 06/23/22 07:43 06/29/22 14:33 129-00-0 Pyridine ND mg/kg 0.41 0.13 1 06/23/22 07:43 06/29/22 14:33 110-86-1 1,2,4-Trichlorobenzene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 14:33 120-82-1 2,4,5-Trichlorophenol ND mg/kg 0.41 0.19 1 06/23/22 07:43 06/29/22 14:33 95-95-4 2,4,6-Trichlorophenol ND mg/kg 0.41 0.17 1 06/23/22 07:43 06/29/22 14:33 88-06-2 Surrogates Nitrobenzene-d5 (S) 56 % 21-130 1 06/23/22 07:43 06/29/22 14:33 4165-60-0 2-Fluorobiphenyl (S) 52 % 19-130 1 06/23/22 07:43 06/29/22 14:33 321-60-8 Terphenyl-d14 (S) 71 % 15-130 1 06/23/22 07:43 06/29/22 14:33 1718-51-0 Phenol-d6 (S) 50 % 18-130 1 06/23/22 07:43 06/29/22 14:33 13127-88-3 2-Fluorophenol (S) 46 % 18-130 1 06/23/22 07:43 06/29/22 14:33 367-12-4 2,4,6-Tribromophenol (S) 61 % 18-130 1 06/23/22 07:43 06/29/22 14:33 118-79-6 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Acetone ND mg/kg 0.15 0.050 1 06/17/22 22:49 06/20/22 15:42 67-64-1 Benzene ND mg/kg 0.0077 0.0031 1 06/17/22 22:49 06/20/22 15:42 71-43-2 Bromobenzene ND mg/kg 0.0077 0.0025 1 06/17/22 22:49 06/20/22 15:42 108-86-1 Bromochloromethane ND mg/kg 0.0077 0.0023 1 06/17/22 22:49 06/20/22 15:42 74-97-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: SP-1 Lab ID: 92610504001 Collected: 06/14/22 08:55 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Bromodichloromethane ND mg/kg 0.0077 0.0030 1 06/17/22 22:49 06/20/22 15:42 75-27-4 Bromoform ND mg/kg 0.0077 0.0027 1 06/17/22 22:49 06/20/22 15:42 75-25-2 Bromomethane ND mg/kg 0.015 0.012 1 06/17/22 22:49 06/20/22 15:42 74-83-9 2-Butanone (MEK) 0.060J mg/kg 0.15 0.037 1 06/17/22 22:49 06/20/22 15:42 78-93-3 n-Butylbenzene ND mg/kg 0.0077 0.0037 1 06/17/22 22:49 06/20/22 15:42 104-51-8 sec-Butylbenzene ND mg/kg 0.0077 0.0034 1 06/17/22 22:49 06/20/22 15:42 135-98-8 tert-Butyl benzene ND mg/kg 0.0077 0.0028 1 06/17/22 22:49 06/20/22 15:42 98-06-6 Carbon tetrachloride ND mg/kg 0.0077 0.0029 1 06/17/22 22:49 06/20/22 15:42 56-23-5 Chlorobenzene ND mg/kg 0.0077 0.0015 1 06/17/22 22:49 06/20/22 15:42 108-90-7 Chloroethane ND mg/kg 0.015 0.0060 1 06/17/22 22:49 06/20/22 15:42 75-00-3 Chloroform ND mg/kg 0.0077 0.0047 1 06/17/22 22:49 06/20/22 15:42 67-66-3 Chloromethane ND mg/kg 0.015 0.0065 1 06/17/22 22:49 06/20/22 15:42 74-87-3 2-Chlorotoluene ND mg/kg 0.0077 0.0027 1 06/17/22 22:49 06/20/22 15:42 95-49-8 4-Chlorotoluene ND mg/kg 0.0077 0.0014 1 06/17/22 22:49 06/20/22 15:42 106-43-4 1,2-Dibromo-3-chloropropane ND mg/kg 0.0077 0.0030 1 06/17/22 22:49 06/20/22 15:42 96-12-8 Dibromochloromethane ND mg/kg 0.0077 0.0044 1 06/17/22 22:49 06/20/22 15:42 124-48-1 1,2-Dibromoethane (EDB) ND mg/kg 0.0077 0.0034 1 06/17/22 22:49 06/20/22 15:42 106-93-4 Dibromomethane ND mg/kg 0.0077 0.0017 1 06/17/22 22:49 06/20/22 15:42 74-95-3 1,2-Dichlorobenzene ND mg/kg 0.0077 0.0028 1 06/17/22 22:49 06/20/22 15:42 95-50-1 1,3-Dichlorobenzene ND mg/kg 0.0077 0.0024 1 06/17/22 22:49 06/20/22 15:42 541-73-1 1,4-Dichlorobenzene ND mg/kg 0.0077 0.0020 1 06/17/22 22:49 06/20/22 15:42 106-46-7 Dichlorodifluoromethane ND mg/kg 0.015 0.0034 1 06/17/22 22:49 06/20/22 15:42 75-71-8 1,1-Dichloroethane ND mg/kg 0.0077 0.0032 1 06/17/22 22:49 06/20/22 15:42 75-34-3 1,2-Dichloroethane ND mg/kg 0.0077 0.0051 1 06/17/22 22:49 06/20/22 15:42 107-06-2 1,1-Dichloroethene ND mg/kg 0.0077 0.0032 1 06/17/22 22:49 06/20/22 15:42 75-35-4 cis-1,2-Dichloroethene ND mg/kg 0.0077 0.0026 1 06/17/22 22:49 06/20/22 15:42 156-59-2 trans-1,2-Dichloroethene ND mg/kg 0.0077 0.0027 1 06/17/22 22:49 06/20/22 15:42 156-60-5 1,2-Dichloropropane ND mg/kg 0.0077 0.0023 1 06/17/22 22:49 06/20/22 15:42 78-87-5 1,3-Dichloropropane ND mg/kg 0.0077 0.0024 1 06/17/22 22:49 06/20/22 15:42 142-28-9 2,2-Dichloropropane ND mg/kg 0.0077 0.0025 1 06/17/22 22:49 06/20/22 15:42 594-20-7 1,1-Dichloropropene ND mg/kg 0.0077 0.0037 1 06/17/22 22:49 06/20/22 15:42 563-58-6 cis-1,3-Dichloropropene ND mg/kg 0.0077 0.0021 1 06/17/22 22:49 06/20/22 15:42 10061-01-5 trans- 1,3-Dichloropropene ND mg/kg 0.0077 0.0027 1 06/17/22 22:49 06/20/22 15:42 10061-02-6 Diisopropyl ether ND mg/kg 0.0077 0.0021 1 06/17/22 22:49 06/20/22 15:42 108-20-3 Ethylbenzene ND mg/kg 0.0077 0.0036 1 06/17/22 22:49 06/20/22 15:42 100-41-4 Hexachloro-1,3-butadiene ND mg/kg 0.015 0.013 1 06/17/22 22:49 06/20/22 15:42 87-68-3 2-Hexanone ND mg/kg 0.077 0.0075 1 06/17/22 22:49 06/20/22 15:42 591-78-6 Isopropylbenzene (Cumene) ND mg/kg 0.0077 0.0026 1 06/17/22 22:49 06/20/22 15:42 98-82-8 p-Isopropyltoluene ND mg/kg 0.0077 0.0038 1 06/17/22 22:49 06/20/22 15:42 99-87-6 Methylene Chloride ND mg/kg 0.031 0.021 1 06/17/22 22:49 06/20/22 15:42 75-09-2 4-Methyl-2-pentanone (MIBK) ND mg/kg 0.077 0.0075 1 06/17/22 22:49 06/20/22 15:42 108-10-1 Methyl-tert-butyl ether ND mg/kg 0.0077 0.0029 1 06/17/22 22:49 06/20/22 15:42 1634-04-4 Naphthalene ND mg/kg 0.0077 0.0041 1 06/17/22 22:49 06/20/22 15:42 91-20-3 n-Propylbenzene ND mg/kg 0.0077 0.0028 1 06/17/22 22:49 06/20/22 15:42 103-65-1 REPORT OF LABORATORY ANALYSIS v1 IK v1 v1 v1 v1 This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: SP-1 Lab ID: 92610504001 Collected: 06/14/22 08:55 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Total Solids 2540 G-2011 Total Solids Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 0.0068J mg/kg 0.0077 0.0020 1 06/17/22 22:49 06/20/22 15:42 100-42-5 ND mg/kg 0.0077 0.0030 1 06/17/22 22:49 06/20/22 15:42 630-20-6 ND mg/kg 0.0077 0.0020 1 06/17/22 22:49 06/20/22 15:42 79-34-5 ND mg/kg 0.0077 0.0024 1 06/17/22 22:49 06/20/22 15:42 127-18-4 ND mg/kg 0.0077 0.0022 1 06/17/22 22:49 06/20/22 15:42 108-88-3 ND mg/kg 0.0077 0.0063 1 06/17/22 22:49 06/20/22 15:42 87-61-6 ND mg/kg 0.0077 0.0065 1 06/17/22 22:49 06/20/22 15:42 120-82-1 ND mg/kg 0.0077 0.0040 1 06/17/22 22:49 06/20/22 15:42 71-55-6 ND mg/kg 0.0077 0.0026 1 06/17/22 22:49 06/20/22 15:42 79-00-5 ND mg/kg 0.0077 0.0020 1 06/17/22 22:49 06/20/22 15:42 79-01-6 ND mg/kg 0.0077 0.0043 1 06/17/22 22:49 06/20/22 15:42 75-69-4 ND mg/kg 0.0077 0.0039 1 06/17/22 22:49 06/20/22 15:42 96-18-4 ND mg/kg 0.0077 0.0021 1 06/17/22 22:49 06/20/22 15:42 95-63-6 ND mg/kg 0.0077 0.0026 1 06/17/22 22:49 06/20/22 15:42 108-67-8 ND mg/kg 0.077 0.0056 1 06/17/22 22:49 06/20/22 15:42 108-05-4 ND mg/kg 0.015 0.0039 1 06/17/22 22:49 06/20/22 15:42 75-01-4 ND mg/kg 0.015 0.0044 1 06/17/22 22:49 06/20/22 15:42 1330-20-7 ND mg/kg 0.015 0.0053 1 06/17/22 22:49 06/20/22 15:42 179601-23-1 ND mg/kg 0.0077 0.0034 1 06/17/22 22:49 06/20/22 15:42 95-47-6 100 % 70-130 1 06/17/22 22:49 06/20/22 15:42 2037-26-5 100 % 69-134 1 06/17/22 22:49 06/20/22 15:42 460-00-4 102 % 70-130 1 06/17/22 22:49 06/20/22 15:42 17060-07-0 Analytical Method: SW-846 Pace Analytical Services - Charlotte 20.9 % 0.10 0.10 1 06/20/2213:15 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet 67.8 % 1 07/12/2214:30 07/12/2214:43 Wet Chemistry 7199 Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Chromium, Hexavalent ND mg/kg 1.48 0.376 1 07/13/22 14:13 07/15/22 13:20 18540-29-9 Date: 07/21 /2022 05:24 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 Page 11 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: SP-2 Lab ID: 92610504002 Collected: 06/14/22 09:15 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual OP Pesticides 8141 B Analytical Method: EPA 8141 B Preparation Method: 3546 Pace National - Mt. Juliet Azinphos, methyl (Guthion) ND mg/kg 0.152 0.0483 1 07/11/22 07:27 07/12/22 04:14 86-50-0 H3 Bolstar ND mg/kg 0.152 0.0226 1 07/11/22 07:27 07/12/22 04:14 35400-43-2 H3 Chlorpyrifos ND mg/kg 0.152 0.0239 1 07/11/22 07:27 07/12/22 04:14 2921-88-2 H3 Coumaphos ND mg/kg 0.152 0.0369 1 07/11/22 07:27 07/12/22 04:14 56-72-4 H3 Total Demeton ND mg/kg 0.106 0.00887 1 07/11/22 07:27 07/12/22 04:14 8065-48-3 H3 Diazinon ND mg/kg 0.152 0.0342 1 07/11/22 07:27 07/12/22 04:14 333-41-5 H3 Dichlorvos ND mg/kg 0.152 0.0456 1 07/11/22 07:27 07/12/22 04:14 62-73-7 H3 Dimethoate ND mg/kg 0.152 0.0508 1 07/11/22 07:27 07/12/22 04:14 60-51-5 H3 Disulfoton ND mg/kg 0.152 0.0386 1 07/11/22 07:27 07/12/22 04:14 298-04-4 H3 EPN (ENT) ND mg/kg 0.152 0.0419 1 07/11/22 07:27 07/12/22 04:14 2104-64-5 H3 Ethoprop ND mg/kg 0.152 0.0179 1 07/11/22 07:27 07/12/22 04:14 13194-48-4 H3 Parathion (Ethyl parathion) ND mg/kg 0.152 0.0249 1 07/11/22 07:27 07/12/22 04:14 56-38-2 H3 Fensulfothion ND mg/kg 0.152 0.0536 1 07/11/22 07:27 07/12/22 04:14 115-90-2 H3 Fenthion ND mg/kg 0.152 0.0202 1 07/11/22 07:27 07/12/22 04:14 55-38-9 H3 Malathion ND mg/kg 0.152 0.0272 1 07/11/22 07:27 07/12/22 04:14 121-75-5 H3 Merphos ND mg/kg 0.152 0.0353 1 07/11/22 07:27 07/12/22 04:14 150-50-5 H3 Methyl parathion ND mg/kg 0.152 0.0308 1 07/11/22 07:27 07/12/22 04:14 298-00-0 H3 Mevinphos ND mg/kg 0.152 0.0349 1 07/11/22 07:27 07/12/22 04:14 7786-34-7 H3 Naled ND mg/kg 0.152 0.0729 1 07/11/22 07:27 07/12/22 04:14 300-76-5 H3 Phorate ND mg/kg 0.152 0.0319 1 07/11/22 07:27 07/12/22 04:14 298-02-2 H3 Ronnel ND mg/kg 0.152 0.0226 1 07/11/22 07:27 07/12/22 04:14 299-84-3 H3 Stirophos (Tetrachlorvinphos) ND mg/kg 0.152 0.0270 1 07/11/22 07:27 07/12/22 04:14 22248-79-9 H3 Sulfotepp (ThiodiphosphoricAc ND mg/kg 0.152 0.0150 1 07/11/22 07:27 07/12/22 04:14 3689-24-5 H3 TEPP ND mg/kg 1.52 0.239 1 07/11/22 07:27 07/12/22 04:14 107-49-3 H3 Tokuthion (Prothiofos) ND mg/kg 0.152 0.0228 1 07/11/22 07:27 07/12/22 04:14 34643-46-4 H3 Trichloronate ND mg/kg 0.152 0.0305 1 07/11/22 07:27 07/12/22 04:14 327-98-0 H3 Surrogates Triphenylphosphate (S) 64.2 % 36.0-121 1 07/11/22 07:27 07/12/22 04:14 115-86-6 Chlorinated Herb. (GC) 8151 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND mg/kg 0.106 0.0107 1 07/13/22 10:13 07/15/22 23:57 94-75-7 H3 Dalapon ND mg/kg 0.106 0.0172 1 07/13/22 10:13 07/15/22 23:57 127-20-8 H3 2,4-DB ND mg/kg 0.106 0.0451 1 07/13/22 10:13 07/15/22 23:57 94-82-6 H3 Dicamba ND mg/kg 0.106 0.0239 1 07/13/22 10:13 07/15/22 23:57 1918-00-9 H3 Dichloroprop ND mg/kg 0.106 0.0372 1 07/13/22 10:13 07/15/22 23:57 15165-67-0 H3 Dinoseb ND mg/kg 0.106 0.0106 1 07/13/22 10:13 07/15/22 23:57 88-85-7 H3 MCPA ND mg/kg 9.88 0.673 1 07/13/22 10:13 07/15/22 23:57 94-74-6 H3 MCPP ND mg/kg 9.88 0.558 1 07/13/22 10:13 07/15/22 23:57 7085-19-0 H3 2,4,5-T ND mg/kg 0.106 0.0129 1 07/13/22 10:13 07/15/22 23:57 93-76-5 H3 2,4,5-TP (Silvex) ND mg/kg 0.106 0.0163 1 07/13/22 10:13 07/15/22 23:57 93-72-1 H3 Surrogates 2,4-DCAA (S) 67.3 % 22.0-132 1 07/13/22 10:13 07/15/22 23:57 19719-28-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: SP-2 Lab ID: 92610504002 Collected: 06/14/22 09:15 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 B Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Aldrin ND mg/kg 0.0025 0.0010 1 06/22/22 16:23 06/27/22 13:09 309-00-2 alpha-BHC ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 13:09 319-84-6 beta-BHC ND mg/kg 0.0025 0.0012 1 06/22/22 16:23 06/27/22 13:09 319-85-7 delta-BHC ND mg/kg 0.0025 0.0013 1 06/22/22 16:23 06/27/22 13:09 319-86-8 gamma-BHC (Lindane) ND mg/kg 0.0025 0.0010 1 06/22/22 16:23 06/27/22 13:09 58-89-9 Chlordane (Technical) ND mg/kg 0.013 0.011 1 06/22/22 16:23 06/27/22 13:09 57-74-9 4,4'-DDD ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 13:09 72-54-8 4,4'-DDE ND mg/kg 0.0025 0.0012 1 06/22/22 16:23 06/27/22 13:09 72-55-9 4,4'-DDT ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 13:09 50-29-3 Dieldrin ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 13:09 60-57-1 Endosulfan I ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 13:09 959-98-8 Endosulfan 11 ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 13:09 33213-65-9 Endosulfan sulfate ND mg/kg 0.0025 0.0014 1 06/22/22 16:23 06/27/22 13:09 1031-07-8 Endrin ND mg/kg 0.0025 0.0012 1 06/22/22 16:23 06/27/22 13:09 72-20-8 Endrin aldehyde ND mg/kg 0.0025 0.0017 1 06/22/22 16:23 06/27/22 13:09 7421-93-4 Endrin ketone ND mg/kg 0.0025 0.0014 1 06/22/22 16:23 06/27/22 13:09 53494-70-5 Heptachlor ND mg/kg 0.0025 0.0012 1 06/22/22 16:23 06/27/22 13:09 76-44-8 Heptachlor epoxide ND mg/kg 0.0025 0.0010 1 06/22/22 16:23 06/27/22 13:09 1024-57-3 Hexachlorobenzene ND mg/kg 0.0025 0.0010 1 06/22/22 16:23 06/27/22 13:09 118-74-1 Methoxychlor ND mg/kg 0.0063 0.0031 1 06/22/22 16:23 06/27/22 13:09 72-43-5 Mirex ND mg/kg 0.0063 0.0028 1 06/22/22 16:23 06/27/22 13:09 2385-85-5 Toxaphene ND mg/kg 0.0089 0.0068 1 06/22/22 16:23 06/27/22 13:09 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 71 % 10-133 1 06/22/22 16:23 06/27/22 13:09 877-09-8 Decachlorobiphenyl (S) 70 % 10-146 1 06/22/22 16:23 06/27/22 13:09 2051-24-3 EPA 6020B Analytical Method: EPA 6020E Preparation Method: EPA 3050B Pace Analytical Gulf Coast Arsenic 3.65 mg/kg 0.45 0.11 10 06/22/22 09:30 06/22/22 20:26 7440-38-2 Arsenic 1.80 mg/kg 0.50 0.13 10 06/26/22 09:00 06/29/22 20:59 7440-38-2 Barium 83.2 mg/kg 0.45 0.11 10 06/22/22 09:30 06/22/22 20:26 7440-39-3 Barium 99.5 mg/kg 0.50 0.13 10 06/26/22 09:00 06/29/22 20:59 7440-39-3 Cadmium ND mg/kg 0.50 0.13 10 06/26/22 09:00 06/29/22 20:59 7440-43-9 Cadmium ND mg/kg 0.45 0.11 10 06/22/22 09:30 06/22/22 20:26 7440-43-9 Chromium 63.5 mg/kg 0.50 0.13 10 06/26/22 09:00 06/29/22 20:59 7440-47-3 Chromium 38.2 mg/kg 0.45 0.11 10 06/22/22 09:30 06/22/22 20:26 7440-47-3 Lead 7.45 mg/kg 0.45 0.11 10 06/22/22 09:30 06/22/22 20:26 7439-92-1 Lead 8.36 mg/kg 0.50 0.13 10 06/26/22 09:00 06/29/22 20:59 7439-92-1 Selenium ND mg/kg 0.50 0.13 10 06/26/22 09:00 06/29/22 20:59 7782-49-2 Selenium ND mg/kg 0.45 0.11 10 06/22/22 09:30 06/22/22 20:26 7782-49-2 Silver ND mg/kg 0.50 0.13 10 06/26/22 09:00 06/29/22 20:59 7440-22-4 Silver ND mg/kg 0.45 0.11 10 06/22/22 09:30 06/22/22 20:26 7440-22-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: SP-2 Lab ID: 92610504002 Collected: 06/14/22 09:15 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual EPA 7471 B Analytical Method: EPA 7471 B Preparation Method: METHOD Pace Analytical Gulf Coast Mercury ND mg/kg 0.014 0.0055 1 06/22/2214:45 06/23/2211:44 7439-97-6 Mercury 0.040 mg/kg 0.015 0.0059 1 06/26/2212:15 06/27/2212:52 7439-97-6 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:00 83-32-9 Acenaphthylene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:00 208-96-8 Aniline ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:00 62-53-3 Anthracene ND mg/kg 0.41 0.13 1 06/23/22 07:43 06/29/22 15:00 120-12-7 Benzo(a)anthracene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:00 56-55-3 Benzo(a)pyrene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:00 50-32-8 Benzo(b)fluoranthene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:00 205-99-2 Benzo(g,h,i)perylene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:00 191-24-2 Benzo(k)fluoranthene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:00 207-08-9 Benzoic Acid ND mg/kg 2.1 0.88 1 06/23/22 07:43 06/29/22 15:00 65-85-0 Benzyl alcohol ND mg/kg 0.82 0.31 1 06/23/22 07:43 06/29/22 15:00 100-51-6 4-Bromophenylphenyl ether ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:00 101-55-3 Butylbenzylphthalate ND mg/kg 0.41 0.17 1 06/23/22 07:43 06/29/22 15:00 85-68-7 4-Chloro-3-methyl phenol ND mg/kg 0.82 0.29 1 06/23/22 07:43 06/29/22 15:00 59-50-7 4-Chloroaniline ND mg/kg 0.82 0.32 1 06/23/22 07:43 06/29/22 15:00 106-47-8 bis(2-Chloroethoxy)methane ND mg/kg 0.41 0.17 1 06/23/22 07:43 06/29/22 15:00 111-91-1 bis(2-Chloroethyl) ether ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:00 111-44-4 2-Chloronaphthalene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:00 91-58-7 2-Chlorophenol ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:00 95-57-8 4-Chlorophenylphenyl ether ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:00 7005-72-3 Chrysene ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:00 218-01-9 Dibenz(a,h)anthracene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:00 53-70-3 Dibenzofuran ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:00 132-64-9 1,2-Dichlorobenzene ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:00 95-50-1 1,3-Dichlorobenzene ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:00 541-73-1 1,4-Dichlorobenzene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:00 106-46-7 3,3'-Dichlorobenzidine ND mg/kg 0.82 0.28 1 06/23/22 07:43 06/29/22 15:00 91-94-1 2,4-Dichlorophenol ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:00 120-83-2 Diethylphthalate ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:00 84-66-2 2,4-Dimethylphenol ND mg/kg 0.41 0.17 1 06/23/22 07:43 06/29/22 15:00 105-67-9 Dimethylphthalate ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:00 131-11-3 Di-n-butylphthalate ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:00 84-74-2 4,6-Dinitro-2-methyl phenol ND mg/kg 0.82 0.38 1 06/23/22 07:43 06/29/22 15:00 534-52-1 2,4-Dinitrophenol ND mg/kg 2.1 1.3 1 06/23/22 07:43 06/29/22 15:00 51-28-5 2,4-Dinitrotoluene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:00 121-14-2 2,6-Dinitrotoluene ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:00 606-20-2 Di-n-octylphthalate ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:00 117-84-0 bis(2- Ethyl hexyl)phthalate ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:00 117-81-7 Fluoranthene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:00 206-44-0 REPORT OF LABORATORY ANALYSIS IL This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: SP-2 Lab ID: 92610504002 Collected: 06/14/22 09:15 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Fluorene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:00 86-73-7 Hexachloro-1,3-butadiene ND mg/kg 0.41 0.18 1 06/23/22 07:43 06/29/22 15:00 87-68-3 Hexachlorobenzene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:00 118-74-1 Hexachlorocyclopentadiene ND mg/kg 0.41 0.24 1 06/23/22 07:43 06/29/22 15:00 77-47-4 v2 Hexachloroethane ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:00 67-72-1 Indeno(1,2,3-cd)pyrene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:00 193-39-5 Isophorone ND mg/kg 0.41 0.18 1 06/23/22 07:43 06/29/22 15:00 78-59-1 1-Methylnaphthalene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:00 90-12-0 2-Methylnaphthalene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:00 91-57-6 2-Methylphenol(o-Cresol) ND mg/kg 0.41 0.17 1 06/23/22 07:43 06/29/22 15:00 95-48-7 3&4-Methyl phenol (m&p Cresol) ND mg/kg 0.41 0.17 1 06/23/22 07:43 06/29/22 15:00 15831-10-4 Naphthalene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:00 91-20-3 2-Nitroaniline ND mg/kg 2.1 0.34 1 06/23/22 07:43 06/29/22 15:00 88-74-4 3-Nitroaniline ND mg/kg 2.1 0.32 1 06/23/22 07:43 06/29/22 15:00 99-09-2 4-Nitroaniline ND mg/kg 0.82 0.31 1 06/23/22 07:43 06/29/22 15:00 100-01-6 Nitrobenzene ND mg/kg 0.41 0.19 1 06/23/22 07:43 06/29/22 15:00 98-95-3 2-Nitrophenol ND mg/kg 0.41 0.18 1 06/23/22 07:43 06/29/22 15:00 88-75-5 4-Nitrophenol ND mg/kg 2.1 0.79 1 06/23/22 07:43 06/29/22 15:00 100-02-7 N-Nitrosodimethylamine ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:00 62-75-9 N-Nitroso-di-n-propylamine ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:00 621-64-7 N-Nitrosodiphenylamine ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:00 86-30-6 2,2'-Oxybis(1-chloropropane) ND mg/kg 0.41 0.20 1 06/23/22 07:43 06/29/22 15:00 108-60-1 Pentachlorophenol ND mg/kg 0.82 0.40 1 06/23/22 07:43 06/29/22 15:00 87-86-5 Phenanthrene ND mg/kg 0.41 0.13 1 06/23/22 07:43 06/29/22 15:00 85-01-8 Phenol ND mg/kg 0.41 0.18 1 06/23/22 07:43 06/29/22 15:00 108-95-2 Pyrene ND mg/kg 0.41 0.17 1 06/23/22 07:43 06/29/22 15:00 129-00-0 Pyridine ND mg/kg 0.41 0.13 1 06/23/22 07:43 06/29/22 15:00 110-86-1 1,2,4-Trichlorobenzene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:00 120-82-1 2,4,5-Trichlorophenol ND mg/kg 0.41 0.19 1 06/23/22 07:43 06/29/22 15:00 95-95-4 2,4,6-Trichlorophenol ND mg/kg 0.41 0.17 1 06/23/22 07:43 06/29/22 15:00 88-06-2 Surrogates Nitrobenzene-d5 (S) 63 % 21-130 1 06/23/22 07:43 06/29/22 15:00 4165-60-0 2-Fluorobiphenyl (S) 59 % 19-130 1 06/23/22 07:43 06/29/22 15:00 321-60-8 Terphenyl-d14 (S) 78 % 15-130 1 06/23/22 07:43 06/29/22 15:00 1718-51-0 Phenol-d6 (S) 56 % 18-130 1 06/23/22 07:43 06/29/22 15:00 13127-88-3 2-Fluorophenol (S) 52 % 18-130 1 06/23/22 07:43 06/29/22 15:00 367-12-4 2,4,6-Tribromophenol (S) 70 % 18-130 1 06/23/22 07:43 06/29/22 15:00 118-79-6 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Acetone ND mg/kg 0.17 0.054 1 06/17/22 22:49 06/20/22 16:00 67-64-1 Benzene ND mg/kg 0.0084 0.0033 1 06/17/22 22:49 06/20/22 16:00 71-43-2 Bromobenzene ND mg/kg 0.0084 0.0027 1 06/17/22 22:49 06/20/22 16:00 108-86-1 Bromochloromethane ND mg/kg 0.0084 0.0025 1 06/17/22 22:49 06/20/22 16:00 74-97-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: SP-2 Lab ID: 92610504002 Collected: 06/14/22 09:15 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Bromodichloromethane ND mg/kg 0.0084 0.0032 1 06/17/22 22:49 06/20/22 16:00 75-27-4 Bromoform ND mg/kg 0.0084 0.0030 1 06/17/22 22:49 06/20/22 16:00 75-25-2 Bromomethane ND mg/kg 0.017 0.013 1 06/17/22 22:49 06/20/22 16:00 74-83-9 2-Butanone (MEK) 0.0991 mg/kg 0.17 0.040 1 06/17/22 22:49 06/20/22 16:00 78-93-3 n-Butylbenzene ND mg/kg 0.0084 0.0040 1 06/17/22 22:49 06/20/22 16:00 104-51-8 sec-Butylbenzene ND mg/kg 0.0084 0.0037 1 06/17/22 22:49 06/20/22 16:00 135-98-8 tert-Butyl benzene ND mg/kg 0.0084 0.0030 1 06/17/22 22:49 06/20/22 16:00 98-06-6 Carbon tetrachloride ND mg/kg 0.0084 0.0031 1 06/17/22 22:49 06/20/22 16:00 56-23-5 Chlorobenzene ND mg/kg 0.0084 0.0016 1 06/17/22 22:49 06/20/22 16:00 108-90-7 Chloroethane ND mg/kg 0.017 0.0065 1 06/17/22 22:49 06/20/22 16:00 75-00-3 Chloroform ND mg/kg 0.0084 0.0051 1 06/17/22 22:49 06/20/22 16:00 67-66-3 Chloromethane ND mg/kg 0.017 0.0070 1 06/17/22 22:49 06/20/22 16:00 74-87-3 2-Chlorotoluene ND mg/kg 0.0084 0.0030 1 06/17/22 22:49 06/20/22 16:00 95-49-8 4-Chlorotoluene ND mg/kg 0.0084 0.0015 1 06/17/22 22:49 06/20/22 16:00 106-43-4 1,2-Dibromo-3-chloropropane ND mg/kg 0.0084 0.0033 1 06/17/22 22:49 06/20/22 16:00 96-12-8 Dibromochloromethane ND mg/kg 0.0084 0.0047 1 06/17/22 22:49 06/20/22 16:00 124-48-1 1,2-Dibromoethane (EDB) ND mg/kg 0.0084 0.0037 1 06/17/22 22:49 06/20/22 16:00 106-93-4 Dibromomethane ND mg/kg 0.0084 0.0018 1 06/17/22 22:49 06/20/22 16:00 74-95-3 1,2-Dichlorobenzene ND mg/kg 0.0084 0.0030 1 06/17/22 22:49 06/20/22 16:00 95-50-1 1,3-Dichlorobenzene ND mg/kg 0.0084 0.0026 1 06/17/22 22:49 06/20/22 16:00 541-73-1 1,4-Dichlorobenzene ND mg/kg 0.0084 0.0022 1 06/17/22 22:49 06/20/22 16:00 106-46-7 Dichlorodifluoromethane ND mg/kg 0.017 0.0036 1 06/17/22 22:49 06/20/22 16:00 75-71-8 1,1-Dichloroethane ND mg/kg 0.0084 0.0035 1 06/17/22 22:49 06/20/22 16:00 75-34-3 1,2-Dichloroethane ND mg/kg 0.0084 0.0056 1 06/17/22 22:49 06/20/22 16:00 107-06-2 1,1-Dichloroethene ND mg/kg 0.0084 0.0035 1 06/17/22 22:49 06/20/22 16:00 75-35-4 cis-1,2-Dichloroethene ND mg/kg 0.0084 0.0029 1 06/17/22 22:49 06/20/22 16:00 156-59-2 trans-1,2-Dichloroethene ND mg/kg 0.0084 0.0029 1 06/17/22 22:49 06/20/22 16:00 156-60-5 1,2-Dichloropropane ND mg/kg 0.0084 0.0025 1 06/17/22 22:49 06/20/22 16:00 78-87-5 1,3-Dichloropropane ND mg/kg 0.0084 0.0026 1 06/17/22 22:49 06/20/22 16:00 142-28-9 2,2-Dichloropropane ND mg/kg 0.0084 0.0027 1 06/17/22 22:49 06/20/22 16:00 594-20-7 1,1-Dichloropropene ND mg/kg 0.0084 0.0040 1 06/17/22 22:49 06/20/22 16:00 563-58-6 cis-1,3-Dichloropropene ND mg/kg 0.0084 0.0023 1 06/17/22 22:49 06/20/22 16:00 10061-01-5 trans- 1,3-Dichloropropene ND mg/kg 0.0084 0.0029 1 06/17/22 22:49 06/20/22 16:00 10061-02-6 Diisopropyl ether ND mg/kg 0.0084 0.0023 1 06/17/22 22:49 06/20/22 16:00 108-20-3 Ethylbenzene ND mg/kg 0.0084 0.0039 1 06/17/22 22:49 06/20/22 16:00 100-41-4 Hexachloro-1,3-butadiene ND mg/kg 0.017 0.014 1 06/17/22 22:49 06/20/22 16:00 87-68-3 2-Hexanone ND mg/kg 0.084 0.0081 1 06/17/22 22:49 06/20/22 16:00 591-78-6 Isopropylbenzene (Cumene) ND mg/kg 0.0084 0.0029 1 06/17/22 22:49 06/20/22 16:00 98-82-8 p-Isopropyltoluene ND mg/kg 0.0084 0.0041 1 06/17/22 22:49 06/20/22 16:00 99-87-6 Methylene Chloride ND mg/kg 0.034 0.023 1 06/17/22 22:49 06/20/22 16:00 75-09-2 4-Methyl-2-pentanone (MIBK) ND mg/kg 0.084 0.0081 1 06/17/22 22:49 06/20/22 16:00 108-10-1 Methyl-tert-butyl ether ND mg/kg 0.0084 0.0031 1 06/17/22 22:49 06/20/22 16:00 1634-04-4 Naphthalene ND mg/kg 0.0084 0.0044 1 06/17/22 22:49 06/20/22 16:00 91-20-3 n-Propylbenzene ND mg/kg 0.0084 0.0030 1 06/17/22 22:49 06/20/22 16:00 103-65-1 REPORT OF LABORATORY ANALYSIS v1 IK v1 v1 v1 v1 This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: SP-2 Lab ID: 92610504002 Collected: 06/14/22 09:15 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Total Solids 2540 G-2011 Total Solids Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 0.011 mg/kg 0.0084 0.0022 1 06/17/22 22:49 06/20/22 16:00 100-42-5 ND mg/kg 0.0084 0.0032 1 06/17/22 22:49 06/20/22 16:00 630-20-6 ND mg/kg 0.0084 0.0022 1 06/17/22 22:49 06/20/22 16:00 79-34-5 ND mg/kg 0.0084 0.0027 1 06/17/22 22:49 06/20/22 16:00 127-18-4 ND mg/kg 0.0084 0.0024 1 06/17/22 22:49 06/20/22 16:00 108-88-3 ND mg/kg 0.0084 0.0068 1 06/17/22 22:49 06/20/22 16:00 87-61-6 ND mg/kg 0.0084 0.0070 1 06/17/22 22:49 06/20/22 16:00 120-82-1 ND mg/kg 0.0084 0.0044 1 06/17/22 22:49 06/20/22 16:00 71-55-6 ND mg/kg 0.0084 0.0028 1 06/17/22 22:49 06/20/22 16:00 79-00-5 ND mg/kg 0.0084 0.0022 1 06/17/22 22:49 06/20/22 16:00 79-01-6 ND mg/kg 0.0084 0.0046 1 06/17/22 22:49 06/20/22 16:00 75-69-4 ND mg/kg 0.0084 0.0042 1 06/17/22 22:49 06/20/22 16:00 96-18-4 ND mg/kg 0.0084 0.0023 1 06/17/22 22:49 06/20/22 16:00 95-63-6 ND mg/kg 0.0084 0.0028 1 06/17/22 22:49 06/20/22 16:00 108-67-8 ND mg/kg 0.084 0.0061 1 06/17/22 22:49 06/20/22 16:00 108-05-4 ND mg/kg 0.017 0.0043 1 06/17/22 22:49 06/20/22 16:00 75-01-4 ND mg/kg 0.017 0.0048 1 06/17/22 22:49 06/20/22 16:00 1330-20-7 ND mg/kg 0.017 0.0057 1 06/17/22 22:49 06/20/22 16:00 179601-23-1 ND mg/kg 0.0084 0.0037 1 06/17/22 22:49 06/20/22 16:00 95-47-6 101 % 70-130 1 06/17/22 22:49 06/20/22 16:00 2037-26-5 101 % 69-134 1 06/17/22 22:49 06/20/22 16:00 460-00-4 103 % 70-130 1 06/17/22 22:49 06/20/22 16:00 17060-07-0 Analytical Method: SW-846 Pace Analytical Services - Charlotte 21.0 % 0.10 0.10 1 06/20/2213:16 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet 65.8 % 1 07/12/2214:30 07/12/2214:43 Wet Chemistry 7199 Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Chromium, Hexavalent ND mg/kg 1.52 0.387 1 07/13/22 14:13 07/15/22 13:25 18540-29-9 Date: 07/21 /2022 05:24 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 Page 17 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: SP-3 Lab ID: 92610504003 Collected: 06/14/22 09:40 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual OP Pesticides 8141 B Analytical Method: EPA 8141 B Preparation Method: 3546 Pace National - Mt. Juliet Azinphos, methyl (Guthion) ND mg/kg 0.142 0.0451 1 07/11/22 07:27 07/12/22 04:47 86-50-0 H3 Bolstar ND mg/kg 0.142 0.0211 1 07/11/22 07:27 07/12/22 04:47 35400-43-2 H3 Chlorpyrifos ND mg/kg 0.142 0.0223 1 07/11/22 07:27 07/12/22 04:47 2921-88-2 H3 Coumaphos ND mg/kg 0.142 0.0345 1 07/11/22 07:27 07/12/22 04:47 56-72-4 H3 Total Demeton ND mg/kg 0.0993 0.00828 1 07/11/22 07:27 07/12/22 04:47 8065-48-3 H3 Diazinon ND mg/kg 0.142 0.0319 1 07/11/22 07:27 07/12/22 04:47 333-41-5 H3 Dichlorvos ND mg/kg 0.142 0.0425 1 07/11/22 07:27 07/12/22 04:47 62-73-7 H3 Dimethoate ND mg/kg 0.142 0.0474 1 07/11/22 07:27 07/12/22 04:47 60-51-5 H3 Disulfoton ND mg/kg 0.142 0.0360 1 07/11/22 07:27 07/12/22 04:47 298-04-4 H3 EPN (ENT) ND mg/kg 0.142 0.0391 1 07/11/22 07:27 07/12/22 04:47 2104-64-5 H3 Ethoprop ND mg/kg 0.142 0.0167 1 07/11/22 07:27 07/12/22 04:47 13194-48-4 H3 Parathion (Ethyl parathion) ND mg/kg 0.142 0.0233 1 07/11/22 07:27 07/12/22 04:47 56-38-2 H3 Fensulfothion ND mg/kg 0.142 0.0501 1 07/11/22 07:27 07/12/22 04:47 115-90-2 H3 Fenthion ND mg/kg 0.142 0.0189 1 07/11/22 07:27 07/12/22 04:47 55-38-9 H3 Malathion ND mg/kg 0.142 0.0254 1 07/11/22 07:27 07/12/22 04:47 121-75-5 H3 Merphos ND mg/kg 0.142 0.0329 1 07/11/22 07:27 07/12/22 04:47 150-50-5 H3 Methyl parathion ND mg/kg 0.142 0.0288 1 07/11/22 07:27 07/12/22 04:47 298-00-0 H3 Mevinphos ND mg/kg 0.142 0.0326 1 07/11/22 07:27 07/12/22 04:47 7786-34-7 H3 Naled ND mg/kg 0.142 0.0681 1 07/11/22 07:27 07/12/22 04:47 300-76-5 H3 Phorate ND mg/kg 0.142 0.0298 1 07/11/22 07:27 07/12/22 04:47 298-02-2 H3 Ronnel ND mg/kg 0.142 0.0211 1 07/11/22 07:27 07/12/22 04:47 299-84-3 H3 Stirophos (Tetrachlorvinphos) ND mg/kg 0.142 0.0252 1 07/11/22 07:27 07/12/22 04:47 22248-79-9 H3 Sulfotepp (ThiodiphosphoricAc ND mg/kg 0.142 0.0140 1 07/11/22 07:27 07/12/22 04:47 3689-24-5 H3 TEPP ND mg/kg 1.42 0.223 1 07/11/22 07:27 07/12/22 04:47 107-49-3 H3 Tokuthion (Prothiofos) ND mg/kg 0.142 0.0213 1 07/11/22 07:27 07/12/22 04:47 34643-46-4 H3 Trichloronate ND mg/kg 0.142 0.0285 1 07/11/22 07:27 07/12/22 04:47 327-98-0 H3 Surrogates Triphenylphosphate (S) 62.1 % 36.0-121 1 07/11/22 07:27 07/12/22 04:47 115-86-6 Chlorinated Herb. (GC) 8151 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND mg/kg 0.100 0.0101 1.01 07/13/22 10:13 07/16/22 00:12 94-75-7 H3 Dalapon ND mg/kg 0.100 0.0162 1.01 07/13/22 10:13 07/16/22 00:12 127-20-8 H3 2,4-DB ND mg/kg 0.100 0.0425 1.01 07/13/22 10:13 07/16/22 00:12 94-82-6 H3 Dicamba ND mg/kg 0.100 0.0226 1.01 07/13/22 10:13 07/16/22 00:12 1918-00-9 H3 Dichloroprop ND mg/kg 0.100 0.0350 1.01 07/13/22 10:13 07/16/22 00:12 15165-67-0 H3 Dinoseb ND mg/kg 0.100 0.00998 1.01 07/13/22 10:13 07/16/22 00:12 88-85-7 H3 MCPA ND mg/kg 9.32 0.634 1.01 07/13/22 10:13 07/16/22 00:12 94-74-6 H3 MCPP ND mg/kg 9.32 0.526 1.01 07/13/22 10:13 07/16/22 00:12 7085-19-0 H3 2,4,5-T ND mg/kg 0.100 0.0122 1.01 07/13/22 10:13 07/16/22 00:12 93-76-5 H3 2,4,5-TP (Silvex) ND mg/kg 0.100 0.0153 1.01 07/13/22 10:13 07/16/22 00:12 93-72-1 H3 Surrogates 2,4-DCAA (S) 79.2 % 22.0-132 1.01 07/13/22 10:13 07/16/22 00:12 19719-28-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: SP-3 Lab ID: 92610504003 Collected: 06/14/22 09:40 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 B Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Aldrin ND mg/kg 0.0025 0.0010 1 06/22/22 16:23 06/27/22 13:21 309-00-2 alpha-BHC ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 13:21 319-84-6 beta-BHC ND mg/kg 0.0025 0.0012 1 06/22/22 16:23 06/27/22 13:21 319-85-7 delta-BHC ND mg/kg 0.0025 0.0012 1 06/22/22 16:23 06/27/22 13:21 319-86-8 gamma-BHC (Lindane) ND mg/kg 0.0025 0.00099 1 06/22/22 16:23 06/27/22 13:21 58-89-9 Chlordane (Technical) ND mg/kg 0.012 0.011 1 06/22/22 16:23 06/27/22 13:21 57-74-9 4,4'-DDD ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 13:21 72-54-8 4,4'-DDE ND mg/kg 0.0025 0.0012 1 06/22/22 16:23 06/27/22 13:21 72-55-9 4,4'-DDT ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 13:21 50-29-3 Dieldrin ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 13:21 60-57-1 Endosulfan I ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 13:21 959-98-8 Endosulfan 11 ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 13:21 33213-65-9 Endosulfan sulfate ND mg/kg 0.0025 0.0014 1 06/22/22 16:23 06/27/22 13:21 1031-07-8 Endrin ND mg/kg 0.0025 0.0012 1 06/22/22 16:23 06/27/22 13:21 72-20-8 Endrin aldehyde ND mg/kg 0.0025 0.0017 1 06/22/22 16:23 06/27/22 13:21 7421-93-4 Endrin ketone ND mg/kg 0.0025 0.0014 1 06/22/22 16:23 06/27/22 13:21 53494-70-5 Heptachlor ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 13:21 76-44-8 Heptachlor epoxide ND mg/kg 0.0025 0.00098 1 06/22/22 16:23 06/27/22 13:21 1024-57-3 Hexachlorobenzene ND mg/kg 0.0025 0.0010 1 06/22/22 16:23 06/27/22 13:21 118-74-1 Methoxychlor ND mg/kg 0.0062 0.0030 1 06/22/22 16:23 06/27/22 13:21 72-43-5 Mirex ND mg/kg 0.0062 0.0027 1 06/22/22 16:23 06/27/22 13:21 2385-85-5 Toxaphene ND mg/kg 0.0087 0.0066 1 06/22/22 16:23 06/27/22 13:21 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 44 % 10-133 1 06/22/22 16:23 06/27/22 13:21 877-09-8 Decachlorobiphenyl (S) 55 % 10-146 1 06/22/22 16:23 06/27/22 13:21 2051-24-3 EPA 6020B Analytical Method: EPA 6020E Preparation Method: EPA 3050B Pace Analytical Gulf Coast Arsenic 1.82 mg/kg 0.48 0.12 10 06/26/22 09:00 06/29/22 21:02 7440-38-2 Arsenic 2.10 mg/kg 0.48 0.12 10 06/22/22 09:30 06/22/22 20:30 7440-38-2 Barium 78.9 mg/kg 0.48 0.12 10 06/22/22 09:30 06/22/22 20:30 7440-39-3 Barium 88.4 mg/kg 0.48 0.12 10 06/26/22 09:00 06/29/22 21:02 7440-39-3 Cadmium ND mg/kg 0.48 0.12 10 06/26/22 09:00 06/29/22 21:02 7440-43-9 Cadmium ND mg/kg 0.48 0.12 10 06/22/22 09:30 06/22/22 20:30 7440-43-9 Chromium 29.6 mg/kg 0.48 0.12 10 06/22/22 09:30 06/22/22 20:30 7440-47-3 Chromium 38.2 mg/kg 0.48 0.12 10 06/26/22 09:00 06/29/22 21:02 7440-47-3 Lead 5.44 mg/kg 0.48 0.12 10 06/26/22 09:00 06/29/22 21:02 7439-92-1 Lead 8.97 mg/kg 0.48 0.12 10 06/22/22 09:30 06/22/22 20:30 7439-92-1 Selenium ND mg/kg 0.48 0.12 10 06/22/22 09:30 06/22/22 20:30 7782-49-2 Selenium ND mg/kg 0.48 0.12 10 06/26/22 09:00 06/29/22 21:02 7782-49-2 Silver ND mg/kg 0.48 0.12 10 06/26/22 09:00 06/29/22 21:02 7440-22-4 Silver ND mg/kg 0.48 0.12 10 06/22/22 09:30 06/22/22 20:30 7440-22-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: SP-3 Lab ID: 92610504003 Collected: 06/14/22 09:40 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual EPA 7471 B Analytical Method: EPA 7471 B Preparation Method: METHOD Pace Analytical Gulf Coast Mercury 0.018 mg/kg 0.013 0.0054 1 06/22/2214:45 06/23/2211:46 7439-97-6 Mercury 0.025 mg/kg 0.013 0.0053 1 06/26/2212:15 06/27/2212:54 7439-97-6 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND mg/kg 0.40 0.14 1 06/23/22 07:43 06/29/22 15:27 83-32-9 Acenaphthylene ND mg/kg 0.40 0.14 1 06/23/22 07:43 06/29/22 15:27 208-96-8 Aniline ND mg/kg 0.40 0.16 1 06/23/22 07:43 06/29/22 15:27 62-53-3 Anthracene ND mg/kg 0.40 0.13 1 06/23/22 07:43 06/29/22 15:27 120-12-7 Benzo(a)anthracene ND mg/kg 0.40 0.13 1 06/23/22 07:43 06/29/22 15:27 56-55-3 Benzo(a)pyrene ND mg/kg 0.40 0.14 1 06/23/22 07:43 06/29/22 15:27 50-32-8 Benzo(b)fluoranthene ND mg/kg 0.40 0.13 1 06/23/22 07:43 06/29/22 15:27 205-99-2 Benzo(g,h,i)perylene ND mg/kg 0.40 0.16 1 06/23/22 07:43 06/29/22 15:27 191-24-2 Benzo(k)fluoranthene ND mg/kg 0.40 0.14 1 06/23/22 07:43 06/29/22 15:27 207-08-9 Benzoic Acid ND mg/kg 2.0 0.87 1 06/23/22 07:43 06/29/22 15:27 65-85-0 Benzyl alcohol ND mg/kg 0.81 0.31 1 06/23/22 07:43 06/29/22 15:27 100-51-6 4-Bromophenylphenyl ether ND mg/kg 0.40 0.16 1 06/23/22 07:43 06/29/22 15:27 101-55-3 Butylbenzylphthalate ND mg/kg 0.40 0.17 1 06/23/22 07:43 06/29/22 15:27 85-68-7 4-Chloro-3-methyl phenol ND mg/kg 0.81 0.28 1 06/23/22 07:43 06/29/22 15:27 59-50-7 4-Chloroaniline ND mg/kg 0.81 0.32 1 06/23/22 07:43 06/29/22 15:27 106-47-8 bis(2-Chloroethoxy)methane ND mg/kg 0.40 0.17 1 06/23/22 07:43 06/29/22 15:27 111-91-1 bis(2-Chloroethyl) ether ND mg/kg 0.40 0.15 1 06/23/22 07:43 06/29/22 15:27 111-44-4 2-Chloronaphthalene ND mg/kg 0.40 0.16 1 06/23/22 07:43 06/29/22 15:27 91-58-7 2-Chlorophenol ND mg/kg 0.40 0.15 1 06/23/22 07:43 06/29/22 15:27 95-57-8 4-Chlorophenylphenyl ether ND mg/kg 0.40 0.15 1 06/23/22 07:43 06/29/22 15:27 7005-72-3 Chrysene ND mg/kg 0.40 0.15 1 06/23/22 07:43 06/29/22 15:27 218-01-9 Dibenz(a,h)anthracene ND mg/kg 0.40 0.16 1 06/23/22 07:43 06/29/22 15:27 53-70-3 Dibenzofuran ND mg/kg 0.40 0.15 1 06/23/22 07:43 06/29/22 15:27 132-64-9 1,2-Dichlorobenzene ND mg/kg 0.40 0.15 1 06/23/22 07:43 06/29/22 15:27 95-50-1 1,3-Dichlorobenzene ND mg/kg 0.40 0.14 1 06/23/22 07:43 06/29/22 15:27 541-73-1 1,4-Dichlorobenzene ND mg/kg 0.40 0.15 1 06/23/22 07:43 06/29/22 15:27 106-46-7 3,3'-Dichlorobenzidine ND mg/kg 0.81 0.27 1 06/23/22 07:43 06/29/22 15:27 91-94-1 2,4-Dichlorophenol ND mg/kg 0.40 0.16 1 06/23/22 07:43 06/29/22 15:27 120-83-2 Diethylphthalate ND mg/kg 0.40 0.15 1 06/23/22 07:43 06/29/22 15:27 84-66-2 2,4-Dimethylphenol ND mg/kg 0.40 0.17 1 06/23/22 07:43 06/29/22 15:27 105-67-9 Dimethylphthalate ND mg/kg 0.40 0.15 1 06/23/22 07:43 06/29/22 15:27 131-11-3 Di-n-butylphthalate ND mg/kg 0.40 0.14 1 06/23/22 07:43 06/29/22 15:27 84-74-2 4,6-Dinitro-2-methyl phenol ND mg/kg 0.81 0.38 1 06/23/22 07:43 06/29/22 15:27 534-52-1 2,4-Dinitrophenol ND mg/kg 2.0 1.2 1 06/23/22 07:43 06/29/22 15:27 51-28-5 2,4-Dinitrotoluene ND mg/kg 0.40 0.16 1 06/23/22 07:43 06/29/22 15:27 121-14-2 2,6-Dinitrotoluene ND mg/kg 0.40 0.15 1 06/23/22 07:43 06/29/22 15:27 606-20-2 Di-n-octylphthalate ND mg/kg 0.40 0.16 1 06/23/22 07:43 06/29/22 15:27 117-84-0 bis(2- Ethyl hexyl)phthalate ND mg/kg 0.40 0.16 1 06/23/22 07:43 06/29/22 15:27 117-81-7 Fluoranthene ND mg/kg 0.40 0.14 1 06/23/22 07:43 06/29/22 15:27 206-44-0 REPORT OF LABORATORY ANALYSIS IL This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: SP-3 Lab ID: 92610504003 Collected: 06/14/22 09:40 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Fluorene ND mg/kg 0.40 0.14 1 06/23/22 07:43 06/29/22 15:27 86-73-7 Hexachloro-1,3-butadiene ND mg/kg 0.40 0.18 1 06/23/22 07:43 06/29/22 15:27 87-68-3 Hexachlorobenzene ND mg/kg 0.40 0.16 1 06/23/22 07:43 06/29/22 15:27 118-74-1 Hexachlorocyclopentadiene ND mg/kg 0.40 0.23 1 06/23/22 07:43 06/29/22 15:27 77-47-4 v2 Hexachloroethane ND mg/kg 0.40 0.15 1 06/23/22 07:43 06/29/22 15:27 67-72-1 Indeno(1,2,3-cd)pyrene ND mg/kg 0.40 0.16 1 06/23/22 07:43 06/29/22 15:27 193-39-5 Isophorone ND mg/kg 0.40 0.18 1 06/23/22 07:43 06/29/22 15:27 78-59-1 1-Methylnaphthalene ND mg/kg 0.40 0.14 1 06/23/22 07:43 06/29/22 15:27 90-12-0 2-Methylnaphthalene ND mg/kg 0.40 0.16 1 06/23/22 07:43 06/29/22 15:27 91-57-6 2-Methylphenol(o-Cresol) ND mg/kg 0.40 0.17 1 06/23/22 07:43 06/29/22 15:27 95-48-7 3&4-Methyl phenol (m&p Cresol) ND mg/kg 0.40 0.16 1 06/23/22 07:43 06/29/22 15:27 15831-10-4 Naphthalene ND mg/kg 0.40 0.14 1 06/23/22 07:43 06/29/22 15:27 91-20-3 2-Nitroaniline ND mg/kg 2.0 0.33 1 06/23/22 07:43 06/29/22 15:27 88-74-4 3-Nitroaniline ND mg/kg 2.0 0.32 1 06/23/22 07:43 06/29/22 15:27 99-09-2 4-Nitroaniline ND mg/kg 0.81 0.31 1 06/23/22 07:43 06/29/22 15:27 100-01-6 Nitrobenzene ND mg/kg 0.40 0.19 1 06/23/22 07:43 06/29/22 15:27 98-95-3 2-Nitrophenol ND mg/kg 0.40 0.18 1 06/23/22 07:43 06/29/22 15:27 88-75-5 4-Nitrophenol ND mg/kg 2.0 0.78 1 06/23/22 07:43 06/29/22 15:27 100-02-7 N-Nitrosodimethylamine ND mg/kg 0.40 0.14 1 06/23/22 07:43 06/29/22 15:27 62-75-9 N-Nitroso-di-n-propylamine ND mg/kg 0.40 0.15 1 06/23/22 07:43 06/29/22 15:27 621-64-7 N-Nitrosodiphenylamine ND mg/kg 0.40 0.14 1 06/23/22 07:43 06/29/22 15:27 86-30-6 2,2'-Oxybis(1-chloropropane) ND mg/kg 0.40 0.19 1 06/23/22 07:43 06/29/22 15:27 108-60-1 Pentachlorophenol ND mg/kg 0.81 0.40 1 06/23/22 07:43 06/29/22 15:27 87-86-5 Phenanthrene ND mg/kg 0.40 0.13 1 06/23/22 07:43 06/29/22 15:27 85-01-8 Phenol ND mg/kg 0.40 0.18 1 06/23/22 07:43 06/29/22 15:27 108-95-2 Pyrene ND mg/kg 0.40 0.16 1 06/23/22 07:43 06/29/22 15:27 129-00-0 Pyridine ND mg/kg 0.40 0.13 1 06/23/22 07:43 06/29/22 15:27 110-86-1 1,2,4-Trichlorobenzene ND mg/kg 0.40 0.16 1 06/23/22 07:43 06/29/22 15:27 120-82-1 2,4,5-Trichlorophenol ND mg/kg 0.40 0.18 1 06/23/22 07:43 06/29/22 15:27 95-95-4 2,4,6-Trichlorophenol ND mg/kg 0.40 0.17 1 06/23/22 07:43 06/29/22 15:27 88-06-2 Surrogates Nitrobenzene-d5 (S) 63 % 21-130 1 06/23/22 07:43 06/29/22 15:27 4165-60-0 2-Fluorobiphenyl (S) 58 % 19-130 1 06/23/22 07:43 06/29/22 15:27 321-60-8 Terphenyl-d14 (S) 76 % 15-130 1 06/23/22 07:43 06/29/22 15:27 1718-51-0 Phenol-d6 (S) 56 % 18-130 1 06/23/22 07:43 06/29/22 15:27 13127-88-3 2-Fluorophenol (S) 52 % 18-130 1 06/23/22 07:43 06/29/22 15:27 367-12-4 2,4,6-Tribromophenol (S) 67 % 18-130 1 06/23/22 07:43 06/29/22 15:27 118-79-6 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Acetone ND mg/kg 0.23 0.075 1 06/17/22 22:49 06/20/22 16:18 67-64-1 Benzene ND mg/kg 0.012 0.0047 1 06/17/22 22:49 06/20/22 16:18 71-43-2 Bromobenzene ND mg/kg 0.012 0.0038 1 06/17/22 22:49 06/20/22 16:18 108-86-1 Bromochloromethane ND mg/kg 0.012 0.0035 1 06/17/22 22:49 06/20/22 16:18 74-97-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: SP-3 Lab ID: 92610504003 Collected: 06/14/22 09:40 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Bromodichloromethane ND mg/kg 0.012 0.0045 1 06/17/22 22:49 06/20/22 16:18 75-27-4 Bromoform ND mg/kg 0.012 0.0041 1 06/17/22 22:49 06/20/22 16:18 75-25-2 Bromomethane ND mg/kg 0.023 0.019 1 06/17/22 22:49 06/20/22 16:18 74-83-9 2-Butanone (MEK) 0.10J mg/kg 0.23 0.056 1 06/17/22 22:49 06/20/22 16:18 78-93-3 n-Butylbenzene ND mg/kg 0.012 0.0055 1 06/17/22 22:49 06/20/22 16:18 104-51-8 sec-Butylbenzene ND mg/kg 0.012 0.0052 1 06/17/22 22:49 06/20/22 16:18 135-98-8 tert-Butyl benzene ND mg/kg 0.012 0.0042 1 06/17/22 22:49 06/20/22 16:18 98-06-6 Carbon tetrachloride ND mg/kg 0.012 0.0044 1 06/17/22 22:49 06/20/22 16:18 56-23-5 Chlorobenzene ND mg/kg 0.012 0.0023 1 06/17/22 22:49 06/20/22 16:18 108-90-7 Chloroethane ND mg/kg 0.023 0.0091 1 06/17/22 22:49 06/20/22 16:18 75-00-3 Chloroform ND mg/kg 0.012 0.0071 1 06/17/22 22:49 06/20/22 16:18 67-66-3 Chloromethane ND mg/kg 0.023 0.0099 1 06/17/22 22:49 06/20/22 16:18 74-87-3 2-Chlorotoluene ND mg/kg 0.012 0.0042 1 06/17/22 22:49 06/20/22 16:18 95-49-8 4-Chlorotoluene ND mg/kg 0.012 0.0021 1 06/17/22 22:49 06/20/22 16:18 106-43-4 1,2-Dibromo-3-chloropropane ND mg/kg 0.012 0.0046 1 06/17/22 22:49 06/20/22 16:18 96-12-8 Dibromochloromethane ND mg/kg 0.012 0.0066 1 06/17/22 22:49 06/20/22 16:18 124-48-1 1,2-Dibromoethane (EDB) ND mg/kg 0.012 0.0052 1 06/17/22 22:49 06/20/22 16:18 106-93-4 Dibromomethane ND mg/kg 0.012 0.0025 1 06/17/22 22:49 06/20/22 16:18 74-95-3 1,2-Dichlorobenzene ND mg/kg 0.012 0.0042 1 06/17/22 22:49 06/20/22 16:18 95-50-1 1,3-Dichlorobenzene ND mg/kg 0.012 0.0036 1 06/17/22 22:49 06/20/22 16:18 541-73-1 1,4-Dichlorobenzene ND mg/kg 0.012 0.0031 1 06/17/22 22:49 06/20/22 16:18 106-46-7 Dichlorodifluoromethane ND mg/kg 0.023 0.0051 1 06/17/22 22:49 06/20/22 16:18 75-71-8 1,1-Dichloroethane ND mg/kg 0.012 0.0048 1 06/17/22 22:49 06/20/22 16:18 75-34-3 1,2-Dichloroethane ND mg/kg 0.012 0.0078 1 06/17/22 22:49 06/20/22 16:18 107-06-2 1,1-Dichloroethene ND mg/kg 0.012 0.0048 1 06/17/22 22:49 06/20/22 16:18 75-35-4 cis-1,2-Dichloroethene ND mg/kg 0.012 0.0040 1 06/17/22 22:49 06/20/22 16:18 156-59-2 trans-1,2-Dichloroethene ND mg/kg 0.012 0.0041 1 06/17/22 22:49 06/20/22 16:18 156-60-5 1,2-Dichloropropane ND mg/kg 0.012 0.0035 1 06/17/22 22:49 06/20/22 16:18 78-87-5 1,3-Dichloropropane ND mg/kg 0.012 0.0037 1 06/17/22 22:49 06/20/22 16:18 142-28-9 2,2-Dichloropropane ND mg/kg 0.012 0.0038 1 06/17/22 22:49 06/20/22 16:18 594-20-7 1,1-Dichloropropene ND mg/kg 0.012 0.0056 1 06/17/22 22:49 06/20/22 16:18 563-58-6 cis-1,3-Dichloropropene ND mg/kg 0.012 0.0032 1 06/17/22 22:49 06/20/22 16:18 10061-01-5 trans- 1,3-Dichloropropene ND mg/kg 0.012 0.0040 1 06/17/22 22:49 06/20/22 16:18 10061-02-6 Diisopropyl ether ND mg/kg 0.012 0.0032 1 06/17/22 22:49 06/20/22 16:18 108-20-3 Ethylbenzene ND mg/kg 0.012 0.0055 1 06/17/22 22:49 06/20/22 16:18 100-41-4 Hexachloro-1,3-butadiene ND mg/kg 0.023 0.019 1 06/17/22 22:49 06/20/22 16:18 87-68-3 2-Hexanone ND mg/kg 0.12 0.011 1 06/17/22 22:49 06/20/22 16:18 591-78-6 Isopropylbenzene (Cumene) ND mg/kg 0.012 0.0040 1 06/17/22 22:49 06/20/22 16:18 98-82-8 p-Isopropyltoluene ND mg/kg 0.012 0.0058 1 06/17/22 22:49 06/20/22 16:18 99-87-6 Methylene Chloride ND mg/kg 0.047 0.032 1 06/17/22 22:49 06/20/22 16:18 75-09-2 4-Methyl-2-pentanone (MIBK) ND mg/kg 0.12 0.011 1 06/17/22 22:49 06/20/22 16:18 108-10-1 Methyl-tert-butyl ether ND mg/kg 0.012 0.0044 1 06/17/22 22:49 06/20/22 16:18 1634-04-4 Naphthalene ND mg/kg 0.012 0.0062 1 06/17/22 22:49 06/20/22 16:18 91-20-3 n-Propylbenzene ND mg/kg 0.012 0.0042 1 06/17/22 22:49 06/20/22 16:18 103-65-1 REPORT OF LABORATORY ANALYSIS v1 IK v1 v1 v1 v1 This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: SP-3 Lab ID: 92610504003 Collected: 06/14/22 09:40 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Total Solids 2540 G-2011 Total Solids Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 0.012 mg/kg 0.012 0.0031 1 06/17/22 22:49 06/20/22 16:18 100-42-5 ND mg/kg 0.012 0.0045 1 06/17/22 22:49 06/20/22 16:18 630-20-6 ND mg/kg 0.012 0.0031 1 06/17/22 22:49 06/20/22 16:18 79-34-5 ND mg/kg 0.012 0.0037 1 06/17/22 22:49 06/20/22 16:18 127-18-4 ND mg/kg 0.012 0.0033 1 06/17/22 22:49 06/20/22 16:18 108-88-3 ND mg/kg 0.012 0.0095 1 06/17/22 22:49 06/20/22 16:18 87-61-6 ND mg/kg 0.012 0.0099 1 06/17/22 22:49 06/20/22 16:18 120-82-1 ND mg/kg 0.012 0.0061 1 06/17/22 22:49 06/20/22 16:18 71-55-6 ND mg/kg 0.012 0.0039 1 06/17/22 22:49 06/20/22 16:18 79-00-5 ND mg/kg 0.012 0.0030 1 06/17/22 22:49 06/20/22 16:18 79-01-6 ND mg/kg 0.012 0.0065 1 06/17/22 22:49 06/20/22 16:18 75-69-4 ND mg/kg 0.012 0.0059 1 06/17/22 22:49 06/20/22 16:18 96-18-4 ND mg/kg 0.012 0.0032 1 06/17/22 22:49 06/20/22 16:18 95-63-6 ND mg/kg 0.012 0.0039 1 06/17/22 22:49 06/20/22 16:18 108-67-8 ND mg/kg 0.12 0.0085 1 06/17/22 22:49 06/20/22 16:18 108-05-4 ND mg/kg 0.023 0.0060 1 06/17/22 22:49 06/20/22 16:18 75-01-4 ND mg/kg 0.023 0.0067 1 06/17/22 22:49 06/20/22 16:18 1330-20-7 ND mg/kg 0.023 0.0080 1 06/17/22 22:49 06/20/22 16:18 179601-23-1 ND mg/kg 0.012 0.0052 1 06/17/22 22:49 06/20/22 16:18 95-47-6 101 % 70-130 1 06/17/22 22:49 06/20/22 16:18 2037-26-5 100 % 69-134 1 06/17/22 22:49 06/20/22 16:18 460-00-4 103 % 70-130 1 06/17/22 22:49 06/20/22 16:18 17060-07-0 Analytical Method: SW-846 Pace Analytical Services - Charlotte 18.9 % 0.10 0.10 1 06/20/2213:16 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet 70.5 % 1 07/12/2214:30 07/12/2214:43 Wet Chemistry 7199 Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Chromium, Hexavalent ND mg/kg 1.42 0.362 1 07/13/22 14:13 07/15/22 13:30 18540-29-9 Date: 07/21 /2022 05:24 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 Page 23 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: DUP-1 Lab ID: 92610504004 Collected: 06/14/22 00:00 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual OP Pesticides 8141 B Analytical Method: EPA 8141 B Preparation Method: 3546 Pace National - Mt. Juliet Azinphos, methyl (Guthion) ND mg/kg 0.142 0.0451 1 07/11/22 07:27 07/12/22 05:20 86-50-0 H3 Bolstar ND mg/kg 0.142 0.0211 1 07/11/22 07:27 07/12/22 05:20 35400-43-2 H3 Chlorpyrifos ND mg/kg 0.142 0.0222 1 07/11/22 07:27 07/12/22 05:20 2921-88-2 H3 Coumaphos ND mg/kg 0.142 0.0344 1 07/11/22 07:27 07/12/22 05:20 56-72-4 H3 Total Demeton ND mg/kg 0.0992 0.00827 1 07/11/22 07:27 07/12/22 05:20 8065-48-3 H3 Diazinon ND mg/kg 0.142 0.0319 1 07/11/22 07:27 07/12/22 05:20 333-41-5 H3 Dichlorvos ND mg/kg 0.142 0.0425 1 07/11/22 07:27 07/12/22 05:20 62-73-7 H3 Dimethoate ND mg/kg 0.142 0.0473 1 07/11/22 07:27 07/12/22 05:20 60-51-5 H3 Disulfoton ND mg/kg 0.142 0.0360 1 07/11/22 07:27 07/12/22 05:20 298-04-4 H3 EPN (ENT) ND mg/kg 0.142 0.0391 1 07/11/22 07:27 07/12/22 05:20 2104-64-5 H3 Ethoprop ND mg/kg 0.142 0.0167 1 07/11/22 07:27 07/12/22 05:20 13194-48-4 H3 Parathion (Ethyl parathion) ND mg/kg 0.142 0.0232 1 07/11/22 07:27 07/12/22 05:20 56-38-2 H3 Fensulfothion ND mg/kg 0.142 0.0500 1 07/11/22 07:27 07/12/22 05:20 115-90-2 H3 Fenthion ND mg/kg 0.142 0.0188 1 07/11/22 07:27 07/12/22 05:20 55-38-9 H3 Malathion ND mg/kg 0.142 0.0254 1 07/11/22 07:27 07/12/22 05:20 121-75-5 H3 Merphos ND mg/kg 0.142 0.0329 1 07/11/22 07:27 07/12/22 05:20 150-50-5 H3 Methyl parathion ND mg/kg 0.142 0.0288 1 07/11/22 07:27 07/12/22 05:20 298-00-0 H3 Mevinphos ND mg/kg 0.142 0.0326 1 07/11/22 07:27 07/12/22 05:20 7786-34-7 H3 Naled ND mg/kg 0.142 0.0680 1 07/11/22 07:27 07/12/22 05:20 300-76-5 H3 Phorate ND mg/kg 0.142 0.0298 1 07/11/22 07:27 07/12/22 05:20 298-02-2 H3 Ronnel ND mg/kg 0.142 0.0211 1 07/11/22 07:27 07/12/22 05:20 299-84-3 H3 Stirophos (Tetrachlorvinphos) ND mg/kg 0.142 0.0252 1 07/11/22 07:27 07/12/22 05:20 22248-79-9 H3 Sulfotepp (ThiodiphosphoricAc ND mg/kg 0.142 0.0140 1 07/11/22 07:27 07/12/22 05:20 3689-24-5 H3 TEPP ND mg/kg 1.42 0.222 1 07/11/22 07:27 07/12/22 05:20 107-49-3 H3 Tokuthion (Prothiofos) ND mg/kg 0.142 0.0213 1 07/11/22 07:27 07/12/22 05:20 34643-46-4 H3 Trichloronate ND mg/kg 0.142 0.0285 1 07/11/22 07:27 07/12/22 05:20 327-98-0 H3 Surrogates Triphenylphosphate (S) 65.3 % 36.0-121 1 07/11/22 07:27 07/12/22 05:20 115-86-6 Chlorinated Herb. (GC) 8151 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND mg/kg 0.0992 0.00995 1 07/13/22 10:13 07/16/22 00:27 94-75-7 H3 Dalapon ND mg/kg 0.0992 0.0160 1 07/13/22 10:13 07/16/22 00:27 127-20-8 H3 2,4-DB ND mg/kg 0.0992 0.0421 1 07/13/22 10:13 07/16/22 00:27 94-82-6 H3 Dicamba ND mg/kg 0.0992 0.0222 1 07/13/22 10:13 07/16/22 00:27 1918-00-9 H3 Dichloroprop ND mg/kg 0.0992 0.0347 1 07/13/22 10:13 07/16/22 00:27 15165-67-0 H3 Dinoseb ND mg/kg 0.0992 0.00988 1 07/13/22 10:13 07/16/22 00:27 88-85-7 H3 MCPA ND mg/kg 9.21 0.628 1 07/13/22 10:13 07/16/22 00:27 94-74-6 H3 MCPP ND mg/kg 9.21 0.520 1 07/13/22 10:13 07/16/22 00:27 7085-19-0 H3 2,4,5-T ND mg/kg 0.0992 0.0121 1 07/13/22 10:13 07/16/22 00:27 93-76-5 H3 2,4,5-TP (Silvex) ND mg/kg 0.0992 0.0152 1 07/13/22 10:13 07/16/22 00:27 93-72-1 H3 Surrogates 2,4-DCAA (S) 80.0 % 22.0-132 1 07/13/22 10:13 07/16/22 00:27 19719-28-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: DUP-1 Lab ID: 92610504004 Collected: 06/14/22 00:00 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 B Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Aldrin ND mg/kg 0.0025 0.0010 1 06/22/22 16:23 06/27/22 13:32 309-00-2 alpha-BHC ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 13:32 319-84-6 beta-BHC ND mg/kg 0.0025 0.0012 1 06/22/22 16:23 06/27/22 13:32 319-85-7 delta-BHC ND mg/kg 0.0025 0.0013 1 06/22/22 16:23 06/27/22 13:32 319-86-8 gamma-BHC (Lindane) ND mg/kg 0.0025 0.0010 1 06/22/22 16:23 06/27/22 13:32 58-89-9 Chlordane (Technical) ND mg/kg 0.013 0.011 1 06/22/22 16:23 06/27/22 13:32 57-74-9 4,4'-DDD ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 13:32 72-54-8 4,4'-DDE ND mg/kg 0.0025 0.0012 1 06/22/22 16:23 06/27/22 13:32 72-55-9 4,4'-DDT ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 13:32 50-29-3 Dieldrin ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 13:32 60-57-1 Endosulfan I ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 13:32 959-98-8 Endosulfan 11 ND mg/kg 0.0025 0.0011 1 06/22/22 16:23 06/27/22 13:32 33213-65-9 Endosulfan sulfate ND mg/kg 0.0025 0.0014 1 06/22/22 16:23 06/27/22 13:32 1031-07-8 Endrin ND mg/kg 0.0025 0.0012 1 06/22/22 16:23 06/27/22 13:32 72-20-8 Endrin aldehyde ND mg/kg 0.0025 0.0017 1 06/22/22 16:23 06/27/22 13:32 7421-93-4 Endrin ketone ND mg/kg 0.0025 0.0014 1 06/22/22 16:23 06/27/22 13:32 53494-70-5 Heptachlor ND mg/kg 0.0025 0.0012 1 06/22/22 16:23 06/27/22 13:32 76-44-8 Heptachlor epoxide ND mg/kg 0.0025 0.0010 1 06/22/22 16:23 06/27/22 13:32 1024-57-3 Hexachlorobenzene ND mg/kg 0.0025 0.0010 1 06/22/22 16:23 06/27/22 13:32 118-74-1 Methoxychlor ND mg/kg 0.0063 0.0031 1 06/22/22 16:23 06/27/22 13:32 72-43-5 Mirex ND mg/kg 0.0063 0.0028 1 06/22/22 16:23 06/27/22 13:32 2385-85-5 Toxaphene ND mg/kg 0.0088 0.0067 1 06/22/22 16:23 06/27/22 13:32 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 60 % 10-133 1 06/22/22 16:23 06/27/22 13:32 877-09-8 Decachlorobiphenyl (S) 57 % 10-146 1 06/22/22 16:23 06/27/22 13:32 2051-24-3 EPA 6020B Analytical Method: EPA 6020E Preparation Method: EPA 3050B Pace Analytical Gulf Coast Arsenic 1.62 mg/kg 0.47 0.12 10 06/26/22 09:00 06/29/22 21:06 7440-38-2 Arsenic 2.28 mg/kg 0.49 0.12 10 06/22/22 09:30 06/22/22 20:40 7440-38-2 Barium 82.6 mg/kg 0.47 0.12 10 06/26/22 09:00 06/29/22 21:06 7440-39-3 Barium 84.7 mg/kg 0.49 0.12 10 06/22/22 09:30 06/22/22 20:40 7440-39-3 Cadmium ND mg/kg 0.47 0.12 10 06/26/22 09:00 06/29/22 21:06 7440-43-9 Cadmium ND mg/kg 0.49 0.12 10 06/22/22 09:30 06/22/22 20:40 7440-43-9 Chromium 78.2 mg/kg 0.49 0.12 10 06/22/22 09:30 06/22/22 20:40 7440-47-3 Chromium 60.9 mg/kg 0.47 0.12 10 06/26/22 09:00 06/29/22 21:06 7440-47-3 Lead 7.20 mg/kg 0.47 0.12 10 06/26/22 09:00 06/29/22 21:06 7439-92-1 Lead 7.56 mg/kg 0.49 0.12 10 06/22/22 09:30 06/22/22 20:40 7439-92-1 Selenium ND mg/kg 0.49 0.12 10 06/22/22 09:30 06/22/22 20:40 7782-49-2 Selenium ND mg/kg 0.47 0.12 10 06/26/22 09:00 06/29/22 21:06 7782-49-2 Silver ND mg/kg 0.49 0.12 10 06/22/22 09:30 06/22/22 20:40 7440-22-4 Silver ND mg/kg 0.47 0.12 10 06/26/22 09:00 06/29/22 21:06 7440-22-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: DUP-1 Lab ID: 92610504004 Collected: 06/14/22 00:00 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual EPA 7471 B Analytical Method: EPA 7471 B Preparation Method: METHOD Pace Analytical Gulf Coast Mercury 0.033 mg/kg 0.014 0.0057 1 06/26/2212:15 06/27/2212:56 7439-97-6 Mercury 0.046 mg/kg 0.015 0.0059 1 06/22/2214:45 06/23/2211:48 7439-97-6 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:54 83-32-9 Acenaphthylene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:54 208-96-8 Aniline ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:54 62-53-3 Anthracene ND mg/kg 0.41 0.13 1 06/23/22 07:43 06/29/22 15:54 120-12-7 Benzo(a)anthracene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:54 56-55-3 Benzo(a)pyrene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:54 50-32-8 Benzo(b)fluoranthene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:54 205-99-2 Benzo(g,h,i)perylene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:54 191-24-2 Benzo(k)fluoranthene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:54 207-08-9 Benzoic Acid ND mg/kg 2.0 0.87 1 06/23/22 07:43 06/29/22 15:54 65-85-0 Benzyl alcohol ND mg/kg 0.81 0.31 1 06/23/22 07:43 06/29/22 15:54 100-51-6 4-Bromophenylphenyl ether ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:54 101-55-3 Butylbenzylphthalate ND mg/kg 0.41 0.17 1 06/23/22 07:43 06/29/22 15:54 85-68-7 4-Chloro-3-methyl phenol ND mg/kg 0.81 0.29 1 06/23/22 07:43 06/29/22 15:54 59-50-7 4-Chloroaniline ND mg/kg 0.81 0.32 1 06/23/22 07:43 06/29/22 15:54 106-47-8 bis(2-Chloroethoxy)methane ND mg/kg 0.41 0.17 1 06/23/22 07:43 06/29/22 15:54 111-91-1 bis(2-Chloroethyl) ether ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:54 111-44-4 2-Chloronaphthalene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:54 91-58-7 2-Chlorophenol ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:54 95-57-8 4-Chlorophenylphenyl ether ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:54 7005-72-3 Chrysene ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:54 218-01-9 Dibenz(a,h)anthracene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:54 53-70-3 Dibenzofuran ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:54 132-64-9 1,2-Dichlorobenzene ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:54 95-50-1 1,3-Dichlorobenzene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:54 541-73-1 1,4-Dichlorobenzene ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:54 106-46-7 3,3'-Dichlorobenzidine ND mg/kg 0.81 0.27 1 06/23/22 07:43 06/29/22 15:54 91-94-1 2,4-Dichlorophenol ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:54 120-83-2 Diethylphthalate ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:54 84-66-2 2,4-Dimethylphenol ND mg/kg 0.41 0.17 1 06/23/22 07:43 06/29/22 15:54 105-67-9 Dimethylphthalate ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:54 131-11-3 Di-n-butylphthalate ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:54 84-74-2 4,6-Dinitro-2-methyl phenol ND mg/kg 0.81 0.38 1 06/23/22 07:43 06/29/22 15:54 534-52-1 2,4-Dinitrophenol ND mg/kg 2.0 1.3 1 06/23/22 07:43 06/29/22 15:54 51-28-5 2,4-Dinitrotoluene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:54 121-14-2 2,6-Dinitrotoluene ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:54 606-20-2 Di-n-octylphthalate ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:54 117-84-0 bis(2- Ethyl hexyl)phthalate ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:54 117-81-7 Fluoranthene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:54 206-44-0 REPORT OF LABORATORY ANALYSIS IL This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: DUP-1 Lab ID: 92610504004 Collected: 06/14/22 00:00 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Fluorene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:54 86-73-7 Hexachloro-1,3-butadiene ND mg/kg 0.41 0.18 1 06/23/22 07:43 06/29/22 15:54 87-68-3 Hexachlorobenzene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:54 118-74-1 Hexachlorocyclopentadiene ND mg/kg 0.41 0.23 1 06/23/22 07:43 06/29/22 15:54 77-47-4 v2 Hexachloroethane ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:54 67-72-1 Indeno(1,2,3-cd)pyrene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:54 193-39-5 Isophorone ND mg/kg 0.41 0.18 1 06/23/22 07:43 06/29/22 15:54 78-59-1 1-Methylnaphthalene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:54 90-12-0 2-Methylnaphthalene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:54 91-57-6 2-Methylphenol(o-Cresol) ND mg/kg 0.41 0.17 1 06/23/22 07:43 06/29/22 15:54 95-48-7 3&4-Methyl phenol (m&p Cresol) ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:54 15831-10-4 Naphthalene ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:54 91-20-3 2-Nitroaniline ND mg/kg 2.0 0.33 1 06/23/22 07:43 06/29/22 15:54 88-74-4 3-Nitroaniline ND mg/kg 2.0 0.32 1 06/23/22 07:43 06/29/22 15:54 99-09-2 4-Nitroaniline ND mg/kg 0.81 0.31 1 06/23/22 07:43 06/29/22 15:54 100-01-6 Nitrobenzene ND mg/kg 0.41 0.19 1 06/23/22 07:43 06/29/22 15:54 98-95-3 2-Nitrophenol ND mg/kg 0.41 0.18 1 06/23/22 07:43 06/29/22 15:54 88-75-5 4-Nitrophenol ND mg/kg 2.0 0.78 1 06/23/22 07:43 06/29/22 15:54 100-02-7 N-Nitrosodimethylamine ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:54 62-75-9 N-Nitroso-di-n-propylamine ND mg/kg 0.41 0.15 1 06/23/22 07:43 06/29/22 15:54 621-64-7 N-Nitrosodiphenylamine ND mg/kg 0.41 0.14 1 06/23/22 07:43 06/29/22 15:54 86-30-6 2,2'-Oxybis(1-chloropropane) ND mg/kg 0.41 0.19 1 06/23/22 07:43 06/29/22 15:54 108-60-1 Pentachlorophenol ND mg/kg 0.81 0.40 1 06/23/22 07:43 06/29/22 15:54 87-86-5 Phenanthrene ND mg/kg 0.41 0.13 1 06/23/22 07:43 06/29/22 15:54 85-01-8 Phenol ND mg/kg 0.41 0.18 1 06/23/22 07:43 06/29/22 15:54 108-95-2 Pyrene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:54 129-00-0 Pyridine ND mg/kg 0.41 0.13 1 06/23/22 07:43 06/29/22 15:54 110-86-1 1,2,4-Trichlorobenzene ND mg/kg 0.41 0.16 1 06/23/22 07:43 06/29/22 15:54 120-82-1 2,4,5-Trichlorophenol ND mg/kg 0.41 0.19 1 06/23/22 07:43 06/29/22 15:54 95-95-4 2,4,6-Trichlorophenol ND mg/kg 0.41 0.17 1 06/23/22 07:43 06/29/22 15:54 88-06-2 Surrogates Nitrobenzene-d5 (S) 76 % 21-130 1 06/23/22 07:43 06/29/22 15:54 4165-60-0 2-Fluorobiphenyl (S) 70 % 19-130 1 06/23/22 07:43 06/29/22 15:54 321-60-8 Terphenyl-d14 (S) 85 % 15-130 1 06/23/22 07:43 06/29/22 15:54 1718-51-0 Phenol-d6 (S) 68 % 18-130 1 06/23/22 07:43 06/29/22 15:54 13127-88-3 2-Fluorophenol (S) 62 % 18-130 1 06/23/22 07:43 06/29/22 15:54 367-12-4 2,4,6-Tribromophenol (S) 79 % 18-130 1 06/23/22 07:43 06/29/22 15:54 118-79-6 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Acetone ND mg/kg 0.16 0.051 1 06/17/22 22:49 06/20/22 16:35 67-64-1 Benzene ND mg/kg 0.0079 0.0031 1 06/17/22 22:49 06/20/22 16:35 71-43-2 Bromobenzene ND mg/kg 0.0079 0.0026 1 06/17/22 22:49 06/20/22 16:35 108-86-1 Bromochloromethane ND mg/kg 0.0079 0.0023 1 06/17/22 22:49 06/20/22 16:35 74-97-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: DUP-1 Lab ID: 92610504004 Collected: 06/14/22 00:00 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Bromodichloromethane ND mg/kg 0.0079 0.0030 1 06/17/22 22:49 06/20/22 16:35 75-27-4 Bromoform ND mg/kg 0.0079 0.0028 1 06/17/22 22:49 06/20/22 16:35 75-25-2 Bromomethane ND mg/kg 0.016 0.012 1 06/17/22 22:49 06/20/22 16:35 74-83-9 2-Butanone (MEK) 0.071J mg/kg 0.16 0.038 1 06/17/22 22:49 06/20/22 16:35 78-93-3 n-Butylbenzene ND mg/kg 0.0079 0.0037 1 06/17/22 22:49 06/20/22 16:35 104-51-8 sec-Butylbenzene ND mg/kg 0.0079 0.0035 1 06/17/22 22:49 06/20/22 16:35 135-98-8 tert-Butyl benzene ND mg/kg 0.0079 0.0028 1 06/17/22 22:49 06/20/22 16:35 98-06-6 Carbon tetrachloride ND mg/kg 0.0079 0.0030 1 06/17/22 22:49 06/20/22 16:35 56-23-5 Chlorobenzene ND mg/kg 0.0079 0.0015 1 06/17/22 22:49 06/20/22 16:35 108-90-7 Chloroethane ND mg/kg 0.016 0.0061 1 06/17/22 22:49 06/20/22 16:35 75-00-3 Chloroform ND mg/kg 0.0079 0.0048 1 06/17/22 22:49 06/20/22 16:35 67-66-3 Chloromethane ND mg/kg 0.016 0.0066 1 06/17/22 22:49 06/20/22 16:35 74-87-3 2-Chlorotoluene ND mg/kg 0.0079 0.0028 1 06/17/22 22:49 06/20/22 16:35 95-49-8 4-Chlorotoluene ND mg/kg 0.0079 0.0014 1 06/17/22 22:49 06/20/22 16:35 106-43-4 1,2-Dibromo-3-chloropropane ND mg/kg 0.0079 0.0031 1 06/17/22 22:49 06/20/22 16:35 96-12-8 Dibromochloromethane ND mg/kg 0.0079 0.0044 1 06/17/22 22:49 06/20/22 16:35 124-48-1 1,2-Dibromoethane (EDB) ND mg/kg 0.0079 0.0035 1 06/17/22 22:49 06/20/22 16:35 106-93-4 Dibromomethane ND mg/kg 0.0079 0.0017 1 06/17/22 22:49 06/20/22 16:35 74-95-3 1,2-Dichlorobenzene ND mg/kg 0.0079 0.0028 1 06/17/22 22:49 06/20/22 16:35 95-50-1 1,3-Dichlorobenzene ND mg/kg 0.0079 0.0024 1 06/17/22 22:49 06/20/22 16:35 541-73-1 1,4-Dichlorobenzene ND mg/kg 0.0079 0.0021 1 06/17/22 22:49 06/20/22 16:35 106-46-7 Dichlorodifluoromethane ND mg/kg 0.016 0.0034 1 06/17/22 22:49 06/20/22 16:35 75-71-8 1,1-Dichloroethane ND mg/kg 0.0079 0.0033 1 06/17/22 22:49 06/20/22 16:35 75-34-3 1,2-Dichloroethane ND mg/kg 0.0079 0.0052 1 06/17/22 22:49 06/20/22 16:35 107-06-2 1,1-Dichloroethene ND mg/kg 0.0079 0.0033 1 06/17/22 22:49 06/20/22 16:35 75-35-4 cis-1,2-Dichloroethene ND mg/kg 0.0079 0.0027 1 06/17/22 22:49 06/20/22 16:35 156-59-2 trans-1,2-Dichloroethene ND mg/kg 0.0079 0.0028 1 06/17/22 22:49 06/20/22 16:35 156-60-5 1,2-Dichloropropane ND mg/kg 0.0079 0.0024 1 06/17/22 22:49 06/20/22 16:35 78-87-5 1,3-Dichloropropane ND mg/kg 0.0079 0.0025 1 06/17/22 22:49 06/20/22 16:35 142-28-9 2,2-Dichloropropane ND mg/kg 0.0079 0.0026 1 06/17/22 22:49 06/20/22 16:35 594-20-7 1,1-Dichloropropene ND mg/kg 0.0079 0.0038 1 06/17/22 22:49 06/20/22 16:35 563-58-6 cis-1,3-Dichloropropene ND mg/kg 0.0079 0.0021 1 06/17/22 22:49 06/20/22 16:35 10061-01-5 trans- 1,3-Dichloropropene ND mg/kg 0.0079 0.0027 1 06/17/22 22:49 06/20/22 16:35 10061-02-6 Diisopropyl ether ND mg/kg 0.0079 0.0021 1 06/17/22 22:49 06/20/22 16:35 108-20-3 Ethylbenzene ND mg/kg 0.0079 0.0037 1 06/17/22 22:49 06/20/22 16:35 100-41-4 Hexachloro-1,3-butadiene ND mg/kg 0.016 0.013 1 06/17/22 22:49 06/20/22 16:35 87-68-3 2-Hexanone ND mg/kg 0.079 0.0076 1 06/17/22 22:49 06/20/22 16:35 591-78-6 Isopropylbenzene (Cumene) ND mg/kg 0.0079 0.0027 1 06/17/22 22:49 06/20/22 16:35 98-82-8 p-Isopropyltoluene ND mg/kg 0.0079 0.0039 1 06/17/22 22:49 06/20/22 16:35 99-87-6 Methylene Chloride ND mg/kg 0.032 0.022 1 06/17/22 22:49 06/20/22 16:35 75-09-2 4-Methyl-2-pentanone (MIBK) ND mg/kg 0.079 0.0076 1 06/17/22 22:49 06/20/22 16:35 108-10-1 Methyl-tert-butyl ether ND mg/kg 0.0079 0.0030 1 06/17/22 22:49 06/20/22 16:35 1634-04-4 Naphthalene ND mg/kg 0.0079 0.0041 1 06/17/22 22:49 06/20/22 16:35 91-20-3 n-Propylbenzene ND mg/kg 0.0079 0.0028 1 06/17/22 22:49 06/20/22 16:35 103-65-1 REPORT OF LABORATORY ANALYSIS v1 IK v1 v1 v1 v1 This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610504 Sample: DUP-1 Lab ID: 92610504004 Collected: 06/14/22 00:00 Received: 06/17/22 10:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Total Solids 2540 G-2011 Total Solids Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 0.0074J mg/kg 0.0079 0.0021 1 06/17/22 22:49 06/20/22 16:35 100-42-5 ND mg/kg 0.0079 0.0030 1 06/17/22 22:49 06/20/22 16:35 630-20-6 ND mg/kg 0.0079 0.0021 1 06/17/22 22:49 06/20/22 16:35 79-34-5 ND mg/kg 0.0079 0.0025 1 06/17/22 22:49 06/20/22 16:35 127-18-4 ND mg/kg 0.0079 0.0022 1 06/17/22 22:49 06/20/22 16:35 108-88-3 ND mg/kg 0.0079 0.0064 1 06/17/22 22:49 06/20/22 16:35 87-61-6 ND mg/kg 0.0079 0.0066 1 06/17/22 22:49 06/20/22 16:35 120-82-1 ND mg/kg 0.0079 0.0041 1 06/17/22 22:49 06/20/22 16:35 71-55-6 ND mg/kg 0.0079 0.0026 1 06/17/22 22:49 06/20/22 16:35 79-00-5 ND mg/kg 0.0079 0.0020 1 06/17/22 22:49 06/20/22 16:35 79-01-6 ND mg/kg 0.0079 0.0043 1 06/17/22 22:49 06/20/22 16:35 75-69-4 ND mg/kg 0.0079 0.0040 1 06/17/22 22:49 06/20/22 16:35 96-18-4 ND mg/kg 0.0079 0.0022 1 06/17/22 22:49 06/20/22 16:35 95-63-6 ND mg/kg 0.0079 0.0027 1 06/17/22 22:49 06/20/22 16:35 108-67-8 ND mg/kg 0.079 0.0057 1 06/17/22 22:49 06/20/22 16:35 108-05-4 ND mg/kg 0.016 0.0040 1 06/17/22 22:49 06/20/22 16:35 75-01-4 ND mg/kg 0.016 0.0045 1 06/17/22 22:49 06/20/22 16:35 1330-20-7 ND mg/kg 0.016 0.0054 1 06/17/22 22:49 06/20/22 16:35 179601-23-1 ND mg/kg 0.0079 0.0035 1 06/17/22 22:49 06/20/22 16:35 95-47-6 100 % 70-130 1 06/17/22 22:49 06/20/22 16:35 2037-26-5 101 % 69-134 1 06/17/22 22:49 06/20/22 16:35 460-00-4 104 % 70-130 1 06/17/22 22:49 06/20/22 16:35 17060-07-0 Analytical Method: SW-846 Pace Analytical Services - Charlotte 19.7 % 0.10 0.10 1 06/20/2213:16 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet 70.6 % 1 07/12/2214:30 07/12/2214:43 Wet Chemistry 7199 Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Chromium, Hexavalent ND mg/kg 1.42 0.361 1 07/13/22 14:13 07/15/22 13:36 18540-29-9 Date: 07/21 /2022 05:24 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 Page 29 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 QC Batch: 1892644 Analysis Method: EPA 8141 B QC Batch Method: 3546 Analysis Description: OP Pesticides 8141 B Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 METHOD BLANK: R3813748-1 Matrix: Solid Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 Blank Reporting Parameter Units Result Limit MDL Analyzed Azinphos, methyl (Guthion) mg/kg ND 0.100 0.0318 07/11/22 23:17 Bolstar mg/kg ND 0.100 0.0149 07/11/22 23:17 Chlorpyrifos mg/kg ND 0.100 0.0157 07/11/22 23:17 Coumaphos mg/kg ND 0.100 0.0243 07/11/22 23:17 Total Demeton mg/kg ND 0.0700 0.00584 07/11/22 23:17 Diazinon mg/kg ND 0.100 0.0225 07/11/22 23:17 Dichlorvos mg/kg ND 0.100 0.0300 07/11/22 23:17 Dimethoate mg/kg ND 0.100 0.0334 07/11/22 23:17 Disulfoton mg/kg ND 0.100 0.0254 07/11/22 23:17 EPN (ENT) mg/kg ND 0.100 0.0276 07/11/22 23:17 Ethoprop mg/kg ND 0.100 0.0118 07/11/22 23:17 Parathion (Ethyl parathion) mg/kg ND 0.100 0.0164 07/11/22 23:17 Fensulfothion mg/kg ND 0.100 0.0353 07/11/22 23:17 Fenthion mg/kg ND 0.100 0.0133 07/11/22 23:17 Malathion mg/kg ND 0.100 0.0179 07/11/22 23:17 Merphos mg/kg ND 0.100 0.0232 07/11/22 23:17 Methyl parathion mg/kg ND 0.100 0.0203 07/11/22 23:17 Mevinphos mg/kg ND 0.100 0.0230 07/11/22 23:17 Naled mg/kg ND 0.100 0.0480 07/11/22 23:17 Phorate mg/kg ND 0.100 0.0210 07/11/22 23:17 Ronnel mg/kg ND 0.100 0.0149 07/11/22 23:17 Stirophos (Tetrachlorvinphos) mg/kg ND 0.100 0.0178 07/11/22 23:17 Sulfotepp (Thiodiphosphoric Ac mg/kg ND 0.100 0.00986 07/11/22 23:17 TEPP mg/kg ND 1.00 0.157 07/11/22 23:17 Tokuthion (Prothiofos) mg/kg ND 0.100 0.0150 07/11/22 23:17 Trichloronate mg/kg ND 0.100 0.0201 07/11/22 23:17 Triphenyl phosphate (S) % 94.9 36.0-121 07/11/22 23:17 Qualifiers LABORATORY CONTROL SAMPLE: Parameter R3813748-2 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Azinphos, methyl (Guthion) mg/kg 0.333 0.322 96.7 58.0-125 Bolstar mg/kg 0.333 0.316 94.9 64.0-120 Chlorpyrifos mg/kg 0.333 0.312 93.7 62.0-120 Coumaphos mg/kg 0.333 0.319 95.8 60.0-120 Total Demeton mg/kg 0.167 0.149 89.2 59.0-120 Diazinon mg/kg 0.333 0.275 82.6 49.0-120 Dichlorvos mg/kg 0.333 0.234 70.3 37.0-120 Dimethoate mg/kg 0.333 0.299 89.8 46.0-127 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 LABORATORY CONTROL SAMPLE: R3813748-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Disulfoton mg/kg 0.333 0.293 88.0 60.0-121 EPN (ENT) mg/kg 0.333 0.309 92.8 60.0-121 Ethoprop mg/kg 0.333 0.313 94.0 59.0-120 Parathion (Ethyl parathion) mg/kg 0.333 0.309 92.8 62.0-120 Fensulfothion mg/kg 0.333 0.307 92.2 58.0-123 Fenthion mg/kg 0.333 0.317 95.2 61.0-121 Malathion mg/kg 0.333 0.305 91.6 59.0-120 Merphos mg/kg 0.333 0.282 84.7 59.0-120 Methyl parathion mg/kg 0.333 0.305 91.6 63.0-120 Mevinphos mg/kg 0.333 0.232 69.7 50.0-120 Naled mg/kg 0.333 0.229 68.8 10.0-125 Phorate mg/kg 0.333 0.290 87.1 60.0-120 Ronnel mg/kg 0.333 0.300 90.1 62.0-120 Stirophos (Tetrachlorvinphos) mg/kg 0.333 0.302 90.7 62.0-120 Sulfotepp (ThiodiphosphoricAc mg/kg 0.333 0.312 93.7 62.0-122 TEPP mg/kg 3.33 0.928 27.9 10.0-135 Tokuthion (Prothiofos) mg/kg 0.333 0.313 94.0 63.0-120 Trichloronate mg/kg 0.333 0.303 91.0 62.0-120 Triphenyl phosphate (S) % 96.7 36.0-121 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3813748-3 R3813748-4 MS MSD L1512002-05 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Azinphos, methyl (Guthion) mg/kg ND 0.335 0.335 0.311 0.316 92.8 94.3 10.0-160 1.61 22 Bolstar mg/kg ND 0.335 0.335 0.315 0.313 94.0 93.4 10.0-151 0.641 20 Chlorpyrifos mg/kg ND 0.335 0.335 0.308 0.305 91.9 91.0 12.0-149 0.985 20 Coumaphos mg/kg ND 0.335 0.335 0.312 0.314 93.1 93.7 10.0-160 0.643 22 Total Demeton mg/kg ND 0.168 0.168 0.126 0.129 74.9 76.6 10.0-160 2.37 23 Diazinon mg/kg ND 0.335 0.335 0.285 0.281 85.0 83.8 11.0-157 1.42 20 Dichlorvos mg/kg ND 0.335 0.335 0.224 0.228 67.0 68.2 10.0-160 1.78 24 Dimethoate mg/kg ND 0.335 0.335 0.193 0.232 57.7 69.1 10.0-150 18.0 27 Disulfoton mg/kg ND 0.335 0.335 0.289 0.284 86.2 84.7 12.0-155 1.76 20 EPN (ENT) mg/kg ND 0.335 0.335 0.311 0.306 92.8 91.3 10.0-159 1.63 20 Ethoprop mg/kg ND 0.335 0.335 0.291 0.299 86.8 89.2 11.0-156 2.73 20 Parathion (Ethyl parathion) mg/kg ND 0.335 0.335 0.305 0.300 91.0 89.5 10.0-147 1.66 20 Fensulfothion mg/kg ND 0.335 0.335 0.208 0.255 62.2 76.0 10.0-157 20.0 27 Fenthion mg/kg ND 0.335 0.335 0.310 0.310 92.5 92.5 13.0-155 0.00 20 Malathion mg/kg ND 0.335 0.335 0.298 0.296 88.9 88.3 13.0-137 0.678 21 Merphos mg/kg ND 0.335 0.335 0.271 0.281 80.8 83.8 10.0-147 3.65 26 Methyl parathion mg/kg ND 0.335 0.335 0.300 0.295 89.5 88.0 10.0-150 1.69 21 Mevinphos mg/kg ND 0.335 0.335 0.166 0.182 49.5 54.4 10.0-158 9.25 24 Naled mg/kg ND 0.335 0.335 0.150 0.142 44.7 42.3 10.0-137 5.52 40 Phorate mg/kg ND 0.335 0.335 0.280 0.278 83.5 82.9 13.0-154 0.722 20 Ronnel mg/kg ND 0.335 0.335 0.307 0.298 91.6 88.9 14.0-149 3.00 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3813748-3 R3813748-4 MS MSD L1512002-05 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Stirophos mg/kg ND 0.335 0.335 0.290 0.292 86.5 87.1 10.0-150 0.692 20 (Tetrachlorvinphos) Sulfotepp mg/kg ND 0.335 0.335 0.303 0.298 90.4 88.9 10.0-160 1.68 20 (Thiodiphosphoric Ac TEPP mg/kg ND 3.35 3.35 U U 1.71 4.38 10.0-142 87.7 28 ML, R1 Tokuthion (Prothiofos) mg/kg ND 0.335 0.335 0.312 0.307 93.1 91.6 12.0-153 1.63 20 Trichloronate mg/kg ND 0.335 0.335 0.300 0.299 89.5 89.2 12.0-152 0.336 20 Triphenyl phosphate (S) % 90.4 89.5 36.0-121 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 QC Batch: 1894221 Analysis Method: EPA 8151 QC Batch Method: 8151A Analysis Description: Chlorinated Herb. (GC) 8151 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 METHOD BLANK: R3815521-1 Matrix: Solid Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 2,4-D mg/kg ND 0.0700 0.00702 07/14/22 19:36 Dalapon mg/kg ND 0.0700 0.0113 07/14/22 19:36 2,4-DB mg/kg ND 0.0700 0.0297 07/14/22 19:36 Dicamba mg/kg ND 0.0700 0.0157 07/14/22 19:36 Dichloroprop mg/kg ND 0.0700 0.0245 07/14/22 19:36 Dinoseb mg/kg ND 0.0700 0.00697 07/14/22 19:36 MCPA mg/kg ND 6.50 0.443 07/14/22 19:36 MCPP mg/kg ND 6.50 0.367 07/14/22 19:36 2,4,5-T mg/kg ND 0.0700 0.00852 07/14/22 19:36 2,4,5-TP (Silvex) mg/kg ND 0.0700 0.0107 07/14/22 19:36 2,4-DCAA (S) % 61.7 22.0-132 07/14/22 19:36 LABORATORY CONTROL SAMPLE: R3815521-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 2,4-D mg/kg 0.167 0.136 81.4 40.0-120 Dalapon mg/kg 0.167 0.117 70.1 15.0-120 2,4-DB mg/kg 0.167 0.119 71.3 25.0-143 Dicamba mg/kg 0.167 0.133 79.6 43.0-120 Dichloroprop mg/kg 0.167 0.144 86.2 32.0-129 Dinoseb mg/kg 0.167 0.124 74.3 10.0-120 MCPA mg/kg 16.7 12.9 77.2 31.0-121 MCPP mg/kg 16.7 10.2 61.1 28.0-133 2,4,5-T mg/kg 0.167 0.114 68.3 41.0-120 2,4,5-TP (Silvex) mg/kg 0.167 0.120 71.9 42.0-120 2,4-DCAA (S) % 65.3 22.0-132 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3815521-3 R3815521-4 MS MSD L1511677-01 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 2,4-D mg/kg ND 0.189 0.187 0.0838 0.0574 44.4 30.7 10.0-160 37.5 24 R1 Dalapon mg/kg ND 0.189 0.187 0.0207 0.0139 11.0 7.42 10.0-121 39.7 27 ML,R1 2,4-DB mg/kg ND 0.189 0.187 0.112 0.106 59.2 57.0 10.0-160 5.04 22 Dicamba mg/kg ND 0.189 0.187 0.0665 0.0460 35.2 24.7 10.0-154 36.4 21 R1 Dichloroprop mg/kg ND 0.189 0.187 0.119 0.0946 63.0 50.7 10.0-158 22.9 20 R1 Dinoseb mg/kg ND 0.189 0.187 0.129 0.126 68.5 67.5 10.0-120 2.69 40 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3815521-3 R3815521-4 MS MSD L1511677-01 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual MCPA mg/kg ND 18.9 18.7 10.4 8.53 55.2 45.7 10.0-160 19.9 40 MCPP mg/kg ND 18.9 18.7 9.40 7.88 49.8 42.2 10.0-160 17.6 40 2,4,5-T mg/kg ND 0.189 0.187 0.0913 0.0666 48.3 35.7 10.0-157 31.2 20 R1 2,4,5-TP (Silvex) mg/kg ND 0.189 0.187 0.0914 0.0851 48.4 45.6 10.0-156 7.14 20 2,4-DCAA (S) % 53.2 47.9 22.0-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 QC Batch: 743660 Analysis Method: EPA 6020B QC Batch Method: EPA 3050B Analysis Description: EPA 6020 Laboratory: Pace Analytical Gulf Coast Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 METHOD BLANK: 2361203 Matrix: Solid Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Arsenic mg/kg ND 0.040 0.010 06/22/22 20:12 Barium mg/kg ND 0.040 0.010 06/22/22 20:12 Cadmium mg/kg ND 0.040 0.010 06/22/22 20:12 Chromium mg/kg ND 0.040 0.010 06/22/22 20:12 Lead mg/kg ND 0.040 0.010 06/22/22 20:12 Selenium mg/kg ND 0.040 0.010 06/22/22 20:12 Silver mg/kg ND 0.040 0.010 06/22/22 20:12 LABORATORY CONTROL SAMPLE: Parameter 2361205 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Arsenic mg/kg 2 1.78 89 80-120 Barium mg/kg 2 2.04 102 80-120 Cadmium mg/kg 2 1.84 92 80-120 Chromium mg/kg 2 2.05 103 80-120 Lead mg/kg 2 2.07 103 80-120 Selenium mg/kg 0.4 0.34 85 80-120 Silver mg/kg 2 1.97 98 80-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 QC Batch: 743891 Analysis Method: EPA 6020B QC Batch Method: EPA 3050B Analysis Description: EPA 6020 Laboratory: Pace Analytical Gulf Coast Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 METHOD BLANK: 2362684 Matrix: Solid Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Arsenic mg/kg ND 0.040 0.010 06/29/2219:52 P8 Barium mg/kg ND 0.040 0.010 06/29/2219:52 Cadmium mg/kg ND 0.040 0.010 06/29/2219:52 Chromium mg/kg ND 0.040 0.010 06/29/2219:52 Lead mg/kg ND 0.040 0.010 06/29/2219:52 Selenium mg/kg ND 0.040 0.010 06/29/2219:52 Silver mg/kg ND 0.040 0.010 06/29/2219:52 LABORATORY CONTROL SAMPLE & LCSD: Parameter 2362686 Units Spike Conc. 2362685 LCS LCSD Result Result LCS LCSD % Rec % Rec % Rec Limits RPD Max RPD Qualifiers Arsenic mg/kg 2 2.08 2.03 104 101 80-120 3 20 Barium mg/kg 2 2.00 2.21 100 110 80-120 10 20 Cadmium mg/kg 2 1.91 2.11 96 105 80-120 10 20 Chromium mg/kg 2 2.07 2.04 104 102 80-120 2 20 Lead mg/kg 2 2.07 2.30 104 115 80-120 10 20 Selenium mg/kg 0.4 0.41 0.41 102 102 80-120 0 20 Silver mg/kg 2 2.07 2.28 103 114 80-120 10 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 QC Batch: 743747 Analysis Method: EPA 7471 B QC Batch Method: METHOD Analysis Description: EPA 7471 B Laboratory: Pace Analytical Gulf Coast Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 METHOD BLANK: 2361731 Matrix: Solid Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Mercury mg/kg ND 0.010 0.0040 06/23/2211:14 LABORATORY CONTROL SAMPLE: 2361732 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury mg/kg 0.25 0.27 107 80-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 QC Batch: 744047 Analysis Method: EPA 7471 B QC Batch Method: METHOD Analysis Description: EPA 7471 B Laboratory: Pace Analytical Gulf Coast Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 METHOD BLANK: 2363602 Matrix: Solid Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Mercury mg/kg ND 0.010 0.0040 06/27/2212:44 P8 LABORATORY CONTROL SAMPLE & LCSD: 2363604 2363603 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Mercury mg/kg 0.25 0.23 0.24 90 95 80-120 5 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 QC Batch: 705419 Analysis Method: EPA 8260D QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 METHOD BLANK: 3680948 Matrix: Solid Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 Blank Reporting Parameter Units Result Limit MDL Analyzed 1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 0.0019 06/20/22 12:45 1,1,1-Trichloroethane mg/kg ND 0.0050 0.0026 06/20/22 12:45 1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 0.0013 06/20/22 12:45 1,1,2-Trichloroethane mg/kg ND 0.0050 0.0017 06/20/22 12:45 1,1-Dichloroethane mg/kg ND 0.0050 0.0021 06/20/22 12:45 1,1-Dichloroethene mg/kg ND 0.0050 0.0021 06/20/22 12:45 1,1-Dichloropropene mg/kg ND 0.0050 0.0024 06/20/22 12:45 1,2,3-Trichlorobenzene mg/kg ND 0.0050 0.0040 06/20/22 12:45 1,2,3-Trichloropropane mg/kg ND 0.0050 0.0025 06/20/22 12:45 1,2,4-Trichlorobenzene mg/kg ND 0.0050 0.0042 06/20/22 12:45 1,2,4-Trimethylbenzene mg/kg ND 0.0050 0.0014 06/20/22 12:45 1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 0.0019 06/20/22 12:45 1,2-Dibromoethane (EDB) mg/kg ND 0.0050 0.0022 06/20/22 12:45 1,2-Dichlorobenzene mg/kg ND 0.0050 0.0018 06/20/22 12:45 1,2-Dichloroethane mg/kg ND 0.0050 0.0033 06/20/22 12:45 1,2-Dichloropropane mg/kg ND 0.0050 0.0015 06/20/22 12:45 1,3,5-Trimethylbenzene mg/kg ND 0.0050 0.0017 06/20/22 12:45 1,3-Dichlorobenzene mg/kg ND 0.0050 0.0016 06/20/22 12:45 1,3-Dichloropropane mg/kg ND 0.0050 0.0016 06/20/22 12:45 1,4-Dichlorobenzene mg/kg ND 0.0050 0.0013 06/20/22 12:45 2,2-Dichloropropane mg/kg ND 0.0050 0.0016 06/20/22 12:45 2-Butanone (MEK) mg/kg ND 0.10 0.024 06/20/22 12:45 2-Chlorotoluene mg/kg ND 0.0050 0.0018 06/20/22 12:45 2-Hexanone mg/kg ND 0.050 0.0048 06/20/22 12:45 4-Chlorotoluene mg/kg ND 0.0050 0.00088 06/20/22 12:45 4-Methyl-2-pentanone (MIBK) mg/kg ND 0.050 0.0048 06/20/22 12:45 Acetone mg/kg ND 0.10 0.032 06/20/22 12:45 Benzene mg/kg ND 0.0050 0.0020 06/20/22 12:45 Bromobenzene mg/kg ND 0.0050 0.0016 06/20/22 12:45 Bromochloromethane mg/kg ND 0.0050 0.0015 06/20/22 12:45 Bromodichloromethane mg/kg ND 0.0050 0.0019 06/20/22 12:45 Bromoform mg/kg ND 0.0050 0.0018 06/20/22 12:45 Bromomethane mg/kg ND 0.010 0.0079 06/20/22 12:45 Carbon tetrachloride mg/kg ND 0.0050 0.0019 06/20/22 12:45 Chlorobenzene mg/kg ND 0.0050 0.00096 06/20/22 12:45 Chloroethane mg/kg ND 0.010 0.0039 06/20/22 12:45 Chloroform mg/kg ND 0.0050 0.0030 06/20/22 12:45 Chloromethane mg/kg ND 0.010 0.0042 06/20/22 12:45 cis-1,2-Dichloroethene mg/kg ND 0.0050 0.0017 06/20/22 12:45 cis-1,3-Dichloropropene mg/kg ND 0.0050 0.0014 06/20/22 12:45 v1 v1 v1 v1 IK Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 METHOD BLANK: 3680948 Matrix: Solid Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 Blank Reporting Parameter Units Result Limit MDL Analyzed Dibromochloromethane mg/kg ND 0.0050 0.0028 06/20/22 12:45 Dibromomethane mg/kg ND 0.0050 0.0011 06/20/22 12:45 Dichlorodifluoromethane mg/kg ND 0.010 0.0022 06/20/22 12:45 Diisopropyl ether mg/kg ND 0.0050 0.0014 06/20/22 12:45 Ethylbenzene mg/kg ND 0.0050 0.0023 06/20/22 12:45 Hexachloro-1,3-butadiene mg/kg ND 0.010 0.0082 06/20/22 12:45 Isopropylbenzene (Cumene) mg/kg ND 0.0050 0.0017 06/20/22 12:45 m&p-Xylene mg/kg ND 0.010 0.0034 06/20/22 12:45 Methyl-tert-butyl ether mg/kg ND 0.0050 0.0019 06/20/22 12:45 Methylene Chloride mg/kg ND 0.020 0.014 06/20/22 12:45 n-Butylbenzene mg/kg ND 0.0050 0.0024 06/20/22 12:45 n-Propylbenzene mg/kg ND 0.0050 0.0018 06/20/22 12:45 Naphthalene mg/kg ND 0.0050 0.0026 06/20/22 12:45 o-Xylene mg/kg ND 0.0050 0.0022 06/20/22 12:45 p-Isopropyltoluene mg/kg ND 0.0050 0.0025 06/20/22 12:45 sec-Butylbenzene mg/kg ND 0.0050 0.0022 06/20/22 12:45 Styrene mg/kg ND 0.0050 0.0013 06/20/22 12:45 tert-Butyl benzene mg/kg ND 0.0050 0.0018 06/20/22 12:45 Tetrachloroethene mg/kg ND 0.0050 0.0016 06/20/22 12:45 Toluene mg/kg ND 0.0050 0.0014 06/20/22 12:45 trans-1,2-Dichloroethene mg/kg ND 0.0050 0.0018 06/20/22 12:45 trans- 1,3-Dichloropropene mg/kg ND 0.0050 0.0017 06/20/22 12:45 Trichloroethene mg/kg ND 0.0050 0.0013 06/20/22 12:45 Trichlorofluoromethane mg/kg ND 0.0050 0.0028 06/20/22 12:45 Vinyl acetate mg/kg ND 0.050 0.0036 06/20/22 12:45 Vinyl chloride mg/kg ND 0.010 0.0025 06/20/22 12:45 Xylene (Total) mg/kg ND 0.010 0.0028 06/20/22 12:45 1,2-Dichloroethane-d4 (S) % 105 70-130 06/20/22 12:45 4-Bromofluorobenzene (S) % 100 69-134 06/20/22 12:45 Toluene-d8 (S) % 100 70-130 06/20/22 12:45 v1 KI IK Qualifiers LABORATORY CONTROL SAMPLE: 3680949 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane mg/kg 1.2 1.3 107 70-130 1,1,1-Trichloroethane mg/kg 1.2 1.4 108 70-130 1,1,2,2-Tetrachloroethane mg/kg 1.2 1.3 106 70-130 1,1,2-Trichloroethane mg/kg 1.2 1.3 106 70-130 1,1-Dichloroethane mg/kg 1.2 1.3 103 70-130 1,1-Dichloroethene mg/kg 1.2 1.4 110 70-130 1,1-Dichloropropene mg/kg 1.2 1.4 112 70-130 1,2,3-Trichlorobenzene mg/kg 1.2 1.3 104 65-130 1,2,3-Trichloropropane mg/kg 1.2 1.3 105 70-130 1,2,4-Trichlorobenzene mg/kg 1.2 1.3 104 68-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 LABORATORY CONTROL SAMPLE: Parameter 3680949 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,2,4-Trimethylbenzene mg/kg 1.2 1.3 103 70-130 1,2-Dibromo-3-chloropropane mg/kg 1.2 1.6 126 70-130 v1 1,2-Dibromoethane (EDB) mg/kg 1.2 1.3 102 70-130 1,2-Dichlorobenzene mg/kg 1.2 1.3 102 70-130 1,2-Dichloroethane mg/kg 1.2 1.3 101 63-130 1,2-Dichloropropane mg/kg 1.2 1.3 106 70-130 1,3,5-Trimethylbenzene mg/kg 1.2 1.4 108 70-130 1,3-Dichlorobenzene mg/kg 1.2 1.3 103 70-130 1,3-Dichloropropane mg/kg 1.2 1.2 97 70-130 1,4-Dichlorobenzene mg/kg 1.2 1.2 99 70-130 2,2-Dichloropropane mg/kg 1.2 1.3 103 66-130 2-Butanone (MEK) mg/kg 2.5 2.7 110 70-130 2-Chlorotoluene mg/kg 1.2 1.3 106 70-130 2-Hexanone mg/kg 2.5 2.9 118 70-130 v1 4-Chlorotoluene mg/kg 1.2 1.3 104 70-130 4-Methyl-2-pentanone (MIBK) mg/kg 2.5 2.9 116 70-130 v1 Acetone mg/kg 2.5 2.9 115 69-130 Benzene mg/kg 1.2 1.2 99 70-130 Bromobenzene mg/kg 1.2 1.3 102 70-130 Bromochloromethane mg/kg 1.2 1.3 103 70-130 Bromodichloromethane mg/kg 1.2 1.4 108 69-130 Bromoform mg/kg 1.2 1.5 117 70-130 v1 Bromomethane mg/kg 1.2 1.2 98 52-130IK Carbon tetrachloride mg/kg 1.2 1.4 112 70-130 Chlorobenzene mg/kg 1.2 1.3 100 70-130 Chloroethane mg/kg 1.2 1.5 116 65-130 Chloroform mg/kg 1.2 1.3 102 70-130 Chloromethane mg/kg 1.2 1.4 115 55-130 cis-1,2-Dichloroethene mg/kg 1.2 1.3 104 70-130 cis-1,3-Dichloropropene mg/kg 1.2 1.4 109 70-130 Dibromochloromethane mg/kg 1.2 1.3 107 70-130 Dibromomethane mg/kg 1.2 1.3 107 70-130 Dichlorodifluoromethane mg/kg 1.2 1.5 121 45-156 v1 Diisopropyl ether mg/kg 1.2 1.3 103 70-130 Ethylbenzene mg/kg 1.2 1.2 93 70-130 Hexachloro-1,3-butadiene mg/kg 1.2 1.3 105 66-130 Isopropylbenzene (Cumene) mg/kg 1.2 1.3 101 70-130 m&p-Xylene mg/kg 2.5 2.5 98 70-130 Methyl-tert-butyl ether mg/kg 1.2 1.1 91 70-130 Methylene Chloride mg/kg 1.2 1.0 83 65-130 n-Butylbenzene mg/kg 1.2 1.4 109 67-130 n-Propylbenzene mg/kg 1.2 1.3 105 70-130 Naphthalene mg/kg 1.2 1.4 116 70-130 o-Xylene mg/kg 1.2 1.2 98 70-130 p-Isopropyltoluene mg/kg 1.2 1.4 111 67-130 sec-Butylbenzene mg/kg 1.2 1.3 106 69-130 Styrene mg/kg 1.2 1.2 98 70-130IK Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 LABORATORY CONTROL SAMPLE: Parameter 3680949 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers tert-Butyl benzene mg/kg 1.2 1.4 109 67-130 Tetrachloroethene mg/kg 1.2 1.3 104 70-130 Toluene mg/kg 1.2 1.3 101 70-1301K trans-1,2-Dichloroethene mg/kg 1.2 1.4 108 70-130 trans- 1,3-Dichloropropene mg/kg 1.2 1.4 110 68-130 Trichloroethene mg/kg 1.2 1.3 108 70-130 Trichlorofluoromethane mg/kg 1.2 1.3 106 70-130 Vinyl acetate mg/kg 2.5 2.5 101 70-130 Vinyl chloride mg/kg 1.2 1.4 115 61-130 Xylene (Total) mg/kg 3.8 3.7 98 70-130 1,2-Dichloroethane-d4 (S) % 92 70-130 4-Bromofluorobenzene (S) % 96 69-134 Toluene-d8(S) % 101 70-130 MATRIX SPIKE SAMPLE: Parameter 3680950 Units 92610193025 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane mg/kg ND 0.83 0.67 81 70-131 1,1,1-Trichloroethane mg/kg ND 0.83 0.77 92 65-133 1,1,2,2-Tetrachloroethane mg/kg ND 0.83 0.69 83 66-130 1,1,2-Trichloroethane mg/kg ND 0.83 0.71 86 66-133 1,1-Dichloroethane mg/kg ND 0.83 0.69 84 65-130 1,1-Dichloroethene mg/kg ND 0.83 0.78 95 10-158 1,1-Dichloropropene mg/kg ND 0.83 0.77 93 68-133 1,2,3-Trichlorobenzene mg/kg ND 0.83 0.13 16 27-138 M1 1,2,3-Trichloropropane mg/kg ND 0.83 0.63 77 67-130 1,2,4-Trichlorobenzene mg/kg ND 0.83 0.29 35 51-134 M1 1,2,4-Trimethylbenzene mg/kg ND 0.83 0.72 86 63-136 1,2-Dibromo-3-chloropropane mg/kg ND 0.83 0.40 48 32-130 v1 1,2-Dibromoethane (EDB) mg/kg ND 0.83 0.72 86 70-130 1,2-Dichlorobenzene mg/kg ND 0.83 0.68 82 69-130 1,2-Dichloroethane mg/kg ND 0.83 0.71 85 59-130 1,2-Dichloropropane mg/kg ND 0.83 0.75 90 70-130 1,3,5-Trimethylbenzene mg/kg ND 0.83 0.73 89 65-137 1,3-Dichlorobenzene mg/kg ND 0.83 0.66 80 70-130 1,3-Dichloropropane mg/kg ND 0.83 0.73 88 70-130 1,4-Dichlorobenzene mg/kg ND 0.83 0.66 80 68-130 2,2-Dichloropropane mg/kg ND 0.83 0.40 48 32-130 2-Butanone (MEK) mg/kg 97.7J ug/kg 1.7 1.4 80 10-136 2-Chlorotoluene mg/kg ND 0.83 0.70 84 69-141 2-Hexanone mg/kg ND 1.7 1.4 81 10-144 v1 4-Chlorotoluene mg/kg ND 0.83 0.68 81 70-132 4-Methyl-2-pentanone (MIBK) mg/kg ND 1.7 1.4 86 25-143 v1 Acetone mg/kg ND 1.7 1.2 71 10-130 Benzene mg/kg ND 0.83 0.72 87 67-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 MATRIX SPIKE SAMPLE: 3680950 92610193025 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Bromobenzene mg/kg ND 0.83 0.71 85 70-130 Bromochloromethane mg/kg ND 0.83 0.71 86 69-134 Bromodichloromethane mg/kg ND 0.83 0.61 74 64-130 Bromoform mg/kg ND 0.83 0.56 68 62-130 v1 Bromomethane mg/kg ND 0.83 0.47 57 20-1761K Carbon tetrachloride mg/kg ND 0.83 0.66 80 65-140 Chlorobenzene mg/kg ND 0.83 0.73 88 70-130 Chloroethane mg/kg ND 0.83 0.26 31 10-130 Chloroform mg/kg ND 0.83 0.72 87 63-130 Chloromethane mg/kg ND 0.83 0.93 112 58-130 cis-1,2-Dichloroethene mg/kg ND 0.83 0.73 89 66-130 cis-1,3-Dichloropropene mg/kg ND 0.83 0.58 71 67-130 Dibromochloromethane mg/kg ND 0.83 0.58 70 67-130 Dibromomethane mg/kg ND 0.83 0.69 83 63-131 Dichlorodifluoromethane mg/kg ND 0.83 0.77 93 44-180 v1 Diisopropyl ether mg/kg ND 0.83 0.77 93 63-130 Ethylbenzene mg/kg ND 0.83 0.68 82 66-130 Hexachloro-1,3-butadiene mg/kg ND 0.83 0.42 50 64-150 M1 Isopropylbenzene (Cumene) mg/kg ND 0.83 0.74 89 69-135 m&p-Xylene mg/kg ND 1.7 1.4 85 60-133 Methyl-tert-butyl ether mg/kg ND 0.83 0.69 83 65-130 Methylene Chloride mg/kg ND 0.83 0.39 47 61-130 M1 n-Butylbenzene mg/kg ND 0.83 0.59 72 65-140 n-Propylbenzene mg/kg ND 0.83 0.67 81 67-140 Naphthalene mg/kg ND 0.83 0.17 21 15-145 o-Xylene mg/kg ND 0.83 0.72 87 66-133 p-Isopropyltoluene mg/kg ND 0.83 0.70 85 56-147 sec-Butylbenzene mg/kg ND 0.83 0.72 87 65-139 Styrene mg/kg 7.7J ug/kg 0.83 0.69 83 70-132 IK tert-Butyl benzene mg/kg ND 0.83 0.77 93 62-135 Tetrachloroethene mg/kg ND 0.83 0.66 79 70-135 Toluene mg/kg ND 0.83 0.73 88 67-1301K trans-1,2-Dichloroethene mg/kg ND 0.83 0.74 89 69-130 trans- 1,3-Dichloropropene mg/kg ND 0.83 0.57 69 62-130 Trichloroethene mg/kg ND 0.83 0.74 89 70-135 Trichlorofluoromethane mg/kg ND 0.83 0.24 29 10-130 Vinyl acetate mg/kg ND 1.7 1.2 71 53-130 Vinyl chloride mg/kg ND 0.83 0.78 94 61-148 Xylene (Total) mg/kg ND 2.5 2.1 86 63-132 1,2-Dichloroethane-d4 (S) % 101 70-130 4-Bromofluorobenzene (S) % 101 69-134 Toluene-d8(S) % 101 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 64 Pace Analytical Services, LLC lac, Analyilcal ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 SAMPLE DUPLICATE: 3680951 Parameter Units 92610193026 Result Dup Result RPD Max RPD Qualifiers 1,1,1,2-Tetrachloroethane mg/kg ND ND 30 1,1,1-Trichloroethane mg/kg ND ND 30 1,1,2,2-Tetrachloroethane mg/kg ND ND 30 1,1,2-Trichloroethane mg/kg ND ND 30 1,1-Dichloroethane mg/kg ND ND 30 1,1-Dichloroethene mg/kg ND ND 30 1,1-Dichloropropene mg/kg ND ND 30 1,2,3-Trichlorobenzene mg/kg ND ND 30 1,2,3-Trichloropropane mg/kg ND ND 30 1,2,4-Trichlorobenzene mg/kg ND ND 30 1,2,4-Trimethylbenzene mg/kg ND ND 30 1,2-Dibromo-3-chloropropane mg/kg ND ND 30 v1 1,2-Dibromoethane (EDB) mg/kg ND ND 30 1,2-Dichlorobenzene mg/kg ND ND 30 1,2-Dichloroethane mg/kg ND ND 30 1,2-Dichloropropane mg/kg ND ND 30 1,3,5-Trimethylbenzene mg/kg ND ND 30 1,3-Dichlorobenzene mg/kg ND ND 30 1,3-Dichloropropane mg/kg ND ND 30 1,4-Dichlorobenzene mg/kg ND ND 30 2,2-Dichloropropane mg/kg ND ND 30 2-Butanone (MEK) mg/kg 92.9J ug/kg 0.047J 30 2-Chlorotoluene mg/kg ND ND 30 2-Hexanone mg/kg ND ND 30 v1 4-Chlorotoluene mg/kg ND ND 30 4-Methyl-2-pentanone (MIBK) mg/kg ND ND 30 v1 Acetone mg/kg ND ND 30 Benzene mg/kg ND ND 30 Bromobenzene mg/kg ND ND 30 Bromochloromethane mg/kg ND ND 30 Bromodichloromethane mg/kg ND ND 30 Bromoform mg/kg ND ND 30 v1 Bromomethane mg/kg ND ND 301K Carbon tetrachloride mg/kg ND ND 30 Chlorobenzene mg/kg ND ND 30 Chloroethane mg/kg ND ND 30 Chloroform mg/kg ND ND 30 Chloromethane mg/kg ND ND 30 cis-1,2-Dichloroethene mg/kg ND ND 30 cis-1,3-Dichloropropene mg/kg ND ND 30 Dibromochloromethane mg/kg ND ND 30 Dibromomethane mg/kg ND ND 30 Dichlorodifluoromethane mg/kg ND ND 30 v1 Diisopropyl ether mg/kg ND ND 30 Ethylbenzene mg/kg ND ND 30 Hexachloro-1,3-butadiene mg/kg ND ND 30 Isopropylbenzene (Cumene) mg/kg ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 SAMPLE DUPLICATE: 3680951 Parameter Units 92610193026 Result Dup Result m&p-Xylene mg/kg ND ND Methyl-tert-butyl ether mg/kg ND ND Methylene Chloride mg/kg ND ND n-Butylbenzene mg/kg ND ND n-Propylbenzene mg/kg ND ND Naphthalene mg/kg ND ND o-Xylene mg/kg ND ND p-Isopropyltoluene mg/kg ND ND sec-Butylbenzene mg/kg ND ND Styrene mg/kg 6.8J ug/kg 0.0056J tert-Butyl benzene mg/kg ND ND Tetrachloroethene mg/kg ND ND Toluene mg/kg ND ND trans-1,2-Dichloroethene mg/kg ND ND trans- 1,3-Dichloropropene mg/kg ND ND Trichloroethene mg/kg ND ND Trichlorofluoromethane mg/kg ND ND Vinyl acetate mg/kg ND ND Vinyl chloride mg/kg ND ND Xylene (Total) mg/kg ND ND 1,2-Dichloroethane-d4 (S) % 103 103 4-Bromofluorobenzene (S) % 101 101 Toluene-d8(S) % 101 101 Max RPD RPD Qualifiers 30 30 30 30 30 30 30 30 30 30 I K 30 30 30 I K 30 30 30 30 30 30 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 QC Batch: 706233 Analysis Method: EPA 8081 B QC Batch Method: EPA 3546 Analysis Description: 8081 GCS Pesticides Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 METHOD BLANK: 3684385 Matrix: Solid Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 4,4'-DDD mg/kg ND 0.0020 0.00092 06/27/22 14:18 4,4'-DDE mg/kg ND 0.0020 0.00096 06/27/22 14:18 4,4'-DDT mg/kg ND 0.0020 0.00090 06/27/22 14:18 Aldrin mg/kg ND 0.0020 0.00082 06/27/22 14:18 alpha-BHC mg/kg ND 0.0020 0.00088 06/27/22 14:18 beta-BHC mg/kg ND 0.0020 0.00098 06/27/22 14:18 Chlordane (Technical) mg/kg ND 0.010 0.0088 06/27/22 14:18 delta-BHC mg/kg ND 0.0020 0.0010 06/27/22 14:18 Dieldrin mg/kg ND 0.0020 0.00088 06/27/22 14:18 Endosulfan I mg/kg ND 0.0020 0.00087 06/27/22 14:18 Endosulfan 11 mg/kg ND 0.0020 0.00092 06/27/22 14:18 Endosulfan sulfate mg/kg ND 0.0020 0.0011 06/27/22 14:18 Endrin mg/kg ND 0.0020 0.00094 06/27/22 14:18 Endrin aldehyde mg/kg ND 0.0020 0.0014 06/27/22 14:18 Endrin ketone mg/kg ND 0.0020 0.0011 06/27/22 14:18 gamma-BHC (Lindane) mg/kg ND 0.0020 0.00081 06/27/22 14:18 Heptachlor mg/kg ND 0.0020 0.00094 06/27/22 14:18 Heptachlor epoxide mg/kg ND 0.0020 0.00080 06/27/22 14:18 Hexachlorobenzene mg/kg ND 0.0020 0.00084 06/27/22 14:18 Methoxychlor mg/kg ND 0.0051 0.0025 06/27/22 14:18 Mirex mg/kg ND 0.0051 0.0022 06/27/22 14:18 Toxaphene mg/kg ND 0.0071 0.0054 06/27/22 14:18 Decachlorobiphenyl (S) % 96 10-146 06/27/22 14:18 Tetrachloro-m-xylene (S) % 71 10-133 06/27/22 14:18 LABORATORY CONTROL SAMPLE: 3684386 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 4,4'-DDD mg/kg 0.0083 0.011 131 40-160 4,4'-DDE mg/kg 0.0083 0.0096 116 41-154 4,4'-DDT mg/kg 0.0083 0.0074 90 34-163 Aldrin mg/kg 0.0083 0.0071 85 39-144 alpha-BHC mg/kg 0.0083 0.0076 91 36-145 beta-BHC mg/kg 0.0083 0.0072 86 39-152 delta-BHC mg/kg 0.0083 0.0076 91 41-147 Dieldrin mg/kg 0.0083 0.0094 113 42-153 Endosulfan I mg/kg 0.0083 0.0071 85 39-148 Endosulfan II mg/kg 0.0083 0.0070 84 40-147 Endosulfan sulfate mg/kg 0.0083 0.0072 87 40-148 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 LABORATORY CONTROL SAMPLE: Parameter 3684386 Units Spike Conc. LCS LCS Result % Rec Endrin mg/kg 0.0083 0.0096 Endrin aldehyde mg/kg 0.0083 0.0063 Endrin ketone mg/kg 0.0083 0.0066 gamma-BHC (Lindane) mg/kg 0.0083 0.0076 Heptachlor mg/kg 0.0083 0.0073 Heptachlor epoxide mg/kg 0.0083 0.0071 Hexachlorobenzene mg/kg 0.0083 0.0075 Methoxychlor mg/kg 0.025 0.017 Mirex mg/kg 0.025 0.020 Decachlorobiphenyl (S) % Tetrachloro-m-xylene (S) % % Rec Limits 116 42-158 76 39-130 80 39-159 92 38-146 88 39-144 86 40-143 90 33-139 67 32-146 80 39-141 85 10-146 84 10-133 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3684387 MS 92610560001 Spike Parameter Units Result Conc. MSD Spike Conc. 3684388 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 4,4'-DDD mg/kg ND 0.0084 0.0083 0.0077 0.0089 92 107 10-160 15 30 4,4'-DDE mg/kg ND 0.0084 0.0083 0.0078 0.0086 93 104 10-170 11 30 4,4'-DDT mg/kg ND 0.0084 0.0083 0.0080 0.0088 96 106 10-194 10 30 Aldrin mg/kg ND 0.0084 0.0083 0.0055 0.0065 66 78 10-143 15 30 alpha-BHC mg/kg ND 0.0084 0.0083 0.0058 0.0068 70 82 10-144 15 30 beta-BHC mg/kg ND 0.0084 0.0083 0.012 0.0068 140 82 10-152 52 30 R1 delta-BHC mg/kg ND 0.0084 0.0083 0.0061 0.0066 73 80 10-147 8 30 Dieldrin mg/kg ND 0.0084 0.0083 0.0075 0.0084 90 101 10-181 11 30 Endosulfan I mg/kg ND 0.0084 0.0083 0.0055 0.0062 65 75 10-147 12 30 Endosulfan II mg/kg ND 0.0084 0.0083 0.0056 0.0062 67 74 11-149 10 30 Endosulfan sulfate mg/kg ND 0.0084 0.0083 0.0057 0.0063 68 76 10-153 10 30 Endrin mg/kg ND 0.0084 0.0083 0.0079 0.0086 94 103 10-160 8 30 Endrin aldehyde mg/kg ND 0.0084 0.0083 0.0048 0.0054 57 65 10-134 13 30 Endrin ketone mg/kg ND 0.0084 0.0083 0.0054 0.0060 65 72 11-155 10 30 gamma-BHC (Lindane) mg/kg ND 0.0084 0.0083 0.0060 0.0067 71 81 10-152 12 30 Heptachlor mg/kg ND 0.0084 0.0083 0.0058 0.0066 70 79 10-149 12 30 Heptachlor epoxide mg/kg ND 0.0084 0.0083 0.0056 0.0063 67 76 10-142 12 30 Hexachlorobenzene mg/kg ND 0.0084 0.0083 0.0056 0.0065 66 79 10-140 16 30 Methoxychlor mg/kg ND 0.025 0.025 0.031 0.030 124 120 10-147 4 30 Mirex mg/kg ND 0.025 0.025 0.016 0.017 63 69 11-139 8 30 Decachlorobiphenyl (S) % 66 75 10-146 Tetrachloro-m-xylene (S) % 60 77 10-133 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 QC Batch: 706395 Analysis Method: EPA 8270E QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 METHOD BLANK: 3685278 Matrix: Solid Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,2,4-Trichlorobenzene mg/kg ND 0.33 0.13 06/27/22 18:20 1,2-Dichlorobenzene mg/kg ND 0.33 0.12 06/27/22 18:20 1,3-Dichlorobenzene mg/kg ND 0.33 0.12 06/27/22 18:20 1,4-Dichlorobenzene mg/kg ND 0.33 0.13 06/27/22 18:20 1-Methylnaphthalene mg/kg ND 0.33 0.12 06/27/22 18:20 2,2'-Oxybis(1-chloropropane) mg/kg ND 0.33 0.16 06/27/22 18:20 v1 2,4,5-Trichlorophenol mg/kg ND 0.33 0.15 06/27/22 18:20 2,4,6-Trichlorophenol mg/kg ND 0.33 0.14 06/27/22 18:20 2,4-Dichlorophenol mg/kg ND 0.33 0.13 06/27/22 18:20 2,4-Dimethylphenol mg/kg ND 0.33 0.14 06/27/22 18:20 2,4-Dinitrophenol mg/kg ND 1.7 1.0 06/27/22 18:20 2,4-Dinitrotoluene mg/kg ND 0.33 0.13 06/27/22 18:20 2,6-Dinitrotoluene mg/kg ND 0.33 0.12 06/27/22 18:20 2-Chloronaphthalene mg/kg ND 0.33 0.13 06/27/22 18:20 2-Chlorophenol mg/kg ND 0.33 0.12 06/27/22 18:20 2-Methylnaphthalene mg/kg ND 0.33 0.13 06/27/22 18:20 2-Methylphenol(o-Cresol) mg/kg ND 0.33 0.14 06/27/22 18:20 2-Nitroaniline mg/kg ND 1.7 0.27 06/27/22 18:20 2-Nitrophenol mg/kg ND 0.33 0.14 06/27/22 18:20 3&4-Methyl phenol (m&p Cresol) mg/kg ND 0.33 0.13 06/27/22 18:20 3,3'-Dichlorobenzidine mg/kg ND 0.66 0.22 06/27/22 18:20 IL 3-Nitroaniline mg/kg ND 1.7 0.26 06/27/22 18:20 IL 4,6-Dinitro-2-methyl phenol mg/kg ND 0.66 0.31 06/27/22 18:20 4-Bromophenylphenyl ether mg/kg ND 0.33 0.13 06/27/22 18:20 4-ChIoro-3-methyl phenol mg/kg ND 0.66 0.23 06/27/22 18:20 4-Chloroaniline mg/kg ND 0.66 0.26 06/27/22 18:20 4-Chlorophenylphenyl ether mg/kg ND 0.33 0.12 06/27/22 18:20 4-Nitroaniline mg/kg ND 0.66 0.25 06/27/22 18:20 IL,v2 4-Nitrophenol mg/kg ND 1.7 0.64 06/27/22 18:20 v2 Acenaphthene mg/kg ND 0.33 0.12 06/27/22 18:20 Acenaphthylene mg/kg ND 0.33 0.12 06/27/22 18:20 Aniline mg/kg ND 0.33 0.13 06/27/22 18:20 v2 Anthracene mg/kg ND 0.33 0.11 06/27/22 18:20 Benzo(a)anthracene mg/kg ND 0.33 0.11 06/27/22 18:20 Benzo(a)pyrene mg/kg ND 0.33 0.11 06/27/22 18:20 Benzo(b)fluoranthene mg/kg ND 0.33 0.11 06/27/22 18:20 Benzo(g,h,i)perylene mg/kg ND 0.33 0.13 06/27/22 18:20 Benzo(k)fluoranthene mg/kg ND 0.33 0.12 06/27/22 18:20 Benzoic Acid mg/kg ND 1.7 0.71 06/27/22 18:20 Benzyl alcohol mg/kg ND 0.66 0.25 06/27/22 18:20 v2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 METHOD BLANK: 3685278 Matrix: Solid Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 Blank Reporting Parameter Units Result Limit MDL Analyzed bis(2-Chloroethoxy)methane mg/kg ND 0.33 0.14 06/27/22 18:20 bis(2-Chloroethyl) ether mg/kg ND 0.33 0.12 06/27/22 18:20 bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 0.13 06/27/22 18:20 Butylbenzylphthalate mg/kg ND 0.33 0.14 06/27/22 18:20 Chrysene mg/kg ND 0.33 0.12 06/27/22 18:20 Di-n-butylphthalate mg/kg ND 0.33 0.11 06/27/22 18:20 Di-n-octylphthalate mg/kg ND 0.33 0.13 06/27/22 18:20 Dibenz(a,h)anthracene mg/kg ND 0.33 0.13 06/27/22 18:20 Dibenzofuran mg/kg ND 0.33 0.12 06/27/22 18:20 Diethylphthalate mg/kg ND 0.33 0.12 06/27/22 18:20 Dimethylphthalate mg/kg ND 0.33 0.12 06/27/22 18:20 Fluoranthene mg/kg ND 0.33 0.11 06/27/22 18:20 Fluorene mg/kg ND 0.33 0.12 06/27/22 18:20 Hexachloro-1,3-butadiene mg/kg ND 0.33 0.14 06/27/22 18:20 Hexachlorobenzene mg/kg ND 0.33 0.13 06/27/22 18:20 Hexachlorocyclopentadiene mg/kg ND 0.33 0.19 06/27/22 18:20 Hexachloroethane mg/kg ND 0.33 0.13 06/27/22 18:20 Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 0.13 06/27/22 18:20 Isophorone mg/kg ND 0.33 0.15 06/27/22 18:20 N-Nitroso-di-n-propylamine mg/kg ND 0.33 0.12 06/27/22 18:20 N-Nitrosodimethylamine mg/kg ND 0.33 0.11 06/27/22 18:20 N-Nitrosodiphenylamine mg/kg ND 0.33 0.12 06/27/22 18:20 Naphthalene mg/kg ND 0.33 0.11 06/27/22 18:20 Nitrobenzene mg/kg ND 0.33 0.15 06/27/22 18:20 Pentachlorophenol mg/kg ND 0.66 0.33 06/27/22 18:20 Phenanthrene mg/kg ND 0.33 0.11 06/27/22 18:20 Phenol mg/kg ND 0.33 0.15 06/27/22 18:20 Pyrene mg/kg ND 0.33 0.13 06/27/22 18:20 Pyridine mg/kg ND 0.33 0.10 06/27/22 18:20 2,4,6-Tribromophenol (S) % 80 18-130 06/27/22 18:20 2-Fluorobiphenyl (S) % 72 19-130 06/27/22 18:20 2-Fluorophenol (S) % 64 18-130 06/27/22 18:20 Nitrobenzene-d5 (S) % 74 21-130 06/27/22 18:20 Phenol-d6 (S) % 65 18-130 06/27/22 18:20 Terphenyl-d14 (S) % 86 15-130 06/27/22 18:20 v2 Qualifiers LABORATORY CONTROL SAMPLE: 3685279 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,2,4-Trichlorobenzene mg/kg 1.7 1.2 74 47-130 1,2-Dichlorobenzene mg/kg 1.7 1.1 68 49-130 1,3-Dichlorobenzene mg/kg 1.7 1.1 69 48-130 1,4-Dichlorobenzene mg/kg 1.7 1.1 69 49-130 1-Methylnaphthalene mg/kg 1.7 1.2 74 54-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 49 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Wright's Executive Sales Pace Project No.: 92610504 LABORATORY CONTROL SAMPLE: 3685279 Parameter QUALITY CONTROL DATA Spike LCS LCS % Rec Units Conc. Result % Rec Limits Qualifiers 2,2'-Oxybis(1-chloropropane) mg/kg 1.7 1.4 84 38-130 v1 2,4,5-Trichlorophenol mg/kg 1.7 1.4 85 49-130 2,4,6-Trichlorophenol mg/kg 1.7 1.4 85 50-130 2,4-Dichlorophenol mg/kg 1.7 1.3 79 51-130 2,4-Dimethylphenol mg/kg 1.7 1.2 74 53-130 2,4-Dinitrophenol mg/kg 8.3 6.6 79 39-130 2,4-Dinitrotoluene mg/kg 1.7 1.4 85 53-130 2,6-Dinitrotoluene mg/kg 1.7 1.6 94 55-130 2-Chloronaphthalene mg/kg 1.7 1.4 84 48-130 2-Chlorophenol mg/kg 1.7 1.2 70 54-130 2-Methylnaphthalene mg/kg 1.7 1.2 74 57-130 2-Methylphenol(o-Cresol) mg/kg 1.7 1.1 66 50-130 2-Nitroaniline mg/kg 3.3 2.7 81 49-130 2-Nitrophenol mg/kg 1.7 1.5 90 50-130 3&4-Methyl phenol (m&p Cresol) mg/kg 1.7 1.0 60 50-130 3,3'-Dichlorobenzidine mg/kg 3.3 2.6 78 47-130IL 3-Nitroaniline mg/kg 3.3 2.6 78 45-130IL 4,6-Dinitro-2-methyl phenol mg/kg 3.3 2.8 84 50-142 4-Bromophenylphenyl ether mg/kg 1.7 1.6 94 55-130 4-ChIoro-3-methyl phenol mg/kg 3.3 2.4 73 52-130 4-Chloroaniline mg/kg 3.3 2.3 69 49-130 4-Chlorophenylphenyl ether mg/kg 1.7 1.3 79 53-130 4-Nitroaniline mg/kg 3.3 2.3 70 51-1301L,v3 4-Nitrophenol mg/kg 8.3 5.1 61 40-130 v3 Acenaphthene mg/kg 1.7 1.4 81 56-130 Acenaphthylene mg/kg 1.7 1.4 82 58-130 Aniline mg/kg 1.7 0.93 56 44-130 v3 Anthracene mg/kg 1.7 1.3 76 60-130 Benzo(a)anthracene mg/kg 1.7 1.4 84 59-130 Benzo(a)pyrene mg/kg 1.7 1.4 83 57-130 Benzo(b)fluoranthene mg/kg 1.7 1.3 80 54-130 Benzo(g,h,i)perylene mg/kg 1.7 1.5 90 59-130 Benzo(k)fluoranthene mg/kg 1.7 1.4 82 54-130 Benzoic Acid mg/kg 8.3 4.6 55 19-130 Benzyl alcohol mg/kg 3.3 2.1 62 50-130 v3 bis(2-Chloroethoxy)methane mg/kg 1.7 1.2 72 55-130 bis(2-Chloroethyl) ether mg/kg 1.7 1.1 64 53-130 bis(2-Ethylhexyl)phthalate mg/kg 1.7 1.5 88 58-130 Butylbenzylphthalate mg/kg 1.7 1.7 100 46-138 Chrysene mg/kg 1.7 1.4 85 57-130 Di-n-butylphthalate mg/kg 1.7 1.4 82 57-130 Di-n-octylphthalate mg/kg 1.7 1.6 97 57-130 Dibenz(a,h)anthracene mg/kg 1.7 1.5 92 60-130 Dibenzofuran mg/kg 1.7 1.4 82 54-130 Diethylphthalate mg/kg 1.7 1.4 81 55-130 Dimethylphthalate mg/kg 1.7 1.4 83 57-130 Fluoranthene mg/kg 1.7 1.3 78 57-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 50 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 LABORATORY CONTROL SAMPLE: Parameter 3685279 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Fluorene mg/kg 1.7 1.2 75 56-130 Hexachloro-1,3-butadiene mg/kg 1.7 1.3 77 41-130 Hexachlorobenzene mg/kg 1.7 1.4 86 53-130 Hexachlorocyclopentadiene mg/kg 1.7 0.85 51 23-130 Hexachloroethane mg/kg 1.7 1.1 66 48-130 Indeno(1,2,3-cd)pyrene mg/kg 1.7 1.5 89 61-130 Isophorone mg/kg 1.7 1.2 71 49-130 N-Nitroso-di-n-propylamine mg/kg 1.7 1.1 63 52-130 v3 N-Nitrosodimethylamine mg/kg 1.7 0.97 58 45-130 N-Nitrosodiphenylamine mg/kg 1.7 1.5 88 56-130 Naphthalene mg/kg 1.7 1.2 73 56-130 Nitrobenzene mg/kg 1.7 1.2 74 50-130 Pentachlorophenol mg/kg 3.3 2.3 70 33-130 Phenanthrene mg/kg 1.7 1.4 85 60-130 Phenol mg/kg 1.7 1.1 69 54-130 Pyrene mg/kg 1.7 1.7 99 61-130 Pyridine mg/kg 1.7 0.86 52 35-130 2,4,6-Tribromophenol (S) % 94 18-130 2-Fluorobiphenyl (S) % 82 19-130 2-Fluorophenol(S) % 64 18-130 Nitrobenzene-d5 (S) % 74 21-130 Phenol-d6 (S) % 67 18-130 Terphenyl-d14 (S) % 94 15-130 MATRIX SPIKE SAMPLE: Parameter 3685280 Units 92610193036 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,2,4-Trichlorobenzene mg/kg ND 1.8 1.0 55 22-130 1,2-Dichlorobenzene mg/kg ND 1.8 0.99 53 23-130 1,3-Dichlorobenzene mg/kg ND 1.8 0.99 53 26-130 1,4-Dichlorobenzene mg/kg ND 1.8 0.99 53 27-130 1-Methylnaphthalene mg/kg ND 1.8 1.0 55 30-130 2,2'-Oxybis(1-chloropropane) mg/kg ND 1.8 1.2 64 30-130 v1 2,4,5-Trichlorophenol mg/kg ND 1.8 1.2 64 26-130 2,4,6-Trichlorophenol mg/kg ND 1.8 1.2 62 23-130 2,4-Dichlorophenol mg/kg ND 1.8 1.1 58 29-130 2,4-Dimethylphenol mg/kg ND 1.8 0.93 50 13-130 2,4-Dinitrophenol mg/kg ND 9.3 6.0 65 10-131 2,4-Dinitrotoluene mg/kg ND 1.8 1.2 66 28-130 2,6-Dinitrotoluene mg/kg ND 1.8 1.4 74 36-130 2-Chloronaphthalene mg/kg ND 1.8 1.2 62 27-130 2-Chlorophenol mg/kg ND 1.8 1.0 54 29-130 2-Methylnaphthalene mg/kg ND 1.8 1.0 55 29-130 2-Methylphenol(o-Cresol) mg/kg ND 1.8 0.89 48 20-130 2-Nitroaniline mg/kg ND 3.7 2.3 62 29-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 51 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 MATRIX SPIKE SAMPLE: 3685280 92610193036 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 2-Nitrophenol mg/kg ND 1.8 1.2 67 26-130 3&4-Methyl phenol (m&p Cresol) mg/kg ND 1.8 0.81 44 10-176 3,3'-Dichlorobenzidine mg/kg ND 3.7 2.1 56 15-130IL 3-Nitroaniline mg/kg ND 3.7 2.3 63 28-130IL 4,6-Dinitro-2-methyl phenol mg/kg ND 3.7 2.5 67 15-132 4-Bromophenylphenyl ether mg/kg ND 1.8 1.3 70 35-130 4-Chloro-3-methylphenol mg/kg ND 3.7 2.0 55 30-130 4-Chloroaniline mg/kg ND 3.7 1.9 51 28-130 4-Chlorophenylphenyl ether mg/kg ND 1.8 1.1 59 32-130 4-Nitroaniline mg/kg ND 3.7 2.1 56 30-1301L,v3 4-Nitrophenol mg/kg ND 9.3 4.4 48 17-130 v3 Acenaphthene mg/kg ND 1.8 1.1 61 29-130 Acenaphthylene mg/kg ND 1.8 1.1 62 31-130 Aniline mg/kg ND 1.8 0.69 37 10-130 v3 Anthracene mg/kg ND 1.8 1.1 58 33-130 Benzo(a)anthracene mg/kg ND 1.8 1.2 63 32-130 Benzo(a)pyrene mg/kg ND 1.8 1.2 63 32-130 Benzo(b)fluoranthene mg/kg ND 1.8 1.1 59 33-130 Benzo(g,h,i)perylene mg/kg ND 1.8 1.2 66 28-130 Benzo(k)fluoranthene mg/kg ND 1.8 1.2 64 31-130 Benzoic Acid mg/kg ND 9.3 3.1 33 10-130 Benzyl alcohol mg/kg ND 3.7 1.7 47 31-130 v3 bis(2-Chloroethoxy)methane mg/kg ND 1.8 0.99 53 30-130 bis(2-Chloroethyl) ether mg/kg ND 1.8 0.91 49 68-130 M1 bis(2-Ethylhexyl)phthalate mg/kg ND 1.8 1.2 65 40-130 Butylbenzylphthalate mg/kg ND 1.8 1.4 75 40-130 Chrysene mg/kg ND 1.8 1.2 64 30-130 Di-n-butylphthalate mg/kg ND 1.8 1.2 63 41-130 Di-n-octylphthalate mg/kg ND 1.8 1.3 72 42-130 Dibenz(a,h)anthracene mg/kg ND 1.8 1.3 68 27-130 Dibenzofuran mg/kg ND 1.8 1.2 63 32-130 Diethylphthalate mg/kg ND 1.8 1.2 63 40-130 Dimethylphthalate mg/kg ND 1.8 1.2 64 37-130 Fluoranthene mg/kg ND 1.8 1.1 60 26-130 Fluorene mg/kg ND 1.8 1.1 57 31-130 Hexachloro-1,3-butadiene mg/kg ND 1.8 1.1 58 20-130 Hexachlorobenzene mg/kg ND 1.8 1.2 64 29-130 Hexachlorocyclopentadiene mg/kg ND 1.8 0.60 32 10-130 Hexachloroethane mg/kg ND 1.8 0.94 51 21-130 Indeno(1,2,3-cd)pyrene mg/kg ND 1.8 1.2 66 28-130 Isophorone mg/kg ND 1.8 0.98 53 32-130 N-Nitroso-di-n-propylamine mg/kg ND 1.8 0.89 48 31-130 v3 N-Nitrosodimethylamine mg/kg ND 1.8 0.84 45 20-130 N-Nitrosodiphenylamine mg/kg ND 1.8 1.2 67 32-130 Naphthalene mg/kg ND 1.8 1.0 55 30-130 Nitrobenzene mg/kg ND 1.8 1.0 55 25-130 Pentachlorophenol mg/kg ND 3.7 1.8 49 10-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 52 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 MATRIX SPIKE SAMPLE: Parameter 3685280 Units 92610193036 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers Phenanthrene mg/kg ND 1.8 1.2 66 34-130 Phenol mg/kg ND 1.8 0.95 51 14-130 Pyrene mg/kg ND 1.8 1.4 74 31-130 Pyridine mg/kg ND 1.8 0.63 34 10-130 2,4,6-Tribromophenol (S) % 65 18-130 2-Fluorobiphenyl (S) % 57 19-130 2-Fluorophenol (S) % 45 18-130 Nitrobenzene-d5 (S) % 53 21-130 Phenol-d6 (S) % 47 18-130 Terphenyl-d14 (S) % 71 15-130 SAMPLE DUPLICATE: 3685281 Parameter Units 92610193037 Result Dup Result RPD Max RPD Qualifiers 1,2,4-Trichlorobenzene mg/kg ND ND 30 1,2-Dichlorobenzene mg/kg ND ND 30 1,3-Dichlorobenzene mg/kg ND ND 30 1,4-Dichlorobenzene mg/kg ND ND 30 1-Methylnaphthalene mg/kg ND ND 30 2,2'-Oxybis(1-chloropropane) mg/kg ND ND 30 v1 2,4,5-Trichlorophenol mg/kg ND ND 30 2,4,6-Trichlorophenol mg/kg ND ND 30 2,4-Dichlorophenol mg/kg ND ND 30 2,4-Dimethylphenol mg/kg ND ND 30 2,4-Dinitrophenol mg/kg ND ND 30 2,4-Dinitrotoluene mg/kg ND ND 30 2,6-Dinitrotoluene mg/kg ND ND 30 2-Chloronaphthalene mg/kg ND ND 30 2-Chlorophenol mg/kg ND ND 30 2-Methylnaphthalene mg/kg ND ND 30 2-Methylphenol(o-Cresol) mg/kg ND ND 30 2-Nitroaniline mg/kg ND ND 30 2-Nitrophenol mg/kg ND ND 30 3&4-Methyl phenol (m&p Cresol) mg/kg ND ND 30 3,3'-Dichlorobenzidine mg/kg ND ND 30 IL 3-Nitroaniline mg/kg ND ND 30 IL 4,6-Dinitro-2-methyl phenol mg/kg ND ND 30 4-Bromophenylphenyl ether mg/kg ND ND 30 4-ChIoro-3-methyl phenol mg/kg ND ND 30 4-Chloroaniline mg/kg ND ND 30 4-Chlorophenylphenyl ether mg/kg ND ND 30 4-Nitroaniline mg/kg ND ND 301L,v2 4-Nitrophenol mg/kg ND ND 30 v2 Acenaphthene mg/kg ND ND 30 Acenaphthylene mg/kg ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 53 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 SAMPLE DUPLICATE: 3685281 Parameter Units 92610193037 Result Dup Result Aniline mg/kg ND ND Anthracene mg/kg ND ND Benzo(a)anthracene mg/kg ND ND Benzo(a)pyrene mg/kg ND ND Benzo(b)fluoranthene mg/kg ND ND Benzo(g,h,i)perylene mg/kg ND ND Benzo(k)fluoranthene mg/kg ND ND Benzoic Acid mg/kg ND ND Benzyl alcohol mg/kg ND ND bis(2-Chloroethoxy)methane mg/kg ND ND bis(2-Chloroethyl) ether mg/kg ND ND bis(2-Ethylhexyl)phthalate mg/kg ND ND Butylbenzylphthalate mg/kg ND ND Chrysene mg/kg ND ND Di-n-butylphthalate mg/kg ND ND Di-n-octylphthalate mg/kg ND ND Dibenz(a,h)anthracene mg/kg ND ND Dibenzofuran mg/kg ND ND Diethylphthalate mg/kg ND ND Dimethylphthalate mg/kg ND ND Fluoranthene mg/kg ND ND Fluorene mg/kg ND ND Hexachloro-1,3-butadiene mg/kg ND ND Hexachlorobenzene mg/kg ND ND Hexachlorocyclopentadiene mg/kg ND ND Hexachloroethane mg/kg ND ND Indeno(1,2,3-cd)pyrene mg/kg ND ND Isophorone mg/kg ND ND N-Nitroso-di-n-propylamine mg/kg ND ND N-Nitrosodimethylamine mg/kg ND ND N-Nitrosodiphenylamine mg/kg ND ND Naphthalene mg/kg ND ND Nitrobenzene mg/kg ND ND Pentachlorophenol mg/kg ND ND Phenanthrene mg/kg ND ND Phenol mg/kg ND ND Pyrene mg/kg ND ND Pyridine mg/kg ND ND 2,4,6-Tribromophenol (S) % 64 64 2-Fluorobiphenyl (S) % 60 60 2-Fluorophenol(S) % 53 54 Nitrobenzene-d5 (S) % 62 64 Phenol-d6 (S) % 53 54 Terphenyl-d14 (S) % 73 75 Max RPD RPD Qualifiers 30 v2 30 30 30 30 30 30 30 30 v2 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 v2 30 30 30 30 30 30 30 30 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 54 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 QC Batch: 705405 Analysis Method: SW-846 QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 SAMPLE DUPLICATE: 3680912 92610545001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Percent Moisture % 8.5 10.0 16 25 N2 SAMPLE DUPLICATE: 3680913 92610530008 Dup Max Parameter Units Result Result RPD RPD Qualifiers Percent Moisture % 10.9 11.3 3 25 N2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 55 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 QC Batch: 1893124 Analysis Method: SM 2540G QC Batch Method: SM 2540 G Analysis Description: Total Solids 2540 G-2011 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 METHOD BLANK: R3814268-1 Matrix: Solid Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Solids % 0.00100 07/12/22 14:43 LABORATORY CONTROL SAMPLE: R3814268-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Solids % 50.0 50.0 100 85.0-115 SAMPLE DUPLICATE: R3814268-3 L1511858-01 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Solids % 79.7 78.6 1.39 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 56 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610504 QC Batch: 1894241 Analysis Method: EPA 7199 QC Batch Method: 3060A Analysis Description: Wet Chemistry 7199 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 METHOD BLANK: R3816510-1 Matrix: Solid Associated Lab Samples: 92610504001, 92610504002, 92610504003, 92610504004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Chromium, Hexavalent mg/kg ND 1.00 0.255 07/15/22 09:39 LABORATORY CONTROL SAMPLE: R3816510-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chromium, Hexavalent mg/kg 10.0 9.85 98.5 80.0-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3816510-4 R3816510-5 MS MSD L1510486-01 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chromium, Hexavalent mg/kg ND 20.0 20.0 6.29 7.74 31.5 38.7 75.0-125 20.7 20 ML,R1 MATRIX SPIKE SAMPLE: R3816510-7 L1510486-01 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Chromium, Hexavalent mg/kg ND 643 588 91.5 75.0-125 SAMPLE DUPLICATE: R3816510-3 L1507120-33 Dup Max Parameter Units Result Result RPD RPD Qualifiers Chromium, Hexavalent mg/kg ND ND 0.00 20 SAMPLE DUPLICATE: R3816510-8 L1510486-02 Dup Max Parameter Units Result Result RPD RPD Qualifiers Chromium, Hexavalent mg/kg ND ND 0.00 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 57 of 64 Pace Analytical Services, LLC lac, Analyilcal ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: Wright's Executive Sales Pace Project No.: 92610504 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. SAMPLE QUALIFIERS Sample: R3816510-4 Ill Wet Chemistry by Method 7199 - Matrix spike failure due to matrix; sample is a reducer. Sample: R3816510-5 Ill Wet Chemistry by Method 7199 - Matrix spike failure due to matrix; sample is a reducer. ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be considered an estimated value. IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be considered an estimated value. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. ML Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased low. N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditations/certifications is available upon request. P8 Analyte was detected in the method blank. All associated samples had concentrations of at least ten times greater than the blank or were below the reporting limit. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 58 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: Wright's Executive Sales Pace Project No.: 92610504 ANALYTE QUALIFIERS R1 RPD value was outside control limits. v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated samples may have a high bias. v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 59 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: Wright's Executive Sales 92610504 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92610504001 SP-1 3546 1892644 EPA 8141B 1892644 92610504002 SP-2 3546 1892644 EPA 8141B 1892644 92610504003 SP-3 3546 1892644 EPA 8141B 1892644 92610504004 DUP-1 3546 1892644 EPA 8141B 1892644 92610504001 SPA 8151A 1894221 EPA 8151 1894221 92610504002 SP-2 8151A 1894221 EPA 8151 1894221 92610504003 SP-3 8151A 1894221 EPA 8151 1894221 92610504004 DUP-1 8151A 1894221 EPA 8151 1894221 92610504001 SPA EPA 3546 706233 EPA 8081B 706428 92610504002 SP-2 EPA 3546 706233 EPA 8081B 706428 92610504003 SP-3 EPA 3546 706233 EPA 8081B 706428 92610504004 DUP-1 EPA 3546 706233 EPA 8081 B 706428 92610504001 SPA EPA 3050B 743660 EPA 6020B 743829 92610504001 SPA EPA 3050B 743891 EPA 6020B 744354 92610504002 SP-2 EPA 3050B 743660 EPA 6020B 743829 92610504002 SP-2 EPA 3050B 743891 EPA 6020B 744354 92610504003 SP-3 EPA 3050B 743660 EPA 6020B 743829 92610504003 SP-3 EPA 3050B 743891 EPA 6020B 744354 92610504004 DUP-1 EPA 3050B 743660 EPA 6020B 743829 92610504004 DUP-1 EPA 3050B 743891 EPA 6020B 744354 92610504001 SPA METHOD 743747 EPA 7471 B 743877 92610504001 SPA METHOD 744047 EPA 7471B 744162 92610504002 SP-2 METHOD 743747 EPA 7471 B 743877 92610504002 SP-2 METHOD 744047 EPA 7471 B 744162 92610504003 SP-3 METHOD 743747 EPA 7471 B 743877 92610504003 SP-3 METHOD 744047 EPA 7471 B 744162 92610504004 DUP-1 METHOD 743747 EPA 7471 B 743877 92610504004 DUP-1 METHOD 744047 EPA 7471 B 744162 92610504001 SPA EPA 3546 706395 EPA 8270E 707177 92610504002 SP-2 EPA 3546 706395 EPA 8270E 707177 92610504003 SP-3 EPA 3546 706395 EPA 8270E 707177 92610504004 DUP-1 EPA 3546 706395 EPA 8270E 707177 92610504001 SPA EPA 5035A/5030B 705419 EPA 8260D 705605 92610504002 SP-2 EPA 5035A/5030B 705419 EPA 8260D 705605 92610504003 SP-3 EPA 5035A/5030B 705419 EPA 8260D 705605 92610504004 DUP-1 EPA 5035A/5030B 705419 EPA 8260D 705605 92610504001 SPA SW-846 705405 92610504002 SP-2 SW-846 705405 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:24 PM without the written consent of Pace Analytical Services, LLC. Page 60 of 64 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Wright's Executive Sales Pace Project No.: 92610504 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92610504003 SP-3 SW-846 705405 92610504004 DUP-1 SW-846 705405 92610504001 SPA SM 2540 G 1893124 SM 2540G 1893124 92610504002 SP-2 SM 2540 G 1893124 SM 2540G 1893124 92610504003 SP-3 SM 2540 G 1893124 SM 2540G 1893124 92610504004 DUP-1 SM 2540 G 1893124 SM 2540G 1893124 92610504001 SPA 3060A 1894241 EPA 7199 1894241 92610504002 SP-2 3060A 1894241 EPA 7199 1894241 92610504003 SP-3 3060A 1894241 EPA 7199 1894241 92610504004 DUP-1 3060A 1894241 EPA 7199 1894241 Date: 07/21 /2022 05:24 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 61 of 64 Effective Date: 05/12/202205/12/2022 Laboratory receiving samples: Asheville ❑ Eden[] Greenwood Huntersville-0// Raleigh❑ Mechanicsvillel] Atlanta[] Kernersville❑ Sample �• Receipt Project#• Client Name: WO# . 92'610504 � Courier: ❑Fed E . ❑UPs ❑USP5 ❑Client ❑ Commercial Pa ❑other: 92810504 Custody Seal Present? Dyes No Seals intact? ❑Yes / Packing material: ❑Bubble Wrap ble Bags ❑None ❑ other Thermometerzun :.t'l(,. TYpe of Ice: Wet ❑Blue s, �� Correction Factor: Cooler Temp ==tom- Add/subtract (T) V Cooler Temp Corrected (°C): _ USDA Regulated soil (❑ N/A, water sample) Did samples originate in a quarantine one within the United states: CA, NYr or SC (check maps)? []Yes FINo Chain of Custody Present? es No ❑N/A Samples Arrived within Hold Time? s []No , [I NIA Short Hold Time Analysis (c72 hr.)? ❑Yes ❑N/A Flush Turn Around Time Requested? ❑Yes N ❑N/q Sufficient Volume? Ye Na Correct Containers Used? y ❑No EON -Pace Containers Used? s ❑No Containers Intact? Y ❑Na ❑N/A Dissolved analysis: Samples Field Filtered? ❑Yes ❑No Sample Labels Match COC? []No ❑N/A -Includes Date/Time/ID/Analysis Matrix: Headspace inVOAVials (>5-6mm)? Des❑No Trip Blank Present? ❑Yes ❑No Trip Blank Custody Seals Present? ❑Yes Quo COMMENTS/SAMPLE DISCREPANa -C11ENTNOT {FI64T!eN Rf Person -contacted - Project Manager SCURF Review: __._� f9J�tt1413nager_SRF Review.__. . 1. 2. 3. 4. S. 6, 7. 8. 9. Date/Initials Person Examining Content) Biological Tissue Frozen? ❑Yes ❑No N/A ❑None Temp should be above freezing to 6°C ❑samples out of temp criteria. Samples on ice, tooling process has begun j Did samples originate from a foreign source (internatio Ily, inciu6ng Hawaii and Puerto Ricol? ❑Yes �❑N Comm ents/Dlscrenanry `"' Lot ID of splitcontain Date/Time: Date: Field Data Required? ❑Yes Qualtrax ID: 69614 Page 1 of 2 Page 62 of 64 -pace Effective Date: 051121202205/12/2022 *Check mark top half of box if pH and/or dechlorination is verified and project - w01_t ' 92610544 within the acceptance range for preservation samples. PM: AI1B Due Date: 07/01/22 Exceptions: VOA, Conform; TOC, Oil and Gr(ase, DRO/8015 [water), DOC, LLHg CLIEN'r : 92-ECS RAL "Bottom half of box is to list number of bottles ***Check all unpreserved Nitrates for chlorine U A Z U lJ v Q Z 2 0. c 7 Ll N �v E N0N O z m ¢ ll N ra i E o M m z m c V N ro a E o N m Z v `^ ¢ c U "n o d _ .-1 m CV v a rq O Y u h 'c J E rn �T 4 m v M z x V a E o NNN—LA Z M m °� 2 4 Q 2 " N ee 7 _J E +n N a m r�8L n = x z V N ro ii J E°' 'M m eo M L O E LL 3 z v 01 w m c O! E ¢ •- ti a r� v _ u = N a E Q •`-' _ N a v i' � Cl E a o !�Iam a a O N x y A E Q ° N a ne v CIL Q z Q7 Ja E a 1 E 0 f M a u Q Z U It 2 z 01 M E a J E o to .7 a z t,] = ¢ � E O T ¢ z m D '^ p z ¢ o a E p O~i ¢ 2 ti v m `p, C Q a a E O C=1 = Z Q a M 4 v J E O a 2 v Q N 2 Q o 1 E 6 d�l p z m 9 , 74 c ' Y as ro I z CL .y � E �1 n m I ¢ Z L .� � E O i, rn a Q M = z U a Ein ONE 0.''E aPE m ? y Z v, v c 7 E Q 2 v m c o ,,p Lq m a v ? v°1i i o c n 1 7 1 3 5 6 7 8 5 10 11 11Z I pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot # NULL. vviit: It!ver mere is a vlscrepancy arrecung Ivor[n k-aronna compndnce samples, a copy or in IS rorm win pe sent to the North Carokna DEN RCertification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Qualtrax ID: 69614 Page 2 of 2 Page 63 of 64 ace CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fieids must be completed a curately. Submitting a sample via this chain of custody constitutes acknowledgment and acceptance of the Pace Terms and Conditions found at htips://info.pacelabs.com/hubfs/pas-standard-terms.pdf. Section A Section B Section C Required Client Information: Required Project Information: Invoice Information: Company: ECS Southeast. LLP Report To: Ron Navarro Attention: Pa e : 1 Of 1 Address: 5260 Greens Dairy Road Copy To: Company Name: Raleigh, NC 27616 Address: Email: RNavarro@ecslimited.Com Purchase Order #: Pace Quote: Regulatory Agency Phone: 919-861-9846 JFax Project Name: Wright's Executive Sales 49:10039-B Pace Project Manager: an ela.baicni g @pacelabs.com, State f Qocation Requested Due Date: ri • Project #: '� " -• L7 Pace Profile #: 15467- NC Requested Analysis Filtered YIN i — Q � MATRIX CODE COLLECTED = Preservatives DN�kirq wetm Dw a o werer WT $ Waate Wet- Ww _ q tj J SAMPLE ID Protlurt P acillsolld K v 6 Z } oli aL START ENQ One Character per box. wipe WP w w f A-Z 0-9 1, -] Air AR oo = a a m V g `o Sample Ids must be unique P 0. om- or u T.—rs x w z Z ro ?` o c w o a to O a U 6 LU < U m M m vJ = D n Q 0 O N v C o 0 0 Q a}� r DATE TJME DATE TIME M s i z z O t/ ob-z' 2-2— o isi 1h.� p - 3 p`!YO11 �- l 4 „rJ 6 7 8 9 10 I 11 12 j ADDITIONAL COMMENTS RELINQUISHED BY 1 AFFILIATION DATE TIME ACCEPTED BY 1 AFFILIATION TIME SAMPLE CONDITIONS IPLER NAME AND SIGNATURE PRINT Name of SAMPLER: y� cq SIGNATURE of SAMPLER: { t A I U o Red: z 61 a z E z v to 0 v r9 N m 11 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 July 21, 2022 Samantha M. Szakasits, G.I.T. ECS Southeast, LLP 5260 Greens Dary Road Raleigh, NC 27616 RE: Project: Wright's Executive Sales Pace Project No.: 92610717 Dear Samantha Szakasits, G.I.T.: Enclosed are the analytical results for sample(s) received by the laboratory on June 17, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Gulf Coast • Pace National - Mt. Juliet • Pace Analytical Services - Charlotte Revised to include MDL's and J Flags per client request 07/21/22. If you have any questions concerning this report, please feel free to contact me. Sincerely, cL,+1,1- Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Austin Deans, ECS ECS Southeast Reporting, ECS Southeast Scott Werley, ECS Southeast, LLP REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 72 lacieAnalyfica(' www,pacelabs.com Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Wright's Executive Sales Pace Project No.: 92610717 Pace Analytical Services National 12065 Lebanon Road, Mt. Juliet, TN 37122 Alabama Certification #: 40660 Alaska Certification 17-026 Arizona Certification #: AZ0612 Arkansas Certification #: 88-0469 California Certification #: 2932 Canada Certification #: 1461.01 Colorado Certification #: TN00003 Connecticut Certification #: PH-0197 DOD Certification: #1461.01 EPA# TN00003 Florida Certification #: E87487 Georgia DW Certification #: 923 Georgia Certification: NELAP Idaho Certification #: TN00003 Illinois Certification #: 200008 Indiana Certification #: C-TN-01 Iowa Certification #: 364 Kansas Certification #: E-10277 Kentucky UST Certification #: 16 Kentucky Certification #: 90010 Louisiana Certification #: A130792 Louisiana DW Certification #: LA180010 Maine Certification #: TN0002 Maryland Certification #: 324 Massachusetts Certification #: M-TNO03 Michigan Certification #: 9958 Minnesota Certification #: 047-999-395 Mississippi Certification #: TN00003 Missouri Certification #: 340 Montana Certification M CERT0086 Nebraska Certification #: NE-OS-15-05 Pace Analytical Gulf Coast 7979 Innovation Park Drive, Baton Rouge, LA 70820 Arkansas Certification #: 88-0655 DoD ELAP Certification M 6429-01 Florida Certification #: E87854 Illinois Certification #: 004585 Kansas Certification #: E-10354 Louisiana/LELAP Certification #: 01955 North Carolina Certification M 618 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 CERTIFICATIONS Nevada Certification #: TN-03-2002-34 New Hampshire Certification #: 2975 New Jersey Certification #: TNO02 New Mexico DW Certification New York Certification #: 11742 North Carolina Aquatic Toxicity Certification #: 41 North Carolina Drinking Water Certification #: 21704 North Carolina Environmental Certificate #: 375 North Dakota Certification #: R-140 Ohio VAP Certification #: CL0069 Oklahoma Certification #: 9915 Oregon Certification #: TN200002 Pennsylvania Certification #: 68-02979 Rhode Island Certification #: LA000356 South Carolina Certification #: 84004 South Dakota Certification Tennessee DW/Chem/Micro Certification #: 2006 Texas Certification #: T 104704245-17-14 Texas Mold Certification #: LAB0152 USDA Soil Permit #: P330-15-00234 Utah Certification #: TN00003 Virginia Certification #: VT2006 Vermont Dept. of Health: ID# VT-2006 Virginia Certification #: 460132 Washington Certification #: C847 West Virginia Certification #: 233 Wisconsin Certification #: 998093910 Wyoming UST Certification #: via A21LA 2926.01 A21-A-ISO 17025 Certification #: 1461.01 A21-A-ISO 17025 Certification #: 1461.02 AIHA-LAP/LLC EMLAP Certification #:100789 North Dakota Certification #: R-195 Oklahoma Certification #: 2019-101 South Carolina Certification #: 73006001 Texas Certification #: T104704178-19-11 USDA Soil Permit # P330-19-00209 Virginia Certification #: 460215 Washington Certification #: C929 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: Wright's Executive Sales Pace Project No.: 92610717 Lab ID Sample ID Matrix Date Collected Date Received 92610717001 UT-1 Solid 06/17/22 08:15 06/17/22 16:56 92610717002 UT4 Solid 06/17/2215:30 06/17/22 16:56 92610717003 DUP-2 Solid 06/17/22 00:00 06/17/22 16:56 92610717004 BG-1 Solid 06/17/22 09:10 06/17/22 16:56 92610717005 13G-2 Solid 06/17/22 09:20 06/17/22 16:56 92610717006 13G-3 Solid 06/17/22 09:45 06/17/22 16:56 92610717007 13G-4 Solid 06/17/22 09:45 06/17/22 16:56 92610717008 13G-5 Solid 06/17/2210:15 06/17/22 16:56 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: Wright's Executive Sales 92610717 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92610717001 UT-1 EPA 8141B HMH 27 PAN EPA 8151 HMH 11 PAN EPA 8081 B BAJ 24 PASI-C EPA 6020E LWZ 7 GCLA EPA 7471 B TDM 1 GCLA EPA 8270E BPJ 75 PASI-C EPA 8260D LMB 70 PASI-C SW-846 KDF 1 PASI-C SM 2540G CMK 1 PAN EPA 7199 ERP 1 PAN 92610717002 UT-4 EPA 8141B HMH 27 PAN EPA 8151 HMH 11 PAN EPA 8081 B BAJ 24 PASI-C EPA 6020E LWZ 7 GCLA EPA 7471 B TDM 1 GCLA EPA 8270E BPJ 75 PASI-C EPA 8260D LMB 70 PASI-C SW-846 KDF 1 PASI-C SM 2540G CMK 1 PAN EPA 7199 ERP 1 PAN 92610717003 DUP-2 EPA 8141B HMH 27 PAN EPA 8151 HMH 11 PAN EPA 8081 B BAJ 24 PASI-C EPA 6020E LWZ 7 GCLA EPA 7471 B TDM 1 GCLA EPA 8270E BPJ 75 PASI-C EPA 8260D LMB 70 PASI-C SW-846 KDF 1 PASI-C SM 2540G CMK 1 PAN EPA 7199 ERP 1 PAN 92610717004 BG-1 EPA 8141B HMH 27 PAN EPA 8151 HMH 11 PAN EPA 8081 B BAJ 24 PASI-C SW-846 KDF 1 PASI-C SM 2540G CMK 1 PAN 92610717005 BG-2 EPA 8141B HMH 27 PAN EPA 8151 HMH 11 PAN REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Wright's Executive Sales Pace Project No.: 92610717 Analytes Lab ID Sample ID Method Analysts Reported Laboratory EPA 8081 B BAJ 24 PASI-C SW-846 KDF 1 PASI-C SM 2540G CMK 1 PAN 92610717006 BG-3 EPA 8141B HMH 27 PAN EPA 8151 HMH 11 PAN EPA 8081 B BAJ 24 PASI-C SW-846 KDF 1 PASI-C SM 2540G CMK 1 PAN 92610717007 BG-4 EPA 8141B HMH 27 PAN EPA 8151 HMH 11 PAN EPA 8081 B BAJ 24 PASI-C SW-846 KDF 1 PASI-C SM 2540G CMK 1 PAN 92610717008 BG-5 EPA 8141B HMH 27 PAN EPA 8151 HMH 11 PAN EPA 8081 B BAJ 24 PASI-C SW-846 KDF 1 PASI-C SM 2540G CMK 1 PAN GCLA = Pace Analytical Gulf Coast PAN = Pace National - Mt. Juliet PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: UT-1 Lab ID: 92610717001 Collected: 06/17/22 08:15 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual OP Pesticides 8141 B Analytical Method: EPA 8141 B Preparation Method: 3546 Pace National - Mt. Juliet Azinphos, methyl (Guthion) ND mg/kg 0.126 0.0399 1 06/23/22 16:09 06/24/22 02:55 86-50-0 Bolstar ND mg/kg 0.126 0.0187 1 06/23/22 16:09 06/24/22 02:55 35400-43-2 Chlorpyrifos ND mg/kg 0.126 0.0197 1 06/23/22 16:09 06/24/22 02:55 2921-88-2 Coumaphos ND mg/kg 0.126 0.0305 1 06/23/22 16:09 06/24/22 02:55 56-72-4 Total Demeton ND mg/kg 0.0879 0.00733 1 06/23/22 16:09 06/24/22 02:55 8065-48-3 Diazinon ND mg/kg 0.126 0.0282 1 06/23/22 16:09 06/24/22 02:55 333-41-5 Dichlorvos ND mg/kg 0.126 0.0377 1 06/23/22 16:09 06/24/22 02:55 62-73-7 Dimethoate ND mg/kg 0.126 0.0419 1 06/23/22 16:09 06/24/22 02:55 60-51-5 Disulfoton ND mg/kg 0.126 0.0319 1 06/23/22 16:09 06/24/22 02:55 298-04-4 EPN (ENT) ND mg/kg 0.126 0.0347 1 06/23/22 16:09 06/24/22 02:55 2104-64-5 Ethoprop ND mg/kg 0.126 0.0148 1 06/23/22 16:09 06/24/22 02:55 13194-48-4 Parathion (Ethyl parathion) ND mg/kg 0.126 0.0206 1 06/23/22 16:09 06/24/22 02:55 56-38-2 Fensulfothion ND mg/kg 0.126 0.0443 1 06/23/22 16:09 06/24/22 02:55 115-90-2 Fenthion ND mg/kg 0.126 0.0167 1 06/23/22 16:09 06/24/22 02:55 55-38-9 Malathion ND mg/kg 0.126 0.0225 1 06/23/22 16:09 06/24/22 02:55 121-75-5 Merphos ND mg/kg 0.126 0.0291 1 06/23/22 16:09 06/24/22 02:55 150-50-5 Methyl parathion ND mg/kg 0.126 0.0255 1 06/23/22 16:09 06/24/22 02:55 298-00-0 Mevinphos ND mg/kg 0.126 0.0289 1 06/23/22 16:09 06/24/22 02:55 7786-34-7 Naled ND mg/kg 0.126 0.0603 1 06/23/22 16:09 06/24/22 02:55 300-76-5 Phorate ND mg/kg 0.126 0.0264 1 06/23/22 16:09 06/24/22 02:55 298-02-2 Ronnel ND mg/kg 0.126 0.0187 1 06/23/22 16:09 06/24/22 02:55 299-84-3 Stirophos (Tetrachlorvinphos) ND mg/kg 0.126 0.0223 1 06/23/22 16:09 06/24/22 02:55 22248-79-9 Sulfotepp (ThiodiphosphoricAc ND mg/kg 0.126 0.0124 1 06/23/22 16:09 06/24/22 02:55 3689-24-5 TEPP ND mg/kg 1.26 0.197 1 06/23/22 16:09 06/24/22 02:55 107-49-3 Tokuthion (Prothiofos) ND mg/kg 0.126 0.0188 1 06/23/22 16:09 06/24/22 02:55 34643-46-4 Trichloronate ND mg/kg 0.126 0.0252 1 06/23/22 16:09 06/24/22 02:55 327-98-0 Surrogates Triphenylphosphate (S) 72.5 % 36.0-121 1 06/23/22 16:09 06/24/22 02:55 115-86-6 Chlorinated Herb. (GC) 8151 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND mg/kg 0.0879 0.00881 1 06/29/2214:20 07/01/2215:37 94-75-7 Dalapon ND mg/kg 0.0879 0.0142 1 06/29/2214:20 07/01/2215:37 127-20-8 2,4-DB ND mg/kg 0.0879 0.0373 1 06/29/2214:20 07/01/2215:37 94-82-6 Dicamba ND mg/kg 0.0879 0.0197 1 06/29/2214:20 07/01/2215:37 1918-00-9 Dichloroprop ND mg/kg 0.0879 0.0308 1 06/29/2214:20 07/01/2215:37 15165-67-0 Dinoseb ND mg/kg 0.0879 0.00875 1 06/29/2214:20 07/01/2215:37 88-85-7 MCPA ND mg/kg 8.16 0.556 1 06/29/2214:20 07/01/2215:37 94-74-6 MCPP ND mg/kg 8.16 0.461 1 06/29/2214:20 07/01/2215:37 7085-19-0 2,4,5-T ND mg/kg 0.0879 0.0107 1 06/29/2214:20 07/01/2215:37 93-76-5 2,4,5-TP (Silvex) ND mg/kg 0.0879 0.0134 1 06/29/22 14:20 07/01/22 15:37 93-72-1 Surrogates 2,4-DCAA(S) 76.0 % 22.0-132 1 06/29/2214:20 07/01/2215:37 19719-28-9 REPORT OF LABORATORY ANALYSIS LO This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: UT-1 Lab ID: 92610717001 Collected: 06/17/22 08:15 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 B Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Aldrin ND mg/kg 0.024 0.0099 10 06/22/22 16:23 06/27/22 15:16 309-00-2 alpha-BHC ND mg/kg 0.024 0.011 10 06/22/22 16:23 06/27/22 15:16 319-84-6 beta-BHC ND mg/kg 0.024 0.012 10 06/22/22 16:23 06/27/22 15:16 319-85-7 delta-BHC ND mg/kg 0.024 0.012 10 06/22/22 16:23 06/27/22 15:16 319-86-8 gamma-BHC (Lindane) ND mg/kg 0.024 0.0098 10 06/22/22 16:23 06/27/22 15:16 58-89-9 Chlordane (Technical) ND mg/kg 0.12 0.11 10 06/22/22 16:23 06/27/22 15:16 57-74-9 4,4'-DDD ND mg/kg 0.024 0.011 10 06/22/22 16:23 06/27/22 15:16 72-54-8 4,4'-DDE ND mg/kg 0.024 0.012 10 06/22/22 16:23 06/27/22 15:16 72-55-9 4,4'-DDT ND mg/kg 0.024 0.011 10 06/22/22 16:23 06/27/22 15:16 50-29-3 Dieldrin ND mg/kg 0.024 0.011 10 06/22/22 16:23 06/27/22 15:16 60-57-1 Endosulfan I ND mg/kg 0.024 0.010 10 06/22/22 16:23 06/27/22 15:16 959-98-8 Endosulfan 11 ND mg/kg 0.024 0.011 10 06/22/22 16:23 06/27/22 15:16 33213-65-9 Endosulfan sulfate ND mg/kg 0.024 0.014 10 06/22/22 16:23 06/27/22 15:16 1031-07-8 Endrin ND mg/kg 0.024 0.011 10 06/22/22 16:23 06/27/22 15:16 72-20-8 Endrin aldehyde ND mg/kg 0.024 0.016 10 06/22/22 16:23 06/27/22 15:16 7421-93-4 Endrin ketone ND mg/kg 0.024 0.013 10 06/22/22 16:23 06/27/22 15:16 53494-70-5 Heptachlor ND mg/kg 0.024 0.011 10 06/22/22 16:23 06/27/22 15:16 76-44-8 Heptachlor epoxide ND mg/kg 0.024 0.0097 10 06/22/22 16:23 06/27/22 15:16 1024-57-3 Hexachlorobenzene ND mg/kg 0.024 0.010 10 06/22/22 16:23 06/27/22 15:16 118-74-1 Methoxychlor ND mg/kg 0.061 0.030 10 06/22/22 16:23 06/27/22 15:16 72-43-5 Mirex ND mg/kg 0.061 0.027 10 06/22/22 16:23 06/27/22 15:16 2385-85-5 Toxaphene ND mg/kg 0.085 0.065 10 06/22/22 16:23 06/27/22 15:16 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 0 % 10-133 10 06/22/22 16:23 06/27/22 15:16 877-09-8 D3,S4 Decachlorobiphenyl (S) 0 % 10-146 10 06/22/22 16:23 06/27/22 15:16 2051-24-3 S4 EPA 6020B Analytical Method: EPA 6020E Preparation Method: EPA 3050B Pace Analytical Gulf Coast Arsenic 0.72 mg/kg 0.48 0.12 10 06/26/22 09:00 06/29/22 20:10 7440-38-2 Barium 39.7 mg/kg 0.48 0.12 10 06/26/22 09:00 06/29/22 20:10 7440-39-3 Cadmium ND mg/kg 0.48 0.12 10 06/26/22 09:00 06/29/22 20:10 7440-43-9 Chromium 11.2 mg/kg 0.48 0.12 10 06/26/22 09:00 06/29/22 20:10 7440-47-3 Lead 9.86 mg/kg 0.48 0.12 10 06/26/22 09:00 06/29/22 20:10 7439-92-1 Selenium ND mg/kg 0.48 0.12 10 06/26/22 09:00 06/29/22 20:10 7782-49-2 Silver ND mg/kg 0.48 0.12 10 06/26/22 09:00 06/29/22 20:10 7440-22-4 EPA 7471 B Analytical Method: EPA 7471 B Preparation Method: METHOD Pace Analytical Gulf Coast Mercury 0.025 mg/kg 0.015 0.0060 1 06/24/2211:30 06/27/2212:28 7439-97-6 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND mg/kg 4.1 1.4 10 06/23/2217:52 06/30/2214:14 83-32-9 Acenaphthylene ND mg/kg 4.1 1.4 10 06/23/2217:52 06/30/2214:14 208-96-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: UT-1 Lab ID: 92610717001 Collected: 06/17/22 08:15 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Aniline ND mg/kg 4.1 1.6 10 06/23/22 17:52 06/30/22 14:14 62-53-3 Anthracene ND mg/kg 4.1 1.3 10 06/23/22 17:52 06/30/22 14:14 120-12-7 Benzo(a)anthracene ND mg/kg 4.1 1.4 10 06/23/22 17:52 06/30/22 14:14 56-55-3 Benzo(a)pyrene ND mg/kg 4.1 1.4 10 06/23/22 17:52 06/30/22 14:14 50-32-8 Benzo(b)fluoranthene ND mg/kg 4.1 1.4 10 06/23/22 17:52 06/30/22 14:14 205-99-2 Benzo(g,h,i)perylene ND mg/kg 4.1 1.6 10 06/23/22 17:52 06/30/22 14:14 191-24-2 Benzo(k)fluoranthene ND mg/kg 4.1 1.4 10 06/23/22 17:52 06/30/22 14:14 207-08-9 Benzoic Acid ND mg/kg 20.5 8.8 10 06/23/22 17:52 06/30/22 14:14 65-85-0 Benzyl alcohol ND mg/kg 8.2 3.1 10 06/23/22 17:52 06/30/22 14:14 100-51-6 4-Bromophenylphenyl ether ND mg/kg 4.1 1.6 10 06/23/22 17:52 06/30/22 14:14 101-55-3 Butylbenzylphthalate ND mg/kg 4.1 1.7 10 06/23/22 17:52 06/30/22 14:14 85-68-7 4-Chloro-3-methyl phenol ND mg/kg 8.2 2.9 10 06/23/22 17:52 06/30/22 14:14 59-50-7 4-Chloroaniline ND mg/kg 8.2 3.2 10 06/23/22 17:52 06/30/22 14:14 106-47-8 bis(2-Chloroethoxy)methane ND mg/kg 4.1 1.7 10 06/23/22 17:52 06/30/22 14:14 111-91-1 bis(2-Chloroethyl) ether ND mg/kg 4.1 1.5 10 06/23/22 17:52 06/30/22 14:14 111-44-4 2-Chloronaphthalene ND mg/kg 4.1 1.6 10 06/23/22 17:52 06/30/22 14:14 91-58-7 2-Chlorophenol ND mg/kg 4.1 1.5 10 06/23/22 17:52 06/30/22 14:14 95-57-8 4-Chlorophenylphenyl ether ND mg/kg 4.1 1.5 10 06/23/22 17:52 06/30/22 14:14 7005-72-3 Chrysene ND mg/kg 4.1 1.5 10 06/23/22 17:52 06/30/22 14:14 218-01-9 Dibenz(a,h)anthracene ND mg/kg 4.1 1.6 10 06/23/22 17:52 06/30/22 14:14 53-70-3 Dibenzofuran ND mg/kg 4.1 1.5 10 06/23/22 17:52 06/30/22 14:14 132-64-9 1,2-Dichlorobenzene ND mg/kg 4.1 1.5 10 06/23/22 17:52 06/30/22 14:14 95-50-1 1,3-Dichlorobenzene ND mg/kg 4.1 1.5 10 06/23/22 17:52 06/30/22 14:14 541-73-1 1,4-Dichlorobenzene ND mg/kg 4.1 1.6 10 06/23/22 17:52 06/30/22 14:14 106-46-7 3,3'-Dichlorobenzidine ND mg/kg 8.2 2.8 10 06/23/22 17:52 06/30/22 14:14 91-94-1 IL 2,4-Dichlorophenol ND mg/kg 4.1 1.6 10 06/23/22 17:52 06/30/22 14:14 120-83-2 Diethylphthalate ND mg/kg 4.1 1.5 10 06/23/22 17:52 06/30/22 14:14 84-66-2 2,4-Dimethylphenol ND mg/kg 4.1 1.7 10 06/23/22 17:52 06/30/22 14:14 105-67-9 Dimethylphthalate ND mg/kg 4.1 1.5 10 06/23/22 17:52 06/30/22 14:14 131-11-3 Di-n-butylphthalate ND mg/kg 4.1 1.4 10 06/23/22 17:52 06/30/22 14:14 84-74-2 4,6-Dinitro-2-methyl phenol ND mg/kg 8.2 3.8 10 06/23/22 17:52 06/30/22 14:14 534-52-1 2,4-Dinitrophenol ND mg/kg 20.5 12.7 10 06/23/22 17:52 06/30/22 14:14 51-28-5 2,4-Dinitrotoluene ND mg/kg 4.1 1.6 10 06/23/22 17:52 06/30/22 14:14 121-14-2 2,6-Dinitrotoluene ND mg/kg 4.1 1.5 10 06/23/22 17:52 06/30/22 14:14 606-20-2 Di-n-octylphthalate ND mg/kg 4.1 1.6 10 06/23/22 17:52 06/30/22 14:14 117-84-0 bis(2- Ethyl hexyl)phthalate ND mg/kg 4.1 1.6 10 06/23/22 17:52 06/30/22 14:14 117-81-7 Fluoranthene ND mg/kg 4.1 1.4 10 06/23/22 17:52 06/30/22 14:14 206-44-0 Fluorene ND mg/kg 4.1 1.4 10 06/23/22 17:52 06/30/22 14:14 86-73-7 Hexachloro-1,3-butadiene ND mg/kg 4.1 1.8 10 06/23/22 17:52 06/30/22 14:14 87-68-3 Hexachlorobenzene ND mg/kg 4.1 1.6 10 06/23/22 17:52 06/30/22 14:14 118-74-1 Hexachlorocyclopentadiene ND mg/kg 4.1 2.3 10 06/23/22 17:52 06/30/22 14:14 77-47-4 L2,v2 Hexachloroethane ND mg/kg 4.1 1.6 10 06/23/22 17:52 06/30/22 14:14 67-72-1 Indeno(1,2,3-cd)pyrene ND mg/kg 4.1 1.6 10 06/23/22 17:52 06/30/22 14:14 193-39-5 Isophorone ND mg/kg 4.1 1.8 10 06/23/22 17:52 06/30/22 14:14 78-59-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: UT-1 Lab ID: 92610717001 Collected: 06/17/22 08:15 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 1-Methylnaphthalene ND mg/kg 4.1 1.4 10 06/23/22 17:52 06/30/22 14:14 90-12-0 2-Methylnaphthalene ND mg/kg 4.1 1.6 10 06/23/22 17:52 06/30/22 14:14 91-57-6 2-Methylphenol(o-Cresol) ND mg/kg 4.1 1.7 10 06/23/22 17:52 06/30/22 14:14 95-48-7 3&4-Methyl phenol (m&p Cresol) ND mg/kg 4.1 1.6 10 06/23/22 17:52 06/30/22 14:14 15831-10-4 Naphthalene ND mg/kg 4.1 1.4 10 06/23/22 17:52 06/30/22 14:14 91-20-3 2-Nitroaniline ND mg/kg 20.5 3.3 10 06/23/22 17:52 06/30/22 14:14 88-74-4 3-Nitroaniline ND mg/kg 20.5 3.2 10 06/23/22 17:52 06/30/22 14:14 99-09-2 4-Nitroaniline ND mg/kg 8.2 3.1 10 06/23/22 17:52 06/30/22 14:14 100-01-6 Nitrobenzene ND mg/kg 4.1 1.9 10 06/23/22 17:52 06/30/22 14:14 98-95-3 2-Nitrophenol ND mg/kg 4.1 1.8 10 06/23/22 17:52 06/30/22 14:14 88-75-5 4-Nitrophenol ND mg/kg 20.5 7.9 10 06/23/22 17:52 06/30/22 14:14 100-02-7 N-Nitrosodimethylamine ND mg/kg 4.1 1.4 10 06/23/22 17:52 06/30/22 14:14 62-75-9 N-Nitroso-di-n-propylamine ND mg/kg 4.1 1.5 10 06/23/22 17:52 06/30/22 14:14 621-64-7 N-Nitrosodiphenylamine ND mg/kg 4.1 1.5 10 06/23/22 17:52 06/30/22 14:14 86-30-6 2,2'-Oxybis(1-chloropropane) ND mg/kg 4.1 1.9 10 06/23/22 17:52 06/30/22 14:14 108-60-1 Pentachlorophenol ND mg/kg 8.2 4.0 10 06/23/22 17:52 06/30/22 14:14 87-86-5 v2 Phenanthrene ND mg/kg 4.1 1.3 10 06/23/22 17:52 06/30/22 14:14 85-01-8 Phenol ND mg/kg 4.1 1.8 10 06/23/22 17:52 06/30/22 14:14 108-95-2 Pyrene ND mg/kg 4.1 1.7 10 06/23/22 17:52 06/30/22 14:14 129-00-0 Pyridine ND mg/kg 4.1 1.3 10 06/23/22 17:52 06/30/22 14:14 110-86-1 1,2,4-Trichlorobenzene ND mg/kg 4.1 1.6 10 06/23/22 17:52 06/30/22 14:14 120-82-1 2,4,5-Trichlorophenol ND mg/kg 4.1 1.9 10 06/23/22 17:52 06/30/22 14:14 95-95-4 2,4,6-Trichlorophenol ND mg/kg 4.1 1.7 10 06/23/22 17:52 06/30/22 14:14 88-06-2 Surrogates Nitrobenzene-d5 (S) 0 % 21-130 10 06/23/22 17:52 06/30/22 14:14 4165-60-0 D3,S4 2-Fluorobiphenyl (S) 0 % 19-130 10 06/23/22 17:52 06/30/22 14:14 321-60-8 S4 Terphenyl-d14 (S) 0 % 15-130 10 06/23/22 17:52 06/30/22 14:14 1718-51-0 S4 Phenol-d6 (S) 0 % 18-130 10 06/23/22 17:52 06/30/22 14:14 13127-88-3 S4 2-Fluorophenol (S) 0 % 18-130 10 06/23/22 17:52 06/30/22 14:14 367-12-4 S4 2,4,6-Tribromophenol (S) 0 % 18-130 10 06/23/22 17:52 06/30/22 14:14 118-79-6 S4 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Acetone ND mg/kg 0.14 0.046 1 06/21/22 23:08 06/22/22 06:54 67-64-1 v2 Benzene ND mg/kg 0.0071 0.0028 1 06/21/22 23:08 06/22/22 06:54 71-43-2 Bromobenzene ND mg/kg 0.0071 0.0023 1 06/21/22 23:08 06/22/22 06:54 108-86-1 Bromochloromethane ND mg/kg 0.0071 0.0021 1 06/21/22 23:08 06/22/22 06:54 74-97-5 Bromodichloromethane ND mg/kg 0.0071 0.0027 1 06/21/22 23:08 06/22/22 06:54 75-27-4 Bromoform ND mg/kg 0.0071 0.0025 1 06/21/22 23:08 06/22/22 06:54 75-25-2 Bromomethane ND mg/kg 0.014 0.011 1 06/21/22 23:08 06/22/22 06:54 74-83-9 IK 2-Butanone (MEK) 0.044J mg/kg 0.14 0.034 1 06/21/22 23:08 06/22/22 06:54 78-93-3 v2 n-Butylbenzene ND mg/kg 0.0071 0.0034 1 06/21/22 23:08 06/22/22 06:54 104-51-8 sec-Butylbenzene ND mg/kg 0.0071 0.0031 1 06/21/22 23:08 06/22/22 06:54 135-98-8 tert-Butyl benzene ND mg/kg 0.0071 0.0025 1 06/21/22 23:08 06/22/22 06:54 98-06-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: UT-1 Lab ID: 92610717001 Collected: 06/17/22 08:15 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Carbon tetrachloride ND mg/kg 0.0071 0.0027 1 06/21/22 23:08 06/22/22 06:54 56-23-5 Chlorobenzene ND mg/kg 0.0071 0.0014 1 06/21/22 23:08 06/22/22 06:54 108-90-7 Chloroethane ND mg/kg 0.014 0.0055 1 06/21/22 23:08 06/22/22 06:54 75-00-3 Chloroform ND mg/kg 0.0071 0.0043 1 06/21/22 23:08 06/22/22 06:54 67-66-3 Chloromethane ND mg/kg 0.014 0.0060 1 06/21/22 23:08 06/22/22 06:54 74-87-3 2-Chlorotoluene ND mg/kg 0.0071 0.0025 1 06/21/22 23:08 06/22/22 06:54 95-49-8 4-Chlorotoluene ND mg/kg 0.0071 0.0013 1 06/21/22 23:08 06/22/22 06:54 106-43-4 1,2-Dibromo-3-chloropropane ND mg/kg 0.0071 0.0028 1 06/21/22 23:08 06/22/22 06:54 96-12-8 Dibromochloromethane ND mg/kg 0.0071 0.0040 1 06/21/22 23:08 06/22/22 06:54 124-48-1 1,2-Dibromoethane (EDB) ND mg/kg 0.0071 0.0031 1 06/21/22 23:08 06/22/22 06:54 106-93-4 Dibromomethane ND mg/kg 0.0071 0.0015 1 06/21/22 23:08 06/22/22 06:54 74-95-3 1,2-Dichlorobenzene ND mg/kg 0.0071 0.0026 1 06/21/22 23:08 06/22/22 06:54 95-50-1 1,3-Dichlorobenzene ND mg/kg 0.0071 0.0022 1 06/21/22 23:08 06/22/22 06:54 541-73-1 1,4-Dichlorobenzene ND mg/kg 0.0071 0.0018 1 06/21/22 23:08 06/22/22 06:54 106-46-7 Dichlorodifluoromethane ND mg/kg 0.014 0.0031 1 06/21/22 23:08 06/22/22 06:54 75-71-8 1,1-Dichloroethane ND mg/kg 0.0071 0.0029 1 06/21/22 23:08 06/22/22 06:54 75-34-3 1,2-Dichloroethane ND mg/kg 0.0071 0.0047 1 06/21/22 23:08 06/22/22 06:54 107-06-2 1,1-Dichloroethene ND mg/kg 0.0071 0.0029 1 06/21/22 23:08 06/22/22 06:54 75-35-4 cis-1,2-Dichloroethene ND mg/kg 0.0071 0.0024 1 06/21/22 23:08 06/22/22 06:54 156-59-2 trans-1,2-Dichloroethene ND mg/kg 0.0071 0.0025 1 06/21/22 23:08 06/22/22 06:54 156-60-5 1,2-Dichloropropane ND mg/kg 0.0071 0.0021 1 06/21/22 23:08 06/22/22 06:54 78-87-5 1,3-Dichloropropane ND mg/kg 0.0071 0.0022 1 06/21/22 23:08 06/22/22 06:54 142-28-9 2,2-Dichloropropane ND mg/kg 0.0071 0.0023 1 06/21/22 23:08 06/22/22 06:54 594-20-7 1,1-Dichloropropene ND mg/kg 0.0071 0.0034 1 06/21/22 23:08 06/22/22 06:54 563-58-6 cis-1,3-Dichloropropene ND mg/kg 0.0071 0.0019 1 06/21/22 23:08 06/22/22 06:54 10061-01-5 trans- 1,3-Dichloropropene ND mg/kg 0.0071 0.0024 1 06/21/22 23:08 06/22/22 06:54 10061-02-6 Diisopropyl ether ND mg/kg 0.0071 0.0019 1 06/21/22 23:08 06/22/22 06:54 108-20-3 Ethylbenzene ND mg/kg 0.0071 0.0033 1 06/21/22 23:08 06/22/22 06:54 100-41-4 Hexachloro-1,3-butadiene ND mg/kg 0.014 0.012 1 06/21/22 23:08 06/22/22 06:54 87-68-3 2-Hexanone ND mg/kg 0.071 0.0069 1 06/21/22 23:08 06/22/22 06:54 591-78-6 Isopropylbenzene (Cumene) ND mg/kg 0.0071 0.0024 1 06/21/22 23:08 06/22/22 06:54 98-82-8 p-Isopropyltoluene ND mg/kg 0.0071 0.0035 1 06/21/22 23:08 06/22/22 06:54 99-87-6 Methylene Chloride ND mg/kg 0.028 0.019 1 06/21/22 23:08 06/22/22 06:54 75-09-2 4-Methyl-2-pentanone (MIBK) ND mg/kg 0.071 0.0069 1 06/21/22 23:08 06/22/22 06:54 108-10-1 Methyl-tert-butyl ether ND mg/kg 0.0071 0.0027 1 06/21/22 23:08 06/22/22 06:54 1634-04-4 Naphthalene ND mg/kg 0.0071 0.0037 1 06/21/22 23:08 06/22/22 06:54 91-20-3 n-Propylbenzene ND mg/kg 0.0071 0.0025 1 06/21/22 23:08 06/22/22 06:54 103-65-1 Styrene ND mg/kg 0.0071 0.0019 1 06/21/22 23:08 06/22/22 06:54 100-42-5 1,1,1,2-Tetrachloroethane ND mg/kg 0.0071 0.0027 1 06/21/22 23:08 06/22/22 06:54 630-20-6 1,1,2,2-Tetrachloroethane ND mg/kg 0.0071 0.0019 1 06/21/22 23:08 06/22/22 06:54 79-34-5 Tetrachloroethene ND mg/kg 0.0071 0.0022 1 06/21/22 23:08 06/22/22 06:54 127-18-4 Toluene ND mg/kg 0.0071 0.0020 1 06/21/22 23:08 06/22/22 06:54 108-88-3 1,2,3-Trichlorobenzene ND mg/kg 0.0071 0.0057 1 06/21/22 23:08 06/22/22 06:54 87-61-6 1,2,4-Trichlorobenzene ND mg/kg 0.0071 0.0060 1 06/21/22 23:08 06/22/22 06:54 120-82-1 REPORT OF LABORATORY ANALYSIS IK IK This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: UT-1 Lab ID: 92610717001 Collected: 06/17/22 08:15 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Total Solids 2540 G-2011 Total Solids Wet Chemistry 7199 Chromium, Hexavalent Date: 07/21 /2022 05:22 PM Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte ND mg/kg 0.0071 0.0037 1 06/21 /22 23:08 06/22/22 06:54 71-55-6 ND mg/kg 0.0071 0.0024 1 06/21 /22 23:08 06/22/22 06:54 79-00-5 ND mg/kg 0.0071 0.0018 1 06/21 /22 23:08 06/22/22 06:54 79-01-6 ND mg/kg 0.0071 0.0039 1 06/21 /22 23:08 06/22/22 06:54 75-69-4 ND mg/kg 0.0071 0.0036 1 06/21/22 23:08 06/22/22 06:54 96-18-4 ND mg/kg 0.0071 0.0019 1 06/21 /22 23:08 06/22/22 06:54 95-63-6 ND mg/kg 0.0071 0.0024 1 06/21 /22 23:08 06/22/22 06:54 108-67-8 ND mg/kg 0.071 0.0052 1 06/21 /22 23:08 06/22/22 06:54 108-05-4 ND mg/kg 0.014 0.0036 1 06/21 /22 23:08 06/22/22 06:54 75-01-4 ND mg/kg 0.014 0.0041 1 06/21 /22 23:08 06/22/22 06:54 1330-20-7 ND mg/kg 0.014 0.0049 1 06/21 /22 23:08 06/22/22 06:54 179601-23-1 ND mg/kg 0.0071 0.0031 1 06/21 /22 23:08 06/22/22 06:54 95-47-6 98 % 70-130 1 06/21 /22 23:08 06/22/22 06:54 2037-26-5 95 % 69-134 1 06/21 /22 23:08 06/22/22 06:54 460-00-4 83 % 70-130 1 06/21 /22 23:08 06/22/22 06:54 17060-07-0 Analytical Method: SW-846 Pace Analytical Services - Charlotte 19.4 % 0.10 0.10 1 06/21 /22 16:47 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet 79.6 % 1 06/27/2213:04 06/27/2213:11 Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet ND mg/kg 1.26 0.320 1 07/13/2214:13 07/15/2211:09 18540-29-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 Page 11 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: UT-4 Lab ID: 92610717002 Collected: 06/17/22 15:30 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual OP Pesticides 8141 B Analytical Method: EPA 8141 B Preparation Method: 3546 Pace National - Mt. Juliet Azinphos, methyl (Guthion) ND mg/kg 0.116 0.0370 1 06/23/22 16:09 06/24/22 03:28 86-50-0 Bolstar ND mg/kg 0.116 0.0173 1 06/23/22 16:09 06/24/22 03:28 35400-43-2 Chlorpyrifos ND mg/kg 0.116 0.0183 1 06/23/22 16:09 06/24/22 03:28 2921-88-2 Coumaphos ND mg/kg 0.116 0.0283 1 06/23/22 16:09 06/24/22 03:28 56-72-4 Total Demeton ND mg/kg 0.0814 0.00679 1 06/23/22 16:09 06/24/22 03:28 8065-48-3 Diazinon ND mg/kg 0.116 0.0262 1 06/23/22 16:09 06/24/22 03:28 333-41-5 Dichlorvos ND mg/kg 0.116 0.0349 1 06/23/22 16:09 06/24/22 03:28 62-73-7 Dimethoate ND mg/kg 0.116 0.0388 1 06/23/22 16:09 06/24/22 03:28 60-51-5 Disulfoton ND mg/kg 0.116 0.0295 1 06/23/22 16:09 06/24/22 03:28 298-04-4 EPN (ENT) ND mg/kg 0.116 0.0321 1 06/23/22 16:09 06/24/22 03:28 2104-64-5 Ethoprop ND mg/kg 0.116 0.0137 1 06/23/22 16:09 06/24/22 03:28 13194-48-4 Parathion (Ethyl parathion) ND mg/kg 0.116 0.0191 1 06/23/22 16:09 06/24/22 03:28 56-38-2 Fensulfothion ND mg/kg 0.116 0.0411 1 06/23/22 16:09 06/24/22 03:28 115-90-2 Fenthion ND mg/kg 0.116 0.0155 1 06/23/22 16:09 06/24/22 03:28 55-38-9 Malathion ND mg/kg 0.116 0.0208 1 06/23/22 16:09 06/24/22 03:28 121-75-5 Merphos ND mg/kg 0.116 0.0270 1 06/23/22 16:09 06/24/22 03:28 150-50-5 Methyl parathion ND mg/kg 0.116 0.0236 1 06/23/22 16:09 06/24/22 03:28 298-00-0 Mevinphos ND mg/kg 0.116 0.0267 1 06/23/22 16:09 06/24/22 03:28 7786-34-7 Naled ND mg/kg 0.116 0.0558 1 06/23/22 16:09 06/24/22 03:28 300-76-5 Phorate ND mg/kg 0.116 0.0244 1 06/23/22 16:09 06/24/22 03:28 298-02-2 Ronnel ND mg/kg 0.116 0.0173 1 06/23/22 16:09 06/24/22 03:28 299-84-3 Stirophos (Tetrachlorvinphos) ND mg/kg 0.116 0.0207 1 06/23/22 16:09 06/24/22 03:28 22248-79-9 Sulfotepp (ThiodiphosphoricAc ND mg/kg 0.116 0.0115 1 06/23/22 16:09 06/24/22 03:28 3689-24-5 TEPP ND mg/kg 1.16 0.183 1 06/23/22 16:09 06/24/22 03:28 107-49-3 Tokuthion (Prothiofos) ND mg/kg 0.116 0.0174 1 06/23/22 16:09 06/24/22 03:28 34643-46-4 Trichloronate ND mg/kg 0.116 0.0234 1 06/23/22 16:09 06/24/22 03:28 327-98-0 Surrogates Triphenylphosphate (S) 86.1 % 36.0-121 1 06/23/22 16:09 06/24/22 03:28 115-86-6 Chlorinated Herb. (GC) 8151 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND mg/kg 0.0814 0.00816 1 06/30/22 21:57 07/03/22 04:16 94-75-7 Dalapon ND mg/kg 0.0814 0.0131 1 06/30/22 21:57 07/03/22 04:16 127-20-8 2,4-DB ND mg/kg 0.0814 0.0345 1 06/30/22 21:57 07/03/22 04:16 94-82-6 Dicamba ND mg/kg 0.0814 0.0183 1 06/30/22 21:57 07/03/22 04:16 1918-00-9 Dichloroprop ND mg/kg 0.0814 0.0285 1 06/30/22 21:57 07/03/22 04:16 15165-67-0 Dinoseb ND mg/kg 0.0814 0.00811 1 06/30/22 21:57 07/03/22 04:16 88-85-7 MCPA ND mg/kg 7.56 0.515 1 06/30/22 21:57 07/03/22 04:16 94-74-6 MCPP ND mg/kg 7.56 0.427 1 06/30/22 21:57 07/03/22 04:16 7085-19-0 2,4,5-T ND mg/kg 0.0814 0.00991 1 06/30/22 21:57 07/03/22 04:16 93-76-5 2,4,5-TP (Silvex) ND mg/kg 0.0814 0.0124 1 06/30/22 21:57 07/03/22 04:16 93-72-1 Surrogates 2,4-DCAA (S) 76.0 % 22.0-132 1 06/30/22 21:57 07/03/22 04:16 19719-28-9 REPORT OF LABORATORY ANALYSIS LO LO LO LO LO LO LO This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: UT-4 Lab ID: 92610717002 Collected: 06/17/22 15:30 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 B Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Aldrin ND mg/kg 0.023 0.0093 10 06/22/22 16:23 06/27/22 15:27 309-00-2 alpha-BHC ND mg/kg 0.023 0.010 10 06/22/22 16:23 06/27/22 15:27 319-84-6 beta-BHC ND mg/kg 0.023 0.011 10 06/22/22 16:23 06/27/22 15:27 319-85-7 delta-BHC ND mg/kg 0.023 0.011 10 06/22/22 16:23 06/27/22 15:27 319-86-8 gamma-BHC (Lindane) ND mg/kg 0.023 0.0092 10 06/22/22 16:23 06/27/22 15:27 58-89-9 Chlordane (Technical) ND mg/kg 0.12 0.10 10 06/22/22 16:23 06/27/22 15:27 57-74-9 4,4'-DDD ND mg/kg 0.023 0.010 10 06/22/22 16:23 06/27/22 15:27 72-54-8 4,4'-DDE ND mg/kg 0.023 0.011 10 06/22/22 16:23 06/27/22 15:27 72-55-9 4,4'-DDT ND mg/kg 0.023 0.010 10 06/22/22 16:23 06/27/22 15:27 50-29-3 Dieldrin ND mg/kg 0.023 0.010 10 06/22/22 16:23 06/27/22 15:27 60-57-1 Endosulfan I ND mg/kg 0.023 0.0099 10 06/22/22 16:23 06/27/22 15:27 959-98-8 Endosulfan 11 ND mg/kg 0.023 0.010 10 06/22/22 16:23 06/27/22 15:27 33213-65-9 Endosulfan sulfate ND mg/kg 0.023 0.013 10 06/22/22 16:23 06/27/22 15:27 1031-07-8 Endrin ND mg/kg 0.023 0.011 10 06/22/22 16:23 06/27/22 15:27 72-20-8 Endrin aldehyde ND mg/kg 0.023 0.015 10 06/22/22 16:23 06/27/22 15:27 7421-93-4 Endrin ketone ND mg/kg 0.023 0.013 10 06/22/22 16:23 06/27/22 15:27 53494-70-5 Heptachlor ND mg/kg 0.023 0.011 10 06/22/22 16:23 06/27/22 15:27 76-44-8 Heptachlor epoxide ND mg/kg 0.023 0.0092 10 06/22/22 16:23 06/27/22 15:27 1024-57-3 Hexachlorobenzene ND mg/kg 0.023 0.0095 10 06/22/22 16:23 06/27/22 15:27 118-74-1 Methoxychlor ND mg/kg 0.058 0.028 10 06/22/22 16:23 06/27/22 15:27 72-43-5 Mirex ND mg/kg 0.058 0.026 10 06/22/22 16:23 06/27/22 15:27 2385-85-5 Toxaphene ND mg/kg 0.081 0.062 10 06/22/22 16:23 06/27/22 15:27 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 0 % 10-133 10 06/22/22 16:23 06/27/22 15:27 877-09-8 D3,S4 Decachlorobiphenyl (S) 0 % 10-146 10 06/22/22 16:23 06/27/22 15:27 2051-24-3 S4 EPA 6020B Analytical Method: EPA 6020E Preparation Method: EPA 3050B Pace Analytical Gulf Coast Arsenic 1.37 mg/kg 0.41 0.10 10 06/26/22 09:00 06/29/22 20:13 7440-38-2 Barium 107 mg/kg 0.41 0.10 10 06/26/22 09:00 06/29/22 20:13 7440-39-3 Cadmium ND mg/kg 0.41 0.10 10 06/26/22 09:00 06/29/22 20:13 7440-43-9 Chromium 24.7 mg/kg 0.41 0.10 10 06/26/22 09:00 06/29/22 20:13 7440-47-3 Lead 14.0 mg/kg 0.41 0.10 10 06/26/22 09:00 06/29/22 20:13 7439-92-1 Selenium ND mg/kg 0.41 0.10 10 06/26/22 09:00 06/29/22 20:13 7782-49-2 Silver ND mg/kg 0.41 0.10 10 06/26/22 09:00 06/29/22 20:13 7440-22-4 EPA 7471 B Analytical Method: EPA 7471 B Preparation Method: METHOD Pace Analytical Gulf Coast Mercury 0.047 mg/kg 0.015 0.0061 1 06/24/2211:30 06/27/2212:30 7439-97-6 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND mg/kg 0.38 0.13 1 06/23/2217:52 06/30/2213:46 83-32-9 Acenaphthylene ND mg/kg 0.38 0.13 1 06/23/2217:52 06/30/2213:46 208-96-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: UT-4 Lab ID: 92610717002 Collected: 06/17/22 15:30 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Aniline ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/30/22 13:46 62-53-3 Anthracene ND mg/kg 0.38 0.12 1 06/23/22 17:52 06/30/22 13:46 120-12-7 Benzo(a)anthracene ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/30/22 13:46 56-55-3 Benzo(a)pyrene ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/30/22 13:46 50-32-8 Benzo(b)fluoranthene ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/30/22 13:46 205-99-2 Benzo(g,h,i)perylene ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/30/22 13:46 191-24-2 Benzo(k)fluoranthene ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/30/22 13:46 207-08-9 Benzoic Acid ND mg/kg 1.9 0.81 1 06/23/22 17:52 06/30/22 13:46 65-85-0 Benzyl alcohol ND mg/kg 0.76 0.29 1 06/23/22 17:52 06/30/22 13:46 100-51-6 4-Bromophenylphenyl ether ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/30/22 13:46 101-55-3 Butylbenzylphthalate ND mg/kg 0.38 0.16 1 06/23/22 17:52 06/30/22 13:46 85-68-7 4-Chloro-3-methyl phenol ND mg/kg 0.76 0.27 1 06/23/22 17:52 06/30/22 13:46 59-50-7 4-Chloroaniline ND mg/kg 0.76 0.30 1 06/23/22 17:52 06/30/22 13:46 106-47-8 bis(2-Chloroethoxy)methane ND mg/kg 0.38 0.16 1 06/23/22 17:52 06/30/22 13:46 111-91-1 bis(2-Chloroethyl) ether ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/30/22 13:46 111-44-4 2-Chloronaphthalene ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/30/22 13:46 91-58-7 2-Chlorophenol ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/30/22 13:46 95-57-8 4-Chlorophenylphenyl ether ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/30/22 13:46 7005-72-3 Chrysene ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/30/22 13:46 218-01-9 Dibenz(a,h)anthracene ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/30/22 13:46 53-70-3 Dibenzofuran ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/30/22 13:46 132-64-9 1,2-Dichlorobenzene ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/30/22 13:46 95-50-1 1,3-Dichlorobenzene ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/30/22 13:46 541-73-1 1,4-Dichlorobenzene ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/30/22 13:46 106-46-7 3,3'-Dichlorobenzidine ND mg/kg 0.76 0.26 1 06/23/22 17:52 06/30/22 13:46 91-94-1 2,4-Dichlorophenol ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/30/22 13:46 120-83-2 Diethylphthalate ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/30/22 13:46 84-66-2 2,4-Dimethylphenol ND mg/kg 0.38 0.16 1 06/23/22 17:52 06/30/22 13:46 105-67-9 Dimethylphthalate ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/30/22 13:46 131-11-3 Di-n-butylphthalate ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/30/22 13:46 84-74-2 4,6-Dinitro-2-methyl phenol ND mg/kg 0.76 0.35 1 06/23/22 17:52 06/30/22 13:46 534-52-1 2,4-Dinitrophenol ND mg/kg 1.9 1.2 1 06/23/22 17:52 06/30/22 13:46 51-28-5 2,4-Dinitrotoluene ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/30/22 13:46 121-14-2 2,6-Dinitrotoluene ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/30/22 13:46 606-20-2 Di-n-octylphthalate ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/30/22 13:46 117-84-0 bis(2- Ethyl hexyl)phthalate ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/30/22 13:46 117-81-7 Fluoranthene ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/30/22 13:46 206-44-0 Fluorene ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/30/22 13:46 86-73-7 Hexachloro-1,3-butadiene ND mg/kg 0.38 0.16 1 06/23/22 17:52 06/30/22 13:46 87-68-3 Hexachlorobenzene ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/30/22 13:46 118-74-1 Hexachlorocyclopentadiene ND mg/kg 0.38 0.22 1 06/23/22 17:52 06/30/22 13:46 77-47-4 Hexachloroethane ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/30/22 13:46 67-72-1 Indeno(1,2,3-cd)pyrene ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/30/22 13:46 193-39-5 Isophorone ND mg/kg 0.38 0.17 1 06/23/22 17:52 06/30/22 13:46 78-59-1 REPORT OF LABORATORY ANALYSIS IL L2.v2 This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: UT-4 Lab ID: 92610717002 Collected: 06/17/22 15:30 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 1-Methylnaphthalene ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/30/22 13:46 90-12-0 2-Methylnaphthalene ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/30/22 13:46 91-57-6 2-Methylphenol(o-Cresol) ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/30/22 13:46 95-48-7 3&4-Methyl phenol (m&p Cresol) ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/30/22 13:46 15831-10-4 Naphthalene ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/30/22 13:46 91-20-3 2-Nitroaniline ND mg/kg 1.9 0.31 1 06/23/22 17:52 06/30/22 13:46 88-74-4 3-Nitroaniline ND mg/kg 1.9 0.30 1 06/23/22 17:52 06/30/22 13:46 99-09-2 4-Nitroaniline ND mg/kg 0.76 0.29 1 06/23/22 17:52 06/30/22 13:46 100-01-6 Nitrobenzene ND mg/kg 0.38 0.18 1 06/23/22 17:52 06/30/22 13:46 98-95-3 2-Nitrophenol ND mg/kg 0.38 0.16 1 06/23/22 17:52 06/30/22 13:46 88-75-5 4-Nitrophenol ND mg/kg 1.9 0.73 1 06/23/22 17:52 06/30/22 13:46 100-02-7 N-Nitrosodimethylamine ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/30/22 13:46 62-75-9 N-Nitroso-di-n-propylamine ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/30/22 13:46 621-64-7 N-Nitrosodiphenylamine ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/30/22 13:46 86-30-6 2,2'-Oxybis(1-chloropropane) ND mg/kg 0.38 0.18 1 06/23/22 17:52 06/30/22 13:46 108-60-1 Pentachlorophenol ND mg/kg 0.76 0.37 1 06/23/22 17:52 06/30/22 13:46 87-86-5 Phenanthrene ND mg/kg 0.38 0.12 1 06/23/22 17:52 06/30/22 13:46 85-01-8 Phenol ND mg/kg 0.38 0.17 1 06/23/22 17:52 06/30/22 13:46 108-95-2 Pyrene ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/30/22 13:46 129-00-0 Pyridine ND mg/kg 0.38 0.12 1 06/23/22 17:52 06/30/22 13:46 110-86-1 1,2,4-Trichlorobenzene ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/30/22 13:46 120-82-1 2,4,5-Trichlorophenol ND mg/kg 0.38 0.17 1 06/23/22 17:52 06/30/22 13:46 95-95-4 2,4,6-Trichlorophenol ND mg/kg 0.38 0.16 1 06/23/22 17:52 06/30/22 13:46 88-06-2 Surrogates Nitrobenzene-d5 (S) 77 % 21-130 1 06/23/22 17:52 06/30/22 13:46 4165-60-0 2-Fluorobiphenyl (S) 71 % 19-130 1 06/23/22 17:52 06/30/22 13:46 321-60-8 Terphenyl-d14 (S) 72 % 15-130 1 06/23/22 17:52 06/30/22 13:46 1718-51-0 Phenol-d6 (S) 66 % 18-130 1 06/23/22 17:52 06/30/22 13:46 13127-88-3 2-Fluorophenol (S) 56 % 18-130 1 06/23/22 17:52 06/30/22 13:46 367-12-4 2,4,6-Tribromophenol (S) 71 % 18-130 1 06/23/22 17:52 06/30/22 13:46 118-79-6 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Acetone ND mg/kg 0.12 0.040 1 06/21/22 23:08 06/22/22 07:13 67-64-1 Benzene ND mg/kg 0.0062 0.0025 1 06/21/22 23:08 06/22/22 07:13 71-43-2 Bromobenzene ND mg/kg 0.0062 0.0020 1 06/21/22 23:08 06/22/22 07:13 108-86-1 Bromochloromethane ND mg/kg 0.0062 0.0018 1 06/21/22 23:08 06/22/22 07:13 74-97-5 Bromodichloromethane ND mg/kg 0.0062 0.0024 1 06/21/22 23:08 06/22/22 07:13 75-27-4 Bromoform ND mg/kg 0.0062 0.0022 1 06/21/22 23:08 06/22/22 07:13 75-25-2 Bromomethane ND mg/kg 0.012 0.0098 1 06/21/22 23:08 06/22/22 07:13 74-83-9 2-Butanone (MEK) 0.040J mg/kg 0.12 0.030 1 06/21/22 23:08 06/22/22 07:13 78-93-3 n-Butylbenzene ND mg/kg 0.0062 0.0029 1 06/21/22 23:08 06/22/22 07:13 104-51-8 sec-Butylbenzene ND mg/kg 0.0062 0.0027 1 06/21/22 23:08 06/22/22 07:13 135-98-8 tert-Butyl benzene ND mg/kg 0.0062 0.0022 1 06/21/22 23:08 06/22/22 07:13 98-06-6 REPORT OF LABORATORY ANALYSIS v2 v2 IK v2 This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: UT-4 Lab ID: 92610717002 Collected: 06/17/22 15:30 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Carbon tetrachloride ND mg/kg 0.0062 0.0023 1 06/21/22 23:08 06/22/22 07:13 56-23-5 Chlorobenzene ND mg/kg 0.0062 0.0012 1 06/21/22 23:08 06/22/22 07:13 108-90-7 Chloroethane ND mg/kg 0.012 0.0048 1 06/21/22 23:08 06/22/22 07:13 75-00-3 Chloroform ND mg/kg 0.0062 0.0038 1 06/21/22 23:08 06/22/22 07:13 67-66-3 Chloromethane ND mg/kg 0.012 0.0052 1 06/21/22 23:08 06/22/22 07:13 74-87-3 2-Chlorotoluene ND mg/kg 0.0062 0.0022 1 06/21/22 23:08 06/22/22 07:13 95-49-8 4-Chlorotoluene ND mg/kg 0.0062 0.0011 1 06/21/22 23:08 06/22/22 07:13 106-43-4 1,2-Dibromo-3-chloropropane ND mg/kg 0.0062 0.0024 1 06/21/22 23:08 06/22/22 07:13 96-12-8 Dibromochloromethane ND mg/kg 0.0062 0.0035 1 06/21/22 23:08 06/22/22 07:13 124-48-1 1,2-Dibromoethane (EDB) ND mg/kg 0.0062 0.0027 1 06/21/22 23:08 06/22/22 07:13 106-93-4 Dibromomethane ND mg/kg 0.0062 0.0013 1 06/21/22 23:08 06/22/22 07:13 74-95-3 1,2-Dichlorobenzene ND mg/kg 0.0062 0.0022 1 06/21/22 23:08 06/22/22 07:13 95-50-1 1,3-Dichlorobenzene ND mg/kg 0.0062 0.0019 1 06/21/22 23:08 06/22/22 07:13 541-73-1 1,4-Dichlorobenzene ND mg/kg 0.0062 0.0016 1 06/21/22 23:08 06/22/22 07:13 106-46-7 Dichlorodifluoromethane ND mg/kg 0.012 0.0027 1 06/21/22 23:08 06/22/22 07:13 75-71-8 1,1-Dichloroethane ND mg/kg 0.0062 0.0026 1 06/21/22 23:08 06/22/22 07:13 75-34-3 1,2-Dichloroethane ND mg/kg 0.0062 0.0041 1 06/21/22 23:08 06/22/22 07:13 107-06-2 1,1-Dichloroethene ND mg/kg 0.0062 0.0026 1 06/21/22 23:08 06/22/22 07:13 75-35-4 cis-1,2-Dichloroethene ND mg/kg 0.0062 0.0021 1 06/21/22 23:08 06/22/22 07:13 156-59-2 trans-1,2-Dichloroethene ND mg/kg 0.0062 0.0022 1 06/21/22 23:08 06/22/22 07:13 156-60-5 1,2-Dichloropropane ND mg/kg 0.0062 0.0019 1 06/21/22 23:08 06/22/22 07:13 78-87-5 1,3-Dichloropropane ND mg/kg 0.0062 0.0019 1 06/21/22 23:08 06/22/22 07:13 142-28-9 2,2-Dichloropropane ND mg/kg 0.0062 0.0020 1 06/21/22 23:08 06/22/22 07:13 594-20-7 1,1-Dichloropropene ND mg/kg 0.0062 0.0030 1 06/21/22 23:08 06/22/22 07:13 563-58-6 cis-1,3-Dichloropropene ND mg/kg 0.0062 0.0017 1 06/21/22 23:08 06/22/22 07:13 10061-01-5 trans- 1,3-Dichloropropene ND mg/kg 0.0062 0.0021 1 06/21/22 23:08 06/22/22 07:13 10061-02-6 Diisopropyl ether ND mg/kg 0.0062 0.0017 1 06/21/22 23:08 06/22/22 07:13 108-20-3 Ethylbenzene ND mg/kg 0.0062 0.0029 1 06/21/22 23:08 06/22/22 07:13 100-41-4 Hexachloro-1,3-butadiene ND mg/kg 0.012 0.010 1 06/21/22 23:08 06/22/22 07:13 87-68-3 2-Hexanone ND mg/kg 0.062 0.0060 1 06/21/22 23:08 06/22/22 07:13 591-78-6 Isopropylbenzene (Cumene) ND mg/kg 0.0062 0.0021 1 06/21/22 23:08 06/22/22 07:13 98-82-8 p-Isopropyltoluene ND mg/kg 0.0062 0.0031 1 06/21/22 23:08 06/22/22 07:13 99-87-6 Methylene Chloride ND mg/kg 0.025 0.017 1 06/21/22 23:08 06/22/22 07:13 75-09-2 4-Methyl-2-pentanone (MIBK) ND mg/kg 0.062 0.0060 1 06/21/22 23:08 06/22/22 07:13 108-10-1 Methyl-tert-butyl ether ND mg/kg 0.0062 0.0023 1 06/21/22 23:08 06/22/22 07:13 1634-04-4 Naphthalene ND mg/kg 0.0062 0.0033 1 06/21/22 23:08 06/22/22 07:13 91-20-3 n-Propylbenzene ND mg/kg 0.0062 0.0022 1 06/21/22 23:08 06/22/22 07:13 103-65-1 Styrene ND mg/kg 0.0062 0.0016 1 06/21/22 23:08 06/22/22 07:13 100-42-5 1,1,1,2-Tetrachloroethane ND mg/kg 0.0062 0.0024 1 06/21/22 23:08 06/22/22 07:13 630-20-6 1,1,2,2-Tetrachloroethane ND mg/kg 0.0062 0.0016 1 06/21/22 23:08 06/22/22 07:13 79-34-5 Tetrachloroethene ND mg/kg 0.0062 0.0020 1 06/21/22 23:08 06/22/22 07:13 127-18-4 Toluene ND mg/kg 0.0062 0.0018 1 06/21/22 23:08 06/22/22 07:13 108-88-3 1,2,3-Trichlorobenzene ND mg/kg 0.0062 0.0050 1 06/21/22 23:08 06/22/22 07:13 87-61-6 1,2,4-Trichlorobenzene ND mg/kg 0.0062 0.0052 1 06/21/22 23:08 06/22/22 07:13 120-82-1 REPORT OF LABORATORY ANALYSIS IK IK This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: UT-4 Lab ID: 92610717002 Collected: 06/17/22 15:30 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Total Solids 2540 G-2011 Total Solids Wet Chemistry 7199 Chromium, Hexavalent Date: 07/21 /2022 05:22 PM Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte ND mg/kg 0.0062 0.0032 1 06/21 /22 23:08 06/22/22 07:13 71-55-6 ND mg/kg 0.0062 0.0021 1 06/21 /22 23:08 06/22/22 07:13 79-00-5 ND mg/kg 0.0062 0.0016 1 06/21 /22 23:08 06/22/22 07:13 79-01-6 ND mg/kg 0.0062 0.0034 1 06/21 /22 23:08 06/22/22 07:13 75-69-4 ND mg/kg 0.0062 0.0031 1 06/21/22 23:08 06/22/22 07:13 96-18-4 ND mg/kg 0.0062 0.0017 1 06/21 /22 23:08 06/22/22 07:13 95-63-6 ND mg/kg 0.0062 0.0021 1 06/21 /22 23:08 06/22/22 07:13 108-67-8 ND mg/kg 0.062 0.0045 1 06/21 /22 23:08 06/22/22 07:13 108-05-4 ND mg/kg 0.012 0.0032 1 06/21 /22 23:08 06/22/22 07:13 75-01-4 ND mg/kg 0.012 0.0035 1 06/21 /22 23:08 06/22/22 07:13 1330-20-7 ND mg/kg 0.012 0.0043 1 06/21 /22 23:08 06/22/22 07:13 179601-23-1 ND mg/kg 0.0062 0.0028 1 06/21 /22 23:08 06/22/22 07:13 95-47-6 99 % 70-130 1 06/21 /22 23:08 06/22/22 07:13 2037-26-5 97 % 69-134 1 06/21 /22 23:08 06/22/22 07:13 460-00-4 88 % 70-130 1 06/21 /22 23:08 06/22/22 07:13 17060-07-0 Analytical Method: SW-846 Pace Analytical Services - Charlotte 14.2 % 0.10 0.10 1 06/21 /22 16:47 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet 86.0 % 1 06/27/2213:04 06/27/2213:11 Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet ND mg/kg 1.16 0.297 1 07/13/2214:13 07/15/2211:14 18540-29-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 Page 17 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: DUP-2 Lab ID: 92610717003 Collected: 06/17/22 00:00 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual OP Pesticides 8141 B Analytical Method: EPA 8141 B Preparation Method: 3546 Pace National - Mt. Juliet Azinphos, methyl (Guthion) ND mg/kg 0.110 0.0351 1 06/23/22 16:09 06/24/22 04:02 86-50-0 Bolstar ND mg/kg 0.110 0.0164 1 06/23/22 16:09 06/24/22 04:02 35400-43-2 Chlorpyrifos ND mg/kg 0.110 0.0173 1 06/23/22 16:09 06/24/22 04:02 2921-88-2 Coumaphos ND mg/kg 0.110 0.0268 1 06/23/22 16:09 06/24/22 04:02 56-72-4 Total Demeton ND mg/kg 0.0773 0.00645 1 06/23/22 16:09 06/24/22 04:02 8065-48-3 Diazinon ND mg/kg 0.110 0.0248 1 06/23/22 16:09 06/24/22 04:02 333-41-5 Dichlorvos ND mg/kg 0.110 0.0331 1 06/23/22 16:09 06/24/22 04:02 62-73-7 Dimethoate ND mg/kg 0.110 0.0369 1 06/23/22 16:09 06/24/22 04:02 60-51-5 Disulfoton ND mg/kg 0.110 0.0280 1 06/23/22 16:09 06/24/22 04:02 298-04-4 EPN (ENT) ND mg/kg 0.110 0.0305 1 06/23/22 16:09 06/24/22 04:02 2104-64-5 Ethoprop ND mg/kg 0.110 0.0130 1 06/23/22 16:09 06/24/22 04:02 13194-48-4 Parathion (Ethyl parathion) ND mg/kg 0.110 0.0181 1 06/23/22 16:09 06/24/22 04:02 56-38-2 Fensulfothion ND mg/kg 0.110 0.0390 1 06/23/22 16:09 06/24/22 04:02 115-90-2 Fenthion ND mg/kg 0.110 0.0147 1 06/23/22 16:09 06/24/22 04:02 55-38-9 Malathion ND mg/kg 0.110 0.0198 1 06/23/22 16:09 06/24/22 04:02 121-75-5 Merphos ND mg/kg 0.110 0.0256 1 06/23/22 16:09 06/24/22 04:02 150-50-5 Methyl parathion ND mg/kg 0.110 0.0224 1 06/23/22 16:09 06/24/22 04:02 298-00-0 Mevinphos ND mg/kg 0.110 0.0254 1 06/23/22 16:09 06/24/22 04:02 7786-34-7 Naled ND mg/kg 0.110 0.0530 1 06/23/22 16:09 06/24/22 04:02 300-76-5 Phorate ND mg/kg 0.110 0.0232 1 06/23/22 16:09 06/24/22 04:02 298-02-2 Ronnel ND mg/kg 0.110 0.0164 1 06/23/22 16:09 06/24/22 04:02 299-84-3 Stirophos (Tetrachlorvinphos) ND mg/kg 0.110 0.0196 1 06/23/22 16:09 06/24/22 04:02 22248-79-9 Sulfotepp (ThiodiphosphoricAc ND mg/kg 0.110 0.0109 1 06/23/22 16:09 06/24/22 04:02 3689-24-5 TEPP ND mg/kg 1.10 0.173 1 06/23/22 16:09 06/24/22 04:02 107-49-3 Tokuthion (Prothiofos) ND mg/kg 0.110 0.0166 1 06/23/22 16:09 06/24/22 04:02 34643-46-4 Trichloronate ND mg/kg 0.110 0.0222 1 06/23/22 16:09 06/24/22 04:02 327-98-0 Surrogates Triphenylphosphate (S) 79.7 % 36.0-121 1 06/23/22 16:09 06/24/22 04:02 115-86-6 Chlorinated Herb. (GC) 8151 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND mg/kg 0.0773 0.00775 1 06/30/22 21:57 07/03/22 04:31 94-75-7 Dalapon ND mg/kg 0.0773 0.0125 1 06/30/22 21:57 07/03/22 04:31 127-20-8 2,4-DB ND mg/kg 0.0773 0.0328 1 06/30/22 21:57 07/03/22 04:31 94-82-6 Dicamba ND mg/kg 0.0773 0.0173 1 06/30/22 21:57 07/03/22 04:31 1918-00-9 Dichloroprop ND mg/kg 0.0773 0.0270 1 06/30/22 21:57 07/03/22 04:31 15165-67-0 Dinoseb ND mg/kg 0.0773 0.00769 1 06/30/22 21:57 07/03/22 04:31 88-85-7 MCPA ND mg/kg 7.17 0.489 1 06/30/22 21:57 07/03/22 04:31 94-74-6 MCPP ND mg/kg 7.17 0.405 1 06/30/22 21:57 07/03/22 04:31 7085-19-0 2,4,5-T ND mg/kg 0.0773 0.00940 1 06/30/22 21:57 07/03/22 04:31 93-76-5 2,4,5-TP (Silvex) ND mg/kg 0.0773 0.0118 1 06/30/22 21:57 07/03/22 04:31 93-72-1 Surrogates 2,4-DCAA (S) 76.0 % 22.0-132 1 06/30/22 21:57 07/03/22 04:31 19719-28-9 REPORT OF LABORATORY ANALYSIS LO LO LO LO LO LO LO This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: DUP-2 Lab ID: 92610717003 Collected: 06/17/22 00:00 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 B Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Aldrin ND mg/kg 0.011 0.0046 5 06/22/22 16:23 06/27/22 15:38 309-00-2 alpha-BHC ND mg/kg 0.011 0.0049 5 06/22/22 16:23 06/27/22 15:38 319-84-6 beta-BHC ND mg/kg 0.011 0.0055 5 06/22/22 16:23 06/27/22 15:38 319-85-7 delta-BHC ND mg/kg 0.011 0.0056 5 06/22/22 16:23 06/27/22 15:38 319-86-8 gamma-BHC (Lindane) ND mg/kg 0.011 0.0045 5 06/22/22 16:23 06/27/22 15:38 58-89-9 Chlordane (Technical) ND mg/kg 0.057 0.049 5 06/22/22 16:23 06/27/22 15:38 57-74-9 4,4'-DDD ND mg/kg 0.011 0.0051 5 06/22/22 16:23 06/27/22 15:38 72-54-8 4,4'-DDE ND mg/kg 0.011 0.0053 5 06/22/22 16:23 06/27/22 15:38 72-55-9 4,4'-DDT ND mg/kg 0.011 0.0050 5 06/22/22 16:23 06/27/22 15:38 50-29-3 Dieldrin ND mg/kg 0.011 0.0049 5 06/22/22 16:23 06/27/22 15:38 60-57-1 Endosulfan I ND mg/kg 0.011 0.0049 5 06/22/22 16:23 06/27/22 15:38 959-98-8 Endosulfan 11 ND mg/kg 0.011 0.0051 5 06/22/22 16:23 06/27/22 15:38 33213-65-9 Endosulfan sulfate ND mg/kg 0.011 0.0063 5 06/22/22 16:23 06/27/22 15:38 1031-07-8 Endrin ND mg/kg 0.011 0.0053 5 06/22/22 16:23 06/27/22 15:38 72-20-8 Endrin aldehyde ND mg/kg 0.011 0.0076 5 06/22/22 16:23 06/27/22 15:38 7421-93-4 Endrin ketone ND mg/kg 0.011 0.0062 5 06/22/22 16:23 06/27/22 15:38 53494-70-5 Heptachlor ND mg/kg 0.011 0.0052 5 06/22/22 16:23 06/27/22 15:38 76-44-8 Heptachlor epoxide ND mg/kg 0.011 0.0045 5 06/22/22 16:23 06/27/22 15:38 1024-57-3 Hexachlorobenzene ND mg/kg 0.011 0.0047 5 06/22/22 16:23 06/27/22 15:38 118-74-1 Methoxychlor ND mg/kg 0.028 0.014 5 06/22/22 16:23 06/27/22 15:38 72-43-5 Mirex ND mg/kg 0.028 0.013 5 06/22/22 16:23 06/27/22 15:38 2385-85-5 Toxaphene ND mg/kg 0.040 0.030 5 06/22/22 16:23 06/27/22 15:38 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 64 % 10-133 5 06/22/22 16:23 06/27/22 15:38 877-09-8 D3 Decachlorobiphenyl (S) 70 % 10-146 5 06/22/22 16:23 06/27/22 15:38 2051-24-3 EPA 6020B Analytical Method: EPA 6020E Preparation Method: EPA 3050B Pace Analytical Gulf Coast Arsenic 1.84 mg/kg 0.40 0.10 10 06/26/22 09:00 06/29/22 20:17 7440-38-2 Barium 123 mg/kg 0.40 0.10 10 06/26/22 09:00 06/29/22 20:17 7440-39-3 Cadmium ND mg/kg 0.40 0.10 10 06/26/22 09:00 06/29/22 20:17 7440-43-9 Chromium 28.3 mg/kg 0.40 0.10 10 06/26/22 09:00 06/29/22 20:17 7440-47-3 Lead 14.6 mg/kg 0.40 0.10 10 06/26/22 09:00 06/29/22 20:17 7439-92-1 Selenium ND mg/kg 0.40 0.10 10 06/26/22 09:00 06/29/22 20:17 7782-49-2 Silver ND mg/kg 0.40 0.10 10 06/26/22 09:00 06/29/22 20:17 7440-22-4 EPA 7471 B Analytical Method: EPA 7471 B Preparation Method: METHOD Pace Analytical Gulf Coast Mercury 0.019 mg/kg 0.013 0.0052 1 06/24/2211:30 06/27/2212:32 7439-97-6 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND mg/kg 0.38 0.13 1 06/24/2210:36 06/30/2212:50 83-32-9 Acenaphthylene ND mg/kg 0.38 0.13 1 06/24/2210:36 06/30/2212:50 208-96-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: DUP-2 Lab ID: 92610717003 Collected: 06/17/22 00:00 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Aniline ND mg/kg 0.38 0.15 1 06/24/22 10:36 06/30/22 12:50 62-53-3 Anthracene ND mg/kg 0.38 0.13 1 06/24/22 10:36 06/30/22 12:50 120-12-7 Benzo(a)anthracene ND mg/kg 0.38 0.13 1 06/24/22 10:36 06/30/22 12:50 56-55-3 Benzo(a)pyrene ND mg/kg 0.38 0.13 1 06/24/22 10:36 06/30/22 12:50 50-32-8 Benzo(b)fluoranthene ND mg/kg 0.38 0.13 1 06/24/22 10:36 06/30/22 12:50 205-99-2 Benzo(g,h,i)perylene ND mg/kg 0.38 0.15 1 06/24/22 10:36 06/30/22 12:50 191-24-2 Benzo(k)fluoranthene ND mg/kg 0.38 0.13 1 06/24/22 10:36 06/30/22 12:50 207-08-9 Benzoic Acid ND mg/kg 1.9 0.82 1 06/24/22 10:36 06/30/22 12:50 65-85-0 Benzyl alcohol ND mg/kg 0.77 0.29 1 06/24/22 10:36 06/30/22 12:50 100-51-6 4-Bromophenylphenyl ether ND mg/kg 0.38 0.15 1 06/24/22 10:36 06/30/22 12:50 101-55-3 Butylbenzylphthalate ND mg/kg 0.38 0.16 1 06/24/22 10:36 06/30/22 12:50 85-68-7 4-Chloro-3-methyl phenol ND mg/kg 0.77 0.27 1 06/24/22 10:36 06/30/22 12:50 59-50-7 4-Chloroaniline ND mg/kg 0.77 0.30 1 06/24/22 10:36 06/30/22 12:50 106-47-8 bis(2-Chloroethoxy)methane ND mg/kg 0.38 0.16 1 06/24/22 10:36 06/30/22 12:50 111-91-1 bis(2-Chloroethyl) ether ND mg/kg 0.38 0.14 1 06/24/22 10:36 06/30/22 12:50 111-44-4 2-Chloronaphthalene ND mg/kg 0.38 0.15 1 06/24/22 10:36 06/30/22 12:50 91-58-7 2-Chlorophenol ND mg/kg 0.38 0.14 1 06/24/22 10:36 06/30/22 12:50 95-57-8 4-Chlorophenylphenyl ether ND mg/kg 0.38 0.14 1 06/24/22 10:36 06/30/22 12:50 7005-72-3 Chrysene ND mg/kg 0.38 0.14 1 06/24/22 10:36 06/30/22 12:50 218-01-9 Dibenz(a,h)anthracene ND mg/kg 0.38 0.15 1 06/24/22 10:36 06/30/22 12:50 53-70-3 Dibenzofuran ND mg/kg 0.38 0.14 1 06/24/22 10:36 06/30/22 12:50 132-64-9 1,2-Dichlorobenzene ND mg/kg 0.38 0.14 1 06/24/22 10:36 06/30/22 12:50 95-50-1 1,3-Dichlorobenzene ND mg/kg 0.38 0.14 1 06/24/22 10:36 06/30/22 12:50 541-73-1 1,4-Dichlorobenzene ND mg/kg 0.38 0.15 1 06/24/22 10:36 06/30/22 12:50 106-46-7 3,3'-Dichlorobenzidine ND mg/kg 0.77 0.26 1 06/24/22 10:36 06/30/22 12:50 91-94-1 2,4-Dichlorophenol ND mg/kg 0.38 0.15 1 06/24/22 10:36 06/30/22 12:50 120-83-2 Diethylphthalate ND mg/kg 0.38 0.14 1 06/24/22 10:36 06/30/22 12:50 84-66-2 2,4-Dimethylphenol ND mg/kg 0.38 0.16 1 06/24/22 10:36 06/30/22 12:50 105-67-9 Dimethylphthalate ND mg/kg 0.38 0.14 1 06/24/22 10:36 06/30/22 12:50 131-11-3 Di-n-butylphthalate ND mg/kg 0.38 0.13 1 06/24/22 10:36 06/30/22 12:50 84-74-2 4,6-Dinitro-2-methyl phenol ND mg/kg 0.77 0.36 1 06/24/22 10:36 06/30/22 12:50 534-52-1 2,4-Dinitrophenol ND mg/kg 1.9 1.2 1 06/24/22 10:36 06/30/22 12:50 51-28-5 2,4-Dinitrotoluene ND mg/kg 0.38 0.15 1 06/24/22 10:36 06/30/22 12:50 121-14-2 2,6-Dinitrotoluene ND mg/kg 0.38 0.14 1 06/24/22 10:36 06/30/22 12:50 606-20-2 Di-n-octylphthalate ND mg/kg 0.38 0.15 1 06/24/22 10:36 06/30/22 12:50 117-84-0 bis(2- Ethyl hexyl)phthalate ND mg/kg 0.38 0.15 1 06/24/22 10:36 06/30/22 12:50 117-81-7 Fluoranthene ND mg/kg 0.38 0.13 1 06/24/22 10:36 06/30/22 12:50 206-44-0 Fluorene ND mg/kg 0.38 0.13 1 06/24/22 10:36 06/30/22 12:50 86-73-7 Hexachloro-1,3-butadiene ND mg/kg 0.38 0.17 1 06/24/22 10:36 06/30/22 12:50 87-68-3 Hexachlorobenzene ND mg/kg 0.38 0.15 1 06/24/22 10:36 06/30/22 12:50 118-74-1 Hexachlorocyclopentadiene ND mg/kg 0.38 0.22 1 06/24/22 10:36 06/30/22 12:50 77-47-4 Hexachloroethane ND mg/kg 0.38 0.15 1 06/24/22 10:36 06/30/22 12:50 67-72-1 Indeno(1,2,3-cd)pyrene ND mg/kg 0.38 0.15 1 06/24/22 10:36 06/30/22 12:50 193-39-5 Isophorone ND mg/kg 0.38 0.17 1 06/24/22 10:36 06/30/22 12:50 78-59-1 REPORT OF LABORATORY ANALYSIS IL L2.v2 This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: DUP-2 Lab ID: 92610717003 Collected: 06/17/22 00:00 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 1-Methylnaphthalene ND mg/kg 0.38 0.13 1 06/24/22 10:36 06/30/22 12:50 90-12-0 2-Methylnaphthalene ND mg/kg 0.38 0.15 1 06/24/22 10:36 06/30/22 12:50 91-57-6 2-Methylphenol(o-Cresol) ND mg/kg 0.38 0.16 1 06/24/22 10:36 06/30/22 12:50 95-48-7 3&4-Methyl phenol (m&p Cresol) ND mg/kg 0.38 0.15 1 06/24/22 10:36 06/30/22 12:50 15831-10-4 Naphthalene ND mg/kg 0.38 0.13 1 06/24/22 10:36 06/30/22 12:50 91-20-3 2-Nitroaniline ND mg/kg 1.9 0.31 1 06/24/22 10:36 06/30/22 12:50 88-74-4 3-Nitroaniline ND mg/kg 1.9 0.30 1 06/24/22 10:36 06/30/22 12:50 99-09-2 4-Nitroaniline ND mg/kg 0.77 0.29 1 06/24/22 10:36 06/30/22 12:50 100-01-6 Nitrobenzene ND mg/kg 0.38 0.18 1 06/24/22 10:36 06/30/22 12:50 98-95-3 2-Nitrophenol ND mg/kg 0.38 0.17 1 06/24/22 10:36 06/30/22 12:50 88-75-5 4-Nitrophenol ND mg/kg 1.9 0.74 1 06/24/22 10:36 06/30/22 12:50 100-02-7 N-Nitrosodimethylamine ND mg/kg 0.38 0.13 1 06/24/22 10:36 06/30/22 12:50 62-75-9 N-Nitroso-di-n-propylamine ND mg/kg 0.38 0.14 1 06/24/22 10:36 06/30/22 12:50 621-64-7 N-Nitrosodiphenylamine ND mg/kg 0.38 0.14 1 06/24/22 10:36 06/30/22 12:50 86-30-6 2,2'-Oxybis(1-chloropropane) ND mg/kg 0.38 0.18 1 06/24/22 10:36 06/30/22 12:50 108-60-1 Pentachlorophenol ND mg/kg 0.77 0.38 1 06/24/22 10:36 06/30/22 12:50 87-86-5 Phenanthrene ND mg/kg 0.38 0.13 1 06/24/22 10:36 06/30/22 12:50 85-01-8 Phenol ND mg/kg 0.38 0.17 1 06/24/22 10:36 06/30/22 12:50 108-95-2 Pyrene ND mg/kg 0.38 0.16 1 06/24/22 10:36 06/30/22 12:50 129-00-0 Pyridine ND mg/kg 0.38 0.12 1 06/24/22 10:36 06/30/22 12:50 110-86-1 1,2,4-Trichlorobenzene ND mg/kg 0.38 0.15 1 06/24/22 10:36 06/30/22 12:50 120-82-1 2,4,5-Trichlorophenol ND mg/kg 0.38 0.18 1 06/24/22 10:36 06/30/22 12:50 95-95-4 2,4,6-Trichlorophenol ND mg/kg 0.38 0.16 1 06/24/22 10:36 06/30/22 12:50 88-06-2 Surrogates Nitrobenzene-d5 (S) 76 % 21-130 1 06/24/22 10:36 06/30/22 12:50 4165-60-0 2-Fluorobiphenyl (S) 69 % 19-130 1 06/24/22 10:36 06/30/22 12:50 321-60-8 Terphenyl-d14 (S) 77 % 15-130 1 06/24/22 10:36 06/30/22 12:50 1718-51-0 Phenol-d6 (S) 63 % 18-130 1 06/24/22 10:36 06/30/22 12:50 13127-88-3 2-Fluorophenol (S) 55 % 18-130 1 06/24/22 10:36 06/30/22 12:50 367-12-4 2,4,6-Tribromophenol (S) 69 % 18-130 1 06/24/22 10:36 06/30/22 12:50 118-79-6 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Acetone ND mg/kg 0.12 0.037 1 06/21/22 23:08 06/22/22 07:31 67-64-1 Benzene ND mg/kg 0.0058 0.0023 1 06/21/22 23:08 06/22/22 07:31 71-43-2 Bromobenzene ND mg/kg 0.0058 0.0019 1 06/21/22 23:08 06/22/22 07:31 108-86-1 Bromochloromethane ND mg/kg 0.0058 0.0017 1 06/21/22 23:08 06/22/22 07:31 74-97-5 Bromodichloromethane ND mg/kg 0.0058 0.0022 1 06/21/22 23:08 06/22/22 07:31 75-27-4 Bromoform ND mg/kg 0.0058 0.0020 1 06/21/22 23:08 06/22/22 07:31 75-25-2 Bromomethane ND mg/kg 0.012 0.0091 1 06/21/22 23:08 06/22/22 07:31 74-83-9 2-Butanone (MEK) 0.041J mg/kg 0.12 0.028 1 06/21/22 23:08 06/22/22 07:31 78-93-3 n-Butylbenzene ND mg/kg 0.0058 0.0027 1 06/21/22 23:08 06/22/22 07:31 104-51-8 sec-Butylbenzene ND mg/kg 0.0058 0.0025 1 06/21/22 23:08 06/22/22 07:31 135-98-8 tert-Butyl benzene ND mg/kg 0.0058 0.0021 1 06/21/22 23:08 06/22/22 07:31 98-06-6 REPORT OF LABORATORY ANALYSIS v2 v2 IK v2 This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: DUP-2 Lab ID: 92610717003 Collected: 06/17/22 00:00 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Carbon tetrachloride ND mg/kg 0.0058 0.0022 1 06/21/22 23:08 06/22/22 07:31 56-23-5 Chlorobenzene ND mg/kg 0.0058 0.0011 1 06/21/22 23:08 06/22/22 07:31 108-90-7 Chloroethane ND mg/kg 0.012 0.0045 1 06/21/22 23:08 06/22/22 07:31 75-00-3 Chloroform ND mg/kg 0.0058 0.0035 1 06/21/22 23:08 06/22/22 07:31 67-66-3 Chloromethane ND mg/kg 0.012 0.0048 1 06/21/22 23:08 06/22/22 07:31 74-87-3 2-Chlorotoluene ND mg/kg 0.0058 0.0020 1 06/21/22 23:08 06/22/22 07:31 95-49-8 4-Chlorotoluene ND mg/kg 0.0058 0.0010 1 06/21/22 23:08 06/22/22 07:31 106-43-4 1,2-Dibromo-3-chloropropane ND mg/kg 0.0058 0.0022 1 06/21/22 23:08 06/22/22 07:31 96-12-8 Dibromochloromethane ND mg/kg 0.0058 0.0032 1 06/21/22 23:08 06/22/22 07:31 124-48-1 1,2-Dibromoethane (EDB) ND mg/kg 0.0058 0.0025 1 06/21/22 23:08 06/22/22 07:31 106-93-4 Dibromomethane ND mg/kg 0.0058 0.0012 1 06/21/22 23:08 06/22/22 07:31 74-95-3 1,2-Dichlorobenzene ND mg/kg 0.0058 0.0021 1 06/21/22 23:08 06/22/22 07:31 95-50-1 1,3-Dichlorobenzene ND mg/kg 0.0058 0.0018 1 06/21/22 23:08 06/22/22 07:31 541-73-1 1,4-Dichlorobenzene ND mg/kg 0.0058 0.0015 1 06/21/22 23:08 06/22/22 07:31 106-46-7 Dichlorodifluoromethane ND mg/kg 0.012 0.0025 1 06/21/22 23:08 06/22/22 07:31 75-71-8 1,1-Dichloroethane ND mg/kg 0.0058 0.0024 1 06/21/22 23:08 06/22/22 07:31 75-34-3 1,2-Dichloroethane ND mg/kg 0.0058 0.0038 1 06/21/22 23:08 06/22/22 07:31 107-06-2 1,1-Dichloroethene ND mg/kg 0.0058 0.0024 1 06/21/22 23:08 06/22/22 07:31 75-35-4 cis-1,2-Dichloroethene ND mg/kg 0.0058 0.0020 1 06/21/22 23:08 06/22/22 07:31 156-59-2 trans-1,2-Dichloroethene ND mg/kg 0.0058 0.0020 1 06/21/22 23:08 06/22/22 07:31 156-60-5 1,2-Dichloropropane ND mg/kg 0.0058 0.0017 1 06/21/22 23:08 06/22/22 07:31 78-87-5 1,3-Dichloropropane ND mg/kg 0.0058 0.0018 1 06/21/22 23:08 06/22/22 07:31 142-28-9 2,2-Dichloropropane ND mg/kg 0.0058 0.0019 1 06/21/22 23:08 06/22/22 07:31 594-20-7 1,1-Dichloropropene ND mg/kg 0.0058 0.0028 1 06/21/22 23:08 06/22/22 07:31 563-58-6 cis-1,3-Dichloropropene ND mg/kg 0.0058 0.0016 1 06/21/22 23:08 06/22/22 07:31 10061-01-5 trans- 1,3-Dichloropropene ND mg/kg 0.0058 0.0020 1 06/21/22 23:08 06/22/22 07:31 10061-02-6 Diisopropyl ether ND mg/kg 0.0058 0.0016 1 06/21/22 23:08 06/22/22 07:31 108-20-3 Ethylbenzene ND mg/kg 0.0058 0.0027 1 06/21/22 23:08 06/22/22 07:31 100-41-4 Hexachloro-1,3-butadiene ND mg/kg 0.012 0.0094 1 06/21/22 23:08 06/22/22 07:31 87-68-3 2-Hexanone ND mg/kg 0.058 0.0056 1 06/21/22 23:08 06/22/22 07:31 591-78-6 Isopropylbenzene (Cumene) ND mg/kg 0.0058 0.0020 1 06/21/22 23:08 06/22/22 07:31 98-82-8 p-Isopropyltoluene ND mg/kg 0.0058 0.0028 1 06/21/22 23:08 06/22/22 07:31 99-87-6 Methylene Chloride ND mg/kg 0.023 0.016 1 06/21/22 23:08 06/22/22 07:31 75-09-2 4-Methyl-2-pentanone (MIBK) ND mg/kg 0.058 0.0056 1 06/21/22 23:08 06/22/22 07:31 108-10-1 Methyl-tert-butyl ether ND mg/kg 0.0058 0.0022 1 06/21/22 23:08 06/22/22 07:31 1634-04-4 Naphthalene ND mg/kg 0.0058 0.0030 1 06/21/22 23:08 06/22/22 07:31 91-20-3 n-Propylbenzene ND mg/kg 0.0058 0.0021 1 06/21/22 23:08 06/22/22 07:31 103-65-1 Styrene ND mg/kg 0.0058 0.0015 1 06/21/22 23:08 06/22/22 07:31 100-42-5 1,1,1,2-Tetrachloroethane ND mg/kg 0.0058 0.0022 1 06/21/22 23:08 06/22/22 07:31 630-20-6 1,1,2,2-Tetrachloroethane ND mg/kg 0.0058 0.0015 1 06/21/22 23:08 06/22/22 07:31 79-34-5 Tetrachloroethene ND mg/kg 0.0058 0.0018 1 06/21/22 23:08 06/22/22 07:31 127-18-4 Toluene ND mg/kg 0.0058 0.0016 1 06/21/22 23:08 06/22/22 07:31 108-88-3 1,2,3-Trichlorobenzene ND mg/kg 0.0058 0.0047 1 06/21/22 23:08 06/22/22 07:31 87-61-6 1,2,4-Trichlorobenzene ND mg/kg 0.0058 0.0048 1 06/21/22 23:08 06/22/22 07:31 120-82-1 REPORT OF LABORATORY ANALYSIS IK IK This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: DUP-2 Lab ID: 92610717003 Collected: 06/17/22 00:00 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Total Solids 2540 G-2011 Total Solids Wet Chemistry 7199 Chromium, Hexavalent Date: 07/21 /2022 05:22 PM Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte ND mg/kg 0.0058 0.0030 1 06/21 /22 23:08 06/22/22 07:31 71-55-6 ND mg/kg 0.0058 0.0019 1 06/21 /22 23:08 06/22/22 07:31 79-00-5 ND mg/kg 0.0058 0.0015 1 06/21 /22 23:08 06/22/22 07:31 79-01-6 ND mg/kg 0.0058 0.0032 1 06/21 /22 23:08 06/22/22 07:31 75-69-4 ND mg/kg 0.0058 0.0029 1 06/21/22 23:08 06/22/22 07:31 96-18-4 ND mg/kg 0.0058 0.0016 1 06/21 /22 23:08 06/22/22 07:31 95-63-6 ND mg/kg 0.0058 0.0019 1 06/21 /22 23:08 06/22/22 07:31 108-67-8 ND mg/kg 0.058 0.0042 1 06/21 /22 23:08 06/22/22 07:31 108-05-4 ND mg/kg 0.012 0.0029 1 06/21 /22 23:08 06/22/22 07:31 75-01-4 ND mg/kg 0.012 0.0033 1 06/21 /22 23:08 06/22/22 07:31 1330-20-7 ND mg/kg 0.012 0.0039 1 06/21 /22 23:08 06/22/22 07:31 179601-23-1 ND mg/kg 0.0058 0.0026 1 06/21 /22 23:08 06/22/22 07:31 95-47-6 99 % 70-130 1 06/21 /22 23:08 06/22/22 07:31 2037-26-5 99 % 69-134 1 06/21 /22 23:08 06/22/22 07:31 460-00-4 86 % 70-130 1 06/21 /22 23:08 06/22/22 07:31 17060-07-0 Analytical Method: SW-846 Pace Analytical Services - Charlotte 13.1 % 0.10 0.10 1 06/21 /22 16:47 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet 90.6 % 1 06/27/2213:04 06/27/2213:11 Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet ND mg/kg 1.10 0.281 1 07/13/2214:13 07/15/2211:20 18540-29-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 Page 23 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: BG-1 Lab ID: 92610717004 Collected: 06/17/22 09:10 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual OP Pesticides 8141 B Analytical Method: EPA 8141 B Preparation Method: 3546 Pace National - Mt. Juliet Azinphos, methyl (Guthion) ND mg/kg 0.122 0.0387 1 06/23/22 16:09 06/24/22 04:35 86-50-0 Bolstar ND mg/kg 0.122 0.0181 1 06/23/22 16:09 06/24/22 04:35 35400-43-2 Chlorpyrifos ND mg/kg 0.122 0.0191 1 06/23/22 16:09 06/24/22 04:35 2921-88-2 Coumaphos ND mg/kg 0.122 0.0296 1 06/23/22 16:09 06/24/22 04:35 56-72-4 Total Demeton ND mg/kg 0.0852 0.00711 1 06/23/22 16:09 06/24/22 04:35 8065-48-3 Diazinon ND mg/kg 0.122 0.0274 1 06/23/22 16:09 06/24/22 04:35 333-41-5 Dichlorvos ND mg/kg 0.122 0.0365 1 06/23/22 16:09 06/24/22 04:35 62-73-7 Dimethoate ND mg/kg 0.122 0.0407 1 06/23/22 16:09 06/24/22 04:35 60-51-5 Disulfoton ND mg/kg 0.122 0.0309 1 06/23/22 16:09 06/24/22 04:35 298-04-4 EPN (ENT) ND mg/kg 0.122 0.0336 1 06/23/22 16:09 06/24/22 04:35 2104-64-5 Ethoprop ND mg/kg 0.122 0.0144 1 06/23/22 16:09 06/24/22 04:35 13194-48-4 Parathion (Ethyl parathion) ND mg/kg 0.122 0.0200 1 06/23/22 16:09 06/24/22 04:35 56-38-2 Fensulfothion ND mg/kg 0.122 0.0430 1 06/23/22 16:09 06/24/22 04:35 115-90-2 Fenthion ND mg/kg 0.122 0.0162 1 06/23/22 16:09 06/24/22 04:35 55-38-9 Malathion ND mg/kg 0.122 0.0218 1 06/23/22 16:09 06/24/22 04:35 121-75-5 Merphos ND mg/kg 0.122 0.0282 1 06/23/22 16:09 06/24/22 04:35 150-50-5 Methyl parathion ND mg/kg 0.122 0.0247 1 06/23/22 16:09 06/24/22 04:35 298-00-0 Mevinphos ND mg/kg 0.122 0.0280 1 06/23/22 16:09 06/24/22 04:35 7786-34-7 Naled ND mg/kg 0.122 0.0584 1 06/23/22 16:09 06/24/22 04:35 300-76-5 Phorate ND mg/kg 0.122 0.0256 1 06/23/22 16:09 06/24/22 04:35 298-02-2 Ronnel ND mg/kg 0.122 0.0181 1 06/23/22 16:09 06/24/22 04:35 299-84-3 Stirophos (Tetrachlorvinphos) ND mg/kg 0.122 0.0217 1 06/23/22 16:09 06/24/22 04:35 22248-79-9 Sulfotepp (ThiodiphosphoricAc ND mg/kg 0.122 0.0120 1 06/23/22 16:09 06/24/22 04:35 3689-24-5 TEPP ND mg/kg 1.22 0.191 1 06/23/22 16:09 06/24/22 04:35 107-49-3 Tokuthion (Prothiofos) ND mg/kg 0.122 0.0183 1 06/23/22 16:09 06/24/22 04:35 34643-46-4 Trichloronate ND mg/kg 0.122 0.0245 1 06/23/22 16:09 06/24/22 04:35 327-98-0 Surrogates Triphenylphosphate (S) 71.1 % 36.0-121 1 06/23/22 16:09 06/24/22 04:35 115-86-6 Chlorinated Herb. (GC) 8151 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND mg/kg 0.0852 0.00854 1 06/29/2214:20 07/01/2215:52 94-75-7 Dalapon ND mg/kg 0.0852 0.0138 1 06/29/2214:20 07/01/2215:52 127-20-8 2,4-DB ND mg/kg 0.0852 0.0361 1 06/29/2214:20 07/01/2215:52 94-82-6 Dicamba ND mg/kg 0.0852 0.0191 1 06/29/2214:20 07/01/2215:52 1918-00-9 Dichloroprop ND mg/kg 0.0852 0.0298 1 06/29/2214:20 07/01/2215:52 15165-67-0 Dinoseb ND mg/kg 0.0852 0.00848 1 06/29/2214:20 07/01/2215:52 88-85-7 MCPA ND mg/kg 7.91 0.539 1 06/29/2214:20 07/01/2215:52 94-74-6 MCPP ND mg/kg 7.91 0.447 1 06/29/2214:20 07/01/2215:52 7085-19-0 2,4,5-T ND mg/kg 0.0852 0.0104 1 06/29/2214:20 07/01/2215:52 93-76-5 2,4,5-TP (Silvex) ND mg/kg 0.0852 0.0130 1 06/29/22 14:20 07/01/22 15:52 93-72-1 Surrogates 2,4-DCAA(S) 73.1 % 22.0-132 1 06/29/2214:20 07/01/2215:52 19719-28-9 REPORT OF LABORATORY ANALYSIS LO R1 R1 R1 R1 R1 R1 R1 R1 This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: BG-1 Lab ID: 92610717004 Collected: 06/17/22 09:10 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan 11 Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Heptachlor Heptachlor epoxide Hexachlorobenzene Methoxychlor Mirex Toxaphene Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) Percent Moisture Percent Moisture Total Solids 2540 G-2011 Total Solids Analytical Method: EPA 8081 B Preparation Method: EPA 3546 Pace Analytical Services - Charlotte ND mg/kg 0.0024 0.00096 1 06/22/2216:23 06/27/2215:50 309-00-2 ND mg/kg 0.0024 0.0010 1 06/22/2216:23 06/27/2215:50 319-84-6 ND mg/kg 0.0024 0.0011 1 06/22/2216:23 06/27/2215:50 319-85-7 ND mg/kg 0.0024 0.0012 1 06/22/2216:23 06/27/2215:50 319-86-8 ND mg/kg 0.0024 0.00095 1 06/22/2216:23 06/27/2215:50 58-89-9 ND mg/kg 0.012 0.010 1 06/22/2216:23 06/27/2215:50 57-74-9 ND mg/kg 0.0024 0.0011 1 06/22/2216:23 06/27/2215:50 72-54-8 ND mg/kg 0.0024 0.0011 1 06/22/2216:23 06/27/2215:50 72-55-9 ND mg/kg 0.0024 0.0011 1 06/22/2216:23 06/27/2215:50 50-29-3 ND mg/kg 0.0024 0.0010 1 06/22/2216:23 06/27/2215:50 60-57-1 ND mg/kg 0.0024 0.0010 1 06/22/2216:23 06/27/2215:50 959-98-8 ND mg/kg 0.0024 0.0011 1 06/22/2216:23 06/27/2215:50 33213-65-9 ND mg/kg 0.0024 0.0013 1 06/22/2216:23 06/27/2215:50 1031-07-8 ND mg/kg 0.0024 0.0011 1 06/22/2216:23 06/27/2215:50 72-20-8 ND mg/kg 0.0024 0.0016 1 06/22/2216:23 06/27/2215:50 7421-93-4 ND mg/kg 0.0024 0.0013 1 06/22/2216:23 06/27/2215:50 53494-70-5 ND mg/kg 0.0024 0.0011 1 06/22/2216:23 06/27/2215:50 76-44-8 ND mg/kg 0.0024 0.00094 1 06/22/2216:23 06/27/2215:50 1024-57-3 ND mg/kg 0.0024 0.00098 1 06/22/2216:23 06/27/2215:50 118-74-1 ND mg/kg 0.0059 0.0029 1 06/22/2216:23 06/27/2215:50 72-43-5 ND mg/kg 0.0059 0.0026 1 06/22/2216:23 06/27/2215:50 2385-85-5 ND mg/kg 0.0083 0.0063 1 06/22/2216:23 06/27/2215:50 8001-35-2 72 % 10-133 1 06/22/2216:23 06/27/2215:50 877-09-8 72 % 10-146 1 06/22/2216:23 06/27/2215:50 2051-24-3 Analytical Method: SW-846 Pace Analytical Services - Charlotte 16.2 % 0.10 0.10 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet 82.2 % 06/21 /22 16:47 1 06/27/2213:04 06/27/2213:11 REPORT OF LABORATORY ANALYSIS N2 This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: 13G-2 Lab ID: 92610717005 Collected: 06/17/22 09:20 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual OP Pesticides 8141 B Analytical Method: EPA 8141 B Preparation Method: 3546 Pace National - Mt. Juliet Azinphos, methyl (Guthion) ND mg/kg 0.128 0.0408 1 06/23/22 16:09 06/24/22 05:09 86-50-0 Bolstar ND mg/kg 0.128 0.0191 1 06/23/22 16:09 06/24/22 05:09 35400-43-2 Chlorpyrifos ND mg/kg 0.128 0.0201 1 06/23/22 16:09 06/24/22 05:09 2921-88-2 Coumaphos ND mg/kg 0.128 0.0312 1 06/23/22 16:09 06/24/22 05:09 56-72-4 Total Demeton ND mg/kg 0.0898 0.00749 1 06/23/22 16:09 06/24/22 05:09 8065-48-3 Diazinon ND mg/kg 0.128 0.0289 1 06/23/22 16:09 06/24/22 05:09 333-41-5 Dichlorvos ND mg/kg 0.128 0.0385 1 06/23/22 16:09 06/24/22 05:09 62-73-7 Dimethoate ND mg/kg 0.128 0.0429 1 06/23/22 16:09 06/24/22 05:09 60-51-5 Disulfoton ND mg/kg 0.128 0.0326 1 06/23/22 16:09 06/24/22 05:09 298-04-4 EPN (ENT) ND mg/kg 0.128 0.0354 1 06/23/22 16:09 06/24/22 05:09 2104-64-5 Ethoprop ND mg/kg 0.128 0.0151 1 06/23/22 16:09 06/24/22 05:09 13194-48-4 Parathion (Ethyl parathion) ND mg/kg 0.128 0.0210 1 06/23/22 16:09 06/24/22 05:09 56-38-2 Fensulfothion ND mg/kg 0.128 0.0453 1 06/23/22 16:09 06/24/22 05:09 115-90-2 Fenthion ND mg/kg 0.128 0.0171 1 06/23/22 16:09 06/24/22 05:09 55-38-9 Malathion ND mg/kg 0.128 0.0230 1 06/23/22 16:09 06/24/22 05:09 121-75-5 Merphos ND mg/kg 0.128 0.0298 1 06/23/22 16:09 06/24/22 05:09 150-50-5 Methyl parathion ND mg/kg 0.128 0.0260 1 06/23/22 16:09 06/24/22 05:09 298-00-0 Mevinphos ND mg/kg 0.128 0.0295 1 06/23/22 16:09 06/24/22 05:09 7786-34-7 Naled ND mg/kg 0.128 0.0616 1 06/23/22 16:09 06/24/22 05:09 300-76-5 Phorate ND mg/kg 0.128 0.0269 1 06/23/22 16:09 06/24/22 05:09 298-02-2 Ronnel ND mg/kg 0.128 0.0191 1 06/23/22 16:09 06/24/22 05:09 299-84-3 Stirophos (Tetrachlorvinphos) ND mg/kg 0.128 0.0228 1 06/23/22 16:09 06/24/22 05:09 22248-79-9 Sulfotepp (ThiodiphosphoricAc ND mg/kg 0.128 0.0127 1 06/23/22 16:09 06/24/22 05:09 3689-24-5 TEPP ND mg/kg 1.28 0.201 1 06/23/22 16:09 06/24/22 05:09 107-49-3 Tokuthion (Prothiofos) ND mg/kg 0.128 0.0192 1 06/23/22 16:09 06/24/22 05:09 34643-46-4 Trichloronate ND mg/kg 0.128 0.0258 1 06/23/22 16:09 06/24/22 05:09 327-98-0 Surrogates Triphenylphosphate (S) 70.4 % 36.0-121 1 06/23/22 16:09 06/24/22 05:09 115-86-6 Chlorinated Herb. (GC) 8151 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND mg/kg 0.0898 0.00901 1 06/30/22 21:57 07/03/22 04:45 94-75-7 Dalapon ND mg/kg 0.0898 0.0145 1 06/30/22 21:57 07/03/22 04:45 127-20-8 2,4-DB ND mg/kg 0.0898 0.0381 1 06/30/22 21:57 07/03/22 04:45 94-82-6 Dicamba ND mg/kg 0.0898 0.0201 1 06/30/22 21:57 07/03/22 04:45 1918-00-9 Dichloroprop ND mg/kg 0.0898 0.0314 1 06/30/22 21:57 07/03/22 04:45 15165-67-0 Dinoseb ND mg/kg 0.0898 0.00894 1 06/30/22 21:57 07/03/22 04:45 88-85-7 MCPA ND mg/kg 8.34 0.568 1 06/30/22 21:57 07/03/22 04:45 94-74-6 MCPP ND mg/kg 8.34 0.471 1 06/30/22 21:57 07/03/22 04:45 7085-19-0 2,4,5-T ND mg/kg 0.0898 0.0109 1 06/30/22 21:57 07/03/22 04:45 93-76-5 2,4,5-TP (Silvex) ND mg/kg 0.0898 0.0137 1 06/30/22 21:57 07/03/22 04:45 93-72-1 Surrogates 2,4-DCAA (S) 55.7 % 22.0-132 1 06/30/22 21:57 07/03/22 04:45 19719-28-9 REPORT OF LABORATORY ANALYSIS LO LO LO LO LO LO LO This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: 13G-2 Lab ID: 92610717005 Collected: 06/17/22 09:20 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan 11 Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Heptachlor Heptachlor epoxide Hexachlorobenzene Methoxychlor Mirex Toxaphene Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) Percent Moisture Percent Moisture Total Solids 2540 G-2011 Total Solids Analytical Method: EPA 8081 B Preparation Method: EPA 3546 Pace Analytical Services - Charlotte ND mg/kg 0.0023 0.00095 1 06/22/2216:23 06/27/2216:02 309-00-2 ND mg/kg 0.0023 0.0010 1 06/22/2216:23 06/27/2216:02 319-84-6 ND mg/kg 0.0023 0.0011 1 06/22/2216:23 06/27/2216:02 319-85-7 ND mg/kg 0.0023 0.0012 1 06/22/2216:23 06/27/2216:02 319-86-8 ND mg/kg 0.0023 0.00094 1 06/22/2216:23 06/27/2216:02 58-89-9 ND mg/kg 0.012 0.010 1 06/22/2216:23 06/27/2216:02 57-74-9 ND mg/kg 0.0023 0.0011 1 06/22/2216:23 06/27/2216:02 72-54-8 ND mg/kg 0.0023 0.0011 1 06/22/2216:23 06/27/2216:02 72-55-9 ND mg/kg 0.0023 0.0010 1 06/22/2216:23 06/27/2216:02 50-29-3 ND mg/kg 0.0023 0.0010 1 06/22/2216:23 06/27/2216:02 60-57-1 ND mg/kg 0.0023 0.0010 1 06/22/2216:23 06/27/2216:02 959-98-8 ND mg/kg 0.0023 0.0011 1 06/22/2216:23 06/27/2216:02 33213-65-9 ND mg/kg 0.0023 0.0013 1 06/22/2216:23 06/27/2216:02 1031-07-8 ND mg/kg 0.0023 0.0011 1 06/22/2216:23 06/27/2216:02 72-20-8 ND mg/kg 0.0023 0.0016 1 06/22/2216:23 06/27/2216:02 7421-93-4 ND mg/kg 0.0023 0.0013 1 06/22/2216:23 06/27/2216:02 53494-70-5 ND mg/kg 0.0023 0.0011 1 06/22/2216:23 06/27/2216:02 76-44-8 ND mg/kg 0.0023 0.00093 1 06/22/2216:23 06/27/2216:02 1024-57-3 ND mg/kg 0.0023 0.00097 1 06/22/2216:23 06/27/2216:02 118-74-1 ND mg/kg 0.0059 0.0029 1 06/22/2216:23 06/27/2216:02 72-43-5 ND mg/kg 0.0059 0.0026 1 06/22/2216:23 06/27/2216:02 2385-85-5 ND mg/kg 0.0082 0.0063 1 06/22/2216:23 06/27/2216:02 8001-35-2 57 % 10-133 1 06/22/2216:23 06/27/2216:02 877-09-8 65 % 10-146 1 06/22/2216:23 06/27/2216:02 2051-24-3 Analytical Method: SW-846 Pace Analytical Services - Charlotte 15.8 % 0.10 0.10 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet 77.9 % 06/21 /22 16:47 1 06/24/22 09:03 06/24/22 09:14 REPORT OF LABORATORY ANALYSIS N2 This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: 13G-3 Lab ID: 92610717006 Collected: 06/17/22 09:45 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual OP Pesticides 8141 B Analytical Method: EPA 8141 B Preparation Method: 3546 Pace National - Mt. Juliet Azinphos, methyl (Guthion) ND mg/kg 0.127 0.0405 1 06/23/22 16:09 06/24/22 05:43 86-50-0 Bolstar ND mg/kg 0.127 0.0190 1 06/23/22 16:09 06/24/22 05:43 35400-43-2 Chlorpyrifos ND mg/kg 0.127 0.0200 1 06/23/22 16:09 06/24/22 05:43 2921-88-2 Coumaphos ND mg/kg 0.127 0.0309 1 06/23/22 16:09 06/24/22 05:43 56-72-4 Total Demeton ND mg/kg 0.0890 0.00743 1 06/23/22 16:09 06/24/22 05:43 8065-48-3 Diazinon ND mg/kg 0.127 0.0286 1 06/23/22 16:09 06/24/22 05:43 333-41-5 Dichlorvos ND mg/kg 0.127 0.0382 1 06/23/22 16:09 06/24/22 05:43 62-73-7 Dimethoate ND mg/kg 0.127 0.0425 1 06/23/22 16:09 06/24/22 05:43 60-51-5 Disulfoton ND mg/kg 0.127 0.0323 1 06/23/22 16:09 06/24/22 05:43 298-04-4 EPN (ENT) ND mg/kg 0.127 0.0351 1 06/23/22 16:09 06/24/22 05:43 2104-64-5 Ethoprop ND mg/kg 0.127 0.0150 1 06/23/22 16:09 06/24/22 05:43 13194-48-4 Parathion (Ethyl parathion) ND mg/kg 0.127 0.0209 1 06/23/22 16:09 06/24/22 05:43 56-38-2 Fensulfothion ND mg/kg 0.127 0.0449 1 06/23/22 16:09 06/24/22 05:43 115-90-2 Fenthion ND mg/kg 0.127 0.0169 1 06/23/22 16:09 06/24/22 05:43 55-38-9 Malathion ND mg/kg 0.127 0.0228 1 06/23/22 16:09 06/24/22 05:43 121-75-5 Merphos ND mg/kg 0.127 0.0295 1 06/23/22 16:09 06/24/22 05:43 150-50-5 Methyl parathion ND mg/kg 0.127 0.0258 1 06/23/22 16:09 06/24/22 05:43 298-00-0 Mevinphos ND mg/kg 0.127 0.0293 1 06/23/22 16:09 06/24/22 05:43 7786-34-7 Naled ND mg/kg 0.127 0.0611 1 06/23/22 16:09 06/24/22 05:43 300-76-5 Phorate ND mg/kg 0.127 0.0267 1 06/23/22 16:09 06/24/22 05:43 298-02-2 Ronnel ND mg/kg 0.127 0.0190 1 06/23/22 16:09 06/24/22 05:43 299-84-3 Stirophos (Tetrachlorvinphos) ND mg/kg 0.127 0.0226 1 06/23/22 16:09 06/24/22 05:43 22248-79-9 Sulfotepp (ThiodiphosphoricAc ND mg/kg 0.127 0.0125 1 06/23/22 16:09 06/24/22 05:43 3689-24-5 TEPP ND mg/kg 1.27 0.200 1 06/23/22 16:09 06/24/22 05:43 107-49-3 Tokuthion (Prothiofos) ND mg/kg 0.127 0.0191 1 06/23/22 16:09 06/24/22 05:43 34643-46-4 Trichloronate ND mg/kg 0.127 0.0256 1 06/23/22 16:09 06/24/22 05:43 327-98-0 Surrogates Triphenylphosphate (S) 79.0 % 36.0-121 1 06/23/22 16:09 06/24/22 05:43 115-86-6 Chlorinated Herb. (GC) 8151 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND mg/kg 0.0890 0.00893 1 06/30/22 21:57 07/03/22 05:00 94-75-7 Dalapon ND mg/kg 0.0890 0.0144 1 06/30/22 21:57 07/03/22 05:00 127-20-8 2,4-DB ND mg/kg 0.0890 0.0378 1 06/30/22 21:57 07/03/22 05:00 94-82-6 Dicamba ND mg/kg 0.0890 0.0200 1 06/30/22 21:57 07/03/22 05:00 1918-00-9 Dichloroprop ND mg/kg 0.0890 0.0312 1 06/30/22 21:57 07/03/22 05:00 15165-67-0 Dinoseb ND mg/kg 0.0890 0.00887 1 06/30/22 21:57 07/03/22 05:00 88-85-7 MCPA ND mg/kg 8.27 0.564 1 06/30/22 21:57 07/03/22 05:00 94-74-6 MCPP ND mg/kg 8.27 0.467 1 06/30/22 21:57 07/03/22 05:00 7085-19-0 2,4,5-T ND mg/kg 0.0890 0.0108 1 06/30/22 21:57 07/03/22 05:00 93-76-5 2,4,5-TP (Silvex) ND mg/kg 0.0890 0.0136 1 06/30/22 21:57 07/03/22 05:00 93-72-1 Surrogates 2,4-DCAA (S) 51.4 % 22.0-132 1 06/30/22 21:57 07/03/22 05:00 19719-28-9 REPORT OF LABORATORY ANALYSIS LO LO LO LO LO LO LO This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: 13G-3 Lab ID: 92610717006 Collected: 06/17/22 09:45 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan 11 Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Heptachlor Heptachlor epoxide Hexachlorobenzene Methoxychlor Mirex Toxaphene Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) Percent Moisture Percent Moisture Total Solids 2540 G-2011 Total Solids Analytical Method: EPA 8081 B Preparation Method: EPA 3546 Pace Analytical Services - Charlotte ND mg/kg 0.011 0.0045 5 06/22/2216:23 06/27/2216:13 309-00-2 ND mg/kg 0.011 0.0049 5 06/22/2216:23 06/27/2216:13 319-84-6 ND mg/kg 0.011 0.0054 5 06/22/2216:23 06/27/2216:13 319-85-7 ND mg/kg 0.011 0.0056 5 06/22/2216:23 06/27/2216:13 319-86-8 ND mg/kg 0.011 0.0045 5 06/22/2216:23 06/27/2216:13 58-89-9 ND mg/kg 0.056 0.049 5 06/22/2216:23 06/27/2216:13 57-74-9 ND mg/kg 0.011 0.0051 5 06/22/2216:23 06/27/2216:13 72-54-8 ND mg/kg 0.011 0.0053 5 06/22/2216:23 06/27/2216:13 72-55-9 ND mg/kg 0.011 0.0050 5 06/22/2216:23 06/27/2216:13 50-29-3 ND mg/kg 0.011 0.0049 5 06/22/2216:23 06/27/2216:13 60-57-1 ND mg/kg 0.011 0.0048 5 06/22/2216:23 06/27/2216:13 959-98-8 ND mg/kg 0.011 0.0051 5 06/22/2216:23 06/27/2216:13 33213-65-9 ND mg/kg 0.011 0.0062 5 06/22/2216:23 06/27/2216:13 1031-07-8 ND mg/kg 0.011 0.0052 5 06/22/2216:23 06/27/2216:13 72-20-8 ND mg/kg 0.011 0.0075 5 06/22/2216:23 06/27/2216:13 7421-93-4 ND mg/kg 0.011 0.0062 5 06/22/2216:23 06/27/2216:13 53494-70-5 ND mg/kg 0.011 0.0052 5 06/22/2216:23 06/27/2216:13 76-44-8 ND mg/kg 0.011 0.0044 5 06/22/2216:23 06/27/2216:13 1024-57-3 ND mg/kg 0.011 0.0046 5 06/22/2216:23 06/27/2216:13 118-74-1 ND mg/kg 0.028 0.014 5 06/22/2216:23 06/27/2216:13 72-43-5 ND mg/kg 0.028 0.012 5 06/22/2216:23 06/27/2216:13 2385-85-5 ND mg/kg 0.039 0.030 5 06/22/2216:23 06/27/2216:13 8001-35-2 75 % 10-133 5 06/22/2216:23 06/27/2216:13 877-09-8 D3 120 % 10-146 5 06/22/2216:23 06/27/2216:13 2051-24-3 Analytical Method: SW-846 Pace Analytical Services - Charlotte 11.1 % 0.10 0.10 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet 78.6 % 06/21 /22 16:47 1 06/24/22 09:03 06/24/22 09:14 REPORT OF LABORATORY ANALYSIS N2 This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: 13G-4 Lab ID: 92610717007 Collected: 06/17/22 09:45 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual OP Pesticides 8141 B Analytical Method: EPA 8141 B Preparation Method: 3546 Pace National - Mt. Juliet Azinphos, methyl (Guthion) ND mg/kg 0.123 0.0392 1 06/23/22 16:09 06/24/22 06:16 86-50-0 Bolstar ND mg/kg 0.123 0.0184 1 06/23/22 16:09 06/24/22 06:16 35400-43-2 Chlorpyrifos ND mg/kg 0.123 0.0194 1 06/23/22 16:09 06/24/22 06:16 2921-88-2 Coumaphos ND mg/kg 0.123 0.0300 1 06/23/22 16:09 06/24/22 06:16 56-72-4 Total Demeton ND mg/kg 0.0863 0.00720 1 06/23/22 16:09 06/24/22 06:16 8065-48-3 Diazinon ND mg/kg 0.123 0.0277 1 06/23/22 16:09 06/24/22 06:16 333-41-5 Dichlorvos ND mg/kg 0.123 0.0370 1 06/23/22 16:09 06/24/22 06:16 62-73-7 Dimethoate ND mg/kg 0.123 0.0412 1 06/23/22 16:09 06/24/22 06:16 60-51-5 Disulfoton ND mg/kg 0.123 0.0313 1 06/23/22 16:09 06/24/22 06:16 298-04-4 EPN (ENT) ND mg/kg 0.123 0.0340 1 06/23/22 16:09 06/24/22 06:16 2104-64-5 Ethoprop ND mg/kg 0.123 0.0145 1 06/23/22 16:09 06/24/22 06:16 13194-48-4 Parathion (Ethyl parathion) ND mg/kg 0.123 0.0202 1 06/23/22 16:09 06/24/22 06:16 56-38-2 Fensulfothion ND mg/kg 0.123 0.0435 1 06/23/22 16:09 06/24/22 06:16 115-90-2 Fenthion ND mg/kg 0.123 0.0164 1 06/23/22 16:09 06/24/22 06:16 55-38-9 Malathion ND mg/kg 0.123 0.0221 1 06/23/22 16:09 06/24/22 06:16 121-75-5 Merphos ND mg/kg 0.123 0.0286 1 06/23/22 16:09 06/24/22 06:16 150-50-5 Methyl parathion ND mg/kg 0.123 0.0250 1 06/23/22 16:09 06/24/22 06:16 298-00-0 Mevinphos ND mg/kg 0.123 0.0284 1 06/23/22 16:09 06/24/22 06:16 7786-34-7 Naled ND mg/kg 0.123 0.0592 1 06/23/22 16:09 06/24/22 06:16 300-76-5 Phorate ND mg/kg 0.123 0.0259 1 06/23/22 16:09 06/24/22 06:16 298-02-2 Ronnel ND mg/kg 0.123 0.0184 1 06/23/22 16:09 06/24/22 06:16 299-84-3 Stirophos (Tetrachlorvinphos) ND mg/kg 0.123 0.0219 1 06/23/22 16:09 06/24/22 06:16 22248-79-9 Sulfotepp (ThiodiphosphoricAc ND mg/kg 0.123 0.0122 1 06/23/22 16:09 06/24/22 06:16 3689-24-5 TEPP ND mg/kg 1.23 0.194 1 06/23/22 16:09 06/24/22 06:16 107-49-3 Tokuthion (Prothiofos) ND mg/kg 0.123 0.0185 1 06/23/22 16:09 06/24/22 06:16 34643-46-4 Trichloronate ND mg/kg 0.123 0.0248 1 06/23/22 16:09 06/24/22 06:16 327-98-0 Surrogates Triphenylphosphate (S) 72.4 % 36.0-121 1 06/23/22 16:09 06/24/22 06:16 115-86-6 Chlorinated Herb. (GC) 8151 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND mg/kg 0.0863 0.00866 1 06/30/22 21:57 07/03/22 05:59 94-75-7 Dalapon ND mg/kg 0.0863 0.0139 1 06/30/22 21:57 07/03/22 05:59 127-20-8 2,4-DB ND mg/kg 0.0863 0.0366 1 06/30/22 21:57 07/03/22 05:59 94-82-6 Dicamba ND mg/kg 0.0863 0.0194 1 06/30/22 21:57 07/03/22 05:59 1918-00-9 Dichloroprop ND mg/kg 0.0863 0.0302 1 06/30/22 21:57 07/03/22 05:59 15165-67-0 Dinoseb ND mg/kg 0.0863 0.00859 1 06/30/22 21:57 07/03/22 05:59 88-85-7 MCPA ND mg/kg 8.01 0.546 1 06/30/22 21:57 07/03/22 05:59 94-74-6 MCPP ND mg/kg 8.01 0.453 1 06/30/22 21:57 07/03/22 05:59 7085-19-0 2,4,5-T ND mg/kg 0.0863 0.0105 1 06/30/22 21:57 07/03/22 05:59 93-76-5 2,4,5-TP (Silvex) ND mg/kg 0.0863 0.0132 1 06/30/22 21:57 07/03/22 05:59 93-72-1 Surrogates 2,4-DCAA (S) 59.5 % 22.0-132 1 06/30/22 21:57 07/03/22 05:59 19719-28-9 REPORT OF LABORATORY ANALYSIS LO LO LO LO LO LO LO This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: 13G-4 Lab ID: 92610717007 Collected: 06/17/22 09:45 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan 11 Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Heptachlor Heptachlor epoxide Hexachlorobenzene Methoxychlor Mirex Toxaphene Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) Percent Moisture Percent Moisture Total Solids 2540 G-2011 Total Solids Analytical Method: EPA 8081 B Preparation Method: EPA 3546 Pace Analytical Services - Charlotte ND mg/kg 0.012 0.0050 5 06/22/2216:23 06/27/2216:24 309-00-2 ND mg/kg 0.012 0.0054 5 06/22/2216:23 06/27/2216:24 319-84-6 ND mg/kg 0.012 0.0060 5 06/22/2216:23 06/27/2216:24 319-85-7 ND mg/kg 0.012 0.0062 5 06/22/2216:23 06/27/2216:24 319-86-8 ND mg/kg 0.012 0.0050 5 06/22/2216:23 06/27/2216:24 58-89-9 ND mg/kg 0.062 0.054 5 06/22/2216:23 06/27/2216:24 57-74-9 ND mg/kg 0.012 0.0056 5 06/22/2216:23 06/27/2216:24 72-54-8 ND mg/kg 0.012 0.0059 5 06/22/2216:23 06/27/2216:24 72-55-9 ND mg/kg 0.012 0.0055 5 06/22/2216:23 06/27/2216:24 50-29-3 ND mg/kg 0.012 0.0054 5 06/22/2216:23 06/27/2216:24 60-57-1 ND mg/kg 0.012 0.0053 5 06/22/2216:23 06/27/2216:24 959-98-8 ND mg/kg 0.012 0.0056 5 06/22/2216:23 06/27/2216:24 33213-65-9 ND mg/kg 0.012 0.0069 5 06/22/2216:23 06/27/2216:24 1031-07-8 ND mg/kg 0.012 0.0058 5 06/22/2216:23 06/27/2216:24 72-20-8 ND mg/kg 0.012 0.0083 5 06/22/2216:23 06/27/2216:24 7421-93-4 ND mg/kg 0.012 0.0068 5 06/22/2216:23 06/27/2216:24 53494-70-5 ND mg/kg 0.012 0.0057 5 06/22/2216:23 06/27/2216:24 76-44-8 ND mg/kg 0.012 0.0049 5 06/22/2216:23 06/27/2216:24 1024-57-3 ND mg/kg 0.012 0.0051 5 06/22/2216:23 06/27/2216:24 118-74-1 ND mg/kg 0.031 0.015 5 06/22/2216:23 06/27/2216:24 72-43-5 ND mg/kg 0.031 0.014 5 06/22/2216:23 06/27/2216:24 2385-85-5 ND mg/kg 0.043 0.033 5 06/22/2216:23 06/27/2216:24 8001-35-2 62 % 10-133 5 06/22/2216:23 06/27/2216:24 877-09-8 D3 97 % 10-146 5 06/22/2216:23 06/27/2216:24 2051-24-3 Analytical Method: SW-846 Pace Analytical Services - Charlotte 19.7 % 0.10 0.10 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet 81.1 % 06/21 /22 16:47 1 06/24/22 09:03 06/24/22 09:14 REPORT OF LABORATORY ANALYSIS N2 This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: 13G-5 Lab ID: 92610717008 Collected: 06/17/22 10:15 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual OP Pesticides 8141 B Analytical Method: EPA 8141 B Preparation Method: 3546 Pace National - Mt. Juliet Azinphos, methyl (Guthion) ND mg/kg 0.121 0.0386 1 06/23/22 16:09 06/24/22 06:50 86-50-0 Bolstar ND mg/kg 0.121 0.0181 1 06/23/22 16:09 06/24/22 06:50 35400-43-2 Chlorpyrifos ND mg/kg 0.121 0.0190 1 06/23/22 16:09 06/24/22 06:50 2921-88-2 Coumaphos ND mg/kg 0.121 0.0295 1 06/23/22 16:09 06/24/22 06:50 56-72-4 Total Demeton ND mg/kg 0.0849 0.00708 1 06/23/22 16:09 06/24/22 06:50 8065-48-3 Diazinon ND mg/kg 0.121 0.0273 1 06/23/22 16:09 06/24/22 06:50 333-41-5 Dichlorvos ND mg/kg 0.121 0.0364 1 06/23/22 16:09 06/24/22 06:50 62-73-7 Dimethoate ND mg/kg 0.121 0.0405 1 06/23/22 16:09 06/24/22 06:50 60-51-5 Disulfoton ND mg/kg 0.121 0.0308 1 06/23/22 16:09 06/24/22 06:50 298-04-4 EPN (ENT) ND mg/kg 0.121 0.0335 1 06/23/22 16:09 06/24/22 06:50 2104-64-5 Ethoprop ND mg/kg 0.121 0.0143 1 06/23/22 16:09 06/24/22 06:50 13194-48-4 Parathion (Ethyl parathion) ND mg/kg 0.121 0.0199 1 06/23/22 16:09 06/24/22 06:50 56-38-2 Fensulfothion ND mg/kg 0.121 0.0428 1 06/23/22 16:09 06/24/22 06:50 115-90-2 Fenthion ND mg/kg 0.121 0.0161 1 06/23/22 16:09 06/24/22 06:50 55-38-9 Malathion ND mg/kg 0.121 0.0217 1 06/23/22 16:09 06/24/22 06:50 121-75-5 Merphos ND mg/kg 0.121 0.0281 1 06/23/22 16:09 06/24/22 06:50 150-50-5 Methyl parathion ND mg/kg 0.121 0.0246 1 06/23/22 16:09 06/24/22 06:50 298-00-0 Mevinphos ND mg/kg 0.121 0.0279 1 06/23/22 16:09 06/24/22 06:50 7786-34-7 Naled ND mg/kg 0.121 0.0582 1 06/23/22 16:09 06/24/22 06:50 300-76-5 Phorate ND mg/kg 0.121 0.0255 1 06/23/22 16:09 06/24/22 06:50 298-02-2 Ronnel ND mg/kg 0.121 0.0181 1 06/23/22 16:09 06/24/22 06:50 299-84-3 Stirophos (Tetrachlorvinphos) ND mg/kg 0.121 0.0216 1 06/23/22 16:09 06/24/22 06:50 22248-79-9 Sulfotepp (ThiodiphosphoricAc ND mg/kg 0.121 0.0120 1 06/23/22 16:09 06/24/22 06:50 3689-24-5 TEPP ND mg/kg 1.21 0.190 1 06/23/22 16:09 06/24/22 06:50 107-49-3 Tokuthion (Prothiofos) ND mg/kg 0.121 0.0182 1 06/23/22 16:09 06/24/22 06:50 34643-46-4 Trichloronate ND mg/kg 0.121 0.0244 1 06/23/22 16:09 06/24/22 06:50 327-98-0 Surrogates Triphenylphosphate (S) 68.5 % 36.0-121 1 06/23/22 16:09 06/24/22 06:50 115-86-6 Chlorinated Herb. (GC) 8151 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND mg/kg 0.0849 0.00851 1 06/30/22 21:57 07/03/22 06:13 94-75-7 Dalapon ND mg/kg 0.0849 0.0137 1 06/30/22 21:57 07/03/22 06:13 127-20-8 2,4-DB ND mg/kg 0.0849 0.0360 1 06/30/22 21:57 07/03/22 06:13 94-82-6 Dicamba ND mg/kg 0.0849 0.0190 1 06/30/22 21:57 07/03/22 06:13 1918-00-9 Dichloroprop ND mg/kg 0.0849 0.0297 1 06/30/22 21:57 07/03/22 06:13 15165-67-0 Dinoseb ND mg/kg 0.0849 0.00845 1 06/30/22 21:57 07/03/22 06:13 88-85-7 MCPA ND mg/kg 7.88 0.537 1 06/30/22 21:57 07/03/22 06:13 94-74-6 MCPP ND mg/kg 7.88 0.445 1 06/30/22 21:57 07/03/22 06:13 7085-19-0 2,4,5-T ND mg/kg 0.0849 0.0103 1 06/30/22 21:57 07/03/22 06:13 93-76-5 2,4,5-TP (Silvex) ND mg/kg 0.0849 0.0130 1 06/30/22 21:57 07/03/22 06:13 93-72-1 Surrogates 2,4-DCAA (S) 51.1 % 22.0-132 1 06/30/22 21:57 07/03/22 06:13 19719-28-9 REPORT OF LABORATORY ANALYSIS LO LO LO LO LO LO LO This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92610717 Sample: 13G-5 Lab ID: 92610717008 Collected: 06/17/22 10:15 Received: 06/17/22 16:56 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan 11 Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Heptachlor Heptachlor epoxide Hexachlorobenzene Methoxychlor Mirex Toxaphene Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) Percent Moisture Percent Moisture Total Solids 2540 G-2011 Total Solids Analytical Method: EPA 8081 B Preparation Method: EPA 3546 Pace Analytical Services - Charlotte ND mg/kg 0.0023 0.00092 1 06/22/2216:23 06/27/2216:36 309-00-2 ND mg/kg 0.0023 0.00099 1 06/22/2216:23 06/27/2216:36 319-84-6 ND mg/kg 0.0023 0.0011 1 06/22/2216:23 06/27/2216:36 319-85-7 ND mg/kg 0.0023 0.0011 1 06/22/2216:23 06/27/2216:36 319-86-8 ND mg/kg 0.0023 0.00091 1 06/22/2216:23 06/27/2216:36 58-89-9 ND mg/kg 0.011 0.0099 1 06/22/2216:23 06/27/2216:36 57-74-9 ND mg/kg 0.0023 0.0010 1 06/22/2216:23 06/27/2216:36 72-54-8 ND mg/kg 0.0023 0.0011 1 06/22/2216:23 06/27/2216:36 72-55-9 ND mg/kg 0.0023 0.0010 1 06/22/2216:23 06/27/2216:36 50-29-3 ND mg/kg 0.0023 0.00099 1 06/22/2216:23 06/27/2216:36 60-57-1 ND mg/kg 0.0023 0.00097 1 06/22/2216:23 06/27/2216:36 959-98-8 ND mg/kg 0.0023 0.0010 1 06/22/2216:23 06/27/2216:36 33213-65-9 ND mg/kg 0.0023 0.0013 1 06/22/2216:23 06/27/2216:36 1031-07-8 ND mg/kg 0.0023 0.0011 1 06/22/2216:23 06/27/2216:36 72-20-8 ND mg/kg 0.0023 0.0015 1 06/22/2216:23 06/27/2216:36 7421-93-4 ND mg/kg 0.0023 0.0012 1 06/22/2216:23 06/27/2216:36 53494-70-5 ND mg/kg 0.0023 0.0010 1 06/22/2216:23 06/27/2216:36 76-44-8 ND mg/kg 0.0023 0.00090 1 06/22/2216:23 06/27/2216:36 1024-57-3 ND mg/kg 0.0023 0.00094 1 06/22/2216:23 06/27/2216:36 118-74-1 ND mg/kg 0.0057 0.0028 1 06/22/2216:23 06/27/2216:36 72-43-5 ND mg/kg 0.0057 0.0025 1 06/22/2216:23 06/27/2216:36 2385-85-5 ND mg/kg 0.0080 0.0061 1 06/22/2216:23 06/27/2216:36 8001-35-2 78 % 10-133 1 06/22/2216:23 06/27/2216:36 877-09-8 84 % 10-146 1 06/22/2216:23 06/27/2216:36 2051-24-3 Analytical Method: SW-846 Pace Analytical Services - Charlotte 12.0 % 0.10 0.10 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet 82.5 % 06/21 /22 16:48 1 06/24/22 09:03 06/24/22 09:14 REPORT OF LABORATORY ANALYSIS N2 This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 QC Batch: 1883600 Analysis Method: EPA 8141 B QC Batch Method: 3546 Analysis Description: OP Pesticides 8141 B Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92610717001, 92610717002, 92610717003, 92610717004, 92610717005, 92610717006, 92610717007, 92610717008 METHOD BLANK: R3807279-1 Matrix: Solid Associated Lab Samples: 92610717001, 92610717002, 92610717003, 92610717004, 92610717005, 92610717006, 92610717007, 92610717008 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Azinphos, methyl (Guthion) mg/kg ND 0.100 0.0318 06/23/22 21:53 Bolstar mg/kg ND 0.100 0.0149 06/23/22 21:53 Chlorpyrifos mg/kg ND 0.100 0.0157 06/23/22 21:53 Coumaphos mg/kg ND 0.100 0.0243 06/23/22 21:53 Total Demeton mg/kg ND 0.0700 0.00584 06/23/22 21:53 Diazinon mg/kg ND 0.100 0.0225 06/23/22 21:53 Dichlorvos mg/kg ND 0.100 0.0300 06/23/22 21:53 Dimethoate mg/kg ND 0.100 0.0334 06/23/22 21:53 Disulfoton mg/kg ND 0.100 0.0254 06/23/22 21:53 EPN (ENT) mg/kg ND 0.100 0.0276 06/23/22 21:53 Ethoprop mg/kg ND 0.100 0.0118 06/23/22 21:53 Parathion (Ethyl parathion) mg/kg ND 0.100 0.0164 06/23/22 21:53 Fensulfothion mg/kg ND 0.100 0.0353 06/23/22 21:53 Fenthion mg/kg ND 0.100 0.0133 06/23/22 21:53 Malathion mg/kg ND 0.100 0.0179 06/23/22 21:53 Merphos mg/kg ND 0.100 0.0232 06/23/22 21:53 Methyl parathion mg/kg ND 0.100 0.0203 06/23/22 21:53 Mevinphos mg/kg ND 0.100 0.0230 06/23/22 21:53 Naled mg/kg ND 0.100 0.0480 06/23/22 21:53 Phorate mg/kg ND 0.100 0.0210 06/23/22 21:53 Ronnel mg/kg ND 0.100 0.0149 06/23/22 21:53 Stirophos (Tetrachlorvinphos) mg/kg ND 0.100 0.0178 06/23/22 21:53 Sulfotepp (ThiodiphosphoricAc mg/kg ND 0.100 0.00986 06/23/22 21:53 TEPP mg/kg ND 1.00 0.157 06/23/22 21:53 Tokuthion (Prothiofos) mg/kg ND 0.100 0.0150 06/23/22 21:53 Trichloronate mg/kg ND 0.100 0.0201 06/23/22 21:53 Triphenylphosphate (S) % 77.5 36.0-121 06/23/22 21:53 LABORATORY CONTROL SAMPLE: R3807279-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Azinphos, methyl (Guthion) mg/kg 0.333 0.266 79.9 58.0-125 Bolstar mg/kg 0.333 0.277 83.2 64.0-120 Chlorpyrifos mg/kg 0.333 0.281 84.4 62.0-120 Coumaphos mg/kg 0.333 0.269 80.8 60.0-120 Total Demeton mg/kg 0.167 0.137 82.0 59.0-120 Diazinon mg/kg 0.333 0.261 78.4 49.0-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 LABORATORY CONTROL SAMPLE: Parameter R3807279-2 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Dichlorvos mg/kg 0.333 0.199 59.8 37.0-120 Dimethoate mg/kg 0.333 0.284 85.3 46.0-127 Disulfoton mg/kg 0.333 0.280 84.1 60.0-121 EPN (ENT) mg/kg 0.333 0.277 83.2 60.0-121 Ethoprop mg/kg 0.333 0.285 85.6 59.0-120 Parathion (Ethyl parathion) mg/kg 0.333 0.282 84.7 62.0-120 Fensulfothion mg/kg 0.333 0.259 77.8 58.0-123 Fenthion mg/kg 0.333 0.295 88.6 61.0-121 Malathion mg/kg 0.333 0.290 87.1 59.0-120 Merphos mg/kg 0.333 0.247 74.2 59.0-120 Methyl parathion mg/kg 0.333 0.255 76.6 63.0-120 Mevinphos mg/kg 0.333 0.238 71.5 50.0-120 Naled mg/kg 0.333 0.137 41.1 10.0-125 Phorate mg/kg 0.333 0.263 79.0 60.0-120 Ronnel mg/kg 0.333 0.284 85.3 62.0-120 Stirophos (Tetrachlorvinphos) mg/kg 0.333 0.258 77.5 62.0-120 Sulfotepp (ThiodiphosphoricAc mg/kg 0.333 0.302 90.7 62.0-122 TEPP mg/kg 3.33 0.102 3.06 10.0-135 LO Tokuthion (Prothiofos) mg/kg 0.333 0.269 80.8 63.0-120 Trichloronate mg/kg 0.333 0.266 79.9 62.0-120 Triphenyl phosphate (S) % 81.1 36.0-121 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3807279-3 MS L1506471-04 Spike Parameter Units Result Conc. MSD Spike Conc. R3807279-4 MS MSD Result Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual Azinphos, methyl (Guthion) mg/kg ND 0.337 0.337 0.195 0.189 58.0 56.2 10.0-160 3.16 22 Bolstar mg/kg ND 0.337 0.337 0.216 0.210 64.3 62.5 10.0-151 2.84 20 Chlorpyrifos mg/kg ND 0.337 0.337 0.209 0.203 62.2 60.4 12.0-149 2.94 20 Coumaphos mg/kg ND 0.337 0.337 0.197 0.195 58.6 58.0 10.0-160 1.03 22 Total Demeton mg/kg ND 0.169 0.169 0.0942 0.0951 55.8 56.3 10.0-160 0.961 23 Diazinon mg/kg ND 0.337 0.337 0.170 0.172 50.5 51.1 11.0-157 1.18 20 Dichlorvos mg/kg ND 0.337 0.337 0.201 0.212 59.8 63.1 10.0-160 5.38 24 Dimethoate mg/kg ND 0.337 0.337 0.174 0.182 51.7 54.1 10.0-150 4.55 27 Disulfoton mg/kg ND 0.337 0.337 0.211 0.206 62.8 61.3 12.0-155 2.42 20 EPN (ENT) mg/kg ND 0.337 0.337 0.219 0.241 65.2 71.5 10.0-159 9.23 20 Ethoprop mg/kg ND 0.337 0.337 0.207 0.202 61.6 60.1 11.0-156 2.47 20 Parathion (Ethyl parathion) mg/kg ND 0.337 0.337 0.222 0.249 66.1 73.9 10.0-147 11.2 20 Fensulfothion mg/kg ND 0.337 0.337 0.171 0.179 50.8 53.2 10.0-157 4.62 27 Fenthion mg/kg ND 0.337 0.337 0.220 0.221 65.5 65.8 13.0-155 0.458 20 Malathion mg/kg ND 0.337 0.337 0.223 0.241 66.4 71.5 13.0-137 7.41 21 Merphos mg/kg ND 0.337 0.337 0.166 0.165 49.2 48.9 10.0-147 0.612 26 P9 Methyl parathion mg/kg ND 0.337 0.337 0.199 0.196 59.2 58.3 10.0-150 1.53 21 Mevinphos mg/kg ND 0.337 0.337 0.134 0.146 39.9 43.2 10.0-158 7.94 24 Naled mg/kg ND 0.337 0.337 0.108 0.0901 32.1 26.8 10.0-137 18.3 40 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3807279-3 R3807279-4 MS MSD L1506471-04 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Phorate mg/kg ND 0.337 0.337 0.202 0.201 60.1 59.8 13.0-154 0.501 20 Ronnel mg/kg ND 0.337 0.337 0.215 0.205 64.0 61.0 14.0-149 4.81 20 Stirophos mg/kg ND 0.337 0.337 0.197 0.194 58.6 57.7 10.0-150 1.55 20 (Tetrachlorvinphos) Sulfotepp mg/kg ND 0.337 0.337 0.229 0.255 68.2 75.7 10.0-160 10.4 20 (Thiodiphosphoric Ac TEPP mg/kg ND 3.37 3.37 U U 3.54 3.15 10.0-142 11.7 28 ML Tokuthion (Prothiofos) mg/kg ND 0.337 0.337 0.206 0.203 61.3 60.4 12.0-153 1.48 20 Trichloronate mg/kg ND 0.337 0.337 0.204 0.193 60.7 57.4 12.0-152 5.60 20 Triphenyl phosphate (S) % 65.8 71.8 36.0-121 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 QC Batch: 1887325 Analysis Method: EPA 8151 QC Batch Method: 8151A Analysis Description: Chlorinated Herb. (GC) 8151 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92610717001, 92610717004 METHOD BLANK: R3810203-1 Associated Lab Samples: 92610717001, 92610717004 Parameter Units Matrix: Blank Result Solid Reporting Limit MDL Analyzed Qualifiers 2,4-D mg/kg ND 0.0700 0.00702 07/01/22 09:55 Dalapon mg/kg ND 0.0700 0.0113 07/01/22 09:55 2,4-DB mg/kg ND 0.0700 0.0297 07/01/22 09:55 Dicamba mg/kg ND 0.0700 0.0157 07/01/22 09:55 Dichloroprop mg/kg ND 0.0700 0.0245 07/01/22 09:55 Dinoseb mg/kg ND 0.0700 0.00697 07/01/22 09:55 MCPA mg/kg ND 6.50 0.443 07/01/22 09:55 MCPP mg/kg ND 6.50 0.367 07/01/22 09:55 2,4,5-T mg/kg ND 0.0700 0.00852 07/01/22 09:55 2,4,5-TP (Silvex) mg/kg ND 0.0700 0.0107 07/01/22 09:55 2,4-DCAA (S) % 60.5 22.0-132 07/01/22 09:55 LABORATORY CONTROL SAMPLE: Parameter R3810203-2 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2,4-D mg/kg 0.167 0.129 77.2 40.0-120 Dalapon mg/kg 0.167 0.0891 53.4 15.0-120 2,4-DB mg/kg 0.167 0.107 64.1 25.0-143 Dicamba mg/kg 0.167 0.135 80.8 43.0-120 Dichloroprop mg/kg 0.167 0.146 87.4 32.0-129 Dinoseb mg/kg 0.167 0.0784 46.9 10.0-120 P9 MCPA mg/kg 16.7 13.3 79.6 31.0-121 MCPP mg/kg 16.7 10.9 65.3 28.0-133 P9 2,4,5-T mg/kg 0.167 0.152 91.0 41.0-120 P9 2,4,5-TP (Silvex) mg/kg 0.167 0.135 80.8 42.0-120 2,4-DCAA (S) % 61.7 22.0-132 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3810203-3 R3810203-4 MS MSD 92610717004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 2,4-D mg/kg ND 0.203 0.203 0.201 0.146 98.8 71.9 10.0-160 31.6 24 P9,R1 Dalapon mg/kg ND 0.203 0.203 0.167 0.123 82.0 60.5 10.0-121 30.3 27 R1 2,4-DB mg/kg ND 0.203 0.203 0.141 0.0969 69.5 47.7 10.0-160 37.2 22 P9,R1 Dicamba mg/kg ND 0.203 0.203 0.198 0.156 97.6 76.6 10.0-154 24.1 21 P9,R1 Dichloroprop mg/kg ND 0.203 0.203 0.201 0.147 98.8 72.5 10.0-158 30.8 20 P9,R1 Dinoseb mg/kg ND 0.203 0.203 0.0989 0.0640 48.7 31.5 10.0-120 42.9 40 P9,R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: Wright's Executive Sales 92610717 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3810203-3 R3810203-4 MS MSD 92610717004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual MCPA mg/kg ND 20.3 20.3 23.6 18.1 116 89.2 10.0-160 26.2 40 E,P9 MCPP mg/kg ND 20.3 20.3 16.1 11.8 79.0 58.3 10.0-160 30.3 40 P9 2,4,5-T mg/kg ND 0.203 0.203 0.213 0.151 105 74.3 10.0-157 34.1 20 E,P9, R1 2,4,5-TP (Silvex) mg/kg ND 0.203 0.203 0.183 0.128 89.8 62.9 10.0-156 35.3 20 P9,R1 2,4-DCAA (S) % 68.3 56.9 22.0-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 QC Batch: 1888224 Analysis Method: EPA 8151 QC Batch Method: 8151A Analysis Description: Chlorinated Herb. (GC) 8151 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92610717002, 92610717003, 92610717005, 92610717006, 92610717007, 92610717008 METHOD BLANK: R3810583-1 Matrix: Solid Associated Lab Samples: 92610717002, 92610717003, 92610717005, 92610717006, 92610717007, 92610717008 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 2,4-D mg/kg ND 0.0700 0.00702 07/02/22 23:21 Dalapon mg/kg ND 0.0700 0.0113 07/02/22 23:21 2,4-DB mg/kg ND 0.0700 0.0297 07/02/22 23:21 Dicamba mg/kg ND 0.0700 0.0157 07/02/22 23:21 Dichloroprop mg/kg ND 0.0700 0.0245 07/02/22 23:21 Dinoseb mg/kg ND 0.0700 0.00697 07/02/22 23:21 MCPA mg/kg ND 6.50 0.443 07/02/22 23:21 MCPP mg/kg ND 6.50 0.367 07/02/22 23:21 2,4,5-T mg/kg ND 0.0700 0.00852 07/02/22 23:21 2,4,5-TP (Silvex) mg/kg ND 0.0700 0.0107 07/02/22 23:21 2,4-DCAA (S) % 82.6 22.0-132 07/02/22 23:21 LABORATORY CONTROL SAMPLE: R3810583-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 2,4-D mg/kg 0.167 0.216 129 40.0-120 E,LO,P9 Dalapon mg/kg 0.167 0.125 74.9 15.0-120 2,4-DB mg/kg 0.167 0.188 113 25.0-143 E,P9 Dicamba mg/kg 0.167 0.225 135 43.0-120 E,LO,P9 Dichloroprop mg/kg 0.167 0.245 147 32.0-129 E,LO,P9 Dinoseb mg/kg 0.167 0.150 89.8 10.0-120 P9 MCPA mg/kg 16.7 25.0 150 31.0-121 E,LO,P9 MCPP mg/kg 16.7 17.7 106 28.0-133 E,P9 2,4,5-T mg/kg 0.167 0.233 140 41.0-120 E,LO,P9 2,4,5-TP (Silvex) mg/kg 0.167 0.241 144 42.0-120 E,LO,P9 2,4-DCAA (S) % 97.6 22.0-132 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3810583-3 R3810583-4 MS MSD L1509303-01 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 2,4-D mg/kg ND 0.171 0.173 0.153 0.171 89.7 98.8 10.0-160 10.9 24 Dalapon mg/kg ND 0.171 0.173 0.118 0.127 69.1 73.7 10.0-121 7.59 27 2,4-DB mg/kg ND 0.171 0.173 0.163 0.177 95.8 102 10.0-160 7.90 22 E Dicamba mg/kg ND 0.171 0.173 0.187 0.203 110 117 10.0-154 7.96 21 E,P9 Dichloroprop mg/kg ND 0.171 0.173 0.220 0.227 129 131 10.0-158 2.78 20 E,P9 Dinoseb mg/kg ND 0.171 0.173 0.108 0.117 63.0 67.7 10.0-120 8.29 40 P9 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: Wright's Executive Sales 92610717 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3810583-3 R3810583-4 MS MSD L1509303-01 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual MCPA mg/kg ND 17.1 17.3 22.1 23.9 130 138 10.0-160 7.64 40 E,P9 MCPP mg/kg ND 17.1 17.3 14.4 14.5 84.2 83.8 10.0-160 0.717 40 P9 2,4,5-T mg/kg ND 0.171 0.173 0.197 0.216 115 125 10.0-157 9.52 20 E,P9 2,4,5-TP (Silvex) mg/kg ND 0.171 0.173 0.160 0.175 93.9 101 10.0-156 8.64 20 E 2,4-DCAA (S) % 87.3 95.2 22.0-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 QC Batch: 743891 Analysis Method: EPA 6020B QC Batch Method: EPA 3050B Analysis Description: EPA 6020 Laboratory: Pace Analytical Gulf Coast Associated Lab Samples: 92610717001, 92610717002, 92610717003 METHOD BLANK: 2362684 Matrix: Solid Associated Lab Samples: 92610717001, 92610717002, 92610717003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Arsenic mg/kg ND 0.040 0.010 06/29/2219:52 P8 Barium mg/kg ND 0.040 0.010 06/29/2219:52 Cadmium mg/kg ND 0.040 0.010 06/29/2219:52 Chromium mg/kg ND 0.040 0.010 06/29/2219:52 Lead mg/kg ND 0.040 0.010 06/29/2219:52 Selenium mg/kg ND 0.040 0.010 06/29/2219:52 Silver mg/kg ND 0.040 0.010 06/29/2219:52 LABORATORY CONTROL SAMPLE & LCSD: Parameter 2362686 Units Spike Conc. 2362685 LCS LCSD Result Result LCS LCSD % Rec % Rec % Rec Limits RPD Max RPD Qualifiers Arsenic mg/kg 2 2.08 2.03 104 101 80-120 3 20 Barium mg/kg 2 2.00 2.21 100 110 80-120 10 20 Cadmium mg/kg 2 1.91 2.11 96 105 80-120 10 20 Chromium mg/kg 2 2.07 2.04 104 102 80-120 2 20 Lead mg/kg 2 2.07 2.30 104 115 80-120 10 20 Selenium mg/kg 0.4 0.41 0.41 102 102 80-120 0 20 Silver mg/kg 2 2.07 2.28 103 114 80-120 10 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 QC Batch: 743963 Analysis Method: EPA 7471 B QC Batch Method: METHOD Analysis Description: EPA 7471 B Laboratory: Pace Analytical Gulf Coast Associated Lab Samples: 92610717001, 92610717002, 92610717003 METHOD BLANK: 2363133 Matrix: Solid Associated Lab Samples: 92610717001, 92610717002, 92610717003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Mercury mg/kg ND 0.010 0.0040 06/27/2212:21 LABORATORY CONTROL SAMPLE & LCSD: 2363135 2363134 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Mercury mg/kg 0.25 0.24 0.27 97 108 80-120 10 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 QC Batch: 706065 Analysis Method: EPA 8260D QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92610717001, 92610717002, 92610717003 METHOD BLANK: 3683772 Matrix: Associated Lab Samples: 92610717001, 92610717002, 92610717003 Blank Parameter Units Result Solid Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 0.0019 06/22/22 00:21 1,1,1-Trichloroethane mg/kg ND 0.0050 0.0026 06/22/22 00:21 1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 0.0013 06/22/22 00:21 1,1,2-Trichloroethane mg/kg ND 0.0050 0.0017 06/22/22 00:21 1,1-Dichloroethane mg/kg ND 0.0050 0.0021 06/22/22 00:21 1,1-Dichloroethene mg/kg ND 0.0050 0.0021 06/22/22 00:21 1,1-Dichloropropene mg/kg ND 0.0050 0.0024 06/22/22 00:21 1,2,3-Trichlorobenzene mg/kg ND 0.0050 0.0040 06/22/22 00:21 1,2,3-Trichloropropane mg/kg ND 0.0050 0.0025 06/22/22 00:21 1,2,4-Trichlorobenzene mg/kg ND 0.0050 0.0042 06/22/22 00:21 1,2,4-Trimethylbenzene mg/kg ND 0.0050 0.0014 06/22/22 00:21 1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 0.0019 06/22/22 00:21 1,2-Dibromoethane (EDB) mg/kg ND 0.0050 0.0022 06/22/22 00:21 1,2-Dichlorobenzene mg/kg ND 0.0050 0.0018 06/22/22 00:21 1,2-Dichloroethane mg/kg ND 0.0050 0.0033 06/22/22 00:21 1,2-Dichloropropane mg/kg ND 0.0050 0.0015 06/22/22 00:21 1,3,5-Trimethylbenzene mg/kg ND 0.0050 0.0017 06/22/22 00:21 1,3-Dichlorobenzene mg/kg ND 0.0050 0.0016 06/22/22 00:21 1,3-Dichloropropane mg/kg ND 0.0050 0.0016 06/22/22 00:21 1,4-Dichlorobenzene mg/kg ND 0.0050 0.0013 06/22/22 00:21 2,2-Dichloropropane mg/kg ND 0.0050 0.0016 06/22/22 00:21 2-Butanone (MEK) mg/kg ND 0.10 0.024 06/22/22 00:21 2-Chlorotoluene mg/kg ND 0.0050 0.0018 06/22/22 00:21 2-Hexanone mg/kg ND 0.050 0.0048 06/22/22 00:21 4-Chlorotoluene mg/kg ND 0.0050 0.00088 06/22/22 00:21 4-Methyl-2-pentanone (MIBK) mg/kg ND 0.050 0.0048 06/22/22 00:21 Acetone mg/kg ND 0.10 0.032 06/22/22 00:21 Benzene mg/kg ND 0.0050 0.0020 06/22/22 00:21 Bromobenzene mg/kg ND 0.0050 0.0016 06/22/22 00:21 Bromochloromethane mg/kg ND 0.0050 0.0015 06/22/22 00:21 Bromodichloromethane mg/kg ND 0.0050 0.0019 06/22/22 00:21 Bromoform mg/kg ND 0.0050 0.0018 06/22/22 00:21 Bromomethane mg/kg ND 0.010 0.0079 06/22/22 00:21 Carbon tetrachloride mg/kg ND 0.0050 0.0019 06/22/22 00:21 Chlorobenzene mg/kg ND 0.0050 0.00096 06/22/22 00:21 Chloroethane mg/kg ND 0.010 0.0039 06/22/22 00:21 Chloroform mg/kg ND 0.0050 0.0030 06/22/22 00:21 Chloromethane mg/kg ND 0.010 0.0042 06/22/22 00:21 cis-1,2-Dichloroethene mg/kg ND 0.0050 0.0017 06/22/22 00:21 cis-1,3-Dichloropropene mg/kg ND 0.0050 0.0014 06/22/22 00:21 v2 v2 IK Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 METHOD BLANK: 3683772 Matrix: Associated Lab Samples: 92610717001, 92610717002, 92610717003 Blank Parameter Units Result Solid Reporting Limit MDL Analyzed Dibromochloromethane mg/kg ND 0.0050 0.0028 06/22/22 00:21 Dibromomethane mg/kg ND 0.0050 0.0011 06/22/22 00:21 Dichlorodifluoromethane mg/kg ND 0.010 0.0022 06/22/22 00:21 Diisopropyl ether mg/kg ND 0.0050 0.0014 06/22/22 00:21 Ethylbenzene mg/kg ND 0.0050 0.0023 06/22/22 00:21 Hexachloro-1,3-butadiene mg/kg ND 0.010 0.0082 06/22/22 00:21 Isopropylbenzene (Cumene) mg/kg ND 0.0050 0.0017 06/22/22 00:21 m&p-Xylene mg/kg ND 0.010 0.0034 06/22/22 00:21 Methyl-tert-butyl ether mg/kg ND 0.0050 0.0019 06/22/22 00:21 Methylene Chloride mg/kg ND 0.020 0.014 06/22/22 00:21 n-Butylbenzene mg/kg ND 0.0050 0.0024 06/22/22 00:21 n-Propylbenzene mg/kg ND 0.0050 0.0018 06/22/22 00:21 Naphthalene mg/kg ND 0.0050 0.0026 06/22/22 00:21 o-Xylene mg/kg ND 0.0050 0.0022 06/22/22 00:21 p-Isopropyltoluene mg/kg ND 0.0050 0.0025 06/22/22 00:21 sec-Butylbenzene mg/kg ND 0.0050 0.0022 06/22/22 00:21 Styrene mg/kg ND 0.0050 0.0013 06/22/22 00:21 tert-Butyl benzene mg/kg ND 0.0050 0.0018 06/22/22 00:21 Tetrachloroethene mg/kg ND 0.0050 0.0016 06/22/22 00:21 Toluene mg/kg ND 0.0050 0.0014 06/22/22 00:21 trans-1,2-Dichloroethene mg/kg ND 0.0050 0.0018 06/22/22 00:21 trans- 1,3-Dichloropropene mg/kg ND 0.0050 0.0017 06/22/22 00:21 Trichloroethene mg/kg ND 0.0050 0.0013 06/22/22 00:21 Trichlorofluoromethane mg/kg ND 0.0050 0.0028 06/22/22 00:21 Vinyl acetate mg/kg ND 0.050 0.0036 06/22/22 00:21 Vinyl chloride mg/kg ND 0.010 0.0025 06/22/22 00:21 Xylene (Total) mg/kg ND 0.010 0.0028 06/22/22 00:21 1,2-Dichloroethane-d4 (S) % 94 70-130 06/22/22 00:21 4-Bromofluorobenzene (S) % 97 69-134 06/22/22 00:21 Toluene-d8 (S) % 96 70-130 06/22/22 00:21 KI IK Qualifiers LABORATORY CONTROL SAMPLE: 3683773 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane mg/kg 1.2 1.3 107 70-130 1,1,1-Trichloroethane mg/kg 1.2 1.3 101 70-130 1,1,2,2-Tetrachloroethane mg/kg 1.2 1.2 95 70-130 1,1,2-Trichloroethane mg/kg 1.2 1.3 102 70-130 1,1-Dichloroethane mg/kg 1.2 1.2 95 70-130 1,1-Dichloroethene mg/kg 1.2 1.3 101 70-130 1,1-Dichloropropene mg/kg 1.2 1.3 101 70-130 1,2,3-Trichlorobenzene mg/kg 1.2 1.2 98 65-130 1,2,3-Trichloropropane mg/kg 1.2 1.1 90 70-130 1,2,4-Trichlorobenzene mg/kg 1.2 1.3 104 68-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 LABORATORY CONTROL SAMPLE: Parameter 3683773 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,2,4-Trimethylbenzene mg/kg 1.2 1.3 102 70-130 1,2-Dibromo-3-chloropropane mg/kg 1.2 1.3 105 70-130 1,2-Dibromoethane (EDB) mg/kg 1.2 1.3 101 70-130 1,2-Dichlorobenzene mg/kg 1.2 1.3 101 70-130 1,2-Dichloroethane mg/kg 1.2 1.1 90 63-130 1,2-Dichloropropane mg/kg 1.2 1.2 100 70-130 1,3,5-Trimethylbenzene mg/kg 1.2 1.3 105 70-130 1,3-Dichlorobenzene mg/kg 1.2 1.3 102 70-130 1,3-Dichloropropane mg/kg 1.2 1.2 94 70-130 1,4-Dichlorobenzene mg/kg 1.2 1.2 100 70-130 2,2-Dichloropropane mg/kg 1.2 1.2 98 66-130 2-Butanone (MEK) mg/kg 2.5 2.1 83 70-130 v3 2-Chlorotoluene mg/kg 1.2 1.2 99 70-130 2-Hexanone mg/kg 2.5 2.3 92 70-130 4-Chlorotoluene mg/kg 1.2 1.2 99 70-130 4-Methyl-2-pentanone (MIBK) mg/kg 2.5 2.4 94 70-130 Acetone mg/kg 2.5 2.0 81 69-130 v3 Benzene mg/kg 1.2 1.2 98 70-130 Bromobenzene mg/kg 1.2 1.3 104 70-130 Bromochloromethane mg/kg 1.2 1.3 104 70-130 Bromodichloromethane mg/kg 1.2 1.2 99 69-130 Bromoform mg/kg 1.2 1.4 111 70-130 Bromomethane mg/kg 1.2 1.2 95 52-130IK Carbon tetrachloride mg/kg 1.2 1.4 109 70-130 Chlorobenzene mg/kg 1.2 1.3 102 70-130 Chloroethane mg/kg 1.2 1.5 117 65-130 Chloroform mg/kg 1.2 1.1 91 70-130 Chloromethane mg/kg 1.2 1.4 112 55-130 cis-1,2-Dichloroethene mg/kg 1.2 1.2 95 70-130 cis-1,3-Dichloropropene mg/kg 1.2 1.3 103 70-130 Dibromochloromethane mg/kg 1.2 1.3 105 70-130 Dibromomethane mg/kg 1.2 1.4 109 70-130 Dichlorodifluoromethane mg/kg 1.2 1.8 141 45-156 Diisopropyl ether mg/kg 1.2 1.2 92 70-130 Ethylbenzene mg/kg 1.2 1.1 91 70-130 Hexachloro-1,3-butadiene mg/kg 1.2 1.3 103 66-130 Isopropylbenzene (Cumene) mg/kg 1.2 1.3 102 70-130 m&p-Xylene mg/kg 2.5 2.4 94 70-130 Methyl-tert-butyl ether mg/kg 1.2 1.2 96 70-130 Methylene Chloride mg/kg 1.2 1.0 83 65-130 n-Butylbenzene mg/kg 1.2 1.2 99 67-130 n-Propylbenzene mg/kg 1.2 1.2 98 70-130 Naphthalene mg/kg 1.2 1.3 101 70-130 o-Xylene mg/kg 1.2 1.3 101 70-130 p-Isopropyltoluene mg/kg 1.2 1.3 107 67-130 sec-Butylbenzene mg/kg 1.2 1.3 102 69-130 Styrene mg/kg 1.2 1.2 97 70-130IK Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 LABORATORY CONTROL SAMPLE: Parameter 3683773 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers tert-Butyl benzene mg/kg 1.2 1.3 105 67-130 Tetrachloroethene mg/kg 1.2 1.4 111 70-130 Toluene mg/kg 1.2 1.2 94 70-1301K trans-1,2-Dichloroethene mg/kg 1.2 1.2 99 70-130 trans- 1,3-Dichloropropene mg/kg 1.2 1.3 102 68-130 Trichloroethene mg/kg 1.2 1.4 109 70-130 Trichlorofluoromethane mg/kg 1.2 1.4 113 70-130 Vinyl acetate mg/kg 2.5 2.4 98 70-130 Vinyl chloride mg/kg 1.2 1.5 121 61-130 Xylene (Total) mg/kg 3.8 3.6 97 70-130 1,2-Dichloroethane-d4 (S) % 79 70-130 4-Bromofluorobenzene (S) % 96 69-134 Toluene-d8 (S) % 99 70-130 MATRIX SPIKE SAMPLE: Parameter 3683774 Units 92610193021 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane mg/kg ND 0.73 0.69 96 70-131 1,1,1-Trichloroethane mg/kg ND 0.73 0.64 89 65-133 1,1,2,2-Tetrachloroethane mg/kg ND 0.73 0.59 82 66-130 1,1,2-Trichloroethane mg/kg ND 0.73 0.63 87 66-133 1,1-Dichloroethane mg/kg ND 0.73 0.51 71 65-130 1,1-Dichloroethene mg/kg ND 0.73 0.54 74 10-158 1,1-Dichloropropene mg/kg ND 0.73 0.60 83 68-133 1,2,3-Trichlorobenzene mg/kg ND 0.73 0.16 21 27-138 M1 1,2,3-Trichloropropane mg/kg ND 0.73 0.55 75 67-130 1,2,4-Trichlorobenzene mg/kg ND 0.73 0.33 46 51-134 M1 1,2,4-Trimethylbenzene mg/kg ND 0.73 0.58 81 63-136 1,2-Dibromo-3-chloropropane mg/kg ND 0.73 0.31 43 32-130 1,2-Dibromoethane (EDB) mg/kg ND 0.73 0.64 89 70-130 1,2-Dichlorobenzene mg/kg ND 0.73 0.63 87 69-130 1,2-Dichloroethane mg/kg ND 0.73 0.57 79 59-130 1,2-Dichloropropane mg/kg ND 0.73 0.63 87 70-130 1,3,5-Trimethylbenzene mg/kg ND 0.73 0.60 83 65-137 1,3-Dichlorobenzene mg/kg ND 0.73 0.60 83 70-130 1,3-Dichloropropane mg/kg ND 0.73 0.59 82 70-130 1,4-Dichlorobenzene mg/kg ND 0.73 0.57 78 68-130 2,2-Dichloropropane mg/kg ND 0.73 0.56 78 32-130 2-Butanone (MEK) mg/kg 54.OJ ug/kg 1.5 0.88 57 10-136 v3 2-Chlorotoluene mg/kg ND 0.73 0.58 81 69-141 2-Hexanone mg/kg ND 1.5 0.93 65 10-144 4-Chlorotoluene mg/kg ND 0.73 0.56 78 70-132 4-Methyl-2-pentanone (MIBK) mg/kg ND 1.5 1.1 74 25-143 Acetone mg/kg ND 1.5 0.67 46 10-130 v3 Benzene mg/kg ND 0.73 0.63 88 67-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 MATRIX SPIKE SAMPLE: 3683774 92610193021 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Bromobenzene mg/kg ND 0.73 0.64 89 70-130 Bromochloromethane mg/kg ND 0.73 0.64 88 69-134 Bromodichloromethane mg/kg ND 0.73 0.60 83 64-130 Bromoform mg/kg ND 0.73 0.67 93 62-130 Bromomethane mg/kg ND 0.73 0.21 29 20-1761K Carbon tetrachloride mg/kg ND 0.73 0.66 91 65-140 Chlorobenzene mg/kg ND 0.73 0.65 90 70-130 Chloroethane mg/kg ND 0.73 0.025 3 10-130 M1 Chloroform mg/kg ND 0.73 0.56 78 63-130 Chloromethane mg/kg ND 0.73 0.80 110 58-130 cis-1,2-Dichloroethene mg/kg ND 0.73 0.58 81 66-130 cis-1,3-Dichloropropene mg/kg ND 0.73 0.62 86 67-130 Dibromochloromethane mg/kg ND 0.73 0.63 87 67-130 Dibromomethane mg/kg ND 0.73 0.68 94 63-131 Dichlorodifluoromethane mg/kg ND 0.73 0.87 120 44-180 Diisopropyl ether mg/kg ND 0.73 0.56 77 63-130 Ethylbenzene mg/kg ND 0.73 0.57 79 66-130 Hexachloro-1,3-butadiene mg/kg ND 0.73 0.53 74 64-150 Isopropylbenzene (Cumene) mg/kg ND 0.73 0.63 87 69-135 m&p-Xylene mg/kg ND 1.5 1.1 79 60-133 Methyl-tert-butyl ether mg/kg ND 0.73 0.58 81 65-130 Methylene Chloride mg/kg ND 0.73 0.44 61 61-130 n-Butylbenzene mg/kg ND 0.73 0.51 70 65-140 n-Propylbenzene mg/kg ND 0.73 0.56 77 67-140 Naphthalene mg/kg ND 0.73 0.13 18 15-145 o-Xylene mg/kg ND 0.73 0.64 88 66-133 p-Isopropyltoluene mg/kg ND 0.73 0.60 83 56-147 sec-Butylbenzene mg/kg ND 0.73 0.60 83 65-139 Styrene mg/kg ND 0.73 0.58 80 70-132 IK tert-Butyl benzene mg/kg ND 0.73 0.64 89 62-135 Tetrachloroethene mg/kg ND 0.73 0.61 85 70-135 Toluene mg/kg ND 0.73 0.57 78 67-1301K trans-1,2-Dichloroethene mg/kg ND 0.73 0.56 77 69-130 trans- 1,3-Dichloropropene mg/kg ND 0.73 0.59 82 62-130 Trichloroethene mg/kg ND 0.73 0.68 94 70-135 Trichlorofluoromethane mg/kg ND 0.73 0.13 18 10-130 Vinyl acetate mg/kg ND 1.5 1.1 75 53-130 Vinyl chloride mg/kg ND 0.73 0.71 98 61-148 Xylene (Total) mg/kg ND 2.2 1.8 82 63-132 1,2-Dichloroethane-d4 (S) % 85 70-130 4-Bromofluorobenzene (S) % 97 69-134 Toluene-d8 (S) % 98 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 72 Pace Analytical Services, LLC lac, Analyilcal ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 SAMPLE DUPLICATE: 3683775 Parameter Units 92610193022 Result Dup Result RPD Max RPD Qualifiers 1,1,1,2-Tetrachloroethane mg/kg ND ND 30 1,1,1-Trichloroethane mg/kg ND ND 30 1,1,2,2-Tetrachloroethane mg/kg ND ND 30 1,1,2-Trichloroethane mg/kg ND ND 30 1,1-Dichloroethane mg/kg ND ND 30 1,1-Dichloroethene mg/kg ND ND 30 1,1-Dichloropropene mg/kg ND ND 30 1,2,3-Trichlorobenzene mg/kg ND ND 30 1,2,3-Trichloropropane mg/kg ND ND 30 1,2,4-Trichlorobenzene mg/kg ND ND 30 1,2,4-Trimethylbenzene mg/kg ND ND 30 1,2-Dibromo-3-chloropropane mg/kg ND ND 30 1,2-Dibromoethane (EDB) mg/kg ND ND 30 1,2-Dichlorobenzene mg/kg ND ND 30 1,2-Dichloroethane mg/kg ND ND 30 1,2-Dichloropropane mg/kg ND ND 30 1,3,5-Trimethylbenzene mg/kg ND ND 30 1,3-Dichlorobenzene mg/kg ND ND 30 1,3-Dichloropropane mg/kg ND ND 30 1,4-Dichlorobenzene mg/kg ND ND 30 2,2-Dichloropropane mg/kg ND ND 30 2-Butanone (MEK) mg/kg 67.3J ug/kg ND 30 v2 2-Chlorotoluene mg/kg ND ND 30 2-Hexanone mg/kg ND ND 30 4-Chlorotoluene mg/kg ND ND 30 4-Methyl-2-pentanone (MIBK) mg/kg ND ND 30 Acetone mg/kg ND ND 30 v2 Benzene mg/kg ND ND 30 Bromobenzene mg/kg ND ND 30 Bromochloromethane mg/kg ND ND 30 Bromodichloromethane mg/kg ND ND 30 Bromoform mg/kg ND ND 30 Bromomethane mg/kg ND ND 301K Carbon tetrachloride mg/kg ND ND 30 Chlorobenzene mg/kg ND ND 30 Chloroethane mg/kg ND ND 30 Chloroform mg/kg ND ND 30 Chloromethane mg/kg ND ND 30 cis-1,2-Dichloroethene mg/kg ND ND 30 cis-1,3-Dichloropropene mg/kg ND ND 30 Dibromochloromethane mg/kg ND ND 30 Dibromomethane mg/kg ND ND 30 Dichlorodifluoromethane mg/kg ND ND 30 Diisopropyl ether mg/kg ND ND 30 Ethylbenzene mg/kg ND ND 30 Hexachloro-1,3-butadiene mg/kg ND ND 30 Isopropylbenzene (Cumene) mg/kg ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 SAMPLE DUPLICATE: 3683775 Parameter Units 92610193022 Result Dup Result m&p-Xylene mg/kg ND ND Methyl-tert-butyl ether mg/kg ND ND Methylene Chloride mg/kg ND ND n-Butylbenzene mg/kg ND ND n-Propylbenzene mg/kg ND ND Naphthalene mg/kg ND ND o-Xylene mg/kg ND ND p-Isopropyltoluene mg/kg ND ND sec-Butylbenzene mg/kg ND ND Styrene mg/kg ND ND tert-Butyl benzene mg/kg ND ND Tetrachloroethene mg/kg ND ND Toluene mg/kg ND ND trans-1,2-Dichloroethene mg/kg ND ND trans- 1,3-Dichloropropene mg/kg ND ND Trichloroethene mg/kg ND ND Trichlorofluoromethane mg/kg ND ND Vinyl acetate mg/kg ND ND Vinyl chloride mg/kg ND ND Xylene (Total) mg/kg ND ND 1,2-Dichloroethane-d4 (S) % 88 86 4-Bromofluorobenzene (S) % 97 97 Toluene-d8 (S) % 99 98 Max RPD RPD Qualifiers 30 30 30 30 30 30 30 30 30 30 I K 30 30 30 I K 30 30 30 30 30 30 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 49 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 QC Batch: 706233 Analysis Method: EPA 8081 B QC Batch Method: EPA 3546 Analysis Description: 8081 GCS Pesticides Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92610717001, 92610717002, 92610717003, 92610717004, 92610717005, 92610717006, 92610717007, 92610717008 METHOD BLANK: 3684385 Matrix: Solid Associated Lab Samples: 92610717001, 92610717002, 92610717003, 92610717004, 92610717005, 92610717006, 92610717007, 92610717008 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 4,4'-DDD mg/kg ND 0.0020 0.00092 06/27/22 14:18 4,4'-DDE mg/kg ND 0.0020 0.00096 06/27/22 14:18 4,4'-DDT mg/kg ND 0.0020 0.00090 06/27/22 14:18 Aldrin mg/kg ND 0.0020 0.00082 06/27/22 14:18 alpha-BHC mg/kg ND 0.0020 0.00088 06/27/22 14:18 beta-BHC mg/kg ND 0.0020 0.00098 06/27/22 14:18 Chlordane (Technical) mg/kg ND 0.010 0.0088 06/27/22 14:18 delta-BHC mg/kg ND 0.0020 0.0010 06/27/22 14:18 Dieldrin mg/kg ND 0.0020 0.00088 06/27/22 14:18 Endosulfan I mg/kg ND 0.0020 0.00087 06/27/22 14:18 Endosulfan 11 mg/kg ND 0.0020 0.00092 06/27/22 14:18 Endosulfan sulfate mg/kg ND 0.0020 0.0011 06/27/22 14:18 Endrin mg/kg ND 0.0020 0.00094 06/27/22 14:18 Endrin aldehyde mg/kg ND 0.0020 0.0014 06/27/22 14:18 Endrin ketone mg/kg ND 0.0020 0.0011 06/27/22 14:18 gamma-BHC (Lindane) mg/kg ND 0.0020 0.00081 06/27/22 14:18 Heptachlor mg/kg ND 0.0020 0.00094 06/27/22 14:18 Heptachlor epoxide mg/kg ND 0.0020 0.00080 06/27/22 14:18 Hexachlorobenzene mg/kg ND 0.0020 0.00084 06/27/22 14:18 Methoxychlor mg/kg ND 0.0051 0.0025 06/27/22 14:18 Mirex mg/kg ND 0.0051 0.0022 06/27/22 14:18 Toxaphene mg/kg ND 0.0071 0.0054 06/27/22 14:18 Decachlorobiphenyl (S) % 96 10-146 06/27/22 14:18 Tetrachloro-m-xylene (S) % 71 10-133 06/27/22 14:18 LABORATORY CONTROL SAMPLE: 3684386 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 4,4'-DDD mg/kg 0.0083 0.011 131 40-160 4,4'-DDE mg/kg 0.0083 0.0096 116 41-154 4,4'-DDT mg/kg 0.0083 0.0074 90 34-163 Aldrin mg/kg 0.0083 0.0071 85 39-144 alpha-BHC mg/kg 0.0083 0.0076 91 36-145 beta-BHC mg/kg 0.0083 0.0072 86 39-152 delta-BHC mg/kg 0.0083 0.0076 91 41-147 Dieldrin mg/kg 0.0083 0.0094 113 42-153 Endosulfan I mg/kg 0.0083 0.0071 85 39-148 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 50 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 LABORATORY CONTROL SAMPLE: Parameter 3684386 Units Spike Conc. LCS LCS Result % Rec Endosulfan II mg/kg 0.0083 0.0070 Endosulfan sulfate mg/kg 0.0083 0.0072 Endrin mg/kg 0.0083 0.0096 Endrin aldehyde mg/kg 0.0083 0.0063 Endrin ketone mg/kg 0.0083 0.0066 gamma-BHC (Lindane) mg/kg 0.0083 0.0076 Heptachlor mg/kg 0.0083 0.0073 Heptachlor epoxide mg/kg 0.0083 0.0071 Hexachlorobenzene mg/kg 0.0083 0.0075 Methoxychlor mg/kg 0.025 0.017 Mirex mg/kg 0.025 0.020 Decachlorobiphenyl (S) % Tetrachloro-m-xylene (S) % % Rec Limits 84 40-147 87 40-148 116 42-158 76 39-130 80 39-159 92 38-146 88 39-144 86 40-143 90 33-139 67 32-146 80 39-141 85 10-146 84 10-133 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3684387 MS 92610560001 Spike Parameter Units Result Conc. MSD Spike Conc. 3684388 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 4,4'-DDD mg/kg ND 0.0084 0.0083 0.0077 0.0089 92 107 10-160 15 30 4,4'-DDE mg/kg ND 0.0084 0.0083 0.0078 0.0086 93 104 10-170 11 30 4,4'-DDT mg/kg ND 0.0084 0.0083 0.0080 0.0088 96 106 10-194 10 30 Aldrin mg/kg ND 0.0084 0.0083 0.0055 0.0065 66 78 10-143 15 30 alpha-BHC mg/kg ND 0.0084 0.0083 0.0058 0.0068 70 82 10-144 15 30 beta-BHC mg/kg ND 0.0084 0.0083 0.012 0.0068 140 82 10-152 52 30 R1 delta-BHC mg/kg ND 0.0084 0.0083 0.0061 0.0066 73 80 10-147 8 30 Dieldrin mg/kg ND 0.0084 0.0083 0.0075 0.0084 90 101 10-181 11 30 Endosulfan I mg/kg ND 0.0084 0.0083 0.0055 0.0062 65 75 10-147 12 30 Endosulfan II mg/kg ND 0.0084 0.0083 0.0056 0.0062 67 74 11-149 10 30 Endosulfan sulfate mg/kg ND 0.0084 0.0083 0.0057 0.0063 68 76 10-153 10 30 Endrin mg/kg ND 0.0084 0.0083 0.0079 0.0086 94 103 10-160 8 30 Endrin aldehyde mg/kg ND 0.0084 0.0083 0.0048 0.0054 57 65 10-134 13 30 Endrin ketone mg/kg ND 0.0084 0.0083 0.0054 0.0060 65 72 11-155 10 30 gamma-BHC (Lindane) mg/kg ND 0.0084 0.0083 0.0060 0.0067 71 81 10-152 12 30 Heptachlor mg/kg ND 0.0084 0.0083 0.0058 0.0066 70 79 10-149 12 30 Heptachlor epoxide mg/kg ND 0.0084 0.0083 0.0056 0.0063 67 76 10-142 12 30 Hexachlorobenzene mg/kg ND 0.0084 0.0083 0.0056 0.0065 66 79 10-140 16 30 Methoxychlor mg/kg ND 0.025 0.025 0.031 0.030 124 120 10-147 4 30 Mirex mg/kg ND 0.025 0.025 0.016 0.017 63 69 11-139 8 30 Decachlorobiphenyl (S) % 66 75 10-146 Tetrachloro-m-xylene (S) % 60 77 10-133 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 51 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 QC Batch: 706520 Analysis Method: EPA 8270E QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92610717001, 92610717002 METHOD BLANK: 3685849 Associated Lab Samples: 92610717001, 92610717002 Parameter Units Matrix: Blank Result Solid Reporting Limit MDL Analyzed 1,2,4-Trichlorobenzene mg/kg ND 0.33 0.13 06/26/22 13:14 1,2-Dichlorobenzene mg/kg ND 0.33 0.12 06/26/22 13:14 1,3-Dichlorobenzene mg/kg ND 0.33 0.12 06/26/22 13:14 1,4-Dichlorobenzene mg/kg ND 0.33 0.13 06/26/22 13:14 1-Methylnaphthalene mg/kg ND 0.33 0.12 06/26/22 13:14 2,2'-Oxybis(1-chloropropane) mg/kg ND 0.33 0.16 06/26/22 13:14 2,4,5-Trichlorophenol mg/kg ND 0.33 0.15 06/26/22 13:14 2,4,6-Trichlorophenol mg/kg ND 0.33 0.14 06/26/22 13:14 2,4-Dichlorophenol mg/kg ND 0.33 0.13 06/26/22 13:14 2,4-Dimethylphenol mg/kg ND 0.33 0.14 06/26/22 13:14 2,4-Dinitrophenol mg/kg ND 1.7 1.0 06/26/22 13:14 2,4-Dinitrotoluene mg/kg ND 0.33 0.13 06/26/22 13:14 2,6-Dinitrotoluene mg/kg ND 0.33 0.12 06/26/22 13:14 2-Chloronaphthalene mg/kg ND 0.33 0.13 06/26/22 13:14 2-Chlorophenol mg/kg ND 0.33 0.13 06/26/22 13:14 2-Methylnaphthalene mg/kg ND 0.33 0.13 06/26/22 13:14 2-Methylphenol(o-Cresol) mg/kg ND 0.33 0.14 06/26/22 13:14 2-Nitroaniline mg/kg ND 1.7 0.27 06/26/22 13:14 2-Nitrophenol mg/kg ND 0.33 0.14 06/26/22 13:14 3&4-Methyl phenol (m&p Cresol) mg/kg ND 0.33 0.13 06/26/22 13:14 3,3'-Dichlorobenzidine mg/kg ND 0.67 0.23 06/26/22 13:14 3-Nitroaniline mg/kg ND 1.7 0.26 06/26/22 13:14 4,6-Dinitro-2-methyl phenol mg/kg ND 0.67 0.31 06/26/22 13:14 4-Bromophenylphenyl ether mg/kg ND 0.33 0.13 06/26/22 13:14 4-ChIoro-3-methyl phenol mg/kg ND 0.67 0.23 06/26/22 13:14 4-Chloroaniline mg/kg ND 0.67 0.26 06/26/22 13:14 4-Chlorophenylphenyl ether mg/kg ND 0.33 0.12 06/26/22 13:14 4-Nitroaniline mg/kg ND 0.67 0.25 06/26/22 13:14 4-Nitrophenol mg/kg ND 1.7 0.64 06/26/22 13:14 Acenaphthene mg/kg ND 0.33 0.12 06/26/22 13:14 Acenaphthylene mg/kg ND 0.33 0.12 06/26/22 13:14 Aniline mg/kg ND 0.33 0.13 06/26/22 13:14 Anthracene mg/kg ND 0.33 0.11 06/26/22 13:14 Benzo(a)anthracene mg/kg ND 0.33 0.11 06/26/22 13:14 Benzo(a)pyrene mg/kg ND 0.33 0.12 06/26/22 13:14 Benzo(b)fluoranthene mg/kg ND 0.33 0.11 06/26/22 13:14 Benzo(g,h,i)perylene mg/kg ND 0.33 0.13 06/26/22 13:14 Benzo(k)fluoranthene mg/kg ND 0.33 0.12 06/26/22 13:14 Benzoic Acid mg/kg ND 1.7 0.72 06/26/22 13:14 Benzyl alcohol mg/kg ND 0.67 0.25 06/26/22 13:14 IL Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 52 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 METHOD BLANK: 3685849 Associated Lab Samples: 92610717001, 92610717002 Parameter Units Matrix: Blank Result Solid Reporting Limit MDL Analyzed bis(2-Chloroethoxy)methane mg/kg ND 0.33 0.14 06/26/22 13:14 bis(2-Chloroethyl) ether mg/kg ND 0.33 0.13 06/26/22 13:14 bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 0.13 06/26/22 13:14 Butylbenzylphthalate mg/kg ND 0.33 0.14 06/26/22 13:14 Chrysene mg/kg ND 0.33 0.12 06/26/22 13:14 Di-n-butylphthalate mg/kg ND 0.33 0.11 06/26/22 13:14 Di-n-octylphthalate mg/kg ND 0.33 0.13 06/26/22 13:14 Dibenz(a,h)anthracene mg/kg ND 0.33 0.13 06/26/22 13:14 Dibenzofuran mg/kg ND 0.33 0.12 06/26/22 13:14 Diethylphthalate mg/kg ND 0.33 0.12 06/26/22 13:14 Dimethylphthalate mg/kg ND 0.33 0.12 06/26/22 13:14 Fluoranthene mg/kg ND 0.33 0.11 06/26/22 13:14 Fluorene mg/kg ND 0.33 0.12 06/26/22 13:14 Hexachloro-1,3-butadiene mg/kg ND 0.33 0.14 06/26/22 13:14 Hexachlorobenzene mg/kg ND 0.33 0.13 06/26/22 13:14 Hexachlorocyclopentadiene mg/kg ND 0.33 0.19 06/26/22 13:14 Hexachloroethane mg/kg ND 0.33 0.13 06/26/22 13:14 Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 0.13 06/26/22 13:14 Isophorone mg/kg ND 0.33 0.15 06/26/22 13:14 N-Nitroso-di-n-propylamine mg/kg ND 0.33 0.13 06/26/22 13:14 N-Nitrosodimethylamine mg/kg ND 0.33 0.11 06/26/22 13:14 N-Nitrosodiphenylamine mg/kg ND 0.33 0.12 06/26/22 13:14 Naphthalene mg/kg ND 0.33 0.11 06/26/22 13:14 Nitrobenzene mg/kg ND 0.33 0.15 06/26/22 13:14 Pentachlorophenol mg/kg ND 0.67 0.33 06/26/22 13:14 Phenanthrene mg/kg ND 0.33 0.11 06/26/22 13:14 Phenol mg/kg ND 0.33 0.15 06/26/22 13:14 Pyrene mg/kg ND 0.33 0.14 06/26/22 13:14 Pyridine mg/kg ND 0.33 0.11 06/26/22 13:14 2,4,6-Tribromophenol (S) % 69 18-130 06/26/22 13:14 2-Fluorobiphenyl (S) % 74 19-130 06/26/22 13:14 2-Fluorophenol (S) % 66 18-130 06/26/22 13:14 Nitrobenzene-d5 (S) % 72 21-130 06/26/22 13:14 Phenol-d6 (S) % 74 18-130 06/26/22 13:14 Terphenyl-d14 (S) % 75 15-130 06/26/22 13:14 v2 Qualifiers LABORATORY CONTROL SAMPLE: 3685850 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,2,4-Trichlorobenzene mg/kg 1.7 1.2 75 47-130 1,2-Dichlorobenzene mg/kg 1.7 1.2 75 49-130 1,3-Dichlorobenzene mg/kg 1.7 1.2 72 48-130 1,4-Dichlorobenzene mg/kg 1.7 1.2 74 49-130 1-Methylnaphthalene mg/kg 1.7 1.4 83 54-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 53 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 LABORATORY CONTROL SAMPLE: Parameter 3685850 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2,2'-Oxybis(1-chloropropane) mg/kg 1.7 1.2 72 38-130 2,4,5-Trichlorophenol mg/kg 1.7 1.4 87 49-130 2,4,6-Trichlorophenol mg/kg 1.7 1.3 81 50-130 2,4-Dichlorophenol mg/kg 1.7 1.5 89 51-130 2,4-Dimethylphenol mg/kg 1.7 1.4 87 53-130 2,4-Dinitrophenol mg/kg 8.3 6.1 74 39-130 2,4-Dinitrotoluene mg/kg 1.7 1.4 87 53-130 2,6-Dinitrotoluene mg/kg 1.7 1.5 90 55-130 2-Chloronaphthalene mg/kg 1.7 1.3 80 48-130 2-Chlorophenol mg/kg 1.7 1.1 68 54-130 2-Methylnaphthalene mg/kg 1.7 1.4 82 57-130 2-Methylphenol(o-Cresol) mg/kg 1.7 1.4 82 50-130 2-Nitroaniline mg/kg 3.3 3.2 96 49-130 2-Nitrophenol mg/kg 1.7 1.3 78 50-130 3&4-Methyl phenol (m&p Cresol) mg/kg 1.7 1.3 76 50-130 3,3'-Dichlorobenzidine mg/kg 3.3 2.7 82 47-130IL 3-Nitroaniline mg/kg 3.3 3.1 93 45-130 4,6-Dinitro-2-methyl phenol mg/kg 3.3 2.8 83 50-142 4-Bromophenylphenyl ether mg/kg 1.7 1.5 91 55-130 4-ChIoro-3-methyl phenol mg/kg 3.3 3.1 92 52-130 4-Chloroaniline mg/kg 3.3 2.8 85 49-130 4-Chlorophenylphenyl ether mg/kg 1.7 1.5 91 53-130 4-Nitroaniline mg/kg 3.3 2.9 87 51-130 4-Nitrophenol mg/kg 8.3 6.8 82 40-130 Acenaphthene mg/kg 1.7 1.4 87 56-130 Acenaphthylene mg/kg 1.7 1.3 81 58-130 Aniline mg/kg 1.7 1.0 63 44-130 Anthracene mg/kg 1.7 1.3 82 60-130 Benzo(a)anthracene mg/kg 1.7 1.4 82 59-130 Benzo(a)pyrene mg/kg 1.7 1.4 82 57-130 Benzo(b)fluoranthene mg/kg 1.7 1.4 83 54-130 Benzo(g,h,i)perylene mg/kg 1.7 1.3 76 59-130 Benzo(k)fluoranthene mg/kg 1.7 1.4 87 54-130 Benzoic Acid mg/kg 8.3 4.1 50 19-130 Benzyl alcohol mg/kg 3.3 2.5 77 50-130 bis(2-Chloroethoxy)methane mg/kg 1.7 1.4 85 55-130 bis(2-Chloroethyl) ether mg/kg 1.7 1.3 81 53-130 bis(2-Ethylhexyl)phthalate mg/kg 1.7 1.8 107 58-130 Butylbenzylphthalate mg/kg 1.7 1.7 102 46-138 Chrysene mg/kg 1.7 1.4 84 57-130 Di-n-butylphthalate mg/kg 1.7 1.5 88 57-130 Di-n-octylphthalate mg/kg 1.7 1.8 106 57-130 Dibenz(a,h)anthracene mg/kg 1.7 1.3 78 60-130 Dibenzofuran mg/kg 1.7 1.5 88 54-130 Diethylphthalate mg/kg 1.7 1.4 87 55-130 Dimethylphthalate mg/kg 1.7 1.4 86 57-130 Fluoranthene mg/kg 1.7 1.4 87 57-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 54 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 LABORATORY CONTROL SAMPLE: Parameter 3685850 Units Spike Conc. LCS LCS Result % Rec Fluorene mg/kg 1.7 1.4 Hexachloro-1,3-butadiene mg/kg 1.7 1.3 Hexachlorobenzene mg/kg 1.7 1.4 Hexachlorocyclopentadiene mg/kg 1.7 0.31J Hexachloroethane mg/kg 1.7 1.2 Indeno(1,2,3-cd)pyrene mg/kg 1.7 1.3 Isophorone mg/kg 1.7 1.4 N-Nitroso-di-n-propylamine mg/kg 1.7 1.5 N-Nitrosodimethylamine mg/kg 1.7 1.1 N-Nitrosodiphenylamine mg/kg 1.7 1.4 Naphthalene mg/kg 1.7 1.3 Nitrobenzene mg/kg 1.7 1.3 Pentachlorophenol mg/kg 3.3 2.4 Phenanthrene mg/kg 1.7 1.4 Phenol mg/kg 1.7 1.3 Pyrene mg/kg 1.7 1.4 Pyridine mg/kg 1.7 1.0 2,4,6-Tribromophenol (S) % 2-Fluorobiphenyl (S) % 2-Fluorophenol (S) % Nitrobenzene-d5 (S) % Phenol-d6 (S) % Terphenyl-d14 (S) % % Rec Limits Qualifiers 86 56-130 77 41-130 82 53-130 19 23-130 L2,v2 73 48-130 78 61-130 86 49-130 90 52-130 68 45-130 86 56-130 77 56-130 81 50-130 73 33-130 86 60-130 80 54-130 87 61-130 60 35-130 70 18-130 65 19-130 53 18-130 68 21-130 60 18-130 70 15-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 55 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 QC Batch: 706771 Analysis Method: EPA 8270E QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92610717003 METHOD BLANK: 3687088 Associated Lab Samples: 92610717003 Parameter Units Matrix: Blank Result Solid Reporting Limit MDL Analyzed 1,2,4-Trichlorobenzene mg/kg ND 0.33 0.13 06/25/22 12:48 1,2-Dichlorobenzene mg/kg ND 0.33 0.12 06/25/22 12:48 1,3-Dichlorobenzene mg/kg ND 0.33 0.12 06/25/22 12:48 1,4-Dichlorobenzene mg/kg ND 0.33 0.13 06/25/22 12:48 1-Methylnaphthalene mg/kg ND 0.33 0.12 06/25/22 12:48 2,2'-Oxybis(1-chloropropane) mg/kg ND 0.33 0.16 06/25/22 12:48 2,4,5-Trichlorophenol mg/kg ND 0.33 0.15 06/25/22 12:48 2,4,6-Trichlorophenol mg/kg ND 0.33 0.14 06/25/22 12:48 2,4-Dichlorophenol mg/kg ND 0.33 0.13 06/25/22 12:48 2,4-Dimethylphenol mg/kg ND 0.33 0.14 06/25/22 12:48 2,4-Dinitrophenol mg/kg ND 1.7 1.0 06/25/22 12:48 2,4-Dinitrotoluene mg/kg ND 0.33 0.13 06/25/22 12:48 2,6-Dinitrotoluene mg/kg ND 0.33 0.12 06/25/22 12:48 2-Chloronaphthalene mg/kg ND 0.33 0.13 06/25/22 12:48 2-Chlorophenol mg/kg ND 0.33 0.13 06/25/22 12:48 2-Methylnaphthalene mg/kg ND 0.33 0.13 06/25/22 12:48 2-Methylphenol(o-Cresol) mg/kg ND 0.33 0.14 06/25/22 12:48 2-Nitroaniline mg/kg ND 1.7 0.27 06/25/22 12:48 2-Nitrophenol mg/kg ND 0.33 0.14 06/25/22 12:48 3&4-Methyl phenol (m&p Cresol) mg/kg ND 0.33 0.13 06/25/22 12:48 3,3'-Dichlorobenzidine mg/kg ND 0.67 0.23 06/25/22 12:48 3-Nitroaniline mg/kg ND 1.7 0.26 06/25/22 12:48 4,6-Dinitro-2-methyl phenol mg/kg ND 0.67 0.31 06/25/22 12:48 4-Bromophenylphenyl ether mg/kg ND 0.33 0.13 06/25/22 12:48 4-ChIoro-3-methyl phenol mg/kg ND 0.67 0.24 06/25/22 12:48 4-Chloroaniline mg/kg ND 0.67 0.26 06/25/22 12:48 4-Chlorophenylphenyl ether mg/kg ND 0.33 0.12 06/25/22 12:48 4-Nitroaniline mg/kg ND 0.67 0.25 06/25/22 12:48 4-Nitrophenol mg/kg ND 1.7 0.65 06/25/22 12:48 Acenaphthene mg/kg ND 0.33 0.12 06/25/22 12:48 Acenaphthylene mg/kg ND 0.33 0.12 06/25/22 12:48 Aniline mg/kg ND 0.33 0.13 06/25/22 12:48 Anthracene mg/kg ND 0.33 0.11 06/25/22 12:48 Benzo(a)anthracene mg/kg ND 0.33 0.11 06/25/22 12:48 Benzo(a)pyrene mg/kg ND 0.33 0.12 06/25/22 12:48 Benzo(b)fluoranthene mg/kg ND 0.33 0.11 06/25/22 12:48 Benzo(g,h,i)perylene mg/kg ND 0.33 0.13 06/25/22 12:48 Benzo(k)fluoranthene mg/kg ND 0.33 0.12 06/25/22 12:48 Benzoic Acid mg/kg ND 1.7 0.72 06/25/22 12:48 Benzyl alcohol mg/kg ND 0.67 0.25 06/25/22 12:48 IL Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 56 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 METHOD BLANK: 3687088 Associated Lab Samples: 92610717003 Parameter Units Matrix: Blank Result Solid Reporting Limit MDL Analyzed bis(2-Chloroethoxy)methane mg/kg ND 0.33 0.14 06/25/22 12:48 bis(2-Chloroethyl) ether mg/kg ND 0.33 0.13 06/25/22 12:48 bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 0.13 06/25/22 12:48 Butylbenzylphthalate mg/kg ND 0.33 0.14 06/25/22 12:48 Chrysene mg/kg ND 0.33 0.12 06/25/22 12:48 Di-n-butylphthalate mg/kg ND 0.33 0.11 06/25/22 12:48 Di-n-octylphthalate mg/kg ND 0.33 0.13 06/25/22 12:48 Dibenz(a,h)anthracene mg/kg ND 0.33 0.13 06/25/22 12:48 Dibenzofuran mg/kg ND 0.33 0.12 06/25/22 12:48 Diethylphthalate mg/kg ND 0.33 0.12 06/25/22 12:48 Dimethylphthalate mg/kg ND 0.33 0.12 06/25/22 12:48 Fluoranthene mg/kg ND 0.33 0.11 06/25/22 12:48 Fluorene mg/kg ND 0.33 0.12 06/25/22 12:48 Hexachloro-1,3-butadiene mg/kg ND 0.33 0.14 06/25/22 12:48 Hexachlorobenzene mg/kg ND 0.33 0.13 06/25/22 12:48 Hexachlorocyclopentadiene mg/kg ND 0.33 0.19 06/25/22 12:48 Hexachloroethane mg/kg ND 0.33 0.13 06/25/22 12:48 Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 0.13 06/25/22 12:48 Isophorone mg/kg ND 0.33 0.15 06/25/22 12:48 N-Nitroso-di-n-propylamine mg/kg ND 0.33 0.13 06/25/22 12:48 N-Nitrosodimethylamine mg/kg ND 0.33 0.11 06/25/22 12:48 N-Nitrosodiphenylamine mg/kg ND 0.33 0.12 06/25/22 12:48 Naphthalene mg/kg ND 0.33 0.11 06/25/22 12:48 Nitrobenzene mg/kg ND 0.33 0.16 06/25/22 12:48 Pentachlorophenol mg/kg ND 0.67 0.33 06/25/22 12:48 Phenanthrene mg/kg ND 0.33 0.11 06/25/22 12:48 Phenol mg/kg ND 0.33 0.15 06/25/22 12:48 Pyrene mg/kg ND 0.33 0.14 06/25/22 12:48 Pyridine mg/kg ND 0.33 0.11 06/25/22 12:48 2,4,6-Tribromophenol (S) % 68 18-130 06/25/22 12:48 2-Fluorobiphenyl (S) % 74 19-130 06/25/22 12:48 2-Fluorophenol (S) % 67 18-130 06/25/22 12:48 Nitrobenzene-d5 (S) % 88 21-130 06/25/22 12:48 Phenol-d6 (S) % 73 18-130 06/25/22 12:48 Terphenyl-d14 (S) % 81 15-130 06/25/22 12:48 v2 v2 Qualifiers LABORATORY CONTROL SAMPLE: 3687089 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,2,4-Trichlorobenzene mg/kg 1.7 1.3 75 47-130 1,2-Dichlorobenzene mg/kg 1.7 1.3 75 49-130 1,3-Dichlorobenzene mg/kg 1.7 1.2 72 48-130 1,4-Dichlorobenzene mg/kg 1.7 1.2 74 49-130 1-Methylnaphthalene mg/kg 1.7 1.4 81 54-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 57 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 LABORATORY CONTROL SAMPLE: Parameter 3687089 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2,2'-Oxybis(1-chloropropane) mg/kg 1.7 1.3 75 38-130 2,4,5-Trichlorophenol mg/kg 1.7 1.4 83 49-130 2,4,6-Trichlorophenol mg/kg 1.7 1.3 74 50-130 2,4-Dichlorophenol mg/kg 1.7 1.4 86 51-130 2,4-Dimethylphenol mg/kg 1.7 1.4 84 53-130 2,4-Dinitrophenol mg/kg 8.4 5.9 70 39-130 2,4-Dinitrotoluene mg/kg 1.7 1.4 83 53-130 2,6-Dinitrotoluene mg/kg 1.7 1.4 85 55-130 2-Chloronaphthalene mg/kg 1.7 1.4 81 48-130 2-Chlorophenol mg/kg 1.7 1.2 69 54-130 2-Methylnaphthalene mg/kg 1.7 1.4 80 57-130 2-Methylphenol(o-Cresol) mg/kg 1.7 1.3 78 50-130 2-Nitroaniline mg/kg 3.4 3.1 91 49-130 2-Nitrophenol mg/kg 1.7 1.3 75 50-130 3&4-Methyl phenol (m&p Cresol) mg/kg 1.7 1.2 72 50-130 3,3'-Dichlorobenzidine mg/kg 3.4 2.9 85 47-130IL 3-Nitroaniline mg/kg 3.4 3.1 91 45-130 4,6-Dinitro-2-methyl phenol mg/kg 3.4 2.5 74 50-142 4-Bromophenylphenyl ether mg/kg 1.7 1.4 86 55-130 4-ChIoro-3-methyl phenol mg/kg 3.4 3.0 88 52-130 4-Chloroaniline mg/kg 3.4 2.8 83 49-130 4-Chlorophenylphenyl ether mg/kg 1.7 1.4 86 53-130 4-Nitroaniline mg/kg 3.4 2.9 86 51-130 4-Nitrophenol mg/kg 8.4 6.3 74 40-130 Acenaphthene mg/kg 1.7 1.5 87 56-130 Acenaphthylene mg/kg 1.7 1.4 84 58-130 Aniline mg/kg 1.7 1.1 62 44-130 Anthracene mg/kg 1.7 1.4 82 60-130 Benzo(a)anthracene mg/kg 1.7 1.4 83 59-130 Benzo(a)pyrene mg/kg 1.7 1.3 78 57-130 Benzo(b)fluoranthene mg/kg 1.7 1.3 76 54-130 Benzo(g,h,i)perylene mg/kg 1.7 1.4 81 59-130 Benzo(k)fluoranthene mg/kg 1.7 1.4 81 54-130 Benzoic Acid mg/kg 8.4 4.2 50 19-130 Benzyl alcohol mg/kg 3.4 2.5 75 50-130 bis(2-Chloroethoxy)methane mg/kg 1.7 1.4 83 55-130 bis(2-Chloroethyl) ether mg/kg 1.7 1.4 80 53-130 bis(2-Ethylhexyl)phthalate mg/kg 1.7 1.7 103 58-130 Butylbenzylphthalate mg/kg 1.7 1.6 97 46-138 Chrysene mg/kg 1.7 1.5 87 57-130 Di-n-butylphthalate mg/kg 1.7 1.5 91 57-130 Di-n-octylphthalate mg/kg 1.7 1.8 106 57-130 Dibenz(a,h)anthracene mg/kg 1.7 1.4 83 60-130 Dibenzofuran mg/kg 1.7 1.5 88 54-130 Diethylphthalate mg/kg 1.7 1.4 85 55-130 Dimethylphthalate mg/kg 1.7 1.4 85 57-130 Fluoranthene mg/kg 1.7 1.6 92 57-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 58 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 LABORATORY CONTROL SAMPLE: 3687089 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Fluorene mg/kg 1.7 1.5 86 56-130 Hexachloro-1,3-butadiene mg/kg 1.7 1.3 77 41-130 Hexachlorobenzene mg/kg 1.7 1.3 78 53-130 Hexachlorocyclopentadiene mg/kg 1.7 ND 11 23-130 L2,v3 Hexachloroethane mg/kg 1.7 1.2 73 48-130 Indeno(1,2,3-cd)pyrene mg/kg 1.7 1.4 82 61-130 Isophorone mg/kg 1.7 1.4 85 49-130 N-Nitroso-di-n-propylamine mg/kg 1.7 1.5 88 52-130 N-Nitrosodimethylamine mg/kg 1.7 1.0 62 45-130 N-Nitrosodiphenylamine mg/kg 1.7 1.4 85 56-130 Naphthalene mg/kg 1.7 1.3 78 56-130 Nitrobenzene mg/kg 1.7 1.4 83 50-130 Pentachlorophenol mg/kg 3.4 2.0 59 33-130 v3 Phenanthrene mg/kg 1.7 1.5 89 60-130 Phenol mg/kg 1.7 1.3 78 54-130 Pyrene mg/kg 1.7 1.5 87 61-130 Pyridine mg/kg 1.7 0.90 53 35-130 2,4,6-Tribromophenol (S) % 81 18-130 2-Fluorobiphenyl (S) % 78 19-130 2-Fluorophenol(S) % 64 18-130 Nitrobenzene-d5 (S) % 79 21-130 Phenol-d6 (S) % 72 18-130 Terphenyl-d14 (S) % 81 15-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3688396 3688397 MS MSD 92604719004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,2,4-Trichoorobenzene mg/kg ND 1.7 1.6 1.2 1.2 73 70 22-130 5 30 1,2-Dichlorobenzene mg/kg ND 1.7 1.6 1.2 1.2 74 73 23-130 4 30 1,3-Dichlorobenzene mg/kg ND 1.7 1.6 1.2 1.1 70 69 26-130 3 30 1,4-Dichlorobenzene mg/kg ND 1.7 1.6 1.2 1.2 73 73 27-130 2 30 1-Methyl naphthalene mg/kg ND 1.7 1.6 1.3 1.3 79 79 30-130 2 30 2,2'-Oxybis(1- mg/kg ND 1.7 1.6 1.2 1.2 71 70 30-130 3 30 chloropropane) 2,4,5-Trichlorophenol mg/kg ND 1.7 1.6 1.3 1.3 75 81 26-130 6 30 2,4,6-Trichlorophenol mg/kg ND 1.7 1.6 1.2 1.2 69 73 23-130 4 30 2,4-Dichlorophenol mg/kg ND 1.7 1.6 1.4 1.4 85 82 29-130 5 30 2,4-Dimethylphenol mg/kg ND 1.7 1.6 1.1 1.0 65 64 13-130 3 30 2,4-Dinitrophenol mg/kg ND 8.4 8.2 5.2 5.4 62 65 10-131 3 30 2,4-Dinitrotoluene mg/kg ND 1.7 1.6 1.3 1.3 76 81 28-130 4 30 2,6-Dinitrotoluene mg/kg ND 1.7 1.6 1.3 1.3 76 82 36-130 6 30 2-Chloronaphthalene mg/kg ND 1.7 1.6 1.3 1.3 75 78 27-130 2 30 2-Chlorophenol mg/kg ND 1.7 1.6 1.1 1.1 67 66 29-130 3 30 2-Methyl naphthalene mg/kg ND 1.7 1.6 1.3 1.3 79 79 29-130 2 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 59 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3688396 3688397 MS MSD 92604719004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 2-Methyl phenol(o-Cresol) mg/kg ND 1.7 1.6 1.2 1.2 73 71 20-130 4 30 2-Nitroaniline mg/kg ND 3.4 3.3 2.8 2.9 85 88 29-130 1 30 2-Nitrophenol mg/kg ND 1.7 1.6 1.2 1.2 72 73 26-130 0 30 3&4-Methylphenol(m&p mg/kg ND 1.7 1.6 1.1 1.1 65 66 10-176 0 30 Cresol) 3,3'-Dichlorobenzidine mg/kg ND 3.4 3.3 2.5 2.5 74 77 15-130 1 30 IL 3-Nitroaniline mg/kg ND 3.4 3.3 2.8 2.9 82 87 28-130 4 30 4,6-Dinitro-2-methylphenol mg/kg ND 3.4 3.3 2.3 2.3 70 71 15-132 0 30 4-Bromophenylphenyl ether mg/kg ND 1.7 1.6 1.3 1.4 78 83 35-130 5 30 4-Chloro-3-methylphenol mg/kg ND 3.4 3.3 2.8 2.9 85 88 30-130 1 30 4-Chloroaniline mg/kg ND 3.4 3.3 2.6 2.6 79 79 28-130 2 30 4-Chlorophenylphenyl ether mg/kg ND 1.7 1.6 1.3 1.4 80 83 32-130 2 30 4-Nitroaniline mg/kg ND 3.4 3.3 2.6 2.6 77 79 30-130 0 30 4-Nitrophenol mg/kg ND 8.4 8.2 5.7 5.8 68 71 17-130 3 30 Acenaphthene mg/kg ND 1.7 1.6 1.3 1.4 80 85 29-130 4 30 Acenaphthylene mg/kg ND 1.7 1.6 1.3 1.3 77 80 31-130 2 30 Aniline mg/kg ND 1.7 1.6 0.78 0.74 46 45 10-130 5 30 Anthracene mg/kg ND 1.7 1.6 1.3 1.3 77 81 33-130 3 30 Benzo(a)anth race ne mg/kg ND 1.7 1.6 1.3 1.3 75 79 32-130 3 30 Benzo(a)pyrene mg/kg ND 1.7 1.6 1.2 1.2 72 73 32-130 0 30 Benzo(b)fluoranthene mg/kg ND 1.7 1.6 1.2 1.2 69 71 33-130 2 30 Benzo(g,h,i)perylene mg/kg ND 1.7 1.6 1.2 1.2 72 75 28-130 2 30 Benzo(k)fluoranthene mg/kg ND 1.7 1.6 1.2 1.3 74 78 31-130 2 30 Benzoic Acid mg/kg ND 8.4 8.2 1.8 1.11 22 13 10-130 30 Benzyl alcohol mg/kg ND 3.4 3.3 2.5 2.4 75 73 31-130 5 30 bis(2- mg/kg ND 1.7 1.6 1.3 1.3 79 80 30-130 1 30 Chloroethoxy)methane bis(2-Chloroethyl) ether mg/kg ND 1.7 1.6 1.3 1.3 77 78 68-130 1 30 bis(2- Ethyl hexyl)phthalate mg/kg ND 1.7 1.6 1.5 1.5 90 93 40-130 1 30 Butylbenzylphthalate mg/kg ND 1.7 1.6 1.4 1.4 84 87 40-130 2 30 Chrysene mg/kg ND 1.7 1.6 1.3 1.4 80 84 30-130 3 30 Di-n-butylphthalate mg/kg ND 1.7 1.6 1.4 1.4 82 86 41-130 2 30 Di-n-octylphthalate mg/kg ND 1.7 1.6 1.6 1.6 94 97 42-130 2 30 Dibenz(a,h)anthracene mg/kg ND 1.7 1.6 1.2 1.3 74 78 27-130 3 30 Dibenzofuran mg/kg ND 1.7 1.6 1.4 1.4 82 86 32-130 3 30 Diethylphthalate mg/kg ND 1.7 1.6 1.3 1.3 78 82 40-130 3 30 Dimethylphthalate mg/kg ND 1.7 1.6 1.3 1.4 79 83 37-130 4 30 Fluoranthene mg/kg ND 1.7 1.6 1.4 1.5 86 90 26-130 3 30 Fluorene mg/kg ND 1.7 1.6 1.3 1.4 79 83 31-130 3 30 Hexachloro-1,3-butadiene mg/kg ND 1.7 1.6 1.2 1.2 73 73 20-130 1 30 Hexachlorobenzene mg/kg ND 1.7 1.6 1.3 1.3 75 76 29-130 0 30 Hexachlorocyclopentadiene mg/kg ND 1.7 1.6 ND ND 9 10 10-130 30 MO,v3 Hexachloroethane mg/kg ND 1.7 1.6 1.2 1.2 72 70 21-130 4 30 Indeno(1,2,3-cd)pyrene mg/kg ND 1.7 1.6 1.2 1.2 72 75 28-130 2 30 Isophorone mg/kg ND 1.7 1.6 1.4 1.4 81 84 32-130 1 30 N-Nitroso-di-n-propylamine mg/kg ND 1.7 1.6 1.5 1.4 88 86 31-130 4 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 60 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3688396 3688397 MS MSD 92604719004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual N-Nitrosodimethylamine mg/kg ND 1.7 1.6 1.1 0.88 64 54 20-130 19 30 N-Nitrosodiphenylamine mg/kg ND 1.7 1.6 1.3 1.3 77 81 32-130 3 30 Naphthalene mg/kg ND 1.7 1.6 1.3 1.2 75 75 30-130 2 30 Nitrobenzene mg/kg ND 1.7 1.6 1.3 1.3 77 79 25-130 1 30 Pentachlorophenol mg/kg ND 3.4 3.3 1.8 1.8 53 55 10-130 2 30 v3 Phenanthrene mg/kg ND 1.7 1.6 1.4 1.4 82 86 34-130 2 30 Phenol mg/kg ND 1.7 1.6 1.2 1.2 73 73 14-130 2 30 Pyrene mg/kg ND 1.7 1.6 1.3 1.3 79 82 31-130 1 30 Pyridine mg/kg ND 1.7 1.6 0.98 0.86 59 52 10-130 13 30 2,4,6-Tribromophenol (S) % 63 66 18-130 2-Fluorobiphenyl (S) % 69 74 19-130 2-Fluorophenol(S) % 54 57 18-130 Nitrobenzene-d5(S) % 75 74 21-130 Phenol-d6 (S) % 67 66 18-130 Terphenyl-d14 (S) % 69 72 15-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 61 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 QC Batch: 706005 Analysis Method: SW-846 QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92610717001, 92610717002, 92610717003, 92610717004, 92610717005, 92610717006, 92610717007, 92610717008 SAMPLE DUPLICATE: 3683571 92610717008 Dup Max Parameter Units Result Result RPD RPD Qualifiers Percent Moisture % 12.0 11.7 2 25 N2 SAMPLE DUPLICATE: 3683573 92610909001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Percent Moisture % 12.8 14.9 15 25 N2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 62 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 QC Batch: 1884410 Analysis Method: SM 2540G QC Batch Method: SM 2540 G Analysis Description: Total Solids 2540 G-2011 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92610717001, 92610717002, 92610717003, 92610717004 METHOD BLANK: R3808223-1 Matrix: Solid Associated Lab Samples: 92610717001, 92610717002, 92610717003, 92610717004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Solids % 0.00300 06/27/22 13:11 LABORATORY CONTROL SAMPLE: R3808223-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Solids % 50.0 50.0 100 85.0-115 SAMPLE DUPLICATE: R3808223-3 L1506535-02 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Solids % 77.0 75.2 2.33 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 63 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 QC Batch: 1884524 Analysis Method: SM 2540G QC Batch Method: SM 2540 G Analysis Description: Total Solids 2540 G-2011 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92610717005, 92610717006, 92610717007, 92610717008 METHOD BLANK: R3807366-1 Matrix: Solid Associated Lab Samples: 92610717005, 92610717006, 92610717007, 92610717008 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Solids % 0.00100 06/24/22 09:14 LABORATORY CONTROL SAMPLE: R3807366-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Solids % 50.0 50.0 100 85.0-115 SAMPLE DUPLICATE: R3807366-3 92610717007 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Solids % 81.1 80.8 0.367 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 64 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92610717 QC Batch: 1894241 Analysis Method: EPA 7199 QC Batch Method: 3060A Analysis Description: Wet Chemistry 7199 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92610717001, 92610717002, 92610717003 METHOD BLANK: R3816510-1 Matrix: Solid Associated Lab Samples: 92610717001, 92610717002, 92610717003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Chromium, Hexavalent mg/kg ND 1.00 0.255 07/15/22 09:39 LABORATORY CONTROL SAMPLE: R3816510-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chromium, Hexavalent mg/kg 10.0 9.85 98.5 80.0-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3816510-4 R3816510-5 MS MSD L1510486-01 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chromium, Hexavalent mg/kg ND 20.0 20.0 6.29 7.74 31.5 38.7 75.0-125 20.7 20 ML,R1 MATRIX SPIKE SAMPLE: R3816510-7 L1510486-01 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Chromium, Hexavalent mg/kg ND 643 588 91.5 75.0-125 SAMPLE DUPLICATE: R3816510-3 L1507120-33 Dup Max Parameter Units Result Result RPD RPD Qualifiers Chromium, Hexavalent mg/kg ND ND 0.00 20 SAMPLE DUPLICATE: R3816510-8 L1510486-02 Dup Max Parameter Units Result Result RPD RPD Qualifiers Chromium, Hexavalent mg/kg ND ND 0.00 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 65 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: Wright's Executive Sales Pace Project No.: 92610717 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. SAMPLE QUALIFIERS Sample: R3816510-4 Ill Wet Chemistry by Method 7199 - Matrix spike failure due to matrix; sample is a reducer. Sample: R3816510-5 Ill Wet Chemistry by Method 7199 - Matrix spike failure due to matrix; sample is a reducer. ANALYTE QUALIFIERS D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference. E Analyte concentration exceeded the calibration range. The reported result is estimated. IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be considered an estimated value. IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be considered an estimated value. LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits. L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samples may be biased low. MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 66 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: Wright's Executive Sales Pace Project No.: 92610717 ANALYTE QUALIFIERS ML Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased low. N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditations/certifications is available upon request. P8 Analyte was detected in the method blank. All associated samples had concentrations of at least ten times greater than the blank or were below the reporting limit. P9 RPD between the primary and confirmatory analysis exceeded 40%. R1 RPD value was outside control limits. S4 Surrogate recovery not evaluated against control limits due to sample dilution. v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 67 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: Wright's Executive Sales 92610717 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92610717001 UT-1 3546 1883600 EPA 8141 B 1883600 92610717002 UT-4 3546 1883600 EPA 8141 B 1883600 92610717003 DUP-2 3546 1883600 EPA 8141 B 1883600 92610717004 BG-1 3546 1883600 EPA 8141 B 1883600 92610717005 BG-2 3546 1883600 EPA 8141 B 1883600 92610717006 BG-3 3546 1883600 EPA 8141 B 1883600 92610717007 BG-4 3546 1883600 EPA 8141 B 1883600 92610717008 BG-5 3546 1883600 EPA 8141 B 1883600 92610717001 UT-1 8151A 1887325 EPA 8151 1887325 92610717002 UT-4 8151A 1888224 EPA 8151 1888224 92610717003 DUP-2 8151A 1888224 EPA 8151 1888224 92610717004 BG-1 8151A 1887325 EPA 8151 1887325 92610717005 BG-2 8151A 1888224 EPA 8151 1888224 92610717006 BG-3 8151A 1888224 EPA 8151 1888224 92610717007 BG-4 8151A 1888224 EPA 8151 1888224 92610717008 BG-5 8151A 1888224 EPA 8151 1888224 92610717001 UT-1 EPA 3546 706233 EPA 8081B 706428 92610717002 UT-4 EPA 3546 706233 EPA 8081B 706428 92610717003 DUP-2 EPA 3546 706233 EPA 8081 B 706428 92610717004 BG-1 EPA 3546 706233 EPA 8081 B 706428 92610717005 BG-2 EPA 3546 706233 EPA 8081 B 706428 92610717006 BG-3 EPA 3546 706233 EPA 8081 B 706428 92610717007 BG-4 EPA 3546 706233 EPA 8081 B 706428 92610717008 BG-5 EPA 3546 706233 EPA 8081 B 706428 92610717001 UT-1 EPA 3050B 743891 EPA 6020B 744354 92610717002 UT-4 EPA 3050B 743891 EPA 6020B 744354 92610717003 DUP-2 EPA 3050B 743891 EPA 6020B 744354 92610717001 UT-1 METHOD 743963 EPA 7471 B 744162 92610717002 UT-4 METHOD 743963 EPA 7471 B 744162 92610717003 DUP-2 METHOD 743963 EPA 7471 B 744162 92610717001 UT-1 EPA 3546 706520 EPA 8270E 707027 92610717002 UT-4 EPA 3546 706520 EPA 8270E 707027 92610717003 DUP-2 EPA 3546 706771 EPA 8270E 707029 92610717001 UT-1 EPA 5035A/5030B 706065 EPA 8260D 706179 92610717002 UT-4 EPA 5035A/5030B 706065 EPA 8260D 706179 92610717003 DUP-2 EPA 5035A/5030B 706065 EPA 8260D 706179 92610717001 UT-1 SW-846 706005 92610717002 UT-4 SW-846 706005 92610717003 DUP-2 SW-846 706005 92610717004 BG-1 SW-846 706005 92610717005 BG-2 SW-846 706005 92610717006 BG-3 SW-846 706005 92610717007 BG-4 SW-846 706005 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:22 PM without the written consent of Pace Analytical Services, LLC. Page 68 of 72 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: Wright's Executive Sales 92610717 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92610717008 BG-5 SW-846 706005 92610717001 UT-1 SM 2540 G 1884410 SM 2540G 1884410 92610717002 UT-4 SM 2540 G 1884410 SM 2540G 1884410 92610717003 DUP-2 SM 2540 G 1884410 SM 2540G 1884410 92610717004 BG-1 SM 2540 G 1884410 SM 2540G 1884410 92610717005 BG-2 SM 2540 G 1884524 SM 2540G 1884524 92610717006 BG-3 SM 2540 G 1884524 SM 2540G 1884524 92610717007 BG-4 SM 2540 G 1884524 SM 2540G 1884524 92610717008 BG-5 SM 2540 G 1884524 SM 2540G 1884524 92610717001 UT-1 3060A 1894241 EPA 7199 1894241 92610717002 UT-4 3060A 1894241 EPA 7199 1894241 92610717003 DUP-2 3060A 1894241 EPA 7199 1894241 Date: 07/21 /2022 05:22 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 69 of 72 L-. r-r F-1-nuly 1-vvoj vu'1 barnple condition Upon Receipt ,!laace - -- Effective Date: 05/112/202205/12/2O22 Laboratory receiving samples: ` Asheville ❑ Eden[] Greenwood ❑ Huntersville [] Raleigh❑ Mechanicsville❑ Atlanta[] Kernersville❑ Sample Condition Client Name: .. c ' Project tf: W01t •• 92610717 Courier: ❑F d Ex ❑UPS LISPS ❑Client ❑ Commercial [Pace ❑Other: I I I Custody Seat Present? Dyes E94 Seals Intact? []Yes E No 9261O717 Packing Material: ❑Bubble Wrap WBbble Bags ❑None ❑ Other Thermomerer: [V� IR Gun ID:� -1 Type of I[e; WeE ❑Blue Correction Factor: Cooler Temp: _� Add/Subtract (°C) 0 Cooler Temp Corrected (IC). USDA Regulated Sail (❑ N/A, water sample) Did samples originate in a q#brantine zone within the United States: CA, NY, or SC (check mans)?MYes FTNn. Chain of Custody Present? &es ❑No ❑N/A 1. Samples Arrived within hold Time? es ONO ❑N/A 2. Short Hold Time Analysis (c72 hr.)? ❑Yes N ❑N/A 3. Rush Turn Around Time Requested? ❑ ees No ❑N/A 4. Sufficient Volume? ®Y s ❑No ❑N/A S. Correct Containers Used? s []No ❑N/A 6. -Pace Containers Used? y s ❑No ❑N/A Containers Intact? es ❑No ❑N A 7, Dissolved analysis: Samples Field Filtered? ❑yes [--]No N/A S. Sample Labels Match CDC? ()Yes ❑No ❑N/A 9. Date/Initials Person Examining Contents.-4 f ^ f Biological Tissue Frozen? ❑Yes [:]No E N/A ❑None Temp should be above freezing to 6°C []Samples out of temp criteria. Samples on ice, cooiing process has begun Did samples originate from a foreign source {internationally, including Hawaii and Puerto Rico)? [-]Yes -Includes Date/Time/ID/Analysis Matrix: Headspace in VOA Vials (>5-6mm)? ❑Yes ❑No N/A 10. Trip Blank Present? ❑Yes ❑No YN/A A 11. Trip Blank Custody Seals Present? []Yes ONO COMMENTS/SAMPLE DISCREPANCY Field Data Required? Des ❑No CLIENT NOTIFICATION/RESOLUTION Lot ID of split containers: Person contacted: Date/Time: Project Manager SCURF Review: Date; ProlectanagetSRF Review:— Page 70 of 72 Quaitrax ID: 69614 Page 1 of 2 �l°�ace ���- i Zara. erYv-rr%m-nLjii i-uua,3 vu'l �ampie uonaitlon upon Keceipt Effective Date: 051121202205112/2022 *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 {waters DOC, LLHg *"Bottom half of box is to list number of bottles ***Check all unpreserved Nitrates for chlorine Project Wo# : 92'610717 PM: F1MB Due Date: 07/01/22 CLIENT: 92—ECS RAL It E of V Z Z7 al m c > a J E ' v a z 'tl a N ti z > a. J E M a Z GN w c > a J E N a Z 'O N v n c � m d v ? r4 a u N V d O ry = M Nl J E rN-{ 1!r 7 a N^y y 2 m 2 S m CL J E N Z M a m 2 o Z Ob .�. z N m a J E „4 .0 a w A S n _ z u m a J E ,1 m d a m C N _m L7 a r o E v 4L 3 U ? 9 Z N a a -0 E Q v r! 7 •+ l9 vt N x n u 2 N .0 E Q a rl 2 .4 4 u -13 a a a v E 4 J E N M l7 a ^r _ a v O v = aJ E Q °' r-1 rf l7 a N v C O `� T A 4 J E N 1A M L7 a U z 2 z ` 01 E Q J E N R M G ¢ z U = Q Q } J E V S M o \ z M N m Z Q o `> E q r di Cf > Q Z t v a m a c D Q Q > J E 7 > T > d z a rn S Q O > J E V > cn ¢ z a N = Q p > E V� N as a Z ..+ Y ^ t3 a 7 ; Yai a � - ° `a l7 a l6 Q V uQJ o. •-- a; ♦7 E N u~1 � f9 I Q y m a = a Vl J E N trV a. fN1 dl 0 O ry M z „ m 0. E Ln N r 1 m d a, m c E Q E � t3 ¢ z 'T Q } Z N m a) c `L o c 7 y n c V E 0 J E E Iry V' C7 m � o 1 \NN 7 3 t 1 aN { s { N\N 6 ` l 7 8 N \'�JNN N N �s 9 10 13 32 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot N "Ut-—UJInver Anere 15 a ulscrepancy arrecring North r.aronna compliance samples, a copy Of this toms will 6e sent to the North Carolina OENRCertifcation dffice (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Quaitrax 1D: 69614 Page 2 of 2 Page 71 of 72 CHAIN -OF -CUSTODY ! Analytical Request Document :4f — Ce The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. I Submitting a sample via this chain of custody constitutes acknowledgment and acceptance of the Pace Terms and Conditions found at https://info,pacelabs.comthubfstpas-standard-terms.odt. Qecnan A Section B Section C Required Client Information: Required Project Information: invoice Information: Page • 1 Of 1 Company ECS Raleigh Report To: Austin Deans Attention: Address 5260 Greens Dairy Road Copy To. _ ( '� _(.<<.F r Company Name: Raleigh, NC 27616 Address: Regulatory Agency Email: ADeans@ecslimited.com Purchase Order Pace Quote: Phone: (919)861-9910 JFax Project Name: Wright's Executive Sales 11039-B Pace Project Manager angela-baioni pacelabs.com, State I Location Requested Due Date. Project #: jry _ Pace Profile #, 13570- NC Re uested Anal sis Filtered YIN MATRIX coal COLLECTED Z Preservatives Z '- E Drinking Weser DW W.W Wr °f H U O U WasteMw Ww '...I P Q 7 F sonlsnua sL SAMPLE ID ou N i7 START END !- 'o L v oL One Character per box. Wipe wp `. r H (A-Z, 0-91, •t l4r AR Ids must be unique of„�1eos X 6 y w F p — `Sample o `m a1 }� ~ om o i 192—Lo DATE TIME DATE TIME m = i 2 o m m tr I 2 3 f>G _i c IC 4 -z- 5 G 6 3 GI V 1 7 t3 M -z c 9 10 11 F 12 I I I I I L-- ADDITIONAL, COMMENTS RELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATEg SAMPLE CQN0rhONS 01 SAMPLER NAME AND SIGNATURE c PRINT Name of SAMPLER: U SIGNATURE of SAMPLER: DATE Signed: ribLz w 3 m g z a m H � ci �- �U leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 July 21, 2022 Ron Navarro ECS Raleigh 5260 Greens Dairy Road Raleigh, NC 27616 RE: Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 Dear Ron Navarro: Enclosed are the analytical results for sample(s) received by the laboratory on June 21, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Gulf Coast • Pace National - Mt. Juliet • Pace Analytical Services - Charlotte Revised to include MDL's and J Flags per client request 07/21/22. If you have any questions concerning this report, please feel free to contact me. Sincerely, cL,+1,1- Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures cc: ECS Southeast Reporting, ECS Southeast Sam Szakasits, ECS Raleigh REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 44 lacieAnalyfica(' www,pacelabs.com Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 Pace Analytical Services National 12065 Lebanon Road, Mt. Juliet, TN 37122 Alabama Certification #: 40660 Alaska Certification 17-026 Arizona Certification #: AZ0612 Arkansas Certification #: 88-0469 California Certification #: 2932 Canada Certification #: 1461.01 Colorado Certification #: TN00003 Connecticut Certification #: PH-0197 DOD Certification: #1461.01 EPA# TN00003 Florida Certification #: E87487 Georgia DW Certification #: 923 Georgia Certification: NELAP Idaho Certification #: TN00003 Illinois Certification #: 200008 Indiana Certification #: C-TN-01 Iowa Certification #: 364 Kansas Certification #: E-10277 Kentucky UST Certification #: 16 Kentucky Certification #: 90010 Louisiana Certification #: A130792 Louisiana DW Certification #: LA180010 Maine Certification #: TN0002 Maryland Certification #: 324 Massachusetts Certification #: M-TNO03 Michigan Certification #: 9958 Minnesota Certification #: 047-999-395 Mississippi Certification #: TN00003 Missouri Certification #: 340 Montana Certification M CERT0086 Nebraska Certification #: NE-OS-15-05 Pace Analytical Gulf Coast 7979 Innovation Park Drive, Baton Rouge, LA 70820 Arkansas Certification #: 88-0655 DoD ELAP Certification M 6429-01 Florida Certification #: E87854 Illinois Certification #: 004585 Kansas Certification #: E-10354 Louisiana/LELAP Certification #: 01955 North Carolina Certification M 618 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 CERTIFICATIONS Nevada Certification #: TN-03-2002-34 New Hampshire Certification #: 2975 New Jersey Certification #: TNO02 New Mexico DW Certification New York Certification #: 11742 North Carolina Aquatic Toxicity Certification #: 41 North Carolina Drinking Water Certification #: 21704 North Carolina Environmental Certificate #: 375 North Dakota Certification #: R-140 Ohio VAP Certification #: CL0069 Oklahoma Certification #: 9915 Oregon Certification #: TN200002 Pennsylvania Certification #: 68-02979 Rhode Island Certification #: LA000356 South Carolina Certification #: 84004 South Dakota Certification Tennessee DW/Chem/Micro Certification #: 2006 Texas Certification #: T 104704245-17-14 Texas Mold Certification #: LAB0152 USDA Soil Permit #: P330-15-00234 Utah Certification #: TN00003 Virginia Certification #: VT2006 Vermont Dept. of Health: ID# VT-2006 Virginia Certification #: 460132 Washington Certification #: C847 West Virginia Certification #: 233 Wisconsin Certification #: 998093910 Wyoming UST Certification #: via A21-A 2926.01 A21-A-ISO 17025 Certification #: 1461.01 A21-A-ISO 17025 Certification #: 1461.02 AIHA-LAP/LLC EMLAP Certification #:100789 North Dakota Certification #: R-195 Oklahoma Certification #: 2019-101 South Carolina Certification #: 73006001 Texas Certification #: T104704178-19-11 USDA Soil Permit # P330-19-00209 Virginia Certification #: 460215 Washington Certification #: C929 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 Lab ID Sample ID Matrix Date Collected Date Received 92611001001 92611001002 UT-3 DUP-3 Solid Solid 06/20/2214:20 06/20/22 00:00 06/21/2214:10 06/21/22 14:10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92611001001 UT-3 EPA 8141 B AO 27 PAN EPA8151 HMH 11 PAN EPA 8081 B BAJ 24 PASI-C EPA 6020E LWZ 7 GCLA EPA 7471 B TDM 1 GCLA EPA 8270E BPJ 75 PASI-C EPA 8260D LMB 70 PASI-C SW-846 KDF 1 PASI-C SM 2540G CMK 1 PAN EPA 7199 ERP 1 PAN 92611001002 DUP-3 EPA 8141B AO 27 PAN EPA 8151 HMH 11 PAN EPA 8081 B BAJ 24 PASI-C EPA 6020E LWZ 7 GCLA EPA 7471 B TDM 1 GCLA EPA 8270E BPJ 75 PASI-C EPA 8260D LMB 70 PASI-C SW-846 KDF 1 PASI-C SM 2540G CMK 1 PAN EPA 7199 ERP 1 PAN GCLA = Pace Analytical Gulf Coast PAN = Pace National - Mt. Juliet PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 Sample: UT-3 Lab ID: 92611001001 Collected: 06/20/22 14:20 Received: 06/21/22 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual OP Pesticides 8141 B Analytical Method: EPA 8141 B Preparation Method: 3546 Pace National - Mt. Juliet Azinphos, methyl (Guthion) ND mg/kg 0.115 0.0365 1 06/27/22 03:37 06/29/22 20:42 86-50-0 Bolstar ND mg/kg 0.115 0.0171 1 06/27/22 03:37 06/29/22 20:42 35400-43-2 Chlorpyrifos ND mg/kg 0.115 0.0180 1 06/27/22 03:37 06/29/22 20:42 2921-88-2 Coumaphos ND mg/kg 0.115 0.0279 1 06/27/22 03:37 06/29/22 20:42 56-72-4 Total Demeton ND mg/kg 0.0803 0.00670 1 06/27/22 03:37 06/29/22 20:42 8065-48-3 Diazinon ND mg/kg 0.115 0.0258 1 06/27/22 03:37 06/29/22 20:42 333-41-5 Dichlorvos ND mg/kg 0.115 0.0344 1 06/27/22 03:37 06/29/22 20:42 62-73-7 Dimethoate ND mg/kg 0.115 0.0383 1 06/27/22 03:37 06/29/22 20:42 60-51-5 Disulfoton ND mg/kg 0.115 0.0291 1 06/27/22 03:37 06/29/22 20:42 298-04-4 EPN (ENT) ND mg/kg 0.115 0.0317 1 06/27/22 03:37 06/29/22 20:42 2104-64-5 Ethoprop ND mg/kg 0.115 0.0135 1 06/27/22 03:37 06/29/22 20:42 13194-48-4 Parathion (Ethyl parathion) ND mg/kg 0.115 0.0188 1 06/27/22 03:37 06/29/22 20:42 56-38-2 Fensulfothion ND mg/kg 0.115 0.0405 1 06/27/22 03:37 06/29/22 20:42 115-90-2 Fenthion ND mg/kg 0.115 0.0153 1 06/27/22 03:37 06/29/22 20:42 55-38-9 Malathion ND mg/kg 0.115 0.0205 1 06/27/22 03:37 06/29/22 20:42 121-75-5 Merphos ND mg/kg 0.115 0.0266 1 06/27/22 03:37 06/29/22 20:42 150-50-5 Methyl parathion ND mg/kg 0.115 0.0233 1 06/27/22 03:37 06/29/22 20:42 298-00-0 Mevinphos ND mg/kg 0.115 0.0264 1 06/27/22 03:37 06/29/22 20:42 7786-34-7 Naled ND mg/kg 0.115 0.0551 1 06/27/22 03:37 06/29/22 20:42 300-76-5 Phorate ND mg/kg 0.115 0.0241 1 06/27/22 03:37 06/29/22 20:42 298-02-2 Ronnel ND mg/kg 0.115 0.0171 1 06/27/22 03:37 06/29/22 20:42 299-84-3 Stirophos (Tetrachlorvinphos) ND mg/kg 0.115 0.0204 1 06/27/22 03:37 06/29/22 20:42 22248-79-9 Sulfotepp (ThiodiphosphoricAc ND mg/kg 0.115 0.0113 1 06/27/22 03:37 06/29/22 20:42 3689-24-5 TEPP ND mg/kg 1.15 0.180 1 06/27/22 03:37 06/29/22 20:42 107-49-3 Tokuthion (Prothiofos) ND mg/kg 0.115 0.0172 1 06/27/22 03:37 06/29/22 20:42 34643-46-4 Trichloronate ND mg/kg 0.115 0.0231 1 06/27/22 03:37 06/29/22 20:42 327-98-0 Surrogates Triphenylphosphate (S) 64.9 % 36.0-121 1 06/27/22 03:37 06/29/22 20:42 115-86-6 Chlorinated Herb. (GC) 8151 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND mg/kg 0.0803 0.00806 1 06/30/22 21:57 07/03/22 06:43 94-75-7 LO Dalapon ND mg/kg 0.0803 0.0130 1 06/30/22 21:57 07/03/22 06:43 127-20-8 2,4-DB ND mg/kg 0.0803 0.0341 1 06/30/22 21:57 07/03/22 06:43 94-82-6 Dicamba ND mg/kg 0.0803 0.0180 1 06/30/22 21:57 07/03/22 06:43 1918-00-9 LO Dichloroprop ND mg/kg 0.0803 0.0281 1 06/30/22 21:57 07/03/22 06:43 15165-67-0 LO Dinoseb ND mg/kg 0.0803 0.00800 1 06/30/22 21:57 07/03/22 06:43 88-85-7 MCPA ND mg/kg 7.46 0.508 1 06/30/22 21:57 07/03/22 06:43 94-74-6 LO MCPP ND mg/kg 7.46 0.421 1 06/30/22 21:57 07/03/22 06:43 7085-19-0 2,4,5-T ND mg/kg 0.0803 0.00978 1 06/30/22 21:57 07/03/22 06:43 93-76-5 LO 2,4,5-TP (Silvex) ND mg/kg 0.0803 0.0123 1 06/30/22 21:57 07/03/22 06:43 93-72-1 LO Surrogates 2,4-DCAA (S) 65.3 % 22.0-132 1 06/30/22 21:57 07/03/22 06:43 19719-28-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 Sample: UT-3 Lab ID: 92611001001 Collected: 06/20/22 14:20 Received: 06/21/22 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 B Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Aldrin ND mg/kg 0.024 0.0096 10 06/24/22 16:02 06/29/22 09:43 309-00-2 alpha-BHC ND mg/kg 0.024 0.010 10 06/24/22 16:02 06/29/22 09:43 319-84-6 beta-BHC ND mg/kg 0.024 0.011 10 06/24/22 16:02 06/29/22 09:43 319-85-7 delta-BHC ND mg/kg 0.024 0.012 10 06/24/22 16:02 06/29/22 09:43 319-86-8 gamma-BHC (Lindane) ND mg/kg 0.024 0.0095 10 06/24/22 16:02 06/29/22 09:43 58-89-9 Chlordane (Technical) ND mg/kg 0.12 0.10 10 06/24/22 16:02 06/29/22 09:43 57-74-9 4,4'-DDD ND mg/kg 0.024 0.011 10 06/24/22 16:02 06/29/22 09:43 72-54-8 4,4'-DDE ND mg/kg 0.024 0.011 10 06/24/22 16:02 06/29/22 09:43 72-55-9 4,4'-DDT ND mg/kg 0.024 0.011 10 06/24/22 16:02 06/29/22 09:43 50-29-3 Dieldrin ND mg/kg 0.024 0.010 10 06/24/22 16:02 06/29/22 09:43 60-57-1 Endosulfan I ND mg/kg 0.024 0.010 10 06/24/22 16:02 06/29/22 09:43 959-98-8 Endosulfan II ND mg/kg 0.024 0.011 10 06/24/22 16:02 06/29/22 09:43 33213-65-9 Endosulfan sulfate ND mg/kg 0.024 0.013 10 06/24/22 16:02 06/29/22 09:43 1031-07-8 Endrin ND mg/kg 0.024 0.011 10 06/24/22 16:02 06/29/22 09:43 72-20-8 Endrin aldehyde ND mg/kg 0.024 0.016 10 06/24/22 16:02 06/29/22 09:43 7421-93-4 Endrin ketone ND mg/kg 0.024 0.013 10 06/24/22 16:02 06/29/22 09:43 53494-70-5 Heptachlor ND mg/kg 0.024 0.011 10 06/24/22 16:02 06/29/22 09:43 76-44-8 Heptachlor epoxide ND mg/kg 0.024 0.0094 10 06/24/22 16:02 06/29/22 09:43 1024-57-3 Hexachlorobenzene ND mg/kg 0.024 0.0098 10 06/24/22 16:02 06/29/22 09:43 118-74-1 Methoxychlor ND mg/kg 0.059 0.029 10 06/24/22 16:02 06/29/22 09:43 72-43-5 Mirex ND mg/kg 0.059 0.026 10 06/24/22 16:02 06/29/22 09:43 2385-85-5 Toxaphene ND mg/kg 0.083 0.063 10 06/24/22 16:02 06/29/22 09:43 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 0 % 10-133 10 06/24/22 16:02 06/29/22 09:43 877-09-8 D3,S4 Decachlorobiphenyl (S) 0 % 10-146 10 06/24/22 16:02 06/29/22 09:43 2051-24-3 S4 EPA 6020B Analytical Method: EPA 6020E Preparation Method: EPA 3050B Pace Analytical Gulf Coast Arsenic 1.97 mg/kg 0.42 0.10 10 06/26/22 09:00 06/29/22 20:20 7440-38-2 Barium 162 mg/kg 0.42 0.10 10 06/26/22 09:00 06/29/22 20:20 7440-39-3 Cadmium ND mg/kg 0.42 0.10 10 06/26/22 09:00 06/29/22 20:20 7440-43-9 Chromium 41.1 mg/kg 0.42 0.10 10 06/26/22 09:00 06/29/22 20:20 7440-47-3 Lead 12.1 mg/kg 0.42 0.10 10 06/26/22 09:00 06/29/22 20:20 7439-92-1 Selenium ND mg/kg 0.42 0.10 10 06/26/22 09:00 06/29/22 20:20 7782-49-2 Silver ND mg/kg 0.42 0.10 10 06/26/22 09:00 06/29/22 20:20 7440-22-4 EPA 7471 B Analytical Method: EPA 7471 B Preparation Method: METHOD Pace Analytical Gulf Coast Mercury 0.039 mg/kg 0.013 0.0053 1 06/24/2211:30 06/27/2212:36 7439-97-6 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND mg/kg 0.39 0.14 1 06/23/2217:52 06/29/2219:45 83-32-9 Acenaphthylene ND mg/kg 0.39 0.14 1 06/23/2217:52 06/29/2219:45 208-96-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 Sample: UT-3 Lab ID: 92611001001 Collected: 06/20/22 14:20 Received: 06/21/22 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Aniline ND mg/kg 0.39 0.15 1 06/23/22 17:52 06/29/22 19:45 62-53-3 Anthracene ND mg/kg 0.39 0.13 1 06/23/22 17:52 06/29/22 19:45 120-12-7 Benzo(a)anthracene ND mg/kg 0.39 0.13 1 06/23/22 17:52 06/29/22 19:45 56-55-3 Benzo(a)pyrene ND mg/kg 0.39 0.14 1 06/23/22 17:52 06/29/22 19:45 50-32-8 Benzo(b)fluoranthene ND mg/kg 0.39 0.13 1 06/23/22 17:52 06/29/22 19:45 205-99-2 Benzo(g,h,i)perylene ND mg/kg 0.39 0.15 1 06/23/22 17:52 06/29/22 19:45 191-24-2 Benzo(k)fluoranthene ND mg/kg 0.39 0.14 1 06/23/22 17:52 06/29/22 19:45 207-08-9 Benzoic Acid ND mg/kg 2.0 0.85 1 06/23/22 17:52 06/29/22 19:45 65-85-0 Benzyl alcohol ND mg/kg 0.79 0.30 1 06/23/22 17:52 06/29/22 19:45 100-51-6 4-Bromophenylphenyl ether ND mg/kg 0.39 0.15 1 06/23/22 17:52 06/29/22 19:45 101-55-3 Butylbenzylphthalate ND mg/kg 0.39 0.17 1 06/23/22 17:52 06/29/22 19:45 85-68-7 4-Chloro-3-methyl phenol ND mg/kg 0.79 0.28 1 06/23/22 17:52 06/29/22 19:45 59-50-7 4-Chloroaniline ND mg/kg 0.79 0.31 1 06/23/22 17:52 06/29/22 19:45 106-47-8 bis(2-Chloroethoxy)methane ND mg/kg 0.39 0.16 1 06/23/22 17:52 06/29/22 19:45 111-91-1 bis(2-Chloroethyl) ether ND mg/kg 0.39 0.15 1 06/23/22 17:52 06/29/22 19:45 111-44-4 2-Chloronaphthalene ND mg/kg 0.39 0.16 1 06/23/22 17:52 06/29/22 19:45 91-58-7 2-Chlorophenol ND mg/kg 0.39 0.15 1 06/23/22 17:52 06/29/22 19:45 95-57-8 4-Chlorophenylphenyl ether ND mg/kg 0.39 0.15 1 06/23/22 17:52 06/29/22 19:45 7005-72-3 Chrysene ND mg/kg 0.39 0.14 1 06/23/22 17:52 06/29/22 19:45 218-01-9 Dibenz(a,h)anthracene ND mg/kg 0.39 0.15 1 06/23/22 17:52 06/29/22 19:45 53-70-3 Dibenzofuran ND mg/kg 0.39 0.14 1 06/23/22 17:52 06/29/22 19:45 132-64-9 1,2-Dichlorobenzene ND mg/kg 0.39 0.14 1 06/23/22 17:52 06/29/22 19:45 95-50-1 1,3-Dichlorobenzene ND mg/kg 0.39 0.14 1 06/23/22 17:52 06/29/22 19:45 541-73-1 1,4-Dichlorobenzene ND mg/kg 0.39 0.15 1 06/23/22 17:52 06/29/22 19:45 106-46-7 3,3'-Dichlorobenzidine ND mg/kg 0.79 0.27 1 06/23/22 17:52 06/29/22 19:45 91-94-1 IL 2,4-Dichlorophenol ND mg/kg 0.39 0.15 1 06/23/22 17:52 06/29/22 19:45 120-83-2 Diethylphthalate ND mg/kg 0.39 0.14 1 06/23/22 17:52 06/29/22 19:45 84-66-2 2,4-Dimethylphenol ND mg/kg 0.39 0.16 1 06/23/22 17:52 06/29/22 19:45 105-67-9 Dimethylphthalate ND mg/kg 0.39 0.14 1 06/23/22 17:52 06/29/22 19:45 131-11-3 Di-n-butylphthalate ND mg/kg 0.39 0.13 1 06/23/22 17:52 06/29/22 19:45 84-74-2 4,6-Dinitro-2-methyl phenol ND mg/kg 0.79 0.37 1 06/23/22 17:52 06/29/22 19:45 534-52-1 2,4-Dinitrophenol ND mg/kg 2.0 1.2 1 06/23/22 17:52 06/29/22 19:45 51-28-5 2,4-Dinitrotoluene ND mg/kg 0.39 0.15 1 06/23/22 17:52 06/29/22 19:45 121-14-2 2,6-Dinitrotoluene ND mg/kg 0.39 0.14 1 06/23/22 17:52 06/29/22 19:45 606-20-2 Di-n-octylphthalate ND mg/kg 0.39 0.16 1 06/23/22 17:52 06/29/22 19:45 117-84-0 bis(2- Ethyl hexyl)phthalate ND mg/kg 0.39 0.15 1 06/23/22 17:52 06/29/22 19:45 117-81-7 Fluoranthene ND mg/kg 0.39 0.13 1 06/23/22 17:52 06/29/22 19:45 206-44-0 Fluorene ND mg/kg 0.39 0.14 1 06/23/22 17:52 06/29/22 19:45 86-73-7 Hexachloro-1,3-butadiene ND mg/kg 0.39 0.17 1 06/23/22 17:52 06/29/22 19:45 87-68-3 Hexachlorobenzene ND mg/kg 0.39 0.15 1 06/23/22 17:52 06/29/22 19:45 118-74-1 Hexachlorocyclopentadiene ND mg/kg 0.39 0.23 1 06/23/22 17:52 06/29/22 19:45 77-47-4 L2,v2 Hexachloroethane ND mg/kg 0.39 0.15 1 06/23/22 17:52 06/29/22 19:45 67-72-1 Indeno(1,2,3-cd)pyrene ND mg/kg 0.39 0.16 1 06/23/22 17:52 06/29/22 19:45 193-39-5 Isophorone ND mg/kg 0.39 0.18 1 06/23/22 17:52 06/29/22 19:45 78-59-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 Sample: UT-3 Lab ID: 92611001001 Collected: 06/20/22 14:20 Received: 06/21/22 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 1-Methylnaphthalene ND mg/kg 0.39 0.14 1 06/23/22 17:52 06/29/22 19:45 90-12-0 2-Methylnaphthalene ND mg/kg 0.39 0.16 1 06/23/22 17:52 06/29/22 19:45 91-57-6 2-Methylphenol(o-Cresol) ND mg/kg 0.39 0.16 1 06/23/22 17:52 06/29/22 19:45 95-48-7 3&4-Methyl phenol (m&p Cresol) ND mg/kg 0.39 0.16 1 06/23/22 17:52 06/29/22 19:45 15831-10-4 Naphthalene ND mg/kg 0.39 0.13 1 06/23/22 17:52 06/29/22 19:45 91-20-3 2-Nitroaniline ND mg/kg 2.0 0.32 1 06/23/22 17:52 06/29/22 19:45 88-74-4 3-Nitroaniline ND mg/kg 2.0 0.31 1 06/23/22 17:52 06/29/22 19:45 99-09-2 4-Nitroaniline ND mg/kg 0.79 0.30 1 06/23/22 17:52 06/29/22 19:45 100-01-6 Nitrobenzene ND mg/kg 0.39 0.18 1 06/23/22 17:52 06/29/22 19:45 98-95-3 2-Nitrophenol ND mg/kg 0.39 0.17 1 06/23/22 17:52 06/29/22 19:45 88-75-5 4-Nitrophenol ND mg/kg 2.0 0.76 1 06/23/22 17:52 06/29/22 19:45 100-02-7 N-Nitrosodimethylamine ND mg/kg 0.39 0.13 1 06/23/22 17:52 06/29/22 19:45 62-75-9 N-Nitroso-di-n-propylamine ND mg/kg 0.39 0.15 1 06/23/22 17:52 06/29/22 19:45 621-64-7 N-Nitrosodiphenylamine ND mg/kg 0.39 0.14 1 06/23/22 17:52 06/29/22 19:45 86-30-6 2,2'-Oxybis(1-chloropropane) ND mg/kg 0.39 0.19 1 06/23/22 17:52 06/29/22 19:45 108-60-1 Pentachlorophenol ND mg/kg 0.79 0.39 1 06/23/22 17:52 06/29/22 19:45 87-86-5 Phenanthrene ND mg/kg 0.39 0.13 1 06/23/22 17:52 06/29/22 19:45 85-01-8 Phenol ND mg/kg 0.39 0.18 1 06/23/22 17:52 06/29/22 19:45 108-95-2 Pyrene ND mg/kg 0.39 0.16 1 06/23/22 17:52 06/29/22 19:45 129-00-0 Pyridine ND mg/kg 0.39 0.12 1 06/23/22 17:52 06/29/22 19:45 110-86-1 1,2,4-Trichlorobenzene ND mg/kg 0.39 0.16 1 06/23/22 17:52 06/29/22 19:45 120-82-1 2,4,5-Trichlorophenol ND mg/kg 0.39 0.18 1 06/23/22 17:52 06/29/22 19:45 95-95-4 2,4,6-Trichlorophenol ND mg/kg 0.39 0.16 1 06/23/22 17:52 06/29/22 19:45 88-06-2 Surrogates Nitrobenzene-d5 (S) 56 % 21-130 1 06/23/22 17:52 06/29/22 19:45 4165-60-0 2-Fluorobiphenyl (S) 61 % 19-130 1 06/23/22 17:52 06/29/22 19:45 321-60-8 Terphenyl-d14 (S) 64 % 15-130 1 06/23/22 17:52 06/29/22 19:45 1718-51-0 Phenol-d6 (S) 56 % 18-130 1 06/23/22 17:52 06/29/22 19:45 13127-88-3 2-Fluorophenol (S) 51 % 18-130 1 06/23/22 17:52 06/29/22 19:45 367-12-4 2,4,6-Tribromophenol (S) 60 % 18-130 1 06/23/22 17:52 06/29/22 19:45 118-79-6 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Acetone ND mg/kg 0.14 0.045 1 06/22/22 23:29 06/23/22 06:16 67-64-1 Benzene ND mg/kg 0.0069 0.0028 1 06/22/22 23:29 06/23/22 06:16 71-43-2 Bromobenzene ND mg/kg 0.0069 0.0023 1 06/22/22 23:29 06/23/22 06:16 108-86-1 Bromochloromethane ND mg/kg 0.0069 0.0021 1 06/22/22 23:29 06/23/22 06:16 74-97-5 Bromodichloromethane ND mg/kg 0.0069 0.0027 1 06/22/22 23:29 06/23/22 06:16 75-27-4 Bromoform ND mg/kg 0.0069 0.0024 1 06/22/22 23:29 06/23/22 06:16 75-25-2 Bromomethane ND mg/kg 0.014 0.011 1 06/22/22 23:29 06/23/22 06:16 74-83-9 IK 2-Butanone (MEK) 0.046J mg/kg 0.14 0.033 1 06/22/22 23:29 06/23/22 06:16 78-93-3 n-Butylbenzene ND mg/kg 0.0069 0.0033 1 06/22/22 23:29 06/23/22 06:16 104-51-8 sec-Butylbenzene ND mg/kg 0.0069 0.0031 1 06/22/22 23:29 06/23/22 06:16 135-98-8 tert-Butyl benzene ND mg/kg 0.0069 0.0025 1 06/22/22 23:29 06/23/22 06:16 98-06-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 Sample: UT-3 Lab ID: 92611001001 Collected: 06/20/22 14:20 Received: 06/21/22 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Carbon tetrachloride ND mg/kg 0.0069 0.0026 1 06/22/22 23:29 06/23/22 06:16 56-23-5 Chlorobenzene ND mg/kg 0.0069 0.0013 1 06/22/22 23:29 06/23/22 06:16 108-90-7 Chloroethane ND mg/kg 0.014 0.0054 1 06/22/22 23:29 06/23/22 06:16 75-00-3 Chloroform ND mg/kg 0.0069 0.0042 1 06/22/22 23:29 06/23/22 06:16 67-66-3 Chloromethane ND mg/kg 0.014 0.0058 1 06/22/22 23:29 06/23/22 06:16 74-87-3 2-Chlorotoluene ND mg/kg 0.0069 0.0025 1 06/22/22 23:29 06/23/22 06:16 95-49-8 4-Chlorotoluene ND mg/kg 0.0069 0.0012 1 06/22/22 23:29 06/23/22 06:16 106-43-4 1,2-Dibromo-3-chloropropane ND mg/kg 0.0069 0.0027 1 06/22/22 23:29 06/23/22 06:16 96-12-8 Dibromochloromethane ND mg/kg 0.0069 0.0039 1 06/22/22 23:29 06/23/22 06:16 124-48-1 1,2-Dibromoethane (EDB) ND mg/kg 0.0069 0.0031 1 06/22/22 23:29 06/23/22 06:16 106-93-4 Dibromomethane ND mg/kg 0.0069 0.0015 1 06/22/22 23:29 06/23/22 06:16 74-95-3 1,2-Dichlorobenzene ND mg/kg 0.0069 0.0025 1 06/22/22 23:29 06/23/22 06:16 95-50-1 1,3-Dichlorobenzene ND mg/kg 0.0069 0.0022 1 06/22/22 23:29 06/23/22 06:16 541-73-1 1,4-Dichlorobenzene ND mg/kg 0.0069 0.0018 1 06/22/22 23:29 06/23/22 06:16 106-46-7 Dichlorodifluoromethane ND mg/kg 0.014 0.0030 1 06/22/22 23:29 06/23/22 06:16 75-71-8 1,1-Dichloroethane ND mg/kg 0.0069 0.0029 1 06/22/22 23:29 06/23/22 06:16 75-34-3 1,2-Dichloroethane ND mg/kg 0.0069 0.0046 1 06/22/22 23:29 06/23/22 06:16 107-06-2 1,1-Dichloroethene ND mg/kg 0.0069 0.0029 1 06/22/22 23:29 06/23/22 06:16 75-35-4 cis-1,2-Dichloroethene ND mg/kg 0.0069 0.0024 1 06/22/22 23:29 06/23/22 06:16 156-59-2 trans-1,2-Dichloroethene ND mg/kg 0.0069 0.0024 1 06/22/22 23:29 06/23/22 06:16 156-60-5 1,2-Dichloropropane ND mg/kg 0.0069 0.0021 1 06/22/22 23:29 06/23/22 06:16 78-87-5 1,3-Dichloropropane ND mg/kg 0.0069 0.0022 1 06/22/22 23:29 06/23/22 06:16 142-28-9 2,2-Dichloropropane ND mg/kg 0.0069 0.0023 1 06/22/22 23:29 06/23/22 06:16 594-20-7 1,1-Dichloropropene ND mg/kg 0.0069 0.0033 1 06/22/22 23:29 06/23/22 06:16 563-58-6 cis-1,3-Dichloropropene ND mg/kg 0.0069 0.0019 1 06/22/22 23:29 06/23/22 06:16 10061-01-5 trans- 1,3-Dichloropropene ND mg/kg 0.0069 0.0024 1 06/22/22 23:29 06/23/22 06:16 10061-02-6 Diisopropyl ether ND mg/kg 0.0069 0.0019 1 06/22/22 23:29 06/23/22 06:16 108-20-3 Ethylbenzene ND mg/kg 0.0069 0.0032 1 06/22/22 23:29 06/23/22 06:16 100-41-4 Hexachloro-1,3-butadiene ND mg/kg 0.014 0.011 1 06/22/22 23:29 06/23/22 06:16 87-68-3 2-Hexanone ND mg/kg 0.069 0.0067 1 06/22/22 23:29 06/23/22 06:16 591-78-6 Isopropylbenzene (Cumene) ND mg/kg 0.0069 0.0024 1 06/22/22 23:29 06/23/22 06:16 98-82-8 p-Isopropyltoluene ND mg/kg 0.0069 0.0034 1 06/22/22 23:29 06/23/22 06:16 99-87-6 Methylene Chloride ND mg/kg 0.028 0.019 1 06/22/22 23:29 06/23/22 06:16 75-09-2 4-Methyl-2-pentanone (MIBK) ND mg/kg 0.069 0.0067 1 06/22/22 23:29 06/23/22 06:16 108-10-1 Methyl-tert-butyl ether ND mg/kg 0.0069 0.0026 1 06/22/22 23:29 06/23/22 06:16 1634-04-4 Naphthalene ND mg/kg 0.0069 0.0037 1 06/22/22 23:29 06/23/22 06:16 91-20-3 n-Propylbenzene ND mg/kg 0.0069 0.0025 1 06/22/22 23:29 06/23/22 06:16 103-65-1 Styrene ND mg/kg 0.0069 0.0018 1 06/22/22 23:29 06/23/22 06:16 100-42-5 1,1,1,2-Tetrachloroethane ND mg/kg 0.0069 0.0027 1 06/22/22 23:29 06/23/22 06:16 630-20-6 1,1,2,2-Tetrachloroethane ND mg/kg 0.0069 0.0018 1 06/22/22 23:29 06/23/22 06:16 79-34-5 Tetrachloroethene ND mg/kg 0.0069 0.0022 1 06/22/22 23:29 06/23/22 06:16 127-18-4 Toluene ND mg/kg 0.0069 0.0020 1 06/22/22 23:29 06/23/22 06:16 108-88-3 1,2,3-Trichlorobenzene ND mg/kg 0.0069 0.0056 1 06/22/22 23:29 06/23/22 06:16 87-61-6 1,2,4-Trichlorobenzene ND mg/kg 0.0069 0.0058 1 06/22/22 23:29 06/23/22 06:16 120-82-1 REPORT OF LABORATORY ANALYSIS L1 v2,v3 IK IK This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 Sample: UT-3 Lab ID: 92611001001 Collected: 06/20/22 14:20 Received: 06/21/22 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Total Solids 2540 G-2011 Total Solids Wet Chemistry 7199 Chromium, Hexavalent Date: 07/21 /2022 05:23 PM Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte ND mg/kg 0.0069 0.0036 1 06/22/22 23:29 06/23/22 06:16 71-55-6 ND mg/kg 0.0069 0.0023 1 06/22/22 23:29 06/23/22 06:16 79-00-5 ND mg/kg 0.0069 0.0018 1 06/22/22 23:29 06/23/22 06:16 79-01-6 ND mg/kg 0.0069 0.0038 1 06/22/22 23:29 06/23/22 06:16 75-69-4 ND mg/kg 0.0069 0.0035 1 06/22/22 23:29 06/23/22 06:16 96-18-4 ND mg/kg 0.0069 0.0019 1 06/22/22 23:29 06/23/22 06:16 95-63-6 ND mg/kg 0.0069 0.0023 1 06/22/22 23:29 06/23/22 06:16 108-67-8 ND mg/kg 0.069 0.0051 1 06/22/22 23:29 06/23/22 06:16 108-05-4 ND mg/kg 0.014 0.0035 1 06/22/22 23:29 06/23/22 06:16 75-01-4 ND mg/kg 0.014 0.0040 1 06/22/22 23:29 06/23/22 06:16 1330-20-7 ND mg/kg 0.014 0.0047 1 06/22/22 23:29 06/23/22 06:16 179601-23-1 ND mg/kg 0.0069 0.0031 1 06/22/22 23:29 06/23/22 06:16 95-47-6 101 % 70-130 1 06/22/22 23:29 06/23/22 06:16 2037-26-5 101 % 69-134 1 06/22/22 23:29 06/23/22 06:16 460-00-4 98 % 70-130 1 06/22/22 23:29 06/23/22 06:16 17060-07-0 Analytical Method: SW-846 Pace Analytical Services - Charlotte 16.6 % 0.10 0.10 1 06/22/2217:17 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet 87.1 % 1 06/25/2216:49 06/25/2217:12 Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet ND mg/kg 1.15 0.293 1 07/13/2215:35 07/15/2217:18 18540-29-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 Page 10 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 Sample: DUP-3 Lab ID: 92611001002 Collected: 06/20/22 00:00 Received: 06/21/22 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual OP Pesticides 8141 B Analytical Method: EPA 8141 B Preparation Method: 3546 Pace National - Mt. Juliet Azinphos, methyl (Guthion) ND mg/kg 0.112 0.0356 1 06/27/22 03:37 06/29/22 21:15 86-50-0 Bolstar ND mg/kg 0.112 0.0167 1 06/27/22 03:37 06/29/22 21:15 35400-43-2 Chlorpyrifos ND mg/kg 0.112 0.0176 1 06/27/22 03:37 06/29/22 21:15 2921-88-2 Coumaphos ND mg/kg 0.112 0.0272 1 06/27/22 03:37 06/29/22 21:15 56-72-4 Total Demeton ND mg/kg 0.0784 0.00654 1 06/27/22 03:37 06/29/22 21:15 8065-48-3 Diazinon ND mg/kg 0.112 0.0252 1 06/27/22 03:37 06/29/22 21:15 333-41-5 Dichlorvos ND mg/kg 0.112 0.0336 1 06/27/22 03:37 06/29/22 21:15 62-73-7 Dimethoate ND mg/kg 0.112 0.0374 1 06/27/22 03:37 06/29/22 21:15 60-51-5 Disulfoton ND mg/kg 0.112 0.0284 1 06/27/22 03:37 06/29/22 21:15 298-04-4 EPN (ENT) ND mg/kg 0.112 0.0309 1 06/27/22 03:37 06/29/22 21:15 2104-64-5 Ethoprop ND mg/kg 0.112 0.0132 1 06/27/22 03:37 06/29/22 21:15 13194-48-4 Parathion (Ethyl parathion) ND mg/kg 0.112 0.0184 1 06/27/22 03:37 06/29/22 21:15 56-38-2 Fensulfothion ND mg/kg 0.112 0.0395 1 06/27/22 03:37 06/29/22 21:15 115-90-2 Fenthion ND mg/kg 0.112 0.0149 1 06/27/22 03:37 06/29/22 21:15 55-38-9 Malathion ND mg/kg 0.112 0.0200 1 06/27/22 03:37 06/29/22 21:15 121-75-5 Merphos ND mg/kg 0.112 0.0260 1 06/27/22 03:37 06/29/22 21:15 150-50-5 Methyl parathion ND mg/kg 0.112 0.0227 1 06/27/22 03:37 06/29/22 21:15 298-00-0 Mevinphos ND mg/kg 0.112 0.0257 1 06/27/22 03:37 06/29/22 21:15 7786-34-7 Naled ND mg/kg 0.112 0.0537 1 06/27/22 03:37 06/29/22 21:15 300-76-5 Phorate ND mg/kg 0.112 0.0235 1 06/27/22 03:37 06/29/22 21:15 298-02-2 Ronnel ND mg/kg 0.112 0.0167 1 06/27/22 03:37 06/29/22 21:15 299-84-3 Stirophos (Tetrachlorvinphos) ND mg/kg 0.112 0.0199 1 06/27/22 03:37 06/29/22 21:15 22248-79-9 Sulfotepp (ThiodiphosphoricAc ND mg/kg 0.112 0.0110 1 06/27/22 03:37 06/29/22 21:15 3689-24-5 TEPP ND mg/kg 1.12 0.176 1 06/27/22 03:37 06/29/22 21:15 107-49-3 Tokuthion (Prothiofos) ND mg/kg 0.112 0.0168 1 06/27/22 03:37 06/29/22 21:15 34643-46-4 Trichloronate ND mg/kg 0.112 0.0225 1 06/27/22 03:37 06/29/22 21:15 327-98-0 Surrogates Triphenylphosphate (S) 66.6 % 36.0-121 1 06/27/22 03:37 06/29/22 21:15 115-86-6 Chlorinated Herb. (GC) 8151 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND mg/kg 0.0784 0.00786 1 06/30/22 21:57 07/03/22 06:58 94-75-7 LO Dalapon ND mg/kg 0.0784 0.0126 1 06/30/22 21:57 07/03/22 06:58 127-20-8 2,4-DB ND mg/kg 0.0784 0.0332 1 06/30/22 21:57 07/03/22 06:58 94-82-6 Dicamba ND mg/kg 0.0784 0.0176 1 06/30/22 21:57 07/03/22 06:58 1918-00-9 LO Dichloroprop ND mg/kg 0.0784 0.0274 1 06/30/22 21:57 07/03/22 06:58 15165-67-0 LO Dinoseb ND mg/kg 0.0784 0.00780 1 06/30/22 21:57 07/03/22 06:58 88-85-7 MCPA ND mg/kg 7.28 0.496 1 06/30/22 21:57 07/03/22 06:58 94-74-6 LO MCPP ND mg/kg 7.28 0.411 1 06/30/22 21:57 07/03/22 06:58 7085-19-0 2,4,5-T ND mg/kg 0.0784 0.00954 1 06/30/22 21:57 07/03/22 06:58 93-76-5 LO 2,4,5-TP (Silvex) ND mg/kg 0.0784 0.0120 1 06/30/22 21:57 07/03/22 06:58 93-72-1 LO Surrogates 2,4-DCAA (S) 70.9 % 22.0-132 1 06/30/22 21:57 07/03/22 06:58 19719-28-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 Sample: DUP-3 Lab ID: 92611001002 Collected: 06/20/22 00:00 Received: 06/21/22 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 B Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Aldrin ND mg/kg 0.023 0.0092 10 06/24/22 16:02 06/29/22 09:55 309-00-2 alpha-BHC ND mg/kg 0.023 0.0099 10 06/24/22 16:02 06/29/22 09:55 319-84-6 beta-BHC ND mg/kg 0.023 0.011 10 06/24/22 16:02 06/29/22 09:55 319-85-7 delta-BHC ND mg/kg 0.023 0.011 10 06/24/22 16:02 06/29/22 09:55 319-86-8 gamma-BHC (Lindane) ND mg/kg 0.023 0.0091 10 06/24/22 16:02 06/29/22 09:55 58-89-9 Chlordane (Technical) ND mg/kg 0.11 0.099 10 06/24/22 16:02 06/29/22 09:55 57-74-9 4,4'-DDD ND mg/kg 0.023 0.010 10 06/24/22 16:02 06/29/22 09:55 72-54-8 4,4'-DDE ND mg/kg 0.023 0.011 10 06/24/22 16:02 06/29/22 09:55 72-55-9 4,4'-DDT ND mg/kg 0.023 0.010 10 06/24/22 16:02 06/29/22 09:55 50-29-3 Dieldrin ND mg/kg 0.023 0.0099 10 06/24/22 16:02 06/29/22 09:55 60-57-1 Endosulfan I ND mg/kg 0.023 0.0098 10 06/24/22 16:02 06/29/22 09:55 959-98-8 Endosulfan II ND mg/kg 0.023 0.010 10 06/24/22 16:02 06/29/22 09:55 33213-65-9 Endosulfan sulfate ND mg/kg 0.023 0.013 10 06/24/22 16:02 06/29/22 09:55 1031-07-8 Endrin ND mg/kg 0.023 0.011 10 06/24/22 16:02 06/29/22 09:55 72-20-8 Endrin aldehyde ND mg/kg 0.023 0.015 10 06/24/22 16:02 06/29/22 09:55 7421-93-4 Endrin ketone ND mg/kg 0.023 0.013 10 06/24/22 16:02 06/29/22 09:55 53494-70-5 Heptachlor ND mg/kg 0.023 0.011 10 06/24/22 16:02 06/29/22 09:55 76-44-8 Heptachlor epoxide ND mg/kg 0.023 0.0090 10 06/24/22 16:02 06/29/22 09:55 1024-57-3 Hexachlorobenzene ND mg/kg 0.023 0.0094 10 06/24/22 16:02 06/29/22 09:55 118-74-1 Methoxychlor ND mg/kg 0.057 0.028 10 06/24/22 16:02 06/29/22 09:55 72-43-5 Mirex ND mg/kg 0.057 0.025 10 06/24/22 16:02 06/29/22 09:55 2385-85-5 Toxaphene ND mg/kg 0.080 0.061 10 06/24/22 16:02 06/29/22 09:55 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 0 % 10-133 10 06/24/22 16:02 06/29/22 09:55 877-09-8 D3,S4 Decachlorobiphenyl (S) 0 % 10-146 10 06/24/22 16:02 06/29/22 09:55 2051-24-3 S4 EPA 6020B Analytical Method: EPA 6020E Preparation Method: EPA 3050B Pace Analytical Gulf Coast Arsenic 2.05 mg/kg 0.36 0.091 10 06/26/22 09:00 06/29/22 20:24 7440-38-2 Barium 128 mg/kg 0.36 0.091 10 06/26/22 09:00 06/29/22 20:24 7440-39-3 Cadmium ND mg/kg 0.36 0.091 10 06/26/22 09:00 06/29/22 20:24 7440-43-9 Chromium 32.4 mg/kg 0.36 0.091 10 06/26/22 09:00 06/29/22 20:24 7440-47-3 Lead 13.0 mg/kg 0.36 0.091 10 06/26/22 09:00 06/29/22 20:24 7439-92-1 Selenium ND mg/kg 0.36 0.091 10 06/26/22 09:00 06/29/22 20:24 7782-49-2 Silver ND mg/kg 0.36 0.091 10 06/26/22 09:00 06/29/22 20:24 7440-22-4 EPA 7471 B Analytical Method: EPA 7471 B Preparation Method: METHOD Pace Analytical Gulf Coast Mercury 0.030 mg/kg 0.013 0.0053 1 06/24/2211:30 06/27/2212:39 7439-97-6 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/29/22 20:13 83-32-9 Acenaphthylene ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/29/22 20:13 208-96-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 Sample: DUP-3 Lab ID: 92611001002 Collected: 06/20/22 00:00 Received: 06/21/22 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Aniline ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/29/22 20:13 62-53-3 Anthracene ND mg/kg 0.38 0.12 1 06/23/22 17:52 06/29/22 20:13 120-12-7 Benzo(a)anthracene ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/29/22 20:13 56-55-3 Benzo(a)pyrene ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/29/22 20:13 50-32-8 Benzo(b)fluoranthene ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/29/22 20:13 205-99-2 Benzo(g,h,i)perylene ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/29/22 20:13 191-24-2 Benzo(k)fluoranthene ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/29/22 20:13 207-08-9 Benzoic Acid ND mg/kg 1.9 0.81 1 06/23/22 17:52 06/29/22 20:13 65-85-0 Benzyl alcohol ND mg/kg 0.76 0.29 1 06/23/22 17:52 06/29/22 20:13 100-51-6 4-Bromophenylphenyl ether ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/29/22 20:13 101-55-3 Butylbenzylphthalate ND mg/kg 0.38 0.16 1 06/23/22 17:52 06/29/22 20:13 85-68-7 4-Chloro-3-methyl phenol ND mg/kg 0.76 0.27 1 06/23/22 17:52 06/29/22 20:13 59-50-7 4-Chloroaniline ND mg/kg 0.76 0.30 1 06/23/22 17:52 06/29/22 20:13 106-47-8 bis(2-Chloroethoxy)methane ND mg/kg 0.38 0.16 1 06/23/22 17:52 06/29/22 20:13 111-91-1 bis(2-Chloroethyl) ether ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/29/22 20:13 111-44-4 2-Chloronaphthalene ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/29/22 20:13 91-58-7 2-Chlorophenol ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/29/22 20:13 95-57-8 4-Chlorophenylphenyl ether ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/29/22 20:13 7005-72-3 Chrysene ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/29/22 20:13 218-01-9 Dibenz(a,h)anthracene ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/29/22 20:13 53-70-3 Dibenzofuran ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/29/22 20:13 132-64-9 1,2-Dichlorobenzene ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/29/22 20:13 95-50-1 1,3-Dichlorobenzene ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/29/22 20:13 541-73-1 1,4-Dichlorobenzene ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/29/22 20:13 106-46-7 3,3'-Dichlorobenzidine ND mg/kg 0.76 0.26 1 06/23/22 17:52 06/29/22 20:13 91-94-1 2,4-Dichlorophenol ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/29/22 20:13 120-83-2 Diethylphthalate ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/29/22 20:13 84-66-2 2,4-Dimethylphenol ND mg/kg 0.38 0.16 1 06/23/22 17:52 06/29/22 20:13 105-67-9 Dimethylphthalate ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/29/22 20:13 131-11-3 Di-n-butylphthalate ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/29/22 20:13 84-74-2 4,6-Dinitro-2-methyl phenol ND mg/kg 0.76 0.35 1 06/23/22 17:52 06/29/22 20:13 534-52-1 2,4-Dinitrophenol ND mg/kg 1.9 1.2 1 06/23/22 17:52 06/29/22 20:13 51-28-5 2,4-Dinitrotoluene ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/29/22 20:13 121-14-2 2,6-Dinitrotoluene ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/29/22 20:13 606-20-2 Di-n-octylphthalate ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/29/22 20:13 117-84-0 bis(2- Ethyl hexyl)phthalate ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/29/22 20:13 117-81-7 Fluoranthene 0.27J mg/kg 0.38 0.13 1 06/23/22 17:52 06/29/22 20:13 206-44-0 Fluorene ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/29/22 20:13 86-73-7 Hexachloro-1,3-butadiene ND mg/kg 0.38 0.16 1 06/23/22 17:52 06/29/22 20:13 87-68-3 Hexachlorobenzene ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/29/22 20:13 118-74-1 Hexachlorocyclopentadiene ND mg/kg 0.38 0.22 1 06/23/22 17:52 06/29/22 20:13 77-47-4 Hexachloroethane ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/29/22 20:13 67-72-1 Indeno(1,2,3-cd)pyrene ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/29/22 20:13 193-39-5 Isophorone ND mg/kg 0.38 0.17 1 06/23/22 17:52 06/29/22 20:13 78-59-1 REPORT OF LABORATORY ANALYSIS IL L2.v2 This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 Sample: DUP-3 Lab ID: 92611001002 Collected: 06/20/22 00:00 Received: 06/21/22 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 1-Methylnaphthalene ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/29/22 20:13 90-12-0 2-Methylnaphthalene ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/29/22 20:13 91-57-6 2-Methylphenol(o-Cresol) ND mg/kg 0.38 0.16 1 06/23/22 17:52 06/29/22 20:13 95-48-7 3&4-Methyl phenol (m&p Cresol) ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/29/22 20:13 15831-10-4 Naphthalene ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/29/22 20:13 91-20-3 2-Nitroaniline ND mg/kg 1.9 0.31 1 06/23/22 17:52 06/29/22 20:13 88-74-4 3-Nitroaniline ND mg/kg 1.9 0.30 1 06/23/22 17:52 06/29/22 20:13 99-09-2 4-Nitroaniline ND mg/kg 0.76 0.29 1 06/23/22 17:52 06/29/22 20:13 100-01-6 Nitrobenzene ND mg/kg 0.38 0.18 1 06/23/22 17:52 06/29/22 20:13 98-95-3 2-Nitrophenol ND mg/kg 0.38 0.16 1 06/23/22 17:52 06/29/22 20:13 88-75-5 4-Nitrophenol ND mg/kg 1.9 0.73 1 06/23/22 17:52 06/29/22 20:13 100-02-7 N-Nitrosodimethylamine ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/29/22 20:13 62-75-9 N-Nitroso-di-n-propylamine ND mg/kg 0.38 0.14 1 06/23/22 17:52 06/29/22 20:13 621-64-7 N-Nitrosodiphenylamine ND mg/kg 0.38 0.13 1 06/23/22 17:52 06/29/22 20:13 86-30-6 2,2'-Oxybis(1-chloropropane) ND mg/kg 0.38 0.18 1 06/23/22 17:52 06/29/22 20:13 108-60-1 Pentachlorophenol ND mg/kg 0.76 0.37 1 06/23/22 17:52 06/29/22 20:13 87-86-5 Phenanthrene 0.22J mg/kg 0.38 0.12 1 06/23/22 17:52 06/29/22 20:13 85-01-8 Phenol ND mg/kg 0.38 0.17 1 06/23/22 17:52 06/29/22 20:13 108-95-2 Pyrene 0.191 mg/kg 0.38 0.15 1 06/23/22 17:52 06/29/22 20:13 129-00-0 Pyridine ND mg/kg 0.38 0.12 1 06/23/22 17:52 06/29/22 20:13 110-86-1 1,2,4-Trichlorobenzene ND mg/kg 0.38 0.15 1 06/23/22 17:52 06/29/22 20:13 120-82-1 2,4,5-Trichlorophenol ND mg/kg 0.38 0.17 1 06/23/22 17:52 06/29/22 20:13 95-95-4 2,4,6-Trichlorophenol ND mg/kg 0.38 0.16 1 06/23/22 17:52 06/29/22 20:13 88-06-2 Surrogates Nitrobenzene-d5 (S) 63 % 21-130 1 06/23/22 17:52 06/29/22 20:13 4165-60-0 2-Fluorobiphenyl (S) 58 % 19-130 1 06/23/22 17:52 06/29/22 20:13 321-60-8 Terphenyl-d14 (S) 68 % 15-130 1 06/23/22 17:52 06/29/22 20:13 1718-51-0 Phenol-d6 (S) 61 % 18-130 1 06/23/22 17:52 06/29/22 20:13 13127-88-3 2-Fluorophenol (S) 53 % 18-130 1 06/23/22 17:52 06/29/22 20:13 367-12-4 2,4,6-Tribromophenol (S) 64 % 18-130 1 06/23/22 17:52 06/29/22 20:13 118-79-6 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Acetone ND mg/kg 0.14 0.045 1 06/22/22 23:29 06/23/22 06:34 67-64-1 Benzene ND mg/kg 0.0070 0.0028 1 06/22/22 23:29 06/23/22 06:34 71-43-2 Bromobenzene ND mg/kg 0.0070 0.0023 1 06/22/22 23:29 06/23/22 06:34 108-86-1 Bromochloromethane ND mg/kg 0.0070 0.0021 1 06/22/22 23:29 06/23/22 06:34 74-97-5 Bromodichloromethane ND mg/kg 0.0070 0.0027 1 06/22/22 23:29 06/23/22 06:34 75-27-4 Bromoform ND mg/kg 0.0070 0.0025 1 06/22/22 23:29 06/23/22 06:34 75-25-2 Bromomethane ND mg/kg 0.014 0.011 1 06/22/22 23:29 06/23/22 06:34 74-83-9 2-Butanone (MEK) 0.053J mg/kg 0.14 0.034 1 06/22/22 23:29 06/23/22 06:34 78-93-3 n-Butylbenzene ND mg/kg 0.0070 0.0033 1 06/22/22 23:29 06/23/22 06:34 104-51-8 sec-Butylbenzene ND mg/kg 0.0070 0.0031 1 06/22/22 23:29 06/23/22 06:34 135-98-8 tert-Butyl benzene ND mg/kg 0.0070 0.0025 1 06/22/22 23:29 06/23/22 06:34 98-06-6 REPORT OF LABORATORY ANALYSIS IK This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 Sample: DUP-3 Lab ID: 92611001002 Collected: 06/20/22 00:00 Received: 06/21/22 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Carbon tetrachloride ND mg/kg 0.0070 0.0026 1 06/22/22 23:29 06/23/22 06:34 56-23-5 Chlorobenzene ND mg/kg 0.0070 0.0013 1 06/22/22 23:29 06/23/22 06:34 108-90-7 Chloroethane ND mg/kg 0.014 0.0054 1 06/22/22 23:29 06/23/22 06:34 75-00-3 Chloroform ND mg/kg 0.0070 0.0042 1 06/22/22 23:29 06/23/22 06:34 67-66-3 Chloromethane ND mg/kg 0.014 0.0059 1 06/22/22 23:29 06/23/22 06:34 74-87-3 2-Chlorotoluene ND mg/kg 0.0070 0.0025 1 06/22/22 23:29 06/23/22 06:34 95-49-8 4-Chlorotoluene ND mg/kg 0.0070 0.0012 1 06/22/22 23:29 06/23/22 06:34 106-43-4 1,2-Dibromo-3-chloropropane ND mg/kg 0.0070 0.0027 1 06/22/22 23:29 06/23/22 06:34 96-12-8 Dibromochloromethane ND mg/kg 0.0070 0.0039 1 06/22/22 23:29 06/23/22 06:34 124-48-1 1,2-Dibromoethane (EDB) ND mg/kg 0.0070 0.0031 1 06/22/22 23:29 06/23/22 06:34 106-93-4 Dibromomethane ND mg/kg 0.0070 0.0015 1 06/22/22 23:29 06/23/22 06:34 74-95-3 1,2-Dichlorobenzene ND mg/kg 0.0070 0.0025 1 06/22/22 23:29 06/23/22 06:34 95-50-1 1,3-Dichlorobenzene ND mg/kg 0.0070 0.0022 1 06/22/22 23:29 06/23/22 06:34 541-73-1 1,4-Dichlorobenzene ND mg/kg 0.0070 0.0018 1 06/22/22 23:29 06/23/22 06:34 106-46-7 Dichlorodifluoromethane ND mg/kg 0.014 0.0030 1 06/22/22 23:29 06/23/22 06:34 75-71-8 1,1-Dichloroethane ND mg/kg 0.0070 0.0029 1 06/22/22 23:29 06/23/22 06:34 75-34-3 1,2-Dichloroethane ND mg/kg 0.0070 0.0046 1 06/22/22 23:29 06/23/22 06:34 107-06-2 1,1-Dichloroethene ND mg/kg 0.0070 0.0029 1 06/22/22 23:29 06/23/22 06:34 75-35-4 cis-1,2-Dichloroethene ND mg/kg 0.0070 0.0024 1 06/22/22 23:29 06/23/22 06:34 156-59-2 trans-1,2-Dichloroethene ND mg/kg 0.0070 0.0024 1 06/22/22 23:29 06/23/22 06:34 156-60-5 1,2-Dichloropropane ND mg/kg 0.0070 0.0021 1 06/22/22 23:29 06/23/22 06:34 78-87-5 1,3-Dichloropropane ND mg/kg 0.0070 0.0022 1 06/22/22 23:29 06/23/22 06:34 142-28-9 2,2-Dichloropropane ND mg/kg 0.0070 0.0023 1 06/22/22 23:29 06/23/22 06:34 594-20-7 1,1-Dichloropropene ND mg/kg 0.0070 0.0034 1 06/22/22 23:29 06/23/22 06:34 563-58-6 cis-1,3-Dichloropropene ND mg/kg 0.0070 0.0019 1 06/22/22 23:29 06/23/22 06:34 10061-01-5 trans- 1,3-Dichloropropene ND mg/kg 0.0070 0.0024 1 06/22/22 23:29 06/23/22 06:34 10061-02-6 Diisopropyl ether ND mg/kg 0.0070 0.0019 1 06/22/22 23:29 06/23/22 06:34 108-20-3 Ethylbenzene ND mg/kg 0.0070 0.0033 1 06/22/22 23:29 06/23/22 06:34 100-41-4 Hexachloro-1,3-butadiene ND mg/kg 0.014 0.011 1 06/22/22 23:29 06/23/22 06:34 87-68-3 2-Hexanone ND mg/kg 0.070 0.0067 1 06/22/22 23:29 06/23/22 06:34 591-78-6 Isopropylbenzene (Cumene) ND mg/kg 0.0070 0.0024 1 06/22/22 23:29 06/23/22 06:34 98-82-8 p-Isopropyltoluene ND mg/kg 0.0070 0.0034 1 06/22/22 23:29 06/23/22 06:34 99-87-6 Methylene Chloride ND mg/kg 0.028 0.019 1 06/22/22 23:29 06/23/22 06:34 75-09-2 4-Methyl-2-pentanone (MIBK) ND mg/kg 0.070 0.0067 1 06/22/22 23:29 06/23/22 06:34 108-10-1 Methyl-tert-butyl ether ND mg/kg 0.0070 0.0026 1 06/22/22 23:29 06/23/22 06:34 1634-04-4 Naphthalene ND mg/kg 0.0070 0.0037 1 06/22/22 23:29 06/23/22 06:34 91-20-3 n-Propylbenzene ND mg/kg 0.0070 0.0025 1 06/22/22 23:29 06/23/22 06:34 103-65-1 Styrene ND mg/kg 0.0070 0.0018 1 06/22/22 23:29 06/23/22 06:34 100-42-5 1,1,1,2-Tetrachloroethane ND mg/kg 0.0070 0.0027 1 06/22/22 23:29 06/23/22 06:34 630-20-6 1,1,2,2-Tetrachloroethane ND mg/kg 0.0070 0.0018 1 06/22/22 23:29 06/23/22 06:34 79-34-5 Tetrachloroethene ND mg/kg 0.0070 0.0022 1 06/22/22 23:29 06/23/22 06:34 127-18-4 Toluene ND mg/kg 0.0070 0.0020 1 06/22/22 23:29 06/23/22 06:34 108-88-3 1,2,3-Trichlorobenzene ND mg/kg 0.0070 0.0056 1 06/22/22 23:29 06/23/22 06:34 87-61-6 1,2,4-Trichlorobenzene ND mg/kg 0.0070 0.0059 1 06/22/22 23:29 06/23/22 06:34 120-82-1 REPORT OF LABORATORY ANALYSIS L1 v2 IK IK This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 Sample: DUP-3 Lab ID: 92611001002 Collected: 06/20/22 00:00 Received: 06/21/22 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Total Solids 2540 G-2011 Total Solids Wet Chemistry 7199 Chromium, Hexavalent Date: 07/21 /2022 05:23 PM Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte ND mg/kg 0.0070 0.0036 1 06/22/22 23:29 06/23/22 06:34 71-55-6 ND mg/kg 0.0070 0.0023 1 06/22/22 23:29 06/23/22 06:34 79-00-5 ND mg/kg 0.0070 0.0018 1 06/22/22 23:29 06/23/22 06:34 79-01-6 ND mg/kg 0.0070 0.0038 1 06/22/22 23:29 06/23/22 06:34 75-69-4 ND mg/kg 0.0070 0.0035 1 06/22/22 23:29 06/23/22 06:34 96-18-4 ND mg/kg 0.0070 0.0019 1 06/22/22 23:29 06/23/22 06:34 95-63-6 ND mg/kg 0.0070 0.0023 1 06/22/22 23:29 06/23/22 06:34 108-67-8 ND mg/kg 0.070 0.0051 1 06/22/22 23:29 06/23/22 06:34 108-05-4 ND mg/kg 0.014 0.0035 1 06/22/22 23:29 06/23/22 06:34 75-01-4 ND mg/kg 0.014 0.0040 1 06/22/22 23:29 06/23/22 06:34 1330-20-7 ND mg/kg 0.014 0.0048 1 06/22/22 23:29 06/23/22 06:34 179601-23-1 ND mg/kg 0.0070 0.0031 1 06/22/22 23:29 06/23/22 06:34 95-47-6 100 % 70-130 1 06/22/22 23:29 06/23/22 06:34 2037-26-5 100 % 69-134 1 06/22/22 23:29 06/23/22 06:34 460-00-4 97 % 70-130 1 06/22/22 23:29 06/23/22 06:34 17060-07-0 Analytical Method: SW-846 Pace Analytical Services - Charlotte 12.9 % 0.10 0.10 1 06/22/2217:17 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet 89.3 % 1 06/28/22 09:14 06/28/22 09:20 Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet ND mg/kg 1.12 0.285 1 07/13/2215:35 07/15/2217:24 18540-29-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 Page 16 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 QC Batch: 1882585 Analysis Method: EPA 8141 B QC Batch Method: 3546 Analysis Description: OP Pesticides 8141 B Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92611001001, 92611001002 METHOD BLANK: R3808945-1 Associated Lab Samples: 92611001001, 92611001002 Parameter Units Matrix: Blank Result Solid Reporting Limit MDL Analyzed Azinphos, methyl (Guthion) mg/kg ND 0.100 0.0318 06/27/22 11:41 Bolstar mg/kg ND 0.100 0.0149 06/27/22 11:41 Chlorpyrifos mg/kg ND 0.100 0.0157 06/27/22 11:41 Coumaphos mg/kg ND 0.100 0.0243 06/27/22 11:41 Total Demeton mg/kg ND 0.0700 0.00584 06/27/22 11:41 Diazinon mg/kg ND 0.100 0.0225 06/27/22 11:41 Dichlorvos mg/kg ND 0.100 0.0300 06/27/22 11:41 Dimethoate mg/kg ND 0.100 0.0334 06/27/22 11:41 Disulfoton mg/kg ND 0.100 0.0254 06/27/22 11:41 EPN (ENT) mg/kg ND 0.100 0.0276 06/27/22 11:41 Ethoprop mg/kg ND 0.100 0.0118 06/27/22 11:41 Parathion (Ethyl parathion) mg/kg ND 0.100 0.0164 06/27/22 11:41 Fensulfothion mg/kg ND 0.100 0.0353 06/27/22 11:41 Fenthion mg/kg ND 0.100 0.0133 06/27/22 11:41 Malathion mg/kg ND 0.100 0.0179 06/27/22 11:41 Merphos mg/kg ND 0.100 0.0232 06/27/22 11:41 Methyl parathion mg/kg ND 0.100 0.0203 06/27/22 11:41 Mevinphos mg/kg ND 0.100 0.0230 06/27/22 11:41 Naled mg/kg ND 0.100 0.0480 06/27/22 11:41 Phorate mg/kg ND 0.100 0.0210 06/27/22 11:41 Ronnel mg/kg ND 0.100 0.0149 06/27/22 11:41 Stirophos (Tetrachlorvinphos) mg/kg ND 0.100 0.0178 06/27/22 11:41 Sulfotepp (Thiodiphosphoric Ac mg/kg ND 0.100 0.00986 06/27/22 11:41 TEPP mg/kg ND 1.00 0.157 06/27/22 11:41 Tokuthion (Prothiofos) mg/kg ND 0.100 0.0150 06/27/22 11:41 Trichloronate mg/kg ND 0.100 0.0201 06/27/22 11:41 Triphenyl phosphate (S) % 89.5 36.0-121 06/27/22 11:41 LABORATORY CONTROL SAMPLE: R3808945-2 Qualifiers Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Azinphos, methyl (Guthion) mg/kg 0.333 0.351 105 58.0-125 Bolstar mg/kg 0.333 0.334 100 64.0-120 Chlorpyrifos mg/kg 0.333 0.327 98.2 62.0-120 Coumaphos mg/kg 0.333 0.348 105 60.0-120 Total Demeton mg/kg 0.167 0.167 100 59.0-120 Diazinon mg/kg 0.333 0.299 89.8 49.0-120 Dichlorvos mg/kg 0.333 0.260 78.1 37.0-120 Dimethoate mg/kg 0.333 0.322 96.7 46.0-127 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 LABORATORY CONTROL SAMPLE: R3808945-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Disulfoton mg/kg 0.333 0.329 98.8 60.0-121 EPN (ENT) mg/kg 0.333 0.339 102 60.0-121 Ethoprop mg/kg 0.333 0.333 100 59.0-120 Parathion (Ethyl parathion) mg/kg 0.333 0.335 101 62.0-120 Fensulfothion mg/kg 0.333 0.337 101 58.0-123 Fenthion mg/kg 0.333 0.337 101 61.0-121 Malathion mg/kg 0.333 0.316 94.9 59.0-120 Merphos mg/kg 0.333 0.286 85.9 59.0-120 Methyl parathion mg/kg 0.333 0.333 100 63.0-120 Mevinphos mg/kg 0.333 0.297 89.2 50.0-120 Naled mg/kg 0.333 0.252 75.7 10.0-125 Phorate mg/kg 0.333 0.315 94.6 60.0-120 Ronnel mg/kg 0.333 0.341 102 62.0-120 Stirophos (Tetrachlorvinphos) mg/kg 0.333 0.326 97.9 62.0-120 Sulfotepp (ThiodiphosphoricAc mg/kg 0.333 0.331 99.4 62.0-122 TEPP mg/kg 3.33 1.44 43.2 10.0-135 Tokuthion (Prothiofos) mg/kg 0.333 0.329 98.8 63.0-120 Trichloronate mg/kg 0.333 0.322 96.7 62.0-120 Triphenyl phosphate (S) % 90.1 36.0-121 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3809251-1 R3809251-2 MS MSD L1507762-01 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Azinphos, methyl (Guthion) mg/kg ND 0.325 0.325 0.231 0.260 71.1 80.0 10.0-160 11.8 22 Bolstar mg/kg ND 0.325 0.325 0.246 0.290 75.7 89.2 10.0-151 16.4 20 Chlorpyrifos mg/kg ND 0.325 0.325 0.263 0.303 80.9 93.2 12.0-149 14.1 20 Coumaphos mg/kg ND 0.325 0.325 0.263 0.294 80.9 90.5 10.0-160 11.1 22 Total Demeton mg/kg ND 0.163 0.163 0.130 0.148 79.8 90.8 10.0-160 12.9 23 Diazinon mg/kg ND 0.325 0.325 0.252 0.290 77.5 89.2 11.0-157 14.0 20 Dichlorvos mg/kg ND 0.325 0.325 0.341 0.397 105 122 10.0-160 15.2 24 Dimethoate mg/kg ND 0.325 0.325 0.266 0.295 81.8 90.8 10.0-150 10.3 27 Disulfoton mg/kg ND 0.325 0.325 0.254 0.290 78.2 89.2 12.0-155 13.2 20 EPN (ENT) mg/kg ND 0.325 0.325 0.246 0.275 75.7 84.6 10.0-159 11.1 20 Ethoprop mg/kg ND 0.325 0.325 0.266 0.304 81.8 93.5 11.0-156 13.3 20 Parathion (Ethyl parathion) mg/kg ND 0.325 0.325 0.261 0.293 80.3 90.2 10.0-147 11.6 20 Fensulfothion mg/kg ND 0.325 0.325 0.252 0.287 77.5 88.3 10.0-157 13.0 27 Fenthion mg/kg ND 0.325 0.325 0.262 0.297 80.6 91.4 13.0-155 12.5 20 Malathion mg/kg ND 0.325 0.325 0.259 0.283 79.7 87.1 13.0-137 8.86 21 Merphos mg/kg ND 0.325 0.325 0.163 0.191 50.2 58.8 10.0-147 15.8 26 Methyl parathion mg/kg ND 0.325 0.325 0.254 0.290 78.2 89.2 10.0-150 13.2 21 Mevinphos mg/kg ND 0.325 0.325 0.263 0.302 80.9 92.9 10.0-158 13.8 24 Naled mg/kg ND 0.325 0.325 ND ND 5.66 5.17 10.0-137 9.09 40 ML Phorate mg/kg ND 0.325 0.325 0.252 0.291 77.5 89.5 13.0-154 14.4 20 Ronnel mg/kg ND 0.325 0.325 0.263 0.303 80.9 93.2 14.0-149 14.1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3809251-1 R3809251-2 MS MSD L1507762-01 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Stirophos mg/kg ND 0.325 0.325 0.238 0.272 73.2 83.7 10.0-150 13.3 20 (Tetrachlorvinphos) Sulfotepp mg/kg ND 0.325 0.325 0.262 0.297 80.6 91.4 10.0-160 12.5 20 (Thiodiphosphoric Ac TEPP mg/kg ND 3.25 3.25 2.24 2.63 68.9 80.9 10.0-142 16.0 28 Tokuthion (Prothiofos) mg/kg ND 0.325 0.325 0.253 0.291 77.8 89.5 12.0-153 14.0 20 Trichloronate mg/kg ND 0.325 0.325 0.255 0.296 78.5 91.1 12.0-152 14.9 20 Triphenyl phosphate (S) % 68.9 77.2 36.0-121 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 QC Batch: 1888224 Analysis Method: EPA 8151 QC Batch Method: 8151A Analysis Description: Chlorinated Herb. (GC) 8151 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92611001001, 92611001002 METHOD BLANK: R3810583-1 Matrix: Solid Associated Lab Samples: 92611001001, 92611001002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 2,4-D mg/kg ND 0.0700 0.00702 07/02/22 23:21 Dalapon mg/kg ND 0.0700 0.0113 07/02/22 23:21 2,4-DB mg/kg ND 0.0700 0.0297 07/02/22 23:21 Dicamba mg/kg ND 0.0700 0.0157 07/02/22 23:21 Dichloroprop mg/kg ND 0.0700 0.0245 07/02/22 23:21 Dinoseb mg/kg ND 0.0700 0.00697 07/02/22 23:21 MCPA mg/kg ND 6.50 0.443 07/02/22 23:21 MCPP mg/kg ND 6.50 0.367 07/02/22 23:21 2,4,5-T mg/kg ND 0.0700 0.00852 07/02/22 23:21 2,4,5-TP (Silvex) mg/kg ND 0.0700 0.0107 07/02/22 23:21 2,4-DCAA (S) % 82.6 22.0-132 07/02/22 23:21 LABORATORY CONTROL SAMPLE: R3810583-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 2,4-D mg/kg 0.167 0.216 129 40.0-120 E,LO,P9 Dalapon mg/kg 0.167 0.125 74.9 15.0-120 2,4-DB mg/kg 0.167 0.188 113 25.0-143 E,P9 Dicamba mg/kg 0.167 0.225 135 43.0-120 E,LO,P9 Dichloroprop mg/kg 0.167 0.245 147 32.0-129 E,LO,P9 Dinoseb mg/kg 0.167 0.150 89.8 10.0-120 P9 MCPA mg/kg 16.7 25.0 150 31.0-121 E,L0,P9 MCPP mg/kg 16.7 17.7 106 28.0-133 E,P9 2,4,5-T mg/kg 0.167 0.233 140 41.0-120 E,L0,P9 2,4,5-TP (Silvex) mg/kg 0.167 0.241 144 42.0-120 E,L0,P9 2,4-DCAA (S) % 97.6 22.0-132 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3810583-3 R3810583-4 MS MSD L1509303-01 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 2,4-D mg/kg ND 0.171 0.173 0.153 0.171 89.7 98.8 10.0-160 10.9 24 Dalapon mg/kg ND 0.171 0.173 0.118 0.127 69.1 73.7 10.0-121 7.59 27 2,4-DB mg/kg ND 0.171 0.173 0.163 0.177 95.8 102 10.0-160 7.90 22 E Dicamba mg/kg ND 0.171 0.173 0.187 0.203 110 117 10.0-154 7.96 21 E,P9 Dichloroprop mg/kg ND 0.171 0.173 0.220 0.227 129 131 10.0-158 2.78 20 E,P9 Dinoseb mg/kg ND 0.171 0.173 0.108 0.117 63.0 67.7 10.0-120 8.29 40 P9 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: 10039-B WRIGHTS EXECUTIVE 92611001 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3810583-3 R3810583-4 MS MSD L1509303-01 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual MCPA mg/kg ND 17.1 17.3 22.1 23.9 130 138 10.0-160 7.64 40 E,P9 MCPP mg/kg ND 17.1 17.3 14.4 14.5 84.2 83.8 10.0-160 0.717 40 P9 2,4,5-T mg/kg ND 0.171 0.173 0.197 0.216 115 125 10.0-157 9.52 20 E,P9 2,4,5-TP (Silvex) mg/kg ND 0.171 0.173 0.160 0.175 93.9 101 10.0-156 8.64 20 E 2,4-DCAA (S) % 87.3 95.2 22.0-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 QC Batch: 743891 Analysis Method: EPA 6020B QC Batch Method: EPA 3050B Analysis Description: EPA 6020 Laboratory: Pace Analytical Gulf Coast Associated Lab Samples: 92611001001, 92611001002 METHOD BLANK: 2362684 Matrix: Solid Associated Lab Samples: 92611001001, 92611001002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Arsenic mg/kg ND 0.040 0.010 06/29/2219:52 P8 Barium mg/kg ND 0.040 0.010 06/29/2219:52 Cadmium mg/kg ND 0.040 0.010 06/29/2219:52 Chromium mg/kg ND 0.040 0.010 06/29/2219:52 Lead mg/kg ND 0.040 0.010 06/29/2219:52 Selenium mg/kg ND 0.040 0.010 06/29/2219:52 Silver mg/kg ND 0.040 0.010 06/29/2219:52 LABORATORY CONTROL SAMPLE & LCSD: 2362686 2362685 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Arsenic mg/kg 2 2.08 2.03 104 101 80-120 3 20 Barium mg/kg 2 2.00 2.21 100 110 80-120 10 20 Cadmium mg/kg 2 1.91 2.11 96 105 80-120 10 20 Chromium mg/kg 2 2.07 2.04 104 102 80-120 2 20 Lead mg/kg 2 2.07 2.30 104 115 80-120 10 20 Selenium mg/kg 0.4 0.41 0.41 102 102 80-120 0 20 Silver mg/kg 2 2.07 2.28 103 114 80-120 10 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 QC Batch: 743963 Analysis Method: EPA 7471 B QC Batch Method: METHOD Analysis Description: EPA 7471 B Laboratory: Pace Analytical Gulf Coast Associated Lab Samples: 92611001001, 92611001002 METHOD BLANK: 2363133 Matrix: Solid Associated Lab Samples: 92611001001, 92611001002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Mercury mg/kg ND 0.010 0.0040 06/27/2212:21 LABORATORY CONTROL SAMPLE & LCSD: 2363135 2363134 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Mercury mg/kg 0.25 0.24 0.27 97 108 80-120 10 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 QC Batch: 706373 Analysis Method: EPA 8260D QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92611001001, 92611001002 METHOD BLANK: 3685232 Associated Lab Samples: 92611001001, 92611001002 Parameter Units Matrix: Blank Result Solid Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 0.0019 06/23/22 04:47 1,1,1-Trichloroethane mg/kg ND 0.0050 0.0026 06/23/22 04:47 1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 0.0013 06/23/22 04:47 1,1,2-Trichloroethane mg/kg ND 0.0050 0.0017 06/23/22 04:47 1,1-Dichloroethane mg/kg ND 0.0050 0.0021 06/23/22 04:47 1,1-Dichloroethene mg/kg ND 0.0050 0.0021 06/23/22 04:47 1,1-Dichloropropene mg/kg ND 0.0050 0.0024 06/23/22 04:47 1,2,3-Trichlorobenzene mg/kg ND 0.0050 0.0040 06/23/22 04:47 1,2,3-Trichloropropane mg/kg ND 0.0050 0.0025 06/23/22 04:47 1,2,4-Trichlorobenzene mg/kg ND 0.0050 0.0042 06/23/22 04:47 1,2,4-Trimethylbenzene mg/kg ND 0.0050 0.0014 06/23/22 04:47 1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 0.0019 06/23/22 04:47 1,2-Dibromoethane (EDB) mg/kg ND 0.0050 0.0022 06/23/22 04:47 1,2-Dichlorobenzene mg/kg ND 0.0050 0.0018 06/23/22 04:47 1,2-Dichloroethane mg/kg ND 0.0050 0.0033 06/23/22 04:47 1,2-Dichloropropane mg/kg ND 0.0050 0.0015 06/23/22 04:47 1,3,5-Trimethylbenzene mg/kg ND 0.0050 0.0017 06/23/22 04:47 1,3-Dichlorobenzene mg/kg ND 0.0050 0.0016 06/23/22 04:47 1,3-Dichloropropane mg/kg ND 0.0050 0.0016 06/23/22 04:47 1,4-Dichlorobenzene mg/kg ND 0.0050 0.0013 06/23/22 04:47 2,2-Dichloropropane mg/kg ND 0.0050 0.0016 06/23/22 04:47 2-Butanone (MEK) mg/kg ND 0.10 0.024 06/23/22 04:47 2-Chlorotoluene mg/kg ND 0.0050 0.0018 06/23/22 04:47 2-Hexanone mg/kg ND 0.050 0.0048 06/23/22 04:47 4-Chlorotoluene mg/kg ND 0.0050 0.00088 06/23/22 04:47 4-Methyl-2-pentanone (MIBK) mg/kg ND 0.050 0.0048 06/23/22 04:47 Acetone mg/kg ND 0.10 0.032 06/23/22 04:47 Benzene mg/kg ND 0.0050 0.0020 06/23/22 04:47 Bromobenzene mg/kg ND 0.0050 0.0016 06/23/22 04:47 Bromochloromethane mg/kg ND 0.0050 0.0015 06/23/22 04:47 Bromodichloromethane mg/kg ND 0.0050 0.0019 06/23/22 04:47 Bromoform mg/kg ND 0.0050 0.0018 06/23/22 04:47 Bromomethane mg/kg ND 0.010 0.0079 06/23/22 04:47 IK Carbon tetrachloride mg/kg ND 0.0050 0.0019 06/23/22 04:47 Chlorobenzene mg/kg ND 0.0050 0.00096 06/23/22 04:47 Chloroethane mg/kg ND 0.010 0.0039 06/23/22 04:47 Chloroform mg/kg ND 0.0050 0.0030 06/23/22 04:47 Chloromethane mg/kg ND 0.010 0.0042 06/23/22 04:47 cis-1,2-Dichloroethene mg/kg ND 0.0050 0.0017 06/23/22 04:47 cis-1,3-Dichloropropene mg/kg ND 0.0050 0.0014 06/23/22 04:47 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 METHOD BLANK: 3685232 Associated Lab Samples: 92611001001, 92611001002 Parameter Units Matrix: Blank Result Solid Reporting Limit MDL Analyzed Dibromochloromethane mg/kg ND 0.0050 0.0028 06/23/22 04:47 Dibromomethane mg/kg ND 0.0050 0.0011 06/23/22 04:47 Dichlorodifluoromethane mg/kg ND 0.010 0.0022 06/23/22 04:47 Diisopropyl ether mg/kg ND 0.0050 0.0014 06/23/22 04:47 Ethylbenzene mg/kg ND 0.0050 0.0023 06/23/22 04:47 Hexachloro-1,3-butadiene mg/kg ND 0.010 0.0082 06/23/22 04:47 Isopropylbenzene (Cumene) mg/kg ND 0.0050 0.0017 06/23/22 04:47 m&p-Xylene mg/kg ND 0.010 0.0034 06/23/22 04:47 Methyl-tert-butyl ether mg/kg ND 0.0050 0.0019 06/23/22 04:47 Methylene Chloride mg/kg ND 0.020 0.014 06/23/22 04:47 n-Butylbenzene mg/kg ND 0.0050 0.0024 06/23/22 04:47 n-Propylbenzene mg/kg ND 0.0050 0.0018 06/23/22 04:47 Naphthalene mg/kg ND 0.0050 0.0026 06/23/22 04:47 o-Xylene mg/kg ND 0.0050 0.0022 06/23/22 04:47 p-Isopropyltoluene mg/kg ND 0.0050 0.0025 06/23/22 04:47 sec-Butylbenzene mg/kg ND 0.0050 0.0022 06/23/22 04:47 Styrene mg/kg ND 0.0050 0.0013 06/23/22 04:47 tert-Butyl benzene mg/kg ND 0.0050 0.0018 06/23/22 04:47 Tetrachloroethene mg/kg ND 0.0050 0.0016 06/23/22 04:47 Toluene mg/kg ND 0.0050 0.0014 06/23/22 04:47 trans-1,2-Dichloroethene mg/kg ND 0.0050 0.0018 06/23/22 04:47 trans- 1,3-Dichloropropene mg/kg ND 0.0050 0.0017 06/23/22 04:47 Trichloroethene mg/kg ND 0.0050 0.0013 06/23/22 04:47 Trichlorofluoromethane mg/kg ND 0.0050 0.0028 06/23/22 04:47 Vinyl acetate mg/kg ND 0.050 0.0036 06/23/22 04:47 Vinyl chloride mg/kg ND 0.010 0.0025 06/23/22 04:47 Xylene (Total) mg/kg ND 0.010 0.0028 06/23/22 04:47 1,2-Dichloroethane-d4 (S) % 103 70-130 06/23/22 04:47 4-Bromofluorobenzene (S) % 100 69-134 06/23/22 04:47 Toluene-d8 (S) % 101 70-130 06/23/22 04:47 v2 I:/ IK Qualifiers LABORATORY CONTROL SAMPLE: 3685233 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane mg/kg 1.2 1.3 102 70-130 1,1,1-Trichloroethane mg/kg 1.2 1.3 107 70-130 1,1,2,2-Tetrachloroethane mg/kg 1.2 1.2 100 70-130 1,1,2-Trichloroethane mg/kg 1.2 1.3 104 70-130 1,1-Dichloroethane mg/kg 1.2 1.3 104 70-130 1,1-Dichloroethene mg/kg 1.2 1.4 112 70-130 1,1-Dichloropropene mg/kg 1.2 1.4 110 70-130 1,2,3-Trichlorobenzene mg/kg 1.2 1.3 101 65-130 1,2,3-Trichloropropane mg/kg 1.2 1.2 97 70-130 1,2,4-Trichlorobenzene mg/kg 1.2 1.3 103 68-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 LABORATORY CONTROL SAMPLE: Parameter 3685233 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,2,4-Trimethylbenzene mg/kg 1.2 1.3 103 70-130 1,2-Dibromo-3-chloropropane mg/kg 1.2 1.3 106 70-130 1,2-Dibromoethane (EDB) mg/kg 1.2 1.2 100 70-130 1,2-Dichlorobenzene mg/kg 1.2 1.3 101 70-130 1,2-Dichloroethane mg/kg 1.2 1.2 99 63-130 1,2-Dichloropropane mg/kg 1.2 1.3 105 70-130 1,3,5-Trimethylbenzene mg/kg 1.2 1.3 106 70-130 1,3-Dichlorobenzene mg/kg 1.2 1.3 103 70-130 1,3-Dichloropropane mg/kg 1.2 1.2 97 70-130 1,4-Dichlorobenzene mg/kg 1.2 1.2 98 70-130 2,2-Dichloropropane mg/kg 1.2 1.3 102 66-130 2-Butanone (MEK) mg/kg 2.5 2.4 98 70-130 2-Chlorotoluene mg/kg 1.2 1.3 103 70-130 2-Hexanone mg/kg 2.5 2.6 106 70-130 4-Chlorotoluene mg/kg 1.2 1.3 102 70-130 4-Methyl-2-pentanone (MIBK) mg/kg 2.5 2.7 106 70-130 Acetone mg/kg 2.5 2.5 98 69-130 Benzene mg/kg 1.2 1.2 99 70-130 Bromobenzene mg/kg 1.2 1.3 102 70-130 Bromochloromethane mg/kg 1.2 1.3 105 70-130 Bromodichloromethane mg/kg 1.2 1.3 101 69-130 Bromoform mg/kg 1.2 1.3 100 70-130 Bromomethane mg/kg 1.2 1.3 105 52-1301K Carbon tetrachloride mg/kg 1.2 1.3 107 70-130 Chlorobenzene mg/kg 1.2 1.2 98 70-130 Chloroethane mg/kg 1.2 1.6 124 65-130 Chloroform mg/kg 1.2 1.2 100 70-130 Chloromethane mg/kg 1.2 1.6 131 55-130 L1 cis-1,2-Dichloroethene mg/kg 1.2 1.3 103 70-130 cis-1,3-Dichloropropene mg/kg 1.2 1.3 104 70-130 Dibromochloromethane mg/kg 1.2 1.2 98 70-130 Dibromomethane mg/kg 1.2 1.3 105 70-130 Dichlorodifluoromethane mg/kg 1.2 1.2 100 45-156 v3 Diisopropyl ether mg/kg 1.2 1.3 103 70-130 Ethylbenzene mg/kg 1.2 1.1 92 70-130 Hexachloro-1,3-butadiene mg/kg 1.2 1.3 101 66-130 Isopropylbenzene (Cumene) mg/kg 1.2 1.2 100 70-130 m&p-Xylene mg/kg 2.5 2.4 97 70-130 Methyl-tert-butyl ether mg/kg 1.2 1.2 95 70-130 Methylene Chloride mg/kg 1.2 1.0 82 65-130 n-Butylbenzene mg/kg 1.2 1.3 104 67-130 n-Propylbenzene mg/kg 1.2 1.3 104 70-130 Naphthalene mg/kg 1.2 1.4 109 70-130 o-Xylene mg/kg 1.2 1.2 98 70-130 p-Isopropyltoluene mg/kg 1.2 1.3 108 67-130 sec-Butylbenzene mg/kg 1.2 1.3 104 69-130 Styrene mg/kg 1.2 1.2 96 70-1301K Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 LABORATORY CONTROL SAMPLE: Parameter 3685233 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers tert-Butyl benzene mg/kg 1.2 1.3 107 67-130 Tetrachloroethene mg/kg 1.2 1.3 103 70-130 Toluene mg/kg 1.2 1.3 100 70-1301K trans-1,2-Dichloroethene mg/kg 1.2 1.4 110 70-130 trans- 1,3-Dichloropropene mg/kg 1.2 1.3 105 68-130 Trichloroethene mg/kg 1.2 1.3 106 70-130 Trichlorofluoromethane mg/kg 1.2 1.2 98 70-130 Vinyl acetate mg/kg 2.5 2.5 101 70-130 Vinyl chloride mg/kg 1.2 1.6 126 61-130 Xylene (Total) mg/kg 3.8 3.6 97 70-130 1,2-Dichloroethane-d4 (S) % 87 70-130 4-Bromofluorobenzene (S) % 96 69-134 Toluene-d8(S) % 101 70-130 MATRIX SPIKE SAMPLE: Parameter 3685234 Units 92611001001 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane mg/kg ND 0.7 0.64 93 70-131 1,1,1-Trichloroethane mg/kg ND 0.7 0.69 99 65-133 1,1,2,2-Tetrachloroethane mg/kg ND 0.7 0.61 87 66-130 1,1,2-Trichloroethane mg/kg ND 0.7 0.64 93 66-133 1,1-Dichloroethane mg/kg ND 0.7 0.65 94 65-130 1,1-Dichloroethene mg/kg ND 0.7 0.73 105 10-158 1,1-Dichloropropene mg/kg ND 0.7 0.71 102 68-133 1,2,3-Trichlorobenzene mg/kg ND 0.7 0.25 35 27-138 1,2,3-Trichloropropane mg/kg ND 0.7 0.58 83 67-130 1,2,4-Trichlorobenzene mg/kg ND 0.7 0.43 62 51-134 1,2,4-Trimethylbenzene mg/kg ND 0.7 0.66 95 63-136 1,2-Dibromo-3-chloropropane mg/kg ND 0.7 0.45 64 32-130 1,2-Dibromoethane (EDB) mg/kg ND 0.7 0.64 92 70-130 1,2-Dichlorobenzene mg/kg ND 0.7 0.64 92 69-130 1,2-Dichloroethane mg/kg ND 0.7 0.62 89 59-130 1,2-Dichloropropane mg/kg ND 0.7 0.68 98 70-130 1,3,5-Trimethylbenzene mg/kg ND 0.7 0.68 97 65-137 1,3-Dichlorobenzene mg/kg ND 0.7 0.63 91 70-130 1,3-Dichloropropane mg/kg ND 0.7 0.64 92 70-130 1,4-Dichlorobenzene mg/kg ND 0.7 0.59 85 68-130 2,2-Dichloropropane mg/kg ND 0.7 0.64 92 32-130 2-Butanone (MEK) mg/kg 0.046J 1.4 1.0 71 10-136 2-Chlorotoluene mg/kg ND 0.7 0.64 92 69-141 2-Hexanone mg/kg ND 1.4 1.1 82 10-144 4-Chlorotoluene mg/kg ND 0.7 0.63 90 70-132 4-Methyl-2-pentanone (MIBK) mg/kg ND 1.4 1.2 84 25-143 Acetone mg/kg ND 1.4 0.90 65 10-130 Benzene mg/kg ND 0.7 0.66 95 67-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 MATRIX SPIKE SAMPLE: 3685234 92611001001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Bromobenzene mg/kg ND 0.7 0.63 91 70-130 Bromochloromethane mg/kg ND 0.7 0.63 91 69-134 Bromodichloromethane mg/kg ND 0.7 0.59 85 64-130 Bromoform mg/kg ND 0.7 0.55 79 62-130 Bromomethane mg/kg ND 0.7 0.52 74 20-1761K Carbon tetrachloride mg/kg ND 0.7 0.67 96 65-140 Chlorobenzene mg/kg ND 0.7 0.67 96 70-130 Chloroethane mg/kg ND 0.7 0.24 35 10-130 Chloroform mg/kg ND 0.7 0.64 92 63-130 Chloromethane mg/kg ND 0.7 0.87 125 58-130 cis-1,2-Dichloroethene mg/kg ND 0.7 0.67 96 66-130 cis-1,3-Dichloropropene mg/kg ND 0.7 0.61 88 67-130 Dibromochloromethane mg/kg ND 0.7 0.57 81 67-130 Dibromomethane mg/kg ND 0.7 0.62 90 63-131 Dichlorodifluoromethane mg/kg ND 0.7 0.86 123 44-180 v3 Diisopropyl ether mg/kg ND 0.7 0.66 96 63-130 Ethylbenzene mg/kg ND 0.7 0.62 89 66-130 Hexachloro-1,3-butadiene mg/kg ND 0.7 0.57 82 64-150 Isopropylbenzene (Cumene) mg/kg ND 0.7 0.68 98 69-135 m&p-Xylene mg/kg ND 1.4 1.3 93 60-133 Methyl-tert-butyl ether mg/kg ND 0.7 0.58 84 65-130 Methylene Chloride mg/kg ND 0.7 0.34 49 61-130 M1 n-Butylbenzene mg/kg ND 0.7 0.63 90 65-140 n-Propylbenzene mg/kg ND 0.7 0.63 91 67-140 Naphthalene mg/kg ND 0.7 0.32 46 15-145 o-Xylene mg/kg ND 0.7 0.65 94 66-133 p-Isopropyltoluene mg/kg ND 0.7 0.67 97 56-147 sec-Butylbenzene mg/kg ND 0.7 0.66 96 65-139 Styrene mg/kg ND 0.7 0.63 90 70-132 IK tert-Butyl benzene mg/kg ND 0.7 0.67 97 62-135 Tetrachloroethene mg/kg ND 0.7 0.64 93 70-135 Toluene mg/kg ND 0.7 0.64 93 67-1301K trans-1,2-Dichloroethene mg/kg ND 0.7 0.70 101 69-130 trans- 1,3-Dichloropropene mg/kg ND 0.7 0.60 86 62-130 Trichloroethene mg/kg ND 0.7 0.69 99 70-135 Trichlorofluoromethane mg/kg ND 0.7 0.24 35 10-130 Vinyl acetate mg/kg ND 1.4 1.2 85 53-130 Vinyl chloride mg/kg ND 0.7 0.79 114 61-148 Xylene (Total) mg/kg ND 2 1.9 93 63-132 1,2-Dichloroethane-d4 (S) % 95 70-130 4-Bromofluorobenzene (S) % 100 69-134 Toluene-d8 (S) % 100 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 44 Pace Analytical Services, LLC lac, Analyilcal ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 SAMPLE DUPLICATE: 3685235 Parameter Units 92611001002 Result Dup Result RPD Max RPD Qualifiers 1,1,1,2-Tetrachloroethane mg/kg ND ND 30 1,1,1-Trichloroethane mg/kg ND ND 30 1,1,2,2-Tetrachloroethane mg/kg ND ND 30 1,1,2-Trichloroethane mg/kg ND ND 30 1,1-Dichloroethane mg/kg ND ND 30 1,1-Dichloroethene mg/kg ND ND 30 1,1-Dichloropropene mg/kg ND ND 30 1,2,3-Trichlorobenzene mg/kg ND ND 30 1,2,3-Trichloropropane mg/kg ND ND 30 1,2,4-Trichlorobenzene mg/kg ND ND 30 1,2,4-Trimethylbenzene mg/kg ND ND 30 1,2-Dibromo-3-chloropropane mg/kg ND ND 30 1,2-Dibromoethane (EDB) mg/kg ND ND 30 1,2-Dichlorobenzene mg/kg ND ND 30 1,2-Dichloroethane mg/kg ND ND 30 1,2-Dichloropropane mg/kg ND ND 30 1,3,5-Trimethylbenzene mg/kg ND ND 30 1,3-Dichlorobenzene mg/kg ND ND 30 1,3-Dichloropropane mg/kg ND ND 30 1,4-Dichlorobenzene mg/kg ND ND 30 2,2-Dichloropropane mg/kg ND ND 30 2-Butanone (MEK) mg/kg 0.053J ND 30 2-Chlorotoluene mg/kg ND ND 30 2-Hexanone mg/kg ND ND 30 4-Chlorotoluene mg/kg ND ND 30 4-Methyl-2-pentanone (MIBK) mg/kg ND ND 30 Acetone mg/kg ND ND 30 Benzene mg/kg ND ND 30 Bromobenzene mg/kg ND ND 30 Bromochloromethane mg/kg ND ND 30 Bromodichloromethane mg/kg ND ND 30 Bromoform mg/kg ND ND 30 Bromomethane mg/kg ND ND 301K Carbon tetrachloride mg/kg ND ND 30 Chlorobenzene mg/kg ND ND 30 Chloroethane mg/kg ND ND 30 Chloroform mg/kg ND ND 30 Chloromethane mg/kg ND ND 30 cis-1,2-Dichloroethene mg/kg ND ND 30 cis-1,3-Dichloropropene mg/kg ND ND 30 Dibromochloromethane mg/kg ND ND 30 Dibromomethane mg/kg ND ND 30 Dichlorodifluoromethane mg/kg ND ND 30 v2 Diisopropyl ether mg/kg ND ND 30 Ethylbenzene mg/kg ND ND 30 Hexachloro-1,3-butadiene mg/kg ND ND 30 Isopropylbenzene (Cumene) mg/kg ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 SAMPLE DUPLICATE: 3685235 Parameter Units 92611001002 Result Dup Result m&p-Xylene mg/kg ND ND Methyl-tert-butyl ether mg/kg ND ND Methylene Chloride mg/kg ND ND n-Butylbenzene mg/kg ND ND n-Propylbenzene mg/kg ND ND Naphthalene mg/kg ND ND o-Xylene mg/kg ND ND p-Isopropyltoluene mg/kg ND ND sec-Butylbenzene mg/kg ND ND Styrene mg/kg ND ND tert-Butyl benzene mg/kg ND ND Tetrachloroethene mg/kg ND ND Toluene mg/kg ND ND trans-1,2-Dichloroethene mg/kg ND ND trans- 1,3-Dichloropropene mg/kg ND ND Trichloroethene mg/kg ND ND Trichlorofluoromethane mg/kg ND ND Vinyl acetate mg/kg ND ND Vinyl chloride mg/kg ND ND Xylene (Total) mg/kg ND ND 1,2-Dichloroethane-d4 (S) % 97 97 4-Bromofluorobenzene (S) % 100 101 Toluene-d8 (S) % 100 100 Max RPD RPD Qualifiers 30 30 30 30 30 30 30 30 30 30 I K 30 30 30 I K 30 30 30 30 30 30 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 QC Batch: 706835 Analysis Method: EPA 8081 B QC Batch Method: EPA 3546 Analysis Description: 8081 GCS Pesticides Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92611001001, 92611001002 METHOD BLANK: 3687430 Associated Lab Samples: 92611001001, 92611001002 Parameter Units Matrix: Blank Result Solid Reporting Limit MDL Analyzed 4,4'-DDD mg/kg ND 0.0020 0.00090 06/29/22 10:41 4,4'-DDE mg/kg ND 0.0020 0.00094 06/29/22 10:41 4,4'-DDT mg/kg ND 0.0020 0.00088 06/29/22 10:41 Aldrin mg/kg ND 0.0020 0.00080 06/29/22 10:41 alpha-BHC mg/kg ND 0.0020 0.00086 06/29/22 10:41 beta-BHC mg/kg ND 0.0020 0.00096 06/29/22 10:41 Chlordane (Technical) mg/kg ND 0.0099 0.0086 06/29/22 10:41 delta-BHC mg/kg ND 0.0020 0.00099 06/29/22 10:41 Dieldrin mg/kg ND 0.0020 0.00086 06/29/22 10:41 Endosulfan I mg/kg ND 0.0020 0.00085 06/29/22 10:41 Endosulfan II mg/kg ND 0.0020 0.00090 06/29/22 10:41 Endosulfan sulfate mg/kg ND 0.0020 0.0011 06/29/22 10:41 Endrin mg/kg ND 0.0020 0.00092 06/29/22 10:41 Endrin aldehyde mg/kg ND 0.0020 0.0013 06/29/22 10:41 Endrin ketone mg/kg ND 0.0020 0.0011 06/29/22 10:41 gamma-BHC (Lindane) mg/kg ND 0.0020 0.00080 06/29/22 10:41 Heptachlor mg/kg ND 0.0020 0.00092 06/29/22 10:41 Heptachlor epoxide mg/kg ND 0.0020 0.00079 06/29/22 10:41 Hexachlorobenzene mg/kg ND 0.0020 0.00082 06/29/22 10:41 Methoxychlor mg/kg ND 0.0050 0.0024 06/29/22 10:41 Mirex mg/kg ND 0.0050 0.0022 06/29/22 10:41 Toxaphene mg/kg ND 0.0070 0.0053 06/29/22 10:41 Decachlorobiphenyl (S) % 102 10-146 06/29/22 10:41 Tetrachloro-m-xylene (S) % 95 10-133 06/29/22 10:41 LABORATORY CONTROL SAMPLE: 3687431 Qualifiers Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 4,4'-DDD mg/kg 0.0083 0.011 134 40-160 4,4'-DDE mg/kg 0.0083 0.010 121 41-154 4,4'-DDT mg/kg 0.0083 0.0084 100 34-163 Aldrin mg/kg 0.0083 0.0072 86 39-144 alpha-BHC mg/kg 0.0083 0.0074 89 36-145 beta-BHC mg/kg 0.0083 0.0074 89 39-152 delta-BHC mg/kg 0.0083 0.0077 93 41-147 Dieldrin mg/kg 0.0083 0.0099 118 42-153 Endosulfan I mg/kg 0.0083 0.0072 86 39-148 Endosulfan II mg/kg 0.0083 0.0074 88 40-147 Endosulfan sulfate mg/kg 0.0083 0.0076 91 40-148 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 LABORATORY CONTROL SAMPLE: Parameter 3687431 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Endrin mg/kg 0.0083 0.010 122 42-158 Endrin aldehyde mg/kg 0.0083 0.0069 83 39-130 Endrin ketone mg/kg 0.0083 0.0071 85 39-159 gamma-BHC (Lindane) mg/kg 0.0083 0.0074 89 38-146 Heptachlor mg/kg 0.0083 0.0073 88 39-144 Heptachlor epoxide mg/kg 0.0083 0.0074 88 40-143 Hexachlorobenzene mg/kg 0.0083 0.0073 88 33-139 Methoxychlor mg/kg 0.025 0.019 76 32-146 Mirex mg/kg 0.025 0.022 86 39-141 Decachlorobiphenyl (S) % 90 10-146 Tetrachloro-m-xylene (S) % 88 10-133 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 QC Batch: 706520 Analysis Method: EPA 8270E QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92611001001, 92611001002 METHOD BLANK: 3685849 Associated Lab Samples: 92611001001, 92611001002 Parameter Units Matrix: Blank Result Solid Reporting Limit MDL Analyzed 1,2,4-Trichlorobenzene mg/kg ND 0.33 0.13 06/26/22 13:14 1,2-Dichlorobenzene mg/kg ND 0.33 0.12 06/26/22 13:14 1,3-Dichlorobenzene mg/kg ND 0.33 0.12 06/26/22 13:14 1,4-Dichlorobenzene mg/kg ND 0.33 0.13 06/26/22 13:14 1-Methylnaphthalene mg/kg ND 0.33 0.12 06/26/22 13:14 2,2'-Oxybis(1-chloropropane) mg/kg ND 0.33 0.16 06/26/22 13:14 2,4,5-Trichlorophenol mg/kg ND 0.33 0.15 06/26/22 13:14 2,4,6-Trichlorophenol mg/kg ND 0.33 0.14 06/26/22 13:14 2,4-Dichlorophenol mg/kg ND 0.33 0.13 06/26/22 13:14 2,4-Dimethylphenol mg/kg ND 0.33 0.14 06/26/22 13:14 2,4-Dinitrophenol mg/kg ND 1.7 1.0 06/26/22 13:14 2,4-Dinitrotoluene mg/kg ND 0.33 0.13 06/26/22 13:14 2,6-Dinitrotoluene mg/kg ND 0.33 0.12 06/26/22 13:14 2-Chloronaphthalene mg/kg ND 0.33 0.13 06/26/22 13:14 2-Chlorophenol mg/kg ND 0.33 0.13 06/26/22 13:14 2-Methylnaphthalene mg/kg ND 0.33 0.13 06/26/22 13:14 2-Methylphenol(o-Cresol) mg/kg ND 0.33 0.14 06/26/22 13:14 2-Nitroaniline mg/kg ND 1.7 0.27 06/26/22 13:14 2-Nitrophenol mg/kg ND 0.33 0.14 06/26/22 13:14 3&4-Methyl phenol (m&p Cresol) mg/kg ND 0.33 0.13 06/26/22 13:14 3,3'-Dichlorobenzidine mg/kg ND 0.67 0.23 06/26/22 13:14 3-Nitroaniline mg/kg ND 1.7 0.26 06/26/22 13:14 4,6-Dinitro-2-methyl phenol mg/kg ND 0.67 0.31 06/26/22 13:14 4-Bromophenylphenyl ether mg/kg ND 0.33 0.13 06/26/22 13:14 4-ChIoro-3-methyl phenol mg/kg ND 0.67 0.23 06/26/22 13:14 4-Chloroaniline mg/kg ND 0.67 0.26 06/26/22 13:14 4-Chlorophenylphenyl ether mg/kg ND 0.33 0.12 06/26/22 13:14 4-Nitroaniline mg/kg ND 0.67 0.25 06/26/22 13:14 4-Nitrophenol mg/kg ND 1.7 0.64 06/26/22 13:14 Acenaphthene mg/kg ND 0.33 0.12 06/26/22 13:14 Acenaphthylene mg/kg ND 0.33 0.12 06/26/22 13:14 Aniline mg/kg ND 0.33 0.13 06/26/22 13:14 Anthracene mg/kg ND 0.33 0.11 06/26/22 13:14 Benzo(a)anthracene mg/kg ND 0.33 0.11 06/26/22 13:14 Benzo(a)pyrene mg/kg ND 0.33 0.12 06/26/22 13:14 Benzo(b)fluoranthene mg/kg ND 0.33 0.11 06/26/22 13:14 Benzo(g,h,i)perylene mg/kg ND 0.33 0.13 06/26/22 13:14 Benzo(k)fluoranthene mg/kg ND 0.33 0.12 06/26/22 13:14 Benzoic Acid mg/kg ND 1.7 0.72 06/26/22 13:14 Benzyl alcohol mg/kg ND 0.67 0.25 06/26/22 13:14 IL Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 METHOD BLANK: 3685849 Associated Lab Samples: 92611001001, 92611001002 Parameter Units Matrix: Blank Result Solid Reporting Limit MDL Analyzed bis(2-Chloroethoxy)methane mg/kg ND 0.33 0.14 06/26/22 13:14 bis(2-Chloroethyl) ether mg/kg ND 0.33 0.13 06/26/22 13:14 bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 0.13 06/26/22 13:14 Butylbenzylphthalate mg/kg ND 0.33 0.14 06/26/22 13:14 Chrysene mg/kg ND 0.33 0.12 06/26/22 13:14 Di-n-butylphthalate mg/kg ND 0.33 0.11 06/26/22 13:14 Di-n-octylphthalate mg/kg ND 0.33 0.13 06/26/22 13:14 Dibenz(a,h)anthracene mg/kg ND 0.33 0.13 06/26/22 13:14 Dibenzofuran mg/kg ND 0.33 0.12 06/26/22 13:14 Diethylphthalate mg/kg ND 0.33 0.12 06/26/22 13:14 Dimethylphthalate mg/kg ND 0.33 0.12 06/26/22 13:14 Fluoranthene mg/kg ND 0.33 0.11 06/26/22 13:14 Fluorene mg/kg ND 0.33 0.12 06/26/22 13:14 Hexachloro-1,3-butadiene mg/kg ND 0.33 0.14 06/26/22 13:14 Hexachlorobenzene mg/kg ND 0.33 0.13 06/26/22 13:14 Hexachlorocyclopentadiene mg/kg ND 0.33 0.19 06/26/22 13:14 Hexachloroethane mg/kg ND 0.33 0.13 06/26/22 13:14 Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 0.13 06/26/22 13:14 Isophorone mg/kg ND 0.33 0.15 06/26/22 13:14 N-Nitroso-di-n-propylamine mg/kg ND 0.33 0.13 06/26/22 13:14 N-Nitrosodimethylamine mg/kg ND 0.33 0.11 06/26/22 13:14 N-Nitrosodiphenylamine mg/kg ND 0.33 0.12 06/26/22 13:14 Naphthalene mg/kg ND 0.33 0.11 06/26/22 13:14 Nitrobenzene mg/kg ND 0.33 0.15 06/26/22 13:14 Pentachlorophenol mg/kg ND 0.67 0.33 06/26/22 13:14 Phenanthrene mg/kg ND 0.33 0.11 06/26/22 13:14 Phenol mg/kg ND 0.33 0.15 06/26/22 13:14 Pyrene mg/kg ND 0.33 0.14 06/26/22 13:14 Pyridine mg/kg ND 0.33 0.11 06/26/22 13:14 2,4,6-Tribromophenol (S) % 69 18-130 06/26/22 13:14 2-Fluorobiphenyl (S) % 74 19-130 06/26/22 13:14 2-Fluorophenol (S) % 66 18-130 06/26/22 13:14 Nitrobenzene-d5 (S) % 72 21-130 06/26/22 13:14 Phenol-d6 (S) % 74 18-130 06/26/22 13:14 Terphenyl-d14 (S) % 75 15-130 06/26/22 13:14 v2 Qualifiers LABORATORY CONTROL SAMPLE: 3685850 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,2,4-Trichlorobenzene mg/kg 1.7 1.2 75 47-130 1,2-Dichlorobenzene mg/kg 1.7 1.2 75 49-130 1,3-Dichlorobenzene mg/kg 1.7 1.2 72 48-130 1,4-Dichlorobenzene mg/kg 1.7 1.2 74 49-130 1-Methylnaphthalene mg/kg 1.7 1.4 83 54-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 LABORATORY CONTROL SAMPLE: Parameter 3685850 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2,2'-Oxybis(1-chloropropane) mg/kg 1.7 1.2 72 38-130 2,4,5-Trichlorophenol mg/kg 1.7 1.4 87 49-130 2,4,6-Trichlorophenol mg/kg 1.7 1.3 81 50-130 2,4-Dichlorophenol mg/kg 1.7 1.5 89 51-130 2,4-Dimethylphenol mg/kg 1.7 1.4 87 53-130 2,4-Dinitrophenol mg/kg 8.3 6.1 74 39-130 2,4-Dinitrotoluene mg/kg 1.7 1.4 87 53-130 2,6-Dinitrotoluene mg/kg 1.7 1.5 90 55-130 2-Chloronaphthalene mg/kg 1.7 1.3 80 48-130 2-Chlorophenol mg/kg 1.7 1.1 68 54-130 2-Methylnaphthalene mg/kg 1.7 1.4 82 57-130 2-Methylphenol(o-Cresol) mg/kg 1.7 1.4 82 50-130 2-Nitroaniline mg/kg 3.3 3.2 96 49-130 2-Nitrophenol mg/kg 1.7 1.3 78 50-130 3&4-Methyl phenol (m&p Cresol) mg/kg 1.7 1.3 76 50-130 3,3'-Dichlorobenzidine mg/kg 3.3 2.7 82 47-130IL 3-Nitroaniline mg/kg 3.3 3.1 93 45-130 4,6-Dinitro-2-methyl phenol mg/kg 3.3 2.8 83 50-142 4-Bromophenylphenyl ether mg/kg 1.7 1.5 91 55-130 4-ChIoro-3-methyl phenol mg/kg 3.3 3.1 92 52-130 4-Chloroaniline mg/kg 3.3 2.8 85 49-130 4-Chlorophenylphenyl ether mg/kg 1.7 1.5 91 53-130 4-Nitroaniline mg/kg 3.3 2.9 87 51-130 4-Nitrophenol mg/kg 8.3 6.8 82 40-130 Acenaphthene mg/kg 1.7 1.4 87 56-130 Acenaphthylene mg/kg 1.7 1.3 81 58-130 Aniline mg/kg 1.7 1.0 63 44-130 Anthracene mg/kg 1.7 1.3 82 60-130 Benzo(a)anthracene mg/kg 1.7 1.4 82 59-130 Benzo(a)pyrene mg/kg 1.7 1.4 82 57-130 Benzo(b)fluoranthene mg/kg 1.7 1.4 83 54-130 Benzo(g,h,i)perylene mg/kg 1.7 1.3 76 59-130 Benzo(k)fluoranthene mg/kg 1.7 1.4 87 54-130 Benzoic Acid mg/kg 8.3 4.1 50 19-130 Benzyl alcohol mg/kg 3.3 2.5 77 50-130 bis(2-Chloroethoxy)methane mg/kg 1.7 1.4 85 55-130 bis(2-Chloroethyl) ether mg/kg 1.7 1.3 81 53-130 bis(2-Ethylhexyl)phthalate mg/kg 1.7 1.8 107 58-130 Butylbenzylphthalate mg/kg 1.7 1.7 102 46-138 Chrysene mg/kg 1.7 1.4 84 57-130 Di-n-butylphthalate mg/kg 1.7 1.5 88 57-130 Di-n-octylphthalate mg/kg 1.7 1.8 106 57-130 Dibenz(a,h)anthracene mg/kg 1.7 1.3 78 60-130 Dibenzofuran mg/kg 1.7 1.5 88 54-130 Diethylphthalate mg/kg 1.7 1.4 87 55-130 Dimethylphthalate mg/kg 1.7 1.4 86 57-130 Fluoranthene mg/kg 1.7 1.4 87 57-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 LABORATORY CONTROL SAMPLE: Parameter 3685850 Units Spike Conc. LCS LCS Result % Rec Fluorene mg/kg 1.7 1.4 Hexachloro-1,3-butadiene mg/kg 1.7 1.3 Hexachlorobenzene mg/kg 1.7 1.4 Hexachlorocyclopentadiene mg/kg 1.7 0.31J Hexachloroethane mg/kg 1.7 1.2 Indeno(1,2,3-cd)pyrene mg/kg 1.7 1.3 Isophorone mg/kg 1.7 1.4 N-Nitroso-di-n-propylamine mg/kg 1.7 1.5 N-Nitrosodimethylamine mg/kg 1.7 1.1 N-Nitrosodiphenylamine mg/kg 1.7 1.4 Naphthalene mg/kg 1.7 1.3 Nitrobenzene mg/kg 1.7 1.3 Pentachlorophenol mg/kg 3.3 2.4 Phenanthrene mg/kg 1.7 1.4 Phenol mg/kg 1.7 1.3 Pyrene mg/kg 1.7 1.4 Pyridine mg/kg 1.7 1.0 2,4,6-Tribromophenol (S) % 2-Fluorobiphenyl (S) % 2-Fluorophenol (S) % Nitrobenzene-d5 (S) % Phenol-d6 (S) % Terphenyl-d14 (S) % % Rec Limits Qualifiers 86 56-130 77 41-130 82 53-130 19 23-130 L2,v2 73 48-130 78 61-130 86 49-130 90 52-130 68 45-130 86 56-130 77 56-130 81 50-130 73 33-130 86 60-130 80 54-130 87 61-130 60 35-130 70 18-130 65 19-130 53 18-130 68 21-130 60 18-130 70 15-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 QC Batch: 706307 Analysis Method: SW-846 QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92611001001, 92611001002 SAMPLE DUPLICATE: 3684875 35725423001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Percent Moisture % 1.7 1.9 11 25 N2 SAMPLE DUPLICATE: 3684967 92611239002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Percent Moisture % 25.5 23.2 9 25 N2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 QC Batch: 1885227 Analysis Method: SM 2540G QC Batch Method: SM 2540 G Analysis Description: Total Solids 2540 G-2011 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92611001001 METHOD BLANK: R3807711-1 Associated Lab Samples: 92611001001 Parameter Units Total Solids % LABORATORY CONTROL SAMPLE: R3807711-2 Parameter Units Total Solids % SAMPLE DUPLICATE: R3807711-3 Parameter Units Total Solids % Matrix: Solid Blank Reporting Result Limit 0.00100 Spike LCS Conc. Result 50.0 50.0 L1507833-12 Dup Result Result 88.9 89.3 MDL Analyzed Qualifiers 06/25/22 17:12 LCS % Rec % Rec Limits Qualifiers 100 85.0-115 Max RPD RPD Qualifiers 0.355 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 QC Batch: 1886113 Analysis Method: SM 2540G QC Batch Method: SM 2540 G Analysis Description: Total Solids 2540 G-2011 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92611001002 METHOD BLANK: R3808457-1 Associated Lab Samples: 92611001002 Parameter Units Total Solids % LABORATORY CONTROL SAMPLE: R3808457-2 Parameter Units Total Solids % SAMPLE DUPLICATE: R3808457-3 Parameter Units Total Solids % Matrix: Solid Blank Reporting Result Limit 0.00200 Spike LCS Conc. Result 50.0 50.0 L1508532-02 Dup Result Result 65.6 65.0 MDL Analyzed Qualifiers 06/28/22 09:20 LCS % Rec % Rec Limits Qualifiers 100 85.0-115 Max RPD RPD Qualifiers 0.921 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 QC Batch: 1894501 Analysis Method: EPA 7199 QC Batch Method: 3060A Analysis Description: Wet Chemistry 7199 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92611001001, 92611001002 METHOD BLANK: R3816512-1 Matrix: Solid Associated Lab Samples: 92611001001, 92611001002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Chromium, Hexavalent mg/kg ND 1.00 0.255 07/15/22 16:50 LABORATORY CONTROL SAMPLE: R3816512-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chromium, Hexavalent mg/kg 10.0 9.40 94.0 80.0-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3816512-3 R3816512-4 MS MSD L1509391-01 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chromium, Hexavalent mg/kg ND 20.0 20.0 16.0 16.2 80.1 81.2 75.0-125 1.33 20 MATRIX SPIKE SAMPLE: R3816512-6 L1509391-01 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Chromium, Hexavalent mg/kg ND 643 665 103 75.0-125 SAMPLE DUPLICATE: R3816512-7 L1509391-06 Dup Max Parameter Units Result Result RPD RPD Qualifiers Chromium, Hexavalent mg/kg ND ND 0.00 20 SAMPLE DUPLICATE: R3816512-8 L1509267-02 Dup Max Parameter Units Result Result RPD RPD Qualifiers Chromium, Hexavalent mg/kg ND ND 0.00 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. ANALYTE QUALIFIERS D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference. E Analyte concentration exceeded the calibration range. The reported result is estimated. IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be considered an estimated value. IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be considered an estimated value. LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits. L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samples may be biased low. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. ML Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased low. N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditations/certifications is available upon request. P8 Analyte was detected in the method blank. All associated samples had concentrations of at least ten times greater than the blank or were below the reporting limit. P9 RPD between the primary and confirmatory analysis exceeded 40%. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: 10039-B WRIGHTS EXECUTIVE Pace Project No.: 92611001 ANALYTE QUALIFIERS S4 Surrogate recovery not evaluated against control limits due to sample dilution. v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/21 /2022 05:23 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 44 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: 10039-B WRIGHTS EXECUTIVE 92611001 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92611001001 UT-3 3546 1882585 EPA 8141 B 1882585 92611001002 DUP-3 3546 1882585 EPA 8141 B 1882585 92611001001 UT-3 8151A 1888224 EPA 8151 1888224 92611001002 DUP-3 8151A 1888224 EPA8151 1888224 92611001001 UT-3 EPA 3546 706835 EPA 8081B 707084 92611001002 DUP-3 EPA 3546 706835 EPA 8081 B 707084 92611001001 UT-3 EPA 3050B 743891 EPA 6020B 744354 92611001002 DUP-3 EPA 3050B 743891 EPA 6020B 744354 92611001001 UT-3 METHOD 743963 EPA 7471 B 744162 92611001002 DUP-3 METHOD 743963 EPA 7471 B 744162 92611001001 UT-3 EPA 3546 706520 EPA 8270E 707027 92611001002 DUP-3 EPA 3546 706520 EPA 8270E 707027 92611001001 UT-3 EPA 5035A/5030B 706373 EPA 8260D 706521 92611001002 DUP-3 EPA 5035A/5030B 706373 EPA 8260D 706521 92611001001 UT-3 SW-846 706307 92611001002 DUP-3 SW-846 706307 92611001001 UT-3 SM 2540 G 1885227 SM 2540G 1885227 92611001002 DUP-3 SM 2540 G 1886113 SM 254OG 1886113 92611001001 UT-3 3060A 1894501 EPA 7199 1894501 92611001002 DUP-3 3060A 1894501 EPA 7199 1894501 Date: 07/21 /2022 05:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 43 of 44 CHAIN -OF -CUSTODY Analytical Request Document Lus USE ONLY -Affixes - 3CgQ1� Cdi� Sub mittingasamplevia rhIsch31rcfdvatodycon stizutesacknowledgmmtardvcceptam, oft hePace Termsand � ■■ 1L�[ � �Q01 Condltiens found at: hWO i ttlnfO.pacNahscom/hybfs/pas-stantlaN-terms.pdf : g2 61 Chain -of -Custody Ls a LEGAL DOCUMEN7- Complete all relevant fields ! Company: ECSSoutheas UP Billing Information: Address: 5260 Greens DSiry Road, Raleigh, NC 27616 ALL BOLD RepoContainerPresen 1192611[30111 I rt 7a Email To: SSZ�ASS SCE r✓CS�[Nlt{�C�_CClr. '• Preservative Types: (1] nitric add, (2) sulfuric add, (3) hydrochloric acid, 14) sodium hydroxide, (5) zinc ac 7 CO To; S)Ce Collection Info/Address- (S) methanol, (7) sodium bisulfate, 18) sodium thiasulfate, IS) exane, (A) ascorbic acid, (8) ammonium surfax, �c t!`rCP� C 5 r[vct. CJ -C4 ^�- (C) ammonium hydroxide, (D) TSP. (U) Unpreserved, (D) Othe Customer Project Name Number: State; NC County/City: U v�41�-� Analyses Lab Profile/line• Phone: s xPc vh / [ ]PT [ ]MT [ !]CT [ ]ET Lab Sample iieceipt Checklist: Email: Site/Facfliry lD#: Compliance Monitoring? ustody seals present/-ritact MR Collected 8.yyyy�--,(print) Purchase Order # : I ]Yes [ ]Na DW PWS iD 71:. O Custody' Signat:uzes Presnnt NA Collector Signature Present 6PN Ng oottxes Intact. - I?S11 C[15 quo[ek: �• N NA. Collected (s DW Location Code: N -.o 1v 4` ..orrect Bottles Sufficient y ore : Turnaround Date Re uir d 9 Immediately Packed on Ice: - volume NA '. Samples -Received on ICo.., .I9N NA Sample isposal� G r Rush: {ExpediteChargesq I Apply) [XI Yes [ ] No Field Filtered (if applicable]: m V— �' t� ;70A —. Hoadspacc 'Acceptable 0t4 Na USDA Regulate /q'� N NA ' J ] Dispose as appropriate [ ]",turn [ ] Same Day [ J Next Day [ ] Yes [ ) No ' t�'� Saniplen in Hol'dln l Time QVN. NA I 1 2 day [ ] 3 Day o esidual- Chlorine ' Present- Y N(P [ ]Archive: �--r I ]Hold:_ I I ] 4 Day I 5 Day Analysis: _ a � - CS Strips.' Sa-P' a PH Acceptable Y- N. �i Matrix Codes (Insert in Product atrix box below): Drinking Water (DW), Ground Water{GW), Wastewater {WW}, y � a r ] ..3 `) PH.. Strips.: Sulfide Present y Lead - (P), Soil/Solid {$L), Oil OL , Wi ( ) pe {WP), Air (AR), Tissue ITS), Bioassay (B), Vapor IV), Other (OT) o (l) ( r Acetate St: ; Collected (or �J 'i^ W x as U$ ONI Y: Customer Sample lD Matrix ` Composite start) Composite End Cis Ctns - �. lab Sample ! / convnents: EGmpb Date Time pate Time 0 U — I ' Customer Remarks alConditions/PossibleHaxaryeUsed: Blui ❑ None SHORTHOLDSPRESENT{c77hours): Y N: IfI/A.'.' LAB Sample Temperature Info: PaCkingMatCrialUsed; - Lab Tracking TeMp Blank Received; Y_ N NA .,� ., _ ('Samples -.. .. Therm TDi :-! ��� c] - - Dole= 1 Temp Upon Aeccippjgt Radchem sample(s) screened �' I Op c N )yA received via: - Cooler 1 Therm Corr, 'Fa,_torl '�C 1 Cooler Reh ,qui hed by/Co p n IS nature] Date im r[ Rece• FEDEX UPS 'Client.. Cour-I ce Eou - 1 Corrected Tempi r p' "C Comments, . LG �7 nY: (Signature) a Ime: 910 NLY - Re[inquis by C L : (5ie-ture) D te/Fi e: Re iv mpany: (Signature } (a6fe ate/Time; 4 ccctnumr Trip Blank Received: Y N' NA. I 'Other �p- 2� �� Z emplate:. HCL -MeOH TSP' Relin ui by/Compan : [Signature] Dat ime: Received b man V.Si nature P Y (Signature) } Date/Time: Prciogln: j ] PM:Non Conformance(s): Page; PB:. YES / NO of: leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 August 25, 2022 Samantha M. Szakasits, G.I.T. ECS Southeast, LLP 5260 Greens Dary Road Raleigh, NC 27616 RE: Project: Wright's Executive Sales Pace Project No.: 92614993 Dear Samantha Szakasits, G.I.T.: Enclosed are the analytical results for sample(s) received by the laboratory on July 13, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace National - Mt. Juliet A revised laboratory report is being submitted on 7/25/22 to update the primary report recipient, per client request. Project Un-Reported on 08/25/22 to report MDLs per client request. If you have any questions concerning this report, please feel free to contact me. Sincerely, Zachary J Tierney for Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures cc: ECS Southeast Reporting, ECS Southeast Scott Werley, ECS Southeast, LLP REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 22 lacieAnalyfica(' www,pacelabs.com Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Wright's Executive Sales Pace Project No.: 92614993 Pace Analytical Services National 12065 Lebanon Road, Mt. Juliet, TN 37122 Alabama Certification #: 40660 Alaska Certification 17-026 Arizona Certification #: AZ0612 Arkansas Certification #: 88-0469 California Certification #: 2932 Canada Certification #: 1461.01 Colorado Certification #: TN00003 Connecticut Certification #: PH-0197 DOD Certification: #1461.01 EPA# TN00003 Florida Certification #: E87487 Georgia DW Certification #: 923 Georgia Certification: NELAP Idaho Certification #: TN00003 Illinois Certification #: 200008 Indiana Certification #: C-TN-01 Iowa Certification #: 364 Kansas Certification #: E-10277 Kentucky UST Certification #: 16 Kentucky Certification #: 90010 Louisiana Certification #: A130792 Louisiana DW Certification #: LA180010 Maine Certification #: TN0002 Maryland Certification #: 324 Massachusetts Certification #: M-TNO03 Michigan Certification #: 9958 Minnesota Certification #: 047-999-395 Mississippi Certification #: TN00003 Missouri Certification #: 340 Montana Certification M CERT0086 Nebraska Certification #: NE-OS-15-05 CERTIFICATIONS Nevada Certification #: TN-03-2002-34 New Hampshire Certification #: 2975 New Jersey Certification #: TNO02 New Mexico DW Certification New York Certification #: 11742 North Carolina Aquatic Toxicity Certification #: 41 North Carolina Drinking Water Certification #: 21704 North Carolina Environmental Certificate #: 375 North Dakota Certification #: R-140 Ohio VAP Certification #: CL0069 Oklahoma Certification #: 9915 Oregon Certification #: TN200002 Pennsylvania Certification #: 68-02979 Rhode Island Certification #: LA000356 South Carolina Certification #: 84004 South Dakota Certification Tennessee DW/Chem/Micro Certification #: 2006 Texas Certification #: T 104704245-17-14 Texas Mold Certification #: LAB0152 USDA Soil Permit #: P330-15-00234 Utah Certification #: TN00003 Virginia Certification #: VT2006 Vermont Dept. of Health: ID# VT-2006 Virginia Certification #: 460132 Washington Certification #: C847 West Virginia Certification #: 233 Wisconsin Certification #: 998093910 Wyoming UST Certification #: via A21LA 2926.01 A21-A-ISO 17025 Certification #: 1461.01 A21-A-ISO 17025 Certification #: 1461.02 AIHA-LAP/LLC EMLAP Certification #:100789 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 22 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: Wright's Executive Sales Pace Project No.: 92614993 Lab ID Sample ID Matrix Date Collected Date Received 92614993001 SPR-1 Solid 07/13/2212:01 07/13/2214:25 92614993002 SPR-2 Solid 07/13/2212:32 07/13/2214:25 92614993003 SPR-3 Solid 07/13/2213:09 07/13/2214:25 92614993004 DUP-4 Solid 07/13/22 00:00 07/13/22 14:25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 22 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: Wright's Executive Sales 92614993 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92614993001 SPR-1 EPA 8141E KLA 27 PAN EPA 8321 GKM 11 PAN SM 2540G CMK 1 PAN 92614993002 SPR-2 EPA 8141E KLA 27 PAN EPA 8321 GKM 11 PAN SM 2540G CMK 1 PAN 92614993003 SPR-3 EPA 8141E KLA 27 PAN EPA 8321 GKM 11 PAN SM 2540G CMK 1 PAN 92614993004 DUP-4 EPA 8141B KLA 27 PAN EPA 8321 GKM 11 PAN SM 2540G CMK 1 PAN PAN = Pace National - Mt. Juliet REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 22 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92614993 Sample: SPR-1 Lab ID: 92614993001 Collected: 07/13/22 12:01 Received: 07/13/22 14:25 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual OP Pesticides 8141 B Azinphos, methyl (Guthion) Bolstar Chlorpyrifos Coumaphos Total Demeton Diazinon Dichlorvos Dimethoate Disulfoton EPN (ENT) Ethoprop Parathion (Ethyl parathion) Fensulfothion Fenthion Malathion Merphos Methyl parathion Mevinphos Naled Phorate Ronnel Stirophos (Tetrachlorvinphos) Sulfotepp (ThiodiphosphoricAc TEPP Tokuthion (Prothiofos) Trichloronate Surrogates Triphenylphosphate (S) SVOA (LCMS) SW-846 8321 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DB-d3 (S) Analytical Method: EPA 8141 B Preparation Method: 3546 Pace National - Mt. Juliet ND mg/kg 0.129 0.0410 1 07/18/2217:02 07/19/2210:24 86-50-0 ND mg/kg 0.129 0.0192 1 07/18/2217:02 07/19/2210:24 35400-43-2 ND mg/kg 0.129 0.0203 1 07/18/2217:02 07/19/2210:24 2921-88-2 ND mg/kg 0.129 0.0313 1 07/18/2217:02 07/19/2210:24 56-72-4 ND mg/kg 0.0903 0.00753 1 07/18/2217:02 07/19/2210:24 8065-48-3 ND mg/kg 0.129 0.0290 1 07/18/2217:02 07/19/2210:24 333-41-5 ND mg/kg 0.129 0.0387 1 07/18/2217:02 07/19/2210:24 62-73-7 ND mg/kg 0.129 0.0431 1 07/18/2217:02 07/19/2210:24 60-51-5 ND mg/kg 0.129 0.0328 1 07/18/2217:02 07/19/2210:24 298-04-4 ND mg/kg 0.129 0.0356 1 07/18/2217:02 07/19/2210:24 2104-64-5 ND mg/kg 0.129 0.0152 1 07/18/2217:02 07/19/2210:24 13194-48-4 ND mg/kg 0.129 0.0212 1 07/18/2217:02 07/19/2210:24 56-38-2 ND mg/kg 0.129 0.0455 1 07/18/2217:02 07/19/2210:24 115-90-2 ND mg/kg 0.129 0.0172 1 07/18/2217:02 07/19/2210:24 55-38-9 ND mg/kg 0.129 0.0231 1 07/18/2217:02 07/19/2210:24 121-75-5 ND mg/kg 0.129 0.0299 1 07/18/2217:02 07/19/2210:24 150-50-5 ND mg/kg 0.129 0.0262 1 07/18/2217:02 07/19/2210:24 298-00-0 ND mg/kg 0.129 0.0297 1 07/18/2217:02 07/19/2210:24 7786-34-7 ND mg/kg 0.129 0.0619 1 07/18/2217:02 07/19/2210:24 300-76-5 ND mg/kg 0.129 0.0271 1 07/18/2217:02 07/19/2210:24 298-02-2 ND mg/kg 0.129 0.0192 1 07/18/2217:02 07/19/2210:24 299-84-3 ND mg/kg 0.129 0.0230 1 07/18/2217:02 07/19/2210:24 22248-79-9 ND mg/kg 0.129 0.0127 1 07/18/2217:02 07/19/2210:24 3689-24-5 ND mg/kg 1.29 0.203 1 07/18/2217:02 07/19/2210:24 107-49-3 ND mg/kg 0.129 0.0193 1 07/18/2217:02 07/19/2210:24 34643-46-4 ND mg/kg 0.129 0.0259 1 07/18/2217:02 07/19/2210:24 327-98-0 72.7 % 36.0-121 1 07/18/2217:02 07/19/2210:24 115-86-6 Analytical Method: EPA 8321 Preparation Method: 8321 Pace National - Mt. Juliet ND mg/kg 0.0258 0.00668 1 07/20/2210:55 07/20/2217:24 94-75-7 ND mg/kg 0.0258 0.00409 1 07/20/2210:55 07/20/2217:24 127-20-8 ND mg/kg 0.0258 0.0117 1 07/20/2210:55 07/20/2217:24 94-82-6 ND mg/kg 0.0258 0.00556 1 07/20/2210:55 07/20/2217:24 1918-00-9 ND mg/kg 0.0258 0.00430 1 07/20/2210:55 07/20/2217:24 15165-67-0 ND mg/kg 0.0258 0.00257 1 07/20/2210:55 07/20/2217:24 88-85-7 ND mg/kg 0.0258 0.00441 1 07/20/2210:55 07/20/2217:24 94-74-6 ND mg/kg 0.0258 0.00302 1 07/20/2210:55 07/20/2217:24 7085-19-0 ND mg/kg 0.0258 0.00885 1 07/20/2210:55 07/20/2217:24 93-76-5 ND mg/kg 0.0258 0.00221 1 07/20/2210:55 07/20/2217:24 93-72-1 109 % 70.0-130 1 07/20/2210:55 07/20/2217:24 1219802-46- REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/25/2022 09:57 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 22 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92614993 Sample: SPR-1 Lab ID: 92614993001 Collected: 07/13/22 12:01 Received: 07/13/22 14:25 Matrix: Solid Results reported on a "wet -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Total Solids 2540 G-2011 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 77.5 % 1 07/19/22 09:43 07/19/22 15:50 Date: 08/25/2022 09:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 22 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92614993 Sample: SPR-2 Lab ID: 92614993002 Collected: 07/13/22 12:32 Received: 07/13/22 14:25 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual OP Pesticides 8141 B Azinphos, methyl (Guthion) Bolstar Chlorpyrifos Coumaphos Total Demeton Diazinon Dichlorvos Dimethoate Disulfoton EPN (ENT) Ethoprop Parathion (Ethyl parathion) Fensulfothion Fenthion Malathion Merphos Methyl parathion Mevinphos Naled Phorate Ronnel Stirophos (Tetrachlorvinphos) Sulfotepp (ThiodiphosphoricAc TEPP Tokuthion (Prothiofos) Trichloronate Surrogates Triphenylphosphate (S) SVOA (LCMS) SW-846 8321 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DB-d3 (S) Analytical Method: EPA 8141 B Preparation Method: 3546 Pace National - Mt. Juliet ND mg/kg 0.155 0.0493 1 07/18/2217:02 07/19/2210:58 86-50-0 ND mg/kg 0.155 0.0231 1 07/18/2217:02 07/19/2210:58 35400-43-2 ND mg/kg 0.155 0.0243 1 07/18/2217:02 07/19/2210:58 2921-88-2 ND mg/kg 0.155 0.0377 1 07/18/2217:02 07/19/2210:58 56-72-4 ND mg/kg 0.109 0.00905 1 07/18/2217:02 07/19/2210:58 8065-48-3 ND mg/kg 0.155 0.0349 1 07/18/2217:02 07/19/2210:58 333-41-5 ND mg/kg 0.155 0.0465 1 07/18/2217:02 07/19/2210:58 62-73-7 ND mg/kg 0.155 0.0518 1 07/18/2217:02 07/19/2210:58 60-51-5 ND mg/kg 0.155 0.0394 1 07/18/2217:02 07/19/2210:58 298-04-4 ND mg/kg 0.155 0.0428 1 07/18/2217:02 07/19/2210:58 2104-64-5 ND mg/kg 0.155 0.0183 1 07/18/2217:02 07/19/2210:58 13194-48-4 ND mg/kg 0.155 0.0254 1 07/18/2217:02 07/19/2210:58 56-38-2 ND mg/kg 0.155 0.0547 1 07/18/2217:02 07/19/2210:58 115-90-2 ND mg/kg 0.155 0.0206 1 07/18/2217:02 07/19/2210:58 55-38-9 ND mg/kg 0.155 0.0278 1 07/18/2217:02 07/19/2210:58 121-75-5 ND mg/kg 0.155 0.0360 1 07/18/2217:02 07/19/2210:58 150-50-5 ND mg/kg 0.155 0.0315 1 07/18/2217:02 07/19/2210:58 298-00-0 ND mg/kg 0.155 0.0357 1 07/18/2217:02 07/19/2210:58 7786-34-7 ND mg/kg 0.155 0.0744 1 07/18/2217:02 07/19/2210:58 300-76-5 ND mg/kg 0.155 0.0326 1 07/18/2217:02 07/19/2210:58 298-02-2 ND mg/kg 0.155 0.0231 1 07/18/2217:02 07/19/2210:58 299-84-3 ND mg/kg 0.155 0.0276 1 07/18/2217:02 07/19/2210:58 22248-79-9 ND mg/kg 0.155 0.0153 1 07/18/2217:02 07/19/2210:58 3689-24-5 ND mg/kg 1.55 0.243 1 07/18/2217:02 07/19/2210:58 107-49-3 ND mg/kg 0.155 0.0233 1 07/18/2217:02 07/19/2210:58 34643-46-4 ND mg/kg 0.155 0.0312 1 07/18/2217:02 07/19/2210:58 327-98-0 81.8 % 36.0-121 1 07/18/2217:02 07/19/2210:58 115-86-6 Analytical Method: EPA 8321 Preparation Method: 8321 Pace National - Mt. Juliet ND mg/kg 0.0310 0.00803 1 07/20/2210:55 07/20/2217:42 94-75-7 ND mg/kg 0.0310 0.00491 1 07/20/2210:55 07/20/2217:42 127-20-8 ND mg/kg 0.0310 0.0141 1 07/20/2210:55 07/20/2217:42 94-82-6 ND mg/kg 0.0310 0.00668 1 07/20/2210:55 07/20/2217:42 1918-00-9 ND mg/kg 0.0310 0.00516 1 07/20/2210:55 07/20/2217:42 15165-67-0 ND mg/kg 0.0310 0.00309 1 07/20/2210:55 07/20/2217:42 88-85-7 ND mg/kg 0.0310 0.00530 1 07/20/2210:55 07/20/2217:42 94-74-6 ND mg/kg 0.0310 0.00363 1 07/20/2210:55 07/20/2217:42 7085-19-0 ND mg/kg 0.0310 0.0106 1 07/20/2210:55 07/20/2217:42 93-76-5 ND mg/kg 0.0310 0.00265 1 07/20/2210:55 07/20/2217:42 93-72-1 101 % 70.0-130 1 07/20/2210:55 07/20/2217:42 1219802-46- REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/25/2022 09:57 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 22 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92614993 Sample: SPR-2 Lab ID: 92614993002 Collected: 07/13/22 12:32 Received: 07/13/22 14:25 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Total Solids 2540 G-2011 Analytical Method: SM 254OG Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 64.5 % 1 07/19/22 09:43 07/19/22 15:50 Date: 08/25/2022 09:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 22 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92614993 Sample: SPR-3 Lab ID: 92614993003 Collected: 07/13/22 13:09 Received: 07/13/22 14:25 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual OP Pesticides 8141 B Analytical Method: EPA 8141 B Preparation Method: 3546 Pace National - Mt. Juliet Azinphos, methyl (Guthion) ND mg/kg 0.126 0.0401 1 07/18/22 17:02 07/19/22 11:31 86-50-0 Bolstar ND mg/kg 0.126 0.0188 1 07/18/22 17:02 07/19/22 11:31 35400-43-2 Chlorpyrifos ND mg/kg 0.126 0.0198 1 07/18/22 17:02 07/19/22 11:31 2921-88-2 Coumaphos ND mg/kg 0.126 0.0307 1 07/18/22 17:02 07/19/22 11:31 56-72-4 Total Demeton ND mg/kg 0.0884 0.00737 1 07/18/22 17:02 07/19/22 11:31 8065-48-3 Diazinon ND mg/kg 0.126 0.0284 1 07/18/22 17:02 07/19/22 11:31 333-41-5 Dichlorvos ND mg/kg 0.126 0.0379 1 07/18/22 17:02 07/19/22 11:31 62-73-7 Dimethoate ND mg/kg 0.126 0.0422 1 07/18/22 17:02 07/19/22 11:31 60-51-5 Disulfoton ND mg/kg 0.126 0.0321 1 07/18/22 17:02 07/19/22 11:31 298-04-4 EPN (ENT) ND mg/kg 0.126 0.0348 1 07/18/22 17:02 07/19/22 11:31 2104-64-5 Ethoprop ND mg/kg 0.126 0.0149 1 07/18/22 17:02 07/19/22 11:31 13194-48-4 Parathion (Ethyl parathion) ND mg/kg 0.126 0.0207 1 07/18/22 17:02 07/19/22 11:31 56-38-2 Fensulfothion ND mg/kg 0.126 0.0446 1 07/18/22 17:02 07/19/22 11:31 115-90-2 Fenthion ND mg/kg 0.126 0.0168 1 07/18/22 17:02 07/19/22 11:31 55-38-9 Malathion ND mg/kg 0.126 0.0226 1 07/18/22 17:02 07/19/22 11:31 121-75-5 Merphos ND mg/kg 0.126 0.0293 1 07/18/22 17:02 07/19/22 11:31 150-50-5 Methyl parathion ND mg/kg 0.126 0.0256 1 07/18/22 17:02 07/19/22 11:31 298-00-0 Mevinphos ND mg/kg 0.126 0.0290 1 07/18/22 17:02 07/19/22 11:31 7786-34-7 Naled ND mg/kg 0.126 0.0606 1 07/18/22 17:02 07/19/22 11:31 300-76-5 Phorate ND mg/kg 0.126 0.0265 1 07/18/22 17:02 07/19/22 11:31 298-02-2 Ronnel ND mg/kg 0.126 0.0188 1 07/18/22 17:02 07/19/22 11:31 299-84-3 Stirophos (Tetrachlorvinphos) ND mg/kg 0.126 0.0225 1 07/18/22 17:02 07/19/22 11:31 22248-79-9 Sulfotepp (ThiodiphosphoricAc ND mg/kg 0.126 0.0124 1 07/18/22 17:02 07/19/22 11:31 3689-24-5 TEPP ND mg/kg 1.26 0.198 1 07/18/22 17:02 07/19/22 11:31 107-49-3 Tokuthion (Prothiofos) ND mg/kg 0.126 0.0189 1 07/18/22 17:02 07/19/22 11:31 34643-46-4 Trichloronate ND mg/kg 0.126 0.0254 1 07/18/22 17:02 07/19/22 11:31 327-98-0 Surrogates Triphenylphosphate (S) 67.3 % 36.0-121 1 07/18/22 17:02 07/19/22 11:31 115-86-6 SVOA (LCMS) SW-846 8321 Analytical Method: EPA 8321 Preparation Method: 8321 Pace National - Mt. Juliet 2,4-D ND mg/kg 0.0263 0.00680 1.04 07/20/22 10:55 07/20/22 18:00 94-75-7 Dalapon ND mg/kg 0.0263 0.00417 1.04 07/20/22 10:55 07/20/22 18:00 127-20-8 2,4-DB ND mg/kg 0.0263 0.0119 1.04 07/20/22 10:55 07/20/22 18:00 94-82-6 Dicamba ND mg/kg 0.0263 0.00566 1.04 07/20/22 10:55 07/20/22 18:00 1918-00-9 Dichloroprop ND mg/kg 0.0263 0.00438 1.04 07/20/22 10:55 07/20/22 18:00 15165-67-0 Dinoseb ND mg/kg 0.0263 0.00261 1.04 07/20/22 10:55 07/20/22 18:00 88-85-7 MCPA ND mg/kg 0.0263 0.00448 1.04 07/20/22 10:55 07/20/22 18:00 94-74-6 MCPP ND mg/kg 0.0263 0.00308 1.04 07/20/22 10:55 07/20/22 18:00 7085-19-0 2,4,5-T ND mg/kg 0.0263 0.00901 1.04 07/20/22 10:55 07/20/22 18:00 93-76-5 2,4,5-TP (Silvex) ND mg/kg 0.0263 0.00225 1.04 07/20/22 10:55 07/20/22 18:00 93-72-1 Surrogates 2,4-DB-d3 (S) 90.9 % 70.0-130 1.04 07/20/22 10:55 07/20/22 18:00 1219802-46- REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/25/2022 09:57 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 22 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92614993 Sample: SPR-3 Lab ID: 92614993003 Collected: 07/13/22 13:09 Received: 07/13/22 14:25 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Total Solids 2540 G-2011 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 79.2 % 1 07/19/22 09:43 07/19/22 15:50 Date: 08/25/2022 09:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 22 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92614993 Sample: DUP-4 Lab ID: 92614993004 Collected: 07/13/22 00:00 Received: 07/13/22 14:25 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual OP Pesticides 8141 B Azinphos, methyl (Guthion) Bolstar Chlorpyrifos Coumaphos Total Demeton Diazinon Dichlorvos Dimethoate Disulfoton EPN (ENT) Ethoprop Parathion (Ethyl parathion) Fensulfothion Fenthion Malathion Merphos Methyl parathion Mevinphos Naled Phorate Ronnel Stirophos (Tetrachlorvinphos) Sulfotepp (ThiodiphosphoricAc TEPP Tokuthion (Prothiofos) Trichloronate Surrogates Triphenylphosphate (S) SVOA (LCMS) SW-846 8321 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DB-d3 (S) Analytical Method: EPA 8141 B Preparation Method: 3546 Pace National - Mt. Juliet ND mg/kg 0.137 0.0435 1 07/18/2217:02 07/19/2212:05 86-50-0 ND mg/kg 0.137 0.0204 1 07/18/2217:02 07/19/2212:05 35400-43-2 ND mg/kg 0.137 0.0215 1 07/18/2217:02 07/19/2212:05 2921-88-2 ND mg/kg 0.137 0.0332 1 07/18/2217:02 07/19/2212:05 56-72-4 ND mg/kg 0.0957 0.00798 1 07/18/2217:02 07/19/2212:05 8065-48-3 ND mg/kg 0.137 0.0308 1 07/18/2217:02 07/19/2212:05 333-41-5 ND mg/kg 0.137 0.0410 1 07/18/2217:02 07/19/2212:05 62-73-7 ND mg/kg 0.137 0.0457 1 07/18/2217:02 07/19/2212:05 60-51-5 ND mg/kg 0.137 0.0347 1 07/18/2217:02 07/19/2212:05 298-04-4 ND mg/kg 0.137 0.0377 1 07/18/2217:02 07/19/2212:05 2104-64-5 ND mg/kg 0.137 0.0161 1 07/18/2217:02 07/19/2212:05 13194-48-4 ND mg/kg 0.137 0.0224 1 07/18/2217:02 07/19/2212:05 56-38-2 ND mg/kg 0.137 0.0482 1 07/18/2217:02 07/19/2212:05 115-90-2 ND mg/kg 0.137 0.0182 1 07/18/2217:02 07/19/2212:05 55-38-9 ND mg/kg 0.137 0.0245 1 07/18/2217:02 07/19/2212:05 121-75-5 ND mg/kg 0.137 0.0317 1 07/18/2217:02 07/19/2212:05 150-50-5 ND mg/kg 0.137 0.0277 1 07/18/2217:02 07/19/2212:05 298-00-0 ND mg/kg 0.137 0.0314 1 07/18/2217:02 07/19/2212:05 7786-34-7 ND mg/kg 0.137 0.0656 1 07/18/2217:02 07/19/2212:05 300-76-5 ND mg/kg 0.137 0.0287 1 07/18/2217:02 07/19/2212:05 298-02-2 ND mg/kg 0.137 0.0204 1 07/18/2217:02 07/19/2212:05 299-84-3 ND mg/kg 0.137 0.0243 1 07/18/2217:02 07/19/2212:05 22248-79-9 ND mg/kg 0.137 0.0135 1 07/18/2217:02 07/19/2212:05 3689-24-5 ND mg/kg 1.37 0.215 1 07/18/2217:02 07/19/2212:05 107-49-3 ND mg/kg 0.137 0.0205 1 07/18/2217:02 07/19/2212:05 34643-46-4 ND mg/kg 0.137 0.0275 1 07/18/2217:02 07/19/2212:05 327-98-0 83.0 % 36.0-121 1 07/18/2217:02 07/19/2212:05 115-86-6 Analytical Method: EPA 8321 Preparation Method: 8321 Pace National - Mt. Juliet ND mg/kg 0.0273 0.00708 1 07/20/22 10:55 07/20/22 23:04 94-75-7 ND mg/kg 0.0273 0.00433 1 07/20/22 10:55 07/20/22 23:04 127-20-8 ND mg/kg 0.0273 0.0124 1 07/20/22 10:55 07/20/22 23:04 94-82-6 ND mg/kg 0.0273 0.00589 1 07/20/22 10:55 07/20/22 23:04 1918-00-9 ND mg/kg 0.0273 0.00455 1 07/20/22 10:55 07/20/22 23:04 15165-67-0 ND mg/kg 0.0273 0.00272 1 07/20/22 10:55 07/20/22 23:04 88-85-7 ND mg/kg 0.0273 0.00467 1 07/20/22 10:55 07/20/22 23:04 94-74-6 ND mg/kg 0.0273 0.00320 1 07/20/22 10:55 07/20/22 23:04 7085-19-0 ND mg/kg 0.0273 0.00938 1 07/20/22 10:55 07/20/22 23:04 93-76-5 ND mg/kg 0.0273 0.00234 1 07/20/22 10:55 07/20/22 23:04 93-72-1 105 % 70.0-130 1 07/20/22 10:55 07/20/22 23:04 1219802-46- REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/25/2022 09:57 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 22 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Wright's Executive Sales Pace Project No.: 92614993 Sample: DUP-4 Lab ID: 92614993004 Collected: 07/13/22 00:00 Received: 07/13/22 14:25 Matrix: Solid Results reported on a "wet -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Total Solids 2540 G-2011 Analytical Method: SM 254OG Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 73.2 % 1 07/19/22 09:43 07/19/22 15:50 Date: 08/25/2022 09:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 12 of 22 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92614993 QC Batch: 1896414 Analysis Method: EPA 8141 B QC Batch Method: 3546 Analysis Description: OP Pesticides 8141 B Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92614993001, 92614993002, 92614993003, 92614993004 METHOD BLANK: R3816711-1 Matrix: Solid Associated Lab Samples: 92614993001, 92614993002, 92614993003, 92614993004 Blank Reporting Parameter Units Result Limit MDL Analyzed Azinphos, methyl (Guthion) mg/kg ND 0.100 0.0318 07/19/22 02:01 Bolstar mg/kg ND 0.100 0.0149 07/19/22 02:01 Chlorpyrifos mg/kg ND 0.100 0.0157 07/19/22 02:01 Coumaphos mg/kg ND 0.100 0.0243 07/19/22 02:01 Total Demeton mg/kg ND 0.0700 0.00584 07/19/22 02:01 Diazinon mg/kg ND 0.100 0.0225 07/19/22 02:01 Dichlorvos mg/kg ND 0.100 0.0300 07/19/22 02:01 Dimethoate mg/kg ND 0.100 0.0334 07/19/22 02:01 Disulfoton mg/kg ND 0.100 0.0254 07/19/22 02:01 EPN (ENT) mg/kg ND 0.100 0.0276 07/19/22 02:01 Ethoprop mg/kg ND 0.100 0.0118 07/19/22 02:01 Parathion (Ethyl parathion) mg/kg ND 0.100 0.0164 07/19/22 02:01 Fensulfothion mg/kg ND 0.100 0.0353 07/19/22 02:01 Fenthion mg/kg ND 0.100 0.0133 07/19/22 02:01 Malathion mg/kg ND 0.100 0.0179 07/19/22 02:01 Merphos mg/kg ND 0.100 0.0232 07/19/22 02:01 Methyl parathion mg/kg ND 0.100 0.0203 07/19/22 02:01 Mevinphos mg/kg ND 0.100 0.0230 07/19/22 02:01 Naled mg/kg ND 0.100 0.0480 07/19/22 02:01 Phorate mg/kg ND 0.100 0.0210 07/19/22 02:01 Ronnel mg/kg ND 0.100 0.0149 07/19/22 02:01 Stirophos (Tetrachlorvinphos) mg/kg ND 0.100 0.0178 07/19/22 02:01 Sulfotepp (Thiodiphosphoric Ac mg/kg ND 0.100 0.00986 07/19/22 02:01 TEPP mg/kg ND 1.00 0.157 07/19/22 02:01 Tokuthion (Prothiofos) mg/kg ND 0.100 0.0150 07/19/22 02:01 Trichloronate mg/kg ND 0.100 0.0201 07/19/22 02:01 Triphenyl phosphate (S) % 105 36.0-121 07/19/22 02:01 Qualifiers LABORATORY CONTROL SAMPLE: Parameter R3816711-2 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Azinphos, methyl (Guthion) mg/kg 0.333 0.360 108 58.0-125 Bolstar mg/kg 0.333 0.348 105 64.0-120 Chlorpyrifos mg/kg 0.333 0.330 99.1 62.0-120 Coumaphos mg/kg 0.333 0.365 110 60.0-120 Total Demeton mg/kg 0.167 0.180 108 59.0-120 Diazinon mg/kg 0.333 0.300 90.1 49.0-120 Dichlorvos mg/kg 0.333 0.224 67.3 37.0-120 Dimethoate mg/kg 0.333 0.307 92.2 46.0-127 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/25/2022 09:57 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 22 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Wright's Executive Sales Pace Project No.: 92614993 LABORATORY CONTROL SAMPLE: R3816711-2 Parameter Units Disulfoton mg/kg EPN (ENT) mg/kg Ethoprop mg/kg Parathion (Ethyl parathion) mg/kg Fensulfothion mg/kg Fenthion mg/kg Malathion mg/kg Merphos mg/kg Methyl parathion mg/kg Mevinphos mg/kg Naled mg/kg Phorate mg/kg Ronnel mg/kg Stirophos (Tetrachlorvinphos) mg/kg Sulfotepp (ThiodiphosphoricAc mg/kg TEPP mg/kg Tokuthion (Prothiofos) mg/kg Trichloronate mg/kg Triphenyl phosphate (S) % QUALITY CONTROL DATA Spike Conc. LCS Result LCS % Rec % Rec Limits 0.333 0.326 97.9 60.0-121 0.333 0.336 101 60.0-121 0.333 0.339 102 59.0-120 0.333 0.311 93.4 62.0-120 0.333 0.347 104 58.0-123 0.333 0.337 101 61.0-121 0.333 0.312 93.7 59.0-120 0.333 0.329 98.8 59.0-120 0.333 0.304 91.3 63.0-120 0.333 0.247 74.2 50.0-120 0.333 0.140 42.0 10.0-125 0.333 0.324 97.3 60.0-120 0.333 0.327 98.2 62.0-120 0.333 0.314 94.3 62.0-120 0.333 0.350 105 62.0-122 3.33 0.281 8.44 10.0-135 0.333 0.334 100 63.0-120 0.333 0.318 95.5 62.0-120 101 36.0-121 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/25/2022 09:57 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 22 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92614993 QC Batch: 1898011 Analysis Method: EPA 8321 QC Batch Method: 8321 Analysis Description: SVOA (LCMS) SW-846 8321 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92614993001, 92614993002, 92614993003, 92614993004 METHOD BLANK: R3817633-2 Matrix: Solid Associated Lab Samples: 92614993001, 92614993002, 92614993003, 92614993004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 2,4-D mg/kg ND 0.0200 0.00518 07/20/22 16:13 Dalapon mg/kg ND 0.0200 0.00317 07/20/22 16:13 2,4-DB mg/kg ND 0.0200 0.00908 07/20/22 16:13 Dicamba mg/kg ND 0.0200 0.00431 07/20/22 16:13 Dichloroprop mg/kg ND 0.0200 0.00333 07/20/22 16:13 Dinoseb mg/kg ND 0.0200 0.00199 07/20/22 16:13 MCPA mg/kg ND 0.0200 0.00342 07/20/22 16:13 MCPP mg/kg ND 0.0200 0.00234 07/20/22 16:13 2,4,5-T mg/kg ND 0.0200 0.00686 07/20/22 16:13 2,4,5-TP (Silvex) mg/kg ND 0.0200 0.00171 07/20/22 16:13 2,4-DB-d3 (S) % 95 70.0-130 07/20/22 16:13 LABORATORY CONTROL SAMPLE: R3817633-1 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 2,4-D mg/kg 0.200 0.202 101 70.0-130 Dalapon mg/kg 0.200 0.219 109 70.0-130 2,4-DB mg/kg 0.200 0.190 95.0 70.0-130 Dicamba mg/kg 0.200 0.190 95.0 70.0-130 Dichloroprop mg/kg 0.200 0.194 97.0 70.0-130 Dinoseb mg/kg 0.200 0.229 115 70.0-130 MCPA mg/kg 0.200 0.212 106 70.0-130 MCPP mg/kg 0.200 0.188 94.0 70.0-130 2,4,5-T mg/kg 0.200 0.193 96.5 70.0-130 2,4,5-TP (Silvex) mg/kg 0.200 0.190 95.0 70.0-130 2,4-DB-d3 (S) % 103 70.0-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3817633-3 R3817633-4 MS MSD L1516222-03 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 2,4-D mg/kg ND 0.200 0.200 0.204 0.235 102 117 70.0-130 14.1 30 Dalapon mg/kg ND 0.200 0.200 0.238 0.272 119 136 70.0-130 13.3 30 2,4-DB mg/kg ND 0.200 0.200 0.232 0.257 116 129 70.0-130 10.2 30 Dicamba mg/kg ND 0.200 0.200 0.219 0.236 109 118 70.0-130 7.47 30 Dichloroprop mg/kg ND 0.200 0.200 0.224 0.239 112 119 70.0-130 6.48 30 Dinoseb mg/kg ND 0.200 0.200 0.228 0.212 114 106 70.0-130 7.27 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/25/2022 09:57 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 22 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: Wright's Executive Sales 92614993 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3817633-3 R3817633-4 MS MSD L1516222-03 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual MCPA mg/kg ND 0.200 0.200 0.240 0.259 120 130 70.0-130 7.62 30 MCPP mg/kg ND 0.200 0.200 0.211 0.225 105 113 70.0-130 6.42 30 2,4,5-T mg/kg ND 0.200 0.200 0.222 0.240 111 120 70.0-130 7.79 30 2,4,5-TP (Silvex) mg/kg ND 0.200 0.200 0.216 0.233 108 117 70.0-130 7.57 30 2,4-DB-d3 (S) % 95.5 106 70.0-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/25/2022 09:57 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 22 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Wright's Executive Sales Pace Project No.: 92614993 QC Batch: 1896888 Analysis Method: SM 2540G QC Batch Method: SM 2540 G Analysis Description: Total Solids 2540 G-2011 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92614993001, 92614993002, 92614993003, 92614993004 METHOD BLANK: R3817029-1 Matrix: Solid Associated Lab Samples: 92614993001, 92614993002, 92614993003, 92614993004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Solids % 0.00200 07/19/22 15:50 LABORATORY CONTROL SAMPLE: R3817029-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Solids % 50.0 50.0 100 85.0-115 SAMPLE DUPLICATE: R3817029-3 92614993003 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Solids % 79.2 79.5 0.309 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/25/2022 09:57 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 22 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: Wright's Executive Sales Pace Project No.: 92614993 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/25/2022 09:57 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 22 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: Wright's Executive Sales 92614993 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92614993001 SPR-1 3546 1896414 EPA 8141B 1896414 92614993002 SPR-2 3546 1896414 EPA 8141B 1896414 92614993003 SPR-3 3546 1896414 EPA 8141B 1896414 92614993004 DUP-4 3546 1896414 EPA 8141 B 1896414 92614993001 SPR-1 8321 1898011 EPA 8321 1898011 92614993002 SPR-2 8321 1898011 EPA 8321 1898011 92614993003 SPR-3 8321 1898011 EPA 8321 1898011 92614993004 DUP-4 8321 1898011 EPA 8321 1898011 92614993001 SPR-1 SM 2540 G 1896888 SM 2540G 1896888 92614993002 SPR-2 SM 2540 G 1896888 SM 2540G 1896888 92614993003 SPR-3 SM 2540 G 1896888 SM 2540G 1896888 92614993004 DUP-4 SM 2540 G 1896888 SM 2540G 1896888 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/25/2022 09:57 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 22 „- ace uLiF i rele: LN-t-KiVl-HUN1-UUU3 vU9 Sample Condition Upon Receipt Effective Date: 05/121202205/12/2022 Laboratory receiving samples: Asheville ❑ Edeno Greenwood ❑ Huntersville ] Raleigh❑ Mechanicsville[] Atlanta❑ Kernersville❑ SampleUpon Receipt Client Name: Project M WO : 92614993 Courier: ❑Fed Ex ❑LIPS ❑LISPS ❑Client III❑ III I I III III III IIII+ICommercial QPace ❑Other; 926141393 Custody Seat Present? Yes [QNo Seals Intact? ❑Yes ❑No Date/Initials Person Examining Contents Z± Z A� Packing Material; ❑Bubble Wrap EjBubble Bags ❑None ❑ Other Biological Tissue Frozen? AAP Thermometer: ❑Yes ❑ND R N A [ Gun ID: c� `�'Type of Ice: ❑Met ❑13lue ❑None Correction Factor: Cooler Temp: L`"5 Add/Subtract (°C) Cooler Temp Corrected (°C): USDA Regulated Soil l ❑ N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? [-]yes F7r�o Chain of Custody Present? ❑Yes ❑No ❑N/A Samples Arrived within Hold Time? i39es ❑No ❑N/A Short Hold Time Analysis (<72 hr.)? ❑yes [ No ❑N/A Rush Turn Around Time Requested? Dyes CTNn ❑N/A Sufficient Volume? Dyes ❑No ❑N/A Correct Containers Used? ❑Yes ❑No ❑N/A -Pace Containers Used? ❑yes El ❑N/A Containers Intact? .-❑Yes ❑No ❑N/A Dissolved analysis: Samples Field Filtered? [—]Yes []No ❑Nl/A Sample Labels Match COC? ❑Yes ❑No [_]N/A -Includes Date/Time/ID/Analysis Matrix: I-)L_ Headspace in UCLA Vials (?5-6mm)? ❑Yes ❑No Trip Blank Present? ❑Yes [-]No Trip Blank Custody Seals Present? ❑Yes ❑No COMMENTS/SAMPLE DISCREPANCY CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: i'rni. rt 11an, ,., cor M....L.,... Temp should be above freezing to 6'C ❑Samples out of temp criteria. Samples on ice, cooling process has begun Did samples originate From a foreign source (internationally, including Hawaii and Puerto Rico)? ❑Yes [,;” Lot ID of split containers: Date/Time: Date: Ltd le: Field Data Required? ❑Yes ❑No Qualtrax ID: 69614 Page 1 of 2 Page 20 of 22 LjLtr i iuv: r-ivv-rmm-nut,4 i-t mii vuI 5ampie C:oncl it! on Upon Receipt -ijace Effective Date: 05/12/202205/12/2022 dM *Check mark top half of box if pH and/or dechlorination is verified and project WO# ` 92-614993 within the acceptance range for preservation samples. PM -. AMB Due Date: 07/27/22 Exceptions: VOA, Coliform, TOC, Oil and Grease, ORO/8015 (water) OOC, LLHg MEW: 92-ECS RRL **Bottom half of box is to list number of bottles ***Check all unpreserved Nitrates for chlorine E E �; z ar C C E Ln 7 r£ o a m z a C L2' d J E 0 N 3 m a m z a Z G d Jcc C q Ur N N a m a Z v N a g m a ti = r1 7 (L a m _71_ u N V 2 O N aV. E "' N v1 a a m N V 2 z = Y a JC C 0 N Z M a m o o2i a a. 4 Z of u 4 E N rl a a a)m u A 2 2 Y d E 0 N ,.y m a tL a alla ip l;J b r a —y 7 r� 3 C Q a y _ r-S 7 .� t7 N a - 2 Q a — rl 2 ry l7 4 a t' � Ql Q J o tn N M i7 a N V Q v Lq N 2 Q °' --- ,..{ „ l7 a x is O N 2 E Q E o N fV m C7 4 Q z 2 2 E E o V1 N vai l7 a ¢ Z U Q E C] m l7 o ? m Q N !o Q O E 0 or'+ [� 7 2 a a a C Q Q E O q o� L] � Z Q M 4 Q E O V m l� n a ? d O N Q O > V m C7 a a 6 7 .�. W Q �_ M Y � 1 Q z LJ ip p. N 'A J E i!1 r4 F ^ I Q z u ti rn d J E p N ni 7 ry N z M 0- J E O N 2' m m y °^' a Q" 7 E Q J aE 7 o a y o 7 O C E VI z v N v v CL C C�C 4 Q E Q m o 1 3 4 5 -NNI 7 I x 9 10 I1 1� pH Adjustment Log for Preserved Samples Sample IA Type of Preservative pH upon receipt pate preservation adjusted Time preservation Amount of Preservative Lot 'q adjusted added cause: vvrienever mere is a cliscrepancyattecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DENR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Qualtrax ID; 69614 Page 2 of 2 Page 21 of 22 � I CHAIN -OF -CUSTODY 1 Analytical Request Document PaceMalXiral The Chain-oi-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. cae PIW gas {av Section A Section B Section C Required Client Information: Required Project Intonnation: Invoice Information: Page: 1 Cr 1 Report To: Samantha Szakasits Attention: Copy To: Company Name: Company: ECS Raleigh Address: 9001 Glenwood Avenue Raleigh, NO 27617 Address:Regulatory n Email: Purchase Order 0: Pace Quote: Phone, Fax: Project Name, �GvtXj6 µi S Pace Project Manager: angela.bamnAgpaceiabs-com, stow I Location ' Requested Due Date: Project M: i 4p3 r fxf /-V% Vf L , S Pace Profile 9, 9396-4 5 NC Re uested lysla Fllteted m a MATRIX coon — o COLLECTED Preservatives prinking water OW °' r; U z 6 WalM WT Wastewalw WW Ptotluci P a C U w N _ Z SAMPLE ID o'us°i'd oL START END N � One Character per box- W'no WP `- .. ¢ rt z m .o # (A-Z, 6.9 !, -) Sample Ids must be unique Ai, AR Othw OT Tissue TS a O a w TDATETIME w r w a z m Z m T Q m O U m m ¢ r� l.,• U R x m ccS 1— N DATE TIME N x z z z s !— m m¢ cc t1l3k, I ►A 7 J Zv '' ✓ I 2 r l a j'&F 1 a a 5 2- 2 L C I [Ell o Isni V/ 5b ( l33 ( ✓ I _ - 6 L C I'L50 130� 7 y L� ' I'd I S t l? - L-1 9 10 11 12 ADOMONAL COMMIMITS RELINQUISHED BY I AFFILIATION DATE TIME ACCEPMO BY/ AFFLIATION DATE ; TM SAMPLE CONDRI ]NS IWA MAL416 6V i i 'Gti Z I' ,t< �d4a lzz5 SAMPLER .NAME AND SIGNATURE O C c o � N PRINT Name of SAMPLER: w 8 Z 0 m T z SIGNATURE of SAMPLER: DATE Signed: H N N 0 N N N ZT N d