25035_National Welders Supply Annual Redevelopment Report_20240131

Via Email
January 31, 2023
NCDEQ – Division of Waste Management
Brownfields Program
1646 Mail Service Center Raleigh, North Carolina 27699-1646 Attn: Mr. Bill Schmithorst, PG

Re: Annual Redevelopment Summary Report National Welders Supply Gesco Street and State Street
Charlotte, North Carolina
Brownfields Project No. 25035-21-060 H&H Project No. RMR-013
Dear Bill:
1.0 Introduction
On behalf of RRPVI Gesco Charlotte LP (Prospective Developer or PD), Hart & Hickman, PC
(H&H) has prepared this report to summarize environment-related activities associated with
redevelopment at the National Welders Supply Brownfields property (Brownfields Project No.
25035-21-060) located at Gesco Street and State Street in Charlotte, Mecklenburg County, North
Carolina (Site or subject Site). The Site consists of two adjacent parcels (Parcel Identification
Nos. 07108103 and 07107806) located in a rapidly densifying mixed-use area approximately one
mile northwest of uptown Charlotte.

Proposed redevelopment of the Brownfields property includes Site work and grading to level the
Site for the construction of two multi-story high-density apartment buildings with associated
amenity areas, access drives, and surface parking lots. A Site location map is provided as Figure
1, and the Site and surrounding area are shown in Figure 2.

Mr. Bill Schmithorst, PG January 31, 2023
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Pursuant to the North Carolina Department of Environmental Quality (DEQ) Brownfields
Program approved Environmental Management Plan (EMP) dated June 21, 2022, a report of
environment-related activities will be prepared each year for as long as physical redevelopment
of the Brownfields property continues. Redevelopment activities at the Site began in October
2022, and this report has been prepared in accordance with the DEQ-approved EMP for the Site.

A brief summary of annual redevelopment activities is provided in the following section.

2.0 Environmental-Related Redevelopment Activities

Redevelopment activities at the Site have been conducted in accordance with the DEQ-approved
EMP dated June 21, 2022. Redevelopment activities at the Site are ongoing and have included
Site wide grading, utility installation activities, and initial building foundation installation. Mass
grading activities resulted in a net export of soil which included the collection of in situ soil
samples for laboratory analysis to assist in the management of the excess soil. In addition,
during the initial building foundation construction, portions of the vapor intrusion mitigation
system (VIMS) were installed. Brief summaries of the soil export, in situ soil sampling
activities, and VIMS installation are provided below.

Initial Site Grading
Redevelopment activities completed at the Site since October 2022 have included surface
grubbing and mass grading activities. Initial grading plans and cut/fill analysis indicated that the
redevelopment would result in a net export of soil. Between October and December 2022,
approximately 4,500 cubic yards of soil generated during grading activities conducted at the Site
was exported to the Republic Services Subtitle D Landfill located in Concord, North Carolina.
The waste manifests documenting disposal of the export soil at Republic are provided in
Appendix A.

Please note, the export soil discussed above does not include the material generated during
remediation activities of the TCE impacted soil located in the northeastern part of the Site, on the
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western side of Gesco Street. The export manifests and a discussion of the remediation activities
will be documented in the Soil Excavation Report which will be submitted under separate cover.

In Situ Test Pit Soil Sampling Activities
As part of mass grading and utility installation at the Site, approximately 4,000 cubic yards of
soil which could not be re-used on Site was planned during excavations in the area of the main
stormwater utility and within select portions of the proposed building pads. The locations of the
planned excavations for installation of the stormwater utility are shown in Figure 2 as COMP-1
and TP-4. The areas of planned cut during grading for the proposed building pad in the southern
portion of the Site (west of Gesco Street) are shown in Figure 2 as COMP-2 and COMP-3.

Due to limited space on-Site for the management of large volumes of soil, H&H collected in situ
soil samples for laboratory analysis from the TP-4 and COMP-1 through COMP-3 evaluation
areas to evaluate the potential for impact in the areas planned for stormwater utility installation
and excavations to level the pad for construction of the proposed apartment buildings. The
grading contractor advanced test pits in each evaluation area using a track-mounted excavator on
September 29, 2022. As noted above, each evaluation area is shown in Figure 2, and H&H
collected aliquot soil samples from each evaluation area, as described below:

• Three test pits were advanced to approximately 8 feet below ground surface (ft bgs) in
the COMP-1 stormwater utility evaluation area located east of Gesco Street.

• Four test pits were advanced to approximately 8 ft bgs in the COMP-2 southern building
pad cut evaluation area.

• Three test pits were advanced to approximately 8 ft bgs in the COMP-3 southern building
pad cut evaluation area.

• One test pit was advanced to approximately 10 ft bgs in TP-4 stormwater utility
evaluation area located west of Gesco Street.

Mr. Bill Schmithorst, PG January 31, 2023
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One representative aliquot soil sample was collected from each test pit excavated in each
evaluation area described above. The aliquot soil samples collected from test pits excavated in
the COMP-1 through COMP-3 evaluation areas were combined and homogenized to form
composite soil samples representative of soil in each evaluation area for a total of three
composite soil samples. Because only one test pit was excavated in the TP-4 evaluation area, the
aliquot soil sample from this area was collected to be representative of soil conditions in the area
of the planned stormwater utility west of Gesco Street.

The soil samples selected for laboratory analysis were collected directly into laboratory supplied
glassware, labeled with the sample identification, date, time, and requested analyses and placed
in a laboratory supplied cooler with ice. The soil samples were submitted to Waypoint
Analytical under standard chain of custody protocols for analysis of semi-volatile organic
compounds (SVOCs) by EPA Method 8270 and RCRA metals plus hexavalent chromium by
EPA Methods 6020/7174/7199. Additionally, grab soil samples were collected from undisturbed
portions of aliquot soil samples collected from each evaluation area and submitted for laboratory
analysis of volatile organic compounds (VOCs) by EPA Method 8260.

A tabular summary of the soil sample laboratory analytical results is provided as Table 1, and a
copy of the laboratory analytical report and chain of custody record is included as Appendix B.
Analytical results were compared to the DEQ Protection of Groundwater, Residential, and
Industrial/Commercial Preliminary Soil Remediation Goals (PSRGs) dated July 2022. In
addition, metals data were compared to Reeves Land Clearing and Inert Debris (LCID) landfill
background metals as well as published regional background concentrations for naturally
occurring levels.

As shown in Table 1, trace concentrations of the organic compounds acetone, hexane, methyl
ethyl ketone, methylene chloride, and fluoranthene were detected above the laboratory method
detection limit in select soil samples. No other organic compounds were detected at
concentrations above the laboratory method detection limits and no organic compounds were
detected at concentrations exceeding the PSRGs in the test pit soil samples.
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As expected, several metals were detected at concentrations above the laboratory method
detection limits in the test pit soil samples. Hexavalent chromium was detected in COMP-1
(0.520 milligrams per kilogram {mg/kg}), COMP-2 (0.460 mg/kg), and TP-4 (0.332 mg/kg) at
concentrations slightly above the Residential PSRG of 0.31 mg/kg, but consistent with the high-
end range of hexavalent chromium concentrations detected at Reeves Landfill (0.43 J mg/kg). In
addition, arsenic (ranging from 0.859 mg/kg to 1.46 mg/kg) was detected in each soil sample at
concentrations above the Residential PSRG of 0.68 mg/kg, but at concentrations below the range
of background arsenic concentrations detected at Reeves Landfill (1.9 mg/kg to 3.0 mg/kg). The
remaining metals concentrations detected in the test pit soil samples are below the PRSGs and
are consistent with naturally occurring background levels.

Based on the results of the in situ test pit soil sampling activities, H&H requested DEQ
Brownfields Program approval to transport up to 4,000 cubic yards of soil from the TP-4 and
COMP-1 through COMP-3 evaluation areas to the Reeves LCID landfill facility in an email
dated October 27, 2022. DEQ Brownfields issued a Brownfields Soil Export approval letter
dated December 2, 2022. A copy of the DEQ approval letter is included in Appendix C.

In accordance with the approval letter, approximately 70 cubic yards of soil generated in the pre-
approved evaluation areas were exported to Reeves LCID landfill on December 5, 2022 and
December 13, 2022. Additional soil from the evaluation areas is planned for transport to the
Reeves facility as part of the development activities planned in 2023. Copies of the December
2022 trucking tickets for the soil export to Reeves are included in Appendix D.

Vapor Mitigation System Installation
As part of initial construction of the multifamily apartment buildings, select components of the
VIMS have been installed in accordance with the DEQ-approved Vapor Intrusion Mitigation
Plan (VIMP) dated December 7, 2022. H&H completed inspection activities during initial
phases of VIMS installation to confirm that the system is being installed in accordance with the
DEQ-approved VIMP. The inspections were completed by, or under direction of the VIMS
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design engineer and included vapor barrier installation within the elevator pits and foundations
within certain portions of the multifamily buildings. Results of VIMS installation inspections
completed to date indicate that the VIMS is being installed in accordance with the DEQ-
approved VIMP.
VIMS installation, inspection, and efficacy sampling details for the Site redevelopment will be
included in a VIMS installation completion report that will be submitted to the DEQ Brownfields
Program following construction completion and under separate cover.

In summary, redevelopment activities at the National Welders Supply Brownfields property are
ongoing and are being conducted in accordance with the DEQ approved EMP and the DEQ-
approved VIMP.

Should you have questions or need additional information, please do not hesitate to call us at
[phone].

Very truly yours,
Hart & Hickman, PC

Ralph McGee, PG Alexis McKenzie, PE
Project Manager Senior Project Engineer
Enclosures
cc: Mr. Quinn Augustine, Ram Realty Advisors (Via Email)
Ms. Karen Geller, Ram Realty Advisors (Via Email) Ms. Amanda Short, McGuire Woods (Via Email)
Mr. Bill Schmithorst, PG January 31, 2023
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Attachments:
Table 1 Summary of Soil Test Pit Analytical Data
Figure 1 Site Location Map Figure 2 Sample Location Map
Appendix A Republic Services Manifests
Appendix B Laboratory Analytical Report Appendix C Brownfields Soil Export Approval Letter Appendix D Reeves LCID Export Tickets

Table
Table 1Summary of Soil Test Pit Analytical Data National Welders Supply Charlotte, North CarolinaH&H Job No. RMR-013 Location Sample IDTP-4 BKG-R-01 BKG-R-02 BKG-R-03 BKG-R-04 BKG-R-05 Sample Date9/29/2022 7/28/2020 7/28/2020 7/28/2020 7/28/2020 7/28/2020 Sample TypeComposite Grab Composite Grab Composite Grab Grab Grab Grab Grab Grab Grab Depth (ft bgs)0-10 0-2 0-2 0-2 0-2 0-2 Range Mean UnitsVOCs (8260D)AcetoneNA0.068NA0.097NA0.110 0.049NA NA NA NA NA14,000 210,000 25-- --HexaneNA0.001 JNA<0.0008NA<0.0008 <0.0008 NA NA NA NA NA130 540 55-- --Methyl Ethyl KetoneNA0.006 JNA<0.0008NA0.012 J<0.0008 NA NA NA NA NA5,500 40,000 17-- --Methylene ChlorideNA0.002 JNA0.002 JNA0.002 J<0.001 NA NA NA NA NA58 650 0.025-- --SVOCs (8270E)Fluoranthene<0.153 NA <0.153 NA0.175 JNA <0.144 NA NA NA NA NA480 6,000 670-- --Metals (6020B/7471B/7199)Arsenic0.980NA0.859NA1.11NA1.46 3.0 1.9 2.6 2.21.90.68 3.0 5.81.0 - 18 4.8Barium68.2NA100NA86.6NA30.2 120 77 J 91 J 1301503,100 47,000 58050-1000 356Cadmium<0.0323NA<0.0323 NA0.0767 JNA <0.03050.13 J 0.075 J<0.0440.10 J<0.0471.4 20 3.01.0 - 10 4.3Chromium (Total)27.1NA28.5NA30.7NA31.8 58 36 46 47 58 NE NE NE7.0 - 300 65Hexavalent Chromium0.520NA0.460NA <0.164 NA0.332<0.240.28 J<0.240.43 J0.33 J0.31 6.5 3.8NS NSTrivalent Chromium26.6NA28.0NA30.7NA31.5 57.8 35.7 45.8 46.657.723,000 350,000 360,000NS NSLead7.87NA6.33NA11.1NA4.58 15 10 12 296.7400 800 NEND - 50 16Mercury0.0493NA0.0373 JNA0.0597NA0.0695 0.097 0.030 J 0.047 J 0.0700.055 J4.7 70 NE0.03 - 0.52 0.121Selenium0.440NA0.323NA0.479NA0.382 6.4 4.8 6.1 4.95.978 1,200 2.1<0.1 - 0.8 0.42Silver0.0288 J, BNA0.0245 J, BNA0.0433 J, BNA0.0243 J, B0.54 J<0.055<0.0610.11 J<0.065781,2003.4ND - 5.0 NSNotes:Compounds are reported to the laboratory method detection limit.With the exception of metals, only constituents detected in at least one sample are shown in the table above.Soil concentrations are reported in milligrams per kilogram (mg/kg).VOCs = volatile organic compounds; SVOCs = semi-VOCs; ft bgs = feet below ground surface-- = Not Applicable; NA = Not Analyzed; ND = not detected; NS = not specified; NE = not establishedJ = compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.B = compound was detected in laboratory associated blank.Protection of Groundwater PSRGs(1)0-8Regional Background Metals in Soil (2)Laboratory analytical methods are shown in parentheses.2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Drugan and Chekiri, 2005. Cd and Ag background concentrations are for Southeastern and Conterminous U.S. soils.mg/kgResidential PSRGs (1)Industrial/Commercial PSRGs (1)1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated July 2022.9/29/2022COMP-2COMP-30-8Reeves LCID LandfillNational Welders Supply Site0-89/29/2022COMP-19/29/2022https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Ram Realty - RMR/RMR-013 Gesco Street/Soil Export/Test Pit Summary Table1/19/2023Table 1 (Page 1 of 1)Hart & Hickman, PC

Figures
Copyright:© 2013 National Geographic Society, i-cubed
SITE LOCATION MAP
NATIONAL WELDERS SUPPLY GESCO STREET & STATE STREET CHARLOTTE, NORTH CAROLINA
DATE: 1-20-23
JOB NO: RMR-013
REVISION NO: 0
FIGURE NO: 1
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
TITLE
PROJECT
0 2,000 4,000
SCALE IN FEET
SITE
Path: S:\AAA-Master Projects\Ram Realty - RMR\RMR-013 Gesco Street\Figures\Figure-1.mxdN
U.S.G.S. QUADRANGLE MAP
CHARLOTTE EAST, NORTH CAROLINA 2013DERITA, NORTH CAROLINA 2013
QUADRANGLE7.5 MINUTE SERIES (TOPOGRAPHIC)
REVISION NO. 0
JOB NO. RMR-013
DATE: 1-19-23
FIGURE NO. 2
NATIONAL WELDERS SUPPLY
GESCO STREET & STATE STREET
CHARLOTTE, NORTH CAROLINA
SAMPLE LOCATION MAP
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL BOUNDARY
SURFACE WATER FEATURE
FORMER RAILROAD
APPROXIMATE EXPORT AREAS
CHARACTERIZED BY TEST PIT SOIL
SAMPLES
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
SOUTHERN CONCRETE
MATERIALS
(715 STATE STREET)
FORSHAW
(650 STATE STREET)
VACANT INDUSTRIAL BUILDING -
UNDER RENOVATION
(FORMER PLYLER PAPER STOCK CO.)
(800 GESCO STREET)STEWART CREEKSEVERSVILLE PARK
(830 S. BRUNS AVENUE)
NOTES:
1.AERIAL IMAGERY AND PARCEL DATA OBTAINED FROM
MECKLENBURG COUNTY GIS (2020).
DUKE ENERGY
RIGHT-OF-WAY
GESCO STREET
STATE STREET
PIPED STORMWATER
DRAINAGE
COMP-1
TP-4
COMP-3
COMP-2
S:\AAA-Master Projects\Ram Realty - RMR\RMR-013 Gesco Street\Figures\Site Map.dwg, FIG 2, 1/20/2023 2:56:35 PM, amckenzie

Appendix A Republic Services Manifests

Appendix B Laboratory Analytical Report

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

10/24/2022
Hart & Hickman (Charlotte) Alexis McKenzie
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 22-277-0037 Client Project Description: RMR-013
Dear Alexis McKenzie:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 10/4/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 61
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/28/202340750State ProgramAlabama
02/07/202388-0650State ProgramArkansas
06/30/20232904State ProgramCalifornia
06/30/2023E871157State Program - NELAPFlorida
02/18/2023C044State ProgramGeorgia
06/30/202304015State ProgramGeorgia
10/10/2023200078State Program - NELAPIllinois
06/30/202380215State ProgramKentucky
12/31/2022KY90047State ProgramKentucky
12/31/2022LA037State Program - NELAPLouisiana
06/30/202304015State Program - NELAPLouisiana
02/11/2023MSState ProgramMississippi
07/31/202347701State ProgramNorth Carolina
12/31/2022415State ProgramNorth Carolina
05/31/202368-03195State Program - NELAPPennsylvania
06/30/202284002State ProgramSouth Carolina
02/11/202302027State ProgramTennessee
09/30/2022T104704180State Program - NELAPTexas
06/30/202300106State ProgramVirginia
09/14/2023460181State Program - NELAPVirginia
Page 1 of 1 00016/22-277-0037
Page 2 of 61
Report Number:
Sample Summary Table
Client Project Description:
22-277-0037
RMR-013
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
09/29/2022 11:50Solids 89885 Comp-1 10/04/2022 15:42
09/29/2022 11:50Solids 89885 Comp-1 10/04/2022 15:42 6020B WP MTN -
09/29/2022 11:50Solids 89885 Comp-1 10/04/2022 15:42 SW-7199 WP MTN -
09/29/2022 12:00Solids 89886 Comp-2 10/04/2022 15:42
09/29/2022 12:00Solids 89886 Comp-2 10/04/2022 15:42 SW-7199 WP MTN -
09/29/2022 12:00Solids 89886 Comp-2 10/04/2022 15:42 6020B WP MTN -
09/29/2022 12:15Solids 89887 Comp-3 10/04/2022 15:42
09/29/2022 12:15Solids 89887 Comp-3 10/04/2022 15:42 SW-7199 WP MTN -
09/29/2022 12:15Solids 89887 Comp-3 10/04/2022 15:42 6020B WP MTN -
09/29/2022 12:45Solids 89888 TP-4 10/04/2022 15:42
09/29/2022 12:45Solids 89888 TP-4 10/04/2022 15:42 SW-7199 WP MTN -
09/29/2022 12:45Solids 89888 TP-4 10/04/2022 15:42 6020B WP MTN -
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 61
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-277-0037
Report Limit
Project:RMR-013
V 89885Comp-1
0.980 10/22/2022 01:276020BArsenicmg/Kg - dry 0.107
68.2 10/22/2022 01:276020BBariummg/Kg - dry 0.053
27.1 10/22/2022 01:276020BChromiummg/Kg - dry 0.144
7.87 10/22/2022 01:276020BLeadmg/Kg - dry 0.0387
0.440 10/22/2022 01:276020BSeleniummg/Kg - dry 0.128
JB0.0288 10/22/2022 01:276020BSilvermg/Kg - dry 0.0084
0.0493 10/19/2022 13:187471BMercury (Total)mg/Kg - dry 0.0150
0.068 10/05/2022 15:278260DAcetonemg/Kg - dry 0.002
J0.001 10/05/2022 15:278260Dn-Hexane mg/Kg - dry 0.0008
J0.006 10/05/2022 15:278260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
J0.002 10/05/2022 15:278260DMethylene Chloride mg/Kg - dry 0.001
0.520 10/11/2022 14:56SW-7199 Chromium, Hexavalent mg/Kg - dry 0.176
19.9 10/07/2022 09:53SW-DRYWT Moisture %
V 89886Comp-2
0.859 10/22/2022 01:336020BArsenicmg/Kg - dry 0.107
100 10/22/2022 01:336020BBariummg/Kg - dry 0.053
28.5 10/22/2022 01:336020BChromiummg/Kg - dry 0.144
6.33 10/22/2022 01:336020BLeadmg/Kg - dry 0.0387
0.323 10/22/2022 01:336020BSeleniummg/Kg - dry 0.128
JB0.0245 10/22/2022 01:336020BSilvermg/Kg - dry 0.0084
J0.0373 10/19/2022 13:207471BMercury (Total)mg/Kg - dry 0.0150
0.097 10/05/2022 15:548260DAcetonemg/Kg - dry 0.002
J0.002 10/05/2022 15:548260DMethylene Chloride mg/Kg - dry 0.001
0.460 10/11/2022 15:39SW-7199 Chromium, Hexavalent mg/Kg - dry 0.178
19.9 10/07/2022 09:53SW-DRYWT Moisture %
V 89887Comp-3
1.11 10/22/2022 01:386020BArsenicmg/Kg - dry 0.0995
86.6 10/22/2022 01:386020BBariummg/Kg - dry 0.049
J0.0767 10/22/2022 01:386020BCadmiummg/Kg - dry 0.0301
30.7 10/22/2022 01:386020BChromiummg/Kg - dry 0.135
11.1 10/22/2022 01:386020BLeadmg/Kg - dry 0.0360
0.479 10/22/2022 01:386020BSeleniummg/Kg - dry 0.119
JB0.0433 10/22/2022 01:386020BSilvermg/Kg - dry 0.0078
0.0597 10/19/2022 13:297471BMercury (Total)mg/Kg - dry 0.0140
0.110 10/05/2022 16:218260DAcetonemg/Kg - dry 0.002
J0.012 10/05/2022 16:218260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
Page 4 of 61
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-277-0037
Report Limit
Project:RMR-013
V 89887Comp-3
J0.002 10/05/2022 16:218260DMethylene Chloride mg/Kg - dry 0.001
J0.175 10/16/2022 21:378270EFluoranthenemg/Kg - dry 0.143
14.1 10/07/2022 09:53SW-DRYWT Moisture %
V 89888TP-4
1.46 10/22/2022 01:446020BArsenicmg/Kg - dry 0.101
30.2 10/22/2022 01:446020BBariummg/Kg - dry 0.050
31.8 10/22/2022 01:446020BChromiummg/Kg - dry 0.136
4.58 10/22/2022 01:446020BLeadmg/Kg - dry 0.0365
0.382 10/22/2022 01:446020BSeleniummg/Kg - dry 0.121
JB0.0243 10/22/2022 01:446020BSilvermg/Kg - dry 0.0079
0.0695 10/19/2022 13:317471BMercury (Total)mg/Kg - dry 0.0141
0.049 10/05/2022 16:488260DAcetonemg/Kg - dry 0.002
0.332 10/11/2022 16:01SW-7199 Chromium, Hexavalent mg/Kg - dry 0.166
15.1 10/07/2022 09:53SW-DRYWT Moisture %
Page 5 of 61

Client: Hart & Hickman (Charlotte) CASE NARRATIVE
Project: RMR-013 Lab Report Number: 22-277-0037
Date: 10/18/2022
Hexavalent Chromium by Ion Chromatography Method SW-7199 Sample 89885 (Comp-1) Analyte: Hexavalent Chromium
QC Batch No: L642479/L641944 MSD: Insoluble Hexavalent chromium spike data
Volatile Organic Compounds - GC/MS Method 8260D
Analyte: Bromomethane QC Batch No: V24741/V24740
CCV result is above control limits but within method parameters. Results are reported but considered estimated. Semivolatile Organic Compounds - GC/MS Method 8270E Sample 89827 (SB-2)
Analyte: 1,2-Dichlorobenzene QC Batch No: V25161/V24969
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Sample 89827 (SB-2) Analyte: 2,4-Dinitrophenol
QC Batch No: V25161/V24969 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Sample 89827 (SB-2)
Analyte: 2-Nitrophenol QC Batch No: V25161/V24969
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Sample 89827 (SB-2) Analyte: 4-Nitrophenol QC Batch No: V25161/V24969 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Sample 89827 (SB-2)
Analyte: Benzoic Acid QC Batch No: V25161/V24969 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Sample 89827 (SB-2)
Analyte: Hexachlorocyclopentadiene QC Batch No: V25161/V24969 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Sample 89827 (SB-2)
Page 6 of 61

Analyte: N-Nitrosodiphenylamine
QC Batch No: V25161/V24969 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference.

Page 7 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-1
89885 Matrix:
9/29/2022 11:50
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.9 %Moisture 1 10/07/22 09:53 SW-DRYWTAMB
0.520 mg/Kg - dry 0.176 0.250Chromium, Hexavalent 1 10/11/22 14:56 SW-7199SAR
0.980 mg/Kg - dry 0.107 0.312Arsenic 5 10/22/22 01:27 6020BBKN
68.2 mg/Kg - dry 0.053 0.312Barium 5 10/22/22 01:27 6020BBKN
<0.0323 mg/Kg - dry 0.0323 0.312Cadmium 5 10/22/22 01:27 6020BBKN
27.1 mg/Kg - dry 0.144 0.312
Chromium 5 10/22/22 01:27 6020BBKN
7.87 mg/Kg - dry 0.0387 0.312Lead 5 10/22/22 01:27 6020BBKN
0.0493 mg/Kg - dry 0.0150 0.0375Mercury (Total)1 10/19/22 13:18 7471BEDV
0.440 mg/Kg - dry 0.128 0.312Selenium 5 10/22/22 01:27 6020BBKN
0.0288 JB mg/Kg - dry 0.0084 0.312Silver 5 10/22/22 01:27 6020BBKN
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 8 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-1
89885 Matrix:
9/29/2022 11:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V24740 10/05/22 08:00
0.068 mg/Kg - dry 0.002 0.024Acetone 1 10/05/22 15:27 V24741TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 10/05/22 15:27 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 10/05/22 15:27 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 10/05/22 15:27 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 10/05/22 15:27 V24741TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 10/05/22 15:27 V24741TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 10/05/22 15:27 V24741TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 10/05/22 15:27 V24741TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 10/05/22 15:27 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 10/05/22 15:27 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 10/05/22 15:27 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 10/05/22 15:27 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 10/05/22 15:27 V24741TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 10/05/22 15:27 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 10/05/22 15:27 V24741TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 10/05/22 15:27 V24741TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 10/05/22 15:27 V24741TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 10/05/22 15:27 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 10/05/22 15:27 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 10/05/22 15:27 V24741TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 10/05/22 15:27 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 10/05/22 15:27 V24741TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 9 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-1
89885 Matrix:
9/29/2022 11:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V24740 10/05/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 10/05/22 15:27 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 10/05/22 15:27 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 10/05/22 15:27 V24741TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 10/05/22 15:27 V24741TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 10/05/22 15:27 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 10/05/22 15:27 V24741TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 10/05/22 15:27 V24741TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 10/05/22 15:27 V24741TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 10/05/22 15:27 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 10/05/22 15:27 V24741TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 10/05/22 15:27 V24741TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 10/05/22 15:27 V24741TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 10/05/22 15:27 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 10/05/22 15:27 V24741TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 10/05/22 15:27 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 10/05/22 15:27 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 10/05/22 15:27 V24741TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 10/05/22 15:27 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 10/05/22 15:27 V24741TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 10/05/22 15:27 V24741TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 10/05/22 15:27 V24741TBL
0.001 J mg/Kg - dry 0.0008 0.012n-Hexane 1 10/05/22 15:27 V24741TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 10 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-1
89885 Matrix:
9/29/2022 11:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V24740 10/05/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 10/05/22 15:27 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 10/05/22 15:27 V24741TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 10/05/22 15:27 V24741TBL
0.006 J mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 10/05/22 15:27 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 10/05/22 15:27 V24741TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 10/05/22 15:27 V24741TBL
0.002 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 10/05/22 15:27 V24741TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 10/05/22 15:27 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.006
n-Propylbenzene 1 10/05/22 15:27 V24741TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 10/05/22 15:27 V24741TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 10/05/22 15:27 V24741TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 10/05/22 15:27 V24741TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 10/05/22 15:27 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 10/05/22 15:27 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 10/05/22 15:27 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.012
1,2,4-Trichlorobenzene 1 10/05/22 15:27 V24741TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 10/05/22 15:27 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 10/05/22 15:27 V24741TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 10/05/22 15:27 V24741TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 10/05/22 15:27 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 10/05/22 15:27 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 10/05/22 15:27 V24741TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 11 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-1
89885 Matrix:
9/29/2022 11:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V24740 10/05/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 10/05/22 15:27 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 10/05/22 15:27 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 10/05/22 15:27 V24741TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 10/05/22 15:27 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 10/05/22 15:27 V24741
Surrogate: 4-Bromofluorobenzene 98.6 Limits: 70-130%10/05/22 15:271 TBL V24741
Surrogate: Dibromofluoromethane 101 Limits: 84-123%10/05/22 15:271 TBL V24741
Surrogate: Toluene-d8 96.3 Limits: 76-129%10/05/22 15:271 TBL V24741
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V24969 10/11/22 10:05
<0.144 mg/Kg - dry 0.144 0.825Acenaphthene 1 10/16/22 17:30 V25161JMV
<0.131 mg/Kg - dry 0.131 0.825Acenaphthylene 1 10/16/22 17:30 V25161JMV
<0.189 mg/Kg - dry 0.189 0.825Aniline 1 10/16/22 17:30 V25161JMV
<0.178 mg/Kg - dry 0.178 0.825Anthracene 1 10/16/22 17:30 V25161JMV
<0.173 mg/Kg - dry 0.173 0.825Benzo(a)anthracene 1 10/16/22 17:30 V25161JMV
<0.183 mg/Kg - dry 0.183 0.825Benzo(a)pyrene 1 10/16/22 17:30 V25161JMV
<0.182 mg/Kg - dry 0.182 0.825
Benzo(b)fluoranthene 1 10/16/22 17:30 V25161JMV
<0.169 mg/Kg - dry 0.169 0.825Benzo(g,h,i)perylene 1 10/16/22 17:30 V25161JMV
<0.171 mg/Kg - dry 0.171 0.825Benzo(k)fluoranthene 1 10/16/22 17:30 V25161JMV
<0.724 mg/Kg - dry 0.724 2.50Benzoic Acid 1 10/16/22 17:30 V25161JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 12 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-1
89885 Matrix:
9/29/2022 11:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V24969 10/11/22 10:05
<0.131 mg/Kg - dry 0.131 0.825Benzyl alcohol 1 10/16/22 17:30 V25161JMV
<0.147 mg/Kg - dry 0.147 0.825Bis(2-Chloroethoxy)methane 1 10/16/22 17:30 V25161JMV
<0.133 mg/Kg - dry 0.133 0.825Bis(2-Chloroethyl)ether 1 10/16/22 17:30 V25161JMV
<0.169 mg/Kg - dry 0.169 0.413Bis(2-Chloroisopropyl)ether 1 10/16/22 17:30 V25161JMV
<0.149 mg/Kg - dry 0.149 0.825Bis(2-ethylhexyl)phthalate 1 10/16/22 17:30 V25161JMV
<0.136 mg/Kg - dry 0.136 0.8254-Bromophenyl phenyl ether 1 10/16/22 17:30 V25161JMV
<0.141 mg/Kg - dry 0.141 0.413Butyl benzyl phthalate 1 10/16/22 17:30 V25161JMV
<0.115 mg/Kg - dry 0.115 0.8254-Chloro-3-methylphenol 1 10/16/22 17:30 V25161JMV
<0.139 mg/Kg - dry 0.139 0.413
4-Chloroaniline 1 10/16/22 17:30 V25161JMV
<0.144 mg/Kg - dry 0.144 0.8252-Chloronaphthalene 1 10/16/22 17:30 V25161JMV
<0.122 mg/Kg - dry 0.122 0.8252-Chlorophenol 1 10/16/22 17:30 V25161JMV
<0.157 mg/Kg - dry 0.157 1.254-Chlorophenyl phenyl ether 1 10/16/22 17:30 V25161JMV
<0.177 mg/Kg - dry 0.177 0.825Chrysene 1 10/16/22 17:30 V25161JMV
<0.287 mg/Kg - dry 0.287 0.825Dibenz(a,h)anthracene 1 10/16/22 17:30 V25161JMV
<0.148 mg/Kg - dry 0.148 0.825Dibenzofuran 1 10/16/22 17:30 V25161JMV
<0.117 mg/Kg - dry 0.117 0.825
1,2-Dichlorobenzene 1 10/16/22 17:30 V25161JMV
<0.121 mg/Kg - dry 0.121 0.8251,3-Dichlorobenzene 1 10/16/22 17:30 V25161JMV
<0.122 mg/Kg - dry 0.122 0.4131,4-Dichlorobenzene 1 10/16/22 17:30 V25161JMV
<0.183 mg/Kg - dry 0.183 0.8253,3'-Dichlorobenzidine 1 10/16/22 17:30 V25161JMV
<0.119 mg/Kg - dry 0.119 0.8252,4-Dichlorophenol 1 10/16/22 17:30 V25161JMV
<0.224 mg/Kg - dry 0.224 0.825Diethyl phthalate 1 10/16/22 17:30 V25161JMV
<0.217 mg/Kg - dry 0.217 0.825Dimethyl phthalate 1 10/16/22 17:30 V25161JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 13 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-1
89885 Matrix:
9/29/2022 11:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V24969 10/11/22 10:05
<0.134 mg/Kg - dry 0.134 0.4132,4-Dimethylphenol 1 10/16/22 17:30 V25161JMV
<0.133 mg/Kg - dry 0.133 0.825Di-n-butyl phthalate 1 10/16/22 17:30 V25161JMV
<0.299 mg/Kg - dry 0.299 1.874,6-Dinitro-2-methylphenol 1 10/16/22 17:30 V25161JMV
<0.649 mg/Kg - dry 0.649 1.872,4-Dinitrophenol 1 10/16/22 17:30 V25161JMV
<0.120 mg/Kg - dry 0.120 0.8252,4-Dinitrotoluene 1 10/16/22 17:30 V25161JMV
<0.134 mg/Kg - dry 0.134 0.8252,6-Dinitrotoluene 1 10/16/22 17:30 V25161JMV
<0.178 mg/Kg - dry 0.178 0.413Di-n-Octyl Phthalate 1 10/16/22 17:30 V25161JMV
<0.153 mg/Kg - dry 0.153 0.825Fluoranthene 1 10/16/22 17:30 V25161JMV
<0.159 mg/Kg - dry 0.159 0.825
Fluorene 1 10/16/22 17:30 V25161JMV
<0.132 mg/Kg - dry 0.132 0.825Hexachlorobenzene 1 10/16/22 17:30 V25161JMV
<0.121 mg/Kg - dry 0.121 0.825Hexachlorobutadiene 1 10/16/22 17:30 V25161JMV
<0.196 mg/Kg - dry 0.196 0.825Hexachlorocyclopentadiene 1 10/16/22 17:30 V25161JMV
<0.099 mg/Kg - dry 0.099 0.825Hexachloroethane 1 10/16/22 17:30 V25161JMV
<0.223 mg/Kg - dry 0.223 0.825Indeno(1,2,3-cd)pyrene 1 10/16/22 17:30 V25161JMV
<0.238 mg/Kg - dry 0.238 0.825Isophorone 1 10/16/22 17:30 V25161JMV
<0.132 mg/Kg - dry 0.132 0.825
1-Methylnaphthalene 1 10/16/22 17:30 V25161JMV
<0.124 mg/Kg - dry 0.124 0.8252-Methylnaphthalene 1 10/16/22 17:30 V25161JMV
<0.121 mg/Kg - dry 0.121 0.8252-Methylphenol 1 10/16/22 17:30 V25161JMV
<0.106 mg/Kg - dry 0.106 0.8253&4 Methylphenol 1 10/16/22 17:30 V25161JMV
<0.179 mg/Kg - dry 0.179 0.825Naphthalene 1 10/16/22 17:30 V25161JMV
<0.120 mg/Kg - dry 0.120 0.8252-Nitroaniline 1 10/16/22 17:30 V25161JMV
<0.149 mg/Kg - dry 0.149 0.8253-Nitroaniline 1 10/16/22 17:30 V25161JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 14 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-1
89885 Matrix:
9/29/2022 11:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V24969 10/11/22 10:05
<0.116 mg/Kg - dry 0.116 0.4134-Nitroaniline 1 10/16/22 17:30 V25161JMV
<0.144 mg/Kg - dry 0.144 0.413Nitrobenzene 1 10/16/22 17:30 V25161JMV
<0.110 mg/Kg - dry 0.110 0.8252-Nitrophenol 1 10/16/22 17:30 V25161JMV
<0.146 mg/Kg - dry 0.146 0.8254-Nitrophenol 1 10/16/22 17:30 V25161JMV
<0.328 mg/Kg - dry 0.328 0.825N-Nitrosodimethylamine 1 10/16/22 17:30 V25161JMV
<0.225 mg/Kg - dry 0.225 0.825N-Nitrosodiphenylamine 1 10/16/22 17:30 V25161JMV
<0.147 mg/Kg - dry 0.147 0.825N-Nitroso-di-n-propylamine 1 10/16/22 17:30 V25161JMV
<0.433 mg/Kg - dry 0.433 1.25Pentachlorophenol 1 10/16/22 17:30 V25161JMV
<0.259 mg/Kg - dry 0.259 0.825
Phenanthrene 1 10/16/22 17:30 V25161JMV
<0.139 mg/Kg - dry 0.139 0.825Phenol 1 10/16/22 17:30 V25161JMV
<0.167 mg/Kg - dry 0.167 0.825Pyrene 1 10/16/22 17:30 V25161JMV
<0.099 mg/Kg - dry 0.099 0.413Pyridine 1 10/16/22 17:30 V25161JMV
<0.133 mg/Kg - dry 0.133 0.8251,2,4-Trichlorobenzene 1 10/16/22 17:30 V25161JMV
<0.120 mg/Kg - dry 0.120 0.8252,4,5-Trichlorophenol 1 10/16/22 17:30 V25161JMV
<0.120 mg/Kg - dry 0.120 0.8252,4,6-Trichlorophenol 1 10/16/22 17:30 V25161JMV
8270ESurrogate: Phenol-d5 89.2 Limits: 34-121%10/16/22 17:301 JMV
Surrogate: 2-Fluorobiphenyl 97.6 Limits: 44-115%10/16/22 17:301 JMV V25161
Surrogate: 2-Fluorophenol 89.2 Limits: 35-115%10/16/22 17:301 JMV V25161
Surrogate: Nitrobenzene-d5 88.6 Limits: 37-122%10/16/22 17:301 JMV V25161
Surrogate: 4-Terphenyl-d14 102 Limits: 54-127%10/16/22 17:301 JMV V25161
Surrogate: 2,4,6-Tribromophenol 101 Limits: 39-132%10/16/22 17:301 JMV V25161
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 15 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-2
89886 Matrix:
9/29/2022 12:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.9 %Moisture 1 10/07/22 09:53 SW-DRYWTAMB
0.460 mg/Kg - dry 0.178 0.253Chromium, Hexavalent 1 10/11/22 15:39 SW-7199SAR
0.859 mg/Kg - dry 0.107 0.312Arsenic 5 10/22/22 01:33 6020BBKN
100 mg/Kg - dry 0.053 0.312Barium 5 10/22/22 01:33 6020BBKN
<0.0323 mg/Kg - dry 0.0323 0.312Cadmium 5 10/22/22 01:33 6020BBKN
28.5 mg/Kg - dry 0.144 0.312
Chromium 5 10/22/22 01:33 6020BBKN
6.33 mg/Kg - dry 0.0387 0.312Lead 5 10/22/22 01:33 6020BBKN
0.0373 J mg/Kg - dry 0.0150 0.0375Mercury (Total)1 10/19/22 13:20 7471BEDV
0.323 mg/Kg - dry 0.128 0.312Selenium 5 10/22/22 01:33 6020BBKN
0.0245 JB mg/Kg - dry 0.0084 0.312Silver 5 10/22/22 01:33 6020BBKN
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 16 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-2
89886 Matrix:
9/29/2022 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V24740 10/05/22 08:00
0.097 mg/Kg - dry 0.002 0.024Acetone 1 10/05/22 15:54 V24741TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 10/05/22 15:54 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 10/05/22 15:54 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 10/05/22 15:54 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 10/05/22 15:54 V24741TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 10/05/22 15:54 V24741TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 10/05/22 15:54 V24741TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 10/05/22 15:54 V24741TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 10/05/22 15:54 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 10/05/22 15:54 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 10/05/22 15:54 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 10/05/22 15:54 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 10/05/22 15:54 V24741TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 10/05/22 15:54 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 10/05/22 15:54 V24741TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 10/05/22 15:54 V24741TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 10/05/22 15:54 V24741TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 10/05/22 15:54 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 10/05/22 15:54 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 10/05/22 15:54 V24741TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 10/05/22 15:54 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 10/05/22 15:54 V24741TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 17 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-2
89886 Matrix:
9/29/2022 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V24740 10/05/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 10/05/22 15:54 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 10/05/22 15:54 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 10/05/22 15:54 V24741TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 10/05/22 15:54 V24741TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 10/05/22 15:54 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 10/05/22 15:54 V24741TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 10/05/22 15:54 V24741TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 10/05/22 15:54 V24741TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 10/05/22 15:54 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 10/05/22 15:54 V24741TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 10/05/22 15:54 V24741TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 10/05/22 15:54 V24741TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 10/05/22 15:54 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 10/05/22 15:54 V24741TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 10/05/22 15:54 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 10/05/22 15:54 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 10/05/22 15:54 V24741TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 10/05/22 15:54 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 10/05/22 15:54 V24741TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 10/05/22 15:54 V24741TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 10/05/22 15:54 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 10/05/22 15:54 V24741TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 18 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-2
89886 Matrix:
9/29/2022 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V24740 10/05/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 10/05/22 15:54 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 10/05/22 15:54 V24741TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 10/05/22 15:54 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 10/05/22 15:54 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 10/05/22 15:54 V24741TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 10/05/22 15:54 V24741TBL
0.002 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 10/05/22 15:54 V24741TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 10/05/22 15:54 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.006
n-Propylbenzene 1 10/05/22 15:54 V24741TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 10/05/22 15:54 V24741TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 10/05/22 15:54 V24741TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 10/05/22 15:54 V24741TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 10/05/22 15:54 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 10/05/22 15:54 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 10/05/22 15:54 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.012
1,2,4-Trichlorobenzene 1 10/05/22 15:54 V24741TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 10/05/22 15:54 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 10/05/22 15:54 V24741TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 10/05/22 15:54 V24741TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 10/05/22 15:54 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 10/05/22 15:54 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 10/05/22 15:54 V24741TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 19 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-2
89886 Matrix:
9/29/2022 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V24740 10/05/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 10/05/22 15:54 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 10/05/22 15:54 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 10/05/22 15:54 V24741TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 10/05/22 15:54 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 10/05/22 15:54 V24741
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%10/05/22 15:541 TBL V24741
Surrogate: Dibromofluoromethane 97.3 Limits: 84-123%10/05/22 15:541 TBL V24741
Surrogate: Toluene-d8 98.1 Limits: 76-129%10/05/22 15:541 TBL V24741
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V24969 10/11/22 10:05
<0.144 mg/Kg - dry 0.144 0.823Acenaphthene 1 10/16/22 17:52 V25161JMV
<0.131 mg/Kg - dry 0.131 0.823Acenaphthylene 1 10/16/22 17:52 V25161JMV
<0.189 mg/Kg - dry 0.189 0.823Aniline 1 10/16/22 17:52 V25161JMV
<0.178 mg/Kg - dry 0.178 0.823Anthracene 1 10/16/22 17:52 V25161JMV
<0.173 mg/Kg - dry 0.173 0.823Benzo(a)anthracene 1 10/16/22 17:52 V25161JMV
<0.183 mg/Kg - dry 0.183 0.823Benzo(a)pyrene 1 10/16/22 17:52 V25161JMV
<0.182 mg/Kg - dry 0.182 0.823
Benzo(b)fluoranthene 1 10/16/22 17:52 V25161JMV
<0.169 mg/Kg - dry 0.169 0.823Benzo(g,h,i)perylene 1 10/16/22 17:52 V25161JMV
<0.171 mg/Kg - dry 0.171 0.823Benzo(k)fluoranthene 1 10/16/22 17:52 V25161JMV
<0.724 mg/Kg - dry 0.724 2.50Benzoic Acid 1 10/16/22 17:52 V25161JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 20 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-2
89886 Matrix:
9/29/2022 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V24969 10/11/22 10:05
<0.131 mg/Kg - dry 0.131 0.823Benzyl alcohol 1 10/16/22 17:52 V25161JMV
<0.147 mg/Kg - dry 0.147 0.823Bis(2-Chloroethoxy)methane 1 10/16/22 17:52 V25161JMV
<0.133 mg/Kg - dry 0.133 0.823Bis(2-Chloroethyl)ether 1 10/16/22 17:52 V25161JMV
<0.169 mg/Kg - dry 0.169 0.411Bis(2-Chloroisopropyl)ether 1 10/16/22 17:52 V25161JMV
<0.149 mg/Kg - dry 0.149 0.823Bis(2-ethylhexyl)phthalate 1 10/16/22 17:52 V25161JMV
<0.136 mg/Kg - dry 0.136 0.8234-Bromophenyl phenyl ether 1 10/16/22 17:52 V25161JMV
<0.141 mg/Kg - dry 0.141 0.411Butyl benzyl phthalate 1 10/16/22 17:52 V25161JMV
<0.115 mg/Kg - dry 0.115 0.8234-Chloro-3-methylphenol 1 10/16/22 17:52 V25161JMV
<0.139 mg/Kg - dry 0.139 0.411
4-Chloroaniline 1 10/16/22 17:52 V25161JMV
<0.144 mg/Kg - dry 0.144 0.8232-Chloronaphthalene 1 10/16/22 17:52 V25161JMV
<0.122 mg/Kg - dry 0.122 0.8232-Chlorophenol 1 10/16/22 17:52 V25161JMV
<0.157 mg/Kg - dry 0.157 1.254-Chlorophenyl phenyl ether 1 10/16/22 17:52 V25161JMV
<0.177 mg/Kg - dry 0.177 0.823Chrysene 1 10/16/22 17:52 V25161JMV
<0.287 mg/Kg - dry 0.287 0.823Dibenz(a,h)anthracene 1 10/16/22 17:52 V25161JMV
<0.148 mg/Kg - dry 0.148 0.823Dibenzofuran 1 10/16/22 17:52 V25161JMV
<0.117 mg/Kg - dry 0.117 0.823
1,2-Dichlorobenzene 1 10/16/22 17:52 V25161JMV
<0.121 mg/Kg - dry 0.121 0.8231,3-Dichlorobenzene 1 10/16/22 17:52 V25161JMV
<0.121 mg/Kg - dry 0.121 0.4111,4-Dichlorobenzene 1 10/16/22 17:52 V25161JMV
<0.183 mg/Kg - dry 0.183 0.8233,3'-Dichlorobenzidine 1 10/16/22 17:52 V25161JMV
<0.119 mg/Kg - dry 0.119 0.8232,4-Dichlorophenol 1 10/16/22 17:52 V25161JMV
<0.224 mg/Kg - dry 0.224 0.823Diethyl phthalate 1 10/16/22 17:52 V25161JMV
<0.217 mg/Kg - dry 0.217 0.823Dimethyl phthalate 1 10/16/22 17:52 V25161JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 21 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-2
89886 Matrix:
9/29/2022 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V24969 10/11/22 10:05
<0.134 mg/Kg - dry 0.134 0.4112,4-Dimethylphenol 1 10/16/22 17:52 V25161JMV
<0.133 mg/Kg - dry 0.133 0.823Di-n-butyl phthalate 1 10/16/22 17:52 V25161JMV
<0.299 mg/Kg - dry 0.299 1.874,6-Dinitro-2-methylphenol 1 10/16/22 17:52 V25161JMV
<0.649 mg/Kg - dry 0.649 1.872,4-Dinitrophenol 1 10/16/22 17:52 V25161JMV
<0.120 mg/Kg - dry 0.120 0.8232,4-Dinitrotoluene 1 10/16/22 17:52 V25161JMV
<0.134 mg/Kg - dry 0.134 0.8232,6-Dinitrotoluene 1 10/16/22 17:52 V25161JMV
<0.178 mg/Kg - dry 0.178 0.411Di-n-Octyl Phthalate 1 10/16/22 17:52 V25161JMV
<0.153 mg/Kg - dry 0.153 0.823Fluoranthene 1 10/16/22 17:52 V25161JMV
<0.159 mg/Kg - dry 0.159 0.823
Fluorene 1 10/16/22 17:52 V25161JMV
<0.132 mg/Kg - dry 0.132 0.823Hexachlorobenzene 1 10/16/22 17:52 V25161JMV
<0.121 mg/Kg - dry 0.121 0.823Hexachlorobutadiene 1 10/16/22 17:52 V25161JMV
<0.196 mg/Kg - dry 0.196 0.823Hexachlorocyclopentadiene 1 10/16/22 17:52 V25161JMV
<0.098 mg/Kg - dry 0.098 0.823Hexachloroethane 1 10/16/22 17:52 V25161JMV
<0.223 mg/Kg - dry 0.223 0.823Indeno(1,2,3-cd)pyrene 1 10/16/22 17:52 V25161JMV
<0.238 mg/Kg - dry 0.238 0.823Isophorone 1 10/16/22 17:52 V25161JMV
<0.132 mg/Kg - dry 0.132 0.823
1-Methylnaphthalene 1 10/16/22 17:52 V25161JMV
<0.124 mg/Kg - dry 0.124 0.8232-Methylnaphthalene 1 10/16/22 17:52 V25161JMV
<0.121 mg/Kg - dry 0.121 0.8232-Methylphenol 1 10/16/22 17:52 V25161JMV
<0.105 mg/Kg - dry 0.105 0.8233&4 Methylphenol 1 10/16/22 17:52 V25161JMV
<0.179 mg/Kg - dry 0.179 0.823Naphthalene 1 10/16/22 17:52 V25161JMV
<0.120 mg/Kg - dry 0.120 0.8232-Nitroaniline 1 10/16/22 17:52 V25161JMV
<0.149 mg/Kg - dry 0.149 0.8233-Nitroaniline 1 10/16/22 17:52 V25161JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 22 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-2
89886 Matrix:
9/29/2022 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V24969 10/11/22 10:05
<0.116 mg/Kg - dry 0.116 0.4114-Nitroaniline 1 10/16/22 17:52 V25161JMV
<0.144 mg/Kg - dry 0.144 0.411Nitrobenzene 1 10/16/22 17:52 V25161JMV
<0.110 mg/Kg - dry 0.110 0.8232-Nitrophenol 1 10/16/22 17:52 V25161JMV
<0.146 mg/Kg - dry 0.146 0.8234-Nitrophenol 1 10/16/22 17:52 V25161JMV
<0.328 mg/Kg - dry 0.328 0.823N-Nitrosodimethylamine 1 10/16/22 17:52 V25161JMV
<0.225 mg/Kg - dry 0.225 0.823N-Nitrosodiphenylamine 1 10/16/22 17:52 V25161JMV
<0.147 mg/Kg - dry 0.147 0.823N-Nitroso-di-n-propylamine 1 10/16/22 17:52 V25161JMV
<0.433 mg/Kg - dry 0.433 1.25Pentachlorophenol 1 10/16/22 17:52 V25161JMV
<0.259 mg/Kg - dry 0.259 0.823
Phenanthrene 1 10/16/22 17:52 V25161JMV
<0.139 mg/Kg - dry 0.139 0.823Phenol 1 10/16/22 17:52 V25161JMV
<0.167 mg/Kg - dry 0.167 0.823Pyrene 1 10/16/22 17:52 V25161JMV
<0.098 mg/Kg - dry 0.098 0.411Pyridine 1 10/16/22 17:52 V25161JMV
<0.133 mg/Kg - dry 0.133 0.8231,2,4-Trichlorobenzene 1 10/16/22 17:52 V25161JMV
<0.120 mg/Kg - dry 0.120 0.8232,4,5-Trichlorophenol 1 10/16/22 17:52 V25161JMV
<0.120 mg/Kg - dry 0.120 0.8232,4,6-Trichlorophenol 1 10/16/22 17:52 V25161JMV
8270ESurrogate: Phenol-d5 89.2 Limits: 34-121%10/16/22 17:521 JMV
Surrogate: 2-Fluorobiphenyl 94.6 Limits: 44-115%10/16/22 17:521 JMV V25161
Surrogate: 2-Fluorophenol 96.7 Limits: 35-115%10/16/22 17:521 JMV V25161
Surrogate: Nitrobenzene-d5 86.8 Limits: 37-122%10/16/22 17:521 JMV V25161
Surrogate: 4-Terphenyl-d14 96.4 Limits: 54-127%10/16/22 17:521 JMV V25161
Surrogate: 2,4,6-Tribromophenol 92.5 Limits: 39-132%10/16/22 17:521 JMV V25161
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 23 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-3
89887 Matrix:
9/29/2022 12:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
14.1 %Moisture 1 10/07/22 09:53 SW-DRYWTAMB
<0.164 mg/Kg - dry 0.164 0.232Chromium, Hexavalent 1 10/11/22 15:50 SW-7199SAR
1.11 mg/Kg - dry 0.0995 0.291Arsenic 5 10/22/22 01:38 6020BBKN
86.6 mg/Kg - dry 0.049 0.291Barium 5 10/22/22 01:38 6020BBKN
0.0767 J mg/Kg - dry 0.0301 0.291Cadmium 5 10/22/22 01:38 6020BBKN
30.7 mg/Kg - dry 0.135 0.291
Chromium 5 10/22/22 01:38 6020BBKN
11.1 mg/Kg - dry 0.0360 0.291Lead 5 10/22/22 01:38 6020BBKN
0.0597 mg/Kg - dry 0.0140 0.0349Mercury (Total)1 10/19/22 13:29 7471BEDV
0.479 mg/Kg - dry 0.119 0.291Selenium 5 10/22/22 01:38 6020BBKN
0.0433 JB mg/Kg - dry 0.0078 0.291Silver 5 10/22/22 01:38 6020BBKN
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 24 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-3
89887 Matrix:
9/29/2022 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V24740 10/05/22 08:00
0.110 mg/Kg - dry 0.002 0.023Acetone 1 10/05/22 16:21 V24741TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 10/05/22 16:21 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 10/05/22 16:21 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 10/05/22 16:21 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 10/05/22 16:21 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 10/05/22 16:21 V24741TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 10/05/22 16:21 V24741TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 10/05/22 16:21 V24741TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 10/05/22 16:21 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 10/05/22 16:21 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 10/05/22 16:21 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 10/05/22 16:21 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 10/05/22 16:21 V24741TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 10/05/22 16:21 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 10/05/22 16:21 V24741TBL
<0.001 mg/Kg - dry 0.001 0.005
Chlorodibromomethane 1 10/05/22 16:21 V24741TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 10/05/22 16:21 V24741TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 10/05/22 16:21 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 10/05/22 16:21 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 10/05/22 16:21 V24741TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 10/05/22 16:21 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 10/05/22 16:21 V24741TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 25 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-3
89887 Matrix:
9/29/2022 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V24740 10/05/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 10/05/22 16:21 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 10/05/22 16:21 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 10/05/22 16:21 V24741TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 10/05/22 16:21 V24741TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 10/05/22 16:21 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 10/05/22 16:21 V24741TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 10/05/22 16:21 V24741TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 10/05/22 16:21 V24741TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 10/05/22 16:21 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 10/05/22 16:21 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 10/05/22 16:21 V24741TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 10/05/22 16:21 V24741TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 10/05/22 16:21 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 10/05/22 16:21 V24741TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 10/05/22 16:21 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.005
1,1-Dichloropropene 1 10/05/22 16:21 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 10/05/22 16:21 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 10/05/22 16:21 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 10/05/22 16:21 V24741TBL
<0.0010 mg/Kg - dry 0.0010 0.058Ethyl Tertiary Butyl Ether (ETBE)1 10/05/22 16:21 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 10/05/22 16:21 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 10/05/22 16:21 V24741TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 26 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-3
89887 Matrix:
9/29/2022 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V24740 10/05/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 10/05/22 16:21 V24741TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 10/05/22 16:21 V24741TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 10/05/22 16:21 V24741TBL
0.012 J mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 10/05/22 16:21 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 10/05/22 16:21 V24741TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 10/05/22 16:21 V24741TBL
0.002 J mg/Kg - dry 0.001 0.011Methylene Chloride 1 10/05/22 16:21 V24741TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 10/05/22 16:21 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.005
n-Propylbenzene 1 10/05/22 16:21 V24741TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 10/05/22 16:21 V24741TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 10/05/22 16:21 V24741TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 10/05/22 16:21 V24741TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 10/05/22 16:21 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 10/05/22 16:21 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 10/05/22 16:21 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.011
1,2,4-Trichlorobenzene 1 10/05/22 16:21 V24741TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 10/05/22 16:21 V24741TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 10/05/22 16:21 V24741TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 10/05/22 16:21 V24741TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 10/05/22 16:21 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 10/05/22 16:21 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 10/05/22 16:21 V24741TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 27 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-3
89887 Matrix:
9/29/2022 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V24740 10/05/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 10/05/22 16:21 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 10/05/22 16:21 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 10/05/22 16:21 V24741TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 10/05/22 16:21 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 10/05/22 16:21 V24741
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%10/05/22 16:211 TBL V24741
Surrogate: Dibromofluoromethane 102 Limits: 84-123%10/05/22 16:211 TBL V24741
Surrogate: Toluene-d8 97.9 Limits: 76-129%10/05/22 16:211 TBL V24741
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V24969 10/11/22 10:05
<0.135 mg/Kg - dry 0.135 0.768Acenaphthene 1 10/16/22 21:37 V25161JMV
<0.122 mg/Kg - dry 0.122 0.768Acenaphthylene 1 10/16/22 21:37 V25161JMV
<0.176 mg/Kg - dry 0.176 0.768Aniline 1 10/16/22 21:37 V25161JMV
<0.166 mg/Kg - dry 0.166 0.768Anthracene 1 10/16/22 21:37 V25161JMV
<0.161 mg/Kg - dry 0.161 0.768Benzo(a)anthracene 1 10/16/22 21:37 V25161JMV
<0.171 mg/Kg - dry 0.171 0.768Benzo(a)pyrene 1 10/16/22 21:37 V25161JMV
<0.169 mg/Kg - dry 0.169 0.768
Benzo(b)fluoranthene 1 10/16/22 21:37 V25161JMV
<0.158 mg/Kg - dry 0.158 0.768Benzo(g,h,i)perylene 1 10/16/22 21:37 V25161JMV
<0.159 mg/Kg - dry 0.159 0.768Benzo(k)fluoranthene 1 10/16/22 21:37 V25161JMV
<0.675 mg/Kg - dry 0.675 2.33Benzoic Acid 1 10/16/22 21:37 V25161JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 28 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-3
89887 Matrix:
9/29/2022 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V24969 10/11/22 10:05
<0.122 mg/Kg - dry 0.122 0.768Benzyl alcohol 1 10/16/22 21:37 V25161JMV
<0.137 mg/Kg - dry 0.137 0.768Bis(2-Chloroethoxy)methane 1 10/16/22 21:37 V25161JMV
<0.124 mg/Kg - dry 0.124 0.768Bis(2-Chloroethyl)ether 1 10/16/22 21:37 V25161JMV
<0.158 mg/Kg - dry 0.158 0.384Bis(2-Chloroisopropyl)ether 1 10/16/22 21:37 V25161JMV
<0.139 mg/Kg - dry 0.139 0.768Bis(2-ethylhexyl)phthalate 1 10/16/22 21:37 V25161JMV
<0.126 mg/Kg - dry 0.126 0.7684-Bromophenyl phenyl ether 1 10/16/22 21:37 V25161JMV
<0.131 mg/Kg - dry 0.131 0.384Butyl benzyl phthalate 1 10/16/22 21:37 V25161JMV
<0.107 mg/Kg - dry 0.107 0.7684-Chloro-3-methylphenol 1 10/16/22 21:37 V25161JMV
<0.130 mg/Kg - dry 0.130 0.384
4-Chloroaniline 1 10/16/22 21:37 V25161JMV
<0.135 mg/Kg - dry 0.135 0.7682-Chloronaphthalene 1 10/16/22 21:37 V25161JMV
<0.114 mg/Kg - dry 0.114 0.7682-Chlorophenol 1 10/16/22 21:37 V25161JMV
<0.146 mg/Kg - dry 0.146 1.164-Chlorophenyl phenyl ether 1 10/16/22 21:37 V25161JMV
<0.165 mg/Kg - dry 0.165 0.768Chrysene 1 10/16/22 21:37 V25161JMV
<0.267 mg/Kg - dry 0.267 0.768Dibenz(a,h)anthracene 1 10/16/22 21:37 V25161JMV
<0.138 mg/Kg - dry 0.138 0.768Dibenzofuran 1 10/16/22 21:37 V25161JMV
<0.109 mg/Kg - dry 0.109 0.768
1,2-Dichlorobenzene 1 10/16/22 21:37 V25161JMV
<0.113 mg/Kg - dry 0.113 0.7681,3-Dichlorobenzene 1 10/16/22 21:37 V25161JMV
<0.113 mg/Kg - dry 0.113 0.3841,4-Dichlorobenzene 1 10/16/22 21:37 V25161JMV
<0.171 mg/Kg - dry 0.171 0.7683,3'-Dichlorobenzidine 1 10/16/22 21:37 V25161JMV
<0.111 mg/Kg - dry 0.111 0.7682,4-Dichlorophenol 1 10/16/22 21:37 V25161JMV
<0.209 mg/Kg - dry 0.209 0.768Diethyl phthalate 1 10/16/22 21:37 V25161JMV
<0.202 mg/Kg - dry 0.202 0.768Dimethyl phthalate 1 10/16/22 21:37 V25161JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 29 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-3
89887 Matrix:
9/29/2022 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V24969 10/11/22 10:05
<0.125 mg/Kg - dry 0.125 0.3842,4-Dimethylphenol 1 10/16/22 21:37 V25161JMV
<0.124 mg/Kg - dry 0.124 0.768Di-n-butyl phthalate 1 10/16/22 21:37 V25161JMV
<0.279 mg/Kg - dry 0.279 1.754,6-Dinitro-2-methylphenol 1 10/16/22 21:37 V25161JMV
<0.605 mg/Kg - dry 0.605 1.752,4-Dinitrophenol 1 10/16/22 21:37 V25161JMV
<0.112 mg/Kg - dry 0.112 0.7682,4-Dinitrotoluene 1 10/16/22 21:37 V25161JMV
<0.125 mg/Kg - dry 0.125 0.7682,6-Dinitrotoluene 1 10/16/22 21:37 V25161JMV
<0.166 mg/Kg - dry 0.166 0.384Di-n-Octyl Phthalate 1 10/16/22 21:37 V25161JMV
0.175 J mg/Kg - dry 0.143 0.768Fluoranthene 1 10/16/22 21:37 V25161JMV
<0.149 mg/Kg - dry 0.149 0.768
Fluorene 1 10/16/22 21:37 V25161JMV
<0.123 mg/Kg - dry 0.123 0.768Hexachlorobenzene 1 10/16/22 21:37 V25161JMV
<0.113 mg/Kg - dry 0.113 0.768Hexachlorobutadiene 1 10/16/22 21:37 V25161JMV
<0.182 mg/Kg - dry 0.182 0.768Hexachlorocyclopentadiene 1 10/16/22 21:37 V25161JMV
<0.092 mg/Kg - dry 0.092 0.768Hexachloroethane 1 10/16/22 21:37 V25161JMV
<0.208 mg/Kg - dry 0.208 0.768Indeno(1,2,3-cd)pyrene 1 10/16/22 21:37 V25161JMV
<0.222 mg/Kg - dry 0.222 0.768Isophorone 1 10/16/22 21:37 V25161JMV
<0.123 mg/Kg - dry 0.123 0.768
1-Methylnaphthalene 1 10/16/22 21:37 V25161JMV
<0.116 mg/Kg - dry 0.116 0.7682-Methylnaphthalene 1 10/16/22 21:37 V25161JMV
<0.112 mg/Kg - dry 0.112 0.7682-Methylphenol 1 10/16/22 21:37 V25161JMV
<0.098 mg/Kg - dry 0.098 0.7683&4 Methylphenol 1 10/16/22 21:37 V25161JMV
<0.167 mg/Kg - dry 0.167 0.768Naphthalene 1 10/16/22 21:37 V25161JMV
<0.112 mg/Kg - dry 0.112 0.7682-Nitroaniline 1 10/16/22 21:37 V25161JMV
<0.139 mg/Kg - dry 0.139 0.7683-Nitroaniline 1 10/16/22 21:37 V25161JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 30 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:Comp-3
89887 Matrix:
9/29/2022 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V24969 10/11/22 10:05
<0.108 mg/Kg - dry 0.108 0.3844-Nitroaniline 1 10/16/22 21:37 V25161JMV
<0.135 mg/Kg - dry 0.135 0.384Nitrobenzene 1 10/16/22 21:37 V25161JMV
<0.103 mg/Kg - dry 0.103 0.7682-Nitrophenol 1 10/16/22 21:37 V25161JMV
<0.136 mg/Kg - dry 0.136 0.7684-Nitrophenol 1 10/16/22 21:37 V25161JMV
<0.306 mg/Kg - dry 0.306 0.768N-Nitrosodimethylamine 1 10/16/22 21:37 V25161JMV
<0.210 mg/Kg - dry 0.210 0.768N-Nitrosodiphenylamine 1 10/16/22 21:37 V25161JMV
<0.137 mg/Kg - dry 0.137 0.768N-Nitroso-di-n-propylamine 1 10/16/22 21:37 V25161JMV
<0.403 mg/Kg - dry 0.403 1.16Pentachlorophenol 1 10/16/22 21:37 V25161JMV
<0.242 mg/Kg - dry 0.242 0.768
Phenanthrene 1 10/16/22 21:37 V25161JMV
<0.130 mg/Kg - dry 0.130 0.768Phenol 1 10/16/22 21:37 V25161JMV
<0.155 mg/Kg - dry 0.155 0.768Pyrene 1 10/16/22 21:37 V25161JMV
<0.092 mg/Kg - dry 0.092 0.384Pyridine 1 10/16/22 21:37 V25161JMV
<0.124 mg/Kg - dry 0.124 0.7681,2,4-Trichlorobenzene 1 10/16/22 21:37 V25161JMV
<0.111 mg/Kg - dry 0.111 0.7682,4,5-Trichlorophenol 1 10/16/22 21:37 V25161JMV
<0.112 mg/Kg - dry 0.112 0.7682,4,6-Trichlorophenol 1 10/16/22 21:37 V25161JMV
8270ESurrogate: Phenol-d5 81.7 Limits: 34-121%10/16/22 21:371 JMV
Surrogate: 2-Fluorobiphenyl 91.6 Limits: 44-115%10/16/22 21:371 JMV V25161
Surrogate: 2-Fluorophenol 86.2 Limits: 35-115%10/16/22 21:371 JMV V25161
Surrogate: Nitrobenzene-d5 85.0 Limits: 37-122%10/16/22 21:371 JMV V25161
Surrogate: 4-Terphenyl-d14 100 Limits: 54-127%10/16/22 21:371 JMV V25161
Surrogate: 2,4,6-Tribromophenol 97.6 Limits: 39-132%10/16/22 21:371 JMV V25161
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 31 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:TP-4
89888 Matrix:
9/29/2022 12:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
15.1 %Moisture 1 10/07/22 09:53 SW-DRYWTAMB
0.332 mg/Kg - dry 0.166 0.236Chromium, Hexavalent 1 10/11/22 16:01 SW-7199SAR
1.46 mg/Kg - dry 0.101 0.294Arsenic 5 10/22/22 01:44 6020BBKN
30.2 mg/Kg - dry 0.050 0.294Barium 5 10/22/22 01:44 6020BBKN
<0.0305 mg/Kg - dry 0.0305 0.294Cadmium 5 10/22/22 01:44 6020BBKN
31.8 mg/Kg - dry 0.136 0.294
Chromium 5 10/22/22 01:44 6020BBKN
4.58 mg/Kg - dry 0.0365 0.294Lead 5 10/22/22 01:44 6020BBKN
0.0695 mg/Kg - dry 0.0141 0.0353Mercury (Total)1 10/19/22 13:31 7471BEDV
0.382 mg/Kg - dry 0.121 0.294Selenium 5 10/22/22 01:44 6020BBKN
0.0243 JB mg/Kg - dry 0.0079 0.294Silver 5 10/22/22 01:44 6020BBKN
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 32 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:TP-4
89888 Matrix:
9/29/2022 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V24740 10/05/22 08:00
0.049 mg/Kg - dry 0.002 0.023Acetone 1 10/05/22 16:48 V24741TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 10/05/22 16:48 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 10/05/22 16:48 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 10/05/22 16:48 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 10/05/22 16:48 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 10/05/22 16:48 V24741TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 10/05/22 16:48 V24741TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 10/05/22 16:48 V24741TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 10/05/22 16:48 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 10/05/22 16:48 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 10/05/22 16:48 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 10/05/22 16:48 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.005Carbon Disulfide 1 10/05/22 16:48 V24741TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 10/05/22 16:48 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 10/05/22 16:48 V24741TBL
<0.001 mg/Kg - dry 0.001 0.005
Chlorodibromomethane 1 10/05/22 16:48 V24741TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 10/05/22 16:48 V24741TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 10/05/22 16:48 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 10/05/22 16:48 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 10/05/22 16:48 V24741TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 10/05/22 16:48 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 10/05/22 16:48 V24741TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 33 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:TP-4
89888 Matrix:
9/29/2022 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V24740 10/05/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 10/05/22 16:48 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 10/05/22 16:48 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 10/05/22 16:48 V24741TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 10/05/22 16:48 V24741TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 10/05/22 16:48 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 10/05/22 16:48 V24741TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 10/05/22 16:48 V24741TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 10/05/22 16:48 V24741TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 10/05/22 16:48 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 10/05/22 16:48 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 10/05/22 16:48 V24741TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 10/05/22 16:48 V24741TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 10/05/22 16:48 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 10/05/22 16:48 V24741TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 10/05/22 16:48 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.005
1,1-Dichloropropene 1 10/05/22 16:48 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 10/05/22 16:48 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 10/05/22 16:48 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 10/05/22 16:48 V24741TBL
<0.0010 mg/Kg - dry 0.0010 0.058Ethyl Tertiary Butyl Ether (ETBE)1 10/05/22 16:48 V24741TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 10/05/22 16:48 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 10/05/22 16:48 V24741TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 34 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:TP-4
89888 Matrix:
9/29/2022 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V24740 10/05/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 10/05/22 16:48 V24741TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 10/05/22 16:48 V24741TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 10/05/22 16:48 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 10/05/22 16:48 V24741TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 10/05/22 16:48 V24741TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 10/05/22 16:48 V24741TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 10/05/22 16:48 V24741TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 10/05/22 16:48 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.005
n-Propylbenzene 1 10/05/22 16:48 V24741TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 10/05/22 16:48 V24741TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 10/05/22 16:48 V24741TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 10/05/22 16:48 V24741TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 10/05/22 16:48 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 10/05/22 16:48 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 10/05/22 16:48 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.011
1,2,4-Trichlorobenzene 1 10/05/22 16:48 V24741TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 10/05/22 16:48 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,1,2-Trichloroethane 1 10/05/22 16:48 V24741TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 10/05/22 16:48 V24741TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 10/05/22 16:48 V24741TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 10/05/22 16:48 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 10/05/22 16:48 V24741TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 35 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:TP-4
89888 Matrix:
9/29/2022 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V24740 10/05/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 10/05/22 16:48 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 10/05/22 16:48 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 10/05/22 16:48 V24741TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 10/05/22 16:48 V24741TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 10/05/22 16:48 V24741
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%10/05/22 16:481 TBL V24741
Surrogate: Dibromofluoromethane 105 Limits: 84-123%10/05/22 16:481 TBL V24741
Surrogate: Toluene-d8 98.7 Limits: 76-129%10/05/22 16:481 TBL V24741
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V24969 10/11/22 10:05
<0.136 mg/Kg - dry 0.136 0.777Acenaphthene 1 10/16/22 18:15 V25161JMV
<0.123 mg/Kg - dry 0.123 0.777Acenaphthylene 1 10/16/22 18:15 V25161JMV
<0.179 mg/Kg - dry 0.179 0.777Aniline 1 10/16/22 18:15 V25161JMV
<0.168 mg/Kg - dry 0.168 0.777Anthracene 1 10/16/22 18:15 V25161JMV
<0.163 mg/Kg - dry 0.163 0.777Benzo(a)anthracene 1 10/16/22 18:15 V25161JMV
<0.173 mg/Kg - dry 0.173 0.777Benzo(a)pyrene 1 10/16/22 18:15 V25161JMV
<0.171 mg/Kg - dry 0.171 0.777
Benzo(b)fluoranthene 1 10/16/22 18:15 V25161JMV
<0.160 mg/Kg - dry 0.160 0.777Benzo(g,h,i)perylene 1 10/16/22 18:15 V25161JMV
<0.161 mg/Kg - dry 0.161 0.777Benzo(k)fluoranthene 1 10/16/22 18:15 V25161JMV
<0.683 mg/Kg - dry 0.683 2.36Benzoic Acid 1 10/16/22 18:15 V25161JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 36 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:TP-4
89888 Matrix:
9/29/2022 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V24969 10/11/22 10:05
<0.123 mg/Kg - dry 0.123 0.777Benzyl alcohol 1 10/16/22 18:15 V25161JMV
<0.138 mg/Kg - dry 0.138 0.777Bis(2-Chloroethoxy)methane 1 10/16/22 18:15 V25161JMV
<0.126 mg/Kg - dry 0.126 0.777Bis(2-Chloroethyl)ether 1 10/16/22 18:15 V25161JMV
<0.160 mg/Kg - dry 0.160 0.388Bis(2-Chloroisopropyl)ether 1 10/16/22 18:15 V25161JMV
<0.141 mg/Kg - dry 0.141 0.777Bis(2-ethylhexyl)phthalate 1 10/16/22 18:15 V25161JMV
<0.128 mg/Kg - dry 0.128 0.7774-Bromophenyl phenyl ether 1 10/16/22 18:15 V25161JMV
<0.133 mg/Kg - dry 0.133 0.388Butyl benzyl phthalate 1 10/16/22 18:15 V25161JMV
<0.108 mg/Kg - dry 0.108 0.7774-Chloro-3-methylphenol 1 10/16/22 18:15 V25161JMV
<0.131 mg/Kg - dry 0.131 0.388
4-Chloroaniline 1 10/16/22 18:15 V25161JMV
<0.136 mg/Kg - dry 0.136 0.7772-Chloronaphthalene 1 10/16/22 18:15 V25161JMV
<0.115 mg/Kg - dry 0.115 0.7772-Chlorophenol 1 10/16/22 18:15 V25161JMV
<0.148 mg/Kg - dry 0.148 1.184-Chlorophenyl phenyl ether 1 10/16/22 18:15 V25161JMV
<0.167 mg/Kg - dry 0.167 0.777Chrysene 1 10/16/22 18:15 V25161JMV
<0.270 mg/Kg - dry 0.270 0.777Dibenz(a,h)anthracene 1 10/16/22 18:15 V25161JMV
<0.140 mg/Kg - dry 0.140 0.777Dibenzofuran 1 10/16/22 18:15 V25161JMV
<0.111 mg/Kg - dry 0.111 0.777
1,2-Dichlorobenzene 1 10/16/22 18:15 V25161JMV
<0.114 mg/Kg - dry 0.114 0.7771,3-Dichlorobenzene 1 10/16/22 18:15 V25161JMV
<0.114 mg/Kg - dry 0.114 0.3881,4-Dichlorobenzene 1 10/16/22 18:15 V25161JMV
<0.173 mg/Kg - dry 0.173 0.7773,3'-Dichlorobenzidine 1 10/16/22 18:15 V25161JMV
<0.112 mg/Kg - dry 0.112 0.7772,4-Dichlorophenol 1 10/16/22 18:15 V25161JMV
<0.212 mg/Kg - dry 0.212 0.777Diethyl phthalate 1 10/16/22 18:15 V25161JMV
<0.204 mg/Kg - dry 0.204 0.777Dimethyl phthalate 1 10/16/22 18:15 V25161JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 37 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:TP-4
89888 Matrix:
9/29/2022 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V24969 10/11/22 10:05
<0.127 mg/Kg - dry 0.127 0.3882,4-Dimethylphenol 1 10/16/22 18:15 V25161JMV
<0.126 mg/Kg - dry 0.126 0.777Di-n-butyl phthalate 1 10/16/22 18:15 V25161JMV
<0.282 mg/Kg - dry 0.282 1.774,6-Dinitro-2-methylphenol 1 10/16/22 18:15 V25161JMV
<0.612 mg/Kg - dry 0.612 1.772,4-Dinitrophenol 1 10/16/22 18:15 V25161JMV
<0.113 mg/Kg - dry 0.113 0.7772,4-Dinitrotoluene 1 10/16/22 18:15 V25161JMV
<0.127 mg/Kg - dry 0.127 0.7772,6-Dinitrotoluene 1 10/16/22 18:15 V25161JMV
<0.168 mg/Kg - dry 0.168 0.388Di-n-Octyl Phthalate 1 10/16/22 18:15 V25161JMV
<0.144 mg/Kg - dry 0.144 0.777Fluoranthene 1 10/16/22 18:15 V25161JMV
<0.150 mg/Kg - dry 0.150 0.777
Fluorene 1 10/16/22 18:15 V25161JMV
<0.124 mg/Kg - dry 0.124 0.777Hexachlorobenzene 1 10/16/22 18:15 V25161JMV
<0.114 mg/Kg - dry 0.114 0.777Hexachlorobutadiene 1 10/16/22 18:15 V25161JMV
<0.184 mg/Kg - dry 0.184 0.777Hexachlorocyclopentadiene 1 10/16/22 18:15 V25161JMV
<0.093 mg/Kg - dry 0.093 0.777Hexachloroethane 1 10/16/22 18:15 V25161JMV
<0.210 mg/Kg - dry 0.210 0.777Indeno(1,2,3-cd)pyrene 1 10/16/22 18:15 V25161JMV
<0.224 mg/Kg - dry 0.224 0.777Isophorone 1 10/16/22 18:15 V25161JMV
<0.124 mg/Kg - dry 0.124 0.777
1-Methylnaphthalene 1 10/16/22 18:15 V25161JMV
<0.117 mg/Kg - dry 0.117 0.7772-Methylnaphthalene 1 10/16/22 18:15 V25161JMV
<0.114 mg/Kg - dry 0.114 0.7772-Methylphenol 1 10/16/22 18:15 V25161JMV
<0.100 mg/Kg - dry 0.100 0.7773&4 Methylphenol 1 10/16/22 18:15 V25161JMV
<0.169 mg/Kg - dry 0.169 0.777Naphthalene 1 10/16/22 18:15 V25161JMV
<0.113 mg/Kg - dry 0.113 0.7772-Nitroaniline 1 10/16/22 18:15 V25161JMV
<0.141 mg/Kg - dry 0.141 0.7773-Nitroaniline 1 10/16/22 18:15 V25161JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 38 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-277-0037
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/04/2022
RMR-013
Report Date : 10/24/2022
Sample ID :
Lab No :
Sampled:TP-4
89888 Matrix:
9/29/2022 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V24969 10/11/22 10:05
<0.109 mg/Kg - dry 0.109 0.3884-Nitroaniline 1 10/16/22 18:15 V25161JMV
<0.136 mg/Kg - dry 0.136 0.388Nitrobenzene 1 10/16/22 18:15 V25161JMV
<0.104 mg/Kg - dry 0.104 0.7772-Nitrophenol 1 10/16/22 18:15 V25161JMV
<0.137 mg/Kg - dry 0.137 0.7774-Nitrophenol 1 10/16/22 18:15 V25161JMV
<0.309 mg/Kg - dry 0.309 0.777N-Nitrosodimethylamine 1 10/16/22 18:15 V25161JMV
<0.213 mg/Kg - dry 0.213 0.777N-Nitrosodiphenylamine 1 10/16/22 18:15 V25161JMV
<0.138 mg/Kg - dry 0.138 0.777N-Nitroso-di-n-propylamine 1 10/16/22 18:15 V25161JMV
<0.408 mg/Kg - dry 0.408 1.18Pentachlorophenol 1 10/16/22 18:15 V25161JMV
<0.244 mg/Kg - dry 0.244 0.777
Phenanthrene 1 10/16/22 18:15 V25161JMV
<0.131 mg/Kg - dry 0.131 0.777Phenol 1 10/16/22 18:15 V25161JMV
<0.157 mg/Kg - dry 0.157 0.777Pyrene 1 10/16/22 18:15 V25161JMV
<0.093 mg/Kg - dry 0.093 0.388Pyridine 1 10/16/22 18:15 V25161JMV
<0.126 mg/Kg - dry 0.126 0.7771,2,4-Trichlorobenzene 1 10/16/22 18:15 V25161JMV
<0.113 mg/Kg - dry 0.113 0.7772,4,5-Trichlorophenol 1 10/16/22 18:15 V25161JMV
<0.113 mg/Kg - dry 0.113 0.7772,4,6-Trichlorophenol 1 10/16/22 18:15 V25161JMV
8270ESurrogate: Phenol-d5 86.5 Limits: 34-121%10/16/22 18:151 JMV
Surrogate: 2-Fluorobiphenyl 95.2 Limits: 44-115%10/16/22 18:151 JMV V25161
Surrogate: 2-Fluorophenol 87.7 Limits: 35-115%10/16/22 18:151 JMV V25161
Surrogate: Nitrobenzene-d5 86.8 Limits: 37-122%10/16/22 18:151 JMV V25161
Surrogate: 4-Terphenyl-d14 94.0 Limits: 54-127%10/16/22 18:151 JMV V25161
Surrogate: 2,4,6-Tribromophenol 85.3 Limits: 39-132%10/16/22 18:151 JMV V25161
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 39 of 61
Quality Control Data
22-277-0037Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Metals Analyses
6020B
L644767QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L644584
Associated Lab Samples: 89885, 89886, 89887, 89888
LRB-L644584 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
10/22/22 01:090.2500.0855<0.0855mg/KgArsenic
10/22/22 01:090.2500.042<0.042mg/KgBarium
10/22/22 01:090.2500.0259<0.0259mg/KgCadmium
10/22/22 01:090.2500.116<0.116mg/KgChromium
10/22/22 01:090.2500.0310<0.0310mg/KgLead
10/22/22 01:090.2500.103<0.103mg/KgSelenium
10/22/22 01:090.2500.00670.0133mg/KgSilver
LCS-L644584Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
96.02.402.50mg/KgArsenic 80-120
96.04.825.00mg/KgBarium 80-120
99.00.4940.500mg/KgCadmium 80-120
98.04.925.00mg/KgChromium 80-120
94.02.362.50mg/KgLead 80-120
94.04.715.00mg/KgSelenium 80-120
1020.5120.500mg/KgSilver 80-120
V 91021-MS-L644584 V 91021-MSD-L644584Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
2.03 58.0*2.022.442.410.644mg/KgArsenic 56.0*75-125 0.4 80
64.2 -100*66.74.894.8269.9mg/KgBarium -65*75-125 3.8 80
0.586 1090.5000.4890.4820.0588mg/KgCadmium 90.0 75-125 15.8 80
10.1 87.010.74.894.825.91mg/KgChromium 98.0 75-125 5.7 80
Page 1 of 20* QC Fail Date:10/24/2022 02:48 PM
Page 40 of 61
Quality Control Data
22-277-0037Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Metals Analyses
6020B
L644767QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L644584
V 91021-MS-L644584 V 91021-MSD-L644584Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
14.3 58.0*13.82.442.4112.9mg/KgLead 37.0*75-125 3.5 80
3.27 56.0*3.074.894.820.550mg/KgSelenium 52.0*75-125 6.3 80
0.488 93.00.4770.4890.4820.0413mg/KgSilver 89.0 75-125 2.2 80
V 91021-PDS-L644584Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
10/22/22 02:5485.01.09mg/KgArsenic
10/22/22 02:5497.09.16mg/KgBarium
10/22/22 02:541050.264mg/KgCadmium
10/22/22 02:541013.08mg/KgChromium
10/22/22 02:5497.02.44mg/KgLead
10/22/22 02:5483.02.07mg/KgSelenium
10/22/22 02:541000.248mg/KgSilver
Page 2 of 20* QC Fail Date:10/24/2022 02:48 PM
Page 41 of 61
Quality Control Data
22-277-0037Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V25326QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V25270
Associated Lab Samples: 89885, 89886, 89887, 89888
LRB-V25270 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
10/19/22 12:540.03000.0120<0.0120mg/KgMercury (Total)
LCS-V25270Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1050.4380.417mg/KgMercury (Total)80-120
V 90753-MS-V25270 V 90753-MSD-V25270Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.453 1090.4500.4170.4170.0266mg/KgMercury (Total)108 80-120 0.6 20
V 90753-PDS-V25270Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
10/19/22 13:101100.229mg/KgMercury (Total)
Page 3 of 20Date:10/24/2022 02:48 PM
Page 42 of 61
Quality Control Data
22-277-0037Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V24741QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V24740
Associated Lab Samples: 89885, 89886, 89887, 89888
LRB-V24740 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/05/22 11:220.0200.002<0.002mg/KgAcetone
10/05/22 11:220.0200.001<0.001mg/KgAcrolein
10/05/22 11:220.0200.0008<0.0008mg/KgAcrylonitrile
10/05/22 11:220.0050.0006<0.0006mg/KgBenzene
10/05/22 11:220.0050.0005<0.0005mg/KgBromobenzene
10/05/22 11:220.0050.0008<0.0008mg/KgBromochloromethane
10/05/22 11:220.0050.001<0.001mg/KgBromodichloromethane
10/05/22 11:220.0050.001<0.001mg/KgBromoform
10/05/22 11:220.0100.001<0.001mg/KgBromomethane
10/05/22 11:220.0050.0005<0.0005mg/Kgn-Butylbenzene
10/05/22 11:220.0050.0006<0.0006mg/Kgsec-Butyl benzene
10/05/22 11:220.0050.0005<0.0005mg/Kgtert-Butyl benzene
10/05/22 11:220.0050.0006<0.0006mg/KgCarbon Disulfide
10/05/22 11:220.0050.001<0.001mg/KgCarbon Tetrachloride
10/05/22 11:220.0050.0007<0.0007mg/KgChlorobenzene
10/05/22 11:220.0050.0009<0.0009mg/KgChlorodibromomethane
10/05/22 11:220.0100.0009<0.0009mg/KgChloroethane
10/05/22 11:220.0050.001<0.001mg/KgChloroform
10/05/22 11:220.0100.0006<0.0006mg/KgChloromethane
10/05/22 11:220.0050.0005<0.0005mg/Kg2-Chlorotoluene
10/05/22 11:220.0050.0004<0.0004mg/Kg4-Chlorotoluene
10/05/22 11:220.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
10/05/22 11:220.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
10/05/22 11:220.0050.0006<0.0006mg/Kg1,2-Dibromoethane
10/05/22 11:220.0050.0006<0.0006mg/KgDibromomethane
10/05/22 11:220.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
10/05/22 11:220.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 4 of 20Date:10/24/2022 02:48 PM
Page 43 of 61
Quality Control Data
22-277-0037Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V24741QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V24740
Associated Lab Samples: 89885, 89886, 89887, 89888
LRB-V24740 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/05/22 11:220.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
10/05/22 11:220.0100.001<0.001mg/KgDichlorodifluoromethane
10/05/22 11:220.0050.0008<0.0008mg/Kg1,1-Dichloroethane
10/05/22 11:220.0050.001<0.001mg/Kg1,2-Dichloroethane
10/05/22 11:220.0050.0007<0.0007mg/Kg1,1-Dichloroethene
10/05/22 11:220.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
10/05/22 11:220.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
10/05/22 11:220.0050.0004<0.0004mg/Kg1,2-Dichloropropane
10/05/22 11:220.0050.0006<0.0006mg/Kg1,3-Dichloropropane
10/05/22 11:220.0050.001<0.001mg/Kg2,2-Dichloropropane
10/05/22 11:220.0050.0008<0.0008mg/Kg1,1-Dichloropropene
10/05/22 11:220.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
10/05/22 11:220.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
10/05/22 11:220.0050.0006<0.0006mg/KgEthylbenzene
10/05/22 11:220.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
10/05/22 11:220.0100.0008<0.0008mg/KgHexachlorobutadiene
10/05/22 11:220.0100.0007<0.0007mg/Kgn-Hexane
10/05/22 11:220.0200.0006<0.0006mg/Kg2-Hexanone
10/05/22 11:220.0050.0005<0.0005mg/KgIsopropylbenzene
10/05/22 11:220.0050.001<0.001mg/Kg4-Isopropyl toluene
10/05/22 11:220.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
10/05/22 11:220.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
10/05/22 11:220.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
10/05/22 11:220.0100.001<0.001mg/KgMethylene Chloride
10/05/22 11:220.0100.0010<0.0010mg/KgNaphthalene
10/05/22 11:220.0050.0005<0.0005mg/Kgn-Propylbenzene
10/05/22 11:220.0050.001<0.001mg/KgStyrene
Page 5 of 20Date:10/24/2022 02:48 PM
Page 44 of 61
Quality Control Data
22-277-0037Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V24741QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V24740
Associated Lab Samples: 89885, 89886, 89887, 89888
LRB-V24740 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/05/22 11:220.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
10/05/22 11:220.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
10/05/22 11:220.0050.0009<0.0009mg/KgTetrachloroethene
10/05/22 11:220.0050.0007<0.0007mg/KgToluene
10/05/22 11:220.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
10/05/22 11:220.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
10/05/22 11:220.0050.001<0.001mg/Kg1,1,1-Trichloroethane
10/05/22 11:220.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
10/05/22 11:220.0050.0009<0.0009mg/KgTrichloroethene
10/05/22 11:220.0100.002<0.002mg/KgTrichlorofluoromethane
10/05/22 11:220.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
10/05/22 11:220.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
10/05/22 11:220.0100.0005<0.0005mg/KgVinyl Acetate
10/05/22 11:220.0100.0005<0.0005mg/KgVinyl Chloride
10/05/22 11:220.0050.0005<0.0005mg/Kgo-Xylene
10/05/22 11:220.0100.001<0.001mg/Kgm,p-Xylene
10/05/22 11:224-Bromofluorobenzene (S)100 70-130
10/05/22 11:22Dibromofluoromethane (S)102 84-123
10/05/22 11:22Toluene-d8 (S)96.0 76-129
LCS-V24740 LCSD-V24740Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.097 97.095.20.0950.100mg/KgAcetone 29-198 1.8 20
0.113 1131210.1210.100mg/KgAcrolein 70-130 6.8 20
0.103 1031010.1010.100mg/KgAcrylonitrile 65-134 1.9 20
Page 6 of 20Date:10/24/2022 02:48 PM
Page 45 of 61
Quality Control Data
22-277-0037Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V24741QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V24740
LCS-V24740 LCSD-V24740Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.047 94.099.20.0490.050mg/KgBenzene 74-127 5.3 20
0.045 91.689.60.0440.050mg/KgBromobenzene 73-125 2.2 20
0.053 1061130.0560.050mg/KgBromochloromethane 72-134 6.2 20
0.049 98.81000.0500.050mg/KgBromodichloromethane 75-122 1.6 20
0.050 1011000.0500.050mg/KgBromoform 66-135 1.3 20
0.048 96.61160.0580.050mg/KgBromomethane 20-180 18.4 20
0.043 86.489.60.0440.050mg/Kgn-Butylbenzene 65-135 3.6 20
0.044 88.090.00.0450.050mg/Kgsec-Butyl benzene 66-131 2.2 20
0.043 86.289.40.0440.050mg/Kgtert-Butyl benzene 67-132 3.6 20
0.045 90.497.80.0480.050mg/KgCarbon Disulfide 61-129 7.8 20
0.043 86.696.20.0480.050mg/KgCarbon Tetrachloride 64-143 10.5 20
0.046 92.493.40.0460.050mg/KgChlorobenzene 74-118 1.0 20
0.048 97.41010.0500.050mg/KgChlorodibromomethane 73-122 3.8 20
0.041 82.489.40.0440.050mg/KgChloroethane 33-149 8.1 20
0.046 92.497.60.0480.050mg/KgChloroform 73-127 5.4 20
0.029 58.464.80.0320.050mg/KgChloromethane 45-143 10.3 20
0.043 86.488.60.0440.050mg/Kg2-Chlorotoluene 67-124 2.5 20
0.043 86.488.60.0440.050mg/Kg4-Chlorotoluene 71-126 2.5 20
0.049 98.097.60.0480.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.4 20
0.056 11298.60.0490.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 12.7 20
0.052 1051040.0510.050mg/Kg1,2-Dibromoethane 70-132 1.7 20
0.054 1101040.0510.050mg/KgDibromomethane 74-133 5.6 20
0.046 92.090.40.0450.050mg/Kg1,2-Dichlorobenzene 72-123 1.7 20
0.046 92.692.60.0460.050mg/Kg1,3-Dichlorobenzene 71-120 0.0 20
0.044 89.893.00.0460.050mg/Kg1,4-Dichlorobenzene 71-123 3.5 20
0.035 70.276.40.0380.050mg/KgDichlorodifluoromethane 26-146 8.4 20
Page 7 of 20Date:10/24/2022 02:48 PM
Page 46 of 61
Quality Control Data
22-277-0037Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V24741QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V24740
LCS-V24740 LCSD-V24740Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.045 91.895.40.0470.050mg/Kg1,1-Dichloroethane 74-127 3.8 20
0.048 96.499.20.0490.050mg/Kg1,2-Dichloroethane 68-128 2.8 20
0.044 88.497.20.0480.050mg/Kg1,1-Dichloroethene 67-149 9.4 20
0.048 96.21010.0500.050mg/Kgcis-1,2-Dichloroethene 76-134 4.6 20
0.045 91.499.80.0490.050mg/Kgtrans-1,2-Dichloroethene 73-132 8.7 20
0.048 97.41010.0500.050mg/Kg1,2-Dichloropropane 73-130 3.8 20
0.049 98.098.20.0490.050mg/Kg1,3-Dichloropropane 75-124 0.2 20
0.045 90.81010.0500.050mg/Kg2,2-Dichloropropane 50-142 10.8 20
0.044 88.896.80.0480.050mg/Kg1,1-Dichloropropene 71-130 8.6 20
0.051 1031040.0520.050mg/Kgcis-1,3-Dichloropropene 71-125 1.3 20
0.051 1021040.0520.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.7 20
0.044 88.092.80.0460.050mg/KgEthylbenzene 74-128 5.3 20
0.099 99.798.50.0980.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 1.2 20
0.043 87.890.60.0450.050mg/KgHexachlorobutadiene 64-125 3.1 20
0.044 89.01050.0520.050mg/Kgn-Hexane 70-130 16.4 20
0.058 1161110.0550.050mg/Kg2-Hexanone 61-157 4.7 20
0.043 86.488.00.0440.050mg/KgIsopropylbenzene 68-126 1.8 20
0.043 87.692.40.0460.050mg/Kg4-Isopropyl toluene 68-129 5.3 20
0.048 97.694.00.0470.050mg/KgMethyl Ethyl Ketone (MEK)63-149 3.7 20
0.052 1041010.0500.050mg/KgMethyl tert-butyl ether (MTBE)70-130 3.3 20
0.055 1121090.0540.050mg/Kg4-Methyl-2-Pentanone 57-162 2.7 20
0.041 82.087.20.0430.050mg/KgMethylene Chloride 74-129 6.1 20
0.047 95.894.40.0470.050mg/KgNaphthalene 57-157 1.4 20
0.043 87.288.80.0440.050mg/Kgn-Propylbenzene 67-130 1.8 20
0.048 96.299.80.0490.050mg/KgStyrene 77-121 3.6 20
0.047 95.099.40.0490.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 4.5 20
Page 8 of 20Date:10/24/2022 02:48 PM
Page 47 of 61
Quality Control Data
22-277-0037Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V24741QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V24740
LCS-V24740 LCSD-V24740Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.050 10195.40.0470.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 5.9 20
0.045 90.492.20.0460.050mg/KgTetrachloroethene 68-130 1.9 20
0.046 92.696.20.0480.050mg/KgToluene 71-129 3.8 20
0.047 94.689.00.0440.050mg/Kg1,2,3-Trichlorobenzene 68-130 6.1 20
0.045 90.890.40.0450.050mg/Kg1,2,4-Trichlorobenzene 66-125 0.4 20
0.044 89.293.80.0460.050mg/Kg1,1,1-Trichloroethane 67-131 5.0 20
0.051 1031010.0500.050mg/Kg1,1,2-Trichloroethane 70-133 2.1 20
0.045 90.495.40.0470.050mg/KgTrichloroethene 75-133 5.3 20
0.038 76.684.20.0420.050mg/KgTrichlorofluoromethane 44-146 9.4 20
0.048 97.093.60.0460.050mg/Kg1,2,3-Trichloropropane 60-137 3.5 20
0.043 87.290.00.0450.050mg/Kg1,3,5-Trimethylbenzene 69-128 3.1 20
0.049 99.21040.0520.050mg/KgVinyl Acetate 60-140 5.1 20
0.040 80.286.60.0430.050mg/KgVinyl Chloride 48-147 7.6 20
0.045 90.494.00.0470.050mg/Kgo-Xylene 74-126 3.9 20
0.090 90.695.40.0950.100mg/Kgm,p-Xylene 75-124 5.1 20
99.295.04-Bromofluorobenzene (S)70-130
103101Dibromofluoromethane (S)84-123
96.696.4Toluene-d8 (S)76-129
Page 9 of 20Date:10/24/2022 02:48 PM
Page 48 of 61
Quality Control Data
22-277-0037Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25161QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V24969
Associated Lab Samples: 89885, 89886, 89887, 89888
LRB-V24969 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/16/22 15:150.6600.116<0.116mg/KgAcenaphthene
10/16/22 15:150.6600.105<0.105mg/KgAcenaphthylene
10/16/22 15:150.6600.152<0.152mg/KgAniline
10/16/22 15:150.6600.143<0.143mg/KgAnthracene
10/16/22 15:150.6600.139<0.139mg/KgBenzo(a)anthracene
10/16/22 15:150.6600.147<0.147mg/KgBenzo(a)pyrene
10/16/22 15:150.6600.146<0.146mg/KgBenzo(b)fluoranthene
10/16/22 15:150.6600.136<0.136mg/KgBenzo(g,h,i)perylene
10/16/22 15:150.6600.137<0.137mg/KgBenzo(k)fluoranthene
10/16/22 15:152.000.580<0.580mg/KgBenzoic Acid
10/16/22 15:150.6600.105<0.105mg/KgBenzyl alcohol
10/16/22 15:150.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
10/16/22 15:150.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
10/16/22 15:150.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
10/16/22 15:150.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
10/16/22 15:150.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
10/16/22 15:150.3300.113<0.113mg/KgButyl benzyl phthalate
10/16/22 15:150.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
10/16/22 15:150.3300.112<0.112mg/Kg4-Chloroaniline
10/16/22 15:150.6600.116<0.116mg/Kg2-Chloronaphthalene
10/16/22 15:150.6600.098<0.098mg/Kg2-Chlorophenol
10/16/22 15:151.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
10/16/22 15:150.6600.142<0.142mg/KgChrysene
10/16/22 15:150.6600.230<0.230mg/KgDibenz(a,h)anthracene
10/16/22 15:150.6600.119<0.119mg/KgDibenzofuran
10/16/22 15:150.6600.094<0.094mg/Kg1,2-Dichlorobenzene
10/16/22 15:150.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 10 of 20Date:10/24/2022 02:48 PM
Page 49 of 61
Quality Control Data
22-277-0037Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25161QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V24969
Associated Lab Samples: 89885, 89886, 89887, 89888
LRB-V24969 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/16/22 15:150.3300.097<0.097mg/Kg1,4-Dichlorobenzene
10/16/22 15:150.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
10/16/22 15:150.6600.095<0.095mg/Kg2,4-Dichlorophenol
10/16/22 15:150.6600.180<0.180mg/KgDiethyl phthalate
10/16/22 15:150.6600.174<0.174mg/KgDimethyl phthalate
10/16/22 15:150.3300.108<0.108mg/Kg2,4-Dimethylphenol
10/16/22 15:150.6600.107<0.107mg/KgDi-n-butyl phthalate
10/16/22 15:151.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
10/16/22 15:151.500.520<0.520mg/Kg2,4-Dinitrophenol
10/16/22 15:150.6600.096<0.096mg/Kg2,4-Dinitrotoluene
10/16/22 15:150.6600.108<0.108mg/Kg2,6-Dinitrotoluene
10/16/22 15:150.3300.143<0.143mg/KgDi-n-Octyl Phthalate
10/16/22 15:150.6600.123<0.123mg/KgFluoranthene
10/16/22 15:150.6600.128<0.128mg/KgFluorene
10/16/22 15:150.6600.106<0.106mg/KgHexachlorobenzene
10/16/22 15:150.6600.097<0.097mg/KgHexachlorobutadiene
10/16/22 15:150.6600.157<0.157mg/KgHexachlorocyclopentadiene
10/16/22 15:150.6600.079<0.079mg/KgHexachloroethane
10/16/22 15:150.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
10/16/22 15:150.6600.191<0.191mg/KgIsophorone
10/16/22 15:150.6600.106<0.106mg/Kg1-Methylnaphthalene
10/16/22 15:150.6600.100<0.100mg/Kg2-Methylnaphthalene
10/16/22 15:150.6600.097<0.097mg/Kg2-Methylphenol
10/16/22 15:150.6600.084<0.084mg/Kg3&4 Methylphenol
10/16/22 15:150.6600.144<0.144mg/KgNaphthalene
10/16/22 15:150.6600.096<0.096mg/Kg2-Nitroaniline
10/16/22 15:150.6600.120<0.120mg/Kg3-Nitroaniline
Page 11 of 20Date:10/24/2022 02:48 PM
Page 50 of 61
Quality Control Data
22-277-0037Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25161QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V24969
Associated Lab Samples: 89885, 89886, 89887, 89888
LRB-V24969 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/16/22 15:150.3300.093<0.093mg/Kg4-Nitroaniline
10/16/22 15:150.3300.116<0.116mg/KgNitrobenzene
10/16/22 15:150.6600.088<0.088mg/Kg2-Nitrophenol
10/16/22 15:150.6600.117<0.117mg/Kg4-Nitrophenol
10/16/22 15:150.6600.263<0.263mg/KgN-Nitrosodimethylamine
10/16/22 15:150.6600.181<0.181mg/KgN-Nitrosodiphenylamine
10/16/22 15:150.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
10/16/22 15:151.000.347<0.347mg/KgPentachlorophenol
10/16/22 15:150.6600.208<0.208mg/KgPhenanthrene
10/16/22 15:150.6600.112<0.112mg/KgPhenol
10/16/22 15:150.6600.134<0.134mg/KgPyrene
10/16/22 15:150.3300.079<0.079mg/KgPyridine
10/16/22 15:150.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
10/16/22 15:150.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
10/16/22 15:150.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
10/16/22 15:152-Fluorobiphenyl (S)89.2 44-115
10/16/22 15:152-Fluorophenol (S)90.0 35-115
10/16/22 15:15Nitrobenzene-d5 (S)83.8 37-122
10/16/22 15:154-Terphenyl-d14 (S)101 54-127
10/16/22 15:152,4,6-Tribromophenol (S)92.4 39-132
10/16/22 15:15Phenol-d5 (S)89.1 34-121
LCS-V24969Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
94.01.571.67mg/KgAcenaphthene 40-123
94.01.571.67mg/KgAcenaphthylene 32-132
Page 12 of 20Date:10/24/2022 02:48 PM
Page 51 of 61
Quality Control Data
22-277-0037Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25161QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V24969
LCS-V24969Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1762.941.67mg/KgAniline 12-197
83.81.401.67mg/KgAnthracene 47-123
88.61.481.67mg/KgBenzo(a)anthracene 49-126
1041.731.67mg/KgBenzo(a)pyrene 45-129
1051.761.67mg/KgBenzo(b)fluoranthene 45-132
70.61.181.67mg/KgBenzo(g,h,i)perylene 43-134
73.01.221.67mg/KgBenzo(k)fluoranthene 47-132
55.20.9231.67mg/KgBenzoic Acid 10-83
98.21.641.67mg/KgBenzyl alcohol 29-122
85.61.431.67mg/KgBis(2-Chloroethoxy)methane 36-121
83.21.391.67mg/KgBis(2-Chloroethyl)ether 31-120
91.61.531.67mg/KgBis(2-Chloroisopropyl)ether 33-131
1111.851.67mg/KgBis(2-ethylhexyl)phthalate 51-133
97.61.631.67mg/Kg4-Bromophenyl phenyl ether 46-124
1091.821.67mg/KgButyl benzyl phthalate 48-132
86.81.451.67mg/Kg4-Chloro-3-methylphenol 45-122
76.01.271.67mg/Kg4-Chloroaniline 17-106
92.21.541.67mg/Kg2-Chloronaphthalene 41-114
94.01.571.67mg/Kg2-Chlorophenol 34-121
95.21.591.67mg/Kg4-Chlorophenyl phenyl ether 45-121
71.81.201.67mg/KgChrysene 50-124
85.01.421.67mg/KgDibenz(a,h)anthracene 45-134
92.81.551.67mg/KgDibenzofuran 44-120
87.41.461.67mg/Kg1,2-Dichlorobenzene 33-117
83.81.401.67mg/Kg1,3-Dichlorobenzene 30-115
82.61.381.67mg/Kg1,4-Dichlorobenzene 31-115
76.01.271.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 13 of 20Date:10/24/2022 02:48 PM
Page 52 of 61
Quality Control Data
22-277-0037Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25161QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V24969
LCS-V24969Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
85.01.421.67mg/Kg2,4-Dichlorophenol 40-122
1011.681.67mg/KgDiethyl phthalate 50-124
97.61.631.67mg/KgDimethyl phthalate 48-124
88.01.471.67mg/Kg2,4-Dimethylphenol 30-127
1131.881.67mg/KgDi-n-butyl phthalate 51-128
91.61.531.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
95.21.591.67mg/Kg2,4-Dinitrophenol 27-129
1041.731.67mg/Kg2,4-Dinitrotoluene 48-126
1061.771.67mg/Kg2,6-Dinitrotoluene 46-124
1081.801.67mg/KgDi-n-Octyl Phthalate 45-140
99.41.661.67mg/KgFluoranthene 50-127
95.21.591.67mg/KgFluorene 43-125
74.81.251.67mg/KgHexachlorobenzene 45-122
80.21.341.67mg/KgHexachlorobutadiene 32-123
74.21.241.67mg/KgHexachlorocyclopentadiene 32-117
80.21.341.67mg/KgHexachloroethane 28-117
91.61.531.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
74.21.241.67mg/KgIsophorone 30-122
80.21.341.67mg/Kg1-Methylnaphthalene 40-119
77.81.301.67mg/Kg2-Methylnaphthalene 38-122
91.01.521.67mg/Kg2-Methylphenol 32-122
85.01.421.67mg/Kg3&4 Methylphenol 34-119
79.61.331.67mg/KgNaphthalene 35-123
96.41.611.67mg/Kg2-Nitroaniline 44-127
91.61.531.67mg/Kg3-Nitroaniline 33-119
1011.691.67mg/Kg4-Nitroaniline 63-147
82.01.371.67mg/KgNitrobenzene 34-122
Page 14 of 20Date:10/24/2022 02:48 PM
Page 53 of 61
Quality Control Data
22-277-0037Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25161QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V24969
LCS-V24969Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
79.01.321.67mg/Kg2-Nitrophenol 36-123
1011.691.67mg/Kg4-Nitrophenol 30-132
77.81.301.67mg/KgN-Nitrosodimethylamine 10-146
1161.931.67mg/KgN-Nitrosodiphenylamine 38-127
89.81.501.67mg/KgN-Nitroso-di-n-propylamine 36-120
1121.871.67mg/KgPentachlorophenol 25-133
97.61.631.67mg/KgPhenanthrene 50-121
92.81.551.67mg/KgPhenol 34-121
1031.721.67mg/KgPyrene 47-127
57.30.9581.67mg/KgPyridine 10-80
77.81.301.67mg/Kg1,2,4-Trichlorobenzene 34-118
92.81.551.67mg/Kg2,4,5-Trichlorophenol 41-124
94.61.581.67mg/Kg2,4,6-Trichlorophenol 39-126
95.22-Fluorobiphenyl (S)44-115
94.82-Fluorophenol (S)35-115
80.2Nitrobenzene-d5 (S)37-122
1044-Terphenyl-d14 (S)54-127
1002,4,6-Tribromophenol (S)39-132
92.1Phenol-d5 (S)34-121
V 89827-MS-V24969 V 89827-MSD-V24969Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.63 97.61.551.661.67<0.116mg/KgAcenaphthene 93.3 40-123 5.0 20
1.66 99.41.581.661.67<0.105mg/KgAcenaphthylene 95.1 32-132 4.9 20
2.97 1782.501.661.67<0.152mg/KgAniline 151 12-197 17.1 20
Page 15 of 20Date:10/24/2022 02:48 PM
Page 54 of 61
Quality Control Data
22-277-0037Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25161QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V24969
V 89827-MS-V24969 V 89827-MSD-V24969Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.69 1011.651.661.67<0.143mg/KgAnthracene 99.3 47-123 2.3 20
1.65 98.81.611.661.67<0.139mg/KgBenzo(a)anthracene 96.9 49-126 2.4 20
2.04 1221.901.661.67<0.147mg/KgBenzo(a)pyrene 114 45-129 7.1 20
1.85 1111.691.661.67<0.146mg/KgBenzo(b)fluoranthene 102 45-132 9.0 20
1.86 1111.701.661.67<0.136mg/KgBenzo(g,h,i)perylene 102 43-134 8.9 20
1.71 1021.601.661.67<0.137mg/KgBenzo(k)fluoranthene 96.3 47-132 6.6 20
2.34 140*2.081.661.67<0.580mg/KgBenzoic Acid 125*10-83 11.7 20
1.73 1041.541.661.67<0.105mg/KgBenzyl alcohol 92.7 29-122 11.6 20
1.36 81.41.351.661.67<0.118mg/KgBis(2-Chloroethoxy)methane 81.3 36-121 0.7 20
1.28 76.61.331.661.67<0.107mg/KgBis(2-Chloroethyl)ether 80.1 31-120 3.8 20
1.51 90.41.401.661.67<0.136mg/KgBis(2-Chloroisopropyl)ether 84.3 33-131 7.5 20
2.10 1262.021.661.67<0.120mg/KgBis(2-ethylhexyl)phthalate 122 51-133 3.8 20
1.71 1021.621.661.67<0.109mg/Kg4-Bromophenyl phenyl ether 97.5 46-124 5.4 20
1.91 1141.871.661.67<0.113mg/KgButyl benzyl phthalate 113 48-132 2.1 20
1.48 88.61.371.661.67<0.092mg/Kg4-Chloro-3-methylphenol 82.5 45-122 7.7 20
1.30 77.81.251.661.67<0.112mg/Kg4-Chloroaniline 75.3 17-106 3.9 20
1.65 98.81.551.661.67<0.116mg/Kg2-Chloronaphthalene 93.3 41-114 6.2 20
1.30 77.81.291.661.67<0.098mg/Kg2-Chlorophenol 77.7 34-121 0.7 20
1.62 97.01.561.661.67<0.126mg/Kg4-Chlorophenyl phenyl ether 93.9 45-121 3.7 20
1.71 1021.671.661.67<0.142mg/KgChrysene 101 50-124 2.3 20
1.45 86.81.351.661.67<0.230mg/KgDibenz(a,h)anthracene 81.3 45-134 7.1 20
1.62 97.01.581.661.67<0.119mg/KgDibenzofuran 95.1 44-120 2.5 20
1.42 85.01.161.661.67<0.094mg/Kg1,2-Dichlorobenzene 69.8 33-117 20.1*20
1.40 83.81.271.661.67<0.097mg/Kg1,3-Dichlorobenzene 76.5 30-115 9.7 20
1.35 80.81.201.661.67<0.097mg/Kg1,4-Dichlorobenzene 72.2 31-115 11.7 20
1.27 76.01.211.661.67<0.147mg/Kg3,3'-Dichlorobenzidine 72.8 22-121 4.8 20
Page 16 of 20* QC Fail Date:10/24/2022 02:48 PM
Page 55 of 61
Quality Control Data
22-277-0037Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25161QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V24969
V 89827-MS-V24969 V 89827-MSD-V24969Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.14 68.21.181.661.67<0.095mg/Kg2,4-Dichlorophenol 71.0 40-122 3.4 20
1.72 1031.681.661.67<0.180mg/KgDiethyl phthalate 101 50-124 2.3 20
1.67 1001.591.661.67<0.174mg/KgDimethyl phthalate 95.7 48-124 4.9 30
1.52 91.01.401.661.67<0.108mg/Kg2,4-Dimethylphenol 84.3 30-127 8.2 20
1.93 1161.851.661.67<0.107mg/KgDi-n-butyl phthalate 111 51-128 4.2 20
1.19 71.20.9841.661.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 59.2 29-132 18.9 20
0.993 59.40.7811.661.67<0.520mg/Kg2,4-Dinitrophenol 47.0 27-129 23.9*20
1.73 1041.741.661.67<0.096mg/Kg2,4-Dinitrotoluene 105 48-126 0.5 20
1.80 1081.771.661.67<0.108mg/Kg2,6-Dinitrotoluene 107 46-124 1.6 20
2.05 1231.911.661.67<0.143mg/KgDi-n-Octyl Phthalate 115 45-140 7.0 20
1.72 1031.621.661.67<0.123mg/KgFluoranthene 97.5 50-127 5.9 20
1.67 1001.611.661.67<0.128mg/KgFluorene 96.9 43-125 3.6 20
1.68 1011.621.661.67<0.106mg/KgHexachlorobenzene 97.5 45-122 3.6 20
1.33 79.61.271.661.67<0.097mg/KgHexachlorobutadiene 76.5 32-123 4.6 20
<0.157 0.0*<0.1571.661.67<0.157mg/KgHexachlorocyclopentadiene 0.0*32-117 0.0 20
1.18 70.60.9701.661.67<0.079mg/KgHexachloroethane 58.4 28-117 19.5 20
1.80 1081.701.661.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 102 45-133 5.7 20
1.36 81.41.251.661.67<0.191mg/KgIsophorone 75.3 30-122 8.4 20
1.39 83.21.291.661.67<0.106mg/Kg1-Methylnaphthalene 77.7 40-119 7.4 20
1.33 79.61.251.661.67<0.100mg/Kg2-Methylnaphthalene 75.3 38-122 6.2 20
1.55 92.81.431.661.67<0.097mg/Kg2-Methylphenol 86.1 32-122 8.0 20
1.40 83.81.251.661.67<0.084mg/Kg3&4 Methylphenol 75.3 34-119 11.3 20
1.35 80.81.181.661.67<0.144mg/KgNaphthalene 71.0 35-123 13.4 20
1.74 1041.651.661.67<0.096mg/Kg2-Nitroaniline 99.3 44-127 5.3 20
1.65 98.81.651.661.67<0.120mg/Kg3-Nitroaniline 99.3 33-119 0.0 20
1.73 1041.701.661.67<0.093mg/Kg4-Nitroaniline 102 63-147 1.7 20
Page 17 of 20* QC Fail Date:10/24/2022 02:48 PM
Page 56 of 61
Quality Control Data
22-277-0037Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25161QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V24969
V 89827-MS-V24969 V 89827-MSD-V24969Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.38 82.61.241.661.67<0.116mg/KgNitrobenzene 74.6 34-122 10.6 20
0.972 58.20.7911.661.67<0.088mg/Kg2-Nitrophenol 47.6 32-123 20.5*20
0.976 58.40.7691.661.67<0.117mg/Kg4-Nitrophenol 46.3 30-132 23.7*20
1.24 74.21.111.661.67<0.263mg/KgN-Nitrosodimethylamine 66.8 10-146 11.0 30
2.13 128*1.961.661.67<0.181mg/KgN-Nitrosodiphenylamine 118 38-127 8.3 20
1.54 92.21.401.661.67<0.118mg/KgN-Nitroso-di-n-propylamine 84.3 36-120 9.5 20
1.44 86.21.441.661.67<0.347mg/KgPentachlorophenol 86.7 25-133 0.0 20
1.71 1021.611.661.67<0.208mg/KgPhenanthrene 96.9 50-121 6.0 20
1.56 93.41.461.661.67<0.112mg/KgPhenol 87.9 34-121 6.6 20
1.68 1011.711.661.67<0.134mg/KgPyrene 103 47-127 1.7 20
0.899 53.80.7941.661.67<0.079mg/KgPyridine 47.8 10-80 12.4 20
1.31 78.41.241.661.67<0.107mg/Kg1,2,4-Trichlorobenzene 74.6 34-118 5.4 20
1.40 83.81.381.661.67<0.096mg/Kg2,4,5-Trichlorophenol 83.1 41-124 1.4 20
1.32 79.01.251.661.67<0.096mg/Kg2,4,6-Trichlorophenol 75.3 39-126 5.4 20
98.22-Fluorobiphenyl (S)93.3 44-115
79.52-Fluorophenol (S)70.5 35-115
80.2Nitrobenzene-d5 (S)68.6 37-122
1024-Terphenyl-d14 (S)100 54-127
82.52,4,6-Tribromophenol (S)76.5 39-132
90.6Phenol-d5 (S)81.6 34-121
Page 18 of 20* QC Fail Date:10/24/2022 02:48 PM
Page 57 of 61
Quality Control Data
22-277-0037Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Hexavalent Chromium by Ion Chromatography
SW-7199
L642479QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3060A
QC Prep:L641944
Associated Lab Samples: 89885, 89886, 89887, 89888
LRB-L641944 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
10/11/22 14:340.2000.141<0.141mg/KgChromium, Hexavalent
LCS-L641944Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1124.494.00mg/KgChromium, Hexavalent 80-120
V 89885-DUP-L641944Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20 10/11/22 15:076.90.4470.417mg/KgChromium, Hexavalent
V 89885-MS-L641944 V 89885-MSD-L641944Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec
42.5 10954765538.7<0.681mg/KgChromium, Hexavalent 83.5 75-125
Page 19 of 20Date:10/24/2022 02:48 PM
Page 58 of 61
Quality Control Data
22-277-0037Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
Dry Weight Determination
SW-DRYWT
V24815QC Analytical Batch:
Analysis Method:
Analysis Description:
V 89830-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 10/07/22 09:534.122.321.4%Moisture
Page 20 of 20Date:10/24/2022 02:48 PM
Page 59 of 61
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-277-0037
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 21.5C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:10/04/2022 18:16:33
Special precautions or instructions included?
Comments:
Page 60 of 61
Page 61 of 61

Appendix C DEQ Approval Letter

Appendix D Reeves LCID Export Tickets