25009_East Side Truck Svc_Final Grade Sampling_20231205

Atlantic Shores
Environmental Services, Ltd.
December 5, 2023
Stephanie Graham
Brownfields Project Manager
217 West Jones Street
Raleigh, North Carolina 27603
Reference: Final Grade Soil Sampling
East Side Trucking Service
520 Judson Church Road, Fayetteville, North Carolina
Brownfields Project Number 25009-21-026
Ms. Graham,
Final grade soil sampling has been conducted at the above referenced East Side Trucking Service
site, located at 520 Judson Church Road in Fayetteville, North Carolina. Atlantic Shores
Environmental Services, Ltd. (ASE) collected final grade soil samples at the site on September 12,
2023, in accordance with the site's approved Environmental Management Plan (EMP), dated
March 18, 2022.
The East Side Trucking Service site is comprised of two (2) adjoining Cumberland County parcels
addressed as 520 Judson Church Road, Fayetteville, North Carolina, and encompasses
approximately 3.39 acres (refer to Figure 1). The subject site is being redeveloped into a 74,733
square -foot, Springhill Suites hotel. The prospective developer submitted a Brownfield application
for the site on January 12, 2021, and received a letter of eligibility on April 16, 2021. Construction
efforts began in 2022, with site final grading occurring in early September 2023.
On September 12, 2023, ASE collected final grade soil samples from select locations across the
site. Ten (10) discrete soil samples, including one (1) duplicate sample, were collected from nine
(9) locations at the site (refer to Figure 2). Samples were collected from depths of 1-foot through
2 feet below ground surface (bgs). The locations of the final grade soil samples were determined
based on sample locations indicated on Figure 3, in the North Carolina Brownfields Program
Environmental Management Plan for the East Side Trucking Services site.
175-1 Venture Drive, Belville NC 28451 P:[phone]
-A Woman Owned Business - License No. C-4762

Final Grade Soil Sampling
East Side Trucking Service
520 Judson Church Road, Fayetteville, North Carolina
Brownfields Project Number 25009-21-026
December 5, 2023
The final grade soil samples were analyzed for the following analytes:
• Volatile organic compounds (VOCs) by EPA method 8260D
• Semi -volatile organic compounds (SVOCs) by EPA Method 8270E
• Resource, Conservation and Recovery Act (RCRA) 8 Metals by EPA Method 6010/74711
• Hexavalent Chromium by EPA Method 7199
A decontaminated, stainless -steel hand auger was used to advance a boring to a depth of 1-foot
through 2 feet bgs at each sample location. Discrete sample aliquots were collected at each sample
location and placed in the appropriate, laboratory prepared containers, using new disposable nitrile
gloves for each sample. After being filled, the sample containers were labeled with the project
name and number, the time and date of sample collection, the analyses to be performed, and the
absence or presence of preservative. The filled sample containers were then placed into an ice -
filled cooler to maintain the temperature of the soil samples at approximately 4° Celsius. A chain -
of -custody was completed, and the samples were transported to ASE's office, where they were
picked up by a Pace Analytical employee and delivered to Pace Analytical in Raleigh, North
Carolina for laboratory analysis.
Sample collection was conducted in accordance with the North Carolina Department of
Environmental Quality (NCDEQ) Inactive Hazardous Sites Program Guidelines for Assessment
and Cleanup (September 2022). The samples were compared to the NCDEQ Preliminary Soil
Remediation Goals (PSRGs), Residential Health Based PSRGs (July 2023). The results of
laboratory analysis of the soil samples submitted are summarized in the attached Table 1. The
Report of Laboratory Analysis and chain -of -custody record are also attached.
VOCs Analysis Summary
Trace concentrations of benzene, ethylbenzene, toluene, n-propylbenzene, methylene chloride, and
total xylenes, including m&p xylene and o-xylene, were identified in the sampled soils. However,
VOCs were not identified above their respective Residential PSRGs. It should be noted that methylene
chloride is a common laboratory contaminant.
SVOCs Analysis Summary
SVOCs were not detected in the soil samples submitted to the laboratory for analysis.
Metals Analysis Summary
When submitting the soil samples for analysis, ASE personnel listed EPA Method 6020/7471 on the
chain -of -custody. This request was forwarded from the Pace Analytical Raleigh, North Carolina
Office's project manager to the Pace Analytical satellite testing laboratory in Florida. However, the
satellite testing laboratory analyzed the samples using EPA Method 6010 due to an apparent internal
communication error within the satellite laboratory. The Pace Analytical Raleigh, North Carolina
Office's project manager indicated that Methods 6010 and 6020 are nearly identical, with Method
6020 having slightly lower method detection limits (MDLs), depending on the dry weight of the
samples.
' Varies from EMP — Explanation above
W

Final Grade Soil Sampling
East Side Trucking Service
520 Judson Church Road, Fayetteville, North Carolina
Brownfields Project Number 25009-21-026
December 5, 2023
Laboratory analysis indicated the presence of barium, cadmium, total chromium, lead, and mercury
in the soil samples below the published Residential PSRGs for those analytes. Arsenic was identified
slightly above the Residential PSRG in samples FG-2, FG-5, and FG-7.
Hexavalent chromium was not identified in the analyzed soil samples. However, due to the
Laboratory internal miscommunication, the method detection limit for hexavalent chromium was
slightly above the Residential PSRG in the soil samples analyzed.
If there are questions regarding this report, or a need for further information, please contact us at
910-371-5980.
Sincerely,
ATLANTIC SHORES ENVIRONMENTAL SERVICES, LTD.
Cheryl J. Moody, PE, REM
Principal Engineer
Attachments: Table 1
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Kevin Dillon, REP
Senior Project Manager
Figure 1
Figure 2
Report of Laboratory Analysis and Chain -of -Custody
Field Notes
3

Final Grade Soil Sampling
East Side Trucking Service
520 Judson Church Road, Fayetteville, North Carolina
Brownfields Project Number 25009-21-026
FIGURES
December 5, 2023

Figure 1: USGS Topographic Location Map
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' Service Layer Credits: USGS The National Map: National Boundaries
Dataset, 3DEP Elevation Program, Geographic Names Information System,
National Hydrography Dataset, National Land Cover Database, National
Structures Dataset, and National Transportation Dataset; USGS Global
Legend
Ecosystems; U.S. Census Bureau TIGER/Line data; USFS Road Data;
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Natural Earth Data; U.S. Department of State Humanitarian Information Unit;
and NOAA National Centers for Environmental Information, U.S. Coastal
0 Site Location
Relief Model. Data refreshed October 2018.
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Environmental Services, Ltd.
520 Judson Church Road
Fayetteville, North Carolina
Project Number: 25009-21-026
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FIGURE 2 —Final Grade Sample Locations � N
Source: Site Plans
East Side Truck Service li��A-0—
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520 Judson Church Road � �s
Fayetteville, North Carolina ASE Project No. 1487
---------------------
Brownfields Project No: 25009-21-026 September 2023Envronmental Services, Ltd.

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FIGURE 2 —Final Grade Sample Locations � N
Source: Site Plans
East Side Truck Service li��A-0—
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Fayetteville, North Carolina ASE Project No. 1487
---------------------
Brownfields Project No: 25009-21-026 September 2023Envronmental Services, Ltd.

Final Grade Soil Sampling
East Side Trucking Service
520 Judson Church Road, Fayetteville, North Carolina
Brownfields Project Number 25009-21-026
TABLES
December 5, 2023

TABLE 1 - Final Grade Soil Sampling Analytical Results
East Side Trucking Service
520 Judson Church Road, Fayetteville, North Carolina
Brownfield No.25009-21-026
Sample ID
FG-1
FG-2
FG-3
FG4
FG-5
FG-6
FG-7
FG-8
FG-9
FG-10
Depth (Feet)
0-1
0-1
0-1
0-1
0-1
0-1
0-1
0-1
0-1
0-1
Residential
Lattitude
35.008911
35.008486
35.009128
35.008681
35.008349
35.009315
35.009276
35.00856
35.009027
35.008681
PSRG
Longitude
-78.815576
-78.815856
-78.815927
-78.816143
-78.816177
-78.816153
-78.816474
-78.816904
-78.817098
-78.816143
(mg/kg)
Date
9/12/23
9/12/23
9/12/23
9/12/23
9/12/23
9/12/23
9/12/23
9/12/23
9/12/23
9/12/23
VOCs - 8260 (mg/kg)
Benzene
<0.0021
<0.0023
<0.0022
0.0041J
<0.0025
<0.0025
<0.0051
<0.0032
<0.0032
<0.0023
1.2
Ethylbenzene
<0.0025
<0.0027
<0.0025
0.0073
<0.0030
<0.0029
<0.0059
<0.0037
0.0092
0.0047J
6.1
n-Propylbenzene
<0.0019
<0.0021
<0.0019
<0.0019
<0.0023
<0.0022
<0.0045
<0.0028
0.0054J
<0.0020
780
Methylene Chloride*
<0.0215
<0.0161
<0.0149
<0.0146
<0.0174
<0.0169
<0.035
<0.0217
<0.022
0.0332
580
Toluene
<0.0037
<0.0041
<0.0038
0.0276
<0.0044
0.0079
1 <0.0088
<0.0055
<0.0055
0.0083
990
Xylene (total)
<0.0031
<0.0034
<0.0031
0.0274
<0.0036
<0.0035
<0.0073
0.0055J
0.0234
0.0083J
120
m&p Xylene
<0.0037
<0.0040
<0.0037
0.0209
<0.0043
<0.0042
<0.0087
0.0055J
0.0178
0.0083J
120
o-Xylene
<0.0024
<0.0026
<0.0024
0.0065
<0.0028
<0.0027
<0.0056
<0.0035
0.0056J
<0.0025
140
SVOCs - 8270 (mg/kg) - Not Detected
Metals (mg/kg)
Arsenic
0.64
0.98
0.55J
0.53J
0.77
<0.31
1.1
0.50J
<0.33
0.47J
0.68
Barium
16.7
5.1
4.6
15.7
16.5
30.3
29.5
15.5
29.1
12.1
3,100
Cadmium
0.055J
0.038J
0.032J
0.049J
0.062
0.089
0.082
0.050J
0.13
0.040J
1.4
Chromium
5.8
6.4
5.2
5.5
6.1
7.3
8.2
4.6
9.5
4.4
NE
Chromium VI (Method 7199)
0.579J
0.940J
0.532J
0.402J
0.652J
0.633J
0.596J
0.492J
0.886J
0.452J
0.31
Lead
4.3
3.4
2.2
4.0
4.2
6.1
15.4
2.5
7.6
2.8
250
Mercury
0.022
0.023
0.048
0.021
0.031
0.036
0.035
0.025
0.046
0.019
4.7
* Methylene Chloride is a common laboratory contaminant
Red items are exceedances of residential PSRGs and/or the method detection limit is above the PSRG
NE - Not Established
Data compared to NCDEQ PSRGs July 2023

Final Grade Soil Sampling
East Side Trucking Service
520 Judson Church Road, Fayetteville, North Carolina
Brownfields Project Number 25009-21-026
REPORT OF LABORATORY ANALYSIS
CHAIN -OF -CUSTODY
December 5, 2023

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
September 25, 2023
Cheryl Moody
Atlantic Shore Environmental
175-1 Venture Drive
Belville, NC 28451
RE: Project: JOB #1487
Pace Project No.: 92688240
Dear Cheryl Moody:
Enclosed are the analytical results for sample(s) received by the laboratory on September 14, 2023. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
704-977-0942
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 88

Project: JOB #1487
Pace Project No.: 92688240
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REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: JOB #1487
Pace Project No.: 92688240
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REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
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[phone]
SAMPLE SUMMARY
Project: JOB #1487
Pace Project No.: 92688240
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92688240001
FG-1
Solid
09/12/23 14:30
09/14/23 09:20
92688240002
FG-2
Solid
09/12/23 14:10
09/14/23 09:20
92688240003
FG-3
Solid
09/12/23 14:42
09/14/23 09:20
92688240004
FG-4
Solid
09/12/23 16:44
09/14/23 09:20
92688240005
FG-5
Solid
09/12/23 16:18
09/14/23 09:20
92688240006
FG-6
Solid
09/12/23 14:56
09/14/23 09:20
92688240007
FG-7
Solid
09/12/23 15:25
09/14/23 09:20
92688240008
FG-8
Solid
09/12/23 15:41
09/14/23 09:20
92688240009
FG-9
Solid
09/12/23 15:53
09/14/23 09:20
92688240010
FG-10
Solid
09/12/23 16:44
09/14/23 09:20
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
JOB #1487
92688240
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92688240001
FG-1
EPA6010
AAM1
7
PASI-O
EPA 7471
JNK
1
PASI-O
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
CMK
1
PAN
EPA 7199
SET
1
PAN
92688240002
FG-2
EPA6010
AAM1
7
PASI-O
EPA 7471
JNK
1
PASI-O
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
CMK
1
PAN
EPA 7199
SET
1
PAN
92688240003
FG-3
EPA6010
AAM1
7
PASI-O
EPA 7471
JNK
1
PASI-O
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
CMK
1
PAN
EPA 7199
SET
1
PAN
92688240004
FG-4
EPA6010
AAM1
7
PASI-O
EPA 7471
JNK
1
PASI-O
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
CMK
1
PAN
EPA 7199
SET
1
PAN
92688240005
FG-5
EPA6010
AAM1
7
PASI-O
EPA 7471
JNK
1
PASI-O
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
CMK
1
PAN
EPA 7199
SET
1
PAN
92688240006
FG-6
EPA6010
AAM1
7
PASI-O
EPA 7471
JNK
1
PASI-O
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 5 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: JOB #1487
Pace Project No.: 92688240
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
CMK
1
PAN
EPA 7199
SET
1
PAN
92688240007
FG-7
EPA6010
AAM1
7
PASI-O
EPA 7471
JNK
1
PASI-O
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
CMK
1
PAN
EPA 7199
SET
1
PAN
92688240008
FG-8
EPA6010
AAM1
7
PASI-O
EPA 7471
JNK
1
PASI-O
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
LMB
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
CMK
1
PAN
EPA 7199
SET
1
PAN
92688240009
FG-9
EPA6010
AAM1
7
PASI-O
EPA 7471
JNK
1
PASI-O
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
LMB
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
CMK
1
PAN
EPA 7199
SET
1
PAN
92688240010
FG-10
EPA6010
AAM1
7
PASI-O
EPA 7471
JNK
1
PASI-O
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
LMB
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
CMK
1
PAN
EPA 7199
SET
1
PAN
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
PASI-O = Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-1
Lab ID:
92688240001
Collected:
09/12/23
14:30
Received: 09/14/23
09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for
percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA
3050
Pace Analytical
Services
- Ormond Beach
Arsenic
0.64
mg/kg
0.56
0.28
1
09/22/2311:05
09/25/2311:12
7440-38-2
Barium
16.7
mg/kg
0.56
0.095
1
09/22/2311:05
09/25/2311:12
7440-39-3
Cadmium
0.055J
mg/kg
0.056
0.028
1
09/22/2311:05
09/25/2311:12
7440-43-9
Chromium
5.8
mg/kg
0.28
0.14
1
09/22/2311:05
09/25/2311:12
7440-47-3
Lead
4.3
mg/kg
0.56
0.28
1
09/22/2311:05
09/25/2311:12
7439-92-1
Selenium
ND
mg/kg
0.84
0.42
1
09/22/2311:05
09/25/2311:12
7782-49-2
Silver
ND
mg/kg
0.28
0.062
1
09/22/2311:05
09/25/2311:12
7440-22-4
7471 Mercury
Analytical
Method: EPA 7471 Preparation
Method: EPA
7471
Pace Analytical
Services
- Ormond Beach
Mercury
0.022
mg/kg
0.0085
0.0042
1
09/21/2312:51
09/22/2310:04
7439-97-6
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services
- Charlotte
Acenaphthene
ND
ug/kg
359
126
1
09/17/23 17:12
09/18/23 09:05
83-32-9
Acenaphthylene
ND
ug/kg
359
126
1
09/17/23 17:12
09/18/23 09:05
208-96-8
Aniline
ND
ug/kg
359
140
1
09/17/23 17:12
09/18/23 09:05
62-53-3
Anthracene
ND
ug/kg
359
118
1
09/17/23 17:12
09/18/23 09:05
120-12-7
Benzo(a)anthracene
ND
ug/kg
359
120
1
09/17/23 17:12
09/18/23 09:05
56-55-3
Benzo(a)pyrene
ND
ug/kg
359
124
1
09/17/23 17:12
09/18/23 09:05
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
359
120
1
09/17/23 17:12
09/18/23 09:05
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
359
139
1
09/17/23 17:12
09/18/23 09:05
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
359
126
1
09/17/23 17:12
09/18/23 09:05
207-08-9
Benzoic Acid
ND
ug/kg
1800
772
1
09/17/23 17:12
09/18/23 09:05
65-85-0 v1
Benzyl alcohol
ND
ug/kg
718
272
1
09/17/23 17:12
09/18/23 09:05
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
359
138
1
09/17/23 17:12
09/18/23 09:05
101-55-3
Butylbenzylphthalate
ND
ug/kg
359
151
1
09/17/23 17:12
09/18/23 09:05
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
718
252
1
09/17/23 17:12
09/18/23 09:05
59-50-7
4-Chloroaniline
ND
ug/kg
718
282
1
09/17/23 17:12
09/18/23 09:05
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
359
149
1
09/17/23 17:12
09/18/23 09:05
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
359
135
1
09/17/23 17:12
09/18/23 09:05
111-44-4
2-Chloronaphthalene
ND
ug/kg
359
143
1
09/17/23 17:12
09/18/23 09:05
91-58-7
2-Chlorophenol
ND
ug/kg
359
135
1
09/17/23 17:12
09/18/23 09:05
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
359
134
1
09/17/23 17:12
09/18/23 09:05
7005-72-3
Chrysene
ND
ug/kg
359
131
1
09/17/23 17:12
09/18/23 09:05
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
359
138
1
09/17/23 17:12
09/18/23 09:05
53-70-3
Dibenzofuran
ND
ug/kg
359
130
1
09/17/23 17:12
09/18/23 09:05
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
359
130
1
09/17/23 17:12
09/18/23 09:05
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
359
127
1
09/17/23 17:12
09/18/23 09:05
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
359
137
1
09/17/23 17:12
09/18/23 09:05
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
718
243
1
09/17/23 17:12
09/18/23 09:05
91-94-1
2,4-Dichlorophenol
ND
ug/kg
359
140
1
09/17/23 17:12
09/18/23 09:05
120-83-2
Diethylphthalate
ND
ug/kg
359
132
1
09/17/23 17:12
09/18/23 09:05
84-66-2
2,4-Dimethylphenol
ND
ug/kg
359
149
1
09/17/23 17:12
09/18/23 09:05
105-67-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-1 Lab ID: 92688240001 Collected: 09/12/23 14:30 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Dimethylphthalate
ND
ug/kg
359
131
1
09/17/23 17:12
09/18/23 09:05
131-11-3
Di-n-butylphthalate
ND
ug/kg
359
121
1
09/17/23 17:12
09/18/23 09:05
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
718
335
1
09/17/23 17:12
09/18/23 09:05
534-52-1
2,4-Dinitrophenol
ND
ug/kg
1800
1110
1
09/17/23 17:12
09/18/23 09:05
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
359
138
1
09/17/23 17:12
09/18/23 09:05
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
359
132
1
09/17/23 17:12
09/18/23 09:05
606-20-2
Di-n-octylphthalate
ND
ug/kg
359
141
1
09/17/23 17:12
09/18/23 09:05
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
359
139
1
09/17/23 17:12
09/18/23 09:05
117-81-7
Fluoranthene
ND
ug/kg
359
123
1
09/17/23 17:12
09/18/23 09:05
206-44-0
Fluorene
ND
ug/kg
359
126
1
09/17/23 17:12
09/18/23 09:05
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
359
156
1
09/17/23 17:12
09/18/23 09:05
87-68-3
Hexachlorobenzene
ND
ug/kg
359
140
1
09/17/23 17:12
09/18/23 09:05
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
359
206
1
09/17/23 17:12
09/18/23 09:05
77-47-4
Hexachloroethane
ND
ug/kg
359
137
1
09/17/23 17:12
09/18/23 09:05
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
359
141
1
09/17/23 17:12
09/18/23 09:05
193-39-5
Isophorone
ND
ug/kg
359
160
1
09/17/23 17:12
09/18/23 09:05
78-59-1
1-Methylnaphthalene
ND
ug/kg
359
126
1
09/17/23 17:12
09/18/23 09:05
90-12-0
2-Methylnaphthalene
ND
ug/kg
359
144
1
09/17/23 17:12
09/18/23 09:05
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
359
147
1
09/17/23 17:12
09/18/23 09:05
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
359
145
1
09/17/23 17:12
09/18/23 09:05
15831-10-4
Naphthalene
ND
ug/kg
359
122
1
09/17/23 17:12
09/18/23 09:05
91-20-3
2-Nitroaniline
ND
ug/kg
1800
294
1
09/17/23 17:12
09/18/23 09:05
88-74-4
3-Nitroaniline
ND
ug/kg
1800
282
1
09/17/23 17:12
09/18/23 09:05
99-09-2
4-Nitroaniline
ND
ug/kg
718
273
1
09/17/23 17:12
09/18/23 09:05
100-01-6
Nitrobenzene
ND
ug/kg
359
167
1
09/17/23 17:12
09/18/23 09:05
98-95-3
2-Nitrophenol
ND
ug/kg
359
156
1
09/17/23 17:12
09/18/23 09:05
88-75-5
4-Nitrophenol
ND
ug/kg
1800
694
1
09/17/23 17:12
09/18/23 09:05
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
359
121
1
09/17/23 17:12
09/18/23 09:05
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
359
135
1
09/17/23 17:12
09/18/23 09:05
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
359
127
1
09/17/23 17:12
09/18/23 09:05
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
359
171
1
09/17/23 17:12
09/18/23 09:05
108-60-1
Pentachlorophenol
ND
ug/kg
718
352
1
09/17/23 17:12
09/18/23 09:05
87-86-5
Phenanthrene
ND
ug/kg
359
118
1
09/17/23 17:12
09/18/23 09:05
85-01-8
Phenol
ND
ug/kg
359
160
1
09/17/23 17:12
09/18/23 09:05
108-95-2
Pyrene
ND
ug/kg
359
146
1
09/17/23 17:12
09/18/23 09:05
129-00-0
Pyridine
ND
ug/kg
359
113
1
09/17/23 17:12
09/18/23 09:05
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
359
141
1
09/17/23 17:12
09/18/23 09:05
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
359
164
1
09/17/23 17:12
09/18/23 09:05
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
359
148
1
09/17/23 17:12
09/18/23 09:05
88-06-2
Surrogates
Nitrobenzene-d5 (S)
62
%
10-130
1
09/17/23 17:12
09/18/23 09:05
4165-60-0
2-Fluorobiphenyl (S)
58
%
10-130
1
09/17/23 17:12
09/18/23 09:05
321-60-8
Terphenyl-d14 (S)
71
%
10-130
1
09/17/23 17:12
09/18/23 09:05
1718-51-0
Phenol-d6 (S)
61
%
10-130
1
09/17/23 17:12
09/18/23 09:05
13127-88-3
REPORT OF LABORATORY ANALYSIS
v1
v1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-1 Lab ID: 92688240001 Collected: 09/12/23 14:30 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Surrogates
2-Fluorophenol (S)
56
%
10-130
1
09/17/23 17:12
09/18/23 09:05
367-12-4
2,4,6-Tribromophenol (S)
76
%
10-131
1
09/17/23 17:12
09/18/23 09:05
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation Method: EPA
5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
107
34.4
1
09/15/23 20:55
09/16/23 03:48
67-64-1
Benzene
ND
ug/kg
5.4
2.1
1
09/15/23 20:55
09/16/23 03:48
71-43-2
Bromobenzene
ND
ug/kg
5.4
1.7
1
09/15/23 20:55
09/16/23 03:48
108-86-1
Bromochloromethane
ND
ug/kg
5.4
1.6
1
09/15/23 20:55
09/16/23 03:48
74-97-5
Bromodichloromethane
ND
ug/kg
5.4
2.1
1
09/15/23 20:55
09/16/23 03:48
75-27-4
Bromoform
ND
ug/kg
5.4
1.9
1
09/15/23 20:55
09/16/23 03:48
75-25-2
Bromomethane
ND
ug/kg
21.5
16.6
1
09/15/23 20:55
09/16/23 03:48
74-83-9
2-Butanone (MEK)
ND
ug/kg
107
25.8
1
09/15/23 20:55
09/16/23 03:48
78-93-3
n-Butylbenzene
ND
ug/kg
5.4
3.4
1
09/15/23 20:55
09/16/23 03:48
104-51-8
sec-Butylbenzene
ND
ug/kg
5.4
2.4
1
09/15/23 20:55
09/16/23 03:48
135-98-8
tert-Butyl benzene
ND
ug/kg
5.4
1.9
1
09/15/23 20:55
09/16/23 03:48
98-06-6
Carbon tetrachloride
ND
ug/kg
5.4
2.0
1
09/15/23 20:55
09/16/23 03:48
56-23-5
Chlorobenzene
ND
ug/kg
5.4
3.1
1
09/15/23 20:55
09/16/23 03:48
108-90-7
Chloroethane
ND
ug/kg
10.7
4.1
1
09/15/23 20:55
09/16/23 03:48
75-00-3
Chloroform
ND
ug/kg
5.4
4.5
1
09/15/23 20:55
09/16/23 03:48
67-66-3
Chloromethane
ND
ug/kg
10.7
4.5
1
09/15/23 20:55
09/16/23 03:48
74-87-3
2-Chlorotoluene
ND
ug/kg
5.4
1.9
1
09/15/23 20:55
09/16/23 03:48
95-49-8
4-Chlorotoluene
ND
ug/kg
5.4
3.0
1
09/15/23 20:55
09/16/23 03:48
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
5.4
2.1
1
09/15/23 20:55
09/16/23 03:48
96-12-8
Dibromochloromethane
ND
ug/kg
5.4
3.0
1
09/15/23 20:55
09/16/23 03:48
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
5.4
2.4
1
09/15/23 20:55
09/16/23 03:48
106-93-4
Dibromomethane
ND
ug/kg
5.4
1.1
1
09/15/23 20:55
09/16/23 03:48
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
5.4
1.9
1
09/15/23 20:55
09/16/23 03:48
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
5.4
1.7
1
09/15/23 20:55
09/16/23 03:48
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
5.4
1.4
1
09/15/23 20:55
09/16/23 03:48
106-46-7
Dichlorodifluoromethane
ND
ug/kg
10.7
5.5
1
09/15/23 20:55
09/16/23 03:48
75-71-8
1,1-Dichloroethane
ND
ug/kg
5.4
2.2
1
09/15/23 20:55
09/16/23 03:48
75-34-3
1,2-Dichloroethane
ND
ug/kg
5.4
3.6
1
09/15/23 20:55
09/16/23 03:48
107-06-2
1,1-Dichloroethene
ND
ug/kg
5.4
2.2
1
09/15/23 20:55
09/16/23 03:48
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
5.4
1.8
1
09/15/23 20:55
09/16/23 03:48
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
5.4
4.6
1
09/15/23 20:55
09/16/23 03:48
156-60-5
1,2-Dichloropropane
ND
ug/kg
5.4
1.6
1
09/15/23 20:55
09/16/23 03:48
78-87-5
1,3-Dichloropropane
ND
ug/kg
5.4
1.7
1
09/15/23 20:55
09/16/23 03:48
142-28-9
2,2-Dichloropropane
ND
ug/kg
5.4
4.1
1
09/15/23 20:55
09/16/23 03:48
594-20-7
1,1-Dichloropropene
ND
ug/kg
5.4
2.6
1
09/15/23 20:55
09/16/23 03:48
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
5.4
1.5
1
09/15/23 20:55
09/16/23 03:48
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
5.4
1.8
1
09/15/23 20:55
09/16/23 03:48
10061-02-6
REPORT OF LABORATORY ANALYSIS
L1,v1
IH,L1,
v1
L1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-1 Lab ID: 92688240001 Collected: 09/12/23 14:30 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Total Solids 2540 G-2011
Total Solids
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
ug/kg
5.4
1.4
1
09/15/23 20:55
09/16/23 03:48
108-20-3
ND
ug/kg
5.4
2.5
1
09/15/23 20:55
09/16/23 03:48
100-41-4
ND
ug/kg
10.7
8.8
1
09/15/23 20:55
09/16/23 03:48
87-68-3
ND
ug/kg
53.7
5.2
1
09/15/23 20:55
09/16/23 03:48
591-78-6
ND
ug/kg
5.4
1.8
1
09/15/23 20:55
09/16/23 03:48
98-82-8
ND
ug/kg
5.4
2.6
1
09/15/23 20:55
09/16/23 03:48
99-87-6
ND
ug/kg
21.5
14.7
1
09/15/23 20:55
09/16/23 03:48
75-09-2
ND
ug/kg
53.7
5.2
1
09/15/23 20:55
09/16/23 03:48
108-10-1
ND
ug/kg
5.4
2.0
1
09/15/23 20:55
09/16/23 03:48
1634-04-4
ND
ug/kg
5.4
2.8
1
09/15/23 20:55
09/16/23 03:48
91-20-3
ND
ug/kg
5.4
1.9
1
09/15/23 20:55
09/16/23 03:48
103-65-1
ND
ug/kg
5.4
1.4
1
09/15/23 20:55
09/16/23 03:48
100-42-5
ND
ug/kg
5.4
2.1
1
09/15/23 20:55
09/16/23 03:48
630-20-6
ND
ug/kg
5.4
1.4
1
09/15/23 20:55
09/16/23 03:48
79-34-5
ND
ug/kg
5.4
1.7
1
09/15/23 20:55
09/16/23 03:48
127-18-4
ND
ug/kg
5.4
3.7
1
09/15/23 20:55
09/16/23 03:48
108-88-3
ND
ug/kg
5.4
4.3
1
09/15/23 20:55
09/16/23 03:48
87-61-6
ND
ug/kg
5.4
4.5
1
09/15/23 20:55
09/16/23 03:48
120-82-1
ND
ug/kg
5.4
2.8
1
09/15/23 20:55
09/16/23 03:48
71-55-6
ND
ug/kg
5.4
1.8
1
09/15/23 20:55
09/16/23 03:48
79-00-5
ND
ug/kg
5.4
4.3
1
09/15/23 20:55
09/16/23 03:48
79-01-6
ND
ug/kg
5.4
3.0
1
09/15/23 20:55
09/16/23 03:48
75-69-4
ND
ug/kg
5.4
2.7
1
09/15/23 20:55
09/16/23 03:48
96-18-4
ND
ug/kg
5.4
3.2
1
09/15/23 20:55
09/16/23 03:48
95-63-6
ND
ug/kg
5.4
1.8
1
09/15/23 20:55
09/16/23 03:48
108-67-8
ND
ug/kg
53.7
11.0
1
09/15/23 20:55
09/16/23 03:48
108-05-4
ND
ug/kg
10.7
2.7
1
09/15/23 20:55
09/16/23 03:48
75-01-4
ND
ug/kg
10.7
3.1
1
09/15/23 20:55
09/16/23 03:48
1330-20-7
ND
ug/kg
10.7
3.7
1
09/15/23 20:55
09/16/23 03:48
179601-23-1
ND
ug/kg
5.4
2.4
1
09/15/23 20:55
09/16/23 03:48
95-47-6
101
%
70-130
1
09/15/23 20:55
09/16/23 03:48
2037-26-5
101
%
70-130
1
09/15/23 20:55
09/16/23 03:48
460-00-4
106
%
70-130
1
09/15/23 20:55
09/16/23 03:48
17060-07-0
Analytical Method: SW-846
Pace Analytical Services - Charlotte
7.2 % 0.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
88.6 %
09/15/23 17:39
1 09/21 /23 06:44 09/21 /23 06:52
REPORT OF LABORATORY ANALYSIS
I:/
v1
I0`a
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-1 Lab ID: 92688240001 Collected: 09/12/23 14:30 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Wet Chemistry 7199 Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Chromium, Hexavalent 0.579J mg/kg 1.13 0.288 1 09/21/23 12:45 09/22/23 10:41 18540-29-9 J
Date: 09/25/2023 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-2 Lab ID: 92688240002 Collected: 09/12/23 14:10 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical
Services
- Ormond Beach
Arsenic
0.98
mg/kg
0.65
0.32
1
09/22/2311:05
09/25/2311:15
7440-38-2
Barium
5.1
mg/kg
0.65
0.11
1
09/22/2311:05
09/25/2311:15
7440-39-3
Cadmium
0.038J
mg/kg
0.065
0.032
1
09/22/2311:05
09/25/2311:15
7440-43-9
Chromium
6.4
mg/kg
0.32
0.16
1
09/22/2311:05
09/25/2311:15
7440-47-3
Lead
3.4
mg/kg
0.65
0.32
1
09/22/2311:05
09/25/2311:15
7439-92-1
Selenium
ND
mg/kg
0.97
0.49
1
09/22/2311:05
09/25/2311:15
7782-49-2
Silver
ND
mg/kg
0.32
0.071
1
09/22/2311:05
09/25/2311:15
7440-22-4
7471 Mercury
Analytical
Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical
Services
- Ormond Beach
Mercury
0.023
mg/kg
0.0089
0.0045
1
09/21/2312:51
09/22/2310:06
7439-97-6
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation
Method: EPA
3546
Pace Analytical
Services
- Charlotte
Acenaphthene
ND
ug/kg
365
128
1
09/17/23 17:12
09/18/23 10:00
83-32-9
Acenaphthylene
ND
ug/kg
365
128
1
09/17/23 17:12
09/18/23 10:00
208-96-8
Aniline
ND
ug/kg
365
143
1
09/17/23 17:12
09/18/23 10:00
62-53-3
Anthracene
ND
ug/kg
365
119
1
09/17/23 17:12
09/18/23 10:00
120-12-7
Benzo(a)anthracene
ND
ug/kg
365
122
1
09/17/23 17:12
09/18/23 10:00
56-55-3
Benzo(a)pyrene
ND
ug/kg
365
126
1
09/17/23 17:12
09/18/23 10:00
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
365
122
1
09/17/23 17:12
09/18/23 10:00
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
365
142
1
09/17/23 17:12
09/18/23 10:00
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
365
128
1
09/17/23 17:12
09/18/23 10:00
207-08-9
Benzoic Acid
ND
ug/kg
1820
784
1
09/17/23 17:12
09/18/23 10:00
65-85-0
Benzyl alcohol
ND
ug/kg
730
276
1
09/17/23 17:12
09/18/23 10:00
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
365
140
1
09/17/23 17:12
09/18/23 10:00
101-55-3
Butylbenzylphthalate
ND
ug/kg
365
154
1
09/17/23 17:12
09/18/23 10:00
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
730
257
1
09/17/23 17:12
09/18/23 10:00
59-50-7
4-Chloroaniline
ND
ug/kg
730
286
1
09/17/23 17:12
09/18/23 10:00
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
365
152
1
09/17/23 17:12
09/18/23 10:00
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
365
137
1
09/17/23 17:12
09/18/23 10:00
111-44-4
2-Chloronaphthalene
ND
ug/kg
365
145
1
09/17/23 17:12
09/18/23 10:00
91-58-7
2-Chlorophenol
ND
ug/kg
365
137
1
09/17/23 17:12
09/18/23 10:00
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
365
136
1
09/17/23 17:12
09/18/23 10:00
7005-72-3
Chrysene
ND
ug/kg
365
133
1
09/17/23 17:12
09/18/23 10:00
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
365
140
1
09/17/23 17:12
09/18/23 10:00
53-70-3
Dibenzofuran
ND
ug/kg
365
132
1
09/17/23 17:12
09/18/23 10:00
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
365
132
1
09/17/23 17:12
09/18/23 10:00
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
365
129
1
09/17/23 17:12
09/18/23 10:00
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
365
139
1
09/17/23 17:12
09/18/23 10:00
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
730
247
1
09/17/23 17:12
09/18/23 10:00
91-94-1
2,4-Dichlorophenol
ND
ug/kg
365
143
1
09/17/23 17:12
09/18/23 10:00
120-83-2
Diethylphthalate
ND
ug/kg
365
134
1
09/17/23 17:12
09/18/23 10:00
84-66-2
2,4-Dimethylphenol
ND
ug/kg
365
152
1
09/17/23 17:12
09/18/23 10:00
105-67-9
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-2 Lab ID: 92688240002 Collected: 09/12/23 14:10 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Dimethylphthalate
ND
ug/kg
365
133
1
09/17/23 17:12
09/18/23 10:00
131-11-3
Di-n-butylphthalate
ND
ug/kg
365
123
1
09/17/23 17:12
09/18/23 10:00
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
730
341
1
09/17/23 17:12
09/18/23 10:00
534-52-1
2,4-Dinitrophenol
ND
ug/kg
1820
1130
1
09/17/23 17:12
09/18/23 10:00
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
365
140
1
09/17/23 17:12
09/18/23 10:00
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
365
134
1
09/17/23 17:12
09/18/23 10:00
606-20-2
Di-n-octylphthalate
ND
ug/kg
365
144
1
09/17/23 17:12
09/18/23 10:00
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
365
142
1
09/17/23 17:12
09/18/23 10:00
117-81-7
Fluoranthene
ND
ug/kg
365
125
1
09/17/23 17:12
09/18/23 10:00
206-44-0
Fluorene
ND
ug/kg
365
128
1
09/17/23 17:12
09/18/23 10:00
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
365
158
1
09/17/23 17:12
09/18/23 10:00
87-68-3
Hexachlorobenzene
ND
ug/kg
365
143
1
09/17/23 17:12
09/18/23 10:00
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
365
209
1
09/17/23 17:12
09/18/23 10:00
77-47-4
Hexachloroethane
ND
ug/kg
365
139
1
09/17/23 17:12
09/18/23 10:00
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
365
144
1
09/17/23 17:12
09/18/23 10:00
193-39-5
Isophorone
ND
ug/kg
365
163
1
09/17/23 17:12
09/18/23 10:00
78-59-1
1-Methylnaphthalene
ND
ug/kg
365
128
1
09/17/23 17:12
09/18/23 10:00
90-12-0
2-Methylnaphthalene
ND
ug/kg
365
146
1
09/17/23 17:12
09/18/23 10:00
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
365
149
1
09/17/23 17:12
09/18/23 10:00
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
365
147
1
09/17/23 17:12
09/18/23 10:00
15831-10-4
Naphthalene
ND
ug/kg
365
124
1
09/17/23 17:12
09/18/23 10:00
91-20-3
2-Nitroaniline
ND
ug/kg
1820
299
1
09/17/23 17:12
09/18/23 10:00
88-74-4
3-Nitroaniline
ND
ug/kg
1820
286
1
09/17/23 17:12
09/18/23 10:00
99-09-2
4-Nitroaniline
ND
ug/kg
730
278
1
09/17/23 17:12
09/18/23 10:00
100-01-6
Nitrobenzene
ND
ug/kg
365
169
1
09/17/23 17:12
09/18/23 10:00
98-95-3
2-Nitrophenol
ND
ug/kg
365
158
1
09/17/23 17:12
09/18/23 10:00
88-75-5
4-Nitrophenol
ND
ug/kg
1820
706
1
09/17/23 17:12
09/18/23 10:00
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
365
123
1
09/17/23 17:12
09/18/23 10:00
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
365
137
1
09/17/23 17:12
09/18/23 10:00
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
365
129
1
09/17/23 17:12
09/18/23 10:00
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
365
174
1
09/17/23 17:12
09/18/23 10:00
108-60-1
Pentachlorophenol
ND
ug/kg
730
357
1
09/17/23 17:12
09/18/23 10:00
87-86-5
Phenanthrene
ND
ug/kg
365
119
1
09/17/23 17:12
09/18/23 10:00
85-01-8
Phenol
ND
ug/kg
365
163
1
09/17/23 17:12
09/18/23 10:00
108-95-2
Pyrene
ND
ug/kg
365
148
1
09/17/23 17:12
09/18/23 10:00
129-00-0
Pyridine
ND
ug/kg
365
115
1
09/17/23 17:12
09/18/23 10:00
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
365
144
1
09/17/23 17:12
09/18/23 10:00
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
365
167
1
09/17/23 17:12
09/18/23 10:00
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
365
150
1
09/17/23 17:12
09/18/23 10:00
88-06-2
Surrogates
Nitrobenzene-d5 (S)
52
%
10-130
1
09/17/23 17:12
09/18/23 10:00
4165-60-0
2-Fluorobiphenyl (S)
46
%
10-130
1
09/17/23 17:12
09/18/23 10:00
321-60-8
Terphenyl-d14 (S)
70
%
10-130
1
09/17/23 17:12
09/18/23 10:00
1718-51-0
Phenol-d6 (S)
49
%
10-130
1
09/17/23 17:12
09/18/23 10:00
13127-88-3
REPORT OF LABORATORY ANALYSIS
v1
v1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-2 Lab ID: 92688240002 Collected: 09/12/23 14:10 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Surrogates
2-Fluorophenol (S)
48
%
10-130
1
09/17/23 17:12
09/18/23 10:00
367-12-4
2,4,6-Tribromophenol (S)
55
%
10-131
1
09/17/23 17:12
09/18/23 10:00
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation Method: EPA
5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
118
37.8
1
09/15/23 20:55
09/16/23 04:07
67-64-1
Benzene
ND
ug/kg
5.9
2.3
1
09/15/23 20:55
09/16/23 04:07
71-43-2
Bromobenzene
ND
ug/kg
5.9
1.9
1
09/15/23 20:55
09/16/23 04:07
108-86-1
Bromochloromethane
ND
ug/kg
5.9
1.7
1
09/15/23 20:55
09/16/23 04:07
74-97-5
Bromodichloromethane
ND
ug/kg
5.9
2.3
1
09/15/23 20:55
09/16/23 04:07
75-27-4
Bromoform
ND
ug/kg
5.9
2.1
1
09/15/23 20:55
09/16/23 04:07
75-25-2
Bromomethane
ND
ug/kg
23.6
18.3
1
09/15/23 20:55
09/16/23 04:07
74-83-9
2-Butanone (MEK)
ND
ug/kg
118
28.3
1
09/15/23 20:55
09/16/23 04:07
78-93-3
n-Butylbenzene
ND
ug/kg
5.9
3.7
1
09/15/23 20:55
09/16/23 04:07
104-51-8
sec-Butylbenzene
ND
ug/kg
5.9
2.6
1
09/15/23 20:55
09/16/23 04:07
135-98-8
tert-Butyl benzene
ND
ug/kg
5.9
2.1
1
09/15/23 20:55
09/16/23 04:07
98-06-6
Carbon tetrachloride
ND
ug/kg
5.9
2.2
1
09/15/23 20:55
09/16/23 04:07
56-23-5
Chlorobenzene
ND
ug/kg
5.9
3.4
1
09/15/23 20:55
09/16/23 04:07
108-90-7
Chloroethane
ND
ug/kg
11.8
4.5
1
09/15/23 20:55
09/16/23 04:07
75-00-3
Chloroform
ND
ug/kg
5.9
4.9
1
09/15/23 20:55
09/16/23 04:07
67-66-3
Chloromethane
ND
ug/kg
11.8
4.9
1
09/15/23 20:55
09/16/23 04:07
74-87-3
2-Chlorotoluene
ND
ug/kg
5.9
2.1
1
09/15/23 20:55
09/16/23 04:07
95-49-8
4-Chlorotoluene
ND
ug/kg
5.9
3.3
1
09/15/23 20:55
09/16/23 04:07
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
5.9
2.3
1
09/15/23 20:55
09/16/23 04:07
96-12-8
Dibromochloromethane
ND
ug/kg
5.9
3.3
1
09/15/23 20:55
09/16/23 04:07
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
5.9
2.6
1
09/15/23 20:55
09/16/23 04:07
106-93-4
Dibromomethane
ND
ug/kg
5.9
1.3
1
09/15/23 20:55
09/16/23 04:07
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
5.9
2.1
1
09/15/23 20:55
09/16/23 04:07
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
5.9
1.8
1
09/15/23 20:55
09/16/23 04:07
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
5.9
1.5
1
09/15/23 20:55
09/16/23 04:07
106-46-7
Dichlorodifluoromethane
ND
ug/kg
11.8
6.0
1
09/15/23 20:55
09/16/23 04:07
75-71-8
1,1-Dichloroethane
ND
ug/kg
5.9
2.4
1
09/15/23 20:55
09/16/23 04:07
75-34-3
1,2-Dichloroethane
ND
ug/kg
5.9
3.9
1
09/15/23 20:55
09/16/23 04:07
107-06-2
1,1-Dichloroethene
ND
ug/kg
5.9
2.4
1
09/15/23 20:55
09/16/23 04:07
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
5.9
2.0
1
09/15/23 20:55
09/16/23 04:07
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
5.9
5.0
1
09/15/23 20:55
09/16/23 04:07
156-60-5
1,2-Dichloropropane
ND
ug/kg
5.9
1.8
1
09/15/23 20:55
09/16/23 04:07
78-87-5
1,3-Dichloropropane
ND
ug/kg
5.9
1.8
1
09/15/23 20:55
09/16/23 04:07
142-28-9
2,2-Dichloropropane
ND
ug/kg
5.9
4.5
1
09/15/23 20:55
09/16/23 04:07
594-20-7
1,1-Dichloropropene
ND
ug/kg
5.9
2.8
1
09/15/23 20:55
09/16/23 04:07
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
5.9
1.6
1
09/15/23 20:55
09/16/23 04:07
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
5.9
2.0
1
09/15/23 20:55
09/16/23 04:07
10061-02-6
REPORT OF LABORATORY ANALYSIS
L1,v1
IH,L1,
v1
L1
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Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-2 Lab ID: 92688240002 Collected: 09/12/23 14:10 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Total Solids 2540 G-2011
Total Solids
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
ug/kg
5.9
1.6
1
09/15/23 20:55
09/16/23 04:07
108-20-3
ND
ug/kg
5.9
2.7
1
09/15/23 20:55
09/16/23 04:07
100-41-4
ND
ug/kg
11.8
9.6
1
09/15/23 20:55
09/16/23 04:07
87-68-3
ND
ug/kg
58.9
5.7
1
09/15/23 20:55
09/16/23 04:07
591-78-6
ND
ug/kg
5.9
2.0
1
09/15/23 20:55
09/16/23 04:07
98-82-8
ND
ug/kg
5.9
2.9
1
09/15/23 20:55
09/16/23 04:07
99-87-6
ND
ug/kg
23.6
16.1
1
09/15/23 20:55
09/16/23 04:07
75-09-2
ND
ug/kg
58.9
5.7
1
09/15/23 20:55
09/16/23 04:07
108-10-1
ND
ug/kg
5.9
2.2
1
09/15/23 20:55
09/16/23 04:07
1634-04-4
ND
ug/kg
5.9
3.1
1
09/15/23 20:55
09/16/23 04:07
91-20-3
ND
ug/kg
5.9
2.1
1
09/15/23 20:55
09/16/23 04:07
103-65-1
ND
ug/kg
5.9
1.6
1
09/15/23 20:55
09/16/23 04:07
100-42-5
ND
ug/kg
5.9
2.3
1
09/15/23 20:55
09/16/23 04:07
630-20-6
ND
ug/kg
5.9
1.6
1
09/15/23 20:55
09/16/23 04:07
79-34-5
ND
ug/kg
5.9
1.9
1
09/15/23 20:55
09/16/23 04:07
127-18-4
ND
ug/kg
5.9
4.1
1
09/15/23 20:55
09/16/23 04:07
108-88-3
ND
ug/kg
5.9
4.8
1
09/15/23 20:55
09/16/23 04:07
87-61-6
ND
ug/kg
5.9
4.9
1
09/15/23 20:55
09/16/23 04:07
120-82-1
ND
ug/kg
5.9
3.1
1
09/15/23 20:55
09/16/23 04:07
71-55-6
ND
ug/kg
5.9
2.0
1
09/15/23 20:55
09/16/23 04:07
79-00-5
ND
ug/kg
5.9
4.7
1
09/15/23 20:55
09/16/23 04:07
79-01-6
ND
ug/kg
5.9
3.2
1
09/15/23 20:55
09/16/23 04:07
75-69-4
ND
ug/kg
5.9
3.0
1
09/15/23 20:55
09/16/23 04:07
96-18-4
ND
ug/kg
5.9
3.5
1
09/15/23 20:55
09/16/23 04:07
95-63-6
ND
ug/kg
5.9
2.0
1
09/15/23 20:55
09/16/23 04:07
108-67-8
ND
ug/kg
58.9
12.1
1
09/15/23 20:55
09/16/23 04:07
108-05-4
ND
ug/kg
11.8
3.0
1
09/15/23 20:55
09/16/23 04:07
75-01-4
ND
ug/kg
11.8
3.4
1
09/15/23 20:55
09/16/23 04:07
1330-20-7
ND
ug/kg
11.8
4.0
1
09/15/23 20:55
09/16/23 04:07
179601-23-1
ND
ug/kg
5.9
2.6
1
09/15/23 20:55
09/16/23 04:07
95-47-6
102
%
70-130
1
09/15/23 20:55
09/16/23 04:07
2037-26-5
102
%
70-130
1
09/15/23 20:55
09/16/23 04:07
460-00-4
104
%
70-130
1
09/15/23 20:55
09/16/23 04:07
17060-07-0
Analytical Method: SW-846
Pace Analytical Services - Charlotte
8.0 % 0.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
90.7 %
09/15/23 17:39
1 09/21 /23 06:44 09/21 /23 06:52
REPORT OF LABORATORY ANALYSIS
I:/
v1
I0`a
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-2 Lab ID: 92688240002 Collected: 09/12/23 14:10 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Wet Chemistry 7199 Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Chromium, Hexavalent 0.940J mg/kg 1.10 0.281 1 09/21/23 12:45 09/22/23 10:51 18540-29-9 J
Date: 09/25/2023 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 16 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-3 Lab ID: 92688240003 Collected: 09/12/23 14:42 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical
Services
- Ormond Beach
Arsenic
0.55J
mg/kg
0.62
0.31
1
09/22/2311:05
09/25/2311:19
7440-38-2
Barium
4.6
mg/kg
0.62
0.10
1
09/22/2311:05
09/25/2311:19
7440-39-3
Cadmium
0.032J
mg/kg
0.062
0.031
1
09/22/2311:05
09/25/2311:19
7440-43-9
Chromium
5.2
mg/kg
0.31
0.16
1
09/22/2311:05
09/25/2311:19
7440-47-3
Lead
2.2
mg/kg
0.62
0.31
1
09/22/2311:05
09/25/2311:19
7439-92-1
Selenium
ND
mg/kg
0.93
0.47
1
09/22/2311:05
09/25/2311:19
7782-49-2
Silver
ND
mg/kg
0.31
0.068
1
09/22/2311:05
09/25/2311:19
7440-22-4
7471 Mercury
Analytical
Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical
Services
- Ormond Beach
Mercury
0.048
mg/kg
0.0073
0.0037
1
09/21/2312:51
09/22/2310:09
7439-97-6
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation
Method: EPA
3546
Pace Analytical
Services
- Charlotte
Acenaphthene
ND
ug/kg
360
126
1
09/17/23 17:12
09/18/23 10:28
83-32-9
Acenaphthylene
ND
ug/kg
360
126
1
09/17/23 17:12
09/18/23 10:28
208-96-8
Aniline
ND
ug/kg
360
141
1
09/17/23 17:12
09/18/23 10:28
62-53-3
Anthracene
ND
ug/kg
360
118
1
09/17/23 17:12
09/18/23 10:28
120-12-7
Benzo(a)anthracene
ND
ug/kg
360
120
1
09/17/23 17:12
09/18/23 10:28
56-55-3
Benzo(a)pyrene
ND
ug/kg
360
124
1
09/17/23 17:12
09/18/23 10:28
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
360
120
1
09/17/23 17:12
09/18/23 10:28
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
360
139
1
09/17/23 17:12
09/18/23 10:28
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
360
126
1
09/17/23 17:12
09/18/23 10:28
207-08-9
Benzoic Acid
ND
ug/kg
1800
772
1
09/17/23 17:12
09/18/23 10:28
65-85-0
Benzyl alcohol
ND
ug/kg
719
272
1
09/17/23 17:12
09/18/23 10:28
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
360
138
1
09/17/23 17:12
09/18/23 10:28
101-55-3
Butylbenzylphthalate
ND
ug/kg
360
151
1
09/17/23 17:12
09/18/23 10:28
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
719
253
1
09/17/23 17:12
09/18/23 10:28
59-50-7
4-Chloroaniline
ND
ug/kg
719
282
1
09/17/23 17:12
09/18/23 10:28
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
360
149
1
09/17/23 17:12
09/18/23 10:28
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
360
135
1
09/17/23 17:12
09/18/23 10:28
111-44-4
2-Chloronaphthalene
ND
ug/kg
360
143
1
09/17/23 17:12
09/18/23 10:28
91-58-7
2-Chlorophenol
ND
ug/kg
360
135
1
09/17/23 17:12
09/18/23 10:28
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
360
134
1
09/17/23 17:12
09/18/23 10:28
7005-72-3
Chrysene
ND
ug/kg
360
131
1
09/17/23 17:12
09/18/23 10:28
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
360
138
1
09/17/23 17:12
09/18/23 10:28
53-70-3
Dibenzofuran
ND
ug/kg
360
130
1
09/17/23 17:12
09/18/23 10:28
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
360
130
1
09/17/23 17:12
09/18/23 10:28
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
360
127
1
09/17/23 17:12
09/18/23 10:28
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
360
137
1
09/17/23 17:12
09/18/23 10:28
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
719
243
1
09/17/23 17:12
09/18/23 10:28
91-94-1
2,4-Dichlorophenol
ND
ug/kg
360
141
1
09/17/23 17:12
09/18/23 10:28
120-83-2
Diethylphthalate
ND
ug/kg
360
132
1
09/17/23 17:12
09/18/23 10:28
84-66-2
2,4-Dimethylphenol
ND
ug/kg
360
149
1
09/17/23 17:12
09/18/23 10:28
105-67-9
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-3 Lab ID: 92688240003 Collected: 09/12/23 14:42 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Dimethylphthalate
ND
ug/kg
360
131
1
09/17/23 17:12
09/18/23 10:28
131-11-3
Di-n-butylphthalate
ND
ug/kg
360
121
1
09/17/23 17:12
09/18/23 10:28
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
719
336
1
09/17/23 17:12
09/18/23 10:28
534-52-1
2,4-Dinitrophenol
ND
ug/kg
1800
1110
1
09/17/23 17:12
09/18/23 10:28
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
360
138
1
09/17/23 17:12
09/18/23 10:28
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
360
132
1
09/17/23 17:12
09/18/23 10:28
606-20-2
Di-n-octylphthalate
ND
ug/kg
360
142
1
09/17/23 17:12
09/18/23 10:28
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
360
139
1
09/17/23 17:12
09/18/23 10:28
117-81-7
Fluoranthene
ND
ug/kg
360
123
1
09/17/23 17:12
09/18/23 10:28
206-44-0
Fluorene
ND
ug/kg
360
126
1
09/17/23 17:12
09/18/23 10:28
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
360
156
1
09/17/23 17:12
09/18/23 10:28
87-68-3
Hexachlorobenzene
ND
ug/kg
360
141
1
09/17/23 17:12
09/18/23 10:28
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
360
206
1
09/17/23 17:12
09/18/23 10:28
77-47-4
Hexachloroethane
ND
ug/kg
360
137
1
09/17/23 17:12
09/18/23 10:28
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
360
142
1
09/17/23 17:12
09/18/23 10:28
193-39-5
Isophorone
ND
ug/kg
360
160
1
09/17/23 17:12
09/18/23 10:28
78-59-1
1-Methylnaphthalene
ND
ug/kg
360
126
1
09/17/23 17:12
09/18/23 10:28
90-12-0
2-Methylnaphthalene
ND
ug/kg
360
144
1
09/17/23 17:12
09/18/23 10:28
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
360
147
1
09/17/23 17:12
09/18/23 10:28
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
360
145
1
09/17/23 17:12
09/18/23 10:28
15831-10-4
Naphthalene
ND
ug/kg
360
122
1
09/17/23 17:12
09/18/23 10:28
91-20-3
2-Nitroaniline
ND
ug/kg
1800
294
1
09/17/23 17:12
09/18/23 10:28
88-74-4
3-Nitroaniline
ND
ug/kg
1800
282
1
09/17/23 17:12
09/18/23 10:28
99-09-2
4-Nitroaniline
ND
ug/kg
719
273
1
09/17/23 17:12
09/18/23 10:28
100-01-6
Nitrobenzene
ND
ug/kg
360
167
1
09/17/23 17:12
09/18/23 10:28
98-95-3
2-Nitrophenol
ND
ug/kg
360
156
1
09/17/23 17:12
09/18/23 10:28
88-75-5
4-Nitrophenol
ND
ug/kg
1800
695
1
09/17/23 17:12
09/18/23 10:28
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
360
121
1
09/17/23 17:12
09/18/23 10:28
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
360
135
1
09/17/23 17:12
09/18/23 10:28
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
360
127
1
09/17/23 17:12
09/18/23 10:28
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
360
171
1
09/17/23 17:12
09/18/23 10:28
108-60-1
Pentachlorophenol
ND
ug/kg
719
352
1
09/17/23 17:12
09/18/23 10:28
87-86-5
Phenanthrene
ND
ug/kg
360
118
1
09/17/23 17:12
09/18/23 10:28
85-01-8
Phenol
ND
ug/kg
360
160
1
09/17/23 17:12
09/18/23 10:28
108-95-2
Pyrene
ND
ug/kg
360
146
1
09/17/23 17:12
09/18/23 10:28
129-00-0
Pyridine
ND
ug/kg
360
113
1
09/17/23 17:12
09/18/23 10:28
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
360
142
1
09/17/23 17:12
09/18/23 10:28
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
360
164
1
09/17/23 17:12
09/18/23 10:28
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
360
148
1
09/17/23 17:12
09/18/23 10:28
88-06-2
Surrogates
Nitrobenzene-d5 (S)
57
%
10-130
1
09/17/23 17:12
09/18/23 10:28
4165-60-0
2-Fluorobiphenyl (S)
47
%
10-130
1
09/17/23 17:12
09/18/23 10:28
321-60-8
Terphenyl-d14 (S)
32
%
10-130
1
09/17/23 17:12
09/18/23 10:28
1718-51-0
Phenol-d6 (S)
59
%
10-130
1
09/17/23 17:12
09/18/23 10:28
13127-88-3
REPORT OF LABORATORY ANALYSIS
v1
v1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-3 Lab ID: 92688240003 Collected: 09/12/23 14:42 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Surrogates
2-Fluorophenol (S)
56
%
10-130
1
09/17/23 17:12
09/18/23 10:28
367-12-4
2,4,6-Tribromophenol (S)
54
%
10-131
1
09/17/23 17:12
09/18/23 10:28
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation Method: EPA
5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
109
35.0
1
09/15/23 20:55
09/16/23 04:25
67-64-1
Benzene
ND
ug/kg
5.4
2.2
1
09/15/23 20:55
09/16/23 04:25
71-43-2
Bromobenzene
ND
ug/kg
5.4
1.8
1
09/15/23 20:55
09/16/23 04:25
108-86-1
Bromochloromethane
ND
ug/kg
5.4
1.6
1
09/15/23 20:55
09/16/23 04:25
74-97-5
Bromodichloromethane
ND
ug/kg
5.4
2.1
1
09/15/23 20:55
09/16/23 04:25
75-27-4
Bromoform
ND
ug/kg
5.4
1.9
1
09/15/23 20:55
09/16/23 04:25
75-25-2
Bromomethane
ND
ug/kg
21.8
16.9
1
09/15/23 20:55
09/16/23 04:25
74-83-9
2-Butanone (MEK)
ND
ug/kg
109
26.1
1
09/15/23 20:55
09/16/23 04:25
78-93-3
n-Butylbenzene
ND
ug/kg
5.4
3.4
1
09/15/23 20:55
09/16/23 04:25
104-51-8
sec-Butylbenzene
ND
ug/kg
5.4
2.4
1
09/15/23 20:55
09/16/23 04:25
135-98-8
tert-Butyl benzene
ND
ug/kg
5.4
1.9
1
09/15/23 20:55
09/16/23 04:25
98-06-6
Carbon tetrachloride
ND
ug/kg
5.4
2.0
1
09/15/23 20:55
09/16/23 04:25
56-23-5
Chlorobenzene
ND
ug/kg
5.4
3.1
1
09/15/23 20:55
09/16/23 04:25
108-90-7
Chloroethane
ND
ug/kg
10.9
4.2
1
09/15/23 20:55
09/16/23 04:25
75-00-3
Chloroform
ND
ug/kg
5.4
4.6
1
09/15/23 20:55
09/16/23 04:25
67-66-3
Chloromethane
ND
ug/kg
10.9
4.6
1
09/15/23 20:55
09/16/23 04:25
74-87-3
2-Chlorotoluene
ND
ug/kg
5.4
1.9
1
09/15/23 20:55
09/16/23 04:25
95-49-8
4-Chlorotoluene
ND
ug/kg
5.4
3.0
1
09/15/23 20:55
09/16/23 04:25
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
5.4
2.1
1
09/15/23 20:55
09/16/23 04:25
96-12-8
Dibromochloromethane
ND
ug/kg
5.4
3.1
1
09/15/23 20:55
09/16/23 04:25
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
5.4
2.4
1
09/15/23 20:55
09/16/23 04:25
106-93-4
Dibromomethane
ND
ug/kg
5.4
1.2
1
09/15/23 20:55
09/16/23 04:25
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
5.4
2.0
1
09/15/23 20:55
09/16/23 04:25
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
5.4
1.7
1
09/15/23 20:55
09/16/23 04:25
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
5.4
1.4
1
09/15/23 20:55
09/16/23 04:25
106-46-7
Dichlorodifluoromethane
ND
ug/kg
10.9
5.5
1
09/15/23 20:55
09/16/23 04:25
75-71-8
1,1-Dichloroethane
ND
ug/kg
5.4
2.2
1
09/15/23 20:55
09/16/23 04:25
75-34-3
1,2-Dichloroethane
ND
ug/kg
5.4
3.6
1
09/15/23 20:55
09/16/23 04:25
107-06-2
1,1-Dichloroethene
ND
ug/kg
5.4
2.2
1
09/15/23 20:55
09/16/23 04:25
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
5.4
1.9
1
09/15/23 20:55
09/16/23 04:25
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
5.4
4.6
1
09/15/23 20:55
09/16/23 04:25
156-60-5
1,2-Dichloropropane
ND
ug/kg
5.4
1.6
1
09/15/23 20:55
09/16/23 04:25
78-87-5
1,3-Dichloropropane
ND
ug/kg
5.4
1.7
1
09/15/23 20:55
09/16/23 04:25
142-28-9
2,2-Dichloropropane
ND
ug/kg
5.4
4.1
1
09/15/23 20:55
09/16/23 04:25
594-20-7
1,1-Dichloropropene
ND
ug/kg
5.4
2.6
1
09/15/23 20:55
09/16/23 04:25
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
5.4
1.5
1
09/15/23 20:55
09/16/23 04:25
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
5.4
1.9
1
09/15/23 20:55
09/16/23 04:25
10061-02-6
REPORT OF LABORATORY ANALYSIS
L1,v1
IH,L1,
v1
L1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-3 Lab ID: 92688240003 Collected: 09/12/23 14:42 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Total Solids 2540 G-2011
Total Solids
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
ug/kg
5.4
1.5
1
09/15/23 20:55
09/16/23 04:25
108-20-3
ND
ug/kg
5.4
2.5
1
09/15/23 20:55
09/16/23 04:25
100-41-4
ND
ug/kg
10.9
8.9
1
09/15/23 20:55
09/16/23 04:25
87-68-3
ND
ug/kg
54.5
5.3
1
09/15/23 20:55
09/16/23 04:25
591-78-6
ND
ug/kg
5.4
1.9
1
09/15/23 20:55
09/16/23 04:25
98-82-8
ND
ug/kg
5.4
2.7
1
09/15/23 20:55
09/16/23 04:25
99-87-6
ND
ug/kg
21.8
14.9
1
09/15/23 20:55
09/16/23 04:25
75-09-2
ND
ug/kg
54.5
5.3
1
09/15/23 20:55
09/16/23 04:25
108-10-1
ND
ug/kg
5.4
2.0
1
09/15/23 20:55
09/16/23 04:25
1634-04-4
ND
ug/kg
5.4
2.9
1
09/15/23 20:55
09/16/23 04:25
91-20-3
ND
ug/kg
5.4
1.9
1
09/15/23 20:55
09/16/23 04:25
103-65-1
ND
ug/kg
5.4
1.4
1
09/15/23 20:55
09/16/23 04:25
100-42-5
ND
ug/kg
5.4
2.1
1
09/15/23 20:55
09/16/23 04:25
630-20-6
ND
ug/kg
5.4
1.4
1
09/15/23 20:55
09/16/23 04:25
79-34-5
ND
ug/kg
5.4
1.7
1
09/15/23 20:55
09/16/23 04:25
127-18-4
ND
ug/kg
5.4
3.8
1
09/15/23 20:55
09/16/23 04:25
108-88-3
ND
ug/kg
5.4
4.4
1
09/15/23 20:55
09/16/23 04:25
87-61-6
ND
ug/kg
5.4
4.6
1
09/15/23 20:55
09/16/23 04:25
120-82-1
ND
ug/kg
5.4
2.8
1
09/15/23 20:55
09/16/23 04:25
71-55-6
ND
ug/kg
5.4
1.8
1
09/15/23 20:55
09/16/23 04:25
79-00-5
ND
ug/kg
5.4
4.4
1
09/15/23 20:55
09/16/23 04:25
79-01-6
ND
ug/kg
5.4
3.0
1
09/15/23 20:55
09/16/23 04:25
75-69-4
ND
ug/kg
5.4
2.8
1
09/15/23 20:55
09/16/23 04:25
96-18-4
ND
ug/kg
5.4
3.2
1
09/15/23 20:55
09/16/23 04:25
95-63-6
ND
ug/kg
5.4
1.8
1
09/15/23 20:55
09/16/23 04:25
108-67-8
ND
ug/kg
54.5
11.2
1
09/15/23 20:55
09/16/23 04:25
108-05-4
ND
ug/kg
10.9
2.8
1
09/15/23 20:55
09/16/23 04:25
75-01-4
ND
ug/kg
10.9
3.1
1
09/15/23 20:55
09/16/23 04:25
1330-20-7
ND
ug/kg
10.9
3.7
1
09/15/23 20:55
09/16/23 04:25
179601-23-1
ND
ug/kg
5.4
2.4
1
09/15/23 20:55
09/16/23 04:25
95-47-6
101
%
70-130
1
09/15/23 20:55
09/16/23 04:25
2037-26-5
102
%
70-130
1
09/15/23 20:55
09/16/23 04:25
460-00-4
105
%
70-130
1
09/15/23 20:55
09/16/23 04:25
17060-07-0
Analytical Method: SW-846
Pace Analytical Services - Charlotte
8.5 % 0.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
90.4 %
09/15/23 17:39
1 09/21 /23 06:44 09/21 /23 06:52
REPORT OF LABORATORY ANALYSIS
I:/
v1
I0`a
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-3 Lab ID: 92688240003 Collected: 09/12/23 14:42 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Wet Chemistry 7199 Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Chromium, Hexavalent 0.532J mg/kg 1.11 0.282 1 09/21/23 12:45 09/22/23 10:56 18540-29-9 J,ML
Date: 09/25/2023 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 21 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-4 Lab ID: 92688240004 Collected: 09/12/23 16:44 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical
Services
- Ormond Beach
Arsenic
0.53J
mg/kg
0.64
0.32
1
09/22/2311:05
09/25/2311:22
7440-38-2
Barium
15.7
mg/kg
0.64
0.11
1
09/22/2311:05
09/25/2311:22
7440-39-3
Cadmium
0.049J
mg/kg
0.064
0.032
1
09/22/2311:05
09/25/2311:22
7440-43-9
Chromium
5.5
mg/kg
0.32
0.16
1
09/22/2311:05
09/25/2311:22
7440-47-3
Lead
4.0
mg/kg
0.64
0.32
1
09/22/2311:05
09/25/2311:22
7439-92-1
Selenium
ND
mg/kg
0.96
0.48
1
09/22/2311:05
09/25/2311:22
7782-49-2
Silver
ND
mg/kg
0.32
0.070
1
09/22/2311:05
09/25/2311:22
7440-22-4
7471 Mercury
Analytical
Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical
Services
- Ormond Beach
Mercury
0.021
mg/kg
0.0074
0.0037
1
09/21/2312:51
09/22/2310:11
7439-97-6
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation
Method: EPA
3546
Pace Analytical
Services
- Charlotte
Acenaphthene
ND
ug/kg
345
121
1
09/17/23 17:12
09/18/23 10:56
83-32-9
Acenaphthylene
ND
ug/kg
345
121
1
09/17/23 17:12
09/18/23 10:56
208-96-8
Aniline
ND
ug/kg
345
135
1
09/17/23 17:12
09/18/23 10:56
62-53-3
Anthracene
ND
ug/kg
345
113
1
09/17/23 17:12
09/18/23 10:56
120-12-7
Benzo(a)anthracene
ND
ug/kg
345
115
1
09/17/23 17:12
09/18/23 10:56
56-55-3
Benzo(a)pyrene
ND
ug/kg
345
119
1
09/17/23 17:12
09/18/23 10:56
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
345
115
1
09/17/23 17:12
09/18/23 10:56
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
345
134
1
09/17/23 17:12
09/18/23 10:56
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
345
121
1
09/17/23 17:12
09/18/23 10:56
207-08-9
Benzoic Acid
ND
ug/kg
1720
740
1
09/17/23 17:12
09/18/23 10:56
65-85-0
Benzyl alcohol
ND
ug/kg
689
261
1
09/17/23 17:12
09/18/23 10:56
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
345
133
1
09/17/23 17:12
09/18/23 10:56
101-55-3
Butylbenzylphthalate
ND
ug/kg
345
145
1
09/17/23 17:12
09/18/23 10:56
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
689
242
1
09/17/23 17:12
09/18/23 10:56
59-50-7
4-Chloroaniline
ND
ug/kg
689
270
1
09/17/23 17:12
09/18/23 10:56
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
345
143
1
09/17/23 17:12
09/18/23 10:56
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
345
129
1
09/17/23 17:12
09/18/23 10:56
111-44-4
2-Chloronaphthalene
ND
ug/kg
345
137
1
09/17/23 17:12
09/18/23 10:56
91-58-7
2-Chlorophenol
ND
ug/kg
345
129
1
09/17/23 17:12
09/18/23 10:56
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
345
128
1
09/17/23 17:12
09/18/23 10:56
7005-72-3
Chrysene
ND
ug/kg
345
125
1
09/17/23 17:12
09/18/23 10:56
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
345
133
1
09/17/23 17:12
09/18/23 10:56
53-70-3
Dibenzofuran
ND
ug/kg
345
124
1
09/17/23 17:12
09/18/23 10:56
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
345
124
1
09/17/23 17:12
09/18/23 10:56
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
345
122
1
09/17/23 17:12
09/18/23 10:56
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
345
132
1
09/17/23 17:12
09/18/23 10:56
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
689
233
1
09/17/23 17:12
09/18/23 10:56
91-94-1
2,4-Dichlorophenol
ND
ug/kg
345
135
1
09/17/23 17:12
09/18/23 10:56
120-83-2
Diethylphthalate
ND
ug/kg
345
126
1
09/17/23 17:12
09/18/23 10:56
84-66-2
2,4-Dimethylphenol
ND
ug/kg
345
143
1
09/17/23 17:12
09/18/23 10:56
105-67-9
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-4 Lab ID: 92688240004 Collected: 09/12/23 16:44 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Dimethylphthalate
ND
ug/kg
345
125
1
09/17/23 17:12
09/18/23 10:56
131-11-3
Di-n-butylphthalate
ND
ug/kg
345
116
1
09/17/23 17:12
09/18/23 10:56
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
689
322
1
09/17/23 17:12
09/18/23 10:56
534-52-1
2,4-Dinitrophenol
ND
ug/kg
1720
1060
1
09/17/23 17:12
09/18/23 10:56
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
345
133
1
09/17/23 17:12
09/18/23 10:56
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
345
126
1
09/17/23 17:12
09/18/23 10:56
606-20-2
Di-n-octylphthalate
ND
ug/kg
345
136
1
09/17/23 17:12
09/18/23 10:56
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
345
134
1
09/17/23 17:12
09/18/23 10:56
117-81-7
Fluoranthene
ND
ug/kg
345
118
1
09/17/23 17:12
09/18/23 10:56
206-44-0
Fluorene
ND
ug/kg
345
121
1
09/17/23 17:12
09/18/23 10:56
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
345
149
1
09/17/23 17:12
09/18/23 10:56
87-68-3
Hexachlorobenzene
ND
ug/kg
345
135
1
09/17/23 17:12
09/18/23 10:56
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
345
197
1
09/17/23 17:12
09/18/23 10:56
77-47-4
Hexachloroethane
ND
ug/kg
345
132
1
09/17/23 17:12
09/18/23 10:56
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
345
136
1
09/17/23 17:12
09/18/23 10:56
193-39-5
Isophorone
ND
ug/kg
345
153
1
09/17/23 17:12
09/18/23 10:56
78-59-1
1-Methylnaphthalene
ND
ug/kg
345
121
1
09/17/23 17:12
09/18/23 10:56
90-12-0
2-Methylnaphthalene
ND
ug/kg
345
138
1
09/17/23 17:12
09/18/23 10:56
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
345
141
1
09/17/23 17:12
09/18/23 10:56
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
345
139
1
09/17/23 17:12
09/18/23 10:56
15831-10-4
Naphthalene
ND
ug/kg
345
117
1
09/17/23 17:12
09/18/23 10:56
91-20-3
2-Nitroaniline
ND
ug/kg
1720
282
1
09/17/23 17:12
09/18/23 10:56
88-74-4
3-Nitroaniline
ND
ug/kg
1720
270
1
09/17/23 17:12
09/18/23 10:56
99-09-2
4-Nitroaniline
ND
ug/kg
689
262
1
09/17/23 17:12
09/18/23 10:56
100-01-6
Nitrobenzene
ND
ug/kg
345
160
1
09/17/23 17:12
09/18/23 10:56
98-95-3
2-Nitrophenol
ND
ug/kg
345
149
1
09/17/23 17:12
09/18/23 10:56
88-75-5
4-Nitrophenol
ND
ug/kg
1720
666
1
09/17/23 17:12
09/18/23 10:56
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
345
116
1
09/17/23 17:12
09/18/23 10:56
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
345
129
1
09/17/23 17:12
09/18/23 10:56
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
345
122
1
09/17/23 17:12
09/18/23 10:56
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
345
164
1
09/17/23 17:12
09/18/23 10:56
108-60-1
Pentachlorophenol
ND
ug/kg
689
337
1
09/17/23 17:12
09/18/23 10:56
87-86-5
Phenanthrene
ND
ug/kg
345
113
1
09/17/23 17:12
09/18/23 10:56
85-01-8
Phenol
ND
ug/kg
345
153
1
09/17/23 17:12
09/18/23 10:56
108-95-2
Pyrene
ND
ug/kg
345
140
1
09/17/23 17:12
09/18/23 10:56
129-00-0
Pyridine
ND
ug/kg
345
109
1
09/17/23 17:12
09/18/23 10:56
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
345
136
1
09/17/23 17:12
09/18/23 10:56
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
345
158
1
09/17/23 17:12
09/18/23 10:56
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
345
142
1
09/17/23 17:12
09/18/23 10:56
88-06-2
Surrogates
Nitrobenzene-d5 (S)
59
%
10-130
1
09/17/23 17:12
09/18/23 10:56
4165-60-0
2-Fluorobiphenyl (S)
52
%
10-130
1
09/17/23 17:12
09/18/23 10:56
321-60-8
Terphenyl-d14 (S)
69
%
10-130
1
09/17/23 17:12
09/18/23 10:56
1718-51-0
Phenol-d6 (S)
56
%
10-130
1
09/17/23 17:12
09/18/23 10:56
13127-88-3
REPORT OF LABORATORY ANALYSIS
v1
v1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-4 Lab ID: 92688240004 Collected: 09/12/23 16:44 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Surrogates
2-Fluorophenol (S)
53
%
10-130
1
09/17/23 17:12
09/18/23 10:56
367-12-4
2,4,6-Tribromophenol (S)
65
%
10-131
1
09/17/23 17:12
09/18/23 10:56
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation Method: EPA
5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
107
34.3
1
09/15/23 20:55
09/16/23 04:44
67-64-1
Benzene
4.1J
ug/kg
5.3
2.1
1
09/15/23 20:55
09/16/23 04:44
71-43-2
Bromobenzene
ND
ug/kg
5.3
1.7
1
09/15/23 20:55
09/16/23 04:44
108-86-1
Bromochloromethane
ND
ug/kg
5.3
1.6
1
09/15/23 20:55
09/16/23 04:44
74-97-5
Bromodichloromethane
ND
ug/kg
5.3
2.1
1
09/15/23 20:55
09/16/23 04:44
75-27-4
Bromoform
ND
ug/kg
5.3
1.9
1
09/15/23 20:55
09/16/23 04:44
75-25-2
Bromomethane
ND
ug/kg
21.4
16.6
1
09/15/23 20:55
09/16/23 04:44
74-83-9
2-Butanone (MEK)
ND
ug/kg
107
25.6
1
09/15/23 20:55
09/16/23 04:44
78-93-3
n-Butylbenzene
ND
ug/kg
5.3
3.4
1
09/15/23 20:55
09/16/23 04:44
104-51-8
sec-Butylbenzene
ND
ug/kg
5.3
2.4
1
09/15/23 20:55
09/16/23 04:44
135-98-8
tert-Butyl benzene
ND
ug/kg
5.3
1.9
1
09/15/23 20:55
09/16/23 04:44
98-06-6
Carbon tetrachloride
ND
ug/kg
5.3
2.0
1
09/15/23 20:55
09/16/23 04:44
56-23-5
Chlorobenzene
ND
ug/kg
5.3
3.1
1
09/15/23 20:55
09/16/23 04:44
108-90-7
Chloroethane
ND
ug/kg
10.7
4.1
1
09/15/23 20:55
09/16/23 04:44
75-00-3
Chloroform
ND
ug/kg
5.3
4.5
1
09/15/23 20:55
09/16/23 04:44
67-66-3
Chloromethane
ND
ug/kg
10.7
4.5
1
09/15/23 20:55
09/16/23 04:44
74-87-3
2-Chlorotoluene
ND
ug/kg
5.3
1.9
1
09/15/23 20:55
09/16/23 04:44
95-49-8
4-Chlorotoluene
ND
ug/kg
5.3
3.0
1
09/15/23 20:55
09/16/23 04:44
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
5.3
2.1
1
09/15/23 20:55
09/16/23 04:44
96-12-8
Dibromochloromethane
ND
ug/kg
5.3
3.0
1
09/15/23 20:55
09/16/23 04:44
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
5.3
2.4
1
09/15/23 20:55
09/16/23 04:44
106-93-4
Dibromomethane
ND
ug/kg
5.3
1.1
1
09/15/23 20:55
09/16/23 04:44
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
5.3
1.9
1
09/15/23 20:55
09/16/23 04:44
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
5.3
1.7
1
09/15/23 20:55
09/16/23 04:44
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
5.3
1.4
1
09/15/23 20:55
09/16/23 04:44
106-46-7
Dichlorodifluoromethane
ND
ug/kg
10.7
5.4
1
09/15/23 20:55
09/16/23 04:44
75-71-8
1,1-Dichloroethane
ND
ug/kg
5.3
2.2
1
09/15/23 20:55
09/16/23 04:44
75-34-3
1,2-Dichloroethane
ND
ug/kg
5.3
3.5
1
09/15/23 20:55
09/16/23 04:44
107-06-2
1,1-Dichloroethene
ND
ug/kg
5.3
2.2
1
09/15/23 20:55
09/16/23 04:44
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
5.3
1.8
1
09/15/23 20:55
09/16/23 04:44
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
5.3
4.5
1
09/15/23 20:55
09/16/23 04:44
156-60-5
1,2-Dichloropropane
ND
ug/kg
5.3
1.6
1
09/15/23 20:55
09/16/23 04:44
78-87-5
1,3-Dichloropropane
ND
ug/kg
5.3
1.7
1
09/15/23 20:55
09/16/23 04:44
142-28-9
2,2-Dichloropropane
ND
ug/kg
5.3
4.1
1
09/15/23 20:55
09/16/23 04:44
594-20-7
1,1-Dichloropropene
ND
ug/kg
5.3
2.6
1
09/15/23 20:55
09/16/23 04:44
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
5.3
1.5
1
09/15/23 20:55
09/16/23 04:44
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
5.3
1.8
1
09/15/23 20:55
09/16/23 04:44
10061-02-6
REPORT OF LABORATORY ANALYSIS
L1,v1
IH,L1,
v1
L1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-4 Lab ID: 92688240004 Collected: 09/12/23 16:44 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Total Solids 2540 G-2011
Total Solids
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
ug/kg
5.3
1.4
1
09/15/23 20:55
09/16/23 04:44
108-20-3
7.3
ug/kg
5.3
2.5
1
09/15/23 20:55
09/16/23 04:44
100-41-4
ND
ug/kg
10.7
8.7
1
09/15/23 20:55
09/16/23 04:44
87-68-3
ND
ug/kg
53.4
5.2
1
09/15/23 20:55
09/16/23 04:44
591-78-6
ND
ug/kg
5.3
1.8
1
09/15/23 20:55
09/16/23 04:44
98-82-8
ND
ug/kg
5.3
2.6
1
09/15/23 20:55
09/16/23 04:44
99-87-6
ND
ug/kg
21.4
14.6
1
09/15/23 20:55
09/16/23 04:44
75-09-2
ND
ug/kg
53.4
5.2
1
09/15/23 20:55
09/16/23 04:44
108-10-1
ND
ug/kg
5.3
2.0
1
09/15/23 20:55
09/16/23 04:44
1634-04-4
ND
ug/kg
5.3
2.8
1
09/15/23 20:55
09/16/23 04:44
91-20-3
ND
ug/kg
5.3
1.9
1
09/15/23 20:55
09/16/23 04:44
103-65-1
ND
ug/kg
5.3
1.4
1
09/15/23 20:55
09/16/23 04:44
100-42-5
ND
ug/kg
5.3
2.1
1
09/15/23 20:55
09/16/23 04:44
630-20-6
ND
ug/kg
5.3
1.4
1
09/15/23 20:55
09/16/23 04:44
79-34-5
ND
ug/kg
5.3
1.7
1
09/15/23 20:55
09/16/23 04:44
127-18-4
27.6
ug/kg
5.3
3.7
1
09/15/23 20:55
09/16/23 04:44
108-88-3
ND
ug/kg
5.3
4.3
1
09/15/23 20:55
09/16/23 04:44
87-61-6
ND
ug/kg
5.3
4.5
1
09/15/23 20:55
09/16/23 04:44
120-82-1
ND
ug/kg
5.3
2.8
1
09/15/23 20:55
09/16/23 04:44
71-55-6
ND
ug/kg
5.3
1.8
1
09/15/23 20:55
09/16/23 04:44
79-00-5
ND
ug/kg
5.3
4.3
1
09/15/23 20:55
09/16/23 04:44
79-01-6
ND
ug/kg
5.3
2.9
1
09/15/23 20:55
09/16/23 04:44
75-69-4
ND
ug/kg
5.3
2.7
1
09/15/23 20:55
09/16/23 04:44
96-18-4
6.5
ug/kg
5.3
3.2
1
09/15/23 20:55
09/16/23 04:44
95-63-6
ND
ug/kg
5.3
1.8
1
09/15/23 20:55
09/16/23 04:44
108-67-8
ND
ug/kg
53.4
11.0
1
09/15/23 20:55
09/16/23 04:44
108-05-4
ND
ug/kg
10.7
2.7
1
09/15/23 20:55
09/16/23 04:44
75-01-4
27.4
ug/kg
10.7
3.0
1
09/15/23 20:55
09/16/23 04:44
1330-20-7
20.9
ug/kg
10.7
3.7
1
09/15/23 20:55
09/16/23 04:44
179601-23-1
6.5
ug/kg
5.3
2.4
1
09/15/23 20:55
09/16/23 04:44
95-47-6
101
%
70-130
1
09/15/23 20:55
09/16/23 04:44
2037-26-5
102
%
70-130
1
09/15/23 20:55
09/16/23 04:44
460-00-4
104
%
70-130
1
09/15/23 20:55
09/16/23 04:44
17060-07-0
Analytical Method: SW-846
Pace Analytical Services - Charlotte
5.8 % 0.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
84.9 %
09/15/23 17:39
1 09/21 /23 06:36 09/21 /23 06:42
REPORT OF LABORATORY ANALYSIS
I:/
v1
I0`a
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-4 Lab ID: 92688240004 Collected: 09/12/23 16:44 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Wet Chemistry 7199 Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Chromium, Hexavalent 0.402J mg/kg 1.18 0.300 1 09/21/23 12:45 09/22/23 12:31 18540-29-9 J
Date: 09/25/2023 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 26 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-5 Lab ID: 92688240005 Collected: 09/12/23 16:18 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical
Services
- Ormond Beach
Arsenic
0.77
mg/kg
0.58
0.29
1
09/22/2311:05
09/25/2311:25
7440-38-2
Barium
16.5
mg/kg
0.58
0.097
1
09/22/2311:05
09/25/2311:25
7440-39-3
Cadmium
0.062
mg/kg
0.058
0.029
1
09/22/2311:05
09/25/2311:25
7440-43-9
Chromium
6.1
mg/kg
0.29
0.14
1
09/22/2311:05
09/25/2311:25
7440-47-3
Lead
4.2
mg/kg
0.58
0.29
1
09/22/2311:05
09/25/2311:25
7439-92-1
Selenium
ND
mg/kg
0.87
0.43
1
09/22/2311:05
09/25/2311:25
7782-49-2
Silver
ND
mg/kg
0.29
0.064
1
09/22/2311:05
09/25/2311:25
7440-22-4
7471 Mercury
Analytical
Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical
Services
- Ormond Beach
Mercury
0.031
mg/kg
0.0074
0.0037
1
09/21/2312:51
09/22/2310:13
7439-97-6
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation
Method: EPA
3546
Pace Analytical
Services
- Charlotte
Acenaphthene
ND
ug/kg
352
124
1
09/17/23 17:12
09/18/23 11:24
83-32-9
Acenaphthylene
ND
ug/kg
352
124
1
09/17/23 17:12
09/18/23 11:24
208-96-8
Aniline
ND
ug/kg
352
138
1
09/17/23 17:12
09/18/23 11:24
62-53-3
Anthracene
ND
ug/kg
352
115
1
09/17/23 17:12
09/18/23 11:24
120-12-7
Benzo(a)anthracene
ND
ug/kg
352
117
1
09/17/23 17:12
09/18/23 11:24
56-55-3
Benzo(a)pyrene
ND
ug/kg
352
122
1
09/17/23 17:12
09/18/23 11:24
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
352
117
1
09/17/23 17:12
09/18/23 11:24
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
352
137
1
09/17/23 17:12
09/18/23 11:24
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
352
124
1
09/17/23 17:12
09/18/23 11:24
207-08-9
Benzoic Acid
ND
ug/kg
1760
756
1
09/17/23 17:12
09/18/23 11:24
65-85-0
Benzyl alcohol
ND
ug/kg
704
267
1
09/17/23 17:12
09/18/23 11:24
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
352
135
1
09/17/23 17:12
09/18/23 11:24
101-55-3
Butylbenzylphthalate
ND
ug/kg
352
148
1
09/17/23 17:12
09/18/23 11:24
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
704
248
1
09/17/23 17:12
09/18/23 11:24
59-50-7
4-Chloroaniline
ND
ug/kg
704
276
1
09/17/23 17:12
09/18/23 11:24
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
352
146
1
09/17/23 17:12
09/18/23 11:24
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
352
132
1
09/17/23 17:12
09/18/23 11:24
111-44-4
2-Chloronaphthalene
ND
ug/kg
352
140
1
09/17/23 17:12
09/18/23 11:24
91-58-7
2-Chlorophenol
ND
ug/kg
352
132
1
09/17/23 17:12
09/18/23 11:24
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
352
131
1
09/17/23 17:12
09/18/23 11:24
7005-72-3
Chrysene
ND
ug/kg
352
128
1
09/17/23 17:12
09/18/23 11:24
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
352
135
1
09/17/23 17:12
09/18/23 11:24
53-70-3
Dibenzofuran
ND
ug/kg
352
127
1
09/17/23 17:12
09/18/23 11:24
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
352
127
1
09/17/23 17:12
09/18/23 11:24
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
352
125
1
09/17/23 17:12
09/18/23 11:24
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
352
134
1
09/17/23 17:12
09/18/23 11:24
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
704
238
1
09/17/23 17:12
09/18/23 11:24
91-94-1
2,4-Dichlorophenol
ND
ug/kg
352
138
1
09/17/23 17:12
09/18/23 11:24
120-83-2
Diethylphthalate
ND
ug/kg
352
129
1
09/17/23 17:12
09/18/23 11:24
84-66-2
2,4-Dimethylphenol
ND
ug/kg
352
146
1
09/17/23 17:12
09/18/23 11:24
105-67-9
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-5 Lab ID: 92688240005 Collected: 09/12/23 16:18 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Dimethylphthalate
ND
ug/kg
352
128
1
09/17/23 17:12
09/18/23 11:24
131-11-3
Di-n-butylphthalate
ND
ug/kg
352
118
1
09/17/23 17:12
09/18/23 11:24
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
704
329
1
09/17/23 17:12
09/18/23 11:24
534-52-1
2,4-Dinitrophenol
ND
ug/kg
1760
1090
1
09/17/23 17:12
09/18/23 11:24
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
352
135
1
09/17/23 17:12
09/18/23 11:24
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
352
129
1
09/17/23 17:12
09/18/23 11:24
606-20-2
Di-n-octylphthalate
ND
ug/kg
352
139
1
09/17/23 17:12
09/18/23 11:24
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
352
137
1
09/17/23 17:12
09/18/23 11:24
117-81-7
Fluoranthene
ND
ug/kg
352
121
1
09/17/23 17:12
09/18/23 11:24
206-44-0
Fluorene
ND
ug/kg
352
124
1
09/17/23 17:12
09/18/23 11:24
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
352
153
1
09/17/23 17:12
09/18/23 11:24
87-68-3
Hexachlorobenzene
ND
ug/kg
352
138
1
09/17/23 17:12
09/18/23 11:24
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
352
202
1
09/17/23 17:12
09/18/23 11:24
77-47-4
Hexachloroethane
ND
ug/kg
352
134
1
09/17/23 17:12
09/18/23 11:24
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
352
139
1
09/17/23 17:12
09/18/23 11:24
193-39-5
Isophorone
ND
ug/kg
352
157
1
09/17/23 17:12
09/18/23 11:24
78-59-1
1-Methylnaphthalene
ND
ug/kg
352
124
1
09/17/23 17:12
09/18/23 11:24
90-12-0
2-Methylnaphthalene
ND
ug/kg
352
141
1
09/17/23 17:12
09/18/23 11:24
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
352
144
1
09/17/23 17:12
09/18/23 11:24
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
352
142
1
09/17/23 17:12
09/18/23 11:24
15831-10-4
Naphthalene
ND
ug/kg
352
119
1
09/17/23 17:12
09/18/23 11:24
91-20-3
2-Nitroaniline
ND
ug/kg
1760
288
1
09/17/23 17:12
09/18/23 11:24
88-74-4
3-Nitroaniline
ND
ug/kg
1760
276
1
09/17/23 17:12
09/18/23 11:24
99-09-2
4-Nitroaniline
ND
ug/kg
704
268
1
09/17/23 17:12
09/18/23 11:24
100-01-6
Nitrobenzene
ND
ug/kg
352
163
1
09/17/23 17:12
09/18/23 11:24
98-95-3
2-Nitrophenol
ND
ug/kg
352
153
1
09/17/23 17:12
09/18/23 11:24
88-75-5
4-Nitrophenol
ND
ug/kg
1760
681
1
09/17/23 17:12
09/18/23 11:24
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
352
118
1
09/17/23 17:12
09/18/23 11:24
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
352
132
1
09/17/23 17:12
09/18/23 11:24
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
352
125
1
09/17/23 17:12
09/18/23 11:24
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
352
167
1
09/17/23 17:12
09/18/23 11:24
108-60-1
Pentachlorophenol
ND
ug/kg
704
345
1
09/17/23 17:12
09/18/23 11:24
87-86-5
Phenanthrene
ND
ug/kg
352
115
1
09/17/23 17:12
09/18/23 11:24
85-01-8
Phenol
ND
ug/kg
352
157
1
09/17/23 17:12
09/18/23 11:24
108-95-2
Pyrene
ND
ug/kg
352
143
1
09/17/23 17:12
09/18/23 11:24
129-00-0
Pyridine
ND
ug/kg
352
ill
1
09/17/23 17:12
09/18/23 11:24
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
352
139
1
09/17/23 17:12
09/18/23 11:24
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
352
161
1
09/17/23 17:12
09/18/23 11:24
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
352
145
1
09/17/23 17:12
09/18/23 11:24
88-06-2
Surrogates
Nitrobenzene-d5 (S)
62
%
10-130
1
09/17/23 17:12
09/18/23 11:24
4165-60-0
2-Fluorobiphenyl (S)
59
%
10-130
1
09/17/23 17:12
09/18/23 11:24
321-60-8
Terphenyl-dl4 (S)
74
%
10-130
1
09/17/23 17:12
09/18/23 11:24
1718-51-0
Phenol-d6 (S)
59
%
10-130
1
09/17/23 17:12
09/18/23 11:24
13127-88-3
REPORT OF LABORATORY ANALYSIS
vl
vl
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-5 Lab ID: 92688240005 Collected: 09/12/23 16:18 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Surrogates
2-Fluorophenol (S)
56
%
10-130
1
09/17/23 17:12
09/18/23 11:24
367-12-4
2,4,6-Tribromophenol (S)
71
%
10-131
1
09/17/23 17:12
09/18/23 11:24
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation Method: EPA
5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
127
40.7
1
09/15/23 20:55
09/16/23 05:03
67-64-1
Benzene
ND
ug/kg
6.3
2.5
1
09/15/23 20:55
09/16/23 05:03
71-43-2
Bromobenzene
ND
ug/kg
6.3
2.1
1
09/15/23 20:55
09/16/23 05:03
108-86-1
Bromochloromethane
ND
ug/kg
6.3
1.9
1
09/15/23 20:55
09/16/23 05:03
74-97-5
Bromodichloromethane
ND
ug/kg
6.3
2.4
1
09/15/23 20:55
09/16/23 05:03
75-27-4
Bromoform
ND
ug/kg
6.3
2.2
1
09/15/23 20:55
09/16/23 05:03
75-25-2
Bromomethane
ND
ug/kg
25.4
19.7
1
09/15/23 20:55
09/16/23 05:03
74-83-9
2-Butanone (MEK)
ND
ug/kg
127
30.4
1
09/15/23 20:55
09/16/23 05:03
78-93-3
n-Butylbenzene
ND
ug/kg
6.3
4.0
1
09/15/23 20:55
09/16/23 05:03
104-51-8
sec-Butylbenzene
ND
ug/kg
6.3
2.8
1
09/15/23 20:55
09/16/23 05:03
135-98-8
tert-Butyl benzene
ND
ug/kg
6.3
2.3
1
09/15/23 20:55
09/16/23 05:03
98-06-6
Carbon tetrachloride
ND
ug/kg
6.3
2.4
1
09/15/23 20:55
09/16/23 05:03
56-23-5
Chlorobenzene
ND
ug/kg
6.3
3.6
1
09/15/23 20:55
09/16/23 05:03
108-90-7
Chloroethane
ND
ug/kg
12.7
4.9
1
09/15/23 20:55
09/16/23 05:03
75-00-3
Chloroform
ND
ug/kg
6.3
5.3
1
09/15/23 20:55
09/16/23 05:03
67-66-3
Chloromethane
ND
ug/kg
12.7
5.3
1
09/15/23 20:55
09/16/23 05:03
74-87-3
2-Chlorotoluene
ND
ug/kg
6.3
2.2
1
09/15/23 20:55
09/16/23 05:03
95-49-8
4-Chlorotoluene
ND
ug/kg
6.3
3.5
1
09/15/23 20:55
09/16/23 05:03
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
6.3
2.5
1
09/15/23 20:55
09/16/23 05:03
96-12-8
Dibromochloromethane
ND
ug/kg
6.3
3.6
1
09/15/23 20:55
09/16/23 05:03
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
6.3
2.8
1
09/15/23 20:55
09/16/23 05:03
106-93-4
Dibromomethane
ND
ug/kg
6.3
1.4
1
09/15/23 20:55
09/16/23 05:03
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
6.3
2.3
1
09/15/23 20:55
09/16/23 05:03
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
6.3
2.0
1
09/15/23 20:55
09/16/23 05:03
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
6.3
1.6
1
09/15/23 20:55
09/16/23 05:03
106-46-7
Dichlorodifluoromethane
ND
ug/kg
12.7
6.5
1
09/15/23 20:55
09/16/23 05:03
75-71-8
1,1-Dichloroethane
ND
ug/kg
6.3
2.6
1
09/15/23 20:55
09/16/23 05:03
75-34-3
1,2-Dichloroethane
ND
ug/kg
6.3
4.2
1
09/15/23 20:55
09/16/23 05:03
107-06-2
1,1-Dichloroethene
ND
ug/kg
6.3
2.6
1
09/15/23 20:55
09/16/23 05:03
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
6.3
2.2
1
09/15/23 20:55
09/16/23 05:03
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
6.3
5.4
1
09/15/23 20:55
09/16/23 05:03
156-60-5
1,2-Dichloropropane
ND
ug/kg
6.3
1.9
1
09/15/23 20:55
09/16/23 05:03
78-87-5
1,3-Dichloropropane
ND
ug/kg
6.3
2.0
1
09/15/23 20:55
09/16/23 05:03
142-28-9
2,2-Dichloropropane
ND
ug/kg
6.3
4.8
1
09/15/23 20:55
09/16/23 05:03
594-20-7
1,1-Dichloropropene
ND
ug/kg
6.3
3.0
1
09/15/23 20:55
09/16/23 05:03
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
6.3
1.7
1
09/15/23 20:55
09/16/23 05:03
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
6.3
2.2
1
09/15/23 20:55
09/16/23 05:03
10061-02-6
REPORT OF LABORATORY ANALYSIS
L1,v1
IH,L1,
v1
L1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-5 Lab ID: 92688240005 Collected: 09/12/23 16:18 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Total Solids 2540 G-2011
Total Solids
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
ug/kg
6.3
1.7
1
09/15/23 20:55
09/16/23 05:03
108-20-3
ND
ug/kg
6.3
3.0
1
09/15/23 20:55
09/16/23 05:03
100-41-4
ND
ug/kg
12.7
10.4
1
09/15/23 20:55
09/16/23 05:03
87-68-3
ND
ug/kg
63.4
6.1
1
09/15/23 20:55
09/16/23 05:03
591-78-6
ND
ug/kg
6.3
2.2
1
09/15/23 20:55
09/16/23 05:03
98-82-8
ND
ug/kg
6.3
3.1
1
09/15/23 20:55
09/16/23 05:03
99-87-6
ND
ug/kg
25.4
17.4
1
09/15/23 20:55
09/16/23 05:03
75-09-2
ND
ug/kg
63.4
6.1
1
09/15/23 20:55
09/16/23 05:03
108-10-1
ND
ug/kg
6.3
2.4
1
09/15/23 20:55
09/16/23 05:03
1634-04-4
ND
ug/kg
6.3
3.3
1
09/15/23 20:55
09/16/23 05:03
91-20-3
ND
ug/kg
6.3
2.3
1
09/15/23 20:55
09/16/23 05:03
103-65-1
ND
ug/kg
6.3
1.7
1
09/15/23 20:55
09/16/23 05:03
100-42-5
ND
ug/kg
6.3
2.4
1
09/15/23 20:55
09/16/23 05:03
630-20-6
ND
ug/kg
6.3
1.7
1
09/15/23 20:55
09/16/23 05:03
79-34-5
ND
ug/kg
6.3
2.0
1
09/15/23 20:55
09/16/23 05:03
127-18-4
ND
ug/kg
6.3
4.4
1
09/15/23 20:55
09/16/23 05:03
108-88-3
ND
ug/kg
6.3
5.1
1
09/15/23 20:55
09/16/23 05:03
87-61-6
ND
ug/kg
6.3
5.3
1
09/15/23 20:55
09/16/23 05:03
120-82-1
ND
ug/kg
6.3
3.3
1
09/15/23 20:55
09/16/23 05:03
71-55-6
ND
ug/kg
6.3
2.1
1
09/15/23 20:55
09/16/23 05:03
79-00-5
ND
ug/kg
6.3
5.1
1
09/15/23 20:55
09/16/23 05:03
79-01-6
ND
ug/kg
6.3
3.5
1
09/15/23 20:55
09/16/23 05:03
75-69-4
ND
ug/kg
6.3
3.2
1
09/15/23 20:55
09/16/23 05:03
96-18-4
ND
ug/kg
6.3
3.8
1
09/15/23 20:55
09/16/23 05:03
95-63-6
ND
ug/kg
6.3
2.1
1
09/15/23 20:55
09/16/23 05:03
108-67-8
ND
ug/kg
63.4
13.1
1
09/15/23 20:55
09/16/23 05:03
108-05-4
ND
ug/kg
12.7
3.2
1
09/15/23 20:55
09/16/23 05:03
75-01-4
ND
ug/kg
12.7
3.6
1
09/15/23 20:55
09/16/23 05:03
1330-20-7
ND
ug/kg
12.7
4.3
1
09/15/23 20:55
09/16/23 05:03
179601-23-1
ND
ug/kg
6.3
2.8
1
09/15/23 20:55
09/16/23 05:03
95-47-6
103
%
70-130
1
09/15/23 20:55
09/16/23 05:03
2037-26-5
101
%
70-130
1
09/15/23 20:55
09/16/23 05:03
460-00-4
104
%
70-130
1
09/15/23 20:55
09/16/23 05:03
17060-07-0
Analytical Method: SW-846
Pace Analytical Services - Charlotte
6.9 % 0.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
90.7 %
09/15/23 17:39
1 09/21 /23 06:36 09/21 /23 06:42
REPORT OF LABORATORY ANALYSIS
I:/
v1
I0`a
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-5 Lab ID: 92688240005 Collected: 09/12/23 16:18 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Wet Chemistry 7199 Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Chromium, Hexavalent 0.652J mg/kg 1.10 0.281 1 09/21/23 12:45 09/22/23 12:39 18540-29-9 J
Date: 09/25/2023 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 31 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-6 Lab ID: 92688240006 Collected: 09/12/23 14:56 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical
Services
- Ormond Beach
Arsenic
ND
mg/kg
0.61
0.31
1
09/22/2311:05
09/25/2311:29
7440-38-2
Barium
30.3
mg/kg
0.61
0.10
1
09/22/2311:05
09/25/2311:29
7440-39-3
Cadmium
0.089
mg/kg
0.061
0.031
1
09/22/2311:05
09/25/2311:29
7440-43-9
Chromium
7.3
mg/kg
0.31
0.15
1
09/22/2311:05
09/25/2311:29
7440-47-3
Lead
6.1
mg/kg
0.61
0.31
1
09/22/2311:05
09/25/2311:29
7439-92-1
Selenium
ND
mg/kg
0.92
0.46
1
09/22/2311:05
09/25/2311:29
7782-49-2
Silver
ND
mg/kg
0.31
0.067
1
09/22/2311:05
09/25/2311:29
7440-22-4
7471 Mercury
Analytical
Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical
Services
- Ormond Beach
Mercury
0.036
mg/kg
0.0097
0.0049
1
09/21/2312:51
09/22/2310:16
7439-97-6
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation
Method: EPA
3546
Pace Analytical
Services
- Charlotte
Acenaphthene
ND
ug/kg
362
127
1
09/17/23 17:12
09/18/23 11:52
83-32-9
Acenaphthylene
ND
ug/kg
362
127
1
09/17/23 17:12
09/18/23 11:52
208-96-8
Aniline
ND
ug/kg
362
142
1
09/17/23 17:12
09/18/23 11:52
62-53-3
Anthracene
ND
ug/kg
362
119
1
09/17/23 17:12
09/18/23 11:52
120-12-7
Benzo(a)anthracene
ND
ug/kg
362
121
1
09/17/23 17:12
09/18/23 11:52
56-55-3
Benzo(a)pyrene
ND
ug/kg
362
125
1
09/17/23 17:12
09/18/23 11:52
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
362
121
1
09/17/23 17:12
09/18/23 11:52
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
362
141
1
09/17/23 17:12
09/18/23 11:52
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
362
127
1
09/17/23 17:12
09/18/23 11:52
207-08-9
Benzoic Acid
ND
ug/kg
1810
778
1
09/17/23 17:12
09/18/23 11:52
65-85-0
Benzyl alcohol
ND
ug/kg
725
274
1
09/17/23 17:12
09/18/23 11:52
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
362
139
1
09/17/23 17:12
09/18/23 11:52
101-55-3
Butylbenzylphthalate
ND
ug/kg
362
153
1
09/17/23 17:12
09/18/23 11:52
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
725
255
1
09/17/23 17:12
09/18/23 11:52
59-50-7
4-Chloroaniline
ND
ug/kg
725
284
1
09/17/23 17:12
09/18/23 11:52
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
362
150
1
09/17/23 17:12
09/18/23 11:52
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
362
136
1
09/17/23 17:12
09/18/23 11:52
111-44-4
2-Chloronaphthalene
ND
ug/kg
362
144
1
09/17/23 17:12
09/18/23 11:52
91-58-7
2-Chlorophenol
ND
ug/kg
362
136
1
09/17/23 17:12
09/18/23 11:52
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
362
135
1
09/17/23 17:12
09/18/23 11:52
7005-72-3
Chrysene
ND
ug/kg
362
132
1
09/17/23 17:12
09/18/23 11:52
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
362
139
1
09/17/23 17:12
09/18/23 11:52
53-70-3
Dibenzofuran
ND
ug/kg
362
131
1
09/17/23 17:12
09/18/23 11:52
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
362
131
1
09/17/23 17:12
09/18/23 11:52
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
362
128
1
09/17/23 17:12
09/18/23 11:52
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
362
138
1
09/17/23 17:12
09/18/23 11:52
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
725
245
1
09/17/23 17:12
09/18/23 11:52
91-94-1
2,4-Dichlorophenol
ND
ug/kg
362
142
1
09/17/23 17:12
09/18/23 11:52
120-83-2
Diethylphthalate
ND
ug/kg
362
133
1
09/17/23 17:12
09/18/23 11:52
84-66-2
2,4-Dimethylphenol
ND
ug/kg
362
150
1
09/17/23 17:12
09/18/23 11:52
105-67-9
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-6 Lab ID: 92688240006 Collected: 09/12/23 14:56 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Dimethylphthalate
ND
ug/kg
362
132
1
09/17/23 17:12
09/18/23 11:52
131-11-3
Di-n-butylphthalate
ND
ug/kg
362
122
1
09/17/23 17:12
09/18/23 11:52
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
725
338
1
09/17/23 17:12
09/18/23 11:52
534-52-1
2,4-Dinitrophenol
ND
ug/kg
1810
1120
1
09/17/23 17:12
09/18/23 11:52
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
362
139
1
09/17/23 17:12
09/18/23 11:52
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
362
133
1
09/17/23 17:12
09/18/23 11:52
606-20-2
Di-n-octylphthalate
ND
ug/kg
362
143
1
09/17/23 17:12
09/18/23 11:52
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
362
141
1
09/17/23 17:12
09/18/23 11:52
117-81-7
Fluoranthene
ND
ug/kg
362
124
1
09/17/23 17:12
09/18/23 11:52
206-44-0
Fluorene
ND
ug/kg
362
127
1
09/17/23 17:12
09/18/23 11:52
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
362
157
1
09/17/23 17:12
09/18/23 11:52
87-68-3
Hexachlorobenzene
ND
ug/kg
362
142
1
09/17/23 17:12
09/18/23 11:52
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
362
207
1
09/17/23 17:12
09/18/23 11:52
77-47-4
Hexachloroethane
ND
ug/kg
362
138
1
09/17/23 17:12
09/18/23 11:52
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
362
143
1
09/17/23 17:12
09/18/23 11:52
193-39-5
Isophorone
ND
ug/kg
362
161
1
09/17/23 17:12
09/18/23 11:52
78-59-1
1-Methylnaphthalene
ND
ug/kg
362
127
1
09/17/23 17:12
09/18/23 11:52
90-12-0
2-Methylnaphthalene
ND
ug/kg
362
145
1
09/17/23 17:12
09/18/23 11:52
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
362
148
1
09/17/23 17:12
09/18/23 11:52
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
362
146
1
09/17/23 17:12
09/18/23 11:52
15831-10-4
Naphthalene
ND
ug/kg
362
123
1
09/17/23 17:12
09/18/23 11:52
91-20-3
2-Nitroaniline
ND
ug/kg
1810
296
1
09/17/23 17:12
09/18/23 11:52
88-74-4
3-Nitroaniline
ND
ug/kg
1810
284
1
09/17/23 17:12
09/18/23 11:52
99-09-2
4-Nitroaniline
ND
ug/kg
725
276
1
09/17/23 17:12
09/18/23 11:52
100-01-6
Nitrobenzene
ND
ug/kg
362
168
1
09/17/23 17:12
09/18/23 11:52
98-95-3
2-Nitrophenol
ND
ug/kg
362
157
1
09/17/23 17:12
09/18/23 11:52
88-75-5
4-Nitrophenol
ND
ug/kg
1810
700
1
09/17/23 17:12
09/18/23 11:52
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
362
122
1
09/17/23 17:12
09/18/23 11:52
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
362
136
1
09/17/23 17:12
09/18/23 11:52
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
362
128
1
09/17/23 17:12
09/18/23 11:52
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
362
172
1
09/17/23 17:12
09/18/23 11:52
108-60-1
Pentachlorophenol
ND
ug/kg
725
355
1
09/17/23 17:12
09/18/23 11:52
87-86-5
Phenanthrene
ND
ug/kg
362
119
1
09/17/23 17:12
09/18/23 11:52
85-01-8
Phenol
ND
ug/kg
362
161
1
09/17/23 17:12
09/18/23 11:52
108-95-2
Pyrene
ND
ug/kg
362
147
1
09/17/23 17:12
09/18/23 11:52
129-00-0
Pyridine
ND
ug/kg
362
114
1
09/17/23 17:12
09/18/23 11:52
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
362
143
1
09/17/23 17:12
09/18/23 11:52
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
362
166
1
09/17/23 17:12
09/18/23 11:52
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
362
149
1
09/17/23 17:12
09/18/23 11:52
88-06-2
Surrogates
Nitrobenzene-d5 (S)
66
%
10-130
1
09/17/23 17:12
09/18/23 11:52
4165-60-0
2-Fluorobiphenyl (S)
49
%
10-130
1
09/17/23 17:12
09/18/23 11:52
321-60-8
Terphenyl-d14 (S)
65
%
10-130
1
09/17/23 17:12
09/18/23 11:52
1718-51-0
Phenol-d6 (S)
63
%
10-130
1
09/17/23 17:12
09/18/23 11:52
13127-88-3
REPORT OF LABORATORY ANALYSIS
v1
v1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-6 Lab ID: 92688240006 Collected: 09/12/23 14:56 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Surrogates
2-Fluorophenol (S)
60
%
10-130
1
09/17/23 17:12
09/18/23 11:52
367-12-4
2,4,6-Tribromophenol (S)
68
%
10-131
1
09/17/23 17:12
09/18/23 11:52
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation Method: EPA
5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
123
39.5
1
09/15/23 20:55
09/16/23 05:22
67-64-1
Benzene
ND
ug/kg
6.2
2.5
1
09/15/23 20:55
09/16/23 05:22
71-43-2
Bromobenzene
ND
ug/kg
6.2
2.0
1
09/15/23 20:55
09/16/23 05:22
108-86-1
Bromochloromethane
ND
ug/kg
6.2
1.8
1
09/15/23 20:55
09/16/23 05:22
74-97-5
Bromodichloromethane
ND
ug/kg
6.2
2.4
1
09/15/23 20:55
09/16/23 05:22
75-27-4
Bromoform
ND
ug/kg
6.2
2.2
1
09/15/23 20:55
09/16/23 05:22
75-25-2
Bromomethane
ND
ug/kg
24.6
19.1
1
09/15/23 20:55
09/16/23 05:22
74-83-9
2-Butanone (MEK)
ND
ug/kg
123
29.6
1
09/15/23 20:55
09/16/23 05:22
78-93-3
n-Butylbenzene
ND
ug/kg
6.2
3.9
1
09/15/23 20:55
09/16/23 05:22
104-51-8
sec-Butylbenzene
ND
ug/kg
6.2
2.7
1
09/15/23 20:55
09/16/23 05:22
135-98-8
tert-Butyl benzene
ND
ug/kg
6.2
2.2
1
09/15/23 20:55
09/16/23 05:22
98-06-6
Carbon tetrachloride
ND
ug/kg
6.2
2.3
1
09/15/23 20:55
09/16/23 05:22
56-23-5
Chlorobenzene
ND
ug/kg
6.2
3.5
1
09/15/23 20:55
09/16/23 05:22
108-90-7
Chloroethane
ND
ug/kg
12.3
4.8
1
09/15/23 20:55
09/16/23 05:22
75-00-3
Chloroform
ND
ug/kg
6.2
5.1
1
09/15/23 20:55
09/16/23 05:22
67-66-3
Chloromethane
ND
ug/kg
12.3
5.2
1
09/15/23 20:55
09/16/23 05:22
74-87-3
2-Chlorotoluene
ND
ug/kg
6.2
2.2
1
09/15/23 20:55
09/16/23 05:22
95-49-8
4-Chlorotoluene
ND
ug/kg
6.2
3.4
1
09/15/23 20:55
09/16/23 05:22
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
6.2
2.4
1
09/15/23 20:55
09/16/23 05:22
96-12-8
Dibromochloromethane
ND
ug/kg
6.2
3.5
1
09/15/23 20:55
09/16/23 05:22
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
6.2
2.7
1
09/15/23 20:55
09/16/23 05:22
106-93-4
Dibromomethane
ND
ug/kg
6.2
1.3
1
09/15/23 20:55
09/16/23 05:22
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
6.2
2.2
1
09/15/23 20:55
09/16/23 05:22
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
6.2
1.9
1
09/15/23 20:55
09/16/23 05:22
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
6.2
1.6
1
09/15/23 20:55
09/16/23 05:22
106-46-7
Dichlorodifluoromethane
ND
ug/kg
12.3
6.3
1
09/15/23 20:55
09/16/23 05:22
75-71-8
1,1-Dichloroethane
ND
ug/kg
6.2
2.5
1
09/15/23 20:55
09/16/23 05:22
75-34-3
1,2-Dichloroethane
ND
ug/kg
6.2
4.1
1
09/15/23 20:55
09/16/23 05:22
107-06-2
1,1-Dichloroethene
ND
ug/kg
6.2
2.5
1
09/15/23 20:55
09/16/23 05:22
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
6.2
2.1
1
09/15/23 20:55
09/16/23 05:22
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
6.2
5.2
1
09/15/23 20:55
09/16/23 05:22
156-60-5
1,2-Dichloropropane
ND
ug/kg
6.2
1.8
1
09/15/23 20:55
09/16/23 05:22
78-87-5
1,3-Dichloropropane
ND
ug/kg
6.2
1.9
1
09/15/23 20:55
09/16/23 05:22
142-28-9
2,2-Dichloropropane
ND
ug/kg
6.2
4.7
1
09/15/23 20:55
09/16/23 05:22
594-20-7
1,1-Dichloropropene
ND
ug/kg
6.2
3.0
1
09/15/23 20:55
09/16/23 05:22
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
6.2
1.7
1
09/15/23 20:55
09/16/23 05:22
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
6.2
2.1
1
09/15/23 20:55
09/16/23 05:22
10061-02-6
REPORT OF LABORATORY ANALYSIS
L1,v1
IH,L1,
v1
L1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-6 Lab ID: 92688240006 Collected: 09/12/23 14:56 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Total Solids 2540 G-2011
Total Solids
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
ug/kg
6.2
1.7
1
09/15/23 20:55
09/16/23 05:22
108-20-3
ND
ug/kg
6.2
2.9
1
09/15/23 20:55
09/16/23 05:22
100-41-4
ND
ug/kg
12.3
10.1
1
09/15/23 20:55
09/16/23 05:22
87-68-3
ND
ug/kg
61.6
5.9
1
09/15/23 20:55
09/16/23 05:22
591-78-6
ND
ug/kg
6.2
2.1
1
09/15/23 20:55
09/16/23 05:22
98-82-8
ND
ug/kg
6.2
3.0
1
09/15/23 20:55
09/16/23 05:22
99-87-6
ND
ug/kg
24.6
16.9
1
09/15/23 20:55
09/16/23 05:22
75-09-2
ND
ug/kg
61.6
5.9
1
09/15/23 20:55
09/16/23 05:22
108-10-1
ND
ug/kg
6.2
2.3
1
09/15/23 20:55
09/16/23 05:22
1634-04-4
ND
ug/kg
6.2
3.2
1
09/15/23 20:55
09/16/23 05:22
91-20-3
ND
ug/kg
6.2
2.2
1
09/15/23 20:55
09/16/23 05:22
103-65-1
ND
ug/kg
6.2
1.6
1
09/15/23 20:55
09/16/23 05:22
100-42-5
ND
ug/kg
6.2
2.4
1
09/15/23 20:55
09/16/23 05:22
630-20-6
ND
ug/kg
6.2
1.6
1
09/15/23 20:55
09/16/23 05:22
79-34-5
ND
ug/kg
6.2
1.9
1
09/15/23 20:55
09/16/23 05:22
127-18-4
7.9
ug/kg
6.2
4.2
1
09/15/23 20:55
09/16/23 05:22
108-88-3
ND
ug/kg
6.2
5.0
1
09/15/23 20:55
09/16/23 05:22
87-61-6
ND
ug/kg
6.2
5.2
1
09/15/23 20:55
09/16/23 05:22
120-82-1
ND
ug/kg
6.2
3.2
1
09/15/23 20:55
09/16/23 05:22
71-55-6
ND
ug/kg
6.2
2.0
1
09/15/23 20:55
09/16/23 05:22
79-00-5
ND
ug/kg
6.2
5.0
1
09/15/23 20:55
09/16/23 05:22
79-01-6
ND
ug/kg
6.2
3.4
1
09/15/23 20:55
09/16/23 05:22
75-69-4
ND
ug/kg
6.2
3.1
1
09/15/23 20:55
09/16/23 05:22
96-18-4
ND
ug/kg
6.2
3.7
1
09/15/23 20:55
09/16/23 05:22
95-63-6
ND
ug/kg
6.2
2.1
1
09/15/23 20:55
09/16/23 05:22
108-67-8
ND
ug/kg
61.6
12.7
1
09/15/23 20:55
09/16/23 05:22
108-05-4
ND
ug/kg
12.3
3.1
1
09/15/23 20:55
09/16/23 05:22
75-01-4
ND
ug/kg
12.3
3.5
1
09/15/23 20:55
09/16/23 05:22
1330-20-7
ND
ug/kg
12.3
4.2
1
09/15/23 20:55
09/16/23 05:22
179601-23-1
ND
ug/kg
6.2
2.7
1
09/15/23 20:55
09/16/23 05:22
95-47-6
100
%
70-130
1
09/15/23 20:55
09/16/23 05:22
2037-26-5
102
%
70-130
1
09/15/23 20:55
09/16/23 05:22
460-00-4
104
%
70-130
1
09/15/23 20:55
09/16/23 05:22
17060-07-0
Analytical Method: SW-846
Pace Analytical Services - Charlotte
10.1 % 0.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
73.9 %
09/15/23 17:39
1 09/21 /23 06:36 09/21 /23 06:42
REPORT OF LABORATORY ANALYSIS
I:/
v1
I0`a
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-6 Lab ID: 92688240006 Collected: 09/12/23 14:56 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Wet Chemistry 7199 Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Chromium, Hexavalent 0.633J mg/kg 1.35 0.345 1 09/21/23 12:45 09/22/23 12:44 18540-29-9 J
Date: 09/25/2023 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 36 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-7 Lab ID: 92688240007 Collected: 09/12/23 15:25 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical
Services
- Ormond Beach
Arsenic
1.1
mg/kg
0.59
0.29
1
09/22/2311:05
09/25/2311:32
7440-38-2
Barium
29.5
mg/kg
0.59
0.099
1
09/22/2311:05
09/25/2311:32
7440-39-3
Cadmium
0.082
mg/kg
0.059
0.029
1
09/22/2311:05
09/25/2311:32
7440-43-9
Chromium
8.2
mg/kg
0.29
0.15
1
09/22/2311:05
09/25/2311:32
7440-47-3
Lead
15.4
mg/kg
0.59
0.29
1
09/22/2311:05
09/25/2311:32
7439-92-1
Selenium
ND
mg/kg
0.88
0.44
1
09/22/2311:05
09/25/2311:32
7782-49-2
Silver
ND
mg/kg
0.29
0.065
1
09/22/2311:05
09/25/2311:32
7440-22-4
7471 Mercury
Analytical
Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical
Services
- Ormond Beach
Mercury
0.035
mg/kg
0.0086
0.0043
1
09/21/2312:51
09/22/2310:18
7439-97-6
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation
Method: EPA
3546
Pace Analytical
Services
- Charlotte
Acenaphthene
ND
ug/kg
364
128
1
09/17/23 17:12
09/18/23 12:20
83-32-9
Acenaphthylene
ND
ug/kg
364
128
1
09/17/23 17:12
09/18/23 12:20
208-96-8
Aniline
ND
ug/kg
364
142
1
09/17/23 17:12
09/18/23 12:20
62-53-3
Anthracene
ND
ug/kg
364
119
1
09/17/23 17:12
09/18/23 12:20
120-12-7
Benzo(a)anthracene
ND
ug/kg
364
121
1
09/17/23 17:12
09/18/23 12:20
56-55-3
Benzo(a)pyrene
ND
ug/kg
364
126
1
09/17/23 17:12
09/18/23 12:20
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
364
121
1
09/17/23 17:12
09/18/23 12:20
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
364
141
1
09/17/23 17:12
09/18/23 12:20
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
364
128
1
09/17/23 17:12
09/18/23 12:20
207-08-9
Benzoic Acid
ND
ug/kg
1820
783
1
09/17/23 17:12
09/18/23 12:20
65-85-0
Benzyl alcohol
ND
ug/kg
729
276
1
09/17/23 17:12
09/18/23 12:20
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
364
140
1
09/17/23 17:12
09/18/23 12:20
101-55-3
Butylbenzylphthalate
ND
ug/kg
364
153
1
09/17/23 17:12
09/18/23 12:20
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
729
256
1
09/17/23 17:12
09/18/23 12:20
59-50-7
4-Chloroaniline
ND
ug/kg
729
286
1
09/17/23 17:12
09/18/23 12:20
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
364
151
1
09/17/23 17:12
09/18/23 12:20
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
364
137
1
09/17/23 17:12
09/18/23 12:20
111-44-4
2-Chloronaphthalene
ND
ug/kg
364
145
1
09/17/23 17:12
09/18/23 12:20
91-58-7
2-Chlorophenol
ND
ug/kg
364
137
1
09/17/23 17:12
09/18/23 12:20
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
364
136
1
09/17/23 17:12
09/18/23 12:20
7005-72-3
Chrysene
ND
ug/kg
364
132
1
09/17/23 17:12
09/18/23 12:20
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
364
140
1
09/17/23 17:12
09/18/23 12:20
53-70-3
Dibenzofuran
ND
ug/kg
364
131
1
09/17/23 17:12
09/18/23 12:20
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
364
131
1
09/17/23 17:12
09/18/23 12:20
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
364
129
1
09/17/23 17:12
09/18/23 12:20
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
364
139
1
09/17/23 17:12
09/18/23 12:20
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
729
246
1
09/17/23 17:12
09/18/23 12:20
91-94-1
2,4-Dichlorophenol
ND
ug/kg
364
142
1
09/17/23 17:12
09/18/23 12:20
120-83-2
Diethylphthalate
ND
ug/kg
364
134
1
09/17/23 17:12
09/18/23 12:20
84-66-2
2,4-Dimethylphenol
ND
ug/kg
364
151
1
09/17/23 17:12
09/18/23 12:20
105-67-9
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-7 Lab ID: 92688240007 Collected: 09/12/23 15:25 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Dimethylphthalate
ND
ug/kg
364
132
1
09/17/23 17:12
09/18/23 12:20
131-11-3
Di-n-butylphthalate
ND
ug/kg
364
123
1
09/17/23 17:12
09/18/23 12:20
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
729
340
1
09/17/23 17:12
09/18/23 12:20
534-52-1
2,4-Dinitrophenol
ND
ug/kg
1820
1130
1
09/17/23 17:12
09/18/23 12:20
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
364
140
1
09/17/23 17:12
09/18/23 12:20
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
364
134
1
09/17/23 17:12
09/18/23 12:20
606-20-2
Di-n-octylphthalate
ND
ug/kg
364
143
1
09/17/23 17:12
09/18/23 12:20
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
364
141
1
09/17/23 17:12
09/18/23 12:20
117-81-7
Fluoranthene
ND
ug/kg
364
125
1
09/17/23 17:12
09/18/23 12:20
206-44-0
Fluorene
ND
ug/kg
364
128
1
09/17/23 17:12
09/18/23 12:20
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
364
158
1
09/17/23 17:12
09/18/23 12:20
87-68-3
Hexachlorobenzene
ND
ug/kg
364
142
1
09/17/23 17:12
09/18/23 12:20
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
364
209
1
09/17/23 17:12
09/18/23 12:20
77-47-4
Hexachloroethane
ND
ug/kg
364
139
1
09/17/23 17:12
09/18/23 12:20
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
364
143
1
09/17/23 17:12
09/18/23 12:20
193-39-5
Isophorone
ND
ug/kg
364
162
1
09/17/23 17:12
09/18/23 12:20
78-59-1
1-Methylnaphthalene
ND
ug/kg
364
128
1
09/17/23 17:12
09/18/23 12:20
90-12-0
2-Methylnaphthalene
ND
ug/kg
364
146
1
09/17/23 17:12
09/18/23 12:20
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
364
149
1
09/17/23 17:12
09/18/23 12:20
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
364
147
1
09/17/23 17:12
09/18/23 12:20
15831-10-4
Naphthalene
ND
ug/kg
364
124
1
09/17/23 17:12
09/18/23 12:20
91-20-3
2-Nitroaniline
ND
ug/kg
1820
298
1
09/17/23 17:12
09/18/23 12:20
88-74-4
3-Nitroaniline
ND
ug/kg
1820
286
1
09/17/23 17:12
09/18/23 12:20
99-09-2
4-Nitroaniline
ND
ug/kg
729
277
1
09/17/23 17:12
09/18/23 12:20
100-01-6
Nitrobenzene
ND
ug/kg
364
169
1
09/17/23 17:12
09/18/23 12:20
98-95-3
2-Nitrophenol
ND
ug/kg
364
158
1
09/17/23 17:12
09/18/23 12:20
88-75-5
4-Nitrophenol
ND
ug/kg
1820
704
1
09/17/23 17:12
09/18/23 12:20
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
364
123
1
09/17/23 17:12
09/18/23 12:20
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
364
137
1
09/17/23 17:12
09/18/23 12:20
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
364
129
1
09/17/23 17:12
09/18/23 12:20
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
364
173
1
09/17/23 17:12
09/18/23 12:20
108-60-1
Pentachlorophenol
ND
ug/kg
729
357
1
09/17/23 17:12
09/18/23 12:20
87-86-5
Phenanthrene
ND
ug/kg
364
119
1
09/17/23 17:12
09/18/23 12:20
85-01-8
Phenol
ND
ug/kg
364
162
1
09/17/23 17:12
09/18/23 12:20
108-95-2
Pyrene
ND
ug/kg
364
148
1
09/17/23 17:12
09/18/23 12:20
129-00-0
Pyridine
ND
ug/kg
364
115
1
09/17/23 17:12
09/18/23 12:20
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
364
143
1
09/17/23 17:12
09/18/23 12:20
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
364
167
1
09/17/23 17:12
09/18/23 12:20
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
364
150
1
09/17/23 17:12
09/18/23 12:20
88-06-2
Surrogates
Nitrobenzene-d5 (S)
62
%
10-130
1
09/17/23 17:12
09/18/23 12:20
4165-60-0
2-Fluorobiphenyl (S)
59
%
10-130
1
09/17/23 17:12
09/18/23 12:20
321-60-8
Terphenyl-d14 (S)
73
%
10-130
1
09/17/23 17:12
09/18/23 12:20
1718-51-0
Phenol-d6 (S)
60
%
10-130
1
09/17/23 17:12
09/18/23 12:20
13127-88-3
REPORT OF LABORATORY ANALYSIS
v1
v1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-7 Lab ID: 92688240007 Collected: 09/12/23 15:25 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Surrogates
2-Fluorophenol (S)
57
%
10-130
1
09/17/23 17:12
09/18/23 12:20
367-12-4
2,4,6-Tribromophenol (S)
77
%
10-131
1
09/17/23 17:12
09/18/23 12:20
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation Method: EPA
5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
255
81.9
1
09/15/23 20:55
09/16/23 05:40
67-64-1
Benzene
ND
ug/kg
12.8
5.1
1
09/15/23 20:55
09/16/23 05:40
71-43-2
Bromobenzene
ND
ug/kg
12.8
4.2
1
09/15/23 20:55
09/16/23 05:40
108-86-1
Bromochloromethane
ND
ug/kg
12.8
3.8
1
09/15/23 20:55
09/16/23 05:40
74-97-5
Bromodichloromethane
ND
ug/kg
12.8
4.9
1
09/15/23 20:55
09/16/23 05:40
75-27-4
Bromoform
ND
ug/kg
12.8
4.5
1
09/15/23 20:55
09/16/23 05:40
75-25-2
Bromomethane
ND
ug/kg
51.0
39.6
1
09/15/23 20:55
09/16/23 05:40
74-83-9
2-Butanone (MEK)
ND
ug/kg
255
61.3
1
09/15/23 20:55
09/16/23 05:40
78-93-3
n-Butylbenzene
ND
ug/kg
12.8
8.0
1
09/15/23 20:55
09/16/23 05:40
104-51-8
sec-Butylbenzene
ND
ug/kg
12.8
5.6
1
09/15/23 20:55
09/16/23 05:40
135-98-8
tert-Butyl benzene
ND
ug/kg
12.8
4.5
1
09/15/23 20:55
09/16/23 05:40
98-06-6
Carbon tetrachloride
ND
ug/kg
12.8
4.8
1
09/15/23 20:55
09/16/23 05:40
56-23-5
Chlorobenzene
ND
ug/kg
12.8
7.3
1
09/15/23 20:55
09/16/23 05:40
108-90-7
Chloroethane
ND
ug/kg
25.5
9.9
1
09/15/23 20:55
09/16/23 05:40
75-00-3
Chloroform
ND
ug/kg
12.8
10.7
1
09/15/23 20:55
09/16/23 05:40
67-66-3
Chloromethane
ND
ug/kg
25.5
10.7
1
09/15/23 20:55
09/16/23 05:40
74-87-3
2-Chlorotoluene
ND
ug/kg
12.8
4.5
1
09/15/23 20:55
09/16/23 05:40
95-49-8
4-Chlorotoluene
ND
ug/kg
12.8
7.1
1
09/15/23 20:55
09/16/23 05:40
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
12.8
5.0
1
09/15/23 20:55
09/16/23 05:40
96-12-8
Dibromochloromethane
ND
ug/kg
12.8
7.2
1
09/15/23 20:55
09/16/23 05:40
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
12.8
5.6
1
09/15/23 20:55
09/16/23 05:40
106-93-4
Dibromomethane
ND
ug/kg
12.8
2.7
1
09/15/23 20:55
09/16/23 05:40
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
12.8
4.6
1
09/15/23 20:55
09/16/23 05:40
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
12.8
4.0
1
09/15/23 20:55
09/16/23 05:40
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
12.8
3.3
1
09/15/23 20:55
09/16/23 05:40
106-46-7
Dichlorodifluoromethane
ND
ug/kg
25.5
13.0
1
09/15/23 20:55
09/16/23 05:40
75-71-8
1,1-Dichloroethane
ND
ug/kg
12.8
5.3
1
09/15/23 20:55
09/16/23 05:40
75-34-3
1,2-Dichloroethane
ND
ug/kg
12.8
8.4
1
09/15/23 20:55
09/16/23 05:40
107-06-2
1,1-Dichloroethene
ND
ug/kg
12.8
5.3
1
09/15/23 20:55
09/16/23 05:40
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
12.8
4.4
1
09/15/23 20:55
09/16/23 05:40
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
12.8
10.8
1
09/15/23 20:55
09/16/23 05:40
156-60-5
1,2-Dichloropropane
ND
ug/kg
12.8
3.8
1
09/15/23 20:55
09/16/23 05:40
78-87-5
1,3-Dichloropropane
ND
ug/kg
12.8
4.0
1
09/15/23 20:55
09/16/23 05:40
142-28-9
2,2-Dichloropropane
ND
ug/kg
12.8
9.7
1
09/15/23 20:55
09/16/23 05:40
594-20-7
1,1-Dichloropropene
ND
ug/kg
12.8
6.1
1
09/15/23 20:55
09/16/23 05:40
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
12.8
3.5
1
09/15/23 20:55
09/16/23 05:40
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
12.8
4.4
1
09/15/23 20:55
09/16/23 05:40
10061-02-6
REPORT OF LABORATORY ANALYSIS
L1,v1
IH,L1,
v1
L1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-7 Lab ID: 92688240007 Collected: 09/12/23 15:25 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Total Solids 2540 G-2011
Total Solids
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
ug/kg
12.8
3.4
1
09/15/23 20:55
09/16/23 05:40
108-20-3
ND
ug/kg
12.8
5.9
1
09/15/23 20:55
09/16/23 05:40
100-41-4
ND
ug/kg
25.5
20.9
1
09/15/23 20:55
09/16/23 05:40
87-68-3
ND
ug/kg
128
12.3
1
09/15/23 20:55
09/16/23 05:40
591-78-6
ND
ug/kg
12.8
4.3
1
09/15/23 20:55
09/16/23 05:40
98-82-8
ND
ug/kg
12.8
6.3
1
09/15/23 20:55
09/16/23 05:40
99-87-6
ND
ug/kg
51.0
35.0
1
09/15/23 20:55
09/16/23 05:40
75-09-2
ND
ug/kg
128
12.3
1
09/15/23 20:55
09/16/23 05:40
108-10-1
ND
ug/kg
12.8
4.8
1
09/15/23 20:55
09/16/23 05:40
1634-04-4
ND
ug/kg
12.8
6.7
1
09/15/23 20:55
09/16/23 05:40
91-20-3
ND
ug/kg
12.8
4.5
1
09/15/23 20:55
09/16/23 05:40
103-65-1
ND
ug/kg
12.8
3.4
1
09/15/23 20:55
09/16/23 05:40
100-42-5
ND
ug/kg
12.8
4.9
1
09/15/23 20:55
09/16/23 05:40
630-20-6
ND
ug/kg
12.8
3.4
1
09/15/23 20:55
09/16/23 05:40
79-34-5
ND
ug/kg
12.8
4.0
1
09/15/23 20:55
09/16/23 05:40
127-18-4
ND
ug/kg
12.8
8.8
1
09/15/23 20:55
09/16/23 05:40
108-88-3
ND
ug/kg
12.8
10.3
1
09/15/23 20:55
09/16/23 05:40
87-61-6
ND
ug/kg
12.8
10.7
1
09/15/23 20:55
09/16/23 05:40
120-82-1
ND
ug/kg
12.8
6.6
1
09/15/23 20:55
09/16/23 05:40
71-55-6
ND
ug/kg
12.8
4.2
1
09/15/23 20:55
09/16/23 05:40
79-00-5
ND
ug/kg
12.8
10.3
1
09/15/23 20:55
09/16/23 05:40
79-01-6
ND
ug/kg
12.8
7.0
1
09/15/23 20:55
09/16/23 05:40
75-69-4
ND
ug/kg
12.8
6.5
1
09/15/23 20:55
09/16/23 05:40
96-18-4
ND
ug/kg
12.8
7.6
1
09/15/23 20:55
09/16/23 05:40
95-63-6
ND
ug/kg
12.8
4.3
1
09/15/23 20:55
09/16/23 05:40
108-67-8
ND
ug/kg
128
26.3
1
09/15/23 20:55
09/16/23 05:40
108-05-4
ND
ug/kg
25.5
6.5
1
09/15/23 20:55
09/16/23 05:40
75-01-4
ND
ug/kg
25.5
7.3
1
09/15/23 20:55
09/16/23 05:40
1330-20-7
ND
ug/kg
25.5
8.7
1
09/15/23 20:55
09/16/23 05:40
179601-23-1
ND
ug/kg
12.8
5.6
1
09/15/23 20:55
09/16/23 05:40
95-47-6
101
%
70-130
1
09/15/23 20:55
09/16/23 05:40
2037-26-5
101
%
70-130
1
09/15/23 20:55
09/16/23 05:40
460-00-4
105
%
70-130
1
09/15/23 20:55
09/16/23 05:40
17060-07-0
Analytical Method: SW-846
Pace Analytical Services - Charlotte
7.9 % 0.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
89.8 %
09/15/23 17:39
1 09/21 /23 06:36 09/21 /23 06:42
REPORT OF LABORATORY ANALYSIS
I:/
v1
I0`a
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-7 Lab ID: 92688240007 Collected: 09/12/23 15:25 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Wet Chemistry 7199 Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Chromium, Hexavalent 0.596J mg/kg 1.11 0.284 1 09/21/23 12:45 09/22/23 12:49 18540-29-9 J
Date: 09/25/2023 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 41 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-8 Lab ID: 92688240008 Collected: 09/12/23 15:41 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical
Services
- Ormond Beach
Arsenic
0.50J
mg/kg
0.62
0.31
1
09/22/2311:05
09/25/2311:36
7440-38-2
Barium
15.5
mg/kg
0.62
0.10
1
09/22/2311:05
09/25/2311:36
7440-39-3
Cadmium
0.0501
mg/kg
0.062
0.031
1
09/22/2311:05
09/25/2311:36
7440-43-9
Chromium
4.6
mg/kg
0.31
0.16
1
09/22/2311:05
09/25/2311:36
7440-47-3
Lead
2.5
mg/kg
0.62
0.31
1
09/22/2311:05
09/25/2311:36
7439-92-1
Selenium
ND
mg/kg
0.93
0.47
1
09/22/2311:05
09/25/2311:36
7782-49-2
Silver
ND
mg/kg
0.31
0.068
1
09/22/2311:05
09/25/2311:36
7440-22-4
7471 Mercury
Analytical
Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical
Services
- Ormond Beach
Mercury
0.025
mg/kg
0.0096
0.0048
1
09/21/2312:51
09/22/2310:20
7439-97-6
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation
Method: EPA
3546
Pace Analytical
Services
- Charlotte
Acenaphthene
ND
ug/kg
365
128
1
09/17/23 17:12
09/18/23 12:48
83-32-9
Acenaphthylene
ND
ug/kg
365
128
1
09/17/23 17:12
09/18/23 12:48
208-96-8
Aniline
ND
ug/kg
365
143
1
09/17/23 17:12
09/18/23 12:48
62-53-3
Anthracene
ND
ug/kg
365
120
1
09/17/23 17:12
09/18/23 12:48
120-12-7
Benzo(a)anthracene
ND
ug/kg
365
122
1
09/17/23 17:12
09/18/23 12:48
56-55-3
Benzo(a)pyrene
ND
ug/kg
365
126
1
09/17/23 17:12
09/18/23 12:48
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
365
122
1
09/17/23 17:12
09/18/23 12:48
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
365
142
1
09/17/23 17:12
09/18/23 12:48
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
365
128
1
09/17/23 17:12
09/18/23 12:48
207-08-9
Benzoic Acid
ND
ug/kg
1830
785
1
09/17/23 17:12
09/18/23 12:48
65-85-0
Benzyl alcohol
ND
ug/kg
731
277
1
09/17/23 17:12
09/18/23 12:48
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
365
141
1
09/17/23 17:12
09/18/23 12:48
101-55-3
Butylbenzylphthalate
ND
ug/kg
365
154
1
09/17/23 17:12
09/18/23 12:48
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
731
257
1
09/17/23 17:12
09/18/23 12:48
59-50-7
4-Chloroaniline
ND
ug/kg
731
287
1
09/17/23 17:12
09/18/23 12:48
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
365
152
1
09/17/23 17:12
09/18/23 12:48
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
365
137
1
09/17/23 17:12
09/18/23 12:48
111-44-4
2-Chloronaphthalene
ND
ug/kg
365
145
1
09/17/23 17:12
09/18/23 12:48
91-58-7
2-Chlorophenol
ND
ug/kg
365
137
1
09/17/23 17:12
09/18/23 12:48
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
365
136
1
09/17/23 17:12
09/18/23 12:48
7005-72-3
Chrysene
ND
ug/kg
365
133
1
09/17/23 17:12
09/18/23 12:48
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
365
141
1
09/17/23 17:12
09/18/23 12:48
53-70-3
Dibenzofuran
ND
ug/kg
365
132
1
09/17/23 17:12
09/18/23 12:48
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
365
132
1
09/17/23 17:12
09/18/23 12:48
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
365
130
1
09/17/23 17:12
09/18/23 12:48
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
365
140
1
09/17/23 17:12
09/18/23 12:48
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
731
247
1
09/17/23 17:12
09/18/23 12:48
91-94-1
2,4-Dichlorophenol
ND
ug/kg
365
143
1
09/17/23 17:12
09/18/23 12:48
120-83-2
Diethylphthalate
ND
ug/kg
365
134
1
09/17/23 17:12
09/18/23 12:48
84-66-2
2,4-Dimethylphenol
ND
ug/kg
365
152
1
09/17/23 17:12
09/18/23 12:48
105-67-9
REPORT OF LABORATORY ANALYSIS
v1
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Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-8 Lab ID: 92688240008 Collected: 09/12/23 15:41 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Dimethylphthalate
ND
ug/kg
365
133
1
09/17/23 17:12
09/18/23 12:48
131-11-3
Di-n-butylphthalate
ND
ug/kg
365
123
1
09/17/23 17:12
09/18/23 12:48
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
731
341
1
09/17/23 17:12
09/18/23 12:48
534-52-1
2,4-Dinitrophenol
ND
ug/kg
1830
1130
1
09/17/23 17:12
09/18/23 12:48
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
365
141
1
09/17/23 17:12
09/18/23 12:48
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
365
134
1
09/17/23 17:12
09/18/23 12:48
606-20-2
Di-n-octylphthalate
ND
ug/kg
365
144
1
09/17/23 17:12
09/18/23 12:48
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
365
142
1
09/17/23 17:12
09/18/23 12:48
117-81-7
Fluoranthene
ND
ug/kg
365
125
1
09/17/23 17:12
09/18/23 12:48
206-44-0
Fluorene
ND
ug/kg
365
128
1
09/17/23 17:12
09/18/23 12:48
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
365
158
1
09/17/23 17:12
09/18/23 12:48
87-68-3
Hexachlorobenzene
ND
ug/kg
365
143
1
09/17/23 17:12
09/18/23 12:48
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
365
209
1
09/17/23 17:12
09/18/23 12:48
77-47-4
Hexachloroethane
ND
ug/kg
365
140
1
09/17/23 17:12
09/18/23 12:48
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
365
144
1
09/17/23 17:12
09/18/23 12:48
193-39-5
Isophorone
ND
ug/kg
365
163
1
09/17/23 17:12
09/18/23 12:48
78-59-1
1-Methylnaphthalene
ND
ug/kg
365
128
1
09/17/23 17:12
09/18/23 12:48
90-12-0
2-Methylnaphthalene
ND
ug/kg
365
146
1
09/17/23 17:12
09/18/23 12:48
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
365
149
1
09/17/23 17:12
09/18/23 12:48
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
365
147
1
09/17/23 17:12
09/18/23 12:48
15831-10-4
Naphthalene
ND
ug/kg
365
124
1
09/17/23 17:12
09/18/23 12:48
91-20-3
2-Nitroaniline
ND
ug/kg
1830
299
1
09/17/23 17:12
09/18/23 12:48
88-74-4
3-Nitroaniline
ND
ug/kg
1830
287
1
09/17/23 17:12
09/18/23 12:48
99-09-2
4-Nitroaniline
ND
ug/kg
731
278
1
09/17/23 17:12
09/18/23 12:48
100-01-6
Nitrobenzene
ND
ug/kg
365
169
1
09/17/23 17:12
09/18/23 12:48
98-95-3
2-Nitrophenol
ND
ug/kg
365
158
1
09/17/23 17:12
09/18/23 12:48
88-75-5
4-Nitrophenol
ND
ug/kg
1830
706
1
09/17/23 17:12
09/18/23 12:48
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
365
123
1
09/17/23 17:12
09/18/23 12:48
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
365
137
1
09/17/23 17:12
09/18/23 12:48
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
365
130
1
09/17/23 17:12
09/18/23 12:48
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
365
174
1
09/17/23 17:12
09/18/23 12:48
108-60-1
Pentachlorophenol
ND
ug/kg
731
358
1
09/17/23 17:12
09/18/23 12:48
87-86-5
Phenanthrene
ND
ug/kg
365
120
1
09/17/23 17:12
09/18/23 12:48
85-01-8
Phenol
ND
ug/kg
365
163
1
09/17/23 17:12
09/18/23 12:48
108-95-2
Pyrene
ND
ug/kg
365
148
1
09/17/23 17:12
09/18/23 12:48
129-00-0
Pyridine
ND
ug/kg
365
115
1
09/17/23 17:12
09/18/23 12:48
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
365
144
1
09/17/23 17:12
09/18/23 12:48
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
365
167
1
09/17/23 17:12
09/18/23 12:48
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
365
151
1
09/17/23 17:12
09/18/23 12:48
88-06-2
Surrogates
Nitrobenzene-d5 (S)
62
%
10-130
1
09/17/23 17:12
09/18/23 12:48
4165-60-0
2-Fluorobiphenyl (S)
49
%
10-130
1
09/17/23 17:12
09/18/23 12:48
321-60-8
Terphenyl-d14 (S)
62
%
10-130
1
09/17/23 17:12
09/18/23 12:48
1718-51-0
Phenol-d6 (S)
61
%
10-130
1
09/17/23 17:12
09/18/23 12:48
13127-88-3
REPORT OF LABORATORY ANALYSIS
v1
v1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-8 Lab ID: 92688240008 Collected: 09/12/23 15:41 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Surrogates
2-Fluorophenol (S)
59
%
10-130
1
09/17/23 17:12
09/18/23 12:48
367-12-4
2,4,6-Tribromophenol (S)
64
%
10-131
1
09/17/23 17:12
09/18/23 12:48
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation Method: EPA
5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
159
50.9
1
09/18/23 15:35
09/19/23 21:11
67-64-1
Benzene
ND
ug/kg
7.9
3.2
1
09/18/23 15:35
09/19/23 21:11
71-43-2
Bromobenzene
ND
ug/kg
7.9
2.6
1
09/18/23 15:35
09/19/23 21:11
108-86-1
Bromochloromethane
ND
ug/kg
7.9
2.3
1
09/18/23 15:35
09/19/23 21:11
74-97-5
Bromodichloromethane
ND
ug/kg
7.9
3.1
1
09/18/23 15:35
09/19/23 21:11
75-27-4
Bromoform
ND
ug/kg
7.9
2.8
1
09/18/23 15:35
09/19/23 21:11
75-25-2
Bromomethane
ND
ug/kg
31.7
24.6
1
09/18/23 15:35
09/19/23 21:11
74-83-9
2-Butanone (MEK)
ND
ug/kg
159
38.1
1
09/18/23 15:35
09/19/23 21:11
78-93-3
n-Butylbenzene
ND
ug/kg
7.9
5.0
1
09/18/23 15:35
09/19/23 21:11
104-51-8
sec-Butylbenzene
ND
ug/kg
7.9
3.5
1
09/18/23 15:35
09/19/23 21:11
135-98-8
tert-Butyl benzene
ND
ug/kg
7.9
2.8
1
09/18/23 15:35
09/19/23 21:11
98-06-6
Carbon tetrachloride
ND
ug/kg
7.9
3.0
1
09/18/23 15:35
09/19/23 21:11
56-23-5
Chlorobenzene
ND
ug/kg
7.9
4.6
1
09/18/23 15:35
09/19/23 21:11
108-90-7
Chloroethane
ND
ug/kg
15.9
6.1
1
09/18/23 15:35
09/19/23 21:11
75-00-3
Chloroform
ND
ug/kg
7.9
6.6
1
09/18/23 15:35
09/19/23 21:11
67-66-3
Chloromethane
ND
ug/kg
15.9
6.7
1
09/18/23 15:35
09/19/23 21:11
74-87-3
2-Chlorotoluene
ND
ug/kg
7.9
2.8
1
09/18/23 15:35
09/19/23 21:11
95-49-8
4-Chlorotoluene
ND
ug/kg
7.9
4.4
1
09/18/23 15:35
09/19/23 21:11
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
7.9
3.1
1
09/18/23 15:35
09/19/23 21:11
96-12-8
Dibromochloromethane
ND
ug/kg
7.9
4.5
1
09/18/23 15:35
09/19/23 21:11
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
7.9
3.5
1
09/18/23 15:35
09/19/23 21:11
106-93-4
Dibromomethane
ND
ug/kg
7.9
1.7
1
09/18/23 15:35
09/19/23 21:11
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
7.9
2.9
1
09/18/23 15:35
09/19/23 21:11
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
7.9
2.5
1
09/18/23 15:35
09/19/23 21:11
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
7.9
2.1
1
09/18/23 15:35
09/19/23 21:11
106-46-7
Dichlorodifluoromethane
ND
ug/kg
15.9
8.1
1
09/18/23 15:35
09/19/23 21:11
75-71-8
1,1-Dichloroethane
ND
ug/kg
7.9
3.3
1
09/18/23 15:35
09/19/23 21:11
75-34-3
1,2-Dichloroethane
ND
ug/kg
7.9
5.2
1
09/18/23 15:35
09/19/23 21:11
107-06-2
1,1-Dichloroethene
ND
ug/kg
7.9
3.3
1
09/18/23 15:35
09/19/23 21:11
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
7.9
2.7
1
09/18/23 15:35
09/19/23 21:11
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
7.9
6.7
1
09/18/23 15:35
09/19/23 21:11
156-60-5
1,2-Dichloropropane
ND
ug/kg
7.9
2.4
1
09/18/23 15:35
09/19/23 21:11
78-87-5
1,3-Dichloropropane
ND
ug/kg
7.9
2.5
1
09/18/23 15:35
09/19/23 21:11
142-28-9
2,2-Dichloropropane
ND
ug/kg
7.9
6.0
1
09/18/23 15:35
09/19/23 21:11
594-20-7
1,1-Dichloropropene
ND
ug/kg
7.9
3.8
1
09/18/23 15:35
09/19/23 21:11
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
7.9
2.2
1
09/18/23 15:35
09/19/23 21:11
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
7.9
2.7
1
09/18/23 15:35
09/19/23 21:11
10061-02-6
Diisopropyl ether
ND
ug/kg
7.9
2.1
1
09/18/23 15:35
09/19/23 21:11
108-20-3
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-8
Lab ID:
92688240008
Collected:
09/12/23
15:41
Received: 09/14/23
09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Ethylbenzene
ND
ug/kg
7.9
3.7
1
09/18/23 15:35
09/19/23 21:11
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
15.9
13.0
1
09/18/23 15:35
09/19/23 21:11
87-68-3
2-Hexanone
ND
ug/kg
79.3
7.6
1
09/18/23 15:35
09/19/23 21:11
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
7.9
2.7
1
09/18/23 15:35
09/19/23 21:11
98-82-8
p-Isopropyltoluene
ND
ug/kg
7.9
3.9
1
09/18/23 15:35
09/19/23 21:11
99-87-6
Methylene Chloride
ND
ug/kg
31.7
21.7
1
09/18/23 15:35
09/19/23 21:11
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
79.3
7.6
1
09/18/23 15:35
09/19/23 21:11
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
7.9
3.0
1
09/18/23 15:35
09/19/23 21:11
1634-04-4
Naphthalene
ND
ug/kg
7.9
4.2
1
09/18/23 15:35
09/19/23 21:11
91-20-3
n-Propylbenzene
ND
ug/kg
7.9
2.8
1
09/18/23 15:35
09/19/23 21:11
103-65-1
Styrene
ND
ug/kg
7.9
2.1
1
09/18/23 15:35
09/19/23 21:11
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
7.9
3.0
1
09/18/23 15:35
09/19/23 21:11
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
7.9
2.1
1
09/18/23 15:35
09/19/23 21:11
79-34-5
Tetrachloroethene
ND
ug/kg
7.9
2.5
1
09/18/23 15:35
09/19/23 21:11
127-18-4
Toluene
ND
ug/kg
7.9
5.5
1
09/18/23 15:35
09/19/23 21:11
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
7.9
6.4
1
09/18/23 15:35
09/19/23 21:11
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
7.9
6.7
1
09/18/23 15:35
09/19/23 21:11
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
7.9
4.1
1
09/18/23 15:35
09/19/23 21:11
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
7.9
2.6
1
09/18/23 15:35
09/19/23 21:11
79-00-5
Trichloroethene
ND
ug/kg
7.9
6.4
1
09/18/23 15:35
09/19/23 21:11
79-01-6
Trichlorofluoromethane
ND
ug/kg
7.9
4.4
1
09/18/23 15:35
09/19/23 21:11
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
7.9
4.0
1
09/18/23 15:35
09/19/23 21:11
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
7.9
4.7
1
09/18/23 15:35
09/19/23 21:11
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
7.9
2.7
1
09/18/23 15:35
09/19/23 21:11
108-67-8
Vinyl acetate
ND
ug/kg
79.3
16.3
1
09/18/23 15:35
09/19/23 21:11
108-05-4
Vinyl chloride
ND
ug/kg
15.9
4.0
1
09/18/23 15:35
09/19/23 21:11
75-01-4
Xylene (Total)
5.51
ug/kg
15.9
4.5
1
09/18/23 15:35
09/19/23 21:11
1330-20-7
m&p-Xylene
5.51
ug/kg
15.9
5.4
1
09/18/23 15:35
09/19/23 21:11
179601-23-1
o-Xylene
ND
ug/kg
7.9
3.5
1
09/18/23 15:35
09/19/23 21:11
95-47-6
Surrogates
Toluene-d8 (S)
101
%
70-130
1
09/18/23 15:35
09/19/23 21:11
2037-26-5
4-Bromofluorobenzene (S)
103
%
70-130
1
09/18/23 15:35
09/19/23 21:11
460-00-4
1,2-Dichloroethane-d4 (S)
102
%
70-130
1
09/18/23 15:35
09/19/23 21:11
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services - Charlotte
Percent Moisture
9.1
%
0.10
0.10
1
09/15/23 17:39
N2
Total Solids 2540 G-2011
Analytical
Method: SM 2540G Preparation Method:
SM
2540 G
Pace National
- Mt. Juliet
Total Solids
83.5
%
1
09/21/23 06:36
09/21/23 06:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-8 Lab ID: 92688240008 Collected: 09/12/23 15:41 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Wet Chemistry 7199 Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Chromium, Hexavalent 0.492J mg/kg 1.20 0.305 1 09/21/23 12:45 09/22/23 12:54 18540-29-9 J
Date: 09/25/2023 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 46 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-9 Lab ID: 92688240009 Collected: 09/12/23 15:53 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical
Services
- Ormond Beach
Arsenic
ND
mg/kg
0.66
0.33
1
09/22/2311:05
09/25/2311:39
7440-38-2
Barium
29.1
mg/kg
0.66
0.11
1
09/22/2311:05
09/25/2311:39
7440-39-3
Cadmium
0.13
mg/kg
0.066
0.033
1
09/22/2311:05
09/25/2311:39
7440-43-9
Chromium
9.5
mg/kg
0.33
0.16
1
09/22/2311:05
09/25/2311:39
7440-47-3
Lead
7.6
mg/kg
0.66
0.33
1
09/22/2311:05
09/25/2311:39
7439-92-1
Selenium
ND
mg/kg
0.98
0.49
1
09/22/2311:05
09/25/2311:39
7782-49-2
Silver
ND
mg/kg
0.33
0.072
1
09/22/2311:05
09/25/2311:39
7440-22-4
7471 Mercury
Analytical
Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical
Services
- Ormond Beach
Mercury
0.046
mg/kg
0.011
0.0055
1
09/21/2312:51
09/22/2310:27
7439-97-6
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation
Method: EPA
3546
Pace Analytical
Services
- Charlotte
Acenaphthene
ND
ug/kg
389
137
1
09/17/23 17:12
09/18/23 13:16
83-32-9
Acenaphthylene
ND
ug/kg
389
137
1
09/17/23 17:12
09/18/23 13:16
208-96-8
Aniline
ND
ug/kg
389
152
1
09/17/23 17:12
09/18/23 13:16
62-53-3
Anthracene
ND
ug/kg
389
127
1
09/17/23 17:12
09/18/23 13:16
120-12-7
Benzo(a)anthracene
ND
ug/kg
389
130
1
09/17/23 17:12
09/18/23 13:16
56-55-3
Benzo(a)pyrene
ND
ug/kg
389
134
1
09/17/23 17:12
09/18/23 13:16
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
389
130
1
09/17/23 17:12
09/18/23 13:16
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
389
151
1
09/17/23 17:12
09/18/23 13:16
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
389
137
1
09/17/23 17:12
09/18/23 13:16
207-08-9
Benzoic Acid
ND
ug/kg
1950
836
1
09/17/23 17:12
09/18/23 13:16
65-85-0
Benzyl alcohol
ND
ug/kg
778
295
1
09/17/23 17:12
09/18/23 13:16
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
389
150
1
09/17/23 17:12
09/18/23 13:16
101-55-3
Butylbenzylphthalate
ND
ug/kg
389
164
1
09/17/23 17:12
09/18/23 13:16
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
778
274
1
09/17/23 17:12
09/18/23 13:16
59-50-7
4-Chloroaniline
ND
ug/kg
778
305
1
09/17/23 17:12
09/18/23 13:16
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
389
162
1
09/17/23 17:12
09/18/23 13:16
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
389
146
1
09/17/23 17:12
09/18/23 13:16
111-44-4
2-Chloronaphthalene
ND
ug/kg
389
154
1
09/17/23 17:12
09/18/23 13:16
91-58-7
2-Chlorophenol
ND
ug/kg
389
146
1
09/17/23 17:12
09/18/23 13:16
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
389
145
1
09/17/23 17:12
09/18/23 13:16
7005-72-3
Chrysene
ND
ug/kg
389
141
1
09/17/23 17:12
09/18/23 13:16
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
389
150
1
09/17/23 17:12
09/18/23 13:16
53-70-3
Dibenzofuran
ND
ug/kg
389
140
1
09/17/23 17:12
09/18/23 13:16
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
389
140
1
09/17/23 17:12
09/18/23 13:16
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
389
138
1
09/17/23 17:12
09/18/23 13:16
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
389
149
1
09/17/23 17:12
09/18/23 13:16
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
778
263
1
09/17/23 17:12
09/18/23 13:16
91-94-1
2,4-Dichlorophenol
ND
ug/kg
389
152
1
09/17/23 17:12
09/18/23 13:16
120-83-2
Diethylphthalate
ND
ug/kg
389
143
1
09/17/23 17:12
09/18/23 13:16
84-66-2
2,4-Dimethylphenol
ND
ug/kg
389
162
1
09/17/23 17:12
09/18/23 13:16
105-67-9
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-9 Lab ID: 92688240009 Collected: 09/12/23 15:53 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Dimethylphthalate
ND
ug/kg
389
141
1
09/17/23 17:12
09/18/23 13:16
131-11-3
Di-n-butylphthalate
ND
ug/kg
389
131
1
09/17/23 17:12
09/18/23 13:16
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
778
363
1
09/17/23 17:12
09/18/23 13:16
534-52-1
2,4-Dinitrophenol
ND
ug/kg
1950
1200
1
09/17/23 17:12
09/18/23 13:16
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
389
150
1
09/17/23 17:12
09/18/23 13:16
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
389
143
1
09/17/23 17:12
09/18/23 13:16
606-20-2
Di-n-octylphthalate
ND
ug/kg
389
153
1
09/17/23 17:12
09/18/23 13:16
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
389
151
1
09/17/23 17:12
09/18/23 13:16
117-81-7
Fluoranthene
ND
ug/kg
389
133
1
09/17/23 17:12
09/18/23 13:16
206-44-0
Fluorene
ND
ug/kg
389
137
1
09/17/23 17:12
09/18/23 13:16
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
389
169
1
09/17/23 17:12
09/18/23 13:16
87-68-3
Hexachlorobenzene
ND
ug/kg
389
152
1
09/17/23 17:12
09/18/23 13:16
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
389
223
1
09/17/23 17:12
09/18/23 13:16
77-47-4
Hexachloroethane
ND
ug/kg
389
149
1
09/17/23 17:12
09/18/23 13:16
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
389
153
1
09/17/23 17:12
09/18/23 13:16
193-39-5
Isophorone
ND
ug/kg
389
173
1
09/17/23 17:12
09/18/23 13:16
78-59-1
1-Methylnaphthalene
ND
ug/kg
389
137
1
09/17/23 17:12
09/18/23 13:16
90-12-0
2-Methylnaphthalene
ND
ug/kg
389
156
1
09/17/23 17:12
09/18/23 13:16
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
389
159
1
09/17/23 17:12
09/18/23 13:16
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
389
157
1
09/17/23 17:12
09/18/23 13:16
15831-10-4
Naphthalene
ND
ug/kg
389
132
1
09/17/23 17:12
09/18/23 13:16
91-20-3
2-Nitroaniline
ND
ug/kg
1950
318
1
09/17/23 17:12
09/18/23 13:16
88-74-4
3-Nitroaniline
ND
ug/kg
1950
305
1
09/17/23 17:12
09/18/23 13:16
99-09-2
4-Nitroaniline
ND
ug/kg
778
296
1
09/17/23 17:12
09/18/23 13:16
100-01-6
Nitrobenzene
ND
ug/kg
389
180
1
09/17/23 17:12
09/18/23 13:16
98-95-3
2-Nitrophenol
ND
ug/kg
389
169
1
09/17/23 17:12
09/18/23 13:16
88-75-5
4-Nitrophenol
ND
ug/kg
1950
752
1
09/17/23 17:12
09/18/23 13:16
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
389
131
1
09/17/23 17:12
09/18/23 13:16
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
389
146
1
09/17/23 17:12
09/18/23 13:16
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
389
138
1
09/17/23 17:12
09/18/23 13:16
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
389
185
1
09/17/23 17:12
09/18/23 13:16
108-60-1
Pentachlorophenol
ND
ug/kg
778
381
1
09/17/23 17:12
09/18/23 13:16
87-86-5
Phenanthrene
ND
ug/kg
389
127
1
09/17/23 17:12
09/18/23 13:16
85-01-8
Phenol
ND
ug/kg
389
173
1
09/17/23 17:12
09/18/23 13:16
108-95-2
Pyrene
ND
ug/kg
389
158
1
09/17/23 17:12
09/18/23 13:16
129-00-0
Pyridine
ND
ug/kg
389
123
1
09/17/23 17:12
09/18/23 13:16
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
389
153
1
09/17/23 17:12
09/18/23 13:16
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
389
178
1
09/17/23 17:12
09/18/23 13:16
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
389
160
1
09/17/23 17:12
09/18/23 13:16
88-06-2
Surrogates
Nitrobenzene-d5 (S)
67
%
10-130
1
09/17/23 17:12
09/18/23 13:16
4165-60-0
2-Fluorobiphenyl (S)
51
%
10-130
1
09/17/23 17:12
09/18/23 13:16
321-60-8
Terphenyl-d14 (S)
65
%
10-130
1
09/17/23 17:12
09/18/23 13:16
1718-51-0
Phenol-d6 (S)
66
%
10-130
1
09/17/23 17:12
09/18/23 13:16
13127-88-3
REPORT OF LABORATORY ANALYSIS
v1
v1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-9 Lab ID: 92688240009 Collected: 09/12/23 15:53 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Surrogates
2-Fluorophenol (S)
62
%
10-130
1
09/17/23 17:12
09/18/23 13:16
367-12-4
2,4,6-Tribromophenol (S)
68
%
10-131
1
09/17/23 17:12
09/18/23 13:16
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation Method: EPA
5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
161
51.6
1
09/18/23 15:35
09/19/23 21:28
67-64-1
Benzene
ND
ug/kg
8.0
3.2
1
09/18/23 15:35
09/19/23 21:28
71-43-2
Bromobenzene
ND
ug/kg
8.0
2.6
1
09/18/23 15:35
09/19/23 21:28
108-86-1
Bromochloromethane
ND
ug/kg
8.0
2.4
1
09/18/23 15:35
09/19/23 21:28
74-97-5
Bromodichloromethane
ND
ug/kg
8.0
3.1
1
09/18/23 15:35
09/19/23 21:28
75-27-4
Bromoform
ND
ug/kg
8.0
2.8
1
09/18/23 15:35
09/19/23 21:28
75-25-2
Bromomethane
ND
ug/kg
32.1
24.9
1
09/18/23 15:35
09/19/23 21:28
74-83-9
2-Butanone (MEK)
ND
ug/kg
161
38.6
1
09/18/23 15:35
09/19/23 21:28
78-93-3
n-Butylbenzene
ND
ug/kg
8.0
5.1
1
09/18/23 15:35
09/19/23 21:28
104-51-8
sec-Butylbenzene
ND
ug/kg
8.0
3.5
1
09/18/23 15:35
09/19/23 21:28
135-98-8
tert-Butyl benzene
ND
ug/kg
8.0
2.9
1
09/18/23 15:35
09/19/23 21:28
98-06-6
Carbon tetrachloride
ND
ug/kg
8.0
3.0
1
09/18/23 15:35
09/19/23 21:28
56-23-5
Chlorobenzene
ND
ug/kg
8.0
4.6
1
09/18/23 15:35
09/19/23 21:28
108-90-7
Chloroethane
ND
ug/kg
16.1
6.2
1
09/18/23 15:35
09/19/23 21:28
75-00-3
Chloroform
ND
ug/kg
8.0
6.7
1
09/18/23 15:35
09/19/23 21:28
67-66-3
Chloromethane
ND
ug/kg
16.1
6.7
1
09/18/23 15:35
09/19/23 21:28
74-87-3
2-Chlorotoluene
ND
ug/kg
8.0
2.8
1
09/18/23 15:35
09/19/23 21:28
95-49-8
4-Chlorotoluene
ND
ug/kg
8.0
4.5
1
09/18/23 15:35
09/19/23 21:28
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
8.0
3.1
1
09/18/23 15:35
09/19/23 21:28
96-12-8
Dibromochloromethane
ND
ug/kg
8.0
4.5
1
09/18/23 15:35
09/19/23 21:28
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
8.0
3.5
1
09/18/23 15:35
09/19/23 21:28
106-93-4
Dibromomethane
ND
ug/kg
8.0
1.7
1
09/18/23 15:35
09/19/23 21:28
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
8.0
2.9
1
09/18/23 15:35
09/19/23 21:28
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
8.0
2.5
1
09/18/23 15:35
09/19/23 21:28
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
8.0
2.1
1
09/18/23 15:35
09/19/23 21:28
106-46-7
Dichlorodifluoromethane
ND
ug/kg
16.1
8.2
1
09/18/23 15:35
09/19/23 21:28
75-71-8
1,1-Dichloroethane
ND
ug/kg
8.0
3.3
1
09/18/23 15:35
09/19/23 21:28
75-34-3
1,2-Dichloroethane
ND
ug/kg
8.0
5.3
1
09/18/23 15:35
09/19/23 21:28
107-06-2
1,1-Dichloroethene
ND
ug/kg
8.0
3.3
1
09/18/23 15:35
09/19/23 21:28
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
8.0
2.7
1
09/18/23 15:35
09/19/23 21:28
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
8.0
6.8
1
09/18/23 15:35
09/19/23 21:28
156-60-5
1,2-Dichloropropane
ND
ug/kg
8.0
2.4
1
09/18/23 15:35
09/19/23 21:28
78-87-5
1,3-Dichloropropane
ND
ug/kg
8.0
2.5
1
09/18/23 15:35
09/19/23 21:28
142-28-9
2,2-Dichloropropane
ND
ug/kg
8.0
6.1
1
09/18/23 15:35
09/19/23 21:28
594-20-7
1,1-Dichloropropene
ND
ug/kg
8.0
3.9
1
09/18/23 15:35
09/19/23 21:28
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
8.0
2.2
1
09/18/23 15:35
09/19/23 21:28
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
8.0
2.8
1
09/18/23 15:35
09/19/23 21:28
10061-02-6
Diisopropyl ether
ND
ug/kg
8.0
2.2
1
09/18/23 15:35
09/19/23 21:28
108-20-3
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 49 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-9
Lab ID:
92688240009
Collected:
09/12/23
15:53
Received: 09/14/23
09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Ethylbenzene
9.2
ug/kg
8.0
3.7
1
09/18/23 15:35
09/19/23 21:28
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
16.1
13.1
1
09/18/23 15:35
09/19/23 21:28
87-68-3
2-Hexanone
ND
ug/kg
80.3
7.7
1
09/18/23 15:35
09/19/23 21:28
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
8.0
2.7
1
09/18/23 15:35
09/19/23 21:28
98-82-8
p-Isopropyltoluene
ND
ug/kg
8.0
4.0
1
09/18/23 15:35
09/19/23 21:28
99-87-6
Methylene Chloride
ND
ug/kg
32.1
22.0
1
09/18/23 15:35
09/19/23 21:28
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
80.3
7.7
1
09/18/23 15:35
09/19/23 21:28
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
8.0
3.0
1
09/18/23 15:35
09/19/23 21:28
1634-04-4
Naphthalene
ND
ug/kg
8.0
4.2
1
09/18/23 15:35
09/19/23 21:28
91-20-3
n-Propylbenzene
5AJ
ug/kg
8.0
2.9
1
09/18/23 15:35
09/19/23 21:28
103-65-1
Styrene
ND
ug/kg
8.0
2.1
1
09/18/23 15:35
09/19/23 21:28
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
8.0
3.1
1
09/18/23 15:35
09/19/23 21:28
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
8.0
2.1
1
09/18/23 15:35
09/19/23 21:28
79-34-5
Tetrachloroethene
ND
ug/kg
8.0
2.5
1
09/18/23 15:35
09/19/23 21:28
127-18-4
Toluene
21.4
ug/kg
8.0
5.5
1
09/18/23 15:35
09/19/23 21:28
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
8.0
6.5
1
09/18/23 15:35
09/19/23 21:28
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
8.0
6.7
1
09/18/23 15:35
09/19/23 21:28
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
8.0
4.2
1
09/18/23 15:35
09/19/23 21:28
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
8.0
2.7
1
09/18/23 15:35
09/19/23 21:28
79-00-5
Trichloroethene
ND
ug/kg
8.0
6.5
1
09/18/23 15:35
09/19/23 21:28
79-01-6
Trichlorofluoromethane
ND
ug/kg
8.0
4.4
1
09/18/23 15:35
09/19/23 21:28
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
8.0
4.1
1
09/18/23 15:35
09/19/23 21:28
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
8.0
4.8
1
09/18/23 15:35
09/19/23 21:28
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
8.0
2.7
1
09/18/23 15:35
09/19/23 21:28
108-67-8
Vinyl acetate
ND
ug/kg
80.3
16.5
1
09/18/23 15:35
09/19/23 21:28
108-05-4
Vinyl chloride
ND
ug/kg
16.1
4.1
1
09/18/23 15:35
09/19/23 21:28
75-01-4
Xylene (Total)
23.4
ug/kg
16.1
4.6
1
09/18/23 15:35
09/19/23 21:28
1330-20-7
m&p-Xylene
17.8
ug/kg
16.1
5.5
1
09/18/23 15:35
09/19/23 21:28
179601-23-1
o-Xylene
5.6J
ug/kg
8.0
3.6
1
09/18/23 15:35
09/19/23 21:28
95-47-6
Surrogates
Toluene-d8 (S)
100
%
70-130
1
09/18/23 15:35
09/19/23 21:28
2037-26-5
4-Bromofluorobenzene (S)
103
%
70-130
1
09/18/23 15:35
09/19/23 21:28
460-00-4
1,2-Dichloroethane-d4 (S)
103
%
70-130
1
09/18/23 15:35
09/19/23 21:28
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services - Charlotte
Percent Moisture
16.3
%
0.10
0.10
1
09/15/23 17:39
N2
Total Solids 2540 G-2011
Analytical
Method: SM 2540G Preparation Method:
SM
2540 G
Pace National
- Mt. Juliet
Total Solids
75.3
%
1
09/21/23 06:36
09/21/23 06:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 50 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-9 Lab ID: 92688240009 Collected: 09/12/23 15:53 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Wet Chemistry 7199 Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Chromium, Hexavalent 0.886J mg/kg 1.33 0.339 1 09/21/23 12:45 09/22/23 12:59 18540-29-9 J
Date: 09/25/2023 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 51 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-10 Lab ID: 92688240010 Collected: 09/12/23 16:44 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical
Services
- Ormond Beach
Arsenic
0.47J
mg/kg
0.54
0.27
1
09/22/2311:05
09/25/2311:42
7440-38-2
Barium
12.1
mg/kg
0.54
0.090
1
09/22/2311:05
09/25/2311:42
7440-39-3
Cadmium
0.040J
mg/kg
0.054
0.027
1
09/22/2311:05
09/25/2311:42
7440-43-9
Chromium
4.4
mg/kg
0.27
0.13
1
09/22/2311:05
09/25/2311:42
7440-47-3
Lead
2.8
mg/kg
0.54
0.27
1
09/22/2311:05
09/25/2311:42
7439-92-1
Selenium
ND
mg/kg
0.80
0.40
1
09/22/2311:05
09/25/2311:42
7782-49-2
Silver
ND
mg/kg
0.27
0.059
1
09/22/2311:05
09/25/2311:42
7440-22-4
7471 Mercury
Analytical
Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical
Services
- Ormond Beach
Mercury
0.019
mg/kg
0.0085
0.0043
1
09/21/2312:51
09/22/2310:29
7439-97-6
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation
Method: EPA
3546
Pace Analytical
Services
- Charlotte
Acenaphthene
ND
ug/kg
359
126
1
09/17/23 17:12
09/18/23 13:44
83-32-9
Acenaphthylene
ND
ug/kg
359
126
1
09/17/23 17:12
09/18/23 13:44
208-96-8
Aniline
ND
ug/kg
359
141
1
09/17/23 17:12
09/18/23 13:44
62-53-3
Anthracene
ND
ug/kg
359
118
1
09/17/23 17:12
09/18/23 13:44
120-12-7
Benzo(a)anthracene
ND
ug/kg
359
120
1
09/17/23 17:12
09/18/23 13:44
56-55-3
Benzo(a)pyrene
ND
ug/kg
359
124
1
09/17/23 17:12
09/18/23 13:44
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
359
120
1
09/17/23 17:12
09/18/23 13:44
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
359
139
1
09/17/23 17:12
09/18/23 13:44
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
359
126
1
09/17/23 17:12
09/18/23 13:44
207-08-9
Benzoic Acid
ND
ug/kg
1800
772
1
09/17/23 17:12
09/18/23 13:44
65-85-0
Benzyl alcohol
ND
ug/kg
719
272
1
09/17/23 17:12
09/18/23 13:44
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
359
138
1
09/17/23 17:12
09/18/23 13:44
101-55-3
Butylbenzylphthalate
ND
ug/kg
359
151
1
09/17/23 17:12
09/18/23 13:44
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
719
253
1
09/17/23 17:12
09/18/23 13:44
59-50-7
4-Chloroaniline
ND
ug/kg
719
282
1
09/17/23 17:12
09/18/23 13:44
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
359
149
1
09/17/23 17:12
09/18/23 13:44
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
359
135
1
09/17/23 17:12
09/18/23 13:44
111-44-4
2-Chloronaphthalene
ND
ug/kg
359
143
1
09/17/23 17:12
09/18/23 13:44
91-58-7
2-Chlorophenol
ND
ug/kg
359
135
1
09/17/23 17:12
09/18/23 13:44
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
359
134
1
09/17/23 17:12
09/18/23 13:44
7005-72-3
Chrysene
ND
ug/kg
359
131
1
09/17/23 17:12
09/18/23 13:44
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
359
138
1
09/17/23 17:12
09/18/23 13:44
53-70-3
Dibenzofuran
ND
ug/kg
359
130
1
09/17/23 17:12
09/18/23 13:44
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
359
130
1
09/17/23 17:12
09/18/23 13:44
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
359
127
1
09/17/23 17:12
09/18/23 13:44
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
359
137
1
09/17/23 17:12
09/18/23 13:44
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
719
243
1
09/17/23 17:12
09/18/23 13:44
91-94-1
2,4-Dichlorophenol
ND
ug/kg
359
141
1
09/17/23 17:12
09/18/23 13:44
120-83-2
Diethylphthalate
ND
ug/kg
359
132
1
09/17/23 17:12
09/18/23 13:44
84-66-2
2,4-Dimethylphenol
ND
ug/kg
359
149
1
09/17/23 17:12
09/18/23 13:44
105-67-9
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 52 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-10 Lab ID: 92688240010 Collected: 09/12/23 16:44 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Dimethylphthalate
ND
ug/kg
359
131
1
09/17/23 17:12
09/18/23 13:44
131-11-3
Di-n-butylphthalate
ND
ug/kg
359
121
1
09/17/23 17:12
09/18/23 13:44
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
719
336
1
09/17/23 17:12
09/18/23 13:44
534-52-1
2,4-Dinitrophenol
ND
ug/kg
1800
1110
1
09/17/23 17:12
09/18/23 13:44
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
359
138
1
09/17/23 17:12
09/18/23 13:44
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
359
132
1
09/17/23 17:12
09/18/23 13:44
606-20-2
Di-n-octylphthalate
ND
ug/kg
359
142
1
09/17/23 17:12
09/18/23 13:44
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
359
139
1
09/17/23 17:12
09/18/23 13:44
117-81-7
Fluoranthene
ND
ug/kg
359
123
1
09/17/23 17:12
09/18/23 13:44
206-44-0
Fluorene
ND
ug/kg
359
126
1
09/17/23 17:12
09/18/23 13:44
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
359
156
1
09/17/23 17:12
09/18/23 13:44
87-68-3
Hexachlorobenzene
ND
ug/kg
359
141
1
09/17/23 17:12
09/18/23 13:44
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
359
206
1
09/17/23 17:12
09/18/23 13:44
77-47-4
Hexachloroethane
ND
ug/kg
359
137
1
09/17/23 17:12
09/18/23 13:44
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
359
142
1
09/17/23 17:12
09/18/23 13:44
193-39-5
Isophorone
ND
ug/kg
359
160
1
09/17/23 17:12
09/18/23 13:44
78-59-1
1-Methylnaphthalene
ND
ug/kg
359
126
1
09/17/23 17:12
09/18/23 13:44
90-12-0
2-Methylnaphthalene
ND
ug/kg
359
144
1
09/17/23 17:12
09/18/23 13:44
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
359
147
1
09/17/23 17:12
09/18/23 13:44
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
359
145
1
09/17/23 17:12
09/18/23 13:44
15831-10-4
Naphthalene
ND
ug/kg
359
122
1
09/17/23 17:12
09/18/23 13:44
91-20-3
2-Nitroaniline
ND
ug/kg
1800
294
1
09/17/23 17:12
09/18/23 13:44
88-74-4
3-Nitroaniline
ND
ug/kg
1800
282
1
09/17/23 17:12
09/18/23 13:44
99-09-2
4-Nitroaniline
ND
ug/kg
719
273
1
09/17/23 17:12
09/18/23 13:44
100-01-6
Nitrobenzene
ND
ug/kg
359
167
1
09/17/23 17:12
09/18/23 13:44
98-95-3
2-Nitrophenol
ND
ug/kg
359
156
1
09/17/23 17:12
09/18/23 13:44
88-75-5
4-Nitrophenol
ND
ug/kg
1800
695
1
09/17/23 17:12
09/18/23 13:44
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
359
121
1
09/17/23 17:12
09/18/23 13:44
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
359
135
1
09/17/23 17:12
09/18/23 13:44
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
359
127
1
09/17/23 17:12
09/18/23 13:44
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
359
171
1
09/17/23 17:12
09/18/23 13:44
108-60-1
Pentachlorophenol
ND
ug/kg
719
352
1
09/17/23 17:12
09/18/23 13:44
87-86-5
Phenanthrene
ND
ug/kg
359
118
1
09/17/23 17:12
09/18/23 13:44
85-01-8
Phenol
ND
ug/kg
359
160
1
09/17/23 17:12
09/18/23 13:44
108-95-2
Pyrene
ND
ug/kg
359
146
1
09/17/23 17:12
09/18/23 13:44
129-00-0
Pyridine
ND
ug/kg
359
113
1
09/17/23 17:12
09/18/23 13:44
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
359
142
1
09/17/23 17:12
09/18/23 13:44
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
359
164
1
09/17/23 17:12
09/18/23 13:44
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
359
148
1
09/17/23 17:12
09/18/23 13:44
88-06-2
Surrogates
Nitrobenzene-d5 (S)
68
%
10-130
1
09/17/23 17:12
09/18/23 13:44
4165-60-0
2-Fluorobiphenyl (S)
60
%
10-130
1
09/17/23 17:12
09/18/23 13:44
321-60-8
Terphenyl-d14 (S)
69
%
10-130
1
09/17/23 17:12
09/18/23 13:44
1718-51-0
Phenol-d6 (S)
66
%
10-130
1
09/17/23 17:12
09/18/23 13:44
13127-88-3
REPORT OF LABORATORY ANALYSIS
v1
v1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 53 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-10 Lab ID: 92688240010 Collected: 09/12/23 16:44 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Surrogates
2-Fluorophenol (S)
62
%
10-130
1
09/17/23 17:12
09/18/23 13:44
367-12-4
2,4,6-Tribromophenol (S)
70
%
10-131
1
09/17/23 17:12
09/18/23 13:44
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation Method: EPA
5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
113
36.4
1
09/18/23 15:35
09/19/23 22:03
67-64-1
Benzene
ND
ug/kg
5.7
2.3
1
09/18/23 15:35
09/19/23 22:03
71-43-2
Bromobenzene
ND
ug/kg
5.7
1.8
1
09/18/23 15:35
09/19/23 22:03
108-86-1
Bromochloromethane
ND
ug/kg
5.7
1.7
1
09/18/23 15:35
09/19/23 22:03
74-97-5
Bromodichloromethane
ND
ug/kg
5.7
2.2
1
09/18/23 15:35
09/19/23 22:03
75-27-4
Bromoform
ND
ug/kg
5.7
2.0
1
09/18/23 15:35
09/19/23 22:03
75-25-2
Bromomethane
ND
ug/kg
22.7
17.6
1
09/18/23 15:35
09/19/23 22:03
74-83-9
2-Butanone (MEK)
ND
ug/kg
113
27.2
1
09/18/23 15:35
09/19/23 22:03
78-93-3
n-Butylbenzene
ND
ug/kg
5.7
3.6
1
09/18/23 15:35
09/19/23 22:03
104-51-8
sec-Butylbenzene
ND
ug/kg
5.7
2.5
1
09/18/23 15:35
09/19/23 22:03
135-98-8
tert-Butyl benzene
ND
ug/kg
5.7
2.0
1
09/18/23 15:35
09/19/23 22:03
98-06-6
Carbon tetrachloride
ND
ug/kg
5.7
2.1
1
09/18/23 15:35
09/19/23 22:03
56-23-5
Chlorobenzene
ND
ug/kg
5.7
3.3
1
09/18/23 15:35
09/19/23 22:03
108-90-7
Chloroethane
ND
ug/kg
11.3
4.4
1
09/18/23 15:35
09/19/23 22:03
75-00-3
Chloroform
ND
ug/kg
5.7
4.7
1
09/18/23 15:35
09/19/23 22:03
67-66-3
Chloromethane
ND
ug/kg
11.3
4.8
1
09/18/23 15:35
09/19/23 22:03
74-87-3
2-Chlorotoluene
ND
ug/kg
5.7
2.0
1
09/18/23 15:35
09/19/23 22:03
95-49-8
4-Chlorotoluene
ND
ug/kg
5.7
3.2
1
09/18/23 15:35
09/19/23 22:03
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
5.7
2.2
1
09/18/23 15:35
09/19/23 22:03
96-12-8
Dibromochloromethane
ND
ug/kg
5.7
3.2
1
09/18/23 15:35
09/19/23 22:03
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
5.7
2.5
1
09/18/23 15:35
09/19/23 22:03
106-93-4
Dibromomethane
ND
ug/kg
5.7
1.2
1
09/18/23 15:35
09/19/23 22:03
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
5.7
2.0
1
09/18/23 15:35
09/19/23 22:03
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
5.7
1.8
1
09/18/23 15:35
09/19/23 22:03
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
5.7
1.5
1
09/18/23 15:35
09/19/23 22:03
106-46-7
Dichlorodifluoromethane
ND
ug/kg
11.3
5.8
1
09/18/23 15:35
09/19/23 22:03
75-71-8
1,1-Dichloroethane
ND
ug/kg
5.7
2.3
1
09/18/23 15:35
09/19/23 22:03
75-34-3
1,2-Dichloroethane
ND
ug/kg
5.7
3.8
1
09/18/23 15:35
09/19/23 22:03
107-06-2
1,1-Dichloroethene
ND
ug/kg
5.7
2.3
1
09/18/23 15:35
09/19/23 22:03
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
5.7
1.9
1
09/18/23 15:35
09/19/23 22:03
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
5.7
4.8
1
09/18/23 15:35
09/19/23 22:03
156-60-5
1,2-Dichloropropane
ND
ug/kg
5.7
1.7
1
09/18/23 15:35
09/19/23 22:03
78-87-5
1,3-Dichloropropane
ND
ug/kg
5.7
1.8
1
09/18/23 15:35
09/19/23 22:03
142-28-9
2,2-Dichloropropane
ND
ug/kg
5.7
4.3
1
09/18/23 15:35
09/19/23 22:03
594-20-7
1,1-Dichloropropene
ND
ug/kg
5.7
2.7
1
09/18/23 15:35
09/19/23 22:03
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
5.7
1.5
1
09/18/23 15:35
09/19/23 22:03
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
5.7
2.0
1
09/18/23 15:35
09/19/23 22:03
10061-02-6
Diisopropyl ether
ND
ug/kg
5.7
1.5
1
09/18/23 15:35
09/19/23 22:03
108-20-3
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 54 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-10 Lab ID: 92688240010 Collected: 09/12/23 16:44 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Ethylbenzene
4.7J
ug/kg
5.7
2.6
1
09/18/23 15:35
09/19/23 22:03
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
11.3
9.3
1
09/18/23 15:35
09/19/23 22:03
87-68-3
2-Hexanone
ND
ug/kg
56.7
5.5
1
09/18/23 15:35
09/19/23 22:03
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
5.7
1.9
1
09/18/23 15:35
09/19/23 22:03
98-82-8
p-Isopropyltoluene
ND
ug/kg
5.7
2.8
1
09/18/23 15:35
09/19/23 22:03
99-87-6
Methylene Chloride
33.2
ug/kg
22.7
15.5
1
09/18/23 15:35
09/19/23 22:03
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
56.7
5.5
1
09/18/23 15:35
09/19/23 22:03
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
5.7
2.1
1
09/18/23 15:35
09/19/23 22:03
1634-04-4
Naphthalene
ND
ug/kg
5.7
3.0
1
09/18/23 15:35
09/19/23 22:03
91-20-3
n-Propylbenzene
ND
ug/kg
5.7
2.0
1
09/18/23 15:35
09/19/23 22:03
103-65-1
Styrene
ND
ug/kg
5.7
1.5
1
09/18/23 15:35
09/19/23 22:03
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
5.7
2.2
1
09/18/23 15:35
09/19/23 22:03
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
5.7
1.5
1
09/18/23 15:35
09/19/23 22:03
79-34-5
Tetrachloroethene
ND
ug/kg
5.7
1.8
1
09/18/23 15:35
09/19/23 22:03
127-18-4
Toluene
8.3
ug/kg
5.7
3.9
1
09/18/23 15:35
09/19/23 22:03
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
5.7
4.6
1
09/18/23 15:35
09/19/23 22:03
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
5.7
4.8
1
09/18/23 15:35
09/19/23 22:03
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
5.7
3.0
1
09/18/23 15:35
09/19/23 22:03
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
5.7
1.9
1
09/18/23 15:35
09/19/23 22:03
79-00-5
Trichloroethene
ND
ug/kg
5.7
4.6
1
09/18/23 15:35
09/19/23 22:03
79-01-6
Trichlorofluoromethane
ND
ug/kg
5.7
3.1
1
09/18/23 15:35
09/19/23 22:03
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
5.7
2.9
1
09/18/23 15:35
09/19/23 22:03
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
5.7
3.4
1
09/18/23 15:35
09/19/23 22:03
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
5.7
1.9
1
09/18/23 15:35
09/19/23 22:03
108-67-8
Vinyl acetate
ND
ug/kg
56.7
11.7
1
09/18/23 15:35
09/19/23 22:03
108-05-4
Vinyl chloride
ND
ug/kg
11.3
2.9
1
09/18/23 15:35
09/19/23 22:03
75-01-4
Xylene (Total)
8.3J
ug/kg
11.3
3.2
1
09/18/23 15:35
09/19/23 22:03
1330-20-7
m&p-Xylene
8.3J
ug/kg
11.3
3.9
1
09/18/23 15:35
09/19/23 22:03
179601-23-1
o-Xylene
ND
ug/kg
5.7
2.5
1
09/18/23 15:35
09/19/23 22:03
95-47-6
Surrogates
Toluene-d8 (S)
100
%
70-130
1
09/18/23 15:35
09/19/23 22:03
2037-26-5
4-Bromofluorobenzene (S)
102
%
70-130
1
09/18/23 15:35
09/19/23 22:03
460-00-4
1,2-Dichloroethane-d4 (S)
103
%
70-130
1
09/18/23 15:35
09/19/23 22:03
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
7.0
%
0.10
0.10
1
09/15/23 17:40
Total Solids 2540 G-2011
Analytical
Method: SM 2540G Preparation Method:
SM 2540 G
Pace National - Mt. Juliet
Total Solids
88.7
%
1
09/21/23 06:36
09/21/23 06:42
REPORT OF LABORATORY ANALYSIS
C9
N2
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 55 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: JOB #1487
Pace Project No.: 92688240
Sample: FG-10 Lab ID: 92688240010 Collected: 09/12/23 16:44 Received: 09/14/23 09:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Wet Chemistry 7199 Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Chromium, Hexavalent 0.452J mg/kg 1.13 0.287 1 09/21/23 12:45 09/22/23 13:05 18540-29-9 J
Date: 09/25/2023 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 56 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
QC Batch: 951692 Analysis Method: EPA 7471
QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Laboratory: Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92688240001, 92688240002, 92688240003, 92688240004, 92688240005, 92688240006, 92688240007,
92688240008,92688240009,92688240010
METHOD BLANK: 5232288 Matrix: Solid
Associated Lab Samples: 92688240001, 92688240002, 92688240003, 92688240004, 92688240005, 92688240006, 92688240007,
92688240008,92688240009,92688240010
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Mercury mg/kg ND 0.0094 0.0047 09/22/23 09:32
LABORATORY CONTROL SAMPLE: 5232289
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg 0.091 0.090 99 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 5232290 5232291
MS MSD
35827396001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Mercury mg/kg 0.18 0.105 0.105 0.16 0.17 -13 -4 80-120 5 20 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 57 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
QC Batch: 952019 Analysis Method: EPA 6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET Solid
Laboratory: Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92688240001, 92688240002, 92688240003, 92688240004, 92688240005, 92688240006, 92688240007,
92688240008,92688240009,92688240010
METHOD BLANK: 5234724
Matrix:
Solid
Associated Lab Samples:
92688240001, 92688240002,
92688240003, 92688240004, 92688240005, 92688240006,
92688240007,
92688240008,92688240009,92688240010
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
Arsenic
mg/kg
ND
0.56
0.28
09/25/2310:45
Barium
mg/kg
ND
0.56
0.094
09/25/2310:45
Cadmium
mg/kg
ND
0.056
0.028
09/25/2310:45
Chromium
mg/kg
ND
0.28
0.14
09/25/2310:45
Lead
mg/kg
ND
0.56
0.28
09/25/2310:45
Selenium
mg/kg
ND
0.84
0.42
09/25/2310:45
Silver
mg/kg
ND
0.28
0.062
09/25/2310:45
LABORATORY CONTROL SAMPLE:
Parameter
5234725
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
13.7
13.4
98
80-120
Barium
mg/kg
13.7
14.3
105
80-120
Cadmium
mg/kg
1.4
1.4
103
80-120
Chromium
mg/kg
13.7
14.0
103
80-120
Lead
mg/kg
13.7
14.4
106
80-120
Selenium
mg/kg
13.7
13.8
101
80-120
Silver
mg/kg
1.4
1.4
102
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 5234726
5234727
MS
MSD
35828873003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Arsenic
mg/kg
0.291-1
15.2
14.9
14.1
14.0
91
92
75-125
1
20
Barium
mg/kg
3.5
15.2
14.9
19.8
19.5
108
107
75-125
2
20
Cadmium
mg/kg
0.0291-1
1.5
1.5
1.5
1.5
98
98
75-125
1
20
Chromium
mg/kg
2.0
15.2
14.9
18.0
18.0
105
107
75-125
0
20
Lead
mg/kg
1.3
15.2
14.9
16.3
16.2
99
100
75-125
0
20
Selenium
mg/kg
0.44U
15.2
14.9
14.4
14.4
94
96
75-125
0
20
Silver
mg/kg
0.0651-1
1.5
1.5
1.5
1.5
95
98
75-125
2
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 58 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
QC Batch: 800123 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92688240001, 92688240002, 92688240003, 92688240004, 92688240005, 92688240006, 92688240007
METHOD BLANK: 4144549 Matrix: Solid
Associated Lab Samples: 92688240001, 92688240002, 92688240003, 92688240004, 92688240005, 92688240006, 92688240007
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.0
1.9
09/16/23 01:00 IK
1,1,1-Trichloroethane
ug/kg
ND
5.0
2.6
09/16/23 01:00
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.0
1.3
09/16/23 01:00
1,1,2-Trichloroethane
ug/kg
ND
5.0
1.7
09/16/23 01:00
1,1-Dichloroethane
ug/kg
ND
5.0
2.1
09/16/23 01:00
1,1-Dichloroethene
ug/kg
ND
5.0
2.1
09/16/23 01:00
1,1-Dichloropropene
ug/kg
ND
5.0
2.4
09/16/23 01:00
1,2,3-Trichlorobenzene
ug/kg
ND
5.0
4.0
09/16/23 01:00
1,2,3-Trichloropropane
ug/kg
ND
5.0
2.5
09/16/23 01:00
1,2,4-Trichlorobenzene
ug/kg
ND
5.0
4.2
09/16/23 01:00
1,2,4-Trimethylbenzene
ug/kg
ND
5.0
3.0
09/16/23 01:00
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.0
1.9
09/16/23 01:00
1,2-Dibromoethane (EDB)
ug/kg
ND
5.0
2.2
09/16/23 01:00
1,2-Dichlorobenzene
ug/kg
ND
5.0
1.8
09/16/23 01:00
1,2-Dichloroethane
ug/kg
ND
5.0
3.3
09/16/23 01:00
1,2-Dichloropropane
ug/kg
ND
5.0
1.5
09/16/23 01:00
1,3,5-Trimethylbenzene
ug/kg
ND
5.0
1.7
09/16/23 01:00
1,3-Dichlorobenzene
ug/kg
ND
5.0
1.6
09/16/23 01:00
1,3-Dichloropropane
ug/kg
ND
5.0
1.6
09/16/23 01:00
1,4-Dichlorobenzene
ug/kg
ND
5.0
1.3
09/16/23 01:00
2,2-Dichloropropane
ug/kg
ND
5.0
3.8
09/16/23 01:00
2-Butanone (MEK)
ug/kg
ND
100
24.0
09/16/23 01:00
2-Chlorotoluene
ug/kg
ND
5.0
1.8
09/16/23 01:00
2-Hexanone
ug/kg
ND
50.0
4.8
09/16/23 01:00
4-Chlorotoluene
ug/kg
ND
5.0
2.8
09/16/23 01:00
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
50.0
4.8
09/16/23 01:00
Acetone
ug/kg
ND
100
32.1
09/16/23 01:00
Benzene
ug/kg
ND
5.0
2.0
09/16/23 01:00
Bromobenzene
ug/kg
ND
5.0
1.6
09/16/23 01:00
Bromochloromethane
ug/kg
ND
5.0
1.5
09/16/23 01:00
Bromodichloromethane
ug/kg
ND
5.0
1.9
09/16/23 01:00
Bromoform
ug/kg
ND
5.0
1.8
09/16/23 01:00
Bromomethane
ug/kg
ND
20.0
15.5
09/16/23 01:00
Carbon tetrachloride
ug/kg
ND
5.0
1.9
09/16/23 01:00
Chlorobenzene
ug/kg
ND
5.0
2.9
09/16/23 01:00
Chloroethane
ug/kg
ND
10.0
3.9
09/16/23 01:00
Chloroform
ug/kg
ND
5.0
4.2
09/16/23 01:00
Chloromethane
ug/kg
ND
10.0
4.2
09/16/23 01:00 v1
cis-1,2-Dichloroethene
ug/kg
ND
5.0
1.7
09/16/23 01:00
cis-1,3-Dichloropropene
ug/kg
ND
5.0
1.4
09/16/23 01:00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 59 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
METHOD BLANK: 4144549 Matrix: Solid
Associated Lab Samples: 92688240001, 92688240002, 92688240003, 92688240004, 92688240005, 92688240006, 92688240007
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Dibromochloromethane
ug/kg
ND
5.0
2.8
09/16/23 01:00
Dibromomethane
ug/kg
ND
5.0
1.1
09/16/23 01:00
Dichlorodifluoromethane
ug/kg
ND
10.0
5.1
09/16/23 01:00 IH,v1
Diisopropyl ether
ug/kg
ND
5.0
1.4
09/16/23 01:00
Ethylbenzene
ug/kg
ND
5.0
2.3
09/16/23 01:00
Hexachloro-1,3-butadiene
ug/kg
ND
10.0
8.2
09/16/23 01:00
Isopropylbenzene (Cumene)
ug/kg
ND
5.0
1.7
09/16/23 01:00
m&p-Xylene
ug/kg
ND
10.0
3.4
09/16/23 01:00
Methyl-tert-butyl ether
ug/kg
ND
5.0
1.9
09/16/23 01:00
Methylene Chloride
ug/kg
ND
20.0
13.7
09/16/23 01:00
n-Butylbenzene
ug/kg
ND
5.0
3.2
09/16/23 01:00
n-Propylbenzene
ug/kg
ND
5.0
1.8
09/16/23 01:00
Naphthalene
ug/kg
ND
5.0
2.6
09/16/23 01:00
o-Xylene
ug/kg
ND
5.0
2.2
09/16/23 01:00
p-Isopropyltoluene
ug/kg
ND
5.0
2.5
09/16/23 01:00
sec-Butylbenzene
ug/kg
ND
5.0
2.2
09/16/23 01:00
Styrene
ug/kg
ND
5.0
1.3
09/16/23 01:00
tert-Butyl benzene
ug/kg
ND
5.0
1.8
09/16/23 01:00
Tetrachloroethene
ug/kg
ND
5.0
1.6
09/16/23 01:00
Toluene
ug/kg
ND
5.0
3.4
09/16/23 01:00
trans-1,2-Dichloroethene
ug/kg
ND
5.0
4.2
09/16/23 01:00
trans- 1,3-Dichloropropene
ug/kg
ND
5.0
1.7
09/16/23 01:00
Trichloroethene
ug/kg
ND
5.0
4.0
09/16/23 01:00
Trichlorofluoromethane
ug/kg
ND
5.0
2.8
09/16/23 01:00
Vinyl acetate
ug/kg
ND
50.0
10.3
09/16/23 01:00
Vinyl chloride
ug/kg
ND
10.0
2.5
09/16/23 01:00 v1
Xylene (Total)
ug/kg
ND
10.0
2.8
09/16/23 01:00
1,2-Dichloroethane-d4 (S)
%
106
70-130
09/16/23 01:00
4-Bromofluorobenzene (S)
%
100
70-130
09/16/23 01:00
Toluene-d8 (S)
%
100
70-130
09/16/23 01:00
LABORATORY CONTROL SAMPLE:
Parameter
4144550
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
500
604
121
70-130IK
1,1,1-Trichloroethane
ug/kg
500
612
122
70-130
1,1,2,2-Tetrachloroethane
ug/kg
500
590
118
70-130
1,1,2-Trichloroethane
ug/kg
500
575
115
70-130
1,1-Dichloroethane
ug/kg
500
610
122
70-130
1,1-Dichloroethene
ug/kg
500
684
137
70-132 L1
1,1-Dichloropropene
ug/kg
500
606
121
70-130
1,2,3-Trichlorobenzene
ug/kg
500
562
112
62-136
1,2,3-Trichloropropane
ug/kg
500
556
111
70-130
1,2,4-Trichlorobenzene
ug/kg
500
576
115
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 60 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: JOB #1487
Pace Project No.: 92688240
LABORATORY CONTROL SAMPLE: 4144550
Parameter
QUALITY CONTROL DATA
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits Qualifiers
1,2,4-Trimethylbenzene
ug/kg
500
584
117
70-130
1,2-Dibromo-3-chloropropane
ug/kg
500
512
102
65-130
1,2-Dibromoethane (EDB)
ug/kg
500
584
117
70-130
1,2-Dichlorobenzene
ug/kg
500
563
113
70-130
1,2-Dichloroethane
ug/kg
500
584
117
70-130
1,2-Dichloropropane
ug/kg
500
572
114
70-130
1,3,5-Trimethylbenzene
ug/kg
500
581
116
70-130
1,3-Dichlorobenzene
ug/kg
500
570
114
70-130
1,3-Dichloropropane
ug/kg
500
554
111
70-130
1,4-Dichlorobenzene
ug/kg
500
539
108
70-130
2,2-Dichloropropane
ug/kg
500
622
124
60-130
2-Butanone (MEK)
ug/kg
1000
1090
109
66-130
2-Chlorotoluene
ug/kg
500
588
118
70-130
2-Hexanone
ug/kg
1000
1130
113
68-130
4-Chlorotoluene
ug/kg
500
581
116
70-130
4-Methyl-2-pentanone (MIBK)
ug/kg
1000
1090
109
70-130
Acetone
ug/kg
1000
1100
110
60-130
Benzene
ug/kg
500
568
114
70-130
Bromobenzene
ug/kg
500
576
115
70-130
Bromochloromethane
ug/kg
500
556
111
70-130
Bromodichloromethane
ug/kg
500
581
116
70-130
Bromoform
ug/kg
500
586
117
70-130
Bromomethane
ug/kg
500
548
110
43-175
Carbon tetrachloride
ug/kg
500
648
130
70-130
Chlorobenzene
ug/kg
500
588
118
70-130
Chloroethane
ug/kg
500
684
137
70-145
Chloroform
ug/kg
500
596
119
70-130
Chloromethane
ug/kg
500
747
149
66-146 L1,v1
cis-1,2-Dichloroethene
ug/kg
500
620
124
70-130
cis-1,3-Dichloropropene
ug/kg
500
539
108
70-130
Dibromochloromethane
ug/kg
500
593
119
70-130
Dibromomethane
ug/kg
500
550
110
70-130
Dichlorodifluoromethane
ug/kg
500
1280
256
42-1971H,L1,v1
Diisopropyl ether
ug/kg
500
552
110
68-130
Ethylbenzene
ug/kg
500
550
110
70-130
Hexachloro-1,3-butadiene
ug/kg
500
567
113
70-130
Isopropylbenzene(Cumene)
ug/kg
500
606
121
70-130
m&p-Xylene
ug/kg
1000
1180
118
70-130
Methyl-tert-butyl ether
ug/kg
500
515
103
70-130
Methylene Chloride
ug/kg
500
579
116
65-130
n-Butylbenzene
ug/kg
500
584
117
70-130
n-Propylbenzene
ug/kg
500
569
114
70-130
Naphthalene
ug/kg
500
558
112
65-135
o-Xylene
ug/kg
500
599
120
70-130
p-Isopropyltoluene
ug/kg
500
598
120
70-130
sec-Butylbenzene
ug/kg
500
568
114
70-130
Styrene
ug/kg
500
588
118
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 61 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
LABORATORY CONTROL SAMPLE:
Parameter
4144550
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
tert-Butyl benzene
ug/kg
500
555
111
70-130
Tetrachloroethene
ug/kg
500
611
122
70-130
Toluene
ug/kg
500
567
113
70-130
trans-1,2-Dichloroethene
ug/kg
500
651
130
70-130
trans- 1,3-Dichloropropene
ug/kg
500
554
111
70-130
Trichloroethene
ug/kg
500
609
122
70-130
Trichlorofluoromethane
ug/kg
500
644
129
62-140
Vinyl acetate
ug/kg
1000
1160
116
70-140
Vinyl chloride
ug/kg
500
648
130
70-152 v1
Xylene (Total)
ug/kg
1500
1780
119
70-130
1,2-Dichloroethane-d4 (S)
%
105
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE SAMPLE:
Parameter
4144551
Units
92688232016
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
588
496
84
22-1661K
1,1,1-Trichloroethane
ug/kg
ND
588
534
91
23-172
1,1,2,2-Tetrachloroethane
ug/kg
ND
588
490
83
21-158
1,1,2-Trichloroethane
ug/kg
ND
588
502
85
25-160
1,1-Dichloroethane
ug/kg
ND
588
536
91
22-166
1,1-Dichloroethene
ug/kg
ND
588
597
102
18-183
1,1-Dichloropropene
ug/kg
ND
588
546
93
20-181
1,2,3-Trichlorobenzene
ug/kg
ND
588
465
79
10-161
1,2,3-Trichloropropane
ug/kg
ND
588
458
78
21-147
1,2,4-Trichlorobenzene
ug/kg
ND
588
469
80
10-159
1,2,4-Trimethylbenzene
ug/kg
ND
588
481
82
17-170
1,2-Dibromo-3-chloropropane
ug/kg
ND
588
419
71
10-135
1,2-Dibromoethane (EDB)
ug/kg
ND
588
475
81
30-154
1,2-Dichlorobenzene
ug/kg
ND
588
482
82
26-162
1,2-Dichloroethane
ug/kg
ND
588
500
85
23-161
1,2-Dichloropropane
ug/kg
ND
588
520
88
29-165
1,3,5-Trimethylbenzene
ug/kg
ND
588
490
83
20-172
1,3-Dichlorobenzene
ug/kg
ND
588
491
83
22-164
1,3-Dichloropropane
ug/kg
ND
588
470
80
27-156
1,4-Dichlorobenzene
ug/kg
ND
588
434
74
20-161
2,2-Dichloropropane
ug/kg
ND
588
519
88
10-159
2-Butanone (MEK)
ug/kg
ND
1170
938
80
13-143
2-Chlorotoluene
ug/kg
ND
588
490
83
21-166
2-Hexanone
ug/kg
ND
1170
909
77
19-145
4-Chlorotoluene
ug/kg
ND
588
482
82
19-163
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
1170
933
79
21-151
Acetone
ug/kg
ND
1170
759
65
10-133
Benzene
ug/kg
ND
588
508
86
29-156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 62 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
MATRIX SPIKE SAMPLE:
Parameter
4144551
Units
92688232016
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Bromobenzene
ug/kg
ND
588
482
82
25-161
Bromochloromethane
ug/kg
ND
588
476
81
27-158
Bromodichloromethane
ug/kg
ND
588
492
84
23-158
Bromoform
ug/kg
ND
588
453
77
19-152
Bromomethane
ug/kg
ND
588
88.3
15
10-152
Carbon tetrachloride
ug/kg
ND
588
558
95
18-172
Chlorobenzene
ug/kg
ND
588
498
85
26-166
Chloroethane
ug/kg
ND
588
123
21
10-130
Chloroform
ug/kg
ND
588
527
90
25-161
Chloromethane
ug/kg
ND
588
690
117
27-197 v1
cis-1,2-Dichloroethene
ug/kg
ND
588
544
93
28-165
cis-1,3-Dichloropropene
ug/kg
ND
588
465
79
23-159
Dibromochloromethane
ug/kg
ND
588
472
80
21-151
Dibromomethane
ug/kg
ND
588
459
78
38-158
Dichlorodifluoromethane
ug/kg
ND
588
1690
288
10-2001H,MO,v1
Diisopropyl ether
ug/kg
ND
588
489
83
23-160
Ethylbenzene
ug/kg
ND
588
471
80
22-163
Hexachloro-1,3-butadiene
ug/kg
ND
588
495
84
10-192
Isopropylbenzene (Cumene)
ug/kg
ND
588
518
88
24-173
m&p-Xylene
ug/kg
ND
1170
988
84
22-171
Methyl-tert-butyl ether
ug/kg
ND
588
437
74
25-153
Methylene Chloride
ug/kg
31.8
588
511
82
10-165
n-Butylbenzene
ug/kg
ND
588
483
82
10-186
n-Propylbenzene
ug/kg
ND
588
491
84
16-171
Naphthalene
ug/kg
ND
588
453
77
10-159
o-Xylene
ug/kg
ND
588
505
86
23-171
p-Isopropyltoluene
ug/kg
ND
588
494
84
13-184
sec-Butylbenzene
ug/kg
ND
588
488
83
16-182
Styrene
ug/kg
ND
588
492
84
25-169
tert-Butyl benzene
ug/kg
ND
588
380
65
20-174
Tetrachloroethene
ug/kg
ND
588
479
82
14-171
Toluene
ug/kg
ND
588
503
86
24-166
trans-1,2-Dichloroethene
ug/kg
ND
588
560
95
24-170
trans- 1,3-Dichloropropene
ug/kg
ND
588
473
80
22-157
Trichloroethene
ug/kg
ND
588
540
92
23-176
Trichlorofluoromethane
ug/kg
ND
588
116
20
10-138
Vinyl acetate
ug/kg
ND
1170
835
71
11-166
Vinyl chloride
ug/kg
ND
588
604
103
21-200 v1
Xylene (Total)
ug/kg
ND
1770
1490
85
23-170
1,2-Dichloroethane-d4 (S)
%
116
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8(S)
%
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 63 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
SAMPLE DUPLICATE: 4144552
92688232017 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
ND
301K
1,1,1-Trichloroethane
ug/kg
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/kg
ND
ND
30
1,1,2-Trichloroethane
ug/kg
ND
ND
30
1,1-Dichloroethane
ug/kg
ND
ND
30
1,1-Dichloroethene
ug/kg
ND
ND
30
1,1-Dichloropropene
ug/kg
ND
ND
30
1,2,3-Trichlorobenzene
ug/kg
ND
ND
30
1,2,3-Trichloropropane
ug/kg
ND
ND
30
1,2,4-Trichlorobenzene
ug/kg
ND
ND
30
1,2,4-Trimethylbenzene
ug/kg
ND
ND
30
1,2-Dibromo-3-chloropropane
ug/kg
ND
ND
30
1,2-Dibromoethane (EDB)
ug/kg
ND
ND
30
1,2-Dichlorobenzene
ug/kg
ND
ND
30
1,2-Dichloroethane
ug/kg
ND
ND
30
1,2-Dichloropropane
ug/kg
ND
ND
30
1,3,5-Trimethylbenzene
ug/kg
ND
ND
30
1,3-Dichlorobenzene
ug/kg
ND
ND
30
1,3-Dichloropropane
ug/kg
ND
ND
30
1,4-Dichlorobenzene
ug/kg
ND
ND
30
2,2-Dichloropropane
ug/kg
ND
ND
30
2-Butanone (MEK)
ug/kg
ND
ND
30
2-Chlorotoluene
ug/kg
ND
ND
30
2-Hexanone
ug/kg
ND
ND
30
4-Chlorotoluene
ug/kg
ND
ND
30
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
ND
30
Acetone
ug/kg
ND
ND
30
Benzene
ug/kg
ND
ND
30
Bromobenzene
ug/kg
ND
ND
30
Bromochloromethane
ug/kg
ND
ND
30
Bromodichloromethane
ug/kg
ND
ND
30
Bromoform
ug/kg
ND
ND
30
Bromomethane
ug/kg
ND
ND
30
Carbon tetrachloride
ug/kg
ND
ND
30
Chlorobenzene
ug/kg
ND
ND
30
Chloroethane
ug/kg
ND
ND
30
Chloroform
ug/kg
ND
ND
30
Chloromethane
ug/kg
ND
ND
30 v1
cis-1,2-Dichloroethene
ug/kg
ND
ND
30
cis-1,3-Dichloropropene
ug/kg
ND
ND
30
Dibromochloromethane
ug/kg
ND
ND
30
Dibromomethane
ug/kg
ND
ND
30
Dichlorodifluoromethane
ug/kg
ND
ND
301H,v1
Diisopropyl ether
ug/kg
ND
ND
30
Ethylbenzene
ug/kg
ND
ND
30
Hexachloro-1,3-butadiene
ug/kg
ND
ND
30
Isopropylbenzene (Cumene)
ug/kg
ND
ND
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 64 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
SAMPLE DUPLICATE: 4144552
Parameter
Units
92688232017
Result
Dup
Result
m&p-Xylene
ug/kg
ND
ND
Methyl-tert-butyl ether
ug/kg
ND
ND
Methylene Chloride
ug/kg
ND
ND
n-Butylbenzene
ug/kg
ND
ND
n-Propylbenzene
ug/kg
ND
ND
Naphthalene
ug/kg
ND
ND
o-Xylene
ug/kg
ND
ND
p-Isopropyltoluene
ug/kg
ND
ND
sec-Butylbenzene
ug/kg
ND
ND
Styrene
ug/kg
ND
ND
tert-Butyl benzene
ug/kg
ND
ND
Tetrachloroethene
ug/kg
625
643
Toluene
ug/kg
ND
ND
trans-1,2-Dichloroethene
ug/kg
ND
ND
trans- 1,3-Dichloropropene
ug/kg
ND
ND
Trichloroethene
ug/kg
ND
ND
Trichlorofluoromethane
ug/kg
ND
ND
Vinyl acetate
ug/kg
ND
ND
Vinyl chloride
ug/kg
ND
ND
Xylene (Total)
ug/kg
ND
ND
1,2-Dichloroethane-d4 (S)
%
106
106
4-Bromofluorobenzene (S)
%
101
102
Toluene-d8(S)
%
101
101
Max
RPD RPD
3
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30 v1
30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 65 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
QC Batch: 800345 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92688240008, 92688240009, 92688240010
METHOD BLANK: 4145467 Matrix:
Associated Lab Samples: 92688240008, 92688240009, 92688240010
Blank
Parameter Units Result
Solid
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.0
1.9
09/19/23 20:53
1,1,1-Trichloroethane
ug/kg
ND
5.0
2.6
09/19/23 20:53
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.0
1.3
09/19/23 20:53
1,1,2-Trichloroethane
ug/kg
ND
5.0
1.7
09/19/23 20:53
1,1-Dichloroethane
ug/kg
ND
5.0
2.1
09/19/23 20:53
1,1-Dichloroethene
ug/kg
ND
5.0
2.1
09/19/23 20:53
1,1-Dichloropropene
ug/kg
ND
5.0
2.4
09/19/23 20:53
1,2,3-Trichlorobenzene
ug/kg
ND
5.0
4.0
09/19/23 20:53
1,2,3-Trichloropropane
ug/kg
ND
5.0
2.5
09/19/23 20:53
1,2,4-Trichlorobenzene
ug/kg
ND
5.0
4.2
09/19/23 20:53
1,2,4-Trimethylbenzene
ug/kg
ND
5.0
3.0
09/19/23 20:53
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.0
1.9
09/19/23 20:53
1,2-Dibromoethane (EDB)
ug/kg
ND
5.0
2.2
09/19/23 20:53
1,2-Dichlorobenzene
ug/kg
ND
5.0
1.8
09/19/23 20:53
1,2-Dichloroethane
ug/kg
ND
5.0
3.3
09/19/23 20:53
1,2-Dichloropropane
ug/kg
ND
5.0
1.5
09/19/23 20:53
1,3,5-Trimethylbenzene
ug/kg
ND
5.0
1.7
09/19/23 20:53
1,3-Dichlorobenzene
ug/kg
ND
5.0
1.6
09/19/23 20:53
1,3-Dichloropropane
ug/kg
ND
5.0
1.6
09/19/23 20:53
1,4-Dichlorobenzene
ug/kg
ND
5.0
1.3
09/19/23 20:53
2,2-Dichloropropane
ug/kg
ND
5.0
3.8
09/19/23 20:53
2-Butanone (MEK)
ug/kg
ND
100
24.0
09/19/23 20:53
2-Chlorotoluene
ug/kg
ND
5.0
1.8
09/19/23 20:53
2-Hexanone
ug/kg
ND
50.0
4.8
09/19/23 20:53
4-Chlorotoluene
ug/kg
ND
5.0
2.8
09/19/23 20:53
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
50.0
4.8
09/19/23 20:53
Acetone
ug/kg
ND
100
32.1
09/19/23 20:53
Benzene
ug/kg
ND
5.0
2.0
09/19/23 20:53
Bromobenzene
ug/kg
ND
5.0
1.6
09/19/23 20:53
Bromochloromethane
ug/kg
ND
5.0
1.5
09/19/23 20:53
Bromodichloromethane
ug/kg
ND
5.0
1.9
09/19/23 20:53
Bromoform
ug/kg
ND
5.0
1.8
09/19/23 20:53
Bromomethane
ug/kg
ND
20.0
15.5
09/19/23 20:53
Carbon tetrachloride
ug/kg
ND
5.0
1.9
09/19/23 20:53
Chlorobenzene
ug/kg
ND
5.0
2.9
09/19/23 20:53
Chloroethane
ug/kg
ND
10.0
3.9
09/19/23 20:53
Chloroform
ug/kg
ND
5.0
4.2
09/19/23 20:53
Chloromethane
ug/kg
ND
10.0
4.2
09/19/23 20:53
cis-1,2-Dichloroethene
ug/kg
ND
5.0
1.7
09/19/23 20:53
cis-1,3-Dichloropropene
ug/kg
ND
5.0
1.4
09/19/23 20:53
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 66 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
METHOD BLANK: 4145467 Matrix:
Associated Lab Samples: 92688240008, 92688240009, 92688240010
Blank
Parameter Units Result
Solid
Reporting
Limit
MDL
Analyzed
Dibromochloromethane
ug/kg
ND
5.0
2.8
09/19/23 20:53
Dibromomethane
ug/kg
ND
5.0
1.1
09/19/23 20:53
Dichlorodifluoromethane
ug/kg
ND
10.0
5.1
09/19/23 20:53
Diisopropyl ether
ug/kg
ND
5.0
1.4
09/19/23 20:53
Ethylbenzene
ug/kg
ND
5.0
2.3
09/19/23 20:53
Hexachloro-1,3-butadiene
ug/kg
ND
10.0
8.2
09/19/23 20:53
Isopropylbenzene (Cumene)
ug/kg
ND
5.0
1.7
09/19/23 20:53
m&p-Xylene
ug/kg
ND
10.0
3.4
09/19/23 20:53
Methyl-tert-butyl ether
ug/kg
ND
5.0
1.9
09/19/23 20:53
Methylene Chloride
ug/kg
ND
20.0
13.7
09/19/23 20:53
n-Butylbenzene
ug/kg
ND
5.0
3.2
09/19/23 20:53
n-Propylbenzene
ug/kg
ND
5.0
1.8
09/19/23 20:53
Naphthalene
ug/kg
ND
5.0
2.6
09/19/23 20:53
o-Xylene
ug/kg
ND
5.0
2.2
09/19/23 20:53
p-Isopropyltoluene
ug/kg
ND
5.0
2.5
09/19/23 20:53
sec-Butylbenzene
ug/kg
ND
5.0
2.2
09/19/23 20:53
Styrene
ug/kg
ND
5.0
1.3
09/19/23 20:53
tert-Butyl benzene
ug/kg
ND
5.0
1.8
09/19/23 20:53
Tetrachloroethene
ug/kg
ND
5.0
1.6
09/19/23 20:53
Toluene
ug/kg
ND
5.0
3.4
09/19/23 20:53
trans-1,2-Dichloroethene
ug/kg
ND
5.0
4.2
09/19/23 20:53
trans- 1,3-Dichloropropene
ug/kg
ND
5.0
1.7
09/19/23 20:53
Trichloroethene
ug/kg
ND
5.0
4.0
09/19/23 20:53
Trichlorofluoromethane
ug/kg
ND
5.0
2.8
09/19/23 20:53
Vinyl acetate
ug/kg
ND
50.0
10.3
09/19/23 20:53
Vinyl chloride
ug/kg
ND
10.0
2.5
09/19/23 20:53
Xylene (Total)
ug/kg
ND
10.0
2.8
09/19/23 20:53
1,2-Dichloroethane-d4 (S)
%
100
70-130
09/19/23 20:53
4-Bromofluorobenzene (S)
%
99
70-130
09/19/23 20:53
Toluene-d8 (S)
%
100
70-130
09/19/23 20:53
v1
Qualifiers
LABORATORY CONTROL SAMPLE:
4145468
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
500
558
112
70-130
1,1,1-Trichloroethane
ug/kg
500
520
104
70-130
1,1,2,2-Tetrachloroethane
ug/kg
500
562
112
70-130
1,1,2-Trichloroethane
ug/kg
500
532
106
70-130
1,1-Dichloroethane
ug/kg
500
523
105
70-130
1,1-Dichloroethene
ug/kg
500
561
112
70-132
1,1-Dichloropropene
ug/kg
500
556
111
70-130
1,2,3-Trichlorobenzene
ug/kg
500
499
100
62-136
1,2,3-Trichloropropane
ug/kg
500
549
110
70-130
1,2,4-Trichlorobenzene
ug/kg
500
494
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 67 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
LABORATORY CONTROL SAMPLE:
Parameter
4145468
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trimethylbenzene
ug/kg
500
541
108
70-130
1,2-Dibromo-3-chloropropane
ug/kg
500
528
106
65-130
1,2-Dibromoethane (EDB)
ug/kg
500
551
110
70-130
1,2-Dichlorobenzene
ug/kg
500
519
104
70-130
1,2-Dichloroethane
ug/kg
500
535
107
70-130
1,2-Dichloropropane
ug/kg
500
544
109
70-130
1,3,5-Trimethylbenzene
ug/kg
500
525
105
70-130
1,3-Dichlorobenzene
ug/kg
500
530
106
70-130
1,3-Dichloropropane
ug/kg
500
541
108
70-130
1,4-Dichlorobenzene
ug/kg
500
515
103
70-130
2,2-Dichloropropane
ug/kg
500
478
96
60-130
2-Butanone (MEK)
ug/kg
1000
971
97
66-130
2-Chlorotoluene
ug/kg
500
535
107
70-130
2-Hexanone
ug/kg
1000
1060
106
68-130
4-Chlorotoluene
ug/kg
500
534
107
70-130
4-Methyl-2-pentanone (MIBK)
ug/kg
1000
1040
104
70-130
Acetone
ug/kg
1000
953
95
60-130
Benzene
ug/kg
500
511
102
70-130
Bromobenzene
ug/kg
500
545
109
70-130
Bromochloromethane
ug/kg
500
495
99
70-130
Bromodichloromethane
ug/kg
500
520
104
70-130
Bromoform
ug/kg
500
554
111
70-130
Bromomethane
ug/kg
500
551
110
43-175
Carbon tetrachloride
ug/kg
500
510
102
70-130
Chlorobenzene
ug/kg
500
524
105
70-130
Chloroethane
ug/kg
500
526
105
70-145
Chloroform
ug/kg
500
532
106
70-130
Chloromethane
ug/kg
500
521
104
66-146
cis-1,2-Dichloroethene
ug/kg
500
521
104
70-130
cis-1,3-Dichloropropene
ug/kg
500
511
102
70-130
Dibromochloromethane
ug/kg
500
536
107
70-130
Dibromomethane
ug/kg
500
548
110
70-130
Dichlorodifluoromethane
ug/kg
500
693
139
42-197 v1
Diisopropyl ether
ug/kg
500
504
101
68-130
Ethylbenzene
ug/kg
500
486
97
70-130
Hexachloro-1,3-butadiene
ug/kg
500
508
102
70-130
Isopropylbenzene(Cumene)
ug/kg
500
546
109
70-130
m&p-Xylene
ug/kg
1000
1060
106
70-130
Methyl-tert-butyl ether
ug/kg
500
488
98
70-130
Methylene Chloride
ug/kg
500
494
99
65-130
n-Butylbenzene
ug/kg
500
534
107
70-130
n-Propylbenzene
ug/kg
500
528
106
70-130
Naphthalene
ug/kg
500
554
111
65-135
o-Xylene
ug/kg
500
539
108
70-130
p-Isopropyltoluene
ug/kg
500
531
106
70-130
sec-Butylbenzene
ug/kg
500
528
106
70-130
Styrene
ug/kg
500
561
112
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 68 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
LABORATORY CONTROL SAMPLE:
Parameter
4145468
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
tert-Butyl benzene
ug/kg
500
511
102
70-130
Tetrachloroethene
ug/kg
500
522
104
70-130
Toluene
ug/kg
500
515
103
70-130
trans-1,2-Dichloroethene
ug/kg
500
538
108
70-130
trans- 1,3-Dichloropropene
ug/kg
500
500
100
70-130
Trichloroethene
ug/kg
500
530
106
70-130
Trichlorofluoromethane
ug/kg
500
495
99
62-140
Vinyl acetate
ug/kg
1000
999
100
70-140
Vinyl chloride
ug/kg
500
483
97
70-152
Xylene (Total)
ug/kg
1500
1600
107
70-130
1,2-Dichloroethane-d4 (S)
%
100
70-130
4-Bromofluorobenzene (S)
%
102
70-130
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE SAMPLE:
Parameter
4145469
Units
92688240008
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
793
756
95
22-166
1,1,1-Trichloroethane
ug/kg
ND
793
764
96
23-172
1,1,2,2-Tetrachloroethane
ug/kg
ND
793
674
85
21-158
1,1,2-Trichloroethane
ug/kg
ND
793
717
90
25-160
1,1-Dichloroethane
ug/kg
ND
793
760
96
22-166
1,1-Dichloroethene
ug/kg
ND
793
828
104
18-183
1,1-Dichloropropene
ug/kg
ND
793
685
86
20-181
1,2,3-Trichlorobenzene
ug/kg
ND
793
518
65
10-161
1,2,3-Trichloropropane
ug/kg
ND
793
638
80
21-147
1,2,4-Trichlorobenzene
ug/kg
ND
793
498
63
10-159
1,2,4-Trimethylbenzene
ug/kg
ND
793
637
80
17-170
1,2-Dibromo-3-chloropropane
ug/kg
ND
793
583
74
10-135
1,2-Dibromoethane (EDB)
ug/kg
ND
793
700
88
30-154
1,2-Dichlorobenzene
ug/kg
ND
793
661
83
26-162
1,2-Dichloroethane
ug/kg
ND
793
722
91
23-161
1,2-Dichloropropane
ug/kg
ND
793
779
98
29-165
1,3,5-Trimethylbenzene
ug/kg
ND
793
655
83
20-172
1,3-Dichlorobenzene
ug/kg
ND
793
633
80
22-164
1,3-Dichloropropane
ug/kg
ND
793
909
115
27-156
1,4-Dichlorobenzene
ug/kg
ND
793
616
78
20-161
2,2-Dichloropropane
ug/kg
ND
793
514
65
10-159
2-Butanone (MEK)
ug/kg
ND
1580
1170
74
13-143
2-Chlorotoluene
ug/kg
ND
793
692
87
21-166
2-Hexanone
ug/kg
ND
1580
1140
72
19-145
4-Chlorotoluene
ug/kg
ND
793
661
83
19-163
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
1580
1190
75
21-151
Acetone
ug/kg
ND
1580
1060
67
10-133
Benzene
ug/kg
ND
793
744
94
29-156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 69 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
MATRIX SPIKE SAMPLE:
Parameter
4145469
Units
92688240008
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Bromobenzene
ug/kg
ND
793
743
94
25-161
Bromochloromethane
ug/kg
ND
793
673
85
27-158
Bromodichloromethane
ug/kg
ND
793
728
92
23-158
Bromoform
ug/kg
ND
793
645
81
19-152
Bromomethane
ug/kg
ND
793
282
36
10-152
Carbon tetrachloride
ug/kg
ND
793
748
94
18-172
Chlorobenzene
ug/kg
ND
793
704
89
26-166
Chloroethane
ug/kg
ND
793
295
37
10-130
Chloroform
ug/kg
ND
793
750
95
25-161
Chloromethane
ug/kg
ND
793
784
99
27-197
cis-1,2-Dichloroethene
ug/kg
ND
793
756
95
28-165
cis-1,3-Dichloropropene
ug/kg
ND
793
672
85
23-159
Dibromochloromethane
ug/kg
ND
793
697
88
21-151
Dibromomethane
ug/kg
ND
793
730
92
38-158
Dichlorodifluoromethane
ug/kg
ND
793
1040
131
10-200 v1
Diisopropyl ether
ug/kg
ND
793
675
85
23-160
Ethylbenzene
ug/kg
ND
793
634
80
22-163
Hexachloro-1,3-butadiene
ug/kg
ND
793
480
60
10-192
Isopropylbenzene (Cumene)
ug/kg
ND
793
675
85
24-173
m&p-Xylene
ug/kg
5.5J
1580
1330
83
22-171
Methyl-tert-butyl ether
ug/kg
ND
793
641
81
25-153
Methylene Chloride
ug/kg
ND
793
751
95
10-165
n-Butylbenzene
ug/kg
ND
793
534
67
10-186
n-Propylbenzene
ug/kg
ND
793
622
78
16-171
Naphthalene
ug/kg
ND
793
631
80
10-159
o-Xylene
ug/kg
ND
793
712
90
23-171
p-Isopropyltoluene
ug/kg
ND
793
571
72
13-184
sec-Butylbenzene
ug/kg
ND
793
633
80
16-182
Styrene
ug/kg
ND
793
716
90
25-169
tert-Butyl benzene
ug/kg
ND
793
609
77
20-174
Tetrachloroethene
ug/kg
ND
793
550
69
14-171
Toluene
ug/kg
ND
793
704
88
24-166
trans-1,2-Dichloroethene
ug/kg
ND
793
675
85
24-170
trans- 1,3-Dichloropropene
ug/kg
ND
793
626
79
22-157
Trichloroethene
ug/kg
ND
793
686
87
23-176
Trichlorofluoromethane
ug/kg
ND
793
412
52
10-138
Vinyl acetate
ug/kg
ND
1580
1170
74
11-166
Vinyl chloride
ug/kg
ND
793
629
79
21-200
Xylene (Total)
ug/kg
5.5J
2380
2040
86
23-170
1,2-Dichloroethane-d4 (S)
%
95
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 70 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
SAMPLE DUPLICATE: 4145470
Parameter
Units
92688240009
Result
Dup
Result RPD
Max
RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
ND
30
1,1,1-Trichloroethane
ug/kg
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/kg
ND
ND
30
1,1,2-Trichloroethane
ug/kg
ND
ND
30
1,1-Dichloroethane
ug/kg
ND
ND
30
1,1-Dichloroethene
ug/kg
ND
ND
30
1,1-Dichloropropene
ug/kg
ND
ND
30
1,2,3-Trichlorobenzene
ug/kg
ND
ND
30
1,2,3-Trichloropropane
ug/kg
ND
ND
30
1,2,4-Trichlorobenzene
ug/kg
ND
ND
30
1,2,4-Trimethylbenzene
ug/kg
ND
ND
30
1,2-Dibromo-3-chloropropane
ug/kg
ND
ND
30
1,2-Dibromoethane (EDB)
ug/kg
ND
ND
30
1,2-Dichlorobenzene
ug/kg
ND
ND
30
1,2-Dichloroethane
ug/kg
ND
ND
30
1,2-Dichloropropane
ug/kg
ND
ND
30
1,3,5-Trimethylbenzene
ug/kg
ND
ND
30
1,3-Dichlorobenzene
ug/kg
ND
ND
30
1,3-Dichloropropane
ug/kg
ND
ND
30
1,4-Dichlorobenzene
ug/kg
ND
ND
30
2,2-Dichloropropane
ug/kg
ND
ND
30
2-Butanone (MEK)
ug/kg
ND
ND
30
2-Chlorotoluene
ug/kg
ND
ND
30
2-Hexanone
ug/kg
ND
ND
30
4-Chlorotoluene
ug/kg
ND
ND
30
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
ND
30
Acetone
ug/kg
ND
ND
30
Benzene
ug/kg
ND
ND
30
Bromobenzene
ug/kg
ND
ND
30
Bromochloromethane
ug/kg
ND
ND
30
Bromodichloromethane
ug/kg
ND
ND
30
Bromoform
ug/kg
ND
ND
30
Bromomethane
ug/kg
ND
ND
30
Carbon tetrachloride
ug/kg
ND
ND
30
Chlorobenzene
ug/kg
ND
ND
30
Chloroethane
ug/kg
ND
ND
30
Chloroform
ug/kg
ND
ND
30
Chloromethane
ug/kg
ND
ND
30
cis-1,2-Dichloroethene
ug/kg
ND
ND
30
cis-1,3-Dichloropropene
ug/kg
ND
ND
30
Dibromochloromethane
ug/kg
ND
ND
30
Dibromomethane
ug/kg
ND
ND
30
Dichlorodifluoromethane
ug/kg
ND
ND
30 v1
Diisopropyl ether
ug/kg
ND
ND
30
Ethylbenzene
ug/kg
9.2
9.1 2
30
Hexachloro-1,3-butadiene
ug/kg
ND
ND
30
Isopropylbenzene (Cumene)
ug/kg
ND
ND
30
Results presented on this page are in the units
indicated by the "Units" column except where an alternate unit is presented
to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 71 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
SAMPLE DUPLICATE: 4145470
Parameter
Units
92688240009
Result
Dup
Result
m&p-Xylene
ug/kg
17.8
18.2
Methyl-tert-butyl ether
ug/kg
ND
ND
Methylene Chloride
ug/kg
ND
ND
n-Butylbenzene
ug/kg
ND
ND
n-Propylbenzene
ug/kg
5AJ
5.1J
Naphthalene
ug/kg
ND
ND
o-Xylene
ug/kg
5.6J
5.9J
p-Isopropyltoluene
ug/kg
ND
7.OJ
sec-Butylbenzene
ug/kg
ND
ND
Styrene
ug/kg
ND
ND
tert-Butyl benzene
ug/kg
ND
ND
Tetrachloroethene
ug/kg
ND
ND
Toluene
ug/kg
21.4
23.7
trans-1,2-Dichloroethene
ug/kg
ND
ND
trans- 1,3-Dichloropropene
ug/kg
ND
ND
Trichloroethene
ug/kg
ND
ND
Trichlorofluoromethane
ug/kg
ND
ND
Vinyl acetate
ug/kg
ND
ND
Vinyl chloride
ug/kg
ND
ND
Xylene (Total)
ug/kg
23.4
18.2
1,2-Dichloroethane-d4 (S)
%
103
102
4-Bromofluorobenzene (S)
%
103
102
Toluene-d8 (S)
%
100
100
IVV
Max
RPD
2 30
30
30
30
30
30
30
30
30
30
30
30
10 30
30
30
30
30
30
30
25 30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 72 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
QC Batch: 800183 Analysis Method: EPA 8270E
QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92688240001, 92688240002, 92688240003, 92688240004, 92688240005, 92688240006, 92688240007,
92688240008,92688240009,92688240010
METHOD BLANK: 4144696 Matrix: Solid
Associated Lab Samples: 92688240001, 92688240002, 92688240003, 92688240004, 92688240005, 92688240006, 92688240007,
92688240008,92688240009,92688240010
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
1,2,4-Trichlorobenzene
ug/kg
ND
329
130
09/18/23 08:10
1,2-Dichlorobenzene
ug/kg
ND
329
119
09/18/23 08:10
1,3-Dichlorobenzene
ug/kg
ND
329
117
09/18/23 08:10
1,4-Dichlorobenzene
ug/kg
ND
329
126
09/18/23 08:10
1-Methylnaphthalene
ug/kg
ND
329
116
09/18/23 08:10
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
329
156
09/18/23 08:10
2,4,5-Trichlorophenol
ug/kg
ND
329
150
09/18/23 08:10
2,4,6-Trichlorophenol
ug/kg
ND
329
136
09/18/23 08:10
2,4-DichIorophenol
ug/kg
ND
329
129
09/18/23 08:10
2,4-Dimethylphenol
ug/kg
ND
329
137
09/18/23 08:10
2,4-Dinitrophenol
ug/kg
ND
1640
1020
09/18/23 08:10
2,4-Dinitrotoluene
ug/kg
ND
329
127
09/18/23 08:10
2,6-Dinitrotoluene
ug/kg
ND
329
121
09/18/23 08:10
2-Chloronaphthalene
ug/kg
ND
329
131
09/18/23 08:10
2-Chlorophenol
ug/kg
ND
329
124
09/18/23 08:10
2-Methylnaphthalene
ug/kg
ND
329
132
09/18/23 08:10
2-Methylphenol(o-Cresol)
ug/kg
ND
329
135
09/18/23 08:10
2-Nitroaniline
ug/kg
ND
1640
269
09/18/23 08:10
2-Nitrophenol
ug/kg
ND
329
143
09/18/23 08:10
3&4-Methylphenol (m&p Cresol)
ug/kg
ND
329
133
09/18/23 08:10
3,3'-Dichlorobenzidine
ug/kg
ND
658
222
09/18/23 08:10
3-Nitroaniline
ug/kg
ND
1640
258
09/18/23 08:10
4,6-Dinitro-2-methyl phenol
ug/kg
ND
658
307
09/18/23 08:10
4-Bromophenylphenyl ether
ug/kg
ND
329
127
09/18/23 08:10
4-Chloro-3-methyl phenol
ug/kg
ND
658
231
09/18/23 08:10
4-Chloroaniline
ug/kg
ND
658
258
09/18/23 08:10
4-Chlorophenylphenyl ether
ug/kg
ND
329
123
09/18/23 08:10
4-Nitroaniline
ug/kg
ND
658
250
09/18/23 08:10
4-Nitrophenol
ug/kg
ND
1640
636
09/18/23 08:10
Acenaphthene
ug/kg
ND
329
116
09/18/23 08:10
Acenaphthylene
ug/kg
ND
329
116
09/18/23 08:10
Aniline
ug/kg
ND
329
129
09/18/23 08:10
Anthracene
ug/kg
ND
329
108
09/18/23 08:10
Benzo(a)anthracene
ug/kg
ND
329
110
09/18/23 08:10
Benzo(a)pyrene
ug/kg
ND
329
114
09/18/23 08:10
Benzo(b)fluoranthene
ug/kg
ND
329
110
09/18/23 08:10
Benzo(g,h,i)perylene
ug/kg
ND
329
128
09/18/23 08:10
Benzo(k)fluoranthene
ug/kg
ND
329
116
09/18/23 08:10
Benzoic Acid
ug/kg
ND
1640
707
09/18/23 08:10 v1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 73 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
METHOD BLANK: 4144696 Matrix: Solid
Associated Lab Samples: 92688240001, 92688240002, 92688240003, 92688240004, 92688240005, 92688240006, 92688240007,
92688240008,92688240009,92688240010
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Benzyl alcohol
ug/kg
ND
658
249
09/18/23 08:10
bis(2-Chloroethoxy)methane
ug/kg
ND
329
137
09/18/23 08:10
bis(2-Chloroethyl) ether
ug/kg
ND
329
124
09/18/23 08:10
bis(2-Ethylhexyl)phthalate
ug/kg
ND
329
128
09/18/23 08:10
Butylbenzylphthalate
ug/kg
ND
329
139
09/18/23 08:10
Chrysene
ug/kg
ND
329
120
09/18/23 08:10
Di-n-butylphthalate
ug/kg
ND
329
111
09/18/23 08:10
Di-n-octylphthalate
ug/kg
ND
329
130
09/18/23 08:10
Dibenz(a,h)anthracene
ug/kg
ND
329
127
09/18/23 08:10
Dibenzofuran
ug/kg
ND
329
119
09/18/23 08:10
Diethylphthalate
ug/kg
ND
329
121
09/18/23 08:10
Dimethylphthalate
ug/kg
ND
329
120
09/18/23 08:10
Fluoranthene
ug/kg
ND
329
113
09/18/23 08:10
Fluorene
ug/kg
ND
329
116
09/18/23 08:10
Hexachloro-1,3-butadiene
ug/kg
ND
329
143
09/18/23 08:10
Hexachlorobenzene
ug/kg
ND
329
129
09/18/23 08:10
Hexachlorocyclopentadiene
ug/kg
ND
329
188
09/18/23 08:10
Hexachloroethane
ug/kg
ND
329
126
09/18/23 08:10
Indeno(1,2,3-cd)pyrene
ug/kg
ND
329
130
09/18/23 08:10
Isophorone
ug/kg
ND
329
147
09/18/23 08:10
N-Nitroso-di-n-propylamine
ug/kg
ND
329
124
09/18/23 08:10
N-Nitrosodimethylamine
ug/kg
ND
329
111
09/18/23 08:10
N-Nitrosodiphenylamine
ug/kg
ND
329
117
09/18/23 08:10
Naphthalene
ug/kg
ND
329
112
09/18/23 08:10
Nitrobenzene
ug/kg
ND
329
152
09/18/23 08:10
Pentachlorophenol
ug/kg
ND
658
322
09/18/23 08:10
Phenanthrene
ug/kg
ND
329
108
09/18/23 08:10
Phenol
ug/kg
ND
329
147
09/18/23 08:10
Pyrene
ug/kg
ND
329
134
09/18/23 08:10
Pyridine
ug/kg
ND
329
104
09/18/23 08:10
2,4,6-Tribromophenol (S)
%
68
10-131
09/18/23 08:10
2-Fluorobiphenyl (S)
%
66
10-130
09/18/23 08:10
2-Fluorophenol (S)
%
65
10-130
09/18/23 08:10
Nitrobenzene-d5 (S)
%
70
10-130
09/18/23 08:10
Phenol-d6 (S)
%
67
10-130
09/18/23 08:10
Terphenyl-d14 (S)
%
77
10-130
09/18/23 08:10
v1
v1
LABORATORY CONTROL SAMPLE:
4144697
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
1680
915 55 43-130
1,2-Dichlorobenzene
ug/kg
1680
947 56 43-130
1,3-Dichlorobenzene
ug/kg
1680
928 55 43-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 74 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
LABORATORY CONTROL SAMPLE:
Parameter
4144697
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,4-Dichlorobenzene
ug/kg
1680
922
55
44-130
1-Methylnaphthalene
ug/kg
1680
994
59
47-130
2,2'-Oxybis(1-chloropropane)
ug/kg
1680
947
56
29-130
2,4,5-Trichlorophenol
ug/kg
1680
1120
67
47-130
2,4,6-Trichlorophenol
ug/kg
1680
1050
62
47-130
2,4-Dichlorophenol
ug/kg
1680
952
57
45-130
2,4-Dimethylphenol
ug/kg
1680
929
55
45-130
2,4-Dinitrophenol
ug/kg
8390
7120
85
27-140
2,4-Dinitrotoluene
ug/kg
1680
1360
81
46-130
2,6-Dinitrotoluene
ug/kg
1680
1280
76
48-130
2-Chloronaphthalene
ug/kg
1680
890
53
46-130
2-Chlorophenol
ug/kg
1680
1040
62
43-130
2-Methylnaphthalene
ug/kg
1680
985
59
47-130
2-Methylphenol(o-Cresol)
ug/kg
1680
980
58
42-130
2-Nitroaniline
ug/kg
3360
2470
74
41-130
2-Nitrophenol
ug/kg
1680
955
57
48-130
3&4-Methyl phenol (m&p Cresol)
ug/kg
1680
1010
60
39-130
3,3'-Dichlorobenzidine
ug/kg
3360
2650
79
41-130
3-Nitroaniline
ug/kg
3360
2680
80
37-130
4,6-Dinitro-2-methyl phenol
ug/kg
3360
2920
87
38-141
4-Bromophenylphenyl ether
ug/kg
1680
1330
79
47-130
4-ChIoro-3-methyl phenol
ug/kg
3360
2300
68
44-130
4-Chloroaniline
ug/kg
3360
2070
62
41-130
4-Chlorophenylphenyl ether
ug/kg
1680
1260
75
45-130
4-Nitroaniline
ug/kg
3360
2850
85
42-130
4-Nitrophenol
ug/kg
8390
6990
83
39-131
Acenaphthene
ug/kg
1680
1050
63
49-130
Acenaphthylene
ug/kg
1680
1050
62
50-130
Aniline
ug/kg
1680
993
59
38-130
Anthracene
ug/kg
1680
1250
75
49-130
Benzo(a)anthracene
ug/kg
1680
1290
77
51-130
Benzo(a)pyrene
ug/kg
1680
1470
88
51-130
Benzo(b)fluoranthene
ug/kg
1680
1500
90
49-130
Benzo(g,h,i)perylene
ug/kg
1680
1480
88
48-140
Benzo(k)fluoranthene
ug/kg
1680
1470
87
51-130
Benzoic Acid
ug/kg
8390
5420
65
22-130 v1
Benzyl alcohol
ug/kg
3360
2070
62
43-130
bis(2-Chloroethoxy)methane
ug/kg
1680
965
58
43-130
bis(2-Chloroethyl) ether
ug/kg
1680
959
57
42-130
bis(2-Ethylhexyl)phthalate
ug/kg
1680
1310
78
43-130
Butylbenzylphthalate
ug/kg
1680
1240
74
44-131
Chrysene
ug/kg
1680
1300
78
51-130
Di-n-butylphthalate
ug/kg
1680
1320
79
46-130
Di-n-octylphthalate
ug/kg
1680
1270
76
45-130
Dibenz(a,h)anthracene
ug/kg
1680
1530
91
48-130
Dibenzofuran
ug/kg
1680
1110
66
10-130
Diethylphthalate
ug/kg
1680
1350
81
48-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 75 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
LABORATORY CONTROL SAMPLE:
Parameter
4144697
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Dimethylphthalate
ug/kg
1680
1320
78
48-130
Fluoranthene
ug/kg
1680
1410
84
48-130
Fluorene
ug/kg
1680
1240
74
48-130
Hexachloro-1,3-butadiene
ug/kg
1680
934
56
39-130
Hexachlorobenzene
ug/kg
1680
1320
78
47-130
Hexachlorocyclopentadiene
ug/kg
1680
645
38
17-130
Hexachloroethane
ug/kg
1680
910
54
40-130
Indeno(1,2,3-cd)pyrene
ug/kg
1680
1450
87
50-130
Isophorone
ug/kg
1680
1020
61
41-130
N-Nitroso-di-n-propylamine
ug/kg
1680
1060
63
36-130
N-Nitrosodimethylamine
ug/kg
1680
941
56
34-130 v1
N-Nitrosodiphenylamine
ug/kg
1680
1210
72
48-130
Naphthalene
ug/kg
1680
942
56
46-130
Nitrobenzene
ug/kg
1680
901
54
39-130
Pentachlorophenol
ug/kg
3360
2310
69
42-130
Phenanthrene
ug/kg
1680
1290
77
50-130
Phenol
ug/kg
1680
1090
65
42-130
Pyrene
ug/kg
1680
1280
76
50-130
Pyridine
ug/kg
1680
842
50
26-130 v1
2,4,6-Tribromophenol (S)
%
83
10-131
2-Fluorobiphenyl (S)
%
53
10-130
2-Fluorophenol(S)
%
58
10-130
Nitrobenzene-d5(S)
%
54
10-130
Phenol-d6 (S)
%
60
10-130
Terphenyl-d14 (S)
%
78
10-130
MATRIX SPIKE SAMPLE:
Parameter
4144698
Units
92688240001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
ND
1780
896
50
16-130
1,2-Dichlorobenzene
ug/kg
ND
1780
869
49
19-130
1,3-Dichlorobenzene
ug/kg
ND
1780
855
48
19-130
1,4-Dichlorobenzene
ug/kg
ND
1780
854
48
20-130
1-Methylnaphthalene
ug/kg
ND
1780
985
55
19-130
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
1780
865
49
10-130
2,4,5-Trichlorophenol
ug/kg
ND
1780
1240
70
19-130
2,4,6-Trichlorophenol
ug/kg
ND
1780
1140
64
18-130
2,4-Dichlorophenol
ug/kg
ND
1780
976
55
16-130
2,4-Dimethylphenol
ug/kg
ND
1780
975
55
10-130
2,4-Dinitrophenol
ug/kg
ND
8890
6790
76
10-143
2,4-Dinitrotoluene
ug/kg
ND
1780
1290
72
19-130
2,6-Dinitrotoluene
ug/kg
ND
1780
1220
69
22-130
2-Chloronaphthalene
ug/kg
ND
1780
893
50
18-130
2-Chlorophenol
ug/kg
ND
1780
943
53
20-130
2-Methylnaphthalene
ug/kg
ND
1780
957
54
18-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 76 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
MATRIX SPIKE SAMPLE:
4144698
92688240001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
2-Methylphenol(o-Cresol)
ug/kg
ND
1780
901
51
13-130
2-Nitroaniline
ug/kg
ND
3560
2390
67
18-130
2-Nitrophenol
ug/kg
ND
1780
940
53
19-130
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
1780
917
52
13-130
3,3'-Dichlorobenzidine
ug/kg
ND
3560
2530
71
10-130
3-Nitroaniline
ug/kg
ND
3560
2510
71
22-130
4,6-Dinitro-2-methyl phenol
ug/kg
ND
3560
2870
81
10-144
4-Bromophenylphenyl ether
ug/kg
ND
1780
1370
77
18-130
4-Chloro-3-methylphenol
ug/kg
ND
3560
2580
73
16-130
4-Chloroaniline
ug/kg
ND
3560
1920
54
17-130
4-Chlorophenylphenyl ether
ug/kg
ND
1780
1300
73
17-130
4-Nitroaniline
ug/kg
ND
3560
2660
75
21-130
4-Nitrophenol
ug/kg
ND
8890
6620
74
13-131
Acenaphthene
ug/kg
ND
1780
1080
61
20-130
Acenaphthylene
ug/kg
ND
1780
1060
60
21-130
Aniline
ug/kg
ND
1780
891
50
10-130
Anthracene
ug/kg
ND
1780
1250
70
19-130
Benzo(a)anthracene
ug/kg
ND
1780
1250
70
17-130
Benzo(a)pyrene
ug/kg
ND
1780
1390
78
14-130
Benzo(b)fluoranthene
ug/kg
ND
1780
1520
85
11-134
Benzo(g,h,i)perylene
ug/kg
ND
1780
1170
66
12-130
Benzo(k)fluoranthene
ug/kg
ND
1780
1470
83
15-130
Benzoic Acid
ug/kg
ND
8890
4440
50
10-130 v1
Benzyl alcohol
ug/kg
ND
3560
1800
51
20-130
bis(2-Chloroethoxy)methane
ug/kg
ND
1780
917
52
16-130
bis(2-Chloroethyl) ether
ug/kg
ND
1780
864
49
18-130
bis(2-Ethylhexyl)phthalate
ug/kg
ND
1780
1340
75
11-130
Butylbenzylphthalate
ug/kg
ND
1780
1260
71
10-130
Chrysene
ug/kg
ND
1780
1250
70
17-130
Di-n-butylphthalate
ug/kg
ND
1780
1280
72
16-130
Di-n-octylphthalate
ug/kg
ND
1780
1240
70
16-130
Dibenz(a,h)anthracene
ug/kg
ND
1780
1210
68
13-130
Dibenzofuran
ug/kg
ND
1780
1120
63
19-130
Diethylphthalate
ug/kg
ND
1780
1290
73
22-130
Dimethylphthalate
ug/kg
ND
1780
1240
70
23-130
Fluoranthene
ug/kg
ND
1780
1350
76
14-130
Fluorene
ug/kg
ND
1780
1240
70
19-130
Hexachloro-1,3-butadiene
ug/kg
ND
1780
942
53
12-130
Hexachlorobenzene
ug/kg
ND
1780
1350
76
17-130
Hexachlorocyclopentadiene
ug/kg
ND
1780
807
45
10-130
Hexachloroethane
ug/kg
ND
1780
834
47
14-130
Indeno(1,2,3-cd)pyrene
ug/kg
ND
1780
1180
66
13-130
Isophorone
ug/kg
ND
1780
950
53
17-130
N-Nitroso-di-n-propylamine
ug/kg
ND
1780
918
52
10-130
N-Nitrosodimethylamine
ug/kg
ND
1780
810
46
16-130 v1
N-Nitrosodiphenylamine
ug/kg
ND
1780
1260
71
19-130
Naphthalene
ug/kg
ND
1780
924
52
18-130
Results presented on this page are in the units indicated
by the "Units" column except where
an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 77 of 88

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
MATRIX SPIKE SAMPLE:
Parameter
4144698
Units
92688240001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Nitrobenzene
ug/kg
ND
1780
853
48
15-130
Pentachlorophenol
ug/kg
ND
3560
2390
67
10-130
Phenanthrene
ug/kg
ND
1780
1280
72
17-130
Phenol
ug/kg
ND
1780
949
53
15-130
Pyrene
ug/kg
ND
1780
1320
74
31-130
Pyridine
ug/kg
ND
1780
728
41
10-130 v1
2,4,6-Tribromophenol (S)
%
81
10-131
2-Fluorobiphenyl (S)
%
46
10-130
2-Fluorophenol (S)
%
48
10-130
Nitrobenzene-d5 (S)
%
49
10-130
Phenol-d6 (S)
%
48
10-130
Terphenyl-d14 (S)
%
73
10-130
SAMPLE DUPLICATE: 4144699
Parameter
Units
92688260001
Result
Dup
Result RPD
Max
RPD Qualifiers
1,2,4-Trichlorobenzene
ug/kg
ND
ND
30
1,2-Dichlorobenzene
ug/kg
ND
ND
30
1,3-Dichlorobenzene
ug/kg
ND
ND
30
1,4-Dichlorobenzene
ug/kg
ND
ND
30
1-Methylnaphthalene
ug/kg
ND
ND
30
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
ND
30
2,4,5-Trichlorophenol
ug/kg
ND
ND
30
2,4,6-Trichlorophenol
ug/kg
ND
ND
30
2,4-Dichlorophenol
ug/kg
ND
ND
30
2,4-Dimethylphenol
ug/kg
ND
ND
30
2,4-Dinitrophenol
ug/kg
ND
ND
30
2,4-Dinitrotoluene
ug/kg
ND
ND
30
2,6-Dinitrotoluene
ug/kg
ND
ND
30
2-Chloronaphthalene
ug/kg
ND
ND
30
2-Chlorophenol
ug/kg
ND
ND
30
2-Methylnaphthalene
ug/kg
ND
ND
30
2-Methylphenol(o-Cresol)
ug/kg
ND
ND
30
2-Nitroaniline
ug/kg
ND
ND
30
2-Nitrophenol
ug/kg
ND
ND
30
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
ND
30
3,3'-Dichlorobenzidine
ug/kg
ND
ND
30
3-Nitroaniline
ug/kg
ND
ND
30
4,6-Dinitro-2-methyl phenol
ug/kg
ND
ND
30
4-Bromophenylphenyl ether
ug/kg
ND
ND
30
4-Chloro-3-methylphenol
ug/kg
ND
ND
30
4-Chloroaniline
ug/kg
ND
ND
30
4-Chlorophenylphenyl ether
ug/kg
ND
ND
30
4-Nitroaniline
ug/kg
ND
ND
30
4-Nitrophenol
ug/kg
ND
ND
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 78 of 88

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: JOB #1487
Pace Project No.: 92688240
SAMPLE DUPLICATE: 4144699
Parameter
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Ethylhexyl)phthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenz(a,h)anthracene
Dibenzofuran
Diethylphthalate
Dimethylphthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
N-Nitroso-di-n-propylamine
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol(S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
QUALITY CONTROL DATA
Units
92688260001 Dup
Result Result
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
71
%
57
61
%
65
63
%
78
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
69
54
61
66
65
70
Max
RPD RPD
30
30
30
30
30
30
30
30
30
30 v1
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30 v1
30
30
30
30
30
30
30
30 v1
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 79 of 88

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
QC Batch: 800106 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92688240001, 92688240002, 92688240003, 92688240004, 92688240005, 92688240006, 92688240007,
92688240008,92688240009,92688240010
SAMPLE DUPLICATE: 4144358
92688229002 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 25.7 28.7 11 25 N2
SAMPLE DUPLICATE: 4144359
92688240010 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 7.0 6.8 3 25 N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 80 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
QC Batch: 2136461 Analysis Method: SM 2540G
QC Batch Method: SM 2540 G Analysis Description: Total Solids 2540 G-2011
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92688240001, 92688240002, 92688240003
METHOD BLANK: R3976025-1 Matrix: Solid
Associated Lab Samples: 92688240001, 92688240002, 92688240003
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Total Solids % 0.00400 09/21/23 06:52
LABORATORY CONTROL SAMPLE: R3976025-2
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Solids % 50.0 50.0 99.9 85.0-115
SAMPLE DUPLICATE: R3976025-3
L1657579-01 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Solids % 90.3 90.3 0.0751 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
QC Batch: 2136463 Analysis Method: SM 2540G
QC Batch Method: SM 2540 G Analysis Description: Total Solids 2540 G-2011
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92688240004, 92688240005, 92688240006, 92688240007, 92688240008, 92688240009, 92688240010
METHOD BLANK: R3976022-1 Matrix: Solid
Associated Lab Samples: 92688240004, 92688240005, 92688240006, 92688240007, 92688240008, 92688240009, 92688240010
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Total Solids % 0.00600J 09/21/23 06:42 J
LABORATORY CONTROL SAMPLE: R3976022-2
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Solids % 50.0 50.0 100 85.0-115
SAMPLE DUPLICATE: R3976022-3
92688240007 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Solids % 89.8 91.8 2.18 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/25/2023 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 82 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOB #1487
Pace Project No.: 92688240
QC Batch: 2136401 Analysis Method: EPA 7199
QC Batch Method: 3060A Analysis Description: Wet Chemistry 7199
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92688240001, 92688240002, 92688240003, 92688240004, 92688240005, 92688240006, 92688240007,
92688240008,92688240009,92688240010
METHOD BLANK: R3976623-1 Matrix: Solid
Associated Lab Samples: 92688240001, 92688240002, 92688240003, 92688240004, 92688240005, 92688240006, 92688240007,
92688240008,92688240009,92688240010
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Chromium, Hexavalent mg/kg ND 1.00 0.255 09/22/23 10:28
LABORATORY CONTROL SAMPLE: R3976623-2
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chromium, Hexavalent mg/kg 10.0 10.3 103 80.0-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3976623-4 R3976623-5
MS MSD
92688240003 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Chromium, Hexavalent mg/kg 0.532 22.1 22.1 23.6 24.0 104 106 75.0-125 1.61 20
MATRIX SPIKE SAMPLE:
R3976623-6
92688240003
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Chromium, Hexavalent
mg/kg
0.532
709
241
34.0
75.0-125 ML
SAMPLE DUPLICATE: R3976623-3
92688240001
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
Chromium, Hexavalent
mg/kg
0.579
0.531J
8.63
20 J
SAMPLE DUPLICATE: R3976623-8
L1657742-02
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
Chromium, Hexavalent
mg/kg
ND
ND
0.00
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: JOB #1487
Pace Project No.: 92688240
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
C9 Common Laboratory Contaminant.
IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
J Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
ML Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased
low.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
JOB #1487
92688240
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92688240001
FG-1
EPA 3050
952019
EPA 6010
952150
92688240002
FG-2
EPA 3050
952019
EPA 6010
952150
92688240003
FG-3
EPA 3050
952019
EPA 6010
952150
92688240004
FG-4
EPA 3050
952019
EPA 6010
952150
92688240005
FG-5
EPA 3050
952019
EPA 6010
952150
92688240006
FG-6
EPA 3050
952019
EPA 6010
952150
92688240007
FG-7
EPA 3050
952019
EPA 6010
952150
92688240008
FG-8
EPA 3050
952019
EPA 6010
952150
92688240009
FG-9
EPA 3050
952019
EPA 6010
952150
92688240010
FG-10
EPA 3050
952019
EPA 6010
952150
92688240001
FG-1
EPA 7471
951692
EPA 7471
951747
92688240002
FG-2
EPA 7471
951692
EPA 7471
951747
92688240003
FG-3
EPA 7471
951692
EPA 7471
951747
92688240004
FG-4
EPA 7471
951692
EPA 7471
951747
92688240005
FG-5
EPA 7471
951692
EPA 7471
951747
92688240006
FG-6
EPA 7471
951692
EPA 7471
951747
92688240007
FG-7
EPA 7471
951692
EPA 7471
951747
92688240008
FG-8
EPA 7471
951692
EPA 7471
951747
92688240009
FG-9
EPA 7471
951692
EPA 7471
951747
92688240010
FG-10
EPA 7471
951692
EPA 7471
951747
92688240001
FG-1
EPA 3546
800183
EPA 8270E
800219
92688240002
FG-2
EPA 3546
800183
EPA 8270E
800219
92688240003
FG-3
EPA 3546
800183
EPA 8270E
800219
92688240004
FG-4
EPA 3546
800183
EPA 8270E
800219
92688240005
FG-5
EPA 3546
800183
EPA 8270E
800219
92688240006
FG-6
EPA 3546
800183
EPA 8270E
800219
92688240007
FG-7
EPA 3546
800183
EPA 8270E
800219
92688240008
FG-8
EPA 3546
800183
EPA 8270E
800219
92688240009
FG-9
EPA 3546
800183
EPA 8270E
800219
92688240010
FG-10
EPA 3546
800183
EPA 8270E
800219
92688240001
FG-1
EPA 5035A/5030B
800123
EPA 8260D
800253
92688240002
FG-2
EPA 5035A/5030B
800123
EPA 8260D
800253
92688240003
FG-3
EPA 5035A/5030B
800123
EPA 8260D
800253
92688240004
FG-4
EPA 5035A/5030B
800123
EPA 8260D
800253
92688240005
FG-5
EPA 5035A/5030B
800123
EPA 8260D
800253
92688240006
FG-6
EPA 5035A/5030B
800123
EPA 8260D
800253
92688240007
FG-7
EPA 5035A/5030B
800123
EPA 8260D
800253
92688240008
FG-8
EPA 5035A/5030B
800345
EPA 8260D
800615
92688240009
FG-9
EPA 5035A/5030B
800345
EPA 8260D
800615
92688240010
FG-10
EPA 5035A/5030B
800345
EPA 8260D
800615
92688240001
FG-1
SW-846
800106
92688240002
FG-2
SW-846
800106
92688240003
FG-3
SW-846
800106
92688240004
FG-4
SW-846
800106
92688240005
FG-5
SW-846
800106
92688240006
FG-6
SW-846
800106
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 09/25/2023
04:50 PM
without the written consent of Pace Analytical Services, LLC.
Page 85 of 88

ceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
JOB #1487
Pace Project No.:
92688240
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92688240007
FG-7
SW-846
800106
92688240008
FG-8
SW-846
800106
92688240009
FG-9
SW-846
800106
92688240010
FG-10
SW-846
800106
92688240001
FG-1
SM 2540 G
2136461
SM 254OG
2136461
92688240002
FG-2
SM 2540 G
2136461
SM 254OG
2136461
92688240003
FG-3
SM 2540 G
2136461
SM 254OG
2136461
92688240004
FG-4
SM 2540 G
2136463
SM 2540G
2136463
92688240005
FG-5
SM 2540 G
2136463
SM 2540G
2136463
92688240006
FG-6
SM 2540 G
2136463
SM 2540G
2136463
92688240007
FG-7
SM 2540 G
2136463
SM 2540G
2136463
92688240008
FG-8
SM 2540 G
2136463
SM 2540G
2136463
92688240009
FG-9
SM 2540 G
2136463
SM 2540G
2136463
92688240010
FG-10
SM 2540 G
2136463
SM 2540G
2136463
92688240001
FG-1
3060A
2136401
EPA 7199
2136401
92688240002
FG-2
3060A
2136401
EPA 7199
2136401
92688240003
FG-3
3060A
2136401
EPA 7199
2136401
92688240004
FG-4
3060A
2136401
EPA 7199
2136401
92688240005
FG-5
3060A
2136401
EPA 7199
2136401
92688240006
FG-6
3060A
2136401
EPA 7199
2136401
92688240007
FG-7
3060A
2136401
EPA 7199
2136401
92688240008
FG-8
3060A
2136401
EPA 7199
2136401
92688240009
FG-9
3060A
2136401
EPA 7199
2136401
92688240010
FG-10
3060A
2136401
EPA 7199
2136401
Date: 09/25/2023 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 86 of 88

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Effective Date: 11/14/2022
*Cheep mark top half of box if pM and/or dechtorination is verified and
within the acceptance range for preservation samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottles
***Check all unpreserved Nitrates for chlorine
Project WO# * 92-6z4O
PM: MWB Due Date: 09/25/23
CLIENT: 92-ATL SHORE
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pH Adjustment Log for Preserved Samples
Sample ID Type of Preservative FD upon receipt Date preservation adjusted Time preservation Amount of Preservative tot #f
adjusted added
Mote: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will he sent to the Nortll Carolina DENR Certification Office {i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers,
Qualtrax ID:69614
Page z of 2
Page 88 of 88

Final Grade Soil Sampling
East Side Trucking Service
520 Judson Church Road, Fayetteville, North Carolina
Brownfields Project Number 25009-21-026
FIELD NOTES
December 5, 2023

Location �� •ate r
Project / Client
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