11037_Double Oaks Atando TH_ Soil Export Rpt and approval 20240404

April 4, 2024 Sent Via E-mail
Avery Rogers Beauxwright 1900 West Morehead St, Suite 201 Charlotte, North Carolina 28208 [e-mail]
Subject: Brownfields Soil Management 1302-1340 Newland Avenue Double Oaks Brownfields Property
Charlotte, Mecklenburg County Brownfields Project No. 11037-07-060
Dear Avery: The North Carolina Department of Environmental Quality (DEQ) Brownfields Redevelopment Section received
and reviewed a request to export an approximate 2,000 cubic yards of soils from the redevelopment of 1302-1340 Newland Avenue at the Double Oaks Brownfields Property. This request was submitted on your behalf by Mr. Matt Ingalls of Hart & Hickman, PC (H&H) in his Stockpile Soil Characterization Report dated April 3, 2024. DEQ Brownfields reviewed the soil analytical data provided in the letter report. Based on our review of the data provided, the DEQ Brownfields agrees that these soils may be exported to Old 27 Landfill (Tate Street Mount Holly, Mecklenburg County, Permit No. 36-A-LCID). All soil export must be conducted under a DEQ Brownfields approved Environmental Management Plan (EMP). Per the EMP, the soils will be field screened
during excavation prior to export from the property. If unanticipated impacts are identified during excavation, please refer to the EMP for further actions and cease transfer until appropriate characterization can be completed. In addition, in accordance with the Double Oaks Newland Avenue EMP, an annual Redevelopment Summary
Report will be submitted to DEQ Brownfields. Details related to the disposition of this soil including but not limited to, total volume, general description of field screening efforts, etc. should be included with the Redevelopment Summary Report.
Please be advised that this approval from DEQ Brownfields does not waive any applicable requirement to obtain any necessary permits, licenses or certifications which may be required from other state or local entities. If you
have any questions, please feel free to contact me at 704-661-0330, or via e-mail at [e-mail] Sincerely,
Carolyn Minnich Brownfields Project Manager ec: BF Property Management Branch Matt Ingalls [e-mail]

Via E-Mail

April 3, 2024

Beauxwright
1900 W. Morehead Street #201
Charlotte, North Carolina, 28208

Attention: Avery Rogers

Re: Soil Stockpile Characterization Report
Double Oaks Brownfields Property
1302 and 1340 Newland Avenue
Charlotte, North Carolina
H&H Project No. BWR-013

Dear Avery:

1.0 Introduction and Background Information

Hart & Hickman, PC (H&H) has completed soil characterization activities for disposal of
approximately 2,000 cubic yards (CYs) of soil stockpiled at the Double Oaks Brownfields property
located at 1302 and 1340 Newland Road in Charlotte, Mecklenburg County, North Carolina (Site).
The Site has a completed Brownfields Agreement (BFA) with the North Carolina Department of
Environmental Quality (DEQ) Brownfields Redevelopment Section (Brownfields Project No.
11037-07-060). A Site Location Map is attached as Figure 1 and the Site and surrounding area is
shown in Figure 2.

The Site consists of two parcels of vacant land (Parcel IDs: 07707902 and 07707903) that total
approximately 5.6 acres. The Site is a portion of a larger Brownfields Property which is comprised
of multiple parcels of contiguous and noncontiguous land that total approximately 56 acres. Most of
the off-site portion of the Brownfields Property has been developed with a single-family residential
subdivision (Brightwalk community) or multi-family apartment complexes (Alexander Apartment
Avery Rogers
April 3, 2024
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Homes and The Stevenson Apartments). The Site portion of the Brownfields property is currently
under redevelopment of a townhome community and contains an approximate 2,000 cubic yard
(CY) soil stockpile recently generated by NVR during construction activities.

Redevelopment plans for the Double Oaks Brownfields property are being conducted in accordance
with a DEQ-approved Environmental Management Plan (EMP) dated May 17, 2022. H&H
understands that unsuitable soil generated from development activities has been stockpiled on-Site.
H&H also understands that the stockpiled soil cannot be reused on-Site and will need to be exported.
As such, H&H collected soil stockpile characterization samples to assist with identifying disposal
facilities based on the analytical results of the soil stockpile sampling event. A summary of the
stockpiled soil characterization activities is provided below.

2.0 Stockpile Sampling Activities

Soil stockpile characterization activities were conducted on March 22, 2024 in accordance with the
DEQ-approved EMP. The EMP states that soil samples will be collected at a rate of one (1) sample
per every approximately 1,000-CYs for specified laboratory analyses mentioned below. Therefore,
H&H divided the approximately 2,000 CY soil pile into two (2) 1,000-CY sample areas (Stockpile-
A32224 and Stockpile-B32224). From each sample area, H&H collected five (5) aliquot soil
samples from borings advanced within the stockpile from depths ranging from 0 to 7 ft using a
decontaminated stainless-steel hand auger. During boring advancement, H&H inspected the soils,
and allowed a portion of the soil sample to volatilize for field screening of volatile organic vapors
using a calibrated photoionization detector (PID). During the stockpile sampling event, H&H did
not identify obvious evidence of staining, unusual odors, or PID readings above background
measurements in the aliquot soil samples. Sample locations are depicted on Figure 2.

One grab sample was collected from an undisturbed portion of an aliquot soil sample collected in
each evaluation area for a total of two (2) grab soil samples that were submitted to Waypoint
Analytical, LLC (Waypoint), a North Carolina-certified laboratory for analysis of volatile organic
Avery Rogers
April 3, 2024
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compounds (VOCs) by EPA Method 8260. The grab samples collected for VOC analysis were
selected based on results of field screening. Remaining portions of the five aliquot soil samples
were homogenized to form a composite soil sample representative of each of the two stockpiles for a
total of two composite stockpile samples. Composite soil samples were also submitted to Waypoint
for analysis of semi-volatile organic compounds (SVOCs) by EPA Method 8270 and Resource
Conservation and Recovery Act (RCRA) metals plus hexavalent chromium by EPA Methods
6020/7471/7199. Analytical results of the soil stockpile samples are discussed below.

3.0 Soil Sampling Results

A tabular summary of the soil stockpile analytical results is presented in Table 1. Trace
concentrations of the VOCs acetone [up to 0.033 milligrams per kilogram (mg/kg)] and ethanol
(0.231 mg/kg) were detected in at least one stockpile sample above the laboratory method detection
limits, but below DEQ Preliminary Soil Remediation Goals (PSRGs). Arsenic (up to 1.29 mg/kg)
was detected in each soil stockpile sample above the Residential PSRG of 0.68 mg/kg, but within
range of Site-specific background arsenic concentrations of 0.33 mg/kg to 2.0 mg/kg. Several other
metals were detected in the soil stockpile samples above laboratory method detection limits that
were either within range of or below established background metals concentrations. None of the
other metals detected exceeded established PSRGs. The laboratory analytical report is provided in
Appendix A.

3.0 Conclusions and Recommendations

Based on the results of the Stockpile-A32224 and the Stockpile-B32224 soil characterization
sampling activities, the Prospective Developer will request DEQ Brownfields approval to send the
soil in Stockpile-A32224 and Stockpile-B32224 to a Land Clearing and Inert Debris (LCID) landfill
(i.e., the Old 27 Landfill in Gaston County) or a Construction & Debris (C&D) landfill for disposal.
In accordance with the EMP, we will ask that DEQ issues written approval for these disposal options
based on the attached characterization information.

Table 1
Summary of Soil Analytical Results
Double Oaks Brownfields Property
1302 & 1340 Newland Avenue
Charlotte, North Carolina
Brownfields Project No. 11037-07-060
H&H Project No. BWR-013
Sample ID
Sample Type Composite Grab Composite Grab Composite Grab
Sample Date 3//22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024
Units
VOCs by EPA 8260D
Acetone NA 0.015 J NA 0.012 J NA 0.033 25 14,000 210,000 ------
Ethanol NA <0.017 NA <0.017 NA 0.231 J NE NE NE ------
SVOCs by 8270E ALL BDL NA ALL BDL NA ALL BDL NA ------------
Metals by 6020/7471/7199
Arsenic 0.908 NA 1.29 NA 1.05 NA 5.8 0.68 3.0 0.33 - 2.9
Barium 104 NA 105 NA 135 NA 580 3,100 47,000 43 - 420 50 - 1,000 356
Cadmium 0.0372 J NA 0.0448 J NA 0.0355 J NA 3.0 1.4 20 <0.0074 - 0.55 (4)(4)
Chromium 35.8 NA 82.0 NA 68.8 NA NE NE NE 13 - 190 7.0 - 300 65
Chromium (III)35.5 NA 81.7 NA 68.53 NA 360,000 23,000 350,000 13 - 188.66 NS NS
Chromium (VI)0.254 NA 0.298 NA 0.270 NA 3.8 0.31 6.5 <0..298 - 2.63 NS NS
Lead 6.79 NA 10.2 NA 7.98 NA 270 400 800 <2.1 - 39 ND - 50 16
Mercury 0.0483 NA 0.0375 NA 0.0272 J NA NE 4.7 70 <0.011 - 0.14 0.03 - 0.52 0.121
Selenium <0.128 NA 0.240 J NA 0.155 J NA 2.1 78 1,200 <0.045 - 1.1 J <0.1 - 0.8 0.42
Silver <0.312 NA <0.310 NA <0.300 NA 3.4 78 1,200 <0.0029 - 0.23 ND - 5.0 NS
Notes:
1)NC Department of Environmental Quality (DEQ) Health Based Preliminary Soil Remediation Goals (PSRGs) dated February 2024 and based upon carcinogenic total risk of 1.0E-06 and non-carcinogenic target hazard quotient of 0.2.
2)Background metals obtained from on-site soil stockpile characterization data collected between 7/28/21 and 7/30/21.
3)Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005.
4)Background values reported for soils of the southeastern United States.
With the exception of metals, only constituents detected in at least one sample are shown.
Compound concentrations are reported to the laboratory method detection limits.
Bold values exceed Residential PSRGs but are within range of Site-specific background concentrations.
VOCs = Volatile Organic Compounds; SVOCs = Semi-Volatile Organic Compounds; NS = Not Specified; ND = Not Detected; NA = Not Analyzed; NE = Not Established; -- = Not Applicable
J = Estimated concentration above method detection limits but below reporting limit.
Site-Specific
Background (2) Soil Stockpile Regional Background (3)
Range MeanRange
DEQ PSRGs (1)
Protection of
Groundwater Residential Industrial/
Commercial
mg/kg
Sample Area
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Beauxwright (BWR)/BWR-013 Atando - Double Oaks Lot/Brownfields/Soil Management/Stockpile Sampling 2024/Table/Stockpile Data 20244/3/2024
Table 1 (Page 1 of 1)
Hart & Hickman, PC
REVISION NO. 0
JOB NO. BWR-013
DATE: 4-3-24
FIGURE NO. 2
DOUBLE OAKS BROWNFIELDS PROPERTY
1302 AND 1340 NEWLAND ROAD
CHARLOTTE, NORTH CAROLINA
SITE AND SAMPLE LOCATION MAP
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL BOUNDARY
SURFACE WATER FEATURE
APPROXIMATE EXTENT OF SOIL
STOCKPILE
SOIL ALIQUOT LOCATION
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
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NOTES:
1.AERIAL IMAGERY AND PARCEL DATA OBTAINED FROM
MECKLENBURG COUNTY GIS, 2024.
2.SOIL STOCKPILE SAMPLES REPRESENT 1,000 CUBIC YARDS.
STOCKPILE - B32224
STOCKPILE - A32224
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Appendix A

Laboratory Analytical Report

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

4/2/2024
Hart & Hickman (Charlotte) Matt Ingalls
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 24-082-0013 Client Project Description: BWR-013
Dear Matt Ingalls:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 3/22/2024 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 51
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2024402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/28/202540750State ProgramAlabama
02/07/202588-0650State ProgramArkansas
06/30/20242904State ProgramCalifornia
06/30/2024E871157State Program - NELAPFlorida
11/14/2025C044State ProgramGeorgia
06/30/202404015State ProgramGeorgia
10/31/2024200078State Program - NELAPIllinois
06/30/202480215State ProgramKentucky
12/31/2024KY90047State ProgramKentucky
12/31/2024LA037State Program - NELAPLouisiana
06/30/202404015State Program - NELAPLouisiana
11/14/2025MSState ProgramMississippi
07/31/202447701State ProgramNorth Carolina
12/31/2024415State ProgramNorth Carolina
05/31/202468-03195State Program - NELAPPennsylvania
06/30/202484002State ProgramSouth Carolina
11/14/202502027State ProgramTennessee
09/30/2024T104704180State Program - NELAPTexas
06/30/202400106State ProgramVirginia
09/14/2024460181State Program - NELAPVirginia
Page 1 of 1 00016/24-082-0013
Page 2 of 51
Report Number:
Sample Summary Table
Client Project Description:
24-082-0013
BWR-013
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
03/22/2024 10:55Solids 89020 Stockpile-A32224 03/22/2024 11:51
03/22/2024 10:55Solids 89020 Stockpile-A32224 03/22/2024 11:51 6020B WP MTN -
03/22/2024 10:55Solids 89020 Stockpile-A32224 03/22/2024 11:51 SW-7199 WP MTN -
03/22/2024 11:10Solids 89021 Stockpile-B32224 03/22/2024 11:51
03/22/2024 11:10Solids 89021 Stockpile-B32224 03/22/2024 11:51 SW-7199 WP MTN -
03/22/2024 11:10Solids 89021 Stockpile-B32224 03/22/2024 11:51 6020B WP MTN -
03/22/2024Solids 89022 Stockpile DUP-32224 03/22/2024 11:51
03/22/2024Solids 89022 Stockpile DUP-32224 03/22/2024 11:51 SW-7199 WP MTN -
03/22/2024Solids 89022 Stockpile DUP-32224 03/22/2024 11:51 6020B WP MTN -
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 51
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
24-082-0013
Report Limit
Project:BWR-013
V 89020Stockpile-A32224
0.908 04/01/2024 15:576020BArsenicmg/Kg - dry 0.107
104 03/29/2024 17:506020BBariummg/Kg - dry 0.053
J0.0372 03/29/2024 17:506020BCadmiummg/Kg - dry 0.0324
35.8 03/29/2024 17:506020BChromiummg/Kg - dry 0.144
6.79 03/29/2024 17:506020BLeadmg/Kg - dry 0.0387
0.0483 03/28/2024 12:587471BMercury (Total)mg/Kg - dry 0.0150
J0.015 03/25/2024 13:128260DAcetonemg/Kg - dry 0.002
0.254 03/29/2024 16:08SW-7199 Chromium, Hexavalent mg/Kg - dry 0.176
19.9 03/25/2024 16:25SW-DRYWT Moisture %
V 89021Stockpile-B32224
1.05 04/01/2024 16:016020BArsenicmg/Kg - dry 0.103
135 03/29/2024 17:556020BBariummg/Kg - dry 0.051
J0.0355 03/29/2024 17:556020BCadmiummg/Kg - dry 0.0312
68.8 04/01/2024 16:016020BChromiummg/Kg - dry 0.139
7.98 03/29/2024 17:556020BLeadmg/Kg - dry 0.0372
J0.155 04/01/2024 16:016020BSeleniummg/Kg - dry 0.123
J0.0272 03/28/2024 13:007471BMercury (Total)mg/Kg - dry 0.0144
0.033 03/26/2024 16:538260DAcetonemg/Kg - dry 0.002
J0.231 03/26/2024 16:538260DEthanolmg/Kg - dry 0.016
0.270 03/29/2024 16:51SW-7199 Chromium, Hexavalent mg/Kg - dry 0.169
16.8 03/25/2024 16:25SW-DRYWT Moisture %
V 89022Stockpile DUP-32224
1.29 04/01/2024 16:076020BArsenicmg/Kg - dry 0.106
105 03/29/2024 18:006020BBariummg/Kg - dry 0.053
J0.0448 03/29/2024 18:006020BCadmiummg/Kg - dry 0.0322
82.0 04/01/2024 16:076020BChromiummg/Kg - dry 0.143
10.2 03/29/2024 18:006020BLeadmg/Kg - dry 0.0384
J0.240 04/01/2024 16:076020BSeleniummg/Kg - dry 0.127
0.0375 03/28/2024 13:037471BMercury (Total)mg/Kg - dry 0.0149
J0.012 03/25/2024 14:068260DAcetonemg/Kg - dry 0.002
0.298 03/29/2024 17:02SW-7199 Chromium, Hexavalent mg/Kg - dry 0.174
19.3 03/25/2024 16:25SW-DRYWT Moisture %
Page 4 of 51

Client: Hart & Hickman (Charlotte) CASE NARRATIVE
Project: BWR-013 Lab Report Number: 24-082-0013
Date: 4/2/2024
Metals Analyses Method 6020B Sample 65237 (North Myrtle Beach N+M) Analyte: Barium
QC Batch No: L741761/L741544 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 65237 (North Myrtle Beach N+M) Analyte: Cadmium
QC Batch No: L741761/L741544 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 65237 (North Myrtle Beach N+M)
Analyte: Chromium QC Batch No: L741761/L741544
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected.
Sample 65237 (North Myrtle Beach N+M) Analyte: Lead QC Batch No: L741761/L741544
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected. Hexavalent Chromium by Ion Chromatography Method SW-7199 Sample 89020 (Stockpile-A32224) Analyte: Hexavalent Chromium QC Batch No: L741598/L741255
Insoluble Hexavalent Chromium spike recovery outside QC limits. See soluble spike recovery and LCS for system verification.
Volatile Organic Compounds - GC/MS Method 8260D Analyte: 1,4-Dichlorobenzene QC Batch No: V45352/V45350 Target analyte did not meet calibration verification criteria. Analysis of a low level check demonstrated that there was adequate sensitivity to report this compound at the laboratory reporting limit as non-detect.
Analyte: 2-Chlorotoluene QC Batch No: V45352/V45350 Target analyte did not meet calibration verification criteria. Analysis of a low level check demonstrated that there was adequate sensitivity to report this compound at the laboratory reporting limit as non-detect.
Page 5 of 51

Analyte: 4-Chlorotoluene
QC Batch No: V45352/V45350 Target analyte did not meet calibration verification criteria. Analysis of a low level check demonstrated that there
was adequate sensitivity to report this compound at the laboratory reporting limit as non-detect.
Analyte: Acrolein QC Batch No: V45265/V45350
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: Ethanol QC Batch No: V45265/V45350
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: Ethanol QC Batch No: V45352/V45350
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Results should be considered estimated due to the potential for a high bias.
Analyte: Hexachlorobutadiene QC Batch No: V45352/V45350 Target analyte did not meet calibration verification criteria. Analysis of a low level check demonstrated that there
was adequate sensitivity to report this compound at the laboratory reporting limit as non-detect.
Analyte: tert-Butylbenzene QC Batch No: V45352/V45350 Target analyte did not meet calibration verification criteria. Analysis of a low level check demonstrated that there was adequate sensitivity to report this compound at the laboratory reporting limit as non-detect. Analyte: trans-1,3-Dichloropropene
QC Batch No: V45265/V45350 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Semivolatile Organic Compounds - GC/MS Method 8270E Analyte: 1,4-Dichlorobenzene QC Batch No: V45311/V45267
Target analyte did not meet calibration verification criteria. Analysis of a low level check demonstrated that there was adequate sensitivity to report this compound at the laboratory reporting limit as non-detect. Analyte: 2-Nitrophenol QC Batch No: V45311/V45267 Target analyte did not meet calibration verification criteria. Analysis of a low level check demonstrated that there was adequate sensitivity to report this compound at the laboratory reporting limit as non-detect. Analyte: Aniline QC Batch No: V45311/V45267 Target analyte did not meet calibration verification criteria. Analysis of a low level check demonstrated that there was adequate sensitivity to report this compound at the laboratory reporting limit as non-detect.
Page 6 of 51

Analyte: Bis(2-chloroethyl)ether QC Batch No: V45311/V45267
Target analyte did not meet calibration verification criteria. Analysis of a low level check demonstrated that there was adequate sensitivity to report this compound at the laboratory reporting limit as non-detect.
Analyte: Phenol
QC Batch No: V45311/V45267 Target analyte did not meet calibration verification criteria. Analysis of a low level check demonstrated that there
was adequate sensitivity to report this compound at the laboratory reporting limit as non-detect.

Page 7 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile-A32224
89020 Matrix:
3/22/2024 10:55
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.9 %Moisture 1 03/25/24 16:25 SW-DRYWTPEB
0.254 mg/Kg - dry 0.176 0.249Chromium, Hexavalent 1 03/29/24 16:08 SW-7199MKD
0.908 mg/Kg - dry 0.107 0.312Arsenic 5 04/01/24 15:57 6020BCPW
104 mg/Kg - dry 0.053 0.312Barium 5 03/29/24 17:50 6020BCPW
0.0372 J mg/Kg - dry 0.0324 0.312Cadmium 5 03/29/24 17:50 6020BCPW
35.8 mg/Kg - dry 0.144 0.312Chromium 5 03/29/24 17:50 6020BCPW
6.79 mg/Kg - dry 0.0387 0.312Lead 5 03/29/24 17:50 6020BCPW
0.0483 mg/Kg - dry 0.0150 0.0375Mercury (Total)1 03/28/24 12:58 7471BNPC
<0.128 mg/Kg - dry 0.128 0.312Selenium 5 04/01/24 15:57 6020BCPW
<0.312 mg/Kg - dry 0.0084 0.312Silver 5 03/29/24 17:50 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile-A32224
89020 Matrix:
3/22/2024 10:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V45350 03/25/24 08:00
0.015 J mg/Kg - dry 0.002 0.024Acetone 1 03/25/24 13:12 V45265TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 03/25/24 13:12 V45265TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 03/25/24 13:12 V45265TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 03/25/24 13:12 V45265TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 03/25/24 13:12 V45265TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 03/25/24 13:12 V45265TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 03/25/24 13:12 V45265TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 03/25/24 13:12 V45265TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 03/25/24 13:12 V45265TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 03/25/24 13:12 V45265TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 03/25/24 13:12 V45265TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 03/25/24 13:12 V45265TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 03/25/24 13:12 V45265TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 03/25/24 13:12 V45265TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 03/25/24 13:12 V45265TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 03/25/24 13:12 V45265TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 03/25/24 13:12 V45265TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 03/25/24 13:12 V45265TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 03/25/24 13:12 V45265TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 03/25/24 13:12 V45265TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 03/25/24 13:12 V45265TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 03/25/24 13:12 V45265TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile-A32224
89020 Matrix:
3/22/2024 10:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V45350 03/25/24 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 03/25/24 13:12 V45265TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 03/25/24 13:12 V45265TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 03/25/24 13:12 V45265TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 03/25/24 13:12 V45265TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 03/25/24 13:12 V45265TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 03/25/24 13:12 V45265TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 03/25/24 13:12 V45265TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 03/25/24 13:12 V45265TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 03/25/24 13:12 V45265TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 03/25/24 13:12 V45265TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 03/25/24 13:12 V45265TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 03/25/24 13:12 V45265TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 03/25/24 13:12 V45265TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 03/25/24 13:12 V45265TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 03/25/24 13:12 V45265TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 03/25/24 13:12 V45265TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 03/25/24 13:12 V45265TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 03/25/24 13:12 V45265TBL
<0.017 mg/Kg - dry 0.017 0.312Ethanol 1 03/25/24 13:12 V45265TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 03/25/24 13:12 V45265TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 03/25/24 13:12 V45265TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 03/25/24 13:12 V45265TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile-A32224
89020 Matrix:
3/22/2024 10:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V45350 03/25/24 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 03/25/24 13:12 V45265TBL
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 03/25/24 13:12 V45265TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 03/25/24 13:12 V45265TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 03/25/24 13:12 V45265TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 03/25/24 13:12 V45265TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 03/25/24 13:12 V45265TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 03/25/24 13:12 V45265TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 03/25/24 13:12 V45265TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 03/25/24 13:12 V45265TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 03/25/24 13:12 V45265TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 03/25/24 13:12 V45265TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 03/25/24 13:12 V45265TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 03/25/24 13:12 V45265TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 03/25/24 13:12 V45265TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 03/25/24 13:12 V45265TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 03/25/24 13:12 V45265TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 03/25/24 13:12 V45265TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 03/25/24 13:12 V45265TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 03/25/24 13:12 V45265TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 03/25/24 13:12 V45265TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 03/25/24 13:12 V45265TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 03/25/24 13:12 V45265TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile-A32224
89020 Matrix:
3/22/2024 10:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V45350 03/25/24 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 03/25/24 13:12 V45265TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 03/25/24 13:12 V45265TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 03/25/24 13:12 V45265TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 03/25/24 13:12 V45265TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 03/25/24 13:12 V45265TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 03/25/24 13:12 V45265TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 03/25/24 13:12 V45265
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%03/25/24 13:121 TBL V45265
Surrogate: Dibromofluoromethane 107 Limits: 84-123%03/25/24 13:121 TBL V45265
Surrogate: Toluene-d8 83.9 Limits: 76-129%03/25/24 13:121 TBL V45265
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V45267 03/26/24 11:30
<0.183 mg/Kg - dry 0.183 0.823Acenaphthene 1 03/27/24 19:21 V45311AMP
<0.187 mg/Kg - dry 0.187 0.823Acenaphthylene 1 03/27/24 19:21 V45311AMP
<0.262 mg/Kg - dry 0.262 0.823Aniline 1 03/27/24 19:21 V45311AMP
<0.207 mg/Kg - dry 0.207 0.823Anthracene 1 03/27/24 19:21 V45311AMP
<0.194 mg/Kg - dry 0.194 0.823Benzo(a)anthracene 1 03/27/24 19:21 V45311AMP
<0.205 mg/Kg - dry 0.205 0.823Benzo(a)pyrene 1 03/27/24 19:21 V45311AMP
<0.183 mg/Kg - dry 0.183 0.823Benzo(b)fluoranthene 1 03/27/24 19:21 V45311AMP
<0.179 mg/Kg - dry 0.179 0.823Benzo(g,h,i)perylene 1 03/27/24 19:21 V45311AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile-A32224
89020 Matrix:
3/22/2024 10:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V45267 03/26/24 11:30
<0.194 mg/Kg - dry 0.194 0.823Benzo(k)fluoranthene 1 03/27/24 19:21 V45311AMP
<0.724 mg/Kg - dry 0.724 2.50Benzoic Acid 1 03/27/24 19:21 V45311AMP
<0.194 mg/Kg - dry 0.194 0.823Benzyl alcohol 1 03/27/24 19:21 V45311AMP
<0.172 mg/Kg - dry 0.172 0.823Bis(2-Chloroethoxy)methane 1 03/27/24 19:21 V45311AMP
<0.152 mg/Kg - dry 0.152 0.823Bis(2-Chloroethyl)ether 1 03/27/24 19:21 V45311AMP
<0.163 mg/Kg - dry 0.163 0.411Bis(2-Chloroisopropyl)ether 1 03/27/24 19:21 V45311AMP
<0.220 mg/Kg - dry 0.220 0.823Bis(2-ethylhexyl)phthalate 1 03/27/24 19:21 V45311AMP
<0.197 mg/Kg - dry 0.197 0.8234-Bromophenyl phenyl ether 1 03/27/24 19:21 V45311AMP
<0.199 mg/Kg - dry 0.199 0.411Butyl benzyl phthalate 1 03/27/24 19:21 V45311AMP
<0.186 mg/Kg - dry 0.186 0.8234-Chloro-3-methylphenol 1 03/27/24 19:21 V45311AMP
<0.187 mg/Kg - dry 0.187 0.4114-Chloroaniline 1 03/27/24 19:21 V45311AMP
<0.192 mg/Kg - dry 0.192 0.8232-Chloronaphthalene 1 03/27/24 19:21 V45311AMP
<0.177 mg/Kg - dry 0.177 0.8232-Chlorophenol 1 03/27/24 19:21 V45311AMP
<0.183 mg/Kg - dry 0.183 1.254-Chlorophenyl phenyl ether 1 03/27/24 19:21 V45311AMP
<0.182 mg/Kg - dry 0.182 0.823Chrysene 1 03/27/24 19:21 V45311AMP
<0.138 mg/Kg - dry 0.138 0.823Dibenz(a,h)anthracene 1 03/27/24 19:21 V45311AMP
<0.197 mg/Kg - dry 0.197 0.823Dibenzofuran 1 03/27/24 19:21 V45311AMP
<0.159 mg/Kg - dry 0.159 0.8231,2-Dichlorobenzene 1 03/27/24 19:21 V45311AMP
<0.156 mg/Kg - dry 0.156 0.8231,3-Dichlorobenzene 1 03/27/24 19:21 V45311AMP
<0.147 mg/Kg - dry 0.147 0.4111,4-Dichlorobenzene 1 03/27/24 19:21 V45311AMP
<0.187 mg/Kg - dry 0.187 0.8233,3'-Dichlorobenzidine 1 03/27/24 19:21 V45311AMP
<0.174 mg/Kg - dry 0.174 0.8232,4-Dichlorophenol 1 03/27/24 19:21 V45311AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile-A32224
89020 Matrix:
3/22/2024 10:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V45267 03/26/24 11:30
<0.183 mg/Kg - dry 0.183 0.823Diethyl phthalate 1 03/27/24 19:21 V45311AMP
<0.196 mg/Kg - dry 0.196 0.823Dimethyl phthalate 1 03/27/24 19:21 V45311AMP
<0.264 mg/Kg - dry 0.264 0.8232,4-Dimethylphenol 1 03/27/24 19:21 V45311AMP
<0.213 mg/Kg - dry 0.213 0.823Di-n-butyl phthalate 1 03/27/24 19:21 V45311AMP
<0.299 mg/Kg - dry 0.299 1.874,6-Dinitro-2-methylphenol 1 03/27/24 19:21 V45311AMP
<0.649 mg/Kg - dry 0.649 1.872,4-Dinitrophenol 1 03/27/24 19:21 V45311AMP
<0.200 mg/Kg - dry 0.200 0.8232,4-Dinitrotoluene 1 03/27/24 19:21 V45311AMP
<0.207 mg/Kg - dry 0.207 0.8232,6-Dinitrotoluene 1 03/27/24 19:21 V45311AMP
<0.203 mg/Kg - dry 0.203 0.411Di-n-Octyl Phthalate 1 03/27/24 19:21 V45311AMP
<0.197 mg/Kg - dry 0.197 0.823Fluoranthene 1 03/27/24 19:21 V45311AMP
<0.191 mg/Kg - dry 0.191 0.823Fluorene 1 03/27/24 19:21 V45311AMP
<0.187 mg/Kg - dry 0.187 0.823Hexachlorobenzene 1 03/27/24 19:21 V45311AMP
<0.121 mg/Kg - dry 0.121 0.823Hexachlorobutadiene 1 03/27/24 19:21 V45311AMP
<0.152 mg/Kg - dry 0.152 0.823Hexachloroethane 1 03/27/24 19:21 V45311AMP
<0.188 mg/Kg - dry 0.188 0.823Indeno(1,2,3-cd)pyrene 1 03/27/24 19:21 V45311AMP
<0.151 mg/Kg - dry 0.151 0.823Isophorone 1 03/27/24 19:21 V45311AMP
<0.173 mg/Kg - dry 0.173 0.8231-Methylnaphthalene 1 03/27/24 19:21 V45311AMP
<0.179 mg/Kg - dry 0.179 0.8232-Methylnaphthalene 1 03/27/24 19:21 V45311AMP
<0.158 mg/Kg - dry 0.158 0.8232-Methylphenol 1 03/27/24 19:21 V45311AMP
<0.159 mg/Kg - dry 0.159 0.8233&4 Methylphenol 1 03/27/24 19:21 V45311AMP
<0.166 mg/Kg - dry 0.166 0.823Naphthalene 1 03/27/24 19:21 V45311AMP
<0.164 mg/Kg - dry 0.164 0.8232-Nitroaniline 1 03/27/24 19:21 V45311AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile-A32224
89020 Matrix:
3/22/2024 10:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V45267 03/26/24 11:30
<0.193 mg/Kg - dry 0.193 0.8233-Nitroaniline 1 03/27/24 19:21 V45311AMP
<0.169 mg/Kg - dry 0.169 0.4114-Nitroaniline 1 03/27/24 19:21 V45311AMP
<0.161 mg/Kg - dry 0.161 0.411Nitrobenzene 1 03/27/24 19:21 V45311AMP
<0.166 mg/Kg - dry 0.166 0.8232-Nitrophenol 1 03/27/24 19:21 V45311AMP
<0.208 mg/Kg - dry 0.208 0.8234-Nitrophenol 1 03/27/24 19:21 V45311AMP
<0.328 mg/Kg - dry 0.328 0.823N-Nitrosodimethylamine 1 03/27/24 19:21 V45311AMP
<0.227 mg/Kg - dry 0.227 0.823N-Nitrosodiphenylamine 1 03/27/24 19:21 V45311AMP
<0.184 mg/Kg - dry 0.184 0.823N-Nitroso-di-n-propylamine 1 03/27/24 19:21 V45311AMP
<0.433 mg/Kg - dry 0.433 1.25Pentachlorophenol 1 03/27/24 19:21 V45311AMP
<0.197 mg/Kg - dry 0.197 0.823Phenanthrene 1 03/27/24 19:21 V45311AMP
<0.177 mg/Kg - dry 0.177 0.823Phenol 1 03/27/24 19:21 V45311AMP
<0.199 mg/Kg - dry 0.199 0.823Pyrene 1 03/27/24 19:21 V45311AMP
<0.095 mg/Kg - dry 0.095 0.411Pyridine 1 03/27/24 19:21 V45311AMP
<0.164 mg/Kg - dry 0.164 0.8231,2,4-Trichlorobenzene 1 03/27/24 19:21 V45311AMP
<0.178 mg/Kg - dry 0.178 0.8232,4,5-Trichlorophenol 1 03/27/24 19:21 V45311AMP
<0.174 mg/Kg - dry 0.174 0.8232,4,6-Trichlorophenol 1 03/27/24 19:21 V45311AMP
8270ESurrogate: Phenol-d5 72.1 Limits: 34-121%03/27/24 19:211 AMP
Surrogate: 2-Fluorobiphenyl 73.7 Limits: 44-115%03/27/24 19:211 AMP V45311
Surrogate: 2-Fluorophenol 75.1 Limits: 35-115%03/27/24 19:211 AMP V45311
Surrogate: Nitrobenzene-d5 82.0 Limits: 37-122%03/27/24 19:211 AMP V45311
Surrogate: 4-Terphenyl-d14 74.9 Limits: 54-127%03/27/24 19:211 AMP V45311
Surrogate: 2,4,6-Tribromophenol 72.1 Limits: 39-132%03/27/24 19:211 AMP V45311
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile-B32224
89021 Matrix:
3/22/2024 11:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
16.8 %Moisture 1 03/25/24 16:25 SW-DRYWTPEB
0.270 mg/Kg - dry 0.169 0.240Chromium, Hexavalent 1 03/29/24 16:51 SW-7199MKD
1.05 mg/Kg - dry 0.103 0.300Arsenic 5 04/01/24 16:01 6020BCPW
135 mg/Kg - dry 0.051 0.300Barium 5 03/29/24 17:55 6020BCPW
0.0355 J mg/Kg - dry 0.0312 0.300Cadmium 5 03/29/24 17:55 6020BCPW
68.8 mg/Kg - dry 0.139 0.300Chromium 5 04/01/24 16:01 6020BCPW
7.98 mg/Kg - dry 0.0372 0.300Lead 5 03/29/24 17:55 6020BCPW
0.0272 J mg/Kg - dry 0.0144 0.0361Mercury (Total)1 03/28/24 13:00 7471BNPC
0.155 J mg/Kg - dry 0.123 0.300Selenium 5 04/01/24 16:01 6020BCPW
<0.300 mg/Kg - dry 0.0081 0.300Silver 5 03/29/24 17:55 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile-B32224
89021 Matrix:
3/22/2024 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V45351 03/26/24 08:00
0.033 mg/Kg - dry 0.002 0.024Acetone 1 03/26/24 16:53 V45352TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 03/26/24 16:53 V45352TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 03/26/24 16:53 V45352TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 03/26/24 16:53 V45352TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 03/26/24 16:53 V45352TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 03/26/24 16:53 V45352TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 03/26/24 16:53 V45352TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 03/26/24 16:53 V45352TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 03/26/24 16:53 V45352TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 03/26/24 16:53 V45352TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 03/26/24 16:53 V45352TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 03/26/24 16:53 V45352TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 03/26/24 16:53 V45352TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 03/26/24 16:53 V45352TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 03/26/24 16:53 V45352TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 03/26/24 16:53 V45352TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 03/26/24 16:53 V45352TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 03/26/24 16:53 V45352TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 03/26/24 16:53 V45352TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 03/26/24 16:53 V45352TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 03/26/24 16:53 V45352TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 03/26/24 16:53 V45352TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile-B32224
89021 Matrix:
3/22/2024 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V45351 03/26/24 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 03/26/24 16:53 V45352TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 03/26/24 16:53 V45352TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 03/26/24 16:53 V45352TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 03/26/24 16:53 V45352TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 03/26/24 16:53 V45352TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 03/26/24 16:53 V45352TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 03/26/24 16:53 V45352TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 03/26/24 16:53 V45352TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 03/26/24 16:53 V45352TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 03/26/24 16:53 V45352TBL
<0.0009 mg/Kg - dry 0.0009 0.006cis-1,2-Dichloroethene 1 03/26/24 16:53 V45352TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 03/26/24 16:53 V45352TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 03/26/24 16:53 V45352TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 03/26/24 16:53 V45352TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 03/26/24 16:53 V45352TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 03/26/24 16:53 V45352TBL
<0.0006 mg/Kg - dry 0.0006 0.006cis-1,3-Dichloropropene 1 03/26/24 16:53 V45352TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 03/26/24 16:53 V45352TBL
0.231 J mg/Kg - dry 0.016 0.300Ethanol 1 03/26/24 16:53 V45352TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 03/26/24 16:53 V45352TBL
<0.0010 mg/Kg - dry 0.0010 0.060Ethyl Tertiary Butyl Ether (ETBE)1 03/26/24 16:53 V45352TBL
<0.0009 mg/Kg - dry 0.0009 0.012Hexachlorobutadiene 1 03/26/24 16:53 V45352TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile-B32224
89021 Matrix:
3/22/2024 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V45351 03/26/24 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 03/26/24 16:53 V45352TBL
<0.0007 mg/Kg - dry 0.0007 0.0242-Hexanone 1 03/26/24 16:53 V45352TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 03/26/24 16:53 V45352TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 03/26/24 16:53 V45352TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 03/26/24 16:53 V45352TBL
<0.0007 mg/Kg - dry 0.0007 0.006Methyl tert-butyl ether (MTBE)1 03/26/24 16:53 V45352TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 03/26/24 16:53 V45352TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 03/26/24 16:53 V45352TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 03/26/24 16:53 V45352TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Propylbenzene 1 03/26/24 16:53 V45352TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 03/26/24 16:53 V45352TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 03/26/24 16:53 V45352TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 03/26/24 16:53 V45352TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 03/26/24 16:53 V45352TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 03/26/24 16:53 V45352TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2,3-Trichlorobenzene 1 03/26/24 16:53 V45352TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 03/26/24 16:53 V45352TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 03/26/24 16:53 V45352TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 03/26/24 16:53 V45352TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 03/26/24 16:53 V45352TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 03/26/24 16:53 V45352TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 03/26/24 16:53 V45352TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile-B32224
89021 Matrix:
3/22/2024 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V45351 03/26/24 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 03/26/24 16:53 V45352TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,3,5-Trimethylbenzene 1 03/26/24 16:53 V45352TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 03/26/24 16:53 V45352TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 03/26/24 16:53 V45352TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 03/26/24 16:53 V45352TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 03/26/24 16:53 V45352TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 03/26/24 16:53 V45352
Surrogate: 4-Bromofluorobenzene 105 Limits: 70-130%03/25/24 13:391 TBL V45265
Surrogate: Dibromofluoromethane 108 Limits: 84-123%03/25/24 13:391 TBL V45265
Surrogate: Toluene-d8 86.2 Limits: 76-129%03/25/24 13:391 TBL V45265
Surrogate: 4-Bromofluorobenzene 106 Limits: 70-130%03/26/24 16:531 TBL V45352
Surrogate: Dibromofluoromethane 106 Limits: 84-123%03/26/24 16:531 TBL V45352
Surrogate: Toluene-d8 84.4 Limits: 76-129%03/26/24 16:531 TBL V45352
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V45267 03/26/24 11:30
<0.176 mg/Kg - dry 0.176 0.793Acenaphthene 1 03/27/24 20:31 V45311AMP
<0.180 mg/Kg - dry 0.180 0.793Acenaphthylene 1 03/27/24 20:31 V45311AMP
<0.252 mg/Kg - dry 0.252 0.793Aniline 1 03/27/24 20:31 V45311AMP
<0.199 mg/Kg - dry 0.199 0.793Anthracene 1 03/27/24 20:31 V45311AMP
<0.187 mg/Kg - dry 0.187 0.793Benzo(a)anthracene 1 03/27/24 20:31 V45311AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile-B32224
89021 Matrix:
3/22/2024 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V45267 03/26/24 11:30
<0.198 mg/Kg - dry 0.198 0.793Benzo(a)pyrene 1 03/27/24 20:31 V45311AMP
<0.176 mg/Kg - dry 0.176 0.793Benzo(b)fluoranthene 1 03/27/24 20:31 V45311AMP
<0.173 mg/Kg - dry 0.173 0.793Benzo(g,h,i)perylene 1 03/27/24 20:31 V45311AMP
<0.187 mg/Kg - dry 0.187 0.793Benzo(k)fluoranthene 1 03/27/24 20:31 V45311AMP
<0.697 mg/Kg - dry 0.697 2.40Benzoic Acid 1 03/27/24 20:31 V45311AMP
<0.187 mg/Kg - dry 0.187 0.793Benzyl alcohol 1 03/27/24 20:31 V45311AMP
<0.165 mg/Kg - dry 0.165 0.793Bis(2-Chloroethoxy)methane 1 03/27/24 20:31 V45311AMP
<0.146 mg/Kg - dry 0.146 0.793Bis(2-Chloroethyl)ether 1 03/27/24 20:31 V45311AMP
<0.157 mg/Kg - dry 0.157 0.396Bis(2-Chloroisopropyl)ether 1 03/27/24 20:31 V45311AMP
<0.212 mg/Kg - dry 0.212 0.793Bis(2-ethylhexyl)phthalate 1 03/27/24 20:31 V45311AMP
<0.189 mg/Kg - dry 0.189 0.7934-Bromophenyl phenyl ether 1 03/27/24 20:31 V45311AMP
<0.192 mg/Kg - dry 0.192 0.396Butyl benzyl phthalate 1 03/27/24 20:31 V45311AMP
<0.179 mg/Kg - dry 0.179 0.7934-Chloro-3-methylphenol 1 03/27/24 20:31 V45311AMP
<0.180 mg/Kg - dry 0.180 0.3964-Chloroaniline 1 03/27/24 20:31 V45311AMP
<0.185 mg/Kg - dry 0.185 0.7932-Chloronaphthalene 1 03/27/24 20:31 V45311AMP
<0.170 mg/Kg - dry 0.170 0.7932-Chlorophenol 1 03/27/24 20:31 V45311AMP
<0.176 mg/Kg - dry 0.176 1.204-Chlorophenyl phenyl ether 1 03/27/24 20:31 V45311AMP
<0.175 mg/Kg - dry 0.175 0.793Chrysene 1 03/27/24 20:31 V45311AMP
<0.133 mg/Kg - dry 0.133 0.793Dibenz(a,h)anthracene 1 03/27/24 20:31 V45311AMP
<0.189 mg/Kg - dry 0.189 0.793Dibenzofuran 1 03/27/24 20:31 V45311AMP
<0.153 mg/Kg - dry 0.153 0.7931,2-Dichlorobenzene 1 03/27/24 20:31 V45311AMP
<0.150 mg/Kg - dry 0.150 0.7931,3-Dichlorobenzene 1 03/27/24 20:31 V45311AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile-B32224
89021 Matrix:
3/22/2024 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V45267 03/26/24 11:30
<0.141 mg/Kg - dry 0.141 0.3961,4-Dichlorobenzene 1 03/27/24 20:31 V45311AMP
<0.180 mg/Kg - dry 0.180 0.7933,3'-Dichlorobenzidine 1 03/27/24 20:31 V45311AMP
<0.168 mg/Kg - dry 0.168 0.7932,4-Dichlorophenol 1 03/27/24 20:31 V45311AMP
<0.176 mg/Kg - dry 0.176 0.793Diethyl phthalate 1 03/27/24 20:31 V45311AMP
<0.188 mg/Kg - dry 0.188 0.793Dimethyl phthalate 1 03/27/24 20:31 V45311AMP
<0.254 mg/Kg - dry 0.254 0.7932,4-Dimethylphenol 1 03/27/24 20:31 V45311AMP
<0.205 mg/Kg - dry 0.205 0.793Di-n-butyl phthalate 1 03/27/24 20:31 V45311AMP
<0.288 mg/Kg - dry 0.288 1.804,6-Dinitro-2-methylphenol 1 03/27/24 20:31 V45311AMP
<0.625 mg/Kg - dry 0.625 1.802,4-Dinitrophenol 1 03/27/24 20:31 V45311AMP
<0.193 mg/Kg - dry 0.193 0.7932,4-Dinitrotoluene 1 03/27/24 20:31 V45311AMP
<0.199 mg/Kg - dry 0.199 0.7932,6-Dinitrotoluene 1 03/27/24 20:31 V45311AMP
<0.195 mg/Kg - dry 0.195 0.396Di-n-Octyl Phthalate 1 03/27/24 20:31 V45311AMP
<0.189 mg/Kg - dry 0.189 0.793Fluoranthene 1 03/27/24 20:31 V45311AMP
<0.183 mg/Kg - dry 0.183 0.793Fluorene 1 03/27/24 20:31 V45311AMP
<0.180 mg/Kg - dry 0.180 0.793Hexachlorobenzene 1 03/27/24 20:31 V45311AMP
<0.117 mg/Kg - dry 0.117 0.793Hexachlorobutadiene 1 03/27/24 20:31 V45311AMP
<0.146 mg/Kg - dry 0.146 0.793Hexachloroethane 1 03/27/24 20:31 V45311AMP
<0.181 mg/Kg - dry 0.181 0.793Indeno(1,2,3-cd)pyrene 1 03/27/24 20:31 V45311AMP
<0.145 mg/Kg - dry 0.145 0.793Isophorone 1 03/27/24 20:31 V45311AMP
<0.167 mg/Kg - dry 0.167 0.7931-Methylnaphthalene 1 03/27/24 20:31 V45311AMP
<0.173 mg/Kg - dry 0.173 0.7932-Methylnaphthalene 1 03/27/24 20:31 V45311AMP
<0.152 mg/Kg - dry 0.152 0.7932-Methylphenol 1 03/27/24 20:31 V45311AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile-B32224
89021 Matrix:
3/22/2024 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V45267 03/26/24 11:30
<0.153 mg/Kg - dry 0.153 0.7933&4 Methylphenol 1 03/27/24 20:31 V45311AMP
<0.159 mg/Kg - dry 0.159 0.793Naphthalene 1 03/27/24 20:31 V45311AMP
<0.158 mg/Kg - dry 0.158 0.7932-Nitroaniline 1 03/27/24 20:31 V45311AMP
<0.186 mg/Kg - dry 0.186 0.7933-Nitroaniline 1 03/27/24 20:31 V45311AMP
<0.163 mg/Kg - dry 0.163 0.3964-Nitroaniline 1 03/27/24 20:31 V45311AMP
<0.155 mg/Kg - dry 0.155 0.396Nitrobenzene 1 03/27/24 20:31 V45311AMP
<0.159 mg/Kg - dry 0.159 0.7932-Nitrophenol 1 03/27/24 20:31 V45311AMP
<0.200 mg/Kg - dry 0.200 0.7934-Nitrophenol 1 03/27/24 20:31 V45311AMP
<0.316 mg/Kg - dry 0.316 0.793N-Nitrosodimethylamine 1 03/27/24 20:31 V45311AMP
<0.218 mg/Kg - dry 0.218 0.793N-Nitrosodiphenylamine 1 03/27/24 20:31 V45311AMP
<0.177 mg/Kg - dry 0.177 0.793N-Nitroso-di-n-propylamine 1 03/27/24 20:31 V45311AMP
<0.417 mg/Kg - dry 0.417 1.20Pentachlorophenol 1 03/27/24 20:31 V45311AMP
<0.189 mg/Kg - dry 0.189 0.793Phenanthrene 1 03/27/24 20:31 V45311AMP
<0.170 mg/Kg - dry 0.170 0.793Phenol 1 03/27/24 20:31 V45311AMP
<0.192 mg/Kg - dry 0.192 0.793Pyrene 1 03/27/24 20:31 V45311AMP
<0.092 mg/Kg - dry 0.092 0.396Pyridine 1 03/27/24 20:31 V45311AMP
<0.158 mg/Kg - dry 0.158 0.7931,2,4-Trichlorobenzene 1 03/27/24 20:31 V45311AMP
<0.171 mg/Kg - dry 0.171 0.7932,4,5-Trichlorophenol 1 03/27/24 20:31 V45311AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile-B32224
89021 Matrix:
3/22/2024 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V45267 03/26/24 11:30
<0.168 mg/Kg - dry 0.168 0.7932,4,6-Trichlorophenol 1 03/27/24 20:31 V45311AMP
8270ESurrogate: Phenol-d5 77.2 Limits: 34-121%03/27/24 20:311 AMP
Surrogate: 2-Fluorobiphenyl 76.0 Limits: 44-115%03/27/24 20:311 AMP V45311
Surrogate: 2-Fluorophenol 82.3 Limits: 35-115%03/27/24 20:311 AMP V45311
Surrogate: Nitrobenzene-d5 83.2 Limits: 37-122%03/27/24 20:311 AMP V45311
Surrogate: 4-Terphenyl-d14 80.8 Limits: 54-127%03/27/24 20:311 AMP V45311
Surrogate: 2,4,6-Tribromophenol 83.5 Limits: 39-132%03/27/24 20:311 AMP V45311
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile DUP-32224
89022 Matrix:
3/22/2024 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.3 %Moisture 1 03/25/24 16:25 SW-DRYWTPEB
0.298 mg/Kg - dry 0.174 0.247Chromium, Hexavalent 1 03/29/24 17:02 SW-7199MKD
1.29 mg/Kg - dry 0.106 0.310Arsenic 5 04/01/24 16:07 6020BCPW
105 mg/Kg - dry 0.053 0.309Barium 5 03/29/24 18:00 6020BCPW
0.0448 J mg/Kg - dry 0.0322 0.310Cadmium 5 03/29/24 18:00 6020BCPW
82.0 mg/Kg - dry 0.143 0.309Chromium 5 04/01/24 16:07 6020BCPW
10.2 mg/Kg - dry 0.0384 0.310Lead 5 03/29/24 18:00 6020BCPW
0.0375 mg/Kg - dry 0.0149 0.0372Mercury (Total)1 03/28/24 13:03 7471BNPC
0.240 J mg/Kg - dry 0.127 0.309Selenium 5 04/01/24 16:07 6020BCPW
<0.310 mg/Kg - dry 0.0083 0.310Silver 5 03/29/24 18:00 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile DUP-32224
89022 Matrix:
3/22/2024 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V45350 03/25/24 08:00
0.012 J mg/Kg - dry 0.002 0.024Acetone 1 03/25/24 14:06 V45265TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 03/25/24 14:06 V45265TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 03/25/24 14:06 V45265TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 03/25/24 14:06 V45265TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 03/25/24 14:06 V45265TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 03/25/24 14:06 V45265TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 03/25/24 14:06 V45265TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 03/25/24 14:06 V45265TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 03/25/24 14:06 V45265TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 03/25/24 14:06 V45265TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 03/25/24 14:06 V45265TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 03/25/24 14:06 V45265TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 03/25/24 14:06 V45265TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 03/25/24 14:06 V45265TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 03/25/24 14:06 V45265TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 03/25/24 14:06 V45265TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 03/25/24 14:06 V45265TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 03/25/24 14:06 V45265TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 03/25/24 14:06 V45265TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 03/25/24 14:06 V45265TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 03/25/24 14:06 V45265TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 03/25/24 14:06 V45265TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile DUP-32224
89022 Matrix:
3/22/2024 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V45350 03/25/24 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 03/25/24 14:06 V45265TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 03/25/24 14:06 V45265TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 03/25/24 14:06 V45265TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 03/25/24 14:06 V45265TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 03/25/24 14:06 V45265TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 03/25/24 14:06 V45265TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 03/25/24 14:06 V45265TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 03/25/24 14:06 V45265TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 03/25/24 14:06 V45265TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 03/25/24 14:06 V45265TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 03/25/24 14:06 V45265TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 03/25/24 14:06 V45265TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 03/25/24 14:06 V45265TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 03/25/24 14:06 V45265TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 03/25/24 14:06 V45265TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 03/25/24 14:06 V45265TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 03/25/24 14:06 V45265TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 03/25/24 14:06 V45265TBL
<0.017 mg/Kg - dry 0.017 0.309Ethanol 1 03/25/24 14:06 V45265TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 03/25/24 14:06 V45265TBL
<0.001 mg/Kg - dry 0.001 0.061Ethyl Tertiary Butyl Ether (ETBE)1 03/25/24 14:06 V45265TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 03/25/24 14:06 V45265TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile DUP-32224
89022 Matrix:
3/22/2024 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V45350 03/25/24 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 03/25/24 14:06 V45265TBL
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 03/25/24 14:06 V45265TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 03/25/24 14:06 V45265TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 03/25/24 14:06 V45265TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 03/25/24 14:06 V45265TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 03/25/24 14:06 V45265TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 03/25/24 14:06 V45265TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 03/25/24 14:06 V45265TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 03/25/24 14:06 V45265TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 03/25/24 14:06 V45265TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 03/25/24 14:06 V45265TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 03/25/24 14:06 V45265TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 03/25/24 14:06 V45265TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 03/25/24 14:06 V45265TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 03/25/24 14:06 V45265TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 03/25/24 14:06 V45265TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 03/25/24 14:06 V45265TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 03/25/24 14:06 V45265TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 03/25/24 14:06 V45265TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 03/25/24 14:06 V45265TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 03/25/24 14:06 V45265TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 03/25/24 14:06 V45265TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile DUP-32224
89022 Matrix:
3/22/2024 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V45350 03/25/24 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 03/25/24 14:06 V45265TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 03/25/24 14:06 V45265TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 03/25/24 14:06 V45265TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 03/25/24 14:06 V45265TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 03/25/24 14:06 V45265TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 03/25/24 14:06 V45265TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 03/25/24 14:06 V45265
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%03/25/24 14:061 TBL V45265
Surrogate: Dibromofluoromethane 108 Limits: 84-123%03/25/24 14:061 TBL V45265
Surrogate: Toluene-d8 83.7 Limits: 76-129%03/25/24 14:061 TBL V45265
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V45267 03/26/24 11:30
<0.182 mg/Kg - dry 0.182 0.817Acenaphthene 1 03/27/24 19:44 V45311AMP
<0.185 mg/Kg - dry 0.185 0.817Acenaphthylene 1 03/27/24 19:44 V45311AMP
<0.260 mg/Kg - dry 0.260 0.817Aniline 1 03/27/24 19:44 V45311AMP
<0.205 mg/Kg - dry 0.205 0.817Anthracene 1 03/27/24 19:44 V45311AMP
<0.193 mg/Kg - dry 0.193 0.817Benzo(a)anthracene 1 03/27/24 19:44 V45311AMP
<0.204 mg/Kg - dry 0.204 0.817Benzo(a)pyrene 1 03/27/24 19:44 V45311AMP
<0.182 mg/Kg - dry 0.182 0.817Benzo(b)fluoranthene 1 03/27/24 19:44 V45311AMP
<0.178 mg/Kg - dry 0.178 0.817Benzo(g,h,i)perylene 1 03/27/24 19:44 V45311AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile DUP-32224
89022 Matrix:
3/22/2024 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V45267 03/26/24 11:30
<0.193 mg/Kg - dry 0.193 0.817Benzo(k)fluoranthene 1 03/27/24 19:44 V45311AMP
<0.718 mg/Kg - dry 0.718 2.48Benzoic Acid 1 03/27/24 19:44 V45311AMP
<0.193 mg/Kg - dry 0.193 0.817Benzyl alcohol 1 03/27/24 19:44 V45311AMP
<0.171 mg/Kg - dry 0.171 0.817Bis(2-Chloroethoxy)methane 1 03/27/24 19:44 V45311AMP
<0.151 mg/Kg - dry 0.151 0.817Bis(2-Chloroethyl)ether 1 03/27/24 19:44 V45311AMP
<0.162 mg/Kg - dry 0.162 0.408Bis(2-Chloroisopropyl)ether 1 03/27/24 19:44 V45311AMP
<0.219 mg/Kg - dry 0.219 0.817Bis(2-ethylhexyl)phthalate 1 03/27/24 19:44 V45311AMP
<0.195 mg/Kg - dry 0.195 0.8174-Bromophenyl phenyl ether 1 03/27/24 19:44 V45311AMP
<0.198 mg/Kg - dry 0.198 0.408Butyl benzyl phthalate 1 03/27/24 19:44 V45311AMP
<0.184 mg/Kg - dry 0.184 0.8174-Chloro-3-methylphenol 1 03/27/24 19:44 V45311AMP
<0.185 mg/Kg - dry 0.185 0.4084-Chloroaniline 1 03/27/24 19:44 V45311AMP
<0.190 mg/Kg - dry 0.190 0.8172-Chloronaphthalene 1 03/27/24 19:44 V45311AMP
<0.175 mg/Kg - dry 0.175 0.8172-Chlorophenol 1 03/27/24 19:44 V45311AMP
<0.182 mg/Kg - dry 0.182 1.244-Chlorophenyl phenyl ether 1 03/27/24 19:44 V45311AMP
<0.180 mg/Kg - dry 0.180 0.817Chrysene 1 03/27/24 19:44 V45311AMP
<0.137 mg/Kg - dry 0.137 0.817Dibenz(a,h)anthracene 1 03/27/24 19:44 V45311AMP
<0.195 mg/Kg - dry 0.195 0.817Dibenzofuran 1 03/27/24 19:44 V45311AMP
<0.158 mg/Kg - dry 0.158 0.8171,2-Dichlorobenzene 1 03/27/24 19:44 V45311AMP
<0.154 mg/Kg - dry 0.154 0.8171,3-Dichlorobenzene 1 03/27/24 19:44 V45311AMP
<0.146 mg/Kg - dry 0.146 0.4081,4-Dichlorobenzene 1 03/27/24 19:44 V45311AMP
<0.185 mg/Kg - dry 0.185 0.8173,3'-Dichlorobenzidine 1 03/27/24 19:44 V45311AMP
<0.173 mg/Kg - dry 0.173 0.8172,4-Dichlorophenol 1 03/27/24 19:44 V45311AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile DUP-32224
89022 Matrix:
3/22/2024 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V45267 03/26/24 11:30
<0.182 mg/Kg - dry 0.182 0.817Diethyl phthalate 1 03/27/24 19:44 V45311AMP
<0.194 mg/Kg - dry 0.194 0.817Dimethyl phthalate 1 03/27/24 19:44 V45311AMP
<0.262 mg/Kg - dry 0.262 0.8172,4-Dimethylphenol 1 03/27/24 19:44 V45311AMP
<0.211 mg/Kg - dry 0.211 0.817Di-n-butyl phthalate 1 03/27/24 19:44 V45311AMP
<0.297 mg/Kg - dry 0.297 1.864,6-Dinitro-2-methylphenol 1 03/27/24 19:44 V45311AMP
<0.644 mg/Kg - dry 0.644 1.862,4-Dinitrophenol 1 03/27/24 19:44 V45311AMP
<0.199 mg/Kg - dry 0.199 0.8172,4-Dinitrotoluene 1 03/27/24 19:44 V45311AMP
<0.205 mg/Kg - dry 0.205 0.8172,6-Dinitrotoluene 1 03/27/24 19:44 V45311AMP
<0.201 mg/Kg - dry 0.201 0.408Di-n-Octyl Phthalate 1 03/27/24 19:44 V45311AMP
<0.195 mg/Kg - dry 0.195 0.817Fluoranthene 1 03/27/24 19:44 V45311AMP
<0.189 mg/Kg - dry 0.189 0.817Fluorene 1 03/27/24 19:44 V45311AMP
<0.185 mg/Kg - dry 0.185 0.817Hexachlorobenzene 1 03/27/24 19:44 V45311AMP
<0.120 mg/Kg - dry 0.120 0.817Hexachlorobutadiene 1 03/27/24 19:44 V45311AMP
<0.151 mg/Kg - dry 0.151 0.817Hexachloroethane 1 03/27/24 19:44 V45311AMP
<0.187 mg/Kg - dry 0.187 0.817Indeno(1,2,3-cd)pyrene 1 03/27/24 19:44 V45311AMP
<0.149 mg/Kg - dry 0.149 0.817Isophorone 1 03/27/24 19:44 V45311AMP
<0.172 mg/Kg - dry 0.172 0.8171-Methylnaphthalene 1 03/27/24 19:44 V45311AMP
<0.178 mg/Kg - dry 0.178 0.8172-Methylnaphthalene 1 03/27/24 19:44 V45311AMP
<0.157 mg/Kg - dry 0.157 0.8172-Methylphenol 1 03/27/24 19:44 V45311AMP
<0.158 mg/Kg - dry 0.158 0.8173&4 Methylphenol 1 03/27/24 19:44 V45311AMP
<0.164 mg/Kg - dry 0.164 0.817Naphthalene 1 03/27/24 19:44 V45311AMP
<0.163 mg/Kg - dry 0.163 0.8172-Nitroaniline 1 03/27/24 19:44 V45311AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
24-082-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 03/22/2024
BWR-013
Report Date : 04/02/2024
Sample ID :
Lab No :
Sampled:Stockpile DUP-32224
89022 Matrix:
3/22/2024 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V45267 03/26/24 11:30
<0.192 mg/Kg - dry 0.192 0.8173-Nitroaniline 1 03/27/24 19:44 V45311AMP
<0.168 mg/Kg - dry 0.168 0.4084-Nitroaniline 1 03/27/24 19:44 V45311AMP
<0.159 mg/Kg - dry 0.159 0.408Nitrobenzene 1 03/27/24 19:44 V45311AMP
<0.164 mg/Kg - dry 0.164 0.8172-Nitrophenol 1 03/27/24 19:44 V45311AMP
<0.206 mg/Kg - dry 0.206 0.8174-Nitrophenol 1 03/27/24 19:44 V45311AMP
<0.325 mg/Kg - dry 0.325 0.817N-Nitrosodimethylamine 1 03/27/24 19:44 V45311AMP
<0.225 mg/Kg - dry 0.225 0.817N-Nitrosodiphenylamine 1 03/27/24 19:44 V45311AMP
<0.183 mg/Kg - dry 0.183 0.817N-Nitroso-di-n-propylamine 1 03/27/24 19:44 V45311AMP
<0.429 mg/Kg - dry 0.429 1.24Pentachlorophenol 1 03/27/24 19:44 V45311AMP
<0.195 mg/Kg - dry 0.195 0.817Phenanthrene 1 03/27/24 19:44 V45311AMP
<0.175 mg/Kg - dry 0.175 0.817Phenol 1 03/27/24 19:44 V45311AMP
<0.198 mg/Kg - dry 0.198 0.817Pyrene 1 03/27/24 19:44 V45311AMP
<0.095 mg/Kg - dry 0.095 0.408Pyridine 1 03/27/24 19:44 V45311AMP
<0.163 mg/Kg - dry 0.163 0.8171,2,4-Trichlorobenzene 1 03/27/24 19:44 V45311AMP
<0.177 mg/Kg - dry 0.177 0.8172,4,5-Trichlorophenol 1 03/27/24 19:44 V45311AMP
<0.173 mg/Kg - dry 0.173 0.8172,4,6-Trichlorophenol 1 03/27/24 19:44 V45311AMP
8270ESurrogate: Phenol-d5 78.1 Limits: 34-121%03/27/24 19:441 AMP
Surrogate: 2-Fluorobiphenyl 77.8 Limits: 44-115%03/27/24 19:441 AMP V45311
Surrogate: 2-Fluorophenol 83.8 Limits: 35-115%03/27/24 19:441 AMP V45311
Surrogate: Nitrobenzene-d5 85.6 Limits: 37-122%03/27/24 19:441 AMP V45311
Surrogate: 4-Terphenyl-d14 77.2 Limits: 54-127%03/27/24 19:441 AMP V45311
Surrogate: 2,4,6-Tribromophenol 78.4 Limits: 39-132%03/27/24 19:441 AMP V45311
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 51
Quality Control Data
24-082-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BWR-013
QC Prep Batch Method:
Metals Analyses
6020B
L741761,L742071QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L741544
Associated Lab Samples: 89020, 89021, 89022
LRB-L741544 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
03/29/24 17:420.2500.0855<0.0855mg/KgArsenic
03/29/24 17:420.2500.042<0.042mg/KgBarium
03/29/24 17:420.2500.0260<0.0260mg/KgCadmium
03/29/24 17:420.2500.116<0.116mg/KgChromium
03/29/24 17:420.2500.0310<0.0310mg/KgLead
03/29/24 17:420.2500.103<0.103mg/KgSelenium
03/29/24 17:420.2500.0067<0.0067mg/KgSilver
LCS-L741544Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1082.692.50mg/KgArsenic 80-120
97.04.835.00mg/KgBarium 80-120
96.00.4780.500mg/KgCadmium 80-120
1025.125.00mg/KgChromium 80-120
98.02.452.50mg/KgLead 80-120
1105.495.00mg/KgSelenium 80-120
97.00.4850.500mg/KgSilver 80-120
E 65237-MS-L741544 E 65237-MSD-L741544Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
4.55 1024.202.382.472.04mg/KgArsenic 91.0 75-125 8.0 80
85.3 0.0*78.74.774.9495.7mg/KgBarium 0.0*75-125 8.0 80
0.389 0.0*0.7830.4770.4940.926mg/KgCadmium 0.0*75-125 67.2 80
27.2 0.0*28.44.774.9432.2mg/KgChromium 0.0*75-125 4.3 80
Page 1 of 17* QC Fail Date:04/02/2024 03:48 PM
Page 33 of 51
Quality Control Data
24-082-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BWR-013
QC Prep Batch Method:
Metals Analyses
6020B
L741761,L742071QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L741544
E 65237-MS-L741544 E 65237-MSD-L741544Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
3.10 0.0*3.242.382.473.56mg/KgLead 0.0*75-125 4.4 80
5.99 96.05.464.774.941.23mg/KgSelenium 89.0 75-125 9.2 80
2.22 1072.280.4770.4941.69mg/KgSilver 124 75-125 2.6 80
E 65237-PDS-L741544Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
04/01/24 16:521021.37mg/KgArsenic
03/29/24 19:4579.09.37mg/KgBarium
03/29/24 19:4593.00.298mg/KgCadmium
03/29/24 19:4585.04.67mg/KgChromium
03/29/24 19:4580.01.20mg/KgLead
04/01/24 16:5299.02.40mg/KgSelenium
04/01/24 16:521000.399mg/KgSilver
Page 2 of 17* QC Fail Date:04/02/2024 03:48 PM
Page 34 of 51
Quality Control Data
24-082-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BWR-013
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V45394QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V45315
Associated Lab Samples: 89020, 89021, 89022
LRB-V45315 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
03/28/24 12:520.03000.0120<0.0120mg/KgMercury (Total)
LCS-V45315Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1130.4700.417mg/KgMercury (Total)80-120
V 89240-MS-V45315 V 89240-MSD-V45315Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.443 1020.4420.4170.4030.0308mg/KgMercury (Total)99.0 80-120 0.2 20
V 89240-PDS-V45315Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
03/28/24 13:081000.216mg/KgMercury (Total)
Page 3 of 17Date:04/02/2024 03:48 PM
Page 35 of 51
Quality Control Data
24-082-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BWR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V45352QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V45351
Associated Lab Samples: 89021
LRB-V45351 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/26/24 16:260.0200.002<0.002mg/KgAcetone
03/26/24 16:260.0200.001<0.001mg/KgAcrolein
03/26/24 16:260.0200.0008<0.0008mg/KgAcrylonitrile
03/26/24 16:260.0050.0006<0.0006mg/KgBenzene
03/26/24 16:260.0050.0005<0.0005mg/KgBromobenzene
03/26/24 16:260.0050.0008<0.0008mg/KgBromochloromethane
03/26/24 16:260.0050.001<0.001mg/KgBromodichloromethane
03/26/24 16:260.0050.001<0.001mg/KgBromoform
03/26/24 16:260.0100.001<0.001mg/KgBromomethane
03/26/24 16:260.0050.0005<0.0005mg/Kgn-Butylbenzene
03/26/24 16:260.0050.0006<0.0006mg/Kgsec-Butyl benzene
03/26/24 16:260.0050.0005<0.0005mg/Kgtert-Butyl benzene
03/26/24 16:260.0050.0006<0.0006mg/KgCarbon Disulfide
03/26/24 16:260.0050.001<0.001mg/KgCarbon Tetrachloride
03/26/24 16:260.0050.0007<0.0007mg/KgChlorobenzene
03/26/24 16:260.0050.0009<0.0009mg/KgChlorodibromomethane
03/26/24 16:260.0100.0009<0.0009mg/KgChloroethane
03/26/24 16:260.0050.001<0.001mg/KgChloroform
03/26/24 16:260.0100.0006<0.0006mg/KgChloromethane
03/26/24 16:260.0050.0005<0.0005mg/Kg2-Chlorotoluene
03/26/24 16:260.0050.0004<0.0004mg/Kg4-Chlorotoluene
03/26/24 16:260.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
03/26/24 16:260.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
03/26/24 16:260.0050.0006<0.0006mg/Kg1,2-Dibromoethane
03/26/24 16:260.0050.0006<0.0006mg/KgDibromomethane
03/26/24 16:260.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
03/26/24 16:260.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 4 of 17Date:04/02/2024 03:48 PM
Page 36 of 51
Quality Control Data
24-082-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BWR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V45352QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V45351
Associated Lab Samples: 89021
LRB-V45351 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/26/24 16:260.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
03/26/24 16:260.0100.001<0.001mg/KgDichlorodifluoromethane
03/26/24 16:260.0050.0008<0.0008mg/Kg1,1-Dichloroethane
03/26/24 16:260.0050.001<0.001mg/Kg1,2-Dichloroethane
03/26/24 16:260.0050.0007<0.0007mg/Kg1,1-Dichloroethene
03/26/24 16:260.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
03/26/24 16:260.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
03/26/24 16:260.0050.0004<0.0004mg/Kg1,2-Dichloropropane
03/26/24 16:260.0050.0006<0.0006mg/Kg1,3-Dichloropropane
03/26/24 16:260.0050.001<0.001mg/Kg2,2-Dichloropropane
03/26/24 16:260.0050.0008<0.0008mg/Kg1,1-Dichloropropene
03/26/24 16:260.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
03/26/24 16:260.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
03/26/24 16:260.2500.014<0.014mg/KgEthanol
03/26/24 16:260.0050.0006<0.0006mg/KgEthylbenzene
03/26/24 16:260.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
03/26/24 16:260.0100.0008<0.0008mg/KgHexachlorobutadiene
03/26/24 16:260.0100.0007<0.0007mg/Kgn-Hexane
03/26/24 16:260.0200.0006<0.0006mg/Kg2-Hexanone
03/26/24 16:260.0050.0005<0.0005mg/KgIsopropylbenzene
03/26/24 16:260.0050.001<0.001mg/Kg4-Isopropyl toluene
03/26/24 16:260.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
03/26/24 16:260.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
03/26/24 16:260.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
03/26/24 16:260.0100.001<0.001mg/KgMethylene Chloride
03/26/24 16:260.0100.0010<0.0010mg/KgNaphthalene
03/26/24 16:260.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 5 of 17Date:04/02/2024 03:48 PM
Page 37 of 51
Quality Control Data
24-082-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BWR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V45352QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V45351
Associated Lab Samples: 89021
LRB-V45351 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/26/24 16:260.0050.001<0.001mg/KgStyrene
03/26/24 16:260.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
03/26/24 16:260.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
03/26/24 16:260.0050.0009<0.0009mg/KgTetrachloroethene
03/26/24 16:260.0050.0007<0.0007mg/KgToluene
03/26/24 16:260.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
03/26/24 16:260.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
03/26/24 16:260.0050.001<0.001mg/Kg1,1,1-Trichloroethane
03/26/24 16:260.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
03/26/24 16:260.0050.0009<0.0009mg/KgTrichloroethene
03/26/24 16:260.0100.002<0.002mg/KgTrichlorofluoromethane
03/26/24 16:260.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
03/26/24 16:260.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
03/26/24 16:260.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
03/26/24 16:260.0100.0005<0.0005mg/KgVinyl Acetate
03/26/24 16:260.0100.0005<0.0005mg/KgVinyl Chloride
03/26/24 16:260.0050.0005<0.0005mg/Kgo-Xylene
03/26/24 16:260.0100.001<0.001mg/Kgm,p-Xylene
03/26/24 16:264-Bromofluorobenzene (S)104 70-130
03/26/24 16:26Dibromofluoromethane (S)104 84-123
03/26/24 16:26Toluene-d8 (S)85.6 76-129
LCS-V45351Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
134*1.671.25mg/KgEthanol 70-130
Page 6 of 17* QC Fail Date:04/02/2024 03:48 PM
Page 38 of 51
Quality Control Data
24-082-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BWR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V45352QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V45351
LCS-V45351 LCSD-V45351Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.120 1201210.1210.100mg/KgAcetone 29-198 0.8 20
0.117 1171150.1150.100mg/KgAcrolein 70-130 1.7 20
0.106 1061100.1100.100mg/KgAcrylonitrile 65-134 3.7 20
0.049 98.21050.0520.050mg/KgBenzene 74-127 6.8 20
0.039 78.681.40.0400.050mg/KgBromobenzene 73-125 3.5 20
0.054 1091160.0580.050mg/KgBromochloromethane 72-134 6.0 20
0.052 1061100.0540.050mg/KgBromodichloromethane 75-122 3.7 20
0.047 95.695.60.0470.050mg/KgBromoform 66-135 0.0 20
0.053 1081090.0540.050mg/KgBromomethane 20-180 1.2 20
0.040 80.083.80.0410.050mg/Kgn-Butylbenzene 65-135 4.6 20
0.036 73.877.80.0380.050mg/Kgsec-Butyl benzene 66-131 5.2 20
0.036 72.877.40.0380.050mg/Kgtert-Butyl benzene 67-132 6.1 20
0.048 96.81060.0530.050mg/KgCarbon Disulfide 61-129 9.4 20
0.047 94.01030.0510.050mg/KgCarbon Tetrachloride 64-143 9.5 20
0.040 81.887.40.0430.050mg/KgChlorobenzene 74-118 6.6 20
0.043 86.689.60.0440.050mg/KgChlorodibromomethane 73-122 3.4 20
0.052 1051160.0570.050mg/KgChloroethane 33-149 9.9 20
0.050 1011070.0530.050mg/KgChloroform 73-127 6.1 20
0.053 1061150.0570.050mg/KgChloromethane 45-143 7.6 20
0.037 74.677.60.0380.050mg/Kg2-Chlorotoluene 67-124 3.9 20
0.037 74.677.60.0380.050mg/Kg4-Chlorotoluene 71-126 3.9 20
0.048 96.699.40.0490.050mg/KgDi-Isopropyl Ether (DIPE)59-159 2.8 20
0.050 10199.80.0490.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 0.7 20
0.048 97.81010.0500.050mg/Kg1,2-Dibromoethane 70-132 3.0 20
0.058 1181200.0590.050mg/KgDibromomethane 74-133 1.5 20
0.039 79.683.00.0410.050mg/Kg1,2-Dichlorobenzene 72-123 4.1 20
Page 7 of 17Date:04/02/2024 03:48 PM
Page 39 of 51
Quality Control Data
24-082-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BWR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V45352QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V45351
LCS-V45351 LCSD-V45351Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.039 79.081.80.0400.050mg/Kg1,3-Dichlorobenzene 71-120 3.4 20
0.037 75.077.00.0380.050mg/Kg1,4-Dichlorobenzene 71-123 2.6 20
0.039 79.890.40.0450.050mg/KgDichlorodifluoromethane 26-146 12.4 20
0.047 95.21030.0510.050mg/Kg1,1-Dichloroethane 74-127 7.8 20
0.052 1051070.0530.050mg/Kg1,2-Dichloroethane 68-128 2.0 20
0.045 91.61020.0500.050mg/Kg1,1-Dichloroethene 67-149 10.3 20
0.048 96.61020.0510.050mg/Kgcis-1,2-Dichloroethene 76-134 5.8 20
0.046 92.899.60.0490.050mg/Kgtrans-1,2-Dichloroethene 73-132 7.0 20
0.050 1011060.0520.050mg/Kg1,2-Dichloropropane 73-130 4.8 20
0.045 91.492.60.0460.050mg/Kg1,3-Dichloropropane 75-124 1.3 20
0.047 95.01030.0510.050mg/Kg2,2-Dichloropropane 50-142 7.8 20
0.047 94.41030.0510.050mg/Kg1,1-Dichloropropene 71-130 8.7 20
0.052 1051120.0550.050mg/Kgcis-1,3-Dichloropropene 71-125 5.7 20
0.057 1151210.0600.050mg/Kgtrans-1,3-Dichloropropene 68-123 4.4 20
0.040 80.084.60.0420.050mg/KgEthylbenzene 74-128 5.5 20
0.103 1031060.1060.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 2.8 20
0.038 77.677.20.0380.050mg/KgHexachlorobutadiene 64-125 0.5 20
0.047 95.81060.0530.050mg/Kgn-Hexane 70-130 10.2 20
0.043 86.286.80.0430.050mg/Kg2-Hexanone 61-157 0.6 20
0.036 73.679.20.0390.050mg/KgIsopropylbenzene 68-126 7.3 20
0.037 74.279.40.0390.050mg/Kg4-Isopropyl toluene 68-129 6.7 20
0.054 1081110.0550.050mg/KgMethyl Ethyl Ketone (MEK)63-149 2.7 20
0.054 1091120.0550.050mg/KgMethyl tert-butyl ether (MTBE)70-130 2.3 20
0.051 1031060.0530.050mg/Kg4-Methyl-2-Pentanone 57-162 3.2 20
0.042 85.889.40.0440.050mg/KgMethylene Chloride 74-129 4.1 20
0.053 10796.60.0480.050mg/KgNaphthalene 57-157 10.4 20
Page 8 of 17Date:04/02/2024 03:48 PM
Page 40 of 51
Quality Control Data
24-082-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BWR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V45352QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V45351
LCS-V45351 LCSD-V45351Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.037 74.679.60.0390.050mg/Kgn-Propylbenzene 67-130 6.4 20
0.043 87.487.40.0430.050mg/KgStyrene 77-121 0.0 20
0.042 85.088.20.0440.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 3.6 20
0.045 91.091.00.0450.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 0.0 20
0.048 96.41060.0530.050mg/KgTetrachloroethene 68-130 9.6 20
0.049 98.81050.0520.050mg/KgToluene 71-129 6.0 20
0.048 97.287.60.0430.050mg/Kg1,2,3-Trichlorobenzene 68-130 10.3 20
0.046 93.089.80.0440.050mg/Kg1,2,4-Trichlorobenzene 66-125 3.5 20
0.048 97.01040.0520.050mg/Kg1,1,1-Trichloroethane 67-131 7.3 20
0.045 91.694.00.0470.050mg/Kg1,1,2-Trichloroethane 70-133 2.5 20
0.051 1021090.0540.050mg/KgTrichloroethene 75-133 6.8 20
0.050 1011120.0560.050mg/KgTrichlorofluoromethane 44-146 10.7 20
0.047 95.698.40.0490.050mg/Kg1,2,3-Trichloropropane 60-137 2.8 20
0.038 76.479.80.0390.050mg/Kg1,2,4-Trimethylbenzene 69-129 4.3 20
0.037 75.879.20.0390.050mg/Kg1,3,5-Trimethylbenzene 69-128 4.3 20
0.059 1191170.0580.050mg/KgVinyl Acetate 60-140 1.8 20
0.056 1121270.0630.050mg/KgVinyl Chloride 48-147 12.0 20
0.040 81.685.80.0420.050mg/Kgo-Xylene 74-126 5.0 20
0.079 79.485.00.0850.100mg/Kgm,p-Xylene 75-124 6.8 20
1021034-Bromofluorobenzene (S)70-130
103103Dibromofluoromethane (S)84-123
85.886.6Toluene-d8 (S)76-129
Page 9 of 17Date:04/02/2024 03:48 PM
Page 41 of 51
Quality Control Data
24-082-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BWR-013
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V45311QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V45267
Associated Lab Samples: 89020, 89021, 89022
LRB-V45267 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/27/24 12:490.6600.147<0.147mg/KgAcenaphthene
03/27/24 12:490.6600.150<0.150mg/KgAcenaphthylene
03/27/24 12:490.6600.210<0.210mg/KgAniline
03/27/24 12:490.6600.166<0.166mg/KgAnthracene
03/27/24 12:490.6600.156<0.156mg/KgBenzo(a)anthracene
03/27/24 12:490.6600.165<0.165mg/KgBenzo(a)pyrene
03/27/24 12:490.6600.147<0.147mg/KgBenzo(b)fluoranthene
03/27/24 12:490.6600.144<0.144mg/KgBenzo(g,h,i)perylene
03/27/24 12:490.6600.156<0.156mg/KgBenzo(k)fluoranthene
03/27/24 12:492.000.580<0.580mg/KgBenzoic Acid
03/27/24 12:490.6600.156<0.156mg/KgBenzyl alcohol
03/27/24 12:490.6600.138<0.138mg/KgBis(2-Chloroethoxy)methane
03/27/24 12:490.6600.122<0.122mg/KgBis(2-Chloroethyl)ether
03/27/24 12:490.3300.131<0.131mg/KgBis(2-Chloroisopropyl)ether
03/27/24 12:490.6600.177<0.177mg/KgBis(2-ethylhexyl)phthalate
03/27/24 12:490.6600.158<0.158mg/Kg4-Bromophenyl phenyl ether
03/27/24 12:490.3300.160<0.160mg/KgButyl benzyl phthalate
03/27/24 12:490.6600.149<0.149mg/Kg4-Chloro-3-methylphenol
03/27/24 12:490.3300.150<0.150mg/Kg4-Chloroaniline
03/27/24 12:490.6600.154<0.154mg/Kg2-Chloronaphthalene
03/27/24 12:490.6600.142<0.142mg/Kg2-Chlorophenol
03/27/24 12:491.000.147<0.147mg/Kg4-Chlorophenyl phenyl ether
03/27/24 12:490.6600.146<0.146mg/KgChrysene
03/27/24 12:490.6600.111<0.111mg/KgDibenz(a,h)anthracene
03/27/24 12:490.6600.158<0.158mg/KgDibenzofuran
03/27/24 12:490.6600.128<0.128mg/Kg1,2-Dichlorobenzene
03/27/24 12:490.6600.125<0.125mg/Kg1,3-Dichlorobenzene
Page 10 of 17Date:04/02/2024 03:48 PM
Page 42 of 51
Quality Control Data
24-082-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BWR-013
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V45311QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V45267
Associated Lab Samples: 89020, 89021, 89022
LRB-V45267 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/27/24 12:490.3300.118<0.118mg/Kg1,4-Dichlorobenzene
03/27/24 12:490.6600.150<0.150mg/Kg3,3'-Dichlorobenzidine
03/27/24 12:490.6600.140<0.140mg/Kg2,4-Dichlorophenol
03/27/24 12:490.6600.147<0.147mg/KgDiethyl phthalate
03/27/24 12:490.6600.157<0.157mg/KgDimethyl phthalate
03/27/24 12:490.6600.212<0.212mg/Kg2,4-Dimethylphenol
03/27/24 12:490.6600.171<0.171mg/KgDi-n-butyl phthalate
03/27/24 12:491.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
03/27/24 12:491.500.520<0.520mg/Kg2,4-Dinitrophenol
03/27/24 12:490.6600.161<0.161mg/Kg2,4-Dinitrotoluene
03/27/24 12:490.6600.166<0.166mg/Kg2,6-Dinitrotoluene
03/27/24 12:490.3300.163<0.163mg/KgDi-n-Octyl Phthalate
03/27/24 12:490.6600.158<0.158mg/KgFluoranthene
03/27/24 12:490.6600.153<0.153mg/KgFluorene
03/27/24 12:490.6600.150<0.150mg/KgHexachlorobenzene
03/27/24 12:490.6600.097<0.097mg/KgHexachlorobutadiene
03/27/24 12:490.6600.122<0.122mg/KgHexachloroethane
03/27/24 12:490.6600.151<0.151mg/KgIndeno(1,2,3-cd)pyrene
03/27/24 12:490.6600.121<0.121mg/KgIsophorone
03/27/24 12:490.6600.139<0.139mg/Kg1-Methylnaphthalene
03/27/24 12:490.6600.144<0.144mg/Kg2-Methylnaphthalene
03/27/24 12:490.6600.127<0.127mg/Kg2-Methylphenol
03/27/24 12:490.6600.128<0.128mg/Kg3&4 Methylphenol
03/27/24 12:490.6600.133<0.133mg/KgNaphthalene
03/27/24 12:490.6600.132<0.132mg/Kg2-Nitroaniline
03/27/24 12:490.6600.155<0.155mg/Kg3-Nitroaniline
03/27/24 12:490.3300.136<0.136mg/Kg4-Nitroaniline
Page 11 of 17Date:04/02/2024 03:48 PM
Page 43 of 51
Quality Control Data
24-082-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BWR-013
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V45311QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V45267
Associated Lab Samples: 89020, 89021, 89022
LRB-V45267 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/27/24 12:490.3300.129<0.129mg/KgNitrobenzene
03/27/24 12:490.6600.133<0.133mg/Kg2-Nitrophenol
03/27/24 12:490.6600.167<0.167mg/Kg4-Nitrophenol
03/27/24 12:490.6600.263<0.263mg/KgN-Nitrosodimethylamine
03/27/24 12:490.6600.182<0.182mg/KgN-Nitrosodiphenylamine
03/27/24 12:490.6600.148<0.148mg/KgN-Nitroso-di-n-propylamine
03/27/24 12:491.000.347<0.347mg/KgPentachlorophenol
03/27/24 12:490.6600.158<0.158mg/KgPhenanthrene
03/27/24 12:490.6600.142<0.142mg/KgPhenol
03/27/24 12:490.6600.160<0.160mg/KgPyrene
03/27/24 12:490.3300.076<0.076mg/KgPyridine
03/27/24 12:490.6600.132<0.132mg/Kg1,2,4-Trichlorobenzene
03/27/24 12:490.6600.143<0.143mg/Kg2,4,5-Trichlorophenol
03/27/24 12:490.6600.140<0.140mg/Kg2,4,6-Trichlorophenol
03/27/24 12:492-Fluorobiphenyl (S)78.4 44-115
03/27/24 12:492-Fluorophenol (S)86.1 35-115
03/27/24 12:49Nitrobenzene-d5 (S)86.2 37-122
03/27/24 12:494-Terphenyl-d14 (S)82.6 54-127
03/27/24 12:492,4,6-Tribromophenol (S)79.5 39-132
03/27/24 12:49Phenol-d5 (S)81.9 34-121
LCS-V45267 LCSD-V45267Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.38 82.682.61.381.67mg/KgAcenaphthene 40-123 0.0 20
1.42 85.084.41.411.67mg/KgAcenaphthylene 32-132 0.7 20
Page 12 of 17Date:04/02/2024 03:48 PM
Page 44 of 51
Quality Control Data
24-082-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BWR-013
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V45311QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V45267
LCS-V45267 LCSD-V45267Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.71 1021051.751.67mg/KgAniline 12-197 2.3 20
1.48 88.689.21.491.67mg/KgAnthracene 47-123 0.6 20
1.52 91.091.61.531.67mg/KgBenzo(a)anthracene 49-126 0.6 20
1.75 1051041.731.67mg/KgBenzo(a)pyrene 45-129 1.1 20
1.68 10199.41.661.67mg/KgBenzo(b)fluoranthene 45-132 1.1 20
1.63 97.694.61.581.67mg/KgBenzo(g,h,i)perylene 43-134 3.1 20
1.36 81.482.61.381.67mg/KgBenzo(k)fluoranthene 47-132 1.4 20
1.18 70.671.21.191.67mg/KgBenzoic Acid 10-83 0.8 20
1.48 88.687.41.461.67mg/KgBenzyl alcohol 29-122 1.3 20
1.36 81.483.21.391.67mg/KgBis(2-Chloroethoxy)methane 36-121 2.1 20
1.24 74.276.01.271.67mg/KgBis(2-Chloroethyl)ether 31-120 2.3 20
1.24 74.275.41.261.67mg/KgBis(2-Chloroisopropyl)ether 33-131 1.6 20
1.69 1011021.711.67mg/KgBis(2-ethylhexyl)phthalate 51-133 1.1 20
1.42 85.086.81.451.67mg/Kg4-Bromophenyl phenyl ether 46-124 2.0 20
1.71 1021041.741.67mg/KgButyl benzyl phthalate 48-132 1.7 20
1.49 89.290.41.511.67mg/Kg4-Chloro-3-methylphenol 45-122 1.3 20
1.33 79.680.81.351.67mg/Kg4-Chloroaniline 17-106 1.4 20
1.40 83.884.41.411.67mg/Kg2-Chloronaphthalene 41-114 0.7 20
1.38 82.683.21.391.67mg/Kg2-Chlorophenol 34-121 0.7 20
1.39 83.282.61.381.67mg/Kg4-Chlorophenyl phenyl ether 45-121 0.7 20
1.46 87.487.41.461.67mg/KgChrysene 50-124 0.0 20
0.888 53.152.80.8831.67mg/KgDibenz(a,h)anthracene 45-134 0.5 20
1.42 85.085.01.421.67mg/KgDibenzofuran 44-120 0.0 20
1.22 73.074.81.251.67mg/Kg1,2-Dichlorobenzene 33-117 2.4 20
1.19 71.271.21.191.67mg/Kg1,3-Dichlorobenzene 30-115 0.0 20
1.14 68.270.01.171.67mg/Kg1,4-Dichlorobenzene 31-115 2.5 20
Page 13 of 17Date:04/02/2024 03:48 PM
Page 45 of 51
Quality Control Data
24-082-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BWR-013
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V45311QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V45267
LCS-V45267 LCSD-V45267Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.30 77.883.21.391.67mg/Kg3,3'-Dichlorobenzidine 22-121 6.6 20
1.54 92.292.21.541.67mg/Kg2,4-Dichlorophenol 40-122 0.0 20
1.53 91.690.41.511.67mg/KgDiethyl phthalate 50-124 1.3 20
1.48 88.687.41.461.67mg/KgDimethyl phthalate 48-124 1.3 20
2.01 1201222.041.67mg/Kg2,4-Dimethylphenol 30-127 1.4 20
1.68 1011011.691.67mg/KgDi-n-butyl phthalate 51-128 0.5 20
1.57 94.089.81.501.67mg/Kg4,6-Dinitro-2-methylphenol 29-132 4.5 20
1.57 94.092.21.541.67mg/Kg2,4-Dinitrophenol 27-129 1.9 20
1.67 10094.01.571.67mg/Kg2,4-Dinitrotoluene 48-126 6.1 20
1.62 97.095.21.591.67mg/Kg2,6-Dinitrotoluene 46-124 1.8 20
1.67 10099.41.661.67mg/KgDi-n-Octyl Phthalate 45-140 0.6 20
1.48 88.690.41.511.67mg/KgFluoranthene 50-127 2.0 20
1.50 89.888.61.481.67mg/KgFluorene 43-125 1.3 20
1.54 92.293.41.561.67mg/KgHexachlorobenzene 45-122 1.2 20
1.43 85.686.21.441.67mg/KgHexachlorobutadiene 32-123 0.6 20
1.21 72.472.41.211.67mg/KgHexachloroethane 28-117 0.0 20
1.50 89.889.81.501.67mg/KgIndeno(1,2,3-cd)pyrene 45-133 0.0 20
1.40 83.886.21.441.67mg/KgIsophorone 30-122 2.8 20
1.34 80.281.41.361.67mg/Kg1-Methylnaphthalene 40-119 1.4 20
1.39 83.283.21.391.67mg/Kg2-Methylnaphthalene 38-122 0.0 20
1.40 83.885.61.431.67mg/Kg2-Methylphenol 32-122 2.1 20
1.28 76.677.21.291.67mg/Kg3&4 Methylphenol 34-119 0.7 20
1.31 78.479.01.321.67mg/KgNaphthalene 35-123 0.7 20
1.49 89.286.21.441.67mg/Kg2-Nitroaniline 44-127 3.4 20
1.49 89.286.21.441.67mg/Kg3-Nitroaniline 33-119 3.4 20
1.57 94.094.01.571.67mg/Kg4-Nitroaniline 63-147 0.0 20
Page 14 of 17Date:04/02/2024 03:48 PM
Page 46 of 51
Quality Control Data
24-082-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BWR-013
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V45311QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V45267
LCS-V45267 LCSD-V45267Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.48 88.688.61.481.67mg/KgNitrobenzene 34-122 0.0 20
1.42 85.082.01.371.67mg/Kg2-Nitrophenol 36-123 3.5 20
1.66 99.496.41.611.67mg/Kg4-Nitrophenol 30-132 3.0 20
1.19 71.272.41.211.67mg/KgN-Nitrosodimethylamine 10-146 1.6 20
1.73 1041051.761.67mg/KgN-Nitrosodiphenylamine 38-127 1.7 20
1.37 82.081.41.361.67mg/KgN-Nitroso-di-n-propylamine 36-120 0.7 20
1.77 1061061.771.67mg/KgPentachlorophenol 25-133 0.0 20
1.45 86.888.01.471.67mg/KgPhenanthrene 50-121 1.3 20
1.35 80.881.41.361.67mg/KgPhenol 34-121 0.7 20
1.47 88.086.21.441.67mg/KgPyrene 47-127 2.0 20
0.946 56.656.90.9511.67mg/KgPyridine 10-80 0.5 20
1.31 78.480.21.341.67mg/Kg1,2,4-Trichlorobenzene 34-118 2.2 20
1.52 91.089.81.501.67mg/Kg2,4,5-Trichlorophenol 41-124 1.3 20
1.55 92.892.21.541.67mg/Kg2,4,6-Trichlorophenol 39-126 0.6 20
83.284.42-Fluorobiphenyl (S)44-115
90.093.02-Fluorophenol (S)35-115
88.691.0Nitrobenzene-d5 (S)37-122
84.486.24-Terphenyl-d14 (S)54-127
92.795.42,4,6-Tribromophenol (S)39-132
84.386.1Phenol-d5 (S)34-121
Page 15 of 17Date:04/02/2024 03:48 PM
Page 47 of 51
Quality Control Data
24-082-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BWR-013
QC Prep Batch Method:
Hexavalent Chromium by Ion Chromatography
SW-7199
L741598QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3060A
QC Prep:L741255
Associated Lab Samples: 89020, 89021, 89022
LRB-L741255 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
03/29/24 15:460.2000.141<0.141mg/KgChromium, Hexavalent
LCS-L741255Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
90.03.614.00mg/KgChromium, Hexavalent 80-120
V 89020-DUP-L741255Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 03/29/24 16:19133*1.010.204mg/KgChromium, Hexavalent
V 89020-MS-L741255Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
31.7 81.038.8< 1.37mg/KgChromium, Hexavalent 75-125
Page 16 of 17* QC Fail Date:04/02/2024 03:48 PM
Page 48 of 51
Quality Control Data
24-082-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BWR-013
Dry Weight Determination
SW-DRYWT
V45243QC Analytical Batch:
Analysis Method:
Analysis Description:
V 89054-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 03/25/24 16:250.910.410.3%Moisture
V 89055-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 03/25/24 16:252.316.717.1%Moisture
Page 17 of 17Date:04/02/2024 03:48 PM
Page 49 of 51
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:24-082-0013
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 5.5C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:03/22/2024 13:57:08
Special precautions or instructions included?
Comments:
Page 50 of 51
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