26019_Report of Environmental Assessment_20211124 (sealed 20230705)

EySC ECS
SOUTHEAST, `'Setting Me ,Standard for Servic, e"
Geoteohnical . Construction Materials • Environmental l - Facilities Nc Registered Engmeenng Firm F-1.07d
NC Registered Geologists Firm G-553
SC Registered Engineering Firm 3233
Ms. Stephanie Graham
NCDEQ Division of Waste Management
Brownfields Redevelopment Section
Stephanie.Graham deg nc gov
Reference: Report of Environmental Assessment
W. Carson Blvd. & S. Tryon Street Site
1102,1106 and 1018 South Tryon Street
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:10606-D
Ms. Graham:
July 5, 2023
On behalf of our client, Crescent Acquisitions, LLC (now working as CC TREA Carson Station, LLC), ECS has
prepared this sealed cover letter for the above -referenced report, dated November 25, 2021. As such, I
Christopher D. Orrell, a Licensed Geologist for ECS Southeast, LLP, do certify that the information
contained in the referenced report is correct and accurate to the best of my knowledge, and at the time
of the completion of the report.
Respectfully,
ECS ,S FR A it *,as represented by:
4p�GENs�4
�a''
704-
Roger A. S , P.G.
Principal Geologist
[e-mail]
704-525-5152
7-5 Q'�
cc: Ms. Fran West, CC TREA Carson Station, LLC @ [e-mail]
ECS Capitol Services, PLLC . ECS Florida, LLC ECS Mid Atlantic, LLC • ECS Midwest, LLC ECS Southeast, LLP , ECS souttttivest„ LLP
www.ecsiimiited.com

C
ECS SOUTHEAST, LLP
"Setting the Standard for Service"
Geotechnical • Construction Materials • Environmental • Facilities
November 24, 2021
Mr. Blake Bickmore
Crescent Acquisitions, LLC
201 North Tryon Street, Suite 3000
Charlotte, North Carolina 28202
Reference: Proposal for Environmental Assessment
W. Carson Blvd. & S. Tryon Street Site
1102, 1106, and 1018 South Tryon Street
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:10606-D
Dear Mr. Bickmore:
As authorized by your acceptance of ECS Proposal No. 49-27281P dated and approved on October 13,
2021, ECS Southeast, LLP (ECS) has completed the attached Report of Environmental Assessment for the
above -referenced site. Included in this report is a description of the field activities, observations made,
soil, groundwater, and soil gas laboratory analytical results, as well as ECS' conclusions and
recommendations.
We appreciate the opportunity to provide our services to you. If there are questions regarding this report,
please do not hesitate to contact us.
Respectfully submitted,
r
4ristopher D. Orrell, P.G.
Environmental Project Manager
[e-mail]
704-200-3436
Pxt�tv-
.Joseph P. Nestor, P.G., P.E.
Environmental Principal
[e-mail]
704-525-5152
Mackie McMahan
Environmental Scientist
[e-mail]
704-525-5152
1812 Center Park Drive, Suite D, Charlotte, NC 28217 • T. 704-525-5152 • www.ecs[imited.com
ECS Capitol Services, PLLC • ECS Florida, LLC • ECS Mid -Atlantic, LLC • ECS Midwest, LLC • ECS Southeast, LLP • ECS Southwest, LLP
NC Engineering No. F-1078 • NC Geology No. C-553 • SC Engineering No. 3239

Report of Environmental Assessment
W. Carson Blvd. & S. Tryon Street Site
ECS Project: 49:10606-D
November 24, 2021
TABLE OF CONTENTS
1.0
BACKGROUND INFORMATION..........................................................................................................1
2.0
FIELD ACTIVITIES...............................................................................................................................1
3.0
RESULTS.............................................................................................................................................4
4.0
CONCLUSIONS...................................................................................................................................5
5.0
RECOMMENDATIONS........................................................................................................................6
6.0
QUALIFICATIONS OF REPORT............................................................................................................6
FIGURES
Figure 1: Topographic Location Map
Figure 2: Sample Location Map
TABLES
Table 1: Summary of Soil Analytical Results
Table 2: Summary of Groundwater Analytical Results
Table 3: Summary of Soil Gas Analytical Results
APPENDICES
Appendix A: NCDEQ Monitoring Well Permit, Mecklenburg County SIP, & Well Construction Records
Appendix B: Soil and Groundwater Analytical Laboratory Reports with COC Documentation
Appendix C: Soil Gas Analytical Laboratory Reports with COC Documentation
Appendix D: NCDEQ Risk Calculator Output Sheets

Report of Environmental Assessment
W. Carson Blvd. & S. Tryon Street Site
ECS Project: 49:10606-D
November 24, 2021
1.0 BACKGROUND INFORMATION
The site consists of a 2.77-acre tract that is identified by the Mecklenburg County GIS as Parcel
Identification Numbers (PINs) 07305302, 07305303, 07305304, and 07305305 and owned by 1102 South
Tryon LLC, Global Investors LLC, Carson Systems LLC c/o Von Patel, and Winnifred Systems LLC,
respectively. The site is located at 1102, 1106, and 1018 South Tryon Street in Charlotte, North Carolina
and contains a two-story 2,244-square foot office building and a parking lot (Figure 1). A Phase I
Environmental Site Assessment (ESA) was previously completed by ECS Southeast, LLP (ECS) on December
11, 2019 (ECS Project No. 49-10606). The findings of the Phase I ESA identified the following Recognized
Environmental Conditions (RECs):
• ECS considers the documented concentrations of benzene, 1,2-dichloroethane (DCA), tert-butyl
alcohol (TBA), naphthalene, xylenes (total), and 1-Methylnaphthalene identified in a groundwater
sample collected approximately 145 feet from the subject property that exceeded their respective
North Carolina Groundwater Standard (NCGWS) or Interim Maximum Allowable Concentration
(IMACs) to be a REC. This groundwater sample was collected on a west adjoining property which
is a Brownfields Site located at 1100 and 1200 South Tryon Street (Former Gathings Motor
Company).
• ECS considers the documented soil impacts approximately 25 feet from the subject property from
a former underground storage tank (UST) at concentrations above their respective Soil -to -
Groundwater Maximum Soil Contaminant Concentrations (MSCCs) to be a REC. This UST was
located on an east adjoining property at 107 West Morehead Street (Broadstone Morehead).
In an effort to determine if the site has been adversely affected by the identified RECs and to provide a
general assessment of the site for future redevelopment activities, ECS was requested to conduct an
Environmental Assessment at the site. The following sections document the Environmental Assessment
activities conducted, the laboratory results as compared to regulatory guidance levels, and a summary of
the findings and conclusions.
2.0 FIELD ACTIVITIES
The assessment activities were conducted by ECS on October 28 & 29, 2021. The field sampling activities
consisted of the collection of soil, groundwater, and soil gas samples for laboratory analysis. Drilling
activities were conducted using a direct push technology (DPT) drill rig, operated by a North Carolina
licensed driller with 3D Environmental Investigations, LLC, based out of Statesville, North Carolina.
Pre -Sampling Activities
Based on our understanding of the project information, ECS conducted the following pre -assessment
services:
• Prior to implementing the field activities, ECS contacted North Carolina public utility locating
service (811) to locate/mark public utilities at the site. Required separation distances between
borehole locations and marked utilities (typically 30-inches) were maintained during the field
activities.
1

Report of Environmental Assessment
W. Carson Blvd. & S. Tryon Street Site
ECS Project: 49-10606-D
November 24, 2021
• ECS contracted the private utility locator Summit Environmental Services, LLC to identify private
utilities at the subject property. The private utility locating activities were conducted using ground
penetrating radar (GPR) and other locating techniques.
• ECS also acquired a groundwater monitoring well permit from the North Carolina Department of
Environmental Quality (NCDEQ Permit # WM0301042) and Subsurface Investigation Permits (SIPs)
from Mecklenburg County Groundwater and Wastewater Services. A copy of the NCDEQ MW
Permit and Mecklenburg County SIPs are included in Appendix A.
Soil Boring Activities
During field activities conducted on October 28, 2021, six soil borings (S13-1 through S13-6) were advanced
at the site by hydraulically driving a five-foot long, 1.5-inch diameter soil sampling probe equipped with a
new disposable clear liner for each 5-foot depth interval. Prior to advancing each boring, the down -hole
equipment and DPT drill rig were decontaminated to minimize to potential for cross -contamination
between soil boring locations.
Soils were collected within the soil sampling probe continuously from the ground surface to the
termination depth at each boring. After the probe was driven and retrieved, the probe was opened, the
liner removed and cut open to expose the soil. ECS visually classified the soil collected from each boring,
noted apparent evidence of staining or odors (if present), and screened the soil for relative levels of
volatile organic vapors using a photo -ionization detector (PID).
Soil Sample Collection
On October 28, 2021, soil samples were collected by ECS personnel from soil borings S13-1 through S13-6
and were submitted to Pace Analytical Services, LLC, a North Carolina certified laboratory located in
Huntersville, North Carolina for laboratory analysis. Sampling personnel changed powder -free nitrile gloves
prior to and in between each sample location to reduce chances of cross contamination between the samples.
Each of the soil borings were advanced to a depth of 15 feet below ground surface (ft bgs), except soil
boring S13-2 which was advanced to a depth of 11 ft bgs due to drilling refusal. The soils selected for
laboratory analysis were selected based on field screening results and collected directly into laboratory
supplied/preserved containers following field screening with a PID. The approximate location of these
borings is shown on Figure 2.
The soil sample containers were labeled with ECS project number, sample identification, sample date and
time, and requested analytical analysis. The containers were placed into protective packaging material
and placed into a cooler with ice to maintain the samples at approximately 4° Celsius (C°). The soil samples
were submitted to Pace for analysis of volatile organic compounds (VOCs) using the EPA Method 8260,
semi -volatile organic compounds (SVOCs) using EPA Method 8270; and Resource Conservation and
Recovery Act (RCRA) Metals plus hexavalent chromium using 6010, 7471, and 7199 methods. ECS
maintained chain of custody (COC) procedures throughout the sample collection and transportation process.
A copy of the analytical laboratory report along with accompanying COC documentation is included in
Appendix B.
Groundwater Sample Collection
Groundwater sampling activities were conducted on October 28, 2021. Two borings (GW-3 and GW-4)
were advanced along the western property boundary. These borings were advanced to depths of 29 ft

Report of Environmental Assessment
W. Carson Blvd. & S. Tryon Street Site
ECS Project: 49-10606-D
November 24, 2021
bgs and 33 ft bgs, respectively. Following the collection of the soil samples from soil borings S13-1 and SB-
3, the borings were advanced to a depth of 29ft bgs and 25ft bgs, respectively, in order to collect
groundwater samples GW-1 and GW-2, respectively. Groundwater sampling was conducted using a
groundwater sampling probe equipped with an exposable stainless -steel screen and a peristaltic pump
and dedicated tubing at each location.
Sampling personnel changed powder -free nitrile gloves prior to and in between each sample location to
reduce chances of cross contamination between the samples. The groundwater samples were placed directly
into laboratory supplied/preserved sample containers, and labeled with ECS project number, sample
identification, sample date and time, and requested analytical analysis. The containers were placed into
protective packaging material and placed into a cooler with ice to maintain the samples at approximately
4°C. The groundwater samples were submitted to Pace for analysis for VOCs using EPA Method 8260, and
SVOCs using EPA Method 8270. ECS maintained COC procedures throughout the sample collection and
transportation process. A copy of the COC is included in Appendix B.
Soil Gas Sample Collection
ECS observed the installation of four soil gas points (SG-1 through SG-4) at the subject property, as shown in
the attached Figure 2.
The soil gas sample points were constructed by advancing a boring to a depth of five feet below ground
surface (bgs) using a DPT drill rig. A vapor implant connected to a length of Nylaflow tubing was positioned in
near the base of each boring. Clean filter sand was placed in the annular space around, and approximately 6
inches above, the vapor implant and bentonite was placed in the remaining annular space. Distilled water
was poured into the bentonite and allowed to hydrate for at least 30 minutes before sampling was
performed.
Prior to collecting the soil gas samples, a sample train consisting of non -reactive tubing and microvalves was
connected to the Nylaflow tubing at each sample point and to a Summa canister. The sample train was used
to purge the sample lines and direct flow to the Summa canister being used to collect the sample at each
point. A shut-in test was performed on the sample train at each sample point to confirm that leaks were not
present in the sampling train. A micro -valve at the connection between the sampling train and the Nylaflow
tubing was closed, and a vacuum was applied to the sampling train using a disposable syringe. The vacuum
gauge on the Summa canister was monitored for declining vacuum indicative of a leak during the shut-in test.
If a leak was indicated, steps were taken to obtain eliminate the leak prior to sampling.
Following the sample train construction and shut-in testing and prior to collecting the soil gas samples, a
helium shroud leak test was performed at each of the sample points to confirm the integrity of the subsurface
bentonite seal. The shroud was placed and sealed over the sampling point. The vapor implant sample tubing
and tracer gas tubing was routed through small diameter holes in the wall of the shroud. The shroud was
flooded with helium from a compressed gas tank through tracer gas tubing routed through the shroud wall.
The helium gas concentration inside the shroud was measured with a helium gas detector. After the shroud
was flooded with helium, a soil gas sample was extracted and measured with the helium detector. If the
concentration of helium in the soil gas sample was less than ten percent of the helium concentration inside
the shroud, the seal was considered tight and not leaking. Leaks were not noted during leak testing in the
sample points.
3

Report of Environmental Assessment
W. Carson Blvd. & S. Tryon Street Site
ECS Project: 49-10606-D
November 24, 2021
Following successful shut-in and helium shroud tests, ECS collected a soil gas sample from each sample point.
ECS collected the soil gas samples in 3-liter Summa canisters from Con -Test Analytical Laboratory (Con -Test),
located in East Longmeadow, Massachusetts, a commercial laboratory that follows National Environmental
Laboratory Accreditation Conference (NELAC) standards. Each canister was pre -cleaned and pre -evacuated
so that it is under negative pressure (i.e., under vacuum). The canisters were batch certified by the laboratory.
Each Summa canister was outfitted with a flow regulator set to 100 milliliters per minute and a vacuum gauge.
ECS opened the valve on the Summa canister and soil gas flowed into the canister. ECS noted the time the
valve was opened and the initial vacuum. When the vacuum decreased to approximately 5 inches of mercury,
ECS shut the valve and recorded the time and final vacuum pressure.
Following sample collection, the canisters were labeled and shipped to Con -Test to be analyzed for VOCs
using EPA Method TO-15. ECS followed chain -of -custody procedures throughout the sample collection and
transportation process. A copy of the chain -of -custody form is included in Appendix C.
3.0 RESULTS
Soil Sampling Results
The soil detections were compared to NCDEQ Preliminary Soil Remediation Goals (PSRGs) for Protection
of Groundwater and Residential, and Industrial/Commercial uses. Review of the laboratory analytical
results for each of the soil samples collected indicated arsenic at concentrations greater than their
respective Residential PSRGs. Additionally, concentrations of arsenic reported in soil sample SB-5 were
greater than the respective Industrial/Commercial PSRG.
Review of the laboratory analytical results for soil samples SB-1 through SB-3, SB-5, and SB-6 also indicated
hexavalent chromium at concentrations greater than their respective Residential PSRGs. Laboratory
analytical results for soil sample SB-1 also indicated lead at concentrations greater than the Protection of
Groundwater and Residential PSRGs. Soil analytical results have been summarized in the attached Table
1. A copy of the laboratory analytical report is included in Appendix B.
Groundwater Sampling Results
The groundwater detections were compared to their respective NCGWS and NCDEQ Residential and Non -
Residential Groundwater Vapor Intrusion Screening Levels (VISLs). Review of the laboratory analytical
results for groundwater samples GW-1, GW-2, and GW-4 did not indicate concentrations of target
analytes above laboratory reporting limits. Review of the laboratory analytical results forthe groundwater
sample collected at GW-3 indicated concentrations of benzene and 1,2-dichloroethane above their
respective NCGWS and both the Residential and Non -Residential Groundwater VISLs. In addition,
chloroform was detected at concentrations greater than both the Residential and Non -Residential
Groundwater VISLs. Groundwater analytical results have been summarized in the attached Table 2. A copy
of the laboratory analytical report is included in Appendix B.
Based on the results of the groundwater sample collected from GW-3, ECS input the results into a NCDEQ
Risk Calculator to determine if a vapor intrusion risk was present based on the groundwater analytical
results. The results of the NCDEQ Risk Calculator did not indicate a risk exceedance for Residential or Non -
Residential use. The NCDEQ Rick Calculator output sheet for GW-3 is included as Appendix D.
4

Report of Environmental Assessment
W. Carson Blvd. & S. Tryon Street Site
ECS Project: 49-10606-D
November 24, 2021
Soil Gas Sampling Results
The soil gas detections were compared to the North Carolina Residential and Non -Residential Vapor
Intrusion Screening Levels (VISLs). Review of the laboratory analytical results for the soil gas samples
indicated multiple compounds above laboratory reporting limits but below respective VISLs with the
exception of soil gas sample SG-4. Review of the laboratory analytical results for soil gas sample SG-4
indicated 1,3-butadiene at a concentration greater than its Residential VISL. Soil gas analytical results have
been summarized in the attached Table 3. A copy of the laboratory analytical report is included in
Appendix C.
Based on the results of the soil gas sample SG-4, ECS input the results into the NCDEQ Risk Calculator to
determine if a vapor intrusion risk was present based on the soil gas analytical results. The results of the
NCDEQ Risk Calculator did not indicate a risk exceedance for Residential or Non -Residential use. The
NCDEQ Rick Calculator output sheet for SG-4 is included as Appendix D.
4.0 CONCLUSIONS
Based on the field screening observations and laboratory analytical results of the soil, groundwater, and
soil gas samples collected during this assessment, ECS concludes the following:
• The detected concentration of arsenic exceeded its residential PSRG in each of the six soil samples
and its industrial/commercial PSRG in one of the six soil samples (SB-5). The detected
concentrations are within the expected range of naturally occurring arsenic in this region.
• The detected concentration of hexavalent chromium exceeded its residential PSRG in each of the
six soil samples.
• The detected concentration of lead exceeded its protection of groundwater and residential PSRG
in one of the six soil samples (SB-1).
• Based on the results of the soil samples collected at the site, special handling of site soil may be
required during site redevelopment activities. Additional sample analysis may be required for soil
export purposes due to the elevated concentrations of lead.
• The detected concentrations of benzene and 1,2-dichloroethane exceeded NCGWS in one of four
groundwater samples (GW-3).
• The detected concentrations of benzene, chloroform, and 1,2-dichloroethane exceeded both
Residential and Non -Residential Groundwater VISLs in one of four groundwater samples (GW-4).
• The results of the NCDEQ Risk Calculator did not indicate a risk exceedance for Residential or Non -
Residential use when the data for groundwater sample GW-4 was entered.
• The detected concentration of 1,3-butadiene exceeded its Residential VISL in one of four soil gas
samples (SB-1).
• The results of the NCDEQ Risk Calculator did not indicate a risk exceedance for Residential or Non -
Residential use when the data for soil gas sample GW-4 was entered.
5

Report of Environmental Assessment
W. Carson Blvd. & S. Tryon Street Site
ECS Project: 49-10606-D
November 24, 2021
5.0 RECOMMENDATIONS
Based on the conclusions of this Environmental Services Report, ECS recommends the following:
• Based on the results of this assessment, ECS understands that a potential reporting obligation may exist
due to the exceedances of the various state standards. ECS recommends that a copy of this report be
provided to the property owner and that they consult legal counsel regarding potential reporting
obligations.
• ECS recommends that the client maintain a copy of this report for its records.
• ECS recommends if the client intends to pursue a Brownfields Agreement that a Brownfields application
and a copy of this report be submitted by the client and/or their attorney to the NCDEQ Brownfields
Program for their review.
6.0 QUALIFICATIONS OF REPORT
The activities and evaluative approaches used in this assessment are consistent with those normally
employed in soil, groundwater, and soil gas assessment projects of this type. Our evaluation of site
conditions has been based on our understanding of the site project information and the data obtained
during our previous assessment and field activities and findings. Environmental sampling performed and
reported herein only provides for specific data points scattered throughout the project area in accordance
with the prior approved scope of work and work authorization. It is not meant to provide a comprehensive
environmental assessment of the entire subject property parcel(s).
A

FIGURES

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FIGURE 1
TOPOGRAPHIC LOCATION MAP
SOURCE:
ECS Phase I Dated December 11, 2019 W. Carson Blvd & S. Tryon Street Site
1102, 1106, & 1018 South Tryon Street
SCALE: Charlotte, Mecklenburg County, North Carolina
AS SHOWN
ECS Project No. 49:10606-D
TM

do t
I _
40
■
t
SB-1/GW-1
097-
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SG-4 ® SB-6
•
SG-3
GW-4 94
SB-2
■
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im
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SG-1
SB-3/GW-2
1
SG-2
SB-4
SB-5
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® LEGEND
APPROXIMATE GROUNDWATER SAMPLE LOCATION • N
APPROXIMATE SOIL& GROUNDWATER SAMPLE LOCATION L
APPROXIMATE SOIL GAS SAMPLE LOCATION
® APPROXIMATE SOIL SAMPLE LOCATION
APPROXIMATE SITE BOUNDARY
FIGURE 2
SOURCE: SAMPLE LOCATION MAP
MECKLENBURG COUNTY GIS WEBSITE
ACCESSED ON OCTOBER 14, 2021 W. Carson Blvd & S. Tryon Street Site
1102, 1106, & 1018 South Tryon Street
SCALE: E9 Charlotte, Mecklenburg County, North Carolina
AS SHOWN
TM ECS Project No. 49:10606-D
fw:
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u

TABLES

Table 1
Summary of Soil Analytical Results
W CARSON BLVD & S TRYON ST SITE
1102, 1106, & 1018 S. TRYON ST
Charlotte, Mecklenburg County, North Carolina
ECS Project No.: 49:10606-D
Parameter
ANALYTICAL RESULTS
COMPARISON CRITERIA
Sample ID
SB-1 SB-2 SB-3 SBA SB-S SB-6
Protection of
Groundwater PSRG
Residential Health
Based PSRG
Industrial/
Commercial Health
Sample Depth (ft)
0-5 5-10 10-15 10-15 10-15 0-5
Collection Date
10/28/21
Based PSRG
Volatile Organic Compounds (VOCs)
by EPA Method 8260
Benzene
<0.0029
<0.0022
<0.0035
c0.0026
<0.0034
<0.0026
0.01
11
5
4-Methyl-2-pentanone(MIBK)
<0.0084
<0.0084
<0.0084
0.0065J
<0.0082
<0.0084
0.45
7000
30,000
Ethylbemene
0.00401
<0.0026
<0.0041
<0.0030
<0.0040
<0.0032
13
6.1
27
Naphthalene
0.014
<0.0029
<0.0046
<0.0034
<0.0045
<0.0036
0.39
2.1
9
Toluene
0.0051J
<0.0016
<0.0025
<0.0019
<0.0024
0.0036J
8.3
990
9,700
1,2,4-Trimethylbenzene
0.0084
<0.0015
<0.0024
<0.0018
<0.0023
<0.0019
12
63
370
Xylene (Total)
0.00801
<0.0031
<0.0050
<0.0037
<0.0049
<0.0039
9.9
120
530
m& -X lene
0.00801
<0.0038
<0.0060
<0.0045
<0.0058
<0.0047
9.8
120
500
Semi -Volatile Organic Compounds
(SVOCs) by EPA Method
8270
For All BRL BRL BRL BRL BRL BRL
Resource Conservation and Recovery Act (RCRA) Metals & Hex Chrome by EPA Methods 6020, 7471, and 7199
Mercury
0.22
<0.0043
0.0072
<0.0038
0.044
0.D48
INS
4.7
70
Arsenic
1.81
0.80J
0.84J
2.OJ
4.9J
2.5J
5.8
0.68
3.0
Barium
190
141
42.1
42.3
267
118
580
3,100
47,000
Cadmium
0.40
0.11
0.070J
<0.054
0.32J
0.88
3.0
14
200
Total Chromium
34.7
8.2
8.1
2.8
72
60.8
INS
NS
INS
Hexavalent Chromium
1.32
3.52
0.359J
<0.302
1.32J
0.579J
3.8
0.31
6.5
Lead
465
5.9
4.1
2.7
3.8J
154
250
400
800
Selenium
1.1
0.511
<0.68
<0.54
<2.9
1.4
2.1
78
1,200
Silver
0.45J
0.59
<0.34
-0.27
<1.5
0.52J
3.4
78
1,200
Notes:
Results presented in milligrams per kilogram (mg/kg), analogous to parts per million (ppm)
Soil sample results are compared to the NCDEQ PSRGs dated January 2021
NCDEQ= North Carolina Department of Environmental Quality
PSRG = Preliminary Soil Remediation Goal
J Flag denotes an estimated concentration between the laboratory reporting limit and the laboratory detection limit
BRL= Below Reporting Limit
Bold denotes an exceedance of the Protection of Groundwater PSRG
Italics denotes an exceedance of the Residential Health Based PSRG
Underline denotes an exceedance of thelndustrial/Commercial Health Based PSRG
INS = No Standard

Table 2
Summary of Groundwater Analytical Results
W CARSON BLVD & S TRYON ST SITE
1102, 1106, & 1018 S. TRYON ST
Charlotte, Mecklenburg County, North Carolina
ECS Project No.: 49:10606-D
SVOCs by
VOCs by EPA Method 8260
EPA
Method
8270
v
s
°1
L
Sample ID
Sample Date
E
o
N
>
a)
a)
0
L
CL
2
u
C
u
L
O
C
L
C
i
Ln
co
I V
Z
NC2LGWQS
1
70
0.4
70
6
Various
Residential Groundwater VISL
1.6
0.81
2.2
1,400
4.6
Various
Non -Residential Groundwater VISL
6.9
3.6
9.8
5,900
20
Various
GW-1
10/28/21
<0.34
<0.43
<0.32
<0.31
<0.64
BRL
GW-2
10/28/21
<0.34
<0.43
<0.32
<0.31
<0.64
BRL
GW-3
10/28/21
28.5
9.3
10.3
0.32J
0.81J
BI
GW-4
10/28/21
<0.43
<0.32
<0.31
<0.64
B
Notes:
All results presented in micrograms per liter (µg/L)
Compounds not shown were not detected
VOCs = Volatile Organic Compounds
SVOCs = Semi -volatile Organic Compounds
NC2LGWQS = North Carolina 2L Groundwater Quality Standards (October 2020)
Residential Groundwater VISL= NCDEQ Residential Groundwater Vapor Instrusion Screening Level (Janaury 2021)
Non -Residential Groundwater VISL= NCDEQ Non -Residential Groundwater Vapor Instrusion Screening Level (Janaury 2021)
NE = Not established
VALUE = concentration greater than the laboratory method reporting limit
VALUE = concentration greater than the NC2LGWQS
VALUE = concentration greater than the Residential Groundwater VISL
VALUE = concentration greater than the Non -Residential Groundwater VISL

TABLE 3
SUMMARY OF SOIL GAS ANALYTICAL RESULTS
W CARSON BLVD & S TRYON ST SITE
1102, 1106, & 1018 S. TRYON ST
Charlotte, Mecklenburg County, North Carolina
ECS Project No.: 49:10606-D
Volatile
Organic
Compounds
by EPA TO-15
N
rl
O
P
Initial Sample
Final Sample
Vaccum
Vaccum
t
v
Sample ID
Sample Date
a
Reading
Reading
-°
v
a
t
(in Hg)
(in Hg)
Y
uJ
72
`O
aJ
22
`0
L
a
O
C
2=
t
aJ
tOo
M
C
aJ
O
0
aJ
C
C
a
N
v
a
-a
m
a
C
O
c
a
aJ
H
0
L
aJ
ai
O
E
E
C:
C
x
ai
w
O
O
t
L
U
N
O
7
O
+�
a1
O
a.,
CO
ro
O
O
O
O
O
`o
-a
O
`O
U
N
O
v
-2
>-
a
U
aJ
M
m
M
M
O
L
O
L
L
?
s
U
N
t-I
0
L
i
-C
W
Q
<
cc
-1
N
U
U
U
U
U
U
U
w
w
V
2
Residential VISL
220,000
120
3.1
35,000
4,900
160
NS
4.1
630
42,000
700
3.6
NS
NS
370
NS
2,800
Non -Residential VISL
2,700,000
1,600
41
440,000
61,000
2,000
NS
53
7,900
88,000
8,800
4.7
NS
NS
4,900
NS
35,000
SG-1
-29
-5
10/29/21
<11
21
<0.44
45
33
<0.38
<0.39
<0.24
<0.17
20
2.4
<G. ,.,
0.46 J
110
1.9
<0.30
13
SG-2
-28
-5
10/29/21
24
2
<0.31
3.71
<1.6
0.581
<0.39
<0.24
1.5
7.1
2.3
<0.30
<0.27
43
0.611
<0.30
2.4
SG-3
-28
-5
10/29/21
1 22
1 31
1 <0.31
1 3.3 J
29
1.6
1 2.9
1 2.5
1 3.6
1 8.4
2.1
1 <0.30
1 <0.27
67
5.7
0.90 J
24
SG-4
-28
-5
10/29/21
1 24
1 18
1 4.4
1 3.8 J
4.1 J
0.45 J
1 <0.39
1 3.8
1 0.81 J
1 16
2.2
1 1.4
1 <0.27
62
2.9
0.451
21
Volatile
Organic Compounds
by EPA
TO-15
M
c-I
O
v
v
C
Initial Sample
Final Sample
y
Vaccum
Vaccum
o
0
Sample ID
Sample Date
v
o
Reading
Reading
(in Hg)
(in Hg)
C
Y
C
C
o
N
v
v
a
-
C
aJ
aJ
aL
aj
C
aJ
C
aJ
t
C
C
N
E
O
rl
p
?
?
O
U
aj
O
?
L
L
4
aJ
cOo
v
v
O
Lj
�
�
aj
aJ
N
V
C
O
H
H
U
NC
m
aJ
O
N
N
c-
22
J
?
a+
a+
U
V
r4
c-I
V
N
Lf)
M
C
S7
T
X
Residential VISL
4,900
1,400
4,200
21,000
7,000
280
14,000
35,000
14
NS
NS
420
420
5.6
700
700
Non -Residential VISL
61,000
18,000
53,000
260,000
88,000
3,500
180,000
440,000
180
NS
NS
5,300
5,300
280
8,800
8,800
SG-1
-29
-5
10/29/21
40
8.0 J
99
13
0.49 J
3.4 J
9.6
1.1
0.45 J
<0.54
1.1
0.39 J
5.1
0.62
SG-2
-28
-5
10/29/21
4.6 J
<4.5
37
3.6
<0.40
4.3
<0.4u
1.3 J
0.83 J
<0.29
<0.27
1.7
0.69 J
SG-3
-28
-5
10/29/21
24 J
<4.5
2.2 J
69
28
1.3 J
62
<0.40
1.6 J
1.3 J
<0.29
1.1
1.8
16
5.3
SG-4
-28
-5
10/29/21
27 J
<4.5
<1.6
6.1 J
11
7.9
42
)
2.0 J
0.74 J
1.4
0.88 J
11
3.6
Notes:
Results presented in micrograms per cubic meter (µg/m3)
in Hg = Inches of mercury
Residential VISL= NCDEQ-DWM Residential Vapor Instrusion Screening Level Indoor Exterior and Sub -Slab Screening Level (June 2021)
Non -Residential VISL= NCDEQ-DWM Non -Residential Vapor Instrusion Screening Level Indoor Exterior and Sub -Slab Screening Level (June 2021)
NS = No Standard Established
J = Estimated concentration detected between laboratory method detection limit and reporting limit
VALUE =concentration above laboratory reporting limits
VALUE =concentration above Residential VISL
VALUE =concentration above Non -Residential VISL

APPENDIX A

ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
LINDA CULPEPPER
Director
Mr. Blake Bickmore (via email)
Crescent Communities
227 W. Trade St.
Suite 1000
Charlotte, NC 28202
Dear Mr. Bickmore,
NORTH CAROLINA
Environmental Quality
December 20, 2019
RE: Monitoring Well Construction Permit
Permit #WM0301042
Property along W. Carson Blvd. and S.
Tryon St., Charlotte
Mecklenburg County
In accordance with your completed application received on December 20, 2019, we are forwarding
herewith Monitoring Well Construction Permit Numbered WM0301042 and issued for the
construction of three monitoring wells located near the subject site in Charlotte, Mecklenburg
County.
This Permit will be effective for one year from the date of issuance and shall be subject to the
conditions and limitations as specified therein.
Should you have any questions, please contact Edward Watson at [phone] ext. 2198,
or by email at [e-mail].
Sincerely,
DocuSigned by:
F161FB69A2D84A3...
Andrew H. Pitner, P.G., Assistant Regional Supervisor
Mooresville Regional Office
Water Quality Regional Operations Section
Division of Water Resources
CC: WQROS, Central Office (via Laserfiche)
Jenna Dew, ECS Limited, Inc. (via email)
3D Environmental (via email)
D Q
�� North Carolina Department of Environmental Quality I Division of Water Resources
Mooresville Regional Office 1 610 East Center Avenue, Suite 301 1 Mooresville, North Carolina 28115
None-icanauNn i
nwm,em of eem—woviRv 704,663.1699

NORTH CAROLINA
DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES
PERMIT FOR THE CONSTRUCTION OF A MONITORING WELL
In accordance with the provisions of Article 7, Chapter 87, North Carolina General Statutes, and other applicable Laws,
Rules and Regulations.
PERMISSION IS HEREBY GRANTED TO
Crescent Communities (ECS Limited, Inc. as Agent)
FOR THE CONSTRUCTION OF A MONITOR WELL SYSTEM consisting of three monitoring wells owned by Crescent
Communities near the subject site, Charlotte, Mecklenburg County. This Permit is issued in accordance with the application
received on December 20, 2019, in conformity with specifications and supporting data, all of which are filed with the
Department of Environmental Quality and are considered integral parts of this Permit.
This Permit is for well construction only, and does not waive any provision or requirement of any other applicable law or
regulation. Construction of any well under this Permit shall be in strict compliance with the North Carolina Well Construction
Regulations and Standards (15A NCAC 02C .0100), and other State and Local Laws and regulations pertaining to well
construction.
If any requirements or limitations specified in this Permit are unacceptable, you have a right to an adjudicatory hearing upon
written request within 30 days of receipt of this Permit. The request must be in the form of a written petition conforming to
Chapter 150B of the North Carolina General Statutes and filed with the Office of Administrative Hearings, 6714 Mail Service
Center, Raleigh, North Carolina 27699-6714. Unless such a demand is made, this Permit is final and binding.
This Permit will be effective for one year from the date of its issuance and shall be subject to other specified conditions,
limitations, or exceptions as follows:
1. Issuance of this Permit does not obligate reimbursement from State trust funds, if these wells are being installed as
part of an investigation for contamination from an underground storage tank or dry cleaner incident.
2. Issuance of this Permit does not supersede any other agreement, permit, or requirement issued by another agency.
3. The well(s) shall be located and constructed as shown on the attachments submitted as part of the Permit application.
4. Each well shall have a Well Contractor Identification Plate in accordance with 15A NCAC 02C .0108(o).
5. Well construction records (GW-1) for each well shall be submitted to the Division of Water Resources' Information
Processing Unit within 30 days of the well completion.
6. When the well is discontinued or abandoned, it shall be abandoned in accordance with 15A NCAC 02C .0113 and a
well abandonment record (GW-30) shall be submitted to the Division of Water Resources' Information Processing
Unit within 30 days of the well abandonment.
7. Adequate permits shall be obtained from Mecklenburg County Groundwater and Wastewater Services.
Permit issued the 20th day of December, 2019
FOR THE NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
DocuSigned by:
F161FB69A2D84A3...
Andrew H. Pitner, P.G., Assistant Regional Supervisor
Division of Water Resources
By Authority of the Environmental Management Commission
Permit No. # WM0301042

Mecklenburg County Health Department
Groundwater & Wastewater Services �Ng°R° c
700 N. Tryon St., Suite 211 °
Charlotte, NC 28202 0� z Permit Issuance Date:
Phone: [phone]
Fax: [phone] �2 JAI ¢ Permit Number:
http://groundwater.charmeck.org
Tti CARD .z
SUBSURFACE INVESTIGATION PERMIT
I. Well Owner Information
Name: Blake Bickmore
Attn:
Phone #: [phone]
Address 1: 227 W Trade St
Address 2: Suite 1000
City: Charlotte State: NC Zip: 28202
Agent Information (if applicable)
Name: Jenna Dew
Attn:
Phone #: [phone]
Address 1: 1812 Center Park Drive
Address 2: Suite D
City: Charlotte
III. Site Information
State: NC
Site Name; W Carson and S Tryon Property
Parcel ID Number: 07305304
Address:
City:
General Conditions of This Permit:
Zip: 28217
State: NC Zip:
Agent
12/30/2019
70002714
• This permit shall be VALID fora period not to exceed twelve (12) months from the date of issuance.
• This permit is VALID for the site specified above and must be on -site during the course of the investigation
and made available to a Department representative upon request.
• A North Carolina Certified Well Contrator must perform any well contractor activities associated with this
permit.
• All wells shall be constructed and abandoned to the standards of Chapter VI, Section V and Section VI
of the Mecklenburg County Groundwater Well Regulations.
• All temporary wells, including those installed using Direct Push Technology, must be abandoned
to the standards of Chapter VI, Section VI of the Mecklenburg County Groundwater Well Regulations.
• Registration information for all wells must be submitted to the Department within thirty (30) days of well
completion. If water samples are collected, it is recommended that the well NOT be registered until the
analytical results are received.
SIP Form — revised 2/15/11

Mecklenburg County Health Department
Groundwater & Wastewater Services �Ng°R° c
700 N. Tryon St., Suite 211 °
Charlotte, NC 28202 0� z Permit Issuance Date:
Phone: [phone]
Fax: [phone] �2 JAI ¢ Permit Number:
http://groundwater.charmeck.org
Tti CARD .z
SUBSURFACE INVESTIGATION PERMIT
I. Well Owner Information
Name: Crescent Communities
Attn: Blake Bickmore
Phone #: [phone]
Address 1: 601 S Tryon Street
Address 2: Suite 800
City: Charlotte State: NC Zip: 28202
Agent Information (if applicable)
Name: ECS Southeast, LLP
Attn: Chris Orrell
Phone #: [phone]
Address 1: 1812 Center Park Drive
Address 2: Suite D
City: Charlotte
III. Site Information
State: NC
Site Name; W Carson and S Tryon Property
Parcel ID Number: 07305304
Address:
City:
General Conditions of This Permit:
Zip: 28217
State: NC Zip:
Agent
10/15/2021
70002714
• This permit shall be VALID fora period not to exceed twelve (12) months from the date of issuance.
• This permit is VALID for the site specified above and must be on -site during the course of the investigation
and made available to a Department representative upon request.
• A North Carolina Certified Well Contrator must perform any well contractor activities associated with this
permit.
• All wells shall be constructed and abandoned to the standards of Chapter VI, Section V and Section VI
of the Mecklenburg County Groundwater Well Regulations.
• All temporary wells, including those installed using Direct Push Technology, must be abandoned
to the standards of Chapter VI, Section VI of the Mecklenburg County Groundwater Well Regulations.
• Registration information for all wells must be submitted to the Department within thirty (30) days of well
completion. If water samples are collected, it is recommended that the well NOT be registered until the
analytical results are received.
SIP Form — revised 2/15/11

WELL CONSTRUCTION RECORD (GW-1)
For Internal Use Only:
1. Well Contractor Information:
Walter L Davis
Well Contractor Name
3162-A
NC Well Contractor Certification Number
3D Environmental Investigations LLC
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural [3Municipal/Public
Geothermal (Heating/Cooling Supply) Residential Water Supply (single)
=.' lndustrial/Commercial Residential Water Supply (shared)
Irriaatton
Non -Water Supply Well:
Recharge
Storage and Recovery
Test
rental Technology
mal (Closed Loop)
4. Date Well(s) Completed:
5a. Well Location:
Groundwater Remediation
Salinity Barrier
Stormwater Drainage
0Subsidence Control
[ITracer
under #21
10-28-21 WtellID# Gw-2
Facility/Owner Name Facility M# (if applicable)
1106 South Tryon Street Charlotte NC
Physical Address, City, and Zip
County
Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
6. Is(are) the well(s)Permanent or jTemporary
14. WATER ZONES
FROM
TO
DESCRIPTION
ft.
ft.
ft.
ft.
15. OUTER CASING (for multi -cased wells) OR LINER (if a tcable)
FROM
TO
DIAMETER
THICKNESS
MATERIAL
ft.
ft.
in.
16. INNER CASING OR TUBING(geothermal closed -loop)
FROM
TO
DIAMETER
THICKNESS
MATERIAL
0 et.
20 ft.
1 In.
sch 40
PVC:
ft.
ft.
in.
17. SCREEN
FROM
TO
DIAMETER
SLOT SIZE
THICKNESS
MATERIAL
Z0 ft.
24 ft.
1 In'
010
40
PVC
ft.
ft.
in.
I& GROUT
FROM
TO
MATERIAL
EMPLACEMENT METHOD & AMOUNT
ft.
ft'
Cement
ft.
ft.
bentanite
ft.
ft.
19. SAND/GRAVEL PACK (if applicable)
FROM
TO
I MATERIAL
EMPLACEMENT METHOD
ft.
ft.
#2sand
ft.
ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM
TO
DESCRIPTION (color, hardness, soil/mck type, gmin siu, etc.)
ft.
ft.
it.
ft.
ft.
ft.
ft.
ft.
ft.
ft.
ft.
ft.
ft.
ft,
21. REMARKS
Water Samples With Geo robe Tooling
W 22;K ti
41 L/
Signature of Certified Well Con ctor
7. Is this a repair to an erasting well: 11Yes or E)No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed -Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: 1 @24 (ft.)
For multiple wells list all depths if different (example- 3@200' and 2@100)
10. Static water level below top of casing:
If water level is above casing, use "+"
11. Borehole diameter: 5 (in )
Direct Push
12. Well construction method: _
(i.e. auger, rotary, cable, direct push, etc.
10-30-21
Hate
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMTI'TAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
(ft.) Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Iniection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
FOR WATER SUPPLY WELLS ONLY: 1636 Mail Service Center, Raleigh, NC 27699-1636
13a. Yield (gpm) Method or test: 24c. For Water Supply & Iniection Wells: In addition to sending the form to
the address(cs) above, also submit one copy of this form within 30 days of
13b. Disinfection type: Amount: completion of well construction to the county health department of the county
where constructed.
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016

WELL CONSTRUCTION RECORD (GW-1)
For Internal Use Only:
1. Well Contractor Information:
Wafter L Davis
Well Contractor Name
3162-A
NC Well Contractor Certification Number
3D Environmental Investigations LLC
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural
-I Geothermal (Heating/Cooling Supply)
Industrial/Commercial
Irrigation
Non -Water Supply Well:
Recharge
Storage and Recovery
Test
rental Technology
mal (Closed Loop)
4. Date Well(s) Completed:
5a. Well Location:
[3Municipal/public
Residential Water Supply (single)
Residential Water Supply (shared)
Groundwater Remediation
[)Salinity Barrier
Oss Stormwater Drainage
Subsidence Control
Tracer
under#21
10-28-21 WeIIID# Gw-1-3-4
Facility/Owner Name Facility ID# (if applicable)
1106 South Tryon Street Charlotte NC
Physical Address, City, and Zip
County
Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N
6. Is(are) the well(s)OPermanent or OTemporary
W
7. Is this a repair to an existing well: EjYes or EjNo
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed -Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: 3@29 (ft.)
For multiple wells list all depths if different (example- 3@200' and 2@100)
10. Static water level below top of casing:
If water level is above casing, use
Direct Push
12. Well construction method: _
(i.e. auger, rotary, cable, direct push, etc
14. WATER ZONES
FROM
TO
DESCRIPTION
ft.
ft.
ft.
ft.
15.OUTER CASING (for multi -cased wells) OR LINER (if!!(if!!p livable
FROM
TO
DIAMETER
THICKNESS
MATERIAL
ft.
ft.
in.
16. INNER CASING OR TUBING(geothermal closed -loop)
FROM
TO
I DIAMETER
THICKNESS
I MATERIAL
a ft.
25 ft.
in-
sch 40
PVC;
ft.
fr.
in.
17. SCREEN
FROM
TO
DIAMETER
SLOT SIZE
THICKNESS
MATERIAL
25 ft
29 ft.
In
010
40
PVC.
ft.
ft.
in.
18. GROUT
FROM
I TO
MATERIAL
EMPLACEMENT METHOD & AMOUNT
ft'
ft'
Cement
ft.
ft.
bentanite
ft.
ft.
19. SAND/GRAVEL PACK (if applicable)
FROM
TO
MATERIAL
EMPLACEMENT METHOD
ft.
ft.
#2sand
ft.
ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM
TO
DESCRIPTION (color, hardness, wfllmck type, grain siz , etc.)
ft.
ft.
ft.
ft.
ft.
ft.
ft.
ft.
ft.
ft.
ft.
ft.
ft.
ft.
21. REMARKS
Water Samples With Geo robe Toolin
22. afro
10-30-21
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBN HTTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
(ft.) Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699.1617
24b. For Iniection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
FOR WATER SUPPLY WELLS ONLY: 1636 Mail Service Center, Raleigh, NC 27699-1636
13a. Yield (gpm) Method of test: 24c. For Water Supply & Iniection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
13b. Disinfection type: Amount: completion of well construction to the county health department of the county
where constructed.
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016

WELL ABANDONMENT RECORD
1. Well Contractor Information:
Walter L Davis
Well Contractor Name (or well owner personally abandoning well on his/her property)
3162-A
NC Well Contractor Certification Number
3D Environmental Investigations LLC
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (Le. UIC, County, State, Variance, etc.) if known
3. Well use (check well use):
Water Supply Well:
❑Agricultural
❑Geothermal (Heating/Cooling Supply)
❑Industrial/Commercial
Non -Water Supply Well:
❑Aquifer Recharge
❑Aquifer Storage and Recovery
❑Aquifer Test
❑Experimental Technology
❑Geothermal (Closed Loop)
❑Geothermal (Heating/Cooling
4. Date well(s) abandoned:
Sa. Well location:
10-28-21
❑Municipal/Public
❑Residential Water Supply (single)
❑Residential Water Supply (shared)
❑Recovery
❑Groundwater Remediation
❑Salinity Barrier
❑Stormwater Drainage
❑Subsidence Control
❑Tracer
❑Other (explain under 7g)
Facility/Owner Name Facility ID# (if applicable)
1106 South Tryon Street Charlotte NC
Physical Address, City, and Zip
County
Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(ifwell field, one lat/long is sufficient)
N
W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non -water supply wells
ONLY with the same constructionlabandonment, you can submit one form.
Gw-2
6a. Well ID#:
24
6b. Total well depth:
1
6c. Borehole diameter:
6d. Water level below ground surface: N/A
For Internal Use ONLY:
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed -Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. ApproAntutte volume of water retraining in well(s): (gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
s Neat Cement Grout
R Bentonite Chips or Pellets
❑ Sand Cement Grout
❑ Dry Clay
❑ Concrete Grout
❑ Drill Cuttings
❑ Specialty Grout
❑ Gravel
❑ Bentonite Slurry
❑ Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
7g. Provide a brief description of the abandonment procedure:
8. Ce ti6pa
� Z /)
10-30-21
rgnawre of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Infection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
6e. Outer casing length (if known): N/A -(ft.) 10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
6f. Inner casing/tubing length (if known): 20 (ft) abandoned.
4
6g. Screen length (if known):
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016

APPENDIX 6

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
November 11, 2021
Chris Orrell
ECS Southeast, LLP
1900 Center Park Dr Suite D
9809 Aviary Hill Way, Charlott
Charlotte, NC 28217
RE: Project: Carson & Tryon
Pace Project No.: 92569749
Dear Chris Orrell:
Enclosed are the analytical results for sample(s) received by the laboratory on November 01, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
(4a,�inl� ,GUA V u
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: ECS Southeast Reporting, ECS Southeast
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 87

lacieAnalyfica('
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Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: Carson & Tryon
Pace Project No.: 92569749
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: A130792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TNO03
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification M CERT0086
Nebraska Certification #: NE-OS-15-05
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification M 37712
CERTIFICATIONS
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TNO02
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LA000356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A21-A 2926.01
A21-A-ISO 17025 Certification #: 1461.01
A21-A-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: Carson & Tryon
Pace Project No.: 92569749
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92569749001
GW-1
Water
10/28/2110:10
11/01/2107:10
92569749002
GW-2
Water
10/28/2110:45
11/01/2107:10
92569749003
GW-3
Water
10/28/2111:55
11/01/2107:10
92569749004
GW-4
Water
10/28/2112:10
11/01/2107:10
92569749005
S13-1
Solid
10/28/2110:00
11/01/2107:10
92569749006
S13-2
Solid
10/28/2110:25
11/01/2107:10
92569749007
S13-3
Solid
10/28/2110:40
11/01/2107:10
92569749008
S13-4
Solid
10/28/2110:55
11/01/2107:10
92569749009
S13-5
Solid
10/28/2111:10
11/01/2107:10
92569749010
S13-6
Solid
10/28/2111:25
11/01/2107:10
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 3 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Carson & Tryon
92569749
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92569749001
GW-1
EPA 8270E
PKS
74
PASI-C
EPA 8260D
SAS
63
PASI-C
92569749002
GW-2
EPA 8270E
PKS
74
PASI-C
EPA 8260D
SAS
63
PASI-C
92569749003
GW-3
EPA 8270E
PKS
74
PASI-C
EPA 8260D
SAS
63
PASI-C
92569749004
GW-4
EPA 8270E
PKS
74
PASI-C
EPA 8260D
SAS
63
PASI-C
92569749005
S13-1
EPA 6010D
CBV
7
PASI-A
EPA 7471B
DBB1
1
PASI-A
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
LMB
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
CMK
1
PAN
EPA 7199
JER
1
PAN
92569749006
S13-2
EPA 6010D
CBV
7
PASI-A
EPA 7471B
DBB1
1
PASI-A
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
LMB
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
CMK
1
PAN
EPA 7199
JER
1
PAN
92569749007
S13-3
EPA 6010D
CBV
7
PASI-A
EPA 7471B
DBB1
1
PASI-A
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
LMB
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
CMK
1
PAN
EPA 7199
JER
1
PAN
92569749008
S13-4
EPA 6010D
CBV
7
PASI-A
EPA 7471B
D13131
1
PASI-A
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
LMB
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
CMK
1
PAN
EPA 7199
JER
1
PAN
92569749009
S13-5
EPA 6010D
CBV
7
PASI-A
REPORT OF LABORATORY ANALYSIS
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leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Carson & Tryon
Pace Project No.: 92569749
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
EPA 7471B
D13131
1
PASI-A
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
LMB
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
CMK
1
PAN
EPA 7199
JER
1
PAN
92569749010 S13-6 EPA 6010D
CBV
7
PASI-A
EPA 7471 B
D661
1
PASI-A
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
LMB
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
CMK
1
PAN
EPA 7199
JER
1
PAN
PAN = Pace National - Mt. Juliet
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: GW-1
Lab ID:
92569749001
Collected:
10/28/21
10:10
Received: 11/01/21 07:10 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8270E RVE
Analytical
Method: EPA 8270E
Preparation Method: EPA 3510C
Pace Analytical
Services
- Charlotte
Acenaphthene
ND
ug/L
8.3
1.7
1
11/02/21 05:10
11/02/21 23:57
83-32-9
Acenaphthylene
ND
ug/L
8.3
1.6
1
11/02/21 05:10
11/02/21 23:57
208-96-8
Aniline
ND
ug/L
8.3
1.4
1
11/02/21 05:10
11/02/21 23:57
62-53-3
Anthracene
ND
ug/L
8.3
1.9
1
11/02/21 05:10
11/02/21 23:57
120-12-7
Benzo(a)anthracene
ND
ug/L
8.3
2.2
1
11/02/21 05:10
11/02/21 23:57
56-55-3
Benzo(a)pyrene
ND
ug/L
8.3
2.3
1
11/02/21 05:10
11/02/21 23:57
50-32-8
Benzo(b)fluoranthene
ND
ug/L
8.3
2.2
1
11/02/21 05:10
11/02/21 23:57
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
8.3
2.4
1
11/02/21 05:10
11/02/21 23:57
191-24-2
Benzo(k)fluoranthene
ND
ug/L
8.3
2.3
1
11/02/21 05:10
11/02/21 23:57
207-08-9
Benzoic Acid
ND
ug/L
41.7
2.8
1
11/02/21 05:10
11/02/21 23:57
65-85-0 L2
Benzyl alcohol
ND
ug/L
16.7
2.4
1
11/02/21 05:10
11/02/21 23:57
100-51-6
4-Bromophenylphenyl ether
ND
ug/L
8.3
1.5
1
11/02/21 05:10
11/02/21 23:57
101-55-3
Butylbenzylphthalate
ND
ug/L
8.3
2.6
1
11/02/21 05:10
11/02/21 23:57
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
8.3
2.8
1
11/02/21 05:10
11/02/21 23:57
59-50-7
4-Chloroaniline
ND
ug/L
16.7
3.0
1
11/02/21 05:10
11/02/21 23:57
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
8.3
1.5
1
11/02/21 05:10
11/02/21 23:57
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
8.3
1.6
1
11/02/21 05:10
11/02/21 23:57
111-44-4
2-Chloronaphthalene
ND
ug/L
8.3
1.4
1
11/02/21 05:10
11/02/21 23:57
91-58-7
2-Chlorophenol
ND
ug/L
8.3
1.0
1
11/02/21 05:10
11/02/21 23:57
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
8.3
1.7
1
11/02/21 05:10
11/02/21 23:57
7005-72-3
Chrysene
ND
ug/L
8.3
2.3
1
11/02/21 05:10
11/02/21 23:57
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
8.3
2.5
1
11/02/21 05:10
11/02/21 23:57
53-70-3
Dibenzofuran
ND
ug/L
8.3
1.8
1
11/02/21 05:10
11/02/21 23:57
132-64-9
1,2-Dichlorobenzene
ND
ug/L
8.3
1.5
1
11/02/21 05:10
11/02/21 23:57
95-50-1
1,3-Dichlorobenzene
ND
ug/L
8.3
1.3
1
11/02/21 05:10
11/02/21 23:57
541-73-1
1,4-Dichlorobenzene
ND
ug/L
8.3
1.4
1
11/02/21 05:10
11/02/21 23:57
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
16.7
6.8
1
11/02/21 05:10
11/02/21 23:57
91-94-1
2,4-Dichlorophenol
ND
ug/L
8.3
1.2
1
11/02/21 05:10
11/02/21 23:57
120-83-2
Diethylphthalate
ND
ug/L
8.3
1.7
1
11/02/21 05:10
11/02/21 23:57
84-66-2
2,4-Dimethylphenol
ND
ug/L
8.3
1.4
1
11/02/21 05:10
11/02/21 23:57
105-67-9
Dimethylphthalate
ND
ug/L
8.3
1.8
1
11/02/21 05:10
11/02/21 23:57
131-11-3
Di-n-butylphthalate
ND
ug/L
8.3
1.8
1
11/02/21 05:10
11/02/21 23:57
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
16.7
2.8
1
11/02/21 05:10
11/02/21 23:57
534-52-1
2,4-Dinitrophenol
ND
ug/L
41.7
21.7
1
11/02/21 05:10
11/02/21 23:57
51-28-5 v1
2,4-Dinitrotoluene
ND
ug/L
8.3
1.4
1
11/02/21 05:10
11/02/21 23:57
121-14-2 v1
2,6-Dinitrotoluene
ND
ug/L
8.3
1.4
1
11/02/21 05:10
11/02/21 23:57
606-20-2
Di-n-octylphthalate
ND
ug/L
8.3
3.3
1
11/02/21 05:10
11/02/21 23:57
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.0
3.1
1
11/02/21 05:10
11/02/21 23:57
117-81-7
Fluoranthene
ND
ug/L
8.3
1.8
1
11/02/21 05:10
11/02/21 23:57
206-44-0
Fluorene
ND
ug/L
8.3
1.7
1
11/02/21 05:10
11/02/21 23:57
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
8.3
1.5
1
11/02/21 05:10
11/02/21 23:57
87-68-3
Hexachlorobenzene
ND
ug/L
8.3
1.8
1
11/02/21 05:10
11/02/21 23:57
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
8.3
1.3
1
11/02/21 05:10
11/02/21 23:57
77-47-4
Hexachloroethane
ND
ug/L
8.3
1.2
1
11/02/21 05:10
11/02/21 23:57
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
8.3
2.4
1
11/02/21 05:10
11/02/21 23:57
193-39-5
REPORT OF LABORATORY ANALYSIS
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Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 87

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ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: GW-1 Lab ID: 92569749001 Collected: 10/28/21 10:10 Received: 11/01/21 07:10 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E RVE
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Date: 11 /11 /2021 09:47 AM
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services
- Charlotte
ND
ug/L
8.3
1.4
1
11/02/2105:10
11/02/2123:57
78-59-1
ND
ug/L
8.3
1.7
1
11/02/2105:10
11/02/2123:57
90-12-0
ND
ug/L
8.3
1.6
1
11 /02/21 05:10
11 /02/21 23:57
91-57-6
ND
ug/L
8.3
1.6
1
11/02/2105:10
11/02/2123:57
95-48-7
ND
ug/L
8.3
1.0
1
11/02/2105:10
11/02/2123:57
15831-10-4
ND
ug/L
8.3
1.7
1
11 /02/21 05:10
11 /02/21 23:57
91-20-3
ND
ug/L
16.7
2.5
1
11/02/2105:10
11/02/2123:57
88-74-4
ND
ug/L
16.7
3.1
1
11/02/2105:10
11/02/2123:57
99-09-2
ND
ug/L
16.7
4.2
1
11 /02/21 05:10
11 /02/21 23:57
100-01-6
ND
ug/L
8.3
1.6
1
11/02/2105:10
11/02/2123:57
98-95-3
ND
ug/L
8.3
1.2
1
11/02/2105:10
11/02/2123:57
88-75-5
ND
ug/L
41.7
5.5
1
11/02/2105:10
11/02/2123:57
100-02-7
ND
ug/L
8.3
1.6
1
11/02/2105:10
11/02/2123:57
62-75-9
ND
ug/L
8.3
1.1
1
11 /02/21 05:10
11 /02/21 23:57
621-64-7
ND
ug/L
8.3
2.5
1
11/02/2105:10
11/02/2123:57
86-30-6
ND
ug/L
8.3
0.96
1
11/02/2105:10
11/02/2123:57
108-60-1
ND
ug/L
16.7
3.1
1
11/02/2105:10
11/02/2123:57
87-86-5
ND
ug/L
8.3
1.7
1
11 /02/21 05:10
11 /02/21 23:57
85-01-8
ND
ug/L
8.3
1.1
1
11/02/2105:10
11/02/2123:57
108-95-2
ND
ug/L
8.3
1.8
1
11/02/2105:10
11/02/2123:57
129-00-0
ND
ug/L
8.3
1.4
1
11/02/2105:10
11/02/2123:57
120-82-1
ND
ug/L
8.3
1.2
1
11/02/2105:10
11/02/2123:57
95-95-4
ND
ug/L
8.3
1.3
1
11/02/2105:10
11/02/2123:57
88-06-2
57
%
10-144
1
11/02/2105:10
11/02/2123:57
4165-60-0
55
%
10-130
1
11 /02/21 05:10
11 /02/21 23:57
321-60-8
73
%
34-163
1
11 /02/21 05:10
11 /02/21 23:57
1718-51-0
29
%
10-130
1
11/02/2105:10
11/02/2123:57
13127-88-3
39
%
10-130
1
11/02/2105:10
11/02/2123:57
367-12-4
67
%
10-144
1
11/02/2105:10
11/02/2123:57
118-79-6
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
ND
ug/L
25.0
5.1
1
11/03/2104:21
67-64-1
ND
ug/L
1.0
0.34
1
11 /03/21 04:21
71-43-2
ND
ug/L
1.0
0.29
1
11/03/2104:21
108-86-1
ND
ug/L
1.0
0.47
1
11/03/2104:21
74-97-5
ND
ug/L
1.0
0.31
1
11/03/2104:21
75-27-4
ND
ug/L
1.0
0.34
1
11/03/2104:21
75-25-2
ND
ug/L
2.0
1.7
1
11/03/2104:21
74-83-9
ND
ug/L
5.0
4.0
1
11/03/2104:21
78-93-3
ND
ug/L
1.0
0.33
1
11/03/2104:21
56-23-5
ND
ug/L
1.0
0.28
1
11/03/2104:21
108-90-7
ND
ug/L
1.0
0.65
1
11/03/2104:21
75-00-3
ND
ug/L
1.0
0.43
1
11/03/2104:21
67-66-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: GW-1 Lab ID: 92569749001 Collected: 10/28/21 10:10 Received: 11/01/21 07:10 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Chloromethane
ND
ug/L
1.0
0.54
1
11/03/21 04:21
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
0.32
1
11/03/21 04:21
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
0.32
1
11/03/21 04:21
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
11/03/21 04:21
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
11/03/21 04:21
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
11/03/21 04:21
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
11/03/21 04:21
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
11/03/21 04:21
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
0.34
1
11/03/21 04:21
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
11/03/21 04:21
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
0.35
1
11/03/21 04:21
75-71-8
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
11/03/21 04:21
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
11/03/21 04:21
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
11/03/21 04:21
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
0.38
1
11/03/21 04:21
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
0.40
1
11/03/21 04:21
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.36
1
11/03/21 04:21
78-87-5
1,3-Dichloropropane
ND
ug/L
1.0
0.28
1
11/03/21 04:21
142-28-9
2,2-Dichloropropane
ND
ug/L
1.0
0.39
1
11/03/21 04:21
594-20-7
1,1-Dichloropropene
ND
ug/L
1.0
0.43
1
11/03/21 04:21
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
11/03/21 04:21
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
11/03/21 04:21
10061-02-6
Diisopropyl ether
ND
ug/L
1.0
0.31
1
11/03/21 04:21
108-20-3
Ethylbenzene
ND
ug/L
1.0
0.30
1
11/03/21 04:21
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1.5
1
11/03/21 04:21
87-68-3
2-Hexanone
ND
ug/L
5.0
0.48
1
11/03/21 04:21
591-78-6
p-Isopropyltoluene
ND
ug/L
1.0
0.41
1
11/03/21 04:21
99-87-6
Methylene Chloride
ND
ug/L
5.0
2.0
1
11/03/21 04:21
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
2.7
1
11/03/21 04:21
108-10-1
Methyl-tert-butyl ether
ND
ug/L
1.0
0.42
1
11/03/21 04:21
1634-04-4
Naphthalene
ND
ug/L
1.0
0.64
1
11/03/21 04:21
91-20-3
Styrene
ND
ug/L
1.0
0.29
1
11/03/21 04:21
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.31
1
11/03/21 04:21
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
11/03/21 04:21
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.29
1
11/03/21 04:21
127-18-4
Toluene
ND
ug/L
1.0
0.48
1
11/03/21 04:21
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
1.0
0.81
1
11/03/21 04:21
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
1.0
0.64
1
11/03/21 04:21
120-82-1
1,1,1-Trichloroethane
ND
ug/L
1.0
0.33
1
11/03/21 04:21
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.32
1
11/03/21 04:21
79-00-5
Trichloroethene
ND
ug/L
1.0
0.38
1
11/03/21 04:21
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.30
1
11/03/21 04:21
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.26
1
11/03/21 04:21
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.3
1
11/03/21 04:21
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.39
1
11/03/21 04:21
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC.
Page 8 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: GW-1
Lab ID:
92569749001
Collected:
10/28/21 10:10
Received: 11/01/21 07:10 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical
Method: EPA 8260D
Pace Analytical
Services
- Charlotte
Xylene (Total)
ND
ug/L
1.0
0.34
1
11/03/21 04:21
1330-20-7
m&p-Xylene
ND
ug/L
2.0
0.71
1
11/03/21 04:21
179601-23-1
o-Xylene
ND
ug/L
1.0
0.34
1
11/03/21 04:21
95-47-6
Surrogates
4-Bromofluorobenzene (S)
104
%
70-130
1
11/03/21 04:21
460-00-4
1,2-Dichloroethane-d4 (S)
95
%
70-130
1
11/03/21 04:21
17060-07-0
Toluene-d8 (S)
102
%
70-130
1
11/03/21 04:21
2037-26-5
Date: 11 /11 /2021 09:47 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: GW-2 Lab ID: 92569749002 Collected: 10/28/21 10:45 Received: 11/01/21 07:10 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Acenaphthene
ND
ug/L
10.0
2.0
1
11/02/21 05:10
11/03/21 00:23
83-32-9
Acenaphthylene
ND
ug/L
10.0
2.0
1
11/02/21 05:10
11/03/21 00:23
208-96-8
Aniline
ND
ug/L
10.0
1.6
1
11/02/21 05:10
11/03/21 00:23
62-53-3
Anthracene
ND
ug/L
10.0
2.3
1
11/02/21 05:10
11/03/21 00:23
120-12-7
Benzo(a)anthracene
ND
ug/L
10.0
2.7
1
11/02/21 05:10
11/03/21 00:23
56-55-3
Benzo(a)pyrene
ND
ug/L
10.0
2.8
1
11/02/21 05:10
11/03/21 00:23
50-32-8
Benzo(b)fluoranthene
ND
ug/L
10.0
2.6
1
11/02/21 05:10
11/03/21 00:23
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
10.0
2.8
1
11/02/21 05:10
11/03/21 00:23
191-24-2
Benzo(k)fluoranthene
ND
ug/L
10.0
2.7
1
11/02/21 05:10
11/03/21 00:23
207-08-9
Benzoic Acid
ND
ug/L
50.0
3.4
1
11/02/21 05:10
11/03/21 00:23
65-85-0
Benzyl alcohol
ND
ug/L
20.0
2.9
1
11/02/21 05:10
11/03/21 00:23
100-51-6
4-Bromophenylphenyl ether
ND
ug/L
10.0
1.8
1
11/02/21 05:10
11/03/21 00:23
101-55-3
Butylbenzylphthalate
ND
ug/L
10.0
3.1
1
11/02/21 05:10
11/03/21 00:23
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
10.0
3.3
1
11/02/21 05:10
11/03/21 00:23
59-50-7
4-Chloroaniline
ND
ug/L
20.0
3.6
1
11/02/21 05:10
11/03/21 00:23
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1.8
1
11/02/21 05:10
11/03/21 00:23
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
10.0
1.9
1
11/02/21 05:10
11/03/21 00:23
111-44-4
2-Chloronaphthalene
ND
ug/L
10.0
1.7
1
11/02/21 05:10
11/03/21 00:23
91-58-7
2-Chlorophenol
ND
ug/L
10.0
1.2
1
11/02/21 05:10
11/03/21 00:23
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
10.0
2.0
1
11/02/21 05:10
11/03/21 00:23
7005-72-3
Chrysene
ND
ug/L
10.0
2.8
1
11/02/21 05:10
11/03/21 00:23
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
10.0
3.0
1
11/02/21 05:10
11/03/21 00:23
53-70-3
Dibenzofuran
ND
ug/L
10.0
2.1
1
11/02/21 05:10
11/03/21 00:23
132-64-9
1,2-Dichlorobenzene
ND
ug/L
10.0
1.8
1
11/02/21 05:10
11/03/21 00:23
95-50-1
1,3-Dichlorobenzene
ND
ug/L
10.0
1.6
1
11/02/21 05:10
11/03/21 00:23
541-73-1
1,4-Dichlorobenzene
ND
ug/L
10.0
1.7
1
11/02/21 05:10
11/03/21 00:23
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
20.0
8.1
1
11/02/21 05:10
11/03/21 00:23
91-94-1
2,4-Dichlorophenol
ND
ug/L
10.0
1.4
1
11/02/21 05:10
11/03/21 00:23
120-83-2
Diethylphthalate
ND
ug/L
10.0
2.0
1
11/02/21 05:10
11/03/21 00:23
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1.7
1
11/02/21 05:10
11/03/21 00:23
105-67-9
Dimethylphthalate
ND
ug/L
10.0
2.1
1
11/02/21 05:10
11/03/21 00:23
131-11-3
Di-n-butylphthalate
ND
ug/L
10.0
2.2
1
11/02/21 05:10
11/03/21 00:23
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
20.0
3.4
1
11/02/21 05:10
11/03/21 00:23
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
26.0
1
11/02/21 05:10
11/03/21 00:23
51-28-5
2,4-Dinitrotoluene
ND
ug/L
10.0
1.6
1
11/02/21 05:10
11/03/21 00:23
121-14-2
2,6-Dinitrotoluene
ND
ug/L
10.0
1.7
1
11/02/21 05:10
11/03/21 00:23
606-20-2
Di-n-octylphthalate
ND
ug/L
10.0
3.9
1
11/02/21 05:10
11/03/21 00:23
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
6.0
3.7
1
11/02/21 05:10
11/03/21 00:23
117-81-7
Fluoranthene
ND
ug/L
10.0
2.2
1
11/02/21 05:10
11/03/21 00:23
206-44-0
Fluorene
ND
ug/L
10.0
2.1
1
11/02/21 05:10
11/03/21 00:23
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
10.0
1.8
1
11/02/21 05:10
11/03/21 00:23
87-68-3
Hexachlorobenzene
ND
ug/L
10.0
2.2
1
11/02/21 05:10
11/03/21 00:23
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1.6
1
11/02/21 05:10
11/03/21 00:23
77-47-4
Hexachloroethane
ND
ug/L
10.0
1.4
1
11/02/21 05:10
11/03/21 00:23
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
10.0
2.9
1
11/02/21 05:10
11/03/21 00:23
193-39-5
REPORT OF LABORATORY ANALYSIS
L2
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: GW-2 Lab ID: 92569749002 Collected: 10/28/21 10:45 Received: 11/01/21 07:10 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E RVE
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Date: 11 /11 /2021 09:47 AM
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services
- Charlotte
ND
ug/L
10.0
1.7
1
11/02/2105:10
11/03/2100:23
78-59-1
ND
ug/L
10.0
2.0
1
11/02/2105:10
11/03/2100:23
90-12-0
ND
ug/L
10.0
1.9
1
11 /02/21 05:10
11 /03/21 00:23
91-57-6
ND
ug/L
10.0
1.9
1
11 /02/21 05:10
11 /03/21 00:23
95-48-7
ND
ug/L
10.0
1.2
1
11 /02/21 05:10
11 /03/21 00:23
15831-10-4
ND
ug/L
10.0
2.1
1
11 /02/21 05:10
11 /03/21 00:23
91-20-3
ND
ug/L
20.0
3.0
1
11 /02/21 05:10
11 /03/21 00:23
88-74-4
ND
ug/L
20.0
3.8
1
11 /02/21 05:10
11 /03/21 00:23
99-09-2
ND
ug/L
20.0
5.1
1
11 /02/21 05:10
11 /03/21 00:23
100-01-6
ND
ug/L
10.0
1.9
1
11 /02/21 05:10
11 /03/21 00:23
98-95-3
ND
ug/L
10.0
1.4
1
11 /02/21 05:10
11 /03/21 00:23
88-75-5
ND
ug/L
50.0
6.6
1
11 /02/21 05:10
11 /03/21 00:23
100-02-7
ND
ug/L
10.0
1.9
1
11 /02/21 05:10
11 /03/21 00:23
62-75-9
ND
ug/L
10.0
1.3
1
11 /02/21 05:10
11 /03/21 00:23
621-64-7
ND
ug/L
10.0
3.0
1
11 /02/21 05:10
11 /03/21 00:23
86-30-6
ND
ug/L
10.0
1.2
1
11/02/2105:10
11/03/2100:23
108-60-1
ND
ug/L
20.0
3.8
1
11 /02/21 05:10
11 /03/21 00:23
87-86-5
ND
ug/L
10.0
2.0
1
11 /02/21 05:10
11 /03/21 00:23
85-01-8
ND
ug/L
10.0
1.4
1
11 /02/21 05:10
11 /03/21 00:23
108-95-2
ND
ug/L
10.0
2.2
1
11 /02/21 05:10
11 /03/21 00:23
129-00-0
ND
ug/L
10.0
1.7
1
11/02/2105:10
11/03/2100:23
120-82-1
ND
ug/L
10.0
1.4
1
11 /02/21 05:10
11 /03/21 00:23
95-95-4
ND
ug/L
10.0
1.6
1
11 /02/21 05:10
11 /03/21 00:23
88-06-2
79
%
10-144
1
11 /02/21 05:10
11 /03/21 00:23
4165-60-0
70
%
10-130
1
11 /02/21 05:10
11 /03/21 00:23
321-60-8
99
%
34-163
1
11 /02/21 05:10
11 /03/21 00:23
1718-51-0
45
%
10-130
1
11 /02/21 05:10
11 /03/21 00:23
13127-88-3
54
%
10-130
1
11/02/2105:10
11/03/2100:23
367-12-4
110
%
10-144
1
11 /02/21 05:10
11 /03/21 00:23
118-79-6
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
ND
ug/L
25.0
5.1
1
11/03/2104:38
67-64-1
ND
ug/L
1.0
0.34
1
11 /03/21 04:38
71-43-2
ND
ug/L
1.0
0.29
1
11/03/2104:38
108-86-1
ND
ug/L
1.0
0.47
1
11/03/2104:38
74-97-5
ND
ug/L
1.0
0.31
1
11/03/2104:38
75-27-4
ND
ug/L
1.0
0.34
1
11/03/2104:38
75-25-2
ND
ug/L
2.0
1.7
1
11/03/2104:38
74-83-9
ND
ug/L
5.0
4.0
1
11/03/2104:38
78-93-3
ND
ug/L
1.0
0.33
1
11/03/2104:38
56-23-5
ND
ug/L
1.0
0.28
1
11/03/2104:38
108-90-7
ND
ug/L
1.0
0.65
1
11/03/2104:38
75-00-3
ND
ug/L
1.0
0.43
1
11/03/2104:38
67-66-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: GW-2 Lab ID: 92569749002 Collected: 10/28/21 10:45 Received: 11/01/21 07:10 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Chloromethane
ND
ug/L
1.0
0.54
1
11/03/21 04:38
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
0.32
1
11/03/21 04:38
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
0.32
1
11/03/21 04:38
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
11/03/21 04:38
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
11/03/21 04:38
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
11/03/21 04:38
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
11/03/21 04:38
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
11/03/21 04:38
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
0.34
1
11/03/21 04:38
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
11/03/21 04:38
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
0.35
1
11/03/21 04:38
75-71-8
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
11/03/21 04:38
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
11/03/21 04:38
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
11/03/21 04:38
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
0.38
1
11/03/21 04:38
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
0.40
1
11/03/21 04:38
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.36
1
11/03/21 04:38
78-87-5
1,3-Dichloropropane
ND
ug/L
1.0
0.28
1
11/03/21 04:38
142-28-9
2,2-Dichloropropane
ND
ug/L
1.0
0.39
1
11/03/21 04:38
594-20-7
1,1-Dichloropropene
ND
ug/L
1.0
0.43
1
11/03/21 04:38
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
11/03/21 04:38
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
11/03/21 04:38
10061-02-6
Diisopropyl ether
ND
ug/L
1.0
0.31
1
11/03/21 04:38
108-20-3
Ethylbenzene
ND
ug/L
1.0
0.30
1
11/03/21 04:38
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1.5
1
11/03/21 04:38
87-68-3
2-Hexanone
ND
ug/L
5.0
0.48
1
11/03/21 04:38
591-78-6
p-Isopropyltoluene
ND
ug/L
1.0
0.41
1
11/03/21 04:38
99-87-6
Methylene Chloride
ND
ug/L
5.0
2.0
1
11/03/21 04:38
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
2.7
1
11/03/21 04:38
108-10-1
Methyl-tert-butyl ether
ND
ug/L
1.0
0.42
1
11/03/21 04:38
1634-04-4
Naphthalene
ND
ug/L
1.0
0.64
1
11/03/21 04:38
91-20-3
Styrene
ND
ug/L
1.0
0.29
1
11/03/21 04:38
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.31
1
11/03/21 04:38
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
11/03/21 04:38
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.29
1
11/03/21 04:38
127-18-4
Toluene
ND
ug/L
1.0
0.48
1
11/03/21 04:38
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
1.0
0.81
1
11/03/21 04:38
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
1.0
0.64
1
11/03/21 04:38
120-82-1
1,1,1-Trichloroethane
ND
ug/L
1.0
0.33
1
11/03/21 04:38
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.32
1
11/03/21 04:38
79-00-5
Trichloroethene
ND
ug/L
1.0
0.38
1
11/03/21 04:38
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.30
1
11/03/21 04:38
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.26
1
11/03/21 04:38
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.3
1
11/03/21 04:38
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.39
1
11/03/21 04:38
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC.
Page 12 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: GW-2
Lab ID:
92569749002
Collected:
10/28/21 10:45
Received: 11/01/21 07:10 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical
Method: EPA 8260D
Pace Analytical
Services
- Charlotte
Xylene (Total)
ND
ug/L
1.0
0.34
1
11/03/21 04:38
1330-20-7
m&p-Xylene
ND
ug/L
2.0
0.71
1
11/03/21 04:38
179601-23-1
o-Xylene
ND
ug/L
1.0
0.34
1
11/03/21 04:38
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
11/03/21 04:38
460-00-4
1,2-Dichloroethane-d4 (S)
94
%
70-130
1
11/03/21 04:38
17060-07-0
Toluene-d8 (S)
108
%
70-130
1
11/03/21 04:38
2037-26-5
Date: 11 /11 /2021 09:47 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: GW-3 Lab ID: 92569749003 Collected: 10/28/21 11:55 Received: 11/01/21 07:10 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Acenaphthene
ND
ug/L
8.3
1.7
1
11/02/21 05:10
11/03/21 00:48
83-32-9
Acenaphthylene
ND
ug/L
8.3
1.6
1
11/02/21 05:10
11/03/21 00:48
208-96-8
Aniline
ND
ug/L
8.3
1.4
1
11/02/21 05:10
11/03/21 00:48
62-53-3
Anthracene
ND
ug/L
8.3
1.9
1
11/02/21 05:10
11/03/21 00:48
120-12-7
Benzo(a)anthracene
ND
ug/L
8.3
2.2
1
11/02/21 05:10
11/03/21 00:48
56-55-3
Benzo(a)pyrene
ND
ug/L
8.3
2.3
1
11/02/21 05:10
11/03/21 00:48
50-32-8
Benzo(b)fluoranthene
ND
ug/L
8.3
2.2
1
11/02/21 05:10
11/03/21 00:48
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
8.3
2.4
1
11/02/21 05:10
11/03/21 00:48
191-24-2
Benzo(k)fluoranthene
ND
ug/L
8.3
2.3
1
11/02/21 05:10
11/03/21 00:48
207-08-9
Benzoic Acid
ND
ug/L
41.7
2.8
1
11/02/21 05:10
11/03/21 00:48
65-85-0
Benzyl alcohol
ND
ug/L
16.7
2.4
1
11/02/21 05:10
11/03/21 00:48
100-51-6
4-Bromophenylphenyl ether
ND
ug/L
8.3
1.5
1
11/02/21 05:10
11/03/21 00:48
101-55-3
Butylbenzylphthalate
ND
ug/L
8.3
2.6
1
11/02/21 05:10
11/03/21 00:48
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
8.3
2.8
1
11/02/21 05:10
11/03/21 00:48
59-50-7
4-Chloroaniline
ND
ug/L
16.7
3.0
1
11/02/21 05:10
11/03/21 00:48
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
8.3
1.5
1
11/02/21 05:10
11/03/21 00:48
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
8.3
1.6
1
11/02/21 05:10
11/03/21 00:48
111-44-4
2-Chloronaphthalene
ND
ug/L
8.3
1.4
1
11/02/21 05:10
11/03/21 00:48
91-58-7
2-Chlorophenol
ND
ug/L
8.3
1.0
1
11/02/21 05:10
11/03/21 00:48
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
8.3
1.7
1
11/02/21 05:10
11/03/21 00:48
7005-72-3
Chrysene
ND
ug/L
8.3
2.3
1
11/02/21 05:10
11/03/21 00:48
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
8.3
2.5
1
11/02/21 05:10
11/03/21 00:48
53-70-3
Dibenzofuran
ND
ug/L
8.3
1.8
1
11/02/21 05:10
11/03/21 00:48
132-64-9
1,2-Dichlorobenzene
ND
ug/L
8.3
1.5
1
11/02/21 05:10
11/03/21 00:48
95-50-1
1,3-Dichlorobenzene
ND
ug/L
8.3
1.3
1
11/02/21 05:10
11/03/21 00:48
541-73-1
1,4-Dichlorobenzene
ND
ug/L
8.3
1.4
1
11/02/21 05:10
11/03/21 00:48
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
16.7
6.8
1
11/02/21 05:10
11/03/21 00:48
91-94-1
2,4-Dichlorophenol
ND
ug/L
8.3
1.2
1
11/02/21 05:10
11/03/21 00:48
120-83-2
Diethylphthalate
ND
ug/L
8.3
1.7
1
11/02/21 05:10
11/03/21 00:48
84-66-2
2,4-Dimethylphenol
ND
ug/L
8.3
1.4
1
11/02/21 05:10
11/03/21 00:48
105-67-9
Dimethylphthalate
ND
ug/L
8.3
1.8
1
11/02/21 05:10
11/03/21 00:48
131-11-3
Di-n-butylphthalate
ND
ug/L
8.3
1.8
1
11/02/21 05:10
11/03/21 00:48
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
16.7
2.8
1
11/02/21 05:10
11/03/21 00:48
534-52-1
2,4-Dinitrophenol
ND
ug/L
41.7
21.7
1
11/02/21 05:10
11/03/21 00:48
51-28-5
2,4-Dinitrotoluene
ND
ug/L
8.3
1.4
1
11/02/21 05:10
11/03/21 00:48
121-14-2
2,6-Dinitrotoluene
ND
ug/L
8.3
1.4
1
11/02/21 05:10
11/03/21 00:48
606-20-2
Di-n-octylphthalate
ND
ug/L
8.3
3.3
1
11/02/21 05:10
11/03/21 00:48
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.0
3.1
1
11/02/21 05:10
11/03/21 00:48
117-81-7
Fluoranthene
ND
ug/L
8.3
1.8
1
11/02/21 05:10
11/03/21 00:48
206-44-0
Fluorene
ND
ug/L
8.3
1.7
1
11/02/21 05:10
11/03/21 00:48
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
8.3
1.5
1
11/02/21 05:10
11/03/21 00:48
87-68-3
Hexachlorobenzene
ND
ug/L
8.3
1.8
1
11/02/21 05:10
11/03/21 00:48
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
8.3
1.3
1
11/02/21 05:10
11/03/21 00:48
77-47-4
Hexachloroethane
ND
ug/L
8.3
1.2
1
11/02/21 05:10
11/03/21 00:48
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
8.3
2.4
1
11/02/21 05:10
11/03/21 00:48
193-39-5
REPORT OF LABORATORY ANALYSIS
L2
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: GW-3 Lab ID: 92569749003 Collected: 10/28/21 11:55 Received: 11/01/21 07:10 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E RVE
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Date: 11 /11 /2021 09:47 AM
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services
- Charlotte
ND
ug/L
8.3
1.4
1
11/02/2105:10
11/03/2100:48
78-59-1
ND
ug/L
8.3
1.7
1
11/02/2105:10
11/03/2100:48
90-12-0
ND
ug/L
8.3
1.6
1
11 /02/21 05:10
11 /03/21 00:48
91-57-6
ND
ug/L
8.3
1.6
1
11 /02/21 05:10
11 /03/21 00:48
95-48-7
ND
ug/L
8.3
1.0
1
11 /02/21 05:10
11 /03/21 00:48
15831-10-4
ND
ug/L
8.3
1.7
1
11 /02/21 05:10
11 /03/21 00:48
91-20-3
ND
ug/L
16.7
2.5
1
11 /02/21 05:10
11 /03/21 00:48
88-74-4
ND
ug/L
16.7
3.1
1
11 /02/21 05:10
11 /03/21 00:48
99-09-2
ND
ug/L
16.7
4.2
1
11 /02/21 05:10
11 /03/21 00:48
100-01-6
ND
ug/L
8.3
1.6
1
11 /02/21 05:10
11 /03/21 00:48
98-95-3
ND
ug/L
8.3
1.2
1
11 /02/21 05:10
11 /03/21 00:48
88-75-5
ND
ug/L
41.7
5.5
1
11 /02/21 05:10
11 /03/21 00:48
100-02-7
ND
ug/L
8.3
1.6
1
11 /02/21 05:10
11 /03/21 00:48
62-75-9
ND
ug/L
8.3
1.1
1
11 /02/21 05:10
11 /03/21 00:48
621-64-7
ND
ug/L
8.3
2.5
1
11 /02/21 05:10
11 /03/21 00:48
86-30-6
ND
ug/L
8.3
0.96
1
11/02/2105:10
11/03/2100:48
108-60-1
ND
ug/L
16.7
3.1
1
11 /02/21 05:10
11 /03/21 00:48
87-86-5
ND
ug/L
8.3
1.7
1
11 /02/21 05:10
11 /03/21 00:48
85-01-8
ND
ug/L
8.3
1.1
1
11 /02/21 05:10
11 /03/21 00:48
108-95-2
ND
ug/L
8.3
1.8
1
11 /02/21 05:10
11 /03/21 00:48
129-00-0
ND
ug/L
8.3
1.4
1
11/02/2105:10
11/03/2100:48
120-82-1
ND
ug/L
8.3
1.2
1
11 /02/21 05:10
11 /03/21 00:48
95-95-4
ND
ug/L
8.3
1.3
1
11 /02/21 05:10
11 /03/21 00:48
88-06-2
47
%
10-144
1
11 /02/21 05:10
11 /03/21 00:48
4165-60-0
45
%
10-130
1
11 /02/21 05:10
11 /03/21 00:48
321-60-8
77
%
34-163
1
11 /02/21 05:10
11 /03/21 00:48
1718-51-0
23
%
10-130
1
11 /02/21 05:10
11 /03/21 00:48
13127-88-3
27
%
10-130
1
11/02/2105:10
11/03/2100:48
367-12-4
57
%
10-144
1
11 /02/21 05:10
11 /03/21 00:48
118-79-6
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
ND
ug/L
25.0
5.1
1
11/03/2104:56
67-64-1
28.5
ug/L
1.0
0.34
1
11/03/2104:56
71-43-2
ND
ug/L
1.0
0.29
1
11/03/2104:56
108-86-1
ND
ug/L
1.0
0.47
1
11/03/2104:56
74-97-5
ND
ug/L
1.0
0.31
1
11/03/2104:56
75-27-4
ND
ug/L
1.0
0.34
1
11/03/2104:56
75-25-2
ND
ug/L
2.0
1.7
1
11/03/2104:56
74-83-9
ND
ug/L
5.0
4.0
1
11/03/2104:56
78-93-3
ND
ug/L
1.0
0.33
1
11/03/2104:56
56-23-5
ND
ug/L
1.0
0.28
1
11/03/2104:56
108-90-7
ND
ug/L
1.0
0.65
1
11/03/2104:56
75-00-3
9.3
ug/L
1.0
0.43
1
11/03/21 04:56
67-66-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: GW-3 Lab ID: 92569749003 Collected: 10/28/21 11:55 Received: 11/01/21 07:10 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Date: 11 /11 /2021 09:47 AM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.54
1
11/03/2104:56
74-87-3
ND
ug/L
1.0
0.32
1
11/03/2104:56
95-49-8
ND
ug/L
1.0
0.32
1
11/03/2104:56
106-43-4
ND
ug/L
2.0
0.34
1
11/03/2104:56
96-12-8
ND
ug/L
1.0
0.36
1
11/03/2104:56
124-48-1
ND
ug/L
1.0
0.27
1
11/03/2104:56
106-93-4
ND
ug/L
1.0
0.39
1
11/03/2104:56
74-95-3
ND
ug/L
1.0
0.34
1
11/03/2104:56
95-50-1
ND
ug/L
1.0
0.34
1
11/03/2104:56
541-73-1
ND
ug/L
1.0
0.33
1
11/03/2104:56
106-46-7
ND
ug/L
1.0
0.35
1
11 /03/21 04:56
75-71-8
ND
ug/L
1.0
0.37
1
11/03/2104:56
75-34-3
10.3
ug/L
1.0
0.32
1
11/03/2104:56
107-06-2
ND
ug/L
1.0
0.35
1
11/03/2104:56
75-35-4
ND
ug/L
1.0
0.38
1
11/03/2104:56
156-59-2
ND
ug/L
1.0
0.40
1
11/03/2104:56
156-60-5
ND
ug/L
1.0
0.36
1
11/03/2104:56
78-87-5
ND
ug/L
1.0
0.28
1
11/03/2104:56
142-28-9
ND
ug/L
1.0
0.39
1
11/03/2104:56
594-20-7
ND
ug/L
1.0
0.43
1
11/03/2104:56
563-58-6
ND
ug/L
1.0
0.36
1
11 /03/21 04:56
10061-01-5
ND
ug/L
1.0
0.36
1
11 /03/21 04:56
10061-02-6
0.32J
ug/L
1.0
0.31
1
11/03/2104:56
108-20-3
ND
ug/L
1.0
0.30
1
11 /03/21 04:56
100-41-4
ND
ug/L
2.0
1.5
1
11/03/2104:56
87-68-3
ND
ug/L
5.0
0.48
1
11 /03/21 04:56
591-78-6
ND
ug/L
1.0
0.41
1
11/03/2104:56
99-87-6
ND
ug/L
5.0
2.0
1
11/03/2104:56
75-09-2
ND
ug/L
5.0
2.7
1
11/03/2104:56
108-10-1
ND
ug/L
1.0
0.42
1
11/03/2104:56
1634-04-4
0.811
ug/L
1.0
0.64
1
11/03/21 04:56
91-20-3
ND
ug/L
1.0
0.29
1
11/03/2104:56
100-42-5
ND
ug/L
1.0
0.31
1
11/03/2104:56
630-20-6
ND
ug/L
1.0
0.22
1
11/03/2104:56
79-34-5
ND
ug/L
1.0
0.29
1
11/03/2104:56
127-18-4
ND
ug/L
1.0
0.48
1
11/03/2104:56
108-88-3
ND
ug/L
1.0
0.81
1
11 /03/21 04:56
87-61-6
ND
ug/L
1.0
0.64
1
11/03/2104:56
120-82-1
ND
ug/L
1.0
0.33
1
11 /03/21 04:56
71-55-6
ND
ug/L
1.0
0.32
1
11/03/2104:56
79-00-5
ND
ug/L
1.0
0.38
1
11 /03/21 04:56
79-01-6
ND
ug/L
1.0
0.30
1
11/03/2104:56
75-69-4
ND
ug/L
1.0
0.26
1
11/03/2104:56
96-18-4
ND
ug/L
2.0
1.3
1
11/03/2104:56
108-05-4
ND
ug/L
1.0
0.39
1
11 /03/21 04:56
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 16 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: GW-3
Lab ID:
92569749003
Collected:
10/28/21 11:55
Received: 11/01/21 07:10 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical
Method: EPA 8260D
Pace Analytical
Services
- Charlotte
Xylene (Total)
ND
ug/L
1.0
0.34
1
11/03/21 04:56
1330-20-7
m&p-Xylene
ND
ug/L
2.0
0.71
1
11/03/21 04:56
179601-23-1
o-Xylene
ND
ug/L
1.0
0.34
1
11/03/21 04:56
95-47-6
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
11/03/21 04:56
460-00-4
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
11/03/21 04:56
17060-07-0
Toluene-d8 (S)
104
%
70-130
1
11/03/21 04:56
2037-26-5
Date: 11 /11 /2021 09:47 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: GW-4 Lab ID: 92569749004 Collected: 10/28/21 12:10 Received: 11/01/21 07:10 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Acenaphthene
ND
ug/L
9.1
1.8
1
11/02/21 05:10
11/03/21 01:13
83-32-9
Acenaphthylene
ND
ug/L
9.1
1.8
1
11/02/21 05:10
11/03/21 01:13
208-96-8
Aniline
ND
ug/L
9.1
1.5
1
11/02/21 05:10
11/03/21 01:13
62-53-3
Anthracene
ND
ug/L
9.1
2.1
1
11/02/21 05:10
11/03/21 01:13
120-12-7
Benzo(a)anthracene
ND
ug/L
9.1
2.4
1
11/02/21 05:10
11/03/21 01:13
56-55-3
Benzo(a)pyrene
ND
ug/L
9.1
2.5
1
11/02/21 05:10
11/03/21 01:13
50-32-8
Benzo(b)fluoranthene
ND
ug/L
9.1
2.4
1
11/02/21 05:10
11/03/21 01:13
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
9.1
2.6
1
11/02/21 05:10
11/03/21 01:13
191-24-2
Benzo(k)fluoranthene
ND
ug/L
9.1
2.5
1
11/02/21 05:10
11/03/21 01:13
207-08-9
Benzoic Acid
ND
ug/L
45.5
3.1
1
11/02/21 05:10
11/03/21 01:13
65-85-0
Benzyl alcohol
ND
ug/L
18.2
2.6
1
11/02/21 05:10
11/03/21 01:13
100-51-6
4-Bromophenylphenyl ether
ND
ug/L
9.1
1.6
1
11/02/21 05:10
11/03/21 01:13
101-55-3
Butylbenzylphthalate
ND
ug/L
9.1
2.9
1
11/02/21 05:10
11/03/21 01:13
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
9.1
3.0
1
11/02/21 05:10
11/03/21 01:13
59-50-7
4-Chloroaniline
ND
ug/L
18.2
3.3
1
11/02/21 05:10
11/03/21 01:13
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
9.1
1.7
1
11/02/21 05:10
11/03/21 01:13
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
9.1
1.7
1
11/02/21 05:10
11/03/21 01:13
111-44-4
2-Chloronaphthalene
ND
ug/L
9.1
1.6
1
11/02/21 05:10
11/03/21 01:13
91-58-7
2-Chlorophenol
ND
ug/L
9.1
1.1
1
11/02/21 05:10
11/03/21 01:13
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
9.1
1.8
1
11/02/21 05:10
11/03/21 01:13
7005-72-3
Chrysene
ND
ug/L
9.1
2.5
1
11/02/21 05:10
11/03/21 01:13
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
9.1
2.7
1
11/02/21 05:10
11/03/21 01:13
53-70-3
Dibenzofuran
ND
ug/L
9.1
1.9
1
11/02/21 05:10
11/03/21 01:13
132-64-9
1,2-Dichlorobenzene
ND
ug/L
9.1
1.6
1
11/02/21 05:10
11/03/21 01:13
95-50-1
1,3-Dichlorobenzene
ND
ug/L
9.1
1.5
1
11/02/21 05:10
11/03/21 01:13
541-73-1
1,4-Dichlorobenzene
ND
ug/L
9.1
1.5
1
11/02/21 05:10
11/03/21 01:13
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
18.2
7.4
1
11/02/21 05:10
11/03/21 01:13
91-94-1
2,4-Dichlorophenol
ND
ug/L
9.1
1.3
1
11/02/21 05:10
11/03/21 01:13
120-83-2
Diethylphthalate
ND
ug/L
9.1
1.9
1
11/02/21 05:10
11/03/21 01:13
84-66-2
2,4-Dimethylphenol
ND
ug/L
9.1
1.5
1
11/02/21 05:10
11/03/21 01:13
105-67-9
Dimethylphthalate
ND
ug/L
9.1
1.9
1
11/02/21 05:10
11/03/21 01:13
131-11-3
Di-n-butylphthalate
ND
ug/L
9.1
2.0
1
11/02/21 05:10
11/03/21 01:13
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
18.2
3.1
1
11/02/21 05:10
11/03/21 01:13
534-52-1
2,4-Dinitrophenol
ND
ug/L
45.5
23.6
1
11/02/21 05:10
11/03/21 01:13
51-28-5
2,4-Dinitrotoluene
ND
ug/L
9.1
1.5
1
11/02/21 05:10
11/03/21 01:13
121-14-2
2,6-Dinitrotoluene
ND
ug/L
9.1
1.6
1
11/02/21 05:10
11/03/21 01:13
606-20-2
Di-n-octylphthalate
ND
ug/L
9.1
3.6
1
11/02/21 05:10
11/03/21 01:13
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.5
3.4
1
11/02/21 05:10
11/03/21 01:13
117-81-7
Fluoranthene
ND
ug/L
9.1
2.0
1
11/02/21 05:10
11/03/21 01:13
206-44-0
Fluorene
ND
ug/L
9.1
1.9
1
11/02/21 05:10
11/03/21 01:13
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
9.1
1.6
1
11/02/21 05:10
11/03/21 01:13
87-68-3
Hexachlorobenzene
ND
ug/L
9.1
2.0
1
11/02/21 05:10
11/03/21 01:13
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
9.1
1.4
1
11/02/21 05:10
11/03/21 01:13
77-47-4
Hexachloroethane
ND
ug/L
9.1
1.3
1
11/02/21 05:10
11/03/21 01:13
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
9.1
2.6
1
11/02/21 05:10
11/03/21 01:13
193-39-5
REPORT OF LABORATORY ANALYSIS
L2
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: GW-4 Lab ID: 92569749004 Collected: 10/28/21 12:10 Received: 11/01/21 07:10 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E RVE
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Date: 11 /11 /2021 09:47 AM
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services
- Charlotte
ND
ug/L
9.1
1.5
1
11/02/2105:10
11/03/2101:13
78-59-1
ND
ug/L
9.1
1.8
1
11/02/2105:10
11/03/2101:13
90-12-0
ND
ug/L
9.1
1.7
1
11 /02/21 05:10
11 /03/21 01:13
91-57-6
ND
ug/L
9.1
1.7
1
11 /02/21 05:10
11 /03/21 01:13
95-48-7
ND
ug/L
9.1
1.1
1
11 /02/21 05:10
11 /03/21 01:13
15831-10-4
ND
ug/L
9.1
1.9
1
11 /02/21 05:10
11 /03/21 01:13
91-20-3
ND
ug/L
18.2
2.7
1
11 /02/21 05:10
11 /03/21 01:13
88-74-4
ND
ug/L
18.2
3.4
1
11 /02/21 05:10
11 /03/21 01:13
99-09-2
ND
ug/L
18.2
4.6
1
11 /02/21 05:10
11 /03/21 01:13
100-01-6
ND
ug/L
9.1
1.7
1
11 /02/21 05:10
11 /03/21 01:13
98-95-3
ND
ug/L
9.1
1.3
1
11 /02/21 05:10
11 /03/21 01:13
88-75-5
ND
ug/L
45.5
6.0
1
11 /02/21 05:10
11 /03/21 01:13
100-02-7
ND
ug/L
9.1
1.7
1
11 /02/21 05:10
11 /03/21 01:13
62-75-9
ND
ug/L
9.1
1.2
1
11 /02/21 05:10
11 /03/21 01:13
621-64-7
ND
ug/L
9.1
2.7
1
11 /02/21 05:10
11 /03/21 01:13
86-30-6
ND
ug/L
9.1
1.0
1
11/02/2105:10
11/03/2101:13
108-60-1
ND
ug/L
18.2
3.4
1
11 /02/21 05:10
11 /03/21 01:13
87-86-5
ND
ug/L
9.1
1.8
1
11 /02/21 05:10
11 /03/21 01:13
85-01-8
ND
ug/L
9.1
1.2
1
11 /02/21 05:10
11 /03/21 01:13
108-95-2
ND
ug/L
9.1
2.0
1
11 /02/21 05:10
11 /03/21 01:13
129-00-0
ND
ug/L
9.1
1.6
1
11/02/2105:10
11/03/2101:13
120-82-1
ND
ug/L
9.1
1.3
1
11 /02/21 05:10
11 /03/21 01:13
95-95-4
ND
ug/L
9.1
1.4
1
11 /02/21 05:10
11 /03/21 01:13
88-06-2
49
%
10-144
1
11 /02/21 05:10
11 /03/21 01:13
4165-60-0
47
%
10-130
1
11 /02/21 05:10
11 /03/21 01:13
321-60-8
81
%
34-163
1
11 /02/21 05:10
11 /03/21 01:13
1718-51-0
26
%
10-130
1
11 /02/21 05:10
11 /03/21 01:13
13127-88-3
33
%
10-130
1
11/02/2105:10
11/03/2101:13
367-12-4
68
%
10-144
1
11 /02/21 05:10
11 /03/21 01:13
118-79-6
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
ND
ug/L
25.0
5.1
1
11/03/2105:14
67-64-1
ND
ug/L
1.0
0.34
1
11 /03/21 05:14
71-43-2
ND
ug/L
1.0
0.29
1
11/03/2105:14
108-86-1
ND
ug/L
1.0
0.47
1
11/03/2105:14
74-97-5
ND
ug/L
1.0
0.31
1
11/03/2105:14
75-27-4
ND
ug/L
1.0
0.34
1
11/03/2105:14
75-25-2
ND
ug/L
2.0
1.7
1
11/03/2105:14
74-83-9
ND
ug/L
5.0
4.0
1
11/03/2105:14
78-93-3
ND
ug/L
1.0
0.33
1
11/03/2105:14
56-23-5
ND
ug/L
1.0
0.28
1
11/03/2105:14
108-90-7
ND
ug/L
1.0
0.65
1
11/03/2105:14
75-00-3
ND
ug/L
1.0
0.43
1
11/03/2105:14
67-66-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 19 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: GW-4 Lab ID: 92569749004 Collected: 10/28/21 12:10 Received: 11/01/21 07:10 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Chloromethane
ND
ug/L
1.0
0.54
1
11/03/21 05:14
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
0.32
1
11/03/21 05:14
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
0.32
1
11/03/21 05:14
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
11/03/21 05:14
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
11/03/21 05:14
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
11/03/21 05:14
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
11/03/21 05:14
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
11/03/21 05:14
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
0.34
1
11/03/21 05:14
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
11/03/21 05:14
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
0.35
1
11/03/21 05:14
75-71-8
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
11/03/21 05:14
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
11/03/21 05:14
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
11/03/21 05:14
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
0.38
1
11/03/21 05:14
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
0.40
1
11/03/21 05:14
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.36
1
11/03/21 05:14
78-87-5
1,3-Dichloropropane
ND
ug/L
1.0
0.28
1
11/03/21 05:14
142-28-9
2,2-Dichloropropane
ND
ug/L
1.0
0.39
1
11/03/21 05:14
594-20-7
1,1-Dichloropropene
ND
ug/L
1.0
0.43
1
11/03/21 05:14
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
11/03/21 05:14
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
11/03/21 05:14
10061-02-6
Diisopropyl ether
ND
ug/L
1.0
0.31
1
11/03/21 05:14
108-20-3
Ethylbenzene
ND
ug/L
1.0
0.30
1
11/03/21 05:14
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1.5
1
11/03/21 05:14
87-68-3
2-Hexanone
ND
ug/L
5.0
0.48
1
11/03/21 05:14
591-78-6
p-Isopropyltoluene
ND
ug/L
1.0
0.41
1
11/03/21 05:14
99-87-6
Methylene Chloride
ND
ug/L
5.0
2.0
1
11/03/21 05:14
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
2.7
1
11/03/21 05:14
108-10-1
Methyl-tert-butyl ether
ND
ug/L
1.0
0.42
1
11/03/21 05:14
1634-04-4
Naphthalene
ND
ug/L
1.0
0.64
1
11/03/21 05:14
91-20-3
Styrene
ND
ug/L
1.0
0.29
1
11/03/21 05:14
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.31
1
11/03/21 05:14
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
11/03/21 05:14
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.29
1
11/03/21 05:14
127-18-4
Toluene
ND
ug/L
1.0
0.48
1
11/03/21 05:14
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
1.0
0.81
1
11/03/21 05:14
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
1.0
0.64
1
11/03/21 05:14
120-82-1
1,1,1-Trichloroethane
ND
ug/L
1.0
0.33
1
11/03/21 05:14
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.32
1
11/03/21 05:14
79-00-5
Trichloroethene
ND
ug/L
1.0
0.38
1
11/03/21 05:14
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.30
1
11/03/21 05:14
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.26
1
11/03/21 05:14
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.3
1
11/03/21 05:14
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.39
1
11/03/21 05:14
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC.
Page 20 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: GW-4
Lab ID:
92569749004
Collected:
10/28/21 12:10
Received: 11/01/21 07:10 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical
Method: EPA 8260D
Pace Analytical
Services
- Charlotte
Xylene (Total)
ND
ug/L
1.0
0.34
1
11/03/21 05:14
1330-20-7
m&p-Xylene
ND
ug/L
2.0
0.71
1
11/03/21 05:14
179601-23-1
o-Xylene
ND
ug/L
1.0
0.34
1
11/03/21 05:14
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
11/03/21 05:14
460-00-4
1,2-Dichloroethane-d4 (S)
96
%
70-130
1
11/03/21 05:14
17060-07-0
Toluene-d8 (S)
104
%
70-130
1
11/03/21 05:14
2037-26-5
Date: 11 /11 /2021 09:47 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 21 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: SB-1 Lab ID: 92569749005 Collected: 10/28/21 10:00 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical
Services
-Asheville
Arsenic
1.8J
mg/kg
2.4
0.48
1
11/02/2113:30
11/08/2104:13
7440-38-2
Barium
190
mg/kg
0.97
0.24
1
11/02/2113:30
11/08/2104:13
7440-39-3
Cadmium
0.40
mg/kg
0.097
0.048
1
11/02/2113:30
11/08/2104:13
7440-43-9
Chromium
34.7
mg/kg
0.48
0.24
1
11/02/2113:30
11/08/2104:13
7440-47-3
Lead
465
mg/kg
0.97
0.24
1
11/02/2113:30
11/08/2104:13
7439-92-1
Selenium
1.1
mg/kg
0.97
0.48
1
11/02/2113:30
11/08/2104:13
7782-49-2
Silver
0.45J
mg/kg
0.48
0.24
1
11/02/2113:30
11/08/2104:13
7440-22-4
7471 Mercury
Analytical
Method: EPA 7471 B Preparation
Method: EPA 7471 B
Pace Analytical
Services
-Asheville
Mercury
0.22
mg/kg
0.012
0.0095
2
11/03/2116:30
11/09/2113:53
7439-97-6 M1,R1
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation
Method: EPA 3546
Pace Analytical
Services
- Charlotte
Acenaphthene
ND
mg/kg
4.4
1.5
10
11/02/21 16:39
11/05/21 08:14
83-32-9
Acenaphthylene
ND
mg/kg
4.4
1.5
10
11/02/21 16:39
11/05/21 08:14
208-96-8
Aniline
ND
mg/kg
4.4
1.7
10
11/02/21 16:39
11/05/21 08:14
62-53-3
Anthracene
ND
mg/kg
4.4
1.4
10
11/02/21 16:39
11/05/21 08:14
120-12-7
Benzo(a)anthracene
ND
mg/kg
4.4
1.5
10
11/02/21 16:39
11/05/21 08:14
56-55-3
Benzo(a)pyrene
ND
mg/kg
4.4
1.5
10
11/02/21 16:39
11/05/21 08:14
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
4.4
1.5
10
11/02/21 16:39
11/05/21 08:14
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
4.4
1.7
10
11/02/21 16:39
11/05/21 08:14
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
4.4
1.5
10
11/02/21 16:39
11/05/21 08:14
207-08-9
Benzoic Acid
ND
mg/kg
21.8
9.4
10
11/02/21 16:39
11/05/21 08:14
65-85-0
Benzyl alcohol
ND
mg/kg
8.7
3.3
10
11/02/21 16:39
11/05/21 08:14
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
4.4
1.7
10
11/02/21 16:39
11/05/21 08:14
101-55-3
Butylbenzylphthalate
ND
mg/kg
4.4
1.8
10
11/02/21 16:39
11/05/21 08:14
85-68-7
4-ChIoro-3-methyl phenol
ND
mg/kg
8.7
3.1
10
11/02/21 16:39
11/05/21 08:14
59-50-7
4-Chloroaniline
ND
mg/kg
8.7
3.4
10
11/02/21 16:39
11/05/21 08:14
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
4.4
1.8
10
11/02/21 16:39
11/05/21 08:14
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
4.4
1.6
10
11/02/21 16:39
11/05/21 08:14
111-44-4
2-Chloronaphthalene
ND
mg/kg
4.4
1.7
10
11/02/21 16:39
11/05/21 08:14
91-58-7
2-Chlorophenol
ND
mg/kg
4.4
1.6
10
11/02/21 16:39
11/05/21 08:14
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
4.4
1.6
10
11/02/21 16:39
11/05/21 08:14
7005-72-3
Chrysene
ND
mg/kg
4.4
1.6
10
11/02/21 16:39
11/05/21 08:14
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
4.4
1.7
10
11/02/21 16:39
11/05/21 08:14
53-70-3
Dibenzofuran
ND
mg/kg
4.4
1.6
10
11/02/21 16:39
11/05/21 08:14
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
4.4
1.6
10
11/02/21 16:39
11/05/21 08:14
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
4.4
1.5
10
11/02/21 16:39
11/05/21 08:14
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
4.4
1.7
10
11/02/21 16:39
11/05/21 08:14
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
8.7
2.9
10
11/02/21 16:39
11/05/21 08:14
91-94-1 IL
2,4-Dichlorophenol
ND
mg/kg
4.4
1.7
10
11/02/21 16:39
11/05/21 08:14
120-83-2
Diethylphthalate
ND
mg/kg
4.4
1.6
10
11/02/21 16:39
11/05/21 08:14
84-66-2
2,4-Dimethylphenol
ND
mg/kg
4.4
1.8
10
11/02/21 16:39
11/05/21 08:14
105-67-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 22 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: S13-1 Lab ID: 92569749005 Collected: 10/28/21 10:00 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methyl phenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2- Ethyl hexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
mg/kg
4.4
1.6
10
11 /02/21 16:39
11 /05/21 08:14
131-11-3
ND
mg/kg
4.4
1.5
10
11 /02/21 16:39
11 /05/21 08:14
84-74-2
ND
mg/kg
8.7
4.1
10
11 /02/21 16:39
11 /05/21 08:14
534-52-1
ND
mg/kg
21.8
13.5
10
11 /02/21 16:39
11 /05/21 08:14
51-28-5
ND
mg/kg
4.4
1.7
10
11 /02/21 16:39
11 /05/21 08:14
121-14-2
ND
mg/kg
4.4
1.6
10
11 /02/21 16:39
11 /05/21 08:14
606-20-2
ND
mg/kg
4.4
1.7
10
11 /02/21 16:39
11 /05/21 08:14
117-84-0
ND
mg/kg
4.4
1.7
10
11 /02/21 16:39
11 /05/21 08:14
117-81-7
ND
mg/kg
4.4
1.5
10
11 /02/21 16:39
11 /05/21 08:14
206-44-0
ND
mg/kg
4.4
1.5
10
11 /02/21 16:39
11 /05/21 08:14
86-73-7
ND
mg/kg
4.4
1.9
10
11 /02/21 16:39
11 /05/21 08:14
87-68-3
ND
mg/kg
4.4
1.7
10
11 /02/21 16:39
11 /05/21 08:14
118-74-1
ND
mg/kg
4.4
2.5
10
11 /02/21 16:39
11 /05/21 08:14
77-47-4
ND
mg/kg
4.4
1.7
10
11 /02/21 16:39
11 /05/21 08:14
67-72-1
ND
mg/kg
4.4
1.7
10
11 /02/21 16:39
11 /05/21 08:14
193-39-5
ND
mg/kg
4.4
1.9
10
11 /02/21 16:39
11 /05/21 08:14
78-59-1
ND
mg/kg
4.4
1.5
10
11 /02/21 16:39
11 /05/21 08:14
90-12-0
ND
mg/kg
4.4
1.7
10
11 /02/21 16:39
11 /05/21 08:14
91-57-6
ND
mg/kg
4.4
1.8
10
11 /02/21 16:39
11 /05/21 08:14
95-48-7
ND
mg/kg
4.4
1.8
10
11 /02/21 16:39
11 /05/21 08:14
15831-10-4
ND
mg/kg
4.4
1.5
10
11 /02/21 16:39
11 /05/21 08:14
91-20-3
ND
mg/kg
21.8
3.6
10
11 /02/21 16:39
11 /05/21 08:14
88-74-4
ND
mg/kg
21.8
3.4
10
11 /02/21 16:39
11 /05/21 08:14
99-09-2
IL
ND
mg/kg
8.7
3.3
10
11 /02/21 16:39
11 /05/21 08:14
100-01-6
ND
mg/kg
4.4
2.0
10
11 /02/21 16:39
11 /05/21 08:14
98-95-3
ND
mg/kg
4.4
1.9
10
11 /02/21 16:39
11 /05/21 08:14
88-75-5
ND
mg/kg
21.8
8.4
10
11 /02/21 16:39
11 /05/21 08:14
100-02-7
ND
mg/kg
4.4
1.5
10
11 /02/21 16:39
11 /05/21 08:14
62-75-9
ND
mg/kg
4.4
1.6
10
11 /02/21 16:39
11 /05/21 08:14
621-64-7
ND
mg/kg
4.4
1.5
10
11 /02/21 16:39
11 /05/21 08:14
86-30-6
ND
mg/kg
4.4
2.1
10
11 /02/21 16:39
11 /05/21 08:14
108-60-1
ND
mg/kg
8.7
4.3
10
11 /02/21 16:39
11 /05/21 08:14
87-86-5
ND
mg/kg
4.4
1.4
10
11 /02/21 16:39
11 /05/21 08:14
85-01-8
ND
mg/kg
4.4
1.9
10
11 /02/21 16:39
11 /05/21 08:14
108-95-2
ND
mg/kg
4.4
1.8
10
11 /02/21 16:39
11 /05/21 08:14
129-00-0
ND
mg/kg
4.4
1.4
10
11 /02/21 16:39
11 /05/21 08:14
110-86-1
ND
mg/kg
4.4
1.7
10
11 /02/21 16:39
11 /05/21 08:14
120-82-1
ND
mg/kg
4.4
2.0
10
11 /02/21 16:39
11 /05/21 08:14
95-95-4
v 1
ND
mg/kg
4.4
1.8
10
11 /02/21 16:39
11 /05/21 08:14
88-06-2
0
%
21-130
10
11/02/2116:39
11/05/2108:14
4165-60-0
D3,S4
0
%
19-130
10
11 /02/21 16:39
11 /05/21 08:14
321-60-8
S4
0
%
15-130
10
11 /02/21 16:39
11 /05/21 08:14
1718-51-0
S4
0
%
18-130
10
11 /02/21 16:39
11 /05/21 08:14
13127-88-3
S4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 23 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: SB-1 Lab ID: 92569749005 Collected: 10/28/21 10:00 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
0 % 18-130 10 11/02/2116:39 11/05/2108:14 367-12-4 S4
0 % 18-130 10 11/02/21 16:39 11 /05/21 08:14 118-79-6 S4
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
mg/kg
0.15
0.047
1
11/02/21 08:58
11/02/21 14:34
67-64-1
Benzene
ND
mg/kg
0.0073
0.0029
1
11/02/21 08:58
11/02/21 14:34
71-43-2
Bromobenzene
ND
mg/kg
0.0073
0.0024
1
11/02/21 08:58
11/02/21 14:34
108-86-1
Bromochloromethane
ND
mg/kg
0.0073
0.0022
1
11/02/21 08:58
11/02/21 14:34
74-97-5
Bromodichloromethane
ND
mg/kg
0.0073
0.0028
1
11/02/21 08:58
11/02/21 14:34
75-27-4
Bromoform
ND
mg/kg
0.0073
0.0026
1
11/02/21 08:58
11/02/21 14:34
75-25-2
Bromomethane
ND
mg/kg
0.015
0.012
1
11/02/21 08:58
11/02/21 14:34
74-83-9 v1
2-Butanone (MEK)
ND
mg/kg
0.15
0.035
1
11/02/21 08:58
11/02/21 14:34
78-93-3
n-Butylbenzene
ND
mg/kg
0.0073
0.0035
1
11/02/21 08:58
11/02/21 14:34
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0073
0.0032
1
11/02/21 08:58
11/02/21 14:34
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0073
0.0026
1
11/02/21 08:58
11/02/21 14:34
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0073
0.0027
1
11/02/21 08:58
11/02/21 14:34
56-23-5
Chlorobenzene
ND
mg/kg
0.0073
0.0014
1
11/02/21 08:58
11/02/21 14:34
108-90-7
Chloroethane
ND
mg/kg
0.015
0.0057
1
11/02/21 08:58
11/02/21 14:34
75-00-3
Chloroform
ND
mg/kg
0.0073
0.0045
1
11/02/21 08:58
11/02/21 14:34
67-66-3
Chloromethane
ND
mg/kg
0.015
0.0062
1
11/02/21 08:58
11/02/21 14:34
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0073
0.0026
1
11/02/21 08:58
11/02/21 14:34
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0073
0.0013
1
11/02/21 08:58
11/02/21 14:34
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0073
0.0028
1
11/02/21 08:58
11/02/21 14:34
96-12-8
Dibromochloromethane
ND
mg/kg
0.0073
0.0041
1
11/02/21 08:58
11/02/21 14:34
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0073
0.0032
1
11/02/21 08:58
11/02/21 14:34
106-93-4
Dibromomethane
ND
mg/kg
0.0073
0.0016
1
11/02/21 08:58
11/02/21 14:34
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0073
0.0026
1
11/02/21 08:58
11/02/21 14:34
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0073
0.0023
1
11/02/21 08:58
11/02/21 14:34
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0073
0.0019
1
11/02/21 08:58
11/02/21 14:34
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.015
0.0032
1
11/02/21 08:58
11/02/21 14:34
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0073
0.0030
1
11/02/21 08:58
11/02/21 14:34
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0073
0.0049
1
11/02/21 08:58
11/02/21 14:34
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0073
0.0030
1
11/02/21 08:58
11/02/21 14:34
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0073
0.0025
1
11/02/21 08:58
11/02/21 14:34
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0073
0.0026
1
11/02/21 08:58
11/02/21 14:34
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0073
0.0022
1
11/02/21 08:58
11/02/21 14:34
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0073
0.0023
1
11/02/21 08:58
11/02/21 14:34
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0073
0.0024
1
11/02/21 08:58
11/02/21 14:34
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0073
0.0035
1
11/02/21 08:58
11/02/21 14:34
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0073
0.0020
1
11/02/21 08:58
11/02/21 14:34
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0073
0.0025
1
11/02/21 08:58
11/02/21 14:34
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0073
0.0020
1
11/02/21 08:58
11/02/21 14:34
108-20-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 24 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: S13-1
Lab ID:
92569749005
Collected:
10/28/21
10:00
Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Ethylbenzene
0.0040J
mg/kg
0.0073
0.0034
1
11/02/21 08:58
11/02/21 14:34
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.015
0.012
1
11/02/21 08:58
11/02/21 14:34
87-68-3
2-Hexanone
ND
mg/kg
0.073
0.0071
1
11/02/21 08:58
11/02/21 14:34
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0073
0.0025
1
11/02/21 08:58
11/02/21 14:34
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0073
0.0036
1
11/02/21 08:58
11/02/21 14:34
99-87-6
Methylene Chloride
ND
mg/kg
0.029
0.020
1
11/02/21 08:58
11/02/21 14:34
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.073
0.0071
1
11/02/21 08:58
11/02/21 14:34
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0073
0.0027
1
11/02/21 08:58
11/02/21 14:34
1634-04-4
Naphthalene
0.014
mg/kg
0.0073
0.0039
1
11/02/21 08:58
11/02/21 14:34
91-20-3
n-Propylbenzene
ND
mg/kg
0.0073
0.0026
1
11/02/21 08:58
11/02/21 14:34
103-65-1
Styrene
ND
mg/kg
0.0073
0.0019
1
11/02/21 08:58
11/02/21 14:34
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0073
0.0028
1
11/02/21 08:58
11/02/21 14:34
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0073
0.0019
1
11/02/21 08:58
11/02/21 14:34
79-34-5
Tetrachloroethene
ND
mg/kg
0.0073
0.0023
1
11/02/21 08:58
11/02/21 14:34
127-18-4
Toluene
0.0051J
mg/kg
0.0073
0.0021
1
11/02/21 08:58
11/02/21 14:34
108-88-3
1,2,3-Trichlorobenzene
ND
mg/kg
0.0073
0.0059
1
11/02/21 08:58
11/02/21 14:34
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0073
0.0062
1
11/02/21 08:58
11/02/21 14:34
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0073
0.0038
1
11/02/21 08:58
11/02/21 14:34
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0073
0.0024
1
11/02/21 08:58
11/02/21 14:34
79-00-5
Trichloroethene
ND
mg/kg
0.0073
0.0019
1
11/02/21 08:58
11/02/21 14:34
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0073
0.0040
1
11/02/21 08:58
11/02/21 14:34
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.0073
0.0037
1
11/02/21 08:58
11/02/21 14:34
96-18-4
1,2,4-Trimethylbenzene
0.0084
mg/kg
0.0073
0.0020
1
11/02/21 08:58
11/02/21 14:34
95-63-6
1,3,5-Trimethylbenzene
ND
mg/kg
0.0073
0.0025
1
11/02/21 08:58
11/02/21 14:34
108-67-8
Vinyl acetate
ND
mg/kg
0.073
0.0053
1
11/02/21 08:58
11/02/21 14:34
108-05-4
Vinyl chloride
ND
mg/kg
0.015
0.0037
1
11/02/21 08:58
11/02/21 14:34
75-01-4
Xylene (Total)
0.0080J
mg/kg
0.015
0.0042
1
11/02/21 08:58
11/02/21 14:34
1330-20-7
m&p-Xylene
0.0080J
mg/kg
0.015
0.0050
1
11/02/21 08:58
11/02/21 14:34
179601-23-1
o-Xylene
ND
mg/kg
0.0073
0.0032
1
11/02/21 08:58
11/02/21 14:34
95-47-6
Surrogates
Toluene-d8 (S)
101
%
70-130
1
11/02/21 08:58
11/02/21 14:34
2037-26-5
4-Bromofluorobenzene (S)
98
%
69-134
1
11/02/21 08:58
11/02/21 14:34
460-00-4
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
11/02/21 08:58
11/02/21 14:34
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services - Charlotte
Percent Moisture
25.2
%
0.10
0.10
1
11/01/21 15:46
N2
Total Solids 2540 G-2011
Analytical
Method: SM 2540G Preparation Method:
SM
2540 G
Pace National
- Mt. Juliet
Total Solids
83.3
%
1
11/04/21 10:18
11/04/21 10:36
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 25 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: S13-1 Lab ID: 92569749005 Collected: 10/28/21 10:00 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Wet Chemistry 7199 Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Chromium, Hexavalent 1.32 mg/kg 1.20 0.306 1 11/04/21 18:00 11/09/21 18:58 18540-29-9
Date: 11 /11 /2021 09:47 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 26 of 87

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: SB-2 Lab ID: 92569749006 Collected: 10/28/21 10:25 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical
Services
-Asheville
Arsenic
0.80J
mg/kg
2.2
0.43
1
11/02/2113:30
11/08/2104:16
7440-38-2
Barium
141
mg/kg
0.86
0.22
1
11/02/2113:30
11/08/2104:16
7440-39-3
Cadmium
0.11
mg/kg
0.086
0.043
1
11/02/2113:30
11/08/2104:16
7440-43-9
Chromium
8.2
mg/kg
0.43
0.22
1
11/02/2113:30
11/08/2104:16
7440-47-3
Lead
5.9
mg/kg
0.86
0.22
1
11/02/2113:30
11/08/2104:16
7439-92-1
Selenium
0.51J
mg/kg
0.86
0.43
1
11/02/2113:30
11/08/2104:16
7782-49-2
Silver
0.59
mg/kg
0.43
0.22
1
11/02/2113:30
11/08/2104:16
7440-22-4
7471 Mercury
Analytical
Method: EPA 7471 B Preparation
Method: EPA
7471 B
Pace Analytical
Services
-Asheville
Mercury
ND
mg/kg
0.0056
0.0043
1
11/03/2116:30
11/09/2112:15
7439-97-6
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation
Method: EPA
3546
Pace Analytical
Services
- Charlotte
Acenaphthene
ND
mg/kg
0.37
0.13
1
11/02/21 16:39
11/03/21 14:21
83-32-9
Acenaphthylene
ND
mg/kg
0.37
0.13
1
11/02/21 16:39
11/03/21 14:21
208-96-8
Aniline
ND
mg/kg
0.37
0.15
1
11/02/21 16:39
11/03/21 14:21
62-53-3
Anthracene
ND
mg/kg
0.37
0.12
1
11/02/21 16:39
11/03/21 14:21
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.37
0.12
1
11/02/21 16:39
11/03/21 14:21
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.37
0.13
1
11/02/21 16:39
11/03/21 14:21
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.37
0.12
1
11/02/21 16:39
11/03/21 14:21
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.37
0.14
1
11/02/21 16:39
11/03/21 14:21
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.37
0.13
1
11/02/21 16:39
11/03/21 14:21
207-08-9
Benzoic Acid
ND
mg/kg
1.9
0.80
1
11/02/21 16:39
11/03/21 14:21
65-85-0
Benzyl alcohol
ND
mg/kg
0.74
0.28
1
11/02/21 16:39
11/03/21 14:21
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.37
0.14
1
11/02/21 16:39
11/03/21 14:21
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.37
0.16
1
11/02/21 16:39
11/03/21 14:21
85-68-7
4-ChIoro-3-methyl phenol
ND
mg/kg
0.74
0.26
1
11/02/21 16:39
11/03/21 14:21
59-50-7
4-Chloroaniline
ND
mg/kg
0.74
0.29
1
11/02/21 16:39
11/03/21 14:21
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.37
0.15
1
11/02/21 16:39
11/03/21 14:21
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.37
0.14
1
11/02/21 16:39
11/03/21 14:21
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.37
0.15
1
11/02/21 16:39
11/03/21 14:21
91-58-7
2-Chlorophenol
ND
mg/kg
0.37
0.14
1
11/02/21 16:39
11/03/21 14:21
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.37
0.14
1
11/02/21 16:39
11/03/21 14:21
7005-72-3
Chrysene
ND
mg/kg
0.37
0.14
1
11/02/21 16:39
11/03/21 14:21
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.37
0.14
1
11/02/21 16:39
11/03/21 14:21
53-70-3
Dibenzofuran
ND
mg/kg
0.37
0.13
1
11/02/21 16:39
11/03/21 14:21
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.37
0.13
1
11/02/21 16:39
11/03/21 14:21
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.37
0.13
1
11/02/21 16:39
11/03/21 14:21
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.37
0.14
1
11/02/21 16:39
11/03/21 14:21
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
0.74
0.25
1
11/02/21 16:39
11/03/21 14:21
91-94-1 IL
2,4-Dichlorophenol
ND
mg/kg
0.37
0.15
1
11/02/21 16:39
11/03/21 14:21
120-83-2
Diethylphthalate
ND
mg/kg
0.37
0.14
1
11/02/21 16:39
11/03/21 14:21
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.37
0.15
1
11/02/21 16:39
11/03/21 14:21
105-67-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 27 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: S13-2 Lab ID: 92569749006 Collected: 10/28/21 10:25 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Dimethylphthalate
ND
mg/kg
0.37
0.14
1
11/02/21 16:39
11/03/21 14:21
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.37
0.13
1
11/02/21 16:39
11/03/21 14:21
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.74
0.35
1
11/02/21 16:39
11/03/21 14:21
534-52-1
2,4-Dinitrophenol
ND
mg/kg
1.9
1.1
1
11/02/21 16:39
11/03/21 14:21
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.37
0.14
1
11/02/21 16:39
11/03/21 14:21
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.37
0.14
1
11/02/21 16:39
11/03/21 14:21
606-20-2
Di-n-octylphthalate
ND
mg/kg
0.37
0.15
1
11/02/21 16:39
11/03/21 14:21
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.37
0.14
1
11/02/21 16:39
11/03/21 14:21
117-81-7
Fluoranthene
ND
mg/kg
0.37
0.13
1
11/02/21 16:39
11/03/21 14:21
206-44-0
Fluorene
ND
mg/kg
0.37
0.13
1
11/02/21 16:39
11/03/21 14:21
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.37
0.16
1
11/02/21 16:39
11/03/21 14:21
87-68-3
Hexachlorobenzene
ND
mg/kg
0.37
0.15
1
11/02/21 16:39
11/03/21 14:21
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.37
0.21
1
11/02/21 16:39
11/03/21 14:21
77-47-4
Hexachloroethane
ND
mg/kg
0.37
0.14
1
11/02/21 16:39
11/03/21 14:21
67-72-1
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.37
0.15
1
11/02/21 16:39
11/03/21 14:21
193-39-5
Isophorone
ND
mg/kg
0.37
0.17
1
11/02/21 16:39
11/03/21 14:21
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.37
0.13
1
11/02/21 16:39
11/03/21 14:21
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.37
0.15
1
11/02/21 16:39
11/03/21 14:21
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.37
0.15
1
11/02/21 16:39
11/03/21 14:21
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.37
0.15
1
11/02/21 16:39
11/03/21 14:21
15831-10-4
Naphthalene
ND
mg/kg
0.37
0.13
1
11/02/21 16:39
11/03/21 14:21
91-20-3
2-Nitroaniline
ND
mg/kg
1.9
0.30
1
11/02/21 16:39
11/03/21 14:21
88-74-4
3-Nitroaniline
ND
mg/kg
1.9
0.29
1
11/02/21 16:39
11/03/21 14:21
99-09-2
4-Nitroaniline
ND
mg/kg
0.74
0.28
1
11/02/21 16:39
11/03/21 14:21
100-01-6
Nitrobenzene
ND
mg/kg
0.37
0.17
1
11/02/21 16:39
11/03/21 14:21
98-95-3
2-Nitrophenol
ND
mg/kg
0.37
0.16
1
11/02/21 16:39
11/03/21 14:21
88-75-5
4-Nitrophenol
ND
mg/kg
1.9
0.72
1
11/02/21 16:39
11/03/21 14:21
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.37
0.13
1
11/02/21 16:39
11/03/21 14:21
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.37
0.14
1
11/02/21 16:39
11/03/21 14:21
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.37
0.13
1
11/02/21 16:39
11/03/21 14:21
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.37
0.18
1
11/02/21 16:39
11/03/21 14:21
108-60-1
Pentachlorophenol
ND
mg/kg
0.74
0.36
1
11/02/21 16:39
11/03/21 14:21
87-86-5
Phenanthrene
ND
mg/kg
0.37
0.12
1
11/02/21 16:39
11/03/21 14:21
85-01-8
Phenol
ND
mg/kg
0.37
0.17
1
11/02/21 16:39
11/03/21 14:21
108-95-2
Pyrene
ND
mg/kg
0.37
0.15
1
11/02/21 16:39
11/03/21 14:21
129-00-0
Pyridine
ND
mg/kg
0.37
0.12
1
11/02/21 16:39
11/03/21 14:21
110-86-1
1,2,4-Trichlorobenzene
ND
mg/kg
0.37
0.15
1
11/02/21 16:39
11/03/21 14:21
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.37
0.17
1
11/02/21 16:39
11/03/21 14:21
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.37
0.15
1
11/02/21 16:39
11/03/21 14:21
88-06-2
Surrogates
Nitrobenzene-d5(S)
42
%
21-130
1
11/02/21 16:39
11/03/21 14:21
4165-60-0
2-Fluorobiphenyl (S)
44
%
19-130
1
11/02/21 16:39
11/03/21 14:21
321-60-8
Terphenyl-d14 (S)
46
%
15-130
1
11/02/21 16:39
11/03/21 14:21
1718-51-0
Phenol-d6 (S)
42
%
18-130
1
11/02/21 16:39
11/03/21 14:21
13127-88-3
REPORT OF LABORATORY ANALYSIS
IL
v1
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 28 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: SB-2 Lab ID: 92569749006 Collected: 10/28/21 10:25 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Surrogates
2-Fluorophenol (S)
40
%
18-130
1
11/02/21 16:39
11/03/21 14:21
367-12-4
2,4,6-Tribromophenol (S)
40
%
18-130
1
11/02/21 16:39
11/03/21 14:21
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation Method: EPA
5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
mg/kg
0.11
0.035
1
11/02/21 08:58
11/02/21 14:51
67-64-1
Benzene
ND
mg/kg
0.0055
0.0022
1
11/02/21 08:58
11/02/21 14:51
71-43-2
Bromobenzene
ND
mg/kg
0.0055
0.0018
1
11/02/21 08:58
11/02/21 14:51
108-86-1
Bromochloromethane
ND
mg/kg
0.0055
0.0016
1
11/02/21 08:58
11/02/21 14:51
74-97-5
Bromodichloromethane
ND
mg/kg
0.0055
0.0021
1
11/02/21 08:58
11/02/21 14:51
75-27-4
Bromoform
ND
mg/kg
0.0055
0.0019
1
11/02/21 08:58
11/02/21 14:51
75-25-2
Bromomethane
ND
mg/kg
0.011
0.0087
1
11/02/21 08:58
11/02/21 14:51
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.11
0.026
1
11/02/21 08:58
11/02/21 14:51
78-93-3
n-Butylbenzene
ND
mg/kg
0.0055
0.0026
1
11/02/21 08:58
11/02/21 14:51
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0055
0.0024
1
11/02/21 08:58
11/02/21 14:51
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0055
0.0020
1
11/02/21 08:58
11/02/21 14:51
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0055
0.0021
1
11/02/21 08:58
11/02/21 14:51
56-23-5
Chlorobenzene
ND
mg/kg
0.0055
0.0011
1
11/02/21 08:58
11/02/21 14:51
108-90-7
Chloroethane
ND
mg/kg
0.011
0.0042
1
11/02/21 08:58
11/02/21 14:51
75-00-3
Chloroform
ND
mg/kg
0.0055
0.0033
1
11/02/21 08:58
11/02/21 14:51
67-66-3
Chloromethane
ND
mg/kg
0.011
0.0046
1
11/02/21 08:58
11/02/21 14:51
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0055
0.0019
1
11/02/21 08:58
11/02/21 14:51
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0055
0.00097
1
11/02/21 08:58
11/02/21 14:51
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0055
0.0021
1
11/02/21 08:58
11/02/21 14:51
96-12-8
Dibromochloromethane
ND
mg/kg
0.0055
0.0031
1
11/02/21 08:58
11/02/21 14:51
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0055
0.0024
1
11/02/21 08:58
11/02/21 14:51
106-93-4
Dibromomethane
ND
mg/kg
0.0055
0.0012
1
11/02/21 08:58
11/02/21 14:51
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0055
0.0020
1
11/02/21 08:58
11/02/21 14:51
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0055
0.0017
1
11/02/21 08:58
11/02/21 14:51
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0055
0.0014
1
11/02/21 08:58
11/02/21 14:51
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.011
0.0024
1
11/02/21 08:58
11/02/21 14:51
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0055
0.0023
1
11/02/21 08:58
11/02/21 14:51
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0055
0.0036
1
11/02/21 08:58
11/02/21 14:51
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0055
0.0023
1
11/02/21 08:58
11/02/21 14:51
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0055
0.0019
1
11/02/21 08:58
11/02/21 14:51
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0055
0.0019
1
11/02/21 08:58
11/02/21 14:51
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0055
0.0016
1
11/02/21 08:58
11/02/21 14:51
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0055
0.0017
1
11/02/21 08:58
11/02/21 14:51
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0055
0.0018
1
11/02/21 08:58
11/02/21 14:51
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0055
0.0026
1
11/02/21 08:58
11/02/21 14:51
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0055
0.0015
1
11/02/21 08:58
11/02/21 14:51
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0055
0.0019
1
11/02/21 08:58
11/02/21 14:51
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0055
0.0015
1
11/02/21 08:58
11/02/21 14:51
108-20-3
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 29 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: S13-2 Lab ID: 92569749006 Collected: 10/28/21 10:25 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Total Solids 2540 G-2011
Total Solids
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
mg/kg
0.0055
0.0026
1
11 /02/21 08:58
11 /02/21 14:51
100-41-4
ND
mg/kg
0.011
0.0090
1
11 /02/21 08:58
11 /02/21 14:51
87-68-3
ND
mg/kg
0.055
0.0053
1
11 /02/21 08:58
11 /02/21 14:51
591-78-6
ND
mg/kg
0.0055
0.0019
1
11 /02/21 08:58
11 /02/21 14:51
98-82-8
ND
mg/kg
0.0055
0.0027
1
11 /02/21 08:58
11 /02/21 14:51
99-87-6
ND
mg/kg
0.022
0.015
1
11 /02/21 08:58
11 /02/21 14:51
75-09-2
ND
mg/kg
0.055
0.0053
1
11/02/2108:58
11/02/2114:51
108-10-1
ND
mg/kg
0.0055
0.0021
1
11 /02/21 08:58
11 /02/21 14:51
1634-04-4
ND
mg/kg
0.0055
0.0029
1
11 /02/21 08:58
11 /02/21 14:51
91-20-3
ND
mg/kg
0.0055
0.0020
1
11 /02/21 08:58
11 /02/21 14:51
103-65-1
ND
mg/kg
0.0055
0.0014
1
11 /02/21 08:58
11 /02/21 14:51
100-42-5
ND
mg/kg
0.0055
0.0021
1
11 /02/21 08:58
11 /02/21 14:51
630-20-6
ND
mg/kg
0.0055
0.0014
1
11 /02/21 08:58
11 /02/21 14:51
79-34-5
ND
mg/kg
0.0055
0.0017
1
11 /02/21 08:58
11 /02/21 14:51
127-18-4
ND
mg/kg
0.0055
0.0016
1
11 /02/21 08:58
11 /02/21 14:51
108-88-3
ND
mg/kg
0.0055
0.0044
1
11 /02/21 08:58
11 /02/21 14:51
87-61-6
ND
mg/kg
0.0055
0.0046
1
11 /02/21 08:58
11 /02/21 14:51
120-82-1
ND
mg/kg
0.0055
0.0029
1
11 /02/21 08:58
11 /02/21 14:51
71-55-6
ND
mg/kg
0.0055
0.0018
1
11 /02/21 08:58
11 /02/21 14:51
79-00-5
ND
mg/kg
0.0055
0.0014
1
11 /02/21 08:58
11 /02/21 14:51
79-01-6
ND
mg/kg
0.0055
0.0030
1
11 /02/21 08:58
11 /02/21 14:51
75-69-4
ND
mg/kg
0.0055
0.0028
1
11 /02/21 08:58
11 /02/21 14:51
96-18-4
ND
mg/kg
0.0055
0.0015
1
11 /02/21 08:58
11 /02/21 14:51
95-63-6
ND
mg/kg
0.0055
0.0018
1
11 /02/21 08:58
11 /02/21 14:51
108-67-8
ND
mg/kg
0.055
0.0040
1
11 /02/21 08:58
11 /02/21 14:51
108-05-4
ND
mg/kg
0.011
0.0028
1
11 /02/21 08:58
11 /02/21 14:51
75-01-4
ND
mg/kg
0.011
0.0031
1
11 /02/21 08:58
11 /02/21 14:51
1330-20-7
ND
mg/kg
0.011
0.0038
1
11 /02/21 08:58
11 /02/21 14:51
179601-23-1
ND
mg/kg
0.0055
0.0024
1
11 /02/21 08:58
11 /02/21 14:51
95-47-6
101
%
70-130
1
11 /02/21 08:58
11 /02/21 14:51
2037-26-5
96
%
69-134
1
11 /02/21 08:58
11 /02/21 14:51
460-00-4
98
%
70-130
1
11 /02/21 08:58
11 /02/21 14:51
17060-07-0
Analytical Method: SW-846
Pace Analytical Services - Charlotte
12.4 % 0.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
88.5 %
11/01/21 15:46
1 11 /04/21 10:18 11 /04/21 10:36
REPORT OF LABORATORY ANALYSIS
N2
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Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 30 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: S13-2 Lab ID: 92569749006 Collected: 10/28/21 10:25 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Wet Chemistry 7199 Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Chromium, Hexavalent 3.52 mg/kg 1.13 0.288 1 11/04/21 18:00 11/09/21 19:04 18540-29-9
Date: 11 /11 /2021 09:47 AM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 31 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: SB-3 Lab ID: 92569749007 Collected: 10/28/21 10:40 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical
Services
-Asheville
Arsenic
0.84J
mg/kg
3.4
0.68
1
11/02/2113:30
11/08/2104:19
7440-38-2
Barium
42.1
mg/kg
1.4
0.34
1
11/02/2113:30
11/08/2104:19
7440-39-3
Cadmium
0.070J
mg/kg
0.14
0.068
1
11/02/2113:30
11/08/2104:19
7440-43-9
Chromium
8.1
mg/kg
0.68
0.34
1
11/02/2113:30
11/08/2104:19
7440-47-3
Lead
4.1
mg/kg
1.4
0.34
1
11/02/2113:30
11/08/2104:19
7439-92-1
Selenium
ND
mg/kg
1.4
0.68
1
11/02/2113:30
11/08/2104:19
7782-49-2
Silver
ND
mg/kg
0.68
0.34
1
11/02/2113:30
11/08/2104:19
7440-22-4
7471 Mercury
Analytical
Method: EPA 7471 B Preparation
Method: EPA
7471 B
Pace Analytical
Services
-Asheville
Mercury
0.0072
mg/kg
0.0058
0.0045
1
11/03/2116:30
11/09/2112:18
7439-97-6
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation
Method: EPA
3546
Pace Analytical
Services
- Charlotte
Acenaphthene
ND
mg/kg
0.49
0.17
1
11/02/21 16:39
11/03/21 14:51
83-32-9
Acenaphthylene
ND
mg/kg
0.49
0.17
1
11/02/21 16:39
11/03/21 14:51
208-96-8
Aniline
ND
mg/kg
0.49
0.19
1
11/02/21 16:39
11/03/21 14:51
62-53-3
Anthracene
ND
mg/kg
0.49
0.16
1
11/02/21 16:39
11/03/21 14:51
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.49
0.16
1
11/02/21 16:39
11/03/21 14:51
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.49
0.17
1
11/02/21 16:39
11/03/21 14:51
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.49
0.16
1
11/02/21 16:39
11/03/21 14:51
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.49
0.19
1
11/02/21 16:39
11/03/21 14:51
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.49
0.17
1
11/02/21 16:39
11/03/21 14:51
207-08-9
Benzoic Acid
ND
mg/kg
2.5
1.1
1
11/02/21 16:39
11/03/21 14:51
65-85-0
Benzyl alcohol
ND
mg/kg
0.98
0.37
1
11/02/21 16:39
11/03/21 14:51
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.49
0.19
1
11/02/21 16:39
11/03/21 14:51
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.49
0.21
1
11/02/21 16:39
11/03/21 14:51
85-68-7
4-ChIoro-3-methyl phenol
ND
mg/kg
0.98
0.35
1
11/02/21 16:39
11/03/21 14:51
59-50-7
4-Chloroaniline
ND
mg/kg
0.98
0.39
1
11/02/21 16:39
11/03/21 14:51
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.49
0.20
1
11/02/21 16:39
11/03/21 14:51
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.49
0.18
1
11/02/21 16:39
11/03/21 14:51
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.49
0.20
1
11/02/21 16:39
11/03/21 14:51
91-58-7
2-Chlorophenol
ND
mg/kg
0.49
0.18
1
11/02/21 16:39
11/03/21 14:51
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.49
0.18
1
11/02/21 16:39
11/03/21 14:51
7005-72-3
Chrysene
ND
mg/kg
0.49
0.18
1
11/02/21 16:39
11/03/21 14:51
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.49
0.19
1
11/02/21 16:39
11/03/21 14:51
53-70-3
Dibenzofuran
ND
mg/kg
0.49
0.18
1
11/02/21 16:39
11/03/21 14:51
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.49
0.18
1
11/02/21 16:39
11/03/21 14:51
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.49
0.17
1
11/02/21 16:39
11/03/21 14:51
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.49
0.19
1
11/02/21 16:39
11/03/21 14:51
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
0.98
0.33
1
11/02/21 16:39
11/03/21 14:51
91-94-1 IL
2,4-Dichlorophenol
ND
mg/kg
0.49
0.19
1
11/02/21 16:39
11/03/21 14:51
120-83-2
Diethylphthalate
ND
mg/kg
0.49
0.18
1
11/02/21 16:39
11/03/21 14:51
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.49
0.20
1
11/02/21 16:39
11/03/21 14:51
105-67-9
REPORT OF LABORATORY ANALYSIS
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Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 32 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: S13-3 Lab ID: 92569749007 Collected: 10/28/21 10:40 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Dimethylphthalate
ND
mg/kg
0.49
0.18
1
11/02/21 16:39
11/03/21 14:51
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.49
0.17
1
11/02/21 16:39
11/03/21 14:51
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.98
0.46
1
11/02/21 16:39
11/03/21 14:51
534-52-1
2,4-Dinitrophenol
ND
mg/kg
2.5
1.5
1
11/02/21 16:39
11/03/21 14:51
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.49
0.19
1
11/02/21 16:39
11/03/21 14:51
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.49
0.18
1
11/02/21 16:39
11/03/21 14:51
606-20-2
Di-n-octylphthalate
ND
mg/kg
0.49
0.19
1
11/02/21 16:39
11/03/21 14:51
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.49
0.19
1
11/02/21 16:39
11/03/21 14:51
117-81-7
Fluoranthene
ND
mg/kg
0.49
0.17
1
11/02/21 16:39
11/03/21 14:51
206-44-0
Fluorene
ND
mg/kg
0.49
0.17
1
11/02/21 16:39
11/03/21 14:51
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.49
0.21
1
11/02/21 16:39
11/03/21 14:51
87-68-3
Hexachlorobenzene
ND
mg/kg
0.49
0.19
1
11/02/21 16:39
11/03/21 14:51
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.49
0.28
1
11/02/21 16:39
11/03/21 14:51
77-47-4
Hexachloroethane
ND
mg/kg
0.49
0.19
1
11/02/21 16:39
11/03/21 14:51
67-72-1
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.49
0.19
1
11/02/21 16:39
11/03/21 14:51
193-39-5
Isophorone
ND
mg/kg
0.49
0.22
1
11/02/21 16:39
11/03/21 14:51
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.49
0.17
1
11/02/21 16:39
11/03/21 14:51
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.49
0.20
1
11/02/21 16:39
11/03/21 14:51
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.49
0.20
1
11/02/21 16:39
11/03/21 14:51
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.49
0.20
1
11/02/21 16:39
11/03/21 14:51
15831-10-4
Naphthalene
ND
mg/kg
0.49
0.17
1
11/02/21 16:39
11/03/21 14:51
91-20-3
2-Nitroaniline
ND
mg/kg
2.5
0.40
1
11/02/21 16:39
11/03/21 14:51
88-74-4
3-Nitroaniline
ND
mg/kg
2.5
0.39
1
11/02/21 16:39
11/03/21 14:51
99-09-2
4-Nitroaniline
ND
mg/kg
0.98
0.37
1
11/02/21 16:39
11/03/21 14:51
100-01-6
Nitrobenzene
ND
mg/kg
0.49
0.23
1
11/02/21 16:39
11/03/21 14:51
98-95-3
2-Nitrophenol
ND
mg/kg
0.49
0.21
1
11/02/21 16:39
11/03/21 14:51
88-75-5
4-Nitrophenol
ND
mg/kg
2.5
0.95
1
11/02/21 16:39
11/03/21 14:51
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.49
0.17
1
11/02/21 16:39
11/03/21 14:51
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.49
0.18
1
11/02/21 16:39
11/03/21 14:51
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.49
0.17
1
11/02/21 16:39
11/03/21 14:51
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.49
0.23
1
11/02/21 16:39
11/03/21 14:51
108-60-1
Pentachlorophenol
ND
mg/kg
0.98
0.48
1
11/02/21 16:39
11/03/21 14:51
87-86-5
Phenanthrene
ND
mg/kg
0.49
0.16
1
11/02/21 16:39
11/03/21 14:51
85-01-8
Phenol
ND
mg/kg
0.49
0.22
1
11/02/21 16:39
11/03/21 14:51
108-95-2
Pyrene
ND
mg/kg
0.49
0.20
1
11/02/21 16:39
11/03/21 14:51
129-00-0
Pyridine
ND
mg/kg
0.49
0.15
1
11/02/21 16:39
11/03/21 14:51
110-86-1
1,2,4-Trichlorobenzene
ND
mg/kg
0.49
0.19
1
11/02/21 16:39
11/03/21 14:51
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.49
0.22
1
11/02/21 16:39
11/03/21 14:51
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.49
0.20
1
11/02/21 16:39
11/03/21 14:51
88-06-2
Surrogates
Nitrobenzene-d5 (S)
41
%
21-130
1
11/02/21 16:39
11/03/21 14:51
4165-60-0
2-Fluorobiphenyl (S)
43
%
19-130
1
11/02/21 16:39
11/03/21 14:51
321-60-8
Terphenyl-d14 (S)
39
%
15-130
1
11/02/21 16:39
11/03/21 14:51
1718-51-0
Phenol-d6 (S)
42
%
18-130
1
11/02/21 16:39
11/03/21 14:51
13127-88-3
REPORT OF LABORATORY ANALYSIS
IL
v1
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 33 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: SB-3 Lab ID: 92569749007 Collected: 10/28/21 10:40 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Surrogates
2-Fluorophenol (S)
40
%
18-130
1
11/02/21 16:39
11/03/21 14:51
367-12-4
2,4,6-Tribromophenol (S)
40
%
18-130
1
11/02/21 16:39
11/03/21 14:51
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation
Method: EPA
5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
mg/kg
0.18
0.056
1
11/02/21 08:58
11/02/21 15:08
67-64-1
Benzene
ND
mg/kg
0.0088
0.0035
1
11/02/21 08:58
11/02/21 15:08
71-43-2
Bromobenzene
ND
mg/kg
0.0088
0.0029
1
11/02/21 08:58
11/02/21 15:08
108-86-1
Bromochloromethane
ND
mg/kg
0.0088
0.0026
1
11/02/21 08:58
11/02/21 15:08
74-97-5
Bromodichloromethane
ND
mg/kg
0.0088
0.0034
1
11/02/21 08:58
11/02/21 15:08
75-27-4
Bromoform
ND
mg/kg
0.0088
0.0031
1
11/02/21 08:58
11/02/21 15:08
75-25-2
Bromomethane
ND
mg/kg
0.018
0.014
1
11/02/21 08:58
11/02/21 15:08
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.18
0.042
1
11/02/21 08:58
11/02/21 15:08
78-93-3
n-Butylbenzene
ND
mg/kg
0.0088
0.0041
1
11/02/21 08:58
11/02/21 15:08
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0088
0.0039
1
11/02/21 08:58
11/02/21 15:08
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0088
0.0031
1
11/02/21 08:58
11/02/21 15:08
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0088
0.0033
1
11/02/21 08:58
11/02/21 15:08
56-23-5
Chlorobenzene
ND
mg/kg
0.0088
0.0017
1
11/02/21 08:58
11/02/21 15:08
108-90-7
Chloroethane
ND
mg/kg
0.018
0.0068
1
11/02/21 08:58
11/02/21 15:08
75-00-3
Chloroform
ND
mg/kg
0.0088
0.0053
1
11/02/21 08:58
11/02/21 15:08
67-66-3
Chloromethane
ND
mg/kg
0.018
0.0074
1
11/02/21 08:58
11/02/21 15:08
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0088
0.0031
1
11/02/21 08:58
11/02/21 15:08
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0088
0.0016
1
11/02/21 08:58
11/02/21 15:08
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0088
0.0034
1
11/02/21 08:58
11/02/21 15:08
96-12-8
Dibromochloromethane
ND
mg/kg
0.0088
0.0049
1
11/02/21 08:58
11/02/21 15:08
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0088
0.0039
1
11/02/21 08:58
11/02/21 15:08
106-93-4
Dibromomethane
ND
mg/kg
0.0088
0.0019
1
11/02/21 08:58
11/02/21 15:08
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0088
0.0032
1
11/02/21 08:58
11/02/21 15:08
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0088
0.0027
1
11/02/21 08:58
11/02/21 15:08
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0088
0.0023
1
11/02/21 08:58
11/02/21 15:08
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.018
0.0038
1
11/02/21 08:58
11/02/21 15:08
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0088
0.0036
1
11/02/21 08:58
11/02/21 15:08
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0088
0.0058
1
11/02/21 08:58
11/02/21 15:08
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0088
0.0036
1
11/02/21 08:58
11/02/21 15:08
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0088
0.0030
1
11/02/21 08:58
11/02/21 15:08
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0088
0.0031
1
11/02/21 08:58
11/02/21 15:08
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0088
0.0026
1
11/02/21 08:58
11/02/21 15:08
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0088
0.0027
1
11/02/21 08:58
11/02/21 15:08
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0088
0.0029
1
11/02/21 08:58
11/02/21 15:08
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0088
0.0042
1
11/02/21 08:58
11/02/21 15:08
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0088
0.0024
1
11/02/21 08:58
11/02/21 15:08
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0088
0.0030
1
11/02/21 08:58
11/02/21 15:08
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0088
0.0024
1
11/02/21 08:58
11/02/21 15:08
108-20-3
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 34 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: S13-3 Lab ID: 92569749007 Collected: 10/28/21 10:40 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Total Solids 2540 G-2011
Total Solids
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
mg/kg
0.0088
0.0041
1
11 /02/21 08:58
11 /02/21 15:08
100-41-4
ND
mg/kg
0.018
0.014
1
11 /02/21 08:58
11 /02/21 15:08
87-68-3
ND
mg/kg
0.088
0.0084
1
11 /02/21 08:58
11 /02/21 15:08
591-78-6
ND
mg/kg
0.0088
0.0030
1
11 /02/21 08:58
11 /02/21 15:08
98-82-8
ND
mg/kg
0.0088
0.0043
1
11 /02/21 08:58
11 /02/21 15:08
99-87-6
ND
mg/kg
0.035
0.024
1
11 /02/21 08:58
11 /02/21 15:08
75-09-2
ND
mg/kg
0.088
0.0084
1
11/02/2108:58
11/02/2115:08
108-10-1
ND
mg/kg
0.0088
0.0033
1
11 /02/21 08:58
11 /02/21 15:08
1634-04-4
ND
mg/kg
0.0088
0.0046
1
11 /02/21 08:58
11 /02/21 15:08
91-20-3
ND
mg/kg
0.0088
0.0031
1
11 /02/21 08:58
11 /02/21 15:08
103-65-1
ND
mg/kg
0.0088
0.0023
1
11 /02/21 08:58
11 /02/21 15:08
100-42-5
ND
mg/kg
0.0088
0.0034
1
11 /02/21 08:58
11 /02/21 15:08
630-20-6
ND
mg/kg
0.0088
0.0023
1
11 /02/21 08:58
11 /02/21 15:08
79-34-5
ND
mg/kg
0.0088
0.0028
1
11 /02/21 08:58
11 /02/21 15:08
127-18-4
ND
mg/kg
0.0088
0.0025
1
11 /02/21 08:58
11 /02/21 15:08
108-88-3
ND
mg/kg
0.0088
0.0071
1
11 /02/21 08:58
11 /02/21 15:08
87-61-6
ND
mg/kg
0.0088
0.0074
1
11 /02/21 08:58
11 /02/21 15:08
120-82-1
ND
mg/kg
0.0088
0.0046
1
11 /02/21 08:58
11 /02/21 15:08
71-55-6
ND
mg/kg
0.0088
0.0029
1
11 /02/21 08:58
11 /02/21 15:08
79-00-5
ND
mg/kg
0.0088
0.0023
1
11 /02/21 08:58
11 /02/21 15:08
79-01-6
ND
mg/kg
0.0088
0.0048
1
11 /02/21 08:58
11 /02/21 15:08
75-69-4
ND
mg/kg
0.0088
0.0044
1
11 /02/21 08:58
11 /02/21 15:08
96-18-4
ND
mg/kg
0.0088
0.0024
1
11 /02/21 08:58
11 /02/21 15:08
95-63-6
ND
mg/kg
0.0088
0.0029
1
11 /02/21 08:58
11 /02/21 15:08
108-67-8
ND
mg/kg
0.088
0.0064
1
11 /02/21 08:58
11 /02/21 15:08
108-05-4
ND
mg/kg
0.018
0.0045
1
11 /02/21 08:58
11 /02/21 15:08
75-01-4
ND
mg/kg
0.018
0.0050
1
11 /02/21 08:58
11 /02/21 15:08
1330-20-7
ND
mg/kg
0.018
0.0060
1
11 /02/21 08:58
11 /02/21 15:08
179601-23-1
ND
mg/kg
0.0088
0.0039
1
11 /02/21 08:58
11 /02/21 15:08
95-47-6
101
%
70-130
1
11 /02/21 08:58
11 /02/21 15:08
2037-26-5
97
%
69-134
1
11 /02/21 08:58
11 /02/21 15:08
460-00-4
97
%
70-130
1
11 /02/21 08:58
11 /02/21 15:08
17060-07-0
Analytical Method: SW-846
Pace Analytical Services - Charlotte
33.0 % 0.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
82.6 %
11/01/21 15:46
1 11 /04/21 10:18 11 /04/21 10:36
REPORT OF LABORATORY ANALYSIS
N2
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 35 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: S13-3 Lab ID: 92569749007 Collected: 10/28/21 10:40 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Wet Chemistry 7199 Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Chromium, Hexavalent 0.359J mg/kg 1.21 0.309 1 11/04/21 18:00 11/09/21 19:09 18540-29-9 J
Date: 11 /11 /2021 09:47 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 36 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: SB-4 Lab ID: 92569749008 Collected: 10/28/21 10:55 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical
Services
-Asheville
Arsenic
2.OJ
mg/kg
2.7
0.54
1
11/02/2113:30
11/08/2104:22
7440-38-2
Barium
42.3
mg/kg
1.1
0.27
1
11/02/2113:30
11/08/2104:22
7440-39-3
Cadmium
ND
mg/kg
0.11
0.054
1
11/02/2113:30
11/08/2104:22
7440-43-9
Chromium
2.8
mg/kg
0.54
0.27
1
11/02/2113:30
11/08/2104:22
7440-47-3
Lead
2.7
mg/kg
1.1
0.27
1
11/02/2113:30
11/08/2104:22
7439-92-1
Selenium
ND
mg/kg
1.1
0.54
1
11/02/2113:30
11/08/2104:22
7782-49-2
Silver
ND
mg/kg
0.54
0.27
1
11/02/2113:30
11/08/2104:22
7440-22-4
7471 Mercury
Analytical
Method: EPA 7471 B Preparation
Method: EPA
7471 B
Pace Analytical
Services
-Asheville
Mercury
ND
mg/kg
0.0050
0.0038
1
11/03/2116:30
11/09/2113:51
7439-97-6
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation
Method: EPA
3546
Pace Analytical
Services
- Charlotte
Acenaphthene
ND
mg/kg
0.39
0.14
1
11/02/21 16:39
11/03/21 15:22
83-32-9
Acenaphthylene
ND
mg/kg
0.39
0.14
1
11/02/21 16:39
11/03/21 15:22
208-96-8
Aniline
ND
mg/kg
0.39
0.15
1
11/02/21 16:39
11/03/21 15:22
62-53-3
Anthracene
ND
mg/kg
0.39
0.13
1
11/02/21 16:39
11/03/21 15:22
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.39
0.13
1
11/02/21 16:39
11/03/21 15:22
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.39
0.13
1
11/02/21 16:39
11/03/21 15:22
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.39
0.13
1
11/02/21 16:39
11/03/21 15:22
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.39
0.15
1
11/02/21 16:39
11/03/21 15:22
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.39
0.14
1
11/02/21 16:39
11/03/21 15:22
207-08-9
Benzoic Acid
ND
mg/kg
1.9
0.83
1
11/02/21 16:39
11/03/21 15:22
65-85-0
Benzyl alcohol
ND
mg/kg
0.78
0.29
1
11/02/21 16:39
11/03/21 15:22
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.39
0.15
1
11/02/21 16:39
11/03/21 15:22
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.39
0.16
1
11/02/21 16:39
11/03/21 15:22
85-68-7
4-ChIoro-3-methyl phenol
ND
mg/kg
0.78
0.27
1
11/02/21 16:39
11/03/21 15:22
59-50-7
4-Chloroaniline
ND
mg/kg
0.78
0.30
1
11/02/21 16:39
11/03/21 15:22
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.39
0.16
1
11/02/21 16:39
11/03/21 15:22
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.39
0.15
1
11/02/21 16:39
11/03/21 15:22
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.39
0.15
1
11/02/21 16:39
11/03/21 15:22
91-58-7
2-Chlorophenol
ND
mg/kg
0.39
0.15
1
11/02/21 16:39
11/03/21 15:22
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.39
0.14
1
11/02/21 16:39
11/03/21 15:22
7005-72-3
Chrysene
ND
mg/kg
0.39
0.14
1
11/02/21 16:39
11/03/21 15:22
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.39
0.15
1
11/02/21 16:39
11/03/21 15:22
53-70-3
Dibenzofuran
ND
mg/kg
0.39
0.14
1
11/02/21 16:39
11/03/21 15:22
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.39
0.14
1
11/02/21 16:39
11/03/21 15:22
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.39
0.14
1
11/02/21 16:39
11/03/21 15:22
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.39
0.15
1
11/02/21 16:39
11/03/21 15:22
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
0.78
0.26
1
11/02/21 16:39
11/03/21 15:22
91-94-1 IL
2,4-Dichlorophenol
ND
mg/kg
0.39
0.15
1
11/02/21 16:39
11/03/21 15:22
120-83-2
Diethylphthalate
ND
mg/kg
0.39
0.14
1
11/02/21 16:39
11/03/21 15:22
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.39
0.16
1
11/02/21 16:39
11/03/21 15:22
105-67-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 37 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: S13-4 Lab ID: 92569749008 Collected: 10/28/21 10:55 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Dimethylphthalate
ND
mg/kg
0.39
0.14
1
11/02/21 16:39
11/03/21 15:22
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.39
0.13
1
11/02/21 16:39
11/03/21 15:22
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.78
0.36
1
11/02/21 16:39
11/03/21 15:22
534-52-1
2,4-Dinitrophenol
ND
mg/kg
1.9
1.2
1
11/02/21 16:39
11/03/21 15:22
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.39
0.15
1
11/02/21 16:39
11/03/21 15:22
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.39
0.14
1
11/02/21 16:39
11/03/21 15:22
606-20-2
Di-n-octylphthalate
ND
mg/kg
0.39
0.15
1
11/02/21 16:39
11/03/21 15:22
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.39
0.15
1
11/02/21 16:39
11/03/21 15:22
117-81-7
Fluoranthene
ND
mg/kg
0.39
0.13
1
11/02/21 16:39
11/03/21 15:22
206-44-0
Fluorene
ND
mg/kg
0.39
0.14
1
11/02/21 16:39
11/03/21 15:22
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.39
0.17
1
11/02/21 16:39
11/03/21 15:22
87-68-3
Hexachlorobenzene
ND
mg/kg
0.39
0.15
1
11/02/21 16:39
11/03/21 15:22
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.39
0.22
1
11/02/21 16:39
11/03/21 15:22
77-47-4
Hexachloroethane
ND
mg/kg
0.39
0.15
1
11/02/21 16:39
11/03/21 15:22
67-72-1
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.39
0.15
1
11/02/21 16:39
11/03/21 15:22
193-39-5
Isophorone
ND
mg/kg
0.39
0.17
1
11/02/21 16:39
11/03/21 15:22
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.39
0.14
1
11/02/21 16:39
11/03/21 15:22
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.39
0.16
1
11/02/21 16:39
11/03/21 15:22
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.39
0.16
1
11/02/21 16:39
11/03/21 15:22
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.39
0.16
1
11/02/21 16:39
11/03/21 15:22
15831-10-4
Naphthalene
ND
mg/kg
0.39
0.13
1
11/02/21 16:39
11/03/21 15:22
91-20-3
2-Nitroaniline
ND
mg/kg
1.9
0.32
1
11/02/21 16:39
11/03/21 15:22
88-74-4
3-Nitroaniline
ND
mg/kg
1.9
0.30
1
11/02/21 16:39
11/03/21 15:22
99-09-2
4-Nitroaniline
ND
mg/kg
0.78
0.30
1
11/02/21 16:39
11/03/21 15:22
100-01-6
Nitrobenzene
ND
mg/kg
0.39
0.18
1
11/02/21 16:39
11/03/21 15:22
98-95-3
2-Nitrophenol
ND
mg/kg
0.39
0.17
1
11/02/21 16:39
11/03/21 15:22
88-75-5
4-Nitrophenol
ND
mg/kg
1.9
0.75
1
11/02/21 16:39
11/03/21 15:22
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.39
0.13
1
11/02/21 16:39
11/03/21 15:22
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.39
0.15
1
11/02/21 16:39
11/03/21 15:22
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.39
0.14
1
11/02/21 16:39
11/03/21 15:22
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.39
0.18
1
11/02/21 16:39
11/03/21 15:22
108-60-1
Pentachlorophenol
ND
mg/kg
0.78
0.38
1
11/02/21 16:39
11/03/21 15:22
87-86-5
Phenanthrene
ND
mg/kg
0.39
0.13
1
11/02/21 16:39
11/03/21 15:22
85-01-8
Phenol
ND
mg/kg
0.39
0.17
1
11/02/21 16:39
11/03/21 15:22
108-95-2
Pyrene
ND
mg/kg
0.39
0.16
1
11/02/21 16:39
11/03/21 15:22
129-00-0
Pyridine
ND
mg/kg
0.39
0.12
1
11/02/21 16:39
11/03/21 15:22
110-86-1
1,2,4-Trichlorobenzene
ND
mg/kg
0.39
0.15
1
11/02/21 16:39
11/03/21 15:22
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.39
0.18
1
11/02/21 16:39
11/03/21 15:22
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.39
0.16
1
11/02/21 16:39
11/03/21 15:22
88-06-2
Surrogates
Nitrobenzene-d5(S)
21
%
21-130
1
11/02/21 16:39
11/03/21 15:22
4165-60-0
2-Fluorobiphenyl (S)
24
%
19-130
1
11/02/21 16:39
11/03/21 15:22
321-60-8
Terphenyl-d14 (S)
27
%
15-130
1
11/02/21 16:39
11/03/21 15:22
1718-51-0
Phenol-d6 (S)
22
%
18-130
1
11/02/21 16:39
11/03/21 15:22
13127-88-3
REPORT OF LABORATORY ANALYSIS
IL
v1
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 38 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: SB-4 Lab ID: 92569749008 Collected: 10/28/21 10:55 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Surrogates
2-Fluorophenol (S)
21
%
18-130
1
11/02/21 16:39
11/03/21 15:22
367-12-4
2,4,6-Tribromophenol (S)
20
%
18-130
1
11/02/21 16:39
11/03/21 15:22
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation
Method: EPA
5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
mg/kg
0.13
0.042
1
11/02/21 08:58
11/02/21 15:25
67-64-1
Benzene
ND
mg/kg
0.0065
0.0026
1
11/02/21 08:58
11/02/21 15:25
71-43-2
Bromobenzene
ND
mg/kg
0.0065
0.0021
1
11/02/21 08:58
11/02/21 15:25
108-86-1
Bromochloromethane
ND
mg/kg
0.0065
0.0019
1
11/02/21 08:58
11/02/21 15:25
74-97-5
Bromodichloromethane
ND
mg/kg
0.0065
0.0025
1
11/02/21 08:58
11/02/21 15:25
75-27-4
Bromoform
ND
mg/kg
0.0065
0.0023
1
11/02/21 08:58
11/02/21 15:25
75-25-2
Bromomethane
ND
mg/kg
0.013
0.010
1
11/02/21 08:58
11/02/21 15:25
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.13
0.031
1
11/02/21 08:58
11/02/21 15:25
78-93-3
n-Butylbenzene
ND
mg/kg
0.0065
0.0031
1
11/02/21 08:58
11/02/21 15:25
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0065
0.0029
1
11/02/21 08:58
11/02/21 15:25
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0065
0.0023
1
11/02/21 08:58
11/02/21 15:25
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0065
0.0024
1
11/02/21 08:58
11/02/21 15:25
56-23-5
Chlorobenzene
ND
mg/kg
0.0065
0.0013
1
11/02/21 08:58
11/02/21 15:25
108-90-7
Chloroethane
ND
mg/kg
0.013
0.0050
1
11/02/21 08:58
11/02/21 15:25
75-00-3
Chloroform
ND
mg/kg
0.0065
0.0040
1
11/02/21 08:58
11/02/21 15:25
67-66-3
Chloromethane
ND
mg/kg
0.013
0.0055
1
11/02/21 08:58
11/02/21 15:25
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0065
0.0023
1
11/02/21 08:58
11/02/21 15:25
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0065
0.0012
1
11/02/21 08:58
11/02/21 15:25
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0065
0.0025
1
11/02/21 08:58
11/02/21 15:25
96-12-8
Dibromochloromethane
ND
mg/kg
0.0065
0.0037
1
11/02/21 08:58
11/02/21 15:25
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0065
0.0029
1
11/02/21 08:58
11/02/21 15:25
106-93-4
Dibromomethane
ND
mg/kg
0.0065
0.0014
1
11/02/21 08:58
11/02/21 15:25
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0065
0.0024
1
11/02/21 08:58
11/02/21 15:25
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0065
0.0020
1
11/02/21 08:58
11/02/21 15:25
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0065
0.0017
1
11/02/21 08:58
11/02/21 15:25
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.013
0.0028
1
11/02/21 08:58
11/02/21 15:25
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0065
0.0027
1
11/02/21 08:58
11/02/21 15:25
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0065
0.0043
1
11/02/21 08:58
11/02/21 15:25
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0065
0.0027
1
11/02/21 08:58
11/02/21 15:25
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0065
0.0022
1
11/02/21 08:58
11/02/21 15:25
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0065
0.0023
1
11/02/21 08:58
11/02/21 15:25
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0065
0.0020
1
11/02/21 08:58
11/02/21 15:25
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0065
0.0020
1
11/02/21 08:58
11/02/21 15:25
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0065
0.0021
1
11/02/21 08:58
11/02/21 15:25
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0065
0.0031
1
11/02/21 08:58
11/02/21 15:25
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0065
0.0018
1
11/02/21 08:58
11/02/21 15:25
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0065
0.0022
1
11/02/21 08:58
11/02/21 15:25
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0065
0.0018
1
11/02/21 08:58
11/02/21 15:25
108-20-3
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 39 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: S13-4
Lab ID:
92569749008
Collected:
10/28/21
10:55
Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Ethylbenzene
ND
mg/kg
0.0065
0.0030
1
11/02/21 08:58
11/02/21 15:25
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.013
0.011
1
11/02/21 08:58
11/02/21 15:25
87-68-3
2-Hexanone
ND
mg/kg
0.065
0.0063
1
11/02/21 08:58
11/02/21 15:25
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0065
0.0022
1
11/02/21 08:58
11/02/21 15:25
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0065
0.0032
1
11/02/21 08:58
11/02/21 15:25
99-87-6
Methylene Chloride
ND
mg/kg
0.026
0.018
1
11/02/21 08:58
11/02/21 15:25
75-09-2
4-Methyl-2-pentanone (MIBK)
0.0065J
mg/kg
0.065
0.0063
1
11/02/21 08:58
11/02/21 15:25
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0065
0.0024
1
11/02/21 08:58
11/02/21 15:25
1634-04-4
Naphthalene
ND
mg/kg
0.0065
0.0034
1
11/02/21 08:58
11/02/21 15:25
91-20-3
n-Propylbenzene
ND
mg/kg
0.0065
0.0023
1
11/02/21 08:58
11/02/21 15:25
103-65-1
Styrene
ND
mg/kg
0.0065
0.0017
1
11/02/21 08:58
11/02/21 15:25
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0065
0.0025
1
11/02/21 08:58
11/02/21 15:25
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0065
0.0017
1
11/02/21 08:58
11/02/21 15:25
79-34-5
Tetrachloroethene
ND
mg/kg
0.0065
0.0021
1
11/02/21 08:58
11/02/21 15:25
127-18-4
Toluene
ND
mg/kg
0.0065
0.0019
1
11/02/21 08:58
11/02/21 15:25
108-88-3
1,2,3-Trichlorobenzene
ND
mg/kg
0.0065
0.0053
1
11/02/21 08:58
11/02/21 15:25
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0065
0.0055
1
11/02/21 08:58
11/02/21 15:25
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0065
0.0034
1
11/02/21 08:58
11/02/21 15:25
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0065
0.0022
1
11/02/21 08:58
11/02/21 15:25
79-00-5
Trichloroethene
ND
mg/kg
0.0065
0.0017
1
11/02/21 08:58
11/02/21 15:25
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0065
0.0036
1
11/02/21 08:58
11/02/21 15:25
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.0065
0.0033
1
11/02/21 08:58
11/02/21 15:25
96-18-4
1,2,4-Trimethylbenzene
ND
mg/kg
0.0065
0.0018
1
11/02/21 08:58
11/02/21 15:25
95-63-6
1,3,5-Trimethylbenzene
ND
mg/kg
0.0065
0.0022
1
11/02/21 08:58
11/02/21 15:25
108-67-8
Vinyl acetate
ND
mg/kg
0.065
0.0048
1
11/02/21 08:58
11/02/21 15:25
108-05-4
Vinyl chloride
ND
mg/kg
0.013
0.0033
1
11/02/21 08:58
11/02/21 15:25
75-01-4
Xylene (Total)
ND
mg/kg
0.013
0.0037
1
11/02/21 08:58
11/02/21 15:25
1330-20-7
m&p-Xylene
ND
mg/kg
0.013
0.0045
1
11/02/21 08:58
11/02/21 15:25
179601-23-1
o-Xylene
ND
mg/kg
0.0065
0.0029
1
11/02/21 08:58
11/02/21 15:25
95-47-6
Surrogates
Toluene-d8 (S)
101
%
70-130
1
11/02/21 08:58
11/02/21 15:25
2037-26-5
4-Bromofluorobenzene (S)
98
%
69-134
1
11/02/21 08:58
11/02/21 15:25
460-00-4
1,2-Dichloroethane-d4 (S)
97
%
70-130
1
11/02/21 08:58
11/02/21 15:25
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services - Charlotte
Percent Moisture
14.1
%
0.10
0.10
1
11/01/21 15:46
N2
Total Solids 2540 G-2011
Analytical
Method: SM 2540G Preparation Method:
SM
2540 G
Pace National
- Mt. Juliet
Total Solids
84.6
%
1
11/04/21 10:18
11/04/21 10:36
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 40 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: S13-4 Lab ID: 92569749008 Collected: 10/28/21 10:55 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Wet Chemistry 7199 Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Chromium, Hexavalent ND mg/kg 1.18 0.302 1 11/04/21 18:00 11/09/21 19:14 18540-29-9
Date: 11 /11 /2021 09:47 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 41 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: SB-5
Lab ID:
92569749009
Collected:
10/28/21 11:10
Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for
percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical
Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical
Services
-Asheville
Arsenic
4.9J
mg/kg
14.5
2.9
5
11/02/2113:30
11/08/2111:30
7440-38-2
D3
Barium
267
mg/kg
5.8
1.5
5
11/02/2113:30
11/08/2111:30
7440-39-3
D3
Cadmium
0.32J
mg/kg
0.58
0.29
5
11/02/2113:30
11/08/2111:30
7440-43-9
D3
Chromium
72.0
mg/kg
2.9
1.5
5
11/02/2113:30
11/08/2111:30
7440-47-3
D3
Lead
3.8J
mg/kg
5.8
1.5
5
11/02/2113:30
11/08/2111:30
7439-92-1
D3
Selenium
ND
mg/kg
5.8
2.9
5
11/02/2113:30
11/08/2111:30
7782-49-2
D3
Silver
ND
mg/kg
2.9
1.5
5
11/02/2113:30
11/08/2111:30
7440-22-4
D3
7471 Mercury
Analytical
Method: EPA 7471 B Preparation Method: EPA 7471 B
Pace Analytical
Services
-Asheville
Mercury
0.044
mg/kg
0.0080
0.0061
1
11/03/2116:30
11/09/2112:25
7439-97-6
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services
- Charlotte
Acenaphthene
ND
mg/kg
0.47
0.16
1
11/02/21 16:39
11/03/21 15:52
83-32-9
Acenaphthylene
ND
mg/kg
0.47
0.16
1
11/02/21 16:39
11/03/21 15:52
208-96-8
Aniline
ND
mg/kg
0.47
0.18
1
11/02/21 16:39
11/03/21 15:52
62-53-3
Anthracene
ND
mg/kg
0.47
0.15
1
11/02/21 16:39
11/03/21 15:52
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.47
0.16
1
11/02/21 16:39
11/03/21 15:52
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.47
0.16
1
11/02/21 16:39
11/03/21 15:52
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.47
0.16
1
11/02/21 16:39
11/03/21 15:52
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.47
0.18
1
11/02/21 16:39
11/03/21 15:52
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.47
0.16
1
11/02/21 16:39
11/03/21 15:52
207-08-9
Benzoic Acid
ND
mg/kg
2.3
1.0
1
11/02/21 16:39
11/03/21 15:52
65-85-0
Benzyl alcohol
ND
mg/kg
0.93
0.35
1
11/02/21 16:39
11/03/21 15:52
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.47
0.18
1
11/02/21 16:39
11/03/21 15:52
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.47
0.20
1
11/02/21 16:39
11/03/21 15:52
85-68-7
4-ChIoro-3-methyl phenol
ND
mg/kg
0.93
0.33
1
11/02/21 16:39
11/03/21 15:52
59-50-7
4-Chloroaniline
ND
mg/kg
0.93
0.37
1
11/02/21 16:39
11/03/21 15:52
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.47
0.19
1
11/02/21 16:39
11/03/21 15:52
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.47
0.18
1
11/02/21 16:39
11/03/21 15:52
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.47
0.19
1
11/02/21 16:39
11/03/21 15:52
91-58-7
2-Chlorophenol
ND
mg/kg
0.47
0.18
1
11/02/21 16:39
11/03/21 15:52
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.47
0.17
1
11/02/21 16:39
11/03/21 15:52
7005-72-3
Chrysene
ND
mg/kg
0.47
0.17
1
11/02/21 16:39
11/03/21 15:52
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.47
0.18
1
11/02/21 16:39
11/03/21 15:52
53-70-3
Dibenzofuran
ND
mg/kg
0.47
0.17
1
11/02/21 16:39
11/03/21 15:52
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.47
0.17
1
11/02/21 16:39
11/03/21 15:52
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.47
0.17
1
11/02/21 16:39
11/03/21 15:52
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.47
0.18
1
11/02/21 16:39
11/03/21 15:52
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
0.93
0.32
1
11/02/21 16:39
11/03/21 15:52
91-94-1
IL
2,4-Dichlorophenol
ND
mg/kg
0.47
0.18
1
11/02/21 16:39
11/03/21 15:52
120-83-2
Diethylphthalate
ND
mg/kg
0.47
0.17
1
11/02/21 16:39
11/03/21 15:52
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.47
0.19
1
11/02/21 16:39
11/03/21 15:52
105-67-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 42 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: S13-5 Lab ID: 92569749009 Collected: 10/28/21 11:10 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Dimethylphthalate
ND
mg/kg
0.47
0.17
1
11/02/21 16:39
11/03/21 15:52
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.47
0.16
1
11/02/21 16:39
11/03/21 15:52
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.93
0.44
1
11/02/21 16:39
11/03/21 15:52
534-52-1
2,4-Dinitrophenol
ND
mg/kg
2.3
1.4
1
11/02/21 16:39
11/03/21 15:52
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.47
0.18
1
11/02/21 16:39
11/03/21 15:52
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.47
0.17
1
11/02/21 16:39
11/03/21 15:52
606-20-2
Di-n-octylphthalate
ND
mg/kg
0.47
0.18
1
11/02/21 16:39
11/03/21 15:52
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.47
0.18
1
11/02/21 16:39
11/03/21 15:52
117-81-7
Fluoranthene
ND
mg/kg
0.47
0.16
1
11/02/21 16:39
11/03/21 15:52
206-44-0
Fluorene
ND
mg/kg
0.47
0.16
1
11/02/21 16:39
11/03/21 15:52
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.47
0.20
1
11/02/21 16:39
11/03/21 15:52
87-68-3
Hexachlorobenzene
ND
mg/kg
0.47
0.18
1
11/02/21 16:39
11/03/21 15:52
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.47
0.27
1
11/02/21 16:39
11/03/21 15:52
77-47-4
Hexachloroethane
ND
mg/kg
0.47
0.18
1
11/02/21 16:39
11/03/21 15:52
67-72-1
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.47
0.18
1
11/02/21 16:39
11/03/21 15:52
193-39-5
Isophorone
ND
mg/kg
0.47
0.21
1
11/02/21 16:39
11/03/21 15:52
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.47
0.16
1
11/02/21 16:39
11/03/21 15:52
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.47
0.19
1
11/02/21 16:39
11/03/21 15:52
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.47
0.19
1
11/02/21 16:39
11/03/21 15:52
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.47
0.19
1
11/02/21 16:39
11/03/21 15:52
15831-10-4
Naphthalene
ND
mg/kg
0.47
0.16
1
11/02/21 16:39
11/03/21 15:52
91-20-3
2-Nitroaniline
ND
mg/kg
2.3
0.38
1
11/02/21 16:39
11/03/21 15:52
88-74-4
3-Nitroaniline
ND
mg/kg
2.3
0.37
1
11/02/21 16:39
11/03/21 15:52
99-09-2
4-Nitroaniline
ND
mg/kg
0.93
0.36
1
11/02/21 16:39
11/03/21 15:52
100-01-6
Nitrobenzene
ND
mg/kg
0.47
0.22
1
11/02/21 16:39
11/03/21 15:52
98-95-3
2-Nitrophenol
ND
mg/kg
0.47
0.20
1
11/02/21 16:39
11/03/21 15:52
88-75-5
4-Nitrophenol
ND
mg/kg
2.3
0.90
1
11/02/21 16:39
11/03/21 15:52
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.47
0.16
1
11/02/21 16:39
11/03/21 15:52
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.47
0.18
1
11/02/21 16:39
11/03/21 15:52
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.47
0.17
1
11/02/21 16:39
11/03/21 15:52
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.47
0.22
1
11/02/21 16:39
11/03/21 15:52
108-60-1
Pentachlorophenol
ND
mg/kg
0.93
0.46
1
11/02/21 16:39
11/03/21 15:52
87-86-5
Phenanthrene
ND
mg/kg
0.47
0.15
1
11/02/21 16:39
11/03/21 15:52
85-01-8
Phenol
ND
mg/kg
0.47
0.21
1
11/02/21 16:39
11/03/21 15:52
108-95-2
Pyrene
ND
mg/kg
0.47
0.19
1
11/02/21 16:39
11/03/21 15:52
129-00-0
Pyridine
ND
mg/kg
0.47
0.15
1
11/02/21 16:39
11/03/21 15:52
110-86-1
1,2,4-Trichlorobenzene
ND
mg/kg
0.47
0.18
1
11/02/21 16:39
11/03/21 15:52
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.47
0.21
1
11/02/21 16:39
11/03/21 15:52
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.47
0.19
1
11/02/21 16:39
11/03/21 15:52
88-06-2
Surrogates
Nitrobenzene-d5(S)
37
%
21-130
1
11/02/21 16:39
11/03/21 15:52
4165-60-0
2-Fluorobiphenyl (S)
40
%
19-130
1
11/02/21 16:39
11/03/21 15:52
321-60-8
Terphenyl-d14 (S)
37
%
15-130
1
11/02/21 16:39
11/03/21 15:52
1718-51-0
Phenol-d6 (S)
37
%
18-130
1
11/02/21 16:39
11/03/21 15:52
13127-88-3
REPORT OF LABORATORY ANALYSIS
IL
v1
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Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 43 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: SB-5 Lab ID: 92569749009 Collected: 10/28/21 11:10 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Surrogates
2-Fluorophenol (S)
34
%
18-130
1
11/02/21 16:39
11/03/21 15:52
367-12-4
2,4,6-Tribromophenol (S)
36
%
18-130
1
11/02/21 16:39
11/03/21 15:52
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation
Method: EPA
5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
mg/kg
0.17
0.055
1
11/02/21 08:58
11/02/21 15:43
67-64-1
Benzene
ND
mg/kg
0.0085
0.0034
1
11/02/21 08:58
11/02/21 15:43
71-43-2
Bromobenzene
ND
mg/kg
0.0085
0.0028
1
11/02/21 08:58
11/02/21 15:43
108-86-1
Bromochloromethane
ND
mg/kg
0.0085
0.0025
1
11/02/21 08:58
11/02/21 15:43
74-97-5
Bromodichloromethane
ND
mg/kg
0.0085
0.0033
1
11/02/21 08:58
11/02/21 15:43
75-27-4
Bromoform
ND
mg/kg
0.0085
0.0030
1
11/02/21 08:58
11/02/21 15:43
75-25-2
Bromomethane
ND
mg/kg
0.017
0.014
1
11/02/21 08:58
11/02/21 15:43
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.17
0.041
1
11/02/21 08:58
11/02/21 15:43
78-93-3
n-Butylbenzene
ND
mg/kg
0.0085
0.0040
1
11/02/21 08:58
11/02/21 15:43
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0085
0.0038
1
11/02/21 08:58
11/02/21 15:43
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0085
0.0030
1
11/02/21 08:58
11/02/21 15:43
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0085
0.0032
1
11/02/21 08:58
11/02/21 15:43
56-23-5
Chlorobenzene
ND
mg/kg
0.0085
0.0016
1
11/02/21 08:58
11/02/21 15:43
108-90-7
Chloroethane
ND
mg/kg
0.017
0.0066
1
11/02/21 08:58
11/02/21 15:43
75-00-3
Chloroform
ND
mg/kg
0.0085
0.0052
1
11/02/21 08:58
11/02/21 15:43
67-66-3
Chloromethane
ND
mg/kg
0.017
0.0072
1
11/02/21 08:58
11/02/21 15:43
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0085
0.0030
1
11/02/21 08:58
11/02/21 15:43
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0085
0.0015
1
11/02/21 08:58
11/02/21 15:43
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0085
0.0033
1
11/02/21 08:58
11/02/21 15:43
96-12-8
Dibromochloromethane
ND
mg/kg
0.0085
0.0048
1
11/02/21 08:58
11/02/21 15:43
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0085
0.0038
1
11/02/21 08:58
11/02/21 15:43
106-93-4
Dibromomethane
ND
mg/kg
0.0085
0.0018
1
11/02/21 08:58
11/02/21 15:43
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0085
0.0031
1
11/02/21 08:58
11/02/21 15:43
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0085
0.0026
1
11/02/21 08:58
11/02/21 15:43
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0085
0.0022
1
11/02/21 08:58
11/02/21 15:43
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.017
0.0037
1
11/02/21 08:58
11/02/21 15:43
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0085
0.0035
1
11/02/21 08:58
11/02/21 15:43
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0085
0.0057
1
11/02/21 08:58
11/02/21 15:43
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0085
0.0035
1
11/02/21 08:58
11/02/21 15:43
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0085
0.0029
1
11/02/21 08:58
11/02/21 15:43
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0085
0.0030
1
11/02/21 08:58
11/02/21 15:43
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0085
0.0026
1
11/02/21 08:58
11/02/21 15:43
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0085
0.0027
1
11/02/21 08:58
11/02/21 15:43
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0085
0.0028
1
11/02/21 08:58
11/02/21 15:43
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0085
0.0041
1
11/02/21 08:58
11/02/21 15:43
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0085
0.0023
1
11/02/21 08:58
11/02/21 15:43
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0085
0.0029
1
11/02/21 08:58
11/02/21 15:43
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0085
0.0023
1
11/02/21 08:58
11/02/21 15:43
108-20-3
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 44 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: S13-5 Lab ID: 92569749009 Collected: 10/28/21 11:10 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Total Solids 2540 G-2011
Total Solids
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
mg/kg
0.0085
0.0040
1
11 /02/21 08:58
11 /02/21 15:43
100-41-4
ND
mg/kg
0.017
0.014
1
11 /02/21 08:58
11 /02/21 15:43
87-68-3
ND
mg/kg
0.085
0.0082
1
11 /02/21 08:58
11 /02/21 15:43
591-78-6
ND
mg/kg
0.0085
0.0029
1
11 /02/21 08:58
11 /02/21 15:43
98-82-8
ND
mg/kg
0.0085
0.0042
1
11 /02/21 08:58
11 /02/21 15:43
99-87-6
ND
mg/kg
0.034
0.023
1
11 /02/21 08:58
11 /02/21 15:43
75-09-2
ND
mg/kg
0.085
0.0082
1
11/02/2108:58
11/02/2115:43
108-10-1
ND
mg/kg
0.0085
0.0032
1
11 /02/21 08:58
11 /02/21 15:43
1634-04-4
ND
mg/kg
0.0085
0.0045
1
11 /02/21 08:58
11 /02/21 15:43
91-20-3
ND
mg/kg
0.0085
0.0030
1
11 /02/21 08:58
11 /02/21 15:43
103-65-1
ND
mg/kg
0.0085
0.0023
1
11 /02/21 08:58
11 /02/21 15:43
100-42-5
ND
mg/kg
0.0085
0.0033
1
11 /02/21 08:58
11 /02/21 15:43
630-20-6
ND
mg/kg
0.0085
0.0023
1
11 /02/21 08:58
11 /02/21 15:43
79-34-5
ND
mg/kg
0.0085
0.0027
1
11 /02/21 08:58
11 /02/21 15:43
127-18-4
ND
mg/kg
0.0085
0.0024
1
11 /02/21 08:58
11 /02/21 15:43
108-88-3
ND
mg/kg
0.0085
0.0069
1
11 /02/21 08:58
11 /02/21 15:43
87-61-6
ND
mg/kg
0.0085
0.0072
1
11 /02/21 08:58
11 /02/21 15:43
120-82-1
ND
mg/kg
0.0085
0.0044
1
11 /02/21 08:58
11 /02/21 15:43
71-55-6
ND
mg/kg
0.0085
0.0028
1
11 /02/21 08:58
11 /02/21 15:43
79-00-5
ND
mg/kg
0.0085
0.0022
1
11 /02/21 08:58
11 /02/21 15:43
79-01-6
ND
mg/kg
0.0085
0.0047
1
11 /02/21 08:58
11 /02/21 15:43
75-69-4
ND
mg/kg
0.0085
0.0043
1
11 /02/21 08:58
11 /02/21 15:43
96-18-4
ND
mg/kg
0.0085
0.0023
1
11 /02/21 08:58
11 /02/21 15:43
95-63-6
ND
mg/kg
0.0085
0.0029
1
11 /02/21 08:58
11 /02/21 15:43
108-67-8
ND
mg/kg
0.085
0.0062
1
11 /02/21 08:58
11 /02/21 15:43
108-05-4
ND
mg/kg
0.017
0.0043
1
11 /02/21 08:58
11 /02/21 15:43
75-01-4
ND
mg/kg
0.017
0.0049
1
11 /02/21 08:58
11 /02/21 15:43
1330-20-7
ND
mg/kg
0.017
0.0058
1
11 /02/21 08:58
11 /02/21 15:43
179601-23-1
ND
mg/kg
0.0085
0.0038
1
11 /02/21 08:58
11 /02/21 15:43
95-47-6
101
%
70-130
1
11 /02/21 08:58
11 /02/21 15:43
2037-26-5
99
%
69-134
1
11 /02/21 08:58
11 /02/21 15:43
460-00-4
101
%
70-130
1
11 /02/21 08:58
11 /02/21 15:43
17060-07-0
Analytical Method: SW-846
Pace Analytical Services - Charlotte
29.4 % 0.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
70.8 %
11/01/21 15:46
1 11 /04/21 10:18 11 /04/21 10:36
REPORT OF LABORATORY ANALYSIS
N2
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 45 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: S13-5 Lab ID: 92569749009 Collected: 10/28/21 11:10 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Wet Chemistry 7199 Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Chromium, Hexavalent 1.32J mg/kg 1.41 0.360 1 11/04/21 18:00 11/09/21 19:30 18540-29-9 J
Date: 11 /11 /2021 09:47 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 46 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: SB-6 Lab ID: 92569749010 Collected: 10/28/21 11:25 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services
-Asheville
Arsenic
2.5J
mg/kg
3.0
0.60
1
11/02/2113:30
11/08/2104:35
7440-38-2
Barium
118
mg/kg
1.2
0.30
1
11/02/2113:30
11/08/2104:35
7440-39-3
Cadmium
0.88
mg/kg
0.12
0.060
1
11/02/2113:30
11/08/2104:35
7440-43-9
Chromium
60.8
mg/kg
0.60
0.30
1
11/02/2113:30
11/08/2104:35
7440-47-3
Lead
154
mg/kg
1.2
0.30
1
11/02/2113:30
11/08/2104:35
7439-92-1
Selenium
1.4
mg/kg
1.2
0.60
1
11/02/2113:30
11/08/2104:35
7782-49-2
Silver
0.52J
mg/kg
0.60
0.30
1
11/02/2113:30
11/08/2104:35
7440-22-4
7471 Mercury
Analytical
Method: EPA 7471 B Preparation
Method: EPA
7471 B
Pace Analytical Services
-Asheville
Mercury
0.048
mg/kg
0.0048
0.0037
1
11/03/2116:30
11/09/2112:27
7439-97-6
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation
Method: EPA
3546
Pace Analytical Services
- Charlotte
Acenaphthene
ND
mg/kg
0.41
0.14
1
11/02/21 16:39
11/03/21 16:22
83-32-9
Acenaphthylene
ND
mg/kg
0.41
0.14
1
11/02/21 16:39
11/03/21 16:22
208-96-8
Aniline
ND
mg/kg
0.41
0.16
1
11/02/21 16:39
11/03/21 16:22
62-53-3
Anthracene
ND
mg/kg
0.41
0.13
1
11/02/21 16:39
11/03/21 16:22
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.41
0.14
1
11/02/21 16:39
11/03/21 16:22
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.41
0.14
1
11/02/21 16:39
11/03/21 16:22
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.41
0.14
1
11/02/21 16:39
11/03/21 16:22
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.41
0.16
1
11/02/21 16:39
11/03/21 16:22
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.41
0.14
1
11/02/21 16:39
11/03/21 16:22
207-08-9
Benzoic Acid
ND
mg/kg
2.1
0.88
1
11/02/21 16:39
11/03/21 16:22
65-85-0
Benzyl alcohol
ND
mg/kg
0.82
0.31
1
11/02/21 16:39
11/03/21 16:22
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.41
0.16
1
11/02/21 16:39
11/03/21 16:22
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.41
0.17
1
11/02/21 16:39
11/03/21 16:22
85-68-7
4-ChIoro-3-methyl phenol
ND
mg/kg
0.82
0.29
1
11/02/21 16:39
11/03/21 16:22
59-50-7
4-Chloroaniline
ND
mg/kg
0.82
0.32
1
11/02/21 16:39
11/03/21 16:22
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.41
0.17
1
11/02/21 16:39
11/03/21 16:22
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.41
0.15
1
11/02/21 16:39
11/03/21 16:22
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.41
0.16
1
11/02/21 16:39
11/03/21 16:22
91-58-7
2-Chlorophenol
ND
mg/kg
0.41
0.15
1
11/02/21 16:39
11/03/21 16:22
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.41
0.15
1
11/02/21 16:39
11/03/21 16:22
7005-72-3
Chrysene
ND
mg/kg
0.41
0.15
1
11/02/21 16:39
11/03/21 16:22
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.41
0.16
1
11/02/21 16:39
11/03/21 16:22
53-70-3
Dibenzofuran
ND
mg/kg
0.41
0.15
1
11/02/21 16:39
11/03/21 16:22
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.41
0.15
1
11/02/21 16:39
11/03/21 16:22
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.41
0.15
1
11/02/21 16:39
11/03/21 16:22
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.41
0.16
1
11/02/21 16:39
11/03/21 16:22
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
0.82
0.28
1
11/02/21 16:39
11/03/21 16:22
91-94-1 IL
2,4-Dichlorophenol
ND
mg/kg
0.41
0.16
1
11/02/21 16:39
11/03/21 16:22
120-83-2
Diethylphthalate
ND
mg/kg
0.41
0.15
1
11/02/21 16:39
11/03/21 16:22
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.41
0.17
1
11/02/21 16:39
11/03/21 16:22
105-67-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 47 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: S13-6 Lab ID: 92569749010 Collected: 10/28/21 11:25 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Dimethylphthalate
ND
mg/kg
0.41
0.15
1
11/02/21 16:39
11/03/21 16:22
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.41
0.14
1
11/02/21 16:39
11/03/21 16:22
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.82
0.38
1
11/02/21 16:39
11/03/21 16:22
534-52-1
2,4-Dinitrophenol
ND
mg/kg
2.1
1.3
1
11/02/21 16:39
11/03/21 16:22
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.41
0.16
1
11/02/21 16:39
11/03/21 16:22
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.41
0.15
1
11/02/21 16:39
11/03/21 16:22
606-20-2
Di-n-octylphthalate
ND
mg/kg
0.41
0.16
1
11/02/21 16:39
11/03/21 16:22
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.41
0.16
1
11/02/21 16:39
11/03/21 16:22
117-81-7
Fluoranthene
ND
mg/kg
0.41
0.14
1
11/02/21 16:39
11/03/21 16:22
206-44-0
Fluorene
ND
mg/kg
0.41
0.14
1
11/02/21 16:39
11/03/21 16:22
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.41
0.18
1
11/02/21 16:39
11/03/21 16:22
87-68-3
Hexachlorobenzene
ND
mg/kg
0.41
0.16
1
11/02/21 16:39
11/03/21 16:22
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.41
0.24
1
11/02/21 16:39
11/03/21 16:22
77-47-4
Hexachloroethane
ND
mg/kg
0.41
0.16
1
11/02/21 16:39
11/03/21 16:22
67-72-1
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.41
0.16
1
11/02/21 16:39
11/03/21 16:22
193-39-5
Isophorone
ND
mg/kg
0.41
0.18
1
11/02/21 16:39
11/03/21 16:22
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.41
0.14
1
11/02/21 16:39
11/03/21 16:22
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.41
0.16
1
11/02/21 16:39
11/03/21 16:22
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.41
0.17
1
11/02/21 16:39
11/03/21 16:22
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.41
0.17
1
11/02/21 16:39
11/03/21 16:22
15831-10-4
Naphthalene
ND
mg/kg
0.41
0.14
1
11/02/21 16:39
11/03/21 16:22
91-20-3
2-Nitroaniline
ND
mg/kg
2.1
0.34
1
11/02/21 16:39
11/03/21 16:22
88-74-4
3-Nitroaniline
ND
mg/kg
2.1
0.32
1
11/02/21 16:39
11/03/21 16:22
99-09-2
4-Nitroaniline
ND
mg/kg
0.82
0.31
1
11/02/21 16:39
11/03/21 16:22
100-01-6
Nitrobenzene
ND
mg/kg
0.41
0.19
1
11/02/21 16:39
11/03/21 16:22
98-95-3
2-Nitrophenol
ND
mg/kg
0.41
0.18
1
11/02/21 16:39
11/03/21 16:22
88-75-5
4-Nitrophenol
ND
mg/kg
2.1
0.79
1
11/02/21 16:39
11/03/21 16:22
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.41
0.14
1
11/02/21 16:39
11/03/21 16:22
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.41
0.15
1
11/02/21 16:39
11/03/21 16:22
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.41
0.15
1
11/02/21 16:39
11/03/21 16:22
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.41
0.20
1
11/02/21 16:39
11/03/21 16:22
108-60-1
Pentachlorophenol
ND
mg/kg
0.82
0.40
1
11/02/21 16:39
11/03/21 16:22
87-86-5
Phenanthrene
ND
mg/kg
0.41
0.13
1
11/02/21 16:39
11/03/21 16:22
85-01-8
Phenol
ND
mg/kg
0.41
0.18
1
11/02/21 16:39
11/03/21 16:22
108-95-2
Pyrene
ND
mg/kg
0.41
0.17
1
11/02/21 16:39
11/03/21 16:22
129-00-0
Pyridine
ND
mg/kg
0.41
0.13
1
11/02/21 16:39
11/03/21 16:22
110-86-1
1,2,4-Trichlorobenzene
ND
mg/kg
0.41
0.16
1
11/02/21 16:39
11/03/21 16:22
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.41
0.19
1
11/02/21 16:39
11/03/21 16:22
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.41
0.17
1
11/02/21 16:39
11/03/21 16:22
88-06-2
Surrogates
Nitrobenzene-d5(S)
29
%
21-130
1
11/02/21 16:39
11/03/21 16:22
4165-60-0
2-Fluorobiphenyl (S)
32
%
19-130
1
11/02/21 16:39
11/03/21 16:22
321-60-8
Terphenyl-d14 (S)
34
%
15-130
1
11/02/21 16:39
11/03/21 16:22
1718-51-0
Phenol-d6 (S)
29
%
18-130
1
11/02/21 16:39
11/03/21 16:22
13127-88-3
REPORT OF LABORATORY ANALYSIS
IL
v1
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 48 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: SB-6 Lab ID: 92569749010 Collected: 10/28/21 11:25 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Surrogates
2-Fluorophenol (S)
28
%
18-130
1
11/02/21 16:39
11/03/21 16:22
367-12-4
2,4,6-Tribromophenol (S)
28
%
18-130
1
11/02/21 16:39
11/03/21 16:22
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation
Method: EPA
5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
mg/kg
0.14
0.044
1
11/02/21 08:58
11/02/21 16:00
67-64-1
Benzene
ND
mg/kg
0.0068
0.0027
1
11/02/21 08:58
11/02/21 16:00
71-43-2
Bromobenzene
ND
mg/kg
0.0068
0.0022
1
11/02/21 08:58
11/02/21 16:00
108-86-1
Bromochloromethane
ND
mg/kg
0.0068
0.0020
1
11/02/21 08:58
11/02/21 16:00
74-97-5
Bromodichloromethane
ND
mg/kg
0.0068
0.0026
1
11/02/21 08:58
11/02/21 16:00
75-27-4
Bromoform
ND
mg/kg
0.0068
0.0024
1
11/02/21 08:58
11/02/21 16:00
75-25-2
Bromomethane
ND
mg/kg
0.014
0.011
1
11/02/21 08:58
11/02/21 16:00
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.14
0.033
1
11/02/21 08:58
11/02/21 16:00
78-93-3
n-Butylbenzene
ND
mg/kg
0.0068
0.0032
1
11/02/21 08:58
11/02/21 16:00
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0068
0.0030
1
11/02/21 08:58
11/02/21 16:00
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0068
0.0024
1
11/02/21 08:58
11/02/21 16:00
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0068
0.0025
1
11/02/21 08:58
11/02/21 16:00
56-23-5
Chlorobenzene
ND
mg/kg
0.0068
0.0013
1
11/02/21 08:58
11/02/21 16:00
108-90-7
Chloroethane
ND
mg/kg
0.014
0.0053
1
11/02/21 08:58
11/02/21 16:00
75-00-3
Chloroform
ND
mg/kg
0.0068
0.0041
1
11/02/21 08:58
11/02/21 16:00
67-66-3
Chloromethane
ND
mg/kg
0.014
0.0057
1
11/02/21 08:58
11/02/21 16:00
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0068
0.0024
1
11/02/21 08:58
11/02/21 16:00
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0068
0.0012
1
11/02/21 08:58
11/02/21 16:00
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0068
0.0026
1
11/02/21 08:58
11/02/21 16:00
96-12-8
Dibromochloromethane
ND
mg/kg
0.0068
0.0038
1
11/02/21 08:58
11/02/21 16:00
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0068
0.0030
1
11/02/21 08:58
11/02/21 16:00
106-93-4
Dibromomethane
ND
mg/kg
0.0068
0.0015
1
11/02/21 08:58
11/02/21 16:00
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0068
0.0025
1
11/02/21 08:58
11/02/21 16:00
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0068
0.0021
1
11/02/21 08:58
11/02/21 16:00
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0068
0.0018
1
11/02/21 08:58
11/02/21 16:00
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.014
0.0030
1
11/02/21 08:58
11/02/21 16:00
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0068
0.0028
1
11/02/21 08:58
11/02/21 16:00
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0068
0.0045
1
11/02/21 08:58
11/02/21 16:00
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0068
0.0028
1
11/02/21 08:58
11/02/21 16:00
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0068
0.0023
1
11/02/21 08:58
11/02/21 16:00
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0068
0.0024
1
11/02/21 08:58
11/02/21 16:00
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0068
0.0020
1
11/02/21 08:58
11/02/21 16:00
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0068
0.0021
1
11/02/21 08:58
11/02/21 16:00
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0068
0.0022
1
11/02/21 08:58
11/02/21 16:00
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0068
0.0033
1
11/02/21 08:58
11/02/21 16:00
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0068
0.0019
1
11/02/21 08:58
11/02/21 16:00
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0068
0.0023
1
11/02/21 08:58
11/02/21 16:00
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0068
0.0018
1
11/02/21 08:58
11/02/21 16:00
108-20-3
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 49 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: S13-6
Lab ID:
92569749010
Collected:
10/28/21
11:25
Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Ethylbenzene
ND
mg/kg
0.0068
0.0032
1
11/02/21 08:58
11/02/21 16:00
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.014
0.011
1
11/02/21 08:58
11/02/21 16:00
87-68-3
2-Hexanone
ND
mg/kg
0.068
0.0066
1
11/02/21 08:58
11/02/21 16:00
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0068
0.0023
1
11/02/21 08:58
11/02/21 16:00
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0068
0.0033
1
11/02/21 08:58
11/02/21 16:00
99-87-6
Methylene Chloride
ND
mg/kg
0.027
0.019
1
11/02/21 08:58
11/02/21 16:00
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.068
0.0066
1
11/02/21 08:58
11/02/21 16:00
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0068
0.0025
1
11/02/21 08:58
11/02/21 16:00
1634-04-4
Naphthalene
ND
mg/kg
0.0068
0.0036
1
11/02/21 08:58
11/02/21 16:00
91-20-3
n-Propylbenzene
ND
mg/kg
0.0068
0.0024
1
11/02/21 08:58
11/02/21 16:00
103-65-1
Styrene
ND
mg/kg
0.0068
0.0018
1
11/02/21 08:58
11/02/21 16:00
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0068
0.0026
1
11/02/21 08:58
11/02/21 16:00
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0068
0.0018
1
11/02/21 08:58
11/02/21 16:00
79-34-5
Tetrachloroethene
ND
mg/kg
0.0068
0.0022
1
11/02/21 08:58
11/02/21 16:00
127-18-4
Toluene
0.0036J
mg/kg
0.0068
0.0019
1
11/02/21 08:58
11/02/21 16:00
108-88-3
1,2,3-Trichlorobenzene
ND
mg/kg
0.0068
0.0055
1
11/02/21 08:58
11/02/21 16:00
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0068
0.0057
1
11/02/21 08:58
11/02/21 16:00
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0068
0.0035
1
11/02/21 08:58
11/02/21 16:00
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0068
0.0023
1
11/02/21 08:58
11/02/21 16:00
79-00-5
Trichloroethene
ND
mg/kg
0.0068
0.0018
1
11/02/21 08:58
11/02/21 16:00
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0068
0.0037
1
11/02/21 08:58
11/02/21 16:00
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.0068
0.0034
1
11/02/21 08:58
11/02/21 16:00
96-18-4
1,2,4-Trimethylbenzene
ND
mg/kg
0.0068
0.0019
1
11/02/21 08:58
11/02/21 16:00
95-63-6
1,3,5-Trimethylbenzene
ND
mg/kg
0.0068
0.0023
1
11/02/21 08:58
11/02/21 16:00
108-67-8
Vinyl acetate
ND
mg/kg
0.068
0.0050
1
11/02/21 08:58
11/02/21 16:00
108-05-4
Vinyl chloride
ND
mg/kg
0.014
0.0035
1
11/02/21 08:58
11/02/21 16:00
75-01-4
Xylene (Total)
ND
mg/kg
0.014
0.0039
1
11/02/21 08:58
11/02/21 16:00
1330-20-7
m&p-Xylene
ND
mg/kg
0.014
0.0047
1
11/02/21 08:58
11/02/21 16:00
179601-23-1
o-Xylene
ND
mg/kg
0.0068
0.0030
1
11/02/21 08:58
11/02/21 16:00
95-47-6
Surrogates
Toluene-d8 (S)
100
%
70-130
1
11/02/21 08:58
11/02/21 16:00
2037-26-5
4-Bromofluorobenzene (S)
98
%
69-134
1
11/02/21 08:58
11/02/21 16:00
460-00-4
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
11/02/21 08:58
11/02/21 16:00
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services - Charlotte
Percent Moisture
18.3
%
0.10
0.10
1
11/01/21 15:47
N2
Total Solids 2540 G-2011
Analytical
Method: SM 2540G Preparation Method:
SM
2540 G
Pace National
- Mt. Juliet
Total Solids
90.5
%
1
11/04/21 10:18
11/04/21 10:36
REPORT OF LABORATORY ANALYSIS
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Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 50 of 87

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ANALYTICAL RESULTS
Project: Carson & Tryon
Pace Project No.: 92569749
Sample: S13-6 Lab ID: 92569749010 Collected: 10/28/21 11:25 Received: 11/01/21 07:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Wet Chemistry 7199 Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Chromium, Hexavalent 0.579J mg/kg 1.10 0.282 1 11/04/21 18:00 11/09/21 19:40 18540-29-9 J
Date: 11 /11 /2021 09:47 AM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 51 of 87

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
QC Batch: 657137 Analysis Method: EPA 7471 B
QC Batch Method: EPA 7471 B Analysis Description: 7471 Mercury
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92569749005, 92569749006, 92569749007, 92569749008, 92569749009, 92569749010
METHOD BLANK: 3444635 Matrix: Solid
Associated Lab Samples: 92569749005, 92569749006, 92569749007, 92569749008, 92569749009, 92569749010
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Mercury mg/kg ND 0.0036 0.0028 11/09/2114:32
LABORATORY CONTROL SAMPLE: 3444636
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg 0.05 0.048 96 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3444637 3444638
MS MSD
92569749005 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Mercury mg/kg 0.22 0.086 0.086 0.22 0.15 -6 -90 75-125 39 20 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC.
Page 52 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
QC Batch: 656810 Analysis Method: EPA 6010D
QC Batch Method: EPA 3050E Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92569749005, 92569749006, 92569749007, 92569749008, 92569749009, 92569749010
METHOD BLANK: 3442923
Matrix:
Solid
Associated Lab Samples:
92569749005, 92569749006,
92569749007, 92569749008, 92569749009, 92569749010
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
Arsenic
mg/kg
ND
2.5
0.50
11/08/2103:10
Barium
mg/kg
ND
1.0
0.25
11/08/2103:10
Cadmium
mg/kg
ND
0.10
0.050
11/08/2111:23
Chromium
mg/kg
ND
0.50
0.25
11/08/2103:10
Lead
mg/kg
ND
1.0
0.25
11/08/2103:10
Selenium
mg/kg
ND
1.0
0.50
11/08/2103:10
Silver
mg/kg
ND
0.50
0.25
11/08/2103:10
LABORATORY CONTROL SAMPLE: 3442924
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Arsenic
mg/kg
50
45.8
92
80-120
Barium
mg/kg
50
50.0
100
80-120
Cadmium
mg/kg
50
48.3
97
80-120
Chromium
mg/kg
50
50.4
101
80-120
Lead
mg/kg
50
49.1
98
80-120
Selenium
mg/kg
50
41.6
83
80-120
Silver
mg/kg
25
24.8
99
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3442925
3442926
MS
MSD
92569860027
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Arsenic
mg/kg
0.94J
52.3
52.3
45.2
43.9
85
82
75-125
3
20
Barium
mg/kg
11.7
52.3
52.3
68.1
66.8
108
105
75-125
2
20
Cadmium
mg/kg
0.059J
52.3
52.3
49.6
48.5
95
93
75-125
2
20
Chromium
mg/kg
5.4
52.3
52.3
58.4
57.7
101
100
75-125
1
20
Lead
mg/kg
12.3
52.3
52.3
56.9
56.0
85
84
75-125
1
20
Selenium
mg/kg
0.57J
52.3
52.3
40.9
39.5
77
74
75-125
4
20 M1
Silver
mg/kg
ND
26.1
26.1
25.4
25.0
97
95
75-125
2
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC.
Page 53 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
QC Batch: 656847 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92569749005, 92569749006, 92569749007, 92569749008, 92569749009, 92569749010
METHOD BLANK: 3443080
Matrix:
Solid
Associated Lab Samples: 92569749005,
92569749006,
92569749007, 92569749008, 92569749009, 92569749010
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
mg/kg
ND
0.0050
0.0019
11/02/21 11:06
1,1,1-Trichloroethane
mg/kg
ND
0.0050
0.0026
11/02/21 11:06
1,1,2,2-Tetrachloroethane
mg/kg
ND
0.0050
0.0013
11/02/21 11:06
1,1,2-Trichloroethane
mg/kg
ND
0.0050
0.0017
11/02/21 11:06
1,1-Dichloroethane
mg/kg
ND
0.0050
0.0021
11/02/21 11:06
1,1-Dichloroethene
mg/kg
ND
0.0050
0.0021
11/02/21 11:06
1,1-Dichloropropene
mg/kg
ND
0.0050
0.0024
11/02/21 11:06
1,2,3-Trichlorobenzene
mg/kg
ND
0.0050
0.0040
11/02/21 11:06
1,2,3-Trichloropropane
mg/kg
ND
0.0050
0.0025
11/02/21 11:06
1,2,4-Trichlorobenzene
mg/kg
ND
0.0050
0.0042
11/02/21 11:06
1,2,4-Trimethylbenzene
mg/kg
ND
0.0050
0.0014
11/02/21 11:06
1,2-Dibromo-3-chloropropane
mg/kg
ND
0.0050
0.0019
11/02/21 11:06
1,2-Dibromoethane (EDB)
mg/kg
ND
0.0050
0.0022
11/02/21 11:06
1,2-Dichlorobenzene
mg/kg
ND
0.0050
0.0018
11/02/21 11:06
1,2-Dichloroethane
mg/kg
ND
0.0050
0.0033
11/02/21 11:06
1,2-Dichloropropane
mg/kg
ND
0.0050
0.0015
11/02/21 11:06
1,3,5-Trimethylbenzene
mg/kg
ND
0.0050
0.0017
11/02/21 11:06
1,3-Dichlorobenzene
mg/kg
ND
0.0050
0.0016
11/02/21 11:06
1,3-Dichloropropane
mg/kg
ND
0.0050
0.0016
11/02/21 11:06
1,4-Dichlorobenzene
mg/kg
ND
0.0050
0.0013
11/02/21 11:06
2,2-Dichloropropane
mg/kg
ND
0.0050
0.0016
11/02/21 11:06
2-Butanone (MEK)
mg/kg
ND
0.10
0.024
11/02/21 11:06
2-Chlorotoluene
mg/kg
ND
0.0050
0.0018
11/02/21 11:06
2-Hexanone
mg/kg
ND
0.050
0.0048
11/02/21 11:06
4-Chlorotoluene
mg/kg
ND
0.0050
0.00088
11/02/21 11:06
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
0.050
0.0048
11/02/21 11:06
Acetone
mg/kg
ND
0.10
0.032
11/02/21 11:06
Benzene
mg/kg
ND
0.0050
0.0020
11/02/21 11:06
Bromobenzene
mg/kg
ND
0.0050
0.0016
11/02/21 11:06
Bromochloromethane
mg/kg
ND
0.0050
0.0015
11/02/21 11:06
Bromodichloromethane
mg/kg
ND
0.0050
0.0019
11/02/21 11:06
Bromoform
mg/kg
ND
0.0050
0.0018
11/02/21 11:06
Bromomethane
mg/kg
ND
0.010
0.0079
11/02/21 11:06 v1
Carbon tetrachloride
mg/kg
ND
0.0050
0.0019
11/02/21 11:06
Chlorobenzene
mg/kg
ND
0.0050
0.00096
11/02/21 11:06
Chloroethane
mg/kg
ND
0.010
0.0039
11/02/21 11:06
Chloroform
mg/kg
ND
0.0050
0.0030
11/02/21 11:06
Chloromethane
mg/kg
ND
0.010
0.0042
11/02/21 11:06
cis-1,2-Dichloroethene
mg/kg
ND
0.0050
0.0017
11/02/21 11:06
cis-1,3-Dichloropropene
mg/kg
ND
0.0050
0.0014
11/02/21 11:06
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 54 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
METHOD BLANK: 3443080 Matrix: Solid
Associated Lab Samples: 92569749005, 92569749006, 92569749007, 92569749008, 92569749009, 92569749010
Blank Reporting
Parameter Units Result Limit MDL Analyzed
Dibromochloromethane
mg/kg
ND
0.0050
0.0028
11/02/21 11:06
Dibromomethane
mg/kg
ND
0.0050
0.0011
11/02/21 11:06
Dichlorodifluoromethane
mg/kg
ND
0.010
0.0022
11/02/21 11:06
Diisopropyl ether
mg/kg
ND
0.0050
0.0014
11/02/21 11:06
Ethylbenzene
mg/kg
ND
0.0050
0.0023
11/02/21 11:06
Hexachloro-1,3-butadiene
mg/kg
ND
0.010
0.0082
11/02/21 11:06
Isopropylbenzene (Cumene)
mg/kg
ND
0.0050
0.0017
11/02/21 11:06
m&p-Xylene
mg/kg
ND
0.010
0.0034
11/02/21 11:06
Methyl-tert-butyl ether
mg/kg
ND
0.0050
0.0019
11/02/21 11:06
Methylene Chloride
mg/kg
ND
0.020
0.014
11/02/21 11:06
n-Butylbenzene
mg/kg
ND
0.0050
0.0024
11/02/21 11:06
n-Propylbenzene
mg/kg
ND
0.0050
0.0018
11/02/21 11:06
Naphthalene
mg/kg
ND
0.0050
0.0026
11/02/21 11:06
o-Xylene
mg/kg
ND
0.0050
0.0022
11/02/21 11:06
p-Isopropyltoluene
mg/kg
ND
0.0050
0.0025
11/02/21 11:06
sec-Butylbenzene
mg/kg
ND
0.0050
0.0022
11/02/21 11:06
Styrene
mg/kg
ND
0.0050
0.0013
11/02/21 11:06
tert-Butyl benzene
mg/kg
ND
0.0050
0.0018
11/02/21 11:06
Tetrachloroethene
mg/kg
ND
0.0050
0.0016
11/02/21 11:06
Toluene
mg/kg
ND
0.0050
0.0014
11/02/21 11:06
trans-1,2-Dichloroethene
mg/kg
ND
0.0050
0.0018
11/02/21 11:06
trans- 1,3-Dichloropropene
mg/kg
ND
0.0050
0.0017
11/02/21 11:06
Trichloroethene
mg/kg
ND
0.0050
0.0013
11/02/21 11:06
Trichlorofluoromethane
mg/kg
ND
0.0050
0.0028
11/02/21 11:06
Vinyl acetate
mg/kg
ND
0.050
0.0036
11/02/21 11:06
Vinyl chloride
mg/kg
ND
0.010
0.0025
11/02/21 11:06
Xylene (Total)
mg/kg
ND
0.010
0.0028
11/02/21 11:06
1,2-Dichloroethane-d4 (S)
%
109
70-130
11/02/21 11:06
4-Bromofluorobenzene (S)
%
99
69-134
11/02/21 11:06
Toluene-d8 (S)
%
102
70-130
11/02/21 11:06
Qualifiers
LABORATORY CONTROL SAMPLE:
3443081
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
1.2
1.3
106
70-130
1,1,1-Trichloroethane
mg/kg
1.2
1.2
96
70-130
1,1,2,2-Tetrachloroethane
mg/kg
1.2
1.3
104
70-130
1,1,2-Trichloroethane
mg/kg
1.2
1.3
102
70-130
1,1-Dichloroethane
mg/kg
1.2
1.3
100
70-130
1,1-Dichloroethene
mg/kg
1.2
1.2
97
70-130
1,1-Dichloropropene
mg/kg
1.2
1.2
96
70-130
1,2,3-Trichlorobenzene
mg/kg
1.2
1.3
104
65-130
1,2,3-Trichloropropane
mg/kg
1.2
1.4
110
70-130
1,2,4-Trichlorobenzene
mg/kg
1.2
1.2
100
68-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 55 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
LABORATORY CONTROL SAMPLE:
Parameter
3443081
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trimethylbenzene
mg/kg
1.2
1.3
106
70-130
1,2-Dibromo-3-chloropropane
mg/kg
1.2
1.2
96
70-130
1,2-Dibromoethane (EDB)
mg/kg
1.2
1.3
100
70-130
1,2-Dichlorobenzene
mg/kg
1.2
1.4
108
70-130
1,2-Dichloroethane
mg/kg
1.2
1.2
99
63-130
1,2-Dichloropropane
mg/kg
1.2
1.2
99
70-130
1,3,5-Trimethylbenzene
mg/kg
1.2
1.4
108
70-130
1,3-Dichlorobenzene
mg/kg
1.2
1.4
110
70-130
1,3-Dichloropropane
mg/kg
1.2
1.3
101
70-130
1,4-Dichlorobenzene
mg/kg
1.2
1.3
102
70-130
2,2-Dichloropropane
mg/kg
1.2
1.2
98
66-130
2-Butanone (MEK)
mg/kg
2.5
2.5
98
70-130
2-Chlorotoluene
mg/kg
1.2
1.3
105
70-130
2-Hexanone
mg/kg
2.5
2.6
104
70-130
4-Chlorotoluene
mg/kg
1.2
1.3
103
70-130
4-Methyl-2-pentanone (MIBK)
mg/kg
2.5
2.6
102
70-130
Acetone
mg/kg
2.5
2.5
99
69-130
Benzene
mg/kg
1.2
1.2
97
70-130
Bromobenzene
mg/kg
1.2
1.3
107
70-130
Bromochloromethane
mg/kg
1.2
1.3
105
70-130
Bromodichloromethane
mg/kg
1.2
1.3
106
69-130
Bromoform
mg/kg
1.2
1.4
113
70-130
Bromomethane
mg/kg
1.2
1.5
122
52-130 v1
Carbon tetrachloride
mg/kg
1.2
1.2
100
70-130
Chlorobenzene
mg/kg
1.2
1.3
106
70-130
Chloroethane
mg/kg
1.2
1.3
102
65-130
Chloroform
mg/kg
1.2
1.3
102
70-130
Chloromethane
mg/kg
1.2
1.1
91
55-130
cis-1,2-Dichloroethene
mg/kg
1.2
1.3
100
70-130
cis-1,3-Dichloropropene
mg/kg
1.2
1.2
99
70-130
Dibromochloromethane
mg/kg
1.2
1.3
107
70-130
Dibromomethane
mg/kg
1.2
1.4
108
70-130
Dichlorodifluoromethane
mg/kg
1.2
1.2
97
45-156
Diisopropyl ether
mg/kg
1.2
1.2
98
70-130
Ethylbenzene
mg/kg
1.2
1.2
99
70-130
Hexachloro-1,3-butadiene
mg/kg
1.2
1.4
109
66-130
Isopropylbenzene (Cumene)
mg/kg
1.2
1.4
111
70-130
m&p-Xylene
mg/kg
2.5
2.7
108
70-130
Methyl-tert-butyl ether
mg/kg
1.2
1.2
95
70-130
Methylene Chloride
mg/kg
1.2
1.2
99
65-130
n-Butylbenzene
mg/kg
1.2
1.3
104
67-130
n-Propylbenzene
mg/kg
1.2
1.3
105
70-130
Naphthalene
mg/kg
1.2
1.3
102
70-130
o-Xylene
mg/kg
1.2
1.3
105
70-130
p-Isopropyltoluene
mg/kg
1.2
1.3
107
67-130
sec-Butylbenzene
mg/kg
1.2
1.3
105
69-130
Styrene
mg/kg
1.2
1.4
109
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 56 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
LABORATORY CONTROL SAMPLE:
Parameter
3443081
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
tert-Butyl benzene
mg/kg
1.2
1.4
110
67-130
Tetrachloroethene
mg/kg
1.2
1.3
106
70-130
Toluene
mg/kg
1.2
1.3
101
70-130
trans-1,2-Dichloroethene
mg/kg
1.2
1.2
98
70-130
trans- 1,3-Dichloropropene
mg/kg
1.2
1.3
100
68-130
Trichloroethene
mg/kg
1.2
1.2
100
70-130
Trichlorofluoromethane
mg/kg
1.2
1.2
94
70-130
Vinyl acetate
mg/kg
2.5
2.8
112
70-130
Vinyl chloride
mg/kg
1.2
1.2
98
61-130
Xylene (Total)
mg/kg
3.8
4.0
107
70-130
1,2-Dichloroethane-d4 (S)
%
92
70-130
4-Bromofluorobenzene (S)
%
101
69-134
Toluene-d8 (S)
%
99
70-130
MATRIX SPIKE SAMPLE:
Parameter
3443083
Units
92569860026
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
ND
0.59
0.58
100
70-131
1,1,1-Trichloroethane
mg/kg
ND
0.59
0.62
106
65-133
1,1,2,2-Tetrachloroethane
mg/kg
ND
0.59
0.58
98
66-130
1,1,2-Trichloroethane
mg/kg
ND
0.59
0.60
103
66-133
1,1-Dichloroethane
mg/kg
ND
0.59
0.63
108
65-130
1,1-Dichloroethene
mg/kg
ND
0.59
0.66
113
10-158
1,1-Dichloropropene
mg/kg
ND
0.59
0.65
111
68-133
1,2,3-Trichlorobenzene
mg/kg
ND
0.59
0.62
106
27-138
1,2,3-Trichloropropane
mg/kg
ND
0.59
0.61
104
67-130
1,2,4-Trichlorobenzene
mg/kg
ND
0.59
0.61
104
51-134
1,2,4-Trimethylbenzene
mg/kg
ND
0.59
0.65
110
63-136
1,2-Dibromo-3-chloropropane
mg/kg
ND
0.59
0.53
90
32-130
1,2-Dibromoethane (EDB)
mg/kg
ND
0.59
0.58
98
70-130
1,2-Dichlorobenzene
mg/kg
ND
0.59
0.66
112
69-130
1,2-Dichloroethane
mg/kg
ND
0.59
0.60
102
59-130
1,2-Dichloropropane
mg/kg
ND
0.59
0.62
106
70-130
1,3,5-Trimethylbenzene
mg/kg
ND
0.59
0.68
116
65-137
1,3-Dichlorobenzene
mg/kg
ND
0.59
0.67
113
70-130
1,3-Dichloropropane
mg/kg
ND
0.59
0.60
102
70-130
1,4-Dichlorobenzene
mg/kg
ND
0.59
0.62
105
68-130
2,2-Dichloropropane
mg/kg
ND
0.59
0.60
101
32-130
2-Butanone (MEK)
mg/kg
ND
1.2
1.2
103
10-136
2-Chlorotoluene
mg/kg
ND
0.59
0.65
110
69-141
2-Hexanone
mg/kg
ND
1.2
1.1
95
10-144
4-Chlorotoluene
mg/kg
ND
0.59
0.63
107
70-132
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
1.2
1.2
101
25-143
Acetone
mg/kg
ND
1.2
1.1
96
10-130
Benzene
mg/kg
ND
0.59
0.62
106
67-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 57 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
MATRIX SPIKE SAMPLE:
3443083
92569860026
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Bromobenzene
mg/kg
ND
0.59
0.64
110
70-130
Bromochloromethane
mg/kg
ND
0.59
0.63
107
69-134
Bromodichloromethane
mg/kg
ND
0.59
0.58
98
64-130
Bromoform
mg/kg
ND
0.59
0.52
88
62-130
Bromomethane
mg/kg
ND
0.59
0.40
69
20-176 v1
Carbon tetrachloride
mg/kg
ND
0.59
0.59
101
65-140
Chlorobenzene
mg/kg
ND
0.59
0.64
109
70-130
Chloroethane
mg/kg
ND
0.59
0.29
49
10-130
Chloroform
mg/kg
ND
0.59
0.64
108
63-130
Chloromethane
mg/kg
ND
0.59
0.58
99
58-130
cis-1,2-Dichloroethene
mg/kg
ND
0.59
0.62
106
66-130
cis-1,3-Dichloropropene
mg/kg
ND
0.59
0.59
100
67-130
Dibromochloromethane
mg/kg
ND
0.59
0.53
90
67-130
Dibromomethane
mg/kg
ND
0.59
0.61
104
63-131
Dichlorodifluoromethane
mg/kg
ND
0.59
0.62
106
44-180
Diisopropyl ether
mg/kg
ND
0.59
0.59
101
63-130
Ethylbenzene
mg/kg
ND
0.59
0.61
104
66-130
Hexachloro-1,3-butadiene
mg/kg
ND
0.59
0.72
123
64-150
Isopropylbenzene (Cumene)
mg/kg
ND
0.59
0.67
115
69-135
m&p-Xylene
mg/kg
ND
1.2
1.3
112
60-133
Methyl-tert-butyl ether
mg/kg
ND
0.59
0.59
101
65-130
Methylene Chloride
mg/kg
ND
0.59
0.59
101
61-130
n-Butylbenzene
mg/kg
ND
0.59
0.70
119
65-140
n-Propylbenzene
mg/kg
ND
0.59
0.67
115
67-140
Naphthalene
mg/kg
ND
0.59
0.59
101
15-145
o-Xylene
mg/kg
ND
0.59
0.63
108
66-133
p-Isopropyltoluene
mg/kg
ND
0.59
0.70
119
56-147
sec-Butylbenzene
mg/kg
ND
0.59
0.69
117
65-139
Styrene
mg/kg
ND
0.59
0.63
108
70-132
tert-Butyl benzene
mg/kg
ND
0.59
0.65
111
62-135
Tetrachloroethene
mg/kg
ND
0.59
0.66
112
70-135
Toluene
mg/kg
ND
0.59
0.64
109
67-130
trans-1,2-Dichloroethene
mg/kg
ND
0.59
0.65
110
69-130
trans- 1,3-Dichloropropene
mg/kg
ND
0.59
0.57
97
62-130
Trichloroethene
mg/kg
ND
0.59
0.64
109
70-135
Trichlorofluoromethane
mg/kg
ND
0.59
0.42
71
10-130
Vinyl acetate
mg/kg
ND
1.2
1.3
108
53-130
Vinyl chloride
mg/kg
ND
0.59
0.59
101
61-148
Xylene (Total)
mg/kg
ND
1.7
1.9
111
63-132
1,2-Dichloroethane-d4 (S)
%
96
70-130
4-Bromofluorobenzene (S)
%
97
69-134
Toluene-d8 (S)
%
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 58 of 87

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
SAMPLE DUPLICATE: 3443082
Parameter
Units
92569860025
Result
Dup
Result RPD
Max
RPD Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
ND
ND
30
1,1,1-Trichloroethane
mg/kg
ND
ND
30
1,1,2,2-Tetrachloroethane
mg/kg
ND
ND
30
1,1,2-Trichloroethane
mg/kg
ND
ND
30
1,1-Dichloroethane
mg/kg
ND
ND
30
1,1-Dichloroethene
mg/kg
ND
ND
30
1,1-Dichloropropene
mg/kg
ND
ND
30
1,2,3-Trichlorobenzene
mg/kg
ND
ND
30
1,2,3-Trichloropropane
mg/kg
ND
ND
30
1,2,4-Trichlorobenzene
mg/kg
ND
ND
30
1,2,4-Trimethylbenzene
mg/kg
ND
ND
30
1,2-Dibromo-3-chloropropane
mg/kg
ND
ND
30
1,2-Dibromoethane (EDB)
mg/kg
ND
ND
30
1,2-Dichlorobenzene
mg/kg
ND
ND
30
1,2-Dichloroethane
mg/kg
ND
ND
30
1,2-Dichloropropane
mg/kg
ND
ND
30
1,3,5-Trimethylbenzene
mg/kg
ND
ND
30
1,3-Dichlorobenzene
mg/kg
ND
ND
30
1,3-Dichloropropane
mg/kg
ND
ND
30
1,4-Dichlorobenzene
mg/kg
ND
ND
30
2,2-Dichloropropane
mg/kg
ND
ND
30
2-Butanone (MEK)
mg/kg
ND
ND
30
2-Chlorotoluene
mg/kg
ND
ND
30
2-Hexanone
mg/kg
ND
ND
30
4-Chlorotoluene
mg/kg
ND
ND
30
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
ND
30
Acetone
mg/kg
ND
ND
30
Benzene
mg/kg
ND
ND
30
Bromobenzene
mg/kg
ND
ND
30
Bromochloromethane
mg/kg
ND
ND
30
Bromodichloromethane
mg/kg
ND
ND
30
Bromoform
mg/kg
ND
ND
30
Bromomethane
mg/kg
ND
ND
30 v1
Carbon tetrachloride
mg/kg
ND
ND
30
Chlorobenzene
mg/kg
ND
ND
30
Chloroethane
mg/kg
ND
ND
30
Chloroform
mg/kg
ND
ND
30
Chloromethane
mg/kg
ND
ND
30
cis-1,2-Dichloroethene
mg/kg
ND
ND
30
cis-1,3-Dichloropropene
mg/kg
ND
ND
30
Dibromochloromethane
mg/kg
ND
ND
30
Dibromomethane
mg/kg
ND
ND
30
Dichlorodifluoromethane
mg/kg
ND
ND
30
Diisopropyl ether
mg/kg
ND
ND
30
Ethylbenzene
mg/kg
ND
ND
30
Hexachloro-1,3-butadiene
mg/kg
ND
ND
30
Isopropylbenzene (Cumene)
mg/kg
ND
ND
30
Results presented on this page are in the units
indicated by the "Units" column except where an alternate unit
is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 59 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
SAMPLE DUPLICATE: 3443082
Parameter
Units
92569860025
Result
Dup
Result
m&p-Xylene
mg/kg
ND
ND
Methyl-tert-butyl ether
mg/kg
ND
ND
Methylene Chloride
mg/kg
ND
ND
n-Butylbenzene
mg/kg
ND
ND
n-Propylbenzene
mg/kg
ND
ND
Naphthalene
mg/kg
ND
ND
o-Xylene
mg/kg
ND
ND
p-Isopropyltoluene
mg/kg
ND
ND
sec-Butylbenzene
mg/kg
ND
ND
Styrene
mg/kg
ND
ND
tert-Butyl benzene
mg/kg
ND
ND
Tetrachloroethene
mg/kg
ND
ND
Toluene
mg/kg
ND
ND
trans-1,2-Dichloroethene
mg/kg
ND
ND
trans- 1,3-Dichloropropene
mg/kg
ND
ND
Trichloroethene
mg/kg
ND
ND
Trichlorofluoromethane
mg/kg
ND
ND
Vinyl acetate
mg/kg
ND
ND
Vinyl chloride
mg/kg
ND
ND
Xylene (Total)
mg/kg
ND
ND
1,2-Dichloroethane-d4 (S)
%
105
104
4-Bromofluorobenzene (S)
%
100
98
Toluene-d8(S)
%
101
100
Max
RPD RPD Qualifiers
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC.
Page 60 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
QC Batch: 656871 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92569749001, 92569749002, 92569749003, 92569749004
METHOD BLANK: 3443239 Matrix: Water
Associated Lab Samples: 92569749001, 92569749002, 92569749003, 92569749004
Blank Reporting
Parameter Units Result Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.31
11/02/21 23:22
1,1,1-Trichloroethane
ug/L
ND
1.0
0.33
11/02/21 23:22
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
11/02/21 23:22
1,1,2-Trichloroethane
ug/L
ND
1.0
0.32
11/02/21 23:22
1,1-Dichloroethane
ug/L
ND
1.0
0.37
11/02/21 23:22
1,1-Dichloroethene
ug/L
ND
1.0
0.35
11/02/21 23:22
1,1-Dichloropropene
ug/L
ND
1.0
0.43
11/02/21 23:22
1,2,3-Trichlorobenzene
ug/L
ND
1.0
0.81
11/02/21 23:22
1,2,3-Trichloropropane
ug/L
ND
1.0
0.26
11/02/21 23:22
1,2,4-Trichlorobenzene
ug/L
ND
1.0
0.64
11/02/21 23:22
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
0.34
11/02/21 23:22
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
11/02/21 23:22
1,2-Dichlorobenzene
ug/L
ND
1.0
0.34
11/02/21 23:22
1,2-Dichloroethane
ug/L
ND
1.0
0.32
11/02/21 23:22
1,2-Dichloropropane
ug/L
ND
1.0
0.36
11/02/21 23:22
1,3-Dichlorobenzene
ug/L
ND
1.0
0.34
11/02/21 23:22
1,3-Dichloropropane
ug/L
ND
1.0
0.28
11/02/21 23:22
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
11/02/21 23:22
2,2-Dichloropropane
ug/L
ND
1.0
0.39
11/02/21 23:22
2-Butanone (MEK)
ug/L
ND
5.0
4.0
11/02/21 23:22
2-Chlorotoluene
ug/L
ND
1.0
0.32
11/02/21 23:22
2-Hexanone
ug/L
ND
5.0
0.48
11/02/21 23:22
4-Chlorotoluene
ug/L
ND
1.0
0.32
11/02/21 23:22
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
2.7
11/02/21 23:22
Acetone
ug/L
ND
25.0
5.1
11/02/21 23:22
Benzene
ug/L
ND
1.0
0.34
11/02/21 23:22
Bromobenzene
ug/L
ND
1.0
0.29
11/02/21 23:22
Bromochloromethane
ug/L
ND
1.0
0.47
11/02/21 23:22
Bromodichloromethane
ug/L
ND
1.0
0.31
11/02/21 23:22
Bromoform
ug/L
ND
1.0
0.34
11/02/21 23:22
Bromomethane
ug/L
ND
2.0
1.7
11/02/21 23:22
Carbon tetrachloride
ug/L
ND
1.0
0.33
11/02/21 23:22
Chlorobenzene
ug/L
ND
1.0
0.28
11/02/21 23:22
Chloroethane
ug/L
ND
1.0
0.65
11/02/21 23:22
Chloroform
ug/L
ND
1.0
0.43
11/02/21 23:22
Chloromethane
ug/L
ND
1.0
0.54
11/02/21 23:22
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.38
11/02/21 23:22
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.36
11/02/21 23:22
Dibromochloromethane
ug/L
ND
1.0
0.36
11/02/21 23:22
Dibromomethane
ug/L
ND
1.0
0.39
11/02/21 23:22
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 61 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
METHOD BLANK: 3443239 Matrix: Water
Associated Lab Samples: 92569749001, 92569749002, 92569749003, 92569749004
Blank Reporting
Parameter Units Result Limit
MDL
Analyzed Qualifiers
Dichlorodifluoromethane
ug/L
ND
1.0
0.35
11/02/21 23:22
Diisopropyl ether
ug/L
ND
1.0
0.31
11/02/21 23:22
Ethylbenzene
ug/L
ND
1.0
0.30
11/02/21 23:22
Hexachloro-1,3-butadiene
ug/L
ND
2.0
1.5
11/02/21 23:22
m&p-Xylene
ug/L
ND
2.0
0.71
11/02/21 23:22
Methyl-tert-butyl ether
ug/L
ND
1.0
0.42
11/02/21 23:22
Methylene Chloride
ug/L
ND
5.0
2.0
11/02/21 23:22
Naphthalene
ug/L
ND
1.0
0.64
11/02/21 23:22
o-Xylene
ug/L
ND
1.0
0.34
11/02/21 23:22
p-Isopropyltoluene
ug/L
ND
1.0
0.41
11/02/21 23:22
Styrene
ug/L
ND
1.0
0.29
11/02/21 23:22
Tetrachloroethene
ug/L
ND
1.0
0.29
11/02/21 23:22
Toluene
ug/L
ND
1.0
0.48
11/02/21 23:22
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.40
11/02/21 23:22
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.36
11/02/21 23:22
Trichloroethene
ug/L
ND
1.0
0.38
11/02/21 23:22
Trichlorofluoromethane
ug/L
ND
1.0
0.30
11/02/21 23:22
Vinyl acetate
ug/L
ND
2.0
1.3
11/02/21 23:22
Vinyl chloride
ug/L
ND
1.0
0.39
11/02/21 23:22
Xylene (Total)
ug/L
ND
1.0
0.34
11/02/21 23:22
1,2-Dichloroethane-d4 (S)
%
96
70-130
11/02/21 23:22
4-Bromofluorobenzene (S)
%
99
70-130
11/02/21 23:22
Toluene-d8 (S)
%
104
70-130
11/02/21 23:22
LABORATORY CONTROL SAMPLE:
3443240
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
48.9
98
70-130
1,1,1-Trichloroethane
ug/L
50
50.4
101
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
48.9
98
70-130
1,1,2-Trichloroethane
ug/L
50
49.6
99
70-130
1,1-Dichloroethane
ug/L
50
48.7
97
70-130
1,1-Dichloroethene
ug/L
50
49.0
98
70-132
1,1-Dichloropropene
ug/L
50
51.2
102
70-131
1,2,3-Trichlorobenzene
ug/L
50
51.1
102
70-134
1,2,3-Trichloropropane
ug/L
50
47.5
95
70-130
1,2,4-Trichlorobenzene
ug/L
50
51.1
102
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
52.6
105
70-132
1,2-Dibromoethane (EDB)
ug/L
50
51.2
102
70-130
1,2-Dichlorobenzene
ug/L
50
46.8
94
70-130
1,2-Dichloroethane
ug/L
50
48.3
97
70-130
1,2-Dichloropropane
ug/L
50
49.8
100
70-130
1,3-Dichlorobenzene
ug/L
50
45.8
92
70-130
1,3-Dichloropropane
ug/L
50
49.9
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 62 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
LABORATORY CONTROL SAMPLE:
Parameter
3443240
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,4-Dichlorobenzene
ug/L
50
48.0
96
70-130
2,2-Dichloropropane
ug/L
50
49.7
99
70-130
2-Butanone (MEK)
ug/L
100
113
113
70-133
2-Chlorotoluene
ug/L
50
47.8
96
70-130
2-Hexanone
ug/L
100
104
104
70-130
4-Chlorotoluene
ug/L
50
45.5
91
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
102
102
70-130
Acetone
ug/L
100
105
105
70-144
Benzene
ug/L
50
47.8
96
70-130
Bromobenzene
ug/L
50
48.2
96
70-130
Bromochloromethane
ug/L
50
50.8
102
70-130
Bromodichloromethane
ug/L
50
47.6
95
70-130
Bromoform
ug/L
50
48.7
97
70-131
Bromomethane
ug/L
50
51.7
103
30-177
Carbon tetrachloride
ug/L
50
48.8
98
70-130
Chlorobenzene
ug/L
50
46.4
93
70-130
Chloroethane
ug/L
50
41.9
84
46-131
Chloroform
ug/L
50
48.8
98
70-130
Chloromethane
ug/L
50
43.5
87
49-130
cis-1,2-Dichloroethene
ug/L
50
48.3
97
70-130
cis-1,3-Dichloropropene
ug/L
50
50.3
101
70-130
Dibromochloromethane
ug/L
50
51.1
102
70-130
Dibromomethane
ug/L
50
49.1
98
70-130
Dichlorodifluoromethane
ug/L
50
49.0
98
52-134
Diisopropyl ether
ug/L
50
49.3
99
70-131
Ethylbenzene
ug/L
50
46.3
93
70-130
Hexachloro-1,3-butadiene
ug/L
50
56.5
113
70-131
m&p-Xylene
ug/L
100
92.7
93
70-130
Methyl-tert-butyl ether
ug/L
50
51.7
103
70-130
Methylene Chloride
ug/L
50
49.1
98
68-130
Naphthalene
ug/L
50
49.6
99
70-133
o-Xylene
ug/L
50
46.8
94
70-130
p-Isopropyltoluene
ug/L
50
49.2
98
70-130
Styrene
ug/L
50
47.8
96
70-130
Tetrachloroethene
ug/L
50
46.5
93
70-130
Toluene
ug/L
50
45.9
92
70-130
trans-1,2-Dichloroethene
ug/L
50
49.6
99
70-130
trans- 1,3-Dichloropropene
ug/L
50
49.2
98
70-130
Trichloroethene
ug/L
50
48.6
97
70-130
Trichlorofluoromethane
ug/L
50
42.7
85
61-130
Vinyl acetate
ug/L
100
119
119
70-140
Vinyl chloride
ug/L
50
46.6
93
59-142
Xylene (Total)
ug/L
150
140
93
70-130
1,2-Dichloroethane-d4 (S)
%
93
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
96
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 63 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3443241
MS
92569678002 Spike
Parameter Units Result Conc.
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1, 2,2-Tetrachloroethane
1,1, 2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2-Dibromo-3-
chloropropane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone
(MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
3443242
MSD
Spike MS MSD MS MSD % Rec
Conc. Result Result % Rec % Rec Limits
ug/L
ND
20
20
23.1
21.0
115
105
70-135
ug/L
ND
20
20
25.6
23.5
128
118
70-148
ug/L
ND
20
20
22.8
20.8
114
104
70-131
ug/L
ND
20
20
24.7
21.9
123
109
70-136
ug/L
ND
20
20
24.2
22.8
121
114
70-147
ug/L
ND
20
20
25.3
23.8
127
119
70-158
ug/L
ND
20
20
24.8
23.2
124
116
70-149
ug/L
ND
20
20
21.5
21.0
107
105
68-140
ug/L
ND
20
20
22.6
20.8
113
104
67-137
ug/L
ND
20
20
21.0
21.4
105
107
70-139
ug/L
ND
20
20
23.0
21.1
115
106
69-136
Max
RPD RPD Qual
9 30
8 30
9 30
12 30
6 30
6 30
7 30
2 30
8 30
2 30
8 30
ug/L
ND
20
20
23.0
21.8
115
109
70-137
6
30
ug/L
ND
20
20
22.3
20.2
111
101
70-133
10
30
ug/L
ND
20
20
24.0
22.3
120
112
67-138
7
30
ug/L
ND
20
20
24.8
22.8
124
114
70-138
8
30
ug/L
ND
20
20
22.4
21.4
112
107
70-133
5
30
ug/L
ND
20
20
23.3
21.3
117
106
70-136
9
30
ug/L
ND
20
20
22.9
21.3
114
107
70-133
7
30
ug/L
ND
20
20
23.6
22.8
118
114
52-155
4
30
ug/L
ND
40
40
51.5
45.8
129
114
61-147
12
30
ug/L
ND
20
20
23.0
21.7
115
109
70-141
6
30
ug/L
ND
40
40
46.7
42.6
117
107
67-139
9
30
ug/L
ND
20
20
22.8
21.1
114
106
70-135
8
30
ug/L
ND
40
40
48.8
43.4
122
109
67-136
12
30
ug/L
ND
40
40
50.5
44.5
126
111
55-159
13
30
ug/L
ND
20
20
24.6
22.9
123
115
67-150
7
30
ug/L
ND
20
20
23.6
21.5
118
107
70-134
10
30
ug/L
ND
20
20
24.9
23.3
125
116
70-146
7
30
ug/L
ND
20
20
24.1
22.0
120
110
70-138
9
30
ug/L
ND
20
20
21.7
20.2
108
101
57-138
7
30
ug/L
ND
20
20
22.7
23.4
113
117
10-200
3
30
ug/L
ND
20
20
27.2
25.2
136
126
70-147
8
30
ug/L
ND
20
20
22.9
21.7
114
109
70-137
5
30
ug/L
ND
20
20
23.5
23.7
118
119
51-166
1
30
ug/L
ND
20
20
24.3
23.4
121
117
70-144
3
30
ug/L
ND
20
20
22.6
21.5
113
108
24-161
5
30
ug/L
ND
20
20
24.0
22.7
120
113
67-148
6
30
ug/L
ND
20
20
23.3
21.7
117
109
70-142
7
30
ug/L
ND
20
20
23.5
20.8
117
104
68-138
12
30
ug/L
ND
20
20
23.7
22.5
119
112
70-134
5
30
ug/L
ND
20
20
23.6
22.4
118
112
43-155
5
30
ug/L
ND
20
20
23.3
21.5
117
107
65-146
8
30
ug/L
ND
20
20
23.0
21.8
115
109
68-143
6
30
ug/L
ND
20
20
22.0
23.0
110
115
62-151
4
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 64 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 3443241
3443242
MS
MSD
92569678002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
m&p-Xylene
ug/L
ND
40
40
45.9
43.7
115
109
53-157
5
30
Methyl-tert-butyl ether
ug/L
ND
20
20
22.7
20.5
113
103
59-156
10
30
Methylene Chloride
ug/L
ND
20
20
25.6
23.6
128
118
64-148
8
30
Naphthalene
ug/L
ND
20
20
21.0
19.9
105
100
57-150
5
30
o-Xylene
ug/L
ND
20
20
22.8
21.3
114
106
68-143
7
30
p-Isopropyltoluene
ug/L
ND
20
20
22.6
22.1
113
111
70-141
2
30
Styrene
ug/L
ND
20
20
22.9
21.5
114
107
70-136
6
30
Tetrachloroethene
ug/L
ND
20
20
22.4
21.3
112
107
70-139
5
30
Toluene
ug/L
ND
20
20
23.5
22.0
118
110
47-157
7
30
trans-1,2-Dichloroethene
ug/L
ND
20
20
24.6
23.2
123
116
70-149
6
30
trans-1,3-Dichloropropene
ug/L
ND
20
20
22.6
21.4
113
107
70-138
5
30
Trichloroethene
ug/L
ND
20
20
24.8
23.1
124
116
70-149
7
30
Trichlorofluoromethane
ug/L
ND
20
20
22.9
20.5
115
103
61-154
11
30
Vinyl acetate
ug/L
ND
40
40
48.3
43.1
121
108
48-156
11
30
Vinyl chloride
ug/L
ND
20
20
23.4
22.2
117
111
55-172
5
30
Xylene (Total)
ug/L
ND
60
60
68.7
64.9
115
108
66-145
6
30
1,2-Dichloroethane-d4 (S)
%
97
97
70-130
4-Bromofluorobenzene (S)
%
98
101
70-130
Toluene-d8 (S)
%
98
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC.
Page 65 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
QC Batch: 656743 Analysis Method: EPA 8270E
QC Batch Method: EPA 3510C Analysis Description: 8270E Water MSSV RVE
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92569749001, 92569749002, 92569749003, 92569749004
METHOD BLANK: 3442705 Matrix: Water
Associated Lab Samples: 92569749001, 92569749002, 92569749003, 92569749004
Blank Reporting
Parameter Units Result Limit
MDL
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
10.0
1.7
11/02/21 11:44
1,2-Dichlorobenzene
ug/L
ND
10.0
1.8
11/02/21 11:44
1,3-Dichlorobenzene
ug/L
ND
10.0
1.6
11/02/21 11:44
1,4-Dichlorobenzene
ug/L
ND
10.0
1.7
11/02/21 11:44
1-Methylnaphthalene
ug/L
ND
10.0
2.0
11/02/21 11:44
2,2'-Oxybis(1-chloropropane)
ug/L
ND
10.0
1.2
11/02/21 11:44
2,4,5-Trichlorophenol
ug/L
ND
10.0
1.4
11/02/21 11:44
2,4,6-Trichlorophenol
ug/L
ND
10.0
1.6
11/02/21 11:44
2,4-Dichlorophenol
ug/L
ND
10.0
1.4
11/02/21 11:44
2,4-Dimethylphenol
ug/L
ND
10.0
1.7
11/02/21 11:44
2,4-Dinitrophenol
ug/L
ND
50.0
26.0
11/02/21 11:44
2,4-Dinitrotoluene
ug/L
ND
10.0
1.6
11/02/21 11:44
2,6-Dinitrotoluene
ug/L
ND
10.0
1.7
11/02/21 11:44
2-Chloronaphthalene
ug/L
ND
10.0
1.7
11/02/21 11:44
2-Chlorophenol
ug/L
ND
10.0
1.2
11/02/21 11:44
2-Methylnaphthalene
ug/L
ND
10.0
1.9
11/02/21 11:44
2-Methylphenol(o-Cresol)
ug/L
ND
10.0
1.9
11/02/21 11:44
2-Nitroaniline
ug/L
ND
20.0
3.0
11/02/21 11:44
2-Nitrophenol
ug/L
ND
10.0
1.4
11/02/21 11:44
3&4-Methyl phenol (m&p Cresol)
ug/L
ND
10.0
1.2
11/02/21 11:44
3,3'-Dichlorobenzidine
ug/L
ND
20.0
8.1
11/02/21 11:44
3-Nitroaniline
ug/L
ND
20.0
3.8
11/02/21 11:44
4,6-Dinitro-2-methyl phenol
ug/L
ND
20.0
3.4
11/02/21 11:44
4-Bromophenylphenyl ether
ug/L
ND
10.0
1.8
11/02/21 11:44
4-ChIoro-3-methyl phenol
ug/L
ND
10.0
3.3
11/02/21 11:44
4-Chloroaniline
ug/L
ND
20.0
3.6
11/02/21 11:44
4-Chlorophenylphenyl ether
ug/L
ND
10.0
2.0
11/02/21 11:44
4-Nitroaniline
ug/L
ND
20.0
5.1
11/02/21 11:44
4-Nitrophenol
ug/L
ND
50.0
6.6
11/02/21 11:44
Acenaphthene
ug/L
ND
10.0
2.0
11/02/21 11:44
Acenaphthylene
ug/L
ND
10.0
2.0
11/02/21 11:44
Aniline
ug/L
ND
10.0
1.6
11/02/21 11:44
Anthracene
ug/L
ND
10.0
2.3
11/02/21 11:44
Benzo(a)anthracene
ug/L
ND
10.0
2.7
11/02/21 11:44
Benzo(a)pyrene
ug/L
ND
10.0
2.8
11/02/21 11:44
Benzo(b)fluoranthene
ug/L
ND
10.0
2.6
11/02/21 11:44
Benzo(g,h,i)perylene
ug/L
ND
10.0
2.8
11/02/21 11:44
Benzo(k)fluoranthene
ug/L
ND
10.0
2.7
11/02/21 11:44
Benzoic Acid
ug/L
ND
50.0
3.4
11/02/21 11:44
Benzyl alcohol
ug/L
ND
20.0
2.9
11/02/21 11:44
v1
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 66 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
METHOD BLANK: 3442705 Matrix: Water
Associated Lab Samples: 92569749001, 92569749002, 92569749003, 92569749004
Blank Reporting
Parameter Units Result Limit
MDL
Analyzed
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
1.8
11/02/21 11:44
bis(2-Chloroethyl) ether
ug/L
ND
10.0
1.9
11/02/21 11:44
bis(2-Ethylhexyl)phthalate
ug/L
ND
6.0
3.7
11/02/21 11:44
Butylbenzylphthalate
ug/L
ND
10.0
3.1
11/02/21 11:44
Chrysene
ug/L
ND
10.0
2.8
11/02/21 11:44
Di-n-butylphthalate
ug/L
ND
10.0
2.2
11/02/21 11:44
Di-n-octylphthalate
ug/L
ND
10.0
3.9
11/02/21 11:44
Dibenz(a,h)anthracene
ug/L
ND
10.0
3.0
11/02/21 11:44
Dibenzofuran
ug/L
ND
10.0
2.1
11/02/21 11:44
Diethylphthalate
ug/L
ND
10.0
2.0
11/02/21 11:44
Dimethylphthalate
ug/L
ND
10.0
2.1
11/02/21 11:44
Fluoranthene
ug/L
ND
10.0
2.2
11/02/21 11:44
Fluorene
ug/L
ND
10.0
2.1
11/02/21 11:44
Hexachloro-1,3-butadiene
ug/L
ND
10.0
1.8
11/02/21 11:44
Hexachlorobenzene
ug/L
ND
10.0
2.2
11/02/21 11:44
Hexachlorocyclopentadiene
ug/L
ND
10.0
1.6
11/02/21 11:44
Hexachloroethane
ug/L
ND
10.0
1.4
11/02/21 11:44
Indeno(1,2,3-cd)pyrene
ug/L
ND
10.0
2.9
11/02/21 11:44
Isophorone
ug/L
ND
10.0
1.7
11/02/21 11:44
N-Nitroso-di-n-propylamine
ug/L
ND
10.0
1.3
11/02/21 11:44
N-Nitrosodimethylamine
ug/L
ND
10.0
1.9
11/02/21 11:44
N-Nitrosodiphenylamine
ug/L
ND
10.0
3.0
11/02/21 11:44
Naphthalene
ug/L
ND
10.0
2.1
11/02/21 11:44
Nitrobenzene
ug/L
ND
10.0
1.9
11/02/21 11:44
Pentachlorophenol
ug/L
ND
20.0
3.8
11/02/21 11:44
Phenanthrene
ug/L
ND
10.0
2.0
11/02/21 11:44
Phenol
ug/L
ND
10.0
1.4
11/02/21 11:44
Pyrene
ug/L
ND
10.0
2.2
11/02/21 11:44
2,4,6-Tribromophenol (S)
%
107
10-144
11/02/21 11:44
2-Fluorobiphenyl (S)
%
99
10-130
11/02/21 11:44
2-Fluorophenol (S)
%
75
10-130
11/02/21 11:44
Nitrobenzene-d5 (S)
%
108
10-144
11/02/21 11:44
Phenol-d6 (S)
%
56
10-130
11/02/21 11:44
Terphenyl-d14 (S)
%
120
34-163
11/02/21 11:44
Qualifiers
LABORATORY CONTROL SAMPLE:
3442706
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
28.0
56
18-130
1,2-Dichlorobenzene
ug/L
50
28.9
58
20-130
1,3-Dichlorobenzene
ug/L
50
26.7
53
18-130
1,4-Dichlorobenzene
ug/L
50
27.7
55
18-130
1-Methylnaphthalene
ug/L
50
36.0
72
29-130
2,2'-Oxybis(1-chloropropane)
ug/L
50
48.2
96
28-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 67 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
LABORATORY CONTROL SAMPLE:
Parameter
3442706
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,4,5-Trichlorophenol
ug/L
50
48.4
97
35-130
2,4,6-Trichlorophenol
ug/L
50
49.5
99
31-130
2,4-Dichlorophenol
ug/L
50
46.9
94
35-130
2,4-Dimethylphenol
ug/L
50
47.0
94
34-130
2,4-Dinitrophenol
ug/L
250
73.8
30
10-153
2,4-Dinitrotoluene
ug/L
50
49.1
98
37-136
2,6-Dinitrotoluene
ug/L
50
50.0
100
33-136
2-Chloronaphthalene
ug/L
50
43.8
88
26-130
2-Chlorophenol
ug/L
50
46.2
92
37-130
2-Methylnaphthalene
ug/L
50
35.5
71
29-130
2-Methylphenol(o-Cresol)
ug/L
50
44.6
89
35-130
2-Nitroaniline
ug/L
100
109
109
37-130
2-Nitrophenol
ug/L
50
46.6
93
32-130
3&4-Methyl phenol (m&p Cresol)
ug/L
50
41.9
84
34-130
3,3'-Dichlorobenzidine
ug/L
100
98.7
99
34-136 v1
3-Nitroaniline
ug/L
100
107
107
37-138
4,6-Dinitro-2-methyl phenol
ug/L
100
88.9
89
21-157
4-Bromophenylphenyl ether
ug/L
50
48.6
97
38-130
4-ChIoro-3-methyl phenol
ug/L
100
87.6
88
37-130
4-Chloroaniline
ug/L
100
98.1
98
38-130
4-Chlorophenylphenyl ether
ug/L
50
45.9
92
33-130
4-Nitroaniline
ug/L
100
106
106
42-137
4-Nitrophenol
ug/L
250
125
50
10-130
Acenaphthene
ug/L
50
51.4
103
33-130
Acenaphthylene
ug/L
50
50.8
102
35-130
Aniline
ug/L
50
45.3
91
22-130
Anthracene
ug/L
50
55.4
111
48-130
Benzo(a)anthracene
ug/L
50
56.6
113
48-137
Benzo(a)pyrene
ug/L
50
61.5
123
49-138
Benzo(b)fluoranthene
ug/L
50
59.6
119
52-138
Benzo(g,h,i)perylene
ug/L
50
64.1
128
48-140
Benzo(k)fluoranthene
ug/L
50
60.1
120
48-139
Benzoic Acid
ug/L
250
14.3J
6
10-130 L2
Benzyl alcohol
ug/L
100
94.1
94
35-130
bis(2-Chloroethoxy)methane
ug/L
50
46.3
93
34-130
bis(2-Chloroethyl) ether
ug/L
50
48.2
96
36-130
bis(2-Ethylhexyl)phthalate
ug/L
50
61.2
122
32-165
Butylbenzylphthalate
ug/L
50
59.0
118
34-161
Chrysene
ug/L
50
55.4
111
47-131
Di-n-butylphthalate
ug/L
50
54.5
109
39-144
Di-n-octylphthalate
ug/L
50
59.2
118
30-170
Dibenz(a,h)anthracene
ug/L
50
61.2
122
49-138
Dibenzofuran
ug/L
50
49.1
98
33-130
Diethylphthalate
ug/L
50
46.7
93
38-131
Dimethylphthalate
ug/L
50
47.2
94
37-130
Fluoranthene
ug/L
50
53.0
106
46-137
Fluorene
ug/L
50
51.6
103
37-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 68 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
LABORATORY CONTROL SAMPLE:
Parameter
3442706
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Hexachloro-1,3-butadiene
ug/L
50
23.2
46
11-130
Hexachlorobenzene
ug/L
50
46.6
93
38-130
Hexachlorocyclopentadiene
ug/L
50
25.7
51
10-130
Hexachloroethane
ug/L
50
25.8
52
14-130
Indeno(1,2,3-cd)pyrene
ug/L
50
60.9
122
41-130
Isophorone
ug/L
50
43.8
88
33-130
N-Nitroso-di-n-propylamine
ug/L
50
48.0
96
36-130
N-Nitrosodimethylamine
ug/L
50
42.6
85
34-130
N-Nitrosodiphenylamine
ug/L
50
53.8
108
37-130
Naphthalene
ug/L
50
36.0
72
30-130
Nitrobenzene
ug/L
50
49.3
99
36-130
Pentachlorophenol
ug/L
100
84.8
85
23-149
Phenanthrene
ug/L
50
55.4
111
44-130
Phenol
ug/L
50
29.3
59
18-130
Pyrene
ug/L
50
59.3
119
47-134
2,4,6-Tribromophenol (S)
%
114
10-144
2-Fluorobiphenyl (S)
%
101
10-130
2-Fluorophenol (S)
%
80
10-130
Nitrobenzene-d5 (S)
%
110
10-144
Phenol-d6 (S)
%
62
10-130
Terphenyl-d14 (S)
%
111
34-163
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3442707
MS
92565649013 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3442708
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,2,4-Trichoorobenzene
ug/L
ND
50
50
25.5
32.3
51
65
10-130
24
30
1,2-Dichlorobenzene
ug/L
ND
50
50
26.2
32.3
52
65
10-130
21
30
1,3-Dichlorobenzene
ug/L
ND
50
50
26.1
30.4
52
61
10-130
15
30
1,4-Dichlorobenzene
ug/L
ND
50
50
25.9
32.2
52
64
10-130
22
30
1-Methyl naphthalene
ug/L
ND
50
50
34.9
41.9
70
84
10-130
18
30
2,2'-Oxybis(1-
ug/L
ND
50
50
33.6
38.5
67
77
12-142
13
30
chloropropane)
2,4,5-Trichlorophenol
ug/L
ND
50
50
44.1
50.8
88
102
10-143
14
30
2,4,6-Trichlorophenol
ug/L
ND
50
50
42.3
47.8
85
96
10-147
12
30
2,4-Dichlorophenol
ug/L
ND
50
50
38.5
43.7
77
87
10-138
13
30
2,4-Dimethylphenol
ug/L
ND
50
50
36.9
42.3
74
85
25-130
14
30
2,4-Dinitrophenol
ug/L
ND
250
250
81.0
81.0
32
32
10-165
0
30
2,4-Dinitrotoluene
ug/L
ND
50
50
51.5
56.9
103
114
29-148
10
30
2,6-Dinitrotoluene
ug/L
ND
50
50
48.5
55.1
97
110
26-146
13
30
2-Chloronaphthalene
ug/L
ND
50
50
36.3
41.9
73
84
11-130
14
30
2-Chlorophenol
ug/L
ND
50
50
43.9
43.5
88
87
10-133
1
30
2-Methyl naphthalene
ug/L
ND
50
50
35.1
41.1
70
82
13-130
16
30
2-Methyl phenol(o-Cresol)
ug/L
ND
50
50
33.9
39.4
68
79
20-130
15
30
2-Nitroaniline
ug/L
ND
100
100
81.2
90.6
81
91
24-136
11
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC.
Page 69 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3442707
MS
92565649013 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3442708
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
2-Nitrophenol
ug/L
ND
50
50
38.9
44.9
78
90
10-153
14
30 v1
3&4-Methylphenol(m&p
ug/L
ND
50
50
33.1
39.3
66
79
16-130
17
30
Cresol)
3,3'-Dichlorobenzidine
ug/L
ND
100
100
103
111
103
111
10-153
8
30 v1
3-Nitroaniline
ug/L
ND
100
100
97.5
108
97
108
22-151
11
30
4,6-Dinitro-2-methylphenol
ug/L
ND
100
100
75.1
80.0
75
80
10-180
6
30
4-Bromophenylphenyl ether
ug/L
ND
50
50
48.0
54.0
96
108
25-130
12
30
4-Chloro-3-methylphenol
ug/L
ND
100
100
83.5
97.3
84
97
25-133
15
30
4-Chloroaniline
ug/L
ND
100
100
74.5
84.7
75
85
14-132
13
30
4-Chlorophenylphenyl ether
ug/L
ND
50
50
58.3
47.4
117
95
19-130
21
30
4-Nitroaniline
ug/L
ND
100
100
142
113
142
113
29-150
23
30
4-Nitrophenol
ug/L
ND
250
250
125
131
50
52
10-130
4
30
Acenaphthene
ug/L
ND
50
50
41.8
47.0
84
94
16-130
12
30
Acenaphthylene
ug/L
ND
50
50
41.7
46.8
83
94
15-137
11
30
Aniline
ug/L
ND
50
50
38.4
35.2
77
70
10-130
9
30
Anthracene
ug/L
ND
50
50
50.5
55.5
101
111
37-136
9
30
Benzo(a)anth race ne
ug/L
ND
50
50
55.6
59.6
111
119
40-145
7
30
Benzo(a)pyrene
ug/L
ND
50
50
62.5
67.0
125
134
41-146
7
30
Benzo(b)fluoranthene
ug/L
ND
50
50
58.8
61.3
118
123
39-151
4
30
Benzo(g,h,i)perylene
ug/L
ND
50
50
60.4
65.8
121
132
40-147
8
30
Benzo(k)fluoranthene
ug/L
ND
50
50
59.1
65.4
118
131
40-146
10
30
Benzoic Acid
ug/L
ND
250
250
16.3J
16AJ
7
7
10-130
30 MO
Benzyl alcohol
ug/L
ND
100
100
73.3
85.8
73
86
25-130
16
30
bis(2-
ug/L
ND
50
50
38.2
43.5
76
87
23-130
13
30
Chloroethoxy)methane
bis(2-Chloroethyl) ether
ug/L
ND
50
50
52.2
45.9
104
92
25-130
13
30
bis(2- Ethyl hexyl)phthalate
ug/L
ND
50
50
63.8
68.2
128
136
28-166
7
30 v1
Butylbenzylphthalate
ug/L
ND
50
50
64.4
69.2
129
138
33-165
7
30 v1
Chrysene
ug/L
ND
50
50
54.2
57.7
108
115
38-141
6
30
Di-n-butylphthalate
ug/L
ND
50
50
56.7
61.6
113
123
32-153
8
30
Di-n-octylphthalate
ug/L
ND
50
50
59.9
64.5
120
129
30-175
7
30
Dibenz(a,h)anthracene
ug/L
ND
50
50
61.2
65.8
122
132
39-148
7
30
Dibenzofuran
ug/L
ND
50
50
41.9
47.7
84
95
20-130
13
30
Diethylphthalate
ug/L
ND
50
50
66.4
52.4
133
105
28-142
24
30
Dimethylphthalate
ug/L
ND
50
50
43.5
48.0
87
96
26-136
10
30
Fluoranthene
ug/L
ND
50
50
53.3
57.8
107
116
39-143
8
30
Fluorene
ug/L
ND
50
50
62.8
50.7
126
101
24-132
21
30
Hexachloro-1,3-butadiene
ug/L
ND
50
50
21.7
27.9
43
56
10-130
25
30
Hexachlorobenzene
ug/L
ND
50
50
45.0
49.0
90
98
29-130
8
30
Hexachlorocyclopentadiene
ug/L
ND
50
50
23.5
30.1
47
60
10-130
25
30
Hexachloroethane
ug/L
ND
50
50
24.1
29.4
48
59
10-130
20
30
Indeno(1,2,3-cd)pyrene
ug/L
ND
50
50
61.8
66.6
124
133
39-148
7
30
Isophorone
ug/L
ND
50
50
36.7
40.7
73
81
23-130
10
30
N-Nitroso-di-n-propylamine
ug/L
ND
50
50
38.8
45.8
78
92
25-130
16
30
N-Nitrosodimethylamine
ug/L
ND
50
50
37.7
41.3
75
83
22-130
9
30 v1
N-Nitrosodiphenylamine
ug/L
ND
50
50
48.0
53.6
96
107
26-134
11
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC.
Page 70 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 3442707
3442708
MS
MSD
92565649013
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Naphthalene
ug/L
ND
50
50
30.6
37.4
61
75
14-130
20
30
Nitrobenzene
ug/L
ND
50
50
37.5
41.5
75
83
25-130
10
30
Pentachlorophenol
ug/L
ND
100
100
87.5
95.7
87
96
10-175
9
30
Phenanthrene
ug/L
ND
50
50
49.7
53.9
99
108
36-133
8
30
Phenol
ug/L
ND
50
50
29.7
26.9
59
54
10-130
10
30
Pyrene
ug/L
ND
50
50
54.2
58.2
108
116
40-143
7
30
2,4,6-Tribromophenol (S)
%
122
137
10-144
2-Fluorobiphenyl (S)
%
74
87
10-130
2-Fluorophenol(S)
%
58
67
10-130
Nitrobenzene-d5(S)
%
79
89
10-144
Phenol-d6 (S)
%
54
51
10-130
Terphenyl-d14(S)
%
105
110
34-163
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC.
Page 71 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
QC Batch: 656955 Analysis Method: EPA 8270E
QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92569749005, 92569749006, 92569749007, 92569749008, 92569749009, 92569749010
METHOD BLANK: 3443687 Matrix: Solid
Associated Lab Samples: 92569749005, 92569749006, 92569749007, 92569749008, 92569749009, 92569749010
Blank Reporting
Parameter Units Result Limit MDL Analyzed
1,2,4-Trichlorobenzene
mg/kg
ND
0.33
0.13
11/03/21 09:17
1,2-Dichlorobenzene
mg/kg
ND
0.33
0.12
11/03/21 09:17
1,3-Dichlorobenzene
mg/kg
ND
0.33
0.12
11/03/21 09:17
1,4-Dichlorobenzene
mg/kg
ND
0.33
0.13
11/03/21 09:17
1-Methylnaphthalene
mg/kg
ND
0.33
0.12
11/03/21 09:17
2,2'-Oxybis(1-chloropropane)
mg/kg
ND
0.33
0.16
11/03/21 09:17
2,4,5-Trichlorophenol
mg/kg
ND
0.33
0.15
11/03/21 09:17
2,4,6-Trichlorophenol
mg/kg
ND
0.33
0.14
11/03/21 09:17
2,4-Dichlorophenol
mg/kg
ND
0.33
0.13
11/03/21 09:17
2,4-Dimethylphenol
mg/kg
ND
0.33
0.14
11/03/21 09:17
2,4-Dinitrophenol
mg/kg
ND
1.6
1.0
11/03/21 09:17
2,4-Dinitrotoluene
mg/kg
ND
0.33
0.13
11/03/21 09:17
2,6-Dinitrotoluene
mg/kg
ND
0.33
0.12
11/03/21 09:17
2-Chloronaphthalene
mg/kg
ND
0.33
0.13
11/03/21 09:17
2-Chlorophenol
mg/kg
ND
0.33
0.12
11/03/21 09:17
2-Methylnaphthalene
mg/kg
ND
0.33
0.13
11/03/21 09:17
2-Methylphenol(o-Cresol)
mg/kg
ND
0.33
0.14
11/03/21 09:17
2-Nitroaniline
mg/kg
ND
1.6
0.27
11/03/21 09:17
2-Nitrophenol
mg/kg
ND
0.33
0.14
11/03/21 09:17
3&4-Methyl phenol (m&p Cresol)
mg/kg
ND
0.33
0.13
11/03/21 09:17
3,3'-Dichlorobenzidine
mg/kg
ND
0.66
0.22
11/03/21 09:17
3-Nitroaniline
mg/kg
ND
1.6
0.26
11/03/21 09:17
4,6-Dinitro-2-methyl phenol
mg/kg
ND
0.66
0.31
11/03/21 09:17
4-Bromophenylphenyl ether
mg/kg
ND
0.33
0.13
11/03/21 09:17
4-ChIoro-3-methyl phenol
mg/kg
ND
0.66
0.23
11/03/21 09:17
4-Chloroaniline
mg/kg
ND
0.66
0.26
11/03/21 09:17
4-Chlorophenylphenyl ether
mg/kg
ND
0.33
0.12
11/03/21 09:17
4-Nitroaniline
mg/kg
ND
0.66
0.25
11/03/21 09:17
4-Nitrophenol
mg/kg
ND
1.6
0.64
11/03/21 09:17
Acenaphthene
mg/kg
ND
0.33
0.12
11/03/21 09:17
Acenaphthylene
mg/kg
ND
0.33
0.12
11/03/21 09:17
Aniline
mg/kg
ND
0.33
0.13
11/03/21 09:17
Anthracene
mg/kg
ND
0.33
0.11
11/03/21 09:17
Benzo(a)anthracene
mg/kg
ND
0.33
0.11
11/03/21 09:17
Benzo(a)pyrene
mg/kg
ND
0.33
0.11
11/03/21 09:17
Benzo(b)fluoranthene
mg/kg
ND
0.33
0.11
11/03/21 09:17
Benzo(g,h,i)perylene
mg/kg
ND
0.33
0.13
11/03/21 09:17
Benzo(k)fluoranthene
mg/kg
ND
0.33
0.12
11/03/21 09:17
Benzoic Acid
mg/kg
ND
1.6
0.71
11/03/21 09:17
Benzyl alcohol
mg/kg
ND
0.66
0.25
11/03/21 09:17
v1
IL
IL
IL
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 72 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
METHOD BLANK: 3443687 Matrix: Solid
Associated Lab Samples: 92569749005, 92569749006, 92569749007, 92569749008, 92569749009, 92569749010
Blank Reporting
Parameter Units Result Limit MDL Analyzed
bis(2-Chloroethoxy)methane
mg/kg
ND
0.33
0.14
11/03/21 09:17
bis(2-Chloroethyl) ether
mg/kg
ND
0.33
0.12
11/03/21 09:17
bis(2-Ethylhexyl)phthalate
mg/kg
ND
0.33
0.13
11/03/21 09:17
Butylbenzylphthalate
mg/kg
ND
0.33
0.14
11/03/21 09:17
Chrysene
mg/kg
ND
0.33
0.12
11/03/21 09:17
Di-n-butylphthalate
mg/kg
ND
0.33
0.11
11/03/21 09:17
Di-n-octylphthalate
mg/kg
ND
0.33
0.13
11/03/21 09:17
Dibenz(a,h)anthracene
mg/kg
ND
0.33
0.13
11/03/21 09:17
Dibenzofuran
mg/kg
ND
0.33
0.12
11/03/21 09:17
Diethylphthalate
mg/kg
ND
0.33
0.12
11/03/21 09:17
Dimethylphthalate
mg/kg
ND
0.33
0.12
11/03/21 09:17
Fluoranthene
mg/kg
ND
0.33
0.11
11/03/21 09:17
Fluorene
mg/kg
ND
0.33
0.12
11/03/21 09:17
Hexachloro-1,3-butadiene
mg/kg
ND
0.33
0.14
11/03/21 09:17
Hexachlorobenzene
mg/kg
ND
0.33
0.13
11/03/21 09:17
Hexachlorocyclopentadiene
mg/kg
ND
0.33
0.19
11/03/21 09:17
Hexachloroethane
mg/kg
ND
0.33
0.13
11/03/21 09:17
Indeno(1,2,3-cd)pyrene
mg/kg
ND
0.33
0.13
11/03/21 09:17
Isophorone
mg/kg
ND
0.33
0.15
11/03/21 09:17
N-Nitroso-di-n-propylamine
mg/kg
ND
0.33
0.12
11/03/21 09:17
N-Nitrosodimethylamine
mg/kg
ND
0.33
0.11
11/03/21 09:17
N-Nitrosodiphenylamine
mg/kg
ND
0.33
0.12
11/03/21 09:17
Naphthalene
mg/kg
ND
0.33
0.11
11/03/21 09:17
Nitrobenzene
mg/kg
ND
0.33
0.15
11/03/21 09:17
Pentachlorophenol
mg/kg
ND
0.66
0.32
11/03/21 09:17
Phenanthrene
mg/kg
ND
0.33
0.11
11/03/21 09:17
Phenol
mg/kg
ND
0.33
0.15
11/03/21 09:17
Pyrene
mg/kg
ND
0.33
0.13
11/03/21 09:17
Pyridine
mg/kg
ND
0.33
0.10
11/03/21 09:17
2,4,6-Tribromophenol (S)
%
74
18-130
11/03/21 09:17
2-Fluorobiphenyl (S)
%
66
19-130
11/03/21 09:17
2-Fluorophenol (S)
%
59
18-130
11/03/21 09:17
Nitrobenzene-d5 (S)
%
57
21-130
11/03/21 09:17
Phenol-d6 (S)
%
58
18-130
11/03/21 09:17
Terphenyl-d14 (S)
%
75
15-130
11/03/21 09:17
Qualifiers
LABORATORY CONTROL SAMPLE:
3443688
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
mg/kg
1.7
1.2
70
47-130
1,2-Dichlorobenzene
mg/kg
1.7
1.1
63
49-130
1,3-Dichlorobenzene
mg/kg
1.7
1.1
63
48-130
1,4-Dichlorobenzene
mg/kg
1.7
1.0
62
49-130
1-Methylnaphthalene
mg/kg
1.7
1.1
65
54-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 73 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
LABORATORY CONTROL SAMPLE:
Parameter
3443688
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,2'-Oxybis(1-chloropropane)
mg/kg
1.7
0.87
52
38-130
2,4,5-Trichlorophenol
mg/kg
1.7
1.3
79
49-130
2,4,6-Trichlorophenol
mg/kg
1.7
1.3
79
50-130
2,4-Dichlorophenol
mg/kg
1.7
1.2
70
51-130
2,4-Dimethylphenol
mg/kg
1.7
1.1
68
53-130
2,4-Dinitrophenol
mg/kg
8.3
6.5
78
39-130
2,4-Dinitrotoluene
mg/kg
1.7
1.3
77
53-130
2,6-Dinitrotoluene
mg/kg
1.7
1.4
85
55-130
2-Chloronaphthalene
mg/kg
1.7
1.3
75
48-130
2-Chlorophenol
mg/kg
1.7
1.1
63
54-130
2-Methylnaphthalene
mg/kg
1.7
1.1
66
57-130
2-Methylphenol(o-Cresol)
mg/kg
1.7
1.0
62
50-130
2-Nitroaniline
mg/kg
3.3
2.1
63
49-130
2-Nitrophenol
mg/kg
1.7
1.3
80
50-130 v1
3&4-Methyl phenol (m&p Cresol)
mg/kg
1.7
0.98
59
50-130
3,3'-Dichlorobenzidine
mg/kg
3.3
2.3
69
47-130IL
3-Nitroaniline
mg/kg
3.3
2.5
74
45-130IL
4,6-Dinitro-2-methyl phenol
mg/kg
3.3
2.4
72
50-142
4-Bromophenylphenyl ether
mg/kg
1.7
1.3
77
55-130
4-ChIoro-3-methyl phenol
mg/kg
3.3
2.1
62
52-130
4-Chloroaniline
mg/kg
3.3
2.2
66
49-130IL
4-Chlorophenylphenyl ether
mg/kg
1.7
1.3
77
53-130
4-Nitroaniline
mg/kg
3.3
2.3
69
51-130
4-Nitrophenol
mg/kg
8.3
5.6
67
40-130
Acenaphthene
mg/kg
1.7
1.3
75
56-130
Acenaphthylene
mg/kg
1.7
1.3
75
58-130
Aniline
mg/kg
1.7
0.88
53
44-130
Anthracene
mg/kg
1.7
1.1
66
60-130
Benzo(a)anthracene
mg/kg
1.7
1.2
73
59-130
Benzo(a)pyrene
mg/kg
1.7
1.3
79
57-130
Benzo(b)fluoranthene
mg/kg
1.7
1.4
83
54-130
Benzo(g,h,i)perylene
mg/kg
1.7
1.3
80
59-130
Benzo(k)fluoranthene
mg/kg
1.7
1.3
81
54-130
Benzoic Acid
mg/kg
8.3
4.9
59
19-130
Benzyl alcohol
mg/kg
3.3
1.9
57
50-130
bis(2-Chloroethoxy)methane
mg/kg
1.7
1.0
63
55-130
bis(2-Chloroethyl) ether
mg/kg
1.7
0.98
59
53-130
bis(2-Ethylhexyl)phthalate
mg/kg
1.7
1.1
67
58-130
Butylbenzylphthalate
mg/kg
1.7
1.3
76
46-138
Chrysene
mg/kg
1.7
1.2
73
57-130
Di-n-butylphthalate
mg/kg
1.7
1.1
64
57-130
Di-n-octylphthalate
mg/kg
1.7
1.2
69
57-130
Dibenz(a,h)anthracene
mg/kg
1.7
1.3
79
60-130
Dibenzofuran
mg/kg
1.7
1.3
77
54-130
Diethylphthalate
mg/kg
1.7
1.2
72
55-130
Dimethylphthalate
mg/kg
1.7
1.2
75
57-130
Fluoranthene
mg/kg
1.7
1.1
64
57-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 74 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
LABORATORY CONTROL SAMPLE:
3443688
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Fluorene
mg/kg
1.7
1.2
75
56-130
Hexachloro-1,3-butadiene
mg/kg
1.7
1.2
71
41-130
Hexachlorobenzene
mg/kg
1.7
1.3
77
53-130
Hexachlorocyclopentadiene
mg/kg
1.7
1.3
81
23-130
Hexachloroethane
mg/kg
1.7
1.0
61
48-130
Indeno(1,2,3-cd)pyrene
mg/kg
1.7
1.3
80
61-130
Isophorone
mg/kg
1.7
0.95
57
49-130
N-Nitroso-di-n-propylamine
mg/kg
1.7
0.93
56
52-130
N-Nitrosodimethylamine
mg/kg
1.7
1.0
61
45-130
N-Nitrosodiphenylamine
mg/kg
1.7
1.1
68
56-130
Naphthalene
mg/kg
1.7
1.1
67
56-130
Nitrobenzene
mg/kg
1.7
1.0
60
50-130
Pentachlorophenol
mg/kg
3.3
2.6
78
33-130
Phenanthrene
mg/kg
1.7
1.1
67
60-130
Phenol
mg/kg
1.7
1.1
64
54-130
Pyrene
mg/kg
1.7
1.2
75
61-130
Pyridine
mg/kg
1.7
0.81
48
35-130
2,4,6-Tribromophenol (S)
%
82
18-130
2-Fluorobiphenyl (S)
%
72
19-130
2-Fluorophenol(S)
%
61
18-130
Nitrobenzene-d5 (S)
%
59
21-130
Phenol-d6 (S)
%
60
18-130
Terphenyl-d14 (S)
%
68
15-130
MATRIX SPIKE SAMPLE:
3443689
92559369008
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
mg/kg
ND
1.7
0.88
53
22-130
1,2-Dichlorobenzene
mg/kg
ND
1.7
0.80
48
23-130
1,3-Dichlorobenzene
mg/kg
ND
1.7
0.81
49
26-130
1,4-Dichlorobenzene
mg/kg
ND
1.7
0.81
48
27-130
1-Methylnaphthalene
mg/kg
ND
1.7
0.81
49
30-130
2,2'-Oxybis(1-chloropropane)
mg/kg
ND
1.7
0.68
41
30-130
2,4,5-Trichlorophenol
mg/kg
ND
1.7
0.99
59
26-130
2,4,6-Trichlorophenol
mg/kg
ND
1.7
0.97
58
23-130
2,4-Dichlorophenol
mg/kg
ND
1.7
0.85
51
29-130
2,4-Dimethylphenol
mg/kg
ND
1.7
0.83
50
13-130
2,4-Dinitrophenol
mg/kg
ND
8.3
5.3
64
10-131
2,4-Dinitrotoluene
mg/kg
ND
1.7
0.96
58
28-130
2,6-Dinitrotoluene
mg/kg
ND
1.7
1.1
65
36-130
2-Chloronaphthalene
mg/kg
ND
1.7
0.92
55
27-130
2-Chlorophenol
mg/kg
ND
1.7
0.81
48
29-130
2-Methylnaphthalene
mg/kg
ND
1.7
0.82
49
29-130
2-Methylphenol(o-Cresol)
mg/kg
ND
1.7
0.81
48
20-130
2-Nitroaniline
mg/kg
ND
3.3
1.6J
48
29-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 75 of 87

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
MATRIX SPIKE SAMPLE:
3443689
92559369008
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
2-Nitrophenol
mg/kg
ND
1.7
1.0
61
26-130 v1
3&4-Methyl phenol (m&p Cresol)
mg/kg
ND
1.7
0.81
49
10-176
3,3'-Dichlorobenzidine
mg/kg
ND
3.3
1.7
50
15-130IL
3-Nitroaniline
mg/kg
ND
3.3
1.9
57
28-130IL
4,6-Dinitro-2-methyl phenol
mg/kg
ND
3.3
2.0
60
15-132
4-Bromophenylphenyl ether
mg/kg
ND
1.7
0.95
57
35-130
4-Chloro-3-methylphenol
mg/kg
ND
3.3
1.6
47
30-130
4-Chloroaniline
mg/kg
ND
3.3
1.6
49
28-130IL
4-Chlorophenylphenyl ether
mg/kg
ND
1.7
0.93
56
32-130
4-Nitroaniline
mg/kg
ND
3.3
1.8
55
30-130
4-Nitrophenol
mg/kg
ND
8.3
4.2
50
17-130
Acenaphthene
mg/kg
ND
1.7
0.92
55
29-130
Acenaphthylene
mg/kg
ND
1.7
0.92
55
31-130
Aniline
mg/kg
ND
1.7
0.64
38
10-130
Anthracene
mg/kg
ND
1.7
0.82
49
33-130
Benzo(a)anthracene
mg/kg
ND
1.7
0.89
54
32-130
Benzo(a)pyrene
mg/kg
ND
1.7
0.98
59
32-130
Benzo(b)fluoranthene
mg/kg
ND
1.7
1.0
61
33-130
Benzo(g,h,i)perylene
mg/kg
ND
1.7
0.99
59
28-130
Benzo(k)fluoranthene
mg/kg
ND
1.7
1.0
60
31-130
Benzoic Acid
mg/kg
ND
8.3
1.4J
17
10-130
Benzyl alcohol
mg/kg
ND
3.3
1.4
42
31-130
bis(2-Chloroethoxy)methane
mg/kg
ND
1.7
0.80
48
30-130
bis(2-Chloroethyl) ether
mg/kg
ND
1.7
0.76
45
68-130 M1
bis(2-Ethylhexyl)phthalate
mg/kg
ND
1.7
0.82
49
40-130
Butylbenzylphthalate
mg/kg
ND
1.7
0.90
54
40-130
Chrysene
mg/kg
ND
1.7
0.90
54
30-130
Di-n-butylphthalate
mg/kg
ND
1.7
0.79
47
41-130
Di-n-octylphthalate
mg/kg
ND
1.7
0.83
50
42-130
Dibenz(a,h)anthracene
mg/kg
ND
1.7
0.95
57
27-130
Dibenzofuran
mg/kg
ND
1.7
0.93
56
32-130
Diethylphthalate
mg/kg
ND
1.7
0.92
55
40-130
Dimethylphthalate
mg/kg
ND
1.7
0.97
58
37-130
Fluoranthene
mg/kg
ND
1.7
0.80
48
26-130
Fluorene
mg/kg
ND
1.7
0.89
53
31-130
Hexachloro-1,3-butadiene
mg/kg
ND
1.7
0.90
54
20-130
Hexachlorobenzene
mg/kg
ND
1.7
0.96
57
29-130
Hexachlorocyclopentadiene
mg/kg
ND
1.7
0.98
59
10-130
Hexachloroethane
mg/kg
ND
1.7
0.78
47
21-130
Indeno(1,2,3-cd)pyrene
mg/kg
ND
1.7
0.96
58
28-130
Isophorone
mg/kg
ND
1.7
0.73
44
32-130
N-Nitroso-di-n-propylamine
mg/kg
ND
1.7
0.70
42
31-130
N-Nitrosodimethylamine
mg/kg
ND
1.7
0.80
48
20-130
N-Nitrosodiphenylamine
mg/kg
ND
1.7
0.85
51
32-130
Naphthalene
mg/kg
ND
1.7
0.85
51
30-130
Nitrobenzene
mg/kg
ND
1.7
0.77
46
25-130
Pentachlorophenol
mg/kg
ND
3.3
1.9
57
10-130
Results presented on this page are in the units indicated
by the "Units" column except where
an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 76 of 87

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[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
MATRIX SPIKE SAMPLE:
Parameter
3443689
Units
92559369008
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Phenanthrene
mg/kg
ND
1.7
0.84
50
34-130
Phenol
mg/kg
ND
1.7
0.79
48
14-130
Pyrene
mg/kg
ND
1.7
0.93
56
31-130
Pyridine
mg/kg
ND
1.7
0.60
36
10-130
2,4,6-Tribromophenol (S)
%
62
18-130
2-Fluorobiphenyl (S)
%
51
19-130
2-Fluorophenol (S)
%
46
18-130
Nitrobenzene-d5 (S)
%
46
21-130
Phenol-d6 (S)
%
45
18-130
Terphenyl-d14 (S)
%
50
15-130
SAMPLE DUPLICATE: 3443690
Parameter
Units
92559369009
Result
Dup
Result RPD
Max
RPD Qualifiers
1,2,4-Trichlorobenzene
mg/kg
ND
ND
30
1,2-Dichlorobenzene
mg/kg
ND
ND
30
1,3-Dichlorobenzene
mg/kg
ND
ND
30
1,4-Dichlorobenzene
mg/kg
ND
ND
30
1-Methylnaphthalene
mg/kg
ND
ND
30
2,2'-Oxybis(1-chloropropane)
mg/kg
ND
ND
30
2,4,5-Trichlorophenol
mg/kg
ND
ND
30
2,4,6-Trichlorophenol
mg/kg
ND
ND
30
2,4-Dichlorophenol
mg/kg
ND
ND
30
2,4-Dimethylphenol
mg/kg
ND
ND
30
2,4-Dinitrophenol
mg/kg
ND
ND
30
2,4-Dinitrotoluene
mg/kg
ND
ND
30
2,6-Dinitrotoluene
mg/kg
ND
ND
30
2-Chloronaphthalene
mg/kg
ND
ND
30
2-Chlorophenol
mg/kg
ND
ND
30
2-Methylnaphthalene
mg/kg
ND
ND
30
2-Methylphenol(o-Cresol)
mg/kg
ND
ND
30
2-Nitroaniline
mg/kg
ND
ND
30
2-Nitrophenol
mg/kg
ND
ND
30 v1
3&4-Methyl phenol (m&p Cresol)
mg/kg
ND
ND
30
3,3'-Dichlorobenzidine
mg/kg
ND
ND
30 IL
3-Nitroaniline
mg/kg
ND
ND
30 IL
4,6-Dinitro-2-methyl phenol
mg/kg
ND
ND
30
4-Bromophenylphenyl ether
mg/kg
ND
ND
30
4-ChIoro-3-methyl phenol
mg/kg
ND
ND
30
4-Chloroaniline
mg/kg
ND
ND
30 IL
4-Chlorophenylphenyl ether
mg/kg
ND
ND
30
4-Nitroaniline
mg/kg
ND
ND
30
4-Nitrophenol
mg/kg
ND
ND
30
Acenaphthene
mg/kg
ND
ND
30
Acenaphthylene
mg/kg
ND
ND
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Carson & Tryon
Pace Project No.: 92569749
SAMPLE DUPLICATE: 3443690
Parameter
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Ethylhexyl)phthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenz(a,h)anthracene
Dibenzofuran
Diethylphthalate
Dimethylphthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
N-Nitroso-di-n-propylamine
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol(S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
QUALITY CONTROL DATA
Units
92559369009 Dup
Result Result
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
mg/kg
ND
47
34
40
%
39
%
38
42
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
62
44
51
49
48
52
Max
RPD RPD
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC.
Page 78 of 87

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
QC Batch: 656666 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92569749005, 92569749006, 92569749007, 92569749008, 92569749009, 92569749010
SAMPLE DUPLICATE: 3442313
92569601027
Dup
Max
Parameter
Units
Result
Result
RPD RPD Qualifiers
Percent Moisture
%
14.6
15.4
5 25 N2
SAMPLE DUPLICATE: 3442314
92569749010
Dup
Max
Parameter
Units
Result
Result
RPD RPD Qualifiers
Percent Moisture
%
18.3
19.4
5 25 N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
QC Batch: 1768099 Analysis Method: SM 2540G
QC Batch Method: SM 2540 G Analysis Description: Total Solids 2540 G-2011
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92569749005, 92569749006, 92569749007, 92569749008, 92569749009, 92569749010
METHOD BLANK: R3725908-1 Matrix: Solid
Associated Lab Samples: 92569749005, 92569749006, 92569749007, 92569749008, 92569749009, 92569749010
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Total Solids % 0.00100 11/04/21 10:36
LABORATORY CONTROL SAMPLE: R3725908-2
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Solids % 50.0 49.9 99.9 85.0-115
SAMPLE DUPLICATE: R3725908-3
L1425517-01 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Solids % 89.7 89.9 0.248 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC.
Page 80 of 87

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Carson & Tryon
Pace Project No.: 92569749
QC Batch: 1769259 Analysis Method: EPA 7199
QC Batch Method: 3060A Analysis Description: Wet Chemistry 7199
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92569749005, 92569749006, 92569749007, 92569749008, 92569749009, 92569749010
METHOD BLANK: R3727885-1 Matrix: Solid
Associated Lab Samples: 92569749005, 92569749006, 92569749007, 92569749008, 92569749009, 92569749010
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Chromium, Hexavalent mg/kg ND 1.00 0.255 11/09/21 17:25
LABORATORY CONTROL SAMPLE:
R3727885-2
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Chromium, Hexavalent
mg/kg
10.0
11.3
113
80.0-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3727885-4
R3727885-5
MS
MSD
L1425499-01
Spike
Spike MS
MSD
MS MSD % Rec Max
Parameter Units
Result
Conc.
Conc. Result
Result
% Rec % Rec Limits RPD RPD Qual
Chromium, Hexavalent mg/kg
ND
20.0
20.0 19.6
18.8
98.2 94.0 75.0-125 4.37 20
SAMPLE DUPLICATE: R3727885-3
L1425489-10 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Chromium, Hexavalent mg/kg 0.664 0.592J 11.5 20 J
SAMPLE DUPLICATE: R3727885-8
92569749009 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Chromium, Hexavalent mg/kg 0.936 1.05 11.2 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2021 09:47 AM without the written consent of Pace Analytical Services, LLC. Page 81 of 87

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: Carson & Tryon
Pace Project No.: 92569749
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.
J Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
REPORT OF LABORATORY ANALYSIS
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Carson & Tryon
92569749
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92569749005
SB-1
EPA 3050B
656810
EPA 6010D
656976
92569749006
SB-2
EPA 3050B
656810
EPA 6010D
656976
92569749007
SB-3
EPA 3050B
656810
EPA 6010D
656976
92569749008
SB-4
EPA 3050B
656810
EPA 6010D
656976
92569749009
SB-5
EPA 3050B
656810
EPA 6010D
656976
92569749010
SB-6
EPA 3050B
656810
EPA 6010D
656976
92569749005
SB-1
EPA 7471 B
657137
EPA 7471 B
657516
92569749006
SB-2
EPA 7471 B
657137
EPA 7471 B
657516
92569749007
SB-3
EPA 7471B
657137
EPA 7471B
657516
92569749008
SB-4
EPA 7471 B
657137
EPA 7471 B
657516
92569749009
SB-5
EPA 7471B
657137
EPA 7471B
657516
92569749010
SB-6
EPA 7471B
657137
EPA 7471B
657516
92569749001
GW-1
EPA 3510C
656743
EPA 8270E
656911
92569749002
GW-2
EPA 3510C
656743
EPA 8270E
656911
92569749003
GW-3
EPA 3510C
656743
EPA 8270E
656911
92569749004
GW-4
EPA 3510C
656743
EPA 8270E
656911
92569749005
SBA
EPA 3546
656955
EPA 8270E
657088
92569749006
SB-2
EPA 3546
656955
EPA 8270E
657088
92569749007
SB-3
EPA 3546
656955
EPA 8270E
657088
92569749008
SB-4
EPA 3546
656955
EPA 8270E
657088
92569749009
SB-5
EPA 3546
656955
EPA 8270E
657088
92569749010
SB-6
EPA 3546
656955
EPA 8270E
657088
92569749005
SB-1
EPA 5035A/5030B
656847
EPA 8260D
656891
92569749006
SB-2
EPA 5035A/5030B
656847
EPA 8260D
656891
92569749007
SB-3
EPA 5035A/5030B
656847
EPA 8260D
656891
92569749008
SB-4
EPA 5035A/5030B
656847
EPA 8260D
656891
92569749009
SB-5
EPA 5035A/5030B
656847
EPA 8260D
656891
92569749010
SB-6
EPA 5035A/5030B
656847
EPA 8260D
656891
92569749001
GW-1
EPA 8260D
656871
92569749002
GW-2
EPA 8260D
656871
92569749003
GW-3
EPA 8260D
656871
92569749004
GW-4
EPA 8260D
656871
92569749005
SB-1
SW-846
656666
92569749006
SB-2
SW-846
656666
92569749007
SB-3
SW-846
656666
92569749008
SB-4
SW-846
656666
92569749009
SB-5
SW-846
656666
92569749010
SB-6
SW-846
656666
92569749005
SBA
SM 2540 G
1768099
SM 2540G
1768099
92569749006
SB-2
SM 2540 G
1768099
SM 2540G
1768099
92569749007
SB-3
SM 2540 G
1768099
SM 2540G
1768099
92569749008
SB-4
SM 2540 G
1768099
SM 2540G
1768099
92569749009
SB-5
SM 2540 G
1768099
SM 2540G
1768099
92569749010
SB-6
SM 2540 G
1768099
SM 2540G
1768099
92569749005
SB-1
3060A
1769259
EPA 7199
1769259
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 11 /11 /2021
09:47 AM
without the written consent of Pace Analytical Services, LLC.
Page 83 of 87

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Carson & Tryon
Pace Project No.: 92569749
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92569749006
SB-2
3060A
1769259
EPA 7199
1769259
92569749007
SB-3
3060A
1769259
EPA 7199
1769259
92569749008
SB-4
3060A
1769259
EPA 7199
1769259
92569749009
SB-5
3060A
1769259
EPA 7199
1769259
92569749010
SB-6
3060A
1769259
EPA 7199
1769259
Date: 11 /11 /2021 09:47 AM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 84 of 87

Document Name:
Document Revised: October 28, 2020
_. aCBARr3lICaI'
Sample Condition Upon Recei t(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.07
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville r/Raleigh❑ Mechanicsville[] Atlanta❑ Kernersville❑
Sample Condition Client Name: %% _ .. f Project riWO# ' 92569749 IIjj II j
Courier: []Fed Ex ❑UPS ❑U5P5 []Client
❑ Commercial [36ce ❑Other: jjll II I I !!
�Custody Seal Present? ❑Yes ❑ 1f l/O Seals Intact? ❑Yes w o 92569749 r 1
Date/Initials Person Examining Contents:
Packing Material: ❑Bubble Wrap Bubble Bags —]None ❑ Other Biological Tlssue rozen?l
Thermometer; [:]Yes❑Na EN/A
❑Wet [—]Blue ❑Nave
ype o ce:
Correction Factor:
Cooler Temp: Add/Subtract (°C) J Temp should be above freezing to 6•C
[]Samples out of temp criteria. Samples an ice, cooling process
Cooler Temp Corrected has begun
USDA Regulated Soil ( E N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Internationally,
myPc FINe nrl—Una Hawaii and Giiartn Mrnl) 11vac f-1N,.
Comments/Discrepancy:
Chain of Custody Present?
6es
❑No
❑NIA
1.
Sam les Arrived within Hold Time?
[Yes
❑No
❑N/A
2.
Short Hold Time Analysis 02 hr.)?
Yes
EINo
El N/A
3.
Rush Turn Around Time Requested?
[]Yes
60
❑N/A
4.
Sufficient Volume?
Yes
Na
CINIA
S,
Correct Containers Used?
-Pace Containers Used?
04es
[6Yes
Ono
❑No
❑N/A
❑N/A
6.
Containers Intact?
Eves
❑No
❑N/A
7.
Dissolved anaty5is: Samples Field Filtered?
❑Yes
QNo
[:jW1A
B.
Sample Labels Match COC7
•Includes Date/Time/ID/Analysis Matrix:
(Drees
i- # /S L
❑No
❑N/A
4.
Headspace in VOA Vials (>5-6mm)?
QYes
E No
NIA
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
[]Yes
❑Ye
2No
❑No
❑N/A
[ 0)A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
PeFson
Project Manager SCURF Review:
Project Manager SRF Review:
Date:
Date:
Field Data Required? ❑Yes ❑No
Page 85 of 87

Document Name:
Document Revised: October 28, 2020
e
aeeArialytical
Sample Condition Upon Receipt(SCUR)
Page 2 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.07
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Col'sform, TOC, oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottles
Project t# WO# : 92569749
PM: AMB Due Date: 11/08/21
CLIENT: 92—ECS
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pH Adjustment Log for Preserved Samples
Sample 10
Type of Preservative
PH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot N
Note: —Wheneverthere-is-a- disc repan cy-affecting'Narth-Carol ina-compliance-samples,—amcopy-of-this-form.will-he-sent-to-the-Nor-th-Carolina-0EH NR-6ert incauon.office-li.a,
Out of hald, incorrect preservative, out of temp, incorrect containers.
Page 86 of 87

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Page 87 of 87

APPENDIX C

con -test®
A Pace Analytical Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
November 10, 2021
Chris Orrell
ECS Southeast - Charlotte, NC
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Project Location: Carson & Tryon
Client Job Number:
Project Number: 10606-D
Laboratory Work Order Number: 21K0213
Enclosed are results of analyses for samples as received by the laboratory on November 1, 2021. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
QA Officer
Katherine Allen
Laboratory Manager
Daren Damboragian
Page 1 of 26

con -test®
A Pace Analytical Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
ECS Southeast - Charlotte, NC REPORT DATE: 11/10/2021
1812 Center Park Drive, Suite D
Charlotte, NC 28217 PURCHASE ORDER NUMBER:
ATTN: Chris Orrell
PROJECT NUMBER: 10606-D
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 21K0213
The results of analyses performed on the following samples submitted to Con -Test, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION: Carson & Tryon
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
SG-1
21K0213-01
Soil Gas
EPATO-15
SG-2
21K0213-02
Soil Gas
EPATO-15
SG-3
21K0213-03
Soil Gas
EPATO-15
SG4
21K0213-04
Soil Gas
EPA TO-15
Page 2 of 26

con -test®
A Pace Analytical Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
EPA TO-15
Qualifications:
Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this compound is likely to be
biased on the low side.
Analyte & Samples(s) Qualified:
Ethyl Acetate, Hexachlorobutadiene, Methyl tert-Butyl Ether (MTBE)
21K0213-01[SG-1], 21K0213-02[SG-2], 21K0213-03[SG-3], 21K0213-04[SG-4], B294400-BLKI, B294400-BSI
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method
specified criteria. Reported result is estimated.
Analyte & Samples(s) Qualified:
1,2,4-Trichlorobenzene
21K0213-01[SG-1], 21K0213-02[SG-2], 21K0213-03[SG-3], 21K0213-04[SG-4], B294400-BLKI, B294400-BSI, S065181-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
Hexachlorobutadiene, Vinyl Acetate
21K0213-01[SG-1], 21K0213-02[SG-2], 21K0213-03[SG-3], 21K0213-04[SG-4], B294400-BLKI, B294400-BSI, S065181-CCVI
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
Ethyl Acetate
21K0213-01[SG-1], 21K0213-02[SG-2], 21K0213-03[SG-3], 21K0213-04[SG-4], B294400-BLKI, B294400-BSI, S065181-CCVI
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data validation is not affected since
sample result was 'hot detected" for this compound.
Analyte & Samples(s) Qualified:
Vinyl Acetate
B294400-BS1, 5065181-CCVI
Page 3 of 26

con -test®
A Pace Analytical Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
The results of analyses reported only relate to samples submitted to Con -Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Tod E. Kopyscinski
Laboratory Director
Page 4 of 26

con -test®
A Pace Analytical Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
ANALYTICAL RESULTS
Project Location: Carson & Tryon
Date Received: 11/1/2021
Field Sample #: SG-1
Sample ID: 21KO213-01
Sample Matrix: Soil Gas
Sampled: 10/29/2021 12:12
Sample Description/Location:
Sub Description/Location:
Canister ID: 2408
Canister Size: 3 liter
Flow Controller ID: 4344
Sample Type: 30 min
Work Order: 21KO213
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7.4
Flow Controller Type: Fixed -Orifice
Flow Controller Calibration
RPD Pre and Post -Sampling:
EPA TO-15
ppbv
ug/m3
Date/Time
Analyte
Results
RL
MDL
Flag/Qual
Results
RL
MDL
Dilution
Analyzed
Analyst
Acetone
ND
8.0
4.8
ND
19
11
4
11/10/21
8:18
BRF
Benzene
6.5
0.20
0.048
21
0.64
0.15
4
11/10/21
8:18
BRF
Benzyl chloride
ND
0.20
0.090
ND
1.0
0.47
4
11/10/21
8:18
BRF
Bromodichloromethane
ND
0.20
0.073
ND
1.3
0.49
4
11/10/21
8:18
BRF
Bromoform
ND
0.20
0.072
ND
2.1
0.74
4
11/10/21
8:18
BRF
Bromomethane
ND
0.20
0.16
ND
0.78
0.63
4
11/10/21
8:18
BRF
1,3-Butadiene
ND
0.20
0.14
ND
0.44
0.31
4
11/10/21
8:18
BRF
2-Butanone (MEK)
15
8.0
0.66
45
24
2.0
4
11/10/21
8:18
BRF
Carbon Disulfide
11
2.0
0.51
33
6.2
1.6
4
11/10/21
8:18
BRF
Carbon Tetrachloride
ND
0.20
0.060
ND
1.3
0.38
4
11/10/21
8:18
BRF
Chlorobenzene
ND
0.20
0.060
ND
0.92
0.27
4
11/10/21
8:18
BRF
Chloroethane
ND
0.20
0.15
ND
0.53
0.39
4
11/10/21
8:18
BRF
Chloroform
ND
0.20
0.048
ND
0.98
0.24
4
11/10/21
8:18
BRF
Chloromethane
ND
0.40
0.082
ND
0.83
0.17
4
11/10/21
8:18
BRF
Cyclohexane
5.8
0.20
0.13
20
0.69
0.46
4
11/10/21
8:18
BRF
Dibromochloromethane
ND
0.20
0.067
ND
1.7
0.57
4
11/10/21
8:18
BRF
1,2-Dibromoethane (EDB)
ND
0.20
0.056
ND
1.5
0.43
4
11/10/21
8:18
BRF
1,2-Dichlorobenzene
ND
0.20
0.074
ND
1.2
0.44
4
11/10/21
8:18
BRF
1,3-Dichlorobenzene
ND
0.20
0.048
ND
1.2
0.29
4
11/10/21
8:18
BRF
1,4-Dichlorobenzene
ND
0.20
0.081
ND
1.2
0.49
4
11/10/21
8:18
BRF
Dichlorodifluoromethane (Freon 12)
0.48
0.20
0.061
2.4
0.99
0.30
4
11/10/21
8:18
BRF
1, 1 -Dichloroethane
ND
0.20
0.067
ND
0.81
0.27
4
11/10/21
8:18
BRF
1,2-Dichloroethane
ND
0.20
0.073
ND
0.81
0.30
4
11/10/21
8:18
BRF
1, 1 -Dichloroethylene
ND
0.20
0.079
ND
0.79
0.31
4
11/10/21
8:18
BRF
cis-1,2-Dichloroethylene
0.12
0.20
0.068
J
0.46
0.79
0.27
4
11/10/21
8:18
BRF
trans-1,2-Dichloroethylene
ND
0.20
0.070
ND
0.79
0.28
4
11/10/21
8:18
BRF
1,2-Dichloropropane
ND
0.20
0.072
ND
0.92
0.33
4
11/10/21
8:18
BRF
cis- 1,3 -Dichloropropene
ND
0.20
0.093
ND
0.91
0.42
4
11/10/21
8:18
BRF
trans- 1, 3 -Dichloropropene
ND
0.20
0.062
ND
0.91
0.28
4
11/10/21
8:18
BRF
1,2-Dichloro- 1, 1,2,2-tetrafluoroethane (Freon 114)
ND
0.20
0.069
ND
1.4
0.48
4
11/10/21
8:18
BRF
1,4-Dioxane
ND
2.0
0.14
ND
7.2
0.49
4
11/10/21
8:18
BRF
Ethanol
59
8.0
2.4
110
15
4.6
4
11/10/21
8:18
BRF
Ethyl Acetate
ND
2.0
1.2
L-03,V-34
ND
7.2
4.3
4
11/10/21
8:18
BRF
Ethylbenzene
0.43
0.20
0.052
1.9
0.87
0.22
4
11/10/21
8:18
BRF
4-Ethyltoluene
ND
0.20
0.062
ND
0.98
0.30
4
11/10/21
8:18
BRF
Heptane
3.1
0.20
0.082
13
0.82
0.34
4
11/10/21
8:18
BRF
Hexachlorobutadiene
ND
0.20
0.11
V-05, L-03
ND
2.1
1.2
4
11/10/21
8:18
BRF
Hexane
11
8.0
0.66
40
28
2.3
4
11/10/21
8:18
BRF
2-Hexanone(MBK)
ND
0.40
0.10
ND
1.6
0.41
4
11/10/21
8:18
BRF
Isopropanol
3.2
8.0
1.8
J
8.0
20
4.5
4
11/10/21
8:18
BRF
Methyl tert-Butyl Ether (MTBE)
ND
0.20
0.080
L-03
ND
0.72
0.29
4
11/10/21
8:18
BRF
Methylene Chloride
ND
2.0
0.46
ND
6.9
1.6
4
11/10/21
8:18
BRF
4-Methyl-2-pentanone (MIBK)
ND
0.20
0.10
ND
0.82
0.42
4
11/10/21
8:18
BRF
Naphthalene
ND
0.20
0.13
ND
1.0
0.66
4
11/10/21
8:18
BRF
Propene
57
8.0
0.67
99
14
1.2
4
11/10/21
8:18
BRF
Styrene
3.1
0.20
0.063
13
0.85
0.27
4
11/10/21
8:18
BRF
1,1,2,2-Tetrachloroethane
ND
0.20
0.061
ND
1.4
0.42
4
11/10/21
8:18
BRF
Page 5 of 26

con -test®
A Pace Analytical Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
ANALYTICAL RESULTS
Project Location: Carson & Tryon
Sample Description/Location:
Work Order: 21KO213
Date Received: 11/1/2021
Sub Description/Location:
Initial Vacuum(in Hg): -29
Field Sample #: SG-1
Canister ID: 2408
Final Vacuum(in Hg): -5
Sample ID: 21KO213-01
Canister Size: 3 liter
Receipt Vacuum(in Hg): -7.4
Sample Matrix: Soil Gas
Flow Controller ID: 4344
Flow Controller Type: Fixed -Orifice
Sampled: 10/29/2021 12:12
Sample Type: 30 min
Flow Controller Calibration
RPD Pre and Post -Sampling:
Analyte
Results
ppbv
RL
EPA TO-15
MDL
Flag/Qual
Results
ug/m3
RL
MDL
Dilution
Date/Time
Analyzed
Analyst
Tetrachloroethylene
0.072
0.20
0.059
J
0.49
1.4
0.40
4
11/10/21
8:18
BRF
Tetrahydrofuran
1.2
2.0
0.49
J
3.4
5.9
1.5
4
11/10/21
8:18
BRF
Toluene
2.5
0.20
0.084
9.6
0.75
0.32
4
11/10/21
8:18
BRF
1,2,4-Trichlorobenzene
ND
0.40
0.14
V-04
ND
3.0
1.0
4
11/10/21
8:18
BRF
1, 1, 1 -Trichloroethane
ND
0.20
0.092
ND
1.1
0.50
4
11/10/21
8:18
BRF
1,1,2-Trichloroethane
ND
0.20
0.080
ND
1.1
0.43
4
11/10/21
8:18
BRF
Trichloroethylene
0.20
0.20
0.074
1.1
1.1
0.40
4
11/10/21
8:18
BRF
Trichlorofluoromethane (Freon 11)
0.080
0.80
0.080
J
0.45
4.5
0.45
4
11/10/21
8:18
BRF
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
ND
0.80
0.071
ND
6.1
0.54
4
11/10/21
8:18
BRF
1,2,4-Trimethylbenzene
0.22
0.20
0.059
1.1
0.98
0.29
4
11/10/21
8:18
BRF
1,3,5-Trimethylbenzene
0.080
0.20
0.055
J
0.39
0.98
0.27
4
11/10/21
8:18
BRF
Vinyl Acetate
ND
4.0
0.37
V-05
ND
14
1.3
4
11/10/21
8:18
BRF
Vinyl Chloride
ND
0.20
0.079
ND
0.51
0.20
4
11/10/21
8:18
BRF
m&p-Xylene
1.2
0.40
0.11
5.1
1.7
0.48
4
11/10/21
8:18
BRF
o-Xylene
0.62
0.20
0.054
2.7
0.87
0.23
4
11/10/21
8:18
BRF
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1) 89.0 70-130 11/10/21 8:18
Page 6 of 26

con -test®
A Pace Analytical Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
ANALYTICAL RESULTS
Project Location: Carson & Tryon
Sample Description/Location:
Work Order: 21KO213
Date Received: 11/1/2021
Sub Description/Location:
Initial Vacuum(in Hg): -28
Field Sample #: SG-2
Canister ID: 2431
Final Vacuum(in Hg): -5
Sample ID: 21KO213-02
Canister Size: 3 liter
Receipt Vacuum(in Hg): -8.2
Sample Matrix: Soil Gas
Flow Controller ID: 4350
Flow Controller Type: Fixed -Orifice
Sampled: 10/29/2021 13:00
Sample Type: 30 min
Flow Controller Calibration
RPD Pre and Post -Sampling:
Analyte
Results
ppbv
RL
EPA TO-15
MDL
Flag/Qual
Results
ug/m3
RL
MDL
Dilution
Date/Time
Analyzed
Analyst
Acetone
10
8.0
4.8
24
19
11
4
11/10/21
8:43
BRF
Benzene
0.62
0.20
0.048
2.0
0.64
0.15
4
11/10/21
8:43
BRF
Benzyl chloride
ND
0.20
0.090
ND
1.0
0.47
4
11/10/21
8:43
BRF
Bromodichloromethane
ND
0.20
0.073
ND
1.3
0.49
4
11/10/21
8:43
BRF
Bromoform
ND
0.20
0.072
ND
2.1
0.74
4
11/10/21
8:43
BRF
Bromomethane
ND
0.20
0.16
ND
0.78
0.63
4
11/10/21
8:43
BRF
1,3-Butadiene
ND
0.20
0.14
ND
0.44
0.31
4
11/10/21
8:43
BRF
2-Butanone (MEK)
1.3
8.0
0.66
J
3.7
24
2.0
4
11/10/21
8:43
BRF
Carbon Disulfide
ND
2.0
0.51
ND
6.2
1.6
4
11/10/21
8:43
BRF
Carbon Tetrachloride
0.092
0.20
0.060
J
0.58
1.3
0.38
4
11/10/21
8:43
BRF
Chlorobenzene
ND
0.20
0.060
ND
0.92
0.27
4
11/10/21
8:43
BRF
Chloroethane
ND
0.20
0.15
ND
0.53
0.39
4
11/10/21
8:43
BRF
Chloroform
ND
0.20
0.048
ND
0.98
0.24
4
11/10/21
8:43
BRF
Chloromethane
0.73
0.40
0.082
1.5
0.83
0.17
4
11/10/21
8:43
BRF
Cyclohexane
2.1
0.20
0.13
7.1
0.69
0.46
4
11/10/21
8:43
BRF
Dibromochloromethane
ND
0.20
0.067
ND
1.7
0.57
4
11/10/21
8:43
BRF
1,2-Dibromoethane (EDB)
ND
0.20
0.056
ND
1.5
0.43
4
11/10/21
8:43
BRF
1,2-Dichlorobenzene
ND
0.20
0.074
ND
1.2
0.44
4
11/10/21
8:43
BRF
1,3-Dichlorobenzene
ND
0.20
0.048
ND
1.2
0.29
4
11/10/21
8:43
BRF
1,4-Dichlorobenzene
ND
0.20
0.081
ND
1.2
0.49
4
11/10/21
8:43
BRF
Dichlorodifluoromethane (Freon 12)
0.46
0.20
0.061
2.3
0.99
0.30
4
11/10/21
8:43
BRF
1,1-Dichloroethane
ND
0.20
0.067
ND
0.81
0.27
4
11/10/21
8:43
BRF
1,2-Dichloroethane
ND
0.20
0.073
ND
0.81
0.30
4
11/10/21
8:43
BRF
1,1-Dichloroethylene
ND
0.20
0.079
ND
0.79
0.31
4
11/10/21
8:43
BRF
cis-1,2-Dichloroethylene
ND
0.20
0.068
ND
0.79
0.27
4
11/10/21
8:43
BRF
trans-1,2-Dichloroethylene
ND
0.20
0.070
ND
0.79
0.28
4
11/10/21
8:43
BRF
1,2-Dichloropropane
ND
0.20
0.072
ND
0.92
0.33
4
11/10/21
8:43
BRF
cis- 1,3 -Dichloropropene
ND
0.20
0.093
ND
0.91
0.42
4
11/10/21
8:43
BRF
trans- 1, 3 -Dichloropropene
ND
0.20
0.062
ND
0.91
0.28
4
11/10/21
8:43
BRF
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
ND
0.20
0.069
ND
1.4
0.48
4
11/10/21
8:43
BRF
1,4-Dioxane
ND
2.0
0.14
ND
7.2
0.49
4
11/10/21
8:43
BRF
Ethanol
23
8.0
2.4
43
15
4.6
4
11/10/21
8:43
BRF
Ethyl Acetate
ND
2.0
1.2
L-03, V-34
ND
7.2
4.3
4
11/10/21
8:43
BRF
Ethylbenzene
0.14
0.20
0.052
J
0.61
0.87
0.22
4
11/10/21
8:43
BRF
4-Ethyltoluene
ND
0.20
0.062
ND
0.98
0.30
4
11/10/21
8:43
BRF
Heptane
0.58
0.20
0.082
2.4
0.82
0.34
4
11/10/21
8:43
BRF
Hexachlorobutadiene
ND
0.20
0.11
L-03, V-05
ND
2.1
1.2
4
11/10/21
8:43
BRF
Hexane
1.3
8.0
0.66
J
4.6
28
2.3
4
11/10/21
8:43
BRF
2-Hexanone (MBK)
ND
0.40
0.10
ND
1.6
0.41
4
11/10/21
8:43
BRF
Isopropanol
ND
8.0
1.8
ND
20
4.5
4
11/10/21
8:43
BRF
Methyl tert-Butyl Ether (MTBE)
ND
0.20
0.080
L-03
ND
0.72
0.29
4
11/10/21
8:43
BRF
Methylene Chloride
ND
2.0
0.46
ND
6.9
1.6
4
11/10/21
8:43
BRF
4-Methyl-2-pentanone (MIBK)
ND
0.20
0.10
ND
0.82
0.42
4
11/10/21
8:43
BRF
Naphthalene
ND
0.20
0.13
ND
1.0
0.66
4
11/10/21
8:43
BRF
Propene
21
8.0
0.67
37
14
1.2
4
11/10/21
8:43
BRF
Styrene
0.84
0.20
0.063
3.6
0.85
0.27
4
11/10/21
8:43
BRF
1,1,2,2-Tetrachloroethane
ND
0.20
0.061
ND
1.4
0.42
4
11/10/21
8:43
BRF
Page 7 of 26

con -test®
A Pace Analytical Laboratory
Project Location: Carson & Tryon
Date Received: 11/1/2021
Field Sample #: SG-2
Sample ID: 21KO213-02
Sample Matrix: Soil Gas
Sampled: 10/29/2021 13:00
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
ANALYTICAL RESULTS
Sample Description/Location:
Sub Description/Location:
Canister ID: 2431
Canister Size: 3 liter
Flow Controller ID: 4350
Sample Type: 30 min
Work Order: 21KO213
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -8.2
Flow Controller Type: Fixed -Orifice
Flow Controller Calibration
RPD Pre and Post -Sampling:
EPA TO-15
ppbv ug/m3 Date/Time
Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst
Tetrachloroethylene
ND
0.20
0.059
ND
1.4
0.40
Tetrahydrofuran
ND
2.0
0.49
ND
5.9
1.5
Toluene
1.1
0.20
0.084
4.3
0.75
0.32
1,2,4-Trichlorobenzene
ND
0.40
0.14
V-04
ND
3.0
1.0
1, 1, 1 -Trichloroethane
ND
0.20
0.092
ND
1.1
0.50
1,1,2-Trichloroethane
ND
0.20
0.080
ND
1.1
0.43
Trichloroethylene
ND
0.20
0.074
ND
1.1
0.40
Trichlorofluoromethane (Freon 11)
0.24
0.80
0.080
J
1.3
4.5
0.45
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
0.11
0.80
0.071
J
0.83
6.1
0.54
1,2,4-Trimethylbenzene
ND
0.20
0.059
ND
0.98
0.29
1,3,5-Trimethylbenzene
ND
0.20
0.055
ND
0.98
0.27
Vinyl Acetate
ND
4.0
0.37
V-05
ND
14
1.3
Vinyl Chloride
ND
0.20
0.079
ND
0.51
0.20
m&p-Xylene
0.40
0.40
0.11
1.7
1.7
0.48
o-Xylene
0.16
0.20
0.054
J
0.69
0.87
0.23
Surrogates
4-Bromofluorobenzene (1)
% Recovery
88.6
% REC Limits
70-130
4 11/10/21
8:43
BRF
4 11/10/21
8:43
BRF
4 11/10/21
8:43
BRF
4 11/10/21
8:43
BRF
4 11/10/21
8:43
BRF
4 11/10/21
8:43
BRF
4 11/10/21
8:43
BRF
4 11/10/21
8:43
BRF
4 11/10/21
8:43
BRF
4 11/10/21
8:43
BRF
4 11/10/21
8:43
BRF
4 11/10/21
8:43
BRF
4 11/10/21
8:43
BRF
4 11/10/21
8:43
BRF
4 11/10/21
8:43
BRF
11/10/21 8:43
Page 8 of 26

con -test®
A Pace Analytical Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
ANALYTICAL RESULTS
Project Location: Carson & Tryon
Sample Description/Location:
Work Order: 21KO213
Date Received: 11/1/2021
Sub Description/Location:
Initial Vacuum(in Hg): -28
Field Sample #: SG-3
Canister ID: 2401
Final Vacuum(in Hg): -5
Sample ID: 21KO213-03
Canister Size: 3 liter
Receipt Vacuum(in Hg): -7.5
Sample Matrix: Soil Gas
Flow Controller ID: 4224
Flow Controller Type: Fixed -Orifice
Sampled: 10/29/2021 13:40
Sample Type: 30 min
Flow Controller Calibration
RPD Pre and Post -Sampling:
Analyte
Results
ppbv
RL
EPA TO-15
MDL
Flag/Qual
Results
ug/m3
RL
MDL
Dilution
Date/Time
Analyzed
Analyst
Acetone
9.2
8.0
4.8
22
19
11
4
11/10/21
9:07
BRF
Benzene
9.6
0.20
0.048
31
0.64
0.15
4
11/10/21
9:07
BRF
Benzyl chloride
ND
0.20
0.090
ND
1.0
0.47
4
11/10/21
9:07
BRF
Bromodichloromethane
ND
0.20
0.073
ND
1.3
0.49
4
11/10/21
9:07
BRF
Bromoform
ND
0.20
0.072
ND
2.1
0.74
4
11/10/21
9:07
BRF
Bromomethane
ND
0.20
0.16
ND
0.78
0.63
4
11/10/21
9:07
BRF
1,3-Butadiene
ND
0.20
0.14
ND
0.44
0.31
4
11/10/21
9:07
BRF
2-Butanone (MEK)
1.1
8.0
0.66
J
3.3
24
2.0
4
11/10/21
9:07
BRF
Carbon Disulfide
9.3
2.0
0.51
29
6.2
1.6
4
11/10/21
9:07
BRF
Carbon Tetrachloride
0.25
0.20
0.060
1.6
1.3
0.38
4
11/10/21
9:07
BRF
Chlorobenzene
ND
0.20
0.060
ND
0.92
0.27
4
11/10/21
9:07
BRF
Chloroethane
1.1
0.20
0.15
2.9
0.53
0.39
4
11/10/21
9:07
BRF
Chloroform
0.50
0.20
0.048
2.5
0.98
0.24
4
11/10/21
9:07
BRF
Chloromethane
1.8
0.40
0.082
3.6
0.83
0.17
4
11/10/21
9:07
BRF
Cyclohexane
2.4
0.20
0.13
8.4
0.69
0.46
4
11/10/21
9:07
BRF
Dibromochloromethane
ND
0.20
0.067
ND
1.7
0.57
4
11/10/21
9:07
BRF
1,2-Dibromoethane (EDB)
ND
0.20
0.056
ND
1.5
0.43
4
11/10/21
9:07
BRF
1,2-Dichlorobenzene
ND
0.20
0.074
ND
1.2
0.44
4
11/10/21
9:07
BRF
1,3-Dichlorobenzene
ND
0.20
0.048
ND
1.2
0.29
4
11/10/21
9:07
BRF
1,4-Dichlorobenzene
ND
0.20
0.081
ND
1.2
0.49
4
11/10/21
9:07
BRF
Dichlorodifluoromethane (Freon 12)
0.42
0.20
0.061
2.1
0.99
0.30
4
11/10/21
9:07
BRF
1,1-Dichloroethane
ND
0.20
0.067
ND
0.81
0.27
4
11/10/21
9:07
BRF
1,2-Dichloroethane
ND
0.20
0.073
ND
0.81
0.30
4
11/10/21
9:07
BRF
1,1-Dichloroethylene
ND
0.20
0.079
ND
0.79
0.31
4
11/10/21
9:07
BRF
cis-1,2-Dichloroethylene
ND
0.20
0.068
ND
0.79
0.27
4
11/10/21
9:07
BRF
trans-1,2-Dichloroethylene
ND
0.20
0.070
ND
0.79
0.28
4
11/10/21
9:07
BRF
1,2-Dichloropropane
ND
0.20
0.072
ND
0.92
0.33
4
11/10/21
9:07
BRF
cis- 1,3 -Dichloropropene
ND
0.20
0.093
ND
0.91
0.42
4
11/10/21
9:07
BRF
trans- 1, 3 -Dichloropropene
ND
0.20
0.062
ND
0.91
0.28
4
11/10/21
9:07
BRF
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
ND
0.20
0.069
ND
1.4
0.48
4
11/10/21
9:07
BRF
1,4-Dioxane
ND
2.0
0.14
ND
7.2
0.49
4
11/10/21
9:07
BRF
Ethanol
36
8.0
2.4
67
15
4.6
4
11/10/21
9:07
BRF
Ethyl Acetate
ND
2.0
1.2
L-03, V-34
ND
7.2
4.3
4
11/10/21
9:07
BRF
Ethylbenzene
1.3
0.20
0.052
5.7
0.87
0.22
4
11/10/21
9:07
BRF
4-Ethyltoluene
0.18
0.20
0.062
J
0.90
0.98
0.30
4
11/10/21
9:07
BRF
Heptane
6.0
0.20
0.082
24
0.82
0.34
4
11/10/21
9:07
BRF
Hexachlorobutadiene
ND
0.20
0.11
L-03, V-05
ND
2.1
1.2
4
11/10/21
9:07
BRF
Hexane
6.9
8.0
0.66
J
24
28
2.3
4
11/10/21
9:07
BRF
2-Hexanone (MBK)
ND
0.40
0.10
ND
1.6
0.41
4
11/10/21
9:07
BRF
Isopropanol
ND
8.0
1.8
ND
20
4.5
4
11/10/21
9:07
BRF
Methyl tert-Butyl Ether (MTBE)
ND
0.20
0.080
L-03
ND
0.72
0.29
4
11/10/21
9:07
BRF
Methylene Chloride
0.63
2.0
0.46
J
2.2
6.9
1.6
4
11/10/21
9:07
BRF
4-Methyl-2-pentanone (MIBK)
ND
0.20
0.10
ND
0.82
0.42
4
11/10/21
9:07
BRF
Naphthalene
ND
0.20
0.13
ND
1.0
0.66
4
11/10/21
9:07
BRF
Propene
40
8.0
0.67
69
14
1.2
4
11/10/21
9:07
BRF
Styrene
6.6
0.20
0.063
28
0.85
0.27
4
11/10/21
9:07
BRF
1,1,2,2-Tetrachloroethane
ND
0.20
0.061
ND
1.4
0.42
4
11/10/21
9:07
BRF
Page 9 of 26

con -test®
A Pace Analytical Laboratory
Project Location: Carson & Tryon
Date Received: 11/1/2021
Field Sample #: SG-3
Sample ID: 21KO213-03
Sample Matrix: Soil Gas
Sampled: 10/29/2021 13:40
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
ANALYTICAL RESULTS
Sample Description/Location:
Sub Description/Location:
Canister ID: 2401
Canister Size: 3 liter
Flow Controller ID: 4224
Sample Type: 30 min
Work Order: 21KO213
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7.5
Flow Controller Type: Fixed -Orifice
Flow Controller Calibration
RPD Pre and Post -Sampling:
EPA TO-15
ppbv ug/m3 Date/Time
Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst
Tetrachloroethylene
0.19
0.20
0.059
J
1.3
1.4
0.40
4
11/10/21
9:07
BRF
Tetrahydrofuran
ND
2.0
0.49
ND
5.9
1.5
4
11/10/21
9:07
BRF
Toluene
16
0.20
0.084
62
0.75
0.32
4
11/10/21
9:07
BRF
1,2,4-Trichlorobenzene
ND
0.40
0.14
V-04
ND
3.0
1.0
4
11/10/21
9:07
BRF
1, 1, 1 -Trichloroethane
ND
0.20
0.092
ND
1.1
0.50
4
11/10/21
9:07
BRF
1,1,2-Trichloroethane
ND
0.20
0.080
ND
1.1
0.43
4
11/10/21
9:07
BRF
Trichloroethylene
ND
0.20
0.074
ND
1.1
0.40
4
11/10/21
9:07
BRF
Trichlorofluoromethane (Freon 11)
0.28
0.80
0.080
J
1.6
4.5
0.45
4
11/10/21
9:07
BRF
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
0.17
0.80
0.071
J
1.3
6.1
0.54
4
11/10/21
9:07
BRF
1,2,4-Trimethylbenzene
ND
0.20
0.059
ND
0.98
0.29
4
11/10/21
9:07
BRF
1,3,5-Trimethylbenzene
0.23
0.20
0.055
1.1
0.98
0.27
4
11/10/21
9:07
BRF
Vinyl Acetate
ND
4.0
0.37
V-05
ND
14
1.3
4
11/10/21
9:07
BRF
Vinyl Chloride
0.71
0.20
0.079
1.8
0.51
0.20
4
11/10/21
9:07
BRF
m&p-Xylene
3.7
0.40
0.11
16
1.7
0.48
4
11/10/21
9:07
BRF
o-Xylene
1.2
0.20
0.054
5.3
0.87
0.23
4
11/10/21
9:07
BRF
Surrogates
4-Bromofluorobenzene (1)
% Recovery
90.7
% REC Limits
70-130
11/10/21 9:07
Page 10 of 26

con -test®
A Pace Analytical Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
ANALYTICAL RESULTS
Project Location: Carson & Tryon
Sample Description/Location:
Work Order: 21KO213
Date Received: 11/1/2021
Sub Description/Location:
Initial Vacuum(in Hg): -28
Field Sample #: SG-4
Canister ID: 2367
Final Vacuum(in Hg): -5
Sample ID: 21KO213-04
Canister Size: 3 liter
Receipt Vacuum(in Hg): -7.4
Sample Matrix: Soil Gas
Flow Controller ID: 4225
Flow Controller Type: Fixed -Orifice
Sampled: 10/29/2021 13:47
Sample Type: 30 min
Flow Controller Calibration
RPD Pre and Post -Sampling:
Analyte
Results
ppbv
RL
EPA TO-15
MDL
Flag/Qual
Results
ug/m3
RL
MDL
Dilution
Date/Time
Analyzed
Analyst
Acetone
10
8.0
4.8
24
19
11
4
11/10/21
9:32
BRF
Benzene
5.7
0.20
0.048
18
0.64
0.15
4
11/10/21
9:32
BRF
Benzyl chloride
ND
0.20
0.090
ND
1.0
0.47
4
11/10/21
9:32
BRF
Bromodichloromethane
ND
0.20
0.073
ND
1.3
0.49
4
11/10/21
9:32
BRF
Bromoform
ND
0.20
0.072
ND
2.1
0.74
4
11/10/21
9:32
BRF
Bromomethane
ND
0.20
0.16
ND
0.78
0.63
4
11/10/21
9:32
BRF
1,3-Butadiene
2.0
0.20
0.14
4.4
0.44
0.31
4
11/10/21
9:32
BRF
2-Butanone (MEK)
1.3
8.0
0.66
J
3.8
24
2.0
4
11/10/21
9:32
BRF
Carbon Disulfide
1.3
2.0
0.51
J
4.1
6.2
1.6
4
11/10/21
9:32
BRF
Carbon Tetrachloride
0.072
0.20
0.060
J
0.45
1.3
0.38
4
11/10/21
9:32
BRF
Chlorobenzene
ND
0.20
0.060
ND
0.92
0.27
4
11/10/21
9:32
BRF
Chloroethane
ND
0.20
0.15
ND
0.53
0.39
4
11/10/21
9:32
BRF
Chloroform
0.78
0.20
0.048
3.8
0.98
0.24
4
11/10/21
9:32
BRF
Chloromethane
0.39
0.40
0.082
J
0.81
0.83
0.17
4
11/10/21
9:32
BRF
Cyclohexane
4.7
0.20
0.13
16
0.69
0.46
4
11/10/21
9:32
BRF
Dibromochloromethane
ND
0.20
0.067
ND
1.7
0.57
4
11/10/21
9:32
BRF
1,2-Dibromoethane (EDB)
ND
0.20
0.056
ND
1.5
0.43
4
11/10/21
9:32
BRF
1,2-Dichlorobenzene
ND
0.20
0.074
ND
1.2
0.44
4
11/10/21
9:32
BRF
1,3-Dichlorobenzene
ND
0.20
0.048
ND
1.2
0.29
4
11/10/21
9:32
BRF
1,4-Dichlorobenzene
ND
0.20
0.081
ND
1.2
0.49
4
11/10/21
9:32
BRF
Dichlorodifluoromethane (Freon 12)
0.44
0.20
0.061
2.2
0.99
0.30
4
11/10/21
9:32
BRF
1,1-Dichloroethane
ND
0.20
0.067
ND
0.81
0.27
4
11/10/21
9:32
BRF
1,2-Dichloroethane
0.36
0.20
0.073
1.4
0.81
0.30
4
11/10/21
9:32
BRF
1,1-Dichloroethylene
ND
0.20
0.079
ND
0.79
0.31
4
11/10/21
9:32
BRF
cis-1,2-Dichloroethylene
ND
0.20
0.068
ND
0.79
0.27
4
11/10/21
9:32
BRF
trans-1,2-Dichloroethylene
ND
0.20
0.070
ND
0.79
0.28
4
11/10/21
9:32
BRF
1,2-Dichloropropane
ND
0.20
0.072
ND
0.92
0.33
4
11/10/21
9:32
BRF
cis- 1,3 -Dichloropropene
ND
0.20
0.093
ND
0.91
0.42
4
11/10/21
9:32
BRF
trans- 1, 3 -Dichloropropene
ND
0.20
0.062
ND
0.91
0.28
4
11/10/21
9:32
BRF
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
ND
0.20
0.069
ND
1.4
0.48
4
11/10/21
9:32
BRF
1,4-Dioxane
ND
2.0
0.14
ND
7.2
0.49
4
11/10/21
9:32
BRF
Ethanol
33
8.0
2.4
62
15
4.6
4
11/10/21
9:32
BRF
Ethyl Acetate
ND
2.0
1.2
L-03, V-34
ND
7.2
4.3
4
11/10/21
9:32
BRF
Ethylbenzene
0.67
0.20
0.052
2.9
0.87
0.22
4
11/10/21
9:32
BRF
4-Ethyltoluene
0.092
0.20
0.062
J
0.45
0.98
0.30
4
11/10/21
9:32
BRF
Heptane
5.0
0.20
0.082
21
0.82
0.34
4
11/10/21
9:32
BRF
Hexachlorobutadiene
ND
0.20
0.11
L-03, V-05
ND
2.1
1.2
4
11/10/21
9:32
BRF
Hexane
7.6
8.0
0.66
J
27
28
2.3
4
11/10/21
9:32
BRF
2-Hexanone (MBK)
ND
0.40
0.10
ND
1.6
0.41
4
11/10/21
9:32
BRF
Isopropanol
ND
8.0
1.8
ND
20
4.5
4
11/10/21
9:32
BRF
Methyl tert-Butyl Ether (MTBE)
ND
0.20
0.080
L-03
ND
0.72
0.29
4
11/10/21
9:32
BRF
Methylene Chloride
ND
2.0
0.46
ND
6.9
1.6
4
11/10/21
9:32
BRF
4-Methyl-2-pentanone (MIBK)
ND
0.20
0.10
ND
0.82
0.42
4
11/10/21
9:32
BRF
Naphthalene
ND
0.20
0.13
ND
1.0
0.66
4
11/10/21
9:32
BRF
Propene
3.5
8.0
0.67
J
6.1
14
1.2
4
11/10/21
9:32
BRF
Styrene
2.6
0.20
0.063
11
0.85
0.27
4
11/10/21
9:32
BRF
1,1,2,2-Tetrachloroethane
ND
0.20
0.061
ND
1.4
0.42
4
11/10/21
9:32
BRF
Page 11 of 26

con -test®
A Pace Analytical Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
ANALYTICAL RESULTS
Project Location: Carson & Tryon
Sample Description/Location:
Work Order: 21KO213
Date Received: 11/1/2021
Sub Description/Location:
Initial Vacuum(in Hg): -28
Field Sample #: SG-4
Canister ID: 2367
Final Vacuum(in Hg): -5
Sample ID: 21KO213-04
Canister Size: 3 liter
Receipt Vacuum(in Hg): -7.4
Sample Matrix: Soil Gas
Flow Controller ID: 4225
Flow Controller Type: Fixed -Orifice
Sampled: 10/29/2021 13:47
Sample Type: 30 min
Flow Controller Calibration
RPD Pre and Post -Sampling:
Analyte
Results
ppbv
RL
EPA TO-15
MDL
Flag/Qual
Results
ug/m3
RL
MDL
Dilution
Date/Time
Analyzed
Analyst
Tetrachloroethylene
1.2
0.20
0.059
7.9
1.4
0.40
4
11/10/21
9:32
BRF
Tetrahydrofuran
ND
2.0
0.49
ND
5.9
1.5
4
11/10/21
9:32
BRF
Toluene
11
0.20
0.084
42
0.75
0.32
4
11/10/21
9:32
BRF
1,2,4-Trichlorobenzene
ND
0.40
0.14
V-04
ND
3.0
1.0
4
11/10/21
9:32
BRF
1, 1, 1 -Trichloroethane
ND
0.20
0.092
ND
1.1
0.50
4
11/10/21
9:32
BRF
1,1,2-Trichloroethane
ND
0.20
0.080
ND
1.1
0.43
4
11/10/21
9:32
BRF
Trichloroethylene
ND
0.20
0.074
ND
1.1
0.40
4
11/10/21
9:32
BRF
Trichlorofluoromethane (Freon 11)
0.36
0.80
0.080
J
2.0
4.5
0.45
4
11/10/21
9:32
BRF
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
0.096
0.80
0.071
J
0.74
6.1
0.54
4
11/10/21
9:32
BRF
1,2,4-Trimethylbenzene
0.28
0.20
0.059
1.4
0.98
0.29
4
11/10/21
9:32
BRF
1,3,5-Trimethylbenzene
0.18
0.20
0.055
J
0.88
0.98
0.27
4
11/10/21
9:32
BRF
Vinyl Acetate
ND
4.0
0.37
V-05
ND
14
1.3
4
11/10/21
9:32
BRF
Vinyl Chloride
ND
0.20
0.079
ND
0.51
0.20
4
11/10/21
9:32
BRF
m&p-Xylene
2.6
0.40
0.11
11
1.7
0.48
4
11/10/21
9:32
BRF
o-Xylene
0.84
0.20
0.054
3.6
0.87
0.23
4
11/10/21
9:32
BRF
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1) 89.8 70-130 11/10/21 9:32
Page 12 of 26

con -test®
A Pace Analytical Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Sample Extraction Data
Prep Method: TO-15 Prep -EPA TO-15
Pre-Dil
Pre-Dil
Default
Actual
Pressure
Pre
Initial
Final
Injection
Injection
Lab Number [Field ID]
Batch
Dilution
Dilution
mL
mL
mL
mL
Date
21K0213-01 [SG-1]
B294400
1.5
1
N/A
1000
200
75
11/09/21
21K0213-02 [SG-2]
B294400
1.5
1
N/A
1000
200
75
11/09/21
21K0213-03 [SG-3]
B294400
1.5
1
N/A
1000
200
75
11/09/21
21K0213-04 [SG-4]
B294400
1.5
1
N/A
1000
200
75
11/09/21
Page 13 of 26

con -test®
A Pace Analytical Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
QUALITY CONTROL
Air Toxics by EPA Compendium Methods - Quality Control
ppbv ug/m3 Spike Level Source %REC RPD
nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua
Batch B294400 - TO-15 Prep
Blank (B294400-BLKl)
Prepared & Analyzed: 11/09/21
Acetone
ND
0.80
Benzene
0.013
0.020
J
Benzyl chloride
ND
0.020
Bromodichloromethane
ND
0.020
Bromoform
ND
0.020
Bromomethane
ND
0.020
113-Butadiene
ND
0.020
2-Butanone (MEK)
ND
0.80
Carbon Disulfide
ND
0.20
Carbon Tetrachloride
ND
0.020
Chlorobenzene
ND
0.020
Chloroethane
ND
0.020
Chloroform
ND
0.020
Chloromethane
ND
0.040
Cyclohexane
ND
0.020
Dibromochloromethane
ND
0.020
1,2-Dibromoethane (EDB)
ND
0.020
1,2-Dichlorobenzene
ND
0.020
1,3-Dichlorobenzene
ND
0.020
114-Dichlorobenzene
ND
0.020
Dichlorodifluoromethane (Freon 12)
ND
0.020
I,I-Dichloroethane
ND
0.020
1,2-Dichloroethane
ND
0.020
1,1-Dichloroethylene
ND
0.020
cis-1,2-Dichloroethylene
ND
0.020
trans-1,2-Dichloroethylene
ND
0.020
1,2-Dichloropropane
ND
0.020
cis- 1,3 -Dichloropropene
ND
0.020
trans- l,3-Dichloropropene
ND
0.020
1,2-Dichloro- 1, 1,2,2-tetrafluoroethane
ND
0.020
(Freon 114)
114-Dioxane
ND
0.20
Ethanol
ND
0.80
Ethyl Acetate
ND
0.20
L-03, V-34
Ethylbenzene
0.0064
0.020
J
4-Ethyltoluene
ND
0.020
Heptane
ND
0.020
Hexachlorobutadiene
ND
0.020
L-03, V-05
Hexane
ND
0.80
2-Hexanone (MBK)
ND
0.020
Isopropanol
ND
0.80
Methyl tert-Butyl Ether (MTBE)
ND
0.020
L-03
Methylene Chloride
ND
0.20
4-Methyl-2-pentanone (MIBK)
ND
0.020
Naphthalene
ND
0.020
Propene
ND
0.80
Styrene
ND
0.020
Page 14 of 26

con -test®
A Pace Analytical Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
QUALITY CONTROL
Air Toxics by EPA Compendium Methods - Quality Control
ppbv ug/m3 Spike Level Source %REC RPD
\nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua]
Batch B294400 - TO-15 Prep
Blank (B294400-BLKI)
Prepared & Analyzed: 11/09/21
1,1,2,2-Tetrachloroethane
ND
0.020
Tetrachloroethylene
ND
0.020
Tetrahydrofuran
ND
0.20
Toluene
ND
0.020
1,2,4-Trichlorobenzene
ND
0.020 V-04
1, 1, 1 -Trichloroethane
ND
0.020
1,1,2-Trichloroethane
ND
0.020
Trichloroethylene
ND
0.020
Trichlorofluoromethane (Freon 11)
ND
0.080
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
ND
0.080
113)
1,2,4-Trimethylbenzene
ND
0.020
1,3,5-Trimethylbenzene
ND
0.020
Vinyl Acetate
ND
0.40 V-0'-
Vinyl Chloride
ND
0.020
m&p-Xylene
ND
0.040
o-Xylene
ND
0.020
Surrogate: 4-Bromofluorobenzene (1)
LCS (B294400-BSI)
7.17
8.00 89.6
Prepared & Analyzed: 11/09/21
70-130
Acetone
4.24
5.00
84.8
70-130
Benzene
5.67
5.00
113
70-130
Benzyl chloride
5.30
5.00
106
70-130
Bromodichloromethane
5.25
5.00
105
70-130
Bromoform
4.69
5.00
93.7
70-130
Bromomethane
4.43
5.00
88.6
70-130
1,3-Butadiene
4.74
5.00
94.7
70-130
2-Butanone (MEK)
4.21
5.00
84.1
70-130
Carbon Disulfide
5.09
5.00
102
70-130
Carbon Tetrachloride
4.48
5.00
89.7
70-130
Chlorobenzene
4.84
5.00
96.7
70-130
Chloroethane
5.04
5.00
101
70-130
Chloroform
4.15
5.00
82.9
70-130
Chloromethane
4.94
5.00
98.8
70-130
Cyclohexane
4.69
5.00
93.7
70-130
Dibromochloromethane
4.82
5.00
96.5
70-130
1,2-Dibromoethane (EDB)
5.01
5.00
100
70-130
1,2-Dichlorobenzene
4.63
5.00
92.6
70-130
1,3-Dichlorobenzene
5.12
5.00
102
70-130
1,4-Dichlorobenzene
4.70
5.00
93.9
70-130
Dichlorodifluoromethane (Freon 12)
4.20
5.00
83.9
70-130
1,1-Dichloroethane
4.40
5.00
88.0
70-130
1,2-Dichloroethane
3.95
5.00
79.1
70-130
1, 1 -Dichloroethylene
5.04
5.00
101
70-130
cis-1,2-Dichloroethylene
4.20
5.00
84.1
70-130
trans-1,2-Dichloroethylene
4.17
5.00
83.4
70-130
1,2-Dichloropropane
5.40
5.00
108
70-130
Page 15 of 26

con -test®
A Pace Analytical Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
QUALITY CONTROL
Air Toxics by EPA Compendium Methods - Quality Control
ppbv ug/m3 Spike Level Source %REC RPD
\nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua]
Batch B294400 - TO-15 Prep
LCS (B294400-BS1)
Prepared & Analyzed: 11/09/21
cis-1,3-Dichloropropene
5.16
5.00
103
70-130
trans-1,3-Dichloropropene
5.24
5.00
105
70-130
1,2-Dichloro- 1, 1,2,2-tetrafluoroethane
4.36
5.00
87.2
70-130
(Freon 114)
1,4-Dioxane
4.78
5.00
95.5
70-130
Ethanol
5.99
5.00
120
70-130
Ethyl Acetate
2.92
5.00
58.3
* 70-130
L-03,V-34
Ethylbenzene
4.79
5.00
95.8
70-130
4-Ethyltoluene
4.66
5.00
93.2
70-130
Heptane
5.42
5.00
108
70-130
Hexachlorobutadiene
3.10
5.00
62.1
* 70-130
L-03, V-05
Hexane
4.30
5.00
86.0
70-130
2-Hexanone (MBK)
5.95
5.00
119
70-130
Isopropanol
3.76
5.00
75.2
70-130
Methyl tert-Butyl Ether (MTBE)
3.44
5.00
68.8
* 70-130
L-03
Methylene Chloride
5.10
5.00
102
70-130
4-Methyl-2-pentanone (MIBK)
5.65
5.00
113
70-130
Naphthalene
3.76
5.00
75.1
70-130
Propene
3.88
5.00
77.6
70-130
Styrene
4.86
5.00
97.3
70-130
1,1,2,2-Tetrachloroethane
5.74
5.00
115
70-130
Tetrachloroethylene
4.20
5.00
83.9
70-130
Tetrahydrofuran
3.80
5.00
76.0
70-130
Toluene
4.84
5.00
96.7
70-130
1,2,4-Trichlorobenzene
3.52
5.00
70.3
70-130
V-04
1, 1, 1 -Trichloroethane
4.46
5.00
89.2
70-130
1,1,2-Trichloroethane
5.20
5.00
104
70-130
Trichloroethylene
4.84
5.00
96.7
70-130
Trichlorofluoromethane (Freon 11)
4.42
5.00
88.4
70-130
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
4.84
5.00
96.8
70-130
113)
1,2,4-Trimethylbenzene
4.41
5.00
88.2
70-130
1,3,5-Trimethylbenzene
4.74
5.00
94.7
70-130
Vinyl Acetate
5.62
5.00
112
70-130
V-05,
V-36
Vinyl Chloride 5.19 5.00 104 70-130
m&p-Xylene 10.2 10.0 102 70-130
o-Xylene 5.02 5.00 100 70-130
Surrogate: 4-Bromofluorobenzene (1) 7.57 8.00 94.6 70-130
Page 16 of 26

con -test®
A Pace Analytical Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Note: Blank Subtraction is not performed unless otherwise noted
FLAG/QUALIFIER SUMMARY
*
QC result is outside of established limits.
t
Wide recovery limits established for difficult compound.
$
Wide RPD limits established for difficult compound.
#
Data exceeded client recommended or regulatory level
RL
Reporting Limit
MDL
Method Detection Limit
RPD
Relative Percent Difference
LCS
Laboratory Control Sample
LCS Dup
Duplicate Laboratory Control Sample
MS
Matrix Spike Sample
MS Dup
Duplicate Matrix Spike Sample
REC
Recovery
QC
Quality Control
ppbv
Parts per billion volume
EPA
United States Environmental Protection Agency
% REC
Percent Recovery
ND
Not Detected
N/A
Not Applicable
DL
Detection Limit
NC Not Calculated
LFB/LCS Lab Fortified Blank/Lab Control Sample
ORP Oxidation -Reduction Potential
wet Not dry weight corrected
% wt Percent weight
Kg Kilogram
g Gram
mg Milligram
µg Microgram
ng Nanogram
L Liter
mL Milliliter
µL Microliter
m3 Cubic Meter
EPH Extractable Petroleum Hydrocarbons
VPH Volatile Petroleum Hydrocarbons
APH Air Petroleum Hydrocarbons
FID Flame Ionization Detector
PID Photo Ionization Detector
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
L-03 Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this
compound is likely to be biased on the low side.
V-04 Initial calibration did not meet method specifications. Compound was calibrated using a response factor where
%RSD is outside of method specified criteria. Reported result is estimated.
V-05 Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for
this compound.
V-34 Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this
compound. Reported result is estimated.
V-36 Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data
validation is not affected since sample result was "not detected" for this compound.
Page 17 of 26

con -test®
A Pace Analytical Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
TPH Thomas P. Hnitecki
RLF Rebecca Faust
STATION PDF Management Station
KKM Kerry K. McGee
BRF Brittany R. Fisk
ANALYST
Page 18 of 26

con -test®
A Pace Analytical Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
INTERNAL STANDARD AREAAND RT SUMMARY
EPA TO-15
Internal Standard
Response
RT
Reference
Response
Reference
RT
Area %
Area o/
Limits
RT Diff
RT Diff
Limit
Q
Initial Cal Check (S062606-ICV1) Lab File ID: J21A232023.D Analyzed: 08/21/21 02:04
Bromochloromethane (1)
152325
2.866
150879
2.863
101
60 - 140
0.0030
+/-0.50
1,4-Difluorobenzene(1)
700372
3.471
694423
3.468
101
60-140
0.0030
+/-0.50
Chlorobenzene-d5(1)
652377
5.056
641566
5.057
102
60-140
-0.0010
+/-0.50
INTERNAL STANDARD AREAAND RT SUMMARY
EPA TO-15
Internal Standard
Response
RT
Reference
Response
Reference
RT
Area %
Area o/
Limits
RT Diff
RT Diff
Limit
Q
Calibration Check (S065181-CCVI) Lab File ID: J21A313004.13 Analyzed: 11/09/21 10:26
Bromochloromethane (1)
177320
2.857
150879
2.863
118
60 - 140
-0.0060
+/-0.50
1,4-Difluorobenzene(1)
649426
3.465
694423
3.468
94
60-140
-0.0030
+/-0.50
Chlorobenzene-d5(1)
595617
5.054
641566
5.057
93
60-140
-0.0030
+/-0.50
LCS (B294400-BS1 ) Lab File ID: J21A313005.13 Analyzed: 11/09/21 10:51
Bromochloromethane (1)
179173
2.857
177320
2.857
101
60 - 140
0.0000
+/-0.50
1,4-Difluorobenzene(1)
654606
3.465
649426
3.465
101
60-140
0.0000
+/-0.50
Chlorobenzene-d5(1)
592872
5.054
595617
5.054
100
60-140
0.0000
+/-0.50
Blank (B294400-BLK1) Lab File ID: J21A313019.13 Analyzed: 11/09/21 18:47
Bromochloromethane (1)
171058
2.847
177320
2.857
96
60 - 140
-0.0100
+/-0.50
1,4-Difluorobenzene(1)
573280
3.459
649426
3.465
88
60-140
-0.0060
+/-0.50
Chlorobenzene-d5 (1)
537049
5.05
595617
5.054
90
60 - 140
-0.0040
+/-0.50
SG-1 (21K0213-01) Lab File ID: J21A313033.13 Analyzed: 11/10/21 08:18
Bromochloromethane (1)
179368
2.854
177320
2.857
101
60 - 140
-0.0030
+/-0.50
1,4-Difluorobenzene(1)
630720
3.462
649426
3.465
97
60-140
-0.0030
+/-0.50
Chlorobenzene-d5(1)
592911
5.054
595617
5.054
100
60-140
0.0000
+/-0.50
SG-2 (21K0213-02) Lab File ID: J21A313034.13 Analyzed: 11/10/21 08:43
Bromochloromethane (1)
178227
2.85
177320
2.857
101
60 - 140
-0.0070
+/-0.50
1,4-Difluorobenzene(1)
610451
3.462
649426
3.465
94
60-140
-0.0030
+/-0.50
Chlorobenzene-d5(1)
571516
5.053
595617
5.054
96
60-140
-0.0010
+/-0.50
SG-3 (21K0213-03) Lab File ID: J21A313035.1) Analyzed: 11/10/21 09:07
Bromochloromethane (1)
181144
2.85
177320
2.857
102
60 - 140
-0.0070
+/-0.50
1,4-Difluorobenzene(1)
624343
3.462
649426
3.465
96
60-140
-0.0030
+/-0.50
Chlorobenzene-d5(1)
597162
5.054
595617
5.054
100
60-140
0.0000
+/-0.50
SG4 (21K0213-04) Lab File ID: J21A313036.1) Analyzed: 11/10/21 09:32
Bromochloromethane (1)
181915
2.853
177320
2.857
103
60 - 140
-0.0040
+/-0.50
1,4-Difluorobenzene(1)
641388
3.465
649426
3.465
99
60-140
0.0000
+/-0.50
Chlorobenzene-d5(1)
603684
5.053
595617
5.054
101
60-140
-0.0010
+/-0.50
Page 19 of 26

con -test®
A Pace Analytical Laboratory
39 Spruce Street' East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S065181-CCV 1
COMPOUND
TYPE
CONC. (ppbv)
RESPONSE FACTOR
% DIFF / DRIFT
STD
CCV
ICAL
CCV
MIN (#)
CCV
LIMIT (#)
Acetone
A
5.00
4.52
1.013483
0.9171938
-9.5
30
Benzene
A
5.00
5.31
0.5773346
0.6130608
6.2
30
Benzyl chloride
A
5.00
5.68
0.5662092
0.6426116
13.5
30
Bromodichloromethane
A
5.00
5.33
0.4493554
0.4790249
6.6
30
Bromoform
A
5.00
4.78
0.6972692
0.6673174
-4.3
30
Bromomethane
A
5.00
4.57
0.795872
0.7275434
-8.6
30
1,3-Butadiene
A
5.00
5.07
0.4907101
0.4972705
1.3
30
2-Butanone (MEK)
A
5.00
3.92
1.40087
1.097487
-21.7
30
Carbon Disulfide
A
5.00
5.25
1.998984
2.098507
5.0
30
Carbon Tetrachloride
A
5.00
4.61
0.5188025
0.4785223
-7.8
30
Chlorobenzene
A
5.00
4.95
0.7193
0.7123772
-1.0
30
Chloroethane
A
5.00
5.12
0.3795632
0.3883691
2.3
30
Chloroform
A
5.00
4.23
1.888134
1.597861
-15.4
30
Chloromethane
A
5.00
5.14
0.5417118
0.5573111
2.9
30
Cyclohexane
A
5.00
4.77
0.265344
0.2530727
-4.6
30
Dibromochloromethane
A
5.00
4.93
0.6098379
0.6016833
-1.3
30
1,2-Dibromoethane(EDB)
A
5.00
5.14
0.4553549
0.4678872
2.8
30
1,2-Dichlorobenzene
A
5.00
4.71
0.757862
0.7141986
-5.8
30
1,3-Dichlorobenzene
A
5.00
5.18
0.7367625
0.763723
3.7
30
1,4-Dichlorobenzene
A
5.00
5.01
0.7493582
0.7513849
0.3
30
Dichlorodifluoromethane (Freon 12)
A
5.00
4.26
2.185662
1.862342
-14.8
30
1,1-Dichloroethane
A
5.00
4.38
1.41636
1.240902
-12.4
30
1,2-Dichloroethane
A
5.00
4.10
1.131436
0.9289871
-17.9
30
1,1-Dichloroethylene
A
5.00
5.19
1.038306
1.077293
3.8
30
cis-1,2-Dichloroethyl-e
A
5.00
4.26
1.058854
0.9025671
-14.8
30
trans-1,2-Dichloroethylene
A
5.00
4.25
1.144971
0.9726776
-15.0
30
1,2-Dichloropropane
A
5.00
5.61
0.2035658
0.2283592
12.2
30
cis- 1,3 -Dichloropropene
A
5.00
5.21
0.3153762
0.328864
4.3
30
trans- l,3-Dichloropropene
A
5.00
5.00
0.2855395
0.285744
0.07
30
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 1
A
5.00
4.74
2.0897
1.980311
-5.2
30
1,4-Dioxane
A
5.00
4.94
0.1348394
0.1331564
-1.2
30
Ethanol
A
5.00
4.67
0.1363511
0.1274712
-6.5
30
Ethyl Acetate
A
5.00
4.20
0.2996362
0.2517122
-16.0
30
Ethylbenzene
A
5.00
4.89
1.068394
1.045249
-2.2
30
4-Ethyltoluene
A
5.00
4.75
1.191921
1.132835
-5.0
30
Heptane
A
5.00
5.69
0.1598388
0.1820118
13.9
30
Hexachlorobutadiene
4
5.00
3.43
1.05506
0.7240465
-31.4
30
Hexane
L
5.00
4.34
0.7820405
0.6245703
-13.2
30
Page 20 of 26

con -test®
A Pace Analytical Laboratory
39 Spruce Street' East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
5065181-CCV 1
COMPOUND
TYPE
CONC. (ppbv)
RESPONSE FACTOR
% DIFF / DRIFT
STD
CCV
ICAL
CCV
MIN (#)
CCV
LIMIT (#)
2-Hexanone (MBK)
A
5.00
5.86
0.3105363
0.363772
17.1
30
Isopropanol
A
5.00
4.52
1.087458
0.9820618
-9.7
30
Methyl tert-Butyl Ether (MTBE)
A
5.00
3.51
2.400388
1.685856
-29.8
30
Methylene Chloride
A
5.00
5.19
0.6720844
0.6973246
3.8
30
4-Methyl-2-pentanone (MI13K)
A
5.00
5.79
0.141787
0.164246
15.8
30
Naphthalene
A
5.00
4.08
1.049522
0.8573644
-18.3
30
Propene
A
5.00
4.30
0.4575591
0.3932236
-14.1
30
Styrene
A
5.00
4.92
0.6387272
0.6279445
-1.7
30
1,1,2,2-Tetrachloroethane
A
5.00
5.91
0.5691929
0.672639
18.2
30
Tetrachloroethylene
A
5.00
4.22
0.5934671
0.5011516
-15.6
30
Tetrahydroforan
A
5.00
3.88
0.811293
0.6288292
-22.5
30
Toluene
A
5.00
4.81
0.8381161
0.805981
-3.8
30
1,2,4-Trichlorobenzene
A
5.00
3.91
0.5285083
0.4136537
-21.7
30
1, 1, 1 -Trichloroethane
A
5.00
4.66
0.4533588
0.4221993
-6.9
30
1,1,2-Trichloroethane
A
5.00
5.24
0.2953724
0.3093773
4.7
30
Trichloroethylene
A
5.00
4.97
0.2950588
0.2934752
-0.5
30
Trichlorofluoromethane (Freon 11)
A
5.00
4.48
2.216429
1.98762
-10.3
30
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 11
A
5.00
4.83
1.637043
1.581845
-3.4
30
1,2,4-Trimethylbenzene
A
5.00
4.58
1.051818
0.96318
-8.4
30
1,3,5-Trimethylbenzene
A
5.00
4.83
1.056033
1.020629
-3.4
30
Vinyl Acetate
A
5.00
3.26
1.072956
0.699788
-34.8
30
Vinyl Chloride
A
5.00
5.21
0.6636142
0.6920189
4.3
30
m&p-Xylene
A
10.0
10.4
0.8662275
0.8993699
3.8
30
o-Xylene
A
5.00
5.04
0.8477905
0.8542107
0.8
30
# Column to be used to flag Response Factor and %Diff/Drift values with an asterisk
* Values outside of QC limits
Page 21 of 26

con -test®
A Pace Analytical Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
EPA TO-15 in Air
Acetone
Benzene
Benzyl chloride
Bromodichloromethane
Bromoform
Bromomethane
1,3-Butadiene
2-Butanone (MEK)
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane (Freon 12)
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethylene
cis-1,2-Dichloroethylene
trans- l,2-Dichloro ethylene
1,2-Dichloropropane
cis- 1,3 -Dichloropropene
trans- 1, 3 -Dichloropropene
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
1,4-Dioxane
Ethanol
Ethyl Acetate
Ethylbenzene
4-Ethyltoluene
Heptane
Hexachlorobutadiene
Hexane
2-Hexanone (MBK)
Isopropanol
Methyl tart -Butyl Ether (MTBE)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Naphthalene
Propene
Styrene
1,1,2,2-Tetrachloroethane
Certifications
AIHA,NY,ME,NH
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,NJ,NY,ME,NH,VA
AIHA,NJ,NY,ME,NH,VA
AIHA,FL,NJ,NY,ME,NH
AIHA,NJ,NY,ME,NH,VA
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,NJ,NY,ME,NH, VA
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,NJ,NY,ME,NH,VA
AIHA,NY,ME,NH
AIHA,NJ,NY,ME,NH
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,NJ,NY,ME,NH
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,NY,ME,NH
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,FL,NY,ME,NH,VA
AIHA,NJ,NY,ME,NH,VA
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,NY,ME,NH
AIHA,NJ,NY,ME,NH,VA
AIHA,NJ,NY,ME,NH,VA
AIHA
AIHA
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,NJ
AIHA,NJ,NY,ME,NH,VA
AIHA,NJ,NY,ME,NH,VA
AIHA,FL,NJ,NY,ME,NH, VA
AIHA
AIHA,NY,ME,NH
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,FL,NJ,NY,ME,NH
NY,ME,NH
AIHA
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,FL,NJ,NY,ME,NH,VA
Page 22 of 26

con -test®
A Pace Analytical Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
EPA TO-15 in Air
Tetrachloroethylene
Tetrahydrofuran
Toluene
1,2,4-Trichlorobenzene
1, 1, 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethylene
Trichlorofluoromethane (Freon 11)
1,1,2-Trichloro-1,2,2-ttifluoroethane (Freon 113)
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl Acetate
Vinyl Chloride
m&p-Xylene
o-Xylene
Certifications
AIHA,FL,NJ,NY,ME,NH, VA
AIHA
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,NJ,NY,ME,NH,VA
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,NY,ME,NH
AIHA,NJ,NY,ME,NH, VA
AIHA,NJ,NY,ME,NH
AIHA,NJ,NY,ME,NH
AIHA,FL,NJ,NY,ME,NH, VA
AIHA,FL,NJ,NY,ME,NH, VA
AIHA, FL,NJ,NY,ME,NH, VA
AIHA,FL,NJ,NY,ME,NH, VA
Con -Test, a Pace Environmental Laboratory, operates under the following certifications and accreditation:
Code
Description
Number
Expires
AHIA
AIHA-LAP, LLC - ISO17025:2017
100033
03/l/2022
MA
Massachusetts DEP
M-MA100
06/30/2022
CT
Connecticut Department of Publilc Health
PH-0165
12/31/2022
NY
New York State Department of Health
10899 NELAP
04/l/2022
NH-S
New Hampshire Environmental Lab
2516 NELAP
02/5/2022
RI
Rhode Island Department of Health
LA000112
12/30/2021
NC
North Carolina Div. of Water Quality
652
12/31/2021
NJ
New Jersey DEP
MA007 NELAP
06/30/2022
FL
Florida Department of Health
E871027 NELAP
06/30/2022
VT
Vermont Department of Health Lead Laboratory
LL720741
07/30/2022
ME
State of Maine
MA00100
06/9/2023
VA
Commonwealth of Virginia
460217
12/14/2021
NH-P
New Hampshire Environmental Lab
2557 NELAP
09/6/2022
VT-DW
Vermont Department of Health Drinking Water
VT-255716
06/12/2022
NC-DW
North Carolina Department of Health
25703
07/31/2022
PA
Commonwealth of Pennsylvania DEP
68-05812
06/30/2022
MI
Dept. of Env, Great Lakes, and Energy
9100
09/6/2022
Page 23 of 26

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Page 24 of 26

1113121, 4:54 PM
Fe&x=
Detailed Tracking
FROM
Huntersville, NC US
Travel History
TIME ZONE
Loca# Scan Time
Wednesday, November 3,
2021
11:09 AM
5.25 AM
5D7 AM
Tuesday, November 2, 2021
1OAS PM
10:20 AM
Monday, November 1,
2021
8:10 PM
4 06 PM
228PM
TRACK ANOTHER SHIPMENT
987548468491
ADD NICKNAME
Delivered
DELIVERED
Signed for by: APRESHEWSKI
GET STATUS UPDATES
OBTAIN PROOF OF DELIVERY
TO
East Longmeadow, MA US
East Longmeadow, MA Delivered
WINDSOR, CT On FedEx vehicle for delivery
WIN DSCR, CT At local FedEx facility
MIDDLETOWN, CT In transit
CONCORD, NC Left FedEx origin facility
CONCORD, NC Arrived at FedEx location
CONCORD, NC Picked up
Shipment information sent to FedEx
li� (D
\Z
https:llwww.fedex.comlfedextrackl?trknbr=987548468491&trkqual=12022-987548468491—FDEG Page 25 of 26

I Have Not Confirmed Sample Container
Numbers With Lab Staff Before ce t
Relinquishing Over A."As LA"rIC .'AL- ¢._AUOU Ft^-rC MM
Samples
Coc# 27& R�� 8:217 . .
Air Media Sample Receipt Checklist - (Rejection Criteria Listing - Using Acceptance Policy) Any False
Statement will be brought to the attention of the Client - State True or False
Client L.0 `1:>
Received By LPL Date
___2TimeI1L�
How were the samples In Cooler
On Ice No Ice
received? In Box
Ambient Melted Ice
Were samples within Temperature By Gun #
Actual Temp -
Compliance? 2-60C By Blank #
Actual Temp -
Was Custody Seal Intact? y
Were Samples Tampered with?
Was COC Relinquished ? Z�
�
Does Chain Agree With Samples? 7
Are there any loose caps/valves on any samples?
Is COC in ink/ Legible? 7�
Did COC Include all Client ; Analysis
i Sampler Name __V
Pertinent Information? Project ID's
i Collection Dates/Times
Are Sample Labels filled out and legible? 7
Are there Rushes? Who was notified?
Samples are received within holding time? __\
Proper Media Used? `
Individually Certified Cans? -F—
Are there Trip Blanks? V_
is there enough Volume? j
Summa Can.
Tedlar Bags
TO-17 Tubes
11s
ommAnts-
t ivuurerrule
Tubing
T-Connector
f Page 26 of 26 1

APPENDIX D

Risk for Individual Pathways
1
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID:
Exposure Unit ID: GW-3
DIRECT CONTACT SOIL AND WATER CALCULATORS
Receptor
Pathway
CarcinogenicRisk
Hazard Index
Risk exceeded?
Resident
Soil
0.0E+00
0.0E+00
NO
Groundwater Use*
NC
NC
NC
Non -Residential Worker
Soil
0.0E+00
0.0E+00
NO
Groundwater Use*
NC
NC
NC
Construction Worker
Soil
NC
NC
NC
Recreator/Trespasser
Soil
NC
NC
NC
Surface Water*
NC
NC
NC
VAPOR INTRUSION CALCULATORS
Receptor
Pathway
Carcinogenic
Risk
Hazard Index
Risk exceeded?
Resident
Groundwater to Indoor Air
3.4E-05
2.9E-01
NO
Soil Gas to Indoor Air
0.0E+00
0.0E+00
NO
Indoor Air
0.0E+00
0.0E+00
NO
Non -Residential Worker
Groundwater to Indoor Air
7.8E-06
7.0E-02
NO
Soil Gas to Indoor Air
0.0E+00
0.0E+00
NO
Indoor Air
0.0E+00
0.0E+00
NO
CONTAMINANT MIGRATION CALCULATORS
Pathway
Source
Target Receptor Concentrations Exceeded?
Groundwater
Source Soil
Exceedence of 2L at Receptor?
NM
Source Groundwater
Exceedence of 2L at Receptor?
NM
Surface Water
Source Soil
Exceedence of 2B at Receptor?
NM
Source Groundwater
Exceedence of 2B at Receptor?
NM
Notes:
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk -based
closure.
3. NM = Not Modeled
4. NC = Pathway not calculated
North Carolina DEQ Risk Calculator

Risk for Individual Pathways
1
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID:
Exposure Unit ID: SG-4
DIRECT CONTACT SOIL AND WATER CALCULATORS
Receptor
Pathway
CarcinogenicRisk
Hazard Index
Risk exceeded?
Resident
Soil
0.0E+00
0.0E+00
NO
Groundwater Use*
NC
NC
NC
Non -Residential Worker
Soil
0.0E+00
0.0E+00
NO
Groundwater Use*
NC
NC
NC
Construction Worker
Soil
NC
NC
NC
Recreator/Trespasser
Soil
NC
NC
NC
Surface Water*
NC
NC
NC
VAPOR INTRUSION CALCULATORS
Receptor
Pathway
Carcinogenic
Risk
Hazard Index
Risk exceeded?
Resident
Groundwater to Indoor Air
0.0E+00
0.0E+00
NO
Soil Gas to Indoor Air
4.4E-06
1.0E-01
NO
Indoor Air
0.0E+00
0.0E+00
NO
Non -Residential Worker
Groundwater to Indoor Air
0.0E+00
0.0E+00
NO
Soil Gas to Indoor Air
3.3E-07
8.2E-03
NO
Indoor Air
0.0E+00
0.0E+00
NO
CONTAMINANT MIGRATION CALCULATORS
Pathway
Source
Target Receptor Concentrations Exceeded?
Groundwater
Source Soil
Exceedence of 2L at Receptor?
NM
Source Groundwater
Exceedence of 2L at Receptor?
NM
Surface Water
Source Soil
Exceedence of 2B at Receptor?
NM
Source Groundwater
Exceedence of 2B at Receptor?
NM
Notes:
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk -based
closure.
3. NM = Not Modeled
4. NC = Pathway not calculated
North Carolina DEQ Risk Calculator