26090_Smokey Mtn Petroleum_ReportofLimitedSoilandGroundwaterAssessment_20220412_Sealed

CECS SOUTHEAST, LLP
eoteoh riical • Construction Materials • Environn ental • Face .
July 18, 2023
Mr. Kris Riddle
Brownfields Redevelopment Section
North Carolina Department of Environmental Quality
Reference: Report of Limited Soil and Groundwater Assessment
Former Smokey Mountain Petroleum Company Site (Buncombe County Parcels)
21 and 99999 Governors View Road
Asheville, Buncombe County, North Carolina
ECS Project No. 49-13699-D
Mr. Riddle:
On behalf of our client, Buckeye Community Hope Foundation ECS has prepared this sealed cover letter
for the above -referenced report, dated April 12, 2022. As such, I Don R. Marlor a Licensed Geologist for
ECS Southeast, LLP, do certify that the information contained in the referenced report is correct and
accurate to the best of my knowledge, and at the time of the completion of the report.
Respectfully,
ECS SOUTHEAST, LLP as repres
Don R. Marlor, P.G. s
Environmental Projec- M
[e-mail].
828-785-4183 I .,
Roger A. mith, P.G.
Principal Geologist
[e-mail]
704-378-9015
erltgo. by;
•+ N CAR••,
SEAL
645 age s
FOr p GOQ'a•

ECS SOUTHEAST, LLP "Setting the Standard for Service"
- - Geotechnical - Construction Materials - Environmental - Facilities NC Registered Engineering Firm F-1078
INC Registered Geologists Firm C-553
SC Registered Engineering Firm 3239
April 12, 2022
Mr. Steve Sceranka
Buckeye Community Hope Foundation
3021 E. Dublin -Granville Road
Suite 200
Columbus, Ohio 43231
Reference:
Report of Limited Soil and Groundwater Assessment
Buncombe County Parcels
21 & 99999 Governors View Road
Asheville, Buncombe County, North Carolina
ECS Project No. 49:13699-D
Dear Mr. Sceranka,
As authorized by your acceptance of ECS Proposal No. 49:29305P dated January 26, 2022 and authorized
on February 15, 2022, ECS Southeast, LLP (ECS) has completed this Report of Limited Soil and
Groundwater Assessment for the above referenced site. Included in this report is a description of the
field activities, the results obtained, and our conclusions and recommendations.
We appreciate the opportunity to provide our services to you. If there are questions regarding this
report, or a need for further information, please contact us.
Respectfully submitted,
ECS SOUTHEAST, LLP
Don R. Marlor, P.G.
Environmental Staff Project Manager
[e-mail]
828-785-4183
Roger A. Smith, P.G.
Principal Geologist
[e-mail]
704-378-9015
ECS Capitol Services, PLLC • ECS Florida, LLC • ECS Mid -Atlantic, LLC • ECS Midwest, LLC • ECS Southeast, LLP • ECS Southwest, LLP
www.ecslimited.com

Report of Limited Soil and Groundwater Assessment
Buncombe County Parcels
21 & 99999 Governors View Road
Asheville, Buncombe County, North Carolina
ECS Project No. 49:13699-D
April 12, 2022
TABLE OF CONTENTS
1.0
BACKGROUND INFORMATION..........................................................................................................1
2.0
ASSESSMENT ACTIVITIES...................................................................................................................2
3.0
RESULTS.............................................................................................................................................4
4.0
FINDINGS AND CONCLUSIONS..........................................................................................................5
5.0
RECOMMENDATIONS........................................................................................................................6
6.0
QUALIFICATIONS OF REPORT............................................................................................................7
FIGURES
Figure 1: Site Topographic Map
Figure 2: Sample Location Map
TABLE
Table 1: Summary of PID Readings
Table 2: Summary of Soil Analytical Results
Table 3: Summary of Groundwater Analytical Results
APPENDIX
Appendix A: Photo Documentation
Appendix B: Boring Logs
Appendix C: Laboratory Analytical Report with COC Documentation
Appendix D: NCDEQ Risk Calculator Output

Report of Limited Soil and Groundwater Assessment
Buncombe County Parcels
21 & 99999 Governors View Road
Asheville, Buncombe County, North Carolina
ECS Project No. 49:13699-D
Apri112, 2022
1.0 BACKGROUND INFORMATION
The subject property is identified by the Buncombe County Geographic Information System (GIS)
website as Parcel Identification Numbers (PINS) 965854606000000 and 965853892200000, consists of
2.73 acres, and is owned by Swannanoa River Road, LLC and Realty II, LLC. A Site Topographic Map is
provided as Figure 1, which indicates the site location. Based on the available information, the subject
property consists of vegetated and wooded land. ECS completed a Phase I Environmental Site
Assessment (Phase I ESA) at the site on December 30, 2021 (ECS Project No. 49-13699-A).
According to the Phase I ESA, Smoky Mountain Petroleum Company, Inc. operated at the subject
property from at least 1970 until the early 2000s. The facility included six (6) vertical 20,000-gallon
aboveground storage tanks (ASTs) with associated tuck loading area, ten (10) horizontal 4,000-gallon
ASTs, four (4) underground storage tanks (USTs) west of facility building, two (2) USTs south of the
facility building, and dispensers near the southwest corner of the facility building.
The facility building, ASTs, USTs, and associated distribution systems have reportedly been removed
from the subject property. When the USTs were removed, contaminated soil was identified and
removed. However, soil and groundwater restrictions were placed on the subject property due to
remaining contaminated soil and identified groundwater contamination above regulatory standards.
Assessment following the removal of the ASTs was not conducted at the subject property.
A review of regulatory documentation identified the adjoining property to the east (currently an Aldi
grocery store) was previously developed with D.O. Creasman Co., Inc. Based on available files, soil and
groundwater sampling was performed in several locations on the property. Areas of concern on the
property included former 1,000 and 4,000-gallon USTs, fuel dispensers, a waste oil AST, a fuel oil AST, a
former 12,000-gallon UST, a hydraulic line leak, and debris piles. One soil sample was collected and
analyzed from each area of concern. Total petroleum hydrocarbon (TPH) diesel range organics (DRO)
was detected at concentrations above the State action level in several soil samples. Groundwater
samples were also collected in several locations on the property. TPH DRO was detected in each of the
groundwater samples collected at concentrations ranging from 150 micrograms per liter (ug/L) to 3,500
ug/L. A North Carolina 2L Groundwater Quality Standard (NC2LGWQS) does not exist for TPH in
groundwater.
A groundwater sample was collected near the western boundary (near the subject site) which identified
that the groundwater was impacted.
The Phase I ESA identified the following recognized environmental conditions (RECs):
• ECS considers the historical use of the property as a petroleum fuel distribution facility, which
potentially resulted in undocumented releases of petroleum products, a REC for the subject
property.
• Bulk fuel ASTs were located on the property for approximately 30 years. Documentation of
sampling in the areas of the ASTs was not identified during the previous assessments. Based on
1

Report of Limited Soil and Groundwater Assessment
Buncombe County Parcels
21 & 99999 Governors View Road
Asheville, Buncombe County, North Carolina
ECS Project No. 49:13699-D
Apri112, 2022
the size of the ASTs and extended period of operations, there is a potential for spillage and
overfilling of the tanks and delivery trucks.
• Gasoline dispensers were located near the southwestern corner of the facility building in the
vicinity of the USTs. Documentation indicating when the dispensers were removed or that
samples were collected beneath the dispensers were not available for review.
• Petroleum releases at the eastern adjoining former D.O. Creasman Co., Inc. facility (now an Aldi
store) have occurred and have the potential to impact the subject property. Documentation
regarding the resolution of this incident was not available for review. The open petroleum
incident is considered to present a REC for the subject property.
In addition, the following controlled recognized environmental condition (CREC) was identified by the
Phase I ESA:
• Based on the residual contamination remaining at the property following the UST closure and
associated land use restrictions, ECS considers the releases and land use restrictions a CREC for
the subject property. Future site use and development should be conducted in accordance with
the deed recorded land use restrictions.
ECS was authorized by Mr. Steve Boone with Buckeye Community Hope Foundation to proceed with the
scope of work described in the following report (ECS Proposal Number 49:29035P). This evaluation
included the collection and laboratory analysis of limited soil and groundwater samples from the subject
property. These activities are summarized in this report.
2.0 ASSESSMENT ACTIVITIES
The limited soil and groundwater assessment activities were conducted by ECS on March 14t" and 15tn
2022 and consisted of the collection of ten soil samples and six groundwater samples, for laboratory
analysis. ECS provided an environmental professional to observe and document soil boring activities,
collect soil samples, and collect groundwater samples from temporary monitoring wells for laboratory
analysis. Photo documentation of field activities is provided in AppendixA.
2.1 Pre -Sampling Activities
Based on our understanding of the project information, ECS conducted the following pre -assessment
services:
• ECS contacted the North Carolina public utility locating service (811) to locate/mark public
utilities at the site. Required separation distances between each borehole location and marked
utilities (typically 30-inches) were maintained during the field activities.
• ECS contracted a private utility locator (Blood Hound) to identify private utilities at the soil and
groundwater sample locations. The private utilities were marked at the subject property by
Blood Hound on March 2, 2022.
• ECS prepared a site -specific Health and Safety Plan (HASP). The HASP documented the known
and suspected hazards, applicable personal protective equipment (PPE) for site personnel, and
2

Report of Limited Soil and Groundwater Assessment
Buncombe County Parcels
21 & 99999 Governors View Road
Asheville, Buncombe County, North Carolina
ECS Project No. 49:13699-D
Apri112, 2022
the emergency response procedures. Prior to commencing with field activities, ECS, its
subcontractors, and applicable site personnel reviewed the site -specific HASP.
2.2 Soil Sampling Activities
On March 14 and 15, 2022, ten soil borings were advanced by hydraulically driving a five foot long, 1.5-
inch diameter soil sampling probe by a direct push technology (DPT) type drilling rig to an approximate
depth of 5 feet below ground surface (bgs). Three (3) soil borings were advanced in the vicinity of the six
(6) reported former vertical 20,000-gallon ASTs, four (4) soil borings were advanced in the vicinity of the
ten (10) reported former horizontal 4,000-gallon ASTs, two (2) soil borings were advanced in the vicinity
of the former loading area, and one (1) soil boring was advanced in the vicinity of the former gasoline
dispensers. Prior to advancing the boring, the downhole equipment and DPT drill rig were
decontaminated by pressure washing with municipal water. The down hole equipment and drill rig were
decontaminated to minimize the potential for cross -contamination. Boring locations are depicted in
Figure 2.
Soils were collected continuously from the ground surface to the termination of each boring using a soil
sampling probe lined with a dedicated disposable clear liner (macro -core) for each 5 foot interval. After the
probe was driven and retrieved, the liner was removed from the probe and cut open to expose the soil.
ECS visually classified the soil collected from the boring and placed a portion of the sample into a bag to
be field screened for relative levels of volatile organic vapors using a photoionization detector (PID). The
Boring Logs are included in Appendix B.
Soil samples were collected by ECS personnel wearing new disposable powder -free nitrile gloves
replaced between each sample to minimize the likelihood of cross -contamination. Based on the PID
readings and field observations a soil sample was collected from each boring (SB-1 through SB-10) for
submittal to the laboratory for analysis. The soils selected for laboratory analysis were collected by
placing directly into laboratory supplied/preserved containers based on field screening results. Table 1
includes a summary of the soil boring depths and PID readings.
The soil sample containers were labeled with ECS project number, sample identification, sample date
and time, and requested analytical analysis. The containers were placed into a cooler with ice to
maintain the samples at approximately 4° Celsius (C). The soil samples were submitted to Pace Analytical
Services, LLC (Pace), a North Carolina certified laboratory located in Asheville, North Carolina. The
samples were submitted for analysis of volatile organic compounds (VOCs) and semi -volatile organic
compounds (SVOCs) using EPA Methods 8260 and 8270, respectively. ECS maintained chain of custody
(COC) procedures throughout the sample collection and transportation process. A copy of the analytical
laboratory report along with accompanying COC documentation is included in Appendix C.
2.3 Groundwater Sampling Activities
A track mounted DPT drill rig advanced one groundwater boring at each of the six (6) selected boring
locations (TW-1, TW-2, TW-3, TW-4, TW-5, and TW-6). Total groundwater boring depths ranged from
approximately 12 to 14 feet bgs. Prior to advancing each boring, the down -hole equipment was
3

Report of Limited Soil and Groundwater Assessment
Buncombe County Parcels
21 & 99999 Governors View Road
Asheville, Buncombe County, North Carolina
ECS Project No. 49:13699-D
Apri112, 2022
decontaminated utilizing a pressure washer with municipal water. The down hole equipment and drill
rig were decontaminated to minimize the potential for cross -contamination.
The groundwater borings were converted to temporary monitoring wells (TW-1 through TW-6) for the
collection of groundwater quality samples. The locations of the temporary monitoring wells are depicted
on Figure 2.
The temporary wells were constructed in general conformance with North Carolina Administrative Code
(NCAC) 2C well construction standards utilizing 1-inch diameter 0.010-inch slotted PVC well screen and
riser pipe set with screen to straddle the water table based upon made at the time of drilling. A 10-foot
length of slotted well screen was installed in temporary monitoring wells MW-1 through MW-4. Above
the screened interval, a solid section of PVC riser was placed that extended to a point just above the
ground surface. The annular space around each well was filled with a washed and graded, medium sand
to approximately two feet above the top of the screen. An approximate two -foot bentonite seal was
then added to the annulus above the sand. Groundwater was encountered at depths ranging from 6.04
feet bgs in TW-1 to 8.63 feet bgs in TW-3, as gauged from the ground surface on March 14, 2022.
On March 14, 2022, groundwater quality samples were collected from the six (6) temporary monitoring
wells. Groundwater quality samples were submitted to Pace, a North Carolina certified laboratory
located in Asheville, North Carolina, for analysis for VOCs and SVOCs using EPA Methods 8260 and 8270,
respectively.
ECS maintained COC procedures throughout the sample collection and transportation process. A copy of
the analytical laboratory report along with accompanying COC documentation is included in Appendix C.
Following the completion of the groundwater gauging and sampling activities, the temporary monitoring
wells were abandoned on March 14, 2022 by the NCCWC.
3.0 RESULTS
3.1 Soil Sampling Results
Laboratory analysis of soil sample S13-1 detected Naphthalene above its Residential and Soil -to -
Groundwater Maximum Soil Contaminant Concentration Levels (MSCC) and multiple other targeted
VOCs and SVOCs were also detected at concentrations above their respective Soil -to -Groundwater
MSCCs. Soil samples S13-2, S13-4, S13-6, S13-8, S13-9, and SB-10 contained multiple targeted VOCs above
their laboratory method detection limits, but below their respective MSCCs. These samples did not
contain target SVOCs above their respective laboratory method detection limits. Soil samples S13-3, S13-5,
and S13-7 did not detect targeted VOCs or SVOCs above their respective laboratory method detection
limits. Soil analytical results have been summarized in Table 2. A copy of the laboratory analytical report
with supporting COC documentation is included in Appendix C.
4

Report of Limited Soil and Groundwater Assessment
Buncombe County Parcels
21 & 99999 Governors View Road
Asheville, Buncombe County, North Carolina
ECS Project No. 49:13699-D
Apri112, 2022
3.2 Groundwater Sampling Results
Laboratory analysis of groundwater sample TW-4 detected 1-Methylnaphthalene at a concentration
above its respective NC2LGWQS. Groundwater sample TW-5 detected Naphthalene, 1-
Methylnaphthalene, and 2-Methylnaphthalene at concentrations above their respective NC2LGWQS.
Additionally, detected concentrations of Ethylbenzene and Naphthalene in TW-5 exceed both the
Residential and Non -Residential Groundwater Screening Levels (GWSL) for Vapor Intrusion (VI).
Groundwater sample TW-6 detected Benzene, Naphthalene, 1-Methylnaphthalene, and 2-
Methylnaphthalene at concentrations above their respective NC2LGWQS. Additionally, detected
concentrations of Ethylbenzene, Naphthalene, and Xylene in TW-6 exceeded their respective Residential
and Non -Residential GWSLs for VI. Groundwater samples TW-1, TW-2, and TW-3 did not detect targeted
VOCs or SVOCs at concentrations above laboratory method detection limits or their respective
NC2LGWQS. Groundwater analytical results have been included in Table 3.
4.0 FINDINGS AND CONCLUSIONS
Based on the field observations and laboratory analytical results of the soil sample collected during this
assessment, ECS concludes the following:
• Ten (10) soil samples were submitted to a North Carolina Certified laboratory for analysis of
VOCs and SVOCs using EPA Methods 8260 and 8270, respectively. One of these soil samples (SB-
1) was collected in the vicinity of the former gasoline dispensers. Laboratory analysis of SB-1
detected Naphthalene above its Residential and Soil -to -Groundwater MSCC and multiple other
targeted VOCs and SVOCs above their respective Soil -to -Groundwater MSCCs. The remaining
soil samples collected in the footprint of the former 4,000-gallon ASTs (SB-2, SB-3, SB-4, and SB-
5), former 20,000-gallon ASTs (SB-6, SB-7, and SB-10), and former loading area (SB-8 and SB-9)
did not contain targeted VOCs or SVOCs above their respective Soil -to -Water, Residential, or
Industrial Commercial MSCCs.
• Six (6) groundwater samples (TW-1 through TW-6) were submitted to a North Carolina certified
laboratory for analysis of VOCs and SVOCs using EPA Methods 8260 and 8270, respectively. TW-
5 collected in the vicinity of the former 20,000-gallon ASTs detected Naphthalene, 1-
Methylnaphthalene, and 2-Methylnaphthalene at a concentration above their respective
NC2LGWQS. Additionally, concentrations of Ethylbenzene and Naphthalene detected in TW-5
exceed both the Residential and Non -Residential GWSL for VI. Groundwater sample TW-6
collected in the vicinity of former gasoline dispensers detected Benzene, Naphthalene, 1-
Methylnaphthalene, and 2-Methylnaphthalene at a concentration above their respective
NC2LGWQS and concentrations of Ethylbenzene, Naphthalene, and Toluene above their
respective Residential and Non -Residential GWSLs for VI. Groundwater sample TW-4 collected in
the vicinity of the former loading area detected 1-Methylnaphthalene at a concentration above
its respective NC2LGWQS.
• Groundwater samples TW-2 and TW-3 located along the eastern property did not contain
targeted VOCs or SVOCs above their respective laboratory method detection limits or their
respective NC2LGWQS. Additionally, TW-1 collected in the vicinity of the former 4,000-gallon
5

Report of Limited Soil and Groundwater Assessment
Buncombe County Parcels
21 & 99999 Governors View Road
Asheville, Buncombe County, North Carolina
ECS Project No. 49:13699-D
Apri112, 2022
ASTs did not contain targeted VOCs or SVOCs above their respective laboratory method
detection limits or their respective NC2LGWQS.
• Due to the GWSL for VI exceedances, ECS input the groundwater data for samples TW-S and
TW-6 into the NCDEQ Risk Calculator (January 2022 Version). Based on the results of the risk
calculators, detected concentrations in groundwater samples TW-S and TW-6 exceeded the risk
threshold for Residential occupancy; however, the detected concentrations did not exceed Non -
Residential occupancy. The data output sheets of the risk -calculators for each sample are
included as Appendix D.
• Based on detections of compounds identified in the groundwater samples and the absence of
detections in soil sample SB-1, it appears soil and groundwater at the site have been impacted
from the on -site RECs, as previously documented.
5.0 RECOMMENDATIONS
• Based on the results of this limited soil and groundwater assessment, the previously identified
soil and groundwater impacts remain from the previous ASTs and USTs. However, the site
currently contains a NFA with soil and groundwater use restrictions. Therefore, ECS
recommends that if the site is to be redeveloped, that the existing restrictions be followed.
• Due to the detections in soil sample SB-1 and potential for other petroleum impacts present at
the site, apparent petroleum impacts encountered during construction or demolition activities
at the subject property, ECS recommends that they be properly managed in accordance with
NCDEQ guidance.
• Due to the Residential and Non -Residential vapor intrusion screening level exceedances for
groundwater, ECS recommends conducting a soil gas assessment at the property to verify if
concentrations in soil gas exceed the Residential VISLs. Additionally, a vapor barrier may need to
be incorporated into future development at the subject property.
• Depending upon potential redevelopment plans, the site appears to be eligible for the NCDEQ'
Brownfields program.
R

Report of Limited Soil and Groundwater Assessment
Buncombe County Parcels
21 & 99999 Governors View Road
Asheville, Buncombe County, North Carolina
ECS Project No. 49:13699-D
Apri112, 2022
6.0 QUALIFICATIONS OF REPORT
The activities and evaluative approaches used in this assessment are consistent with those normally
employed in assessment projects of this type. Our evaluation of site conditions has been based on our
understanding of the site project information and the data obtained during our previous assessment and
field activities. Environmental sampling performed and reported herein only provides for specific data
points scattered throughout the project area in accordance with the prior approved scope of work and
work authorization. It is not meant to provide a comprehensive environmental assessment of the entire
subject property parcel. Please note, the laboratory analytical results of the samples collected and
summarized in this report are representative of the date, time and location as stated within this report.
VA

FIGURES

70
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SOURCE:
��� USGS TOPOGRAPHIC MAP
ASHEVILLE OTEEN, NORTH CAROLINA
QUADRANGLE DATED 2019
SCALE: 1:24,000
SITE
0
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-/S
t
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a - ASIle e Re re ign fore
Park A ke I!
U
SLUE RIDGE',,•
Gaylie5�-- , PAR ',WAY
FIGURE 1
SITE TOPOGRAPHIC MAP
GOVERNORS VIEW ROAD
ASHEVILLE, BUNCOMBE COUNTY,
NORTH CAROLINA
ECS PROJECT NO. 49:13699-D

ti .r
qr�,_ �•
• r• 5;go
•� ,1
e
f �- {IL aa,,
r ~ �
�' �• _
-� FORMER SB-2
• BUILDINGS r 1• ..�
S13-5
ej
+ • r- SB-3 _
1 r• i FORMER
•• r~ 4,000-GALLON
I TW_1 ASTs
' - - SB-4
SB-10 _ -
i
TW-2 ' ti
TW-5 SB-9 i
�•' SB-7 �* Or
r FORMER
TW-4 SB-1 r- GASOLINE ,
..�• DISPENSERS R•••
SB-6 +
- z SB-8 • -
FORMER _ •`•
r a
20,000-GALLON FORMER TW-6 •• ••
ASTs LOADING
AREA • 1
r
TW-3
' FORMER USTs
(previously assessed)
-loI�r
. i
LEGEND
N
APPROXIMATE GROUNDWATER SAMPLE LOCATION
® APPROXIMATE SOIL SAMPLE LOCATION wg
APPROXIMATE SITE BOUNDARY
FIGURE 2
SOURCE: SAMPLE LOCATION MAP
GOOGLE EARTH, DATED 2020 GOVERNORS VIEW ROAD
ASHEVILLE, BUNCOMBE COUNTY,
SCALE: NORTH CAROLINA
= 100 FEET ECS PROJECT NO. 49:13699-D
TM

TABLES

Table 1
Summary of PID Readings
Governors View Road Soil and Groundwater Assessment
Governors View Road
Asheville, Buncombe County, North Carolina
ECS Project No.: 49:13699-D
Sample ID
Sample Depth
(ft bgs)
PID Reading (ppm)
0.0-1.0
0.3
1.0-2.0
6.9
2.0-3.0
126
SB-1
3.0-4.0
131
4.0-5.0
127
5.0-7.5
95
0.0-1.0
0.0
1.0-2.0
6.5
5B-2
2.0-3.0
0.5
3.0-4.0
0.0
4.0-5.0
0.1
0.0-1.0
0.5
1.0-2.0
4.5
5B-3
2.0-3.0
1.5
3.0-4.0
1.1
4.0-5.0
0.8
0.0-1.0
7.8
1.0-2.0
0.9
5B-4
2.0-3.0
0.2
3.0-4.0
0.1
4.0-5.0
0.3
0.0-1.0
0.1
1.0-2.0
0.1
5B-5
2.0-3.0
0.3
3.0-4.0
4.2
4.0-5.0
6.3
0.0-1.0
2.3
1.0-2.0
0.7
5B-6
2.0-3.0
0.0
3.0-4.0
0.0
4.0-5.0
0.0
0.0-1.0
0.3
1.0-2.0
0.5
SB-7
2.0-3.0
0.7
3.0-4.0
3.5
4.0-5.0
1.1
0.0-1.0
0.4
1.0-2.0
2.9
5B-8
2.0-3.0
0.8
3.0-4.0
4.5
4.0-5.0
0.6
0.0-1.0
0.7
1.0-2.0
0.4
SB-9
2.0-3.0
3.2
3.0-4.0
8.1
4.0-5.0
16.4
0.0-1.0
0
1.0-2.0
0.1
SB-10
2.0-3.0
0.5
3.0-4.0
0.3
4.0-5.0
6.8
Notes
PID = photoicnization detector
ppm = parts per million
ft bgs = feet below the ground surface
Bold intervals were selected for analysis

Table 2
Summary of Soil Analytical Results
Governors View Road Soil and Groundwater Assessment
Governors View Road
Asheville, Buncombe County, North Carolina
ECS Project No.: 49:13699-D
VOCs by
EPA Method
8260
Notes:
Results presented in milligrams per kilograms (mg/kg)
Targeted Compounds not shown were not detected above laboratory reporting limits
MSCCs = Maximum Soil Contaminant Concentration Levels (March 2022)
VOCs = Volatile Organic Compounds
SVOCs = Semi -Volatile Organic Compounds
J = Estimated concentration detected between laboratory method detection limit and reporting limit

Table 3
Summary of Groundwater Analytical Results
Governors View Road Soil and Groundwater Assessment
Governors View Road
Asheville, Buncombe County, North Carolina
ECS Project No.: 49:13699-D
VOCs
by EPA
Method 8260
SVOCs
by EPA
Method 8270
U
0
c
c
U
0
Sample ID
Sample Date
c
W
Z
X
C
UJ
UJ
Z
C
E
6
TW-1
03/14/22
<0.34
<0.30
<0.64
<0.48
<0.34
BMDL
<1.7
<1.6
<1.7
BMDL
TW-2
<0.34
<0.30
<0.64
<0.48
<0.34
BMDL
<1.7
<1.6
<1.7
BMDL
TW-3
<0.34
<0.30
<0.64
<0.48
<0.34
BMDL
-1.7
<1.6
<1.7
BMDL
TW-4
<0.34
<0.30
<0.64
<0.48
<0.48
BMDL
12.7
2.81
<2.1
BMDL
TW-5
<14
2.0J
301
BMDL
55.7
102
BMDL
TW-6
5.1
193
307
<2.4
BMDL
70.3
126
BMDL
NC2LGWQ5
1
600
6
600
500
Various
1
30
6
Gross Contimantion Levels for Groundwater
5,000
8,000
6,000
260,000
50,000
Various
1,000
12,000
6,000
Residential Groundwater VISL
1.6
3.5
4.6
3,800
77
Various
NA
NA
5
Non -Residential Groundwater VISL
6.9
15
1 20
16,000
320
Various
NA
NA
20
Notes:
Results presented in milligrams per kilograms (ug/L)
BMDL= Below Method Detection Limit
Targeted Compounds not shown were not detected above laboratory method detection limits
VOCs = Volatile Organic Compounds
SVOCs = Semi -Volatile Organic Compounds
NC2LGWQS = North Carolina 2L Groundwater Quality Standards
Residential Groundwater VISL = NCDEQ Residential Groundwater Vapor Intrusion Screening Level (January 2022)
Non -Residential Groundwater VISL = NCDEQ Non -Residential Groundwater Vapor Intrusion Screening Level (January 2022)
Bold = Concentration exceeeds NC2LGWQS
Light Shaded Cell = Concentration Exceeds Residential Groundwater VISL
Dark Shaded Cell = Concentration Exceeds both Residential and Non -Residential Groundwater VISLs

APPENDIX A
Photo Documentation

ti r
i
-
7d"p+`_
Photo 1— View facing south of instillation of Temporary Monitoring Well TW-1 .
�,� •, y�
4 fix
1
~ � V
•�+ „1 W ry B
ii r c ti',
p ` - - ;r', ✓tad L � i Y <' � 'N`
Photo 2 — View facing east of Temporary Monitoring Well TW-2.
BUNCOMBE COUNTY PARCELS
PHOTO DOCUMENTATION
21 & 99999 GOVERNORS VIEW ROAD
ASHEVILLE, NC
ECS PROJECT NO. 49:13699-D

� � 1•
0�
z.
s�i 'q,,". � �` � '•
Pn � . it r ��,F F�..� [ �i" ? t� �
�•�r �� �2,si�� ����F 11 � ;,1 3 �� .,�'�t'j6T,� �e�.- -zse�K
,4��Y
Photo 3 — View of macro core activities.
rAaue�6/17A1/17A1
a�r �
J �
u
s
F Mxtry 1
—
s � S �
Photo 4 — View of decon activities.
BUNCOMBE COUNTY PARCELS
PHOTO DOCUMENTATION
21 & 99999 GOVERNORS VIEW ROAD
ASHEVILLE, NC
ECS PROJECT NO. 49:13699-D

_ i'
BORING LOGS

Governors View Drive Soil and
Project Name: Sheet: 1 of 1 Boring No: S11131
Groundwater Assessment
Client: Buckeye Community Hope Foundation Project No.: 49:13699-D
Site Location: Governors View Drive, Ashevillle, North
Driller: CSI
Drill Rig: GeoProbe
Carolina 28805
Latitude/Longitude:
UO
c
i
m
LE
E
j
J
Depth/Elevation
v
Q
Soil Classification
Description
Of
Q
cc
E
a,
Q
12
(D
Red brown sandy silty with gravel
0.3
SM/MH
6.9
Gray sandy silt with odor
126.0
131.0
S M/M H
127.0
5
-5
S61
Gray brown sandy silt with petroleum odor
95.0
SM/MH
10
SZ WL (First Encountered)
Boring Started: Mar 14 2022
1 WL (Completion)
Boring Completed: Mar 14 2022
Remarks:
Logged By: DMarlor
Principal Engineer/
Roger Smith
Responsible PG:

Governors View Drive Soil and
Project Name: Sheet: 1 of 1 Boring No: SB2
Groundwater Assessment
Client: Buckeye Community Hope Foundation Project No.: 49:13699-D
Site Location: Governors View Drive, Ashevillle, North
Driller: CSI
Drill Rig: GeoProbe
Carolina 28805
Latitude/Longitude:
UO
c
i
m
LE
E
j
J
Depth/Elevation
v
Q
Soil Classification
Description
Of
Q
cc
C
a,
Q
12
a
n
E
M
Red brown clayey silty with organics
0.0
CL/ML
6.5
Brown red silt
0.5
SB2
MH/ML
0.0
Brown sandy silt
0.1
W
SM/MH
SZ WL (First Encountered)
Boring Started: Mar 15 2022
1 WL (Completion)
Boring Completed: Mar 15 2022
Remarks:
Logged By: DMarlor
Principal Engineer/
Roger Smith
Responsible PG:

Governors View Drive Soil and
Project Name: Sheet: 1 of 1 Boring No: $11133
Groundwater Assessment
Client: Buckeye Community Hope Foundation Project No.: 49:13699-D
Site Location: Governors View Drive, Ashevillle, North
Driller: CSI
Drill Rig: GeoProbe
Carolina 28805
Latitude/Longitude:
UO
c
i
m
LE
E
j
J
Depth/Elevation
v
Q
Soil Classification
Description
Of
Q
cc
C
a,
Q
12
a
n
E
M
Tan brown red clayey silt with organics
0.5
4.5
SC/CL
1.5
S63
Tan brown sandy silt
SM/MH
0.8
SZ WL (First Encountered)
Boring Started: Mar 15 2022
1 WL (Completion)
Boring Completed: Mar 15 2022
Remarks:
Logged By: DMarlor
Principal Engineer/
Roger Smith
Responsible PG:

Governors View Drive Soil and
Project Name: Sheet: 1 of 1 Boring No: S11134
Groundwater Assessment
Client: Buckeye Community Hope Foundation Project No.: 49:13699-D
Site Location: Governors View Drive, Ashevillle, North
Driller: CSI
Drill Rig: GeoProbe
Carolina 28805
Latitude/Longitude:
UO
c
i
m
LE
E
j
J
Depth/Elevation
v
Q
Soil Classification
Description
Of
Q
cc
C
a,
Q
12
a
n
E
M
Gray tan clayey silt with organics
7.8
CL/ML
0.9
Brown tan clayey silt
0.2
SB4
0.1
CL/ML
0.3
SZ WL (First Encountered)
Boring Started: Mar 15 2022
1 WL (Completion)
Boring Completed: Mar 15 2022
Remarks:
Logged By: DMarlor
Principal Engineer/
Roger Smith
Responsible PG:

Governors View Drive Soil and
Project Name: Sheet: 1 of 1 Boring No: SB5
Groundwater Assessment
Client: Buckeye Community Hope Foundation Project No.: 49:13699-D
Site Location: Governors View Drive, Ashevillle, North
Driller: CSI
Drill Rig: GeoProbe
Carolina 28805
Latitude/Longitude:
UO
c
i
m
LE
E
j
J
Depth/Elevation
v
Q
Soil Classification
Description
Of
Q
cc
C
a,
Q
12
a
n
E
M
Tan brown clayey silt with organics
0.1
0.1
CL/ML
0.3
S65
Tan sandy silt
4.2
SM/MH
6.3
SZ WL (First Encountered)
Boring Started: Mar 15 2022
1 WL (Completion)
Boring Completed: Mar 15 2022
Remarks:
Logged By: DMarlor
Principal Engineer/
Roger Smith
Responsible PG:

Governors View Drive Soil and
Project Name: Sheet: 1 of 1 Boring No: $11136
Groundwater Assessment
Client: Buckeye Community Hope Foundation Project No.: 49:13699-D
Site Location: Governors View Drive, Ashevillle, North
Driller: CSI
Drill Rig: GeoProbe
Carolina 28805
Latitude/Longitude:
UO
c
i
m
LE
E
j
J
Depth/Elevation
v
Q
Soil Classification
Description
Of
Q
cc
E
a,
Q
12
(D
Gray tan sandy silt with organics
2.3
0.7
SM/MH
0.0
S66
Tan sandy silt
0.0
SM/MH
0.0
SZ WL (First Encountered)
Boring Started: Mar 15 2022
1 WL (Completion)
Boring Completed: Mar 15 2022
Remarks:
Logged By: DMarlor
Principal Engineer/
Roger Smith
Responsible PG:

Governors View Drive Soil and
Project Name: Sheet: 1 of 1 Boring No: S11137
Groundwater Assessment
Client: Buckeye Community Hope Foundation Project No.: 49:13699-D
Site Location: Governors View Drive, Ashevillle, North
Driller: CSI
Drill Rig: GeoProbe
Carolina 28805
Latitude/Longitude:
UO
c
i
m
LE
E
j
J
Depth/Elevation
v
Q
Soil Classification
Description
Of
Q
cc
E
a,
Q
12
(D
Brown tan sandy silt with organics
0.3
0.5
SM/MH
0.7
S67
Tan red sandy silt
3.5
SM/MH
1.1
SZ WL (First Encountered)
Boring Started: Mar 15 2022
1 WL (Completion)
Boring Completed: Mar 15 2022
Remarks:
Logged By: DMarlor
Principal Engineer/
Roger Smith
Responsible PG:

Governors View Drive Soil and
Project Name: Sheet: 1 of 1 Boring No: S11138
Groundwater Assessment
Client: Buckeye Community Hope Foundation Project No.: 49:13699-D
Site Location: Governors View Drive, Ashevillle, North
Driller: CSI
Drill Rig: GeoProbe
Carolina 28805
Latitude/Longitude:
UO
c
i
m
LE
E
j
J
Depth/Elevation
v
Q
Soil Classification
Description
Of
Q
cc
E
a,
Q
12
(D
Brown tan sandy silt with organics
0.4
2.9
SM/MH
0.8
5138
Red gray clayey silt
4.5
CL/ML
Tan sandy silt
0.6
CL/ML
SZ WL (First Encountered)
Boring Started: Mar 15 2022
1 WL (Completion)
Boring Completed: Mar 15 2022
Remarks:
Logged By: DMarlor
Principal Engineer/
Roger Smith
Responsible PG:

Governors View Drive Soil and
Project Name: Sheet: 1 of 1 Boring No: $11139
Groundwater Assessment
Client: Buckeye Community Hope Foundation Project No.: 49:13699-D
Site Location: Governors View Drive, Ashevillle, North
Driller: CSI
Drill Rig: GeoProbe
Carolina 28805
Latitude/Longitude:
UO
c
i
m
LE
E
j
J
Depth/Elevation
v
Q
Soil Classification
Description
Of
Q
cc
E
a,
Q
12
(D
Tan gray sandy silt
0.7
SM/MH
0.4
Tan red sandy silt
3.2
S69
SM/MH
8.1
Gray silty sand with odors
16.4
W
SM/M H
SZ WL (First Encountered)
Boring Started: Mar 15 2022
1 WL (Completion)
Boring Completed: Mar 15 2022
Remarks:
Logged By: DMarlor
Principal Engineer/
Roger Smith
Responsible PG:

Governors View Drive Soil and
Project Name: Sheet: 1 of 1 Boring No: 5610
Groundwater Assessment
Client: Buckeye Community Hope Foundation Project No.: 49:13699-D
Site Location: Governors View Drive, Ashevillle, North
Driller: CSI
Drill Rig: GeoProbe
Carolina 28805
Latitude/Longitude:
UO
c
i
m
LE
E
j
J
Depth/Elevation
v
Q
Soil Classification
Description
Of
Q
cc
E
a,
Q
12
(D
Tan gray sandy silt with organics
0.0
0.1
SM/MH
0.5
Red tan sandy silt
0.3
SM/MH
6.8
SZ WL (First Encountered)
Boring Started: Mar 15 2022
1 WL (Completion)
Boring Completed: Mar 15 2022
Remarks:
Logged By: DMarlor
Principal Engineer/
Roger Smith
Responsible PG:

Governors View Drive Soil and
Project Name: Sheet: 1 of 1 Boring No: TW1
Groundwater Assessment
Client: Buckeye Community Hope Foundation Project No.: 49:13699-D
to
Site Location: Governors View Drive, Ashevillle, North
Driller: CSI
Drill Rig: GeoProbe
Carolina 28805
Latitude/Longitude:
Elevation:
U0
c
i
m
LE
E
j
J
Depth/Elevation
7
v
Q
Soil Classification
Description
WELL CONSTRUCTION
of
Q
cc
E
a,
Q
12
(D
Brown Red sandy silt with organics
0.1
SM/MH
Brown red sandy silt
0.4
5
-5
SM/MH
TW1
Brown sandy silt
SM/MH
10
-10
SZ WL (First Encountered)
Boring Started: Mar 14 2022
1 WL (Completion) 8.35
Boring Completed: Mar 14 2022
Remarks:
Logged By: DMarlor
Principal Engineer/
Roger Smith
Responsible PG:

Governors View Drive Soil and
Project Name: Sheet: 1 of 1 Boring No: TW2
Groundwater Assessment
Client: Buckeye Community Hope Foundation Project No.: 49:13699-D
to
Site Location: Governors View Drive, Ashevillle, North
Driller: CSI
Drill Rig: GeoProbe
Carolina 28805
Latitude/Longitude:
Elevation:
U0
c
i
m
LE
E
j
J
Depth/Elevation
7
v
Q
Soil Classification
Description
WELL CONSTRUCTION
of
Q
cc
E
a,
Q
12
(D
d
n
E
Red sandy silt
SM/MH
5
-5
Brown sandy silt
N:
TW2
N.
SM/MH
10
-10
SZ WL (First Encountered)
Boring Started: Mar 14 2022
1 WL (Completion) 8.36
Boring Completed: Mar 14 2022
Remarks: Soil saturated at 7 feet bgs.
Logged By: DMarlor
Principal Engineer/
Roger Smith
Responsible PG:

Governors View Drive Soil and
Project Name: Sheet: 1 of 1 Boring No: TW3
Groundwater Assessment
Client: Buckeye Community Hope Foundation Project No.: 49:13699-D
to
Site Location: Governors View Drive, Ashevillle, North
Driller: CSI
Drill Rig: GeoProbe
Carolina 28805
Latitude/Longitude:
Elevation:
U0
c
i
m
LE
E
j
J
Depth/Elevation
7
v
Q
Soil Classification
Description
WELL CONSTRUCTION
of
Q
Of
E
a,
Q
12
(D
d
n
E
M
Tan red clayey silt
1.5
M L/CL
Gray brown sandy silt
0.1
N.
N.
5
-5
SM/MH
TW3
0.3
Tan brown gray sandy silt
i
i
SM/MH
10
-10
SZ WL (First Encountered)
Boring Started: Mar 14 2022
1 WL (Completion) 8.56
Boring Completed: Mar 14 2022
Remarks:
Logged By: DMarlor
Principal Engineer/
Roger Smith
Responsible PG:

Governors View Drive Soil and
Project Name: Sheet: 1 of 1 Boring No: TW4
Groundwater Assessment
Client: Buckeye Community Hope Foundation Project No.: 49:13699-D
to
Site Location: Governors View Drive, Ashevillle, North
Driller: CSI
Drill Rig: GeoProbe
Carolina 28805
Latitude/Longitude:
Elevation:
U0
c
i
m
LE
E
j
J
Depth/Elevation
7
v
Q
Soil Classification
Description
WELL CONSTRUCTION
of
Q
cc
E
a,
Q
12
(D
d
n
E
Tan brown sandy silt
SM/MH
5
-5
Gray brown sandy silt
TW4
N.
N.
SM/MH
10
-10
SZ WL (First Encountered)
Boring Started: Mar 14 2022
1 WL (Completion) 7.72
Boring Completed: Mar 14 2022
Remarks: Soil saturated at 8 feet bgs.
Logged By: DMarlor
Principal Engineer/
Roger Smith
Responsible PG:

Governors View Drive Soil and
Project Name: Sheet: 1 of 1 Boring No: TW5
Groundwater Assessment
Client: Buckeye Community Hope Foundation Project No.: 49:13699-D
to
Site Location: Governors View Drive, Ashevillle, North
Driller: CSI
Drill Rig: GeoProbe
Carolina 28805
Latitude/Longitude:
Elevation:
U0
c
i
m
LE
E
j
J
Depth/Elevation
7
v
Q
Soil Classification
Description
WELL CONSTRUCTION
of
Q
cc
E
a,
Q
12
(D
d
n
E
Gray brown sandy silt with organics
SM/MH
5
-5
Gray brown sandy silt
TW5
SM/MH
10
-10
<:
SZ WL (First Encountered)
Boring Started: Mar 14 2022
1 WL (Completion) 7.68
Boring Completed: Mar 14 2022
Remarks: Soil saturated at 8 feet bgs. Odors were observed at approximately 8
Logged By: DMarlor
feet bgs.
Principal Engineer/
Roger Smith
Responsible PG:

Governors View Drive Soil and
Project Name: Sheet: 1 of 1 Boring No: TW6
Groundwater Assessment
Client: Buckeye Community Hope Foundation Project No.: 49:13699-D
to
Site Location: Governors View Drive, Ashevillle, North
Driller: CSI
Drill Rig: GeoProbe
Carolina 28805
Latitude/Longitude:
Elevation:
U0
c
i
m
LE
E
j
J
Depth/Elevation
7
v
Q
Soil Classification
Description
WELL CONSTRUCTION
of
Q
cc
E
a,
Q
12
(D
Brown red sandy silt with organics
SM/MH
Brown red sandy silt
5
-5
N.
SM/MH
TW6
N.
Brown sandy silt
10
-10
<:
SM/MH
SZ WL (First Encountered)
Boring Started: Mar 14 2022
1 WL (Completion) 6.64
Boring Completed: Mar 14 2022
Remarks:
Logged By: DMarlor
Principal Engineer/
Roger Smith
Responsible PG:

APPENDIX C
Laboratory Analytical Reports with COC Documentation

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
March 29, 2022
Jim Bevers
ECS Southeast, LLP
1900 Hendersonville Road
Suite 10
Asheville, NC 28803
RE: Project: 49:13699-D
Pace Project No.: 92593947
Dear Jim Bevers:
Enclosed are the analytical results for sample(s) received by the laboratory on March 15, 2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
A revised laboratory report is being submitted on 3/29/22 to include MDLs and J values, per client request.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
c +1 , �-'a`-.oN
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Don Marlor, ECS Southeast
ECS Southeast Reporting, ECS Southeast
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: 49:13699-D
Pace Project No.: 92593947
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
VirginiaNELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE SUMMARY
Project: 49:13699-D
Pace Project No.: 92593947
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92593947001
TW-1
Water
03/14/2214:50
03/15/22 16:38
92593947002
TW-2
Water
03/14/2215:15
03/15/22 16:38
92593947003
TW-3
Water
03/14/2215:55
03/15/22 16:38
92593947004
TW-4
Water
03/14/2216:25
03/15/22 16:38
92593947005
TW-5
Water
03/14/2216:50
03/15/22 16:38
92593947006
TW-6
Water
03/14/2217:20
03/15/22 16:38
92593947007
SB-1
Solid
03/14/2213:48
03/15/22 16:38
92593947008
S13-2
Solid
03/15/22 08:17
03/15/22 16:38
92593947009
S13-3
Solid
03/15/22 08:37
03/15/22 16:38
92593947010
S13-4
Solid
03/15/22 08:51
03/15/22 16:38
92593947011
S13-5
Solid
03/15/22 09:15
03/15/22 16:38
92593947012
S13-6
Solid
03/15/22 09:32
03/15/22 16:38
92593947013
S13-7
Solid
03/15/22 09:53
03/15/22 16:38
92593947014
S13-8
Solid
03/15/2210:13
03/15/22 16:38
92593947015
S13-9
Solid
03/15/2210:35
03/15/22 16:38
92593947016
SB-10
Solid
03/15/2210:50
03/15/22 16:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
49:13699-D
92593947
Analytes
Lab lD
Sample ID
Method
Analysts
Reported
Laboratory
92593947001
TW-1
EPA 8270E
PKS
74
PASI-C
EPA 8260D
SAS
63
PASI-C
92593947002
TW-2
EPA 8270E
PKS
74
PASI-C
EPA 8260D
SAS
63
PASI-C
92593947003
TW-3
EPA 8270E
PKS
74
PASI-C
EPA 8260D
SAS
63
PASI-C
92593947004
TW-4
EPA 8270E
PKS
74
PASI-C
EPA 8260D
SAS
63
PASI-C
92593947005
TW-5
EPA 8270E
PKS
74
PASI-C
EPA 8260D
SAS
63
PASI-C
92593947006
TW-6
EPA 8270E
PKS
74
PASI-C
EPA 8260D
SAS
63
PASI-C
92593947007
S13-1
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
CL
70
PASI-C
SW-846
KDF
1
PASI-C
92593947008
SB-2
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
CL
70
PASI-C
SW-846
KDF
1
PASI-C
92593947009
S13-3
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
CL
70
PASI-C
SW-846
KDF
1
PASI-C
92593947010
S13-4
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
CL
70
PASI-C
SW-846
KDF
1
PASI-C
92593947011
S13-5
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
CL
70
PASI-C
SW-846
KDF
1
PASI-C
92593947012
S13-6
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
CL
70
PASI-C
SW-846
KDF
1
PASI-C
92593947013
S13-7
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
CL
70
PASI-C
SW-846
KDF
1
PASI-C
92593947014
S13-8
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
CL
70
PASI-C
SW-846
KDF
1
PASI-C
92593947015
SB-9
EPA 8270E
BPJ
75
PASI-C
REPORT OF LABORATORY ANALYSIS
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2225 Riverside Dr.
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[phone]
SAMPLE ANALYTE COUNT
Project:
49:13699-D
Pace Project No.:
92593947
Analytes
Lab lD
Sample ID
Method
Analysts
Reported
Laboratory
EPA 8260D
CL
70
PASI-C
SW-846
KDF
1
PASI-C
92593947016
SB-10
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
CL
70
PASI-C
SW-846
KDF
1
PASI-C
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 5 of 122

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SUMMARY OF DETECTION
Project:
Pace Project No.:
49:13699-D
92593947
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92593947004
TW-4
EPA 8270E
1-Methylnaphthalene
12.7
ug/L
10.0
03/18/2217:03
EPA 8270E
2-Methylnaphthalene
2.8J
ug/L
10.0
03/18/22 17:03
92593947005
TW-5
EPA 8270E
1-Methylnaphthalene
55.7
ug/L
9.1
03/18/22 17:28
EPA 8270E
2-Methylnaphthalene
102
ug/L
9.1
03/18/22 17:28
EPA 8270E
Naphthalene
59.1
ug/L
9.1
03/18/22 17:28
EPA 8260D
Ethylbenzene
128
ug/L
4.0
03/21/22 20:46
EPA 8260D
Naphthalene
116
ug/L
4.0
03/21/22 20:46
EPA 8260D
Toluene
2.OJ
ug/L
4.0
03/21/22 20:46
EPA 8260D
Xylene (Total)
301
ug/L
4.0
03/21/22 20:46
EPA 8260D
m&p-Xylene
240
ug/L
8.0
03/21/22 20:46
EPA 8260D
o-Xylene
60.9
ug/L
4.0
03/21/22 20:46
92593947006
TW-6
EPA 8270E
1-Methylnaphthalene
70.3
ug/L
9.1
03/21/2216:46
EPA 8270E
2-Methylnaphthalene
126
ug/L
9.1
03/21/2216:46
EPA 8270E
Naphthalene
186
ug/L
18.2
03/22/22 00:46
EPA 8260D
Benzene
5.1
ug/L
5.0
03/21/22 21:04
EPA 8260D
Ethylbenzene
193
ug/L
5.0
03/21/22 21:04
EPA 8260D
Naphthalene
307
ug/L
5.0
03/21/22 21:04
EPA 8260D
Xylene (Total)
865
ug/L
5.0
03/21/22 21:04
EPA 8260D
m&p-Xylene
804
ug/L
10.0
03/21/22 21:04
EPA 8260D
o-Xylene
60.8
ug/L
5.0
03/21/22 21:04
92593947007
S13-1
EPA 8270E
1-Methylnaphthalene
7.1
mg/kg
4.2
03/21/2213:44
EPA 8270E
2-Methylnaphthalene
13.8
mg/kg
4.2
03/21/2213:44
EPA 8270E
Naphthalene
8.5
mg/kg
4.2
03/21/2213:44
EPA 8260D
Benzene
0.17
mg/kg
0.039
03/22/22 01:02
EPA 8260D
n-Butylbenzene
3.2
mg/kg
0.039
03/22/22 01:02
EPA 8260D
sec-Butylbenzene
1.9
mg/kg
0.039
03/22/22 01:02
EPA 8260D
Ethylbenzene
11.1
mg/kg
0.039
03/22/22 01:02
EPA 8260D
Isopropylbenzene (Cumene)
1.4
mg/kg
0.039
03/22/22 01:02
EPA 8260D
p-Isopropyltoluene
2.7
mg/kg
0.039
03/22/22 01:02
EPA 8260D
Methylene Chloride
0.42
mg/kg
0.16
03/22/22 01:02 C7,v2
EPA 8260D
4-Methyl-2-pentanone (MIBK)
1.1
mg/kg
0.39
03/22/22 01:02
EPA 8260D
Naphthalene
11.3
mg/kg
0.039
03/22/22 01:02
EPA 8260D
n-Propylbenzene
4.0
mg/kg
0.039
03/22/22 01:02
EPA 8260D
Toluene
0.17
mg/kg
0.039
03/22/22 01:02
EPA 8260D
Trichloroethene
0.056
mg/kg
0.039
03/22/22 01:02
EPA 8260D
1,2,4-Trimethylbenzene
17.8
mg/kg
0.039
03/22/22 01:02
EPA 8260D
1,3,5-Trimethylbenzene
4.7
mg/kg
0.039
03/22/22 01:02
EPA 8260D
Xylene (Total)
6.1
mg/kg
0.078
03/22/22 01:02
EPA 8260D
m&p-Xylene
5.5
mg/kg
0.078
03/22/22 01:02
EPA 8260D
o-Xylene
0.54
mg/kg
0.039
03/22/22 01:02
SW-846
Percent Moisture
21.7
%
0.10
03/17/22 14:46 N2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 6 of 122

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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: 49:13699-D
Pace Project No.: 92593947
Lab Sample ID Client Sample ID
Method Parameters
SUMMARY OF DETECTION
Result Units Report Limit Analyzed Qualifiers
92593947008
S13-2
EPA 8260D
Acetone
0.051 J
mg/kg
0.14
03/18/22 15:45
C7,v2
EPA 8260D
Ethylbenzene
0.0049J
mg/kg
0.0072
03/18/22 15:45
M1
EPA 8260D
Naphthalene
0.016
mg/kg
0.0072
03/18/22 15:45
EPA 8260D
Toluene
0.015
mg/kg
0.0072
03/18/22 15:45
M1
EPA 8260D
1,2,4-Trimethylbenzene
0.0083
mg/kg
0.0072
03/18/22 15:45
M1
EPA 8260D
1,3,5-Trimethylbenzene
0.0044J
mg/kg
0.0072
03/18/22 15:45
M1
EPA 8260D
Xylene (Total)
0.032
mg/kg
0.014
03/18/22 15:45
MS
EPA 8260D
m&p-Xylene
0.021
mg/kg
0.014
03/18/22 15:45
M1
EPA 8260D
o-Xylene
0.012
mg/kg
0.0072
03/18/22 15:45
M1
SW-846
Percent Moisture
17.2
%
0.10
03/17/22 14:46
N2
92593947009
S13-3
SW-846
Percent Moisture
19.5
%
0.10
03/17/22 14:46
N2
92593947010
S13-4
EPA 8260D
Ethylbenzene
0.0036J
mg/kg
0.0066
03/18/22 17:31
EPA 8260D
Naphthalene
0.0065J
mg/kg
0.0066
03/18/22 17:31
EPA 8260D
Toluene
0.0079
mg/kg
0.0066
03/18/22 17:31
EPA 8260D
1,2,4-Trimethylbenzene
0.0046J
mg/kg
0.0066
03/18/22 17:31
EPA 8260D
m&p-Xylene
0.0081 J
mg/kg
0.013
03/18/22 17:31
EPA 8260D
o-Xylene
0.0046J
mg/kg
0.0066
03/18/22 17:31
SW-846
Percent Moisture
16.5
%
0.10
03/17/22 14:46
N2
92593947011
S13-5
SW-846
Percent Moisture
21.1
%
0.10
03/17/22 14:46
N2
92593947012
S13-6
EPA 8260D
Ethylbenzene
0.0041 J
mg/kg
0.0061
03/18/22 18:06
EPA 8260D
Naphthalene
0.012
mg/kg
0.0061
03/18/22 18:06
EPA 8260D
Toluene
0.012
mg/kg
0.0061
03/18/22 18:06
EPA 8260D
1,2,4-Trimethylbenzene
0.0064
mg/kg
0.0061
03/18/22 18:06
EPA 8260D
Xylene (Total)
0.024
mg/kg
0.012
03/18/22 18:06
EPA 8260D
m&p-Xylene
0.015
mg/kg
0.012
03/18/22 18:06
EPA 8260D
o-Xylene
0.0093
mg/kg
0.0061
03/18/22 18:06
SW-846
Percent Moisture
14.1
%
0.10
03/17/22 14:46
N2
92593947013
S13-7
SW-846
Percent Moisture
9.8
%
0.10
03/17/22 14:46
N2
92593947014
S13-8
EPA 8260D
Naphthalene
0.0068J
mg/kg
0.0089
03/18/22 18:41
EPA 8260D
n-Propylbenzene
0.0098
mg/kg
0.0089
03/18/22 18:41
EPA 8260D
Toluene
0.0060J
mg/kg
0.0089
03/18/22 18:41
EPA 8260D
1,2,4-Trimethylbenzene
0.0045J
mg/kg
0.0089
03/18/22 18:41
EPA 8260D
m&p-Xylene
0.011 J
mg/kg
0.018
03/18/22 18:41
SW-846
Percent Moisture
22.4
%
0.10
03/17/22 14:46
N2
92593947015
S13-9
EPA 8260D
Acetone
0.074J
mg/kg
0.19
03/18/22 18:59
C7,v2
EPA 8260D
sec-Butylbenzene
0.0063J
mg/kg
0.0095
03/18/22 18:59
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 7 of 122

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SUMMARY OF DETECTION
Project:
Pace Project No.:
49:13699-D
92593947
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92593947015
S13-9
EPA 8260D
Ethylbenzene
0.0053J
mg/kg
0.0095
03/18/22 18:59
EPA 8260D
Isopropylbenzene (Cumene)
0.0036J
mg/kg
0.0095
03/18/22 18:59
EPA 8260D
n-Propylbenzene
0.011
mg/kg
0.0095
03/18/22 18:59
EPA 8260D
Toluene
0.016
mg/kg
0.0095
03/18/22 18:59
EPA 8260D
m&p-Xylene
0.011 J
mg/kg
0.019
03/18/22 18:59
SW-846
Percent Moisture
9.6
%
0.10
03/17/22 14:46 N2
92593947016
SB-10
EPA 8260D
Ethylbenzene
0.00511
mg/kg
0.0084
03/18/22 19:17
EPA 8260D
Naphthalene
0.016
mg/kg
0.0084
03/18/22 19:17
EPA 8260D
Toluene
0.0073J
mg/kg
0.0084
03/18/22 19:17
EPA 8260D
1,2,4-Trimethylbenzene
0.0099
mg/kg
0.0084
03/18/22 19:17
EPA 8260D
Xylene (Total)
0.012J
mg/kg
0.017
03/18/22 19:17
EPA 8260D
m&p-Xylene
0.016J
mg/kg
0.017
03/18/22 19:17
EPA 8260D
o-Xylene
0.012
mg/kg
0.0084
03/18/22 19:17
SW-846
Percent Moisture
17.4
%
0.10
03/17/22 14:47 N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 122

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Asheville, NC 28804
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ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-1 Lab ID: 92593947001 Collected: 03/14/22 14:50 Received: 03/15/22 16:38 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Acenaphthene
ND
ug/L
8.3
1.7
1
03/18/22 05:16
03/18/22 15:47
83-32-9
Acenaphthylene
ND
ug/L
8.3
1.6
1
03/18/22 05:16
03/18/22 15:47
208-96-8
Aniline
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 15:47
62-53-3
Anthracene
ND
ug/L
8.3
1.9
1
03/18/22 05:16
03/18/22 15:47
120-12-7
Benzo(a)anthracene
ND
ug/L
8.3
2.2
1
03/18/22 05:16
03/18/22 15:47
56-55-3
Benzo(a)pyrene
ND
ug/L
8.3
2.3
1
03/18/22 05:16
03/18/22 15:47
50-32-8
Benzo(b)fluoranthene
ND
ug/L
8.3
2.2
1
03/18/22 05:16
03/18/22 15:47
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
8.3
2.4
1
03/18/22 05:16
03/18/22 15:47
191-24-2
Benzo(k)fluoranthene
ND
ug/L
8.3
2.3
1
03/18/22 05:16
03/18/22 15:47
207-08-9
Benzoic Acid
ND
ug/L
41.7
2.8
1
03/18/22 05:16
03/18/22 15:47
65-85-0
Benzyl alcohol
ND
ug/L
16.7
2.4
1
03/18/22 05:16
03/18/22 15:47
100-51-6
4-Bromophenylphenyl ether
ND
ug/L
8.3
1.5
1
03/18/22 05:16
03/18/22 15:47
101-55-3
Butylbenzylphthalate
ND
ug/L
8.3
2.6
1
03/18/22 05:16
03/18/22 15:47
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
8.3
2.8
1
03/18/22 05:16
03/18/22 15:47
59-50-7
4-Chloroaniline
ND
ug/L
16.7
3.0
1
03/18/22 05:16
03/18/22 15:47
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
8.3
1.5
1
03/18/22 05:16
03/18/22 15:47
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
8.3
1.6
1
03/18/22 05:16
03/18/22 15:47
111-44-4
2-Chloronaphthalene
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 15:47
91-58-7
2-Chlorophenol
ND
ug/L
8.3
1.0
1
03/18/22 05:16
03/18/22 15:47
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
8.3
1.7
1
03/18/22 05:16
03/18/22 15:47
7005-72-3
Chrysene
ND
ug/L
8.3
2.3
1
03/18/22 05:16
03/18/22 15:47
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
8.3
2.5
1
03/18/22 05:16
03/18/22 15:47
53-70-3
Dibenzofuran
ND
ug/L
8.3
1.8
1
03/18/22 05:16
03/18/22 15:47
132-64-9
1,2-Dichlorobenzene
ND
ug/L
8.3
1.5
1
03/18/22 05:16
03/18/22 15:47
95-50-1
1,3-Dichlorobenzene
ND
ug/L
8.3
1.3
1
03/18/22 05:16
03/18/22 15:47
541-73-1
1,4-Dichlorobenzene
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 15:47
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
16.7
6.8
1
03/18/22 05:16
03/18/22 15:47
91-94-1
2,4-Dichlorophenol
ND
ug/L
8.3
1.2
1
03/18/22 05:16
03/18/22 15:47
120-83-2
Diethylphthalate
ND
ug/L
8.3
1.7
1
03/18/22 05:16
03/18/22 15:47
84-66-2
2,4-Dimethylphenol
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 15:47
105-67-9
Dimethylphthalate
ND
ug/L
8.3
1.8
1
03/18/22 05:16
03/18/22 15:47
131-11-3
Di-n-butylphthalate
ND
ug/L
8.3
1.8
1
03/18/22 05:16
03/18/22 15:47
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
16.7
2.8
1
03/18/22 05:16
03/18/22 15:47
534-52-1
2,4-Dinitrophenol
ND
ug/L
41.7
21.7
1
03/18/22 05:16
03/18/22 15:47
51-28-5
2,4-Dinitrotoluene
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 15:47
121-14-2
2,6-Dinitrotoluene
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 15:47
606-20-2
Di-n-octylphthalate
ND
ug/L
8.3
3.3
1
03/18/22 05:16
03/18/22 15:47
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.0
3.1
1
03/18/22 05:16
03/18/22 15:47
117-81-7
Fluoranthene
ND
ug/L
8.3
1.8
1
03/18/22 05:16
03/18/22 15:47
206-44-0
Fluorene
ND
ug/L
8.3
1.7
1
03/18/22 05:16
03/18/22 15:47
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
8.3
1.5
1
03/18/22 05:16
03/18/22 15:47
87-68-3
Hexachlorobenzene
ND
ug/L
8.3
1.8
1
03/18/22 05:16
03/18/22 15:47
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
8.3
1.3
1
03/18/22 05:16
03/18/22 15:47
77-47-4
Hexachloroethane
ND
ug/L
8.3
1.2
1
03/18/22 05:16
03/18/22 15:47
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
8.3
2.4
1
03/18/22 05:16
03/18/22 15:47
193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 122

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Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-1 Lab ID: 92593947001 Collected: 03/14/22 14:50 Received: 03/15/22 16:38 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E RVE
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Date: 03/29/2022 06:07 AM
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services
- Charlotte
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 15:47
78-59-1
ND
ug/L
8.3
1.7
1
03/18/22 05:16
03/18/22 15:47
90-12-0
ND
ug/L
8.3
1.6
1
03/18/22 05:16
03/18/22 15:47
91-57-6
ND
ug/L
8.3
1.6
1
03/18/22 05:16
03/18/22 15:47
95-48-7
ND
ug/L
8.3
1.0
1
03/18/22 05:16
03/18/22 15:47
15831-10-4
ND
ug/L
8.3
1.7
1
03/18/22 05:16
03/18/22 15:47
91-20-3
ND
ug/L
16.7
2.5
1
03/18/22 05:16
03/18/22 15:47
88-74-4
ND
ug/L
16.7
3.1
1
03/18/22 05:16
03/18/22 15:47
99-09-2
ND
ug/L
16.7
4.2
1
03/18/22 05:16
03/18/22 15:47
100-01-6
ND
ug/L
8.3
1.6
1
03/18/22 05:16
03/18/22 15:47
98-95-3
ND
ug/L
8.3
1.2
1
03/18/22 05:16
03/18/22 15:47
88-75-5
ND
ug/L
41.7
5.5
1
03/18/22 05:16
03/18/22 15:47
100-02-7
ND
ug/L
8.3
1.6
1
03/18/22 05:16
03/18/22 15:47
62-75-9
ND
ug/L
8.3
1.1
1
03/18/22 05:16
03/18/22 15:47
621-64-7
ND
ug/L
8.3
2.5
1
03/18/22 05:16
03/18/22 15:47
86-30-6
ND
ug/L
8.3
0.96
1
03/18/22 05:16
03/18/22 15:47
108-60-1
ND
ug/L
16.7
3.1
1
03/18/22 05:16
03/18/22 15:47
87-86-5
ND
ug/L
8.3
1.7
1
03/18/22 05:16
03/18/22 15:47
85-01-8
ND
ug/L
8.3
1.1
1
03/18/22 05:16
03/18/22 15:47
108-95-2
ND
ug/L
8.3
1.8
1
03/18/22 05:16
03/18/22 15:47
129-00-0
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 15:47
120-82-1
ND
ug/L
8.3
1.2
1
03/18/22 05:16
03/18/22 15:47
95-95-4
ND
ug/L
8.3
1.3
1
03/18/22 05:16
03/18/22 15:47
88-06-2
76
%
10-144
1
03/18/22 05:16
03/18/22 15:47
4165-60-0
70
%
10-130
1
03/18/22 05:16
03/18/22 15:47
321-60-8
112
%
34-163
1
03/18/22 05:16
03/18/22 15:47
1718-51-0
34
%
10-130
1
03/18/22 05:16
03/18/22 15:47
13127-88-3
34
%
10-130
1
03/18/22 05:16
03/18/22 15:47
367-12-4
36
%
10-144
1
03/18/22 05:16
03/18/22 15:47
118-79-6
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
ND
ug/L
25.0
5.1
1
03/18/2217:15
67-64-1
ND
ug/L
1.0
0.34
1
03/18/2217:15
71-43-2
ND
ug/L
1.0
0.29
1
03/18/2217:15
108-86-1
ND
ug/L
1.0
0.47
1
03/18/2217:15
74-97-5
ND
ug/L
1.0
0.31
1
03/18/2217:15
75-27-4
ND
ug/L
1.0
0.34
1
03/18/2217:15
75-25-2
ND
ug/L
2.0
1.7
1
03/18/2217:15
74-83-9
ND
ug/L
5.0
4.0
1
03/18/2217:15
78-93-3
ND
ug/L
1.0
0.33
1
03/18/2217:15
56-23-5
ND
ug/L
1.0
0.28
1
03/18/2217:15
108-90-7
ND
ug/L
1.0
0.65
1
03/18/2217:15
75-00-3
ND
ug/L
1.0
0.43
1
03/18/2217:15
67-66-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
L1
Page 10 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-1 Lab ID: 92593947001 Collected: 03/14/22 14:50 Received: 03/15/22 16:38 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Date: 03/29/2022 06:07 AM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.54
1
03/18/2217:15
74-87-3
ND
ug/L
1.0
0.32
1
03/18/2217:15
95-49-8
ND
ug/L
1.0
0.32
1
03/18/2217:15
106-43-4
ND
ug/L
2.0
0.34
1
03/18/2217:15
96-12-8
ND
ug/L
1.0
0.36
1
03/18/2217:15
124-48-1
ND
ug/L
1.0
0.27
1
03/18/2217:15
106-93-4
ND
ug/L
1.0
0.39
1
03/18/2217:15
74-95-3
ND
ug/L
1.0
0.34
1
03/18/2217:15
95-50-1
ND
ug/L
1.0
0.34
1
03/18/2217:15
541-73-1
ND
ug/L
1.0
0.33
1
03/18/2217:15
106-46-7
ND
ug/L
1.0
0.35
1
03/18/2217:15
75-71-8
ND
ug/L
1.0
0.37
1
03/18/2217:15
75-34-3
ND
ug/L
1.0
0.32
1
03/18/2217:15
107-06-2
ND
ug/L
1.0
0.35
1
03/18/2217:15
75-35-4
ND
ug/L
1.0
0.38
1
03/18/2217:15
156-59-2
ND
ug/L
1.0
0.40
1
03/18/2217:15
156-60-5
ND
ug/L
1.0
0.36
1
03/18/2217:15
78-87-5
ND
ug/L
1.0
0.28
1
03/18/2217:15
142-28-9
ND
ug/L
1.0
0.39
1
03/18/2217:15
594-20-7
ND
ug/L
1.0
0.43
1
03/18/2217:15
563-58-6
ND
ug/L
1.0
0.36
1
03/18/2217:15
10061-01-5
ND
ug/L
1.0
0.36
1
03/18/2217:15
10061-02-6
ND
ug/L
1.0
0.31
1
03/18/2217:15
108-20-3
ND
ug/L
1.0
0.30
1
03/18/2217:15
100-41-4
ND
ug/L
2.0
1.5
1
03/18/2217:15
87-68-3
ND
ug/L
5.0
0.48
1
03/18/2217:15
591-78-6
ND
ug/L
1.0
0.41
1
03/18/2217:15
99-87-6
ND
ug/L
5.0
2.0
1
03/18/2217:15
75-09-2
ND
ug/L
5.0
2.7
1
03/18/2217:15
108-10-1
ND
ug/L
1.0
0.42
1
03/18/2217:15
1634-04-4
ND
ug/L
1.0
0.64
1
03/18/2217:15
91-20-3
ND
ug/L
1.0
0.29
1
03/18/2217:15
100-42-5
ND
ug/L
1.0
0.31
1
03/18/2217:15
630-20-6
ND
ug/L
1.0
0.22
1
03/18/2217:15
79-34-5
ND
ug/L
1.0
0.29
1
03/18/2217:15
127-18-4
ND
ug/L
1.0
0.48
1
03/18/2217:15
108-88-3
ND
ug/L
1.0
0.81
1
03/18/2217:15
87-61-6
ND
ug/L
1.0
0.64
1
03/18/2217:15
120-82-1
ND
ug/L
1.0
0.33
1
03/18/2217:15
71-55-6
ND
ug/L
1.0
0.32
1
03/18/2217:15
79-00-5
ND
ug/L
1.0
0.38
1
03/18/2217:15
79-01-6
ND
ug/L
1.0
0.30
1
03/18/2217:15
75-69-4
ND
ug/L
1.0
0.26
1
03/18/2217:15
96-18-4
ND
ug/L
2.0
1.3
1
03/18/2217:15
108-05-4
ND
ug/L
1.0
0.39
1
03/18/2217:15
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v3
v1
Page 11 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-1
Lab ID:
92593947001
Collected:
03/14/22 14:50
Received: 03/15/22 16:38 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical
Method: EPA 8260D
Pace Analytical
Services
- Charlotte
Xylene (Total)
ND
ug/L
1.0
0.34
1
03/18/22 17:15
1330-20-7
m&p-Xylene
ND
ug/L
2.0
0.71
1
03/18/22 17:15
179601-23-1
o-Xylene
ND
ug/L
1.0
0.34
1
03/18/22 17:15
95-47-6
Surrogates
4-Bromofluorobenzene (S)
95
%
70-130
1
03/18/22 17:15
460-00-4
1,2-Dichloroethane-d4 (S)
91
%
70-130
1
03/18/22 17:15
17060-07-0
Toluene-d8 (S)
105
%
70-130
1
03/18/22 17:15
2037-26-5
Date: 03/29/2022 06:07 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-2 Lab ID: 92593947002 Collected: 03/14/22 15:15 Received: 03/15/22 16:38 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Acenaphthene
ND
ug/L
8.3
1.7
1
03/18/22 05:16
03/18/22 16:13
83-32-9
Acenaphthylene
ND
ug/L
8.3
1.6
1
03/18/22 05:16
03/18/22 16:13
208-96-8
Aniline
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 16:13
62-53-3
Anthracene
ND
ug/L
8.3
1.9
1
03/18/22 05:16
03/18/22 16:13
120-12-7
Benzo(a)anthracene
ND
ug/L
8.3
2.2
1
03/18/22 05:16
03/18/22 16:13
56-55-3
Benzo(a)pyrene
ND
ug/L
8.3
2.3
1
03/18/22 05:16
03/18/22 16:13
50-32-8
Benzo(b)fluoranthene
ND
ug/L
8.3
2.2
1
03/18/22 05:16
03/18/22 16:13
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
8.3
2.4
1
03/18/22 05:16
03/18/22 16:13
191-24-2
Benzo(k)fluoranthene
ND
ug/L
8.3
2.3
1
03/18/22 05:16
03/18/22 16:13
207-08-9
Benzoic Acid
ND
ug/L
41.7
2.8
1
03/18/22 05:16
03/18/22 16:13
65-85-0
Benzyl alcohol
ND
ug/L
16.7
2.4
1
03/18/22 05:16
03/18/22 16:13
100-51-6
4-Bromophenylphenyl ether
ND
ug/L
8.3
1.5
1
03/18/22 05:16
03/18/22 16:13
101-55-3
Butylbenzylphthalate
ND
ug/L
8.3
2.6
1
03/18/22 05:16
03/18/22 16:13
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
8.3
2.8
1
03/18/22 05:16
03/18/22 16:13
59-50-7
4-Chloroaniline
ND
ug/L
16.7
3.0
1
03/18/22 05:16
03/18/22 16:13
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
8.3
1.5
1
03/18/22 05:16
03/18/22 16:13
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
8.3
1.6
1
03/18/22 05:16
03/18/22 16:13
111-44-4
2-Chloronaphthalene
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 16:13
91-58-7
2-Chlorophenol
ND
ug/L
8.3
1.0
1
03/18/22 05:16
03/18/22 16:13
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
8.3
1.7
1
03/18/22 05:16
03/18/22 16:13
7005-72-3
Chrysene
ND
ug/L
8.3
2.3
1
03/18/22 05:16
03/18/22 16:13
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
8.3
2.5
1
03/18/22 05:16
03/18/22 16:13
53-70-3
Dibenzofuran
ND
ug/L
8.3
1.8
1
03/18/22 05:16
03/18/22 16:13
132-64-9
1,2-Dichlorobenzene
ND
ug/L
8.3
1.5
1
03/18/22 05:16
03/18/22 16:13
95-50-1
1,3-Dichlorobenzene
ND
ug/L
8.3
1.3
1
03/18/22 05:16
03/18/22 16:13
541-73-1
1,4-Dichlorobenzene
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 16:13
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
16.7
6.8
1
03/18/22 05:16
03/18/22 16:13
91-94-1
2,4-Dichlorophenol
ND
ug/L
8.3
1.2
1
03/18/22 05:16
03/18/22 16:13
120-83-2
Diethylphthalate
ND
ug/L
8.3
1.7
1
03/18/22 05:16
03/18/22 16:13
84-66-2
2,4-Dimethylphenol
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 16:13
105-67-9
Dimethylphthalate
ND
ug/L
8.3
1.8
1
03/18/22 05:16
03/18/22 16:13
131-11-3
Di-n-butylphthalate
ND
ug/L
8.3
1.8
1
03/18/22 05:16
03/18/22 16:13
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
16.7
2.8
1
03/18/22 05:16
03/18/22 16:13
534-52-1
2,4-Dinitrophenol
ND
ug/L
41.7
21.7
1
03/18/22 05:16
03/18/22 16:13
51-28-5
2,4-Dinitrotoluene
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 16:13
121-14-2
2,6-Dinitrotoluene
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 16:13
606-20-2
Di-n-octylphthalate
ND
ug/L
8.3
3.3
1
03/18/22 05:16
03/18/22 16:13
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.0
3.1
1
03/18/22 05:16
03/18/22 16:13
117-81-7
Fluoranthene
ND
ug/L
8.3
1.8
1
03/18/22 05:16
03/18/22 16:13
206-44-0
Fluorene
ND
ug/L
8.3
1.7
1
03/18/22 05:16
03/18/22 16:13
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
8.3
1.5
1
03/18/22 05:16
03/18/22 16:13
87-68-3
Hexachlorobenzene
ND
ug/L
8.3
1.8
1
03/18/22 05:16
03/18/22 16:13
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
8.3
1.3
1
03/18/22 05:16
03/18/22 16:13
77-47-4
Hexachloroethane
ND
ug/L
8.3
1.2
1
03/18/22 05:16
03/18/22 16:13
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
8.3
2.4
1
03/18/22 05:16
03/18/22 16:13
193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-2 Lab ID: 92593947002 Collected: 03/14/22 15:15 Received: 03/15/22 16:38 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E RVE
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Date: 03/29/2022 06:07 AM
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services
- Charlotte
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 16:13
78-59-1
ND
ug/L
8.3
1.7
1
03/18/22 05:16
03/18/22 16:13
90-12-0
ND
ug/L
8.3
1.6
1
03/18/22 05:16
03/18/22 16:13
91-57-6
ND
ug/L
8.3
1.6
1
03/18/22 05:16
03/18/22 16:13
95-48-7
ND
ug/L
8.3
1.0
1
03/18/22 05:16
03/18/22 16:13
15831-10-4
ND
ug/L
8.3
1.7
1
03/18/22 05:16
03/18/22 16:13
91-20-3
ND
ug/L
16.7
2.5
1
03/18/22 05:16
03/18/22 16:13
88-74-4
ND
ug/L
16.7
3.1
1
03/18/22 05:16
03/18/22 16:13
99-09-2
ND
ug/L
16.7
4.2
1
03/18/22 05:16
03/18/22 16:13
100-01-6
ND
ug/L
8.3
1.6
1
03/18/22 05:16
03/18/22 16:13
98-95-3
ND
ug/L
8.3
1.2
1
03/18/22 05:16
03/18/22 16:13
88-75-5
ND
ug/L
41.7
5.5
1
03/18/22 05:16
03/18/22 16:13
100-02-7
ND
ug/L
8.3
1.6
1
03/18/22 05:16
03/18/22 16:13
62-75-9
ND
ug/L
8.3
1.1
1
03/18/22 05:16
03/18/22 16:13
621-64-7
ND
ug/L
8.3
2.5
1
03/18/22 05:16
03/18/22 16:13
86-30-6
ND
ug/L
8.3
0.96
1
03/18/22 05:16
03/18/22 16:13
108-60-1
ND
ug/L
16.7
3.1
1
03/18/22 05:16
03/18/22 16:13
87-86-5
ND
ug/L
8.3
1.7
1
03/18/22 05:16
03/18/22 16:13
85-01-8
ND
ug/L
8.3
1.1
1
03/18/22 05:16
03/18/22 16:13
108-95-2
ND
ug/L
8.3
1.8
1
03/18/22 05:16
03/18/22 16:13
129-00-0
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 16:13
120-82-1
ND
ug/L
8.3
1.2
1
03/18/22 05:16
03/18/22 16:13
95-95-4
ND
ug/L
8.3
1.3
1
03/18/22 05:16
03/18/22 16:13
88-06-2
100
%
10-144
1
03/18/22 05:16
03/18/22 16:13
4165-60-0
94
%
10-130
1
03/18/22 05:16
03/18/22 16:13
321-60-8
113
%
34-163
1
03/18/22 05:16
03/18/22 16:13
1718-51-0
46
%
10-130
1
03/18/22 05:16
03/18/22 16:13
13127-88-3
48
%
10-130
1
03/18/22 05:16
03/18/22 16:13
367-12-4
48
%
10-144
1
03/18/22 05:16
03/18/22 16:13
118-79-6
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
ND
ug/L
25.0
5.1
1
03/18/2217:33
67-64-1
ND
ug/L
1.0
0.34
1
03/18/2217:33
71-43-2
ND
ug/L
1.0
0.29
1
03/18/2217:33
108-86-1
ND
ug/L
1.0
0.47
1
03/18/2217:33
74-97-5
ND
ug/L
1.0
0.31
1
03/18/2217:33
75-27-4
ND
ug/L
1.0
0.34
1
03/18/2217:33
75-25-2
ND
ug/L
2.0
1.7
1
03/18/2217:33
74-83-9
ND
ug/L
5.0
4.0
1
03/18/2217:33
78-93-3
ND
ug/L
1.0
0.33
1
03/18/2217:33
56-23-5
ND
ug/L
1.0
0.28
1
03/18/2217:33
108-90-7
ND
ug/L
1.0
0.65
1
03/18/2217:33
75-00-3
ND
ug/L
1.0
0.43
1
03/18/2217:33
67-66-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
L1
Page 14 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-2 Lab ID: 92593947002 Collected: 03/14/22 15:15 Received: 03/15/22 16:38 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Date: 03/29/2022 06:07 AM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.54
1
03/18/2217:33
74-87-3
ND
ug/L
1.0
0.32
1
03/18/2217:33
95-49-8
ND
ug/L
1.0
0.32
1
03/18/2217:33
106-43-4
ND
ug/L
2.0
0.34
1
03/18/2217:33
96-12-8
ND
ug/L
1.0
0.36
1
03/18/2217:33
124-48-1
ND
ug/L
1.0
0.27
1
03/18/2217:33
106-93-4
ND
ug/L
1.0
0.39
1
03/18/2217:33
74-95-3
ND
ug/L
1.0
0.34
1
03/18/2217:33
95-50-1
ND
ug/L
1.0
0.34
1
03/18/2217:33
541-73-1
ND
ug/L
1.0
0.33
1
03/18/2217:33
106-46-7
ND
ug/L
1.0
0.35
1
03/18/2217:33
75-71-8
ND
ug/L
1.0
0.37
1
03/18/2217:33
75-34-3
ND
ug/L
1.0
0.32
1
03/18/2217:33
107-06-2
ND
ug/L
1.0
0.35
1
03/18/2217:33
75-35-4
ND
ug/L
1.0
0.38
1
03/18/2217:33
156-59-2
ND
ug/L
1.0
0.40
1
03/18/2217:33
156-60-5
ND
ug/L
1.0
0.36
1
03/18/2217:33
78-87-5
ND
ug/L
1.0
0.28
1
03/18/2217:33
142-28-9
ND
ug/L
1.0
0.39
1
03/18/2217:33
594-20-7
ND
ug/L
1.0
0.43
1
03/18/2217:33
563-58-6
ND
ug/L
1.0
0.36
1
03/18/2217:33
10061-01-5
ND
ug/L
1.0
0.36
1
03/18/2217:33
10061-02-6
ND
ug/L
1.0
0.31
1
03/18/2217:33
108-20-3
ND
ug/L
1.0
0.30
1
03/18/2217:33
100-41-4
ND
ug/L
2.0
1.5
1
03/18/2217:33
87-68-3
ND
ug/L
5.0
0.48
1
03/18/2217:33
591-78-6
ND
ug/L
1.0
0.41
1
03/18/2217:33
99-87-6
ND
ug/L
5.0
2.0
1
03/18/2217:33
75-09-2
ND
ug/L
5.0
2.7
1
03/18/2217:33
108-10-1
ND
ug/L
1.0
0.42
1
03/18/2217:33
1634-04-4
ND
ug/L
1.0
0.64
1
03/18/2217:33
91-20-3
ND
ug/L
1.0
0.29
1
03/18/2217:33
100-42-5
ND
ug/L
1.0
0.31
1
03/18/2217:33
630-20-6
ND
ug/L
1.0
0.22
1
03/18/2217:33
79-34-5
ND
ug/L
1.0
0.29
1
03/18/2217:33
127-18-4
ND
ug/L
1.0
0.48
1
03/18/2217:33
108-88-3
ND
ug/L
1.0
0.81
1
03/18/2217:33
87-61-6
ND
ug/L
1.0
0.64
1
03/18/2217:33
120-82-1
ND
ug/L
1.0
0.33
1
03/18/2217:33
71-55-6
ND
ug/L
1.0
0.32
1
03/18/2217:33
79-00-5
ND
ug/L
1.0
0.38
1
03/18/2217:33
79-01-6
ND
ug/L
1.0
0.30
1
03/18/2217:33
75-69-4
ND
ug/L
1.0
0.26
1
03/18/2217:33
96-18-4
ND
ug/L
2.0
1.3
1
03/18/2217:33
108-05-4
ND
ug/L
1.0
0.39
1
03/18/2217:33
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 15 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-2
Lab ID:
92593947002
Collected:
03/14/22 15:15
Received: 03/15/22 16:38 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical
Method: EPA 8260D
Pace Analytical
Services
- Charlotte
Xylene (Total)
ND
ug/L
1.0
0.34
1
03/18/22 17:33
1330-20-7
m&p-Xylene
ND
ug/L
2.0
0.71
1
03/18/22 17:33
179601-23-1
o-Xylene
ND
ug/L
1.0
0.34
1
03/18/22 17:33
95-47-6
Surrogates
4-Bromofluorobenzene (S)
95
%
70-130
1
03/18/22 17:33
460-00-4
1,2-Dichloroethane-d4 (S)
89
%
70-130
1
03/18/22 17:33
17060-07-0
Toluene-d8 (S)
104
%
70-130
1
03/18/22 17:33
2037-26-5
Date: 03/29/2022 06:07 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 16 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-3 Lab ID: 92593947003 Collected: 03/14/22 15:55 Received: 03/15/22 16:38 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Acenaphthene
ND
ug/L
8.3
1.7
1
03/18/22 05:16
03/18/22 16:38
83-32-9
Acenaphthylene
ND
ug/L
8.3
1.6
1
03/18/22 05:16
03/18/22 16:38
208-96-8
Aniline
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 16:38
62-53-3
Anthracene
ND
ug/L
8.3
1.9
1
03/18/22 05:16
03/18/22 16:38
120-12-7
Benzo(a)anthracene
ND
ug/L
8.3
2.2
1
03/18/22 05:16
03/18/22 16:38
56-55-3
Benzo(a)pyrene
ND
ug/L
8.3
2.3
1
03/18/22 05:16
03/18/22 16:38
50-32-8
Benzo(b)fluoranthene
ND
ug/L
8.3
2.2
1
03/18/22 05:16
03/18/22 16:38
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
8.3
2.4
1
03/18/22 05:16
03/18/22 16:38
191-24-2
Benzo(k)fluoranthene
ND
ug/L
8.3
2.3
1
03/18/22 05:16
03/18/22 16:38
207-08-9
Benzoic Acid
ND
ug/L
41.7
2.8
1
03/18/22 05:16
03/18/22 16:38
65-85-0
Benzyl alcohol
ND
ug/L
16.7
2.4
1
03/18/22 05:16
03/18/22 16:38
100-51-6
4-Bromophenylphenyl ether
ND
ug/L
8.3
1.5
1
03/18/22 05:16
03/18/22 16:38
101-55-3
Butylbenzylphthalate
ND
ug/L
8.3
2.6
1
03/18/22 05:16
03/18/22 16:38
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
8.3
2.8
1
03/18/22 05:16
03/18/22 16:38
59-50-7
4-Chloroaniline
ND
ug/L
16.7
3.0
1
03/18/22 05:16
03/18/22 16:38
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
8.3
1.5
1
03/18/22 05:16
03/18/22 16:38
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
8.3
1.6
1
03/18/22 05:16
03/18/22 16:38
111-44-4
2-Chloronaphthalene
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 16:38
91-58-7
2-Chlorophenol
ND
ug/L
8.3
1.0
1
03/18/22 05:16
03/18/22 16:38
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
8.3
1.7
1
03/18/22 05:16
03/18/22 16:38
7005-72-3
Chrysene
ND
ug/L
8.3
2.3
1
03/18/22 05:16
03/18/22 16:38
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
8.3
2.5
1
03/18/22 05:16
03/18/22 16:38
53-70-3
Dibenzofuran
ND
ug/L
8.3
1.8
1
03/18/22 05:16
03/18/22 16:38
132-64-9
1,2-Dichlorobenzene
ND
ug/L
8.3
1.5
1
03/18/22 05:16
03/18/22 16:38
95-50-1
1,3-Dichlorobenzene
ND
ug/L
8.3
1.3
1
03/18/22 05:16
03/18/22 16:38
541-73-1
1,4-Dichlorobenzene
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 16:38
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
16.7
6.8
1
03/18/22 05:16
03/18/22 16:38
91-94-1
2,4-Dichlorophenol
ND
ug/L
8.3
1.2
1
03/18/22 05:16
03/18/22 16:38
120-83-2
Diethylphthalate
ND
ug/L
8.3
1.7
1
03/18/22 05:16
03/18/22 16:38
84-66-2
2,4-Dimethylphenol
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 16:38
105-67-9
Dimethylphthalate
ND
ug/L
8.3
1.8
1
03/18/22 05:16
03/18/22 16:38
131-11-3
Di-n-butylphthalate
ND
ug/L
8.3
1.8
1
03/18/22 05:16
03/18/22 16:38
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
16.7
2.8
1
03/18/22 05:16
03/18/22 16:38
534-52-1
2,4-Dinitrophenol
ND
ug/L
41.7
21.7
1
03/18/22 05:16
03/18/22 16:38
51-28-5
2,4-Dinitrotoluene
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 16:38
121-14-2
2,6-Dinitrotoluene
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 16:38
606-20-2
Di-n-octylphthalate
ND
ug/L
8.3
3.3
1
03/18/22 05:16
03/18/22 16:38
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.0
3.1
1
03/18/22 05:16
03/18/22 16:38
117-81-7
Fluoranthene
ND
ug/L
8.3
1.8
1
03/18/22 05:16
03/18/22 16:38
206-44-0
Fluorene
ND
ug/L
8.3
1.7
1
03/18/22 05:16
03/18/22 16:38
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
8.3
1.5
1
03/18/22 05:16
03/18/22 16:38
87-68-3
Hexachlorobenzene
ND
ug/L
8.3
1.8
1
03/18/22 05:16
03/18/22 16:38
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
8.3
1.3
1
03/18/22 05:16
03/18/22 16:38
77-47-4
Hexachloroethane
ND
ug/L
8.3
1.2
1
03/18/22 05:16
03/18/22 16:38
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
8.3
2.4
1
03/18/22 05:16
03/18/22 16:38
193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-3 Lab ID: 92593947003 Collected: 03/14/22 15:55 Received: 03/15/22 16:38 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E RVE
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Date: 03/29/2022 06:07 AM
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services
- Charlotte
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 16:38
78-59-1
ND
ug/L
8.3
1.7
1
03/18/22 05:16
03/18/22 16:38
90-12-0
ND
ug/L
8.3
1.6
1
03/18/22 05:16
03/18/22 16:38
91-57-6
ND
ug/L
8.3
1.6
1
03/18/22 05:16
03/18/22 16:38
95-48-7
ND
ug/L
8.3
1.0
1
03/18/22 05:16
03/18/22 16:38
15831-10-4
ND
ug/L
8.3
1.7
1
03/18/22 05:16
03/18/22 16:38
91-20-3
ND
ug/L
16.7
2.5
1
03/18/22 05:16
03/18/22 16:38
88-74-4
ND
ug/L
16.7
3.1
1
03/18/22 05:16
03/18/22 16:38
99-09-2
ND
ug/L
16.7
4.2
1
03/18/22 05:16
03/18/22 16:38
100-01-6
ND
ug/L
8.3
1.6
1
03/18/22 05:16
03/18/22 16:38
98-95-3
ND
ug/L
8.3
1.2
1
03/18/22 05:16
03/18/22 16:38
88-75-5
ND
ug/L
41.7
5.5
1
03/18/22 05:16
03/18/22 16:38
100-02-7
ND
ug/L
8.3
1.6
1
03/18/22 05:16
03/18/22 16:38
62-75-9
ND
ug/L
8.3
1.1
1
03/18/22 05:16
03/18/22 16:38
621-64-7
ND
ug/L
8.3
2.5
1
03/18/22 05:16
03/18/22 16:38
86-30-6
ND
ug/L
8.3
0.96
1
03/18/22 05:16
03/18/22 16:38
108-60-1
ND
ug/L
16.7
3.1
1
03/18/22 05:16
03/18/22 16:38
87-86-5
ND
ug/L
8.3
1.7
1
03/18/22 05:16
03/18/22 16:38
85-01-8
ND
ug/L
8.3
1.1
1
03/18/22 05:16
03/18/22 16:38
108-95-2
ND
ug/L
8.3
1.8
1
03/18/22 05:16
03/18/22 16:38
129-00-0
ND
ug/L
8.3
1.4
1
03/18/22 05:16
03/18/22 16:38
120-82-1
ND
ug/L
8.3
1.2
1
03/18/22 05:16
03/18/22 16:38
95-95-4
ND
ug/L
8.3
1.3
1
03/18/22 05:16
03/18/22 16:38
88-06-2
62
%
10-144
1
03/18/22 05:16
03/18/22 16:38
4165-60-0
60
%
10-130
1
03/18/22 05:16
03/18/22 16:38
321-60-8
81
%
34-163
1
03/18/22 05:16
03/18/22 16:38
1718-51-0
30
%
10-130
1
03/18/22 05:16
03/18/22 16:38
13127-88-3
43
%
10-130
1
03/18/22 05:16
03/18/22 16:38
367-12-4
63
%
10-144
1
03/18/22 05:16
03/18/22 16:38
118-79-6
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
ND
ug/L
25.0
5.1
1
03/18/2217:51
67-64-1
ND
ug/L
1.0
0.34
1
03/18/2217:51
71-43-2
ND
ug/L
1.0
0.29
1
03/18/2217:51
108-86-1
ND
ug/L
1.0
0.47
1
03/18/2217:51
74-97-5
ND
ug/L
1.0
0.31
1
03/18/2217:51
75-27-4
ND
ug/L
1.0
0.34
1
03/18/2217:51
75-25-2
ND
ug/L
2.0
1.7
1
03/18/2217:51
74-83-9
ND
ug/L
5.0
4.0
1
03/18/2217:51
78-93-3
ND
ug/L
1.0
0.33
1
03/18/2217:51
56-23-5
ND
ug/L
1.0
0.28
1
03/18/2217:51
108-90-7
ND
ug/L
1.0
0.65
1
03/18/2217:51
75-00-3
ND
ug/L
1.0
0.43
1
03/18/2217:51
67-66-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
L1
Page 18 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-3 Lab ID: 92593947003 Collected: 03/14/22 15:55 Received: 03/15/22 16:38 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Date: 03/29/2022 06:07 AM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.54
1
03/18/2217:51
74-87-3
ND
ug/L
1.0
0.32
1
03/18/2217:51
95-49-8
ND
ug/L
1.0
0.32
1
03/18/2217:51
106-43-4
ND
ug/L
2.0
0.34
1
03/18/2217:51
96-12-8
ND
ug/L
1.0
0.36
1
03/18/2217:51
124-48-1
ND
ug/L
1.0
0.27
1
03/18/2217:51
106-93-4
ND
ug/L
1.0
0.39
1
03/18/2217:51
74-95-3
ND
ug/L
1.0
0.34
1
03/18/2217:51
95-50-1
ND
ug/L
1.0
0.34
1
03/18/2217:51
541-73-1
ND
ug/L
1.0
0.33
1
03/18/2217:51
106-46-7
ND
ug/L
1.0
0.35
1
03/18/2217:51
75-71-8
ND
ug/L
1.0
0.37
1
03/18/2217:51
75-34-3
ND
ug/L
1.0
0.32
1
03/18/2217:51
107-06-2
ND
ug/L
1.0
0.35
1
03/18/2217:51
75-35-4
ND
ug/L
1.0
0.38
1
03/18/2217:51
156-59-2
ND
ug/L
1.0
0.40
1
03/18/2217:51
156-60-5
ND
ug/L
1.0
0.36
1
03/18/2217:51
78-87-5
ND
ug/L
1.0
0.28
1
03/18/2217:51
142-28-9
ND
ug/L
1.0
0.39
1
03/18/2217:51
594-20-7
ND
ug/L
1.0
0.43
1
03/18/2217:51
563-58-6
ND
ug/L
1.0
0.36
1
03/18/2217:51
10061-01-5
ND
ug/L
1.0
0.36
1
03/18/2217:51
10061-02-6
ND
ug/L
1.0
0.31
1
03/18/2217:51
108-20-3
ND
ug/L
1.0
0.30
1
03/18/2217:51
100-41-4
ND
ug/L
2.0
1.5
1
03/18/2217:51
87-68-3
ND
ug/L
5.0
0.48
1
03/18/2217:51
591-78-6
ND
ug/L
1.0
0.41
1
03/18/2217:51
99-87-6
ND
ug/L
5.0
2.0
1
03/18/2217:51
75-09-2
ND
ug/L
5.0
2.7
1
03/18/2217:51
108-10-1
ND
ug/L
1.0
0.42
1
03/18/2217:51
1634-04-4
ND
ug/L
1.0
0.64
1
03/18/2217:51
91-20-3
ND
ug/L
1.0
0.29
1
03/18/2217:51
100-42-5
ND
ug/L
1.0
0.31
1
03/18/2217:51
630-20-6
ND
ug/L
1.0
0.22
1
03/18/2217:51
79-34-5
ND
ug/L
1.0
0.29
1
03/18/2217:51
127-18-4
ND
ug/L
1.0
0.48
1
03/18/2217:51
108-88-3
ND
ug/L
1.0
0.81
1
03/18/2217:51
87-61-6
ND
ug/L
1.0
0.64
1
03/18/2217:51
120-82-1
ND
ug/L
1.0
0.33
1
03/18/2217:51
71-55-6
ND
ug/L
1.0
0.32
1
03/18/2217:51
79-00-5
ND
ug/L
1.0
0.38
1
03/18/2217:51
79-01-6
ND
ug/L
1.0
0.30
1
03/18/2217:51
75-69-4
ND
ug/L
1.0
0.26
1
03/18/2217:51
96-18-4
ND
ug/L
2.0
1.3
1
03/18/2217:51
108-05-4
ND
ug/L
1.0
0.39
1
03/18/2217:51
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 19 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-3
Lab ID:
92593947003
Collected:
03/14/22 15:55
Received: 03/15/22 16:38 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical
Method: EPA 8260D
Pace Analytical
Services
- Charlotte
Xylene (Total)
ND
ug/L
1.0
0.34
1
03/18/22 17:51
1330-20-7
m&p-Xylene
ND
ug/L
2.0
0.71
1
03/18/22 17:51
179601-23-1
o-Xylene
ND
ug/L
1.0
0.34
1
03/18/22 17:51
95-47-6
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
03/18/22 17:51
460-00-4
1,2-Dichloroethane-d4 (S)
87
%
70-130
1
03/18/22 17:51
17060-07-0
Toluene-d8 (S)
107
%
70-130
1
03/18/22 17:51
2037-26-5
Date: 03/29/2022 06:07 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 20 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-4 Lab ID: 92593947004 Collected: 03/14/22 16:25 Received: 03/15/22 16:38 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Acenaphthene
ND
ug/L
10.0
2.0
1
03/18/22 05:16
03/18/22 17:03
83-32-9
Acenaphthylene
ND
ug/L
10.0
2.0
1
03/18/22 05:16
03/18/22 17:03
208-96-8
Aniline
ND
ug/L
10.0
1.6
1
03/18/22 05:16
03/18/22 17:03
62-53-3
Anthracene
ND
ug/L
10.0
2.3
1
03/18/22 05:16
03/18/22 17:03
120-12-7
Benzo(a)anthracene
ND
ug/L
10.0
2.7
1
03/18/22 05:16
03/18/22 17:03
56-55-3
Benzo(a)pyrene
ND
ug/L
10.0
2.8
1
03/18/22 05:16
03/18/22 17:03
50-32-8
Benzo(b)fluoranthene
ND
ug/L
10.0
2.6
1
03/18/22 05:16
03/18/22 17:03
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
10.0
2.8
1
03/18/22 05:16
03/18/22 17:03
191-24-2
Benzo(k)fluoranthene
ND
ug/L
10.0
2.7
1
03/18/22 05:16
03/18/22 17:03
207-08-9
Benzoic Acid
ND
ug/L
50.0
3.4
1
03/18/22 05:16
03/18/22 17:03
65-85-0
Benzyl alcohol
ND
ug/L
20.0
2.9
1
03/18/22 05:16
03/18/22 17:03
100-51-6
4-Bromophenylphenyl ether
ND
ug/L
10.0
1.8
1
03/18/22 05:16
03/18/22 17:03
101-55-3
Butylbenzylphthalate
ND
ug/L
10.0
3.1
1
03/18/22 05:16
03/18/22 17:03
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
10.0
3.3
1
03/18/22 05:16
03/18/22 17:03
59-50-7
4-Chloroaniline
ND
ug/L
20.0
3.6
1
03/18/22 05:16
03/18/22 17:03
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1.8
1
03/18/22 05:16
03/18/22 17:03
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
10.0
1.9
1
03/18/22 05:16
03/18/22 17:03
111-44-4
2-Chloronaphthalene
ND
ug/L
10.0
1.7
1
03/18/22 05:16
03/18/22 17:03
91-58-7
2-Chlorophenol
ND
ug/L
10.0
1.2
1
03/18/22 05:16
03/18/22 17:03
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
10.0
2.0
1
03/18/22 05:16
03/18/22 17:03
7005-72-3
Chrysene
ND
ug/L
10.0
2.8
1
03/18/22 05:16
03/18/22 17:03
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
10.0
3.0
1
03/18/22 05:16
03/18/22 17:03
53-70-3
Dibenzofuran
ND
ug/L
10.0
2.1
1
03/18/22 05:16
03/18/22 17:03
132-64-9
1,2-Dichlorobenzene
ND
ug/L
10.0
1.8
1
03/18/22 05:16
03/18/22 17:03
95-50-1
1,3-Dichlorobenzene
ND
ug/L
10.0
1.6
1
03/18/22 05:16
03/18/22 17:03
541-73-1
1,4-Dichlorobenzene
ND
ug/L
10.0
1.7
1
03/18/22 05:16
03/18/22 17:03
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
20.0
8.1
1
03/18/22 05:16
03/18/22 17:03
91-94-1
2,4-Dichlorophenol
ND
ug/L
10.0
1.4
1
03/18/22 05:16
03/18/22 17:03
120-83-2
Diethylphthalate
ND
ug/L
10.0
2.0
1
03/18/22 05:16
03/18/22 17:03
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1.7
1
03/18/22 05:16
03/18/22 17:03
105-67-9
Dimethylphthalate
ND
ug/L
10.0
2.1
1
03/18/22 05:16
03/18/22 17:03
131-11-3
Di-n-butylphthalate
ND
ug/L
10.0
2.2
1
03/18/22 05:16
03/18/22 17:03
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
20.0
3.4
1
03/18/22 05:16
03/18/22 17:03
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
26.0
1
03/18/22 05:16
03/18/22 17:03
51-28-5
2,4-Dinitrotoluene
ND
ug/L
10.0
1.6
1
03/18/22 05:16
03/18/22 17:03
121-14-2
2,6-Dinitrotoluene
ND
ug/L
10.0
1.7
1
03/18/22 05:16
03/18/22 17:03
606-20-2
Di-n-octylphthalate
ND
ug/L
10.0
3.9
1
03/18/22 05:16
03/18/22 17:03
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
6.0
3.7
1
03/18/22 05:16
03/18/22 17:03
117-81-7
Fluoranthene
ND
ug/L
10.0
2.2
1
03/18/22 05:16
03/18/22 17:03
206-44-0
Fluorene
ND
ug/L
10.0
2.1
1
03/18/22 05:16
03/18/22 17:03
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
10.0
1.8
1
03/18/22 05:16
03/18/22 17:03
87-68-3
Hexachlorobenzene
ND
ug/L
10.0
2.2
1
03/18/22 05:16
03/18/22 17:03
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1.6
1
03/18/22 05:16
03/18/22 17:03
77-47-4
Hexachloroethane
ND
ug/L
10.0
1.4
1
03/18/22 05:16
03/18/22 17:03
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
10.0
2.9
1
03/18/22 05:16
03/18/22 17:03
193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-4 Lab ID: 92593947004 Collected: 03/14/22 16:25 Received: 03/15/22 16:38 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E RVE
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Date: 03/29/2022 06:07 AM
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services
- Charlotte
ND
ug/L
10.0
1.7
1
03/18/22 05:16
03/18/22 17:03
78-59-1
12.7
ug/L
10.0
2.0
1
03/18/22 05:16
03/18/22 17:03
90-12-0
2.8J
ug/L
10.0
1.9
1
03/18/22 05:16
03/18/22 17:03
91-57-6
ND
ug/L
10.0
1.9
1
03/18/22 05:16
03/18/22 17:03
95-48-7
ND
ug/L
10.0
1.2
1
03/18/22 05:16
03/18/22 17:03
15831-10-4
ND
ug/L
10.0
2.1
1
03/18/22 05:16
03/18/22 17:03
91-20-3
ND
ug/L
20.0
3.0
1
03/18/22 05:16
03/18/22 17:03
88-74-4
ND
ug/L
20.0
3.8
1
03/18/22 05:16
03/18/22 17:03
99-09-2
ND
ug/L
20.0
5.1
1
03/18/22 05:16
03/18/22 17:03
100-01-6
ND
ug/L
10.0
1.9
1
03/18/22 05:16
03/18/22 17:03
98-95-3
ND
ug/L
10.0
1.4
1
03/18/22 05:16
03/18/22 17:03
88-75-5
ND
ug/L
50.0
6.6
1
03/18/22 05:16
03/18/22 17:03
100-02-7
ND
ug/L
10.0
1.9
1
03/18/22 05:16
03/18/22 17:03
62-75-9
ND
ug/L
10.0
1.3
1
03/18/22 05:16
03/18/22 17:03
621-64-7
ND
ug/L
10.0
3.0
1
03/18/22 05:16
03/18/22 17:03
86-30-6
ND
ug/L
10.0
1.2
1
03/18/22 05:16
03/18/22 17:03
108-60-1
ND
ug/L
20.0
3.8
1
03/18/22 05:16
03/18/22 17:03
87-86-5
ND
ug/L
10.0
2.0
1
03/18/22 05:16
03/18/22 17:03
85-01-8
ND
ug/L
10.0
1.4
1
03/18/22 05:16
03/18/22 17:03
108-95-2
ND
ug/L
10.0
2.2
1
03/18/22 05:16
03/18/22 17:03
129-00-0
ND
ug/L
10.0
1.7
1
03/18/22 05:16
03/18/22 17:03
120-82-1
ND
ug/L
10.0
1.4
1
03/18/22 05:16
03/18/22 17:03
95-95-4
ND
ug/L
10.0
1.6
1
03/18/22 05:16
03/18/22 17:03
88-06-2
77
%
10-144
1
03/18/22 05:16
03/18/22 17:03
4165-60-0
73
%
10-130
1
03/18/22 05:16
03/18/22 17:03
321-60-8
96
%
34-163
1
03/18/22 05:16
03/18/22 17:03
1718-51-0
40
%
10-130
1
03/18/22 05:16
03/18/22 17:03
13127-88-3
53
%
10-130
1
03/18/22 05:16
03/18/22 17:03
367-12-4
72
%
10-144
1
03/18/22 05:16
03/18/22 17:03
118-79-6
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
ND
ug/L
25.0
5.1
1
03/18/2218:09
67-64-1
ND
ug/L
1.0
0.34
1
03/18/2218:09
71-43-2
ND
ug/L
1.0
0.29
1
03/18/2218:09
108-86-1
ND
ug/L
1.0
0.47
1
03/18/2218:09
74-97-5
ND
ug/L
1.0
0.31
1
03/18/2218:09
75-27-4
ND
ug/L
1.0
0.34
1
03/18/2218:09
75-25-2
ND
ug/L
2.0
1.7
1
03/18/2218:09
74-83-9
ND
ug/L
5.0
4.0
1
03/18/2218:09
78-93-3
ND
ug/L
1.0
0.33
1
03/18/2218:09
56-23-5
ND
ug/L
1.0
0.28
1
03/18/2218:09
108-90-7
ND
ug/L
1.0
0.65
1
03/18/2218:09
75-00-3
ND
ug/L
1.0
0.43
1
03/18/2218:09
67-66-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
L1
Page 22 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-4 Lab ID: 92593947004 Collected: 03/14/22 16:25 Received: 03/15/22 16:38 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Date: 03/29/2022 06:07 AM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.54
1
03/18/2218:09
74-87-3
ND
ug/L
1.0
0.32
1
03/18/2218:09
95-49-8
ND
ug/L
1.0
0.32
1
03/18/2218:09
106-43-4
ND
ug/L
2.0
0.34
1
03/18/2218:09
96-12-8
ND
ug/L
1.0
0.36
1
03/18/2218:09
124-48-1
ND
ug/L
1.0
0.27
1
03/18/2218:09
106-93-4
ND
ug/L
1.0
0.39
1
03/18/2218:09
74-95-3
ND
ug/L
1.0
0.34
1
03/18/2218:09
95-50-1
ND
ug/L
1.0
0.34
1
03/18/2218:09
541-73-1
ND
ug/L
1.0
0.33
1
03/18/2218:09
106-46-7
ND
ug/L
1.0
0.35
1
03/18/2218:09
75-71-8
ND
ug/L
1.0
0.37
1
03/18/2218:09
75-34-3
ND
ug/L
1.0
0.32
1
03/18/2218:09
107-06-2
ND
ug/L
1.0
0.35
1
03/18/2218:09
75-35-4
ND
ug/L
1.0
0.38
1
03/18/2218:09
156-59-2
ND
ug/L
1.0
0.40
1
03/18/2218:09
156-60-5
ND
ug/L
1.0
0.36
1
03/18/2218:09
78-87-5
ND
ug/L
1.0
0.28
1
03/18/2218:09
142-28-9
ND
ug/L
1.0
0.39
1
03/18/2218:09
594-20-7
ND
ug/L
1.0
0.43
1
03/18/2218:09
563-58-6
ND
ug/L
1.0
0.36
1
03/18/2218:09
10061-01-5
ND
ug/L
1.0
0.36
1
03/18/2218:09
10061-02-6
ND
ug/L
1.0
0.31
1
03/18/2218:09
108-20-3
ND
ug/L
1.0
0.30
1
03/18/2218:09
100-41-4
ND
ug/L
2.0
1.5
1
03/18/2218:09
87-68-3
ND
ug/L
5.0
0.48
1
03/18/2218:09
591-78-6
ND
ug/L
1.0
0.41
1
03/18/2218:09
99-87-6
ND
ug/L
5.0
2.0
1
03/18/2218:09
75-09-2
ND
ug/L
5.0
2.7
1
03/18/2218:09
108-10-1
ND
ug/L
1.0
0.42
1
03/18/2218:09
1634-04-4
ND
ug/L
1.0
0.64
1
03/18/2218:09
91-20-3
ND
ug/L
1.0
0.29
1
03/18/2218:09
100-42-5
ND
ug/L
1.0
0.31
1
03/18/2218:09
630-20-6
ND
ug/L
1.0
0.22
1
03/18/2218:09
79-34-5
ND
ug/L
1.0
0.29
1
03/18/2218:09
127-18-4
ND
ug/L
1.0
0.48
1
03/18/2218:09
108-88-3
ND
ug/L
1.0
0.81
1
03/18/2218:09
87-61-6
ND
ug/L
1.0
0.64
1
03/18/2218:09
120-82-1
ND
ug/L
1.0
0.33
1
03/18/2218:09
71-55-6
ND
ug/L
1.0
0.32
1
03/18/2218:09
79-00-5
ND
ug/L
1.0
0.38
1
03/18/2218:09
79-01-6
ND
ug/L
1.0
0.30
1
03/18/2218:09
75-69-4
ND
ug/L
1.0
0.26
1
03/18/2218:09
96-18-4
ND
ug/L
2.0
1.3
1
03/18/2218:09
108-05-4
ND
ug/L
1.0
0.39
1
03/18/2218:09
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 23 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-4
Lab ID:
92593947004
Collected:
03/14/22 16:25
Received: 03/15/22 16:38 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical
Method: EPA 8260D
Pace Analytical
Services
- Charlotte
Xylene (Total)
ND
ug/L
1.0
0.34
1
03/18/22 18:09
1330-20-7
m&p-Xylene
ND
ug/L
2.0
0.71
1
03/18/22 18:09
179601-23-1
o-Xylene
ND
ug/L
1.0
0.34
1
03/18/22 18:09
95-47-6
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
03/18/22 18:09
460-00-4
1,2-Dichloroethane-d4 (S)
89
%
70-130
1
03/18/22 18:09
17060-07-0
Toluene-d8 (S)
106
%
70-130
1
03/18/22 18:09
2037-26-5
Date: 03/29/2022 06:07 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 24 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-5 Lab ID: 92593947005 Collected: 03/14/22 16:50 Received: 03/15/22 16:38 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Acenaphthene
ND
ug/L
9.1
1.8
1
03/18/22 05:16
03/18/22 17:28
83-32-9
Acenaphthylene
ND
ug/L
9.1
1.8
1
03/18/22 05:16
03/18/22 17:28
208-96-8
Aniline
ND
ug/L
9.1
1.5
1
03/18/22 05:16
03/18/22 17:28
62-53-3
Anthracene
ND
ug/L
9.1
2.1
1
03/18/22 05:16
03/18/22 17:28
120-12-7
Benzo(a)anthracene
ND
ug/L
9.1
2.4
1
03/18/22 05:16
03/18/22 17:28
56-55-3
Benzo(a)pyrene
ND
ug/L
9.1
2.5
1
03/18/22 05:16
03/18/22 17:28
50-32-8
Benzo(b)fluoranthene
ND
ug/L
9.1
2.4
1
03/18/22 05:16
03/18/22 17:28
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
9.1
2.6
1
03/18/22 05:16
03/18/22 17:28
191-24-2
Benzo(k)fluoranthene
ND
ug/L
9.1
2.5
1
03/18/22 05:16
03/18/22 17:28
207-08-9
Benzoic Acid
ND
ug/L
45.5
3.1
1
03/18/22 05:16
03/18/22 17:28
65-85-0
Benzyl alcohol
ND
ug/L
18.2
2.6
1
03/18/22 05:16
03/18/22 17:28
100-51-6
4-Bromophenylphenyl ether
ND
ug/L
9.1
1.6
1
03/18/22 05:16
03/18/22 17:28
101-55-3
Butylbenzylphthalate
ND
ug/L
9.1
2.9
1
03/18/22 05:16
03/18/22 17:28
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
9.1
3.0
1
03/18/22 05:16
03/18/22 17:28
59-50-7
4-Chloroaniline
ND
ug/L
18.2
3.3
1
03/18/22 05:16
03/18/22 17:28
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
9.1
1.7
1
03/18/22 05:16
03/18/22 17:28
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
9.1
1.7
1
03/18/22 05:16
03/18/22 17:28
111-44-4
2-Chloronaphthalene
ND
ug/L
9.1
1.6
1
03/18/22 05:16
03/18/22 17:28
91-58-7
2-Chlorophenol
ND
ug/L
9.1
1.1
1
03/18/22 05:16
03/18/22 17:28
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
9.1
1.8
1
03/18/22 05:16
03/18/22 17:28
7005-72-3
Chrysene
ND
ug/L
9.1
2.5
1
03/18/22 05:16
03/18/22 17:28
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
9.1
2.7
1
03/18/22 05:16
03/18/22 17:28
53-70-3
Dibenzofuran
ND
ug/L
9.1
1.9
1
03/18/22 05:16
03/18/22 17:28
132-64-9
1,2-Dichlorobenzene
ND
ug/L
9.1
1.6
1
03/18/22 05:16
03/18/22 17:28
95-50-1
1,3-Dichlorobenzene
ND
ug/L
9.1
1.5
1
03/18/22 05:16
03/18/22 17:28
541-73-1
1,4-Dichlorobenzene
ND
ug/L
9.1
1.5
1
03/18/22 05:16
03/18/22 17:28
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
18.2
7.4
1
03/18/22 05:16
03/18/22 17:28
91-94-1
2,4-Dichlorophenol
ND
ug/L
9.1
1.3
1
03/18/22 05:16
03/18/22 17:28
120-83-2
Diethylphthalate
ND
ug/L
9.1
1.9
1
03/18/22 05:16
03/18/22 17:28
84-66-2
2,4-Dimethylphenol
ND
ug/L
9.1
1.5
1
03/18/22 05:16
03/18/22 17:28
105-67-9
Dimethylphthalate
ND
ug/L
9.1
1.9
1
03/18/22 05:16
03/18/22 17:28
131-11-3
Di-n-butylphthalate
ND
ug/L
9.1
2.0
1
03/18/22 05:16
03/18/22 17:28
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
18.2
3.1
1
03/18/22 05:16
03/18/22 17:28
534-52-1
2,4-Dinitrophenol
ND
ug/L
45.5
23.6
1
03/18/22 05:16
03/18/22 17:28
51-28-5
2,4-Dinitrotoluene
ND
ug/L
9.1
1.5
1
03/18/22 05:16
03/18/22 17:28
121-14-2
2,6-Dinitrotoluene
ND
ug/L
9.1
1.6
1
03/18/22 05:16
03/18/22 17:28
606-20-2
Di-n-octylphthalate
ND
ug/L
9.1
3.6
1
03/18/22 05:16
03/18/22 17:28
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.5
3.4
1
03/18/22 05:16
03/18/22 17:28
117-81-7
Fluoranthene
ND
ug/L
9.1
2.0
1
03/18/22 05:16
03/18/22 17:28
206-44-0
Fluorene
ND
ug/L
9.1
1.9
1
03/18/22 05:16
03/18/22 17:28
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
9.1
1.6
1
03/18/22 05:16
03/18/22 17:28
87-68-3
Hexachlorobenzene
ND
ug/L
9.1
2.0
1
03/18/22 05:16
03/18/22 17:28
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
9.1
1.4
1
03/18/22 05:16
03/18/22 17:28
77-47-4
Hexachloroethane
ND
ug/L
9.1
1.3
1
03/18/22 05:16
03/18/22 17:28
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
9.1
2.6
1
03/18/22 05:16
03/18/22 17:28
193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 25 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-5 Lab ID: 92593947005 Collected: 03/14/22 16:50 Received: 03/15/22 16:38 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E RVE
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Date: 03/29/2022 06:07 AM
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services
- Charlotte
ND
ug/L
9.1
1.5
1
03/18/22 05:16
03/18/22 17:28
78-59-1
55.7
ug/L
9.1
1.8
1
03/18/22 05:16
03/18/22 17:28
90-12-0
102
ug/L
9.1
1.7
1
03/18/22 05:16
03/18/22 17:28
91-57-6
ND
ug/L
9.1
1.7
1
03/18/22 05:16
03/18/22 17:28
95-48-7
ND
ug/L
9.1
1.1
1
03/18/22 05:16
03/18/22 17:28
15831-10-4
59.1
ug/L
9.1
1.9
1
03/18/22 05:16
03/18/22 17:28
91-20-3
ND
ug/L
18.2
2.7
1
03/18/22 05:16
03/18/22 17:28
88-74-4
ND
ug/L
18.2
3.4
1
03/18/22 05:16
03/18/22 17:28
99-09-2
ND
ug/L
18.2
4.6
1
03/18/22 05:16
03/18/22 17:28
100-01-6
ND
ug/L
9.1
1.7
1
03/18/22 05:16
03/18/22 17:28
98-95-3
ND
ug/L
9.1
1.3
1
03/18/22 05:16
03/18/22 17:28
88-75-5
ND
ug/L
45.5
6.0
1
03/18/22 05:16
03/18/22 17:28
100-02-7
ND
ug/L
9.1
1.7
1
03/18/22 05:16
03/18/22 17:28
62-75-9
ND
ug/L
9.1
1.2
1
03/18/22 05:16
03/18/22 17:28
621-64-7
ND
ug/L
9.1
2.7
1
03/18/22 05:16
03/18/22 17:28
86-30-6
ND
ug/L
9.1
1.0
1
03/18/22 05:16
03/18/22 17:28
108-60-1
ND
ug/L
18.2
3.4
1
03/18/22 05:16
03/18/22 17:28
87-86-5
ND
ug/L
9.1
1.8
1
03/18/22 05:16
03/18/22 17:28
85-01-8
ND
ug/L
9.1
1.2
1
03/18/22 05:16
03/18/22 17:28
108-95-2
ND
ug/L
9.1
2.0
1
03/18/22 05:16
03/18/22 17:28
129-00-0
ND
ug/L
9.1
1.6
1
03/18/22 05:16
03/18/22 17:28
120-82-1
ND
ug/L
9.1
1.3
1
03/18/22 05:16
03/18/22 17:28
95-95-4
ND
ug/L
9.1
1.4
1
03/18/22 05:16
03/18/22 17:28
88-06-2
73
%
10-144
1
03/18/22 05:16
03/18/22 17:28
4165-60-0
69
%
10-130
1
03/18/22 05:16
03/18/22 17:28
321-60-8
81
%
34-163
1
03/18/22 05:16
03/18/22 17:28
1718-51-0
40
%
10-130
1
03/18/22 05:16
03/18/22 17:28
13127-88-3
50
%
10-130
1
03/18/22 05:16
03/18/22 17:28
367-12-4
69
%
10-144
1
03/18/22 05:16
03/18/22 17:28
118-79-6
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
ND
ug/L
100
20.4
4
03/21/22 20:46
67-64-1
ND
ug/L
4.0
1.4
4
03/21/22 20:46
71-43-2
ND
ug/L
4.0
1.2
4
03/21/22 20:46
108-86-1
ND
ug/L
4.0
1.9
4
03/21/22 20:46
74-97-5
ND
ug/L
4.0
1.2
4
03/21/22 20:46
75-27-4
ND
ug/L
4.0
1.4
4
03/21/22 20:46
75-25-2
ND
ug/L
8.0
6.6
4
03/21/22 20:46
74-83-9
ND
ug/L
20.0
15.8
4
03/21/22 20:46
78-93-3
ND
ug/L
4.0
1.3
4
03/21/22 20:46
56-23-5
ND
ug/L
4.0
1.1
4
03/21/22 20:46
108-90-7
ND
ug/L
4.0
2.6
4
03/21/22 20:46
75-00-3
ND
ug/L
4.0
1.7
4
03/21/22 20:46
67-66-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 26 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-5 Lab ID: 92593947005 Collected: 03/14/22 16:50 Received: 03/15/22 16:38 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Date: 03/29/2022 06:07 AM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
4.0
2.2
4
03/21/22 20:46
74-87-3
ND
ug/L
4.0
1.3
4
03/21/22 20:46
95-49-8
ND
ug/L
4.0
1.3
4
03/21/22 20:46
106-43-4
ND
ug/L
8.0
1.4
4
03/21/22 20:46
96-12-8
ND
ug/L
4.0
1.4
4
03/21/22 20:46
124-48-1
ND
ug/L
4.0
1.1
4
03/21/22 20:46
106-93-4
ND
ug/L
4.0
1.6
4
03/21/22 20:46
74-95-3
ND
ug/L
4.0
1.4
4
03/21/22 20:46
95-50-1
ND
ug/L
4.0
1.4
4
03/21/22 20:46
541-73-1
ND
ug/L
4.0
1.3
4
03/21/22 20:46
106-46-7
ND
ug/L
4.0
1.4
4
03/21/22 20:46
75-71-8
ND
ug/L
4.0
1.5
4
03/21/22 20:46
75-34-3
ND
ug/L
4.0
1.3
4
03/21/22 20:46
107-06-2
ND
ug/L
4.0
1.4
4
03/21/22 20:46
75-35-4
ND
ug/L
4.0
1.5
4
03/21/22 20:46
156-59-2
ND
ug/L
4.0
1.6
4
03/21/22 20:46
156-60-5
ND
ug/L
4.0
1.4
4
03/21/22 20:46
78-87-5
ND
ug/L
4.0
1.1
4
03/21/22 20:46
142-28-9
ND
ug/L
4.0
1.6
4
03/21/22 20:46
594-20-7
ND
ug/L
4.0
1.7
4
03/21/22 20:46
563-58-6
ND
ug/L
4.0
1.5
4
03/21/22 20:46
10061-01-5
ND
ug/L
4.0
1.5
4
03/21/22 20:46
10061-02-6
ND
ug/L
4.0
1.2
4
03/21/22 20:46
108-20-3
128
ug/L
4.0
1.2
4
03/21/22 20:46
100-41-4
ND
ug/L
8.0
6.1
4
03/21/22 20:46
87-68-3
ND
ug/L
20.0
1.9
4
03/21/22 20:46
591-78-6
ND
ug/L
4.0
1.7
4
03/21/22 20:46
99-87-6
ND
ug/L
20.0
7.8
4
03/21/22 20:46
75-09-2
ND
ug/L
20.0
10.8
4
03/21/22 20:46
108-10-1
ND
ug/L
4.0
1.7
4
03/21/22 20:46
1634-04-4
116
ug/L
4.0
2.6
4
03/21/22 20:46
91-20-3
ND
ug/L
4.0
1.2
4
03/21/22 20:46
100-42-5
ND
ug/L
4.0
1.2
4
03/21/22 20:46
630-20-6
ND
ug/L
4.0
0.90
4
03/21/22 20:46
79-34-5
ND
ug/L
4.0
1.2
4
03/21/22 20:46
127-18-4
2.OJ
ug/L
4.0
1.9
4
03/21/22 20:46
108-88-3
ND
ug/L
4.0
3.2
4
03/21/22 20:46
87-61-6
ND
ug/L
4.0
2.6
4
03/21/22 20:46
120-82-1
ND
ug/L
4.0
1.3
4
03/21/22 20:46
71-55-6
ND
ug/L
4.0
1.3
4
03/21/22 20:46
79-00-5
ND
ug/L
4.0
1.5
4
03/21/22 20:46
79-01-6
ND
ug/L
4.0
1.2
4
03/21/22 20:46
75-69-4
ND
ug/L
4.0
1.0
4
03/21/22 20:46
96-18-4
ND
ug/L
8.0
5.2
4
03/21/22 20:46
108-05-4
ND
ug/L
4.0
1.5
4
03/21/22 20:46
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v2
v1
Page 27 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-5
Lab ID:
92593947005
Collected:
03/14/22 16:50
Received: 03/15/22 16:38 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical
Method: EPA 8260D
Pace Analytical
Services
- Charlotte
Xylene (Total)
301
ug/L
4.0
1.4 4
03/21/22 20:46
1330-20-7
m&p-Xylene
240
ug/L
8.0
2.8 4
03/21/22 20:46
179601-23-1
o-Xylene
60.9
ug/L
4.0
1.4 4
03/21/22 20:46
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
4
03/21/22 20:46
460-00-4 D3
1,2-Dichloroethane-d4 (S)
82
%
70-130
4
03/21/22 20:46
17060-07-0
Toluene-d8 (S)
107
%
70-130
4
03/21/22 20:46
2037-26-5
Date: 03/29/2022 06:07 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 28 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-6 Lab ID: 92593947006 Collected: 03/14/22 17:20 Received: 03/15/22 16:38 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Acenaphthene
ND
ug/L
9.1
1.8
1
03/21/22 12:52
03/21/22 16:46
83-32-9
Acenaphthylene
ND
ug/L
9.1
1.8
1
03/21/22 12:52
03/21/22 16:46
208-96-8
Aniline
ND
ug/L
9.1
1.5
1
03/21/22 12:52
03/21/22 16:46
62-53-3
Anthracene
ND
ug/L
9.1
2.1
1
03/21/22 12:52
03/21/22 16:46
120-12-7
Benzo(a)anthracene
ND
ug/L
9.1
2.4
1
03/21/22 12:52
03/21/22 16:46
56-55-3
Benzo(a)pyrene
ND
ug/L
9.1
2.5
1
03/21/22 12:52
03/21/22 16:46
50-32-8
Benzo(b)fluoranthene
ND
ug/L
9.1
2.4
1
03/21/22 12:52
03/21/22 16:46
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
9.1
2.6
1
03/21/22 12:52
03/21/22 16:46
191-24-2
Benzo(k)fluoranthene
ND
ug/L
9.1
2.5
1
03/21/22 12:52
03/21/22 16:46
207-08-9
Benzoic Acid
ND
ug/L
45.5
3.1
1
03/21/22 12:52
03/21/22 16:46
65-85-0
Benzyl alcohol
ND
ug/L
18.2
2.6
1
03/21/22 12:52
03/21/22 16:46
100-51-6
4-Bromophenylphenyl ether
ND
ug/L
9.1
1.6
1
03/21/22 12:52
03/21/22 16:46
101-55-3
Butylbenzylphthalate
ND
ug/L
9.1
2.9
1
03/21/22 12:52
03/21/22 16:46
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
9.1
3.0
1
03/21/22 12:52
03/21/22 16:46
59-50-7
4-Chloroaniline
ND
ug/L
18.2
3.3
1
03/21/22 12:52
03/21/22 16:46
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
9.1
1.7
1
03/21/22 12:52
03/21/22 16:46
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
9.1
1.7
1
03/21/22 12:52
03/21/22 16:46
111-44-4
2-Chloronaphthalene
ND
ug/L
9.1
1.6
1
03/21/22 12:52
03/21/22 16:46
91-58-7
2-Chlorophenol
ND
ug/L
9.1
1.1
1
03/21/22 12:52
03/21/22 16:46
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
9.1
1.8
1
03/21/22 12:52
03/21/22 16:46
7005-72-3
Chrysene
ND
ug/L
9.1
2.5
1
03/21/22 12:52
03/21/22 16:46
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
9.1
2.7
1
03/21/22 12:52
03/21/22 16:46
53-70-3
Dibenzofuran
ND
ug/L
9.1
1.9
1
03/21/22 12:52
03/21/22 16:46
132-64-9
1,2-Dichlorobenzene
ND
ug/L
9.1
1.6
1
03/21/22 12:52
03/21/22 16:46
95-50-1
1,3-Dichlorobenzene
ND
ug/L
9.1
1.5
1
03/21/22 12:52
03/21/22 16:46
541-73-1
1,4-Dichlorobenzene
ND
ug/L
9.1
1.5
1
03/21/22 12:52
03/21/22 16:46
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
18.2
7.4
1
03/21/22 12:52
03/21/22 16:46
91-94-1
2,4-Dichlorophenol
ND
ug/L
9.1
1.3
1
03/21/22 12:52
03/21/22 16:46
120-83-2
Diethylphthalate
ND
ug/L
9.1
1.9
1
03/21/22 12:52
03/21/22 16:46
84-66-2
2,4-Dimethylphenol
ND
ug/L
9.1
1.5
1
03/21/22 12:52
03/21/22 16:46
105-67-9
Dimethylphthalate
ND
ug/L
9.1
1.9
1
03/21/22 12:52
03/21/22 16:46
131-11-3
Di-n-butylphthalate
ND
ug/L
9.1
2.0
1
03/21/22 12:52
03/21/22 16:46
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
18.2
3.1
1
03/21/22 12:52
03/21/22 16:46
534-52-1
2,4-Dinitrophenol
ND
ug/L
45.5
23.6
1
03/21/22 12:52
03/21/22 16:46
51-28-5
2,4-Dinitrotoluene
ND
ug/L
9.1
1.5
1
03/21/22 12:52
03/21/22 16:46
121-14-2
2,6-Dinitrotoluene
ND
ug/L
9.1
1.6
1
03/21/22 12:52
03/21/22 16:46
606-20-2
Di-n-octylphthalate
ND
ug/L
9.1
3.6
1
03/21/22 12:52
03/21/22 16:46
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.5
3.4
1
03/21/22 12:52
03/21/22 16:46
117-81-7
Fluoranthene
ND
ug/L
9.1
2.0
1
03/21/22 12:52
03/21/22 16:46
206-44-0
Fluorene
ND
ug/L
9.1
1.9
1
03/21/22 12:52
03/21/22 16:46
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
9.1
1.6
1
03/21/22 12:52
03/21/22 16:46
87-68-3
Hexachlorobenzene
ND
ug/L
9.1
2.0
1
03/21/22 12:52
03/21/22 16:46
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
9.1
1.4
1
03/21/22 12:52
03/21/22 16:46
77-47-4
Hexachloroethane
ND
ug/L
9.1
1.3
1
03/21/22 12:52
03/21/22 16:46
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
9.1
2.6
1
03/21/22 12:52
03/21/22 16:46
193-39-5
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 29 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-6 Lab ID: 92593947006 Collected: 03/14/22 17:20 Received: 03/15/22 16:38 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E RVE
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Date: 03/29/2022 06:07 AM
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services
- Charlotte
N D
ug/L
9.1
1.5
1
03/21/22 12:52
03/21/22 16:46
78-59-1
70.3
ug/L
9.1
1.8
1
03/21/22 12:52
03/21/22 16:46
90-12-0
126
ug/L
9.1
1.7
1
03/21/22 12:52
03/21/22 16:46
91-57-6
N D
ug/L
9.1
1.7
1
03/21/22 12:52
03/21/22 16:46
95-48-7
N D
ug/L
9.1
1.1
1
03/21/22 12:52
03/21/22 16:46
15831-10-4
186
ug/L
18.2
3.8
2
03/21/22 12:52
03/22/22 00:46
91-20-3
N D
ug/L
18.2
2.7
1
03/21/22 12:52
03/21/22 16:46
88-74-4
N D
ug/L
18.2
3.4
1
03/21/22 12:52
03/21/22 16:46
99-09-2
ND
ug/L
18.2
4.6
1
03/21/22 12:52
03/21/22 16:46
100-01-6
ND
ug/L
9.1
1.7
1
03/21/22 12:52
03/21/22 16:46
98-95-3
ND
ug/L
9.1
1.3
1
03/21/22 12:52
03/21/22 16:46
88-75-5
ND
ug/L
45.5
6.0
1
03/21/22 12:52
03/21/22 16:46
100-02-7
ND
ug/L
9.1
1.7
1
03/21/22 12:52
03/21/22 16:46
62-75-9
ND
ug/L
9.1
1.2
1
03/21/22 12:52
03/21/22 16:46
621-64-7
ND
ug/L
9.1
2.7
1
03/21/22 12:52
03/21/22 16:46
86-30-6
ND
ug/L
9.1
1.0
1
03/21/22 12:52
03/21/22 16:46
108-60-1
ND
ug/L
18.2
3.4
1
03/21/22 12:52
03/21/22 16:46
87-86-5
ND
ug/L
9.1
1.8
1
03/21/22 12:52
03/21/22 16:46
85-01-8
ND
ug/L
9.1
1.2
1
03/21/22 12:52
03/21/22 16:46
108-95-2
ND
ug/L
9.1
2.0
1
03/21/22 12:52
03/21/22 16:46
129-00-0
ND
ug/L
9.1
1.6
1
03/21/22 12:52
03/21/22 16:46
120-82-1
ND
ug/L
9.1
1.3
1
03/21/22 12:52
03/21/22 16:46
95-95-4
ND
ug/L
9.1
1.4
1
03/21/22 12:52
03/21/22 16:46
88-06-2
77
%
10-144
1
03/21/22 12:52
03/21/22 16:46
4165-60-0
71
%
10-130
1
03/21/22 12:52
03/21/22 16:46
321-60-8
85
%
34-163
1
03/21/22 12:52
03/21/22 16:46
1718-51-0
41
%
10-130
1
03/21/22 12:52
03/21/22 16:46
13127-88-3
52
%
10-130
1
03/21/22 12:52
03/21/22 16:46
367-12-4
89
%
10-144
1
03/21/22 12:52
03/21/22 16:46
118-79-6
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
ND
ug/L
125
25.6
5
03/21/22 21:04
67-64-1
5.1
ug/L
5.0
1.7
5
03/21/22 21:04
71-43-2
ND
ug/L
5.0
1.4
5
03/21/22 21:04
108-86-1
ND
ug/L
5.0
2.3
5
03/21/22 21:04
74-97-5
ND
ug/L
5.0
1.5
5
03/21/22 21:04
75-27-4
ND
ug/L
5.0
1.7
5
03/21/22 21:04
75-25-2
ND
ug/L
10.0
8.3
5
03/21/22 21:04
74-83-9
ND
ug/L
25.0
19.8
5
03/21/22 21:04
78-93-3
ND
ug/L
5.0
1.7
5
03/21/22 21:04
56-23-5
ND
ug/L
5.0
1.4
5
03/21/22 21:04
108-90-7
ND
ug/L
5.0
3.2
5
03/21/22 21:04
75-00-3
ND
ug/L
5.0
2.2
5
03/21/22 21:04
67-66-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 30 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-6 Lab ID: 92593947006 Collected: 03/14/22 17:20 Received: 03/15/22 16:38 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Date: 03/29/2022 06:07 AM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
5.0
2.7
5
03/21/22 21:04
74-87-3
ND
ug/L
5.0
1.6
5
03/21/22 21:04
95-49-8
ND
ug/L
5.0
1.6
5
03/21/22 21:04
106-43-4
ND
ug/L
10.0
1.7
5
03/21/22 21:04
96-12-8
ND
ug/L
5.0
1.8
5
03/21/22 21:04
124-48-1
ND
ug/L
5.0
1.4
5
03/21/22 21:04
106-93-4
ND
ug/L
5.0
2.0
5
03/21/22 21:04
74-95-3
ND
ug/L
5.0
1.7
5
03/21/22 21:04
95-50-1
ND
ug/L
5.0
1.7
5
03/21/22 21:04
541-73-1
ND
ug/L
5.0
1.7
5
03/21/22 21:04
106-46-7
ND
ug/L
5.0
1.7
5
03/21/22 21:04
75-71-8
ND
ug/L
5.0
1.8
5
03/21/22 21:04
75-34-3
ND
ug/L
5.0
1.6
5
03/21/22 21:04
107-06-2
ND
ug/L
5.0
1.7
5
03/21/22 21:04
75-35-4
ND
ug/L
5.0
1.9
5
03/21/22 21:04
156-59-2
ND
ug/L
5.0
2.0
5
03/21/22 21:04
156-60-5
ND
ug/L
5.0
1.8
5
03/21/22 21:04
78-87-5
ND
ug/L
5.0
1.4
5
03/21/22 21:04
142-28-9
ND
ug/L
5.0
1.9
5
03/21/22 21:04
594-20-7
ND
ug/L
5.0
2.1
5
03/21/22 21:04
563-58-6
ND
ug/L
5.0
1.8
5
03/21/22 21:04
10061-01-5
ND
ug/L
5.0
1.8
5
03/21/22 21:04
10061-02-6
ND
ug/L
5.0
1.5
5
03/21/22 21:04
108-20-3
193
ug/L
5.0
1.5
5
03/21/22 21:04
100-41-4
ND
ug/L
10.0
7.6
5
03/21/22 21:04
87-68-3
ND
ug/L
25.0
2.4
5
03/21/22 21:04
591-78-6
ND
ug/L
5.0
2.1
5
03/21/22 21:04
99-87-6
ND
ug/L
25.0
9.8
5
03/21/22 21:04
75-09-2
ND
ug/L
25.0
13.6
5
03/21/22 21:04
108-10-1
ND
ug/L
5.0
2.1
5
03/21/22 21:04
1634-04-4
307
ug/L
5.0
3.2
5
03/21/22 21:04
91-20-3
ND
ug/L
5.0
1.5
5
03/21/22 21:04
100-42-5
ND
ug/L
5.0
1.6
5
03/21/22 21:04
630-20-6
ND
ug/L
5.0
1.1
5
03/21/22 21:04
79-34-5
ND
ug/L
5.0
1.5
5
03/21/22 21:04
127-18-4
ND
ug/L
5.0
2.4
5
03/21/22 21:04
108-88-3
ND
ug/L
5.0
4.0
5
03/21/22 21:04
87-61-6
ND
ug/L
5.0
3.2
5
03/21/22 21:04
120-82-1
ND
ug/L
5.0
1.7
5
03/21/22 21:04
71-55-6
ND
ug/L
5.0
1.6
5
03/21/22 21:04
79-00-5
ND
ug/L
5.0
1.9
5
03/21/22 21:04
79-01-6
ND
ug/L
5.0
1.5
5
03/21/22 21:04
75-69-4
ND
ug/L
5.0
1.3
5
03/21/22 21:04
96-18-4
ND
ug/L
10.0
6.6
5
03/21/22 21:04
108-05-4
ND
ug/L
5.0
1.9
5
03/21/22 21:04
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v2
v1
Page 31 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: TW-6
Lab ID:
92593947006
Collected:
03/14/22 17:20
Received: 03/15/22 16:38 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical
Method: EPA 8260D
Pace Analytical
Services
- Charlotte
Xylene (Total)
865
ug/L
5.0
1.7 5
03/21/22 21:04
1330-20-7
m&p-Xylene
804
ug/L
10.0
3.5 5
03/21/22 21:04
179601-23-1
o-Xylene
60.8
ug/L
5.0
1.7 5
03/21/22 21:04
95-47-6
Surrogates
4-Bromofluorobenzene (S)
101
%
70-130
5
03/21/22 21:04
460-00-4 D3
1,2-Dichloroethane-d4 (S)
88
%
70-130
5
03/21/22 21:04
17060-07-0
Toluene-d8 (S)
115
%
70-130
5
03/21/22 21:04
2037-26-5
Date: 03/29/2022 06:07 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 32 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-1 Lab ID: 92593947007 Collected: 03/14/22 13:48 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
mg/kg
4.2
1.5
10
03/18/22 16:02
03/21/22 13:44
83-32-9
Acenaphthylene
ND
mg/kg
4.2
1.5
10
03/18/22 16:02
03/21/22 13:44
208-96-8
Aniline
ND
mg/kg
4.2
1.6
10
03/18/22 16:02
03/21/22 13:44
62-53-3
Anthracene
ND
mg/kg
4.2
1.4
10
03/18/22 16:02
03/21/22 13:44
120-12-7
Benzo(a)anthracene
ND
mg/kg
4.2
1.4
10
03/18/22 16:02
03/21/22 13:44
56-55-3
Benzo(a)pyrene
ND
mg/kg
4.2
1.4
10
03/18/22 16:02
03/21/22 13:44
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
4.2
1.4
10
03/18/22 16:02
03/21/22 13:44
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
4.2
1.6
10
03/18/22 16:02
03/21/22 13:44
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
4.2
1.5
10
03/18/22 16:02
03/21/22 13:44
207-08-9
Benzoic Acid
ND
mg/kg
20.8
8.9
10
03/18/22 16:02
03/21/22 13:44
65-85-0
Benzyl alcohol
ND
mg/kg
8.3
3.2
10
03/18/22 16:02
03/21/22 13:44
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
4.2
1.6
10
03/18/22 16:02
03/21/22 13:44
101-55-3
Butylbenzylphthalate
ND
mg/kg
4.2
1.8
10
03/18/22 16:02
03/21/22 13:44
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
8.3
2.9
10
03/18/22 16:02
03/21/22 13:44
59-50-7
4-Chloroaniline
ND
mg/kg
8.3
3.3
10
03/18/22 16:02
03/21/22 13:44
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
4.2
1.7
10
03/18/22 16:02
03/21/22 13:44
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
4.2
1.6
10
03/18/22 16:02
03/21/22 13:44
111-44-4
2-Chloronaphthalene
ND
mg/kg
4.2
1.7
10
03/18/22 16:02
03/21/22 13:44
91-58-7
2-Chlorophenol
ND
mg/kg
4.2
1.6
10
03/18/22 16:02
03/21/22 13:44
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
4.2
1.5
10
03/18/22 16:02
03/21/22 13:44
7005-72-3
Chrysene
ND
mg/kg
4.2
1.5
10
03/18/22 16:02
03/21/22 13:44
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
4.2
1.6
10
03/18/22 16:02
03/21/22 13:44
53-70-3
Dibenzofuran
ND
mg/kg
4.2
1.5
10
03/18/22 16:02
03/21/22 13:44
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
4.2
1.5
10
03/18/22 16:02
03/21/22 13:44
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
4.2
1.5
10
03/18/22 16:02
03/21/22 13:44
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
4.2
1.6
10
03/18/22 16:02
03/21/22 13:44
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
8.3
2.8
10
03/18/22 16:02
03/21/22 13:44
91-94-1
2,4-Dichlorophenol
ND
mg/kg
4.2
1.6
10
03/18/22 16:02
03/21/22 13:44
120-83-2
Diethylphthalate
ND
mg/kg
4.2
1.5
10
03/18/22 16:02
03/21/22 13:44
84-66-2
2,4-Dimethylphenol
ND
mg/kg
4.2
1.7
10
03/18/22 16:02
03/21/22 13:44
105-67-9
Dimethylphthalate
ND
mg/kg
4.2
1.5
10
03/18/22 16:02
03/21/22 13:44
131-11-3
Di-n-butylphthalate
ND
mg/kg
4.2
1.4
10
03/18/22 16:02
03/21/22 13:44
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
8.3
3.9
10
03/18/22 16:02
03/21/22 13:44
534-52-1
2,4-Dinitrophenol
ND
mg/kg
20.8
12.9
10
03/18/22 16:02
03/21/22 13:44
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
4.2
1.6
10
03/18/22 16:02
03/21/22 13:44
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
4.2
1.5
10
03/18/22 16:02
03/21/22 13:44
606-20-2
Di-n-octylphthalate
ND
mg/kg
4.2
1.6
10
03/18/22 16:02
03/21/22 13:44
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
4.2
1.6
10
03/18/22 16:02
03/21/22 13:44
117-81-7
Fluoranthene
ND
mg/kg
4.2
1.4
10
03/18/22 16:02
03/21/22 13:44
206-44-0
Fluorene
ND
mg/kg
4.2
1.5
10
03/18/22 16:02
03/21/22 13:44
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
4.2
1.8
10
03/18/22 16:02
03/21/22 13:44
87-68-3
Hexachlorobenzene
ND
mg/kg
4.2
1.6
10
03/18/22 16:02
03/21/22 13:44
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
4.2
2.4
10
03/18/22 16:02
03/21/22 13:44
77-47-4
Hexachloroethane
ND
mg/kg
4.2
1.6
10
03/18/22 16:02
03/21/22 13:44
67-72-1
REPORT OF LABORATORY ANALYSIS
IL
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 33 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: SB-1
Lab ID:
92593947007
Collected:
03/14/22
13:48
Received: 03/15/22
16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services
- Charlotte
Indeno(1,2,3-cd)pyrene
ND
mg/kg
4.2
1.6
10
03/18/22 16:02
03/21/22 13:44
193-39-5
Isophorone
ND
mg/kg
4.2
1.9
10
03/18/22 16:02
03/21/22 13:44
78-59-1
1-Methylnaphthalene
7.1
mg/kg
4.2
1.5
10
03/18/22 16:02
03/21/22 13:44
90-12-0
2-Methylnaphthalene
13.8
mg/kg
4.2
1.7
10
03/18/22 16:02
03/21/22 13:44
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
4.2
1.7
10
03/18/22 16:02
03/21/22 13:44
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
4.2
1.7
10
03/18/22 16:02
03/21/22 13:44
15831-10-4
Naphthalene
8.5
mg/kg
4.2
1.4
10
03/18/22 16:02
03/21/22 13:44
91-20-3
2-Nitroaniline
ND
mg/kg
20.8
3.4
10
03/18/22 16:02
03/21/22 13:44
88-74-4
3-Nitroaniline
ND
mg/kg
20.8
3.3
10
03/18/22 16:02
03/21/22 13:44
99-09-2
IL
4-Nitroaniline
ND
mg/kg
8.3
3.2
10
03/18/22 16:02
03/21/22 13:44
100-01-6
IL
Nitrobenzene
ND
mg/kg
4.2
1.9
10
03/18/22 16:02
03/21/22 13:44
98-95-3
2-Nitrophenol
ND
mg/kg
4.2
1.8
10
03/18/22 16:02
03/21/22 13:44
88-75-5
4-Nitrophenol
ND
mg/kg
20.8
8.0
10
03/18/22 16:02
03/21/22 13:44
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
4.2
1.4
10
03/18/22 16:02
03/21/22 13:44
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
4.2
1.6
10
03/18/22 16:02
03/21/22 13:44
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
4.2
1.5
10
03/18/22 16:02
03/21/22 13:44
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
4.2
2.0
10
03/18/22 16:02
03/21/22 13:44
108-60-1
Pentachlorophenol
ND
mg/kg
8.3
4.1
10
03/18/22 16:02
03/21/22 13:44
87-86-5
Phenanthrene
ND
mg/kg
4.2
1.4
10
03/18/22 16:02
03/21/22 13:44
85-01-8
Phenol
ND
mg/kg
4.2
1.9
10
03/18/22 16:02
03/21/22 13:44
108-95-2
Pyrene
ND
mg/kg
4.2
1.7
10
03/18/22 16:02
03/21/22 13:44
129-00-0
Pyridine
ND
mg/kg
4.2
1.3
10
03/18/22 16:02
03/21/22 13:44
110-86-1
1,2,4-Trichlorobenzene
ND
mg/kg
4.2
1.6
10
03/18/22 16:02
03/21/22 13:44
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
4.2
1.9
10
03/18/22 16:02
03/21/22 13:44
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
4.2
1.7
10
03/18/22 16:02
03/21/22 13:44
88-06-2
Surrogates
Nitrobenzene-d5 (S)
0
%
21-130
10
03/18/22 16:02
03/21/22 13:44
4165-60-0
D3,S4
2-Fluorobiphenyl (S)
0
%
19-130
10
03/18/22 16:02
03/21/22 13:44
321-60-8
S4
Terphenyl-d14 (S)
0
%
15-130
10
03/18/22 16:02
03/21/22 13:44
1718-51-0
S4
Phenol-d6 (S)
0
%
18-130
10
03/18/22 16:02
03/21/22 13:44
13127-88-3
S4
2-Fluorophenol (S)
0
%
18-130
10
03/18/22 16:02
03/21/22 13:44
367-12-4
S4
2,4,6-Tribromophenol (S)
0
%
18-130
10
03/18/22 16:02
03/21/22 13:44
118-79-6
S4
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D
Preparation Method: EPA 5035A/5030B
Pace Analytical
Services
- Charlotte
Acetone
ND
mg/kg
0.78
0.25
5
03/21/22 14:59
03/22/22 01:02
67-64-1
v2
Benzene
0.17
mg/kg
0.039
0.016
5
03/21/22 14:59
03/22/22 01:02
71-43-2
Bromobenzene
ND
mg/kg
0.039
0.013
5
03/21/22 14:59
03/22/22 01:02
108-86-1
Bromochloromethane
ND
mg/kg
0.039
0.012
5
03/21/22 14:59
03/22/22 01:02
74-97-5
Bromodichloromethane
ND
mg/kg
0.039
0.015
5
03/21/22 14:59
03/22/22 01:02
75-27-4
Bromoform
ND
mg/kg
0.039
0.014
5
03/21/22 14:59
03/22/22 01:02
75-25-2
Bromomethane
ND
mg/kg
0.078
0.062
5
03/21/22 14:59
03/22/22 01:02
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.78
0.19
5
03/21/22 14:59
03/22/22 01:02
78-93-3
n-Butylbenzene
3.2
mg/kg
0.039
0.018
5
03/21/22 14:59
03/22/22 01:02
104-51-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 34 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-1 Lab ID: 92593947007 Collected: 03/14/22 13:48 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
sec-Butylbenzene
1.9
mg/kg
0.039
0.017
5
03/21/22 14:59
03/22/22 01:02
135-98-8
tert-Butyl benzene
ND
mg/kg
0.039
0.014
5
03/21/22 14:59
03/22/22 01:02
98-06-6
Carbon tetrachloride
ND
mg/kg
0.039
0.015
5
03/21/22 14:59
03/22/22 01:02
56-23-5
Chlorobenzene
ND
mg/kg
0.039
0.0075
5
03/21/22 14:59
03/22/22 01:02
108-90-7
Chloroethane
ND
mg/kg
0.078
0.030
5
03/21/22 14:59
03/22/22 01:02
75-00-3
Chloroform
ND
mg/kg
0.039
0.024
5
03/21/22 14:59
03/22/22 01:02
67-66-3
Chloromethane
ND
mg/kg
0.078
0.033
5
03/21/22 14:59
03/22/22 01:02
74-87-3
2-Chlorotoluene
ND
mg/kg
0.039
0.014
5
03/21/22 14:59
03/22/22 01:02
95-49-8
4-Chlorotoluene
ND
mg/kg
0.039
0.0069
5
03/21/22 14:59
03/22/22 01:02
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.039
0.015
5
03/21/22 14:59
03/22/22 01:02
96-12-8
Dibromochloromethane
ND
mg/kg
0.039
0.022
5
03/21/22 14:59
03/22/22 01:02
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.039
0.017
5
03/21/22 14:59
03/22/22 01:02
106-93-4
Dibromomethane
ND
mg/kg
0.039
0.0084
5
03/21/22 14:59
03/22/22 01:02
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.039
0.014
5
03/21/22 14:59
03/22/22 01:02
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.039
0.012
5
03/21/22 14:59
03/22/22 01:02
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.039
0.010
5
03/21/22 14:59
03/22/22 01:02
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.078
0.017
5
03/21/22 14:59
03/22/22 01:02
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.039
0.016
5
03/21/22 14:59
03/22/22 01:02
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.039
0.026
5
03/21/22 14:59
03/22/22 01:02
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.039
0.016
5
03/21/22 14:59
03/22/22 01:02
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.039
0.013
5
03/21/22 14:59
03/22/22 01:02
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.039
0.014
5
03/21/22 14:59
03/22/22 01:02
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.039
0.012
5
03/21/22 14:59
03/22/22 01:02
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.039
0.012
5
03/21/22 14:59
03/22/22 01:02
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.039
0.013
5
03/21/22 14:59
03/22/22 01:02
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.039
0.019
5
03/21/22 14:59
03/22/22 01:02
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.039
0.011
5
03/21/22 14:59
03/22/22 01:02
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.039
0.013
5
03/21/22 14:59
03/22/22 01:02
10061-02-6
Diisopropyl ether
ND
mg/kg
0.039
0.011
5
03/21/22 14:59
03/22/22 01:02
108-20-3
Ethylbenzene
11.1
mg/kg
0.039
0.018
5
03/21/22 14:59
03/22/22 01:02
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.078
0.064
5
03/21/22 14:59
03/22/22 01:02
87-68-3
2-Hexanone
ND
mg/kg
0.39
0.038
5
03/21/22 14:59
03/22/22 01:02
591-78-6
Isopropylbenzene (Cumene)
1.4
mg/kg
0.039
0.013
5
03/21/22 14:59
03/22/22 01:02
98-82-8
p-Isopropyltoluene
2.7
mg/kg
0.039
0.019
5
03/21/22 14:59
03/22/22 01:02
99-87-6
Methylene Chloride
0.42
mg/kg
0.16
0.11
5
03/21/22 14:59
03/22/22 01:02
75-09-2
4-Methyl-2-pentanone (MIBK)
1.1
mg/kg
0.39
0.038
5
03/21/22 14:59
03/22/22 01:02
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.039
0.015
5
03/21/22 14:59
03/22/22 01:02
1634-04-4
Naphthalene
11.3
mg/kg
0.039
0.021
5
03/21/22 14:59
03/22/22 01:02
91-20-3
n-Propylbenzene
4.0
mg/kg
0.039
0.014
5
03/21/22 14:59
03/22/22 01:02
103-65-1
Styrene
ND
mg/kg
0.039
0.010
5
03/21/22 14:59
03/22/22 01:02
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.039
0.015
5
03/21/22 14:59
03/22/22 01:02
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.039
0.010
5
03/21/22 14:59
03/22/22 01:02
79-34-5
Tetrachloroethene
ND
mg/kg
0.039
0.012
5
03/21/22 14:59
03/22/22 01:02
127-18-4
Toluene
0.17
mg/kg
0.039
0.011
5
03/21/22 14:59
03/22/22 01:02
108-88-3
REPORT OF LABORATORY ANALYSIS
v2
v2
C7,v2
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 35 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-1
Lab ID:
92593947007
Collected:
03/14/22
13:48
Received: 03/15/22
16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services
- Charlotte
1,2,3-Trichlorobenzene
ND
mg/kg
0.039
0.032
5
03/21/22 14:59
03/22/22 01:02
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.039
0.033
5
03/21/22 14:59
03/22/22 01:02
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.039
0.020
5
03/21/22 14:59
03/22/22 01:02
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.039
0.013
5
03/21/22 14:59
03/22/22 01:02
79-00-5
Trichloroethene
0.056
mg/kg
0.039
0.010
5
03/21/22 14:59
03/22/22 01:02
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.039
0.022
5
03/21/22 14:59
03/22/22 01:02
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.039
0.020
5
03/21/22 14:59
03/22/22 01:02
96-18-4
1,2,4-Trimethylbenzene
17.8
mg/kg
0.039
0.011
5
03/21/22 14:59
03/22/22 01:02
95-63-6
1,3,5-Trimethylbenzene
4.7
mg/kg
0.039
0.013
5
03/21/22 14:59
03/22/22 01:02
108-67-8
Vinyl acetate
ND
mg/kg
0.39
0.028
5
03/21/22 14:59
03/22/22 01:02
108-05-4
Vinyl chloride
ND
mg/kg
0.078
0.020
5
03/21/22 14:59
03/22/22 01:02
75-01-4
Xylene (Total)
6.1
mg/kg
0.078
0.022
5
03/21/22 14:59
03/22/22 01:02
1330-20-7
m&p-Xylene
5.5
mg/kg
0.078
0.027
5
03/21/22 14:59
03/22/22 01:02
179601-23-1
o-Xylene
0.54
mg/kg
0.039
0.017
5
03/21/22 14:59
03/22/22 01:02
95-47-6
Surrogates
Toluene-d8 (S)
100
%
70-130
5
03/21/22 14:59
03/22/22 01:02
2037-26-5
4-Bromofluorobenzene (S)
117
%
69-134
5
03/21/22 14:59
03/22/22 01:02
460-00-4
1,2-Dichloroethane-d4 (S)
87
%
70-130
5
03/21/22 14:59
03/22/22 01:02
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services
- Charlotte
Percent Moisture
21.7
%
0.10
0.10
1
03/17/22 14:46
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 36 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-2 Lab ID: 92593947008 Collected: 03/15/22 08:17 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 12:01
83-32-9
Acenaphthylene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 12:01
208-96-8
Aniline
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 12:01
62-53-3
Anthracene
ND
mg/kg
0.40
0.13
1
03/18/22 16:02
03/21/22 12:01
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.40
0.13
1
03/18/22 16:02
03/21/22 12:01
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 12:01
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.40
0.13
1
03/18/22 16:02
03/21/22 12:01
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 12:01
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 12:01
207-08-9
Benzoic Acid
ND
mg/kg
2.0
0.86
1
03/18/22 16:02
03/21/22 12:01
65-85-0
Benzyl alcohol
ND
mg/kg
0.80
0.30
1
03/18/22 16:02
03/21/22 12:01
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 12:01
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.40
0.17
1
03/18/22 16:02
03/21/22 12:01
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
0.80
0.28
1
03/18/22 16:02
03/21/22 12:01
59-50-7
4-Chloroaniline
ND
mg/kg
0.80
0.31
1
03/18/22 16:02
03/21/22 12:01
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.40
0.17
1
03/18/22 16:02
03/21/22 12:01
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 12:01
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 12:01
91-58-7
2-Chlorophenol
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 12:01
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 12:01
7005-72-3
Chrysene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 12:01
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 12:01
53-70-3
Dibenzofuran
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 12:01
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 12:01
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 12:01
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 12:01
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
0.80
0.27
1
03/18/22 16:02
03/21/22 12:01
91-94-1
2,4-Dichlorophenol
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 12:01
120-83-2
Diethylphthalate
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 12:01
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.40
0.17
1
03/18/22 16:02
03/21/22 12:01
105-67-9
Dimethylphthalate
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 12:01
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.40
0.13
1
03/18/22 16:02
03/21/22 12:01
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.80
0.37
1
03/18/22 16:02
03/21/22 12:01
534-52-1
2,4-Dinitrophenol
ND
mg/kg
2.0
1.2
1
03/18/22 16:02
03/21/22 12:01
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 12:01
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 12:01
606-20-2
Di-n-octylphthalate
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 12:01
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 12:01
117-81-7
Fluoranthene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 12:01
206-44-0
Fluorene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 12:01
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.40
0.17
1
03/18/22 16:02
03/21/22 12:01
87-68-3
Hexachlorobenzene
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 12:01
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.40
0.23
1
03/18/22 16:02
03/21/22 12:01
77-47-4
Hexachloroethane
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 12:01
67-72-1
REPORT OF LABORATORY ANALYSIS
IL
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 37 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: SB-2
Lab ID:
92593947008
Collected:
03/15/22
08:17
Received: 03/15/22
16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services
- Charlotte
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 12:01
193-39-5
Isophorone
ND
mg/kg
0.40
0.18
1
03/18/22 16:02
03/21/22 12:01
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 12:01
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 12:01
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 12:01
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 12:01
15831-10-4
Naphthalene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 12:01
91-20-3
2-Nitroaniline
ND
mg/kg
2.0
0.33
1
03/18/22 16:02
03/21/22 12:01
88-74-4
3-Nitroaniline
ND
mg/kg
2.0
0.31
1
03/18/22 16:02
03/21/22 12:01
99-09-2
IL
4-Nitroaniline
ND
mg/kg
0.80
0.30
1
03/18/22 16:02
03/21/22 12:01
100-01-6
IL
Nitrobenzene
ND
mg/kg
0.40
0.18
1
03/18/22 16:02
03/21/22 12:01
98-95-3
2-Nitrophenol
ND
mg/kg
0.40
0.17
1
03/18/22 16:02
03/21/22 12:01
88-75-5
4-Nitrophenol
ND
mg/kg
2.0
0.77
1
03/18/22 16:02
03/21/22 12:01
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.40
0.13
1
03/18/22 16:02
03/21/22 12:01
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 12:01
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 12:01
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.40
0.19
1
03/18/22 16:02
03/21/22 12:01
108-60-1
Pentachlorophenol
ND
mg/kg
0.80
0.39
1
03/18/22 16:02
03/21/22 12:01
87-86-5
Phenanthrene
ND
mg/kg
0.40
0.13
1
03/18/22 16:02
03/21/22 12:01
85-01-8
Phenol
ND
mg/kg
0.40
0.18
1
03/18/22 16:02
03/21/22 12:01
108-95-2
Pyrene
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 12:01
129-00-0
Pyridine
ND
mg/kg
0.40
0.13
1
03/18/22 16:02
03/21/22 12:01
110-86-1
1,2,4-Trichlorobenzene
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 12:01
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.40
0.18
1
03/18/22 16:02
03/21/22 12:01
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 12:01
88-06-2
Surrogates
Nitrobenzene-d5 (S)
70
%
21-130
1
03/18/22 16:02
03/21/22 12:01
4165-60-0
2-Fluorobiphenyl (S)
56
%
19-130
1
03/18/22 16:02
03/21/22 12:01
321-60-8
Terphenyl-d14 (S)
63
%
15-130
1
03/18/22 16:02
03/21/22 12:01
1718-51-0
Phenol-d6 (S)
49
%
18-130
1
03/18/22 16:02
03/21/22 12:01
13127-88-3
2-Fluorophenol (S)
41
%
18-130
1
03/18/22 16:02
03/21/22 12:01
367-12-4
2,4,6-Tribromophenol (S)
42
%
18-130
1
03/18/22 16:02
03/21/22 12:01
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D
Preparation Method: EPA 5035A/5030B
Pace Analytical
Services
- Charlotte
Acetone
0.051J
mg/kg
0.14
0.046
1
03/18/2214:41
03/18/2215:45
67-64-1
C7,v2
Benzene
ND
mg/kg
0.0072
0.0029
1
03/18/2214:41
03/18/2215:45
71-43-2
M1
Bromobenzene
ND
mg/kg
0.0072
0.0023
1
03/18/2214:41
03/18/2215:45
108-86-1
M1
Bromochloromethane
ND
mg/kg
0.0072
0.0021
1
03/18/2214:41
03/18/2215:45
74-97-5
M1
Bromodichloromethane
ND
mg/kg
0.0072
0.0028
1
03/18/2214:41
03/18/2215:45
75-27-4
M1
Bromoform
ND
mg/kg
0.0072
0.0025
1
03/18/2214:41
03/18/2215:45
75-25-2
M1
Bromomethane
ND
mg/kg
0.014
0.011
1
03/18/2214:41
03/18/2215:45
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.14
0.035
1
03/18/22 14:41
03/18/22 15:45
78-93-3
n-Butylbenzene
ND
mg/kg
0.0072
0.0034
1
03/18/2214:41
03/18/2215:45
104-51-8
M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 38 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-2
Lab ID:
92593947008
Collected:
03/15/22
08:17
Received: 03/15/22
16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services
- Charlotte
sec-Butylbenzene
ND
mg/kg
0.0072
0.0032
1
03/18/22 14:41
03/18/22 15:45
135-98-8
M1
tert-Butyl benzene
ND
mg/kg
0.0072
0.0026
1
03/18/22 14:41
03/18/22 15:45
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0072
0.0027
1
03/18/22 14:41
03/18/22 15:45
56-23-5
M1
Chlorobenzene
ND
mg/kg
0.0072
0.0014
1
03/18/22 14:41
03/18/22 15:45
108-90-7
M1
Chloroethane
ND
mg/kg
0.014
0.0056
1
03/18/22 14:41
03/18/22 15:45
75-00-3
Chloroform
ND
mg/kg
0.0072
0.0044
1
03/18/22 14:41
03/18/22 15:45
67-66-3
M1
Chloromethane
ND
mg/kg
0.014
0.0060
1
03/18/22 14:41
03/18/22 15:45
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0072
0.0025
1
03/18/22 14:41
03/18/22 15:45
95-49-8
M1
4-Chlorotoluene
ND
mg/kg
0.0072
0.0013
1
03/18/22 14:41
03/18/22 15:45
106-43-4
M1
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0072
0.0028
1
03/18/22 14:41
03/18/22 15:45
96-12-8
Dibromochloromethane
ND
mg/kg
0.0072
0.0040
1
03/18/22 14:41
03/18/22 15:45
124-48-1
M1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0072
0.0032
1
03/18/22 14:41
03/18/22 15:45
106-93-4
M1
Dibromomethane
ND
mg/kg
0.0072
0.0015
1
03/18/22 14:41
03/18/22 15:45
74-95-3
M1
1,2-Dichlorobenzene
ND
mg/kg
0.0072
0.0026
1
03/18/22 14:41
03/18/22 15:45
95-50-1
M1
1,3-Dichlorobenzene
ND
mg/kg
0.0072
0.0022
1
03/18/22 14:41
03/18/22 15:45
541-73-1
M1
1,4-Dichlorobenzene
ND
mg/kg
0.0072
0.0019
1
03/18/22 14:41
03/18/22 15:45
106-46-7
M1
Dichlorodifluoromethane
ND
mg/kg
0.014
0.0031
1
03/18/22 14:41
03/18/22 15:45
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0072
0.0030
1
03/18/22 14:41
03/18/22 15:45
75-34-3
M1
1,2-Dichloroethane
ND
mg/kg
0.0072
0.0048
1
03/18/22 14:41
03/18/22 15:45
107-06-2
M1
1,1-Dichloroethene
ND
mg/kg
0.0072
0.0030
1
03/18/22 14:41
03/18/22 15:45
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0072
0.0025
1
03/18/22 14:41
03/18/22 15:45
156-59-2
M1
trans-1,2-Dichloroethene
ND
mg/kg
0.0072
0.0025
1
03/18/22 14:41
03/18/22 15:45
156-60-5
M1
1,2-Dichloropropane
ND
mg/kg
0.0072
0.0022
1
03/18/22 14:41
03/18/22 15:45
78-87-5
M1
1,3-Dichloropropane
ND
mg/kg
0.0072
0.0022
1
03/18/22 14:41
03/18/22 15:45
142-28-9
M1
2,2-Dichloropropane
ND
mg/kg
0.0072
0.0023
1
03/18/22 14:41
03/18/22 15:45
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0072
0.0035
1
03/18/22 14:41
03/18/22 15:45
563-58-6
M1
cis-1,3-Dichloropropene
ND
mg/kg
0.0072
0.0020
1
03/18/22 14:41
03/18/22 15:45
10061-01-5
M1
trans- 1,3-Dichloropropene
ND
mg/kg
0.0072
0.0025
1
03/18/22 14:41
03/18/22 15:45
10061-02-6
M1
Diisopropyl ether
ND
mg/kg
0.0072
0.0019
1
03/18/22 14:41
03/18/22 15:45
108-20-3
M1
Ethylbenzene
0.0049J
mg/kg
0.0072
0.0034
1
03/18/22 14:41
03/18/22 15:45
100-41-4
M1
Hexachloro-1,3-butadiene
ND
mg/kg
0.014
0.012
1
03/18/22 14:41
03/18/22 15:45
87-68-3
2-Hexanone
ND
mg/kg
0.072
0.0069
1
03/18/22 14:41
03/18/22 15:45
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0072
0.0024
1
03/18/22 14:41
03/18/22 15:45
98-82-8
M1
p-Isopropyltoluene
ND
mg/kg
0.0072
0.0035
1
03/18/22 14:41
03/18/22 15:45
99-87-6
Methylene Chloride
ND
mg/kg
0.029
0.020
1
03/18/22 14:41
03/18/22 15:45
75-09-2
M1
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.072
0.0069
1
03/18/22 14:41
03/18/22 15:45
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0072
0.0027
1
03/18/22 14:41
03/18/22 15:45
1634-04-4
M1
Naphthalene
0.016
mg/kg
0.0072
0.0038
1
03/18/22 14:41
03/18/22 15:45
91-20-3
n-Propylbenzene
ND
mg/kg
0.0072
0.0026
1
03/18/22 14:41
03/18/22 15:45
103-65-1
M1
Styrene
ND
mg/kg
0.0072
0.0019
1
03/18/22 14:41
03/18/22 15:45
100-42-5
M1
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0072
0.0028
1
03/18/22 14:41
03/18/22 15:45
630-20-6
M1
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0072
0.0019
1
03/18/22 14:41
03/18/22 15:45
79-34-5
M1
Tetrachloroethene
ND
mg/kg
0.0072
0.0023
1
03/18/22 14:41
03/18/22 15:45
127-18-4
M1
Toluene
0.015
mg/kg
0.0072
0.0020
1
03/18/22 14:41
03/18/22 15:45
108-88-3
M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 39 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-2
Lab ID:
92593947008
Collected:
03/15/22
08:17
Received: 03/15/22
16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services
- Charlotte
1,2,3-Trichlorobenzene
ND
mg/kg
0.0072
0.0058
1
03/18/22 14:41
03/18/22 15:45
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0072
0.0060
1
03/18/22 14:41
03/18/22 15:45
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0072
0.0037
1
03/18/22 14:41
03/18/22 15:45
71-55-6
M1
1,1,2-Trichloroethane
ND
mg/kg
0.0072
0.0024
1
03/18/22 14:41
03/18/22 15:45
79-00-5
M1
Trichloroethene
ND
mg/kg
0.0072
0.0019
1
03/18/22 14:41
03/18/22 15:45
79-01-6
M1
Trichlorofluoromethane
ND
mg/kg
0.0072
0.0040
1
03/18/22 14:41
03/18/22 15:45
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.0072
0.0036
1
03/18/22 14:41
03/18/22 15:45
96-18-4
M1
1,2,4-Trimethylbenzene
0.0083
mg/kg
0.0072
0.0020
1
03/18/22 14:41
03/18/22 15:45
95-63-6
M1
1,3,5-Trimethylbenzene
0.0044J
mg/kg
0.0072
0.0024
1
03/18/22 14:41
03/18/22 15:45
108-67-8
M1
Vinyl acetate
ND
mg/kg
0.072
0.0052
1
03/18/22 14:41
03/18/22 15:45
108-05-4
M1
Vinyl chloride
ND
mg/kg
0.014
0.0037
1
03/18/22 14:41
03/18/22 15:45
75-01-4
Xylene (Total)
0.032
mg/kg
0.014
0.0041
1
03/18/22 14:41
03/18/22 15:45
1330-20-7
MS
m&p-Xylene
0.021
mg/kg
0.014
0.0049
1
03/18/22 14:41
03/18/22 15:45
179601-23-1
M1
o-Xylene
0.012
mg/kg
0.0072
0.0032
1
03/18/22 14:41
03/18/22 15:45
95-47-6
M1
Surrogates
Toluene-d8 (S)
98
%
70-130
1
03/18/22 14:41
03/18/22 15:45
2037-26-5
4-Bromofluorobenzene (S)
98
%
69-134
1
03/18/22 14:41
03/18/22 15:45
460-00-4
1,2-Dichloroethane-d4 (S)
97
%
70-130
1
03/18/22 14:41
03/18/22 15:45
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services
- Charlotte
Percent Moisture
17.2
%
0.10
0.10
1
03/17/22 14:46
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 40 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-3 Lab ID: 92593947009 Collected: 03/15/22 08:37 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 14:10
83-32-9
Acenaphthylene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 14:10
208-96-8
Aniline
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 14:10
62-53-3
Anthracene
ND
mg/kg
0.40
0.13
1
03/18/22 16:02
03/21/22 14:10
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.40
0.13
1
03/18/22 16:02
03/21/22 14:10
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 14:10
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.40
0.13
1
03/18/22 16:02
03/21/22 14:10
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 14:10
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 14:10
207-08-9
Benzoic Acid
ND
mg/kg
2.0
0.87
1
03/18/22 16:02
03/21/22 14:10
65-85-0
Benzyl alcohol
ND
mg/kg
0.81
0.31
1
03/18/22 16:02
03/21/22 14:10
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 14:10
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.40
0.17
1
03/18/22 16:02
03/21/22 14:10
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
0.81
0.28
1
03/18/22 16:02
03/21/22 14:10
59-50-7
4-Chloroaniline
ND
mg/kg
0.81
0.32
1
03/18/22 16:02
03/21/22 14:10
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.40
0.17
1
03/18/22 16:02
03/21/22 14:10
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 14:10
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 14:10
91-58-7
2-Chlorophenol
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 14:10
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 14:10
7005-72-3
Chrysene
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 14:10
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 14:10
53-70-3
Dibenzofuran
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 14:10
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 14:10
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 14:10
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 14:10
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
0.81
0.27
1
03/18/22 16:02
03/21/22 14:10
91-94-1
2,4-Dichlorophenol
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 14:10
120-83-2
Diethylphthalate
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 14:10
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.40
0.17
1
03/18/22 16:02
03/21/22 14:10
105-67-9
Dimethylphthalate
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 14:10
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 14:10
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.81
0.38
1
03/18/22 16:02
03/21/22 14:10
534-52-1
2,4-Dinitrophenol
ND
mg/kg
2.0
1.3
1
03/18/22 16:02
03/21/22 14:10
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 14:10
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 14:10
606-20-2
Di-n-octylphthalate
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 14:10
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 14:10
117-81-7
Fluoranthene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 14:10
206-44-0
Fluorene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 14:10
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.40
0.18
1
03/18/22 16:02
03/21/22 14:10
87-68-3
Hexachlorobenzene
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 14:10
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.40
0.23
1
03/18/22 16:02
03/21/22 14:10
77-47-4
Hexachloroethane
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 14:10
67-72-1
REPORT OF LABORATORY ANALYSIS
IL
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 41 of 122

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: SB-3 Lab ID: 92593947009 Collected: 03/15/22 08:37 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 14:10
193-39-5
Isophorone
ND
mg/kg
0.40
0.18
1
03/18/22 16:02
03/21/22 14:10
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 14:10
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 14:10
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.40
0.17
1
03/18/22 16:02
03/21/22 14:10
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 14:10
15831-10-4
Naphthalene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 14:10
91-20-3
2-Nitroaniline
ND
mg/kg
2.0
0.33
1
03/18/22 16:02
03/21/22 14:10
88-74-4
3-Nitroaniline
ND
mg/kg
2.0
0.32
1
03/18/22 16:02
03/21/22 14:10
99-09-2
4-Nitroaniline
ND
mg/kg
0.81
0.31
1
03/18/22 16:02
03/21/22 14:10
100-01-6
Nitrobenzene
ND
mg/kg
0.40
0.19
1
03/18/22 16:02
03/21/22 14:10
98-95-3
2-Nitrophenol
ND
mg/kg
0.40
0.18
1
03/18/22 16:02
03/21/22 14:10
88-75-5
4-Nitrophenol
ND
mg/kg
2.0
0.78
1
03/18/22 16:02
03/21/22 14:10
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 14:10
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 14:10
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 14:10
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.40
0.19
1
03/18/22 16:02
03/21/22 14:10
108-60-1
Pentachlorophenol
ND
mg/kg
0.81
0.40
1
03/18/22 16:02
03/21/22 14:10
87-86-5
Phenanthrene
ND
mg/kg
0.40
0.13
1
03/18/22 16:02
03/21/22 14:10
85-01-8
Phenol
ND
mg/kg
0.40
0.18
1
03/18/22 16:02
03/21/22 14:10
108-95-2
Pyrene
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 14:10
129-00-0
Pyridine
ND
mg/kg
0.40
0.13
1
03/18/22 16:02
03/21/22 14:10
110-86-1
1,2,4-Trichlorobenzene
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 14:10
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.40
0.19
1
03/18/22 16:02
03/21/22 14:10
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.40
0.17
1
03/18/22 16:02
03/21/22 14:10
88-06-2
Surrogates
Nitrobenzene-d5 (S)
43
%
21-130
1
03/18/22 16:02
03/21/22 14:10
4165-60-0
2-Fluorobiphenyl (S)
43
%
19-130
1
03/18/22 16:02
03/21/22 14:10
321-60-8
Terphenyl-d14 (S)
52
%
15-130
1
03/18/22 16:02
03/21/22 14:10
1718-51-0
Phenol-d6 (S)
35
%
18-130
1
03/18/22 16:02
03/21/22 14:10
13127-88-3
2-Fluorophenol (S)
30
%
18-130
1
03/18/22 16:02
03/21/22 14:10
367-12-4
2,4,6-Tribromophenol (S)
45
%
18-130
1
03/18/22 16:02
03/21/22 14:10
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation
Method: EPA
5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
mg/kg
0.20
0.064
1
03/18/2214:41
03/18/2216:55
67-64-1
Benzene
ND
mg/kg
0.0099
0.0039
1
03/18/2214:41
03/18/2216:55
71-43-2
Bromobenzene
ND
mg/kg
0.0099
0.0032
1
03/18/2214:41
03/18/2216:55
108-86-1
Bromochloromethane
ND
mg/kg
0.0099
0.0029
1
03/18/2214:41
03/18/2216:55
74-97-5
Bromodichloromethane
ND
mg/kg
0.0099
0.0038
1
03/18/2214:41
03/18/2216:55
75-27-4
Bromoform
ND
mg/kg
0.0099
0.0035
1
03/18/2214:41
03/18/2216:55
75-25-2
Bromomethane
ND
mg/kg
0.020
0.016
1
03/18/2214:41
03/18/2216:55
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.20
0.048
1
03/18/22 14:41
03/18/22 16:55
78-93-3
n-Butylbenzene
ND
mg/kg
0.0099
0.0047
1
03/18/2214:41
03/18/2216:55
104-51-8
REPORT OF LABORATORY ANALYSIS
IL
IL
v2
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 42 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-3 Lab ID: 92593947009 Collected: 03/15/22 08:37 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
sec-Butylbenzene
ND
mg/kg
0.0099
0.0044
1
03/18/22 14:41
03/18/22 16:55
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0099
0.0035
1
03/18/22 14:41
03/18/22 16:55
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0099
0.0037
1
03/18/22 14:41
03/18/22 16:55
56-23-5
Chlorobenzene
ND
mg/kg
0.0099
0.0019
1
03/18/22 14:41
03/18/22 16:55
108-90-7
Chloroethane
ND
mg/kg
0.020
0.0077
1
03/18/22 14:41
03/18/22 16:55
75-00-3
Chloroform
ND
mg/kg
0.0099
0.0060
1
03/18/22 14:41
03/18/22 16:55
67-66-3
Chloromethane
ND
mg/kg
0.020
0.0083
1
03/18/22 14:41
03/18/22 16:55
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0099
0.0035
1
03/18/22 14:41
03/18/22 16:55
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0099
0.0018
1
03/18/22 14:41
03/18/22 16:55
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0099
0.0038
1
03/18/22 14:41
03/18/22 16:55
96-12-8
Dibromochloromethane
ND
mg/kg
0.0099
0.0056
1
03/18/22 14:41
03/18/22 16:55
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0099
0.0044
1
03/18/22 14:41
03/18/22 16:55
106-93-4
Dibromomethane
ND
mg/kg
0.0099
0.0021
1
03/18/22 14:41
03/18/22 16:55
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0099
0.0036
1
03/18/22 14:41
03/18/22 16:55
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0099
0.0031
1
03/18/22 14:41
03/18/22 16:55
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0099
0.0026
1
03/18/22 14:41
03/18/22 16:55
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.020
0.0043
1
03/18/22 14:41
03/18/22 16:55
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0099
0.0041
1
03/18/22 14:41
03/18/22 16:55
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0099
0.0066
1
03/18/22 14:41
03/18/22 16:55
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0099
0.0041
1
03/18/22 14:41
03/18/22 16:55
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0099
0.0034
1
03/18/22 14:41
03/18/22 16:55
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0099
0.0035
1
03/18/22 14:41
03/18/22 16:55
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0099
0.0030
1
03/18/22 14:41
03/18/22 16:55
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0099
0.0031
1
03/18/22 14:41
03/18/22 16:55
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0099
0.0032
1
03/18/22 14:41
03/18/22 16:55
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0099
0.0048
1
03/18/22 14:41
03/18/22 16:55
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0099
0.0027
1
03/18/22 14:41
03/18/22 16:55
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0099
0.0034
1
03/18/22 14:41
03/18/22 16:55
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0099
0.0027
1
03/18/22 14:41
03/18/22 16:55
108-20-3
Ethylbenzene
ND
mg/kg
0.0099
0.0046
1
03/18/22 14:41
03/18/22 16:55
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.020
0.016
1
03/18/22 14:41
03/18/22 16:55
87-68-3
2-Hexanone
ND
mg/kg
0.099
0.0096
1
03/18/22 14:41
03/18/22 16:55
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0099
0.0034
1
03/18/22 14:41
03/18/22 16:55
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0099
0.0049
1
03/18/22 14:41
03/18/22 16:55
99-87-6
Methylene Chloride
ND
mg/kg
0.040
0.027
1
03/18/22 14:41
03/18/22 16:55
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.099
0.0096
1
03/18/22 14:41
03/18/22 16:55
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0099
0.0037
1
03/18/22 14:41
03/18/22 16:55
1634-04-4
Naphthalene
ND
mg/kg
0.0099
0.0052
1
03/18/22 14:41
03/18/22 16:55
91-20-3
n-Propylbenzene
ND
mg/kg
0.0099
0.0035
1
03/18/22 14:41
03/18/22 16:55
103-65-1
Styrene
ND
mg/kg
0.0099
0.0026
1
03/18/22 14:41
03/18/22 16:55
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0099
0.0038
1
03/18/22 14:41
03/18/22 16:55
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0099
0.0026
1
03/18/22 14:41
03/18/22 16:55
79-34-5
Tetrachloroethene
ND
mg/kg
0.0099
0.0031
1
03/18/22 14:41
03/18/22 16:55
127-18-4
Toluene
ND
mg/kg
0.0099
0.0028
1
03/18/22 14:41
03/18/22 16:55
108-88-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 43 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-3
Lab ID:
92593947009
Collected:
03/15/22
08:37
Received: 03/15/22
16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services
- Charlotte
1,2,3-Trichlorobenzene
ND
mg/kg
0.0099
0.0080
1
03/18/22 14:41
03/18/22 16:55
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0099
0.0083
1
03/18/22 14:41
03/18/22 16:55
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0099
0.0052
1
03/18/22 14:41
03/18/22 16:55
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0099
0.0033
1
03/18/22 14:41
03/18/22 16:55
79-00-5
Trichloroethene
ND
mg/kg
0.0099
0.0026
1
03/18/22 14:41
03/18/22 16:55
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0099
0.0055
1
03/18/22 14:41
03/18/22 16:55
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.0099
0.0050
1
03/18/22 14:41
03/18/22 16:55
96-18-4
1,2,4-Trimethylbenzene
ND
mg/kg
0.0099
0.0027
1
03/18/22 14:41
03/18/22 16:55
95-63-6
1,3,5-Trimethylbenzene
ND
mg/kg
0.0099
0.0033
1
03/18/22 14:41
03/18/22 16:55
108-67-8
Vinyl acetate
ND
mg/kg
0.099
0.0072
1
03/18/22 14:41
03/18/22 16:55
108-05-4
Vinyl chloride
ND
mg/kg
0.020
0.0050
1
03/18/22 14:41
03/18/22 16:55
75-01-4
Xylene (Total)
ND
mg/kg
0.020
0.0056
1
03/18/22 14:41
03/18/22 16:55
1330-20-7
m&p-Xylene
ND
mg/kg
0.020
0.0068
1
03/18/22 14:41
03/18/22 16:55
179601-23-1
o-Xylene
ND
mg/kg
0.0099
0.0044
1
03/18/22 14:41
03/18/22 16:55
95-47-6
Surrogates
Toluene-d8 (S)
99
%
70-130
1
03/18/22 14:41
03/18/22 16:55
2037-26-5
4-Bromofluorobenzene (S)
96
%
69-134
1
03/18/22 14:41
03/18/22 16:55
460-00-4
1,2-Dichloroethane-d4 (S)
92
%
70-130
1
03/18/22 14:41
03/18/22 16:55
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services
- Charlotte
Percent Moisture
19.5
%
0.10
0.10
1
03/17/22 14:46
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 44 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-4 Lab ID: 92593947010 Collected: 03/15/22 08:51 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
mg/kg
0.39
0.14
1
03/18/22 16:02
03/21/22 14:37
83-32-9
Acenaphthylene
ND
mg/kg
0.39
0.14
1
03/18/22 16:02
03/21/22 14:37
208-96-8
Aniline
ND
mg/kg
0.39
0.15
1
03/18/22 16:02
03/21/22 14:37
62-53-3
Anthracene
ND
mg/kg
0.39
0.13
1
03/18/22 16:02
03/21/22 14:37
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.39
0.13
1
03/18/22 16:02
03/21/22 14:37
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.39
0.13
1
03/18/22 16:02
03/21/22 14:37
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.39
0.13
1
03/18/22 16:02
03/21/22 14:37
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.39
0.15
1
03/18/22 16:02
03/21/22 14:37
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.39
0.14
1
03/18/22 16:02
03/21/22 14:37
207-08-9
Benzoic Acid
ND
mg/kg
1.9
0.84
1
03/18/22 16:02
03/21/22 14:37
65-85-0
Benzyl alcohol
ND
mg/kg
0.78
0.30
1
03/18/22 16:02
03/21/22 14:37
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.39
0.15
1
03/18/22 16:02
03/21/22 14:37
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.39
0.16
1
03/18/22 16:02
03/21/22 14:37
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
0.78
0.27
1
03/18/22 16:02
03/21/22 14:37
59-50-7
4-Chloroaniline
ND
mg/kg
0.78
0.31
1
03/18/22 16:02
03/21/22 14:37
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.39
0.16
1
03/18/22 16:02
03/21/22 14:37
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.39
0.15
1
03/18/22 16:02
03/21/22 14:37
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.39
0.15
1
03/18/22 16:02
03/21/22 14:37
91-58-7
2-Chlorophenol
ND
mg/kg
0.39
0.15
1
03/18/22 16:02
03/21/22 14:37
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.39
0.15
1
03/18/22 16:02
03/21/22 14:37
7005-72-3
Chrysene
ND
mg/kg
0.39
0.14
1
03/18/22 16:02
03/21/22 14:37
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.39
0.15
1
03/18/22 16:02
03/21/22 14:37
53-70-3
Dibenzofuran
ND
mg/kg
0.39
0.14
1
03/18/22 16:02
03/21/22 14:37
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.39
0.14
1
03/18/22 16:02
03/21/22 14:37
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.39
0.14
1
03/18/22 16:02
03/21/22 14:37
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.39
0.15
1
03/18/22 16:02
03/21/22 14:37
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
0.78
0.26
1
03/18/22 16:02
03/21/22 14:37
91-94-1
2,4-Dichlorophenol
ND
mg/kg
0.39
0.15
1
03/18/22 16:02
03/21/22 14:37
120-83-2
Diethylphthalate
ND
mg/kg
0.39
0.14
1
03/18/22 16:02
03/21/22 14:37
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.39
0.16
1
03/18/22 16:02
03/21/22 14:37
105-67-9
Dimethylphthalate
ND
mg/kg
0.39
0.14
1
03/18/22 16:02
03/21/22 14:37
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.39
0.13
1
03/18/22 16:02
03/21/22 14:37
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.78
0.36
1
03/18/22 16:02
03/21/22 14:37
534-52-1
2,4-Dinitrophenol
ND
mg/kg
1.9
1.2
1
03/18/22 16:02
03/21/22 14:37
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.39
0.15
1
03/18/22 16:02
03/21/22 14:37
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.39
0.14
1
03/18/22 16:02
03/21/22 14:37
606-20-2
Di-n-octylphthalate
ND
mg/kg
0.39
0.15
1
03/18/22 16:02
03/21/22 14:37
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.39
0.15
1
03/18/22 16:02
03/21/22 14:37
117-81-7
Fluoranthene
ND
mg/kg
0.39
0.13
1
03/18/22 16:02
03/21/22 14:37
206-44-0
Fluorene
ND
mg/kg
0.39
0.14
1
03/18/22 16:02
03/21/22 14:37
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.39
0.17
1
03/18/22 16:02
03/21/22 14:37
87-68-3
Hexachlorobenzene
ND
mg/kg
0.39
0.15
1
03/18/22 16:02
03/21/22 14:37
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.39
0.22
1
03/18/22 16:02
03/21/22 14:37
77-47-4
Hexachloroethane
ND
mg/kg
0.39
0.15
1
03/18/22 16:02
03/21/22 14:37
67-72-1
REPORT OF LABORATORY ANALYSIS
IL
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 45 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: SB-4 Lab ID: 92593947010 Collected: 03/15/22 08:51 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.39
0.15
1
03/18/22 16:02
03/21/22 14:37
193-39-5
Isophorone
ND
mg/kg
0.39
0.17
1
03/18/22 16:02
03/21/22 14:37
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.39
0.14
1
03/18/22 16:02
03/21/22 14:37
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.39
0.16
1
03/18/22 16:02
03/21/22 14:37
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.39
0.16
1
03/18/22 16:02
03/21/22 14:37
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.39
0.16
1
03/18/22 16:02
03/21/22 14:37
15831-10-4
Naphthalene
ND
mg/kg
0.39
0.13
1
03/18/22 16:02
03/21/22 14:37
91-20-3
2-Nitroaniline
ND
mg/kg
1.9
0.32
1
03/18/22 16:02
03/21/22 14:37
88-74-4
3-Nitroaniline
ND
mg/kg
1.9
0.31
1
03/18/22 16:02
03/21/22 14:37
99-09-2
4-Nitroaniline
ND
mg/kg
0.78
0.30
1
03/18/22 16:02
03/21/22 14:37
100-01-6
Nitrobenzene
ND
mg/kg
0.39
0.18
1
03/18/22 16:02
03/21/22 14:37
98-95-3
2-Nitrophenol
ND
mg/kg
0.39
0.17
1
03/18/22 16:02
03/21/22 14:37
88-75-5
4-Nitrophenol
ND
mg/kg
1.9
0.75
1
03/18/22 16:02
03/21/22 14:37
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.39
0.13
1
03/18/22 16:02
03/21/22 14:37
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.39
0.15
1
03/18/22 16:02
03/21/22 14:37
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.39
0.14
1
03/18/22 16:02
03/21/22 14:37
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.39
0.19
1
03/18/22 16:02
03/21/22 14:37
108-60-1
Pentachlorophenol
ND
mg/kg
0.78
0.38
1
03/18/22 16:02
03/21/22 14:37
87-86-5
Phenanthrene
ND
mg/kg
0.39
0.13
1
03/18/22 16:02
03/21/22 14:37
85-01-8
Phenol
ND
mg/kg
0.39
0.17
1
03/18/22 16:02
03/21/22 14:37
108-95-2
Pyrene
ND
mg/kg
0.39
0.16
1
03/18/22 16:02
03/21/22 14:37
129-00-0
Pyridine
ND
mg/kg
0.39
0.12
1
03/18/22 16:02
03/21/22 14:37
110-86-1
1,2,4-Trichlorobenzene
ND
mg/kg
0.39
0.15
1
03/18/22 16:02
03/21/22 14:37
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.39
0.18
1
03/18/22 16:02
03/21/22 14:37
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.39
0.16
1
03/18/22 16:02
03/21/22 14:37
88-06-2
Surrogates
Nitrobenzene-d5 (S)
54
%
21-130
1
03/18/22 16:02
03/21/22 14:37
4165-60-0
2-Fluorobiphenyl (S)
60
%
19-130
1
03/18/22 16:02
03/21/22 14:37
321-60-8
Terphenyl-d14 (S)
59
%
15-130
1
03/18/22 16:02
03/21/22 14:37
1718-51-0
Phenol-d6 (S)
48
%
18-130
1
03/18/22 16:02
03/21/22 14:37
13127-88-3
2-Fluorophenol (S)
48
%
18-130
1
03/18/22 16:02
03/21/22 14:37
367-12-4
2,4,6-Tribromophenol (S)
68
%
18-130
1
03/18/22 16:02
03/21/22 14:37
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation
Method: EPA
5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
mg/kg
0.13
0.042
1
03/18/2214:41
03/18/2217:31
67-64-1
Benzene
ND
mg/kg
0.0066
0.0026
1
03/18/2214:41
03/18/2217:31
71-43-2
Bromobenzene
ND
mg/kg
0.0066
0.0022
1
03/18/2214:41
03/18/2217:31
108-86-1
Bromochloromethane
ND
mg/kg
0.0066
0.0020
1
03/18/2214:41
03/18/2217:31
74-97-5
Bromodichloromethane
ND
mg/kg
0.0066
0.0026
1
03/18/2214:41
03/18/2217:31
75-27-4
Bromoform
ND
mg/kg
0.0066
0.0023
1
03/18/2214:41
03/18/2217:31
75-25-2
Bromomethane
ND
mg/kg
0.013
0.010
1
03/18/2214:41
03/18/2217:31
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.13
0.032
1
03/18/22 14:41
03/18/22 17:31
78-93-3
n-Butylbenzene
ND
mg/kg
0.0066
0.0031
1
03/18/2214:41
03/18/2217:31
104-51-8
REPORT OF LABORATORY ANALYSIS
IL
IL
v2
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 46 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-4 Lab ID: 92593947010 Collected: 03/15/22 08:51 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
sec-Butylbenzene
ND
mg/kg
0.0066
0.0029
1
03/18/22 14:41
03/18/22 17:31
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0066
0.0024
1
03/18/22 14:41
03/18/22 17:31
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0066
0.0025
1
03/18/22 14:41
03/18/22 17:31
56-23-5
Chlorobenzene
ND
mg/kg
0.0066
0.0013
1
03/18/22 14:41
03/18/22 17:31
108-90-7
Chloroethane
ND
mg/kg
0.013
0.0051
1
03/18/22 14:41
03/18/22 17:31
75-00-3
Chloroform
ND
mg/kg
0.0066
0.0040
1
03/18/22 14:41
03/18/22 17:31
67-66-3
Chloromethane
ND
mg/kg
0.013
0.0056
1
03/18/22 14:41
03/18/22 17:31
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0066
0.0023
1
03/18/22 14:41
03/18/22 17:31
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0066
0.0012
1
03/18/22 14:41
03/18/22 17:31
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0066
0.0026
1
03/18/22 14:41
03/18/22 17:31
96-12-8
Dibromochloromethane
ND
mg/kg
0.0066
0.0037
1
03/18/22 14:41
03/18/22 17:31
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0066
0.0029
1
03/18/22 14:41
03/18/22 17:31
106-93-4
Dibromomethane
ND
mg/kg
0.0066
0.0014
1
03/18/22 14:41
03/18/22 17:31
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0066
0.0024
1
03/18/22 14:41
03/18/22 17:31
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0066
0.0020
1
03/18/22 14:41
03/18/22 17:31
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0066
0.0017
1
03/18/22 14:41
03/18/22 17:31
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.013
0.0029
1
03/18/22 14:41
03/18/22 17:31
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0066
0.0027
1
03/18/22 14:41
03/18/22 17:31
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0066
0.0044
1
03/18/22 14:41
03/18/22 17:31
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0066
0.0027
1
03/18/22 14:41
03/18/22 17:31
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0066
0.0023
1
03/18/22 14:41
03/18/22 17:31
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0066
0.0023
1
03/18/22 14:41
03/18/22 17:31
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0066
0.0020
1
03/18/22 14:41
03/18/22 17:31
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0066
0.0021
1
03/18/22 14:41
03/18/22 17:31
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0066
0.0022
1
03/18/22 14:41
03/18/22 17:31
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0066
0.0032
1
03/18/22 14:41
03/18/22 17:31
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0066
0.0018
1
03/18/22 14:41
03/18/22 17:31
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0066
0.0023
1
03/18/22 14:41
03/18/22 17:31
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0066
0.0018
1
03/18/22 14:41
03/18/22 17:31
108-20-3
Ethylbenzene
0.0036J
mg/kg
0.0066
0.0031
1
03/18/22 14:41
03/18/22 17:31
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.013
0.011
1
03/18/22 14:41
03/18/22 17:31
87-68-3
2-Hexanone
ND
mg/kg
0.066
0.0064
1
03/18/22 14:41
03/18/22 17:31
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0066
0.0022
1
03/18/22 14:41
03/18/22 17:31
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0066
0.0033
1
03/18/22 14:41
03/18/22 17:31
99-87-6
Methylene Chloride
ND
mg/kg
0.026
0.018
1
03/18/22 14:41
03/18/22 17:31
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.066
0.0064
1
03/18/22 14:41
03/18/22 17:31
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0066
0.0025
1
03/18/22 14:41
03/18/22 17:31
1634-04-4
Naphthalene
0.0065J
mg/kg
0.0066
0.0035
1
03/18/22 14:41
03/18/22 17:31
91-20-3
n-Propylbenzene
ND
mg/kg
0.0066
0.0024
1
03/18/22 14:41
03/18/22 17:31
103-65-1
Styrene
ND
mg/kg
0.0066
0.0017
1
03/18/22 14:41
03/18/22 17:31
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0066
0.0025
1
03/18/22 14:41
03/18/22 17:31
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0066
0.0017
1
03/18/22 14:41
03/18/22 17:31
79-34-5
Tetrachloroethene
ND
mg/kg
0.0066
0.0021
1
03/18/22 14:41
03/18/22 17:31
127-18-4
Toluene
0.0079
mg/kg
0.0066
0.0019
1
03/18/22 14:41
03/18/22 17:31
108-88-3
REPORT OF LABORATORY ANALYSIS
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Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 47 of 122

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-4
Lab ID:
92593947010
Collected:
03/15/22
08:51
Received: 03/15/22
16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services
- Charlotte
1,2,3-Trichlorobenzene
ND
mg/kg
0.0066
0.0053
1
03/18/22 14:41
03/18/22 17:31
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0066
0.0056
1
03/18/22 14:41
03/18/22 17:31
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0066
0.0034
1
03/18/22 14:41
03/18/22 17:31
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0066
0.0022
1
03/18/22 14:41
03/18/22 17:31
79-00-5
Trichloroethene
ND
mg/kg
0.0066
0.0017
1
03/18/22 14:41
03/18/22 17:31
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0066
0.0036
1
03/18/22 14:41
03/18/22 17:31
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.0066
0.0033
1
03/18/22 14:41
03/18/22 17:31
96-18-4
1,2,4-Trimethylbenzene
0.0046J
mg/kg
0.0066
0.0018
1
03/18/22 14:41
03/18/22 17:31
95-63-6
1,3,5-Trimethylbenzene
ND
mg/kg
0.0066
0.0022
1
03/18/22 14:41
03/18/22 17:31
108-67-8
Vinyl acetate
ND
mg/kg
0.066
0.0048
1
03/18/22 14:41
03/18/22 17:31
108-05-4
Vinyl chloride
ND
mg/kg
0.013
0.0034
1
03/18/22 14:41
03/18/22 17:31
75-01-4
Xylene (Total)
ND
mg/kg
0.013
0.0038
1
03/18/22 14:41
03/18/22 17:31
1330-20-7
m&p-Xylene
0.0081J
mg/kg
0.013
0.0045
1
03/18/22 14:41
03/18/22 17:31
179601-23-1
o-Xylene
0.0046J
mg/kg
0.0066
0.0029
1
03/18/22 14:41
03/18/22 17:31
95-47-6
Surrogates
Toluene-d8 (S)
99
%
70-130
1
03/18/22 14:41
03/18/22 17:31
2037-26-5
4-Bromofluorobenzene (S)
98
%
69-134
1
03/18/22 14:41
03/18/22 17:31
460-00-4
1,2-Dichloroethane-d4 (S)
94
%
70-130
1
03/18/22 14:41
03/18/22 17:31
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services
- Charlotte
Percent Moisture
16.5
%
0.10
0.10
1
03/17/22 14:46
N2
REPORT OF LABORATORY ANALYSIS
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Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 48 of 122

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2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-5 Lab ID: 92593947011 Collected: 03/15/22 09:15 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
mg/kg
0.41
0.15
1
03/18/22 16:02
03/21/22 15:04
83-32-9
Acenaphthylene
ND
mg/kg
0.41
0.15
1
03/18/22 16:02
03/21/22 15:04
208-96-8
Aniline
ND
mg/kg
0.41
0.16
1
03/18/22 16:02
03/21/22 15:04
62-53-3
Anthracene
ND
mg/kg
0.41
0.14
1
03/18/22 16:02
03/21/22 15:04
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.41
0.14
1
03/18/22 16:02
03/21/22 15:04
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.41
0.14
1
03/18/22 16:02
03/21/22 15:04
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.41
0.14
1
03/18/22 16:02
03/21/22 15:04
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.41
0.16
1
03/18/22 16:02
03/21/22 15:04
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.41
0.15
1
03/18/22 16:02
03/21/22 15:04
207-08-9
Benzoic Acid
ND
mg/kg
2.1
0.89
1
03/18/22 16:02
03/21/22 15:04
65-85-0
Benzyl alcohol
ND
mg/kg
0.83
0.31
1
03/18/22 16:02
03/21/22 15:04
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.41
0.16
1
03/18/22 16:02
03/21/22 15:04
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.41
0.17
1
03/18/22 16:02
03/21/22 15:04
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
0.83
0.29
1
03/18/22 16:02
03/21/22 15:04
59-50-7
4-Chloroaniline
ND
mg/kg
0.83
0.32
1
03/18/22 16:02
03/21/22 15:04
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.41
0.17
1
03/18/22 16:02
03/21/22 15:04
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.41
0.16
1
03/18/22 16:02
03/21/22 15:04
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.41
0.16
1
03/18/22 16:02
03/21/22 15:04
91-58-7
2-Chlorophenol
ND
mg/kg
0.41
0.16
1
03/18/22 16:02
03/21/22 15:04
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.41
0.15
1
03/18/22 16:02
03/21/22 15:04
7005-72-3
Chrysene
ND
mg/kg
0.41
0.15
1
03/18/22 16:02
03/21/22 15:04
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.41
0.16
1
03/18/22 16:02
03/21/22 15:04
53-70-3
Dibenzofuran
ND
mg/kg
0.41
0.15
1
03/18/22 16:02
03/21/22 15:04
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.41
0.15
1
03/18/22 16:02
03/21/22 15:04
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.41
0.15
1
03/18/22 16:02
03/21/22 15:04
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.41
0.16
1
03/18/22 16:02
03/21/22 15:04
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
0.83
0.28
1
03/18/22 16:02
03/21/22 15:04
91-94-1
2,4-Dichlorophenol
ND
mg/kg
0.41
0.16
1
03/18/22 16:02
03/21/22 15:04
120-83-2
Diethylphthalate
ND
mg/kg
0.41
0.15
1
03/18/22 16:02
03/21/22 15:04
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.41
0.17
1
03/18/22 16:02
03/21/22 15:04
105-67-9
Dimethylphthalate
ND
mg/kg
0.41
0.15
1
03/18/22 16:02
03/21/22 15:04
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.41
0.14
1
03/18/22 16:02
03/21/22 15:04
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.83
0.39
1
03/18/22 16:02
03/21/22 15:04
534-52-1
2,4-Dinitrophenol
ND
mg/kg
2.1
1.3
1
03/18/22 16:02
03/21/22 15:04
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.41
0.16
1
03/18/22 16:02
03/21/22 15:04
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.41
0.15
1
03/18/22 16:02
03/21/22 15:04
606-20-2
Di-n-octylphthalate
ND
mg/kg
0.41
0.16
1
03/18/22 16:02
03/21/22 15:04
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.41
0.16
1
03/18/22 16:02
03/21/22 15:04
117-81-7
Fluoranthene
ND
mg/kg
0.41
0.14
1
03/18/22 16:02
03/21/22 15:04
206-44-0
Fluorene
ND
mg/kg
0.41
0.15
1
03/18/22 16:02
03/21/22 15:04
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.41
0.18
1
03/18/22 16:02
03/21/22 15:04
87-68-3
Hexachlorobenzene
ND
mg/kg
0.41
0.16
1
03/18/22 16:02
03/21/22 15:04
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.41
0.24
1
03/18/22 16:02
03/21/22 15:04
77-47-4
Hexachloroethane
ND
mg/kg
0.41
0.16
1
03/18/22 16:02
03/21/22 15:04
67-72-1
REPORT OF LABORATORY ANALYSIS
IL
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Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 49 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: SB-5 Lab ID: 92593947011 Collected: 03/15/22 09:15 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.41
0.16
1
03/18/22 16:02
03/21/22 15:04
193-39-5
Isophorone
ND
mg/kg
0.41
0.18
1
03/18/22 16:02
03/21/22 15:04
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.41
0.15
1
03/18/22 16:02
03/21/22 15:04
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.41
0.17
1
03/18/22 16:02
03/21/22 15:04
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.41
0.17
1
03/18/22 16:02
03/21/22 15:04
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.41
0.17
1
03/18/22 16:02
03/21/22 15:04
15831-10-4
Naphthalene
ND
mg/kg
0.41
0.14
1
03/18/22 16:02
03/21/22 15:04
91-20-3
2-Nitroaniline
ND
mg/kg
2.1
0.34
1
03/18/22 16:02
03/21/22 15:04
88-74-4
3-Nitroaniline
ND
mg/kg
2.1
0.32
1
03/18/22 16:02
03/21/22 15:04
99-09-2
4-Nitroaniline
ND
mg/kg
0.83
0.31
1
03/18/22 16:02
03/21/22 15:04
100-01-6
Nitrobenzene
ND
mg/kg
0.41
0.19
1
03/18/22 16:02
03/21/22 15:04
98-95-3
2-Nitrophenol
ND
mg/kg
0.41
0.18
1
03/18/22 16:02
03/21/22 15:04
88-75-5
4-Nitrophenol
ND
mg/kg
2.1
0.80
1
03/18/22 16:02
03/21/22 15:04
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.41
0.14
1
03/18/22 16:02
03/21/22 15:04
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.41
0.16
1
03/18/22 16:02
03/21/22 15:04
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.41
0.15
1
03/18/22 16:02
03/21/22 15:04
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.41
0.20
1
03/18/22 16:02
03/21/22 15:04
108-60-1
Pentachlorophenol
ND
mg/kg
0.83
0.40
1
03/18/22 16:02
03/21/22 15:04
87-86-5
Phenanthrene
ND
mg/kg
0.41
0.14
1
03/18/22 16:02
03/21/22 15:04
85-01-8
Phenol
ND
mg/kg
0.41
0.18
1
03/18/22 16:02
03/21/22 15:04
108-95-2
Pyrene
ND
mg/kg
0.41
0.17
1
03/18/22 16:02
03/21/22 15:04
129-00-0
Pyridine
ND
mg/kg
0.41
0.13
1
03/18/22 16:02
03/21/22 15:04
110-86-1
1,2,4-Trichlorobenzene
ND
mg/kg
0.41
0.16
1
03/18/22 16:02
03/21/22 15:04
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.41
0.19
1
03/18/22 16:02
03/21/22 15:04
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.41
0.17
1
03/18/22 16:02
03/21/22 15:04
88-06-2
Surrogates
Nitrobenzene-d5 (S)
60
%
21-130
1
03/18/22 16:02
03/21/22 15:04
4165-60-0
2-Fluorobiphenyl (S)
69
%
19-130
1
03/18/22 16:02
03/21/22 15:04
321-60-8
Terphenyl-d14 (S)
79
%
15-130
1
03/18/22 16:02
03/21/22 15:04
1718-51-0
Phenol-d6 (S)
62
%
18-130
1
03/18/22 16:02
03/21/22 15:04
13127-88-3
2-Fluorophenol (S)
56
%
18-130
1
03/18/22 16:02
03/21/22 15:04
367-12-4
2,4,6-Tribromophenol (S)
72
%
18-130
1
03/18/22 16:02
03/21/22 15:04
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation
Method: EPA
5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
mg/kg
0.15
0.047
1
03/18/2214:41
03/18/2217:48
67-64-1
Benzene
ND
mg/kg
0.0073
0.0029
1
03/18/2214:41
03/18/2217:48
71-43-2
Bromobenzene
ND
mg/kg
0.0073
0.0024
1
03/18/2214:41
03/18/2217:48
108-86-1
Bromochloromethane
ND
mg/kg
0.0073
0.0021
1
03/18/2214:41
03/18/2217:48
74-97-5
Bromodichloromethane
ND
mg/kg
0.0073
0.0028
1
03/18/2214:41
03/18/2217:48
75-27-4
Bromoform
ND
mg/kg
0.0073
0.0026
1
03/18/2214:41
03/18/2217:48
75-25-2
Bromomethane
ND
mg/kg
0.015
0.011
1
03/18/2214:41
03/18/2217:48
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.15
0.035
1
03/18/22 14:41
03/18/22 17:48
78-93-3
n-Butylbenzene
ND
mg/kg
0.0073
0.0034
1
03/18/2214:41
03/18/2217:48
104-51-8
REPORT OF LABORATORY ANALYSIS
IL
IL
v2
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 50 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-5 Lab ID: 92593947011 Collected: 03/15/22 09:15 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
sec-Butylbenzene
ND
mg/kg
0.0073
0.0032
1
03/18/22 14:41
03/18/22 17:48
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0073
0.0026
1
03/18/22 14:41
03/18/22 17:48
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0073
0.0027
1
03/18/22 14:41
03/18/22 17:48
56-23-5
Chlorobenzene
ND
mg/kg
0.0073
0.0014
1
03/18/22 14:41
03/18/22 17:48
108-90-7
Chloroethane
ND
mg/kg
0.015
0.0056
1
03/18/22 14:41
03/18/22 17:48
75-00-3
Chloroform
ND
mg/kg
0.0073
0.0044
1
03/18/22 14:41
03/18/22 17:48
67-66-3
Chloromethane
ND
mg/kg
0.015
0.0061
1
03/18/22 14:41
03/18/22 17:48
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0073
0.0026
1
03/18/22 14:41
03/18/22 17:48
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0073
0.0013
1
03/18/22 14:41
03/18/22 17:48
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0073
0.0028
1
03/18/22 14:41
03/18/22 17:48
96-12-8
Dibromochloromethane
ND
mg/kg
0.0073
0.0041
1
03/18/22 14:41
03/18/22 17:48
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0073
0.0032
1
03/18/22 14:41
03/18/22 17:48
106-93-4
Dibromomethane
ND
mg/kg
0.0073
0.0016
1
03/18/22 14:41
03/18/22 17:48
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0073
0.0026
1
03/18/22 14:41
03/18/22 17:48
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0073
0.0022
1
03/18/22 14:41
03/18/22 17:48
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0073
0.0019
1
03/18/22 14:41
03/18/22 17:48
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.015
0.0031
1
03/18/22 14:41
03/18/22 17:48
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0073
0.0030
1
03/18/22 14:41
03/18/22 17:48
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0073
0.0048
1
03/18/22 14:41
03/18/22 17:48
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0073
0.0030
1
03/18/22 14:41
03/18/22 17:48
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0073
0.0025
1
03/18/22 14:41
03/18/22 17:48
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0073
0.0025
1
03/18/22 14:41
03/18/22 17:48
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0073
0.0022
1
03/18/22 14:41
03/18/22 17:48
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0073
0.0023
1
03/18/22 14:41
03/18/22 17:48
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0073
0.0024
1
03/18/22 14:41
03/18/22 17:48
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0073
0.0035
1
03/18/22 14:41
03/18/22 17:48
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0073
0.0020
1
03/18/22 14:41
03/18/22 17:48
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0073
0.0025
1
03/18/22 14:41
03/18/22 17:48
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0073
0.0020
1
03/18/22 14:41
03/18/22 17:48
108-20-3
Ethylbenzene
ND
mg/kg
0.0073
0.0034
1
03/18/22 14:41
03/18/22 17:48
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.015
0.012
1
03/18/22 14:41
03/18/22 17:48
87-68-3
2-Hexanone
ND
mg/kg
0.073
0.0070
1
03/18/22 14:41
03/18/22 17:48
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0073
0.0025
1
03/18/22 14:41
03/18/22 17:48
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0073
0.0036
1
03/18/22 14:41
03/18/22 17:48
99-87-6
Methylene Chloride
ND
mg/kg
0.029
0.020
1
03/18/22 14:41
03/18/22 17:48
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.073
0.0070
1
03/18/22 14:41
03/18/22 17:48
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0073
0.0027
1
03/18/22 14:41
03/18/22 17:48
1634-04-4
Naphthalene
ND
mg/kg
0.0073
0.0038
1
03/18/22 14:41
03/18/22 17:48
91-20-3
n-Propylbenzene
ND
mg/kg
0.0073
0.0026
1
03/18/22 14:41
03/18/22 17:48
103-65-1
Styrene
ND
mg/kg
0.0073
0.0019
1
03/18/22 14:41
03/18/22 17:48
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0073
0.0028
1
03/18/22 14:41
03/18/22 17:48
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0073
0.0019
1
03/18/22 14:41
03/18/22 17:48
79-34-5
Tetrachloroethene
ND
mg/kg
0.0073
0.0023
1
03/18/22 14:41
03/18/22 17:48
127-18-4
Toluene
ND
mg/kg
0.0073
0.0021
1
03/18/22 14:41
03/18/22 17:48
108-88-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 51 of 122

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-5
Lab ID:
92593947011
Collected:
03/15/22
09:15
Received: 03/15/22
16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services
- Charlotte
1,2,3-Trichlorobenzene
ND
mg/kg
0.0073
0.0059
1
03/18/22 14:41
03/18/22 17:48
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0073
0.0061
1
03/18/22 14:41
03/18/22 17:48
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0073
0.0038
1
03/18/22 14:41
03/18/22 17:48
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0073
0.0024
1
03/18/22 14:41
03/18/22 17:48
79-00-5
Trichloroethene
ND
mg/kg
0.0073
0.0019
1
03/18/22 14:41
03/18/22 17:48
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0073
0.0040
1
03/18/22 14:41
03/18/22 17:48
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.0073
0.0037
1
03/18/22 14:41
03/18/22 17:48
96-18-4
1,2,4-Trimethylbenzene
ND
mg/kg
0.0073
0.0020
1
03/18/22 14:41
03/18/22 17:48
95-63-6
1,3,5-Trimethylbenzene
ND
mg/kg
0.0073
0.0024
1
03/18/22 14:41
03/18/22 17:48
108-67-8
Vinyl acetate
ND
mg/kg
0.073
0.0053
1
03/18/22 14:41
03/18/22 17:48
108-05-4
Vinyl chloride
ND
mg/kg
0.015
0.0037
1
03/18/22 14:41
03/18/22 17:48
75-01-4
Xylene (Total)
ND
mg/kg
0.015
0.0041
1
03/18/22 14:41
03/18/22 17:48
1330-20-7
m&p-Xylene
ND
mg/kg
0.015
0.0050
1
03/18/22 14:41
03/18/22 17:48
179601-23-1
o-Xylene
ND
mg/kg
0.0073
0.0032
1
03/18/22 14:41
03/18/22 17:48
95-47-6
Surrogates
Toluene-d8 (S)
99
%
70-130
1
03/18/22 14:41
03/18/22 17:48
2037-26-5
4-Bromofluorobenzene (S)
99
%
69-134
1
03/18/22 14:41
03/18/22 17:48
460-00-4
1,2-Dichloroethane-d4 (S)
94
%
70-130
1
03/18/22 14:41
03/18/22 17:48
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services
- Charlotte
Percent Moisture
21.1
%
0.10
0.10
1
03/17/22 14:46
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 52 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-6 Lab ID: 92593947012 Collected: 03/15/22 09:32 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
mg/kg
0.38
0.13
1
03/18/22 16:02
03/21/22 15:31
83-32-9
Acenaphthylene
ND
mg/kg
0.38
0.13
1
03/18/22 16:02
03/21/22 15:31
208-96-8
Aniline
ND
mg/kg
0.38
0.15
1
03/18/22 16:02
03/21/22 15:31
62-53-3
Anthracene
ND
mg/kg
0.38
0.13
1
03/18/22 16:02
03/21/22 15:31
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.38
0.13
1
03/18/22 16:02
03/21/22 15:31
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.38
0.13
1
03/18/22 16:02
03/21/22 15:31
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.38
0.13
1
03/18/22 16:02
03/21/22 15:31
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.38
0.15
1
03/18/22 16:02
03/21/22 15:31
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.38
0.13
1
03/18/22 16:02
03/21/22 15:31
207-08-9
Benzoic Acid
ND
mg/kg
1.9
0.83
1
03/18/22 16:02
03/21/22 15:31
65-85-0
Benzyl alcohol
ND
mg/kg
0.77
0.29
1
03/18/22 16:02
03/21/22 15:31
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.38
0.15
1
03/18/22 16:02
03/21/22 15:31
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.38
0.16
1
03/18/22 16:02
03/21/22 15:31
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
0.77
0.27
1
03/18/22 16:02
03/21/22 15:31
59-50-7
4-Chloroaniline
ND
mg/kg
0.77
0.30
1
03/18/22 16:02
03/21/22 15:31
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.38
0.16
1
03/18/22 16:02
03/21/22 15:31
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.38
0.14
1
03/18/22 16:02
03/21/22 15:31
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.38
0.15
1
03/18/22 16:02
03/21/22 15:31
91-58-7
2-Chlorophenol
ND
mg/kg
0.38
0.14
1
03/18/22 16:02
03/21/22 15:31
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.38
0.14
1
03/18/22 16:02
03/21/22 15:31
7005-72-3
Chrysene
ND
mg/kg
0.38
0.14
1
03/18/22 16:02
03/21/22 15:31
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.38
0.15
1
03/18/22 16:02
03/21/22 15:31
53-70-3
Dibenzofuran
ND
mg/kg
0.38
0.14
1
03/18/22 16:02
03/21/22 15:31
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.38
0.14
1
03/18/22 16:02
03/21/22 15:31
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.38
0.14
1
03/18/22 16:02
03/21/22 15:31
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.38
0.15
1
03/18/22 16:02
03/21/22 15:31
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
0.77
0.26
1
03/18/22 16:02
03/21/22 15:31
91-94-1
2,4-Dichlorophenol
ND
mg/kg
0.38
0.15
1
03/18/22 16:02
03/21/22 15:31
120-83-2
Diethylphthalate
ND
mg/kg
0.38
0.14
1
03/18/22 16:02
03/21/22 15:31
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.38
0.16
1
03/18/22 16:02
03/21/22 15:31
105-67-9
Dimethylphthalate
ND
mg/kg
0.38
0.14
1
03/18/22 16:02
03/21/22 15:31
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.38
0.13
1
03/18/22 16:02
03/21/22 15:31
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.77
0.36
1
03/18/22 16:02
03/21/22 15:31
534-52-1
2,4-Dinitrophenol
ND
mg/kg
1.9
1.2
1
03/18/22 16:02
03/21/22 15:31
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.38
0.15
1
03/18/22 16:02
03/21/22 15:31
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.38
0.14
1
03/18/22 16:02
03/21/22 15:31
606-20-2
Di-n-octylphthalate
ND
mg/kg
0.38
0.15
1
03/18/22 16:02
03/21/22 15:31
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.38
0.15
1
03/18/22 16:02
03/21/22 15:31
117-81-7
Fluoranthene
ND
mg/kg
0.38
0.13
1
03/18/22 16:02
03/21/22 15:31
206-44-0
Fluorene
ND
mg/kg
0.38
0.13
1
03/18/22 16:02
03/21/22 15:31
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.38
0.17
1
03/18/22 16:02
03/21/22 15:31
87-68-3
Hexachlorobenzene
ND
mg/kg
0.38
0.15
1
03/18/22 16:02
03/21/22 15:31
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.38
0.22
1
03/18/22 16:02
03/21/22 15:31
77-47-4
Hexachloroethane
ND
mg/kg
0.38
0.15
1
03/18/22 16:02
03/21/22 15:31
67-72-1
REPORT OF LABORATORY ANALYSIS
IL
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 53 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: SB-6 Lab ID: 92593947012 Collected: 03/15/22 09:32 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.38
0.15
1
03/18/22 16:02
03/21/22 15:31
193-39-5
Isophorone
ND
mg/kg
0.38
0.17
1
03/18/22 16:02
03/21/22 15:31
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.38
0.13
1
03/18/22 16:02
03/21/22 15:31
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.38
0.15
1
03/18/22 16:02
03/21/22 15:31
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.38
0.16
1
03/18/22 16:02
03/21/22 15:31
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.38
0.15
1
03/18/22 16:02
03/21/22 15:31
15831-10-4
Naphthalene
ND
mg/kg
0.38
0.13
1
03/18/22 16:02
03/21/22 15:31
91-20-3
2-Nitroaniline
ND
mg/kg
1.9
0.31
1
03/18/22 16:02
03/21/22 15:31
88-74-4
3-Nitroaniline
ND
mg/kg
1.9
0.30
1
03/18/22 16:02
03/21/22 15:31
99-09-2
4-Nitroaniline
ND
mg/kg
0.77
0.29
1
03/18/22 16:02
03/21/22 15:31
100-01-6
Nitrobenzene
ND
mg/kg
0.38
0.18
1
03/18/22 16:02
03/21/22 15:31
98-95-3
2-Nitrophenol
ND
mg/kg
0.38
0.17
1
03/18/22 16:02
03/21/22 15:31
88-75-5
4-Nitrophenol
ND
mg/kg
1.9
0.74
1
03/18/22 16:02
03/21/22 15:31
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.38
0.13
1
03/18/22 16:02
03/21/22 15:31
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.38
0.14
1
03/18/22 16:02
03/21/22 15:31
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.38
0.14
1
03/18/22 16:02
03/21/22 15:31
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.38
0.18
1
03/18/22 16:02
03/21/22 15:31
108-60-1
Pentachlorophenol
ND
mg/kg
0.77
0.38
1
03/18/22 16:02
03/21/22 15:31
87-86-5
Phenanthrene
ND
mg/kg
0.38
0.13
1
03/18/22 16:02
03/21/22 15:31
85-01-8
Phenol
ND
mg/kg
0.38
0.17
1
03/18/22 16:02
03/21/22 15:31
108-95-2
Pyrene
ND
mg/kg
0.38
0.16
1
03/18/22 16:02
03/21/22 15:31
129-00-0
Pyridine
ND
mg/kg
0.38
0.12
1
03/18/22 16:02
03/21/22 15:31
110-86-1
1,2,4-Trichlorobenzene
ND
mg/kg
0.38
0.15
1
03/18/22 16:02
03/21/22 15:31
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.38
0.18
1
03/18/22 16:02
03/21/22 15:31
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.38
0.16
1
03/18/22 16:02
03/21/22 15:31
88-06-2
Surrogates
Nitrobenzene-d5 (S)
43
%
21-130
1
03/18/22 16:02
03/21/22 15:31
4165-60-0
2-Fluorobiphenyl (S)
45
%
19-130
1
03/18/22 16:02
03/21/22 15:31
321-60-8
Terphenyl-d14 (S)
48
%
15-130
1
03/18/22 16:02
03/21/22 15:31
1718-51-0
Phenol-d6 (S)
47
%
18-130
1
03/18/22 16:02
03/21/22 15:31
13127-88-3
2-Fluorophenol (S)
44
%
18-130
1
03/18/22 16:02
03/21/22 15:31
367-12-4
2,4,6-Tribromophenol (S)
48
%
18-130
1
03/18/22 16:02
03/21/22 15:31
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation
Method: EPA
5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
mg/kg
0.12
0.039
1
03/18/2214:41
03/18/2218:06
67-64-1
Benzene
ND
mg/kg
0.0061
0.0024
1
03/18/2214:41
03/18/2218:06
71-43-2
Bromobenzene
ND
mg/kg
0.0061
0.0020
1
03/18/2214:41
03/18/2218:06
108-86-1
Bromochloromethane
ND
mg/kg
0.0061
0.0018
1
03/18/2214:41
03/18/2218:06
74-97-5
Bromodichloromethane
ND
mg/kg
0.0061
0.0024
1
03/18/2214:41
03/18/2218:06
75-27-4
Bromoform
ND
mg/kg
0.0061
0.0022
1
03/18/2214:41
03/18/2218:06
75-25-2
Bromomethane
ND
mg/kg
0.012
0.0097
1
03/18/2214:41
03/18/2218:06
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.12
0.030
1
03/18/22 14:41
03/18/22 18:06
78-93-3
n-Butylbenzene
ND
mg/kg
0.0061
0.0029
1
03/18/2214:41
03/18/2218:06
104-51-8
REPORT OF LABORATORY ANALYSIS
IL
IL
v2
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Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 54 of 122

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-6 Lab ID: 92593947012 Collected: 03/15/22 09:32 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
sec-Butylbenzene
ND
mg/kg
0.0061
0.0027
1
03/18/22 14:41
03/18/22 18:06
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0061
0.0022
1
03/18/22 14:41
03/18/22 18:06
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0061
0.0023
1
03/18/22 14:41
03/18/22 18:06
56-23-5
Chlorobenzene
ND
mg/kg
0.0061
0.0012
1
03/18/22 14:41
03/18/22 18:06
108-90-7
Chloroethane
ND
mg/kg
0.012
0.0047
1
03/18/22 14:41
03/18/22 18:06
75-00-3
Chloroform
ND
mg/kg
0.0061
0.0037
1
03/18/22 14:41
03/18/22 18:06
67-66-3
Chloromethane
ND
mg/kg
0.012
0.0052
1
03/18/22 14:41
03/18/22 18:06
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0061
0.0022
1
03/18/22 14:41
03/18/22 18:06
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0061
0.0011
1
03/18/22 14:41
03/18/22 18:06
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0061
0.0024
1
03/18/22 14:41
03/18/22 18:06
96-12-8
Dibromochloromethane
ND
mg/kg
0.0061
0.0035
1
03/18/22 14:41
03/18/22 18:06
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0061
0.0027
1
03/18/22 14:41
03/18/22 18:06
106-93-4
Dibromomethane
ND
mg/kg
0.0061
0.0013
1
03/18/22 14:41
03/18/22 18:06
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0061
0.0022
1
03/18/22 14:41
03/18/22 18:06
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0061
0.0019
1
03/18/22 14:41
03/18/22 18:06
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0061
0.0016
1
03/18/22 14:41
03/18/22 18:06
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.012
0.0027
1
03/18/22 14:41
03/18/22 18:06
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0061
0.0025
1
03/18/22 14:41
03/18/22 18:06
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0061
0.0041
1
03/18/22 14:41
03/18/22 18:06
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0061
0.0025
1
03/18/22 14:41
03/18/22 18:06
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0061
0.0021
1
03/18/22 14:41
03/18/22 18:06
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0061
0.0022
1
03/18/22 14:41
03/18/22 18:06
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0061
0.0018
1
03/18/22 14:41
03/18/22 18:06
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0061
0.0019
1
03/18/22 14:41
03/18/22 18:06
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0061
0.0020
1
03/18/22 14:41
03/18/22 18:06
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0061
0.0030
1
03/18/22 14:41
03/18/22 18:06
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0061
0.0017
1
03/18/22 14:41
03/18/22 18:06
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0061
0.0021
1
03/18/22 14:41
03/18/22 18:06
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0061
0.0017
1
03/18/22 14:41
03/18/22 18:06
108-20-3
Ethylbenzene
0.0041J
mg/kg
0.0061
0.0029
1
03/18/22 14:41
03/18/22 18:06
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.012
0.010
1
03/18/22 14:41
03/18/22 18:06
87-68-3
2-Hexanone
ND
mg/kg
0.061
0.0059
1
03/18/22 14:41
03/18/22 18:06
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0061
0.0021
1
03/18/22 14:41
03/18/22 18:06
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0061
0.0030
1
03/18/22 14:41
03/18/22 18:06
99-87-6
Methylene Chloride
ND
mg/kg
0.025
0.017
1
03/18/22 14:41
03/18/22 18:06
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.061
0.0059
1
03/18/22 14:41
03/18/22 18:06
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0061
0.0023
1
03/18/22 14:41
03/18/22 18:06
1634-04-4
Naphthalene
0.012
mg/kg
0.0061
0.0032
1
03/18/22 14:41
03/18/22 18:06
91-20-3
n-Propylbenzene
ND
mg/kg
0.0061
0.0022
1
03/18/22 14:41
03/18/22 18:06
103-65-1
Styrene
ND
mg/kg
0.0061
0.0016
1
03/18/22 14:41
03/18/22 18:06
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0061
0.0024
1
03/18/22 14:41
03/18/22 18:06
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0061
0.0016
1
03/18/22 14:41
03/18/22 18:06
79-34-5
Tetrachloroethene
ND
mg/kg
0.0061
0.0019
1
03/18/22 14:41
03/18/22 18:06
127-18-4
Toluene
0.012
mg/kg
0.0061
0.0017
1
03/18/22 14:41
03/18/22 18:06
108-88-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 55 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-6
Lab ID:
92593947012
Collected:
03/15/22
09:32
Received: 03/15/22
16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services
- Charlotte
1,2,3-Trichlorobenzene
ND
mg/kg
0.0061
0.0050
1
03/18/22 14:41
03/18/22 18:06
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0061
0.0052
1
03/18/22 14:41
03/18/22 18:06
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0061
0.0032
1
03/18/22 14:41
03/18/22 18:06
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0061
0.0020
1
03/18/22 14:41
03/18/22 18:06
79-00-5
Trichloroethene
ND
mg/kg
0.0061
0.0016
1
03/18/22 14:41
03/18/22 18:06
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0061
0.0034
1
03/18/22 14:41
03/18/22 18:06
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.0061
0.0031
1
03/18/22 14:41
03/18/22 18:06
96-18-4
1,2,4-Trimethylbenzene
0.0064
mg/kg
0.0061
0.0017
1
03/18/22 14:41
03/18/22 18:06
95-63-6
1,3,5-Trimethylbenzene
ND
mg/kg
0.0061
0.0021
1
03/18/22 14:41
03/18/22 18:06
108-67-8
Vinyl acetate
ND
mg/kg
0.061
0.0045
1
03/18/22 14:41
03/18/22 18:06
108-05-4
Vinyl chloride
ND
mg/kg
0.012
0.0031
1
03/18/22 14:41
03/18/22 18:06
75-01-4
Xylene (Total)
0.024
mg/kg
0.012
0.0035
1
03/18/22 14:41
03/18/22 18:06
1330-20-7
m&p-Xylene
0.015
mg/kg
0.012
0.0042
1
03/18/22 14:41
03/18/22 18:06
179601-23-1
o-Xylene
0.0093
mg/kg
0.0061
0.0027
1
03/18/22 14:41
03/18/22 18:06
95-47-6
Surrogates
Toluene-d8 (S)
98
%
70-130
1
03/18/22 14:41
03/18/22 18:06
2037-26-5
4-Bromofluorobenzene (S)
96
%
69-134
1
03/18/22 14:41
03/18/22 18:06
460-00-4
1,2-Dichloroethane-d4 (S)
94
%
70-130
1
03/18/22 14:41
03/18/22 18:06
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services
- Charlotte
Percent Moisture
14.1
%
0.10
0.10
1
03/17/22 14:46
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 56 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-7 Lab ID: 92593947013 Collected: 03/15/22 09:53 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 15:57
83-32-9
Acenaphthylene
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 15:57
208-96-8
Aniline
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 15:57
62-53-3
Anthracene
ND
mg/kg
0.36
0.12
1
03/18/22 16:02
03/21/22 15:57
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.36
0.12
1
03/18/22 16:02
03/21/22 15:57
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 15:57
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.36
0.12
1
03/18/22 16:02
03/21/22 15:57
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 15:57
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 15:57
207-08-9
Benzoic Acid
ND
mg/kg
1.8
0.78
1
03/18/22 16:02
03/21/22 15:57
65-85-0
Benzyl alcohol
ND
mg/kg
0.73
0.28
1
03/18/22 16:02
03/21/22 15:57
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 15:57
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.36
0.15
1
03/18/22 16:02
03/21/22 15:57
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
0.73
0.26
1
03/18/22 16:02
03/21/22 15:57
59-50-7
4-Chloroaniline
ND
mg/kg
0.73
0.29
1
03/18/22 16:02
03/21/22 15:57
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.36
0.15
1
03/18/22 16:02
03/21/22 15:57
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 15:57
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 15:57
91-58-7
2-Chlorophenol
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 15:57
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 15:57
7005-72-3
Chrysene
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 15:57
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 15:57
53-70-3
Dibenzofuran
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 15:57
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 15:57
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 15:57
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 15:57
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
0.73
0.25
1
03/18/22 16:02
03/21/22 15:57
91-94-1
2,4-Dichlorophenol
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 15:57
120-83-2
Diethylphthalate
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 15:57
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.36
0.15
1
03/18/22 16:02
03/21/22 15:57
105-67-9
Dimethylphthalate
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 15:57
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.36
0.12
1
03/18/22 16:02
03/21/22 15:57
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.73
0.34
1
03/18/22 16:02
03/21/22 15:57
534-52-1
2,4-Dinitrophenol
ND
mg/kg
1.8
1.1
1
03/18/22 16:02
03/21/22 15:57
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 15:57
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 15:57
606-20-2
Di-n-octylphthalate
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 15:57
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 15:57
117-81-7
Fluoranthene
ND
mg/kg
0.36
0.12
1
03/18/22 16:02
03/21/22 15:57
206-44-0
Fluorene
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 15:57
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.36
0.16
1
03/18/22 16:02
03/21/22 15:57
87-68-3
Hexachlorobenzene
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 15:57
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.36
0.21
1
03/18/22 16:02
03/21/22 15:57
77-47-4
Hexachloroethane
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 15:57
67-72-1
REPORT OF LABORATORY ANALYSIS
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Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 57 of 122

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: SB-7 Lab ID: 92593947013 Collected: 03/15/22 09:53 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 15:57
193-39-5
Isophorone
ND
mg/kg
0.36
0.16
1
03/18/22 16:02
03/21/22 15:57
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 15:57
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.36
0.15
1
03/18/22 16:02
03/21/22 15:57
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.36
0.15
1
03/18/22 16:02
03/21/22 15:57
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.36
0.15
1
03/18/22 16:02
03/21/22 15:57
15831-10-4
Naphthalene
ND
mg/kg
0.36
0.12
1
03/18/22 16:02
03/21/22 15:57
91-20-3
2-Nitroaniline
ND
mg/kg
1.8
0.30
1
03/18/22 16:02
03/21/22 15:57
88-74-4
3-Nitroaniline
ND
mg/kg
1.8
0.29
1
03/18/22 16:02
03/21/22 15:57
99-09-2
4-Nitroaniline
ND
mg/kg
0.73
0.28
1
03/18/22 16:02
03/21/22 15:57
100-01-6
Nitrobenzene
ND
mg/kg
0.36
0.17
1
03/18/22 16:02
03/21/22 15:57
98-95-3
2-Nitrophenol
ND
mg/kg
0.36
0.16
1
03/18/22 16:02
03/21/22 15:57
88-75-5
4-Nitrophenol
ND
mg/kg
1.8
0.71
1
03/18/22 16:02
03/21/22 15:57
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.36
0.12
1
03/18/22 16:02
03/21/22 15:57
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 15:57
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 15:57
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.36
0.17
1
03/18/22 16:02
03/21/22 15:57
108-60-1
Pentachlorophenol
ND
mg/kg
0.73
0.36
1
03/18/22 16:02
03/21/22 15:57
87-86-5
Phenanthrene
ND
mg/kg
0.36
0.12
1
03/18/22 16:02
03/21/22 15:57
85-01-8
Phenol
ND
mg/kg
0.36
0.16
1
03/18/22 16:02
03/21/22 15:57
108-95-2
Pyrene
ND
mg/kg
0.36
0.15
1
03/18/22 16:02
03/21/22 15:57
129-00-0
Pyridine
ND
mg/kg
0.36
0.11
1
03/18/22 16:02
03/21/22 15:57
110-86-1
1,2,4-Trichlorobenzene
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 15:57
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.36
0.17
1
03/18/22 16:02
03/21/22 15:57
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.36
0.15
1
03/18/22 16:02
03/21/22 15:57
88-06-2
Surrogates
Nitrobenzene-d5 (S)
42
%
21-130
1
03/18/22 16:02
03/21/22 15:57
4165-60-0
2-Fluorobiphenyl (S)
44
%
19-130
1
03/18/22 16:02
03/21/22 15:57
321-60-8
Terphenyl-d14 (S)
50
%
15-130
1
03/18/22 16:02
03/21/22 15:57
1718-51-0
Phenol-d6 (S)
43
%
18-130
1
03/18/22 16:02
03/21/22 15:57
13127-88-3
2-Fluorophenol (S)
39
%
18-130
1
03/18/22 16:02
03/21/22 15:57
367-12-4
2,4,6-Tribromophenol (S)
35
%
18-130
1
03/18/22 16:02
03/21/22 15:57
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation
Method: EPA
5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
mg/kg
0.15
0.047
1
03/18/2214:41
03/18/2218:24
67-64-1
Benzene
ND
mg/kg
0.0073
0.0029
1
03/18/2214:41
03/18/2218:24
71-43-2
Bromobenzene
ND
mg/kg
0.0073
0.0024
1
03/18/2214:41
03/18/2218:24
108-86-1
Bromochloromethane
ND
mg/kg
0.0073
0.0022
1
03/18/2214:41
03/18/2218:24
74-97-5
Bromodichloromethane
ND
mg/kg
0.0073
0.0028
1
03/18/2214:41
03/18/2218:24
75-27-4
Bromoform
ND
mg/kg
0.0073
0.0026
1
03/18/2214:41
03/18/2218:24
75-25-2
Bromomethane
ND
mg/kg
0.015
0.012
1
03/18/2214:41
03/18/2218:24
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.15
0.035
1
03/18/22 14:41
03/18/22 18:24
78-93-3
n-Butylbenzene
ND
mg/kg
0.0073
0.0034
1
03/18/2214:41
03/18/2218:24
104-51-8
REPORT OF LABORATORY ANALYSIS
IL
IL
v2
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Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 58 of 122

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-7 Lab ID: 92593947013 Collected: 03/15/22 09:53 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
sec-Butylbenzene
ND
mg/kg
0.0073
0.0032
1
03/18/22 14:41
03/18/22 18:24
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0073
0.0026
1
03/18/22 14:41
03/18/22 18:24
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0073
0.0027
1
03/18/22 14:41
03/18/22 18:24
56-23-5
Chlorobenzene
ND
mg/kg
0.0073
0.0014
1
03/18/22 14:41
03/18/22 18:24
108-90-7
Chloroethane
ND
mg/kg
0.015
0.0056
1
03/18/22 14:41
03/18/22 18:24
75-00-3
Chloroform
ND
mg/kg
0.0073
0.0044
1
03/18/22 14:41
03/18/22 18:24
67-66-3
Chloromethane
ND
mg/kg
0.015
0.0061
1
03/18/22 14:41
03/18/22 18:24
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0073
0.0026
1
03/18/22 14:41
03/18/22 18:24
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0073
0.0013
1
03/18/22 14:41
03/18/22 18:24
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0073
0.0028
1
03/18/22 14:41
03/18/22 18:24
96-12-8
Dibromochloromethane
ND
mg/kg
0.0073
0.0041
1
03/18/22 14:41
03/18/22 18:24
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0073
0.0032
1
03/18/22 14:41
03/18/22 18:24
106-93-4
Dibromomethane
ND
mg/kg
0.0073
0.0016
1
03/18/22 14:41
03/18/22 18:24
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0073
0.0026
1
03/18/22 14:41
03/18/22 18:24
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0073
0.0023
1
03/18/22 14:41
03/18/22 18:24
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0073
0.0019
1
03/18/22 14:41
03/18/22 18:24
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.015
0.0032
1
03/18/22 14:41
03/18/22 18:24
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0073
0.0030
1
03/18/22 14:41
03/18/22 18:24
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0073
0.0048
1
03/18/22 14:41
03/18/22 18:24
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0073
0.0030
1
03/18/22 14:41
03/18/22 18:24
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0073
0.0025
1
03/18/22 14:41
03/18/22 18:24
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0073
0.0026
1
03/18/22 14:41
03/18/22 18:24
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0073
0.0022
1
03/18/22 14:41
03/18/22 18:24
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0073
0.0023
1
03/18/22 14:41
03/18/22 18:24
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0073
0.0024
1
03/18/22 14:41
03/18/22 18:24
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0073
0.0035
1
03/18/22 14:41
03/18/22 18:24
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0073
0.0020
1
03/18/22 14:41
03/18/22 18:24
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0073
0.0025
1
03/18/22 14:41
03/18/22 18:24
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0073
0.0020
1
03/18/22 14:41
03/18/22 18:24
108-20-3
Ethylbenzene
ND
mg/kg
0.0073
0.0034
1
03/18/22 14:41
03/18/22 18:24
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.015
0.012
1
03/18/22 14:41
03/18/22 18:24
87-68-3
2-Hexanone
ND
mg/kg
0.073
0.0070
1
03/18/22 14:41
03/18/22 18:24
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0073
0.0025
1
03/18/22 14:41
03/18/22 18:24
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0073
0.0036
1
03/18/22 14:41
03/18/22 18:24
99-87-6
Methylene Chloride
ND
mg/kg
0.029
0.020
1
03/18/22 14:41
03/18/22 18:24
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.073
0.0070
1
03/18/22 14:41
03/18/22 18:24
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0073
0.0027
1
03/18/22 14:41
03/18/22 18:24
1634-04-4
Naphthalene
ND
mg/kg
0.0073
0.0038
1
03/18/22 14:41
03/18/22 18:24
91-20-3
n-Propylbenzene
ND
mg/kg
0.0073
0.0026
1
03/18/22 14:41
03/18/22 18:24
103-65-1
Styrene
ND
mg/kg
0.0073
0.0019
1
03/18/22 14:41
03/18/22 18:24
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0073
0.0028
1
03/18/22 14:41
03/18/22 18:24
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0073
0.0019
1
03/18/22 14:41
03/18/22 18:24
79-34-5
Tetrachloroethene
ND
mg/kg
0.0073
0.0023
1
03/18/22 14:41
03/18/22 18:24
127-18-4
Toluene
ND
mg/kg
0.0073
0.0021
1
03/18/22 14:41
03/18/22 18:24
108-88-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 59 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-7
Lab ID:
92593947013
Collected:
03/15/22
09:53
Received: 03/15/22
16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services
- Charlotte
1,2,3-Trichlorobenzene
ND
mg/kg
0.0073
0.0059
1
03/18/22 14:41
03/18/22 18:24
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0073
0.0061
1
03/18/22 14:41
03/18/22 18:24
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0073
0.0038
1
03/18/22 14:41
03/18/22 18:24
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0073
0.0024
1
03/18/22 14:41
03/18/22 18:24
79-00-5
Trichloroethene
ND
mg/kg
0.0073
0.0019
1
03/18/22 14:41
03/18/22 18:24
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0073
0.0040
1
03/18/22 14:41
03/18/22 18:24
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.0073
0.0037
1
03/18/22 14:41
03/18/22 18:24
96-18-4
1,2,4-Trimethylbenzene
ND
mg/kg
0.0073
0.0020
1
03/18/22 14:41
03/18/22 18:24
95-63-6
1,3,5-Trimethylbenzene
ND
mg/kg
0.0073
0.0025
1
03/18/22 14:41
03/18/22 18:24
108-67-8
Vinyl acetate
ND
mg/kg
0.073
0.0053
1
03/18/22 14:41
03/18/22 18:24
108-05-4
Vinyl chloride
ND
mg/kg
0.015
0.0037
1
03/18/22 14:41
03/18/22 18:24
75-01-4
Xylene (Total)
ND
mg/kg
0.015
0.0042
1
03/18/22 14:41
03/18/22 18:24
1330-20-7
m&p-Xylene
ND
mg/kg
0.015
0.0050
1
03/18/22 14:41
03/18/22 18:24
179601-23-1
o-Xylene
ND
mg/kg
0.0073
0.0032
1
03/18/22 14:41
03/18/22 18:24
95-47-6
Surrogates
Toluene-d8 (S)
98
%
70-130
1
03/18/22 14:41
03/18/22 18:24
2037-26-5
4-Bromofluorobenzene (S)
96
%
69-134
1
03/18/22 14:41
03/18/22 18:24
460-00-4
1,2-Dichloroethane-d4 (S)
86
%
70-130
1
03/18/22 14:41
03/18/22 18:24
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services
- Charlotte
Percent Moisture
9.8
%
0.10
0.10
1
03/17/22 14:46
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 60 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-8 Lab ID: 92593947014 Collected: 03/15/22 10:13 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
mg/kg
0.43
0.15
1
03/18/22 16:02
03/21/22 16:25
83-32-9
Acenaphthylene
ND
mg/kg
0.43
0.15
1
03/18/22 16:02
03/21/22 16:25
208-96-8
Aniline
ND
mg/kg
0.43
0.17
1
03/18/22 16:02
03/21/22 16:25
62-53-3
Anthracene
ND
mg/kg
0.43
0.14
1
03/18/22 16:02
03/21/22 16:25
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.43
0.14
1
03/18/22 16:02
03/21/22 16:25
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.43
0.15
1
03/18/22 16:02
03/21/22 16:25
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.43
0.14
1
03/18/22 16:02
03/21/22 16:25
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.43
0.16
1
03/18/22 16:02
03/21/22 16:25
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.43
0.15
1
03/18/22 16:02
03/21/22 16:25
207-08-9
Benzoic Acid
ND
mg/kg
2.1
0.91
1
03/18/22 16:02
03/21/22 16:25
65-85-0
Benzyl alcohol
ND
mg/kg
0.85
0.32
1
03/18/22 16:02
03/21/22 16:25
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.43
0.16
1
03/18/22 16:02
03/21/22 16:25
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.43
0.18
1
03/18/22 16:02
03/21/22 16:25
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
0.85
0.30
1
03/18/22 16:02
03/21/22 16:25
59-50-7
4-Chloroaniline
ND
mg/kg
0.85
0.33
1
03/18/22 16:02
03/21/22 16:25
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.43
0.18
1
03/18/22 16:02
03/21/22 16:25
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.43
0.16
1
03/18/22 16:02
03/21/22 16:25
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.43
0.17
1
03/18/22 16:02
03/21/22 16:25
91-58-7
2-Chlorophenol
ND
mg/kg
0.43
0.16
1
03/18/22 16:02
03/21/22 16:25
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.43
0.16
1
03/18/22 16:02
03/21/22 16:25
7005-72-3
Chrysene
ND
mg/kg
0.43
0.15
1
03/18/22 16:02
03/21/22 16:25
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.43
0.16
1
03/18/22 16:02
03/21/22 16:25
53-70-3
Dibenzofuran
ND
mg/kg
0.43
0.15
1
03/18/22 16:02
03/21/22 16:25
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.43
0.15
1
03/18/22 16:02
03/21/22 16:25
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.43
0.15
1
03/18/22 16:02
03/21/22 16:25
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.43
0.16
1
03/18/22 16:02
03/21/22 16:25
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
0.85
0.29
1
03/18/22 16:02
03/21/22 16:25
91-94-1
2,4-Dichlorophenol
ND
mg/kg
0.43
0.17
1
03/18/22 16:02
03/21/22 16:25
120-83-2
Diethylphthalate
ND
mg/kg
0.43
0.16
1
03/18/22 16:02
03/21/22 16:25
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.43
0.18
1
03/18/22 16:02
03/21/22 16:25
105-67-9
Dimethylphthalate
ND
mg/kg
0.43
0.15
1
03/18/22 16:02
03/21/22 16:25
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.43
0.14
1
03/18/22 16:02
03/21/22 16:25
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.85
0.40
1
03/18/22 16:02
03/21/22 16:25
534-52-1
2,4-Dinitrophenol
ND
mg/kg
2.1
1.3
1
03/18/22 16:02
03/21/22 16:25
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.43
0.16
1
03/18/22 16:02
03/21/22 16:25
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.43
0.16
1
03/18/22 16:02
03/21/22 16:25
606-20-2
Di-n-octylphthalate
ND
mg/kg
0.43
0.17
1
03/18/22 16:02
03/21/22 16:25
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.43
0.16
1
03/18/22 16:02
03/21/22 16:25
117-81-7
Fluoranthene
ND
mg/kg
0.43
0.15
1
03/18/22 16:02
03/21/22 16:25
206-44-0
Fluorene
ND
mg/kg
0.43
0.15
1
03/18/22 16:02
03/21/22 16:25
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.43
0.18
1
03/18/22 16:02
03/21/22 16:25
87-68-3
Hexachlorobenzene
ND
mg/kg
0.43
0.17
1
03/18/22 16:02
03/21/22 16:25
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.43
0.24
1
03/18/22 16:02
03/21/22 16:25
77-47-4
Hexachloroethane
ND
mg/kg
0.43
0.16
1
03/18/22 16:02
03/21/22 16:25
67-72-1
REPORT OF LABORATORY ANALYSIS
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Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 61 of 122

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: SB-8 Lab ID: 92593947014 Collected: 03/15/22 10:13 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.43
0.17
1
03/18/22 16:02
03/21/22 16:25
193-39-5
Isophorone
ND
mg/kg
0.43
0.19
1
03/18/22 16:02
03/21/22 16:25
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.43
0.15
1
03/18/22 16:02
03/21/22 16:25
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.43
0.17
1
03/18/22 16:02
03/21/22 16:25
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.43
0.17
1
03/18/22 16:02
03/21/22 16:25
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.43
0.17
1
03/18/22 16:02
03/21/22 16:25
15831-10-4
Naphthalene
ND
mg/kg
0.43
0.14
1
03/18/22 16:02
03/21/22 16:25
91-20-3
2-Nitroaniline
ND
mg/kg
2.1
0.35
1
03/18/22 16:02
03/21/22 16:25
88-74-4
3-Nitroaniline
ND
mg/kg
2.1
0.33
1
03/18/22 16:02
03/21/22 16:25
99-09-2
4-Nitroaniline
ND
mg/kg
0.85
0.32
1
03/18/22 16:02
03/21/22 16:25
100-01-6
Nitrobenzene
ND
mg/kg
0.43
0.20
1
03/18/22 16:02
03/21/22 16:25
98-95-3
2-Nitrophenol
ND
mg/kg
0.43
0.18
1
03/18/22 16:02
03/21/22 16:25
88-75-5
4-Nitrophenol
ND
mg/kg
2.1
0.82
1
03/18/22 16:02
03/21/22 16:25
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.43
0.14
1
03/18/22 16:02
03/21/22 16:25
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.43
0.16
1
03/18/22 16:02
03/21/22 16:25
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.43
0.15
1
03/18/22 16:02
03/21/22 16:25
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.43
0.20
1
03/18/22 16:02
03/21/22 16:25
108-60-1
Pentachlorophenol
ND
mg/kg
0.85
0.42
1
03/18/22 16:02
03/21/22 16:25
87-86-5
Phenanthrene
ND
mg/kg
0.43
0.14
1
03/18/22 16:02
03/21/22 16:25
85-01-8
Phenol
ND
mg/kg
0.43
0.19
1
03/18/22 16:02
03/21/22 16:25
108-95-2
Pyrene
ND
mg/kg
0.43
0.17
1
03/18/22 16:02
03/21/22 16:25
129-00-0
Pyridine
ND
mg/kg
0.43
0.13
1
03/18/22 16:02
03/21/22 16:25
110-86-1
1,2,4-Trichlorobenzene
ND
mg/kg
0.43
0.17
1
03/18/22 16:02
03/21/22 16:25
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.43
0.19
1
03/18/22 16:02
03/21/22 16:25
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.43
0.18
1
03/18/22 16:02
03/21/22 16:25
88-06-2
Surrogates
Nitrobenzene-d5 (S)
37
%
21-130
1
03/18/22 16:02
03/21/22 16:25
4165-60-0
2-Fluorobiphenyl (S)
42
%
19-130
1
03/18/22 16:02
03/21/22 16:25
321-60-8
Terphenyl-d14 (S)
50
%
15-130
1
03/18/22 16:02
03/21/22 16:25
1718-51-0
Phenol-d6 (S)
35
%
18-130
1
03/18/22 16:02
03/21/22 16:25
13127-88-3
2-Fluorophenol (S)
31
%
18-130
1
03/18/22 16:02
03/21/22 16:25
367-12-4
2,4,6-Tribromophenol (S)
46
%
18-130
1
03/18/22 16:02
03/21/22 16:25
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation
Method: EPA
5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
mg/kg
0.18
0.057
1
03/18/2214:41
03/18/2218:41
67-64-1
Benzene
ND
mg/kg
0.0089
0.0036
1
03/18/2214:41
03/18/2218:41
71-43-2
Bromobenzene
ND
mg/kg
0.0089
0.0029
1
03/18/2214:41
03/18/2218:41
108-86-1
Bromochloromethane
ND
mg/kg
0.0089
0.0026
1
03/18/2214:41
03/18/2218:41
74-97-5
Bromodichloromethane
ND
mg/kg
0.0089
0.0034
1
03/18/2214:41
03/18/2218:41
75-27-4
Bromoform
ND
mg/kg
0.0089
0.0031
1
03/18/2214:41
03/18/2218:41
75-25-2
Bromomethane
ND
mg/kg
0.018
0.014
1
03/18/2214:41
03/18/2218:41
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.18
0.043
1
03/18/22 14:41
03/18/22 18:41
78-93-3
n-Butylbenzene
ND
mg/kg
0.0089
0.0042
1
03/18/2214:41
03/18/2218:41
104-51-8
REPORT OF LABORATORY ANALYSIS
IL
IL
v2
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Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 62 of 122

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2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-8 Lab ID: 92593947014 Collected: 03/15/22 10:13 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
sec-Butylbenzene
ND
mg/kg
0.0089
0.0039
1
03/18/22 14:41
03/18/22 18:41
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0089
0.0032
1
03/18/22 14:41
03/18/22 18:41
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0089
0.0033
1
03/18/22 14:41
03/18/22 18:41
56-23-5
Chlorobenzene
ND
mg/kg
0.0089
0.0017
1
03/18/22 14:41
03/18/22 18:41
108-90-7
Chloroethane
ND
mg/kg
0.018
0.0069
1
03/18/22 14:41
03/18/22 18:41
75-00-3
Chloroform
ND
mg/kg
0.0089
0.0054
1
03/18/22 14:41
03/18/22 18:41
67-66-3
Chloromethane
ND
mg/kg
0.018
0.0075
1
03/18/22 14:41
03/18/22 18:41
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0089
0.0032
1
03/18/22 14:41
03/18/22 18:41
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0089
0.0016
1
03/18/22 14:41
03/18/22 18:41
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0089
0.0035
1
03/18/22 14:41
03/18/22 18:41
96-12-8
Dibromochloromethane
ND
mg/kg
0.0089
0.0050
1
03/18/22 14:41
03/18/22 18:41
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0089
0.0039
1
03/18/22 14:41
03/18/22 18:41
106-93-4
Dibromomethane
ND
mg/kg
0.0089
0.0019
1
03/18/22 14:41
03/18/22 18:41
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0089
0.0032
1
03/18/22 14:41
03/18/22 18:41
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0089
0.0028
1
03/18/22 14:41
03/18/22 18:41
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0089
0.0023
1
03/18/22 14:41
03/18/22 18:41
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.018
0.0039
1
03/18/22 14:41
03/18/22 18:41
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0089
0.0037
1
03/18/22 14:41
03/18/22 18:41
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0089
0.0059
1
03/18/22 14:41
03/18/22 18:41
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0089
0.0037
1
03/18/22 14:41
03/18/22 18:41
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0089
0.0031
1
03/18/22 14:41
03/18/22 18:41
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0089
0.0031
1
03/18/22 14:41
03/18/22 18:41
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0089
0.0027
1
03/18/22 14:41
03/18/22 18:41
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0089
0.0028
1
03/18/22 14:41
03/18/22 18:41
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0089
0.0029
1
03/18/22 14:41
03/18/22 18:41
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0089
0.0043
1
03/18/22 14:41
03/18/22 18:41
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0089
0.0024
1
03/18/22 14:41
03/18/22 18:41
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0089
0.0031
1
03/18/22 14:41
03/18/22 18:41
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0089
0.0024
1
03/18/22 14:41
03/18/22 18:41
108-20-3
Ethylbenzene
ND
mg/kg
0.0089
0.0042
1
03/18/22 14:41
03/18/22 18:41
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.018
0.015
1
03/18/22 14:41
03/18/22 18:41
87-68-3
2-Hexanone
ND
mg/kg
0.089
0.0086
1
03/18/22 14:41
03/18/22 18:41
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0089
0.0030
1
03/18/22 14:41
03/18/22 18:41
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0089
0.0044
1
03/18/22 14:41
03/18/22 18:41
99-87-6
Methylene Chloride
ND
mg/kg
0.036
0.024
1
03/18/22 14:41
03/18/22 18:41
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.089
0.0086
1
03/18/22 14:41
03/18/22 18:41
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0089
0.0033
1
03/18/22 14:41
03/18/22 18:41
1634-04-4
Naphthalene
0.0068J
mg/kg
0.0089
0.0047
1
03/18/22 14:41
03/18/22 18:41
91-20-3
n-Propylbenzene
0.0098
mg/kg
0.0089
0.0032
1
03/18/22 14:41
03/18/22 18:41
103-65-1
Styrene
ND
mg/kg
0.0089
0.0024
1
03/18/22 14:41
03/18/22 18:41
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0089
0.0034
1
03/18/22 14:41
03/18/22 18:41
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0089
0.0024
1
03/18/22 14:41
03/18/22 18:41
79-34-5
Tetrachloroethene
ND
mg/kg
0.0089
0.0028
1
03/18/22 14:41
03/18/22 18:41
127-18-4
Toluene
0.0060J
mg/kg
0.0089
0.0025
1
03/18/22 14:41
03/18/22 18:41
108-88-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 63 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-8
Lab ID:
92593947014
Collected:
03/15/22
10:13
Received: 03/15/22
16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services
- Charlotte
1,2,3-Trichlorobenzene
ND
mg/kg
0.0089
0.0072
1
03/18/22 14:41
03/18/22 18:41
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0089
0.0075
1
03/18/22 14:41
03/18/22 18:41
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0089
0.0046
1
03/18/22 14:41
03/18/22 18:41
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0089
0.0030
1
03/18/22 14:41
03/18/22 18:41
79-00-5
Trichloroethene
ND
mg/kg
0.0089
0.0023
1
03/18/22 14:41
03/18/22 18:41
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0089
0.0049
1
03/18/22 14:41
03/18/22 18:41
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.0089
0.0045
1
03/18/22 14:41
03/18/22 18:41
96-18-4
1,2,4-Trimethylbenzene
0.0045J
mg/kg
0.0089
0.0024
1
03/18/22 14:41
03/18/22 18:41
95-63-6
1,3,5-Trimethylbenzene
ND
mg/kg
0.0089
0.0030
1
03/18/22 14:41
03/18/22 18:41
108-67-8
Vinyl acetate
ND
mg/kg
0.089
0.0065
1
03/18/22 14:41
03/18/22 18:41
108-05-4
Vinyl chloride
ND
mg/kg
0.018
0.0045
1
03/18/22 14:41
03/18/22 18:41
75-01-4
Xylene (Total)
ND
mg/kg
0.018
0.0051
1
03/18/22 14:41
03/18/22 18:41
1330-20-7
m&p-Xylene
0.011J
mg/kg
0.018
0.0061
1
03/18/22 14:41
03/18/22 18:41
179601-23-1
o-Xylene
ND
mg/kg
0.0089
0.0039
1
03/18/22 14:41
03/18/22 18:41
95-47-6
Surrogates
Toluene-d8 (S)
99
%
70-130
1
03/18/22 14:41
03/18/22 18:41
2037-26-5
4-Bromofluorobenzene (S)
96
%
69-134
1
03/18/22 14:41
03/18/22 18:41
460-00-4
1,2-Dichloroethane-d4 (S)
97
%
70-130
1
03/18/22 14:41
03/18/22 18:41
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services
- Charlotte
Percent Moisture
22.4
%
0.10
0.10
1
03/17/22 14:46
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 64 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-9 Lab ID: 92593947015 Collected: 03/15/22 10:35 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 16:51
83-32-9
Acenaphthylene
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 16:51
208-96-8
Aniline
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 16:51
62-53-3
Anthracene
ND
mg/kg
0.36
0.12
1
03/18/22 16:02
03/21/22 16:51
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.36
0.12
1
03/18/22 16:02
03/21/22 16:51
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.36
0.12
1
03/18/22 16:02
03/21/22 16:51
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.36
0.12
1
03/18/22 16:02
03/21/22 16:51
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 16:51
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 16:51
207-08-9
Benzoic Acid
ND
mg/kg
1.8
0.77
1
03/18/22 16:02
03/21/22 16:51
65-85-0
Benzyl alcohol
ND
mg/kg
0.72
0.27
1
03/18/22 16:02
03/21/22 16:51
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 16:51
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.36
0.15
1
03/18/22 16:02
03/21/22 16:51
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
0.72
0.25
1
03/18/22 16:02
03/21/22 16:51
59-50-7
4-Chloroaniline
ND
mg/kg
0.72
0.28
1
03/18/22 16:02
03/21/22 16:51
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.36
0.15
1
03/18/22 16:02
03/21/22 16:51
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 16:51
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 16:51
91-58-7
2-Chlorophenol
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 16:51
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 16:51
7005-72-3
Chrysene
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 16:51
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 16:51
53-70-3
Dibenzofuran
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 16:51
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 16:51
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 16:51
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 16:51
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
0.72
0.24
1
03/18/22 16:02
03/21/22 16:51
91-94-1
2,4-Dichlorophenol
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 16:51
120-83-2
Diethylphthalate
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 16:51
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.36
0.15
1
03/18/22 16:02
03/21/22 16:51
105-67-9
Dimethylphthalate
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 16:51
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.36
0.12
1
03/18/22 16:02
03/21/22 16:51
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.72
0.33
1
03/18/22 16:02
03/21/22 16:51
534-52-1
2,4-Dinitrophenol
ND
mg/kg
1.8
1.1
1
03/18/22 16:02
03/21/22 16:51
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 16:51
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 16:51
606-20-2
Di-n-octylphthalate
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 16:51
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 16:51
117-81-7
Fluoranthene
ND
mg/kg
0.36
0.12
1
03/18/22 16:02
03/21/22 16:51
206-44-0
Fluorene
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 16:51
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.36
0.16
1
03/18/22 16:02
03/21/22 16:51
87-68-3
Hexachlorobenzene
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 16:51
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.36
0.21
1
03/18/22 16:02
03/21/22 16:51
77-47-4
Hexachloroethane
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 16:51
67-72-1
REPORT OF LABORATORY ANALYSIS
IL
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 65 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: SB-9 Lab ID: 92593947015 Collected: 03/15/22 10:35 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 16:51
193-39-5
Isophorone
ND
mg/kg
0.36
0.16
1
03/18/22 16:02
03/21/22 16:51
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 16:51
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 16:51
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.36
0.15
1
03/18/22 16:02
03/21/22 16:51
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 16:51
15831-10-4
Naphthalene
ND
mg/kg
0.36
0.12
1
03/18/22 16:02
03/21/22 16:51
91-20-3
2-Nitroaniline
ND
mg/kg
1.8
0.29
1
03/18/22 16:02
03/21/22 16:51
88-74-4
3-Nitroaniline
ND
mg/kg
1.8
0.28
1
03/18/22 16:02
03/21/22 16:51
99-09-2
4-Nitroaniline
ND
mg/kg
0.72
0.27
1
03/18/22 16:02
03/21/22 16:51
100-01-6
Nitrobenzene
ND
mg/kg
0.36
0.17
1
03/18/22 16:02
03/21/22 16:51
98-95-3
2-Nitrophenol
ND
mg/kg
0.36
0.16
1
03/18/22 16:02
03/21/22 16:51
88-75-5
4-Nitrophenol
ND
mg/kg
1.8
0.69
1
03/18/22 16:02
03/21/22 16:51
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.36
0.12
1
03/18/22 16:02
03/21/22 16:51
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 16:51
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.36
0.13
1
03/18/22 16:02
03/21/22 16:51
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.36
0.17
1
03/18/22 16:02
03/21/22 16:51
108-60-1
Pentachlorophenol
ND
mg/kg
0.72
0.35
1
03/18/22 16:02
03/21/22 16:51
87-86-5
Phenanthrene
ND
mg/kg
0.36
0.12
1
03/18/22 16:02
03/21/22 16:51
85-01-8
Phenol
ND
mg/kg
0.36
0.16
1
03/18/22 16:02
03/21/22 16:51
108-95-2
Pyrene
ND
mg/kg
0.36
0.15
1
03/18/22 16:02
03/21/22 16:51
129-00-0
Pyridine
ND
mg/kg
0.36
0.11
1
03/18/22 16:02
03/21/22 16:51
110-86-1
1,2,4-Trichlorobenzene
ND
mg/kg
0.36
0.14
1
03/18/22 16:02
03/21/22 16:51
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.36
0.16
1
03/18/22 16:02
03/21/22 16:51
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.36
0.15
1
03/18/22 16:02
03/21/22 16:51
88-06-2
Surrogates
Nitrobenzene-d5 (S)
51
%
21-130
1
03/18/22 16:02
03/21/22 16:51
4165-60-0
2-Fluorobiphenyl (S)
57
%
19-130
1
03/18/22 16:02
03/21/22 16:51
321-60-8
Terphenyl-d14 (S)
72
%
15-130
1
03/18/22 16:02
03/21/22 16:51
1718-51-0
Phenol-d6 (S)
60
%
18-130
1
03/18/22 16:02
03/21/22 16:51
13127-88-3
2-Fluorophenol (S)
58
%
18-130
1
03/18/22 16:02
03/21/22 16:51
367-12-4
2,4,6-Tribromophenol (S)
66
%
18-130
1
03/18/22 16:02
03/21/22 16:51
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation
Method: EPA
5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
0.074J
mg/kg
0.19
0.061
1
03/18/2214:41
03/18/2218:59
67-64-1
Benzene
ND
mg/kg
0.0095
0.0038
1
03/18/2214:41
03/18/2218:59
71-43-2
Bromobenzene
ND
mg/kg
0.0095
0.0031
1
03/18/2214:41
03/18/2218:59
108-86-1
Bromochloromethane
ND
mg/kg
0.0095
0.0028
1
03/18/2214:41
03/18/2218:59
74-97-5
Bromodichloromethane
ND
mg/kg
0.0095
0.0037
1
03/18/2214:41
03/18/2218:59
75-27-4
Bromoform
ND
mg/kg
0.0095
0.0034
1
03/18/2214:41
03/18/2218:59
75-25-2
Bromomethane
ND
mg/kg
0.019
0.015
1
03/18/2214:41
03/18/2218:59
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.19
0.046
1
03/18/22 14:41
03/18/22 18:59
78-93-3
n-Butylbenzene
ND
mg/kg
0.0095
0.0045
1
03/18/2214:41
03/18/2218:59
104-51-8
REPORT OF LABORATORY ANALYSIS
IL
IL
C7,v2
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 66 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-9 Lab ID: 92593947015 Collected: 03/15/22 10:35 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
sec-Butylbenzene
0.0063J
mg/kg
0.0095
0.0042
1
03/18/22 14:41
03/18/22 18:59
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0095
0.0034
1
03/18/22 14:41
03/18/22 18:59
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0095
0.0036
1
03/18/22 14:41
03/18/22 18:59
56-23-5
Chlorobenzene
ND
mg/kg
0.0095
0.0018
1
03/18/22 14:41
03/18/22 18:59
108-90-7
Chloroethane
ND
mg/kg
0.019
0.0074
1
03/18/22 14:41
03/18/22 18:59
75-00-3
Chloroform
ND
mg/kg
0.0095
0.0058
1
03/18/22 14:41
03/18/22 18:59
67-66-3
Chloromethane
ND
mg/kg
0.019
0.0080
1
03/18/22 14:41
03/18/22 18:59
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0095
0.0034
1
03/18/22 14:41
03/18/22 18:59
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0095
0.0017
1
03/18/22 14:41
03/18/22 18:59
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0095
0.0037
1
03/18/22 14:41
03/18/22 18:59
96-12-8
Dibromochloromethane
ND
mg/kg
0.0095
0.0054
1
03/18/22 14:41
03/18/22 18:59
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0095
0.0042
1
03/18/22 14:41
03/18/22 18:59
106-93-4
Dibromomethane
ND
mg/kg
0.0095
0.0020
1
03/18/22 14:41
03/18/22 18:59
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0095
0.0034
1
03/18/22 14:41
03/18/22 18:59
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0095
0.0030
1
03/18/22 14:41
03/18/22 18:59
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0095
0.0025
1
03/18/22 14:41
03/18/22 18:59
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.019
0.0041
1
03/18/22 14:41
03/18/22 18:59
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0095
0.0039
1
03/18/22 14:41
03/18/22 18:59
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0095
0.0063
1
03/18/22 14:41
03/18/22 18:59
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0095
0.0039
1
03/18/22 14:41
03/18/22 18:59
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0095
0.0033
1
03/18/22 14:41
03/18/22 18:59
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0095
0.0033
1
03/18/22 14:41
03/18/22 18:59
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0095
0.0029
1
03/18/22 14:41
03/18/22 18:59
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0095
0.0030
1
03/18/22 14:41
03/18/22 18:59
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0095
0.0031
1
03/18/22 14:41
03/18/22 18:59
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0095
0.0046
1
03/18/22 14:41
03/18/22 18:59
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0095
0.0026
1
03/18/22 14:41
03/18/22 18:59
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0095
0.0033
1
03/18/22 14:41
03/18/22 18:59
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0095
0.0026
1
03/18/22 14:41
03/18/22 18:59
108-20-3
Ethylbenzene
0.0053J
mg/kg
0.0095
0.0044
1
03/18/22 14:41
03/18/22 18:59
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.019
0.016
1
03/18/22 14:41
03/18/22 18:59
87-68-3
2-Hexanone
ND
mg/kg
0.095
0.0092
1
03/18/22 14:41
03/18/22 18:59
591-78-6
Isopropylbenzene (Cumene)
0.0036J
mg/kg
0.0095
0.0032
1
03/18/22 14:41
03/18/22 18:59
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0095
0.0047
1
03/18/22 14:41
03/18/22 18:59
99-87-6
Methylene Chloride
ND
mg/kg
0.038
0.026
1
03/18/22 14:41
03/18/22 18:59
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.095
0.0092
1
03/18/22 14:41
03/18/22 18:59
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0095
0.0036
1
03/18/22 14:41
03/18/22 18:59
1634-04-4
Naphthalene
ND
mg/kg
0.0095
0.0050
1
03/18/22 14:41
03/18/22 18:59
91-20-3
n-Propylbenzene
0.011
mg/kg
0.0095
0.0034
1
03/18/22 14:41
03/18/22 18:59
103-65-1
Styrene
ND
mg/kg
0.0095
0.0025
1
03/18/22 14:41
03/18/22 18:59
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0095
0.0037
1
03/18/22 14:41
03/18/22 18:59
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0095
0.0025
1
03/18/22 14:41
03/18/22 18:59
79-34-5
Tetrachloroethene
ND
mg/kg
0.0095
0.0030
1
03/18/22 14:41
03/18/22 18:59
127-18-4
Toluene
0.016
mg/kg
0.0095
0.0027
1
03/18/22 14:41
03/18/22 18:59
108-88-3
REPORT OF LABORATORY ANALYSIS
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Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 67 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: S13-9
Lab ID:
92593947015
Collected:
03/15/22
10:35
Received: 03/15/22
16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services
- Charlotte
1,2,3-Trichlorobenzene
ND
mg/kg
0.0095
0.0077
1
03/18/22 14:41
03/18/22 18:59
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0095
0.0080
1
03/18/22 14:41
03/18/22 18:59
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0095
0.0050
1
03/18/22 14:41
03/18/22 18:59
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0095
0.0032
1
03/18/22 14:41
03/18/22 18:59
79-00-5
Trichloroethene
ND
mg/kg
0.0095
0.0025
1
03/18/22 14:41
03/18/22 18:59
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0095
0.0053
1
03/18/22 14:41
03/18/22 18:59
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.0095
0.0048
1
03/18/22 14:41
03/18/22 18:59
96-18-4
1,2,4-Trimethylbenzene
ND
mg/kg
0.0095
0.0026
1
03/18/22 14:41
03/18/22 18:59
95-63-6
1,3,5-Trimethylbenzene
ND
mg/kg
0.0095
0.0032
1
03/18/22 14:41
03/18/22 18:59
108-67-8
Vinyl acetate
ND
mg/kg
0.095
0.0070
1
03/18/22 14:41
03/18/22 18:59
108-05-4
Vinyl chloride
ND
mg/kg
0.019
0.0049
1
03/18/22 14:41
03/18/22 18:59
75-01-4
Xylene (Total)
ND
mg/kg
0.019
0.0054
1
03/18/22 14:41
03/18/22 18:59
1330-20-7
m&p-Xylene
0.011J
mg/kg
0.019
0.0065
1
03/18/22 14:41
03/18/22 18:59
179601-23-1
o-Xylene
ND
mg/kg
0.0095
0.0042
1
03/18/22 14:41
03/18/22 18:59
95-47-6
Surrogates
Toluene-d8 (S)
98
%
70-130
1
03/18/22 14:41
03/18/22 18:59
2037-26-5
4-Bromofluorobenzene (S)
97
%
69-134
1
03/18/22 14:41
03/18/22 18:59
460-00-4
1,2-Dichloroethane-d4 (S)
94
%
70-130
1
03/18/22 14:41
03/18/22 18:59
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services
- Charlotte
Percent Moisture
9.6
%
0.10
0.10
1
03/17/22 14:46
N2
REPORT OF LABORATORY ANALYSIS
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Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 68 of 122

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: SB-10 Lab ID: 92593947016 Collected: 03/15/22 10:50 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 17:18
83-32-9
Acenaphthylene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 17:18
208-96-8
Aniline
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 17:18
62-53-3
Anthracene
ND
mg/kg
0.40
0.13
1
03/18/22 16:02
03/21/22 17:18
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.40
0.13
1
03/18/22 16:02
03/21/22 17:18
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 17:18
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.40
0.13
1
03/18/22 16:02
03/21/22 17:18
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 17:18
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 17:18
207-08-9
Benzoic Acid
ND
mg/kg
2.0
0.86
1
03/18/22 16:02
03/21/22 17:18
65-85-0
Benzyl alcohol
ND
mg/kg
0.80
0.30
1
03/18/22 16:02
03/21/22 17:18
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 17:18
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.40
0.17
1
03/18/22 16:02
03/21/22 17:18
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
0.80
0.28
1
03/18/22 16:02
03/21/22 17:18
59-50-7
4-Chloroaniline
ND
mg/kg
0.80
0.32
1
03/18/22 16:02
03/21/22 17:18
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.40
0.17
1
03/18/22 16:02
03/21/22 17:18
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 17:18
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 17:18
91-58-7
2-Chlorophenol
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 17:18
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 17:18
7005-72-3
Chrysene
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 17:18
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 17:18
53-70-3
Dibenzofuran
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 17:18
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 17:18
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 17:18
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 17:18
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
0.80
0.27
1
03/18/22 16:02
03/21/22 17:18
91-94-1
2,4-Dichlorophenol
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 17:18
120-83-2
Diethylphthalate
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 17:18
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.40
0.17
1
03/18/22 16:02
03/21/22 17:18
105-67-9
Dimethylphthalate
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 17:18
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 17:18
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.80
0.38
1
03/18/22 16:02
03/21/22 17:18
534-52-1
2,4-Dinitrophenol
ND
mg/kg
2.0
1.2
1
03/18/22 16:02
03/21/22 17:18
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 17:18
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 17:18
606-20-2
Di-n-octylphthalate
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 17:18
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 17:18
117-81-7
Fluoranthene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 17:18
206-44-0
Fluorene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 17:18
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.40
0.17
1
03/18/22 16:02
03/21/22 17:18
87-68-3
Hexachlorobenzene
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 17:18
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.40
0.23
1
03/18/22 16:02
03/21/22 17:18
77-47-4
Hexachloroethane
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 17:18
67-72-1
REPORT OF LABORATORY ANALYSIS
IL
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 69 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: SB-10 Lab ID: 92593947016 Collected: 03/15/22 10:50 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 17:18
193-39-5
Isophorone
ND
mg/kg
0.40
0.18
1
03/18/22 16:02
03/21/22 17:18
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 17:18
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 17:18
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 17:18
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 17:18
15831-10-4
Naphthalene
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 17:18
91-20-3
2-Nitroaniline
ND
mg/kg
2.0
0.33
1
03/18/22 16:02
03/21/22 17:18
88-74-4
3-Nitroaniline
ND
mg/kg
2.0
0.32
1
03/18/22 16:02
03/21/22 17:18
99-09-2
4-Nitroaniline
ND
mg/kg
0.80
0.31
1
03/18/22 16:02
03/21/22 17:18
100-01-6
Nitrobenzene
ND
mg/kg
0.40
0.19
1
03/18/22 16:02
03/21/22 17:18
98-95-3
2-Nitrophenol
ND
mg/kg
0.40
0.17
1
03/18/22 16:02
03/21/22 17:18
88-75-5
4-Nitrophenol
ND
mg/kg
2.0
0.78
1
03/18/22 16:02
03/21/22 17:18
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 17:18
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.40
0.15
1
03/18/22 16:02
03/21/22 17:18
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.40
0.14
1
03/18/22 16:02
03/21/22 17:18
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.40
0.19
1
03/18/22 16:02
03/21/22 17:18
108-60-1
Pentachlorophenol
ND
mg/kg
0.80
0.39
1
03/18/22 16:02
03/21/22 17:18
87-86-5
Phenanthrene
ND
mg/kg
0.40
0.13
1
03/18/22 16:02
03/21/22 17:18
85-01-8
Phenol
ND
mg/kg
0.40
0.18
1
03/18/22 16:02
03/21/22 17:18
108-95-2
Pyrene
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 17:18
129-00-0
Pyridine
ND
mg/kg
0.40
0.13
1
03/18/22 16:02
03/21/22 17:18
110-86-1
1,2,4-Trichlorobenzene
ND
mg/kg
0.40
0.16
1
03/18/22 16:02
03/21/22 17:18
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.40
0.18
1
03/18/22 16:02
03/21/22 17:18
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.40
0.17
1
03/18/22 16:02
03/21/22 17:18
88-06-2
Surrogates
Nitrobenzene-d5 (S)
57
%
21-130
1
03/18/22 16:02
03/21/22 17:18
4165-60-0
2-Fluorobiphenyl (S)
61
%
19-130
1
03/18/22 16:02
03/21/22 17:18
321-60-8
Terphenyl-d14 (S)
71
%
15-130
1
03/18/22 16:02
03/21/22 17:18
1718-51-0
Phenol-d6 (S)
55
%
18-130
1
03/18/22 16:02
03/21/22 17:18
13127-88-3
2-Fluorophenol (S)
50
%
18-130
1
03/18/22 16:02
03/21/22 17:18
367-12-4
2,4,6-Tribromophenol (S)
53
%
18-130
1
03/18/22 16:02
03/21/22 17:18
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation
Method: EPA
5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
mg/kg
0.17
0.054
1
03/18/2214:41
03/18/2219:17
67-64-1
Benzene
ND
mg/kg
0.0084
0.0033
1
03/18/2214:41
03/18/2219:17
71-43-2
Bromobenzene
ND
mg/kg
0.0084
0.0027
1
03/18/2214:41
03/18/2219:17
108-86-1
Bromochloromethane
ND
mg/kg
0.0084
0.0025
1
03/18/2214:41
03/18/2219:17
74-97-5
Bromodichloromethane
ND
mg/kg
0.0084
0.0032
1
03/18/2214:41
03/18/2219:17
75-27-4
Bromoform
ND
mg/kg
0.0084
0.0029
1
03/18/2214:41
03/18/2219:17
75-25-2
Bromomethane
ND
mg/kg
0.017
0.013
1
03/18/2214:41
03/18/2219:17
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.17
0.040
1
03/18/22 14:41
03/18/22 19:17
78-93-3
n-Butylbenzene
ND
mg/kg
0.0084
0.0040
1
03/18/2214:41
03/18/2219:17
104-51-8
REPORT OF LABORATORY ANALYSIS
IL
IL
v2
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 70 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: SB-10 Lab ID: 92593947016 Collected: 03/15/22 10:50 Received: 03/15/22 16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
sec-Butylbenzene
ND
mg/kg
0.0084
0.0037
1
03/18/22 14:41
03/18/22 19:17
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0084
0.0030
1
03/18/22 14:41
03/18/22 19:17
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0084
0.0031
1
03/18/22 14:41
03/18/22 19:17
56-23-5
Chlorobenzene
ND
mg/kg
0.0084
0.0016
1
03/18/22 14:41
03/18/22 19:17
108-90-7
Chloroethane
ND
mg/kg
0.017
0.0065
1
03/18/22 14:41
03/18/22 19:17
75-00-3
Chloroform
ND
mg/kg
0.0084
0.0051
1
03/18/22 14:41
03/18/22 19:17
67-66-3
Chloromethane
ND
mg/kg
0.017
0.0070
1
03/18/22 14:41
03/18/22 19:17
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0084
0.0030
1
03/18/22 14:41
03/18/22 19:17
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0084
0.0015
1
03/18/22 14:41
03/18/22 19:17
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0084
0.0032
1
03/18/22 14:41
03/18/22 19:17
96-12-8
Dibromochloromethane
ND
mg/kg
0.0084
0.0047
1
03/18/22 14:41
03/18/22 19:17
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0084
0.0037
1
03/18/22 14:41
03/18/22 19:17
106-93-4
Dibromomethane
ND
mg/kg
0.0084
0.0018
1
03/18/22 14:41
03/18/22 19:17
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0084
0.0030
1
03/18/22 14:41
03/18/22 19:17
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0084
0.0026
1
03/18/22 14:41
03/18/22 19:17
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0084
0.0022
1
03/18/22 14:41
03/18/22 19:17
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.017
0.0036
1
03/18/22 14:41
03/18/22 19:17
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0084
0.0034
1
03/18/22 14:41
03/18/22 19:17
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0084
0.0055
1
03/18/22 14:41
03/18/22 19:17
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0084
0.0034
1
03/18/22 14:41
03/18/22 19:17
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0084
0.0029
1
03/18/22 14:41
03/18/22 19:17
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0084
0.0029
1
03/18/22 14:41
03/18/22 19:17
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0084
0.0025
1
03/18/22 14:41
03/18/22 19:17
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0084
0.0026
1
03/18/22 14:41
03/18/22 19:17
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0084
0.0027
1
03/18/22 14:41
03/18/22 19:17
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0084
0.0040
1
03/18/22 14:41
03/18/22 19:17
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0084
0.0023
1
03/18/22 14:41
03/18/22 19:17
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0084
0.0029
1
03/18/22 14:41
03/18/22 19:17
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0084
0.0023
1
03/18/22 14:41
03/18/22 19:17
108-20-3
Ethylbenzene
0.0051J
mg/kg
0.0084
0.0039
1
03/18/22 14:41
03/18/22 19:17
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.017
0.014
1
03/18/22 14:41
03/18/22 19:17
87-68-3
2-Hexanone
ND
mg/kg
0.084
0.0081
1
03/18/22 14:41
03/18/22 19:17
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0084
0.0028
1
03/18/22 14:41
03/18/22 19:17
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0084
0.0041
1
03/18/22 14:41
03/18/22 19:17
99-87-6
Methylene Chloride
ND
mg/kg
0.033
0.023
1
03/18/22 14:41
03/18/22 19:17
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.084
0.0081
1
03/18/22 14:41
03/18/22 19:17
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0084
0.0031
1
03/18/22 14:41
03/18/22 19:17
1634-04-4
Naphthalene
0.016
mg/kg
0.0084
0.0044
1
03/18/22 14:41
03/18/22 19:17
91-20-3
n-Propylbenzene
ND
mg/kg
0.0084
0.0030
1
03/18/22 14:41
03/18/22 19:17
103-65-1
Styrene
ND
mg/kg
0.0084
0.0022
1
03/18/22 14:41
03/18/22 19:17
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0084
0.0032
1
03/18/22 14:41
03/18/22 19:17
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0084
0.0022
1
03/18/22 14:41
03/18/22 19:17
79-34-5
Tetrachloroethene
ND
mg/kg
0.0084
0.0026
1
03/18/22 14:41
03/18/22 19:17
127-18-4
Toluene
0.0073J
mg/kg
0.0084
0.0024
1
03/18/22 14:41
03/18/22 19:17
108-88-3
REPORT OF LABORATORY ANALYSIS
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Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 71 of 122

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ANALYTICAL RESULTS
Project: 49:13699-D
Pace Project No.: 92593947
Sample: SB-10
Lab ID:
92593947016
Collected:
03/15/22
10:50
Received: 03/15/22
16:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services
- Charlotte
1,2,3-Trichlorobenzene
ND
mg/kg
0.0084
0.0068
1
03/18/22 14:41
03/18/22 19:17
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0084
0.0070
1
03/18/22 14:41
03/18/22 19:17
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0084
0.0044
1
03/18/22 14:41
03/18/22 19:17
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0084
0.0028
1
03/18/22 14:41
03/18/22 19:17
79-00-5
Trichloroethene
ND
mg/kg
0.0084
0.0022
1
03/18/22 14:41
03/18/22 19:17
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0084
0.0046
1
03/18/22 14:41
03/18/22 19:17
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.0084
0.0042
1
03/18/22 14:41
03/18/22 19:17
96-18-4
1,2,4-Trimethylbenzene
0.0099
mg/kg
0.0084
0.0023
1
03/18/22 14:41
03/18/22 19:17
95-63-6
1,3,5-Trimethylbenzene
ND
mg/kg
0.0084
0.0028
1
03/18/22 14:41
03/18/22 19:17
108-67-8
Vinyl acetate
ND
mg/kg
0.084
0.0061
1
03/18/22 14:41
03/18/22 19:17
108-05-4
Vinyl chloride
ND
mg/kg
0.017
0.0043
1
03/18/22 14:41
03/18/22 19:17
75-01-4
Xylene (Total)
0.012J
mg/kg
0.017
0.0048
1
03/18/22 14:41
03/18/22 19:17
1330-20-7
m&p-Xylene
0.016J
mg/kg
0.017
0.0057
1
03/18/22 14:41
03/18/22 19:17
179601-23-1
o-Xylene
0.012
mg/kg
0.0084
0.0037
1
03/18/22 14:41
03/18/22 19:17
95-47-6
Surrogates
Toluene-d8 (S)
98
%
70-130
1
03/18/22 14:41
03/18/22 19:17
2037-26-5
4-Bromofluorobenzene (S)
97
%
69-134
1
03/18/22 14:41
03/18/22 19:17
460-00-4
1,2-Dichloroethane-d4 (S)
97
%
70-130
1
03/18/22 14:41
03/18/22 19:17
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services
- Charlotte
Percent Moisture
17.4
%
0.10
0.10
1
03/17/22 14:47
N2
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
QC Batch: 685823 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92593947008,92593947009,92593947010,92593947011,92593947012,92593947013,92593947014,
92593947015,92593947016
METHOD BLANK: 3586303
Matrix: Solid
Associated Lab Samples: 92593947008,92593947009,92593947010,92593947011,92593947012,92593947013,92593947014,
92593947015,92593947016
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
ND
0.0050
0.0019
03/18/22 16:37
1,1,1-Trichloroethane
mg/kg
ND
0.0050
0.0026
03/18/22 16:37
1,1,2,2-Tetrachloroethane
mg/kg
ND
0.0050
0.0013
03/18/22 16:37
1,1,2-Trichloroethane
mg/kg
ND
0.0050
0.0017
03/18/22 16:37
1,1-Dichloroethane
mg/kg
ND
0.0050
0.0021
03/18/22 16:37
1,1-Dichloroethene
mg/kg
ND
0.0050
0.0021
03/18/22 16:37
1,1-Dichloropropene
mg/kg
ND
0.0050
0.0024
03/18/22 16:37
1,2,3-Trichlorobenzene
mg/kg
ND
0.0050
0.0040
03/18/22 16:37
1,2,3-Trichloropropane
mg/kg
ND
0.0050
0.0025
03/18/22 16:37
1,2,4-Trichlorobenzene
mg/kg
ND
0.0050
0.0042
03/18/22 16:37
1,2,4-Trimethylbenzene
mg/kg
ND
0.0050
0.0014
03/18/22 16:37
1,2-Dibromo-3-chloropropane
mg/kg
ND
0.0050
0.0019
03/18/22 16:37
1,2-Dibromoethane (EDB)
mg/kg
ND
0.0050
0.0022
03/18/22 16:37
1,2-Dichlorobenzene
mg/kg
ND
0.0050
0.0018
03/18/22 16:37
1,2-Dichloroethane
mg/kg
ND
0.0050
0.0033
03/18/22 16:37
1,2-Dichloropropane
mg/kg
ND
0.0050
0.0015
03/18/22 16:37
1,3,5-Trimethylbenzene
mg/kg
ND
0.0050
0.0017
03/18/22 16:37
1,3-Dichlorobenzene
mg/kg
ND
0.0050
0.0016
03/18/22 16:37
1,3-Dichloropropane
mg/kg
ND
0.0050
0.0016
03/18/22 16:37
1,4-Dichlorobenzene
mg/kg
ND
0.0050
0.0013
03/18/22 16:37
2,2-Dichloropropane
mg/kg
ND
0.0050
0.0016
03/18/22 16:37
2-Butanone (MEK)
mg/kg
ND
0.10
0.024
03/18/22 16:37
2-Chlorotoluene
mg/kg
ND
0.0050
0.0018
03/18/22 16:37
2-Hexanone
mg/kg
ND
0.050
0.0048
03/18/22 16:37
4-Chlorotoluene
mg/kg
ND
0.0050
0.00088
03/18/22 16:37
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
0.050
0.0048
03/18/22 16:37
Acetone
mg/kg
ND
0.10
0.032
03/18/22 16:37 v2
Benzene
mg/kg
ND
0.0050
0.0020
03/18/22 16:37
Bromobenzene
mg/kg
ND
0.0050
0.0016
03/18/22 16:37
Bromochloromethane
mg/kg
ND
0.0050
0.0015
03/18/22 16:37
Bromodichloromethane
mg/kg
ND
0.0050
0.0019
03/18/22 16:37
Bromoform
mg/kg
ND
0.0050
0.0018
03/18/22 16:37
Bromomethane
mg/kg
ND
0.010
0.0079
03/18/22 16:37
Carbon tetrachloride
mg/kg
ND
0.0050
0.0019
03/18/22 16:37
Chlorobenzene
mg/kg
ND
0.0050
0.00096
03/18/22 16:37
Chloroethane
mg/kg
ND
0.010
0.0039
03/18/22 16:37
Chloroform
mg/kg
ND
0.0050
0.0030
03/18/22 16:37
Chloromethane
mg/kg
ND
0.010
0.0042
03/18/22 16:37
cis-1,2-Dichloroethene
mg/kg
ND
0.0050
0.0017
03/18/22 16:37
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 73 of 122

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2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
METHOD BLANK: 3586303 Matrix: Solid
Associated Lab Samples: 92593947008, 92593947009, 92593947010, 92593947011, 92593947012, 92593947013, 92593947014,
92593947015,92593947016
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
cis-1,3-Dichloropropene
mg/kg
ND
0.0050
0.0014
03/18/22 16:37
Dibromochloromethane
mg/kg
ND
0.0050
0.0028
03/18/22 16:37
Dibromomethane
mg/kg
ND
0.0050
0.0011
03/18/22 16:37
Dichlorodifluoromethane
mg/kg
ND
0.010
0.0022
03/18/22 16:37
Diisopropyl ether
mg/kg
ND
0.0050
0.0014
03/18/22 16:37
Ethylbenzene
mg/kg
ND
0.0050
0.0023
03/18/22 16:37
Hexachloro-1,3-butadiene
mg/kg
ND
0.010
0.0082
03/18/22 16:37
Isopropylbenzene (Cumene)
mg/kg
ND
0.0050
0.0017
03/18/22 16:37
m&p-Xylene
mg/kg
ND
0.010
0.0034
03/18/22 16:37
Methyl-tert-butyl ether
mg/kg
ND
0.0050
0.0019
03/18/22 16:37
Methylene Chloride
mg/kg
ND
0.020
0.014
03/18/22 16:37
n-Butylbenzene
mg/kg
ND
0.0050
0.0024
03/18/22 16:37
n-Propylbenzene
mg/kg
ND
0.0050
0.0018
03/18/22 16:37
Naphthalene
mg/kg
ND
0.0050
0.0026
03/18/22 16:37
o-Xylene
mg/kg
ND
0.0050
0.0022
03/18/22 16:37
p-Isopropyltoluene
mg/kg
ND
0.0050
0.0025
03/18/22 16:37
sec-Butylbenzene
mg/kg
ND
0.0050
0.0022
03/18/22 16:37
Styrene
mg/kg
ND
0.0050
0.0013
03/18/22 16:37
tert-Butyl benzene
mg/kg
ND
0.0050
0.0018
03/18/22 16:37
Tetrachloroethene
mg/kg
ND
0.0050
0.0016
03/18/22 16:37
Toluene
mg/kg
ND
0.0050
0.0014
03/18/22 16:37
trans-1,2-Dichloroethene
mg/kg
ND
0.0050
0.0018
03/18/22 16:37
trans- 1,3-Dichloropropene
mg/kg
ND
0.0050
0.0017
03/18/22 16:37
Trichloroethene
mg/kg
ND
0.0050
0.0013
03/18/22 16:37
Trichlorofluoromethane
mg/kg
ND
0.0050
0.0028
03/18/22 16:37
Vinyl acetate
mg/kg
ND
0.050
0.0036
03/18/22 16:37
Vinyl chloride
mg/kg
ND
0.010
0.0025
03/18/22 16:37
Xylene (Total)
mg/kg
ND
0.010
0.0028
03/18/22 16:37
1,2-Dichloroethane-d4 (S)
%
97
70-130
03/18/22 16:37
4-Bromofluorobenzene (S)
%
97
69-134
03/18/22 16:37
Toluene-d8 (S)
%
98
70-130
03/18/22 16:37
LABORATORY CONTROL SAMPLE:
3586304
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
1.2
1.2
99
70-130
1,1,1-Trichloroethane
mg/kg
1.2
1.1
90
70-130
1,1,2,2-Tetrachloroethane
mg/kg
1.2
1.2
98
70-130
1,1,2-Trichloroethane
mg/kg
1.2
1.2
93
70-130
1,1-Dichloroethane
mg/kg
1.2
1.2
93
70-130
1,1-Dichloroethene
mg/kg
1.2
1.2
92
70-130
1,1-Dichloropropene
mg/kg
1.2
1.2
95
70-130
1,2,3-Trichlorobenzene
mg/kg
1.2
1.3
106
65-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 74 of 122

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QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
LABORATORY CONTROL SAMPLE:
Parameter
3586304
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,3-Trichloropropane
mg/kg
1.2
1.2
96
70-130
1,2,4-Trichlorobenzene
mg/kg
1.2
1.3
104
68-130
1,2,4-Trimethylbenzene
mg/kg
1.2
1.3
102
70-130
1,2-Dibromo-3-chloropropane
mg/kg
1.2
1.2
94
70-130
1,2-Dibromoethane (EDB)
mg/kg
1.2
1.2
97
70-130
1,2-Dichlorobenzene
mg/kg
1.2
1.3
100
70-130
1,2-Dichloroethane
mg/kg
1.2
1.1
86
63-130
1,2-Dichloropropane
mg/kg
1.2
1.2
97
70-130
1,3,5-Trimethylbenzene
mg/kg
1.2
1.3
102
70-130
1,3-Dichlorobenzene
mg/kg
1.2
1.2
99
70-130
1,3-Dichloropropane
mg/kg
1.2
1.2
97
70-130
1,4-Dichlorobenzene
mg/kg
1.2
1.2
99
70-130
2,2-Dichloropropane
mg/kg
1.2
1.2
93
66-130
2-Butanone (MEK)
mg/kg
2.5
2.1
85
70-130
2-Chlorotoluene
mg/kg
1.2
1.3
104
70-130
2-Hexanone
mg/kg
2.5
2.3
93
70-130
4-Chlorotoluene
mg/kg
1.2
1.2
99
70-130
4-Methyl-2-pentanone (MIBK)
mg/kg
2.5
2.3
91
70-130
Acetone
mg/kg
2.5
2.0
79
69-130 v3
Benzene
mg/kg
1.2
1.1
92
70-130
Bromobenzene
mg/kg
1.2
1.3
101
70-130
Bromochloromethane
mg/kg
1.2
1.2
92
70-130
Bromodichloromethane
mg/kg
1.2
1.2
95
69-130
Bromoform
mg/kg
1.2
1.3
102
70-130
Bromomethane
mg/kg
1.2
1.3
103
52-130
Carbon tetrachloride
mg/kg
1.2
1.2
95
70-130
Chlorobenzene
mg/kg
1.2
1.2
98
70-130
Chloroethane
mg/kg
1.2
1.3
106
65-130
Chloroform
mg/kg
1.2
1.1
92
70-130
Chloromethane
mg/kg
1.2
1.1
91
55-130
cis-1,2-Dichloroethene
mg/kg
1.2
1.2
93
70-130
cis-1,3-Dichloropropene
mg/kg
1.2
1.2
93
70-130
Dibromochloromethane
mg/kg
1.2
1.2
92
70-130
Dibromomethane
mg/kg
1.2
1.2
93
70-130
Dichlorodifluoromethane
mg/kg
1.2
1.2
99
45-156
Diisopropyl ether
mg/kg
1.2
1.1
86
70-130
Ethylbenzene
mg/kg
1.2
1.2
95
70-130
Hexachloro-1,3-butadiene
mg/kg
1.2
1.3
102
66-130
Isopropylbenzene (Cumene)
mg/kg
1.2
1.3
104
70-130
m&p-Xylene
mg/kg
2.5
2.5
99
70-130
Methyl-tert-butyl ether
mg/kg
1.2
1.1
87
70-130
Methylene Chloride
mg/kg
1.2
1.0
83
65-130
n-Butylbenzene
mg/kg
1.2
1.3
103
67-130
n-Propylbenzene
mg/kg
1.2
1.3
101
70-130
Naphthalene
mg/kg
1.2
1.3
102
70-130
o-Xylene
mg/kg
1.2
1.3
101
70-130
p-Isopropyltoluene
mg/kg
1.2
1.3
103
67-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 75 of 122

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
LABORATORY CONTROL SAMPLE:
3586304
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
sec-Butylbenzene
mg/kg
1.2
1.3
100
69-130
Styrene
mg/kg
1.2
1.3
104
70-130
tert-Butyl benzene
mg/kg
1.2
1.3
101
67-130
Tetrachloroethene
mg/kg
1.2
1.2
96
70-130
Toluene
mg/kg
1.2
1.2
93
70-130
trans-1,2-Dichloroethene
mg/kg
1.2
1.2
95
70-130
trans- 1,3-Dichloropropene
mg/kg
1.2
1.2
95
68-130
Trichloroethene
mg/kg
1.2
1.2
94
70-130
Trichlorofluoromethane
mg/kg
1.2
1.1
90
70-130
Vinyl acetate
mg/kg
2.5
2.2
89
70-130
Vinyl chloride
mg/kg
1.2
1.2
99
61-130
Xylene (Total)
mg/kg
3.8
3.7
100
70-130
1,2-Dichloroethane-d4 (S)
%
89
70-130
4-Bromofluorobenzene (S)
%
99
69-134
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE SAMPLE:
3586305
92593947008
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
ND
0.72
0.45
62
70-131 M1
1,1,1-Trichloroethane
mg/kg
ND
0.72
0.38
53
65-133 M1
1,1,2,2-Tetrachloroethane
mg/kg
ND
0.72
0.45
62
66-130 M1
1,1,2-Trichloroethane
mg/kg
ND
0.72
0.42
59
66-133 M1
1,1-Dichloroethane
mg/kg
ND
0.72
0.41
57
65-130 M1
1,1-Dichloroethene
mg/kg
ND
0.72
0.38
53
10-158
1,1-Dichloropropene
mg/kg
ND
0.72
0.38
53
68-133 M1
1,2,3-Trichlorobenzene
mg/kg
ND
0.72
0.46
64
27-138
1,2,3-Trichloropropane
mg/kg
ND
0.72
0.42
58
67-130 M1
1,2,4-Trichlorobenzene
mg/kg
ND
0.72
0.43
60
51-134
1,2,4-Trimethylbenzene
mg/kg
0.0083
0.72
0.44
61
63-136 M1
1,2-Dibromo-3-chloropropane
mg/kg
ND
0.72
0.41
56
32-130
1,2-Dibromoethane (EDB)
mg/kg
ND
0.72
0.45
63
70-130 M1
1,2-Dichlorobenzene
mg/kg
ND
0.72
0.46
64
69-130 M1
1,2-Dichloroethane
mg/kg
ND
0.72
0.35
49
59-130 M1
1,2-Dichloropropane
mg/kg
ND
0.72
0.44
61
70-130 M1
1,3,5-Trimethylbenzene
mg/kg
0.0044J
0.72
0.46
63
65-137 M1
1,3-Dichlorobenzene
mg/kg
ND
0.72
0.44
61
70-130 M1
1,3-Dichloropropane
mg/kg
ND
0.72
0.46
64
70-130 M1
1,4-Dichlorobenzene
mg/kg
ND
0.72
0.41
57
68-130 M1
2,2-Dichloropropane
mg/kg
ND
0.72
0.36
50
32-130
2-Butanone (MEK)
mg/kg
ND
1.4
0.68
47
10-136
2-Chlorotoluene
mg/kg
ND
0.72
0.44
61
69-141 M1
2-Hexanone
mg/kg
ND
1.4
0.75
52
10-144
4-Chlorotoluene
mg/kg
ND
0.72
0.40
56
70-132 M1
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
1.4
0.73
50
25-143
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 76 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
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QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
MATRIX SPIKE SAMPLE: 3586305
92593947008 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Acetone
mg/kg
0.051 J
1.4
0.65
42
10-130 v3
Benzene
mg/kg
ND
0.72
0.43
60
67-130 M1
Bromobenzene
mg/kg
ND
0.72
0.46
63
70-130 M1
Bromochloromethane
mg/kg
ND
0.72
0.42
59
69-134 M1
Bromodichloromethane
mg/kg
ND
0.72
0.39
54
64-130 M1
Bromoform
mg/kg
ND
0.72
0.41
57
62-130 M1
Bromomethane
mg/kg
ND
0.72
0.23
32
20-176
Carbon tetrachloride
mg/kg
ND
0.72
0.40
55
65-140 M1
Chlorobenzene
mg/kg
ND
0.72
0.45
62
70-130 M1
Chloroethane
mg/kg
ND
0.72
0.19
26
10-130
Chloroform
mg/kg
ND
0.72
0.40
56
63-130 M1
Chloromethane
mg/kg
ND
0.72
0.44
61
58-130
cis-1,2-Dichloroethene
mg/kg
ND
0.72
0.41
57
66-130 M1
cis-1,3-Dichloropropene
mg/kg
ND
0.72
0.40
56
67-130 M1
Dibromochloromethane
mg/kg
ND
0.72
0.38
53
67-130 M1
Dibromomethane
mg/kg
ND
0.72
0.43
60
63-131 M1
Dichlorodifluoromethane
mg/kg
ND
0.72
0.34
48
44-180
Diisopropyl ether
mg/kg
ND
0.72
0.38
52
63-130 M1
Ethylbenzene
mg/kg
0.0049J
0.72
0.42
58
66-130 M1
Hexachloro-1,3-butadiene
mg/kg
ND
0.72
0.47
65
64-150
Isopropylbenzene (Cumene)
mg/kg
ND
0.72
0.48
66
69-135 M1
m&p-Xylene
mg/kg
0.021
1.4
0.87
59
60-133 M1
Methyl-tert-butyl ether
mg/kg
ND
0.72
0.39
54
65-130 M1
Methylene Chloride
mg/kg
ND
0.72
0.36
50
61-130 M1
n-Butylbenzene
mg/kg
ND
0.72
0.39
54
65-140 M1
n-Propylbenzene
mg/kg
ND
0.72
0.42
59
67-140 M1
Naphthalene
mg/kg
0.016
0.72
0.46
62
15-145
o-Xylene
mg/kg
0.012
0.72
0.47
64
66-133 M1
p-Isopropyltoluene
mg/kg
ND
0.72
0.43
60
56-147
sec-Butylbenzene
mg/kg
ND
0.72
0.45
63
65-139 M1
Styrene
mg/kg
ND
0.72
0.45
63
70-132 M1
tert-Butyl benzene
mg/kg
ND
0.72
0.52
73
62-135
Tetrachloroethene
mg/kg
ND
0.72
0.39
55
70-135 M1
Toluene
mg/kg
0.015
0.72
0.43
57
67-130 M1
trans-1,2-Dichloroethene
mg/kg
ND
0.72
0.40
55
69-130 M1
trans- 1,3-Dichloropropene
mg/kg
ND
0.72
0.40
55
62-130 M1
Trichloroethene
mg/kg
ND
0.72
0.41
56
70-135 M1
Trichlorofluoromethane
mg/kg
ND
0.72
0.15
21
10-130
Vinyl acetate
mg/kg
ND
1.4
0.71
49
53-130 M1
Vinyl chloride
mg/kg
ND
0.72
0.45
62
61-148
Xylene (Total)
mg/kg
0.032
2.2
1.3
60
63-132 MS
1,2-Dichloroethane-d4 (S)
%
84
70-130
4-Bromofluorobenzene (S)
%
96
69-134
Toluene-d8 (S)
%
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 77 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
SAMPLE DUPLICATE: 3586306
Parameter
Units
92593947009
Result
Dup
Result RPD
Max
RPD Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
ND
ND
30
1,1,1-Trichloroethane
mg/kg
ND
ND
30
1,1,2,2-Tetrachloroethane
mg/kg
ND
ND
30
1,1,2-Trichloroethane
mg/kg
ND
ND
30
1,1-Dichloroethane
mg/kg
ND
ND
30
1,1-Dichloroethene
mg/kg
ND
ND
30
1,1-Dichloropropene
mg/kg
ND
ND
30
1,2,3-Trichlorobenzene
mg/kg
ND
ND
30
1,2,3-Trichloropropane
mg/kg
ND
ND
30
1,2,4-Trichlorobenzene
mg/kg
ND
ND
30
1,2,4-Trimethylbenzene
mg/kg
ND
ND
30
1,2-Dibromo-3-chloropropane
mg/kg
ND
ND
30
1,2-Dibromoethane (EDB)
mg/kg
ND
ND
30
1,2-Dichlorobenzene
mg/kg
ND
ND
30
1,2-Dichloroethane
mg/kg
ND
ND
30
1,2-Dichloropropane
mg/kg
ND
ND
30
1,3,5-Trimethylbenzene
mg/kg
ND
ND
30
1,3-Dichlorobenzene
mg/kg
ND
ND
30
1,3-Dichloropropane
mg/kg
ND
ND
30
1,4-Dichlorobenzene
mg/kg
ND
ND
30
2,2-Dichloropropane
mg/kg
ND
ND
30
2-Butanone (MEK)
mg/kg
ND
ND
30
2-Chlorotoluene
mg/kg
ND
ND
30
2-Hexanone
mg/kg
ND
ND
30
4-Chlorotoluene
mg/kg
ND
ND
30
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
ND
30
Acetone
mg/kg
ND
ND
30 v2
Benzene
mg/kg
ND
ND
30
Bromobenzene
mg/kg
ND
ND
30
Bromochloromethane
mg/kg
ND
ND
30
Bromodichloromethane
mg/kg
ND
ND
30
Bromoform
mg/kg
ND
ND
30
Bromomethane
mg/kg
ND
ND
30
Carbon tetrachloride
mg/kg
ND
ND
30
Chlorobenzene
mg/kg
ND
ND
30
Chloroethane
mg/kg
ND
ND
30
Chloroform
mg/kg
ND
ND
30
Chloromethane
mg/kg
ND
ND
30
cis-1,2-Dichloroethene
mg/kg
ND
ND
30
cis-1,3-Dichloropropene
mg/kg
ND
ND
30
Dibromochloromethane
mg/kg
ND
ND
30
Dibromomethane
mg/kg
ND
ND
30
Dichlorodifluoromethane
mg/kg
ND
ND
30
Diisopropyl ether
mg/kg
ND
ND
30
Ethylbenzene
mg/kg
ND
ND
30
Hexachloro-1,3-butadiene
mg/kg
ND
ND
30
Isopropylbenzene (Cumene)
mg/kg
ND
ND
30
Results presented on this page are in the units
indicated by the "Units" column except where an alternate unit
is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 78 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
SAMPLE DUPLICATE: 3586306
Parameter
Units
92593947009
Result
Dup
Result
m&p-Xylene
mg/kg
ND
ND
Methyl-tert-butyl ether
mg/kg
ND
ND
Methylene Chloride
mg/kg
ND
ND
n-Butylbenzene
mg/kg
ND
ND
n-Propylbenzene
mg/kg
ND
ND
Naphthalene
mg/kg
ND
ND
o-Xylene
mg/kg
ND
ND
p-Isopropyltoluene
mg/kg
ND
ND
sec-Butylbenzene
mg/kg
ND
ND
Styrene
mg/kg
ND
ND
tert-Butyl benzene
mg/kg
ND
ND
Tetrachloroethene
mg/kg
ND
ND
Toluene
mg/kg
ND
ND
trans-1,2-Dichloroethene
mg/kg
ND
ND
trans- 1,3-Dichloropropene
mg/kg
ND
ND
Trichloroethene
mg/kg
ND
ND
Trichlorofluoromethane
mg/kg
ND
ND
Vinyl acetate
mg/kg
ND
ND
Vinyl chloride
mg/kg
ND
ND
Xylene (Total)
mg/kg
ND
ND
1,2-Dichloroethane-d4 (S)
%
92
96
4-Bromofluorobenzene (S)
%
96
96
Toluene-d8 (S)
%
99
99
Max
RPD RPD Qualifiers
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC.
Page 79 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
QC Batch: 686161 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92593947007
METHOD BLANK: 3587711
Associated Lab Samples: 92593947007
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
mg/kg
ND
0.0050
0.0019
03/21/22 15:53
1,1,1-Trichloroethane
mg/kg
ND
0.0050
0.0026
03/21/22 15:53
1,1,2,2-Tetrachloroethane
mg/kg
ND
0.0050
0.0013
03/21/22 15:53
1,1,2-Trichloroethane
mg/kg
ND
0.0050
0.0017
03/21/22 15:53
1,1-Dichloroethane
mg/kg
ND
0.0050
0.0021
03/21/22 15:53
1,1-Dichloroethene
mg/kg
ND
0.0050
0.0021
03/21/22 15:53
1,1-Dichloropropene
mg/kg
ND
0.0050
0.0024
03/21/22 15:53
1,2,3-Trichlorobenzene
mg/kg
ND
0.0050
0.0040
03/21/22 15:53
1,2,3-Trichloropropane
mg/kg
ND
0.0050
0.0025
03/21/22 15:53
1,2,4-Trichlorobenzene
mg/kg
ND
0.0050
0.0042
03/21/22 15:53
1,2,4-Trimethylbenzene
mg/kg
ND
0.0050
0.0014
03/21/22 15:53
1,2-Dibromo-3-chloropropane
mg/kg
ND
0.0050
0.0019
03/21/22 15:53
1,2-Dibromoethane (EDB)
mg/kg
ND
0.0050
0.0022
03/21/22 15:53
1,2-Dichlorobenzene
mg/kg
ND
0.0050
0.0018
03/21/22 15:53
1,2-Dichloroethane
mg/kg
ND
0.0050
0.0033
03/21/22 15:53
1,2-Dichloropropane
mg/kg
ND
0.0050
0.0015
03/21/22 15:53
1,3,5-Trimethylbenzene
mg/kg
ND
0.0050
0.0017
03/21/22 15:53
1,3-Dichlorobenzene
mg/kg
ND
0.0050
0.0016
03/21/22 15:53
1,3-Dichloropropane
mg/kg
ND
0.0050
0.0016
03/21/22 15:53
1,4-Dichlorobenzene
mg/kg
ND
0.0050
0.0013
03/21/22 15:53
2,2-Dichloropropane
mg/kg
ND
0.0050
0.0016
03/21/22 15:53
2-Butanone (MEK)
mg/kg
ND
0.10
0.024
03/21/22 15:53
2-Chlorotoluene
mg/kg
ND
0.0050
0.0018
03/21/22 15:53
2-Hexanone
mg/kg
ND
0.050
0.0048
03/21/22 15:53
4-Chlorotoluene
mg/kg
ND
0.0050
0.00088
03/21/22 15:53
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
0.050
0.0048
03/21/22 15:53
Acetone
mg/kg
ND
0.10
0.032
03/21/22 15:53
Benzene
mg/kg
ND
0.0050
0.0020
03/21/22 15:53
Bromobenzene
mg/kg
ND
0.0050
0.0016
03/21/22 15:53
Bromochloromethane
mg/kg
ND
0.0050
0.0015
03/21/22 15:53
Bromodichloromethane
mg/kg
ND
0.0050
0.0019
03/21/22 15:53
Bromoform
mg/kg
ND
0.0050
0.0018
03/21/22 15:53
Bromomethane
mg/kg
ND
0.010
0.0079
03/21/22 15:53
Carbon tetrachloride
mg/kg
ND
0.0050
0.0019
03/21/22 15:53
Chlorobenzene
mg/kg
ND
0.0050
0.00096
03/21/22 15:53
Chloroethane
mg/kg
ND
0.010
0.0039
03/21/22 15:53
Chloroform
mg/kg
ND
0.0050
0.0030
03/21/22 15:53
Chloromethane
mg/kg
ND
0.010
0.0042
03/21/22 15:53
cis-1,2-Dichloroethene
mg/kg
ND
0.0050
0.0017
03/21/22 15:53
cis-1,3-Dichloropropene
mg/kg
ND
0.0050
0.0014
03/21/22 15:53
v2
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 80 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
METHOD BLANK: 3587711
Associated Lab Samples: 92593947007
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
Dibromochloromethane
mg/kg
ND
0.0050
0.0028
03/21/22 15:53
Dibromomethane
mg/kg
ND
0.0050
0.0011
03/21/22 15:53
Dichlorodifluoromethane
mg/kg
ND
0.010
0.0022
03/21/22 15:53
Diisopropyl ether
mg/kg
ND
0.0050
0.0014
03/21/22 15:53
Ethylbenzene
mg/kg
ND
0.0050
0.0023
03/21/22 15:53
Hexachloro-1,3-butadiene
mg/kg
ND
0.010
0.0082
03/21/22 15:53
Isopropylbenzene (Cumene)
mg/kg
ND
0.0050
0.0017
03/21/22 15:53
m&p-Xylene
mg/kg
ND
0.010
0.0034
03/21/22 15:53
Methyl-tert-butyl ether
mg/kg
ND
0.0050
0.0019
03/21/22 15:53
Methylene Chloride
mg/kg
ND
0.020
0.014
03/21/22 15:53
n-Butylbenzene
mg/kg
ND
0.0050
0.0024
03/21/22 15:53
n-Propylbenzene
mg/kg
ND
0.0050
0.0018
03/21/22 15:53
Naphthalene
mg/kg
ND
0.0050
0.0026
03/21/22 15:53
o-Xylene
mg/kg
ND
0.0050
0.0022
03/21/22 15:53
p-Isopropyltoluene
mg/kg
ND
0.0050
0.0025
03/21/22 15:53
sec-Butylbenzene
mg/kg
ND
0.0050
0.0022
03/21/22 15:53
Styrene
mg/kg
ND
0.0050
0.0013
03/21/22 15:53
tert-Butyl benzene
mg/kg
ND
0.0050
0.0018
03/21/22 15:53
Tetrachloroethene
mg/kg
ND
0.0050
0.0016
03/21/22 15:53
Toluene
mg/kg
ND
0.0050
0.0014
03/21/22 15:53
trans-1,2-Dichloroethene
mg/kg
ND
0.0050
0.0018
03/21/22 15:53
trans- 1,3-Dichloropropene
mg/kg
ND
0.0050
0.0017
03/21/22 15:53
Trichloroethene
mg/kg
ND
0.0050
0.0013
03/21/22 15:53
Trichlorofluoromethane
mg/kg
ND
0.0050
0.0028
03/21/22 15:53
Vinyl acetate
mg/kg
ND
0.050
0.0036
03/21/22 15:53
Vinyl chloride
mg/kg
ND
0.010
0.0025
03/21/22 15:53
Xylene (Total)
mg/kg
ND
0.010
0.0028
03/21/22 15:53
1,2-Dichloroethane-d4 (S)
%
87
70-130
03/21/22 15:53
4-Bromofluorobenzene (S)
%
96
69-134
03/21/22 15:53
Toluene-d8 (S)
%
99
70-130
03/21/22 15:53
v2
v2
Qualifiers
LABORATORY CONTROL SAMPLE:
3587712
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
1.2
1.2
95
70-130
1,1,1-Trichloroethane
mg/kg
1.2
1.0
81
70-130
1,1,2,2-Tetrachloroethane
mg/kg
1.2
1.2
97
70-130
1,1,2-Trichloroethane
mg/kg
1.2
1.1
92
70-130
1,1-Dichloroethane
mg/kg
1.2
1.1
85
70-130
1,1-Dichloroethene
mg/kg
1.2
1.0
84
70-130
1,1-Dichloropropene
mg/kg
1.2
1.1
89
70-130
1,2,3-Trichlorobenzene
mg/kg
1.2
1.4
109
65-130
1,2,3-Trichloropropane
mg/kg
1.2
1.2
95
70-130
1,2,4-Trichlorobenzene
mg/kg
1.2
1.3
106
68-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 81 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
LABORATORY CONTROL SAMPLE:
Parameter
3587712
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trimethylbenzene
mg/kg
1.2
1.2
98
70-130
1,2-Dibromo-3-chloropropane
mg/kg
1.2
1.3
105
70-130
1,2-Dibromoethane (EDB)
mg/kg
1.2
1.2
93
70-130
1,2-Dichlorobenzene
mg/kg
1.2
1.3
101
70-130
1,2-Dichloroethane
mg/kg
1.2
0.91
73
63-130 v3
1,2-Dichloropropane
mg/kg
1.2
1.2
93
70-130
1,3,5-Trimethylbenzene
mg/kg
1.2
1.3
101
70-130
1,3-Dichlorobenzene
mg/kg
1.2
1.2
100
70-130
1,3-Dichloropropane
mg/kg
1.2
1.1
92
70-130
1,4-Dichlorobenzene
mg/kg
1.2
1.2
93
70-130
2,2-Dichloropropane
mg/kg
1.2
1.0
81
66-130
2-Butanone (MEK)
mg/kg
2.5
2.2
88
70-130
2-Chlorotoluene
mg/kg
1.2
1.2
99
70-130
2-Hexanone
mg/kg
2.5
2.4
95
70-130
4-Chlorotoluene
mg/kg
1.2
1.2
95
70-130
4-Methyl-2-pentanone (MIBK)
mg/kg
2.5
2.3
91
70-130
Acetone
mg/kg
2.5
1.9
78
69-130 v3
Benzene
mg/kg
1.2
1.1
88
70-130
Bromobenzene
mg/kg
1.2
1.3
102
70-130
Bromochloromethane
mg/kg
1.2
1.1
88
70-130
Bromodichloromethane
mg/kg
1.2
1.1
87
69-130
Bromoform
mg/kg
1.2
1.3
102
70-130
Bromomethane
mg/kg
1.2
1.0
82
52-130
Carbon tetrachloride
mg/kg
1.2
1.1
89
70-130
Chlorobenzene
mg/kg
1.2
1.2
93
70-130
Chloroethane
mg/kg
1.2
1.2
97
65-130
Chloroform
mg/kg
1.2
1.0
83
70-130
Chloromethane
mg/kg
1.2
1.1
85
55-130
cis-1,2-Dichloroethene
mg/kg
1.2
1.1
86
70-130
cis-1,3-Dichloropropene
mg/kg
1.2
1.1
89
70-130
Dibromochloromethane
mg/kg
1.2
1.1
88
70-130
Dibromomethane
mg/kg
1.2
1.2
93
70-130
Dichlorodifluoromethane
mg/kg
1.2
1.1
89
45-156
Diisopropyl ether
mg/kg
1.2
0.99
79
70-130 v3
Ethylbenzene
mg/kg
1.2
1.1
90
70-130
Hexachloro-1,3-butadiene
mg/kg
1.2
1.3
105
66-130
Isopropylbenzene (Cumene)
mg/kg
1.2
1.2
100
70-130
m&p-Xylene
mg/kg
2.5
2.3
94
70-130
Methyl-tert-butyl ether
mg/kg
1.2
1.0
80
70-130
Methylene Chloride
mg/kg
1.2
0.92
74
65-130 v3
n-Butylbenzene
mg/kg
1.2
1.2
99
67-130
n-Propylbenzene
mg/kg
1.2
1.2
97
70-130
Naphthalene
mg/kg
1.2
1.3
108
70-130
o-Xylene
mg/kg
1.2
1.2
97
70-130
p-Isopropyltoluene
mg/kg
1.2
1.3
102
67-130
sec-Butylbenzene
mg/kg
1.2
1.2
100
69-130
Styrene
mg/kg
1.2
1.3
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 82 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
LABORATORY CONTROL SAMPLE:
Parameter
3587712
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
tert-Butyl benzene
mg/kg
1.2
1.2
97
67-130
Tetrachloroethene
mg/kg
1.2
1.2
95
70-130
Toluene
mg/kg
1.2
1.1
89
70-130
trans-1,2-Dichloroethene
mg/kg
1.2
1.1
87
70-130
trans- 1,3-Dichloropropene
mg/kg
1.2
1.1
88
68-130
Trichloroethene
mg/kg
1.2
1.2
93
70-130
Trichlorofluoromethane
mg/kg
1.2
1.0
81
70-130
Vinyl acetate
mg/kg
2.5
2.0
80
70-130
Vinyl chloride
mg/kg
1.2
1.2
94
61-130
Xylene (Total)
mg/kg
3.8
3.6
95
70-130
1,2-Dichloroethane-d4 (S)
%
85
70-130
4-Bromofluorobenzene (S)
%
94
69-134
Toluene-d8 (S)
%
99
70-130
MATRIX SPIKE SAMPLE:
Parameter
3587713
Units
92594268001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
ND
0.89
0.85
96
70-131
1,1,1-Trichloroethane
mg/kg
ND
0.89
0.87
98
65-133
1,1,2,2-Tetrachloroethane
mg/kg
ND
0.89
0.79
89
66-130
1,1,2-Trichloroethane
mg/kg
ND
0.89
0.66
74
66-133
1,1-Dichloroethane
mg/kg
ND
0.89
0.86
97
65-130
1,1-Dichloroethene
mg/kg
ND
0.89
0.83
93
10-158
1,1-Dichloropropene
mg/kg
ND
0.89
0.87
98
68-133
1,2,3-Trichlorobenzene
mg/kg
ND
0.89
0.70
79
27-138
1,2,3-Trichloropropane
mg/kg
ND
0.89
0.77
87
67-130
1,2,4-Trichlorobenzene
mg/kg
ND
0.89
0.81
91
51-134
1,2,4-Trimethylbenzene
mg/kg
34.3 ug/kg
0.89
0.82
88
63-136
1,2-Dibromo-3-chloropropane
mg/kg
ND
0.89
0.78
87
32-130
1,2-Dibromoethane (EDB)
mg/kg
ND
0.89
0.80
90
70-130
1,2-Dichlorobenzene
mg/kg
ND
0.89
0.80
90
69-130
1,2-Dichloroethane
mg/kg
ND
0.89
0.84
94
59-130
1,2-Dichloropropane
mg/kg
ND
0.89
0.95
107
70-130
1,3,5-Trimethylbenzene
mg/kg
18.6 ug/kg
0.89
0.82
90
65-137
1,3-Dichlorobenzene
mg/kg
ND
0.89
0.79
88
70-130
1,3-Dichloropropane
mg/kg
ND
0.89
0.76
86
70-130
1,4-Dichlorobenzene
mg/kg
ND
0.89
0.77
86
68-130
2,2-Dichloropropane
mg/kg
ND
0.89
0.89
100
32-130
2-Butanone (MEK)
mg/kg
ND
1.8
1.4
77
10-136
2-Chlorotoluene
mg/kg
ND
0.89
0.79
88
69-141
2-Hexanone
mg/kg
ND
1.8
1.4
77
10-144
4-Chlorotoluene
mg/kg
ND
0.89
0.77
86
70-132
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
1.8
1.4
77
25-143
Acetone
mg/kg
ND
1.8
1.0
58
10-130
Benzene
mg/kg
ND
0.89
0.68
76
67-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 83 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
MATRIX SPIKE SAMPLE:
3587713
92594268001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Bromobenzene
mg/kg
ND
0.89
0.84
94
70-130
Bromochloromethane
mg/kg
ND
0.89
0.80
90
69-134
Bromodichloromethane
mg/kg
ND
0.89
0.89
100
64-130
Bromoform
mg/kg
ND
0.89
0.83
93
62-130
Bromomethane
mg/kg
ND
0.89
1.1
124
20-176 v3
Carbon tetrachloride
mg/kg
ND
0.89
0.71
80
65-140 v1
Chlorobenzene
mg/kg
ND
0.89
0.84
94
70-130
Chloroethane
mg/kg
ND
0.89
0.71
79
10-130
Chloroform
mg/kg
ND
0.89
0.85
96
63-130
Chloromethane
mg/kg
ND
0.89
0.85
96
58-130
cis-1,2-Dichloroethene
mg/kg
ND
0.89
0.84
94
66-130
cis-1,3-Dichloropropene
mg/kg
ND
0.89
0.95
106
67-130
Dibromochloromethane
mg/kg
ND
0.89
0.74
83
67-130
Dibromomethane
mg/kg
ND
0.89
0.88
99
63-131
Dichlorodifluoromethane
mg/kg
ND
0.89
0.94
105
44-180
Diisopropyl ether
mg/kg
ND
0.89
0.77
87
63-130
Ethylbenzene
mg/kg
13.0 ug/kg
0.89
0.80
89
66-130
Hexachloro-1,3-butadiene
mg/kg
ND
0.89
0.93
105
64-150
Isopropylbenzene (Cumene)
mg/kg
ND
0.89
0.90
101
69-135
m&p-Xylene
mg/kg
69.8 ug/kg
1.8
1.7
94
60-133
Methyl-tert-butyl ether
mg/kg
ND
0.89
0.78
87
65-130
Methylene Chloride
mg/kg
ND
0.89
0.81
91
61-130
n-Butylbenzene
mg/kg
ND
0.89
0.80
89
65-140
n-Propylbenzene
mg/kg
ND
0.89
0.79
88
67-140
Naphthalene
mg/kg
66.3 ug/kg
0.89
0.74
75
15-145
o-Xylene
mg/kg
42.7 ug/kg
0.89
0.91
98
66-133
p-Isopropyltoluene
mg/kg
ND
0.89
0.82
92
56-147
sec-Butylbenzene
mg/kg
ND
0.89
0.83
93
65-139
Styrene
mg/kg
ND
0.89
0.87
98
70-132
tert-Butyl benzene
mg/kg
ND
0.89
0.82
92
62-135
Tetrachloroethene
mg/kg
ND
0.89
0.94
106
70-135
Toluene
mg/kg
57.7 ug/kg
0.89
0.96
102
67-130
trans-1,2-Dichloroethene
mg/kg
ND
0.89
0.84
94
69-130
trans- 1,3-Dichloropropene
mg/kg
ND
0.89
0.75
84
62-130
Trichloroethene
mg/kg
9.8 ug/kg
0.89
0.89
99
70-135
Trichlorofluoromethane
mg/kg
ND
0.89
0.90
102
10-130
Vinyl acetate
mg/kg
ND
1.8
1.4
81
53-130
Vinyl chloride
mg/kg
ND
0.89
0.95
107
61-148
Xylene (Total)
mg/kg
113 ug/kg
2.7
2.6
95
63-132
1,2-Dichloroethane-d4 (S)
%
100
70-130
4-Bromofluorobenzene (S)
%
101
69-134
Toluene-d8 (S)
%
111
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 84 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
SAMPLE DUPLICATE: 3587714
Parameter
Units
92594268002
Result
Dup
Result
RPD
Max
RPD Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
ND
ND
30
1,1,1-Trichloroethane
mg/kg
ND
ND
30
1,1,2,2-Tetrachloroethane
mg/kg
ND
ND
30
1,1,2-Trichloroethane
mg/kg
ND
ND
30
1,1-Dichloroethane
mg/kg
ND
ND
30
1,1-Dichloroethene
mg/kg
ND
ND
30
1,1-Dichloropropene
mg/kg
ND
ND
30
1,2,3-Trichlorobenzene
mg/kg
ND
ND
30
1,2,3-Trichloropropane
mg/kg
ND
ND
30
1,2,4-Trichlorobenzene
mg/kg
ND
ND
30
1,2,4-Trimethylbenzene
mg/kg
41.7 ug/kg
0.038
10
30
1,2-Dibromo-3-chloropropane
mg/kg
ND
ND
30
1,2-Dibromoethane (EDB)
mg/kg
ND
ND
30
1,2-Dichlorobenzene
mg/kg
ND
ND
30
1,2-Dichloroethane
mg/kg
ND
ND
30
1,2-Dichloropropane
mg/kg
ND
ND
30
1,3,5-Trimethylbenzene
mg/kg
21.9 ug/kg
0.015
40
30 D6
1,3-Dichlorobenzene
mg/kg
ND
ND
30
1,3-Dichloropropane
mg/kg
ND
ND
30
1,4-Dichlorobenzene
mg/kg
ND
ND
30
2,2-Dichloropropane
mg/kg
ND
ND
30
2-Butanone (MEK)
mg/kg
ND
ND
30
2-Chlorotoluene
mg/kg
ND
ND
30
2-Hexanone
mg/kg
ND
ND
30
4-Chlorotoluene
mg/kg
ND
ND
30
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
ND
30
Acetone
mg/kg
ND
ND
30
Benzene
mg/kg
9.2 ug/kg
0.0088
5
30
Bromobenzene
mg/kg
ND
ND
30
Bromochloromethane
mg/kg
ND
ND
30
Bromodichloromethane
mg/kg
ND
ND
30
Bromoform
mg/kg
ND
ND
30
Bromomethane
mg/kg
ND
ND
30 v2
Carbon tetrachloride
mg/kg
ND
ND
30 v1
Chlorobenzene
mg/kg
ND
ND
30
Chloroethane
mg/kg
ND
ND
30
Chloroform
mg/kg
ND
ND
30
Chloromethane
mg/kg
ND
ND
30
cis-1,2-Dichloroethene
mg/kg
ND
ND
30
cis-1,3-Dichloropropene
mg/kg
ND
ND
30
Dibromochloromethane
mg/kg
ND
ND
30
Dibromomethane
mg/kg
ND
ND
30
Dichlorodifluoromethane
mg/kg
ND
ND
30
Diisopropyl ether
mg/kg
ND
ND
30
Ethylbenzene
mg/kg
14.2 ug/kg
0.015
5
30
Hexachloro-1,3-butadiene
mg/kg
ND
ND
30
Isopropylbenzene (Cumene)
mg/kg
9.8 ug/kg
0.0095
3
30
Results presented on this page are in the units
indicated by the "Units" column except where an alternate unit is presented
to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 85 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
SAMPLE DUPLICATE: 3587714
Parameter
Units
92594268002
Result
Dup
Result
m&p-Xylene
mg/kg
95.1 ug/kg
0.098
Methyl-tert-butyl ether
mg/kg
ND
ND
Methylene Chloride
mg/kg
ND
ND
n-Butylbenzene
mg/kg
ND
0.0060J
n-Propylbenzene
mg/kg
ND
0.0072J
Naphthalene
mg/kg
96.1 ug/kg
0.11
o-Xylene
mg/kg
57.3 ug/kg
0.055
p-Isopropyltoluene
mg/kg
ND
0.0081
sec-Butylbenzene
mg/kg
ND
ND
Styrene
mg/kg
ND
ND
tert-Butyl benzene
mg/kg
ND
ND
Tetrachloroethene
mg/kg
ND
ND
Toluene
mg/kg
73.9 ug/kg
0.065
trans-1,2-Dichloroethene
mg/kg
ND
ND
trans- 1,3-Dichloropropene
mg/kg
ND
ND
Trichloroethene
mg/kg
24.9 ug/kg
0.027
Trichlorofluoromethane
mg/kg
ND
ND
Vinyl acetate
mg/kg
ND
ND
Vinyl chloride
mg/kg
ND
ND
Xylene (Total)
mg/kg
152 ug/kg
0.15
1,2-Dichloroethane-d4 (S)
%
86
96
4-Bromofluorobenzene (S)
%
96
101
Toluene-d8 (S)
%
98
85
IVV
Max
RPD
3 30
30
30
30
30
15 30
4 30
30
30
30
30
30
12 30
30
30
7 30
30
30
30
0 30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC.
Page 86 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
QC Batch: 685751 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92593947001, 92593947002, 92593947003, 92593947004
METHOD BLANK: 3585802 Matrix: Water
Associated Lab Samples: 92593947001, 92593947002, 92593947003, 92593947004
Blank Reporting
Parameter Units Result Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.31
03/18/22 12:42
1,1,1-Trichloroethane
ug/L
ND
1.0
0.33
03/18/22 12:42
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
03/18/22 12:42
1,1,2-Trichloroethane
ug/L
ND
1.0
0.32
03/18/22 12:42
1,1-Dichloroethane
ug/L
ND
1.0
0.37
03/18/22 12:42
1,1-Dichloroethene
ug/L
ND
1.0
0.35
03/18/22 12:42
1,1-Dichloropropene
ug/L
ND
1.0
0.43
03/18/22 12:42
1,2,3-Trichlorobenzene
ug/L
ND
1.0
0.81
03/18/22 12:42
1,2,3-Trichloropropane
ug/L
ND
1.0
0.26
03/18/22 12:42
1,2,4-Trichlorobenzene
ug/L
ND
1.0
0.64
03/18/22 12:42
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
0.34
03/18/22 12:42
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
03/18/22 12:42
1,2-Dichlorobenzene
ug/L
ND
1.0
0.34
03/18/22 12:42
1,2-Dichloroethane
ug/L
ND
1.0
0.32
03/18/22 12:42
1,2-Dichloropropane
ug/L
ND
1.0
0.36
03/18/22 12:42
1,3-Dichlorobenzene
ug/L
ND
1.0
0.34
03/18/22 12:42
1,3-Dichloropropane
ug/L
ND
1.0
0.28
03/18/22 12:42
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
03/18/22 12:42
2,2-Dichloropropane
ug/L
ND
1.0
0.39
03/18/22 12:42
2-Butanone (MEK)
ug/L
ND
5.0
4.0
03/18/22 12:42
2-Chlorotoluene
ug/L
ND
1.0
0.32
03/18/22 12:42
2-Hexanone
ug/L
ND
5.0
0.48
03/18/22 12:42
4-Chlorotoluene
ug/L
ND
1.0
0.32
03/18/22 12:42
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
2.7
03/18/22 12:42
Acetone
ug/L
ND
25.0
5.1
03/18/22 12:42
Benzene
ug/L
ND
1.0
0.34
03/18/22 12:42
Bromobenzene
ug/L
ND
1.0
0.29
03/18/22 12:42
Bromochloromethane
ug/L
ND
1.0
0.47
03/18/22 12:42
Bromodichloromethane
ug/L
ND
1.0
0.31
03/18/22 12:42
Bromoform
ug/L
ND
1.0
0.34
03/18/22 12:42
Bromomethane
ug/L
ND
2.0
1.7
03/18/22 12:42
Carbon tetrachloride
ug/L
ND
1.0
0.33
03/18/22 12:42
Chlorobenzene
ug/L
ND
1.0
0.28
03/18/22 12:42
Chloroethane
ug/L
ND
1.0
0.65
03/18/22 12:42
Chloroform
ug/L
ND
1.0
0.43
03/18/22 12:42
Chloromethane
ug/L
ND
1.0
0.54
03/18/22 12:42
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.38
03/18/22 12:42
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.36
03/18/22 12:42
Dibromochloromethane
ug/L
ND
1.0
0.36
03/18/22 12:42
Dibromomethane
ug/L
ND
1.0
0.39
03/18/22 12:42
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 87 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
METHOD BLANK: 3585802 Matrix: Water
Associated Lab Samples: 92593947001, 92593947002, 92593947003, 92593947004
Blank Reporting
Parameter Units Result Limit
MDL
Analyzed Qualifiers
Dichlorodifluoromethane
ug/L
ND
1.0
0.35
03/18/22 12:42
Diisopropyl ether
ug/L
ND
1.0
0.31
03/18/22 12:42
Ethylbenzene
ug/L
ND
1.0
0.30
03/18/22 12:42
Hexachloro-1,3-butadiene
ug/L
ND
2.0
1.5
03/18/22 12:42 v1
m&p-Xylene
ug/L
ND
2.0
0.71
03/18/22 12:42
Methyl-tert-butyl ether
ug/L
ND
1.0
0.42
03/18/22 12:42
Methylene Chloride
ug/L
ND
5.0
2.0
03/18/22 12:42
Naphthalene
ug/L
ND
1.0
0.64
03/18/22 12:42
o-Xylene
ug/L
ND
1.0
0.34
03/18/22 12:42
p-Isopropyltoluene
ug/L
ND
1.0
0.41
03/18/22 12:42
Styrene
ug/L
ND
1.0
0.29
03/18/22 12:42
Tetrachloroethene
ug/L
ND
1.0
0.29
03/18/22 12:42
Toluene
ug/L
ND
1.0
0.48
03/18/22 12:42
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.40
03/18/22 12:42
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.36
03/18/22 12:42
Trichloroethene
ug/L
ND
1.0
0.38
03/18/22 12:42
Trichlorofluoromethane
ug/L
ND
1.0
0.30
03/18/22 12:42
Vinyl acetate
ug/L
ND
2.0
1.3
03/18/22 12:42
Vinyl chloride
ug/L
ND
1.0
0.39
03/18/22 12:42
Xylene (Total)
ug/L
ND
1.0
0.34
03/18/22 12:42
1,2-Dichloroethane-d4 (S)
%
91
70-130
03/18/22 12:42
4-Bromofluorobenzene (S)
%
97
70-130
03/18/22 12:42
Toluene-d8 (S)
%
106
70-130
03/18/22 12:42
LABORATORY CONTROL SAMPLE:
3585803
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
51.8
104
70-130
1,1,1-Trichloroethane
ug/L
50
46.1
92
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
52.5
105
70-130
1,1,2-Trichloroethane
ug/L
50
49.4
99
70-130
1,1-Dichloroethane
ug/L
50
46.7
93
70-130
1,1-Dichloroethene
ug/L
50
45.4
91
70-132
1,1-Dichloropropene
ug/L
50
50.0
100
70-131
1,2,3-Trichlorobenzene
ug/L
50
51.5
103
70-134
1,2,3-Trichloropropane
ug/L
50
52.9
106
70-130
1,2,4-Trichlorobenzene
ug/L
50
52.2
104
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
48.9
98
70-132
1,2-Dibromoethane (EDB)
ug/L
50
53.9
108
70-130
1,2-Dichlorobenzene
ug/L
50
50.5
101
70-130
1,2-Dichloroethane
ug/L
50
48.6
97
70-130
1,2-Dichloropropane
ug/L
50
51.4
103
70-130
1,3-Dichlorobenzene
ug/L
50
51.3
103
70-130
1,3-Dichloropropane
ug/L
50
51.6
103
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 88 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
LABORATORY CONTROL SAMPLE:
Parameter
3585803
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,4-Dichlorobenzene
ug/L
50
51.1
102
70-130
2,2-Dichloropropane
ug/L
50
44.3
89
70-130
2-Butanone (MEK)
ug/L
100
84.5
85
70-133
2-Chlorotoluene
ug/L
50
51.8
104
70-130
2-Hexanone
ug/L
100
100
100
70-130
4-Chlorotoluene
ug/L
50
49.2
98
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
91.6
92
70-130
Acetone
ug/L
100
90.6
91
70-144
Benzene
ug/L
50
46.9
94
70-130
Bromobenzene
ug/L
50
49.5
99
70-130
Bromochloromethane
ug/L
50
47.0
94
70-130
Bromodichloromethane
ug/L
50
47.3
95
70-130
Bromoform
ug/L
50
51.0
102
70-131
Bromomethane
ug/L
50
49.5
99
30-177
Carbon tetrachloride
ug/L
50
45.2
90
70-130
Chlorobenzene
ug/L
50
47.2
94
70-130
Chloroethane
ug/L
50
68.1
136
46-131 L1
Chloroform
ug/L
50
47.1
94
70-130
Chloromethane
ug/L
50
43.9
88
49-130
cis-1,2-Dichloroethene
ug/L
50
46.8
94
70-130
cis-1,3-Dichloropropene
ug/L
50
48.1
96
70-130
Dibromochloromethane
ug/L
50
49.8
100
70-130
Dibromomethane
ug/L
50
45.3
91
70-130
Dichlorodifluoromethane
ug/L
50
44.0
88
52-134
Diisopropyl ether
ug/L
50
47.6
95
70-131
Ethylbenzene
ug/L
50
48.7
97
70-130
Hexachloro-1,3-butadiene
ug/L
50
63.4
127
70-131 v1
m&p-Xylene
ug/L
100
98.1
98
70-130
Methyl-tert-butyl ether
ug/L
50
48.3
97
70-130
Methylene Chloride
ug/L
50
44.6
89
68-130
Naphthalene
ug/L
50
50.1
100
70-133
o-Xylene
ug/L
50
48.4
97
70-130
p-Isopropyltoluene
ug/L
50
55.3
111
70-130
Styrene
ug/L
50
49.3
99
70-130
Tetrachloroethene
ug/L
50
48.1
96
70-130
Toluene
ug/L
50
44.6
89
70-130
trans-1,2-Dichloroethene
ug/L
50
45.9
92
70-130
trans- 1,3-Dichloropropene
ug/L
50
48.5
97
70-130
Trichloroethene
ug/L
50
47.6
95
70-130
Trichlorofluoromethane
ug/L
50
47.5
95
61-130
Vinyl acetate
ug/L
100
86.0
86
70-140
Vinyl chloride
ug/L
50
45.6
91
59-142
Xylene (Total)
ug/L
150
146
98
70-130
1,2-Dichloroethane-d4 (S)
%
98
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
96
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 89 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3585804
MS
92593947001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3585805
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
20.5
20.3
103
101
70-135
1
30
1,1,1-Trichloroethane
ug/L
ND
20
20
20.1
19.7
101
99
70-148
2
30
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
21.5
21.2
108
106
70-131
1
30
1,1,2-Trichloroethane
ug/L
ND
20
20
21.7
19.8
109
99
70-136
9
30
1,1-Dichloroethane
ug/L
ND
20
20
19.1
19.4
95
97
70-147
2
30
1,1-Dichloroethene
ug/L
ND
20
20
20.0
18.9
100
95
70-158
6
30
1,1-Dichloropropene
ug/L
ND
20
20
21.8
20.9
109
105
70-149
4
30
1,2,3-Trichlorobenzene
ug/L
ND
20
20
22.4
21.2
112
106
68-140
6
30
1,2,3-Trichloropropane
ug/L
ND
20
20
21.9
21.2
110
106
67-137
3
30
1,2,4-Trichlorobenzene
ug/L
ND
20
20
22.9
21.3
115
106
70-139
7
30
1,2-Dibromo-3-
ug/L
ND
20
20
19.3
21.5
97
108
69-136
11
30
chloropropane
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.3
22.1
107
111
70-137
4
30
1,2-Dichlorobenzene
ug/L
ND
20
20
21.8
21.3
109
106
70-133
2
30
1,2-Dichloroethane
ug/L
ND
20
20
21.9
20.7
109
103
67-138
5
30
1,2-Dichloropropane
ug/L
ND
20
20
22.7
21.9
114
110
70-138
4
30
1,3-Dichlorobenzene
ug/L
ND
20
20
22.2
21.4
111
107
70-133
4
30
1,3-Dichloropropane
ug/L
ND
20
20
21.4
20.3
107
101
70-136
5
30
1,4-Dichlorobenzene
ug/L
ND
20
20
22.4
21.5
112
108
70-133
4
30
2,2-Dichloropropane
ug/L
ND
20
20
19.3
20.1
97
100
52-155
4
30
2-Butanone (MEK)
ug/L
ND
40
40
39.7
40.2
99
100
61-147
1
30
2-Chlorotoluene
ug/L
ND
20
20
22.8
21.7
114
108
70-141
5
30
2-Hexanone
ug/L
ND
40
40
40.3
42.4
101
106
67-139
5
30
4-Chlorotoluene
ug/L
ND
20
20
21.5
21.3
107
107
70-135
1
30
4-Methyl-2-pentanone
ug/L
ND
40
40
38.6
39.6
97
99
67-136
2
30
(MIBK)
Acetone
ug/L
ND
40
40
38.0
36.2
95
91
55-159
5
30
Benzene
ug/L
ND
20
20
20.0
19.8
100
99
67-150
1
30
Bromobenzene
ug/L
ND
20
20
21.9
21.7
109
108
70-134
1
30
Bromochloromethane
ug/L
ND
20
20
21.2
21.1
106
105
70-146
1
30
Bromodichloromethane
ug/L
ND
20
20
21.5
20.2
108
101
70-138
6
30
Bromoform
ug/L
ND
20
20
19.0
19.4
95
97
57-138
2
30
Bromomethane
ug/L
ND
20
20
21.6
20.6
108
103
10-200
5
30
Carbon tetrachloride
ug/L
ND
20
20
20.0
19.8
100
99
70-147
1
30
Chlorobenzene
ug/L
ND
20
20
20.9
20.3
105
101
70-137
3
30
Chloroethane
ug/L
ND
20
20
29.3
25.9
147
130
51-166
12
30
Chloroform
ug/L
ND
20
20
21.0
19.4
105
97
70-144
8
30
Chloromethane
ug/L
ND
20
20
18.5
18.4
93
92
24-161
1
30
cis-1,2-Dichloroethene
ug/L
ND
20
20
19.5
21.0
97
105
67-148
8
30
cis-1,3-Dichloropropene
ug/L
ND
20
20
19.6
19.8
98
99
70-142
1
30
Dibromochloromethane
ug/L
ND
20
20
19.6
18.0
98
90
68-138
8
30
Dibromomethane
ug/L
ND
20
20
20.7
19.6
103
98
70-134
5
30
Dichlorodifluoromethane
ug/L
ND
20
20
17.6
17.9
88
89
43-155
1
30 v3
Diisopropyl ether
ug/L
ND
20
20
17.8
17.8
89
89
65-146
0
30
Ethylbenzene
ug/L
ND
20
20
21.9
21.1
110
106
68-143
4
30
Hexachloro-1,3-butadiene
ug/L
ND
20
20
26.6
26.0
133
130
62-151
3
30 v1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC.
Page 90 of 122

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3585804
3585805
MS
MSD
92593947001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
m&p-Xylene
ug/L
ND
40
40
43.8
43.0
109
108
53-157
2
30
Methyl-tert-butyl ether
ug/L
ND
20
20
18.4
17.4
92
87
59-156
6
30
Methylene Chloride
ug/L
ND
20
20
17.5
18.5
88
93
64-148
5
30
Naphthalene
ug/L
ND
20
20
21.9
21.3
109
107
57-150
3
30
o-Xylene
ug/L
ND
20
20
21.1
21.0
105
105
68-143
1
30
p-Isopropyltoluene
ug/L
ND
20
20
23.5
22.7
118
113
70-141
4
30
Styrene
ug/L
ND
20
20
21.3
20.8
106
104
70-136
2
30
Tetrachloroethene
ug/L
ND
20
20
20.2
19.7
101
98
70-139
3
30
Toluene
ug/L
ND
20
20
20.4
20.0
102
100
47-157
2
30
trans-1,2-Dichloroethene
ug/L
ND
20
20
19.1
19.0
96
95
70-149
0
30
trans-1,3-Dichloropropene
ug/L
ND
20
20
20.8
19.5
104
98
70-138
6
30
Trichloroethene
ug/L
ND
20
20
21.1
20.5
105
103
70-149
3
30
Trichlorofluoromethane
ug/L
ND
20
20
19.7
18.8
99
94
61-154
5
30
Vinyl acetate
ug/L
ND
40
40
31.8
32.7
80
82
48-156
3
30
Vinyl chloride
ug/L
ND
20
20
20.0
19.7
100
99
55-172
1
30
Xylene (Total)
ug/L
ND
60
60
64.8
64.0
108
107
66-145
1
30
1,2-Dichloroethane-d4 (S)
%
100
106
70-130
4-Bromofluorobenzene (S)
%
100
100
70-130
Toluene-d8 (S)
%
97
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC.
Page 91 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
QC Batch: 686126 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92593947005, 92593947006
METHOD BLANK: 3587545
Associated Lab Samples: 92593947005, 92593947006
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.31
03/21/22 13:47
1,1,1-Trichloroethane
ug/L
ND
1.0
0.33
03/21/22 13:47
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
03/21/22 13:47
1,1,2-Trichloroethane
ug/L
ND
1.0
0.32
03/21/22 13:47
1,1-Dichloroethane
ug/L
ND
1.0
0.37
03/21/22 13:47
1,1-Dichloroethene
ug/L
ND
1.0
0.35
03/21/22 13:47
1,1-Dichloropropene
ug/L
ND
1.0
0.43
03/21/22 13:47
1,2,3-Trichlorobenzene
ug/L
ND
1.0
0.81
03/21/22 13:47
1,2,3-Trichloropropane
ug/L
ND
1.0
0.26
03/21/22 13:47
1,2,4-Trichlorobenzene
ug/L
ND
1.0
0.64
03/21/22 13:47
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
0.34
03/21/22 13:47
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
03/21/22 13:47
1,2-Dichlorobenzene
ug/L
ND
1.0
0.34
03/21/22 13:47
1,2-Dichloroethane
ug/L
ND
1.0
0.32
03/21/22 13:47
1,2-Dichloropropane
ug/L
ND
1.0
0.36
03/21/22 13:47
1,3-Dichlorobenzene
ug/L
ND
1.0
0.34
03/21/22 13:47
1,3-Dichloropropane
ug/L
ND
1.0
0.28
03/21/22 13:47
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
03/21/22 13:47
2,2-Dichloropropane
ug/L
ND
1.0
0.39
03/21/22 13:47
2-Butanone (MEK)
ug/L
ND
5.0
4.0
03/21/22 13:47
2-Chlorotoluene
ug/L
ND
1.0
0.32
03/21/22 13:47
2-Hexanone
ug/L
ND
5.0
0.48
03/21/22 13:47
4-Chlorotoluene
ug/L
ND
1.0
0.32
03/21/22 13:47
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
2.7
03/21/22 13:47
Acetone
ug/L
ND
25.0
5.1
03/21/22 13:47
Benzene
ug/L
ND
1.0
0.34
03/21/22 13:47
Bromobenzene
ug/L
ND
1.0
0.29
03/21/22 13:47
Bromochloromethane
ug/L
ND
1.0
0.47
03/21/22 13:47
Bromodichloromethane
ug/L
ND
1.0
0.31
03/21/22 13:47
Bromoform
ug/L
ND
1.0
0.34
03/21/22 13:47
Bromomethane
ug/L
ND
2.0
1.7
03/21/22 13:47
Carbon tetrachloride
ug/L
ND
1.0
0.33
03/21/22 13:47
Chlorobenzene
ug/L
ND
1.0
0.28
03/21/22 13:47
Chloroethane
ug/L
ND
1.0
0.65
03/21/22 13:47
Chloroform
ug/L
ND
1.0
0.43
03/21/22 13:47
Chloromethane
ug/L
ND
1.0
0.54
03/21/22 13:47
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.38
03/21/22 13:47
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.36
03/21/22 13:47
Dibromochloromethane
ug/L
ND
1.0
0.36
03/21/22 13:47
Dibromomethane
ug/L
ND
1.0
0.39
03/21/22 13:47
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC.
Page 92 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
METHOD BLANK: 3587545
Associated Lab Samples: 92593947005, 92593947006
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed Qualifiers
Dichlorodifluoromethane
ug/L
ND
1.0
0.35
03/21/22 13:47 v2
Diisopropyl ether
ug/L
ND
1.0
0.31
03/21/22 13:47
Ethylbenzene
ug/L
ND
1.0
0.30
03/21/22 13:47
Hexachloro-1,3-butadiene
ug/L
ND
2.0
1.5
03/21/22 13:47 v1
m&p-Xylene
ug/L
ND
2.0
0.71
03/21/22 13:47
Methyl-tert-butyl ether
ug/L
ND
1.0
0.42
03/21/22 13:47
Methylene Chloride
ug/L
ND
5.0
2.0
03/21/22 13:47
Naphthalene
ug/L
ND
1.0
0.64
03/21/22 13:47
o-Xylene
ug/L
ND
1.0
0.34
03/21/22 13:47
p-Isopropyltoluene
ug/L
ND
1.0
0.41
03/21/22 13:47
Styrene
ug/L
ND
1.0
0.29
03/21/22 13:47
Tetrachloroethene
ug/L
ND
1.0
0.29
03/21/22 13:47
Toluene
ug/L
ND
1.0
0.48
03/21/22 13:47
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.40
03/21/22 13:47
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.36
03/21/22 13:47
Trichloroethene
ug/L
ND
1.0
0.38
03/21/22 13:47
Trichlorofluoromethane
ug/L
ND
1.0
0.30
03/21/22 13:47
Vinyl acetate
ug/L
ND
2.0
1.3
03/21/22 13:47
Vinyl chloride
ug/L
ND
1.0
0.39
03/21/22 13:47
Xylene (Total)
ug/L
ND
1.0
0.34
03/21/22 13:47
1,2-Dichloroethane-d4 (S)
%
94
70-130
03/21/22 13:47
4-Bromofluorobenzene (S)
%
97
70-130
03/21/22 13:47
Toluene-d8 (S)
%
105
70-130
03/21/22 13:47
LABORATORY CONTROL SAMPLE:
3587546
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
50.2
100
70-130
1,1,1-Trichloroethane
ug/L
50
42.8
86
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
51.4
103
70-130
1,1,2-Trichloroethane
ug/L
50
48.3
97
70-130
1,1-Dichloroethane
ug/L
50
40.0
80
70-130
1,1-Dichloroethene
ug/L
50
41.6
83
70-132
1,1-Dichloropropene
ug/L
50
48.8
98
70-131
1,2,3-Trichlorobenzene
ug/L
50
52.3
105
70-134
1,2,3-Trichloropropane
ug/L
50
50.6
101
70-130
1,2,4-Trichlorobenzene
ug/L
50
52.2
104
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
50.3
101
70-132
1,2-Dibromoethane (EDB)
ug/L
50
52.6
105
70-130
1,2-Dichlorobenzene
ug/L
50
49.9
100
70-130
1,2-Dichloroethane
ug/L
50
47.5
95
70-130
1,2-Dichloropropane
ug/L
50
49.6
99
70-130
1,3-Dichlorobenzene
ug/L
50
50.1
100
70-130
1,3-Dichloropropane
ug/L
50
51.0
102
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 93 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
LABORATORY CONTROL SAMPLE:
Parameter
3587546
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,4-Dichlorobenzene
ug/L
50
49.7
99
70-130
2,2-Dichloropropane
ug/L
50
41.5
83
70-130
2-Butanone (MEK)
ug/L
100
84.3
84
70-133
2-Chlorotoluene
ug/L
50
51.0
102
70-130
2-Hexanone
ug/L
100
107
107
70-130
4-Chlorotoluene
ug/L
50
48.0
96
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
96.2
96
70-130
Acetone
ug/L
100
84.9
85
70-144
Benzene
ug/L
50
45.7
91
70-130
Bromobenzene
ug/L
50
49.5
99
70-130
Bromochloromethane
ug/L
50
44.8
90
70-130
Bromodichloromethane
ug/L
50
46.1
92
70-130
Bromoform
ug/L
50
50.5
101
70-131
Bromomethane
ug/L
50
43.0
86
30-177
Carbon tetrachloride
ug/L
50
41.7
83
70-130
Chlorobenzene
ug/L
50
46.9
94
70-130
Chloroethane
ug/L
50
62.7
125
46-131
Chloroform
ug/L
50
44.8
90
70-130
Chloromethane
ug/L
50
39.5
79
49-130
cis-1,2-Dichloroethene
ug/L
50
43.2
86
70-130
cis-1,3-Dichloropropene
ug/L
50
48.1
96
70-130
Dibromochloromethane
ug/L
50
48.7
97
70-130
Dibromomethane
ug/L
50
43.8
88
70-130
Dichlorodifluoromethane
ug/L
50
36.4
73
52-134 v3
Diisopropyl ether
ug/L
50
45.1
90
70-131
Ethylbenzene
ug/L
50
48.5
97
70-130
Hexachloro-1,3-butadiene
ug/L
50
61.6
123
70-131 v1
m&p-Xylene
ug/L
100
96.6
97
70-130
Methyl-tert-butyl ether
ug/L
50
46.0
92
70-130
Methylene Chloride
ug/L
50
39.8
80
68-130
Naphthalene
ug/L
50
52.1
104
70-133
o-Xylene
ug/L
50
46.9
94
70-130
p-Isopropyltoluene
ug/L
50
53.5
107
70-130
Styrene
ug/L
50
48.8
98
70-130
Tetrachloroethene
ug/L
50
46.1
92
70-130
Toluene
ug/L
50
43.9
88
70-130
trans-1,2-Dichloroethene
ug/L
50
42.6
85
70-130
trans- 1,3-Dichloropropene
ug/L
50
47.9
96
70-130
Trichloroethene
ug/L
50
48.5
97
70-130
Trichlorofluoromethane
ug/L
50
44.2
88
61-130
Vinyl acetate
ug/L
100
79.4
79
70-140
Vinyl chloride
ug/L
50
42.4
85
59-142
Xylene (Total)
ug/L
150
144
96
70-130
1,2-Dichloroethane-d4 (S)
%
106
70-130
4-Bromofluorobenzene (S)
%
98
70-130
Toluene-d8 (S)
%
95
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 94 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3587547
MS
92594153011 Spike
Parameter Units Result Conc.
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1, 2,2-Tetrachloroethane
1,1, 2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2-Dibromo-3-
chloropropane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone
(MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
3587548
MSD
Spike MS MSD MS MSD % Rec
Conc. Result Result % Rec % Rec Limits
ug/L
ND
1000
1000
990
948
99
95
70-135
ug/L
ND
1000
1000
978
908
98
91
70-148
ug/L
ND
1000
1000
1000
999
100
100
70-131
ug/L
ND
1000
1000
995
979
100
98
70-136
ug/L
ND
1000
1000
943
946
94
95
70-147
ug/L
ND
1000
1000
1000
925
100
93
70-158
ug/L
ND
1000
1000
1070
1010
107
101
70-149
ug/L
ND
1000
1000
1040
1020
104
102
68-140
ug/L
ND
1000
1000
1010
1000
101
100
67-137
ug/L
ND
1000
1000
1050
1050
105
105
70-139
ug/L
ND
1000
1000
874
904
87
90
69-136
Max
RPD RPD Qual
4 30
7 30
0 30
2 30
0 30
8 30
7 30
2 30
0 30
1 30
3 30
ug/L
ND
1000
1000
1030
970
103
97
70-137
6
30
ug/L
ND
1000
1000
1040
997
104
100
70-133
4
30
ug/L
ND
1000
1000
985
976
98
98
67-138
1
30
ug/L
ND
1000
1000
1080
997
108
100
70-138
8
30
ug/L
ND
1000
1000
1020
1050
102
105
70-133
3
30
ug/L
ND
1000
1000
995
979
100
98
70-136
2
30
ug/L
ND
1000
1000
1040
1040
104
104
70-133
0
30
ug/L
ND
1000
1000
945
903
95
90
52-155
5
30
ug/L
ND
2000
2000
1560
1720
78
86
61-147
9
30
ug/L
ND
1000
1000
1010
1020
101
102
70-141
1
30
ug/L
ND
2000
2000
1780
1860
89
93
67-139
5
30
ug/L
ND
1000
1000
987
986
99
99
70-135
0
30
ug/L
ND
2000
2000
1770
1790
88
89
67-136
1
30
ug/L
ND
2000
2000
1810
1870
91
93
55-159
3
30
ug/L
ND
1000
1000
968
943
97
94
67-150
3
30
ug/L
ND
1000
1000
995
974
100
97
70-134
2
30
ug/L
ND
1000
1000
986
958
99
96
70-146
3
30
ug/L
ND
1000
1000
933
934
93
93
70-138
0
30
ug/L
ND
1000
1000
940
896
94
90
57-138
5
30
ug/L
ND
1000
1000
950
955
95
96
10-200
1
30
ug/L
ND
1000
1000
911
943
91
94
70-147
3
30
ug/L
ND
1000
1000
986
967
99
97
70-137
2
30
ug/L
ND
1000
1000
1360
1310
136
131
51-166
3
30
ug/L
ND
1000
1000
1000
871
100
87
70-144
14
30
ug/L
ND
1000
1000
948
944
95
94
24-161
0
30
ug/L
89.2
1000
1000
1090
1020
101
93
67-148
7
30
ug/L
ND
1000
1000
941
916
94
92
70-142
3
30
ug/L
ND
1000
1000
933
889
93
89
68-138
5
30
ug/L
ND
1000
1000
964
923
96
92
70-134
4
30
ug/L
ND
1000
1000
878
828
88
83
43-155
6
30 v3
ug/L
ND
1000
1000
921
927
92
93
65-146
1
30
ug/L
ND
1000
1000
997
971
100
97
68-143
3
30
ug/L
ND
1000
1000
1300
1270
130
127
62-151
2
30 v1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3587547
3587548
MS
MSD
92594153011
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
m&p-Xylene
ug/L
ND
2000
2000
2060
1960
103
98
53-157
5
30
Methyl-tert-butyl ether
ug/L
ND
1000
1000
957
926
96
93
59-156
3
30
Methylene Chloride
ug/L
ND
1000
1000
1040
1020
104
102
64-148
2
30
Naphthalene
ug/L
ND
1000
1000
977
990
98
99
57-150
1
30
o-Xylene
ug/L
ND
1000
1000
978
971
98
97
68-143
1
30
p-Isopropyltoluene
ug/L
ND
1000
1000
1120
1100
112
110
70-141
2
30
Styrene
ug/L
ND
1000
1000
1020
954
102
95
70-136
7
30
Tetrachloroethene
ug/L
4720
1000
1000
5590
5380
86
66
70-139
4
30 M1
Toluene
ug/L
ND
1000
1000
941
925
94
93
47-157
2
30
trans-1,2-Dichloroethene
ug/L
ND
1000
1000
968
979
97
98
70-149
1
30
trans-1,3-Dichloropropene
ug/L
ND
1000
1000
942
919
94
92
70-138
2
30
Trichloroethene
ug/L
393
1000
1000
1560
1460
116
106
70-149
7
30
Trichlorofluoromethane
ug/L
ND
1000
1000
998
959
100
96
61-154
4
30
Vinyl acetate
ug/L
ND
2000
2000
1570
1620
78
81
48-156
3
30
Vinyl chloride
ug/L
ND
1000
1000
1020
942
102
94
55-172
8
30
Xylene (Total)
ug/L
ND
3000
3000
3030
2930
101
98
66-145
4
30
1,2-Dichloroethane-d4 (S)
%
100
101
70-130
4-Bromofluorobenzene (S)
%
100
100
70-130
Toluene-d8 (S)
%
99
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC.
Page 96 of 122

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
QC Batch: 685634 Analysis Method: EPA 8270E
QC Batch Method: EPA 3510C Analysis Description: 8270E Water MSSV RVE
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92593947001, 92593947002, 92593947003, 92593947004, 92593947005
METHOD BLANK: 3585376 Matrix: Water
Associated Lab Samples: 92593947001, 92593947002, 92593947003, 92593947004, 92593947005
Blank Reporting
Parameter Units Result Limit MDL
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
10.0
1.7
03/18/22 11:35
1,2-Dichlorobenzene
ug/L
ND
10.0
1.8
03/18/22 11:35
1,3-Dichlorobenzene
ug/L
ND
10.0
1.6
03/18/22 11:35
1,4-Dichlorobenzene
ug/L
ND
10.0
1.7
03/18/22 11:35
1-Methylnaphthalene
ug/L
ND
10.0
2.0
03/18/22 11:35
2,2'-Oxybis(1-chloropropane)
ug/L
ND
10.0
1.2
03/18/22 11:35
2,4,5-Trichlorophenol
ug/L
ND
10.0
1.4
03/18/22 11:35
2,4,6-Trichlorophenol
ug/L
ND
10.0
1.6
03/18/22 11:35
2,4-Dichlorophenol
ug/L
ND
10.0
1.4
03/18/22 11:35
2,4-Dimethylphenol
ug/L
ND
10.0
1.7
03/18/22 11:35
2,4-Dinitrophenol
ug/L
ND
50.0
26.0
03/18/22 11:35
2,4-Dinitrotoluene
ug/L
ND
10.0
1.6
03/18/22 11:35
2,6-Dinitrotoluene
ug/L
ND
10.0
1.7
03/18/22 11:35
2-Chloronaphthalene
ug/L
ND
10.0
1.7
03/18/22 11:35
2-Chlorophenol
ug/L
ND
10.0
1.2
03/18/22 11:35
2-Methylnaphthalene
ug/L
ND
10.0
1.9
03/18/22 11:35
2-Methylphenol(o-Cresol)
ug/L
ND
10.0
1.9
03/18/22 11:35
2-Nitroaniline
ug/L
ND
20.0
3.0
03/18/22 11:35
2-Nitrophenol
ug/L
ND
10.0
1.4
03/18/22 11:35
3&4-Methyl phenol (m&p Cresol)
ug/L
ND
10.0
1.2
03/18/22 11:35
3,3'-Dichlorobenzidine
ug/L
ND
20.0
8.1
03/18/22 11:35
3-Nitroaniline
ug/L
ND
20.0
3.8
03/18/22 11:35
4,6-Dinitro-2-methyl phenol
ug/L
ND
20.0
3.4
03/18/22 11:35
4-Bromophenylphenyl ether
ug/L
ND
10.0
1.8
03/18/22 11:35
4-Chloro-3-methyl phenol
ug/L
ND
10.0
3.3
03/18/22 11:35
4-Chloroaniline
ug/L
ND
20.0
3.6
03/18/22 11:35
4-Chlorophenylphenyl ether
ug/L
ND
10.0
2.0
03/18/22 11:35
4-Nitroaniline
ug/L
ND
20.0
5.1
03/18/22 11:35
4-Nitrophenol
ug/L
ND
50.0
6.6
03/18/22 11:35
Acenaphthene
ug/L
ND
10.0
2.0
03/18/22 11:35
Acenaphthylene
ug/L
ND
10.0
2.0
03/18/22 11:35
Aniline
ug/L
ND
10.0
1.6
03/18/22 11:35
Anthracene
ug/L
ND
10.0
2.3
03/18/22 11:35
Benzo(a)anthracene
ug/L
ND
10.0
2.7
03/18/22 11:35
Benzo(a)pyrene
ug/L
ND
10.0
2.8
03/18/22 11:35
Benzo(b)fluoranthene
ug/L
ND
10.0
2.6
03/18/22 11:35
Benzo(g,h,i)perylene
ug/L
ND
10.0
2.8
03/18/22 11:35
Benzo(k)fluoranthene
ug/L
ND
10.0
2.7
03/18/22 11:35
Benzoic Acid
ug/L
ND
50.0
3.4
03/18/22 11:35
Benzyl alcohol
ug/L
ND
20.0
2.9
03/18/22 11:35
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 97 of 122

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
METHOD BLANK: 3585376 Matrix: Water
Associated Lab Samples: 92593947001, 92593947002, 92593947003, 92593947004, 92593947005
Blank Reporting
Parameter Units Result Limit MDL
Analyzed
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
1.8
03/18/22 11:35
bis(2-Chloroethyl) ether
ug/L
ND
10.0
1.9
03/18/22 11:35
bis(2-Ethylhexyl)phthalate
ug/L
ND
6.0
3.7
03/18/22 11:35
Butylbenzylphthalate
ug/L
ND
10.0
3.1
03/18/22 11:35
Chrysene
ug/L
ND
10.0
2.8
03/18/22 11:35
Di-n-butylphthalate
ug/L
ND
10.0
2.2
03/18/22 11:35
Di-n-octylphthalate
ug/L
ND
10.0
3.9
03/18/22 11:35
Dibenz(a,h)anthracene
ug/L
ND
10.0
3.0
03/18/22 11:35
Dibenzofuran
ug/L
ND
10.0
2.1
03/18/22 11:35
Diethylphthalate
ug/L
ND
10.0
2.0
03/18/22 11:35
Dimethylphthalate
ug/L
ND
10.0
2.1
03/18/22 11:35
Fluoranthene
ug/L
ND
10.0
2.2
03/18/22 11:35
Fluorene
ug/L
ND
10.0
2.1
03/18/22 11:35
Hexachloro-1,3-butadiene
ug/L
ND
10.0
1.8
03/18/22 11:35
Hexachlorobenzene
ug/L
ND
10.0
2.2
03/18/22 11:35
Hexachlorocyclopentadiene
ug/L
ND
10.0
1.6
03/18/22 11:35
Hexachloroethane
ug/L
ND
10.0
1.4
03/18/22 11:35
Indeno(1,2,3-cd)pyrene
ug/L
ND
10.0
2.9
03/18/22 11:35
Isophorone
ug/L
ND
10.0
1.7
03/18/22 11:35
N-Nitroso-di-n-propylamine
ug/L
ND
10.0
1.3
03/18/22 11:35
N-Nitrosodimethylamine
ug/L
ND
10.0
1.9
03/18/22 11:35
N-Nitrosodiphenylamine
ug/L
ND
10.0
3.0
03/18/22 11:35
Naphthalene
ug/L
ND
10.0
2.1
03/18/22 11:35
Nitrobenzene
ug/L
ND
10.0
1.9
03/18/22 11:35
Pentachlorophenol
ug/L
ND
20.0
3.8
03/18/22 11:35
Phenanthrene
ug/L
ND
10.0
2.0
03/18/22 11:35
Phenol
ug/L
ND
10.0
1.4
03/18/22 11:35
Pyrene
ug/L
ND
10.0
2.2
03/18/22 11:35
2,4,6-Tribromophenol (S)
%
104
10-144
03/18/22 11:35
2-Fluorobiphenyl (S)
%
91
10-130
03/18/22 11:35
2-Fluorophenol (S)
%
84
10-130
03/18/22 11:35
Nitrobenzene-d5 (S)
%
100
10-144
03/18/22 11:35
Phenol-d6 (S)
%
65
10-130
03/18/22 11:35
Terphenyl-d14 (S)
%
102
34-163
03/18/22 11:35
Qualifiers
LABORATORY CONTROL SAMPLE:
3585377
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
36.6
73
18-130
1,2-Dichlorobenzene
ug/L
50
36.1
72
20-130
1,3-Dichlorobenzene
ug/L
50
33.7
67
18-130
1,4-Dichlorobenzene
ug/L
50
34.8
70
18-130
1-Methylnaphthalene
ug/L
50
44.5
89
29-130
2,2'-Oxybis(1-chloropropane)
ug/L
50
46.6
93
28-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 98 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
LABORATORY CONTROL SAMPLE:
Parameter
3585377
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,4,5-Trichlorophenol
ug/L
50
50.4
101
35-130
2,4,6-Trichlorophenol
ug/L
50
51.8
104
31-130
2,4-Dichlorophenol
ug/L
50
47.3
95
35-130
2,4-Dimethylphenol
ug/L
50
53.5
107
34-130
2,4-Dinitrophenol
ug/L
250
190
76
10-153
2,4-Dinitrotoluene
ug/L
50
49.6
99
37-136
2,6-Dinitrotoluene
ug/L
50
48.4
97
33-136
2-Chloronaphthalene
ug/L
50
46.5
93
26-130
2-Chlorophenol
ug/L
50
46.5
93
37-130
2-Methylnaphthalene
ug/L
50
44.1
88
29-130
2-Methylphenol(o-Cresol)
ug/L
50
45.9
92
35-130
2-Nitroaniline
ug/L
100
106
106
37-130
2-Nitrophenol
ug/L
50
55.8
112
32-130
3&4-Methyl phenol (m&p Cresol)
ug/L
50
45.1
90
34-130
3,3'-Dichlorobenzidine
ug/L
100
89.7
90
34-136
3-Nitroaniline
ug/L
100
104
104
37-138
4,6-Dinitro-2-methyl phenol
ug/L
100
100
100
21-157
4-Bromophenylphenyl ether
ug/L
50
46.7
93
38-130
4-Chloro-3-methyl phenol
ug/L
100
97.6
98
37-130
4-Chloroaniline
ug/L
100
91.0
91
38-130
4-Chlorophenylphenyl ether
ug/L
50
45.6
91
33-130
4-Nitroaniline
ug/L
100
89.2
89
42-137
4-Nitrophenol
ug/L
250
162
65
10-130
Acenaphthene
ug/L
50
48.9
98
33-130
Acenaphthylene
ug/L
50
48.3
97
35-130
Aniline
ug/L
50
42.3
85
22-130
Anthracene
ug/L
50
48.5
97
48-130
Benzo(a)anthracene
ug/L
50
49.9
100
48-137
Benzo(a)pyrene
ug/L
50
56.6
113
49-138
Benzo(b)fluoranthene
ug/L
50
55.2
110
52-138
Benzo(g,h,i)perylene
ug/L
50
59.7
119
48-140
Benzo(k)fluoranthene
ug/L
50
56.8
114
48-139
Benzoic Acid
ug/L
250
79.6
32
10-130
Benzyl alcohol
ug/L
100
89.6
90
35-130
bis(2-Chloroethoxy)methane
ug/L
50
49.4
99
34-130
bis(2-Chloroethyl) ether
ug/L
50
47.9
96
36-130
bis(2-Ethylhexyl)phthalate
ug/L
50
56.7
113
32-165
Butylbenzylphthalate
ug/L
50
59.9
120
34-161
Chrysene
ug/L
50
50.7
101
47-131
Di-n-butylphthalate
ug/L
50
49.6
99
39-144
Di-n-octylphthalate
ug/L
50
56.4
113
30-170
Dibenz(a,h)anthracene
ug/L
50
55.5
111
49-138
Dibenzofuran
ug/L
50
48.0
96
33-130
Diethylphthalate
ug/L
50
46.1
92
38-131
Dimethylphthalate
ug/L
50
46.2
92
37-130
Fluoranthene
ug/L
50
44.9
90
46-137
Fluorene
ug/L
50
47.5
95
37-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 99 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
LABORATORY CONTROL SAMPLE:
Parameter
3585377
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Hexachloro-1,3-butadiene
ug/L
50
33.0
66
11-130
Hexachlorobenzene
ug/L
50
43.9
88
38-130
Hexachlorocyclopentadiene
ug/L
50
36.8
74
10-130
Hexachloroethane
ug/L
50
34.1
68
14-130
Indeno(1,2,3-cd)pyrene
ug/L
50
55.2
110
41-130
Isophorone
ug/L
50
45.9
92
33-130
N-Nitroso-di-n-propylamine
ug/L
50
45.6
91
36-130
N-Nitrosodimethylamine
ug/L
50
43.0
86
34-130
N-Nitrosodiphenylamine
ug/L
50
49.3
99
37-130
Naphthalene
ug/L
50
42.7
85
30-130
Nitrobenzene
ug/L
50
47.4
95
36-130
Pentachlorophenol
ug/L
100
94.1
94
23-149
Phenanthrene
ug/L
50
49.4
99
44-130
Phenol
ug/L
50
36.3
73
18-130
Pyrene
ug/L
50
55.1
110
47-134
2,4,6-Tribromophenol (S)
%
124
10-144
2-Fluorobiphenyl (S)
%
99
10-130
2-Fluorophenol (S)
%
92
10-130
Nitrobenzene-d5 (S)
%
114
10-144
Phenol-d6 (S)
%
70
10-130
Terphenyl-d14 (S)
%
116
34-163
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3585378
MS
92593653003 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3585379
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,2,4-Trichoorobenzene
ug/L
ND
50
50
34.5
31.7
69
63
10-130
9
30
1,2-Dichlorobenzene
ug/L
ND
50
50
49.2
44.9
98
90
10-130
9
30
1,3-Dichlorobenzene
ug/L
ND
50
50
30.3
26.4
61
53
10-130
14
30
1,4-Dichlorobenzene
ug/L
ND
50
50
31.0
27.2
62
54
10-130
13
30
1-Methyl naphthalene
ug/L
ND
50
50
38.2
34.8
76
70
10-130
9
30
2,2'-Oxybis(1-
ug/L
ND
50
50
33.8
33.0
68
66
12-142
2
30
chloropropane)
2,4,5-Trichlorophenol
ug/L
ND
50
50
53.2
43.4
106
87
10-143
20
30
2,4,6-Trichlorophenol
ug/L
ND
50
50
48.4
40.7
97
81
10-147
17
30
2,4-Dichlorophenol
ug/L
ND
50
50
40.5
34.2
81
68
10-138
17
30
2,4-Dimethylphenol
ug/L
ND
50
50
9.11
6.7J
18
13
25-130
30 M1
2,4-Dinitrophenol
ug/L
ND
250
250
248
62.5
99
25
10-165
119
30 R1
2,4-Dinitrotoluene
ug/L
ND
50
50
49.9
41.1
100
82
29-148
19
30
2,6-Dinitrotoluene
ug/L
ND
50
50
45.9
39.9
92
80
26-146
14
30
2-Chloronaphthalene
ug/L
ND
50
50
37.4
36.6
75
73
11-130
2
30
2-Chlorophenol
ug/L
ND
50
50
33.4
31.2
67
62
10-133
7
30
2-Methyl naphthalene
ug/L
ND
50
50
37.4
34.8
75
70
13-130
7
30
2-Methyl phenol(o-Cresol)
ug/L
ND
50
50
27.1
24.5
54
49
20-130
10
30
2-Nitroaniline
ug/L
ND
100
100
17.9J
30.5
18
30
24-136
30 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC.
Page 100 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3585378
MS
92593653003 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3585379
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
2-Nitrophenol
ug/L
ND
50
50
49.7
43.8
99
88
10-153
13
30
3&4-Methylphenol(m&p
ug/L
ND
50
50
26.9
24.4
54
49
16-130
10
30
Cresol)
3,3'-Dichlorobenzidine
ug/L
ND
100
100
ND
ND
0
0
10-153
30 M1
3-Nitroaniline
ug/L
ND
100
100
18.9J
31.8
19
32
22-151
30 M1
4,6-Dinitro-2-methylphenol
ug/L
ND
100
100
95.7
58.0
96
58
10-180
49
30 R1
4-Bromophenylphenyl ether
ug/L
ND
50
50
45.6
39.7
91
79
25-130
14
30
4-Chloro-3-methylphenol
ug/L
ND
100
100
85.5
67.3
86
67
25-133
24
30
4-Chloroaniline
ug/L
ND
100
100
ND
ND
0
0
14-132
30 M1
4-Chlorophenylphenyl ether
ug/L
ND
50
50
44.8
41.2
90
82
19-130
8
30
4-Nitroaniline
ug/L
ND
100
100
ND
ND
0
0
29-150
30 M1
4-Nitrophenol
ug/L
ND
250
250
197
115
79
46
10-130
53
30 R1
Acenaphthene
ug/L
ND
50
50
38.3
36.5
77
73
16-130
5
30
Acenaphthylene
ug/L
ND
50
50
34.7
33.6
69
67
15-137
3
30
Aniline
ug/L
ND
50
50
ND
ND
0
0
10-130
30 M1
Anthracene
ug/L
ND
50
50
40.3
33.4
81
67
37-136
19
30
Benzo(a)anth race ne
ug/L
ND
50
50
47.6
41.0
95
82
40-145
15
30
Benzo(a)pyrene
ug/L
ND
50
50
47.1
39.2
94
78
41-146
18
30
Benzo(b)fluoranthene
ug/L
ND
50
50
52.9
46.6
106
93
39-151
13
30
Benzo(g,h,i)perylene
ug/L
ND
50
50
58.1
50.2
116
100
40-147
15
30
Benzo(k)fluoranthene
ug/L
ND
50
50
51.9
44.6
104
89
40-146
15
30
Benzoic Acid
ug/L
ND
250
250
154
14.1J
62
6
10-130
30 M1
Benzyl alcohol
ug/L
ND
100
100
66.4
60.9
66
61
25-130
9
30
bis(2-
ug/L
ND
50
50
40.2
37.1
80
74
23-130
8
30
Chloroethoxy)methane
bis(2-Chloroethyl) ether
ug/L
ND
50
50
35.3
33.6
71
67
25-130
5
30
bis(2- Ethyl hexyl)phthalate
ug/L
ND
50
50
53.7
46.9
103
89
28-166
13
30
Butylbenzylphthalate
ug/L
ND
50
50
53.0
44.3
106
89
33-165
18
30
Chrysene
ug/L
ND
50
50
48.1
42.2
96
84
38-141
13
30
Di-n-butylphthalate
ug/L
ND
50
50
50.3
43.6
101
87
32-153
14
30
Di-n-octylphthalate
ug/L
ND
50
50
57.5
48.9
115
98
30-175
16
30 v1
Dibenz(a,h)anthracene
ug/L
ND
50
50
57.8
50.2
116
100
39-148
14
30
Dibenzofuran
ug/L
ND
50
50
40.6
38.4
81
77
20-130
6
30
Diethylphthalate
ug/L
ND
50
50
48.0
40.7
96
81
28-142
16
30
Dimethylphthalate
ug/L
ND
50
50
45.5
39.9
91
80
26-136
13
30
Fluoranthene
ug/L
ND
50
50
51.9
44.4
104
89
39-143
16
30
Fluorene
ug/L
ND
50
50
43.0
39.6
86
79
24-132
8
30
Hexachloro-1,3-butadiene
ug/L
ND
50
50
32.3
30.4
65
61
10-130
6
30
Hexachlorobenzene
ug/L
ND
50
50
42.6
36.8
85
74
29-130
15
30
Hexachlorocyclopentadiene
ug/L
ND
50
50
33.8
33.3
68
67
10-130
1
30
Hexachloroethane
ug/L
ND
50
50
28.1
25.8
56
52
10-130
9
30
Indeno(1,2,3-cd)pyrene
ug/L
ND
50
50
56.3
49.2
113
98
39-148
13
30
Isophorone
ug/L
ND
50
50
38.3
35.6
77
71
23-130
7
30
N-Nitroso-di-n-propylamine
ug/L
ND
50
50
36.3
33.6
73
67
25-130
8
30
N-Nitrosodimethylamine
ug/L
ND
50
50
39.9
35.8
80
72
22-130
11
30
N-Nitrosodiphenylamine
ug/L
ND
50
50
38.4
34.2
77
68
26-134
12
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC.
Page 101 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3585378
3585379
MS
MSD
92593653003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Naphthalene
ug/L
ND
50
50
37.8
33.6
76
67
14-130
12
30
Nitrobenzene
ug/L
ND
50
50
111
103
222
206
25-130
8
30 M1
Pentachlorophenol
ug/L
ND
100
100
97.0
56.9
97
57
10-175
52
30 R1
Phenanthrene
ug/L
ND
50
50
45.1
38.3
90
77
36-133
16
30
Phenol
ug/L
ND
50
50
22.4
20.0
45
40
10-130
11
30
Pyrene
ug/L
ND
50
50
47.9
40.9
96
82
40-143
16
30
2,4,6-Tribromophenol (S)
%
110
87
10-144
2-Fluorobiphenyl (S)
%
76
77
10-130
2-Fluorophenol(S)
%
58
53
10-130
Nitrobenzene-d5(S)
%
83
79
10-144
Phenol-d6 (S)
%
49
41
10-130
Terphenyl-d14(S)
%
100
87
34-163
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC.
Page 102 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
QC Batch: 686047 Analysis Method: EPA 8270E
QC Batch Method: EPA 3510C Analysis Description: 8270E Water MSSV RVE
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92593947006
METHOD BLANK: 3587099
Associated Lab Samples: 92593947006
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
10.0
1.7
03/21/22 16:10
1,2-Dichlorobenzene
ug/L
ND
10.0
1.8
03/21/22 16:10
1,3-Dichlorobenzene
ug/L
ND
10.0
1.6
03/21/22 16:10
1,4-Dichlorobenzene
ug/L
ND
10.0
1.7
03/21/22 16:10
1-Methylnaphthalene
ug/L
ND
10.0
2.0
03/21/22 16:10
2,2'-Oxybis(1-chloropropane)
ug/L
ND
10.0
1.2
03/21/22 16:10
2,4,5-Trichlorophenol
ug/L
ND
10.0
1.4
03/21/22 16:10
2,4,6-Trichlorophenol
ug/L
ND
10.0
1.6
03/21/22 16:10
2,4-Dichlorophenol
ug/L
ND
10.0
1.4
03/21/22 16:10
2,4-Dimethylphenol
ug/L
ND
10.0
1.7
03/21/22 16:10
2,4-Dinitrophenol
ug/L
ND
50.0
26.0
03/21/22 16:10
2,4-Dinitrotoluene
ug/L
ND
10.0
1.6
03/21/22 16:10
2,6-Dinitrotoluene
ug/L
ND
10.0
1.7
03/21/22 16:10
2-Chloronaphthalene
ug/L
ND
10.0
1.7
03/21/22 16:10
2-Chlorophenol
ug/L
ND
10.0
1.2
03/21/22 16:10
2-Methylnaphthalene
ug/L
ND
10.0
1.9
03/21/22 16:10
2-Methylphenol(o-Cresol)
ug/L
ND
10.0
1.9
03/21/22 16:10
2-Nitroaniline
ug/L
ND
20.0
3.0
03/21/22 16:10
2-Nitrophenol
ug/L
ND
10.0
1.4
03/21/22 16:10
3&4-Methyl phenol (m&p Cresol)
ug/L
ND
10.0
1.2
03/21/22 16:10
3,3'-Dichlorobenzidine
ug/L
ND
20.0
8.1
03/21/22 16:10
3-Nitroaniline
ug/L
ND
20.0
3.8
03/21/22 16:10
4,6-Dinitro-2-methyl phenol
ug/L
ND
20.0
3.4
03/21/22 16:10
4-Bromophenylphenyl ether
ug/L
ND
10.0
1.8
03/21/22 16:10
4-Chloro-3-methyl phenol
ug/L
ND
10.0
3.3
03/21/22 16:10
4-Chloroaniline
ug/L
ND
20.0
3.6
03/21/22 16:10
4-Chlorophenylphenyl ether
ug/L
ND
10.0
2.0
03/21/22 16:10
4-Nitroaniline
ug/L
ND
20.0
5.1
03/21/22 16:10
4-Nitrophenol
ug/L
ND
50.0
6.6
03/21/22 16:10
Acenaphthene
ug/L
ND
10.0
2.0
03/21/22 16:10
Acenaphthylene
ug/L
ND
10.0
2.0
03/21/22 16:10
Aniline
ug/L
ND
10.0
1.6
03/21/22 16:10
Anthracene
ug/L
ND
10.0
2.3
03/21/22 16:10
Benzo(a)anthracene
ug/L
ND
10.0
2.7
03/21/22 16:10
Benzo(a)pyrene
ug/L
ND
10.0
2.8
03/21/22 16:10
Benzo(b)fluoranthene
ug/L
ND
10.0
2.6
03/21/22 16:10
Benzo(g,h,i)perylene
ug/L
ND
10.0
2.8
03/21/22 16:10
Benzo(k)fluoranthene
ug/L
ND
10.0
2.7
03/21/22 16:10
Benzoic Acid
ug/L
ND
50.0
3.4
03/21/22 16:10
Benzyl alcohol
ug/L
ND
20.0
2.9
03/21/22 16:10
v1
IL
v1
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 103 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
METHOD BLANK: 3587099
Associated Lab Samples: 92593947006
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
1.8
03/21/22 16:10
bis(2-Chloroethyl) ether
ug/L
ND
10.0
1.9
03/21/22 16:10
bis(2-Ethylhexyl)phthalate
ug/L
ND
6.0
3.7
03/21/22 16:10
Butylbenzylphthalate
ug/L
ND
10.0
3.1
03/21/22 16:10
Chrysene
ug/L
ND
10.0
2.8
03/21/22 16:10
Di-n-butylphthalate
ug/L
ND
10.0
2.2
03/21/22 16:10
Di-n-octylphthalate
ug/L
ND
10.0
3.9
03/21/22 16:10
Dibenz(a,h)anthracene
ug/L
ND
10.0
3.0
03/21/22 16:10
Dibenzofuran
ug/L
ND
10.0
2.1
03/21/22 16:10
Diethylphthalate
ug/L
ND
10.0
2.0
03/21/22 16:10
Dimethylphthalate
ug/L
ND
10.0
2.1
03/21/22 16:10
Fluoranthene
ug/L
ND
10.0
2.2
03/21/22 16:10
Fluorene
ug/L
ND
10.0
2.1
03/21/22 16:10
Hexachloro-1,3-butadiene
ug/L
ND
10.0
1.8
03/21/22 16:10
Hexachlorobenzene
ug/L
ND
10.0
2.2
03/21/22 16:10
Hexachlorocyclopentadiene
ug/L
ND
10.0
1.6
03/21/22 16:10
Hexachloroethane
ug/L
ND
10.0
1.4
03/21/22 16:10
Indeno(1,2,3-cd)pyrene
ug/L
ND
10.0
2.9
03/21/22 16:10
Isophorone
ug/L
ND
10.0
1.7
03/21/22 16:10
N-Nitroso-di-n-propylamine
ug/L
ND
10.0
1.3
03/21/22 16:10
N-Nitrosodimethylamine
ug/L
ND
10.0
1.9
03/21/22 16:10
N-Nitrosodiphenylamine
ug/L
ND
10.0
3.0
03/21/22 16:10
Naphthalene
ug/L
ND
10.0
2.1
03/21/22 16:10
Nitrobenzene
ug/L
ND
10.0
1.9
03/21/22 16:10
Pentachlorophenol
ug/L
ND
20.0
3.8
03/21/22 16:10
Phenanthrene
ug/L
ND
10.0
2.0
03/21/22 16:10
Phenol
ug/L
ND
10.0
1.4
03/21/22 16:10
Pyrene
ug/L
ND
10.0
2.2
03/21/22 16:10
2,4,6-Tribromophenol (S)
%
65
10-144
03/21/22 16:10
2-Fluorobiphenyl (S)
%
62
10-130
03/21/22 16:10
2-Fluorophenol (S)
%
59
10-130
03/21/22 16:10
Nitrobenzene-d5 (S)
%
70
10-144
03/21/22 16:10
Phenol-d6 (S)
%
47
10-130
03/21/22 16:10
Terphenyl-d14 (S)
%
73
34-163
03/21/22 16:10
Qualifiers
LABORATORY CONTROL SAMPLE:
3587100
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
23.0
46
18-130
1,2-Dichlorobenzene
ug/L
50
22.7
45
20-130
1,3-Dichlorobenzene
ug/L
50
21.7
43
18-130
1,4-Dichlorobenzene
ug/L
50
22.0
44
18-130
1-Methylnaphthalene
ug/L
50
26.7
53
29-130
2,2'-Oxybis(1-chloropropane)
ug/L
50
30.1
60
28-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 104 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
LABORATORY CONTROL SAMPLE:
Parameter
3587100
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,4,5-Trichlorophenol
ug/L
50
35.9
72
35-130
2,4,6-Trichlorophenol
ug/L
50
35.1
70
31-130
2,4-Dichlorophenol
ug/L
50
33.9
68
35-130
2,4-Dimethylphenol
ug/L
50
30.5
61
34-130
2,4-Dinitrophenol
ug/L
250
168
67
10-153 v1
2,4-Dinitrotoluene
ug/L
50
36.0
72
37-136
2,6-Dinitrotoluene
ug/L
50
34.5
69
33-136
2-Chloronaphthalene
ug/L
50
26.8
54
26-130
2-Chlorophenol
ug/L
50
32.2
64
37-130
2-Methylnaphthalene
ug/L
50
26.3
53
29-130
2-Methylphenol(o-Cresol)
ug/L
50
33.7
67
35-130
2-Nitroaniline
ug/L
100
71.1
71
37-130
2-Nitrophenol
ug/L
50
34.1
68
32-130
3&4-Methyl phenol (m&p Cresol)
ug/L
50
32.8
66
34-130
3,3'-Dichlorobenzidine
ug/L
100
47.6
48
34-136
3-Nitroaniline
ug/L
100
71.3
71
37-138IL
4,6-Dinitro-2-methyl phenol
ug/L
100
67.2
67
21-157
4-Bromophenylphenyl ether
ug/L
50
34.5
69
38-130
4-Chloro-3-methyl phenol
ug/L
100
72.6
73
37-130
4-Chloroaniline
ug/L
100
69.7
70
38-130
4-Chlorophenylphenyl ether
ug/L
50
32.0
64
33-130
4-Nitroaniline
ug/L
100
66.6
67
42-137
4-Nitrophenol
ug/L
250
131
52
10-130 v1
Acenaphthene
ug/L
50
30.8
62
33-130
Acenaphthylene
ug/L
50
30.5
61
35-130
Aniline
ug/L
50
26.8
54
22-130
Anthracene
ug/L
50
34.2
68
48-130
Benzo(a)anthracene
ug/L
50
37.7
75
48-137
Benzo(a)pyrene
ug/L
50
38.3
77
49-138
Benzo(b)fluoranthene
ug/L
50
38.5
77
52-138
Benzo(g,h,i)perylene
ug/L
50
39.1
78
48-140
Benzo(k)fluoranthene
ug/L
50
37.6
75
48-139
Benzoic Acid
ug/L
250
112
45
10-130
Benzyl alcohol
ug/L
100
71.9
72
35-130
bis(2-Chloroethoxy)methane
ug/L
50
34.8
70
34-130
bis(2-Chloroethyl) ether
ug/L
50
33.5
67
36-130
bis(2-Ethylhexyl)phthalate
ug/L
50
40.1
80
32-165
Butylbenzylphthalate
ug/L
50
39.1
78
34-161
Chrysene
ug/L
50
36.8
74
47-131
Di-n-butylphthalate
ug/L
50
40.4
81
39-144
Di-n-octylphthalate
ug/L
50
33.8
68
30-170
Dibenz(a,h)anthracene
ug/L
50
39.4
79
49-138
Dibenzofuran
ug/L
50
31.3
63
33-130
Diethylphthalate
ug/L
50
35.7
71
38-131
Dimethylphthalate
ug/L
50
34.0
68
37-130
Fluoranthene
ug/L
50
37.5
75
46-137
Fluorene
ug/L
50
32.9
66
37-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 105 of 122

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
LABORATORY CONTROL SAMPLE:
Parameter
3587100
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Hexachloro-1,3-butadiene
ug/L
50
21.6
43
11-130
Hexachlorobenzene
ug/L
50
31.4
63
38-130
Hexachlorocyclopentadiene
ug/L
50
22.6
45
10-130
Hexachloroethane
ug/L
50
21.9
44
14-130
Indeno(1,2,3-cd)pyrene
ug/L
50
37.4
75
41-130
Isophorone
ug/L
50
33.4
67
33-130
N-Nitroso-di-n-propylamine
ug/L
50
34.5
69
36-130
N-Nitrosodimethylamine
ug/L
50
32.2
64
34-130
N-Nitrosodiphenylamine
ug/L
50
32.7
65
37-130
Naphthalene
ug/L
50
25.9
52
30-130
Nitrobenzene
ug/L
50
33.0
66
36-130
Pentachlorophenol
ug/L
100
65.2
65
23-149
Phenanthrene
ug/L
50
35.3
71
44-130
Phenol
ug/L
50
25.7
51
18-130
Pyrene
ug/L
50
36.6
73
47-134
2,4,6-Tribromophenol (S)
%
72
10-144
2-Fluorobiphenyl (S)
%
57
10-130
2-Fluorophenol(S)
%
54
10-130
Nitrobenzene-d5 (S)
%
67
10-144
Phenol-d6 (S)
%
44
10-130
Terphenyl-d14 (S)
%
69
34-163
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3587101
MS
92593909008 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3587102
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,2,4-Trichoorobenzene
ug/L
ND
45.5
45.5
27.4
28.3
60
62
10-130
3
30
1,2-Dichlorobenzene
ug/L
ND
45.5
45.5
27.4
28.2
60
62
10-130
3
30
1,3-Dichlorobenzene
ug/L
ND
45.5
45.5
25.9
27.0
57
59
10-130
4
30
1,4-Dichlorobenzene
ug/L
ND
45.5
45.5
26.5
27.7
58
61
10-130
4
30
1-Methyl naphthalene
ug/L
ND
45.5
45.5
32.8
33.3
72
73
10-130
1
30
2,2'-Oxybis(1-
ug/L
ND
45.5
45.5
35.4
35.4
78
78
12-142
0
30
chloropropane)
2,4,5-Trichlorophenol
ug/L
ND
45.5
45.5
33.6
42.5
74
94
10-143
23
30
2,4,6-Trichlorophenol
ug/L
ND
45.5
45.5
29.2
41.9
64
92
10-147
36
30 R1
2,4-Dichlorophenol
ug/L
ND
45.5
45.5
33.6
39.2
74
86
10-138
15
30
2,4-Dimethylphenol
ug/L
ND
45.5
45.5
35.5
36.9
78
81
25-130
4
30
2,4-Dinitrophenol
ug/L
ND
227
227
30.OJ
195
13
86
10-165
30 v1
2,4-Dinitrotoluene
ug/L
ND
45.5
45.5
38.9
41.8
86
92
29-148
7
30
2,6-Dinitrotoluene
ug/L
ND
45.5
45.5
38.5
40.0
85
88
26-146
4
30
2-Chloronaphthalene
ug/L
ND
45.5
45.5
35.3
35.8
78
79
11-130
1
30
2-Chlorophenol
ug/L
ND
45.5
45.5
33.0
35.8
73
79
10-133
8
30
2-Methyl naphthalene
ug/L
ND
45.5
45.5
32.8
33.3
72
73
13-130
1
30
2-Methyl phenol(o-Cresol)
ug/L
ND
45.5
45.5
33.1
34.4
73
76
20-130
4
30
2-Nitroaniline
ug/L
ND
90.9
90.9
77.8
82.1
86
90
24-136
5
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC.
Page 106 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3587101
MS
92593909008 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3587102
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
2-Nitrophenol
ug/L
ND
45.5
45.5
36.5
41.6
80
91
10-153
13
30
3&4-Methylphenol(m&p
ug/L
ND
45.5
45.5
32.0
32.9
70
72
16-130
3
30
Cresol)
3,3'-Dichlorobenzidine
ug/L
ND
90.9
90.9
71.5
69.2
79
76
10-153
3
30
3-Nitroaniline
ug/L
ND
90.9
90.9
78.6
76.5
86
84
22-151
3
30 IL
4,6-Dinitro-2-methylphenol
ug/L
ND
90.9
90.9
26.2
77.4
29
85
10-180
99
30 R1
4-Bromophenylphenyl ether
ug/L
ND
45.5
45.5
38.5
39.1
85
86
25-130
2
30
4-Chloro-3-methylphenol
ug/L
ND
90.9
90.9
70.9
75.4
78
83
25-133
6
30
4-Chloroaniline
ug/L
ND
90.9
90.9
70.4
69.4
77
76
14-132
1
30
4-Chlorophenylphenyl ether
ug/L
ND
45.5
45.5
38.0
38.6
84
85
19-130
2
30
4-Nitroaniline
ug/L
ND
90.9
90.9
78.2
79.8
86
88
29-150
2
30
4-Nitrophenol
ug/L
ND
227
227
29.5J
124
13
55
10-130
30 v1
Acenaphthene
ug/L
ND
45.5
45.5
37.5
38.4
82
84
16-130
2
30
Acenaphthylene
ug/L
ND
45.5
45.5
37.3
38.0
82
84
15-137
2
30
Aniline
ug/L
ND
45.5
45.5
32.1
18.1
71
40
10-130
56
30 R1
Anthracene
ug/L
ND
45.5
45.5
37.5
38.7
83
85
37-136
3
30
Benzo(a)anth race ne
ug/L
ND
45.5
45.5
40.2
42.3
89
93
40-145
5
30
Benzo(a)pyrene
ug/L
ND
45.5
45.5
32.5
34.8
72
76
41-146
7
30
Benzo(b)fluoranthene
ug/L
ND
45.5
45.5
30.7
34.3
68
75
39-151
11
30
Benzo(g,h,i)perylene
ug/L
ND
45.5
45.5
32.8
35.5
72
78
40-147
8
30
Benzo(k)fluoranthene
ug/L
ND
45.5
45.5
31.7
34.2
70
75
40-146
8
30
Benzoic Acid
ug/L
ND
227
227
ND
104
0
46
10-130
30 M1
Benzyl alcohol
ug/L
ND
90.9
90.9
70.7
73.2
78
81
25-130
4
30
bis(2-
ug/L
ND
45.5
45.5
39.1
40.8
86
90
23-130
4
30
Chloroethoxy)methane
bis(2-Chloroethyl) ether
ug/L
ND
45.5
45.5
38.9
38.8
86
85
25-130
0
30
bis(2- Ethyl hexyl)phthalate
ug/L
ND
45.5
45.5
39.8
45.0
88
99
28-166
12
30
Butylbenzylphthalate
ug/L
ND
45.5
45.5
38.3
43.2
84
95
33-165
12
30
Chrysene
ug/L
ND
45.5
45.5
40.1
41.9
88
92
38-141
4
30
Di-n-butylphthalate
ug/L
ND
45.5
45.5
39.2
43.7
86
96
32-153
11
30
Di-n-octylphthalate
ug/L
ND
45.5
45.5
35.2
38.2
77
84
30-175
8
30
Dibenz(a,h)anthracene
ug/L
ND
45.5
45.5
33.5
35.1
74
77
39-148
4
30
Dibenzofuran
ug/L
ND
45.5
45.5
37.7
38.1
83
84
20-130
1
30
Diethylphthalate
ug/L
ND
45.5
45.5
38.6
39.6
85
87
28-142
3
30
Dimethylphthalate
ug/L
ND
45.5
45.5
38.1
39.0
84
86
26-136
2
30
Fluoranthene
ug/L
ND
45.5
45.5
39.4
41.9
87
92
39-143
6
30
Fluorene
ug/L
ND
45.5
45.5
38.5
39.4
85
87
24-132
2
30
Hexachloro-1,3-butadiene
ug/L
ND
45.5
45.5
23.4
25.3
52
56
10-130
7
30
Hexachlorobenzene
ug/L
ND
45.5
45.5
34.7
35.9
76
79
29-130
3
30
Hexachlorocyclopentadiene
ug/L
ND
45.5
45.5
28.8
29.8
63
66
10-130
3
30
Hexachloroethane
ug/L
ND
45.5
45.5
24.7
25.6
54
56
10-130
4
30
Indeno(1,2,3-cd)pyrene
ug/L
ND
45.5
45.5
31.9
33.7
70
74
39-148
5
30
Isophorone
ug/L
ND
45.5
45.5
38.0
38.5
84
85
23-130
1
30
N-Nitroso-di-n-propylamine
ug/L
ND
45.5
45.5
39.3
40.0
87
88
25-130
2
30
N-Nitrosodimethylamine
ug/L
ND
45.5
45.5
31.4
31.8
69
70
22-130
1
30
N-Nitrosodiphenylamine
ug/L
ND
45.5
45.5
37.6
38.9
83
86
26-134
3
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC.
Page 107 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3587101
3587102
MS
MSD
92593909008
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Naphthalene
ug/L
ND
45.5
45.5
31.1
32.3
68
71
14-130
4
30
Nitrobenzene
ug/L
ND
45.5
45.5
38.6
40.5
85
89
25-130
5
30
Pentachlorophenol
ug/L
ND
90.9
90.9
37.5
72.6
41
80
10-175
64
30 R1
Phenanthrene
ug/L
ND
45.5
45.5
38.5
39.6
85
87
36-133
3
30
Phenol
ug/L
ND
45.5
45.5
24.6
24.3
54
53
10-130
1
30
Pyrene
ug/L
ND
45.5
45.5
38.1
40.7
84
90
40-143
7
30
2,4,6-Tribromophenol (S)
%
79
88
10-144
2-Fluorobiphenyl (S)
%
83
80
10-130
2-Fluorophenol(S)
%
55
60
10-130
Nitrobenzene-d5(S)
%
93
90
10-144
Phenol-d6 (S)
%
49
47
10-130
Terphenyl-d14(S)
%
86
85
34-163
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC.
Page 108 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
QC Batch: 685822 Analysis Method: EPA 8270E
QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92593947007,92593947008,92593947009,92593947010,92593947011,92593947012,92593947013,
92593947014,92593947015,92593947016
METHOD BLANK: 3586298 Matrix: Solid
Associated Lab Samples: 92593947007,92593947008,92593947009,92593947010,92593947011,92593947012,92593947013,
92593947014,92593947015,92593947016
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
1,2,4-Trichlorobenzene
mg/kg
ND
0.33
0.13
03/21/22 10:13
1,2-Dichlorobenzene
mg/kg
ND
0.33
0.12
03/21/22 10:13
1,3-Dichlorobenzene
mg/kg
ND
0.33
0.12
03/21/22 10:13
1,4-Dichlorobenzene
mg/kg
ND
0.33
0.13
03/21/22 10:13
1-Methylnaphthalene
mg/kg
ND
0.33
0.12
03/21/22 10:13
2,2'-Oxybis(1-chloropropane)
mg/kg
ND
0.33
0.16
03/21/22 10:13
2,4,5-Trichlorophenol
mg/kg
ND
0.33
0.15
03/21/22 10:13
2,4,6-Trichlorophenol
mg/kg
ND
0.33
0.14
03/21/22 10:13
2,4-DichIorophenol
mg/kg
ND
0.33
0.13
03/21/22 10:13
2,4-Dimethylphenol
mg/kg
ND
0.33
0.14
03/21/22 10:13
2,4-Dinitrophenol
mg/kg
ND
1.6
1.0
03/21/22 10:13
2,4-Dinitrotoluene
mg/kg
ND
0.33
0.13
03/21/22 10:13
2,6-Dinitrotoluene
mg/kg
ND
0.33
0.12
03/21/22 10:13
2-Chloronaphthalene
mg/kg
ND
0.33
0.13
03/21/22 10:13
2-Chlorophenol
mg/kg
ND
0.33
0.12
03/21/22 10:13
2-Methylnaphthalene
mg/kg
ND
0.33
0.13
03/21/22 10:13
2-Methylphenol(o-Cresol)
mg/kg
ND
0.33
0.14
03/21/22 10:13
2-Nitroaniline
mg/kg
ND
1.6
0.27
03/21/22 10:13
2-Nitrophenol
mg/kg
ND
0.33
0.14
03/21/22 10:13
3&4-Methylphenol (m&p Cresol)
mg/kg
ND
0.33
0.13
03/21/22 10:13
3,3'-Dichlorobenzidine
mg/kg
ND
0.66
0.22
03/21/22 10:13
3-Nitroaniline
mg/kg
ND
1.6
0.26
03/21/22 10:13
4,6-Dinitro-2-methyl phenol
mg/kg
ND
0.66
0.31
03/21/22 10:13
4-Bromophenylphenyl ether
mg/kg
ND
0.33
0.13
03/21/22 10:13
4-Chloro-3-methyl phenol
mg/kg
ND
0.66
0.23
03/21/22 10:13
4-Chloroaniline
mg/kg
ND
0.66
0.26
03/21/22 10:13
4-Chlorophenylphenyl ether
mg/kg
ND
0.33
0.12
03/21/22 10:13
4-Nitroaniline
mg/kg
ND
0.66
0.25
03/21/22 10:13
4-Nitrophenol
mg/kg
ND
1.6
0.64
03/21/22 10:13
Acenaphthene
mg/kg
ND
0.33
0.12
03/21/22 10:13
Acenaphthylene
mg/kg
ND
0.33
0.12
03/21/22 10:13
Aniline
mg/kg
ND
0.33
0.13
03/21/22 10:13
Anthracene
mg/kg
ND
0.33
0.11
03/21/22 10:13
Benzo(a)anthracene
mg/kg
ND
0.33
0.11
03/21/22 10:13
Benzo(a)pyrene
mg/kg
ND
0.33
0.11
03/21/22 10:13
Benzo(b)fluoranthene
mg/kg
ND
0.33
0.11
03/21/22 10:13
Benzo(g,h,i)perylene
mg/kg
ND
0.33
0.13
03/21/22 10:13
Benzo(k)fluoranthene
mg/kg
ND
0.33
0.12
03/21/22 10:13
Benzoic Acid
mg/kg
ND
1.6
0.71
03/21/22 10:13
IL
IL
IL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC. Page 109 of 122

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
METHOD BLANK: 3586298 Matrix: Solid
Associated Lab Samples: 92593947007, 92593947008, 92593947009, 92593947010, 92593947011, 92593947012, 92593947013,
92593947014,92593947015,92593947016
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Benzyl alcohol
mg/kg
ND
0.66
0.25
03/21/22 10:13
bis(2-Chloroethoxy)methane
mg/kg
ND
0.33
0.14
03/21/22 10:13
bis(2-Chloroethyl) ether
mg/kg
ND
0.33
0.12
03/21/22 10:13
bis(2-Ethylhexyl)phthalate
mg/kg
ND
0.33
0.13
03/21/22 10:13
Butylbenzylphthalate
mg/kg
ND
0.33
0.14
03/21/22 10:13
Chrysene
mg/kg
ND
0.33
0.12
03/21/22 10:13
Di-n-butylphthalate
mg/kg
ND
0.33
0.11
03/21/22 10:13
Di-n-octylphthalate
mg/kg
ND
0.33
0.13
03/21/22 10:13
Dibenz(a,h)anthracene
mg/kg
ND
0.33
0.13
03/21/22 10:13
Dibenzofuran
mg/kg
ND
0.33
0.12
03/21/22 10:13
Diethylphthalate
mg/kg
ND
0.33
0.12
03/21/22 10:13
Dimethylphthalate
mg/kg
ND
0.33
0.12
03/21/22 10:13
Fluoranthene
mg/kg
ND
0.33
0.11
03/21/22 10:13
Fluorene
mg/kg
ND
0.33
0.12
03/21/22 10:13
Hexachloro-1,3-butadiene
mg/kg
ND
0.33
0.14
03/21/22 10:13
Hexachlorobenzene
mg/kg
ND
0.33
0.13
03/21/22 10:13
Hexachlorocyclopentadiene
mg/kg
ND
0.33
0.19
03/21/22 10:13
Hexachloroethane
mg/kg
ND
0.33
0.13
03/21/22 10:13
Indeno(1,2,3-cd)pyrene
mg/kg
ND
0.33
0.13
03/21/22 10:13
Isophorone
mg/kg
ND
0.33
0.15
03/21/22 10:13
N-Nitroso-di-n-propylamine
mg/kg
ND
0.33
0.12
03/21/22 10:13
N-Nitrosodimethylamine
mg/kg
ND
0.33
0.11
03/21/22 10:13
N-Nitrosodiphenylamine
mg/kg
ND
0.33
0.12
03/21/22 10:13
Naphthalene
mg/kg
ND
0.33
0.11
03/21/22 10:13
Nitrobenzene
mg/kg
ND
0.33
0.15
03/21/22 10:13
Pentachlorophenol
mg/kg
ND
0.66
0.32
03/21/22 10:13
Phenanthrene
mg/kg
ND
0.33
0.11
03/21/22 10:13
Phenol
mg/kg
ND
0.33
0.15
03/21/22 10:13
Pyrene
mg/kg
ND
0.33
0.13
03/21/22 10:13
Pyridine
mg/kg
ND
0.33
0.10
03/21/22 10:13
2,4,6-Tribromophenol (S)
%
63
18-130
03/21/22 10:13
2-Fluorobiphenyl (S)
%
59
19-130
03/21/22 10:13
2-Fluorophenol (S)
%
56
18-130
03/21/22 10:13
Nitrobenzene-d5 (S)
%
59
21-130
03/21/22 10:13
Phenol-d6 (S)
%
58
18-130
03/21/22 10:13
Terphenyl-d14 (S)
%
61
15-130
03/21/22 10:13
LABORATORY CONTROL SAMPLE:
3586299
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
1,2,4-Trichlorobenzene
mg/kg
1.7
1.1 67 47-130
1,2-Dichlorobenzene
mg/kg
1.7
1.1 65 49-130
1,3-Dichlorobenzene
mg/kg
1.7
1.1 66 48-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
LABORATORY CONTROL SAMPLE:
Parameter
3586299
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,4-Dichlorobenzene
mg/kg
1.7
1.1
65
49-130
1-Methylnaphthalene
mg/kg
1.7
1.2
69
54-130
2,2'-Oxybis(1-chloropropane)
mg/kg
1.7
1.0
61
38-130
2,4,5-Trichlorophenol
mg/kg
1.7
1.2
73
49-130
2,4,6-Trichlorophenol
mg/kg
1.7
1.2
73
50-130
2,4-Dichlorophenol
mg/kg
1.7
1.2
71
51-130
2,4-Dimethylphenol
mg/kg
1.7
1.1
68
53-130
2,4-Dinitrophenol
mg/kg
8.3
5.6
67
39-130
2,4-Dinitrotoluene
mg/kg
1.7
1.2
71
53-130
2,6-Dinitrotoluene
mg/kg
1.7
1.3
76
55-130
2-Chloronaphthalene
mg/kg
1.7
1.1
68
48-130
2-Chlorophenol
mg/kg
1.7
1.1
68
54-130
2-Methylnaphthalene
mg/kg
1.7
1.2
69
57-130
2-Methylphenol(o-Cresol)
mg/kg
1.7
1.1
67
50-130
2-Nitroaniline
mg/kg
3.3
2.1
62
49-130
2-Nitrophenol
mg/kg
1.7
1.3
79
50-130
3&4-Methyl phenol (m&p Cresol)
mg/kg
1.7
1.1
64
50-130
3,3'-Dichlorobenzidine
mg/kg
3.3
2.0
61
47-130IL
3-Nitroaniline
mg/kg
3.3
2.1
64
45-130IL
4,6-Dinitro-2-methyl phenol
mg/kg
3.3
2.3
69
50-142
4-Bromophenylphenyl ether
mg/kg
1.7
1.2
74
55-130
4-Chloro-3-methyl phenol
mg/kg
3.3
2.2
66
52-130
4-Chloroaniline
mg/kg
3.3
2.0
61
49-130
4-Chlorophenylphenyl ether
mg/kg
1.7
1.1
67
53-130
4-Nitroaniline
mg/kg
3.3
2.1
64
51-130IL
4-Nitrophenol
mg/kg
8.3
5.6
67
40-130
Acenaphthene
mg/kg
1.7
1.2
70
56-130
Acenaphthylene
mg/kg
1.7
1.2
71
58-130
Aniline
mg/kg
1.7
0.98
59
44-130
Anthracene
mg/kg
1.7
1.1
68
60-130
Benzo(a)anthracene
mg/kg
1.7
1.1
69
59-130
Benzo(a)pyrene
mg/kg
1.7
1.2
72
57-130
Benzo(b)fluoranthene
mg/kg
1.7
1.2
74
54-130
Benzo(g,h,i)perylene
mg/kg
1.7
1.1
68
59-130
Benzo(k)fluoranthene
mg/kg
1.7
1.2
74
54-130
Benzoic Acid
mg/kg
8.3
4.5
54
19-130
Benzyl alcohol
mg/kg
3.3
2.1
63
50-130
bis(2-Chloroethoxy)methane
mg/kg
1.7
1.1
66
55-130
bis(2-Chloroethyl) ether
mg/kg
1.7
1.1
63
53-130
bis(2-Ethylhexyl)phthalate
mg/kg
1.7
1.2
71
58-130
Butylbenzylphthalate
mg/kg
1.7
1.3
79
46-138
Chrysene
mg/kg
1.7
1.1
69
57-130
Di-n-butylphthalate
mg/kg
1.7
1.2
69
57-130
Di-n-octylphthalate
mg/kg
1.7
1.3
77
57-130
Dibenz(a,h)anthracene
mg/kg
1.7
1.1
65
60-130
Dibenzofuran
mg/kg
1.7
1.1
69
54-130
Diethylphthalate
mg/kg
1.7
1.1
68
55-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Asheville, NC 28804
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QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
LABORATORY CONTROL SAMPLE:
Parameter
3586299
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Dimethylphthalate
mg/kg
1.7
1.2
70
57-130
Fluoranthene
mg/kg
1.7
1.1
67
57-130
Fluorene
mg/kg
1.7
1.1
69
56-130
Hexachloro-1,3-butadiene
mg/kg
1.7
1.1
68
41-130
Hexachlorobenzene
mg/kg
1.7
1.2
70
53-130
Hexachlorocyclopentadiene
mg/kg
1.7
1.1
64
23-130
Hexachloroethane
mg/kg
1.7
1.1
65
48-130
Indeno(1,2,3-cd)pyrene
mg/kg
1.7
1.1
65
61-130
Isophorone
mg/kg
1.7
1.0
63
49-130
N-Nitroso-di-n-propylamine
mg/kg
1.7
1.0
60
52-130
N-Nitrosodimethylamine
mg/kg
1.7
0.98
59
45-130
N-Nitrosodiphenylamine
mg/kg
1.7
1.1
69
56-130
Naphthalene
mg/kg
1.7
1.1
69
56-130
Nitrobenzene
mg/kg
1.7
1.1
65
50-130
Pentachlorophenol
mg/kg
3.3
2.3
68
33-130
Phenanthrene
mg/kg
1.7
1.2
71
60-130
Phenol
mg/kg
1.7
1.2
72
54-130
Pyrene
mg/kg
1.7
1.3
79
61-130
Pyridine
mg/kg
1.7
0.85
51
35-130
2,4,6-Tribromophenol (S)
%
80
18-130
2-Fluorobiphenyl (S)
%
69
19-130
2-Fluorophenol(S)
%
69
18-130
Nitrobenzene-d5 (S)
%
67
21-130
Phenol-d6 (S)
%
68
18-130
Terphenyl-d14 (S)
%
73
15-130
Qualifiers
SAMPLE DUPLICATE: 3586301
Parameter
Units
92593947008
Result
Dup
Result RPD
Max
RPD
1,2,4-Trichlorobenzene
mg/kg
ND
ND
30
1,2-Dichlorobenzene
mg/kg
ND
ND
30
1,3-Dichlorobenzene
mg/kg
ND
ND
30
1,4-Dichlorobenzene
mg/kg
ND
ND
30
1-Methylnaphthalene
mg/kg
ND
ND
30
2,2'-Oxybis(1-chloropropane)
mg/kg
ND
ND
30
2,4,5-Trichlorophenol
mg/kg
ND
ND
30
2,4,6-Trichlorophenol
mg/kg
ND
ND
30
2,4-Dichlorophenol
mg/kg
ND
ND
30
2,4-Dimethylphenol
mg/kg
ND
ND
30
2,4-Dinitrophenol
mg/kg
ND
ND
30
2,4-Dinitrotoluene
mg/kg
ND
ND
30
2,6-Dinitrotoluene
mg/kg
ND
ND
30
2-Chloronaphthalene
mg/kg
ND
ND
30
2-Chlorophenol
mg/kg
ND
ND
30
2-Methylnaphthalene
mg/kg
ND
ND
30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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2225 Riverside Dr.
Asheville, NC 28804
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QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
SAMPLE DUPLICATE: 3586301
Parameter
Units
92593947008
Result
Dup
Result RPD
Max
RPD Qualifiers
2-Methylphenol(o-Cresol)
mg/kg
ND
ND
30
2-Nitroaniline
mg/kg
ND
ND
30
2-Nitrophenol
mg/kg
ND
ND
30
3&4-Methyl phenol (m&p Cresol)
mg/kg
ND
ND
30
3,3'-Dichlorobenzidine
mg/kg
ND
ND
30 IL
3-Nitroaniline
mg/kg
ND
ND
30 IL
4,6-Dinitro-2-methyl phenol
mg/kg
ND
ND
30
4-Bromophenylphenyl ether
mg/kg
ND
ND
30
4-Chloro-3-methylphenol
mg/kg
ND
ND
30
4-Chloroaniline
mg/kg
ND
ND
30
4-Chlorophenylphenyl ether
mg/kg
ND
ND
30
4-Nitroaniline
mg/kg
ND
ND
30 IL
4-Nitrophenol
mg/kg
ND
ND
30
Acenaphthene
mg/kg
ND
ND
30
Acenaphthylene
mg/kg
ND
ND
30
Aniline
mg/kg
ND
ND
30
Anthracene
mg/kg
ND
ND
30
Benzo(a)anthracene
mg/kg
ND
ND
30
Benzo(a)pyrene
mg/kg
ND
ND
30
Benzo(b)fluoranthene
mg/kg
ND
ND
30
Benzo(g,h,i)perylene
mg/kg
ND
ND
30
Benzo(k)fluoranthene
mg/kg
ND
ND
30
Benzoic Acid
mg/kg
ND
ND
30
Benzyl alcohol
mg/kg
ND
ND
30
bis(2-Chloroethoxy)methane
mg/kg
ND
ND
30
bis(2-Chloroethyl) ether
mg/kg
ND
ND
30
bis(2-Ethylhexyl)phthalate
mg/kg
ND
ND
30
Butylbenzylphthalate
mg/kg
ND
ND
30
Chrysene
mg/kg
ND
ND
30
Di-n-butylphthalate
mg/kg
ND
ND
30
Di-n-octylphthalate
mg/kg
ND
ND
30
Dibenz(a,h)anthracene
mg/kg
ND
ND
30
Dibenzofuran
mg/kg
ND
ND
30
Diethylphthalate
mg/kg
ND
ND
30
Dimethylphthalate
mg/kg
ND
ND
30
Fluoranthene
mg/kg
ND
ND
30
Fluorene
mg/kg
ND
ND
30
Hexachloro-1,3-butadiene
mg/kg
ND
ND
30
Hexachlorobenzene
mg/kg
ND
ND
30
Hexachlorocyclopentadiene
mg/kg
ND
ND
30
Hexachloroethane
mg/kg
ND
ND
30
Indeno(1,2,3-cd)pyrene
mg/kg
ND
ND
30
Isophorone
mg/kg
ND
ND
30
N-Nitroso-di-n-propylamine
mg/kg
ND
ND
30
N-Nitrosodimethylamine
mg/kg
ND
ND
30
N-Nitrosodiphenylamine
mg/kg
ND
ND
30
Naphthalene
mg/kg
ND
ND
30
Results presented on this page are in the units
indicated by the "Units" column except where an alternate unit
is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
SAMPLE DUPLICATE: 3586301
Parameter
Units
92593947008
Result
Dup
Result
Nitrobenzene
mg/kg
ND
ND
Pentachlorophenol
mg/kg
ND
ND
Phenanthrene
mg/kg
ND
ND
Phenol
mg/kg
ND
ND
Pyrene
mg/kg
ND
ND
Pyridine
mg/kg
ND
ND
2,4,6-Tribromophenol (S)
%
42
47
2-Fluorobiphenyl (S)
%
56
53
2-Fluorophenol(S)
%
41
35
Nitrobenzene-d5 (S)
%
70
61
Phenol-d6 (S)
%
49
41
Terphenyl-d14 (S)
%
63
59
Max
RPD RPD Qualifiers
30
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Page 114 of 122

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2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 49:13699-D
Pace Project No.: 92593947
QC Batch: 685512 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92593947007,92593947008,92593947009,92593947010,92593947011,92593947012,92593947013,
92593947014,92593947015,92593947016
SAMPLE DUPLICATE: 3584624
92593842001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 16.7 15.5 7 25 N2
SAMPLE DUPLICATE: 3584625
92593906003 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 24.4 24.6 1 25 N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/29/2022 06:07 AM without the written consent of Pace Analytical Services, LLC.
Page 115 of 122

Pace Analytical Services, LLC
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Asheville, NC 28804
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QUALIFIERS
Project: 49:13699-D
Pace Project No.: 92593947
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
C7 Analyte is a possible laboratory contaminant (not present in method blank).
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
MS Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
REPORT OF LABORATORY ANALYSIS
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[phone]
QUALIFIERS
Project: 49:13699-D
Pace Project No.: 92593947
ANALYTE QUALIFIERS
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
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[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
49:13699-D
92593947
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92593947001
TW-1
EPA 3510C
685634
EPA 8270E
685746
92593947002
TW-2
EPA 3510C
685634
EPA 8270E
685746
92593947003
TW-3
EPA 3510C
685634
EPA 8270E
685746
92593947004
TW-4
EPA 3510C
685634
EPA 8270E
685746
92593947005
TW-5
EPA 3510C
685634
EPA 8270E
685746
92593947006
TW-6
EPA 3510C
686047
EPA 8270E
686213
92593947007
SBA
EPA 3546
685822
EPA 8270E
686010
92593947008
SB-2
EPA 3546
685822
EPA 8270E
686010
92593947009
SB-3
EPA 3546
685822
EPA 8270E
686010
92593947010
SB-4
EPA 3546
685822
EPA 8270E
686010
92593947011
SB-5
EPA 3546
685822
EPA 8270E
686010
92593947012
SB-6
EPA 3546
685822
EPA 8270E
686010
92593947013
SB-7
EPA 3546
685822
EPA 8270E
686010
92593947014
SB-8
EPA 3546
685822
EPA 8270E
686010
92593947015
SB-9
EPA 3546
685822
EPA 8270E
686010
92593947016
SB-10
EPA 3546
685822
EPA 8270E
686010
92593947007
SBA
EPA 5035A/5030B
686161
EPA 8260D
686214
92593947008
SB-2
EPA 5035A/5030B
685823
EPA 8260D
685869
92593947009
SB-3
EPA 5035A/5030B
685823
EPA 8260D
685869
92593947010
SB-4
EPA 5035A/5030B
685823
EPA 8260D
685869
92593947011
SB-5
EPA 5035A/5030B
685823
EPA 8260D
685869
92593947012
SB-6
EPA 5035A/5030B
685823
EPA 8260D
685869
92593947013
SB-7
EPA 5035A/5030B
685823
EPA 8260D
685869
92593947014
SB-8
EPA 5035A/5030B
685823
EPA 8260D
685869
92593947015
SB-9
EPA 5035A/5030B
685823
EPA 8260D
685869
92593947016
SB-10
EPA 5035A/5030B
685823
EPA 8260D
685869
92593947001
TW-1
EPA 8260D
685751
92593947002
TW-2
EPA 8260D
685751
92593947003
TW-3
EPA 8260D
685751
92593947004
TW-4
EPA 8260D
685751
92593947005
TW-5
EPA 8260D
686126
92593947006
TW-6
EPA 8260D
686126
92593947007
SBA
SW-846
685512
92593947008
SB-2
SW-846
685512
92593947009
SB-3
SW-846
685512
92593947010
SB-4
SW-846
685512
92593947011
SB-5
SW-846
685512
92593947012
SB-6
SW-846
685512
92593947013
SB-7
SW-846
685512
92593947014
SB-8
SW-846
685512
92593947015
SB-9
SW-846
685512
92593947016
SB-10
SW-846
685512
Date: 03/29/2022 06:07 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 118 of 122

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Document Name:
Document Revised: November 15, 2021
Sample Condition Upon Receipt {SCUR)
Page 2 of 2
Document Nu.:
issuing Authority:
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f-CAR-CS-033-Rev.08
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottles
Project # W01t ; 92593947
PM: A19B Due Date: 03/22/22
CL,IEN'r: 93-ECS ASH
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Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy or this form will oe srnt tome worm Carolina DEHNR Cennlanon unite (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 121 of 122

Document Name:
Sample Condition Upon Recelt
Document No.:
F-CAR-CS•033-Rev.08
"Check mark top half of box if pH and/or dechlorination is
Verified and within the acceptance range for preservation
samples.
Uceptions: VOA, Coliform, TOC, Oil and Grease, DRO/2015 (water) DOC, Wis
"Bottom half of box is to list number of bottles
Dacurnent Revised: November 15, 2021
Page 2 of 2
Issuing Authority:
Project it W01t : 92'593947
PM: AI48 Due Date: 03/22/22
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Now Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form wits be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers,
Page 122 of 122

APPENDIX D
RISK CALCULATOR OUTPUT DATA SHEETS

Risk for Individual Pathways
L9,A it riM
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID:
Exposure Unit ID: TW-5
DIRECT CONTACT SOIL AND WATER CALCULATORS
Receptor
Pathway
CarcinogenicRisk
Hazard Index
Risk exceeded?
Resident
Soil
0.0E+00
0.0E+00
NO
Groundwater Use*
NC
NC
NC
Non -Residential Worker
Soil
0.0E+00
0.0E+00
NO
Groundwater Use*
NC
NC
NC
Construction Worker
Soil
NC
NC
NC
Recreator/Trespasser
Soil
NC
NC
NC
Surface Water*
NC
NC
NC
VAPOR INTRUSION CALCULATORS
Receptor
Pathway
CarcinogenicRisk
Hazard Index
Risk exceeded?
Resident
Groundwater to Indoor Air
6.3E-05
1.5E+00
YES
Soil Gas to Indoor Air
0.0E+00
0.0E+00
NO
Indoor Air
0.0E+00
0.0E+00
NO
Non -Residential Worker
Groundwater to Indoor Air
1.4E-05
3.6E-01
NO
Soil Gas to Indoor Air
0.0E+00
0.0E+00
NO
Indoor Air
0.0E+00
0.0E+00
NO
CONTAMINANT MIGRATION CALCULATORS
Pathway
Source
Target Receptor Concentrations Exceeded?
Groundwater
Source Soil
Exceedence of 2L at Receptor?
NM
Source Groundwater
Exceedence of 2L at Receptor?
NM
Surface Water
Source Soil
Exceedence of 2B at Receptor?
NM
Source Groundwater
Exceedence of 213 at Receptor?
NM
Notes:
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 213 Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk -based
closure.
3. NM = Not Modeled
4. NC = Pathway not calculated
North Carolina DEQ Risk Calculator

Risk for Individual Pathways
L9,A it riM
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID:
Exposure Unit ID: TW-6
DIRECT CONTACT SOIL AND WATER CALCULATORS
Receptor
Pathway
CarcinogenicRisk
Hazard Index
Risk exceeded?
Resident
Soil
0.0E+00
0.0E+00
NO
Groundwater Use*
NC
NC
NC
Non -Residential Worker
Soil
0.0E+00
0.0E+00
NO
Groundwater Use*
NC
NC
NC
Construction Worker
Soil
NC
NC
NC
Recreator/Trespasser
Soil
NC
NC
NC
Surface Water*
NC
NC
NC
VAPOR INTRUSION CALCULATORS
Receptor
Pathway
CarcinogenicRisk
Hazard Index
Risk exceeded?
Resident
Groundwater to Indoor Air
1.3E-04
4.1E+00
YES
Soil Gas to Indoor Air
0.0E+00
0.0E+00
NO
Indoor Air
0.0E+00
0.0E+00
NO
Non -Residential Worker
Groundwater to Indoor Air
2.9E-05
9.8E-01
NO
Soil Gas to Indoor Air
0.0E+00
0.0E+00
NO
Indoor Air
0.0E+00
0.0E+00
NO
CONTAMINANT MIGRATION CALCULATORS
Pathway
Source
Target Receptor Concentrations Exceeded?
Groundwater
Source Soil
Exceedence of 2L at Receptor?
NM
Source Groundwater
Exceedence of 2L at Receptor?
NM
Surface Water
Source Soil
Exceedence of 2B at Receptor?
NM
Source Groundwater
Exceedence of 213 at Receptor?
NM
Notes:
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 213 Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk -based
closure.
3. NM = Not Modeled
4. NC = Pathway not calculated
North Carolina DEQ Risk Calculator