13023_Beacon Manufacturing_EMP Phase One Revised 2_20240314

NORTH CAROLINA BROWNFIELDS REDEVELOPMENT SECTION
ENVIRONMENTAL MANAGEMENT PLAN
This form is to be used to prepare an Environmental Management Plan (EMP) for projects in
the North Carolina Brownfields Redevelopment Section at the direction of a Brownfields
project manager.
The EMP is a standard requirement of a Brownfields Agreement (BFA). Its purpose is to clarify
actions to be taken during demolition and construction at Brownfields properties in an effort
to avoid delays in the event of the discovery of new contamination sources or other
environmental conditions. The EMP provides a means to document redevelopment plans and
environmental data for each applicable environmental medium to inform regulatory -compliant
decision -making at the site. As much detail as possible should be included in the EMP,
including contingency planning for unknowns. Consult your project manager if you have
questions.
Prospective Developers and/or their consultants must complete and submit this form and all
pertinent attachments, see checklist below, to their Brownfields project manager prior to any
earthmoving or other development -related activities that have the potential to disturb soil at
the Brownfields Property, including demolition. For the EMP to be valid for use, it must be
completed, reviewed by the Section, signed by all parties working on the project, and
approved by the Brownfields project manager. Failure to comply with the requirements of the
EMP could jeopardize project eligibility, or in the event of a recorded agreement, be cause for
a reopener.
The EMP is valid only for the scope of work described herein and must be updated to be
applicable for new phases of redevelopment or after significant changes in applicable
regulatory guidance. Risk characterization of a Brownfields Property to DEQ's written
satisfaction is required prior to EMP approval.
Voluntary Metrics Tab
The NC Brownfields Redevelopment Section updates estimated capital investment (from the
Brownfields Property Application) and estimated jobs created (from the Brownfields
Agreement) whenever possible. As a voluntary measure, you may opt to complete the below
information for capital investment and jobs created as estimated by your final redevelopment
plans for the Brownfields Property:
1. Estimated capital investment in redevelopment project: $4.65 million
2. Estimated jobs created:
a. Construction Jobs: 36
b. Full Time Post -Redevelopment Jobs: 8
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Table of Contents
NORTH CAROLINA BROWNFIELDS REDEVELOPMENT SECTION.................................................................. 1
ENVIRONMENTAL MANAGEMENT PLAN....................................................................................................
1
GENERAL INFORMATION........................................................................................................................
4
COMMUNICATIONS................................................................................................................................
4
NOTIFICATIONS TO THE BROWNFIELDS REDEVELOPMENT SECTION .....................................................
5
REDEVELOPMENT PLANS........................................................................................................................
5
CONTAMINATED MEDIA.........................................................................................................................
8
PART1. SOIL........................................................................................................................................
8
PART 2. GROUNDWATER..................................................................................................................
17
PART 3. SURFACE WATER..................................................................................................................
18
PART 4. SEDIMENT............................................................................................................................
18
PARTS. SOIL VAPOR.........................................................................................................................
19
PART6. INDOOR AIR.........................................................................................................................
20
VAPOR INTRUSION MITIGATION SYSTEM.............................................................................................
20
CONTINGENCYPLAN.............................................................................................................................
20
POST -REDEVELOPMENT REPORTING.....................................................................................................
22
APPROVAL SIGNATURES.......................................................................................................................
24
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So that the EMP provides value in protecting Brownfields eligibility and public health, the
preparer shall ensure that the following steps have been completed prior to submitting the
EMP for review. Any EMP prepared without completing all of the following is premature and may
be returned without comment.
® Site sampling and assessment that meets Brownfields' objectives is complete and has
been reviewed and approved by the Brownfields project manager.
® Specific redevelopment plans, even if conceptual, have been developed for the project,
submitted and reviewed by the Brownfields project manager.
Please submit, along with the completed EMP form, the following attachments, as relevant
and applicable to the proposed redevelopment:
® A set of redevelopment plans, including architectural/engineering plans, if available; if
not, conceptual plans may suffice if updated when detailed plans are drafted.
M A figure overlaying redevelopment plans on a map of the extent of contamination for
each media.
® Site grading plans that include a cut and fill analysis.
® A figure showing the proposed location and depth of impacted soil that would remain
onsite after construction grading.
❑ Any necessary permits for redevelopment (i.e. demolition, etc.).
® A detailed construction schedule that includes timing and phases of construction.
® Tabulated data summaries for each impacted media (i.e. soil, groundwater, soil gas,
etc.) applicable to the proposed redevelopment.
® Figures with the sampling locations and contamination extents for each impacted media
applicable to the proposed redevelopment.
❑ A full final grade sampling and analysis plan, if the redevelopment plan is final.
❑ If known, information about each proposed potential borrow soil source, such as aerial
photos, historic site maps, historic Sanborn maps, a site history, necessary for
Brownfields approval.
❑ Information and, analytical data if required, for quarries, or other borrow sources,
detailing the type of material proposed for import to the Brownfields Property.
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❑ A work plan for the sampling and analysis of soil to be brought onto the Brownfields
Property. Refer to Issue Resolution 15 in Brownfields Redevelopment Section
Guidelines.
❑ A map of the Brownfields Property showing the location of soils proposed for export
and sampling data from those areas.
❑ If a Vapor Intrusion Mitigation System (VIMS) is required by the Brownfields
Redevelopment Section, the VIMS plan will be signed and sealed by a NC Professional
Engineer. The VIMS Plan may also be submitted under separate cover.
GENERAL INFORMATION
Date: 2/13/2024 Revision Date (if applicable): 3/14/2024
Brownfields Assigned Project Name: Beacon Manufacturing Co.
Brownfields Project Number: 13023-09-011
Brownfields Property Address: 202 Whitson Avenue, Swannanoa, Buncombe County, North Carolina
Brownfields Property Area (acres): 42.29
Is Brownfields Property Subject to RCRA Permit? ....................... ❑ Yes ® No
If yes enter Permit No.: flick or tap here to enter text.
Is Brownfields Property Subject to a Solid Waste Permit ............ ❑ Yes ® No
If yes, enter Permit No.: Click or tap here to enter text.
COMMUNICATIONS
A copy of this EMP shall be distributed to all the parties below as well as any contractors or site workers
that may be exposed to site vapors, soil, groundwater, and/or surface water. Additionally, a copy of the
EMP shall be maintained at the Brownfields Property during redevelopment activities in an area that is
prominently accessible to site workers. NOTE, THE EMP DOES NOT TAKE THE PLACE OF A SITE -SPECIFIC
HEALTH AND SAFETY PLAN.
Prospective Developer (PD): Beacon Foundation, Inc.
Contact Person: Meredith Ellison
Phone Numbers: Office: 828-581-0475 Mobile: -lick or tap here to enter text.
Email: [e-mail]
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Contractor for PD: Velosolutions
Contact Person: Alon Karpman
Phone Numbers: Office: 917-304-2566
Email: TBD
Environmental Consultant: ECS Southeast, LLC
Contact Person: James C. Bevers, P.E.
Phone Numbers: Office: 828-665-2307
Email: [e-mail]
Brownfields Redevelopment Section Project Manager: Kris Riddle
Phone Numbers: Office: 828-251-7440
Email: [e-mail]
Mobile: Click or tap here to enter text.
Mobile: [phone]
Mobile: [phone]
Other DEQ Program Contacts (if applicable, i.e., UST Section, Inactive Hazardous Site Branch,
Hazardous Waste, Solid Waste):
-lick or tap here to enter text.
NOTIFICATIONS TO THE BROWNFIELDS REDEVELOPMENT SECTION
Written advance Notification Times to Brownfields project manager: Check each box to accept
minimum advance notice periods (in calendar days) for each type of onsitetask:
On -site assessment or remedial activities: .................................................... 10 days Prior
Construction or grading start: .......................................................................... 10 days Prior
Discovery of stained soil, odors, USTs, buried drums or waste, landfill, or other signs of previously
unknown contamination: ................................................................................ Within 48 hours
Implementation of emergency actions (e.g. dewatering, flood or soil erosion control measures in
area of contamination, ventilation of work zones): ................................... Within 48 hours
Installation of mitigation systems: ................................................................ 10 days Prior
Other notifications as required by local, state or federal agencies to implement redevelopment
activities: (as applicable): ................................................................................. Within 30 days
REDEVELOPMENT PLANS
1) Type of Redevelopment (check all that apply):
El Residential ❑Townhomes (Prior written DEQ approval REQUIRED regardless of ownership
structure) ®Recreational El Institutional ®Commercial ❑Office ❑Retail ❑ Industrial
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❑ Other specify:
Current plans are to redevelop the site with outdoor walking trails, bike track, open event lawn,
and mobile structures such as bandstand, bathrooms, bike shop, and office.
2) Check the following activities that will be conducted prior to commencing earth -moving activities
at the site:
® Review of historic maps (Sanborn Maps, facility maps)
❑ Conducting geophysical surveys to evaluate the location of suspect UST, fuel lines, utility
lines, etc.
❑ Interviews with employees/former employees/facility managers/neighbors
3) Summary of Redevelopment Plans (MANDATORY: attach detailed plans or conceptual plans, if
detailed plans are not available. EMP review without such information would be premature):
Provide brief summary of redevelopment plans, including demolition, removal of building
slabs/pavement, grading plans and planned construction of new structures:
The central portion of the property is proposed to be developed with a multi -use paved surface
bike park. The bike park will be open to the public free of charge and is designed for multiple
user groups (mountain bikes, skateboards, inline skates, and adaptive wheelchairs). Trail features
include berms, wooden features (bridges, wall rides, etc.), and jump lines. Ancillary uses will
include bike park pavilions, a temporary bike shop/park office, perimeter pedestrian trail,
parking, event lawn, food truck staging area, and general landscaping of the disturbed areas.
Perimeter Pedestrian Trail: the perimeter pedestrian path would generally travel the exterior
boundary line of the central property. This would be a gravel/natural surface path designed to
accommodate walking, running, biking, etc. for the general public.
Parking: Develop gravel parking areas to serve the bike park and surrounding uses along Whitson
Avenue. Integrate low impact development strategies to deal with stormwater runoff to include
bioswales, rain gardens, etc.
Bike Park: Construct a paved surface, multi -use bike park on approximately 4.7 acres of the
Beacon property. This will include land grading, construction of wooden bike park features,
drainage improvements, and final asphalt paving of the trail surface (approx. 4-6' wide). All
adjacent disturbed areas to be sodded with turf grass or capped with artificial turf surfacing.
Event Lawn: Transform a portion of the existing vacant land into a maintained lawn area capable
of hosting small events and supporting daily use by the general public (frisbee, dog walking,
movie nights, music events, portable stage, etc.).
General Landscaping: Areas disturbed in the scope of this project will be landscaped with native
trees, shrubs, grasses, living turf grass, or artificial turf.
Bike Park Pavilions: Construct one or more covered open air mobile pavilions in and around the
bike park.
Temporary Bike Shop/Office: Construct or place a temporary mobile building to house the bike
park operations office and bike shop (bike rentals, guides, merchandise, etc.). This initial
structure to be temporary in nature (converted shipping container, prefab modular, etc. and
elevated off the ground surface). This structure would include bathrooms and covered gathering
space for inclement weather.
Food Truck Staging Area: Create an area adjacent to the improved parking areas to host multiple
food trucks for events and daily use.
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The structures would be elevated a minimum of six inches off the ground surface with roofs and
placed on packed stone base course. Due to the separation between the ground surface and the
base of the structure, there should be ample space to allow for potential vapors to vent to the
atmosphere instead of potentially entering the elevated structures. Electrical and water services
will be provided to the bike shop/office and food trucks by exterior hookups/connections. Sewer
connections for the bike shop/office would be made via stickup plumbing into the elevated
building. Based on the elevated structures and nature of the connections to electrical, water, and
sewer services, it is not anticipated that utilities will be a conduit for vapors to enter the
structures. Sewer connections would be coordinated with Buncombe County MSD regulations.
Disturbed soils are to be finished/capped with grass, artificial turf, or mulched landscape
plantings. There is no anticipated export of soil material for the proposed project. On -site soil will
be used as much as possible. Import soil will be tested prior to being placed on the property as
described below. Other areas of the property are to be cleared to create a maintained
appearance. Invasive species to be removed per best management practices. The jurisdictional
stream on the property will not be impacted by the proposed project.
4) Do plans include demolition of structure(s)?:
❑ Yes ® No ❑ Unknown
❑ If yes, please check here to confirm that demolition will be conducted in accordance with
applicable legal requirements, including without limitation those related to lead and asbestos
abatement that are administered by the Health Hazards Control Unit within the Division of Public
Health of the North Carolina Department of Health and Human Services. If available, please
provide a copy of your demolition permit.
5) Are sediment and erosion control measures required by federal, state, or local regulations?
S&EC requirements can be found at: https://deg.nc.gov/about/divisions/energy-mineral-and-land-
resources/erosion-and-sediment-control/erosion-and-sediment-control-laws-and-rules
® Yes ❑ No ❑ Unknown
® If yes, please check here to confirm that earth -work will be conducted in accordance with
applicable legal requirements. If soil disturbance is necessary to install sediment and erosion
control measures, they may not begin until this EMP is approved.
6) Which category of risk -based screening level is used or is anticipated to be specified in the
Brownfields Agreement? Note: If children frequent the property, residential screening levels shall
be cited in the Brownfields Agreement for comparison purposes.
® Residential ❑ Non -Residential or Industrial/Commercial
7) Schedule for Redevelopment (attach construction schedule):
a) Construction start date: 3/10/2024
b) Anticipated duration (specify activities during each phase):
4 months
c) Additional phases planned? ® Yes ❑ No
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If yes, specify the start date and/or activities if known:
Start Date: No anticipated start date at this time. Additional work will be covered under a
separate EMP
Planned Activity:
1.1IUK UI LdP I ICI e to enter text.
Start Date: Click or tap to enter a date.
Planned Activity:
_I. L.,1 LPN I Lam, e to enter text.
Start Date: Click or tap to enter a date.
Planned Activity:
Click or tap here to enter text.
d) Provide the planned date of occupancy for new buildings: N/A
CONTAMINATED MEDIA
Please fill out the sections below, using detailed site plans, if available, or estimate using known areas
of contaminated soil and a conceptual redevelopment plan. Provide a figure overlaying new
construction onto figure showing contaminated soil and groundwater locations.
1) Contaminated Media on the Brownfields Property
Part 1. Soil:
®
Yes
❑ No
❑ Suspected
❑ Unknown
Part 2. Groundwater: ....................................
®
Yes
❑ No
❑ Suspected
❑ Unknown
Part 3. Surface Water:
®
Yes
❑ No
❑ Suspected
❑ Unknown ❑ N/A
Part 4. Sediment: ..........................................
©
Yes
❑ No
❑ Suspected
❑ Unknown ❑ N/A
Part 5. Soil Vapor: .........................................
❑
Yes
❑ No
® Suspected
❑ Unknown
Part 6. Sub -Slab Soil Vapor: ..........................
❑
Yes
❑ No
❑ Suspected
® Unknown
Part 7. Indoor Air: .........................................
❑
Yes
❑ No
❑ Suspected
® Unknown
2) For the Area of Proposed Redevelopment on the Brownfields Property, attach tabulated data
summaries for each impacted media and figure(s) with sample locations.
PART 1. SOIL
1) Known or suspected contaminants in soil (list general groups of contaminants):
Metals, PAHs
2) Depth of known or suspected contaminants (feet):
0-6 (up to 21 feet for arsenic and chromium)
3) Area of soil disturbed by redevelopment (square feet):
675,180
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4) Depths of soil to be excavated (feet):
5) Estimated volume of soil (cubic yards) to be excavated (attach grading plan):
178,400
6) Estimated volume of excavated soil (cubic yards) anticipated to be impacted by contaminants:
unknown
7) Estimated volume of contaminated soil expected to be disposed of offsite, if applicable:
0 — no planned export of soil from the site
PART 1.A. MANAGING ONSITE SOIL
If soil is anticipated to be excavated fromthe Brownfield Property, relocated on the Brownfields
Property, or otherwise disturbed during site grading or other redevelopment activities, please
provide a grading plan that clearly illustrates areas of cut and fill (approximate areas & volumes are
acceptable, if only preliminarydata available).
1) HAZARDOUS WASTE DETERMINATION:
a) Does the soil contain a LISTED WASTE as defined in the North Carolina Hazardous
Waste Section under 40 CFR Part 261.31-261.35?....................................... ❑Yes ®No
❑ If yes, explain why below, including the level of knowledge regarding processes
generating the waste (include pertinent analytical results as needed).
N/A
❑ If yes, do the soils exceed the "Contained -Out" levels in Attachment 1 of the
North Carolina Contained -In Policy? ................................................. ❑ Yes ® No
b) NOTE: IF SOIL MEETS THE DEFINITION OF A LISTED HAZARDOUS WASTE AND EXCEEDS
THE CONTAINED -OUT LEVELS IN ATTACHMENT 1 TO THE NORTH CAROLINA
CONTAINED -IN POLICY,THE SOIL MAY NOT BE RE -USED ONSITE AND MUST BE
DISPOSED OF IN ACCORDANCE WITH DEQ HAZARDOUS WASTE SECTION RULES AND
REGULATIONS.
c) Does the soil contain a CHARACTERISTIC WASTE? .................................... ❑ Yes ® No
❑ If yes, mark reason(s) why below (and include pertinent analytical results).
❑ Ignitability CIicK or tap nere to enter text
❑ Corrosivity Click or tap here to enter text.
❑ Reactivity Click or tap here to enter text.
❑ Toxicity Click or tap here to enter text.
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❑ TCLP results Click or tap here to enter text.
❑ Rule of 20 results (20 times total analytical results for an individual
hazardous constituent on TCLP list cannot, by test method, exceed regulatory
TCLP standard)
uicK or iap nere to enter text.
© If no, explain rationale:
Laboratory results of soil samples collected to date do not warrant a hazardous
waste classification.
d) NOTE: IF SOIL MEETS THE DEFINITION OF A CHARACTERISTIC HAZARDOUS WASTE, THE
SOIL MAYNOT BE RE -USED ONSITE AND MUST BE DISPOSED OF IN ACCORDANCE WITH
DEQ HAZARDOUS WASTE SECTION RULES AND REGULATIONS.
2) Screening criteria by which soil disposition decisions will be made (e.g., left in place, capped in
place with low permeability barrier, removed to onsite location and capped, removed offsite):
® Preliminary Health -Based Residential SRGs
❑ Preliminary Health -Based Industrial/Commercial SRGs
❑ Division of Waste Management Risk Calculator (For Brownfields Properties Only)
❑ Site -specific risk -based cleanup level. Please provide details of methods used for
determination/explanation.
N/A
Additional comments:
N/A
3) If known impacted soil is proposed to be reused within the Brownfields Property boundary,
please check the measures that will be utilized to ensure safe placement and documentation of
same. Please attach a proposed location diagram/site map.
® Provide documentation of analytical report(s) to Brownfields project manager.
© Provide documentation of final location, thickness and depth of relocated soil onsite map to
Brownfields project manager once known.
❑ Geotextile to mark depth of fill material.
Provide description of material:
l.I Ik-I% UI LCIP I ICI C lU CI IICI LU.
® Manage soil under impervious cap ® or clean fill
® Describe cap or fill:
The exposed surfaces will either be covered with impervious surfaces or 2 feet of clean fill
from an off -site source.
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® Confer with NC BF project manager if Brownfield Plat must be revised (or re -recorded if
actions are Post -Recordation).
© GPS the location and provide site map with final location.
❑ Other. Please provide a description of the measure:
lick or tap herF `- _` ­
4) Please describe the following action(s) to be taken during and following excavation and
management of site soils:
© Check to confirm that management of fugitive dust from site activities will be handled in
accordance with applicable local, state, and federal requirements._
Field screening of site soil
At a minimum, contractors shall be made aware of protocols should impacted soils (e.g. staining,
unusual odors, fill materials) be identified.
Describe the field screening method, frequency of field screening, person conducting field
screening:
During excavation of cut areas, environmental personnel (ECS) will be present to screen
the soils using visual and olfactory senses and a photoionization detector (PID) and/or
flame ionization detector (FID). Screening will be conducted at a frequency of one sample
every approximate 500 cubic yards.
Soil sample collection
❑ Yes
© Not anticipated - In order to avoid delays in construction, a plan shall be in place for sampling
of suspect soils should they be encountered during redevelopment. If soil sample collection is
not anticipated but the need to do so is identified during redevelopment, notify the Brownfields
project manager of the anticipated sample and report dates for scheduling purposes.
Describe the sampling method (e.g., in -situ grab, composite, stockpile, etc.) and confirm that all
procedures outlined in applicable DEQ guidance for assessment shall be followed Typically, at
least one representative sample (per 500 yd3for residential and 1,000 yd3 for commercial)
consisting of a 3 to 5-point composite sample with grab sample for VOCs based on the highest PID
reading is required to determine soil management options:
The excavated soil will either be sampled in place or stockpiled in accordance with Figure
1 (NCBP Diagram for Temporary Containment of Impacted or Potentially Impacted Soil)
and sampled. Sampling results will be used to determine if soil can be reused onsite,
used at another Brownfields site, and/or disposed of at a NCDEQ permitted facility.
However, export of soil is not anticipated for this project. One soil sample consisting of a
grab sample, and composite sample, will be collected per 1,000 cubic yards of impacted
soil, if identified.
Check applicable chemical analytes for soil samples:
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® Minimum Sample Requirements: Volatile organic compounds (VOCs) by EPA Method
8260; Semi -volatile organic compounds (SVOCs) by EPA Method 8270; and_Metals RCRA
List + Hexavalent Chromium by EPA Method 6020/7199
❑ Pesticides: Specify Analytical Method Number(s):
Click or tap here to enter text
❑ PCBs: Specify Analytical Method Number(s):
Click or tap here to enter text
❑ Other Constituents & Respective Analytical Method(s) (e.g. Herbicides):
...lick or tap here to enter tF
® Check to confirm that by the owner's signature and the North Carolina Professional
Engineer/Geologist sealing this EMP the consultant understands that no work plan for suspect
soil sample collection will be submitted beyond this EMP, and that it is the responsibility of the
sealing professional and property owner to ensure that all applicable guidelines and
methodologies are followed and reported to DEQ for determination and approval of soil
placement prior to final relocation.
If impacted soils above applicable PSRGs and/or site specific risk thresholds are proposed to be
relocated on -site, prior to final placement on -site, the following shall be submitted for DEQ
review/approval
- Analytical data that has been sampled in accordance with the above referenced frequency and
following procedures outlined in the most recent Brownfields Redevelopment Section
Environmental Site Assessment Work Plan Minimum Requirements Checklist (Checklist) and in
accordance with DEQ IHSB Guidelines for Assessment and Cleanup of Contaminated Sites
(Guidelines)
Figure outlining planned soil placement and any future site features including
buildings/hardscape/open areas
A North Carolina PE/PG recommendation of placement
Options
Onsite Placement without
Onsite placement under 2 ft
Impacts
conditions
of cap or clean filll, 2
All Constituents below applicable
PSRGs
X
Constituents3 below applicable
PSRGs; Metals below background
X
but above PSRGs
Constituents3 below applicable
PSRGs; Metals above Background
X
/PSRGs
Constituents above Applicable
X
PSRGs
1: Requires Prior Written DEQ Approval
2: VOC impacted soils above applicable PSRGs shall not be placed directly beneath building footprints
without prior written DEQ approval.
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3: Constituents indicate any samples evaluated for other than metals.
© Check to confirm that stockpiling of known or suspected impacted soils will be conducted in
accordance with Figure 1 of this EMP. Stockpile methodology should provide erosion control,
prohibiting contact between surface water/precipitation and contaminated soil, and preventing
contaminated runoff. Explain any variances or provide additional details as needed:
Excavated soil will be placed on a liner in a properly contained stockpile until the results are
obtained. The results of the sampling will determine if the soil can be reused on the property. The
soil cannot be spread on the property until the data is reviewed and Brownfields approval is
obtained.
© Final grade sampling of exposed native soil (i.e., soil that will not be under buildings or
permanent hardscape). Select chemical analyses for final grade samples with check boxes below
(Check all thatapply):
® Minimum Sample Requirements: Volatile organic compounds (VOCs) by EPA Method
8260; Semi -volatile organic compounds (SVOCs) by EPA Method 8270; and_Metals RCRA
List + Hexavalent Chromium by EPA Method 6020/7199
❑ Pesticides: Specify Analytical Method Number(s):
Click or tap here to enter text
❑ PCBs: Specify Analytical Method Number(s):
Click or tap here to enter text.
❑ Other Constituents & Respective Analytical Method(s) (e.g. Herbicides):
Click or tap here to enter text
Please provide a scope of work for final grade sampling, including a diagram of soil
sampling locations, number of samples to be collected, and brief sampling methodology.
Samples should be collected from 0-2 ft below ground surface, with the exception of VOCs
which should be taken from 1-2 ft below ground surface. Alternatively, indicate if a work
plan for final grade sampling may be submitted under separate cover.
A work plan for final grade sampling will be submitted under separate cover.
❑ If final grade sampling was NOT selected, please explain rationale:
Click or tap here to enter text
PART 1.13. IMPORTED FILL SOIL
NO SOIL MAY BE BROUGHT ONTO THE BROWNFIELDS PROPERTY WITHOUT PRIOR APPROVAL FROM
THE BROWNFIELDS REDEVELOPMENT SECTION. According to the Brownfields IR 15, "Documenting
imported soil (by sampling, analysis, and reporting in accordance with review and written approval
in advance by the Brownfields Redevelopment Section), will safeguard the liability protections
provided by the brownfields agreement and is in the best interest of the prospective
developer/property owner."
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Requirements for importing fill:
❑ Check to confirm that the import volumes outlined below have been confirmed based on
geotechnical evaluations.
1) Will fill soil be imported to the site? ................................................ ® Yes ❑ No ❑ Unknown
2) If yes, what is the estimated volume of fill soil to be imported?
3,000 cubic yards
3) If yes, what is the anticipated depth that fill soil will be placed at the property? (If a range
of depths, list the range.)
0-12 feet
PRIOR TO SOIL PLACEMENT AT THE BROWNFIELDS PROPERTY, a Soil Import Request must be
submitted for DEQ Brownfields review and approval. The request shall consist of a data
package that details:
- Fill source location/history (Phase I if available, current aerials, etc.)
- Analytical data that has been sampled in accordance with the below frequency and
following procedures outlined in the most recent Brownfields Redevelopment Section
Environmental Site Assessment Work Plan Minimum Requirements Checklist (Checklist)
and in accordance with DEQ IHSB Guidelines for Assessment and Cleanup of
Contaminated Sites (Guidelines)
- A table comparing the import soil to existing site concentrations
- A PE/PG recommendation of import
- All relevant attachments listed in the Checklist
Soil Import Sampling Requirements:
Source
Sample Frequency
I Sample Analysis
Virgin Material from DEQ
None (Contact Brownfields project manager for list of pre-
Brownfields Pre -
approved Quarries
approved Quarry
DEQ Permitted Quarry
At least one
VOCs, SVOCs, RCRA
(Not Brownfields Pre-
representative sample
Metals, any site specific
approved)
from area of planned
COCs (e.g. pesticides,
import
PCBs, etc.)
Other NC DEQ
At least one
Brownfields Property
representative sample
VOCs, SVOCs, RCRA
per 1,000 yd3 consisting
Metals, any site specific
Off -site
of a 3-point composite
COCs (e.g. pesticides,
unpermitted/regulated
sample with grab sample
PCBs, etc.)
property
for VOCs based on the
highest PID reading
Bulk Landscape Material
from Commercial Vendor
No Sampling Required
(i.e. topsoil)
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If other special considerations apply, discuss:
-III,I\ VI LOP IICIC lV CI IICI U=AL
© Check to confirm that by the owner's signature and the North Carolina Professional
Engineer/Geologist sealing this EMP the consultant understands that no work plan for suspect soil
sample collection will be submitted beyond this EMP, and that it is the responsibility of the sealing
professional and property owner to ensure that all applicable guidelines are followed and reported in
the Soil Import Request for DEQ approval. Failure to meet these requirements could result in
resampling and/or failure to approve import.
PART 1.C. SOIL EXPORT
NO SOIL MAY LEAVE THE BROWNFIELDS PROPERTY WITHOUT APPROVAL FROM THE
BROWNFIELDS REDEVELOPMENT SECTION. Failure to obtain approval may violate a brownfields
agreement causing a reopener or jeopardizing eligibility in the Section, endangering liability
protections and making said action possibly subject to enforcement. Justifications provided
below must be approved by the Section in writing prior to completing transport activities. Refer
to Brownfields IR 15 for additional details.
1) If export from the Brownfields Property is anticipated, export soil must be sampled at a
frequency of one sample per 1,000 yd' consisting of a 3-point composite sample with a
grab sample for VOCs based on the highest PID reading. Samples shall be analyzed at a
minimum for VOCs, SVOCs, and RCRA metals plus any site specific COCs.
PRIOR TO EXPORT FROM THE BROWNFIELDS PROPERTY, a Soil Export Request must be
submitted for DEQ Brownfields review and approval. The request shall consist of a Data
Package that details:
- Proposed Receiving Facility
- Analytical data that has been sampled in accordance with the above referenced
frequency and following procedures outlined in the most recent Brownfields
Redevelopment Section Environmental Site Assessment Work Plan Minimum
Requirements Checklist (Checklist) and in accordance with DEQ IHSB Guidelines for
Assessment and Cleanup of Contaminated Sites (Guidelines)
- A table comparing the export soil to concentrations on the receiving site concentrations
including risk comparison (Note that calculated risk cannot be increased on the receiving
site)
- A North Carolina PE/PG recommendation of export
- Written approval from the receiving site property owner representative for export
- All relevant attachments listed in the Checklist
Soil Export Options
Impacts
Options
Use as
Off -site disposal at
Off -site disposal
Off -site disposal at Subtitle
Beneficial Fill
other Brownfields
at LCID/CD
D MSW/Permitted
Property2,6,'
Landfill'.'
Landfarm4
All Constituents below
X
X
X
X
15
EMP Version 3, March 2023

applicable PSRGs
Constituents' below
applicable PSRGs; Metals
X
X
X
below background but
above PSRGs
Constituents' below
applicable PSRGs; Metals
X
X
X
above Background /PSRGs
Constituents above
X
X
Applicable PSRGs
1: Requires Prior Written DEQ Approval
2: VOC impacted soils above applicable PSRGs shall not be placed directly beneath building footprints
without prior written DEQ approval.
3: Requires comparison to site specific metals concentrations.
4: Facility to determine if they can accept soil within their permit.
5: Constituents indicate any samples evaluated for other than metals.
6: Requires written approval from receiving site property owner representative.
7. Site COCs must be in comparable concentrations to receiving site and not significantly raise risk of
the receiving site.
® Check to confirm that by the owner's signature and the North Carolina Professional
Engineer/Geologist sealing this EMP the consultant understands that no work plan for suspect soil
sample collection will be submitted beyond this EMP, and that it is the responsibility of the sealing
professional and property owner to ensure that all applicable guidelines are followed and reported in
the Soil Export Request for DEQ approval. Failure to meet these requirements could result in
resampling and/or failure to approve export.
If other special considerations apply, discuss:
Click or tap here to enter text.
PART 1.13. MANAGEMENT OF UTILITY TRENCHES
❑ Install liner between native impacted soils and base of utility trench before filling with clean fill
(Preferred)
® Last out, first in principle for impacted soils (if soil can safely be reused onsite and is not
hazardous waste), i.e., impacted soils are placed back at approximately the depths they were
removed from such that impacted soil is not placed at a greater depth than the original depth
from which it was excavated.
❑ Evaluate whether necessary to install barriers in conduits to prevent soil vapor transport,
and/or degradation of conduit materials due to direct impact with contaminants.
❑ If yes, provide specifications on barrier materials or provide the results of this evaluation in the
Vapor Mitigation Plan. Note that if vapor mitigation is planned for site buildings, utility corridors
will need to be evaluated as part of mitigation designs:
Click or tap here to enter tex-_
16
EMP Version 3, March 2023

® If no, include rationale here:
It is not anticipated that impacted soil will be encountered during the utility installations. If
impacted soil is encountered, it will be handled as detailed above and covered with a cap as
necessary. If previously unknown areas of impacted soil are identified, the Brownfields
Redevelopment Section will be notified within 48-hours of discovery. Additional sampling may
be required, based on nature of the unanticipated impacted soil.
❑ Unknown, details to be provided in the Vapor Mitigation Plan for site buildings
Other comments regarding managing impacted soil in utility trenches:
Not at this time
PART 2. GROUNDWATER
1) What is the depth to groundwater at the Brownfields Property?
Approximately 10 feet
2) What is the maximum depth of soil disturbance onsite?
2 feet
3) Is groundwater known to be contaminated by ®onsite ❑offsite ❑both or ❑unknown
sources? Describe source(s):
Operation of the former Beacon Manufacturing, Inc. textile mill causing chlorinated solvent
contamination.
4) What is the direction of groundwater flow at the Brownfields Property?
North towards the Swannanoa River
5) Will groundwater likely be encountered during planned redevelopment activities (e.g.
footer/utility construction or helical pilings?)
❑Yes ®No
If yes, describe these activities:
Although the final depth of redevelopment activities are not determined, based on the reported
depth to groundwater at the site (approximately 10 feet below grade) as compared to the
anticipated depth of site grading and cut, groundwater is not anticipated to be encountered.
In the event that groundwater is encountered during redevelopment activities (even if no is
checked above), list activities for contingent management of groundwater (e.g., dewatering
of groundwater from excavations or foundations, containerizing, offsite disposal, discharge to
sanitary sewer, NPDES permit, or sampling procedures).
If groundwater is encountered; groundwater will be characterized and managed in accordance
with local, state, and federal regulations. The volume of groundwater to be encountered is
unknown at this time. Deepest footing versus groundwater depth is currently unknown. Water
will either be allowed to re -infiltrate or be pumped into an approved container. Sampling and
analysis would be conducted as needed to characterize the water for disposal purposes based
on the requirements of the disposal facility. If the results of the samples collected do not
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EMP Version 3, March 2023

identify impacts, the water will be discharged onsite in accordance with local, state, and
federal regulations.
6) Are monitoring wells currently present on the Brownfields Property? ................. ❑X Yes ❑ No
If yes, are any monitoring wells routinely monitored through DEQ or other
agencies?
❑X Yes ❑ No
7) Please check methods to be utilized in the management of known and previously
unidentified wells.
® Abandonment of site monitoring wells in accordance with all applicable regulations. It
is the Brownfields Redevelopment Section's intent to allow proper abandonment of
well(s) as specified in the Brownfields Agreement, except if required for active
monitoring through another section of DEQ or the EPA.
® Location of existing monitoring wells marked
® Existing monitoring wells protected from disturbance
© Newly identified monitoring wells will be marked and protected from further
disturbance until notification to DEQ Brownfields can be made and approval for
abandonment is given.
8) Please provide additional details as needed:
None at this time
Please note, disturbance of existing site monitoring wells without approval by DEQ is not
permissible. If monitoring wells are damaged and/or destroyed, DEQ may require that the PD
be responsible for replacement of the well.
PART 3. SURFACE WATER
1) Is surface water present at the property? ® Yes ❑ No
2) If yes, attach a map showing the location of surface water at the Brownfields Property
3) Is surface water at the property known to be contaminated? ® Yes ❑ No ❑ Unknown
4) Will workers or the public be in contact with surface water during planned redevelopment
activities or as part of the final redevelopment? ❑ Yes ® No
5) In the event that contaminated surface water is encountered during redevelopment
activities, or clean surface water enters open excavations, list activities for management of
such events (e.g. flooding, contaminated surface water run-off, stormwater impacts):
If precipitation/surface water enters an open excavation, the water will be allowed to infiltrate
into the ground and/or containerized and managed in accordance with local, state, and federal
regulations.
PART 4. SEDIMENT
1) Are sediment sources present on the property? ® Yes ❑ No
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EMP Version 3, March 2023

2) If yes, is sediment at the property known to be contaminated? ® Yes ❑ No ❑ Unknown
3) Will workers or the public be in contact with sediment during planned redevelopment
activities? ❑ Yes ® No
4) Attach a map showing the location of known contaminated sediment at the property.
5) In the event that contaminated sediment is encountered during redevelopment activities, list
activities for management of such events (stream bed disturbance):
If stream beds were disturbed (not planned or anticipated); sediment will be characterized and
managed in accordance with local, state, and federal regulations.
PART 5. SOIL VAPOR
1) Do concentrations of volatile organic compounds at the Brownfields property exceed the
vapor intrusion screening levels (current version) in the following media:
Groundwater
Exterior Soil Vapor
Sub -Slab Soil Vapor
Residential
® Yes ❑ No
❑ Yes ❑ No
❑ Yes ❑ No
❑ Unknown
® Unknown
® Unknown
Commercial
® Yes ❑ No
❑ Yes ❑ No
❑ Yes ❑ No
❑ Unknown
® Unknown
® Unknown
2) Attach a map showing the locations of all soil vapor samples including any soil vapor
contaminants that exceeds screening levels and overlays planned site development features.
3) If applicable, at what depth(s) is exterior soil vapor known to be contaminated?
Soil vapor sampling has not been conducted at the property
4) If applicable, at what depth(s) is sub -slab soil vapor known to be contaminated?
❑0-6 inches ❑Other, please describe:
Unknown
5) Will workers encounter contaminated exterior or sub -slab soil vapor during planned
redevelopment activities? ❑ Yes ❑ No ❑X Unknown
In the event that apparent contaminated soil vapor is encountered (based on elevated PID
readings, unusual odors, etc.) during redevelopment activities (trenches, manways, basements or
other subsurface work,) list activities for management of such contact, INCLUDING notification to
DEQ within 48 hours of identification of the issue for determination of additional requirements:
Subsurface areas where work is being conducted will be monitored/field screened with a
photoionization detector (PID) or similar device. Although not anticipated based on sampling
results, should contaminated soil vapor be encountered, the area will be evacuated and allowed
to ventilate until it is confirmed that workers can safely return. NCDEQ Brownfields will be
notified if contaminated soil vapor is encountered within 48 hours of discovery.
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PART 6. INDOOR AIR
1) Are indoor air data available for the Brownfields Property? ❑ Yes ® No
2) If applicable, attach a map showing the location(s) where indoor air contaminants exceed site
screening levels.
3) If the structures where indoor air has been documented to exceed risk -based screening levels will
not be demolished as part of redevelopment activities, will workers encounter contaminated
indoor air during planned redevelopment activities? ❑ Yes ❑ No ❑ Unknown © N/A
❑ If no, include rationale here:
Click or tap here to enter text
4) In the event that contaminated indoor air is encountered during redevelopment activities, list
activities for management of such contact:
If contaminated indoor air is encountered based on field screening (odors or PID readings), work in
the area will cease and the area will be allowed to ventilate prior to continuing work in the area.
NCDEQ Brownfields will be notified if contaminated indoor air is encountered within 48 hours to
determine if further sampling, reporting, or mitigation is needed.
VAPOR INTRUSION MITIGATION SYSTEM
1) Is a vapor intrusion mitigation system (VIMS) proposed for this Brownfields Property?
❑ Yes ®No ❑ Unknown
© If no or unknown, include rationale here as well as plans for pre -occupancy sampling, as
necessary:
Slab on grade and/or permanent structures are not proposed at the property at this time.
If yes, ❑ VIMS Plan Attached or ❑ VIMS Plan to be submitted separately
If submitted separately provide date:
VIMS Plan shall be signed and sealed by a NC Professional Engineer and follow the DEQ
Brownfields Redevelopment Section's Vapor Intrusion Mitigation System Design Submittal
Requirements.
Note that approval of this EMP does not imply approval with any vapor intrusion mitigation land
use restrictions or requirements of the recorded or draft Brownfields Agreement and that
separate approval of mitigation measures will be required.
CONTINGENCY PLAN
In this section, please provide actions that will be taken to identify or manage unknown
potential new sources of contamination. During redevelopment activities, it is not uncommon
that unknown tanks, drums, fuel lines, landfills, orother waste materials are encountered.
20
EMP Version 3, March 2023

Notification to DEQ Brownfields project manager, UST Section, Fire Department, and/or other
officials, as necessary and appropriate, is required when new potential source(s) of
contamination are discovered. These Notification Requirements were outlined on Page 1 of this
EMP.
Should potentially impacted materials be identified that are inconsistent with known site
impacts, the DEQ Brownfields project manager will be notified, and a sampling plan will be
prepared based on the EMP requirements and site -specific factors. Samples will generally be
collected to document the location of the potential impacts.
Check the following chemical analysis that are to be conducted on newly identified releases:
® Minimum Sample Requirements: Volatile organic compounds (VOCs) by EPA Method 8260;
Semi -volatile organic compounds (SVOCs) by EPA Method 8270; and_Metals RCRA List +
Hexavalent Chromium by EPA Method 6020/7199
❑ Pesticides: Specify Analytical Method Number(s):
Click or tap here to enter text
❑ PCBs: Specify Analytical Method Number(s):
❑ Other Constituents & Analytical Method(s) (e.g. Herbicides)
Please note, if field observations indicate the need for additional analyses, they should
be conducted, even if not listed here.
Click or tap here to enter text
Please provide details on the proposed methods of managing the following commonly
encountered issues during redevelopment of Brownfields Properties.
Underground Storage Tanks — Note that UST Section guidelines must be followed for sample
frequency during UST closure. Unless damage to onsite structures to remain as part of
redevelopment would occur, USTs shall be removed from the Brownfields Property:
If encountered, the contents of an Underground Storage Tank (UST) will be evaluated, and based
on the contents, the UST will be removed and transported offsite for disposal/recycling. Any fluids
within a discovered UST will be removed using a vacuum truck and properly disposed of in
accordance with applicable regulations. Soil samples will be collected from the base and sidewalls
of the UST excavation and submitted for laboratory analysis of VOCs, SVOCs, and RCRA Metals plus
hexavalent chromium.
In the event that an unknown UST or impacts associated with an UST release are discovered at the
Site during redevelopment activities, the UST and/or UST related impacts will be addressed
through the Brownfields Program. DEQ Brownfields will be notified within 48 hours of the
discovery of the UST.
Sub -Grade Feature/Pit:
If sub -grade features, pits, etc. are encountered, the contractor will be instructed to stop work and
contact ECS to evaluate the feature. If a feature, pit, etc. is identified, the contents and the feature,
21
EMP Version 3, March 2023

pit, etc. itself will be removed and transported offsite for disposal. The contents would be sampled
for profile purposes prior to transportation and disposal. Following removal, soil samples will be
collected from the base of the excavation and submitted for laboratory analysis of VOCs, SVOCs,
RCRA Metals, and hexavalent chromium.
In the event that an unknown sub -grade feature, pit or associated impacts from a release are
discovered at the site during redevelopment activities, the feature and /or related impacts will be
addressed through the Brownfields Program. DEQ Brownfields will be notified within 48 hours of
the discovery.
Buried Waste Material — Note that if buried waste, non-native fill, or any obviously filled materials
is encountered, the DEQ Brownfields Redevelopment Section must be notified to determine if
investigation of landfill gases is required:
If buried waste material is encountered, the contractor will be instructed to stop work and contact
ECS to evaluate. Following evaluation, if confirmed, the waste will be removed, characterized, and
disposed of off -site. Soil samples will be collected from the base and sidewalls (one for every 10
feet of base/sidewall) of the excavated material and submitted for laboratory analysis of VOCs,
SVOCs, RCRA Metals, and hexavalent chromium.
If the event that buried waste material is encountered at the site during redevelopment activities,
the material and/or related impacts will be addressed through the Brownfields Program. DEQ
Brownfields will be notified within 48 hours of the discovery to determine if investigation of landfill
gases is required.
Re -Use of Impacted Soils Onsite:
If impacted soil is encountered during redevelopment activities and is able to be reused onsite
based on geotechnical characteristics, the soil reuse will be surveyed in and the plat will be
updated to include the location and depth of impacted soil. NCDEQ approval will be required prior
to reuse of impacted soil on the site.
If unknown, impacted soil is identified onsite, management onsite can be considered after the
project team provides the necessary information, outlined in Part I.A. Item 11, for Brownfields
project manager approval prior to final placement onsite.
If other potential contingency plans are pertinent, please provide other details or scenarios as
needed below:
N/A
POST -REDEVELOPMENT REPORTING
® Check this box to acknowledge that a Redevelopment Summary Report will be required for the
project. If the project duration is longer than one year, an annual update is required and will be
due by January 31 of each year, or 30 days after each one-year anniversary of the effective date of
this EMP (as agreed upon with the project manager). These reports will be required for as long as
physical redevelopment of the Brownfields Property continues, except that the final
Redevelopment Summary Report will be submitted within 90 days after completion of
redevelopment. Based on the estimated construction schedule, the first Redevelopment Summary
22
EMP Version 3, March 2023

Report is anticipated to be submitted on 1/31/2025
The Redevelopment Summary Report shall include environment -related activities since the last
report, with a summary and drawings, that describes:
1. actions taken on the Brownfields Property;
2. soil grading and cut and fill actions;
3. methodology(ies) employed for field screening, sampling and laboratory analysis of
environmental media;
4. stockpiling, containerizing, decontaminating, treating, handling, laboratory analysis and
ultimate disposition of any soil, groundwater or other materials suspected or confirmed
to be contaminated with regulated substances; and
5. removal of any contaminated soil, water or other contaminated materials (for example,
concrete, demolition debris) from the Brownfields Property (copies of all legally required
manifests shall be included).
X❑ Check box to acknowledge consent to provide a NC licensed P.G. or P.E. sealed, Redevelopment
Summary Report in compliance with the site's Brownfields Agreement.
23
EMP Version 3, March 2023

APPROVAL SIGNATURES
Brownfields Project Number:13023-09-011
Brownfields Project Name: Beacon Manufacturing Co.
ProspeceIeveloper: Beacon Foundation, Inc. Date 3/14/2024
Printed ame/Title/Company: Meredith Ellison
Consultant: ECS Southeast, LLC
Printed Name/Title/Company: James C. Bevers, Project
Manager
PE/PG Professional License #: 044440
Firm PE/PG License #: F-1519
Date 3/14/2024
Insert PE/PG Seal Above
3/14/2024
Manager: Kris Riddle Date Click or tap to enter a date:
24
EMP Version 3, March 2023

Figure 1
NCBP Diagram for Temporary
Containment of Impacted or Potentially
Impacted Soil
Cross -Section View
Top Plastic Cover Sheeting: Underliner: 1 layer, minimum of 10
(1 Layer, minimum: 10 mil thick) mil thick plastic
Berm
(Straw bales,
composted earth, etc.)
Land
Surface
\ z
Straw Bale Berm
0
Contaminated Soils
Map View
Weight
(If plastic
cover used)
I�
' ■ El j. . ................ ___ ................................ . ... lki Weight
O^
""' Contaminated Soils
.....................................................
000 o Plastic
\ Sheeting
Note: Adapted from NC DEQ UST Section "Guidelines for Ex Situ Petroleum Contaminated Soil Remediation" dated December, 1, 2013
25
EMP Version 3, March 2023

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PIN NUMBER: 969910036100000
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VELO TRACK = 46,904 SF
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TOTAL CUT SOILS = 178,400 CF
TOTAL FILL SOILS = 203,400 CF
TOTAL IMPORT = 3,000 CY
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THIS DOCUMENT IS THE PROPERTY OF FIND THE LINE STUDIOS, PLLC. IT IS TO BE USED FOR THIS SPECIFIC PROJECT ONLY AND IS NOT TO BE USED OTHERWISE WITHOUT OBTAINING WRITTEN CONSENT FROM FIND THE LINE STUDIOS, PLLC.

58-1-0
Depth 0-1'
Date 5/4/2004
Aluminum
56000 mg/Kg
Chromium
35 mg/Kg
Cobalt
17 mg/Kg
Iron
28000 m K
Thallium
12 m JK
SB-19-0
Depth
Date
Aluminum
Arsenic
Chromium
Cobalt
Iron
Thallium
SB-1.9-5
Depth
Date
Aluminum
Arsenic
Chromium
Cobalt
Iron
Thallium
SB-41-0
Depth
Date
Aluminum
Arsenic
Chromium
Cobalt
Iron
Thallium
SB-41-5
Depth
Date
Aluminum
Arsenic
Cadmium
Chromium
Cobalt
Iron
Thallium
SB-3-0
Depth
Date
D-1'
514/2004
Aluminum
39,000 mgJKg
Arsenic
2.8 rr
K
Chromium
3D mg/Kg
Cobalt
8 m
K
Iron
36 DDD m
K
Thallium
7.6 m
K
S-8
Depth 1-3'
Date 5/5/2011
Aluminum
19,600 mg/Kg
Arsenic
0.98 mg/Kg
Chromium
38.7 mg/Kg
Cobalt
11.6 mg/Kg
Iron
43,300 mg/Kg
Manganese
453 mg/Kg
f/ -
TOTAL CUT SOILS = 178,400 CF RFD
`z6 cF CI IT� � L>p 63' ¢ '•� _ TOTAL FILL SOILS= 203.400 CF GREEN
L
TOTAL IMPORT = 3,000 CY
•-' / P' _'�"'.�� f <sg - O T '- `' ,� G --- TOTAL EXPORT = 0 CY '
1
5/4/2004 N s> \66 r s, 22i 5f 14 N11 PRE -DEVELOPMENT IMPERMEABLE=76%
�. •pe8;: o$ i K NAIL �]� ,..
♦ _ L, % �`'---' - (BASED DEVELOPMENT
AERIAL)
46,000 mg/Kg y w ���, \ Y 2 MAGYdAILIN POST DEVELOPMENTIMPERMEABLE=7.4%
a'_- �� �13 PAVEMENT
2.9m K BG-'S�'= - - _RICH OND SAVE ! T ouND J~
40 mg/Kg E
10 mg/Kg
' ✓\�° _, P.B.2142, :
P 58
40,000 m PB24P88.2 m K J
t
,
!so�Nlp t $B-1 $B-3
N. 690.759 +z
5/4/2004 3(2011) h,l
47,D0D mg/Kg 1_ Ott i P.B. 2? 51
SB-21
Depth D-1'
Date 5/4/2DO4
Aluminum
23000 mg/Kg
Arsenic
1.6 mg/Kg
Chromium
27 mg/Kg
Cobalt
140 mg/Kg
Iron
30,000 mg/Kg
Manganese
13000 mg/Kg
Thallium
6.3 mg/Kg
S-9
Depth 3-5'
Date 5/612011
Aluminum
36A00 mg/Kg
Arsenic
1.3 mg/Kg
Chromium
32.5 mg/Kg
Iron
39,300 mg/Kg
2.1 m d K W
�S V���� 6 c1 =i�t ti� Imo-
37 mg/Kg \ �'' �., - ....- - s6 $ x Ms ' tt►� - 0� -
``;fit '4I. 1 � s *il-
v w l� se 1V-t-
9 mg/Kg
B-2 4
Depth
35,000 m K . O V� m 6 O .� w p i
2-14 1, T Date
s
8.0 m K a 2 .� A ES - ----- �- {
\ - - --�PIN 9699-10060 -"-
r r / ~ — �ti / \ ` \ Bz P.. P. 51
SB-19 'l
y SWANNANOA V � I Fv
SB� ' B 2 , //
`_-21 PROPERTIES L�� °- <•' I \ , V�,
D.B. 3949, P. 727 B l
P.B. 801P2,1854486
i
B.
P.
a ' / I M � soo�F<�T S
MpW21
5/4/2DO4 f`-•. P.B. 158, P. 1 j 29, P. 107
53,000 mg/Kg
—
4.2 m K
S1�
43 mg/Kg
$-2 B-4
w3, ,
10 mg/Kg
56ODD m K 1 3 a i5 ro
11.0 mg/Kg
5 6
0
5/4/2004 J _�� y ---- - — A G E �� 3 s1V
,
49,000 mg/Kg p E R �, - - - _ �,. % ( �17 C Y'
3.1 mg/Kg % P i aoCFFiC/ - - ooFmoT _
ITI
740 mg/Kg
45 mg/Kg -
9 mg/Kg s-
c
53,000 mg/Kg' }-- E
, t
-
12 0 mg/Kg —� N U _ -- SB-66 / u; — o�}� o alisa
I g w P, V E 3TH(� A G I
� // + 1 5 PCB
S R D. CH�
�i
1
5-2
Depth 3-51
Date 5/6/2011
Aluminum
18,800 mg/Kg
Arsenic
0.99 mg/Kg
Chromium
18.3 mg/Kg
Iron
22,800 mg/Kg
mg/Kg = millgrams per Kilogram
r CF FILL
-
j
Y ; .
r-
V se66
('
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Figure 1
Soil Sample Analytical Results in Close Proximity to Excavations
Scale
0 75 150 The Beacon Phase One
-N- Whitson Avenue
finch =150ft. Asheville, Buncombe County, North Carolina 28778
ECS Project No. 49-22023
4'
SB-50-0
Depth 0-1'
Date 5/4/2004
Aluminum
32,000 mg/Kg
Arsenic
2.4 mg/Kg
Chromium
23 mg/Kg
Cobalt
10 mg/Kg
Iron
27,000 mg/Kg
Manganese
520 mg/Kg
Thallium
8.1 mg/Kg
SB-66-0
Depth 0-1'
Date 5/4/2004
Aluminum
31,000 mg/Kg
Arsenic
2.0 mg/Kg
Chromium
32 /K
Cobalt
12 mg/Kg
Iron
37,000 mg/Kg
Manganese
1,700mg/Kg
Thallium
6.5 m /K
Dibenzo(a,h)anthracene
290.0 mg/Kg
SB-66-5
Depth 0-1'
Date 5/4/2004
Aluminum
20,300 mg /K
Chromium
l0 mg/Kg
Iron
17.000 m /K

58-1-0
Depth 0-1'
Date 5/4/2004
Aluminum
56000 mg/Kg
Chromium
35 mg/Kg
Cobalt
17 mg/Kg
Iron
28000 m K
Thallium
12 m JK
SB-19-0
Depth
Date
Aluminum
Arsenic
Chromium
Cobalt
Iron
Thallium
SB-1.9-5
Depth
Date
Aluminum
Arsenic
Chromium
Cobalt
Iron
Thallium
SB-41-0
Depth
Date
Aluminum
Arsenic
Chromium
Cobalt
Iron
Thallium
SB-41-5
Depth
Date
Aluminum
Arsenic
Cadmium
Chromium
Cobalt
Iron
Thallium
SB-3-0
Depth
Date
D-1'
514/2004
Aluminum
39,000 mgJKg
Arsenic
2.8 rr
K
Chromium
3D mg/Kg
Cobalt
8 m
K
Iron
36 DDD m
K
Thallium
7.6 m
K
S-8
Depth 1-3'
Date 5/5/2011
Aluminum
19,600 mg/Kg
Arsenic
0.98 mg/Kg
Chromium
38.7 mg/Kg
Cobalt
11.6 mg/Kg
Iron
43,300 mg/Kg
Manganese
453 mg/Kg
f/ -
TOTAL CUT SOILS = 178,400 CF RFD
`z6 cF CI IT� � L>p 63' ¢ '•� _ TOTAL FILL SOILS= 203.400 CF GREEN
L
TOTAL IMPORT = 3,000 CY
•-' / P' _'�"'.�� f <sg - O T '- `' ,� G --- TOTAL EXPORT = 0 CY '
1
5/4/2004 N s> \66 r s, 22i 5f 14 N11 PRE -DEVELOPMENT IMPERMEABLE=76%
�. •pe8;: o$ i K NAIL �]� ,..
♦ _ L, % �`'---' - (BASED DEVELOPMENT
AERIAL)
46,000 mg/Kg y w ���, \ Y 2 MAGYdAILIN POST DEVELOPMENTIMPERMEABLE=7.4%
a'_- �� �13 PAVEMENT
2.9m K BG-'S�'= - - _RICH OND SAVE ! T ouND J~
40 mg/Kg E
10 mg/Kg
' ✓\�° _, P.B.2142, :
P 58
40,000 m PB24P88.2 m K J
t
,
!so�Nlp t $B-1 $B-3
N. 690.759 +z
5/4/2004 3(2011) h,l
47,D0D mg/Kg 1_ Ott i P.B. 2? 51
SB-21
Depth D-1'
Date 5/4/2DO4
Aluminum
23000 mg/Kg
Arsenic
1.6 mg/Kg
Chromium
27 mg/Kg
Cobalt
140 mg/Kg
Iron
30,000 mg/Kg
Manganese
13000 mg/Kg
Thallium
6.3 mg/Kg
S-9
Depth 3-5'
Date 5/612011
Aluminum
36A00 mg/Kg
Arsenic
1.3 mg/Kg
Chromium
32.5 mg/Kg
Iron
39,300 mg/Kg
2.1 m d K W
�S V���� 6 c1 =i�t ti� Imo-
37 mg/Kg \ �'' �., - ....- - s6 $ x Ms ' tt►� - 0� -
``;fit '4I. 1 � s *il-
v w l� se 1V-t-
9 mg/Kg
B-2 4
Depth
35,000 m K . O V� m 6 O .� w p i
2-14 1, T Date
s
8.0 m K a 2 .� A ES - ----- �- {
\ - - --�PIN 9699-10060 -"-
r r / ~ — �ti / \ ` \ Bz P.. P. 51
SB-19 'l
y SWANNANOA V � I Fv
SB� ' B 2 , //
`_-21 PROPERTIES L�� °- <•' I \ , V�,
D.B. 3949, P. 727 B l
P.B. 801P2,1854486
i
B.
P.
a ' / I M � soo�F<�T S
MpW21
5/4/2DO4 f`-•. P.B. 158, P. 1 j 29, P. 107
53,000 mg/Kg
—
4.2 m K
S1�
43 mg/Kg
$-2 B-4
w3, ,
10 mg/Kg
56ODD m K 1 3 a i5 ro
11.0 mg/Kg
5 6
0
5/4/2004 J _�� y ---- - — A G E �� 3 s1V
,
49,000 mg/Kg p E R �, - - - _ �,. % ( �17 C Y'
3.1 mg/Kg % P i aoCFFiC/ - - ooFmoT _
ITI
740 mg/Kg
45 mg/Kg -
9 mg/Kg s-
c
53,000 mg/Kg' }-- E
, t
-
12 0 mg/Kg —� N U _ -- SB-66 / u; — o�}� o alisa
I g w P, V E 3TH(� A G I
� // + 1 5 PCB
S R D. CH�
�i
1
5-2
Depth 3-51
Date 5/6/2011
Aluminum
18,800 mg/Kg
Arsenic
0.99 mg/Kg
Chromium
18.3 mg/Kg
Iron
22,800 mg/Kg
mg/Kg = millgrams per Kilogram
r CF FILL
-
j
Y ; .
r-
V se66
('
,r- -��,: \ r.� t .✓_ r. G % i O Pam`969 If
GE _
o
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4 �2
A
`�' .B. 1 �23 .
r,
Figure 1
Soil Sample Analytical Results in Close Proximity to Excavations
Scale
0 75 150 The Beacon Phase One
-N- Whitson Avenue
finch =150ft. Asheville, Buncombe County, North Carolina 28778
ECS Project No. 49-22023
4'
SB-50-0
Depth 0-1'
Date 5/4/2004
Aluminum
32,000 mg/Kg
Arsenic
2.4 mg/Kg
Chromium
23 mg/Kg
Cobalt
10 mg/Kg
Iron
27,000 mg/Kg
Manganese
520 mg/Kg
Thallium
8.1 mg/Kg
SB-66-0
Depth 0-1'
Date 5/4/2004
Aluminum
31,000 mg/Kg
Arsenic
2.0 mg/Kg
Chromium
32 /K
Cobalt
12 mg/Kg
Iron
37,000 mg/Kg
Manganese
1,700mg/Kg
Thallium
6.5 m /K
Dibenzo(a,h)anthracene
290.0 mg/Kg
SB-66-5
Depth 0-1'
Date 5/4/2004
Aluminum
20,300 mg /K
Chromium
l0 mg/Kg
Iron
17.000 m /K

The Beacon Phase One 2.8.24
Proposed Construction Schedule
March 1, 2024
• Brownfields Phase One EMP approved; Buncombe County Zoning Permit Approved; NCG01 Land
Disturbance Permit Approved
• Site to be bush -hogged and forestry mulched
• Mobilize grading contractor
• Surveyor to lay out limits of disturbance and grading benchmarks
• General Contractor to establish temporary erosion control measures
• Mass grading begins
• Imported soils tested and placed on -site per Brownfields EMIR
• Parking area graded and graveled for construction phase
March 15, 2024
• VeloSolutions Bike Park contractor mobilizes
• Drainage conveyance and stormwater BMP's installed
• Final grading and shaping of trail system
April 1, 2024
• General contractor shapes perimeter walking trail and event lawn
• All outlying disturbed areas seeded with native seed blend during optimal seeding season
• VeloSolutions contractor continues with trail system development
• Landscaping of outlying areas begins
May 1, 2024
• Final grading and shaping of VeloSolutions Bike Park complete
• Event Lawn / Perimeter Trail grading finalized
• Mobile Bike Shop / Office / Stage placed on -site
• MEP systems connected to mobile units (mechanical, electrical, plumbing)
• Landscaping installation continues

June 1, 2024
• VeloSolutions contractor begins final asphalt paving of the trail system
• Perimeter trail final surfacing begins
• Final graveling of access drive / parking area
• Site testing as required by approved EMP
July 1, 2024
• Final surfacing of all trails complete
• Final landscaping complete
• Remove temporary erosion control measures once final soil stabilization is established
• Project complete with Brownfields Approval +/- July 15tn
Prepared By:
Rob Dull, PLA
Project Landscape Architect / Project Manager
General Contractor:
Beverly -Grant
Project Contact: Chris Smith
VeloSolutions Bike Park Contractor
Project Contact: Alon Karpmann

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EXHIBIT "B" to the Notice of
Brownfields Property - SURVEY PLAT
a...% s.-.w Fx
PROSPECTIVE DEVELOPER
$WANNANOA VALLEY PRDPEwPES. LLC
xry
�f�,FR`NEhICES
•a nx xoa �-rr
w w+,r W�A�a,Nar. P+v.ti
y �urwrv_„ ararayowa rc
5s Ici„w i+awMfie [rE buveynx FY
266 O.SWaSrl.MleanBP. rxL 2axp6
34iB'8P COrvr']�C2146
-090 re %LE I--10,

'A
Exhibit 2
The most recent environmental sampling at the Property reported in the Environmental
Reports occurred on November 16th & 171h, 2016. The following tables set forth, for
contaminants present at the Property above unrestricted use standards or screening levels, the
concentration found at each sample location, and the applicable standard or screening level.
Screening levels and groundwater standards are shown for reference only and are not set forth as
cleanup levels for purposes of this Agreement.
GROUNDWATER
Groundwater contaminants in micrograms per liter (the equivalent of parts per billion),
the standards for which are contained in Title 15A of the North Carolina Administrative Code,
Subchapter 2L (2L), Rule .0202, (April 1, 2013 version); or the 2L Groundwater Interim
Maximum Allowable Concentration (IMACs), (April 1, 2013 version):
Groundwater
Contaminant
Sample
Location
Date of Sampling
Concentration
Exceeding
Standard ( g/L)
Standard
(µg/L)
Antimony
MW-25
11/16&17/2015
3.19
1
Arsenic
MW-2
5/29/1994
20
10
4/18/1995
10
MW-3
5/29/1994
170
MW-4
5/29/1994
50
Barium
Dup-2(MW-25)
5/6/2011
707
700
MW-1
5/29/1994
1700
MW-2
5/29/1994
840
MW-3
5/29/1994
1910
MW-4
5/29/1994
3160
MW -4
6/2007
33.9
Beryllium
Dup-2(MW-25)
5/6/2011
4.8
4
MW-2
4/20/2004
10
Cadmium
MW-2
4/18/1995
20
2
MW-3
5/29/1994
20
4/18/1995
3.9
MW-4
5/29/1994
10
Chromium
MW-10
11/16&17/2015
13.0
10
MW-21
11/16&17/2015
39.5
MW-24
5/6/2011
15.2
Dup-2(MW-25)
5/6/2011
74.1
MW-1
5/29/1994
290
MW-2
5/29/1994
70
4/18/1995
80
13023-09-011Beacon Manufacturing Co. (09/29/2017)

MW-3
5/29/1994
250
4/18/1995
40
MW-4
5/29/1994
290
4/18/1995
10
6/2007
ND
MW-6
5/29/1994
80
Cobalt
MW-17
5/6/2011
8.2
1
MW-21
5/6/2011
7.5
MW-24
5/6/2011
14.8
MW-25
5/6/2011
11.6
Dup-2(MW-25)
5/6/2011
44
MW-8
5/5/2011
7.4
Dup-1(MW-8)
5/5/2011
7.6
MW-2
4/20/2004
60
1,1 Dichloroethene
MW-20
5/6/2011
12.9
7
MW-20
11 /16& 11 /17/2015
17.5
MW-1
5/29/1994
11
l l/1/2004
14
MW-4
5/29/1994
27
12/19/2000
8.5
l l /l /2004
9.6
6/2007
1.3
MW-4A
12/19/2000
8.2
Iron
MW-16
5/6/2011
401
300
MW-17
5/6/2011
6390
MW-18
5/6/2011
390
MW-20
5/6/2011
302
MW-21
5/6/2011
7970
MW-24
5/6/2011
26000
MW-25
11/16&17/2015
4410
Dup-2(MW-25)
5/6/2011
96500
MW-8
5/6/2011
18500
Du-1(MW-8)
5/6/2011
18800
MW-1
4/20/2004
620
MW-2
4/20/2004
4800
MW-3
4/20/2004
1400
MW-4
4/20/2004
840
MW-4
6/2007
70
MW-5
4/20/2004
4000
MW-6
4/20/2004
4100
Lead
MW-21
11/16&17/2015
22.3
15
13023-09-011/Beacon Manufacturing Co. (09/29/2017)

I
Lead
Dup-2(MW-25)
5/6/2011
40.3
MW-1
5/29/1994
207
MW-2
5/29/1994
72
4/18/1995
82
MW-3
5/29/1994
191
4/18/1995
55
MW-4
5/29/1994
214
4/20/2004
45
6/2007
12
MW-5
5/29/1994
47
MW-6
5/29/1994
54
Manganese
MW-25
11/16&17/2015
98.5
50
MW-13
5/6/2011
101
MW-16
5/6/2011
166
MW-17
5/6/2011
365
MW-18
5/6/2011
122
MW-20
5/6/2011
215
MW-21
5/6/2011
680
MW-24
5/6/2011
424
MW-25
5/6/2011
429
Dup-2(MW-25)
5/6/2011
1810
MW-8
5/6/2011
1690
Dup-l(MW-8)
5/6/2011
1710
MW-10
5/6/2011
320
MW-2
4/20/2004
6800
MW-3
4/20/2004
70
MW-5
4/20/2004
330
MW-6
4/20/2004
360
Mercury
MW-4
5/29/1994
2.7
1
Tetrachloroethene
MW-10
11/16&17/2015
6.13
0.7
5/5/2011
5.3
MW-16
5/6/2011
3.2
MW-17
5/6/2011
35.2
MW-18
5/6/2011
7.5
MW-20
11/16&17/2015
2.48
MW-21
11/16&17/2015
32.9
5/6/2011
77.8
MW-1
5/29/1994
2
11/1/2004
3.2
MW-4
12/19/2000
2
11 /1 /2004
1.8
6/2007
ND
13023-09-011/Beacon Manufacturing Co. (09/29/2017)

MW-4A
12/19/2000
5.8
Trichloroethene
MW-1
5/29/1994
10
3
l l / 1 /2004
4.8
MW-4
12/19/2000
6.3
7/3/2001
3.6
l l /1 /2004
3.1
6/2007
2
MW-4A
12/19/2000
8.3
MW-16
5/6/2011
20
MW-20
11/16&17/2015
3.95
MW-21
11/16&17/2015
3.88
5/6/2011
20.2
Vanadium
MW-17
5/6/2011
5.7
0.3
MW-21
5/6/2011
6.7
MW-24
5/6/2011
32.3
Dup-2(MW-25)
5/6/2011
152
Shading indicates a more recent sample is below the applicable standard.
GROUNDWATER -VAPOR INTRUSION
Groundwater contaminants with potential for vapor intrusion (VI) in micrograms per liter
(the equivalent of parts per billion), the vapor intrusion screening levels for which are derived
from the Residential Vapor Intrusion Screening Levels of the Division of Waste Management
June 2014 version):
Groundwater
Sample
Date of Sampling
Concentration
Non-
Residential
Contaminant with
Location
Exceeding
Residential VI
VI Screening
Potential for Vapor
Screening
Screening
Level'
Intrusion
Level (µg/L)
Level'
(µg/L)
(µg/L)
5/29/1994
8.4
35.5
8.14
Chloroform
MW-1
11/1/2004
0.66
35.5
8.14
MW-1
5/29/1994
0.3
0.563
5/29/1994
0.5
0.563
MW-3
4/18/1995.
ND
0.563
Mercury
0.134
5/29/1994
2.7
0.563
MW-4
4/18/1995
ND
0.563
MW-6
5/29/1994
0.2
0.563
MW-17
5/6/2011
35.2
48.4
Tetrachloroethene
11.5
MW-21
5/6/2011
77.8
48.4
11/16&11/17/2015
32.9
Trichloroethene
MW-9
5/5/2011
1.4
4.35
1.04
MW-16
5/6/2011
20
4.35
13023-09-011Beacon Manufacturing Co. (09/29/2017)
4

MW-20
11/16&11/17/2015
3.95
4.35
MW-21
5/6/2011
11/16&11/17/2015
20.2
3.88
4.35
MW-1
5/29/1994
10
4.35
l l /l /2004
4.8
4.35
12/19/2000
6.3
4.35
MW-4
7/3/2001
3.6
4.35
l l /l /2004
6/2007
3.1
2
4.35
MW-4A
12/19/2000
8.3
1 4.35
I Screening levels displayed for non -carcinogens are for a hazard quotient equal to 0.2. Screening levels
displayed for carcinogens are for a 1.0E-5 lifetime incremental cancer risk.
Shading indicates a more recent sample is below the applicable screening level.
SOIL
Soil contaminants in milligrams per kilogram (the equivalent of parts per million), the
screening levels for which are derived from the Preliminary Industrial Health- Based Soil
Remediation Goals of the Inactive Hazardous Sites Branch of DEQ's Superfund Section
(September 2015 version):
Soil
Contaminant
Sample
Location
Depth
(ft)
Date of
Sampling
Concentration
Exceeding
Screening
Level
(mpg)
Residential
Screening
Level'
(mg/kg)
Aluminum
MW-16
2-4
5/5/2011
18000
15000
MW-17
2-4
5/5/2011
23500
MW-24
3-5
5/5/2011
27600
S-2
3-5
5/6/2011
18800
S-7
2-4
5/5/2011
21700
S-8
1-3
5/5/2011
19600
S-9
3-5
5/6/2011
36400
5-10
3-5
5/5/2011
25800
5-15
3-5
5/6/2011
26900
5-17
3-5
5/5/2011
31900
SB-41-0
0-1
5/4/2004
53000
SB-41-5
5-6
5/4/2004
49000
SB-19-0
0-1
5/4/2004
46000
SB-19-5
5-6
5/4/2004
47000
SB-1-0
0-1
5/4/2004
56000
SB-3-0
0-1
1 5/4/2004
39000
13023-09-011/Beacon Manufacturing Co. (09/29/2017)

Soil
Contaminant
Sample
Location
Depth
(ft)
Date of
Sampling
Concentration
Exceeding
Screening
Level
(mg/kg)
Residential
Screening
Level'
(mg/kg)
SB-11-0
0-1
5/4/2004
54000
SB-21-0
0-1
5/4/2004
23000
SB-68-0
0-1
5/4/2004
54000
SB-55-0
0-1
5/4/2004
19000
SB-66-0
0-1
5/4/2004
31000
SB-66-5
0-1
5/4/2004
20000
SB-58-0
0-1
5/4/2004
35000
SB-58-5
5-6
5/4/2004
36000
SB-60-0
0-1
5/4/2004
27000
SB-60-5
5-6
5/4/2004
15000
SB-49-0
0-1
5/4/2004
30000
SB-49-5
5-6
5/4/2004
45000
SB-50-0
0-1
5/4/2004
32000
Arsenic
MW-24
3-5
5/5/2011
2.4
0.68
MW-25
3-5
5/5/2011
5.1
S-2
3-5
5/6/2011
0.99
S-7
2-4
5/5/2011
1.8
S-8
1-3
5/5/2011
0.98
S-9
3-5
5/6/2011
1.3
S-10
3-5
5/5/2011
1.4
S-11
2-4
5/5/2011
1.7
S-16
3-5
5/6/2011
0.92
S-17
3-5
5/5/2011
2.2
SW-ls
SED
6/l/2007
1.3
SW-2s
SED
6/l/2007
1.3
SW-3s
SED
6/l/2007
0.71
SB-41-0
0-1
5/4/2004
4.2
SB-41-5
5-6
5/4/2004
3.1
SB-19-0
0-1
5/4/2004
2.9
SB-19-5
5-6
5/4/2004
2.1
SB-3-0
0-1
5/4/2004
2.8
SB-11-0
0-1
5/4/2004
3
SB-21-0
0-1
5/4/2004
1.6
SB-68-0
0-1
5/4/2004
3
SB-55-0
0-1
5/4/2004
1.8
SB-66-0
0-1
5/4/2004
2
SB-60-0
0-1
5/4/2004
2.4
13023-09-011Beacon Manufacturing Co. (09/29/2017)

LI�5
Soil
Contaminant
Sample
Location
Depth
(ft)
Date of
Sampling
Concentration
Exceeding
Screening
Level
(mpg)
Residential
Screening
Level'
(mg/kg)
SB-60-5
5-6 1
5/4/2004
4.6
SB-49-0
0-1
5/4/2004
1.9
SB-49-5
5-6
5/4/2004
3.5
SB-50-0
0-1
5/4/2004
2.4
B-1-18
18
l l/l/2000
1.2
B-2-4
4
l l/ 1 /2000
4.5
B-2-19
19
ll/1/2000
6.9
B-3-21
21
l l / 1 /2000
1.9
B-4-3
3
l l /l /2000
1.3
B-5-3
3
ll/l/2000
1.5
B-6-3
3
l l /l /2000
5.7
BG-7
N/A
11/1/1994
2.2
BG-8
N/A
11/1/1994
2.7
BG-9
N/A
11/1/1994
2.8
BG-10
N/A
11/1/1994
3.7
B-30-15
15
8/24/1994
1.2
B-31-5
5
8/24/1994
1.1
B-32-5
5
8/24/1994
1.8
B-32-51)
5
8/24/1994
2.4
B-32-9
9
8/24/1994
0.86
Benzo(a)anthracene
S-11
2-4
5/5/2011
556
160
SW-ls
SED
6/l/2007
700
SW-3s
SED
6/l/2007
1600
SB-55-0
0-1
5/4/2004
170
SB-60-5
5-6
5/4/2004
980
Benzo(a)pyrene
S-11
2-4
5/5/2011
525
16
SW-ls
SED
6/1/2007
770
SW-3s
SED
6/1/2007
1600
SB-55-0
0-1
5/4/2004
130
SB-60-5
5-6
5/4/2004
590
Benzo(b)fluoranthene
S-11
2-4
5/5/2011
435
160
SW-ls
SED
6/l/2007
750
SW-3s
SED
6/l/2007
1300
SB-55-0
0-1
5/4/2004
180
SB-60-5
5-6
5/4/2004
1000
Dibenzo(a,h)anthracene
SB-66-0
0-1
5/4/2004
0
2916
SB-60-5
5-6
5/4/2004
150
13023-09-011/Beacon Manufacturing Co. (09/29/2017)

Soil
Contaminant
Sample
Location
Depth
(ft)
Date of
Sampling
Concentration
Exceeding
Screening
Level
(mg/kg)
Residential
Screening
Level'
(mg/kg)
Indena(1,2,3-c,d)pyrene
SB-66-0
0-1
5/4/2004
290
160
SB-60-5
5-6
5/4/2004
380
Cadmium
SB-41-5
5-6
5/4/2004
740
14
Chromium
MW-16
2-4
5/5/2011
20.4
0.3
MW-17
2-4
5/5/2011
32.2
MW-24
3-5
5/5/2011
14.0
MW-25
3-5
5/5/2011
48.2
S-2
3-5
5/6/2011
18.3
S-7
2-4
5/5/2011
21.4
0.3
S-8
1-3
1 5/5/2011
38.7
S-9
3-5
5/6/2011
32.5
S-10
3-5
5/5/2011
27.8
S-11
2-4
5/5/2011
11.3
S-15
3-5
5/6/2011
76.3
S-16
3-5
5/6/2011
13.6
S-17
3-5
5/5/2011
21.2
SS-4
SED
5/6/2011
24.4
SS-5
SED
5/6/2011
17.2
SS-6
SED
5/6/2011
14.3
SS-7
SED
5/6/2011
11.3
SW-ls
SED
6/1/2007
26
SW-2s
SED
6/l/2007
48
SW-3s
SED
6/l/2007
27
SB-41-0
0-1
5/4/2004
43
SB-41-5
5-6
5/4/2004
45
SB-19-0
0-1
5/4/2004
40
SB-19-5
5-6
5/4/2004
37
SB-1-0
0-1
5/4/2004
35
SB-3-0
0-1
5/4/2004
30
SB-11-0
0-1
5/4/2004
38
SB-21-0
0-1
5/4/2004
27
SB-68-0
0-1
5/4/2004
120
SB-55-0
0-1
5/4/2004
18
SB-66-0
0-1
5/4/2004
32
SB-66-5
0-1
5/4/2004
10
SB-58-0
0-1
5/4/2004
22
SB-58-5
5-6
5/4/2004
24
13023-09-011/Beacon Manufacturing Co. (09/29/2017)

-A,
Soil
Contaminant
Sample
Location
Depth
(ft)
Date of
Sampling
Concentration
Exceeding
Screening
Level
(mg/kg)
Residential
Screening
Level'
(mg/kg)
SB-60-0
0-1
5/4/2004
23
SB-60-5
5-6
5/4/2004
70
SB-49-0
0-1
5/4/2004
20
SB-49-5
5-6
5/4/2004
29
SB-50-0
0-1
5/4/2004
23
B-1-18
18
ll/1/2000
26
B-2-4
4
ll/1/2000
43
B-2-19
19
ll/l/2000
14
B-3-21
21
ll/l/2000
7.8
0.3
B-4-3
3
ll/l/2000
14
B-5-3
3
ll/l/2000
29
B-6-3
3
ll/l/2000
14
BG-7
N/A
11/1/1994
23.1
BG-8
N/A
11/1/1994
29.4
BG-9
N/A
11/1/1994
34.9
BG-10
N/A
11/l/1994
31.7
SS-1
SED
9/1/1994
17
B-30-5
5
8/24/1994
38.5
B-30-15
15
8/24/1994
4
B-31-5
5
8/24/1994
13.2
B-32-5
5
8/24/1994
17.2
B-32-513
5
8/24/1994
19.4
B-32-9
9
8/24/1994
13.6
B-33-5
5
8/24/1994
12
Cobalt
MW-17
2-4
5/5/2011
8.7
4.6
MW-25
3-5
5/5/2011
8.3
S-8
1-3
5/5/2011
11.6
S-15
3-5
5/6/2011
10.3
S-16
3-5
5/6/2011
9.8
SB-41-0
0-1
5/4/2004
10
SB-41-5
5-6
5/4/2004
9.4
SB-19-0
0-1
5/4/2004
4.9
SB-19-5
5-6
5/4/2004
7.1
SB-1-0
0-1
5/4/2004
17
SB-3-0
0-1
5/4/2004
8
SB-11-0
0-1
5/4/2004
12
SB-21-0
0-1
5/4/2004
1 140
13023-09-011/Beacon Manufacturing Co. (09/29/2017)

Soil
Contaminant
Sample
Location
Depth
(ft)
Date of
Sampling
Concentration
Exceeding
Screening
Level
(mg/kg)
Residential
Screening
Lever
(mg/kg)
SB-68-0
0-1
5/4/2004
16
SB-55-0
0-1
5/4/2004
7
SB-66-0
0-1
5/4/2004
12
SB-58-0
0-1
5/4/2004
7.8
SB-58-5
5-6
5/4/2004
13
SB-60-0
0-1
5/4/2004
11
SB-60-5
5-6
5/4/2004
19
SB-49-0
0-1
5/4/2004
12
SB-49-5
5-6
5/4/2004
12
4.6
SB-50-0
0-1
5/4/2004
10
Iron
MW-16
2-4
5/5/2011
33700
11000
MW-17
2-4
5/5/2011
55700
MW-25
3-5
5/5/2011
27800
S-2
3-5
5/6/2011
22800
S-7
2-4
5/5/2011
20900
S-8
1-3
5/5/2011
43300
S-9
3-5
5/6/2011
39300
S-10
3-5
5/5/2011
17100
S-11
2-4
5/5/2011
14900
S-15
3-5
5/6/2011
49800
S-17
3-5
5/5/2011
11600
SS-4
SED
5/6/2011
18100
SS-6
SED
5/6/2011
25300
SS-7
SED
5/6/2011
14500
SW-ls
SED
6/l/2007
26000
SW-2s
SED
6/l/2007
34000
SW-3s
SED
6/1/2007
24000
SB-41-0
0-1
5/4/2004
56000
SB-41-5
5-6
5/4/2004
53000
SB-19-0
0-1
5/4/2004
40000
SB-19-5
5-6
5/4/2004
35000
SB-1-0
0-1
5/4/2004
28000
SB-3-0
0-1
5/4/2004
36000
SB-11-0
0-1
5/4/2004
65000
S13-21-0
0-1
5/4/2004
30000
SB-68-0
0-1
5/4/2004
60000
SB-55-0
0-1
5/4/2004
20000
13023-09-011/Beacon Manufacturing Co. (09/29/2017)
10

y
Soil
Contaminant
Sample
Location
Depth
(ft)
Date of
Sampling
Concentration
Exceeding
Screening
Level
(mpg)
Residential
Screening
Level'
(mg/kg)
SB-66-0
0-1
1 5/4/2004
37000
SB-66-5
0-1
5/4/2004
17000
SB-58-0
0-1
5/4/2004
22000
SB-58-5
5-6
5/4/2004
49000
SB-60-0
0-1
5/4/2004
46000
SB-60-5
5-6
5/4/2004
22000
SB-49-0
0-1
5/4/2004
34000
SB-49-5
5-6
5/4/2004
38000
11000
SB-50-0
0-1
5/4/2004
27000
Manganese
S-8
1-3
5/5/2011
453
360
S-15
3-5
5/6/2011
441
SB-21-0
0-1
5/4/2004
13000
SB-55-0
0-1
5/4/2004
400
SB-66-0
0-1
5/4/2004
1700
SB-58-0
0-1
5/4/2004
1500
SB-60-0
0-1
5/4/2004
1200
SB-60-5
5-6
5/4/2004
380
SB-49-0
0-1
5/4/2004
1100
SB-50-0
0-1
5/4/2004
520
Mercury
B-32-5
5
8/24/1994
3.8
1.9
Thallium
SW-ls
SED
6/l/2007
3.3
0.16
SW-2s
SED
6/l/2007
2.6
SW-2s
SED
6/l/2007
3
SB-41-0
0-1
5/4/2004
11
SB-41-5
5-6
5/4/2004
12
SB-19-0
0-1
5/4/2004
8.2
SB-19-5
5-6
5/4/2004
8
SB-1-0
0-1
5/4/2004
12
SB-3-0
0-1
5/4/2004
7.6
SB-11-0
0-1
5/4/2004
12
SB-21-0
0-1
5/4/2004
6.3
SB-68-0
0-1
5/4/2004
10
SB-55-0
0-1
5/4/2004
6.3
SB-66-0
0-1
5/4/2004
6.5
SB-58-0
0-1
5/4/2004
3.4
SB-58-5
5-6
5/4/2004
12
SB-60-0
0-1
5/4/2004
10
13023-09-011/Beacon Manufacturing Co. (09/29/2017)
11

raj
Soil
Sample
Depth
Date of
Concentration
Residential
Contaminant
Location
(ft)
Sampling
Exceeding
Screening
Screening
Level'
Level
(mg/kg)
(mpg)
SB-60-5
5-6
1 5/4/2004
6.7
SB-49-0
0-1
5/4/2004
7.9
SB-49-5
5-6
5/4/2004
9.5
SB-50-0
0-1
5/4/2004
8.1
Vanadium
SB-68-0
0-1
5/4/2004
160
78
SB-60-5
5-6
5/4/2004
130
'Screening levels displayed for non -carcinogens are for a hazard quotient equal to 0.2. Screening levels
displayed for carcinogens are for a 1.0E-6 lifetime incremental cancer risk.
13023-09-011/Beacon Manufacturing Co. (09/29/2017)
12

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1111111811111111011111
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4

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
May 20, 2011
Mr. Steve Irminger
Irminger Consulting
7015 Erinbrook Road
Concord, NC 28025
RE: Project: Swannanoa
Pace Project No.: 9293679
[phone]
Dear Mr. Irminger:
Enclosed are the analytical results for sample(s) received by the laboratory on May 07, 2011. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
[phone]
Page 1 of 227

IF
acmnalytical
www.pacolabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/LELAP Certification #: 04034
New Jersey Certification #: NC012
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pennsylvania Certification #: 68-00784
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Connecticut Certification M PH-0106
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
New Jersey Certification #: NC011
North Carolina Bioassay Certification #: 9
North Carolina Drinking Water Certification #: 37712
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
South Carolina Drinking Water Cert. #: 99006003
Virginia Certification #: 00213
Connecticut Certification #: PH-0104
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DHH Drinking Water # LA 100031
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 40
Pennsylvania Certification #: 68-03578
South Carolina Bioassay Certification #: 99030002
South Carolina Certification #: 99030001
Virginia Certification #: 00072
West Virginia Certification #: 356
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
♦E OA�9
0
�i
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Lab ID Sample ID
9293679001 MW-10
9293679002 MW-9
9293679003 MW-8
9293679004 DUP-1
9293679005 MW-13
9293679006 MW-14
9293679007 MW-16
9293679008 MW-17
9293679009 MW-18
9293679010 MW-20
9293679011 MW-21
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Method
EPA 6010
EPA 7470
EPA 8260
EPA 6010
EPA 7470
EPA 8260
EPA 6010
EPA 7470
EPA 8260
EPA 6010
EPA 7470
EPA 8260
MADEP VPH
EPA 6010
EPA 7470
EPA 8270
EPA 8260
EPA 8260
EPA 6010
EPA 7470
EPA 8270
EPA 8260
EPA 6010
EPA 7470
EPA 8270
EPA 8260
EPA 6010
EPA 7470
EPA 8270
EPA 8260
EPA 6010
EPA 7470
EPA 8270
EPA 8260
EPA 6010
EPA 7470
EPA 8270
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analysts
JMW
SHB
MCK
JMW
SHB
MCK
JMW
SHB
MCK
JMW
SHB
MCK
AW
JMW
SHB
PPM
MCK
MCK
JMW
SHB
PPM
MCK
JMW
SHB
PPM
MCK
JMW
SHB
BPJ
MCK
JMW
SHB
BPJ
MCK
JMW
SHB
BPJ
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Reported
Laboratory
22
PASI-A
1
PASI-A
63
PASI-C
22
PASI-A
1
PASI-A
63
PASI-C
22
PASI-A
1
PASI-A
63
PASI-C
22
PASI-A
1
PASI-A
63
PASI-C
5
PASI-C
22
PASI-A
1
PASI-A
74
PASI-C
63
PASI-C
63
PASI-C
22
PASI-A
1
PASI-A
74
PASI-C
63
PASI-C
22
PASI-A
1
PASI-A
74
PASI-C
63
PASI-C
22
PASI-A
1
PASI-A
74
PASI-C
63
PASI-C
22
PASI-A
1
PASI-A
74
PASI-C
63
PASI-C
22
PASI-A
1
PASI-A
74
PASI-C
Page 3 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Lab ID Sample ID
9293679012
MW-22
9293679013
MW-24
9293679014
MW-25
9293679015
DUP-2
9293679016 Field Blank
9293679017 MW-16
9293679018 MW-17
9293679019 S-10
9293679020 S-8
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Method
EPA 8260
EPA 6010
EPA 7470
EPA 8270
EPA 8260
EPA 6010
EPA 7470
EPA 8270
EPA 8260
EPA 6010
EPA 7470
EPA 8270
EPA 8260
EPA 6010
EPA 7470
EPA 8270
EPA 8260
EPA 8260
EPA 6010
EPA 7471
EPA 8270
EPA 8260
ASTM D2974-87
EPA 6010
EPA 7471
EPA 8270
EPA 8260
ASTM D2974-87
EPA 6010
EPA 7471
EPA 8270
EPA 8260
ASTM D2974-87
EPA 6010
EPA 7471
EPA 8270
EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Analysts
MCK
JMW
SHB
BPJ
MCK
JMW
SHB
BPJ
MCK
JMW
SHB
BPJ
MCK
JMW
SHB
BPJ
MCK
MCK
JMW
SHB
PPM
DLK
TNM
JMW
SHB
PPM
DLK
TNM
JMW
SHB
PPM
DLK
TNM
JMW
SHB
PPM
DLK
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Reported
Laboratory
63
PASI-C
22
PASI-A
1
PASI-A
74
PASI-C
63
PASI-C
22
PASI-A
1
PASI-A
74
PASI-C
63
PASI-C
22
PASI-A
1
PASI-A
74
PASI-C
63
PASI-C
22
PASI-A
1
PASI-A
74
PASI-C
63
PASI-C
63
PASI-C
22
PASI-A
1
PASI-A
74
PASI-C
71
PASI-C
1
PASI-C
22
PASI-A
1
PASI-A
74
PASI-C
71
PASI-C
1
PASI-C
22
PASI-A
1
PASI-A
74
PASI-C
71
PASI-C
1
PASI-C
22
PASI-A
1
PASI-A
74
PASI-C
71
PASI-C
Page 4 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Lab ID Sample ID
9293679021 S-7
9293679023 MW-23
9293679024 MW-24
9293679025 MW-25
9293679026 S-17
9293679027 S-16
9293679028 S-15
9293679029 S-11
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Method
ASTM D2974-87
EPA 6010
EPA 7471
EPA 8270
EPA 8260
ASTM D2974-87
9071 B
EPA 8270
ASTM D2974-87
EPA 6010
EPA 7471
EPA 8270
EPA 8260
ASTM D2974-87
EPA 6010
EPA 7471
EPA 8270
EPA 8260
ASTM D2974-87
EPA 6010
EPA 7471
EPA 8270
EPA 8260
ASTM D2974-87
EPA 6010
EPA 7471
EPA 8270
EPA 8260
ASTM D2974-87
EPA 6010
EPA 7471
EPA 8270
EPA 8260
ASTM D2974-87
EPA 6010
EPA 7471
EPA 8270
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Analysts
TNM
JDA, JMW
SHB
PPM
DLK
TNM
CLW
PPM
TNM
JDA, JMW
SHB
BPJ
DLK
TNM
JDA, JMW
SHB
BPJ
DLK
TNM
JDA, JMW
SHB
BPJ
DLK
TNM
JDA, JMW
SHB
BPJ
DLK
TNM
JDA, JMW
SHB
BPJ
DLK
TNM
JDA, JMW
SHB
BPJ
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Reported
Laboratory
1
PASI-C
22
PASI-A
1
PASI-A
74
PASI-C
71
PASI-C
1
PASI-C
1
PASI-C
74
PASI-C
1
PASI-C
22
PASI-A
1
PASI-A
74
PASI-C
71
PASI-C
1
PASI-C
22
PASI-A
1
PASI-A
74
PASI-C
71
PASI-C
1
PASI-C
22
PASI-A
1
PASI-A
74
PASI-C
71
PASI-C
1
PASI-C
22
PASI-A
1
PASI-A
74
PASI-C
71
PASI-C
1
PASI-C
22
PASI-A
1
PASI-A
74
PASI-C
71
PASI-C
1
PASI-C
22
PASI-A
1
PASI-A
74
PASI-C
Page 5 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Lab ID Sample ID
9293679030 S-2
9293679031
S-3 0-2'
9293679032
S-3 8-10'
9293679033
S-4
9293679034
S-5
9293679035
S-6
9293679036 S-9
9293679037 Myers MW-15
9293679038 Myers MW-15
9293679039 MW-13
9293679040 S-12
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Method
EPA 8260
ASTM D2974-87
EPA 6010
EPA 7471
EPA 8270
EPA 8260
ASTM D2974-87
EPA 8082
ASTM D2974-87
EPA 8082
ASTM D2974-87
EPA 8270
EPA 8260
ASTM D2974-87
EPA 8260
ASTM D2974-87
9071 B
EPA 8270
EPA 8260
ASTM D2974-87
EPA 6010
EPA 7471
EPA 8270
EPA 8260
ASTM D2974-87
MADEP VPH
EPA 6010
EPA 8260
ASTM D2974-87
MADEP VPH
EPA 8260
MADEP EPH
MADEP VPH
EPA 8270
EPA 8260
ASTM D2974-87
9071 B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Analysts Reported Laboratory
DLK
71
PASI-C
TNM
1
PASI-C
JDA, JMW
22
PASI-A
SHB
1
PASI-A
BPJ
74
PASI-C
DLK
71
PASI-C
TNM
1
PASI-C
RES
8
PASI-C
TNM
1
PASI-C
RES
8
PASI-C
TNM
1
PASI-C
BPJ
74
PASI-C
DLK
71
PASI-C
TNM
1
PASI-C
DLK
71
PASI-C
TNM
1
PASI-C
CLW
1
PASI-C
BPJ
74
PASI-C
DLK
71
PASI-C
TNM
1
PASI-C
JDA, JMW
22
PASI-A
SHB
1
PASI-A
BPJ
74
PASI-C
DLK
71
PASI-C
TNM
1
PASI-C
AW
5
PASI-C
JDA
1
PASI-A
DLK
71
PASI-C
TNM
1
PASI-C
AW
5
PASI-C
MCK
63
PASI-C
RES
7
PASI-C
AW
5
PASI-C
BPJ
74
PASI-C
DLK
71
PASI-C
TNM
1
PASI-C
CLW
1
PASI-C
Page 6 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Lab ID Sample ID
9293679041 S-13
9293679042 S-14
9293679043 SS-4
9293679044 SS-5
9293679045 SS-6
9293679046 SS-7
9293679047 SW-4
9293679048 SW-5
9293679049 SW-6
9293679050 SW-7
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Method
EPA 8270
ASTM D2974-87
9071 B
EPA 8270
ASTM D2974-87
9071 B
EPA 8270
ASTM D2974-87
EPA 6010
EPA 8270
ASTM D2974-87
EPA 6010
EPA 8270
ASTM D2974-87
EPA 6010
EPA 8270
ASTM D2974-87
EPA 6010
EPA 8270
ASTM D2974-87
EPA 6010
EPA 8270
EPA 8260
EPA 6010
EPA 8270
EPA 8260
EPA 6010
EPA 8270
EPA 8260
EPA 6010
EPA 8270
EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Analysts Reported Laboratory
BPJ
74
PASI-C
TNM
1
PASI-C
CLW
1
PASI-C
BPJ
74
PASI-C
TNM
1
PASI-C
CLW
1
PASI-C
BPJ
74
PASI-C
TNM
1
PASI-C
JMW
6
PASI-A
BPJ
74
PASI-C
TNM
1
PASI-C
JMW
6
PASI-A
BPJ
74
PASI-C
TNM
1
PASI-C
JMW
6
PASI-A
BPJ
74
PASI-C
TNM
1
PASI-C
JMW
6
PASI-A
BPJ
74
PASI-C
TNM
1
PASI-C
JMW
6
PASI-A
BPJ
74
PASI-C
MCK
63
PASI-C
JMW
6
PASI-A
BPJ
74
PASI-C
MCK
63
PASI-C
JMW
6
PASI-A
BPJ
74
PASI-C
MCK
63
PASI-C
JMW
6
PASI-A
BPJ
74
PASI-C
MCK
63
PASI-C
Page 7 of 227

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-10 Lab ID: 9293679001 Collected: 05/05/11 18:40 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Aluminum
ND ug/L
100
1
05/12/11 12:30
05/16/11 19:02
7429-90-5
Antimony
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:02
7440-36-0
Arsenic
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:02
7440-38-2
Barium
68.6 ug/L
5.0
1
05/12/11 12:30
05/16/11 19:02
7440-39-3
Beryllium
ND ug/L
1.0
1
05/12/11 12:30
05/16/11 19:02
7440-41-7
Cadmium
ND ug/L
1.0
1
05/12/11 12:30
05/16/11 19:02
7440-43-9
Calcium
46000 ug/L
100
1
05/12/11 12:30
05/16/11 19:02
7440-70-2
Chromium
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:02
7440-47-3
Cobalt
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:02
7440-48-4
Copper
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:02
7440-50-8
Iron
72.0 ug/L
50.0
1
05/12/11 12:30
05/16/11 19:02
7439-89-6
Lead
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:02
7439-92-1
Magnesium
12100 ug/L
100
1
05/12/11 12:30
05/16/11 19:02
7439-95-4
Manganese
320 ug/L
5.0
1
05/12/11 12:30
05/16/11 19:02
7439-96-5
Nickel
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:02
7440-02-0
Potassium
ND ug/L
5000
1
05/12/11 12:30
05/17/11 10:51
7440-09-7
Selenium
ND ug/L
10.0
1
05/12/11 12:30
05/16/11 19:02
7782-49-2
Silver
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:02
7440-22-4
Sodium
11100 ug/L
5000
1
05/12/11 12:30
05/16/11 19:02
7440-23-5
Thallium
ND ug/L
10.0
1
05/12/11 12:30
05/16/11 19:02
7440-28-0
Vanadium
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:02
7440-62-2
Zinc
15.3 ug/L
10.0
1
05/12/11 12:30
05/16/11 19:02
7440-66-6
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
05/17/11 09:40
05/17/11 15:33
7439-97-6
8260 MSV Low Level
Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/11/11 02:09
67-64-1
Benzene
ND ug/L
1.0
1
05/11/11 02:09
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/11/11 02:09
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/11/11 02:09
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
05/11/11 02:09
75-27-4
Bromoform
ND ug/L
1.0
1
05/11/11 02:09
75-25-2
Bromomethane
ND ug/L
2.0
1
05/11/11 02:09
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/11/11 02:09
78-93-3
Carbon tetrachloride
ND ug/L
1.0
1
05/11/11 02:09
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/11/11 02:09
108-90-7
Chloroethane
ND ug/L
1.0
1
05/11/11 02:09
75-00-3
Chloroform
ND ug/L
1.0
1
05/11/11 02:09
67-66-3
Chloromethane
ND ug/L
1.0
1
05/11/11 02:09
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/11/11 02:09
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/11/11 02:09
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
1
05/11/11 02:09
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/11/11 02:09
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/11/11 02:09
106-93-4
Dibromomethane
ND ug/L
1.0
1
05/11/11 02:09
74-95-3
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 8 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-10 Lab ID: 9293679001 Collected: 05/05/11 18:40 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 02:09
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 02:09
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 02:09
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/11/11 02:09
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
1
05/11/11 02:09
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/11/11 02:09
107-06-2
1,1-Dichloroethene
1.2 ug/L
1.0
1
05/11/11 02:09
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 02:09
156-59-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 02:09
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 02:09
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/11/11 02:09
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 02:09
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/11/11 02:09
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 02:09
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 02:09
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/11/11 02:09
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/11/11 02:09
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/11/11 02:09
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/11/11 02:09
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
1
05/11/11 02:09
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/11/11 02:09
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/11/11 02:09
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/11/11 02:09
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/11/11 02:09
91-20-3
Styrene
ND ug/L
1.0
1
05/11/11 02:09
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 02:09
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 02:09
79-34-5
Tetrachloroethene
5.3 ug/L
1.0
1
05/11/11 02:09
127-18-4
Toluene
ND ug/L
1.0
1
05/11/11 02:09
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 02:09
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 02:09
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/11/11 02:09
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/11/11 02:09
79-00-5
Trichloroethene
ND ug/L
1.0
1
05/11/11 02:09
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/11/11 02:09
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/11/11 02:09
96-18-4
Vinyl acetate
ND ug/L
2.0
1
05/11/11 02:09
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/11/11 02:09
75-01-4
m&p-Xylene
ND ug/L
2.0
1
05/11/11 02:09
179601-23-1
o-Xylene
ND ug/L
1.0
1
05/11/11 02:09
95-47-6
4-Bromofluorobenzene (S)
96 %
70-130
1
05/11/11 02:09
460-00-4
Dibromofluoromethane (S)
102 %
70-130
1
05/11/11 02:09
1868-53-7
1,2-Dichloroethane-d4 (S)
106 %
70-130
1
05/11/11 02:09
17060-07-0
Toluene-d8 (S)
100 %
70-130
1
05/11/11 02:09
2037-26-5
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 9 of 227

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-9 Lab ID: 9293679002 Collected: 05/05/11 19:10 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Aluminum
ND ug/L
100
1
05/12/11 12:30
05/16/11 19:06
7429-90-5
Antimony
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:06
7440-36-0
Arsenic
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:06
7440-38-2
Barium
68.7 ug/L
5.0
1
05/12/11 12:30
05/16/11 19:06
7440-39-3
Beryllium
ND ug/L
1.0
1
05/12/11 12:30
05/16/11 19:06
7440-41-7
Cadmium
ND ug/L
1.0
1
05/12/11 12:30
05/16/11 19:06
7440-43-9
Calcium
63800 ug/L
100
1
05/12/11 12:30
05/16/11 19:06
7440-70-2
Chromium
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:06
7440-47-3
Cobalt
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:06
7440-48-4
Copper
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:06
7440-50-8
Iron
72.7 ug/L
50.0
1
05/12/11 12:30
05/16/11 19:06
7439-89-6
Lead
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:06
7439-92-1
Magnesium
20200 ug/L
100
1
05/12/11 12:30
05/16/11 19:06
7439-95-4
Manganese
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:06
7439-96-5
Nickel
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:06
7440-02-0
Potassium
7000 ug/L
5000
1
05/12/11 12:30
05/17/11 10:54
7440-09-7
Selenium
ND ug/L
10.0
1
05/12/11 12:30
05/16/11 19:06
7782-49-2
Silver
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:06
7440-22-4
Sodium
7470 ug/L
5000
1
05/12/11 12:30
05/16/11 19:06
7440-23-5
Thallium
ND ug/L
10.0
1
05/12/11 12:30
05/16/11 19:06
7440-28-0
Vanadium
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:06
7440-62-2
Zinc
ND ug/L
10.0
1
05/12/11 12:30
05/16/11 19:06
7440-66-6
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
05/17/11 09:40
05/17/11 15:41
7439-97-6
8260 MSV Low Level
Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/11/11 02:33
67-64-1
Benzene
ND ug/L
1.0
1
05/11/11 02:33
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/11/11 02:33
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/11/11 02:33
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
05/11/11 02:33
75-27-4
Bromoform
ND ug/L
1.0
1
05/11/11 02:33
75-25-2
Bromomethane
ND ug/L
2.0
1
05/11/11 02:33
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/11/11 02:33
78-93-3
Carbon tetrachloride
ND ug/L
1.0
1
05/11/11 02:33
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/11/11 02:33
108-90-7
Chloroethane
ND ug/L
1.0
1
05/11/11 02:33
75-00-3
Chloroform
ND ug/L
1.0
1
05/11/11 02:33
67-66-3
Chloromethane
ND ug/L
1.0
1
05/11/11 02:33
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/11/11 02:33
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/11/11 02:33
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
1
05/11/11 02:33
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/11/11 02:33
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/11/11 02:33
106-93-4
Dibromomethane
ND ug/L
1.0
1
05/11/11 02:33
74-95-3
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 10 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-9 Lab ID: 9293679002 Collected: 05/05/11 19:10 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 02:33
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 02:33
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 02:33
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/11/11 02:33
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
1
05/11/11 02:33
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/11/11 02:33
107-06-2
1,1-Dichloroethene
4.8 ug/L
1.0
1
05/11/11 02:33
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 02:33
156-59-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 02:33
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 02:33
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/11/11 02:33
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 02:33
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/11/11 02:33
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 02:33
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 02:33
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/11/11 02:33
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/11/11 02:33
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/11/11 02:33
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/11/11 02:33
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
1
05/11/11 02:33
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/11/11 02:33
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/11/11 02:33
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/11/11 02:33
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/11/11 02:33
91-20-3
Styrene
ND ug/L
1.0
1
05/11/11 02:33
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 02:33
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 02:33
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
05/11/11 02:33
127-18-4
Toluene
ND ug/L
1.0
1
05/11/11 02:33
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 02:33
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 02:33
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/11/11 02:33
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/11/11 02:33
79-00-5
Trichloroethene
1.4 ug/L
1.0
1
05/11/11 02:33
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/11/11 02:33
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/11/11 02:33
96-18-4
Vinyl acetate
ND ug/L
2.0
1
05/11/11 02:33
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/11/11 02:33
75-01-4
m&p-Xylene
ND ug/L
2.0
1
05/11/11 02:33
179601-23-1
o-Xylene
ND ug/L
1.0
1
05/11/11 02:33
95-47-6
4-Bromofluorobenzene (S)
96 %
70-130
1
05/11/11 02:33
460-00-4
Dibromofluoromethane (S)
103 %
70-130
1
05/11/11 02:33
1868-53-7
1,2-Dichloroethane-d4 (S)
107 %
70-130
1
05/11/11 02:33
17060-07-0
Toluene-d8 (S)
102 %
70-130
1
05/11/11 02:33
2037-26-5
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 11 of 227

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-8 Lab ID: 9293679003 Collected: 05/05/11 19:45 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Aluminum
ND ug/L
100
1
05/12/11 12:30
05/16/11 19:10
7429-90-5
Antimony
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:10
7440-36-0
Arsenic
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:10
7440-38-2
Barium
40.5 ug/L
5.0
1
05/12/11 12:30
05/16/11 19:10
7440-39-3
Beryllium
ND ug/L
1.0
1
05/12/11 12:30
05/16/11 19:10
7440-41-7
Cadmium
ND ug/L
1.0
1
05/12/11 12:30
05/16/11 19:10
7440-43-9
Calcium
9520 ug/L
100
1
05/12/11 12:30
05/16/11 19:10
7440-70-2
Chromium
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:10
7440-47-3
Cobalt
7.4 ug/L
5.0
1
05/12/11 12:30
05/16/11 19:10
7440-48-4
Copper
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:10
7440-50-8
Iron
18500 ug/L
50.0
1
05/12/11 12:30
05/16/11 19:10
7439-89-6
Lead
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:10
7439-92-1
Magnesium
4500 ug/L
100
1
05/12/11 12:30
05/16/11 19:10
7439-95-4
Manganese
1690 ug/L
5.0
1
05/12/11 12:30
05/16/11 19:10
7439-96-5
Nickel
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:10
7440-02-0
Potassium
ND ug/L
5000
1
05/12/11 12:30
05/17/11 10:58
7440-09-7
Selenium
ND ug/L
10.0
1
05/12/11 12:30
05/16/11 19:10
7782-49-2
Silver
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:10
7440-22-4
Sodium
6820 ug/L
5000
1
05/12/11 12:30
05/16/11 19:10
7440-23-5
Thallium
ND ug/L
10.0
1
05/12/11 12:30
05/16/11 19:10
7440-28-0
Vanadium
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:10
7440-62-2
Zinc
ND ug/L
10.0
1
05/12/11 12:30
05/16/11 19:10
7440-66-6
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
05/17/11 09:40
05/17/11 15:45
7439-97-6
8260 MSV Low Level
Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/11/11 02:58
67-64-1
Benzene
ND ug/L
1.0
1
05/11/11 02:58
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/11/11 02:58
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/11/11 02:58
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
05/11/11 02:58
75-27-4
Bromoform
ND ug/L
1.0
1
05/11/11 02:58
75-25-2
Bromomethane
ND ug/L
2.0
1
05/11/11 02:58
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/11/11 02:58
78-93-3
Carbon tetrachloride
ND ug/L
1.0
1
05/11/11 02:58
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/11/11 02:58
108-90-7
Chloroethane
ND ug/L
1.0
1
05/11/11 02:58
75-00-3
Chloroform
ND ug/L
1.0
1
05/11/11 02:58
67-66-3
Chloromethane
ND ug/L
1.0
1
05/11/11 02:58
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/11/11 02:58
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/11/11 02:58
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
1
05/11/11 02:58
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/11/11 02:58
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/11/11 02:58
106-93-4
Dibromomethane
ND ug/L
1.0
1
05/11/11 02:58
74-95-3
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 12 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-8 Lab ID: 9293679003 Collected: 05/05/11 19:45 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 02:58
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 02:58
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 02:58
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/11/11 02:58
75-71-8
1,1-Dichloroethane
1.5 ug/L
1.0
1
05/11/11 02:58
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/11/11 02:58
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
05/11/11 02:58
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 02:58
156-59-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 02:58
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 02:58
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/11/11 02:58
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 02:58
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/11/11 02:58
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 02:58
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 02:58
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/11/11 02:58
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/11/11 02:58
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/11/11 02:58
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/11/11 02:58
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
1
05/11/11 02:58
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/11/11 02:58
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/11/11 02:58
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/11/11 02:58
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/11/11 02:58
91-20-3
Styrene
ND ug/L
1.0
1
05/11/11 02:58
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 02:58
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 02:58
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
05/11/11 02:58
127-18-4
Toluene
ND ug/L
1.0
1
05/11/11 02:58
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 02:58
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 02:58
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/11/11 02:58
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/11/11 02:58
79-00-5
Trichloroethene
ND ug/L
1.0
1
05/11/11 02:58
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/11/11 02:58
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/11/11 02:58
96-18-4
Vinyl acetate
ND ug/L
2.0
1
05/11/11 02:58
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/11/11 02:58
75-01-4
m&p-Xylene
ND ug/L
2.0
1
05/11/11 02:58
179601-23-1
o-Xylene
ND ug/L
1.0
1
05/11/11 02:58
95-47-6
4-Bromofluorobenzene (S)
95 %
70-130
1
05/11/11 02:58
460-00-4
Dibromofluoromethane (S)
102 %
70-130
1
05/11/11 02:58
1868-53-7
1,2-Dichloroethane-d4 (S)
107 %
70-130
1
05/11/11 02:58
17060-07-0
Toluene-d8 (S)
101 %
70-130
1
05/11/11 02:58
2037-26-5
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 13 of 227

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: DUP-1 Lab ID: 9293679004 Collected: 05/05/11 19:46 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Aluminum
ND ug/L
100
1
05/12/11 12:30
05/16/11 19:14
7429-90-5
Antimony
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:14
7440-36-0
Arsenic
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:14
7440-38-2
Barium
40.9 ug/L
5.0
1
05/12/11 12:30
05/16/11 19:14
7440-39-3
Beryllium
ND ug/L
1.0
1
05/12/11 12:30
05/16/11 19:14
7440-41-7
Cadmium
ND ug/L
1.0
1
05/12/11 12:30
05/16/11 19:14
7440-43-9
Calcium
9640 ug/L
100
1
05/12/11 12:30
05/16/11 19:14
7440-70-2
Chromium
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:14
7440-47-3
Cobalt
7.6 ug/L
5.0
1
05/12/11 12:30
05/16/11 19:14
7440-48-4
Copper
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:14
7440-50-8
Iron
18800 ug/L
50.0
1
05/12/11 12:30
05/16/11 19:14
7439-89-6
Lead
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:14
7439-92-1
Magnesium
4540 ug/L
100
1
05/12/11 12:30
05/16/11 19:14
7439-95-4
Manganese
1710 ug/L
5.0
1
05/12/11 12:30
05/16/11 19:14
7439-96-5
Nickel
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:14
7440-02-0
Potassium
ND ug/L
5000
1
05/12/11 12:30
05/17/11 11:01
7440-09-7
Selenium
ND ug/L
10.0
1
05/12/11 12:30
05/16/11 19:14
7782-49-2
Silver
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:14
7440-22-4
Sodium
6910 ug/L
5000
1
05/12/11 12:30
05/16/11 19:14
7440-23-5
Thallium
ND ug/L
10.0
1
05/12/11 12:30
05/16/11 19:14
7440-28-0
Vanadium
ND ug/L
5.0
1
05/12/11 12:30
05/16/11 19:14
7440-62-2
Zinc
10.2 ug/L
10.0
1
05/12/11 12:30
05/16/11 19:14
7440-66-6
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
05/17/11 09:40
05/17/11 15:48
7439-97-6
8260 MSV Low Level
Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/11/11 03:22
67-64-1
Benzene
ND ug/L
1.0
1
05/11/11 03:22
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/11/11 03:22
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/11/11 03:22
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
05/11/11 03:22
75-27-4
Bromoform
ND ug/L
1.0
1
05/11/11 03:22
75-25-2
Bromomethane
ND ug/L
2.0
1
05/11/11 03:22
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/11/11 03:22
78-93-3
Carbon tetrachloride
ND ug/L
1.0
1
05/11/11 03:22
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/11/11 03:22
108-90-7
Chloroethane
ND ug/L
1.0
1
05/11/11 03:22
75-00-3
Chloroform
ND ug/L
1.0
1
05/11/11 03:22
67-66-3
Chloromethane
ND ug/L
1.0
1
05/11/11 03:22
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/11/11 03:22
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/11/11 03:22
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
1
05/11/11 03:22
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/11/11 03:22
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/11/11 03:22
106-93-4
Dibromomethane
ND ug/L
1.0
1
05/11/11 03:22
74-95-3
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 14 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: DUP-1 Lab ID: 9293679004 Collected: 05/05/11 19:46 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 03:22
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 03:22
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 03:22
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/11/11 03:22
75-71-8
1,1-Dichloroethane
1.5 ug/L
1.0
1
05/11/11 03:22
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/11/11 03:22
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
05/11/11 03:22
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 03:22
156-59-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 03:22
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 03:22
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/11/11 03:22
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 03:22
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/11/11 03:22
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 03:22
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 03:22
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/11/11 03:22
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/11/11 03:22
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/11/11 03:22
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/11/11 03:22
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
1
05/11/11 03:22
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/11/11 03:22
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/11/11 03:22
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/11/11 03:22
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/11/11 03:22
91-20-3
Styrene
ND ug/L
1.0
1
05/11/11 03:22
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 03:22
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 03:22
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
05/11/11 03:22
127-18-4
Toluene
ND ug/L
1.0
1
05/11/11 03:22
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 03:22
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 03:22
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/11/11 03:22
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/11/11 03:22
79-00-5
Trichloroethene
ND ug/L
1.0
1
05/11/11 03:22
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/11/11 03:22
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/11/11 03:22
96-18-4
Vinyl acetate
ND ug/L
2.0
1
05/11/11 03:22
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/11/11 03:22
75-01-4
m&p-Xylene
ND ug/L
2.0
1
05/11/11 03:22
179601-23-1
o-Xylene
ND ug/L
1.0
1
05/11/11 03:22
95-47-6
4-Bromofluorobenzene (S)
93 %
70-130
1
05/11/11 03:22
460-00-4
Dibromofluoromethane (S)
103 %
70-130
1
05/11/11 03:22
1868-53-7
1,2-Dichloroethane-d4 (S)
111 %
70-130
1
05/11/11 03:22
17060-07-0
Toluene-d8 (S)
102 %
70-130
1
05/11/11 03:22
2037-26-5
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 15 of 227

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-13 Lab ID: 9293679005 Collected: 05/06/11 16:00 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-CO8)
ND ug/L
30.0
1
05/17/11 01:38 N2
Aliphatic (C09-C12)
ND ug/L
30.0
1
05/17/11 01:38 N2
Aromatic (C09-C10)
ND ug/L
30.0
1
05/17/11 01:38 N2
2,5-Dibromotoluene (PID)(S)
105 %
70-130
1
05/17/11 01:38
2,5-Dibromotoluene (FID)(S)
106 %
70-130
1
05/17/11 01:38
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Aluminum
ND ug/L
100
1
05/12/11 12:30
05/12/11 21:57
7429-90-5
Antimony
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 21:57
7440-36-0
Arsenic
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 21:57
7440-38-2
Barium
69.1 ug/L
5.0
1
05/12/11 12:30
05/12/11 21:57
7440-39-3
Beryllium
ND ug/L
1.0
1
05/12/11 12:30
05/12/11 21:57
7440-41-7
Cadmium
ND ug/L
1.0
1
05/12/11 12:30
05/12/11 21:57
7440-43-9
Calcium
10400 ug/L
100
1
05/12/11 12:30
05/12/11 21:57
7440-70-2
Chromium
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 21:57
7440-47-3
Cobalt
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 21:57
7440-48-4
Copper
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 21:57
7440-50-8
Iron
121 ug/L
50.0
1
05/12/11 12:30
05/12/11 21:57
7439-89-6
Lead
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 21:57
7439-92-1
Magnesium
6530 ug/L
100
1
05/12/11 12:30
05/12/11 21:57
7439-95-4
Manganese
101 ug/L
5.0
1
05/12/11 12:30
05/12/11 21:57
7439-96-5
Nickel
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 21:57
7440-02-0
Potassium
ND ug/L
5000
1
05/12/11 12:30
05/13/11 12:58
7440-09-7
Selenium
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 21:57
7782-49-2
Silver
9.3 ug/L
5.0
1
05/12/11 12:30
05/12/11 21:57
7440-22-4
Sodium
73300 ug/L
5000
1
05/12/11 12:30
05/13/11 12:58
7440-23-5
Thallium
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 21:57
7440-28-0
Vanadium
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 21:57
7440-62-2
Zinc
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 21:57
7440-66-6
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 0.20 1 05/17/11 09:40 05/17/11 15:51 7439-97-6
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
83-32-9
Acenaphthylene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
208-96-8
Aniline
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
62-53-3
Anthracene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
120-12-7
Benzo(a)anthracene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
56-55-3
Benzo(a)pyrene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
50-32-8
Benzo(b)fluoranthene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
205-99-2
Benzo(g,h,i)perylene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
191-24-2
Benzo(k)fluoranthene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
207-08-9
Benzoic Acid
ND ug/L
55.6
1
05/12/11 14:00
05/16/11 18:33
65-85-0
Benzyl alcohol
ND ug/L
22.2
1
05/12/11 14:00
05/16/11 18:33
100-51-6
4-Bromophenylphenyl ether
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
101-55-3
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 16 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-13 Lab ID: 9293679005 Collected: 05/06/11 16:00 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Butyl benzylphthalate
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
85-68-7
4-Chloro-3-methylphenol
ND ug/L
22.2
1
05/12/11 14:00
05/16/11 18:33
59-50-7
4-Chloroaniline
ND ug/L
22.2
1
05/12/11 14:00
05/16/11 18:33
106-47-8
bis(2-Chloroethoxy)methane
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
111-91-1
bis(2-Chloroethyl) ether
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
108-60-1
2-Chloronaphthalene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
91-58-7
2-Chlorophenol
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
7005-72-3
Chrysene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
218-01-9
Dibenz(a,h)anthracene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
53-70-3
Dibenzofuran
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
132-64-9
1,2-Dichlorobenzene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
95-50-1
1,3-Dichlorobenzene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
541-73-1
1,4-Dichlorobenzene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
106-46-7
3,3'-Dichlorobenzidine
ND ug/L
22.2
1
05/12/11 14:00
05/16/11 18:33
91-94-1
2,4-Dichlorophenol
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
120-83-2
Diethylphthalate
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
84-66-2
2,4-Dimethylphenol
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
105-67-9
Dimethylphthalate
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
131-11-3
Di-n-butylphthalate
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
84-74-2
4,6-Dinitro-2-methylphenol
ND ug/L
22.2
1
05/12/11 14:00
05/16/11 18:33
534-52-1
2,4-Dinitrophenol
ND ug/L
55.6
1
05/12/11 14:00
05/16/11 18:33
51-28-5
2,4-Dinitrotoluene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
121-14-2
2,6-Dinitrotoluene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
606-20-2
Di-n-octylphthalate
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/L
6.7
1
05/12/11 14:00
05/16/11 18:33
117-81-7
Fluoranthene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
206-44-0
Fluorene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
87-68-3
Hexachlorobenzene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
118-74-1
Hexachlorocyclopentadiene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
77-47-4
Hexachloroethane
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
193-39-5
Isophorone
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
78-59-1
1-Methylnaphthalene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
90-12-0
2-Methylnaphthalene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
91-57-6
2-Methylphenol(o-Cresol)
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
Naphthalene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
91-20-3
2-Nitroaniline
ND ug/L
55.6
1
05/12/11 14:00
05/16/11 18:33
88-74-4
3-Nitroaniline
ND ug/L
55.6
1
05/12/11 14:00
05/16/11 18:33
99-09-2
4-Nitroaniline
ND ug/L
22.2
1
05/12/11 14:00
05/16/11 18:33
100-01-6
Nitrobenzene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
98-95-3
2-Nitrophenol
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
88-75-5
4-Nitrophenol
ND ug/L
55.6
1
05/12/11 14:00
05/16/11 18:33
100-02-7
N-Nitrosodimethylamine
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
62-75-9
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 17 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-13 Lab ID: 9293679005 Collected: 05/06/11 16:00 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
N-Nitroso-di-n-propylamine
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
621-64-7
N-Nitrosodiphenylamine
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
86-30-6
Pentachlorophenol
ND ug/L
27.8
1
05/12/11 14:00
05/16/11 18:33
87-86-5
Phenanthrene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
85-01-8
Phenol
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
108-95-2
Pyrene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
129-00-0
1,2,4-Trichlorobenzene
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
120-82-1
2,4,5-Trichlorophenol
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
95-95-4
2,4,6-Trichlorophenol
ND ug/L
11.1
1
05/12/11 14:00
05/16/11 18:33
88-06-2
Nitrobenzene-d5 (S)
64 %
21-110
1
05/12/11 14:00
05/16/11 18:33
4165-60-0
2-Fluorobiphenyl (S)
72 %
27-110
1
05/12/11 14:00
05/16/11 18:33
321-60-8
Terphenyl-d14 (S)
80 %
31-107
1
05/12/11 14:00
05/16/11 18:33
1718-51-0
Phenol-d6 (S)
24 %
10-110
1
05/12/11 14:00
05/16/11 18:33
13127-88-3
2-Fluorophenol (S)
42 %
12-110
1
05/12/11 14:00
05/16/11 18:33
367-12-4
2,4,6-Tribromophenol (S)
66 %
27-110
1
05/12/11 14:00
05/16/11 18:33
118-79-6
8260 MSV Low Level
Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/11/11 03:46
67-64-1
Benzene
ND ug/L
1.0
1
05/11/11 03:46
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/11/11 03:46
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/11/11 03:46
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
05/11/11 03:46
75-27-4
Bromoform
ND ug/L
1.0
1
05/11/11 03:46
75-25-2
Bromomethane
ND ug/L
2.0
1
05/11/11 03:46
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/11/11 03:46
78-93-3
Carbon tetrachloride
ND ug/L
1.0
1
05/11/11 03:46
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/11/11 03:46
108-90-7
Chloroethane
ND ug/L
1.0
1
05/11/11 03:46
75-00-3
Chloroform
ND ug/L
1.0
1
05/11/11 03:46
67-66-3
Chloromethane
ND ug/L
1.0
1
05/11/11 03:46
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/11/11 03:46
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/11/11 03:46
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
1
05/11/11 03:46
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/11/11 03:46
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/11/11 03:46
106-93-4
Dibromomethane
ND ug/L
1.0
1
05/11/11 03:46
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 03:46
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 03:46
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 03:46
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/11/11 03:46
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
1
05/11/11 03:46
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/11/11 03:46
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
05/11/11 03:46
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 03:46
156-59-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 03:46
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 03:46
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/11/11 03:46
142-28-9
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY
ANALYSIS
Page 18 of 227
This report shall not be reproduced, except
in
full,
without the written consent of Pace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-13 Lab ID: 9293679005 Collected: 05/06/11 16:00 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
2,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 03:46
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/11/11 03:46
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 03:46
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 03:46
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/11/11 03:46
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/11/11 03:46
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/11/11 03:46
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/11/11 03:46
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
1
05/11/11 03:46
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/11/11 03:46
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/11/11 03:46
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/11/11 03:46
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/11/11 03:46
91-20-3
Styrene
ND ug/L
1.0
1
05/11/11 03:46
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 03:46
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 03:46
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
05/11/11 03:46
127-18-4
Toluene
ND ug/L
1.0
1
05/11/11 03:46
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 03:46
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 03:46
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/11/11 03:46
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/11/11 03:46
79-00-5
Trichloroethene
ND ug/L
1.0
1
05/11/11 03:46
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/11/11 03:46
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/11/11 03:46
96-18-4
Vinyl acetate
ND ug/L
2.0
1
05/11/11 03:46
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/11/11 03:46
75-01-4
m&p-Xylene
ND ug/L
2.0
1
05/11/11 03:46
179601-23-1
o-Xylene
ND ug/L
1.0
1
05/11/11 03:46
95-47-6
4-Bromofluorobenzene (S)
95 %
70-130
1
05/11/11 03:46
460-00-4
Dibromofluoromethane (S)
101 %
70-130
1
05/11/11 03:46
1868-53-7
1,2-Dichloroethane-d4 (S)
107 %
70-130
1
05/11/11 03:46
17060-07-0
Toluene-d8 (S)
101 %
70-130
1
05/11/11 03:46
2037-26-5
Sample: MW-14 Lab ID: 9293679006 Collected: 05/06/11 16:40 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Date: 05/20/2011 04:57 PM
Analytical Method: EPA 8260
ND ug/L
25.0 1
ND ug/L
1.0 1
ND ug/L
1.0 1
ND ug/L
1.0 1
ND ug/L
1.0 1
ND ug/L
1.0 1
ND ug/L
2.0 1
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written
consent of Analytical Services, Inc..
PPace
05/11/1104:10
67-64-1
05/11/1104:10
71-43-2
05/11/11 04:10
108-86-1
05/11/1104:10
74-97-5
05/11/1104:10
75-27-4
05/11/1104:10
75-25-2
05/11/1104:10
74-83-9
Page 19 of 227

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-14 Lab ID: 9293679006 Collected: 05/06/11 16:40 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
2-Butanone (MEK)
ND ug/L
5.0
1
05/11/11 04:10
78-93-3
Carbon tetrachloride
ND ug/L
1.0
1
05/11/11 04:10
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/11/11 04:10
108-90-7
Chloroethane
ND ug/L
1.0
1
05/11/11 04:10
75-00-3
Chloroform
ND ug/L
1.0
1
05/11/11 04:10
67-66-3
Chloromethane
ND ug/L
1.0
1
05/11/11 04:10
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/11/11 04:10
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/11/11 04:10
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
1
05/11/11 04:10
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/11/11 04:10
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/11/11 04:10
106-93-4
Dibromomethane
ND ug/L
1.0
1
05/11/11 04:10
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 04:10
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 04:10
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 04:10
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/11/11 04:10
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
1
05/11/11 04:10
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/11/11 04:10
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
05/11/11 04:10
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 04:10
156-59-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 04:10
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 04:10
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/11/11 04:10
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 04:10
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/11/11 04:10
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 04:10
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 04:10
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/11/11 04:10
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/11/11 04:10
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/11/11 04:10
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/11/11 04:10
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
1
05/11/11 04:10
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/11/11 04:10
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/11/11 04:10
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/11/11 04:10
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/11/11 04:10
91-20-3
Styrene
ND ug/L
1.0
1
05/11/11 04:10
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 04:10
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 04:10
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
05/11/11 04:10
127-18-4
Toluene
ND ug/L
1.0
1
05/11/11 04:10
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 04:10
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 04:10
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/11/11 04:10
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/11/11 04:10
79-00-5
Trichloroethene
ND ug/L
1.0
1
05/11/11 04:10
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/11/11 04:10
75-69-4
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 20 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-14
Lab ID: 9293679006
Collected: 05/06/11
16:40
Received:
05/07/11 10:40 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8260 MSV Low Level
Analytical Method: EPA 8260
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/11/11 04:10
96-18-4
Vinyl acetate
ND ug/L
2.0
1
05/11/11 04:10
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/11/11 04:10
75-01-4
m&p-Xylene
ND ug/L
2.0
1
05/11/11 04:10
179601-23-1
o-Xylene
ND ug/L
1.0
1
05/11/11 04:10
95-47-6
4-Bromofluorobenzene (S)
96 %
70-130
1
05/11/11 04:10
460-00-4
Dibromofluoromethane (S)
101 %
70-130
1
05/11/11 04:10
1868-53-7
1,2-Dichloroethane-d4 (S)
108 %
70-130
1
05/11/11 04:10
17060-07-0
Toluene-d8 (S)
101 %
70-130
1
05/11/11 04:10
2037-26-5
Sample: MW-16
Lab ID: 9293679007
Collected: 05/06/11 14:15
Received:
05/07/11 10:40 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Aluminum
220 ug/L
100
1
05/12/11 12:30
05/12/11 22:03
7429-90-5
Antimony
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:03
7440-36-0
Arsenic
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:03
7440-38-2
Barium
63.8 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:03
7440-39-3
Beryllium
ND ug/L
1.0
1
05/12/11 12:30
05/12/11 22:03
7440-41-7
Cadmium
ND ug/L
1.0
1
05/12/11 12:30
05/12/11 22:03
7440-43-9
Calcium
19400 ug/L
100
1
05/12/11 12:30
05/12/11 22:03
7440-70-2
Chromium
5.0 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:03
7440-47-3
Cobalt
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:03
7440-48-4
Copper
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:03
7440-50-8
Iron
401 ug/L
50.0
1
05/12/11 12:30
05/12/11 22:03
7439-89-6
Lead
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:03
7439-92-1
Magnesium
8670 ug/L
100
1
05/12/11 12:30
05/12/11 22:03
7439-95-4
Manganese
166 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:03
7439-96-5
Nickel
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:03
7440-02-0
Potassium
ND ug/L
5000
1
05/12/11 12:30
05/13/11 13:01
7440-09-7
Selenium
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:03
7782-49-2
Silver
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:03
7440-22-4
Sodium
17200 ug/L
5000
1
05/12/11 12:30
05/13/11 13:01
7440-23-5
Thallium
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:03
7440-28-0
Vanadium
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:03
7440-62-2
Zinc
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:03
7440-66-6
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
05/17/11 09:40
05/17/11 15:53
7439-97-6
8270 MSSV Semivolatile Organic
Analytical Method: EPA 8270 Preparation Method:
EPA 3510
Acenaphthene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
83-32-9
Acenaphthylene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
208-96-8
Aniline
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
62-53-3
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 21 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-16 Lab ID: 9293679007 Collected: 05/06/11 14:15 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Anthracene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
120-12-7
Benzo(a)anthracene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
56-55-3
Benzo(a)pyrene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
50-32-8
Benzo(b)fluoranthene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
205-99-2
Benzo(g,h,i)perylene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
191-24-2
Benzo(k)fluoranthene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
207-08-9
Benzoic Acid
ND ug/L
58.1
1
05/12/11 14:00
05/16/11 19:00
65-85-0
Benzyl alcohol
ND ug/L
23.3
1
05/12/11 14:00
05/16/11 19:00
100-51-6
4-Bromophenylphenyl ether
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
101-55-3
Butylbenzylphthalate
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
85-68-7
4-Chloro-3-methylphenol
ND ug/L
23.3
1
05/12/11 14:00
05/16/11 19:00
59-50-7
4-Chloroaniline
ND ug/L
23.3
1
05/12/11 14:00
05/16/11 19:00
106-47-8
bis(2-Chloroethoxy)methane
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
111-91-1
bis(2-Chloroethyl) ether
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
108-60-1
2-Chloronaphthalene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
91-58-7
2-Chlorophenol
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
7005-72-3
Chrysene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
218-01-9
Dibenz(a,h)anthracene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
53-70-3
Dibenzofuran
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
132-64-9
1,2-Dichlorobenzene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
95-50-1
1,3-Dichlorobenzene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
541-73-1
1,4-Dichlorobenzene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
106-46-7
3,3'-Dichlorobenzidine
ND ug/L
23.3
1
05/12/11 14:00
05/16/11 19:00
91-94-1
2,4-Dichlorophenol
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
120-83-2
Diethylphtha late
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
84-66-2
2,4-Dimethylphenol
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
105-67-9
Dimethylphthalate
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
131-11-3
Di-n-butylphthalate
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
84-74-2
4,6-Dinitro-2-methylphenol
ND ug/L
23.3
1
05/12/11 14:00
05/16/11 19:00
534-52-1
2,4-Dinitrophenol
ND ug/L
58.1
1
05/12/11 14:00
05/16/11 19:00
51-28-5
2,4-Dinitrotoluene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
121-14-2
2,6-Dinitrotoluene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
606-20-2
Di-n-octylphthalate
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/L
7.0
1
05/12/11 14:00
05/16/11 19:00
117-81-7
Fluoranthene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
206-44-0
Fluorene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
87-68-3
Hexachlorobenzene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
118-74-1
Hexachlorocyclopentadiene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
77-47-4
Hexachloroethane
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
193-39-5
Isophorone
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
78-59-1
1-Methylnaphthalene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
90-12-0
2-Methylnaphthalene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
91-57-6
2-Methylphenol(o-Cresol)
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
95-48-7
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 22 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-16 Lab ID: 9293679007 Collected: 05/06/11 14:15 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
3&4-Methylphenol(m&p Cresol)
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
Naphthalene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
91-20-3
2-Nitroaniline
ND ug/L
58.1
1
05/12/11 14:00
05/16/11 19:00
88-74-4
3-Nitroaniline
ND ug/L
58.1
1
05/12/11 14:00
05/16/11 19:00
99-09-2
4-Nitroaniline
ND ug/L
23.3
1
05/12/11 14:00
05/16/11 19:00
100-01-6
Nitrobenzene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
98-95-3
2-Nitrophenol
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
88-75-5
4-Nitrophenol
ND ug/L
58.1
1
05/12/11 14:00
05/16/11 19:00
100-02-7
N-Nitrosodimethylamine
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
621-64-7
N-Nitrosodiphenylamine
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
86-30-6
Pentachlorophenol
ND ug/L
29.1
1
05/12/11 14:00
05/16/11 19:00
87-86-5
Phenanthrene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
85-01-8
Phenol
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
108-95-2
Pyrene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
129-00-0
1,2,4-Trichlorobenzene
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
120-82-1
2,4,5-Trichlorophenol
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
95-95-4
2,4,6-Trichlorophenol
ND ug/L
11.6
1
05/12/11 14:00
05/16/11 19:00
88-06-2
Nitrobenzene-d5 (S)
43 %
21-110
1
05/12/11 14:00
05/16/11 19:00
4165-60-0
2-Fluorobiphenyl (S)
49 %
27-110
1
05/12/11 14:00
05/16/11 19:00
321-60-8
Terphenyl-d14 (S)
74 %
31-107
1
05/12/11 14:00
05/16/11 19:00
1718-51-0
Phenol-d6 (S)
19 %
10-110
1
05/12/11 14:00
05/16/11 19:00
13127-88-3
2-Fluorophenol (S)
31 %
12-110
1
05/12/11 14:00
05/16/11 19:00
367-12-4
2,4,6-Tribromophenol (S)
47 %
27-110
1
05/12/11 14:00
05/16/11 19:00
118-79-6
8260 MSV Low Level
Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/11/11 04:35
67-64-1
Benzene
ND ug/L
1.0
1
05/11/11 04:35
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/11/11 04:35
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/11/11 04:35
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
05/11/11 04:35
75-27-4
Bromoform
ND ug/L
1.0
1
05/11/11 04:35
75-25-2
Bromomethane
ND ug/L
2.0
1
05/11/11 04:35
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/11/11 04:35
78-93-3
Carbon tetrachloride
ND ug/L
1.0
1
05/11/11 04:35
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/11/11 04:35
108-90-7
Chloroethane
ND ug/L
1.0
1
05/11/11 04:35
75-00-3
Chloroform
ND ug/L
1.0
1
05/11/11 04:35
67-66-3
Chloromethane
ND ug/L
1.0
1
05/11/11 04:35
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/11/11 04:35
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/11/11 04:35
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
1
05/11/11 04:35
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/11/11 04:35
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/11/11 04:35
106-93-4
Dibromomethane
ND ug/L
1.0
1
05/11/11 04:35
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 04:35
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 04:35
541-73-1
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY
ANALYSIS
Page 23 of 227
This report shall not be reproduced, except
in
full,
without the written consent of Pace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-16 Lab ID: 9293679007 Collected: 05/06/11 14:15 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 04:35
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/11/11 04:35
75-71-8
1,1-Dichloroethane
2.4 ug/L
1.0
1
05/11/11 04:35
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/11/11 04:35
107-06-2
1,1-Dichloroethene
3.6 ug/L
1.0
1
05/11/11 04:35
75-35-4
cis-1,2-Dichloroethene
1.7 ug/L
1.0
1
05/11/11 04:35
156-59-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 04:35
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 04:35
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/11/11 04:35
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 04:35
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/11/11 04:35
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 04:35
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 04:35
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/11/11 04:35
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/11/11 04:35
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/11/11 04:35
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/11/11 04:35
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
1
05/11/11 04:35
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/11/11 04:35
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/11/11 04:35
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/11/11 04:35
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/11/11 04:35
91-20-3
Styrene
ND ug/L
1.0
1
05/11/11 04:35
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 04:35
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 04:35
79-34-5
Tetrachloroethene
3.2 ug/L
1.0
1
05/11/11 04:35
127-18-4
Toluene
ND ug/L
1.0
1
05/11/11 04:35
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 04:35
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 04:35
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/11/11 04:35
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/11/11 04:35
79-00-5
Trichloroethene
20.0 ug/L
1.0
1
05/11/11 04:35
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/11/11 04:35
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/11/11 04:35
96-18-4
Vinyl acetate
ND ug/L
2.0
1
05/11/11 04:35
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/11/11 04:35
75-01-4
m&p-Xylene
ND ug/L
2.0
1
05/11/11 04:35
179601-23-1
o-Xylene
ND ug/L
1.0
1
05/11/11 04:35
95-47-6
4-Bromofluorobenzene (S)
94 %
70-130
1
05/11/11 04:35
460-00-4
Dibromofluoromethane (S)
102 %
70-130
1
05/11/11 04:35
1868-53-7
1,2-Dichloroethane-d4 (S)
109 %
70-130
1
05/11/11 04:35
17060-07-0
Toluene-d8 (S)
101 %
70-130
1
05/11/11 04:35
2037-26-5
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 24 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-17 Lab ID: 9293679008 Collected: 05/06/11 13:00 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Aluminum
3100 ug/L
100
1
05/12/11 12:30
05/12/11 22:10
7429-90-5
Antimony
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:10
7440-36-0
Arsenic
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:10
7440-38-2
Barium
98.3 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:10
7440-39-3
Beryllium
ND ug/L
1.0
1
05/12/11 12:30
05/12/11 22:10
7440-41-7
Cadmium
ND ug/L
1.0
1
05/12/11 12:30
05/12/11 22:10
7440-43-9
Calcium
15800 ug/L
100
1
05/12/11 12:30
05/12/11 22:10
7440-70-2
Chromium
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:10
7440-47-3
Cobalt
8.2 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:10
7440-48-4
Copper
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:10
7440-50-8
Iron
6390 ug/L
50.0
1
05/12/11 12:30
05/12/11 22:10
7439-89-6
Lead
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:10
7439-92-1
Magnesium
9830 ug/L
100
1
05/12/11 12:30
05/12/11 22:10
7439-95-4
Manganese
365 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:10
7439-96-5
Nickel
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:10
7440-02-0
Potassium
ND ug/L
5000
1
05/12/11 12:30
05/13/11 13:04
7440-09-7
Selenium
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:10
7782-49-2
Silver
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:10
7440-22-4
Sodium
10600 ug/L
5000
1
05/12/11 12:30
05/13/11 13:04
7440-23-5
Thallium
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:10
7440-28-0
Vanadium
5.7 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:10
7440-62-2
Zinc
32.7 ug/L
10.0
1
05/12/11 12:30
05/12/11 22:10
7440-66-6
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
05/17/11 09:40
05/17/11 15:56
7439-97-6
8270 MSSV Semivolatile Organic
Analytical Method: EPA 8270 Preparation Method:
EPA 3510
Acenaphthene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
83-32-9
Acenaphthylene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
208-96-8
Aniline
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
62-53-3
Anthracene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
120-12-7
Benzo(a)anthracene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
56-55-3
Benzo(a)pyrene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
50-32-8
Benzo(b)fluoranthene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
205-99-2
Benzo(g,h,i)perylene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
191-24-2
Benzo(k)fluoranthene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
207-08-9
Benzoic Acid
ND ug/L
56.2
1
05/12/11 14:00
05/16/11 19:27
65-85-0
Benzyl alcohol
ND ug/L
22.5
1
05/12/11 14:00
05/16/11 19:27
100-51-6
4-Bromophenylphenyl ether
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
101-55-3
Butylbenzylphthalate
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
85-68-7
4-Chloro-3-methylphenol
ND ug/L
22.5
1
05/12/11 14:00
05/16/11 19:27
59-50-7
4-Chloroaniline
ND ug/L
22.5
1
05/12/11 14:00
05/16/11 19:27
106-47-8
bis(2-Chloroethoxy)methane
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
111-91-1
bis(2-Chloroethyl) ether
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
108-60-1
2-Chloronaphthalene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
91-58-7
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 25 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-17 Lab ID: 9293679008 Collected: 05/06/11 13:00 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
2-Chlorophenol
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
7005-72-3
Chrysene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
218-01-9
Dibenz(a,h)anthracene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
53-70-3
Dibenzofuran
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
132-64-9
1,2-Dichlorobenzene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
95-50-1
1,3-Dichlorobenzene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
541-73-1
1,4-Dichlorobenzene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
106-46-7
3,3'-Dichlorobenzidine
ND ug/L
22.5
1
05/12/11 14:00
05/16/11 19:27
91-94-1
2,4-Dichlorophenol
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
120-83-2
Diethylphthalate
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
84-66-2
2,4-Dimethylphenol
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
105-67-9
Dimethylphthalate
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
131-11-3
Di-n-butylphthalate
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/L
22.5
1
05/12/11 14:00
05/16/11 19:27
534-52-1
2,4-Dinitrophenol
ND ug/L
56.2
1
05/12/11 14:00
05/16/11 19:27
51-28-5
2,4-Dinitrotoluene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
121-14-2
2,6-Dinitrotoluene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
606-20-2
Di-n-octylphthalate
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/L
6.7
1
05/12/11 14:00
05/16/11 19:27
117-81-7
Fluoranthene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
206-44-0
Fluorene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
87-68-3
Hexachlorobenzene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
118-74-1
Hexachlorocyclopentadiene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
77-47-4
Hexachloroethane
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
193-39-5
Isophorone
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
78-59-1
1-Methylnaphthalene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
90-12-0
2-Methylnaphthalene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
91-57-6
2-Methylphenol(o-Cresol)
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
Naphthalene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
91-20-3
2-Nitroaniline
ND ug/L
56.2
1
05/12/11 14:00
05/16/11 19:27
88-74-4
3-Nitroaniline
ND ug/L
56.2
1
05/12/11 14:00
05/16/11 19:27
99-09-2
4-Nitroaniline
ND ug/L
22.5
1
05/12/11 14:00
05/16/11 19:27
100-01-6
Nitrobenzene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
98-95-3
2-Nitrophenol
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
88-75-5
4-Nitrophenol
ND ug/L
56.2
1
05/12/11 14:00
05/16/11 19:27
100-02-7
N-Nitrosodimethylamine
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
621-64-7
N-Nitrosodiphenylamine
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
86-30-6
Pentachlorophenol
ND ug/L
28.1
1
05/12/11 14:00
05/16/11 19:27
87-86-5
Phenanthrene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
85-01-8
Phenol
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
108-95-2
Pyrene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
129-00-0
1,2,4-Trichlorobenzene
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
120-82-1
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 26 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-17 Lab ID: 9293679008 Collected: 05/06/11 13:00 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
2,4,5-Trichlorophenol
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
95-95-4
2,4,6-Trichlorophenol
ND ug/L
11.2
1
05/12/11 14:00
05/16/11 19:27
88-06-2
Nitrobenzene-d5 (S)
50 %
21-110
1
05/12/11 14:00
05/16/11 19:27
4165-60-0
2-Fluorobiphenyl (S)
61 %
27-110
1
05/12/11 14:00
05/16/11 19:27
321-60-8
Terphenyl-d14 (S)
80 %
31-107
1
05/12/11 14:00
05/16/11 19:27
1718-51-0
Phenol-d6 (S)
24 %
10-110
1
05/12/11 14:00
05/16/11 19:27
13127-88-3
2-Fluorophenol (S)
33 %
12-110
1
05/12/11 14:00
05/16/11 19:27
367-12-4
2,4,6-Tribromophenol (S)
49 %
27-110
1
05/12/11 14:00
05/16/11 19:27
118-79-6
8260 MSV Low Level
Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/11/11 04:59
67-64-1
Benzene
ND ug/L
1.0
1
05/11/11 04:59
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/11/11 04:59
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/11/11 04:59
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
05/11/11 04:59
75-27-4
Bromoform
ND ug/L
1.0
1
05/11/11 04:59
75-25-2
Bromomethane
ND ug/L
2.0
1
05/11/11 04:59
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/11/11 04:59
78-93-3
Carbon tetrachloride
ND ug/L
1.0
1
05/11/11 04:59
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/11/11 04:59
108-90-7
Chloroethane
ND ug/L
1.0
1
05/11/11 04:59
75-00-3
Chloroform
ND ug/L
1.0
1
05/11/11 04:59
67-66-3
Chloromethane
ND ug/L
1.0
1
05/11/11 04:59
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/11/11 04:59
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/11/11 04:59
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
1
05/11/11 04:59
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/11/11 04:59
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/11/11 04:59
106-93-4
Dibromomethane
ND ug/L
1.0
1
05/11/11 04:59
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 04:59
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 04:59
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 04:59
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/11/11 04:59
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
1
05/11/11 04:59
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/11/11 04:59
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
05/11/11 04:59
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 04:59
156-59-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 04:59
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 04:59
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/11/11 04:59
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 04:59
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/11/11 04:59
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 04:59
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 04:59
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/11/11 04:59
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/11/11 04:59
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/11/11 04:59
87-68-3
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 27 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-17 Lab ID: 9293679008 Collected: 05/06/11 13:00 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
2-Hexanone
ND ug/L
5.0
1
05/11/11 04:59
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
1
05/11/11 04:59
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/11/11 04:59
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/11/11 04:59
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/11/11 04:59
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/11/11 04:59
91-20-3
Styrene
ND ug/L
1.0
1
05/11/11 04:59
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 04:59
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 04:59
79-34-5
Tetrachloroethene
35.2 ug/L
1.0
1
05/11/11 04:59
127-18-4
Toluene
ND ug/L
1.0
1
05/11/11 04:59
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 04:59
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 04:59
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/11/11 04:59
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/11/11 04:59
79-00-5
Trichloroethene
ND ug/L
1.0
1
05/11/11 04:59
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/11/11 04:59
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/11/11 04:59
96-18-4
Vinyl acetate
ND ug/L
2.0
1
05/11/11 04:59
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/11/11 04:59
75-01-4
m&p-Xylene
ND ug/L
2.0
1
05/11/11 04:59
179601-23-1
o-Xylene
ND ug/L
1.0
1
05/11/11 04:59
95-47-6
4-Bromofluorobenzene (S)
94 %
70-130
1
05/11/11 04:59
460-00-4
Dibromofluoromethane (S)
103 %
70-130
1
05/11/11 04:59
1868-53-7
1,2-Dichloroethane-d4 (S)
107 %
70-130
1
05/11/11 04:59
17060-07-0
Toluene-d8 (S)
103 %
70-130
1
05/11/11 04:59
2037-26-5
Sample: MW-18 Lab ID: 9293679009 Collected: 05/06/11 10:00 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Aluminum
424 ug/L
100
1
05/12/11 12:30
05/12/11 22:13
7429-90-5
Antimony
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:13
7440-36-0
Arsenic
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:13
7440-38-2
Barium
56.6 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:13
7440-39-3
Beryllium
ND ug/L
1.0
1
05/12/11 12:30
05/12/11 22:13
7440-41-7
Cadmium
ND ug/L
1.0
1
05/12/11 12:30
05/12/11 22:13
7440-43-9
Calcium
9740 ug/L
100
1
05/12/11 12:30
05/12/11 22:13
7440-70-2
Chromium
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:13
7440-47-3
Cobalt
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:13
7440-48-4
Copper
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:13
7440-50-8
Iron
390 ug/L
50.0
1
05/12/11 12:30
05/12/11 22:13
7439-89-6
Lead
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:13
7439-92-1
Magnesium
5750 ug/L
100
1
05/12/11 12:30
05/12/11 22:13
7439-95-4
Manganese
122 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:13
7439-96-5
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY
ANALYSIS
Page 28 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-18 Lab ID: 9293679009 Collected: 05/06/11 10:00 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Nickel
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:13
7440-02-0
Potassium
ND ug/L
5000
1
05/12/11 12:30
05/13/11 13:08
7440-09-7
Selenium
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:13
7782-49-2
Silver
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:13
7440-22-4
Sodium
9160 ug/L
5000
1
05/12/11 12:30
05/13/11 13:08
7440-23-5
Thallium
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:13
7440-28-0
Vanadium
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:13
7440-62-2
Zinc
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:13
7440-66-6
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
05/17/11 09:40
05/17/11 15:59
7439-97-6
8270 MSSV Semivolatile Organic
Analytical Method: EPA 8270 Preparation Method:
EPA 3510
Acenaphthene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
83-32-9
Acenaphthylene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
208-96-8
Aniline
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
62-53-3
Anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
120-12-7
Benzo(a)anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
56-55-3
Benzo(a)pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
50-32-8
Benzo(b)fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
205-99-2
Benzo(g,h,i)perylene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
191-24-2
Benzo(k)fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
207-08-9
Benzoic Acid
ND ug/L
50.0
1
05/13/11 10:39
05/17/11 21:24
65-85-0
Benzyl alcohol
ND ug/L
20.0
1
05/13/11 10:39
05/17/11 21:24
100-51-6
4-Bromophenylphenyl ether
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
101-55-3
Butylbenzylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
85-68-7
4-Chloro-3-methylphenol
ND ug/L
20.0
1
05/13/11 10:39
05/17/11 21:24
59-50-7
4-Chloroaniline
ND ug/L
20.0
1
05/13/11 10:39
05/17/11 21:24
106-47-8
bis(2-Chloroethoxy)methane
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
111-91-1
bis(2-Chloroethyl) ether
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
108-60-1
2-Chloronaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
91-58-7
2-Chlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
7005-72-3
Chrysene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
218-01-9
Dibenz(a,h)anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
53-70-3
Dibenzofuran
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
132-64-9
1,2-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
95-50-1
1,3-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
541-73-1
1,4-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
106-46-7
3,3'-Dichlorobenzidine
ND ug/L
20.0
1
05/13/11 10:39
05/17/11 21:24
91-94-1
2,4-Dichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
120-83-2
Diethylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
84-66-2
2,4-Dimethylphenol
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
105-67-9
Dimethylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
131-11-3
Di-n-butylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
84-74-2
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 29 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-18 Lab ID: 9293679009 Collected: 05/06/11 10:00 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
4,6-Dinitro-2-methyl phenol
ND ug/L
20.0
1
05/13/11 10:39
05/17/11 21:24
534-52-1
2,4-Dinitrophenol
ND ug/L
50.0
1
05/13/11 10:39
05/17/11 21:24
51-28-5
2,4-Dinitrotoluene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
121-14-2
2,6-Dinitrotoluene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
606-20-2
Di-n-octylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/L
6.0
1
05/13/11 10:39
05/17/11 21:24
117-81-7
Fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
206-44-0
Fluorene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
87-68-3
Hexachlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
118-74-1
Hexachlorocyclopentadiene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
77-47-4
Hexachloroethane
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
193-39-5
Isophorone
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
78-59-1
1-Methylnaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
90-12-0
2-Methylnaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
91-57-6
2-Methylphenol(o-Cresol)
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
Naphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
91-20-3
2-Nitroaniline
ND ug/L
50.0
1
05/13/11 10:39
05/17/11 21:24
88-74-4
3-Nitroaniline
ND ug/L
50.0
1
05/13/11 10:39
05/17/11 21:24
99-09-2
4-Nitroaniline
ND ug/L
20.0
1
05/13/11 10:39
05/17/11 21:24
100-01-6
Nitrobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
98-95-3
2-Nitrophenol
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
88-75-5
4-Nitrophenol
ND ug/L
50.0
1
05/13/11 10:39
05/17/11 21:24
100-02-7
N-Nitrosodimethylamine
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
621-64-7
N-Nitrosodiphenylamine
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
86-30-6
Pentachlorophenol
ND ug/L
25.0
1
05/13/11 10:39
05/17/11 21:24
87-86-5
Phenanthrene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
85-01-8
Phenol
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
108-95-2
Pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
129-00-0
1,2,4-Trichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
120-82-1
2,4,5-Trichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
95-95-4
2,4,6-Trichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/17/11 21:24
88-06-2
Nitrobenzene-d5 (S)
42 %
21-110
1
05/13/11 10:39
05/17/11 21:24
4165-60-0
2-Fluorobiphenyl (S)
46 %
27-110
1
05/13/11 10:39
05/17/11 21:24
321-60-8
Terphenyl-d14 (S)
65 %
31-107
1
05/13/11 10:39
05/17/11 21:24
1718-51-0
Phenol-d6 (S)
14 %
10-110
1
05/13/11 10:39
05/17/11 21:24
13127-88-3
2-Fluorophenol (S)
26 %
12-110
1
05/13/11 10:39
05/17/11 21:24
367-12-4
2,4,6-Tribromophenol (S)
45 %
27-110
1
05/13/11 10:39
05/17/11 21:24
118-79-6
8260 MSV Low Level
Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/11/11 05:23
67-64-1
Benzene
ND ug/L
1.0
1
05/11/11 05:23
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/11/11 05:23
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/11/11 05:23
74-97-5
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 30 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-18 Lab ID: 9293679009 Collected: 05/06/11 10:00 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Bromodichloromethane
ND ug/L
1.0
1
05/11/11 05:23
75-27-4
Bromoform
ND ug/L
1.0
1
05/11/11 05:23
75-25-2
Bromomethane
ND ug/L
2.0
1
05/11/11 05:23
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/11/11 05:23
78-93-3
Carbon tetrachloride
ND ug/L
1.0
1
05/11/11 05:23
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/11/11 05:23
108-90-7
Chloroethane
ND ug/L
1.0
1
05/11/11 05:23
75-00-3
Chloroform
ND ug/L
1.0
1
05/11/11 05:23
67-66-3
Chloromethane
ND ug/L
1.0
1
05/11/11 05:23
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/11/11 05:23
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/11/11 05:23
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
1
05/11/11 05:23
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/11/11 05:23
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/11/11 05:23
106-93-4
Dibromomethane
ND ug/L
1.0
1
05/11/11 05:23
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 05:23
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 05:23
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 05:23
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/11/11 05:23
75-71-8
1,1-Dichloroethane
1.0 ug/L
1.0
1
05/11/11 05:23
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/11/11 05:23
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
05/11/11 05:23
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 05:23
156-59-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 05:23
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 05:23
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/11/11 05:23
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 05:23
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/11/11 05:23
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 05:23
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 05:23
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/11/11 05:23
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/11/11 05:23
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/11/11 05:23
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/11/11 05:23
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
1
05/11/11 05:23
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/11/11 05:23
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/11/11 05:23
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/11/11 05:23
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/11/11 05:23
91-20-3
Styrene
ND ug/L
1.0
1
05/11/11 05:23
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 05:23
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 05:23
79-34-5
Tetrachloroethene
7.5 ug/L
1.0
1
05/11/11 05:23
127-18-4
Toluene
ND ug/L
1.0
1
05/11/11 05:23
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 05:23
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 05:23
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/11/11 05:23
71-55-6
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 31 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-18 Lab ID: 9293679009 Collected: 05/06/11 10:00 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Analytical Method: EPA 8260
ND ug/L
1.0
1
05/11/11 05:23
79-00-5
ND ug/L
1.0
1
05/11/11 05:23
79-01-6
ND ug/L
1.0
1
05/11/11 05:23
75-69-4
ND ug/L
1.0
1
05/11/11 05:23
96-18-4
ND ug/L
2.0
1
05/11/11 05:23
108-05-4
ND ug/L
1.0
1
05/11/11 05:23
75-01-4
ND ug/L
2.0
1
05/11/11 05:23
179601-23-1
ND ug/L
1.0
1
05/11/11 05:23
95-47-6
97 %
70-130
1
05/11/11 05:23
460-00-4
102 %
70-130
1
05/11/11 05:23
1868-53-7
108 %
70-130
1
05/11/11 05:23
17060-07-0
101 %
70-130
1
05/11/11 05:23
2037-26-5
Sample: MW-20 Lab ID: 9293679010 Collected: 05/06/11 08:30 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
7470 Mercury
Mercury
Date: 05/20/2011 04:57 PM
Analytical Method: EPA 6010 Preparation Method: EPA 3010
180 ug/L
100
1
05/12/11 12:30
05/12/11 22:16
7429-90-5
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:16
7440-36-0
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:16
7440-38-2
43.6 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:16
7440-39-3
ND ug/L
1.0
1
05/12/11 12:30
05/12/11 22:16
7440-41-7
ND ug/L
1.0
1
05/12/11 12:30
05/12/11 22:16
7440-43-9
8170 ug/L
100
1
05/12/11 12:30
05/12/11 22:16
7440-70-2
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:16
7440-47-3
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:16
7440-48-4
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:16
7440-50-8
302 ug/L
50.0
1
05/12/11 12:30
05/12/11 22:16
7439-89-6
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:16
7439-92-1
5160 ug/L
100
1
05/12/11 12:30
05/12/11 22:16
7439-95-4
215 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:16
7439-96-5
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:16
7440-02-0
ND ug/L
5000
1
05/12/11 12:30
05/13/11 13:22
7440-09-7
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:16
7782-49-2
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:16
7440-22-4
6870 ug/L
5000
1
05/12/11 12:30
05/13/11 13:22
7440-23-5
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:16
7440-28-0
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:16
7440-62-2
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:16
7440-66-6
Analytical Method: EPA 7470 Preparation Method: EPA 7470
ND ug/L 0.20 1 05/17/11 09:40 05/17/11 16:01 7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 32 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-20 Lab ID: 9293679010 Collected: 05/06/11 08:30 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
83-32-9
Acenaphthylene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
208-96-8
Aniline
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
62-53-3
Anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
120-12-7
Benzo(a)anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
56-55-3
Benzo(a)pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
50-32-8
Benzo(b)fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
205-99-2
Benzo(g,h,i)perylene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
191-24-2
Benzo(k)fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
207-08-9
Benzoic Acid
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 14:56
65-85-0
Benzyl alcohol
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 14:56
100-51-6
4-Bromophenylphenyl ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
101-55-3
Butylbenzylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
85-68-7
4-Chloro-3-methylphenol
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 14:56
59-50-7
4-Chloroaniline
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 14:56
106-47-8
bis(2-Chloroethoxy)methane
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
111-91-1
bis(2-Chloroethyl) ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
108-60-1
2-Chloronaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
91-58-7
2-Chlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
7005-72-3
Chrysene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
218-01-9
Dibenz(a,h)anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
53-70-3
Dibenzofuran
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
132-64-9
1,2-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
95-50-1
1,3-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
541-73-1
1,4-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
106-46-7
3,3'-Dichlorobenzidine
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 14:56
91-94-1
2,4-Dichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
120-83-2
Diethylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
84-66-2
2,4-Dimethylphenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
105-67-9
Dimethylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
131-11-3
Di-n-butylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
84-74-2
4,6-Dinitro-2-methylphenol
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 14:56
534-52-1
2,4-Dinitrophenol
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 14:56
51-28-5
2,4-Dinitrotoluene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
121-14-2
2,6-Dinitrotoluene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
606-20-2
Di-n-octylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/L
6.0
1
05/13/11 10:39
05/18/11 14:56
117-81-7
Fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
206-44-0
Fluorene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
87-68-3
Hexachlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
118-74-1
Hexachlorocyclopentadiene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
77-47-4
Hexachloroethane
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
193-39-5
Isophorone
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
78-59-1
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 33 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-20
Lab ID: 9293679010 Collected: 05/06/11 08:30
Received: 05/07/11 10:40 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8270 MSSV Semivolatile Organic
Analytical Method: EPA 8270 Preparation Method: EPA 3510
1-Methylnaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
90-12-0
2-Methylnaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
91-57-6
2-Methylphenol(o-Cresol)
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
Naphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
91-20-3
2-Nitroaniline
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 14:56
88-74-4
3-Nitroaniline
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 14:56
99-09-2
4-Nitroaniline
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 14:56
100-01-6
Nitrobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
98-95-3
2-Nitrophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
88-75-5
4-Nitrophenol
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 14:56
100-02-7
N-Nitrosodimethylamine
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
621-64-7
N-Nitrosodiphenylamine
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
86-30-6
Pentachlorophenol
ND ug/L
25.0
1
05/13/11 10:39
05/18/11 14:56
87-86-5
Phenanthrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
85-01-8
Phenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
108-95-2
Pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
129-00-0
1,2,4-Trichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
120-82-1
2,4,5-Trichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
95-95-4
2,4,6-Trichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 14:56
88-06-2
Nitrobenzene-d5 (S)
43 %
21-110
1
05/13/11 10:39
05/18/11 14:56
4165-60-0
2-Fluorobiphenyl (S)
44 %
27-110
1
05/13/11 10:39
05/18/11 14:56
321-60-8
Terphenyl-d14 (S)
63 %
31-107
1
05/13/11 10:39
05/18/11 14:56
1718-51-0
Phenol-d6 (S)
16 %
10-110
1
05/13/11 10:39
05/18/11 14:56
13127-88-3
2-Fluorophenol (S)
25 %
12-110
1
05/13/11 10:39
05/18/11 14:56
367-12-4
2,4,6-Tribromophenol (S)
19 %
27-110
1
05/13/11 10:39
05/18/11 14:56
118-79-6 SO
8260 MSV Low Level
Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/11/11 05:47
67-64-1
Benzene
ND ug/L
1.0
1
05/11/11 05:47
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/11/11 05:47
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/11/11 05:47
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
05/11/11 05:47
75-27-4
Bromoform
ND ug/L
1.0
1
05/11/11 05:47
75-25-2
Bromomethane
ND ug/L
2.0
1
05/11/11 05:47
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/11/11 05:47
78-93-3
Carbon tetrachloride
ND ug/L
1.0
1
05/11/11 05:47
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/11/11 05:47
108-90-7
Chloroethane
ND ug/L
1.0
1
05/11/11 05:47
75-00-3
Chloroform
ND ug/L
1.0
1
05/11/11 05:47
67-66-3
Chloromethane
ND ug/L
1.0
1
05/11/11 05:47
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/11/11 05:47
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/11/11 05:47
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
1
05/11/11 05:47
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/11/11 05:47
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/11/11 05:47
106-93-4
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
Page 34 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-20 Lab ID: 9293679010 Collected: 05/06/11 08:30 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Dibromomethane
ND ug/L
1.0
1
05/11/11 05:47
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 05:47
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 05:47
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 05:47
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/11/11 05:47
75-71-8
1,1-Dichloroethane
2.3 ug/L
1.0
1
05/11/11 05:47
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/11/11 05:47
107-06-2
1,1-Dichloroethene
12.9 ug/L
1.0
1
05/11/11 05:47
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 05:47
156-59-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 05:47
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 05:47
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/11/11 05:47
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 05:47
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/11/11 05:47
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 05:47
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 05:47
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/11/11 05:47
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/11/11 05:47
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/11/11 05:47
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/11/11 05:47
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
1
05/11/11 05:47
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/11/11 05:47
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/11/11 05:47
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/11/11 05:47
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/11/11 05:47
91-20-3
Styrene
ND ug/L
1.0
1
05/11/11 05:47
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 05:47
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 05:47
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
05/11/11 05:47
127-18-4
Toluene
ND ug/L
1.0
1
05/11/11 05:47
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 05:47
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 05:47
120-82-1
1,1,1-Trichloroethane
80.8 ug/L
1.0
1
05/11/11 05:47
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/11/11 05:47
79-00-5
Trichloroethene
2.3 ug/L
1.0
1
05/11/11 05:47
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/11/11 05:47
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/11/11 05:47
96-18-4
Vinyl acetate
ND ug/L
2.0
1
05/11/11 05:47
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/11/11 05:47
75-01-4
m&p-Xylene
ND ug/L
2.0
1
05/11/11 05:47
179601-23-1
o-Xylene
ND ug/L
1.0
1
05/11/11 05:47
95-47-6
4-Bromofluorobenzene (S)
94 %
70-130
1
05/11/11 05:47
460-00-4
Dibromofluoromethane (S)
101 %
70-130
1
05/11/11 05:47
1868-53-7
1,2-Dichloroethane-d4 (S)
109 %
70-130
1
05/11/11 05:47
17060-07-0
Toluene-d8 (S)
101 %
70-130
1
05/11/11 05:47
2037-26-5
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 35 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-21 Lab ID: 9293679011 Collected: 05/06/11 11:50 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Aluminum
5600 ug/L
100
1
05/12/11 12:30
05/12/11 22:20
7429-90-5
Antimony
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:20
7440-36-0
Arsenic
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:20
7440-38-2
Barium
92.7 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:20
7440-39-3
Beryllium
ND ug/L
1.0
1
05/12/11 12:30
05/12/11 22:20
7440-41-7
Cadmium
ND ug/L
1.0
1
05/12/11 12:30
05/12/11 22:20
7440-43-9
Calcium
10700 ug/L
100
1
05/12/11 12:30
05/12/11 22:20
7440-70-2
Chromium
5.5 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:20
7440-47-3
Cobalt
7.5 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:20
7440-48-4
Copper
5.9 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:20
7440-50-8
Iron
7970 ug/L
50.0
1
05/12/11 12:30
05/12/11 22:20
7439-89-6
Lead
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:20
7439-92-1
Magnesium
6110 ug/L
100
1
05/12/11 12:30
05/12/11 22:20
7439-95-4
Manganese
680 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:20
7439-96-5
Nickel
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:20
7440-02-0
Potassium
ND ug/L
5000
1
05/12/11 12:30
05/13/11 13:25
7440-09-7
Selenium
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:20
7782-49-2
Silver
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:20
7440-22-4
Sodium
26700 ug/L
5000
1
05/12/11 12:30
05/13/11 13:25
7440-23-5
Thallium
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:20
7440-28-0
Vanadium
6.7 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:20
7440-62-2
Zinc
28.9 ug/L
10.0
1
05/12/11 12:30
05/12/11 22:20
7440-66-6
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
05/17/11 09:40
05/17/11 16:04
7439-97-6
8270 MSSV Semivolatile Organic
Analytical Method: EPA 8270 Preparation Method:
EPA 3510
Acenaphthene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
83-32-9
Acenaphthylene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
208-96-8
Aniline
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
62-53-3
Anthracene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
120-12-7
Benzo(a)anthracene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
56-55-3
Benzo(a)pyrene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
50-32-8
Benzo(b)fluoranthene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
205-99-2
Benzo(g,h,i)perylene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
191-24-2
Benzo(k)fluoranthene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
207-08-9
Benzoic Acid
ND ug/L
54.3
1
05/13/11 10:39
05/18/11 15:23
65-85-0
Benzyl alcohol
ND ug/L
21.7
1
05/13/11 10:39
05/18/11 15:23
100-51-6
4-Bromophenylphenyl ether
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
101-55-3
Butylbenzylphthalate
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
85-68-7
4-Chloro-3-methylphenol
ND ug/L
21.7
1
05/13/11 10:39
05/18/11 15:23
59-50-7
4-Chloroaniline
ND ug/L
21.7
1
05/13/11 10:39
05/18/11 15:23
106-47-8
bis(2-Chloroethoxy)methane
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
111-91-1
bis(2-Chloroethyl) ether
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
108-60-1
2-Chloronaphthalene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
91-58-7
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 36 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-21 Lab ID: 9293679011 Collected: 05/06/11 11:50 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
2-Chlorophenol
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
7005-72-3
Chrysene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
218-01-9
Dibenz(a,h)anthracene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
53-70-3
Dibenzofuran
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
132-64-9
1,2-Dichlorobenzene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
95-50-1
1,3-Dichlorobenzene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
541-73-1
1,4-Dichlorobenzene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
106-46-7
3,3'-Dichlorobenzidine
ND ug/L
21.7
1
05/13/11 10:39
05/18/11 15:23
91-94-1
2,4-Dichlorophenol
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
120-83-2
Diethylphthalate
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
84-66-2
2,4-Dimethylphenol
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
105-67-9
Dimethylphthalate
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
131-11-3
Di-n-butylphthalate
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/L
21.7
1
05/13/11 10:39
05/18/11 15:23
534-52-1
2,4-Dinitrophenol
ND ug/L
54.3
1
05/13/11 10:39
05/18/11 15:23
51-28-5
2,4-Dinitrotoluene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
121-14-2
2,6-Dinitrotoluene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
606-20-2
Di-n-octylphthalate
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/L
6.5
1
05/13/11 10:39
05/18/11 15:23
117-81-7
Fluoranthene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
206-44-0
Fluorene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
87-68-3
Hexachlorobenzene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
118-74-1
Hexachlorocyclopentadiene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
77-47-4
Hexachloroethane
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
193-39-5
Isophorone
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
78-59-1
1-Methylnaphthalene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
90-12-0
2-Methylnaphthalene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
91-57-6
2-Methylphenol(o-Cresol)
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
Naphthalene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
91-20-3
2-Nitroaniline
ND ug/L
54.3
1
05/13/11 10:39
05/18/11 15:23
88-74-4
3-Nitroaniline
ND ug/L
54.3
1
05/13/11 10:39
05/18/11 15:23
99-09-2
4-Nitroaniline
ND ug/L
21.7
1
05/13/11 10:39
05/18/11 15:23
100-01-6
Nitrobenzene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
98-95-3
2-Nitrophenol
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
88-75-5
4-Nitrophenol
ND ug/L
54.3
1
05/13/11 10:39
05/18/11 15:23
100-02-7
N-Nitrosodimethylamine
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
621-64-7
N-Nitrosodiphenylamine
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
86-30-6
Pentachlorophenol
ND ug/L
27.2
1
05/13/11 10:39
05/18/11 15:23
87-86-5
Phenanthrene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
85-01-8
Phenol
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
108-95-2
Pyrene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
129-00-0
1,2,4-Trichlorobenzene
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
120-82-1
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 37 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-21 Lab ID: 9293679011 Collected: 05/06/11 11:50 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
2,4,5-Trichlorophenol
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
95-95-4
2,4,6-Trichlorophenol
ND ug/L
10.9
1
05/13/11 10:39
05/18/11 15:23
88-06-2
Nitrobenzene-d5 (S)
51 %
21-110
1
05/13/11 10:39
05/18/11 15:23
4165-60-0
2-Fluorobiphenyl (S)
52 %
27-110
1
05/13/11 10:39
05/18/11 15:23
321-60-8
Terphenyl-d14 (S)
64 %
31-107
1
05/13/11 10:39
05/18/11 15:23
1718-51-0
Phenol-d6 (S)
20 %
10-110
1
05/13/11 10:39
05/18/11 15:23
13127-88-3
2-Fluorophenol (S)
36 %
12-110
1
05/13/11 10:39
05/18/11 15:23
367-12-4
2,4,6-Tribromophenol (S)
49 %
27-110
1
05/13/11 10:39
05/18/11 15:23
118-79-6
8260 MSV Low Level
Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/11/11 06:12
67-64-1
Benzene
ND ug/L
1.0
1
05/11/11 06:12
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/11/11 06:12
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/11/11 06:12
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
05/11/11 06:12
75-27-4
Bromoform
ND ug/L
1.0
1
05/11/11 06:12
75-25-2
Bromomethane
ND ug/L
2.0
1
05/11/11 06:12
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/11/11 06:12
78-93-3
Carbon tetrachloride
ND ug/L
1.0
1
05/11/11 06:12
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/11/11 06:12
108-90-7
Chloroethane
ND ug/L
1.0
1
05/11/11 06:12
75-00-3
Chloroform
ND ug/L
1.0
1
05/11/11 06:12
67-66-3
Chloromethane
ND ug/L
1.0
1
05/11/11 06:12
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/11/11 06:12
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/11/11 06:12
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
1
05/11/11 06:12
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/11/11 06:12
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/11/11 06:12
106-93-4
Dibromomethane
ND ug/L
1.0
1
05/11/11 06:12
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 06:12
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 06:12
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 06:12
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/11/11 06:12
75-71-8
1,1-Dichloroethane
2.6 ug/L
1.0
1
05/11/11 06:12
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/11/11 06:12
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
05/11/11 06:12
75-35-4
cis-1,2-Dichloroethene
22.0 ug/L
1.0
1
05/11/11 06:12
156-59-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 06:12
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 06:12
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/11/11 06:12
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 06:12
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/11/11 06:12
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 06:12
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 06:12
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/11/11 06:12
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/11/11 06:12
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/11/11 06:12
87-68-3
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 38 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-21 Lab ID: 9293679011 Collected: 05/06/11 11:50 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
2-Hexanone
ND ug/L
5.0
1
05/11/11 06:12
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
1
05/11/11 06:12
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/11/11 06:12
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/11/11 06:12
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/11/11 06:12
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/11/11 06:12
91-20-3
Styrene
ND ug/L
1.0
1
05/11/11 06:12
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 06:12
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 06:12
79-34-5
Tetrachloroethene
77.8 ug/L
1.0
1
05/11/11 06:12
127-18-4
Toluene
ND ug/L
1.0
1
05/11/11 06:12
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 06:12
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 06:12
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/11/11 06:12
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/11/11 06:12
79-00-5
Trichloroethene
20.2 ug/L
1.0
1
05/11/11 06:12
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/11/11 06:12
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/11/11 06:12
96-18-4
Vinyl acetate
ND ug/L
2.0
1
05/11/11 06:12
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/11/11 06:12
75-01-4
m&p-Xylene
ND ug/L
2.0
1
05/11/11 06:12
179601-23-1
o-Xylene
ND ug/L
1.0
1
05/11/11 06:12
95-47-6
4-Bromofluorobenzene (S)
95 %
70-130
1
05/11/11 06:12
460-00-4
Dibromofluoromethane (S)
105 %
70-130
1
05/11/11 06:12
1868-53-7
1,2-Dichloroethane-d4 (S)
110 %
70-130
1
05/11/11 06:12
17060-07-0
Toluene-d8 (S)
101 %
70-130
1
05/11/11 06:12
2037-26-5
Sample: MW-22 Lab ID: 9293679012 Collected: 05/06/11 15:15 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Aluminum
149 ug/L
100
1
05/12/11 12:30
05/12/11 22:33
7429-90-5
Antimony
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:33
7440-36-0
Arsenic
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:33
7440-38-2
Barium
41.3 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:33
7440-39-3
Beryllium
ND ug/L
1.0
1
05/12/11 12:30
05/12/11 22:33
7440-41-7
Cadmium
ND ug/L
1.0
1
05/12/11 12:30
05/12/11 22:33
7440-43-9
Calcium
20200 ug/L
100
1
05/12/11 12:30
05/12/11 22:33
7440-70-2
Chromium
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:33
7440-47-3
Cobalt
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:33
7440-48-4
Copper
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:33
7440-50-8
Iron
265 ug/L
50.0
1
05/12/11 12:30
05/12/11 22:33
7439-89-6
Lead
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:33
7439-92-1
Magnesium
8930 ug/L
100
1
05/12/11 12:30
05/12/11 22:33
7439-95-4
Manganese
44.3 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:33
7439-96-5
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY
ANALYSIS
Page 39 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-22 Lab ID: 9293679012 Collected: 05/06/11 15:15 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Nickel
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:33
7440-02-0
Potassium
ND ug/L
5000
1
05/12/11 12:30
05/13/11 13:29
7440-09-7
Selenium
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:33
7782-49-2
Silver
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:33
7440-22-4
Sodium
10000 ug/L
5000
1
05/12/11 12:30
05/13/11 13:29
7440-23-5
Thallium
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:33
7440-28-0
Vanadium
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:33
7440-62-2
Zinc
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:33
7440-66-6
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
05/17/11 09:40
05/17/11 16:07
7439-97-6
8270 MSSV Semivolatile Organic
Analytical Method: EPA 8270 Preparation Method:
EPA 3510
Acenaphthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
83-32-9
Acenaphthylene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
208-96-8
Aniline
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
62-53-3
Anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
120-12-7
Benzo(a)anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
56-55-3
Benzo(a)pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
50-32-8
Benzo(b)fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
205-99-2
Benzo(g,h,i)perylene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
191-24-2
Benzo(k)fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
207-08-9
Benzoic Acid
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 15:50
65-85-0
Benzyl alcohol
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 15:50
100-51-6
4-Bromophenylphenyl ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
101-55-3
Butylbenzylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
85-68-7
4-Chloro-3-methylphenol
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 15:50
59-50-7
4-Chloroaniline
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 15:50
106-47-8
bis(2-Chloroethoxy)methane
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
111-91-1
bis(2-Chloroethyl) ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
108-60-1
2-Chloronaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
91-58-7
2-Chlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
7005-72-3
Chrysene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
218-01-9
Dibenz(a,h)anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
53-70-3
Dibenzofuran
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
132-64-9
1,2-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
95-50-1
1,3-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
541-73-1
1,4-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
106-46-7
3,3'-Dichlorobenzidine
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 15:50
91-94-1
2,4-Dichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
120-83-2
Diethylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
84-66-2
2,4-Dimethylphenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
105-67-9
Dimethylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
131-11-3
Di-n-butylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
84-74-2
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 40 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-22 Lab ID: 9293679012 Collected: 05/06/11 15:15 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
4,6-Dinitro-2-methyl phenol
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 15:50
534-52-1
2,4-Dinitrophenol
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 15:50
51-28-5
2,4-Dinitrotoluene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
121-14-2
2,6-Dinitrotoluene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
606-20-2
Di-n-octylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/L
6.0
1
05/13/11 10:39
05/18/11 15:50
117-81-7
Fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
206-44-0
Fluorene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
87-68-3
Hexachlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
118-74-1
Hexachlorocyclopentadiene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
77-47-4
Hexachloroethane
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
193-39-5
Isophorone
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
78-59-1
1-Methylnaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
90-12-0
2-Methylnaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
91-57-6
2-Methylphenol(o-Cresol)
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
Naphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
91-20-3
2-Nitroaniline
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 15:50
88-74-4
3-Nitroaniline
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 15:50
99-09-2
4-Nitroaniline
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 15:50
100-01-6
Nitrobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
98-95-3
2-Nitrophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
88-75-5
4-Nitrophenol
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 15:50
100-02-7
N-Nitrosodimethylamine
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
621-64-7
N-Nitrosodiphenylamine
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
86-30-6
Pentachlorophenol
ND ug/L
25.0
1
05/13/11 10:39
05/18/11 15:50
87-86-5
Phenanthrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
85-01-8
Phenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
108-95-2
Pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
129-00-0
1,2,4-Trichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
120-82-1
2,4,5-Trichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
95-95-4
2,4,6-Trichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 15:50
88-06-2
Nitrobenzene-d5 (S)
38 %
21-110
1
05/13/11 10:39
05/18/11 15:50
4165-60-0
2-Fluorobiphenyl (S)
39 %
27-110
1
05/13/11 10:39
05/18/11 15:50
321-60-8
Terphenyl-d14 (S)
56 %
31-107
1
05/13/11 10:39
05/18/11 15:50
1718-51-0
Phenol-d6 (S)
14 %
10-110
1
05/13/11 10:39
05/18/11 15:50
13127-88-3
2-Fluorophenol (S)
26 %
12-110
1
05/13/11 10:39
05/18/11 15:50
367-12-4
2,4,6-Tribromophenol (S)
45 %
27-110
1
05/13/11 10:39
05/18/11 15:50
118-79-6
8260 MSV Low Level
Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/11/11 06:36
67-64-1
Benzene
ND ug/L
1.0
1
05/11/11 06:36
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/11/11 06:36
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/11/11 06:36
74-97-5
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 41 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-22 Lab ID: 9293679012 Collected: 05/06/11 15:15 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Bromodichloromethane
ND ug/L
1.0
1
05/11/11 06:36
75-27-4
Bromoform
ND ug/L
1.0
1
05/11/11 06:36
75-25-2
Bromomethane
ND ug/L
2.0
1
05/11/11 06:36
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/11/11 06:36
78-93-3
Carbon tetrachloride
ND ug/L
1.0
1
05/11/11 06:36
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/11/11 06:36
108-90-7
Chloroethane
ND ug/L
1.0
1
05/11/11 06:36
75-00-3
Chloroform
ND ug/L
1.0
1
05/11/11 06:36
67-66-3
Chloromethane
ND ug/L
1.0
1
05/11/11 06:36
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/11/11 06:36
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/11/11 06:36
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
1
05/11/11 06:36
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/11/11 06:36
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/11/11 06:36
106-93-4
Dibromomethane
ND ug/L
1.0
1
05/11/11 06:36
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 06:36
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 06:36
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 06:36
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/11/11 06:36
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
1
05/11/11 06:36
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/11/11 06:36
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
05/11/11 06:36
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 06:36
156-59-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 06:36
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 06:36
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/11/11 06:36
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 06:36
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/11/11 06:36
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 06:36
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 06:36
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/11/11 06:36
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/11/11 06:36
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/11/11 06:36
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/11/11 06:36
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
1
05/11/11 06:36
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/11/11 06:36
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/11/11 06:36
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/11/11 06:36
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/11/11 06:36
91-20-3
Styrene
ND ug/L
1.0
1
05/11/11 06:36
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 06:36
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 06:36
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
05/11/11 06:36
127-18-4
Toluene
ND ug/L
1.0
1
05/11/11 06:36
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 06:36
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 06:36
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/11/11 06:36
71-55-6
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 42 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-22 Lab ID: 9293679012 Collected: 05/06/11 15:15 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Analytical Method: EPA 8260
ND ug/L
1.0
1
05/11/11 06:36
79-00-5
ND ug/L
1.0
1
05/11/11 06:36
79-01-6
ND ug/L
1.0
1
05/11/11 06:36
75-69-4
ND ug/L
1.0
1
05/11/11 06:36
96-18-4
ND ug/L
2.0
1
05/11/11 06:36
108-05-4
ND ug/L
1.0
1
05/11/11 06:36
75-01-4
ND ug/L
2.0
1
05/11/11 06:36
179601-23-1
ND ug/L
1.0
1
05/11/11 06:36
95-47-6
95 %
70-130
1
05/11/11 06:36
460-00-4
105 %
70-130
1
05/11/11 06:36
1868-53-7
107 %
70-130
1
05/11/11 06:36
17060-07-0
99 %
70-130
1
05/11/11 06:36
2037-26-5
Sample: MW-24 Lab ID: 9293679013 Collected: 05/06/11 17:15 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
7470 Mercury
Mercury
Date: 05/20/2011 04:57 PM
Analytical Method: EPA 6010 Preparation Method: EPA 3010
15000 ug/L
100
1
05/12/11 12:30
05/12/11 22:36
7429-90-5
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:36
7440-36-0
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:36
7440-38-2
240 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:36
7440-39-3
1.1 ug/L
1.0
1
05/12/11 12:30
05/12/11 22:36
7440-41-7
ND ug/L
1.0
1
05/12/11 12:30
05/12/11 22:36
7440-43-9
2400 ug/L
100
1
05/12/11 12:30
05/12/11 22:36
7440-70-2
15.2 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:36
7440-47-3
14.8 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:36
7440-48-4
14.3 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:36
7440-50-8
26000 ug/L
50.0
1
05/12/11 12:30
05/12/11 22:36
7439-89-6
7.8 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:36
7439-92-1
3030 ug/L
100
1
05/12/11 12:30
05/12/11 22:36
7439-95-4
424 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:36
7439-96-5
11.8 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:36
7440-02-0
ND ug/L
5000
1
05/12/11 12:30
05/13/11 13:32
7440-09-7
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:36
7782-49-2
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:36
7440-22-4
5250 ug/L
5000
1
05/12/11 12:30
05/13/11 13:32
7440-23-5
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:36
7440-28-0
32.3 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:36
7440-62-2
34.5 ug/L
10.0
1
05/12/11 12:30
05/12/11 22:36
7440-66-6
Analytical Method: EPA 7470 Preparation Method: EPA 7470
ND ug/L 0.20 1 05/17/11 09:40 05/17/11 16:15 7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 43 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-24 Lab ID: 9293679013 Collected: 05/06/11 17:15 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
83-32-9
Acenaphthylene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
208-96-8
Aniline
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
62-53-3
Anthracene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
120-12-7
Benzo(a)anthracene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
56-55-3
Benzo(a)pyrene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
50-32-8
Benzo(b)fluoranthene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
205-99-2
Benzo(g,h,i)perylene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
191-24-2
Benzo(k)fluoranthene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
207-08-9
Benzoic Acid
ND ug/L
52.6
1
05/13/11 10:39
05/18/11 16:18
65-85-0
Benzyl alcohol
ND ug/L
21.1
1
05/13/11 10:39
05/18/11 16:18
100-51-6
4-Bromophenylphenyl ether
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
101-55-3
Butylbenzylphthalate
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
85-68-7
4-Chloro-3-methylphenol
ND ug/L
21.1
1
05/13/11 10:39
05/18/11 16:18
59-50-7
4-Chloroaniline
ND ug/L
21.1
1
05/13/11 10:39
05/18/11 16:18
106-47-8
bis(2-Chloroethoxy)methane
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
111-91-1
bis(2-Chloroethyl) ether
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
108-60-1
2-Chloronaphthalene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
91-58-7
2-Chlorophenol
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
7005-72-3
Chrysene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
218-01-9
Dibenz(a,h)anthracene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
53-70-3
Dibenzofuran
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
132-64-9
1,2-Dichlorobenzene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
95-50-1
1,3-Dichlorobenzene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
541-73-1
1,4-Dichlorobenzene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
106-46-7
3,3'-Dichlorobenzidine
ND ug/L
21.1
1
05/13/11 10:39
05/18/11 16:18
91-94-1
2,4-Dichlorophenol
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
120-83-2
Diethylphthalate
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
84-66-2
2,4-Dimethylphenol
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
105-67-9
Dimethylphthalate
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
131-11-3
Di-n-butylphthalate
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
84-74-2
4,6-Dinitro-2-methylphenol
ND ug/L
21.1
1
05/13/11 10:39
05/18/11 16:18
534-52-1
2,4-Dinitrophenol
ND ug/L
52.6
1
05/13/11 10:39
05/18/11 16:18
51-28-5
2,4-Dinitrotoluene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
121-14-2
2,6-Dinitrotoluene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
606-20-2
Di-n-octylphthalate
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/L
6.3
1
05/13/11 10:39
05/18/11 16:18
117-81-7
Fluoranthene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
206-44-0
Fluorene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
87-68-3
Hexachlorobenzene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
118-74-1
Hexachlorocyclopentadiene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
77-47-4
Hexachloroethane
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
193-39-5
Isophorone
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
78-59-1
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 44 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-24 Lab ID: 9293679013 Collected: 05/06/11 17:15 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
1-Methylnaphthalene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
90-12-0
2-Methylnaphthalene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
91-57-6
2-Methylphenol(o-Cresol)
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
Naphthalene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
91-20-3
2-Nitroaniline
ND ug/L
52.6
1
05/13/11 10:39
05/18/11 16:18
88-74-4
3-Nitroaniline
ND ug/L
52.6
1
05/13/11 10:39
05/18/11 16:18
99-09-2
4-Nitroaniline
ND ug/L
21.1
1
05/13/11 10:39
05/18/11 16:18
100-01-6
Nitrobenzene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
98-95-3
2-Nitrophenol
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
88-75-5
4-Nitrophenol
ND ug/L
52.6
1
05/13/11 10:39
05/18/11 16:18
100-02-7
N-Nitrosodimethylamine
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
621-64-7
N-Nitrosodiphenylamine
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
86-30-6
Pentachlorophenol
ND ug/L
26.3
1
05/13/11 10:39
05/18/11 16:18
87-86-5
Phenanthrene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
85-01-8
Phenol
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
108-95-2
Pyrene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
129-00-0
1,2,4-Trichlorobenzene
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
120-82-1
2,4,5-Trichlorophenol
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
95-95-4
2,4,6-Trichlorophenol
ND ug/L
10.5
1
05/13/11 10:39
05/18/11 16:18
88-06-2
Nitrobenzene-d5 (S)
50 %
21-110
1
05/13/11 10:39
05/18/11 16:18
4165-60-0
2-Fluorobiphenyl (S)
52 %
27-110
1
05/13/11 10:39
05/18/11 16:18
321-60-8
Terphenyl-d14 (S)
65 %
31-107
1
05/13/11 10:39
05/18/11 16:18
1718-51-0
Phenol-d6 (S)
18 %
10-110
1
05/13/11 10:39
05/18/11 16:18
13127-88-3
2-Fluorophenol (S)
33 %
12-110
1
05/13/11 10:39
05/18/11 16:18
367-12-4
2,4,6-Tribromophenol (S)
51 %
27-110
1
05/13/11 10:39
05/18/11 16:18
118-79-6
8260 MSV Low Level
Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/11/11 07:00
67-64-1
Benzene
ND ug/L
1.0
1
05/11/11 07:00
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/11/11 07:00
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/11/11 07:00
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
05/11/11 07:00
75-27-4
Bromoform
ND ug/L
1.0
1
05/11/11 07:00
75-25-2
Bromomethane
ND ug/L
2.0
1
05/11/11 07:00
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/11/11 07:00
78-93-3
Carbon tetrachloride
ND ug/L
1.0
1
05/11/11 07:00
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/11/11 07:00
108-90-7
Chloroethane
ND ug/L
1.0
1
05/11/11 07:00
75-00-3
Chloroform
ND ug/L
1.0
1
05/11/11 07:00
67-66-3
Chloromethane
ND ug/L
1.0
1
05/11/11 07:00
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/11/11 07:00
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/11/11 07:00
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
1
05/11/11 07:00
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/11/11 07:00
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/11/11 07:00
106-93-4
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY
ANALYSIS
Page 45 of 227
This report shall not be reproduced, except
in
full,
without the written consent of Pace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-24 Lab ID: 9293679013 Collected: 05/06/11 17:15 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Dibromomethane
ND ug/L
1.0
1
05/11/11 07:00
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 07:00
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 07:00
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 07:00
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/11/11 07:00
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
1
05/11/11 07:00
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/11/11 07:00
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
05/11/11 07:00
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 07:00
156-59-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 07:00
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 07:00
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/11/11 07:00
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 07:00
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/11/11 07:00
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 07:00
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 07:00
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/11/11 07:00
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/11/11 07:00
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/11/11 07:00
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/11/11 07:00
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
1
05/11/11 07:00
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/11/11 07:00
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/11/11 07:00
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/11/11 07:00
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/11/11 07:00
91-20-3
Styrene
ND ug/L
1.0
1
05/11/11 07:00
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 07:00
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 07:00
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
05/11/11 07:00
127-18-4
Toluene
ND ug/L
1.0
1
05/11/11 07:00
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 07:00
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 07:00
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/11/11 07:00
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/11/11 07:00
79-00-5
Trichloroethene
ND ug/L
1.0
1
05/11/11 07:00
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/11/11 07:00
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/11/11 07:00
96-18-4
Vinyl acetate
ND ug/L
2.0
1
05/11/11 07:00
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/11/11 07:00
75-01-4
m&p-Xylene
ND ug/L
2.0
1
05/11/11 07:00
179601-23-1
o-Xylene
ND ug/L
1.0
1
05/11/11 07:00
95-47-6
4-Bromofluorobenzene (S)
96 %
70-130
1
05/11/11 07:00
460-00-4
Dibromofluoromethane (S)
104 %
70-130
1
05/11/11 07:00
1868-53-7
1,2-Dichloroethane-d4 (S)
110 %
70-130
1
05/11/11 07:00
17060-07-0
Toluene-d8 (S)
100 %
70-130
1
05/11/11 07:00
2037-26-5
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 46 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-25 Lab ID: 9293679014 Collected: 05/06/11 17:36 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Aluminum
296 ug/L
100
1
05/12/11 12:30
05/12/11 22:40
7429-90-5
Antimony
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:40
7440-36-0
Arsenic
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:40
7440-38-2
Barium
30.6 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:40
7440-39-3
Beryllium
ND ug/L
1.0
1
05/12/11 12:30
05/12/11 22:40
7440-41-7
Cadmium
ND ug/L
1.0
1
05/12/11 12:30
05/12/11 22:40
7440-43-9
Calcium
12900 ug/L
100
1
05/12/11 12:30
05/12/11 22:40
7440-70-2
Chromium
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:40
7440-47-3
Cobalt
11.6 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:40
7440-48-4
Copper
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:40
7440-50-8
Iron
279 ug/L
50.0
1
05/12/11 12:30
05/12/11 22:40
7439-89-6
Lead
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:40
7439-92-1
Magnesium
3060 ug/L
100
1
05/12/11 12:30
05/12/11 22:40
7439-95-4
Manganese
429 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:40
7439-96-5
Nickel
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:40
7440-02-0
Potassium
ND ug/L
5000
1
05/12/11 12:30
05/13/11 13:35
7440-09-7
Selenium
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:40
7782-49-2
Silver
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:40
7440-22-4
Sodium
7660 ug/L
5000
1
05/12/11 12:30
05/13/11 13:35
7440-23-5
Thallium
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:40
7440-28-0
Vanadium
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:40
7440-62-2
Zinc
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:40
7440-66-6
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
05/17/11 09:40
05/17/11 16:17
7439-97-6
8270 MSSV Semivolatile Organic
Analytical Method: EPA 8270 Preparation Method:
EPA 3510
Acenaphthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
83-32-9
Acenaphthylene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
208-96-8
Aniline
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
62-53-3
Anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
120-12-7
Benzo(a)anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
56-55-3
Benzo(a)pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
50-32-8
Benzo(b)fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
205-99-2
Benzo(g,h,i)perylene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
191-24-2
Benzo(k)fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
207-08-9
Benzoic Acid
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 16:45
65-85-0
Benzyl alcohol
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 16:45
100-51-6
4-Bromophenylphenyl ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
101-55-3
Butylbenzylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
85-68-7
4-Chloro-3-methylphenol
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 16:45
59-50-7
4-Chloroaniline
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 16:45
106-47-8
bis(2-Chloroethoxy)methane
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
111-91-1
bis(2-Chloroethyl) ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
108-60-1
2-Chloronaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
91-58-7
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 47 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-25 Lab ID: 9293679014 Collected: 05/06/11 17:36 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
2-Chlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
7005-72-3
Chrysene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
218-01-9
Dibenz(a,h)anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
53-70-3
Dibenzofuran
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
132-64-9
1,2-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
95-50-1
1,3-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
541-73-1
1,4-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
106-46-7
3,3'-Dichlorobenzidine
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 16:45
91-94-1
2,4-Dichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
120-83-2
Diethylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
84-66-2
2,4-Dimethylphenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
105-67-9
Dimethylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
131-11-3
Di-n-butylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 16:45
534-52-1
2,4-Dinitrophenol
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 16:45
51-28-5
2,4-Dinitrotoluene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
121-14-2
2,6-Dinitrotoluene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
606-20-2
Di-n-octylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/L
6.0
1
05/13/11 10:39
05/18/11 16:45
117-81-7
Fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
206-44-0
Fluorene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
87-68-3
Hexachlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
118-74-1
Hexachlorocyclopentadiene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
77-47-4
Hexachloroethane
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
193-39-5
Isophorone
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
78-59-1
1-Methylnaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
90-12-0
2-Methylnaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
91-57-6
2-Methylphenol(o-Cresol)
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
Naphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
91-20-3
2-Nitroaniline
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 16:45
88-74-4
3-Nitroaniline
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 16:45
99-09-2
4-Nitroaniline
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 16:45
100-01-6
Nitrobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
98-95-3
2-Nitrophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
88-75-5
4-Nitrophenol
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 16:45
100-02-7
N-Nitrosodimethylamine
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
621-64-7
N-Nitrosodiphenylamine
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
86-30-6
Pentachlorophenol
ND ug/L
25.0
1
05/13/11 10:39
05/18/11 16:45
87-86-5
Phenanthrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
85-01-8
Phenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
108-95-2
Pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
129-00-0
1,2,4-Trichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
120-82-1
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 48 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-25 Lab ID: 9293679014 Collected: 05/06/11 17:36 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
2,4,5-Trichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
95-95-4
2,4,6-Trichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 16:45
88-06-2
Nitrobenzene-d5 (S)
56 %
21-110
1
05/13/11 10:39
05/18/11 16:45
4165-60-0
2-Fluorobiphenyl (S)
64 %
27-110
1
05/13/11 10:39
05/18/11 16:45
321-60-8
Terphenyl-d14 (S)
81 %
31-107
1
05/13/11 10:39
05/18/11 16:45
1718-51-0
Phenol-d6 (S)
20 %
10-110
1
05/13/11 10:39
05/18/11 16:45
13127-88-3
2-Fluorophenol (S)
36 %
12-110
1
05/13/11 10:39
05/18/11 16:45
367-12-4
2,4,6-Tribromophenol (S)
65 %
27-110
1
05/13/11 10:39
05/18/11 16:45
118-79-6
8260 MSV Low Level
Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/11/11 07:25
67-64-1
Benzene
ND ug/L
1.0
1
05/11/11 07:25
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/11/11 07:25
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/11/11 07:25
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
05/11/11 07:25
75-27-4
Bromoform
ND ug/L
1.0
1
05/11/11 07:25
75-25-2
Bromomethane
ND ug/L
2.0
1
05/11/11 07:25
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/11/11 07:25
78-93-3
Carbon tetrachloride
ND ug/L
1.0
1
05/11/11 07:25
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/11/11 07:25
108-90-7
Chloroethane
ND ug/L
1.0
1
05/11/11 07:25
75-00-3
Chloroform
ND ug/L
1.0
1
05/11/11 07:25
67-66-3
Chloromethane
ND ug/L
1.0
1
05/11/11 07:25
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/11/11 07:25
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/11/11 07:25
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
1
05/11/11 07:25
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/11/11 07:25
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/11/11 07:25
106-93-4
Dibromomethane
ND ug/L
1.0
1
05/11/11 07:25
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 07:25
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 07:25
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 07:25
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/11/11 07:25
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
1
05/11/11 07:25
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/11/11 07:25
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
05/11/11 07:25
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 07:25
156-59-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 07:25
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 07:25
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/11/11 07:25
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 07:25
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/11/11 07:25
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 07:25
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 07:25
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/11/11 07:25
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/11/11 07:25
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/11/11 07:25
87-68-3
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 49 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-25 Lab ID: 9293679014 Collected: 05/06/11 17:36 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
2-Hexanone
ND ug/L
5.0
1
05/11/11 07:25
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
1
05/11/11 07:25
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/11/11 07:25
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/11/11 07:25
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/11/11 07:25
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/11/11 07:25
91-20-3
Styrene
ND ug/L
1.0
1
05/11/11 07:25
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 07:25
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 07:25
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
05/11/11 07:25
127-18-4
Toluene
1.2 ug/L
1.0
1
05/11/11 07:25
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 07:25
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 07:25
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/11/11 07:25
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/11/11 07:25
79-00-5
Trichloroethene
ND ug/L
1.0
1
05/11/11 07:25
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/11/11 07:25
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/11/11 07:25
96-18-4
Vinyl acetate
ND ug/L
2.0
1
05/11/11 07:25
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/11/11 07:25
75-01-4
m&p-Xylene
ND ug/L
2.0
1
05/11/11 07:25
179601-23-1
o-Xylene
ND ug/L
1.0
1
05/11/11 07:25
95-47-6
4-Bromofluorobenzene (S)
96 %
70-130
1
05/11/11 07:25
460-00-4
Dibromofluoromethane (S)
103 %
70-130
1
05/11/11 07:25
1868-53-7
1,2-Dichloroethane-d4 (S)
109 %
70-130
1
05/11/11 07:25
17060-07-0
Toluene-d8 (S)
101 %
70-130
1
05/11/11 07:25
2037-26-5
Sample: DUP-2 Lab ID: 9293679015 Collected: 05/06/11 17:20 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Aluminum
73100 ug/L
100
1
05/12/11 12:30
05/12/11 22:43
7429-90-5
Antimony
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:43
7440-36-0
Arsenic
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:43
7440-38-2
Barium
707 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:43
7440-39-3
Beryllium
4.8 ug/L
1.0
1
05/12/11 12:30
05/12/11 22:43
7440-41-7
Cadmium
ND ug/L
1.0
1
05/12/11 12:30
05/12/11 22:43
7440-43-9
Calcium
3540 ug/L
100
1
05/12/11 12:30
05/12/11 22:43
7440-70-2
Chromium
74.1 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:43
7440-47-3
Cobalt
44.0 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:43
7440-48-4
Copper
64.5 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:43
7440-50-8
Iron
96500 ug/L
50.0
1
05/12/11 12:30
05/12/11 22:43
7439-89-6
Lead
40.3 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:43
7439-92-1
Magnesium
8870 ug/L
100
1
05/12/11 12:30
05/12/11 22:43
7439-95-4
Manganese
1810 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:43
7439-96-5
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY
ANALYSIS
Page 50 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: DUP-2 Lab ID: 9293679015 Collected: 05/06/11 17:20 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Nickel
52.2 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:43
7440-02-0
Potassium
11000 ug/L
5000
1
05/12/11 12:30
05/13/11 13:39
7440-09-7
Selenium
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:43
7782-49-2
Silver
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:43
7440-22-4
Sodium
6270 ug/L
5000
1
05/12/11 12:30
05/13/11 13:39
7440-23-5
Thallium
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:43
7440-28-0
Vanadium
152 ug/L
5.0
1
05/12/11 12:30
05/12/11 22:43
7440-62-2
Zinc
157 ug/L
10.0
1
05/12/11 12:30
05/12/11 22:43
7440-66-6
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
05/17/11 09:40
05/17/11 16:20
7439-97-6
8270 MSSV Semivolatile Organic
Analytical Method: EPA 8270 Preparation Method:
EPA 3510
Acenaphthene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
83-32-9
Acenaphthylene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
208-96-8
Aniline
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
62-53-3
Anthracene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
120-12-7
Benzo(a)anthracene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
56-55-3
Benzo(a)pyrene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
50-32-8
Benzo(b)fluoranthene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
205-99-2
Benzo(g,h,i)perylene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
191-24-2
Benzo(k)fluoranthene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
207-08-9
Benzoic Acid
ND ug/L
58.1
1
05/13/11 10:39
05/18/11 17:12
65-85-0
Benzyl alcohol
ND ug/L
23.3
1
05/13/11 10:39
05/18/11 17:12
100-51-6
4-Bromophenylphenyl ether
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
101-55-3
Butylbenzylphthalate
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
85-68-7
4-Chloro-3-methylphenol
ND ug/L
23.3
1
05/13/11 10:39
05/18/11 17:12
59-50-7
4-Chloroaniline
ND ug/L
23.3
1
05/13/11 10:39
05/18/11 17:12
106-47-8
bis(2-Chloroethoxy)methane
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
111-91-1
bis(2-Chloroethyl) ether
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
108-60-1
2-Chloronaphthalene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
91-58-7
2-Chlorophenol
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
7005-72-3
Chrysene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
218-01-9
Dibenz(a,h)anthracene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
53-70-3
Dibenzofuran
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
132-64-9
1,2-Dichlorobenzene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
95-50-1
1,3-Dichlorobenzene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
541-73-1
1,4-Dichlorobenzene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
106-46-7
3,3'-Dichlorobenzidine
ND ug/L
23.3
1
05/13/11 10:39
05/18/11 17:12
91-94-1
2,4-Dichlorophenol
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
120-83-2
Diethylphthalate
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
84-66-2
2,4-Dimethylphenol
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
105-67-9
Dimethylphthalate
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
131-11-3
Di-n-butylphthalate
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
84-74-2
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 51 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: DUP-2 Lab ID: 9293679015 Collected: 05/06/11 17:20 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
4,6-Dinitro-2-methyl phenol
ND ug/L
23.3
1
05/13/11 10:39
05/18/11 17:12
534-52-1
2,4-Dinitrophenol
ND ug/L
58.1
1
05/13/11 10:39
05/18/11 17:12
51-28-5
2,4-Dinitrotoluene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
121-14-2
2,6-Dinitrotoluene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
606-20-2
Di-n-octylphthalate
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/L
7.0
1
05/13/11 10:39
05/18/11 17:12
117-81-7
Fluoranthene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
206-44-0
Fluorene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
87-68-3
Hexachlorobenzene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
118-74-1
Hexachlorocyclopentadiene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
77-47-4
Hexachloroethane
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
193-39-5
Isophorone
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
78-59-1
1-Methylnaphthalene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
90-12-0
2-Methylnaphthalene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
91-57-6
2-Methylphenol(o-Cresol)
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
Naphthalene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
91-20-3
2-Nitroaniline
ND ug/L
58.1
1
05/13/11 10:39
05/18/11 17:12
88-74-4
3-Nitroaniline
ND ug/L
58.1
1
05/13/11 10:39
05/18/11 17:12
99-09-2
4-Nitroaniline
ND ug/L
23.3
1
05/13/11 10:39
05/18/11 17:12
100-01-6
Nitrobenzene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
98-95-3
2-Nitrophenol
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
88-75-5
4-Nitrophenol
ND ug/L
58.1
1
05/13/11 10:39
05/18/11 17:12
100-02-7
N-Nitrosodimethylamine
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
621-64-7
N-Nitrosodiphenylamine
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
86-30-6
Pentachlorophenol
ND ug/L
29.1
1
05/13/11 10:39
05/18/11 17:12
87-86-5
Phenanthrene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
85-01-8
Phenol
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
108-95-2
Pyrene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
129-00-0
1,2,4-Trichlorobenzene
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
120-82-1
2,4,5-Trichlorophenol
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
95-95-4
2,4,6-Trichlorophenol
ND ug/L
11.6
1
05/13/11 10:39
05/18/11 17:12
88-06-2
Nitrobenzene-d5 (S)
38 %
21-110
1
05/13/11 10:39
05/18/11 17:12
4165-60-0
2-Fluorobiphenyl (S)
43 %
27-110
1
05/13/11 10:39
05/18/11 17:12
321-60-8
Terphenyl-d14 (S)
59 %
31-107
1
05/13/11 10:39
05/18/11 17:12
1718-51-0
Phenol-d6 (S)
15 %
10-110
1
05/13/11 10:39
05/18/11 17:12
13127-88-3
2-Fluorophenol (S)
26 %
12-110
1
05/13/11 10:39
05/18/11 17:12
367-12-4
2,4,6-Tribromophenol (S)
39 %
27-110
1
05/13/11 10:39
05/18/11 17:12
118-79-6
8260 MSV Low Level
Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/11/11 07:49
67-64-1
Benzene
ND ug/L
1.0
1
05/11/11 07:49
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/11/11 07:49
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/11/11 07:49
74-97-5
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 52 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: DUP-2 Lab ID: 9293679015 Collected: 05/06/11 17:20 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Bromodichloromethane
ND ug/L
1.0
1
05/11/11 07:49
75-27-4
Bromoform
ND ug/L
1.0
1
05/11/11 07:49
75-25-2
Bromomethane
ND ug/L
2.0
1
05/11/11 07:49
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/11/11 07:49
78-93-3
Carbon tetrachloride
ND ug/L
1.0
1
05/11/11 07:49
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/11/11 07:49
108-90-7
Chloroethane
ND ug/L
1.0
1
05/11/11 07:49
75-00-3
Chloroform
ND ug/L
1.0
1
05/11/11 07:49
67-66-3
Chloromethane
ND ug/L
1.0
1
05/11/11 07:49
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/11/11 07:49
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/11/11 07:49
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
1
05/11/11 07:49
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/11/11 07:49
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/11/11 07:49
106-93-4
Dibromomethane
ND ug/L
1.0
1
05/11/11 07:49
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 07:49
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 07:49
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 07:49
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/11/11 07:49
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
1
05/11/11 07:49
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/11/11 07:49
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
05/11/11 07:49
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 07:49
156-59-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 07:49
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 07:49
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/11/11 07:49
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 07:49
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/11/11 07:49
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 07:49
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 07:49
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/11/11 07:49
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/11/11 07:49
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/11/11 07:49
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/11/11 07:49
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
1
05/11/11 07:49
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/11/11 07:49
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/11/11 07:49
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/11/11 07:49
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/11/11 07:49
91-20-3
Styrene
ND ug/L
1.0
1
05/11/11 07:49
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 07:49
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 07:49
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
05/11/11 07:49
127-18-4
Toluene
ND ug/L
1.0
1
05/11/11 07:49
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 07:49
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 07:49
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/11/11 07:49
71-55-6
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 53 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: DUP-2 Lab ID: 9293679015 Collected: 05/06/11 17:20 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
4-Bromofluorobenzene (S)
Dibromocuoromethane (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Analytical Method: EPA 8260
ND ug/L
1.0
1
05/11/11 07:49
79-00-5
ND ug/L
1.0
1
05/11/11 07:49
79-01-6
ND ug/L
1.0
1
05/11/11 07:49
75-69-4
ND ug/L
1.0
1
05/11/11 07:49
96-18-4
ND ug/L
2.0
1
05/11/11 07:49
108-05-4
ND ug/L
1.0
1
05/11/11 07:49
75-01-4
ND ug/L
2.0
1
05/11/11 07:49
179601-23-1
ND ug/L
1.0
1
05/11/11 07:49
95-47-6
95 %
70-130
1
05/11/11 07:49
460-00-4
104 %
70-130
1
05/11/11 07:49
1868-53-7
112 %
70-130
1
05/11/11 07:49
17060-07-0
101 %
70-130
1
05/11/11 07:49
2037-26-5
Sample: Field Blank Lab ID: 9293679016 Collected: 05/06/11 11:30 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-ch loropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dich loroethene
Date: 05/20/2011 04:57 PM
Analytical Method: EPA 8260
ND ug/L
25.0
1
05/11/11 01:45
67-64-1
ND ug/L
1.0
1
05/11/11 01:45
71-43-2
ND ug/L
1.0
1
05/11/11 01:45
108-86-1
ND ug/L
1.0
1
05/11/11 01:45
74-97-5
ND ug/L
1.0
1
05/11/11 01:45
75-27-4
ND ug/L
1.0
1
05/11/11 01:45
75-25-2
ND ug/L
2.0
1
05/11/11 01:45
74-83-9
ND ug/L
5.0
1
05/11/11 01:45
78-93-3
ND ug/L
1.0
1
05/11/11 01:45
56-23-5
ND ug/L
1.0
1
05/11/11 01:45
108-90-7
ND ug/L
1.0
1
05/11/11 01:45
75-00-3
1.9 ug/L
1.0
1
05/11/11 01:45
67-66-3
ND ug/L
1.0
1
05/11/11 01:45
74-87-3
ND ug/L
1.0
1
05/11/11 01:45
95-49-8
ND ug/L
1.0
1
05/11/11 01:45
106-43-4
ND ug/L
5.0
1
05/11/11 01:45
96-12-8
ND ug/L
1.0
1
05/11/11 01:45
124-48-1
ND ug/L
1.0
1
05/11/11 01:45
106-93-4
ND ug/L
1.0
1
05/11/11 01:45
74-95-3
ND ug/L
1.0
1
05/11/11 01:45
95-50-1
ND ug/L
1.0
1
05/11/11 01:45
541-73-1
ND ug/L
1.0
1
05/11/11 01:45
106-46-7
ND ug/L
1.0
1
05/11/11 01:45
75-71-8
ND ug/L
1.0
1
05/11/11 01:45
75-34-3
ND ug/L
1.0
1
05/11/11 01:45
107-06-2
ND ug/L
1.0
1
05/11/11 01:45
75-35-4
ND ug/L
1.0
1
05/11/11 01:45
156-59-2
ND ug/L
1.0
1
05/11/11 01:45
156-60-5
REPORT
OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
without the written
consent of Analytical Services, Inc..
PPace
CO
Page 54 of 227

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: Field Blank Lab ID: 9293679016 Collected: 05/06/11 11:30 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
1,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 01:45
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/11/11 01:45
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 01:45
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/11/11 01:45
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 01:45
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 01:45
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/11/11 01:45
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/11/11 01:45
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/11/11 01:45
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/11/11 01:45
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
1
05/11/11 01:45
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/11/11 01:45
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/11/11 01:45
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/11/11 01:45
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/11/11 01:45
91-20-3
Styrene
ND ug/L
1.0
1
05/11/11 01:45
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 01:45
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 01:45
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
05/11/11 01:45
127-18-4
Toluene
ND ug/L
1.0
1
05/11/11 01:45
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 01:45
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 01:45
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/11/11 01:45
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/11/11 01:45
79-00-5
Trichloroethene
ND ug/L
1.0
1
05/11/11 01:45
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/11/11 01:45
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/11/11 01:45
96-18-4
Vinyl acetate
ND ug/L
2.0
1
05/11/11 01:45
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/11/11 01:45
75-01-4
m&p-Xylene
ND ug/L
2.0
1
05/11/11 01:45
179601-23-1
o-Xylene
ND ug/L
1.0
1
05/11/11 01:45
95-47-6
4-Bromofluorobenzene (S)
96 %
70-130
1
05/11/11 01:45
460-00-4
Dibromofluoromethane (S)
102 %
70-130
1
05/11/11 01:45
1868-53-7
1,2-Dichloroethane-d4 (S)
107 %
70-130
1
05/11/11 01:45
17060-07-0
Toluene-d8 (S)
100 %
70-130
1
05/11/11 01:45
2037-26-5
Sample: MW-16
Lab ID: 9293679017
Collected: 05/05/11 08:40
Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
18000 mg/kg
169
20
05/11/11 14:30
05/13/11 14:33
7429-90-5
Antimony
ND mg/kg
0.42
1
05/11/11 14:30
05/12/11 15:47
7440-36-0
Arsenic
ND mg/kg
0.42
1
05/11/11 14:30
05/12/11 15:47
7440-38-2
Barium
95.1 mg/kg
0.42
1
05/11/11 14:30
05/12/11 15:47
7440-39-3
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 55 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-16 Lab ID: 9293679017 Collected: 05/05/11 08:40 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Beryllium
1.5 mg/kg
0.084
1
05/11/11 14:30
05/12/11 15:47
7440-41-7
Cadmium
3.3 mg/kg
0.084
1
05/11/11 14:30
05/12/11 15:47
7440-43-9
Calcium
183 mg/kg
8.4
1
05/11/11 14:30
05/12/11 15:47
7440-70-2
Chromium
20.4 mg/kg
0.42
1
05/11/11 14:30
05/12/11 15:47
7440-47-3
Cobalt
0.75 mg/kg
0.42
1
05/11/11 14:30
05/12/11 15:47
7440-48-4
Copper
16.9 mg/kg
0.42
1
05/11/11 14:30
05/12/11 15:47
7440-50-8
Iron
33700 mg/kg
84.5
20
05/11/11 14:30
05/13/11 14:33
7439-89-6
Lead
6.8 mg/kg
0.42
1
05/11/11 14:30
05/12/11 15:47
7439-92-1
Magnesium
1920 mg/kg
8.4
1
05/11/11 14:30
05/12/11 15:47
7439-95-4
Manganese
111 mg/kg
0.42
1
05/11/11 14:30
05/12/11 15:47
7439-96-5
Nickel
8.2 mg/kg
0.42
1
05/11/11 14:30
05/12/11 15:47
7440-02-0
Potassium
2830 mg/kg
422
1
05/11/11 14:30
05/12/11 15:47
7440-09-7
Selenium
ND mg/kg
0.84
1
05/11/11 14:30
05/12/11 15:47
7782-49-2
Silver
ND mg/kg
0.42
1
05/11/11 14:30
05/12/11 15:47
7440-22-4
Sodium
ND mg/kg
422
1
05/11/11 14:30
05/12/11 15:47
7440-23-5
Thallium
ND mg/kg
0.84
1
05/11/11 14:30
05/12/11 15:47
7440-28-0
Vanadium
35.9 mg/kg
0.42
1
05/11/11 14:30
05/12/11 15:47
7440-62-2
Zinc
52.0 mg/kg
0.84
1
05/11/11 14:30
05/12/11 15:47
7440-66-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.014 mg/kg
0.0039
1
05/13/11 08:45
05/13/11 15:41
7439-97-6
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
83-32-9
Acenaphthylene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
208-96-8
Aniline
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
62-53-3
Anthracene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
120-12-7
Benzo(a)anthracene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
56-55-3
Benzo(a)pyrene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
50-32-8
Benzo(b)fluoranthene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
191-24-2
Benzo(k)fluoranthene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
207-08-9
Benzoic Acid
ND ug/kg
1900
1
05/11/11 10:15
05/12/11 22:46
65-85-0
Benzyl alcohol
ND ug/kg
761
1
05/11/11 10:15
05/12/11 22:46
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
101-55-3
Butylbenzylphthalate
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
85-68-7
4-Chloro-3-methylphenol
ND ug/kg
761
1
05/11/11 10:15
05/12/11 22:46
59-50-7
4-Chloroaniline
ND ug/kg
1900
1
05/11/11 10:15
05/12/11 22:46
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
108-60-1
2-Chloronaphthalene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
91-58-7
2-Chlorophenol
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
7005-72-3
Chrysene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
218-01-9
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 56 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-16 Lab ID: 9293679017 Collected: 05/05/11 08:40 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
53-70-3
Dibenzofuran
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
132-64-9
1,2-Dichlorobenzene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
95-50-1
1,3-Dichlorobenzene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
541-73-1
1,4-Dichlorobenzene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
1900
1
05/11/11 10:15
05/12/11 22:46
91-94-1
2,4-Dichlorophenol
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
120-83-2
Diethylphthalate
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
84-66-2
2,4-Dimethylphenol
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
105-67-9
Dimethylphthalate
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
131-11-3
Di-n-butylphthalate
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/kg
761
1
05/11/11 10:15
05/12/11 22:46
534-52-1
2,4-Dinitrophenol
ND ug/kg
1900
1
05/11/11 10:15
05/12/11 22:46
51-28-5
2,4-Dinitrotoluene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
121-14-2
2,6-Dinitrotoluene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
606-20-2
Di-n-octylphthalate
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
117-81-7
Fluoranthene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
206-44-0
Fluorene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
87-68-3
Hexachlorobenzene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
77-47-4
Hexachloroethane
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
193-39-5
Isophorone
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
78-59-1
1-Methylnaphthalene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
90-12-0
2-Methylnaphthalene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
Naphthalene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
91-20-3
2-Nitroaniline
ND ug/kg
1900
1
05/11/11 10:15
05/12/11 22:46
88-74-4
3-Nitroaniline
ND ug/kg
1900
1
05/11/11 10:15
05/12/11 22:46
99-09-2
4-Nitroaniline
ND ug/kg
761
1
05/11/11 10:15
05/12/11 22:46
100-01-6
Nitrobenzene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
98-95-3
2-Nitrophenol
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
88-75-5
4-Nitrophenol
ND ug/kg
1900
1
05/11/11 10:15
05/12/11 22:46
100-02-7
N-Nitrosodimethylamine
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
86-30-6
Pentachlorophenol
ND ug/kg
1900
1
05/11/11 10:15
05/12/11 22:46
87-86-5
Phenanthrene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
85-01-8
Phenol
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
108-95-2
Pyrene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
380
1
05/11/11 10:15
05/12/11 22:46
88-06-2
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY
ANALYSIS
This report
shall not be reproduced, except
in
full,
without the written consent of Analytical Services, Inc..
PPace
Page 57 of 227

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-16 Lab ID: 9293679017 Collected: 05/05/11 08:40 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)
58 %
23-110
1
05/11/11 10:15
05/12/11 22:46
4165-60-0
2-Fluorobiphenyl (S)
59 %
30-110
1
05/11/11 10:15
05/12/11 22:46
321-60-8
Terphenyl-d14 (S)
62 %
28-110
1
05/11/11 10:15
05/12/11 22:46
1718-51-0
Phenol-d6 (S)
50 %
22-110
1
05/11/11 10:15
05/12/11 22:46
13127-88-3
2-Fluorophenol (S)
48 %
13-110
1
05/11/11 10:15
05/12/11 22:46
367-12-4
2,4,6-Tribromophenol (S)
49 %
27-110
1
05/11/11 10:15
05/12/11 22:46
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND ug/kg
62.7
1
05/10/11 21:09
67-64-1
Benzene
ND ug/kg
3.1
1
05/10/11 21:09
71-43-2
Bromobenzene
ND ug/kg
3.1
1
05/10/11 21:09
108-86-1
Bromochloromethane
ND ug/kg
3.1
1
05/10/11 21:09
74-97-5
Bromodichloromethane
ND ug/kg
3.1
1
05/10/11 21:09
75-27-4
Bromoform
ND ug/kg
3.1
1
05/10/11 21:09
75-25-2
Bromomethane
ND ug/kg
6.3
1
05/10/11 21:09
74-83-9
2-Butanone (MEK)
ND ug/kg
62.7
1
05/10/11 21:09
78-93-3
n-Butylbenzene
ND ug/kg
3.1
1
05/10/11 21:09
104-51-8
sec -Butyl benzene
ND ug/kg
3.1
1
05/10/11 21:09
135-98-8
tert-Butyl benzene
ND ug/kg
3.1
1
05/10/11 21:09
98-06-6
Carbon tetrachloride
ND ug/kg
3.1
1
05/10/11 21:09
56-23-5
Chlorobenzene
ND ug/kg
3.1
1
05/10/11 21:09
108-90-7
Chloroethane
ND ug/kg
6.3
1
05/10/11 21:09
75-00-3
Chloroform
ND ug/kg
3.1
1
05/10/11 21:09
67-66-3
Chloromethane
ND ug/kg
6.3
1
05/10/11 21:09
74-87-3
2-Chlorotoluene
ND ug/kg
3.1
1
05/10/11 21:09
95-49-8
4-Chlorotoluene
ND ug/kg
3.1
1
05/10/11 21:09
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
3.1
1
05/10/11 21:09
96-12-8
Dibromochloromethane
ND ug/kg
3.1
1
05/10/11 21:09
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
3.1
1
05/10/11 21:09
106-93-4
Dibromomethane
ND ug/kg
3.1
1
05/10/11 21:09
74-95-3
1,2-Dichlorobenzene
ND ug/kg
3.1
1
05/10/11 21:09
95-50-1
1,3-Dichlorobenzene
ND ug/kg
3.1
1
05/10/11 21:09
541-73-1
1,4-Dichlorobenzene
ND ug/kg
3.1
1
05/10/11 21:09
106-46-7
Dichlorodifluoromethane
ND ug/kg
6.3
1
05/10/11 21:09
75-71-8
1,1-Dichloroethane
ND ug/kg
3.1
1
05/10/11 21:09
75-34-3
1,2-Dichloroethane
ND ug/kg
3.1
1
05/10/11 21:09
107-06-2
1,1-Dichloroethene
ND ug/kg
3.1
1
05/10/11 21:09
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
3.1
1
05/10/11 21:09
156-59-2
trans- 1,2-Dichloroethene
ND ug/kg
3.1
1
05/10/11 21:09
156-60-5
1,2-Dichloropropane
ND ug/kg
3.1
1
05/10/11 21:09
78-87-5
1,3-Dichloropropane
ND ug/kg
3.1
1
05/10/11 21:09
142-28-9
2,2-Dichloropropane
ND ug/kg
3.1
1
05/10/11 21:09
594-20-7
1,1-Dichloropropene
ND ug/kg
3.1
1
05/10/11 21:09
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
3.1
1
05/10/11 21:09
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
3.1
1
05/10/11 21:09
10061-02-6
Diisopropyl ether
ND ug/kg
3.1
1
05/10/11 21:09
108-20-3
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 58 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-16 Lab ID: 9293679017 Collected: 05/05/11 08:40 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene
ND ug/kg
3.1
1
05/10/11 21:09
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
3.1
1
05/10/11 21:09
87-68-3
2-Hexanone
ND ug/kg
31.4
1
05/10/11 21:09
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
3.1
1
05/10/11 21:09
98-82-8
p-Isopropyltoluene
ND ug/kg
3.1
1
05/10/11 21:09
99-87-6
Methylene Chloride
ND ug/kg
12.5
1
05/10/11 21:09
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
31.4
1
05/10/11 21:09
108-10-1
Methyl-tert-butyl ether
ND ug/kg
3.1
1
05/10/11 21:09
1634-04-4
Naphthalene
ND ug/kg
3.1
1
05/10/11 21:09
91-20-3
n-Propylbenzene
ND ug/kg
3.1
1
05/10/11 21:09
103-65-1
Styrene
ND ug/kg
3.1
1
05/10/11 21:09
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
3.1
1
05/10/11 21:09
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
3.1
1
05/10/11 21:09
79-34-5
Tetrachloroethene
ND ug/kg
3.1
1
05/10/11 21:09
127-18-4
Toluene
ND ug/kg
3.1
1
05/10/11 21:09
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
3.1
1
05/10/11 21:09
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
3.1
1
05/10/11 21:09
120-82-1
1,1,1-Trichloroethane
ND ug/kg
3.1
1
05/10/11 21:09
71-55-6
1,1,2-Trichloroethane
ND ug/kg
3.1
1
05/10/11 21:09
79-00-5
Trichloroethene
ND ug/kg
3.1
1
05/10/11 21:09
79-01-6
Trichlorofluoromethane
ND ug/kg
3.1
1
05/10/11 21:09
75-69-4
1,2,3-Trichloropropane
ND ug/kg
3.1
1
05/10/11 21:09
96-18-4
1,2,4-Trimethylbenzene
ND ug/kg
3.1
1
05/10/11 21:09
95-63-6
1,3,5-Trimethylbenzene
ND ug/kg
3.1
1
05/10/11 21:09
108-67-8
Vinyl acetate
ND ug/kg
31.4
1
05/10/11 21:09
108-05-4
Vinyl chloride
ND ug/kg
6.3
1
05/10/11 21:09
75-01-4
Xylene (Total)
ND ug/kg
6.3
1
05/10/11 21:09
1330-20-7
m&p-Xylene
ND ug/kg
6.3
1
05/10/11 21:09
179601-23-1
o-Xylene
ND ug/kg
3.1
1
05/10/11 21:09
95-47-6
Dibromofluoromethane (S)
102 %
70-130
1
05/10/11 21:09
1868-53-7
Toluene-d8 (S)
102 %
70-130
1
05/10/11 21:09
2037-26-5
4-Bromofluorobenzene (S)
98 %
70-130
1
05/10/11 21:09
460-00-4
1,2-Dichloroethane-d4 (S)
92 %
70-132
1
05/10/11 21:09
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
13.0 %
0.10
1
05/11/11 08:51
Sample: MW-17
Lab ID: 9293679018
Collected: 05/05/11 08:45
Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters
Results Units
Report Limit DF
Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
23500 mg/kg
197 20
05/11/11 14:30 05/13/11 14:36 7429-90-5
Antimony
ND mg/kg
0.49 1
05/11/11 14:30 05/12/11 15:51 7440-36-0
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 59 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-17 Lab ID: 9293679018 Collected: 05/05/11 08:45 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
ND mg/kg
0.49
1
05/11/11 14:30
05/12/11 15:51
7440-38-2
Barium
147 mg/kg
0.49
1
05/11/11 14:30
05/12/11 15:51
7440-39-3
Beryllium
1.3 mg/kg
0.098
1
05/11/11 14:30
05/12/11 15:51
7440-41-7
Cadmium
6.4 mg/kg
0.098
1
05/11/11 14:30
05/12/11 15:51
7440-43-9
Calcium
238 mg/kg
9.8
1
05/11/11 14:30
05/12/11 15:51
7440-70-2
Chromium
32.2 mg/kg
0.49
1
05/11/11 14:30
05/12/11 15:51
7440-47-3
Cobalt
0.70 mg/kg
0.49
1
05/11/11 14:30
05/12/11 15:51
7440-48-4
Copper
27.0 mg/kg
0.49
1
05/11/11 14:30
05/12/11 15:51
7440-50-8
Iron
55700 mg/kg
98.3
20
05/11/11 14:30
05/13/11 14:36
7439-89-6
Lead
13.3 mg/kg
0.49
1
05/11/11 14:30
05/12/11 15:51
7439-92-1
Magnesium
4020 mg/kg
9.8
1
05/11/11 14:30
05/12/11 15:51
7439-95-4
Manganese
114 mg/kg
0.49
1
05/11/11 14:30
05/12/11 15:51
7439-96-5
Nickel
12.5 mg/kg
0.49
1
05/11/11 14:30
05/12/11 15:51
7440-02-0
Potassium
7160 mg/kg
491
1
05/11/11 14:30
05/12/11 15:51
7440-09-7
Selenium
1.9 mg/kg
0.98
1
05/11/11 14:30
05/12/11 15:51
7782-49-2
Silver
ND mg/kg
0.49
1
05/11/11 14:30
05/12/11 15:51
7440-22-4
Sodium
ND mg/kg
491
1
05/11/11 14:30
05/12/11 15:51
7440-23-5
Thallium
ND mg/kg
0.98
1
05/11/11 14:30
05/12/11 15:51
7440-28-0
Vanadium
42.2 mg/kg
0.49
1
05/11/11 14:30
05/12/11 15:51
7440-62-2
Zinc
77.4 mg/kg
0.98
1
05/11/11 14:30
05/12/11 15:51
7440-66-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.030 mg/kg
0.0052
1
05/13/11 08:45
05/13/11 15:46
7439-97-6
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
83-32-9
Acenaphthylene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
208-96-8
Aniline
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
62-53-3
Anthracene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
120-12-7
Benzo(a)anthracene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
56-55-3
Benzo(a)pyrene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
50-32-8
Benzo(b)fluoranthene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
191-24-2
Benzo(k)fluoranthene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
207-08-9
Benzoic Acid
ND ug/kg
2160
1
05/11/11 10:15
05/12/11 23:14
65-85-0
Benzyl alcohol
ND ug/kg
863
1
05/11/11 10:15
05/12/11 23:14
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
101-55-3
Butylbenzylphthalate
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
85-68-7
4-Chloro-3-methylphenol
ND ug/kg
863
1
05/11/11 10:15
05/12/11 23:14
59-50-7
4-Chloroaniline
ND ug/kg
2160
1
05/11/11 10:15
05/12/11 23:14
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
108-60-1
2-Chloronaphthalene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
91-58-7
2-Chlorophenol
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
95-57-8
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 60 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-17 Lab ID: 9293679018 Collected: 05/05/11 08:45 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
4-Chlorophenylphenyl ether
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
7005-72-3
Chrysene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
53-70-3
Dibenzofuran
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
132-64-9
1,2-Dichlorobenzene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
95-50-1
1,3-Dichlorobenzene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
541-73-1
1,4-Dichlorobenzene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
2160
1
05/11/11 10:15
05/12/11 23:14
91-94-1
2,4-Dichlorophenol
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
120-83-2
Diethylphthalate
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
84-66-2
2,4-Dimethylphenol
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
105-67-9
Dimethylphthalate
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
131-11-3
Di-n-butylphthalate
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/kg
863
1
05/11/11 10:15
05/12/11 23:14
534-52-1
2,4-Dinitrophenol
ND ug/kg
2160
1
05/11/11 10:15
05/12/11 23:14
51-28-5
2,4-Dinitrotoluene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
121-14-2
2,6-Dinitrotoluene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
606-20-2
Di-n-octylphthalate
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
117-81-7
Fluoranthene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
206-44-0
Fluorene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
87-68-3
Hexachlorobenzene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
77-47-4
Hexachloroethane
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
193-39-5
Isophorone
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
78-59-1
1-Methylnaphthalene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
90-12-0
2-Methylnaphthalene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
Naphthalene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
91-20-3
2-Nitroaniline
ND ug/kg
2160
1
05/11/11 10:15
05/12/11 23:14
88-74-4
3-Nitroaniline
ND ug/kg
2160
1
05/11/11 10:15
05/12/11 23:14
99-09-2
4-Nitroaniline
ND ug/kg
863
1
05/11/11 10:15
05/12/11 23:14
100-01-6
Nitrobenzene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
98-95-3
2-Nitrophenol
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
88-75-5
4-Nitrophenol
ND ug/kg
2160
1
05/11/11 10:15
05/12/11 23:14
100-02-7
N-Nitrosodimethylamine
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
86-30-6
Pentachlorophenol
ND ug/kg
2160
1
05/11/11 10:15
05/12/11 23:14
87-86-5
Phenanthrene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
85-01-8
Phenol
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
108-95-2
Pyrene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
120-82-1
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 61 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-17 Lab ID: 9293679018 Collected: 05/05/11 08:45 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4,5-Trichlorophenol
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
432
1
05/11/11 10:15
05/12/11 23:14
88-06-2
Nitrobenzene-d5 (S)
37 %
23-110
1
05/11/11 10:15
05/12/11 23:14
4165-60-0
2-Fluorobiphenyl (S)
38 %
30-110
1
05/11/11 10:15
05/12/11 23:14
321-60-8
Terphenyl-d14 (S)
59 %
28-110
1
05/11/11 10:15
05/12/11 23:14
1718-51-0
Phenol-d6 (S)
30 %
22-110
1
05/11/11 10:15
05/12/11 23:14
13127-88-3
2-Fluorophenol (S)
32 %
13-110
1
05/11/11 10:15
05/12/11 23:14
367-12-4
2,4,6-Tribromophenol (S)
45 %
27-110
1
05/11/11 10:15
05/12/11 23:14
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND ug/kg
74.0
1
05/10/11 21:29
67-64-1
Benzene
ND ug/kg
3.7
1
05/10/11 21:29
71-43-2
Bromobenzene
ND ug/kg
3.7
1
05/10/11 21:29
108-86-1
Bromochloromethane
ND ug/kg
3.7
1
05/10/11 21:29
74-97-5
Bromodichloromethane
ND ug/kg
3.7
1
05/10/11 21:29
75-27-4
Bromoform
ND ug/kg
3.7
1
05/10/11 21:29
75-25-2
Bromomethane
ND ug/kg
7.4
1
05/10/11 21:29
74-83-9
2-Butanone (MEK)
ND ug/kg
74.0
1
05/10/11 21:29
78-93-3
n-Butylbenzene
ND ug/kg
3.7
1
05/10/11 21:29
104-51-8
sec -Butyl benzene
ND ug/kg
3.7
1
05/10/11 21:29
135-98-8
tert-Butyl benzene
ND ug/kg
3.7
1
05/10/11 21:29
98-06-6
Carbon tetrachloride
ND ug/kg
3.7
1
05/10/11 21:29
56-23-5
Chlorobenzene
ND ug/kg
3.7
1
05/10/11 21:29
108-90-7
Chloroethane
ND ug/kg
7.4
1
05/10/11 21:29
75-00-3
Chloroform
ND ug/kg
3.7
1
05/10/11 21:29
67-66-3
Chloromethane
ND ug/kg
7.4
1
05/10/11 21:29
74-87-3
2-Chlorotoluene
ND ug/kg
3.7
1
05/10/11 21:29
95-49-8
4-Chlorotoluene
ND ug/kg
3.7
1
05/10/11 21:29
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
3.7
1
05/10/11 21:29
96-12-8
Dibromochloromethane
ND ug/kg
3.7
1
05/10/11 21:29
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
3.7
1
05/10/11 21:29
106-93-4
Dibromomethane
ND ug/kg
3.7
1
05/10/11 21:29
74-95-3
1,2-Dichlorobenzene
ND ug/kg
3.7
1
05/10/11 21:29
95-50-1
1,3-Dichlorobenzene
ND ug/kg
3.7
1
05/10/11 21:29
541-73-1
1,4-Dichlorobenzene
ND ug/kg
3.7
1
05/10/11 21:29
106-46-7
Dichlorodifluoromethane
ND ug/kg
7.4
1
05/10/11 21:29
75-71-8
1,1-Dichloroethane
ND ug/kg
3.7
1
05/10/11 21:29
75-34-3
1,2-Dichloroethane
ND ug/kg
3.7
1
05/10/11 21:29
107-06-2
1,1-Dichloroethene
ND ug/kg
3.7
1
05/10/11 21:29
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
3.7
1
05/10/11 21:29
156-59-2
trans- 1,2-Dichloroethene
ND ug/kg
3.7
1
05/10/11 21:29
156-60-5
1,2-Dichloropropane
ND ug/kg
3.7
1
05/10/11 21:29
78-87-5
1,3-Dichloropropane
ND ug/kg
3.7
1
05/10/11 21:29
142-28-9
2,2-Dichloropropane
ND ug/kg
3.7
1
05/10/11 21:29
594-20-7
1,1-Dichloropropene
ND ug/kg
3.7
1
05/10/11 21:29
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
3.7
1
05/10/11 21:29
10061-01-5
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 62 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-17 Lab ID: 9293679018 Collected: 05/05/11 08:45 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1, 2-Tetrach loroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1, 3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Dibromofluoromethane (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 05/20/2011 04:57 PM
ND ug/kg
3.7
1
05/10/11 21:29
10061-02-6
ND ug/kg
3.7
1
05/10/11 21:29
108-20-3
ND ug/kg
3.7
1
05/10/11 21:29
100-41-4
ND ug/kg
3.7
1
05/10/11 21:29
87-68-3
ND ug/kg
37.0
1
05/10/11 21:29
591-78-6
ND ug/kg
3.7
1
05/10/11 21:29
98-82-8
ND ug/kg
3.7
1
05/10/11 21:29
99-87-6
ND ug/kg
14.8
1
05/10/11 21:29
75-09-2
ND ug/kg
37.0
1
05/10/11 21:29
108-10-1
ND ug/kg
3.7
1
05/10/11 21:29
1634-04-4
ND ug/kg
3.7
1
05/10/11 21:29
91-20-3
ND ug/kg
3.7
1
05/10/11 21:29
103-65-1
ND ug/kg
3.7
1
05/10/11 21:29
100-42-5
ND ug/kg
3.7
1
05/10/11 21:29
630-20-6
ND ug/kg
3.7
1
05/10/11 21:29
79-34-5
ND ug/kg
3.7
1
05/10/11 21:29
127-18-4
ND ug/kg
3.7
1
05/10/11 21:29
108-88-3
ND ug/kg
3.7
1
05/10/11 21:29
87-61-6
ND ug/kg
3.7
1
05/10/11 21:29
120-82-1
ND ug/kg
3.7
1
05/10/11 21:29
71-55-6
ND ug/kg
3.7
1
05/10/11 21:29
79-00-5
ND ug/kg
3.7
1
05/10/11 21:29
79-01-6
ND ug/kg
3.7
1
05/10/11 21:29
75-69-4
ND ug/kg
3.7
1
05/10/11 21:29
96-18-4
ND ug/kg
3.7
1
05/10/11 21:29
95-63-6
ND ug/kg
3.7
1
05/10/11 21:29
108-67-8
ND ug/kg
37.0
1
05/10/11 21:29
108-05-4
ND ug/kg
7.4
1
05/10/11 21:29
75-01-4
ND ug/kg
7.4
1
05/10/11 21:29
1330-20-7
ND ug/kg
7.4
1
05/10/11 21:29
179601-23-1
ND ug/kg
3.7
1
05/10/11 21:29
95-47-6
103 %
70-130
1
05/10/11 21:29
1868-53-7
100 %
70-130
1
05/10/11 21:29
2037-26-5
96 %
70-130
1
05/10/11 21:29
460-00-4
90 %
70-132
1
05/10/11 21:29
17060-07-0
Analytical Method: ASTM D2974-87
24.1 %
0.10
1
05/11/11 08:51
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 63 of 227

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-10 Lab ID: 9293679019 Collected: 05/05/11 10:11 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
25800 mg/kg
165
20
05/11/11 14:30
05/13/11 14:39
7429-90-5
Antimony
ND mg/kg
0.41
1
05/11/11 14:30
05/12/11 15:55
7440-36-0
Arsenic
1.4 mg/kg
0.41
1
05/11/11 14:30
05/12/11 15:55
7440-38-2
Barium
186 mg/kg
0.41
1
05/11/11 14:30
05/12/11 15:55
7440-39-3
Beryllium
0.95 mg/kg
0.083
1
05/11/11 14:30
05/12/11 15:55
7440-41-7
Cadmium
1.0 mg/kg
0.083
1
05/11/11 14:30
05/12/11 15:55
7440-43-9
Calcium
1790 mg/kg
8.3
1
05/11/11 14:30
05/12/11 15:55
7440-70-2
Chromium
27.8 mg/kg
0.41
1
05/11/11 14:30
05/12/11 15:55
7440-47-3
Cobalt
1.8 mg/kg
0.41
1
05/11/11 14:30
05/12/11 15:55
7440-48-4
Copper
25.4 mg/kg
0.41
1
05/11/11 14:30
05/12/11 15:55
7440-50-8
Iron
17100 mg/kg
82.6
20
05/11/11 14:30
05/13/11 14:39
7439-89-6
Lead
9.0 mg/kg
0.41
1
05/11/11 14:30
05/12/11 15:55
7439-92-1
Magnesium
4180 mg/kg
8.3
1
05/11/11 14:30
05/12/11 15:55
7439-95-4
Manganese
162 mg/kg
0.41
1
05/11/11 14:30
05/12/11 15:55
7439-96-5
Nickel
16.8 mg/kg
0.41
1
05/11/11 14:30
05/12/11 15:55
7440-02-0
Potassium
2890 mg/kg
413
1
05/11/11 14:30
05/12/11 15:55
7440-09-7
Selenium
0.88 mg/kg
0.83
1
05/11/11 14:30
05/12/11 15:55
7782-49-2
Silver
ND mg/kg
0.41
1
05/11/11 14:30
05/12/11 15:55
7440-22-4
Sodium
ND mg/kg
413
1
05/11/11 14:30
05/12/11 15:55
7440-23-5
Thallium
ND mg/kg
0.83
1
05/11/11 14:30
05/12/11 15:55
7440-28-0
Vanadium
40.5 mg/kg
0.41
1
05/11/11 14:30
05/12/11 15:55
7440-62-2
Zinc
57.9 mg/kg
0.83
1
05/11/11 14:30
05/12/11 15:55
7440-66-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.017 mg/kg
0.0042
1
05/13/11 08:45
05/13/11 15:51
7439-97-6
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
83-32-9
Acenaphthylene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
208-96-8
Aniline
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
62-53-3
Anthracene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
120-12-7
Benzo(a)anthracene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
56-55-3
Benzo(a)pyrene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
50-32-8
Benzo(b)fluoranthene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
191-24-2
Benzo(k)fluoranthene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
207-08-9
Benzoic Acid
ND ug/kg
2020
1
05/11/11 10:15
05/12/11 23:42
65-85-0
Benzyl alcohol
ND ug/kg
807
1
05/11/11 10:15
05/12/11 23:42
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
101-55-3
Butylbenzylphthalate
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
85-68-7
4-Chloro-3-methylphenol
ND ug/kg
807
1
05/11/11 10:15
05/12/11 23:42
59-50-7
4-Chloroaniline
ND ug/kg
2020
1
05/11/11 10:15
05/12/11 23:42
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
108-60-1
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 64 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-10 Lab ID: 9293679019 Collected: 05/05/11 10:11 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Chloronaphthalene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
91-58-7
2-Chlorophenol
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
7005-72-3
Chrysene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
53-70-3
Dibenzofuran
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
132-64-9
1,2-Dichlorobenzene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
95-50-1
1,3-Dichlorobenzene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
541-73-1
1,4-Dichlorobenzene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
2020
1
05/11/11 10:15
05/12/11 23:42
91-94-1
2,4-Dichlorophenol
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
120-83-2
Diethylphthalate
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
84-66-2
2,4-Dimethylphenol
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
105-67-9
Dimethylphthalate
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
131-11-3
Di-n-butylphthalate
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/kg
807
1
05/11/11 10:15
05/12/11 23:42
534-52-1
2,4-Dinitrophenol
ND ug/kg
2020
1
05/11/11 10:15
05/12/11 23:42
51-28-5
2,4-Dinitrotoluene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
121-14-2
2,6-Dinitrotoluene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
606-20-2
Di-n-octylphthalate
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
117-81-7
Fluoranthene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
206-44-0
Fluorene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
87-68-3
Hexachlorobenzene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
77-47-4
Hexachloroethane
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
193-39-5
Isophorone
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
78-59-1
1-Methylnaphthalene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
90-12-0
2-Methylnaphthalene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
Naphthalene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
91-20-3
2-Nitroaniline
ND ug/kg
2020
1
05/11/11 10:15
05/12/11 23:42
88-74-4
3-Nitroaniline
ND ug/kg
2020
1
05/11/11 10:15
05/12/11 23:42
99-09-2
4-Nitroaniline
ND ug/kg
807
1
05/11/11 10:15
05/12/11 23:42
100-01-6
Nitrobenzene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
98-95-3
2-Nitrophenol
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
88-75-5
4-Nitrophenol
ND ug/kg
2020
1
05/11/11 10:15
05/12/11 23:42
100-02-7
N-Nitrosodimethylamine
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
86-30-6
Pentachlorophenol
ND ug/kg
2020
1
05/11/11 10:15
05/12/11 23:42
87-86-5
Phenanthrene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
85-01-8
Phenol
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
108-95-2
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 65 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-10 Lab ID: 9293679019 Collected: 05/05/11 10:11 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Pyrene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
403
1
05/11/11 10:15
05/12/11 23:42
88-06-2
Nitrobenzene-d5 (S)
69 %
23-110
1
05/11/11 10:15
05/12/11 23:42
4165-60-0
2-Fluorobiphenyl (S)
73 %
30-110
1
05/11/11 10:15
05/12/11 23:42
321-60-8
Terphenyl-d14 (S)
56 %
28-110
1
05/11/11 10:15
05/12/11 23:42
1718-51-0
Phenol-d6 (S)
54 %
22-110
1
05/11/11 10:15
05/12/11 23:42
13127-88-3
2-Fluorophenol (S)
61 %
13-110
1
05/11/11 10:15
05/12/11 23:42
367-12-4
2,4,6-Tribromophenol (S)
57 %
27-110
1
05/11/11 10:15
05/12/11 23:42
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND ug/kg
74.7
1
05/10/11 21:49
67-64-1
Benzene
ND ug/kg
3.7
1
05/10/11 21:49
71-43-2
Bromobenzene
ND ug/kg
3.7
1
05/10/11 21:49
108-86-1
Bromochloromethane
ND ug/kg
3.7
1
05/10/11 21:49
74-97-5
Bromodichloromethane
ND ug/kg
3.7
1
05/10/11 21:49
75-27-4
Bromoform
ND ug/kg
3.7
1
05/10/11 21:49
75-25-2
Bromomethane
ND ug/kg
7.5
1
05/10/11 21:49
74-83-9
2-Butanone (MEK)
ND ug/kg
74.7
1
05/10/11 21:49
78-93-3
n-Butylbenzene
ND ug/kg
3.7
1
05/10/11 21:49
104-51-8
sec -Butyl benzene
ND ug/kg
3.7
1
05/10/11 21:49
135-98-8
tert-Butyl benzene
ND ug/kg
3.7
1
05/10/11 21:49
98-06-6
Carbon tetrachloride
ND ug/kg
3.7
1
05/10/11 21:49
56-23-5
Chlorobenzene
ND ug/kg
3.7
1
05/10/11 21:49
108-90-7
Chloroethane
ND ug/kg
7.5
1
05/10/11 21:49
75-00-3
Chloroform
ND ug/kg
3.7
1
05/10/11 21:49
67-66-3
Chloromethane
ND ug/kg
7.5
1
05/10/11 21:49
74-87-3
2-Chlorotoluene
ND ug/kg
3.7
1
05/10/11 21:49
95-49-8
4-Chlorotoluene
ND ug/kg
3.7
1
05/10/11 21:49
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
3.7
1
05/10/11 21:49
96-12-8
Dibromochloromethane
ND ug/kg
3.7
1
05/10/11 21:49
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
3.7
1
05/10/11 21:49
106-93-4
Dibromomethane
ND ug/kg
3.7
1
05/10/11 21:49
74-95-3
1,2-Dichlorobenzene
ND ug/kg
3.7
1
05/10/11 21:49
95-50-1
1,3-Dichlorobenzene
ND ug/kg
3.7
1
05/10/11 21:49
541-73-1
1,4-Dichlorobenzene
ND ug/kg
3.7
1
05/10/11 21:49
106-46-7
Dichlorodifluoromethane
ND ug/kg
7.5
1
05/10/11 21:49
75-71-8
1,1-Dichloroethane
ND ug/kg
3.7
1
05/10/11 21:49
75-34-3
1,2-Dichloroethane
ND ug/kg
3.7
1
05/10/11 21:49
107-06-2
1,1-Dichloroethene
ND ug/kg
3.7
1
05/10/11 21:49
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
3.7
1
05/10/11 21:49
156-59-2
trans- 1,2-Dichloroethene
ND ug/kg
3.7
1
05/10/11 21:49
156-60-5
1,2-Dichloropropane
ND ug/kg
3.7
1
05/10/11 21:49
78-87-5
1,3-Dichloropropane
ND ug/kg
3.7
1
05/10/11 21:49
142-28-9
2,2-Dichloropropane
ND ug/kg
3.7
1
05/10/11 21:49
594-20-7
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY
ANALYSIS
Page 66 of 227
This report shall not be reproduced, except
in
full,
without the written consent of Pace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-10 Lab ID: 9293679019 Collected: 05/05/11 10:11 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1-Dichloropropene
ND ug/kg
3.7
1
05/10/11 21:49
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
3.7
1
05/10/11 21:49
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
3.7
1
05/10/11 21:49
10061-02-6
Diisopropyl ether
ND ug/kg
3.7
1
05/10/11 21:49
108-20-3
Ethylbenzene
ND ug/kg
3.7
1
05/10/11 21:49
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
3.7
1
05/10/11 21:49
87-68-3
2-Hexanone
ND ug/kg
37.4
1
05/10/11 21:49
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
3.7
1
05/10/11 21:49
98-82-8
p-Isopropyltoluene
ND ug/kg
3.7
1
05/10/11 21:49
99-87-6
Methylene Chloride
ND ug/kg
14.9
1
05/10/11 21:49
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
37.4
1
05/10/11 21:49
108-10-1
Methyl-tert-butyl ether
ND ug/kg
3.7
1
05/10/11 21:49
1634-04-4
Naphthalene
ND ug/kg
3.7
1
05/10/11 21:49
91-20-3
n-Propylbenzene
ND ug/kg
3.7
1
05/10/11 21:49
103-65-1
Styrene
ND ug/kg
3.7
1
05/10/11 21:49
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
3.7
1
05/10/11 21:49
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
3.7
1
05/10/11 21:49
79-34-5
Tetrachloroethene
ND ug/kg
3.7
1
05/10/11 21:49
127-18-4
Toluene
ND ug/kg
3.7
1
05/10/11 21:49
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
3.7
1
05/10/11 21:49
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
3.7
1
05/10/11 21:49
120-82-1
1,1,1-Trichloroethane
ND ug/kg
3.7
1
05/10/11 21:49
71-55-6
1,1,2-Trichloroethane
ND ug/kg
3.7
1
05/10/11 21:49
79-00-5
Trichloroethene
ND ug/kg
3.7
1
05/10/11 21:49
79-01-6
Trichlorofluoromethane
ND ug/kg
3.7
1
05/10/11 21:49
75-69-4
1,2,3-Trichloropropane
ND ug/kg
3.7
1
05/10/11 21:49
96-18-4
1,2,4-Trimethylbenzene
ND ug/kg
3.7
1
05/10/11 21:49
95-63-6
1,3,5-Trimethylbenzene
ND ug/kg
3.7
1
05/10/11 21:49
108-67-8
Vinyl acetate
ND ug/kg
37.4
1
05/10/11 21:49
108-05-4
Vinyl chloride
ND ug/kg
7.5
1
05/10/11 21:49
75-01-4
Xylene (Total)
ND ug/kg
7.5
1
05/10/11 21:49
1330-20-7
m&p-Xylene
ND ug/kg
7.5
1
05/10/11 21:49
179601-23-1
o-Xylene
ND ug/kg
3.7
1
05/10/11 21:49
95-47-6
Dibromofluoromethane (S)
104 %
70-130
1
05/10/11 21:49
1868-53-7
Toluene-d8 (S)
99 %
70-130
1
05/10/11 21:49
2037-26-5
4-Bromofluorobenzene (S)
92 %
70-130
1
05/10/11 21:49
460-00-4
1,2-Dichloroethane-d4 (S)
98 %
70-132
1
05/10/11 21:49
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
18.2 %
0.10
1
05/11/11 08:51
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 67 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-8 Lab ID: 9293679020 Collected: 05/05/11 10:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
19600 mg/kg
264
20
05/11/11 14:30
05/13/11 14:43
7429-90-5
Antimony
ND mg/kg
0.66
1
05/11/11 14:30
05/12/11 16:00
7440-36-0
Arsenic
0.98 mg/kg
0.66
1
05/11/11 14:30
05/12/11 16:00
7440-38-2
Barium
148 mg/kg
0.66
1
05/11/11 14:30
05/12/11 16:00
7440-39-3
Beryllium
1.2 mg/kg
0.13
1
05/11/11 14:30
05/12/11 16:00
7440-41-7
Cadmium
3.5 mg/kg
0.13
1
05/11/11 14:30
05/12/11 16:00
7440-43-9
Calcium
6710 mg/kg
13.2
1
05/11/11 14:30
05/12/11 16:00
7440-70-2
Chromium
38.7 mg/kg
0.66
1
05/11/11 14:30
05/12/11 16:00
7440-47-3
Cobalt
11.6 mg/kg
0.66
1
05/11/11 14:30
05/12/11 16:00
7440-48-4
Copper
20.6 mg/kg
0.66
1
05/11/11 14:30
05/12/11 16:00
7440-50-8
Iron
43300 mg/kg
132
20
05/11/11 14:30
05/13/11 14:43
7439-89-6
Lead
21.0 mg/kg
0.66
1
05/11/11 14:30
05/12/11 16:00
7439-92-1
Magnesium
3000 mg/kg
13.2
1
05/11/11 14:30
05/12/11 16:00
7439-95-4
Manganese
453 mg/kg
0.66
1
05/11/11 14:30
05/12/11 16:00
7439-96-5
Nickel
10.4 mg/kg
0.66
1
05/11/11 14:30
05/12/11 16:00
7440-02-0
Potassium
4300 mg/kg
660
1
05/11/11 14:30
05/12/11 16:00
7440-09-7
Selenium
1.5 mg/kg
1.3
1
05/11/11 14:30
05/12/11 16:00
7782-49-2
Silver
ND mg/kg
0.66
1
05/11/11 14:30
05/12/11 16:00
7440-22-4
Sodium
ND mg/kg
660
1
05/11/11 14:30
05/12/11 16:00
7440-23-5
Thallium
ND mg/kg
1.3
1
05/11/11 14:30
05/12/11 16:00
7440-28-0
Vanadium
50.0 mg/kg
0.66
1
05/11/11 14:30
05/12/11 16:00
7440-62-2
Zinc
78.9 mg/kg
1.3
1
05/11/11 14:30
05/12/11 16:00
7440-66-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
1.4 mg/kg
0.13
20
05/13/11 08:45
05/16/11 13:29
7439-97-6
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
83-32-9
Acenaphthylene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
208-96-8
Aniline
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
62-53-3
Anthracene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
120-12-7
Benzo(a)anthracene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
56-55-3
Benzo(a)pyrene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
50-32-8
Benzo(b)fluoranthene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
191-24-2
Benzo(k)fluoranthene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
207-08-9
Benzoic Acid
ND ug/kg
2340
1
05/11/11 10:15
05/13/11 01:05
65-85-0
Benzyl alcohol
ND ug/kg
937
1
05/11/11 10:15
05/13/11 01:05
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
101-55-3
Butylbenzylphthalate
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
85-68-7
4-Chloro-3-methylphenol
ND ug/kg
937
1
05/11/11 10:15
05/13/11 01:05
59-50-7
4-Chloroaniline
ND ug/kg
2340
1
05/11/11 10:15
05/13/11 01:05
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
108-60-1
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 68 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-8 Lab ID: 9293679020 Collected: 05/05/11 10:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Chloronaphthalene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
91-58-7
2-Chlorophenol
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
7005-72-3
Chrysene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
53-70-3
Dibenzofuran
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
132-64-9
1,2-Dichlorobenzene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
95-50-1
1,3-Dichlorobenzene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
541-73-1
1,4-Dichlorobenzene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
2340
1
05/11/11 10:15
05/13/11 01:05
91-94-1
2,4-Dichlorophenol
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
120-83-2
Diethylphthalate
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
84-66-2
2,4-Dimethylphenol
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
105-67-9
Dimethylphthalate
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
131-11-3
Di-n-butylphthalate
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/kg
937
1
05/11/11 10:15
05/13/11 01:05
534-52-1
2,4-Dinitrophenol
ND ug/kg
2340
1
05/11/11 10:15
05/13/11 01:05
51-28-5
2,4-Dinitrotoluene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
121-14-2
2,6-Dinitrotoluene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
606-20-2
Di-n-octylphthalate
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
117-81-7
Fluoranthene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
206-44-0
Fluorene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
87-68-3
Hexachlorobenzene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
77-47-4
Hexachloroethane
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
193-39-5
Isophorone
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
78-59-1
1-Methylnaphthalene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
90-12-0
2-Methylnaphthalene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
Naphthalene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
91-20-3
2-Nitroaniline
ND ug/kg
2340
1
05/11/11 10:15
05/13/11 01:05
88-74-4
3-Nitroaniline
ND ug/kg
2340
1
05/11/11 10:15
05/13/11 01:05
99-09-2
4-Nitroaniline
ND ug/kg
937
1
05/11/11 10:15
05/13/11 01:05
100-01-6
Nitrobenzene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
98-95-3
2-Nitrophenol
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
88-75-5
4-Nitrophenol
ND ug/kg
2340
1
05/11/11 10:15
05/13/11 01:05
100-02-7
N-Nitrosodimethylamine
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
86-30-6
Pentachlorophenol
ND ug/kg
2340
1
05/11/11 10:15
05/13/11 01:05
87-86-5
Phenanthrene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
85-01-8
Phenol
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
108-95-2
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 69 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-8 Lab ID: 9293679020 Collected: 05/05/11 10:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Pyrene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
469
1
05/11/11 10:15
05/13/11 01:05
88-06-2
Nitrobenzene-d5 (S)
65 %
23-110
1
05/11/11 10:15
05/13/11 01:05
4165-60-0
2-Fluorobiphenyl (S)
64 %
30-110
1
05/11/11 10:15
05/13/11 01:05
321-60-8
Terphenyl-d14 (S)
60 %
28-110
1
05/11/11 10:15
05/13/11 01:05
1718-51-0
Phenol-d6 (S)
51 %
22-110
1
05/11/11 10:15
05/13/11 01:05
13127-88-3
2-Fluorophenol (S)
56 %
13-110
1
05/11/11 10:15
05/13/11 01:05
367-12-4
2,4,6-Tribromophenol (S)
58 %
27-110
1
05/11/11 10:15
05/13/11 01:05
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND ug/kg
106
1
05/10/11 22:09
67-64-1
Benzene
ND ug/kg
5.3
1
05/10/11 22:09
71-43-2
Bromobenzene
ND ug/kg
5.3
1
05/10/11 22:09
108-86-1
Bromochloromethane
ND ug/kg
5.3
1
05/10/11 22:09
74-97-5
Bromodichloromethane
ND ug/kg
5.3
1
05/10/11 22:09
75-27-4
Bromoform
ND ug/kg
5.3
1
05/10/11 22:09
75-25-2
Bromomethane
ND ug/kg
10.6
1
05/10/11 22:09
74-83-9
2-Butanone (MEK)
ND ug/kg
106
1
05/10/11 22:09
78-93-3
n-Butylbenzene
ND ug/kg
5.3
1
05/10/11 22:09
104-51-8
sec -Butyl benzene
ND ug/kg
5.3
1
05/10/11 22:09
135-98-8
tert-Butyl benzene
ND ug/kg
5.3
1
05/10/11 22:09
98-06-6
Carbon tetrachloride
ND ug/kg
5.3
1
05/10/11 22:09
56-23-5
Chlorobenzene
ND ug/kg
5.3
1
05/10/11 22:09
108-90-7
Chloroethane
ND ug/kg
10.6
1
05/10/11 22:09
75-00-3
Chloroform
ND ug/kg
5.3
1
05/10/11 22:09
67-66-3
Chloromethane
ND ug/kg
10.6
1
05/10/11 22:09
74-87-3
2-Chlorotoluene
ND ug/kg
5.3
1
05/10/11 22:09
95-49-8
4-Chlorotoluene
ND ug/kg
5.3
1
05/10/11 22:09
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
5.3
1
05/10/11 22:09
96-12-8
Dibromochloromethane
ND ug/kg
5.3
1
05/10/11 22:09
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
5.3
1
05/10/11 22:09
106-93-4
Dibromomethane
ND ug/kg
5.3
1
05/10/11 22:09
74-95-3
1,2-Dichlorobenzene
ND ug/kg
5.3
1
05/10/11 22:09
95-50-1
1,3-Dichlorobenzene
ND ug/kg
5.3
1
05/10/11 22:09
541-73-1
1,4-Dichlorobenzene
ND ug/kg
5.3
1
05/10/11 22:09
106-46-7
Dichlorodifluoromethane
ND ug/kg
10.6
1
05/10/11 22:09
75-71-8
1,1-Dichloroethane
ND ug/kg
5.3
1
05/10/11 22:09
75-34-3
1,2-Dichloroethane
ND ug/kg
5.3
1
05/10/11 22:09
107-06-2
1,1-Dichloroethene
ND ug/kg
5.3
1
05/10/11 22:09
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
5.3
1
05/10/11 22:09
156-59-2
trans- 1,2-Dichloroethene
ND ug/kg
5.3
1
05/10/11 22:09
156-60-5
1,2-Dichloropropane
ND ug/kg
5.3
1
05/10/11 22:09
78-87-5
1,3-Dichloropropane
ND ug/kg
5.3
1
05/10/11 22:09
142-28-9
2,2-Dichloropropane
ND ug/kg
5.3
1
05/10/11 22:09
594-20-7
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY
ANALYSIS
Page 70 of 227
This report shall not be reproduced, except
in
full,
without the written consent of Pace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-8 Lab ID: 9293679020 Collected: 05/05/11 10:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1-Dichloropropene
ND ug/kg
5.3
1
05/10/11 22:09
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
5.3
1
05/10/11 22:09
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
5.3
1
05/10/11 22:09
10061-02-6
Diisopropyl ether
ND ug/kg
5.3
1
05/10/11 22:09
108-20-3
Ethylbenzene
ND ug/kg
5.3
1
05/10/11 22:09
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
5.3
1
05/10/11 22:09
87-68-3
2-Hexanone
ND ug/kg
52.9
1
05/10/11 22:09
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
5.3
1
05/10/11 22:09
98-82-8
p-Isopropyltoluene
ND ug/kg
5.3
1
05/10/11 22:09
99-87-6
Methylene Chloride
ND ug/kg
21.2
1
05/10/11 22:09
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
52.9
1
05/10/11 22:09
108-10-1
Methyl-tert-butyl ether
ND ug/kg
5.3
1
05/10/11 22:09
1634-04-4
Naphthalene
ND ug/kg
5.3
1
05/10/11 22:09
91-20-3
n-Propylbenzene
ND ug/kg
5.3
1
05/10/11 22:09
103-65-1
Styrene
ND ug/kg
5.3
1
05/10/11 22:09
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
5.3
1
05/10/11 22:09
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
5.3
1
05/10/11 22:09
79-34-5
Tetrachloroethene
ND ug/kg
5.3
1
05/10/11 22:09
127-18-4
Toluene
ND ug/kg
5.3
1
05/10/11 22:09
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
5.3
1
05/10/11 22:09
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
5.3
1
05/10/11 22:09
120-82-1
1,1,1-Trichloroethane
ND ug/kg
5.3
1
05/10/11 22:09
71-55-6
1,1,2-Trichloroethane
ND ug/kg
5.3
1
05/10/11 22:09
79-00-5
Trichloroethene
ND ug/kg
5.3
1
05/10/11 22:09
79-01-6
Trichlorofluoromethane
ND ug/kg
5.3
1
05/10/11 22:09
75-69-4
1,2,3-Trichloropropane
ND ug/kg
5.3
1
05/10/11 22:09
96-18-4
1,2,4-Trimethylbenzene
ND ug/kg
5.3
1
05/10/11 22:09
95-63-6
1,3,5-Trimethylbenzene
ND ug/kg
5.3
1
05/10/11 22:09
108-67-8
Vinyl acetate
ND ug/kg
52.9
1
05/10/11 22:09
108-05-4
Vinyl chloride
ND ug/kg
10.6
1
05/10/11 22:09
75-01-4
Xylene (Total)
ND ug/kg
10.6
1
05/10/11 22:09
1330-20-7
m&p-Xylene
ND ug/kg
10.6
1
05/10/11 22:09
179601-23-1
o-Xylene
ND ug/kg
5.3
1
05/10/11 22:09
95-47-6
Dibromofluoromethane (S)
108 %
70-130
1
05/10/11 22:09
1868-53-7
Toluene-d8 (S)
103 %
70-130
1
05/10/11 22:09
2037-26-5
4-Bromofluorobenzene (S)
99 %
70-130
1
05/10/11 22:09
460-00-4
1,2-Dichloroethane-d4 (S)
95 %
70-132
1
05/10/11 22:09
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
29.8 %
0.10
1
05/11/11 14:53
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 71 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-7 Lab ID: 9293679021 Collected: 05/05/11 11:20 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
21700 mg/kg
102
10
05/12/11 15:15
05/16/11 11:45
7429-90-5
Antimony
ND mg/kg
0.51
1
05/12/11 15:15
05/14/11 15:01
7440-36-0
Arsenic
1.8 mg/kg
0.51
1
05/12/11 15:15
05/15/11 20:56
7440-38-2
Barium
58.9 mg/kg
0.51
1
05/12/11 15:15
05/14/11 15:01
7440-39-3
Beryllium
0.47 mg/kg
0.10
1
05/12/11 15:15
05/14/11 15:01
7440-41-7
Cadmium
0.63 mg/kg
0.10
1
05/12/11 15:15
05/14/11 15:01
7440-43-9
Calcium
103 mg/kg
10.2
1
05/12/11 15:15
05/14/11 15:01
7440-70-2
Chromium
21.4 mg/kg
0.51
1
05/12/11 15:15
05/14/11 15:01
7440-47-3
Cobalt
2.2 mg/kg
0.51
1
05/12/11 15:15
05/14/11 15:01
7440-48-4
Copper
11.7 mg/kg
0.51
1
05/12/11 15:15
05/14/11 15:01
7440-50-8
Iron
20900 mg/kg
50.8
10
05/12/11 15:15
05/16/11 11:45
7439-89-6
Lead
11.8 mg/kg
0.51
1
05/12/11 15:15
05/14/11 15:01
7439-92-1
Magnesium
3180 mg/kg
10.2
1
05/12/11 15:15
05/14/11 15:01
7439-95-4
Manganese
59.6 mg/kg
0.51
1
05/12/11 15:15
05/14/11 15:01
7439-96-5
Nickel
9.8 mg/kg
0.51
1
05/12/11 15:15
05/14/11 15:01
7440-02-0
Potassium
2790 mg/kg
508
1
05/12/11 15:15
05/14/11 15:01
7440-09-7
Selenium
1.4 mg/kg
1.0
1
05/12/11 15:15
05/15/11 20:56
7782-49-2
Silver
ND mg/kg
0.51
1
05/12/11 15:15
05/14/11 15:01
7440-22-4
Sodium
ND mg/kg
508
1
05/12/11 15:15
05/14/11 15:01
7440-23-5
Thallium
ND mg/kg
1.0
1
05/12/11 15:15
05/14/11 15:01
7440-28-0
Vanadium
30.4 mg/kg
0.51
1
05/12/11 15:15
05/14/11 15:01
7440-62-2
Zinc
39.7 mg/kg
1.0
1
05/12/11 15:15
05/14/11 15:01
7440-66-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.054 mg/kg
0.0036
1
05/13/11 08:45
05/13/11 16:01
7439-97-6
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
83-32-9
Acenaphthylene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
208-96-8
Aniline
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
62-53-3
Anthracene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
120-12-7
Benzo(a)anthracene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
56-55-3
Benzo(a)pyrene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
50-32-8
Benzo(b)fluoranthene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
191-24-2
Benzo(k)fluoranthene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
207-08-9
Benzoic Acid
ND ug/kg
1940
1
05/11/11 10:15
05/13/11 01:33
65-85-0
Benzyl alcohol
ND ug/kg
777
1
05/11/11 10:15
05/13/11 01:33
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
101-55-3
Butylbenzylphthalate
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
85-68-7
4-Chloro-3-methylphenol
ND ug/kg
777
1
05/11/11 10:15
05/13/11 01:33
59-50-7
4-Chloroaniline
ND ug/kg
1940
1
05/11/11 10:15
05/13/11 01:33
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
108-60-1
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 72 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-7 Lab ID: 9293679021 Collected: 05/05/11 11:20 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Chloronaphthalene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
91-58-7
2-Chlorophenol
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
7005-72-3
Chrysene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
53-70-3
Dibenzofuran
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
132-64-9
1,2-Dichlorobenzene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
95-50-1
1,3-Dichlorobenzene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
541-73-1
1,4-Dichlorobenzene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
1940
1
05/11/11 10:15
05/13/11 01:33
91-94-1
2,4-Dichlorophenol
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
120-83-2
Diethylphthalate
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
84-66-2
2,4-Dimethylphenol
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
105-67-9
Dimethylphthalate
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
131-11-3
Di-n-butylphthalate
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/kg
777
1
05/11/11 10:15
05/13/11 01:33
534-52-1
2,4-Dinitrophenol
ND ug/kg
1940
1
05/11/11 10:15
05/13/11 01:33
51-28-5
2,4-Dinitrotoluene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
121-14-2
2,6-Dinitrotoluene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
606-20-2
Di-n-octylphthalate
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
117-81-7
Fluoranthene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
206-44-0
Fluorene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
87-68-3
Hexachlorobenzene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
77-47-4
Hexachloroethane
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
193-39-5
Isophorone
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
78-59-1
1-Methylnaphthalene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
90-12-0
2-Methylnaphthalene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
Naphthalene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
91-20-3
2-Nitroaniline
ND ug/kg
1940
1
05/11/11 10:15
05/13/11 01:33
88-74-4
3-Nitroaniline
ND ug/kg
1940
1
05/11/11 10:15
05/13/11 01:33
99-09-2
4-Nitroaniline
ND ug/kg
777
1
05/11/11 10:15
05/13/11 01:33
100-01-6
Nitrobenzene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
98-95-3
2-Nitrophenol
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
88-75-5
4-Nitrophenol
ND ug/kg
1940
1
05/11/11 10:15
05/13/11 01:33
100-02-7
N-Nitrosodimethylamine
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
86-30-6
Pentachlorophenol
ND ug/kg
1940
1
05/11/11 10:15
05/13/11 01:33
87-86-5
Phenanthrene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
85-01-8
Phenol
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
108-95-2
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 73 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-7 Lab ID: 9293679021 Collected: 05/05/11 11:20 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Pyrene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
389
1
05/11/11 10:15
05/13/11 01:33
88-06-2
Nitrobenzene-d5 (S)
44 %
23-110
1
05/11/11 10:15
05/13/11 01:33
4165-60-0
2-Fluorobiphenyl (S)
52 %
30-110
1
05/11/11 10:15
05/13/11 01:33
321-60-8
Terphenyl-d14 (S)
55 %
28-110
1
05/11/11 10:15
05/13/11 01:33
1718-51-0
Phenol-d6 (S)
34 %
22-110
1
05/11/11 10:15
05/13/11 01:33
13127-88-3
2-Fluorophenol (S)
38 %
13-110
1
05/11/11 10:15
05/13/11 01:33
367-12-4
2,4,6-Tribromophenol (S)
44 %
27-110
1
05/11/11 10:15
05/13/11 01:33
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND ug/kg
87.9
1
05/10/11 22:29
67-64-1
Benzene
ND ug/kg
4.4
1
05/10/11 22:29
71-43-2
Bromobenzene
ND ug/kg
4.4
1
05/10/11 22:29
108-86-1
Bromochloromethane
ND ug/kg
4.4
1
05/10/11 22:29
74-97-5
Bromodichloromethane
ND ug/kg
4.4
1
05/10/11 22:29
75-27-4
Bromoform
ND ug/kg
4.4
1
05/10/11 22:29
75-25-2
Bromomethane
ND ug/kg
8.8
1
05/10/11 22:29
74-83-9
2-Butanone (MEK)
ND ug/kg
87.9
1
05/10/11 22:29
78-93-3
n-Butylbenzene
ND ug/kg
4.4
1
05/10/11 22:29
104-51-8
sec -Butyl benzene
ND ug/kg
4.4
1
05/10/11 22:29
135-98-8
tert-Butyl benzene
ND ug/kg
4.4
1
05/10/11 22:29
98-06-6
Carbon tetrachloride
ND ug/kg
4.4
1
05/10/11 22:29
56-23-5
Chlorobenzene
ND ug/kg
4.4
1
05/10/11 22:29
108-90-7
Chloroethane
ND ug/kg
8.8
1
05/10/11 22:29
75-00-3
Chloroform
ND ug/kg
4.4
1
05/10/11 22:29
67-66-3
Chloromethane
ND ug/kg
8.8
1
05/10/11 22:29
74-87-3
2-Chlorotoluene
ND ug/kg
4.4
1
05/10/11 22:29
95-49-8
4-Chlorotoluene
ND ug/kg
4.4
1
05/10/11 22:29
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
4.4
1
05/10/11 22:29
96-12-8
Dibromochloromethane
ND ug/kg
4.4
1
05/10/11 22:29
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
4.4
1
05/10/11 22:29
106-93-4
Dibromomethane
ND ug/kg
4.4
1
05/10/11 22:29
74-95-3
1,2-Dichlorobenzene
ND ug/kg
4.4
1
05/10/11 22:29
95-50-1
1,3-Dichlorobenzene
ND ug/kg
4.4
1
05/10/11 22:29
541-73-1
1,4-Dichlorobenzene
ND ug/kg
4.4
1
05/10/11 22:29
106-46-7
Dichlorodifluoromethane
ND ug/kg
8.8
1
05/10/11 22:29
75-71-8
1,1-Dichloroethane
ND ug/kg
4.4
1
05/10/11 22:29
75-34-3
1,2-Dichloroethane
ND ug/kg
4.4
1
05/10/11 22:29
107-06-2
1,1-Dichloroethene
ND ug/kg
4.4
1
05/10/11 22:29
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
4.4
1
05/10/11 22:29
156-59-2
trans- 1,2-Dichloroethene
ND ug/kg
4.4
1
05/10/11 22:29
156-60-5
1,2-Dichloropropane
ND ug/kg
4.4
1
05/10/11 22:29
78-87-5
1,3-Dichloropropane
ND ug/kg
4.4
1
05/10/11 22:29
142-28-9
2,2-Dichloropropane
ND ug/kg
4.4
1
05/10/11 22:29
594-20-7
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY
ANALYSIS
Page 74 of 227
This report shall not be reproduced, except
in
full,
without the written consent of Pace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-7 Lab ID: 9293679021 Collected: 05/05/11 11:20 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1-Dichloropropene
ND ug/kg
4.4
1
05/10/11 22:29
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
4.4
1
05/10/11 22:29
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
4.4
1
05/10/11 22:29
10061-02-6
Diisopropyl ether
ND ug/kg
4.4
1
05/10/11 22:29
108-20-3
Ethylbenzene
ND ug/kg
4.4
1
05/10/11 22:29
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
4.4
1
05/10/11 22:29
87-68-3
2-Hexanone
ND ug/kg
44.0
1
05/10/11 22:29
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
4.4
1
05/10/11 22:29
98-82-8
p-Isopropyltoluene
ND ug/kg
4.4
1
05/10/11 22:29
99-87-6
Methylene Chloride
ND ug/kg
17.6
1
05/10/11 22:29
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
44.0
1
05/10/11 22:29
108-10-1
Methyl-tert-butyl ether
ND ug/kg
4.4
1
05/10/11 22:29
1634-04-4
Naphthalene
ND ug/kg
4.4
1
05/10/11 22:29
91-20-3
n-Propylbenzene
ND ug/kg
4.4
1
05/10/11 22:29
103-65-1
Styrene
ND ug/kg
4.4
1
05/10/11 22:29
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
4.4
1
05/10/11 22:29
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
4.4
1
05/10/11 22:29
79-34-5
Tetrachloroethene
ND ug/kg
4.4
1
05/10/11 22:29
127-18-4
Toluene
ND ug/kg
4.4
1
05/10/11 22:29
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
4.4
1
05/10/11 22:29
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
4.4
1
05/10/11 22:29
120-82-1
1,1,1-Trichloroethane
ND ug/kg
4.4
1
05/10/11 22:29
71-55-6
1,1,2-Trichloroethane
ND ug/kg
4.4
1
05/10/11 22:29
79-00-5
Trichloroethene
ND ug/kg
4.4
1
05/10/11 22:29
79-01-6
Trichlorofluoromethane
ND ug/kg
4.4
1
05/10/11 22:29
75-69-4
1,2,3-Trichloropropane
ND ug/kg
4.4
1
05/10/11 22:29
96-18-4
1,2,4-Trimethylbenzene
ND ug/kg
4.4
1
05/10/11 22:29
95-63-6
1,3,5-Trimethylbenzene
ND ug/kg
4.4
1
05/10/11 22:29
108-67-8
Vinyl acetate
ND ug/kg
44.0
1
05/10/11 22:29
108-05-4
Vinyl chloride
ND ug/kg
8.8
1
05/10/11 22:29
75-01-4
Xylene (Total)
ND ug/kg
8.8
1
05/10/11 22:29
1330-20-7
m&p-Xylene
ND ug/kg
8.8
1
05/10/11 22:29
179601-23-1
o-Xylene
ND ug/kg
4.4
1
05/10/11 22:29
95-47-6
Dibromofluoromethane (S)
107 %
70-130
1
05/10/11 22:29
1868-53-7
Toluene-d8 (S)
100 %
70-130
1
05/10/11 22:29
2037-26-5
4-Bromofluorobenzene (S)
98 %
70-130
1
05/10/11 22:29
460-00-4
1,2-Dichloroethane-d4 (S)
98 %
70-132
1
05/10/11 22:29
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
15.1 %
0.10
1
05/11/11 14:53
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 75 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-23 Lab ID: 9293679023 Collected: 05/05/11 15:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
9071 Oil and Grease
Analytical Method: 9071 B Preparation Method: 9071 B
Oil and Grease
ND mg/kg
81.3
1
05/11/11 10:45
05/11/11 11:21
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
83-32-9
Acenaphthylene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
208-96-8
Aniline
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
62-53-3
Anthracene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
120-12-7
Benzo(a)anthracene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
56-55-3
Benzo(a)pyrene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
50-32-8
Benzo(b)fluoranthene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
191-24-2
Benzo(k)fluoranthene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
207-08-9
Benzoic Acid
ND ug/kg
1920
1
05/11/11 10:15
05/13/11 02:01
65-85-0
Benzyl alcohol
ND ug/kg
769
1
05/11/11 10:15
05/13/11 02:01
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
101-55-3
Butylbenzylphthalate
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
85-68-7
4-Chloro-3-methylphenol
ND ug/kg
769
1
05/11/11 10:15
05/13/11 02:01
59-50-7
4-Chloroaniline
ND ug/kg
1920
1
05/11/11 10:15
05/13/11 02:01
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
108-60-1
2-Chloronaphthalene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
91-58-7
2-Chlorophenol
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
7005-72-3
Chrysene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
53-70-3
Dibenzofuran
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
132-64-9
1,2-Dichlorobenzene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
95-50-1
1,3-Dichlorobenzene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
541-73-1
1,4-Dichlorobenzene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
1920
1
05/11/11 10:15
05/13/11 02:01
91-94-1
2,4-Dichlorophenol
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
120-83-2
Diethylphthalate
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
84-66-2
2,4-Dimethylphenol
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
105-67-9
Dimethylphthalate
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
131-11-3
Di-n-butylphthalate
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
84-74-2
4,6-Dinitro-2-methylphenol
ND ug/kg
769
1
05/11/11 10:15
05/13/11 02:01
534-52-1
2,4-Dinitrophenol
ND ug/kg
1920
1
05/11/11 10:15
05/13/11 02:01
51-28-5
2,4-Dinitrotoluene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
121-14-2
2,6-Dinitrotoluene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
606-20-2
Di-n-octylphthalate
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
117-81-7
Fluoranthene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
206-44-0
Fluorene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
87-68-3
Hexachlorobenzene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
118-74-1
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 76 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-23
Lab ID: 9293679023
Collected: 05/05/11
15:00
Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight"
basis
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8270 MSSV Microwave
Analytical Method: EPA 8270 Preparation Method: EPA 3546
Hexachlorocyclopentadiene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
77-47-4
Hexachloroethane
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
193-39-5
Isophorone
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
78-59-1
1-Methylnaphthalene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
90-12-0
2-Methylnaphthalene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
Naphthalene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
91-20-3
2-Nitroaniline
ND ug/kg
1920
1
05/11/11 10:15
05/13/11 02:01
88-74-4
3-Nitroaniline
ND ug/kg
1920
1
05/11/11 10:15
05/13/11 02:01
99-09-2
4-Nitroaniline
ND ug/kg
769
1
05/11/11 10:15
05/13/11 02:01
100-01-6
Nitrobenzene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
98-95-3
2-Nitrophenol
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
88-75-5
4-Nitrophenol
ND ug/kg
1920
1
05/11/11 10:15
05/13/11 02:01
100-02-7
N-Nitrosodimethylamine
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
86-30-6
Pentachlorophenol
ND ug/kg
1920
1
05/11/11 10:15
05/13/11 02:01
87-86-5
Phenanthrene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
85-01-8
Phenol
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
108-95-2
Pyrene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
384
1
05/11/11 10:15
05/13/11 02:01
88-06-2
Nitrobenzene-d5 (S)
50 %
23-110
1
05/11/11 10:15
05/13/11 02:01
4165-60-0
2-Fluorobiphenyl (S)
51 %
30-110
1
05/11/11 10:15
05/13/11 02:01
321-60-8
Terphenyl-d14 (S)
51 %
28-110
1
05/11/11 10:15
05/13/11 02:01
1718-51-0
Phenol-d6 (S)
31 %
22-110
1
05/11/11 10:15
05/13/11 02:01
13127-88-3
2-Fluorophenol (S)
29 %
13-110
1
05/11/11 10:15
05/13/11 02:01
367-12-4
2,4,6-Tribromophenol (S)
25 %
27-110
1
05/11/11 10:15
05/13/11 02:01
118-79-6 SO
Percent Moisture
Analytical Method: ASTM
D2974-87
Percent Moisture
13.9 %
0.10
1
05/12/11 09:30
Sample: MW-24
Lab ID: 9293679024
Collected: 05/05/11 15:30
Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight"
basis
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
27600 mg/kg
123
10
05/12/11 15:15
05/16/11 11:49
7429-90-5
Antimony
ND mg/kg
0.62
1
05/12/11 15:15
05/14/11 15:06
7440-36-0
Arsenic
2.4 mg/kg
0.62
1
05/12/11 15:15
05/15/11 21:01
7440-38-2
Barium
75.3 mg/kg
0.62
1
05/12/11 15:15
05/14/11 15:06
7440-39-3
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
Page 77 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-24 Lab ID: 9293679024 Collected: 05/05/11 15:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Beryllium
0.76 mg/kg
0.12
1
05/12/11 15:15
05/14/11 15:06
7440-41-7
Cadmium
ND mg/kg
0.12
1
05/12/11 15:15
05/14/11 15:06
7440-43-9
Calcium
169 mg/kg
12.3
1
05/12/11 15:15
05/14/11 15:06
7440-70-2
Chromium
14.0 mg/kg
0.62
1
05/12/11 15:15
05/14/11 15:06
7440-47-3
Cobalt
ND mg/kg
0.62
1
05/12/11 15:15
05/14/11 15:06
7440-48-4
Copper
16.6 mg/kg
0.62
1
05/12/11 15:15
05/14/11 15:06
7440-50-8
Iron
4210 mg/kg
6.2
1
05/12/11 15:15
05/14/11 15:06
7439-89-6
Lead
13.4 mg/kg
0.62
1
05/12/11 15:15
05/14/11 15:06
7439-92-1
Magnesium
685 mg/kg
12.3
1
05/12/11 15:15
05/14/11 15:06
7439-95-4
Manganese
23.3 mg/kg
0.62
1
05/12/11 15:15
05/14/11 15:06
7439-96-5
Nickel
9.1 mg/kg
0.62
1
05/12/11 15:15
05/14/11 15:06
7440-02-0
Potassium
935 mg/kg
616
1
05/12/11 15:15
05/14/11 15:06
7440-09-7
Selenium
ND mg/kg
1.2
1
05/12/11 15:15
05/15/11 21:01
7782-49-2
Silver
ND mg/kg
0.62
1
05/12/11 15:15
05/14/11 15:06
7440-22-4
Sodium
ND mg/kg
616
1
05/12/11 15:15
05/14/11 15:06
7440-23-5
Thallium
ND mg/kg
1.2
1
05/12/11 15:15
05/14/11 15:06
7440-28-0
Vanadium
27.1 mg/kg
0.62
1
05/12/11 15:15
05/14/11 15:06
7440-62-2
Zinc
17.7 mg/kg
1.2
1
05/12/11 15:15
05/14/11 15:06
7440-66-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.092 mg/kg
0.0065
1
05/13/11 08:45
05/13/11 16:04
7439-97-6
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
83-32-9
Acenaphthylene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
208-96-8
Aniline
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
62-53-3
Anthracene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
120-12-7
Benzo(a)anthracene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
56-55-3
Benzo(a)pyrene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
50-32-8
Benzo(b)fluoranthene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
191-24-2
Benzo(k)fluoranthene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
207-08-9
Benzoic Acid
ND ug/kg
2360
1
05/14/11 10:32
05/17/11 14:58
65-85-0
Benzyl alcohol
ND ug/kg
943
1
05/14/11 10:32
05/17/11 14:58
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
101-55-3
Butylbenzylphthalate
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
85-68-7
4-Chloro-3-methylphenol
ND ug/kg
943
1
05/14/11 10:32
05/17/11 14:58
59-50-7
4-Chloroaniline
ND ug/kg
2360
1
05/14/11 10:32
05/17/11 14:58
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
108-60-1
2-Chloronaphthalene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
91-58-7
2-Chlorophenol
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
7005-72-3
Chrysene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
218-01-9
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 78 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-24 Lab ID: 9293679024 Collected: 05/05/11 15:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
53-70-3
Dibenzofuran
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
132-64-9
1,2-Dichlorobenzene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
95-50-1
1,3-Dichlorobenzene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
541-73-1
1,4-Dichlorobenzene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
2360
1
05/14/11 10:32
05/17/11 14:58
91-94-1
2,4-Dichlorophenol
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
120-83-2
Diethylphthalate
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
84-66-2
2,4-Dimethylphenol
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
105-67-9
Dimethylphthalate
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
131-11-3
Di-n-butylphthalate
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/kg
943
1
05/14/11 10:32
05/17/11 14:58
534-52-1
2,4-Dinitrophenol
ND ug/kg
2360
1
05/14/11 10:32
05/17/11 14:58
51-28-5
2,4-Dinitrotoluene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
121-14-2
2,6-Dinitrotoluene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
606-20-2
Di-n-octylphthalate
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
117-81-7
Fluoranthene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
206-44-0
Fluorene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
87-68-3
Hexachlorobenzene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
77-47-4
Hexachloroethane
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
193-39-5
Isophorone
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
78-59-1
1-Methylnaphthalene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
90-12-0
2-Methylnaphthalene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
Naphthalene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
91-20-3
2-Nitroaniline
ND ug/kg
2360
1
05/14/11 10:32
05/17/11 14:58
88-74-4
3-Nitroaniline
ND ug/kg
2360
1
05/14/11 10:32
05/17/11 14:58
99-09-2
4-Nitroaniline
ND ug/kg
943
1
05/14/11 10:32
05/17/11 14:58
100-01-6
Nitrobenzene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
98-95-3
2-Nitrophenol
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
88-75-5
4-Nitrophenol
ND ug/kg
2360
1
05/14/11 10:32
05/17/11 14:58
100-02-7
N-Nitrosodimethylamine
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
86-30-6
Pentachlorophenol
ND ug/kg
2360
1
05/14/11 10:32
05/17/11 14:58
87-86-5
Phenanthrene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
85-01-8
Phenol
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
108-95-2
Pyrene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
471
1
05/14/11 10:32
05/17/11 14:58
88-06-2
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY
ANALYSIS
This report
shall not be reproduced, except
in
full,
without the written consent of Analytical Services, Inc..
PPace
Page 79 of 227

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-24 Lab ID: 9293679024 Collected: 05/05/11 15:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)
68 %
23-110
1
05/14/11 10:32
05/17/11 14:58
4165-60-0
2-Fluorobiphenyl (S)
74 %
30-110
1
05/14/11 10:32
05/17/11 14:58
321-60-8
Terphenyl-d14 (S)
77 %
28-110
1
05/14/11 10:32
05/17/11 14:58
1718-51-0
Phenol-d6 (S)
55 %
22-110
1
05/14/11 10:32
05/17/11 14:58
13127-88-3
2-Fluorophenol (S)
63 %
13-110
1
05/14/11 10:32
05/17/11 14:58
367-12-4
2,4,6-Tribromophenol (S)
53 %
27-110
1
05/14/11 10:32
05/17/11 14:58
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND ug/kg
107
1
05/10/11 22:49
67-64-1
Benzene
ND ug/kg
5.3
1
05/10/11 22:49
71-43-2
Bromobenzene
ND ug/kg
5.3
1
05/10/11 22:49
108-86-1
Bromochloromethane
ND ug/kg
5.3
1
05/10/11 22:49
74-97-5
Bromodichloromethane
ND ug/kg
5.3
1
05/10/11 22:49
75-27-4
Bromoform
ND ug/kg
5.3
1
05/10/11 22:49
75-25-2
Bromomethane
ND ug/kg
10.7
1
05/10/11 22:49
74-83-9
2-Butanone (MEK)
ND ug/kg
107
1
05/10/11 22:49
78-93-3
n-Butylbenzene
ND ug/kg
5.3
1
05/10/11 22:49
104-51-8
sec -Butyl benzene
ND ug/kg
5.3
1
05/10/11 22:49
135-98-8
tert-Butyl benzene
ND ug/kg
5.3
1
05/10/11 22:49
98-06-6
Carbon tetrachloride
ND ug/kg
5.3
1
05/10/11 22:49
56-23-5
Chlorobenzene
ND ug/kg
5.3
1
05/10/11 22:49
108-90-7
Chloroethane
ND ug/kg
10.7
1
05/10/11 22:49
75-00-3
Chloroform
ND ug/kg
5.3
1
05/10/11 22:49
67-66-3
Chloromethane
ND ug/kg
10.7
1
05/10/11 22:49
74-87-3
2-Chlorotoluene
ND ug/kg
5.3
1
05/10/11 22:49
95-49-8
4-Chlorotoluene
ND ug/kg
5.3
1
05/10/11 22:49
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
5.3
1
05/10/11 22:49
96-12-8
Dibromochloromethane
ND ug/kg
5.3
1
05/10/11 22:49
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
5.3
1
05/10/11 22:49
106-93-4
Dibromomethane
ND ug/kg
5.3
1
05/10/11 22:49
74-95-3
1,2-Dichlorobenzene
ND ug/kg
5.3
1
05/10/11 22:49
95-50-1
1,3-Dichlorobenzene
ND ug/kg
5.3
1
05/10/11 22:49
541-73-1
1,4-Dichlorobenzene
ND ug/kg
5.3
1
05/10/11 22:49
106-46-7
Dichlorodifluoromethane
ND ug/kg
10.7
1
05/10/11 22:49
75-71-8
1,1-Dichloroethane
ND ug/kg
5.3
1
05/10/11 22:49
75-34-3
1,2-Dichloroethane
ND ug/kg
5.3
1
05/10/11 22:49
107-06-2
1,1-Dichloroethene
ND ug/kg
5.3
1
05/10/11 22:49
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
5.3
1
05/10/11 22:49
156-59-2
trans- 1,2-Dichloroethene
ND ug/kg
5.3
1
05/10/11 22:49
156-60-5
1,2-Dichloropropane
ND ug/kg
5.3
1
05/10/11 22:49
78-87-5
1,3-Dichloropropane
ND ug/kg
5.3
1
05/10/11 22:49
142-28-9
2,2-Dichloropropane
ND ug/kg
5.3
1
05/10/11 22:49
594-20-7
1,1-Dichloropropene
ND ug/kg
5.3
1
05/10/11 22:49
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
5.3
1
05/10/11 22:49
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
5.3
1
05/10/11 22:49
10061-02-6
Diisopropyl ether
ND ug/kg
5.3
1
05/10/11 22:49
108-20-3
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 80 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-24 Lab ID: 9293679024 Collected: 05/05/11 15:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene
ND ug/kg
5.3
1
05/10/11 22:49
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
5.3
1
05/10/11 22:49
87-68-3
2-Hexanone
ND ug/kg
53.4
1
05/10/11 22:49
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
5.3
1
05/10/11 22:49
98-82-8
p-Isopropyltoluene
ND ug/kg
5.3
1
05/10/11 22:49
99-87-6
Methylene Chloride
ND ug/kg
21.4
1
05/10/11 22:49
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
53.4
1
05/10/11 22:49
108-10-1
Methyl-tert-butyl ether
ND ug/kg
5.3
1
05/10/11 22:49
1634-04-4
Naphthalene
ND ug/kg
5.3
1
05/10/11 22:49
91-20-3
n-Propylbenzene
ND ug/kg
5.3
1
05/10/11 22:49
103-65-1
Styrene
ND ug/kg
5.3
1
05/10/11 22:49
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
5.3
1
05/10/11 22:49
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
5.3
1
05/10/11 22:49
79-34-5
Tetrachloroethene
ND ug/kg
5.3
1
05/10/11 22:49
127-18-4
Toluene
ND ug/kg
5.3
1
05/10/11 22:49
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
5.3
1
05/10/11 22:49
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
5.3
1
05/10/11 22:49
120-82-1
1,1,1-Trichloroethane
ND ug/kg
5.3
1
05/10/11 22:49
71-55-6
1,1,2-Trichloroethane
ND ug/kg
5.3
1
05/10/11 22:49
79-00-5
Trichloroethene
ND ug/kg
5.3
1
05/10/11 22:49
79-01-6
Trichlorofluoromethane
ND ug/kg
5.3
1
05/10/11 22:49
75-69-4
1,2,3-Trichloropropane
ND ug/kg
5.3
1
05/10/11 22:49
96-18-4
1,2,4-Trimethylbenzene
ND ug/kg
5.3
1
05/10/11 22:49
95-63-6
1,3,5-Trimethylbenzene
ND ug/kg
5.3
1
05/10/11 22:49
108-67-8
Vinyl acetate
ND ug/kg
53.4
1
05/10/11 22:49
108-05-4
Vinyl chloride
ND ug/kg
10.7
1
05/10/11 22:49
75-01-4
Xylene (Total)
ND ug/kg
10.7
1
05/10/11 22:49
1330-20-7
m&p-Xylene
ND ug/kg
10.7
1
05/10/11 22:49
179601-23-1
o-Xylene
ND ug/kg
5.3
1
05/10/11 22:49
95-47-6
Dibromofluoromethane (S)
104 %
70-130
1
05/10/11 22:49
1868-53-7
Toluene-d8 (S)
99 %
70-130
1
05/10/11 22:49
2037-26-5
4-Bromofluorobenzene (S)
99 %
70-130
1
05/10/11 22:49
460-00-4
1,2-Dichloroethane-d4 (S)
89 %
70-132
1
05/10/11 22:49
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
30.0 %
0.10
1
05/11/11 14:54
Sample: MW-25 Lab ID: 9293679025 Collected: 05/05/11 15:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum 14500 mg/kg 96.8 10 05/12/11 15:15 05/16/11 11:52 7429-90-5
Antimony 1.5 mg/kg 0.48 1 05/12/11 15:15 05/14/11 15:11 7440-36-0
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 81 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-25 Lab ID: 9293679025 Collected: 05/05/11 15:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
5.1 mg/kg
0.48
1
05/12/11 15:15
05/15/11 21:05
7440-38-2
Barium
92.1 mg/kg
0.48
1
05/12/11 15:15
05/14/11 15:11
7440-39-3
Beryllium
0.61 mg/kg
0.097
1
05/12/11 15:15
05/14/11 15:11
7440-41-7
Cadmium
1.4 mg/kg
0.097
1
05/12/11 15:15
05/14/11 15:11
7440-43-9
Calcium
1660 mg/kg
9.7
1
05/12/11 15:15
05/14/11 15:11
7440-70-2
Chromium
48.2 mg/kg
0.48
1
05/12/11 15:15
05/14/11 15:11
7440-47-3
Cobalt
8.3 mg/kg
0.48
1
05/12/11 15:15
05/14/11 15:11
7440-48-4
Copper
19.3 mg/kg
0.48
1
05/12/11 15:15
05/14/11 15:11
7440-50-8
Iron
27800 mg/kg
48.4
10
05/12/11 15:15
05/16/11 11:52
7439-89-6
Lead
41.9 mg/kg
0.48
1
05/12/11 15:15
05/14/11 15:11
7439-92-1
Magnesium
1720 mg/kg
9.7
1
05/12/11 15:15
05/14/11 15:11
7439-95-4
Manganese
353 mg/kg
0.48
1
05/12/11 15:15
05/14/11 15:11
7439-96-5
Nickel
9.3 mg/kg
0.48
1
05/12/11 15:15
05/14/11 15:11
7440-02-0
Potassium
1860 mg/kg
484
1
05/12/11 15:15
05/14/11 15:11
7440-09-7
Selenium
1.5 mg/kg
0.97
1
05/12/11 15:15
05/15/11 21:05
7782-49-2
Silver
ND mg/kg
0.48
1
05/12/11 15:15
05/14/11 15:11
7440-22-4
Sodium
ND mg/kg
484
1
05/12/11 15:15
05/14/11 15:11
7440-23-5
Thallium
ND mg/kg
0.97
1
05/12/11 15:15
05/14/11 15:11
7440-28-0
Vanadium
38.9 mg/kg
0.48
1
05/12/11 15:15
05/14/11 15:11
7440-62-2
Zinc
206 mg/kg
0.97
1
05/12/11 15:15
05/14/11 15:11
7440-66-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.59 mg/kg
0.041
10
05/13/11 08:45
05/16/11 13:32
7439-97-6
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
83-32-9
Acenaphthylene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
208-96-8
Aniline
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
62-53-3
Anthracene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
120-12-7
Benzo(a)anthracene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
56-55-3
Benzo(a)pyrene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
50-32-8
Benzo(b)fluoranthene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
191-24-2
Benzo(k)fluoranthene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
207-08-9
Benzoic Acid
ND ug/kg
1980
1
05/14/11 10:32
05/17/11 15:26
65-85-0
Benzyl alcohol
ND ug/kg
792
1
05/14/11 10:32
05/17/11 15:26
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
101-55-3
Butylbenzylphthalate
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
85-68-7
4-Chloro-3-methylphenol
ND ug/kg
792
1
05/14/11 10:32
05/17/11 15:26
59-50-7
4-Chloroaniline
ND ug/kg
1980
1
05/14/11 10:32
05/17/11 15:26
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
108-60-1
2-Chloronaphthalene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
91-58-7
2-Chlorophenol
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
95-57-8
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 82 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-25 Lab ID: 9293679025 Collected: 05/05/11 15:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
4-Chlorophenylphenyl ether
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
7005-72-3
Chrysene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
53-70-3
Dibenzofuran
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
132-64-9
1,2-Dichlorobenzene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
95-50-1
1,3-Dichlorobenzene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
541-73-1
1,4-Dichlorobenzene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
1980
1
05/14/11 10:32
05/17/11 15:26
91-94-1
2,4-Dichlorophenol
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
120-83-2
Diethylphthalate
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
84-66-2
2,4-Dimethylphenol
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
105-67-9
Dimethylphthalate
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
131-11-3
Di-n-butylphthalate
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/kg
792
1
05/14/11 10:32
05/17/11 15:26
534-52-1
2,4-Dinitrophenol
ND ug/kg
1980
1
05/14/11 10:32
05/17/11 15:26
51-28-5
2,4-Dinitrotoluene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
121-14-2
2,6-Dinitrotoluene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
606-20-2
Di-n-octylphthalate
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
117-81-7
Fluoranthene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
206-44-0
Fluorene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
87-68-3
Hexachlorobenzene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
77-47-4
Hexachloroethane
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
193-39-5
Isophorone
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
78-59-1
1-Methylnaphthalene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
90-12-0
2-Methylnaphthalene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
Naphthalene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
91-20-3
2-Nitroaniline
ND ug/kg
1980
1
05/14/11 10:32
05/17/11 15:26
88-74-4
3-Nitroaniline
ND ug/kg
1980
1
05/14/11 10:32
05/17/11 15:26
99-09-2
4-Nitroaniline
ND ug/kg
792
1
05/14/11 10:32
05/17/11 15:26
100-01-6
Nitrobenzene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
98-95-3
2-Nitrophenol
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
88-75-5
4-Nitrophenol
ND ug/kg
1980
1
05/14/11 10:32
05/17/11 15:26
100-02-7
N-Nitrosodimethylamine
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
86-30-6
Pentachlorophenol
ND ug/kg
1980
1
05/14/11 10:32
05/17/11 15:26
87-86-5
Phenanthrene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
85-01-8
Phenol
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
108-95-2
Pyrene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
120-82-1
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 83 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-25 Lab ID: 9293679025 Collected: 05/05/11 15:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4,5-Trichlorophenol
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
396
1
05/14/11 10:32
05/17/11 15:26
88-06-2
Nitrobenzene-d5 (S)
45 %
23-110
1
05/14/11 10:32
05/17/11 15:26
4165-60-0
2-Fluorobiphenyl (S)
47 %
30-110
1
05/14/11 10:32
05/17/11 15:26
321-60-8
Terphenyl-d14 (S)
56 %
28-110
1
05/14/11 10:32
05/17/11 15:26
1718-51-0
Phenol-d6 (S)
32 %
22-110
1
05/14/11 10:32
05/17/11 15:26
13127-88-3
2-Fluorophenol (S)
34 %
13-110
1
05/14/11 10:32
05/17/11 15:26
367-12-4
2,4,6-Tribromophenol (S)
33 %
27-110
1
05/14/11 10:32
05/17/11 15:26
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND ug/kg
83.2
1
05/10/11 23:09
67-64-1
Benzene
ND ug/kg
4.2
1
05/10/11 23:09
71-43-2
Bromobenzene
ND ug/kg
4.2
1
05/10/11 23:09
108-86-1
Bromochloromethane
ND ug/kg
4.2
1
05/10/11 23:09
74-97-5
Bromodichloromethane
ND ug/kg
4.2
1
05/10/11 23:09
75-27-4
Bromoform
ND ug/kg
4.2
1
05/10/11 23:09
75-25-2
Bromomethane
ND ug/kg
8.3
1
05/10/11 23:09
74-83-9
2-Butanone (MEK)
ND ug/kg
83.2
1
05/10/11 23:09
78-93-3
n-Butylbenzene
ND ug/kg
4.2
1
05/10/11 23:09
104-51-8
sec -Butyl benzene
ND ug/kg
4.2
1
05/10/11 23:09
135-98-8
tert-Butyl benzene
ND ug/kg
4.2
1
05/10/11 23:09
98-06-6
Carbon tetrachloride
ND ug/kg
4.2
1
05/10/11 23:09
56-23-5
Chlorobenzene
ND ug/kg
4.2
1
05/10/11 23:09
108-90-7
Chloroethane
ND ug/kg
8.3
1
05/10/11 23:09
75-00-3
Chloroform
ND ug/kg
4.2
1
05/10/11 23:09
67-66-3
Chloromethane
ND ug/kg
8.3
1
05/10/11 23:09
74-87-3
2-Chlorotoluene
ND ug/kg
4.2
1
05/10/11 23:09
95-49-8
4-Chlorotoluene
ND ug/kg
4.2
1
05/10/11 23:09
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
4.2
1
05/10/11 23:09
96-12-8
Dibromochloromethane
ND ug/kg
4.2
1
05/10/11 23:09
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
4.2
1
05/10/11 23:09
106-93-4
Dibromomethane
ND ug/kg
4.2
1
05/10/11 23:09
74-95-3
1,2-Dichlorobenzene
ND ug/kg
4.2
1
05/10/11 23:09
95-50-1
1,3-Dichlorobenzene
ND ug/kg
4.2
1
05/10/11 23:09
541-73-1
1,4-Dichlorobenzene
ND ug/kg
4.2
1
05/10/11 23:09
106-46-7
Dichlorodifluoromethane
ND ug/kg
8.3
1
05/10/11 23:09
75-71-8
1,1-Dichloroethane
ND ug/kg
4.2
1
05/10/11 23:09
75-34-3
1,2-Dichloroethane
ND ug/kg
4.2
1
05/10/11 23:09
107-06-2
1,1-Dichloroethene
ND ug/kg
4.2
1
05/10/11 23:09
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
4.2
1
05/10/11 23:09
156-59-2
trans- 1,2-Dichloroethene
ND ug/kg
4.2
1
05/10/11 23:09
156-60-5
1,2-Dichloropropane
ND ug/kg
4.2
1
05/10/11 23:09
78-87-5
1,3-Dichloropropane
ND ug/kg
4.2
1
05/10/11 23:09
142-28-9
2,2-Dichloropropane
ND ug/kg
4.2
1
05/10/11 23:09
594-20-7
1,1-Dichloropropene
ND ug/kg
4.2
1
05/10/11 23:09
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
4.2
1
05/10/11 23:09
10061-01-5
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 84 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-25 Lab ID: 9293679025 Collected: 05/05/11 15:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1, 2-Tetrach loroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1, 3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Dibromofluoromethane (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 05/20/2011 04:57 PM
ND ug/kg
4.2
1
05/10/11 23:09
10061-02-6
ND ug/kg
4.2
1
05/10/11 23:09
108-20-3
ND ug/kg
4.2
1
05/10/11 23:09
100-41-4
ND ug/kg
4.2
1
05/10/11 23:09
87-68-3
ND ug/kg
41.6
1
05/10/11 23:09
591-78-6
ND ug/kg
4.2
1
05/10/11 23:09
98-82-8
ND ug/kg
4.2
1
05/10/11 23:09
99-87-6
ND ug/kg
16.6
1
05/10/11 23:09
75-09-2
ND ug/kg
41.6
1
05/10/11 23:09
108-10-1
ND ug/kg
4.2
1
05/10/11 23:09
1634-04-4
ND ug/kg
4.2
1
05/10/11 23:09
91-20-3
ND ug/kg
4.2
1
05/10/11 23:09
103-65-1
ND ug/kg
4.2
1
05/10/11 23:09
100-42-5
ND ug/kg
4.2
1
05/10/11 23:09
630-20-6
ND ug/kg
4.2
1
05/10/11 23:09
79-34-5
ND ug/kg
4.2
1
05/10/11 23:09
127-18-4
ND ug/kg
4.2
1
05/10/11 23:09
108-88-3
ND ug/kg
4.2
1
05/10/11 23:09
87-61-6
ND ug/kg
4.2
1
05/10/11 23:09
120-82-1
ND ug/kg
4.2
1
05/10/11 23:09
71-55-6
ND ug/kg
4.2
1
05/10/11 23:09
79-00-5
ND ug/kg
4.2
1
05/10/11 23:09
79-01-6
ND ug/kg
4.2
1
05/10/11 23:09
75-69-4
ND ug/kg
4.2
1
05/10/11 23:09
96-18-4
ND ug/kg
4.2
1
05/10/11 23:09
95-63-6
ND ug/kg
4.2
1
05/10/11 23:09
108-67-8
ND ug/kg
41.6
1
05/10/11 23:09
108-05-4
ND ug/kg
8.3
1
05/10/11 23:09
75-01-4
ND ug/kg
8.3
1
05/10/11 23:09
1330-20-7
ND ug/kg
8.3
1
05/10/11 23:09
179601-23-1
ND ug/kg
4.2
1
05/10/11 23:09
95-47-6
108 %
70-130
1
05/10/11 23:09
1868-53-7
98 %
70-130
1
05/10/11 23:09
2037-26-5
91 %
70-130
1
05/10/11 23:09
460-00-4
93 %
70-132
1
05/10/11 23:09
17060-07-0
Analytical Method: ASTM D2974-87
16.7 %
0.10
1
05/11/11 14:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 85 of 227

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-17 Lab ID: 9293679026 Collected: 05/05/11 16:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
31900 mg/kg
131
10
05/12/11 15:15
05/16/11 11:56
7429-90-5
Antimony
ND mg/kg
0.65
1
05/12/11 15:15
05/14/11 15:15
7440-36-0
Arsenic
2.2 mg/kg
0.65
1
05/12/11 15:15
05/15/11 21:10
7440-38-2
Barium
114 mg/kg
0.65
1
05/12/11 15:15
05/14/11 15:15
7440-39-3
Beryllium
0.68 mg/kg
0.13
1
05/12/11 15:15
05/14/11 15:15
7440-41-7
Cadmium
0.25 mg/kg
0.13
1
05/12/11 15:15
05/14/11 15:15
7440-43-9
Calcium
105 mg/kg
13.1
1
05/12/11 15:15
05/14/11 15:15
7440-70-2
Chromium
21.2 mg/kg
0.65
1
05/12/11 15:15
05/14/11 15:15
7440-47-3
Cobalt
ND mg/kg
0.65
1
05/12/11 15:15
05/14/11 15:15
7440-48-4
Copper
28.0 mg/kg
0.65
1
05/12/11 15:15
05/14/11 15:15
7440-50-8
Iron
11600 mg/kg
6.5
1
05/12/11 15:15
05/14/11 15:15
7439-89-6
Lead
11.9 mg/kg
0.65
1
05/12/11 15:15
05/14/11 15:15
7439-92-1
Magnesium
2750 mg/kg
13.1
1
05/12/11 15:15
05/14/11 15:15
7439-95-4
Manganese
56.7 mg/kg
0.65
1
05/12/11 15:15
05/14/11 15:15
7439-96-5
Nickel
15.3 mg/kg
0.65
1
05/12/11 15:15
05/14/11 15:15
7440-02-0
Potassium
2810 mg/kg
654
1
05/12/11 15:15
05/14/11 15:15
7440-09-7
Selenium
1.4 mg/kg
1.3
1
05/12/11 15:15
05/15/11 21:10
7782-49-2
Silver
ND mg/kg
0.65
1
05/12/11 15:15
05/14/11 15:15
7440-22-4
Sodium
ND mg/kg
654
1
05/12/11 15:15
05/14/11 15:15
7440-23-5
Thallium
ND mg/kg
1.3
1
05/12/11 15:15
05/14/11 15:15
7440-28-0
Vanadium
47.2 mg/kg
0.65
1
05/12/11 15:15
05/14/11 15:15
7440-62-2
Zinc
48.9 mg/kg
1.3
1
05/12/11 15:15
05/14/11 15:15
7440-66-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.033 mg/kg
0.0052
1
05/13/11 08:45
05/13/11 16:17
7439-97-6
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
83-32-9
Acenaphthylene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
208-96-8
Aniline
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
62-53-3
Anthracene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
120-12-7
Benzo(a)anthracene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
56-55-3
Benzo(a)pyrene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
50-32-8
Benzo(b)fluoranthene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
191-24-2
Benzo(k)fluoranthene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
207-08-9
Benzoic Acid
ND ug/kg
2160
1
05/14/11 10:32
05/17/11 15:53
65-85-0
Benzyl alcohol
ND ug/kg
864
1
05/14/11 10:32
05/17/11 15:53
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
101-55-3
Butylbenzylphthalate
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
85-68-7
4-Chloro-3-methylphenol
ND ug/kg
864
1
05/14/11 10:32
05/17/11 15:53
59-50-7
4-Chloroaniline
ND ug/kg
2160
1
05/14/11 10:32
05/17/11 15:53
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
108-60-1
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 86 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-17 Lab ID: 9293679026 Collected: 05/05/11 16:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Chloronaphthalene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
91-58-7
2-Chlorophenol
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
7005-72-3
Chrysene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
53-70-3
Dibenzofuran
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
132-64-9
1,2-Dichlorobenzene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
95-50-1
1,3-Dichlorobenzene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
541-73-1
1,4-Dichlorobenzene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
2160
1
05/14/11 10:32
05/17/11 15:53
91-94-1
2,4-Dichlorophenol
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
120-83-2
Diethylphthalate
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
84-66-2
2,4-Dimethylphenol
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
105-67-9
Dimethylphthalate
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
131-11-3
Di-n-butylphthalate
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/kg
864
1
05/14/11 10:32
05/17/11 15:53
534-52-1
2,4-Dinitrophenol
ND ug/kg
2160
1
05/14/11 10:32
05/17/11 15:53
51-28-5
2,4-Dinitrotoluene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
121-14-2
2,6-Dinitrotoluene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
606-20-2
Di-n-octylphthalate
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
117-81-7
Fluoranthene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
206-44-0
Fluorene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
87-68-3
Hexachlorobenzene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
77-47-4
Hexachloroethane
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
193-39-5
Isophorone
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
78-59-1
1-Methylnaphthalene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
90-12-0
2-Methylnaphthalene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
Naphthalene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
91-20-3
2-Nitroaniline
ND ug/kg
2160
1
05/14/11 10:32
05/17/11 15:53
88-74-4
3-Nitroaniline
ND ug/kg
2160
1
05/14/11 10:32
05/17/11 15:53
99-09-2
4-Nitroaniline
ND ug/kg
864
1
05/14/11 10:32
05/17/11 15:53
100-01-6
Nitrobenzene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
98-95-3
2-Nitrophenol
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
88-75-5
4-Nitrophenol
ND ug/kg
2160
1
05/14/11 10:32
05/17/11 15:53
100-02-7
N-Nitrosodimethylamine
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
86-30-6
Pentachlorophenol
ND ug/kg
2160
1
05/14/11 10:32
05/17/11 15:53
87-86-5
Phenanthrene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
85-01-8
Phenol
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
108-95-2
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 87 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-17 Lab ID: 9293679026 Collected: 05/05/11 16:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Pyrene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
432
1
05/14/11 10:32
05/17/11 15:53
88-06-2
Nitrobenzene-d5 (S)
61 %
23-110
1
05/14/11 10:32
05/17/11 15:53
4165-60-0
2-Fluorobiphenyl (S)
67 %
30-110
1
05/14/11 10:32
05/17/11 15:53
321-60-8
Terphenyl-d14 (S)
76 %
28-110
1
05/14/11 10:32
05/17/11 15:53
1718-51-0
Phenol-d6 (S)
51 %
22-110
1
05/14/11 10:32
05/17/11 15:53
13127-88-3
2-Fluorophenol (S)
55 %
13-110
1
05/14/11 10:32
05/17/11 15:53
367-12-4
2,4,6-Tribromophenol (S)
48 %
27-110
1
05/14/11 10:32
05/17/11 15:53
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND ug/kg
53.5
1
05/11/11 19:17
67-64-1
Benzene
ND ug/kg
2.7
1
05/11/11 19:17
71-43-2
Bromobenzene
ND ug/kg
2.7
1
05/11/11 19:17
108-86-1
Bromochloromethane
ND ug/kg
2.7
1
05/11/11 19:17
74-97-5
Bromodichloromethane
ND ug/kg
2.7
1
05/11/11 19:17
75-27-4
Bromoform
ND ug/kg
2.7
1
05/11/11 19:17
75-25-2
Bromomethane
ND ug/kg
5.3
1
05/11/11 19:17
74-83-9
2-Butanone (MEK)
ND ug/kg
53.5
1
05/11/11 19:17
78-93-3
n-Butylbenzene
ND ug/kg
2.7
1
05/11/11 19:17
104-51-8
sec -Butyl benzene
ND ug/kg
2.7
1
05/11/11 19:17
135-98-8
tert-Butyl benzene
ND ug/kg
2.7
1
05/11/11 19:17
98-06-6
Carbon tetrachloride
ND ug/kg
2.7
1
05/11/11 19:17
56-23-5
Chlorobenzene
ND ug/kg
2.7
1
05/11/11 19:17
108-90-7
Chloroethane
ND ug/kg
5.3
1
05/11/11 19:17
75-00-3
Chloroform
ND ug/kg
2.7
1
05/11/11 19:17
67-66-3
Chloromethane
ND ug/kg
5.3
1
05/11/11 19:17
74-87-3
2-Chlorotoluene
ND ug/kg
2.7
1
05/11/11 19:17
95-49-8
4-Chlorotoluene
ND ug/kg
2.7
1
05/11/11 19:17
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
2.7
1
05/11/11 19:17
96-12-8
Dibromochloromethane
ND ug/kg
2.7
1
05/11/11 19:17
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
2.7
1
05/11/11 19:17
106-93-4
Dibromomethane
ND ug/kg
2.7
1
05/11/11 19:17
74-95-3
1,2-Dichlorobenzene
ND ug/kg
2.7
1
05/11/11 19:17
95-50-1
1,3-Dichlorobenzene
ND ug/kg
2.7
1
05/11/11 19:17
541-73-1
1,4-Dichlorobenzene
ND ug/kg
2.7
1
05/11/11 19:17
106-46-7
Dichlorodifluoromethane
ND ug/kg
5.3
1
05/11/11 19:17
75-71-8
1,1-Dichloroethane
ND ug/kg
2.7
1
05/11/11 19:17
75-34-3
1,2-Dichloroethane
ND ug/kg
2.7
1
05/11/11 19:17
107-06-2
1,1-Dichloroethene
ND ug/kg
2.7
1
05/11/11 19:17
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
2.7
1
05/11/11 19:17
156-59-2
trans- 1,2-Dichloroethene
ND ug/kg
2.7
1
05/11/11 19:17
156-60-5
1,2-Dichloropropane
ND ug/kg
2.7
1
05/11/11 19:17
78-87-5
1,3-Dichloropropane
ND ug/kg
2.7
1
05/11/11 19:17
142-28-9
2,2-Dichloropropane
ND ug/kg
2.7
1
05/11/11 19:17
594-20-7
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY
ANALYSIS
Page 88 of 227
This report shall not be reproduced, except
in
full,
without the written consent of Pace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-17 Lab ID: 9293679026 Collected: 05/05/11 16:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1-Dichloropropene
ND ug/kg
2.7
1
05/11/11 19:17
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
2.7
1
05/11/11 19:17
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
2.7
1
05/11/11 19:17
10061-02-6
Diisopropyl ether
ND ug/kg
2.7
1
05/11/11 19:17
108-20-3
Ethylbenzene
ND ug/kg
2.7
1
05/11/11 19:17
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
2.7
1
05/11/11 19:17
87-68-3
2-Hexanone
ND ug/kg
26.7
1
05/11/11 19:17
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
2.7
1
05/11/11 19:17
98-82-8
p-Isopropyltoluene
ND ug/kg
2.7
1
05/11/11 19:17
99-87-6
Methylene Chloride
ND ug/kg
10.7
1
05/11/11 19:17
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
26.7
1
05/11/11 19:17
108-10-1
Methyl-tert-butyl ether
ND ug/kg
2.7
1
05/11/11 19:17
1634-04-4
Naphthalene
ND ug/kg
2.7
1
05/11/11 19:17
91-20-3
n-Propylbenzene
ND ug/kg
2.7
1
05/11/11 19:17
103-65-1
Styrene
ND ug/kg
2.7
1
05/11/11 19:17
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
2.7
1
05/11/11 19:17
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
2.7
1
05/11/11 19:17
79-34-5
Tetrachloroethene
ND ug/kg
2.7
1
05/11/11 19:17
127-18-4
Toluene
ND ug/kg
2.7
1
05/11/11 19:17
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
2.7
1
05/11/11 19:17
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
2.7
1
05/11/11 19:17
120-82-1
1,1,1-Trichloroethane
ND ug/kg
2.7
1
05/11/11 19:17
71-55-6
1,1,2-Trichloroethane
ND ug/kg
2.7
1
05/11/11 19:17
79-00-5
Trichloroethene
ND ug/kg
2.7
1
05/11/11 19:17
79-01-6
Trichlorofluoromethane
ND ug/kg
2.7
1
05/11/11 19:17
75-69-4
1,2,3-Trichloropropane
ND ug/kg
2.7
1
05/11/11 19:17
96-18-4
1,2,4-Trimethylbenzene
ND ug/kg
2.7
1
05/11/11 19:17
95-63-6
1,3,5-Trimethylbenzene
ND ug/kg
2.7
1
05/11/11 19:17
108-67-8
Vinyl acetate
ND ug/kg
26.7
1
05/11/11 19:17
108-05-4
Vinyl chloride
ND ug/kg
5.3
1
05/11/11 19:17
75-01-4
Xylene (Total)
ND ug/kg
5.3
1
05/11/11 19:17
1330-20-7
m&p-Xylene
ND ug/kg
5.3
1
05/11/11 19:17
179601-23-1
o-Xylene
ND ug/kg
2.7
1
05/11/11 19:17
95-47-6
Dibromofluoromethane (S)
103 %
70-130
1
05/11/11 19:17
1868-53-7
Toluene-d8 (S)
102 %
70-130
1
05/11/11 19:17
2037-26-5
4-Bromofluorobenzene (S)
94 %
70-130
1
05/11/11 19:17
460-00-4
1,2-Dichloroethane-d4 (S)
97 %
70-132
1
05/11/11 19:17
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
23.6 %
0.10
1
05/11/11 18:41
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 89 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-16 Lab ID: 9293679027 Collected: 05/06/11 08:10 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
13800 mg/kg
106
10
05/12/11 15:15
05/16/11 12:00
7429-90-5
Antimony
ND mg/kg
0.53
1
05/12/11 15:15
05/14/11 15:20
7440-36-0
Arsenic
0.92 mg/kg
0.53
1
05/12/11 15:15
05/15/11 21:17
7440-38-2
Barium
66.7 mg/kg
0.53
1
05/12/11 15:15
05/14/11 15:20
7440-39-3
Beryllium
0.43 mg/kg
0.11
1
05/12/11 15:15
05/14/11 15:20
7440-41-7
Cadmium
ND mg/kg
0.11
1
05/12/11 15:15
05/14/11 15:20
7440-43-9
Calcium
75.1 mg/kg
10.6
1
05/12/11 15:15
05/14/11 15:20
7440-70-2
Chromium
13.6 mg/kg
0.53
1
05/12/11 15:15
05/14/11 15:20
7440-47-3
Cobalt
9.8 mg/kg
0.53
1
05/12/11 15:15
05/14/11 15:20
7440-48-4
Copper
11.4 mg/kg
0.53
1
05/12/11 15:15
05/14/11 15:20
7440-50-8
Iron
8760 mg/kg
5.3
1
05/12/11 15:15
05/14/11 15:20
7439-89-6
Lead
6.8 mg/kg
0.53
1
05/12/11 15:15
05/14/11 15:20
7439-92-1
Magnesium
1190 mg/kg
10.6
1
05/12/11 15:15
05/14/11 15:20
7439-95-4
Manganese
141 mg/kg
0.53
1
05/12/11 15:15
05/14/11 15:20
7439-96-5
Nickel
8.7 mg/kg
0.53
1
05/12/11 15:15
05/14/11 15:20
7440-02-0
Potassium
1140 mg/kg
529
1
05/12/11 15:15
05/14/11 15:20
7440-09-7
Selenium
1.6 mg/kg
1.1
1
05/12/11 15:15
05/15/11 21:17
7782-49-2
Silver
ND mg/kg
0.53
1
05/12/11 15:15
05/14/11 15:20
7440-22-4
Sodium
ND mg/kg
529
1
05/12/11 15:15
05/14/11 15:20
7440-23-5
Thallium
ND mg/kg
1.1
1
05/12/11 15:15
05/14/11 15:20
7440-28-0
Vanadium
25.2 mg/kg
0.53
1
05/12/11 15:15
05/14/11 15:20
7440-62-2
Zinc
18.8 mg/kg
1.1
1
05/12/11 15:15
05/14/11 15:20
7440-66-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.040 mg/kg
0.0039
1
05/13/11 08:45
05/13/11 16:20
7439-97-6
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
83-32-9
Acenaphthylene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
208-96-8
Aniline
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
62-53-3
Anthracene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
120-12-7
Benzo(a)anthracene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
56-55-3
Benzo(a)pyrene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
50-32-8
Benzo(b)fluoranthene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
191-24-2
Benzo(k)fluoranthene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
207-08-9
Benzoic Acid
ND ug/kg
1960
1
05/14/11 10:32
05/17/11 16:21
65-85-0
Benzyl alcohol
ND ug/kg
782
1
05/14/11 10:32
05/17/11 16:21
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
101-55-3
Butylbenzylphthalate
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
85-68-7
4-Chloro-3-methylphenol
ND ug/kg
782
1
05/14/11 10:32
05/17/11 16:21
59-50-7
4-Chloroaniline
ND ug/kg
1960
1
05/14/11 10:32
05/17/11 16:21
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
108-60-1
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 90 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-16 Lab ID: 9293679027 Collected: 05/06/11 08:10 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Chloronaphthalene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
91-58-7
2-Chlorophenol
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
7005-72-3
Chrysene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
53-70-3
Dibenzofuran
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
132-64-9
1,2-Dichlorobenzene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
95-50-1
1,3-Dichlorobenzene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
541-73-1
1,4-Dichlorobenzene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
1960
1
05/14/11 10:32
05/17/11 16:21
91-94-1
2,4-Dichlorophenol
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
120-83-2
Diethylphthalate
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
84-66-2
2,4-Dimethylphenol
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
105-67-9
Dimethylphthalate
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
131-11-3
Di-n-butylphthalate
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/kg
782
1
05/14/11 10:32
05/17/11 16:21
534-52-1
2,4-Dinitrophenol
ND ug/kg
1960
1
05/14/11 10:32
05/17/11 16:21
51-28-5
2,4-Dinitrotoluene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
121-14-2
2,6-Dinitrotoluene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
606-20-2
Di-n-octylphthalate
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
117-81-7
Fluoranthene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
206-44-0
Fluorene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
87-68-3
Hexachlorobenzene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
77-47-4
Hexachloroethane
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
193-39-5
Isophorone
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
78-59-1
1-Methylnaphthalene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
90-12-0
2-Methylnaphthalene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
Naphthalene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
91-20-3
2-Nitroaniline
ND ug/kg
1960
1
05/14/11 10:32
05/17/11 16:21
88-74-4
3-Nitroaniline
ND ug/kg
1960
1
05/14/11 10:32
05/17/11 16:21
99-09-2
4-Nitroaniline
ND ug/kg
782
1
05/14/11 10:32
05/17/11 16:21
100-01-6
Nitrobenzene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
98-95-3
2-Nitrophenol
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
88-75-5
4-Nitrophenol
ND ug/kg
1960
1
05/14/11 10:32
05/17/11 16:21
100-02-7
N-Nitrosodimethylamine
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
86-30-6
Pentachlorophenol
ND ug/kg
1960
1
05/14/11 10:32
05/17/11 16:21
87-86-5
Phenanthrene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
85-01-8
Phenol
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
108-95-2
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 91 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-16 Lab ID: 9293679027 Collected: 05/06/11 08:10 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Pyrene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
391
1
05/14/11 10:32
05/17/11 16:21
88-06-2
Nitrobenzene-d5 (S)
60 %
23-110
1
05/14/11 10:32
05/17/11 16:21
4165-60-0
2-Fluorobiphenyl (S)
63 %
30-110
1
05/14/11 10:32
05/17/11 16:21
321-60-8
Terphenyl-d14 (S)
64 %
28-110
1
05/14/11 10:32
05/17/11 16:21
1718-51-0
Phenol-d6 (S)
48 %
22-110
1
05/14/11 10:32
05/17/11 16:21
13127-88-3
2-Fluorophenol (S)
54 %
13-110
1
05/14/11 10:32
05/17/11 16:21
367-12-4
2,4,6-Tribromophenol (S)
38 %
27-110
1
05/14/11 10:32
05/17/11 16:21
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND ug/kg
74.3
1
05/11/11 19:37
67-64-1
Benzene
ND ug/kg
3.7
1
05/11/11 19:37
71-43-2
Bromobenzene
ND ug/kg
3.7
1
05/11/11 19:37
108-86-1
Bromochloromethane
ND ug/kg
3.7
1
05/11/11 19:37
74-97-5
Bromodichloromethane
ND ug/kg
3.7
1
05/11/11 19:37
75-27-4
Bromoform
ND ug/kg
3.7
1
05/11/11 19:37
75-25-2
Bromomethane
ND ug/kg
7.4
1
05/11/11 19:37
74-83-9
2-Butanone (MEK)
ND ug/kg
74.3
1
05/11/11 19:37
78-93-3
n-Butylbenzene
ND ug/kg
3.7
1
05/11/11 19:37
104-51-8
sec -Butyl benzene
ND ug/kg
3.7
1
05/11/11 19:37
135-98-8
tert-Butyl benzene
ND ug/kg
3.7
1
05/11/11 19:37
98-06-6
Carbon tetrachloride
ND ug/kg
3.7
1
05/11/11 19:37
56-23-5
Chlorobenzene
ND ug/kg
3.7
1
05/11/11 19:37
108-90-7
Chloroethane
ND ug/kg
7.4
1
05/11/11 19:37
75-00-3
Chloroform
ND ug/kg
3.7
1
05/11/11 19:37
67-66-3
Chloromethane
ND ug/kg
7.4
1
05/11/11 19:37
74-87-3
2-Chlorotoluene
ND ug/kg
3.7
1
05/11/11 19:37
95-49-8
4-Chlorotoluene
ND ug/kg
3.7
1
05/11/11 19:37
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
3.7
1
05/11/11 19:37
96-12-8
Dibromochloromethane
ND ug/kg
3.7
1
05/11/11 19:37
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
3.7
1
05/11/11 19:37
106-93-4
Dibromomethane
ND ug/kg
3.7
1
05/11/11 19:37
74-95-3
1,2-Dichlorobenzene
ND ug/kg
3.7
1
05/11/11 19:37
95-50-1
1,3-Dichlorobenzene
ND ug/kg
3.7
1
05/11/11 19:37
541-73-1
1,4-Dichlorobenzene
ND ug/kg
3.7
1
05/11/11 19:37
106-46-7
Dichlorodifluoromethane
ND ug/kg
7.4
1
05/11/11 19:37
75-71-8
1,1-Dichloroethane
ND ug/kg
3.7
1
05/11/11 19:37
75-34-3
1,2-Dichloroethane
ND ug/kg
3.7
1
05/11/11 19:37
107-06-2
1,1-Dichloroethene
ND ug/kg
3.7
1
05/11/11 19:37
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
3.7
1
05/11/11 19:37
156-59-2
trans- 1,2-Dichloroethene
ND ug/kg
3.7
1
05/11/11 19:37
156-60-5
1,2-Dichloropropane
ND ug/kg
3.7
1
05/11/11 19:37
78-87-5
1,3-Dichloropropane
ND ug/kg
3.7
1
05/11/11 19:37
142-28-9
2,2-Dichloropropane
ND ug/kg
3.7
1
05/11/11 19:37
594-20-7
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY
ANALYSIS
Page 92 of 227
This report shall not be reproduced, except
in
full,
without the written consent of Pace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-16 Lab ID: 9293679027 Collected: 05/06/11 08:10 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1-Dichloropropene
ND ug/kg
3.7
1
05/11/11 19:37
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
3.7
1
05/11/11 19:37
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
3.7
1
05/11/11 19:37
10061-02-6
Diisopropyl ether
ND ug/kg
3.7
1
05/11/11 19:37
108-20-3
Ethylbenzene
ND ug/kg
3.7
1
05/11/11 19:37
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
3.7
1
05/11/11 19:37
87-68-3
2-Hexanone
ND ug/kg
37.1
1
05/11/11 19:37
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
3.7
1
05/11/11 19:37
98-82-8
p-Isopropyltoluene
ND ug/kg
3.7
1
05/11/11 19:37
99-87-6
Methylene Chloride
ND ug/kg
14.9
1
05/11/11 19:37
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
37.1
1
05/11/11 19:37
108-10-1
Methyl-tert-butyl ether
ND ug/kg
3.7
1
05/11/11 19:37
1634-04-4
Naphthalene
ND ug/kg
3.7
1
05/11/11 19:37
91-20-3
n-Propylbenzene
ND ug/kg
3.7
1
05/11/11 19:37
103-65-1
Styrene
ND ug/kg
3.7
1
05/11/11 19:37
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
3.7
1
05/11/11 19:37
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
3.7
1
05/11/11 19:37
79-34-5
Tetrachloroethene
ND ug/kg
3.7
1
05/11/11 19:37
127-18-4
Toluene
ND ug/kg
3.7
1
05/11/11 19:37
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
3.7
1
05/11/11 19:37
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
3.7
1
05/11/11 19:37
120-82-1
1,1,1-Trichloroethane
ND ug/kg
3.7
1
05/11/11 19:37
71-55-6
1,1,2-Trichloroethane
ND ug/kg
3.7
1
05/11/11 19:37
79-00-5
Trichloroethene
ND ug/kg
3.7
1
05/11/11 19:37
79-01-6
Trichlorofluoromethane
ND ug/kg
3.7
1
05/11/11 19:37
75-69-4
1,2,3-Trichloropropane
ND ug/kg
3.7
1
05/11/11 19:37
96-18-4
1,2,4-Trimethylbenzene
ND ug/kg
3.7
1
05/11/11 19:37
95-63-6
1,3,5-Trimethylbenzene
ND ug/kg
3.7
1
05/11/11 19:37
108-67-8
Vinyl acetate
ND ug/kg
37.1
1
05/11/11 19:37
108-05-4
Vinyl chloride
ND ug/kg
7.4
1
05/11/11 19:37
75-01-4
Xylene (Total)
ND ug/kg
7.4
1
05/11/11 19:37
1330-20-7
m&p-Xylene
ND ug/kg
7.4
1
05/11/11 19:37
179601-23-1
o-Xylene
ND ug/kg
3.7
1
05/11/11 19:37
95-47-6
Dibromofluoromethane (S)
104 %
70-130
1
05/11/11 19:37
1868-53-7
Toluene-d8 (S)
98 %
70-130
1
05/11/11 19:37
2037-26-5
4-Bromofluorobenzene (S)
92 %
70-130
1
05/11/11 19:37
460-00-4
1,2-Dichloroethane-d4 (S)
98 %
70-132
1
05/11/11 19:37
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
15.6 %
0.10
1
05/11/11 18:42
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 93 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-15 Lab ID: 9293679028 Collected: 05/06/11 08:35 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
26900 mg/kg
108
10
05/12/11 15:15
05/16/11 12:13
7429-90-5
Antimony
ND mg/kg
0.54
1
05/12/11 15:15
05/14/11 15:26
7440-36-0
Arsenic
ND mg/kg
0.54
1
05/12/11 15:15
05/16/11 10:03
7440-38-2
Barium
116 mg/kg
0.54
1
05/12/11 15:15
05/14/11 15:26
7440-39-3
Beryllium
2.7 mg/kg
0.11
1
05/12/11 15:15
05/14/11 15:26
7440-41-7
Cadmium
3.6 mg/kg
0.11
1
05/12/11 15:15
05/14/11 15:26
7440-43-9
Calcium
90.6 mg/kg
10.8
1
05/12/11 15:15
05/14/11 15:26
7440-70-2
Chromium
76.3 mg/kg
0.54
1
05/12/11 15:15
05/14/11 15:26
7440-47-3
Cobalt
10.3 mg/kg
0.54
1
05/12/11 15:15
05/14/11 15:26
7440-48-4
Copper
23.4 mg/kg
0.54
1
05/12/11 15:15
05/14/11 15:26
7440-50-8
Iron
49800 mg/kg
54.2
10
05/12/11 15:15
05/16/11 12:13
7439-89-6
Lead
12.6 mg/kg
0.54
1
05/12/11 15:15
05/14/11 15:26
7439-92-1
Magnesium
2170 mg/kg
10.8
1
05/12/11 15:15
05/14/11 15:26
7439-95-4
Manganese
441 mg/kg
0.54
1
05/12/11 15:15
05/14/11 15:26
7439-96-5
Nickel
11.2 mg/kg
0.54
1
05/12/11 15:15
05/14/11 15:26
7440-02-0
Potassium
2820 mg/kg
542
1
05/12/11 15:15
05/14/11 15:26
7440-09-7
Selenium
2.8 mg/kg
1.1
1
05/12/11 15:15
05/16/11 10:03
7782-49-2
Silver
ND mg/kg
0.54
1
05/12/11 15:15
05/14/11 15:26
7440-22-4
Sodium
ND mg/kg
542
1
05/12/11 15:15
05/14/11 15:26
7440-23-5
Thallium
ND mg/kg
1.1
1
05/12/11 15:15
05/14/11 15:26
7440-28-0
Vanadium
58.8 mg/kg
0.54
1
05/12/11 15:15
05/14/11 15:26
7440-62-2
Zinc
46.2 mg/kg
1.1
1
05/12/11 15:15
05/14/11 15:26
7440-66-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.0092 mg/kg
0.0053
1
05/13/11 08:45
05/13/11 16:25
7439-97-6
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
83-32-9
Acenaphthylene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
208-96-8
Aniline
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
62-53-3
Anthracene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
120-12-7
Benzo(a)anthracene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
56-55-3
Benzo(a)pyrene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
50-32-8
Benzo(b)fluoranthene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
191-24-2
Benzo(k)fluoranthene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
207-08-9
Benzoic Acid
ND ug/kg
2250
1
05/14/11 10:32
05/17/11 16:48
65-85-0
Benzyl alcohol
ND ug/kg
901
1
05/14/11 10:32
05/17/11 16:48
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
101-55-3
Butylbenzylphthalate
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
85-68-7
4-Chloro-3-methylphenol
ND ug/kg
901
1
05/14/11 10:32
05/17/11 16:48
59-50-7
4-Chloroaniline
ND ug/kg
2250
1
05/14/11 10:32
05/17/11 16:48
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
108-60-1
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 94 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-15 Lab ID: 9293679028 Collected: 05/06/11 08:35 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Chloronaphthalene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
91-58-7
2-Chlorophenol
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
7005-72-3
Chrysene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
53-70-3
Dibenzofuran
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
132-64-9
1,2-Dichlorobenzene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
95-50-1
1,3-Dichlorobenzene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
541-73-1
1,4-Dichlorobenzene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
2250
1
05/14/11 10:32
05/17/11 16:48
91-94-1
2,4-Dichlorophenol
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
120-83-2
Diethylphthalate
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
84-66-2
2,4-Dimethylphenol
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
105-67-9
Dimethylphthalate
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
131-11-3
Di-n-butylphthalate
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/kg
901
1
05/14/11 10:32
05/17/11 16:48
534-52-1
2,4-Dinitrophenol
ND ug/kg
2250
1
05/14/11 10:32
05/17/11 16:48
51-28-5
2,4-Dinitrotoluene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
121-14-2
2,6-Dinitrotoluene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
606-20-2
Di-n-octylphthalate
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
117-81-7
Fluoranthene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
206-44-0
Fluorene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
87-68-3
Hexachlorobenzene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
77-47-4
Hexachloroethane
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
193-39-5
Isophorone
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
78-59-1
1-Methylnaphthalene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
90-12-0
2-Methylnaphthalene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
Naphthalene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
91-20-3
2-Nitroaniline
ND ug/kg
2250
1
05/14/11 10:32
05/17/11 16:48
88-74-4
3-Nitroaniline
ND ug/kg
2250
1
05/14/11 10:32
05/17/11 16:48
99-09-2
4-Nitroaniline
ND ug/kg
901
1
05/14/11 10:32
05/17/11 16:48
100-01-6
Nitrobenzene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
98-95-3
2-Nitrophenol
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
88-75-5
4-Nitrophenol
ND ug/kg
2250
1
05/14/11 10:32
05/17/11 16:48
100-02-7
N-Nitrosodimethylamine
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
86-30-6
Pentachlorophenol
ND ug/kg
2250
1
05/14/11 10:32
05/17/11 16:48
87-86-5
Phenanthrene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
85-01-8
Phenol
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
108-95-2
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 95 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-15
Lab ID: 9293679028 Collected: 05/06/11 08:35
Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight"
basis
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8270 MSSV Microwave
Analytical Method: EPA 8270 Preparation Method: EPA 3546
Pyrene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
450
1
05/14/11 10:32
05/17/11 16:48
88-06-2
Nitrobenzene-d5 (S)
50 %
23-110
1
05/14/11 10:32
05/17/11 16:48
4165-60-0
2-Fluorobiphenyl (S)
54 %
30-110
1
05/14/11 10:32
05/17/11 16:48
321-60-8
Terphenyl-d14 (S)
52 %
28-110
1
05/14/11 10:32
05/17/11 16:48
1718-51-0
Phenol-d6 (S)
34 %
22-110
1
05/14/11 10:32
05/17/11 16:48
13127-88-3
2-Fluorophenol (S)
33 %
13-110
1
05/14/11 10:32
05/17/11 16:48
367-12-4
2,4,6-Tribromophenol (S)
20 %
27-110
1
05/14/11 10:32
05/17/11 16:48
118-79-6 SO
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND ug/kg
80.8
1
05/11/11 19:57
67-64-1
Benzene
ND ug/kg
4.0
1
05/11/11 19:57
71-43-2
Bromobenzene
ND ug/kg
4.0
1
05/11/11 19:57
108-86-1
Bromochloromethane
ND ug/kg
4.0
1
05/11/11 19:57
74-97-5
Bromodichloromethane
ND ug/kg
4.0
1
05/11/11 19:57
75-27-4
Bromoform
ND ug/kg
4.0
1
05/11/11 19:57
75-25-2
Bromomethane
ND ug/kg
8.1
1
05/11/11 19:57
74-83-9
2-Butanone (MEK)
ND ug/kg
80.8
1
05/11/11 19:57
78-93-3
n-Butylbenzene
ND ug/kg
4.0
1
05/11/11 19:57
104-51-8
sec -Butyl benzene
ND ug/kg
4.0
1
05/11/11 19:57
135-98-8
tert-Butyl benzene
ND ug/kg
4.0
1
05/11/11 19:57
98-06-6
Carbon tetrachloride
ND ug/kg
4.0
1
05/11/11 19:57
56-23-5
Chlorobenzene
ND ug/kg
4.0
1
05/11/11 19:57
108-90-7
Chloroethane
ND ug/kg
8.1
1
05/11/11 19:57
75-00-3
Chloroform
ND ug/kg
4.0
1
05/11/11 19:57
67-66-3
Chloromethane
ND ug/kg
8.1
1
05/11/11 19:57
74-87-3
2-Chlorotoluene
ND ug/kg
4.0
1
05/11/11 19:57
95-49-8
4-Chlorotoluene
ND ug/kg
4.0
1
05/11/11 19:57
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
4.0
1
05/11/11 19:57
96-12-8
Dibromochloromethane
ND ug/kg
4.0
1
05/11/11 19:57
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
4.0
1
05/11/11 19:57
106-93-4
Dibromomethane
ND ug/kg
4.0
1
05/11/11 19:57
74-95-3
1,2-Dichlorobenzene
ND ug/kg
4.0
1
05/11/11 19:57
95-50-1
1,3-Dichlorobenzene
ND ug/kg
4.0
1
05/11/11 19:57
541-73-1
1,4-Dichlorobenzene
ND ug/kg
4.0
1
05/11/11 19:57
106-46-7
Dichlorodifluoromethane
ND ug/kg
8.1
1
05/11/11 19:57
75-71-8
1,1-Dichloroethane
ND ug/kg
4.0
1
05/11/11 19:57
75-34-3
1,2-Dichloroethane
ND ug/kg
4.0
1
05/11/11 19:57
107-06-2
1,1-Dichloroethene
ND ug/kg
4.0
1
05/11/11 19:57
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
4.0
1
05/11/11 19:57
156-59-2
trans- 1,2-Dichloroethene
ND ug/kg
4.0
1
05/11/11 19:57
156-60-5
1,2-Dichloropropane
ND ug/kg
4.0
1
05/11/11 19:57
78-87-5
1,3-Dichloropropane
ND ug/kg
4.0
1
05/11/11 19:57
142-28-9
2,2-Dichloropropane
ND ug/kg
4.0
1
05/11/11 19:57
594-20-7
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
Page 96 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-15 Lab ID: 9293679028 Collected: 05/06/11 08:35 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1-Dichloropropene
ND ug/kg
4.0
1
05/11/11 19:57
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
4.0
1
05/11/11 19:57
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
4.0
1
05/11/11 19:57
10061-02-6
Diisopropyl ether
ND ug/kg
4.0
1
05/11/11 19:57
108-20-3
Ethylbenzene
ND ug/kg
4.0
1
05/11/11 19:57
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
4.0
1
05/11/11 19:57
87-68-3
2-Hexanone
ND ug/kg
40.4
1
05/11/11 19:57
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
4.0
1
05/11/11 19:57
98-82-8
p-Isopropyltoluene
ND ug/kg
4.0
1
05/11/11 19:57
99-87-6
Methylene Chloride
ND ug/kg
16.2
1
05/11/11 19:57
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
40.4
1
05/11/11 19:57
108-10-1
Methyl-tert-butyl ether
ND ug/kg
4.0
1
05/11/11 19:57
1634-04-4
Naphthalene
ND ug/kg
4.0
1
05/11/11 19:57
91-20-3
n-Propylbenzene
ND ug/kg
4.0
1
05/11/11 19:57
103-65-1
Styrene
ND ug/kg
4.0
1
05/11/11 19:57
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
4.0
1
05/11/11 19:57
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
4.0
1
05/11/11 19:57
79-34-5
Tetrachloroethene
ND ug/kg
4.0
1
05/11/11 19:57
127-18-4
Toluene
ND ug/kg
4.0
1
05/11/11 19:57
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
4.0
1
05/11/11 19:57
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
4.0
1
05/11/11 19:57
120-82-1
1,1,1-Trichloroethane
ND ug/kg
4.0
1
05/11/11 19:57
71-55-6
1,1,2-Trichloroethane
ND ug/kg
4.0
1
05/11/11 19:57
79-00-5
Trichloroethene
ND ug/kg
4.0
1
05/11/11 19:57
79-01-6
Trichlorofluoromethane
ND ug/kg
4.0
1
05/11/11 19:57
75-69-4
1,2,3-Trichloropropane
ND ug/kg
4.0
1
05/11/11 19:57
96-18-4
1,2,4-Trimethylbenzene
ND ug/kg
4.0
1
05/11/11 19:57
95-63-6
1,3,5-Trimethylbenzene
ND ug/kg
4.0
1
05/11/11 19:57
108-67-8
Vinyl acetate
ND ug/kg
40.4
1
05/11/11 19:57
108-05-4
Vinyl chloride
ND ug/kg
8.1
1
05/11/11 19:57
75-01-4
Xylene (Total)
ND ug/kg
8.1
1
05/11/11 19:57
1330-20-7
m&p-Xylene
ND ug/kg
8.1
1
05/11/11 19:57
179601-23-1
o-Xylene
ND ug/kg
4.0
1
05/11/11 19:57
95-47-6
Dibromofluoromethane (S)
108 %
70-130
1
05/11/11 19:57
1868-53-7
Toluene-d8 (S)
100 %
70-130
1
05/11/11 19:57
2037-26-5
4-Bromofluorobenzene (S)
90 %
70-130
1
05/11/11 19:57
460-00-4
1,2-Dichloroethane-d4 (S)
106 %
70-132
1
05/11/11 19:57
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
26.7 %
0.10
1
05/11/11 18:42
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 97 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-11 Lab ID: 9293679029 Collected: 05/05/11 00:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
14200 mg/kg
67.0
10
05/12/11 15:15
05/16/11 12:17
7429-90-5
Antimony
ND mg/kg
0.34
1
05/12/11 15:15
05/14/11 15:32
7440-36-0
Arsenic
1.7 mg/kg
0.34
1
05/12/11 15:15
05/16/11 10:06
7440-38-2
Barium
85.0 mg/kg
0.34
1
05/12/11 15:15
05/14/11 15:32
7440-39-3
Beryllium
0.60 mg/kg
0.067
1
05/12/11 15:15
05/14/11 15:32
7440-41-7
Cadmium
0.48 mg/kg
0.067
1
05/12/11 15:15
05/14/11 15:32
7440-43-9
Calcium
10100 mg/kg
67.0
10
05/12/11 15:15
05/16/11 12:17
7440-70-2
Chromium
11.3 mg/kg
0.34
1
05/12/11 15:15
05/14/11 15:32
7440-47-3
Cobalt
3.5 mg/kg
0.34
1
05/12/11 15:15
05/14/11 15:32
7440-48-4
Copper
11.9 mg/kg
0.34
1
05/12/11 15:15
05/14/11 15:32
7440-50-8
Iron
14900 mg/kg
33.5
10
05/12/11 15:15
05/16/11 12:17
7439-89-6
Lead
9.9 mg/kg
0.34
1
05/12/11 15:15
05/14/11 15:32
7439-92-1
Magnesium
2160 mg/kg
6.7
1
05/12/11 15:15
05/14/11 15:32
7439-95-4
Manganese
140 mg/kg
0.34
1
05/12/11 15:15
05/14/11 15:32
7439-96-5
Nickel
6.9 mg/kg
0.34
1
05/12/11 15:15
05/14/11 15:32
7440-02-0
Potassium
2270 mg/kg
335
1
05/12/11 15:15
05/14/11 15:32
7440-09-7
Selenium
ND mg/kg
0.67
1
05/12/11 15:15
05/16/11 10:06
7782-49-2
Silver
ND mg/kg
0.34
1
05/12/11 15:15
05/14/11 15:32
7440-22-4
Sodium
ND mg/kg
335
1
05/12/11 15:15
05/14/11 15:32
7440-23-5
Thallium
ND mg/kg
0.67
1
05/12/11 15:15
05/14/11 15:32
7440-28-0
Vanadium
16.6 mg/kg
0.34
1
05/12/11 15:15
05/14/11 15:32
7440-62-2
Zinc
35.7 mg/kg
0.67
1
05/12/11 15:15
05/14/11 15:32
7440-66-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.33 mg/kg
0.051
10
05/13/11 08:45
05/16/11 14:27
7439-97-6
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
83-32-9
Acenaphthylene
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
208-96-8
Aniline
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
62-53-3
Anthracene
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
120-12-7
Benzo(a)anthracene
556 ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
56-55-3
Benzo(a)pyrene
525 ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
50-32-8
Benzo(b)fluoranthene
435 ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
205-99-2
Benzo(g,h,i)perylene
457 ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
191-24-2
Benzo(k)fluoranthene
436 ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
207-08-9
Benzoic Acid
ND ug/kg
2010
1
05/14/11 10:32
05/17/11 17:15
65-85-0
Benzyl alcohol
ND ug/kg
805
1
05/14/11 10:32
05/17/11 17:15
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
101-55-3
Butylbenzylphthalate
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
85-68-7
4-Chloro-3-methylphenol
ND ug/kg
805
1
05/14/11 10:32
05/17/11 17:15
59-50-7
4-Chloroaniline
ND ug/kg
2010
1
05/14/11 10:32
05/17/11 17:15
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
108-60-1
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 98 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-11 Lab ID: 9293679029 Collected: 05/05/11 00:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Chloronaphthalene
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
91-58-7
2-Chlorophenol
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
7005-72-3
Chrysene
595 ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
53-70-3
Dibenzofuran
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
132-64-9
1,2-Dichlorobenzene
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
95-50-1
1,3-Dichlorobenzene
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
541-73-1
1,4-Dichlorobenzene
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
2010
1
05/14/11 10:32
05/17/11 17:15
91-94-1
2,4-Dichlorophenol
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
120-83-2
Diethylphthalate
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
84-66-2
2,4-Dimethylphenol
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
105-67-9
Dimethylphthalate
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
131-11-3
Di-n-butylphthalate
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/kg
805
1
05/14/11 10:32
05/17/11 17:15
534-52-1
2,4-Dinitrophenol
ND ug/kg
2010
1
05/14/11 10:32
05/17/11 17:15
51-28-5
2,4-Dinitrotoluene
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
121-14-2
2,6-Dinitrotoluene
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
606-20-2
Di-n-octylphthalate
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
117-81-7
Fluoranthene
1400 ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
206-44-0
Fluorene
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
87-68-3
Hexachlorobenzene
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
77-47-4
Hexachloroethane
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
193-39-5
Isophorone
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
78-59-1
1-Methylnaphthalene
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
90-12-0
2-Methylnaphthalene
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
Naphthalene
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
91-20-3
2-Nitroaniline
ND ug/kg
2010
1
05/14/11 10:32
05/17/11 17:15
88-74-4
3-Nitroaniline
ND ug/kg
2010
1
05/14/11 10:32
05/17/11 17:15
99-09-2
4-Nitroaniline
ND ug/kg
805
1
05/14/11 10:32
05/17/11 17:15
100-01-6
Nitrobenzene
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
98-95-3
2-Nitrophenol
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
88-75-5
4-Nitrophenol
ND ug/kg
2010
1
05/14/11 10:32
05/17/11 17:15
100-02-7
N-Nitrosodimethylamine
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
86-30-6
Pentachlorophenol
ND ug/kg
2010
1
05/14/11 10:32
05/17/11 17:15
87-86-5
Phenanthrene
825 ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
85-01-8
Phenol
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
108-95-2
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 99 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-11 Lab ID: 9293679029 Collected: 05/05/11 00:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Pyrene
1090 ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
403
1
05/14/11 10:32
05/17/11 17:15
88-06-2
Nitrobenzene-d5 (S)
52 %
23-110
1
05/14/11 10:32
05/17/11 17:15
4165-60-0
2-Fluorobiphenyl (S)
62 %
30-110
1
05/14/11 10:32
05/17/11 17:15
321-60-8
Terphenyl-d14 (S)
69 %
28-110
1
05/14/11 10:32
05/17/11 17:15
1718-51-0
Phenol-d6 (S)
47 %
22-110
1
05/14/11 10:32
05/17/11 17:15
13127-88-3
2-Fluorophenol (S)
49 %
13-110
1
05/14/11 10:32
05/17/11 17:15
367-12-4
2,4,6-Tribromophenol (S)
56 %
27-110
1
05/14/11 10:32
05/17/11 17:15
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND ug/kg
88.8
1
05/11/11 16:58
67-64-1
Benzene
ND ug/kg
4.4
1
05/11/11 16:58
71-43-2
Bromobenzene
ND ug/kg
4.4
1
05/11/11 16:58
108-86-1
Bromochloromethane
ND ug/kg
4.4
1
05/11/11 16:58
74-97-5
Bromodichloromethane
ND ug/kg
4.4
1
05/11/11 16:58
75-27-4
Bromoform
ND ug/kg
4.4
1
05/11/11 16:58
75-25-2
Bromomethane
ND ug/kg
8.9
1
05/11/11 16:58
74-83-9
2-Butanone (MEK)
ND ug/kg
88.8
1
05/11/11 16:58
78-93-3
n-Butylbenzene
ND ug/kg
4.4
1
05/11/11 16:58
104-51-8
sec -Butyl benzene
ND ug/kg
4.4
1
05/11/11 16:58
135-98-8
tert-Butyl benzene
ND ug/kg
4.4
1
05/11/11 16:58
98-06-6
Carbon tetrachloride
ND ug/kg
4.4
1
05/11/11 16:58
56-23-5
Chlorobenzene
ND ug/kg
4.4
1
05/11/11 16:58
108-90-7
Chloroethane
ND ug/kg
8.9
1
05/11/11 16:58
75-00-3
Chloroform
ND ug/kg
4.4
1
05/11/11 16:58
67-66-3
Chloromethane
ND ug/kg
8.9
1
05/11/11 16:58
74-87-3
2-Chlorotoluene
ND ug/kg
4.4
1
05/11/11 16:58
95-49-8
4-Chlorotoluene
ND ug/kg
4.4
1
05/11/11 16:58
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
4.4
1
05/11/11 16:58
96-12-8
Dibromochloromethane
ND ug/kg
4.4
1
05/11/11 16:58
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
4.4
1
05/11/11 16:58
106-93-4
Dibromomethane
ND ug/kg
4.4
1
05/11/11 16:58
74-95-3
1,2-Dichlorobenzene
ND ug/kg
4.4
1
05/11/11 16:58
95-50-1
1,3-Dichlorobenzene
ND ug/kg
4.4
1
05/11/11 16:58
541-73-1
1,4-Dichlorobenzene
ND ug/kg
4.4
1
05/11/11 16:58
106-46-7
Dichlorodifluoromethane
ND ug/kg
8.9
1
05/11/11 16:58
75-71-8
1,1-Dichloroethane
ND ug/kg
4.4
1
05/11/11 16:58
75-34-3
1,2-Dichloroethane
ND ug/kg
4.4
1
05/11/11 16:58
107-06-2
1,1-Dichloroethene
ND ug/kg
4.4
1
05/11/11 16:58
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
4.4
1
05/11/11 16:58
156-59-2
trans- 1,2-Dichloroethene
ND ug/kg
4.4
1
05/11/11 16:58
156-60-5
1,2-Dichloropropane
ND ug/kg
4.4
1
05/11/11 16:58
78-87-5
1,3-Dichloropropane
ND ug/kg
4.4
1
05/11/11 16:58
142-28-9
2,2-Dichloropropane
ND ug/kg
4.4
1
05/11/11 16:58
594-20-7
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 100 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-11 Lab ID: 9293679029 Collected: 05/05/11 00:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1-Dichloropropene
ND ug/kg
4.4
1
05/11/11 16:58
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
4.4
1
05/11/11 16:58
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
4.4
1
05/11/11 16:58
10061-02-6
Diisopropyl ether
ND ug/kg
4.4
1
05/11/11 16:58
108-20-3
Ethylbenzene
ND ug/kg
4.4
1
05/11/11 16:58
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
4.4
1
05/11/11 16:58
87-68-3
2-Hexanone
ND ug/kg
44.4
1
05/11/11 16:58
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
4.4
1
05/11/11 16:58
98-82-8
p-Isopropyltoluene
ND ug/kg
4.4
1
05/11/11 16:58
99-87-6
Methylene Chloride
ND ug/kg
17.8
1
05/11/11 16:58
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
44.4
1
05/11/11 16:58
108-10-1
Methyl-tert-butyl ether
ND ug/kg
4.4
1
05/11/11 16:58
1634-04-4
Naphthalene
ND ug/kg
4.4
1
05/11/11 16:58
91-20-3
n-Propylbenzene
ND ug/kg
4.4
1
05/11/11 16:58
103-65-1
Styrene
ND ug/kg
4.4
1
05/11/11 16:58
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
4.4
1
05/11/11 16:58
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
4.4
1
05/11/11 16:58
79-34-5
Tetrachloroethene
ND ug/kg
4.4
1
05/11/11 16:58
127-18-4
Toluene
ND ug/kg
4.4
1
05/11/11 16:58
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
4.4
1
05/11/11 16:58
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
4.4
1
05/11/11 16:58
120-82-1
1,1,1-Trichloroethane
ND ug/kg
4.4
1
05/11/11 16:58
71-55-6
1,1,2-Trichloroethane
ND ug/kg
4.4
1
05/11/11 16:58
79-00-5
Trichloroethene
ND ug/kg
4.4
1
05/11/11 16:58
79-01-6
Trichlorofluoromethane
ND ug/kg
4.4
1
05/11/11 16:58
75-69-4
1,2,3-Trichloropropane
ND ug/kg
4.4
1
05/11/11 16:58
96-18-4
1,2,4-Trimethylbenzene
ND ug/kg
4.4
1
05/11/11 16:58
95-63-6
1,3,5-Trimethylbenzene
ND ug/kg
4.4
1
05/11/11 16:58
108-67-8
Vinyl acetate
ND ug/kg
44.4
1
05/11/11 16:58
108-05-4
Vinyl chloride
ND ug/kg
8.9
1
05/11/11 16:58
75-01-4
Xylene (Total)
ND ug/kg
8.9
1
05/11/11 16:58
1330-20-7
m&p-Xylene
ND ug/kg
8.9
1
05/11/11 16:58
179601-23-1
o-Xylene
ND ug/kg
4.4
1
05/11/11 16:58
95-47-6
Dibromofluoromethane (S)
106 %
70-130
1
05/11/11 16:58
1868-53-7
Toluene-d8 (S)
104 %
70-130
1
05/11/11 16:58
2037-26-5
4-Bromofluorobenzene (S)
94 %
70-130
1
05/11/11 16:58
460-00-4
1,2-Dichloroethane-d4 (S)
105 %
70-132
1
05/11/11 16:58
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
18.0 %
0.10
1
05/11/11 18:42
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 101 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-2 Lab ID: 9293679030 Collected: 05/06/11 00:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
18800 mg/kg
90.1
10
05/12/11 15:15
05/16/11 12:21
7429-90-5
Antimony
ND mg/kg
0.45
1
05/12/11 15:15
05/14/11 15:47
7440-36-0
Arsenic
0.99 mg/kg
0.45
1
05/12/11 15:15
05/16/11 10:10
7440-38-2
Barium
55.4 mg/kg
0.45
1
05/12/11 15:15
05/14/11 15:47
7440-39-3
Beryllium
0.42 mg/kg
0.090
1
05/12/11 15:15
05/14/11 15:47
7440-41-7
Cadmium
0.70 mg/kg
0.090
1
05/12/11 15:15
05/14/11 15:47
7440-43-9
Calcium
314 mg/kg
9.0
1
05/12/11 15:15
05/14/11 15:47
7440-70-2
Chromium
18.3 mg/kg
0.45
1
05/12/11 15:15
05/14/11 15:47
7440-47-3
Cobalt
0.68 mg/kg
0.45
1
05/12/11 15:15
05/14/11 15:47
7440-48-4
Copper
8.2 mg/kg
0.45
1
05/12/11 15:15
05/14/11 15:47
7440-50-8
Iron
22800 mg/kg
45.0
10
05/12/11 15:15
05/16/11 12:21
7439-89-6
Lead
6.4 mg/kg
0.45
1
05/12/11 15:15
05/14/11 15:47
7439-92-1
Magnesium
2010 mg/kg
9.0
1
05/12/11 15:15
05/14/11 15:47
7439-95-4
Manganese
35.1 mg/kg
0.45
1
05/12/11 15:15
05/14/11 15:47
7439-96-5
Nickel
7.3 mg/kg
0.45
1
05/12/11 15:15
05/14/11 15:47
7440-02-0
Potassium
2140 mg/kg
450
1
05/12/11 15:15
05/14/11 15:47
7440-09-7
Selenium
1.3 mg/kg
0.90
1
05/12/11 15:15
05/16/11 10:10
7782-49-2
Silver
ND mg/kg
0.45
1
05/12/11 15:15
05/14/11 15:47
7440-22-4
Sodium
ND mg/kg
450
1
05/12/11 15:15
05/14/11 15:47
7440-23-5
Thallium
ND mg/kg
0.90
1
05/12/11 15:15
05/14/11 15:47
7440-28-0
Vanadium
28.9 mg/kg
0.45
1
05/12/11 15:15
05/14/11 15:47
7440-62-2
Zinc
25.1 mg/kg
0.90
1
05/12/11 15:15
05/14/11 15:47
7440-66-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.059 mg/kg
0.0040
1
05/13/11 08:45
05/13/11 16:37
7439-97-6
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
83-32-9
Acenaphthylene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
208-96-8
Aniline
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
62-53-3
Anthracene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
120-12-7
Benzo(a)anthracene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
56-55-3
Benzo(a)pyrene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
50-32-8
Benzo(b)fluoranthene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
191-24-2
Benzo(k)fluoranthene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
207-08-9
Benzoic Acid
ND ug/kg
2140
1
05/14/11 10:32
05/17/11 17:43
65-85-0
Benzyl alcohol
ND ug/kg
856
1
05/14/11 10:32
05/17/11 17:43
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
101-55-3
Butylbenzylphthalate
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
85-68-7
4-Chloro-3-methylphenol
ND ug/kg
856
1
05/14/11 10:32
05/17/11 17:43
59-50-7
4-Chloroaniline
ND ug/kg
2140
1
05/14/11 10:32
05/17/11 17:43
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
108-60-1
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 102 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-2 Lab ID: 9293679030 Collected: 05/06/11 00:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Chloronaphthalene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
91-58-7
2-Chlorophenol
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
7005-72-3
Chrysene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
53-70-3
Dibenzofuran
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
132-64-9
1,2-Dichlorobenzene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
95-50-1
1,3-Dichlorobenzene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
541-73-1
1,4-Dichlorobenzene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
2140
1
05/14/11 10:32
05/17/11 17:43
91-94-1
2,4-Dichlorophenol
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
120-83-2
Diethylphthalate
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
84-66-2
2,4-Dimethylphenol
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
105-67-9
Dimethylphthalate
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
131-11-3
Di-n-butylphthalate
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/kg
856
1
05/14/11 10:32
05/17/11 17:43
534-52-1
2,4-Dinitrophenol
ND ug/kg
2140
1
05/14/11 10:32
05/17/11 17:43
51-28-5
2,4-Dinitrotoluene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
121-14-2
2,6-Dinitrotoluene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
606-20-2
Di-n-octylphthalate
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
117-81-7
Fluoranthene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
206-44-0
Fluorene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
87-68-3
Hexachlorobenzene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
77-47-4
Hexachloroethane
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
193-39-5
Isophorone
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
78-59-1
1-Methylnaphthalene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
90-12-0
2-Methylnaphthalene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
Naphthalene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
91-20-3
2-Nitroaniline
ND ug/kg
2140
1
05/14/11 10:32
05/17/11 17:43
88-74-4
3-Nitroaniline
ND ug/kg
2140
1
05/14/11 10:32
05/17/11 17:43
99-09-2
4-Nitroaniline
ND ug/kg
856
1
05/14/11 10:32
05/17/11 17:43
100-01-6
Nitrobenzene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
98-95-3
2-Nitrophenol
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
88-75-5
4-Nitrophenol
ND ug/kg
2140
1
05/14/11 10:32
05/17/11 17:43
100-02-7
N-Nitrosodimethylamine
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
86-30-6
Pentachlorophenol
ND ug/kg
2140
1
05/14/11 10:32
05/17/11 17:43
87-86-5
Phenanthrene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
85-01-8
Phenol
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
108-95-2
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 103 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-2 Lab ID: 9293679030 Collected: 05/06/11 00:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Pyrene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
428
1
05/14/11 10:32
05/17/11 17:43
88-06-2
Nitrobenzene-d5 (S)
45 %
23-110
1
05/14/11 10:32
05/17/11 17:43
4165-60-0
2-Fluorobiphenyl (S)
46 %
30-110
1
05/14/11 10:32
05/17/11 17:43
321-60-8
Terphenyl-d14 (S)
61 %
28-110
1
05/14/11 10:32
05/17/11 17:43
1718-51-0
Phenol-d6 (S)
37 %
22-110
1
05/14/11 10:32
05/17/11 17:43
13127-88-3
2-Fluorophenol (S)
41 %
13-110
1
05/14/11 10:32
05/17/11 17:43
367-12-4
2,4,6-Tribromophenol (S)
49 %
27-110
1
05/14/11 10:32
05/17/11 17:43
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND ug/kg
77.6
1
05/11/11 17:18
67-64-1
Benzene
ND ug/kg
3.9
1
05/11/11 17:18
71-43-2
Bromobenzene
ND ug/kg
3.9
1
05/11/11 17:18
108-86-1
Bromochloromethane
ND ug/kg
3.9
1
05/11/11 17:18
74-97-5
Bromodichloromethane
ND ug/kg
3.9
1
05/11/11 17:18
75-27-4
Bromoform
ND ug/kg
3.9
1
05/11/11 17:18
75-25-2
Bromomethane
ND ug/kg
7.8
1
05/11/11 17:18
74-83-9
2-Butanone (MEK)
ND ug/kg
77.6
1
05/11/11 17:18
78-93-3
n-Butylbenzene
ND ug/kg
3.9
1
05/11/11 17:18
104-51-8
sec -Butyl benzene
ND ug/kg
3.9
1
05/11/11 17:18
135-98-8
tert-Butyl benzene
ND ug/kg
3.9
1
05/11/11 17:18
98-06-6
Carbon tetrachloride
ND ug/kg
3.9
1
05/11/11 17:18
56-23-5
Chlorobenzene
ND ug/kg
3.9
1
05/11/11 17:18
108-90-7
Chloroethane
ND ug/kg
7.8
1
05/11/11 17:18
75-00-3
Chloroform
ND ug/kg
3.9
1
05/11/11 17:18
67-66-3
Chloromethane
ND ug/kg
7.8
1
05/11/11 17:18
74-87-3
2-Chlorotoluene
ND ug/kg
3.9
1
05/11/11 17:18
95-49-8
4-Chlorotoluene
ND ug/kg
3.9
1
05/11/11 17:18
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
3.9
1
05/11/11 17:18
96-12-8
Dibromochloromethane
ND ug/kg
3.9
1
05/11/11 17:18
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
3.9
1
05/11/11 17:18
106-93-4
Dibromomethane
ND ug/kg
3.9
1
05/11/11 17:18
74-95-3
1,2-Dichlorobenzene
ND ug/kg
3.9
1
05/11/11 17:18
95-50-1
1,3-Dichlorobenzene
ND ug/kg
3.9
1
05/11/11 17:18
541-73-1
1,4-Dichlorobenzene
ND ug/kg
3.9
1
05/11/11 17:18
106-46-7
Dichlorodifluoromethane
ND ug/kg
7.8
1
05/11/11 17:18
75-71-8
1,1-Dichloroethane
ND ug/kg
3.9
1
05/11/11 17:18
75-34-3
1,2-Dichloroethane
ND ug/kg
3.9
1
05/11/11 17:18
107-06-2
1,1-Dichloroethene
ND ug/kg
3.9
1
05/11/11 17:18
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
3.9
1
05/11/11 17:18
156-59-2
trans- 1,2-Dichloroethene
ND ug/kg
3.9
1
05/11/11 17:18
156-60-5
1,2-Dichloropropane
ND ug/kg
3.9
1
05/11/11 17:18
78-87-5
1,3-Dichloropropane
ND ug/kg
3.9
1
05/11/11 17:18
142-28-9
2,2-Dichloropropane
ND ug/kg
3.9
1
05/11/11 17:18
594-20-7
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 104 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-2 Lab ID: 9293679030 Collected: 05/06/11 00:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1-Dichloropropene
ND ug/kg
3.9
1
05/11/11 17:18
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
3.9
1
05/11/11 17:18
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
3.9
1
05/11/11 17:18
10061-02-6
Diisopropyl ether
ND ug/kg
3.9
1
05/11/11 17:18
108-20-3
Ethylbenzene
ND ug/kg
3.9
1
05/11/11 17:18
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
3.9
1
05/11/11 17:18
87-68-3
2-Hexanone
ND ug/kg
38.8
1
05/11/11 17:18
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
3.9
1
05/11/11 17:18
98-82-8
p-Isopropyltoluene
ND ug/kg
3.9
1
05/11/11 17:18
99-87-6
Methylene Chloride
ND ug/kg
15.5
1
05/11/11 17:18
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
38.8
1
05/11/11 17:18
108-10-1
Methyl-tert-butyl ether
ND ug/kg
3.9
1
05/11/11 17:18
1634-04-4
Naphthalene
ND ug/kg
3.9
1
05/11/11 17:18
91-20-3
n-Propylbenzene
ND ug/kg
3.9
1
05/11/11 17:18
103-65-1
Styrene
ND ug/kg
3.9
1
05/11/11 17:18
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
3.9
1
05/11/11 17:18
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
3.9
1
05/11/11 17:18
79-34-5
Tetrachloroethene
ND ug/kg
3.9
1
05/11/11 17:18
127-18-4
Toluene
ND ug/kg
3.9
1
05/11/11 17:18
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
3.9
1
05/11/11 17:18
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
3.9
1
05/11/11 17:18
120-82-1
1,1,1-Trichloroethane
ND ug/kg
3.9
1
05/11/11 17:18
71-55-6
1,1,2-Trichloroethane
ND ug/kg
3.9
1
05/11/11 17:18
79-00-5
Trichloroethene
ND ug/kg
3.9
1
05/11/11 17:18
79-01-6
Trichlorofluoromethane
ND ug/kg
3.9
1
05/11/11 17:18
75-69-4
1,2,3-Trichloropropane
ND ug/kg
3.9
1
05/11/11 17:18
96-18-4
1,2,4-Trimethylbenzene
ND ug/kg
3.9
1
05/11/11 17:18
95-63-6
1,3,5-Trimethylbenzene
ND ug/kg
3.9
1
05/11/11 17:18
108-67-8
Vinyl acetate
ND ug/kg
38.8
1
05/11/11 17:18
108-05-4
Vinyl chloride
ND ug/kg
7.8
1
05/11/11 17:18
75-01-4
Xylene (Total)
ND ug/kg
7.8
1
05/11/11 17:18
1330-20-7
m&p-Xylene
ND ug/kg
7.8
1
05/11/11 17:18
179601-23-1
o-Xylene
ND ug/kg
3.9
1
05/11/11 17:18
95-47-6
Dibromofluoromethane (S)
102 %
70-130
1
05/11/11 17:18
1868-53-7
Toluene-d8 (S)
98 %
70-130
1
05/11/11 17:18
2037-26-5
4-Bromofluorobenzene (S)
90 %
70-130
1
05/11/11 17:18
460-00-4
1,2-Dichloroethane-d4 (S)
98 %
70-132
1
05/11/11 17:18
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
22.9 %
0.10
1
05/11/11 18:42
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 105 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: S-3 0-2' Lab ID: 9293679031 Collected: 05/06/11 09:45 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Decachlorobiphenyl (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8082 Preparation Method: EPA 3546
ND ug/kg
42.5
1
05/17/11 09:55
05/14/11 15:26
12674-11-2
ND ug/kg
42.5
1
05/17/11 09:55
05/14/11 15:26
11104-28-2
ND ug/kg
42.5
1
05/17/11 09:55
05/14/11 15:26
11141-16-5
ND ug/kg
42.5
1
05/17/11 09:55
05/14/11 15:26
53469-21-9
ND ug/kg
42.5
1
05/17/11 09:55
05/14/11 15:26
12672-29-6
ND ug/kg
42.5
1
05/17/11 09:55
05/14/11 15:26
11097-69-1
ND ug/kg
42.5
1
05/17/11 09:55
05/14/11 15:26
11096-82-5
184 %
21-132
1
05/17/11 09:55
05/14/11 15:26
2051-24-3 S5
Analytical Method: ASTM D2974-87
22.9 % 0.10 1 05/12/11 09:30
Sample: S-3 8-10' Lab ID: 9293679032 Collected: 05/06/11 09:50 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Decachlorobiphenyl (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8082 Preparation Method: EPA 3546
ND ug/kg
42.1
1
05/17/11 09:55
05/14/11 00:12
12674-11-2
ND ug/kg
42.1
1
05/17/11 09:55
05/14/11 00:12
11104-28-2
ND ug/kg
42.1
1
05/17/11 09:55
05/14/11 00:12
11141-16-5
ND ug/kg
42.1
1
05/17/11 09:55
05/14/11 00:12
53469-21-9
ND ug/kg
42.1
1
05/17/11 09:55
05/14/11 00:12
12672-29-6
ND ug/kg
42.1
1
05/17/11 09:55
05/14/11 00:12
11097-69-1
ND ug/kg
42.1
1
05/17/11 09:55
05/14/11 00:12
11096-82-5
73 %
21-132
1
05/17/11 09:55
05/14/11 00:12
2051-24-3
Analytical Method: ASTM D2974-87
21.5 % 0.10 1 05/12/11 09:30
Sample: S-4 Lab ID: 9293679033 Collected: 05/06/11 10:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Date: 05/20/2011 04:57 PM
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
83-32-9
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
208-96-8
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
62-53-3
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
120-12-7
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
56-55-3
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
50-32-8
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
205-99-2
REPORT OF LABORATORY ANALYSIS Page 106 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-4 Lab ID: 9293679033 Collected: 05/06/11 10:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Benzo(g,h,i)perylene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
191-24-2
Benzo(k)fluoranthene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
207-08-9
Benzoic Acid
ND ug/kg
2020
1
05/14/11 10:32
05/17/11 18:10
65-85-0
Benzyl alcohol
ND ug/kg
809
1
05/14/11 10:32
05/17/11 18:10
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
101-55-3
Butylbenzylphthalate
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
85-68-7
4-Chloro-3-methylphenol
ND ug/kg
809
1
05/14/11 10:32
05/17/11 18:10
59-50-7
4-Chloroaniline
ND ug/kg
2020
1
05/14/11 10:32
05/17/11 18:10
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
108-60-1
2-Chloronaphthalene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
91-58-7
2-Chlorophenol
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
7005-72-3
Chrysene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
53-70-3
Dibenzofuran
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
132-64-9
1,2-Dichlorobenzene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
95-50-1
1,3-Dichlorobenzene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
541-73-1
1,4-Dichlorobenzene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
2020
1
05/14/11 10:32
05/17/11 18:10
91-94-1
2,4-Dichlorophenol
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
120-83-2
Diethylphthalate
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
84-66-2
2,4-Dimethylphenol
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
105-67-9
Dimethylphthalate
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
131-11-3
Di-n-butylphthalate
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
84-74-2
4,6-Dinitro-2-methylphenol
ND ug/kg
809
1
05/14/11 10:32
05/17/11 18:10
534-52-1
2,4-Dinitrophenol
ND ug/kg
2020
1
05/14/11 10:32
05/17/11 18:10
51-28-5
2,4-Dinitrotoluene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
121-14-2
2,6-Dinitrotoluene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
606-20-2
Di-n-octylphthalate
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
117-81-7
Fluoranthene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
206-44-0
Fluorene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
87-68-3
Hexachlorobenzene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
77-47-4
Hexachloroethane
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
193-39-5
Isophorone
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
78-59-1
1-Methylnaphthalene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
90-12-0
2-Methylnaphthalene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
Naphthalene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
91-20-3
2-Nitroaniline
ND ug/kg
2020
1
05/14/11 10:32
05/17/11 18:10
88-74-4
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 107 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-4 Lab ID: 9293679033 Collected: 05/06/11 10:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
3-Nitroaniline
ND ug/kg
2020
1
05/14/11 10:32
05/17/11 18:10
99-09-2
4-Nitroaniline
ND ug/kg
809
1
05/14/11 10:32
05/17/11 18:10
100-01-6
Nitrobenzene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
98-95-3
2-Nitrophenol
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
88-75-5
4-Nitrophenol
ND ug/kg
2020
1
05/14/11 10:32
05/17/11 18:10
100-02-7
N-Nitrosodimethylamine
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
86-30-6
Pentachlorophenol
ND ug/kg
2020
1
05/14/11 10:32
05/17/11 18:10
87-86-5
Phenanthrene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
85-01-8
Phenol
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
108-95-2
Pyrene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
404
1
05/14/11 10:32
05/17/11 18:10
88-06-2
Nitrobenzene-d5 (S)
51 %
23-110
1
05/14/11 10:32
05/17/11 18:10
4165-60-0
2-Fluorobiphenyl (S)
51 %
30-110
1
05/14/11 10:32
05/17/11 18:10
321-60-8
Terphenyl-d14 (S)
38 %
28-110
1
05/14/11 10:32
05/17/11 18:10
1718-51-0
Phenol-d6 (S)
40 %
22-110
1
05/14/11 10:32
05/17/11 18:10
13127-88-3
2-Fluorophenol (S)
43 %
13-110
1
05/14/11 10:32
05/17/11 18:10
367-12-4
2,4,6-Tribromophenol (S)
40 %
27-110
1
05/14/11 10:32
05/17/11 18:10
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND ug/kg
73.0
1
05/11/11 16:38
67-64-1
Benzene
ND ug/kg
3.7
1
05/11/11 16:38
71-43-2
Bromobenzene
ND ug/kg
3.7
1
05/11/11 16:38
108-86-1
Bromochloromethane
ND ug/kg
3.7
1
05/11/11 16:38
74-97-5
Bromodichloromethane
ND ug/kg
3.7
1
05/11/11 16:38
75-27-4
Bromoform
ND ug/kg
3.7
1
05/11/11 16:38
75-25-2
Bromomethane
ND ug/kg
7.3
1
05/11/11 16:38
74-83-9
2-Butanone (MEK)
ND ug/kg
73.0
1
05/11/11 16:38
78-93-3
n-Butylbenzene
ND ug/kg
3.7
1
05/11/11 16:38
104-51-8
sec -Butyl benzene
ND ug/kg
3.7
1
05/11/11 16:38
135-98-8
tert-Butyl benzene
ND ug/kg
3.7
1
05/11/11 16:38
98-06-6
Carbon tetrachloride
ND ug/kg
3.7
1
05/11/11 16:38
56-23-5
Chlorobenzene
ND ug/kg
3.7
1
05/11/11 16:38
108-90-7
Chloroethane
ND ug/kg
7.3
1
05/11/11 16:38
75-00-3
Chloroform
ND ug/kg
3.7
1
05/11/11 16:38
67-66-3
Chloromethane
ND ug/kg
7.3
1
05/11/11 16:38
74-87-3
2-Chlorotoluene
ND ug/kg
3.7
1
05/11/11 16:38
95-49-8
4-Chlorotoluene
ND ug/kg
3.7
1
05/11/11 16:38
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
3.7
1
05/11/11 16:38
96-12-8
Dibromochloromethane
ND ug/kg
3.7
1
05/11/11 16:38
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
3.7
1
05/11/11 16:38
106-93-4
Dibromomethane
ND ug/kg
3.7
1
05/11/11 16:38
74-95-3
1,2-Dichlorobenzene
ND ug/kg
3.7
1
05/11/11 16:38
95-50-1
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 108 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-4 Lab ID: 9293679033 Collected: 05/06/11 10:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,3-Dichlorobenzene
ND ug/kg
3.7
1
05/11/11 16:38
541-73-1
1,4-Dichlorobenzene
ND ug/kg
3.7
1
05/11/11 16:38
106-46-7
Dichlorodifluoromethane
ND ug/kg
7.3
1
05/11/11 16:38
75-71-8
1,1-Dichloroethane
ND ug/kg
3.7
1
05/11/11 16:38
75-34-3
1,2-Dichloroethane
ND ug/kg
3.7
1
05/11/11 16:38
107-06-2
1,1-Dichloroethene
ND ug/kg
3.7
1
05/11/11 16:38
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
3.7
1
05/11/11 16:38
156-59-2
trans- 1,2-Dichloroethene
ND ug/kg
3.7
1
05/11/11 16:38
156-60-5
1,2-Dichloropropane
ND ug/kg
3.7
1
05/11/11 16:38
78-87-5
1,3-Dichloropropane
ND ug/kg
3.7
1
05/11/11 16:38
142-28-9
2,2-Dichloropropane
ND ug/kg
3.7
1
05/11/11 16:38
594-20-7
1,1-Dichloropropene
ND ug/kg
3.7
1
05/11/11 16:38
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
3.7
1
05/11/11 16:38
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
3.7
1
05/11/11 16:38
10061-02-6
Diisopropyl ether
ND ug/kg
3.7
1
05/11/11 16:38
108-20-3
Ethylbenzene
ND ug/kg
3.7
1
05/11/11 16:38
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
3.7
1
05/11/11 16:38
87-68-3
2-Hexanone
ND ug/kg
36.5
1
05/11/11 16:38
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
3.7
1
05/11/11 16:38
98-82-8
p-Isopropyltoluene
ND ug/kg
3.7
1
05/11/11 16:38
99-87-6
Methylene Chloride
ND ug/kg
14.6
1
05/11/11 16:38
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
36.5
1
05/11/11 16:38
108-10-1
Methyl-tert-butyl ether
ND ug/kg
3.7
1
05/11/11 16:38
1634-04-4
Naphthalene
ND ug/kg
3.7
1
05/11/11 16:38
91-20-3
n-Propylbenzene
ND ug/kg
3.7
1
05/11/11 16:38
103-65-1
Styrene
ND ug/kg
3.7
1
05/11/11 16:38
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
3.7
1
05/11/11 16:38
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
3.7
1
05/11/11 16:38
79-34-5
Tetrachloroethene
ND ug/kg
3.7
1
05/11/11 16:38
127-18-4
Toluene
ND ug/kg
3.7
1
05/11/11 16:38
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
3.7
1
05/11/11 16:38
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
3.7
1
05/11/11 16:38
120-82-1
1,1,1-Trichloroethane
ND ug/kg
3.7
1
05/11/11 16:38
71-55-6
1,1,2-Trichloroethane
ND ug/kg
3.7
1
05/11/11 16:38
79-00-5
Trichloroethene
ND ug/kg
3.7
1
05/11/11 16:38
79-01-6
Trichlorofluoromethane
ND ug/kg
3.7
1
05/11/11 16:38
75-69-4
1,2,3-Trichloropropane
ND ug/kg
3.7
1
05/11/11 16:38
96-18-4
1,2,4-Trimethylbenzene
ND ug/kg
3.7
1
05/11/11 16:38
95-63-6
1,3,5-Trimethylbenzene
ND ug/kg
3.7
1
05/11/11 16:38
108-67-8
Vinyl acetate
ND ug/kg
36.5
1
05/11/11 16:38
108-05-4
Vinyl chloride
ND ug/kg
7.3
1
05/11/11 16:38
75-01-4
Xylene (Total)
ND ug/kg
7.3
1
05/11/11 16:38
1330-20-7
m&p-Xylene
ND ug/kg
7.3
1
05/11/11 16:38
179601-23-1
o-Xylene
ND ug/kg
3.7
1
05/11/11 16:38
95-47-6
Dibromofluoromethane (S)
106 %
70-130
1
05/11/11 16:38
1868-53-7
Toluene-d8 (S)
100 %
70-130
1
05/11/11 16:38
2037-26-5
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 109 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: S-4
Lab ID: 9293679033 Collected:
05/06/11 10:30
Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight"
basis
Parameters
Results Units Report
Limit
DF
Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Analytical Method: EPA 8260
4-Bromofluorobenzene (S)
94 %
70-130
1
05/11/11 16:38 460-00-4
1,2-Dichloroethane-d4 (S)
96 %
70-132
1
05/11/11 16:38 17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
18.4 %
0.10
1
05/11/11 18:42
Sample: S-5 Lab ID: 9293679034 Collected: 05/06/11 10:45 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone
ND ug/kg
62.5
1
Benzene
ND ug/kg
3.1
1
Bromobenzene
ND ug/kg
3.1
1
Bromochloromethane
ND ug/kg
3.1
1
Bromodichloromethane
ND ug/kg
3.1
1
Bromoform
ND ug/kg
3.1
1
Bromomethane
ND ug/kg
6.2
1
2-Butanone (MEK)
ND ug/kg
62.5
1
n-Butylbenzene
ND ug/kg
3.1
1
sec -Butyl benzene
ND ug/kg
3.1
1
tert-Butyl benzene
ND ug/kg
3.1
1
Carbon tetrachloride
ND ug/kg
3.1
1
Chlorobenzene
ND ug/kg
3.1
1
Chloroethane
ND ug/kg
6.2
1
Chloroform
ND ug/kg
3.1
1
Chloromethane
ND ug/kg
6.2
1
2-Chlorotoluene
ND ug/kg
3.1
1
4-Chlorotoluene
ND ug/kg
3.1
1
1,2-Dibromo-3-chloropropane
ND ug/kg
3.1
1
Dibromochloromethane
ND ug/kg
3.1
1
1,2-Dibromoethane (EDB)
ND ug/kg
3.1
1
Dibromomethane
ND ug/kg
3.1
1
1,2-Dichlorobenzene
ND ug/kg
3.1
1
1,3-Dichlorobenzene
ND ug/kg
3.1
1
1,4-Dichlorobenzene
ND ug/kg
3.1
1
Dichlorodifluoromethane
ND ug/kg
6.2
1
1,1-Dichloroethane
ND ug/kg
3.1
1
1,2-Dichloroethane
ND ug/kg
3.1
1
1,1-Dichloroethene
ND ug/kg
3.1
1
cis-1,2-Dichloroethene
ND ug/kg
3.1
1
trans- 1,2-Dichloroethene
ND ug/kg
3.1
1
1,2-Dichloropropane
ND ug/kg
3.1
1
1,3-Dichloropropane
ND ug/kg
3.1
1
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY
ANALYSIS
This report
shall not be reproduced, except
in full,
without the written consent of Analytical Services, Inc..
PPace
05/11/11 17:38
67-64-1
05/11/11 17:38
71-43-2
05/11/11 17:38
108-86-1
05/11/11 17:38
74-97-5
05/11/11 17:38
75-27-4
05/11/11 17:38
75-25-2
05/11/11 17:38
74-83-9
05/11/11 17:38
78-93-3
05/11/11 17:38
104-51-8
05/11/11 17:38
135-98-8
05/11/11 17:38
98-06-6
05/11/11 17:38
56-23-5
05/11/11 17:38
108-90-7
05/11/11 17:38
75-00-3
05/11/11 17:38
67-66-3
05/11/11 17:38
74-87-3
05/11/11 17:38
95-49-8
05/11/11 17:38
106-43-4
05/11/11 17:38
96-12-8
05/11/11 17:38
124-48-1
05/11/11 17:38
106-93-4
05/11/11 17:38
74-95-3
05/11/11 17:38
95-50-1
05/11/11 17:38
541-73-1
05/11/11 17:38
106-46-7
05/11/11 17:38
75-71-8
05/11/11 17:38
75-34-3
05/11/11 17:38
107-06-2
05/11/11 17:38
75-35-4
05/11/11 17:38
156-59-2
05/11/11 17:38
156-60-5
05/11/11 17:38
78-87-5
05/11/11 17:38
142-28-9
Page 110 of 227

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-5 Lab ID: 9293679034 Collected: 05/06/11 10:45 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
2,2-Dichloropropane
ND ug/kg
3.1
1
05/11/11 17:38
594-20-7
1,1-Dichloropropene
ND ug/kg
3.1
1
05/11/11 17:38
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
3.1
1
05/11/11 17:38
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
3.1
1
05/11/11 17:38
10061-02-6
Diisopropyl ether
ND ug/kg
3.1
1
05/11/11 17:38
108-20-3
Ethylbenzene
ND ug/kg
3.1
1
05/11/11 17:38
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
3.1
1
05/11/11 17:38
87-68-3
2-Hexanone
ND ug/kg
31.2
1
05/11/11 17:38
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
3.1
1
05/11/11 17:38
98-82-8
p-Isopropyltoluene
ND ug/kg
3.1
1
05/11/11 17:38
99-87-6
Methylene Chloride
ND ug/kg
12.5
1
05/11/11 17:38
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
31.2
1
05/11/11 17:38
108-10-1
Methyl-tert-butyl ether
ND ug/kg
3.1
1
05/11/11 17:38
1634-04-4
Naphthalene
ND ug/kg
3.1
1
05/11/11 17:38
91-20-3
n-Propylbenzene
ND ug/kg
3.1
1
05/11/11 17:38
103-65-1
Styrene
ND ug/kg
3.1
1
05/11/11 17:38
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
3.1
1
05/11/11 17:38
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
3.1
1
05/11/11 17:38
79-34-5
Tetrachloroethene
ND ug/kg
3.1
1
05/11/11 17:38
127-18-4
Toluene
ND ug/kg
3.1
1
05/11/11 17:38
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
3.1
1
05/11/11 17:38
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
3.1
1
05/11/11 17:38
120-82-1
1,1,1-Trichloroethane
ND ug/kg
3.1
1
05/11/11 17:38
71-55-6
1,1,2-Trichloroethane
ND ug/kg
3.1
1
05/11/11 17:38
79-00-5
Trichloroethene
ND ug/kg
3.1
1
05/11/11 17:38
79-01-6
Trichlorofluoromethane
ND ug/kg
3.1
1
05/11/11 17:38
75-69-4
1,2,3-Trichloropropane
ND ug/kg
3.1
1
05/11/11 17:38
96-18-4
1,2,4-Trimethylbenzene
ND ug/kg
3.1
1
05/11/11 17:38
95-63-6
1,3,5-Trimethylbenzene
ND ug/kg
3.1
1
05/11/11 17:38
108-67-8
Vinyl acetate
ND ug/kg
31.2
1
05/11/11 17:38
108-05-4
Vinyl chloride
ND ug/kg
6.2
1
05/11/11 17:38
75-01-4
Xylene (Total)
ND ug/kg
6.2
1
05/11/11 17:38
1330-20-7
m&p-Xylene
ND ug/kg
6.2
1
05/11/11 17:38
179601-23-1
o-Xylene
ND ug/kg
3.1
1
05/11/11 17:38
95-47-6
Dibromofluoromethane (S)
98 %
70-130
1
05/11/11 17:38
1868-53-7
Toluene-d8 (S)
100 %
70-130
1
05/11/11 17:38
2037-26-5
4-Bromofluorobenzene (S)
95 %
70-130
1
05/11/11 17:38
460-00-4
1,2-Dichloroethane-d4 (S)
100 %
70-132
1
05/11/11 17:38
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
18.7 %
0.10
1
05/11/11 18:43
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 111 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-6 Lab ID: 9293679035 Collected: 05/06/11 00:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
9071 Oil and Grease
Analytical Method: 9071 B Preparation Method: 9071 B
Oil and Grease
ND mg/kg
87.2
1
05/11/11 10:45
05/11/11 11:21
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
83-32-9
Acenaphthylene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
208-96-8
Aniline
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
62-53-3
Anthracene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
120-12-7
Benzo(a)anthracene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
56-55-3
Benzo(a)pyrene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
50-32-8
Benzo(b)fluoranthene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
191-24-2
Benzo(k)fluoranthene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
207-08-9
Benzoic Acid
ND ug/kg
2060
1
05/14/11 10:32
05/17/11 18:38
65-85-0
Benzyl alcohol
ND ug/kg
822
1
05/14/11 10:32
05/17/11 18:38
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
101-55-3
Butylbenzylphthalate
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
85-68-7
4-Chloro-3-methylphenol
ND ug/kg
822
1
05/14/11 10:32
05/17/11 18:38
59-50-7
4-Chloroaniline
ND ug/kg
2060
1
05/14/11 10:32
05/17/11 18:38
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
108-60-1
2-Chloronaphthalene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
91-58-7
2-Chlorophenol
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
7005-72-3
Chrysene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
53-70-3
Dibenzofuran
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
132-64-9
1,2-Dichlorobenzene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
95-50-1
1,3-Dichlorobenzene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
541-73-1
1,4-Dichlorobenzene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
2060
1
05/14/11 10:32
05/17/11 18:38
91-94-1
2,4-Dichlorophenol
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
120-83-2
Diethylphthalate
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
84-66-2
2,4-Dimethylphenol
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
105-67-9
Dimethylphthalate
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
131-11-3
Di-n-butylphthalate
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
84-74-2
4,6-Dinitro-2-methylphenol
ND ug/kg
822
1
05/14/11 10:32
05/17/11 18:38
534-52-1
2,4-Dinitrophenol
ND ug/kg
2060
1
05/14/11 10:32
05/17/11 18:38
51-28-5
2,4-Dinitrotoluene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
121-14-2
2,6-Dinitrotoluene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
606-20-2
Di-n-octylphthalate
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
117-81-7
Fluoranthene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
206-44-0
Fluorene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
87-68-3
Hexachlorobenzene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
118-74-1
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 112 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-6 Lab ID: 9293679035 Collected: 05/06/11 00:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Hexachlorocyclopentadiene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
77-47-4
Hexachloroethane
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
193-39-5
Isophorone
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
78-59-1
1-Methylnaphthalene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
90-12-0
2-Methylnaphthalene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
Naphthalene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
91-20-3
2-Nitroaniline
ND ug/kg
2060
1
05/14/11 10:32
05/17/11 18:38
88-74-4
3-Nitroaniline
ND ug/kg
2060
1
05/14/11 10:32
05/17/11 18:38
99-09-2
4-Nitroaniline
ND ug/kg
822
1
05/14/11 10:32
05/17/11 18:38
100-01-6
Nitrobenzene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
98-95-3
2-Nitrophenol
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
88-75-5
4-Nitrophenol
ND ug/kg
2060
1
05/14/11 10:32
05/17/11 18:38
100-02-7
N-Nitrosodimethylamine
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
86-30-6
Pentachlorophenol
ND ug/kg
2060
1
05/14/11 10:32
05/17/11 18:38
87-86-5
Phenanthrene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
85-01-8
Phenol
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
108-95-2
Pyrene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
411
1
05/14/11 10:32
05/17/11 18:38
88-06-2
Nitrobenzene-d5 (S)
50 %
23-110
1
05/14/11 10:32
05/17/11 18:38
4165-60-0
2-Fluorobiphenyl (S)
52 %
30-110
1
05/14/11 10:32
05/17/11 18:38
321-60-8
Terphenyl-d14 (S)
66 %
28-110
1
05/14/11 10:32
05/17/11 18:38
1718-51-0
Phenol-d6 (S)
42 %
22-110
1
05/14/11 10:32
05/17/11 18:38
13127-88-3
2-Fluorophenol (S)
48 %
13-110
1
05/14/11 10:32
05/17/11 18:38
367-12-4
2,4,6-Tribromophenol (S)
41 %
27-110
1
05/14/11 10:32
05/17/11 18:38
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND ug/kg
65.0
1
05/11/11 17:58
67-64-1
Benzene
ND ug/kg
3.3
1
05/11/11 17:58
71-43-2
Bromobenzene
ND ug/kg
3.3
1
05/11/11 17:58
108-86-1
Bromochloromethane
ND ug/kg
3.3
1
05/11/11 17:58
74-97-5
Bromodichloromethane
ND ug/kg
3.3
1
05/11/11 17:58
75-27-4
Bromoform
ND ug/kg
3.3
1
05/11/11 17:58
75-25-2
Bromomethane
ND ug/kg
6.5
1
05/11/11 17:58
74-83-9
2-Butanone (MEK)
ND ug/kg
65.0
1
05/11/11 17:58
78-93-3
n-Butylbenzene
ND ug/kg
3.3
1
05/11/11 17:58
104-51-8
sec -Butyl benzene
ND ug/kg
3.3
1
05/11/11 17:58
135-98-8
tert-Butyl benzene
ND ug/kg
3.3
1
05/11/11 17:58
98-06-6
Carbon tetrachloride
ND ug/kg
3.3
1
05/11/11 17:58
56-23-5
Chlorobenzene
ND ug/kg
3.3
1
05/11/11 17:58
108-90-7
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 113 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-6 Lab ID: 9293679035 Collected: 05/06/11 00:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
Chloroethane
ND ug/kg
6.5
1
05/11/11 17:58
75-00-3
Chloroform
ND ug/kg
3.3
1
05/11/11 17:58
67-66-3
Chloromethane
ND ug/kg
6.5
1
05/11/11 17:58
74-87-3
2-Chlorotoluene
ND ug/kg
3.3
1
05/11/11 17:58
95-49-8
4-Chlorotoluene
ND ug/kg
3.3
1
05/11/11 17:58
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
3.3
1
05/11/11 17:58
96-12-8
Dibromochloromethane
ND ug/kg
3.3
1
05/11/11 17:58
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
3.3
1
05/11/11 17:58
106-93-4
Dibromomethane
ND ug/kg
3.3
1
05/11/11 17:58
74-95-3
1,2-Dichlorobenzene
ND ug/kg
3.3
1
05/11/11 17:58
95-50-1
1,3-Dichlorobenzene
ND ug/kg
3.3
1
05/11/11 17:58
541-73-1
1,4-Dichlorobenzene
ND ug/kg
3.3
1
05/11/11 17:58
106-46-7
Dichlorodifluoromethane
ND ug/kg
6.5
1
05/11/11 17:58
75-71-8
1,1-Dichloroethane
ND ug/kg
3.3
1
05/11/11 17:58
75-34-3
1,2-Dichloroethane
ND ug/kg
3.3
1
05/11/11 17:58
107-06-2
1,1-Dichloroethene
ND ug/kg
3.3
1
05/11/11 17:58
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
3.3
1
05/11/11 17:58
156-59-2
trans- 1,2-Dichloroethene
ND ug/kg
3.3
1
05/11/11 17:58
156-60-5
1,2-Dichloropropane
ND ug/kg
3.3
1
05/11/11 17:58
78-87-5
1,3-Dichloropropane
ND ug/kg
3.3
1
05/11/11 17:58
142-28-9
2,2-Dichloropropane
ND ug/kg
3.3
1
05/11/11 17:58
594-20-7
1,1-Dichloropropene
ND ug/kg
3.3
1
05/11/11 17:58
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
3.3
1
05/11/11 17:58
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
3.3
1
05/11/11 17:58
10061-02-6
Diisopropyl ether
ND ug/kg
3.3
1
05/11/11 17:58
108-20-3
Ethylbenzene
ND ug/kg
3.3
1
05/11/11 17:58
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
3.3
1
05/11/11 17:58
87-68-3
2-Hexanone
ND ug/kg
32.5
1
05/11/11 17:58
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
3.3
1
05/11/11 17:58
98-82-8
p-Isopropyltoluene
ND ug/kg
3.3
1
05/11/11 17:58
99-87-6
Methylene Chloride
ND ug/kg
13.0
1
05/11/11 17:58
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
32.5
1
05/11/11 17:58
108-10-1
Methyl-tert-butyl ether
ND ug/kg
3.3
1
05/11/11 17:58
1634-04-4
Naphthalene
ND ug/kg
3.3
1
05/11/11 17:58
91-20-3
n-Propylbenzene
ND ug/kg
3.3
1
05/11/11 17:58
103-65-1
Styrene
ND ug/kg
3.3
1
05/11/11 17:58
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
3.3
1
05/11/11 17:58
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
3.3
1
05/11/11 17:58
79-34-5
Tetrachloroethene
ND ug/kg
3.3
1
05/11/11 17:58
127-18-4
Toluene
ND ug/kg
3.3
1
05/11/11 17:58
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
3.3
1
05/11/11 17:58
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
3.3
1
05/11/11 17:58
120-82-1
1,1,1-Trichloroethane
ND ug/kg
3.3
1
05/11/11 17:58
71-55-6
1,1,2-Trichloroethane
ND ug/kg
3.3
1
05/11/11 17:58
79-00-5
Trichloroethene
ND ug/kg
3.3
1
05/11/11 17:58
79-01-6
Trichlorofluoromethane
ND ug/kg
3.3
1
05/11/11 17:58
75-69-4
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 114 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: S-6 Lab ID: 9293679035 Collected: 05/06/11 00:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,2,3-Trichloropropane
ND ug/kg
3.3
1
05/11/11 17:58
96-18-4
1,2,4-Trimethylbenzene
ND ug/kg
3.3
1
05/11/11 17:58
95-63-6
1,3,5-Trimethylbenzene
ND ug/kg
3.3
1
05/11/11 17:58
108-67-8
Vinyl acetate
ND ug/kg
32.5
1
05/11/11 17:58
108-05-4
Vinyl chloride
ND ug/kg
6.5
1
05/11/11 17:58
75-01-4
Xylene (Total)
ND ug/kg
6.5
1
05/11/11 17:58
1330-20-7
m&p-Xylene
ND ug/kg
6.5
1
05/11/11 17:58
179601-23-1
o-Xylene
ND ug/kg
3.3
1
05/11/11 17:58
95-47-6
Dibromofluoromethane (S)
106 %
70-130
1
05/11/11 17:58
1868-53-7
Toluene-d8 (S)
100 %
70-130
1
05/11/11 17:58
2037-26-5
4-Bromofluorobenzene (S)
89 %
70-130
1
05/11/11 17:58
460-00-4
1,2-Dichloroethane-d4 (S)
101 %
70-132
1
05/11/11 17:58
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
19.7 %
0.10
1
05/11/11 18:43
Sample: S-9 Lab ID: 9293679036 Collected: 05/06/11 12:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
36400 mg/kg
83.6
10
05/12/11 15:15
05/16/11 12:25
7429-90-5
Antimony
ND mg/kg
0.42
1
05/12/11 15:15
05/14/11 15:53
7440-36-0
Arsenic
1.3 mg/kg
0.42
1
05/12/11 15:15
05/16/11 10:23
7440-38-2
Barium
119 mg/kg
0.42
1
05/12/11 15:15
05/14/11 15:53
7440-39-3
Beryllium
0.89 mg/kg
0.084
1
05/12/11 15:15
05/14/11 15:53
7440-41-7
Cadmium
2.9 mg/kg
0.084
1
05/12/11 15:15
05/14/11 15:53
7440-43-9
Calcium
797 mg/kg
8.4
1
05/12/11 15:15
05/14/11 15:53
7440-70-2
Chromium
32.5 mg/kg
0.42
1
05/12/11 15:15
05/14/11 15:53
7440-47-3
Cobalt
ND mg/kg
0.42
1
05/12/11 15:15
05/14/11 15:53
7440-48-4
Copper
22.8 mg/kg
0.42
1
05/12/11 15:15
05/14/11 15:53
7440-50-8
Iron
39300 mg/kg
41.8
10
05/12/11 15:15
05/16/11 12:25
7439-89-6
Lead
8.7 mg/kg
0.42
1
05/12/11 15:15
05/14/11 15:53
7439-92-1
Magnesium
3510 mg/kg
8.4
1
05/12/11 15:15
05/14/11 15:53
7439-95-4
Manganese
121 mg/kg
0.42
1
05/12/11 15:15
05/14/11 15:53
7439-96-5
Nickel
13.5 mg/kg
0.42
1
05/12/11 15:15
05/14/11 15:53
7440-02-0
Potassium
5600 mg/kg
418
1
05/12/11 15:15
05/14/11 15:53
7440-09-7
Selenium
1.0 mg/kg
0.84
1
05/12/11 15:15
05/16/11 10:23
7782-49-2
Silver
ND mg/kg
0.42
1
05/12/11 15:15
05/14/11 15:53
7440-22-4
Sodium
ND mg/kg
418
1
05/12/11 15:15
05/14/11 15:53
7440-23-5
Thallium
ND mg/kg
0.84
1
05/12/11 15:15
05/14/11 15:53
7440-28-0
Vanadium
42.6 mg/kg
0.42
1
05/12/11 15:15
05/14/11 15:53
7440-62-2
Zinc
49.2 mg/kg
0.84
1
05/12/11 15:15
05/14/11 15:53
7440-66-6
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 115 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-9 Lab ID: 9293679036 Collected: 05/06/11 12:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7471 Mercury
Analytical Method: EPA 7471
Preparation Method: EPA 7471
Mercury
0.053 mg/kg
0.0044
1
05/13/11 08:45
05/13/11 16:40
7439-97-6
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
83-32-9
Acenaphthylene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
208-96-8
Aniline
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
62-53-3
Anthracene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
120-12-7
Benzo(a)anthracene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
56-55-3
Benzo(a)pyrene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
50-32-8
Benzo(b)fluoranthene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
191-24-2
Benzo(k)fluoranthene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
207-08-9
Benzoic Acid
ND ug/kg
1990
1
05/14/11 10:32
05/17/11 19:05
65-85-0
Benzyl alcohol
ND ug/kg
795
1
05/14/11 10:32
05/17/11 19:05
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
101-55-3
Butylbenzylphthalate
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
85-68-7
4-Chloro-3-methylphenol
ND ug/kg
795
1
05/14/11 10:32
05/17/11 19:05
59-50-7
4-Chloroaniline
ND ug/kg
1990
1
05/14/11 10:32
05/17/11 19:05
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
108-60-1
2-Chloronaphthalene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
91-58-7
2-Chlorophenol
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
7005-72-3
Chrysene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
53-70-3
Dibenzofuran
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
132-64-9
1,2-Dichlorobenzene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
95-50-1
1,3-Dichlorobenzene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
541-73-1
1,4-Dichlorobenzene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
1990
1
05/14/11 10:32
05/17/11 19:05
91-94-1
2,4-Dichlorophenol
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
120-83-2
Diethylphthalate
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
84-66-2
2,4-Dimethylphenol
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
105-67-9
Dimethylphthalate
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
131-11-3
Di-n-butylphthalate
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
84-74-2
4,6-Dinitro-2-methylphenol
ND ug/kg
795
1
05/14/11 10:32
05/17/11 19:05
534-52-1
2,4-Dinitrophenol
ND ug/kg
1990
1
05/14/11 10:32
05/17/11 19:05
51-28-5
2,4-Dinitrotoluene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
121-14-2
2,6-Dinitrotoluene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
606-20-2
Di-n-octylphthalate
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
117-81-7
Fluoranthene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
206-44-0
Fluorene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
87-68-3
Hexachlorobenzene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
118-74-1
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 116 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-9 Lab ID: 9293679036 Collected: 05/06/11 12:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Hexachlorocyclopentadiene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
77-47-4
Hexachloroethane
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
193-39-5
Isophorone
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
78-59-1
1-Methylnaphthalene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
90-12-0
2-Methylnaphthalene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
Naphthalene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
91-20-3
2-Nitroaniline
ND ug/kg
1990
1
05/14/11 10:32
05/17/11 19:05
88-74-4
3-Nitroaniline
ND ug/kg
1990
1
05/14/11 10:32
05/17/11 19:05
99-09-2
4-Nitroaniline
ND ug/kg
795
1
05/14/11 10:32
05/17/11 19:05
100-01-6
Nitrobenzene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
98-95-3
2-Nitrophenol
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
88-75-5
4-Nitrophenol
ND ug/kg
1990
1
05/14/11 10:32
05/17/11 19:05
100-02-7
N-Nitrosodimethylamine
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
86-30-6
Pentachlorophenol
ND ug/kg
1990
1
05/14/11 10:32
05/17/11 19:05
87-86-5
Phenanthrene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
85-01-8
Phenol
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
108-95-2
Pyrene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
397
1
05/14/11 10:32
05/17/11 19:05
88-06-2
Nitrobenzene-d5 (S)
53 %
23-110
1
05/14/11 10:32
05/17/11 19:05
4165-60-0
2-Fluorobiphenyl (S)
58 %
30-110
1
05/14/11 10:32
05/17/11 19:05
321-60-8
Terphenyl-d14 (S)
71 %
28-110
1
05/14/11 10:32
05/17/11 19:05
1718-51-0
Phenol-d6 (S)
43 %
22-110
1
05/14/11 10:32
05/17/11 19:05
13127-88-3
2-Fluorophenol (S)
47 %
13-110
1
05/14/11 10:32
05/17/11 19:05
367-12-4
2,4,6-Tribromophenol (S)
41 %
27-110
1
05/14/11 10:32
05/17/11 19:05
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND ug/kg
64.7
1
05/11/11 18:18
67-64-1
Benzene
ND ug/kg
3.2
1
05/11/11 18:18
71-43-2
Bromobenzene
ND ug/kg
3.2
1
05/11/11 18:18
108-86-1
Bromochloromethane
ND ug/kg
3.2
1
05/11/11 18:18
74-97-5
Bromodichloromethane
ND ug/kg
3.2
1
05/11/11 18:18
75-27-4
Bromoform
ND ug/kg
3.2
1
05/11/11 18:18
75-25-2
Bromomethane
ND ug/kg
6.5
1
05/11/11 18:18
74-83-9
2-Butanone (MEK)
ND ug/kg
64.7
1
05/11/11 18:18
78-93-3
n-Butylbenzene
ND ug/kg
3.2
1
05/11/11 18:18
104-51-8
sec -Butyl benzene
ND ug/kg
3.2
1
05/11/11 18:18
135-98-8
tert-Butyl benzene
ND ug/kg
3.2
1
05/11/11 18:18
98-06-6
Carbon tetrachloride
ND ug/kg
3.2
1
05/11/11 18:18
56-23-5
Chlorobenzene
ND ug/kg
3.2
1
05/11/11 18:18
108-90-7
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 117 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-9 Lab ID: 9293679036 Collected: 05/06/11 12:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
Chloroethane
ND ug/kg
6.5
1
05/11/11 18:18
75-00-3
Chloroform
ND ug/kg
3.2
1
05/11/11 18:18
67-66-3
Chloromethane
ND ug/kg
6.5
1
05/11/11 18:18
74-87-3
2-Chlorotoluene
ND ug/kg
3.2
1
05/11/11 18:18
95-49-8
4-Chlorotoluene
ND ug/kg
3.2
1
05/11/11 18:18
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
3.2
1
05/11/11 18:18
96-12-8
Dibromochloromethane
ND ug/kg
3.2
1
05/11/11 18:18
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
3.2
1
05/11/11 18:18
106-93-4
Dibromomethane
ND ug/kg
3.2
1
05/11/11 18:18
74-95-3
1,2-Dichlorobenzene
ND ug/kg
3.2
1
05/11/11 18:18
95-50-1
1,3-Dichlorobenzene
ND ug/kg
3.2
1
05/11/11 18:18
541-73-1
1,4-Dichlorobenzene
ND ug/kg
3.2
1
05/11/11 18:18
106-46-7
Dichlorodifluoromethane
ND ug/kg
6.5
1
05/11/11 18:18
75-71-8
1,1-Dichloroethane
ND ug/kg
3.2
1
05/11/11 18:18
75-34-3
1,2-Dichloroethane
ND ug/kg
3.2
1
05/11/11 18:18
107-06-2
1,1-Dichloroethene
ND ug/kg
3.2
1
05/11/11 18:18
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
3.2
1
05/11/11 18:18
156-59-2
trans- 1,2-Dichloroethene
ND ug/kg
3.2
1
05/11/11 18:18
156-60-5
1,2-Dichloropropane
ND ug/kg
3.2
1
05/11/11 18:18
78-87-5
1,3-Dichloropropane
ND ug/kg
3.2
1
05/11/11 18:18
142-28-9
2,2-Dichloropropane
ND ug/kg
3.2
1
05/11/11 18:18
594-20-7
1,1-Dichloropropene
ND ug/kg
3.2
1
05/11/11 18:18
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
3.2
1
05/11/11 18:18
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
3.2
1
05/11/11 18:18
10061-02-6
Diisopropyl ether
ND ug/kg
3.2
1
05/11/11 18:18
108-20-3
Ethylbenzene
ND ug/kg
3.2
1
05/11/11 18:18
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
3.2
1
05/11/11 18:18
87-68-3
2-Hexanone
ND ug/kg
32.3
1
05/11/11 18:18
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
3.2
1
05/11/11 18:18
98-82-8
p-Isopropyltoluene
ND ug/kg
3.2
1
05/11/11 18:18
99-87-6
Methylene Chloride
ND ug/kg
12.9
1
05/11/11 18:18
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
32.3
1
05/11/11 18:18
108-10-1
Methyl-tert-butyl ether
ND ug/kg
3.2
1
05/11/11 18:18
1634-04-4
Naphthalene
ND ug/kg
3.2
1
05/11/11 18:18
91-20-3
n-Propylbenzene
ND ug/kg
3.2
1
05/11/11 18:18
103-65-1
Styrene
ND ug/kg
3.2
1
05/11/11 18:18
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
3.2
1
05/11/11 18:18
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
3.2
1
05/11/11 18:18
79-34-5
Tetrachloroethene
ND ug/kg
3.2
1
05/11/11 18:18
127-18-4
Toluene
ND ug/kg
3.2
1
05/11/11 18:18
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
3.2
1
05/11/11 18:18
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
3.2
1
05/11/11 18:18
120-82-1
1,1,1-Trichloroethane
ND ug/kg
3.2
1
05/11/11 18:18
71-55-6
1,1,2-Trichloroethane
ND ug/kg
3.2
1
05/11/11 18:18
79-00-5
Trichloroethene
ND ug/kg
3.2
1
05/11/11 18:18
79-01-6
Trichlorofluoromethane
ND ug/kg
3.2
1
05/11/11 18:18
75-69-4
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 118 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: S-9 Lab ID: 9293679036 Collected: 05/06/11 12:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1, 3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Dibromofluoromethane (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
108 %
100 %
90 %
101 %
Analytical Method: ASTM D2974-87
17.0 %
3.2
1
05/11/11 18:18
96-18-4
3.2
1
05/11/11 18:18
95-63-6
3.2
1
05/11/11 18:18
108-67-8
32.3
1
05/11/11 18:18
108-05-4
6.5
1
05/11/11 18:18
75-01-4
6.5
1
05/11/11 18:18
1330-20-7
6.5
1
05/11/11 18:18
179601-23-1
3.2
1
05/11/11 18:18
95-47-6
70-130
1
05/11/11 18:18
1868-53-7
70-130
1
05/11/11 18:18
2037-26-5
70-130
1
05/11/11 18:18
460-00-4
70-132
1
05/11/11 18:18
17060-07-0
0.10 1
05/11/11 18:43
Sample: Myers MW-15 Lab ID: 9293679037 Collected: 05/05/11 09:30
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF
Received: 05/07/11 10:40 Matrix: Solid
Prepared Analyzed CAS No. Qual
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-CO8)
ND mg/kg
2.3
1
05/17/11 16:18
05/17/11 22:03
N2
Aliphatic (C09-C12)
ND mg/kg
2.3
1
05/17/11 16:18
05/17/11 22:03
N2
Aromatic (C09-C10)
ND mg/kg
2.3
1
05/17/11 16:18
05/17/11 22:03
N2
2,5-Dibromotoluene (PID)(S)
150 %
70-130
1
05/17/11 16:18
05/17/11 22:03
2,5-Dibromotoluene (FID)(S)
146 %
70-130
1
05/17/11 16:18
05/17/11 22:03
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Lead
6.8 mg/kg
0.55
1
05/12/11 15:15
05/14/11 16:00
7439-92-1
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND ug/kg
108
1
05/11/11 18:38
67-64-1
Benzene
ND ug/kg
5.4
1
05/11/11 18:38
71-43-2
Bromobenzene
ND ug/kg
5.4
1
05/11/11 18:38
108-86-1
Bromochloromethane
ND ug/kg
5.4
1
05/11/11 18:38
74-97-5
Bromodichloromethane
ND ug/kg
5.4
1
05/11/11 18:38
75-27-4
Bromoform
ND ug/kg
5.4
1
05/11/11 18:38
75-25-2
Bromomethane
ND ug/kg
10.8
1
05/11/11 18:38
74-83-9
2-Butanone (MEK)
ND ug/kg
108
1
05/11/11 18:38
78-93-3
n-Butylbenzene
ND ug/kg
5.4
1
05/11/11 18:38
104-51-8
sec -Butyl benzene
ND ug/kg
5.4
1
05/11/11 18:38
135-98-8
tert-Butyl benzene
ND ug/kg
5.4
1
05/11/11 18:38
98-06-6
Carbon tetrachloride
ND ug/kg
5.4
1
05/11/11 18:38
56-23-5
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 119 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: Myers MW-15 Lab ID: 9293679037 Collected: 05/05/11 09:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
Chlorobenzene
ND ug/kg
5.4
1
05/11/11 18:38
108-90-7
Chloroethane
ND ug/kg
10.8
1
05/11/11 18:38
75-00-3
Chloroform
ND ug/kg
5.4
1
05/11/11 18:38
67-66-3
Chloromethane
ND ug/kg
10.8
1
05/11/11 18:38
74-87-3
2-Chlorotoluene
ND ug/kg
5.4
1
05/11/11 18:38
95-49-8
4-Chlorotoluene
ND ug/kg
5.4
1
05/11/11 18:38
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
5.4
1
05/11/11 18:38
96-12-8
Dibromochloromethane
ND ug/kg
5.4
1
05/11/11 18:38
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
5.4
1
05/11/11 18:38
106-93-4
Dibromomethane
ND ug/kg
5.4
1
05/11/11 18:38
74-95-3
1,2-Dichlorobenzene
ND ug/kg
5.4
1
05/11/11 18:38
95-50-1
1,3-Dichlorobenzene
ND ug/kg
5.4
1
05/11/11 18:38
541-73-1
1,4-Dichlorobenzene
ND ug/kg
5.4
1
05/11/11 18:38
106-46-7
Dichlorodifluoromethane
ND ug/kg
10.8
1
05/11/11 18:38
75-71-8
1,1-Dichloroethane
ND ug/kg
5.4
1
05/11/11 18:38
75-34-3
1,2-Dichloroethane
ND ug/kg
5.4
1
05/11/11 18:38
107-06-2
1,1-Dichloroethene
ND ug/kg
5.4
1
05/11/11 18:38
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
5.4
1
05/11/11 18:38
156-59-2
trans- 1,2-Dichloroethene
ND ug/kg
5.4
1
05/11/11 18:38
156-60-5
1,2-Dichloropropane
ND ug/kg
5.4
1
05/11/11 18:38
78-87-5
1,3-Dichloropropane
ND ug/kg
5.4
1
05/11/11 18:38
142-28-9
2,2-Dichloropropane
ND ug/kg
5.4
1
05/11/11 18:38
594-20-7
1,1-Dichloropropene
ND ug/kg
5.4
1
05/11/11 18:38
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
5.4
1
05/11/11 18:38
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
5.4
1
05/11/11 18:38
10061-02-6
Diisopropyl ether
ND ug/kg
5.4
1
05/11/11 18:38
108-20-3
Ethylbenzene
ND ug/kg
5.4
1
05/11/11 18:38
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
5.4
1
05/11/11 18:38
87-68-3
2-Hexanone
ND ug/kg
53.8
1
05/11/11 18:38
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
5.4
1
05/11/11 18:38
98-82-8
p-Isopropyltoluene
ND ug/kg
5.4
1
05/11/11 18:38
99-87-6
Methylene Chloride
ND ug/kg
21.5
1
05/11/11 18:38
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
53.8
1
05/11/11 18:38
108-10-1
Methyl-tert-butyl ether
ND ug/kg
5.4
1
05/11/11 18:38
1634-04-4
Naphthalene
ND ug/kg
5.4
1
05/11/11 18:38
91-20-3
n-Propylbenzene
ND ug/kg
5.4
1
05/11/11 18:38
103-65-1
Styrene
ND ug/kg
5.4
1
05/11/11 18:38
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
5.4
1
05/11/11 18:38
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
5.4
1
05/11/11 18:38
79-34-5
Tetrachloroethene
ND ug/kg
5.4
1
05/11/11 18:38
127-18-4
Toluene
ND ug/kg
5.4
1
05/11/11 18:38
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
5.4
1
05/11/11 18:38
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
5.4
1
05/11/11 18:38
120-82-1
1,1,1-Trichloroethane
ND ug/kg
5.4
1
05/11/11 18:38
71-55-6
1,1,2-Trichloroethane
ND ug/kg
5.4
1
05/11/11 18:38
79-00-5
Trichloroethene
ND ug/kg
5.4
1
05/11/11 18:38
79-01-6
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 120 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Myers MW-15 Lab ID: 9293679037 Collected: 05/05/11 09:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
Trichlorofluoromethane
ND ug/kg
5.4
1
05/11/11 18:38
75-69-4
1,2,3-Trichloropropane
ND ug/kg
5.4
1
05/11/11 18:38
96-18-4
1,2,4-Trimethylbenzene
ND ug/kg
5.4
1
05/11/11 18:38
95-63-6
1,3,5-Trimethylbenzene
ND ug/kg
5.4
1
05/11/11 18:38
108-67-8
Vinyl acetate
ND ug/kg
53.8
1
05/11/11 18:38
108-05-4
Vinyl chloride
ND ug/kg
10.8
1
05/11/11 18:38
75-01-4
Xylene (Total)
ND ug/kg
10.8
1
05/11/11 18:38
1330-20-7
m&p-Xylene
ND ug/kg
10.8
1
05/11/11 18:38
179601-23-1
o-Xylene
ND ug/kg
5.4
1
05/11/11 18:38
95-47-6
Dibromofluoromethane (S)
107 %
70-130
1
05/11/11 18:38
1868-53-7
Toluene-d8 (S)
101 %
70-130
1
05/11/11 18:38
2037-26-5
4-Bromofluorobenzene (S)
95 %
70-130
1
05/11/11 18:38
460-00-4
1,2-Dichloroethane-d4 (S)
104 %
70-132
1
05/11/11 18:38
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
30.8 %
0.10
1
05/11/11 18:43
Sample: Myers MW-15 Lab ID: 9293679038 Collected: 05/06/11 16:15 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-CO8)
ND ug/L
30.0
1
05/17/11 02:03
N2
Aliphatic (C09-C12)
452 ug/L
30.0
1
05/17/11 02:03
N2
Aromatic (C09-C10)
91.7 ug/L
30.0
1
05/17/11 02:03
N2
2,5-Dibromotoluene (PID)(S)
105 %
70-130
1
05/17/11 02:03
2,5-Dibromotoluene (FID)(S)
103 %
70-130
1
05/17/11 02:03
8260 MSV Low Level
Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/11/11 08:13
67-64-1
Benzene
ND ug/L
1.0
1
05/11/11 08:13
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/11/11 08:13
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/11/11 08:13
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
05/11/11 08:13
75-27-4
Bromoform
ND ug/L
1.0
1
05/11/11 08:13
75-25-2
Bromomethane
ND ug/L
2.0
1
05/11/11 08:13
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/11/11 08:13
78-93-3
Carbon tetrachloride
ND ug/L
1.0
1
05/11/11 08:13
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/11/11 08:13
108-90-7
Chloroethane
ND ug/L
1.0
1
05/11/11 08:13
75-00-3
Chloroform
ND ug/L
1.0
1
05/11/11 08:13
67-66-3
Chloromethane
ND ug/L
1.0
1
05/11/11 08:13
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/11/11 08:13
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/11/11 08:13
106-43-4
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 121 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: Myers MW-15 Lab ID: 9293679038 Collected: 05/06/11 16:15 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
1
05/11/11 08:13
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/11/11 08:13
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/11/11 08:13
106-93-4
Dibromomethane
ND ug/L
1.0
1
05/11/11 08:13
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 08:13
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 08:13
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 08:13
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/11/11 08:13
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
1
05/11/11 08:13
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/11/11 08:13
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
05/11/11 08:13
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 08:13
156-59-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 08:13
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 08:13
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/11/11 08:13
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 08:13
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/11/11 08:13
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 08:13
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 08:13
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/11/11 08:13
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/11/11 08:13
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/11/11 08:13
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/11/11 08:13
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
1
05/11/11 08:13
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/11/11 08:13
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/11/11 08:13
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/11/11 08:13
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/11/11 08:13
91-20-3
Styrene
ND ug/L
1.0
1
05/11/11 08:13
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 08:13
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 08:13
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
05/11/11 08:13
127-18-4
Toluene
ND ug/L
1.0
1
05/11/11 08:13
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 08:13
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 08:13
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/11/11 08:13
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/11/11 08:13
79-00-5
Trichloroethene
ND ug/L
1.0
1
05/11/11 08:13
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/11/11 08:13
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/11/11 08:13
96-18-4
Vinyl acetate
ND ug/L
2.0
1
05/11/11 08:13
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/11/11 08:13
75-01-4
m&p-Xylene
ND ug/L
2.0
1
05/11/11 08:13
179601-23-1
o-Xylene
ND ug/L
1.0
1
05/11/11 08:13
95-47-6
4-Bromofluorobenzene (S)
96 %
70-130
1
05/11/11 08:13
460-00-4
Dibromocuoromethane (S)
104 %
70-130
1
05/11/11 08:13
1868-53-7
1,2-Dichloroethane-d4 (S)
109 %
70-130
1
05/11/11 08:13
17060-07-0
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 122 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Myers MW-15 Lab ID: 9293679038 Collected: 05/06/11 16:15 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level
Toluene-d8 (S)
Analytical Method: EPA 8260
101 % 70-130 1 05/11/11 08:13 2037-26-5
Sample: MW-13 Lab ID: 9293679039 Collected: 05/05/11 14:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Nonatriacontane (S)
o-Terphenyl(S)
2-Fluorobiphenyl (S)
2-13romonaphthalene (S)
VPH NC Soil
Aliphatic (C05-CO8)
Aliphatic (C09-C12)
Aromatic (C09-C10)
2,5-Dibromotoluene (PID)(S)
2,5-Dibromotoluene (FID)(S)
8270 MSSV Microwave
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Date: 05/20/2011 04:57 PM
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
ND mg/kg
13.3
1
05/12/11 07:01
05/14/11 18:18
ND mg/kg
13.3
1
05/12/11 07:01
05/14/11 18:18
ND mg/kg
13.3
1
05/12/11 07:01
05/15/11 06:52
72 %
40-140
1
05/12/11 07:01
05/14/11 18:18
7194-86-7
76 %
40-140
1
05/12/11 07:01
05/15/11 06:52
84-15-1
100 %
40-140
1
05/12/11 07:01
05/15/11 06:52
321-60-8
104 %
40-140
1
05/12/11 07:01
05/15/11 06:52
580-13-2
Analytical Method: MADEP VPH Preparation Method:
MADEP VPH
ND mg/kg
2.0
1
05/17/11 16:18
05/17/11 22:28
ND mg/kg
2.0
1
05/17/11 16:18
05/17/11 22:28
ND mg/kg
2.0
1
05/17/11 16:18
05/17/11 22:28
136 %
70-130
1
05/17/11 16:18
05/17/11 22:28
137 %
70-130
1
05/17/11 16:18
05/17/11 22:28
Analytical Method: EPA 8270 Preparation Method:
EPA 3546
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
83-32-9
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
208-96-8
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
62-53-3
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
120-12-7
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
56-55-3
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
50-32-8
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
205-99-2
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
191-24-2
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
207-08-9
ND ug/kg
2190
1
05/16/11 08:50
05/18/11 16:07
65-85-0
ND ug/kg
876
1
05/16/11 08:50
05/18/11 16:07
100-51-6
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
101-55-3
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
85-68-7
ND ug/kg
876
1
05/16/11 08:50
05/18/11 16:07
59-50-7
ND ug/kg
2190
1
05/16/11 08:50
05/18/11 16:07
106-47-8
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
111-91-1
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
111-44-4
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
108-60-1
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
91-58-7
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
95-57-8
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
7005-72-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
N2
N2
N2
N2
N2
N2
Page 123 of 227

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-13 Lab ID: 9293679039 Collected: 05/05/11 14:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Chrysene
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
53-70-3
Dibenzofuran
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
132-64-9
1,2-Dichlorobenzene
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
95-50-1
1,3-Dichlorobenzene
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
541-73-1
1,4-Dichlorobenzene
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
2190
1
05/16/11 08:50
05/18/11 16:07
91-94-1
2,4-Dichlorophenol
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
120-83-2
Diethylphthalate
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
84-66-2
2,4-Dimethylphenol
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
105-67-9
Dimethylphthalate
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
131-11-3
Di-n-butylphthalate
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/kg
876
1
05/16/11 08:50
05/18/11 16:07
534-52-1
2,4-Dinitrophenol
ND ug/kg
2190
1
05/16/11 08:50
05/18/11 16:07
51-28-5
2,4-Dinitrotoluene
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
121-14-2
2,6-Dinitrotoluene
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
606-20-2
Di-n-octylphthalate
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
117-81-7
Fluoranthene
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
206-44-0
Fluorene
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
87-68-3
Hexachlorobenzene
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
77-47-4
Hexachloroethane
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
193-39-5
Isophorone
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
78-59-1
1-Methylnaphthalene
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
90-12-0
2-Methylnaphthalene
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
Naphthalene
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
91-20-3
2-Nitroaniline
ND ug/kg
2190
1
05/16/11 08:50
05/18/11 16:07
88-74-4
3-Nitroaniline
ND ug/kg
2190
1
05/16/11 08:50
05/18/11 16:07
99-09-2
4-Nitroaniline
ND ug/kg
876
1
05/16/11 08:50
05/18/11 16:07
100-01-6
Nitrobenzene
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
98-95-3
2-Nitrophenol
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
88-75-5
4-Nitrophenol
ND ug/kg
2190
1
05/16/11 08:50
05/18/11 16:07
100-02-7
N-Nitrosodimethylamine
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
86-30-6
Pentachlorophenol
ND ug/kg
2190
1
05/16/11 08:50
05/18/11 16:07
87-86-5
Phenanthrene
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
85-01-8
Phenol
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
108-95-2
Pyrene
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
95-95-4
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 124 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: MW-13 Lab ID: 9293679039 Collected: 05/05/11 14:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4,6-Trichlorophenol
ND ug/kg
438
1
05/16/11 08:50
05/18/11 16:07
88-06-2
Nitrobenzene-d5 (S)
56 %
23-110
1
05/16/11 08:50
05/18/11 16:07
4165-60-0
2-Fluorobiphenyl (S)
65 %
30-110
1
05/16/11 08:50
05/18/11 16:07
321-60-8
Terphenyl-d14 (S)
78 %
28-110
1
05/16/11 08:50
05/18/11 16:07
1718-51-0
Phenol-d6 (S)
47 %
22-110
1
05/16/11 08:50
05/18/11 16:07
13127-88-3
2-Fluorophenol (S)
53 %
13-110
1
05/16/11 08:50
05/18/11 16:07
367-12-4
2,4,6-Tribromophenol (S)
57 %
27-110
1
05/16/11 08:50
05/18/11 16:07
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND ug/kg
102
1
05/11/11 18:58
67-64-1
Benzene
ND ug/kg
5.1
1
05/11/11 18:58
71-43-2
Bromobenzene
ND ug/kg
5.1
1
05/11/11 18:58
108-86-1
Bromochloromethane
ND ug/kg
5.1
1
05/11/11 18:58
74-97-5
Bromodichloromethane
ND ug/kg
5.1
1
05/11/11 18:58
75-27-4
Bromoform
ND ug/kg
5.1
1
05/11/11 18:58
75-25-2
Bromomethane
ND ug/kg
10.2
1
05/11/11 18:58
74-83-9
2-Butanone (MEK)
ND ug/kg
102
1
05/11/11 18:58
78-93-3
n-Butylbenzene
ND ug/kg
5.1
1
05/11/11 18:58
104-51-8
sec -Butyl benzene
ND ug/kg
5.1
1
05/11/11 18:58
135-98-8
tert-Butyl benzene
ND ug/kg
5.1
1
05/11/11 18:58
98-06-6
Carbon tetrachloride
ND ug/kg
5.1
1
05/11/11 18:58
56-23-5
Chlorobenzene
ND ug/kg
5.1
1
05/11/11 18:58
108-90-7
Chloroethane
ND ug/kg
10.2
1
05/11/11 18:58
75-00-3
Chloroform
ND ug/kg
5.1
1
05/11/11 18:58
67-66-3
Chloromethane
ND ug/kg
10.2
1
05/11/11 18:58
74-87-3
2-Chlorotoluene
ND ug/kg
5.1
1
05/11/11 18:58
95-49-8
4-Chlorotoluene
ND ug/kg
5.1
1
05/11/11 18:58
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
5.1
1
05/11/11 18:58
96-12-8
Dibromochloromethane
ND ug/kg
5.1
1
05/11/11 18:58
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
5.1
1
05/11/11 18:58
106-93-4
Dibromomethane
ND ug/kg
5.1
1
05/11/11 18:58
74-95-3
1,2-Dichlorobenzene
ND ug/kg
5.1
1
05/11/11 18:58
95-50-1
1,3-Dichlorobenzene
ND ug/kg
5.1
1
05/11/11 18:58
541-73-1
1,4-Dichlorobenzene
ND ug/kg
5.1
1
05/11/11 18:58
106-46-7
Dichlorodifluoromethane
ND ug/kg
10.2
1
05/11/11 18:58
75-71-8
1,1-Dichloroethane
ND ug/kg
5.1
1
05/11/11 18:58
75-34-3
1,2-Dichloroethane
ND ug/kg
5.1
1
05/11/11 18:58
107-06-2
1,1-Dichloroethene
ND ug/kg
5.1
1
05/11/11 18:58
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
5.1
1
05/11/11 18:58
156-59-2
trans- 1,2-Dichloroethene
ND ug/kg
5.1
1
05/11/11 18:58
156-60-5
1,2-Dichloropropane
ND ug/kg
5.1
1
05/11/11 18:58
78-87-5
1,3-Dichloropropane
ND ug/kg
5.1
1
05/11/11 18:58
142-28-9
2,2-Dichloropropane
ND ug/kg
5.1
1
05/11/11 18:58
594-20-7
1,1-Dichloropropene
ND ug/kg
5.1
1
05/11/11 18:58
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
5.1
1
05/11/11 18:58
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
5.1
1
05/11/11 18:58
10061-02-6
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 125 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-13 Lab ID: 9293679039 Collected: 05/05/11 14:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
Diisopropyl ether
ND ug/kg
5.1
1
05/11/11 18:58
108-20-3
Ethylbenzene
ND ug/kg
5.1
1
05/11/11 18:58
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
5.1
1
05/11/11 18:58
87-68-3
2-Hexanone
ND ug/kg
51.1
1
05/11/11 18:58
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
5.1
1
05/11/11 18:58
98-82-8
p-Isopropyltoluene
ND ug/kg
5.1
1
05/11/11 18:58
99-87-6
Methylene Chloride
ND ug/kg
20.4
1
05/11/11 18:58
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
51.1
1
05/11/11 18:58
108-10-1
Methyl-tert-butyl ether
ND ug/kg
5.1
1
05/11/11 18:58
1634-04-4
Naphthalene
ND ug/kg
5.1
1
05/11/11 18:58
91-20-3
n-Propylbenzene
ND ug/kg
5.1
1
05/11/11 18:58
103-65-1
Styrene
ND ug/kg
5.1
1
05/11/11 18:58
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
5.1
1
05/11/11 18:58
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
5.1
1
05/11/11 18:58
79-34-5
Tetrachloroethene
ND ug/kg
5.1
1
05/11/11 18:58
127-18-4
Toluene
ND ug/kg
5.1
1
05/11/11 18:58
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
5.1
1
05/11/11 18:58
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
5.1
1
05/11/11 18:58
120-82-1
1,1,1-Trichloroethane
ND ug/kg
5.1
1
05/11/11 18:58
71-55-6
1,1,2-Trichloroethane
ND ug/kg
5.1
1
05/11/11 18:58
79-00-5
Trichloroethene
ND ug/kg
5.1
1
05/11/11 18:58
79-01-6
Trichlorofluoromethane
ND ug/kg
5.1
1
05/11/11 18:58
75-69-4
1,2,3-Trichloropropane
ND ug/kg
5.1
1
05/11/11 18:58
96-18-4
1,2,4-Trimethylbenzene
ND ug/kg
5.1
1
05/11/11 18:58
95-63-6
1,3,5-Trimethylbenzene
ND ug/kg
5.1
1
05/11/11 18:58
108-67-8
Vinyl acetate
ND ug/kg
51.1
1
05/11/11 18:58
108-05-4
Vinyl chloride
ND ug/kg
10.2
1
05/11/11 18:58
75-01-4
Xylene (Total)
ND ug/kg
10.2
1
05/11/11 18:58
1330-20-7
m&p-Xylene
ND ug/kg
10.2
1
05/11/11 18:58
179601-23-1
o-Xylene
ND ug/kg
5.1
1
05/11/11 18:58
95-47-6
Dibromofluoromethane (S)
108 %
70-130
1
05/11/11 18:58
1868-53-7
Toluene-d8 (S)
98 %
70-130
1
05/11/11 18:58
2037-26-5
4-Bromofluorobenzene (S)
92 %
70-130
1
05/11/11 18:58
460-00-4
1,2-Dichloroethane-d4 (S)
108 %
70-132
1
05/11/11 18:58
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
24.7 %
0.10
1
05/11/11 08:51
Sample: S-12 Lab ID: 9293679040 Collected: 05/06/11 13:25 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
9071 Oil and Grease Analytical Method: 9071 B Preparation Method: 9071 B
Oil and Grease 351 mg/kg 81.9 1 05/11/11 10:46 05/11/11 11:21
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 126 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-12 Lab ID: 9293679040 Collected: 05/06/11 13:25 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
83-32-9
Acenaphthylene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
208-96-8
Aniline
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
62-53-3
Anthracene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
120-12-7
Benzo(a)anthracene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
56-55-3
Benzo(a)pyrene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
50-32-8
Benzo(b)fluoranthene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
191-24-2
Benzo(k)fluoranthene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
207-08-9
Benzoic Acid
ND ug/kg
1930
1
05/16/11 08:50
05/18/11 16:35
65-85-0
Benzyl alcohol
ND ug/kg
772
1
05/16/11 08:50
05/18/11 16:35
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
101-55-3
Butylbenzylphthalate
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
85-68-7
4-Chloro-3-methylphenol
ND ug/kg
772
1
05/16/11 08:50
05/18/11 16:35
59-50-7
4-Chloroaniline
ND ug/kg
1930
1
05/16/11 08:50
05/18/11 16:35
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
108-60-1
2-Chloronaphthalene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
91-58-7
2-Chlorophenol
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
7005-72-3
Chrysene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
53-70-3
Dibenzofuran
460 ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
132-64-9
1,2-Dichlorobenzene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
95-50-1
1,3-Dichlorobenzene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
541-73-1
1,4-Dichlorobenzene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
1930
1
05/16/11 08:50
05/18/11 16:35
91-94-1
2,4-Dichlorophenol
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
120-83-2
Diethylphthalate
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
84-66-2
2,4-Dimethylphenol
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
105-67-9
Dimethylphthalate
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
131-11-3
Di-n-butylphthalate
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
84-74-2
4,6-Dinitro-2-methylphenol
ND ug/kg
772
1
05/16/11 08:50
05/18/11 16:35
534-52-1
2,4-Dinitrophenol
ND ug/kg
1930
1
05/16/11 08:50
05/18/11 16:35
51-28-5
2,4-Dinitrotoluene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
121-14-2
2,6-Dinitrotoluene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
606-20-2
Di-n-octylphthalate
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
117-81-7
Fluoranthene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
206-44-0
Fluorene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
87-68-3
Hexachlorobenzene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
77-47-4
Hexachloroethane
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
193-39-5
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 127 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: S-12 Lab ID: 9293679040 Collected: 05/06/11 13:25 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Isophorone
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
78-59-1
1-Methylnaphthalene
1700 ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
90-12-0
2-Methylnaphthalene
2310 ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
Naphthalene
1490 ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
91-20-3
2-Nitroaniline
ND ug/kg
1930
1
05/16/11 08:50
05/18/11 16:35
88-74-4
3-Nitroaniline
ND ug/kg
1930
1
05/16/11 08:50
05/18/11 16:35
99-09-2
4-Nitroaniline
ND ug/kg
772
1
05/16/11 08:50
05/18/11 16:35
100-01-6
Nitrobenzene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
98-95-3
2-Nitrophenol
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
88-75-5
4-Nitrophenol
ND ug/kg
1930
1
05/16/11 08:50
05/18/11 16:35
100-02-7
N-Nitrosodimethylamine
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
86-30-6
Pentachlorophenol
ND ug/kg
1930
1
05/16/11 08:50
05/18/11 16:35
87-86-5
Phenanthrene
940 ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
85-01-8
Phenol
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
108-95-2
Pyrene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
386
1
05/16/11 08:50
05/18/11 16:35
88-06-2
Nitrobenzene-d5 (S)
68 %
23-110
1
05/16/11 08:50
05/18/11 16:35
4165-60-0
2-Fluorobiphenyl (S)
79 %
30-110
1
05/16/11 08:50
05/18/11 16:35
321-60-8
Terphenyl-d14 (S)
85 %
28-110
1
05/16/11 08:50
05/18/11 16:35
1718-51-0
Phenol-d6 (S)
56 %
22-110
1
05/16/11 08:50
05/18/11 16:35
13127-88-3
2-Fluorophenol (S)
57 %
13-110
1
05/16/11 08:50
05/18/11 16:35
367-12-4
2,4,6-Tribromophenol (S)
72 %
27-110
1
05/16/11 08:50
05/18/11 16:35
118-79-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
14.5 %
0.10
1
05/12/11 09:30
Sample: S-13 Lab ID: 9293679041 Collected: 05/06/11 13:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
9071 Oil and Grease Analytical Method: 9071 B Preparation Method: 9071 B
Oil and Grease
97.4 mg/kg
78.7
1
05/11/11 10:47
05/11/11 11:21
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03 83-32-9
Acenaphthylene
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03 208-96-8
Aniline
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03 62-53-3
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 128 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: S-13 Lab ID: 9293679041 Collected: 05/06/11 13:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Anthracene
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
120-12-7
Benzo(a)anthracene
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
56-55-3
Benzo(a)pyrene
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
50-32-8
Benzo(b)fluoranthene
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
191-24-2
Benzo(k)fluoranthene
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
207-08-9
Benzoic Acid
ND ug/kg
1850
1
05/16/11 08:50
05/18/11 17:03
65-85-0
Benzyl alcohol
ND ug/kg
742
1
05/16/11 08:50
05/18/11 17:03
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
101-55-3
Butylbenzylphthalate
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
85-68-7
4-Chloro-3-methylphenol
ND ug/kg
742
1
05/16/11 08:50
05/18/11 17:03
59-50-7
4-Chloroaniline
ND ug/kg
1850
1
05/16/11 08:50
05/18/11 17:03
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
108-60-1
2-Chloronaphthalene
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
91-58-7
2-Chlorophenol
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
7005-72-3
Chrysene
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
53-70-3
Dibenzofuran
1170 ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
132-64-9
1,2-Dichlorobenzene
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
95-50-1
1,3-Dichlorobenzene
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
541-73-1
1,4-Dichlorobenzene
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
1850
1
05/16/11 08:50
05/18/11 17:03
91-94-1
2,4-Dichlorophenol
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
120-83-2
Diethylphthalate
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
84-66-2
2,4-Dimethylphenol
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
105-67-9
Dimethylphthalate
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
131-11-3
Di-n-butylphthalate
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
84-74-2
4,6-Dinitro-2-methylphenol
ND ug/kg
742
1
05/16/11 08:50
05/18/11 17:03
534-52-1
2,4-Dinitrophenol
ND ug/kg
1850
1
05/16/11 08:50
05/18/11 17:03
51-28-5
2,4-Dinitrotoluene
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
121-14-2
2,6-Dinitrotoluene
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
606-20-2
Di-n-octylphthalate
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
117-81-7
Fluoranthene
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
206-44-0
Fluorene
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
87-68-3
Hexachlorobenzene
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
77-47-4
Hexachloroethane
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
193-39-5
Isophorone
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
78-59-1
1-Methylnaphthalene
3760 ug/kg
742
2
05/16/11 08:50
05/19/11 10:21
90-12-0
2-Methylnaphthalene
5170 ug/kg
742
2
05/16/11 08:50
05/19/11 10:21
91-57-6
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 129 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: S-13 Lab ID: 9293679041 Collected: 05/06/11 13:30 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-N itroso-d i-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Percent Moisture
Percent Moisture
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
95-48-7
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
3680 ug/kg
742
2
05/16/11 08:50
05/19/11 10:21
91-20-3
ND ug/kg
1850
1
05/16/11 08:50
05/18/11 17:03
88-74-4
ND ug/kg
1850
1
05/16/11 08:50
05/18/11 17:03
99-09-2
ND ug/kg
742
1
05/16/11 08:50
05/18/11 17:03
100-01-6
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
98-95-3
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
88-75-5
ND ug/kg
1850
1
05/16/11 08:50
05/18/11 17:03
100-02-7
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
62-75-9
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
621-64-7
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
86-30-6
ND ug/kg
1850
1
05/16/11 08:50
05/18/11 17:03
87-86-5
2080 ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
85-01-8
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
108-95-2
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
129-00-0
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
120-82-1
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
95-95-4
ND ug/kg
371
1
05/16/11 08:50
05/18/11 17:03
88-06-2
67 %
23-110
1
05/16/11 08:50
05/18/11 17:03
4165-60-0
79 %
30-110
1
05/16/11 08:50
05/18/11 17:03
321-60-8
64 %
28-110
1
05/16/11 08:50
05/18/11 17:03
1718-51-0
45 %
22-110
1
05/16/11 08:50
05/18/11 17:03
13127-88-3
48 %
13-110
1
05/16/11 08:50
05/18/11 17:03
367-12-4
57 %
27-110
1
05/16/11 08:50
05/18/11 17:03
118-79-6
Analytical Method: ASTM D2974-87
11.0 % 0.10 1 05/12/11 09:31
Sample: S-14 Lab ID: 9293679042 Collected: 05/06/11 13:40 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
9071 Oil and Grease
Analytical Method: 9071 B Preparation Method: 9071 B
Oil and Grease
ND mg/kg
85.9
1
05/11/11 10:47
05/11/11 11:21
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
83-32-9
Acenaphthylene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
208-96-8
Aniline
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
62-53-3
Anthracene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
120-12-7
Benzo(a)anthracene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
56-55-3
Benzo(a)pyrene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
50-32-8
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 130 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Sample: S-14 Lab ID: 9293679042 Collected: 05/06/11 13:40 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Benzo(b)fluoranthene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
Benzo(g,h,i)perylene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
Benzo(k)fluoranthene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
Benzoic Acid
ND ug/kg
2020
1
05/16/11 08:50
05/18/11 17:31
Benzyl alcohol
ND ug/kg
810
1
05/16/11 08:50
05/18/11 17:31
4-Bromophenylphenyl ether
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
Butylbenzylphthalate
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
4-Chloro-3-methylphenol
ND ug/kg
810
1
05/16/11 08:50
05/18/11 17:31
4-Chloroaniline
ND ug/kg
2020
1
05/16/11 08:50
05/18/11 17:31
bis(2-Chloroethoxy)methane
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
bis(2-Chloroethyl) ether
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
bis(2-Chloroisopropyl) ether
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
2-Chloronaphthalene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
2-Chlorophenol
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
4-Chlorophenylphenyl ether
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
Chrysene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
Dibenz(a,h)anthracene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
Dibenzofuran
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
1,2-Dichlorobenzene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
1,3-Dichlorobenzene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
1,4-Dichlorobenzene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
3,3'-Dichlorobenzidine
ND ug/kg
2020
1
05/16/11 08:50
05/18/11 17:31
2,4-Dichlorophenol
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
Diethylphthalate
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
2,4-Dimethylphenol
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
Dimethylphthalate
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
Di-n-butylphthalate
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
4,6-Dinitro-2-methylphenol
ND ug/kg
810
1
05/16/11 08:50
05/18/11 17:31
2,4-Dinitrophenol
ND ug/kg
2020
1
05/16/11 08:50
05/18/11 17:31
2,4-Dinitrotoluene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
2,6-Dinitrotoluene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
Di-n-octylphthalate
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
bis(2- Ethyl hexyl)phthalate
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
Fluoranthene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
Fluorene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
Hexachloro-1,3-butadiene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
Hexachlorobenzene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
Hexachlorocyclopentadiene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
Hexachloroethane
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
Indeno(1,2,3-cd)pyrene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
Isophorone
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
1-Methylnaphthalene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
2-Methylnaphthalene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
2-Methylphenol(o-Cresol)
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
3&4-Methylphenol(m&p Cresol)
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
Naphthalene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY
ANALYSIS
This report
shall not be reproduced, except
in
full,
without the written consent of Analytical Services, Inc..
PPace
[phone]
CAS No. Qual
205-99-2
191-24-2
207-08-9
65-85-0
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
95-50-1
541-73-1
106-46-7
91-94-1
120-83-2
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
90-12-0
91-57-6
95-48-7
91-20-3
Page 131 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: S-14 Lab ID: 9293679042 Collected: 05/06/11 13:40 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Nitroaniline
ND ug/kg
2020
1
05/16/11 08:50
05/18/11 17:31
88-74-4
3-Nitroaniline
ND ug/kg
2020
1
05/16/11 08:50
05/18/11 17:31
99-09-2
4-Nitroaniline
ND ug/kg
810
1
05/16/11 08:50
05/18/11 17:31
100-01-6
Nitrobenzene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
98-95-3
2-Nitrophenol
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
88-75-5
4-Nitrophenol
ND ug/kg
2020
1
05/16/11 08:50
05/18/11 17:31
100-02-7
N-Nitrosodimethylamine
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
86-30-6
Pentachlorophenol
ND ug/kg
2020
1
05/16/11 08:50
05/18/11 17:31
87-86-5
Phenanthrene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
85-01-8
Phenol
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
108-95-2
Pyrene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
405
1
05/16/11 08:50
05/18/11 17:31
88-06-2
Nitrobenzene-d5 (S)
62 %
23-110
1
05/16/11 08:50
05/18/11 17:31
4165-60-0
2-Fluorobiphenyl (S)
76 %
30-110
1
05/16/11 08:50
05/18/11 17:31
321-60-8
Terphenyl-d14 (S)
70 %
28-110
1
05/16/11 08:50
05/18/11 17:31
1718-51-0
Phenol-d6 (S)
43 %
22-110
1
05/16/11 08:50
05/18/11 17:31
13127-88-3
2-Fluorophenol (S)
43 %
13-110
1
05/16/11 08:50
05/18/11 17:31
367-12-4
2,4,6-Tribromophenol (S)
58 %
27-110
1
05/16/11 08:50
05/18/11 17:31
118-79-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
18.5 %
0.10
1
05/13/11 14:34
Sample: SS-4 Lab ID: 9293679043 Collected: 05/06/11 14:35 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Chromium
24.4 mg/kg
0.47
1
05/18/11 15:30
05/20/11 03:38
7440-47-3
Copper
12.2 mg/kg
0.47
1
05/18/11 15:30
05/20/11 03:38
7440-50-8
Iron
18100 mg/kg
47.5
10
05/18/11 15:30
05/20/11 12:22
7439-89-6
Lead
22.8 mg/kg
0.47
1
05/18/11 15:30
05/20/11 03:38
7439-92-1
Nickel
5.8 mg/kg
0.47
1
05/18/11 15:30
05/20/11 03:38
7440-02-0
Zinc
72.9 mg/kg
0.95
1
05/18/11 15:30
05/20/11 03:38
7440-66-6
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
83-32-9
Acenaphthylene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
208-96-8
Aniline
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
62-53-3
Anthracene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
120-12-7
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 132 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Sample: SS-4 Lab ID: 9293679043 Collected: 05/06/11 14:35 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No.
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Benzo(a)anthracene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
56-55-3
Benzo(a)pyrene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
50-32-8
Benzo(b)fluoranthene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
191-24-2
Benzo(k)fluoranthene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
207-08-9
Benzoic Acid
ND ug/kg
2300
1
05/16/11 08:50
05/18/11 17:58
65-85-0
Benzyl alcohol
ND ug/kg
918
1
05/16/11 08:50
05/18/11 17:58
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
101-55-3
Butylbenzylphthalate
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
85-68-7
4-Chloro-3-methylphenol
ND ug/kg
918
1
05/16/11 08:50
05/18/11 17:58
59-50-7
4-Chloroaniline
ND ug/kg
2300
1
05/16/11 08:50
05/18/11 17:58
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
108-60-1
2-Chloronaphthalene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
91-58-7
2-Chlorophenol
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
7005-72-3
Chrysene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
53-70-3
Dibenzofuran
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
132-64-9
1,2-Dichlorobenzene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
95-50-1
1,3-Dichlorobenzene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
541-73-1
1,4-Dichlorobenzene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
2300
1
05/16/11 08:50
05/18/11 17:58
91-94-1
2,4-Dichlorophenol
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
120-83-2
Diethylphthalate
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
84-66-2
2,4-Dimethylphenol
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
105-67-9
Dimethylphthalate
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
131-11-3
Di-n-butylphthalate
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
84-74-2
4,6-Dinitro-2-methylphenol
ND ug/kg
918
1
05/16/11 08:50
05/18/11 17:58
534-52-1
2,4-Dinitrophenol
ND ug/kg
2300
1
05/16/11 08:50
05/18/11 17:58
51-28-5
2,4-Dinitrotoluene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
121-14-2
2,6-Dinitrotoluene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
606-20-2
Di-n-octylphthalate
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
117-81-7
Fluoranthene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
206-44-0
Fluorene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
87-68-3
Hexachlorobenzene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
77-47-4
Hexachloroethane
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
193-39-5
Isophorone
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
78-59-1
1-Methylnaphthalene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
90-12-0
2-Methylnaphthalene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
95-48-7
[phone]
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 133 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SS-4 Lab ID: 9293679043 Collected: 05/06/11 14:35 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
3&4-Methylphenol(m&p Cresol)
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
Naphthalene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
91-20-3
2-Nitroaniline
ND ug/kg
2300
1
05/16/11 08:50
05/18/11 17:58
88-74-4
3-Nitroaniline
ND ug/kg
2300
1
05/16/11 08:50
05/18/11 17:58
99-09-2
4-Nitroaniline
ND ug/kg
918
1
05/16/11 08:50
05/18/11 17:58
100-01-6
Nitrobenzene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
98-95-3
2-Nitrophenol
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
88-75-5
4-Nitrophenol
ND ug/kg
2300
1
05/16/11 08:50
05/18/11 17:58
100-02-7
N-Nitrosodimethylamine
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
86-30-6
Pentachlorophenol
ND ug/kg
2300
1
05/16/11 08:50
05/18/11 17:58
87-86-5
Phenanthrene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
85-01-8
Phenol
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
108-95-2
Pyrene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
459
1
05/16/11 08:50
05/18/11 17:58
88-06-2
Nitrobenzene-d5 (S)
73 %
23-110
1
05/16/11 08:50
05/18/11 17:58
4165-60-0
2-Fluorobiphenyl (S)
63 %
30-110
1
05/16/11 08:50
05/18/11 17:58
321-60-8
Terphenyl-d14 (S)
55 %
28-110
1
05/16/11 08:50
05/18/11 17:58
1718-51-0
Phenol-d6 (S)
58 %
22-110
1
05/16/11 08:50
05/18/11 17:58
13127-88-3
2-Fluorophenol (S)
60 %
13-110
1
05/16/11 08:50
05/18/11 17:58
367-12-4
2,4,6-Tribromophenol (S)
58 %
27-110
1
05/16/11 08:50
05/18/11 17:58
118-79-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
28.8 %
0.10
1
05/13/11 14:34
Sample: SS-5 Lab ID: 9293679044 Collected: 05/06/11 15:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Chromium
17.2 mg/kg
0.60
1
05/18/11 15:30
05/20/11 03:50
7440-47-3
Copper
8.1 mg/kg
0.60
1
05/18/11 15:30
05/20/11 03:50
7440-50-8
Iron
10800 mg/kg
6.0
1
05/18/11 15:30
05/20/11 03:50
7439-89-6
Lead
8.9 mg/kg
0.60
1
05/18/11 15:30
05/20/11 03:50
7439-92-1
Nickel
4.8 mg/kg
0.60
1
05/18/11 15:30
05/20/11 03:50
7440-02-0
Zinc
52.0 mg/kg
1.2
1
05/18/11 15:30
05/20/11 03:50
7440-66-6
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 466 1 05/16/11 08:50 05/18/11 18:26 83-32-9
Acenaphthylene ND ug/kg 466 1 05/16/11 08:50 05/18/11 18:26 208-96-8
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 134 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: SS-5 Lab ID: 9293679044 Collected: 05/06/11 15:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Aniline
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
62-53-3
Anthracene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
120-12-7
Benzo(a)anthracene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
56-55-3
Benzo(a)pyrene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
50-32-8
Benzo(b)fluoranthene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
191-24-2
Benzo(k)fluoranthene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
207-08-9
Benzoic Acid
ND ug/kg
2330
1
05/16/11 08:50
05/18/11 18:26
65-85-0
Benzyl alcohol
ND ug/kg
931
1
05/16/11 08:50
05/18/11 18:26
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
101-55-3
Butylbenzylphthalate
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
85-68-7
4-Chloro-3-methylphenol
ND ug/kg
931
1
05/16/11 08:50
05/18/11 18:26
59-50-7
4-Chloroaniline
ND ug/kg
2330
1
05/16/11 08:50
05/18/11 18:26
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
108-60-1
2-Chloronaphthalene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
91-58-7
2-Chlorophenol
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
7005-72-3
Chrysene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
53-70-3
Dibenzofuran
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
132-64-9
1,2-Dichlorobenzene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
95-50-1
1,3-Dichlorobenzene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
541-73-1
1,4-Dichlorobenzene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
2330
1
05/16/11 08:50
05/18/11 18:26
91-94-1
2,4-Dichlorophenol
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
120-83-2
Diethylphthalate
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
84-66-2
2,4-Dimethylphenol
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
105-67-9
Dimethylphthalate
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
131-11-3
Di-n-butylphthalate
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
84-74-2
4,6-Dinitro-2-methylphenol
ND ug/kg
931
1
05/16/11 08:50
05/18/11 18:26
534-52-1
2,4-Dinitrophenol
ND ug/kg
2330
1
05/16/11 08:50
05/18/11 18:26
51-28-5
2,4-Dinitrotoluene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
121-14-2
2,6-Dinitrotoluene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
606-20-2
Di-n-octylphthalate
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
117-81-7
Fluoranthene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
206-44-0
Fluorene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
87-68-3
Hexachlorobenzene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
77-47-4
Hexachloroethane
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
193-39-5
Isophorone
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
78-59-1
1-Methylnaphthalene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
90-12-0
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 135 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: SS-5 Lab ID: 9293679044 Collected: 05/06/11 15:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Methylnaphthalene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
Naphthalene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
91-20-3
2-Nitroaniline
ND ug/kg
2330
1
05/16/11 08:50
05/18/11 18:26
88-74-4
3-Nitroaniline
ND ug/kg
2330
1
05/16/11 08:50
05/18/11 18:26
99-09-2
4-Nitroaniline
ND ug/kg
931
1
05/16/11 08:50
05/18/11 18:26
100-01-6
Nitrobenzene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
98-95-3
2-Nitrophenol
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
88-75-5
4-Nitrophenol
ND ug/kg
2330
1
05/16/11 08:50
05/18/11 18:26
100-02-7
N-Nitrosodimethylamine
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
86-30-6
Pentachlorophenol
ND ug/kg
2330
1
05/16/11 08:50
05/18/11 18:26
87-86-5
Phenanthrene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
85-01-8
Phenol
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
108-95-2
Pyrene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
466
1
05/16/11 08:50
05/18/11 18:26
88-06-2
Nitrobenzene-d5 (S)
60 %
23-110
1
05/16/11 08:50
05/18/11 18:26
4165-60-0
2-Fluorobiphenyl (S)
68 %
30-110
1
05/16/11 08:50
05/18/11 18:26
321-60-8
Terphenyl-d14 (S)
56 %
28-110
1
05/16/11 08:50
05/18/11 18:26
1718-51-0
Phenol-d6 (S)
45 %
22-110
1
05/16/11 08:50
05/18/11 18:26
13127-88-3
2-Fluorophenol (S)
48 %
13-110
1
05/16/11 08:50
05/18/11 18:26
367-12-4
2,4,6-Tribromophenol (S)
49 %
27-110
1
05/16/11 08:50
05/18/11 18:26
118-79-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
29.1 %
0.10
1
05/13/11 14:34
Sample: SS-6 Lab ID: 9293679045 Collected: 05/06/11 14:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Chromium
14.3 mg/kg
0.68
1
05/18/11 15:30
05/20/11 04:01
7440-47-3
Copper
11.5 mg/kg
0.68
1
05/18/11 15:30
05/20/11 04:01
7440-50-8
Iron
25300 mg/kg
68.2
10
05/18/11 15:30
05/20/11 12:29
7439-89-6
Lead
6.0 mg/kg
0.68
1
05/18/11 15:30
05/20/11 04:01
7439-92-1
Nickel
7.3 mg/kg
0.68
1
05/18/11 15:30
05/20/11 04:01
7440-02-0
Zinc
36.8 mg/kg
1.4
1
05/18/11 15:30
05/20/11 04:01
7440-66-6
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 136 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Sample: SS-6 Lab ID: 9293679045 Collected: 05/06/11 14:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No.
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
83-32-9
Acenaphthylene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
208-96-8
Aniline
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
62-53-3
Anthracene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
120-12-7
Benzo(a)anthracene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
56-55-3
Benzo(a)pyrene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
50-32-8
Benzo(b)fluoranthene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
191-24-2
Benzo(k)fluoranthene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
207-08-9
Benzoic Acid
ND ug/kg
2470
1
05/16/11 08:50
05/18/11 18:54
65-85-0
Benzyl alcohol
ND ug/kg
990
1
05/16/11 08:50
05/18/11 18:54
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
101-55-3
Butylbenzylphthalate
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
85-68-7
4-Chloro-3-methylphenol
ND ug/kg
990
1
05/16/11 08:50
05/18/11 18:54
59-50-7
4-Chloroaniline
ND ug/kg
2470
1
05/16/11 08:50
05/18/11 18:54
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
108-60-1
2-Chloronaphthalene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
91-58-7
2-Chlorophenol
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
7005-72-3
Chrysene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
53-70-3
Dibenzofuran
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
132-64-9
1,2-Dichlorobenzene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
95-50-1
1,3-Dichlorobenzene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
541-73-1
1,4-Dichlorobenzene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
2470
1
05/16/11 08:50
05/18/11 18:54
91-94-1
2,4-Dichlorophenol
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
120-83-2
Diethylphthalate
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
84-66-2
2,4-Dimethylphenol
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
105-67-9
Dimethylphthalate
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
131-11-3
Di-n-butylphthalate
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
84-74-2
4,6-Dinitro-2-methylphenol
ND ug/kg
990
1
05/16/11 08:50
05/18/11 18:54
534-52-1
2,4-Dinitrophenol
ND ug/kg
2470
1
05/16/11 08:50
05/18/11 18:54
51-28-5
2,4-Dinitrotoluene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
121-14-2
2,6-Dinitrotoluene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
606-20-2
Di-n-octylphthalate
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
117-81-7
Fluoranthene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
206-44-0
Fluorene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
87-68-3
Hexachlorobenzene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
77-47-4
Hexachloroethane
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
193-39-5
[phone]
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 137 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: SS-6 Lab ID: 9293679045 Collected: 05/06/11 14:00 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Isophorone
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
78-59-1
1-Methylnaphthalene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
90-12-0
2-Methylnaphthalene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
Naphthalene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
91-20-3
2-Nitroaniline
ND ug/kg
2470
1
05/16/11 08:50
05/18/11 18:54
88-74-4
3-Nitroaniline
ND ug/kg
2470
1
05/16/11 08:50
05/18/11 18:54
99-09-2
4-Nitroaniline
ND ug/kg
990
1
05/16/11 08:50
05/18/11 18:54
100-01-6
Nitrobenzene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
98-95-3
2-Nitrophenol
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
88-75-5
4-Nitrophenol
ND ug/kg
2470
1
05/16/11 08:50
05/18/11 18:54
100-02-7
N-Nitrosodimethylamine
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
86-30-6
Pentachlorophenol
ND ug/kg
2470
1
05/16/11 08:50
05/18/11 18:54
87-86-5
Phenanthrene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
85-01-8
Phenol
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
108-95-2
Pyrene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
495
1
05/16/11 08:50
05/18/11 18:54
88-06-2
Nitrobenzene-d5 (S)
54 %
23-110
1
05/16/11 08:50
05/18/11 18:54
4165-60-0
2-Fluorobiphenyl (S)
55 %
30-110
1
05/16/11 08:50
05/18/11 18:54
321-60-8
Terphenyl-d14 (S)
47 %
28-110
1
05/16/11 08:50
05/18/11 18:54
1718-51-0
Phenol-d6 (S)
37 %
22-110
1
05/16/11 08:50
05/18/11 18:54
13127-88-3
2-Fluorophenol (S)
45 %
13-110
1
05/16/11 08:50
05/18/11 18:54
367-12-4
2,4,6-Tribromophenol (S)
50 %
27-110
1
05/16/11 08:50
05/18/11 18:54
118-79-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
33.3 %
0.10
1
05/13/11 14:34
Sample: SS-7 Lab ID: 9293679046 Collected: 05/06/11 15:20 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Chromium
11.3 mg/kg
0.42
1
05/18/11 15:30
05/20/11 04:06
7440-47-3
Copper
8.4 mg/kg
0.42
1
05/18/11 15:30
05/20/11 04:06
7440-50-8
Iron
14500 mg/kg
42.3
10
05/18/11 15:30
05/20/11 12:33
7439-89-6
Lead
6.9 mg/kg
0.42
1
05/18/11 15:30
05/20/11 04:06
7439-92-1
Nickel
5.1 mg/kg
0.42
1
05/18/11 15:30
05/20/11 04:06
7440-02-0
Zinc
46.0 mg/kg
0.85
1
05/18/11 15:30
05/20/11 04:06
7440-66-6
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 138 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: SS-7 Lab ID: 9293679046 Collected: 05/06/11 15:20 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
83-32-9
Acenaphthylene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
208-96-8
Aniline
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
62-53-3
Anthracene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
120-12-7
Benzo(a)anthracene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
56-55-3
Benzo(a)pyrene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
50-32-8
Benzo(b)fluoranthene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
191-24-2
Benzo(k)fluoranthene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
207-08-9
Benzoic Acid
ND ug/kg
2060
1
05/16/11 08:50
05/18/11 19:22
65-85-0
Benzyl alcohol
ND ug/kg
826
1
05/16/11 08:50
05/18/11 19:22
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
101-55-3
Butylbenzylphthalate
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
85-68-7
4-Chloro-3-methylphenol
ND ug/kg
826
1
05/16/11 08:50
05/18/11 19:22
59-50-7
4-Chloroaniline
ND ug/kg
2060
1
05/16/11 08:50
05/18/11 19:22
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
108-60-1
2-Chloronaphthalene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
91-58-7
2-Chlorophenol
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
7005-72-3
Chrysene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
53-70-3
Dibenzofuran
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
132-64-9
1,2-Dichlorobenzene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
95-50-1
1,3-Dichlorobenzene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
541-73-1
1,4-Dichlorobenzene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
2060
1
05/16/11 08:50
05/18/11 19:22
91-94-1
2,4-Dichlorophenol
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
120-83-2
Diethylphthalate
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
84-66-2
2,4-Dimethylphenol
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
105-67-9
Dimethylphthalate
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
131-11-3
Di-n-butylphthalate
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
84-74-2
4,6-Dinitro-2-methylphenol
ND ug/kg
826
1
05/16/11 08:50
05/18/11 19:22
534-52-1
2,4-Dinitrophenol
ND ug/kg
2060
1
05/16/11 08:50
05/18/11 19:22
51-28-5
2,4-Dinitrotoluene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
121-14-2
2,6-Dinitrotoluene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
606-20-2
Di-n-octylphthalate
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
117-81-7
Fluoranthene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
206-44-0
Fluorene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
87-68-3
Hexachlorobenzene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
77-47-4
Hexachloroethane
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
193-39-5
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 139 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SS-7 Lab ID: 9293679046 Collected: 05/06/11 15:20 Received: 05/07/11 10:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Isophorone
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
78-59-1
1-Methylnaphthalene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
90-12-0
2-Methylnaphthalene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
Naphthalene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
91-20-3
2-Nitroaniline
ND ug/kg
2060
1
05/16/11 08:50
05/18/11 19:22
88-74-4
3-Nitroaniline
ND ug/kg
2060
1
05/16/11 08:50
05/18/11 19:22
99-09-2
4-Nitroaniline
ND ug/kg
826
1
05/16/11 08:50
05/18/11 19:22
100-01-6
Nitrobenzene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
98-95-3
2-Nitrophenol
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
88-75-5
4-Nitrophenol
ND ug/kg
2060
1
05/16/11 08:50
05/18/11 19:22
100-02-7
N-Nitrosodimethylamine
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
86-30-6
Pentachlorophenol
ND ug/kg
2060
1
05/16/11 08:50
05/18/11 19:22
87-86-5
Phenanthrene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
85-01-8
Phenol
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
108-95-2
Pyrene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
413
1
05/16/11 08:50
05/18/11 19:22
88-06-2
Nitrobenzene-d5 (S)
75 %
23-110
1
05/16/11 08:50
05/18/11 19:22
4165-60-0
2-Fluorobiphenyl (S)
62 %
30-110
1
05/16/11 08:50
05/18/11 19:22
321-60-8
Terphenyl-d14 (S)
49 %
28-110
1
05/16/11 08:50
05/18/11 19:22
1718-51-0
Phenol-d6 (S)
53 %
22-110
1
05/16/11 08:50
05/18/11 19:22
13127-88-3
2-Fluorophenol (S)
60 %
13-110
1
05/16/11 08:50
05/18/11 19:22
367-12-4
2,4,6-Tribromophenol (S)
51 %
27-110
1
05/16/11 08:50
05/18/11 19:22
118-79-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
20.1 %
0.10
1
05/18/11 13:54
Sample: SW-4 Lab ID: 9293679047 Collected: 05/06/11 14:35 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:47
7440-47-3
Copper
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:47
7440-50-8
Iron
342 ug/L
50.0
1
05/12/11 12:30
05/12/11 22:47
7439-89-6
Lead
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:47
7439-92-1
Nickel
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:47
7440-02-0
Zinc
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:47
7440-66-6
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 140 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW-4 Lab ID: 9293679047 Collected: 05/06/11 14:35 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
83-32-9
Acenaphthylene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
208-96-8
Aniline
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
62-53-3
Anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
120-12-7
Benzo(a)anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
56-55-3
Benzo(a)pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
50-32-8
Benzo(b)fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
205-99-2
Benzo(g,h,i)perylene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
191-24-2
Benzo(k)fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
207-08-9
Benzoic Acid
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 17:39
65-85-0
Benzyl alcohol
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 17:39
100-51-6
4-Bromophenylphenyl ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
101-55-3
Butylbenzylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
85-68-7
4-Chloro-3-methylphenol
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 17:39
59-50-7
4-Chloroaniline
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 17:39
106-47-8
bis(2-Chloroethoxy)methane
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
111-91-1
bis(2-Chloroethyl) ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
108-60-1
2-Chloronaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
91-58-7
2-Chlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
7005-72-3
Chrysene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
218-01-9
Dibenz(a,h)anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
53-70-3
Dibenzofuran
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
132-64-9
1,2-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
95-50-1
1,3-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
541-73-1
1,4-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
106-46-7
3,3'-Dichlorobenzidine
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 17:39
91-94-1
2,4-Dichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
120-83-2
Diethylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
84-66-2
2,4-Dimethylphenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
105-67-9
Dimethylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
131-11-3
Di-n-butylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
84-74-2
4,6-Dinitro-2-methylphenol
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 17:39
534-52-1
2,4-Dinitrophenol
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 17:39
51-28-5
2,4-Dinitrotoluene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
121-14-2
2,6-Dinitrotoluene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
606-20-2
Di-n-octylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/L
6.0
1
05/13/11 10:39
05/18/11 17:39
117-81-7
Fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
206-44-0
Fluorene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
87-68-3
Hexachlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
118-74-1
Hexachlorocyclopentadiene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
77-47-4
Hexachloroethane
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
193-39-5
Isophorone
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
78-59-1
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 141 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW-4 Lab ID: 9293679047 Collected: 05/06/11 14:35 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
1-Methylnaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
90-12-0
2-Methylnaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
91-57-6
2-Methylphenol(o-Cresol)
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
Naphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
91-20-3
2-Nitroaniline
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 17:39
88-74-4
3-Nitroaniline
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 17:39
99-09-2
4-Nitroaniline
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 17:39
100-01-6
Nitrobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
98-95-3
2-Nitrophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
88-75-5
4-Nitrophenol
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 17:39
100-02-7
N-Nitrosodimethylamine
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
621-64-7
N-Nitrosodiphenylamine
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
86-30-6
Pentachlorophenol
ND ug/L
25.0
1
05/13/11 10:39
05/18/11 17:39
87-86-5
Phenanthrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
85-01-8
Phenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
108-95-2
Pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
129-00-0
1,2,4-Trichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
120-82-1
2,4,5-Trichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
95-95-4
2,4,6-Trichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 17:39
88-06-2
Nitrobenzene-d5 (S)
62 %
21-110
1
05/13/11 10:39
05/18/11 17:39
4165-60-0
2-Fluorobiphenyl (S)
69 %
27-110
1
05/13/11 10:39
05/18/11 17:39
321-60-8
Terphenyl-d14 (S)
82 %
31-107
1
05/13/11 10:39
05/18/11 17:39
1718-51-0
Phenol-d6 (S)
23 %
10-110
1
05/13/11 10:39
05/18/11 17:39
13127-88-3
2-Fluorophenol (S)
41 %
12-110
1
05/13/11 10:39
05/18/11 17:39
367-12-4
2,4,6-Tribromophenol (S)
68 %
27-110
1
05/13/11 10:39
05/18/11 17:39
118-79-6
8260 MSV Low Level
Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/11/11 18:58
67-64-1
Benzene
ND ug/L
1.0
1
05/11/11 18:58
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/11/11 18:58
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/11/11 18:58
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
05/11/11 18:58
75-27-4
Bromoform
ND ug/L
1.0
1
05/11/11 18:58
75-25-2
Bromomethane
ND ug/L
2.0
1
05/11/11 18:58
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/11/11 18:58
78-93-3
Carbon tetrachloride
ND ug/L
1.0
1
05/11/11 18:58
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/11/11 18:58
108-90-7
Chloroethane
ND ug/L
1.0
1
05/11/11 18:58
75-00-3
Chloroform
ND ug/L
1.0
1
05/11/11 18:58
67-66-3
Chloromethane
ND ug/L
1.0
1
05/11/11 18:58
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/11/11 18:58
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/11/11 18:58
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
1
05/11/11 18:58
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/11/11 18:58
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/11/11 18:58
106-93-4
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 142 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: SW-4 Lab ID: 9293679047 Collected: 05/06/11 14:35 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Dibromomethane
ND ug/L
1.0
1
05/11/11 18:58
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 18:58
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 18:58
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 18:58
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/11/11 18:58
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
1
05/11/11 18:58
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/11/11 18:58
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
05/11/11 18:58
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 18:58
156-59-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 18:58
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 18:58
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/11/11 18:58
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 18:58
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/11/11 18:58
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 18:58
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 18:58
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/11/11 18:58
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/11/11 18:58
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/11/11 18:58
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/11/11 18:58
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
1
05/11/11 18:58
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/11/11 18:58
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/11/11 18:58
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/11/11 18:58
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/11/11 18:58
91-20-3
Styrene
ND ug/L
1.0
1
05/11/11 18:58
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 18:58
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 18:58
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
05/11/11 18:58
127-18-4
Toluene
ND ug/L
1.0
1
05/11/11 18:58
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 18:58
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 18:58
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/11/11 18:58
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/11/11 18:58
79-00-5
Trichloroethene
ND ug/L
1.0
1
05/11/11 18:58
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/11/11 18:58
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/11/11 18:58
96-18-4
Vinyl acetate
ND ug/L
2.0
1
05/11/11 18:58
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/11/11 18:58
75-01-4
m&p-Xylene
ND ug/L
2.0
1
05/11/11 18:58
179601-23-1
o-Xylene
ND ug/L
1.0
1
05/11/11 18:58
95-47-6
4-Bromofluorobenzene (S)
97 %
70-130
1
05/11/11 18:58
460-00-4
Dibromofluoromethane (S)
105 %
70-130
1
05/11/11 18:58
1868-53-7
1,2-Dichloroethane-d4 (S)
111 %
70-130
1
05/11/11 18:58
17060-07-0
Toluene-d8 (S)
100 %
70-130
1
05/11/11 18:58
2037-26-5
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 143 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW-5 Lab ID: 9293679048 Collected: 05/06/11 15:00 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:50
7440-47-3
Copper
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:50
7440-50-8
Iron
251 ug/L
50.0
1
05/12/11 12:30
05/12/11 22:50
7439-89-6
Lead
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:50
7439-92-1
Nickel
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:50
7440-02-0
Zinc
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:50
7440-66-6
8270 MSSV Semivolatile Organic
Analytical Method: EPA 8270 Preparation Method:
EPA 3510
Acenaphthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
83-32-9
Acenaphthylene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
208-96-8
Aniline
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
62-53-3
Anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
120-12-7
Benzo(a)anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
56-55-3
Benzo(a)pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
50-32-8
Benzo(b)fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
205-99-2
Benzo(g,h,i)perylene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
191-24-2
Benzo(k)fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
207-08-9
Benzoic Acid
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 18:07
65-85-0
Benzyl alcohol
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 18:07
100-51-6
4-Bromophenylphenyl ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
101-55-3
Butylbenzylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
85-68-7
4-Chloro-3-methylphenol
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 18:07
59-50-7
4-Chloroaniline
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 18:07
106-47-8
bis(2-Chloroethoxy)methane
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
111-91-1
bis(2-Chloroethyl) ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
108-60-1
2-Chloronaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
91-58-7
2-Chlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
7005-72-3
Chrysene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
218-01-9
Dibenz(a,h)anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
53-70-3
Dibenzofuran
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
132-64-9
1,2-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
95-50-1
1,3-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
541-73-1
1,4-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
106-46-7
3,3'-Dichlorobenzidine
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 18:07
91-94-1
2,4-Dichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
120-83-2
Diethylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
84-66-2
2,4-Dimethylphenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
105-67-9
Dimethylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
131-11-3
Di-n-butylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
84-74-2
4,6-Dinitro-2-methylphenol
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 18:07
534-52-1
2,4-Dinitrophenol
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 18:07
51-28-5
2,4-Dinitrotoluene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
121-14-2
2,6-Dinitrotoluene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
606-20-2
Di-n-octylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
117-84-0
bis(2- Ethyl hexyl)phthalate
20.1 ug/L
6.0
1
05/13/11 10:39
05/18/11 18:07
117-81-7
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 144 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW-5 Lab ID: 9293679048 Collected: 05/06/11 15:00 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
206-44-0
Fluorene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
87-68-3
Hexachlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
118-74-1
Hexachlorocyclopentadiene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
77-47-4
Hexachloroethane
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
193-39-5
Isophorone
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
78-59-1
1-Methylnaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
90-12-0
2-Methylnaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
91-57-6
2-Methylphenol(o-Cresol)
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
Naphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
91-20-3
2-Nitroaniline
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 18:07
88-74-4
3-Nitroaniline
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 18:07
99-09-2
4-Nitroaniline
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 18:07
100-01-6
Nitrobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
98-95-3
2-Nitrophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
88-75-5
4-Nitrophenol
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 18:07
100-02-7
N-Nitrosodimethylamine
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
621-64-7
N-Nitrosodiphenylamine
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
86-30-6
Pentachlorophenol
ND ug/L
25.0
1
05/13/11 10:39
05/18/11 18:07
87-86-5
Phenanthrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
85-01-8
Phenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
108-95-2
Pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
129-00-0
1,2,4-Trichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
120-82-1
2,4,5-Trichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
95-95-4
2,4,6-Trichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:07
88-06-2
Nitrobenzene-d5 (S)
63 %
21-110
1
05/13/11 10:39
05/18/11 18:07
4165-60-0
2-Fluorobiphenyl (S)
72 %
27-110
1
05/13/11 10:39
05/18/11 18:07
321-60-8
Terphenyl-d14 (S)
106 %
31-107
1
05/13/11 10:39
05/18/11 18:07
1718-51-0
Phenol-d6 (S)
22 %
10-110
1
05/13/11 10:39
05/18/11 18:07
13127-88-3
2-Fluorophenol (S)
40 %
12-110
1
05/13/11 10:39
05/18/11 18:07
367-12-4
2,4,6-Tribromophenol (S)
75 %
27-110
1
05/13/11 10:39
05/18/11 18:07
118-79-6
8260 MSV Low Level
Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/11/11 19:24
67-64-1
Benzene
ND ug/L
1.0
1
05/11/11 19:24
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/11/11 19:24
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/11/11 19:24
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
05/11/11 19:24
75-27-4
Bromoform
ND ug/L
1.0
1
05/11/11 19:24
75-25-2
Bromomethane
ND ug/L
2.0
1
05/11/11 19:24
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/11/11 19:24
78-93-3
Carbon tetrachloride
ND ug/L
1.0
1
05/11/11 19:24
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/11/11 19:24
108-90-7
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 145 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: SW-5 Lab ID: 9293679048 Collected: 05/06/11 15:00 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Chloroethane
ND ug/L
1.0
1
05/11/11 19:24
75-00-3
Chloroform
ND ug/L
1.0
1
05/11/11 19:24
67-66-3
Chloromethane
ND ug/L
1.0
1
05/11/11 19:24
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/11/11 19:24
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/11/11 19:24
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
1
05/11/11 19:24
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/11/11 19:24
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/11/11 19:24
106-93-4
Dibromomethane
ND ug/L
1.0
1
05/11/11 19:24
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 19:24
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 19:24
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 19:24
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/11/11 19:24
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
1
05/11/11 19:24
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/11/11 19:24
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
05/11/11 19:24
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 19:24
156-59-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 19:24
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 19:24
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/11/11 19:24
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 19:24
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/11/11 19:24
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 19:24
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 19:24
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/11/11 19:24
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/11/11 19:24
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/11/11 19:24
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/11/11 19:24
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
1
05/11/11 19:24
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/11/11 19:24
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/11/11 19:24
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/11/11 19:24
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/11/11 19:24
91-20-3
Styrene
ND ug/L
1.0
1
05/11/11 19:24
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 19:24
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 19:24
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
05/11/11 19:24
127-18-4
Toluene
ND ug/L
1.0
1
05/11/11 19:24
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 19:24
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 19:24
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/11/11 19:24
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/11/11 19:24
79-00-5
Trichloroethene
ND ug/L
1.0
1
05/11/11 19:24
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/11/11 19:24
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/11/11 19:24
96-18-4
Vinyl acetate
ND ug/L
2.0
1
05/11/11 19:24
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/11/11 19:24
75-01-4
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 146 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: SW-5 Lab ID: 9293679048 Collected: 05/06/11 15:00 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
m&p-Xylene
ND ug/L
2.0
1
05/11/11 19:24
179601-23-1
o-Xylene
ND ug/L
1.0
1
05/11/11 19:24
95-47-6
4-Bromofluorobenzene (S)
97 %
70-130
1
05/11/11 19:24
460-00-4
Dibromofluoromethane (S)
105 %
70-130
1
05/11/11 19:24
1868-53-7
1,2-Dichloroethane-d4 (S)
111 %
70-130
1
05/11/11 19:24
17060-07-0
Toluene-d8 (S)
98 %
70-130
1
05/11/11 19:24
2037-26-5
Sample: SW-6 Lab ID: 9293679049 Collected: 05/06/11 14:00 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:53
7440-47-3
Copper
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:53
7440-50-8
Iron
257 ug/L
50.0
1
05/12/11 12:30
05/12/11 22:53
7439-89-6
Lead
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:53
7439-92-1
Nickel
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:53
7440-02-0
Zinc
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:53
7440-66-6
8270 MSSV Semivolatile Organic
Analytical Method: EPA 8270 Preparation Method:
EPA 3510
Acenaphthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
83-32-9
Acenaphthylene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
208-96-8
Aniline
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
62-53-3
Anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
120-12-7
Benzo(a)anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
56-55-3
Benzo(a)pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
50-32-8
Benzo(b)fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
205-99-2
Benzo(g,h,i)perylene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
191-24-2
Benzo(k)fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
207-08-9
Benzoic Acid
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 18:34
65-85-0
Benzyl alcohol
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 18:34
100-51-6
4-Bromophenylphenyl ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
101-55-3
Butylbenzylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
85-68-7
4-Chloro-3-methylphenol
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 18:34
59-50-7
4-Chloroaniline
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 18:34
106-47-8
bis(2-Chloroethoxy)methane
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
111-91-1
bis(2-Chloroethyl) ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
108-60-1
2-Chloronaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
91-58-7
2-Chlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
7005-72-3
Chrysene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
218-01-9
Dibenz(a,h)anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
53-70-3
Dibenzofuran
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
132-64-9
1,2-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
95-50-1
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 147 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW-6 Lab ID: 9293679049 Collected: 05/06/11 14:00 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
1,3-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
541-73-1
1,4-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
106-46-7
3,3'-Dichlorobenzidine
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 18:34
91-94-1
2,4-Dichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
120-83-2
Diethylphtha late
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
84-66-2
2,4-Dimethylphenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
105-67-9
Dimethylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
131-11-3
Di-n-butylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 18:34
534-52-1
2,4-Dinitrophenol
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 18:34
51-28-5
2,4-Dinitrotoluene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
121-14-2
2,6-Dinitrotoluene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
606-20-2
Di-n-octylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/L
6.0
1
05/13/11 10:39
05/18/11 18:34
117-81-7
Fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
206-44-0
Fluorene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
87-68-3
Hexachlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
118-74-1
Hexachlorocyclopentadiene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
77-47-4
Hexachloroethane
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
193-39-5
Isophorone
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
78-59-1
1-Methylnaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
90-12-0
2-Methylnaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
91-57-6
2-Methylphenol(o-Cresol)
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
Naphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
91-20-3
2-Nitroaniline
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 18:34
88-74-4
3-Nitroaniline
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 18:34
99-09-2
4-Nitroaniline
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 18:34
100-01-6
Nitrobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
98-95-3
2-Nitrophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
88-75-5
4-Nitrophenol
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 18:34
100-02-7
N-Nitrosodimethylamine
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
621-64-7
N-Nitrosodiphenylamine
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
86-30-6
Pentachlorophenol
ND ug/L
25.0
1
05/13/11 10:39
05/18/11 18:34
87-86-5
Phenanthrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
85-01-8
Phenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
108-95-2
Pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
129-00-0
1,2,4-Trichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
120-82-1
2,4,5-Trichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
95-95-4
2,4,6-Trichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 18:34
88-06-2
Nitrobenzene-d5 (S)
51 %
21-110
1
05/13/11 10:39
05/18/11 18:34
4165-60-0
2-Fluorobiphenyl (S)
59 %
27-110
1
05/13/11 10:39
05/18/11 18:34
321-60-8
Terphenyl-d14 (S)
96 %
31-107
1
05/13/11 10:39
05/18/11 18:34
1718-51-0
Phenol-d6 (S)
17 %
10-110
1
05/13/11 10:39
05/18/11 18:34
13127-88-3
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 148 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: SW-6 Lab ID: 9293679049 Collected: 05/06/11 14:00 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
2-Fluorophenol (S)
30 %
12-110
1 05/13/11 10:39
05/18/11 18:34
367-12-4
2,4,6-Tribromophenol (S)
71 %
27-110
1 05/13/11 10:39
05/18/11 18:34
118-79-6
8260 MSV Low Level
Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/11/11 19:49
67-64-1
Benzene
ND ug/L
1.0
1
05/11/11 19:49
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/11/11 19:49
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/11/11 19:49
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
05/11/11 19:49
75-27-4
Bromoform
ND ug/L
1.0
1
05/11/11 19:49
75-25-2
Bromomethane
ND ug/L
2.0
1
05/11/11 19:49
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/11/11 19:49
78-93-3
Carbon tetrachloride
ND ug/L
1.0
1
05/11/11 19:49
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/11/11 19:49
108-90-7
Chloroethane
ND ug/L
1.0
1
05/11/11 19:49
75-00-3
Chloroform
ND ug/L
1.0
1
05/11/11 19:49
67-66-3
Chloromethane
ND ug/L
1.0
1
05/11/11 19:49
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/11/11 19:49
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/11/11 19:49
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
1
05/11/11 19:49
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/11/11 19:49
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/11/11 19:49
106-93-4
Dibromomethane
ND ug/L
1.0
1
05/11/11 19:49
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 19:49
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 19:49
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 19:49
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/11/11 19:49
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
1
05/11/11 19:49
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/11/11 19:49
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
05/11/11 19:49
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 19:49
156-59-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 19:49
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 19:49
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/11/11 19:49
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 19:49
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/11/11 19:49
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 19:49
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 19:49
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/11/11 19:49
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/11/11 19:49
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/11/11 19:49
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/11/11 19:49
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
1
05/11/11 19:49
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/11/11 19:49
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/11/11 19:49
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/11/11 19:49
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/11/11 19:49
91-20-3
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY
ANALYSIS
Page 149 of 227
This report shall not be reproduced, except
in full,
without the written consent of Pace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
Sample: SW-6 Lab ID: 9293679049 Collected: 05/06/11 14:00 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Styrene
ND ug/L
1.0
1
05/11/11 19:49
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 19:49
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 19:49
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
05/11/11 19:49
127-18-4
Toluene
ND ug/L
1.0
1
05/11/11 19:49
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 19:49
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 19:49
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/11/11 19:49
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/11/11 19:49
79-00-5
Trichloroethene
ND ug/L
1.0
1
05/11/11 19:49
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/11/11 19:49
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/11/11 19:49
96-18-4
Vinyl acetate
ND ug/L
2.0
1
05/11/11 19:49
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/11/11 19:49
75-01-4
m&p-Xylene
ND ug/L
2.0
1
05/11/11 19:49
179601-23-1
o-Xylene
ND ug/L
1.0
1
05/11/11 19:49
95-47-6
4-Bromofluorobenzene (S)
98 %
70-130
1
05/11/11 19:49
460-00-4
Dibromofluoromethane (S)
103 %
70-130
1
05/11/11 19:49
1868-53-7
1,2-Dichloroethane-d4 (S)
112 %
70-130
1
05/11/11 19:49
17060-07-0
Toluene-d8 (S)
98 %
70-130
1
05/11/11 19:49
2037-26-5
Sample: SW-7 Lab ID: 9293679050 Collected: 05/06/11 15:20 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:56
7440-47-3
Copper
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:56
7440-50-8
Iron
253 ug/L
50.0
1
05/12/11 12:30
05/12/11 22:56
7439-89-6
Lead
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:56
7439-92-1
Nickel
ND ug/L
5.0
1
05/12/11 12:30
05/12/11 22:56
7440-02-0
Zinc
ND ug/L
10.0
1
05/12/11 12:30
05/12/11 22:56
7440-66-6
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
83-32-9
Acenaphthylene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
208-96-8
Aniline
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
62-53-3
Anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
120-12-7
Benzo(a)anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
56-55-3
Benzo(a)pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
50-32-8
Benzo(b)fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
205-99-2
Benzo(g,h,i)perylene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
191-24-2
Benzo(k)fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
207-08-9
Benzoic Acid
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 19:01
65-85-0
Benzyl alcohol
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 19:01
100-51-6
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 150 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW-7 Lab ID: 9293679050 Collected: 05/06/11 15:20 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
4-Bromophenylphenyl ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
101-55-3
Butyl benzylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
85-68-7
4-Chloro-3-methylphenol
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 19:01
59-50-7
4-Chloroaniline
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 19:01
106-47-8
bis(2-Chloroethoxy)methane
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
111-91-1
bis(2-Chloroethyl) ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
108-60-1
2-Chloronaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
91-58-7
2-Chlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
7005-72-3
Chrysene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
218-01-9
Dibenz(a,h)anthracene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
53-70-3
Dibenzofuran
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
132-64-9
1,2-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
95-50-1
1,3-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
541-73-1
1,4-Dichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
106-46-7
3,3'-Dichlorobenzidine
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 19:01
91-94-1
2,4-Dichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
120-83-2
Diethylphtha late
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
84-66-2
2,4-Dimethylphenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
105-67-9
Dimethylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
131-11-3
Di-n-butylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
84-74-2
4,6-Dinitro-2-methylphenol
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 19:01
534-52-1
2,4-Dinitrophenol
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 19:01
51-28-5
2,4-Dinitrotoluene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
121-14-2
2,6-Dinitrotoluene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
606-20-2
Di-n-octylphthalate
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
117-84-0
bis(2- Ethyl hexyl)phthalate
ND ug/L
6.0
1
05/13/11 10:39
05/18/11 19:01
117-81-7
Fluoranthene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
206-44-0
Fluorene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
87-68-3
Hexachlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
118-74-1
Hexachlorocyclopentadiene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
77-47-4
Hexachloroethane
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
193-39-5
Isophorone
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
78-59-1
1-Methylnaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
90-12-0
2-Methylnaphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
91-57-6
2-Methylphenol(o-Cresol)
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
Naphthalene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
91-20-3
2-Nitroaniline
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 19:01
88-74-4
3-Nitroaniline
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 19:01
99-09-2
4-Nitroaniline
ND ug/L
20.0
1
05/13/11 10:39
05/18/11 19:01
100-01-6
Nitrobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
98-95-3
2-Nitrophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
88-75-5
4-Nitrophenol
ND ug/L
50.0
1
05/13/11 10:39
05/18/11 19:01
100-02-7
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 151 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW-7 Lab ID: 9293679050 Collected: 05/06/11 15:20 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
N-Nitrosodimethylamine
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
621-64-7
N-Nitrosodiphenylamine
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
86-30-6
Pentachlorophenol
ND ug/L
25.0
1
05/13/11 10:39
05/18/11 19:01
87-86-5
Phenanthrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
85-01-8
Phenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
108-95-2
Pyrene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
129-00-0
1,2,4-Trichlorobenzene
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
120-82-1
2,4,5-Trichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
95-95-4
2,4,6-Trichlorophenol
ND ug/L
10.0
1
05/13/11 10:39
05/18/11 19:01
88-06-2
Nitrobenzene-d5 (S)
49 %
21-110
1
05/13/11 10:39
05/18/11 19:01
4165-60-0
2-Fluorobiphenyl (S)
55 %
27-110
1
05/13/11 10:39
05/18/11 19:01
321-60-8
Terphenyl-d14 (S)
83 %
31-107
1
05/13/11 10:39
05/18/11 19:01
1718-51-0
Phenol-d6 (S)
17 %
10-110
1
05/13/11 10:39
05/18/11 19:01
13127-88-3
2-Fluorophenol (S)
31 %
12-110
1
05/13/11 10:39
05/18/11 19:01
367-12-4
2,4,6-Tribromophenol (S)
60 %
27-110
1
05/13/11 10:39
05/18/11 19:01
118-79-6
8260 MSV Low Level
Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/11/11 20:14
67-64-1
Benzene
ND ug/L
1.0
1
05/11/11 20:14
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/11/11 20:14
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/11/11 20:14
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
05/11/11 20:14
75-27-4
Bromoform
ND ug/L
1.0
1
05/11/11 20:14
75-25-2
Bromomethane
ND ug/L
2.0
1
05/11/11 20:14
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/11/11 20:14
78-93-3
Carbon tetrachloride
ND ug/L
1.0
1
05/11/11 20:14
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/11/11 20:14
108-90-7
Chloroethane
ND ug/L
1.0
1
05/11/11 20:14
75-00-3
Chloroform
ND ug/L
1.0
1
05/11/11 20:14
67-66-3
Chloromethane
ND ug/L
1.0
1
05/11/11 20:14
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/11/11 20:14
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/11/11 20:14
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
1
05/11/11 20:14
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/11/11 20:14
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/11/11 20:14
106-93-4
Dibromomethane
ND ug/L
1.0
1
05/11/11 20:14
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 20:14
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 20:14
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/11/11 20:14
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/11/11 20:14
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
1
05/11/11 20:14
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/11/11 20:14
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
05/11/11 20:14
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 20:14
156-59-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
05/11/11 20:14
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 20:14
78-87-5
Qual
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 152 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW-7 Lab ID: 9293679050 Collected: 05/06/11 15:20 Received: 05/07/11 10:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
1,3-Dichloropropane
ND ug/L
1.0
1
05/11/11 20:14
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/11/11 20:14
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/11/11 20:14
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 20:14
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/11/11 20:14
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/11/11 20:14
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/11/11 20:14
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/11/11 20:14
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/11/11 20:14
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
1
05/11/11 20:14
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/11/11 20:14
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/11/11 20:14
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/11/11 20:14
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/11/11 20:14
91-20-3
Styrene
ND ug/L
1.0
1
05/11/11 20:14
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 20:14
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/11/11 20:14
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
05/11/11 20:14
127-18-4
Toluene
ND ug/L
1.0
1
05/11/11 20:14
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 20:14
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/11/11 20:14
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/11/11 20:14
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/11/11 20:14
79-00-5
Trichloroethene
ND ug/L
1.0
1
05/11/11 20:14
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/11/11 20:14
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/11/11 20:14
96-18-4
Vinyl acetate
ND ug/L
2.0
1
05/11/11 20:14
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/11/11 20:14
75-01-4
m&p-Xylene
ND ug/L
2.0
1
05/11/11 20:14
179601-23-1
o-Xylene
ND ug/L
1.0
1
05/11/11 20:14
95-47-6
4-Bromofluorobenzene (S)
98 %
70-130
1
05/11/11 20:14
460-00-4
Dibromofluoromethane (S)
106 %
70-130
1
05/11/11 20:14
1868-53-7
1,2-Dichloroethane-d4 (S)
111 %
70-130
1
05/11/11 20:14
17060-07-0
Toluene-d8 (S)
98 %
70-130
1
05/11/11 20:14
2037-26-5
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 153 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: OEXT/13562 Analysis Method: EPA 8082
QC Batch Method: EPA 3546 Analysis Description: 8082 GCS PCB
Associated Lab Samples: 9293679031, 9293679032
METHOD BLANK: 605212
Matrix:
Solid
Associated Lab Samples:
9293679031, 9293679032
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
PCB-1016 (Aroclor 1016)
ug/kg
ND
32.8
05/13/11 17:15
PCB-1221 (Aroclor 1221)
ug/kg
ND
32.8
05/13/11 17:15
PCB-1232 (Aroclor 1232)
ug/kg
ND
32.8
05/13/11 17:15
PCB-1242 (Aroclor 1242)
ug/kg
ND
32.8
05/13/11 17:15
PCB-1248 (Aroclor 1248)
ug/kg
ND
32.8
05/13/11 17:15
PCB-1254 (Aroclor 1254)
ug/kg
ND
32.8
05/13/11 17:15
PCB-1260 (Aroclor 1260)
ug/kg
ND
32.8
05/13/11 17:15
Decachlorobiphenyl (S)
%
76
21-132
05/13/11 17:15
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
605213
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
PCB-1016 (Aroclor 1016)
ug/kg
167
105 63 49-110
PCB-1260 (Aroclor 1260)
ug/kg
167
102 61 50-110
Decachlorobiphenyl (S)
%
73 21-132
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 605214
605215
MS
MSD
9293873002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
PCB-1016 (Aroclor 1016)
ug/kg ND
184
184
102
94.1
56
51
49-150 8
PCB-1260 (Aroclor 1260)
ug/kg ND
184
184
103
96.2
56
52
50-150 7
Decachlorobiphenyl (S)
%
59
58
21-132
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 154 of 227

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
QC Batch: GCSV/9741
Analysis Method: 9071 B
QC Batch Method: 9071E
Analysis Description: 9071 Oil and Grease
Associated Lab Samples: 9293679023, 9293679035, 9293679040, 9293679041, 9293679042
METHOD BLANK: 604284
Matrix: Solid
Associated Lab Samples: 9293679023, 9293679035, 9293679040, 9293679041, 9293679042
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Oil and Grease mg/kg
ND 70.0 05/11/11 11:21
LABORATORY CONTROL SAMPLE: 604285
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Oil and Grease mg/kg
1330 1250 94 78-114
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 604286
604287
MS MSD
9293679035
Spike Spike MS MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Oil and Grease mg/kg ND
1660 1660 1470 1440 88 86 78-114 2
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 155 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: OEXT/13560 Analysis Method: MADEP EPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Soil
Associated Lab Samples: 9293679039
METHOD BLANK: 605121
Matrix:
Solid
Associated Lab Samples:
9293679039
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Aliphatic (C09-C18)
mg/kg
ND
10.0
05/14/11 08:10 N2
Aliphatic (C19-C36)
mg/kg
ND
10.0
05/14/11 08:10 N2
Aromatic (C11-C22)
mg/kg
ND
10.0
05/14/11 21:54 N2
2-Bromonaphthalene (S)
%
94
40-140
05/14/11 21:54
2-Fluorobiphenyl (S)
%
85
40-140
05/14/11 21:54
Nonatriacontane (S)
%
53
40-140
05/14/11 08:10
o-Terphenyl (S)
%
65
40-140
05/14/11 21:54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE & LCSD: 605122
605123
Spike
LCS LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C09-C18)
mg/kg
10
ND ND
53
56
40-140 50 N2
Aliphatic (C19-C36)
mg/kg
13.3
ND ND
66
62
40-140 50 N2
Aromatic (C11-C22)
mg/kg
28.3
24.0 22.1
85
78
40-140 8 50 N2
2-Bromonaphthalene (S)
%
119
89
40-140
2-Fluorobiphenyl (S)
%
110
89
40-140
Nonatriacontane (S)
%
61
60
40-140
o-Terphenyl(S)
%
86
73
40-140
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 156 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: GCV/5000 Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH Analysis Description: VPH NC Soil
Associated Lab Samples: 9293679037, 9293679039
METHOD BLANK: 607390
Associated Lab Samples:
9293679037, 9293679039
Parameter
Units
Aliphatic (C05-CO8)
mg/kg
Aliphatic (C09-C12)
mg/kg
Aromatic (C09-C10)
mg/kg
2,5-Dibromotoluene (FID)(S)
%
2,5-Dibromotoluene (PID)(S)
%
Matrix: Solid
Blank
Reporting
Result
Limit
Analyzed Qualifiers
ND
1.5
05/17/1117:55 N2
ND
1.5
05/17/1117:55 N2
ND
1.5
05/17/1117:55 N2
111
70-130
05/17/1117:55
115
70-130
05/17/1117:55
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE & LCSD: 607391
607392
Spike LCS LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc. Result Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-008)
mg/kg
15 14.4 13.9
96
92
70-130 4 25 N2
Aliphatic (C09-C12)
mg/kg
15 19.3 15.1
129
101
30-130 24 25 N2
Aromatic (C09-C10)
mg/kg
5 5.0 5.0
101
99
70-130 1 25 N2
2,5-Dibromotoluene (FID)(S)
%
107
98
70-130
2,5-Dibromotoluene (PID)(S)
%
108
99
70-130
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 157 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: GCV/4996 Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH Analysis Description: VPH NC Water
Associated Lab Samples: 9293679005, 9293679038
METHOD BLANK: 607095
Associated Lab Samples:
9293679005, 9293679038
Parameter
Units
Aliphatic (C05-CO8)
ug/L
Aliphatic (C09-C12)
ug/L
Aromatic (C09-C10)
ug/L
2,5-Dibromotoluene (FID)(S)
%
2,5-Dibromotoluene (PID)(S)
%
Matrix: Water
Blank
Reporting
Result
Limit
Analyzed Qualifiers
ND
30.0
05/16/1121:29 N2
ND
30.0
05/16/1121:29 N2
ND
30.0
05/16/1121:29 N2
107
70-130
05/16/1121:29
110
70-130
05/16/1121:29
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE & LCSD: 607096
607097
Spike
LCS
LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-008)
ug/L
300
285
272
95
91
70-130 5 25 N2
Aliphatic (C09-C12)
ug/L
300
360
385
120
128
30-130 7 25 N2
Aromatic (C09-C10)
ug/L
100
97.3
97.5
97
98
70-130 0 25 N2
2,5-Dibromotoluene (FID)(S)
%
93
90
70-130
2,5-Dibromotoluene (PID)(S)
%
93
90
70-130
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 158 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/8346 Analysis Method: EPA6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET
Associated Lab Samples: 9293679017, 9293679018, 9293679019, 9293679020
METHOD BLANK: 604566
Associated Lab Samples:
Parameter
Matrix: Solid
9293679017, 9293679018, 9293679019, 9293679020
Blank Reporting
Units Result Limit
Analyzed
Aluminum
mg/kg
ND
10.0
05/12/1113:54
Antimony
mg/kg
ND
0.50
05/12/1113:54
Arsenic
mg/kg
ND
0.50
05/12/1113:54
Barium
mg/kg
ND
0.50
05/12/1113:54
Beryllium
mg/kg
ND
0.10
05/12/1113:54
Cadmium
mg/kg
ND
0.10
05/12/1113:54
Calcium
mg/kg
ND
10.0
05/12/1113:54
Chromium
mg/kg
ND
0.50
05/12/1113:54
Cobalt
mg/kg
ND
0.50
05/12/1113:54
Copper
mg/kg
ND
0.50
05/12/1113:54
Iron
mg/kg
ND
5.0
05/12/1113:54
Lead
mg/kg
ND
0.50
05/12/1113:54
Magnesium
mg/kg
ND
10.0
05/12/1113:54
Manganese
mg/kg
ND
0.50
05/12/1113:54
Nickel
mg/kg
ND
0.50
05/12/1113:54
Potassium
mg/kg
ND
500
05/12/1113:54
Selenium
mg/kg
ND
1.0
05/12/1113:54
Silver
mg/kg
ND
0.50
05/12/1113:54
Sodium
mg/kg
ND
500
05/12/1113:54
Thallium
mg/kg
ND
1.0
05/12/1113:54
Vanadium
mg/kg
ND
0.50
05/12/1113:54
Zinc
mg/kg
ND
1.0
05/12/1113:54
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
604567
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Aluminum
mg/kg
500
498
100
80-120
Antimony
mg/kg
50
47.6
95
80-120
Arsenic
mg/kg
50
50.5
101
80-120
Barium
mg/kg
50
51.2
102
80-120
Beryllium
mg/kg
50
51.1
102
80-120
Cadmium
mg/kg
50
51.3
103
80-120
Calcium
mg/kg
500
518
104
80-120
Chromium
mg/kg
50
51.2
102
80-120
Cobalt
mg/kg
50
51.2
102
80-120
Copper
mg/kg
50
50.8
102
80-120
Iron
mg/kg
500
521
104
80-120
Lead
mg/kg
50
51.3
103
80-120
Magnesium
mg/kg
500
524
105
80-120
Manganese
mg/kg
50
51.1
102
80-120
Nickel
mg/kg
50
52.4
105
80-120
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 159 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
604567
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Potassium
mg/kg
500
475J
95
80-120
Selenium
mg/kg
50
50.1
100
80-120
Silver
mg/kg
25
24.5
98
80-120
Sodium
mg/kg
500
485J
97
80-120
Thallium
mg/kg
50
50.1
100
80-120
Vanadium
mg/kg
50
51.4
103
80-120
Zinc
mg/kg
50
50.7
101
80-120
MATRIX SPIKE SAMPLE:
Parameter
604599
Units
9293311009
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Aluminum
mg/kg
11300
428
18700
1727
75-125 MO
Antimony
mg/kg
2.9
42.8
32.8
70
75-125 MO
Arsenic
mg/kg
3.7
42.8
46.5
100
75-125
Barium
mg/kg
89.5
42.8
142
122
75-125
Beryllium
mg/kg
0.20
42.8
42.3
99
75-125
Cadmium
mg/kg
6.9
42.8
45.1
89
75-125
Calcium
mg/kg
1830
428
2000
40
75-125 MO
Chromium
mg/kg
16.5
42.8
60.2
102
75-125
Cobalt
mg/kg
3.4
42.8
40.2
86
75-125
Copper
mg/kg
55.8
42.8
126
165
75-125 MO
Iron
mg/kg
13400
428
13000
-104
75-125 MO
Lead
mg/kg
262
42.8
249
-31
75-125 MO
Magnesium
mg/kg
686
428
1130
104
75-125
Manganese
mg/kg
127
42.8
112
-35
75-125 MO
Nickel
mg/kg
18.4
42.8
58.2
93
75-125
Potassium
mg/kg
551
428
2270
403
75-125 MO
Selenium
mg/kg
0.93J
42.8
43.0
98
75-125
Silver
mg/kg
0.13J
21.3
21.7
101
75-125
Sodium
mg/kg
133J
428
741
142
75-125 MO
Thallium
mg/kg
0.33J
42.8
35.2
82
75-125
Vanadium
mg/kg
37.1
42.8
82.0
105
75-125
Zinc
mg/kg
535
42.8
445
-210
75-125 MO
SAMPLE DUPLICATE: 604600
9293727001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Aluminum
mg/kg
33000
33100
0
Antimony
mg/kg
ND
ND
Arsenic
mg/kg
1.5
1.4
5
Barium
mg/kg
317
341
7
Beryllium
mg/kg
1.4
1.4
4
Cadmium
mg/kg
6.3
7.5
16
Calcium
mg/kg
271
170
46 R1
Chromium
mg/kg
92.1
87.8
5
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 160 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
SAMPLE DUPLICATE: 604600
Parameter
Units
9293727001
Result
Dup
Result
RPD Qualifiers
Cobalt
mg/kg
17.5
20.8
17
Copper
mg/kg
13.0
14.8
13
Iron
mg/kg
27100
24400
11
Lead
mg/kg
12.8
14.4
12
Magnesium
mg/kg
10100
10000
0
Manganese
mg/kg
1530
1680
9
Nickel
mg/kg
44.5
44.9
1
Potassium
mg/kg
17200
16900
2
Selenium
mg/kg
4.2
2.4
55 R1
Silver
mg/kg
ND
.44J
Sodium
mg/kg
ND
379J
Thallium
mg/kg
1.5
1.8
19
Vanadium
mg/kg
175
177
1
Zinc
mg/kg
109
112
3
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 161 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: MPRP/8352 Analysis Method: EPA6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET
Associated Lab Samples: 9293679021, 9293679024, 9293679025, 9293679026, 9293679027, 9293679028, 9293679029, 9293679030,
9293679036
METHOD BLANK: 605474 Matrix: Solid
Associated Lab Samples: 9293679021, 9293679024, 9293679025, 9293679026, 9293679027, 9293679028, 9293679029, 9293679030,
9293679036,9293679037
Parameter
Units
Blank
Result
Reporting
Limit
Aluminum
mg/kg
ND
10.0
Antimony
mg/kg
ND
0.50
Arsenic
mg/kg
ND
0.50
Barium
mg/kg
ND
0.50
Beryllium
mg/kg
ND
0.10
Cadmium
mg/kg
ND
0.10
Calcium
mg/kg
ND
10.0
Chromium
mg/kg
ND
0.50
Cobalt
mg/kg
ND
0.50
Copper
mg/kg
ND
0.50
Iron
mg/kg
ND
5.0
Lead
mg/kg
ND
0.50
Magnesium
mg/kg
ND
10.0
Manganese
mg/kg
ND
0.50
Nickel
mg/kg
ND
0.50
Potassium
mg/kg
ND
500
Selenium
mg/kg
ND
1.0
Silver
mg/kg
ND
0.50
Sodium
mg/kg
ND
500
Thallium
mg/kg
ND
1.0
Vanadium
mg/kg
ND
0.50
Zinc
mg/kg
ND
1.0
Analyzed Qualifiers
05/14/11 14:14
05/14/11 14:14
05/14/11 14:14
05/14/11 14:14
05/14/11 14:14
05/14/11 14:14
05/14/11 14:14
05/14/11 14:14
05/14/11 14:14
05/14/11 14:14
05/14/11 14:14
05/14/11 14:14
05/14/11 14:14
05/14/11 14:14
05/14/11 14:14
05/14/11 14:14
05/14/11 14:14
05/14/11 14:14
05/14/11 14:14
05/14/11 14:14
05/14/11 14:14
05/14/11 14:14
LABORATORY CONTROL SAMPLE:
Parameter
605475
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Aluminum
mg/kg
500
498
100
80-120
Antimony
mg/kg
50
45.7
91
80-120
Arsenic
mg/kg
50
49.7
99
80-120
Barium
mg/kg
50
49.4
99
80-120
Beryllium
mg/kg
50
52.0
104
80-120
Cadmium
mg/kg
50
51.4
103
80-120
Calcium
mg/kg
500
502
100
80-120
Chromium
mg/kg
50
50.3
101
80-120
Cobalt
mg/kg
50
50.6
101
80-120
Copper
mg/kg
50
48.7
97
80-120
Iron
mg/kg
500
518
104
80-120
Lead
mg/kg
50
50.8
102
80-120
Magnesium
mg/kg
500
513
103
80-120
Manganese
mg/kg
50
49.9
100
80-120
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall
not be reproduced, except in full,
without the written consent
of Analytical
Services, Inc..
PPace
Qualifiers
Page 162 of 227

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
LABORATORY CONTROL SAMPLE:
605475
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Nickel
mg/kg
50
50.8
102
80-120
Potassium
mg/kg
500
484J
97
80-120
Selenium
mg/kg
50
49.4
99
80-120
Silver
mg/kg
25
23.7
95
80-120
Sodium
mg/kg
500
521
104
80-120
Thallium
mg/kg
50
48.4
97
80-120
Vanadium
mg/kg
50
49.1
98
80-120
Zinc
mg/kg
50
51.4
103
80-120
MATRIX SPIKE SAMPLE:
605476
9293302001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Aluminum
mg/kg
11300
626
16500
830
75-125 MO
Antimony
mg/kg
3.3
62.6
51.9
78
75-125
Arsenic
mg/kg
39.1
62.6
115
121
75-125
Barium
mg/kg
249
62.6
337
141
75-125 MO
Beryllium
mg/kg
1.5
62.6
61.5
96
75-125
Cadmium
mg/kg
0.73
62.6
56.8
89
75-125
Calcium
mg/kg
54400
626
82900
4530
75-125 MO
Chromium
mg/kg
27.5
62.6
89.3
99
75-125
Cobalt
mg/kg
11.1
62.6
65.2
86
75-125
Copper
mg/kg
130
62.6
192
99
75-125
Iron
mg/kg
10100
626
10900
131
75-125 MO
Lead
mg/kg
11.8
62.6
65.0
85
75-125
Magnesium
mg/kg
4410
626
4950
86
75-125
Manganese
mg/kg
309
62.6
353
70
75-125 MO
Nickel
mg/kg
12.2
62.6
67.6
88
75-125
Potassium
mg/kg
11100
626
8890
-346
75-125 MO
Selenium
mg/kg
5.0
62.6
74.5
111
75-125
Silver
mg/kg
1.9
31.3
33.6
101
75-125
Sodium
mg/kg
2150
626
3530
221
75-125 MO
Thallium
mg/kg
ND
62.6
45.9
73
75-125 MO
Vanadium
mg/kg
29.2
62.6
87.5
93
75-125
Zinc
mg/kg
249
62.6
362
179
75-125 MO
SAMPLE DUPLICATE: 605477
9293302002
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Aluminum
mg/kg
19500
23500
19
Antimony
mg/kg
1.7
2.4
31
R1
Arsenic
mg/kg
15.6
18.6
18
Barium
mg/kg
213
302
34
R1
Beryllium
mg/kg
1.2
1.4
13
Cadmium
mg/kg
0.68
0.75
10
Calcium
mg/kg
68500
62800
9
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
Page 163 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
SAMPLE DUPLICATE: 605477
Parameter
Units
9293302002
Result
Dup
Result
RPD Qualifiers
Chromium
mg/kg
22.9
23.2
1
Cobalt
mg/kg
1.5
1.0
39 R1
Copper
mg/kg
216
280
26 R1
Iron
mg/kg
9560
10700
11
Lead
mg/kg
15.4
19.9
26 R1
Magnesium
mg/kg
3370
4190
22 R1
Manganese
mg/kg
786
958
20
Nickel
mg/kg
12.2
12.4
2
Potassium
mg/kg
9410
9670
3
Selenium
mg/kg
5.8
5.6
2
Silver
mg/kg
3.4
3.0
12
Sodium
mg/kg
3570
3740
5
Thallium
mg/kg
ND
ND
Vanadium
mg/kg
27.5
32.2
16
Zinc
mg/kg
373
466
22 R1
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 164 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/8395 Analysis Method: EPA6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET
Associated Lab Samples: 9293679043, 9293679044, 9293679045, 9293679046
METHOD BLANK: 608208
Matrix:
Solid
Associated Lab Samples:
9293679043, 9293679044, 9293679045, 9293679046
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Chromium
mg/kg
ND
0.50
05/20/1103:31
Copper
mg/kg
ND
0.50
05/20/1103:31
Iron
mg/kg
ND
5.0
05/20/1114:04
Lead
mg/kg
ND
0.50
05/20/1103:31
Nickel
mg/kg
ND
0.50
05/20/1103:31
Zinc
mg/kg
ND
1.0
05/20/1103:31
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
608209
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Chromium
mg/kg
50 45.4
91
80-120
Copper
mg/kg
50 46.6
93
80-120
Iron
mg/kg
500 533
107
80-120
Lead
mg/kg
50 46.1
92
80-120
Nickel
mg/kg
50 46.4
93
80-120
Zinc
mg/kg
50 46.7
93
80-120
MATRIX SPIKE SAMPLE:
608210
9293679043 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Chromium
mg/kg
24.4 46.8
55.8
67
75-125 MO
Copper
mg/kg
12.2 46.8
54.0
89
75-125
Iron
mg/kg
18100 468
15700
-524
75-125 MO
Lead
mg/kg
22.8 46.8
53.0
65
75-125 MO
Nickel
mg/kg
5.8 46.8
44.2
82
75-125
Zinc
mg/kg
72.9 46.8
109
77
75-125
SAMPLE DUPLICATE: 608211
9293679044 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Chromium
mg/kg
17.2 15.4
11
Copper
mg/kg
8.1 9.4
15
Iron
mg/kg
10800 10400
3
Lead
mg/kg
8.9 11.3
23
R1
Nickel
mg/kg
4.8 5.7
19
Zinc
mg/kg
52.0 52.7
1
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
Page 165 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/8344 Analysis Method: EPA6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET
Associated Lab Samples: 9293679001, 9293679002, 9293679003, 9293679004
METHOD BLANK: 604451
Associated Lab Samples:
Parameter
Matrix: Water
9293679001, 9293679002, 9293679003, 9293679004
Blank Reporting
Units Result Limit
Analyzed
Aluminum
ug/L
ND
100
05/16/1118:36
Antimony
ug/L
ND
5.0
05/16/1118:36
Arsenic
ug/L
ND
5.0
05/16/1118:36
Barium
ug/L
ND
5.0
05/16/1118:36
Beryllium
ug/L
ND
1.0
05/16/1118:36
Cadmium
ug/L
ND
1.0
05/16/1118:36
Calcium
ug/L
ND
100
05/16/1118:36
Chromium
ug/L
ND
5.0
05/16/1118:36
Cobalt
ug/L
ND
5.0
05/16/1118:36
Copper
ug/L
ND
5.0
05/16/1118:36
Iron
ug/L
ND
50.0
05/16/1118:36
Lead
ug/L
ND
5.0
05/16/1118:36
Magnesium
ug/L
ND
100
05/16/1118:36
Manganese
ug/L
ND
5.0
05/16/1118:36
Nickel
ug/L
ND
5.0
05/16/1118:36
Potassium
ug/L
ND
5000
05/16/1118:36
Selenium
ug/L
ND
10.0
05/16/1118:36
Silver
ug/L
ND
5.0
05/16/1118:36
Sodium
ug/L
ND
5000
05/16/1118:36
Thallium
ug/L
ND
10.0
05/16/1118:36
Vanadium
ug/L
ND
5.0
05/16/1118:36
Zinc
ug/L
ND
10.0
05/16/1118:36
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
604452
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Aluminum
ug/L
5000
5250
105
80-120
Antimony
ug/L
500
498
100
80-120
Arsenic
ug/L
500
530
106
80-120
Barium
ug/L
500
555
111
80-120
Beryllium
ug/L
500
558
112
80-120
Cadmium
ug/L
500
547
109
80-120
Calcium
ug/L
5000
5510
110
80-120
Chromium
ug/L
500
526
105
80-120
Cobalt
ug/L
500
540
108
80-120
Copper
ug/L
500
530
106
80-120
Iron
ug/L
5000
5510
110
80-120
Lead
ug/L
500
540
108
80-120
Magnesium
ug/L
5000
5490
110
80-120
Manganese
ug/L
500
552
110
80-120
Nickel
ug/L
500
540
108
80-120
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 166 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
604452
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Potassium
ug/L
5000
4880J
98
80-120
Selenium
ug/L
500
535
107
80-120
Silver
ug/L
250
264
106
80-120
Sodium
ug/L
5000
5150
103
80-120
Thallium
ug/L
500
533
107
80-120
Vanadium
ug/L
500
533
107
80-120
Zinc
ug/L
500
532
106
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 605246
9293844001
Parameter Units Result
MS
Spike
Conc.
MSD
Spike
Conc.
605247
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Aluminum
ug/L
163
5000
5000
5580
5680
108
110
75-125
2
Antimony
ug/L
ND
500
500
487
492
97
98
75-125
1
Arsenic
ug/L
ND
500
500
533
540
107
108
75-125
1
Barium
ug/L
152
500
500
669
678
103
105
75-125
1
Beryllium
ug/L
ND
500
500
536
546
107
109
75-125
2
Cadmium
ug/L
ND
500
500
517
524
103
105
75-125
1
Calcium
ug/L
35800
5000
5000
41200
42800
109
140
75-125
4 MO
Chromium
ug/L
ND
500
500
498
507
99
101
75-125
2
Cobalt
ug/L
ND
500
500
506
514
101
103
75-125
2
Copper
ug/L
2.1J
500
500
514
523
102
104
75-125
2
Iron
ug/L
205
5000
5000
5370
5450
103
105
75-125
1
Lead
ug/L
ND
500
500
494
501
99
100
75-125
1
Magnesium
ug/L
22900
5000
5000
28000
28400
102
109
75-125
1
Manganese
ug/L
51.2
500
500
567
576
103
105
75-125
2
Nickel
ug/L
ND
500
500
504
510
101
102
75-125
1
Potassium
ug/L
10900
5000
5000
17400
17700
131
137
75-125
2 MO
Selenium
ug/L
ND
500
500
527
531
105
106
75-125
1
Silver
ug/L
ND
250
250
257
260
103
104
75-125
1
Sodium
ug/L
31300
5000
5000
37100
37800
114
129
75-125
2 MO
Thallium
ug/L
ND
500
500
484
493
97
99
75-125
2
Vanadium
ug/L
ND
500
500
515
521
103
104
75-125
1
Zinc
ug/L
11.8
500
500
536
542
105
106
75-125
1
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 167 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: MPRP/8349 Analysis Method: EPA6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET
Associated Lab Samples: 9293679005, 9293679007, 9293679008, 9293679009, 9293679010, 9293679011, 9293679012, 9293679013,
9293679014,9293679015,9293679047,9293679048,9293679049,9293679050
METHOD BLANK: 604928 Matrix: Water
Associated Lab Samples: 9293679005, 9293679007, 9293679008, 9293679009, 9293679010, 9293679011, 9293679012, 9293679013,
9293679014,9293679015,9293679047,9293679048,9293679049,9293679050
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Aluminum
ug/L
ND
100
05/12/1121:50
Antimony
ug/L
ND
5.0
05/12/1121:50
Arsenic
ug/L
ND
5.0
05/12/1121:50
Barium
ug/L
ND
5.0
05/12/1121:50
Beryllium
ug/L
ND
1.0
05/12/1121:50
Cadmium
ug/L
ND
1.0
05/12/1121:50
Calcium
ug/L
ND
100
05/12/1121:50
Chromium
ug/L
ND
5.0
05/12/1121:50
Cobalt
ug/L
ND
5.0
05/12/1121:50
Copper
ug/L
ND
5.0
05/12/1121:50
Iron
ug/L
ND
50.0
05/12/1121:50
Lead
ug/L
ND
5.0
05/12/1121:50
Magnesium
ug/L
ND
100
05/12/1121:50
Manganese
ug/L
ND
5.0
05/12/1121:50
Nickel
ug/L
ND
5.0
05/12/1121:50
Potassium
ug/L
ND
5000
05/12/1121:50
Selenium
ug/L
ND
10.0
05/12/1121:50
Silver
ug/L
ND
5.0
05/12/1121:50
Sodium
ug/L
ND
5000
05/12/1121:50
Thallium
ug/L
ND
10.0
05/12/1121:50
Vanadium
ug/L
ND
5.0
05/12/1121:50
Zinc
ug/L
ND
10.0
05/12/1121:50
LABORATORY CONTROL SAMPLE:
Parameter
604929
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Aluminum
ug/L
5000
5110
102
80-120
Antimony
ug/L
500
478
96
80-120
Arsenic
ug/L
500
518
104
80-120
Barium
ug/L
500
512
102
80-120
Beryllium
ug/L
500
484
97
80-120
Cadmium
ug/L
500
534
107
80-120
Calcium
ug/L
5000
5430
109
80-120
Chromium
ug/L
500
519
104
80-120
Cobalt
ug/L
500
522
104
80-120
Copper
ug/L
500
499
100
80-120
Iron
ug/L
5000
5280
106
80-120
Lead
ug/L
500
533
107
80-120
Magnesium
ug/L
5000
5440
109
80-120
Manganese
ug/L
500
519
104
80-120
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 168 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE:
Parameter
604929
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Nickel
ug/L
500
537
107
80-120
Potassium
ug/L
5000
5140
103
80-120
Selenium
ug/L
500
514
103
80-120
Silver
ug/L
250
208
83
80-120
Sodium
ug/L
5000
5010
100
80-120
Thallium
ug/L
500
530
106
80-120
Vanadium
ug/L
500
511
102
80-120
Zinc
ug/L
500
535
107
80-120
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE SAMPLE:
Parameter
604930
Units
9293679005
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Aluminum
ug/L
ND
5000
5310
105
75-125
Antimony
ug/L
ND
500
480
95
75-125
Arsenic
ug/L
ND
500
517
103
75-125
Barium
ug/L
69.1
500
560
98
75-125
Beryllium
ug/L
ND
500
520
104
75-125
Cadmium
ug/L
ND
500
503
101
75-125
Calcium
ug/L
10400
5000
15400
100
75-125
Chromium
ug/L
ND
500
504
100
75-125
Cobalt
ug/L
ND
500
502
100
75-125
Copper
ug/L
ND
500
505
101
75-125
Iron
ug/L
121
5000
5150
101
75-125
Lead
ug/L
ND
500
491
98
75-125
Magnesium
ug/L
6530
5000
11400
98
75-125
Manganese
ug/L
101
500
592
98
75-125
Nickel
ug/L
ND
500
506
101
75-125
Potassium
ug/L
ND
5000
10200
118
75-125
Selenium
ug/L
ND
500
515
103
75-125
Silver
ug/L
9.3
250
248
95
75-125
Sodium
ug/L
73300
5000
71200
-42
75-125 MO
Thallium
ug/L
ND
500
477
95
75-125
Vanadium
ug/L
ND
500
505
101
75-125
Zinc
ug/L
ND
500
521
104
75-125
SAMPLE DUPLICATE: 604931
Parameter
Aluminum
ug/L
Antimony
ug/L
Arsenic
ug/L
Barium
ug/L
Beryllium
ug/L
Cadmium
ug/L
Calcium
ug/L
Date: 05/20/2011 04:57 PM
9293679007 Dup
Units Result Result RPD Qualifiers
220 333 41 R1
ND ND
ND ND
63.8 63.0 1
ND ND
ND ND
19400 19100 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 169 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
SAMPLE DUPLICATE: 604931
Parameter
Units
9293679007
Result
Dup
Result
RPD Qualifiers
Chromium
ug/L
5.0
5.5
8
Cobalt
ug/L
ND
4AJ
Copper
ug/L
ND
ND
Iron
ug/L
401
667
50 R1
Lead
ug/L
ND
ND
Magnesium
ug/L
8670
8600
1
Manganese
ug/L
166
167
1
Nickel
ug/L
ND
ND
Potassium
ug/L
ND
2780J
Selenium
ug/L
ND
ND
Silver
ug/L
ND
ND
Sodium
ug/L
17200
14600
17
Thallium
ug/L
ND
ND
Vanadium
ug/L
ND
ND
Zinc
ug/L
ND
ND
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 170 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: MERP/3478 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury
Associated Lab Samples: 9293679001, 9293679002, 9293679003, 9293679004, 9293679005, 9293679007, 9293679008, 9293679009,
9293679010,9293679011,9293679012,9293679013,9293679014,9293679015
METHOD BLANK: 606746 Matrix: Water
Associated Lab Samples: 9293679001,9293679002,9293679003,9293679004,9293679005,9293679007,9293679008,9293679009,
9293679010,9293679011,9293679012,9293679013,9293679014,9293679015
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.20 05/17/1114:59
LABORATORY CONTROL SAMPLE: 606747
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury ug/L 2.5 2.4 94 80-120
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 171 of 227

®
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
acmnalytical
205 East Meadow Road - Suite A 2225 Riverside Dr.
9800 Kincey Ave. Suite 100
www.paceJabs.com
Eden, NC 27288 Asheville, NC 28804
Huntersville, NC 28078
[phone] [phone]
[phone]
QUALITY CONTROL DATA
Project: Swannanoa
Pace Project No.: 9293679
QC Batch: MERP/3475
Analysis Method: EPA 7471
QC Batch Method: EPA 7471
Analysis Description: 7471 Mercury
Associated Lab Samples: 9293679017, 9293679018, 9293679019, 9293679020, 9293679021, 9293679024, 9293679025,
9293679026,
9293679027, 9293679028, 9293679029, 9293679030, 9293679036
METHOD BLANK: 605185
Matrix: Solid
Associated Lab Samples: 9293679017,9293679018,9293679019,9293679020,9293679021,9293679024,9293679025,9293679026,
9293679027, 9293679028, 9293679029, 9293679030, 9293679036
Blank Reporting
Parameter
Units Result Limit Analyzed Qualifiers
Mercury
mg/kg ND 0.0050 05/13/1115:25
LABORATORY CONTROL SAMPLE:
605186
Spike LCS LCS % Rec
Parameter
Units Conc. Result % Rec Limits Qualifiers
Mercury
mg/kg .067 0.070 104 80-120
MATRIX SPIKE SAMPLE:
605187
9293679017 Spike MS MS
% Rec
Parameter
Units Result Conc. Result % Rec
Limits Qualifiers
Mercury
mg/kg 0.014 .071 0.080 92
75-125
MATRIX SPIKE SAMPLE:
605189
9293679027 Spike MS MS
% Rec
Parameter
Units Result Conc. Result % Rec
Limits Qualifiers
Mercury
mg/kg 0.040 .059 0.079 65
75-125 MO
SAMPLE DUPLICATE: 605188
9293679018 Dup
Parameter
Units Result Result RPD Qualifiers
Mercury
mg/kg 0.030 0.019 45 R1
SAMPLE DUPLICATE: 605190
9293679028 Dup
Parameter
Units Result Result RPD Qualifiers
Mercury
mg/kg 0.0092 0.0069 28 R1
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 172 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: OEXT/13542 Analysis Method: EPA 8270
QC Batch Method: EPA 3546 Analysis Description: 8270 Solid MSSV Microwave
Associated Lab Samples: 9293679017, 9293679018, 9293679019, 9293679020, 9293679021, 9293679023
METHOD BLANK: 604378 Matrix: Solid
Associated Lab Samples: 9293679017, 9293679018, 9293679019, 9293679020, 9293679021, 9293679023
Blank Reporting
Parameter Units Result Limit Analyzed
1,2,4-Trichlorobenzene
ug/kg
ND
330
05/12/11 17:39
1,2-Dichlorobenzene
ug/kg
ND
330
05/12/11 17:39
1,3-Dichlorobenzene
ug/kg
ND
330
05/12/11 17:39
1,4-Dichlorobenzene
ug/kg
ND
330
05/12/11 17:39
1-Methylnaphthalene
ug/kg
ND
330
05/12/11 17:39
2,4,5-Trichlorophenol
ug/kg
ND
330
05/12/11 17:39
2,4,6-Trichlorophenol
ug/kg
ND
330
05/12/11 17:39
2,4-Dichlorophenol
ug/kg
ND
330
05/12/11 17:39
2,4-Dimethylphenol
ug/kg
ND
330
05/12/11 17:39
2,4-Dinitrophenol
ug/kg
ND
1650
05/12/11 17:39
2,4-Dinitrotoluene
ug/kg
ND
330
05/12/11 17:39
2,6-Dinitrotoluene
ug/kg
ND
330
05/12/11 17:39
2-Chloronaphthalene
ug/kg
ND
330
05/12/11 17:39
2-Chlorophenol
ug/kg
ND
330
05/12/11 17:39
2-Methylnaphthalene
ug/kg
ND
330
05/12/11 17:39
2-Methylphenol(o-Cresol)
ug/kg
ND
330
05/12/11 17:39
2-Nitroaniline
ug/kg
ND
1650
05/12/11 17:39
2-Nitrophenol
ug/kg
ND
330
05/12/11 17:39
3&4-Methylphenol(m&p Cresol)
ug/kg
ND
330
05/12/11 17:39
3,3'-Dichlorobenzidine
ug/kg
ND
1650
05/12/11 17:39
3-Nitroaniline
ug/kg
ND
1650
05/12/11 17:39
4,6-Dinitro-2-methyl phenol
ug/kg
ND
660
05/12/11 17:39
4-Bromophenylphenyl ether
ug/kg
ND
330
05/12/11 17:39
4-Chloro-3-methylphenol
ug/kg
ND
660
05/12/11 17:39
4-Chloroaniline
ug/kg
ND
1650
05/12/11 17:39
4-Chlorophenylphenyl ether
ug/kg
ND
330
05/12/11 17:39
4-Nitroaniline
ug/kg
ND
660
05/12/11 17:39
4-Nitrophenol
ug/kg
ND
1650
05/12/11 17:39
Acenaphthene
ug/kg
ND
330
05/12/11 17:39
Acenaphthylene
ug/kg
ND
330
05/12/11 17:39
Aniline
ug/kg
ND
330
05/12/11 17:39
Anthracene
ug/kg
ND
330
05/12/11 17:39
Benzo(a)anthracene
ug/kg
ND
330
05/12/11 17:39
Benzo(a)pyrene
ug/kg
ND
330
05/12/11 17:39
Benzo(b)fluoranthene
ug/kg
ND
330
05/12/11 17:39
Benzo(g,h,i)perylene
ug/kg
ND
330
05/12/11 17:39
Benzo(k)fluoranthene
ug/kg
ND
330
05/12/11 17:39
Benzoic Acid
ug/kg
ND
1650
05/12/11 17:39
Benzyl alcohol
ug/kg
ND
660
05/12/11 17:39
bis(2-Chloroethoxy)methane
ug/kg
ND
330
05/12/11 17:39
bis(2-Chloroethyl) ether
ug/kg
ND
330
05/12/11 17:39
bis(2-Chloroisopropyl) ether
ug/kg
ND
330
05/12/11 17:39
bis(2- Ethyl hexyl)phthalate
ug/kg
ND
330
05/12/11 17:39
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY
ANALYSIS
This report shall not be
reproduced, except in full,
without the written consent
of Pace Analytical
Services, Inc..
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 173 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
METHOD BLANK: 604378
Associated Lab Samples:
Parameter
Matrix: Solid
9293679017, 9293679018, 9293679019, 9293679020, 9293679021, 9293679023
Blank Reporting
Units Result Limit Analyzed
Butyl benzylphthalate
ug/kg
ND
330
05/12/11 17:39
Chrysene
ug/kg
ND
330
05/12/11 17:39
Di-n-butylphthalate
ug/kg
ND
330
05/12/11 17:39
Di-n-octylphthalate
ug/kg
ND
330
05/12/11 17:39
Dibenz(a,h)anthracene
ug/kg
ND
330
05/12/11 17:39
Dibenzofuran
ug/kg
ND
330
05/12/11 17:39
Diethylphthalate
ug/kg
ND
330
05/12/11 17:39
Dimethylphthalate
ug/kg
ND
330
05/12/11 17:39
Fluoranthene
ug/kg
ND
330
05/12/11 17:39
Fluorene
ug/kg
ND
330
05/12/11 17:39
Hexachloro-1,3-butadiene
ug/kg
ND
330
05/12/11 17:39
Hexachlorobenzene
ug/kg
ND
330
05/12/11 17:39
Hexachlorocyclopentadiene
ug/kg
ND
330
05/12/11 17:39
Hexachloroethane
ug/kg
ND
330
05/12/11 17:39
Indeno(1,2,3-cd)pyrene
ug/kg
ND
330
05/12/11 17:39
Isophorone
ug/kg
ND
330
05/12/11 17:39
N-Nitroso-di-n-propylamine
ug/kg
ND
330
05/12/11 17:39
N-Nitrosodimethylamine
ug/kg
ND
330
05/12/11 17:39
N-Nitrosodiphenylamine
ug/kg
ND
330
05/12/11 17:39
Naphthalene
ug/kg
ND
330
05/12/11 17:39
Nitrobenzene
ug/kg
ND
330
05/12/11 17:39
Pentachlorophenol
ug/kg
ND
1650
05/12/11 17:39
Phenanthrene
ug/kg
ND
330
05/12/11 17:39
Phenol
ug/kg
ND
330
05/12/11 17:39
Pyrene
ug/kg
ND
330
05/12/11 17:39
2,4,6-Tribromophenol (S)
%
55
27-110
05/12/11 17:39
2-Fluorobiphenyl (S)
%
60
30-110
05/12/11 17:39
2-Fluorophenol (S)
%
53
13-110
05/12/11 17:39
Nitrobenzene-d5 (S)
%
57
23-110
05/12/11 17:39
Phenol-d6 (S)
%
55
22-110
05/12/11 17:39
Terphenyl-d14 (S)
%
73
28-110
05/12/11 17:39
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
604379
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trichlorobenzene
ug/kg
1670
1200
72
39-101
1,2-Dichlorobenzene
ug/kg
1670
1220
73
36-110
1,3-Dichlorobenzene
ug/kg
1670
1150
69
35-110
1,4-Dichlorobenzene
ug/kg
1670
1220
73
35-110
1-Methylnaphthalene
ug/kg
1670
1200
72
45-105
2,4,5-Trichlorophenol
ug/kg
1670
1250
75
48-109
2,4,6-Trichlorophenol
ug/kg
1670
1250
75
45-111
2,4-Dichlorophenol
ug/kg
1670
1230
74
51-116
2,4-Dimethylphenol
ug/kg
1670
1190
71
42-103
2,4-Dinitrophenol
ug/kg
8330
3550
43
28-103
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Qualifiers
[phone]
Page 174 of 227

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
acmnalytical 205 East Meadow Road - Suite A 2225 Riverside Dr.
www.paceJabs.com Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Project: Swannanoa
Pace Project No.: 9293679
LABORATORY CONTROL SAMPLE:
Parameter
604379
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,4-Dinitrotoluene
ug/kg
1670
1230
74
46-114
2,6-Dinitrotoluene
ug/kg
1670
1190
71
48-112
2-Chloronaphthalene
ug/kg
1670
1220
73
44-105
2-Chlorophenol
ug/kg
1670
1230
74
36-110
2-Methylnaphthalene
ug/kg
1670
1130
68
39-112
2-Methylphenol(o-Cresol)
ug/kg
1670
1260
75
39-101
2-Nitroaniline
ug/kg
3330
2560
77
44-111
2-Nitrophenol
ug/kg
1670
1150
69
41-100
3&4-Methylphenol(m&p Cresol)
ug/kg
1670
1270
76
43-103
3,3'-Dichlorobenzidine
ug/kg
3330
2290
69
10-150
3-Nitroaniline
ug/kg
3330
2190
66
35-110
4,6-Dinitro-2-methyl phenol
ug/kg
3330
1860
56
38-118
4-Bromophenylphenyl ether
ug/kg
1670
1230
74
47-115
4-Chloro-3-methylphenol
ug/kg
3330
2440
73
43-127
4-Chloroaniline
ug/kg
3330
2030
61
34-109
4-Chlorophenylphenyl ether
ug/kg
1670
1210
73
44-115
4-Nitroaniline
ug/kg
3330
2240
67
37-111
4-Nitrophenol
ug/kg
8330
6260
75
21-152
Acenaphthene
ug/kg
1670
1330
80
38-117
Acenaphthylene
ug/kg
1670
1260
76
46-107
Aniline
ug/kg
1670
1070
64
29-110
Anthracene
ug/kg
1670
1350
81
50-110
Benzo(a)anthracene
ug/kg
1670
1340
80
47-116
Benzo(a)pyrene
ug/kg
1670
1200
72
47-106
Benzo(b)fluoranthene
ug/kg
1670
1270
76
47-109
Benzo(g,h,i)perylene
ug/kg
1670
1390
83
39-115
Benzo(k)fluoranthene
ug/kg
1670
1230
74
45-117
Benzoic Acid
ug/kg
8330
2230
27
16-110
Benzyl alcohol
ug/kg
3330
2570
77
38-105
bis(2-Chloroethoxy)methane
ug/kg
1670
1120
67
39-110
bis(2-Chloroethyl) ether
ug/kg
1670
1240
75
19-119
bis(2-Chloroisopropyl) ether
ug/kg
1670
1140
69
21-110
bis(2- Ethyl hexyl)phthalate
ug/kg
1670
1240
75
35-116
Butylbenzylphthalate
ug/kg
1670
1200
72
38-110
Chrysene
ug/kg
1670
1340
80
49-110
Di-n-butylphthalate
ug/kg
1670
1190
72
43-109
Di-n-octylphthalate
ug/kg
1670
1090
65
37-109
Dibenz(a,h)anthracene
ug/kg
1670
1350
81
43-116
Dibenzofuran
ug/kg
1670
1290
77
45-106
Diethylphthalate
ug/kg
1670
1180
71
41-114
Dimethylphthalate
ug/kg
1670
1190
71
43-110
Fluoranthene
ug/kg
1670
1270
76
50-114
Fluorene
ug/kg
1670
1310
79
46-114
Hexachloro-1,3-butadiene
ug/kg
1670
1190
71
28-111
Hexachlorobenzene
ug/kg
1670
1280
77
46-120
Hexachlorocyclopentadiene
ug/kg
1670
896
54
18-119
Hexachloroethane
ug/kg
1670
1100
66
33-110
Indeno(1,2,3-cd)pyrene
ug/kg
1670
1360
81
42-115
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Qualifiers
[phone]
Page 175 of 227

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
LABORATORY CONTROL SAMPLE:
604379
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Isophorone
ug/kg
1670
1170
70
44-109
N-Nitroso-di-n-propylamine
ug/kg
1670
1240
74
43-104
N-Nitrosodimethylamine
ug/kg
1670
1060
64
29-110
N-Nitrosodiphenylamine
ug/kg
1670
1340
81
48-113
Naphthalene
ug/kg
1670
1190
72
41-110
Nitrobenzene
ug/kg
1670
1150
69
38-110
Pentachlorophenol
ug/kg
3330
2010
60
32-128
Phenanthrene
ug/kg
1670
1310
79
50-110
Phenol
ug/kg
1670
1340
80
28-106
Pyrene
ug/kg
1670
1400
84
45-114
2,4,6-Tribromophenol (S)
%
80
27-110
2-Fluorobiphenyl (S)
%
77
30-110
2-Fluorophenol (S)
%
71
13-110
Nitrobenzene-d5 (S)
%
73
23-110
Phenol-d6 (S)
%
73
22-110
Terphenyl-d14 (S)
%
83
28-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
604380
604381
MS
MSD
9293679019
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD Qual
1,2,4-Trichlorobenzene
ug/kg
ND
2040
2040
1330
1080
65
53
18-119
20
1,2-Dichlorobenzene
ug/kg
ND
2040
2040
1350
1060
66
52
50-110
24
1,3-Dichlorobenzene
ug/kg
ND
2040
2040
1300
988
64
48
27-110
27
1,4-Dichlorobenzene
ug/kg
ND
2040
2040
1350
1050
66
52
28-110
25
1-Methylnaphthalene
ug/kg
ND
2040
2040
1380
1120
68
55
24-116
21
2,4,5-Trichlorophenol
ug/kg
ND
2040
2040
1420
1240
70
61
28-110
14
2,4,6-Trichlorophenol
ug/kg
ND
2040
2040
1350
1130
66
55
17-117
18
2,4-Dichlorophenol
ug/kg
ND
2040
2040
1420
1200
70
59
21-128
17
2,4-Dimethylphenol
ug/kg
ND
2040
2040
1160
1020
57
50
10-120
12
2,4-Dinitrophenol
ug/kg
ND
10200
10200
659J
479J
6
5
10-107
M0,M1
2,4-Dinitrotoluene
ug/kg
ND
2040
2040
1230
1080
60
53
36-109
13
2,6-Dinitrotoluene
ug/kg
ND
2040
2040
1260
1110
62
55
32-110
13
2-Chloronaphthalene
ug/kg
ND
2040
2040
1310
1120
64
55
30-107
16
2-Chlorophenol
ug/kg
ND
2040
2040
1290
1050
63
52
14-106
20
2-Methylnaphthalene
ug/kg
ND
2040
2040
1300
1060
64
52
10-135
20
2-Methylphenol(o-Cresol)
ug/kg
ND
2040
2040
1080
982
53
48
10-124
9
2-Nitroaniline
ug/kg
ND
4070
4070
2790
2400
69
59
26-116
15
2-Nitrophenol
ug/kg
ND
2040
2040
1260
1080
62
53
28-103
15
3&4-Methylphenol(m&p
ug/kg
ND
2040
2040
1160
1090
57
53
10-109
7
Cresol)
3,3'-Dichlorobenzidine
ug/kg
ND
4070
4070
1940J
19001
48
47
10-150
3-Nitroaniline
ug/kg
ND
4070
4070
2470
2150
61
53
22-110
14
4,6-Dinitro-2-methyl phenol
ug/kg
ND
4070
4070
1240
977
30
24
13-121
24
4-Bromophenylphenyl ether
ug/kg
ND
2040
2040
1260
1070
62
53
31-109
16
4-Chloro-3-methylphenol
ug/kg
ND
4070
4070
2910
2400
71
59
13-128
19
4-Chloroaniline
ug/kg
ND
4070
4070
2500
2090
61
51
18-102
18
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 176 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 604380
Parameter
4-Chlorophenylphenyl ether
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
bis(2- Ethyl hexyl)phthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenz(a,h)anthracene
Dibenzofuran
Diethylphthalate
Dimethylphthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
I ndeno(1,2,3-cd)pyrene
Isophorone
N-N itroso-d i-n-propylamine
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol(S)
Nitrobenzene-d5 (S)
Date: 05/20/2011 04:57 PM
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
9293679019
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
604381
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MS MSD
Spike Spike MS MSD MS MSD % Rec
Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
2040
2040
1240
1100
4070
4070
2420
2030
10200
10200
5600
4510
2040
2040
1420
1210
2040
2040
1340
1140
2040
2040
1010
874
2040
2040
1330
1150
2040
2040
1230
1160
2040
2040
1070
997
2040
2040
1150
1180
2040
2040
1210
1090
2040
2040
1120
993
10200
10200
ND
ND
4070
4070
2560
2210
2040
2040
1310
1090
2040
2040
1350
1090
2040
2040
1290
1040
2040
2040
1220
1110
2040
2040
1100
1050
2040
2040
1230
1160
2040
2040
1120
975
2040
2040
999
903
2040
2040
1180
1070
2040
2040
1350
1160
2040
2040
1230
1030
2040
2040
1330
1120
2040
2040
1190
1010
2040
2040
1330
1170
2040
2040
1340
1070
2040
2040
1360
1160
2040
2040
583
518
2040
2040
1220
923
2040
2040
1210
1090
2040
2040
1480
1110
2040
2040
1270
1100
2040
2040
1190
894
2040
2040
1310
1160
2040
2040
1330
1090
2040
2040
1330
1120
4070
4070
1940J
1450J
2040
2040
1290
1100
2040
2040
1220
1060
2040
2040
1330
1280
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
61 54
29-112
12
59 50
16-111
17
55 44
14-135
22
70 59
26-114
16
66 56
32-108
16
50 43
10-107
14
65 56
32-111
15
60 57
25-117
6
53 49
25-106
7
56 58
24-110
2
60 53
19-112
11
55 49
24-114
12
0 0
10-110
M0,M1
63 54
24-106
15
64 54
13-119
18
66 54
10-134
21
63 51
10-113
21
60 55
10-125
9
54 52
18-110
5
60 57
30-110
6
55 48
19-112
14
49 44
17-105
10
58 53
23-111
9
66 57
35-103
15
60 50
27-113
18
65 55
26-111
17
58 50
33-109
16
65 57
32-113
13
66 53
16-116
22
67 57
27-120
16
29 25
10-108
12
60 45
10-117
28
60 54
10-122
10
72 55
28-114
28
62 54
27-113
15
58 44
10-109
28
64 57
10-128
12
65 54
25-110
20
65 55
18-114
17
48 36
10-122
63 54
30-114
16
60 52
11-102
14
65 63
25-116
3
69 59
27-110
64 55
30-110
60 48
13-110
66 56
23-110
Page 177 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 604380 604381
MS MSD
9293679019 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phenol-d6 (S) % 54 47 22-110
Terphenyl-d14 (S) % 63 61 28-110
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 178 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: OEXT/13593 Analysis Method: EPA 8270
QC Batch Method: EPA 3546 Analysis Description: 8270 Solid MSSV Microwave
Associated Lab Samples: 9293679024,9293679025,9293679026,9293679027,9293679028,9293679029,9293679030,9293679033,
9293679035,9293679036
METHOD BLANK: 606558 Matrix: Solid
Associated Lab Samples: 9293679024,9293679025,9293679026,9293679027,9293679028,9293679029,9293679030,9293679033,
9293679035,9293679036
Blank Reporting
Parameter
Units Result Limit
Analyzed Qualifiers
1,2,4-Trichlorobenzene
ug/kg
ND
330
05/16/11 22:35
1,2-Dichlorobenzene
ug/kg
ND
330
05/16/11 22:35
1,3-Dichlorobenzene
ug/kg
ND
330
05/16/11 22:35
1,4-Dichlorobenzene
ug/kg
ND
330
05/16/11 22:35
1-Methylnaphthalene
ug/kg
ND
330
05/16/11 22:35
2,4,5-Trichlorophenol
ug/kg
ND
330
05/16/11 22:35
2,4,6-Trichlorophenol
ug/kg
ND
330
05/16/11 22:35
2,4-Dichlorophenol
ug/kg
ND
330
05/16/11 22:35
2,4-Dimethylphenol
ug/kg
ND
330
05/16/11 22:35
2,4-Dinitrophenol
ug/kg
ND
1650
05/16/11 22:35
2,4-Dinitrotoluene
ug/kg
ND
330
05/16/11 22:35
2,6-Dinitrotoluene
ug/kg
ND
330
05/16/11 22:35
2-Chloronaphthalene
ug/kg
ND
330
05/16/11 22:35
2-Chlorophenol
ug/kg
ND
330
05/16/11 22:35
2-Methylnaphthalene
ug/kg
ND
330
05/16/11 22:35
2-Methylphenol(o-Cresol)
ug/kg
ND
330
05/16/11 22:35
2-Nitroaniline
ug/kg
ND
1650
05/16/11 22:35
2-Nitrophenol
ug/kg
ND
330
05/16/11 22:35
3&4-Methylphenol(m&p Cresol)
ug/kg
ND
330
05/16/11 22:35
3,3'-Dichlorobenzidine
ug/kg
ND
1650
05/16/11 22:35
3-Nitroaniline
ug/kg
ND
1650
05/16/11 22:35
4,6-Dinitro-2-methyl phenol
ug/kg
ND
660
05/16/11 22:35
4-Bromophenylphenyl ether
ug/kg
ND
330
05/16/11 22:35
4-Chloro-3-methylphenol
ug/kg
ND
660
05/16/11 22:35
4-Chloroaniline
ug/kg
ND
1650
05/16/11 22:35
4-Chlorophenylphenyl ether
ug/kg
ND
330
05/16/11 22:35
4-Nitroaniline
ug/kg
ND
660
05/16/11 22:35
4-Nitrophenol
ug/kg
ND
1650
05/16/11 22:35
Acenaphthene
ug/kg
ND
330
05/16/11 22:35
Acenaphthylene
ug/kg
ND
330
05/16/11 22:35
Aniline
ug/kg
ND
330
05/16/11 22:35
Anthracene
ug/kg
ND
330
05/16/11 22:35
Benzo(a)anthracene
ug/kg
ND
330
05/16/11 22:35
Benzo(a)pyrene
ug/kg
ND
330
05/16/11 22:35
Benzo(b)fluoranthene
ug/kg
ND
330
05/16/11 22:35
Benzo(g,h,i)perylene
ug/kg
ND
330
05/16/11 22:35
Benzo(k)fluoranthene
ug/kg
ND
330
05/16/11 22:35
Benzoic Acid
ug/kg
ND
1650
05/16/11 22:35
Benzyl alcohol
ug/kg
ND
660
05/16/11 22:35
bis(2-Chloroethoxy)methane
ug/kg
ND
330
05/16/11 22:35
bis(2-Chloroethyl) ether
ug/kg
ND
330
05/16/11 22:35
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Analytical
Services, Inc..
PPace
Page 179 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 606558 Matrix: Solid
Associated Lab Samples: 9293679024,9293679025,9293679026,9293679027,9293679028,9293679029,9293679030,9293679033,
9293679035,9293679036
Parameter
Units
Blank
Result
Reporting
Limit
Analyzed Qualifiers
bis(2-Chloroisopropyl) ether
ug/kg
ND
330
05/16/11 22:35
bis(2- Ethyl hexyl)phthalate
ug/kg
ND
330
05/16/11 22:35
Butylbenzylphthalate
ug/kg
ND
330
05/16/11 22:35
Chrysene
ug/kg
ND
330
05/16/11 22:35
Di-n-butylphthalate
ug/kg
ND
330
05/16/11 22:35
Di-n-octylphthalate
ug/kg
ND
330
05/16/11 22:35
Dibenz(a,h)anthracene
ug/kg
ND
330
05/16/11 22:35
Dibenzofuran
ug/kg
ND
330
05/16/11 22:35
Diethylphthalate
ug/kg
ND
330
05/16/11 22:35
Dimethylphthalate
ug/kg
ND
330
05/16/11 22:35
Fluoranthene
ug/kg
ND
330
05/16/11 22:35
Fluorene
ug/kg
ND
330
05/16/11 22:35
Hexachloro-1,3-butadiene
ug/kg
ND
330
05/16/11 22:35
Hexachlorobenzene
ug/kg
ND
330
05/16/11 22:35
Hexachlorocyclopentadiene
ug/kg
ND
330
05/16/11 22:35
Hexachloroethane
ug/kg
ND
330
05/16/11 22:35
Indeno(1,2,3-cd)pyrene
ug/kg
ND
330
05/16/11 22:35
Isophorone
ug/kg
ND
330
05/16/11 22:35
N-Nitroso-di-n-propylamine
ug/kg
ND
330
05/16/11 22:35
N-Nitrosodimethylamine
ug/kg
ND
330
05/16/11 22:35
N-Nitrosodiphenylamine
ug/kg
ND
330
05/16/11 22:35
Naphthalene
ug/kg
ND
330
05/16/11 22:35
Nitrobenzene
ug/kg
ND
330
05/16/11 22:35
Pentachlorophenol
ug/kg
ND
1650
05/16/11 22:35
Phenanthrene
ug/kg
ND
330
05/16/11 22:35
Phenol
ug/kg
ND
330
05/16/11 22:35
Pyrene
ug/kg
ND
330
05/16/11 22:35
2,4,6-Tribromophenol (S)
%
55
27-110
05/16/11 22:35
2-Fluorobiphenyl (S)
%
68
30-110
05/16/11 22:35
2-Fluorophenol (S)
%
62
13-110
05/16/11 22:35
Nitrobenzene-d5 (S)
%
63
23-110
05/16/11 22:35
Phenol-d6 (S)
%
55
22-110
05/16/11 22:35
Terphenyl-d14 (S)
%
79
28-110
05/16/11 22:35
LABORATORY CONTROL SAMPLE:
Parameter
606559
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
1670
1020
61
39-101
1,2-Dichlorobenzene
ug/kg
1670
1010
60
36-110
1,3-Dichlorobenzene
ug/kg
1670
1010
61
35-110
1,4-Dichlorobenzene
ug/kg
1670
1020
61
35-110
1-Methylnaphthalene
ug/kg
1670
998
60
45-105
2,4,5-Trichlorophenol
ug/kg
1670
989
59
48-109
2,4,6-Trichlorophenol
ug/kg
1670
1030
62
45-111
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 180 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE:
Parameter
606559
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,4-Dichlorophenol
ug/kg
1670
1000
60
51-116
2,4-Dimethylphenol
ug/kg
1670
1010
61
42-103
2,4-Dinitrophenol
ug/kg
8330
4240
51
28-103
2,4-Dinitrotoluene
ug/kg
1670
1230
74
46-114
2,6-Dinitrotoluene
ug/kg
1670
1110
67
48-112
2-Chloronaphthalene
ug/kg
1670
957
57
44-105
2-Chlorophenol
ug/kg
1670
966
58
36-110
2-Methylnaphthalene
ug/kg
1670
935
56
39-112
2-Methylphenol(o-Cresol)
ug/kg
1670
911
55
39-101
2-Nitroaniline
ug/kg
3330
2330
70
44-111
2-Nitrophenol
ug/kg
1670
951
57
41-100
3&4-Methylphenol(m&p Cresol)
ug/kg
1670
891
53
43-103
3,3'-Dichlorobenzidine
ug/kg
3330
1770
53
10-150
3-Nitroaniline
ug/kg
3330
2160
65
35-110
4,6-Dinitro-2-methyl phenol
ug/kg
3330
1790
54
38-118
4-Bromophenylphenyl ether
ug/kg
1670
999
60
47-115
4-Chloro-3-methylphenol
ug/kg
3330
2120
64
43-127
4-Chloroaniline
ug/kg
3330
1730
52
34-109
4-Chlorophenylphenyl ether
ug/kg
1670
1120
67
44-115
4-Nitroaniline
ug/kg
3330
2290
69
37-111
4-Nitrophenol
ug/kg
8330
6240
75
21-152
Acenaphthene
ug/kg
1670
1140
68
38-117
Acenaphthylene
ug/kg
1670
1070
64
46-107
Aniline
ug/kg
1670
895
54
29-110
Anthracene
ug/kg
1670
1150
69
50-110
Benzo(a)anthracene
ug/kg
1670
1090
65
47-116
Benzo(a)pyrene
ug/kg
1670
1010
60
47-106
Benzo(b)fluoranthene
ug/kg
1670
1040
63
47-109
Benzo(g,h,i)perylene
ug/kg
1670
1060
64
39-115
Benzo(k)fluoranthene
ug/kg
1670
1120
67
45-117
Benzoic Acid
ug/kg
8330
2380
29
16-110
Benzyl alcohol
ug/kg
3330
1900
57
38-105
bis(2-Chloroethoxy)methane
ug/kg
1670
992
60
39-110
bis(2-Chloroethyl) ether
ug/kg
1670
997
60
19-119
bis(2-Chloroisopropyl) ether
ug/kg
1670
979
59
21-110
bis(2- Ethyl hexyl)phthalate
ug/kg
1670
998
60
35-116
Butylbenzylphthalate
ug/kg
1670
993
60
38-110
Chrysene
ug/kg
1670
1100
66
49-110
Di-n-butylphthalate
ug/kg
1670
1060
64
43-109
Di-n-octylphthalate
ug/kg
1670
822
49
37-109
Dibenz(a,h)anthracene
ug/kg
1670
1030
62
43-116
Dibenzofuran
ug/kg
1670
1150
69
45-106
Diethylphthalate
ug/kg
1670
1200
72
41-114
Dimethylphthalate
ug/kg
1670
1160
70
43-110
Fluoranthene
ug/kg
1670
1100
66
50-114
Fluorene
ug/kg
1670
1240
74
46-114
Hexachloro-1,3-butadiene
ug/kg
1670
1070
64
28-111
Hexachlorobenzene
ug/kg
1670
1090
65
46-120
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 181 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE:
Parameter
606559
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Hexachlorocyclopentadiene
ug/kg
1670
778
47
18-119
Hexachloroethane
ug/kg
1670
1000
60
33-110
Indeno(1,2,3-cd)pyrene
ug/kg
1670
1030
62
42-115
Isophorone
ug/kg
1670
1060
63
44-109
N-Nitroso-di-n-propylamine
ug/kg
1670
879
53
43-104
N-Nitrosodimethylamine
ug/kg
1670
996
60
29-110
N-Nitrosodiphenylamine
ug/kg
1670
1080
65
48-113
Naphthalene
ug/kg
1670
1030
62
41-110
Nitrobenzene
ug/kg
1670
1010
61
38-110
Pentachlorophenol
ug/kg
3330
1710
51
32-128
Phenanthrene
ug/kg
1670
1120
67
50-110
Phenol
ug/kg
1670
1030
62
28-106
Pyrene
ug/kg
1670
1200
72
45-114
2,4,6-Tribromophenol (S)
%
65
27-110
2-Fluorobiphenyl (S)
%
61
30-110
2-Fluorophenol (S)
%
61
13-110
Nitrobenzene-d5 (S)
%
63
23-110
Phenol-d6 (S)
%
55
22-110
Terphenyl-d14 (S)
%
74
28-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 606560
Parameter
Units
1,2,4-Trichlorobenzene
ug/kg
1,2-Dichlorobenzene
ug/kg
1,3-Dichlorobenzene
ug/kg
1,4-Dichlorobenzene
ug/kg
1-Methylnaphthalene
ug/kg
2,4,5-Trichlorophenol
ug/kg
2,4,6-Trichlorophenol
ug/kg
2,4-Dichlorophenol
ug/kg
2,4-Dimethylphenol
ug/kg
2,4-Dinitrophenol
ug/kg
2,4-Dinitrotoluene
ug/kg
2,6-Dinitrotoluene
ug/kg
2-Chloronaphthalene
ug/kg
2-Chlorophenol
ug/kg
2-Methylnaphthalene
ug/kg
2-Methylphenol(o-Cresol)
ug/kg
2-Nitroaniline
ug/kg
2-Nitrophenol
ug/kg
3&4-Methylphenol(m&p
ug/kg
Cresol)
3,3'-Dichlorobenzidine
ug/kg
3-Nitroaniline
ug/kg
4,6-Dinitro-2-methyl phenol
ug/kg
Date: 05/20/2011 04:57 PM
606561
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
9294023011
Result
MS
Spike
Conc.
MSD
Spike
Conc.
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
ND
1950
1950
1070
1080
55
56
18-119
1
ND
1950
1950
1120
1060
57
54
50-110
6
ND
1950
1950
1110
1050
57
54
27-110
6
ND
1950
1950
1110
1050
57
54
28-110
6
ND
1950
1950
1150
1140
59
59
24-116
1
ND
1950
1950
1150
1140
59
59
28-110
1
ND
1950
1950
1230
1180
63
61
17-117
4
ND
1950
1950
1150
1140
59
59
21-128
1
ND
1950
1950
1200
1170
62
60
10-120
2
ND
9720
9720
2410
2880
25
30
10-107
18
ND
1950
1950
1220
1290
63
66
36-109
6
ND
1950
1950
1180
1220
61
63
32-110
3
ND
1950
1950
1110
1110
57
57
30-107
0
ND
1950
1950
1080
1020
55
53
14-106
5
ND
1950
1950
1080
1060
56
55
10-135
2
ND
1950
1950
1060
1020
55
52
10-124
4
ND
3890
3890
2540
2580
65
66
26-116
2
ND
1950
1950
1050
1050
54
54
28-103
1
ND
1950
1950
1080
1020
56
53
10-109
6
ND
3890
3890
1990
2010
51
52
10-150
1
ND
3890
3890
2240
2350
58
60
22-110
4
ND
3890
3890
1840
1930
47
50
13-121
5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Qual
Page 182 of 227

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
606560
606561
MS
MSD
9294023011
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
4-Bromophenylphenyl ether
ug/kg
ND
1950
1950
1100
1100
56
57
31-109
0
4-Chloro-3-methylphenol
ug/kg
ND
3890
3890
2610
2500
67
64
13-128
5
4-Chloroaniline
ug/kg
ND
3890
3890
2150
2060
55
53
18-102
4
4-Chlorophenylphenyl ether
ug/kg
ND
1950
1950
1170
1220
60
63
29-112
4
4-Nitroaniline
ug/kg
ND
3890
3890
2220
2460
57
63
16-111
10
4-Nitrophenol
ug/kg
ND
9720
9720
5840
6360
60
65
14-135
9
Acenaphthene
ug/kg
ND
1950
1950
1300
1310
67
67
26-114
1
Acenaphthylene
ug/kg
ND
1950
1950
1230
1230
63
63
32-108
0
Aniline
ug/kg
1040
970
7
Anthracene
ug/kg
ND
1950
1950
1260
1280
65
66
32-111
1
Benzo(a)anthracene
ug/kg
ND
1950
1950
1100
1190
56
61
25-117
8
Benzo(a)pyrene
ug/kg
ND
1950
1950
972
1070
50
55
25-106
9
Benzo(b)fluoranthene
ug/kg
ND
1950
1950
972
1070
50
55
24-110
10
Benzo(g,h,i)perylene
ug/kg
ND
1950
1950
1010
1150
52
59
19-112
14
Benzo(k)fluoranthene
ug/kg
ND
1950
1950
1070
1200
55
61
24-114
11
Benzoic Acid
ug/kg
ND
9720
9720
1901
272J
2
3
10-110
M0,M1
Benzyl alcohol
ug/kg
ND
3890
3890
2270
2150
58
55
24-106
6
bis(2-Chloroethoxy)methane
ug/kg
ND
1950
1950
1080
1080
55
56
13-119
1
bis(2-Chloroethyl) ether
ug/kg
ND
1950
1950
1100
1050
56
54
10-134
4
bis(2-Chloroisopropyl) ether
ug/kg
ND
1950
1950
1080
1030
56
53
10-113
5
bis(2- Ethyl hexyl)phthalate
ug/kg
ND
1950
1950
984
1050
51
54
10-125
7
Butylbenzylphthalate
ug/kg
ND
1950
1950
1040
1070
53
55
18-110
3
Chrysene
ug/kg
ND
1950
1950
1120
1200
58
62
30-110
7
Di-n-butylphthalate
ug/kg
ND
1950
1950
1030
1130
53
58
19-112
9
Di-n-octylphthalate
ug/kg
ND
1950
1950
838
892
43
46
17-105
6
Dibenz(a,h)anthracene
ug/kg
ND
1950
1950
986
1070
51
55
23-111
8
Dibenzofuran
ug/kg
ND
1950
1950
1260
1280
65
66
35-103
2
Diethylphthalate
ug/kg
ND
1950
1950
1180
1260
61
65
27-113
7
Dimethylphthalate
ug/kg
ND
1950
1950
1200
1230
62
63
26-111
3
Fluoranthene
ug/kg
ND
1950
1950
1110
1220
57
63
33-109
10
Fluorene
ug/kg
ND
1950
1950
1280
1340
66
69
32-113
4
Hexachloro-1,3-butadiene
ug/kg
ND
1950
1950
1060
1110
54
57
16-116
4
Hexachlorobenzene
ug/kg
ND
1950
1950
1170
1190
60
61
27-120
2
Hexachlorocyclopentadiene
ug/kg
ND
1950
1950
814
868
42
45
10-108
6
Hexachloroethane
ug/kg
ND
1950
1950
1090
1030
56
53
10-117
6
Indeno(1,2,3-cd)pyrene
ug/kg
ND
1950
1950
981
1100
50
57
10-122
12
Isophorone
ug/kg
ND
1950
1950
1270
1220
65
63
28-114
4
N-Nitroso-di-n-propylamine
ug/kg
ND
1950
1950
1090
1020
56
52
27-113
7
N-Nitrosodimethylamine
ug/kg
ND
1950
1950
1090
996
56
51
10-109
9
N-Nitrosodiphenylamine
ug/kg
ND
1950
1950
1280
1240
66
64
10-128
3
Naphthalene
ug/kg
ND
1950
1950
1120
1100
57
56
25-110
2
Nitrobenzene
ug/kg
ND
1950
1950
1100
1090
57
56
18-114
1
Pentachlorophenol
ug/kg
ND
3890
3890
1790J
1890J
46
48
10-122
Phenanthrene
ug/kg
ND
1950
1950
1230
1250
63
64
30-114
2
Phenol
ug/kg
ND
1950
1950
1180
1120
61
58
11-102
5
Pyrene
ug/kg
ND
1950
1950
1340
1320
69
68
25-116
1
2,4,6-Tribromophenol (S)
%
62
60
27-110
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 183 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 606560
606561
MS
MSD
9294023011 Spike
Spike MS MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result Result % Rec
% Rec
Limits RPD Qual
2-Fluorobiphenyl (S)
%
58
58
30-110
2-Fluorophenol (S)
%
57
51
13-110
Nitrobenzene-d5 (S)
%
58
54
23-110
Phenol-d6 (S)
%
52
48
22-110
Terphenyl-d14 (S)
%
62
64
28-110
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 184 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: OEXT/13600 Analysis Method: EPA 8270
QC Batch Method: EPA 3546 Analysis Description: 8270 Solid MSSV Microwave
Associated Lab Samples: 9293679039, 9293679040, 9293679041, 9293679042, 9293679043, 9293679044, 9293679045, 9293679046
METHOD BLANK: 606756 Matrix: Solid
Associated Lab Samples: 9293679039, 9293679040, 9293679041, 9293679042, 9293679043, 9293679044, 9293679045, 9293679046
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,2,4-Trichlorobenzene
ug/kg
ND
330
05/18/11 15:12
1,2-Dichlorobenzene
ug/kg
ND
330
05/18/11 15:12
1,3-Dichlorobenzene
ug/kg
ND
330
05/18/11 15:12
1,4-Dichlorobenzene
ug/kg
ND
330
05/18/11 15:12
1-Methylnaphthalene
ug/kg
ND
330
05/18/11 15:12
2,4,5-Trichlorophenol
ug/kg
ND
330
05/18/11 15:12
2,4,6-Trichlorophenol
ug/kg
ND
330
05/18/11 15:12
2,4-Dichlorophenol
ug/kg
ND
330
05/18/11 15:12
2,4-Dimethylphenol
ug/kg
ND
330
05/18/11 15:12
2,4-Dinitrophenol
ug/kg
ND
1650
05/18/11 15:12
2,4-Dinitrotoluene
ug/kg
ND
330
05/18/11 15:12
2,6-Dinitrotoluene
ug/kg
ND
330
05/18/11 15:12
2-Chloronaphthalene
ug/kg
ND
330
05/18/11 15:12
2-Chlorophenol
ug/kg
ND
330
05/18/11 15:12
2-Methylnaphthalene
ug/kg
ND
330
05/18/11 15:12
2-Methylphenol(o-Cresol)
ug/kg
ND
330
05/18/11 15:12
2-Nitroaniline
ug/kg
ND
1650
05/18/11 15:12
2-Nitrophenol
ug/kg
ND
330
05/18/11 15:12
3&4-Methylphenol(m&p Cresol)
ug/kg
ND
330
05/18/11 15:12
3,3'-Dichlorobenzidine
ug/kg
ND
1650
05/18/11 15:12
3-Nitroaniline
ug/kg
ND
1650
05/18/11 15:12
4,6-Dinitro-2-methyl phenol
ug/kg
ND
660
05/18/11 15:12
4-Bromophenylphenyl ether
ug/kg
ND
330
05/18/11 15:12
4-Chloro-3-methylphenol
ug/kg
ND
660
05/18/11 15:12
4-Chloroaniline
ug/kg
ND
1650
05/18/11 15:12
4-Chlorophenylphenyl ether
ug/kg
ND
330
05/18/11 15:12
4-Nitroaniline
ug/kg
ND
660
05/18/11 15:12
4-Nitrophenol
ug/kg
ND
1650
05/18/11 15:12
Acenaphthene
ug/kg
ND
330
05/18/11 15:12
Acenaphthylene
ug/kg
ND
330
05/18/11 15:12
Aniline
ug/kg
ND
330
05/18/11 15:12
Anthracene
ug/kg
ND
330
05/18/11 15:12
Benzo(a)anthracene
ug/kg
ND
330
05/18/11 15:12
Benzo(a)pyrene
ug/kg
ND
330
05/18/11 15:12
Benzo(b)fluoranthene
ug/kg
ND
330
05/18/11 15:12
Benzo(g,h,i)perylene
ug/kg
ND
330
05/18/11 15:12
Benzo(k)fluoranthene
ug/kg
ND
330
05/18/11 15:12
Benzoic Acid
ug/kg
ND
1650
05/18/11 15:12
Benzyl alcohol
ug/kg
ND
660
05/18/11 15:12
bis(2-Chloroethoxy)methane
ug/kg
ND
330
05/18/11 15:12
bis(2-Chloroethyl) ether
ug/kg
ND
330
05/18/11 15:12
bis(2-Chloroisopropyl) ether
ug/kg
ND
330
05/18/11 15:12
bis(2- Ethyl hexyl)phthalate
ug/kg
ND
330
05/18/11 15:12
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY
ANALYSIS
This report shall not be
reproduced, except in full,
without the written consent
of Pace Analytical
Services, Inc..
Page 185 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
METHOD BLANK: 606756 Matrix: Solid
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Associated Lab Samples: 9293679039, 9293679040, 9293679041, 9293679042, 9293679043, 9293679044, 9293679045, 9293679046
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Butyl benzylphthalate
ug/kg
ND
330
05/18/11 15:12
Chrysene
ug/kg
ND
330
05/18/11 15:12
Di-n-butylphthalate
ug/kg
ND
330
05/18/11 15:12
Di-n-octylphthalate
ug/kg
ND
330
05/18/11 15:12
Dibenz(a,h)anthracene
ug/kg
ND
330
05/18/11 15:12
Dibenzofuran
ug/kg
ND
330
05/18/11 15:12
Diethylphthalate
ug/kg
ND
330
05/18/11 15:12
Dimethylphthalate
ug/kg
ND
330
05/18/11 15:12
Fluoranthene
ug/kg
ND
330
05/18/11 15:12
Fluorene
ug/kg
ND
330
05/18/11 15:12
Hexachloro-1,3-butadiene
ug/kg
ND
330
05/18/11 15:12
Hexachlorobenzene
ug/kg
ND
330
05/18/11 15:12
Hexachlorocyclopentadiene
ug/kg
ND
330
05/18/11 15:12
Hexachloroethane
ug/kg
ND
330
05/18/11 15:12
Indeno(1,2,3-cd)pyrene
ug/kg
ND
330
05/18/11 15:12
Isophorone
ug/kg
ND
330
05/18/11 15:12
N-Nitroso-di-n-propylamine
ug/kg
ND
330
05/18/11 15:12
N-Nitrosodimethylamine
ug/kg
ND
330
05/18/11 15:12
N-Nitrosodiphenylamine
ug/kg
ND
330
05/18/11 15:12
Naphthalene
ug/kg
ND
330
05/18/11 15:12
Nitrobenzene
ug/kg
ND
330
05/18/11 15:12
Pentachlorophenol
ug/kg
ND
1650
05/18/11 15:12
Phenanthrene
ug/kg
ND
330
05/18/11 15:12
Phenol
ug/kg
ND
330
05/18/11 15:12
Pyrene
ug/kg
ND
330
05/18/11 15:12
2,4,6-Tribromophenol (S)
%
59
27-110
05/18/11 15:12
2-Fluorobiphenyl (S)
%
71
30-110
05/18/11 15:12
2-Fluorophenol (S)
%
57
13-110
05/18/11 15:12
Nitrobenzene-d5 (S)
%
59
23-110
05/18/11 15:12
Phenol-d6 (S)
%
54
22-110
05/18/11 15:12
Terphenyl-d14 (S)
%
83
28-110
05/18/11 15:12
LABORATORY CONTROL SAMPLE:
Parameter
606757
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
1670
1110
66
39-101
1,2-Dichlorobenzene
ug/kg
1670
1090
65
36-110
1,3-Dichlorobenzene
ug/kg
1670
1080
65
35-110
1,4-Dichlorobenzene
ug/kg
1670
1070
64
35-110
1-Methylnaphthalene
ug/kg
1670
1170
70
45-105
2,4,5-Trichlorophenol
ug/kg
1670
1250
75
48-109
2,4,6-Trichlorophenol
ug/kg
1670
1330
80
45-111
2,4-Dichlorophenol
ug/kg
1670
1190
71
51-116
2,4-Dimethylphenol
ug/kg
1670
1200
72
42-103
2,4-Dinitrophenol
ug/kg
8330
4690
56
28-103
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
[phone]
Page 186 of 227

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
acmnalytical 205 East Meadow Road - Suite A 2225 Riverside Dr.
www.paceJabs.com Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Project: Swannanoa
Pace Project No.: 9293679
LABORATORY CONTROL SAMPLE:
Parameter
606757
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,4-Dinitrotoluene
ug/kg
1670
1530
92
46-114
2,6-Dinitrotoluene
ug/kg
1670
1330
80
48-112
2-Chloronaphthalene
ug/kg
1670
1300
78
44-105
2-Chlorophenol
ug/kg
1670
1010
61
36-110
2-Methylnaphthalene
ug/kg
1670
1100
66
39-112
2-Methylphenol(o-Cresol)
ug/kg
1670
1010
60
39-101
2-Nitroaniline
ug/kg
3330
2920
88
44-111
2-Nitrophenol
ug/kg
1670
1000
60
41-100
3&4-Methylphenol(m&p Cresol)
ug/kg
1670
1020
61
43-103
3,3'-Dichlorobenzidine
ug/kg
3330
2070
62
10-150
3-Nitroaniline
ug/kg
3330
2720
82
35-110
4,6-Dinitro-2-methyl phenol
ug/kg
3330
2180
65
38-118
4-Bromophenylphenyl ether
ug/kg
1670
1230
74
47-115
4-Chloro-3-methylphenol
ug/kg
3330
2460
74
43-127
4-Chloroaniline
ug/kg
3330
2120
63
34-109
4-Chlorophenylphenyl ether
ug/kg
1670
1400
84
44-115
4-Nitroaniline
ug/kg
3330
2960
89
37-111
4-Nitrophenol
ug/kg
8330
8310
100
21-152
Acenaphthene
ug/kg
1670
1500
90
38-117
Acenaphthylene
ug/kg
1670
1410
85
46-107
Aniline
ug/kg
1670
944
57
29-110
Anthracene
ug/kg
1670
1500
90
50-110
Benzo(a)anthracene
ug/kg
1670
1370
82
47-116
Benzo(a)pyrene
ug/kg
1670
1300
78
47-106
Benzo(b)fluoranthene
ug/kg
1670
1270
76
47-109
Benzo(g,h,i)perylene
ug/kg
1670
1640
99
39-115
Benzo(k)fluoranthene
ug/kg
1670
1470
88
45-117
Benzoic Acid
ug/kg
8330
1640J
20
16-110
Benzyl alcohol
ug/kg
3330
2110
63
38-105
bis(2-Chloroethoxy)methane
ug/kg
1670
1150
69
39-110
bis(2-Chloroethyl) ether
ug/kg
1670
1070
64
19-119
bis(2-Chloroisopropyl) ether
ug/kg
1670
1060
64
21-110
bis(2- Ethyl hexyl)phthalate
ug/kg
1670
1190
71
35-116
Butylbenzylphthalate
ug/kg
1670
1190
71
38-110
Chrysene
ug/kg
1670
1420
85
49-110
Di-n-butylphthalate
ug/kg
1670
1340
80
43-109
Di-n-octylphthalate
ug/kg
1670
828
50
37-109
Dibenz(a,h)anthracene
ug/kg
1670
1500
90
43-116
Dibenzofuran
ug/kg
1670
1490
90
45-106
Diethylphthalate
ug/kg
1670
1510
91
41-114
Dimethylphthalate
ug/kg
1670
1440
86
43-110
Fluoranthene
ug/kg
1670
1470
88
50-114
Fluorene
ug/kg
1670
1560
94
46-114
Hexachloro-1,3-butadiene
ug/kg
1670
1130
68
28-111
Hexachlorobenzene
ug/kg
1670
1340
81
46-120
Hexachlorocyclopentadiene
ug/kg
1670
839
50
18-119
Hexachloroethane
ug/kg
1670
1060
63
33-110
Indeno(1,2,3-cd)pyrene
ug/kg
1670
1520
91
42-115
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Qualifiers
[phone]
Page 187 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
606757
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Isophorone
ug/kg
1670
1240
75
44-109
N-Nitroso-di-n-propylamine
ug/kg
1670
1030
62
43-104
N-Nitrosodimethylamine
ug/kg
1670
1010
61
29-110
N-Nitrosodiphenylamine
ug/kg
1670
1380
83
48-113
Naphthalene
ug/kg
1670
1140
68
41-110
Nitrobenzene
ug/kg
1670
1130
68
38-110
Pentachlorophenol
ug/kg
3330
2120
64
32-128
Phenanthrene
ug/kg
1670
1480
89
50-110
Phenol
ug/kg
1670
1140
68
28-106
Pyrene
ug/kg
1670
1520
91
45-114
2,4,6-Tribromophenol (S)
%
78
27-110
2-Fluorobiphenyl (S)
%
81
30-110
2-Fluorophenol (S)
%
62
13-110
Nitrobenzene-d5 (S)
%
67
23-110
Phenol-d6 (S)
%
59
22-110
Terphenyl-d14 (S)
%
89
28-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 606758
9293847005
Parameter Units Result
MS
Spike
Conc.
MSD
Spike
Conc.
606759
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,2,4-Trichlorobenzene
ug/kg
ND
2060
2060
1150
1160
56
57
18-119
1
1,2-Dichlorobenzene
ug/kg
ND
2060
2060
1260
1150
62
56
50-110
9
1,3-Dichlorobenzene
ug/kg
ND
2060
2060
1220
1100
59
54
27-110
10
1,4-Dichlorobenzene
ug/kg
ND
2060
2060
1230
1130
60
55
28-110
9
1-Methylnaphthalene
ug/kg
ND
2060
2060
1150
1360
56
66
24-116
17
2,4,5-Trichlorophenol
ug/kg
ND
2060
2060
1270
1360
62
66
28-110
7
2,4,6-Trichlorophenol
ug/kg
ND
2060
2060
1350
1480
66
72
17-117
9
2,4-Dichlorophenol
ug/kg
ND
2060
2060
1230
1360
60
66
21-128
10
2,4-Dimethylphenol
ug/kg
ND
2060
2060
1360
1470
67
72
10-120
8
2,4-Dinitrophenol
ug/kg
ND
10300
10300
6370
7410
62
72
10-107
15
2,4-Dinitrotoluene
ug/kg
ND
2060
2060
1270
1590
62
78
36-109
22
2,6-Dinitrotoluene
ug/kg
ND
2060
2060
1280
1500
62
73
32-110
16
2-Chloronaphthalene
ug/kg
ND
2060
2060
1190
1310
58
64
30-107
9
2-Chlorophenol
ug/kg
ND
2060
2060
1360
1190
66
58
14-106
13
2-Methylnaphthalene
ug/kg
ND
2060
2060
1080
1280
53
62
10-135
17
2-Methylphenol(o-Cresol)
ug/kg
ND
2060
2060
1390
1260
68
61
10-124
10
2-Nitroaniline
ug/kg
ND
4100
4100
2660
2950
65
72
26-116
10
2-Nitrophenol
ug/kg
ND
2060
2060
1270
1270
62
62
28-103
0
3&4-Methylphenol(m&p
ug/kg
ND
2060
2060
1390
1340
68
65
10-109
4
Cresol)
3,3'-Dichlorobenzidine
ug/kg
ND
4100
4100
2330
2780
57
68
10-150
18
3-Nitroaniline
ug/kg
ND
4100
4100
2460
2840
60
69
22-110
15
4,6-Dinitro-2-methyl phenol
ug/kg
ND
4100
4100
2920
3040
71
74
13-121
4
4-Bromophenylphenyl ether
ug/kg
ND
2060
2060
1250
1320
61
64
31-109
5
4-Chloro-3-methylphenol
ug/kg
ND
4100
4100
2650
3250
65
79
13-128
21
4-Chloroaniline
ug/kg
ND
4100
4100
2200
2600
54
63
18-102
16
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 188 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 606758
9293847005
Parameter Units Result
MS
Spike
Conc.
MSD
Spike
Conc.
606759
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
4-Chlorophenylphenyl ether
ug/kg
ND
2060
2060
1210
1430
59
70
29-112
17
4-Nitroaniline
ug/kg
ND
4100
4100
2640
3150
64
77
16-111
18
4-Nitrophenol
ug/kg
ND
10300
10300
6940
8050
68
78
14-135
15
Acenaphthene
ug/kg
ND
2060
2060
1340
1540
65
75
26-114
14
Acenaphthylene
ug/kg
ND
2060
2060
1310
1480
64
72
32-108
12
Aniline
ug/kg
1290
1140
12
Anthracene
ug/kg
ND
2060
2060
1380
1510
67
74
32-111
9
Benzo(a)anthracene
ug/kg
ND
2060
2060
1350
1520
66
74
25-117
11
Benzo(a)pyrene
ug/kg
ND
2060
2060
1230
1390
60
68
25-106
12
Benzo(b)fluoranthene
ug/kg
ND
2060
2060
1290
1440
63
70
24-110
11
Benzo(g,h,i)perylene
ug/kg
ND
2060
2060
1310
1480
64
72
19-112
12
Benzo(k)fluoranthene
ug/kg
ND
2060
2060
1290
1430
63
70
24-114
11
Benzoic Acid
ug/kg
ND
10300
10300
3150
2880
31
28
10-110
9
Benzyl alcohol
ug/kg
ND
4100
4100
2920
2750
71
67
24-106
6
bis(2-Chloroethoxy)methane
ug/kg
ND
2060
2060
1150
1250
56
61
13-119
9
bis(2-Chloroethyl) ether
ug/kg
ND
2060
2060
1290
1150
63
56
10-134
11
bis(2-Chloroisopropyl) ether
ug/kg
ND
2060
2060
1220
1100
60
53
10-113
11
bis(2- Ethyl hexyl)phthalate
ug/kg
ND
2060
2060
1300
1400
63
68
10-125
8
Butylbenzylphthalate
ug/kg
ND
2060
2060
1270
1380
62
67
18-110
8
Chrysene
ug/kg
ND
2060
2060
1350
1490
66
73
30-110
10
Di-n-butylphthalate
ug/kg
ND
2060
2060
1200
1410
58
69
19-112
16
Di-n-octylphthalate
ug/kg
ND
2060
2060
1160
1330
57
65
17-105
14
Dibenz(a,h)anthracene
ug/kg
ND
2060
2060
1280
1450
62
71
23-111
13
Dibenzofuran
ug/kg
ND
2060
2060
1290
1490
63
73
35-103
15
Diethylphthalate
ug/kg
ND
2060
2060
1180
1460
58
71
27-113
21
Dimethylphthalate
ug/kg
ND
2060
2060
1220
1430
60
70
26-111
16
Fluoranthene
ug/kg
ND
2060
2060
1340
1580
65
77
33-109
16
Fluorene
ug/kg
ND
2060
2060
1290
1520
63
74
32-113
16
Hexachloro-1,3-butadiene
ug/kg
ND
2060
2060
1160
1130
56
55
16-116
2
Hexachlorobenzene
ug/kg
ND
2060
2060
1310
1390
64
68
27-120
6
Hexachlorocyclopentadiene
ug/kg
ND
2060
2060
1290
1260
63
61
10-108
2
Hexachloroethane
ug/kg
ND
2060
2060
1230
1100
60
54
10-117
11
Indeno(1,2,3-cd)pyrene
ug/kg
ND
2060
2060
1260
1450
62
71
10-122
14
Isophorone
ug/kg
ND
2060
2060
1250
1500
61
73
28-114
18
N-Nitroso-di-n-propylamine
ug/kg
ND
2060
2060
1280
1340
62
65
27-113
4
N-Nitrosodimethylamine
ug/kg
ND
2060
2060
1200
1020
58
50
10-109
15
N-Nitrosodiphenylamine
ug/kg
ND
2060
2060
1360
1430
66
70
10-128
5
Naphthalene
ug/kg
ND
2060
2060
1210
1240
59
60
25-110
2
Nitrobenzene
ug/kg
ND
2060
2060
1180
1160
58
57
18-114
2
Pentachlorophenol
ug/kg
ND
4100
4100
2810
3080
68
75
10-122
9
Phenanthrene
ug/kg
ND
2060
2060
1340
1440
65
70
30-114
8
Phenol
ug/kg
ND
2060
2060
1530
1340
75
66
11-102
13
Pyrene
ug/kg
ND
2060
2060
1410
1450
69
71
25-116
3
2,4,6-Tribromophenol (S)
%
71
72
27-110
2-Fluorobiphenyl (S)
%
61
63
30-110
2-Fluorophenol (S)
%
62
54
13-110
Nitrobenzene-d5 (S)
%
62
58
23-110
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 189 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 606758 606759
MS MSD
9293847005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phenol-d6 (S) % 63 54 22-110
Terphenyl-d14 (S) % 68 68 28-110
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 190 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: OEXT/13567 Analysis Method: EPA 8270
QC Batch Method: EPA 3510 Analysis Description: 8270 Water MSSV
Associated Lab Samples: 9293679005, 9293679007, 9293679008
METHOD BLANK: 605340 Matrix:
Associated Lab Samples: 9293679005, 9293679007, 9293679008
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
10.0
05/16/11 18:56
1,2-Dichlorobenzene
ug/L
ND
10.0
05/16/11 18:56
1,3-Dichlorobenzene
ug/L
ND
10.0
05/16/11 18:56
1,4-Dichlorobenzene
ug/L
ND
10.0
05/16/11 18:56
1-Methylnaphthalene
ug/L
ND
10.0
05/16/11 18:56
2,4,5-Trichlorophenol
ug/L
ND
10.0
05/16/11 18:56
2,4,6-Trichlorophenol
ug/L
ND
10.0
05/16/11 18:56
2,4-Dichlorophenol
ug/L
ND
10.0
05/16/11 18:56
2,4-Dimethylphenol
ug/L
ND
10.0
05/16/11 18:56
2,4-Dinitrophenol
ug/L
ND
50.0
05/16/11 18:56
2,4-Dinitrotoluene
ug/L
ND
10.0
05/16/11 18:56
2,6-Dinitrotoluene
ug/L
ND
10.0
05/16/11 18:56
2-Chloronaphthalene
ug/L
ND
10.0
05/16/11 18:56
2-Chlorophenol
ug/L
ND
10.0
05/16/11 18:56
2-Methylnaphthalene
ug/L
ND
10.0
05/16/11 18:56
2-Methylphenol(o-Cresol)
ug/L
ND
10.0
05/16/11 18:56
2-Nitroaniline
ug/L
ND
50.0
05/16/11 18:56
2-Nitrophenol
ug/L
ND
10.0
05/16/11 18:56
3&4-Methylphenol(m&p Cresol)
ug/L
ND
10.0
05/16/11 18:56
3,3'-Dichlorobenzidine
ug/L
ND
20.0
05/16/11 18:56
3-Nitroaniline
ug/L
ND
50.0
05/16/11 18:56
4,6-Dinitro-2-methyl phenol
ug/L
ND
20.0
05/16/11 18:56
4-Bromophenylphenyl ether
ug/L
ND
10.0
05/16/11 18:56
4-Chloro-3-methylphenol
ug/L
ND
20.0
05/16/11 18:56
4-Chloroaniline
ug/L
ND
20.0
05/16/11 18:56
4-Chlorophenylphenyl ether
ug/L
ND
10.0
05/16/11 18:56
4-Nitroaniline
ug/L
ND
20.0
05/16/11 18:56
4-Nitrophenol
ug/L
ND
50.0
05/16/11 18:56
Acenaphthene
ug/L
ND
10.0
05/16/11 18:56
Acenaphthylene
ug/L
ND
10.0
05/16/11 18:56
Aniline
ug/L
ND
10.0
05/16/11 18:56
Anthracene
ug/L
ND
10.0
05/16/11 18:56
Benzo(a)anthracene
ug/L
ND
10.0
05/16/11 18:56
Benzo(a)pyrene
ug/L
ND
10.0
05/16/11 18:56
Benzo(b)fluoranthene
ug/L
ND
10.0
05/16/11 18:56
Benzo(g,h,i)perylene
ug/L
ND
10.0
05/16/11 18:56
Benzo(k)fluoranthene
ug/L
ND
10.0
05/16/11 18:56
Benzoic Acid
ug/L
ND
50.0
05/16/11 18:56
Benzyl alcohol
ug/L
ND
20.0
05/16/11 18:56
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
05/16/11 18:56
bis(2-Chloroethyl) ether
ug/L
ND
10.0
05/16/11 18:56
bis(2-Chloroisopropyl) ether
ug/L
ND
10.0
05/16/11 18:56
bis(2- Ethyl hexyl)phthalate
ug/L
ND
6.0
05/16/11 18:56
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY
ANALYSIS
This report shall not be
reproduced, except in full,
without the written consent
of Pace Analytical
Services, Inc..
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 191 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
METHOD BLANK: 605340
Associated Lab Samples:
Parameter
Matrix:
9293679005, 9293679007, 9293679008
Blank
Units Result
Water
Reporting
Limit
Analyzed
Butyl benzylphthalate
ug/L
ND
10.0
05/16/11 18:56
Chrysene
ug/L
ND
10.0
05/16/11 18:56
Di-n-butylphthalate
ug/L
ND
10.0
05/16/11 18:56
Di-n-octylphthalate
ug/L
ND
10.0
05/16/11 18:56
Dibenz(a,h)anthracene
ug/L
ND
10.0
05/16/11 18:56
Dibenzofuran
ug/L
ND
10.0
05/16/11 18:56
Diethylphthalate
ug/L
ND
10.0
05/16/11 18:56
Dimethylphthalate
ug/L
ND
10.0
05/16/11 18:56
Fluoranthene
ug/L
ND
10.0
05/16/11 18:56
Fluorene
ug/L
ND
10.0
05/16/11 18:56
Hexachloro-1,3-butadiene
ug/L
ND
10.0
05/16/11 18:56
Hexachlorobenzene
ug/L
ND
10.0
05/16/11 18:56
Hexachlorocyclopentadiene
ug/L
ND
10.0
05/16/11 18:56
Hexachloroethane
ug/L
ND
10.0
05/16/11 18:56
Indeno(1,2,3-cd)pyrene
ug/L
ND
10.0
05/16/11 18:56
Isophorone
ug/L
ND
10.0
05/16/11 18:56
N-Nitroso-di-n-propylamine
ug/L
ND
10.0
05/16/11 18:56
N-Nitrosodimethylamine
ug/L
ND
10.0
05/16/11 18:56
N-Nitrosodiphenylamine
ug/L
ND
10.0
05/16/11 18:56
Naphthalene
ug/L
ND
10.0
05/16/11 18:56
Nitrobenzene
ug/L
ND
10.0
05/16/11 18:56
Pentachlorophenol
ug/L
ND
25.0
05/16/11 18:56
Phenanthrene
ug/L
ND
10.0
05/16/11 18:56
Phenol
ug/L
ND
10.0
05/16/11 18:56
Pyrene
ug/L
ND
10.0
05/16/11 18:56
2,4,6-Tribromophenol (S)
%
94
27-110
05/16/11 18:56
2-Fluorobiphenyl (S)
%
72
27-110
05/16/11 18:56
2-Fluorophenol (S)
%
35
12-110
05/16/11 18:56
Nitrobenzene-d5 (S)
%
85
21-110
05/16/11 18:56
Phenol-d6 (S)
%
22
10-110
05/16/11 18:56
Terphenyl-d14 (S)
%
93
31-107
05/16/11 18:56
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
605341
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trichlorobenzene
ug/L
50
22.8
46
10-110
1,2-Dichlorobenzene
ug/L
50
27.8
56
10-110
1,3-Dichlorobenzene
ug/L
50
26.2
52
10-110
1,4-Dichlorobenzene
ug/L
50
27.2
54
10-110
1-Methylnaphthalene
ug/L
50
26.3
53
21-110
2,4,5-Trichlorophenol
ug/L
50
35.6
71
23-116
2,4,6-Trichlorophenol
ug/L
50
37.7
75
21-114
2,4-Dichlorophenol
ug/L
50
28.2
56
22-120
2,4-Dimethylphenol
ug/L
50
27.1
54
15-109
2,4-Dinitrophenol
ug/L
250
216
86
10-103
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 192 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE:
Parameter
605341
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,4-Dinitrotoluene
ug/L
50
40.5
81
24-119
2,6-Dinitrotoluene
ug/L
50
40.6
81
25-116
2-Chloronaphthalene
ug/L
50
35.0
70
18-110
2-Chlorophenol
ug/L
50
31.4
63
10-104
2-Methylnaphthalene
ug/L
50
24.7
49
16-110
2-Methylphenol(o-Cresol)
ug/L
50
25.5
51
13-110
2-Nitroaniline
ug/L
100
78.1
78
20-117
2-Nitrophenol
ug/L
50
32.9
66
16-108
3&4-Methylphenol(m&p Cresol)
ug/L
50
22.6
45
14-110
3,3'-Dichlorobenzidine
ug/L
100
62.5
63
13-131
3-Nitroaniline
ug/L
100
77.8
78
15-117
4,6-Dinitro-2-methyl phenol
ug/L
100
96.0
96
13-119
4-Bromophenylphenyl ether
ug/L
50
33.1
66
23-120
4-Chloro-3-methylphenol
ug/L
100
58.3
58
21-119
4-Chloroaniline
ug/L
100
53.3
53
10-122
4-Chlorophenylphenyl ether
ug/L
50
34.3
69
22-112
4-Nitroaniline
ug/L
100
78.1
78
14-118
4-Nitrophenol
ug/L
250
70.8
28
10-110
Acenaphthene
ug/L
50
34.3
69
20-105
Acenaphthylene
ug/L
50
31.4
63
23-106
Aniline
ug/L
50
28.6
57
10-110
Anthracene
ug/L
50
35.3
71
25-120
Benzo(a)anthracene
ug/L
50
33.9
68
21-128
Benzo(a)pyrene
ug/L
50
29.1
58
25-116
Benzo(b)fluoranthene
ug/L
50
32.4
65
23-117
Benzo(g,h,i)perylene
ug/L
50
31.1
62
17-128
Benzo(k)fluoranthene
ug/L
50
34.9
70
25-127
Benzoic Acid
ug/L
250
48.2J
19
10-110
Benzyl alcohol
ug/L
100
55.4
55
10-101
bis(2-Chloroethoxy)methane
ug/L
50
30.6
61
19-107
bis(2-Chloroethyl) ether
ug/L
50
31.4
63
10-108
bis(2-Chloroisopropyl) ether
ug/L
50
28.6
57
10-108
bis(2- Ethyl hexyl)phthalate
ug/L
50
32.0
64
16-123
Butylbenzylphthalate
ug/L
50
33.9
68
20-118
Chrysene
ug/L
50
34.5
69
24-125
Di-n-butylphthalate
ug/L
50
32.3
65
23-115
Di-n-octylphthalate
ug/L
50
26.5
53
20-115
Dibenz(a,h)anthracene
ug/L
50
29.6
59
18-131
Dibenzofuran
ug/L
50
33.7
67
23-106
Diethylphthalate
ug/L
50
32.3
65
24-115
Dimethylphthalate
ug/L
50
31.6
63
22-113
Fluoranthene
ug/L
50
36.1
72
24-125
Fluorene
ug/L
50
35.1
70
24-114
Hexachloro-1,3-butadiene
ug/L
50
23.7
47
10-110
Hexachlorobenzene
ug/L
50
34.8
70
22-127
Hexachlorocyclopentadiene
ug/L
50
32.7
65
10-110
Hexachloroethane
ug/L
50
29.7
59
10-110
Indeno(1,2,3-cd)pyrene
ug/L
50
29.9
60
18-130
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 193 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE:
Parameter
605341
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Isophorone
ug/L
50
25.3
51
23-114
N-Nitroso-di-n-propylamine
ug/L
50
31.1
62
21-114
N-Nitrosodimethylamine
ug/L
50
18.5
37
10-110
N-Nitrosodiphenylamine
ug/L
50
32.4
65
24-123
Naphthalene
ug/L
50
25.7
51
14-110
Nitrobenzene
ug/L
50
28.5
57
16-106
Pentachlorophenol
ug/L
100
79.8
80
10-123
Phenanthrene
ug/L
50
34.3
69
25-119
Phenol
ug/L
50
12.3
25
10-110
Pyrene
ug/L
50
34.3
69
22-127
2,4,6-Tribromophenol (S)
%
80
27-110
2-Fluorobiphenyl (S)
%
62
27-110
2-Fluorophenol (S)
%
33
12-110
Nitrobenzene-d5 (S)
%
62
21-110
Phenol-d6 (S)
%
21
10-110
Terphenyl-d14(S)
%
68
31-107
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 194 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: OEXT/13578 Analysis Method: EPA 8270
QC Batch Method: EPA 3510 Analysis Description: 8270 Water MSSV
Associated Lab Samples: 9293679009, 9293679010, 9293679011, 9293679012, 9293679013, 9293679014, 9293679015, 9293679047,
9293679048,9293679049,9293679050
METHOD BLANK: 605916 Matrix: Water
Associated Lab Samples: 9293679009, 9293679010, 9293679011, 9293679012, 9293679013, 9293679014, 9293679015, 9293679047,
9293679048,9293679049,9293679050
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,2,4-Trichlorobenzene
ug/L
ND
10.0
05/17/11 19:33
1,2-Dichlorobenzene
ug/L
ND
10.0
05/17/11 19:33
1,3-Dichlorobenzene
ug/L
ND
10.0
05/17/11 19:33
1,4-Dichlorobenzene
ug/L
ND
10.0
05/17/11 19:33
1-Methylnaphthalene
ug/L
ND
10.0
05/17/11 19:33
2,4,5-Trichlorophenol
ug/L
ND
10.0
05/17/11 19:33
2,4,6-Trichlorophenol
ug/L
ND
10.0
05/17/11 19:33
2,4-Dichlorophenol
ug/L
ND
10.0
05/17/11 19:33
2,4-Dimethylphenol
ug/L
ND
10.0
05/17/11 19:33
2,4-Dinitrophenol
ug/L
ND
50.0
05/17/11 19:33
2,4-Dinitrotoluene
ug/L
ND
10.0
05/17/11 19:33
2,6-Dinitrotoluene
ug/L
ND
10.0
05/17/11 19:33
2-Chloronaphthalene
ug/L
ND
10.0
05/17/11 19:33
2-Chlorophenol
ug/L
ND
10.0
05/17/11 19:33
2-Methylnaphthalene
ug/L
ND
10.0
05/17/11 19:33
2-Methylphenol(o-Cresol)
ug/L
ND
10.0
05/17/11 19:33
2-Nitroaniline
ug/L
ND
50.0
05/17/11 19:33
2-Nitrophenol
ug/L
ND
10.0
05/17/11 19:33
3&4-Methylphenol(m&p Cresol)
ug/L
ND
10.0
05/17/11 19:33
3,3'-Dichlorobenzidine
ug/L
ND
20.0
05/17/11 19:33
3-Nitroaniline
ug/L
ND
50.0
05/17/11 19:33
4,6-Dinitro-2-methyl phenol
ug/L
ND
20.0
05/17/11 19:33
4-Bromophenylphenyl ether
ug/L
ND
10.0
05/17/11 19:33
4-Chloro-3-methylphenol
ug/L
ND
20.0
05/17/11 19:33
4-Chloroaniline
ug/L
ND
20.0
05/17/11 19:33
4-Chlorophenylphenyl ether
ug/L
ND
10.0
05/17/11 19:33
4-Nitroaniline
ug/L
ND
20.0
05/17/11 19:33
4-Nitrophenol
ug/L
ND
50.0
05/17/11 19:33
Acenaphthene
ug/L
ND
10.0
05/17/11 19:33
Acenaphthylene
ug/L
ND
10.0
05/17/11 19:33
Aniline
ug/L
ND
10.0
05/17/11 19:33
Anthracene
ug/L
ND
10.0
05/17/11 19:33
Benzo(a)anthracene
ug/L
ND
10.0
05/17/11 19:33
Benzo(a)pyrene
ug/L
ND
10.0
05/17/11 19:33
Benzo(b)fluoranthene
ug/L
ND
10.0
05/17/11 19:33
Benzo(g,h,i)perylene
ug/L
ND
10.0
05/17/11 19:33
Benzo(k)fluoranthene
ug/L
ND
10.0
05/17/11 19:33
Benzoic Acid
ug/L
ND
50.0
05/17/11 19:33
Benzyl alcohol
ug/L
ND
20.0
05/17/11 19:33
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
05/17/11 19:33
bis(2-Chloroethyl) ether
ug/L
ND
10.0
05/17/11 19:33
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 195 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
METHOD BLANK: 605916 Matrix: Water
Associated Lab Samples: 9293679009, 9293679010, 9293679011, 9293679012, 9293679013, 9293679014, 9293679015, 9293679047,
9293679048,9293679049,9293679050
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
bis(2-Chloroisopropyl) ether
ug/L
ND
10.0
05/17/11 19:33
bis(2- Ethyl hexyl)phthalate
ug/L
ND
6.0
05/17/11 19:33
Butylbenzylphthalate
ug/L
ND
10.0
05/17/11 19:33
Chrysene
ug/L
ND
10.0
05/17/11 19:33
Di-n-butylphthalate
ug/L
ND
10.0
05/17/11 19:33
Di-n-octylphthalate
ug/L
ND
10.0
05/17/11 19:33
Dibenz(a,h)anthracene
ug/L
ND
10.0
05/17/11 19:33
Dibenzofuran
ug/L
ND
10.0
05/17/11 19:33
Diethylphthalate
ug/L
ND
10.0
05/17/11 19:33
Dimethylphthalate
ug/L
ND
10.0
05/17/11 19:33
Fluoranthene
ug/L
ND
10.0
05/17/11 19:33
Fluorene
ug/L
ND
10.0
05/17/11 19:33
Hexachloro-1,3-butadiene
ug/L
ND
10.0
05/17/11 19:33
Hexachlorobenzene
ug/L
ND
10.0
05/17/11 19:33
Hexachlorocyclopentadiene
ug/L
ND
10.0
05/17/11 19:33
Hexachloroethane
ug/L
ND
10.0
05/17/11 19:33
Indeno(1,2,3-cd)pyrene
ug/L
ND
10.0
05/17/11 19:33
Isophorone
ug/L
ND
10.0
05/17/11 19:33
N-Nitroso-di-n-propylamine
ug/L
ND
10.0
05/17/11 19:33
N-Nitrosodimethylamine
ug/L
ND
10.0
05/17/11 19:33
N-Nitrosodiphenylamine
ug/L
ND
10.0
05/17/11 19:33
Naphthalene
ug/L
ND
10.0
05/17/11 19:33
Nitrobenzene
ug/L
ND
10.0
05/17/11 19:33
Pentachlorophenol
ug/L
ND
25.0
05/17/11 19:33
Phenanthrene
ug/L
ND
10.0
05/17/11 19:33
Phenol
ug/L
ND
10.0
05/17/11 19:33
Pyrene
ug/L
ND
10.0
05/17/11 19:33
2,4,6-Tribromophenol (S)
%
44
27-110
05/17/11 19:33
2-Fluorobiphenyl (S)
%
60
27-110
05/17/11 19:33
2-Fluorophenol (S)
%
34
12-110
05/17/11 19:33
Nitrobenzene-d5 (S)
%
56
21-110
05/17/11 19:33
Phenol-d6 (S)
%
19
10-110
05/17/11 19:33
Terphenyl-d14 (S)
%
72
31-107
05/17/11 19:33
LABORATORY CONTROL SAMPLE:
Parameter
605917
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
23.3
47
10-110
1,2-Dichlorobenzene
ug/L
50
22.5
45
10-110
1,3-Dichlorobenzene
ug/L
50
21.4
43
10-110
1,4-Dichlorobenzene
ug/L
50
21.9
44
10-110
1-Methylnaphthalene
ug/L
50
25.8
52
21-110
2,4,5-Trichlorophenol
ug/L
50
28.4
57
23-116
2,4,6-Trichlorophenol
ug/L
50
28.8
58
21-114
[phone]
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 196 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
605917
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,4-Dichlorophenol
ug/L
50
26.9
54
22-120
2,4-Dimethylphenol
ug/L
50
28.4
57
15-109
2,4-Dinitrophenol
ug/L
250
67.9
27
10-103
2,4-Dinitrotoluene
ug/L
50
34.1
68
24-119
2,6-Dinitrotoluene
ug/L
50
31.2
62
25-116
2-Chloronaphthalene
ug/L
50
27.1
54
18-110
2-Chlorophenol
ug/L
50
24.9
50
10-104
2-Methylnaphthalene
ug/L
50
24.0
48
16-110
2-Methylphenol(o-Cresol)
ug/L
50
22.3
45
13-110
2-Nitroaniline
ug/L
100
65.2
65
20-117
2-Nitrophenol
ug/L
50
25.0
50
16-108
3&4-Methylphenol(m&p Cresol)
ug/L
50
19.7
39
14-110
3,3'-Dichlorobenzidine
ug/L
100
49.9
50
13-131
3-Nitroaniline
ug/L
100
62.0
62
15-117
4,6-Dinitro-2-methyl phenol
ug/L
100
41.2
41
13-119
4-Bromophenylphenyl ether
ug/L
50
28.8
58
23-120
4-Chloro-3-methylphenol
ug/L
100
56.3
56
21-119
4-Chloroaniline
ug/L
100
49.3
49
10-122
4-Chlorophenylphenyl ether
ug/L
50
30.9
62
22-112
4-Nitroaniline
ug/L
100
63.2
63
14-118
4-Nitrophenol
ug/L
250
64.4
26
10-110
Acenaphthene
ug/L
50
32.7
65
20-105
Acenaphthylene
ug/L
50
30.3
61
23-106
Aniline
ug/L
50
23.6
47
10-110
Anthracene
ug/L
50
34.7
69
25-120
Benzo(a)anthracene
ug/L
50
31.7
63
21-128
Benzo(a)pyrene
ug/L
50
29.8
60
25-116
Benzo(b)fluoranthene
ug/L
50
29.2
58
23-117
Benzo(g,h,i)perylene
ug/L
50
35.5
71
17-128
Benzo(k)fluoranthene
ug/L
50
33.9
68
25-127
Benzoic Acid
ug/L
250
ND
1
10-110 L2
Benzyl alcohol
ug/L
100
45.3
45
10-101
bis(2-Chloroethoxy)methane
ug/L
50
26.9
54
19-107
bis(2-Chloroethyl) ether
ug/L
50
27.0
54
10-108
bis(2-Chloroisopropyl) ether
ug/L
50
26.9
54
10-108
bis(2- Ethyl hexyl)phthalate
ug/L
50
29.5
59
16-123
Butylbenzylphthalate
ug/L
50
28.9
58
20-118
Chrysene
ug/L
50
32.9
66
24-125
Di-n-butylphthalate
ug/L
50
31.4
63
23-115
Di-n-octylphthalate
ug/L
50
21.5
43
20-115
Dibenz(a,h)anthracene
ug/L
50
33.6
67
18-131
Dibenzofuran
ug/L
50
32.4
65
23-106
Diethylphthalate
ug/L
50
34.2
68
24-115
Dimethylphthalate
ug/L
50
32.8
66
22-113
Fluoranthene
ug/L
50
32.4
65
24-125
Fluorene
ug/L
50
34.6
69
24-114
Hexachloro-1,3-butadiene
ug/L
50
20.8
42
10-110
Hexachlorobenzene
ug/L
50
32.0
64
22-127
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 197 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE:
Parameter
605917
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Hexachlorocyclopentadiene
ug/L
50
13.5
27
10-110
Hexachloroethane
ug/L
50
19.2
38
10-110
Indeno(1,2,3-cd)pyrene
ug/L
50
34.0
68
18-130
Isophorone
ug/L
50
29.2
58
23-114
N-Nitroso-di-n-propylamine
ug/L
50
24.5
49
21-114
N-Nitrosodimethylamine
ug/L
50
17.6
35
10-110
N-Nitrosodiphenylamine
ug/L
50
32.5
65
24-123
Naphthalene
ug/L
50
26.8
54
14-110
Nitrobenzene
ug/L
50
28.7
57
16-106
Pentachlorophenol
ug/L
100
42.9
43
10-123
Phenanthrene
ug/L
50
33.9
68
25-119
Phenol
ug/L
50
13.3
27
10-110
Pyrene
ug/L
50
36.5
73
22-127
2,4,6-Tribromophenol (S)
%
59
27-110
2-Fluorobiphenyl (S)
%
59
27-110
2-Fluorophenol (S)
%
34
12-110
Nitrobenzene-d5 (S)
%
57
21-110
Phenol-d6 (S)
%
20
10-110
Terphenyl-d14(S)
%
72
31-107
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 605918
Parameter
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1-Methylnaphthalene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
2-Nitroaniline
2-Nitrophenol
3&4-Methylphenol(m&p
Cresol)
3,3'-Dichlorobenzidine
3-Nitroaniline
4,6-Dinitro-2-methyl phenol
Date: 05/20/2011 04:57 PM
605919
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Units
9293679009
Result
MS
Spike
Conc.
MSD
Spike
Conc.
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
ug/L
ND
50
50
19.8
19.8
40
40
10-110
ug/L
ND
50
50
18.5
19.3
37
39
10-110
ug/L
ND
50
50
17.0
18.0
34
36
10-110
ug/L
ND
50
50
17.4
18.6
35
37
10-110
ug/L
ND
50
50
25.0
24.9
50
50
14-110
ug/L
ND
50
50
6.2J
27.4
12
55
19-105
ug/L
ND
50
50
3J
29.5
6
59
13-108
ug/L
ND
50
50
14.1
27.0
28
54
29-111
ug/L
ND
50
50
28.6
29.6
57
59
21-103
ug/L
ND
250
250
ND
14.9J
0
6
10-109
ug/L
ND
50
50
25.8
28.7
52
57
27-104
ug/L
ND
50
50
28.4
29.8
57
60
28-101
ug/L
ND
50
50
28.7
28.1
57
56
14-102
ug/L
ND
50
50
16.7
23.7
33
47
16-110
ug/L
ND
50
50
23.2
23.4
46
47
13-110
ug/L
ND
50
50
25.4
25.5
51
51
19-110
ug/L
ND
100
100
56.2
57.6
56
58
26-103
ug/L
ND
50
50
11.6
26.3
23
53
20-110
ug/L
ND
50
50
24.6
25.8
49
52
20-110
ug/L
ND
100
100
47.4
47.3
47
47
25-112
ug/L
ND
100
100
53.4
54.2
53
54
29-110
ug/L
ND
100
100
ND
32.0
0
32
10-117
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
RPD Qual
0
4
6
6
0
M0,M1
M0,M1
63 M0,M1,R1
3
M0,M1
10
5
2
35 R1
1
1
2
78 R1
5
0
1
M0,M1
Page 198 of 227

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Swannanoa
Pace Project No.: 9293679
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
605918
605919
MS
MSD
9293679009
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
Qual
4-Bromophenylphenyl ether
ug/L
ND
50
50
31.9
30.9
64
62
20-105
3
4-Chloro-3-methylphenol
ug/L
ND
100
100
54.6
56.3
55
56
22-110
3
4-Chloroaniline
ug/L
ND
100
100
52.4
51.7
52
52
20-100
1
4-Chlorophenylphenyl ether
ug/L
ND
50
50
29.1
29.7
58
59
19-102
2
4-Nitroaniline
ug/L
ND
100
100
45.5
49.3
46
49
29-110
8
4-Nitrophenol
ug/L
ND
250
250
ND
71.7
0
29
10-110
M0,M1
Acenaphthene
ug/L
ND
50
50
32.3
31.8
65
64
17-100
2
Acenaphthylene
ug/L
ND
50
50
30.7
30.1
61
60
21-100
2
Aniline
ug/L
ND
50
50
23.4
24.5
47
49
10-110
4
Anthracene
ug/L
ND
50
50
33.7
32.9
67
66
24-109
2
Benzo(a)anthracene
ug/L
ND
50
50
32.3
32.7
65
65
22-117
1
Benzo(a)pyrene
ug/L
ND
50
50
27.4
29.3
55
59
23-104
7
Benzo(b)fluoranthene
ug/L
ND
50
50
29.5
32.0
59
64
23-103
8
Benzo(g,h,i)perylene
ug/L
ND
50
50
28.9
29.1
58
58
18-111
1
Benzo(k)fluoranthene
ug/L
ND
50
50
30.1
32.8
60
66
22-113
8
Benzoic Acid
ug/L
ND
250
250
ND
ND
0
0
10-110
MO
Benzyl alcohol
ug/L
ND
100
100
52.9
54.9
53
55
19-101
4
bis(2-Chloroethoxy)methane
ug/L
ND
50
50
25.2
25.8
50
52
22-110
2
bis(2-Chloroethyl) ether
ug/L
ND
50
50
22.9
23.9
46
48
16-110
4
bis(2-Chloroisopropyl) ether
ug/L
ND
50
50
22.2
22.9
44
46
14-110
3
bis(2- Ethyl hexyl)phthalate
ug/L
ND
50
50
31.4
31.5
63
63
23-102
0
Butylbenzylphthalate
ug/L
ND
50
50
30.5
30.9
61
62
25-110
1
Chrysene
ug/L
ND
50
50
33.4
33.3
67
67
23-115
0
Di-n-butylphthalate
ug/L
ND
50
50
28.6
28.1
57
56
26-110
2
Di-n-octylphthalate
ug/L
ND
50
50
26.5
26.9
53
54
22-110
2
Dibenz(a,h)anthracene
ug/L
ND
50
50
28.2
28.6
56
57
21-112
1
Dibenzofuran
ug/L
ND
50
50
31.6
31.1
63
62
19-102
2
Diethylphthalate
ug/L
ND
50
50
27.5
28.9
55
58
29-110
5
Dimethylphthalate
ug/L
ND
50
50
29.1
29.7
58
59
27-110
2
Fluoranthene
ug/L
ND
50
50
30.0
29.4
60
59
23-112
2
Fluorene
ug/L
ND
50
50
30.8
31.0
62
62
22-104
1
Hexachloro-1,3-butadiene
ug/L
ND
50
50
17.3
16.9
35
34
10-110
2
Hexachlorobenzene
ug/L
ND
50
50
34.3
32.7
69
65
21-116
5
Hexachlorocyclopentadiene
ug/L
ND
50
50
20.7
21.0
41
42
10-110
2
Hexachloroethane
ug/L
ND
50
50
15.1
16.0
30
32
10-110
6
Indeno(1,2,3-cd)pyrene
ug/L
ND
50
50
28.1
28.6
56
57
20-113
2
Isophorone
ug/L
ND
50
50
28.4
29.4
57
59
50-150
3
N-Nitroso-di-n-propylamine
ug/L
ND
50
50
24.8
25.6
50
51
21-105
3
N-Nitrosodimethylamine
ug/L
ND
50
50
19.1
19.7
38
39
10-110
3
N-Nitrosodiphenylamine
ug/L
ND
50
50
30.4
29.7
61
59
23-107
2
Naphthalene
ug/L
ND
50
50
23.9
23.9
48
48
10-110
0
Nitrobenzene
ug/L
ND
50
50
25.8
26.6
52
53
20-110
3
Pentachlorophenol
ug/L
ND
100
100
ND
18.6J
0
19
10-118
M0,M1
Phenanthrene
ug/L
ND
50
50
32.5
31.8
65
64
24-106
2
Phenol
ug/L
ND
50
50
17.7
19.7
35
39
12-110
10
Pyrene
ug/L
ND
50
50
34.5
35.3
69
71
24-114
2
2,4,6-Tribromophenol (S)
%
11
60
27-110
SO
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 199 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 605918
605919
MS
MSD
9293679009 Spike
Spike MS MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result Result % Rec
% Rec
Limits RPD Qual
2-Fluorobiphenyl (S)
%
60
61
27-110
2-Fluorophenol (S)
%
18
38
12-110
Nitrobenzene-d5 (S)
%
48
49
21-110
Phenol-d6 (S)
%
28
31
10-110
Terphenyl-d14(S)
%
66
70
31-107
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 200 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
QC Batch: MSV/15193 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level
Associated Lab Samples: 9293679001, 9293679002, 9293679003, 9293679004, 9293679005, 9293679006, 9293679007, 9293679008,
9293679009,9293679010,9293679011,9293679012,9293679013,9293679014,9293679015,9293679016,
9293679038
METHOD BLANK: 603954
Matrix: Water
Associated Lab Samples: 9293679001,9293679002,9293679003,9293679004,9293679005,9293679006,9293679007,9293679008,
9293679009,9293679010,9293679011,9293679012,9293679013,9293679014,9293679015,9293679016,
9293679038
Blank Reporting
Parameter
Units Result Limit
Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
05/11/11 00:56
1,1,1-Trichloroethane
ug/L
ND
1.0
05/11/11 00:56
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
05/11/11 00:56
1,1,2-Trichloroethane
ug/L
ND
1.0
05/11/11 00:56
1,1-Dichloroethane
ug/L
ND
1.0
05/11/11 00:56
1,1-Dichloroethene
ug/L
ND
1.0
05/11/11 00:56
1,1-Dichloropropene
ug/L
ND
1.0
05/11/11 00:56
1,2,3-Trichlorobenzene
ug/L
ND
1.0
05/11/11 00:56
1,2,3-Trichloropropane
ug/L
ND
1.0
05/11/11 00:56
1,2,4-Trichlorobenzene
ug/L
ND
1.0
05/11/11 00:56
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
05/11/11 00:56
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
05/11/11 00:56
1,2-Dichlorobenzene
ug/L
ND
1.0
05/11/11 00:56
1,2-Dichloroethane
ug/L
ND
1.0
05/11/11 00:56
1,2-Dichloropropane
ug/L
ND
1.0
05/11/11 00:56
1,3-Dichlorobenzene
ug/L
ND
1.0
05/11/11 00:56
1,3-Dichloropropane
ug/L
ND
1.0
05/11/11 00:56
1,4-Dichlorobenzene
ug/L
ND
1.0
05/11/11 00:56
2,2-Dichloropropane
ug/L
ND
1.0
05/11/11 00:56
2-Butanone (MEK)
ug/L
ND
5.0
05/11/11 00:56
2-Chlorotoluene
ug/L
ND
1.0
05/11/11 00:56
2-Hexanone
ug/L
ND
5.0
05/11/11 00:56
4-Chlorotoluene
ug/L
ND
1.0
05/11/11 00:56
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
05/11/11 00:56
Acetone
ug/L
ND
25.0
05/11/11 00:56
Benzene
ug/L
ND
1.0
05/11/11 00:56
Bromobenzene
ug/L
ND
1.0
05/11/11 00:56
Bromochloromethane
ug/L
ND
1.0
05/11/11 00:56
Bromodichloromethane
ug/L
ND
1.0
05/11/11 00:56
Bromoform
ug/L
ND
1.0
05/11/11 00:56
Bromomethane
ug/L
ND
2.0
05/11/11 00:56
Carbon tetrachloride
ug/L
ND
1.0
05/11/11 00:56
Chlorobenzene
ug/L
ND
1.0
05/11/11 00:56
Chloroethane
ug/L
ND
1.0
05/11/11 00:56
Chloroform
ug/L
ND
1.0
05/11/11 00:56
Chloromethane
ug/L
ND
1.0
05/11/11 00:56
cis-1,2-Dichloroethene
ug/L
ND
1.0
05/11/11 00:56
cis-1,3-Dichloropropene
ug/L
ND
1.0
05/11/11 00:56
Dibromochloromethane
ug/L
ND
1.0
05/11/11 00:56
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Analytical
Services, Inc..
PPace
[phone]
Page 201 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 603954 Matrix: Water
Associated Lab Samples: 9293679001, 9293679002, 9293679003, 9293679004, 9293679005, 9293679006, 9293679007, 9293679008,
9293679009,9293679010,9293679011,9293679012,9293679013,9293679014,9293679015,9293679016,
9293679038
Parameter
Units
Blank
Result
Reporting
Limit
Dibromomethane
ug/L
ND
1.0
Dichlorodifluoromethane
ug/L
ND
1.0
Diisopropyl ether
ug/L
ND
1.0
Ethylbenzene
ug/L
ND
1.0
Hexachloro-1,3-butadiene
ug/L
ND
1.0
m&p-Xylene
ug/L
ND
2.0
Methyl-tert-butyl ether
ug/L
ND
1.0
Methylene Chloride
ug/L
ND
2.0
Naphthalene
ug/L
ND
1.0
o-Xylene
ug/L
ND
1.0
p-Isopropyltoluene
ug/L
ND
1.0
Styrene
ug/L
ND
1.0
Tetrachloroethene
ug/L
ND
1.0
Toluene
ug/L
ND
1.0
trans- 1,2-Dichloroethene
ug/L
ND
1.0
trans- 1,3-Dichloropropene
ug/L
ND
1.0
Trichloroethene
ug/L
ND
1.0
Trichlorofluoromethane
ug/L
ND
1.0
Vinyl acetate
ug/L
ND
2.0
Vinyl chloride
ug/L
ND
1.0
1,2-Dichloroethane-d4 (S)
%
107
70-130
4-Bromofluorobenzene (S)
%
94
70-130
Dibromofluoromethane (S)
%
102
70-130
Toluene-d8 (S)
%
102
70-130
Analyzed Qualifiers
05/11 /11 00:56
05/11 /11 00:56
05/11 /11 00:56
05/11 /11 00:56
05/11 /11 00:56
05/11 /11 00:56
05/11 /11 00:56
05/11 /11 00:56
05/11 /11 00:56
05/11 /11 00:56
05/11 /11 00:56
05/11 /11 00:56
05/11 /11 00:56
05/11 /11 00:56
05/11 /11 00:56
05/11 /11 00:56
05/11 /11 00:56
05/11 /11 00:56
05/11 /11 00:56
05/11 /11 00:56
05/11 /11 00:56
05/11 /11 00:56
05/11 /11 00:56
05/11 /11 00:56
LABORATORY CONTROL SAMPLE:
Parameter
603955
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
52.5
105
70-130
1,1,1-Trichloroethane
ug/L
50
52.8
106
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
51.2
102
70-130
1,1,2-Trichloroethane
ug/L
50
50.9
102
70-130
1,1-Dichloroethane
ug/L
50
56.7
113
70-130
1,1-Dichloroethene
ug/L
50
53.9
108
70-132
1,1-Dichloropropene
ug/L
50
49.1
98
70-130
1,2,3-Trichlorobenzene
ug/L
50
51.3
103
70-135
1,2,3-Trichloropropane
ug/L
50
48.9
98
70-130
1,2,4-Trichlorobenzene
ug/L
50
50.5
101
70-134
1,2-Dibromo-3-chloropropane
ug/L
50
51.5
103
70-130
1,2-Dibromoethane (EDB)
ug/L
50
52.4
105
70-130
1,2-Dichlorobenzene
ug/L
50
50.9
102
70-130
1,2-Dichloroethane
ug/L
50
55.4
111
70-130
1,2-Dichloropropane
ug/L
50
52.4
105
70-130
1,3-Dichlorobenzene
ug/L
50
51.3
103
70-130
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not
be reproduced, except in full,
without the written consent of Pace Analytical
Services, Inc..
Qualifiers
Page 202 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE:
Parameter
603955
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichloropropane
ug/L
50
51.4
103
70-130
1,4-Dichlorobenzene
ug/L
50
49.6
99
70-130
2,2-Dichloropropane
ug/L
50
50.1
100
58-145
2-Butanone (MEK)
ug/L
100
102
102
70-145
2-Chlorotoluene
ug/L
50
50.2
100
70-130
2-Hexanone
ug/L
100
101
101
70-144
4-Chlorotoluene
ug/L
50
52.5
105
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
104
104
70-140
Acetone
ug/L
100
99.3
99
50-175
Benzene
ug/L
50
51.0
102
70-130
Bromobenzene
ug/L
50
52.4
105
70-130
Bromochloromethane
ug/L
50
50.8
102
70-130
Bromodichloromethane
ug/L
50
54.0
108
70-130
Bromoform
ug/L
50
50.8
102
70-130
Bromomethane
ug/L
50
51.7
103
54-130
Carbon tetrachloride
ug/L
50
50.3
101
70-132
Chlorobenzene
ug/L
50
50.3
101
70-130
Chloroethane
ug/L
50
51.9
104
64-134
Chloroform
ug/L
50
55.5
111
70-130
Chloromethane
ug/L
50
50.4
101
64-130
cis-1,2-Dichloroethene
ug/L
50
53.7
107
70-131
cis-1,3-Dichloropropene
ug/L
50
51.2
102
70-130
Dibromochloromethane
ug/L
50
51.4
103
70-130
Dibromomethane
ug/L
50
51.3
103
70-131
Dichlorodifluoromethane
ug/L
50
50.6
101
56-130
Diisopropyl ether
ug/L
50
57.4
115
70-130
Ethylbenzene
ug/L
50
51.0
102
70-130
Hexachloro-1,3-butadiene
ug/L
50
49.7
99
70-130
m&p-Xylene
ug/L
100
103
103
70-130
Methyl-tert-butyl ether
ug/L
50
52.5
105
70-130
Methylene Chloride
ug/L
50
57.1
114
63-130
Naphthalene
ug/L
50
49.7
99
70-138
o-Xylene
ug/L
50
51.2
102
70-130
p-Isopropyltoluene
ug/L
50
52.3
105
70-130
Styrene
ug/L
50
52.1
104
70-130
Tetrachloroethene
ug/L
50
51.3
103
70-130
Toluene
ug/L
50
50.1
100
70-130
trans- 1,2-Dichloroethene
ug/L
50
54.3
109
70-130
trans- 1,3-Dichloropropene
ug/L
50
52.4
105
70-132
Trichloroethene
ug/L
50
49.8
100
70-130
Trichlorofluoromethane
ug/L
50
51.1
102
62-133
Vinyl acetate
ug/L
100
112
112
66-157
Vinyl chloride
ug/L
50
51.3
103
69-130
1,2-Dichloroethane-d4 (S)
%
105
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Dibromocuoromethane (S)
%
105
70-130
Toluene-d8(S)
%
100
70-130
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 203 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
604448
604449
MS
MSD
9293679001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,1-Dichloroethene
ug/L
1.2
50
50
59.9
62.5
118
123
70-166
4
Benzene
ug/L
ND
50
50
58.0
63.3
116
127
70-148
9
Chlorobenzene
ug/L
ND
50
50
57.2
61.7
114
123
70-146
8
Toluene
ug/L
ND
50
50
57.5
63.0
115
126
70-155
9
Trichloroethene
ug/L
ND
50
50
57.0
62.1
113
124
69-151
9
1,2-Dichloroethane-d4 (S)
%
109
108
70-130
4-Bromofluorobenzene (S)
%
94
94
70-130
Dibromofluoromethane (S)
%
101
102
70-130
Toluene-d8(S)
%
99
101
70-130
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 204 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MSV/15203 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level
Associated Lab Samples: 9293679047, 9293679048, 9293679049, 9293679050
METHOD BLANK: 604510 Matrix: Water
Associated Lab Samples: 9293679047, 9293679048, 9293679049, 9293679050
Blank Reporting
Parameter Units Result Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
05/11/11 14:18
1,1,1-Trichloroethane
ug/L
ND
1.0
05/11/11 14:18
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
05/11/11 14:18
1,1,2-Trichloroethane
ug/L
ND
1.0
05/11/11 14:18
1,1-Dichloroethane
ug/L
ND
1.0
05/11/11 14:18
1,1-Dichloroethene
ug/L
ND
1.0
05/11/11 14:18
1,1-Dichloropropene
ug/L
ND
1.0
05/11/11 14:18
1,2,3-Trichlorobenzene
ug/L
ND
1.0
05/11/11 14:18
1,2,3-Trichloropropane
ug/L
ND
1.0
05/11/11 14:18
1,2,4-Trichlorobenzene
ug/L
ND
1.0
05/11/11 14:18
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
05/11/11 14:18
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
05/11/11 14:18
1,2-Dichlorobenzene
ug/L
ND
1.0
05/11/11 14:18
1,2-Dichloroethane
ug/L
ND
1.0
05/11/11 14:18
1,2-Dichloropropane
ug/L
ND
1.0
05/11/11 14:18
1,3-Dichlorobenzene
ug/L
ND
1.0
05/11/11 14:18
1,3-Dichloropropane
ug/L
ND
1.0
05/11/11 14:18
1,4-Dichlorobenzene
ug/L
ND
1.0
05/11/11 14:18
2,2-Dichloropropane
ug/L
ND
1.0
05/11/11 14:18
2-Butanone (MEK)
ug/L
ND
5.0
05/11/11 14:18
2-Chlorotoluene
ug/L
ND
1.0
05/11/11 14:18
2-Hexanone
ug/L
ND
5.0
05/11/11 14:18
4-Chlorotoluene
ug/L
ND
1.0
05/11/11 14:18
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
05/11/11 14:18
Acetone
ug/L
ND
25.0
05/11/11 14:18
Benzene
ug/L
ND
1.0
05/11/11 14:18
Bromobenzene
ug/L
ND
1.0
05/11/11 14:18
Bromochloromethane
ug/L
ND
1.0
05/11/11 14:18
Bromodichloromethane
ug/L
ND
1.0
05/11/11 14:18
Bromoform
ug/L
ND
1.0
05/11/11 14:18
Bromomethane
ug/L
ND
2.0
05/11/11 14:18
Carbon tetrachloride
ug/L
ND
1.0
05/11/11 14:18
Chlorobenzene
ug/L
ND
1.0
05/11/11 14:18
Chloroethane
ug/L
ND
1.0
05/11/11 14:18
Chloroform
ug/L
ND
1.0
05/11/11 14:18
Chloromethane
ug/L
ND
1.0
05/11/11 14:18
cis-1,2-Dichloroethene
ug/L
ND
1.0
05/11/11 14:18
cis-1,3-Dichloropropene
ug/L
ND
1.0
05/11/11 14:18
Dibromochloromethane
ug/L
ND
1.0
05/11/11 14:18
Dibromomethane
ug/L
ND
1.0
05/11/11 14:18
Dichlorodifluoromethane
ug/L
ND
1.0
05/11/11 14:18
Diisopropyl ether
ug/L
ND
1.0
05/11/11 14:18
Ethylbenzene
ug/L
ND
1.0
05/11/11 14:18
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY
ANALYSIS
This report shall not be
reproduced, except in full,
without the written consent
of Pace Analytical
Services, Inc..
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 205 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
METHOD BLANK: 604510
Associated Lab Samples:
Parameter
Matrix: Water
9293679047, 9293679048, 9293679049, 9293679050
Blank Reporting
Units Result Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
1.0
05/11/11 14:18
m&p-Xylene
ug/L
ND
2.0
05/11/11 14:18
Methyl-tert-butyl ether
ug/L
ND
1.0
05/11/11 14:18
Methylene Chloride
ug/L
ND
2.0
05/11/11 14:18
Naphthalene
ug/L
ND
1.0
05/11/11 14:18
o-Xylene
ug/L
ND
1.0
05/11/11 14:18
p-Isopropyltoluene
ug/L
ND
1.0
05/11/11 14:18
Styrene
ug/L
ND
1.0
05/11/11 14:18
Tetrachloroethene
ug/L
ND
1.0
05/11/11 14:18
Toluene
ug/L
ND
1.0
05/11/11 14:18
trans- 1,2-Dichloroethene
ug/L
ND
1.0
05/11/11 14:18
trans- 1,3-Dichloropropene
ug/L
ND
1.0
05/11/11 14:18
Trichloroethene
ug/L
ND
1.0
05/11/11 14:18
Trichlorofluoromethane
ug/L
ND
1.0
05/11/11 14:18
Vinyl acetate
ug/L
ND
2.0
05/11/11 14:18
Vinyl chloride
ug/L
ND
1.0
05/11/11 14:18
1,2-Dichloroethane-d4 (S)
%
108
70-130
05/11/11 14:18
4-Bromofluorobenzene (S)
%
96
70-130
05/11/11 14:18
Dibromofluoromethane (S)
%
94
70-130
05/11/11 14:18
Toluene-d8 (S)
%
99
70-130
05/11/11 14:18
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
604511
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
53.7
107
70-130
1,1,1-Trichloroethane
ug/L
50
50.8
102
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
52.8
106
70-130
1,1,2-Trichloroethane
ug/L
50
53.6
107
70-130
1,1-Dichloroethane
ug/L
50
54.8
110
70-130
1,1-Dichloroethene
ug/L
50
53.4
107
70-132
1,1-Dichloropropene
ug/L
50
48.7
97
70-130
1,2,3-Trichlorobenzene
ug/L
50
52.7
105
70-135
1,2,3-Trichloropropane
ug/L
50
51.3
103
70-130
1,2,4-Trichlorobenzene
ug/L
50
52.9
106
70-134
1,2-Dibromo-3-chloropropane
ug/L
50
54.2
108
70-130
1,2-Dibromoethane (EDB)
ug/L
50
54.8
110
70-130
1,2-Dichlorobenzene
ug/L
50
52.0
104
70-130
1,2-Dichloroethane
ug/L
50
55.8
112
70-130
1,2-Dichloropropane
ug/L
50
50.4
101
70-130
1,3-Dichlorobenzene
ug/L
50
51.8
104
70-130
1,3-Dichloropropane
ug/L
50
51.8
104
70-130
1,4-Dichlorobenzene
ug/L
50
51.6
103
70-130
2,2-Dichloropropane
ug/L
50
55.0
110
58-145
2-Butanone (MEK)
ug/L
100
104
104
70-145
2-Chlorotoluene
ug/L
50
51.3
103
70-130
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Qualifiers
[phone]
Page 206 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE:
Parameter
604511
Units
Spike
Conc.
LCS
Result
2-Hexanone
ug/L
100
111
4-Chlorotoluene
ug/L
50
53.0
4-Methyl-2-pentanone (MIBK)
ug/L
100
110
Acetone
ug/L
100
115
Benzene
ug/L
50
49.4
Bromobenzene
ug/L
50
52.1
Bromochloromethane
ug/L
50
52.3
Bromodichloromethane
ug/L
50
52.2
Bromoform
ug/L
50
44.3
Bromomethane
ug/L
50
55.1
Carbon tetrachloride
ug/L
50
48.9
Chlorobenzene
ug/L
50
51.3
Chloroethane
ug/L
50
49.0
Chloroform
ug/L
50
54.8
Chloromethane
ug/L
50
51.8
cis-1,2-Dichloroethene
ug/L
50
52.7
cis-1,3-Dichloropropene
ug/L
50
53.0
Dibromochloromethane
ug/L
50
49.9
Dibromomethane
ug/L
50
52.4
Dichlorodifluoromethane
ug/L
50
51.2
Diisopropyl ether
ug/L
50
55.8
Ethylbenzene
ug/L
50
52.7
Hexachloro-1,3-butadiene
ug/L
50
52.6
m&p-Xylene
ug/L
100
106
Methyl-tert-butyl ether
ug/L
50
54.0
Methylene Chloride
ug/L
50
57.3
Naphthalene
ug/L
50
52.3
o-Xylene
ug/L
50
53.2
p-Isopropyltoluene
ug/L
50
54.2
Styrene
ug/L
50
54.0
Tetrachloroethene
ug/L
50
53.8
Toluene
ug/L
50
51.1
trans- 1,2-Dichloroethene
ug/L
50
52.7
trans- 1,3-Dichloropropene
ug/L
50
51.2
Trichloroethene
ug/L
50
52.8
Trichlorofluoromethane
ug/L
50
53.7
Vinyl acetate
ug/L
100
109
Vinyl chloride
ug/L
50
51.5
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Dibromocuoromethane (S)
%
Toluene-d8 (S)
%
Date: 05/20/2011 04:57 PM
LCS
% Rec
% Rec
Limits
111 70-144
106 70-130
110 70-140
115 50-175
99 70-130
104 70-130
105 70-130
104 70-130
89 70-130
110 54-130
98 70-132
103 70-130
98 64-134
110 70-130
104 64-130
105 70-131
106 70-130
100 70-130
105 70-131
102 56-130
112 70-130
105 70-130
105 70-130
106 70-130
108 70-130
115 63-130
105 70-138
106 70-130
108 70-130
108 70-130
108 70-130
102 70-130
105 70-130
102 70-132
106 70-130
107 62-133
109 66-157
103 69-130
106 70-130
102 70-130
92 70-130
100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 207 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
604512
604513
MS
MSD
9293679049
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,1-Dichloroethene
ug/L
ND
50
50
58.0
57.3
116
115
70-166
1
Benzene
ug/L
ND
50
50
55.7
54.2
111
108
70-148
3
Chlorobenzene
ug/L
ND
50
50
55.4
53.2
111
106
70-146
4
Toluene
ug/L
ND
50
50
56.1
54.5
112
109
70-155
3
Trichloroethene
ug/L
ND
50
50
57.1
55.5
114
111
69-151
3
1,2-Dichloroethane-d4 (S)
%
116
119
70-130
4-Bromofluorobenzene (S)
%
99
97
70-130
Dibromofluoromethane (S)
%
105
107
70-130
Toluene-d8(S)
%
97
96
70-130
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 208 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MSV/15185 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV 5035A Volatile Organics
Associated Lab Samples: 9293679017, 9293679018, 9293679019, 9293679020, 9293679021, 9293679024, 9293679025
METHOD BLANK: 603839 Matrix: Solid
Associated Lab Samples: 9293679017, 9293679018, 9293679019, 9293679020, 9293679021, 9293679024, 9293679025
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.0
05/10/11 14:30
1,1,1-Trichloroethane
ug/kg
ND
5.0
05/10/11 14:30
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.0
05/10/11 14:30
1,1,2-Trichloroethane
ug/kg
ND
5.0
05/10/11 14:30
1,1-Dichloroethane
ug/kg
ND
5.0
05/10/11 14:30
1,1-Dichloroethene
ug/kg
ND
5.0
05/10/11 14:30
1,1-Dichloropropene
ug/kg
ND
5.0
05/10/11 14:30
1,2,3-Trichlorobenzene
ug/kg
ND
5.0
05/10/11 14:30
1,2,3-Trichloropropane
ug/kg
ND
5.0
05/10/11 14:30
1,2,4-Trichlorobenzene
ug/kg
ND
5.0
05/10/11 14:30
1,2,4-Trimethylbenzene
ug/kg
ND
5.0
05/10/11 14:30
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.0
05/10/11 14:30
1,2-Dibromoethane (EDB)
ug/kg
ND
5.0
05/10/11 14:30
1,2-Dichlorobenzene
ug/kg
ND
5.0
05/10/11 14:30
1,2-Dichloroethane
ug/kg
ND
5.0
05/10/11 14:30
1,2-Dichloropropane
ug/kg
ND
5.0
05/10/11 14:30
1,3,5-Trimethylbenzene
ug/kg
ND
5.0
05/10/11 14:30
1,3-Dichlorobenzene
ug/kg
ND
5.0
05/10/11 14:30
1,3-Dichloropropane
ug/kg
ND
5.0
05/10/11 14:30
1,4-Dichlorobenzene
ug/kg
ND
5.0
05/10/11 14:30
2,2-Dichloropropane
ug/kg
ND
5.0
05/10/11 14:30
2-Butanone (MEK)
ug/kg
ND
100
05/10/11 14:30
2-Chlorotoluene
ug/kg
ND
5.0
05/10/11 14:30
2-Hexanone
ug/kg
ND
50.0
05/10/11 14:30
4-Chlorotoluene
ug/kg
ND
5.0
05/10/11 14:30
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
50.0
05/10/11 14:30
Acetone
ug/kg
ND
100
05/10/11 14:30
Benzene
ug/kg
ND
5.0
05/10/11 14:30
Bromobenzene
ug/kg
ND
5.0
05/10/11 14:30
Bromochloromethane
ug/kg
ND
5.0
05/10/11 14:30
Bromodichloromethane
ug/kg
ND
5.0
05/10/11 14:30
Bromoform
ug/kg
ND
5.0
05/10/11 14:30
Bromomethane
ug/kg
ND
10.0
05/10/11 14:30
Carbon tetrachloride
ug/kg
ND
5.0
05/10/11 14:30
Chlorobenzene
ug/kg
ND
5.0
05/10/11 14:30
Chloroethane
ug/kg
ND
10.0
05/10/11 14:30
Chloroform
ug/kg
ND
5.0
05/10/11 14:30
Chloromethane
ug/kg
ND
10.0
05/10/11 14:30
cis-1,2-Dichloroethene
ug/kg
ND
5.0
05/10/11 14:30
cis-1,3-Dichloropropene
ug/kg
ND
5.0
05/10/11 14:30
Dibromochloromethane
ug/kg
ND
5.0
05/10/11 14:30
Dibromomethane
ug/kg
ND
5.0
05/10/11 14:30
Dichlorodifluoromethane
ug/kg
ND
10.0
05/10/11 14:30
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Analytical
Services, Inc..
PPace
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 209 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
METHOD BLANK: 603839 Matrix: Solid
Associated Lab Samples: 9293679017, 9293679018, 9293679019, 9293679020, 9293679021, 9293679024, 9293679025
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Diisopropyl ether
ug/kg
ND
5.0
05/10/11 14:30
Ethylbenzene
ug/kg
ND
5.0
05/10/11 14:30
Hexachloro-1,3-butadiene
ug/kg
ND
5.0
05/10/11 14:30
Isopropylbenzene (Cumene)
ug/kg
ND
5.0
05/10/11 14:30
m&p-Xylene
ug/kg
ND
10.0
05/10/11 14:30
Methyl-tert-butyl ether
ug/kg
ND
5.0
05/10/11 14:30
Methylene Chloride
ug/kg
ND
20.0
05/10/11 14:30
n-Butylbenzene
ug/kg
ND
5.0
05/10/11 14:30
n-Propylbenzene
ug/kg
ND
5.0
05/10/11 14:30
Naphthalene
ug/kg
ND
5.0
05/10/11 14:30
o-Xylene
ug/kg
ND
5.0
05/10/11 14:30
p-Isopropyltoluene
ug/kg
ND
5.0
05/10/11 14:30
sec -Butyl benzene
ug/kg
ND
5.0
05/10/11 14:30
Styrene
ug/kg
ND
5.0
05/10/11 14:30
tert-Butyl benzene
ug/kg
ND
5.0
05/10/11 14:30
Tetrachloroethene
ug/kg
ND
5.0
05/10/11 14:30
Toluene
ug/kg
ND
5.0
05/10/11 14:30
trans- 1,2-Dichloroethene
ug/kg
ND
5.0
05/10/11 14:30
trans- 1,3-Dichloropropene
ug/kg
ND
5.0
05/10/11 14:30
Trichloroethene
ug/kg
ND
5.0
05/10/11 14:30
Trichlorofluoromethane
ug/kg
ND
5.0
05/10/11 14:30
Vinyl acetate
ug/kg
ND
50.0
05/10/11 14:30
Vinyl chloride
ug/kg
ND
10.0
05/10/11 14:30
Xylene (Total)
ug/kg
ND
10.0
05/10/11 14:30
1,2-Dichloroethane-d4 (S)
%
92
70-132
05/10/11 14:30
4-Bromofluorobenzene (S)
%
102
70-130
05/10/11 14:30
Dibromofluoromethane (S)
%
96
70-130
05/10/11 14:30
Toluene-d8 (S)
%
104
70-130
05/10/11 14:30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
LABORATORY CONTROL SAMPLE:
Parameter
603840
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
50
56.3
113
70-131
1,1,1-Trichloroethane
ug/kg
50
53.2
106
70-141
1,1,2,2-Tetrachloroethane
ug/kg
50
53.3
107
70-130
1,1,2-Trichloroethane
ug/kg
50
55.9
112
70-132
1,1-Dichloroethane
ug/kg
50
54.5
109
70-143
1,1-Dichloroethene
ug/kg
50
53.0
106
70-137
1,1-Dichloropropene
ug/kg
50
49.2
98
70-135
1,2,3-Trichlorobenzene
ug/kg
50
52.9
106
69-153
1,2,3-Trichloropropane
ug/kg
50
47.9
96
70-130
1,2,4-Trichlorobenzene
ug/kg
50
53.8
108
55-171
1,2,4-Trimethylbenzene
ug/kg
50
50.5
101
70-149
1,2-Dibromo-3-chloropropane
ug/kg
50
44.2
88
68-141
1,2-Dibromoethane (EDB)
ug/kg
50
53.5
107
70-130
[phone]
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 210 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
603840
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2-Dichlorobenzene
ug/kg
50
52.7
105
70-140
1,2-Dichloroethane
ug/kg
50
48.6
97
70-137
1,2-Dichloropropane
ug/kg
50
53.5
107
70-133
1,3,5-Trimethylbenzene
ug/kg
50
50.9
102
70-143
1,3-Dichlorobenzene
ug/kg
50
54.4
109
70-144
1,3-Dichloropropane
ug/kg
50
51.5
103
70-132
1,4-Dichlorobenzene
ug/kg
50
52.2
104
70-142
2,2-Dichloropropane
ug/kg
50
55.2
110
68-152
2-Butanone (MEK)
ug/kg
100
92.7J
93
70-149
2-Chlorotoluene
ug/kg
50
51.0
102
70-141
2-Hexanone
ug/kg
100
102
102
70-149
4-Chlorotoluene
ug/kg
50
52.9
106
70-149
4-Methyl-2-pentanone (MIBK)
ug/kg
100
105
105
70-153
Acetone
ug/kg
100
84.5J
85
70-157
Benzene
ug/kg
50
53.7
107
70-130
Bromobenzene
ug/kg
50
49.7
99
70-141
Bromochloromethane
ug/kg
50
52.8
106
70-149
Bromodichloromethane
ug/kg
50
52.4
105
70-130
Bromoform
ug/kg
50
55.4
111
70-131
Bromomethane
ug/kg
50
79.1
158
64-136 L3
Carbon tetrachloride
ug/kg
50
52.8
106
70-154
Chlorobenzene
ug/kg
50
55.7
111
70-135
Chloroethane
ug/kg
50
59.5
119
68-151
Chloroform
ug/kg
50
54.5
109
70-130
Chloromethane
ug/kg
50
53.9
108
70-132
cis-1,2-Dichloroethene
ug/kg
50
49.6
99
70-140
cis-1,3-Dichloropropene
ug/kg
50
53.4
107
70-137
Dibromochloromethane
ug/kg
50
53.1
106
70-130
Dibromomethane
ug/kg
50
54.0
108
70-136
Dichlorodifluoromethane
ug/kg
50
45.0
90
36-148
Diisopropyl ether
ug/kg
50
49.3
99
70-139
Ethylbenzene
ug/kg
50
56.3
113
70-137
Hexachloro-1,3-butadiene
ug/kg
50
51.2
102
70-145
Isopropylbenzene (Cumene)
ug/kg
50
59.0
118
70-141
m&p-Xylene
ug/kg
100
110
110
70-140
Methyl-tert-butyl ether
ug/kg
50
47.6
95
45-150
Methylene Chloride
ug/kg
50
42.2
84
70-133
n-Butylbenzene
ug/kg
50
53.5
107
65-155
n-Propylbenzene
ug/kg
50
52.9
106
70-148
Naphthalene
ug/kg
50
47.9
96
70-148
o-Xylene
ug/kg
50
55.2
110
70-141
p-Isopropyltoluene
ug/kg
50
53.5
107
70-148
sec -Butyl benzene
ug/kg
50
53.1
106
70-145
Styrene
ug/kg
50
59.2
118
70-138
tert-Butyl benzene
ug/kg
50
52.5
105
70-143
Tetrachloroethene
ug/kg
50
59.4
119
70-140
Toluene
ug/kg
50
57.2
114
70-130
trans- 1,2-Dichloroethene
ug/kg
50
52.1
104
70-136
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 211 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
603840
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
trans- 1,3-Dichloropropene
ug/kg
50
51.7
103
70-138
Trichloroethene
ug/kg
50
57.8
116
70-132
Trichlorofluoromethane
ug/kg
50
53.1
106
69-134
Vinyl acetate
ug/kg
100
123
123
24-161
Vinyl chloride
ug/kg
50
53.2
106
55-140
Xylene (Total)
ug/kg
150
166
110
70-141
1,2-Dichloroethane-d4 (S)
%
91
70-132
4-Bromofluorobenzene (S)
%
103
70-130
Dibromofluoromethane (S)
%
99
70-130
Toluene-d8(S)
%
101
70-130
MATRIX SPIKE SAMPLE:
Parameter
604314
Units
9293679017
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1-Dichloroethene
ug/kg
ND
54.3
57.1
105
49-180
Benzene
ug/kg
ND
54.3
57.4
106
50-166
Chlorobenzene
ug/kg
ND
54.3
55.5
102
43-169
Toluene
ug/kg
ND
54.3
59.5
110
52-163
Trichloroethene
ug/kg
ND
54.3
56.7
103
49-167
1,2-Dichloroethane-d4 (S)
%
102
70-132
4-Bromofluorobenzene (S)
%
89
70-130
Dibromofluoromethane (S)
%
111
70-130
Toluene-d8 (S)
%
103
70-130
SAMPLE DUPLICATE: 604313
9293655003
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
ND
1,1,1-Trichloroethane
ug/kg
ND
ND
1,1,2,2-Tetrachloroethane
ug/kg
ND
ND
1,1,2-Trichloroethane
ug/kg
ND
ND
1,1-Dichloroethane
ug/kg
ND
ND
1,1-Dichloroethene
ug/kg
ND
ND
1,1-Dichloropropene
ug/kg
ND
ND
1,2,3-Trichlorobenzene
ug/kg
ND
ND
1,2,3-Trichloropropane
ug/kg
ND
ND
1,2,4-Trichlorobenzene
ug/kg
ND
ND
1,2,4-Trimethylbenzene
ug/kg
ND
ND
1,2-Dibromo-3-chloropropane
ug/kg
ND
ND
1,2-Dibromoethane (EDB)
ug/kg
ND
ND
1,2-Dichlorobenzene
ug/kg
ND
ND
1,2-Dichloroethane
ug/kg
ND
ND
1,2-Dichloropropane
ug/kg
ND
ND
1,3,5-Trimethylbenzene
ug/kg
ND
ND
1,3-Dichlorobenzene
ug/kg
ND
ND
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
Page 212 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
SAMPLE DUPLICATE: 604313
Parameter
Units
9293655003
Result
Dup
Result
1,3-Dichloropropane
ug/kg
ND
ND
1,4-Dichlorobenzene
ug/kg
ND
ND
2,2-Dichloropropane
ug/kg
ND
ND
2-Butanone (MEK)
ug/kg
ND
ND
2-Chlorotoluene
ug/kg
ND
ND
2-Hexanone
ug/kg
ND
ND
4-Chlorotoluene
ug/kg
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
ND
Acetone
ug/kg
ND
40.5J
Benzene
ug/kg
ND
ND
Bromobenzene
ug/kg
ND
ND
Bromochloromethane
ug/kg
ND
ND
Bromodichloromethane
ug/kg
ND
ND
Bromoform
ug/kg
ND
ND
Bromomethane
ug/kg
ND
ND
Carbon tetrachloride
ug/kg
ND
ND
Chlorobenzene
ug/kg
ND
ND
Chloroethane
ug/kg
ND
ND
Chloroform
ug/kg
ND
ND
Chloromethane
ug/kg
ND
ND
cis-1,2-Dichloroethene
ug/kg
ND
ND
cis-1,3-Dichloropropene
ug/kg
ND
ND
Dibromochloromethane
ug/kg
ND
ND
Dibromomethane
ug/kg
ND
ND
Dichlorodifluoromethane
ug/kg
ND
ND
Diisopropyl ether
ug/kg
ND
ND
Ethylbenzene
ug/kg
ND
ND
Hexachloro-1,3-butadiene
ug/kg
ND
ND
Isopropylbenzene (Cumene)
ug/kg
ND
ND
m&p-Xylene
ug/kg
ND
ND
Methyl-tert-butyl ether
ug/kg
ND
ND
Methylene Chloride
ug/kg
ND
ND
n-Butylbenzene
ug/kg
ND
ND
n-Propylbenzene
ug/kg
ND
ND
Naphthalene
ug/kg
ND
ND
o-Xylene
ug/kg
ND
ND
p-Isopropyltoluene
ug/kg
ND
ND
sec -Butyl benzene
ug/kg
ND
ND
Styrene
ug/kg
ND
ND
tert-Butyl benzene
ug/kg
ND
ND
Tetrachloroethene
ug/kg
ND
ND
Toluene
ug/kg
ND
ND
trans- 1,2-Dichloroethene
ug/kg
ND
ND
trans- 1,3-Dichloropropene
ug/kg
ND
ND
Trichloroethene
ug/kg
ND
ND
Trichlorofluoromethane
ug/kg
ND
ND
Vinyl acetate
ug/kg
ND
ND
Vinyl chloride
ug/kg
ND
ND
Date: 05/20/2011 04:57 PM
RPD Qualifiers
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 213 of 227

®
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
acmnalytical
205 East Meadow Road - Suite A
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
www.paceJabs.com
Eden, NC 27288
Asheville, NC 28804
Huntersville, NC 28078
[phone]
[phone]
[phone]
QUALITY CONTROL DATA
Project: Swannanoa
Pace Project No.: 9293679
SAMPLE DUPLICATE: 604313
9293655003
Dup
Parameter
Units Result
Result
RPD Qualifiers
Xylene (Total)
ug/kg
ND
ND
1,2-Dichloroethane-d4 (S)
%
99
110
8
4-Bromofluorobenzene (S)
%
98
91
8
Dibromofluoromethane (S)
%
107
114
5
Toluene-d8(S)
%
99
100
0
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 214 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: MSV/15201 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV 5035A Volatile Organics
Associated Lab Samples: 9293679026, 9293679027, 9293679028, 9293679029, 9293679030, 9293679033, 9293679034, 9293679035,
9293679036,9293679037,9293679039
METHOD BLANK: 604485 Matrix: Solid
Associated Lab Samples: 9293679026, 9293679027, 9293679028, 9293679029, 9293679030, 9293679033, 9293679034, 9293679035,
9293679036,9293679037,9293679039
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.0
05/11/11 13:59
1,1,1-Trichloroethane
ug/kg
ND
5.0
05/11/11 13:59
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.0
05/11/11 13:59
1,1,2-Trichloroethane
ug/kg
ND
5.0
05/11/11 13:59
1,1-Dichloroethane
ug/kg
ND
5.0
05/11/11 13:59
1,1-Dichloroethene
ug/kg
ND
5.0
05/11/11 13:59
1,1-Dichloropropene
ug/kg
ND
5.0
05/11/11 13:59
1,2,3-Trichlorobenzene
ug/kg
ND
5.0
05/11/11 13:59
1,2,3-Trichloropropane
ug/kg
ND
5.0
05/11/11 13:59
1,2,4-Trichlorobenzene
ug/kg
ND
5.0
05/11/11 13:59
1,2,4-Trimethylbenzene
ug/kg
ND
5.0
05/11/11 13:59
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.0
05/11/11 13:59
1,2-Dibromoethane (EDB)
ug/kg
ND
5.0
05/11/11 13:59
1,2-Dichlorobenzene
ug/kg
ND
5.0
05/11/11 13:59
1,2-Dichloroethane
ug/kg
ND
5.0
05/11/11 13:59
1,2-Dichloropropane
ug/kg
ND
5.0
05/11/11 13:59
1,3,5-Trimethylbenzene
ug/kg
ND
5.0
05/11/11 13:59
1,3-Dichlorobenzene
ug/kg
ND
5.0
05/11/11 13:59
1,3-Dichloropropane
ug/kg
ND
5.0
05/11/11 13:59
1,4-Dichlorobenzene
ug/kg
ND
5.0
05/11/11 13:59
2,2-Dichloropropane
ug/kg
ND
5.0
05/11/11 13:59
2-Butanone (MEK)
ug/kg
ND
100
05/11/11 13:59
2-Chlorotoluene
ug/kg
ND
5.0
05/11/11 13:59
2-Hexanone
ug/kg
ND
50.0
05/11/11 13:59
4-Chlorotoluene
ug/kg
ND
5.0
05/11/11 13:59
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
50.0
05/11/11 13:59
Acetone
ug/kg
ND
100
05/11/11 13:59
Benzene
ug/kg
ND
5.0
05/11/11 13:59
Bromobenzene
ug/kg
ND
5.0
05/11/11 13:59
Bromochloromethane
ug/kg
ND
5.0
05/11/11 13:59
Bromodichloromethane
ug/kg
ND
5.0
05/11/11 13:59
Bromoform
ug/kg
ND
5.0
05/11/11 13:59
Bromomethane
ug/kg
ND
10.0
05/11/11 13:59
Carbon tetrachloride
ug/kg
ND
5.0
05/11/11 13:59
Chlorobenzene
ug/kg
ND
5.0
05/11/11 13:59
Chloroethane
ug/kg
ND
10.0
05/11/11 13:59
Chloroform
ug/kg
ND
5.0
05/11/11 13:59
Chloromethane
ug/kg
ND
10.0
05/11/11 13:59
cis-1,2-Dichloroethene
ug/kg
ND
5.0
05/11/11 13:59
cis-1,3-Dichloropropene
ug/kg
ND
5.0
05/11/11 13:59
Dibromochloromethane
ug/kg
ND
5.0
05/11/11 13:59
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 215 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
METHOD BLANK: 604485 Matrix: Solid
Associated Lab Samples: 9293679026,9293679027,9293679028,9293679029,9293679030,9293679033,9293679034,9293679035,
9293679036,9293679037,9293679039
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Dibromomethane
ug/kg
ND
5.0
05/11/11 13:59
Dichlorodifluoromethane
ug/kg
ND
10.0
05/11/11 13:59
Diisopropyl ether
ug/kg
ND
5.0
05/11/11 13:59
Ethylbenzene
ug/kg
ND
5.0
05/11/11 13:59
Hexachloro-1,3-butadiene
ug/kg
ND
5.0
05/11/11 13:59
Isopropylbenzene (Cumene)
ug/kg
ND
5.0
05/11/11 13:59
m&p-Xylene
ug/kg
ND
10.0
05/11/11 13:59
Methyl-tert-butyl ether
ug/kg
ND
5.0
05/11/11 13:59
Methylene Chloride
ug/kg
ND
20.0
05/11/11 13:59
n-Butylbenzene
ug/kg
ND
5.0
05/11/11 13:59
n-Propylbenzene
ug/kg
ND
5.0
05/11/11 13:59
Naphthalene
ug/kg
ND
5.0
05/11/11 13:59
o-Xylene
ug/kg
ND
5.0
05/11/11 13:59
p-Isopropyltoluene
ug/kg
ND
5.0
05/11/11 13:59
sec -Butyl benzene
ug/kg
ND
5.0
05/11/11 13:59
Styrene
ug/kg
ND
5.0
05/11/11 13:59
tert-Butyl benzene
ug/kg
ND
5.0
05/11/11 13:59
Tetrachloroethene
ug/kg
ND
5.0
05/11/11 13:59
Toluene
ug/kg
ND
5.0
05/11/11 13:59
trans- 1,2-Dichloroethene
ug/kg
ND
5.0
05/11/11 13:59
trans- 1,3-Dichloropropene
ug/kg
ND
5.0
05/11/11 13:59
Trichloroethene
ug/kg
ND
5.0
05/11/11 13:59
Trichlorofluoromethane
ug/kg
ND
5.0
05/11/11 13:59
Vinyl acetate
ug/kg
ND
50.0
05/11/11 13:59
Vinyl chloride
ug/kg
ND
10.0
05/11/11 13:59
Xylene (Total)
ug/kg
ND
10.0
05/11/11 13:59
1,2-Dichloroethane-d4 (S)
%
107
70-132
05/11/11 13:59
4-Bromofluorobenzene (S)
%
94
70-130
05/11/11 13:59
Dibromofluoromethane (S)
%
112
70-130
05/11/11 13:59
Toluene-d8 (S)
%
103
70-130
05/11/11 13:59
LABORATORY CONTROL SAMPLE:
Parameter
604486
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
50
45.8
92
70-131
1,1,1-Trichloroethane
ug/kg
50
48.5
97
70-141
1,1,2,2-Tetrachloroethane
ug/kg
50
47.4
95
70-130
1,1,2-Trichloroethane
ug/kg
50
47.9
96
70-132
1,1-Dichloroethane
ug/kg
50
47.8
96
70-143
1,1-Dichloroethene
ug/kg
50
44.5
89
70-137
1,1-Dichloropropene
ug/kg
50
41.6
83
70-135
1,2,3-Trichlorobenzene
ug/kg
50
47.4
95
69-153
1,2,3-Trichloropropane
ug/kg
50
45.8
92
70-130
1,2,4-Trichlorobenzene
ug/kg
50
46.0
92
55-171
[phone]
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 216 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE:
Parameter
604486
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trimethylbenzene
ug/kg
50
47.1
94
70-149
1,2-Dibromo-3-chloropropane
ug/kg
50
47.1
94
68-141
1,2-Dibromoethane (EDB)
ug/kg
50
47.2
94
70-130
1,2-Dichlorobenzene
ug/kg
50
46.4
93
70-140
1,2-Dichloroethane
ug/kg
50
46.8
94
70-137
1,2-Dichloropropane
ug/kg
50
46.7
93
70-133
1,3,5-Trimethylbenzene
ug/kg
50
47.0
94
70-143
1,3-Dichlorobenzene
ug/kg
50
44.7
89
70-144
1,3-Dichloropropane
ug/kg
50
46.0
92
70-132
1,4-Dichlorobenzene
ug/kg
50
45.8
92
70-142
2,2-Dichloropropane
ug/kg
50
45.9
92
68-152
2-Butanone (MEK)
ug/kg
100
90.2J
90
70-149
2-Chlorotoluene
ug/kg
50
46.6
93
70-141
2-Hexanone
ug/kg
100
91.8
92
70-149
4-Chlorotoluene
ug/kg
50
48.3
97
70-149
4-Methyl-2-pentanone (MIBK)
ug/kg
100
94.3
94
70-153
Acetone
ug/kg
100
103
103
70-157
Benzene
ug/kg
50
44.7
89
70-130
Bromobenzene
ug/kg
50
48.4
97
70-141
Bromochloromethane
ug/kg
50
46.0
92
70-149
Bromodichloromethane
ug/kg
50
47.2
94
70-130
Bromoform
ug/kg
50
47.5
95
70-131
Bromomethane
ug/kg
50
42.9
86
64-136
Carbon tetrachloride
ug/kg
50
44.8
90
70-154
Chlorobenzene
ug/kg
50
43.8
88
70-135
Chloroethane
ug/kg
50
57.9
116
68-151
Chloroform
ug/kg
50
47.5
95
70-130
Chloromethane
ug/kg
50
54.0
108
70-132
cis-1,2-Dichloroethene
ug/kg
50
47.1
94
70-140
cis-1,3-Dichloropropene
ug/kg
50
48.1
96
70-137
Dibromochloromethane
ug/kg
50
46.8
94
70-130
Dibromomethane
ug/kg
50
45.8
92
70-136
Dichlorodifluoromethane
ug/kg
50
50.3
101
36-148
Diisopropyl ether
ug/kg
50
48.0
96
70-139
Ethylbenzene
ug/kg
50
44.9
90
70-137
Hexachloro-1,3-butadiene
ug/kg
50
41.9
84
70-145
Isopropylbenzene (Cumene)
ug/kg
50
47.7
95
70-141
m&p-Xylene
ug/kg
100
88.8
89
70-140
Methyl-tert-butyl ether
ug/kg
50
48.6
97
45-150
Methylene Chloride
ug/kg
50
43.3
87
70-133
n-Butylbenzene
ug/kg
50
46.7
93
65-155
n-Propylbenzene
ug/kg
50
46.6
93
70-148
Naphthalene
ug/kg
50
48.1
96
70-148
o-Xylene
ug/kg
50
47.3
95
70-141
p-Isopropyltoluene
ug/kg
50
47.2
94
70-148
sec -Butyl benzene
ug/kg
50
46.2
92
70-145
Styrene
ug/kg
50
47.1
94
70-138
tert-Butyl benzene
ug/kg
50
48.1
96
70-143
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 217 of 227

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
604486
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Tetrachloroethene
ug/kg
50
44.5
89
70-140
Toluene
ug/kg
50
46.2
92
70-130
trans- 1,2-Dichloroethene
ug/kg
50
45.4
91
70-136
trans- 1,3-Dichloropropene
ug/kg
50
47.8
96
70-138
Trichloroethene
ug/kg
50
44.8
90
70-132
Trichlorofluoromethane
ug/kg
50
53.4
107
69-134
Vinyl acetate
ug/kg
100
78.7
79
24-161
Vinyl chloride
ug/kg
50
54.6
109
55-140
Xylene (Total)
ug/kg
150
136
91
70-141
1,2-Dichloroethane-d4 (S)
%
98
70-132
4-Bromofluorobenzene (S)
%
96
70-130
Dibromofluoromethane (S)
%
102
70-130
Toluene-d8(S)
%
103
70-130
MATRIX SPIKE SAMPLE:
Parameter
604855
Units
9293679029
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1-Dichloroethene
ug/kg
ND
42
37.5
89
49-180
Benzene
ug/kg
ND
42
38.8
92
50-166
Chlorobenzene
ug/kg
ND
42
40.7
97
43-169
Toluene
ug/kg
ND
42
40.2
96
52-163
Trichloroethene
ug/kg
ND
42
38.5
92
49-167
1,2-Dichloroethane-d4 (S)
%
107
70-132
4-Bromofluorobenzene (S)
%
88
70-130
Dibromofluoromethane (S)
%
103
70-130
Toluene-d8 (S)
%
97
70-130
SAMPLE DUPLICATE: 604856
9293679033
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
ND
1,1,1-Trichloroethane
ug/kg
ND
ND
1,1,2,2-Tetrachloroethane
ug/kg
ND
ND
1,1,2-Trichloroethane
ug/kg
ND
ND
1,1-Dichloroethane
ug/kg
ND
ND
1,1-Dichloroethene
ug/kg
ND
ND
1,1-Dichloropropene
ug/kg
ND
ND
1,2,3-Trichlorobenzene
ug/kg
ND
ND
1,2,3-Trichloropropane
ug/kg
ND
ND
1,2,4-Trichlorobenzene
ug/kg
ND
ND
1,2,4-Trimethylbenzene
ug/kg
ND
ND
1,2-Dibromo-3-chloropropane
ug/kg
ND
ND
1,2-Dibromoethane (EDB)
ug/kg
ND
ND
1,2-Dichlorobenzene
ug/kg
ND
ND
1,2-Dichloroethane
ug/kg
ND
ND
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
Page 218 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc

acmnalytical
www.paceJabs.com
Project: Swannanoa
Pace Project No.: 9293679
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
SAMPLE DUPLICATE: 604856
Parameter
Units
9293679033
Result
Dup
Result
1,2-Dichloropropane
ug/kg
ND
ND
1,3,5-Trimethylbenzene
ug/kg
ND
ND
1,3-Dichlorobenzene
ug/kg
ND
ND
1,3-Dichloropropane
ug/kg
ND
ND
1,4-Dichlorobenzene
ug/kg
ND
ND
2,2-Dichloropropane
ug/kg
ND
ND
2-Butanone (MEK)
ug/kg
ND
ND
2-Chlorotoluene
ug/kg
ND
ND
2-Hexanone
ug/kg
ND
ND
4-Chlorotoluene
ug/kg
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
ND
Acetone
ug/kg
ND
ND
Benzene
ug/kg
ND
ND
Bromobenzene
ug/kg
ND
ND
Bromochloromethane
ug/kg
ND
ND
Bromodichloromethane
ug/kg
ND
ND
Bromoform
ug/kg
ND
ND
Bromomethane
ug/kg
ND
ND
Carbon tetrachloride
ug/kg
ND
ND
Chlorobenzene
ug/kg
ND
ND
Chloroethane
ug/kg
ND
ND
Chloroform
ug/kg
ND
ND
Chloromethane
ug/kg
ND
ND
cis-1,2-Dichloroethene
ug/kg
ND
ND
cis-1,3-Dichloropropene
ug/kg
ND
ND
Dibromochloromethane
ug/kg
ND
ND
Dibromomethane
ug/kg
ND
ND
Dichlorodifluoromethane
ug/kg
ND
ND
Diisopropyl ether
ug/kg
ND
ND
Ethylbenzene
ug/kg
ND
ND
Hexachloro-1,3-butadiene
ug/kg
ND
ND
Isopropylbenzene (Cumene)
ug/kg
ND
ND
m&p-Xylene
ug/kg
ND
ND
Methyl-tert-butyl ether
ug/kg
ND
ND
Methylene Chloride
ug/kg
ND
ND
n-Butylbenzene
ug/kg
ND
ND
n-Propylbenzene
ug/kg
ND
ND
Naphthalene
ug/kg
ND
ND
o-Xylene
ug/kg
ND
ND
p-Isopropyltoluene
ug/kg
ND
ND
sec -Butyl benzene
ug/kg
ND
ND
Styrene
ug/kg
ND
ND
tert-Butyl benzene
ug/kg
ND
ND
Tetrachloroethene
ug/kg
ND
ND
Toluene
ug/kg
ND
ND
trans- 1,2-Dichloroethene
ug/kg
ND
ND
trans- 1,3-Dichloropropene
ug/kg
ND
ND
Trichloroethene
ug/kg
ND
ND
RPD Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 219 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

®
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
acmnalytical
205 East Meadow Road - Suite A
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
www.paceJabs.com
Eden, NC 27288
Asheville, NC 28804
Huntersville, NC 28078
[phone]
[phone]
[phone]
QUALITY CONTROL DATA
Project: Swannanoa
Pace Project No.: 9293679
SAMPLE DUPLICATE: 604856
9293679033
Dup
Parameter
Units Result
Result
RPD Qualifiers
Trichlorofluoromethane
ug/kg
ND
ND
Vinyl acetate
ug/kg
ND
ND
Vinyl chloride
ug/kg
ND
ND
Xylene (Total)
ug/kg
ND
ND
1,2-Dichloroethane-d4 (S)
%
96
106
13
4-Bromofluorobenzene (S)
%
94
91
0
Dibromofluoromethane (S)
%
106
110
6
Toluene-d8(S)
%
100
98
1
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 220 of 227

®
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
acmnalytical
205 East Meadow Road - Suite A
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
www.paceJabs.com
Eden, NC 27288
Asheville, NC 28804
Huntersville, NC 28078
[phone]
[phone]
[phone]
QUALITY CONTROL DATA
Project: Swannanoa
Pace Project No.: 9293679
QC Batch: PMST/3915
Analysis Method:
ASTM D2974-87
QC Batch Method: ASTM D2974-87
Analysis Description:
Dry Weight/Percent Moisture
Associated Lab Samples: 9293679017, 9293679018, 9293679019, 9293679039
SAMPLE DUPLICATE: 604086
9293557001 Dup
Parameter
Units Result Result
RPD Qualifiers
Percent Moisture %
9.3
8.4 10
SAMPLE DUPLICATE: 604087
9293710001 Dup
Parameter
Units Result Result
RPD Qualifiers
Percent Moisture %
14.2
14.5 2
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 221 of 227

®
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
acmnalytical
205 East Meadow Road - Suite A 2225 Riverside Dr.
9800 Kincey Ave. Suite 100
www.paceJabs.com
Eden, NC 27288 Asheville, NC 28804
Huntersville, NC 28078
[phone] [phone]
[phone]
QUALITY CONTROL DATA
Project: Swannanoa
Pace Project No.: 9293679
QC Batch: PMST/3917
Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 9293679020, 9293679021, 9293679024, 9293679025
SAMPLE DUPLICATE: 604331
9293626004 Dup
Parameter
Units Result Result RPD Qualifiers
Percent Moisture %
20.8 21.0 1
SAMPLE DUPLICATE: 604332
9293851004 Dup
Parameter
Units Result Result RPD Qualifiers
Percent Moisture %
10.2 11.2 9
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 222 of 227

®
Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
acmnalytical
205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.paceJabs.com
Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
QUALITY CONTROL DATA
Project: Swannanoa
Pace Project No.: 9293679
QC Batch: PMST/3918
Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 9293679026, 9293679027, 9293679028, 9293679029, 9293679030, 9293679033, 9293679034, 9293679035,
9293679036,9293679037
SAMPLE DUPLICATE: 604358
9293302001 Dup
Parameter
Units Result Result RPD Qualifiers
Percent Moisture %
50.2 51.4 2
SAMPLE DUPLICATE: 604359
9293844010 Dup
Parameter
Units Result Result RPD Qualifiers
Percent Moisture %
7.7 8.6 11
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 223 of 227

®
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
acmnalytical
205 East Meadow Road - Suite A 2225 Riverside Dr.
9800 Kincey Ave. Suite 100
www.paceJabs.com
Eden, NC 27288 Asheville, NC 28804
Huntersville, NC 28078
[phone] [phone]
[phone]
QUALITY CONTROL DATA
Project: Swannanoa
Pace Project No.: 9293679
QC Batch: PMST/3919
Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 9293679023, 9293679031, 9293679032, 9293679040, 9293679041
SAMPLE DUPLICATE: 604363
9293306001 Dup
Parameter
Units Result Result RPD Qualifiers
Percent Moisture %
15.9 15.8 0
SAMPLE DUPLICATE: 604364
9293679041 Dup
Parameter
Units Result Result RPD Qualifiers
Percent Moisture %
11.0 11.2 1
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 224 of 227

®
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
acmnalytical
205 East Meadow Road - Suite A 2225 Riverside Dr.
9800 Kincey Ave. Suite 100
www.paceJabs.com
Eden, NC 27288 Asheville, NC 28804
Huntersville, NC 28078
[phone] [phone]
[phone]
QUALITY CONTROL DATA
Project: Swannanoa
Pace Project No.: 9293679
QC Batch: PMST/3923
Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 9293679042, 9293679043, 9293679044, 9293679045
SAMPLE DUPLICATE: 605473
9294020001 Dup
Parameter
Units Result Result RPD Qualifiers
Percent Moisture %
12.6 12.5 1
SAMPLE DUPLICATE: 605517
9294023013 Dup
Parameter
Units Result Result RPD Qualifiers
Percent Moisture %
13.9 13.2 5
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..
Page 225 of 227

®
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
acmnalytical
205 East Meadow Road - Suite A 2225 Riverside Dr.
9800 Kincey Ave. Suite 100
www.paceJabs.com
Eden, NC 27288 Asheville, NC 28804
Huntersville, NC 28078
[phone] [phone]
[phone]
QUALITY CONTROL DATA
Project: Swannanoa
Pace Project No.: 9293679
QC Batch: PMST/3934
Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 9293679046
SAMPLE DUPLICATE: 607684
9293679046 Dup
Parameter
Units Result Result RPD Qualifiers
Percent Moisture %
20.1 20.0 0
SAMPLE DUPLICATE: 607685
9294245002 Dup
Parameter
Units Result Result RPD Qualifiers
Percent Moisture %
38.0 38.1 0
Date: 05/20/2011 04:57 PM
REPORT OF LABORATORY ANALYSIS
Page 226 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc

acmnalytical
www.paceJabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Project: Swannanoa
Pace Project No.: 9293679
DEFINITIONS
[phone]
QUALIFIERS
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
CO Result confirmed by second analysis.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
L3 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC accreditation for this parameter.
R1 RPD value was outside control limits.
SO Surrogate recovery outside laboratory control limits.
S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
[phone]
Date: 05/20/2011 04:57 PM REPORT OF LABORATORY ANALYSIS Page 227 of 227
This report shall not be reproduced, except in full,
without the written consent of PPace Analytical Services, Inc..

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TABLE 5
GROUNDWATER SAMPLE ANALYTICAL RESULTS SUMMARY (VOC and SVOC COMPOUNDS)
FORMER BEACON MANUFACTURING FACILITY
SWANNANOA, NORTH CAROLINA
J
m
W
\
L
pq
?
O
L
r
W
O
W
C
O
=
O
G
O
L
.2
SAMPLE POINT
Well
Depth
(feet)
Depth to
Water
(feet)
DATE
SAMPLED
Analysis
o
o
z
m
C
�,
X
r
5+
o
z
.
c
0
m
F�
o
O
z
c
N�
V
a
MW-8
17.5
9.70
5/5/2011
8260, metals
<1.0
<1.0
<3.0
<3.0
1.5
<1.0
<1.0
<1.0
<1.0
NS
DUP-1 (MW-8)
5/5/2011
8260, metals
<1.0
<1.0
<3.0
<3.0
1.5
<1.0
<1.0
<1.0
<1.0
NS
MW-9
20.3
16.21
5/5/2011
8260, metals
<1.0
<1.0
<3.0
<3.0
4.8
<1.0
<1.0
1.4
<1.0
NS
MW-30
20.6
15.16
5/5/2011
8260, metals
<1.0
<1.0
<3.0
<3.0
1.2
5.3
<1.0
<1.0
<1.0
NS
MW-13
20
12.25
5/6/2011
8260, 8270, metals, VPH
<1.0
<1.0
<3.0
<3.0
<1.0
<1.0
<1.0
<1.0
<1.0
NS
MW-14
18
9.73
5/6/2011
8260
<1.0
<1.0
<3.0
<3.0
<1.0
<1.0
<1.0
<1.0
<1.0
NS
MW-15
20
4.68
5/6/2011
8260, 8270, VPH
<1.0
<1.0
<3.0
<3.0
<1.0
<1.0
<1.0
<1.0
<1.0
NS
MW-16
20
4.99
5/6/2011
8260, 8270, metals
<1.0
<1.0
<3.0
2.4
3.6
3.2
<1.0
20.0
1.7
NS
MW-17
20
3.80
5/6/2011
8260, 8270, metals
<1.0
<1.0
<3.0
<1.0
<3.0
35.2
<3.0
<1.0
<3.0
NS
MW-18
20
7.65
5/6/2011
8260, 8270, metals
<1.0
<1.0
<3.0
1.0
<1.0
7.5
<1.0
<1.0
<1.0
NS
MW-20
20
6.00
5/6/2011
8260, 8270, metals
<1.0
<1.0
<3.0
2.3
12.9
<1.0
80.8
2.3
<1.0
NS
MW-21
20
4.64
5/6/2011
8260, 8270, metals
<1.0
<1.0
<3.0
2.6
<1.0
77.8
<1.0
20.2
22.0
NS
MW-22
20
4.80
5/6/2011
8260, 8270, metals
<3.0
<3.0
<3.0
<3.0
<1.0
<3.0
<1.0
<1.0
<1.0
NS
MW-24
20
7.23
5/6/2011
8260, 8270, metals
<1.0
<1.0
<3.0
<1.0
<3.0
<3.0
<3.0
<3.0
<3.0
NS
MW-25
16
6.80
5/6/2011
8260, 8270, metals
<1.0
1.2
<3.0
<3.0
<3.0
<3.0
<1.0
<1.0
<1.0
NS
DUP-2 (MW-25)
5/6/2011
8260, 8270, metals
1.9
<1.0
<3.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NS
SW-4
Downstream
5/6/2011
8260, 8270, metals
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
NS
SW-5
At facility
5/6/2011
8260, 8270, metals
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
NS
SW-6
5/6/2011
8260, 8270, metals
<1.0
<1.0
<3.0
<3.0
<1.0
<1.0
<1.0
<1.0
<1.0
NS
Area 3 pond
Upstream
SW-7
5/6/2011
8260, 8270, metals
<1.0
<1.0
<3.0
<3.0
<1.0
<1.0
<1.0
<1.0
<1.0
NS
MW-1
33.8
Unknown
5/29/1994
Unknown
8.4
ND
ND
3.2
11
2
54
10
ND
110
11.84
4/20/2004
Unknown
ND
ND
ND
ND
6.0
ND
38
ND
NS
NS
11/1/2004
Unknown
0.66
ND
NS
3.6
14
3.2
65
4.8
NS
NS
MW-2
17.22
Unknown
5/29/1994
Unknown
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Unknown
4/18/1995
Unknown
ND
ND
ND
ND
ND
ND
ND
ND
ND
220
Unknown
12/19/2000
8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
NS
7.4
4/20/2004
Unknown
NS
ND
ND
NS
NS
NS
NS
NS
NS
NS
MW-3
25.9
Unknown
5/29/1994
Unknown
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Unknown
4/18/1995
Unknown
ND
ND
ND
ND
ND
ND
ND
ND
ND
340
Unknown
12/19/2000
8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
NS
19.95
4/20/2004
Unknown
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Unknown
11/1/2004
Unknown
0.86
ND
0.29
NS
NS
NS
NS
NS
NS
NS
MW-4
15.9
Unknown
5/29/1994
Unknown
ND
ND
ND
ND
27
ND
190
ND
ND
NS
Unknown
4/18/1995
Unknown
ND
ND
ND
ND
ND
ND
ND
ND
ND
180
Unknown
12/19/2000
8260
ND
ND
ND
1.4
8.5
2
37
6.3
ND
NS
Unknown
7/3/2001
8260
3.2
ND
ND
ND
2.9
ND
25
3.6
ND
NS
12
4/20/2004
Unknown
ND
ND
ND
ND
ND
ND
32
ND
NS
NS
Unknown
11/1/2004
Unknown
0.42
ND
ND
2.2
9.6
1.8
38
3.1
NS
NS
MW-4A
Unknown
Unknown
12/19/2000
8260
ND
ND
NS
2.6
8.2
5.8
43
8.3
0.58
NS
MW-5
19.5
Unknown
5/29/1994
Unknown
NS
NS
NS
NS
NS
NS
NS
NS
NS
69
Unknown
12/19/2000
8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
NS
11.16
4/20/2004
Unknown
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-6
10.8
Unknown
5/29/1994
Unknown
1.8
ND
ND
ND
ND
ND
ND
ND
ND
NS
Unknown
12/19/2000
8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
NS
3.12
4/20/2004
Unknown
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Unknown
11/1/2004
Unknown
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-7
Unknown
Unknown
4/1/2004
Unknown
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Unknown
11/1/2004
Unknown
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
SW-1
Upstream
7/3/2001
8260
5.4
ND
ND
ND
ND
ND
ND
ND
ND
NS
SW-2
7/3/2001
8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
NS
At facility
SW-3
Downstream
7/3/2001
8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
NS
Guidance Residential Use
7.3
3900
95
65
38
5.7
1500
30
NR
Commercial/Industrial Use
35
16000
420
330
160
29
6300
150
NRNC
Tnce
2L Standard (January 2010) or IMAC (June 2011)
70
600
500
70
7
0.7
200
2.8
70
Notes: ND=Not Detected NR=Not Regulated
NS=Not Sampled Bold indicates a result greater than the detection limit.
IHSB = Inactive Hazardous Sites Branch
IMAC= Interim Maximum Allowable Concentration
Yellow shading indicates an exceedance of a groundwater standard
Rose indicates an exceedance of the IHSB VI Guidance concentration
VI =Vapor Intrusion
ug/L= micrograms per Liter