18002_Precisoin Dynamics_ Remediationand Sampling Report_20160308

Remediation and Additional Sampling
Former Precision Dynamics Site

1033 Carter Avenue
Charlotte, North Carolina

H&H Job No. CHP-22
March 8, 2016

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Remediation and Additional Sampling Former Precision Dynamics Site
Charlotte, North Carolina
H&H Job No. CHP-22

Table of Contents

1.0 Introduction ............................................................................................................................ 1
2.0 Removal Activities ................................................................................................................. 2
2.1 Metal Slag Removal ............................................................................................................. 2
2.2 Heating Oil UST .................................................................................................................. 3
2.3 Waste Oil AST ...................................................................................................................... 3
3.0 Results ..................................................................................................................................... 5
3.1 Metal Slag Removal ............................................................................................................. 5
3.2 IHSB Industrial PSRG Adjustment and Historical Data Review ........................................ 5
3.3 Heating Oil UST .................................................................................................................. 7
3.4 Waste Oil AST ..................................................................................................................... 7
4.0 Summary and Conclusions ................................................................................................... 9

List of Tables
Table 1 Soil Analytical Data Summary

List of Figures
Figure 1 Site Location Map
Figure 2 Sample Location Map

List of Appendices
Appendix A Disposal Documentation
Appendix B Laboratory Analytical Report

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Remediation and Additional Sampling Former Precision Dynamics Site
Charlotte, North Carolina
H&H Job No. CHP-22
1.0 Introduction

H&H is pleased to present this report documenting removal of poured metal slag and a heating
oil underground storage tank (UST), and additional soil sampling activities conducted at the
Precision Dynamics Brownfields site located at 1033 Carter Ave in Charlotte, North Carolina. A
site location map is provided as Figure 1. The Brownfields project number is #18002-14-060.
The purpose of the metal slag and UST removal was to address certain environmental conditions
prior to site redevelopment. The purpose of the additional soil sampling was to determine if
elevated metal concentrations (documented during previous assessment activities) were present
in shallow soil above calculated site-specific final remediation goals for industrial use following
removal of the metal slag and to determine if compound-specific soil impacts were present in the
vicinity of the former heating oil UST and a former waste oil AST. A summary of the removal
and sampling activities is provided below.

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2.0 Removal Activities

2.1 Metal Slag Removal

During the Phase I Environmental Site Assessment (ESA) conducted in 2013, H&H observed
poured metal slag around the property near and on each side of the building. During the
subsequent Phase II ESA activities conducted in September 2013 and January 2014, samples of
the metal slag and underlying soil were collected. The results of the laboratory analysis
indicated that the slag material was not hazardous; however, elevated metal concentrations
(including arsenic, hexavalent chromium, and thallium) were detected in the soil below and
mixed with the slag. A summary of the previous soil analytical data is provided in Table 1.

On November 30 through December 2, 2015, visible metal slag was removed from the site.
Potential solidified/dense metal slag material present below hardscape surfaces (such as the
northeast paved area) or used as a soil retaining wall for neighboring property (southeast corner)
were left in place. The extent of metal slag removal is shown on Figure 2. In addition to the slag
removal, a small amount of surficial soil (approximately 3 inches to 6 inches) was removed from
below the slag material in areas that indicated the presence of elevated metal concentrations
during previous assessment activities. The purpose of the surficial soil removal was to reduce
surficial elevated metal concentrations. The surficial soil excavation was conducted in the
vicinity of previous shallow soil samples SB-3, SB-8, and SB-11 (Figure 2).

To determine if the surficial soil removal had reduced metal concentrations in those areas and as
final grade sampling, H&H collected shallow soil samples following the metal slag and soil
removal. The samples were collected for analysis of Hazardous Substance List (HSL) Metals by
EPA Method 6010/7471 and hexavalent chromium by EPA Method 7199. The sample locations
included samples SB-16, SB-17, and SB-18. In addition, H&H collected samples SB-15 and SB-
19 in areas of metal slag removal not previously accessed. The results of the sampling are
discussed in Section 3.

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Approximately 75.29 tons of metal slag and surficial soil was excavated from the site and
disposed off-site. Disposal documentation for the metal slag and surficial soil is included in
Appendix A.

2.2 Heating Oil UST

During previous Phase II ESA activities, H&H collected soil sample SB-1 adjacent to an inactive
heating oil UST. The results of the laboratory analysis indicated the presence of diesel-range
total petroleum hydrocarbons (TPH) above the Department of Environmental Quality (DEQ)
UST Section Action Level of 10 mg/kg. At the request of the prospective developer (Charlotte-
Mecklenburg Housing Partnership), H&H removed the UST on November 30, 2015. Following
removal of the tank, H&H collected a sample from below the tank (UST-Base) at the same depth
as previous sample SB-1 and collected a shallow (0 ft to 2 ft) soil sample (UST-N) to determine
if shallow soil impacts were present in the vicinity of the former UST. The samples were
analyzed for volatile organic compounds (VOCs) by EPA Method 8260 and semi-volatile
organic compounds (SVOCs) by EPA Method 8270. Prior to collecting the sidewall sample,
H&H utilized a photoionization detector (PID) to screen each sidewall for elevated organic vapor
concentrations; however, an elevated PID level was not observed. Therefore, H&H collected the
sample from the sidewall nearest the fill port of the former tank. The locations of samples UST-
N and UST-Base are shown on Figure 2, and the results of the laboratory analysis are discussed
in Section 3.3.

Following sample collection, the soil overburden was placed back in the hole and the upper
portion of the excavation was backfilled with ABC stone. The tank was then sent to DH Griffin
in Greensboro, North Carolina for recycling. A disposal certification for the UST is included in
Appendix A.

2.3 Waste Oil AST
During previous assessment activities, H&H collected a soil sample (SB-2) in the vicinity of
surficial soil staining observed adjacent to a former waste oil above ground storage tank (AST)
located on the western portion of the property. The result of the laboratory analysis indicated the
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presence of diesel range TPH above the DEQ UST Section Action Level of 10 mg/kg. H&H
collected shallow soil sample SB-14 (0- ft to 2 ft) adjacent to previous sample SB-2 (Figure 2)
for analysis of VOCs, SVOCs, HSL metals, and hexavalent chromium. The results of the
laboratory analysis are discussed in Section 3.4.

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3.0 Results

3.1 Metal Slag Removal

The results of the shallow soil samples collected following the removal of the metal slag and
surficial soil indicated a concentration of arsenic in samples SB-15 (6.57 mg/kg), SB-16
(6.36 mg/kg), SB-17 (6.23 mg/kg), and SB-18 (7.20 mg/kg) above the Inactive Hazardous Site
Branch (IHSB) Industrial Preliminary Soil Remedial Goal (PSRG) of 3.0 mg/kg and the site
specific maximum background concentration of 5.6 mg/kg (determined during previous
assessment activities). The results of the soil samples are summarized on Table 1, and the
laboratory report along with chain-of-custody is provided in Appendix B

Although the arsenic concentrations detected in SB-15, SB-16, SB-17, and SB-18 exceed the
IHSB Industrial PSRG of 3.0 mg/kg, they do not exceed the site-specific adjusted IHSB
Industrial Screening Level of 75 mg/kg for arsenic. The site-specific adjusted IHSB Screening
Level was calculated using the Registered Environmental Consultant (REC) Program
Implementation Guidance (October 2015). Instructions for calculating the adjusted site specific
IHSB Industrial Screening Levels are included in Appendix E of the above guidance and a
description of how the guidance was used to calculate the adjusted site specific IHSB Industrial
Screening Level is included below.

3.2 IHSB Industrial PSRG Adjustment and Historical Data Review

In accordance with REC Program guidance, the IHSB PSRGs can be used as a final health-based
soil remediation goal. However, the IHSB PSRG can also be adjusted for the number of
contaminants present to a site-specific IHSB Screening Level. The REC program defines a
contaminant as any compound detected at a concentration within one order of magnitude of the
PSRG. Using the definition of contaminant provided by the REC program in conjunction with
the current and historical data, the Precision Dynamics Site has a total of six (6) “contaminants”
(benzo(a)pyrene, benzo(b)fluoranthene, arsenic, hexavalent chromium, manganese, and
thallium). Once the total number of contaminants present at the site is determined, the USEPA
Regional Screening Level (RSL) Table is used to classify the contaminants as carcinogenic, non-
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carcinogenic, or both. For ease of reference, the following table is included with the site
contaminants classified.

Contaminant Carcinogenic Non-Carcinogenic
benzo(a)pyrene X
benzo(b)fluoranthene X
arsenic X X
hexavalent chromium X X
manganese X
thallium X
Total 4 4

As indicated in the table above, arsenic has both carcinogenic and non-carcinogenic effects. In
order to calculate the adjusted site-specific IHSB Screening Level for arsenic, the user must
calculate both the adjusted carcinogenic and adjusted non-carcinogenic IHSB Screening Level.
Then, the more stringent of the two adjusted values is used.

To calculate the adjusted carcinogenic IHSB Screening Level for arsenic, the REC guidance
indicates that the EPA Industrial Soil Screening Level for arsenic (3.0 mg/kg) should be
multiplied by 100 and then divided by the total number of carcinogenic contaminants present at
the site (four). Using the equation provided by the REC program, the adjusted carcinogenic
IHSB Screening Level for arsenic at the site is 75 mg/kg.

To calculate the adjusted non-carcinogenic IHSB Screening Level for arsenic, the REC guidance
indicates that the EPA Carcinogenic Industrial Soil Screening Level for arsenic (480 mg/kg)
should be divided by the total number of non-carcinogenic contaminants present at the site
(four). Using the equation provided by the REC program, the adjusted non-carcinogenic IHSB
Screening Level for arsenic at the site is 120 mg/kg.

Comparing the two adjusted IHSB Industrial Screening Levels calculated above, the adjusted
IHSB Screening Level for arsenic for the Precision Dynamics site is 75 mg/kg.

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In addition to arsenic, H&H utilized the REC Program’s method for calculating adjusted site
specific IHSB Screening Levels for hexavalent chromium and thallium which were also detected
onsite above IHSB PSRGs and site-specific background concentrations. The result of the
calculation indicated an adjusted IHSB Screening Level of 157.5 mg/kg for hexavalent
chromium and 3.0 mg/kg for thallium.

The adjusted IHSB Industrial Screening Levels for arsenic, hexavalent chromium, and are
included in Table 1. As indicated in the Table 1, the concentration of thallium detected in
sample SB-3B 9 ft - 10 ft (3.7 mg/kg) is the only detected concentrations on-site above site
specific adjusted IHSB Industrial Screening Levels. The location of the thallium exceedances is
deep below ground and is not likely to be encountered during site redevelopment.

3.3 Heating Oil UST

Following removal of the heating oil UST, H&H collected shallow soil sample UST-Base from
below the former UST and shallow soil sample UST-N from the sidewall nearest the fill port of
the former UST. The results of the laboratory analysis did not indicate the presence of VOCs or
SVOCs above IHSB Industrial PSRGs.

A concentration of acetone was detected in UST-N (0.0488 mg/kg) and UST-Base
(0.0654 mg/kg); however, both concentrations detected were below the IHSB Industrial PSRG of
100,000 mg/kg. In addition, these detections may be from laboratory introduced contamination.
The results of the soil samples are summarized on Table 1, and the laboratory report with chain-
of-custody record is provided in Appendix B.

3.4 Waste Oil AST

H&H collected shallow soil sample (0 ft to 2 ft) SB-14 adjacent to previous sample SB-2. The
result of the laboratory analysis indicated the presence of acetone, benzo(a)anthracene,
benzo(a)pyrene, benzo(b)fluoranthene, benzo(g,h,i)perylene, benzo(k)fluoranthene, chrysene,
fluoranthene, indeno(1,2,3-cd)pyrene, phenanthrene, and pyrene; however, the concentrations
detected were below IHSB Industrial PSRGs. Several metals were also detected in sample SB-
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14, but the concentrations detected were below their respective IHSB Industrial PSRG and/or
site-specific maximum background concentrations. The results of the soil samples are
summarized on Table 1, and the laboratory report with chain-of-custody record is provided in
Appendix B.
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4.0 Summary and Conclusions

On November 30 through December 1, 2015, H&H removed poured metal slag and a heating oil
underground storage tank (UST) and conducted additional soil sampling activities at the
Precision Dynamics Brownfields site located at 1033 Carter Ave in Charlotte, North Carolina.
The purpose of the metal slag and UST removal was to address certain environmental conditions
prior to site redevelopment. The purpose of the additional soil sampling was to determine if
elevated metal concentrations (documented during previous assessment activities) were present
above calculated site-specific final remediation goals for industrial use following removal of the
metal slag and to determine if compound-specific soil impacts were present in the vicinity of the
former heating oil UST and former waste oil AST.

Metal Slag Removal, Sampling, Data Review
On November 30 through December 2, 2015, visible metal slag was removed from the site.
Potential solidified/dense metal slag material present below hardscape surfaces (such as the
northeast paved area) or used as a soil retaining wall for neighboring property (southeast corner)
were left in place. In addition to the slag removal, a small amount of surficial soil
(approximately 3 inches to 6 inches) was removed from below the slag material in areas that
indicated the presence of elevated metal concentrations during previous assessment activities.
The purpose of the surficial soil removal was to reduce surficial elevated metal concentrations.

The results of the final grade shallow soil samples collected below the metal slag indicated a
concentration of arsenic in samples SB-15 (6.57 mg/kg), SB-16 (6.36 mg/kg), SB-17
(6.23 mg/kg), and SB-18 (7.20 mg/kg) above the IHSB Industrial PSRG of 3.0 mg/kg and the
site specific maximum background concentration of 5.6 mg/kg.

Although the arsenic concentrations detected in SB-15, SB-16, SB-17, and SB-18 exceed the
IHSB Industrial PSRG of 3.0 mg/kg, they do not exceed the adjusted site-specific IHSB
Industrial Screening Level of 75 mg/kg for arsenic. The site specific IHSB Industrial PSRG was
calculated using the REC Program Implementation Guidance.

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In addition to arsenic, H&H utilized the REC Program’s method for calculating adjusted site
specific screening levels for hexavalent chromium and thallium which were previously detected
on-site above IHSB PSRGs and site-specific background concentrations. The result of the
calculation indicated an adjusted IHSB screening level of 157.5 mg/kg for hexavalent chromium
and 3.0 mg/kg for thallium.

Based on the adjusted IHSB Industrial Screening Levels, only the concentration of thallium
detected in sample SB-3B 9 ft - 10 ft (3.7 mg/kg) was detected above its site specific adjusted
IHSB Industrial Screening Level of 3.0 mg/kg. The location of the thallium exceedances is deep
below ground and is not anticipated to be encountered during site redevelopment.

Heating Oil UST
During previous Phase II ESA activities, H&H collected sample SB-1 adjacent to an inactive
heating oil UST. The results of the analysis indicated the presence of diesel-range TPH above
the DEQ UST Section Action Level of 10 mg/kg. At the request of the prospective developer
(Charlotte-Mecklenburg Housing Partnership), H&H removed the UST on November 30, 2015.
Following removal of the tank, H&H collected a sample from below the tank (UST-Base) at the
same depth as previous sample SB-1 and collected a shallow (0 ft to 2 ft) soil sample (UST-N) to
determine if shallow soil impacts were present in the vicinity of the former UST. The results of
the samples UST-N and UST-Base indicate that VOCs and SVOCs are not present in the vicinity
of the former heating oil UST above IHSB Industrial PSRGs.

Waste Oil AST
During previous assessment activities, H&H collected a soil sample (SB-2) in the vicinity of
surficial soil staining observed adjacent to a former waste oil AST located on the western portion
of the property. The result of the laboratory analysis indicated the presence of diesel range TPH
above the DEQ UST Action Level of 10 mg/kg. For redevelopment purposes, H&H collected
shallow soil sample SB-14 (0- ft to 2 ft) adjacent to previous sample SB-2 for analysis of VOCs,
SVOCs, and HSL metals, and hexavalent chromium. The results of the laboratory indicated the
presence of acetone, benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene,
benzo(g,h,i)perylene, benzo(k)fluoranthene, chrysene, fluoranthene, indeno(1,2,3-cd)pyrene,
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phenanthrene, and pyrene above laboratory reporting limits; however, the concentrations
detected were below IHSB Industrial PSRGs. Several metals were also detected in sample SB-
14, but the concentrations detected were below their respective IHSB Industrial PSRG and/or
site-specific maximum background concentrations.

The analytical results of sample SB-14 indicate that VOCs, SVOCs, and HSL metals are not
present in the vicinity of the former heating oil UST above IHSB Industrial PSRGs.

Table 1
Soil Analytical Data Summary
Former Precision Dynamics Facility
Charlotte, North Carolina
H&H Job No. CHP.022
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Table 1 (Page 1 of 3)
Hart & Hickman, PC
Sample Location Drain
Patched Concrete Near Door
Sample ID SB-1 UST-N UST-Base SB-2 SB-14 SB-15 SB-16 SB-5 SB-6 SB-7
Sample Depth (ft)11-13 0-2 11-13 2-3 0-2 0-0.5(4)2.0-2.5 5-6 9-10 0-2 0-2 4-5 5-6 0.4-1
Sample Date 9/17/2013 11/30/2015 11/30/2015 9/17/2013 12/1/2015 9/17/2013 9/17/2013 1/24/2014 1/24/2014 12/1/2015 12/1/2015 9/17/2013 9/17/2013 9/17/2013
VOCs (8260)
Acetone NA 0.0488 0.0654 NA 0.323 NA NA NA NA NA NA <0.025 <0.023 0.12 12,000 100,000 24 NC
SVOCs (8270)
Benzo(a)anthracene NA <0.0067 <0.0067 NA 0.244 NA NA NA NA NA NA <0.44 <0.44 <0.44 0.16 2.9 0.18 NC
Benzo(a)pyrene NA <0.0067 <0.0067 NA 0.229 NA NA NA NA NA NA <0.44 <0.44 <0.44 0.016 0.29 0.059 7.25
Benzo(b)fluoranthene NA <0.0067 <0.0067 NA 0.302 NA NA NA NA NA NA <0.44 <0.44 <0.44 0.42 1.8 0.60 72.5
Benzo(g,h,i)perylene NA <0.0067 <0.0067 NA 0.179 NA NA NA NA NA NA <0.44 <0.44 <0.44 NS NS 7,800 NC
Benzo(k)fluoranthene NA <0.0067 <0.0067 NA 0.209 NA NA NA NA NA NA <0.44 <0.44 <0.44 1.6 29 5.9 NC
Chysene NA <0.0067 <0.0067 NA 0.293 NA NA NA NA NA NA <0.44 <0.44 <0.44 16 290 18 NC
Fluoranthene NA <0.0067 <0.0067 NA 0.623 NA NA NA NA NA NA <0.44 <0.44 <0.44 480 6,000 330 NC
Indeno(1,2,3-cd)pyrene NA <0.0067 <0.0067 NA 0.151 NA NA NA NA NA NA <0.44 <0.44 <0.44 0.16 2.9 2.0 NC
Phenanthrene NA <0.0067 <0.0067 NA 0.265 NA NA NA NA NA NA <0.44 <0.44 <0.44 NS NS 68 NC
Pyrene NA <0.0067 <0.0067 NA 0.496 NA NA NA NA NA NA <0.44 <0.44 <0.44 360 4,600 220 NC
HSL Metals (6010/7471/7196**) Range Mean
Antimony NA NA NA NA <1.27 4.2 <0.33 1.5 6.3 <1.70 <1.29 <0.34 <0.31 <0.33 6.2 94 0.9 NC 1.6 - 2.8 2.10
Arsenic NA NA NA NA 4.53 21 5.0 2.7 4.3 6.57 6.36 2.0 1.2 3.4 0.68 3.0 5.8 75 2.6 - 5.6 3.29
Beryllium NA NA NA NA <1.27 1.3 2.2 1.6 1.6 <1.70 <1.29 2.0 1.6 1.3 32 460 63 NC 1.1 - 1.8 1.48
Cadmium NA NA NA NA <1.27 <0.27 <0.33 <0.33 <0.36 1.94 <1.29 <0.34 <0.31 <0.33 14 160 3.0 NC ND ND
Chromium NA NA NA NA 41.5 580 37 30 290 103 35.3 34 53 53 24,000*100,000*360,000*NC 35 - 79 60.13
Chromium VI (Hexavalent)NA NA NA NA <1.29 6.7 7.1 <0.52 1.0 <0.540 <0.401 4.2 4.5 6.6 0.30 6.3 3.8 157.5 2.3 - 6.3 4.10
Copper NA NA NA NA 66.9 85 41 59 45 39.0 46.5 68 53 59 620 9,400 700 NC 39 - 79 56.88
Lead NA NA NA NA 38.3 35 17 4.0 <0.36 43.7 18.4 11 7.6 23 400 800 270 NC 1.5 - 27 7.20
Manganese NA NA NA NA 599 1,200 760 370 860 288 411 78 480 3,000 360 5,200 65 NC 160 - 2,600 562.50
Nickel NA NA NA NA 30.1 320 35 19 160 14.5 22.2 14 16 24 300 4,400 130 NC 14 - 28 19.00
Thallium NA NA NA NA <0.763 <0.54 <0.67 <0.66 3.7 <1.02 0.983 J <0.68 <0.62 2.7 0.16 2.4 0.28 3.0 0.99 - 1.5 1.25
Zinc NA NA NA NA 103 570 150 49 150 49.8 50.5 64 56 46 4,600 70,000 1,200 NC 28 - 56 40.13
Mercury NA NA NA NA <0.123 0.023 <0.028 <0.025 <0.030 <0.179 <1.36 <0.026 0.028 0.028 4.6 70 1.0 NC 0.032 - 0.050 0.04
TPH-DRO/GRO (8015)
Diesel-Range Organics (DRO)260 NA NA 160 NA NA NA NA NA NA NA NA NA NA 10
Gasoline-Range Organics (GRO)<5.9 NA NA <4.1 NA NA NA NA NA NA NA NA NA NA 10
Notes:
Units are mg/kg
1. NC DEQ Inactive Hazardous Sites Branch (IHSB) Residential and Industrial Health Based Preliminary Soil Remediation Goals (PSRGs) - September 2015
2. NC DEQ IHSB Protection of Groundwater Preliminary Soil Remediation Goals (POG PSRG) - September 2015
3. Site-specific IHSB Industrial Screening Levels
4. Sample SB-3 0ft-0.5ft is superseded by sample SB-16 0ft-2ft following metal slag removal and soil excavation.
5. Sample SB-8 0ft-0.5ft is superseded by sample SB-17 0ft-2ft following metal slag removal and soil excavation.
6. Sample SB-11 1ft-2ft is superseded by sample SB-18 0ft-2ft following metal slag removal and soil excavation.
*Chromium (III) screening criteria used
**Hexavalent chromium analyzed by EPA Method 7199 during December 2015 sampling event
Only constituents with at least one detection shown
EPA Method follows parameter in parenthesis
NA = Not Analyzed; NE = Not Established; ND = Not Detected;
NC = Not calculated
TPH = total petroleum hydrocarbons; DRO = Diesel Range Organics; GRO = Gasoline Range Organics
VOCs = Volatile Organic Compounds; SVOCs = Semi-VOCs; HSL = Hazardous Substance List
Bold and Underline indicates concentration is above adjusted IHSB Industrial Health Based Screening Level and the maximum background concentration or NC DEQ Action Level
SB-4 designation is not used.
SB-3 Residential
PSRG1
Industrial
PSRG1 POG PSRG2
UST Area Soil Staining Near Metal Fragments (southern area)Screening Levels
SB-3B
Site-Specific Background
Metals in Soil
NC DENR Action Level
Site Specific
Industrial SL3
Table 1
Soil Analytical Data Summary
Former Precision Dynamics Facility
Charlotte, North Carolina
H&H Job No. CHP.022
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Table 1 (Page 2 of 3)
Hart & Hickman, PC
Sample Location
Metal Fragments (eastern area)
Sample ID SB-8B SB-17 SB-19
Sample Depth (ft)0-0.5(5)2-2.5 4-5 0-2 0-2 1-2 4-5 1-2 4-5
Sample Date 9/17/2013 9/17/2013 1/24/2014 12/1/2015 12/1/2015 1/24/2014 1/24/2014 1/24/2014 1/24/2014
VOCs (8260)
Acetone NA NA NA NA NA NA NA NA NA 12,000 100,000 24 NC
SVOCs (8270)
Benzo(a)anthracene NA NA NA NA NA NA NA NA NA 0.16 2.9 0.18 NC
Benzo(a)pyrene NA NA NA NA NA NA NA NA NA 0.016 0.29 0.059 7.25
Benzo(b)fluoranthene NA NA NA NA NA NA NA NA NA 0.42 1.8 0.60 72.5
Benzo(g,h,i)perylene NA NA NA NA NA NA NA NA NA NS NS 7,800 NC
Benzo(k)fluoranthene NA NA NA NA NA NA NA NA NA 1.6 29 5.9 NC
Chysene NA NA NA NA NA NA NA NA NA 16 290 18 NC
Fluoranthene NA NA NA NA NA NA NA NA NA 480 6,000 330 NC
Indeno(1,2,3-cd)pyrene NA NA NA NA NA NA NA NA NA 0.16 2.9 2.0 NC
Phenanthrene NA NA NA NA NA NA NA NA NA NS NS 68 NC
Pyrene NA NA NA NA NA NA NA NA NA 360 4,600 220 NC
HSL Metals (6010/7471/7196) Range Mean
Antimony 0.41 0.77 1.9 <1.57 <1.22 3.7 4.5 1.7 1.5 6.2 94 0.9 NC 1.6 - 2.8 2.10
Arsenic 4.6 18 22 6.23 4.58 3.0 2.7 3.1 1.4 0.68 3.0 5.8 75 2.6 - 5.6 3.29
Beryllium 1.6 1.8 1.1 <1.57 <1.22 1.6 1.2 1.4 1.2 32 460 63 NC 1.1 - 1.8 1.48
Cadmium <0.30 <0.30 <0.32 2.01 <1.22 <0.34 <0.34 <0.34 <0.34 14 160 3.0 NC ND ND
Chromium 55 76 38 110 53.2 180 210 40 27 24,000*100,000*360,000*NC 35 - 79 60.13
Chromium VI (Hexavalent)8.6 7.8 2.2 <0.475 0.418 2.6 4.3 5.8 4.2 0.30 6.3 3.8 157.5 2.3 - 6.3 4.10
Copper 46 37 45 77.7 23.9 150 57 50 37 620 9,400 700 NC 39 - 79 56.88
Lead 12 11 21 27.4 18.4 <0.34 <0.36 4.5 4.2 400 800 270 NC 1.5 - 27 7.20
Manganese 280 1,900 320 89.2 872 290 760 81 82 360 5,200 65 NC 160 - 2,600 562.50
Nickel 15 20 14 25.7 14.9 52 70 11 8.4 300 4,400 130 NC 14 - 28 19.00
Thallium <0.60 1.4 <0.64 <0.944 <0.732 <0.67 1.3 <0.68 <0.66 0.16 2.4 0.28 3.0 0.99 - 1.5 1.25
Zinc 46 37 61 50.0 34.6 63 67 27 21 4,600 70,000 1,200 NC 28 - 56 40.13
Mercury <0.025 0.024 0.045 <0.159 <0.122 0.041 <0.027 0.13 <0.027 4.6 70 1.0 NC 0.032 - 0.050 0.04
TPH-DRO/GRO (8015)
Diesel-Range Organics (DRO)NA NA NA NA NA NA NA NA NA 10
Gasoline-Range Organics (GRO)NA NA NA NA NA NA NA NA NA 10
Notes:
Units are mg/kg
1. NC DEQ Inactive Hazardous Sites Branch (IHSB) Residential and Industrial Health Based Preliminary Soil Remediation Goals (PSRGs) - September 2015
2. NC DEQ IHSB Protection of Groundwater Preliminary Soil Remediation Goals (POG PSRG) - September 2015
3. Site-specific IHSB Industrial Screening Levels
4. Sample SB-3 0ft-0.5ft is superseded by sample SB-16 0ft-2ft following metal slag removal and soil excavation.
5. Sample SB-8 0ft-0.5ft is superseded by sample SB-17 0ft-2ft following metal slag removal and soil excavation.
6. Sample SB-11 1ft-2ft is superseded by sample SB-18 0ft-2ft following metal slag removal and soil excavation.
*Chromium (III) screening criteria used
**Hexavalent chromium analyzed by EPA Method 7199 during December 2015 sampling event
Only constituents with at least one detection shown
EPA Method follows parameter in parenthesis
NA = Not Analyzed; NE = Not Established; ND = Not Detected
NC = Not calculated
TPH = total petroleum hydrocarbons; DRO = Diesel Range Organics; GRO = Gasoline Range Organics
VOCs = Volatile Organic Compounds; SVOCs = Semi-VOCs; HSL = Hazardous Substance List
Bold and Underline indicates concentration is above adjusted IHSB Industrial Health Based Screening Level and the maximum background concentration or NC DEQ Action Level
SB-4 designation is not used.
POG PSRG2
SB-8 SB-10
Near Metal Fragments (northern area)Screening LevelsAsphalt
(northeastern area)Gravel (central area)
NC DENR Action Level
Site-Specific Background
Metals in Soil
SB-9 Residential
PSRG1
Industrial
PSRG1
Site Specific
Industrial SL3
Table 1
Soil Analytical Data Summary
Former Precision Dynamics Facility
Charlotte, North Carolina
H&H Job No. CHP.022
\\hhfs01.harthickman.local\masterfiles\AAA-Master Projects\Charlotte Mecklenburg Housing Partnership - CHP\CHP-022 Precision Dynamics Brownfields\Remediation\Tables for Report
Table 1 (Page 3 of 3)
Hart & Hickman, PC
Sample Location
Sample ID SB-18
Sample Depth (ft)1-2(6)4-5 9-10 0-2 1-2 4-5 4-5 9-10 1-2 3-4 6-7 1-2 3-4 1-2 3-4 6-7
Sample Date 1/24/2014 1/24/2014 1/24/2014 12/1/2015 1/24/2014 1/24/2014 1/24/2014 1/24/2014 1/24/2014 1/24/2014 1/24/2014 1/24/2014 1/24/2014 1/24/2014 1/24/2014 1/24/2014
VOCs (8260)
Acetone NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12,000 100,000 24 NC
SVOCs (8270)
Benzo(a)anthracene NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 0.16 2.9 0.18 NC
Benzo(a)pyrene NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 0.016 0.29 0.059 7.25
Benzo(b)fluoranthene NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 0.42 1.8 0.60 72.5
Benzo(g,h,i)perylene NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NS NS 7,800 NC
Benzo(k)fluoranthene NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 1.6 29 5.9 NC
Chysene NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 16 290 18 NC
Fluoranthene NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 480 6,000 330 NC
Indeno(1,2,3-cd)pyrene NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 0.16 2.9 2.0 NC
Phenanthrene NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NS NS 68 NC
Pyrene NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 360 4,600 220 NC
HSL Metals (6010/7471/7196) Range Mean
Antimony 1.8 1.6 2.0 <1.58 2.5 3.3 1.5 0.45 2.2 2.5 2.8 2.0 1.8 1.9 2.0 1.6 6.2 94 0.9 NC 1.6 - 2.8 2.10
Arsenic 27 2.3 3.2 7.20 3.0 2.5 2.8 0.43 3.0 2.9 3.0 2.9 2.6 3.0 5.6 3.3 0.68 3.0 5.8 75 2.6 - 5.6 3.29
Beryllium 1.3 1.1 1.3 <1.58 1.3 2.3 0.86 0.55 1.3 1.6 1.5 1.5 1.3 1.1 1.8 1.7 32 460 63 NC 1.1 - 1.8 1.48
Cadmium <0.30 <0.32 <0.34 1.99 <0.30 <0.33 <0.31 <0.29 <0.36 <0.33 <0.35 <0.33 <0.34 <0.31 <0.34 <0.31 14 160 3.0 NC ND ND
Chromium 50 50 60 82.0 130 180 53 21 58 79 63 71 38 71 66 35 24,000*100,000*360,000*NC 35 - 79 60.13
Chromium VI (Hexavalent)3.0 1.4 1.7 <0.477 1.6 1.7 1.6 0.75 6.3 4.3 3.7 3.8 3.3 5.5 3.6 2.3 0.30 6.3 3.8 157.5 2.3 - 6.3 4.10
Copper 31 30 57 44.4 31 62 28 12 46 55 60 51 51 39 79 74 620 9,400 700 NC 39 - 79 56.88
Lead 5.3 0.61 1.9 32.5 1.7 5.6 5.5 3.5 3.7 1.5 <0.35 3.6 2.9 27 8.7 3.0 400 800 270 NC 1.5 - 27 7.20
Manganese 230 99 170 126 78 1900 260 23 360 160 190 270 190 570 160 2600 360 5,200 65 NC 160 - 2,600 562.50
Nickel 13 12 13 20.8 14 26 8.3 4.9 18 18 28 16 16 14 20 22 300 4,400 130 NC 14 - 28 19.00
Thallium <0.61 <0.63 <0.68 0.948 J <0.59 <0.65 <0.62 <0.58 <0.73 <0.66 0.99 <0.65 <0.68 <0.62 <0.67 1.5 0.16 2.4 0.28 3.0 0.99 - 1.5 1.25
Zinc 28 20 25 38.4 28 35 21 12 33 31 44 28 40 42 56 47 4,600 70,000 1,200 NC 28 - 56 40.13
Mercury 0.041 0.042 0.084 <0.159 <0.024 0.094 0.029 0.034 0.038 0.037 0.050 0.032 0.049 0.047 <0.026 <0.026 4.6 70 1.0 NC 0.032 - 0.050 0.04
TPH-DRO/GRO (8015)
Diesel-Range Organics (DRO)NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 10
Gasoline-Range Organics (GRO)NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 10
Notes:
Units are mg/kg
1. NC DEQ Inactive Hazardous Sites Branch (IHSB) Residential and Industrial Health Based Preliminary Soil Remediation Goals (PSRGs) - September 2015
2. NC DEQ IHSB Protection of Groundwater Preliminary Soil Remediation Goals (POG PSRG) - September 2015
3. Site-specific IHSB Industrial Screening Levels
4. Sample SB-3 0ft-0.5ft is superseded by sample SB-16 0ft-2ft following metal slag removal and soil excavation.
5. Sample SB-8 0ft-0.5ft is superseded by sample SB-17 0ft-2ft following metal slag removal and soil excavation.
6. Sample SB-11 1ft-2ft is superseded by sample SB-18 0ft-2ft following metal slag removal and soil excavation.
*Chromium (III) screening criteria used
**Hexavalent chromium analyzed by EPA Method 7199 during December 2015 sampling event
Only constituents with at least one detection shown
EPA Method follows parameter in parenthesis
NA = Not Analyzed; NE = Not Established; ND = Not Detected
NC = Not Calculated
TPH = total petroleum hydrocarbons; DRO = Diesel Range Organics; GRO = Gasoline Range Organics
VOCs = Volatile Organic Compounds; SVOCs = Semi-VOCs; HSL = Hazardous Substance List
Bold and Underline indicates concentration is above adjusted IHSB Industrial Health Based Screening Level and the maximum background concentration or NC DEQ Action Level
SB-4 designation is not used.
SB-11 BG-1
Background
(northwestern area)
NC DENR Action Level
Background (southwestern area)
BG-3SB-12
Near Woodward Ave
(southeastern area)
Near Metal Fragments
(southerneastern area)Near Metal Fragments (northern area)
Site-Specific Background
Metals in Soil
Residential
PSRG1
Industrial
PSRG1 POG PSRG2
Background (northwestern area)
BG-2
Screening Levels
Site Specific
Industrial SL3
SB-13
SITE LOCATION MAP
Former Precision Dynamics Property
1033 CARTER AVENUE
CHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE NO:
1/13/2016 0
1 CHP-022
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
7.5 MINUTE SERIES (TOPOGRAPHIC)

2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f)
DERITA, NORTH CAROLINA 1996
CHARLOTTE EAST, NORTH CAROLINA 1991
SITE

APPENDIX A
Disposal Documentation

APPENDIX B
Laboratory Analytical Reports
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-93258-1
TestAmerica Sample Delivery Group: CHP-002
Client Project/Site: Precision Dynamics-NC
Revision: 3
For:
Hart & Hickman, PC
2923 S Tryon Street
Suite 100
Charlotte, North Carolina 28203
Attn: John Lopez
Authorized for release by:
1/13/2016 11:03:17 AM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Hart & Hickman, PC
Project/Site: Precision Dynamics-NC
TestAmerica Job ID: 490-93258-1
SDG: CHP-002
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Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .23
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .40
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .43
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .46
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .47
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .48
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .51
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Sample Summary
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-93258-1 UST-N(0-2)Solid 11/30/15 14:00 12/04/15 09:05
490-93258-2 UST-Base(11-13)Solid 11/30/15 14:30 12/04/15 09:05
490-93258-3 SB-14(0-2)Solid 12/01/15 16:00 12/04/15 09:05
490-93258-4 SB-15(0-2)Solid 12/01/15 16:15 12/04/15 09:05
490-93258-5 SB-16(0-2)Solid 12/01/15 16:30 12/04/15 09:05
490-93258-6 SB-17(0-2)Solid 12/01/15 16:45 12/04/15 09:05
490-93258-7 SB-18(0-2)Solid 12/01/15 17:00 12/04/15 09:05
490-93258-8 SB-19(0-2)Solid 12/01/15 17:15 12/04/15 09:05
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Case Narrative
Client: Hart & Hickman, PC TestAmerica Job ID: 490-93258-1
Project/Site: Precision Dynamics-NC SDG: CHP-002
Job ID: 490-93258-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-93258-1
REVISED REPORT3: Revised to report data to the RL, while addressing the detection of Antimony and Thallium to the MDL at the client's
request. This report replaces the one generated on 12/18/15 @ 1550.
Comments
No additional comments.
Receipt
The samples were received on 12/4/2015 9:05 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 1.2º C.
GC/MS VOA
Method(s) 8260B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
analytical batch 490-304578.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
Method(s) 8270D: The continuing calibration verification (CCV) associated with batch 490-304472 recovered above the upper control limit
for 2,4-Dinitrophenol and Hexachlorobutadiene. The samples associated with this CCV were non-detect for the affected analytes;
therefore, the data has been reported. The following sample is impacted: UST-N(0-2) (490-93258-1).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
HPLC/IC
Method(s) 7199: The following sample was diluted due to the nature of the sample matrix: SB-14(0-2) (490-93258-3). Elevated reporting
limits (RLs) are provided.The sample has dark brown matrix.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
6010C Thallium Evaluation to the MDL. The following samples were evaluated for Thallium to the Method Detection Level with the
following results:
SB-14(0-2) (490-93258-3) Sb = <1.27 mg/Kg, Tl = <0.763 mg/Kg;
SB-15(0-2) (490-93258-4) Sb = <1.70 mg/Kg, Tl = <1.02 mg/Kg;
SB-16(0-2) (490-93258-5) Sb = <1.29 mg/Kg, Tl = 0.983 mg/Kg with J flag;
SB-17(0-2) (490-93258-6) Sb = <1.57 mg/Kg, Tl - <0.944 mg/kg;
SB-18(0-2) (490-93258-7) Sb = <1.58 mg/Kg, Tl = 0.948 mg/Kg with J flag;
SB-19(0-2) (490-93258-8) Sb = <1.22 mg/Kg, Tl = <0.732 mg/Kg.
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Qualifiers
Metals
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
F2 MS/MSD RPD exceeds control limits
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Lab Sample ID: 490-93258-1Client Sample ID: UST-N(0-2)
Matrix: SolidDate Collected: 11/30/15 14:00
Date Received: 12/04/15 09:05
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.0488 0.0483 mg/Kg ☼11/30/15 14:00 12/08/15 04:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Benzene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Bromobenzene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Bromochloromethane ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Bromodichloromethane ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Bromoform ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Bromomethane ND
0.0483 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼2-Butanone (MEK)ND
0.00483 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Carbon disulfide ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Carbon tetrachloride ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Chlorobenzene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Chlorodibromomethane ND
0.00483 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Chloroethane ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Chloroform ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Chloromethane ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼2-Chlorotoluene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼4-Chlorotoluene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼cis-1,2-Dichloroethene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼cis-1,3-Dichloropropene ND
0.00483 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼1,2-Dibromo-3-Chloropropane ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼1,2-Dibromoethane (EDB)ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Dibromomethane ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼1,2-Dichlorobenzene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼1,3-Dichlorobenzene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼1,4-Dichlorobenzene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Dichlorodifluoromethane ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼1,1-Dichloroethane ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼1,2-Dichloroethane ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼1,1-Dichloroethene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼1,2-Dichloroethene, Total ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼1,2-Dichloropropane ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼1,3-Dichloropropane ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼2,2-Dichloropropane ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼1,1-Dichloropropene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Diisopropyl ether ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Ethylbenzene ND
0.00483 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Hexachlorobutadiene ND
0.0483 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼2-Hexanone ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Isopropylbenzene ND
0.00965 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Methylene Chloride ND
0.0483 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼4-Methyl-2-pentanone (MIBK)ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Methyl tert-butyl ether ND
0.00483 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Naphthalene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼n-Butylbenzene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼N-Propylbenzene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼p-Isopropyltoluene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼sec-Butylbenzene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Styrene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Lab Sample ID: 490-93258-1Client Sample ID: UST-N(0-2)
Matrix: SolidDate Collected: 11/30/15 14:00
Date Received: 12/04/15 09:05
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00193 mg/Kg ☼11/30/15 14:00 12/08/15 04:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼1,1,2,2-Tetrachloroethane ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Tetrachloroethene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Toluene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼trans-1,2-Dichloroethene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼trans-1,3-Dichloropropene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼1,2,3-Trichlorobenzene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼1,2,4-Trichlorobenzene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼1,1,1-Trichloroethane ND
0.00483 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼1,1,2-Trichloroethane ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Trichloroethene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Trichlorofluoromethane ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼1,2,3-Trichloropropane ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼1,2,4-Trimethylbenzene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼1,3,5-Trimethylbenzene ND
0.00193 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Vinyl chloride ND
0.00579 mg/Kg 11/30/15 14:00 12/08/15 04:43 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)103 70-130 11/30/15 14:00 12/08/15 04:43 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)104 11/30/15 14:00 12/08/15 04:43 170-130
1,2-Dichloroethane-d4 (Surr)104 11/30/15 14:00 12/08/15 04:43 170-130
Toluene-d8 (Surr)96 11/30/15 14:00 12/08/15 04:43 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0667 mg/Kg ☼12/07/15 14:20 12/08/15 01:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0667 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Acenaphthylene ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Anthracene ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Benzo[a]anthracene ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Benzo[a]pyrene ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Benzo[b]fluoranthene ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Benzo[g,h,i]perylene ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Benzo[k]fluoranthene ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Bis(2-chloroethoxy)methane ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Bis(2-chloroethyl)ether ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼bis (2-chloroisopropyl) ether ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Bis(2-ethylhexyl) phthalate ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼4-Bromophenyl phenyl ether ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Butyl benzyl phthalate ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Carbazole ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼4-Chloroaniline ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼4-Chloro-3-methylphenol ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼2-Chloronaphthalene ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼2-Chlorophenol ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼4-Chlorophenyl phenyl ether ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Chrysene ND
0.663 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Cresols ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Dibenz(a,h)anthracene ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Lab Sample ID: 490-93258-1Client Sample ID: UST-N(0-2)
Matrix: SolidDate Collected: 11/30/15 14:00
Date Received: 12/04/15 09:05
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 0.332 mg/Kg ☼12/07/15 14:20 12/08/15 01:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼1,3-Dichlorobenzene ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼1,4-Dichlorobenzene ND
0.664 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼3,3'-Dichlorobenzidine ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼2,4-Dichlorophenol ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Diethyl phthalate ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼2,4-Dimethylphenol ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Dimethyl phthalate ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Di-n-butyl phthalate ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼4,6-Dinitro-2-methylphenol ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼2,4-Dinitrophenol ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼2,4-Dinitrotoluene ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼2,6-Dinitrotoluene ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Di-n-octyl phthalate ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Fluoranthene ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Fluorene ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Hexachlorobenzene ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Hexachlorobutadiene ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Hexachlorocyclopentadiene ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Hexachloroethane ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Indeno[1,2,3-cd]pyrene ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Isophorone ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼1-Methylnaphthalene ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼2-Methylnaphthalene ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼2-Methylphenol ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼3 & 4 Methylphenol ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Naphthalene ND
0.829 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼2-Nitroaniline ND
0.829 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼3-Nitroaniline ND
0.829 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼4-Nitroaniline ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Nitrobenzene ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼2-Nitrophenol ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼4-Nitrophenol ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼N-Nitrosodi-n-propylamine ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.829 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Pentachlorophenol ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Phenanthrene ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Phenol ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼Pyrene ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼1,2,4-Trichlorobenzene ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼2,4,5-Trichlorophenol ND
0.332 mg/Kg 12/07/15 14:20 12/08/15 01:52 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)72 29-120 12/07/15 14:20 12/08/15 01:52 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)76 12/07/15 14:20 12/08/15 01:52 110-120
Nitrobenzene-d5 (Surr)77 12/07/15 14:20 12/08/15 01:52 127-120
Phenol-d5 (Surr)74 12/07/15 14:20 12/08/15 01:52 110-120
Terphenyl-d14 (Surr)72 12/07/15 14:20 12/08/15 01:52 113-120
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Client Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Lab Sample ID: 490-93258-1Client Sample ID: UST-N(0-2)
Matrix: SolidDate Collected: 11/30/15 14:00
Date Received: 12/04/15 09:05
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)102 10-120 12/07/15 14:20 12/08/15 01:52 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL RL
Percent Solids 76 0.10 %12/04/15 13:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Lab Sample ID: 490-93258-2Client Sample ID: UST-Base(11-13)
Matrix: SolidDate Collected: 11/30/15 14:30
Date Received: 12/04/15 09:05
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.0654 0.0583 mg/Kg ☼11/30/15 14:30 12/08/15 04:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Benzene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Bromobenzene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Bromochloromethane ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Bromodichloromethane ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Bromoform ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Bromomethane ND
0.0583 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼2-Butanone (MEK)ND
0.00583 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Carbon disulfide ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Carbon tetrachloride ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Chlorobenzene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Chlorodibromomethane ND
0.00583 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Chloroethane ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Chloroform ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Chloromethane ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼2-Chlorotoluene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼4-Chlorotoluene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼cis-1,2-Dichloroethene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼cis-1,3-Dichloropropene ND
0.00583 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼1,2-Dibromo-3-Chloropropane ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼1,2-Dibromoethane (EDB)ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Dibromomethane ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼1,2-Dichlorobenzene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼1,3-Dichlorobenzene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼1,4-Dichlorobenzene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Dichlorodifluoromethane ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼1,1-Dichloroethane ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼1,2-Dichloroethane ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼1,1-Dichloroethene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼1,2-Dichloroethene, Total ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼1,2-Dichloropropane ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼1,3-Dichloropropane ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼2,2-Dichloropropane ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼1,1-Dichloropropene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Diisopropyl ether ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Ethylbenzene ND
0.00583 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Hexachlorobutadiene ND
0.0583 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼2-Hexanone ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Isopropylbenzene ND
0.0117 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Methylene Chloride ND
0.0583 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼4-Methyl-2-pentanone (MIBK)ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Methyl tert-butyl ether ND
0.00583 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Naphthalene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼n-Butylbenzene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼N-Propylbenzene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼p-Isopropyltoluene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼sec-Butylbenzene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Styrene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Lab Sample ID: 490-93258-2Client Sample ID: UST-Base(11-13)
Matrix: SolidDate Collected: 11/30/15 14:30
Date Received: 12/04/15 09:05
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00233 mg/Kg ☼11/30/15 14:30 12/08/15 04:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼1,1,2,2-Tetrachloroethane ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Tetrachloroethene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Toluene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼trans-1,2-Dichloroethene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼trans-1,3-Dichloropropene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼1,2,3-Trichlorobenzene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼1,2,4-Trichlorobenzene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼1,1,1-Trichloroethane ND
0.00583 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼1,1,2-Trichloroethane ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Trichloroethene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Trichlorofluoromethane ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼1,2,3-Trichloropropane ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼1,2,4-Trimethylbenzene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼1,3,5-Trimethylbenzene ND
0.00233 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Vinyl chloride ND
0.00699 mg/Kg 11/30/15 14:30 12/08/15 04:12 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)97 70-130 11/30/15 14:30 12/08/15 04:12 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)109 11/30/15 14:30 12/08/15 04:12 170-130
1,2-Dichloroethane-d4 (Surr)105 11/30/15 14:30 12/08/15 04:12 170-130
Toluene-d8 (Surr)97 11/30/15 14:30 12/08/15 04:12 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0667 mg/Kg ☼12/07/15 14:20 12/08/15 15:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0667 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Acenaphthylene ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Anthracene ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Benzo[a]anthracene ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Benzo[a]pyrene ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Benzo[b]fluoranthene ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Benzo[g,h,i]perylene ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Benzo[k]fluoranthene ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Bis(2-chloroethoxy)methane ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Bis(2-chloroethyl)ether ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼bis (2-chloroisopropyl) ether ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Bis(2-ethylhexyl) phthalate ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼4-Bromophenyl phenyl ether ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Butyl benzyl phthalate ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Carbazole ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼4-Chloroaniline ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼4-Chloro-3-methylphenol ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼2-Chloronaphthalene ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼2-Chlorophenol ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼4-Chlorophenyl phenyl ether ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Chrysene ND
0.663 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Cresols ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Dibenz(a,h)anthracene ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Lab Sample ID: 490-93258-2Client Sample ID: UST-Base(11-13)
Matrix: SolidDate Collected: 11/30/15 14:30
Date Received: 12/04/15 09:05
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 0.331 mg/Kg ☼12/07/15 14:20 12/08/15 15:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼1,3-Dichlorobenzene ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼1,4-Dichlorobenzene ND
0.664 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼3,3'-Dichlorobenzidine ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼2,4-Dichlorophenol ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Diethyl phthalate ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼2,4-Dimethylphenol ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Dimethyl phthalate ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Di-n-butyl phthalate ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼4,6-Dinitro-2-methylphenol ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼2,4-Dinitrophenol ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼2,4-Dinitrotoluene ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼2,6-Dinitrotoluene ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Di-n-octyl phthalate ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Fluoranthene ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Fluorene ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Hexachlorobenzene ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Hexachlorobutadiene ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Hexachlorocyclopentadiene ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Hexachloroethane ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Indeno[1,2,3-cd]pyrene ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Isophorone ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼1-Methylnaphthalene ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼2-Methylnaphthalene ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼2-Methylphenol ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼3 & 4 Methylphenol ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Naphthalene ND
0.829 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼2-Nitroaniline ND
0.829 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼3-Nitroaniline ND
0.829 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼4-Nitroaniline ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Nitrobenzene ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼2-Nitrophenol ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼4-Nitrophenol ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼N-Nitrosodi-n-propylamine ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.829 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Pentachlorophenol ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Phenanthrene ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Phenol ND
0.0667 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼Pyrene ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼1,2,4-Trichlorobenzene ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼2,4,5-Trichlorophenol ND
0.331 mg/Kg 12/07/15 14:20 12/08/15 15:34 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)64 29-120 12/07/15 14:20 12/08/15 15:34 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)62 12/07/15 14:20 12/08/15 15:34 110-120
Nitrobenzene-d5 (Surr)63 12/07/15 14:20 12/08/15 15:34 127-120
Phenol-d5 (Surr)64 12/07/15 14:20 12/08/15 15:34 110-120
Terphenyl-d14 (Surr)69 12/07/15 14:20 12/08/15 15:34 113-120
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Client Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Lab Sample ID: 490-93258-2Client Sample ID: UST-Base(11-13)
Matrix: SolidDate Collected: 11/30/15 14:30
Date Received: 12/04/15 09:05
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)84 10-120 12/07/15 14:20 12/08/15 15:34 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL RL
Percent Solids 76 0.10 %12/04/15 13:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Lab Sample ID: 490-93258-3Client Sample ID: SB-14(0-2)
Matrix: SolidDate Collected: 12/01/15 16:00
Date Received: 12/04/15 09:05
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.323 0.0482 mg/Kg ☼12/01/15 16:00 12/08/15 03:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Benzene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Bromobenzene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Bromochloromethane ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Bromodichloromethane ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Bromoform ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Bromomethane ND
0.0482 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼2-Butanone (MEK)ND
0.00482 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Carbon disulfide ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Carbon tetrachloride ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Chlorobenzene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Chlorodibromomethane ND
0.00482 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Chloroethane ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Chloroform ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Chloromethane ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼2-Chlorotoluene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼4-Chlorotoluene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼cis-1,2-Dichloroethene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼cis-1,3-Dichloropropene ND
0.00482 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼1,2-Dibromo-3-Chloropropane ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼1,2-Dibromoethane (EDB)ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Dibromomethane ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼1,2-Dichlorobenzene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼1,3-Dichlorobenzene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼1,4-Dichlorobenzene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Dichlorodifluoromethane ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼1,1-Dichloroethane ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼1,2-Dichloroethane ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼1,1-Dichloroethene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼1,2-Dichloroethene, Total ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼1,2-Dichloropropane ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼1,3-Dichloropropane ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼2,2-Dichloropropane ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼1,1-Dichloropropene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Diisopropyl ether ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Ethylbenzene ND
0.00482 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Hexachlorobutadiene ND
0.0482 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼2-Hexanone ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Isopropylbenzene ND
0.00964 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Methylene Chloride ND
0.0482 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼4-Methyl-2-pentanone (MIBK)ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Methyl tert-butyl ether ND
0.00482 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Naphthalene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼n-Butylbenzene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼N-Propylbenzene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼p-Isopropyltoluene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼sec-Butylbenzene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Styrene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Lab Sample ID: 490-93258-3Client Sample ID: SB-14(0-2)
Matrix: SolidDate Collected: 12/01/15 16:00
Date Received: 12/04/15 09:05
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00193 mg/Kg ☼12/01/15 16:00 12/08/15 03:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼1,1,2,2-Tetrachloroethane ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Tetrachloroethene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Toluene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼trans-1,2-Dichloroethene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼trans-1,3-Dichloropropene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼1,2,3-Trichlorobenzene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼1,2,4-Trichlorobenzene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼1,1,1-Trichloroethane ND
0.00482 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼1,1,2-Trichloroethane ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Trichloroethene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Trichlorofluoromethane ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼1,2,3-Trichloropropane ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼1,2,4-Trimethylbenzene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼1,3,5-Trimethylbenzene ND
0.00193 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Vinyl chloride ND
0.00578 mg/Kg 12/01/15 16:00 12/08/15 03:41 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)104 70-130 12/01/15 16:00 12/08/15 03:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)108 12/01/15 16:00 12/08/15 03:41 170-130
1,2-Dichloroethane-d4 (Surr)106 12/01/15 16:00 12/08/15 03:41 170-130
Toluene-d8 (Surr)101 12/01/15 16:00 12/08/15 03:41 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.133 mg/Kg ☼12/07/15 14:20 12/08/15 15:58 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.133 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Acenaphthylene ND
0.133 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Anthracene ND
0.133 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Benzo[a]anthracene 0.244
0.133 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Benzo[a]pyrene 0.229
0.133 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Benzo[b]fluoranthene 0.302
0.133 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Benzo[g,h,i]perylene 0.179
0.133 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Benzo[k]fluoranthene 0.209
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Bis(2-chloroethoxy)methane ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Bis(2-chloroethyl)ether ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼bis (2-chloroisopropyl) ether ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Bis(2-ethylhexyl) phthalate ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼4-Bromophenyl phenyl ether ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Butyl benzyl phthalate ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Carbazole ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼4-Chloroaniline ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼4-Chloro-3-methylphenol ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼2-Chloronaphthalene ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼2-Chlorophenol ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼4-Chlorophenyl phenyl ether ND
0.133 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Chrysene 0.293
1.32 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Cresols ND
0.133 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Dibenz(a,h)anthracene ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Lab Sample ID: 490-93258-3Client Sample ID: SB-14(0-2)
Matrix: SolidDate Collected: 12/01/15 16:00
Date Received: 12/04/15 09:05
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 0.662 mg/Kg ☼12/07/15 14:20 12/08/15 15:58 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼1,3-Dichlorobenzene ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼1,4-Dichlorobenzene ND
1.33 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼3,3'-Dichlorobenzidine ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼2,4-Dichlorophenol ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Diethyl phthalate ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼2,4-Dimethylphenol ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Dimethyl phthalate ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Di-n-butyl phthalate ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼4,6-Dinitro-2-methylphenol ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼2,4-Dinitrophenol ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼2,4-Dinitrotoluene ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼2,6-Dinitrotoluene ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Di-n-octyl phthalate ND
0.133 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Fluoranthene 0.623
0.133 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Fluorene ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Hexachlorobenzene ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Hexachlorobutadiene ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Hexachlorocyclopentadiene ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Hexachloroethane ND
0.133 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Indeno[1,2,3-cd]pyrene 0.151
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Isophorone ND
0.133 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼1-Methylnaphthalene ND
0.133 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼2-Methylnaphthalene ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼2-Methylphenol ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼3 & 4 Methylphenol ND
0.133 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Naphthalene ND
1.66 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼2-Nitroaniline ND
1.66 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼3-Nitroaniline ND
1.66 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼4-Nitroaniline ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Nitrobenzene ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼2-Nitrophenol ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼4-Nitrophenol ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼N-Nitrosodi-n-propylamine ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
1.66 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Pentachlorophenol ND
0.133 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Phenanthrene 0.265
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Phenol ND
0.133 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼Pyrene 0.496
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼1,2,4-Trichlorobenzene ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼2,4,5-Trichlorophenol ND
0.662 mg/Kg 12/07/15 14:20 12/08/15 15:58 2☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)67 29-120 12/07/15 14:20 12/08/15 15:58 2
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)61 12/07/15 14:20 12/08/15 15:58 210-120
Nitrobenzene-d5 (Surr)66 12/07/15 14:20 12/08/15 15:58 227-120
Phenol-d5 (Surr)58 12/07/15 14:20 12/08/15 15:58 210-120
Terphenyl-d14 (Surr)72 12/07/15 14:20 12/08/15 15:58 213-120
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Client Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Lab Sample ID: 490-93258-3Client Sample ID: SB-14(0-2)
Matrix: SolidDate Collected: 12/01/15 16:00
Date Received: 12/04/15 09:05
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)84 10-120 12/07/15 14:20 12/08/15 15:58 2
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 7199 - Chromium, Hexavalent (IC)
RL MDL
Cr (VI)ND 1.29 mg/Kg ☼12/08/15 14:45 12/10/15 00:00 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Method: 6010C - Metals (ICP)
RL MDL
Antimony ND F2 F1 12.7 mg/Kg ☼12/07/15 08:40 12/07/15 16:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.54 mg/Kg 12/07/15 08:40 12/07/15 16:02 1☼Arsenic 4.53
1.27 mg/Kg 12/07/15 08:40 12/07/15 16:02 1☼Beryllium ND
1.27 mg/Kg 12/07/15 08:40 12/07/15 16:02 1☼Cadmium ND
1.27 mg/Kg 12/07/15 08:40 12/07/15 16:02 1☼Chromium 41.5
2.54 mg/Kg 12/07/15 08:40 12/07/15 16:02 1☼Copper 66.9
1.27 mg/Kg 12/07/15 08:40 12/07/15 16:02 1☼Lead 38.3 F1
3.82 mg/Kg 12/07/15 08:40 12/07/15 16:02 1☼Manganese 599 F1
2.54 mg/Kg 12/07/15 08:40 12/07/15 16:02 1☼Nickel 30.1
2.54 mg/Kg 12/07/15 08:40 12/07/15 16:02 1☼Selenium ND
1.27 mg/Kg 12/07/15 08:40 12/07/15 16:02 1☼Silver ND F2 F1
2.54 mg/Kg 12/07/15 08:40 12/07/15 16:02 1☼Thallium ND
12.7 mg/Kg 12/07/15 08:40 12/07/15 16:02 1☼Zinc 103
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.123 mg/Kg ☼12/07/15 15:28 12/07/15 21:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 78 0.10 %12/04/15 13:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Lab Sample ID: 490-93258-4Client Sample ID: SB-15(0-2)
Matrix: SolidDate Collected: 12/01/15 16:15
Date Received: 12/04/15 09:05
Method: 7199 - Chromium, Hexavalent (IC)
RL MDL
Cr (VI)ND 0.540 mg/Kg ☼12/08/15 14:45 12/10/15 00:13 3
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Method: 6010C - Metals (ICP)
RL MDL
Antimony ND 17.0 mg/Kg ☼12/07/15 08:40 12/07/15 16:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3.40 mg/Kg 12/07/15 08:40 12/07/15 16:32 1☼Arsenic 6.57
1.70 mg/Kg 12/07/15 08:40 12/07/15 16:32 1☼Beryllium ND
1.70 mg/Kg 12/07/15 08:40 12/07/15 16:32 1☼Cadmium 1.94
1.70 mg/Kg 12/07/15 08:40 12/07/15 16:32 1☼Chromium 103
3.40 mg/Kg 12/07/15 08:40 12/07/15 16:32 1☼Copper 39.0
1.70 mg/Kg 12/07/15 08:40 12/07/15 16:32 1☼Lead 43.7
5.10 mg/Kg 12/07/15 08:40 12/07/15 16:32 1☼Manganese 288
3.40 mg/Kg 12/07/15 08:40 12/07/15 16:32 1☼Nickel 14.5
3.40 mg/Kg 12/07/15 08:40 12/07/15 16:32 1☼Selenium ND
1.70 mg/Kg 12/07/15 08:40 12/07/15 16:32 1☼Silver ND
3.40 mg/Kg 12/07/15 08:40 12/07/15 16:32 1☼Thallium ND
17.0 mg/Kg 12/07/15 08:40 12/07/15 16:32 1☼Zinc 49.8
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.179 mg/Kg ☼12/07/15 15:28 12/07/15 21:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 56 0.10 %12/04/15 13:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Lab Sample ID: 490-93258-5Client Sample ID: SB-16(0-2)
Matrix: SolidDate Collected: 12/01/15 16:30
Date Received: 12/04/15 09:05
Method: 7199 - Chromium, Hexavalent (IC)
RL MDL
Cr (VI)ND 0.401 mg/Kg ☼12/08/15 14:45 12/10/15 00:25 3
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Method: 6010C - Metals (ICP)
RL MDL
Antimony ND 12.9 mg/Kg ☼12/07/15 08:40 12/07/15 16:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.59 mg/Kg 12/07/15 08:40 12/07/15 16:36 1☼Arsenic 6.36
1.29 mg/Kg 12/07/15 08:40 12/07/15 16:36 1☼Beryllium ND
1.29 mg/Kg 12/07/15 08:40 12/07/15 16:36 1☼Cadmium ND
1.29 mg/Kg 12/07/15 08:40 12/07/15 16:36 1☼Chromium 35.3
2.59 mg/Kg 12/07/15 08:40 12/07/15 16:36 1☼Copper 46.5
1.29 mg/Kg 12/07/15 08:40 12/07/15 16:36 1☼Lead 18.4
3.88 mg/Kg 12/07/15 08:40 12/07/15 16:36 1☼Manganese 411
2.59 mg/Kg 12/07/15 08:40 12/07/15 16:36 1☼Nickel 22.2
2.59 mg/Kg 12/07/15 08:40 12/07/15 16:36 1☼Selenium ND
1.29 mg/Kg 12/07/15 08:40 12/07/15 16:36 1☼Silver ND
2.59 mg/Kg 12/07/15 08:40 12/07/15 16:36 1☼Thallium ND
12.9 mg/Kg 12/07/15 08:40 12/07/15 16:36 1☼Zinc 50.5
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.136 mg/Kg ☼12/07/15 15:28 12/07/15 21:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 74 0.10 %12/04/15 13:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Lab Sample ID: 490-93258-6Client Sample ID: SB-17(0-2)
Matrix: SolidDate Collected: 12/01/15 16:45
Date Received: 12/04/15 09:05
Method: 7199 - Chromium, Hexavalent (IC)
RL MDL
Cr (VI)ND 0.475 mg/Kg ☼12/08/15 14:45 12/10/15 00:38 3
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Method: 6010C - Metals (ICP)
RL MDL
Antimony ND 15.7 mg/Kg ☼12/07/15 08:40 12/07/15 16:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3.15 mg/Kg 12/07/15 08:40 12/07/15 16:40 1☼Arsenic 6.23
1.57 mg/Kg 12/07/15 08:40 12/07/15 16:40 1☼Beryllium ND
1.57 mg/Kg 12/07/15 08:40 12/07/15 16:40 1☼Cadmium 2.01
1.57 mg/Kg 12/07/15 08:40 12/07/15 16:40 1☼Chromium 110
3.15 mg/Kg 12/07/15 08:40 12/07/15 16:40 1☼Copper 77.7
1.57 mg/Kg 12/07/15 08:40 12/07/15 16:40 1☼Lead 27.4
4.72 mg/Kg 12/07/15 08:40 12/07/15 16:40 1☼Manganese 89.2
3.15 mg/Kg 12/07/15 08:40 12/07/15 16:40 1☼Nickel 25.7
3.15 mg/Kg 12/07/15 08:40 12/07/15 16:40 1☼Selenium ND
1.57 mg/Kg 12/07/15 08:40 12/07/15 16:40 1☼Silver ND
3.15 mg/Kg 12/07/15 08:40 12/07/15 16:40 1☼Thallium ND
15.7 mg/Kg 12/07/15 08:40 12/07/15 16:40 1☼Zinc 50.0
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.159 mg/Kg ☼12/07/15 15:28 12/07/15 21:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 63 0.10 %12/04/15 13:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Lab Sample ID: 490-93258-7Client Sample ID: SB-18(0-2)
Matrix: SolidDate Collected: 12/01/15 17:00
Date Received: 12/04/15 09:05
Method: 7199 - Chromium, Hexavalent (IC)
RL MDL
Cr (VI)ND 0.477 mg/Kg ☼12/08/15 14:45 12/10/15 00:50 3
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Method: 6010C - Metals (ICP)
RL MDL
Antimony ND 15.8 mg/Kg ☼12/07/15 08:40 12/07/15 16:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3.16 mg/Kg 12/07/15 08:40 12/07/15 16:44 1☼Arsenic 7.20
1.58 mg/Kg 12/07/15 08:40 12/07/15 16:44 1☼Beryllium ND
1.58 mg/Kg 12/07/15 08:40 12/07/15 16:44 1☼Cadmium 1.99
1.58 mg/Kg 12/07/15 08:40 12/07/15 16:44 1☼Chromium 82.0
3.16 mg/Kg 12/07/15 08:40 12/07/15 16:44 1☼Copper 44.4
1.58 mg/Kg 12/07/15 08:40 12/07/15 16:44 1☼Lead 32.5
4.74 mg/Kg 12/07/15 08:40 12/07/15 16:44 1☼Manganese 126
3.16 mg/Kg 12/07/15 08:40 12/07/15 16:44 1☼Nickel 20.8
3.16 mg/Kg 12/07/15 08:40 12/07/15 16:44 1☼Selenium ND
1.58 mg/Kg 12/07/15 08:40 12/07/15 16:44 1☼Silver ND
3.16 mg/Kg 12/07/15 08:40 12/07/15 16:44 1☼Thallium ND
15.8 mg/Kg 12/07/15 08:40 12/07/15 16:44 1☼Zinc 38.4
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.159 mg/Kg ☼12/07/15 15:28 12/07/15 21:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 63 0.10 %12/04/15 13:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Lab Sample ID: 490-93258-8Client Sample ID: SB-19(0-2)
Matrix: SolidDate Collected: 12/01/15 17:15
Date Received: 12/04/15 09:05
Method: 7199 - Chromium, Hexavalent (IC)
RL MDL
Cr (VI)0.418 0.361 mg/Kg ☼12/08/15 14:45 12/10/15 01:03 3
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Method: 6010C - Metals (ICP)
RL MDL
Antimony ND 12.2 mg/Kg ☼12/07/15 08:40 12/07/15 16:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.44 mg/Kg 12/07/15 08:40 12/07/15 16:48 1☼Arsenic 4.58
1.22 mg/Kg 12/07/15 08:40 12/07/15 16:48 1☼Beryllium ND
1.22 mg/Kg 12/07/15 08:40 12/07/15 16:48 1☼Cadmium ND
1.22 mg/Kg 12/07/15 08:40 12/07/15 16:48 1☼Chromium 53.2
2.44 mg/Kg 12/07/15 08:40 12/07/15 16:48 1☼Copper 23.9
1.22 mg/Kg 12/07/15 08:40 12/07/15 16:48 1☼Lead 18.4
3.66 mg/Kg 12/07/15 08:40 12/07/15 16:48 1☼Manganese 872
2.44 mg/Kg 12/07/15 08:40 12/07/15 16:48 1☼Nickel 14.9
2.44 mg/Kg 12/07/15 08:40 12/07/15 16:48 1☼Selenium ND
1.22 mg/Kg 12/07/15 08:40 12/07/15 16:48 1☼Silver ND
2.44 mg/Kg 12/07/15 08:40 12/07/15 16:48 1☼Thallium ND
12.2 mg/Kg 12/07/15 08:40 12/07/15 16:48 1☼Zinc 34.6
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.122 mg/Kg ☼12/07/15 15:28 12/07/15 22:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 83 0.10 %12/04/15 13:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-304578/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304578
RL MDL
Acetone ND 0.0500 mg/Kg 12/08/15 00:05 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.00200 mg/Kg 12/08/15 00:05 1Benzene
ND 0.00200 mg/Kg 12/08/15 00:05 1Bromobenzene
ND 0.00200 mg/Kg 12/08/15 00:05 1Bromochloromethane
ND 0.00200 mg/Kg 12/08/15 00:05 1Bromodichloromethane
ND 0.00200 mg/Kg 12/08/15 00:05 1Bromoform
ND 0.00200 mg/Kg 12/08/15 00:05 1Bromomethane
ND 0.0500 mg/Kg 12/08/15 00:05 12-Butanone (MEK)
ND 0.00500 mg/Kg 12/08/15 00:05 1Carbon disulfide
ND 0.00200 mg/Kg 12/08/15 00:05 1Carbon tetrachloride
ND 0.00200 mg/Kg 12/08/15 00:05 1Chlorobenzene
ND 0.00200 mg/Kg 12/08/15 00:05 1Chlorodibromomethane
ND 0.00500 mg/Kg 12/08/15 00:05 1Chloroethane
ND 0.00200 mg/Kg 12/08/15 00:05 1Chloroform
ND 0.00200 mg/Kg 12/08/15 00:05 1Chloromethane
ND 0.00200 mg/Kg 12/08/15 00:05 12-Chlorotoluene
ND 0.00200 mg/Kg 12/08/15 00:05 14-Chlorotoluene
ND 0.00200 mg/Kg 12/08/15 00:05 1cis-1,2-Dichloroethene
ND 0.00200 mg/Kg 12/08/15 00:05 1cis-1,3-Dichloropropene
ND 0.00500 mg/Kg 12/08/15 00:05 11,2-Dibromo-3-Chloropropane
ND 0.00200 mg/Kg 12/08/15 00:05 11,2-Dibromoethane (EDB)
ND 0.00200 mg/Kg 12/08/15 00:05 1Dibromomethane
ND 0.00200 mg/Kg 12/08/15 00:05 11,2-Dichlorobenzene
ND 0.00200 mg/Kg 12/08/15 00:05 11,3-Dichlorobenzene
ND 0.00200 mg/Kg 12/08/15 00:05 11,4-Dichlorobenzene
ND 0.00200 mg/Kg 12/08/15 00:05 1Dichlorodifluoromethane
ND 0.00200 mg/Kg 12/08/15 00:05 11,1-Dichloroethane
ND 0.00200 mg/Kg 12/08/15 00:05 11,2-Dichloroethane
ND 0.00200 mg/Kg 12/08/15 00:05 11,1-Dichloroethene
ND 0.00200 mg/Kg 12/08/15 00:05 11,2-Dichloroethene, Total
ND 0.00200 mg/Kg 12/08/15 00:05 11,2-Dichloropropane
ND 0.00200 mg/Kg 12/08/15 00:05 11,3-Dichloropropane
ND 0.00200 mg/Kg 12/08/15 00:05 12,2-Dichloropropane
ND 0.00200 mg/Kg 12/08/15 00:05 11,1-Dichloropropene
ND 0.00200 mg/Kg 12/08/15 00:05 1Diisopropyl ether
ND 0.00200 mg/Kg 12/08/15 00:05 1Ethylbenzene
ND 0.00500 mg/Kg 12/08/15 00:05 1Hexachlorobutadiene
ND 0.0500 mg/Kg 12/08/15 00:05 12-Hexanone
ND 0.00200 mg/Kg 12/08/15 00:05 1Isopropylbenzene
ND 0.0100 mg/Kg 12/08/15 00:05 1Methylene Chloride
ND 0.0500 mg/Kg 12/08/15 00:05 14-Methyl-2-pentanone (MIBK)
ND 0.00200 mg/Kg 12/08/15 00:05 1Methyl tert-butyl ether
ND 0.00500 mg/Kg 12/08/15 00:05 1Naphthalene
ND 0.00200 mg/Kg 12/08/15 00:05 1n-Butylbenzene
ND 0.00200 mg/Kg 12/08/15 00:05 1N-Propylbenzene
ND 0.00200 mg/Kg 12/08/15 00:05 1p-Isopropyltoluene
ND 0.00200 mg/Kg 12/08/15 00:05 1sec-Butylbenzene
ND 0.00200 mg/Kg 12/08/15 00:05 1Styrene
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QC Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-304578/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304578
RL MDL
tert-Butylbenzene ND 0.00200 mg/Kg 12/08/15 00:05 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.00200 mg/Kg 12/08/15 00:05 11,1,1,2-Tetrachloroethane
ND 0.00200 mg/Kg 12/08/15 00:05 11,1,2,2-Tetrachloroethane
ND 0.00200 mg/Kg 12/08/15 00:05 1Tetrachloroethene
ND 0.00200 mg/Kg 12/08/15 00:05 1Toluene
ND 0.00200 mg/Kg 12/08/15 00:05 1trans-1,2-Dichloroethene
ND 0.00200 mg/Kg 12/08/15 00:05 1trans-1,3-Dichloropropene
ND 0.00200 mg/Kg 12/08/15 00:05 11,2,3-Trichlorobenzene
ND 0.00200 mg/Kg 12/08/15 00:05 11,2,4-Trichlorobenzene
ND 0.00200 mg/Kg 12/08/15 00:05 11,1,1-Trichloroethane
ND 0.00500 mg/Kg 12/08/15 00:05 11,1,2-Trichloroethane
ND 0.00200 mg/Kg 12/08/15 00:05 1Trichloroethene
ND 0.00200 mg/Kg 12/08/15 00:05 1Trichlorofluoromethane
ND 0.00200 mg/Kg 12/08/15 00:05 11,2,3-Trichloropropane
ND 0.00200 mg/Kg 12/08/15 00:05 11,2,4-Trimethylbenzene
ND 0.00200 mg/Kg 12/08/15 00:05 11,3,5-Trimethylbenzene
ND 0.00200 mg/Kg 12/08/15 00:05 1Vinyl chloride
ND 0.00600 mg/Kg 12/08/15 00:05 1Xylenes, Total
4-Bromofluorobenzene (Surr)118 70-130 12/08/15 00:05 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
107 12/08/15 00:05 1Dibromofluoromethane (Surr)70-130
107 12/08/15 00:05 11,2-Dichloroethane-d4 (Surr)70-130
97 12/08/15 00:05 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-304578/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304578
Acetone 0.250 0.2417 mg/Kg 97 51-149
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 0.0500 0.05072 mg/Kg 101 75-127
Bromobenzene 0.0500 0.04842 mg/Kg 97 75-130
Bromochloromethane 0.0500 0.05246 mg/Kg 105 70-132
Bromodichloromethane 0.0500 0.05376 mg/Kg 108 68-135
Bromoform 0.0500 0.05456 mg/Kg 109 36-150
Bromomethane 0.0500 0.03776 mg/Kg 76 43-142
2-Butanone (MEK)0.250 0.2805 mg/Kg 112 61-132
Carbon disulfide 0.0500 0.04315 mg/Kg 86 74-135
Carbon tetrachloride 0.0500 0.05096 mg/Kg 102 70-141
Chlorobenzene 0.0500 0.04948 mg/Kg 99 84-125
Chlorodibromomethane 0.0500 0.05351 mg/Kg 107 66-134
Chloroethane 0.0500 0.05163 mg/Kg 103 53-144
Chloroform 0.0500 0.05028 mg/Kg 101 76-130
Chloromethane 0.0500 0.04627 mg/Kg 93 23-150
2-Chlorotoluene 0.0500 0.04784 mg/Kg 96 78-132
4-Chlorotoluene 0.0500 0.04864 mg/Kg 97 77-138
cis-1,2-Dichloroethene 0.0500 0.05005 mg/Kg 100 75-125
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QC Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-304578/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304578
cis-1,3-Dichloropropene 0.0500 0.04865 mg/Kg 97 73-148
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,2-Dibromo-3-Chloropropane 0.0500 0.05126 mg/Kg 103 49-142
1,2-Dibromoethane (EDB)0.0500 0.05167 mg/Kg 103 80-135
Dibromomethane 0.0500 0.05410 mg/Kg 108 71-130
1,2-Dichlorobenzene 0.0500 0.05028 mg/Kg 101 80-134
1,3-Dichlorobenzene 0.0500 0.05150 mg/Kg 103 79-137
1,4-Dichlorobenzene 0.0500 0.04899 mg/Kg 98 77-139
Dichlorodifluoromethane 0.0500 0.04820 mg/Kg 96 12-144
1,1-Dichloroethane 0.0500 0.05282 mg/Kg 106 75-124
1,2-Dichloroethane 0.0500 0.05465 mg/Kg 109 65-134
1,1-Dichloroethene 0.0500 0.04486 mg/Kg 90 75-131
1,2-Dichloroethene, Total 0.100 0.09908 mg/Kg 99 75-128
1,2-Dichloropropane 0.0500 0.05156 mg/Kg 103 69-120
1,3-Dichloropropane 0.0500 0.05129 mg/Kg 103 78-126
2,2-Dichloropropane 0.0500 0.05136 mg/Kg 103 68-145
1,1-Dichloropropene 0.0500 0.04792 mg/Kg 96 79-127
Diisopropyl ether 0.0500 0.05168 mg/Kg 103 68-124
Ethylbenzene 0.0500 0.04846 mg/Kg 97 80-134
Hexachlorobutadiene 0.0500 0.05022 mg/Kg 100 65-148
2-Hexanone 0.250 0.2715 mg/Kg 109 57-148
Isopropylbenzene 0.0500 0.04842 mg/Kg 97 80-150
Methylene Chloride 0.0500 0.05237 mg/Kg 105 68-144
4-Methyl-2-pentanone (MIBK)0.250 0.2710 mg/Kg 108 59-138
Methyl tert-butyl ether 0.0500 0.04998 mg/Kg 100 70-136
Naphthalene 0.0500 0.04188 mg/Kg 84 69-150
n-Butylbenzene 0.0500 0.04921 mg/Kg 98 72-152
N-Propylbenzene 0.0500 0.05028 mg/Kg 101 75-137
p-Isopropyltoluene 0.0500 0.04933 mg/Kg 99 77-141
sec-Butylbenzene 0.0500 0.04916 mg/Kg 98 79-141
Styrene 0.0500 0.05059 mg/Kg 101 74-131
tert-Butylbenzene 0.0500 0.04857 mg/Kg 97 80-132
1,1,1,2-Tetrachloroethane 0.0500 0.05238 mg/Kg 105 80-136
1,1,2,2-Tetrachloroethane 0.0500 0.05687 mg/Kg 114 66-134
Tetrachloroethene 0.0500 0.04741 mg/Kg 95 78-140
Toluene 0.0500 0.04799 mg/Kg 96 80-132
trans-1,2-Dichloroethene 0.0500 0.04903 mg/Kg 98 76-128
trans-1,3-Dichloropropene 0.0500 0.04961 mg/Kg 99 62-139
1,2,3-Trichlorobenzene 0.0500 0.04893 mg/Kg 98 70-150
1,2,4-Trichlorobenzene 0.0500 0.04079 mg/Kg 82 62-150
1,1,1-Trichloroethane 0.0500 0.05150 mg/Kg 103 72-140
1,1,2-Trichloroethane 0.0500 0.05269 mg/Kg 105 78-128
Trichloroethene 0.0500 0.04910 mg/Kg 98 77-127
Trichlorofluoromethane 0.0500 0.05056 mg/Kg 101 50-140
1,2,3-Trichloropropane 0.0500 0.05666 mg/Kg 113 65-139
1,2,4-Trimethylbenzene 0.0500 0.04942 mg/Kg 99 77-139
1,3,5-Trimethylbenzene 0.0500 0.04909 mg/Kg 98 78-138
Vinyl chloride 0.0500 0.04886 mg/Kg 98 47-136
Xylenes, Total 0.100 0.09691 mg/Kg 97 80-137
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QC Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-304578/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304578
4-Bromofluorobenzene (Surr)70 -130
Surrogate
98
LCS LCS
Qualifier Limits%Recovery
105Dibromofluoromethane (Surr)70 -130
1051,2-Dichloroethane-d4 (Surr)70 -130
96Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-304578/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304578
Acetone 0.250 0.3220 mg/Kg 129 51-149 28 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 0.0500 0.05073 mg/Kg 101 75-127 0 50
Bromobenzene 0.0500 0.04877 mg/Kg 98 75-130 1 50
Bromochloromethane 0.0500 0.05294 mg/Kg 106 70-132 1 50
Bromodichloromethane 0.0500 0.05335 mg/Kg 107 68-135 1 50
Bromoform 0.0500 0.05922 mg/Kg 118 36-150 8 50
Bromomethane 0.0500 0.03657 mg/Kg 73 43-142 3 50
2-Butanone (MEK)0.250 0.2908 mg/Kg 116 61-132 4 50
Carbon disulfide 0.0500 0.04736 mg/Kg 95 74-135 9 50
Carbon tetrachloride 0.0500 0.05126 mg/Kg 103 70-141 1 50
Chlorobenzene 0.0500 0.04956 mg/Kg 99 84-125 0 50
Chlorodibromomethane 0.0500 0.06111 mg/Kg 122 66-134 13 50
Chloroethane 0.0500 0.05214 mg/Kg 104 53-144 1 50
Chloroform 0.0500 0.05007 mg/Kg 100 76-130 0 49
Chloromethane 0.0500 0.04817 mg/Kg 96 23-150 4 50
2-Chlorotoluene 0.0500 0.04847 mg/Kg 97 78-132 1 50
4-Chlorotoluene 0.0500 0.04921 mg/Kg 98 77-138 1 50
cis-1,2-Dichloroethene 0.0500 0.04773 mg/Kg 95 75-125 5 50
cis-1,3-Dichloropropene 0.0500 0.05422 mg/Kg 108 73-148 11 50
1,2-Dibromo-3-Chloropropane 0.0500 0.05692 mg/Kg 114 49-142 10 50
1,2-Dibromoethane (EDB)0.0500 0.05608 mg/Kg 112 80-135 8 50
Dibromomethane 0.0500 0.05558 mg/Kg 111 71-130 3 50
1,2-Dichlorobenzene 0.0500 0.05060 mg/Kg 101 80-134 1 50
1,3-Dichlorobenzene 0.0500 0.05137 mg/Kg 103 79-137 0 50
1,4-Dichlorobenzene 0.0500 0.04851 mg/Kg 97 77-139 1 50
Dichlorodifluoromethane 0.0500 0.04894 mg/Kg 98 12-144 2 50
1,1-Dichloroethane 0.0500 0.05182 mg/Kg 104 75-124 2 50
1,2-Dichloroethane 0.0500 0.05479 mg/Kg 110 65-134 0 50
1,1-Dichloroethene 0.0500 0.05007 mg/Kg 100 75-131 11 50
1,2-Dichloroethene, Total 0.100 0.09643 mg/Kg 96 75-128 3 41
1,2-Dichloropropane 0.0500 0.05135 mg/Kg 103 69-120 0 50
1,3-Dichloropropane 0.0500 0.05640 mg/Kg 113 78-126 9 42
2,2-Dichloropropane 0.0500 0.04925 mg/Kg 98 68-145 4 50
1,1-Dichloropropene 0.0500 0.04791 mg/Kg 96 79-127 0 50
Diisopropyl ether 0.0500 0.05079 mg/Kg 102 68-124 2 45
Ethylbenzene 0.0500 0.04842 mg/Kg 97 80-134 0 50
Hexachlorobutadiene 0.0500 0.05065 mg/Kg 101 65-148 1 50
2-Hexanone 0.250 0.3197 mg/Kg 128 57-148 16 50
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QC Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-304578/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304578
Isopropylbenzene 0.0500 0.05170 mg/Kg 103 80-150 7 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Methylene Chloride 0.0500 0.05256 mg/Kg 105 68-144 0 50
4-Methyl-2-pentanone (MIBK)0.250 0.3189 mg/Kg 128 59-138 16 50
Methyl tert-butyl ether 0.0500 0.04995 mg/Kg 100 70-136 0 50
Naphthalene 0.0500 0.04515 mg/Kg 90 69-150 8 50
n-Butylbenzene 0.0500 0.05044 mg/Kg 101 72-152 2 50
N-Propylbenzene 0.0500 0.05103 mg/Kg 102 75-137 1 50
p-Isopropyltoluene 0.0500 0.05014 mg/Kg 100 77-141 2 50
sec-Butylbenzene 0.0500 0.04989 mg/Kg 100 79-141 1 50
Styrene 0.0500 0.05199 mg/Kg 104 74-131 3 50
tert-Butylbenzene 0.0500 0.04895 mg/Kg 98 80-132 1 50
1,1,1,2-Tetrachloroethane 0.0500 0.05293 mg/Kg 106 80-136 1 50
1,1,2,2-Tetrachloroethane 0.0500 0.05765 mg/Kg 115 66-134 1 50
Tetrachloroethene 0.0500 0.05302 mg/Kg 106 78-140 11 50
Toluene 0.0500 0.05400 mg/Kg 108 80-132 12 50
trans-1,2-Dichloroethene 0.0500 0.04870 mg/Kg 97 76-128 1 50
trans-1,3-Dichloropropene 0.0500 0.05634 mg/Kg 113 62-139 13 50
1,2,3-Trichlorobenzene 0.0500 0.04746 mg/Kg 95 70-150 3 50
1,2,4-Trichlorobenzene 0.0500 0.04619 mg/Kg 92 62-150 12 50
1,1,1-Trichloroethane 0.0500 0.05238 mg/Kg 105 72-140 2 50
1,1,2-Trichloroethane 0.0500 0.05917 mg/Kg 118 78-128 12 50
Trichloroethene 0.0500 0.04985 mg/Kg 100 77-127 2 50
Trichlorofluoromethane 0.0500 0.05162 mg/Kg 103 50-140 2 50
1,2,3-Trichloropropane 0.0500 0.05864 mg/Kg 117 65-139 3 50
1,2,4-Trimethylbenzene 0.0500 0.05004 mg/Kg 100 77-139 1 50
1,3,5-Trimethylbenzene 0.0500 0.05007 mg/Kg 100 78-138 2 50
Vinyl chloride 0.0500 0.04802 mg/Kg 96 47-136 2 50
Xylenes, Total 0.100 0.09779 mg/Kg 98 80-137 1 50
4-Bromofluorobenzene (Surr)70 -130
Surrogate
96
LCSD LCSD
Qualifier Limits%Recovery
107Dibromofluoromethane (Surr)70 -130
1071,2-Dichloroethane-d4 (Surr)70 -130
108Toluene-d8 (Surr)70 -130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-304385/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304472 Prep Batch: 304385
RL MDL
Acenaphthene ND 0.0670 mg/Kg 12/07/15 09:57 12/07/15 19:59 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.0670 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Acenaphthylene
ND 0.0670 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Anthracene
ND 0.0670 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Benzo[a]anthracene
ND 0.0670 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Benzo[a]pyrene
ND 0.0670 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Benzo[b]fluoranthene
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QC Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-304385/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304472 Prep Batch: 304385
RL MDL
Benzo[g,h,i]perylene ND 0.0670 mg/Kg 12/07/15 09:57 12/07/15 19:59 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.0670 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Benzo[k]fluoranthene
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Bis(2-chloroethoxy)methane
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Bis(2-chloroethyl)ether
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 1bis (2-chloroisopropyl) ether
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Bis(2-ethylhexyl) phthalate
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 14-Bromophenyl phenyl ether
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Butyl benzyl phthalate
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Carbazole
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 14-Chloroaniline
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 14-Chloro-3-methylphenol
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 12-Chloronaphthalene
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 12-Chlorophenol
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 14-Chlorophenyl phenyl ether
ND 0.0670 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Chrysene
ND 0.666 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Cresols
ND 0.0670 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Dibenz(a,h)anthracene
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Dibenzofuran
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 11,2-Dichlorobenzene
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 11,3-Dichlorobenzene
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 11,4-Dichlorobenzene
ND 0.667 mg/Kg 12/07/15 09:57 12/07/15 19:59 13,3'-Dichlorobenzidine
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 12,4-Dichlorophenol
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Diethyl phthalate
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 12,4-Dimethylphenol
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Dimethyl phthalate
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Di-n-butyl phthalate
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 14,6-Dinitro-2-methylphenol
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 12,4-Dinitrophenol
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 12,4-Dinitrotoluene
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 12,6-Dinitrotoluene
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Di-n-octyl phthalate
ND 0.0670 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Fluoranthene
ND 0.0670 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Fluorene
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Hexachlorobenzene
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Hexachlorobutadiene
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Hexachlorocyclopentadiene
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Hexachloroethane
ND 0.0670 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Indeno[1,2,3-cd]pyrene
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Isophorone
ND 0.0670 mg/Kg 12/07/15 09:57 12/07/15 19:59 11-Methylnaphthalene
ND 0.0670 mg/Kg 12/07/15 09:57 12/07/15 19:59 12-Methylnaphthalene
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 12-Methylphenol
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 13 & 4 Methylphenol
ND 0.0670 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Naphthalene
ND 0.833 mg/Kg 12/07/15 09:57 12/07/15 19:59 12-Nitroaniline
ND 0.833 mg/Kg 12/07/15 09:57 12/07/15 19:59 13-Nitroaniline
ND 0.833 mg/Kg 12/07/15 09:57 12/07/15 19:59 14-Nitroaniline
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QC Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-304385/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304472 Prep Batch: 304385
RL MDL
Nitrobenzene ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 12-Nitrophenol
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 14-Nitrophenol
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 1N-Nitrosodi-n-propylamine
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 1n-Nitrosodiphenylamine(as
diphenylamine)
ND 0.833 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Pentachlorophenol
ND 0.0670 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Phenanthrene
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Phenol
ND 0.0670 mg/Kg 12/07/15 09:57 12/07/15 19:59 1Pyrene
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 11,2,4-Trichlorobenzene
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 12,4,5-Trichlorophenol
ND 0.333 mg/Kg 12/07/15 09:57 12/07/15 19:59 12,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)62 29-120 12/07/15 19:59 1
MB MB
Surrogate
12/07/15 09:57
Dil FacPreparedAnalyzedQualifierLimits%Recovery
68 12/07/15 09:57 12/07/15 19:59 12-Fluorophenol (Surr)10-120
67 12/07/15 09:57 12/07/15 19:59 1Nitrobenzene-d5 (Surr)27-120
67 12/07/15 09:57 12/07/15 19:59 1Phenol-d5 (Surr)10-120
67 12/07/15 09:57 12/07/15 19:59 1Terphenyl-d14 (Surr)13-120
83 12/07/15 09:57 12/07/15 19:59 12,4,6-Tribromophenol (Surr)10-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-304385/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304472 Prep Batch: 304385
Acenaphthene 1.67 1.098 mg/Kg 66 36-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 1.67 1.060 mg/Kg 64 38-120
Anthracene 1.67 1.104 mg/Kg 66 46-124
Benzo[a]anthracene 1.67 1.158 mg/Kg 70 45-120
Benzo[a]pyrene 1.67 1.117 mg/Kg 67 45-120
Benzo[b]fluoranthene 1.67 1.081 mg/Kg 65 42-120
Benzo[g,h,i]perylene 1.67 1.188 mg/Kg 71 38-120
Benzo[k]fluoranthene 1.67 1.198 mg/Kg 72 42-120
Bis(2-chloroethoxy)methane 1.67 1.072 mg/Kg 64 32-120
Bis(2-chloroethyl)ether 1.67 0.9623 mg/Kg 58 31-120
bis (2-chloroisopropyl) ether 1.67 1.217 mg/Kg 73 32-120
Bis(2-ethylhexyl) phthalate 1.67 1.140 mg/Kg 68 43-120
4-Bromophenyl phenyl ether 1.67 1.273 mg/Kg 76 40-120
Butyl benzyl phthalate 1.67 1.142 mg/Kg 69 43-133
Carbazole 1.67 1.080 mg/Kg 65 44-120
4-Chloroaniline 1.67 1.323 mg/Kg 79 35-120
4-Chloro-3-methylphenol 1.67 1.431 mg/Kg 86 38-120
2-Chloronaphthalene 1.67 1.092 mg/Kg 66 34-120
2-Chlorophenol 1.67 1.209 mg/Kg 73 32-120
4-Chlorophenyl phenyl ether 1.67 1.222 mg/Kg 73 42-120
Chrysene 1.67 1.168 mg/Kg 70 43-120
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QC Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-304385/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304472 Prep Batch: 304385
Cresols 3.33 2.454 mg/Kg 74 36-129
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Dibenz(a,h)anthracene 1.67 1.179 mg/Kg 71 32-128
Dibenzofuran 1.67 1.118 mg/Kg 67 41-120
1,2-Dichlorobenzene 1.67 1.159 mg/Kg 70 33-120
1,3-Dichlorobenzene 1.67 1.114 mg/Kg 67 32-120
1,4-Dichlorobenzene 1.67 1.153 mg/Kg 69 32-120
3,3'-Dichlorobenzidine 1.67 1.345 mg/Kg 81 39-120
2,4-Dichlorophenol 1.67 1.290 mg/Kg 77 32-120
Diethyl phthalate 1.67 1.287 mg/Kg 77 41-122
2,4-Dimethylphenol 1.67 1.378 mg/Kg 83 32-120
Dimethyl phthalate 1.67 1.191 mg/Kg 71 55-120
Di-n-butyl phthalate 1.67 1.165 mg/Kg 70 46-127
4,6-Dinitro-2-methylphenol 3.33 2.650 mg/Kg 79 27-134
2,4-Dinitrophenol 3.33 2.736 mg/Kg 82 10-142
2,4-Dinitrotoluene 1.67 1.350 mg/Kg 81 43-120
2,6-Dinitrotoluene 1.67 1.276 mg/Kg 77 43-120
Di-n-octyl phthalate 1.67 1.079 mg/Kg 65 40-130
Fluoranthene 1.67 1.151 mg/Kg 69 46-120
Fluorene 1.67 1.133 mg/Kg 68 42-120
Hexachlorobenzene 1.67 1.451 mg/Kg 87 44-120
Hexachlorobutadiene 1.67 1.653 mg/Kg 99 31-120
Hexachlorocyclopentadiene 1.67 1.387 mg/Kg 83 24-120
Hexachloroethane 1.67 1.339 mg/Kg 80 33-120
Indeno[1,2,3-cd]pyrene 1.67 1.173 mg/Kg 70 41-121
Isophorone 1.67 1.193 mg/Kg 72 33-120
1-Methylnaphthalene 1.67 1.200 mg/Kg 72 32-120
2-Methylnaphthalene 1.67 1.159 mg/Kg 70 28-120
2-Methylphenol 1.67 1.247 mg/Kg 75 36-120
3 & 4 Methylphenol 1.67 1.207 mg/Kg 72 37-120
Naphthalene 1.67 1.240 mg/Kg 74 32-120
2-Nitroaniline 1.67 1.246 mg/Kg 75 40-120
3-Nitroaniline 1.67 1.148 mg/Kg 69 42-120
4-Nitroaniline 1.67 1.200 mg/Kg 72 43-120
Nitrobenzene 1.67 1.233 mg/Kg 74 26-120
2-Nitrophenol 1.67 1.333 mg/Kg 80 29-120
4-Nitrophenol 3.33 2.662 mg/Kg 80 32-136
N-Nitrosodi-n-propylamine 1.67 1.105 mg/Kg 66 35-120
n-Nitrosodiphenylamine(as
diphenylamine)
3.33 2.212 mg/Kg 66 52-140
Pentachlorophenol 3.33 2.835 mg/Kg 85 44-134
Phenanthrene 1.67 1.062 mg/Kg 64 45-120
Phenol 1.67 1.099 mg/Kg 66 30-120
Pyrene 1.67 1.062 mg/Kg 64 43-120
1,2,4-Trichlorobenzene 1.67 1.306 mg/Kg 78 29-120
2,4,5-Trichlorophenol 1.67 1.298 mg/Kg 78 39-120
2,4,6-Trichlorophenol 1.67 1.281 mg/Kg 77 39-120
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QC Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-304385/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304472 Prep Batch: 304385
2-Fluorobiphenyl (Surr)29 -120
Surrogate
66
LCS LCS
Qualifier Limits%Recovery
662-Fluorophenol (Surr)10 -120
80Nitrobenzene-d5 (Surr)27 -120
69Phenol-d5 (Surr)10 -120
70Terphenyl-d14 (Surr)13 -120
922,4,6-Tribromophenol (Surr)10 -120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-304385/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304472 Prep Batch: 304385
Acenaphthene 1.67 1.199 mg/Kg 72 36-120 9 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acenaphthylene 1.67 1.148 mg/Kg 69 38-120 8 50
Anthracene 1.67 1.165 mg/Kg 70 46-124 5 49
Benzo[a]anthracene 1.67 1.251 mg/Kg 75 45-120 8 50
Benzo[a]pyrene 1.67 1.225 mg/Kg 74 45-120 9 50
Benzo[b]fluoranthene 1.67 1.210 mg/Kg 73 42-120 11 50
Benzo[g,h,i]perylene 1.67 1.195 mg/Kg 72 38-120 1 50
Benzo[k]fluoranthene 1.67 1.349 mg/Kg 81 42-120 12 45
Bis(2-chloroethoxy)methane 1.67 1.139 mg/Kg 68 32-120 6 50
Bis(2-chloroethyl)ether 1.67 1.092 mg/Kg 66 31-120 13 50
bis (2-chloroisopropyl) ether 1.67 1.335 mg/Kg 80 32-120 9 50
Bis(2-ethylhexyl) phthalate 1.67 1.234 mg/Kg 74 43-120 8 50
4-Bromophenyl phenyl ether 1.67 1.362 mg/Kg 82 40-120 7 37
Butyl benzyl phthalate 1.67 1.283 mg/Kg 77 43-133 12 50
Carbazole 1.67 1.147 mg/Kg 69 44-120 6 46
4-Chloroaniline 1.67 1.371 mg/Kg 82 35-120 4 50
4-Chloro-3-methylphenol 1.67 1.389 mg/Kg 83 38-120 3 49
2-Chloronaphthalene 1.67 1.053 mg/Kg 63 34-120 4 50
2-Chlorophenol 1.67 1.345 mg/Kg 81 32-120 11 50
4-Chlorophenyl phenyl ether 1.67 1.299 mg/Kg 78 42-120 6 50
Chrysene 1.67 1.261 mg/Kg 76 43-120 8 49
Cresols 3.33 2.665 mg/Kg 80 36-129 8 50
Dibenz(a,h)anthracene 1.67 1.165 mg/Kg 70 32-128 1 50
Dibenzofuran 1.67 1.204 mg/Kg 72 41-120 7 50
1,2-Dichlorobenzene 1.67 1.205 mg/Kg 72 33-120 4 50
1,3-Dichlorobenzene 1.67 1.200 mg/Kg 72 32-120 7 50
1,4-Dichlorobenzene 1.67 1.240 mg/Kg 74 32-120 7 50
3,3'-Dichlorobenzidine 1.67 1.497 mg/Kg 90 39-120 11 50
2,4-Dichlorophenol 1.67 1.316 mg/Kg 79 32-120 2 50
Diethyl phthalate 1.67 1.336 mg/Kg 80 41-122 4 45
2,4-Dimethylphenol 1.67 1.423 mg/Kg 85 32-120 3 50
Dimethyl phthalate 1.67 1.308 mg/Kg 78 55-120 9 46
Di-n-butyl phthalate 1.67 1.253 mg/Kg 75 46-127 7 49
4,6-Dinitro-2-methylphenol 3.33 2.980 mg/Kg 89 27-134 12 50
2,4-Dinitrophenol 3.33 2.937 mg/Kg 88 10-142 7 50
2,4-Dinitrotoluene 1.67 1.462 mg/Kg 88 43-120 8 50
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QC Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-304385/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304472 Prep Batch: 304385
2,6-Dinitrotoluene 1.67 1.373 mg/Kg 82 43-120 7 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Di-n-octyl phthalate 1.67 1.090 mg/Kg 65 40-130 1 50
Fluoranthene 1.67 1.222 mg/Kg 73 46-120 6 50
Fluorene 1.67 1.192 mg/Kg 72 42-120 5 50
Hexachlorobenzene 1.67 1.533 mg/Kg 92 44-120 6 50
Hexachlorobutadiene 1.67 1.602 mg/Kg 96 31-120 3 50
Hexachlorocyclopentadiene 1.67 1.352 mg/Kg 81 24-120 3 50
Hexachloroethane 1.67 1.354 mg/Kg 81 33-120 1 50
Indeno[1,2,3-cd]pyrene 1.67 1.172 mg/Kg 70 41-121 0 50
Isophorone 1.67 1.287 mg/Kg 77 33-120 8 50
1-Methylnaphthalene 1.67 1.198 mg/Kg 72 32-120 0 50
2-Methylnaphthalene 1.67 1.101 mg/Kg 66 28-120 5 50
2-Methylphenol 1.67 1.359 mg/Kg 82 36-120 9 50
3 & 4 Methylphenol 1.67 1.306 mg/Kg 78 37-120 8 50
Naphthalene 1.67 1.265 mg/Kg 76 32-120 2 50
2-Nitroaniline 1.67 1.159 mg/Kg 70 40-120 7 50
3-Nitroaniline 1.67 1.235 mg/Kg 74 42-120 7 49
4-Nitroaniline 1.67 1.297 mg/Kg 78 43-120 8 49
Nitrobenzene 1.67 1.350 mg/Kg 81 26-120 9 50
2-Nitrophenol 1.67 1.413 mg/Kg 85 29-120 6 50
4-Nitrophenol 3.33 2.939 mg/Kg 88 32-136 10 45
N-Nitrosodi-n-propylamine 1.67 1.223 mg/Kg 73 35-120 10 50
n-Nitrosodiphenylamine(as
diphenylamine)
3.33 2.399 mg/Kg 72 52-140 8 50
Pentachlorophenol 3.33 3.049 mg/Kg 91 44-134 7 50
Phenanthrene 1.67 1.149 mg/Kg 69 45-120 8 50
Phenol 1.67 1.174 mg/Kg 70 30-120 7 50
Pyrene 1.67 1.207 mg/Kg 72 43-120 13 50
1,2,4-Trichlorobenzene 1.67 1.343 mg/Kg 81 29-120 3 50
2,4,5-Trichlorophenol 1.67 1.206 mg/Kg 72 39-120 7 50
2,4,6-Trichlorophenol 1.67 1.223 mg/Kg 73 39-120 5 50
2-Fluorobiphenyl (Surr)29 -120
Surrogate
60
LCSD LCSD
Qualifier Limits%Recovery
732-Fluorophenol (Surr)10 -120
87Nitrobenzene-d5 (Surr)27 -120
71Phenol-d5 (Surr)10 -120
79Terphenyl-d14 (Surr)13 -120
932,4,6-Tribromophenol (Surr)10 -120
Client Sample ID: Matrix SpikeLab Sample ID: 490-93371-B-8-G MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304472 Prep Batch: 304385
Acenaphthene ND 2.21 1.500 mg/Kg 68 19-120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acenaphthylene ND 2.21 1.481 mg/Kg 67 25-120☼
Anthracene ND 2.21 1.515 mg/Kg 69 28-125☼
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QC Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-93371-B-8-G MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304472 Prep Batch: 304385
Benzo[a]anthracene ND 2.21 1.581 mg/Kg 72 23-120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Benzo[a]pyrene ND 2.21 1.543 mg/Kg 70 15-128☼
Benzo[b]fluoranthene ND 2.21 1.738 mg/Kg 79 12-133☼
Benzo[g,h,i]perylene ND 2.21 1.481 mg/Kg 67 22-120☼
Benzo[k]fluoranthene ND 2.21 1.690 mg/Kg 77 28-120☼
Bis(2-chloroethoxy)methane ND 2.21 1.435 mg/Kg 65 24-120☼
Bis(2-chloroethyl)ether ND 2.21 1.366 mg/Kg 62 22-120☼
bis (2-chloroisopropyl) ether ND 2.21 1.774 mg/Kg 80 20-120☼
Bis(2-ethylhexyl) phthalate ND 2.21 1.602 mg/Kg 73 26-120☼
4-Bromophenyl phenyl ether ND 2.21 1.766 mg/Kg 80 31-120☼
Butyl benzyl phthalate ND 2.21 1.625 mg/Kg 74 24-133☼
Carbazole ND 2.21 1.508 mg/Kg 68 25-123☼
4-Chloroaniline ND 2.21 1.761 mg/Kg 80 26-120☼
4-Chloro-3-methylphenol ND 2.21 1.868 mg/Kg 85 21-120☼
2-Chloronaphthalene ND 2.21 1.510 mg/Kg 68 24-120☼
2-Chlorophenol ND 2.21 1.672 mg/Kg 76 25-120☼
4-Chlorophenyl phenyl ether ND 2.21 1.660 mg/Kg 75 26-120☼
Chrysene ND 2.21 1.603 mg/Kg 73 20-120☼
Cresols ND 4.41 3.397 mg/Kg 77 10-200☼
Dibenz(a,h)anthracene ND 2.21 1.546 mg/Kg 70 12-128☼
Dibenzofuran ND 2.21 1.526 mg/Kg 69 21-120☼
1,2-Dichlorobenzene ND 2.21 1.504 mg/Kg 68 10-120☼
1,3-Dichlorobenzene ND 2.21 1.540 mg/Kg 70 10-120☼
1,4-Dichlorobenzene ND 2.21 1.616 mg/Kg 73 10-120☼
3,3'-Dichlorobenzidine ND 2.21 1.841 mg/Kg 83 10-120☼
2,4-Dichlorophenol ND 2.21 1.703 mg/Kg 77 17-120☼
Diethyl phthalate ND 2.21 1.690 mg/Kg 77 29-122☼
2,4-Dimethylphenol ND 2.21 1.810 mg/Kg 82 17-120☼
Dimethyl phthalate ND 2.21 1.620 mg/Kg 73 30-120☼
Di-n-butyl phthalate ND 2.21 1.630 mg/Kg 74 29-126☼
4,6-Dinitro-2-methylphenol ND 4.41 3.736 mg/Kg 85 10-134☼
2,4-Dinitrophenol ND 4.41 3.324 mg/Kg 75 10-150☼
2,4-Dinitrotoluene ND 2.21 1.808 mg/Kg 82 24-121☼
2,6-Dinitrotoluene ND 2.21 1.829 mg/Kg 83 24-120☼
Di-n-octyl phthalate ND 2.21 1.688 mg/Kg 76 27-130☼
Fluoranthene ND 2.21 1.560 mg/Kg 71 10-143☼
Fluorene ND 2.21 1.524 mg/Kg 69 20-120☼
Hexachlorobenzene ND 2.21 1.936 mg/Kg 88 25-120☼
Hexachlorobutadiene ND 2.21 2.094 mg/Kg 95 10-120☼
Hexachlorocyclopentadiene ND 2.21 1.844 mg/Kg 84 10-120☼
Hexachloroethane ND 2.21 1.787 mg/Kg 81 10-120☼
Indeno[1,2,3-cd]pyrene ND 2.21 1.520 mg/Kg 69 22-121☼
Isophorone ND 2.21 1.614 mg/Kg 73 24-120☼
1-Methylnaphthalene ND 2.21 1.611 mg/Kg 73 10-120☼
2-Methylnaphthalene ND 2.21 1.525 mg/Kg 69 13-120☼
2-Methylphenol ND 2.21 1.701 mg/Kg 77 23-120☼
3 & 4 Methylphenol ND 2.21 1.696 mg/Kg 77 19-120☼
Naphthalene ND 2.21 1.626 mg/Kg 74 10-120☼
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-93371-B-8-G MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304472 Prep Batch: 304385
2-Nitroaniline ND 2.21 1.776 mg/Kg 80 31-120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
3-Nitroaniline ND 2.21 1.590 mg/Kg 72 31-120☼
4-Nitroaniline ND 2.21 1.637 mg/Kg 74 28-120☼
Nitrobenzene ND 2.21 1.682 mg/Kg 76 19-120☼
2-Nitrophenol ND 2.21 1.776 mg/Kg 80 23-120☼
4-Nitrophenol ND 4.41 3.723 mg/Kg 84 16-139☼
N-Nitrosodi-n-propylamine ND 2.21 1.476 mg/Kg 67 24-120☼
n-Nitrosodiphenylamine(as
diphenylamine)
ND 4.41 3.022 mg/Kg 68 26-150☼
Pentachlorophenol ND 4.41 4.278 mg/Kg 97 19-145☼
Phenanthrene ND 2.21 1.513 mg/Kg 69 21-122☼
Phenol ND 2.21 1.476 mg/Kg 67 15-120☼
Pyrene ND 2.21 1.513 mg/Kg 69 20-123☼
1,2,4-Trichlorobenzene ND 2.21 1.679 mg/Kg 76 14-120☼
2,4,5-Trichlorophenol ND 2.21 1.790 mg/Kg 81 27-120☼
2,4,6-Trichlorophenol ND 2.21 1.713 mg/Kg 78 24-122☼
2-Fluorobiphenyl (Surr)29 -120
Surrogate
69
MS MS
Qualifier Limits%Recovery
652-Fluorophenol (Surr)10 -120
79Nitrobenzene-d5 (Surr)27 -120
68Phenol-d5 (Surr)10 -120
76Terphenyl-d14 (Surr)13 -120
952,4,6-Tribromophenol (Surr)10 -120
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-93371-B-8-H MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304472 Prep Batch: 304385
Acenaphthene ND 2.18 1.345 mg/Kg 62 19-120 11 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acenaphthylene ND 2.18 1.295 mg/Kg 59 25-120 13 50☼
Anthracene ND 2.18 1.311 mg/Kg 60 28-125 14 49☼
Benzo[a]anthracene ND 2.18 1.386 mg/Kg 64 23-120 13 50☼
Benzo[a]pyrene ND 2.18 1.332 mg/Kg 61 15-128 15 50☼
Benzo[b]fluoranthene ND 2.18 1.361 mg/Kg 62 12-133 24 50☼
Benzo[g,h,i]perylene ND 2.18 1.396 mg/Kg 64 22-120 6 50☼
Benzo[k]fluoranthene ND 2.18 1.378 mg/Kg 63 28-120 20 45☼
Bis(2-chloroethoxy)methane ND 2.18 1.265 mg/Kg 58 24-120 13 50☼
Bis(2-chloroethyl)ether ND 2.18 1.250 mg/Kg 57 22-120 9 50☼
bis (2-chloroisopropyl) ether ND 2.18 1.369 mg/Kg 63 20-120 26 50☼
Bis(2-ethylhexyl) phthalate ND 2.18 1.421 mg/Kg 65 26-120 12 50☼
4-Bromophenyl phenyl ether ND 2.18 1.594 mg/Kg 73 31-120 10 37☼
Butyl benzyl phthalate ND 2.18 1.383 mg/Kg 63 24-133 16 50☼
Carbazole ND 2.18 1.316 mg/Kg 60 25-123 14 46☼
4-Chloroaniline ND 2.18 1.460 mg/Kg 67 26-120 19 50☼
4-Chloro-3-methylphenol ND 2.18 1.629 mg/Kg 75 21-120 14 49☼
2-Chloronaphthalene ND 2.18 1.349 mg/Kg 62 24-120 11 50☼
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QC Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-93371-B-8-H MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304472 Prep Batch: 304385
2-Chlorophenol ND 2.18 1.405 mg/Kg 64 25-120 17 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
4-Chlorophenyl phenyl ether ND 2.18 1.516 mg/Kg 70 26-120 9 50☼
Chrysene ND 2.18 1.359 mg/Kg 62 20-120 17 49☼
Cresols ND 4.36 2.797 mg/Kg 64 10-200 19 50☼
Dibenz(a,h)anthracene ND 2.18 1.433 mg/Kg 66 12-128 8 50☼
Dibenzofuran ND 2.18 1.381 mg/Kg 63 21-120 10 50☼
1,2-Dichlorobenzene ND 2.18 1.301 mg/Kg 60 10-120 14 50☼
1,3-Dichlorobenzene ND 2.18 1.278 mg/Kg 59 10-120 19 50☼
1,4-Dichlorobenzene ND 2.18 1.276 mg/Kg 58 10-120 24 50☼
3,3'-Dichlorobenzidine ND 2.18 1.668 mg/Kg 76 10-120 10 50☼
2,4-Dichlorophenol ND 2.18 1.433 mg/Kg 66 17-120 17 50☼
Diethyl phthalate ND 2.18 1.527 mg/Kg 70 29-122 10 45☼
2,4-Dimethylphenol ND 2.18 1.555 mg/Kg 71 17-120 15 50☼
Dimethyl phthalate ND 2.18 1.453 mg/Kg 67 30-120 11 46☼
Di-n-butyl phthalate ND 2.18 1.456 mg/Kg 67 29-126 11 49☼
4,6-Dinitro-2-methylphenol ND 4.36 3.300 mg/Kg 76 10-134 12 50☼
2,4-Dinitrophenol ND 4.36 3.126 mg/Kg 72 10-150 6 50☼
2,4-Dinitrotoluene ND 2.18 1.632 mg/Kg 75 24-121 10 50☼
2,6-Dinitrotoluene ND 2.18 1.547 mg/Kg 71 24-120 17 50☼
Di-n-octyl phthalate ND 2.18 1.317 mg/Kg 60 27-130 25 50☼
Fluoranthene ND 2.18 1.393 mg/Kg 64 10-143 11 50☼
Fluorene ND 2.18 1.356 mg/Kg 62 20-120 12 50☼
Hexachlorobenzene ND 2.18 1.740 mg/Kg 80 25-120 11 50☼
Hexachlorobutadiene ND 2.18 1.751 mg/Kg 80 10-120 18 50☼
Hexachlorocyclopentadiene ND 2.18 1.585 mg/Kg 73 10-120 15 50☼
Hexachloroethane ND 2.18 1.461 mg/Kg 67 10-120 20 50☼
Indeno[1,2,3-cd]pyrene ND 2.18 1.391 mg/Kg 64 22-121 9 50☼
Isophorone ND 2.18 1.364 mg/Kg 63 24-120 17 50☼
1-Methylnaphthalene ND 2.18 1.355 mg/Kg 62 10-120 17 50☼
2-Methylnaphthalene ND 2.18 1.285 mg/Kg 59 13-120 17 50☼
2-Methylphenol ND 2.18 1.411 mg/Kg 65 23-120 19 50☼
3 & 4 Methylphenol ND 2.18 1.386 mg/Kg 64 19-120 20 50☼
Naphthalene ND 2.18 1.379 mg/Kg 63 10-120 16 50☼
2-Nitroaniline ND 2.18 1.612 mg/Kg 74 31-120 10 50☼
3-Nitroaniline ND 2.18 1.396 mg/Kg 64 31-120 13 49☼
4-Nitroaniline ND 2.18 1.494 mg/Kg 69 28-120 9 49☼
Nitrobenzene ND 2.18 1.462 mg/Kg 67 19-120 14 50☼
2-Nitrophenol ND 2.18 1.490 mg/Kg 68 23-120 17 50☼
4-Nitrophenol ND 4.36 3.373 mg/Kg 77 16-139 10 45☼
N-Nitrosodi-n-propylamine ND 2.18 1.319 mg/Kg 60 24-120 11 50☼
n-Nitrosodiphenylamine(as
diphenylamine)
ND 4.36 2.697 mg/Kg 62 26-150 11 50☼
Pentachlorophenol ND 4.36 3.725 mg/Kg 85 19-145 14 50☼
Phenanthrene ND 2.18 1.282 mg/Kg 59 21-122 17 50☼
Phenol ND 2.18 1.211 mg/Kg 56 15-120 20 50☼
Pyrene ND 2.18 1.254 mg/Kg 57 20-123 19 50☼
1,2,4-Trichlorobenzene ND 2.18 1.433 mg/Kg 66 14-120 16 50☼
2,4,5-Trichlorophenol ND 2.18 1.586 mg/Kg 73 27-120 12 50☼
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QC Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-93371-B-8-H MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304472 Prep Batch: 304385
2,4,6-Trichlorophenol ND 2.18 1.576 mg/Kg 72 24-122 8 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
2-Fluorobiphenyl (Surr)29 -120
Surrogate
59
MSD MSD
Qualifier Limits%Recovery
572-Fluorophenol (Surr)10 -120
70Nitrobenzene-d5 (Surr)27 -120
58Phenol-d5 (Surr)10 -120
64Terphenyl-d14 (Surr)13 -120
822,4,6-Tribromophenol (Surr)10 -120
Method: 7199 - Chromium, Hexavalent (IC)
Client Sample ID: Method BlankLab Sample ID: MB 440-299047/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 299159 Prep Batch: 299047
RL MDL
Cr (VI)ND 0.299 mg/Kg 12/08/15 14:45 12/09/15 19:11 3
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 440-299047/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 299159 Prep Batch: 299047
Cr (VI)39.7 38.75 mg/Kg 98 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 440-129898-A-2-I MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 299159 Prep Batch: 299047
Cr (VI)ND 39.4 38.07 mg/Kg 97 55-110
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 440-129898-A-2-J MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 299159 Prep Batch: 299047
Cr (VI)ND 40.2 38.63 mg/Kg 96 55-110 1 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Matrix SpikeLab Sample ID: 440-129898-A-2-K MSI
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 299159 Prep Batch: 299047
Cr (VI)ND 868 615.9 mg/Kg 71 55-110
Analyte
MSI MSI
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
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QC Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Method: 7199 - Chromium, Hexavalent (IC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: MRL 440-299159/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 299159
Cr (VI)1.00 ND ug/L 126
Analyte
MRL MRL
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control SampleLab Sample ID: MRL 440-299399/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 299399
Cr (VI)1.00 ND ug/L 110
Analyte
MRL MRL
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Method: 6010C - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-304342/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304594 Prep Batch: 304342
RL MDL
Antimony ND 9.58 mg/Kg 12/07/15 08:40 12/07/15 14:37 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.92 mg/Kg 12/07/15 08:40 12/07/15 14:37 1Arsenic
ND 0.958 mg/Kg 12/07/15 08:40 12/07/15 14:37 1Beryllium
ND 0.958 mg/Kg 12/07/15 08:40 12/07/15 14:37 1Cadmium
ND 0.958 mg/Kg 12/07/15 08:40 12/07/15 14:37 1Chromium
ND 1.92 mg/Kg 12/07/15 08:40 12/07/15 14:37 1Copper
ND 0.958 mg/Kg 12/07/15 08:40 12/07/15 14:37 1Lead
ND 2.87 mg/Kg 12/07/15 08:40 12/07/15 14:37 1Manganese
ND 1.92 mg/Kg 12/07/15 08:40 12/07/15 14:37 1Nickel
ND 1.92 mg/Kg 12/07/15 08:40 12/07/15 14:37 1Selenium
ND 0.958 mg/Kg 12/07/15 08:40 12/07/15 14:37 1Silver
ND 1.92 mg/Kg 12/07/15 08:40 12/07/15 14:37 1Thallium
ND 9.58 mg/Kg 12/07/15 08:40 12/07/15 14:37 1Zinc
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-304342/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304594 Prep Batch: 304342
Antimony 39.8 39.88 mg/Kg 100 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 19.9 18.96 mg/Kg 95 80-120
Beryllium 19.9 20.46 mg/Kg 103 80-120
Cadmium 19.9 19.84 mg/Kg 100 80-120
Chromium 79.7 81.61 mg/Kg 102 80-120
Copper 99.6 99.32 mg/Kg 100 80-120
Lead 19.9 20.36 mg/Kg 102 80-120
Manganese 199 198.9 mg/Kg 100 80-120
Nickel 199 196.7 mg/Kg 99 80-120
Selenium 19.9 18.84 mg/Kg 95 80-120
Silver 19.9 20.46 mg/Kg 103 80-120
Thallium 120 121.7 mg/Kg 102 80-120
Zinc 199 194.0 mg/Kg 97 80-120
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QC Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Method: 6010C - Metals (ICP) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-304342/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304594 Prep Batch: 304342
Antimony 39.6 38.63 mg/Kg 98 80-120 3 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Arsenic 19.8 18.55 mg/Kg 94 80-120 2 20
Beryllium 19.8 20.14 mg/Kg 102 80-120 2 20
Cadmium 19.8 19.45 mg/Kg 98 80-120 2 20
Chromium 79.2 79.60 mg/Kg 100 80-120 2 20
Copper 99.0 96.85 mg/Kg 98 80-120 3 20
Lead 19.8 19.88 mg/Kg 100 80-120 2 20
Manganese 198 194.8 mg/Kg 98 80-120 2 20
Nickel 198 192.5 mg/Kg 97 80-120 2 20
Selenium 19.8 18.18 mg/Kg 92 80-120 4 20
Silver 19.8 19.88 mg/Kg 100 80-120 3 20
Thallium 119 115.9 mg/Kg 98 80-120 5 20
Zinc 198 188.5 mg/Kg 95 80-120 3 20
Client Sample ID: SB-14(0-2)Lab Sample ID: 490-93258-3 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304594 Prep Batch: 304342
Antimony ND F2 F1 50.8 46.61 mg/Kg 92 75-125☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic 4.53 25.4 25.40 mg/Kg 82 75-125☼
Beryllium ND 25.4 24.15 mg/Kg 94 75-125☼
Cadmium ND 25.4 23.65 mg/Kg 90 75-125☼
Chromium 41.5 102 126.6 mg/Kg 84 75-125☼
Copper 66.9 127 167.7 mg/Kg 79 75-125☼
Lead 38.3 F1 25.4 47.19 F1 mg/Kg 35 75-125☼
Manganese 599 F1 254 693.1 F1 mg/Kg 37 75-125☼
Nickel 30.1 254 247.7 mg/Kg 86 75-125☼
Selenium ND 25.4 22.25 mg/Kg 88 75-125☼
Silver ND F2 F1 25.4 25.02 mg/Kg 99 75-125☼
Thallium ND 152 137.1 mg/Kg 90 75-125☼
Zinc 103 254 300.2 mg/Kg 78 75-125☼
Client Sample ID: SB-14(0-2)Lab Sample ID: 490-93258-3 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304594 Prep Batch: 304342
Antimony ND F2 F1 49.8 ND F1 F2 mg/Kg 15 75-125 144 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Arsenic 4.53 24.9 24.80 mg/Kg 81 75-125 2 20☼
Beryllium ND 24.9 23.41 mg/Kg 93 75-125 3 20☼
Cadmium ND 24.9 23.16 mg/Kg 89 75-125 2 20☼
Chromium 41.5 99.6 125.4 mg/Kg 84 75-125 1 20☼
Copper 66.9 125 181.8 mg/Kg 92 75-125 8 20☼
Lead 38.3 F1 24.9 57.53 mg/Kg 77 75-125 20 20☼
Manganese 599 F1 249 739.6 F1 mg/Kg 57 75-125 6 20☼
Nickel 30.1 249 247.9 mg/Kg 87 75-125 0 20☼
Selenium ND 24.9 21.24 mg/Kg 85 75-125 5 20☼
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QC Sample Results
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Method: 6010C - Metals (ICP) (Continued)
Client Sample ID: SB-14(0-2)Lab Sample ID: 490-93258-3 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304594 Prep Batch: 304342
Silver ND F2 F1 24.9 18.18 F1 F2 mg/Kg 73 75-125 32 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Thallium ND 149 135.4 mg/Kg 91 75-125 1 20☼
Zinc 103 249 322.0 mg/Kg 88 75-125 7 20☼
Method: 7471B - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-304510/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304583 Prep Batch: 304510
RL MDL
Mercury ND 0.100 mg/Kg 12/07/15 15:28 12/07/15 21:26 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-304510/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304583 Prep Batch: 304510
Mercury 0.163 0.1505 mg/Kg 92 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 310-70253-D-1-D MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304583 Prep Batch: 304510
Mercury ND 0.167 0.1765 mg/Kg 106 80-120
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 310-70253-D-1-E MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304583 Prep Batch: 304510
Mercury ND 0.161 0.1780 mg/Kg 111 80-120 1 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: Moisture - Percent Moisture
Client Sample ID: SB-19(0-2)Lab Sample ID: 490-93258-8 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 304033
Percent Solids 83 83 %0.1 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Percent Solids 83 83 %0.1 20
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QC Association Summary
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
GC/MS VOA
Prep Batch: 304079
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035490-93258-1 UST-N(0-2)Total/NA
Solid 5035490-93258-2 UST-Base(11-13)Total/NA
Solid 5035490-93258-3 SB-14(0-2)Total/NA
Analysis Batch: 304578
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260B 304079490-93258-1 UST-N(0-2)Total/NA
Solid 8260B 304079490-93258-2 UST-Base(11-13)Total/NA
Solid 8260B 304079490-93258-3 SB-14(0-2)Total/NA
Solid 8260BLCS 490-304578/4 Lab Control Sample Total/NA
Solid 8260BLCSD 490-304578/5 Lab Control Sample Dup Total/NA
Solid 8260BMB 490-304578/7 Method Blank Total/NA
GC/MS Semi VOA
Prep Batch: 304385
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3550C490-93258-1 UST-N(0-2)Total/NA
Solid 3550C490-93258-2 UST-Base(11-13)Total/NA
Solid 3550C490-93258-3 SB-14(0-2)Total/NA
Solid 3550C490-93371-B-8-G MS Matrix Spike Total/NA
Solid 3550C490-93371-B-8-H MSD Matrix Spike Duplicate Total/NA
Solid 3550CLCS 490-304385/2-A Lab Control Sample Total/NA
Solid 3550CLCSD 490-304385/3-A Lab Control Sample Dup Total/NA
Solid 3550CMB 490-304385/1-A Method Blank Total/NA
Analysis Batch: 304472
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270D 304385490-93258-1 UST-N(0-2)Total/NA
Solid 8270D 304385490-93371-B-8-G MS Matrix Spike Total/NA
Solid 8270D 304385490-93371-B-8-H MSD Matrix Spike Duplicate Total/NA
Solid 8270D 304385LCS 490-304385/2-A Lab Control Sample Total/NA
Solid 8270D 304385LCSD 490-304385/3-A Lab Control Sample Dup Total/NA
Solid 8270D 304385MB 490-304385/1-A Method Blank Total/NA
Analysis Batch: 304706
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270D 304385490-93258-2 UST-Base(11-13)Total/NA
Solid 8270D 304385490-93258-3 SB-14(0-2)Total/NA
HPLC/IC
Prep Batch: 299047
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3060A440-129898-A-2-I MS Matrix Spike Total/NA
Solid 3060A440-129898-A-2-J MSD Matrix Spike Duplicate Total/NA
Solid 3060A440-129898-A-2-K MSI Matrix Spike Total/NA
Solid 3060A490-93258-3 SB-14(0-2)Total/NA
Solid 3060A490-93258-4 SB-15(0-2)Total/NA
Solid 3060A490-93258-5 SB-16(0-2)Total/NA
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QC Association Summary
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
HPLC/IC (Continued)
Prep Batch: 299047 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3060A490-93258-6 SB-17(0-2)Total/NA
Solid 3060A490-93258-7 SB-18(0-2)Total/NA
Solid 3060A490-93258-8 SB-19(0-2)Total/NA
Solid 3060ALCS 440-299047/2-A Lab Control Sample Total/NA
Solid 3060AMB 440-299047/1-A Method Blank Total/NA
Analysis Batch: 299159
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7199 299047440-129898-A-2-I MS Matrix Spike Total/NA
Solid 7199 299047440-129898-A-2-J MSD Matrix Spike Duplicate Total/NA
Solid 7199 299047440-129898-A-2-K MSI Matrix Spike Total/NA
Solid 7199 299047490-93258-3 SB-14(0-2)Total/NA
Solid 7199 299047490-93258-4 SB-15(0-2)Total/NA
Solid 7199 299047490-93258-5 SB-16(0-2)Total/NA
Solid 7199 299047490-93258-6 SB-17(0-2)Total/NA
Solid 7199 299047490-93258-7 SB-18(0-2)Total/NA
Solid 7199 299047490-93258-8 SB-19(0-2)Total/NA
Solid 7199 299047LCS 440-299047/2-A Lab Control Sample Total/NA
Solid 7199 299047MB 440-299047/1-A Method Blank Total/NA
Solid 7199MRL 440-299159/4 Lab Control Sample Total/NA
Analysis Batch: 299399
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7199MRL 440-299399/5 Lab Control Sample Total/NA
Metals
Prep Batch: 304342
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3051A490-93258-3 SB-14(0-2)Total/NA
Solid 3051A490-93258-3 MS SB-14(0-2)Total/NA
Solid 3051A490-93258-3 MSD SB-14(0-2)Total/NA
Solid 3051A490-93258-4 SB-15(0-2)Total/NA
Solid 3051A490-93258-5 SB-16(0-2)Total/NA
Solid 3051A490-93258-6 SB-17(0-2)Total/NA
Solid 3051A490-93258-7 SB-18(0-2)Total/NA
Solid 3051A490-93258-8 SB-19(0-2)Total/NA
Solid 3051ALCS 490-304342/2-A Lab Control Sample Total/NA
Solid 3051ALCSD 490-304342/3-A Lab Control Sample Dup Total/NA
Solid 3051AMB 490-304342/1-A Method Blank Total/NA
Prep Batch: 304510
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471B310-70253-D-1-D MS Matrix Spike Total/NA
Solid 7471B310-70253-D-1-E MSD Matrix Spike Duplicate Total/NA
Solid 7471B490-93258-3 SB-14(0-2)Total/NA
Solid 7471B490-93258-4 SB-15(0-2)Total/NA
Solid 7471B490-93258-5 SB-16(0-2)Total/NA
Solid 7471B490-93258-6 SB-17(0-2)Total/NA
Solid 7471B490-93258-7 SB-18(0-2)Total/NA
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QC Association Summary
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Metals (Continued)
Prep Batch: 304510 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471B490-93258-8 SB-19(0-2)Total/NA
Solid 7471BLCS 490-304510/2-A Lab Control Sample Total/NA
Solid 7471BMB 490-304510/1-A Method Blank Total/NA
Analysis Batch: 304583
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471B 304510310-70253-D-1-D MS Matrix Spike Total/NA
Solid 7471B 304510310-70253-D-1-E MSD Matrix Spike Duplicate Total/NA
Solid 7471B 304510490-93258-3 SB-14(0-2)Total/NA
Solid 7471B 304510490-93258-4 SB-15(0-2)Total/NA
Solid 7471B 304510490-93258-5 SB-16(0-2)Total/NA
Solid 7471B 304510490-93258-6 SB-17(0-2)Total/NA
Solid 7471B 304510490-93258-7 SB-18(0-2)Total/NA
Solid 7471B 304510490-93258-8 SB-19(0-2)Total/NA
Solid 7471B 304510LCS 490-304510/2-A Lab Control Sample Total/NA
Solid 7471B 304510MB 490-304510/1-A Method Blank Total/NA
Analysis Batch: 304594
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010C 304342490-93258-3 SB-14(0-2)Total/NA
Solid 6010C 304342490-93258-3 MS SB-14(0-2)Total/NA
Solid 6010C 304342490-93258-3 MSD SB-14(0-2)Total/NA
Solid 6010C 304342490-93258-4 SB-15(0-2)Total/NA
Solid 6010C 304342490-93258-5 SB-16(0-2)Total/NA
Solid 6010C 304342490-93258-6 SB-17(0-2)Total/NA
Solid 6010C 304342490-93258-7 SB-18(0-2)Total/NA
Solid 6010C 304342490-93258-8 SB-19(0-2)Total/NA
Solid 6010C 304342LCS 490-304342/2-A Lab Control Sample Total/NA
Solid 6010C 304342LCSD 490-304342/3-A Lab Control Sample Dup Total/NA
Solid 6010C 304342MB 490-304342/1-A Method Blank Total/NA
General Chemistry
Analysis Batch: 304033
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture490-93258-1 UST-N(0-2)Total/NA
Solid Moisture490-93258-2 UST-Base(11-13)Total/NA
Solid Moisture490-93258-3 SB-14(0-2)Total/NA
Solid Moisture490-93258-4 SB-15(0-2)Total/NA
Solid Moisture490-93258-5 SB-16(0-2)Total/NA
Solid Moisture490-93258-6 SB-17(0-2)Total/NA
Solid Moisture490-93258-7 SB-18(0-2)Total/NA
Solid Moisture490-93258-8 SB-19(0-2)Total/NA
Solid Moisture490-93258-8 DU SB-19(0-2)Total/NA
Solid Moisture490-93259-G-1 MS Matrix Spike Total/NA
Solid Moisture490-93259-G-1 MSD Matrix Spike Duplicate Total/NA
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-93258-1
Project/Site: Precision Dynamics-NC SDG: CHP-002
Client Sample ID: UST-N(0-2)Lab Sample ID: 490-93258-1
Matrix: SolidDate Collected: 11/30/15 14:00
Date Received: 12/04/15 09:05
Prep 5035 JLP11/30/15 14:00 TAL NSH304079
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.797 g 5.0 mL
Analysis 8260B 1 304578 12/08/15 04:43 EML TAL NSHTotal/NA 6.797 g 5.0 mL
Prep 3550C 304385 12/07/15 14:20 LOJ TAL NSHTotal/NA 39.54 g 1.00 mL
Analysis 8270D 1 304472 12/08/15 01:52 WDS TAL NSHTotal/NA 39.54 g 1.00 mL
Analysis Moisture 1 304033 12/04/15 13:12 MNM TAL NSHTotal/NA
Client Sample ID: UST-Base(11-13)Lab Sample ID: 490-93258-2
Matrix: SolidDate Collected: 11/30/15 14:30
Date Received: 12/04/15 09:05
Prep 5035 JLP11/30/15 14:30 TAL NSH304079
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.642 g 5.0 mL
Analysis 8260B 1 304578 12/08/15 04:12 EML TAL NSHTotal/NA 5.642 g 5.0 mL
Prep 3550C 304385 12/07/15 14:20 LOJ TAL NSHTotal/NA 39.63 g 1.00 mL
Analysis 8270D 1 304706 12/08/15 15:34 WDS TAL NSHTotal/NA 39.63 g 1.00 mL
Analysis Moisture 1 304033 12/04/15 13:12 MNM TAL NSHTotal/NA
Client Sample ID: SB-14(0-2)Lab Sample ID: 490-93258-3
Matrix: SolidDate Collected: 12/01/15 16:00
Date Received: 12/04/15 09:05
Prep 5035 JLP12/01/15 16:00 TAL NSH304079
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.628 g 5.0 mL
Analysis 8260B 1 304578 12/08/15 03:41 EML TAL NSHTotal/NA 6.628 g 5.0 mL
Prep 3550C 304385 12/07/15 14:20 LOJ TAL NSHTotal/NA 38.53 g 1.00 mL
Analysis 8270D 2 304706 12/08/15 15:58 WDS TAL NSHTotal/NA 38.53 g 1.00 mL
Prep 3060A 299047 12/08/15 14:45 TMB TAL IRVTotal/NA 2.48 g 100 mL
Analysis 7199 10 299159 12/10/15 00:00 RW TAL IRVTotal/NA 2.48 g 100 mL
Prep 3051A 304342 12/07/15 08:40 KMS TAL NSHTotal/NA 0.502 g 100 mL
Analysis 6010C 1 304594 12/07/15 16:02 NJB TAL NSHTotal/NA 0.502 g 100 mL
Prep 7471B 304510 12/07/15 15:28 BLG TAL NSHTotal/NA 0.622 g 100 mL
Analysis 7471B 1 304583 12/07/15 21:48 RDF TAL NSHTotal/NA 0.622 g 100 mL
Analysis Moisture 1 304033 12/04/15 13:12 MNM TAL NSHTotal/NA
Client Sample ID: SB-15(0-2)Lab Sample ID: 490-93258-4
Matrix: SolidDate Collected: 12/01/15 16:15
Date Received: 12/04/15 09:05
Prep 3060A TMB12/08/15 14:45 TAL IRV299047
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 2.48 g 100 mL
Analysis 7199 3 299159 12/10/15 00:13 RW TAL IRVTotal/NA 2.48 g 100 mL
Prep 3051A 304342 12/07/15 08:40 KMS TAL NSHTotal/NA 0.525 g 100 mL
Analysis 6010C 1 304594 12/07/15 16:32 NJB TAL NSHTotal/NA 0.525 g 100 mL
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-93258-1
Project/Site: Precision Dynamics-NC SDG: CHP-002
Prep 7471B BLG12/07/15 15:28 TAL NSH304510
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 0.598 g 100 mL
Analysis 7471B 1 304583 12/07/15 21:50 RDF TAL NSHTotal/NA 0.598 g 100 mL
Analysis Moisture 1 304033 12/04/15 13:12 MNM TAL NSHTotal/NA
Client Sample ID: SB-16(0-2)Lab Sample ID: 490-93258-5
Matrix: SolidDate Collected: 12/01/15 16:30
Date Received: 12/04/15 09:05
Prep 3060A TMB12/08/15 14:45 TAL IRV299047
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 2.54 g 100 mL
Analysis 7199 3 299159 12/10/15 00:25 RW TAL IRVTotal/NA 2.54 g 100 mL
Prep 3051A 304342 12/07/15 08:40 KMS TAL NSHTotal/NA 0.525 g 100 mL
Analysis 6010C 1 304594 12/07/15 16:36 NJB TAL NSHTotal/NA 0.525 g 100 mL
Prep 7471B 304510 12/07/15 15:28 BLG TAL NSHTotal/NA 0.600 g 100 mL
Analysis 7471B 1 304583 12/07/15 21:53 RDF TAL NSHTotal/NA 0.600 g 100 mL
Analysis Moisture 1 304033 12/04/15 13:12 MNM TAL NSHTotal/NA
Client Sample ID: SB-17(0-2)Lab Sample ID: 490-93258-6
Matrix: SolidDate Collected: 12/01/15 16:45
Date Received: 12/04/15 09:05
Prep 3060A TMB12/08/15 14:45 TAL IRV299047
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 2.51 g 100 mL
Analysis 7199 3 299159 12/10/15 00:38 RW TAL IRVTotal/NA 2.51 g 100 mL
Prep 3051A 304342 12/07/15 08:40 KMS TAL NSHTotal/NA 0.505 g 100 mL
Analysis 6010C 1 304594 12/07/15 16:40 NJB TAL NSHTotal/NA 0.505 g 100 mL
Prep 7471B 304510 12/07/15 15:28 BLG TAL NSHTotal/NA 0.598 g 100 mL
Analysis 7471B 1 304583 12/07/15 21:56 RDF TAL NSHTotal/NA 0.598 g 100 mL
Analysis Moisture 1 304033 12/04/15 13:12 MNM TAL NSHTotal/NA
Client Sample ID: SB-18(0-2)Lab Sample ID: 490-93258-7
Matrix: SolidDate Collected: 12/01/15 17:00
Date Received: 12/04/15 09:05
Prep 3060A TMB12/08/15 14:45 TAL IRV299047
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 2.48 g 100 mL
Analysis 7199 3 299159 12/10/15 00:50 RW TAL IRVTotal/NA 2.48 g 100 mL
Prep 3051A 304342 12/07/15 08:40 KMS TAL NSHTotal/NA 0.499 g 100 mL
Analysis 6010C 1 304594 12/07/15 16:44 NJB TAL NSHTotal/NA 0.499 g 100 mL
Prep 7471B 304510 12/07/15 15:28 BLG TAL NSHTotal/NA 0.595 g 100 mL
Analysis 7471B 1 304583 12/07/15 21:59 RDF TAL NSHTotal/NA 0.595 g 100 mL
Analysis Moisture 1 304033 12/04/15 13:12 MNM TAL NSHTotal/NA
TestAmerica Nashville
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-93258-1
Project/Site: Precision Dynamics-NC SDG: CHP-002
Client Sample ID: SB-19(0-2)Lab Sample ID: 490-93258-8
Matrix: SolidDate Collected: 12/01/15 17:15
Date Received: 12/04/15 09:05
Prep 3060A TMB12/08/15 14:45 TAL IRV299047
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 2.52 g 100 mL
Analysis 7199 3 299159 12/10/15 01:03 RW TAL IRVTotal/NA 2.52 g 100 mL
Prep 3051A 304342 12/07/15 08:40 KMS TAL NSHTotal/NA 0.497 g 100 mL
Analysis 6010C 1 304594 12/07/15 16:48 NJB TAL NSHTotal/NA 0.497 g 100 mL
Prep 7471B 304510 12/07/15 15:28 BLG TAL NSHTotal/NA 0.595 g 100 mL
Analysis 7471B 1 304583 12/07/15 22:01 RDF TAL NSHTotal/NA 0.595 g 100 mL
Analysis Moisture 1 304033 12/04/15 13:12 MNM TAL NSHTotal/NA
Laboratory References:
TAL IRV = TestAmerica Irvine, 17461 Derian Ave, Suite 100, Irvine, CA 92614-5817, TEL [phone]
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Method Summary
TestAmerica Job ID: 490-93258-1Client: Hart & Hickman, PC
SDG: CHP-002Project/Site: Precision Dynamics-NC
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8468270DSemivolatile Organic Compounds (GC/MS)TAL NSH
SW8467199Chromium, Hexavalent (IC)TAL IRV
SW8466010CMetals (ICP)TAL NSH
SW8467471BMercury (CVAA)TAL NSH
EPAMoisturePercent Moisture TAL NSH
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL IRV = TestAmerica Irvine, 17461 Derian Ave, Suite 100, Irvine, CA 92614-5817, TEL [phone]
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Certification Summary
Client: Hart & Hickman, PC TestAmerica Job ID: 490-93258-1
Project/Site: Precision Dynamics-NC SDG: CHP-002
Laboratory: TestAmerica Nashville
Unless otherwise noted, all analytes for this laboratory were covered under each certification below.
Authority Program EPA Region Certification ID Expiration Date
North Carolina (WW/SW)3874State Program 12-31-16
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but certification is not offered by the governing authority:
6010C 3051A Solid Antimony
6010C 3051A Solid Arsenic
6010C 3051A Solid Beryllium
6010C 3051A Solid Cadmium
6010C 3051A Solid Chromium
6010C 3051A Solid Copper
6010C 3051A Solid Lead
6010C 3051A Solid Manganese
6010C 3051A Solid Nickel
6010C 3051A Solid Selenium
6010C 3051A Solid Silver
6010C 3051A Solid Thallium
6010C 3051A Solid Zinc
Moisture Solid Percent Solids
Laboratory: TestAmerica Irvine
All certifications held by this laboratory are listed. Not all certifications are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
Alaska CA0153110State Program 06-30-16
Arizona State Program 9 AZ0671 10-13-16
California LA Cty Sanitation Districts 9 10256 01-31-16 *
California State Program 9 2706 06-30-16
Guam State Program 9 Cert. No. 12.002r 01-23-16
Hawaii State Program 9 N/A 01-29-16
Kansas NELAP Secondary AB 7 E-10420 07-31-16
New Mexico State Program 6 N/A 01-29-16
Northern Mariana Islands State Program 9 MP0002 01-29-16
Oregon NELAP 10 4005 01-29-16
USDA Federal P330-09-00080 07-08-18
TestAmerica Nashville
* Certification renewal pending - certification considered valid.
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Login Sample Receipt Checklist
Client: Hart & Hickman, PC Job Number: 490-93258-1
SDG Number: CHP-002
Login Number: 93258
Question Answer Comment
Creator: Vest, Laura E
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.1.2
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Nashville
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