MO-29889_48982_CA_IAR_20231011

hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS
Via Email
October 11, 2023
NC DEQ Division of Waste Management
UST Section
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Attention: Ms. Trudy Beverly
RE: IAA Report
Former Church Property
3201 Tuckeseegee Road
Charlotte, NC
H&H Job No. TPM.001
Dear Trudy,
On behalf of TPM Properties Limited Partnership, Hart & Hickman is submitting the
attached Initial Abetment Action (IAA) Report for the above referenced property (Incident
No. 48982) located in Charlotte, Mecklenburg County, North Carolina.
If you have any questions or comments, please do not hesitate to contact me.
Sincerely,
Hart & Hickman, PC
Stephen R. Libbey, P.G.
Project Manager
Enclosures
cc: TPM Properties Limited Partnership (via email)
2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301
Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com
704.586.0007 main 919.847.4241 main

Initial Abatement Action Report
Former Church Property
3201 Tuckaseegee Road
Charlotte, North Carolina
DEQ Incident No. 48982
H&H Job No. TPM-001
October 11, 2023
hart � hickman
SMARTER ENVIRONMENTAL SOLUTIONS
C-1269 Engineering
#C-245 Geology
2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301
Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com
704.586.0007 main 919.847.4241 main

Initial Abatement Action Report
A. Site Information
1. Site Identification
Date of Report: October 11, 2023
Facility ID: N/A UST Incident Number: 48982
Site Name: Former Church Property
Site Street Address: 3201 Tuckeseegee Road
City, Town: Charlotte Zip Code: 28208 County: Mecklenburg
Description of Geographical Data Point: Former UST-1 location
Location Method: Google Earth
Latitude: 35.2431 N Longitude:-80.8818 W
2. Information about Contacts Associated with the Leaking UST System
UST Owner: TPM Properties Limited PartnershiD
Address: 3816 Mooreland Farm Road, Charlotte, NC Tel.: [phone]
UST Operator: Unknown
Address: N/A Tel.: Unknown
Property Owner: TPM Properties Limited Partnership
Address: 3816 Mooreland Farm Road, Charlotte, NC Tel.: [phone]
Property Occupant: Vacant Address: Tel.:
Consultant/Contractor: Hart & Hickman, PC
Address: 2923 South Tryon Street, Suite 100, Charlotte, NC 28203
Tel.: [phone] (Attn: Steve Libbey, PG)
Analytical Laboratory: Waypoint Analytical State Cert. No. 402
Address: 449 Springbrook Road, Charlotte, NC 28217 Tel.: [phone]
3. Information About Release
Date Discovered: June 2023
Estimated Quantity of Release: Unknown
Cause of Release: UST
Source of Release: Heating Oil USTs
Sizes and contents of UST system: Three 1,100-gallon heating oil USTs
4. Certification
I, Stephen Libbey, PG a Licensed Geologist at Hart & Hickman, PC, do certify that the
information c`,, gWiuwd,� n this report is correct and accurate to the best of my knowledge.
\ �0� ��A CARD
SEAL St ,G Z_,A�
. 1658
10/11/23
Hart & Hickman, PC is licensed to practice geology/engineering in North Carolina. The
certification numbers of the company are C-245/C-1269.
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B. Site History and Characterization
1. UST/AST Owner and Operator Information:
UST/AST ID No.
UST-1 — UST-3, and
AST-1 and AST-2
Facility ID Number
N/A
Name of Owner
Dates of Ownership
TPM Properties Limited Partnership
2017 - Current
Street Address
3816 Mooreland Farm Road
City
State
Zip
Telephone Number
Charlotte
NC
28226
704-361-3330
Name of Operator
Dates of Operation
Former Church
Unknown
Street Address
3201 Tuckaseegee Road
City
State
Zip
Telephone Number
Charlotte
NC
28208
Unknown
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SMAKTEA ENVIRONMENTAL SOLUTIONS

2. UST/AST Information:
Was
Approximate
Description of
Date
release
UST ID
Current/Last
Previous
Capacity
Construction
Status of
associated
Number
Contents
Contents
(gallons)
Details
Tank
Associated Piping and
Tank
UST
with the
Dimensions
Pumps
Installed
UST
System?
Steel - extended
UST-1
Heating Oil
N/A
1,100
Steel
12' x 4'
underground to former
Unknown
Removed
Yes
nearby building
Steel — extended
Unknown
UST-2
Heating Oil
N/A
1,100
Steel
12' x 4'
underground to former
Removed
Yes
nearby building
Steel — extended
Unknown
UST-3
Heating Oil
N/A
1,100
Steel
12' x 4'
underground to former
Removed
No
nearby building
Was
release
AST ID
Current/Last
Previous
Capacity
Construction
Approximate
Description of
Date
Status of
associated
Number
Contents
Contents
(gallons)
Details
Tank
Associated Piping and
Tank
AST
with the
Dimensions
Pumps
Installed
AST
System?
AST-1
Heating Oil
N/A
Unknown
Unknown
Unknown
Steel - above ground
Unknown
Removed
No
AST-2
I Heatin Oil
I N/A
1 150
1 Steel
1 30" x 4'
Steel - above ground
I Unknown
I Removed
I No
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SMARTER EWRONMENTAL SOLUTIONS

3. Non-UST/AST spills at the site:
No non-UST/AST spills are known to have occurred at the site.
4. Description of release:
An accidental heating oil discharge was discovered by Charlotte -Mecklenburg
Storm Water Services (CMSWS) personnel on April 28, 2023. Specifically,
CMSWS personnel observed heating oil on the ground surface beneath a
stormwater outfall and in shallow soils on two nearby properties. CMSWS
personnel suspected that during a heavy rain event, heating oil migrated from an
on -site leaking heating oil underground storage tank (UST) and traveled onto the
adjacent properties via stormwater piping. After release discovery, CMSWS
contracted with Carolina Environmental Response Team (CERT) to recover
floating heating oil using absorbent pads and booms.
On May 12, 2023, representatives from TPM Properties and H&H visited the
property and inspected the surface release area. No heating oil free product was
observed on the ground surfaces or in residual rain puddles located on -site;
however, petroleum odors (heating oil) were detected in the shallow surficial soils
in the release areas on the adjacent properties and coming from cracks in the
stormwater piping where it was exposed at the ground surface. Based on
observations during this site visit, a review of historical documents, and
discussions with CMSWS personnel, H&H determined that three heating oil
USTs were left in the ground when the site buildings were razed in late 2022.
H&H agreed with CMSWS personnel that one or more of these USTs were
potentially the source of the free product and surficial soil impacts.
Between June 6 and 12, 2023, and on August 14 and 15, 2023, H&H oversaw the
removal of the petroleum -impacted surficial soils, approximately 190 ft of
petroleum -impacted stormwater piping, and three (3) 1,100-gallon non-
commercial/non-regulated heating oil USTs (UST-1, UST-2, and UST-3) by EVO
Corporation (EVO) of Winston-Salem, North Carolina. The closure activities are
discussed further in Section D below.
5. Site characteristics:
The site is approximately 2.2 acres in area and formerly contained an approximate
2,942-square foot (sq ft) vacant residence/church annex, an approximate 1,000-sq
ft storage garage, and an approximate 30,636-sq ft vacant church. A site location
map is presented as Figure 1, and a site map is presented as Figure 2.
The subject property is located in the Piedmont Physiographic Province of North
Carolina. According to the Geologic Map of North Carolina dated 1985, the
subject property lies within the Charlotte Belt. In the site area, underlying
bedrock is composed of granitic rock. The land surface of the area is generally
characterized as gently sloping, which may become moderately steep where
intersected by streams.
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In the Piedmont, the bedrock is overlain by a mantle of weathered rock termed
saprolite or residuum. The saprolite consists of unconsolidated clay, silt, and sand
with lesser amounts of rock fragments. Due to the range of parent rock types and
their variable susceptibility to weathering, the saprolite ranges widely in color,
texture, and thickness. Generally, the saprolite is thickest near interstream divides
and thins toward streambeds. In profile, the saprolite normally grades from
clayey soils near the land surface to highly weathered rock above competent
bedrock.
The occurrence and movement of groundwater in the Piedmont is typically within
two separate but interconnected water -bearing zones. A shallow water -bearing
zone occurs within the saprolite, and a deeper water -bearing zone occurs within
the underlying bedrock.
The site is located at an approximate elevation of 740 ft above mean sea level.
Topography in the source area generally slopes to the southwest (Figure 1).
Based on topography, H&H anticipates that the groundwater flow direction at the
site is to the southwest.
Visual observations during excavation activities and soil sample collection
indicated that the soil surrounding the UST system consisted of brownish silty
clays and clayey silts (saprolite).
Municipal water is available to the site and the areas surrounding the site. While
a formal water supply survey was not completed, no water supply wells were
observed within 150 ft of the non -regulated heating oil USTs. Additionally, no
surface water bodies were identified within 500 ft of the USTs (Figure 1).
6. Initial abatement actions, assessment activities, and corrective actions
performed to date:
Prior to the June 2023 UST closure activities, no other known initial abatement
actions, assessments, or corrective action activities were conducted at the site.
However, monitoring wells were observed on the property that appear to be
associated with an upgradient off -site UST release.
C. Site Check Report
Not applicable.
D. UST Closure Report following UST-12 format and Site Investigation Report
for Permanent Closure or Change -in -Service of UST (UST-2 Form)
1. Preparations for closure including the steps taken to notify authorities,
permits obtained and the steps taken to clean and purge the tanks:
Prior to UST closure activities, EVO obtained a permit from the Mecklenburg
County Fire Marshal authorizing the UST removals.
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Prior to removal, residual fluids were removed using a vacuum truck by EVO.
Following residual fluid removal, the USTs were triple -rinsed by EVO in
accordance with Mecklenburg County Fire Marshal requirements. Approximately
1,800 gallons of residual fluids, sludge, and rinse water were removed from the
UST systems.
Following residual fluids removal, the USTs were purged of combustible vapors
with dry -ice and tested with a combustible gas indicator to check that potentially
combustible vapors had dissipated.
2. Closure procedures:
Initially, soil was removed from the top and sides of the USTs and stormwater
piping with a track hoe so that the tanks and piping could be removed from the
ground. Soils encountered during the surface release, stormwater piping, and
UST excavations were evaluated in the field for the presence of odors and
staining, and for the presence of organic vapor readings with a calibrated
photoionization detector (PID). The PID was calibrated prior to its use against an
isobutylene standard.
Following removal, the USTs and stormwater piping were inspected for holes or
other signs of structural damage. The USTs were single -walled and constructed
of steel. Multiple holes and moderate pitting were observed on the bottom
surfaces of the USTs. The stormwater piping was constructed of 5 ft sections of
18" diameter reinforced concrete pipe. Several cracks were observed along the
190 ft section of piping removed.
Subsurface product piping connected to the USTs also was removed for proper
disposal. The product piping was constructed of steel. Multiple holes were
observed in the product piping.
3. Note the amount of residual material pumped from the tank and describes
the storage, sampling and disposal of the residual material and the disposal
of the tank, pumps and piping:
As stated above, EVO removed approximately 1,800 total gallons of residual
fluids, sludge, and rinse water from the USTs. The fluids were treated at the
HOH Corporation facility in Winston-Salem, NC. The non -hazardous material
manifest for the residual fluids is included in Appendix A.
The USTs were transported off -site by EVO for disposal at Foss Recycling in
Winston-Salem, North Carolina. The tank disposal certificate for the USTs is
included in Appendix A. The concrete stormwater piping was disposed of at a
local construction and demolition (C&D) landfill.
4. Initial response actions and initial abatement actions:
Initial response and abatement actions are discussed in the following section.
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5. Soil excavation and Site Investigation activities:
Surface Release Excavation and Stormwater Piping Removal
Surficial impacted soil in the stormwater piping outfall and adjacent homeowner's
backyard areas were excavated using a small excavator on June 6 and 7, 2023.
The extent of soil impacts was identified using a calibrated PID. Following
impacted soil excavation, seven confirmation soil samples (EX-4, EX-5, EX-6,
EX-12, EX-13, EX-14, and EX-15) were sent to Waypoint Analytical (Waypoint)
for analyses of gasoline -range total petroleum hydrocarbons (TPH-GRO) by EPA
Method 5030/8015M and diesel -range TPH (TPH-DRO) by EPA Method
3550/8015M. Approximately 0.5 to 1.0 ft of soil was excavated in the area
depicted in Figure 3.
As shown in Table 1, apart from soil sample EX-13, TPH-GRO and TPH-DRO
were not detected above the DEQ Action Levels of 50 mg/kg and 100 mg/kg,
respectively, in the post -excavation confirmation soil samples. TPH-DRO was
detected at a concentration of 124 mg/kg in soil sample EX-13 which slightly
exceeds the Action Level of 100 mg/kg.
Based on the detection of TPH-DRO in soil sample EX-13 above the TPH-DRO
Action Level, on August 14, 2023, H&H excavated an additional approximately
10 tons of impacted soils in the vicinity of this soil sample. Following soil
excavation, a post -excavation soil sample (EX-18-F) was collected from the base
of the excavation. The soil sample was analyzed by Waypoint for TPH-GRO and
TPH-DRO. As shown in Table 2, TPH-GRO and TPH-DRO were not detected
above the laboratory detection limits in the sample.
On June 7 and 8, 2023, an estimated 190 ft section of 18" diameter out -of -service
concrete stormwater piping was removed for off -site disposal. The section of
pipe removed began immediately upgrade of a crack in the pipe exposed at the
ground surface near the former church building to the downgradient property
boundary outfall (Figure 3). After removal, soil samples were collected below the
piping and screened with a PID. Six of these samples (EX-1, EX-2, EX-3, EX-9,
EX-16, and EX-17) were sent to Waypoint for analyses of TPH-GRO and TPH-
DRO.
Soil impacts were identified with the PID in four locations along the stormwater
piping. In these locations, soil impacts were identified below piping joints where
a 5 ft section of pipe was attached to an adjacent 5 ft section of pipe. The
impacted soils were excavated and post -excavation trench base soil samples were
collected. In the vicinity of soil samples EX-10 and EX-11, only the soil
immediately below the stormwater piping joint was found to be impacted and
excavated. Because of the limited impacted soil volume, soil samples EX-10 and
EX -II were analyzed by Waypoint for TPH-GRO and TPH-DRO only. The
remaining two soil excavations varied in length and were approximately 5 ft or
less in width and 5 ft or less deep. The post -excavation trench base soil samples
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(EX-7 and EX-8) in these locations were analyzed by Waypoint for volatile
organic compounds (VOCs) by EPA Method 8260, semi-VOCs by EPA Method
8270, and Volatile Petroleum Hydrocarbons (VPH) and Extractable Petroleum
Hydrocarbons (EPH) by the Massachusetts Department of Environmental
Protection (MADEP) methods.
The analytical results for the stormwater piping closure and post -excavation soil
samples are presented in Tables 1 and 2, respectively. As shown in Table 1, TPH-
GRO and TPH-DRO were detected as high as 235 mg/kg and 142 mg/kg in the
closure samples, respectively. As shown in Table 2, TPH-GRO and TPH-DRO
were not detected above the DEQ Action Level in post -excavation soil samples
EX-10 and EX-10. Additionally, detected compound concentrations did not
exceed the Soil -to -Groundwater, Residential, or Commercial/Industrial Maximum
Soil Contaminant Concentrations (MSCCs) in post -excavation soil samples EX-7
and EX-8.
It is important that even though field screening did not identify elevated PID
readings in soils near soil sample EX-16, TPH-GRO was detected at a
concentration of 150 mg/kg in this sample. TPH-DRO was not detected at a
concentration above the laboratory detection limit in this sample. As a result,
H&H collected a subsequent soil sample (EX-16-13) at this location on July 17,
2023 using a decontaminated hand auger (Figure 3). The sample was analyzed by
Waypoint for VOCs by EPA Method 8260, semi-VOCs by EPA Method 8270,
and VPH and EPH by the MADEP methods. As shown in Table 2, no target
compounds were detected above laboratory detection limits in soil sample EX-16-
B.
Approximately 103 total tons of impacted soil were excavated from the surface
and stormwater piping release areas. The excavated soil was transported to
EVO's treatment facility in Winston-Salem, NC for proper disposal. A copy of
the certificate of disposal, non -hazardous waste manifests, and certified weight
tickets for the excavated soil are provided in Appendix A. Following soil
removal, the excavations were backfilled with clean imported backfill material.
The imported backfill material consisted primarily of brown sandy silts. In
addition, in the adjacent property owner's backyard, the excavation was backfilled
with topsoil and the excavation area was seeded and covered with straw.
All soil samples were analyzed by a North Carolina certified laboratory. A chain -
of -custody record was completed for samples collected and included sample
description, date collected, time collected, matrix, sample container information,
and analyses required. The chain -of -custody was signed by H&H prior to
placement in an iced cooler for shipment to the laboratory. Prior to shipment, the
cooler was closed with a seal indicating the H&H representative's signature and
date such that a potential disturbance of the cooler contents could be detected by
the laboratory. Laboratory analytical reports are presented in Appendix B.
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UST Closures
After the removal of tanks UST-1, UST-2, and UST-3 on June 8, 2023, two
closure soil samples were collected below each tank in accordance with DEQ
guidelines. The samples were collected and shipped to the laboratory using the
same chain -of -custody procedures discussed above. The closure samples were
analyzed by Waypoint for TPH-GRO and TPH-DRO (Appendix B). The
analytical results for the closure soil samples collected below UST-1 (UST-1-A
and UST-1-13) and UST-2 (UST-2-A and UST-2-13) indicated the presence of
TPH-DRO and TPH-GRO above the DEQ Action Levels. TPH-GRO was
detected as high as 895 mg/kg and TPH-DRO was detected as high as 43,900
mg/kg. Closure soil samples collected below UST-3 (UST-3-A and UST-3-13) did
not contain TPH-DRO or TPH-GRO concentrations above DEQ Action Levels.
A total of approximately 163 tons of impacted soils were excavated from below
tanks UST-1 and UST-2. Based on field screening with a PID and closure soil
sampling, soil impacts below UST-2 were predominantly limited to the southern
end of the UST. The dimensions of the UST-1 excavation were approximately 18
ft long by 16 ft wide by 24 ft deep and the dimensions of the UST-2 excavation
were approximately 8 ft long by 6 ft wide by 16 ft deep. Note that the excavation
for UST-1 extended into the groundwater capillary fringe and ended immediately
above the groundwater interface at a depth of approximately 24 ft below ground
surface (bgs). During excavation, H&H estimated that the groundwater interface
was located at a depth of approximately 25 ft bgs. The excavated soil was
transported to EVO's treatment facility in Winston-Salem, NC for proper
disposal. A copy of the certificate of disposal, non -hazardous waste manifests,
and certified weight tickets for the excavated soil are provided in Appendix A.
During and following soil over -excavation activities, confirmation soil samples
were collected from the UST basin excavations (Figure 4). Four shallow sidewall
samples (UST-1-C, UST-1-13, UST-1-E, and UST-1-17), four deeper sidewall
samples (UST-1-H, UST-1-I, UST-14, and UST-1-K), and one base soil sample
(UST-1-G) were collected in the UST-1 basin excavation at depths of 10 ft bgs,
18 ft bgs, and 18 ft bgs, respectively. In the UST-2 basin excavation, four
sidewall samples (UST-2-C, UST-2-13, UST-2-E, and UST-2-17) were collected at
approximate depths of 15 ft bgs, and one base soil sample (UST-2-G) was
collected at an approximate depth of 16 ft bgs. In accordance with DEQ
guidance, the post -excavation confirmation soil samples were analyzed by
Waypoint for VOCs by EPA Method 826013/5035A, SVOCs by EPA Method
8270, and EPH and VPH using the MADEP Methods (Appendix B).
It is important to note that due to an inadvertent sampling error, soil sample UST-
2-G collected from the base of the UST-2 basin excavation was originally omitted
from laboratory submittal during the June 2023 excavation activities. As a result,
the sample was collected using a decontaminated hand auger on July 17, 2023. In
addition, due to the detection of TPH-DRO above the Action Level in soil sample
UST-2-A collected below the northern end of UST-2, H&H collected an
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additional soil sample (UST-2-G) at this location on July 17, 2023 using a
decontaminated hand auger. Soil sample UST-2-G was analyzed by Waypoint for
VOCs, SVOCs, and EPH and VPH using the MADEP Methods (Appendix B).
As shown in Table 2, Total C 19-C 18 Aliphatics, Total C9-C22 Aromatics, and 1-
methylnaphthalene concentrations in soil sample UST-I-G exceeded Soil -to -
Groundwater MSCCs. The detected Total C9-C22 Aromatics concentration also
exceeded its Residential MSCC, but is below the Commercial/Industrial MSCC.
As noted above, the impacted soils in the vicinity of soil sample UST- 1-G (18 ft)
were excavated when the excavation was extended into the capillary fringe (24
ft). No other compounds were detected above the MSCCs in the post -excavation
confirmation soil samples collected from the UST -I basin excavation.
In the UST-2 basin excavation, Total C9-C22 Aromatics concentrations exceeded
Soil -to -Groundwater MSCCs in the confirmation sidewall soil samples UST-2-1)
and UST-2-F. However, the detected concentrations are below the Residential
and Commercial/Industrial MSCCs. No other compounds were detected above
MSCCs in the post -excavation confirmation soil samples collected from the UST-
2 basin excavation.
Following soil removal, the excavations were backfilled with clean imported
backfill material. The imported backfill material consisted primarily of brown
sandy silts.
E. Free Product Investigation and Recovery Report
Not applicable.
F. Groundwater and Surface Water Investigation
Not applicable.
G. Initial Response and Abatement Activities
See Section B.
H. Excavation of Contaminated Soil
See Section D.
I. Conclusions and Recommendations:
In June and August 2023, H&H oversaw the removal of petroleum -impacted
surficial soils, approximately 190 ft of petroleum -impacted stormwater piping, and
three 1,100-gallon non-commercial/non-regulated heating oil USTs at the subject
property. Approximately 113 total tons of impacted soils were excavated from the
petroleum -impacted surficial soil and stormwater piping excavations, and
approximately 163 total tons of impacted soils were excavated from two UST basin
excavations. Soil impacts were not identified above DEQ Action Levels in the
third UST basin.
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Results of post -excavation confirmation soil sampling in the petroleum -impacted
surficial soil, stormwater piping, and UST basin excavation areas indicated
compound concentrations below DEQ Soil -to -Groundwater, Residential, and
Commercial/Industrial MSCCs.
Based on the results of the soil excavation activities and the lack of potential
receptors in the vicinity of the site, H&H requests no further action (NFA) for the
heating oil UST release incident. As part of the NFA, a Notice of Residual
Petroleum (NRP) which restricts groundwater usage at the property will be prepared
and recorded with the property deed.
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SMAKTEA ENVIRONMENTAL SOLUTIONS

Table 1
Summary of Closure Soil Sample Results
Former Church Property
3201 Tuckaseegee Road
Charlotte, North Carolina
H&H Job. No. TPM-001
Analytical Method
5030/
8015C
3550/
8015C
Contaminant of Concern
0
(D
=
a.
0
_
0-
Sample ID
Date
Collected
Source Area
Sample
Depth (ft)
Incident
Phase
EX- 1
06/06/23
Storm Drain
3
IA
<7.90
<23.7
EX-2
06/06/23
Storm Drain
3
IA
<6.02
24.7
EX-3
06/06/23
Storm Drain
3
IA
235
142
EX-9
06/07/23
Storm Drain
3
IA
<6.53
<13.1
EX-16
06/08/23
Storm Drain
3
IA
150
<14.6
EX-17
06/08/23
Storm Drain
3
IA
<6.80
<13.6
UST-1-A
06/08/23
UST
7
IA
895
18,100
UST-1-13
06/08/23
UST
7
IA
827
7,450
UST-2-A
06/08/23
UST
7
IA
<7.34
160
UST-2-13
06/08/23
UST
7
IA
21.5
43,900
UST-3-A
06/08/23
UST
7
IA
<7.31
<14.6
UST-3-13
06/08/23
UST
7
IA
<7.61
18.9
Action Levels' (mg/kg)
50
100
Notes:
1 = UST Section Action Levels for TPH-GRO and TPH-DRO of 50 mg/kg and 100 mg/kg, respectively (May 2021).
Concentrations are reported in milligrams per kilogram (mg/kg).
Values in bold exceed the Action Level(s).
TPH = Total Petroleum Hydrocarbons; GRO = Gasoline Range Organics; DRO = Diesel Range Organics; UST =
Underground Storage Tank; PL = Product Line; DISP = Product Dispenser
Table 1 (Page 1 of 1)
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/TPM Properties Limited Partnership/ReporUTables.xls man ! Haft &Hick
10/10/2023 f n1,

Table 2
Summary of Post -Excavation Confirmation Soil Sample Results
Former Church Property
3201 Tuckaseegee Road
Charlotte, North Carolina
H&H Job. No. TPM-001
Analytical Method
5030/
8015C
3550/
8015C
MADEP
MADEP
MADEP
MADEP
MADEP
MADEP
MADEP
MADEP
8260B
8260B
8260E
8260B
8260E
8260B 8260B
8270E
8270E
8270E
Contaminant of Concern
O
(7
=
F
O
O
_
F
L
Q
U
U
_
>
In
fl.
'-
N
_
U
U
_
>
to
sZ
aO
U
U
_
w
to
U
fl-
co
U
U
�
�-
Q
M
U
_
w
U
EO
O
_
U
U
_
>
_(n
O
Q
N
V
U
_
w
U
EO
N
N
U
U
F
m
fJ
a)
C
m
C
=3
00
w
C
a)
7
O
a
n
o
a
N
c
L
-
z
C
Q
t
E
F
cli
C
L
t
E
F
U')
M
to
a)
a>
X
N
N
L
L
O_
c
L
a)
N
L
L
a
ca
c
N
L
m
a
Sample ID
Date
Collected
Source Area
Sample
Depth (ft)
Incident
Phase
EX-4
06/06/23
Storm Drain
1
IA
<6.76
<13.5
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
EX-5
06/07/23
Storm Drain
1
IA
<8.22
<24.7
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
EX-6
06/07/23
Storm Drain
1
IA
<6.58
<13.2
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
EX-7
06/07/23
Storm Drain
4
IA
NA
NA
<11.0
<11.0
<68.8
BDL
<68.8
<11.0
<68.8
BDL
<0.006
<0.006
<0.006
<0.909
<0.006
<0.007
<0.006
<0.909
<0.909
<0.909
EX-8
06/07/23
Storm Drain
4
IA
NA
NA
<11.0
<11.1
<69.4
BDL
<69.4
<11.1
<69.4
BDL
<0.006
<0.006
<0.006
0.027
0.026
1.026
0.024
<0.916
<0.916
<0.916
EX-10
06/07/23
Storm Drain
3
IA
<7.25
<17.4
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
EX-11
06/07/23
Storm Drain
3
IA
<7.11
<14.2
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
EX-12
06/07/23
Storm Drain
1
IA
<7.00
27.9
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
EX-13
06/07/23
Storm Drain
1
IA
<7.2
124
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
EX-14
06/07/23
Storm Drain
1
IA
<8.29
26.0
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
EX-15
06/07/23
Storm Drain
1
IA
<6.35
<12.7
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
EX-16-13
08/14/23
Storm Drain
3
IA
NA
NA
<10.1
<10.1
<62.2
BDL
<62.2
<10.1
<62.2
BDL
<0.006
<0.006
<0.006
<0.012
<0.006
<0.006
<0.006
<0.822
<0.822
<0.822
EX-18-F
06/09/23
Storm Drain
5
IA
<7.98
<14.8
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
UST-1-C
06/09/23
UST
10
IA
NA
NA
<10.8
<10.8
<67.9
BDL
<67.9
<10.8
<67.9
BDL
<0.006
<0.006
<0.006
<0.013
<0.006
<0.006
<0.006
<0.893
<0.893
<0.893
UST-1-D
06/09/23
UST
10
IA
NA
NA
<10.6
<10.6
<66.6
BDL
<66.6
<10.6
<66.6
BDL
<0.006
<0.006
<0.006
<0.013
<0.006
<0.006
<0.006
<0.877
<0.877
<0.877
UST-1-E
06/09/23
UST
10
IA
NA
NA
<10.7
<10.7
BDL
<66.6
<10.7
<66.6
BDL
<0.006
<0.006
<0.006
<0.013
<0.006
<0.006
<0.006
<0.882
<0.882
<0.882
UST-1-F
06/09/23
UST
10
IA
NA
NA
<10.4
<10.4
BDL
<64.6
<10.4
<64.6
BDL
<0.006
<0.006
<0.006
<0.012
<0.006
<0.006
<0.006
<0.854
<0.854
<0.854
UST-1-G
06/09/23
UST
18
IA
NA
NA
<11.6
86.2
q66
1,146
<289
12.3
1,290
1�
0.016
0.025
0.045
<0.014
0.008
0.056
<0.007
2.98
1.11
2.67
UST-1-H
06/09/23
UST
18
IA
NA
NA
<10.7
<10.7
BDL
<66.6
<10.7
<66.6
BDL
<0.006
<0.006
<0.006
<0.013
<0.006
<0.006
<0.006
<0.878
<0.878
<0.878
UST-1-1
06/09/23
UST
18
IA
NA
NA
<11.2
<11.2
<70.1
BDL
<70.1
<11.2
<70.1
BDL
<0.007
<0.007
<0.007
<0.014
<0.007
<0.007
<0.007
<0.926
<0.926
<0.926
UST-1-J
06/09/23
UST
18
IA
NA
NA
<10.1
<10.1
<63.0
BDL
<63.0
<10.1
<63.0
BDL
<0.006
<0.006
<0.006
<0.012
<0.006
<0.006
<0.006
<0.830
<0.830
<0.830
UST-1-K
06/09/23
UST
18
IA
NA
NA
<11.1
<11.1
<69.5
BDL
<69.5
<11.1
<69.5
BDL
<0.006
<0.006
<0.006
<0.013
<0.006
<0.006
<0.006
<0.919
<0.919
<0.919
UST-2-C
06/08/23
UST
15
IA
NA
NA
<10.8
<10.8
<66.9
BDL
<66.9
<10.8
<66.9
BDL
<0.006
<0.006
<0.006
<0.013
<0.006
<0.006
<0.006
<0.887
<0.887
<0.887
UST-2-D
06/08/23
UST
15
IA
NA
NA
<11.7
<11.7
<73.5
BDL
<73.5
<11.7
131
131
<0.007
<0.007
<0.007
<0.014
<0.007
<0.007
<0.007
<0.967
<0.967
<0.967
UST-2-E
06/08/23
UST
15
IA
NA
NA
<11.2
<11.2
<69.7
BDL
<69.7
<11.2
<69.7
BDL
<0.006
<0.006
<0.006
<0.013
<0.006
<0.006
<0.006
<0.923
<0.923
<0.923
UST-2-F
06/08/23
UST
15
IA
NA
NA
<12.5
<12.5
218
218
93.1
<12.5
224
224
<0.007
<0.007
<0.007
<0.015
<0.007
<0.007
<0.007
<1.03
<1.03
<1.03
UST-2-G
07/17/23
UST
7
IA
NA
NA
<12.8
<12.8
91.9
91.9
<64.6
<12.8
<64.6
BDL
<0.006
<0.006
<0.006
<0.012
<0.006
<0.006
<0.006
<0.849
<0.849
<0.849
UST-2-H
07/17/23
UST
16
IA
NA
NA
<16.8
<16.8
<65.1
BDL
<65.1
<16.8
<65.1
BDL
<0.006
<0.006
<0.006
<0.013
<0.006
<0.006
<0.006
<0.861
<0.861
<0.861
Action Levels' (mg/kg)
50
100
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Soil to Ground Water MSCC (mg/kg)2
NS
NS
68
NS
NS
540
NS
NS
NS
31
2.4
2.2
0.12
0.2
6.6
6.6
6
0.054
1.5
64
Residential MSCC (mg/kg)2
NS
NS
625
NS
NS
1,560
31,200
NS
NS
469
782
1,560
1,560
5.5
156
156
3,120
22.8
62.5
469
Industrial/Commercial MSCC (mg/kg)2
NS
NS
9,340
NS
NS
23,300
467,000
NS
NS
7,000
11,600
23,300
23,300
27
2,330
2,330
46,700
112
934
7,000
Notes:
1 = UST Section Action Levels for TPH-GRO and TPH-DRO of 50 mg/kg and 100 mg/kg, respectively (May 2021).
2 = Division of Waste Management Maximum Soil Contaminant Concentration Levels (MSCCs; October 2021)
Apart from VPH and EPH, only those compounds detected are shown.
Concentrations are reported in milligrams per kilogram (mg/kg).
Values in bold exceed the Action Level or Soil -to -Groundwater MSCC.
Underlined values exceed Residential MSCCs.
Underlined and italic values exceed Residential and Industrial/Commercial MSCCs.
TPH = Total Petroleum Hydrocarbons; GRO = Gasoline Range Organics; DRO = Diesel Range Organics; IA = Initial Abatement; MADEP = Massachusetts Department of Environmental Protection; VPH = Volatile Petroleum Hydrocarbons;
EPH = Extractable Petroleum Hydrocarbons; NA = Not Analyzed; NS = Not Specified; MSCC = Maximum Soil Contaminant Concentration
BDL = Below Laboratory Detection Limit; J = Estimated Value Above Method Detection Limit, But Below Laboratory Reporting Limit; SVOCs = Semi -Volatile Organic Compounds
Table 2 (Page 1 of 1)
helps://haMick.sharepoint.wMsiteslMasterFiles-1/$hared Dwumenlsl -Master Projects PM PmpeOies Limited Pa0nership1ReporVTab1es.x1s
1
0
110/2023 Hart & Hickman, PC

Ro
Ch i
SITE
46
• .` - :� � fl,, re i - . �t ems'/] � • ,g -- i
- i C _ �" S ��} � 7 "'din $1 R7Y � . .•t�V, � ,A ,9' '
�• 1 ' � •� !, � � � — -.Copyright:0.2(' �ographRciroei,�,y�i-cubed,
0 2,000 4,000
N
SCALE IN FEET
U.S.G.S. QUADRANGLE MAP
CHARLOTTE WEST, NORTH CAROLINA 2013
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)

_ _EX-13- — — — — —EX 14— EX-1 ; )
X-12O EX-18-F
i
EX-6 O
EX-5 O— — —EX-4 O
ASPHALT
FORMER
RESIDENTIAL
FORMER
CHURCH
APPROXIMATE LOCATION OF
CRACK IN STORMWATER PIPE
EXPOSED AT GROUND \
EX-17 S�
i EX-16 — SO
SDr E��� - J DI so—so XD16B
EX-9�� L - __EX-3 `r0
SD� \
— 'EX-1
D -1=O JSD — ISDX $
_� SD E��,D
EX-11
EX_l SD 1 lO
so
so
\O
O
so
so
RESIDENCE \
(1304 ENDERLY ROAD)
so
RESIDENCE \
(1224 ENDERLY ROAD)
so
FORMER
CHURCH
LEGEND
SITE PROPERTY BOUNDARY
PARCELBOUNDARY
SD
18" RCP STORMWATER PIPE
— — — —
APPROXIMATE EXTENT OF SOIL
EXCAVATION
DI
DROP INLET
STORMWATER OUTFLOW
EX-1 0
CLOSURE SOIL SAMPLE
EX-18-F
POST -EXCAVATION
CONFIRMATION SOIL SAMPLE
NOTES:
1. BASE DATA OBTAINED FROM MECKLENBURG COUNTY
GIS. 2023.
8
APPROXIMATE
0 25 50
SCALE IN FEET
SURFACE RELEASE SAMPLE LOCATIONS MAP
---- FORMER CHURCH PROPERTY
3201 TUCKASEEGEE ROAD
CHARLOTTE, NORTH CAROLINA
• 2923 South Tryon Street -Suite 100
hart hickman Charlottc,North Carolina 28203
P. 704-586-0007(p) 704-586-0373(f)
SMARTER ENVIRONMENTAL SOLUTIONS Licensc # C-1269 / #C-245 Gcolop
DATE: 7-13-23
REVISION NO. 0
JOB NO. TMP-001
FIGURE NO. 3

UST-1-C/I ♦♦
•
i
Ci0 ♦ UST-1-F/H
UST-1-A• •
♦ UST-1-GOO
♦ U�ST-1-13
UST-1-D/J
♦♦ UST-1-E/K
V �
\'-ASPHALT-,\
UST-2-A UST-2-G
—�
UST-2-B
UST-2-F ♦ \
+; GUST-2\
UST-2-C
•
♦i UST-2-D
UST-2-H
FORMER
CHURCH
BUILDING
UST-3-B y
UST-3=A
FORMER
CHURCH
BUILDING
LEGEND
SITE PROPERTY BOUNDARY
PARCELBOUNDARY
- - - - APPROXIMATE EXTENT OF SOIL
EXCAVATION
FORMER UNDERGROUND
STORAGE TANK (UST)
UST-1-Aq CLOSURE SOIL SAMPLE
UST-1-Co POST -EXCAVATION
CONFIRMATION SOIL SAMPLE
NOTES:
1. BASE DATA OBTAINED FROM MECKLENBURG COUNTY
GIS,2020.
8
APPROXIMATE
0 15 30
SCALE IN FEET
UST CLOSURE SAMPLE LOCATIONS MAP
FORMER CHURCH PROPERTY
3201 TUCKASEEGEE ROAD
CHARLOTTE, NORTH CAROLINA
2923 South Tryon Street -Suite 100
dart � hickman Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
SMARTER ENVIRONMENTAL SOLUTIONS Licensc # C-1269 / #C-245 Geology
DATE: 7-13-23
REVISION NO. 0
JOB NO. TMP-001
FIGURE NO. 4

Appendix A
Certificate of Disposal and Non -Hazardous Waste Manifests, and Weight Tickets
hart '` hickman
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/TPM Properties Limited Partnership/Report/48982 CA )� 20231011.doc
SMARTER ENVIRONMENTAL SOLU71ONS

CORPORATION
1703 Vargrave Street
Winston-Salem, NC 27147
ph 336-725-5844
fax [phone]
Tank Owner: TPM Properties
Site Address: 3201 Tuckaseegee Road
Charlotte, NC
Description of Tanks:
Tank Size of Tank Contents
Number
1 1,000 Gallons #2 Fuel Oil
2 1,000 Gallons #2 Fuel Oil
3 1,000 Gallons 42 Fuel Oil
Transporter: Evo Corporation
EC Project #. 062310
Disposal Certification:
Evo Corporation does hereby certify that the above named storage tanks were
transported to Foss Recycling, 3459 Thomasville Road, Winston-Salem, NC for
proper disposal and recycling.
Signature
Thomas W. Hammett
CEO
Evo Corporation
www.evocorp.net = '"a i

-19
MERMNIE3
CORPORATION
1703 Vargrave Street
Winston-Salem, NC 27107
ph 336-725..5844
fax [phone]
Evo Corporation does hereby certify that 850 gallons of non -hazardous
contaminated water received on 6/7/2023 from:
Generator: TPM Properties
Originating at: 3201 Tuckaseegee Road
Charlotte, NC
EC Waste ID -: 062310
has been disposed of by Evo Corporation in a manner approved by the North
Carolina Department of Environmental Quality.
Signature
Thomas W. Hammett
CEO
Eva Corporation
www.evocorp.net

lwaw_M�XIC3
CORPORATION
1703 Vargrave Street
Winston-Salem, NC 27107
ph 336-725-5844
fax [phone]
1
Evo Corporation sloes hereby certify that 950 gallons of non -hazardous
contaminated sludge received on 6/7 and 6/S/2023 from:
Generator: TPM Properties
Originating at: 3201 Tuckaseegee Road
Charlotte, NC
EC Waste ID #: 062310
has been disposed of by Evo Corporation. in a manner approved by the North
Carolina Department of Environmental Quality.
k'
Signature
Thomas W. Hammett
CEO
Evo Corporation
www.evocorp.net ..,

-9990in '
wm,E?XI[:3
C0RP0RAT€ON
1703 Va, grave Street
Winston-Salem, NC 27107
ph 336-725-5844
fax [phone]
Evo Corporation does hereby certify that 103.09 tons of non -hazardous
contaminated material received on 6/6 and 6/7t2023 from:
Generator: TPM Properties
Originating at: 3201 Tuckaseegee Road
Charlotte, NC
EC Waste 1D #: 062310
has been disposed of by Evo Corporation in a manner approved by the North
Carolina Department of Environmental Quality.
0
Signature
Thomas W. Hammett
CEO
Evo Corporation
www.evocorp net

C O R P O R A T I O N
1703 Vargrave Street
Winston-Salem, NC 27107
fah 336-725-5844
fax [phone]
Eva Corporation does hereby certify that 163.14 tuns of non -hazardous
contaminated material received on 6/8, 61/9 and 6i12i2023 from:
Generator: TPM Properties
Originating at: 3201 Tuckaseeffee road
Charlotte, NC
EC Waste ID 4: 062310
has been disposed of by Evo Corporation in a manner approved by the North
Carolina Department of Environmental Quality.
Signature
Thomas W. Hammett
CEO
Evo Corporation
f-
www.evocorp.net I i�'£

EVO CORPORATION
1703
. ,:
t, Winston-Salem, NC 27107
NON -HAZARDOUS MATERIALS MANIFEST
Load V Manifest No. 1-8065
GENERATOR INFORMATION
Generator: Phone:
bite address:
City/State:
Charlotte, M
Gross Weight (lbs):
Empty Weight (lbs):
Net Weight (ibs:
_ 4-302-4404
rontact, 1homas Abore
TERit..-DESCiPTIO QUANTITY 1 WEIGHT
Material: ter
Contaminant: 19 e
l on
Quantity � Tans Drums Pails Sacs Yards Other:
________________-- _ _. -------- _-----
TRANSPORTER INFORMATION
Transporter: BV0 corwratio:a Phone: --
5844
`r ck ##,- Contact: Tonv Disher
As the transporter, l certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility designate.
Driver Signature, -----------
.: Date:
FACILITY INFORMATION
Bvo Cbrporation
Evo Project 052310
1703 XbLrgrave &reet- 5-
Phone:
i certify that the carrier has
material for treatment and/or
Facifity Signature:
Contact:
the materials described above to this facility, and I hereby accept this
n a manVthat has been authorized by the State of North Carolina.
Date. (0 / ? /fig
Canary/Invoice
Pink/Carrier

EVO CORPORATION
1703 Vargrave Street, Winston-Salem, NC
1.
MATERIALS,
IFEST
City/State: Charlotte,
Contact: ThOimas l�
MATERIAL IAL DESCRIPTION IPTIO( l QUANTITY / WEIGHT
Gross Weight (lbs): ......... ..... . Material: product
Empty Weight (lbs):
Net Weight (Ibs):
Contaminant; Q Biel
Oil
Quantity f Tons Drums Pails Sacs Wards ®then:
----
TRANSPORTER lNFGRMAT1Ghf
Transporter: r r Phone: --
Truck HUD, Contact: Tonv Usher
As the transporter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility designate.
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment and/or p al in a rn er that has been authorized by the State of Borth Carolina.
Facile r�ature:� Date:
White/Facility Canary/Invoice

EVO CORPORATION
Winston-Salem, NC
NON -HAZARDOUS MATERIALS MANIFEST
City/State: Contact. ThOmaA Abore
Gross Weight (Ibs ):
Empty Weight (lbs);
Net Weight (Ibs):
MAC Rl L DESCRIPTION / QUANTITY / WEIGHT
Material:
412 Fad Oil
Quantity Tons Drums Pails Sacs Yards Other:Uj =W1
>
---------------
TRANSPORTER INFORMATION
Truck #: � r _
Phone: [phone],1
Contact: lb Elisher
As the transporter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in comet, erce under the applicable regulations governing transportation. and I hereby receive this material for
delivery to the facility designate.
Driver Sictnatre:
peraCion
I certify that the carrier has dd
material for treatment and/or Esp
WC C i_ , � _._� . Date: �� bE
FACILITY INFORMATION
the materials described above to this facility, and I hereby accept this
in a man y that has been authorized by the State of North Carolina.
Date:
White/Facility Canary/Invoice
n

EVO CORPORATION
1703 Vargrave Street, Winston-Salem, NC 27107
NON -HAZARDOUS MATERIALS MANIFEST
Load # Manifest No.
------------
GENERATOR INFORMATION
"ems -
Generator- Phone:
City/State: Chairlotte, RC
Contact: Ore,
_____
MATERIAL DESCRIPTit / C UANTITY / WEIGHT
Grass Weight (lbs): 61,75
Material., SDA
Empty Weight (ibs)- 29 WI L-) Contaminant:
Net Weight (lbs):`�
Quantity �} /, � Tans Drums Pails Sacs Wards Other:
TRANSPORTER INFORMATION
----------------
ration Phone:[phone]
Trck #: a Contact: e-
s the transporter, I certify that the materials described above being slipped under this non -hazardous
materials manifest are properly classified: packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility designate.
Driver Si nat re:
Dvo ClDrlmration
Date:'
FACILITY INFORMATION
Evo Project #:
Iris
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment and/car disposal in a manner that has been authorized by the State of Borth Carolina.
Facility Si nature:
Gate:6 --c-X-3
White/Facility
Canary/Invoice
er

City/State:
1703 EVO CORPORATION
NON -HAZARDOUS
MATERIAL DESCRIPTION I QUANTITY i WEIGHT
�4
Grass Weight ibs): �� material: SDil
b
Empty Weight (lbs': �-to€rant:
Net Weight (lbs): � 7
Quantity e Tons Drums Fails Sacs Yards Other:
TRANSPORTER INFORMATION
Bvo '. l a Phone: [phone]
Truck #: Contact: - .Ibitv Usher
As the transporter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classif€ed, packaged: iabeled, secured and are in proper condition for transport
in commerce Linder the applicable regulations governing transportation, and i hereby receive this material for
delivery to the facility designate,
Driver Sicinature.
_. Date lz�
FACILITY INFORMATION
Rhone:
Contact -
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility iqrature: Date: 4k
Ito
e
2

CORPORATIONEVO
1703 Vargrave Street, Winston-Salem, NC 1'
NON -HAZARDOUS MATERIALS MANIFEST
Load # _ _ _ Manifest No.
GENERATOR INFORMATION
!PM PropeAiea
Generator: Phone- 704-302-4404
Site Address: 4201 s. Rbad
city/state: e, lu
Grass ?sleight (lbs)
Empty Weight (Ibs)
Net :height (€bs')
Quantity
MT€AL DESCRIPTION I QUANTITY l WEIGHT
7-5 f Mo
.2-9
q5.
lz. s
Contaminant.,
Tons Drums Pails Sacs Yards Other.
TRANSPORTER INFORMATION
Transporter: Bvo ObrWrationPhone: -' ->
844
Truck #, Contact:
s the transporter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly ciassified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facHity designate.
Driver Signature:
Date- K7-2
FACILITY INFORMATION
Evo Project #:
Contact:
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment andior disposal ire a manner that has been authorized by the State of North Carolina.
Facility inat�re�_'' _ _Cate, 6-7
White/Facility Canary/invoicemm� � Pink/Carrier

EVO CORPORATION
Vargrave Street, Winston-Salem, NC 27107
www.evocorp.net
MATERIALS
GENERATOR INFORMATION
ATION
Generator: TPM Properties
Site Address:;3201 ltckaseegee Road
City tate;
Gross Weight (Ibs,
Empty Weight lbs)
Net Weight (lb )
Manifest No
Phone, 704-302-44&4'
MATERIAL ERIAL DESCRIPTION / QUANTITY / WEIGHT
10 5 00
2'J,H 6
-ZS1 OHO
Contaminant:
Quantity Roz
Tons Drums Pails Sacs Yards Gather:
TRANSPORTER INFORMATION
Transporter
Truck
Phone- 336-725-5844
Dishe
Contact:;.
(754
As the transporter, i certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
del=very to the facility designate.
[giver ionature:
Gate: " Z
FACILITY INFORMATION
I. �vo Project #:
Contact:
I certify that the carrier has delivered the materials described above to this facility, and i hereby accept this
material for treatment and/or disposal in a manner that has been authorized by the Mate of North Carolina,
gnatutje s Date: c'' a �`•
White/Facility Canary/invoice Pink/Carrier

1703 Vargrave Street, Winston-Salem, NC EVO CORPORATION
NON -HAZARDOUS MATERIALS MANIFEST
Load 41 Manifest No,17-755
GENERATOR INFORMATION
___mm_ ----.... _ ..-..._.--_.-.--- _ __.._..
-
Oe4404
rsratr�r, IPM Properties Pone:
Site Address: 3201 lUckaseegee Road
_Mlomas Abore
...............
MATERIAL DESORIPTJON / QUANTITY WEIGHT
Gross Weight (lbs)
Empty Weight (lbs): _
Net Weight (lbs): 10-,.. .,.�,
Material: so 1"I
Contaminant-
Tons Drums Pails Sacs Yards Other:
._..m_------ _-___._-__._-_._.__-.._---__.__.__
TR NS ORTER INFORMATION
A
r,
As the transporter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged. labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility designate.
Driver Signature:
_ Date:
FACILITY YINFORMATION
Evo Project #:
Contact:
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment and/or disposal in a m� , �r that has been authorized by the Mate of North Carolina,
FacilitySignature: �l`� Date:
White/Facility Canary/Invoice Pink/Carrier

i CKET NUMBER
1069523157570
®e2)
F1
CERTIFIED
AUTOMATED
TRUCK
SCALE
THE CAT SCALE GUARANTEE
The CAT Scale Company guarantees that our scales will give an accurate weight. What makes
us different from other scale companies is that we back up our guarantee with cash'
WEIGH WHAT WE SAY OR WE PAYS
If you get an overweight fine from the state AFTER one of our CAT Scales showed a legal weight, we will
immediately check our scale and we will:
(1) Reimburse you for the cost of the overweight fine it our scale is wrong, OR
(2) A representative of CAT Scale Company will appear in court WITH the driver as an expert witness if we
believe our scale was correct.
IF YOU SHOULD GET AN OVERWEIGHT FINE, YOU SHOULD DO THE FOLLOWING TO GET THE PROBLEM RESOLVED:
1) Post bond and request a court date.
2) Call CAT Scale Company direct 24 hours a day at 1-877-CATSCALE, ext. 7 (Toll Free) or visit www.catscaleguarantee.com
for instructions.
3) IMMEDIATELY send a copy of the citation, CAT Scale Ticket, your name, company, address, and phone number to
CAT Scale Company Attn: Guarantee Department.
The four weights shown below are separate weights. The GROSS WEIGHT is the CERTIFIED WEIGHT
and was weighed on a full length platform scale. All weights are guaranteed by CAT Scale.
DATE: o—ub- 2:5
14:33 SCAM:
LOCATION:
PUBLIC WEIGHMASTEWS
CERTIFICATE OF
WEIGHT& MEASURE
1 � �
r I't78LIG 5
I WEIGHMASTER •'
47
,r
WEIGH NUMBER
? tDf % (D
695
PILOT TRAVEL CE14TERS
1 95 EXIT 71
SAL. I SHURY NC
4i"EER A,,' LE
LCNE ABLE
rRAII ER AXLE
2 GROSS WEIGHT
-L ")2(D10 1 t)
30160 1 b
2 1-7' .1 4 C-) 1 b
(�:a 9 1-5 [=] C> 1 (ram
This is to certify that the following described merchandise was weighed, counted, or measured by a
public or deputy weighmaster, and when properly signed and sealed shall be prima facia evidence of the
accuracy of the weight shown as prescribed by law.
LIVESTOCK, PRODUCE, PROPERTY, COMMODITY, OR ARTICLE WEIGHED h RE I GHT ALL KINDS
COMPANY EV TRACTOFI,p L0 TRAILER A 545
711
WEIGHMASTER OR I I ] : ;, ! � TICKET # OF
FEE WEIGHER SIGNATURE S A" s f a,�
/ uS ti �',. i "4�V I FULL $ WEIGH
1 _ (IF REWEIGH)
�TOMER COPY 0CAT scade+Rog "l 11122
2 7,-/

� Scale Ticket
This is to certify that the following described merchandise was weighed, counted, or measured by a public or deputy weighmaster,
and when properly signed and sealed shall be prima facia evidence of the accuracy of the weight shown as prescribed by law.
Jun 06 2023
Ticket : 8394
Cust. Name:
Truck ID: 215
Trailer ID: 315
Reweigh Fee 3.50
Quiktrip 1044
2790 Lane St
Kannapolis, NC 28083
Axle 1 : 10100 lb
Axle 2 : 32100 lb
Axle 3 : 32640 lb
Total : 74840 lb
NORQU*TOO'
PUBLIC WEIGHMASTER
NSE EXPIRES JUNE 30, 2023
COREY ALVE SON 41656
WEIGHMASTER OR
WEI"ZA
INVALID N
DRIVER IN TRUCK
HERE:
PUBLIC WEIGHMASTER'S
CERTIFICATE OF
WEIGHT & MEASURE
IMPRINT SEAL HERE
(IF APPLICABLE)
FULL WEIGH
TICKET N
(IF REWEIGH)

THE CAT_ SCALE_ GUARANTEE
The CAT Scale Company guarantees that our scales will give an accurate weight, What makes
us different from other scale companies is that we back up our guarantee with cash 0,
WEIGH WHAT WE SAY OR WE PAY't`'
If you get an overweight fine from the state AFTER one of our CAT Scales showed a legal weight, we will
immediately check our scale and we will:
(1) Reimburse you for the cost of the overweight fined our scale is wrong, OR
(2) A representative of CAT Scale Company will appear in court WITH the driver as an expert witness if we
believe our scale was correct.
IF YOU SHOULD GET AN OVERWEIGHT FINE, YOU SHOULD DO THE FOLLOWING TO GET THE PROBLEM RESOLVED:
1) Post bond and request a court date.
2) Call CAT Scale Company direct 24 hours a day at 1-877-CAT-SCALE, ext. 7 (Toll Free) or visit www.catscaleguarantee.com
for instructions.
3) IMMEDIATELY send a copy of the citation, CAT Scale Ticket, your name, company, address, and phone number to
CAT Scale Company Attn: Guarantee Department.
CAT SCALE COMPANY
P0. BOX 634
WALCOTT, IA 52773
(87-7) 228-7225
www,catscale.com DATE:
09: 42 SCALE:
LOCATION:
PUBLIC WEIGHFMASTEWS
CERTIFICATE OF
WEIGHT & MEASURE
CA P
f 1'�1RLfG - 1
i :WE.IGHMASTER" t
WE I GH NUMBER
The four weights shown below are separate weights. The GROSS WEIGHT is the CERTIFIED WEIGHT
and was weighed on a full length platform scale. All weights are guaranteed by CAT Scale.
to --0 7 --- 2'y
t95
PILOT TRAVEL CENTERS
I 85 EXIT 71
SALISBURY NC
41.E A. ;LE
Cgb'E 0LE
IRaTEP, P-"J E
* �-ROS3S WEIGH
1. ""eat() 1 b
3 -3- V 1 L�
3 (. -
c 1 b
7�-51.�U 1 to
This is to certify that the following described merchandise was weighed, counted, or measured by a
public or deputy weighmaster, and when properiy signed and seated shall be prima facia evidence of the
accuracy of the weight shown as prescribed by law.
LIVESTOCK, PRODUCE, PROPERTY, COMMODITY, OR ARTICLE WEIGHED r RE i GMT HLL KINDS
COMPANY fiRACTCIR�._ 216 TRAILER # 3$ 5
WEIGHMASTER OR _ TICKET # OF
FEE $4.00 WEIGHERSIGNATURE _' l � FULL $WEIGH 1069523157570
(IF REWEIGH)
0 CAT Scale* Reg W81 I I M

T,HE CAT SCARF. 91JARANTEE
The CAT Scale Company guarantees that our scales will give an accurate weight. What makes
us different from other scale companies is that we back up our guarantee with cash m
WEIGH WHAT WE SAY OR WE PAYt
If you get an overweight fine from the state AFTE13 one of our CAT Scales showed a legal weight, we will
immediately check our scale and we will:
(1) Reimburse you for the cost of the overweight fine if our scale is wrong, OR
(2) A representative of GAT Scale Company will appear in court WITH the driver as an expert witness if we
believe our scale was correct.
IF YOU SHOULD GET AN OVERWEIGHT FINE, YOU SHOULD DO THE FOLLOWING TO GET THE PROBLEM RESOLVED:
1) Post bond and request a court date.
2) Call CAT Scale Company direct 24 hours a day at 1-877-CATSCALE, ext. 7 (Toll Free) or visit www.catscaleguarantee,com
for instructions.
3) IMMEDIATELY send a copy of the citation, CAT Scale Ticket, your name, company, address, and phone number to
CAT Scale Company Attn: Guarantee Department.
DATE
1 2 : 59 SCALE:
LOCATION:
PUBLIC WEIGHNASTEWS
(ERTIFICATE OF
WEIGHT & MEASURE
XiACArio
J • • i'L18LtC �
I - WFJGHMA5TER
1
k
WEIGH NUMBER
0621
TOMER COPY
7 / Ste/
' The four weights shown below are separate weights. The GROSS WEIGHT is the CERTIFIED WEIGHT
and was weighed an a full length platform scale. All weights are guaranteed by CAT Scale.
b—u7-23
695
PILOT TRAVEL.. CENTERS
I 85 EXIT 71
SAL. I SBURY NC
''ITEER Ari
TH.e.It.EH A"Xi-E
6RCISS WEiG 4 i
L QC.)2C) 1 b
:2<:;)7C)CD 1 b
�27-7E3CD :I. b
b 7 tD_"(-j 10
This is to certify that the following described merchandise was weighed, counted, or measured by a
public or deputy weighmaster, and when properly signed and sealed shall be prima facia evidence of the
accuracy of the weight shown as prescribed by law.
LIVESTOCK, PRODUCE, PROPERTY, COMMODITY, OR ARTICLE WEIGHED F RE I bHT ALL_ k I ND16
COMPANYTRACTOR* 11b TRAILER # 245
WEiGHMASTER OR TICKET * OF
FEE $ WEIGHER SIGNATURE FULLWEIGH
(IF REWEIGH)
© CAT Scale* Reg 3C81 11122

i CKET NUMBER
1069523158653
Ii
CERTIFIED
AUTOMATED
TRUCK
SCALE
THELCAT_SCALE GUARANTEE
The CAT Scale Company guarantees that our scales will give an accurate weight. What makes
us different from other scale companies is that we back up our guarantee with cash,O
WEIGH WHAT WE SAY OR WE PAY®
If you get an overweight fine from the state A_ FTEf one of our CAT Scales showed a legal weight, we will
immediately check our scale and we will:
(1) Reimburse you for the cost of the overweight fine if our scale Is wrong, OR
(2) A representative of CAT Scale Company will appear in court WITH the driver as an expert witness if we
believe our scale was correct.
IF YOU SHOULD GET AN OVERWEIGHT FINE, YOU SHOULD DO THE FOLLOWING TO GET THE PROBLEM RESOLVED-
1 ) Post bond and request a court date.
2) Call CAT Scale Company direct 24 hours a day at 1-877-CAT-SCALE, ext. 7 (Toll Free) or visit www.calsoaleguarantee.com
for instructions.
3) IMMEDIATELY send a copy of the citation, CAT Scale Ticket, your name, company, address, and phone number to
CAT Scale Company Attn: Guarantee Department.
11I,1111Iq
1 b : 45 SCALE,
LOCATION,
PUBLIC WEIGNWASTWS
fERTIFICATE OF
IWEIGHT & MEASURE
f FI16L1C
WE.IGHMASTER 7
WEIGH NUMBER
'The four weights shown below are separate weights. The GROSS WEIGHT Is the CERTIFIED WEIGHT
and was weighed on a full length platform scale. Ail weights are guaranteed by CAT Scale.
b-07-23
655
PILOT TRAVEL CENTERS
I 95 EXIT 71
SALISBURY NC
4TEER AYJ-E -? 9 4 C7 1 b
IDF,1v`E A -',{-LE :2 `=?, E3 8 C7 I b
THAR-ER AXLE 2 9 3 C3 4 1t:3
fiRSSS WEIGHT E3 S' 1 2 4 1 b
This is to certify that the following described merchandise was weighed, counted, or measured by a
public or deputy weighmaster, and when properly signed and sealed shall be prima facia evidence of the
accuracy of the weight shown as prescribed by law,
LIVESTOCK, PRODUCE, PROPERTY, COMMODITY, OR ARTICLE WEIGHED 1-: RE I GH I HLL KINDS
evo
COMPANY
FEE $ 1 3. 50
TRACTOR! )- TRAILER#
WEIGHMASTER OR TICKET # OF
WEIGHER SIGNATURE l� +� ' t'' 4 `� t' (� PULL $ WEIGH
(IF REWEIGH)
.45
�) CAT Scale# Flea 3061 11,72

NON -HAZARDOUS
Load _ _ _ _ faniest No.
77,56
GENERATOR INFORMATION
��TI Chi __._..._. �
W
es
Generator: phone:
r ._
MATERIAL DESCRIPTION l QUANTITY l `'EIGHT
Gross Weight (lbs): 7 /,0'!0 Material: SDII
Empty Weight (lbs): 2 g, 6 7 Contaminant:
Net Weight (lbs)- Z �
Quantity oTonsrtrrs Fails sacs Wards ®then.
TRANSPORTER INFORMATION
Truck #: Contact: .:r _
s the transporter; I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility designate.
Driver Signature:
T > I.
715-71
INMV3
10=55111111
--d the materials described move to this facility, and I hereby accept this
'al ° nner that has been authorized by the Mate of North Carolina.
f
®ate:
.cility
Canarv/Invoice
er

EVO
CORPORATION
1703 Vargrave Street, Winston-Salem, NC 0
NON -HAZARDOUS MATERIALS MANIFEST
Load # _ Manifest No,17
r
57
GENERATOR INFORMATION
„.._............... ....._.._...m._.._..._.____Generator: -IPM Properties Phone: .___-_.________,.,..,.,...._-_......_._.......-.....__.__._._.__._ ._.._.-...� _.,...._.._-_. _................m..�____!
4404 -
3201
Site Address: e
MATERIAL
ATE l L DESCRIPTION / QUANTITY / WEIGHT
------------
Grass Weight (Ibs: Material;
Empty Weight (Ibs). --27�0:..,...,..:, �__. Contaminaft
Net Weight ibsPi080
Quantity b r Tons Drums Pails Sacs Yards Other:
___-__-_.-__-_
TRANSPO TER INFORMATION
'
Transporter: BVO CDrWratiOnPhone3
Truc #--, 2 (tr _
Contact:
s the transporter, i certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce cinder the applicable regulations governing transportation, and i hereby receive this material for
delivery to the facility designate.
Driver Sianature:
_ Efate: �5„ 6-�3
FACILITY INFORMATION
Evo Project i s
her
Contact:
i certify that the carrier has delivered the materials described above to this facility, and i hereby accept this
material for treatment and/or dispos n a manner that has been authorized by the State of North Carolina.
Facility Signature. 6i'` date:
White/Facility Canary/Invoice � Pink/Car

EVO CORPwww.evocorpORATION
NON-HAZARDOUSnet
MATERIALS
Load _ _ Manifest No. 1 51
GENERATOR INFORMATION
Generator: Properties Phone: [phone]
_.
Site Address, 3201 _, s:-
City/State:
._-___.._..-__....-...-_-_.-__ MAT E i DESCRIPTION / 1I EIGHT
Gross Weight (ibs): Material:
Empty Weight (lbs): ��, I� Contaminant:
inant:
Net Weight (ibs): �+
Quantity t Ons Drums Pails Sacs Wards Other,
_..��.TRANSPORTER INFORMATION
Drp _ Phone:3
Truck : A) 7 `" 3 ell Contact: ny Ejsh!ffL_
As the transporter, I certify that the materials described above being slipped € nder this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility designate.
Driver Si€ nature:
_ _ __ Date:,/K __3.
I( -IT NC�lifl i0N
I certify that the carrier has delivered the rnaterials described above to this facility, and I hereby accept this
material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
FacilitySignature- tD_�_Gate: 61;5� kpo
acility
3 _,1, Como, ti=.,r . 2010
Canary/invoice
er

EVO CORPORATION
NON -HAZARDOUS MATERIALS MANIFEST
Load # _ _ Manifest No. 1-1759
GENERATOR INFORMATION
_ -----------
IPM ie -
Generator- Phone:
4404
Site Address:
. —Q.
ad
City/State:
-.________---_._.-_W_.-_.___.__-___------_____ TE��_�
IAL DESCRIPTION ]QUANTITY f WEIGHT I
Gross Weight (Ibs
Empty Weight (Ibs)
Net' eight (ibs):
Quantity
Material:
Contaminant:
Tons Drums Pails Sacs Yards Other:
TRANSPORTER INFORMATION —
r Cbrporation
Truck #: 2,16- 3q.� Contact;
As the transporter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility designate.
A1k
--Driver ;c nadir _. _ � Date:
� ___ FACILITYINFORMATION
r.i.
Wm8toll-BallcemM- 2.7107
Evo Project :
Phone:
Contact:
I certify that the carrier has delivered the materials described above to this facility, and i hereby accept this
material for treatment and/or disposal in a manner that has been authorized by the Mate of North Carolina.
Facilitv Siqnature:_ _ ��-� _._ _._ Date: _ -
_____._�.�_�___.._.___ White/Facility Canary/invoice �-Pink

EVO CORPORATION
www.evocorp.net
NON -HAZARDOUS MATERIALS MANIFEST
Load _ _ Manifest No.
GENERATOR INFORMATION
Generator: IPM Properties Phone: [phone]
Site Address: ,
o
MATERIAL DESCRIPTIONmt QUANTITY 1 WEIGHT
Grass Weight (lbs): 7�i 920 Material; SDA
Pr pty Weight (Ibs): y ` � c�= Contaminants #2 Phel
Net Weight (lbs):
uantity .7 Ton ®rums Pais Sacs Yards Other:
TRANSPORTER INFORMATION
Transporter.,
Phoned336-725-5944
Truck ##: 16-31/- Contact.
As the transporter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility designate,
Driver Sianaturee
W-aneten-Salle-inN_ W2 °
Date:
FACILITY INFORMATION
i certify that the carrier has delivered the materials described above to this facility, and i hereby accept this
material for treatment andlor disposal in a manner that has been authorized by the Mate of North Carolina.
Facility ionature:
Gate: -,--; ---- —
W
acility
nvoice Pink/Carrier

EVO CORPORATION
Winston-Salem,
0
www.evocorp.net
NON -HAZARDOUS MATERIALS MANIFEST
Load Manifest No. 17763
___._ ___.__-._..-._._._-_ _ _----------
---
GENERATOR INFORMATION
Generator: Phone: [phone]
Site Address:
Charlotte,; _ More
---------- _-_____---
MATERIAL DESCRIPTION IPTION /QUANTITY / WEIGHT
Cross Weight (Ibs): � 20 Material, SOR
Empty Weight (lbs): Z'� L166 Contaminant: #2 Fad Oil
Net Weight (ibs): ��Yt 66
Quantity 31-33 can Drums Pails Sacs `bards Other:
TRANSPORTER INFORMATION
---------------
vo Cbrporation:
Truck : Z} 4 -3 4S Contact: , n
As the transporter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility designate,
Driver Signature:
Date:
FACILITY INFORMATION
ATION
2
1 certify that the carrier has delivered the materials described above to this facility, and l hereby accept this
material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Fablit ianat re:L 61 k�5
� � /'� ___-P Date-
White/Facility Canary/Invoice Pink/Carrier

�� ee
fr
NON-HAZARDOUSMATERIALS
-r,
Generator, Irm
Site Address: '
—Charlotte, ic
Manifest No
GENERATOR INFORMATION
Phone- 704-302-4444
MATERIAL DESCRIPTION / QUANTITY / WEIGHT
Gross Weight (Ibs)- rraq UMaterial: SDil
Empty Weight lbs): � �� ' Contaminant:
Net le9ght(ibs): SQ)QSO
Quantity 1 VY L Drums Pails Sacs Yards Other:
fr
TRANSPORTER INFORMATION
Phone: [phone]
As the transporter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility designate.
Driver Signature: Date:'
FACILITY INFORMATION
Evo Omporation
Evo Prefect
#336-725-5844
Phone:
WMston- r
Contact:
I certify that the carrier has delivered the materials described above to this facility, and l hereby accept this
material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility rat are: Date:
m White/Facility Canary/Invoice Pink/Carrier
,....r inn, 210IN,

Foss Recycling Winston Salem
3459 Thomasville Road
Winston-Salem, NC 27107
Phone : [phone]
DISHER TON'Y'
EVO TRUCKING
WINSTON SALEM NC
�c� 01io o
217 - 3
SCALE TICKET
Ticket No. 16891788 Scale: 88
In 08 Jun 2023 2:04 pm
Supplier-# DISO40
Plate No. : £VO
Vehicle WRITE TR. 217
Served By rgonzales
Material Gross Tare: Wt Add Net weight
CATCH WEIGHTS 74,080 74,080 LBS
Continents: paid $5
PURL EIGHMAS R
il'&ALID
NS PI S JUN
Q � 42941
UNLESS SIGNED
Mission: Excellence in Recycling
Core Values: Honesty/Integrity,
Customer Experience, Hardworking,
Accountability
s
Asperational Value: Glorify God By

i 1CXET NUMEER
106952315970
Ae
I,1
CERTIFIED
AUTOMATED
TRUCK
SCALE
THE -CAT -SCALE GUARANTEE
The CAT Scale Company guarantees that our scales will give an accurate weight. What makes
us different from other scale companies is that we back up our guarantee with cash,O
WEIGH WHAT WE SAY OR WE PAY®
If you get an overweight fine from the state AFC ER one of our CAT Scales showed a legal weight, we will
immediately check our scale and we will:
(1) Reimburse you for the cost of the overweight fine it our scale is wrong, OR
(2) A representative of CAT Scale Company will appear in court WITH the driver as an expert witness if we
believe our scale was correct.
IF YOU SHOULD GET AN OVERWEIGHT FINE, YOU SHOULD DO THE FOLLOWING TO GET THE PROBLEM RESOLVED:
1) Post bond and request a court date.
2) Call CAT Scale Company direct 24 hours a day at 1-A77-CATSCALE, ext. 7 (Toll Free) or visit www.catscaleguarantee.com
for instructions.
3) IMMEDIATELY send a copy of the citation, CAT Scale Ticket, your name, company, address, and phone number to
CAT Scale Company Attn. Guarantee Department.
DATE
16:41 SCALE:
LOCATION:
PUULIC WEIGTlMASTEWS
TFRTIF1CAiF OF
WTILNT & MEASURE
,--
l `
:WEIGHmA5'Tr=R' t
1
WEIGH NUMBER
8b53
iMER COPY
/7 75'7
*The four weights shown below are separate weights. The GROSS WEIGHT Is the CERTIFIED WEIGHT
and was weighed on a full length platform scale. All weights are guaranteed by CAT Scale.
b--OB—G3 ti1FER Arm
1Lip'lic A :.E
695
PILOT TRAVEL CENTER iRafE_'n-R
1 85 EX 1'T 71
SALISBURY NC
1L(D �2�2 C—) 1 b
=� J-
-i 6-, t5 4(Lj 1 b
This is to certify that the following described merchandise was weighed, counted, or measured by a
public or deputy weighmaster, and when properly signed and seated shall be prima facia evidence of the
accuracy of the weight shown as prescribed by law.
LIVESTOCK, PRODUCE, PROPERTY, COMMODITY, OR ARTICLE WEIGHED FREIGHT ALL KINDS
EVE) 21345
COMPANY I TRACTOR # _ TRAILER#'
= 1 f F
WEIGHMASTER OR TICKET # OF
PEE WEIGHER SIGNATURE f =f � �� ,ii"{ , r /i, I �� � rf' � ! FULL S WEIGH 169523159653
s4.00 ` (IF REWEIGH) -
0 GAT Scale* Reg 3081 1122

Lj
Truck ID: 217
Trailer ID: 341
Weigh Fee: 13.00
Quiktrip 1044
2790 Lane St
Kannapolis,NC 28083
Axle 1 : 9900 lb
Axle 2 : 34800 lb
Axle 3 : 29560 lb
Total : 74260 lb
Scale Ticket
PUBLIC WEIGHMASTER
NSE EXPIRES JUNE 30, 2023
COREY ALVER 0 41656
WEIGHMASTER OR
WEI
INVALl0 �S IGIvED
DRIVER IN TRUCK U ES HECKED HERE:
IMPRINT SEAL MERE
(IF APPLICABLE)
FULL WEIGH
TICKET k
{IF REWEIGH}

HKET Nllf EER
iA645T�I8�i2t
I,l
CERTIFIED
AUTOMATED
TRUCK
SCALE
THE CAT SCALE GUARANTEE
The CAT Scale Company guarantees that our scales will give an accurate weight. What makes
us different from other scale companies is that we track up our guarantee with cash
WEIGH WHAT WE SAY OR WE PAYt N
If you get an overweight tine from the state AFTER one of our CAT Scales showed a legal weight, we will
immediately check our scale and we will-
(1) Reimburse you for the cost of the overweight fine if our scale Is wrong, OR
(2) A representative of CAT Scale Company will appear in court WITH the driver as an expert witness if we
believe our scale was correct.
IF YOU SHOULD GETAN OVERWEIGHT FINE, YOU SHOULD DO THE FOLLOWING TO GET THE PROBLEM RESOLVED:
1) Post bond and request a court date.
2) Call CAT Scale Company direct 24 hours a day at 1-877-CAT-SCALE, ext. 7 (Toll Free) or visit www.catsGaleguarantee.com
for instructions.
3) IMMEDIATELY send a copy of the citation, CAT Scale Ticket, your name, company, address, and phone number to
CAT Scale Company Attn: Guarantee Department.
The four weights shown below are separate weights. The GROSS WEIGHT is the CERTIFIED WEIGHT
and was weighed on a full length platform scale. All weights are guaranteed by CAT Scale.
DATE: (n-09—, ",
09 ; O3 SCALE:
LOCATION:
PUBLIC WEIGRMASTEWS
CERTIFICATE OF
VIIIGIiT at NEA0RE
1 �
r IGLIC +<
t ;YUEIGHMAS ER' }
t !
WEIGH NUMBER
C)72AL
695
PILOT TRAVEL CENTERS
i 85 EXIT 71
SAL I SBURY NC
^" ER AXL
Tf'a I ram• A-/i-F
" 6HOSS WEIGHT
1_ C) V 2 [J 1 t:D
7 ea 16a V [T3 1-0
This is to certify that the following described merchandise was weighed, counted, or measured by a
public or deputy weighmaster, and when properly signed and sealed shall be prima facia evidence of the
accuracy of the weight shown as prescribed by law.
LIVESTOCK, PRODUCE, PROPERTY, COMMODITY, OR ARTICLE WEIGHED F• RF 16H T HL_L K I N t75
E V
COMPANY TRACTOR # �6 J$
TRAILER #
WEIGHMASTER OR -_ i 4. TICKEI Y OF
FEE .� WEIGHER SIGNATURE Ri: l f FULL$ WEIGH
(IFREWEIGH)
FOMEH COPY © GAT scaWReg 30811M22
>>sq

11CKET NUK8EA
069523160735
®®
Gl
CERTIFIED
AUTOMATED
TRUCK
SCALE
THE CAT SCALE GUARANTEE,
The CAT Scale Company guarantees that our scales will give an accurate weight. What makes
us different from other scale companies is that we back up our guarantee with cash.`
WEIGH WHAT WE SAY OR WE PAYS
If you get an overweight fine from the state AFTER one of our CAT Scales showed a legal weight, we will
immediately check our scale and we will:
(1) Reimburse you for the cost of the overweight fine if our scale is wrong, OR
(2) A representative of CAT Scale Company will appear in court WITH the driver as an expert witness if we
believe our scale was correct.
IF YOU SHOULD GET AN OVERWEIGHT FINE, YOU SHOULD DO THE FOLLOWING TO GET THE PROBLEM RESOLVED:
1) Post bond and request a court date.
2) Call CAT Scale Company direct 24 hours a day at 1-877-CATSCALE, ext. 7 (Toll Free) or visit www.catscaleguaranteo.com
for instructions.
3) IMMEDIATELY send a copy of the citation, CAT Scale Ticket, your name, company, address, and phone number to
CAT Scale Company Attn: Guarantee Department.
The four weights shown below are separate weights. The GROSS WEIGHT is the CERTIFIED WEIGHT
and was weighed on a full length platform scale. All weights are guaranteed by CAT Scale.
DATE: h-01` 3
12.21 SCALE:
LOCATION:
PUPLIC WEIGHHAST[WR
CERTIFICATE OF
VrEIGHT $ HEASUU
GA r
! f"118LiC {
f=WFEGHMASTF-R i
1� •'1 ,- art
� r f
w
WEIGH NUMBER
b95
P1LOi' TRF�VEL CENTERS
1 85 i X 1'T 71
SOL I SBURY WC.
i-7' C? C) Ca 1 b
= 1-HOBS WF:!;H i 4 1' 1 iJ
This is to certify that the following described merchandise was weighed, counted, or measured by a
public or deputy weighmaster, and when properly signed and sealed shall be prima facia evidence of the
accuracy of the weight shown as prescribed by law.
LIVESTOCK, PRODUCE, PROPERTY, COMMODITY, OR ARTICLE WEIGHED t-RE I GHT ALL IC 1 IVLiS
COMPANY TRACTOR*
345
TRACTOTRACTOR*11b TRAILER,#
FEE WEIGHER SSIIGNATURE +•�" w �- pia _ f'~ �1 � TIL L $ WEIGH
F 1069523160721
FULL. s wEiGH
s4.CJU Imo`., _�.Z's \, ^��--t- i(IFREWEfGH)
TOMEPR COY cc) CAT Scala+ Reg3Wt 11,22
r7 " /�l I

i;Ci ET NUMBER
1069523160746
! do
I1
CERTIFIED
AUTOMATED
TRUCK
SCALE
JOE CAT SCALE GUARANTEE
The CAT Scale Company guarantees that our scales will give an accurate weight. What makes
us different from other scale companies is that we back up our guarantee with cash.m'
WEIGH WHAT WE SAY OR WE PAYS
It you get an overweight fine from the state AFTER one of our CAT Scales showed a legal weight, we will
immediately check our scale and we will:
(1) Reimburse you for the cost of the overweight tine if our scale is wrong, OR
(2) A representative of CAT Scale Company will appear in court WITH the driver as an expert witness if we
believe our scale was correct.
IF YOU SHOULD GET AN OVERWEIGHT FINE, YOU SHOULD DO THE FOLLOWING TO GET THE PROBLEM RESOLVED:
1) Post bond and request a court date.
2) Call CAT Scale Company direct za hours a day at 1-877-CATSCALE, ext. 7 (Tall Free) or visit www.Galscaleguarantee.com
for instructions.
3) IMMEDIATELY send a copy of the citation, CAT Scale Ticket, your name, company, address, and phone number to
CAT Scale Company Attn: Guarantee Department.
DATE
15.41 SCALE:
LOCATION:
PUBLIC WEILHHASTER S
CERTIFICATE OF
EIGHT I MEASURE
r b1 G�41rt'
t WEfGHMA,9TER- I
it - F
WE I GH €IUM13ER
* The four weights shown below are separate weights. The GROSS WEIGHT is the CERTIFIED WEIGHT
and was weighed on a full length platform scale. All weights are guaranteed by CAT Scale,
b—u9--23
6 y ID
PILOT TRAVEL CEIATERS
I 05 EXIT 71
SAL I SBURY NC
1'111 EER AXIl -
UPS EA"�11F
�Pr- �1�1' A_>;"-E
F `t7 I H7
V9v() 1 tD
:-f� ��40 1 tD
._s c.-�) "" (-�) I t-,)
76112C�) 1 to
This is to certify that the following described merchandise was weighed, counted, or measured by a
public or deputy weighmaster, and when properly signed and sealed shall be prima facia evidence of the
accuracy of the weight shown as prescribed by law.
WESTOCK, PRODUCE, PROPERTY, COMMODrTY, OR ARTICLE WEIGHED FREIGHT ALL K I IVDS
O COMPANY TRACTOR # -- TRAILER 05 4 5
WEIGHMASTER ORV TICKET # OF
FEE ,z4 . UU WEIGHER SIGNATURE rk FULL $ WEIGH 1Jb4523160721
- — (IF REWEIGH)
C CAT Scale* Reg 3081 1 1l22

Scale Ticket 0f j`jr)
This is to certify that the following described merchandise was weighed, counted, or measured by a public or deputy weighmaster,
and when properly signed and sealed shall be prima facia evidence of the accuracy of the weight shown as prescribed by law.
Jun 12 2023
Ticket : 8420
Cust. Name: EVO
Truck ID: 222
Trailer ID:
Reweigh Fee 4.00
Quiktrip 1044
2790 Lane St
Kannapolis, NC 28083
Axle 1 :
9760
lb
Axle 2 :
37240
lb
Axle 3 :
37220
lb
Total :
84240
lb
UUIKinp
NOR I H CAROLrINA
EUBLIC WEIGHMASTER
JSE EXPIRES JUNE 30 2023
COREY ALVER6
WEIGHMASTER OR /J
WEIGHER SIGNATURE
DRIV
1 7 Co �f
PUBLIC WEIGHMASTER'S
CERTIFICATE OF
WEIGHT & MEASURE
IMPRINT SEAL HERE
(IF APPLICABLE)
FULL WEIGH
TICKET n
{IF REWEIGH)

XIC3
C0RP©RAT10N
1703 Vargrave Street
Winston-Salem, NC 27107
ph 336.725-5844
fax [phone]
Evo Corporation does hereby certify that I0.17 tons of non -hazardous
contaminated material received on 8!1412023 from:
Generator: TPM Properties
Originating at: 3201 Tuckaseegee Road
Charlotte, NC
EC Waste ID 4: 062310
has been disposed of by Evo Corporation in a manner approved by the North
Carolina Department of Environmental Quality.
Signature
Thomas W. Hammett
CEO
Evo Corporation
www.evoeorp net

1703 Vargrave Street, Winston-Salem, NC EVO CORPORATION
www.evocorp.net
NON -HAZARDOUS MATERIALS MANIFEST
Load # Manifest No. 2 0 1'5
GENERATOR INFORMAT�ON
Generator: Phone: [phone]
Site Address;
ATElL DESCRIPTION i QUANTITY 1 WEIGHT
Grass Weight (ibs): ` Material:
Empty Weight (lbs): 51 L1q 6 Contaminant:
Net Weight (lbs):
Quantity � � � � c�r�s Drums Pails Sacs Yards Gather:
v
TRANSPORTE
INFORMATION
Transporter-
Bro o
Truck : Contact:
As the transporter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable` guiations governing transportation, and ( hereby receive this material for
delivery to the facility designate. I/
i certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment andlor disposal in a manner that has been authorized by the State of North Carolina.
Paility Sisnatrr' `�> Date:
White/Facility
v.:v0 (_=.P: St17 .:: ivn. 20(N
arynnvc
Pink/Carrier

Foss Recycling Winston Salem
34-59 Thomasville Road
Winston-Salem, NC 27107
phonc� : (336) -W-9122
DISHER TONY
EVO TRUCKING
WINSTON SALEM NC
T-,cket No. 16957069 Scale: 88
In 14 Aug 2023 2:21
Supplier-4 DIS040
Plate Noc Edit?
Vehicle WHITE TR. 216
Served By rgonzales
Material
Gross Tare Wt Adj Net Weight
CATCH WEIGHTS 51.,780 51,780 LBS
NORTH CAROLUNA
PUBLIC WEIG
2023
LICEN E EXPIREs
CHSFT:IrLp 46523
IF17 - --
INVALID UNLESS SIGNED
pm
Mission: Excellence iq Recycling
Core Valueo: Honesty/lntegrty,
Customer Experience, Hardworking,
Accountability
Asperatio"al value: Glorify God By

Appendix B
Laboratory Analytical Reports
hart '+ hickman
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/TPM Properties Limited Partnership/Report/48982 CA ILW20231011.doc
SMARTER ENVIRONMENTAL SOLUTIONS

Waypointo
ANALYTICAL
6/21 /2023
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 23-163-0001
Client Project Description: TPM-001
Dear Steve Libbey:
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Waypoint Analytical, LLC (Charlotte) received sample(s) on 6/9/2023 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
a'-1
Angela D Overcash
Senior Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 229

Waypoint.0
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State
Program
Lab ID
Expiration Date
North Carolina
State Program
37735
07/31/2023
North Carolina
State Program
402
12/31/2023
South Carolina
State Program
99012
07/31/2023
South Carolina
State Program
99012
12/31/2022
Page 1 of 1 00016/23-163-0001
Page 2 of 229

Waypoint.(2)
ANALYTICAL
Report Number: 23-163-0001
Client Project Description: TPM-001
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Sample Summary Table
Lab No Client Sample ID Matrix Date Collected Date Received
98043
EX-1
Solids
06/06/2023
11:30
06/09/2023
16:22
98044
EX-2
Solids
06/06/2023
11:35
06/09/2023
16:22
98045
EX-3
Solids
06/06/2023
15:30
06/09/2023
16:22
98046
EX-4
Solids
06/06/2023
15:40
06/09/2023
16:22
98047
EX-5
Solids
06/07/2023
08:05
06/09/2023
16:22
98048
EX-6
Solids
06/07/2023
08:20
06/09/2023
16:22
98049
EX-7
Solids
06/07/2023
11:30
06/09/2023
16:22
98050
EX-8
Solids
06/07/2023
11:45
06/09/2023
16:22
98051
EX-9
Solids
06/07/2023
14:10
06/09/2023
16:22
98052
EX-10
Solids
06/07/2023
14:15
06/09/2023
16:22
98053
EX-11
Solids
06/07/2023
14:20
06/09/2023
16:22
98054
EX-12
Solids
06/07/2023
15:35
06/09/2023
16:22
98055
EX-13
Solids
06/07/2023
15:40
06/09/2023
16:22
98056
EX-14
Solids
06/07/2023
15:45
06/09/2023
16:22
98057
EX-15
Solids
06/07/2023
16:15
06/09/2023
16:22
98058
EX-16
Solids
06/08/2023
17:00
06/09/2023
16:22
98059
EX-17
Solids
06/08/2023
17:10
06/09/2023
16:22
98060
UST-1-A
Solids
06/08/2023
13:45
06/09/2023
16:22
98061
UST-1-13
Solids
06/08/2023
13:55
06/09/2023
16:22
98062
UST-2-A
Solids
06/08/2023
16:00
06/09/2023
16:22
98063
UST-2-13
Solids
06/08/2023
14:00
06/09/2023
16:22
98064
UST-2-C
Solids
06/08/2023
17:35
06/09/2023
16:22
98065
UST-2-D
Solids
06/08/2023
15:50
06/09/2023
16:22
98066
UST-2-E
Solids
06/08/2023
15:40
06/09/2023
16:22
98067
UST-2-F
Solids
06/08/2023
17:45
06/09/2023
16:22
98068
UST-3-A
Solids
06/08/2023
16:10
06/09/2023
16:22
98069
UST-3-13
Solids
06/08/2023
16:50
06/09/2023
16:22
Page 3 of 229

Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointana lyti ca I som
Sample Summary Table
Report Number: 23-163-0001
Client Project Description: TPM-001
Lab No Client Sample ID Matrix Date Collected Date Received
98070
UST-1-C
Solids
06/09/2023
14:45
06/09/2023
16:22
98071
UST-1-D
Solids
06/09/2023
14:30
06/09/2023
16:22
98072
UST-1-E
Solids
06/09/2023
15:00
06/09/2023
16:22
98073
UST-1-F
Solids
06/09/2023
13:55
06/09/2023
16:22
98074
UST-1-G
Solids
06/09/2023
11:40
06/09/2023
16:22
98075
UST-1-1-1
Solids
06/09/2023
14:20
06/09/2023
16:22
98076
UST-1-I
Solids
06/09/2023
15:10
06/09/2023
16:22
98077
UST-1-3
Solids
06/09/2023
14:05
06/09/2023
16:22
98078
UST-1-K
Solids
06/09/2023
14:35
06/09/2023
16:22
Page 4 of 229

(2)
Waypoint. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointana lyti ca I som
Summary of Detected Analytes
Project: TPM-001
Report Number: 23-163-0001
Client Sample ID Lab Sample ID
Method Parameters Result Units Report Limit Analyzed Qualifiers
EX-1
V 98043
SW-DRYWT
Moisture
36.7
%
06/12/202317:50
EX-2
V 98044
8015C DRO
Diesel Range Organics (C10-C28)
24.7
mg/Kg -
dry
12.0
06/15/2023 19:14
SW-DRYWT
Moisture
16.9
%
06/12/202317:50
EX-3
V 98045
8015C DRO
Diesel Range Organics (C10-C28)
142
mg/Kg -
dry
13.5
06/15/2023 19:35
8015C GRO
Gasoline Range Organics (C6-C10)
235
mg/Kg -
dry
67.4
06/12/2023 22:42
SW-DRYWT
Moisture
25.8
%
06/12/202317:50
EX-4
V 98046
SW-DRYWT
Moisture
26.0
%
06/12/202317:50
EX-5
V 98047
SW-DRYWT
Moisture
39.2
%
06/12/202317:50
EX-6
V 98048
SW-DRYWT
Moisture
24.0
%
06/12/202317:50
EX-7
V 98049
SW-DRYWT
Moisture
27.3
%
06/12/202317:50
EX-8
V 98050
8260D
Naphthalene
0.027
mg/Kg -
dry
0.013
06/12/2023 22:22
8260D
1,2,4-Trimethyl benzene
0.026
mg/Kg -
dry
0.006
06/12/2023 22:22
8260D
o-Xylene
0.010
mg/Kg -
dry
0.006
06/12/2023 22:22
8260D
m,p-Xylene
0.013
mg/Kg -
dry
0.013
06/12/2023 22:22
8260D
Xylene (Total)
0.024
mg/Kg -
dry
0.006
06/12/2023 22:22
SW-DRYWT
Moisture
28.0
%
06/12/202317:50
EX-9
V 98051
SW-DRYWT
Moisture
23.4
%
06/12/202317:50
EX-10
V 98052
SW-DRYWT
Moisture
31.0
%
06/13/202316:32
EX-11
V 98053
SW-DRYWT
Moisture
29.7
%
06/13/202316:32
Page 5 of 229

Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointana lyti ca I som
Summary of Detected Analytes
Project: TPM-001
Report Number: 23-163-0001
Client Sample ID Lab Sample ID
Method Parameters Result Units Report Limit Analyzed Qualifiers
EX-12
V 98054
8015C DRO
Diesel Range Organics (C10-C28)
SW-DRYWT
Moisture
EX-13
V 98055
8015C DRO
Diesel Range Organics (C10-C28)
SW-DRYWT
Moisture
EX-14
V 98056
8015C DRO
Diesel Range Organics (C10-C28)
SW-DRYWT
Moisture
EX-15
V 98057
SW-DRYWT
Moisture
EX-16
V 98058
8015C GRO
Gasoline Range Organics (C6-C10)
SW-DRYWT
Moisture
EX-17
V 98059
SW-DRYWT
Moisture
UST-1-A
V 98060
8015C DRO
Diesel Range Organics (C10-C28)
8015C GRO
Gasoline Range Organics (C6-C10)
SW-DRYWT
Moisture
UST-1-13
V 98061
8015C DRO
Diesel Range Organics (C10-C28)
8015C GRO
Gasoline Range Organics (C6-C10)
SW-DRYWT
Moisture
UST-2-A
V 98062
8015C DRO
Diesel Range Organics (C10-C28)
SW-DRYWT
Moisture
UST-2-13
V 98063
8015C DRO
Diesel Range Organics (C10-C28)
8015C GRO
Gasoline Range Organics (C6-C10)
SW-DRYWT
Moisture
27.9 mq/Kq - dry 14.0 06/15/2023 22:05
28.6 % 06/13/202316:32
124 mq/Kq - dry 14.4 06/15/2023 22:26
30.6 % 06/13/202316:32
26.0 mq/Kq - dry 16.6 06/15/2023 22:48
39.7 % 06/13/202316:32
21.3 % 06/13/202316:32
150 mg/Kg - dry 72.9 06/12/2023 23:10
31.4 % 06/13/202316:32
26.5 % 06/13/202316:32
18100 mq/Kq - dry 5630 06/16/2023 11:14
895 mg/Kg - dry 70.3 06/12/2023 23:38
28.9 % 06/13/202316:32
7450 mg/Kg - dry 2740 06/16/2023 11:36
827 mg/Kg - dry 68.5 06/13/2023 00:06
27.0 % 06/13/202316:32
160 mq/Kq - dry 14.7 06/16/2023 02:00
31.9 % 06/13/202316:32
43900 mq/Kq - dry 10800 06/16/2023 11:57
21.5 mg/Kg - dry 6.76 06/12/2023 21:46
26.0 % 06/13/202316:32
Page 6 of 229

Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointana lyti ca I som
Summary of Detected Analytes
Project: TPM-001
Report Number: 23-163-0001
Client Sample ID Lab Sample ID
Method Parameters Result Units Report Limit Analyzed Qualifiers
UST-2-C
V 98064
SW-DRYWT
Moisture
25.6
%
06/13/2023 16:32
UST-2-13
V 98065
MADEP-EPH
Aromatic C11-C22
131
mg/Kg -
dry
73.5
06/20/2023 15:55
SW-DRYWT
Moisture
31.8
%
06/13/2023 16:32
UST-2-E
V 98066
SW-DRYWT
Moisture
28.5
%
06/13/2023 16:32
UST-24
V 98067
MADEP-EPH
Aliphatic C9-C18
218
mg/Kg -
dry
77.9
06/20/2023 16:32
MADEP-EPH
Aliphatic C19-06
93.1
mg/Kg -
dry
77.9
06/20/2023 16:32
MADEP-EPH
Aromatic C11-C22
224
mg/Kg -
dry
77.9
06/20/2023 16:32
SW-DRYWT
Moisture
36.1
%
06/13/2023 16:32
UST-3-A
V 98068
SW-DRYWT
Moisture
31.6
%
06/13/2023 16:32
UST-3-13
V 98069
8015C DRO
Diesel Range Organics (C10-C28)
18.9
mg/Kg -
dry
18.3
06/16/2023 03:05
SW-DRYWT
Moisture
34.3
%
06/13/2023 16:32
UST-1-C
V 98070
SW-DRYWT
Moisture
26.1
%
06/13/2023 16:32
UST-1-13
V 98071
SW-DRYWT
Moisture
24.8
%
06/13/2023 16:32
UST-1-E
V 98072
SW-DRYWT
Moisture
25.2
%
06/13/2023 16:32
UST-14
V 98073
SW-DRYWT
Moisture
22.8
%
06/13/2023 16:32
UST-1-G
V 98074
8260D
n-Butylbenzene
0.016
mg/Kg -
dry
0.007
06/13/2023 14:17
8260D
sec -Butyl benzene
0.025
mg/Kg -
dry
0.007
06/13/2023 14:17
8260D
4-Isopropyl toluene
0.045
mg/Kg -
dry
0.007
06/13/2023 14:17
8260D
1,2,4-Trimethyl benzene
0.008
mg/Kg -
dry
0.007
06/13/2023 14:17
8260D
1,3,5-Trimethyl benzene
0.056
mg/Kg -
dry
0.007
06/13/2023 14:17
Page 7 of 229

Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointana lyti ca I som
Summary of Detected Analytes
Project: TPM-001
Report Number: 23-163-0001
Client Sample ID Lab Sample ID
Method Parameters Result Units Report Limit Analyzed Qualifiers
UST-1-G
V 98074
8270E
1-Methylnaphthalene
2.98
mq/Kq -
dry
0.959
06/14/2023 23:27
8270E
2-Methylnaphthalene
1.11
mg/Kg -
dry
0.959
06/14/2023 23:27
8270E
Phenanthrene
2.67
mq/Kq -
dry
0.959
06/14/2023 23:27
MADEP-EPH
Aliphatic C9-C18
1060
mg/Kg -
dry
289
06/20/2023 17:08
MADEP-EPH
Aromatic C11-C22
1290
mq/Kq -
dry
289
06/20/2023 17:08
MADEP-VPH
Aliphatic C9-C12
86.2
mg/Kg -
dry
11.6
06/12/2023 22:17
MADEP-VPH
Aromatic C9-Cl0
12.3
mq/Kq -
dry
11.6
06/12/2023 22:17
SW-DRYWT
Moisture
31.1
%
06/13/202316:32
UST-1-1-1
V 98075
SW-DRYWT
Moisture
24.9
%
06/13/202316:32
UST-1-1
V 98076
SW-DRYWT
Moisture
28.8
%
06/13/202316:32
UST-1-J
V 98077
SW-DRYWT
Moisture
20.5
%
06/13/202316:32
UST-1-K
V 98078
SW-DRYWT
Moisture
28.2
%
06/13/202316:32
Page 8 of 229

Waypointo
ANALYTICAL
Client: Hart & Hickman (Charlotte)
Project: TPM-001
Lab Report Number: 23-163-0001
Date: 6/21 /2023
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
CASE NARRATIVE
Massachusetts EPH Method MADEP-EPH
Sample 98074 (UST-1-G)
QC Batch No: V34449
Surrogate(s) flagged for recovery outside QC limits in this project sample due to a required dilution. The dilution
factor resulted in surrogate concentration(s) below the minimum detectable level. Batch QC samples (method
blank and laboratory control samples) all showed surrogates within QC limits.
Total Petroleum Hydrocarbons - Extractable Method 8015C DRO
Sample 98317 (Stockpile)
QC Batch No: V34416/V34381
Surrogate(s) flagged for recovery outside QC limits in this project sample due to a required dilution. The dilution
factor resulted in surrogate concentration(s) below the minimum detectable level. Batch QC samples (method
blank and laboratory control samples) all showed surrogates within QC limits.
Sample 98317 (Stockpile)
QC Batch No: V34416/V34381
The MS/MSD recoveries are outside QC limits due to the level of analyte present in the parent sample relative to
the spike level. RPD is based on the MS/MSD results and should be evaluated as laboratory duplicates.
Sample 98060 (UST-1-A)
QC Batch No: V34417/V34382
Surrogate(s) flagged for recovery outside QC limits in this project sample due to a required dilution. The dilution
factor resulted in surrogate concentration(s) below the minimum detectable level. Batch QC samples (method
blank and laboratory control samples) all showed surrogates within QC limits.
Sample 98061 (UST-1-B)
QC Batch No: V34417/V34382
Surrogate(s) flagged for recovery outside QC limits in this project sample due to a required dilution. The dilution
factor resulted in surrogate concentration(s) below the minimum detectable level. Batch QC samples (method
blank and laboratory control samples) all showed surrogates within QC limits.
Sample 98063 (UST-2-B)
QC Batch No: V34417/V34382
Surrogate(s) flagged for recovery outside QC limits in this project sample due to a required dilution. The dilution
factor resulted in surrogate concentration(s) below the minimum detectable level. Batch QC samples (method
blank and laboratory control samples) all showed surrogates within QC limits.
Semivolatile Organic Compounds - GC/MS Method 8270E
Analyte: 2,4-Dinitrophenol
QC Batch No: V34353/V34327
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference.
Analyte: 2,4-Dinitrotoluene
QC Batch No: V34353/V34327
Page 9 of 229

Waypointo
ANALYTICAL
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference.
Analyte: 2,4-Dinitrotoluene
QC Batch No: V34353/V34327
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: 2,6-Dinitrotoluene
QC Batch No: V34353/V34327
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: 2,6-Dinitrotoluene
QC Batch No: V34353/V34327
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference.
Sample 97822
Analyte: 2-Nitroaniline
QC Batch No: V34353/V34327
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: 2-Nitrophenol
QC Batch No: V34353/V34327
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference.
Analyte: 3-Nitroaniline
QC Batch No: V34353/V34327
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: 4,6-Dinitro-2-methylphenol
QC Batch No: V34353/V34327
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: 4,6-Dinitro-2-methylphenol
QC Batch No: V34353/V34327
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference.
Analyte: 4-Nitroaniline
QC Batch No: V34353/V34327
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference.
Analyte: Hexachlorocyclopentadiene
QC Batch No: V34353/V34327
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference.
Analyte: Nitrobenzene
QC Batch No: V34353/V34327
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Page 10 of 229

Waypointo
ANALYTICAL
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Analyte: Nitrobenzene
QC Batch No: V34353/V34327
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference.
Sample 97822
Analyte: Nitrobenzene-d5
QC Batch No: V34353/V34327
Surrogate(s) was flagged for low recovery in this project sample. This sample will be re -analyzed for verification.
Surrogate Nitrobenzene-d5 was low in the original and the reprep. Second run reported.
Page 11 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98043 Matrix: Solids
Sample ID: EX-1 Sampled: 6/6/2023 11:30
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
36.7 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/12/2317:50 CNC SW-DRYWT
DF Dilution Factor
Page 12 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001
REPOR T OF A NA L YSIS
Lab No : 98043
Matrix: Solids
Sample ID: EX-1
Sampled: 6/6/2023
11:30
Analytical Method: 8015C DRO
Prep Batch(es):
V34381
06/15/23 10:30
Prep Method: 3546
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
<23.7
mg/Kg - dry
23.7
1 06/15/23 18:52 TJW
V34416
Surrogate: OTP Surrogate
71.5
Limits: 31-123% 1 06/15/23 18:52 TJW
8015C DRO
Analytical Method: 8015C GRO
Prep Batch(es):
V34234
06/12/23 08:00
Prep Method: 5035 MED
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
<7.90
mg/Kg - dry
7.90
50 06/12/23 14:43 TBL
V34235
Surrogate: a,a,a-Trifluorotoluene
92.2
Limits: 50-137% 50 06/12/23 14:43 TBL
8015C GRO
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
DF Dilution Factor
Page 13 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98044 Matrix: Solids
Sample ID: EX-2 Sampled: 6/6/2023 11:35
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
16.9 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/12/2317:50 CNC SW-DRYWT
DF Dilution Factor
Page 14 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001
REPOR T OF A NA L YSIS
Lab No : 98044
Matrix: Solids
Sample ID: EX-2
Sampled: 6/6/2023
11:35
Analytical Method: 8015C DRO
Prep Batch(es):
V34381
06/15/23 10:30
Prep Method: 3546
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
24.7
mg/Kg - dry
12.0
1 06/15/23 19:14 TJW
V34416
Surrogate: OTP Surrogate
71.6
Limits: 31-123% 1 06/15/23 19:14 TJW
8015C DRO
Analytical Method: 8015C GRO
Prep Batch(es):
V34234
06/12/23 08:00
Prep Method: 5035 MED
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
<6.02
mg/Kg - dry
6.02
50 06/12/23 15:11 TBL
V34235
Surrogate: a,a,a-Trifluorotoluene
117
Limits: 50-137% 50 06/12/23 15:11 TBL
8015C GRO
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
DF Dilution Factor
Page 15 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98045 Matrix: Solids
Sample ID: EX-3 Sampled: 6/6/2023 15:30
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
25.8 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/12/2317:50 CNC SW-DRYWT
DF Dilution Factor
Page 16 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001
REPOR T OF A NA L YSIS
Lab No : 98045
Matrix: Solids
Sample ID: EX-3
Sampled: 6/6/2023
15:30
Analytical Method: 8015C DRO
Prep Batch(es):
V34381 06/15/23 10:30
Prep Method: 3546
Test
Results
Units
MQL DF
Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
142
mg/Kg - dry
13.5 1
06/15/23 19:35 TJW
V34416
Surrogate: OTP Surrogate
108
Limits: 31-123%
1 06/15/23 19:35 TJW
8015C DRO
Analytical Method: 8015C GRO
Prep Batch(es):
V34234 06/12/23 08:00
Prep Method: 5035 MED
Test
Results
Units
MQL DF
Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
235
mg/Kg - dry
67.4 500
06/12/23 22:42 TBL
V34235
Surrogate: a,a,a-Trifluorotoluene
105
Limits: 50-137% 500 06/12/23 22:42 TBL
8015C GRO
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
DF Dilution Factor
Page 17 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98046 Matrix: Solids
Sample ID: EX-4 Sampled: 6/6/2023 15:40
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
26.0 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/12/2317:50 CNC SW-DRYWT
DF Dilution Factor
Page 18 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001
REPOR T OF A NA L YSIS
Lab No : 98046
Matrix: Solids
Sample ID: EX-4
Sampled: 6/6/2023
15:40
Analytical Method: 8015C DRO
Prep Batch(es):
V34381
06/15/23 10:30
Prep Method: 3546
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
<13.5
mg/Kg - dry
13.5
1 06/15/23 19:56 TJW
V34416
Surrogate: OTP Surrogate
77.4
Limits: 31-123% 1 06/15/23 19:56 TJW
8015C DRO
Analytical Method: 8015C GRO
Prep Batch(es):
V34234
06/12/23 08:00
Prep Method: 5035 MED
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
<6.76
mg/Kg - dry
6.76
50 06/12/23 15:39 TBL
V34235
Surrogate: a,a,a-Trifluorotoluene
111
Limits: 50-137% 50 06/12/23 15:39 TBL
8015C GRO
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
DF Dilution Factor
Page 19 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98047 Matrix: Solids
Sample ID: EX-5 Sampled: 6/7/2023 8:05
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
39.2 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/12/2317:50 CNC SW-DRYWT
DF Dilution Factor
Page 20 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001
REPOR T OF A NA L YSIS
Lab No : 98047
Matrix: Solids
Sample ID: EX-5
Sampled: 6/7/2023
8:05
Analytical Method: 8015C DRO
Prep Batch(es):
V34381
06/15/23 10:30
Prep Method: 3546
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
<24.7
mg/Kg - dry
24.7
1 06/15/23 20:18 TJW
V34416
Surrogate: OTP Surrogate
77.5
Limits: 31-123% 1 06/15/23 20:18 TJW
8015C DRO
Analytical Method: 8015C GRO
Prep Batch(es):
V34234
06/12/23 08:00
Prep Method: 5035 MED
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
<8.22
mg/Kg - dry
8.22
50 06/12/23 16:08 TBL
V34235
Surrogate: a,a,a-Trifluorotoluene
107
Limits: 50-137% 50 06/12/23 16:08 TBL
8015C GRO
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
DF Dilution Factor
Page 21 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98048 Matrix: Solids
Sample ID: EX-6 Sampled: 6/7/2023 8:20
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
24.0 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/12/2317:50 CNC SW-DRYWT
DF Dilution Factor
Page 22 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001
REPOR T OF A NA L YSIS
Lab No : 98048
Matrix: Solids
Sample ID: EX-6
Sampled: 6/7/2023
8:20
Analytical Method: 8015C DRO
Prep Batch(es):
V34381
06/15/23 10:30
Prep Method: 3546
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
<13.2
mg/Kg - dry
13.2
1 06/15/23 20:39 TJW
V34416
Surrogate: OTP Surrogate
78.2
Limits: 31-123% 1 06/15/23 20:39 TJW
8015C DRO
Analytical Method: 8015C GRO
Prep Batch(es):
V34234
06/12/23 08:00
Prep Method: 5035 MED
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
<6.58
mg/Kg - dry
6.58
50 06/12/23 16:37 TBL
V34235
Surrogate: a,a,a-Trifluorotoluene
98.6
Limits: 50-137% 50 06/12/23 16:37 TBL
8015C GRO
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
DF Dilution Factor
Page 23 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98049 Matrix: Solids
Sample ID: EX-7 Sampled: 6/7/2023 11:30
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
27.3 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/12/2317:50 CNC SW-DRYWT
DF Dilution Factor
Page 24 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98049 Matrix: Solids
Sample ID: EX-7 Sampled: 6/7/2023 11:30
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Acetone
<0.027
mg/Kg - dry
0.027
1
06/12/23 16:29
TBL
V34278
Acrolein
<0.027
mg/Kg - dry
0.027
1
06/12/23 16:29
TBL
V34278
Acrylonitrile
<0.027
mg/Kg - dry
0.027
1
06/12/23 16:29
TBL
V34278
Benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Bromobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Bromochloromethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Bromodichloromethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Bromoform
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Bromomethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:29
TBL
V34278
n-Butylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
sec -Butyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
tert-Butyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Carbon Disulfide
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Carbon Tetrachloride
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Chlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Chlorodibromomethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Chloroethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:29
TBL
V34278
Chloroform
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Chloromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:29
TBL
V34278
2-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
4-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Di -Isopropyl Ether (DIPE)
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 25 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98049 Matrix: Solids
Sample ID: EX-7 Sampled: 6/7/2023 11:30
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dibromo-3-Chloropropane
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:29
TBL
V34278
1,2-Dibromoethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Dibromomethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
1,2-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
1,3-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
1,4-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Dichlorodifluoromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:29
TBL
V34278
1,1-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
1,2-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
1,1-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
cis- 1,2-Dich loroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
trans-1,2-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
1,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
1,3-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
2,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
1,1-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
cis-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
trans-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Ethanol
<0.343
mg/Kg - dry
0.343
1
06/12/23 16:29
TBL
V34278
Ethylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Ethyl Tertiary Butyl Ether (ETBE) <0.068
mg/Kg - dry
0.068
1
06/12/23 16:29
TBL
V34278
Hexachlorobutadiene
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:29
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 26 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98049 Matrix: Solids
Sample ID: EX-7 Sampled: 6/7/2023 11:30
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
n-Hexane
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:29
TBL
V34278
2-Hexanone
<0.027
mg/Kg - dry
0.027
1
06/12/23 16:29
TBL
V34278
Isopropyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
4-Isopropyl toluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Methyl Ethyl Ketone (MEK)
<0.027
mg/Kg - dry
0.027
1
06/12/23 16:29
TBL
V34278
Methyl tert-butyl ether (MTBE) <0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
4-Methyl-2-Pentanone
<0.027
mg/Kg - dry
0.027
1
06/12/23 16:29
TBL
V34278
Methylene Chloride
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:29
TBL
V34278
Naphthalene
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:29
TBL
V34278
n-Propylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Styrene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
1,1,1,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
1,1,2,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Tetrachloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Toluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
1,2,3-Trichlorobenzene
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:29
TBL
V34278
1,2,4-Trichlorobenzene
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:29
TBL
V34278
1,1,1-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
1,1,2-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Trichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Trichlorofluoromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:29
TBL
V34278
1,2,3-Trichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 27 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Report Date : 06/21/2023
Received : 06/09/2023
Lab No : 98049 Matrix: Solids
Sample ID: EX-7 Sampled: 6/7/2023 11:30
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
1,3,5-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
Vinyl Acetate
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:29
TBL
V34278
Vinyl Chloride
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:29
TBL
V34278
o-Xylene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
TBL
V34278
m,p-Xylene
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:29
TBL
V34278
Xylene (Total)
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:29
V34278
Surrogate:4-Bromofluorobenzene
99.4
Limits:70-130%
1 06/12/23 16:29 TBL
V34278
Surrogate: Dibromofluoromethane
106
Limits: 84-123%
1 06/12/23 16:29 TBL
V34278
Surrogate: Toluene-d8
96.0
Limits: 76-129%
1 06/12/23 16:29 TBL
V34278
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Acenaphthylene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Aniline
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Anthracene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Benzo(a)anthracene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Benzo(a)pyrene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Benzo(b)fluoranthene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Benzo(g,h,i)perylene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 28 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98049
Matrix: Solids
Sample ID: EX-7
Sampled:
6/7/2023 11:30
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzo(k)fluoranthene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Benzoic Acid
<2.75
mg/Kg - dry
2.75
1
06/14/23 18:35
AMP
V34353
Benzyl alcohol
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Bis(2-Chloroethoxy)methane
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Bis(2-Chloroethyl)ether
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Bis(2-Chloroisopropyl)ether
<0.453
mg/Kg - dry
0.453
1
06/14/23 18:35
AMP
V34353
Bis(2-ethylhexyl)phthalate
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
4-13romophenyl phenyl ether
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Butyl benzyl phthalate
<0.453
mg/Kg - dry
0.453
1
06/14/23 18:35
AMP
V34353
4-Chloro-3-methylphenol
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
4-Chloroaniline
<0.453
mg/Kg - dry
0.453
1
06/14/23 18:35
AMP
V34353
2-Chloronaphthalene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
2-Chlorophenol
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
4-Chlorophenyl phenyl ether
<1.38
mg/Kg - dry
1.38
1
06/14/23 18:35
AMP
V34353
Chrysene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Dibenz(a,h)anthracene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Dibenzofuran
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
1,2-Dichlorobenzene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
1,3-Dichlorobenzene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
1,4-Dichlorobenzene
<0.453
mg/Kg - dry
0.453
1
06/14/23 18:35
AMP
V34353
3,3'-Dichlorobenzidine
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
2,4-Dichlorophenol
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 29 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98049
Matrix: Solids
Sample ID: EX-7
Sampled:
6/7/2023 11:30
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Dimethyl phthalate
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
2,4-Dimethyl phenol
<0.453
mg/Kg - dry
0.453
1
06/14/23 18:35
AMP
V34353
Di-n-butyl phthalate
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
4,6-Dinitro-2-methylphenol
<2.06
mg/Kg - dry
2.06
1
06/14/23 18:35
AMP
V34353
2,4-Dinitrophenol
<2.06
mg/Kg - dry
2.06
1
06/14/23 18:35
AMP
V34353
2,4-Dinitrotoluene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
2,6-Dinitrotoluene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Di-n-Octyl Phthalate
<0.453
mg/Kg - dry
0.453
1
06/14/23 18:35
AMP
V34353
Fluoranthene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Fluorene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Hexachlorobenzene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Hexachlorobutadiene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Hexachlorocyclopentadiene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Hexachloroethane
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Indeno(1,2,3-cd)pyrene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Isophorone
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
1-Methylnaphthalene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
2-Methylnaphthalene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
2-Methylphenol
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
3&4 Methylphenol
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Naphthalene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 30 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98049
Matrix: Solids
Sample ID: EX-7
Sampled: 6/7/2023
11:30
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
2-Nitroaniline
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35 AMP
V34353
3-Nitroaniline
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35 AMP
V34353
4-Nitroaniline
<0.453
mg/Kg - dry
0.453
1
06/14/23 18:35 AMP
V34353
Nitrobenzene
<0.453
mg/Kg - dry
0.453
1
06/14/23 18:35 AMP
V34353
2-Nitrophenol
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35 AMP
V34353
4-Nitrophenol
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35 AMP
V34353
N-Nitrosodimethylamine
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35 AMP
V34353
N-Nitrosodiphenylamine
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35 AMP
V34353
N-Nitroso-di-n-propylamine
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35 AMP
V34353
Pentachlorophenol
<1.38
mg/Kg - dry
1.38
1
06/14/23 18:35 AMP
V34353
Phenanthrene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35 AMP
V34353
Phenol
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35 AMP
V34353
Pyrene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35 AMP
V34353
Pyridine
<0.453
mg/Kg - dry
0.453
1
06/14/23 18:35 AMP
V34353
1,2,4-Trichlorobenzene
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35 AMP
V34353
2,4,5-Trichlorophenol
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35 AMP
V34353
2,4,6-Trichlorophenol
<0.909
mg/Kg - dry
0.909
1
06/14/23 18:35 AMP
V34353
Surrogate: Phenol-d5
56.3
Limits: 34-121%
1 06/14/23 18:35 AMP
8270E
Surrogate:2-Fluorobiphenyl
75.4
Limits:44-115%
1 06/14/23 18:35 AMP
V34353
Surrogate:2-Fluorophenol
61.1
Limits:35-115%
1 06/14/23 18:35 AMP
V34353
Surrogate: Nitrobenzene-d5
67.1
Limits: 37-122%
1 06/14/23 18:35 AMP
V34353
Surrogate:4-Terphenyl-d14
83.2
Limits:54-127%
1 06/14/23 18:35 AMP
V34353
Surrogate: 2,4,6-Tribromophenol
65.9
Limits:39-132%
1 06/14/23 18:35 AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 31 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98049 Matrix: Solids
Sample ID: EX-7 Sampled: 6/7/2023 11:30
Analytical Method: MADEP-EPH
Prep Method: MAEPH (Prep)
Test
Aliphatic C9-C18
Aliphatic C19-C36
Aromatic C11-C22
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Analytical Method: MADEP-VPH
Prep Method: MAVPH (Prep)
Test
Prep Batch(es): V34271 06/13/23 10:20
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
<68.8 mg/Kg - dry
68.8 1
06/16/23 20:38 AMP
V34449
<68.8 mg/Kg - dry
68.8 1
06/16/23 20:38 AMP
V34449
<68.8 mg/Kg - dry
68.8 1
06/16/23 20:38 AMP
V34449
109
Limits: 40-140%
1 06/16/23 20:38 AMP
MADEP-EPH
70.0
Limits: 40-140%
1 06/16/23 20:38 AMP
MADEP-EPH
97.0
Limits: 40-140%
1 06/16/23 20:38 AMP
MADEP-EPH
106
Limits: 40-140%
1 06/16/23 20:38 AMP
V34449
Prep Batch(es):
V34232 06/12/23 08:00
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Aliphatic C5-C8 <11.0
Aliphatic C9-C12 <11.0
Aromatic C9-C10 <11.0
Surrogate: 2,5-Dibromotoluene (FID)
Surrogate: 2,5-Dibromotoluene (PID)
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
mg/Kg - dry
11.0
100 06/12/23 16:01 TBL
V34233
mg/Kg - dry
11.0
100 06/12/23 16:01 TBL
V34233
mg/Kg - dry
11.0
100 06/12/23 16:01 TBL
V34233
89.0
Limits: 70-130%
100 06/12/23 16:01 TBL
MADEP-VPH
107
Limits: 70-130%
100 06/12/23 16:01 TBL
MADEP-VPH
DF Dilution Factor
Page 32 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98050 Matrix: Solids
Sample ID: EX-8 Sampled: 6/7/2023 11:45
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
28.0 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/12/2317:50 CNC SW-DRYWT
DF Dilution Factor
Page 33 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98050 Matrix: Solids
Sample ID: EX-8 Sampled: 6/7/2023 11:45
Analytical Method: 8260D Prep Batch(es): V34281 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Acetone
<0.027
mg/Kg - dry
0.027
1
06/12/23 22:22
TBL
V34282
Acrolein
<0.027
mg/Kg - dry
0.027
1
06/12/23 22:22
TBL
V34282
Acrylonitrile
<0.027
mg/Kg - dry
0.027
1
06/12/23 22:22
TBL
V34282
Benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Bromobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Bromochloromethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Bromodichloromethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Bromoform
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Bromomethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 22:22
TBL
V34282
n-Butylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
sec -Butyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
tert-Butyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Carbon Disulfide
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Carbon Tetrachloride
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Chlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Chlorodibromomethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Chloroethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 22:22
TBL
V34282
Chloroform
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Chloromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 22:22
TBL
V34282
2-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
4-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Di -Isopropyl Ether (DIPE)
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 34 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98050 Matrix: Solids
Sample ID: EX-8 Sampled: 6/7/2023 11:45
Analytical Method: 8260D Prep Batch(es): V34281 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dibromo-3-Chloropropane
<0.013
mg/Kg - dry
0.013
1
06/12/23 22:22
TBL
V34282
1,2-Dibromoethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Dibromomethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
1,2-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
1,3-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
1,4-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Dichlorodifluoromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 22:22
TBL
V34282
1,1-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
1,2-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
1,1-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
cis- 1,2-Dich loroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
trans-1,2-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
1,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
1,3-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
2,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
1,1-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
cis-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
trans-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Ethanol
<0.347
mg/Kg - dry
0.347
1
06/12/23 22:22
TBL
V34282
Ethylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Ethyl Tertiary Butyl Ether (ETBE) <0.069
mg/Kg - dry
0.069
1
06/12/23 22:22
TBL
V34282
Hexachlorobutadiene
<0.013
mg/Kg - dry
0.013
1
06/12/23 22:22
TBL
V34282
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 35 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98050 Matrix: Solids
Sample ID: EX-8 Sampled: 6/7/2023 11:45
Analytical Method: 8260D Prep Batch(es): V34281 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
n-Hexane
<0.013
mg/Kg - dry
0.013
1
06/12/23 22:22
TBL
V34282
2-Hexanone
<0.027
mg/Kg - dry
0.027
1
06/12/23 22:22
TBL
V34282
Isopropyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
4-Isopropyl toluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Methyl Ethyl Ketone (MEK)
<0.027
mg/Kg - dry
0.027
1
06/12/23 22:22
TBL
V34282
Methyl tert-butyl ether (MTBE) <0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
4-Methyl-2-Pentanone
<0.027
mg/Kg - dry
0.027
1
06/12/23 22:22
TBL
V34282
Methylene Chloride
<0.013
mg/Kg - dry
0.013
1
06/12/23 22:22
TBL
V34282
Naphthalene
0.027
mg/Kg - dry
0.013
1
06/12/23 22:22
TBL
V34282
n-Propylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Styrene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
1,1,1,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
1,1,2,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Tetrachloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Toluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
1,2,3-Trichlorobenzene
<0.013
mg/Kg - dry
0.013
1
06/12/23 22:22
TBL
V34282
1,2,4-Trichlorobenzene
<0.013
mg/Kg - dry
0.013
1
06/12/23 22:22
TBL
V34282
1,1,1-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
1,1,2-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Trichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Trichlorofluoromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 22:22
TBL
V34282
1,2,3-Trichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 36 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Report Date : 06/21/2023
Received : 06/09/2023
Lab No : 98050 Matrix: Solids
Sample ID: EX-8 Sampled: 6/7/2023 11:45
Analytical Method: 8260D Prep Batch(es): V34281 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
0.026
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
1,3,5-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
Vinyl Acetate
<0.013
mg/Kg - dry
0.013
1
06/12/23 22:22
TBL
V34282
Vinyl Chloride
<0.013
mg/Kg - dry
0.013
1
06/12/23 22:22
TBL
V34282
o-Xylene
0.010
mg/Kg - dry
0.006
1
06/12/23 22:22
TBL
V34282
m,p-Xylene
0.013
mg/Kg - dry
0.013
1
06/12/23 22:22
TBL
V34282
Xylene (Total)
0.024
mg/Kg - dry
0.006
1
06/12/23 22:22
V34282
Surrogate: 4-Bromofluorobenzene
102
Limits: 70-130%
1 06/12/23 22:22 TBL
V34282
Surrogate: Dibromofluoromethane
105
Limits: 84-123%
1 06/12/23 22:22 TBL
V34282
Surrogate: Toluene-d8
95.4
Limits: 76-129%
1 06/12/23 22:22 TBL
V34282
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Acenaphthylene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Aniline
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Anthracene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Benzo(a)anthracene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Benzo(a)pyrene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Benzo(b)fluoranthene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Benzo(g,h,i)perylene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 37 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98050
Matrix: Solids
Sample ID: EX-8
Sampled:
6/7/2023 11:45
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzo(k)fluoranthene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Benzoic Acid
<2.78
mg/Kg - dry
2.78
1
06/14/23 18:57
AMP
V34353
Benzyl alcohol
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Bis(2-Chloroethoxy)methane
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Bis(2-Chloroethyl)ether
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Bis(2-Chloroisopropyl)ether
<0.458
mg/Kg - dry
0.458
1
06/14/23 18:57
AMP
V34353
Bis(2-ethylhexyl)phthalate
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
4-13romophenyl phenyl ether
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Butyl benzyl phthalate
<0.458
mg/Kg - dry
0.458
1
06/14/23 18:57
AMP
V34353
4-Chloro-3-methylphenol
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
4-Chloroaniline
<0.458
mg/Kg - dry
0.458
1
06/14/23 18:57
AMP
V34353
2-Chloronaphthalene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
2-Chlorophenol
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
4-Chlorophenyl phenyl ether
<1.39
mg/Kg - dry
1.39
1
06/14/23 18:57
AMP
V34353
Chrysene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Dibenz(a,h)anthracene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Dibenzofuran
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
1,2-Dichlorobenzene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
1,3-Dichlorobenzene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
1,4-Dichlorobenzene
<0.458
mg/Kg - dry
0.458
1
06/14/23 18:57
AMP
V34353
3,3'-Dichlorobenzidine
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
2,4-Dichlorophenol
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 38 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98050
Matrix: Solids
Sample ID: EX-8
Sampled:
6/7/2023 11:45
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Dimethyl phthalate
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
2,4-Dimethyl phenol
<0.458
mg/Kg - dry
0.458
1
06/14/23 18:57
AMP
V34353
Di-n-butyl phthalate
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
4,6-Dinitro-2-methylphenol
<2.08
mg/Kg - dry
2.08
1
06/14/23 18:57
AMP
V34353
2,4-Dinitrophenol
<2.08
mg/Kg - dry
2.08
1
06/14/23 18:57
AMP
V34353
2,4-Dinitrotoluene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
2,6-Dinitrotoluene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Di-n-Octyl Phthalate
<0.458
mg/Kg - dry
0.458
1
06/14/23 18:57
AMP
V34353
Fluoranthene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Fluorene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Hexachlorobenzene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Hexachlorobutadiene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Hexachlorocyclopentadiene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Hexachloroethane
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Indeno(1,2,3-cd)pyrene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Isophorone
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
1-Methylnaphthalene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
2-Methylnaphthalene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
2-Methylphenol
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
3&4 Methylphenol
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Naphthalene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 39 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98050
Matrix: Solids
Sample ID: EX-8
Sampled: 6/7/2023
11:45
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
2-Nitroaniline
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57 AMP
V34353
3-Nitroaniline
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57 AMP
V34353
4-Nitroaniline
<0.458
mg/Kg - dry
0.458
1
06/14/23 18:57 AMP
V34353
Nitrobenzene
<0.458
mg/Kg - dry
0.458
1
06/14/23 18:57 AMP
V34353
2-Nitrophenol
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57 AMP
V34353
4-Nitrophenol
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57 AMP
V34353
N-Nitrosodimethylamine
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57 AMP
V34353
N-Nitrosodiphenylamine
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57 AMP
V34353
N-Nitroso-di-n-propylamine
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57 AMP
V34353
Pentachlorophenol
<1.39
mg/Kg - dry
1.39
1
06/14/23 18:57 AMP
V34353
Phenanthrene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57 AMP
V34353
Phenol
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57 AMP
V34353
Pyrene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57 AMP
V34353
Pyridine
<0.458
mg/Kg - dry
0.458
1
06/14/23 18:57 AMP
V34353
1,2,4-Trichlorobenzene
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57 AMP
V34353
2,4,5-Trichlorophenol
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57 AMP
V34353
2,4,6-Trichlorophenol
<0.916
mg/Kg - dry
0.916
1
06/14/23 18:57 AMP
V34353
Surrogate: Phenol-d5
55.9
Limits: 34-121%
1 06/14/23 18:57 AMP
8270E
Surrogate:2-Fluorobiphenyl
72.5
Limits:44-115%
1 06/14/23 18:57 AMP
V34353
Surrogate:2-Fluorophenol
60.7
Limits:35-115%
1 06/14/23 18:57 AMP
V34353
Surrogate: Nitrobenzene-d5
73.1
Limits: 37-122%
1 06/14/23 18:57 AMP
V34353
Surrogate:4-Terphenyl-d14
80.8
Limits:54-127%
1 06/14/23 18:57 AMP
V34353
Surrogate: 2,4,6-Tribromophenol
68.8
Limits:39-132%
1 06/14/23 18:57 AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 40 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98050 Matrix: Solids
Sample ID: EX-8 Sampled: 6/7/2023 11:45
Analytical Method: MADEP-EPH
Prep Method: MAEPH (Prep)
Test
Aliphatic C9-C18
Aliphatic C19-C36
Aromatic C11-C22
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Analytical Method: MADEP-VPH
Prep Method: MAVPH (Prep)
Test
Prep Batch(es): V34271 06/13/23 10:20
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
<69.4 mg/Kg - dry
69.4 1
06/16/23 21:14 AMP
V34449
<69.4 mg/Kg - dry
69.4 1
06/16/23 21:14 AMP
V34449
<69.4 mg/Kg - dry
69.4 1
06/16/23 21:14 AMP
V34449
104
Limits: 40-140%
1 06/16/23 21:14 AMP
MADEP-EPH
73.0
Limits: 40-140%
1 06/16/23 21:14 AMP
MADEP-EPH
96.9
Limits: 40-140%
1 06/16/23 21:14 AMP
MADEP-EPH
103
Limits: 40-140%
1 06/16/23 21:14 AMP
V34449
Prep Batch(es):
V34232 06/12/23 08:00
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Aliphatic C5-C8
Aliphatic C9-C12
Aromatic C9-C10
Surrogate: 2,5-Dibromotoluene (FID)
Surrogate: 2,5-Dibromotoluene (PID)
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
mg/Kg - dry
11.1
100 06/12/23 16:24 TBL
V34233
mg/Kg - dry
11.1
100 06/12/23 16:24 TBL
V34233
mg/Kg - dry
11.1
100 06/12/23 16:24 TBL
V34233
91.2
Limits: 70-130%
100 06/12/23 16:24 TBL
MADEP-VPH
99.1
Limits: 70-130%
100 06/12/23 16:24 TBL
MADEP-VPH
DF Dilution Factor
Page 41 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98051 Matrix: Solids
Sample ID: EX-9 Sampled: 6/7/2023 14:10
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
23.4 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/12/2317:50 CNC SW-DRYWT
DF Dilution Factor
Page 42 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001
REPOR T OF A NA L YSIS
Lab No : 98051
Matrix: Solids
Sample ID: EX-9
Sampled: 6/7/2023
14:10
Analytical Method: 8015C DRO
Prep Batch(es):
V34381
06/15/23 10:30
Prep Method: 3546
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
<13.1
mg/Kg - dry
13.1
1 06/15/23 21:01 TJW
V34416
Surrogate: OTP Surrogate
90.2
Limits: 31-123% 1 06/15/23 21:01 TJW
8015C DRO
Analytical Method: 8015C GRO
Prep Batch(es):
V34234
06/12/23 08:00
Prep Method: 5035 MED
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
<6.53
mg/Kg - dry
6.53
50 06/12/23 17:05 TBL
V34235
Surrogate: a,a,a-Trifluorotoluene
101
Limits: 50-137% 50 06/12/23 17:05 TBL
8015C GRO
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
DF Dilution Factor
Page 43 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98052 Matrix: Solids
Sample ID: EX-10 Sampled: 6/7/2023 14:15
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
31.0 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 44 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001
REPOR T OF A NA L YSIS
Lab No : 98052
Matrix: Solids
Sample ID: EX-10
Sampled: 6/7/2023
14:15
Analytical Method: 8015C DRO
Prep Batch(es):
V34381
06/15/23 10:30
Prep Method: 3546
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
<17.4
mg/Kg - dry
17.4
1 06/15/23 21:22 TJW
V34416
Surrogate: OTP Surrogate
78.1
Limits: 31-123% 1 06/15/23 21:22 TJW
8015C DRO
Analytical Method: 8015C GRO
Prep Batch(es):
V34234
06/12/23 08:00
Prep Method: 5035 MED
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
<7.25
mg/Kg - dry
7.25
50 06/12/23 17:34 TBL
V34235
Surrogate: a,a,a-Trifluorotoluene
130
Limits: 50-137% 50 06/12/23 17:34 TBL
8015C GRO
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
DF Dilution Factor
Page 45 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98053 Matrix: Solids
Sample ID: EX-11 Sampled: 6/7/2023 14:20
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
29.7 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 46 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001
REPOR T OF A NA L YSIS
Lab No : 98053
Matrix: Solids
Sample ID: EX-11
Sampled: 6/7/2023
14:20
Analytical Method: 8015C DRO
Prep Batch(es):
V34381
06/15/23 10:30
Prep Method: 3546
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
<14.2
mg/Kg - dry
14.2
1 06/15/23 21:43 TJW
V34416
Surrogate: OTP Surrogate
80.5
Limits: 31-123% 1 06/15/23 21:43 TJW
8015C DRO
Analytical Method: 8015C GRO
Prep Batch(es):
V34234
06/12/23 08:00
Prep Method: 5035 MED
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
<7.11
mg/Kg - dry
7.11
50 06/12/23 18:02 TBL
V34235
Surrogate: a,a,a-Trifluorotoluene
108
Limits: 50-137% 50 06/12/23 18:02 TBL
8015C GRO
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
DF Dilution Factor
Page 47 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98054 Matrix: Solids
Sample ID: EX-12 Sampled: 6/7/2023 15:35
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
28.6 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 48 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001
REPOR T OF A NA L YSIS
Lab No : 98054
Matrix: Solids
Sample ID: EX-12
Sampled: 6/7/2023
15:35
Analytical Method: 8015C DRO
Prep Batch(es):
V34381
06/15/23 10:30
Prep Method: 3546
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
27.9
mg/Kg - dry
14.0
1 06/15/23 22:05 TJW
V34416
Surrogate: OTP Surrogate
77.4
Limits: 31-123% 1 06/15/23 22:05 TJW
8015C DRO
Analytical Method: 8015C GRO
Prep Batch(es):
V34234
06/12/23 08:00
Prep Method: 5035 MED
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
<7.00
mg/Kg - dry
7.00
50 06/12/23 18:30 TBL
V34235
Surrogate: a,a,a-Trifluorotoluene
114
Limits: 50-137% 50 06/12/23 18:30 TBL
8015C GRO
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
DF Dilution Factor
Page 49 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98055 Matrix: Solids
Sample ID: EX-13 Sampled: 6/7/2023 15:40
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
30.6 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 50 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001
REPOR T OF A NA L YSIS
Lab No : 98055
Matrix: Solids
Sample ID: EX-13
Sampled: 6/7/2023
15:40
Analytical Method: 8015C DRO
Prep Batch(es):
V34381
06/15/23 10:30
Prep Method: 3546
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
124
mg/Kg - dry
14.4
1 06/15/23 22:26 TJW
V34416
Surrogate: OTP Surrogate
83.6
Limits: 31-123% 1 06/15/23 22:26 TJW
8015C DRO
Analytical Method: 8015C GRO
Prep Batch(es):
V34234
06/12/23 08:00
Prep Method: 5035 MED
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
<7.20
mg/Kg - dry
7.20
50 06/12/23 18:58 TBL
V34235
Surrogate: a,a,a-Trifluorotoluene
98.2
Limits: 50-137% 50 06/12/23 18:58 TBL
8015C GRO
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
DF Dilution Factor
Page 51 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98056 Matrix: Solids
Sample ID: EX-14 Sampled: 6/7/2023 15:45
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
39.7 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 52 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001
REPOR T OF A NA L YSIS
Lab No : 98056
Matrix: Solids
Sample ID: EX-14
Sampled: 6/7/2023
15:45
Analytical Method: 8015C DRO
Prep Batch(es):
V34381
06/15/23 10:30
Prep Method: 3546
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
26.0
mg/Kg - dry
16.6
1 06/15/23 22:48 TJW
V34416
Surrogate: OTP Surrogate
74.1
Limits: 31-123% 1 06/15/23 22:48 TJW
8015C DRO
Analytical Method: 8015C GRO
Prep Batch(es):
V34234
06/12/23 08:00
Prep Method: 5035 MED
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
<8.29
mg/Kg - dry
8.29
50 06/12/23 19:54 TBL
V34235
Surrogate: a,a,a-Trifluorotoluene
101
Limits: 50-137% 50 06/12/23 19:54 TBL
8015C GRO
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
DF Dilution Factor
Page 53 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98057 Matrix: Solids
Sample ID: EX-15 Sampled: 6/7/2023 16:15
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
21.3 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 54 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001
REPOR T OF A NA L YSIS
Lab No : 98057
Matrix: Solids
Sample ID: EX-15
Sampled: 6/7/2023
16:15
Analytical Method: 8015C DRO
Prep Batch(es):
V34381
06/15/23 10:30
Prep Method: 3546
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
<12.7
mg/Kg - dry
12.7
1 06/15/23 23:09 TJW
V34416
Surrogate: OTP Surrogate
80.5
Limits: 31-123% 1 06/15/23 23:09 TJW
8015C DRO
Analytical Method: 8015C GRO
Prep Batch(es):
V34234
06/12/23 08:00
Prep Method: 5035 MED
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
<6.35
mg/Kg - dry
6.35
50 06/12/23 20:22 TBL
V34235
Surrogate: a,a,a-Trifluorotoluene
100
Limits: 50-137% 50 06/12/23 20:22 TBL
8015C GRO
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
DF Dilution Factor
Page 55 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98058 Matrix: Solids
Sample ID: EX-16 Sampled: 6/8/2023 17:00
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
31.4 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 56 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001
REPOR T OF A NA L YSIS
Lab No : 98058
Matrix: Solids
Sample ID: EX-16
Sampled: 6/8/2023
17:00
Analytical Method: 8015C DRO
Prep Batch(es):
V34381 06/15/23 10:30
Prep Method: 3546
Test
Results
Units
MQL DF
Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
<14.6
mg/Kg - dry
14.6 1
06/15/23 23:31 TJW
V34416
Surrogate: OTP Surrogate
76.7
Limits: 31-123%
1 06/15/23 23:31 TJW
8015C DRO
Analytical Method: 8015C GRO
Prep Batch(es):
V34234 06/12/23 08:00
Prep Method: 5035 MED
Test
Results
Units
MQL DF
Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
150
mg/Kg - dry
72.9 500
06/12/23 23:10 TBL
V34235
Surrogate: a,a,a-Trifluorotoluene
118
Limits: 50-137% 500 06/12/23 23:10 TBL
8015C GRO
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
DF Dilution Factor
Page 57 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98059 Matrix: Solids
Sample ID: EX-17 Sampled: 6/8/2023 17:10
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
26.5 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 58 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001
REPOR T OF A NA L YSIS
Lab No : 98059
Matrix: Solids
Sample ID: EX-17
Sampled: 6/8/2023
17:10
Analytical Method: 8015C DRO
Prep Batch(es):
V34381
06/15/23 10:30
Prep Method: 3546
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
<13.6
mg/Kg - dry
13.6
1 06/15/23 23:52 TJW
V34416
Surrogate: OTP Surrogate
73.6
Limits: 31-123% 1 06/15/23 23:52 TJW
8015C DRO
Analytical Method: 8015C GRO
Prep Batch(es):
V34234
06/12/23 08:00
Prep Method: 5035 MED
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
<6.80
mg/Kg - dry
6.80
50 06/12/23 20:50 TBL
V34235
Surrogate: a,a,a-Trifluorotoluene
124
Limits: 50-137% 50 06/12/23 20:50 TBL
8015C GRO
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
DF Dilution Factor
Page 59 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98060 Matrix: Solids
Sample ID: UST-1-A Sampled: 6/8/2023 13:45
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
28.9 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 60 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98060 Matrix: Solids
Sample ID: UST-1-A Sampled: 6/8/2023 13:45
Analytical Method: 8015C DRO
Prep Batch(es):
V34382
06/15/23 10:30
Prep Method: 3546
Test
Results Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
18100 mg/Kg - dry
5630
400 06/16/23 11:14 TJW
V34417
Surrogate: OTP Surrogate
0 *
Limits: 31-123% 400 06/16/23 11:14 TJW
8015C DRO
Analytical Method: 8015C GRO
Prep Batch(es):
V34234
06/12/23 08:00
Prep Method: 5035 MED
Test
Results Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
Surrogate: a,a,a-Trifluorotoluene
895 mg/Kg - dry
70.3
500 06/12/23 23:38 TBL
V34235
86.4
Limits: 50-137%
500 06/12/23 23:38 TBL
8015C GRO
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
DF Dilution Factor
Page 61 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98061 Matrix: Solids
Sample ID: UST-1-B Sampled: 6/8/2023 13:55
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
27.0 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 62 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001
REPOR T OF A NA L YSIS
Lab No : 98061
Matrix: Solids
Sample ID: UST-1-B
Sampled: 6/8/2023
13:55
Analytical Method: 8015C DRO
Prep Batch(es):
V34382
06/15/23 10:30
Prep Method: 3546
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
7450
mg/Kg - dry
2740
200 06/16/23 11:36 TJW
V34417
Surrogate: OTP Surrogate
0 *
Limits: 31-123% 200 06/16/23 11:36 TJW
8015C DRO
Analytical Method: 8015C GRO
Prep Batch(es):
V34234
06/12/23 08:00
Prep Method: 5035 MED
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
827
mg/Kg - dry
68.5
500 06/13/23 00:06 TBL
V34235
Surrogate: a,a,a-Trifluorotoluene
86.4
Limits: 50-137% 500 06/13/23 00:06 TBL
8015C GRO
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
DF Dilution Factor
Page 63 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98062 Matrix: Solids
Sample ID: UST-2-A Sampled: 6/8/2023 16:00
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
31.9 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 64 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001
REPOR T OF A NA L YSIS
Lab No : 98062
Matrix: Solids
Sample ID: UST-2-A
Sampled: 6/8/2023
16:00
Analytical Method: 8015C DRO
Prep Batch(es):
V34382
06/15/23 10:30
Prep Method: 3546
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
160
mg/Kg - dry
14.7
1 06/16/23 02:00 TJW
V34417
Surrogate: OTP Surrogate
76.7
Limits: 31-123% 1 06/16/23 02:00 TJW
8015C DRO
Analytical Method: 8015C GRO
Prep Batch(es):
V34234
06/12/23 08:00
Prep Method: 5035 MED
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
<7.34
mg/Kg - dry
7.34
50 06/12/23 21:18 TBL
V34235
Surrogate: a,a,a-Trifluorotoluene
105
Limits: 50-137% 50 06/12/23 21:18 TBL
8015C GRO
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
DF Dilution Factor
Page 65 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98063 Matrix: Solids
Sample ID: UST-2-B Sampled: 6/8/2023 14:00
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
26.0 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 66 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001
REPOR T OF A NA L YSIS
Lab No : 98063
Matrix: Solids
Sample ID: UST-2-B
Sampled: 6/8/2023
14:00
Analytical Method: 8015C DRO
Prep Batch(es):
V34382
06/15/23 10:30
Prep Method: 3546
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
43900
mg/Kg - dry
10800
800 06/16/23 11:57 TJW
V34417
Surrogate: OTP Surrogate
0 *
Limits: 31-123% 800 06/16/23 11:57 TJW
8015C DRO
Analytical Method: 8015C GRO
Prep Batch(es):
V34234
06/12/23 08:00
Prep Method: 5035 MED
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
21.5
mg/Kg - dry
6.76
50 06/12/23 21:46 TBL
V34235
Surrogate: a,a,a-Trifluorotoluene
108
Limits: 50-137% 50 06/12/23 21:46 TBL
8015C GRO
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
DF Dilution Factor
Page 67 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98064 Matrix: Solids
Sample ID: UST-2-C Sampled: 6/8/2023 17:35
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
25.6 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 68 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98064 Matrix: Solids
Sample ID: UST-2-C Sampled: 6/8/2023 17:35
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Acetone
<0.026
mg/Kg - dry
0.026
1
06/12/23 16:56
TBL
V34278
Acrolein
<0.026
mg/Kg - dry
0.026
1
06/12/23 16:56
TBL
V34278
Acrylonitrile
<0.026
mg/Kg - dry
0.026
1
06/12/23 16:56
TBL
V34278
Benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Bromobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Bromochloromethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Bromodichloromethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Bromoform
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Bromomethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:56
TBL
V34278
n-Butylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
sec -Butyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
tert-Butyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Carbon Disulfide
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Carbon Tetrachloride
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Chlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Chlorodibromomethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Chloroethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:56
TBL
V34278
Chloroform
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Chloromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:56
TBL
V34278
2-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
4-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Di -Isopropyl Ether (DIPE)
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 69 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98064 Matrix: Solids
Sample ID: UST-2-C Sampled: 6/8/2023 17:35
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dibromo-3-Chloropropane
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:56
TBL
V34278
1,2-Dibromoethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Dibromomethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
1,2-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
1,3-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
1,4-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Dichlorodifluoromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:56
TBL
V34278
1,1-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
1,2-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
1,1-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
cis- 1,2-Dich loroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
trans-1,2-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
1,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
1,3-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
2,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
1,1-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
cis-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
trans-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Ethanol
<0.336
mg/Kg - dry
0.336
1
06/12/23 16:56
TBL
V34278
Ethylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Ethyl Tertiary Butyl Ether (ETBE) <0.067
mg/Kg - dry
0.067
1
06/12/23 16:56
TBL
V34278
Hexachlorobutadiene
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:56
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 70 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98064 Matrix: Solids
Sample ID: UST-2-C Sampled: 6/8/2023 17:35
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
n-Hexane
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:56
TBL
V34278
2-Hexanone
<0.026
mg/Kg - dry
0.026
1
06/12/23 16:56
TBL
V34278
Isopropyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
4-Isopropyl toluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Methyl Ethyl Ketone (MEK)
<0.026
mg/Kg - dry
0.026
1
06/12/23 16:56
TBL
V34278
Methyl tert-butyl ether (MTBE) <0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
4-Methyl-2-Pentanone
<0.026
mg/Kg - dry
0.026
1
06/12/23 16:56
TBL
V34278
Methylene Chloride
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:56
TBL
V34278
Naphthalene
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:56
TBL
V34278
n-Propylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Styrene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
1,1,1,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
1,1,2,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Tetrachloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Toluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
1,2,3-Trichlorobenzene
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:56
TBL
V34278
1,2,4-Trichlorobenzene
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:56
TBL
V34278
1,1,1-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
1,1,2-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Trichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Trichlorofluoromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:56
TBL
V34278
1,2,3-Trichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 71 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Report Date : 06/21/2023
Received : 06/09/2023
Lab No : 98064 Matrix: Solids
Sample ID: UST-2-C Sampled: 6/8/2023 17:35
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
1,3,5-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
Vinyl Acetate
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:56
TBL
V34278
Vinyl Chloride
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:56
TBL
V34278
o-Xylene
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
TBL
V34278
m,p-Xylene
<0.013
mg/Kg - dry
0.013
1
06/12/23 16:56
TBL
V34278
Xylene (Total)
<0.006
mg/Kg - dry
0.006
1
06/12/23 16:56
V34278
Surrogate:4-Bromofluorobenzene
101
Limits:70-130%
1 06/12/23 16:56 TBL
V34278
Surrogate: Dibromofluoromethane
107
Limits: 84-123%
1 06/12/23 16:56 TBL
V34278
Surrogate: Toluene-d8
96.4
Limits: 76-129%
1 06/12/23 16:56 TBL
V34278
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Acenaphthylene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Aniline
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Anthracene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Benzo(a)anthracene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Benzo(a)pyrene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Benzo(b)fluoranthene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Benzo(g,h,i)perylene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 72 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98064 Matrix: Solids
Sample ID: UST-2-C Sampled: 6/8/2023 17:35
Analytical Method: 8270E Prep Batch(es): V34327 06/14/23 09:30
Prep Method: 3546
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Benzo(k)fluoranthene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Benzoic Acid
<2.69
mg/Kg - dry
2.69
1
06/14/23 19:20
AMP
V34353
Benzyl alcohol
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Bis(2-Chloroethoxy)methane
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Bis(2-Chloroethyl)ether
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Bis(2-Chloroisopropyl)ether
<0.443
mg/Kg - dry
0.443
1
06/14/23 19:20
AMP
V34353
Bis(2-ethylhexyl)phthalate
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
4-13romophenyl phenyl ether
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Butyl benzyl phthalate
<0.443
mg/Kg - dry
0.443
1
06/14/23 19:20
AMP
V34353
4-Chloro-3-methylphenol
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
4-Chloroaniline
<0.443
mg/Kg - dry
0.443
1
06/14/23 19:20
AMP
V34353
2-Chloronaphthalene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
2-Chlorophenol
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
4-Chlorophenyl phenyl ether
<1.34
mg/Kg - dry
1.34
1
06/14/23 19:20
AMP
V34353
Chrysene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Dibenz(a,h)anthracene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Dibenzofuran
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
1,2-Dichlorobenzene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
1,3-Dichlorobenzene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
1,4-Dichlorobenzene
<0.443
mg/Kg - dry
0.443
1
06/14/23 19:20
AMP
V34353
3,3'-Dichlorobenzidine
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
2,4-Dichlorophenol
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 73 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98064
Matrix: Solids
Sample ID: UST-2-C
Sampled:
6/8/2023 17:35
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Dimethyl phthalate
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
2,4-Dimethyl phenol
<0.443
mg/Kg - dry
0.443
1
06/14/23 19:20
AMP
V34353
Di-n-butyl phthalate
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
4,6-Dinitro-2-methylphenol
<2.02
mg/Kg - dry
2.02
1
06/14/23 19:20
AMP
V34353
2,4-Dinitrophenol
<2.02
mg/Kg - dry
2.02
1
06/14/23 19:20
AMP
V34353
2,4-Dinitrotoluene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
2,6-Dinitrotoluene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Di-n-Octyl Phthalate
<0.443
mg/Kg - dry
0.443
1
06/14/23 19:20
AMP
V34353
Fluoranthene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Fluorene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Hexachlorobenzene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Hexachlorobutadiene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Hexachlorocyclopentadiene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Hexachloroethane
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Indeno(1,2,3-cd)pyrene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Isophorone
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
1-Methylnaphthalene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
2-Methylnaphthalene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
2-Methylphenol
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
3&4 Methylphenol
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Naphthalene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 74 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98064
Matrix: Solids
Sample ID: UST-2-C
Sampled: 6/8/2023
17:35
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
2-Nitroaniline
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20 AMP
V34353
3-Nitroaniline
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20 AMP
V34353
4-Nitroaniline
<0.443
mg/Kg - dry
0.443
1
06/14/23 19:20 AMP
V34353
Nitrobenzene
<0.443
mg/Kg - dry
0.443
1
06/14/23 19:20 AMP
V34353
2-Nitrophenol
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20 AMP
V34353
4-Nitrophenol
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20 AMP
V34353
N-Nitrosodimethylamine
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20 AMP
V34353
N-Nitrosodiphenylamine
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20 AMP
V34353
N-Nitroso-di-n-propylamine
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20 AMP
V34353
Pentachlorophenol
<1.34
mg/Kg - dry
1.34
1
06/14/23 19:20 AMP
V34353
Phenanthrene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20 AMP
V34353
Phenol
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20 AMP
V34353
Pyrene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20 AMP
V34353
Pyridine
<0.443
mg/Kg - dry
0.443
1
06/14/23 19:20 AMP
V34353
1,2,4-Trichlorobenzene
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20 AMP
V34353
2,4,5-Trichlorophenol
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20 AMP
V34353
2,4,6-Trichlorophenol
<0.887
mg/Kg - dry
0.887
1
06/14/23 19:20 AMP
V34353
Surrogate: Phenol-d5
55.3
Limits: 34-121%
1 06/14/23 19:20 AMP
8270E
Surrogate:2-Fluorobiphenyl
72.9
Limits:44-115%
1 06/14/23 19:20 AMP
V34353
Surrogate:2-Fluorophenol
60.7
Limits:35-115%
1 06/14/23 19:20 AMP
V34353
Surrogate: Nitrobenzene-d5
70.5
Limits: 37-122%
1 06/14/23 19:20 AMP
V34353
Surrogate:4-Terphenyl-d14
75.9
Limits:54-127%
1 06/14/23 19:20 AMP
V34353
Surrogate: 2,4,6-Tribromophenol
54.7
Limits:39-132%
1 06/14/23 19:20 AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 75 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98064 Matrix: Solids
Sample ID: UST-2-C Sampled: 6/8/2023 17:35
Analytical Method: MADEP-EPH
Prep Method: MAEPH (Prep)
Test
Aliphatic C9-C18
Aliphatic C19-C36
Aromatic C11-C22
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Analytical Method: MADEP-VPH
Prep Method: MAVPH (Prep)
Test
Prep Batch(es): V34271 06/13/23 10:20
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
<66.9 mg/Kg - dry
66.9 1
06/16/23 21:50 AMP
V34449
<66.9 mg/Kg - dry
66.9 1
06/16/23 21:50 AMP
V34449
<66.9 mg/Kg - dry
66.9 1
06/16/23 21:50 AMP
V34449
115
Limits: 40-140%
1 06/16/23 21:50 AMP
MADEP-EPH
68.1
Limits: 40-140%
1 06/16/23 21:50 AMP
MADEP-EPH
106
Limits: 40-140%
1 06/16/23 21:50 AMP
MADEP-EPH
113
Limits: 40-140%
1 06/16/23 21:50 AMP
V34449
Prep Batch(es):
V34232 06/12/23 08:00
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Aliphatic C5-C8 <10.8
Aliphatic C9-C12 <10.8
Aromatic C9-C10 <10.8
Surrogate: 2,5-Dibromotoluene (FID)
Surrogate: 2,5-Dibromotoluene (PID)
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
mg/Kg - dry
10.8
100 06/12/23 16:48 TBL
V34233
mg/Kg - dry
10.8
100 06/12/23 16:48 TBL
V34233
mg/Kg - dry
10.8
100 06/12/23 16:48 TBL
V34233
96.3
Limits: 70-130%
100 06/12/23 16:48 TBL
MADEP-VPH
96.3
Limits: 70-130%
100 06/12/23 16:48 TBL
MADEP-VPH
DF Dilution Factor
Page 76 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98065 Matrix: Solids
Sample ID: UST-2-113 Sampled: 6/8/2023 15:50
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
31.8 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 77 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98065 Matrix: Solids
Sample ID: UST-2-D Sampled: 6/8/2023 15:50
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Acetone
<0.029
mg/Kg - dry
0.029
1
06/12/23 17:23
TBL
V34278
Acrolein
<0.029
mg/Kg - dry
0.029
1
06/12/23 17:23
TBL
V34278
Acrylonitrile
<0.029
mg/Kg - dry
0.029
1
06/12/23 17:23
TBL
V34278
Benzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Bromobenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Bromochloromethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Bromodichloromethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Bromoform
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Bromomethane
<0.014
mg/Kg - dry
0.014
1
06/12/23 17:23
TBL
V34278
n-Butylbenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
sec -Butyl benzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
tert-Butyl benzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Carbon Disulfide
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Carbon Tetrachloride
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Chlorobenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Chlorodibromomethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Chloroethane
<0.014
mg/Kg - dry
0.014
1
06/12/23 17:23
TBL
V34278
Chloroform
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Chloromethane
<0.014
mg/Kg - dry
0.014
1
06/12/23 17:23
TBL
V34278
2-Chlorotoluene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
4-Chlorotoluene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Di -Isopropyl Ether (DIPE)
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 78 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98065 Matrix: Solids
Sample ID: UST-2-D Sampled: 6/8/2023 15:50
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dibromo-3-Chloropropane
<0.014
mg/Kg - dry
0.014
1
06/12/23 17:23
TBL
V34278
1,2-Dibromoethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Dibromomethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
1,2-Dichlorobenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
1,3-Dichlorobenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
1,4-Dichlorobenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Dichlorodifluoromethane
<0.014
mg/Kg - dry
0.014
1
06/12/23 17:23
TBL
V34278
1,1-Dichloroethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
1,2-Dichloroethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
1,1-Dichloroethene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
cis- 1,2-Dich loroethene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
trans-1,2-Dichloroethene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
1,2-Dichloropropane
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
1,3-Dichloropropane
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
2,2-Dichloropropane
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
1,1-Dichloropropene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
cis-1,3-Dichloropropene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
trans-1,3-Dichloropropene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Ethanol
<0.366
mg/Kg - dry
0.366
1
06/12/23 17:23
TBL
V34278
Ethylbenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Ethyl Tertiary Butyl Ether (ETBE) <0.073
mg/Kg - dry
0.073
1
06/12/23 17:23
TBL
V34278
Hexachlorobutadiene
<0.014
mg/Kg - dry
0.014
1
06/12/23 17:23
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 79 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98065 Matrix: Solids
Sample ID: UST-2-D Sampled: 6/8/2023 15:50
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
n-Hexane
<0.014
mg/Kg - dry
0.014
1
06/12/23 17:23
TBL
V34278
2-Hexanone
<0.029
mg/Kg - dry
0.029
1
06/12/23 17:23
TBL
V34278
Isopropyl benzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
4-Isopropyl toluene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Methyl Ethyl Ketone (MEK)
<0.029
mg/Kg - dry
0.029
1
06/12/23 17:23
TBL
V34278
Methyl tert-butyl ether (MTBE) <0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
4-Methyl-2-Pentanone
<0.029
mg/Kg - dry
0.029
1
06/12/23 17:23
TBL
V34278
Methylene Chloride
<0.014
mg/Kg - dry
0.014
1
06/12/23 17:23
TBL
V34278
Naphthalene
<0.014
mg/Kg - dry
0.014
1
06/12/23 17:23
TBL
V34278
n-Propylbenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Styrene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
1,1,1,2-Tetrachloroethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
1,1,2,2-Tetrachloroethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Tetrachloroethene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Toluene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
1,2,3-Trichlorobenzene
<0.014
mg/Kg - dry
0.014
1
06/12/23 17:23
TBL
V34278
1,2,4-Trichlorobenzene
<0.014
mg/Kg - dry
0.014
1
06/12/23 17:23
TBL
V34278
1,1,1-Trichloroethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
1,1,2-Trichloroethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Trichloroethene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Trichlorofluoromethane
<0.014
mg/Kg - dry
0.014
1
06/12/23 17:23
TBL
V34278
1,2,3-Trichloropropane
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 80 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Report Date : 06/21/2023
Received : 06/09/2023
Lab No : 98065 Matrix: Solids
Sample ID: UST-2-D Sampled: 6/8/2023 15:50
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
1,3,5-Trimethyl benzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
Vinyl Acetate
<0.014
mg/Kg - dry
0.014
1
06/12/23 17:23
TBL
V34278
Vinyl Chloride
<0.014
mg/Kg - dry
0.014
1
06/12/23 17:23
TBL
V34278
o-Xylene
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
TBL
V34278
m,p-Xylene
<0.014
mg/Kg - dry
0.014
1
06/12/23 17:23
TBL
V34278
Xylene (Total)
<0.007
mg/Kg - dry
0.007
1
06/12/23 17:23
V34278
Surrogate:4-Bromofluorobenzene
102
Limits:70-130%
1 06/12/23 17:23 TBL
V34278
Surrogate: Dibromofluoromethane
107
Limits: 84-123%
1 06/12/23 17:23 TBL
V34278
Surrogate: Toluene-d8
96.6
Limits: 76-129%
1 06/12/23 17:23 TBL
V34278
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Acenaphthylene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Aniline
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Anthracene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Benzo(a)anthracene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Benzo(a)pyrene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Benzo(b)fluoranthene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Benzo(g,h,i)perylene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 81 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98065
Matrix: Solids
Sample ID: UST-2-D
Sampled:
6/8/2023 15:50
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzo(k)fluoranthene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Benzoic Acid
<2.93
mg/Kg - dry
2.93
1
06/14/23 23:50
AMP
V34353
Benzyl alcohol
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Bis(2-Chloroethoxy)methane
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Bis(2-Chloroethyl)ether
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Bis(2-Chloroisopropyl)ether
<0.483
mg/Kg - dry
0.483
1
06/14/23 23:50
AMP
V34353
Bis(2-ethylhexyl)phthalate
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
4-13romophenyl phenyl ether
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Butyl benzyl phthalate
<0.483
mg/Kg - dry
0.483
1
06/14/23 23:50
AMP
V34353
4-Chloro-3-methylphenol
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
4-Chloroaniline
<0.483
mg/Kg - dry
0.483
1
06/14/23 23:50
AMP
V34353
2-Chloronaphthalene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
2-Chlorophenol
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
4-Chlorophenyl phenyl ether
<1.47
mg/Kg - dry
1.47
1
06/14/23 23:50
AMP
V34353
Chrysene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Dibenz(a,h)anthracene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Dibenzofuran
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
1,2-Dichlorobenzene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
1,3-Dichlorobenzene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
1,4-Dichlorobenzene
<0.483
mg/Kg - dry
0.483
1
06/14/23 23:50
AMP
V34353
3,3'-Dichlorobenzidine
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
2,4-Dichlorophenol
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 82 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98065
Matrix: Solids
Sample ID: UST-2-D
Sampled:
6/8/2023 15:50
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Dimethyl phthalate
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
2,4-Dimethyl phenol
<0.483
mg/Kg - dry
0.483
1
06/14/23 23:50
AMP
V34353
Di-n-butyl phthalate
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
4,6-Dinitro-2-methylphenol
<2.20
mg/Kg - dry
2.20
1
06/14/23 23:50
AMP
V34353
2,4-Dinitrophenol
<2.20
mg/Kg - dry
2.20
1
06/14/23 23:50
AMP
V34353
2,4-Dinitrotoluene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
2,6-Dinitrotoluene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Di-n-Octyl Phthalate
<0.483
mg/Kg - dry
0.483
1
06/14/23 23:50
AMP
V34353
Fluoranthene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Fluorene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Hexachlorobenzene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Hexachlorobutadiene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Hexachlorocyclopentadiene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Hexachloroethane
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Indeno(1,2,3-cd)pyrene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Isophorone
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
1-Methylnaphthalene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
2-Methylnaphthalene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
2-Methylphenol
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
3&4 Methylphenol
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Naphthalene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 83 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98065
Matrix: Solids
Sample ID: UST-2-D
Sampled: 6/8/2023
15:50
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
2-Nitroaniline
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50 AMP
V34353
3-Nitroaniline
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50 AMP
V34353
4-Nitroaniline
<0.483
mg/Kg - dry
0.483
1
06/14/23 23:50 AMP
V34353
Nitrobenzene
<0.483
mg/Kg - dry
0.483
1
06/14/23 23:50 AMP
V34353
2-Nitrophenol
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50 AMP
V34353
4-Nitrophenol
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50 AMP
V34353
N-Nitrosodimethylamine
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50 AMP
V34353
N-Nitrosodiphenylamine
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50 AMP
V34353
N-Nitroso-di-n-propylamine
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50 AMP
V34353
Pentachlorophenol
<1.47
mg/Kg - dry
1.47
1
06/14/23 23:50 AMP
V34353
Phenanthrene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50 AMP
V34353
Phenol
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50 AMP
V34353
Pyrene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50 AMP
V34353
Pyridine
<0.483
mg/Kg - dry
0.483
1
06/14/23 23:50 AMP
V34353
1,2,4-Trichlorobenzene
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50 AMP
V34353
2,4,5-Trichlorophenol
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50 AMP
V34353
2,4,6-Trichlorophenol
<0.967
mg/Kg - dry
0.967
1
06/14/23 23:50 AMP
V34353
Surrogate: Phenol-d5
48.9
Limits: 34-121%
1 06/14/23 23:50 AMP
8270E
Surrogate: 2-Fluorobiphenyl
64.7
Limits: 44-115%
1 06/14/23 23:50 AMP
V34353
Surrogate: 2-Fluorophenol
53.5
Limits: 35-115%
1 06/14/23 23:50 AMP
V34353
Surrogate: Nitrobenzene-d5
61.1
Limits: 37-122%
1 06/14/23 23:50 AMP
V34353
Surrogate: 4-Terphenyl-d14
66.5
Limits: 54-127%
1 06/14/23 23:50 AMP
V34353
Surrogate: 2,4,6-Tribromophenol
50.2
Limits: 39-132%
1 06/14/23 23:50 AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 84 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98065 Matrix: Solids
Sample ID: UST-2-D Sampled: 6/8/2023 15:50
Analytical Method: MADEP-EPH
Prep Method: MAEPH (Prep)
Test
Aliphatic C9-C18
Aliphatic C19-C36
Aromatic C11-C22
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Analytical Method: MADEP-VPH
Prep Method: MAVPH (Prep)
Test
Prep Batch(es): V34271 06/13/23 10:20
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
<73.5 mg/Kg - dry
73.5 1
06/20/23 15:55 AMP
V34449
<73.5 mg/Kg - dry
73.5 1
06/20/23 15:55 AMP
V34449
131 mg/Kg - dry
73.5 1
06/20/23 15:55 AMP
V34449
117
Limits:40-140%
1 06/20/23 15:55 AMP
MADEP-EPH
63.1
Limits:40-140%
1 06/20/23 15:55 AMP
MADEP-EPH
91.1
Limits:40-140%
1 06/20/23 15:55 AMP
MADEP-EPH
114
Limits:40-140%
1 06/20/23 15:55 AMP
V34449
Prep Batch(es):
V34232 06/12/23 08:00
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Aliphatic C5-C8 <11.7
Aliphatic C9-C12 <11.7
Aromatic C9-C10 <11.7
Surrogate: 2,5-Dibromotoluene (FID)
Surrogate: 2,5-Dibromotoluene (PID)
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
mg/Kg - dry
11.7
100 06/12/23 17:11 TBL
V34233
mg/Kg - dry
11.7
100 06/12/23 17:11 TBL
V34233
mg/Kg - dry
11.7
100 06/12/23 17:11 TBL
V34233
114
Limits: 70-130%
100 06/12/23 17:11 TBL
MADEP-VPH
118
Limits: 70-130%
100 06/12/23 17:11 TBL
MADEP-VPH
DF Dilution Factor
Page 85 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98066 Matrix: Solids
Sample ID: UST-2-E Sampled: 6/8/2023 15:40
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
28.5 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 86 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98066 Matrix: Solids
Sample ID: UST-2-E Sampled: 6/8/2023 15:40
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Acetone
<0.027
mg/Kg - dry
0.027
1
06/12/23 17:50
TBL
V34278
Acrolein
<0.027
mg/Kg - dry
0.027
1
06/12/23 17:50
TBL
V34278
Acrylonitrile
<0.027
mg/Kg - dry
0.027
1
06/12/23 17:50
TBL
V34278
Benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Bromobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Bromochloromethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Bromodichloromethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Bromoform
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Bromomethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 17:50
TBL
V34278
n-Butylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
sec -Butyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
tert-Butyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Carbon Disulfide
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Carbon Tetrachloride
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Chlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Chlorodibromomethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Chloroethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 17:50
TBL
V34278
Chloroform
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Chloromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 17:50
TBL
V34278
2-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
4-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Di -Isopropyl Ether (DIPE)
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 87 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98066 Matrix: Solids
Sample ID: UST-2-E Sampled: 6/8/2023 15:40
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dibromo-3-Chloropropane
<0.013
mg/Kg - dry
0.013
1
06/12/23 17:50
TBL
V34278
1,2-Dibromoethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Dibromomethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
1,2-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
1,3-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
1,4-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Dichlorodifluoromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 17:50
TBL
V34278
1,1-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
1,2-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
1,1-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
cis- 1,2-Dich loroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
trans-1,2-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
1,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
1,3-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
2,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
1,1-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
cis-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
trans-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Ethanol
<0.349
mg/Kg - dry
0.349
1
06/12/23 17:50
TBL
V34278
Ethylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Ethyl Tertiary Butyl Ether (ETBE) <0.069
mg/Kg - dry
0.069
1
06/12/23 17:50
TBL
V34278
Hexachlorobutadiene
<0.013
mg/Kg - dry
0.013
1
06/12/23 17:50
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 88 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98066 Matrix: Solids
Sample ID: UST-2-E Sampled: 6/8/2023 15:40
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
n-Hexane
<0.013
mg/Kg - dry
0.013
1
06/12/23 17:50
TBL
V34278
2-Hexanone
<0.027
mg/Kg - dry
0.027
1
06/12/23 17:50
TBL
V34278
Isopropyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
4-Isopropyl toluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Methyl Ethyl Ketone (MEK)
<0.027
mg/Kg - dry
0.027
1
06/12/23 17:50
TBL
V34278
Methyl tert-butyl ether (MTBE) <0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
4-Methyl-2-Pentanone
<0.027
mg/Kg - dry
0.027
1
06/12/23 17:50
TBL
V34278
Methylene Chloride
<0.013
mg/Kg - dry
0.013
1
06/12/23 17:50
TBL
V34278
Naphthalene
<0.013
mg/Kg - dry
0.013
1
06/12/23 17:50
TBL
V34278
n-Propylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Styrene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
1,1,1,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
1,1,2,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Tetrachloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Toluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
1,2,3-Trichlorobenzene
<0.013
mg/Kg - dry
0.013
1
06/12/23 17:50
TBL
V34278
1,2,4-Trichlorobenzene
<0.013
mg/Kg - dry
0.013
1
06/12/23 17:50
TBL
V34278
1,1,1-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
1,1,2-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Trichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Trichlorofluoromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 17:50
TBL
V34278
1,2,3-Trichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 89 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Report Date : 06/21/2023
Received : 06/09/2023
Lab No : 98066 Matrix: Solids
Sample ID: UST-2-E Sampled: 6/8/2023 15:40
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
1,3,5-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
Vinyl Acetate
<0.013
mg/Kg - dry
0.013
1
06/12/23 17:50
TBL
V34278
Vinyl Chloride
<0.013
mg/Kg - dry
0.013
1
06/12/23 17:50
TBL
V34278
o-Xylene
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
TBL
V34278
m,p-Xylene
<0.013
mg/Kg - dry
0.013
1
06/12/23 17:50
TBL
V34278
Xylene (Total)
<0.006
mg/Kg - dry
0.006
1
06/12/23 17:50
V34278
Surrogate:4-Bromofluorobenzene
101
Limits:70-130%
1 06/12/23 17:50 TBL
V34278
Surrogate: Dibromofluoromethane
107
Limits: 84-123%
1 06/12/23 17:50 TBL
V34278
Surrogate: Toluene-d8
95.4
Limits: 76-129%
1 06/12/23 17:50 TBL
V34278
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Acenaphthylene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Aniline
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Anthracene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Benzo(a)anthracene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Benzo(a)pyrene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Benzo(b)fluoranthene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Benzo(g,h,i)perylene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 90 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98066
Matrix: Solids
Sample ID: UST-2-E
Sampled:
6/8/2023 15:40
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzo(k)fluoranthene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Benzoic Acid
<2.80
mg/Kg - dry
2.80
1
06/14/23 19:42
AMP
V34353
Benzyl alcohol
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Bis(2-Chloroethoxy)methane
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Bis(2-Chloroethyl)ether
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Bis(2-Chloroisopropyl)ether
<0.461
mg/Kg - dry
0.461
1
06/14/23 19:42
AMP
V34353
Bis(2-ethylhexyl)phthalate
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
4-13romophenyl phenyl ether
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Butyl benzyl phthalate
<0.461
mg/Kg - dry
0.461
1
06/14/23 19:42
AMP
V34353
4-Chloro-3-methylphenol
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
4-Chloroaniline
<0.461
mg/Kg - dry
0.461
1
06/14/23 19:42
AMP
V34353
2-Chloronaphthalene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
2-Chlorophenol
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
4-Chlorophenyl phenyl ether
<1.40
mg/Kg - dry
1.40
1
06/14/23 19:42
AMP
V34353
Chrysene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Dibenz(a,h)anthracene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Dibenzofuran
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
1,2-Dichlorobenzene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
1,3-Dichlorobenzene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
1,4-Dichlorobenzene
<0.461
mg/Kg - dry
0.461
1
06/14/23 19:42
AMP
V34353
3,3'-Dichlorobenzidine
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
2,4-Dichlorophenol
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 91 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98066
Matrix: Solids
Sample ID: UST-2-E
Sampled:
6/8/2023 15:40
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Dimethyl phthalate
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
2,4-Dimethyl phenol
<0.461
mg/Kg - dry
0.461
1
06/14/23 19:42
AMP
V34353
Di-n-butyl phthalate
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
4,6-Dinitro-2-methylphenol
<2.10
mg/Kg - dry
2.10
1
06/14/23 19:42
AMP
V34353
2,4-Dinitrophenol
<2.10
mg/Kg - dry
2.10
1
06/14/23 19:42
AMP
V34353
2,4-Dinitrotoluene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
2,6-Dinitrotoluene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Di-n-Octyl Phthalate
<0.461
mg/Kg - dry
0.461
1
06/14/23 19:42
AMP
V34353
Fluoranthene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Fluorene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Hexachlorobenzene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Hexachlorobutadiene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Hexachlorocyclopentadiene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Hexachloroethane
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Indeno(1,2,3-cd)pyrene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Isophorone
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
1-Methylnaphthalene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
2-Methylnaphthalene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
2-Methylphenol
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
3&4 Methylphenol
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Naphthalene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 92 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98066
Matrix: Solids
Sample ID: UST-2-E
Sampled: 6/8/2023
15:40
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
2-Nitroaniline
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42 AMP
V34353
3-Nitroaniline
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42 AMP
V34353
4-Nitroaniline
<0.461
mg/Kg - dry
0.461
1
06/14/23 19:42 AMP
V34353
Nitrobenzene
<0.461
mg/Kg - dry
0.461
1
06/14/23 19:42 AMP
V34353
2-Nitrophenol
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42 AMP
V34353
4-Nitrophenol
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42 AMP
V34353
N-Nitrosodimethylamine
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42 AMP
V34353
N-Nitrosodiphenylamine
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42 AMP
V34353
N-Nitroso-di-n-propylamine
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42 AMP
V34353
Pentachlorophenol
<1.40
mg/Kg - dry
1.40
1
06/14/23 19:42 AMP
V34353
Phenanthrene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42 AMP
V34353
Phenol
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42 AMP
V34353
Pyrene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42 AMP
V34353
Pyridine
<0.461
mg/Kg - dry
0.461
1
06/14/23 19:42 AMP
V34353
1,2,4-Trichlorobenzene
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42 AMP
V34353
2,4,5-Trichlorophenol
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42 AMP
V34353
2,4,6-Trichlorophenol
<0.923
mg/Kg - dry
0.923
1
06/14/23 19:42 AMP
V34353
Surrogate: Phenol-d5
58.3
Limits: 34-121%
1 06/14/23 19:42 AMP
8270E
Surrogate:2-Fluorobiphenyl
72.9
Limits:44-115%
1 06/14/23 19:42 AMP
V34353
Surrogate:2-Fluorophenol
63.1
Limits:35-115%
1 06/14/23 19:42 AMP
V34353
Surrogate: Nitrobenzene-d5
69.9
Limits: 37-122%
1 06/14/23 19:42 AMP
V34353
Surrogate:4-Terphenyl-d14
78.3
Limits:54-127%
1 06/14/23 19:42 AMP
V34353
Surrogate: 2,4,6-Tribromophenol
53.8
Limits:39-132%
1 06/14/23 19:42 AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 93 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98066 Matrix: Solids
Sample ID: UST-2-E Sampled: 6/8/2023 15:40
Analytical Method: MADEP-EPH
Prep Method: MAEPH (Prep)
Test
Aliphatic C9-C18
Aliphatic C19-C36
Aromatic C11-C22
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Analytical Method: MADEP-VPH
Prep Method: MAVPH (Prep)
Test
Prep Batch(es): V34271 06/13/23 10:20
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
<69.7 mg/Kg - dry
69.7 1
06/16/23 23:03 AMP
V34449
<69.7 mg/Kg - dry
69.7 1
06/16/23 23:03 AMP
V34449
<69.7 mg/Kg - dry
69.7 1
06/16/23 23:03 AMP
V34449
116
Limits: 40-140%
1 06/16/23 23:03 AMP
MADEP-EPH
74.0
Limits: 40-140%
1 06/16/23 23:03 AMP
MADEP-EPH
107
Limits: 40-140%
1 06/16/23 23:03 AMP
MADEP-EPH
114
Limits: 40-140%
1 06/16/23 23:03 AMP
V34449
Prep Batch(es):
V34232 06/12/23 08:00
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Aliphatic C5-C8 <11.2
Aliphatic C9-C12 <11.2
Aromatic C9-C10 <11.2
Surrogate: 2,5-Dibromotoluene (FID)
Surrogate: 2,5-Dibromotoluene (PID)
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
mg/Kg - dry
11.2
100 06/12/23 17:35 TBL
V34233
mg/Kg - dry
11.2
100 06/12/23 17:35 TBL
V34233
mg/Kg - dry
11.2
100 06/12/23 17:35 TBL
V34233
108
Limits: 70-130%
100 06/12/23 17:35 TBL
MADEP-VPH
106
Limits: 70-130%
100 06/12/23 17:35 TBL
MADEP-VPH
DF Dilution Factor
Page 94 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98067 Matrix: Solids
Sample ID: UST-24 Sampled: 6/8/2023 17:45
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
36.1 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 95 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98067 Matrix: Solids
Sample ID: UST-2-F Sampled: 6/8/2023 17:45
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Acetone
<0.031
mg/Kg - dry
0.031
1
06/12/23 18:18
TBL
V34278
Acrolein
<0.031
mg/Kg - dry
0.031
1
06/12/23 18:18
TBL
V34278
Acrylonitrile
<0.031
mg/Kg - dry
0.031
1
06/12/23 18:18
TBL
V34278
Benzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Bromobenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Bromochloromethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Bromodichloromethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Bromoform
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Bromomethane
<0.015
mg/Kg - dry
0.015
1
06/12/23 18:18
TBL
V34278
n-Butylbenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
sec -Butyl benzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
tert-Butyl benzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Carbon Disulfide
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Carbon Tetrachloride
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Chlorobenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Chlorodibromomethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Chloroethane
<0.015
mg/Kg - dry
0.015
1
06/12/23 18:18
TBL
V34278
Chloroform
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Chloromethane
<0.015
mg/Kg - dry
0.015
1
06/12/23 18:18
TBL
V34278
2-Chlorotoluene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
4-Chlorotoluene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Di -Isopropyl Ether (DIPE)
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 96 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98067 Matrix: Solids
Sample ID: UST-2-F Sampled: 6/8/2023 17:45
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dibromo-3-Chloropropane
<0.015
mg/Kg - dry
0.015
1
06/12/23 18:18
TBL
V34278
1,2-Dibromoethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Dibromomethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
1,2-Dichlorobenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
1,3-Dichlorobenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
1,4-Dichlorobenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Dichlorodifluoromethane
<0.015
mg/Kg - dry
0.015
1
06/12/23 18:18
TBL
V34278
1,1-Dichloroethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
1,2-Dichloroethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
1,1-Dichloroethene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
cis- 1,2-Dich loroethene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
trans-1,2-Dichloroethene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
1,2-Dichloropropane
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
1,3-Dichloropropane
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
2,2-Dichloropropane
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
1,1-Dichloropropene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
cis-1,3-Dichloropropene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
trans-1,3-Dichloropropene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Ethanol
<0.391
mg/Kg - dry
0.391
1
06/12/23 18:18
TBL
V34278
Ethylbenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Ethyl Tertiary Butyl Ether (ETBE) <0.078
mg/Kg - dry
0.078
1
06/12/23 18:18
TBL
V34278
Hexachlorobutadiene
<0.015
mg/Kg - dry
0.015
1
06/12/23 18:18
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 97 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98067 Matrix: Solids
Sample ID: UST-2-F Sampled: 6/8/2023 17:45
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
n-Hexane
<0.015
mg/Kg - dry
0.015
1
06/12/23 18:18
TBL
V34278
2-Hexanone
<0.031
mg/Kg - dry
0.031
1
06/12/23 18:18
TBL
V34278
Isopropyl benzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
4-Isopropyl toluene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Methyl Ethyl Ketone (MEK)
<0.031
mg/Kg - dry
0.031
1
06/12/23 18:18
TBL
V34278
Methyl tert-butyl ether (MTBE) <0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
4-Methyl-2-Pentanone
<0.031
mg/Kg - dry
0.031
1
06/12/23 18:18
TBL
V34278
Methylene Chloride
<0.015
mg/Kg - dry
0.015
1
06/12/23 18:18
TBL
V34278
Naphthalene
<0.015
mg/Kg - dry
0.015
1
06/12/23 18:18
TBL
V34278
n-Propylbenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Styrene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
1,1,1,2-Tetrachloroethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
1,1,2,2-Tetrachloroethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Tetrachloroethene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Toluene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
1,2,3-Trichlorobenzene
<0.015
mg/Kg - dry
0.015
1
06/12/23 18:18
TBL
V34278
1,2,4-Trichlorobenzene
<0.015
mg/Kg - dry
0.015
1
06/12/23 18:18
TBL
V34278
1,1,1-Trichloroethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
1,1,2-Trichloroethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Trichloroethene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Trichlorofluoromethane
<0.015
mg/Kg - dry
0.015
1
06/12/23 18:18
TBL
V34278
1,2,3-Trichloropropane
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 98 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Report Date : 06/21/2023
Received : 06/09/2023
Lab No : 98067 Matrix: Solids
Sample ID: UST-2-F Sampled: 6/8/2023 17:45
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
1,3,5-Trimethyl benzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
Vinyl Acetate
<0.015
mg/Kg - dry
0.015
1
06/12/23 18:18
TBL
V34278
Vinyl Chloride
<0.015
mg/Kg - dry
0.015
1
06/12/23 18:18
TBL
V34278
o-Xylene
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
TBL
V34278
m,p-Xylene
<0.015
mg/Kg - dry
0.015
1
06/12/23 18:18
TBL
V34278
Xylene (Total)
<0.007
mg/Kg - dry
0.007
1
06/12/23 18:18
V34278
Surrogate:4-Bromofluorobenzene
101
Limits:70-130%
1 06/12/23 18:18 TBL
V34278
Surrogate: Dibromofluoromethane
105
Limits: 84-123%
1 06/12/23 18:18 TBL
V34278
Surrogate: Toluene-d8
96.6
Limits: 76-129%
1 06/12/23 18:18 TBL
V34278
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Acenaphthylene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Aniline
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Anthracene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Benzo(a)anthracene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Benzo(a)pyrene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Benzo(b)fluoranthene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Benzo(g,h,i)perylene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 99 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98067
Matrix: Solids
Sample ID: UST-2-F
Sampled:
6/8/2023 17:45
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzo(k)fluoranthene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Benzoic Acid
<3.13
mg/Kg - dry
3.13
1
06/14/23 23:05
AMP
V34353
Benzyl alcohol
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Bis(2-Chloroethoxy)methane
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Bis(2-Chloroethyl)ether
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Bis(2-Chloroisopropyl)ether
<0.517
mg/Kg - dry
0.517
1
06/14/23 23:05
AMP
V34353
Bis(2-ethylhexyl)phthalate
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
4-13romophenyl phenyl ether
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Butyl benzyl phthalate
<0.517
mg/Kg - dry
0.517
1
06/14/23 23:05
AMP
V34353
4-Chloro-3-methylphenol
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
4-Chloroaniline
<0.517
mg/Kg - dry
0.517
1
06/14/23 23:05
AMP
V34353
2-Chloronaphthalene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
2-Chlorophenol
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
4-Chlorophenyl phenyl ether
<1.56
mg/Kg - dry
1.56
1
06/14/23 23:05
AMP
V34353
Chrysene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Dibenz(a,h)anthracene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Dibenzofuran
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
1,2-Dichlorobenzene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
1,3-Dichlorobenzene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
1,4-Dichlorobenzene
<0.517
mg/Kg - dry
0.517
1
06/14/23 23:05
AMP
V34353
3,3'-Dichlorobenzidine
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
2,4-Dichlorophenol
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 100 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98067
Matrix: Solids
Sample ID: UST-2-F
Sampled:
6/8/2023 17:45
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Dimethyl phthalate
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
2,4-Dimethyl phenol
<0.517
mg/Kg - dry
0.517
1
06/14/23 23:05
AMP
V34353
Di-n-butyl phthalate
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
4,6- Din itro-2- methyl phenol
<2.35
mg/Kg - dry
2.35
1
06/14/23 23:05
AMP
V34353
2,4-Dinitrophenol
<2.35
mg/Kg - dry
2.35
1
06/14/23 23:05
AMP
V34353
2,4-Dinitrotoluene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
2,6-Dinitrotoluene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Di-n-Octyl Phthalate
<0.517
mg/Kg - dry
0.517
1
06/14/23 23:05
AMP
V34353
Fluoranthene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Fluorene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Hexachlorobenzene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Hexachlorobutadiene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Hexachlorocyclopentadiene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Hexachloroethane
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Indeno(1,2,3-cd)pyrene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Isophorone
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
1-Methylnaphthalene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
2-Methylnaphthalene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
2-Methylphenol
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
3&4 Methylphenol
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Naphthalene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 101 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98067
Matrix: Solids
Sample ID: UST-2-F
Sampled: 6/8/2023
17:45
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
2-Nitroaniline
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05 AMP
V34353
3-Nitroaniline
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05 AMP
V34353
4-Nitroaniline
<0.517
mg/Kg - dry
0.517
1
06/14/23 23:05 AMP
V34353
Nitrobenzene
<0.517
mg/Kg - dry
0.517
1
06/14/23 23:05 AMP
V34353
2-Nitrophenol
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05 AMP
V34353
4-Nitrophenol
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05 AMP
V34353
N-N itrosodimethyla mine
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05 AMP
V34353
N-Nitrosodiphenylamine
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05 AMP
V34353
N-Nitroso-di-n-propylamine
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05 AMP
V34353
Pentachlorophenol
<1.56
mg/Kg - dry
1.56
1
06/14/23 23:05 AMP
V34353
Phenanthrene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05 AMP
V34353
Phenol
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05 AMP
V34353
Pyrene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05 AMP
V34353
Pyridine
<0.517
mg/Kg - dry
0.517
1
06/14/23 23:05 AMP
V34353
1,2,4-Trichlorobenzene
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05 AMP
V34353
2,4,5-Trichlorophenol
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05 AMP
V34353
2,4,6-Trichlorophenol
<1.03
mg/Kg - dry
1.03
1
06/14/23 23:05 AMP
V34353
Surrogate: Phenol-d5
53.3
Limits: 34-121%
1 06/14/23 23:05 AMP
8270E
Surrogate: 2-Fluorobiphenyl
67.7
Limits: 44-115%
1 06/14/23 23:05 AMP
V34353
Surrogate: 2-Fluorophenol
57.8
Limits: 35-115%
1 06/14/23 23:05 AMP
V34353
Surrogate: Nitrobenzene-d5
63.5
Limits: 37-122%
1 06/14/23 23:05 AMP
V34353
Surrogate: 4-Terphenyl-d14
71.9
Limits: 54-127%
1 06/14/23 23:05 AMP
V34353
Surrogate: 2,4,6-Tribromophenol
56.6
Limits: 39-132%
1 06/14/23 23:05 AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 102 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98067 Matrix: Solids
Sample ID: UST-24 Sampled: 6/8/2023 17:45
Analytical Method: MADEP-EPH
Prep Method: MAEPH (Prep)
Test
Aliphatic C9-C18
Aliphatic C19-C36
Aromatic C11-C22
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Analytical Method: MADEP-VPH
Prep Method: MAVPH (Prep)
Test
Prep Batch(es): V34271 06/13/23 10:20
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
218 mg/Kg - dry
77.9 1
06/20/23 16:32 AMP
V34449
93.1 mg/Kg - dry
77.9 1
06/20/23 16:32 AMP
V34449
224 mg/Kg - dry
77.9 1
06/20/23 16:32 AMP
V34449
104
Limits:40-140%
1 06/20/23 16:32 AMP
MADEP-EPH
47.4
Limits:40-140%
1 06/20/23 16:32 AMP
MADEP-EPH
79.3
Limits:40-140%
1 06/20/23 16:32 AMP
MADEP-EPH
96.7
Limits:40-140%
1 06/20/23 16:32 AMP
V34449
Prep Batch(es):
V34232 06/12/23 08:00
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Aliphatic C5-C8 <12.5
Aliphatic C9-C12 <12.5
Aromatic C9-C10 <12.5
Surrogate: 2,5-Dibromotoluene (FID)
Surrogate: 2,5-Dibromotoluene (PID)
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
mg/Kg - dry
12.5
100 06/12/23 21:30 TBL
V34233
mg/Kg - dry
12.5
100 06/12/23 21:30 TBL
V34233
mg/Kg - dry
12.5
100 06/12/23 21:30 TBL
V34233
96.3
Limits: 70-130%
100 06/12/23 21:30 TBL
MADEP-VPH
103
Limits: 70-130%
100 06/12/23 21:30 TBL
MADEP-VPH
DF Dilution Factor
Page 103 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98068 Matrix: Solids
Sample ID: UST-3-A Sampled: 6/8/2023 16:10
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
31.6 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 104 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001
REPOR T OF A NA L YSIS
Lab No : 98068
Matrix: Solids
Sample ID: UST-3-A
Sampled: 6/8/2023
16:10
Analytical Method: 8015C DRO
Prep Batch(es):
V34382
06/15/23 10:30
Prep Method: 3546
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
<14.6
mg/Kg - dry
14.6
1 06/16/23 02:43 TJW
V34417
Surrogate: OTP Surrogate
66.4
Limits: 31-123% 1 06/16/23 02:43 TJW
8015C DRO
Analytical Method: 8015C GRO
Prep Batch(es):
V34234
06/12/23 08:00
Prep Method: 5035 MED
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
<7.31
mg/Kg - dry
7.31
50 06/12/23 22:14 TBL
V34235
Surrogate: a,a,a-Trifluorotoluene
108
Limits: 50-137% 50 06/12/23 22:14 TBL
8015C GRO
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
DF Dilution Factor
Page 105 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98069 Matrix: Solids
Sample ID: UST-3-B Sampled: 6/8/2023 16:50
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
34.3 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 106 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001
REPOR T OF A NA L YSIS
Lab No : 98069
Matrix: Solids
Sample ID: UST-3-B
Sampled: 6/8/2023
16:50
Analytical Method: 8015C DRO
Prep Batch(es):
V34382
06/15/23 10:30
Prep Method: 3546
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
18.9
mg/Kg - dry
18.3
1 06/16/23 03:05 TJW
V34417
Surrogate: OTP Surrogate
71.3
Limits: 31-123% 1 06/16/23 03:05 TJW
8015C DRO
Analytical Method: 8015C GRO
Prep Batch(es):
V34275
06/13/23 08:00
Prep Method: 5035 MED
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
<7.61
mg/Kg - dry
7.61
50 06/13/23 12:03 TBL
V34276
Surrogate: a,a,a-Trifluorotoluene
115
Limits: 50-137% 50 06/13/23 12:03 TBL
8015C GRO
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
DF Dilution Factor
Page 107 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98070 Matrix: Solids
Sample ID: UST-1-C Sampled: 6/9/2023 14:45
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
26.1 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 108 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98070
Matrix: Solids
Sample ID: UST-1-C
Sampled:
6/9/2023 14:45
Analytical Method: 8260D
Prep Batch(es):
V34277
06/12/23 08:00
Prep Method: 5035
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<0.027
mg/Kg - dry
0.027
1
06/12/23 18:45
TBL
V34278
Acrolein
<0.027
mg/Kg - dry
0.027
1
06/12/23 18:45
TBL
V34278
Acrylonitrile
<0.027
mg/Kg - dry
0.027
1
06/12/23 18:45
TBL
V34278
Benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Bromobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Bromochloromethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Bromodichloromethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Bromoform
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Bromomethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 18:45
TBL
V34278
n-Butylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
sec -Butyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
tert-Butyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Carbon Disulfide
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Carbon Tetrachloride
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Chlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Chlorodibromomethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Chloroethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 18:45
TBL
V34278
Chloroform
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Chloromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 18:45
TBL
V34278
2-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
4-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Di -Isopropyl Ether (DIPE)
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 109 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98070
Matrix: Solids
Sample ID: UST-1-C
Sampled:
6/9/2023 14:45
Analytical Method: 8260D
Prep Batch(es):
V34277
06/12/23 08:00
Prep Method: 5035
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,2-Dibromo-3-Chloropropane
<0.013
mg/Kg - dry
0.013
1
06/12/23 18:45
TBL
V34278
1,2-Dibromoethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Dibromomethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
1,2-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
1,3-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
1,4-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Dichlorodifluoromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 18:45
TBL
V34278
1,1-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
1,2-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
1,1-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
cis- 1,2-Dich loroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
trans-1,2-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
1,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
1,3-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
2,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
1,1-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
cis-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
trans-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Ethanol
<0.338
mg/Kg - dry
0.338
1
06/12/23 18:45
TBL
V34278
Ethylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Ethyl Tertiary Butyl Ether (ETBE)
<0.067
mg/Kg - dry
0.067
1
06/12/23 18:45
TBL
V34278
Hexachlorobutadiene
<0.013
mg/Kg - dry
0.013
1
06/12/23 18:45
TBL
V34278
Qualifiers/ * Outside QC Limit
DF Dilution Factor
Definitions MQL Method Quantitation Limit
Page 110 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98070 Matrix: Solids
Sample ID: UST-1-C Sampled: 6/9/2023 14:45
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
n-Hexane
<0.013
mg/Kg - dry
0.013
1
06/12/23 18:45
TBL
V34278
2-Hexanone
<0.027
mg/Kg - dry
0.027
1
06/12/23 18:45
TBL
V34278
Isopropyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
4-Isopropyl toluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Methyl Ethyl Ketone (MEK)
<0.027
mg/Kg - dry
0.027
1
06/12/23 18:45
TBL
V34278
Methyl tert-butyl ether (MTBE) <0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
4-Methyl-2-Pentanone
<0.027
mg/Kg - dry
0.027
1
06/12/23 18:45
TBL
V34278
Methylene Chloride
<0.013
mg/Kg - dry
0.013
1
06/12/23 18:45
TBL
V34278
Naphthalene
<0.013
mg/Kg - dry
0.013
1
06/12/23 18:45
TBL
V34278
n-Propylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Styrene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
1,1,1,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
1,1,2,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Tetrachloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Toluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
1,2,3-Trichlorobenzene
<0.013
mg/Kg - dry
0.013
1
06/12/23 18:45
TBL
V34278
1,2,4-Trichlorobenzene
<0.013
mg/Kg - dry
0.013
1
06/12/23 18:45
TBL
V34278
1,1,1-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
1,1,2-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Trichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Trichlorofluoromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 18:45
TBL
V34278
1,2,3-Trichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 111 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Report Date : 06/21/2023
Received : 06/09/2023
Lab No : 98070 Matrix: Solids
Sample ID: UST-1-C Sampled: 6/9/2023 14:45
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
1,3,5-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
Vinyl Acetate
<0.013
mg/Kg - dry
0.013
1
06/12/23 18:45
TBL
V34278
Vinyl Chloride
<0.013
mg/Kg - dry
0.013
1
06/12/23 18:45
TBL
V34278
o-Xylene
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
TBL
V34278
m,p-Xylene
<0.013
mg/Kg - dry
0.013
1
06/12/23 18:45
TBL
V34278
Xylene (Total)
<0.006
mg/Kg - dry
0.006
1
06/12/23 18:45
V34278
Surrogate:4-Bromofluorobenzene
101
Limits:70-130%
1 06/12/23 18:45 TBL
V34278
Surrogate: Dibromofluoromethane
105
Limits: 84-123%
1 06/12/23 18:45 TBL
V34278
Surrogate: Toluene-d8
96.4
Limits: 76-129%
1 06/12/23 18:45 TBL
V34278
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Acenaphthylene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Aniline
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Anthracene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Benzo(a)anthracene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Benzo(a)pyrene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Benzo(b)fluoranthene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Benzo(g,h,i)perylene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 112 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98070
Matrix: Solids
Sample ID: UST-1-C
Sampled:
6/9/2023 14:45
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzo(k)fluoranthene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Benzoic Acid
<2.71
mg/Kg - dry
2.71
1
06/14/23 20:05
AMP
V34353
Benzyl alcohol
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Bis(2-Chloroethoxy)methane
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Bis(2-Chloroethyl)ether
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Bis(2-Chloroisopropyl)ether
<0.446
mg/Kg - dry
0.446
1
06/14/23 20:05
AMP
V34353
Bis(2-ethylhexyl)phthalate
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
4-13romophenyl phenyl ether
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Butyl benzyl phthalate
<0.446
mg/Kg - dry
0.446
1
06/14/23 20:05
AMP
V34353
4-Chloro-3-methylphenol
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
4-Chloroaniline
<0.446
mg/Kg - dry
0.446
1
06/14/23 20:05
AMP
V34353
2-Chloronaphthalene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
2-Chlorophenol
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
4-Chlorophenyl phenyl ether
<1.35
mg/Kg - dry
1.35
1
06/14/23 20:05
AMP
V34353
Chrysene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Dibenz(a,h)anthracene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Dibenzofuran
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
1,2-Dichlorobenzene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
1,3-Dichlorobenzene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
1,4-Dichlorobenzene
<0.446
mg/Kg - dry
0.446
1
06/14/23 20:05
AMP
V34353
3,3'-Dichlorobenzidine
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
2,4-Dichlorophenol
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 113 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98070
Matrix: Solids
Sample ID: UST-1-C
Sampled:
6/9/2023 14:45
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Dimethyl phthalate
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
2,4-Dimethyl phenol
<0.446
mg/Kg - dry
0.446
1
06/14/23 20:05
AMP
V34353
Di-n-butyl phthalate
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
4,6-Dinitro-2-methylphenol
<2.03
mg/Kg - dry
2.03
1
06/14/23 20:05
AMP
V34353
2,4-Dinitrophenol
<2.03
mg/Kg - dry
2.03
1
06/14/23 20:05
AMP
V34353
2,4-Dinitrotoluene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
2,6-Dinitrotoluene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Di-n-Octyl Phthalate
<0.446
mg/Kg - dry
0.446
1
06/14/23 20:05
AMP
V34353
Fluoranthene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Fluorene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Hexachlorobenzene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Hexachlorobutadiene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Hexachlorocyclopentadiene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Hexachloroethane
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Indeno(1,2,3-cd)pyrene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Isophorone
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
1-Methylnaphthalene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
2-Methylnaphthalene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
2-Methylphenol
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
3&4 Methylphenol
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Naphthalene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 114 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98070
Matrix: Solids
Sample ID: UST-1-C
Sampled: 6/9/2023
14:45
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
2-Nitroaniline
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05 AMP
V34353
3-Nitroaniline
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05 AMP
V34353
4-Nitroaniline
<0.446
mg/Kg - dry
0.446
1
06/14/23 20:05 AMP
V34353
Nitrobenzene
<0.446
mg/Kg - dry
0.446
1
06/14/23 20:05 AMP
V34353
2-Nitrophenol
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05 AMP
V34353
4-Nitrophenol
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05 AMP
V34353
N-Nitrosodimethylamine
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05 AMP
V34353
N-Nitrosodiphenylamine
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05 AMP
V34353
N-Nitroso-di-n-propylamine
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05 AMP
V34353
Pentachlorophenol
<1.35
mg/Kg - dry
1.35
1
06/14/23 20:05 AMP
V34353
Phenanthrene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05 AMP
V34353
Phenol
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05 AMP
V34353
Pyrene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05 AMP
V34353
Pyridine
<0.446
mg/Kg - dry
0.446
1
06/14/23 20:05 AMP
V34353
1,2,4-Trichlorobenzene
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05 AMP
V34353
2,4,5-Trichlorophenol
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05 AMP
V34353
2,4,6-Trichlorophenol
<0.893
mg/Kg - dry
0.893
1
06/14/23 20:05 AMP
V34353
Surrogate: Phenol-d5
59.8
Limits: 34-121%
1 06/14/23 20:05 AMP
8270E
Surrogate: 2-Fluorobiphenyl
75.4
Limits: 44-115%
1 06/14/23 20:05 AMP
V34353
Surrogate: 2-Fluorophenol
64.6
Limits: 35-115%
1 06/14/23 20:05 AMP
V34353
Surrogate: Nitrobenzene-d5
71.3
Limits: 37-122%
1 06/14/23 20:05 AMP
V34353
Surrogate: 4-Terphenyl-d14
79.0
Limits: 54-127%
1 06/14/23 20:05 AMP
V34353
Surrogate: 2,4,6-Tribromophenol
58.0
Limits: 39-132%
1 06/14/23 20:05 AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 115 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98070 Matrix: Solids
Sample ID: UST-1-C Sampled: 6/9/2023 14:45
Analytical Method: MADEP-EPH
Prep Method: MAEPH (Prep)
Test
Aliphatic C9-C18
Aliphatic C19-C36
Aromatic C11-C22
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Analytical Method: MADEP-VPH
Prep Method: MAVPH (Prep)
Test
Prep Batch(es): V34271 06/13/23 10:20
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
<67.9 mg/Kg - dry
67.9 1
06/17/23 00:16 AMP
V34449
<67.9 mg/Kg - dry
67.9 1
06/17/23 00:16 AMP
V34449
<67.9 mg/Kg - dry
67.9 1
06/17/23 00:16 AMP
V34449
125
Limits: 40-140%
1 06/17/23 00:16 AMP
MADEP-EPH
68.3
Limits: 40-140%
1 06/17/23 00:16 AMP
MADEP-EPH
114
Limits: 40-140%
1 06/17/23 00:16 AMP
MADEP-EPH
122
Limits: 40-140%
1 06/17/23 00:16 AMP
V34449
Prep Batch(es):
V34232 06/12/23 08:00
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Aliphatic C5-C8 <10.8
Aliphatic C9-C12 <10.8
Aromatic C9-C10 <10.8
Surrogate: 2,5-Dibromotoluene (FID)
Surrogate: 2,5-Dibromotoluene (PID)
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
mg/Kg - dry
10.8
100 06/12/23 17:58 TBL
V34233
mg/Kg - dry
10.8
100 06/12/23 17:58 TBL
V34233
mg/Kg - dry
10.8
100 06/12/23 17:58 TBL
V34233
99.1
Limits: 70-130%
100 06/12/23 17:58 TBL
MADEP-VPH
100
Limits: 70-130%
100 06/12/23 17:58 TBL
MADEP-VPH
DF Dilution Factor
Page 116 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98071 Matrix: Solids
Sample ID: UST-1-113 Sampled: 6/9/2023 14:30
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
24.8 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 117 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98071 Matrix: Solids
Sample ID: UST-1-D Sampled: 6/9/2023 14:30
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Acetone
<0.026
mg/Kg - dry
0.026
1
06/12/23 19:12
TBL
V34278
Acrolein
<0.026
mg/Kg - dry
0.026
1
06/12/23 19:12
TBL
V34278
Acrylonitrile
<0.026
mg/Kg - dry
0.026
1
06/12/23 19:12
TBL
V34278
Benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Bromobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Bromochloromethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Bromodichloromethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Bromoform
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Bromomethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:12
TBL
V34278
n-Butylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
sec -Butyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
tert-Butyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Carbon Disulfide
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Carbon Tetrachloride
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Chlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Chlorodibromomethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Chloroethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:12
TBL
V34278
Chloroform
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Chloromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:12
TBL
V34278
2-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
4-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Di -Isopropyl Ether (DIPE)
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 118 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98071 Matrix: Solids
Sample ID: UST-1-D Sampled: 6/9/2023 14:30
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dibromo-3-Chloropropane
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:12
TBL
V34278
1,2-Dibromoethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Dibromomethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
1,2-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
1,3-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
1,4-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Dichlorodifluoromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:12
TBL
V34278
1,1-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
1,2-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
1,1-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
cis- 1,2-Dich loroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
trans-1,2-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
1,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
1,3-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
2,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
1,1-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
cis-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
trans-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Ethanol
<0.332
mg/Kg - dry
0.332
1
06/12/23 19:12
TBL
V34278
Ethylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Ethyl Tertiary Butyl Ether (ETBE) <0.066
mg/Kg - dry
0.066
1
06/12/23 19:12
TBL
V34278
Hexachlorobutadiene
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:12
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 119 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98071 Matrix: Solids
Sample ID: UST-1-D Sampled: 6/9/2023 14:30
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
n-Hexane
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:12
TBL
V34278
2-Hexanone
<0.026
mg/Kg - dry
0.026
1
06/12/23 19:12
TBL
V34278
Isopropyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
4-Isopropyl toluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Methyl Ethyl Ketone (MEK)
<0.026
mg/Kg - dry
0.026
1
06/12/23 19:12
TBL
V34278
Methyl tert-butyl ether (MTBE) <0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
4-Methyl-2-Pentanone
<0.026
mg/Kg - dry
0.026
1
06/12/23 19:12
TBL
V34278
Methylene Chloride
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:12
TBL
V34278
Naphthalene
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:12
TBL
V34278
n-Propylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Styrene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
1,1,1,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
1,1,2,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Tetrachloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Toluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
1,2,3-Trichlorobenzene
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:12
TBL
V34278
1,2,4-Trichlorobenzene
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:12
TBL
V34278
1,1,1-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
1,1,2-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Trichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Trichlorofluoromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:12
TBL
V34278
1,2,3-Trichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 120 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Report Date : 06/21/2023
Received : 06/09/2023
Lab No : 98071 Matrix: Solids
Sample ID: UST-1-D Sampled: 6/9/2023 14:30
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
1,3,5-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
Vinyl Acetate
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:12
TBL
V34278
Vinyl Chloride
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:12
TBL
V34278
o-Xylene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
TBL
V34278
m,p-Xylene
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:12
TBL
V34278
Xylene (Total)
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:12
V34278
Surrogate:4-Bromofluorobenzene
101
Limits:70-130%
1 06/12/23 19:12 TBL
V34278
Surrogate: Dibromofluoromethane
107
Limits: 84-123%
1 06/12/23 19:12 TBL
V34278
Surrogate: Toluene-d8
96.8
Limits: 76-129%
1 06/12/23 19:12 TBL
V34278
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Acenaphthylene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Aniline
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Anthracene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Benzo(a)anthracene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Benzo(a)pyrene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Benzo(b)fluoranthene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Benzo(g,h,i)perylene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 121 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98071
Matrix: Solids
Sample ID: UST-1-D
Sampled:
6/9/2023 14:30
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzo(k)fluoranthene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Benzoic Acid
<2.66
mg/Kg - dry
2.66
1
06/14/23 20:27
AMP
V34353
Benzyl alcohol
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Bis(2-Chloroethoxy)methane
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Bis(2-Chloroethyl)ether
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Bis(2-Chloroisopropyl)ether
<0.438
mg/Kg - dry
0.438
1
06/14/23 20:27
AMP
V34353
Bis(2-ethylhexyl)phthalate
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
4-13romophenyl phenyl ether
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Butyl benzyl phthalate
<0.438
mg/Kg - dry
0.438
1
06/14/23 20:27
AMP
V34353
4-Chloro-3-methylphenol
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
4-Chloroaniline
<0.438
mg/Kg - dry
0.438
1
06/14/23 20:27
AMP
V34353
2-Chloronaphthalene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
2-Chlorophenol
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
4-Chlorophenyl phenyl ether
<1.33
mg/Kg - dry
1.33
1
06/14/23 20:27
AMP
V34353
Chrysene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Dibenz(a,h)anthracene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Dibenzofuran
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
1,2-Dichlorobenzene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
1,3-Dichlorobenzene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
1,4-Dichlorobenzene
<0.438
mg/Kg - dry
0.438
1
06/14/23 20:27
AMP
V34353
3,3'-Dichlorobenzidine
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
2,4-Dichlorophenol
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 122 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98071
Matrix: Solids
Sample ID: UST-1-D
Sampled:
6/9/2023 14:30
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Dimethyl phthalate
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
2,4-Dimethyl phenol
<0.438
mg/Kg - dry
0.438
1
06/14/23 20:27
AMP
V34353
Di-n-butyl phthalate
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
4,6-Dinitro-2-methylphenol
<1.99
mg/Kg - dry
1.99
1
06/14/23 20:27
AMP
V34353
2,4-Dinitrophenol
<1.99
mg/Kg - dry
1.99
1
06/14/23 20:27
AMP
V34353
2,4-Dinitrotoluene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
2,6-Dinitrotoluene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Di-n-Octyl Phthalate
<0.438
mg/Kg - dry
0.438
1
06/14/23 20:27
AMP
V34353
Fluoranthene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Fluorene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Hexachlorobenzene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Hexachlorobutadiene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Hexachlorocyclopentadiene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Hexachloroethane
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Indeno(1,2,3-cd)pyrene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Isophorone
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
1-Methylnaphthalene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
2-Methylnaphthalene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
2-Methylphenol
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
3&4 Methylphenol
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Naphthalene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 123 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98071
Matrix: Solids
Sample ID: UST-1-D
Sampled: 6/9/2023
14:30
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
2-Nitroaniline
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27 AMP
V34353
3-Nitroaniline
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27 AMP
V34353
4-Nitroaniline
<0.438
mg/Kg - dry
0.438
1
06/14/23 20:27 AMP
V34353
Nitrobenzene
<0.438
mg/Kg - dry
0.438
1
06/14/23 20:27 AMP
V34353
2-Nitrophenol
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27 AMP
V34353
4-Nitrophenol
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27 AMP
V34353
N-Nitrosodimethylamine
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27 AMP
V34353
N-Nitrosodiphenylamine
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27 AMP
V34353
N-Nitroso-di-n-propylamine
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27 AMP
V34353
Pentachlorophenol
<1.33
mg/Kg - dry
1.33
1
06/14/23 20:27 AMP
V34353
Phenanthrene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27 AMP
V34353
Phenol
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27 AMP
V34353
Pyrene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27 AMP
V34353
Pyridine
<0.438
mg/Kg - dry
0.438
1
06/14/23 20:27 AMP
V34353
1,2,4-Trichlorobenzene
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27 AMP
V34353
2,4,5-Trichlorophenol
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27 AMP
V34353
2,4,6-Trichlorophenol
<0.877
mg/Kg - dry
0.877
1
06/14/23 20:27 AMP
V34353
Surrogate: Phenol-d5
58.3
Limits: 34-121%
1 06/14/23 20:27 AMP
8270E
Surrogate: 2-Fluorobiphenyl
75.3
Limits: 44-115%
1 06/14/23 20:27 AMP
V34353
Surrogate: 2-Fluorophenol
63.1
Limits: 35-115%
1 06/14/23 20:27 AMP
V34353
Surrogate: Nitrobenzene-d5
71.7
Limits: 37-122%
1 06/14/23 20:27 AMP
V34353
Surrogate: 4-Terphenyl-d14
77.1
Limits: 54-127%
1 06/14/23 20:27 AMP
V34353
Surrogate: 2,4,6-Tribromophenol
55.0
Limits: 39-132%
1 06/14/23 20:27 AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 124 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98071 Matrix: Solids
Sample ID: UST-1-D Sampled: 6/9/2023 14:30
Analytical Method: MADEP-EPH
Prep Method: MAEPH (Prep)
Test
Aliphatic C9-C18
Aliphatic C19-C36
Aromatic C11-C22
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Analytical Method: MADEP-VPH
Prep Method: MAVPH (Prep)
Test
Prep Batch(es): V34271 06/13/23 10:20
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
<66.6 mg/Kg - dry
66.6 1
06/17/23 00:52 AMP
V34449
<66.6 mg/Kg - dry
66.6 1
06/17/23 00:52 AMP
V34449
<66.6 mg/Kg - dry
66.6 1
06/17/23 00:52 AMP
V34449
112
Limits: 40-140%
1 06/17/23 00:52 AMP
MADEP-EPH
69.3
Limits: 40-140%
1 06/17/23 00:52 AMP
MADEP-EPH
106
Limits: 40-140%
1 06/17/23 00:52 AMP
MADEP-EPH
112
Limits: 40-140%
1 06/17/23 00:52 AMP
V34449
Prep Batch(es):
V34232 06/12/23 08:00
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Aliphatic C5-C8 <10.6
Aliphatic C9-C12 <10.6
Aromatic C9-C10 <10.6
Surrogate: 2,5-Dibromotoluene (FID)
Surrogate: 2,5-Dibromotoluene (PID)
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
mg/Kg - dry
10.6
100 06/12/23 18:22 TBL
V34233
mg/Kg - dry
10.6
100 06/12/23 18:22 TBL
V34233
mg/Kg - dry
10.6
100 06/12/23 18:22 TBL
V34233
106
Limits: 70-130%
100 06/12/23 18:22 TBL
MADEP-VPH
101
Limits: 70-130%
100 06/12/23 18:22 TBL
MADEP-VPH
DF Dilution Factor
Page 125 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98072 Matrix: Solids
Sample ID: UST-1-E Sampled: 6/9/2023 15:00
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
25.2 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 126 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98072 Matrix: Solids
Sample ID: UST-1-E Sampled: 6/9/2023 15:00
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Acetone
<0.026
mg/Kg - dry
0.026
1
06/12/23 19:39
TBL
V34278
Acrolein
<0.026
mg/Kg - dry
0.026
1
06/12/23 19:39
TBL
V34278
Acrylonitrile
<0.026
mg/Kg - dry
0.026
1
06/12/23 19:39
TBL
V34278
Benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Bromobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Bromochloromethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Bromodichloromethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Bromoform
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Bromomethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:39
TBL
V34278
n-Butylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
sec -Butyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
tert-Butyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Carbon Disulfide
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Carbon Tetrachloride
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Chlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Chlorodibromomethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Chloroethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:39
TBL
V34278
Chloroform
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Chloromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:39
TBL
V34278
2-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
4-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Di -Isopropyl Ether (DIPE)
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 127 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98072 Matrix: Solids
Sample ID: UST-1-E Sampled: 6/9/2023 15:00
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dibromo-3-Chloropropane
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:39
TBL
V34278
1,2-Dibromoethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Dibromomethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
1,2-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
1,3-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
1,4-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Dichlorodifluoromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:39
TBL
V34278
1,1-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
1,2-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
1,1-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
cis- 1,2-Dich loroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
trans-1,2-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
1,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
1,3-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
2,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
1,1-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
cis-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
trans-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Ethanol
<0.334
mg/Kg - dry
0.334
1
06/12/23 19:39
TBL
V34278
Ethylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Ethyl Tertiary Butyl Ether (ETBE) <0.066
mg/Kg - dry
0.066
1
06/12/23 19:39
TBL
V34278
Hexachlorobutadiene
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:39
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 128 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98072 Matrix: Solids
Sample ID: UST-1-E Sampled: 6/9/2023 15:00
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
n-Hexane
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:39
TBL
V34278
2-Hexanone
<0.026
mg/Kg - dry
0.026
1
06/12/23 19:39
TBL
V34278
Isopropyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
4-Isopropyl toluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Methyl Ethyl Ketone (MEK)
<0.026
mg/Kg - dry
0.026
1
06/12/23 19:39
TBL
V34278
Methyl tert-butyl ether (MTBE) <0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
4-Methyl-2-Pentanone
<0.026
mg/Kg - dry
0.026
1
06/12/23 19:39
TBL
V34278
Methylene Chloride
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:39
TBL
V34278
Naphthalene
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:39
TBL
V34278
n-Propylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Styrene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
1,1,1,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
1,1,2,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Tetrachloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Toluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
1,2,3-Trichlorobenzene
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:39
TBL
V34278
1,2,4-Trichlorobenzene
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:39
TBL
V34278
1,1,1-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
1,1,2-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Trichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Trichlorofluoromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:39
TBL
V34278
1,2,3-Trichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 129 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Report Date : 06/21/2023
Received : 06/09/2023
Lab No : 98072 Matrix: Solids
Sample ID: UST-1-E Sampled: 6/9/2023 15:00
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
1,3,5-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
Vinyl Acetate
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:39
TBL
V34278
Vinyl Chloride
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:39
TBL
V34278
o-Xylene
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
TBL
V34278
m,p-Xylene
<0.013
mg/Kg - dry
0.013
1
06/12/23 19:39
TBL
V34278
Xylene (Total)
<0.006
mg/Kg - dry
0.006
1
06/12/23 19:39
V34278
Surrogate:4-Bromofluorobenzene
102
Limits:70-130%
1 06/12/23 19:39 TBL
V34278
Surrogate: Dibromofluoromethane
105
Limits: 84-123%
1 06/12/23 19:39 TBL
V34278
Surrogate: Toluene-d8
96.2
Limits: 76-129%
1 06/12/23 19:39 TBL
V34278
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Acenaphthylene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Aniline
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Anthracene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Benzo(a)anthracene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Benzo(a)pyrene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Benzo(b)fluoranthene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Benzo(g,h,i)perylene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 130 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98072
Matrix: Solids
Sample ID: UST-1-E
Sampled:
6/9/2023 15:00
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzo(k)fluoranthene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Benzoic Acid
<2.67
mg/Kg - dry
2.67
1
06/14/23 20:50
AMP
V34353
Benzyl alcohol
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Bis(2-Chloroethoxy)methane
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Bis(2-Chloroethyl)ether
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Bis(2-Chloroisopropyl)ether
<0.441
mg/Kg - dry
0.441
1
06/14/23 20:50
AMP
V34353
Bis(2-ethylhexyl)phthalate
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
4-13romophenyl phenyl ether
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Butyl benzyl phthalate
<0.441
mg/Kg - dry
0.441
1
06/14/23 20:50
AMP
V34353
4-Chloro-3-methylphenol
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
4-Chloroaniline
<0.441
mg/Kg - dry
0.441
1
06/14/23 20:50
AMP
V34353
2-Chloronaphthalene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
2-Chlorophenol
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
4-Chlorophenyl phenyl ether
<1.34
mg/Kg - dry
1.34
1
06/14/23 20:50
AMP
V34353
Chrysene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Dibenz(a,h)anthracene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Dibenzofuran
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
1,2-Dichlorobenzene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
1,3-Dichlorobenzene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
1,4-Dichlorobenzene
<0.441
mg/Kg - dry
0.441
1
06/14/23 20:50
AMP
V34353
3,3'-Dichlorobenzidine
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
2,4-Dichlorophenol
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 131 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98072
Matrix: Solids
Sample ID: UST-1-E
Sampled:
6/9/2023 15:00
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Dimethyl phthalate
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
2,4-Dimethyl phenol
<0.441
mg/Kg - dry
0.441
1
06/14/23 20:50
AMP
V34353
Di-n-butyl phthalate
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
4,6-Dinitro-2-methylphenol
<2.01
mg/Kg - dry
2.01
1
06/14/23 20:50
AMP
V34353
2,4-Dinitrophenol
<2.01
mg/Kg - dry
2.01
1
06/14/23 20:50
AMP
V34353
2,4-Dinitrotoluene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
2,6-Dinitrotoluene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Di-n-Octyl Phthalate
<0.441
mg/Kg - dry
0.441
1
06/14/23 20:50
AMP
V34353
Fluoranthene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Fluorene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Hexachlorobenzene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Hexachlorobutadiene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Hexachlorocyclopentadiene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Hexachloroethane
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Indeno(1,2,3-cd)pyrene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Isophorone
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
1-Methylnaphthalene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
2-Methylnaphthalene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
2-Methylphenol
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
3&4 Methylphenol
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Naphthalene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 132 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98072
Matrix: Solids
Sample ID: UST-1-E
Sampled: 6/9/2023
15:00
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
2-Nitroaniline
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50 AMP
V34353
3-Nitroaniline
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50 AMP
V34353
4-Nitroaniline
<0.441
mg/Kg - dry
0.441
1
06/14/23 20:50 AMP
V34353
Nitrobenzene
<0.441
mg/Kg - dry
0.441
1
06/14/23 20:50 AMP
V34353
2-Nitrophenol
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50 AMP
V34353
4-Nitrophenol
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50 AMP
V34353
N-Nitrosodimethylamine
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50 AMP
V34353
N-Nitrosodiphenylamine
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50 AMP
V34353
N-Nitroso-di-n-propylamine
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50 AMP
V34353
Pentachlorophenol
<1.34
mg/Kg - dry
1.34
1
06/14/23 20:50 AMP
V34353
Phenanthrene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50 AMP
V34353
Phenol
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50 AMP
V34353
Pyrene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50 AMP
V34353
Pyridine
<0.441
mg/Kg - dry
0.441
1
06/14/23 20:50 AMP
V34353
1,2,4-Trichlorobenzene
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50 AMP
V34353
2,4,5-Trichlorophenol
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50 AMP
V34353
2,4,6-Trichlorophenol
<0.882
mg/Kg - dry
0.882
1
06/14/23 20:50 AMP
V34353
Surrogate: Phenol-d5
57.4
Limits: 34-121%
1 06/14/23 20:50 AMP
8270E
Surrogate: 2-Fluorobiphenyl
74.3
Limits: 44-115%
1 06/14/23 20:50 AMP
V34353
Surrogate: 2-Fluorophenol
61.6
Limits: 35-115%
1 06/14/23 20:50 AMP
V34353
Surrogate: Nitrobenzene-d5
68.9
Limits: 37-122%
1 06/14/23 20:50 AMP
V34353
Surrogate: 4-Terphenyl-d14
76.0
Limits: 54-127%
1 06/14/23 20:50 AMP
V34353
Surrogate: 2,4,6-Tribromophenol
57.1
Limits: 39-132%
1 06/14/23 20:50 AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 133 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98072 Matrix: Solids
Sample ID: UST-1-E Sampled: 6/9/2023 15:00
Analytical Method: MADEP-EPH
Prep Method: MAEPH (Prep)
Test
Aliphatic C9-C18
Aliphatic C19-C36
Aromatic C11-C22
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Analytical Method: MADEP-VPH
Prep Method: MAVPH (Prep)
Test
Prep Batch(es): V34271 06/13/23 10:20
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
<66.6 mg/Kg - dry
66.6 1
06/17/23 01:29 AMP
V34449
<66.6 mg/Kg - dry
66.6 1
06/17/23 01:29 AMP
V34449
<66.6 mg/Kg - dry
66.6 1
06/17/23 01:29 AMP
V34449
108
Limits: 40-140%
1 06/17/23 01:29 AMP
MADEP-EPH
71.8
Limits: 40-140%
1 06/17/23 01:29 AMP
MADEP-EPH
96.2
Limits: 40-140%
1 06/17/23 01:29 AMP
MADEP-EPH
105
Limits: 40-140%
1 06/17/23 01:29 AMP
V34449
Prep Batch(es):
V34232 06/12/23 08:00
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Aliphatic C5-C8 <10.7
Aliphatic C9-C12 <10.7
Aromatic C9-C10 <10.7
Surrogate: 2,5-Dibromotoluene (FID)
Surrogate: 2,5-Dibromotoluene (PID)
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
mg/Kg - dry
10.7
100 06/12/23 18:45 TBL
V34233
mg/Kg - dry
10.7
100 06/12/23 18:45 TBL
V34233
mg/Kg - dry
10.7
100 06/12/23 18:45 TBL
V34233
100
Limits: 70-130%
100 06/12/23 18:45 TBL
MADEP-VPH
102
Limits: 70-130%
100 06/12/23 18:45 TBL
MADEP-VPH
DF Dilution Factor
Page 134 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98073 Matrix: Solids
Sample ID: UST-14 Sampled: 6/9/2023 13:55
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
22.8 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 135 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98073 Matrix: Solids
Sample ID: UST-1-F Sampled: 6/9/2023 13:55
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Acetone
<0.025
mg/Kg - dry
0.025
1
06/12/23 20:06
TBL
V34278
Acrolein
<0.025
mg/Kg - dry
0.025
1
06/12/23 20:06
TBL
V34278
Acrylonitrile
<0.025
mg/Kg - dry
0.025
1
06/12/23 20:06
TBL
V34278
Benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Bromobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Bromochloromethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Bromodichloromethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Bromoform
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Bromomethane
<0.012
mg/Kg - dry
0.012
1
06/12/23 20:06
TBL
V34278
n-Butylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
sec -Butyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
tert-Butyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Carbon Disulfide
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Carbon Tetrachloride
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Chlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Chlorodibromomethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Chloroethane
<0.012
mg/Kg - dry
0.012
1
06/12/23 20:06
TBL
V34278
Chloroform
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Chloromethane
<0.012
mg/Kg - dry
0.012
1
06/12/23 20:06
TBL
V34278
2-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
4-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Di -Isopropyl Ether (DIPE)
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 136 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98073 Matrix: Solids
Sample ID: UST-1-F Sampled: 6/9/2023 13:55
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dibromo-3-Chloropropane
<0.012
mg/Kg - dry
0.012
1
06/12/23 20:06
TBL
V34278
1,2-Dibromoethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Dibromomethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
1,2-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
1,3-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
1,4-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Dichlorodifluoromethane
<0.012
mg/Kg - dry
0.012
1
06/12/23 20:06
TBL
V34278
1,1-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
1,2-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
1,1-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
cis- 1,2-Dich loroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
trans-1,2-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
1,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
1,3-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
2,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
1,1-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
cis-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
trans-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Ethanol
<0.323
mg/Kg - dry
0.323
1
06/12/23 20:06
TBL
V34278
Ethylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Ethyl Tertiary Butyl Ether (ETBE) <0.064
mg/Kg - dry
0.064
1
06/12/23 20:06
TBL
V34278
Hexachlorobutadiene
<0.012
mg/Kg - dry
0.012
1
06/12/23 20:06
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 137 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98073 Matrix: Solids
Sample ID: UST-1-F Sampled: 6/9/2023 13:55
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
n-Hexane
<0.012
mg/Kg - dry
0.012
1
06/12/23 20:06
TBL
V34278
2-Hexanone
<0.025
mg/Kg - dry
0.025
1
06/12/23 20:06
TBL
V34278
Isopropyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
4-Isopropyl toluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Methyl Ethyl Ketone (MEK)
<0.025
mg/Kg - dry
0.025
1
06/12/23 20:06
TBL
V34278
Methyl tert-butyl ether (MTBE) <0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
4-Methyl-2-Pentanone
<0.025
mg/Kg - dry
0.025
1
06/12/23 20:06
TBL
V34278
Methylene Chloride
<0.012
mg/Kg - dry
0.012
1
06/12/23 20:06
TBL
V34278
Naphthalene
<0.012
mg/Kg - dry
0.012
1
06/12/23 20:06
TBL
V34278
n-Propylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Styrene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
1,1,1,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
1,1,2,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Tetrachloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Toluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
1,2,3-Trichlorobenzene
<0.012
mg/Kg - dry
0.012
1
06/12/23 20:06
TBL
V34278
1,2,4-Trichlorobenzene
<0.012
mg/Kg - dry
0.012
1
06/12/23 20:06
TBL
V34278
1,1,1-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
1,1,2-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Trichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Trichlorofluoromethane
<0.012
mg/Kg - dry
0.012
1
06/12/23 20:06
TBL
V34278
1,2,3-Trichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 138 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Report Date : 06/21/2023
Received : 06/09/2023
Lab No : 98073 Matrix: Solids
Sample ID: UST-1-F Sampled: 6/9/2023 13:55
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
1,3,5-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
Vinyl Acetate
<0.012
mg/Kg - dry
0.012
1
06/12/23 20:06
TBL
V34278
Vinyl Chloride
<0.012
mg/Kg - dry
0.012
1
06/12/23 20:06
TBL
V34278
o-Xylene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
TBL
V34278
m,p-Xylene
<0.012
mg/Kg - dry
0.012
1
06/12/23 20:06
TBL
V34278
Xylene (Total)
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:06
V34278
Surrogate: 4-Bromofluorobenzene
101
Limits: 70-130%
1 06/12/23 20:06 TBL
V34278
Surrogate: Dibromofluoromethane
106
Limits: 84-123%
1 06/12/23 20:06 TBL
V34278
Surrogate: Toluene-d8
97.2
Limits: 76-129%
1 06/12/23 20:06 TBL
V34278
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Acenaphthylene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Aniline
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Anthracene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Benzo(a)anthracene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Benzo(a)pyrene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Benzo(b)fluoranthene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Benzo(g,h,i)perylene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 139 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98073
Matrix: Solids
Sample ID: UST-1-F
Sampled:
6/9/2023 13:55
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzo(k)fluoranthene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Benzoic Acid
<2.59
mg/Kg - dry
2.59
1
06/14/23 21:12
AMP
V34353
Benzyl alcohol
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Bis(2-Chloroethoxy)methane
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Bis(2-Chloroethyl)ether
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Bis(2-Chloroisopropyl)ether
<0.427
mg/Kg - dry
0.427
1
06/14/23 21:12
AMP
V34353
Bis(2-ethylhexyl)phthalate
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
4-13romophenyl phenyl ether
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Butyl benzyl phthalate
<0.427
mg/Kg - dry
0.427
1
06/14/23 21:12
AMP
V34353
4-Chloro-3-methylphenol
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
4-Chloroaniline
<0.427
mg/Kg - dry
0.427
1
06/14/23 21:12
AMP
V34353
2-Chloronaphthalene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
2-Chlorophenol
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
4-Chlorophenyl phenyl ether
<1.30
mg/Kg - dry
1.30
1
06/14/23 21:12
AMP
V34353
Chrysene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Dibenz(a,h)anthracene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Dibenzofuran
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
1,2-Dichlorobenzene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
1,3-Dichlorobenzene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
1,4-Dichlorobenzene
<0.427
mg/Kg - dry
0.427
1
06/14/23 21:12
AMP
V34353
3,3'-Dichlorobenzidine
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
2,4-Dichlorophenol
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 140 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98073
Matrix: Solids
Sample ID: UST-1-F
Sampled:
6/9/2023 13:55
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Dimethyl phthalate
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
2,4-Dimethyl phenol
<0.427
mg/Kg - dry
0.427
1
06/14/23 21:12
AMP
V34353
Di-n-butyl phthalate
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
4,6-Dinitro-2-methylphenol
<1.94
mg/Kg - dry
1.94
1
06/14/23 21:12
AMP
V34353
2,4-Dinitrophenol
<1.94
mg/Kg - dry
1.94
1
06/14/23 21:12
AMP
V34353
2,4-Dinitrotoluene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
2,6-Dinitrotoluene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Di-n-Octyl Phthalate
<0.427
mg/Kg - dry
0.427
1
06/14/23 21:12
AMP
V34353
Fluoranthene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Fluorene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Hexachlorobenzene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Hexachlorobutadiene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Hexachlorocyclopentadiene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Hexachloroethane
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Indeno(1,2,3-cd)pyrene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Isophorone
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
1-Methylnaphthalene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
2-Methylnaphthalene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
2-Methylphenol
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
3&4 Methylphenol
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Naphthalene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 141 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98073
Matrix: Solids
Sample ID: UST-1-F
Sampled: 6/9/2023
13:55
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
2-Nitroaniline
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12 AMP
V34353
3-Nitroaniline
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12 AMP
V34353
4-Nitroaniline
<0.427
mg/Kg - dry
0.427
1
06/14/23 21:12 AMP
V34353
Nitrobenzene
<0.427
mg/Kg - dry
0.427
1
06/14/23 21:12 AMP
V34353
2-Nitrophenol
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12 AMP
V34353
4-Nitrophenol
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12 AMP
V34353
N-Nitrosodimethylamine
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12 AMP
V34353
N-Nitrosodiphenylamine
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12 AMP
V34353
N-Nitroso-di-n-propylamine
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12 AMP
V34353
Pentachlorophenol
<1.30
mg/Kg - dry
1.30
1
06/14/23 21:12 AMP
V34353
Phenanthrene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12 AMP
V34353
Phenol
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12 AMP
V34353
Pyrene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12 AMP
V34353
Pyridine
<0.427
mg/Kg - dry
0.427
1
06/14/23 21:12 AMP
V34353
1,2,4-Trichlorobenzene
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12 AMP
V34353
2,4,5-Trichlorophenol
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12 AMP
V34353
2,4,6-Trichlorophenol
<0.854
mg/Kg - dry
0.854
1
06/14/23 21:12 AMP
V34353
Surrogate: Phenol-d5
54.7
Limits: 34-121%
1 06/14/23 21:12 AMP
8270E
Surrogate: 2-Fluorobiphenyl
69.9
Limits: 44-115%
1 06/14/23 21:12 AMP
V34353
Surrogate: 2-Fluorophenol
61.6
Limits: 35-115%
1 06/14/23 21:12 AMP
V34353
Surrogate: Nitrobenzene-d5
65.1
Limits: 37-122%
1 06/14/23 21:12 AMP
V34353
Surrogate: 4-Terphenyl-d14
78.9
Limits: 54-127%
1 06/14/23 21:12 AMP
V34353
Surrogate: 2,4,6-Tribromophenol
57.7
Limits: 39-132%
1 06/14/23 21:12 AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 142 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98073 Matrix: Solids
Sample ID: UST-14 Sampled: 6/9/2023 13:55
Analytical Method: MADEP-EPH
Prep Method: MAEPH (Prep)
Test
Aliphatic C9-C18
Aliphatic C19-C36
Aromatic C11-C22
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Analytical Method: MADEP-VPH
Prep Method: MAVPH (Prep)
Test
Prep Batch(es): V34271 06/13/23 10:20
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
<64.6 mg/Kg - dry
64.6 1
06/17/23 02:05 AMP
V34449
<64.6 mg/Kg - dry
64.6 1
06/17/23 02:05 AMP
V34449
<64.6 mg/Kg - dry
64.6 1
06/17/23 02:05 AMP
V34449
122
Limits: 40-140%
1 06/17/23 02:05 AMP
MADEP-EPH
72.2
Limits: 40-140%
1 06/17/23 02:05 AMP
MADEP-EPH
112
Limits: 40-140%
1 06/17/23 02:05 AMP
MADEP-EPH
120
Limits: 40-140%
1 06/17/23 02:05 AMP
V34449
Prep Batch(es):
V34232 06/12/23 08:00
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Aliphatic C5-C8 <10.4
Aliphatic C9-C12 <10.4
Aromatic C9-C10 <10.4
Surrogate: 2,5-Dibromotoluene (FID)
Surrogate: 2,5-Dibromotoluene (PID)
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
mg/Kg - dry
10.4
100 06/12/23 19:32 TBL
V34233
mg/Kg - dry
10.4
100 06/12/23 19:32 TBL
V34233
mg/Kg - dry
10.4
100 06/12/23 19:32 TBL
V34233
89.2
Limits: 70-130%
100 06/12/23 19:32 TBL
MADEP-VPH
92.9
Limits: 70-130%
100 06/12/23 19:32 TBL
MADEP-VPH
DF Dilution Factor
Page 143 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98074 Matrix: Solids
Sample ID: UST-1-G Sampled: 6/9/2023 11:40
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
31.1 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 144 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98074 Matrix: Solids
Sample ID: UST-1-G Sampled: 6/9/2023 11:40
Analytical Method: 8260D Prep Batch(es): V34299 06/13/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Acetone
<0.029
mg/Kg - dry
0.029
1
06/13/23 14:17
TBL
V34300
Acrolein
<0.029
mg/Kg - dry
0.029
1
06/13/23 14:17
TBL
V34300
Acrylonitrile
<0.029
mg/Kg - dry
0.029
1
06/13/23 14:17
TBL
V34300
Benzene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Bromobenzene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Bromochloromethane
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Bromodichloromethane
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Bromoform
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Bromomethane
<0.014
mg/Kg - dry
0.014
1
06/13/23 14:17
TBL
V34300
n-Butylbenzene
0.016
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
sec -Butyl benzene
0.025
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
tert-Butyl benzene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Carbon Disulfide
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Carbon Tetrachloride
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Chlorobenzene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Chlorodibromomethane
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Chloroethane
<0.014
mg/Kg - dry
0.014
1
06/13/23 14:17
TBL
V34300
Chloroform
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Chloromethane
<0.014
mg/Kg - dry
0.014
1
06/13/23 14:17
TBL
V34300
2-Chlorotoluene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
4-Chlorotoluene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Di -Isopropyl Ether (DIPE)
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 145 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98074
Matrix: Solids
Sample ID: UST-1-G
Sampled:
6/9/2023 11:40
Analytical Method: 8260D
Prep Batch(es):
V34299
06/13/23 08:00
Prep Method: 5035
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,2-Dibromo-3-Chloropropane
<0.014
mg/Kg - dry
0.014
1
06/13/23 14:17
TBL
V34300
1,2-Dibromoethane
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Dibromomethane
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
1,2-Dichlorobenzene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
1,3-Dichlorobenzene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
1,4-Dichlorobenzene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Dichlorodifluoromethane
<0.014
mg/Kg - dry
0.014
1
06/13/23 14:17
TBL
V34300
1,1-Dichloroethane
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
1,2-Dichloroethane
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
1,1-Dichloroethene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
cis- 1,2-Dich loroethene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
trans-1,2-Dichloroethene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
1,2-Dichloropropane
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
1,3-Dichloropropane
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
2,2-Dichloropropane
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
1,1-Dichloropropene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
cis-1,3-Dichloropropene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
trans-1,3-Dichloropropene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Ethanol
<0.362
mg/Kg - dry
0.362
1
06/13/23 14:17
TBL
V34300
Ethylbenzene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Ethyl Tertiary Butyl Ether (ETBE)
<0.072
mg/Kg - dry
0.072
1
06/13/23 14:17
TBL
V34300
Hexachlorobutadiene
<0.014
mg/Kg - dry
0.014
1
06/13/23 14:17
TBL
V34300
Qualifiers/ * Outside QC Limit
DF Dilution Factor
Definitions MQL Method Quantitation Limit
Page 146 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98074 Matrix: Solids
Sample ID: UST-1-G Sampled: 6/9/2023 11:40
Analytical Method: 8260D Prep Batch(es): V34299 06/13/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
n-Hexane
<0.014
mg/Kg - dry
0.014
1
06/13/23 14:17
TBL
V34300
2-Hexanone
<0.029
mg/Kg - dry
0.029
1
06/13/23 14:17
TBL
V34300
Isopropyl benzene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
4-Isopropyl toluene
0.045
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Methyl Ethyl Ketone (MEK)
<0.029
mg/Kg - dry
0.029
1
06/13/23 14:17
TBL
V34300
Methyl tert-butyl ether (MTBE) <0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
4-Methyl-2-Pentanone
<0.029
mg/Kg - dry
0.029
1
06/13/23 14:17
TBL
V34300
Methylene Chloride
<0.014
mg/Kg - dry
0.014
1
06/13/23 14:17
TBL
V34300
Naphthalene
<0.014
mg/Kg - dry
0.014
1
06/13/23 14:17
TBL
V34300
n-Propylbenzene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Styrene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
1,1,1,2-Tetrachloroethane
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
1,1,2,2-Tetrachloroethane
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Tetrachloroethene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Toluene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
1,2,3-Trichlorobenzene
<0.014
mg/Kg - dry
0.014
1
06/13/23 14:17
TBL
V34300
1,2,4-Trichlorobenzene
<0.014
mg/Kg - dry
0.014
1
06/13/23 14:17
TBL
V34300
1,1,1-Trichloroethane
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
1,1,2-Trichloroethane
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Trichloroethene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Trichlorofluoromethane
<0.014
mg/Kg - dry
0.014
1
06/13/23 14:17
TBL
V34300
1,2,3-Trichloropropane
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 147 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Report Date : 06/21/2023
Received : 06/09/2023
Lab No : 98074 Matrix: Solids
Sample ID: UST-1-G Sampled: 6/9/2023 11:40
Analytical Method: 8260D Prep Batch(es): V34299 06/13/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
0.008
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
1,3,5-Trimethyl benzene
0.056
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
Vinyl Acetate
<0.014
mg/Kg - dry
0.014
1
06/13/23 14:17
TBL
V34300
Vinyl Chloride
<0.014
mg/Kg - dry
0.014
1
06/13/23 14:17
TBL
V34300
o-Xylene
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
TBL
V34300
m,p-Xylene
<0.014
mg/Kg - dry
0.014
1
06/13/23 14:17
TBL
V34300
Xylene (Total)
<0.007
mg/Kg - dry
0.007
1
06/13/23 14:17
V34300
Surrogate:4-Bromofluorobenzene
102
Limits:70-130%
1 06/13/23 14:17 TBL
V34300
Surrogate: Dibromofluoromethane
104
Limits: 84-123%
1 06/13/23 14:17
TBL
V34300
Surrogate: Toluene-d8
97.0
Limits: 76-129%
1 06/13/23 14:17
TBL
V34300
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Acenaphthylene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Aniline
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Anthracene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Benzo(a)anthracene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Benzo(a)pyrene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Benzo(b)fluoranthene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Benzo(g,h,i)perylene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 148 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98074
Matrix: Solids
Sample ID: UST-1-G
Sampled:
6/9/2023 11:40
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzo(k)fluoranthene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Benzoic Acid
<2.90
mg/Kg - dry
2.90
1
06/14/23 23:27
AMP
V34353
Benzyl alcohol
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Bis(2-Chloroethoxy)methane
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Bis(2-Chloroethyl)ether
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Bis(2-Chloroisopropyl)ether
<0.478
mg/Kg - dry
0.478
1
06/14/23 23:27
AMP
V34353
Bis(2-ethylhexyl)phthalate
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
4-13romophenyl phenyl ether
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Butyl benzyl phthalate
<0.478
mg/Kg - dry
0.478
1
06/14/23 23:27
AMP
V34353
4-Chloro-3-methylphenol
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
4-Chloroaniline
<0.478
mg/Kg - dry
0.478
1
06/14/23 23:27
AMP
V34353
2-Chloronaphthalene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
2-Chlorophenol
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
4-Chlorophenyl phenyl ether
<1.45
mg/Kg - dry
1.45
1
06/14/23 23:27
AMP
V34353
Chrysene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Dibenz(a,h)anthracene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Dibenzofuran
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
1,2-Dichlorobenzene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
1,3-Dichlorobenzene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
1,4-Dichlorobenzene
<0.478
mg/Kg - dry
0.478
1
06/14/23 23:27
AMP
V34353
3,3'-Dichlorobenzidine
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
2,4-Dichlorophenol
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 149 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98074
Matrix: Solids
Sample ID: UST-1-G
Sampled:
6/9/2023 11:40
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Dimethyl phthalate
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
2,4-Dimethyl phenol
<0.478
mg/Kg - dry
0.478
1
06/14/23 23:27
AMP
V34353
Di-n-butyl phthalate
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
4,6-Dinitro-2-methylphenol
<2.18
mg/Kg - dry
2.18
1
06/14/23 23:27
AMP
V34353
2,4-Dinitrophenol
<2.18
mg/Kg - dry
2.18
1
06/14/23 23:27
AMP
V34353
2,4-Dinitrotoluene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
2,6-Dinitrotoluene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Di-n-Octyl Phthalate
<0.478
mg/Kg - dry
0.478
1
06/14/23 23:27
AMP
V34353
Fluoranthene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Fluorene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Hexachlorobenzene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Hexachlorobutadiene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Hexachlorocyclopentadiene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Hexachloroethane
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Indeno(1,2,3-cd)pyrene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Isophorone
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
1-Methylnaphthalene
2.98
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
2-Methylnaphthalene
1.11
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
2-Methylphenol
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
3&4 Methylphenol
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Naphthalene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 150 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98074
Matrix: Solids
Sample ID: UST-1-G
Sampled: 6/9/2023
11:40
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
2-Nitroaniline
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27 AMP
V34353
3-Nitroaniline
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27 AMP
V34353
4-Nitroaniline
<0.478
mg/Kg - dry
0.478
1
06/14/23 23:27 AMP
V34353
Nitrobenzene
<0.478
mg/Kg - dry
0.478
1
06/14/23 23:27 AMP
V34353
2-Nitrophenol
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27 AMP
V34353
4-Nitrophenol
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27 AMP
V34353
N-Nitrosodimethylamine
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27 AMP
V34353
N-Nitrosodiphenylamine
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27 AMP
V34353
N-Nitroso-di-n-propylamine
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27 AMP
V34353
Pentachlorophenol
<1.45
mg/Kg - dry
1.45
1
06/14/23 23:27 AMP
V34353
Phenanthrene
2.67
mg/Kg - dry
0.959
1
06/14/23 23:27 AMP
V34353
Phenol
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27 AMP
V34353
Pyrene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27 AMP
V34353
Pyridine
<0.478
mg/Kg - dry
0.478
1
06/14/23 23:27 AMP
V34353
1,2,4-Trichlorobenzene
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27 AMP
V34353
2,4,5-Trichlorophenol
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27 AMP
V34353
2,4,6-Trichlorophenol
<0.959
mg/Kg - dry
0.959
1
06/14/23 23:27 AMP
V34353
Surrogate: Phenol-d5
54.2
Limits: 34-121%
1 06/14/23 23:27 AMP
8270E
Surrogate: 2-Fluorobiphenyl
70.1
Limits: 44-115%
1 06/14/23 23:27 AMP
V34353
Surrogate: 2-Fluorophenol
59.3
Limits: 35-115%
1 06/14/23 23:27 AMP
V34353
Surrogate: Nitrobenzene-d5
65.9
Limits: 37-122%
1 06/14/23 23:27 AMP
V34353
Surrogate: 4-Terphenyl-d14
76.0
Limits: 54-127%
1 06/14/23 23:27 AMP
V34353
Surrogate: 2,4,6-Tribromophenol
60.8
Limits: 39-132%
1 06/14/23 23:27 AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 151 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98074 Matrix: Solids
Sample ID: UST-1-G Sampled: 6/9/2023 11:40
Analytical Method: MADEP-EPH
Prep Method: MAEPH (Prep)
Test
Aliphatic C9-C18
Aliphatic C19-C36
Aromatic C11-C22
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Analytical Method: MADEP-VPH
Prep Method: MAVPH (Prep)
Test
Prep Batch(es): V34271 06/13/23 10:20
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1060 mg/Kg - dry
289
4 06/20/23 17:08 AMP
V34449
<289 mg/Kg - dry
289
4 06/20/23 17:08 AMP
V34449
1290 mg/Kg - dry
289
4 06/20/23 17:08 AMP
V34449
155 *
Limits:40-140%
4 06/20/23 17:08 AMP
MADEP-EPH
37.5 *
Limits:40-140%
4 06/20/23 17:08 AMP
MADEP-EPH
96.1
Limits:40-140%
4 06/20/23 17:08 AMP
MADEP-EPH
82.5
Limits:40-140%
4 06/20/23 17:08 AMP
V34449
Prep Batch(es):
V34232 06/12/23 08:00
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Aliphatic C5-C8 <11.6
Aliphatic C9-C12 86.2
Aromatic C9-C10 12.3
Surrogate: 2,5-Dibromotoluene (FID)
Surrogate: 2,5-Dibromotoluene (PID)
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
mg/Kg - dry
11.6
100 06/12/23 22:17 TBL
V34233
mg/Kg - dry
11.6
100 06/12/23 22:17 TBL
V34233
mg/Kg - dry
11.6
100 06/12/23 22:17 TBL
V34233
76.0
Limits: 70-130%
100 06/12/23 22:17 TBL
MADEP-VPH
77.1
Limits: 70-130%
100 06/12/23 22:17 TBL
MADEP-VPH
DF Dilution Factor
Page 152 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98075 Matrix: Solids
Sample ID: UST-1-111 Sampled: 6/9/2023 14:20
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
24.9 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 153 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98075 Matrix: Solids
Sample ID: UST-1-111 Sampled: 6/9/2023 14:20
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Acetone
<0.026
mg/Kg - dry
0.026
1
06/12/23 20:34
TBL
V34278
Acrolein
<0.026
mg/Kg - dry
0.026
1
06/12/23 20:34
TBL
V34278
Acrylonitrile
<0.026
mg/Kg - dry
0.026
1
06/12/23 20:34
TBL
V34278
Benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Bromobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Bromochloromethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Bromodichloromethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Bromoform
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Bromomethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 20:34
TBL
V34278
n-Butylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
sec -Butyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
tert-Butyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Carbon Disulfide
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Carbon Tetrachloride
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Chlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Chlorodibromomethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Chloroethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 20:34
TBL
V34278
Chloroform
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Chloromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 20:34
TBL
V34278
2-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
4-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Di -Isopropyl Ether (DIPE)
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 154 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98075
Matrix: Solids
Sample ID: UST-1-111
Sampled:
6/9/2023 14:20
Analytical Method: 8260D
Prep Batch(es):
V34277
06/12/23 08:00
Prep Method: 5035
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,2-Dibromo-3-Chloropropane
<0.013
mg/Kg - dry
0.013
1
06/12/23 20:34
TBL
V34278
1,2-Dibromoethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Dibromomethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
1,2-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
1,3-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
1,4-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Dichlorodifluoromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 20:34
TBL
V34278
1,1-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
1,2-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
1,1-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
cis- 1,2-Dich loroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
trans-1,2-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
1,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
1,3-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
2,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
1,1-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
cis-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
trans-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Ethanol
<0.332
mg/Kg - dry
0.332
1
06/12/23 20:34
TBL
V34278
Ethylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Ethyl Tertiary Butyl Ether (ETBE)
<0.066
mg/Kg - dry
0.066
1
06/12/23 20:34
TBL
V34278
Hexachlorobutadiene
<0.013
mg/Kg - dry
0.013
1
06/12/23 20:34
TBL
V34278
Qualifiers/ * Outside QC Limit
DF Dilution Factor
Definitions MQL Method Quantitation Limit
Page 155 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98075 Matrix: Solids
Sample ID: UST-1-111 Sampled: 6/9/2023 14:20
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
n-Hexane
<0.013
mg/Kg - dry
0.013
1
06/12/23 20:34
TBL
V34278
2-Hexanone
<0.026
mg/Kg - dry
0.026
1
06/12/23 20:34
TBL
V34278
Isopropyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
4-Isopropyl toluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Methyl Ethyl Ketone (MEK)
<0.026
mg/Kg - dry
0.026
1
06/12/23 20:34
TBL
V34278
Methyl tert-butyl ether (MTBE) <0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
4-Methyl-2-Pentanone
<0.026
mg/Kg - dry
0.026
1
06/12/23 20:34
TBL
V34278
Methylene Chloride
<0.013
mg/Kg - dry
0.013
1
06/12/23 20:34
TBL
V34278
Naphthalene
<0.013
mg/Kg - dry
0.013
1
06/12/23 20:34
TBL
V34278
n-Propylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Styrene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
1,1,1,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
1,1,2,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Tetrachloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Toluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
1,2,3-Trichlorobenzene
<0.013
mg/Kg - dry
0.013
1
06/12/23 20:34
TBL
V34278
1,2,4-Trichlorobenzene
<0.013
mg/Kg - dry
0.013
1
06/12/23 20:34
TBL
V34278
1,1,1-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
1,1,2-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Trichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Trichlorofluoromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 20:34
TBL
V34278
1,2,3-Trichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 156 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Report Date : 06/21/2023
Received : 06/09/2023
Lab No : 98075 Matrix: Solids
Sample ID: UST-1-111 Sampled: 6/9/2023 14:20
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
1,3,5-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
Vinyl Acetate
<0.013
mg/Kg - dry
0.013
1
06/12/23 20:34
TBL
V34278
Vinyl Chloride
<0.013
mg/Kg - dry
0.013
1
06/12/23 20:34
TBL
V34278
o-Xylene
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
TBL
V34278
m,p-Xylene
<0.013
mg/Kg - dry
0.013
1
06/12/23 20:34
TBL
V34278
Xylene (Total)
<0.006
mg/Kg - dry
0.006
1
06/12/23 20:34
V34278
Surrogate: 4-Bromofluorobenzene
99.6
Limits: 70-130%
1 06/12/23 20:34 TBL
V34278
Surrogate: Dibromofluoromethane
105
Limits: 84-123%
1 06/12/23 20:34 TBL
V34278
Surrogate: Toluene-d8
96.4
Limits: 76-129%
1 06/12/23 20:34 TBL
V34278
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Acenaphthylene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Aniline
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Anthracene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Benzo(a)anthracene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Benzo(a)pyrene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Benzo(b)fluoranthene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Benzo(g,h,i)perylene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 157 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98075
Matrix: Solids
Sample ID: UST-1-111
Sampled:
6/9/2023 14:20
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzo(k)fluoranthene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Benzoic Acid
<2.66
mg/Kg - dry
2.66
1
06/14/23 21:35
AMP
V34353
Benzyl alcohol
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Bis(2-Chloroethoxy)methane
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Bis(2-Chloroethyl)ether
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Bis(2-Chloroisopropyl)ether
<0.439
mg/Kg - dry
0.439
1
06/14/23 21:35
AMP
V34353
Bis(2-ethylhexyl)phthalate
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
4-13romophenyl phenyl ether
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Butyl benzyl phthalate
<0.439
mg/Kg - dry
0.439
1
06/14/23 21:35
AMP
V34353
4-Chloro-3-methylphenol
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
4-Chloroaniline
<0.439
mg/Kg - dry
0.439
1
06/14/23 21:35
AMP
V34353
2-Chloronaphthalene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
2-Chlorophenol
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
4-Chlorophenyl phenyl ether
<1.33
mg/Kg - dry
1.33
1
06/14/23 21:35
AMP
V34353
Chrysene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Dibenz(a,h)anthracene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Dibenzofuran
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
1,2-Dichlorobenzene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
1,3-Dichlorobenzene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
1,4-Dichlorobenzene
<0.439
mg/Kg - dry
0.439
1
06/14/23 21:35
AMP
V34353
3,3'-Dichlorobenzidine
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
2,4-Dichlorophenol
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 158 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98075
Matrix: Solids
Sample ID: UST-1-111
Sampled:
6/9/2023 14:20
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Dimethyl phthalate
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
2,4-Dimethyl phenol
<0.439
mg/Kg - dry
0.439
1
06/14/23 21:35
AMP
V34353
Di-n-butyl phthalate
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
4,6-Dinitro-2-methylphenol
<2.00
mg/Kg - dry
2.00
1
06/14/23 21:35
AMP
V34353
2,4-Dinitrophenol
<2.00
mg/Kg - dry
2.00
1
06/14/23 21:35
AMP
V34353
2,4-Dinitrotoluene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
2,6-Dinitrotoluene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Di-n-Octyl Phthalate
<0.439
mg/Kg - dry
0.439
1
06/14/23 21:35
AMP
V34353
Fluoranthene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Fluorene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Hexachlorobenzene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Hexachlorobutadiene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Hexachlorocyclopentadiene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Hexachloroethane
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Indeno(1,2,3-cd)pyrene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Isophorone
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
1-Methylnaphthalene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
2-Methylnaphthalene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
2-Methylphenol
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
3&4 Methylphenol
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Naphthalene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 159 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98075
Matrix: Solids
Sample ID: UST-1-111
Sampled: 6/9/2023
14:20
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
2-Nitroaniline
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35 AMP
V34353
3-Nitroaniline
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35 AMP
V34353
4-Nitroaniline
<0.439
mg/Kg - dry
0.439
1
06/14/23 21:35 AMP
V34353
Nitrobenzene
<0.439
mg/Kg - dry
0.439
1
06/14/23 21:35 AMP
V34353
2-Nitrophenol
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35 AMP
V34353
4-Nitrophenol
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35 AMP
V34353
N-Nitrosodimethylamine
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35 AMP
V34353
N-Nitrosodiphenylamine
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35 AMP
V34353
N-Nitroso-di-n-propylamine
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35 AMP
V34353
Pentachlorophenol
<1.33
mg/Kg - dry
1.33
1
06/14/23 21:35 AMP
V34353
Phenanthrene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35 AMP
V34353
Phenol
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35 AMP
V34353
Pyrene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35 AMP
V34353
Pyridine
<0.439
mg/Kg - dry
0.439
1
06/14/23 21:35 AMP
V34353
1,2,4-Trichlorobenzene
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35 AMP
V34353
2,4,5-Trichlorophenol
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35 AMP
V34353
2,4,6-Trichlorophenol
<0.878
mg/Kg - dry
0.878
1
06/14/23 21:35 AMP
V34353
Surrogate: Phenol-d5
56.2
Limits: 34-121%
1 06/14/23 21:35 AMP
8270E
Surrogate: 2-Fluorobiphenyl
71.9
Limits: 44-115%
1 06/14/23 21:35 AMP
V34353
Surrogate: 2-Fluorophenol
61.6
Limits: 35-115%
1 06/14/23 21:35 AMP
V34353
Surrogate: Nitrobenzene-d5
67.1
Limits: 37-122%
1 06/14/23 21:35 AMP
V34353
Surrogate: 4-Terphenyl-d14
78.4
Limits: 54-127%
1 06/14/23 21:35 AMP
V34353
Surrogate: 2,4,6-Tribromophenol
58.9
Limits: 39-132%
1 06/14/23 21:35 AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 160 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98075 Matrix: Solids
Sample ID: UST-1-111 Sampled: 6/9/2023 14:20
Analytical Method: MADEP-EPH
Prep Method: MAEPH (Prep)
Test
Aliphatic C9-C18
Aliphatic C19-C36
Aromatic C11-C22
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Analytical Method: MADEP-VPH
Prep Method: MAVPH (Prep)
Test
Prep Batch(es): V34271 06/13/23 10:20
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
<66.6 mg/Kg - dry
66.6 1
06/17/23 03:18 AMP
V34449
<66.6 mg/Kg - dry
66.6 1
06/17/23 03:18 AMP
V34449
<66.6 mg/Kg - dry
66.6 1
06/17/23 03:18 AMP
V34449
123
Limits: 40-140%
1 06/17/23 03:18 AMP
MADEP-EPH
80.8
Limits: 40-140%
1 06/17/23 03:18 AMP
MADEP-EPH
113
Limits: 40-140%
1 06/17/23 03:18 AMP
MADEP-EPH
122
Limits: 40-140%
1 06/17/23 03:18 AMP
V34449
Prep Batch(es):
V34232 06/12/23 08:00
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Aliphatic C5-C8 <10.7
Aliphatic C9-C12 <10.7
Aromatic C9-C10 <10.7
Surrogate: 2,5-Dibromotoluene (FID)
Surrogate: 2,5-Dibromotoluene (PID)
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
mg/Kg - dry
10.7
100 06/12/23 19:56 TBL
V34233
mg/Kg - dry
10.7
100 06/12/23 19:56 TBL
V34233
mg/Kg - dry
10.7
100 06/12/23 19:56 TBL
V34233
107
Limits: 70-130%
100 06/12/23 19:56 TBL
MADEP-VPH
104
Limits: 70-130%
100 06/12/23 19:56 TBL
MADEP-VPH
DF Dilution Factor
Page 161 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98076 Matrix: Solids
Sample ID: UST-1-I Sampled: 6/9/2023 15:10
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
28.8 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 162 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98076 Matrix: Solids
Sample ID: UST-1-I Sampled: 6/9/2023 15:10
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Acetone
<0.028
mg/Kg - dry
0.028
1
06/12/23 21:01
TBL
V34278
Acrolein
<0.028
mg/Kg - dry
0.028
1
06/12/23 21:01
TBL
V34278
Acrylonitrile
<0.028
mg/Kg - dry
0.028
1
06/12/23 21:01
TBL
V34278
Benzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Bromobenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Bromochloromethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Bromodichloromethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Bromoform
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Bromomethane
<0.014
mg/Kg - dry
0.014
1
06/12/23 21:01
TBL
V34278
n-Butylbenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
sec -Butyl benzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
tert-Butyl benzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Carbon Disulfide
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Carbon Tetrachloride
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Chlorobenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Chlorodibromomethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Chloroethane
<0.014
mg/Kg - dry
0.014
1
06/12/23 21:01
TBL
V34278
Chloroform
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Chloromethane
<0.014
mg/Kg - dry
0.014
1
06/12/23 21:01
TBL
V34278
2-Chlorotoluene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
4-Chlorotoluene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Di -Isopropyl Ether (DIPE)
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 163 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98076
Matrix: Solids
Sample ID: UST-1-I
Sampled:
6/9/2023 15:10
Analytical Method: 8260D
Prep Batch(es):
V34277
06/12/23 08:00
Prep Method: 5035
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,2-Dibromo-3-Chloropropane
<0.014
mg/Kg - dry
0.014
1
06/12/23 21:01
TBL
V34278
1,2-Dibromoethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Dibromomethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
1,2-Dichlorobenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
1,3-Dichlorobenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
1,4-Dichlorobenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Dichlorodifluoromethane
<0.014
mg/Kg - dry
0.014
1
06/12/23 21:01
TBL
V34278
1,1-Dichloroethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
1,2-Dichloroethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
1,1-Dichloroethene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
cis- 1,2-Dich loroethene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
trans-1,2-Dichloroethene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
1,2-Dichloropropane
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
1,3-Dichloropropane
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
2,2-Dichloropropane
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
1,1-Dichloropropene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
cis-1,3-Dichloropropene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
trans-1,3-Dichloropropene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Ethanol
<0.351
mg/Kg - dry
0.351
1
06/12/23 21:01
TBL
V34278
Ethylbenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Ethyl Tertiary Butyl Ether (ETBE)
<0.070
mg/Kg - dry
0.070
1
06/12/23 21:01
TBL
V34278
Hexachlorobutadiene
<0.014
mg/Kg - dry
0.014
1
06/12/23 21:01
TBL
V34278
Qualifiers/ * Outside QC Limit
DF Dilution Factor
Definitions MQL Method Quantitation Limit
Page 164 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98076 Matrix: Solids
Sample ID: UST-1-I Sampled: 6/9/2023 15:10
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
n-Hexane
<0.014
mg/Kg - dry
0.014
1
06/12/23 21:01
TBL
V34278
2-Hexanone
<0.028
mg/Kg - dry
0.028
1
06/12/23 21:01
TBL
V34278
Isopropyl benzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
4-Isopropyl toluene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Methyl Ethyl Ketone (MEK)
<0.028
mg/Kg - dry
0.028
1
06/12/23 21:01
TBL
V34278
Methyl tert-butyl ether (MTBE) <0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
4-Methyl-2-Pentanone
<0.028
mg/Kg - dry
0.028
1
06/12/23 21:01
TBL
V34278
Methylene Chloride
<0.014
mg/Kg - dry
0.014
1
06/12/23 21:01
TBL
V34278
Naphthalene
<0.014
mg/Kg - dry
0.014
1
06/12/23 21:01
TBL
V34278
n-Propylbenzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Styrene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
1,1,1,2-Tetrachloroethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
1,1,2,2-Tetrachloroethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Tetrachloroethene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Toluene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
1,2,3-Trichlorobenzene
<0.014
mg/Kg - dry
0.014
1
06/12/23 21:01
TBL
V34278
1,2,4-Trichlorobenzene
<0.014
mg/Kg - dry
0.014
1
06/12/23 21:01
TBL
V34278
1,1,1-Trichloroethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
1,1,2-Trichloroethane
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Trichloroethene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Trichlorofluoromethane
<0.014
mg/Kg - dry
0.014
1
06/12/23 21:01
TBL
V34278
1,2,3-Trichloropropane
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 165 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Report Date : 06/21/2023
Received : 06/09/2023
Lab No : 98076 Matrix: Solids
Sample ID: UST-1-I Sampled: 6/9/2023 15:10
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
1,3,5-Trimethyl benzene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
Vinyl Acetate
<0.014
mg/Kg - dry
0.014
1
06/12/23 21:01
TBL
V34278
Vinyl Chloride
<0.014
mg/Kg - dry
0.014
1
06/12/23 21:01
TBL
V34278
o-Xylene
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
TBL
V34278
m,p-Xylene
<0.014
mg/Kg - dry
0.014
1
06/12/23 21:01
TBL
V34278
Xylene (Total)
<0.007
mg/Kg - dry
0.007
1
06/12/23 21:01
V34278
Surrogate: 4-Bromofluorobenzene
101
Limits: 70-130%
1 06/12/23 21:01 TBL
V34278
Surrogate: Dibromofluoromethane
104
Limits: 84-123%
1 06/12/23 21:01 TBL
V34278
Surrogate: Toluene-d8
95.4
Limits: 76-129%
1 06/12/23 21:01 TBL
V34278
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Acenaphthylene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Aniline
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Anthracene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Benzo(a)anthracene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Benzo(a)pyrene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Benzo(b)fluoranthene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Benzo(g,h,i)perylene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 166 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98076
Matrix: Solids
Sample ID: UST-1-I
Sampled:
6/9/2023 15:10
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzo(k)fluoranthene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Benzoic Acid
<2.81
mg/Kg - dry
2.81
1
06/14/23 21:57
AMP
V34353
Benzyl alcohol
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Bis(2-Chloroethoxy)methane
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Bis(2-Chloroethyl)ether
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Bis(2-Chloroisopropyl)ether
<0.463
mg/Kg - dry
0.463
1
06/14/23 21:57
AMP
V34353
Bis(2-ethylhexyl)phthalate
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
4-13romophenyl phenyl ether
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Butyl benzyl phthalate
<0.463
mg/Kg - dry
0.463
1
06/14/23 21:57
AMP
V34353
4-Chloro-3-methylphenol
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
4-Chloroaniline
<0.463
mg/Kg - dry
0.463
1
06/14/23 21:57
AMP
V34353
2-Chloronaphthalene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
2-Chlorophenol
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
4-Chlorophenyl phenyl ether
<1.40
mg/Kg - dry
1.40
1
06/14/23 21:57
AMP
V34353
Chrysene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Dibenz(a,h)anthracene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Dibenzofuran
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
1,2-Dichlorobenzene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
1,3-Dichlorobenzene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
1,4-Dichlorobenzene
<0.463
mg/Kg - dry
0.463
1
06/14/23 21:57
AMP
V34353
3,3'-Dichlorobenzidine
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
2,4-Dichlorophenol
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 167 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98076
Matrix: Solids
Sample ID: UST-1-I
Sampled:
6/9/2023 15:10
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Dimethyl phthalate
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
2,4-Dimethyl phenol
<0.463
mg/Kg - dry
0.463
1
06/14/23 21:57
AMP
V34353
Di-n-butyl phthalate
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
4,6-Dinitro-2-methylphenol
<2.11
mg/Kg - dry
2.11
1
06/14/23 21:57
AMP
V34353
2,4-Dinitrophenol
<2.11
mg/Kg - dry
2.11
1
06/14/23 21:57
AMP
V34353
2,4-Dinitrotoluene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
2,6-Dinitrotoluene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Di-n-Octyl Phthalate
<0.463
mg/Kg - dry
0.463
1
06/14/23 21:57
AMP
V34353
Fluoranthene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Fluorene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Hexachlorobenzene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Hexachlorobutadiene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Hexachlorocyclopentadiene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Hexachloroethane
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Indeno(1,2,3-cd)pyrene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Isophorone
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
1-Methylnaphthalene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
2-Methylnaphthalene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
2-Methylphenol
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
3&4 Methylphenol
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Naphthalene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 168 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98076
Matrix: Solids
Sample ID: UST-1-I
Sampled: 6/9/2023
15:10
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
2-Nitroaniline
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57 AMP
V34353
3-Nitroaniline
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57 AMP
V34353
4-Nitroaniline
<0.463
mg/Kg - dry
0.463
1
06/14/23 21:57 AMP
V34353
Nitrobenzene
<0.463
mg/Kg - dry
0.463
1
06/14/23 21:57 AMP
V34353
2-Nitrophenol
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57 AMP
V34353
4-Nitrophenol
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57 AMP
V34353
N-Nitrosodimethylamine
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57 AMP
V34353
N-Nitrosodiphenylamine
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57 AMP
V34353
N-Nitroso-di-n-propylamine
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57 AMP
V34353
Pentachlorophenol
<1.40
mg/Kg - dry
1.40
1
06/14/23 21:57 AMP
V34353
Phenanthrene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57 AMP
V34353
Phenol
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57 AMP
V34353
Pyrene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57 AMP
V34353
Pyridine
<0.463
mg/Kg - dry
0.463
1
06/14/23 21:57 AMP
V34353
1,2,4-Trichlorobenzene
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57 AMP
V34353
2,4,5-Trichlorophenol
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57 AMP
V34353
2,4,6-Trichlorophenol
<0.926
mg/Kg - dry
0.926
1
06/14/23 21:57 AMP
V34353
Surrogate: Phenol-d5
56.5
Limits: 34-121%
1 06/14/23 21:57 AMP
8270E
Surrogate: 2-Fluorobiphenyl
71.9
Limits: 44-115%
1 06/14/23 21:57 AMP
V34353
Surrogate: 2-Fluorophenol
62.8
Limits: 35-115%
1 06/14/23 21:57 AMP
V34353
Surrogate: Nitrobenzene-d5
68.9
Limits: 37-122%
1 06/14/23 21:57 AMP
V34353
Surrogate: 4-Terphenyl-d14
75.4
Limits: 54-127%
1 06/14/23 21:57 AMP
V34353
Surrogate: 2,4,6-Tribromophenol
58.3
Limits: 39-132%
1 06/14/23 21:57 AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 169 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98076 Matrix: Solids
Sample ID: UST-1-I Sampled: 6/9/2023 15:10
Analytical Method: MADEP-EPH
Prep Method: MAEPH (Prep)
Test
Aliphatic C9-C18
Aliphatic C19-C36
Aromatic C11-C22
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Analytical Method: MADEP-VPH
Prep Method: MAVPH (Prep)
Test
Prep Batch(es): V34271 06/13/23 10:20
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
<70.1 mg/Kg - dry
70.1 1
06/17/23 03:55 AMP
V34449
<70.1 mg/Kg - dry
70.1 1
06/17/23 03:55 AMP
V34449
<70.1 mg/Kg - dry
70.1 1
06/17/23 03:55 AMP
V34449
131
Limits: 40-140%
1 06/17/23 03:55 AMP
MADEP-EPH
72.7
Limits: 40-140%
1 06/17/23 03:55 AMP
MADEP-EPH
113
Limits: 40-140%
1 06/17/23 03:55 AMP
MADEP-EPH
127
Limits: 40-140%
1 06/17/23 03:55 AMP
V34449
Prep Batch(es):
V34232 06/12/23 08:00
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Aliphatic C5-C8 <11.2
Aliphatic C9-C12 <11.2
Aromatic C9-C10 <11.2
Surrogate: 2,5-Dibromotoluene (FID)
Surrogate: 2,5-Dibromotoluene (PID)
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
mg/Kg - dry
11.2
100 06/12/23 20:20 TBL
V34233
mg/Kg - dry
11.2
100 06/12/23 20:20 TBL
V34233
mg/Kg - dry
11.2
100 06/12/23 20:20 TBL
V34233
96.3
Limits: 70-130%
100 06/12/23 20:20 TBL
MADEP-VPH
98.1
Limits: 70-130%
100 06/12/23 20:20 TBL
MADEP-VPH
DF Dilution Factor
Page 170 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98077 Matrix: Solids
Sample ID: UST-1-1 Sampled: 6/9/2023 14:05
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
20.5 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 171 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98077 Matrix: Solids
Sample ID: UST-1-1 Sampled: 6/9/2023 14:05
Analytical Method: 8260D Prep Batch(es): V34299 06/13/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Acetone
<0.025
mg/Kg - dry
0.025
1
06/13/23 12:56
TBL
V34300
Acrolein
<0.025
mg/Kg - dry
0.025
1
06/13/23 12:56
TBL
V34300
Acrylonitrile
<0.025
mg/Kg - dry
0.025
1
06/13/23 12:56
TBL
V34300
Benzene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Bromobenzene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Bromochloromethane
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Bromodichloromethane
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Bromoform
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Bromomethane
<0.012
mg/Kg - dry
0.012
1
06/13/23 12:56
TBL
V34300
n-Butylbenzene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
sec -Butyl benzene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
tert-Butyl benzene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Carbon Disulfide
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Carbon Tetrachloride
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Chlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Chlorodibromomethane
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Chloroethane
<0.012
mg/Kg - dry
0.012
1
06/13/23 12:56
TBL
V34300
Chloroform
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Chloromethane
<0.012
mg/Kg - dry
0.012
1
06/13/23 12:56
TBL
V34300
2-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
4-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Di -Isopropyl Ether (DIPE)
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 172 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98077 Matrix: Solids
Sample ID: UST-1-1 Sampled: 6/9/2023 14:05
Analytical Method: 8260D Prep Batch(es): V34299 06/13/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dibromo-3-Chloropropane
<0.012
mg/Kg - dry
0.012
1
06/13/23 12:56
TBL
V34300
1,2-Dibromoethane
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Dibromomethane
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
1,2-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
1,3-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
1,4-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Dichlorodifluoromethane
<0.012
mg/Kg - dry
0.012
1
06/13/23 12:56
TBL
V34300
1,1-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
1,2-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
1,1-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
cis- 1,2-Dich loroethene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
trans-1,2-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
1,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
1,3-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
2,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
1,1-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
cis-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
trans-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Ethanol
<0.314
mg/Kg - dry
0.314
1
06/13/23 12:56
TBL
V34300
Ethylbenzene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Ethyl Tertiary Butyl Ether (ETBE) <0.062
mg/Kg - dry
0.062
1
06/13/23 12:56
TBL
V34300
Hexachlorobutadiene
<0.012
mg/Kg - dry
0.012
1
06/13/23 12:56
TBL
V34300
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 173 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98077 Matrix: Solids
Sample ID: UST-1-1 Sampled: 6/9/2023 14:05
Analytical Method: 8260D Prep Batch(es): V34299 06/13/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
n-Hexane
<0.012
mg/Kg - dry
0.012
1
06/13/23 12:56
TBL
V34300
2-Hexanone
<0.025
mg/Kg - dry
0.025
1
06/13/23 12:56
TBL
V34300
Isopropyl benzene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
4-Isopropyl toluene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Methyl Ethyl Ketone (MEK)
<0.025
mg/Kg - dry
0.025
1
06/13/23 12:56
TBL
V34300
Methyl tert-butyl ether (MTBE) <0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
4-Methyl-2-Pentanone
<0.025
mg/Kg - dry
0.025
1
06/13/23 12:56
TBL
V34300
Methylene Chloride
<0.012
mg/Kg - dry
0.012
1
06/13/23 12:56
TBL
V34300
Naphthalene
<0.012
mg/Kg - dry
0.012
1
06/13/23 12:56
TBL
V34300
n-Propylbenzene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Styrene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
1,1,1,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
1,1,2,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Tetrachloroethene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Toluene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
1,2,3-Trichlorobenzene
<0.012
mg/Kg - dry
0.012
1
06/13/23 12:56
TBL
V34300
1,2,4-Trichlorobenzene
<0.012
mg/Kg - dry
0.012
1
06/13/23 12:56
TBL
V34300
1,1,1-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
1,1,2-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Trichloroethene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Trichlorofluoromethane
<0.012
mg/Kg - dry
0.012
1
06/13/23 12:56
TBL
V34300
1,2,3-Trichloropropane
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 174 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Report Date : 06/21/2023
Received : 06/09/2023
Lab No : 98077 Matrix: Solids
Sample ID: UST-1-1 Sampled: 6/9/2023 14:05
Analytical Method: 8260D Prep Batch(es): V34299 06/13/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
1,3,5-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
Vinyl Acetate
<0.012
mg/Kg - dry
0.012
1
06/13/23 12:56
TBL
V34300
Vinyl Chloride
<0.012
mg/Kg - dry
0.012
1
06/13/23 12:56
TBL
V34300
o-Xylene
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
TBL
V34300
m,p-Xylene
<0.012
mg/Kg - dry
0.012
1
06/13/23 12:56
TBL
V34300
Xylene (Total)
<0.006
mg/Kg - dry
0.006
1
06/13/23 12:56
V34300
Surrogate:4-Bromofluorobenzene
102
Limits:70-130%
1 06/13/23 12:56 TBL
V34300
Surrogate: Dibromofluoromethane
103
Limits: 84-123%
1 06/13/23 12:56 TBL
V34300
Surrogate: Toluene-d8
95.5
Limits: 76-129%
1 06/13/23 12:56 TBL
V34300
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Acenaphthylene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Aniline
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Anthracene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Benzo(a)anthracene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Benzo(a)pyrene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Benzo(b)fluoranthene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Benzo(g,h,i)perylene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 175 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98077
Matrix: Solids
Sample ID: UST-1-1
Sampled:
6/9/2023 14:05
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzo(k)fluoranthene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Benzoic Acid
<2.52
mg/Kg - dry
2.52
1
06/14/23 22:20
AMP
V34353
Benzyl alcohol
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Bis(2-Chloroethoxy)methane
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Bis(2-Chloroethyl)ether
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Bis(2-Chloroisopropyl)ether
<0.415
mg/Kg - dry
0.415
1
06/14/23 22:20
AMP
V34353
Bis(2-ethylhexyl)phthalate
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
4-13romophenyl phenyl ether
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Butyl benzyl phthalate
<0.415
mg/Kg - dry
0.415
1
06/14/23 22:20
AMP
V34353
4-Chloro-3-methylphenol
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
4-Chloroaniline
<0.415
mg/Kg - dry
0.415
1
06/14/23 22:20
AMP
V34353
2-Chloronaphthalene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
2-Chlorophenol
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
4-Chlorophenyl phenyl ether
<1.26
mg/Kg - dry
1.26
1
06/14/23 22:20
AMP
V34353
Chrysene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Dibenz(a,h)anthracene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Dibenzofuran
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
1,2-Dichlorobenzene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
1,3-Dichlorobenzene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
1,4-Dichlorobenzene
<0.415
mg/Kg - dry
0.415
1
06/14/23 22:20
AMP
V34353
3,3'-Dichlorobenzidine
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
2,4-Dichlorophenol
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 176 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98077
Matrix: Solids
Sample ID: UST-1-1
Sampled:
6/9/2023 14:05
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Dimethyl phthalate
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
2,4-Dimethyl phenol
<0.415
mg/Kg - dry
0.415
1
06/14/23 22:20
AMP
V34353
Di-n-butyl phthalate
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
4,6-Dinitro-2-methylphenol
<1.89
mg/Kg - dry
1.89
1
06/14/23 22:20
AMP
V34353
2,4-Dinitrophenol
<1.89
mg/Kg - dry
1.89
1
06/14/23 22:20
AMP
V34353
2,4-Dinitrotoluene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
2,6-Dinitrotoluene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Di-n-Octyl Phthalate
<0.415
mg/Kg - dry
0.415
1
06/14/23 22:20
AMP
V34353
Fluoranthene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Fluorene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Hexachlorobenzene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Hexachlorobutadiene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Hexachlorocyclopentadiene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Hexachloroethane
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Indeno(1,2,3-cd)pyrene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Isophorone
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
1-Methylnaphthalene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
2-Methylnaphthalene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
2-Methylphenol
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
3&4 Methylphenol
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Naphthalene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 177 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98077
Matrix: Solids
Sample ID: UST-1-1
Sampled: 6/9/2023
14:05
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
2-Nitroaniline
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20 AMP
V34353
3-Nitroaniline
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20 AMP
V34353
4-Nitroaniline
<0.415
mg/Kg - dry
0.415
1
06/14/23 22:20 AMP
V34353
Nitrobenzene
<0.415
mg/Kg - dry
0.415
1
06/14/23 22:20 AMP
V34353
2-Nitrophenol
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20 AMP
V34353
4-Nitrophenol
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20 AMP
V34353
N-Nitrosodimethylamine
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20 AMP
V34353
N-Nitrosodiphenylamine
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20 AMP
V34353
N-Nitroso-di-n-propylamine
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20 AMP
V34353
Pentachlorophenol
<1.26
mg/Kg - dry
1.26
1
06/14/23 22:20 AMP
V34353
Phenanthrene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20 AMP
V34353
Phenol
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20 AMP
V34353
Pyrene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20 AMP
V34353
Pyridine
<0.415
mg/Kg - dry
0.415
1
06/14/23 22:20 AMP
V34353
1,2,4-Trichlorobenzene
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20 AMP
V34353
2,4,5-Trichlorophenol
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20 AMP
V34353
2,4,6-Trichlorophenol
<0.830
mg/Kg - dry
0.830
1
06/14/23 22:20 AMP
V34353
Surrogate: Phenol-d5
57.1
Limits: 34-121%
1 06/14/23 22:20 AMP
8270E
Surrogate: 2-Fluorobiphenyl
73.5
Limits: 44-115%
1 06/14/23 22:20 AMP
V34353
Surrogate: 2-Fluorophenol
61.9
Limits: 35-115%
1 06/14/23 22:20 AMP
V34353
Surrogate: Nitrobenzene-d5
70.5
Limits: 37-122%
1 06/14/23 22:20 AMP
V34353
Surrogate: 4-Terphenyl-d14
72.3
Limits: 54-127%
1 06/14/23 22:20 AMP
V34353
Surrogate: 2,4,6-Tribromophenol
55.0
Limits: 39-132%
1 06/14/23 22:20 AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 178 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98077 Matrix: Solids
Sample ID: UST-1-1 Sampled: 6/9/2023 14:05
Analytical Method: MADEP-EPH
Prep Method: MAEPH (Prep)
Test
Aliphatic C9-C18
Aliphatic C19-C36
Aromatic C11-C22
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Analytical Method: MADEP-VPH
Prep Method: MAVPH (Prep)
Test
Prep Batch(es): V34271 06/13/23 10:20
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
<63.0 mg/Kg - dry
63.0 1
06/17/23 04:31 AMP
V34449
<63.0 mg/Kg - dry
63.0 1
06/17/23 04:31 AMP
V34449
<63.0 mg/Kg - dry
63.0 1
06/17/23 04:31 AMP
V34449
121
Limits: 40-140%
1 06/17/23 04:31 AMP
MADEP-EPH
83.3
Limits: 40-140%
1 06/17/23 04:31 AMP
MADEP-EPH
114
Limits: 40-140%
1 06/17/23 04:31 AMP
MADEP-EPH
119
Limits: 40-140%
1 06/17/23 04:31 AMP
V34449
Prep Batch(es):
V34232 06/12/23 08:00
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Aliphatic C5-C8 <10.1
Aliphatic C9-C12 <10.1
Aromatic C9-C10 <10.1
Surrogate: 2,5-Dibromotoluene (FID)
Surrogate: 2,5-Dibromotoluene (PID)
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
mg/Kg - dry
10.1
100 06/12/23 20:43 TBL
V34233
mg/Kg - dry
10.1
100 06/12/23 20:43 TBL
V34233
mg/Kg - dry
10.1
100 06/12/23 20:43 TBL
V34233
110
Limits: 70-130%
100 06/12/23 20:43 TBL
MADEP-VPH
118
Limits: 70-130%
100 06/12/23 20:43 TBL
MADEP-VPH
DF Dilution Factor
Page 179 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98078 Matrix: Solids
Sample ID: UST-1-K Sampled: 6/9/2023 14:35
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
28.2 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 06/13/2316:32 CNC SW-DRYWT
DF Dilution Factor
Page 180 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98078 Matrix: Solids
Sample ID: UST-1-K Sampled: 6/9/2023 14:35
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Acetone
<0.027
mg/Kg - dry
0.027
1
06/12/23 21:55
TBL
V34278
Acrolein
<0.027
mg/Kg - dry
0.027
1
06/12/23 21:55
TBL
V34278
Acrylonitrile
<0.027
mg/Kg - dry
0.027
1
06/12/23 21:55
TBL
V34278
Benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Bromobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Bromochloromethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Bromodichloromethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Bromoform
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Bromomethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 21:55
TBL
V34278
n-Butylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
sec -Butyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
tert-Butyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Carbon Disulfide
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Carbon Tetrachloride
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Chlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Chlorodibromomethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Chloroethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 21:55
TBL
V34278
Chloroform
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Chloromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 21:55
TBL
V34278
2-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
4-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Di -Isopropyl Ether (DIPE)
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 181 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98078 Matrix: Solids
Sample ID: UST-1-K Sampled: 6/9/2023 14:35
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dibromo-3-Chloropropane
<0.013
mg/Kg - dry
0.013
1
06/12/23 21:55
TBL
V34278
1,2-Dibromoethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Dibromomethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
1,2-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
1,3-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
1,4-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Dichlorodifluoromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 21:55
TBL
V34278
1,1-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
1,2-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
1,1-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
cis- 1,2-Dich loroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
trans-1,2-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
1,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
1,3-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
2,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
1,1-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
cis-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
trans-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Ethanol
<0.348
mg/Kg - dry
0.348
1
06/12/23 21:55
TBL
V34278
Ethylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Ethyl Tertiary Butyl Ether (ETBE) <0.069
mg/Kg - dry
0.069
1
06/12/23 21:55
TBL
V34278
Hexachlorobutadiene
<0.013
mg/Kg - dry
0.013
1
06/12/23 21:55
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 182 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98078 Matrix: Solids
Sample ID: UST-1-K Sampled: 6/9/2023 14:35
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
n-Hexane
<0.013
mg/Kg - dry
0.013
1
06/12/23 21:55
TBL
V34278
2-Hexanone
<0.027
mg/Kg - dry
0.027
1
06/12/23 21:55
TBL
V34278
Isopropyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
4-Isopropyl toluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Methyl Ethyl Ketone (MEK)
<0.027
mg/Kg - dry
0.027
1
06/12/23 21:55
TBL
V34278
Methyl tert-butyl ether (MTBE) <0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
4-Methyl-2-Pentanone
<0.027
mg/Kg - dry
0.027
1
06/12/23 21:55
TBL
V34278
Methylene Chloride
<0.013
mg/Kg - dry
0.013
1
06/12/23 21:55
TBL
V34278
Naphthalene
<0.013
mg/Kg - dry
0.013
1
06/12/23 21:55
TBL
V34278
n-Propylbenzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Styrene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
1,1,1,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
1,1,2,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Tetrachloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Toluene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
1,2,3-Trichlorobenzene
<0.013
mg/Kg - dry
0.013
1
06/12/23 21:55
TBL
V34278
1,2,4-Trichlorobenzene
<0.013
mg/Kg - dry
0.013
1
06/12/23 21:55
TBL
V34278
1,1,1-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
1,1,2-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Trichloroethene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Trichlorofluoromethane
<0.013
mg/Kg - dry
0.013
1
06/12/23 21:55
TBL
V34278
1,2,3-Trichloropropane
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 183 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Report Date : 06/21/2023
Received : 06/09/2023
Lab No : 98078 Matrix: Solids
Sample ID: UST-1-K Sampled: 6/9/2023 14:35
Analytical Method: 8260D Prep Batch(es): V34277 06/12/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
1,3,5-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
Vinyl Acetate
<0.013
mg/Kg - dry
0.013
1
06/12/23 21:55
TBL
V34278
Vinyl Chloride
<0.013
mg/Kg - dry
0.013
1
06/12/23 21:55
TBL
V34278
o-Xylene
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
TBL
V34278
m,p-Xylene
<0.013
mg/Kg - dry
0.013
1
06/12/23 21:55
TBL
V34278
Xylene (Total)
<0.006
mg/Kg - dry
0.006
1
06/12/23 21:55
V34278
Surrogate: 4-Bromofluorobenzene
101
Limits: 70-130%
1 06/12/23 21:55 TBL
V34278
Surrogate: Dibromofluoromethane
106
Limits: 84-123%
1 06/12/23 21:55 TBL
V34278
Surrogate: Toluene-d8
96.2
Limits: 76-129%
1 06/12/23 21:55 TBL
V34278
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Acenaphthylene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Aniline
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Anthracene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Benzo(a)anthracene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Benzo(a)pyrene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Benzo(b)fluoranthene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Benzo(g,h,i)perylene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 184 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98078
Matrix: Solids
Sample ID: UST-1-K
Sampled:
6/9/2023 14:35
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzo(k)fluoranthene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Benzoic Acid
<2.79
mg/Kg - dry
2.79
1
06/14/23 22:42
AMP
V34353
Benzyl alcohol
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Bis(2-Chloroethoxy)methane
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Bis(2-Chloroethyl)ether
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Bis(2-Chloroisopropyl)ether
<0.459
mg/Kg - dry
0.459
1
06/14/23 22:42
AMP
V34353
Bis(2-ethylhexyl)phthalate
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
4-13romophenyl phenyl ether
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Butyl benzyl phthalate
<0.459
mg/Kg - dry
0.459
1
06/14/23 22:42
AMP
V34353
4-Chloro-3-methylphenol
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
4-Chloroaniline
<0.459
mg/Kg - dry
0.459
1
06/14/23 22:42
AMP
V34353
2-Chloronaphthalene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
2-Chlorophenol
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
4-Chlorophenyl phenyl ether
<1.39
mg/Kg - dry
1.39
1
06/14/23 22:42
AMP
V34353
Chrysene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Dibenz(a,h)anthracene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Dibenzofuran
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
1,2-Dichlorobenzene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
1,3-Dichlorobenzene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
1,4-Dichlorobenzene
<0.459
mg/Kg - dry
0.459
1
06/14/23 22:42
AMP
V34353
3,3'-Dichlorobenzidine
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
2,4-Dichlorophenol
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 185 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98078
Matrix: Solids
Sample ID: UST-1-K
Sampled:
6/9/2023 14:35
Analytical Method: 8270E
Prep Batch(es):
V34327
06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Dimethyl phthalate
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
2,4-Dimethyl phenol
<0.459
mg/Kg - dry
0.459
1
06/14/23 22:42
AMP
V34353
Di-n-butyl phthalate
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
4,6-Dinitro-2-methylphenol
<2.09
mg/Kg - dry
2.09
1
06/14/23 22:42
AMP
V34353
2,4-Dinitrophenol
<2.09
mg/Kg - dry
2.09
1
06/14/23 22:42
AMP
V34353
2,4-Dinitrotoluene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
2,6-Dinitrotoluene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Di-n-Octyl Phthalate
<0.459
mg/Kg - dry
0.459
1
06/14/23 22:42
AMP
V34353
Fluoranthene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Fluorene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Hexachlorobenzene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Hexachlorobutadiene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Hexachlorocyclopentadiene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Hexachloroethane
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Indeno(1,2,3-cd)pyrene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Isophorone
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
1-Methylnaphthalene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
2-Methylnaphthalene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
2-Methylphenol
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
3&4 Methylphenol
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Naphthalene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42
AMP
V34353
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 186 of 229

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 06/21/2023
2923 South Tryon St. Ste 100 Information : Received : 06/09/2023
Charlotte , NC 28203
Report Number : 23-163-0001
REPORT OF ANAL YSIS
Lab No : 98078
Matrix: Solids
Sample ID: UST-1-K
Sampled: 6/9/2023
14:35
Analytical Method: 8270E
Prep Batch(es):
V34327 06/14/23 09:30
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
2-Nitroaniline
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42 AMP
V34353
3-Nitroaniline
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42 AMP
V34353
4-Nitroaniline
<0.459
mg/Kg - dry
0.459
1
06/14/23 22:42 AMP
V34353
Nitrobenzene
<0.459
mg/Kg - dry
0.459
1
06/14/23 22:42 AMP
V34353
2-Nitrophenol
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42 AMP
V34353
4-Nitrophenol
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42 AMP
V34353
N-Nitrosodimethylamine
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42 AMP
V34353
N-Nitrosodiphenylamine
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42 AMP
V34353
N-Nitroso-di-n-propylamine
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42 AMP
V34353
Pentachlorophenol
<1.39
mg/Kg - dry
1.39
1
06/14/23 22:42 AMP
V34353
Phenanthrene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42 AMP
V34353
Phenol
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42 AMP
V34353
Pyrene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42 AMP
V34353
Pyridine
<0.459
mg/Kg - dry
0.459
1
06/14/23 22:42 AMP
V34353
1,2,4-Trichlorobenzene
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42 AMP
V34353
2,4,5-Trichlorophenol
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42 AMP
V34353
2,4,6-Trichlorophenol
<0.919
mg/Kg - dry
0.919
1
06/14/23 22:42 AMP
V34353
Surrogate: Phenol-d5
55.6
Limits: 34-121%
1 06/14/23 22:42 AMP
8270E
Surrogate: 2-Fluorobiphenyl
70.5
Limits: 44-115%
1 06/14/23 22:42 AMP
V34353
Surrogate: 2-Fluorophenol
60.7
Limits: 35-115%
1 06/14/23 22:42 AMP
V34353
Surrogate: Nitrobenzene-d5
66.9
Limits: 37-122%
1 06/14/23 22:42 AMP
V34353
Surrogate: 4-Terphenyl-d14
75.9
Limits: 54-127%
1 06/14/23 22:42 AMP
V34353
Surrogate: 2,4,6-Tribromophenol
54.7
Limits: 39-132%
1 06/14/23 22:42 AMP
V34353
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 187 of 229

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 06/21/2023
Received : 06/09/2023
Report Number : 23-163-0001 REPOR T OF A NA L YSIS
Lab No : 98078 Matrix: Solids
Sample ID: UST-1-K Sampled: 6/9/2023 14:35
Analytical Method: MADEP-EPH
Prep Method: MAEPH (Prep)
Test
Aliphatic C9-C18
Aliphatic C19-C36
Aromatic C11-C22
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Analytical Method: MADEP-VPH
Prep Method: MAVPH (Prep)
Test
Prep Batch(es): V34271 06/13/23 10:20
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
<69.5 mg/Kg - dry
69.5 1
06/17/23 05:08 AMP
V34449
<69.5 mg/Kg - dry
69.5 1
06/17/23 05:08 AMP
V34449
<69.5 mg/Kg - dry
69.5 1
06/17/23 05:08 AMP
V34449
125
Limits: 40-140%
1 06/17/23 05:08 AMP
MADEP-EPH
76.8
Limits: 40-140%
1 06/17/23 05:08 AMP
MADEP-EPH
117
Limits: 40-140%
1 06/17/23 05:08 AMP
MADEP-EPH
122
Limits: 40-140%
1 06/17/23 05:08 AMP
V34449
Prep Batch(es):
V34232 06/12/23 08:00
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Aliphatic C5-C8
Aliphatic C9-C12
Aromatic C9-C10
Surrogate: 2,5-Dibromotoluene (FID)
Surrogate: 2,5-Dibromotoluene (PID)
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
mg/Kg - dry
11.1
100 06/12/23 21:07 TBL
V34233
mg/Kg - dry
11.1
100 06/12/23 21:07 TBL
V34233
mg/Kg - dry
11.1
100 06/12/23 21:07 TBL
V34233
99.1
Limits: 70-130%
100 06/12/23 21:07 TBL
MADEP-VPH
98.1
Limits: 70-130%
100 06/12/23 21:07 TBL
MADEP-VPH
DF Dilution Factor
Page 188 of 229

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
QC Prep: V34381 QC Analytical Batch(es): V34416
QC Prep Batch Method: 3546 Analysis Method: 8015C DRO
Analysis Description: Total Petroleum Hydrocarbons - Extractable
Lab Reagent Blank LRB-V34381 Matrix: SOL
Associated Lab Samples: 98043, 98044, 98045, 98046, 98047, 98048, 98051, 98052, 98053, 98054, 98055, 98056, 98057, 98058, 98059
Blank MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Diesel Range Organics (00-C28) mg/Kg <10.0 10.0 06/15/23 16:44
OTP Surrogate (S) 06/15/23 16:44 78.1 31-123
Laboratory Control Sample LCS-V34381
Spike LCS LCS %Rec % Rec
Parameter Units Conc. Result Limits
Diesel Range Organics (00-C28) mg/Kg
66.7 70.4
106
46-126
OTP Surrogate (S)
84.9
31-123
Matrix Spike & Matrix Spike Duplicate
V 98317-MS-V34381 V 98317-MSD-V34381
MS Spike MSD MS Result
MSD
MS MSD %Rec Max
Parameter Units
Result Conc. Spike
Result
%Rec %Rec Limits RPD RPD
Conc.
Diesel Range Organics (C10-C28) mg/Kg 7800 66.7 66.6 2080
OTP Surrogate (S)
1790 0.0* 0.0* 50-117 3.9 24
105 82.7 31-123
* QC Fail Date: 06/21/2023 02:47 PM Page 1 of 36
Page 189 of 229

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
QC Prep: V34382 QC Analytical Batch(es): V34417
QC Prep Batch Method: 3546 Analysis Method: 8015C DRO
Analysis Description: Total Petroleum Hydrocarbons - Extractable
Lab Reagent Blank LRB-V34382 Matrix: SOL
Associated Lab Samples: 98060, 98061, 98062, 98063, 98068, 98069
Blank MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Diesel Range Organics (00-C28) mg/Kg <10.0 10.0 06/15/23 16:44
OTP Surrogate (S) 06/15/23 16:44 78.1 31-123
Laboratory Control Sample & LCSD LCS-V34382 LCSD-V34382
Spike LCS LCSD LCS LCSD % Rec
Parameter Units Conc. Result Result %Rec a/o Rec Limits RPD Max
RPD
Diesel Range Organics (C10-C28) mg/Kg 66.7 70.4 62.0 106
OTP Surrogate (S) 84.9
92.9 46-126 12.6 20
71.4 31-123
Date: 06/21/2023 02:47 PM
Page 190 of 229
Page 2 of 36

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
QC Prep: V34234 QC Analytical Batch(es): V34235
QC Prep Batch Method: 5035 MED Analysis Method: 8015C GRO
Analysis Description: Total Petroleum Hydrocarbons - Volatile
Lab Reagent Blank LRB-V34234 Matrix: SOL
Associated Lab Samples: 98043, 98044, 98045, 98046, 98047, 98048, 98051, 98052, 98053, 98054, 98055, 98056, 98057, 98058, 98059,
98060, 98061, 98062, 98063, 98068
Blank MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Gasoline Range Organics (C6-C10) mg/Kg <5.00 5.00 06/12/23 14:15
a,a,a-Trifluorotoluene (S) 06/12/23 14:15 109 50-137
Laboratory Control Sample LCS-V34234
Spike LCS LCS %Rec % Rec
Parameter Units Conc. Result Limits
Gasoline Range Organics (C6-00) mg/Kg
50.0 62.0
124
41-138
a,a,a-Trifluorotoluene (S)
118
50-137
Matrix Spike & Matrix Spike Duplicate
V 98043-MS-V34234 V 98043-MSD-V34234
MS Spike MSD MS Result
MSD
MS MSD %Rec Max
Parameter Units
Result Conc. Spike
Result
%Rec %Rec Limits RPD RPD
Conc.
Gasoline Range Organics (C6-C10) mg/Kg <5.00 50.0 50.0 55.8 56.6 112
a,a,a-Trifluorotoluene (S) 114
113 41-138 1.4 34
122 50-137
Date: 06/21/2023 02:47 PM
Page 191 of 229
Page 3 of 36

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
QC Prep: V34275
QC Analytical Batch(es): V34276
QC Prep Batch Method: 5035 MED
Analysis Method:
8015C GRO
Analysis Description:
Total Petroleum Hydrocarbons - Volatile
Lab Reagent Blank
LRB-V34275
Matrix: SOL
Associated Lab Samples: 98069
Blank
MQL
Analyzed % % Rec
Parameter Units
Result
Recovery Limits
Gasoline Range Organics (C6-C10) mg/Kg
<5.00
5.00
06/13/23 11:35
a,a,a-Trifluorotoluene (S)
06/13/23 11:35 116 50-137
Laboratory Control Sample LCS-V34275
Spike LCS LCS %Rec % Rec
Parameter Units Conc. Result Limits
Gasoline Range Organics (C6-00) mg/Kg
50.0 60.2
120
41-138
a,a,a-Trifluorotoluene (S)
129
50-137
Matrix Spike & Matrix Spike Duplicate
V 98069-MS-V34275 V 98069-MSD-V34275
MS Spike MSD MS Result
MSD
MS MSD %Rec Max
Parameter Units
Result Conc. Spike
Result
%Rec %Rec Limits RPD RPD
Conc.
Gasoline Range Organics (C6-C10) mg/Kg <5.00 50.0 50.0 62.5
a,a,a-Trifluorotoluene (S)
57.9 125 116 41-138 7.6 34
128 133 50-137
Date: 06/21/2023 02:47 PM
Page 192 of 229
Page 4 of 36

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
QC Prep: V34277
QC Prep Batch Method: 5035
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Analytical Batch(es): V34278
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V34277 Matrix: SOL
Associated Lab Samples: 98049, 98064, 98065, 98066, 98067, 98070, 98071, 98072, 98073, 98075, 98076, 98078
Blank MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Acetone
mg/Kg
<0.020
0.020
06/12/23 11:02
Acrolein
mg/Kg
<0.020
0.020
06/12/23 11:02
Acrylonitrile
mg/Kg
<0.020
0.020
06/12/23 11:02
Benzene
mg/Kg
<0.005
0.005
06/12/23 11:02
Bromobenzene
mg/Kg
<0.005
0.005
06/12/23 11:02
Bromochloromethane
mg/Kg
<0.005
0.005
06/12/23 11:02
Bromodichloromethane
mg/Kg
<0.005
0.005
06/12/23 11:02
Bromoform
mg/Kg
<0.005
0.005
06/12/23 11:02
Bromomethane
mg/Kg
<0.010
0.010
06/12/23 11:02
n-Butylbenzene
mg/Kg
<0.005
0.005
06/12/23 11:02
sec -Butyl benzene
mg/Kg
<0.005
0.005
06/12/23 11:02
tert-Butyl benzene
mg/Kg
<0.005
0.005
06/12/23 11:02
Carbon Disulfide
mg/Kg
<0.005
0.005
06/12/23 11:02
Carbon Tetrachloride
mg/Kg
<0.005
0.005
06/12/23 11:02
Chlorobenzene
mg/Kg
<0.005
0.005
06/12/23 11:02
Chlorodibromomethane
mg/Kg
<0.005
0.005
06/12/23 11:02
Chloroethane
mg/Kg
<0.010
0.010
06/12/23 11:02
Chloroform
mg/Kg
<0.005
0.005
06/12/23 11:02
Chloromethane
mg/Kg
<0.010
0.010
06/12/23 11:02
2-Chlorotoluene
mg/Kg
<0.005
0.005
06/12/23 11:02
4-Chlorotoluene
mg/Kg
<0.005
0.005
06/12/23 11:02
Di -Isopropyl Ether (DIPE)
mg/Kg
<0.005
0.005
06/12/23 11:02
1,2-Dibromo-3-Chloropropane
mg/Kg
<0.010
0.010
06/12/23 11:02
1,2-Dibromoethane
mg/Kg
<0.005
0.005
06/12/23 11:02
Dibromomethane
mg/Kg
<0.005
0.005
06/12/23 11:02
1,2-Dichlorobenzene
mg/Kg
<0.005
0.005
06/12/23 11:02
1,3-Dichlorobenzene
mg/Kg
<0.005
0.005
06/12/23 11:02
Date: 06/21/2023 02:47 PM
Page 5 of 36
Page 193 of 229

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
QC Prep: V34277
QC Prep Batch Method: 5035
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Analytical Batch(es): V34278
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V34277 Matrix: SOL
Associated Lab Samples: 98049, 98064, 98065, 98066, 98067, 98070, 98071, 98072, 98073, 98075, 98076, 98078
Blank MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
1,4-Dichlorobenzene
mg/Kg
<0.005
0.005
06/12/23 11:02
Dichlorodifluoromethane
mg/Kg
<0.010
0.010
06/12/23 11:02
1,1-Dichloroethane
mg/Kg
<0.005
0.005
06/12/23 11:02
1,2-Dichloroethane
mg/Kg
<0.005
0.005
06/12/23 11:02
1,1-Dichloroethene
mg/Kg
<0.005
0.005
06/12/23 11:02
cis-1,2-Dichloroethene
mg/Kg
<0.005
0.005
06/12/23 11:02
trans-1,2-Dichloroethene
mg/Kg
<0.005
0.005
06/12/23 11:02
1,2-Dichloropropane
mg/Kg
<0.005
0.005
06/12/23 11:02
1,3-Dichloropropane
mg/Kg
<0.005
0.005
06/12/23 11:02
2,2-Dichloropropane
mg/Kg
<0.005
0.005
06/12/23 11:02
1,1-Dichloropropene
mg/Kg
<0.005
0.005
06/12/23 11:02
cis-1,3-Dichloropropene
mg/Kg
<0.005
0.005
06/12/23 11:02
trans-1,3-Dichloropropene
mg/Kg
<0.005
0.005
06/12/23 11:02
Ethanol
mg/Kg
<0.250
0.250
06/12/23 11:02
Ethylbenzene
mg/Kg
<0.005
0.005
06/12/23 11:02
Ethyl Tertiary Butyl Ether (ETBE)
mg/Kg
<0.050
0.050
06/12/23 11:02
Hexachlorobutadiene
mg/Kg
<0.010
0.010
06/12/23 11:02
n-Hexane
mg/Kg
<0.010
0.010
06/12/23 11:02
2-Hexanone
mg/Kg
<0.020
0.020
06/12/23 11:02
Isopropyl benzene
mg/Kg
<0.005
0.005
06/12/23 11:02
4-Isopropyl toluene
mg/Kg
<0.005
0.005
06/12/23 11:02
Methyl Ethyl Ketone (MEK)
mg/Kg
<0.020
0.020
06/12/23 11:02
Methyl tert-butyl ether (MTBE)
mg/Kg
<0.005
0.005
06/12/23 11:02
4-Methyl-2-Pentanone
mg/Kg
<0.020
0.020
06/12/23 11:02
Methylene Chloride
mg/Kg
<0.010
0.010
06/12/23 11:02
Naphthalene
mg/Kg
<0.010
0.010
06/12/23 11:02
n-Propylbenzene
mg/Kg
<0.005
0.005
06/12/23 11:02
Date: 06/21/2023 02:47 PM
Page 6 of 36
Page 194 of 229

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
QC Prep: V34277
QC Prep Batch Method: 5035
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Analytical Batch(es): V34278
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank
LRB-V34277
Matrix: SOL
Associated Lab Samples:
98049, 98064, 98065, 98066, 98067,
98070, 98071, 98072, 98073, 98075, 98076, 98078
Blank
MQL
Analyzed % % Rec
Parameter
Units
Result
Recovery Limits
Styrene
mg/Kg
<0.005
0.005
06/12/23 11:02
1,1,1,2-Tetrachloroethane
mg/Kg
<0.005
0.005
06/12/23 11:02
1,1,2,2-Tetrachloroethane
mg/Kg
<0.005
0.005
06/12/23 11:02
Tetrachloroethene
mg/Kg
<0.005
0.005
06/12/23 11:02
Toluene
mg/Kg
<0.005
0.005
06/12/23 11:02
1,2,3-Trichlorobenzene
mg/Kg
<0.010
0.010
06/12/23 11:02
1,2,4-Trichlorobenzene
mg/Kg
<0.010
0.010
06/12/23 11:02
1,1,1-Trichloroethane
mg/Kg
<0.005
0.005
06/12/23 11:02
1,1,2-Trichloroethane
mg/Kg
<0.005
0.005
06/12/23 11:02
Trichloroethene
mg/Kg
<0.005
0.005
06/12/23 11:02
Trichlorofluoromethane
mg/Kg
<0.010
0.010
06/12/23 11:02
1,2,3-Trichloropropane
mg/Kg
<0.005
0.005
06/12/23 11:02
1,2,4-Trimethyl benzene
mg/Kg
<0.005
0.005
06/12/23 11:02
1,3,5-Trimethyl benzene
mg/Kg
<0.005
0.005
06/12/23 11:02
Vinyl Acetate
mg/Kg
<0.010
0.010
06/12/23 11:02
Vinyl Chloride
mg/Kg
<0.010
0.010
06/12/23 11:02
o-Xylene
mg/Kg
<0.005
0.005
06/12/23 11:02
m,p-Xylene
mg/Kg
<0.010
0.010
06/12/23 11:02
4-Bromofluorobenzene (S)
06/12/23 11:02
111
70-130
Dibromofluoromethane (S)
06/12/23 11:02
103
84-123
Toluene-d8 (S)
06/12/23 11:02
98.4
76-129
Laboratory Control Sample & LCSD
LCS-V34277
LCSD-V34277
Spike
LCS
LCSD LCS LCSD
% Rec
Parameter Units
Conc.
Result
Result %Rec a/o Rec
Limits
RPD Max
RPD
Acetone mg/Kg
0.100
0.109
0.120 109 120
29-198
9.6 20
Date: 06/21/2023 02:47 PM Page 7 of 36
Page 195 of 229

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V34277 QC Analytical Batch(es): V34278
QC Prep Batch Method: 5035 Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V34277 LCSD-V34277
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
Acrolein
mg/Kg
0.100
0.126
0.128
126
128
70-130
1.5
20
Acrylonitrile
mg/Kg
0.100
0.118
0.127
118
127
65-134
7.3
20
Benzene
mg/Kg
0.050
0.051
0.050
102
100
74-127
2.3
20
Bromobenzene
mg/Kg
0.050
0.046
0.048
93.8
97.2
73-125
3.5
20
Bromochloromethane
mg/Kg
0.050
0.052
0.052
105
105
72-134
0.0
20
Bromodichloromethane
mg/Kg
0.050
0.051
0.051
102
103
75-122
0.5
20
Bromoform
mg/Kg
0.050
0.050
0.057
102
116
66-135
12.8
20
Bromomethane
mg/Kg
0.050
0.042
0.048
84.8
96.4
20-180
12.8
20
n-Butylbenzene
mg/Kg
0.050
0.053
0.049
106
99.8
65-135
6.2
20
sec -Butyl benzene
mg/Kg
0.050
0.051
0.047
102
95.8
66-131
6.2
20
tert-Butyl benzene
mg/Kg
0.050
0.051
0.047
102
95.8
67-132
6.2
20
Carbon Disulfide
mg/Kg
0.050
0.050
0.050
100
101
61-129
0.7
20
Carbon Tetrachloride
mg/Kg
0.050
0.051
0.049
102
98.4
64-143
3.9
20
Chlorobenzene
mg/Kg
0.050
0.050
0.049
102
98.4
74-118
3.2
20
Chlorodibromomethane
mg/Kg
0.050
0.052
0.053
105
107
73-122
1.6
20
Chloroethane
mg/Kg
0.050
0.045
0.045
91.0
91.6
33-149
0.6
20
Chloroform
mg/Kg
0.050
0.051
0.050
103
101
73-127
2.1
20
Chloromethane
mg/Kg
0.050
0.041
0.040
82.0
81.4
45-143
0.7
20
2-Chlorotoluene
mg/Kg
0.050
0.047
0.047
94.6
95.8
67-124
1.2
20
4-Chlorotoluene
mg/Kg
0.050
0.047
0.047
94.6
95.8
71-126
1.2
20
Di -Isopropyl Ether (DIPE)
mg/Kg
0.050
0.049
0.049
98.6
98.2
59-159
0.4
20
1,2-Dibromo-3-Chloropropane
mg/Kg
0.050
0.057
0.058
115
117
55-157
1.8
20
1,2-Dibromoethane
mg/Kg
0.050
0.052
0.053
104
108
70-132
3.5
20
Dibromomethane
mg/Kg
0.050
0.053
0.054
107
109
74-133
1.6
20
1,2-Dichlorobenzene
mg/Kg
0.050
0.051
0.050
103
100
72-123
2.5
20
1,3-Dichlorobenzene
mg/Kg
0.050
0.051
0.049
103
99.4
71-120
3.5
20
Date: 06/21/2023 02:47 PM Page 8 of 36
Page 196 of 229

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V34277 QC Analytical Batch(es): V34278
QC Prep Batch Method: 5035 Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V34277 LCSD-V34277
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
1,4-Dichlorobenzene
mg/Kg
0.050
0.051
0.049
103
98.6
71-123
3.9
20
Dichlorodifluoromethane
mg/Kg
0.050
0.044
0.042
89.8
84.4
26-146
6.1
20
1,1-Dichloroethane
mg/Kg
0.050
0.050
0.049
101
98.8
74-127
2.5
20
1,2-Dichloroethane
mg/Kg
0.050
0.050
0.050
101
101
68-128
0.0
20
1,1-Dichloroethene
mg/Kg
0.050
0.048
0.048
96.4
97.4
67-149
1.0
20
cis-1,2-Dichloroethene
mg/Kg
0.050
0.051
0.050
103
101
76-134
1.7
20
trans-1,2-Dichloroethene
mg/Kg
0.050
0.052
0.049
104
98.8
73-132
5.5
20
1,2-Dichloropropane
mg/Kg
0.050
0.050
0.050
101
102
73-130
0.7
20
1,3-Dichloropropane
mg/Kg
0.050
0.051
0.050
103
101
75-124
1.9
20
2,2-Dichloropropane
mg/Kg
0.050
0.051
0.049
103
98.0
50-142
4.7
20
1,1-Dichloropropene
mg/Kg
0.050
0.051
0.048
104
97.2
71-130
6.5
20
cis-1,3-Dichloropropene
mg/Kg
0.050
0.052
0.052
106
105
71-125
0.9
20
trans-1,3-Dichloropropene
mg/Kg
0.050
0.054
0.054
110
110
68-123
0.1
20
Ethanol
mg/Kg
1.25
1.35
1.59
108
127
70-130
16.3
20
Ethylbenzene
mg/Kg
0.050
0.049
0.048
99.6
96.4
74-128
3.2
20
Ethyl Tertiary Butyl Ether (ETBE)
mg/Kg
0.100
0.099
0.102
99.6
102
70-130
2.3
20
Hexachlorobutadiene
mg/Kg
0.050
0.053
0.051
108
103
64-125
4.9
20
n-Hexane
mg/Kg
0.050
0.053
0.050
106
102
70-130
4.2
20
2-Hexanone
mg/Kg
0.050
0.062
0.065
124
130
61-157
4.4
20
Isopropyl benzene
mg/Kg
0.050
0.048
0.047
96.8
95.4
68-126
1.4
20
4-Isopropyl toluene
mg/Kg
0.050
0.052
0.049
105
98.0
68-129
7.0
20
Methyl Ethyl Ketone (MEK)
mg/Kg
0.050
0.052
0.057
106
114
63-149
8.0
20
Methyl tert-butyl ether (MTBE)
mg/Kg
0.050
0.050
0.052
101
104
70-130
2.7
20
4-Methyl-2-Pentanone
mg/Kg
0.050
0.055
0.059
112
119
57-162
6.0
20
Methylene Chloride
mg/Kg
0.050
0.047
0.046
94.0
92.0
74-129
2.1
20
Naphthalene
mg/Kg
0.050
0.050
0.051
101
102
57-157
0.7
20
Date: 06/21/2023 02:47 PM Page 9 of 36
Page 197 of 229

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
Hart & Hickman (Charlotte)
TPM-001
23-163-0001
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V34277 QC Analytical Batch(es): V34278
QC Prep Batch Method: 5035 Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V34277 LCSD-V34277
Spike LCS LCSD LCS LCSD % Rec
Parameter Units Conc. Result Result %Rec % Rec Limits RPD Max
RPD
n-Propylbenzene
mg/Kg
0.050
0.048
0.048
96.2
97.4
67-130
Styrene
mg/Kg
0.050
0.050
0.053
102
108
77-121
1,1,1,2-Tetrachloroethane
mg/Kg
0.050
0.050
0.051
101
104
72-115
1,1,2,2-Tetrachloroethane
mg/Kg
0.050
0.047
0.051
95.6
102
56-126
Tetrachloroethene
mg/Kg
0.050
0.051
0.049
102
98.6
68-130
Toluene
mg/Kg
0.050
0.051
0.049
103
99.8
71-129
1,2,3-Trichlorobenzene
mg/Kg
0.050
0.051
0.050
102
102
68-130
1,2,4-Trichlorobenzene
mg/Kg
0.050
0.053
0.053
106
106
66-125
1,1,1-Trichloroethane
mg/Kg
0.050
0.051
0.048
103
97.2
67-131
1,1,2-Trichloroethane
mg/Kg
0.050
0.051
0.051
104
104
70-133
Trichloroethene
mg/Kg
0.050
0.051
0.049
103
98.4
75-133
Trichlorofluoromethane
mg/Kg
0.050
0.043
0.044
87.6
88.0
44-146
1,2,3-Trichloropropane
mg/Kg
0.050
0.049
0.053
98.6
107
60-137
1,2,4-Trimethyl benzene
mg/Kg
0.050
0.051
0.049
104
98.6
69-129
1,3,5-Trimethylbenzene
mg/Kg
0.050
0.048
0.049
97.4
98.0
69-128
Vinyl Acetate
mg/Kg
0.050
0.060
0.061
122
123
60-140
Vinyl Chloride
mg/Kg
0.050
0.048
0.046
96.0
92.2
48-147
o-Xylene
mg/Kg
0.050
0.047
0.049
95.2
99.2
74-126
m,p-Xylene
mg/Kg
0.100
0.098
0.094
98.9
94.4
75-124
4-Bromofluorobenzene (S)
96.8
101
70-130
Dibromofluoromethane (S)
103
103
84-123
Toluene-d8(S)
101
111
76-129
1.2
5.5
2.9
6.8
3.5
2.9
0.3
0.3
5.4
0.1
4.7
0.4
8.3
4.9
0.6
0.8
4.0
4.1
4.6
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Date: 06/21/2023 02:47 PM Page 10 of 36
Page 198 of 229

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
QC Prep: V34281
QC Prep Batch Method: 5035
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Analytical Batch(es): V34282
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V34281 Matrix: SOL
Associated Lab Samples: 98050
Blank MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Acetone
mg/Kg
<0.020
0.020
06/12/23 11:02
Acrolein
mg/Kg
<0.020
0.020
06/12/23 11:02
Acrylonitrile
mg/Kg
<0.020
0.020
06/12/23 11:02
Benzene
mg/Kg
<0.005
0.005
06/12/23 11:02
Bromobenzene
mg/Kg
<0.005
0.005
06/12/23 11:02
Bromochloromethane
mg/Kg
<0.005
0.005
06/12/23 11:02
Bromodichloromethane
mg/Kg
<0.005
0.005
06/12/23 11:02
Bromoform
mg/Kg
<0.005
0.005
06/12/23 11:02
Bromomethane
mg/Kg
<0.010
0.010
06/12/23 11:02
n-Butylbenzene
mg/Kg
<0.005
0.005
06/12/23 11:02
sec -Butyl benzene
mg/Kg
<0.005
0.005
06/12/23 11:02
tert-Butyl benzene
mg/Kg
<0.005
0.005
06/12/23 11:02
Carbon Disulfide
mg/Kg
<0.005
0.005
06/12/23 11:02
Carbon Tetrachloride
mg/Kg
<0.005
0.005
06/12/23 11:02
Chlorobenzene
mg/Kg
<0.005
0.005
06/12/23 11:02
Chlorodibromomethane
mg/Kg
<0.005
0.005
06/12/23 11:02
Chloroethane
mg/Kg
<0.010
0.010
06/12/23 11:02
Chloroform
mg/Kg
<0.005
0.005
06/12/23 11:02
Chloromethane
mg/Kg
<0.010
0.010
06/12/23 11:02
2-Chlorotoluene
mg/Kg
<0.005
0.005
06/12/23 11:02
4-Chlorotoluene
mg/Kg
<0.005
0.005
06/12/23 11:02
Di -Isopropyl Ether (DIPE)
mg/Kg
<0.005
0.005
06/12/23 11:02
1,2-Dibromo-3-Chloropropane
mg/Kg
<0.010
0.010
06/12/23 11:02
1,2-Dibromoethane
mg/Kg
<0.005
0.005
06/12/23 11:02
Dibromomethane
mg/Kg
<0.005
0.005
06/12/23 11:02
1,2-Dichlorobenzene
mg/Kg
<0.005
0.005
06/12/23 11:02
1,3-Dichlorobenzene
mg/Kg
<0.005
0.005
06/12/23 11:02
Date: 06/21/2023 02:47 PM
Page 11 of 36
Page 199 of 229

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
QC Prep: V34281
QC Prep Batch Method: 5035
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Analytical Batch(es): V34282
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V34281 Matrix: SOL
Associated Lab Samples: 98050
Blank MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
1,4-Dichlorobenzene
mg/Kg
<0.005
0.005
06/12/23 11:02
Dichlorodifluoromethane
mg/Kg
<0.010
0.010
06/12/23 11:02
1,1-Dichloroethane
mg/Kg
<0.005
0.005
06/12/23 11:02
1,2-Dichloroethane
mg/Kg
<0.005
0.005
06/12/23 11:02
1,1-Dichloroethene
mg/Kg
<0.005
0.005
06/12/23 11:02
cis-1,2-Dichloroethene
mg/Kg
<0.005
0.005
06/12/23 11:02
trans-1,2-Dichloroethene
mg/Kg
<0.005
0.005
06/12/23 11:02
1,2-Dichloropropane
mg/Kg
<0.005
0.005
06/12/23 11:02
1,3-Dichloropropane
mg/Kg
<0.005
0.005
06/12/23 11:02
2,2-Dichloropropane
mg/Kg
<0.005
0.005
06/12/23 11:02
1,1-Dichloropropene
mg/Kg
<0.005
0.005
06/12/23 11:02
cis-1,3-Dichloropropene
mg/Kg
<0.005
0.005
06/12/23 11:02
trans-1,3-Dichloropropene
mg/Kg
<0.005
0.005
06/12/23 11:02
Ethanol
mg/Kg
<0.250
0.250
06/12/23 11:02
Ethylbenzene
mg/Kg
<0.005
0.005
06/12/23 11:02
Ethyl Tertiary Butyl Ether (ETBE)
mg/Kg
<0.050
0.050
06/12/23 11:02
Hexachlorobutadiene
mg/Kg
<0.010
0.010
06/12/23 11:02
n-Hexane
mg/Kg
<0.010
0.010
06/12/23 11:02
2-Hexanone
mg/Kg
<0.020
0.020
06/12/23 11:02
Isopropyl benzene
mg/Kg
<0.005
0.005
06/12/23 11:02
4-Isopropyl toluene
mg/Kg
<0.005
0.005
06/12/23 11:02
Methyl Ethyl Ketone (MEK)
mg/Kg
<0.020
0.020
06/12/23 11:02
Methyl tert-butyl ether (MTBE)
mg/Kg
<0.005
0.005
06/12/23 11:02
4-Methyl-2-Pentanone
mg/Kg
<0.020
0.020
06/12/23 11:02
Methylene Chloride
mg/Kg
<0.010
0.010
06/12/23 11:02
Naphthalene
mg/Kg
<0.010
0.010
06/12/23 11:02
n-Propylbenzene
mg/Kg
<0.005
0.005
06/12/23 11:02
Date: 06/21/2023 02:47 PM
Page 12 of 36
Page 200 of 229

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Hart & Hickman (Charlotte)
Project Description:
TPM-001
Report No:
23-163-0001
QC Prep:
V34281
QC Analytical Batch(es): V34282
QC Prep Batch Method:
5035
Analysis Method:
8260D
Analysis Description:
Volatile Organic Compounds - GC/MS
Lab Reagent Blank
LRB-V34281
Matrix: SOL
Associated Lab Samples:
98050
Blank
MQL
Analyzed
% % Rec
Parameter
Units
Result
Recovery Limits
Styrene
mg/Kg
<0.005
0.005
06/12/23 11:02
1,1,1,2-Tetrachloroethane
mg/Kg
<0.005
0.005
06/12/23 11:02
1,1,2,2-Tetrachloroethane
mg/Kg
<0.005
0.005
06/12/23 11:02
Tetrachloroethene
mg/Kg
<0.005
0.005
06/12/23 11:02
Toluene
mg/Kg
<0.005
0.005
06/12/23 11:02
1,2,3-Trichlorobenzene
mg/Kg
<0.010
0.010
06/12/23 11:02
1,2,4-Trichlorobenzene
mg/Kg
<0.010
0.010
06/12/23 11:02
1,1,1-Trichloroethane
mg/Kg
<0.005
0.005
06/12/23 11:02
1,1,2-Trichloroethane
mg/Kg
<0.005
0.005
06/12/23 11:02
Trichloroethene
mg/Kg
<0.005
0.005
06/12/23 11:02
Trichlorofluoromethane
mg/Kg
<0.010
0.010
06/12/23 11:02
1,2,3-Trichloropropane
mg/Kg
<0.005
0.005
06/12/23 11:02
1,2,4-Trimethyl benzene
mg/Kg
<0.005
0.005
06/12/23 11:02
1,3,5-Trimethyl benzene
mg/Kg
<0.005
0.005
06/12/23 11:02
Vinyl Acetate
mg/Kg
<0.010
0.010
06/12/23 11:02
Vinyl Chloride
mg/Kg
<0.010
0.010
06/12/23 11:02
o-Xylene
mg/Kg
<0.005
0.005
06/12/23 11:02
m,p-Xylene
mg/Kg
<0.010
0.010
06/12/23 11:02
4-Bromofluorobenzene (S)
06/12/23 11:02
111 70-130
Dibromofluoromethane (S)
06/12/23 11:02
103 84-123
Toluene-d8 (S)
06/12/23 11:02
98.4 76-129
Laboratory Control Sample & LCSD
LCS-V34281
LCSD-V34281
Spike
LCS LCSD
LCS LCSD
% Rec
Parameter
Units
Conc.
Result Result
%Rec a/o Rec
Limits RPD Max
RPD
Acetone
mg/Kg
0.100
0.109 0.120
109 120
29-198 9.6 20
Date: 06/21/2023 02:47 PM
Page 13 of 36
Page 201 of 229

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V34281 QC Analytical Batch(es): V34282
QC Prep Batch Method: 5035 Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V34281 LCSD-V34281
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
Acrolein
mg/Kg
0.100
0.126
0.128
126
128
70-130
1.5
20
Acrylonitrile
mg/Kg
0.100
0.118
0.127
118
127
65-134
7.3
20
Benzene
mg/Kg
0.050
0.051
0.050
102
100
74-127
2.3
20
Bromobenzene
mg/Kg
0.050
0.046
0.048
93.8
97.2
73-125
3.5
20
Bromochloromethane
mg/Kg
0.050
0.052
0.052
105
105
72-134
0.0
20
Bromodichloromethane
mg/Kg
0.050
0.051
0.051
102
103
75-122
0.5
20
Bromoform
mg/Kg
0.050
0.050
0.057
102
116
66-135
12.8
20
Bromomethane
mg/Kg
0.050
0.042
0.048
84.8
96.4
20-180
12.8
20
n-Butylbenzene
mg/Kg
0.050
0.053
0.049
106
99.8
65-135
6.2
20
sec -Butyl benzene
mg/Kg
0.050
0.051
0.047
102
95.8
66-131
6.2
20
tert-Butyl benzene
mg/Kg
0.050
0.051
0.047
102
95.8
67-132
6.2
20
Carbon Disulfide
mg/Kg
0.050
0.050
0.050
100
101
61-129
0.7
20
Carbon Tetrachloride
mg/Kg
0.050
0.051
0.049
102
98.4
64-143
3.9
20
Chlorobenzene
mg/Kg
0.050
0.050
0.049
102
98.4
74-118
3.2
20
Chlorodibromomethane
mg/Kg
0.050
0.052
0.053
105
107
73-122
1.6
20
Chloroethane
mg/Kg
0.050
0.045
0.045
91.0
91.6
33-149
0.6
20
Chloroform
mg/Kg
0.050
0.051
0.050
103
101
73-127
2.1
20
Chloromethane
mg/Kg
0.050
0.041
0.040
82.0
81.4
45-143
0.7
20
2-Chlorotoluene
mg/Kg
0.050
0.047
0.047
94.6
95.8
67-124
1.2
20
4-Chlorotoluene
mg/Kg
0.050
0.047
0.047
94.6
95.8
71-126
1.2
20
Di -Isopropyl Ether (DIPE)
mg/Kg
0.050
0.049
0.049
98.6
98.2
59-159
0.4
20
1,2-Dibromo-3-Chloropropane
mg/Kg
0.050
0.057
0.058
115
117
55-157
1.8
20
1,2-Dibromoethane
mg/Kg
0.050
0.052
0.053
104
108
70-132
3.5
20
Dibromomethane
mg/Kg
0.050
0.053
0.054
107
109
74-133
1.6
20
1,2-Dichlorobenzene
mg/Kg
0.050
0.051
0.050
103
100
72-123
2.5
20
1,3-Dichlorobenzene
mg/Kg
0.050
0.051
0.049
103
99.4
71-120
3.5
20
Date: 06/21/2023 02:47 PM Page 14 of 36
Page 202 of 229

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V34281 QC Analytical Batch(es): V34282
QC Prep Batch Method: 5035 Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V34281 LCSD-V34281
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
1,4-Dichlorobenzene
mg/Kg
0.050
0.051
0.049
103
98.6
71-123
3.9
20
Dichlorodifluoromethane
mg/Kg
0.050
0.044
0.042
89.8
84.4
26-146
6.1
20
1,1-Dichloroethane
mg/Kg
0.050
0.050
0.049
101
98.8
74-127
2.5
20
1,2-Dichloroethane
mg/Kg
0.050
0.050
0.050
101
101
68-128
0.0
20
1,1-Dichloroethene
mg/Kg
0.050
0.048
0.048
96.4
97.4
67-149
1.0
20
cis-1,2-Dichloroethene
mg/Kg
0.050
0.051
0.050
103
101
76-134
1.7
20
trans-1,2-Dichloroethene
mg/Kg
0.050
0.052
0.049
104
98.8
73-132
5.5
20
1,2-Dichloropropane
mg/Kg
0.050
0.050
0.050
101
102
73-130
0.7
20
1,3-Dichloropropane
mg/Kg
0.050
0.051
0.050
103
101
75-124
1.9
20
2,2-Dichloropropane
mg/Kg
0.050
0.051
0.049
103
98.0
50-142
4.7
20
1,1-Dichloropropene
mg/Kg
0.050
0.051
0.048
104
97.2
71-130
6.5
20
cis-1,3-Dichloropropene
mg/Kg
0.050
0.052
0.052
106
105
71-125
0.9
20
trans-1,3-Dichloropropene
mg/Kg
0.050
0.054
0.054
110
110
68-123
0.1
20
Ethanol
mg/Kg
1.25
1.35
1.59
108
127
70-130
16.3
20
Ethylbenzene
mg/Kg
0.050
0.049
0.048
99.6
96.4
74-128
3.2
20
Ethyl Tertiary Butyl Ether (ETBE)
mg/Kg
0.100
0.099
0.102
99.6
102
70-130
2.3
20
Hexachlorobutadiene
mg/Kg
0.050
0.053
0.051
108
103
64-125
4.9
20
n-Hexane
mg/Kg
0.050
0.053
0.050
106
102
70-130
4.2
20
2-Hexanone
mg/Kg
0.050
0.062
0.065
124
130
61-157
4.4
20
Isopropyl benzene
mg/Kg
0.050
0.048
0.047
96.8
95.4
68-126
1.4
20
4-Isopropyl toluene
mg/Kg
0.050
0.052
0.049
105
98.0
68-129
7.0
20
Methyl Ethyl Ketone (MEK)
mg/Kg
0.050
0.052
0.057
106
114
63-149
8.0
20
Methyl tert-butyl ether (MTBE)
mg/Kg
0.050
0.050
0.052
101
104
70-130
2.7
20
4-Methyl-2-Pentanone
mg/Kg
0.050
0.055
0.059
112
119
57-162
6.0
20
Methylene Chloride
mg/Kg
0.050
0.047
0.046
94.0
92.0
74-129
2.1
20
Naphthalene
mg/Kg
0.050
0.050
0.051
101
102
57-157
0.7
20
Date: 06/21/2023 02:47 PM Page 15 of 36
Page 203 of 229

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
Hart & Hickman (Charlotte)
TPM-001
23-163-0001
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V34281 QC Analytical Batch(es): V34282
QC Prep Batch Method: 5035 Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V34281 LCSD-V34281
Spike LCS LCSD LCS LCSD % Rec
Parameter Units Conc. Result Result %Rec % Rec Limits RPD Max
RPD
n-Propylbenzene
mg/Kg
0.050
0.048
0.048
96.2
97.4
67-130
Styrene
mg/Kg
0.050
0.050
0.053
102
108
77-121
1,1,1,2-Tetrachloroethane
mg/Kg
0.050
0.050
0.051
101
104
72-115
1,1,2,2-Tetrachloroethane
mg/Kg
0.050
0.047
0.051
95.6
102
56-126
Tetrachloroethene
mg/Kg
0.050
0.051
0.049
102
98.6
68-130
Toluene
mg/Kg
0.050
0.051
0.049
103
99.8
71-129
1,2,3-Trichlorobenzene
mg/Kg
0.050
0.051
0.050
102
102
68-130
1,2,4-Trichlorobenzene
mg/Kg
0.050
0.053
0.053
106
106
66-125
1,1,1-Trichloroethane
mg/Kg
0.050
0.051
0.048
103
97.2
67-131
1,1,2-Trichloroethane
mg/Kg
0.050
0.051
0.051
104
104
70-133
Trichloroethene
mg/Kg
0.050
0.051
0.049
103
98.4
75-133
Trichlorofluoromethane
mg/Kg
0.050
0.043
0.044
87.6
88.0
44-146
1,2,3-Trichloropropane
mg/Kg
0.050
0.049
0.053
98.6
107
60-137
1,2,4-Trimethyl benzene
mg/Kg
0.050
0.051
0.049
104
98.6
69-129
1,3,5-Trimethylbenzene
mg/Kg
0.050
0.048
0.049
97.4
98.0
69-128
Vinyl Acetate
mg/Kg
0.050
0.060
0.061
122
123
60-140
Vinyl Chloride
mg/Kg
0.050
0.048
0.046
96.0
92.2
48-147
o-Xylene
mg/Kg
0.050
0.047
0.049
95.2
99.2
74-126
m,p-Xylene
mg/Kg
0.100
0.098
0.094
98.9
94.4
75-124
4-Bromofluorobenzene (S)
96.8
101
70-130
Dibromofluoromethane (S)
103
103
84-123
Toluene-d8(S)
101
111
76-129
1.2
5.5
2.9
6.8
3.5
2.9
0.3
0.3
5.4
0.1
4.7
0.4
8.3
4.9
0.6
0.8
4.0
4.1
4.6
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Date: 06/21/2023 02:47 PM Page 16 of 36
Page 204 of 229

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
QC Prep: V34299
QC Prep Batch Method: 5035
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Analytical Batch(es): V34300
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V34299 Matrix: SOL
Associated Lab Samples: 98074, 98077
Blank MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Acetone
mg/Kg
<0.020
0.020
06/13/23 12:01
Acrolein
mg/Kg
<0.020
0.020
06/13/23 12:01
Acrylonitrile
mg/Kg
<0.020
0.020
06/13/23 12:01
Benzene
mg/Kg
<0.005
0.005
06/13/23 12:01
Bromobenzene
mg/Kg
<0.005
0.005
06/13/23 12:01
Bromochloromethane
mg/Kg
<0.005
0.005
06/13/23 12:01
Bromodichloromethane
mg/Kg
<0.005
0.005
06/13/23 12:01
Bromoform
mg/Kg
<0.005
0.005
06/13/23 12:01
Bromomethane
mg/Kg
<0.010
0.010
06/13/23 12:01
n-Butylbenzene
mg/Kg
<0.005
0.005
06/13/23 12:01
sec -Butyl benzene
mg/Kg
<0.005
0.005
06/13/23 12:01
tert-Butyl benzene
mg/Kg
<0.005
0.005
06/13/23 12:01
Carbon Disulfide
mg/Kg
<0.005
0.005
06/13/23 12:01
Carbon Tetrachloride
mg/Kg
<0.005
0.005
06/13/23 12:01
Chlorobenzene
mg/Kg
<0.005
0.005
06/13/23 12:01
Chlorodibromomethane
mg/Kg
<0.005
0.005
06/13/23 12:01
Chloroethane
mg/Kg
<0.010
0.010
06/13/23 12:01
Chloroform
mg/Kg
<0.005
0.005
06/13/23 12:01
Chloromethane
mg/Kg
<0.010
0.010
06/13/23 12:01
2-Chlorotoluene
mg/Kg
<0.005
0.005
06/13/23 12:01
4-Chlorotoluene
mg/Kg
<0.005
0.005
06/13/23 12:01
Di -Isopropyl Ether (DIPE)
mg/Kg
<0.005
0.005
06/13/23 12:01
1,2-Dibromo-3-Chloropropane
mg/Kg
<0.010
0.010
06/13/23 12:01
1,2-Dibromoethane
mg/Kg
<0.005
0.005
06/13/23 12:01
Dibromomethane
mg/Kg
<0.005
0.005
06/13/23 12:01
1,2-Dichlorobenzene
mg/Kg
<0.005
0.005
06/13/23 12:01
1,3-Dichlorobenzene
mg/Kg
<0.005
0.005
06/13/23 12:01
Date: 06/21/2023 02:47 PM
Page 17 of 36
Page 205 of 229

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
QC Prep: V34299
QC Prep Batch Method: 5035
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Analytical Batch(es): V34300
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V34299 Matrix: SOL
Associated Lab Samples: 98074, 98077
Blank MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
1,4-Dichlorobenzene
mg/Kg
<0.005
0.005
06/13/23 12:01
Dichlorodifluoromethane
mg/Kg
<0.010
0.010
06/13/23 12:01
1,1-Dichloroethane
mg/Kg
<0.005
0.005
06/13/23 12:01
1,2-Dichloroethane
mg/Kg
<0.005
0.005
06/13/23 12:01
1,1-Dichloroethene
mg/Kg
<0.005
0.005
06/13/23 12:01
cis-1,2-Dichloroethene
mg/Kg
<0.005
0.005
06/13/23 12:01
trans-1,2-Dichloroethene
mg/Kg
<0.005
0.005
06/13/23 12:01
1,2-Dichloropropane
mg/Kg
<0.005
0.005
06/13/23 12:01
1,3-Dichloropropane
mg/Kg
<0.005
0.005
06/13/23 12:01
2,2-Dichloropropane
mg/Kg
<0.005
0.005
06/13/23 12:01
1,1-Dichloropropene
mg/Kg
<0.005
0.005
06/13/23 12:01
cis-1,3-Dichloropropene
mg/Kg
<0.005
0.005
06/13/23 12:01
trans-1,3-Dichloropropene
mg/Kg
<0.005
0.005
06/13/23 12:01
Ethanol
mg/Kg
<0.250
0.250
06/13/23 12:01
Ethylbenzene
mg/Kg
<0.005
0.005
06/13/23 12:01
Ethyl Tertiary Butyl Ether (ETBE)
mg/Kg
<0.050
0.050
06/13/23 12:01
Hexachlorobutadiene
mg/Kg
<0.010
0.010
06/13/23 12:01
n-Hexane
mg/Kg
<0.010
0.010
06/13/23 12:01
2-Hexanone
mg/Kg
<0.020
0.020
06/13/23 12:01
Isopropyl benzene
mg/Kg
<0.005
0.005
06/13/23 12:01
4-Isopropyl toluene
mg/Kg
<0.005
0.005
06/13/23 12:01
Methyl Ethyl Ketone (MEK)
mg/Kg
<0.020
0.020
06/13/23 12:01
Methyl tert-butyl ether (MTBE)
mg/Kg
<0.005
0.005
06/13/23 12:01
4-Methyl-2-Pentanone
mg/Kg
<0.020
0.020
06/13/23 12:01
Methylene Chloride
mg/Kg
<0.010
0.010
06/13/23 12:01
Naphthalene
mg/Kg
<0.010
0.010
06/13/23 12:01
n-Propylbenzene
mg/Kg
<0.005
0.005
06/13/23 12:01
Date: 06/21/2023 02:47 PM
Page 18 of 36
Page 206 of 229

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Hart & Hickman (Charlotte)
Project Description:
TPM-001
Report No:
23-163-0001
QC Prep:
V34299
QC Analytical Batch(es): V34300
QC Prep Batch Method:
5035
Analysis Method:
8260D
Analysis Description:
Volatile Organic Compounds - GC/MS
Lab Reagent Blank
LRB-V34299
Matrix: SOL
Associated Lab Samples:
98074, 98077
Blank
MQL
Analyzed
% % Rec
Parameter
Units
Result
Recovery Limits
Styrene
mg/Kg
<0.005
0.005
06/13/23 12:01
1,1,1,2-Tetrachloroethane
mg/Kg
<0.005
0.005
06/13/23 12:01
1,1,2,2-Tetrachloroethane
mg/Kg
<0.005
0.005
06/13/23 12:01
Tetrachloroethene
mg/Kg
<0.005
0.005
06/13/23 12:01
Toluene
mg/Kg
<0.005
0.005
06/13/23 12:01
1,2,3-Trichlorobenzene
mg/Kg
<0.010
0.010
06/13/23 12:01
1,2,4-Trichlorobenzene
mg/Kg
<0.010
0.010
06/13/23 12:01
1,1,1-Trichloroethane
mg/Kg
<0.005
0.005
06/13/23 12:01
1,1,2-Trichloroethane
mg/Kg
<0.005
0.005
06/13/23 12:01
Trichloroethene
mg/Kg
<0.005
0.005
06/13/23 12:01
Trichlorofluoromethane
mg/Kg
<0.010
0.010
06/13/23 12:01
1,2,3-Trichloropropane
mg/Kg
<0.005
0.005
06/13/23 12:01
1,2,4-Trimethyl benzene
mg/Kg
<0.005
0.005
06/13/23 12:01
1,3,5-Trimethyl benzene
mg/Kg
<0.005
0.005
06/13/23 12:01
Vinyl Acetate
mg/Kg
<0.010
0.010
06/13/23 12:01
Vinyl Chloride
mg/Kg
<0.010
0.010
06/13/23 12:01
o-Xylene
mg/Kg
<0.005
0.005
06/13/23 12:01
m,p-Xylene
mg/Kg
<0.010
0.010
06/13/23 12:01
4-Bromofluorobenzene (S)
06/13/23 12:01
103 70-130
Dibromofluoromethane (S)
06/13/23 12:01
101 84-123
Toluene-d8 (S)
06/13/23 12:01
98.4 76-129
Laboratory Control Sample & LCSD
LCS-V34299
LCSD-V34299
Spike
LCS LCSD
LCS LCSD
% Rec
Parameter
Units
Conc.
Result Result
%Rec a/o Rec
Limits RPD Max
RPD
Acetone
mg/Kg
0.100
0.104 0.105
104 105
29-198 0.9 20
Date: 06/21/2023 02:47 PM Page 19 of 36
Page 207 of 229

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V34299 QC Analytical Batch(es): V34300
QC Prep Batch Method: 5035 Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V34299 LCSD-V34299
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
Acrolein
mg/Kg
0.100
0.129
0.130
129
130
70-130
0.7
20
Acrylonitrile
mg/Kg
0.100
0.123
0.117
123
117
65-134
5.0
20
Benzene
mg/Kg
0.050
0.050
0.048
100
97.4
74-127
3.0
20
Bromobenzene
mg/Kg
0.050
0.047
0.045
95.2
91.8
73-125
3.6
20
Bromochloromethane
mg/Kg
0.050
0.051
0.049
103
98.8
72-134
4.3
20
Bromodichloromethane
mg/Kg
0.050
0.049
0.049
99.6
99.6
75-122
0.0
20
Bromoform
mg/Kg
0.050
0.053
0.050
108
101
66-135
6.5
20
Bromomethane
mg/Kg
0.050
0.044
0.038
89.2
76.6
20-180
15.1
20
n-Butylbenzene
mg/Kg
0.050
0.050
0.049
101
98.8
65-135
2.5
20
sec -Butyl benzene
mg/Kg
0.050
0.049
0.047
98.0
95.0
66-131
3.1
20
tert-Butyl benzene
mg/Kg
0.050
0.048
0.047
96.8
94.2
67-132
2.7
20
Carbon Disulfide
mg/Kg
0.050
0.052
0.047
105
95.6
61-129
9.3
20
Carbon Tetrachloride
mg/Kg
0.050
0.044
0.041
88.0
83.8
64-143
4.8
20
Chlorobenzene
mg/Kg
0.050
0.048
0.046
96.2
93.8
74-118
2.5
20
Chlorodibromomethane
mg/Kg
0.050
0.051
0.048
103
97.4
73-122
5.9
20
Chloroethane
mg/Kg
0.050
0.044
0.042
89.4
85.0
33-149
5.0
20
Chloroform
mg/Kg
0.050
0.050
0.049
100
98.6
73-127
1.6
20
Chloromethane
mg/Kg
0.050
0.044
0.039
88.6
79.6
45-143
10.7
20
2-Chlorotoluene
mg/Kg
0.050
0.047
0.045
95.6
91.8
67-124
4.0
20
4-Chlorotoluene
mg/Kg
0.050
0.047
0.045
95.6
91.8
71-126
4.0
20
Di -Isopropyl Ether (DIPE)
mg/Kg
0.050
0.049
0.048
98.0
96.4
59-159
1.6
20
1,2-Dibromo-3-Chloropropane
mg/Kg
0.050
0.053
0.052
107
104
55-157
2.6
20
1,2-Dibromoethane
mg/Kg
0.050
0.051
0.048
104
97.6
70-132
5.9
20
Dibromomethane
mg/Kg
0.050
0.052
0.050
104
100
74-133
3.5
20
1,2-Dichlorobenzene
mg/Kg
0.050
0.049
0.049
99.2
98.6
72-123
0.6
20
1,3-Dichlorobenzene
mg/Kg
0.050
0.049
0.049
99.4
98.2
71-120
1.2
20
Date: 06/21/2023 02:47 PM Page 20 of 36
Page 208 of 229

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V34299 QC Analytical Batch(es): V34300
QC Prep Batch Method: 5035 Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V34299 LCSD-V34299
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
1,4-Dichlorobenzene
mg/Kg
0.050
0.048
0.048
97.2
96.2
71-123
1.0
20
Dichlorodifluoromethane
mg/Kg
0.050
0.047
0.045
95.4
90.8
26-146
4.9
20
1,1-Dichloroethane
mg/Kg
0.050
0.050
0.048
100
97.0
74-127
3.0
20
1,2-Dichloroethane
mg/Kg
0.050
0.048
0.047
97.8
94.2
68-128
3.7
20
1,1-Dichloroethene
mg/Kg
0.050
0.050
0.043
101
87.6
67-149
14.0
20
cis-1,2-Dichloroethene
mg/Kg
0.050
0.050
0.049
100
98.6
76-134
1.8
20
trans-1,2-Dichloroethene
mg/Kg
0.050
0.050
0.049
101
98.2
73-132
3.0
20
1,2-Dichloropropane
mg/Kg
0.050
0.049
0.048
98.4
96.2
73-130
2.2
20
1,3-Dichloropropane
mg/Kg
0.050
0.051
0.048
103
96.0
75-124
6.8
20
2,2-Dichloropropane
mg/Kg
0.050
0.050
0.047
102
95.2
50-142
6.5
20
1,1-Dichloropropene
mg/Kg
0.050
0.050
0.047
100
94.6
71-130
5.5
20
cis-1,3-Dichloropropene
mg/Kg
0.050
0.051
0.050
102
100
71-125
1.7
20
trans-1,3-Dichloropropene
mg/Kg
0.050
0.052
0.053
106
106
68-123
0.3
20
Ethanol
mg/Kg
1.25
1.46
1.26
117
101
70-130
14.7
20
Ethylbenzene
mg/Kg
0.050
0.047
0.046
95.0
93.0
74-128
2.1
20
Ethyl Tertiary Butyl Ether (ETBE)
mg/Kg
0.100
0.098
0.096
98.1
96.5
70-130
1.6
20
Hexachlorobutadiene
mg/Kg
0.050
0.052
0.049
104
99.6
64-125
4.5
20
n-Hexane
mg/Kg
0.050
0.053
0.047
107
94.2
70-130
13.0
20
2-Hexanone
mg/Kg
0.050
0.059
0.058
119
117
61-157
1.8
20
Isopropyl benzene
mg/Kg
0.050
0.048
0.047
96.4
94.4
68-126
2.0
20
4-Isopropyl toluene
mg/Kg
0.050
0.049
0.048
98.8
96.0
68-129
2.8
20
Methyl Ethyl Ketone (MEK)
mg/Kg
0.050
0.047
0.048
95.0
97.0
63-149
2.0
20
Methyl tert-butyl ether (MTBE)
mg/Kg
0.050
0.049
0.048
98.8
96.8
70-130
2.0
20
4-Methyl-2-Pentanone
mg/Kg
0.050
0.051
0.053
104
107
57-162
3.0
20
Methylene Chloride
mg/Kg
0.050
0.047
0.045
95.0
91.4
74-129
3.8
20
Naphthalene
mg/Kg
0.050
0.049
0.047
99.6
95.6
57-157
4.0
20
Date: 06/21/2023 02:47 PM Page 21 of 36
Page 209 of 229

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
Hart & Hickman (Charlotte)
TPM-001
23-163-0001
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V34299 QC Analytical Batch(es): V34300
QC Prep Batch Method: 5035 Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V34299 LCSD-V34299
Spike LCS LCSD LCS LCSD % Rec
Parameter Units Conc. Result Result %Rec % Rec Limits RPD Max
RPD
n-Propylbenzene
mg/Kg
0.050
0.048
0.046
96.8
92.0
67-130
Styrene
mg/Kg
0.050
0.053
0.051
107
103
77-121
1,1,1,2-Tetrachloroethane
mg/Kg
0.050
0.048
0.046
96.4
93.8
72-115
1,1,2,2-Tetrachloroethane
mg/Kg
0.050
0.048
0.044
97.0
89.8
56-126
Tetrachloroethene
mg/Kg
0.050
0.050
0.048
101
96.2
68-130
Toluene
mg/Kg
0.050
0.050
0.048
100
97.8
71-129
1,2,3-Trichlorobenzene
mg/Kg
0.050
0.048
0.049
97.0
98.6
68-130
1,2,4-Trichlorobenzene
mg/Kg
0.050
0.053
0.051
108
104
66-125
1,1,1-Trichloroethane
mg/Kg
0.050
0.049
0.047
99.8
94.6
67-131
1,1,2-Trichloroethane
mg/Kg
0.050
0.051
0.047
103
95.4
70-133
Trichloroethene
mg/Kg
0.050
0.050
0.049
101
99.4
75-133
Trichlorofluoromethane
mg/Kg
0.050
0.045
0.041
90.0
82.6
44-146
1,2,3-Trichloropropane
mg/Kg
0.050
0.049
0.045
98.6
90.4
60-137
1,2,4-Trimethyl benzene
mg/Kg
0.050
0.049
0.049
98.6
98.2
69-129
1,3,5-Trimethylbenzene
mg/Kg
0.050
0.049
0.046
98.4
93.0
69-128
Vinyl Acetate
mg/Kg
0.050
0.062
0.059
125
120
60-140
Vinyl Chloride
mg/Kg
0.050
0.051
0.048
102
96.2
48-147
o-Xylene
mg/Kg
0.050
0.051
0.047
102
95.6
74-126
m,p-Xylene
mg/Kg
0.100
0.101
0.094
101
94.8
75-124
4-Bromofluorobenzene (S)
101
103
70-130
Dibromofluoromethane (S)
102
101
84-123
Toluene-d8(S)
103
98.8
76-129
5.0
3.9
2.7
7.7
4.4
2.6
1.6
3.5
5.3
7.6
1.7
8.5
8.6
0.4
5.6
3.9
5.8
6.6
6.3
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Date: 06/21/2023 02:47 PM Page 22 of 36
Page 210 of 229

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
QC Prep: V34327
QC Prep Batch Method: 3546
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Analytical Batch(es): V34353
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V34327 Matrix: SOL
Associated Lab Samples: 98049, 98050, 98064, 98065, 98066, 98067, 98070, 98071, 98072, 98073, 98074, 98075, 98076, 98077, 98078
Blank MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Acenaphthene
mg/Kg
<0.660
0.660
06/14/23 16:20
Acenaphthylene
mg/Kg
<0.660
0.660
06/14/23 16:20
Aniline
mg/Kg
<0.660
0.660
06/14/23 16:20
Anthracene
mg/Kg
<0.660
0.660
06/14/23 16:20
Benzo(a)anthracene
mg/Kg
<0.660
0.660
06/14/23 16:20
Benzo(a)pyrene
mg/Kg
<0.660
0.660
06/14/23 16:20
Benzo(b)fluoranthene
mg/Kg
<0.660
0.660
06/14/23 16:20
Benzo(g,h,i)perylene
mg/Kg
<0.660
0.660
06/14/23 16:20
Benzo(k)fluoranthene
mg/Kg
<0.660
0.660
06/14/23 16:20
Benzoic Acid
mg/Kg
<2.00
2.00
06/14/23 16:20
Benzyl alcohol
mg/Kg
<0.660
0.660
06/14/23 16:20
Bis(2-Chloroethoxy)methane
mg/Kg
<0.660
0.660
06/14/23 16:20
Bis(2-Chloroethyl)ether
mg/Kg
<0.660
0.660
06/14/23 16:20
Bis(2-Chloroisopropyl)ether
mg/Kg
<0.330
0.330
06/14/23 16:20
Bis(2-ethylhexyl)phthalate
mg/Kg
<0.660
0.660
06/14/23 16:20
4-Bromophenyl phenyl ether
mg/Kg
<0.660
0.660
06/14/23 16:20
Butyl benzyl phthalate
mg/Kg
<0.330
0.330
06/14/23 16:20
4-Chloro-3-methylphenol
mg/Kg
<0.660
0.660
06/14/23 16:20
4-Chloroaniline
mg/Kg
<0.330
0.330
06/14/23 16:20
2-Chloronaphthalene
mg/Kg
<0.660
0.660
06/14/23 16:20
2-Chlorophenol
mg/Kg
<0.660
0.660
06/14/23 16:20
4-Chlorophenyl phenyl ether
mg/Kg
<1.00
1.00
06/14/23 16:20
Chrysene
mg/Kg
<0.660
0.660
06/14/23 16:20
Dibenz(a,h)anthracene
mg/Kg
<0.660
0.660
06/14/23 16:20
Dibenzofuran
mg/Kg
<0.660
0.660
06/14/23 16:20
1,2-Dichlorobenzene
mg/Kg
<0.660
0.660
06/14/23 16:20
1,3-Dichlorobenzene
mg/Kg
<0.660
0.660
06/14/23 16:20
Date: 06/21/2023 02:47 PM Page 23 of 36
Page 211 of 229

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
QC Prep: V34327
QC Prep Batch Method: 3546
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Analytical Batch(es): V34353
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V34327 Matrix: SOL
Associated Lab Samples: 98049, 98050, 98064, 98065, 98066, 98067, 98070, 98071, 98072, 98073, 98074, 98075, 98076, 98077, 98078
Blank MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
1,4-Dichlorobenzene
mg/Kg
<0.330
0.330
06/14/23 16:20
3,3'-Dichlorobenzidine
mg/Kg
<0.660
0.660
06/14/23 16:20
2,4-Dichlorophenol
mg/Kg
<0.660
0.660
06/14/23 16:20
Diethyl phthalate
mg/Kg
<0.660
0.660
06/14/23 16:20
Dimethyl phthalate
mg/Kg
<0.660
0.660
06/14/23 16:20
2,4-Dimethylphenol
mg/Kg
<0.330
0.330
06/14/23 16:20
Di-n-butyl phthalate
mg/Kg
<0.660
0.660
06/14/23 16:20
4,6- Din itro-2-methylphenol
mg/Kg
<1.50
1.50
06/14/23 16:20
2,4-Dinitrophenol
mg/Kg
<1.50
1.50
06/14/23 16:20
2,4-Dinitrotoluene
mg/Kg
<0.660
0.660
06/14/23 16:20
2,6-Dinitrotoluene
mg/Kg
<0.660
0.660
06/14/23 16:20
Di-n-Octyl Phthalate
mg/Kg
<0.330
0.330
06/14/23 16:20
Fluoranthene
mg/Kg
<0.660
0.660
06/14/23 16:20
Fluorene
mg/Kg
<0.660
0.660
06/14/23 16:20
Hexachlorobenzene
mg/Kg
<0.660
0.660
06/14/23 16:20
Hexachlorobutadiene
mg/Kg
<0.660
0.660
06/14/23 16:20
Hexachlorocyclopentadiene
mg/Kg
<0.660
0.660
06/14/23 16:20
Hexachloroethane
mg/Kg
<0.660
0.660
06/14/23 16:20
Indeno(1,2,3-cd)pyrene
mg/Kg
<0.660
0.660
06/14/23 16:20
Isophorone
mg/Kg
<0.660
0.660
06/14/23 16:20
1-Methylnaphthalene
mg/Kg
<0.660
0.660
06/14/23 16:20
2-Methylnaphthalene
mg/Kg
<0.660
0.660
06/14/23 16:20
2-Methylphenol
mg/Kg
<0.660
0.660
06/14/23 16:20
3&4 Methylphenol
mg/Kg
<0.660
0.660
06/14/23 16:20
Naphthalene
mg/Kg
<0.660
0.660
06/14/23 16:20
2-Nitroaniline
mg/Kg
<0.660
0.660
06/14/23 16:20
3-Nitroaniline
mg/Kg
<0.660
0.660
06/14/23 16:20
Date: 06/21/2023 02:47 PM Page 24 of 36
Page 212 of 229

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
QC Prep: V34327
QC Prep Batch Method: 3546
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Analytical Batch(es): V34353
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Lab Reagent Blank
LRB-V34327
Matrix: SOL
Associated Lab Samples:
98049, 98050, 98064, 98065, 98066,
98067, 98070, 98071, 98072, 98073, 98074, 98075, 98076, 98077, 98078
Blank
MQL
Analyzed % % Rec
Parameter
Units
Result
Recovery Limits
4-Nitroaniline
mg/Kg
<0.330
0.330
06/14/23 16:20
Nitrobenzene
mg/Kg
<0.330
0.330
06/14/23 16:20
2-Nitrophenol
mg/Kg
<0.660
0.660
06/14/23 16:20
4-Nitrophenol
mg/Kg
<0.660
0.660
06/14/23 16:20
N-Nitrosodimethylamine
mg/Kg
<0.660
0.660
06/14/23 16:20
N-Nitrosodiphenylamine
mg/Kg
<0.660
0.660
06/14/23 16:20
N-Nitroso-di-n-propylamine
mg/Kg
<0.660
0.660
06/14/23 16:20
Pentachlorophenol
mg/Kg
<1.00
1.00
06/14/23 16:20
Phenanthrene
mg/Kg
<0.660
0.660
06/14/23 16:20
Phenol
mg/Kg
<0.660
0.660
06/14/23 16:20
Pyrene
mg/Kg
<0.660
0.660
06/14/23 16:20
Pyridine
mg/Kg
<0.330
0.330
06/14/23 16:20
1,2,4-Trichlorobenzene
mg/Kg
<0.660
0.660
06/14/23 16:20
2,4,5-Trichlorophenol
mg/Kg
<0.660
0.660
06/14/23 16:20
2,4,6-Trichlorophenol
mg/Kg
<0.660
0.660
06/14/23 16:20
2-Fluorobiphenyl (S)
06/14/23 16:20
73.6
44-115
2-Fluorophenol (S)
06/14/23 16:20
60.9
35-115
Nitrobenzene-d5 (S)
06/14/23 16:20
65.8
37-122
4-Terphenyl-d14 (S)
06/14/23 16:20
83.8
54-127
2,4,6-Tribromophenol(S)
06/14/23 16:20
54.0
39-132
Phenol-d5 (S)
06/14/23 16:20
56.4
34-121
Laboratory Control Sample
LCS-V34327
Spike
LCS
LCS %Rec
% Rec
Parameter
Units Conc.
Result
Limits
Acenaphthene
mg/Kg 1.67
1.18
70.6
40-123
Acenaphthylene
mg/Kg 1.67
1.19
71.2
32-132
Date: 06/21/2023 02:47 PM Page 25 of 36
Page 213 of 229

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V34327 QC Analytical Batch(es): V34353
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample LCS-V34327
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
Aniline
mg/Kg
1.67
1.69
101
12-197
Anthracene
mg/Kg
1.67
1.39
83.2
47-123
Benzo(a)anthracene
mg/Kg
1.67
1.32
79.0
49-126
Benzo(a)pyrene
mg/Kg
1.67
1.41
84.4
45-129
Benzo(b)fluoranthene
mg/Kg
1.67
1.39
83.2
45-132
Benzo(g,h,i)perylene
mg/Kg
1.67
1.17
70.0
43-134
Benzo(k)fluoranthene
mg/Kg
1.67
1.32
79.0
47-132
Benzoic Acid
mg/Kg
1.67
<2.00
56.7
10-83
Benzyl alcohol
mg/Kg
1.67
1.12
67.0
29-122
Bis(2-Chloroethoxy)methane
mg/Kg
1.67
1.19
71.2
36-121
Bis(2-Chloroethyl)ether
mg/Kg
1.67
1.03
61.6
31-120
Bis(2-Chloroisopropyl)ether
mg/Kg
1.67
1.12
67.0
33-131
Bis(2-ethylhexyl)phthalate
mg/Kg
1.67
1.21
72.4
51-133
4-Bromophenyl phenyl ether
mg/Kg
1.67
1.34
80.2
46-124
Butyl benzyl phthalate
mg/Kg
1.67
1.28
76.6
48-132
4-Chloro-3-methyl phenol
mg/Kg
1.67
1.22
73.0
45-122
4-Chloroaniline
mg/Kg
1.67
1.22
73.0
17-106
2-Chloronaphthalene
mg/Kg
1.67
1.18
70.6
41-114
2-Chlorophenol
mg/Kg
1.67
1.05
62.8
34-121
4-Chlorophenyl phenyl ether
mg/Kg
1.67
1.27
76.0
45-121
Chrysene
mg/Kg
1.67
1.32
79.0
50-124
Dibenz(a,h)anthracene
mg/Kg
1.67
1.13
67.6
45-134
Dibenzofuran
mg/Kg
1.67
1.16
69.4
44-120
1,2-Dichlorobenzene
mg/Kg
1.67
1.01
60.4
33-117
1,3-Dichlorobenzene
mg/Kg
1.67
0.990
59.2
30-115
1,4-Dichlorobenzene
mg/Kg
1.67
1.02
61.0
31-115
3,3'-Dichlorobenzidine
mg/Kg
1.67
1.13
67.6
22-121
Date: 06/21/2023 02:47 PM Page 26 of 36
Page 214 of 229

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V34327 QC Analytical Batch(es): V34353
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample LCS-V34327
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
2,4-Dichlorophenol
mg/Kg
1.67
1.21
72.4
40-122
Diethyl phthalate
mg/Kg
1.67
1.24
74.2
50-124
Dimethyl phthalate
mg/Kg
1.67
1.27
76.0
48-124
2,4-Dimethylphenol
mg/Kg
1.67
1.55
92.8
30-127
Di-n-butyl phthalate
mg/Kg
1.67
1.45
86.8
51-128
4,6- Din itro-2-methylphenol
mg/Kg
1.67
<1.50
76.0
29-132
2,4-Dinitrophenol
mg/Kg
1.67
<1.50
74.2
27-129
2,4-Dinitrotoluene
mg/Kg
1.67
1.24
74.2
48-126
2,6-Dinitrotoluene
mg/Kg
1.67
1.26
75.4
46-124
Di-n-Octyl Phthalate
mg/Kg
1.67
1.33
79.6
45-140
Fluoranthene
mg/Kg
1.67
1.34
80.2
50-127
Fluorene
mg/Kg
1.67
1.25
74.8
43-125
Hexachlorobenzene
mg/Kg
1.67
1.26
75.4
45-122
Hexachlorobutadiene
mg/Kg
1.67
1.18
70.6
32-123
Hexachlorocyclopentadiene
mg/Kg
1.67
1.11
66.4
32-117
Hexachloroethane
mg/Kg
1.67
0.999
59.8
28-117
Indeno(1,2,3-cd)pyrene
mg/Kg
1.67
1.20
71.8
45-133
Isophorone
mg/Kg
1.67
1.04
62.2
30-122
1-Methylnaphthalene
mg/Kg
1.67
1.08
64.6
40-119
2-Methylnaphthalene
mg/Kg
1.67
1.11
66.4
38-122
2-Methylphenol
mg/Kg
1.67
1.09
65.2
32-122
3&4 Methylphenol
mg/Kg
1.67
0.987
59.1
34-119
Naphthalene
mg/Kg
1.67
1.11
66.4
35-123
2-Nitroaniline
mg/Kg
1.67
1.33
79.6
44-127
3-Nitroaniline
mg/Kg
1.67
1.22
73.0
33-119
4-Nitroaniline
mg/Kg
1.67
1.36
81.4
63-147
Nitrobenzene
mg/Kg
1.67
1.08
64.6
34-122
Date: 06/21/2023 02:47 PM Page 27 of 36
Page 215 of 229

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
QC Prep: V34327
QC Prep Batch Method: 3546
Laboratory Control Sample
Parameter
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
N-N itroso-d i-n-propyl a m i ne
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
4-Terphenyl-d14 (S)
2,4,6-Tribromophenol (S)
Phenol-d5 (S)
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
LCS-V34327
Spike
Units Conc.
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
QC Analytical Batch(es): V34353
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
LCS
Result
1.12
1.10
0.915
1.57
1.07
1.30
1.32
1.06
1.33
0.717
1.11
1.18
1.15
LCS %Rec
67.0
65.8
54.7
94.0
64.0
77.8
79.0
63.4
79.6
42.9
66.4
70.6
68.8
75.4
63.9
70.0
90.4
69.9
58.8
Rec
Limits
36-123
30-132
10-146
38-127
36-120
25-133
50-121
34-121
47-127
10-80
34-118
41-124
39-126
44-115
35-115
37-122
54-127
39-132
34-121
Matrix Spike & Matrix Spike Duplicate
V 97822-MS-V34327
V 97822-MSD-V34327
MS Spike
MSD
MS Result
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Conc.
Spike
Result
%Rec
%Rec
Limits
RPD
RPD
Conc.
Acenaphthene
mg/Kg
<0.661
1.67
1.66
1.02
1.10
61.0
66.2
40-123
7.5
20
Acenaphthylene
mg/Kg
<0.661
1.67
1.66
1.01
1.05
60.4
63.2
32-132
3.8
20
Aniline
mg/Kg
<0.661
1.67
1.66
1.74
2.02
104
122
12-197
14.8
20
Date: 06/21/2023 02:47 PM Page 28 of 36
Page 216 of 229

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V34327 QC Analytical Batch(es): V34353
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix Spike & Matrix Spike Duplicate V 97822-MS-V34327 V 97822-MSD-V34327
Parameter
Units
Result
MS Spike
Conc.
MSD
Spike
Conc.
MS Result
MSD
Result
MS
a/oRec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
Anthracene
mg/Kg
<0.661
1.67
1.66
1.16
1.24
69.4
74.6
47-123
6.6
20
Benzo(a)anthracene
mg/Kg
<0.661
1.67
1.66
1.13
1.17
67.6
70.4
49-126
3.4
20
Benzo(a)pyrene
mg/Kg
<0.661
1.67
1.66
1.20
1.26
71.8
75.9
45-129
4.8
20
Benzo(b)fluoranthene
mg/Kg
<0.661
1.67
1.66
1.19
1.24
71.2
74.6
45-132
4.1
20
Benzo(g,h,i)perylene
mg/Kg
<0.661
1.67
1.66
1.01
1.04
60.4
62.6
43-134
2.9
20
Benzo(k)fluoranthene
mg/Kg
<0.661
1.67
1.66
1.14
1.17
68.2
70.4
47-132
2.5
20
Benzoic Acid
mg/Kg
<2.00
1.67
1.66
0.694
0.716
41.5
43.1
10-83
3.1
20
Benzyl alcohol
mg/Kg
<0.661
1.67
1.66
0.985
1.01
58.9
60.8
29-122
2.5
20
Bis(2-Chloroethoxy)methane
mg/Kg
<0.661
1.67
1.66
1.04
1.08
62.2
65.0
36-121
3.7
20
Bis(2-Chloroethyl)ether
mg/Kg
<0.661
1.67
1.66
0.934
0.950
55.9
57.2
31-120
1.6
20
Bis(2-Chloroisopropyl)ether
mg/Kg
<0.330
1.67
1.66
1.04
1.05
62.2
63.2
33-131
0.9
20
Bis(2-ethylhexyl)phthalate
mg/Kg
<0.661
1.67
1.66
1.05
1.06
62.8
63.8
51-133
0.9
20
4-Bromophenyl phenyl ether
mg/Kg
<0.661
1.67
1.66
1.08
1.20
64.6
72.2
46-124
10.5
20
Butyl benzyl phthalate
mg/Kg
<0.330
1.67
1.66
1.12
1.13
67.0
68.0
48-132
0.8
20
4-Chloro-3-methyl phenol
mg/Kg
<0.661
1.67
1.66
1.01
1.06
60.4
63.8
45-122
4.8
20
4-Chloroaniline
mg/Kg
<0.330
1.67
1.66
1.11
1.14
66.4
68.6
17-106
2.6
20
2-Chloronaphthalene
mg/Kg
<0.661
1.67
1.66
1.07
1.10
64.0
66.2
41-114
2.7
20
2-Chlorophenol
mg/Kg
<0.661
1.67
1.66
0.944
0.936
56.5
56.3
34-121
0.8
20
4-Chlorophenyl phenyl ether
mg/Kg
<1.00
1.67
1.66
1.04
1.15
62.2
69.2
45-121
10.0
20
Chrysene
mg/Kg
<0.661
1.67
1.66
1.12
1.18
67.0
71.0
50-124
5.2
20
Dibenz(a,h)anthracene
mg/Kg
<0.661
1.67
1.66
0.944
1.02
56.5
61.4
45-134
7.7
20
Dibenzofuran
mg/Kg
<0.661
1.67
1.66
1.00
1.05
59.8
63.2
44-120
4.8
20
1,2-Dichlorobenzene
mg/Kg
<0.661
1.67
1.66
0.909
0.949
54.4
57.1
33-117
4.3
20
1,3-Dichlorobenzene
mg/Kg
<0.661
1.67
1.66
0.854
0.882
51.1
53.1
30-115
3.2
20
1,4-Dichlorobenzene
mg/Kg
<0.330
1.67
1.66
0.878
0.909
52.5
54.7
31-115
3.4
20
3,3'-Dichlorobenzidine
mg/Kg
<0.661
1.67
1.66
0.990
1.05
59.2
63.2
22-121
5.8
20
Date: 06/21/2023 02:47 PM Page 29 of 36
Page 217 of 229

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V34327 QC Analytical Batch(es): V34353
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix Spike & Matrix Spike Duplicate V 97822-MS-V34327 V 97822-MSD-V34327
Parameter
Units
Result
MS Spike
Conc.
MSD
Spike
Conc.
MS Result
MSD
Result
MS
a/oRec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
2,4-Dichlorophenol
mg/Kg
<0.661
1.67
1.66
1.04
1.12
62.2
67.4
40-122
7.4
20
Diethyl phthalate
mg/Kg
<0.661
1.67
1.66
1.06
1.12
63.4
67.4
50-124
5.5
20
Dimethyl phthalate
mg/Kg
<0.661
1.67
1.66
1.06
1.13
63.4
68.0
48-124
6.3
30
2,4-Dimethylphenol
mg/Kg
<0.330
1.67
1.66
1.38
1.41
82.6
84.9
30-127
2.1
20
Di-n-butyl phthalate
mg/Kg
<0.661
1.67
1.66
1.22
1.25
73.0
75.3
51-128
2.4
20
4,6- Din itro-2-methylphenol
mg/Kg
<1.50
1.67
1.66
0.493
0.361
29.5
21.7*
29-132
30.9*
20
2,4-Dinitrophenol
mg/Kg
<1.50
1.67
1.66
<0.520
<0.520
0.0*
0.0*
27-129
0.0
20
2,4-Dinitrotoluene
mg/Kg
<0.661
1.67
1.66
0.716
0.479
42.8*
28.8*
48-126
39.6*
20
2,6-Dinitrotoluene
mg/Kg
<0.661
1.67
1.66
0.818
0.526
48.9
31.6*
46-124
43.4*
20
Di-n-Octyl Phthalate
mg/Kg
<0.330
1.67
1.66
1.15
1.18
68.8
71.0
45-140
2.5
20
Fluoranthene
mg/Kg
<0.661
1.67
1.66
1.10
1.15
65.8
69.2
50-127
4.4
20
Fluorene
mg/Kg
<0.661
1.67
1.66
1.03
1.13
61.6
68.0
43-125
9.2
20
Hexachlorobenzene
mg/Kg
<0.661
1.67
1.66
0.996
1.12
59.6
67.4
45-122
11.7
20
Hexachlorobutadiene
mg/Kg
<0.661
1.67
1.66
1.02
1.05
61.0
63.2
32-123
2.8
20
Hexachlorocyclopentadiene
mg/Kg
<0.661
1.67
1.66
0.507
0.435
30.3*
26.2*
32-117
15.2
20
Hexachloroethane
mg/Kg
<0.661
1.67
1.66
0.850
0.804
50.8
48.4
28-117
5.5
20
Indeno(1,2,3-cd)pyrene
mg/Kg
<0.661
1.67
1.66
1.02
1.08
61.0
65.0
45-133
5.7
20
Isophorone
mg/Kg
<0.661
1.67
1.66
0.889
0.924
53.2
55.6
30-122
3.8
20
1-Methylnaphthalene
mg/Kg
<0.661
1.67
1.66
0.961
1.01
57.5
60.8
40-119
4.9
20
2-Methylnaphthalene
mg/Kg
<0.661
1.67
1.66
0.948
1.01
56.7
60.8
38-122
6.3
20
2-Methylphenol
mg/Kg
<0.661
1.67
1.66
0.996
1.03
59.6
62.0
32-122
3.3
20
3&4 Methylphenol
mg/Kg
<0.661
1.67
1.66
0.894
0.918
53.5
55.3
34-119
2.6
20
Naphthalene
mg/Kg
<0.661
1.67
1.66
0.962
1.01
57.6
60.8
35-123
4.8
20
2-Nitroaniline
mg/Kg
<0.661
1.67
1.66
1.09
0.869
65.2
52.3
44-127
22.5*
20
3-Nitroaniline
mg/Kg
<0.661
1.67
1.66
0.774
0.632
46.3
38.0
33-119
20.1*
20
4-Nitroaniline
mg/Kg
<0.330
1.67
1.66
1.15
0.975
68.8
58.7*
63-147
16.4
20
* QC Fail Date: 06/21/2023 02:47 PM Page 30 of 36
Page 218 of 229

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V34327 QC Analytical Batch(es): V34353
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix Spike & Matrix Spike Duplicate V 97822-MS-V34327 V 97822-MSD-V34327
Parameter
Units
Result
MS Spike
Conc.
MSD
Spike
Conc.
MS Result
MSD
Result
MS
a/oRec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
Nitrobenzene
mg/Kg
<0.330
1.67
1.66
0.757
0.550
45.3
33.1*
34-122
31.6*
20
2-Nitrophenol
mg/Kg
<0.661
1.67
1.66
0.397
0.339
23.7*
20.4*
32-123
15.7
20
4-Nitrophenol
mg/Kg
<0.661
1.67
1.66
0.799
0.702
47.8
42.2
30-132
12.9
20
N-Nitrosodimethylamine
mg/Kg
<0.661
1.67
1.66
0.801
0.814
47.9
49.0
10-146
1.6
30
N-Nitrosodiphenylamine
mg/Kg
<0.661
1.67
1.66
1.31
1.37
78.4
82.5
38-127
4.4
20
N-Nitroso-di-n-propylamine
mg/Kg
<0.661
1.67
1.66
0.972
0.986
58.2
59.3
36-120
1.4
20
Pentachlorophenol
mg/Kg
<1.00
1.67
1.66
1.04
1.16
62.2
69.8
25-133
10.9
20
Phenanthrene
mg/Kg
<0.661
1.67
1.66
1.12
1.17
67.0
70.4
50-121
4.3
20
Phenol
mg/Kg
<0.661
1.67
1.66
0.964
0.981
57.7
59.0
34-121
1.7
20
Pyrene
mg/Kg
<0.661
1.67
1.66
1.10
1.13
65.8
68.0
47-127
2.6
20
Pyridine
mg/Kg
<0.330
1.67
1.66
0.658
0.652
39.4
39.2
10-80
0.9
20
1,2,4-Trichlorobenzene
mg/Kg
<0.661
1.67
1.66
0.970
1.01
58.0
60.8
34-118
4.0
20
2,4,5-Trichlorophenol
mg/Kg
<0.661
1.67
1.66
1.08
1.13
64.6
68.0
41-124
4.5
20
2,4,6-Trichlorophenol
mg/Kg
<0.661
1.67
1.66
1.03
1.09
61.6
65.6
39-126
5.6
20
2-Fluorobiphenyl (S)
67.6
72.8
44-115
2-Fluorophenol (S)
58.3
57.0
35-115
Nitrobenzene-d5 (S)
51.7
44.7
37-122
4-Terphenyl-d14 (S)
73.0
77.1
54-127
2,4,6-Tribromophenol (S)
53.2
60.3
39-132
Phenol-d5 (S)
52.6
53.1
34-121
* QC Fail Date: 06/21/2023 02:47 PM Page 31 of 36
Page 219 of 229

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
QC Prep:
V34271
QC Analytical Batch(es): V34449
QC Prep Batch Method:
MAEPH (Prep)
Analysis Method: MADEP-EPH
Analysis Description: Massachusetts EPH
Lab Reagent Blank
LRB-V34271
Matrix: SOL
Associated Lab Samples:
98049, 98050, 98064, 98065, 98066,
98067, 98070, 98071, 98072, 98073, 98074, 98075, 98076, 98077, 98078
Blank
MQL Analyzed % % Rec
Parameter
Units
Result
Recovery Limits
Aliphatic C9-C18
mg/Kg
<50.0
50.0 06/16/23 17:35
Aliphatic C19-06
mg/Kg
<50.0
50.0 06/16/23 17:35
Aromatic C11-C22
mg/Kg
<50.0
50.0 06/16/23 17:35
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
Chlorooctadecane (S)
OTP Surrogate (S)
06/16/23 17:35
06/16/23 17:35
06/16/23 17:35
06/16/23 17:35
111
114
78.7
100
40-140
40-140
40-140
40-140
Laboratory Control Sample
& LCSD
LCS-V34271
LCSD-V34271
Spike
LCS
LCSD
LCS LCSD
% Rec
Parameter
Units
Conc.
Result
Result
%Rec a/o Rec
Limits
RPD
Max
RPD
Aliphatic C9-C18
mg/Kg
60.0
<50.0
<50.0
72.6 62.3
40-140
15.3
50
Aliphatic C19-06
mg/Kg
80.0
75.1
64.3
93.8 80.3
40-140
15.4
50
Aromatic Cll-C22
mg/Kg
170
221
209
130 123
40-140
5.5
50
2-Fluorobiphenyl (S)
109 100
40-140
2-Bromonaphthalene (S)
107 99.2
40-140
Chlorooctadecane (S)
76.1 69.0
40-140
OTP Surrogate (S)
106 103
40-140
Date: 06/21/2023 02:47 PM Page 32 of 36
Page 220 of 229

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
QC Prep:
V34232
QC Analytical Batch(es): V34233
QC Prep Batch Method:
MAVPH (Prep)
Analysis Method:
MADEP-VPH
Analysis Description:
Massachusetts VPH
Lab Reagent Blank
LRB-V34232
Matrix: SOL
Associated Lab Samples: 98049, 98050, 98064, 98065, 98066,
98067, 98070, 98071, 98072,
98073, 98074, 98075, 98076, 98077, 98078
Blank
MQL
Analyzed %
% Rec
Parameter
Units
Result
Recovery
Limits
Aliphatic C5-C8
mg/Kg
<8.00
8.00
06/12/23 14:50
Aliphatic C9-C12
mg/Kg
<8.00
8.00
06/12/23 14:50
Aromatic C9-C10
mg/Kg
<8.00
8.00
06/12/23 14:50
2,5-Dibromotoluene (FID)(S)
06/12/23 14:50 89.3
70-130
2,5-Dibromotoluene (PID)(S)
06/12/23 14:50 97.1
70-130
Laboratory Control Sample & LCSD
LCS-V34232
LCSD-V34232
Spike
LCS
LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result
Result
%Rec
% Rec
Limits
RPD
Max
RPD
Aliphatic C5-C8
mg/Kg
32.0
34.5
35.1
108
110
70-130
1.7
50
Aliphatic C9-C12
mg/Kg
32.0
35.4
36.2
111
113
70-130
2.2
50
Aromatic C9-C10
mg/Kg
10.7
12.4
12.4
116
116
70-130
0.0
50
2,5-Dibromotoluene (FID) (S)
88.5
96.2
70-130
2,5-Dibromotoluene (PID) (S)
104
99.0
70-130
Date: 06/21/2023 02:47 PM Page 33 of 36
Page 221 of 229

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
QC Analytical Batch: V34226
Analysis Method: SW-DRYWT
Analysis Description: Dry Weight Determination
Duplicate V 97938-DUP
Result DUP
Parameter Units Result
Moisture % 15.1 15.1
Duplicate V 97950-DUP
RPD Max RPD Analyzed
0.0 20.0 06/12/23 17:50
Result DUP RPD Max RPD Analyzed
Parameter Units Result
Moisture % 12.7 12.8 0.7 20.0 06/12/23 17:50
Date: 06/21/2023 02:47 PM Page 34 of 36
Page 222 of 229

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
QC Analytical Batch: V34289
Analysis Method: SW-DRYWT
Analysis Description: Dry Weight Determination
Duplicate V 98063-DUP
Result DUP
Parameter Units Result
Moisture % 26.0 26.1
Duplicate V 98182-DUP
RPD Max RPD Analyzed
0.3 20.0 06/13/23 16:32
Result DUP RPD Max RPD Analyzed
Parameter Units Result
Moisture % 19.1 19.1 0.0 20.0 06/13/23 16:32
Date: 06/21/2023 02:47 PM Page 35 of 36
Page 223 of 229

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-163-0001
QC Analytical Batch: V34290
Analysis Method: SW-DRYWT
Analysis Description: Dry Weight Determination
Duplicate V 98068-DUP
Result DUP
Parameter Units Result
Moisture % 31.6 31.1
Duplicate V 98178-DUP
RPD Max RPD Analyzed
1.5 20.0 06/13/23 16:32
Result DUP RPD Max RPD Analyzed
Parameter Units Result
Moisture % 25.1 25.0 0.3 20.0 06/13/2316:32
Date: 06/21/2023 02:47 PM Page 36 of 36
Page 224 of 229

WayPAoint.
NALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 01102
Customer Name: Hart & Hickman (Charlotte)
Report Number: 23-163-0001
Shipping Method
0 Fed Ex 0 US Postal # Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
IRT15 2.6C
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
# Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
# Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample Iabel(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
U Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
U Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
CO,) N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
F Low concentration EnCore samplers (48 hr)
I✓ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: ngelo Norvell Date & Time: 06/12/2023 09:04:23
Page 225 of 229

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Page 229 of 229

Waypointo
ANALYTICAL
7/25/2023
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 23-199-0028
Client Project Description: TPM-001
Dear Steve Libbey:
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Waypoint Analytical, LLC (Charlotte) received sample(s) on 7/18/2023 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
a'-1
Angela D Overcash
Senior Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 52

Waypoint.0
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State
Program
Lab ID
Expiration Date
North Carolina
State Program
37735
07/31/2023
North Carolina
State Program
402
12/31/2023
South Carolina
State Program
99012
07/31/2023
South Carolina
State Program
99012
12/31/2022
Page 1 of 1 00016/23-199-0028
Page 2 of 52

Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointana lyti ca I som
Sample Summary Table
Report Number: 23-199-0028
Client Project Description: TPM-001
Lab No Client Sample ID Matrix Date Collected Date Received
90011
EX-16-B
Solids
07/17/2023
10:40
07/18/2023
16:39
90012
UST-2-G
Solids
07/17/2023
10:25
07/18/2023
16:39
90013
UST-2-1-1
Solids
07/17/2023
10:50
07/18/2023
16:39
Page 3 of 52

Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointana lyti ca I som
Summary of Detected Analytes
Project: TPM-001
Report Number: 23-199-0028
Client Sample ID Lab Sample ID
Method Parameters Result Units Report Limit Analyzed Qualifiers
EX-16-B
V 90011
8260D
Acetone
SW-DRYWT
Moisture
UST-2-G
V 90012
MADEP-EPH
Aliphatic C9-C18
SW-DRYWT
Moisture
UST-2-1-1
V 90013
SW-DRYWT
Moisture
0.027 mq/Kq - dry 0.024 07/19/2023 13:33
19.8 % 07/19/2023 18:30
91.9 mq/Kq - dry
22.3 %
23.4
64.6 07/21/202319:57
07/19/2023 18:30
07/19/2023 18:30
Page 4 of 52

Waypointo
ANALYTICAL
Client: Hart & Hickman (Charlotte)
Project: TPM-001
Lab Report Number: 23-199-0028
Date: 7/25/2023
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
CASE NARRATIVE
Massachusetts VPH Method MADEP-VPH
Sample 90013 (UST-2-H)
Analyte: 2,5-Dibromotoluene (PID)
QC Batch No: V35510/V35509
Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high
recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all
showed surrogates within QC limits.
Semivolatile Organic Compounds - GC/MS Method 8270E
Sample 90001 (BF-SB-2 (1-3))
Analyte: Aniline
QC Batch No: V35586/V35554
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Sample 90001 (BF-SB-2 (1-3))
Analyte: Pentachlorophenol
QC Batch No: V35586/V35554
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Page 5 of 52

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 07/25/2023
Received : 07/18/2023
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Lab No : 90011 Matrix: Solids
Sample ID: EX-16-B Sampled: 7/17/2023 10:40
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
19.8 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 07/19/2318:30 CNC SW-DRYWT
DF Dilution Factor
Page 6 of 52

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 07/25/2023
2923 South Tryon St. Ste 100 Information : Received : 07/18/2023
Charlotte , NC 28203
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Lab No : 90011
Matrix: Solids
Sample ID: EX-16-B
Sampled:
7/17/2023 10:40
Analytical Method: 8260D
Prep Batch(es):
V35530
07/19/23 08:00
Prep Method: 5035
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
0.027
mg/Kg - dry
0.024
1
07/19/23 13:33
TBL
V35531
Acrolein
<0.024
mg/Kg - dry
0.024
1
07/19/23 13:33
TBL
V35531
Acrylonitrile
<0.024
mg/Kg - dry
0.024
1
07/19/23 13:33
TBL
V35531
Benzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Bromobenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Bromochloromethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Bromodichloromethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Bromoform
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Bromomethane
<0.012
mg/Kg - dry
0.012
1
07/19/23 13:33
TBL
V35531
n-Butylbenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
sec -Butyl benzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
tert-Butyl benzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Carbon Disulfide
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Carbon Tetrachloride
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Chlorobenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Chlorodibromomethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Chloroethane
<0.012
mg/Kg - dry
0.012
1
07/19/23 13:33
TBL
V35531
Chloroform
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Chloromethane
<0.012
mg/Kg - dry
0.012
1
07/19/23 13:33
TBL
V35531
2-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
4-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Di -Isopropyl Ether (DIPE)
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 7 of 52

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 07/25/2023
2923 South Tryon St. Ste 100 Information : Received : 07/18/2023
Charlotte , NC 28203
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Lab No : 90011
Matrix: Solids
Sample ID: EX-16-B
Sampled:
7/17/2023 10:40
Analytical Method: 8260D
Prep Batch(es):
V35530
07/19/23 08:00
Prep Method: 5035
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,2-Dibromo-3-Chloropropane
<0.012
mg/Kg - dry
0.012
1
07/19/23 13:33
TBL
V35531
1,2-Dibromoethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Dibromomethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
1,2-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
1,3-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
1,4-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Dichlorodifluoromethane
<0.012
mg/Kg - dry
0.012
1
07/19/23 13:33
TBL
V35531
1,1-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
1,2-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
1,1-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
cis- 1,2-Dich loroethene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
trans-1,2-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
1,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
1,3-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
2,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
1,1-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
cis-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
trans-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Ethanol
<0.311
mg/Kg - dry
0.311
1
07/19/23 13:33
TBL
V35531
Ethylbenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Ethyl Tertiary Butyl Ether (ETBE)
<0.062
mg/Kg - dry
0.062
1
07/19/23 13:33
TBL
V35531
Hexachlorobutadiene
<0.012
mg/Kg - dry
0.012
1
07/19/23 13:33
TBL
V35531
Qualifiers/ * Outside QC Limit
DF Dilution Factor
Definitions MQL Method Quantitation Limit
Page 8 of 52

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 07/25/2023
2923 South Tryon St. Ste 100 Information : Received : 07/18/2023
Charlotte , NC 28203
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Lab No : 90011
Matrix: Solids
Sample ID: EX-16-B
Sampled:
7/17/2023 10:40
Analytical Method: 8260D
Prep Batch(es):
V35530
07/19/23 08:00
Prep Method: 5035
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
n-Hexane
<0.012
mg/Kg - dry
0.012
1
07/19/23 13:33
TBL
V35531
2-Hexanone
<0.024
mg/Kg - dry
0.024
1
07/19/23 13:33
TBL
V35531
Isopropyl benzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
4-Isopropyl toluene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Methyl Ethyl Ketone (MEK)
<0.024
mg/Kg - dry
0.024
1
07/19/23 13:33
TBL
V35531
Methyl tert-butyl ether (MTBE)
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
4-Methyl-2-Pentanone
<0.024
mg/Kg - dry
0.024
1
07/19/23 13:33
TBL
V35531
Methylene Chloride
<0.012
mg/Kg - dry
0.012
1
07/19/23 13:33
TBL
V35531
Naphthalene
<0.012
mg/Kg - dry
0.012
1
07/19/23 13:33
TBL
V35531
n-Propylbenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Styrene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
1,1,1,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
1,1,2,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Tetrachloroethene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Toluene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
1,2,3-Trichlorobenzene
<0.012
mg/Kg - dry
0.012
1
07/19/23 13:33
TBL
V35531
1,2,4-Trichlorobenzene
<0.012
mg/Kg - dry
0.012
1
07/19/23 13:33
TBL
V35531
1,1,1-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
1,1,2-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Trichloroethene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Trichlorofluoromethane
<0.012
mg/Kg - dry
0.012
1
07/19/23 13:33
TBL
V35531
1,2,3-Trichloropropane
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Qualifiers/ * Outside QC Limit
DF Dilution Factor
Definitions MQL Method
Quantitation Limit
Page 9 of 52

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Report Date : 07/25/2023
Received : 07/18/2023
Lab No : 90011 Matrix: Solids
Sample ID: EX-16-B Sampled: 7/17/2023 10:40
Analytical Method: 8260D Prep Batch(es): V35530 07/19/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
1,3,5-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
Vinyl Acetate
<0.012
mg/Kg - dry
0.012
1
07/19/23 13:33
TBL
V35531
Vinyl Chloride
<0.012
mg/Kg - dry
0.012
1
07/19/23 13:33
TBL
V35531
o-Xylene
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
TBL
V35531
m,p-Xylene
<0.012
mg/Kg - dry
0.012
1
07/19/23 13:33
TBL
V35531
Xylene (Total)
<0.006
mg/Kg - dry
0.006
1
07/19/23 13:33
V35531
Surrogate:4-Bromofluorobenzene
97.7
Limits:70-130%
1 07/19/23 13:33 TBL
V35531
Surrogate: Dibromofluoromethane
98.8
Limits: 84-123%
1 07/19/23 13:33 TBL
V35531
Surrogate: Toluene-d8
97.3
Limits: 76-129%
1 07/19/23 13:33 TBL
V35531
Analytical Method: 8270E
Prep Batch(es):
V35554 07/20/23 11:20
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Acenaphthylene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Aniline
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Anthracene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Benzo(a)anthracene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Benzo(a)pyrene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Benzo(b)fluoranthene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Benzo(g,h,i)perylene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 10 of 52

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 07/25/2023
2923 South Tryon St. Ste 100 Information : Received : 07/18/2023
Charlotte , NC 28203
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Lab No : 90011
Matrix: Solids
Sample ID: EX-16-B
Sampled:
7/17/2023 10:40
Analytical Method: 8270E
Prep Batch(es):
V35554
07/20/23 11:20
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzo(k)fluoranthene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Benzoic Acid
<2.49
mg/Kg - dry
2.49
1
07/24/23 18:05
AMP
V35586
Benzyl alcohol
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Bis(2-Chloroethoxy)methane
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Bis(2-Chloroethyl)ether
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Bis(2-Chloroisopropyl)ether
<0.411
mg/Kg - dry
0.411
1
07/24/23 18:05
AMP
V35586
Bis(2-ethylhexyl)phthalate
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
4-13romophenyl phenyl ether
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Butyl benzyl phthalate
<0.411
mg/Kg - dry
0.411
1
07/24/23 18:05
AMP
V35586
4-Chloro-3-methylphenol
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
4-Chloroaniline
<0.411
mg/Kg - dry
0.411
1
07/24/23 18:05
AMP
V35586
2-Chloronaphthalene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
2-Chlorophenol
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
4-Chlorophenyl phenyl ether
<1.25
mg/Kg - dry
1.25
1
07/24/23 18:05
AMP
V35586
Chrysene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Dibenz(a,h)anthracene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Dibenzofuran
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
1,2-Dichlorobenzene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
1,3-Dichlorobenzene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
1,4-Dichlorobenzene
<0.411
mg/Kg - dry
0.411
1
07/24/23 18:05
AMP
V35586
3,3'-Dichlorobenzidine
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
2,4-Dichlorophenol
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 11 of 52

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 07/25/2023
2923 South Tryon St. Ste 100 Information : Received : 07/18/2023
Charlotte , NC 28203
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Lab No : 90011
Matrix: Solids
Sample ID: EX-16-B
Sampled:
7/17/2023 10:40
Analytical Method: 8270E
Prep Batch(es):
V35554
07/20/23 11:20
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Dimethyl phthalate
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
2,4-Dimethyl phenol
<0.411
mg/Kg - dry
0.411
1
07/24/23 18:05
AMP
V35586
Di-n-butyl phthalate
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
4,6-Dinitro-2-methylphenol
<1.87
mg/Kg - dry
1.87
1
07/24/23 18:05
AMP
V35586
2,4-Dinitrophenol
<1.87
mg/Kg - dry
1.87
1
07/24/23 18:05
AMP
V35586
2,4-Dinitrotoluene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
2,6-Dinitrotoluene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Di-n-Octyl Phthalate
<0.411
mg/Kg - dry
0.411
1
07/24/23 18:05
AMP
V35586
Fluoranthene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Fluorene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Hexachlorobenzene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Hexachlorobutadiene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Hexachlorocyclopentadiene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Hexachloroethane
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Indeno(1,2,3-cd)pyrene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Isophorone
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
1-Methylnaphthalene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
2-Methylnaphthalene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
2-Methylphenol
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
3&4 Methylphenol
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Naphthalene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05
AMP
V35586
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 12 of 52

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 07/25/2023
2923 South Tryon St. Ste 100 Information : Received : 07/18/2023
Charlotte , NC 28203
Report Number : 23-199-0028
REPORT OF ANAL YSIS
Lab No : 90011
Matrix: Solids
Sample ID: EX-16-B
Sampled: 7/17/2023
10:40
Analytical Method: 8270E
Prep Batch(es):
V35554 07/20/23 11:20
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
2-Nitroaniline
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05 AMP
V35586
3-Nitroaniline
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05 AMP
V35586
4-Nitroaniline
<0.411
mg/Kg - dry
0.411
1
07/24/23 18:05 AMP
V35586
Nitrobenzene
<0.411
mg/Kg - dry
0.411
1
07/24/23 18:05 AMP
V35586
2-Nitrophenol
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05 AMP
V35586
4-Nitrophenol
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05 AMP
V35586
N-Nitrosodimethylamine
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05 AMP
V35586
N-Nitrosodiphenylamine
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05 AMP
V35586
N-Nitroso-di-n-propylamine
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05 AMP
V35586
Pentachlorophenol
<1.25
mg/Kg - dry
1.25
1
07/24/23 18:05 AMP
V35586
Phenanthrene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05 AMP
V35586
Phenol
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05 AMP
V35586
Pyrene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05 AMP
V35586
Pyridine
<0.411
mg/Kg - dry
0.411
1
07/24/23 18:05 AMP
V35586
1,2,4-Trichlorobenzene
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05 AMP
V35586
2,4,5-Trichlorophenol
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05 AMP
V35586
2,4,6-Trichlorophenol
<0.822
mg/Kg - dry
0.822
1
07/24/23 18:05 AMP
V35586
Surrogate: Phenol-d5
46.1
Limits: 34-121%
1 07/24/23 18:05 AMP
8270E
Surrogate:2-Fluorobiphenyl
61.7
Limits:44-115%
1 07/24/23 18:05 AMP
V35586
Surrogate:2-Fluorophenol
51.8
Limits:35-115%
1 07/24/23 18:05 AMP
V35586
Surrogate: Nitrobenzene-d5
53.8
Limits: 37-122%
1 07/24/23 18:05 AMP
V35586
Surrogate:4-Terphenyl-d14
74.9
Limits:54-127%
1 07/24/23 18:05 AMP
V35586
Surrogate: 2,4,6-Tribromophenol
59.0
Limits:39-132%
1 07/24/23 18:05 AMP
V35586
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 13 of 52

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 07/25/2023
Received : 07/18/2023
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Lab No : 90011 Matrix: Solids
Sample ID: EX-16-B Sampled: 7/17/2023 10:40
Analytical Method: MADEP-EPH
Prep Method: MAEPH (Prep)
Test
Aliphatic C9-C18
Aliphatic C19-06
Aromatic C11-C22
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Analytical Method: MADEP-VPH
Prep Method: MAVPH (Prep)
Test
Prep Batch(es): V35553 07/20/23 09:30
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
<62.2 mg/Kg - dry
62.2 1
07/21/23 19:21 NDL
V35656
<62.2 mg/Kg - dry
62.2 1
07/21/23 19:21 NDL
V35656
<62.2 mg/Kg - dry
62.2 1
07/21/23 19:21 NDL
V35656
96.2
Limits:40-140%
1 07/21/23 19:21 NDL
MADEP-EPH
65.8
Limits:40-140%
1 07/21/23 19:21 NDL
MADEP-EPH
72.4
Limits:40-140%
1 07/21/23 19:21 NDL
MADEP-EPH
78.2
Limits:40-140%
1 07/21/23 19:21 NDL
V35656
Prep Batch(es):
V35509 07/19/23 08:00
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Aliphatic C5-C8 <10.1
Aliphatic C9-C12 <10.1
Aromatic C9-C10 <10.1
Surrogate: 2,5-Dibromotoluene (FID)
Surrogate: 2,5-Dibromotoluene (PID)
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
mg/Kg - dry
10.1
100 07/19/23 11:58 TBL
V35510
mg/Kg - dry
10.1
100 07/19/23 11:58 TBL
V35510
mg/Kg - dry
10.1
100 07/19/23 11:58 TBL
V35510
95.7
Limits: 70-130%
100 07/19/23 11:58 TBL
MADEP-VPH
111
Limits: 70-130%
100 07/19/23 11:58 TBL
MADEP-VPH
DF Dilution Factor
Page 14 of 52

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 07/25/2023
Received : 07/18/2023
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Lab No : 90012 Matrix: Solids
Sample ID: UST-2-G Sampled: 7/17/2023 10:25
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
22.3 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 07/19/2318:30 CNC SW-DRYWT
DF Dilution Factor
Page 15 of 52

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 07/25/2023
2923 South Tryon St. Ste 100 Information : Received : 07/18/2023
Charlotte , NC 28203
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Lab No : 90012
Matrix: Solids
Sample ID: UST-2-G
Sampled:
7/17/2023 10:25
Analytical Method: 8260D
Prep Batch(es):
V35530
07/19/23 08:00
Prep Method: 5035
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<0.025
mg/Kg - dry
0.025
1
07/19/23 14:00
TBL
V35531
Acrolein
<0.025
mg/Kg - dry
0.025
1
07/19/23 14:00
TBL
V35531
Acrylonitrile
<0.025
mg/Kg - dry
0.025
1
07/19/23 14:00
TBL
V35531
Benzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Bromobenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Bromochloromethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Bromodichloromethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Bromoform
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Bromomethane
<0.012
mg/Kg - dry
0.012
1
07/19/23 14:00
TBL
V35531
n-Butylbenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
sec -Butyl benzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
tert-Butyl benzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Carbon Disulfide
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Carbon Tetrachloride
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Chlorobenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Chlorodibromomethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Chloroethane
<0.012
mg/Kg - dry
0.012
1
07/19/23 14:00
TBL
V35531
Chloroform
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Chloromethane
<0.012
mg/Kg - dry
0.012
1
07/19/23 14:00
TBL
V35531
2-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
4-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Di -Isopropyl Ether (DIPE)
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 16 of 52

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 07/25/2023
2923 South Tryon St. Ste 100 Information : Received : 07/18/2023
Charlotte , NC 28203
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Lab No : 90012
Matrix: Solids
Sample ID: UST-2-G
Sampled:
7/17/2023 10:25
Analytical Method: 8260D
Prep Batch(es):
V35530
07/19/23 08:00
Prep Method: 5035
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,2-Dibromo-3-Chloropropane
<0.012
mg/Kg - dry
0.012
1
07/19/23 14:00
TBL
V35531
1,2-Dibromoethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Dibromomethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
1,2-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
1,3-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
1,4-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Dichlorodifluoromethane
<0.012
mg/Kg - dry
0.012
1
07/19/23 14:00
TBL
V35531
1,1-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
1,2-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
1,1-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
cis- 1,2-Dich loroethene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
trans-1,2-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
1,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
1,3-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
2,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
1,1-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
cis-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
trans-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Ethanol
<0.321
mg/Kg - dry
0.321
1
07/19/23 14:00
TBL
V35531
Ethylbenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Ethyl Tertiary Butyl Ether (ETBE)
<0.064
mg/Kg - dry
0.064
1
07/19/23 14:00
TBL
V35531
Hexachlorobutadiene
<0.012
mg/Kg - dry
0.012
1
07/19/23 14:00
TBL
V35531
Qualifiers/ * Outside QC Limit
DF Dilution Factor
Definitions MQL Method Quantitation Limit
Page 17 of 52

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 07/25/2023
2923 South Tryon St. Ste 100 Information : Received : 07/18/2023
Charlotte , NC 28203
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Lab No : 90012
Matrix: Solids
Sample ID: UST-2-G
Sampled:
7/17/2023 10:25
Analytical Method: 8260D
Prep Batch(es):
V35530
07/19/23 08:00
Prep Method: 5035
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
n-Hexane
<0.012
mg/Kg - dry
0.012
1
07/19/23 14:00
TBL
V35531
2-Hexanone
<0.025
mg/Kg - dry
0.025
1
07/19/23 14:00
TBL
V35531
Isopropyl benzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
4-Isopropyl toluene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Methyl Ethyl Ketone (MEK)
<0.025
mg/Kg - dry
0.025
1
07/19/23 14:00
TBL
V35531
Methyl tert-butyl ether (MTBE)
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
4-Methyl-2-Pentanone
<0.025
mg/Kg - dry
0.025
1
07/19/23 14:00
TBL
V35531
Methylene Chloride
<0.012
mg/Kg - dry
0.012
1
07/19/23 14:00
TBL
V35531
Naphthalene
<0.012
mg/Kg - dry
0.012
1
07/19/23 14:00
TBL
V35531
n-Propylbenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Styrene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
1,1,1,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
1,1,2,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Tetrachloroethene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Toluene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
1,2,3-Trichlorobenzene
<0.012
mg/Kg - dry
0.012
1
07/19/23 14:00
TBL
V35531
1,2,4-Trichlorobenzene
<0.012
mg/Kg - dry
0.012
1
07/19/23 14:00
TBL
V35531
1,1,1-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
1,1,2-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Trichloroethene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Trichlorofluoromethane
<0.012
mg/Kg - dry
0.012
1
07/19/23 14:00
TBL
V35531
1,2,3-Trichloropropane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Qualifiers/ * Outside QC Limit
DF Dilution Factor
Definitions MQL Method
Quantitation Limit
Page 18 of 52

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Report Date : 07/25/2023
Received : 07/18/2023
Lab No : 90012 Matrix: Solids
Sample ID: UST-2-G Sampled: 7/17/2023 10:25
Analytical Method: 8260D Prep Batch(es): V35530 07/19/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
1,3,5-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
Vinyl Acetate
<0.012
mg/Kg - dry
0.012
1
07/19/23 14:00
TBL
V35531
Vinyl Chloride
<0.012
mg/Kg - dry
0.012
1
07/19/23 14:00
TBL
V35531
o-Xylene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
TBL
V35531
m,p-Xylene
<0.012
mg/Kg - dry
0.012
1
07/19/23 14:00
TBL
V35531
Xylene (Total)
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:00
V35531
Surrogate:4-Bromofluorobenzene
97.9
Limits:70-130%
1 07/19/23 14:00 TBL
V35531
Surrogate: Dibromofluoromethane
99.1
Limits: 84-123%
1 07/19/23 14:00 TBL
V35531
Surrogate: Toluene-d8
96.0
Limits: 76-129%
1 07/19/23 14:00 TBL
V35531
Analytical Method: 8270E
Prep Batch(es):
V35554 07/20/23 11:20
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Acenaphthylene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Aniline
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Anthracene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Benzo(a)anthracene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Benzo(a)pyrene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Benzo(b)fluoranthene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Benzo(g,h,i)perylene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 19 of 52

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 07/25/2023
2923 South Tryon St. Ste 100 Information : Received : 07/18/2023
Charlotte , NC 28203
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Lab No : 90012
Matrix: Solids
Sample ID: UST-2-G
Sampled:
7/17/2023 10:25
Analytical Method: 8270E
Prep Batch(es):
V35554
07/20/23 11:20
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzo(k)fluoranthene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Benzoic Acid
<2.57
mg/Kg - dry
2.57
1
07/24/23 18:28
AMP
V35586
Benzyl alcohol
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Bis(2-Chloroethoxy)methane
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Bis(2-Chloroethyl)ether
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Bis(2-Chloroisopropyl)ether
<0.424
mg/Kg - dry
0.424
1
07/24/23 18:28
AMP
V35586
Bis(2-ethylhexyl)phthalate
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
4-13romophenyl phenyl ether
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Butyl benzyl phthalate
<0.424
mg/Kg - dry
0.424
1
07/24/23 18:28
AMP
V35586
4-Chloro-3-methylphenol
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
4-Chloroaniline
<0.424
mg/Kg - dry
0.424
1
07/24/23 18:28
AMP
V35586
2-Chloronaphthalene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
2-Chlorophenol
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
4-Chlorophenyl phenyl ether
<1.29
mg/Kg - dry
1.29
1
07/24/23 18:28
AMP
V35586
Chrysene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Dibenz(a,h)anthracene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Dibenzofuran
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
1,2-Dichlorobenzene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
1,3-Dichlorobenzene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
1,4-Dichlorobenzene
<0.424
mg/Kg - dry
0.424
1
07/24/23 18:28
AMP
V35586
3,3'-Dichlorobenzidine
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
2,4-Dichlorophenol
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 20 of 52

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 07/25/2023
2923 South Tryon St. Ste 100 Information : Received : 07/18/2023
Charlotte , NC 28203
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Lab No : 90012
Matrix: Solids
Sample ID: UST-2-G
Sampled:
7/17/2023 10:25
Analytical Method: 8270E
Prep Batch(es):
V35554
07/20/23 11:20
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Dimethyl phthalate
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
2,4-Dimethyl phenol
<0.424
mg/Kg - dry
0.424
1
07/24/23 18:28
AMP
V35586
Di-n-butyl phthalate
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
4,6-Dinitro-2-methylphenol
<1.93
mg/Kg - dry
1.93
1
07/24/23 18:28
AMP
V35586
2,4-Dinitrophenol
<1.93
mg/Kg - dry
1.93
1
07/24/23 18:28
AMP
V35586
2,4-Dinitrotoluene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
2,6-Dinitrotoluene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Di-n-Octyl Phthalate
<0.424
mg/Kg - dry
0.424
1
07/24/23 18:28
AMP
V35586
Fluoranthene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Fluorene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Hexachlorobenzene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Hexachlorobutadiene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Hexachlorocyclopentadiene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Hexachloroethane
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Indeno(1,2,3-cd)pyrene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Isophorone
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
1-Methylnaphthalene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
2-Methylnaphthalene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
2-Methylphenol
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
3&4 Methylphenol
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Naphthalene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28
AMP
V35586
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 21 of 52

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 07/25/2023
2923 South Tryon St. Ste 100 Information : Received : 07/18/2023
Charlotte , NC 28203
Report Number : 23-199-0028
REPORT OF ANAL YSIS
Lab No : 90012
Matrix: Solids
Sample ID: UST-2-G
Sampled: 7/17/2023
10:25
Analytical Method: 8270E
Prep Batch(es):
V35554 07/20/23 11:20
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
2-Nitroaniline
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28 AMP
V35586
3-Nitroaniline
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28 AMP
V35586
4-Nitroaniline
<0.424
mg/Kg - dry
0.424
1
07/24/23 18:28 AMP
V35586
Nitrobenzene
<0.424
mg/Kg - dry
0.424
1
07/24/23 18:28 AMP
V35586
2-Nitrophenol
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28 AMP
V35586
4-Nitrophenol
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28 AMP
V35586
N-Nitrosodimethylamine
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28 AMP
V35586
N-Nitrosodiphenylamine
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28 AMP
V35586
N-Nitroso-di-n-propylamine
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28 AMP
V35586
Pentachlorophenol
<1.29
mg/Kg - dry
1.29
1
07/24/23 18:28 AMP
V35586
Phenanthrene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28 AMP
V35586
Phenol
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28 AMP
V35586
Pyrene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28 AMP
V35586
Pyridine
<0.424
mg/Kg - dry
0.424
1
07/24/23 18:28 AMP
V35586
1,2,4-Trichlorobenzene
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28 AMP
V35586
2,4,5-Trichlorophenol
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28 AMP
V35586
2,4,6-Trichlorophenol
<0.849
mg/Kg - dry
0.849
1
07/24/23 18:28 AMP
V35586
Surrogate: Phenol-d5
42.9
Limits: 34-121%
1 07/24/23 18:28 AMP
8270E
Surrogate:2-Fluorobiphenyl
57.4
Limits:44-115%
1 07/24/23 18:28 AMP
V35586
Surrogate:2-Fluorophenol
46.8
Limits:35-115%
1 07/24/23 18:28 AMP
V35586
Surrogate: Nitrobenzene-d5
50.0
Limits: 37-122%
1 07/24/23 18:28 AMP
V35586
Surrogate:4-Terphenyl-d14
70.1
Limits:54-127%
1 07/24/23 18:28 AMP
V35586
Surrogate: 2,4,6-Tribromophenol
62.2
Limits:39-132%
1 07/24/23 18:28 AMP
V35586
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 22 of 52

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 07/25/2023
Received : 07/18/2023
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Lab No : 90012 Matrix: Solids
Sample ID: UST-2-G Sampled: 7/17/2023 10:25
Analytical Method: MADEP-EPH
Prep Method: MAEPH (Prep)
Test
Aliphatic C9-C18
Aliphatic C19-C36
Aromatic C11-C22
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Analytical Method: MADEP-VPH
Prep Method: MAVPH (Prep)
Test
Prep Batch(es): V35553 07/20/23 09:30
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
91.9 mg/Kg - dry
64.6 1
07/21/23 19:57 NDL
V35656
<64.6 mg/Kg - dry
64.6 1
07/21/23 19:57 NDL
V35656
<64.6 mg/Kg - dry
64.6 1
07/21/23 19:57 NDL
V35656
86.8
Limits:40-140%
1 07/21/23 19:57 NDL
MADEP-EPH
61.4
Limits:40-140%
1 07/21/23 19:57 NDL
MADEP-EPH
82.6
Limits:40-140%
1 07/21/23 19:57 NDL
MADEP-EPH
87.1
Limits:40-140%
1 07/21/23 19:57 NDL
V35656
Prep Batch(es):
V35509 07/19/23 08:00
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Aliphatic C5-C8 <12.8
Aliphatic C9-C12 <12.8
Aromatic C9-C10 <12.8
Surrogate: 2,5-Dibromotoluene (FID)
Surrogate: 2,5-Dibromotoluene (PID)
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
mg/Kg - dry
12.8
100 07/19/23 12:21 TBL
V35510
mg/Kg - dry
12.8
100 07/19/23 12:21 TBL
V35510
mg/Kg - dry
12.8
100 07/19/23 12:21 TBL
V35510
92.7
Limits: 70-130%
100 07/19/23 12:21 TBL
MADEP-VPH
106
Limits: 70-130%
100 07/19/23 12:21 TBL
MADEP-VPH
DF Dilution Factor
Page 23 of 52

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 07/25/2023
Received : 07/18/2023
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Lab No : 90013 Matrix: Solids
Sample ID: UST-2-111 Sampled: 7/17/2023 10:50
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
23.4 %
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
1 07/19/2318:30 CNC SW-DRYWT
DF Dilution Factor
Page 24 of 52

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 07/25/2023
2923 South Tryon St. Ste 100 Information : Received : 07/18/2023
Charlotte , NC 28203
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Lab No : 90013
Matrix: Solids
Sample ID: UST-2-111
Sampled:
7/17/2023 10:50
Analytical Method: 8260D
Prep Batch(es):
V35530
07/19/23 08:00
Prep Method: 5035
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<0.026
mg/Kg - dry
0.026
1
07/19/23 14:27
TBL
V35531
Acrolein
<0.026
mg/Kg - dry
0.026
1
07/19/23 14:27
TBL
V35531
Acrylonitrile
<0.026
mg/Kg - dry
0.026
1
07/19/23 14:27
TBL
V35531
Benzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Bromobenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Bromochloromethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Bromodichloromethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Bromoform
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Bromomethane
<0.013
mg/Kg - dry
0.013
1
07/19/23 14:27
TBL
V35531
n-Butylbenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
sec -Butyl benzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
tert-Butyl benzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Carbon Disulfide
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Carbon Tetrachloride
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Chlorobenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Chlorodibromomethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Chloroethane
<0.013
mg/Kg - dry
0.013
1
07/19/23 14:27
TBL
V35531
Chloroform
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Chloromethane
<0.013
mg/Kg - dry
0.013
1
07/19/23 14:27
TBL
V35531
2-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
4-Chlorotoluene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Di -Isopropyl Ether (DIPE)
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 25 of 52

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 07/25/2023
2923 South Tryon St. Ste 100 Information : Received : 07/18/2023
Charlotte , NC 28203
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Lab No : 90013
Matrix: Solids
Sample ID: UST-2-111
Sampled:
7/17/2023 10:50
Analytical Method: 8260D
Prep Batch(es):
V35530
07/19/23 08:00
Prep Method: 5035
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,2-Dibromo-3-Chloropropane
<0.013
mg/Kg - dry
0.013
1
07/19/23 14:27
TBL
V35531
1,2-Dibromoethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Dibromomethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
1,2-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
1,3-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
1,4-Dichlorobenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Dichlorodifluoromethane
<0.013
mg/Kg - dry
0.013
1
07/19/23 14:27
TBL
V35531
1,1-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
1,2-Dichloroethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
1,1-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
cis- 1,2-Dich loroethene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
trans-1,2-Dichloroethene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
1,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
1,3-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
2,2-Dichloropropane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
1,1-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
cis-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
trans-1,3-Dichloropropene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Ethanol
<0.326
mg/Kg - dry
0.326
1
07/19/23 14:27
TBL
V35531
Ethylbenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Ethyl Tertiary Butyl Ether (ETBE)
<0.065
mg/Kg - dry
0.065
1
07/19/23 14:27
TBL
V35531
Hexachlorobutadiene
<0.013
mg/Kg - dry
0.013
1
07/19/23 14:27
TBL
V35531
Qualifiers/ * Outside QC Limit
DF Dilution Factor
Definitions MQL Method Quantitation Limit
Page 26 of 52

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 07/25/2023
2923 South Tryon St. Ste 100 Information : Received : 07/18/2023
Charlotte , NC 28203
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Lab No : 90013
Matrix: Solids
Sample ID: UST-2-111
Sampled:
7/17/2023 10:50
Analytical Method: 8260D
Prep Batch(es):
V35530
07/19/23 08:00
Prep Method: 5035
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
n-Hexane
<0.013
mg/Kg - dry
0.013
1
07/19/23 14:27
TBL
V35531
2-Hexanone
<0.026
mg/Kg - dry
0.026
1
07/19/23 14:27
TBL
V35531
Isopropyl benzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
4-Isopropyl toluene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Methyl Ethyl Ketone (MEK)
<0.026
mg/Kg - dry
0.026
1
07/19/23 14:27
TBL
V35531
Methyl tert-butyl ether (MTBE)
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
4-Methyl-2-Pentanone
<0.026
mg/Kg - dry
0.026
1
07/19/23 14:27
TBL
V35531
Methylene Chloride
<0.013
mg/Kg - dry
0.013
1
07/19/23 14:27
TBL
V35531
Naphthalene
<0.013
mg/Kg - dry
0.013
1
07/19/23 14:27
TBL
V35531
n-Propylbenzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Styrene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
1,1,1,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
1,1,2,2-Tetrachloroethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Tetrachloroethene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Toluene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
1,2,3-Trichlorobenzene
<0.013
mg/Kg - dry
0.013
1
07/19/23 14:27
TBL
V35531
1,2,4-Trichlorobenzene
<0.013
mg/Kg - dry
0.013
1
07/19/23 14:27
TBL
V35531
1,1,1-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
1,1,2-Trichloroethane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Trichloroethene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Trichlorofluoromethane
<0.013
mg/Kg - dry
0.013
1
07/19/23 14:27
TBL
V35531
1,2,3-Trichloropropane
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Qualifiers/ * Outside QC Limit
DF Dilution Factor
Definitions MQL Method
Quantitation Limit
Page 27 of 52

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Report Date : 07/25/2023
Received : 07/18/2023
Lab No : 90013 Matrix: Solids
Sample ID: UST-2-111 Sampled: 7/17/2023 10:50
Analytical Method: 8260D Prep Batch(es): V35530 07/19/23 08:00
Prep Method: 5035
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
1,3,5-Trimethyl benzene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
Vinyl Acetate
<0.013
mg/Kg - dry
0.013
1
07/19/23 14:27
TBL
V35531
Vinyl Chloride
<0.013
mg/Kg - dry
0.013
1
07/19/23 14:27
TBL
V35531
o-Xylene
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
TBL
V35531
m,p-Xylene
<0.013
mg/Kg - dry
0.013
1
07/19/23 14:27
TBL
V35531
Xylene (Total)
<0.006
mg/Kg - dry
0.006
1
07/19/23 14:27
V35531
Surrogate:4-Bromofluorobenzene
100
Limits:70-130%
1 07/19/23 14:27 TBL
V35531
Surrogate: Dibromofluoromethane
102
Limits: 84-123%
1 07/19/23 14:27 TBL
V35531
Surrogate: Toluene-d8
95.6
Limits: 76-129%
1 07/19/23 14:27 TBL
V35531
Analytical Method: 8270E
Prep Batch(es):
V35554 07/20/23 11:20
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Acenaphthylene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Aniline
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Anthracene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Benzo(a)anthracene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Benzo(a)pyrene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Benzo(b)fluoranthene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Benzo(g,h,i)perylene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 28 of 52

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 07/25/2023
2923 South Tryon St. Ste 100 Information : Received : 07/18/2023
Charlotte , NC 28203
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Lab No : 90013
Matrix: Solids
Sample ID: UST-2-111
Sampled:
7/17/2023 10:50
Analytical Method: 8270E
Prep Batch(es):
V35554
07/20/23 11:20
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzo(k)fluoranthene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Benzoic Acid
<2.61
mg/Kg - dry
2.61
1
07/24/23 16:56
AMP
V35586
Benzyl alcohol
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Bis(2-Chloroethoxy)methane
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Bis(2-Chloroethyl)ether
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Bis(2-Chloroisopropyl)ether
<0.430
mg/Kg - dry
0.430
1
07/24/23 16:56
AMP
V35586
Bis(2-ethylhexyl)phthalate
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
4-13romophenyl phenyl ether
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Butyl benzyl phthalate
<0.430
mg/Kg - dry
0.430
1
07/24/23 16:56
AMP
V35586
4-Chloro-3-methylphenol
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
4-Chloroaniline
<0.430
mg/Kg - dry
0.430
1
07/24/23 16:56
AMP
V35586
2-Chloronaphthalene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
2-Chlorophenol
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
4-Chlorophenyl phenyl ether
<1.31
mg/Kg - dry
1.31
1
07/24/23 16:56
AMP
V35586
Chrysene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Dibenz(a,h)anthracene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Dibenzofuran
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
1,2-Dichlorobenzene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
1,3-Dichlorobenzene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
1,4-Dichlorobenzene
<0.430
mg/Kg - dry
0.430
1
07/24/23 16:56
AMP
V35586
3,3'-Dichlorobenzidine
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
2,4-Dichlorophenol
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 29 of 52

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 07/25/2023
2923 South Tryon St. Ste 100 Information : Received : 07/18/2023
Charlotte , NC 28203
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Lab No : 90013
Matrix: Solids
Sample ID: UST-2-111
Sampled:
7/17/2023 10:50
Analytical Method: 8270E
Prep Batch(es):
V35554
07/20/23 11:20
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Dimethyl phthalate
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
2,4-Dimethyl phenol
<0.430
mg/Kg - dry
0.430
1
07/24/23 16:56
AMP
V35586
Di-n-butyl phthalate
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
4,6-Dinitro-2-methylphenol
<1.96
mg/Kg - dry
1.96
1
07/24/23 16:56
AMP
V35586
2,4-Dinitrophenol
<1.96
mg/Kg - dry
1.96
1
07/24/23 16:56
AMP
V35586
2,4-Dinitrotoluene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
2,6-Dinitrotoluene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Di-n-Octyl Phthalate
<0.430
mg/Kg - dry
0.430
1
07/24/23 16:56
AMP
V35586
Fluoranthene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Fluorene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Hexachlorobenzene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Hexachlorobutadiene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Hexachlorocyclopentadiene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Hexachloroethane
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Indeno(1,2,3-cd)pyrene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Isophorone
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
1-Methylnaphthalene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
2-Methylnaphthalene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
2-Methylphenol
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
3&4 Methylphenol
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Naphthalene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56
AMP
V35586
Qualifiers/ *
Outside QC Limit
DF Dilution Factor
Definitions MQL
Method Quantitation Limit
Page 30 of 52

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project TPM-001
Steve Libbey Report Date : 07/25/2023
2923 South Tryon St. Ste 100 Information : Received : 07/18/2023
Charlotte , NC 28203
Report Number : 23-199-0028
REPORT OF ANAL YSIS
Lab No : 90013
Matrix: Solids
Sample ID: UST-2-111
Sampled: 7/17/2023
10:50
Analytical Method: 8270E
Prep Batch(es):
V35554 07/20/23 11:20
Prep Method: 3546
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
2-Nitroaniline
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56 AMP
V35586
3-Nitroaniline
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56 AMP
V35586
4-Nitroaniline
<0.430
mg/Kg - dry
0.430
1
07/24/23 16:56 AMP
V35586
Nitrobenzene
<0.430
mg/Kg - dry
0.430
1
07/24/23 16:56 AMP
V35586
2-Nitrophenol
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56 AMP
V35586
4-Nitrophenol
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56 AMP
V35586
N-Nitrosodimethylamine
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56 AMP
V35586
N-Nitrosodiphenylamine
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56 AMP
V35586
N-Nitroso-di-n-propylamine
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56 AMP
V35586
Pentachlorophenol
<1.31
mg/Kg - dry
1.31
1
07/24/23 16:56 AMP
V35586
Phenanthrene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56 AMP
V35586
Phenol
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56 AMP
V35586
Pyrene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56 AMP
V35586
Pyridine
<0.430
mg/Kg - dry
0.430
1
07/24/23 16:56 AMP
V35586
1,2,4-Trichlorobenzene
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56 AMP
V35586
2,4,5-Trichlorophenol
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56 AMP
V35586
2,4,6-Trichlorophenol
<0.861
mg/Kg - dry
0.861
1
07/24/23 16:56 AMP
V35586
Surrogate: Phenol-d5
48.0
Limits: 34-121%
1 07/24/23 16:56 AMP
8270E
Surrogate:2-Fluorobiphenyl
60.2
Limits:44-115%
1 07/24/23 16:56 AMP
V35586
Surrogate:2-Fluorophenol
53.5
Limits:35-115%
1 07/24/23 16:56 AMP
V35586
Surrogate: Nitrobenzene-d5
53.4
Limits: 37-122%
1 07/24/23 16:56 AMP
V35586
Surrogate:4-Terphenyl-d14
71.7
Limits:54-127%
1 07/24/23 16:56 AMP
V35586
Surrogate: 2,4,6-Tribromophenol
65.2
Limits:39-132%
1 07/24/23 16:56 AMP
V35586
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions MQL Method Quantitation Limit
Page 31 of 52

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 07/25/2023
Received : 07/18/2023
Report Number : 23-199-0028 REPOR T OF A NA L YSIS
Lab No : 90013 Matrix: Solids
Sample ID: UST-2-111 Sampled: 7/17/2023 10:50
Analytical Method: MADEP-EPH
Prep Method: MAEPH (Prep)
Test
Aliphatic C9-C18
Aliphatic C19-C36
Aromatic C11-C22
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Analytical Method: MADEP-VPH
Prep Method: MAVPH (Prep)
Test
Prep Batch(es): V35553 07/20/23 09:30
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
<65.1 mg/Kg - dry
65.1 1
07/21/23 20:34 NDL
V35656
<65.1 mg/Kg - dry
65.1 1
07/21/23 20:34 NDL
V35656
<65.1 mg/Kg - dry
65.1 1
07/21/23 20:34 NDL
V35656
90.7
Limits: 40-140%
1 07/21/23 20:34 NDL
MADEP-EPH
67.9
Limits: 40-140%
1 07/21/23 20:34 NDL
MADEP-EPH
79.9
Limits: 40-140%
1 07/21/23 20:34 NDL
MADEP-EPH
87.5
Limits: 40-140%
1 07/21/23 20:34 NDL
V35656
Prep Batch(es):
V35509 07/19/23 08:00
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Aliphatic C5-C8 <16.8
Aliphatic C9-C12 <16.8
Aromatic C9-C10 <16.8
Surrogate: 2,5-Dibromotoluene (FID)
Surrogate: 2,5-Dibromotoluene (PID)
Qualifiers/ * Outside QC Limit
Definitions MQL Method Quantitation Limit
mg/Kg - dry
16.8
100 07/19/23 12:45 TBL
V35510
mg/Kg - dry
16.8
100 07/19/23 12:45 TBL
V35510
mg/Kg - dry
16.8
100 07/19/23 12:45 TBL
V35510
106
Limits: 70-130%
100 07/19/23 12:45 TBL
MADEP-VPH
130 *
Limits: 70-130%
100 07/19/23 12:45 TBL
MADEP-VPH
DF Dilution Factor
Page 32 of 52

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-199-0028
QC Prep: V35530
QC Prep Batch Method: 5035
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Lab Reagent Blank LRB-V35530
Associated Lab Samples: 90011, 90012, 90013
QC Analytical Batch(es): V35531
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Matrix: SOL
Blank MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Acetone
mg/Kg
<0.020
0.020
07/19/23 10:50
Acrolein
mg/Kg
<0.020
0.020
07/19/23 10:50
Acrylonitrile
mg/Kg
<0.020
0.020
07/19/23 10:50
Benzene
mg/Kg
<0.005
0.005
07/19/23 10:50
Bromobenzene
mg/Kg
<0.005
0.005
07/19/23 10:50
Bromochloromethane
mg/Kg
<0.005
0.005
07/19/23 10:50
Bromodichloromethane
mg/Kg
<0.005
0.005
07/19/23 10:50
Bromoform
mg/Kg
<0.005
0.005
07/19/23 10:50
Bromomethane
mg/Kg
<0.010
0.010
07/19/23 10:50
n-Butylbenzene
mg/Kg
<0.005
0.005
07/19/23 10:50
sec -Butyl benzene
mg/Kg
<0.005
0.005
07/19/23 10:50
tert-Butyl benzene
mg/Kg
<0.005
0.005
07/19/23 10:50
Carbon Disulfide
mg/Kg
<0.005
0.005
07/19/23 10:50
Carbon Tetrachloride
mg/Kg
<0.005
0.005
07/19/23 10:50
Chlorobenzene
mg/Kg
<0.005
0.005
07/19/23 10:50
Chlorodibromomethane
mg/Kg
<0.005
0.005
07/19/23 10:50
Chloroethane
mg/Kg
<0.010
0.010
07/19/23 10:50
Chloroform
mg/Kg
<0.005
0.005
07/19/23 10:50
Chloromethane
mg/Kg
<0.010
0.010
07/19/23 10:50
2-Chlorotoluene
mg/Kg
<0.005
0.005
07/19/23 10:50
4-Chlorotoluene
mg/Kg
<0.005
0.005
07/19/23 10:50
Di -Isopropyl Ether (DIPE)
mg/Kg
<0.005
0.005
07/19/23 10:50
1,2-Dibromo-3-Chloropropane
mg/Kg
<0.010
0.010
07/19/23 10:50
1,2-Dibromoethane
mg/Kg
<0.005
0.005
07/19/23 10:50
Dibromomethane
mg/Kg
<0.005
0.005
07/19/23 10:50
1,2-Dichlorobenzene
mg/Kg
<0.005
0.005
07/19/23 10:50
1,3-Dichlorobenzene
mg/Kg
<0.005
0.005
07/19/23 10:50
Date: 07/25/2023 10:35 AM
Page 1 of 18
Page 33 of 52

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-199-0028
QC Prep: V35530
QC Prep Batch Method: 5035
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Lab Reagent Blank LRB-V35530
Associated Lab Samples: 90011, 90012, 90013
QC Analytical Batch(es): V35531
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Matrix: SOL
Blank MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
1,4-Dichlorobenzene
mg/Kg
<0.005
0.005
07/19/23 10:50
Dichlorodifluoromethane
mg/Kg
<0.010
0.010
07/19/23 10:50
1,1-Dichloroethane
mg/Kg
<0.005
0.005
07/19/23 10:50
1,2-Dichloroethane
mg/Kg
<0.005
0.005
07/19/23 10:50
1,1-Dichloroethene
mg/Kg
<0.005
0.005
07/19/23 10:50
cis-1,2-Dichloroethene
mg/Kg
<0.005
0.005
07/19/23 10:50
trans-1,2-Dichloroethene
mg/Kg
<0.005
0.005
07/19/23 10:50
1,2-Dichloropropane
mg/Kg
<0.005
0.005
07/19/23 10:50
1,3-Dichloropropane
mg/Kg
<0.005
0.005
07/19/23 10:50
2,2-Dichloropropane
mg/Kg
<0.005
0.005
07/19/23 10:50
1,1-Dichloropropene
mg/Kg
<0.005
0.005
07/19/23 10:50
cis-1,3-Dichloropropene
mg/Kg
<0.005
0.005
07/19/23 10:50
trans-1,3-Dichloropropene
mg/Kg
<0.005
0.005
07/19/23 10:50
Ethanol
mg/Kg
<0.250
0.250
07/19/23 10:50
Ethylbenzene
mg/Kg
<0.005
0.005
07/19/23 10:50
Ethyl Tertiary Butyl Ether (ETBE)
mg/Kg
<0.050
0.050
07/19/23 10:50
Hexachlorobutadiene
mg/Kg
<0.010
0.010
07/19/23 10:50
n-Hexane
mg/Kg
<0.010
0.010
07/19/23 10:50
2-Hexanone
mg/Kg
<0.020
0.020
07/19/23 10:50
Isopropyl benzene
mg/Kg
<0.005
0.005
07/19/23 10:50
4-Isopropyl toluene
mg/Kg
<0.005
0.005
07/19/23 10:50
Methyl Ethyl Ketone (MEK)
mg/Kg
<0.020
0.020
07/19/23 10:50
Methyl tert-butyl ether (MTBE)
mg/Kg
<0.005
0.005
07/19/23 10:50
4-Methyl-2-Pentanone
mg/Kg
<0.020
0.020
07/19/23 10:50
Methylene Chloride
mg/Kg
<0.010
0.010
07/19/23 10:50
Naphthalene
mg/Kg
<0.010
0.010
07/19/23 10:50
n-Propylbenzene
mg/Kg
<0.005
0.005
07/19/23 10:50
Date: 07/25/2023 10:35 AM
Page 2 of 18
Page 34 of 52

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-199-0028
QC Prep:
V35530
QC Analytical Batch(es): V35531
QC Prep Batch Method:
5035
Analysis Method:
8260D
Analysis Description:
Volatile Organic
Compounds - GC/MS
Lab Reagent Blank
LRB-V35530
Matrix: SOL
Associated Lab Samples:
90011, 90012, 90013
Blank
MQL
Analyzed
% % Rec
Parameter
Units
Result
Recovery Limits
Styrene
mg/Kg
<0.005
0.005
07/19/23 10:50
1,1,1,2-Tetrachloroethane
mg/Kg
<0.005
0.005
07/19/23 10:50
1,1,2,2-Tetrachloroethane
mg/Kg
<0.005
0.005
07/19/23 10:50
Tetrachloroethene
mg/Kg
<0.005
0.005
07/19/23 10:50
Toluene
mg/Kg
<0.005
0.005
07/19/23 10:50
1,2,3-Trichlorobenzene
mg/Kg
<0.010
0.010
07/19/23 10:50
1,2,4-Trichlorobenzene
mg/Kg
<0.010
0.010
07/19/23 10:50
1,1,1-Trichloroethane
mg/Kg
<0.005
0.005
07/19/23 10:50
1,1,2-Trichloroethane
mg/Kg
<0.005
0.005
07/19/23 10:50
Trichloroethene
mg/Kg
<0.005
0.005
07/19/23 10:50
Trichlorofluoromethane
mg/Kg
<0.010
0.010
07/19/23 10:50
1,2,3-Trichloropropane
mg/Kg
<0.005
0.005
07/19/23 10:50
1,2,4-Trimethyl benzene
mg/Kg
<0.005
0.005
07/19/23 10:50
1,3,5-Trimethyl benzene
mg/Kg
<0.005
0.005
07/19/23 10:50
Vinyl Acetate
mg/Kg
<0.010
0.010
07/19/23 10:50
Vinyl Chloride
mg/Kg
<0.010
0.010
07/19/23 10:50
o-Xylene
mg/Kg
<0.005
0.005
07/19/23 10:50
m,p-Xylene
mg/Kg
<0.010
0.010
07/19/23 10:50
4-Bromofluorobenzene (S)
07/19/23 10:50
98.0 70-130
Dibromofluoromethane (S)
07/19/23 10:50
98.0 84-123
Toluene-d8 (S)
07/19/23 10:50
97.6 76-129
Laboratory Control Sample & LCSD LCS-V35530 LCSD-V35530
Spike LCS LCSD LCS LCSD % Rec
Parameter Units Conc. Result Result %Rec % Rec Limits RPD Max
RPD
Acetone mg/Kg 0.100 0.103 0.095 103 95.5 29-198
7.5 20
Date: 07/25/2023 10:35 AM
Page 35 of 52
Page 3 of 18

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-199-0028
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V35530 QC Analytical Batch(es): V35531
QC Prep Batch Method: 5035 Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V35530 LCSD-V35530
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
Acrolein
mg/Kg
0.100
0.111
0.109
111
109
70-130
1.8
20
Acrylonitrile
mg/Kg
0.100
0.114
0.109
114
109
65-134
4.4
20
Benzene
mg/Kg
0.050
0.051
0.049
102
98.8
74-127
3.1
20
Bromobenzene
mg/Kg
0.050
0.047
0.045
94.6
91.8
73-125
3.0
20
Bromochloromethane
mg/Kg
0.050
0.052
0.050
105
101
72-134
4.2
20
Bromodichloromethane
mg/Kg
0.050
0.051
0.049
103
99.8
75-122
2.7
20
Bromoform
mg/Kg
0.050
0.050
0.050
102
102
66-135
0.0
20
Bromomethane
mg/Kg
0.050
0.058
0.053
117
107
20-180
8.7
20
n-Butylbenzene
mg/Kg
0.050
0.048
0.045
96.8
91.4
65-135
5.7
20
sec -Butyl benzene
mg/Kg
0.050
0.047
0.044
94.6
89.2
66-131
5.8
20
tert-Butyl benzene
mg/Kg
0.050
0.046
0.043
92.2
86.4
67-132
6.4
20
Carbon Disulfide
mg/Kg
0.050
0.050
0.046
100
93.8
61-129
6.7
20
Carbon Tetrachloride
mg/Kg
0.050
0.048
0.044
96.4
89.4
64-143
7.5
20
Chlorobenzene
mg/Kg
0.050
0.049
0.048
99.4
96.8
74-118
2.6
20
Chlorodibromomethane
mg/Kg
0.050
0.050
0.049
101
99.2
73-122
1.6
20
Chloroethane
mg/Kg
0.050
0.058
0.053
116
108
33-149
7.5
20
Chloroform
mg/Kg
0.050
0.050
0.048
101
97.6
73-127
3.6
20
Chloromethane
mg/Kg
0.050
0.049
0.044
98.0
88.4
45-143
10.3
20
2-Chlorotoluene
mg/Kg
0.050
0.046
0.044
93.4
88.0
67-124
5.9
20
4-Chlorotoluene
mg/Kg
0.050
0.046
0.044
93.4
88.0
71-126
5.9
20
Di -Isopropyl Ether (DIPE)
mg/Kg
0.050
0.050
0.048
101
97.6
59-159
3.4
20
1,2-Dibromo-3-Chloropropane
mg/Kg
0.050
0.051
0.048
103
97.6
55-157
5.1
20
1,2-Dibromoethane
mg/Kg
0.050
0.052
0.050
104
102
70-132
2.3
20
Dibromomethane
mg/Kg
0.050
0.052
0.051
105
103
74-133
2.3
20
1,2-Dichlorobenzene
mg/Kg
0.050
0.048
0.046
96.0
92.4
72-123
3.8
20
1,3-Dichlorobenzene
mg/Kg
0.050
0.047
0.045
94.8
91.8
71-120
3.2
20
Date: 07/25/2023 10:35 AM Page 4 of 18
Page 36 of 52

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-199-0028
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V35530 QC Analytical Batch(es): V35531
QC Prep Batch Method: 5035 Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V35530 LCSD-V35530
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
1,4-Dichlorobenzene
mg/Kg
0.050
0.046
0.045
93.0
91.6
71-123
1.5
20
Dichlorodifluoromethane
mg/Kg
0.050
0.041
0.038
83.6
76.6
26-146
8.7
20
1,1-Dichloroethane
mg/Kg
0.050
0.050
0.048
101
96.0
74-127
4.6
20
1,2-Dichloroethane
mg/Kg
0.050
0.049
0.048
98.4
97.2
68-128
1.2
20
1,1-Dichloroethene
mg/Kg
0.050
0.049
0.046
98.8
93.6
67-149
5.4
20
cis-1,2-Dichloroethene
mg/Kg
0.050
0.050
0.048
101
97.2
76-134
4.0
20
trans-1,2-Dichloroethene
mg/Kg
0.050
0.050
0.048
102
96.8
73-132
4.8
20
1,2-Dichloropropane
mg/Kg
0.050
0.050
0.050
102
102
73-130
0.1
20
1,3-Dichloropropane
mg/Kg
0.050
0.050
0.049
100
99.2
75-124
1.0
20
2,2-Dichloropropane
mg/Kg
0.050
0.049
0.046
98.6
93.6
50-142
5.2
20
1,1-Dichloropropene
mg/Kg
0.050
0.050
0.047
101
94.0
71-130
7.3
20
cis-1,3-Dichloropropene
mg/Kg
0.050
0.052
0.050
104
100
71-125
3.7
20
trans-1,3-Dichloropropene
mg/Kg
0.050
0.051
0.051
104
103
68-123
0.5
20
Ethanol
mg/Kg
1.25
1.47
1.38
118
110
70-130
6.3
20
Ethylbenzene
mg/Kg
0.050
0.048
0.046
97.0
92.4
74-128
4.8
20
Ethyl Tertiary Butyl Ether (ETBE)
mg/Kg
0.100
0.101
0.098
101
98.2
70-130
2.8
20
Hexachlorobutadiene
mg/Kg
0.050
0.046
0.043
93.2
87.8
64-125
5.9
20
n-Hexane
mg/Kg
0.050
0.051
0.048
104
97.2
70-130
6.5
20
2-Hexanone
mg/Kg
0.050
0.055
0.052
112
105
61-157
5.9
20
Isopropyl benzene
mg/Kg
0.050
0.045
0.044
91.8
88.6
68-126
3.5
20
4-Isopropyl toluene
mg/Kg
0.050
0.048
0.044
96.0
89.6
68-129
6.8
20
Methyl Ethyl Ketone (MEK)
mg/Kg
0.050
0.046
0.042
92.2
85.2
63-149
7.8
20
Methyl tert-butyl ether (MTBE)
mg/Kg
0.050
0.051
0.049
103
99.6
70-130
3.3
20
4-Methyl-2-Pentanone
mg/Kg
0.050
0.055
0.053
111
107
57-162
4.2
20
Methylene Chloride
mg/Kg
0.050
0.051
0.049
102
99.6
74-129
2.7
20
Naphthalene
mg/Kg
0.050
0.048
0.046
97.2
93.2
57-157
4.2
20
Date: 07/25/2023 10:35 AM Page 5 of 18
Page 37 of 52

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
Hart & Hickman (Charlotte)
TPM-001
23-199-0028
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V35530 QC Analytical Batch(es): V35531
QC Prep Batch Method: 5035 Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V35530 LCSD-V35530
Spike LCS LCSD LCS LCSD % Rec
Parameter Units Conc. Result Result %Rec % Rec Limits RPD
n-Propylbenzene
mg/Kg
0.050
0.047
0.044
95.0
89.6
67-130
5.8
Styrene
mg/Kg
0.050
0.050
0.048
101
97.8
77-121
3.2
1,1,1,2-Tetrachloroethane
mg/Kg
0.050
0.049
0.048
99.0
97.0
72-115
2.0
1,1,2,2-Tetrachloroethane
mg/Kg
0.050
0.048
0.047
97.6
95.2
56-126
2.4
Tetrachloroethene
mg/Kg
0.050
0.051
0.048
103
96.8
68-130
6.2
Toluene
mg/Kg
0.050
0.049
0.048
99.8
96.6
71-129
3.2
1,2,3-Trichlorobenzene
mg/Kg
0.050
0.046
0.046
93.6
92.4
68-130
1.2
1,2,4-Trichlorobenzene
mg/Kg
0.050
0.049
0.046
98.0
92.4
66-125
5.8
1,1,1-Trichloroethane
mg/Kg
0.050
0.049
0.046
98.8
93.2
67-131
5.8
1,1,2-Trichloroethane
mg/Kg
0.050
0.050
0.049
101
99.6
70-133
1.3
Trichloroethene
mg/Kg
0.050
0.049
0.047
99.2
94.8
75-133
4.5
Trichlorofluoromethane
mg/Kg
0.050
0.050
0.045
100
91.6
44-146
8.7
1,2,3-Trichloropropane
mg/Kg
0.050
0.048
0.047
96.8
94.0
60-137
2.9
1,2,4-Trimethyl benzene
mg/Kg
0.050
0.046
0.045
93.2
90.0
69-129
3.4
1,3,5-Trimethylbenzene
mg/Kg
0.050
0.046
0.044
92.4
88.2
69-128
4.6
Vinyl Acetate
mg/Kg
0.050
0.057
0.054
114
110
60-140
4.1
Vinyl Chloride
mg/Kg
0.050
0.050
0.046
101
92.2
48-147
9.5
o-Xylene
mg/Kg
0.050
0.048
0.047
96.4
94.0
74-126
2.5
m,p-Xylene
mg/Kg
0.100
0.096
0.092
96.7
92.9
75-124
4.0
4-Bromofluorobenzene (S)
97.2
97.4
70-130
Dibromofluoromethane (S)
96.8
98.0
84-123
Toluene-d8(S)
97.8
99.0
76-129
Max
RPD
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Date: 07/25/2023 10:35 AM Page 6 of 18
Page 38 of 52

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-199-0028
QC Prep: V35554
QC Prep Batch Method: 3546
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Lab Reagent Blank LRB-V35554
Associated Lab Samples: 90011, 90012, 90013
QC Analytical Batch(es): V35586
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix: SOL
Blank MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Acenaphthene
mg/Kg
<0.660
0.660
07/24/23 11:56
Acenaphthylene
mg/Kg
<0.660
0.660
07/24/23 11:56
Aniline
mg/Kg
<0.660
0.660
07/24/23 11:56
Anthracene
mg/Kg
<0.660
0.660
07/24/23 11:56
Benzo(a)anthracene
mg/Kg
<0.660
0.660
07/24/23 11:56
Benzo(a)pyrene
mg/Kg
<0.660
0.660
07/24/23 11:56
Benzo(b)fluoranthene
mg/Kg
<0.660
0.660
07/24/23 11:56
Benzo(g,h,i)perylene
mg/Kg
<0.660
0.660
07/24/23 11:56
Benzo(k)fluoranthene
mg/Kg
<0.660
0.660
07/24/23 11:56
Benzoic Acid
mg/Kg
<2.00
2.00
07/24/23 11:56
Benzyl alcohol
mg/Kg
<0.660
0.660
07/24/23 11:56
Bis(2-Chloroethoxy)methane
mg/Kg
<0.660
0.660
07/24/23 11:56
Bis(2-Chloroethyl)ether
mg/Kg
<0.660
0.660
07/24/23 11:56
Bis(2-Chloroisopropyl)ether
mg/Kg
<0.330
0.330
07/24/23 11:56
Bis(2-ethylhexyl)phthalate
mg/Kg
<0.660
0.660
07/24/23 11:56
4-Bromophenyl phenyl ether
mg/Kg
<0.660
0.660
07/24/23 11:56
Butyl benzyl phthalate
mg/Kg
<0.330
0.330
07/24/23 11:56
4-Chloro-3-methylphenol
mg/Kg
<0.660
0.660
07/24/23 11:56
4-Chloroaniline
mg/Kg
<0.330
0.330
07/24/23 11:56
2-Chloronaphthalene
mg/Kg
<0.660
0.660
07/24/23 11:56
2-Chlorophenol
mg/Kg
<0.660
0.660
07/24/23 11:56
4-Chlorophenyl phenyl ether
mg/Kg
<1.00
1.00
07/24/23 11:56
Chrysene
mg/Kg
<0.660
0.660
07/24/23 11:56
Dibenz(a,h)anthracene
mg/Kg
<0.660
0.660
07/24/23 11:56
Dibenzofuran
mg/Kg
<0.660
0.660
07/24/23 11:56
1,2-Dichlorobenzene
mg/Kg
<0.660
0.660
07/24/23 11:56
1,3-Dichlorobenzene
mg/Kg
<0.660
0.660
07/24/23 11:56
Date: 07/25/2023 10:35 AM
Page 7 of 18
Page 39 of 52

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-199-0028
QC Prep: V35554
QC Prep Batch Method: 3546
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Lab Reagent Blank LRB-V35554
Associated Lab Samples: 90011, 90012, 90013
QC Analytical Batch(es): V35586
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix: SOL
Blank MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
1,4-Dichlorobenzene
mg/Kg
<0.330
0.330
07/24/23 11:56
3,3'-Dichlorobenzidine
mg/Kg
<0.660
0.660
07/24/23 11:56
2,4-Dichlorophenol
mg/Kg
<0.660
0.660
07/24/23 11:56
Diethyl phthalate
mg/Kg
<0.660
0.660
07/24/23 11:56
Dimethyl phthalate
mg/Kg
<0.660
0.660
07/24/23 11:56
2,4-Dimethylphenol
mg/Kg
<0.330
0.330
07/24/23 11:56
Di-n-butyl phthalate
mg/Kg
<0.660
0.660
07/24/23 11:56
4,6- Din itro-2-methylphenol
mg/Kg
<1.50
1.50
07/24/23 11:56
2,4-Dinitrophenol
mg/Kg
<1.50
1.50
07/24/23 11:56
2,4-Dinitrotoluene
mg/Kg
<0.660
0.660
07/24/23 11:56
2,6-Dinitrotoluene
mg/Kg
<0.660
0.660
07/24/23 11:56
Di-n-Octyl Phthalate
mg/Kg
<0.330
0.330
07/24/23 11:56
Fluoranthene
mg/Kg
<0.660
0.660
07/24/23 11:56
Fluorene
mg/Kg
<0.660
0.660
07/24/23 11:56
Hexachlorobenzene
mg/Kg
<0.660
0.660
07/24/23 11:56
Hexachlorobutadiene
mg/Kg
<0.660
0.660
07/24/23 11:56
Hexachlorocyclopentadiene
mg/Kg
<0.660
0.660
07/24/23 11:56
Hexachloroethane
mg/Kg
<0.660
0.660
07/24/23 11:56
Indeno(1,2,3-cd)pyrene
mg/Kg
<0.660
0.660
07/24/23 11:56
Isophorone
mg/Kg
<0.660
0.660
07/24/23 11:56
1-Methylnaphthalene
mg/Kg
<0.660
0.660
07/24/23 11:56
2-Methylnaphthalene
mg/Kg
<0.660
0.660
07/24/23 11:56
2-Methylphenol
mg/Kg
<0.660
0.660
07/24/23 11:56
3&4 Methylphenol
mg/Kg
<0.660
0.660
07/24/23 11:56
Naphthalene
mg/Kg
<0.660
0.660
07/24/23 11:56
2-Nitroaniline
mg/Kg
<0.660
0.660
07/24/23 11:56
3-Nitroaniline
mg/Kg
<0.660
0.660
07/24/23 11:56
Date: 07/25/2023 10:35 AM
Page 8 of 18
Page 40 of 52

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-199-0028
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep:
V35554
QC Analytical Batch(es): V35586
QC Prep Batch Method:
3546
Analysis Method:
8270E
Analysis Description:
Semivolatile Organic
Compounds -
GC/MS
Lab Reagent Blank
LRB-V35554
Matrix: SOL
Associated Lab Samples:
90011, 90012, 90013
Blank
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
4-Nitroaniline
mg/Kg
<0.330
0.330
07/24/23 11:56
Nitrobenzene
mg/Kg
<0.330
0.330
07/24/23 11:56
2-Nitrophenol
mg/Kg
<0.660
0.660
07/24/23 11:56
4-Nitrophenol
mg/Kg
<0.660
0.660
07/24/23 11:56
N-Nitrosodimethylamine
mg/Kg
<0.660
0.660
07/24/23 11:56
N-Nitrosodiphenylamine
mg/Kg
<0.660
0.660
07/24/23 11:56
N-Nitroso-di-n-propylamine
mg/Kg
<0.660
0.660
07/24/23 11:56
Pentachlorophenol
mg/Kg
<1.00
1.00
07/24/23 11:56
Phenanthrene
mg/Kg
<0.660
0.660
07/24/23 11:56
Phenol
mg/Kg
<0.660
0.660
07/24/23 11:56
Pyrene
mg/Kg
<0.660
0.660
07/24/23 11:56
Pyridine
mg/Kg
<0.330
0.330
07/24/23 11:56
1,2,4-Trichlorobenzene
mg/Kg
<0.660
0.660
07/24/23 11:56
2,4,5-Trichlorophenol
mg/Kg
<0.660
0.660
07/24/23 11:56
2,4,6-Trichlorophenol
mg/Kg
<0.660
0.660
07/24/23 11:56
2-Fluorobiphenyl(S)
07/24/23 11:56
75.4
44-115
2-Fluorophenol(S)
07/24/23 11:56
66.0
35-115
Nitrobenzene-d5 (S)
07/24/23 11:56
72.4
37-122
4-Terphenyl-d14 (S)
07/24/23 11:56
86.8
54-127
2,4,6-Tribromophenol(S)
07/24/23 11:56
69.3
39-132
Phenol-d5 (S)
07/24/23 11:56
60.0
34-121
Laboratory Control Sample LCS-V35554
Spike
Parameter Units Conc.
LCS LCS %Rec % Rec
Result Limits
Acenaphthene mg/Kg 1.67 1.28 76.6 40-123
Acenaphthylene mg/Kg 1.67 1.26 75.4 32-132
Date: 07/25/2023 10:35 AM Page 9 of 18
Page 41 of 52

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-199-0028
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V35554 QC Analytical Batch(es): V35586
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample LCS-V35554
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
Aniline
mg/Kg
1.67
2.09
125
12-197
Anthracene
mg/Kg
1.67
1.40
83.8
47-123
Benzo(a)anthracene
mg/Kg
1.67
1.40
83.8
49-126
Benzo(a)pyrene
mg/Kg
1.67
1.50
89.8
45-129
Benzo(b)fluoranthene
mg/Kg
1.67
1.39
83.2
45-132
Benzo(g,h,i)perylene
mg/Kg
1.67
1.39
83.2
43-134
Benzo(k)fluoranthene
mg/Kg
1.67
1.51
90.4
47-132
Benzoic Acid
mg/Kg
1.67
<2.00
58.2
10-83
Benzyl alcohol
mg/Kg
1.67
1.30
77.8
29-122
Bis(2-Chloroethoxy)methane
mg/Kg
1.67
1.32
79.0
36-121
Bis(2-Chloroethyl)ether
mg/Kg
1.67
1.37
82.0
31-120
Bis(2-Chloroisopropyl)ether
mg/Kg
1.67
1.31
78.4
33-131
Bis(2-ethylhexyl)phthalate
mg/Kg
1.67
1.44
86.2
51-133
4-Bromophenyl phenyl ether
mg/Kg
1.67
1.47
88.0
46-124
Butyl benzyl phthalate
mg/Kg
1.67
1.59
95.2
48-132
4-Chloro-3-methyl phenol
mg/Kg
1.67
1.42
85.0
45-122
4-Chloroaniline
mg/Kg
1.67
1.56
93.4
17-106
2-Chloronaphthalene
mg/Kg
1.67
1.31
78.4
41-114
2-Chlorophenol
mg/Kg
1.67
1.24
74.2
34-121
4-Chlorophenyl phenyl ether
mg/Kg
1.67
1.36
81.4
45-121
Chrysene
mg/Kg
1.67
1.41
84.4
50-124
Dibenz(a,h)anthracene
mg/Kg
1.67
1.30
77.8
45-134
Dibenzofuran
mg/Kg
1.67
1.29
77.2
44-120
1,2-Dichlorobenzene
mg/Kg
1.67
1.17
70.0
33-117
1,3-Dichlorobenzene
mg/Kg
1.67
1.13
67.6
30-115
1,4-Dichlorobenzene
mg/Kg
1.67
1.13
67.6
31-115
3,3'-Dichlorobenzidine
mg/Kg
1.67
1.30
77.8
22-121
Date: 07/25/2023 10:35 AM Page 10 of 18
Page 42 of 52

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-199-0028
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V35554 QC Analytical Batch(es): V35586
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample LCS-V35554
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
2,4-Dichlorophenol
mg/Kg
1.67
1.38
82.6
40-122
Diethyl phthalate
mg/Kg
1.67
1.42
85.0
50-124
Dimethyl phthalate
mg/Kg
1.67
1.39
83.2
48-124
2,4-Dimethylphenol
mg/Kg
1.67
1.61
96.4
30-127
Di-n-butyl phthalate
mg/Kg
1.67
1.59
95.2
51-128
4,6- Din itro-2-methylphenol
mg/Kg
1.67
<1.50
77.2
29-132
2,4-Dinitrophenol
mg/Kg
1.67
<1.50
76.6
27-129
2,4-Dinitrotoluene
mg/Kg
1.67
1.44
86.2
48-126
2,6-Dinitrotoluene
mg/Kg
1.67
1.45
86.8
46-124
Di-n-Octyl Phthalate
mg/Kg
1.67
1.46
87.4
45-140
Fluoranthene
mg/Kg
1.67
1.32
79.0
50-127
Fluorene
mg/Kg
1.67
1.34
80.2
43-125
Hexachlorobenzene
mg/Kg
1.67
1.47
88.0
45-122
Hexachlorobutadiene
mg/Kg
1.67
1.30
77.8
32-123
Hexachlorocyclopentadiene
mg/Kg
1.67
1.21
72.4
32-117
Hexachloroethane
mg/Kg
1.67
1.15
68.8
28-117
Indeno(1,2,3-cd)pyrene
mg/Kg
1.67
1.39
83.2
45-133
Isophorone
mg/Kg
1.67
1.11
66.4
30-122
1-Methylnaphthalene
mg/Kg
1.67
1.27
76.0
40-119
2-Methylnaphthalene
mg/Kg
1.67
1.25
74.8
38-122
2-Methylphenol
mg/Kg
1.67
1.35
80.8
32-122
3&4 Methylphenol
mg/Kg
1.67
1.22
73.0
34-119
Naphthalene
mg/Kg
1.67
1.23
73.6
35-123
2-Nitroaniline
mg/Kg
1.67
1.48
88.6
44-127
3-Nitroaniline
mg/Kg
1.67
1.48
88.6
33-119
4-Nitroaniline
mg/Kg
1.67
1.54
92.2
63-147
Nitrobenzene
mg/Kg
1.67
1.15
68.8
34-122
Date: 07/25/2023 10:35 AM Page 11 of 18
Page 43 of 52

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-199-0028
QC Prep: V35554
QC Prep Batch Method: 3546
Laboratory Control Sample
Parameter
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
N-N itroso-d i-n-propyl a m i ne
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
4-Terphenyl-d14 (S)
2,4,6-Tribromophenol (S)
Phenol-d5 (S)
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
LCS-V35554
Spike
Units Conc.
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
QC Analytical Batch(es): V35586
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
LCS
Result
1.22
1.95
1.11
1.67
1.26
1.21
1.40
1.23
1.34
0.747
1.18
1.33
1.29
LCS %Rec
73.0
117
66.4
100
75.4
72.4
83.8
73.6
80.2
44.7
70.6
79.6
77.2
74.8
66.0
71.8
89.2
84.0
59.7
Rec
Limits
36-123
30-132
10-146
38-127
36-120
25-133
50-121
34-121
47-127
10-80
34-118
41-124
39-126
44-115
35-115
37-122
54-127
39-132
34-121
Matrix Spike & Matrix Spike Duplicate
V 90001-MS-V35554
V 90001-MSD-V35554
MS Spike
MSD
MS Result
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Conc.
Spike
Result
%Rec
%Rec
Limits
RPD
RPD
Conc.
Acenaphthene
mg/Kg
<0.661
1.67
1.67
1.19
1.17
71.2
70.0
40-123
1.6
20
Acenaphthylene
mg/Kg
<0.661
1.67
1.67
1.21
1.18
72.4
70.6
32-132
2.5
20
Aniline
mg/Kg
<0.661
1.67
1.67
2.01
1.07
120
64.0
12-197
61.0*
20
* QC Fail Date: 07/25/2023 10:35 AM Page 12 of 18
Page 44 of 52

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-199-0028
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V35554 QC Analytical Batch(es): V35586
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix Spike & Matrix Spike Duplicate V 90001-MS-V35554 V 90001-MSD-V35554
Parameter
Units
Result
MS Spike
Conc.
MSD
Spike
Conc.
MS Result
MSD
Result
MS
a/oRec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
Anthracene
mg/Kg
<0.661
1.67
1.67
1.32
1.32
79.0
79.0
47-123
0.0
20
Benzo(a)anthracene
mg/Kg
<0.661
1.67
1.67
1.32
1.31
79.0
78.4
49-126
0.7
20
Benzo(a)pyrene
mg/Kg
<0.661
1.67
1.67
1.40
1.42
83.8
85.0
45-129
1.4
20
Benzo(b)fluoranthene
mg/Kg
<0.661
1.67
1.67
1.27
1.32
76.0
79.0
45-132
3.8
20
Benzo(g,h,i)perylene
mg/Kg
<0.661
1.67
1.67
1.26
1.28
75.4
76.6
43-134
1.5
20
Benzo(k)fluoranthene
mg/Kg
<0.661
1.67
1.67
1.32
1.38
79.0
82.6
47-132
4.4
20
Benzoic Acid
mg/Kg
<2.00
1.67
1.67
0.805
0.660
48.2
39.5
10-83
19.7
20
Benzyl alcohol
mg/Kg
<0.661
1.67
1.67
1.31
1.09
78.4
65.2
29-122
18.3
20
Bis(2-Chloroethoxy)methane
mg/Kg
<0.661
1.67
1.67
1.23
1.14
73.6
68.2
36-121
7.5
20
Bis(2-Chloroethyl)ether
mg/Kg
<0.661
1.67
1.67
1.18
1.22
70.6
73.0
31-120
3.3
20
Bis(2-Chloroisopropyl)ether
mg/Kg
<0.330
1.67
1.67
1.21
1.14
72.4
68.2
33-131
5.9
20
Bis(2-ethylhexyl)phthalate
mg/Kg
<0.661
1.67
1.67
1.45
1.42
86.8
85.0
51-133
2.0
20
4-Bromophenyl phenyl ether
mg/Kg
<0.661
1.67
1.67
1.42
1.39
85.0
83.2
46-124
2.1
20
Butyl benzyl phthalate
mg/Kg
<0.330
1.67
1.67
1.47
1.41
88.0
84.4
48-132
4.1
20
4-Chloro-3-methyl phenol
mg/Kg
<0.661
1.67
1.67
1.33
1.32
79.6
79.0
45-122
0.7
20
4-Chloroaniline
mg/Kg
<0.330
1.67
1.67
1.48
1.38
88.6
82.6
17-106
6.9
20
2-Chloronaphthalene
mg/Kg
<0.661
1.67
1.67
1.21
1.17
72.4
70.0
41-114
3.3
20
2-Chlorophenol
mg/Kg
<0.661
1.67
1.67
1.23
1.13
73.6
67.6
34-121
8.4
20
4-Chlorophenyl phenyl ether
mg/Kg
<1.00
1.67
1.67
1.28
1.27
76.6
76.0
45-121
0.7
20
Chrysene
mg/Kg
<0.661
1.67
1.67
1.31
1.29
78.4
77.2
50-124
1.5
20
Dibenz(a,h)anthracene
mg/Kg
<0.661
1.67
1.67
1.18
1.22
70.6
73.0
45-134
3.3
20
Dibenzofuran
mg/Kg
<0.661
1.67
1.67
1.19
1.19
71.2
71.2
44-120
0.0
20
1,2-Dichlorobenzene
mg/Kg
<0.661
1.67
1.67
1.11
1.01
66.4
60.4
33-117
9.4
20
1,3-Dichlorobenzene
mg/Kg
<0.661
1.67
1.67
1.03
0.975
61.6
58.3
30-115
5.4
20
1,4-Dichlorobenzene
mg/Kg
<0.330
1.67
1.67
1.04
0.961
62.2
57.5
31-115
7.8
20
3,3'-Dichlorobenzidine
mg/Kg
<0.661
1.67
1.67
1.03
1.03
61.6
61.6
22-121
0.0
20
Date: 07/25/2023 10:35 AM Page 13 of 18
Page 45 of 52

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-199-0028
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V35554 QC Analytical Batch(es): V35586
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix Spike & Matrix Spike Duplicate V 90001-MS-V35554 V 90001-MSD-V35554
Parameter
Units
Result
MS Spike
Conc.
MSD
Spike
Conc.
MS Result
MSD
Result
MS
a/oRec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
2,4-Dichlorophenol
mg/Kg
<0.661
1.67
1.67
1.31
1.22
78.4
73.0
40-122
7.1
20
Diethyl phthalate
mg/Kg
<0.661
1.67
1.67
1.30
1.39
77.8
83.2
50-124
6.6
20
Dimethyl phthalate
mg/Kg
<0.661
1.67
1.67
1.30
1.30
77.8
77.8
48-124
0.0
30
2,4-Dimethylphenol
mg/Kg
<0.330
1.67
1.67
1.59
1.49
95.2
89.2
30-127
6.4
20
Di-n-butyl phthalate
mg/Kg
<0.661
1.67
1.67
1.47
1.47
88.0
88.0
51-128
0.0
20
4,6- Din itro-2-methylphenol
mg/Kg
<1.50
1.67
1.67
1.10
1.02
65.8
61.0
29-132
7.5
20
2,4-Dinitrophenol
mg/Kg
<1.50
1.67
1.67
0.982
0.887
58.8
53.1
27-129
10.1
20
2,4-Dinitrotoluene
mg/Kg
<0.661
1.67
1.67
1.33
1.42
79.6
85.0
48-126
6.5
20
2,6-Dinitrotoluene
mg/Kg
<0.661
1.67
1.67
1.35
1.37
80.8
82.0
46-124
1.4
20
Di-n-Octyl Phthalate
mg/Kg
<0.330
1.67
1.67
1.39
1.40
83.2
83.8
45-140
0.7
20
Fluoranthene
mg/Kg
<0.661
1.67
1.67
1.21
1.25
72.4
74.8
50-127
3.2
20
Fluorene
mg/Kg
<0.661
1.67
1.67
1.26
1.26
75.4
75.4
43-125
0.0
20
Hexachlorobenzene
mg/Kg
<0.661
1.67
1.67
1.38
1.45
82.6
86.8
45-122
4.9
20
Hexachlorobutadiene
mg/Kg
<0.661
1.67
1.67
1.21
1.13
72.4
67.6
32-123
6.8
20
Hexachlorocyclopentadiene
mg/Kg
<0.661
1.67
1.67
1.03
0.923
61.6
55.2
32-117
10.9
20
Hexachloroethane
mg/Kg
<0.661
1.67
1.67
1.03
0.958
61.6
57.3
28-117
7.2
20
Indeno(1,2,3-cd)pyrene
mg/Kg
<0.661
1.67
1.67
1.27
1.29
76.0
77.2
45-133
1.5
20
Isophorone
mg/Kg
<0.661
1.67
1.67
1.05
0.990
62.8
59.2
30-122
5.8
20
1-Methylnaphthalene
mg/Kg
<0.661
1.67
1.67
1.22
1.11
73.0
66.4
40-119
9.4
20
2-Methylnaphthalene
mg/Kg
<0.661
1.67
1.67
1.20
1.12
71.8
67.0
38-122
6.8
20
2-Methylphenol
mg/Kg
<0.661
1.67
1.67
1.18
1.15
70.6
68.8
32-122
2.5
20
3&4 Methylphenol
mg/Kg
<0.661
1.67
1.67
1.08
1.06
64.6
63.4
34-119
1.8
20
Naphthalene
mg/Kg
<0.661
1.67
1.67
1.18
1.07
70.6
64.0
35-123
9.7
20
2-Nitroaniline
mg/Kg
<0.661
1.67
1.67
1.33
1.33
79.6
79.6
44-127
0.0
20
3-Nitroaniline
mg/Kg
<0.661
1.67
1.67
1.33
1.33
79.6
79.6
33-119
0.0
20
4-Nitroaniline
mg/Kg
<0.330
1.67
1.67
1.35
1.46
80.8
87.4
63-147
7.8
20
Date: 07/25/2023 10:35 AM Page 14 of 18
Page 46 of 52

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-199-0028
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V35554 QC Analytical Batch(es): V35586
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix Spike & Matrix Spike Duplicate V 90001-MS-V35554 V 90001-MSD-V35554
Parameter
Units
Result
MS Spike
Conc.
MSD
Spike
Conc.
MS Result
MSD
Result
MS
a/oRec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
Nitrobenzene
mg/Kg
<0.330
1.67
1.67
1.09
0.997
65.2
59.7
34-122
8.9
20
2-Nitrophenol
mg/Kg
<0.661
1.67
1.67
1.18
1.10
70.6
65.8
32-123
7.0
20
4-Nitrophenol
mg/Kg
<0.661
1.67
1.67
1.72
1.89
103
113
30-132
9.4
20
N-Nitrosodimethylamine
mg/Kg
<0.661
1.67
1.67
0.964
0.979
57.7
58.6
10-146
1.5
30
N-Nitrosodiphenylamine
mg/Kg
<0.661
1.67
1.67
1.51
1.50
90.4
89.8
38-127
0.6
20
N-Nitroso-di-n-propylamine
mg/Kg
<0.661
1.67
1.67
1.17
1.09
70.0
65.2
36-120
7.0
20
Pentachlorophenol
mg/Kg
<1.00
1.67
1.67
1.03
1.32
61.6
79.0
25-133
24.6*
20
Phenanthrene
mg/Kg
<0.661
1.67
1.67
1.32
1.34
79.0
80.2
50-121
1.5
20
Phenol
mg/Kg
<0.661
1.67
1.67
1.10
1.05
65.8
62.8
34-121
4.6
20
Pyrene
mg/Kg
<0.661
1.67
1.67
1.33
1.29
79.6
77.2
47-127
3.0
20
Pyridine
mg/Kg
<0.330
1.67
1.67
0.752
0.682
45.0
40.8
10-80
9.7
20
1,2,4-Trichlorobenzene
mg/Kg
<0.661
1.67
1.67
1.16
1.04
69.4
62.2
34-118
10.9
20
2,4,5-Trichlorophenol
mg/Kg
<0.661
1.67
1.67
1.25
1.24
74.8
74.2
41-124
0.8
20
2,4,6-Trichlorophenol
mg/Kg
<0.661
1.67
1.67
1.21
1.21
72.4
72.4
39-126
0.0
20
2-Fluorobiphenyl (S)
68.2
68.8
44-115
2-Fluorophenol (S)
58.6
57.3
35-115
Nitrobenzene-d5 (S)
67.0
61.6
37-122
4-Terphenyl-d14 (S)
81.4
82.0
54-127
2,4,6-Tribromophenol(S)
73.0
80.4
39-132
Phenol-d5 (S)
53.2
52.2
34-121
* QC Fail Date: 07/25/2023 10:35 AM Page 15 of 18
Page 47 of 52

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Hart & Hickman (Charlotte)
Project Description:
TPM-001
Report No:
23-199-0028
QC Prep:
V35553
QC Analytical Batch(es): V35656
QC Prep Batch Method:
MAEPH (Prep)
Analysis Method:
MADEP-EPH
Analysis Description:
Massachusetts EPH
Lab Reagent Blank
LRB-V35553
Matrix: SOL
Associated Lab Samples:
90011, 90012, 90013
Blank
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
Aliphatic C9-C18
mg/Kg
<50.0
50.0
07/21/23 16:55
Aliphatic C19-06
mg/Kg
<50.0
50.0
07/21/23 16:55
Aromatic Cll-C22
mg/Kg
<50.0
50.0
07/21/23 16:55
2-Fluorobiphenyl(S)
07/21/23 16:55
68.5
40-140
2-Bromonaphthalene (S)
07/21/23 16:55
69.5
40-140
Chlorooctadecane (S)
07/21/23 16:55
67.2
40-140
OTP Surrogate (S)
07/21/23 16:55
62.5
40-140
Laboratory Control Sample & LCSD
LCS-V35553
LCSD-V35553
Spike
LCS LCSD
LCS LCSD
% Rec
Parameter
Units
Conc.
Result Result
%Rec a/o Rec
Limits
RPD
Max
RPD
Aliphatic C9-C18
mg/Kg
60.0
<50.0 <50.0
76.8 76.8
40-140
0.0
50
Aliphatic C19-06
mg/Kg
80.0
72.3 68.9
90.3 86.1
40-140
4.8
50
Aromatic Cll-C22
mg/Kg
170
172 189
101 111
40-140
9.4
50
2-Fluorobiphenyl (S)
84.0 88.0
40-140
2-Bromonaphthalene (S)
87.2 90.7
40-140
Chlorooctadecane (S)
66.8 61.5
40-140
OTP Surrogate (S)
79.0 84.2
40-140
Date: 07/25/2023 10:35 AM Page 16 of 18
Page 48 of 52

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-199-0028
QC Prep: V35509
QC Analytical Batch(es): V35510
QC Prep Batch Method: MAVPH (Prep)
Analysis Method:
MADEP-VPH
Analysis Description:
Massachusetts VPH
Lab Reagent Blank
LRB-V35509
Matrix: SOL
Associated Lab Samples: 90011, 90012, 90013
Blank
MQL
Analyzed
%
% Rec
Parameter Units
Result
Recovery
Limits
Aliphatic C5-C8 mg/Kg
<8.00
8.00
07/19/23 10:47
Aliphatic C9-C12 mg/Kg
<8.00
8.00
07/19/23 10:47
Aromatic C9-C10 mg/Kg
<8.00
8.00
07/19/23 10:47
2,5-Dibromotoluene (FID) (S)
07/19/23 10:47
90.7
70-130
2,5-Dibromotoluene (PID) (S)
07/19/23 10:47
99.0
70-130
Laboratory Control Sample & LCSD
LCS-V35509
LCSD-V35509
Spike
LCS LCSD
LCS LCSD
% Rec
Parameter Units
Conc.
Result Result
%Rec a/o Rec
Limits
RPD
Max
RPD
Aliphatic C5-C8 mg/Kg
32.0
36.9 35.6
115 111
70-130
3.5
50
Aliphatic C9-C12 mg/Kg
32.0
36.3 37.2
113 116
70-130
2.4
50
Aromatic C9-C10 mg/Kg
10.7
12.3 12.9
115 121
70-130
4.7
50
2,5-Dibromotoluene (FID) (S)
84.4 84.0
70-130
2,5-Dibromotoluene (PID) (S)
87.5 89.9
70-130
Date: 07/25/2023 10:35 AM Page 17 of 18
Page 49 of 52

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-199-0028
QC Analytical Batch: V35528
Analysis Method: SW-DRYWT
Analysis Description: Dry Weight Determination
Duplicate V 90002-DUP
Result DUP
Parameter Units Result
Moisture % 13.5 13.7
Duplicate V 90011-DUP
RPD Max RPD Analyzed
1.4 20.0 07/19/23 18:30
Result DUP RPD Max RPD Analyzed
Parameter Units Result
Moisture % 19.8 20.4 2.9 20.0 07/19/2318:30
Date: 07/25/2023 10:35 AM Page 18 of 18
Page 50 of 52

WayPAoint.
NALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 01102
Customer Name: Hart & Hickman (Charlotte)
Report Number: 23-199-0028
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
IRT15 2.3C
Shipping container/cooler uncompromised?
CO,) Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
# Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
# Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample Iabel(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
U Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
U Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
F_ High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Special precautions or instructions included?
Comments:
0 Yes 0 No 0 N/A
F Low concentration EnCore samplers (48 hr)
I✓ Low conc pre -weighed vials (Sod Bis -14 d)
0Yes ONo
Signature: Angelo Norvell
Date & Time: 07/18/2023 17:11:58
Page 51 of 52

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Page 52 of 52

Waypointo
ANALYTICAL
8/24/2023
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 23-226-0007
Client Project Description: TPM-001
Dear Steve Libbey:
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Waypoint Analytical, LLC (Charlotte) received sample(s) on 8/14/2023 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
a'-1
Angela D Overcash
Senior Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 11

Waypoint.0
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State
Program
Lab ID
Expiration Date
North Carolina
State Program
37735
07/31/2024
North Carolina
State Program
402
12/31/2023
South Carolina
State Program
99012
07/31/2023
South Carolina
State Program
99012
12/31/2022
Page 1 of 1 00016/23-226-0007
Page 2 of 11

Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointana lyti ca I som
Sample Summary Table
Report Number: 23-226-0007
Client Project Description: TPM-001
Lab No Client Sample ID Matrix Date Collected Date Received
92371 EX-18-F Solids 08/14/2023 13:20 08/14/2023 15:19
Page 3 of 11

(2)
Waypoint. 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointana lyti ca I som
Summary of Detected Analytes
Project: TPM-001
Report Number: 23-226-0007
Client Sample ID Lab Sample ID
Method Parameters Result Units Report Limit Analyzed Qualifiers
EX-18-F V 92371
SW-DRYWT Moisture
32.3
08/15/2023 13:30
Page 4 of 11

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Report Date : 08/24/2023
Received : 08/14/2023
Report Number : 23-226-0007 REPOR T OF A NA L YSIS
Lab No : 92371 Matrix: Solids
Sample ID : EX-18-F Sampled: 8/14/2023 13:20
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
Qualifiers/ DF Dilution Factor
Definitions
32.3 %
1 08/15/2313:30 CNC SW-DRYWT
MQL Method Quantitation Limit
Page 5 of 11

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project TPM-001
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 08/24/2023
Received : 08/14/2023
Report Number : 23-226-0007
REPOR T OF A NA L YSIS
Lab No : 92371
Matrix: Solids
Sample ID : EX-18-F
Sampled: 8/14/2023
13:20
Analytical Method: 8015C DRO
Prep Batch(es):
V36640
08/15/23 15:10
Prep Method: 3546
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
<14.8
mg/Kg - dry
14.8
1 08/16/23 17:01 NDL
V36714
Surrogate: OTP Surrogate
108
Limits: 31-123% 1 08/16/23 17:01 NDL
8015C DRO
Analytical Method: 8015C GRO
Prep Batch(es):
V36575
08/14/23 08:00
Prep Method: 5035 MED
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
<7.98
mg/Kg - dry
7.98
50 08/14/23 23:51 TBL
V36576
Surrogate: a,a,a-Trifluorotoluene
111
Limits: 50-137% 50 08/14/23 23:51 TBL
8015C GRO
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 6 of 11

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-226-0007
QC Prep: V36640
QC Analytical Batch(es): V36714
QC Prep Batch Method: 3546
Analysis Method:
8015C DRO
Analysis Description:
Total Petroleum Hydrocarbons - Extractable
Lab Reagent Blank
LRB-V36640
Matrix: SOL
Associated Lab Samples: 92371
Blank
MQL
Analyzed % % Rec
Parameter Units
Result
Recovery Limits
Diesel Range Organics (00-C28) mg/Kg
<10.0
10.0
08/16/23 13:06
OTP Surrogate (S)
08/16/23 13:06 88.7 31-123
Laboratory Control Sample & LCSD LCS-V36640 LCSD-V36640
Spike LCS LCSD LCS LCSD % Rec
Parameter Units Conc. Result Result %Rec a/o Rec Limits RPD Max
RPD
Diesel Range Organics (C10-C28) mg/Kg 66.7 70.0 64.7 105
OTP Surrogate (S) 98.4
97.0 46-126 7.8 20
81.9 31-123
Date: 08/24/2023 02:10 PM
Page 7 of 11
Page 1 of 3

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-226-0007
QC Prep: V36575
QC Analytical Batch(es): V36576
QC Prep Batch Method: 5035 MED
Analysis Method:
8015C GRO
Analysis Description:
Total Petroleum Hydrocarbons - Volatile
Lab Reagent Blank
LRB-V36575
Matrix: SOL
Associated Lab Samples: 92371
Blank
MQL
Analyzed % % Rec
Parameter Units
Result
Recovery Limits
Gasoline Range Organics (C6-C10) mg/Kg
<5.00
5.00
08/14/23 15:23
a,a,a-Trifluorotoluene (S)
08/14/23 15:23 110 50-137
Laboratory Control Sample & LCSD LCS-V36575 LCSD-V36575
Spike LCS LCSD LCS LCSD % Rec
Parameter Units Conc. Result Result %Rec a/o Rec Limits RPD Max
RPD
Gasoline Range Organics (C6-C10) mg/Kg 50.0 65.1 64.7 130
a,a,a-Trifluorotoluene (S) 122
129 41-138 0.6 20
119 50-137
Date: 08/24/2023 02:10 PM
Page 8 of 11
Page 2 of 3

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Hart & Hickman (Charlotte)
Project Description: TPM-001
Report No: 23-226-0007
QC Analytical Batch: V36607
Analysis Method: SW-DRYWT
Analysis Description: Dry Weight Determination
Duplicate V 92168-DUP
Result DUP
Parameter Units Result
Moisture % 8.40 8.06
Duplicate V 92412-DUP
RPD Max RPD Analyzed
4.1 20.0 08/15/2313:30
Result DUP RPD Max RPD Analyzed
Parameter Units Result
Moisture % 18.5 17.9 3.2 20.0 08/15/2313:30
Date: 08/24/2023 02:10 PM Page 3 of 3
Page 9 of 11

WayPAoint.
NALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 01102
Customer Name: Hart & Hickman (Charlotte)
Report Number: 23-226-0007
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
IRT15 2.9C
Shipping container/cooler uncompromised?
CO,) Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
# Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
# Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample Iabel(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
U Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
U Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
F_ High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Special precautions or instructions included?
Comments:
0 Yes 0 No 0 N/A
F Low concentration EnCore samplers (48 hr)
I✓ Low conc pre -weighed vials (Sod Bis -14 d)
0Yes ONo
Signature: Angelo Norvell
Date & Time: 08/14/2023 15:44:49
Page 10 of 11

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Page 11 of 11

From:
Beverly, Trudy
To:
Steve Libbev
Subject:
RE: [External] Former Church Property, 3201 Tuckeseegee Road, Charlotte, NC ; Incident 48982
Date:
Wednesday, October 11, 2023 12:45:00 PM
Attachments:
image001ma
image007.ma
Received.
Trudy
D. Eg�Q�::
YG"pjrlm n[06mn'onm w6u�Yly��
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy.13everlykdeq. nc. gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: httos://deq.nagov/about/divisions/waste-mana,ement/ust
Branch's Above Ground Storage Tanks Website Address: httns://deq.nc.gov/about/divisions/waste-management/ust/ast-pram
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httus:Hdeg.nc.gov/about/divisions/waste-management/waste-management-rules-data/waste-mana eg ment ig s=maps
File Review Procedures:
htips:Hdeq.ne.,gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
htips:Hdcg.nc. gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
https://files.nc.gov/nedeg[W aste%2OManagement/DWMIUST[WhatsNew/Final-Electronic-Document-Submittal-Poligy_pdf
httl2s:Hfiles.nc.gov/ncdeq[Waste .20Management/DWM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: Steve Libbey <[e-mail]>
Sent: Wednesday, October 11, 2023 12:23 PM
To: Beverly, Trudy <[e-mail]>
Subject: [External] Former Church Property, 3201 Tuckeseegee Road, Charlotte, NC ; Incident 48982
CAUTION: External email. Do not click links or open attachments unless verified. Report suspicious emails with the
Report Message button located on your Outlook menu bar on the Home tab.
Hi Trudy, the IAA for the above -referenced site is attached for review.
Please call me if you have any questions.
Thanks,
Steve
Stephen Libbey, PG, Project Manager
Hart & Hickman, PC
2923 S Tryon Street, Suite 100 •Charlotte, NC 28203
Direct: 704-887-4606 • Mobile: [phone]
www.harthickman.com Im

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