FA-92507_92464_CA_MRP_20231221_MWAnalyticalReports

ANALYTICAL REPORT
March 17, 2023
S&ME Inc. - Raleigh NC
Sample Delivery Group:L1592757
Samples Received:03/08/2023
Project Number:210818
Description:Colonial Pipeline - Jennifer Drive
Report To:Mr. Michael Pfeifer
3201 Spring Forest Road
Raleigh, NC 27616
Entire Report Reviewed By:
March 17, 2023
[Preliminary Report]
Craig Cothron
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 1 of 78
March 20, 2023
Craig Cothron
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 1 of 78
TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 6
Sr: Sample Results 7
MW-2 L1592757-01 7
MW-3 L1592757-02 10
MW-5 L1592757-03 13
MW-6 L1592757-04 16
MW-7 L1592757-05 19
MW-8 L1592757-06 22
MW-9 L1592757-07 25
MW-10 L1592757-08 28
MW-12 L1592757-09 30
MW-1D L1592757-10 33
MW-4D L1592757-11 36
MW-5D L1592757-12 39
MW-6D L1592757-13 42
MW-13 L1592757-14 45
Qc: Quality Control Summary 48
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 48
TPH by Method MADEPE 58
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 61
Gl: Glossary of Terms 71
Al: Accreditations & Locations 72
Sc: Sample Chain of Custody 73
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 2 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 2 of 78
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-2 L1592757-01 GW James Waters 03/06/23 15:40 03/08/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020042 1 03/09/23 13:59 03/09/23 13:59 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020940 1 03/10/23 15:51 03/10/23 15:51 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/14/23 16:38 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/14/23 23:25 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2019718 1 03/10/23 06:32 03/11/23 00:22 DSH Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-3 L1592757-02 GW James Waters 03/06/23 10:45 03/08/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020042 100 03/09/23 19:24 03/09/23 19:24 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020940 100 03/10/23 19:50 03/10/23 19:50 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/14/23 17:02 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/14/23 23:01 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2019718 1 03/10/23 06:32 03/11/23 00:43 DSH Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-5 L1592757-03 GW James Waters 03/06/23 14:25 03/08/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020042 1 03/09/23 14:21 03/09/23 14:21 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020940 1 03/10/23 16:13 03/10/23 16:13 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/14/23 17:26 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/14/23 22:37 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2019718 1 03/10/23 06:32 03/11/23 01:04 DSH Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-6 L1592757-04 GW James Waters 03/06/23 14:20 03/08/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020042 1 03/09/23 15:48 03/09/23 15:48 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020940 1 03/10/23 16:34 03/10/23 16:34 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/14/23 17:50 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/14/23 22:14 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2019718 1 03/10/23 06:32 03/11/23 01:26 DSH Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-7 L1592757-05 GW James Waters 03/06/23 14:55 03/08/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020042 1 03/09/23 16:09 03/09/23 16:09 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020940 1 03/10/23 16:56 03/10/23 16:56 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/14/23 18:14 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/14/23 21:50 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2019718 1 03/10/23 06:32 03/11/23 01:47 DSH Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 3 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 3 of 78
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-8 L1592757-06 GW James Waters 03/06/23 09:45 03/08/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020042 1 03/09/23 16:31 03/09/23 16:31 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020940 1 03/10/23 17:18 03/10/23 17:18 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/14/23 18:38 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/14/23 21:26 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2019718 1 03/10/23 06:32 03/11/23 02:08 DSH Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-9 L1592757-07 GW James Waters 03/06/23 12:25 03/08/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020042 1 03/09/23 16:53 03/09/23 16:53 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020940 1 03/10/23 17:39 03/10/23 17:39 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/14/23 19:02 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/14/23 21:02 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2019718 1 03/10/23 06:32 03/11/23 02:29 DSH Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-10 L1592757-08 GW James Waters 03/06/23 15:00 03/08/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020042 1 03/09/23 17:14 03/09/23 17:14 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020940 1 03/10/23 18:01 03/10/23 18:01 ADM Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-12 L1592757-09 GW James Waters 03/06/23 12:20 03/08/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020042 1 03/09/23 17:36 03/09/23 17:36 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020940 1 03/10/23 18:23 03/10/23 18:23 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/14/23 19:26 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/14/23 20:38 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2019718 1 03/10/23 06:32 03/11/23 02:50 DSH Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-1D L1592757-10 GW James Waters 03/07/23 09:10 03/08/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020042 1 03/09/23 17:58 03/09/23 17:58 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020940 1 03/10/23 18:45 03/10/23 18:45 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/14/23 19:50 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/14/23 20:14 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2020599 1 03/11/23 02:19 03/12/23 00:29 DSH Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-4D L1592757-11 GW James Waters 03/07/23 12:15 03/08/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020042 50 03/09/23 19:46 03/09/23 19:46 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020940 50 03/10/23 20:12 03/10/23 20:12 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/15/23 01:25 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/15/23 02:37 DMG Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 4 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 4 of 78
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-4D L1592757-11 GW James Waters 03/07/23 12:15 03/08/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2020599 1 03/11/23 02:19 03/12/23 00:50 DSH Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-5D L1592757-12 GW James Waters 03/07/23 10:25 03/08/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020042 1 03/09/23 18:19 03/09/23 18:19 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020940 1 03/10/23 19:07 03/10/23 19:07 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/15/23 01:49 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/15/23 03:01 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2020599 1 03/11/23 02:19 03/12/23 01:11 DSH Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-6D L1592757-13 GW James Waters 03/07/23 11:20 03/08/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020042 1 03/09/23 18:41 03/09/23 18:41 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2020940 1 03/10/23 19:28 03/10/23 19:28 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/15/23 02:13 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2020454 1 03/09/23 08:44 03/15/23 03:25 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2020599 1 03/11/23 02:19 03/12/23 01:32 DSH Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-13 L1592757-14 GW James Waters 03/06/23 11:35 03/09/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2023464 1 03/16/23 01:53 03/16/23 01:53 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2024328 1 03/16/23 11:53 03/16/23 11:53 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2022391 1 03/13/23 08:46 03/15/23 17:19 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2022391 1 03/13/23 08:46 03/15/23 21:21 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2020599 1 03/11/23 02:19 03/12/23 09:39 DSH Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 5 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 5 of 78
CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Craig Cothron
Project Manager
Sample Delivery Group (SDG) Narrative
An aliquot for analysis was taken from the original container received due to the level of sediment present in the sample.
Rinsing of the original sample container for inclusion in the sample extraction was not performed.
Lab Sample ID Project Sample ID Method
L1592757-01 MW-2 625.1
L1592757-04 MW-6 625.1
L1592757-05 MW-7 625.1
L1592757-09 MW-12 625.1
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 6 of 78
Craig Cothron
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 6 of 78
SAMPLE RESULTS - 01
L1592757
MW-2
Collected date/time: 03/06/23 15:40
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene ND 1.00 1 03/09/2023 13:59 WG2020042
Bromobenzene ND 1.00 1 03/09/2023 13:59 WG2020042
Bromodichloromethane ND 1.00 1 03/09/2023 13:59 WG2020042
Bromochloromethane ND 1.00 1 03/09/2023 13:59 WG2020042
Bromoform ND 1.00 1 03/09/2023 13:59 WG2020042
Bromomethane ND 5.00 1 03/09/2023 13:59 WG2020042
n-Butylbenzene ND 1.00 1 03/09/2023 13:59 WG2020042
sec-Butylbenzene ND 1.00 1 03/09/2023 13:59 WG2020042
tert-Butylbenzene ND 1.00 1 03/09/2023 13:59 WG2020042
Carbon tetrachloride ND 1.00 1 03/09/2023 13:59 WG2020042
Chlorobenzene ND 1.00 1 03/09/2023 13:59 WG2020042
Chlorodibromomethane ND 1.00 1 03/09/2023 13:59 WG2020042
Chloroethane ND 5.00 1 03/09/2023 13:59 WG2020042
Chloroform ND 5.00 1 03/09/2023 13:59 WG2020042
Chloromethane ND 2.50 1 03/09/2023 13:59 WG2020042
2-Chlorotoluene ND 1.00 1 03/09/2023 13:59 WG2020042
4-Chlorotoluene ND 1.00 1 03/09/2023 13:59 WG2020042
1,2-Dibromo-3-Chloropropane ND 5.00 1 03/09/2023 13:59 WG2020042
1,2-Dibromoethane ND 1.00 1 03/09/2023 13:59 WG2020042
Dibromomethane ND 1.00 1 03/09/2023 13:59 WG2020042
1,2-Dichlorobenzene ND 1.00 1 03/09/2023 13:59 WG2020042
1,3-Dichlorobenzene ND 1.00 1 03/09/2023 13:59 WG2020042
1,4-Dichlorobenzene ND 1.00 1 03/09/2023 13:59 WG2020042
Dichlorodifluoromethane ND 5.00 1 03/09/2023 13:59 WG2020042
1,1-Dichloroethane ND 1.00 1 03/09/2023 13:59 WG2020042
1,2-Dichloroethane ND 1.00 1 03/09/2023 13:59 WG2020042
1,1-Dichloroethene ND 1.00 1 03/09/2023 13:59 WG2020042
cis-1,2-Dichloroethene ND 1.00 1 03/09/2023 13:59 WG2020042
trans-1,2-Dichloroethene ND 1.00 1 03/09/2023 13:59 WG2020042
1,2-Dichloropropane ND 1.00 1 03/09/2023 13:59 WG2020042
1,1-Dichloropropene ND 1.00 1 03/09/2023 13:59 WG2020042
1,3-Dichloropropane ND 1.00 1 03/09/2023 13:59 WG2020042
cis-1,3-Dichloropropene ND 1.00 1 03/09/2023 13:59 WG2020042
trans-1,3-Dichloropropene ND 1.00 1 03/09/2023 13:59 WG2020042
2,2-Dichloropropane ND 1.00 1 03/09/2023 13:59 WG2020042
Di-isopropyl ether ND 1.00 1 03/09/2023 13:59 WG2020042
Ethylbenzene ND 1.00 1 03/09/2023 13:59 WG2020042
Hexachloro-1,3-butadiene ND 1.00 1 03/09/2023 13:59 WG2020042
Isopropylbenzene ND 1.00 1 03/09/2023 13:59 WG2020042
Methylene Chloride ND 5.00 1 03/09/2023 13:59 WG2020042
Methyl tert-butyl ether ND 1.00 1 03/09/2023 13:59 WG2020042
Naphthalene ND 5.00 1 03/09/2023 13:59 WG2020042
n-Propylbenzene ND 1.00 1 03/09/2023 13:59 WG2020042
Styrene ND 1.00 1 03/09/2023 13:59 WG2020042
1,1,1,2-Tetrachloroethane ND 1.00 1 03/09/2023 13:59 WG2020042
1,1,2,2-Tetrachloroethane ND 1.00 1 03/09/2023 13:59 WG2020042
Tetrachloroethene ND 1.00 1 03/09/2023 13:59 WG2020042
Toluene ND 1.00 1 03/09/2023 13:59 WG2020042
1,2,3-Trichlorobenzene ND 1.00 1 03/09/2023 13:59 WG2020042
1,2,4-Trichlorobenzene ND 1.00 1 03/09/2023 13:59 WG2020042
1,1,1-Trichloroethane ND 1.00 1 03/09/2023 13:59 WG2020042
1,1,2-Trichloroethane ND 1.00 1 03/09/2023 13:59 WG2020042
Trichloroethene ND 1.00 1 03/09/2023 13:59 WG2020042
Trichlorofluoromethane ND 5.00 1 03/09/2023 13:59 WG2020042
1,2,3-Trichloropropane ND 2.50 1 03/09/2023 13:59 WG2020042
1,2,4-Trimethylbenzene ND 1.00 1 03/09/2023 13:59 WG2020042
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 7 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 7 of 78
SAMPLE RESULTS - 01
L1592757
MW-2
Collected date/time: 03/06/23 15:40
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 03/09/2023 13:59 WG2020042
Vinyl chloride ND 1.00 1 03/09/2023 13:59 WG2020042
o-Xylene ND 1.00 1 03/09/2023 13:59 WG2020042
m&p-Xylenes ND 2.00 1 03/09/2023 13:59 WG2020042
ethanol ND 100 1 03/09/2023 13:59 WG2020042
tert-Amyl Methyl Ether ND 1.00 1 03/09/2023 13:59 WG2020042
Ethyl tert-butyl ether ND 1.00 1 03/09/2023 13:59 WG2020042
tert-Butyl alcohol ND 5.00 1 03/09/2023 13:59 WG2020042
t-Amyl Alcohol ND 50.0 1 03/09/2023 13:59 WG2020042
tert-Butyl formate ND 20.0 1 03/10/2023 15:51 WG2020940
(S) Toluene-d8 100 80.0-120 03/09/2023 13:59 WG2020042
(S) Toluene-d8 104 80.0-120 03/10/2023 15:51 WG2020940
(S) 4-Bromofluorobenzene 91.6 77.0-126 03/09/2023 13:59 WG2020042
(S) 4-Bromofluorobenzene 105 77.0-126 03/10/2023 15:51 WG2020940
(S) 1,2-Dichloroethane-d4 90.4 70.0-130 03/09/2023 13:59 WG2020042
(S) 1,2-Dichloroethane-d4 111 70.0-130 03/10/2023 15:51 WG2020940
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 03/14/2023 16:38 WG2020454
Unadjusted C19-C36 Aliphatics ND 100 1 03/14/2023 16:38 WG2020454
Unadjusted C11-C22 Aromatics ND 100 1 03/14/2023 23:25 WG2020454
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 03/14/2023 16:38 WG2020454
(S) o-Terphenyl 74.5 40.0-140 03/14/2023 23:25 WG2020454
(S) 1-Chloro-octadecane 52.5 40.0-140 03/14/2023 16:38 WG2020454
(S) 2-Fluorobiphenyl 91.1 40.0-140 03/14/2023 23:25 WG2020454
(S) 2-Bromonaphthalene 99.6 40.0-140 03/14/2023 23:25 WG2020454
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 03/11/2023 00:22 WG2019718
Acenaphthylene ND 1.00 1 03/11/2023 00:22 WG2019718
Anthracene ND 1.00 1 03/11/2023 00:22 WG2019718
Benzo(a)anthracene ND 1.00 1 03/11/2023 00:22 WG2019718
Benzo(b)fluoranthene ND 1.00 1 03/11/2023 00:22 WG2019718
Benzo(k)fluoranthene ND 1.00 1 03/11/2023 00:22 WG2019718
Benzo(g,h,i)perylene ND 1.00 1 03/11/2023 00:22 WG2019718
Benzo(a)pyrene ND 1.00 1 03/11/2023 00:22 WG2019718
Bis(2-chlorethoxy)methane ND 10.0 1 03/11/2023 00:22 WG2019718
Bis(2-chloroethyl)ether ND 10.0 1 03/11/2023 00:22 WG2019718
2,2-Oxybis(1-Chloropropane)ND 10.0 1 03/11/2023 00:22 WG2019718
4-Bromophenyl-phenylether ND 10.0 1 03/11/2023 00:22 WG2019718
2-Chloronaphthalene ND 1.00 1 03/11/2023 00:22 WG2019718
4-Chlorophenyl-phenylether ND 10.0 1 03/11/2023 00:22 WG2019718
Chrysene ND 1.00 1 03/11/2023 00:22 WG2019718
Dibenz(a,h)anthracene ND 1.00 1 03/11/2023 00:22 WG2019718
3,3-Dichlorobenzidine ND 10.0 1 03/11/2023 00:22 WG2019718
2,4-Dinitrotoluene ND 10.0 1 03/11/2023 00:22 WG2019718
2,6-Dinitrotoluene ND 10.0 1 03/11/2023 00:22 WG2019718
Fluoranthene ND 1.00 1 03/11/2023 00:22 WG2019718
Fluorene ND 1.00 1 03/11/2023 00:22 WG2019718
Hexachlorobenzene ND 1.00 1 03/11/2023 00:22 WG2019718
Hexachloro-1,3-butadiene ND 10.0 1 03/11/2023 00:22 WG2019718
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 8 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 8 of 78
SAMPLE RESULTS - 01
L1592757
MW-2
Collected date/time: 03/06/23 15:40
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Hexachlorocyclopentadiene ND 10.0 1 03/11/2023 00:22 WG2019718
Hexachloroethane ND 10.0 1 03/11/2023 00:22 WG2019718
Indeno(1,2,3-cd)pyrene ND 1.00 1 03/11/2023 00:22 WG2019718
Isophorone ND 10.0 1 03/11/2023 00:22 WG2019718
Naphthalene ND 1.00 1 03/11/2023 00:22 WG2019718
Nitrobenzene ND 10.0 1 03/11/2023 00:22 WG2019718
n-Nitrosodimethylamine ND 10.0 1 03/11/2023 00:22 WG2019718
n-Nitrosodiphenylamine ND 10.0 1 03/11/2023 00:22 WG2019718
n-Nitrosodi-n-propylamine ND 10.0 1 03/11/2023 00:22 WG2019718
Phenanthrene ND 1.00 1 03/11/2023 00:22 WG2019718
Benzylbutyl phthalate ND 3.00 1 03/11/2023 00:22 WG2019718
Bis(2-ethylhexyl)phthalate ND 3.00 1 03/11/2023 00:22 WG2019718
Di-n-butyl phthalate ND 3.00 1 03/11/2023 00:22 WG2019718
Diethyl phthalate ND 3.00 1 03/11/2023 00:22 WG2019718
Dimethyl phthalate ND 3.00 1 03/11/2023 00:22 WG2019718
Di-n-octyl phthalate ND 3.00 1 03/11/2023 00:22 WG2019718
Pyrene ND 1.00 1 03/11/2023 00:22 WG2019718
1,2,4-Trichlorobenzene ND 10.0 1 03/11/2023 00:22 WG2019718
4-Chloro-3-methylphenol ND 10.0 1 03/11/2023 00:22 WG2019718
2-Chlorophenol ND 10.0 1 03/11/2023 00:22 WG2019718
2,4-Dichlorophenol ND 10.0 1 03/11/2023 00:22 WG2019718
2,4-Dimethylphenol ND 10.0 1 03/11/2023 00:22 WG2019718
4,6-Dinitro-2-methylphenol ND 10.0 1 03/11/2023 00:22 WG2019718
2,4-Dinitrophenol ND 10.0 1 03/11/2023 00:22 WG2019718
2-Nitrophenol ND 10.0 1 03/11/2023 00:22 WG2019718
4-Nitrophenol ND 10.0 1 03/11/2023 00:22 WG2019718
Pentachlorophenol ND 10.0 1 03/11/2023 00:22 WG2019718
Phenol ND 10.0 1 03/11/2023 00:22 WG2019718
2,4,6-Trichlorophenol ND 10.0 1 03/11/2023 00:22 WG2019718
(S) Nitrobenzene-d5 92.0 15.0-314 03/11/2023 00:22 WG2019718
(S) 2-Fluorobiphenyl 73.8 22.0-127 03/11/2023 00:22 WG2019718
(S) p-Terphenyl-d14 80.1 29.0-141 03/11/2023 00:22 WG2019718
(S) Phenol-d5 24.5 8.00-424 03/11/2023 00:22 WG2019718
(S) 2-Fluorophenol 33.0 10.0-120 03/11/2023 00:22 WG2019718
(S) 2,4,6-Tribromophenol 59.5 10.0-153 03/11/2023 00:22 WG2019718
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 9 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 9 of 78
SAMPLE RESULTS - 02
L1592757
MW-3
Collected date/time: 03/06/23 10:45
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene 3580 100 100 03/09/2023 19:24 WG2020042
Bromobenzene ND 100 100 03/09/2023 19:24 WG2020042
Bromodichloromethane ND 100 100 03/09/2023 19:24 WG2020042
Bromochloromethane ND 100 100 03/09/2023 19:24 WG2020042
Bromoform ND 100 100 03/09/2023 19:24 WG2020042
Bromomethane ND 500 100 03/09/2023 19:24 WG2020042
n-Butylbenzene ND 100 100 03/09/2023 19:24 WG2020042
sec-Butylbenzene ND 100 100 03/09/2023 19:24 WG2020042
tert-Butylbenzene ND 100 100 03/09/2023 19:24 WG2020042
Carbon tetrachloride ND 100 100 03/09/2023 19:24 WG2020042
Chlorobenzene ND 100 100 03/09/2023 19:24 WG2020042
Chlorodibromomethane ND 100 100 03/09/2023 19:24 WG2020042
Chloroethane ND 500 100 03/09/2023 19:24 WG2020042
Chloroform ND 500 100 03/09/2023 19:24 WG2020042
Chloromethane ND 250 100 03/09/2023 19:24 WG2020042
2-Chlorotoluene ND 100 100 03/09/2023 19:24 WG2020042
4-Chlorotoluene ND 100 100 03/09/2023 19:24 WG2020042
1,2-Dibromo-3-Chloropropane ND 500 100 03/09/2023 19:24 WG2020042
1,2-Dibromoethane ND 100 100 03/09/2023 19:24 WG2020042
Dibromomethane ND 100 100 03/09/2023 19:24 WG2020042
1,2-Dichlorobenzene ND 100 100 03/09/2023 19:24 WG2020042
1,3-Dichlorobenzene ND 100 100 03/09/2023 19:24 WG2020042
1,4-Dichlorobenzene ND 100 100 03/09/2023 19:24 WG2020042
Dichlorodifluoromethane ND 500 100 03/09/2023 19:24 WG2020042
1,1-Dichloroethane ND 100 100 03/09/2023 19:24 WG2020042
1,2-Dichloroethane ND 100 100 03/09/2023 19:24 WG2020042
1,1-Dichloroethene ND 100 100 03/09/2023 19:24 WG2020042
cis-1,2-Dichloroethene ND 100 100 03/09/2023 19:24 WG2020042
trans-1,2-Dichloroethene ND 100 100 03/09/2023 19:24 WG2020042
1,2-Dichloropropane ND 100 100 03/09/2023 19:24 WG2020042
1,1-Dichloropropene ND 100 100 03/09/2023 19:24 WG2020042
1,3-Dichloropropane ND 100 100 03/09/2023 19:24 WG2020042
cis-1,3-Dichloropropene ND 100 100 03/09/2023 19:24 WG2020042
trans-1,3-Dichloropropene ND 100 100 03/09/2023 19:24 WG2020042
2,2-Dichloropropane ND 100 100 03/09/2023 19:24 WG2020042
Di-isopropyl ether ND 100 100 03/09/2023 19:24 WG2020042
Ethylbenzene 411 100 100 03/09/2023 19:24 WG2020042
Hexachloro-1,3-butadiene ND 100 100 03/09/2023 19:24 WG2020042
Isopropylbenzene ND 100 100 03/09/2023 19:24 WG2020042
Methylene Chloride ND 500 100 03/09/2023 19:24 WG2020042
Methyl tert-butyl ether ND 100 100 03/09/2023 19:24 WG2020042
Naphthalene ND 500 100 03/09/2023 19:24 WG2020042
n-Propylbenzene ND 100 100 03/09/2023 19:24 WG2020042
Styrene ND 100 100 03/09/2023 19:24 WG2020042
1,1,1,2-Tetrachloroethane ND 100 100 03/09/2023 19:24 WG2020042
1,1,2,2-Tetrachloroethane ND 100 100 03/09/2023 19:24 WG2020042
Tetrachloroethene ND 100 100 03/09/2023 19:24 WG2020042
Toluene 5600 100 100 03/09/2023 19:24 WG2020042
1,2,3-Trichlorobenzene ND 100 100 03/09/2023 19:24 WG2020042
1,2,4-Trichlorobenzene ND 100 100 03/09/2023 19:24 WG2020042
1,1,1-Trichloroethane ND 100 100 03/09/2023 19:24 WG2020042
1,1,2-Trichloroethane ND 100 100 03/09/2023 19:24 WG2020042
Trichloroethene ND 100 100 03/09/2023 19:24 WG2020042
Trichlorofluoromethane ND 500 100 03/09/2023 19:24 WG2020042
1,2,3-Trichloropropane ND 250 100 03/09/2023 19:24 WG2020042
1,2,4-Trimethylbenzene 477 100 100 03/09/2023 19:24 WG2020042
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 10 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 10 of 78
SAMPLE RESULTS - 02
L1592757
MW-3
Collected date/time: 03/06/23 10:45
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene 127 100 100 03/09/2023 19:24 WG2020042
Vinyl chloride ND 100 100 03/09/2023 19:24 WG2020042
o-Xylene 1280 100 100 03/09/2023 19:24 WG2020042
m&p-Xylenes 2550 200 100 03/09/2023 19:24 WG2020042
ethanol ND 10000 100 03/09/2023 19:24 WG2020042
tert-Amyl Methyl Ether ND 100 100 03/09/2023 19:24 WG2020042
Ethyl tert-butyl ether ND 100 100 03/09/2023 19:24 WG2020042
tert-Butyl alcohol ND 500 100 03/09/2023 19:24 WG2020042
t-Amyl Alcohol ND 5000 100 03/09/2023 19:24 WG2020042
tert-Butyl formate ND 2000 100 03/10/2023 19:50 WG2020940
(S) Toluene-d8 95.9 80.0-120 03/09/2023 19:24 WG2020042
(S) Toluene-d8 102 80.0-120 03/10/2023 19:50 WG2020940
(S) 4-Bromofluorobenzene 91.3 77.0-126 03/09/2023 19:24 WG2020042
(S) 4-Bromofluorobenzene 106 77.0-126 03/10/2023 19:50 WG2020940
(S) 1,2-Dichloroethane-d4 95.0 70.0-130 03/09/2023 19:24 WG2020042
(S) 1,2-Dichloroethane-d4 108 70.0-130 03/10/2023 19:50 WG2020940
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 03/14/2023 17:02 WG2020454
Unadjusted C19-C36 Aliphatics ND 100 1 03/14/2023 17:02 WG2020454
Unadjusted C11-C22 Aromatics 213 100 1 03/14/2023 23:01 WG2020454
Unadjusted Total Petroleum
Hydrocarbons 213 100 1 03/14/2023 17:02 WG2020454
(S) o-Terphenyl 92.6 40.0-140 03/14/2023 23:01 WG2020454
(S) 1-Chloro-octadecane 77.5 40.0-140 03/14/2023 17:02 WG2020454
(S) 2-Fluorobiphenyl 93.5 40.0-140 03/14/2023 23:01 WG2020454
(S) 2-Bromonaphthalene 102 40.0-140 03/14/2023 23:01 WG2020454
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 03/11/2023 00:43 WG2019718
Acenaphthylene ND 1.00 1 03/11/2023 00:43 WG2019718
Anthracene ND 1.00 1 03/11/2023 00:43 WG2019718
Benzo(a)anthracene ND 1.00 1 03/11/2023 00:43 WG2019718
Benzo(b)fluoranthene ND 1.00 1 03/11/2023 00:43 WG2019718
Benzo(k)fluoranthene ND 1.00 1 03/11/2023 00:43 WG2019718
Benzo(g,h,i)perylene ND 1.00 1 03/11/2023 00:43 WG2019718
Benzo(a)pyrene ND 1.00 1 03/11/2023 00:43 WG2019718
Bis(2-chlorethoxy)methane ND 10.0 1 03/11/2023 00:43 WG2019718
Bis(2-chloroethyl)ether ND 10.0 1 03/11/2023 00:43 WG2019718
2,2-Oxybis(1-Chloropropane)ND 10.0 1 03/11/2023 00:43 WG2019718
4-Bromophenyl-phenylether ND 10.0 1 03/11/2023 00:43 WG2019718
2-Chloronaphthalene ND 1.00 1 03/11/2023 00:43 WG2019718
4-Chlorophenyl-phenylether ND 10.0 1 03/11/2023 00:43 WG2019718
Chrysene ND 1.00 1 03/11/2023 00:43 WG2019718
Dibenz(a,h)anthracene ND 1.00 1 03/11/2023 00:43 WG2019718
3,3-Dichlorobenzidine ND 10.0 1 03/11/2023 00:43 WG2019718
2,4-Dinitrotoluene ND 10.0 1 03/11/2023 00:43 WG2019718
2,6-Dinitrotoluene ND 10.0 1 03/11/2023 00:43 WG2019718
Fluoranthene ND 1.00 1 03/11/2023 00:43 WG2019718
Fluorene ND 1.00 1 03/11/2023 00:43 WG2019718
Hexachlorobenzene ND 1.00 1 03/11/2023 00:43 WG2019718
Hexachloro-1,3-butadiene ND 10.0 1 03/11/2023 00:43 WG2019718
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 11 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 11 of 78
SAMPLE RESULTS - 02
L1592757
MW-3
Collected date/time: 03/06/23 10:45
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Hexachlorocyclopentadiene ND 10.0 1 03/11/2023 00:43 WG2019718
Hexachloroethane ND 10.0 1 03/11/2023 00:43 WG2019718
Indeno(1,2,3-cd)pyrene ND 1.00 1 03/11/2023 00:43 WG2019718
Isophorone ND 10.0 1 03/11/2023 00:43 WG2019718
Naphthalene 42.3 1.00 1 03/11/2023 00:43 WG2019718
Nitrobenzene ND 10.0 1 03/11/2023 00:43 WG2019718
n-Nitrosodimethylamine ND 10.0 1 03/11/2023 00:43 WG2019718
n-Nitrosodiphenylamine ND 10.0 1 03/11/2023 00:43 WG2019718
n-Nitrosodi-n-propylamine ND 10.0 1 03/11/2023 00:43 WG2019718
Phenanthrene ND 1.00 1 03/11/2023 00:43 WG2019718
Benzylbutyl phthalate ND 3.00 1 03/11/2023 00:43 WG2019718
Bis(2-ethylhexyl)phthalate ND 3.00 1 03/11/2023 00:43 WG2019718
Di-n-butyl phthalate ND 3.00 1 03/11/2023 00:43 WG2019718
Diethyl phthalate ND 3.00 1 03/11/2023 00:43 WG2019718
Dimethyl phthalate ND 3.00 1 03/11/2023 00:43 WG2019718
Di-n-octyl phthalate ND 3.00 1 03/11/2023 00:43 WG2019718
Pyrene ND 1.00 1 03/11/2023 00:43 WG2019718
1,2,4-Trichlorobenzene ND 10.0 1 03/11/2023 00:43 WG2019718
4-Chloro-3-methylphenol ND 10.0 1 03/11/2023 00:43 WG2019718
2-Chlorophenol ND 10.0 1 03/11/2023 00:43 WG2019718
2,4-Dichlorophenol ND 10.0 1 03/11/2023 00:43 WG2019718
2,4-Dimethylphenol ND 10.0 1 03/11/2023 00:43 WG2019718
4,6-Dinitro-2-methylphenol ND 10.0 1 03/11/2023 00:43 WG2019718
2,4-Dinitrophenol ND 10.0 1 03/11/2023 00:43 WG2019718
2-Nitrophenol ND 10.0 1 03/11/2023 00:43 WG2019718
4-Nitrophenol ND 10.0 1 03/11/2023 00:43 WG2019718
Pentachlorophenol ND 10.0 1 03/11/2023 00:43 WG2019718
Phenol ND 10.0 1 03/11/2023 00:43 WG2019718
2,4,6-Trichlorophenol ND 10.0 1 03/11/2023 00:43 WG2019718
(S) Nitrobenzene-d5 79.0 15.0-314 03/11/2023 00:43 WG2019718
(S) 2-Fluorobiphenyl 74.3 22.0-127 03/11/2023 00:43 WG2019718
(S) p-Terphenyl-d14 72.2 29.0-141 03/11/2023 00:43 WG2019718
(S) Phenol-d5 16.4 8.00-424 03/11/2023 00:43 WG2019718
(S) 2-Fluorophenol 21.9 10.0-120 03/11/2023 00:43 WG2019718
(S) 2,4,6-Tribromophenol 72.1 10.0-153 03/11/2023 00:43 WG2019718
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 12 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 12 of 78
SAMPLE RESULTS - 03
L1592757
MW-5
Collected date/time: 03/06/23 14:25
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene ND 1.00 1 03/09/2023 14:21 WG2020042
Bromobenzene ND 1.00 1 03/09/2023 14:21 WG2020042
Bromodichloromethane ND 1.00 1 03/09/2023 14:21 WG2020042
Bromochloromethane ND 1.00 1 03/09/2023 14:21 WG2020042
Bromoform ND 1.00 1 03/09/2023 14:21 WG2020042
Bromomethane ND 5.00 1 03/09/2023 14:21 WG2020042
n-Butylbenzene ND 1.00 1 03/09/2023 14:21 WG2020042
sec-Butylbenzene ND 1.00 1 03/09/2023 14:21 WG2020042
tert-Butylbenzene ND 1.00 1 03/09/2023 14:21 WG2020042
Carbon tetrachloride ND 1.00 1 03/09/2023 14:21 WG2020042
Chlorobenzene ND 1.00 1 03/09/2023 14:21 WG2020042
Chlorodibromomethane ND 1.00 1 03/09/2023 14:21 WG2020042
Chloroethane ND 5.00 1 03/09/2023 14:21 WG2020042
Chloroform ND 5.00 1 03/09/2023 14:21 WG2020042
Chloromethane ND 2.50 1 03/09/2023 14:21 WG2020042
2-Chlorotoluene ND 1.00 1 03/09/2023 14:21 WG2020042
4-Chlorotoluene ND 1.00 1 03/09/2023 14:21 WG2020042
1,2-Dibromo-3-Chloropropane ND 5.00 1 03/09/2023 14:21 WG2020042
1,2-Dibromoethane ND 1.00 1 03/09/2023 14:21 WG2020042
Dibromomethane ND 1.00 1 03/09/2023 14:21 WG2020042
1,2-Dichlorobenzene ND 1.00 1 03/09/2023 14:21 WG2020042
1,3-Dichlorobenzene ND 1.00 1 03/09/2023 14:21 WG2020042
1,4-Dichlorobenzene ND 1.00 1 03/09/2023 14:21 WG2020042
Dichlorodifluoromethane ND 5.00 1 03/09/2023 14:21 WG2020042
1,1-Dichloroethane ND 1.00 1 03/09/2023 14:21 WG2020042
1,2-Dichloroethane ND 1.00 1 03/09/2023 14:21 WG2020042
1,1-Dichloroethene ND 1.00 1 03/09/2023 14:21 WG2020042
cis-1,2-Dichloroethene ND 1.00 1 03/09/2023 14:21 WG2020042
trans-1,2-Dichloroethene ND 1.00 1 03/09/2023 14:21 WG2020042
1,2-Dichloropropane ND 1.00 1 03/09/2023 14:21 WG2020042
1,1-Dichloropropene ND 1.00 1 03/09/2023 14:21 WG2020042
1,3-Dichloropropane ND 1.00 1 03/09/2023 14:21 WG2020042
cis-1,3-Dichloropropene ND 1.00 1 03/09/2023 14:21 WG2020042
trans-1,3-Dichloropropene ND 1.00 1 03/09/2023 14:21 WG2020042
2,2-Dichloropropane ND 1.00 1 03/09/2023 14:21 WG2020042
Di-isopropyl ether ND 1.00 1 03/09/2023 14:21 WG2020042
Ethylbenzene ND 1.00 1 03/09/2023 14:21 WG2020042
Hexachloro-1,3-butadiene ND 1.00 1 03/09/2023 14:21 WG2020042
Isopropylbenzene ND 1.00 1 03/09/2023 14:21 WG2020042
Methylene Chloride ND 5.00 1 03/09/2023 14:21 WG2020042
Methyl tert-butyl ether ND 1.00 1 03/09/2023 14:21 WG2020042
Naphthalene ND 5.00 1 03/09/2023 14:21 WG2020042
n-Propylbenzene ND 1.00 1 03/09/2023 14:21 WG2020042
Styrene ND 1.00 1 03/09/2023 14:21 WG2020042
1,1,1,2-Tetrachloroethane ND 1.00 1 03/09/2023 14:21 WG2020042
1,1,2,2-Tetrachloroethane ND 1.00 1 03/09/2023 14:21 WG2020042
Tetrachloroethene ND 1.00 1 03/09/2023 14:21 WG2020042
Toluene ND 1.00 1 03/09/2023 14:21 WG2020042
1,2,3-Trichlorobenzene ND 1.00 1 03/09/2023 14:21 WG2020042
1,2,4-Trichlorobenzene ND 1.00 1 03/09/2023 14:21 WG2020042
1,1,1-Trichloroethane ND 1.00 1 03/09/2023 14:21 WG2020042
1,1,2-Trichloroethane ND 1.00 1 03/09/2023 14:21 WG2020042
Trichloroethene ND 1.00 1 03/09/2023 14:21 WG2020042
Trichlorofluoromethane ND 5.00 1 03/09/2023 14:21 WG2020042
1,2,3-Trichloropropane ND 2.50 1 03/09/2023 14:21 WG2020042
1,2,4-Trimethylbenzene ND 1.00 1 03/09/2023 14:21 WG2020042
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 13 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 13 of 78
SAMPLE RESULTS - 03
L1592757
MW-5
Collected date/time: 03/06/23 14:25
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 03/09/2023 14:21 WG2020042
Vinyl chloride ND 1.00 1 03/09/2023 14:21 WG2020042
o-Xylene ND 1.00 1 03/09/2023 14:21 WG2020042
m&p-Xylenes ND 2.00 1 03/09/2023 14:21 WG2020042
ethanol ND 100 1 03/09/2023 14:21 WG2020042
tert-Amyl Methyl Ether ND 1.00 1 03/09/2023 14:21 WG2020042
Ethyl tert-butyl ether ND 1.00 1 03/09/2023 14:21 WG2020042
tert-Butyl alcohol ND 5.00 1 03/09/2023 14:21 WG2020042
t-Amyl Alcohol ND 50.0 1 03/09/2023 14:21 WG2020042
tert-Butyl formate ND 20.0 1 03/10/2023 16:13 WG2020940
(S) Toluene-d8 99.4 80.0-120 03/09/2023 14:21 WG2020042
(S) Toluene-d8 104 80.0-120 03/10/2023 16:13 WG2020940
(S) 4-Bromofluorobenzene 89.4 77.0-126 03/09/2023 14:21 WG2020042
(S) 4-Bromofluorobenzene 109 77.0-126 03/10/2023 16:13 WG2020940
(S) 1,2-Dichloroethane-d4 92.9 70.0-130 03/09/2023 14:21 WG2020042
(S) 1,2-Dichloroethane-d4 109 70.0-130 03/10/2023 16:13 WG2020940
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 03/14/2023 17:26 WG2020454
Unadjusted C19-C36 Aliphatics ND 100 1 03/14/2023 17:26 WG2020454
Unadjusted C11-C22 Aromatics ND 100 1 03/14/2023 22:37 WG2020454
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 03/14/2023 17:26 WG2020454
(S) o-Terphenyl 90.5 40.0-140 03/14/2023 22:37 WG2020454
(S) 1-Chloro-octadecane 87.0 40.0-140 03/14/2023 17:26 WG2020454
(S) 2-Fluorobiphenyl 94.2 40.0-140 03/14/2023 22:37 WG2020454
(S) 2-Bromonaphthalene 103 40.0-140 03/14/2023 22:37 WG2020454
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 03/11/2023 01:04 WG2019718
Acenaphthylene ND 1.00 1 03/11/2023 01:04 WG2019718
Anthracene ND 1.00 1 03/11/2023 01:04 WG2019718
Benzo(a)anthracene ND 1.00 1 03/11/2023 01:04 WG2019718
Benzo(b)fluoranthene ND 1.00 1 03/11/2023 01:04 WG2019718
Benzo(k)fluoranthene ND 1.00 1 03/11/2023 01:04 WG2019718
Benzo(g,h,i)perylene ND 1.00 1 03/11/2023 01:04 WG2019718
Benzo(a)pyrene ND 1.00 1 03/11/2023 01:04 WG2019718
Bis(2-chlorethoxy)methane ND 10.0 1 03/11/2023 01:04 WG2019718
Bis(2-chloroethyl)ether ND 10.0 1 03/11/2023 01:04 WG2019718
2,2-Oxybis(1-Chloropropane)ND 10.0 1 03/11/2023 01:04 WG2019718
4-Bromophenyl-phenylether ND 10.0 1 03/11/2023 01:04 WG2019718
2-Chloronaphthalene ND 1.00 1 03/11/2023 01:04 WG2019718
4-Chlorophenyl-phenylether ND 10.0 1 03/11/2023 01:04 WG2019718
Chrysene ND 1.00 1 03/11/2023 01:04 WG2019718
Dibenz(a,h)anthracene ND 1.00 1 03/11/2023 01:04 WG2019718
3,3-Dichlorobenzidine ND 10.0 1 03/11/2023 01:04 WG2019718
2,4-Dinitrotoluene ND 10.0 1 03/11/2023 01:04 WG2019718
2,6-Dinitrotoluene ND 10.0 1 03/11/2023 01:04 WG2019718
Fluoranthene ND 1.00 1 03/11/2023 01:04 WG2019718
Fluorene ND 1.00 1 03/11/2023 01:04 WG2019718
Hexachlorobenzene ND 1.00 1 03/11/2023 01:04 WG2019718
Hexachloro-1,3-butadiene ND 10.0 1 03/11/2023 01:04 WG2019718
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 14 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 14 of 78
SAMPLE RESULTS - 03
L1592757
MW-5
Collected date/time: 03/06/23 14:25
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Hexachlorocyclopentadiene ND 10.0 1 03/11/2023 01:04 WG2019718
Hexachloroethane ND 10.0 1 03/11/2023 01:04 WG2019718
Indeno(1,2,3-cd)pyrene ND 1.00 1 03/11/2023 01:04 WG2019718
Isophorone ND 10.0 1 03/11/2023 01:04 WG2019718
Naphthalene ND 1.00 1 03/11/2023 01:04 WG2019718
Nitrobenzene ND 10.0 1 03/11/2023 01:04 WG2019718
n-Nitrosodimethylamine ND 10.0 1 03/11/2023 01:04 WG2019718
n-Nitrosodiphenylamine ND 10.0 1 03/11/2023 01:04 WG2019718
n-Nitrosodi-n-propylamine ND 10.0 1 03/11/2023 01:04 WG2019718
Phenanthrene ND 1.00 1 03/11/2023 01:04 WG2019718
Benzylbutyl phthalate ND 3.00 1 03/11/2023 01:04 WG2019718
Bis(2-ethylhexyl)phthalate ND 3.00 1 03/11/2023 01:04 WG2019718
Di-n-butyl phthalate ND 3.00 1 03/11/2023 01:04 WG2019718
Diethyl phthalate ND 3.00 1 03/11/2023 01:04 WG2019718
Dimethyl phthalate ND 3.00 1 03/11/2023 01:04 WG2019718
Di-n-octyl phthalate ND 3.00 1 03/11/2023 01:04 WG2019718
Pyrene ND 1.00 1 03/11/2023 01:04 WG2019718
1,2,4-Trichlorobenzene ND 10.0 1 03/11/2023 01:04 WG2019718
4-Chloro-3-methylphenol ND 10.0 1 03/11/2023 01:04 WG2019718
2-Chlorophenol ND 10.0 1 03/11/2023 01:04 WG2019718
2,4-Dichlorophenol ND 10.0 1 03/11/2023 01:04 WG2019718
2,4-Dimethylphenol ND 10.0 1 03/11/2023 01:04 WG2019718
4,6-Dinitro-2-methylphenol ND 10.0 1 03/11/2023 01:04 WG2019718
2,4-Dinitrophenol ND 10.0 1 03/11/2023 01:04 WG2019718
2-Nitrophenol ND 10.0 1 03/11/2023 01:04 WG2019718
4-Nitrophenol ND 10.0 1 03/11/2023 01:04 WG2019718
Pentachlorophenol ND 10.0 1 03/11/2023 01:04 WG2019718
Phenol ND 10.0 1 03/11/2023 01:04 WG2019718
2,4,6-Trichlorophenol ND 10.0 1 03/11/2023 01:04 WG2019718
(S) Nitrobenzene-d5 96.8 15.0-314 03/11/2023 01:04 WG2019718
(S) 2-Fluorobiphenyl 76.7 22.0-127 03/11/2023 01:04 WG2019718
(S) p-Terphenyl-d14 78.5 29.0-141 03/11/2023 01:04 WG2019718
(S) Phenol-d5 21.3 8.00-424 03/11/2023 01:04 WG2019718
(S) 2-Fluorophenol 31.5 10.0-120 03/11/2023 01:04 WG2019718
(S) 2,4,6-Tribromophenol 61.5 10.0-153 03/11/2023 01:04 WG2019718
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 15 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 15 of 78
SAMPLE RESULTS - 04
L1592757
MW-6
Collected date/time: 03/06/23 14:20
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene ND 1.00 1 03/09/2023 15:48 WG2020042
Bromobenzene ND 1.00 1 03/09/2023 15:48 WG2020042
Bromodichloromethane ND 1.00 1 03/09/2023 15:48 WG2020042
Bromochloromethane ND 1.00 1 03/09/2023 15:48 WG2020042
Bromoform ND 1.00 1 03/09/2023 15:48 WG2020042
Bromomethane ND 5.00 1 03/09/2023 15:48 WG2020042
n-Butylbenzene ND 1.00 1 03/09/2023 15:48 WG2020042
sec-Butylbenzene ND 1.00 1 03/09/2023 15:48 WG2020042
tert-Butylbenzene ND 1.00 1 03/09/2023 15:48 WG2020042
Carbon tetrachloride ND 1.00 1 03/09/2023 15:48 WG2020042
Chlorobenzene ND 1.00 1 03/09/2023 15:48 WG2020042
Chlorodibromomethane ND 1.00 1 03/09/2023 15:48 WG2020042
Chloroethane ND 5.00 1 03/09/2023 15:48 WG2020042
Chloroform ND 5.00 1 03/09/2023 15:48 WG2020042
Chloromethane ND 2.50 1 03/09/2023 15:48 WG2020042
2-Chlorotoluene ND 1.00 1 03/09/2023 15:48 WG2020042
4-Chlorotoluene ND 1.00 1 03/09/2023 15:48 WG2020042
1,2-Dibromo-3-Chloropropane ND 5.00 1 03/09/2023 15:48 WG2020042
1,2-Dibromoethane ND 1.00 1 03/09/2023 15:48 WG2020042
Dibromomethane ND 1.00 1 03/09/2023 15:48 WG2020042
1,2-Dichlorobenzene ND 1.00 1 03/09/2023 15:48 WG2020042
1,3-Dichlorobenzene ND 1.00 1 03/09/2023 15:48 WG2020042
1,4-Dichlorobenzene ND 1.00 1 03/09/2023 15:48 WG2020042
Dichlorodifluoromethane ND 5.00 1 03/09/2023 15:48 WG2020042
1,1-Dichloroethane ND 1.00 1 03/09/2023 15:48 WG2020042
1,2-Dichloroethane ND 1.00 1 03/09/2023 15:48 WG2020042
1,1-Dichloroethene ND 1.00 1 03/09/2023 15:48 WG2020042
cis-1,2-Dichloroethene ND 1.00 1 03/09/2023 15:48 WG2020042
trans-1,2-Dichloroethene ND 1.00 1 03/09/2023 15:48 WG2020042
1,2-Dichloropropane ND 1.00 1 03/09/2023 15:48 WG2020042
1,1-Dichloropropene ND 1.00 1 03/09/2023 15:48 WG2020042
1,3-Dichloropropane ND 1.00 1 03/09/2023 15:48 WG2020042
cis-1,3-Dichloropropene ND 1.00 1 03/09/2023 15:48 WG2020042
trans-1,3-Dichloropropene ND 1.00 1 03/09/2023 15:48 WG2020042
2,2-Dichloropropane ND 1.00 1 03/09/2023 15:48 WG2020042
Di-isopropyl ether ND 1.00 1 03/09/2023 15:48 WG2020042
Ethylbenzene ND 1.00 1 03/09/2023 15:48 WG2020042
Hexachloro-1,3-butadiene ND 1.00 1 03/09/2023 15:48 WG2020042
Isopropylbenzene ND 1.00 1 03/09/2023 15:48 WG2020042
Methylene Chloride ND 5.00 1 03/09/2023 15:48 WG2020042
Methyl tert-butyl ether ND 1.00 1 03/09/2023 15:48 WG2020042
Naphthalene ND 5.00 1 03/09/2023 15:48 WG2020042
n-Propylbenzene ND 1.00 1 03/09/2023 15:48 WG2020042
Styrene ND 1.00 1 03/09/2023 15:48 WG2020042
1,1,1,2-Tetrachloroethane ND 1.00 1 03/09/2023 15:48 WG2020042
1,1,2,2-Tetrachloroethane ND 1.00 1 03/09/2023 15:48 WG2020042
Tetrachloroethene ND 1.00 1 03/09/2023 15:48 WG2020042
Toluene ND 1.00 1 03/09/2023 15:48 WG2020042
1,2,3-Trichlorobenzene ND 1.00 1 03/09/2023 15:48 WG2020042
1,2,4-Trichlorobenzene ND 1.00 1 03/09/2023 15:48 WG2020042
1,1,1-Trichloroethane ND 1.00 1 03/09/2023 15:48 WG2020042
1,1,2-Trichloroethane ND 1.00 1 03/09/2023 15:48 WG2020042
Trichloroethene ND 1.00 1 03/09/2023 15:48 WG2020042
Trichlorofluoromethane ND 5.00 1 03/09/2023 15:48 WG2020042
1,2,3-Trichloropropane ND 2.50 1 03/09/2023 15:48 WG2020042
1,2,4-Trimethylbenzene ND 1.00 1 03/09/2023 15:48 WG2020042
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 16 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 16 of 78
SAMPLE RESULTS - 04
L1592757
MW-6
Collected date/time: 03/06/23 14:20
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 03/09/2023 15:48 WG2020042
Vinyl chloride ND 1.00 1 03/09/2023 15:48 WG2020042
o-Xylene ND 1.00 1 03/09/2023 15:48 WG2020042
m&p-Xylenes ND 2.00 1 03/09/2023 15:48 WG2020042
ethanol ND 100 1 03/09/2023 15:48 WG2020042
tert-Amyl Methyl Ether ND 1.00 1 03/09/2023 15:48 WG2020042
Ethyl tert-butyl ether ND 1.00 1 03/09/2023 15:48 WG2020042
tert-Butyl alcohol ND 5.00 1 03/09/2023 15:48 WG2020042
t-Amyl Alcohol ND 50.0 1 03/09/2023 15:48 WG2020042
tert-Butyl formate ND 20.0 1 03/10/2023 16:34 WG2020940
(S) Toluene-d8 99.5 80.0-120 03/09/2023 15:48 WG2020042
(S) Toluene-d8 102 80.0-120 03/10/2023 16:34 WG2020940
(S) 4-Bromofluorobenzene 94.1 77.0-126 03/09/2023 15:48 WG2020042
(S) 4-Bromofluorobenzene 104 77.0-126 03/10/2023 16:34 WG2020940
(S) 1,2-Dichloroethane-d4 94.9 70.0-130 03/09/2023 15:48 WG2020042
(S) 1,2-Dichloroethane-d4 108 70.0-130 03/10/2023 16:34 WG2020940
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 03/14/2023 17:50 WG2020454
Unadjusted C19-C36 Aliphatics ND 100 1 03/14/2023 17:50 WG2020454
Unadjusted C11-C22 Aromatics ND 100 1 03/14/2023 22:14 WG2020454
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 03/14/2023 17:50 WG2020454
(S) o-Terphenyl 86.7 40.0-140 03/14/2023 22:14 WG2020454
(S) 1-Chloro-octadecane 57.4 40.0-140 03/14/2023 17:50 WG2020454
(S) 2-Fluorobiphenyl 91.2 40.0-140 03/14/2023 22:14 WG2020454
(S) 2-Bromonaphthalene 99.7 40.0-140 03/14/2023 22:14 WG2020454
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 03/11/2023 01:26 WG2019718
Acenaphthylene ND 1.00 1 03/11/2023 01:26 WG2019718
Anthracene ND 1.00 1 03/11/2023 01:26 WG2019718
Benzo(a)anthracene ND 1.00 1 03/11/2023 01:26 WG2019718
Benzo(b)fluoranthene ND 1.00 1 03/11/2023 01:26 WG2019718
Benzo(k)fluoranthene ND 1.00 1 03/11/2023 01:26 WG2019718
Benzo(g,h,i)perylene ND 1.00 1 03/11/2023 01:26 WG2019718
Benzo(a)pyrene ND 1.00 1 03/11/2023 01:26 WG2019718
Bis(2-chlorethoxy)methane ND 10.0 1 03/11/2023 01:26 WG2019718
Bis(2-chloroethyl)ether ND 10.0 1 03/11/2023 01:26 WG2019718
2,2-Oxybis(1-Chloropropane)ND 10.0 1 03/11/2023 01:26 WG2019718
4-Bromophenyl-phenylether ND 10.0 1 03/11/2023 01:26 WG2019718
2-Chloronaphthalene ND 1.00 1 03/11/2023 01:26 WG2019718
4-Chlorophenyl-phenylether ND 10.0 1 03/11/2023 01:26 WG2019718
Chrysene ND 1.00 1 03/11/2023 01:26 WG2019718
Dibenz(a,h)anthracene ND 1.00 1 03/11/2023 01:26 WG2019718
3,3-Dichlorobenzidine ND 10.0 1 03/11/2023 01:26 WG2019718
2,4-Dinitrotoluene ND 10.0 1 03/11/2023 01:26 WG2019718
2,6-Dinitrotoluene ND 10.0 1 03/11/2023 01:26 WG2019718
Fluoranthene ND 1.00 1 03/11/2023 01:26 WG2019718
Fluorene ND 1.00 1 03/11/2023 01:26 WG2019718
Hexachlorobenzene ND 1.00 1 03/11/2023 01:26 WG2019718
Hexachloro-1,3-butadiene ND 10.0 1 03/11/2023 01:26 WG2019718
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 17 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 17 of 78
SAMPLE RESULTS - 04
L1592757
MW-6
Collected date/time: 03/06/23 14:20
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Hexachlorocyclopentadiene ND 10.0 1 03/11/2023 01:26 WG2019718
Hexachloroethane ND 10.0 1 03/11/2023 01:26 WG2019718
Indeno(1,2,3-cd)pyrene ND 1.00 1 03/11/2023 01:26 WG2019718
Isophorone ND 10.0 1 03/11/2023 01:26 WG2019718
Naphthalene ND 1.00 1 03/11/2023 01:26 WG2019718
Nitrobenzene ND 10.0 1 03/11/2023 01:26 WG2019718
n-Nitrosodimethylamine ND 10.0 1 03/11/2023 01:26 WG2019718
n-Nitrosodiphenylamine ND 10.0 1 03/11/2023 01:26 WG2019718
n-Nitrosodi-n-propylamine ND 10.0 1 03/11/2023 01:26 WG2019718
Phenanthrene ND 1.00 1 03/11/2023 01:26 WG2019718
Benzylbutyl phthalate ND 3.00 1 03/11/2023 01:26 WG2019718
Bis(2-ethylhexyl)phthalate ND 3.00 1 03/11/2023 01:26 WG2019718
Di-n-butyl phthalate ND 3.00 1 03/11/2023 01:26 WG2019718
Diethyl phthalate ND 3.00 1 03/11/2023 01:26 WG2019718
Dimethyl phthalate ND 3.00 1 03/11/2023 01:26 WG2019718
Di-n-octyl phthalate ND 3.00 1 03/11/2023 01:26 WG2019718
Pyrene ND 1.00 1 03/11/2023 01:26 WG2019718
1,2,4-Trichlorobenzene ND 10.0 1 03/11/2023 01:26 WG2019718
4-Chloro-3-methylphenol ND 10.0 1 03/11/2023 01:26 WG2019718
2-Chlorophenol ND 10.0 1 03/11/2023 01:26 WG2019718
2,4-Dichlorophenol ND 10.0 1 03/11/2023 01:26 WG2019718
2,4-Dimethylphenol ND 10.0 1 03/11/2023 01:26 WG2019718
4,6-Dinitro-2-methylphenol ND 10.0 1 03/11/2023 01:26 WG2019718
2,4-Dinitrophenol ND 10.0 1 03/11/2023 01:26 WG2019718
2-Nitrophenol ND 10.0 1 03/11/2023 01:26 WG2019718
4-Nitrophenol ND 10.0 1 03/11/2023 01:26 WG2019718
Pentachlorophenol ND 10.0 1 03/11/2023 01:26 WG2019718
Phenol ND 10.0 1 03/11/2023 01:26 WG2019718
2,4,6-Trichlorophenol ND 10.0 1 03/11/2023 01:26 WG2019718
(S) Nitrobenzene-d5 87.5 15.0-314 03/11/2023 01:26 WG2019718
(S) 2-Fluorobiphenyl 70.8 22.0-127 03/11/2023 01:26 WG2019718
(S) p-Terphenyl-d14 80.1 29.0-141 03/11/2023 01:26 WG2019718
(S) Phenol-d5 22.8 8.00-424 03/11/2023 01:26 WG2019718
(S) 2-Fluorophenol 32.1 10.0-120 03/11/2023 01:26 WG2019718
(S) 2,4,6-Tribromophenol 61.5 10.0-153 03/11/2023 01:26 WG2019718
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 18 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 18 of 78
SAMPLE RESULTS - 05
L1592757
MW-7
Collected date/time: 03/06/23 14:55
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene ND 1.00 1 03/09/2023 16:09 WG2020042
Bromobenzene ND 1.00 1 03/09/2023 16:09 WG2020042
Bromodichloromethane ND 1.00 1 03/09/2023 16:09 WG2020042
Bromochloromethane ND 1.00 1 03/09/2023 16:09 WG2020042
Bromoform ND 1.00 1 03/09/2023 16:09 WG2020042
Bromomethane ND 5.00 1 03/09/2023 16:09 WG2020042
n-Butylbenzene ND 1.00 1 03/09/2023 16:09 WG2020042
sec-Butylbenzene ND 1.00 1 03/09/2023 16:09 WG2020042
tert-Butylbenzene ND 1.00 1 03/09/2023 16:09 WG2020042
Carbon tetrachloride ND 1.00 1 03/09/2023 16:09 WG2020042
Chlorobenzene ND 1.00 1 03/09/2023 16:09 WG2020042
Chlorodibromomethane ND 1.00 1 03/09/2023 16:09 WG2020042
Chloroethane ND 5.00 1 03/09/2023 16:09 WG2020042
Chloroform ND 5.00 1 03/09/2023 16:09 WG2020042
Chloromethane ND 2.50 1 03/09/2023 16:09 WG2020042
2-Chlorotoluene ND 1.00 1 03/09/2023 16:09 WG2020042
4-Chlorotoluene ND 1.00 1 03/09/2023 16:09 WG2020042
1,2-Dibromo-3-Chloropropane ND 5.00 1 03/09/2023 16:09 WG2020042
1,2-Dibromoethane ND 1.00 1 03/09/2023 16:09 WG2020042
Dibromomethane ND 1.00 1 03/09/2023 16:09 WG2020042
1,2-Dichlorobenzene ND 1.00 1 03/09/2023 16:09 WG2020042
1,3-Dichlorobenzene ND 1.00 1 03/09/2023 16:09 WG2020042
1,4-Dichlorobenzene ND 1.00 1 03/09/2023 16:09 WG2020042
Dichlorodifluoromethane ND 5.00 1 03/09/2023 16:09 WG2020042
1,1-Dichloroethane ND 1.00 1 03/09/2023 16:09 WG2020042
1,2-Dichloroethane ND 1.00 1 03/09/2023 16:09 WG2020042
1,1-Dichloroethene ND 1.00 1 03/09/2023 16:09 WG2020042
cis-1,2-Dichloroethene ND 1.00 1 03/09/2023 16:09 WG2020042
trans-1,2-Dichloroethene ND 1.00 1 03/09/2023 16:09 WG2020042
1,2-Dichloropropane ND 1.00 1 03/09/2023 16:09 WG2020042
1,1-Dichloropropene ND 1.00 1 03/09/2023 16:09 WG2020042
1,3-Dichloropropane ND 1.00 1 03/09/2023 16:09 WG2020042
cis-1,3-Dichloropropene ND 1.00 1 03/09/2023 16:09 WG2020042
trans-1,3-Dichloropropene ND 1.00 1 03/09/2023 16:09 WG2020042
2,2-Dichloropropane ND 1.00 1 03/09/2023 16:09 WG2020042
Di-isopropyl ether ND 1.00 1 03/09/2023 16:09 WG2020042
Ethylbenzene ND 1.00 1 03/09/2023 16:09 WG2020042
Hexachloro-1,3-butadiene ND 1.00 1 03/09/2023 16:09 WG2020042
Isopropylbenzene ND 1.00 1 03/09/2023 16:09 WG2020042
Methylene Chloride ND 5.00 1 03/09/2023 16:09 WG2020042
Methyl tert-butyl ether ND 1.00 1 03/09/2023 16:09 WG2020042
Naphthalene ND 5.00 1 03/09/2023 16:09 WG2020042
n-Propylbenzene ND 1.00 1 03/09/2023 16:09 WG2020042
Styrene ND 1.00 1 03/09/2023 16:09 WG2020042
1,1,1,2-Tetrachloroethane ND 1.00 1 03/09/2023 16:09 WG2020042
1,1,2,2-Tetrachloroethane ND 1.00 1 03/09/2023 16:09 WG2020042
Tetrachloroethene ND 1.00 1 03/09/2023 16:09 WG2020042
Toluene ND 1.00 1 03/09/2023 16:09 WG2020042
1,2,3-Trichlorobenzene ND 1.00 1 03/09/2023 16:09 WG2020042
1,2,4-Trichlorobenzene ND 1.00 1 03/09/2023 16:09 WG2020042
1,1,1-Trichloroethane ND 1.00 1 03/09/2023 16:09 WG2020042
1,1,2-Trichloroethane ND 1.00 1 03/09/2023 16:09 WG2020042
Trichloroethene ND 1.00 1 03/09/2023 16:09 WG2020042
Trichlorofluoromethane ND 5.00 1 03/09/2023 16:09 WG2020042
1,2,3-Trichloropropane ND 2.50 1 03/09/2023 16:09 WG2020042
1,2,4-Trimethylbenzene ND 1.00 1 03/09/2023 16:09 WG2020042
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 19 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 19 of 78
SAMPLE RESULTS - 05
L1592757
MW-7
Collected date/time: 03/06/23 14:55
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 03/09/2023 16:09 WG2020042
Vinyl chloride ND 1.00 1 03/09/2023 16:09 WG2020042
o-Xylene ND 1.00 1 03/09/2023 16:09 WG2020042
m&p-Xylenes ND 2.00 1 03/09/2023 16:09 WG2020042
ethanol ND 100 1 03/09/2023 16:09 WG2020042
tert-Amyl Methyl Ether ND 1.00 1 03/09/2023 16:09 WG2020042
Ethyl tert-butyl ether ND 1.00 1 03/09/2023 16:09 WG2020042
tert-Butyl alcohol ND 5.00 1 03/09/2023 16:09 WG2020042
t-Amyl Alcohol ND 50.0 1 03/09/2023 16:09 WG2020042
tert-Butyl formate ND 20.0 1 03/10/2023 16:56 WG2020940
(S) Toluene-d8 101 80.0-120 03/09/2023 16:09 WG2020042
(S) Toluene-d8 100 80.0-120 03/10/2023 16:56 WG2020940
(S) 4-Bromofluorobenzene 93.1 77.0-126 03/09/2023 16:09 WG2020042
(S) 4-Bromofluorobenzene 103 77.0-126 03/10/2023 16:56 WG2020940
(S) 1,2-Dichloroethane-d4 92.8 70.0-130 03/09/2023 16:09 WG2020042
(S) 1,2-Dichloroethane-d4 111 70.0-130 03/10/2023 16:56 WG2020940
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 03/14/2023 18:14 WG2020454
Unadjusted C19-C36 Aliphatics ND 100 1 03/14/2023 18:14 WG2020454
Unadjusted C11-C22 Aromatics ND 100 1 03/14/2023 21:50 WG2020454
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 03/14/2023 18:14 WG2020454
(S) o-Terphenyl 91.3 40.0-140 03/14/2023 21:50 WG2020454
(S) 1-Chloro-octadecane 86.8 40.0-140 03/14/2023 18:14 WG2020454
(S) 2-Fluorobiphenyl 91.2 40.0-140 03/14/2023 21:50 WG2020454
(S) 2-Bromonaphthalene 99.7 40.0-140 03/14/2023 21:50 WG2020454
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 03/11/2023 01:47 WG2019718
Acenaphthylene ND 1.00 1 03/11/2023 01:47 WG2019718
Anthracene ND 1.00 1 03/11/2023 01:47 WG2019718
Benzo(a)anthracene ND 1.00 1 03/11/2023 01:47 WG2019718
Benzo(b)fluoranthene ND 1.00 1 03/11/2023 01:47 WG2019718
Benzo(k)fluoranthene ND 1.00 1 03/11/2023 01:47 WG2019718
Benzo(g,h,i)perylene ND 1.00 1 03/11/2023 01:47 WG2019718
Benzo(a)pyrene ND 1.00 1 03/11/2023 01:47 WG2019718
Bis(2-chlorethoxy)methane ND 10.0 1 03/11/2023 01:47 WG2019718
Bis(2-chloroethyl)ether ND 10.0 1 03/11/2023 01:47 WG2019718
2,2-Oxybis(1-Chloropropane)ND 10.0 1 03/11/2023 01:47 WG2019718
4-Bromophenyl-phenylether ND 10.0 1 03/11/2023 01:47 WG2019718
2-Chloronaphthalene ND 1.00 1 03/11/2023 01:47 WG2019718
4-Chlorophenyl-phenylether ND 10.0 1 03/11/2023 01:47 WG2019718
Chrysene ND 1.00 1 03/11/2023 01:47 WG2019718
Dibenz(a,h)anthracene ND 1.00 1 03/11/2023 01:47 WG2019718
3,3-Dichlorobenzidine ND 10.0 1 03/11/2023 01:47 WG2019718
2,4-Dinitrotoluene ND 10.0 1 03/11/2023 01:47 WG2019718
2,6-Dinitrotoluene ND 10.0 1 03/11/2023 01:47 WG2019718
Fluoranthene ND 1.00 1 03/11/2023 01:47 WG2019718
Fluorene ND 1.00 1 03/11/2023 01:47 WG2019718
Hexachlorobenzene ND 1.00 1 03/11/2023 01:47 WG2019718
Hexachloro-1,3-butadiene ND 10.0 1 03/11/2023 01:47 WG2019718
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 20 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 20 of 78
SAMPLE RESULTS - 05
L1592757
MW-7
Collected date/time: 03/06/23 14:55
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Hexachlorocyclopentadiene ND 10.0 1 03/11/2023 01:47 WG2019718
Hexachloroethane ND 10.0 1 03/11/2023 01:47 WG2019718
Indeno(1,2,3-cd)pyrene ND 1.00 1 03/11/2023 01:47 WG2019718
Isophorone ND 10.0 1 03/11/2023 01:47 WG2019718
Naphthalene ND 1.00 1 03/11/2023 01:47 WG2019718
Nitrobenzene ND 10.0 1 03/11/2023 01:47 WG2019718
n-Nitrosodimethylamine ND 10.0 1 03/11/2023 01:47 WG2019718
n-Nitrosodiphenylamine ND 10.0 1 03/11/2023 01:47 WG2019718
n-Nitrosodi-n-propylamine ND 10.0 1 03/11/2023 01:47 WG2019718
Phenanthrene ND 1.00 1 03/11/2023 01:47 WG2019718
Benzylbutyl phthalate ND 3.00 1 03/11/2023 01:47 WG2019718
Bis(2-ethylhexyl)phthalate ND 3.00 1 03/11/2023 01:47 WG2019718
Di-n-butyl phthalate ND 3.00 1 03/11/2023 01:47 WG2019718
Diethyl phthalate ND 3.00 1 03/11/2023 01:47 WG2019718
Dimethyl phthalate ND 3.00 1 03/11/2023 01:47 WG2019718
Di-n-octyl phthalate ND 3.00 1 03/11/2023 01:47 WG2019718
Pyrene ND 1.00 1 03/11/2023 01:47 WG2019718
1,2,4-Trichlorobenzene ND 10.0 1 03/11/2023 01:47 WG2019718
4-Chloro-3-methylphenol ND 10.0 1 03/11/2023 01:47 WG2019718
2-Chlorophenol ND 10.0 1 03/11/2023 01:47 WG2019718
2,4-Dichlorophenol ND 10.0 1 03/11/2023 01:47 WG2019718
2,4-Dimethylphenol ND 10.0 1 03/11/2023 01:47 WG2019718
4,6-Dinitro-2-methylphenol ND 10.0 1 03/11/2023 01:47 WG2019718
2,4-Dinitrophenol ND 10.0 1 03/11/2023 01:47 WG2019718
2-Nitrophenol ND 10.0 1 03/11/2023 01:47 WG2019718
4-Nitrophenol ND 10.0 1 03/11/2023 01:47 WG2019718
Pentachlorophenol ND 10.0 1 03/11/2023 01:47 WG2019718
Phenol ND 10.0 1 03/11/2023 01:47 WG2019718
2,4,6-Trichlorophenol ND 10.0 1 03/11/2023 01:47 WG2019718
(S) Nitrobenzene-d5 91.2 15.0-314 03/11/2023 01:47 WG2019718
(S) 2-Fluorobiphenyl 73.0 22.0-127 03/11/2023 01:47 WG2019718
(S) p-Terphenyl-d14 81.1 29.0-141 03/11/2023 01:47 WG2019718
(S) Phenol-d5 22.7 8.00-424 03/11/2023 01:47 WG2019718
(S) 2-Fluorophenol 36.9 10.0-120 03/11/2023 01:47 WG2019718
(S) 2,4,6-Tribromophenol 70.0 10.0-153 03/11/2023 01:47 WG2019718
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 21 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 21 of 78
SAMPLE RESULTS - 06
L1592757
MW-8
Collected date/time: 03/06/23 09:45
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene ND 1.00 1 03/09/2023 16:31 WG2020042
Bromobenzene ND 1.00 1 03/09/2023 16:31 WG2020042
Bromodichloromethane ND 1.00 1 03/09/2023 16:31 WG2020042
Bromochloromethane ND 1.00 1 03/09/2023 16:31 WG2020042
Bromoform ND 1.00 1 03/09/2023 16:31 WG2020042
Bromomethane ND 5.00 1 03/09/2023 16:31 WG2020042
n-Butylbenzene ND 1.00 1 03/09/2023 16:31 WG2020042
sec-Butylbenzene ND 1.00 1 03/09/2023 16:31 WG2020042
tert-Butylbenzene ND 1.00 1 03/09/2023 16:31 WG2020042
Carbon tetrachloride ND 1.00 1 03/09/2023 16:31 WG2020042
Chlorobenzene ND 1.00 1 03/09/2023 16:31 WG2020042
Chlorodibromomethane ND 1.00 1 03/09/2023 16:31 WG2020042
Chloroethane ND 5.00 1 03/09/2023 16:31 WG2020042
Chloroform ND 5.00 1 03/09/2023 16:31 WG2020042
Chloromethane ND 2.50 1 03/09/2023 16:31 WG2020042
2-Chlorotoluene ND 1.00 1 03/09/2023 16:31 WG2020042
4-Chlorotoluene ND 1.00 1 03/09/2023 16:31 WG2020042
1,2-Dibromo-3-Chloropropane ND 5.00 1 03/09/2023 16:31 WG2020042
1,2-Dibromoethane ND 1.00 1 03/09/2023 16:31 WG2020042
Dibromomethane ND 1.00 1 03/09/2023 16:31 WG2020042
1,2-Dichlorobenzene ND 1.00 1 03/09/2023 16:31 WG2020042
1,3-Dichlorobenzene ND 1.00 1 03/09/2023 16:31 WG2020042
1,4-Dichlorobenzene ND 1.00 1 03/09/2023 16:31 WG2020042
Dichlorodifluoromethane ND 5.00 1 03/09/2023 16:31 WG2020042
1,1-Dichloroethane ND 1.00 1 03/09/2023 16:31 WG2020042
1,2-Dichloroethane ND 1.00 1 03/09/2023 16:31 WG2020042
1,1-Dichloroethene ND 1.00 1 03/09/2023 16:31 WG2020042
cis-1,2-Dichloroethene ND 1.00 1 03/09/2023 16:31 WG2020042
trans-1,2-Dichloroethene ND 1.00 1 03/09/2023 16:31 WG2020042
1,2-Dichloropropane ND 1.00 1 03/09/2023 16:31 WG2020042
1,1-Dichloropropene ND 1.00 1 03/09/2023 16:31 WG2020042
1,3-Dichloropropane ND 1.00 1 03/09/2023 16:31 WG2020042
cis-1,3-Dichloropropene ND 1.00 1 03/09/2023 16:31 WG2020042
trans-1,3-Dichloropropene ND 1.00 1 03/09/2023 16:31 WG2020042
2,2-Dichloropropane ND 1.00 1 03/09/2023 16:31 WG2020042
Di-isopropyl ether ND 1.00 1 03/09/2023 16:31 WG2020042
Ethylbenzene ND 1.00 1 03/09/2023 16:31 WG2020042
Hexachloro-1,3-butadiene ND 1.00 1 03/09/2023 16:31 WG2020042
Isopropylbenzene ND 1.00 1 03/09/2023 16:31 WG2020042
Methylene Chloride ND 5.00 1 03/09/2023 16:31 WG2020042
Methyl tert-butyl ether ND 1.00 1 03/09/2023 16:31 WG2020042
Naphthalene ND 5.00 1 03/09/2023 16:31 WG2020042
n-Propylbenzene ND 1.00 1 03/09/2023 16:31 WG2020042
Styrene ND 1.00 1 03/09/2023 16:31 WG2020042
1,1,1,2-Tetrachloroethane ND 1.00 1 03/09/2023 16:31 WG2020042
1,1,2,2-Tetrachloroethane ND 1.00 1 03/09/2023 16:31 WG2020042
Tetrachloroethene ND 1.00 1 03/09/2023 16:31 WG2020042
Toluene ND 1.00 1 03/09/2023 16:31 WG2020042
1,2,3-Trichlorobenzene ND 1.00 1 03/09/2023 16:31 WG2020042
1,2,4-Trichlorobenzene ND 1.00 1 03/09/2023 16:31 WG2020042
1,1,1-Trichloroethane ND 1.00 1 03/09/2023 16:31 WG2020042
1,1,2-Trichloroethane ND 1.00 1 03/09/2023 16:31 WG2020042
Trichloroethene ND 1.00 1 03/09/2023 16:31 WG2020042
Trichlorofluoromethane ND 5.00 1 03/09/2023 16:31 WG2020042
1,2,3-Trichloropropane ND 2.50 1 03/09/2023 16:31 WG2020042
1,2,4-Trimethylbenzene ND 1.00 1 03/09/2023 16:31 WG2020042
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 22 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 22 of 78
SAMPLE RESULTS - 06
L1592757
MW-8
Collected date/time: 03/06/23 09:45
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 03/09/2023 16:31 WG2020042
Vinyl chloride ND 1.00 1 03/09/2023 16:31 WG2020042
o-Xylene ND 1.00 1 03/09/2023 16:31 WG2020042
m&p-Xylenes ND 2.00 1 03/09/2023 16:31 WG2020042
ethanol ND 100 1 03/09/2023 16:31 WG2020042
tert-Amyl Methyl Ether ND 1.00 1 03/09/2023 16:31 WG2020042
Ethyl tert-butyl ether ND 1.00 1 03/09/2023 16:31 WG2020042
tert-Butyl alcohol ND 5.00 1 03/09/2023 16:31 WG2020042
t-Amyl Alcohol ND 50.0 1 03/09/2023 16:31 WG2020042
tert-Butyl formate ND 20.0 1 03/10/2023 17:18 WG2020940
(S) Toluene-d8 97.0 80.0-120 03/09/2023 16:31 WG2020042
(S) Toluene-d8 103 80.0-120 03/10/2023 17:18 WG2020940
(S) 4-Bromofluorobenzene 85.3 77.0-126 03/09/2023 16:31 WG2020042
(S) 4-Bromofluorobenzene 105 77.0-126 03/10/2023 17:18 WG2020940
(S) 1,2-Dichloroethane-d4 92.8 70.0-130 03/09/2023 16:31 WG2020042
(S) 1,2-Dichloroethane-d4 111 70.0-130 03/10/2023 17:18 WG2020940
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 03/14/2023 18:38 WG2020454
Unadjusted C19-C36 Aliphatics ND 100 1 03/14/2023 18:38 WG2020454
Unadjusted C11-C22 Aromatics ND 100 1 03/14/2023 21:26 WG2020454
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 03/14/2023 18:38 WG2020454
(S) o-Terphenyl 86.8 40.0-140 03/14/2023 21:26 WG2020454
(S) 1-Chloro-octadecane 71.8 40.0-140 03/14/2023 18:38 WG2020454
(S) 2-Fluorobiphenyl 89.6 40.0-140 03/14/2023 21:26 WG2020454
(S) 2-Bromonaphthalene 98.2 40.0-140 03/14/2023 21:26 WG2020454
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 03/11/2023 02:08 WG2019718
Acenaphthylene ND 1.00 1 03/11/2023 02:08 WG2019718
Anthracene ND 1.00 1 03/11/2023 02:08 WG2019718
Benzo(a)anthracene ND 1.00 1 03/11/2023 02:08 WG2019718
Benzo(b)fluoranthene ND 1.00 1 03/11/2023 02:08 WG2019718
Benzo(k)fluoranthene ND 1.00 1 03/11/2023 02:08 WG2019718
Benzo(g,h,i)perylene ND 1.00 1 03/11/2023 02:08 WG2019718
Benzo(a)pyrene ND 1.00 1 03/11/2023 02:08 WG2019718
Bis(2-chlorethoxy)methane ND 10.0 1 03/11/2023 02:08 WG2019718
Bis(2-chloroethyl)ether ND 10.0 1 03/11/2023 02:08 WG2019718
2,2-Oxybis(1-Chloropropane)ND 10.0 1 03/11/2023 02:08 WG2019718
4-Bromophenyl-phenylether ND 10.0 1 03/11/2023 02:08 WG2019718
2-Chloronaphthalene ND 1.00 1 03/11/2023 02:08 WG2019718
4-Chlorophenyl-phenylether ND 10.0 1 03/11/2023 02:08 WG2019718
Chrysene ND 1.00 1 03/11/2023 02:08 WG2019718
Dibenz(a,h)anthracene ND 1.00 1 03/11/2023 02:08 WG2019718
3,3-Dichlorobenzidine ND 10.0 1 03/11/2023 02:08 WG2019718
2,4-Dinitrotoluene ND 10.0 1 03/11/2023 02:08 WG2019718
2,6-Dinitrotoluene ND 10.0 1 03/11/2023 02:08 WG2019718
Fluoranthene ND 1.00 1 03/11/2023 02:08 WG2019718
Fluorene ND 1.00 1 03/11/2023 02:08 WG2019718
Hexachlorobenzene ND 1.00 1 03/11/2023 02:08 WG2019718
Hexachloro-1,3-butadiene ND 10.0 1 03/11/2023 02:08 WG2019718
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 23 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 23 of 78
SAMPLE RESULTS - 06
L1592757
MW-8
Collected date/time: 03/06/23 09:45
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Hexachlorocyclopentadiene ND 10.0 1 03/11/2023 02:08 WG2019718
Hexachloroethane ND 10.0 1 03/11/2023 02:08 WG2019718
Indeno(1,2,3-cd)pyrene ND 1.00 1 03/11/2023 02:08 WG2019718
Isophorone ND 10.0 1 03/11/2023 02:08 WG2019718
Naphthalene ND 1.00 1 03/11/2023 02:08 WG2019718
Nitrobenzene ND 10.0 1 03/11/2023 02:08 WG2019718
n-Nitrosodimethylamine ND 10.0 1 03/11/2023 02:08 WG2019718
n-Nitrosodiphenylamine ND 10.0 1 03/11/2023 02:08 WG2019718
n-Nitrosodi-n-propylamine ND 10.0 1 03/11/2023 02:08 WG2019718
Phenanthrene ND 1.00 1 03/11/2023 02:08 WG2019718
Benzylbutyl phthalate ND 3.00 1 03/11/2023 02:08 WG2019718
Bis(2-ethylhexyl)phthalate ND 3.00 1 03/11/2023 02:08 WG2019718
Di-n-butyl phthalate ND 3.00 1 03/11/2023 02:08 WG2019718
Diethyl phthalate ND 3.00 1 03/11/2023 02:08 WG2019718
Dimethyl phthalate ND 3.00 1 03/11/2023 02:08 WG2019718
Di-n-octyl phthalate ND 3.00 1 03/11/2023 02:08 WG2019718
Pyrene ND 1.00 1 03/11/2023 02:08 WG2019718
1,2,4-Trichlorobenzene ND 10.0 1 03/11/2023 02:08 WG2019718
4-Chloro-3-methylphenol ND 10.0 1 03/11/2023 02:08 WG2019718
2-Chlorophenol ND 10.0 1 03/11/2023 02:08 WG2019718
2,4-Dichlorophenol ND 10.0 1 03/11/2023 02:08 WG2019718
2,4-Dimethylphenol ND 10.0 1 03/11/2023 02:08 WG2019718
4,6-Dinitro-2-methylphenol ND 10.0 1 03/11/2023 02:08 WG2019718
2,4-Dinitrophenol ND 10.0 1 03/11/2023 02:08 WG2019718
2-Nitrophenol ND 10.0 1 03/11/2023 02:08 WG2019718
4-Nitrophenol ND 10.0 1 03/11/2023 02:08 WG2019718
Pentachlorophenol ND 10.0 1 03/11/2023 02:08 WG2019718
Phenol ND 10.0 1 03/11/2023 02:08 WG2019718
2,4,6-Trichlorophenol ND 10.0 1 03/11/2023 02:08 WG2019718
(S) Nitrobenzene-d5 73.1 15.0-314 03/11/2023 02:08 WG2019718
(S) 2-Fluorobiphenyl 61.6 22.0-127 03/11/2023 02:08 WG2019718
(S) p-Terphenyl-d14 72.4 29.0-141 03/11/2023 02:08 WG2019718
(S) Phenol-d5 15.4 8.00-424 03/11/2023 02:08 WG2019718
(S) 2-Fluorophenol 20.3 10.0-120 03/11/2023 02:08 WG2019718
(S) 2,4,6-Tribromophenol 58.8 10.0-153 03/11/2023 02:08 WG2019718
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 24 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 24 of 78
SAMPLE RESULTS - 07
L1592757
MW-9
Collected date/time: 03/06/23 12:25
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene ND 1.00 1 03/09/2023 16:53 WG2020042
Bromobenzene ND 1.00 1 03/09/2023 16:53 WG2020042
Bromodichloromethane ND 1.00 1 03/09/2023 16:53 WG2020042
Bromochloromethane ND 1.00 1 03/09/2023 16:53 WG2020042
Bromoform ND 1.00 1 03/09/2023 16:53 WG2020042
Bromomethane ND 5.00 1 03/09/2023 16:53 WG2020042
n-Butylbenzene ND 1.00 1 03/09/2023 16:53 WG2020042
sec-Butylbenzene ND 1.00 1 03/09/2023 16:53 WG2020042
tert-Butylbenzene ND 1.00 1 03/09/2023 16:53 WG2020042
Carbon tetrachloride ND 1.00 1 03/09/2023 16:53 WG2020042
Chlorobenzene ND 1.00 1 03/09/2023 16:53 WG2020042
Chlorodibromomethane ND 1.00 1 03/09/2023 16:53 WG2020042
Chloroethane ND 5.00 1 03/09/2023 16:53 WG2020042
Chloroform ND 5.00 1 03/09/2023 16:53 WG2020042
Chloromethane ND 2.50 1 03/09/2023 16:53 WG2020042
2-Chlorotoluene ND 1.00 1 03/09/2023 16:53 WG2020042
4-Chlorotoluene ND 1.00 1 03/09/2023 16:53 WG2020042
1,2-Dibromo-3-Chloropropane ND 5.00 1 03/09/2023 16:53 WG2020042
1,2-Dibromoethane ND 1.00 1 03/09/2023 16:53 WG2020042
Dibromomethane ND 1.00 1 03/09/2023 16:53 WG2020042
1,2-Dichlorobenzene ND 1.00 1 03/09/2023 16:53 WG2020042
1,3-Dichlorobenzene ND 1.00 1 03/09/2023 16:53 WG2020042
1,4-Dichlorobenzene ND 1.00 1 03/09/2023 16:53 WG2020042
Dichlorodifluoromethane ND 5.00 1 03/09/2023 16:53 WG2020042
1,1-Dichloroethane ND 1.00 1 03/09/2023 16:53 WG2020042
1,2-Dichloroethane ND 1.00 1 03/09/2023 16:53 WG2020042
1,1-Dichloroethene ND 1.00 1 03/09/2023 16:53 WG2020042
cis-1,2-Dichloroethene ND 1.00 1 03/09/2023 16:53 WG2020042
trans-1,2-Dichloroethene ND 1.00 1 03/09/2023 16:53 WG2020042
1,2-Dichloropropane ND 1.00 1 03/09/2023 16:53 WG2020042
1,1-Dichloropropene ND 1.00 1 03/09/2023 16:53 WG2020042
1,3-Dichloropropane ND 1.00 1 03/09/2023 16:53 WG2020042
cis-1,3-Dichloropropene ND 1.00 1 03/09/2023 16:53 WG2020042
trans-1,3-Dichloropropene ND 1.00 1 03/09/2023 16:53 WG2020042
2,2-Dichloropropane ND 1.00 1 03/09/2023 16:53 WG2020042
Di-isopropyl ether ND 1.00 1 03/09/2023 16:53 WG2020042
Ethylbenzene ND 1.00 1 03/09/2023 16:53 WG2020042
Hexachloro-1,3-butadiene ND 1.00 1 03/09/2023 16:53 WG2020042
Isopropylbenzene ND 1.00 1 03/09/2023 16:53 WG2020042
Methylene Chloride ND 5.00 1 03/09/2023 16:53 WG2020042
Methyl tert-butyl ether ND 1.00 1 03/09/2023 16:53 WG2020042
Naphthalene ND 5.00 1 03/09/2023 16:53 WG2020042
n-Propylbenzene ND 1.00 1 03/09/2023 16:53 WG2020042
Styrene ND 1.00 1 03/09/2023 16:53 WG2020042
1,1,1,2-Tetrachloroethane ND 1.00 1 03/09/2023 16:53 WG2020042
1,1,2,2-Tetrachloroethane ND 1.00 1 03/09/2023 16:53 WG2020042
Tetrachloroethene ND 1.00 1 03/09/2023 16:53 WG2020042
Toluene ND 1.00 1 03/09/2023 16:53 WG2020042
1,2,3-Trichlorobenzene ND 1.00 1 03/09/2023 16:53 WG2020042
1,2,4-Trichlorobenzene ND 1.00 1 03/09/2023 16:53 WG2020042
1,1,1-Trichloroethane ND 1.00 1 03/09/2023 16:53 WG2020042
1,1,2-Trichloroethane ND 1.00 1 03/09/2023 16:53 WG2020042
Trichloroethene ND 1.00 1 03/09/2023 16:53 WG2020042
Trichlorofluoromethane ND 5.00 1 03/09/2023 16:53 WG2020042
1,2,3-Trichloropropane ND 2.50 1 03/09/2023 16:53 WG2020042
1,2,4-Trimethylbenzene ND 1.00 1 03/09/2023 16:53 WG2020042
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 25 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 25 of 78
SAMPLE RESULTS - 07
L1592757
MW-9
Collected date/time: 03/06/23 12:25
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 03/09/2023 16:53 WG2020042
Vinyl chloride ND 1.00 1 03/09/2023 16:53 WG2020042
o-Xylene ND 1.00 1 03/09/2023 16:53 WG2020042
m&p-Xylenes ND 2.00 1 03/09/2023 16:53 WG2020042
ethanol ND 100 1 03/09/2023 16:53 WG2020042
tert-Amyl Methyl Ether ND 1.00 1 03/09/2023 16:53 WG2020042
Ethyl tert-butyl ether ND 1.00 1 03/09/2023 16:53 WG2020042
tert-Butyl alcohol ND 5.00 1 03/09/2023 16:53 WG2020042
t-Amyl Alcohol ND 50.0 1 03/09/2023 16:53 WG2020042
tert-Butyl formate ND 20.0 1 03/10/2023 17:39 WG2020940
(S) Toluene-d8 97.8 80.0-120 03/09/2023 16:53 WG2020042
(S) Toluene-d8 102 80.0-120 03/10/2023 17:39 WG2020940
(S) 4-Bromofluorobenzene 91.1 77.0-126 03/09/2023 16:53 WG2020042
(S) 4-Bromofluorobenzene 106 77.0-126 03/10/2023 17:39 WG2020940
(S) 1,2-Dichloroethane-d4 93.3 70.0-130 03/09/2023 16:53 WG2020042
(S) 1,2-Dichloroethane-d4 109 70.0-130 03/10/2023 17:39 WG2020940
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 03/14/2023 19:02 WG2020454
Unadjusted C19-C36 Aliphatics ND 100 1 03/14/2023 19:02 WG2020454
Unadjusted C11-C22 Aromatics ND 100 1 03/14/2023 21:02 WG2020454
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 03/14/2023 19:02 WG2020454
(S) o-Terphenyl 89.2 40.0-140 03/14/2023 21:02 WG2020454
(S) 1-Chloro-octadecane 79.2 40.0-140 03/14/2023 19:02 WG2020454
(S) 2-Fluorobiphenyl 88.7 40.0-140 03/14/2023 21:02 WG2020454
(S) 2-Bromonaphthalene 97.2 40.0-140 03/14/2023 21:02 WG2020454
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 03/11/2023 02:29 WG2019718
Acenaphthylene ND 1.00 1 03/11/2023 02:29 WG2019718
Anthracene ND 1.00 1 03/11/2023 02:29 WG2019718
Benzo(a)anthracene ND 1.00 1 03/11/2023 02:29 WG2019718
Benzo(b)fluoranthene ND 1.00 1 03/11/2023 02:29 WG2019718
Benzo(k)fluoranthene ND 1.00 1 03/11/2023 02:29 WG2019718
Benzo(g,h,i)perylene ND 1.00 1 03/11/2023 02:29 WG2019718
Benzo(a)pyrene ND 1.00 1 03/11/2023 02:29 WG2019718
Bis(2-chlorethoxy)methane ND 10.0 1 03/11/2023 02:29 WG2019718
Bis(2-chloroethyl)ether ND 10.0 1 03/11/2023 02:29 WG2019718
2,2-Oxybis(1-Chloropropane)ND 10.0 1 03/11/2023 02:29 WG2019718
4-Bromophenyl-phenylether ND 10.0 1 03/11/2023 02:29 WG2019718
2-Chloronaphthalene ND 1.00 1 03/11/2023 02:29 WG2019718
4-Chlorophenyl-phenylether ND 10.0 1 03/11/2023 02:29 WG2019718
Chrysene ND 1.00 1 03/11/2023 02:29 WG2019718
Dibenz(a,h)anthracene ND 1.00 1 03/11/2023 02:29 WG2019718
3,3-Dichlorobenzidine ND 10.0 1 03/11/2023 02:29 WG2019718
2,4-Dinitrotoluene ND 10.0 1 03/11/2023 02:29 WG2019718
2,6-Dinitrotoluene ND 10.0 1 03/11/2023 02:29 WG2019718
Fluoranthene ND 1.00 1 03/11/2023 02:29 WG2019718
Fluorene ND 1.00 1 03/11/2023 02:29 WG2019718
Hexachlorobenzene ND 1.00 1 03/11/2023 02:29 WG2019718
Hexachloro-1,3-butadiene ND 10.0 1 03/11/2023 02:29 WG2019718
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 26 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 26 of 78
SAMPLE RESULTS - 07
L1592757
MW-9
Collected date/time: 03/06/23 12:25
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Hexachlorocyclopentadiene ND 10.0 1 03/11/2023 02:29 WG2019718
Hexachloroethane ND 10.0 1 03/11/2023 02:29 WG2019718
Indeno(1,2,3-cd)pyrene ND 1.00 1 03/11/2023 02:29 WG2019718
Isophorone ND 10.0 1 03/11/2023 02:29 WG2019718
Naphthalene ND 1.00 1 03/11/2023 02:29 WG2019718
Nitrobenzene ND 10.0 1 03/11/2023 02:29 WG2019718
n-Nitrosodimethylamine ND 10.0 1 03/11/2023 02:29 WG2019718
n-Nitrosodiphenylamine ND 10.0 1 03/11/2023 02:29 WG2019718
n-Nitrosodi-n-propylamine ND 10.0 1 03/11/2023 02:29 WG2019718
Phenanthrene ND 1.00 1 03/11/2023 02:29 WG2019718
Benzylbutyl phthalate ND 3.00 1 03/11/2023 02:29 WG2019718
Bis(2-ethylhexyl)phthalate ND 3.00 1 03/11/2023 02:29 WG2019718
Di-n-butyl phthalate ND 3.00 1 03/11/2023 02:29 WG2019718
Diethyl phthalate ND 3.00 1 03/11/2023 02:29 WG2019718
Dimethyl phthalate ND 3.00 1 03/11/2023 02:29 WG2019718
Di-n-octyl phthalate ND 3.00 1 03/11/2023 02:29 WG2019718
Pyrene ND 1.00 1 03/11/2023 02:29 WG2019718
1,2,4-Trichlorobenzene ND 10.0 1 03/11/2023 02:29 WG2019718
4-Chloro-3-methylphenol ND 10.0 1 03/11/2023 02:29 WG2019718
2-Chlorophenol ND 10.0 1 03/11/2023 02:29 WG2019718
2,4-Dichlorophenol ND 10.0 1 03/11/2023 02:29 WG2019718
2,4-Dimethylphenol ND 10.0 1 03/11/2023 02:29 WG2019718
4,6-Dinitro-2-methylphenol ND 10.0 1 03/11/2023 02:29 WG2019718
2,4-Dinitrophenol ND 10.0 1 03/11/2023 02:29 WG2019718
2-Nitrophenol ND 10.0 1 03/11/2023 02:29 WG2019718
4-Nitrophenol ND 10.0 1 03/11/2023 02:29 WG2019718
Pentachlorophenol ND 10.0 1 03/11/2023 02:29 WG2019718
Phenol ND 10.0 1 03/11/2023 02:29 WG2019718
2,4,6-Trichlorophenol ND 10.0 1 03/11/2023 02:29 WG2019718
(S) Nitrobenzene-d5 79.3 15.0-314 03/11/2023 02:29 WG2019718
(S) 2-Fluorobiphenyl 64.3 22.0-127 03/11/2023 02:29 WG2019718
(S) p-Terphenyl-d14 62.5 29.0-141 03/11/2023 02:29 WG2019718
(S) Phenol-d5 16.9 8.00-424 03/11/2023 02:29 WG2019718
(S) 2-Fluorophenol 23.0 10.0-120 03/11/2023 02:29 WG2019718
(S) 2,4,6-Tribromophenol 41.3 10.0-153 03/11/2023 02:29 WG2019718
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 27 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 27 of 78
SAMPLE RESULTS - 08
L1592757
MW-10
Collected date/time: 03/06/23 15:00
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene 8.33 1.00 1 03/09/2023 17:14 WG2020042
Bromobenzene ND 1.00 1 03/09/2023 17:14 WG2020042
Bromodichloromethane ND 1.00 1 03/09/2023 17:14 WG2020042
Bromochloromethane ND 1.00 1 03/09/2023 17:14 WG2020042
Bromoform ND 1.00 1 03/09/2023 17:14 WG2020042
Bromomethane ND 5.00 1 03/09/2023 17:14 WG2020042
n-Butylbenzene ND 1.00 1 03/09/2023 17:14 WG2020042
sec-Butylbenzene ND 1.00 1 03/09/2023 17:14 WG2020042
tert-Butylbenzene ND 1.00 1 03/09/2023 17:14 WG2020042
Carbon tetrachloride ND 1.00 1 03/09/2023 17:14 WG2020042
Chlorobenzene ND 1.00 1 03/09/2023 17:14 WG2020042
Chlorodibromomethane ND 1.00 1 03/09/2023 17:14 WG2020042
Chloroethane ND 5.00 1 03/09/2023 17:14 WG2020042
Chloroform ND 5.00 1 03/09/2023 17:14 WG2020042
Chloromethane ND 2.50 1 03/09/2023 17:14 WG2020042
2-Chlorotoluene ND 1.00 1 03/09/2023 17:14 WG2020042
4-Chlorotoluene ND 1.00 1 03/09/2023 17:14 WG2020042
1,2-Dibromo-3-Chloropropane ND 5.00 1 03/09/2023 17:14 WG2020042
1,2-Dibromoethane ND 1.00 1 03/09/2023 17:14 WG2020042
Dibromomethane ND 1.00 1 03/09/2023 17:14 WG2020042
1,2-Dichlorobenzene ND 1.00 1 03/09/2023 17:14 WG2020042
1,3-Dichlorobenzene ND 1.00 1 03/09/2023 17:14 WG2020042
1,4-Dichlorobenzene ND 1.00 1 03/09/2023 17:14 WG2020042
Dichlorodifluoromethane ND 5.00 1 03/09/2023 17:14 WG2020042
1,1-Dichloroethane ND 1.00 1 03/09/2023 17:14 WG2020042
1,2-Dichloroethane ND 1.00 1 03/09/2023 17:14 WG2020042
1,1-Dichloroethene ND 1.00 1 03/09/2023 17:14 WG2020042
cis-1,2-Dichloroethene ND 1.00 1 03/09/2023 17:14 WG2020042
trans-1,2-Dichloroethene ND 1.00 1 03/09/2023 17:14 WG2020042
1,2-Dichloropropane ND 1.00 1 03/09/2023 17:14 WG2020042
1,1-Dichloropropene ND 1.00 1 03/09/2023 17:14 WG2020042
1,3-Dichloropropane ND 1.00 1 03/09/2023 17:14 WG2020042
cis-1,3-Dichloropropene ND 1.00 1 03/09/2023 17:14 WG2020042
trans-1,3-Dichloropropene ND 1.00 1 03/09/2023 17:14 WG2020042
2,2-Dichloropropane ND 1.00 1 03/09/2023 17:14 WG2020042
Di-isopropyl ether ND 1.00 1 03/09/2023 17:14 WG2020042
Ethylbenzene ND 1.00 1 03/09/2023 17:14 WG2020042
Hexachloro-1,3-butadiene ND 1.00 1 03/09/2023 17:14 WG2020042
Isopropylbenzene ND 1.00 1 03/09/2023 17:14 WG2020042
Methylene Chloride ND 5.00 1 03/09/2023 17:14 WG2020042
Methyl tert-butyl ether ND 1.00 1 03/09/2023 17:14 WG2020042
Naphthalene ND 5.00 1 03/09/2023 17:14 WG2020042
n-Propylbenzene ND 1.00 1 03/09/2023 17:14 WG2020042
Styrene ND 1.00 1 03/09/2023 17:14 WG2020042
1,1,1,2-Tetrachloroethane ND 1.00 1 03/09/2023 17:14 WG2020042
1,1,2,2-Tetrachloroethane ND 1.00 1 03/09/2023 17:14 WG2020042
Tetrachloroethene ND 1.00 1 03/09/2023 17:14 WG2020042
Toluene ND 1.00 1 03/09/2023 17:14 WG2020042
1,2,3-Trichlorobenzene ND 1.00 1 03/09/2023 17:14 WG2020042
1,2,4-Trichlorobenzene ND 1.00 1 03/09/2023 17:14 WG2020042
1,1,1-Trichloroethane ND 1.00 1 03/09/2023 17:14 WG2020042
1,1,2-Trichloroethane ND 1.00 1 03/09/2023 17:14 WG2020042
Trichloroethene ND 1.00 1 03/09/2023 17:14 WG2020042
Trichlorofluoromethane ND 5.00 1 03/09/2023 17:14 WG2020042
1,2,3-Trichloropropane ND 2.50 1 03/09/2023 17:14 WG2020042
1,2,4-Trimethylbenzene ND 1.00 1 03/09/2023 17:14 WG2020042
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 28 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 28 of 78
SAMPLE RESULTS - 08
L1592757
MW-10
Collected date/time: 03/06/23 15:00
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 03/09/2023 17:14 WG2020042
Vinyl chloride ND 1.00 1 03/09/2023 17:14 WG2020042
o-Xylene ND 1.00 1 03/09/2023 17:14 WG2020042
m&p-Xylenes ND 2.00 1 03/09/2023 17:14 WG2020042
ethanol ND 100 1 03/09/2023 17:14 WG2020042
tert-Amyl Methyl Ether ND 1.00 1 03/09/2023 17:14 WG2020042
Ethyl tert-butyl ether ND 1.00 1 03/09/2023 17:14 WG2020042
tert-Butyl alcohol ND 5.00 1 03/09/2023 17:14 WG2020042
t-Amyl Alcohol ND 50.0 1 03/09/2023 17:14 WG2020042
tert-Butyl formate ND 20.0 1 03/10/2023 18:01 WG2020940
(S) Toluene-d8 97.3 80.0-120 03/09/2023 17:14 WG2020042
(S) Toluene-d8 102 80.0-120 03/10/2023 18:01 WG2020940
(S) 4-Bromofluorobenzene 93.3 77.0-126 03/09/2023 17:14 WG2020042
(S) 4-Bromofluorobenzene 108 77.0-126 03/10/2023 18:01 WG2020940
(S) 1,2-Dichloroethane-d4 92.8 70.0-130 03/09/2023 17:14 WG2020042
(S) 1,2-Dichloroethane-d4 110 70.0-130 03/10/2023 18:01 WG2020940
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 29 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 29 of 78
SAMPLE RESULTS - 09
L1592757
MW-12
Collected date/time: 03/06/23 12:20
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene ND 1.00 1 03/09/2023 17:36 WG2020042
Bromobenzene ND 1.00 1 03/09/2023 17:36 WG2020042
Bromodichloromethane ND 1.00 1 03/09/2023 17:36 WG2020042
Bromochloromethane ND 1.00 1 03/09/2023 17:36 WG2020042
Bromoform ND 1.00 1 03/09/2023 17:36 WG2020042
Bromomethane ND 5.00 1 03/09/2023 17:36 WG2020042
n-Butylbenzene ND 1.00 1 03/09/2023 17:36 WG2020042
sec-Butylbenzene ND 1.00 1 03/09/2023 17:36 WG2020042
tert-Butylbenzene ND 1.00 1 03/09/2023 17:36 WG2020042
Carbon tetrachloride ND 1.00 1 03/09/2023 17:36 WG2020042
Chlorobenzene ND 1.00 1 03/09/2023 17:36 WG2020042
Chlorodibromomethane ND 1.00 1 03/09/2023 17:36 WG2020042
Chloroethane ND 5.00 1 03/09/2023 17:36 WG2020042
Chloroform ND 5.00 1 03/09/2023 17:36 WG2020042
Chloromethane ND 2.50 1 03/09/2023 17:36 WG2020042
2-Chlorotoluene ND 1.00 1 03/09/2023 17:36 WG2020042
4-Chlorotoluene ND 1.00 1 03/09/2023 17:36 WG2020042
1,2-Dibromo-3-Chloropropane ND 5.00 1 03/09/2023 17:36 WG2020042
1,2-Dibromoethane ND 1.00 1 03/09/2023 17:36 WG2020042
Dibromomethane ND 1.00 1 03/09/2023 17:36 WG2020042
1,2-Dichlorobenzene ND 1.00 1 03/09/2023 17:36 WG2020042
1,3-Dichlorobenzene ND 1.00 1 03/09/2023 17:36 WG2020042
1,4-Dichlorobenzene ND 1.00 1 03/09/2023 17:36 WG2020042
Dichlorodifluoromethane ND 5.00 1 03/09/2023 17:36 WG2020042
1,1-Dichloroethane ND 1.00 1 03/09/2023 17:36 WG2020042
1,2-Dichloroethane ND 1.00 1 03/09/2023 17:36 WG2020042
1,1-Dichloroethene ND 1.00 1 03/09/2023 17:36 WG2020042
cis-1,2-Dichloroethene ND 1.00 1 03/09/2023 17:36 WG2020042
trans-1,2-Dichloroethene ND 1.00 1 03/09/2023 17:36 WG2020042
1,2-Dichloropropane ND 1.00 1 03/09/2023 17:36 WG2020042
1,1-Dichloropropene ND 1.00 1 03/09/2023 17:36 WG2020042
1,3-Dichloropropane ND 1.00 1 03/09/2023 17:36 WG2020042
cis-1,3-Dichloropropene ND 1.00 1 03/09/2023 17:36 WG2020042
trans-1,3-Dichloropropene ND 1.00 1 03/09/2023 17:36 WG2020042
2,2-Dichloropropane ND 1.00 1 03/09/2023 17:36 WG2020042
Di-isopropyl ether ND 1.00 1 03/09/2023 17:36 WG2020042
Ethylbenzene ND 1.00 1 03/09/2023 17:36 WG2020042
Hexachloro-1,3-butadiene ND 1.00 1 03/09/2023 17:36 WG2020042
Isopropylbenzene ND 1.00 1 03/09/2023 17:36 WG2020042
Methylene Chloride ND 5.00 1 03/09/2023 17:36 WG2020042
Methyl tert-butyl ether ND 1.00 1 03/09/2023 17:36 WG2020042
Naphthalene ND 5.00 1 03/09/2023 17:36 WG2020042
n-Propylbenzene ND 1.00 1 03/09/2023 17:36 WG2020042
Styrene ND 1.00 1 03/09/2023 17:36 WG2020042
1,1,1,2-Tetrachloroethane ND 1.00 1 03/09/2023 17:36 WG2020042
1,1,2,2-Tetrachloroethane ND 1.00 1 03/09/2023 17:36 WG2020042
Tetrachloroethene ND 1.00 1 03/09/2023 17:36 WG2020042
Toluene ND 1.00 1 03/09/2023 17:36 WG2020042
1,2,3-Trichlorobenzene ND 1.00 1 03/09/2023 17:36 WG2020042
1,2,4-Trichlorobenzene ND 1.00 1 03/09/2023 17:36 WG2020042
1,1,1-Trichloroethane ND 1.00 1 03/09/2023 17:36 WG2020042
1,1,2-Trichloroethane ND 1.00 1 03/09/2023 17:36 WG2020042
Trichloroethene ND 1.00 1 03/09/2023 17:36 WG2020042
Trichlorofluoromethane ND 5.00 1 03/09/2023 17:36 WG2020042
1,2,3-Trichloropropane ND 2.50 1 03/09/2023 17:36 WG2020042
1,2,4-Trimethylbenzene ND 1.00 1 03/09/2023 17:36 WG2020042
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 30 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 30 of 78
SAMPLE RESULTS - 09
L1592757
MW-12
Collected date/time: 03/06/23 12:20
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 03/09/2023 17:36 WG2020042
Vinyl chloride ND 1.00 1 03/09/2023 17:36 WG2020042
o-Xylene ND 1.00 1 03/09/2023 17:36 WG2020042
m&p-Xylenes ND 2.00 1 03/09/2023 17:36 WG2020042
ethanol ND 100 1 03/09/2023 17:36 WG2020042
tert-Amyl Methyl Ether ND 1.00 1 03/09/2023 17:36 WG2020042
Ethyl tert-butyl ether ND 1.00 1 03/09/2023 17:36 WG2020042
tert-Butyl alcohol ND 5.00 1 03/09/2023 17:36 WG2020042
t-Amyl Alcohol ND 50.0 1 03/09/2023 17:36 WG2020042
tert-Butyl formate ND 20.0 1 03/10/2023 18:23 WG2020940
(S) Toluene-d8 99.4 80.0-120 03/09/2023 17:36 WG2020042
(S) Toluene-d8 103 80.0-120 03/10/2023 18:23 WG2020940
(S) 4-Bromofluorobenzene 89.7 77.0-126 03/09/2023 17:36 WG2020042
(S) 4-Bromofluorobenzene 107 77.0-126 03/10/2023 18:23 WG2020940
(S) 1,2-Dichloroethane-d4 91.6 70.0-130 03/09/2023 17:36 WG2020042
(S) 1,2-Dichloroethane-d4 113 70.0-130 03/10/2023 18:23 WG2020940
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 03/14/2023 19:26 WG2020454
Unadjusted C19-C36 Aliphatics ND 100 1 03/14/2023 19:26 WG2020454
Unadjusted C11-C22 Aromatics ND 100 1 03/14/2023 20:38 WG2020454
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 03/14/2023 19:26 WG2020454
(S) o-Terphenyl 93.7 40.0-140 03/14/2023 20:38 WG2020454
(S) 1-Chloro-octadecane 93.0 40.0-140 03/14/2023 19:26 WG2020454
(S) 2-Fluorobiphenyl 93.4 40.0-140 03/14/2023 20:38 WG2020454
(S) 2-Bromonaphthalene 102 40.0-140 03/14/2023 20:38 WG2020454
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 03/11/2023 02:50 WG2019718
Acenaphthylene ND 1.00 1 03/11/2023 02:50 WG2019718
Anthracene ND 1.00 1 03/11/2023 02:50 WG2019718
Benzo(a)anthracene ND 1.00 1 03/11/2023 02:50 WG2019718
Benzo(b)fluoranthene ND 1.00 1 03/11/2023 02:50 WG2019718
Benzo(k)fluoranthene ND 1.00 1 03/11/2023 02:50 WG2019718
Benzo(g,h,i)perylene ND 1.00 1 03/11/2023 02:50 WG2019718
Benzo(a)pyrene ND 1.00 1 03/11/2023 02:50 WG2019718
Bis(2-chlorethoxy)methane ND 10.0 1 03/11/2023 02:50 WG2019718
Bis(2-chloroethyl)ether ND 10.0 1 03/11/2023 02:50 WG2019718
2,2-Oxybis(1-Chloropropane)ND 10.0 1 03/11/2023 02:50 WG2019718
4-Bromophenyl-phenylether ND 10.0 1 03/11/2023 02:50 WG2019718
2-Chloronaphthalene ND 1.00 1 03/11/2023 02:50 WG2019718
4-Chlorophenyl-phenylether ND 10.0 1 03/11/2023 02:50 WG2019718
Chrysene ND 1.00 1 03/11/2023 02:50 WG2019718
Dibenz(a,h)anthracene ND 1.00 1 03/11/2023 02:50 WG2019718
3,3-Dichlorobenzidine ND 10.0 1 03/11/2023 02:50 WG2019718
2,4-Dinitrotoluene ND 10.0 1 03/11/2023 02:50 WG2019718
2,6-Dinitrotoluene ND 10.0 1 03/11/2023 02:50 WG2019718
Fluoranthene ND 1.00 1 03/11/2023 02:50 WG2019718
Fluorene ND 1.00 1 03/11/2023 02:50 WG2019718
Hexachlorobenzene ND 1.00 1 03/11/2023 02:50 WG2019718
Hexachloro-1,3-butadiene ND 10.0 1 03/11/2023 02:50 WG2019718
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 31 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 31 of 78
SAMPLE RESULTS - 09
L1592757
MW-12
Collected date/time: 03/06/23 12:20
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Hexachlorocyclopentadiene ND 10.0 1 03/11/2023 02:50 WG2019718
Hexachloroethane ND 10.0 1 03/11/2023 02:50 WG2019718
Indeno(1,2,3-cd)pyrene ND 1.00 1 03/11/2023 02:50 WG2019718
Isophorone ND 10.0 1 03/11/2023 02:50 WG2019718
Naphthalene ND 1.00 1 03/11/2023 02:50 WG2019718
Nitrobenzene ND 10.0 1 03/11/2023 02:50 WG2019718
n-Nitrosodimethylamine ND 10.0 1 03/11/2023 02:50 WG2019718
n-Nitrosodiphenylamine ND 10.0 1 03/11/2023 02:50 WG2019718
n-Nitrosodi-n-propylamine ND 10.0 1 03/11/2023 02:50 WG2019718
Phenanthrene ND 1.00 1 03/11/2023 02:50 WG2019718
Benzylbutyl phthalate ND 3.00 1 03/11/2023 02:50 WG2019718
Bis(2-ethylhexyl)phthalate ND 3.00 1 03/11/2023 02:50 WG2019718
Di-n-butyl phthalate ND 3.00 1 03/11/2023 02:50 WG2019718
Diethyl phthalate ND 3.00 1 03/11/2023 02:50 WG2019718
Dimethyl phthalate ND 3.00 1 03/11/2023 02:50 WG2019718
Di-n-octyl phthalate ND 3.00 1 03/11/2023 02:50 WG2019718
Pyrene ND 1.00 1 03/11/2023 02:50 WG2019718
1,2,4-Trichlorobenzene ND 10.0 1 03/11/2023 02:50 WG2019718
4-Chloro-3-methylphenol ND 10.0 1 03/11/2023 02:50 WG2019718
2-Chlorophenol ND 10.0 1 03/11/2023 02:50 WG2019718
2,4-Dichlorophenol ND 10.0 1 03/11/2023 02:50 WG2019718
2,4-Dimethylphenol ND 10.0 1 03/11/2023 02:50 WG2019718
4,6-Dinitro-2-methylphenol ND 10.0 1 03/11/2023 02:50 WG2019718
2,4-Dinitrophenol ND 10.0 1 03/11/2023 02:50 WG2019718
2-Nitrophenol ND 10.0 1 03/11/2023 02:50 WG2019718
4-Nitrophenol ND 10.0 1 03/11/2023 02:50 WG2019718
Pentachlorophenol ND 10.0 1 03/11/2023 02:50 WG2019718
Phenol ND 10.0 1 03/11/2023 02:50 WG2019718
2,4,6-Trichlorophenol ND 10.0 1 03/11/2023 02:50 WG2019718
(S) Nitrobenzene-d5 72.3 15.0-314 03/11/2023 02:50 WG2019718
(S) 2-Fluorobiphenyl 60.0 22.0-127 03/11/2023 02:50 WG2019718
(S) p-Terphenyl-d14 76.4 29.0-141 03/11/2023 02:50 WG2019718
(S) Phenol-d5 19.0 8.00-424 03/11/2023 02:50 WG2019718
(S) 2-Fluorophenol 28.0 10.0-120 03/11/2023 02:50 WG2019718
(S) 2,4,6-Tribromophenol 59.5 10.0-153 03/11/2023 02:50 WG2019718
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 32 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 32 of 78
SAMPLE RESULTS - 10
L1592757
MW-1D
Collected date/time: 03/07/23 09:10
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene ND 1.00 1 03/09/2023 17:58 WG2020042
Bromobenzene ND 1.00 1 03/09/2023 17:58 WG2020042
Bromodichloromethane ND 1.00 1 03/09/2023 17:58 WG2020042
Bromochloromethane ND 1.00 1 03/09/2023 17:58 WG2020042
Bromoform ND 1.00 1 03/09/2023 17:58 WG2020042
Bromomethane ND 5.00 1 03/09/2023 17:58 WG2020042
n-Butylbenzene ND 1.00 1 03/09/2023 17:58 WG2020042
sec-Butylbenzene ND 1.00 1 03/09/2023 17:58 WG2020042
tert-Butylbenzene ND 1.00 1 03/09/2023 17:58 WG2020042
Carbon tetrachloride ND 1.00 1 03/09/2023 17:58 WG2020042
Chlorobenzene ND 1.00 1 03/09/2023 17:58 WG2020042
Chlorodibromomethane ND 1.00 1 03/09/2023 17:58 WG2020042
Chloroethane ND 5.00 1 03/09/2023 17:58 WG2020042
Chloroform ND 5.00 1 03/09/2023 17:58 WG2020042
Chloromethane ND 2.50 1 03/09/2023 17:58 WG2020042
2-Chlorotoluene ND 1.00 1 03/09/2023 17:58 WG2020042
4-Chlorotoluene ND 1.00 1 03/09/2023 17:58 WG2020042
1,2-Dibromo-3-Chloropropane ND 5.00 1 03/09/2023 17:58 WG2020042
1,2-Dibromoethane ND 1.00 1 03/09/2023 17:58 WG2020042
Dibromomethane ND 1.00 1 03/09/2023 17:58 WG2020042
1,2-Dichlorobenzene ND 1.00 1 03/09/2023 17:58 WG2020042
1,3-Dichlorobenzene ND 1.00 1 03/09/2023 17:58 WG2020042
1,4-Dichlorobenzene ND 1.00 1 03/09/2023 17:58 WG2020042
Dichlorodifluoromethane ND 5.00 1 03/09/2023 17:58 WG2020042
1,1-Dichloroethane ND 1.00 1 03/09/2023 17:58 WG2020042
1,2-Dichloroethane ND 1.00 1 03/09/2023 17:58 WG2020042
1,1-Dichloroethene ND 1.00 1 03/09/2023 17:58 WG2020042
cis-1,2-Dichloroethene ND 1.00 1 03/09/2023 17:58 WG2020042
trans-1,2-Dichloroethene ND 1.00 1 03/09/2023 17:58 WG2020042
1,2-Dichloropropane ND 1.00 1 03/09/2023 17:58 WG2020042
1,1-Dichloropropene ND 1.00 1 03/09/2023 17:58 WG2020042
1,3-Dichloropropane ND 1.00 1 03/09/2023 17:58 WG2020042
cis-1,3-Dichloropropene ND 1.00 1 03/09/2023 17:58 WG2020042
trans-1,3-Dichloropropene ND 1.00 1 03/09/2023 17:58 WG2020042
2,2-Dichloropropane ND 1.00 1 03/09/2023 17:58 WG2020042
Di-isopropyl ether ND 1.00 1 03/09/2023 17:58 WG2020042
Ethylbenzene ND 1.00 1 03/09/2023 17:58 WG2020042
Hexachloro-1,3-butadiene ND 1.00 1 03/09/2023 17:58 WG2020042
Isopropylbenzene ND 1.00 1 03/09/2023 17:58 WG2020042
Methylene Chloride ND 5.00 1 03/09/2023 17:58 WG2020042
Methyl tert-butyl ether ND 1.00 1 03/09/2023 17:58 WG2020042
Naphthalene ND 5.00 1 03/09/2023 17:58 WG2020042
n-Propylbenzene ND 1.00 1 03/09/2023 17:58 WG2020042
Styrene ND 1.00 1 03/09/2023 17:58 WG2020042
1,1,1,2-Tetrachloroethane ND 1.00 1 03/09/2023 17:58 WG2020042
1,1,2,2-Tetrachloroethane ND 1.00 1 03/09/2023 17:58 WG2020042
Tetrachloroethene ND 1.00 1 03/09/2023 17:58 WG2020042
Toluene ND 1.00 1 03/09/2023 17:58 WG2020042
1,2,3-Trichlorobenzene ND 1.00 1 03/09/2023 17:58 WG2020042
1,2,4-Trichlorobenzene ND 1.00 1 03/09/2023 17:58 WG2020042
1,1,1-Trichloroethane ND 1.00 1 03/09/2023 17:58 WG2020042
1,1,2-Trichloroethane ND 1.00 1 03/09/2023 17:58 WG2020042
Trichloroethene ND 1.00 1 03/09/2023 17:58 WG2020042
Trichlorofluoromethane ND 5.00 1 03/09/2023 17:58 WG2020042
1,2,3-Trichloropropane ND 2.50 1 03/09/2023 17:58 WG2020042
1,2,4-Trimethylbenzene ND 1.00 1 03/09/2023 17:58 WG2020042
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 33 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 33 of 78
SAMPLE RESULTS - 10
L1592757
MW-1D
Collected date/time: 03/07/23 09:10
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 03/09/2023 17:58 WG2020042
Vinyl chloride ND 1.00 1 03/09/2023 17:58 WG2020042
o-Xylene ND 1.00 1 03/09/2023 17:58 WG2020042
m&p-Xylenes ND 2.00 1 03/09/2023 17:58 WG2020042
ethanol ND 100 1 03/09/2023 17:58 WG2020042
tert-Amyl Methyl Ether ND 1.00 1 03/09/2023 17:58 WG2020042
Ethyl tert-butyl ether ND 1.00 1 03/09/2023 17:58 WG2020042
tert-Butyl alcohol ND 5.00 1 03/09/2023 17:58 WG2020042
t-Amyl Alcohol ND 50.0 1 03/09/2023 17:58 WG2020042
tert-Butyl formate ND 20.0 1 03/10/2023 18:45 WG2020940
(S) Toluene-d8 100 80.0-120 03/09/2023 17:58 WG2020042
(S) Toluene-d8 103 80.0-120 03/10/2023 18:45 WG2020940
(S) 4-Bromofluorobenzene 90.6 77.0-126 03/09/2023 17:58 WG2020042
(S) 4-Bromofluorobenzene 107 77.0-126 03/10/2023 18:45 WG2020940
(S) 1,2-Dichloroethane-d4 94.4 70.0-130 03/09/2023 17:58 WG2020042
(S) 1,2-Dichloroethane-d4 113 70.0-130 03/10/2023 18:45 WG2020940
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 247 100 1 03/14/2023 19:50 WG2020454
Unadjusted C19-C36 Aliphatics ND 100 1 03/14/2023 19:50 WG2020454
Unadjusted C11-C22 Aromatics ND 100 1 03/14/2023 20:14 WG2020454
Unadjusted Total Petroleum
Hydrocarbons 426 100 1 03/14/2023 20:14 WG2020454
(S) o-Terphenyl 81.2 40.0-140 03/14/2023 20:14 WG2020454
(S) 1-Chloro-octadecane 60.0 40.0-140 03/14/2023 19:50 WG2020454
(S) 2-Fluorobiphenyl 89.1 40.0-140 03/14/2023 20:14 WG2020454
(S) 2-Bromonaphthalene 96.2 40.0-140 03/14/2023 20:14 WG2020454
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 03/12/2023 00:29 WG2020599
Acenaphthylene ND 1.00 1 03/12/2023 00:29 WG2020599
Anthracene ND 1.00 1 03/12/2023 00:29 WG2020599
Benzo(a)anthracene ND 1.00 1 03/12/2023 00:29 WG2020599
Benzo(b)fluoranthene ND 1.00 1 03/12/2023 00:29 WG2020599
Benzo(k)fluoranthene ND 1.00 1 03/12/2023 00:29 WG2020599
Benzo(g,h,i)perylene ND 1.00 1 03/12/2023 00:29 WG2020599
Benzo(a)pyrene ND 1.00 1 03/12/2023 00:29 WG2020599
Bis(2-chlorethoxy)methane ND 10.0 1 03/12/2023 00:29 WG2020599
Bis(2-chloroethyl)ether ND 10.0 1 03/12/2023 00:29 WG2020599
2,2-Oxybis(1-Chloropropane)ND 10.0 1 03/12/2023 00:29 WG2020599
4-Bromophenyl-phenylether ND 10.0 1 03/12/2023 00:29 WG2020599
2-Chloronaphthalene ND 1.00 1 03/12/2023 00:29 WG2020599
4-Chlorophenyl-phenylether ND 10.0 1 03/12/2023 00:29 WG2020599
Chrysene ND 1.00 1 03/12/2023 00:29 WG2020599
Dibenz(a,h)anthracene ND 1.00 1 03/12/2023 00:29 WG2020599
3,3-Dichlorobenzidine ND 10.0 1 03/12/2023 00:29 WG2020599
2,4-Dinitrotoluene ND 10.0 1 03/12/2023 00:29 WG2020599
2,6-Dinitrotoluene ND 10.0 1 03/12/2023 00:29 WG2020599
Fluoranthene ND 1.00 1 03/12/2023 00:29 WG2020599
Fluorene ND 1.00 1 03/12/2023 00:29 WG2020599
Hexachlorobenzene ND 1.00 1 03/12/2023 00:29 WG2020599
Hexachloro-1,3-butadiene ND 10.0 1 03/12/2023 00:29 WG2020599
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 34 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 34 of 78
SAMPLE RESULTS - 10
L1592757
MW-1D
Collected date/time: 03/07/23 09:10
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Hexachlorocyclopentadiene ND 10.0 1 03/12/2023 00:29 WG2020599
Hexachloroethane ND 10.0 1 03/12/2023 00:29 WG2020599
Indeno(1,2,3-cd)pyrene ND 1.00 1 03/12/2023 00:29 WG2020599
Isophorone ND 10.0 1 03/12/2023 00:29 WG2020599
Naphthalene ND 1.00 1 03/12/2023 00:29 WG2020599
Nitrobenzene ND 10.0 1 03/12/2023 00:29 WG2020599
n-Nitrosodimethylamine ND 10.0 1 03/12/2023 00:29 WG2020599
n-Nitrosodiphenylamine ND 10.0 1 03/12/2023 00:29 WG2020599
n-Nitrosodi-n-propylamine ND 10.0 1 03/12/2023 00:29 WG2020599
Phenanthrene ND 1.00 1 03/12/2023 00:29 WG2020599
Benzylbutyl phthalate ND 3.00 1 03/12/2023 00:29 WG2020599
Bis(2-ethylhexyl)phthalate ND 3.00 1 03/12/2023 00:29 WG2020599
Di-n-butyl phthalate ND 3.00 1 03/12/2023 00:29 WG2020599
Diethyl phthalate ND 3.00 1 03/12/2023 00:29 WG2020599
Dimethyl phthalate ND 3.00 1 03/12/2023 00:29 WG2020599
Di-n-octyl phthalate ND 3.00 1 03/12/2023 00:29 WG2020599
Pyrene ND 1.00 1 03/12/2023 00:29 WG2020599
1,2,4-Trichlorobenzene ND 10.0 1 03/12/2023 00:29 WG2020599
4-Chloro-3-methylphenol ND 10.0 1 03/12/2023 00:29 WG2020599
2-Chlorophenol ND 10.0 1 03/12/2023 00:29 WG2020599
2,4-Dichlorophenol ND 10.0 1 03/12/2023 00:29 WG2020599
2,4-Dimethylphenol ND 10.0 1 03/12/2023 00:29 WG2020599
4,6-Dinitro-2-methylphenol ND 10.0 1 03/12/2023 00:29 WG2020599
2,4-Dinitrophenol ND 10.0 1 03/12/2023 00:29 WG2020599
2-Nitrophenol ND 10.0 1 03/12/2023 00:29 WG2020599
4-Nitrophenol ND 10.0 1 03/12/2023 00:29 WG2020599
Pentachlorophenol ND 10.0 1 03/12/2023 00:29 WG2020599
Phenol ND 10.0 1 03/12/2023 00:29 WG2020599
2,4,6-Trichlorophenol ND 10.0 1 03/12/2023 00:29 WG2020599
(S) Nitrobenzene-d5 88.1 15.0-314 03/12/2023 00:29 WG2020599
(S) 2-Fluorobiphenyl 68.9 22.0-127 03/12/2023 00:29 WG2020599
(S) p-Terphenyl-d14 65.6 29.0-141 03/12/2023 00:29 WG2020599
(S) Phenol-d5 20.3 8.00-424 03/12/2023 00:29 WG2020599
(S) 2-Fluorophenol 30.0 10.0-120 03/12/2023 00:29 WG2020599
(S) 2,4,6-Tribromophenol 68.7 10.0-153 03/12/2023 00:29 WG2020599
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 35 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 35 of 78
SAMPLE RESULTS - 11
L1592757
MW-4D
Collected date/time: 03/07/23 12:15
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene 2300 50.0 50 03/09/2023 19:46 WG2020042
Bromobenzene ND 50.0 50 03/09/2023 19:46 WG2020042
Bromodichloromethane ND 50.0 50 03/09/2023 19:46 WG2020042
Bromochloromethane ND 50.0 50 03/09/2023 19:46 WG2020042
Bromoform ND 50.0 50 03/09/2023 19:46 WG2020042
Bromomethane ND 250 50 03/09/2023 19:46 WG2020042
n-Butylbenzene ND 50.0 50 03/09/2023 19:46 WG2020042
sec-Butylbenzene ND 50.0 50 03/09/2023 19:46 WG2020042
tert-Butylbenzene ND 50.0 50 03/09/2023 19:46 WG2020042
Carbon tetrachloride ND 50.0 50 03/09/2023 19:46 WG2020042
Chlorobenzene ND 50.0 50 03/09/2023 19:46 WG2020042
Chlorodibromomethane ND 50.0 50 03/09/2023 19:46 WG2020042
Chloroethane ND 250 50 03/09/2023 19:46 WG2020042
Chloroform ND 250 50 03/09/2023 19:46 WG2020042
Chloromethane ND 125 50 03/09/2023 19:46 WG2020042
2-Chlorotoluene ND 50.0 50 03/09/2023 19:46 WG2020042
4-Chlorotoluene ND 50.0 50 03/09/2023 19:46 WG2020042
1,2-Dibromo-3-Chloropropane ND 250 50 03/09/2023 19:46 WG2020042
1,2-Dibromoethane ND 50.0 50 03/09/2023 19:46 WG2020042
Dibromomethane ND 50.0 50 03/09/2023 19:46 WG2020042
1,2-Dichlorobenzene ND 50.0 50 03/09/2023 19:46 WG2020042
1,3-Dichlorobenzene ND 50.0 50 03/09/2023 19:46 WG2020042
1,4-Dichlorobenzene ND 50.0 50 03/09/2023 19:46 WG2020042
Dichlorodifluoromethane ND 250 50 03/09/2023 19:46 WG2020042
1,1-Dichloroethane ND 50.0 50 03/09/2023 19:46 WG2020042
1,2-Dichloroethane ND 50.0 50 03/09/2023 19:46 WG2020042
1,1-Dichloroethene ND 50.0 50 03/09/2023 19:46 WG2020042
cis-1,2-Dichloroethene ND 50.0 50 03/09/2023 19:46 WG2020042
trans-1,2-Dichloroethene ND 50.0 50 03/09/2023 19:46 WG2020042
1,2-Dichloropropane ND 50.0 50 03/09/2023 19:46 WG2020042
1,1-Dichloropropene ND 50.0 50 03/09/2023 19:46 WG2020042
1,3-Dichloropropane ND 50.0 50 03/09/2023 19:46 WG2020042
cis-1,3-Dichloropropene ND 50.0 50 03/09/2023 19:46 WG2020042
trans-1,3-Dichloropropene ND 50.0 50 03/09/2023 19:46 WG2020042
2,2-Dichloropropane ND 50.0 50 03/09/2023 19:46 WG2020042
Di-isopropyl ether ND 50.0 50 03/09/2023 19:46 WG2020042
Ethylbenzene 328 50.0 50 03/09/2023 19:46 WG2020042
Hexachloro-1,3-butadiene ND 50.0 50 03/09/2023 19:46 WG2020042
Isopropylbenzene ND 50.0 50 03/09/2023 19:46 WG2020042
Methylene Chloride ND 250 50 03/09/2023 19:46 WG2020042
Methyl tert-butyl ether ND 50.0 50 03/09/2023 19:46 WG2020042
Naphthalene ND 250 50 03/09/2023 19:46 WG2020042
n-Propylbenzene ND 50.0 50 03/09/2023 19:46 WG2020042
Styrene ND 50.0 50 03/09/2023 19:46 WG2020042
1,1,1,2-Tetrachloroethane ND 50.0 50 03/09/2023 19:46 WG2020042
1,1,2,2-Tetrachloroethane ND 50.0 50 03/09/2023 19:46 WG2020042
Tetrachloroethene ND 50.0 50 03/09/2023 19:46 WG2020042
Toluene 249 50.0 50 03/09/2023 19:46 WG2020042
1,2,3-Trichlorobenzene ND 50.0 50 03/09/2023 19:46 WG2020042
1,2,4-Trichlorobenzene ND 50.0 50 03/09/2023 19:46 WG2020042
1,1,1-Trichloroethane ND 50.0 50 03/09/2023 19:46 WG2020042
1,1,2-Trichloroethane ND 50.0 50 03/09/2023 19:46 WG2020042
Trichloroethene ND 50.0 50 03/09/2023 19:46 WG2020042
Trichlorofluoromethane ND 250 50 03/09/2023 19:46 WG2020042
1,2,3-Trichloropropane ND 125 50 03/09/2023 19:46 WG2020042
1,2,4-Trimethylbenzene 153 50.0 50 03/09/2023 19:46 WG2020042
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 36 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 36 of 78
SAMPLE RESULTS - 11
L1592757
MW-4D
Collected date/time: 03/07/23 12:15
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 50.0 50 03/09/2023 19:46 WG2020042
Vinyl chloride ND 50.0 50 03/09/2023 19:46 WG2020042
o-Xylene 414 50.0 50 03/09/2023 19:46 WG2020042
m&p-Xylenes 612 100 50 03/09/2023 19:46 WG2020042
ethanol ND 5000 50 03/09/2023 19:46 WG2020042
tert-Amyl Methyl Ether ND 50.0 50 03/09/2023 19:46 WG2020042
Ethyl tert-butyl ether ND 50.0 50 03/09/2023 19:46 WG2020042
tert-Butyl alcohol ND 250 50 03/09/2023 19:46 WG2020042
t-Amyl Alcohol ND 2500 50 03/09/2023 19:46 WG2020042
tert-Butyl formate ND 1000 50 03/10/2023 20:12 WG2020940
(S) Toluene-d8 99.7 80.0-120 03/09/2023 19:46 WG2020042
(S) Toluene-d8 101 80.0-120 03/10/2023 20:12 WG2020940
(S) 4-Bromofluorobenzene 92.4 77.0-126 03/09/2023 19:46 WG2020042
(S) 4-Bromofluorobenzene 102 77.0-126 03/10/2023 20:12 WG2020940
(S) 1,2-Dichloroethane-d4 88.6 70.0-130 03/09/2023 19:46 WG2020042
(S) 1,2-Dichloroethane-d4 113 70.0-130 03/10/2023 20:12 WG2020940
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 03/15/2023 01:25 WG2020454
Unadjusted C19-C36 Aliphatics ND 100 1 03/15/2023 01:25 WG2020454
Unadjusted C11-C22 Aromatics ND 100 1 03/15/2023 02:37 WG2020454
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 03/15/2023 01:25 WG2020454
(S) o-Terphenyl 90.4 40.0-140 03/15/2023 02:37 WG2020454
(S) 1-Chloro-octadecane 91.3 40.0-140 03/15/2023 01:25 WG2020454
(S) 2-Fluorobiphenyl 92.2 40.0-140 03/15/2023 02:37 WG2020454
(S) 2-Bromonaphthalene 101 40.0-140 03/15/2023 02:37 WG2020454
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 03/12/2023 00:50 WG2020599
Acenaphthylene ND 1.00 1 03/12/2023 00:50 WG2020599
Anthracene ND 1.00 1 03/12/2023 00:50 WG2020599
Benzo(a)anthracene ND 1.00 1 03/12/2023 00:50 WG2020599
Benzo(b)fluoranthene ND 1.00 1 03/12/2023 00:50 WG2020599
Benzo(k)fluoranthene ND 1.00 1 03/12/2023 00:50 WG2020599
Benzo(g,h,i)perylene ND 1.00 1 03/12/2023 00:50 WG2020599
Benzo(a)pyrene ND 1.00 1 03/12/2023 00:50 WG2020599
Bis(2-chlorethoxy)methane ND 10.0 1 03/12/2023 00:50 WG2020599
Bis(2-chloroethyl)ether ND 10.0 1 03/12/2023 00:50 WG2020599
2,2-Oxybis(1-Chloropropane)ND 10.0 1 03/12/2023 00:50 WG2020599
4-Bromophenyl-phenylether ND 10.0 1 03/12/2023 00:50 WG2020599
2-Chloronaphthalene ND 1.00 1 03/12/2023 00:50 WG2020599
4-Chlorophenyl-phenylether ND 10.0 1 03/12/2023 00:50 WG2020599
Chrysene ND 1.00 1 03/12/2023 00:50 WG2020599
Dibenz(a,h)anthracene ND 1.00 1 03/12/2023 00:50 WG2020599
3,3-Dichlorobenzidine ND 10.0 1 03/12/2023 00:50 WG2020599
2,4-Dinitrotoluene ND 10.0 1 03/12/2023 00:50 WG2020599
2,6-Dinitrotoluene ND 10.0 1 03/12/2023 00:50 WG2020599
Fluoranthene ND 1.00 1 03/12/2023 00:50 WG2020599
Fluorene ND 1.00 1 03/12/2023 00:50 WG2020599
Hexachlorobenzene ND 1.00 1 03/12/2023 00:50 WG2020599
Hexachloro-1,3-butadiene ND 10.0 1 03/12/2023 00:50 WG2020599
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 37 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 37 of 78
SAMPLE RESULTS - 11
L1592757
MW-4D
Collected date/time: 03/07/23 12:15
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Hexachlorocyclopentadiene ND 10.0 1 03/12/2023 00:50 WG2020599
Hexachloroethane ND 10.0 1 03/12/2023 00:50 WG2020599
Indeno(1,2,3-cd)pyrene ND 1.00 1 03/12/2023 00:50 WG2020599
Isophorone ND 10.0 1 03/12/2023 00:50 WG2020599
Naphthalene 19.7 1.00 1 03/12/2023 00:50 WG2020599
Nitrobenzene ND 10.0 1 03/12/2023 00:50 WG2020599
n-Nitrosodimethylamine ND 10.0 1 03/12/2023 00:50 WG2020599
n-Nitrosodiphenylamine ND 10.0 1 03/12/2023 00:50 WG2020599
n-Nitrosodi-n-propylamine ND 10.0 1 03/12/2023 00:50 WG2020599
Phenanthrene ND 1.00 1 03/12/2023 00:50 WG2020599
Benzylbutyl phthalate ND 3.00 1 03/12/2023 00:50 WG2020599
Bis(2-ethylhexyl)phthalate ND 3.00 1 03/12/2023 00:50 WG2020599
Di-n-butyl phthalate ND 3.00 1 03/12/2023 00:50 WG2020599
Diethyl phthalate ND 3.00 1 03/12/2023 00:50 WG2020599
Dimethyl phthalate ND 3.00 1 03/12/2023 00:50 WG2020599
Di-n-octyl phthalate ND 3.00 1 03/12/2023 00:50 WG2020599
Pyrene ND 1.00 1 03/12/2023 00:50 WG2020599
1,2,4-Trichlorobenzene ND 10.0 1 03/12/2023 00:50 WG2020599
4-Chloro-3-methylphenol ND 10.0 1 03/12/2023 00:50 WG2020599
2-Chlorophenol ND 10.0 1 03/12/2023 00:50 WG2020599
2,4-Dichlorophenol ND 10.0 1 03/12/2023 00:50 WG2020599
2,4-Dimethylphenol ND 10.0 1 03/12/2023 00:50 WG2020599
4,6-Dinitro-2-methylphenol ND 10.0 1 03/12/2023 00:50 WG2020599
2,4-Dinitrophenol ND 10.0 1 03/12/2023 00:50 WG2020599
2-Nitrophenol ND 10.0 1 03/12/2023 00:50 WG2020599
4-Nitrophenol ND 10.0 1 03/12/2023 00:50 WG2020599
Pentachlorophenol ND 10.0 1 03/12/2023 00:50 WG2020599
Phenol ND 10.0 1 03/12/2023 00:50 WG2020599
2,4,6-Trichlorophenol ND 10.0 1 03/12/2023 00:50 WG2020599
(S) Nitrobenzene-d5 80.0 15.0-314 03/12/2023 00:50 WG2020599
(S) 2-Fluorobiphenyl 61.0 22.0-127 03/12/2023 00:50 WG2020599
(S) p-Terphenyl-d14 50.9 29.0-141 03/12/2023 00:50 WG2020599
(S) Phenol-d5 17.4 8.00-424 03/12/2023 00:50 WG2020599
(S) 2-Fluorophenol 23.1 10.0-120 03/12/2023 00:50 WG2020599
(S) 2,4,6-Tribromophenol 49.5 10.0-153 03/12/2023 00:50 WG2020599
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 38 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 38 of 78
SAMPLE RESULTS - 12
L1592757
MW-5D
Collected date/time: 03/07/23 10:25
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene ND 1.00 1 03/09/2023 18:19 WG2020042
Bromobenzene ND 1.00 1 03/09/2023 18:19 WG2020042
Bromodichloromethane ND 1.00 1 03/09/2023 18:19 WG2020042
Bromochloromethane ND 1.00 1 03/09/2023 18:19 WG2020042
Bromoform ND 1.00 1 03/09/2023 18:19 WG2020042
Bromomethane ND 5.00 1 03/09/2023 18:19 WG2020042
n-Butylbenzene ND 1.00 1 03/09/2023 18:19 WG2020042
sec-Butylbenzene ND 1.00 1 03/09/2023 18:19 WG2020042
tert-Butylbenzene ND 1.00 1 03/09/2023 18:19 WG2020042
Carbon tetrachloride ND 1.00 1 03/09/2023 18:19 WG2020042
Chlorobenzene ND 1.00 1 03/09/2023 18:19 WG2020042
Chlorodibromomethane ND 1.00 1 03/09/2023 18:19 WG2020042
Chloroethane ND 5.00 1 03/09/2023 18:19 WG2020042
Chloroform ND 5.00 1 03/09/2023 18:19 WG2020042
Chloromethane ND 2.50 1 03/09/2023 18:19 WG2020042
2-Chlorotoluene ND 1.00 1 03/09/2023 18:19 WG2020042
4-Chlorotoluene ND 1.00 1 03/09/2023 18:19 WG2020042
1,2-Dibromo-3-Chloropropane ND 5.00 1 03/09/2023 18:19 WG2020042
1,2-Dibromoethane ND 1.00 1 03/09/2023 18:19 WG2020042
Dibromomethane ND 1.00 1 03/09/2023 18:19 WG2020042
1,2-Dichlorobenzene ND 1.00 1 03/09/2023 18:19 WG2020042
1,3-Dichlorobenzene ND 1.00 1 03/09/2023 18:19 WG2020042
1,4-Dichlorobenzene ND 1.00 1 03/09/2023 18:19 WG2020042
Dichlorodifluoromethane ND 5.00 1 03/09/2023 18:19 WG2020042
1,1-Dichloroethane ND 1.00 1 03/09/2023 18:19 WG2020042
1,2-Dichloroethane ND 1.00 1 03/09/2023 18:19 WG2020042
1,1-Dichloroethene ND 1.00 1 03/09/2023 18:19 WG2020042
cis-1,2-Dichloroethene ND 1.00 1 03/09/2023 18:19 WG2020042
trans-1,2-Dichloroethene ND 1.00 1 03/09/2023 18:19 WG2020042
1,2-Dichloropropane ND 1.00 1 03/09/2023 18:19 WG2020042
1,1-Dichloropropene ND 1.00 1 03/09/2023 18:19 WG2020042
1,3-Dichloropropane ND 1.00 1 03/09/2023 18:19 WG2020042
cis-1,3-Dichloropropene ND 1.00 1 03/09/2023 18:19 WG2020042
trans-1,3-Dichloropropene ND 1.00 1 03/09/2023 18:19 WG2020042
2,2-Dichloropropane ND 1.00 1 03/09/2023 18:19 WG2020042
Di-isopropyl ether ND 1.00 1 03/09/2023 18:19 WG2020042
Ethylbenzene ND 1.00 1 03/09/2023 18:19 WG2020042
Hexachloro-1,3-butadiene ND 1.00 1 03/09/2023 18:19 WG2020042
Isopropylbenzene ND 1.00 1 03/09/2023 18:19 WG2020042
Methylene Chloride ND 5.00 1 03/09/2023 18:19 WG2020042
Methyl tert-butyl ether ND 1.00 1 03/09/2023 18:19 WG2020042
Naphthalene ND 5.00 1 03/09/2023 18:19 WG2020042
n-Propylbenzene ND 1.00 1 03/09/2023 18:19 WG2020042
Styrene ND 1.00 1 03/09/2023 18:19 WG2020042
1,1,1,2-Tetrachloroethane ND 1.00 1 03/09/2023 18:19 WG2020042
1,1,2,2-Tetrachloroethane ND 1.00 1 03/09/2023 18:19 WG2020042
Tetrachloroethene ND 1.00 1 03/09/2023 18:19 WG2020042
Toluene ND 1.00 1 03/09/2023 18:19 WG2020042
1,2,3-Trichlorobenzene ND 1.00 1 03/09/2023 18:19 WG2020042
1,2,4-Trichlorobenzene ND 1.00 1 03/09/2023 18:19 WG2020042
1,1,1-Trichloroethane ND 1.00 1 03/09/2023 18:19 WG2020042
1,1,2-Trichloroethane ND 1.00 1 03/09/2023 18:19 WG2020042
Trichloroethene ND 1.00 1 03/09/2023 18:19 WG2020042
Trichlorofluoromethane ND 5.00 1 03/09/2023 18:19 WG2020042
1,2,3-Trichloropropane ND 2.50 1 03/09/2023 18:19 WG2020042
1,2,4-Trimethylbenzene ND 1.00 1 03/09/2023 18:19 WG2020042
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 39 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 39 of 78
SAMPLE RESULTS - 12
L1592757
MW-5D
Collected date/time: 03/07/23 10:25
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 03/09/2023 18:19 WG2020042
Vinyl chloride ND 1.00 1 03/09/2023 18:19 WG2020042
o-Xylene ND 1.00 1 03/09/2023 18:19 WG2020042
m&p-Xylenes ND 2.00 1 03/09/2023 18:19 WG2020042
ethanol ND 100 1 03/09/2023 18:19 WG2020042
tert-Amyl Methyl Ether ND 1.00 1 03/09/2023 18:19 WG2020042
Ethyl tert-butyl ether ND 1.00 1 03/09/2023 18:19 WG2020042
tert-Butyl alcohol ND 5.00 1 03/09/2023 18:19 WG2020042
t-Amyl Alcohol ND 50.0 1 03/09/2023 18:19 WG2020042
tert-Butyl formate ND 20.0 1 03/10/2023 19:07 WG2020940
(S) Toluene-d8 97.4 80.0-120 03/09/2023 18:19 WG2020042
(S) Toluene-d8 101 80.0-120 03/10/2023 19:07 WG2020940
(S) 4-Bromofluorobenzene 87.6 77.0-126 03/09/2023 18:19 WG2020042
(S) 4-Bromofluorobenzene 105 77.0-126 03/10/2023 19:07 WG2020940
(S) 1,2-Dichloroethane-d4 95.3 70.0-130 03/09/2023 18:19 WG2020042
(S) 1,2-Dichloroethane-d4 114 70.0-130 03/10/2023 19:07 WG2020940
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 03/15/2023 01:49 WG2020454
Unadjusted C19-C36 Aliphatics ND 100 1 03/15/2023 01:49 WG2020454
Unadjusted C11-C22 Aromatics ND 100 1 03/15/2023 03:01 WG2020454
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 03/15/2023 01:49 WG2020454
(S) o-Terphenyl 87.5 40.0-140 03/15/2023 03:01 WG2020454
(S) 1-Chloro-octadecane 82.8 40.0-140 03/15/2023 01:49 WG2020454
(S) 2-Fluorobiphenyl 89.2 40.0-140 03/15/2023 03:01 WG2020454
(S) 2-Bromonaphthalene 97.6 40.0-140 03/15/2023 03:01 WG2020454
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 03/12/2023 01:11 WG2020599
Acenaphthylene ND 1.00 1 03/12/2023 01:11 WG2020599
Anthracene ND 1.00 1 03/12/2023 01:11 WG2020599
Benzo(a)anthracene ND 1.00 1 03/12/2023 01:11 WG2020599
Benzo(b)fluoranthene ND 1.00 1 03/12/2023 01:11 WG2020599
Benzo(k)fluoranthene ND 1.00 1 03/12/2023 01:11 WG2020599
Benzo(g,h,i)perylene ND 1.00 1 03/12/2023 01:11 WG2020599
Benzo(a)pyrene ND 1.00 1 03/12/2023 01:11 WG2020599
Bis(2-chlorethoxy)methane ND 10.0 1 03/12/2023 01:11 WG2020599
Bis(2-chloroethyl)ether ND 10.0 1 03/12/2023 01:11 WG2020599
2,2-Oxybis(1-Chloropropane)ND 10.0 1 03/12/2023 01:11 WG2020599
4-Bromophenyl-phenylether ND 10.0 1 03/12/2023 01:11 WG2020599
2-Chloronaphthalene ND 1.00 1 03/12/2023 01:11 WG2020599
4-Chlorophenyl-phenylether ND 10.0 1 03/12/2023 01:11 WG2020599
Chrysene ND 1.00 1 03/12/2023 01:11 WG2020599
Dibenz(a,h)anthracene ND 1.00 1 03/12/2023 01:11 WG2020599
3,3-Dichlorobenzidine ND 10.0 1 03/12/2023 01:11 WG2020599
2,4-Dinitrotoluene ND 10.0 1 03/12/2023 01:11 WG2020599
2,6-Dinitrotoluene ND 10.0 1 03/12/2023 01:11 WG2020599
Fluoranthene ND 1.00 1 03/12/2023 01:11 WG2020599
Fluorene ND 1.00 1 03/12/2023 01:11 WG2020599
Hexachlorobenzene ND 1.00 1 03/12/2023 01:11 WG2020599
Hexachloro-1,3-butadiene ND 10.0 1 03/12/2023 01:11 WG2020599
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 40 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 40 of 78
SAMPLE RESULTS - 12
L1592757
MW-5D
Collected date/time: 03/07/23 10:25
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Hexachlorocyclopentadiene ND 10.0 1 03/12/2023 01:11 WG2020599
Hexachloroethane ND 10.0 1 03/12/2023 01:11 WG2020599
Indeno(1,2,3-cd)pyrene ND 1.00 1 03/12/2023 01:11 WG2020599
Isophorone ND 10.0 1 03/12/2023 01:11 WG2020599
Naphthalene ND 1.00 1 03/12/2023 01:11 WG2020599
Nitrobenzene ND 10.0 1 03/12/2023 01:11 WG2020599
n-Nitrosodimethylamine ND 10.0 1 03/12/2023 01:11 WG2020599
n-Nitrosodiphenylamine ND 10.0 1 03/12/2023 01:11 WG2020599
n-Nitrosodi-n-propylamine ND 10.0 1 03/12/2023 01:11 WG2020599
Phenanthrene ND 1.00 1 03/12/2023 01:11 WG2020599
Benzylbutyl phthalate ND 3.00 1 03/12/2023 01:11 WG2020599
Bis(2-ethylhexyl)phthalate ND 3.00 1 03/12/2023 01:11 WG2020599
Di-n-butyl phthalate ND 3.00 1 03/12/2023 01:11 WG2020599
Diethyl phthalate ND 3.00 1 03/12/2023 01:11 WG2020599
Dimethyl phthalate ND 3.00 1 03/12/2023 01:11 WG2020599
Di-n-octyl phthalate ND 3.00 1 03/12/2023 01:11 WG2020599
Pyrene ND 1.00 1 03/12/2023 01:11 WG2020599
1,2,4-Trichlorobenzene ND 10.0 1 03/12/2023 01:11 WG2020599
4-Chloro-3-methylphenol ND 10.0 1 03/12/2023 01:11 WG2020599
2-Chlorophenol ND 10.0 1 03/12/2023 01:11 WG2020599
2,4-Dichlorophenol ND 10.0 1 03/12/2023 01:11 WG2020599
2,4-Dimethylphenol ND 10.0 1 03/12/2023 01:11 WG2020599
4,6-Dinitro-2-methylphenol ND 10.0 1 03/12/2023 01:11 WG2020599
2,4-Dinitrophenol ND 10.0 1 03/12/2023 01:11 WG2020599
2-Nitrophenol ND 10.0 1 03/12/2023 01:11 WG2020599
4-Nitrophenol ND 10.0 1 03/12/2023 01:11 WG2020599
Pentachlorophenol ND 10.0 1 03/12/2023 01:11 WG2020599
Phenol ND 10.0 1 03/12/2023 01:11 WG2020599
2,4,6-Trichlorophenol ND 10.0 1 03/12/2023 01:11 WG2020599
(S) Nitrobenzene-d5 94.1 15.0-314 03/12/2023 01:11 WG2020599
(S) 2-Fluorobiphenyl 70.7 22.0-127 03/12/2023 01:11 WG2020599
(S) p-Terphenyl-d14 63.3 29.0-141 03/12/2023 01:11 WG2020599
(S) Phenol-d5 18.7 8.00-424 03/12/2023 01:11 WG2020599
(S) 2-Fluorophenol 27.1 10.0-120 03/12/2023 01:11 WG2020599
(S) 2,4,6-Tribromophenol 67.6 10.0-153 03/12/2023 01:11 WG2020599
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 41 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 41 of 78
SAMPLE RESULTS - 13
L1592757
MW-6D
Collected date/time: 03/07/23 11:20
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene ND 1.00 1 03/09/2023 18:41 WG2020042
Bromobenzene ND 1.00 1 03/09/2023 18:41 WG2020042
Bromodichloromethane ND 1.00 1 03/09/2023 18:41 WG2020042
Bromochloromethane ND 1.00 1 03/09/2023 18:41 WG2020042
Bromoform ND 1.00 1 03/09/2023 18:41 WG2020042
Bromomethane ND 5.00 1 03/09/2023 18:41 WG2020042
n-Butylbenzene ND 1.00 1 03/09/2023 18:41 WG2020042
sec-Butylbenzene ND 1.00 1 03/09/2023 18:41 WG2020042
tert-Butylbenzene ND 1.00 1 03/09/2023 18:41 WG2020042
Carbon tetrachloride ND 1.00 1 03/09/2023 18:41 WG2020042
Chlorobenzene ND 1.00 1 03/09/2023 18:41 WG2020042
Chlorodibromomethane ND 1.00 1 03/09/2023 18:41 WG2020042
Chloroethane ND 5.00 1 03/09/2023 18:41 WG2020042
Chloroform ND 5.00 1 03/09/2023 18:41 WG2020042
Chloromethane ND 2.50 1 03/09/2023 18:41 WG2020042
2-Chlorotoluene ND 1.00 1 03/09/2023 18:41 WG2020042
4-Chlorotoluene ND 1.00 1 03/09/2023 18:41 WG2020042
1,2-Dibromo-3-Chloropropane ND 5.00 1 03/09/2023 18:41 WG2020042
1,2-Dibromoethane ND 1.00 1 03/09/2023 18:41 WG2020042
Dibromomethane ND 1.00 1 03/09/2023 18:41 WG2020042
1,2-Dichlorobenzene ND 1.00 1 03/09/2023 18:41 WG2020042
1,3-Dichlorobenzene ND 1.00 1 03/09/2023 18:41 WG2020042
1,4-Dichlorobenzene ND 1.00 1 03/09/2023 18:41 WG2020042
Dichlorodifluoromethane ND 5.00 1 03/09/2023 18:41 WG2020042
1,1-Dichloroethane ND 1.00 1 03/09/2023 18:41 WG2020042
1,2-Dichloroethane ND 1.00 1 03/09/2023 18:41 WG2020042
1,1-Dichloroethene ND 1.00 1 03/09/2023 18:41 WG2020042
cis-1,2-Dichloroethene ND 1.00 1 03/09/2023 18:41 WG2020042
trans-1,2-Dichloroethene ND 1.00 1 03/09/2023 18:41 WG2020042
1,2-Dichloropropane ND 1.00 1 03/09/2023 18:41 WG2020042
1,1-Dichloropropene ND 1.00 1 03/09/2023 18:41 WG2020042
1,3-Dichloropropane ND 1.00 1 03/09/2023 18:41 WG2020042
cis-1,3-Dichloropropene ND 1.00 1 03/09/2023 18:41 WG2020042
trans-1,3-Dichloropropene ND 1.00 1 03/09/2023 18:41 WG2020042
2,2-Dichloropropane ND 1.00 1 03/09/2023 18:41 WG2020042
Di-isopropyl ether ND 1.00 1 03/09/2023 18:41 WG2020042
Ethylbenzene ND 1.00 1 03/09/2023 18:41 WG2020042
Hexachloro-1,3-butadiene ND 1.00 1 03/09/2023 18:41 WG2020042
Isopropylbenzene ND 1.00 1 03/09/2023 18:41 WG2020042
Methylene Chloride ND 5.00 1 03/09/2023 18:41 WG2020042
Methyl tert-butyl ether ND 1.00 1 03/09/2023 18:41 WG2020042
Naphthalene ND 5.00 1 03/09/2023 18:41 WG2020042
n-Propylbenzene ND 1.00 1 03/09/2023 18:41 WG2020042
Styrene ND 1.00 1 03/09/2023 18:41 WG2020042
1,1,1,2-Tetrachloroethane ND 1.00 1 03/09/2023 18:41 WG2020042
1,1,2,2-Tetrachloroethane ND 1.00 1 03/09/2023 18:41 WG2020042
Tetrachloroethene ND 1.00 1 03/09/2023 18:41 WG2020042
Toluene ND 1.00 1 03/09/2023 18:41 WG2020042
1,2,3-Trichlorobenzene ND 1.00 1 03/09/2023 18:41 WG2020042
1,2,4-Trichlorobenzene ND 1.00 1 03/09/2023 18:41 WG2020042
1,1,1-Trichloroethane ND 1.00 1 03/09/2023 18:41 WG2020042
1,1,2-Trichloroethane ND 1.00 1 03/09/2023 18:41 WG2020042
Trichloroethene ND 1.00 1 03/09/2023 18:41 WG2020042
Trichlorofluoromethane ND 5.00 1 03/09/2023 18:41 WG2020042
1,2,3-Trichloropropane ND 2.50 1 03/09/2023 18:41 WG2020042
1,2,4-Trimethylbenzene ND 1.00 1 03/09/2023 18:41 WG2020042
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 42 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 42 of 78
SAMPLE RESULTS - 13
L1592757
MW-6D
Collected date/time: 03/07/23 11:20
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 03/09/2023 18:41 WG2020042
Vinyl chloride ND 1.00 1 03/09/2023 18:41 WG2020042
o-Xylene ND 1.00 1 03/09/2023 18:41 WG2020042
m&p-Xylenes ND 2.00 1 03/09/2023 18:41 WG2020042
ethanol ND 100 1 03/09/2023 18:41 WG2020042
tert-Amyl Methyl Ether ND 1.00 1 03/09/2023 18:41 WG2020042
Ethyl tert-butyl ether ND 1.00 1 03/09/2023 18:41 WG2020042
tert-Butyl alcohol ND 5.00 1 03/09/2023 18:41 WG2020042
t-Amyl Alcohol ND 50.0 1 03/09/2023 18:41 WG2020042
tert-Butyl formate ND 20.0 1 03/10/2023 19:28 WG2020940
(S) Toluene-d8 98.3 80.0-120 03/09/2023 18:41 WG2020042
(S) Toluene-d8 102 80.0-120 03/10/2023 19:28 WG2020940
(S) 4-Bromofluorobenzene 89.9 77.0-126 03/09/2023 18:41 WG2020042
(S) 4-Bromofluorobenzene 103 77.0-126 03/10/2023 19:28 WG2020940
(S) 1,2-Dichloroethane-d4 102 70.0-130 03/09/2023 18:41 WG2020042
(S) 1,2-Dichloroethane-d4 115 70.0-130 03/10/2023 19:28 WG2020940
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 03/15/2023 02:13 WG2020454
Unadjusted C19-C36 Aliphatics ND 100 1 03/15/2023 02:13 WG2020454
Unadjusted C11-C22 Aromatics ND 100 1 03/15/2023 03:25 WG2020454
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 03/15/2023 02:13 WG2020454
(S) o-Terphenyl 90.0 40.0-140 03/15/2023 03:25 WG2020454
(S) 1-Chloro-octadecane 88.4 40.0-140 03/15/2023 02:13 WG2020454
(S) 2-Fluorobiphenyl 91.3 40.0-140 03/15/2023 03:25 WG2020454
(S) 2-Bromonaphthalene 100 40.0-140 03/15/2023 03:25 WG2020454
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 03/12/2023 01:32 WG2020599
Acenaphthylene ND 1.00 1 03/12/2023 01:32 WG2020599
Anthracene ND 1.00 1 03/12/2023 01:32 WG2020599
Benzo(a)anthracene ND 1.00 1 03/12/2023 01:32 WG2020599
Benzo(b)fluoranthene ND 1.00 1 03/12/2023 01:32 WG2020599
Benzo(k)fluoranthene ND 1.00 1 03/12/2023 01:32 WG2020599
Benzo(g,h,i)perylene ND 1.00 1 03/12/2023 01:32 WG2020599
Benzo(a)pyrene ND 1.00 1 03/12/2023 01:32 WG2020599
Bis(2-chlorethoxy)methane ND 10.0 1 03/12/2023 01:32 WG2020599
Bis(2-chloroethyl)ether ND 10.0 1 03/12/2023 01:32 WG2020599
2,2-Oxybis(1-Chloropropane)ND 10.0 1 03/12/2023 01:32 WG2020599
4-Bromophenyl-phenylether ND 10.0 1 03/12/2023 01:32 WG2020599
2-Chloronaphthalene ND 1.00 1 03/12/2023 01:32 WG2020599
4-Chlorophenyl-phenylether ND 10.0 1 03/12/2023 01:32 WG2020599
Chrysene ND 1.00 1 03/12/2023 01:32 WG2020599
Dibenz(a,h)anthracene ND 1.00 1 03/12/2023 01:32 WG2020599
3,3-Dichlorobenzidine ND 10.0 1 03/12/2023 01:32 WG2020599
2,4-Dinitrotoluene ND 10.0 1 03/12/2023 01:32 WG2020599
2,6-Dinitrotoluene ND 10.0 1 03/12/2023 01:32 WG2020599
Fluoranthene ND 1.00 1 03/12/2023 01:32 WG2020599
Fluorene ND 1.00 1 03/12/2023 01:32 WG2020599
Hexachlorobenzene ND 1.00 1 03/12/2023 01:32 WG2020599
Hexachloro-1,3-butadiene ND 10.0 1 03/12/2023 01:32 WG2020599
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 43 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 43 of 78
SAMPLE RESULTS - 13
L1592757
MW-6D
Collected date/time: 03/07/23 11:20
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Hexachlorocyclopentadiene ND 10.0 1 03/12/2023 01:32 WG2020599
Hexachloroethane ND 10.0 1 03/12/2023 01:32 WG2020599
Indeno(1,2,3-cd)pyrene ND 1.00 1 03/12/2023 01:32 WG2020599
Isophorone ND 10.0 1 03/12/2023 01:32 WG2020599
Naphthalene ND 1.00 1 03/12/2023 01:32 WG2020599
Nitrobenzene ND 10.0 1 03/12/2023 01:32 WG2020599
n-Nitrosodimethylamine ND 10.0 1 03/12/2023 01:32 WG2020599
n-Nitrosodiphenylamine ND 10.0 1 03/12/2023 01:32 WG2020599
n-Nitrosodi-n-propylamine ND 10.0 1 03/12/2023 01:32 WG2020599
Phenanthrene ND 1.00 1 03/12/2023 01:32 WG2020599
Benzylbutyl phthalate ND 3.00 1 03/12/2023 01:32 WG2020599
Bis(2-ethylhexyl)phthalate ND 3.00 1 03/12/2023 01:32 WG2020599
Di-n-butyl phthalate ND 3.00 1 03/12/2023 01:32 WG2020599
Diethyl phthalate ND 3.00 1 03/12/2023 01:32 WG2020599
Dimethyl phthalate ND 3.00 1 03/12/2023 01:32 WG2020599
Di-n-octyl phthalate ND 3.00 1 03/12/2023 01:32 WG2020599
Pyrene ND 1.00 1 03/12/2023 01:32 WG2020599
1,2,4-Trichlorobenzene ND 10.0 1 03/12/2023 01:32 WG2020599
4-Chloro-3-methylphenol ND 10.0 1 03/12/2023 01:32 WG2020599
2-Chlorophenol ND 10.0 1 03/12/2023 01:32 WG2020599
2,4-Dichlorophenol ND 10.0 1 03/12/2023 01:32 WG2020599
2,4-Dimethylphenol ND 10.0 1 03/12/2023 01:32 WG2020599
4,6-Dinitro-2-methylphenol ND 10.0 1 03/12/2023 01:32 WG2020599
2,4-Dinitrophenol ND 10.0 1 03/12/2023 01:32 WG2020599
2-Nitrophenol ND 10.0 1 03/12/2023 01:32 WG2020599
4-Nitrophenol ND 10.0 1 03/12/2023 01:32 WG2020599
Pentachlorophenol ND 10.0 1 03/12/2023 01:32 WG2020599
Phenol ND 10.0 1 03/12/2023 01:32 WG2020599
2,4,6-Trichlorophenol ND 10.0 1 03/12/2023 01:32 WG2020599
(S) Nitrobenzene-d5 89.9 15.0-314 03/12/2023 01:32 WG2020599
(S) 2-Fluorobiphenyl 70.8 22.0-127 03/12/2023 01:32 WG2020599
(S) p-Terphenyl-d14 61.8 29.0-141 03/12/2023 01:32 WG2020599
(S) Phenol-d5 21.0 8.00-424 03/12/2023 01:32 WG2020599
(S) 2-Fluorophenol 28.2 10.0-120 03/12/2023 01:32 WG2020599
(S) 2,4,6-Tribromophenol 63.2 10.0-153 03/12/2023 01:32 WG2020599
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 44 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 44 of 78
SAMPLE RESULTS - 14
L1592757
MW-13
Collected date/time: 03/06/23 11:35
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene ND 1.00 1 03/16/2023 01:53 WG2023464
Bromobenzene ND 1.00 1 03/16/2023 01:53 WG2023464
Bromodichloromethane ND 1.00 1 03/16/2023 01:53 WG2023464
Bromochloromethane ND 1.00 1 03/16/2023 01:53 WG2023464
Bromoform ND 1.00 1 03/16/2023 01:53 WG2023464
Bromomethane ND 5.00 1 03/16/2023 01:53 WG2023464
n-Butylbenzene ND 1.00 1 03/16/2023 01:53 WG2023464
sec-Butylbenzene ND 1.00 1 03/16/2023 01:53 WG2023464
tert-Butylbenzene ND 1.00 1 03/16/2023 01:53 WG2023464
Carbon tetrachloride ND 1.00 1 03/16/2023 01:53 WG2023464
Chlorobenzene ND J4 1.00 1 03/16/2023 01:53 WG2023464
Chlorodibromomethane ND 1.00 1 03/16/2023 01:53 WG2023464
Chloroethane ND 5.00 1 03/16/2023 01:53 WG2023464
Chloroform ND 5.00 1 03/16/2023 01:53 WG2023464
Chloromethane ND 2.50 1 03/16/2023 01:53 WG2023464
2-Chlorotoluene ND 1.00 1 03/16/2023 01:53 WG2023464
4-Chlorotoluene ND 1.00 1 03/16/2023 01:53 WG2023464
1,2-Dibromo-3-Chloropropane ND 5.00 1 03/16/2023 01:53 WG2023464
1,2-Dibromoethane ND 1.00 1 03/16/2023 01:53 WG2023464
Dibromomethane ND 1.00 1 03/16/2023 01:53 WG2023464
1,2-Dichlorobenzene ND 1.00 1 03/16/2023 01:53 WG2023464
1,3-Dichlorobenzene ND 1.00 1 03/16/2023 01:53 WG2023464
1,4-Dichlorobenzene ND 1.00 1 03/16/2023 01:53 WG2023464
Dichlorodifluoromethane ND 5.00 1 03/16/2023 01:53 WG2023464
1,1-Dichloroethane ND 1.00 1 03/16/2023 01:53 WG2023464
1,2-Dichloroethane ND 1.00 1 03/16/2023 01:53 WG2023464
1,1-Dichloroethene ND 1.00 1 03/16/2023 01:53 WG2023464
cis-1,2-Dichloroethene ND 1.00 1 03/16/2023 01:53 WG2023464
trans-1,2-Dichloroethene ND 1.00 1 03/16/2023 01:53 WG2023464
1,2-Dichloropropane ND 1.00 1 03/16/2023 01:53 WG2023464
1,1-Dichloropropene ND 1.00 1 03/16/2023 01:53 WG2023464
1,3-Dichloropropane ND 1.00 1 03/16/2023 01:53 WG2023464
cis-1,3-Dichloropropene ND 1.00 1 03/16/2023 01:53 WG2023464
trans-1,3-Dichloropropene ND 1.00 1 03/16/2023 01:53 WG2023464
2,2-Dichloropropane ND 1.00 1 03/16/2023 01:53 WG2023464
Di-isopropyl ether ND 1.00 1 03/16/2023 01:53 WG2023464
Ethylbenzene ND 1.00 1 03/16/2023 01:53 WG2023464
Hexachloro-1,3-butadiene ND 1.00 1 03/16/2023 01:53 WG2023464
Isopropylbenzene ND 1.00 1 03/16/2023 01:53 WG2023464
Methylene Chloride ND 5.00 1 03/16/2023 01:53 WG2023464
Methyl tert-butyl ether ND 1.00 1 03/16/2023 01:53 WG2023464
Naphthalene ND 5.00 1 03/16/2023 01:53 WG2023464
n-Propylbenzene ND 1.00 1 03/16/2023 01:53 WG2023464
Styrene ND 1.00 1 03/16/2023 01:53 WG2023464
1,1,1,2-Tetrachloroethane ND 1.00 1 03/16/2023 01:53 WG2023464
1,1,2,2-Tetrachloroethane ND 1.00 1 03/16/2023 01:53 WG2023464
Tetrachloroethene ND 1.00 1 03/16/2023 11:53 WG2024328
Toluene ND 1.00 1 03/16/2023 01:53 WG2023464
1,2,3-Trichlorobenzene ND 1.00 1 03/16/2023 01:53 WG2023464
1,2,4-Trichlorobenzene ND 1.00 1 03/16/2023 01:53 WG2023464
1,1,1-Trichloroethane ND 1.00 1 03/16/2023 01:53 WG2023464
1,1,2-Trichloroethane ND 1.00 1 03/16/2023 01:53 WG2023464
Trichloroethene ND 1.00 1 03/16/2023 01:53 WG2023464
Trichlorofluoromethane ND 5.00 1 03/16/2023 01:53 WG2023464
1,2,3-Trichloropropane ND 2.50 1 03/16/2023 01:53 WG2023464
1,2,4-Trimethylbenzene ND 1.00 1 03/16/2023 01:53 WG2023464
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 45 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 45 of 78
SAMPLE RESULTS - 14
L1592757
MW-13
Collected date/time: 03/06/23 11:35
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 03/16/2023 01:53 WG2023464
Vinyl chloride ND 1.00 1 03/16/2023 01:53 WG2023464
o-Xylene ND 1.00 1 03/16/2023 01:53 WG2023464
m&p-Xylenes ND 2.00 1 03/16/2023 01:53 WG2023464
ethanol ND 100 1 03/16/2023 11:53 WG2024328
tert-Amyl Methyl Ether ND 1.00 1 03/16/2023 01:53 WG2023464
Ethyl tert-butyl ether ND 1.00 1 03/16/2023 01:53 WG2023464
tert-Butyl alcohol ND J3 5.00 1 03/16/2023 01:53 WG2023464
t-Amyl Alcohol ND 50.0 1 03/16/2023 01:53 WG2023464
tert-Butyl formate ND 20.0 1 03/16/2023 11:53 WG2024328
(S) Toluene-d8 112 80.0-120 03/16/2023 01:53 WG2023464
(S) Toluene-d8 108 80.0-120 03/16/2023 11:53 WG2024328
(S) 4-Bromofluorobenzene 94.9 77.0-126 03/16/2023 01:53 WG2023464
(S) 4-Bromofluorobenzene 109 77.0-126 03/16/2023 11:53 WG2024328
(S) 1,2-Dichloroethane-d4 88.6 70.0-130 03/16/2023 01:53 WG2023464
(S) 1,2-Dichloroethane-d4 113 70.0-130 03/16/2023 11:53 WG2024328
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 03/15/2023 17:19 WG2022391
Unadjusted C19-C36 Aliphatics ND 100 1 03/15/2023 17:19 WG2022391
Unadjusted C11-C22 Aromatics ND 100 1 03/15/2023 21:21 WG2022391
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 03/15/2023 21:21 WG2022391
(S) o-Terphenyl 73.9 40.0-140 03/15/2023 21:21 WG2022391
(S) 1-Chloro-octadecane 45.9 40.0-140 03/15/2023 17:19 WG2022391
(S) 2-Fluorobiphenyl 88.2 40.0-140 03/15/2023 21:21 WG2022391
(S) 2-Bromonaphthalene 96.4 40.0-140 03/15/2023 21:21 WG2022391
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 03/12/2023 09:39 WG2020599
Acenaphthylene ND 1.00 1 03/12/2023 09:39 WG2020599
Anthracene ND 1.00 1 03/12/2023 09:39 WG2020599
Benzo(a)anthracene ND 1.00 1 03/12/2023 09:39 WG2020599
Benzo(b)fluoranthene ND 1.00 1 03/12/2023 09:39 WG2020599
Benzo(k)fluoranthene ND 1.00 1 03/12/2023 09:39 WG2020599
Benzo(g,h,i)perylene ND 1.00 1 03/12/2023 09:39 WG2020599
Benzo(a)pyrene ND 1.00 1 03/12/2023 09:39 WG2020599
Bis(2-chlorethoxy)methane ND 10.0 1 03/12/2023 09:39 WG2020599
Bis(2-chloroethyl)ether ND 10.0 1 03/12/2023 09:39 WG2020599
2,2-Oxybis(1-Chloropropane)ND 10.0 1 03/12/2023 09:39 WG2020599
4-Bromophenyl-phenylether ND 10.0 1 03/12/2023 09:39 WG2020599
2-Chloronaphthalene ND 1.00 1 03/12/2023 09:39 WG2020599
4-Chlorophenyl-phenylether ND 10.0 1 03/12/2023 09:39 WG2020599
Chrysene ND 1.00 1 03/12/2023 09:39 WG2020599
Dibenz(a,h)anthracene ND 1.00 1 03/12/2023 09:39 WG2020599
3,3-Dichlorobenzidine ND 10.0 1 03/12/2023 09:39 WG2020599
2,4-Dinitrotoluene ND 10.0 1 03/12/2023 09:39 WG2020599
2,6-Dinitrotoluene ND 10.0 1 03/12/2023 09:39 WG2020599
Fluoranthene ND 1.00 1 03/12/2023 09:39 WG2020599
Fluorene ND 1.00 1 03/12/2023 09:39 WG2020599
Hexachlorobenzene ND 1.00 1 03/12/2023 09:39 WG2020599
Hexachloro-1,3-butadiene ND 10.0 1 03/12/2023 09:39 WG2020599
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 46 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 46 of 78
SAMPLE RESULTS - 14
L1592757
MW-13
Collected date/time: 03/06/23 11:35
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Hexachlorocyclopentadiene ND 10.0 1 03/12/2023 09:39 WG2020599
Hexachloroethane ND 10.0 1 03/12/2023 09:39 WG2020599
Indeno(1,2,3-cd)pyrene ND 1.00 1 03/12/2023 09:39 WG2020599
Isophorone ND 10.0 1 03/12/2023 09:39 WG2020599
Naphthalene ND 1.00 1 03/12/2023 09:39 WG2020599
Nitrobenzene ND 10.0 1 03/12/2023 09:39 WG2020599
n-Nitrosodimethylamine ND 10.0 1 03/12/2023 09:39 WG2020599
n-Nitrosodiphenylamine ND 10.0 1 03/12/2023 09:39 WG2020599
n-Nitrosodi-n-propylamine ND 10.0 1 03/12/2023 09:39 WG2020599
Phenanthrene ND 1.00 1 03/12/2023 09:39 WG2020599
Benzylbutyl phthalate ND 3.00 1 03/12/2023 09:39 WG2020599
Bis(2-ethylhexyl)phthalate ND 3.00 1 03/12/2023 09:39 WG2020599
Di-n-butyl phthalate ND 3.00 1 03/12/2023 09:39 WG2020599
Diethyl phthalate ND 3.00 1 03/12/2023 09:39 WG2020599
Dimethyl phthalate ND 3.00 1 03/12/2023 09:39 WG2020599
Di-n-octyl phthalate ND 3.00 1 03/12/2023 09:39 WG2020599
Pyrene ND 1.00 1 03/12/2023 09:39 WG2020599
1,2,4-Trichlorobenzene ND 10.0 1 03/12/2023 09:39 WG2020599
4-Chloro-3-methylphenol ND 10.0 1 03/12/2023 09:39 WG2020599
2-Chlorophenol ND 10.0 1 03/12/2023 09:39 WG2020599
2,4-Dichlorophenol ND 10.0 1 03/12/2023 09:39 WG2020599
2,4-Dimethylphenol ND 10.0 1 03/12/2023 09:39 WG2020599
4,6-Dinitro-2-methylphenol ND 10.0 1 03/12/2023 09:39 WG2020599
2,4-Dinitrophenol ND 10.0 1 03/12/2023 09:39 WG2020599
2-Nitrophenol ND 10.0 1 03/12/2023 09:39 WG2020599
4-Nitrophenol ND 10.0 1 03/12/2023 09:39 WG2020599
Pentachlorophenol ND 10.0 1 03/12/2023 09:39 WG2020599
Phenol ND 10.0 1 03/12/2023 09:39 WG2020599
2,4,6-Trichlorophenol ND 10.0 1 03/12/2023 09:39 WG2020599
(S) Nitrobenzene-d5 77.6 15.0-314 03/12/2023 09:39 WG2020599
(S) 2-Fluorobiphenyl 58.6 22.0-127 03/12/2023 09:39 WG2020599
(S) p-Terphenyl-d14 51.5 29.0-141 03/12/2023 09:39 WG2020599
(S) Phenol-d5 16.4 8.00-424 03/12/2023 09:39 WG2020599
(S) 2-Fluorophenol 22.9 10.0-120 03/12/2023 09:39 WG2020599
(S) 2,4,6-Tribromophenol 46.2 10.0-153 03/12/2023 09:39 WG2020599
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 47 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 47 of 78
QUALITY CONTROL SUMMARYWG2020042
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1592757-01,02,03,04,05,06,07,08,09,10,11,12,13
Method Blank (MB)
(MB) R3899200-2 03/09/23 10:35
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Benzene U 0.0941 1.00
Bromobenzene U 0.118 1.00
Bromodichloromethane U 0.136 1.00
Bromochloromethane U 0.128 1.00
Bromoform U 0.129 1.00
Bromomethane U 0.605 5.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
cis-1,3-Dichloropropene U 0.111 1.00
trans-1,3-Dichloropropene U 0.118 1.00
2,2-Dichloropropane U 0.161 1.00
Di-isopropyl ether U 0.105 1.00
Ethylbenzene U 0.137 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
Isopropylbenzene U 0.105 1.00
Methylene Chloride U 0.430 5.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 48 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 48 of 78
QUALITY CONTROL SUMMARYWG2020042
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1592757-01,02,03,04,05,06,07,08,09,10,11,12,13
Method Blank (MB)
(MB) R3899200-2 03/09/23 10:35
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Methyl tert-butyl ether U 0.101 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.0993 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Trichlorofluoromethane U 0.160 5.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,4-Trimethylbenzene U 0.322 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
Vinyl chloride U 0.234 1.00
o-Xylene U 0.174 1.00
m&p-Xylenes U 0.430 2.00
Ethanol U 42.0 100
tert-Amyl Methyl Ether U 0.195 1.00
Ethyl tert-butyl ether U 0.101 1.00
tert-Butyl alcohol U 4.06 5.00
t-Amyl Alcohol U 4.90 50.0
(S) Toluene-d8 96.6 80.0-120
(S) 4-Bromofluorobenzene 87.8 77.0-126
(S) 1,2-Dichloroethane-d4 95.5 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3899200-1 03/09/23 09:52
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Benzene 5.00 5.10 102 70.0-123
Bromobenzene 5.00 4.87 97.4 73.0-121
Bromodichloromethane 5.00 4.81 96.2 75.0-120
Bromochloromethane 5.00 4.95 99.0 76.0-122
Bromoform 5.00 4.63 92.6 68.0-132
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 49 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 49 of 78
QUALITY CONTROL SUMMARYWG2020042
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1592757-01,02,03,04,05,06,07,08,09,10,11,12,13
Laboratory Control Sample (LCS)
(LCS) R3899200-1 03/09/23 09:52
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Bromomethane 5.00 3.51 70.2 10.0-160
n-Butylbenzene 5.00 4.90 98.0 73.0-125
sec-Butylbenzene 5.00 4.94 98.8 75.0-125
tert-Butylbenzene 5.00 4.84 96.8 76.0-124
Carbon tetrachloride 5.00 4.73 94.6 68.0-126
Chlorobenzene 5.00 5.04 101 80.0-121
Chlorodibromomethane 5.00 4.64 92.8 77.0-125
Chloroethane 5.00 4.77 95.4 47.0-150
Chloroform 5.00 4.79 95.8 73.0-120
Chloromethane 5.00 4.21 84.2 41.0-142
2-Chlorotoluene 5.00 5.08 102 76.0-123
4-Chlorotoluene 5.00 4.91 98.2 75.0-122
1,2-Dibromo-3-Chloropropane 5.00 4.33 86.6 58.0-134
1,2-Dibromoethane 5.00 5.01 100 80.0-122
Dibromomethane 5.00 5.14 103 80.0-120
1,2-Dichlorobenzene 5.00 4.91 98.2 79.0-121
1,3-Dichlorobenzene 5.00 4.89 97.8 79.0-120
1,4-Dichlorobenzene 5.00 4.89 97.8 79.0-120
Dichlorodifluoromethane 5.00 5.10 102 51.0-149
1,1-Dichloroethane 5.00 5.11 102 70.0-126
1,2-Dichloroethane 5.00 4.92 98.4 70.0-128
1,1-Dichloroethene 5.00 5.28 106 71.0-124
cis-1,2-Dichloroethene 5.00 5.12 102 73.0-120
trans-1,2-Dichloroethene 5.00 5.01 100 73.0-120
1,2-Dichloropropane 5.00 4.98 99.6 77.0-125
1,1-Dichloropropene 5.00 5.04 101 74.0-126
1,3-Dichloropropane 5.00 5.09 102 80.0-120
cis-1,3-Dichloropropene 5.00 4.68 93.6 80.0-123
trans-1,3-Dichloropropene 5.00 4.64 92.8 78.0-124
2,2-Dichloropropane 5.00 5.17 103 58.0-130
Di-isopropyl ether 5.00 5.02 100 58.0-138
Ethylbenzene 5.00 5.11 102 79.0-123
Hexachloro-1,3-butadiene 5.00 4.81 96.2 54.0-138
Isopropylbenzene 5.00 4.90 98.0 76.0-127
Methylene Chloride 5.00 4.90 98.0 67.0-120
Methyl tert-butyl ether 5.00 4.67 93.4 68.0-125
Naphthalene 5.00 3.58 71.6 54.0-135
n-Propylbenzene 5.00 4.95 99.0 77.0-124
Styrene 5.00 4.71 94.2 73.0-130
1,1,1,2-Tetrachloroethane 5.00 4.76 95.2 75.0-125
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 50 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 50 of 78
QUALITY CONTROL SUMMARYWG2020042
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1592757-01,02,03,04,05,06,07,08,09,10,11,12,13
Laboratory Control Sample (LCS)
(LCS) R3899200-1 03/09/23 09:52
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
1,1,2,2-Tetrachloroethane 5.00 5.02 100 65.0-130
Tetrachloroethene 5.00 4.95 99.0 72.0-132
Toluene 5.00 5.07 101 79.0-120
1,2,3-Trichlorobenzene 5.00 4.43 88.6 50.0-138
1,2,4-Trichlorobenzene 5.00 4.52 90.4 57.0-137
1,1,1-Trichloroethane 5.00 5.09 102 73.0-124
1,1,2-Trichloroethane 5.00 4.81 96.2 80.0-120
Trichloroethene 5.00 5.10 102 78.0-124
Trichlorofluoromethane 5.00 4.58 91.6 59.0-147
1,2,3-Trichloropropane 5.00 5.06 101 73.0-130
1,2,4-Trimethylbenzene 5.00 4.99 99.8 76.0-121
1,3,5-Trimethylbenzene 5.00 4.87 97.4 76.0-122
Vinyl chloride 5.00 4.85 97.0 67.0-131
o-Xylene 5.00 5.09 102 80.0-122
m&p-Xylenes 10.0 10.2 102 80.0-122
ethanol 250 267 107 10.0-160
tert-Amyl Methyl Ether 5.00 4.47 89.4 66.0-125
Ethyl tert-butyl ether 5.00 4.63 92.6 63.0-138
tert-Butyl alcohol 25.0 24.3 97.2 27.0-160
(S) Toluene-d8 96.6 80.0-120
(S) 4-Bromofluorobenzene 92.0 77.0-126
(S) 1,2-Dichloroethane-d4 97.0 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 51 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 51 of 78
QUALITY CONTROL SUMMARYWG2020940
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1592757-01,02,03,04,05,06,07,08,09,10,11,12,13
Method Blank (MB)
(MB) R3900770-4 03/10/23 12:49
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
tert-Butyl formate U 4.51 20.0
(S) Toluene-d8 102 80.0-120
(S) 4-Bromofluorobenzene 107 77.0-126
(S) 1,2-Dichloroethane-d4 108 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3900770-3 03/10/23 12:06
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
tert-Butyl Formate 100 78.5 78.5 10.0-160
(S) Toluene-d8 104 80.0-120
(S) 4-Bromofluorobenzene 108 77.0-126
(S) 1,2-Dichloroethane-d4 102 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 52 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 52 of 78
QUALITY CONTROL SUMMARYWG2023464
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1592757-14
Method Blank (MB)
(MB) R3901650-4 03/15/23 23:13
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Benzene U 0.0941 1.00
Bromobenzene U 0.118 1.00
Bromodichloromethane U 0.136 1.00
Bromochloromethane U 0.128 1.00
Bromoform U 0.129 1.00
Bromomethane U 0.605 5.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
cis-1,3-Dichloropropene U 0.111 1.00
trans-1,3-Dichloropropene U 0.118 1.00
2,2-Dichloropropane U 0.161 1.00
Di-isopropyl ether U 0.105 1.00
Ethylbenzene U 0.137 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
Isopropylbenzene U 0.105 1.00
Methylene Chloride U 0.430 5.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 53 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 53 of 78
QUALITY CONTROL SUMMARYWG2023464
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1592757-14
Method Blank (MB)
(MB) R3901650-4 03/15/23 23:13
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Methyl tert-butyl ether U 0.101 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.0993 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
Toluene U 0.278 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Trichlorofluoromethane U 0.160 5.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,4-Trimethylbenzene U 0.322 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
Vinyl chloride U 0.234 1.00
o-Xylene U 0.174 1.00
m&p-Xylenes U 0.430 2.00
tert-Amyl Methyl Ether U 0.195 1.00
Ethyl tert-butyl ether U 0.101 1.00
tert-Butyl alcohol U 4.06 5.00
t-Amyl Alcohol U 4.90 50.0
(S) Toluene-d8 116 80.0-120
(S) 4-Bromofluorobenzene 90.8 77.0-126
(S) 1,2-Dichloroethane-d4 86.8 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3901650-1 03/15/23 21:31 • (LCSD) R3901650-2 03/15/23 21:52
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Benzene 5.00 5.25 5.05 105 101 70.0-123 3.88 20
Bromobenzene 5.00 4.66 4.45 93.2 89.0 73.0-121 4.61 20
Bromodichloromethane 5.00 5.29 5.03 106 101 75.0-120 5.04 20
Bromochloromethane 5.00 5.99 5.69 120 114 76.0-122 5.14 20
Bromoform 5.00 6.13 5.95 123 119 68.0-132 2.98 20
Bromomethane 5.00 3.91 4.13 78.2 82.6 10.0-160 5.47 25
n-Butylbenzene 5.00 4.28 3.89 85.6 77.8 73.0-125 9.55 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 54 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 54 of 78
QUALITY CONTROL SUMMARYWG2023464
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1592757-14
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3901650-1 03/15/23 21:31 • (LCSD) R3901650-2 03/15/23 21:52
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
sec-Butylbenzene 5.00 4.87 4.61 97.4 92.2 75.0-125 5.49 20
tert-Butylbenzene 5.00 5.08 4.76 102 95.2 76.0-124 6.50 20
Carbon tetrachloride 5.00 5.47 5.29 109 106 68.0-126 3.35 20
Chlorobenzene 5.00 6.22 6.03 124 121 80.0-121 J4 3.10 20
Chlorodibromomethane 5.00 5.90 5.83 118 117 77.0-125 1.19 20
Chloroethane 5.00 4.94 4.68 98.8 93.6 47.0-150 5.41 20
Chloroform 5.00 5.28 5.02 106 100 73.0-120 5.05 20
Chloromethane 5.00 4.97 4.53 99.4 90.6 41.0-142 9.26 20
2-Chlorotoluene 5.00 5.26 4.80 105 96.0 76.0-123 9.15 20
4-Chlorotoluene 5.00 4.60 4.50 92.0 90.0 75.0-122 2.20 20
1,2-Dibromo-3-Chloropropane 5.00 5.33 5.22 107 104 58.0-134 2.09 20
1,2-Dibromoethane 5.00 5.76 5.59 115 112 80.0-122 3.00 20
Dibromomethane 5.00 5.81 5.67 116 113 80.0-120 2.44 20
1,2-Dichlorobenzene 5.00 5.23 4.81 105 96.2 79.0-121 8.37 20
1,3-Dichlorobenzene 5.00 5.32 4.99 106 99.8 79.0-120 6.40 20
1,4-Dichlorobenzene 5.00 5.38 5.02 108 100 79.0-120 6.92 20
Dichlorodifluoromethane 5.00 5.10 5.06 102 101 51.0-149 0.787 20
1,1-Dichloroethane 5.00 4.49 4.32 89.8 86.4 70.0-126 3.86 20
1,2-Dichloroethane 5.00 4.67 4.57 93.4 91.4 70.0-128 2.16 20
1,1-Dichloroethene 5.00 5.13 4.80 103 96.0 71.0-124 6.65 20
cis-1,2-Dichloroethene 5.00 5.27 5.24 105 105 73.0-120 0.571 20
trans-1,2-Dichloroethene 5.00 5.48 5.10 110 102 73.0-120 7.18 20
1,2-Dichloropropane 5.00 4.73 4.56 94.6 91.2 77.0-125 3.66 20
1,1-Dichloropropene 5.00 4.73 4.54 94.6 90.8 74.0-126 4.10 20
1,3-Dichloropropane 5.00 5.18 5.07 104 101 80.0-120 2.15 20
cis-1,3-Dichloropropene 5.00 4.82 4.67 96.4 93.4 80.0-123 3.16 20
trans-1,3-Dichloropropene 5.00 4.87 4.77 97.4 95.4 78.0-124 2.07 20
2,2-Dichloropropane 5.00 4.90 4.54 98.0 90.8 58.0-130 7.63 20
Di-isopropyl ether 5.00 4.09 3.96 81.8 79.2 58.0-138 3.23 20
Ethylbenzene 5.00 5.81 5.54 116 111 79.0-123 4.76 20
Hexachloro-1,3-butadiene 5.00 5.29 4.88 106 97.6 54.0-138 8.06 20
Isopropylbenzene 5.00 5.43 5.19 109 104 76.0-127 4.52 20
Methylene Chloride 5.00 5.42 5.10 108 102 67.0-120 6.08 20
Methyl tert-butyl ether 5.00 4.89 4.60 97.8 92.0 68.0-125 6.11 20
Naphthalene 5.00 3.92 3.98 78.4 79.6 54.0-135 1.52 20
n-Propylbenzene 5.00 4.83 4.54 96.6 90.8 77.0-124 6.19 20
Styrene 5.00 5.33 5.11 107 102 73.0-130 4.21 20
1,1,1,2-Tetrachloroethane 5.00 5.97 5.92 119 118 75.0-125 0.841 20
1,1,2,2-Tetrachloroethane 5.00 4.75 4.66 95.0 93.2 65.0-130 1.91 20
Toluene 5.00 5.56 5.46 111 109 79.0-120 1.81 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 55 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 55 of 78
QUALITY CONTROL SUMMARYWG2023464
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1592757-14
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3901650-1 03/15/23 21:31 • (LCSD) R3901650-2 03/15/23 21:52
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
1,2,3-Trichlorobenzene 5.00 4.34 4.30 86.8 86.0 50.0-138 0.926 20
1,2,4-Trichlorobenzene 5.00 4.38 4.12 87.6 82.4 57.0-137 6.12 20
1,1,1-Trichloroethane 5.00 5.37 5.05 107 101 73.0-124 6.14 20
1,1,2-Trichloroethane 5.00 5.74 5.68 115 114 80.0-120 1.05 20
Trichloroethene 5.00 5.88 5.62 118 112 78.0-124 4.52 20
Trichlorofluoromethane 5.00 6.03 5.83 121 117 59.0-147 3.37 20
1,2,3-Trichloropropane 5.00 5.54 5.29 111 106 73.0-130 4.62 20
1,2,4-Trimethylbenzene 5.00 5.09 4.74 102 94.8 76.0-121 7.12 20
1,3,5-Trimethylbenzene 5.00 5.27 4.93 105 98.6 76.0-122 6.67 20
Vinyl chloride 5.00 4.20 4.01 84.0 80.2 67.0-131 4.63 20
o-Xylene 5.00 5.42 5.21 108 104 80.0-122 3.95 20
m&p-Xylenes 10.0 11.9 11.5 119 115 80.0-122 3.42 20
tert-Amyl Methyl Ether 5.00 4.52 4.38 90.4 87.6 66.0-125 3.15 20
Ethyl tert-butyl ether 5.00 4.21 3.94 84.2 78.8 63.0-138 6.63 20
tert-Butyl alcohol 25.0 21.2 13.4 84.8 53.6 27.0-160 J3 45.1 30
(S) Toluene-d8 112 114 80.0-120
(S) 4-Bromofluorobenzene 95.6 95.7 77.0-126
(S) 1,2-Dichloroethane-d4 89.2 87.8 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 56 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 56 of 78
QUALITY CONTROL SUMMARYWG2024328
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1592757-14
Method Blank (MB)
(MB) R3901907-4 03/16/23 10:57
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Tetrachloroethene U 0.300 1.00
Ethanol U 42.0 100
tert-Butyl formate U 4.51 20.0
(S) Toluene-d8 106 80.0-120
(S) 4-Bromofluorobenzene 106 77.0-126
(S) 1,2-Dichloroethane-d4 115 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3901907-1 03/16/23 09:14 • (LCSD) R3901907-2 03/16/23 09:35
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Tetrachloroethene 5.00 5.23 5.23 105 105 72.0-132 0.000 20
ethanol 250 278 262 111 105 10.0-160 5.93 30
(S) Toluene-d8 103 102 80.0-120
(S) 4-Bromofluorobenzene 107 102 77.0-126
(S) 1,2-Dichloroethane-d4 116 116 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3901907-3 03/16/23 10:16
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
tert-Butyl Formate 100 131 131 10.0-160
(S) Toluene-d8 107 80.0-120
(S) 4-Bromofluorobenzene 106 77.0-126
(S) 1,2-Dichloroethane-d4 109 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 57 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 57 of 78
QUALITY CONTROL SUMMARYWG2020454
TPH by Method MADEPE L1592757-01,02,03,04,05,06,07,09,10,11,12,13
Method Blank (MB)
(MB) R3901093-1 03/14/23 13:50
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics U 33.3 100
Unadjusted C19-C36 Aliphatics U 33.3 100
(S) 1-Chloro-octadecane 91.0 40.0-140
Method Blank (MB)
(MB) R3901093-4 03/14/23 15:02
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics U 33.3 100
(S) o-Terphenyl 92.9 40.0-140
(S) 2-Fluorobiphenyl 91.6 40.0-140
(S) 2-Bromonaphthalene 100 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3901093-2 03/14/23 14:14 • (LCSD) R3901093-3 03/14/23 14:38
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 420 450 70.0 75.0 40.0-140 6.90 25
Unadjusted C19-C36 Aliphatics 800 751 764 93.9 95.5 40.0-140 1.72 25
(S) 1-Chloro-octadecane 85.8 88.6 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3901093-5 03/14/23 15:26 • (LCSD) R3901093-6 03/14/23 15:50
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1410 1430 82.9 84.1 40.0-140 1.41 25
(S) o-Terphenyl 88.9 86.8 40.0-140
(S) 2-Fluorobiphenyl 93.9 91.8 40.0-140
(S) 2-Bromonaphthalene 102 99.6 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 58 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 58 of 78
QUALITY CONTROL SUMMARYWG2022391
TPH by Method MADEPE L1592757-14
Method Blank (MB)
(MB) R3901669-1 03/15/23 13:39
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics 43.2 J 33.3 100
Unadjusted C19-C36 Aliphatics U 33.3 100
(S) 1-Chloro-octadecane 86.5 40.0-140
Method Blank (MB)
(MB) R3901669-4 03/15/23 14:45
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics 37.9 J 33.3 100
(S) o-Terphenyl 90.0 40.0-140
(S) 2-Fluorobiphenyl 91.1 40.0-140
(S) 2-Bromonaphthalene 99.6 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3901669-2 03/15/23 14:01 • (LCSD) R3901669-3 03/15/23 14:23
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 450 487 75.0 81.2 40.0-140 7.90 25
Unadjusted C19-C36 Aliphatics 800 727 761 90.9 95.1 40.0-140 4.57 25
(S) 1-Chloro-octadecane 86.1 85.1 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3901669-5 03/15/23 15:07 • (LCSD) R3901669-6 03/15/23 15:29
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1350 1390 79.4 81.8 40.0-140 2.92 25
(S) o-Terphenyl 83.9 85.0 40.0-140
(S) 2-Fluorobiphenyl 86.9 87.5 40.0-140
(S) 2-Bromonaphthalene 94.2 95.3 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 59 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 59 of 78
QUALITY CONTROL SUMMARYWG2022391
TPH by Method MADEPE L1592757-14
L1593807-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1593807-04 03/16/23 13:54 • (MS) R3901865-1 03/16/23 14:16 • (MSD) R3901865-2 03/16/23 14:38
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 570 ND 446 459 78.2 80.5 1 40.0-140 2.87 50
Unadjusted C19-C36 Aliphatics 760 ND 696 728 82.2 86.4 1 40.0-140 4.49 50
(S) 1-Chloro-octadecane 52.9 59.3 40.0-140
L1593807-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1593807-04 03/16/23 15:44 • (MS) R3901865-4 03/16/23 15:22 • (MSD) R3901865-3 03/16/23 15:00
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1620 ND 1340 1390 82.7 85.8 1 40.0-140 3.66 50
(S) o-Terphenyl 79.3 83.9 40.0-140
(S) 2-Fluorobiphenyl 92.4 93.6 40.0-140
(S) 2-Bromonaphthalene 101 102 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 60 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 60 of 78
QUALITY CONTROL SUMMARYWG2019718
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1592757-01,02,03,04,05,06,07,09
Method Blank (MB)
(MB) R3900229-2 03/10/23 16:18
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.0886 1.00
Acenaphthylene U 0.0921 1.00
Anthracene U 0.0804 1.00
Benzo(a)anthracene U 0.199 1.00
Benzo(b)fluoranthene U 0.130 1.00
Benzo(k)fluoranthene U 0.120 1.00
Benzo(g,h,i)perylene U 0.121 1.00
Benzo(a)pyrene U 0.0381 1.00
Bis(2-chlorethoxy)methane U 0.116 10.0
Bis(2-chloroethyl)ether U 0.137 10.0
2,2-oxybis(1-chloropropane)U 0.210 10.0
4-Bromophenyl-phenylether U 0.0877 10.0
2-Chloronaphthalene U 0.0648 1.00
4-Chlorophenyl-phenylether U 0.0926 10.0
Chrysene U 0.130 1.00
Dibenz(a,h)anthracene U 0.0644 1.00
3,3-Dichlorobenzidine U 0.212 10.0
2,4-Dinitrotoluene U 0.0983 10.0
2,6-Dinitrotoluene U 0.250 10.0
Fluoranthene U 0.102 1.00
Fluorene U 0.0844 1.00
Hexachlorobenzene U 0.0755 1.00
Hexachloro-1,3-butadiene U 0.0968 10.0
Hexachlorocyclopentadiene U 0.0598 10.0
Hexachloroethane U 0.127 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.143 10.0
Naphthalene U 0.159 1.00
Nitrobenzene U 0.297 10.0
n-Nitrosodimethylamine U 0.998 10.0
n-Nitrosodiphenylamine U 2.37 10.0
n-Nitrosodi-n-propylamine U 0.261 10.0
Phenanthrene U 0.112 1.00
Benzylbutyl phthalate U 0.765 3.00
Bis(2-ethylhexyl)phthalate U 0.895 3.00
Di-n-butyl phthalate U 0.453 3.00
Diethyl phthalate U 0.287 3.00
Dimethyl phthalate U 0.260 3.00
Di-n-octyl phthalate U 0.932 3.00
Pyrene U 0.107 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 61 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 61 of 78
QUALITY CONTROL SUMMARYWG2019718
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1592757-01,02,03,04,05,06,07,09
Method Blank (MB)
(MB) R3900229-2 03/10/23 16:18
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
1,2,4-Trichlorobenzene U 0.0698 10.0
4-Chloro-3-methylphenol U 0.131 10.0
2-Chlorophenol U 0.133 10.0
2,4-Dichlorophenol U 0.102 10.0
2,4-Dimethylphenol U 0.0636 10.0
4,6-Dinitro-2-methylphenol U 1.12 10.0
2,4-Dinitrophenol U 5.93 10.0
2-Nitrophenol U 0.117 10.0
4-Nitrophenol U 0.143 10.0
Pentachlorophenol U 0.313 10.0
Phenol U 4.33 10.0
2,4,6-Trichlorophenol U 0.100 10.0
(S) Nitrobenzene-d5 53.2 15.0-314
(S) 2-Fluorobiphenyl 60.7 22.0-127
(S) p-Terphenyl-d14 79.7 29.0-141
(S) Phenol-d5 16.1 8.00-424
(S) 2-Fluorophenol 27.0 10.0-120
(S) 2,4,6-Tribromophenol 66.5 10.0-153
Laboratory Control Sample (LCS)
(LCS) R3900229-1 03/10/23 15:57
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acenaphthene 50.0 36.5 73.0 47.0-145
Acenaphthylene 50.0 38.6 77.2 33.0-145
Anthracene 50.0 39.8 79.6 27.0-133
Benzo(a)anthracene 50.0 42.5 85.0 33.0-143
Benzo(b)fluoranthene 50.0 44.4 88.8 24.0-159
Benzo(k)fluoranthene 50.0 41.8 83.6 11.0-162
Benzo(g,h,i)perylene 50.0 45.8 91.6 1.00-219
Benzo(a)pyrene 50.0 46.8 93.6 17.0-163
Bis(2-chlorethoxy)methane 50.0 26.7 53.4 1.00-219
Bis(2-chloroethyl)ether 50.0 23.9 47.8 33.0-185
2,2-oxybis(1-chloropropane)50.0 26.4 52.8 36.0-166
4-Bromophenyl-phenylether 50.0 42.6 85.2 53.0-127
2-Chloronaphthalene 50.0 33.5 67.0 60.0-120
4-Chlorophenyl-phenylether 50.0 42.8 85.6 25.0-158
Chrysene 50.0 43.8 87.6 17.0-168
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 62 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 62 of 78
QUALITY CONTROL SUMMARYWG2019718
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1592757-01,02,03,04,05,06,07,09
Laboratory Control Sample (LCS)
(LCS) R3900229-1 03/10/23 15:57
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Dibenz(a,h)anthracene 50.0 46.1 92.2 1.00-227
3,3-Dichlorobenzidine 100 77.3 77.3 1.00-262
2,4-Dinitrotoluene 50.0 43.9 87.8 39.0-139
2,6-Dinitrotoluene 50.0 40.6 81.2 50.0-158
Fluoranthene 50.0 44.7 89.4 26.0-137
Fluorene 50.0 40.1 80.2 59.0-121
Hexachlorobenzene 50.0 46.7 93.4 1.00-152
Hexachloro-1,3-butadiene 50.0 28.9 57.8 24.0-120
Hexachlorocyclopentadiene 50.0 27.1 54.2 10.0-120
Hexachloroethane 50.0 22.7 45.4 40.0-120
Indeno(1,2,3-cd)pyrene 50.0 41.7 83.4 1.00-171
Isophorone 50.0 27.7 55.4 21.0-196
Naphthalene 50.0 24.5 49.0 21.0-133
Nitrobenzene 50.0 23.0 46.0 35.0-180
n-Nitrosodimethylamine 50.0 12.7 25.4 10.0-120
n-Nitrosodiphenylamine 50.0 35.5 71.0 44.0-120
n-Nitrosodi-n-propylamine 50.0 26.7 53.4 1.00-230
Phenanthrene 50.0 38.9 77.8 54.0-120
Benzylbutyl phthalate 50.0 40.1 80.2 1.00-152
Bis(2-ethylhexyl)phthalate 50.0 41.6 83.2 8.00-158
Di-n-butyl phthalate 50.0 42.9 85.8 1.00-120
Diethyl phthalate 50.0 41.9 83.8 1.00-120
Dimethyl phthalate 50.0 40.7 81.4 1.00-120
Di-n-octyl phthalate 50.0 38.0 76.0 4.00-146
Pyrene 50.0 39.1 78.2 52.0-120
1,2,4-Trichlorobenzene 50.0 26.6 53.2 44.0-142
4-Chloro-3-methylphenol 50.0 27.0 54.0 22.0-147
2-Chlorophenol 50.0 18.2 36.4 23.0-134
2,4-Dichlorophenol 50.0 24.7 49.4 39.0-135
2,4-Dimethylphenol 50.0 22.6 45.2 32.0-120
4,6-Dinitro-2-methylphenol 50.0 35.0 70.0 1.00-181
2,4-Dinitrophenol 50.0 27.7 55.4 1.00-191
2-Nitrophenol 50.0 24.5 49.0 29.0-182
4-Nitrophenol 50.0 11.8 23.6 1.00-132
Pentachlorophenol 50.0 30.1 60.2 14.0-176
Phenol 50.0 8.48 17.0 5.00-120
2,4,6-Trichlorophenol 50.0 33.3 66.6 37.0-144
(S) Nitrobenzene-d5 45.4 15.0-314
(S) 2-Fluorobiphenyl 69.1 22.0-127
(S) p-Terphenyl-d14 80.9 29.0-141
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 63 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 63 of 78
QUALITY CONTROL SUMMARYWG2019718
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1592757-01,02,03,04,05,06,07,09
Laboratory Control Sample (LCS)
(LCS) R3900229-1 03/10/23 15:57
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
(S) Phenol-d5 15.7 8.00-424
(S) 2-Fluorophenol 22.0 10.0-120
(S) 2,4,6-Tribromophenol 90.5 10.0-153
L1592728-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1592728-01 03/10/23 19:05 • (MS) R3900229-3 03/10/23 19:26 • (MSD) R3900229-4 03/10/23 19:47
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Acenaphthene 50.0 ND 33.9 35.2 67.8 70.4 1 47.0-145 3.76 48
Acenaphthylene 50.0 ND 35.0 36.6 70.0 73.2 1 33.0-145 4.47 74
Anthracene 50.0 ND 38.2 40.3 76.4 80.6 1 27.0-133 5.35 66
Benzo(a)anthracene 50.0 ND 39.1 40.2 78.2 80.4 1 33.0-143 2.77 53
Benzo(b)fluoranthene 50.0 ND 40.7 40.3 81.4 80.6 1 24.0-159 0.988 71
Benzo(k)fluoranthene 50.0 ND 37.2 39.0 74.4 78.0 1 11.0-162 4.72 63
Benzo(g,h,i)perylene 50.0 ND 39.4 40.7 78.8 81.4 1 1.00-219 3.25 97
Benzo(a)pyrene 50.0 ND 42.5 43.9 85.0 87.8 1 17.0-163 3.24 72
Bis(2-chlorethoxy)methane 50.0 ND 24.7 25.0 49.4 50.0 1 33.0-184 1.21 54
Bis(2-chloroethyl)ether 50.0 ND 22.6 21.6 45.2 43.2 1 12.0-158 4.52 108
2,2-oxybis(1-chloropropane)50.0 ND 25.1 23.5 50.2 47.0 1 36.0-166 6.58 76
4-Bromophenyl-phenylether 50.0 ND 39.5 41.0 79.0 82.0 1 53.0-127 3.73 43
2-Chloronaphthalene 50.0 ND 29.4 30.3 58.8 60.6 1 60.0-120 J6 3.02 24
4-Chlorophenyl-phenylether 50.0 ND 40.6 41.9 81.2 83.8 1 25.0-158 3.15 61
Chrysene 50.0 ND 39.2 41.3 78.4 82.6 1 17.0-168 5.22 87
Dibenz(a,h)anthracene 50.0 ND 40.7 41.1 81.4 82.2 1 1.00-227 0.978 126
3,3-Dichlorobenzidine 100 ND 66.3 71.3 66.3 71.3 1 1.00-262 7.27 108
2,4-Dinitrotoluene 50.0 ND 43.4 46.5 86.8 93.0 1 39.0-139 6.90 42
2,6-Dinitrotoluene 50.0 ND 38.8 40.3 77.6 80.6 1 50.0-158 3.79 48
Fluoranthene 50.0 ND 43.5 44.1 87.0 88.2 1 26.0-137 1.37 66
Fluorene 50.0 ND 38.3 39.7 76.6 79.4 1 59.0-121 3.59 38
Hexachlorobenzene 50.0 ND 43.0 45.3 86.0 90.6 1 1.00-152 5.21 55
Hexachloro-1,3-butadiene 50.0 ND 20.7 20.5 41.4 41.0 1 24.0-120 0.971 62
Hexachlorocyclopentadiene 50.0 ND 26.2 26.4 52.4 52.8 1 10.0-146 0.760 34
Hexachloroethane 50.0 ND 13.7 15.1 27.4 30.2 1 40.0-120 J6 J6 9.72 52
Indeno(1,2,3-cd)pyrene 50.0 ND 37.8 37.7 75.6 75.4 1 1.00-171 0.265 99
Isophorone 50.0 ND 27.0 27.6 54.0 55.2 1 21.0-196 2.20 93
Naphthalene 50.0 ND 20.9 21.8 41.8 43.6 1 21.0-133 4.22 65
Nitrobenzene 50.0 ND 21.7 20.9 43.4 41.8 1 35.0-180 3.76 62
n-Nitrosodimethylamine 50.0 ND 12.1 11.3 24.2 22.6 1 10.0-120 6.84 40
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 64 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 64 of 78
QUALITY CONTROL SUMMARYWG2019718
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1592757-01,02,03,04,05,06,07,09
L1592728-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1592728-01 03/10/23 19:05 • (MS) R3900229-3 03/10/23 19:26 • (MSD) R3900229-4 03/10/23 19:47
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
n-Nitrosodiphenylamine 50.0 ND 32.6 35.0 65.2 70.0 1 16.0-160 7.10 28
n-Nitrosodi-n-propylamine 50.0 ND 26.4 26.0 52.8 52.0 1 1.00-230 1.53 87
Phenanthrene 50.0 ND 36.1 38.5 72.2 77.0 1 54.0-120 6.43 39
Benzylbutyl phthalate 50.0 ND 36.6 37.4 73.2 74.8 1 1.00-152 2.16 60
Bis(2-ethylhexyl)phthalate 50.0 ND 39.2 39.7 78.4 79.4 1 8.00-158 1.27 82
Di-n-butyl phthalate 50.0 ND 40.5 41.9 81.0 83.8 1 1.00-120 3.40 47
Diethyl phthalate 50.0 ND 41.8 42.5 83.6 85.0 1 1.00-120 1.66 100
Dimethyl phthalate 50.0 ND 39.1 40.4 78.2 80.8 1 1.00-120 3.27 183
Di-n-octyl phthalate 50.0 ND 35.0 35.7 70.0 71.4 1 4.00-146 1.98 69
Pyrene 50.0 ND 35.1 36.4 70.2 72.8 1 52.0-120 3.64 49
1,2,4-Trichlorobenzene 50.0 ND 21.4 21.4 42.8 42.8 1 44.0-142 J6 J6 0.000 50
4-Chloro-3-methylphenol 50.0 ND 27.6 31.2 55.2 62.4 1 22.0-147 12.2 73
2-Chlorophenol 50.0 ND 19.3 18.3 38.6 36.6 1 23.0-134 5.32 61
2,4-Dichlorophenol 50.0 ND 25.6 26.6 51.2 53.2 1 39.0-135 3.83 50
2,4-Dimethylphenol 50.0 ND 22.5 23.1 45.0 46.2 1 32.0-120 2.63 58
4,6-Dinitro-2-methylphenol 50.0 ND 34.0 37.7 68.0 75.4 1 1.00-181 10.3 203
2,4-Dinitrophenol 50.0 ND 30.0 34.8 60.0 69.6 1 1.00-191 14.8 132
2-Nitrophenol 50.0 ND 24.0 24.7 48.0 49.4 1 29.0-182 2.87 55
4-Nitrophenol 50.0 ND 12.1 13.9 24.2 27.8 1 1.00-132 13.8 131
Pentachlorophenol 50.0 ND 29.9 36.5 57.1 70.3 1 14.0-176 19.9 86
Phenol 50.0 ND ND ND 17.8 15.9 1 5.00-120 11.5 64
2,4,6-Trichlorophenol 50.0 ND 30.3 33.5 60.6 67.0 1 37.0-144 10.0 58
(S) Nitrobenzene-d5 44.0 42.7 15.0-314
(S) 2-Fluorobiphenyl 62.7 65.2 22.0-127
(S) p-Terphenyl-d14 74.1 75.6 29.0-141
(S) Phenol-d5 16.8 14.8 8.00-424
(S) 2-Fluorophenol 25.7 22.9 10.0-120
(S) 2,4,6-Tribromophenol 89.0 97.5 10.0-153
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 65 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 65 of 78
QUALITY CONTROL SUMMARYWG2020599
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1592757-10,11,12,13,14
Method Blank (MB)
(MB) R3900305-3 03/11/23 15:59
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.0886 1.00
Acenaphthylene U 0.0921 1.00
Anthracene U 0.0804 1.00
Benzo(a)anthracene U 0.199 1.00
Benzo(b)fluoranthene U 0.130 1.00
Benzo(k)fluoranthene U 0.120 1.00
Benzo(g,h,i)perylene U 0.121 1.00
Benzo(a)pyrene U 0.0381 1.00
Bis(2-chlorethoxy)methane U 0.116 10.0
Bis(2-chloroethyl)ether U 0.137 10.0
2,2-oxybis(1-chloropropane)U 0.210 10.0
4-Bromophenyl-phenylether U 0.0877 10.0
2-Chloronaphthalene U 0.0648 1.00
4-Chlorophenyl-phenylether U 0.0926 10.0
Chrysene U 0.130 1.00
Dibenz(a,h)anthracene U 0.0644 1.00
3,3-Dichlorobenzidine U 0.212 10.0
2,4-Dinitrotoluene U 0.0983 10.0
2,6-Dinitrotoluene U 0.250 10.0
Fluoranthene U 0.102 1.00
Fluorene U 0.0844 1.00
Hexachlorobenzene U 0.0755 1.00
Hexachloro-1,3-butadiene U 0.0968 10.0
Hexachlorocyclopentadiene U 0.0598 10.0
Hexachloroethane U 0.127 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.143 10.0
Naphthalene U 0.159 1.00
Nitrobenzene 0.523 J 0.297 10.0
n-Nitrosodimethylamine U 0.998 10.0
n-Nitrosodiphenylamine U 2.37 10.0
n-Nitrosodi-n-propylamine U 0.261 10.0
Phenanthrene U 0.112 1.00
Benzylbutyl phthalate U 0.765 3.00
Bis(2-ethylhexyl)phthalate U 0.895 3.00
Di-n-butyl phthalate U 0.453 3.00
Diethyl phthalate U 0.287 3.00
Dimethyl phthalate U 0.260 3.00
Di-n-octyl phthalate U 0.932 3.00
Pyrene U 0.107 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 66 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 66 of 78
QUALITY CONTROL SUMMARYWG2020599
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1592757-10,11,12,13,14
Method Blank (MB)
(MB) R3900305-3 03/11/23 15:59
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
1,2,4-Trichlorobenzene U 0.0698 10.0
4-Chloro-3-methylphenol U 0.131 10.0
2-Chlorophenol U 0.133 10.0
2,4-Dichlorophenol U 0.102 10.0
2,4-Dimethylphenol U 0.0636 10.0
4,6-Dinitro-2-methylphenol U 1.12 10.0
2,4-Dinitrophenol U 5.93 10.0
2-Nitrophenol U 0.117 10.0
4-Nitrophenol U 0.143 10.0
Pentachlorophenol U 0.313 10.0
Phenol U 4.33 10.0
2,4,6-Trichlorophenol U 0.100 10.0
(S) Nitrobenzene-d5 67.0 15.0-314
(S) 2-Fluorobiphenyl 71.8 22.0-127
(S) p-Terphenyl-d14 82.3 29.0-141
(S) Phenol-d5 22.1 8.00-424
(S) 2-Fluorophenol 34.6 10.0-120
(S) 2,4,6-Tribromophenol 59.0 10.0-153
Laboratory Control Sample (LCS)
(LCS) R3900305-1 03/11/23 15:16
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acenaphthene 50.0 36.8 73.6 47.0-145
Acenaphthylene 50.0 40.2 80.4 33.0-145
Anthracene 50.0 39.0 78.0 27.0-133
Benzo(a)anthracene 50.0 39.4 78.8 33.0-143
Benzo(b)fluoranthene 50.0 40.4 80.8 24.0-159
Benzo(k)fluoranthene 50.0 37.2 74.4 11.0-162
Benzo(g,h,i)perylene 50.0 46.7 93.4 1.00-219
Benzo(a)pyrene 50.0 43.2 86.4 17.0-163
Bis(2-chlorethoxy)methane 50.0 33.4 66.8 1.00-219
Bis(2-chloroethyl)ether 50.0 37.0 74.0 33.0-185
2,2-oxybis(1-chloropropane)50.0 34.4 68.8 36.0-166
4-Bromophenyl-phenylether 50.0 36.5 73.0 53.0-127
2-Chloronaphthalene 50.0 35.1 70.2 60.0-120
4-Chlorophenyl-phenylether 50.0 34.7 69.4 25.0-158
Chrysene 50.0 39.7 79.4 17.0-168
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 67 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 67 of 78
QUALITY CONTROL SUMMARYWG2020599
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1592757-10,11,12,13,14
Laboratory Control Sample (LCS)
(LCS) R3900305-1 03/11/23 15:16
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Dibenz(a,h)anthracene 50.0 45.1 90.2 1.00-227
3,3-Dichlorobenzidine 100 75.5 75.5 1.00-262
2,4-Dinitrotoluene 50.0 44.2 88.4 39.0-139
2,6-Dinitrotoluene 50.0 39.3 78.6 50.0-158
Fluoranthene 50.0 40.2 80.4 26.0-137
Fluorene 50.0 39.1 78.2 59.0-121
Hexachlorobenzene 50.0 35.2 70.4 1.00-152
Hexachloro-1,3-butadiene 50.0 23.3 46.6 24.0-120
Hexachlorocyclopentadiene 50.0 22.4 44.8 10.0-120
Hexachloroethane 50.0 29.3 58.6 40.0-120
Indeno(1,2,3-cd)pyrene 50.0 42.7 85.4 1.00-171
Isophorone 50.0 34.8 69.6 21.0-196
Naphthalene 50.0 29.6 59.2 21.0-133
Nitrobenzene 50.0 30.1 60.2 35.0-180
n-Nitrosodimethylamine 50.0 13.9 27.8 10.0-120
n-Nitrosodiphenylamine 50.0 37.4 74.8 44.0-120
n-Nitrosodi-n-propylamine 50.0 38.0 76.0 1.00-230
Phenanthrene 50.0 37.7 75.4 54.0-120
Benzylbutyl phthalate 50.0 42.9 85.8 1.00-152
Bis(2-ethylhexyl)phthalate 50.0 42.4 84.8 8.00-158
Di-n-butyl phthalate 50.0 45.4 90.8 1.00-120
Diethyl phthalate 50.0 43.6 87.2 1.00-120
Dimethyl phthalate 50.0 38.7 77.4 1.00-120
Di-n-octyl phthalate 50.0 43.7 87.4 4.00-146
Pyrene 50.0 39.8 79.6 52.0-120
1,2,4-Trichlorobenzene 50.0 25.7 51.4 44.0-142
4-Chloro-3-methylphenol 50.0 33.5 67.0 22.0-147
2-Chlorophenol 50.0 30.2 60.4 23.0-134
2,4-Dichlorophenol 50.0 30.3 60.6 39.0-135
2,4-Dimethylphenol 50.0 29.3 58.6 32.0-120
4,6-Dinitro-2-methylphenol 50.0 37.8 75.6 1.00-181
2,4-Dinitrophenol 50.0 33.5 67.0 1.00-191
2-Nitrophenol 50.0 31.0 62.0 29.0-182
4-Nitrophenol 50.0 15.6 31.2 1.00-132
Pentachlorophenol 50.0 30.1 60.2 14.0-176
Phenol 50.0 12.1 24.2 5.00-120
2,4,6-Trichlorophenol 50.0 33.1 66.2 37.0-144
(S) Nitrobenzene-d5 57.3 15.0-314
(S) 2-Fluorobiphenyl 67.4 22.0-127
(S) p-Terphenyl-d14 74.4 29.0-141
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 68 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 68 of 78
QUALITY CONTROL SUMMARYWG2020599
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1592757-10,11,12,13,14
Laboratory Control Sample (LCS)
(LCS) R3900305-1 03/11/23 15:16
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
(S) Phenol-d5 21.8 8.00-424
(S) 2-Fluorophenol 35.1 10.0-120
(S) 2,4,6-Tribromophenol 69.5 10.0-153
L1592058-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1592058-02 03/11/23 16:42 • (MS) R3900305-4 03/11/23 17:03 • (MSD) R3900305-5 03/11/23 17:25
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Acenaphthene 45.5 ND 28.7 29.4 63.1 64.6 1 47.0-145 2.41 48
Acenaphthylene 45.5 ND 31.2 31.6 68.6 69.5 1 33.0-145 1.27 74
Anthracene 45.5 ND 31.9 30.4 70.1 66.8 1 27.0-133 4.82 66
Benzo(a)anthracene 45.5 ND 32.3 29.7 71.0 65.3 1 33.0-143 8.39 53
Benzo(b)fluoranthene 45.5 ND 33.3 31.5 73.2 69.2 1 24.0-159 5.56 71
Benzo(k)fluoranthene 45.5 ND 31.3 29.5 68.8 64.8 1 11.0-162 5.92 63
Benzo(g,h,i)perylene 45.5 ND 39.0 36.1 85.7 79.3 1 1.00-219 7.72 97
Benzo(a)pyrene 45.5 ND 35.7 33.1 78.5 72.7 1 17.0-163 7.56 72
Bis(2-chlorethoxy)methane 45.5 ND 26.4 27.3 58.0 60.0 1 33.0-184 3.35 54
Bis(2-chloroethyl)ether 45.5 ND 30.2 30.9 66.4 67.9 1 12.0-158 2.29 108
2,2-oxybis(1-chloropropane)45.5 ND 27.0 28.6 59.3 62.9 1 36.0-166 5.76 76
4-Bromophenyl-phenylether 45.5 ND 30.8 30.5 67.7 67.0 1 53.0-127 0.979 43
2-Chloronaphthalene 45.5 ND 26.7 27.2 58.7 59.8 1 60.0-120 J6 J6 1.86 24
4-Chlorophenyl-phenylether 45.5 ND 28.7 28.8 63.1 63.3 1 25.0-158 0.348 61
Chrysene 45.5 ND 32.3 29.9 71.0 65.7 1 17.0-168 7.72 87
Dibenz(a,h)anthracene 45.5 ND 37.6 34.5 82.6 75.8 1 1.00-227 8.60 126
3,3-Dichlorobenzidine 91.0 ND 58.2 59.9 64.0 65.8 1 1.00-262 2.88 108
2,4-Dinitrotoluene 45.5 ND 37.5 36.8 82.4 80.9 1 39.0-139 1.88 42
2,6-Dinitrotoluene 45.5 ND 33.0 34.0 72.5 74.7 1 50.0-158 2.99 48
Fluoranthene 45.5 ND 33.3 31.5 73.2 69.2 1 26.0-137 5.56 66
Fluorene 45.5 ND 30.7 30.7 67.5 67.5 1 59.0-121 0.000 38
Hexachlorobenzene 45.5 ND 30.2 29.3 66.4 64.4 1 1.00-152 3.03 55
Hexachloro-1,3-butadiene 45.5 ND 18.1 17.5 39.8 38.5 1 24.0-120 3.37 62
Hexachlorocyclopentadiene 45.5 ND 15.4 15.0 33.8 33.0 1 10.0-146 2.63 34
Hexachloroethane 45.5 ND 20.1 21.0 44.2 46.2 1 40.0-120 4.38 52
Indeno(1,2,3-cd)pyrene 45.5 ND 37.2 32.4 81.8 71.2 1 1.00-171 13.8 99
Isophorone 45.5 ND 28.1 29.1 61.8 64.0 1 21.0-196 3.50 93
Naphthalene 45.5 ND 22.6 23.6 49.7 51.9 1 21.0-133 4.33 65
Nitrobenzene 45.5 ND 25.3 25.6 55.6 56.3 1 35.0-180 1.18 62
n-Nitrosodimethylamine 45.5 ND 14.5 16.8 31.9 36.9 1 10.0-120 14.7 40
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 69 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 69 of 78
QUALITY CONTROL SUMMARYWG2020599
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1592757-10,11,12,13,14
L1592058-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1592058-02 03/11/23 16:42 • (MS) R3900305-4 03/11/23 17:03 • (MSD) R3900305-5 03/11/23 17:25
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
n-Nitrosodiphenylamine 45.5 ND 31.0 30.6 68.1 67.3 1 16.0-160 1.30 28
n-Nitrosodi-n-propylamine 45.5 ND 27.9 31.2 61.3 68.6 1 1.00-230 11.2 87
Phenanthrene 45.5 ND 30.9 29.1 67.9 64.0 1 54.0-120 6.00 39
Benzylbutyl phthalate 45.5 ND 35.9 36.9 78.9 81.1 1 1.00-152 2.75 60
Bis(2-ethylhexyl)phthalate 45.5 ND 34.0 31.5 74.7 69.2 1 8.00-158 7.63 82
Di-n-butyl phthalate 45.5 ND 36.9 33.1 81.1 72.7 1 1.00-120 10.9 47
Diethyl phthalate 45.5 ND 36.9 36.5 81.1 80.2 1 1.00-120 1.09 100
Dimethyl phthalate 45.5 ND 31.4 31.9 69.0 70.1 1 1.00-120 1.58 183
Di-n-octyl phthalate 45.5 ND 35.5 36.4 78.0 80.0 1 4.00-146 2.50 69
Pyrene 45.5 ND 34.2 31.4 75.2 69.0 1 52.0-120 8.54 49
1,2,4-Trichlorobenzene 45.5 ND 20.1 19.9 44.2 43.7 1 44.0-142 J6 1.00 50
4-Chloro-3-methylphenol 45.5 ND 23.5 22.6 51.6 49.7 1 22.0-147 3.90 73
2-Chlorophenol 45.5 ND 19.9 20.5 43.7 45.1 1 23.0-134 2.97 61
2,4-Dichlorophenol 45.5 ND 20.3 21.2 44.6 46.6 1 39.0-135 4.34 50
2,4-Dimethylphenol 45.5 ND 19.9 20.2 43.1 43.8 1 32.0-120 1.50 58
4,6-Dinitro-2-methylphenol 45.5 ND 28.7 28.5 63.1 62.6 1 1.00-181 0.699 203
2,4-Dinitrophenol 45.5 ND 26.4 24.5 58.0 53.8 1 1.00-191 7.47 132
2-Nitrophenol 45.5 ND 22.7 24.1 49.9 53.0 1 29.0-182 5.98 55
4-Nitrophenol 45.5 ND 12.7 11.2 27.9 24.6 1 1.00-132 12.6 131
Pentachlorophenol 45.5 ND 28.8 27.4 63.3 60.2 1 14.0-176 4.98 86
Phenol 45.5 ND 10.1 ND 22.2 21.3 1 5.00-120 4.35 64
2,4,6-Trichlorophenol 45.5 ND 23.6 25.1 51.9 55.2 1 37.0-144 6.16 58
(S) Nitrobenzene-d5 56.7 57.1 15.0-314
(S) 2-Fluorobiphenyl 60.0 61.3 22.0-127
(S) p-Terphenyl-d14 73.6 72.0 29.0-141
(S) Phenol-d5 20.6 18.8 8.00-424
(S) 2-Fluorophenol 29.9 30.1 10.0-120
(S) 2,4,6-Tribromophenol 65.4 66.5 10.0-153
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 70 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 70 of 78
GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 71 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 71 of 78

Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/17/23 17:10 72 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1592757 03/20/23 08:19 72 of 78
ANALYTICAL REPORT
June 29, 2023
S&ME Inc. - Raleigh NC
Sample Delivery Group:L1626779
Samples Received:06/16/2023
Project Number:210818
Description:Colonial Pipeline - Jennifer Drive
Report To:Mr. Michael Pfeifer
3201 Spring Forest Road
Raleigh, NC 27616
Entire Report Reviewed By:
June 29, 2023
[Preliminary Report]
Craig Cothron
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 1 of 69
June 29, 2023
Craig Cothron
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 1 of 69
TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 6
Sr: Sample Results 7
MW-2 L1626779-01 7
MW-3 L1626779-02 10
MW-5 L1626779-03 13
MW-6 L1626779-04 16
MW-7 L1626779-05 19
MW-8 L1626779-06 22
MW-9 L1626779-07 25
MW-12 L1626779-08 28
MW-13 L1626779-09 31
MW-1D L1626779-10 34
MW-4D L1626779-11 37
MW-5D L1626779-12 40
MW-6D L1626779-13 43
Qc: Quality Control Summary 46
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 46
TPH by Method MADEPE 55
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 56
Gl: Glossary of Terms 65
Al: Accreditations & Locations 66
Sc: Sample Chain of Custody 67
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 2 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 2 of 69
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-2 L1626779-01 GW J.W/L.H 06/14/23 11:15 06/16/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2082702 1 06/22/23 15:58 06/22/23 15:58 JHH Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1.03 06/22/23 11:00 06/24/23 11:41 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1.03 06/22/23 11:00 06/24/23 12:48 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2082003 1 06/21/23 16:20 06/22/23 03:20 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-3 L1626779-02 GW J.W/L.H 06/14/23 14:15 06/16/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2082702 100 06/22/23 19:24 06/22/23 19:24 JHH Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1 06/22/23 11:00 06/24/23 12:25 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1 06/22/23 11:00 06/24/23 14:00 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2082003 1 06/21/23 16:20 06/22/23 03:41 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-5 L1626779-03 GW J.W/L.H 06/14/23 13:10 06/16/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2082702 1 06/22/23 16:18 06/22/23 16:18 JHH Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1 06/22/23 11:00 06/24/23 13:09 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1 06/22/23 11:00 06/24/23 14:44 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2082003 1 06/21/23 16:20 06/22/23 04:03 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-6 L1626779-04 GW J.W/L.H 06/14/23 12:20 06/16/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2082702 1 06/22/23 16:39 06/22/23 16:39 JHH Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1.03 06/22/23 11:00 06/24/23 14:03 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1.03 06/22/23 11:00 06/24/23 15:42 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2082003 1 06/21/23 16:20 06/22/23 04:25 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-7 L1626779-05 GW J.W/L.H 06/14/23 12:50 06/16/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2082702 1 06/22/23 17:00 06/22/23 17:00 JHH Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1 06/22/23 11:00 06/24/23 15:10 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1 06/22/23 11:00 06/24/23 16:26 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2082003 1 06/21/23 16:20 06/22/23 04:47 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-8 L1626779-06 GW J.W/L.H 06/14/23 13:20 06/16/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2082702 1 06/22/23 17:20 06/22/23 17:20 JHH Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1 06/22/23 11:00 06/24/23 15:55 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1 06/22/23 11:00 06/24/23 17:11 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2082003 1 06/21/23 16:20 06/22/23 05:09 AGW Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 3 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 3 of 69
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-9 L1626779-07 GW J.W/L.H 06/14/23 13:34 06/16/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2082702 1 06/22/23 17:41 06/22/23 17:41 JHH Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1 06/22/23 11:00 06/24/23 16:39 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1 06/22/23 11:00 06/24/23 17:55 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2082003 1 06/21/23 16:20 06/22/23 05:31 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-12 L1626779-08 GW J.W/L.H 06/14/23 11:25 06/16/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2082702 1 06/22/23 18:02 06/22/23 18:02 JHH Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1 06/22/23 11:00 06/24/23 17:23 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1 06/22/23 11:00 06/24/23 18:40 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2082003 1 06/21/23 16:20 06/22/23 05:53 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-13 L1626779-09 GW J.W/L.H 06/14/23 14:00 06/16/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2082702 1 06/22/23 18:22 06/22/23 18:22 JHH Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1.03 06/22/23 11:00 06/24/23 18:07 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1.03 06/22/23 11:00 06/24/23 19:25 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2082003 1 06/21/23 16:20 06/22/23 06:15 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-1D L1626779-10 GW J.W/L.H 06/15/23 13:40 06/16/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2082702 1 06/22/23 18:43 06/22/23 18:43 JHH Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1 06/22/23 11:00 06/24/23 18:52 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1 06/22/23 11:00 06/24/23 20:09 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2082003 1 06/21/23 16:20 06/22/23 06:37 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-4D L1626779-11 GW J.W/L.H 06/15/23 12:30 06/16/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2082702 50 06/22/23 19:45 06/22/23 19:45 JHH Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1 06/22/23 11:00 06/24/23 19:36 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1 06/22/23 11:00 06/24/23 21:19 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2082003 1 06/21/23 16:20 06/22/23 06:59 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-5D L1626779-12 GW J.W/L.H 06/15/23 10:50 06/16/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2082702 1 06/22/23 19:03 06/22/23 19:03 JHH Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1 06/22/23 11:00 06/24/23 21:31 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1 06/22/23 11:00 06/24/23 22:03 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2080645 1 06/21/23 15:53 06/22/23 02:15 CCW Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 4 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 4 of 69
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-6D L1626779-13 GW J.W/L.H 06/15/23 11:50 06/16/23 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2083396 1 06/25/23 02:25 06/25/23 02:25 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2084660 1 06/28/23 12:31 06/28/23 12:31 JBE Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1 06/22/23 11:00 06/24/23 22:16 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2083284 1 06/22/23 11:00 06/24/23 22:48 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2080645 1 06/21/23 15:53 06/22/23 02:37 CCW Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 5 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 5 of 69
CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Craig Cothron
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 6 of 69
Craig Cothron
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 6 of 69
SAMPLE RESULTS - 01
L1626779
MW-2
Collected date/time: 06/14/23 11:15
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene ND 1.00 1 06/22/2023 15:58 WG2082702
Bromobenzene ND 1.00 1 06/22/2023 15:58 WG2082702
Bromodichloromethane ND 1.00 1 06/22/2023 15:58 WG2082702
Bromochloromethane ND 1.00 1 06/22/2023 15:58 WG2082702
Bromoform ND 1.00 1 06/22/2023 15:58 WG2082702
Bromomethane ND 5.00 1 06/22/2023 15:58 WG2082702
n-Butylbenzene ND 1.00 1 06/22/2023 15:58 WG2082702
sec-Butylbenzene ND 1.00 1 06/22/2023 15:58 WG2082702
tert-Butylbenzene ND 1.00 1 06/22/2023 15:58 WG2082702
Carbon tetrachloride ND 1.00 1 06/22/2023 15:58 WG2082702
Chlorobenzene ND 1.00 1 06/22/2023 15:58 WG2082702
Chlorodibromomethane ND 1.00 1 06/22/2023 15:58 WG2082702
Chloroethane ND 5.00 1 06/22/2023 15:58 WG2082702
Chloroform ND 5.00 1 06/22/2023 15:58 WG2082702
Chloromethane ND 2.50 1 06/22/2023 15:58 WG2082702
2-Chlorotoluene ND 1.00 1 06/22/2023 15:58 WG2082702
4-Chlorotoluene ND 1.00 1 06/22/2023 15:58 WG2082702
1,2-Dibromo-3-Chloropropane ND 5.00 1 06/22/2023 15:58 WG2082702
1,2-Dibromoethane ND 1.00 1 06/22/2023 15:58 WG2082702
Dibromomethane ND 1.00 1 06/22/2023 15:58 WG2082702
1,2-Dichlorobenzene ND 1.00 1 06/22/2023 15:58 WG2082702
1,3-Dichlorobenzene ND 1.00 1 06/22/2023 15:58 WG2082702
1,4-Dichlorobenzene ND 1.00 1 06/22/2023 15:58 WG2082702
Dichlorodifluoromethane ND 5.00 1 06/22/2023 15:58 WG2082702
1,1-Dichloroethane ND 1.00 1 06/22/2023 15:58 WG2082702
1,2-Dichloroethane ND 1.00 1 06/22/2023 15:58 WG2082702
1,1-Dichloroethene ND 1.00 1 06/22/2023 15:58 WG2082702
cis-1,2-Dichloroethene ND 1.00 1 06/22/2023 15:58 WG2082702
trans-1,2-Dichloroethene ND 1.00 1 06/22/2023 15:58 WG2082702
1,2-Dichloropropane ND J4 1.00 1 06/22/2023 15:58 WG2082702
1,1-Dichloropropene ND 1.00 1 06/22/2023 15:58 WG2082702
1,3-Dichloropropane ND 1.00 1 06/22/2023 15:58 WG2082702
cis-1,3-Dichloropropene ND 1.00 1 06/22/2023 15:58 WG2082702
trans-1,3-Dichloropropene ND 1.00 1 06/22/2023 15:58 WG2082702
2,2-Dichloropropane ND 1.00 1 06/22/2023 15:58 WG2082702
Di-isopropyl ether ND 1.00 1 06/22/2023 15:58 WG2082702
Ethylbenzene ND 1.00 1 06/22/2023 15:58 WG2082702
Hexachloro-1,3-butadiene ND 1.00 1 06/22/2023 15:58 WG2082702
Isopropylbenzene ND 1.00 1 06/22/2023 15:58 WG2082702
Methylene Chloride ND 5.00 1 06/22/2023 15:58 WG2082702
Methyl tert-butyl ether ND 1.00 1 06/22/2023 15:58 WG2082702
Naphthalene ND C4 5.00 1 06/22/2023 15:58 WG2082702
n-Propylbenzene ND 1.00 1 06/22/2023 15:58 WG2082702
Styrene ND 1.00 1 06/22/2023 15:58 WG2082702
1,1,1,2-Tetrachloroethane ND 1.00 1 06/22/2023 15:58 WG2082702
1,1,2,2-Tetrachloroethane ND 1.00 1 06/22/2023 15:58 WG2082702
Tetrachloroethene ND 1.00 1 06/22/2023 15:58 WG2082702
Toluene ND 1.00 1 06/22/2023 15:58 WG2082702
1,2,3-Trichlorobenzene ND 1.00 1 06/22/2023 15:58 WG2082702
1,2,4-Trichlorobenzene ND 1.00 1 06/22/2023 15:58 WG2082702
1,1,1-Trichloroethane ND 1.00 1 06/22/2023 15:58 WG2082702
1,1,2-Trichloroethane ND 1.00 1 06/22/2023 15:58 WG2082702
Trichloroethene ND 1.00 1 06/22/2023 15:58 WG2082702
Trichlorofluoromethane ND 5.00 1 06/22/2023 15:58 WG2082702
1,2,3-Trichloropropane ND 2.50 1 06/22/2023 15:58 WG2082702
1,2,4-Trimethylbenzene ND 1.00 1 06/22/2023 15:58 WG2082702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 7 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 7 of 69
SAMPLE RESULTS - 01
L1626779
MW-2
Collected date/time: 06/14/23 11:15
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 06/22/2023 15:58 WG2082702
Vinyl chloride ND 1.00 1 06/22/2023 15:58 WG2082702
o-Xylene ND 1.00 1 06/22/2023 15:58 WG2082702
m&p-Xylenes ND 2.00 1 06/22/2023 15:58 WG2082702
ethanol ND 100 1 06/22/2023 15:58 WG2082702
tert-Amyl Methyl Ether ND 1.00 1 06/22/2023 15:58 WG2082702
Ethyl tert-butyl ether ND 1.00 1 06/22/2023 15:58 WG2082702
tert-Butyl alcohol ND 5.00 1 06/22/2023 15:58 WG2082702
t-Amyl Alcohol ND 50.0 1 06/22/2023 15:58 WG2082702
tert-Butyl formate ND 20.0 1 06/22/2023 15:58 WG2082702
(S) Toluene-d8 116 80.0-120 06/22/2023 15:58 WG2082702
(S) 4-Bromofluorobenzene 93.1 77.0-126 06/22/2023 15:58 WG2082702
(S) 1,2-Dichloroethane-d4 124 70.0-130 06/22/2023 15:58 WG2082702
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 103 1.03 06/24/2023 11:41 WG2083284
Unadjusted C19-C36 Aliphatics ND 103 1.03 06/24/2023 11:41 WG2083284
Unadjusted C11-C22 Aromatics ND 103 1.03 06/24/2023 12:48 WG2083284
Unadjusted Total Petroleum
Hydrocarbons 119 103 1.03 06/24/2023 12:48 WG2083284
(S) o-Terphenyl 67.7 40.0-140 06/24/2023 12:48 WG2083284
(S) 1-Chloro-octadecane 55.0 40.0-140 06/24/2023 11:41 WG2083284
(S) 2-Fluorobiphenyl 86.0 40.0-140 06/24/2023 12:48 WG2083284
(S) 2-Bromonaphthalene 85.0 40.0-140 06/24/2023 12:48 WG2083284
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 06/22/2023 03:20 WG2082003
Acenaphthylene ND 1.00 1 06/22/2023 03:20 WG2082003
Anthracene ND 1.00 1 06/22/2023 03:20 WG2082003
Benzo(a)anthracene ND 1.00 1 06/22/2023 03:20 WG2082003
Benzo(b)fluoranthene ND 1.00 1 06/22/2023 03:20 WG2082003
Benzo(k)fluoranthene ND 1.00 1 06/22/2023 03:20 WG2082003
Benzo(g,h,i)perylene ND 1.00 1 06/22/2023 03:20 WG2082003
Benzo(a)pyrene ND 1.00 1 06/22/2023 03:20 WG2082003
Bis(2-chlorethoxy)methane ND 10.0 1 06/22/2023 03:20 WG2082003
Bis(2-chloroethyl)ether ND 10.0 1 06/22/2023 03:20 WG2082003
2,2-Oxybis(1-Chloropropane)ND 10.0 1 06/22/2023 03:20 WG2082003
4-Bromophenyl-phenylether ND 10.0 1 06/22/2023 03:20 WG2082003
2-Chloronaphthalene ND 1.00 1 06/22/2023 03:20 WG2082003
4-Chlorophenyl-phenylether ND 10.0 1 06/22/2023 03:20 WG2082003
Chrysene ND 1.00 1 06/22/2023 03:20 WG2082003
Dibenz(a,h)anthracene ND 1.00 1 06/22/2023 03:20 WG2082003
3,3-Dichlorobenzidine ND 10.0 1 06/22/2023 03:20 WG2082003
2,4-Dinitrotoluene ND 10.0 1 06/22/2023 03:20 WG2082003
2,6-Dinitrotoluene ND 10.0 1 06/22/2023 03:20 WG2082003
Fluoranthene ND 1.00 1 06/22/2023 03:20 WG2082003
Fluorene ND 1.00 1 06/22/2023 03:20 WG2082003
Hexachlorobenzene ND 1.00 1 06/22/2023 03:20 WG2082003
Hexachloro-1,3-butadiene ND 10.0 1 06/22/2023 03:20 WG2082003
Hexachlorocyclopentadiene ND 10.0 1 06/22/2023 03:20 WG2082003
Hexachloroethane ND 10.0 1 06/22/2023 03:20 WG2082003
Indeno(1,2,3-cd)pyrene ND 1.00 1 06/22/2023 03:20 WG2082003
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 8 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 8 of 69
SAMPLE RESULTS - 01
L1626779
MW-2
Collected date/time: 06/14/23 11:15
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Isophorone ND 10.0 1 06/22/2023 03:20 WG2082003
Naphthalene ND 1.00 1 06/22/2023 03:20 WG2082003
Nitrobenzene ND 10.0 1 06/22/2023 03:20 WG2082003
n-Nitrosodimethylamine ND 10.0 1 06/22/2023 03:20 WG2082003
n-Nitrosodiphenylamine ND 10.0 1 06/22/2023 03:20 WG2082003
n-Nitrosodi-n-propylamine ND 10.0 1 06/22/2023 03:20 WG2082003
Phenanthrene ND 1.00 1 06/22/2023 03:20 WG2082003
Benzylbutyl phthalate ND 3.00 1 06/22/2023 03:20 WG2082003
Bis(2-ethylhexyl)phthalate ND 3.00 1 06/22/2023 03:20 WG2082003
Di-n-butyl phthalate ND 3.00 1 06/22/2023 03:20 WG2082003
Diethyl phthalate ND 3.00 1 06/22/2023 03:20 WG2082003
Dimethyl phthalate ND 3.00 1 06/22/2023 03:20 WG2082003
Di-n-octyl phthalate ND 3.00 1 06/22/2023 03:20 WG2082003
Pyrene ND 1.00 1 06/22/2023 03:20 WG2082003
1,2,4-Trichlorobenzene ND 10.0 1 06/22/2023 03:20 WG2082003
4-Chloro-3-methylphenol ND 10.0 1 06/22/2023 03:20 WG2082003
2-Chlorophenol ND 10.0 1 06/22/2023 03:20 WG2082003
2,4-Dichlorophenol ND 10.0 1 06/22/2023 03:20 WG2082003
2,4-Dimethylphenol ND 10.0 1 06/22/2023 03:20 WG2082003
4,6-Dinitro-2-methylphenol ND 10.0 1 06/22/2023 03:20 WG2082003
2,4-Dinitrophenol ND 10.0 1 06/22/2023 03:20 WG2082003
2-Nitrophenol ND 10.0 1 06/22/2023 03:20 WG2082003
4-Nitrophenol ND 10.0 1 06/22/2023 03:20 WG2082003
Pentachlorophenol ND 10.0 1 06/22/2023 03:20 WG2082003
Phenol ND 10.0 1 06/22/2023 03:20 WG2082003
2,4,6-Trichlorophenol ND 10.0 1 06/22/2023 03:20 WG2082003
(S) Nitrobenzene-d5 78.2 15.0-314 06/22/2023 03:20 WG2082003
(S) 2-Fluorobiphenyl 48.2 22.0-127 06/22/2023 03:20 WG2082003
(S) p-Terphenyl-d14 69.4 29.0-141 06/22/2023 03:20 WG2082003
(S) Phenol-d5 20.7 8.00-424 06/22/2023 03:20 WG2082003
(S) 2-Fluorophenol 21.4 10.0-120 06/22/2023 03:20 WG2082003
(S) 2,4,6-Tribromophenol 40.6 10.0-153 06/22/2023 03:20 WG2082003
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 9 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 9 of 69
SAMPLE RESULTS - 02
L1626779
MW-3
Collected date/time: 06/14/23 14:15
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene 5060 100 100 06/22/2023 19:24 WG2082702
Bromobenzene ND 100 100 06/22/2023 19:24 WG2082702
Bromodichloromethane ND 100 100 06/22/2023 19:24 WG2082702
Bromochloromethane ND 100 100 06/22/2023 19:24 WG2082702
Bromoform ND 100 100 06/22/2023 19:24 WG2082702
Bromomethane ND 500 100 06/22/2023 19:24 WG2082702
n-Butylbenzene ND 100 100 06/22/2023 19:24 WG2082702
sec-Butylbenzene ND 100 100 06/22/2023 19:24 WG2082702
tert-Butylbenzene ND 100 100 06/22/2023 19:24 WG2082702
Carbon tetrachloride ND 100 100 06/22/2023 19:24 WG2082702
Chlorobenzene ND 100 100 06/22/2023 19:24 WG2082702
Chlorodibromomethane ND 100 100 06/22/2023 19:24 WG2082702
Chloroethane ND 500 100 06/22/2023 19:24 WG2082702
Chloroform ND 500 100 06/22/2023 19:24 WG2082702
Chloromethane ND 250 100 06/22/2023 19:24 WG2082702
2-Chlorotoluene ND 100 100 06/22/2023 19:24 WG2082702
4-Chlorotoluene ND 100 100 06/22/2023 19:24 WG2082702
1,2-Dibromo-3-Chloropropane ND 500 100 06/22/2023 19:24 WG2082702
1,2-Dibromoethane ND 100 100 06/22/2023 19:24 WG2082702
Dibromomethane ND 100 100 06/22/2023 19:24 WG2082702
1,2-Dichlorobenzene ND 100 100 06/22/2023 19:24 WG2082702
1,3-Dichlorobenzene ND 100 100 06/22/2023 19:24 WG2082702
1,4-Dichlorobenzene ND 100 100 06/22/2023 19:24 WG2082702
Dichlorodifluoromethane ND 500 100 06/22/2023 19:24 WG2082702
1,1-Dichloroethane ND 100 100 06/22/2023 19:24 WG2082702
1,2-Dichloroethane ND 100 100 06/22/2023 19:24 WG2082702
1,1-Dichloroethene ND 100 100 06/22/2023 19:24 WG2082702
cis-1,2-Dichloroethene ND 100 100 06/22/2023 19:24 WG2082702
trans-1,2-Dichloroethene ND 100 100 06/22/2023 19:24 WG2082702
1,2-Dichloropropane ND J4 100 100 06/22/2023 19:24 WG2082702
1,1-Dichloropropene ND 100 100 06/22/2023 19:24 WG2082702
1,3-Dichloropropane ND 100 100 06/22/2023 19:24 WG2082702
cis-1,3-Dichloropropene ND 100 100 06/22/2023 19:24 WG2082702
trans-1,3-Dichloropropene ND 100 100 06/22/2023 19:24 WG2082702
2,2-Dichloropropane ND 100 100 06/22/2023 19:24 WG2082702
Di-isopropyl ether ND 100 100 06/22/2023 19:24 WG2082702
Ethylbenzene 706 100 100 06/22/2023 19:24 WG2082702
Hexachloro-1,3-butadiene ND 100 100 06/22/2023 19:24 WG2082702
Isopropylbenzene ND 100 100 06/22/2023 19:24 WG2082702
Methylene Chloride ND 500 100 06/22/2023 19:24 WG2082702
Methyl tert-butyl ether ND 100 100 06/22/2023 19:24 WG2082702
Naphthalene ND C4 500 100 06/22/2023 19:24 WG2082702
n-Propylbenzene ND 100 100 06/22/2023 19:24 WG2082702
Styrene ND 100 100 06/22/2023 19:24 WG2082702
1,1,1,2-Tetrachloroethane ND 100 100 06/22/2023 19:24 WG2082702
1,1,2,2-Tetrachloroethane ND 100 100 06/22/2023 19:24 WG2082702
Tetrachloroethene ND 100 100 06/22/2023 19:24 WG2082702
Toluene 10400 100 100 06/22/2023 19:24 WG2082702
1,2,3-Trichlorobenzene ND 100 100 06/22/2023 19:24 WG2082702
1,2,4-Trichlorobenzene ND 100 100 06/22/2023 19:24 WG2082702
1,1,1-Trichloroethane ND 100 100 06/22/2023 19:24 WG2082702
1,1,2-Trichloroethane ND 100 100 06/22/2023 19:24 WG2082702
Trichloroethene ND 100 100 06/22/2023 19:24 WG2082702
Trichlorofluoromethane ND 500 100 06/22/2023 19:24 WG2082702
1,2,3-Trichloropropane ND 250 100 06/22/2023 19:24 WG2082702
1,2,4-Trimethylbenzene 645 100 100 06/22/2023 19:24 WG2082702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 10 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 10 of 69
SAMPLE RESULTS - 02
L1626779
MW-3
Collected date/time: 06/14/23 14:15
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene 165 100 100 06/22/2023 19:24 WG2082702
Vinyl chloride ND 100 100 06/22/2023 19:24 WG2082702
o-Xylene 1720 100 100 06/22/2023 19:24 WG2082702
m&p-Xylenes 3550 200 100 06/22/2023 19:24 WG2082702
ethanol ND 10000 100 06/22/2023 19:24 WG2082702
tert-Amyl Methyl Ether ND 100 100 06/22/2023 19:24 WG2082702
Ethyl tert-butyl ether ND 100 100 06/22/2023 19:24 WG2082702
tert-Butyl alcohol ND 500 100 06/22/2023 19:24 WG2082702
t-Amyl Alcohol 5570 5000 100 06/22/2023 19:24 WG2082702
tert-Butyl formate ND 2000 100 06/22/2023 19:24 WG2082702
(S) Toluene-d8 114 80.0-120 06/22/2023 19:24 WG2082702
(S) 4-Bromofluorobenzene 95.3 77.0-126 06/22/2023 19:24 WG2082702
(S) 1,2-Dichloroethane-d4 124 70.0-130 06/22/2023 19:24 WG2082702
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 06/24/2023 12:25 WG2083284
Unadjusted C19-C36 Aliphatics ND 100 1 06/24/2023 12:25 WG2083284
Unadjusted C11-C22 Aromatics 371 100 1 06/24/2023 14:00 WG2083284
Unadjusted Total Petroleum
Hydrocarbons 408 100 1 06/24/2023 14:00 WG2083284
(S) o-Terphenyl 71.4 40.0-140 06/24/2023 14:00 WG2083284
(S) 1-Chloro-octadecane 62.3 40.0-140 06/24/2023 12:25 WG2083284
(S) 2-Fluorobiphenyl 89.6 40.0-140 06/24/2023 14:00 WG2083284
(S) 2-Bromonaphthalene 90.0 40.0-140 06/24/2023 14:00 WG2083284
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 06/22/2023 03:41 WG2082003
Acenaphthylene ND 1.00 1 06/22/2023 03:41 WG2082003
Anthracene ND 1.00 1 06/22/2023 03:41 WG2082003
Benzo(a)anthracene ND 1.00 1 06/22/2023 03:41 WG2082003
Benzo(b)fluoranthene ND 1.00 1 06/22/2023 03:41 WG2082003
Benzo(k)fluoranthene ND 1.00 1 06/22/2023 03:41 WG2082003
Benzo(g,h,i)perylene ND 1.00 1 06/22/2023 03:41 WG2082003
Benzo(a)pyrene ND 1.00 1 06/22/2023 03:41 WG2082003
Bis(2-chlorethoxy)methane ND 10.0 1 06/22/2023 03:41 WG2082003
Bis(2-chloroethyl)ether ND 10.0 1 06/22/2023 03:41 WG2082003
2,2-Oxybis(1-Chloropropane)ND 10.0 1 06/22/2023 03:41 WG2082003
4-Bromophenyl-phenylether ND 10.0 1 06/22/2023 03:41 WG2082003
2-Chloronaphthalene ND 1.00 1 06/22/2023 03:41 WG2082003
4-Chlorophenyl-phenylether ND 10.0 1 06/22/2023 03:41 WG2082003
Chrysene ND 1.00 1 06/22/2023 03:41 WG2082003
Dibenz(a,h)anthracene ND 1.00 1 06/22/2023 03:41 WG2082003
3,3-Dichlorobenzidine ND 10.0 1 06/22/2023 03:41 WG2082003
2,4-Dinitrotoluene ND 10.0 1 06/22/2023 03:41 WG2082003
2,6-Dinitrotoluene ND 10.0 1 06/22/2023 03:41 WG2082003
Fluoranthene ND 1.00 1 06/22/2023 03:41 WG2082003
Fluorene ND 1.00 1 06/22/2023 03:41 WG2082003
Hexachlorobenzene ND 1.00 1 06/22/2023 03:41 WG2082003
Hexachloro-1,3-butadiene ND 10.0 1 06/22/2023 03:41 WG2082003
Hexachlorocyclopentadiene ND 10.0 1 06/22/2023 03:41 WG2082003
Hexachloroethane ND 10.0 1 06/22/2023 03:41 WG2082003
Indeno(1,2,3-cd)pyrene ND 1.00 1 06/22/2023 03:41 WG2082003
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 11 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 11 of 69
SAMPLE RESULTS - 02
L1626779
MW-3
Collected date/time: 06/14/23 14:15
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Isophorone ND 10.0 1 06/22/2023 03:41 WG2082003
Naphthalene 68.9 1.00 1 06/22/2023 03:41 WG2082003
Nitrobenzene ND 10.0 1 06/22/2023 03:41 WG2082003
n-Nitrosodimethylamine ND 10.0 1 06/22/2023 03:41 WG2082003
n-Nitrosodiphenylamine ND 10.0 1 06/22/2023 03:41 WG2082003
n-Nitrosodi-n-propylamine ND 10.0 1 06/22/2023 03:41 WG2082003
Phenanthrene ND 1.00 1 06/22/2023 03:41 WG2082003
Benzylbutyl phthalate ND 3.00 1 06/22/2023 03:41 WG2082003
Bis(2-ethylhexyl)phthalate ND 3.00 1 06/22/2023 03:41 WG2082003
Di-n-butyl phthalate ND 3.00 1 06/22/2023 03:41 WG2082003
Diethyl phthalate ND 3.00 1 06/22/2023 03:41 WG2082003
Dimethyl phthalate ND 3.00 1 06/22/2023 03:41 WG2082003
Di-n-octyl phthalate ND 3.00 1 06/22/2023 03:41 WG2082003
Pyrene ND 1.00 1 06/22/2023 03:41 WG2082003
1,2,4-Trichlorobenzene ND 10.0 1 06/22/2023 03:41 WG2082003
4-Chloro-3-methylphenol ND 10.0 1 06/22/2023 03:41 WG2082003
2-Chlorophenol ND 10.0 1 06/22/2023 03:41 WG2082003
2,4-Dichlorophenol ND 10.0 1 06/22/2023 03:41 WG2082003
2,4-Dimethylphenol ND 10.0 1 06/22/2023 03:41 WG2082003
4,6-Dinitro-2-methylphenol ND 10.0 1 06/22/2023 03:41 WG2082003
2,4-Dinitrophenol ND 10.0 1 06/22/2023 03:41 WG2082003
2-Nitrophenol ND 10.0 1 06/22/2023 03:41 WG2082003
4-Nitrophenol ND 10.0 1 06/22/2023 03:41 WG2082003
Pentachlorophenol ND 10.0 1 06/22/2023 03:41 WG2082003
Phenol ND 10.0 1 06/22/2023 03:41 WG2082003
2,4,6-Trichlorophenol ND 10.0 1 06/22/2023 03:41 WG2082003
(S) Nitrobenzene-d5 81.4 15.0-314 06/22/2023 03:41 WG2082003
(S) 2-Fluorobiphenyl 46.4 22.0-127 06/22/2023 03:41 WG2082003
(S) p-Terphenyl-d14 65.4 29.0-141 06/22/2023 03:41 WG2082003
(S) Phenol-d5 24.8 8.00-424 06/22/2023 03:41 WG2082003
(S) 2-Fluorophenol 13.9 10.0-120 06/22/2023 03:41 WG2082003
(S) 2,4,6-Tribromophenol 37.7 10.0-153 06/22/2023 03:41 WG2082003
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 12 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 12 of 69
SAMPLE RESULTS - 03
L1626779
MW-5
Collected date/time: 06/14/23 13:10
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene ND 1.00 1 06/22/2023 16:18 WG2082702
Bromobenzene ND 1.00 1 06/22/2023 16:18 WG2082702
Bromodichloromethane ND 1.00 1 06/22/2023 16:18 WG2082702
Bromochloromethane ND 1.00 1 06/22/2023 16:18 WG2082702
Bromoform ND 1.00 1 06/22/2023 16:18 WG2082702
Bromomethane ND 5.00 1 06/22/2023 16:18 WG2082702
n-Butylbenzene ND 1.00 1 06/22/2023 16:18 WG2082702
sec-Butylbenzene ND 1.00 1 06/22/2023 16:18 WG2082702
tert-Butylbenzene ND 1.00 1 06/22/2023 16:18 WG2082702
Carbon tetrachloride ND 1.00 1 06/22/2023 16:18 WG2082702
Chlorobenzene ND 1.00 1 06/22/2023 16:18 WG2082702
Chlorodibromomethane ND 1.00 1 06/22/2023 16:18 WG2082702
Chloroethane ND 5.00 1 06/22/2023 16:18 WG2082702
Chloroform ND 5.00 1 06/22/2023 16:18 WG2082702
Chloromethane ND 2.50 1 06/22/2023 16:18 WG2082702
2-Chlorotoluene ND 1.00 1 06/22/2023 16:18 WG2082702
4-Chlorotoluene ND 1.00 1 06/22/2023 16:18 WG2082702
1,2-Dibromo-3-Chloropropane ND 5.00 1 06/22/2023 16:18 WG2082702
1,2-Dibromoethane ND 1.00 1 06/22/2023 16:18 WG2082702
Dibromomethane ND 1.00 1 06/22/2023 16:18 WG2082702
1,2-Dichlorobenzene ND 1.00 1 06/22/2023 16:18 WG2082702
1,3-Dichlorobenzene ND 1.00 1 06/22/2023 16:18 WG2082702
1,4-Dichlorobenzene ND 1.00 1 06/22/2023 16:18 WG2082702
Dichlorodifluoromethane ND 5.00 1 06/22/2023 16:18 WG2082702
1,1-Dichloroethane ND 1.00 1 06/22/2023 16:18 WG2082702
1,2-Dichloroethane ND 1.00 1 06/22/2023 16:18 WG2082702
1,1-Dichloroethene ND 1.00 1 06/22/2023 16:18 WG2082702
cis-1,2-Dichloroethene ND 1.00 1 06/22/2023 16:18 WG2082702
trans-1,2-Dichloroethene ND 1.00 1 06/22/2023 16:18 WG2082702
1,2-Dichloropropane ND J4 1.00 1 06/22/2023 16:18 WG2082702
1,1-Dichloropropene ND 1.00 1 06/22/2023 16:18 WG2082702
1,3-Dichloropropane ND 1.00 1 06/22/2023 16:18 WG2082702
cis-1,3-Dichloropropene ND 1.00 1 06/22/2023 16:18 WG2082702
trans-1,3-Dichloropropene ND 1.00 1 06/22/2023 16:18 WG2082702
2,2-Dichloropropane ND 1.00 1 06/22/2023 16:18 WG2082702
Di-isopropyl ether ND 1.00 1 06/22/2023 16:18 WG2082702
Ethylbenzene ND 1.00 1 06/22/2023 16:18 WG2082702
Hexachloro-1,3-butadiene ND 1.00 1 06/22/2023 16:18 WG2082702
Isopropylbenzene ND 1.00 1 06/22/2023 16:18 WG2082702
Methylene Chloride ND 5.00 1 06/22/2023 16:18 WG2082702
Methyl tert-butyl ether ND 1.00 1 06/22/2023 16:18 WG2082702
Naphthalene ND C4 5.00 1 06/22/2023 16:18 WG2082702
n-Propylbenzene ND 1.00 1 06/22/2023 16:18 WG2082702
Styrene ND 1.00 1 06/22/2023 16:18 WG2082702
1,1,1,2-Tetrachloroethane ND 1.00 1 06/22/2023 16:18 WG2082702
1,1,2,2-Tetrachloroethane ND 1.00 1 06/22/2023 16:18 WG2082702
Tetrachloroethene ND 1.00 1 06/22/2023 16:18 WG2082702
Toluene ND 1.00 1 06/22/2023 16:18 WG2082702
1,2,3-Trichlorobenzene ND 1.00 1 06/22/2023 16:18 WG2082702
1,2,4-Trichlorobenzene ND 1.00 1 06/22/2023 16:18 WG2082702
1,1,1-Trichloroethane ND 1.00 1 06/22/2023 16:18 WG2082702
1,1,2-Trichloroethane ND 1.00 1 06/22/2023 16:18 WG2082702
Trichloroethene ND 1.00 1 06/22/2023 16:18 WG2082702
Trichlorofluoromethane ND 5.00 1 06/22/2023 16:18 WG2082702
1,2,3-Trichloropropane ND 2.50 1 06/22/2023 16:18 WG2082702
1,2,4-Trimethylbenzene ND 1.00 1 06/22/2023 16:18 WG2082702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 13 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 13 of 69
SAMPLE RESULTS - 03
L1626779
MW-5
Collected date/time: 06/14/23 13:10
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 06/22/2023 16:18 WG2082702
Vinyl chloride ND 1.00 1 06/22/2023 16:18 WG2082702
o-Xylene ND 1.00 1 06/22/2023 16:18 WG2082702
m&p-Xylenes ND 2.00 1 06/22/2023 16:18 WG2082702
ethanol ND 100 1 06/22/2023 16:18 WG2082702
tert-Amyl Methyl Ether ND 1.00 1 06/22/2023 16:18 WG2082702
Ethyl tert-butyl ether ND 1.00 1 06/22/2023 16:18 WG2082702
tert-Butyl alcohol ND 5.00 1 06/22/2023 16:18 WG2082702
t-Amyl Alcohol ND 50.0 1 06/22/2023 16:18 WG2082702
tert-Butyl formate ND 20.0 1 06/22/2023 16:18 WG2082702
(S) Toluene-d8 118 80.0-120 06/22/2023 16:18 WG2082702
(S) 4-Bromofluorobenzene 90.4 77.0-126 06/22/2023 16:18 WG2082702
(S) 1,2-Dichloroethane-d4 119 70.0-130 06/22/2023 16:18 WG2082702
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 06/24/2023 13:09 WG2083284
Unadjusted C19-C36 Aliphatics ND 100 1 06/24/2023 13:09 WG2083284
Unadjusted C11-C22 Aromatics ND 100 1 06/24/2023 14:44 WG2083284
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 06/24/2023 14:44 WG2083284
(S) o-Terphenyl 62.1 40.0-140 06/24/2023 14:44 WG2083284
(S) 1-Chloro-octadecane 59.9 40.0-140 06/24/2023 13:09 WG2083284
(S) 2-Fluorobiphenyl 79.3 40.0-140 06/24/2023 14:44 WG2083284
(S) 2-Bromonaphthalene 76.9 40.0-140 06/24/2023 14:44 WG2083284
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 06/22/2023 04:03 WG2082003
Acenaphthylene ND 1.00 1 06/22/2023 04:03 WG2082003
Anthracene ND 1.00 1 06/22/2023 04:03 WG2082003
Benzo(a)anthracene ND 1.00 1 06/22/2023 04:03 WG2082003
Benzo(b)fluoranthene ND 1.00 1 06/22/2023 04:03 WG2082003
Benzo(k)fluoranthene ND 1.00 1 06/22/2023 04:03 WG2082003
Benzo(g,h,i)perylene ND 1.00 1 06/22/2023 04:03 WG2082003
Benzo(a)pyrene ND 1.00 1 06/22/2023 04:03 WG2082003
Bis(2-chlorethoxy)methane ND 10.0 1 06/22/2023 04:03 WG2082003
Bis(2-chloroethyl)ether ND 10.0 1 06/22/2023 04:03 WG2082003
2,2-Oxybis(1-Chloropropane)ND 10.0 1 06/22/2023 04:03 WG2082003
4-Bromophenyl-phenylether ND 10.0 1 06/22/2023 04:03 WG2082003
2-Chloronaphthalene ND 1.00 1 06/22/2023 04:03 WG2082003
4-Chlorophenyl-phenylether ND 10.0 1 06/22/2023 04:03 WG2082003
Chrysene ND 1.00 1 06/22/2023 04:03 WG2082003
Dibenz(a,h)anthracene ND 1.00 1 06/22/2023 04:03 WG2082003
3,3-Dichlorobenzidine ND 10.0 1 06/22/2023 04:03 WG2082003
2,4-Dinitrotoluene ND 10.0 1 06/22/2023 04:03 WG2082003
2,6-Dinitrotoluene ND 10.0 1 06/22/2023 04:03 WG2082003
Fluoranthene ND 1.00 1 06/22/2023 04:03 WG2082003
Fluorene ND 1.00 1 06/22/2023 04:03 WG2082003
Hexachlorobenzene ND 1.00 1 06/22/2023 04:03 WG2082003
Hexachloro-1,3-butadiene ND 10.0 1 06/22/2023 04:03 WG2082003
Hexachlorocyclopentadiene ND 10.0 1 06/22/2023 04:03 WG2082003
Hexachloroethane ND 10.0 1 06/22/2023 04:03 WG2082003
Indeno(1,2,3-cd)pyrene ND 1.00 1 06/22/2023 04:03 WG2082003
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 14 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 14 of 69
SAMPLE RESULTS - 03
L1626779
MW-5
Collected date/time: 06/14/23 13:10
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Isophorone ND 10.0 1 06/22/2023 04:03 WG2082003
Naphthalene ND 1.00 1 06/22/2023 04:03 WG2082003
Nitrobenzene ND 10.0 1 06/22/2023 04:03 WG2082003
n-Nitrosodimethylamine ND 10.0 1 06/22/2023 04:03 WG2082003
n-Nitrosodiphenylamine ND 10.0 1 06/22/2023 04:03 WG2082003
n-Nitrosodi-n-propylamine ND 10.0 1 06/22/2023 04:03 WG2082003
Phenanthrene ND 1.00 1 06/22/2023 04:03 WG2082003
Benzylbutyl phthalate ND 3.00 1 06/22/2023 04:03 WG2082003
Bis(2-ethylhexyl)phthalate ND 3.00 1 06/22/2023 04:03 WG2082003
Di-n-butyl phthalate ND 3.00 1 06/22/2023 04:03 WG2082003
Diethyl phthalate ND 3.00 1 06/22/2023 04:03 WG2082003
Dimethyl phthalate ND 3.00 1 06/22/2023 04:03 WG2082003
Di-n-octyl phthalate ND 3.00 1 06/22/2023 04:03 WG2082003
Pyrene ND 1.00 1 06/22/2023 04:03 WG2082003
1,2,4-Trichlorobenzene ND 10.0 1 06/22/2023 04:03 WG2082003
4-Chloro-3-methylphenol ND 10.0 1 06/22/2023 04:03 WG2082003
2-Chlorophenol ND 10.0 1 06/22/2023 04:03 WG2082003
2,4-Dichlorophenol ND 10.0 1 06/22/2023 04:03 WG2082003
2,4-Dimethylphenol ND 10.0 1 06/22/2023 04:03 WG2082003
4,6-Dinitro-2-methylphenol ND 10.0 1 06/22/2023 04:03 WG2082003
2,4-Dinitrophenol ND 10.0 1 06/22/2023 04:03 WG2082003
2-Nitrophenol ND 10.0 1 06/22/2023 04:03 WG2082003
4-Nitrophenol ND 10.0 1 06/22/2023 04:03 WG2082003
Pentachlorophenol ND 10.0 1 06/22/2023 04:03 WG2082003
Phenol ND 10.0 1 06/22/2023 04:03 WG2082003
2,4,6-Trichlorophenol ND 10.0 1 06/22/2023 04:03 WG2082003
(S) Nitrobenzene-d5 75.0 15.0-314 06/22/2023 04:03 WG2082003
(S) 2-Fluorobiphenyl 42.8 22.0-127 06/22/2023 04:03 WG2082003
(S) p-Terphenyl-d14 79.8 29.0-141 06/22/2023 04:03 WG2082003
(S) Phenol-d5 22.8 8.00-424 06/22/2023 04:03 WG2082003
(S) 2-Fluorophenol 21.6 10.0-120 06/22/2023 04:03 WG2082003
(S) 2,4,6-Tribromophenol 34.0 10.0-153 06/22/2023 04:03 WG2082003
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 15 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 15 of 69
SAMPLE RESULTS - 04
L1626779
MW-6
Collected date/time: 06/14/23 12:20
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene ND 1.00 1 06/22/2023 16:39 WG2082702
Bromobenzene ND 1.00 1 06/22/2023 16:39 WG2082702
Bromodichloromethane ND 1.00 1 06/22/2023 16:39 WG2082702
Bromochloromethane ND 1.00 1 06/22/2023 16:39 WG2082702
Bromoform ND 1.00 1 06/22/2023 16:39 WG2082702
Bromomethane ND 5.00 1 06/22/2023 16:39 WG2082702
n-Butylbenzene ND 1.00 1 06/22/2023 16:39 WG2082702
sec-Butylbenzene ND 1.00 1 06/22/2023 16:39 WG2082702
tert-Butylbenzene ND 1.00 1 06/22/2023 16:39 WG2082702
Carbon tetrachloride ND 1.00 1 06/22/2023 16:39 WG2082702
Chlorobenzene ND 1.00 1 06/22/2023 16:39 WG2082702
Chlorodibromomethane ND 1.00 1 06/22/2023 16:39 WG2082702
Chloroethane ND 5.00 1 06/22/2023 16:39 WG2082702
Chloroform ND 5.00 1 06/22/2023 16:39 WG2082702
Chloromethane ND 2.50 1 06/22/2023 16:39 WG2082702
2-Chlorotoluene ND 1.00 1 06/22/2023 16:39 WG2082702
4-Chlorotoluene ND 1.00 1 06/22/2023 16:39 WG2082702
1,2-Dibromo-3-Chloropropane ND 5.00 1 06/22/2023 16:39 WG2082702
1,2-Dibromoethane ND 1.00 1 06/22/2023 16:39 WG2082702
Dibromomethane ND 1.00 1 06/22/2023 16:39 WG2082702
1,2-Dichlorobenzene ND 1.00 1 06/22/2023 16:39 WG2082702
1,3-Dichlorobenzene ND 1.00 1 06/22/2023 16:39 WG2082702
1,4-Dichlorobenzene ND 1.00 1 06/22/2023 16:39 WG2082702
Dichlorodifluoromethane ND 5.00 1 06/22/2023 16:39 WG2082702
1,1-Dichloroethane ND 1.00 1 06/22/2023 16:39 WG2082702
1,2-Dichloroethane ND 1.00 1 06/22/2023 16:39 WG2082702
1,1-Dichloroethene ND 1.00 1 06/22/2023 16:39 WG2082702
cis-1,2-Dichloroethene ND 1.00 1 06/22/2023 16:39 WG2082702
trans-1,2-Dichloroethene ND 1.00 1 06/22/2023 16:39 WG2082702
1,2-Dichloropropane ND J4 1.00 1 06/22/2023 16:39 WG2082702
1,1-Dichloropropene ND 1.00 1 06/22/2023 16:39 WG2082702
1,3-Dichloropropane ND 1.00 1 06/22/2023 16:39 WG2082702
cis-1,3-Dichloropropene ND 1.00 1 06/22/2023 16:39 WG2082702
trans-1,3-Dichloropropene ND 1.00 1 06/22/2023 16:39 WG2082702
2,2-Dichloropropane ND 1.00 1 06/22/2023 16:39 WG2082702
Di-isopropyl ether ND 1.00 1 06/22/2023 16:39 WG2082702
Ethylbenzene ND 1.00 1 06/22/2023 16:39 WG2082702
Hexachloro-1,3-butadiene ND 1.00 1 06/22/2023 16:39 WG2082702
Isopropylbenzene ND 1.00 1 06/22/2023 16:39 WG2082702
Methylene Chloride ND 5.00 1 06/22/2023 16:39 WG2082702
Methyl tert-butyl ether ND 1.00 1 06/22/2023 16:39 WG2082702
Naphthalene ND C4 5.00 1 06/22/2023 16:39 WG2082702
n-Propylbenzene ND 1.00 1 06/22/2023 16:39 WG2082702
Styrene ND 1.00 1 06/22/2023 16:39 WG2082702
1,1,1,2-Tetrachloroethane ND 1.00 1 06/22/2023 16:39 WG2082702
1,1,2,2-Tetrachloroethane ND 1.00 1 06/22/2023 16:39 WG2082702
Tetrachloroethene ND 1.00 1 06/22/2023 16:39 WG2082702
Toluene ND 1.00 1 06/22/2023 16:39 WG2082702
1,2,3-Trichlorobenzene ND 1.00 1 06/22/2023 16:39 WG2082702
1,2,4-Trichlorobenzene ND 1.00 1 06/22/2023 16:39 WG2082702
1,1,1-Trichloroethane ND 1.00 1 06/22/2023 16:39 WG2082702
1,1,2-Trichloroethane ND 1.00 1 06/22/2023 16:39 WG2082702
Trichloroethene ND 1.00 1 06/22/2023 16:39 WG2082702
Trichlorofluoromethane ND 5.00 1 06/22/2023 16:39 WG2082702
1,2,3-Trichloropropane ND 2.50 1 06/22/2023 16:39 WG2082702
1,2,4-Trimethylbenzene ND 1.00 1 06/22/2023 16:39 WG2082702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 16 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 16 of 69
SAMPLE RESULTS - 04
L1626779
MW-6
Collected date/time: 06/14/23 12:20
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 06/22/2023 16:39 WG2082702
Vinyl chloride ND 1.00 1 06/22/2023 16:39 WG2082702
o-Xylene ND 1.00 1 06/22/2023 16:39 WG2082702
m&p-Xylenes ND 2.00 1 06/22/2023 16:39 WG2082702
ethanol ND 100 1 06/22/2023 16:39 WG2082702
tert-Amyl Methyl Ether ND 1.00 1 06/22/2023 16:39 WG2082702
Ethyl tert-butyl ether ND 1.00 1 06/22/2023 16:39 WG2082702
tert-Butyl alcohol ND 5.00 1 06/22/2023 16:39 WG2082702
t-Amyl Alcohol ND 50.0 1 06/22/2023 16:39 WG2082702
tert-Butyl formate ND 20.0 1 06/22/2023 16:39 WG2082702
(S) Toluene-d8 120 80.0-120 06/22/2023 16:39 WG2082702
(S) 4-Bromofluorobenzene 92.4 77.0-126 06/22/2023 16:39 WG2082702
(S) 1,2-Dichloroethane-d4 123 70.0-130 06/22/2023 16:39 WG2082702
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 103 1.03 06/24/2023 14:03 WG2083284
Unadjusted C19-C36 Aliphatics ND 103 1.03 06/24/2023 14:03 WG2083284
Unadjusted C11-C22 Aromatics ND 103 1.03 06/24/2023 15:42 WG2083284
Unadjusted Total Petroleum
Hydrocarbons ND 103 1.03 06/24/2023 15:42 WG2083284
(S) o-Terphenyl 58.3 40.0-140 06/24/2023 15:42 WG2083284
(S) 1-Chloro-octadecane 42.7 40.0-140 06/24/2023 14:03 WG2083284
(S) 2-Fluorobiphenyl 81.2 40.0-140 06/24/2023 15:42 WG2083284
(S) 2-Bromonaphthalene 79.9 40.0-140 06/24/2023 15:42 WG2083284
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 06/22/2023 04:25 WG2082003
Acenaphthylene ND 1.00 1 06/22/2023 04:25 WG2082003
Anthracene ND 1.00 1 06/22/2023 04:25 WG2082003
Benzo(a)anthracene ND 1.00 1 06/22/2023 04:25 WG2082003
Benzo(b)fluoranthene ND 1.00 1 06/22/2023 04:25 WG2082003
Benzo(k)fluoranthene ND 1.00 1 06/22/2023 04:25 WG2082003
Benzo(g,h,i)perylene ND 1.00 1 06/22/2023 04:25 WG2082003
Benzo(a)pyrene ND 1.00 1 06/22/2023 04:25 WG2082003
Bis(2-chlorethoxy)methane ND 10.0 1 06/22/2023 04:25 WG2082003
Bis(2-chloroethyl)ether ND 10.0 1 06/22/2023 04:25 WG2082003
2,2-Oxybis(1-Chloropropane)ND 10.0 1 06/22/2023 04:25 WG2082003
4-Bromophenyl-phenylether ND 10.0 1 06/22/2023 04:25 WG2082003
2-Chloronaphthalene ND 1.00 1 06/22/2023 04:25 WG2082003
4-Chlorophenyl-phenylether ND 10.0 1 06/22/2023 04:25 WG2082003
Chrysene ND 1.00 1 06/22/2023 04:25 WG2082003
Dibenz(a,h)anthracene ND 1.00 1 06/22/2023 04:25 WG2082003
3,3-Dichlorobenzidine ND 10.0 1 06/22/2023 04:25 WG2082003
2,4-Dinitrotoluene ND 10.0 1 06/22/2023 04:25 WG2082003
2,6-Dinitrotoluene ND 10.0 1 06/22/2023 04:25 WG2082003
Fluoranthene ND 1.00 1 06/22/2023 04:25 WG2082003
Fluorene ND 1.00 1 06/22/2023 04:25 WG2082003
Hexachlorobenzene ND 1.00 1 06/22/2023 04:25 WG2082003
Hexachloro-1,3-butadiene ND 10.0 1 06/22/2023 04:25 WG2082003
Hexachlorocyclopentadiene ND 10.0 1 06/22/2023 04:25 WG2082003
Hexachloroethane ND 10.0 1 06/22/2023 04:25 WG2082003
Indeno(1,2,3-cd)pyrene ND 1.00 1 06/22/2023 04:25 WG2082003
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 17 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 17 of 69
SAMPLE RESULTS - 04
L1626779
MW-6
Collected date/time: 06/14/23 12:20
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Isophorone ND 10.0 1 06/22/2023 04:25 WG2082003
Naphthalene ND 1.00 1 06/22/2023 04:25 WG2082003
Nitrobenzene ND 10.0 1 06/22/2023 04:25 WG2082003
n-Nitrosodimethylamine ND 10.0 1 06/22/2023 04:25 WG2082003
n-Nitrosodiphenylamine ND 10.0 1 06/22/2023 04:25 WG2082003
n-Nitrosodi-n-propylamine ND 10.0 1 06/22/2023 04:25 WG2082003
Phenanthrene ND 1.00 1 06/22/2023 04:25 WG2082003
Benzylbutyl phthalate ND 3.00 1 06/22/2023 04:25 WG2082003
Bis(2-ethylhexyl)phthalate ND 3.00 1 06/22/2023 04:25 WG2082003
Di-n-butyl phthalate ND 3.00 1 06/22/2023 04:25 WG2082003
Diethyl phthalate ND 3.00 1 06/22/2023 04:25 WG2082003
Dimethyl phthalate ND 3.00 1 06/22/2023 04:25 WG2082003
Di-n-octyl phthalate ND 3.00 1 06/22/2023 04:25 WG2082003
Pyrene ND 1.00 1 06/22/2023 04:25 WG2082003
1,2,4-Trichlorobenzene ND 10.0 1 06/22/2023 04:25 WG2082003
4-Chloro-3-methylphenol ND 10.0 1 06/22/2023 04:25 WG2082003
2-Chlorophenol ND 10.0 1 06/22/2023 04:25 WG2082003
2,4-Dichlorophenol ND 10.0 1 06/22/2023 04:25 WG2082003
2,4-Dimethylphenol ND 10.0 1 06/22/2023 04:25 WG2082003
4,6-Dinitro-2-methylphenol ND 10.0 1 06/22/2023 04:25 WG2082003
2,4-Dinitrophenol ND 10.0 1 06/22/2023 04:25 WG2082003
2-Nitrophenol ND 10.0 1 06/22/2023 04:25 WG2082003
4-Nitrophenol ND 10.0 1 06/22/2023 04:25 WG2082003
Pentachlorophenol ND 10.0 1 06/22/2023 04:25 WG2082003
Phenol ND 10.0 1 06/22/2023 04:25 WG2082003
2,4,6-Trichlorophenol ND 10.0 1 06/22/2023 04:25 WG2082003
(S) Nitrobenzene-d5 85.4 15.0-314 06/22/2023 04:25 WG2082003
(S) 2-Fluorobiphenyl 47.7 22.0-127 06/22/2023 04:25 WG2082003
(S) p-Terphenyl-d14 86.0 29.0-141 06/22/2023 04:25 WG2082003
(S) Phenol-d5 24.7 8.00-424 06/22/2023 04:25 WG2082003
(S) 2-Fluorophenol 25.2 10.0-120 06/22/2023 04:25 WG2082003
(S) 2,4,6-Tribromophenol 33.5 10.0-153 06/22/2023 04:25 WG2082003
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 18 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 18 of 69
SAMPLE RESULTS - 05
L1626779
MW-7
Collected date/time: 06/14/23 12:50
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene ND 1.00 1 06/22/2023 17:00 WG2082702
Bromobenzene ND 1.00 1 06/22/2023 17:00 WG2082702
Bromodichloromethane ND 1.00 1 06/22/2023 17:00 WG2082702
Bromochloromethane ND 1.00 1 06/22/2023 17:00 WG2082702
Bromoform ND 1.00 1 06/22/2023 17:00 WG2082702
Bromomethane ND 5.00 1 06/22/2023 17:00 WG2082702
n-Butylbenzene ND 1.00 1 06/22/2023 17:00 WG2082702
sec-Butylbenzene ND 1.00 1 06/22/2023 17:00 WG2082702
tert-Butylbenzene ND 1.00 1 06/22/2023 17:00 WG2082702
Carbon tetrachloride ND 1.00 1 06/22/2023 17:00 WG2082702
Chlorobenzene ND 1.00 1 06/22/2023 17:00 WG2082702
Chlorodibromomethane ND 1.00 1 06/22/2023 17:00 WG2082702
Chloroethane ND 5.00 1 06/22/2023 17:00 WG2082702
Chloroform ND 5.00 1 06/22/2023 17:00 WG2082702
Chloromethane ND 2.50 1 06/22/2023 17:00 WG2082702
2-Chlorotoluene ND 1.00 1 06/22/2023 17:00 WG2082702
4-Chlorotoluene ND 1.00 1 06/22/2023 17:00 WG2082702
1,2-Dibromo-3-Chloropropane ND 5.00 1 06/22/2023 17:00 WG2082702
1,2-Dibromoethane ND 1.00 1 06/22/2023 17:00 WG2082702
Dibromomethane ND 1.00 1 06/22/2023 17:00 WG2082702
1,2-Dichlorobenzene ND 1.00 1 06/22/2023 17:00 WG2082702
1,3-Dichlorobenzene ND 1.00 1 06/22/2023 17:00 WG2082702
1,4-Dichlorobenzene ND 1.00 1 06/22/2023 17:00 WG2082702
Dichlorodifluoromethane ND 5.00 1 06/22/2023 17:00 WG2082702
1,1-Dichloroethane ND 1.00 1 06/22/2023 17:00 WG2082702
1,2-Dichloroethane ND 1.00 1 06/22/2023 17:00 WG2082702
1,1-Dichloroethene ND 1.00 1 06/22/2023 17:00 WG2082702
cis-1,2-Dichloroethene ND 1.00 1 06/22/2023 17:00 WG2082702
trans-1,2-Dichloroethene ND 1.00 1 06/22/2023 17:00 WG2082702
1,2-Dichloropropane ND J4 1.00 1 06/22/2023 17:00 WG2082702
1,1-Dichloropropene ND 1.00 1 06/22/2023 17:00 WG2082702
1,3-Dichloropropane ND 1.00 1 06/22/2023 17:00 WG2082702
cis-1,3-Dichloropropene ND 1.00 1 06/22/2023 17:00 WG2082702
trans-1,3-Dichloropropene ND 1.00 1 06/22/2023 17:00 WG2082702
2,2-Dichloropropane ND 1.00 1 06/22/2023 17:00 WG2082702
Di-isopropyl ether ND 1.00 1 06/22/2023 17:00 WG2082702
Ethylbenzene ND 1.00 1 06/22/2023 17:00 WG2082702
Hexachloro-1,3-butadiene ND 1.00 1 06/22/2023 17:00 WG2082702
Isopropylbenzene ND 1.00 1 06/22/2023 17:00 WG2082702
Methylene Chloride ND 5.00 1 06/22/2023 17:00 WG2082702
Methyl tert-butyl ether ND 1.00 1 06/22/2023 17:00 WG2082702
Naphthalene ND C4 5.00 1 06/22/2023 17:00 WG2082702
n-Propylbenzene ND 1.00 1 06/22/2023 17:00 WG2082702
Styrene ND 1.00 1 06/22/2023 17:00 WG2082702
1,1,1,2-Tetrachloroethane ND 1.00 1 06/22/2023 17:00 WG2082702
1,1,2,2-Tetrachloroethane ND 1.00 1 06/22/2023 17:00 WG2082702
Tetrachloroethene ND 1.00 1 06/22/2023 17:00 WG2082702
Toluene ND 1.00 1 06/22/2023 17:00 WG2082702
1,2,3-Trichlorobenzene ND 1.00 1 06/22/2023 17:00 WG2082702
1,2,4-Trichlorobenzene ND 1.00 1 06/22/2023 17:00 WG2082702
1,1,1-Trichloroethane ND 1.00 1 06/22/2023 17:00 WG2082702
1,1,2-Trichloroethane ND 1.00 1 06/22/2023 17:00 WG2082702
Trichloroethene ND 1.00 1 06/22/2023 17:00 WG2082702
Trichlorofluoromethane ND 5.00 1 06/22/2023 17:00 WG2082702
1,2,3-Trichloropropane ND 2.50 1 06/22/2023 17:00 WG2082702
1,2,4-Trimethylbenzene ND 1.00 1 06/22/2023 17:00 WG2082702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 19 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 19 of 69
SAMPLE RESULTS - 05
L1626779
MW-7
Collected date/time: 06/14/23 12:50
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 06/22/2023 17:00 WG2082702
Vinyl chloride ND 1.00 1 06/22/2023 17:00 WG2082702
o-Xylene ND 1.00 1 06/22/2023 17:00 WG2082702
m&p-Xylenes ND 2.00 1 06/22/2023 17:00 WG2082702
ethanol ND 100 1 06/22/2023 17:00 WG2082702
tert-Amyl Methyl Ether ND 1.00 1 06/22/2023 17:00 WG2082702
Ethyl tert-butyl ether ND 1.00 1 06/22/2023 17:00 WG2082702
tert-Butyl alcohol ND 5.00 1 06/22/2023 17:00 WG2082702
t-Amyl Alcohol ND 50.0 1 06/22/2023 17:00 WG2082702
tert-Butyl formate ND 20.0 1 06/22/2023 17:00 WG2082702
(S) Toluene-d8 115 80.0-120 06/22/2023 17:00 WG2082702
(S) 4-Bromofluorobenzene 88.0 77.0-126 06/22/2023 17:00 WG2082702
(S) 1,2-Dichloroethane-d4 122 70.0-130 06/22/2023 17:00 WG2082702
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 06/24/2023 15:10 WG2083284
Unadjusted C19-C36 Aliphatics ND 100 1 06/24/2023 15:10 WG2083284
Unadjusted C11-C22 Aromatics ND 100 1 06/24/2023 16:26 WG2083284
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 06/24/2023 16:26 WG2083284
(S) o-Terphenyl 59.0 40.0-140 06/24/2023 16:26 WG2083284
(S) 1-Chloro-octadecane 40.4 40.0-140 06/24/2023 15:10 WG2083284
(S) 2-Fluorobiphenyl 87.3 40.0-140 06/24/2023 16:26 WG2083284
(S) 2-Bromonaphthalene 85.1 40.0-140 06/24/2023 16:26 WG2083284
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 06/22/2023 04:47 WG2082003
Acenaphthylene ND 1.00 1 06/22/2023 04:47 WG2082003
Anthracene ND 1.00 1 06/22/2023 04:47 WG2082003
Benzo(a)anthracene ND 1.00 1 06/22/2023 04:47 WG2082003
Benzo(b)fluoranthene ND 1.00 1 06/22/2023 04:47 WG2082003
Benzo(k)fluoranthene ND 1.00 1 06/22/2023 04:47 WG2082003
Benzo(g,h,i)perylene ND 1.00 1 06/22/2023 04:47 WG2082003
Benzo(a)pyrene ND 1.00 1 06/22/2023 04:47 WG2082003
Bis(2-chlorethoxy)methane ND 10.0 1 06/22/2023 04:47 WG2082003
Bis(2-chloroethyl)ether ND 10.0 1 06/22/2023 04:47 WG2082003
2,2-Oxybis(1-Chloropropane)ND 10.0 1 06/22/2023 04:47 WG2082003
4-Bromophenyl-phenylether ND 10.0 1 06/22/2023 04:47 WG2082003
2-Chloronaphthalene ND 1.00 1 06/22/2023 04:47 WG2082003
4-Chlorophenyl-phenylether ND 10.0 1 06/22/2023 04:47 WG2082003
Chrysene ND 1.00 1 06/22/2023 04:47 WG2082003
Dibenz(a,h)anthracene ND 1.00 1 06/22/2023 04:47 WG2082003
3,3-Dichlorobenzidine ND 10.0 1 06/22/2023 04:47 WG2082003
2,4-Dinitrotoluene ND 10.0 1 06/22/2023 04:47 WG2082003
2,6-Dinitrotoluene ND 10.0 1 06/22/2023 04:47 WG2082003
Fluoranthene ND 1.00 1 06/22/2023 04:47 WG2082003
Fluorene ND 1.00 1 06/22/2023 04:47 WG2082003
Hexachlorobenzene ND 1.00 1 06/22/2023 04:47 WG2082003
Hexachloro-1,3-butadiene ND 10.0 1 06/22/2023 04:47 WG2082003
Hexachlorocyclopentadiene ND 10.0 1 06/22/2023 04:47 WG2082003
Hexachloroethane ND 10.0 1 06/22/2023 04:47 WG2082003
Indeno(1,2,3-cd)pyrene ND 1.00 1 06/22/2023 04:47 WG2082003
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 20 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 20 of 69
SAMPLE RESULTS - 05
L1626779
MW-7
Collected date/time: 06/14/23 12:50
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Isophorone ND 10.0 1 06/22/2023 04:47 WG2082003
Naphthalene ND 1.00 1 06/22/2023 04:47 WG2082003
Nitrobenzene ND 10.0 1 06/22/2023 04:47 WG2082003
n-Nitrosodimethylamine ND 10.0 1 06/22/2023 04:47 WG2082003
n-Nitrosodiphenylamine ND 10.0 1 06/22/2023 04:47 WG2082003
n-Nitrosodi-n-propylamine ND 10.0 1 06/22/2023 04:47 WG2082003
Phenanthrene ND 1.00 1 06/22/2023 04:47 WG2082003
Benzylbutyl phthalate ND 3.00 1 06/22/2023 04:47 WG2082003
Bis(2-ethylhexyl)phthalate ND 3.00 1 06/22/2023 04:47 WG2082003
Di-n-butyl phthalate ND 3.00 1 06/22/2023 04:47 WG2082003
Diethyl phthalate ND 3.00 1 06/22/2023 04:47 WG2082003
Dimethyl phthalate ND 3.00 1 06/22/2023 04:47 WG2082003
Di-n-octyl phthalate ND 3.00 1 06/22/2023 04:47 WG2082003
Pyrene ND 1.00 1 06/22/2023 04:47 WG2082003
1,2,4-Trichlorobenzene ND 10.0 1 06/22/2023 04:47 WG2082003
4-Chloro-3-methylphenol ND 10.0 1 06/22/2023 04:47 WG2082003
2-Chlorophenol ND 10.0 1 06/22/2023 04:47 WG2082003
2,4-Dichlorophenol ND 10.0 1 06/22/2023 04:47 WG2082003
2,4-Dimethylphenol ND 10.0 1 06/22/2023 04:47 WG2082003
4,6-Dinitro-2-methylphenol ND 10.0 1 06/22/2023 04:47 WG2082003
2,4-Dinitrophenol ND 10.0 1 06/22/2023 04:47 WG2082003
2-Nitrophenol ND 10.0 1 06/22/2023 04:47 WG2082003
4-Nitrophenol ND 10.0 1 06/22/2023 04:47 WG2082003
Pentachlorophenol ND 10.0 1 06/22/2023 04:47 WG2082003
Phenol ND 10.0 1 06/22/2023 04:47 WG2082003
2,4,6-Trichlorophenol ND 10.0 1 06/22/2023 04:47 WG2082003
(S) Nitrobenzene-d5 73.5 15.0-314 06/22/2023 04:47 WG2082003
(S) 2-Fluorobiphenyl 49.1 22.0-127 06/22/2023 04:47 WG2082003
(S) p-Terphenyl-d14 72.1 29.0-141 06/22/2023 04:47 WG2082003
(S) Phenol-d5 22.3 8.00-424 06/22/2023 04:47 WG2082003
(S) 2-Fluorophenol 23.4 10.0-120 06/22/2023 04:47 WG2082003
(S) 2,4,6-Tribromophenol 39.3 10.0-153 06/22/2023 04:47 WG2082003
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 21 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 21 of 69
SAMPLE RESULTS - 06
L1626779
MW-8
Collected date/time: 06/14/23 13:20
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene ND 1.00 1 06/22/2023 17:20 WG2082702
Bromobenzene ND 1.00 1 06/22/2023 17:20 WG2082702
Bromodichloromethane ND 1.00 1 06/22/2023 17:20 WG2082702
Bromochloromethane ND 1.00 1 06/22/2023 17:20 WG2082702
Bromoform ND 1.00 1 06/22/2023 17:20 WG2082702
Bromomethane ND 5.00 1 06/22/2023 17:20 WG2082702
n-Butylbenzene ND 1.00 1 06/22/2023 17:20 WG2082702
sec-Butylbenzene ND 1.00 1 06/22/2023 17:20 WG2082702
tert-Butylbenzene ND 1.00 1 06/22/2023 17:20 WG2082702
Carbon tetrachloride ND 1.00 1 06/22/2023 17:20 WG2082702
Chlorobenzene ND 1.00 1 06/22/2023 17:20 WG2082702
Chlorodibromomethane ND 1.00 1 06/22/2023 17:20 WG2082702
Chloroethane ND 5.00 1 06/22/2023 17:20 WG2082702
Chloroform ND 5.00 1 06/22/2023 17:20 WG2082702
Chloromethane ND 2.50 1 06/22/2023 17:20 WG2082702
2-Chlorotoluene ND 1.00 1 06/22/2023 17:20 WG2082702
4-Chlorotoluene ND 1.00 1 06/22/2023 17:20 WG2082702
1,2-Dibromo-3-Chloropropane ND 5.00 1 06/22/2023 17:20 WG2082702
1,2-Dibromoethane ND 1.00 1 06/22/2023 17:20 WG2082702
Dibromomethane ND 1.00 1 06/22/2023 17:20 WG2082702
1,2-Dichlorobenzene ND 1.00 1 06/22/2023 17:20 WG2082702
1,3-Dichlorobenzene ND 1.00 1 06/22/2023 17:20 WG2082702
1,4-Dichlorobenzene ND 1.00 1 06/22/2023 17:20 WG2082702
Dichlorodifluoromethane ND 5.00 1 06/22/2023 17:20 WG2082702
1,1-Dichloroethane ND 1.00 1 06/22/2023 17:20 WG2082702
1,2-Dichloroethane ND 1.00 1 06/22/2023 17:20 WG2082702
1,1-Dichloroethene ND 1.00 1 06/22/2023 17:20 WG2082702
cis-1,2-Dichloroethene ND 1.00 1 06/22/2023 17:20 WG2082702
trans-1,2-Dichloroethene ND 1.00 1 06/22/2023 17:20 WG2082702
1,2-Dichloropropane ND J4 1.00 1 06/22/2023 17:20 WG2082702
1,1-Dichloropropene ND 1.00 1 06/22/2023 17:20 WG2082702
1,3-Dichloropropane ND 1.00 1 06/22/2023 17:20 WG2082702
cis-1,3-Dichloropropene ND 1.00 1 06/22/2023 17:20 WG2082702
trans-1,3-Dichloropropene ND 1.00 1 06/22/2023 17:20 WG2082702
2,2-Dichloropropane ND 1.00 1 06/22/2023 17:20 WG2082702
Di-isopropyl ether ND 1.00 1 06/22/2023 17:20 WG2082702
Ethylbenzene ND 1.00 1 06/22/2023 17:20 WG2082702
Hexachloro-1,3-butadiene ND 1.00 1 06/22/2023 17:20 WG2082702
Isopropylbenzene ND 1.00 1 06/22/2023 17:20 WG2082702
Methylene Chloride ND 5.00 1 06/22/2023 17:20 WG2082702
Methyl tert-butyl ether ND 1.00 1 06/22/2023 17:20 WG2082702
Naphthalene ND C4 5.00 1 06/22/2023 17:20 WG2082702
n-Propylbenzene ND 1.00 1 06/22/2023 17:20 WG2082702
Styrene ND 1.00 1 06/22/2023 17:20 WG2082702
1,1,1,2-Tetrachloroethane ND 1.00 1 06/22/2023 17:20 WG2082702
1,1,2,2-Tetrachloroethane ND 1.00 1 06/22/2023 17:20 WG2082702
Tetrachloroethene ND 1.00 1 06/22/2023 17:20 WG2082702
Toluene ND 1.00 1 06/22/2023 17:20 WG2082702
1,2,3-Trichlorobenzene ND 1.00 1 06/22/2023 17:20 WG2082702
1,2,4-Trichlorobenzene ND 1.00 1 06/22/2023 17:20 WG2082702
1,1,1-Trichloroethane ND 1.00 1 06/22/2023 17:20 WG2082702
1,1,2-Trichloroethane ND 1.00 1 06/22/2023 17:20 WG2082702
Trichloroethene ND 1.00 1 06/22/2023 17:20 WG2082702
Trichlorofluoromethane ND 5.00 1 06/22/2023 17:20 WG2082702
1,2,3-Trichloropropane ND 2.50 1 06/22/2023 17:20 WG2082702
1,2,4-Trimethylbenzene ND 1.00 1 06/22/2023 17:20 WG2082702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 22 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 22 of 69
SAMPLE RESULTS - 06
L1626779
MW-8
Collected date/time: 06/14/23 13:20
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 06/22/2023 17:20 WG2082702
Vinyl chloride ND 1.00 1 06/22/2023 17:20 WG2082702
o-Xylene ND 1.00 1 06/22/2023 17:20 WG2082702
m&p-Xylenes ND 2.00 1 06/22/2023 17:20 WG2082702
ethanol ND 100 1 06/22/2023 17:20 WG2082702
tert-Amyl Methyl Ether ND 1.00 1 06/22/2023 17:20 WG2082702
Ethyl tert-butyl ether ND 1.00 1 06/22/2023 17:20 WG2082702
tert-Butyl alcohol ND 5.00 1 06/22/2023 17:20 WG2082702
t-Amyl Alcohol ND 50.0 1 06/22/2023 17:20 WG2082702
tert-Butyl formate ND 20.0 1 06/22/2023 17:20 WG2082702
(S) Toluene-d8 114 80.0-120 06/22/2023 17:20 WG2082702
(S) 4-Bromofluorobenzene 90.8 77.0-126 06/22/2023 17:20 WG2082702
(S) 1,2-Dichloroethane-d4 132 J1 70.0-130 06/22/2023 17:20 WG2082702
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 06/24/2023 15:55 WG2083284
Unadjusted C19-C36 Aliphatics ND 100 1 06/24/2023 15:55 WG2083284
Unadjusted C11-C22 Aromatics ND 100 1 06/24/2023 17:11 WG2083284
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 06/24/2023 17:11 WG2083284
(S) o-Terphenyl 57.6 40.0-140 06/24/2023 17:11 WG2083284
(S) 1-Chloro-octadecane 38.9 J2 40.0-140 06/24/2023 15:55 WG2083284
(S) 2-Fluorobiphenyl 89.3 40.0-140 06/24/2023 17:11 WG2083284
(S) 2-Bromonaphthalene 85.8 40.0-140 06/24/2023 17:11 WG2083284
Sample Narrative:
L1626779-06 WG2083284: Sample produced emulsion during Extraction process, low surr/spike recoveries due to matrix.
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 06/22/2023 05:09 WG2082003
Acenaphthylene ND 1.00 1 06/22/2023 05:09 WG2082003
Anthracene ND 1.00 1 06/22/2023 05:09 WG2082003
Benzo(a)anthracene ND 1.00 1 06/22/2023 05:09 WG2082003
Benzo(b)fluoranthene ND 1.00 1 06/22/2023 05:09 WG2082003
Benzo(k)fluoranthene ND 1.00 1 06/22/2023 05:09 WG2082003
Benzo(g,h,i)perylene ND 1.00 1 06/22/2023 05:09 WG2082003
Benzo(a)pyrene ND 1.00 1 06/22/2023 05:09 WG2082003
Bis(2-chlorethoxy)methane ND 10.0 1 06/22/2023 05:09 WG2082003
Bis(2-chloroethyl)ether ND 10.0 1 06/22/2023 05:09 WG2082003
2,2-Oxybis(1-Chloropropane)ND 10.0 1 06/22/2023 05:09 WG2082003
4-Bromophenyl-phenylether ND 10.0 1 06/22/2023 05:09 WG2082003
2-Chloronaphthalene ND 1.00 1 06/22/2023 05:09 WG2082003
4-Chlorophenyl-phenylether ND 10.0 1 06/22/2023 05:09 WG2082003
Chrysene ND 1.00 1 06/22/2023 05:09 WG2082003
Dibenz(a,h)anthracene ND 1.00 1 06/22/2023 05:09 WG2082003
3,3-Dichlorobenzidine ND 10.0 1 06/22/2023 05:09 WG2082003
2,4-Dinitrotoluene ND 10.0 1 06/22/2023 05:09 WG2082003
2,6-Dinitrotoluene ND 10.0 1 06/22/2023 05:09 WG2082003
Fluoranthene ND 1.00 1 06/22/2023 05:09 WG2082003
Fluorene ND 1.00 1 06/22/2023 05:09 WG2082003
Hexachlorobenzene ND 1.00 1 06/22/2023 05:09 WG2082003
Hexachloro-1,3-butadiene ND 10.0 1 06/22/2023 05:09 WG2082003
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 23 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 23 of 69
SAMPLE RESULTS - 06
L1626779
MW-8
Collected date/time: 06/14/23 13:20
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Hexachlorocyclopentadiene ND 10.0 1 06/22/2023 05:09 WG2082003
Hexachloroethane ND 10.0 1 06/22/2023 05:09 WG2082003
Indeno(1,2,3-cd)pyrene ND 1.00 1 06/22/2023 05:09 WG2082003
Isophorone ND 10.0 1 06/22/2023 05:09 WG2082003
Naphthalene ND 1.00 1 06/22/2023 05:09 WG2082003
Nitrobenzene ND 10.0 1 06/22/2023 05:09 WG2082003
n-Nitrosodimethylamine ND 10.0 1 06/22/2023 05:09 WG2082003
n-Nitrosodiphenylamine ND 10.0 1 06/22/2023 05:09 WG2082003
n-Nitrosodi-n-propylamine ND 10.0 1 06/22/2023 05:09 WG2082003
Phenanthrene ND 1.00 1 06/22/2023 05:09 WG2082003
Benzylbutyl phthalate ND 3.00 1 06/22/2023 05:09 WG2082003
Bis(2-ethylhexyl)phthalate ND 3.00 1 06/22/2023 05:09 WG2082003
Di-n-butyl phthalate ND 3.00 1 06/22/2023 05:09 WG2082003
Diethyl phthalate ND 3.00 1 06/22/2023 05:09 WG2082003
Dimethyl phthalate ND 3.00 1 06/22/2023 05:09 WG2082003
Di-n-octyl phthalate ND 3.00 1 06/22/2023 05:09 WG2082003
Pyrene ND 1.00 1 06/22/2023 05:09 WG2082003
1,2,4-Trichlorobenzene ND 10.0 1 06/22/2023 05:09 WG2082003
4-Chloro-3-methylphenol ND 10.0 1 06/22/2023 05:09 WG2082003
2-Chlorophenol ND 10.0 1 06/22/2023 05:09 WG2082003
2,4-Dichlorophenol ND 10.0 1 06/22/2023 05:09 WG2082003
2,4-Dimethylphenol ND 10.0 1 06/22/2023 05:09 WG2082003
4,6-Dinitro-2-methylphenol ND 10.0 1 06/22/2023 05:09 WG2082003
2,4-Dinitrophenol ND 10.0 1 06/22/2023 05:09 WG2082003
2-Nitrophenol ND 10.0 1 06/22/2023 05:09 WG2082003
4-Nitrophenol ND 10.0 1 06/22/2023 05:09 WG2082003
Pentachlorophenol ND 10.0 1 06/22/2023 05:09 WG2082003
Phenol ND 10.0 1 06/22/2023 05:09 WG2082003
2,4,6-Trichlorophenol ND 10.0 1 06/22/2023 05:09 WG2082003
(S) Nitrobenzene-d5 80.5 15.0-314 06/22/2023 05:09 WG2082003
(S) 2-Fluorobiphenyl 48.6 22.0-127 06/22/2023 05:09 WG2082003
(S) p-Terphenyl-d14 84.0 29.0-141 06/22/2023 05:09 WG2082003
(S) Phenol-d5 25.4 8.00-424 06/22/2023 05:09 WG2082003
(S) 2-Fluorophenol 23.7 10.0-120 06/22/2023 05:09 WG2082003
(S) 2,4,6-Tribromophenol 40.8 10.0-153 06/22/2023 05:09 WG2082003
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 24 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 24 of 69
SAMPLE RESULTS - 07
L1626779
MW-9
Collected date/time: 06/14/23 13:34
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene ND 1.00 1 06/22/2023 17:41 WG2082702
Bromobenzene ND 1.00 1 06/22/2023 17:41 WG2082702
Bromodichloromethane ND 1.00 1 06/22/2023 17:41 WG2082702
Bromochloromethane ND 1.00 1 06/22/2023 17:41 WG2082702
Bromoform ND 1.00 1 06/22/2023 17:41 WG2082702
Bromomethane ND 5.00 1 06/22/2023 17:41 WG2082702
n-Butylbenzene ND 1.00 1 06/22/2023 17:41 WG2082702
sec-Butylbenzene ND 1.00 1 06/22/2023 17:41 WG2082702
tert-Butylbenzene ND 1.00 1 06/22/2023 17:41 WG2082702
Carbon tetrachloride ND 1.00 1 06/22/2023 17:41 WG2082702
Chlorobenzene ND 1.00 1 06/22/2023 17:41 WG2082702
Chlorodibromomethane ND 1.00 1 06/22/2023 17:41 WG2082702
Chloroethane ND 5.00 1 06/22/2023 17:41 WG2082702
Chloroform ND 5.00 1 06/22/2023 17:41 WG2082702
Chloromethane ND 2.50 1 06/22/2023 17:41 WG2082702
2-Chlorotoluene ND 1.00 1 06/22/2023 17:41 WG2082702
4-Chlorotoluene ND 1.00 1 06/22/2023 17:41 WG2082702
1,2-Dibromo-3-Chloropropane ND 5.00 1 06/22/2023 17:41 WG2082702
1,2-Dibromoethane ND 1.00 1 06/22/2023 17:41 WG2082702
Dibromomethane ND 1.00 1 06/22/2023 17:41 WG2082702
1,2-Dichlorobenzene ND 1.00 1 06/22/2023 17:41 WG2082702
1,3-Dichlorobenzene ND 1.00 1 06/22/2023 17:41 WG2082702
1,4-Dichlorobenzene ND 1.00 1 06/22/2023 17:41 WG2082702
Dichlorodifluoromethane ND 5.00 1 06/22/2023 17:41 WG2082702
1,1-Dichloroethane ND 1.00 1 06/22/2023 17:41 WG2082702
1,2-Dichloroethane ND 1.00 1 06/22/2023 17:41 WG2082702
1,1-Dichloroethene ND 1.00 1 06/22/2023 17:41 WG2082702
cis-1,2-Dichloroethene ND 1.00 1 06/22/2023 17:41 WG2082702
trans-1,2-Dichloroethene ND 1.00 1 06/22/2023 17:41 WG2082702
1,2-Dichloropropane ND J4 1.00 1 06/22/2023 17:41 WG2082702
1,1-Dichloropropene ND 1.00 1 06/22/2023 17:41 WG2082702
1,3-Dichloropropane ND 1.00 1 06/22/2023 17:41 WG2082702
cis-1,3-Dichloropropene ND 1.00 1 06/22/2023 17:41 WG2082702
trans-1,3-Dichloropropene ND 1.00 1 06/22/2023 17:41 WG2082702
2,2-Dichloropropane ND 1.00 1 06/22/2023 17:41 WG2082702
Di-isopropyl ether ND 1.00 1 06/22/2023 17:41 WG2082702
Ethylbenzene ND 1.00 1 06/22/2023 17:41 WG2082702
Hexachloro-1,3-butadiene ND 1.00 1 06/22/2023 17:41 WG2082702
Isopropylbenzene ND 1.00 1 06/22/2023 17:41 WG2082702
Methylene Chloride ND 5.00 1 06/22/2023 17:41 WG2082702
Methyl tert-butyl ether ND 1.00 1 06/22/2023 17:41 WG2082702
Naphthalene ND C4 5.00 1 06/22/2023 17:41 WG2082702
n-Propylbenzene ND 1.00 1 06/22/2023 17:41 WG2082702
Styrene ND 1.00 1 06/22/2023 17:41 WG2082702
1,1,1,2-Tetrachloroethane ND 1.00 1 06/22/2023 17:41 WG2082702
1,1,2,2-Tetrachloroethane ND 1.00 1 06/22/2023 17:41 WG2082702
Tetrachloroethene ND 1.00 1 06/22/2023 17:41 WG2082702
Toluene ND 1.00 1 06/22/2023 17:41 WG2082702
1,2,3-Trichlorobenzene ND 1.00 1 06/22/2023 17:41 WG2082702
1,2,4-Trichlorobenzene ND 1.00 1 06/22/2023 17:41 WG2082702
1,1,1-Trichloroethane ND 1.00 1 06/22/2023 17:41 WG2082702
1,1,2-Trichloroethane ND 1.00 1 06/22/2023 17:41 WG2082702
Trichloroethene ND 1.00 1 06/22/2023 17:41 WG2082702
Trichlorofluoromethane ND 5.00 1 06/22/2023 17:41 WG2082702
1,2,3-Trichloropropane ND 2.50 1 06/22/2023 17:41 WG2082702
1,2,4-Trimethylbenzene ND 1.00 1 06/22/2023 17:41 WG2082702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 25 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 25 of 69
SAMPLE RESULTS - 07
L1626779
MW-9
Collected date/time: 06/14/23 13:34
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 06/22/2023 17:41 WG2082702
Vinyl chloride ND 1.00 1 06/22/2023 17:41 WG2082702
o-Xylene ND 1.00 1 06/22/2023 17:41 WG2082702
m&p-Xylenes ND 2.00 1 06/22/2023 17:41 WG2082702
ethanol ND 100 1 06/22/2023 17:41 WG2082702
tert-Amyl Methyl Ether ND 1.00 1 06/22/2023 17:41 WG2082702
Ethyl tert-butyl ether ND 1.00 1 06/22/2023 17:41 WG2082702
tert-Butyl alcohol ND 5.00 1 06/22/2023 17:41 WG2082702
t-Amyl Alcohol ND 50.0 1 06/22/2023 17:41 WG2082702
tert-Butyl formate ND 20.0 1 06/22/2023 17:41 WG2082702
(S) Toluene-d8 116 80.0-120 06/22/2023 17:41 WG2082702
(S) 4-Bromofluorobenzene 91.8 77.0-126 06/22/2023 17:41 WG2082702
(S) 1,2-Dichloroethane-d4 126 70.0-130 06/22/2023 17:41 WG2082702
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 06/24/2023 16:39 WG2083284
Unadjusted C19-C36 Aliphatics ND 100 1 06/24/2023 16:39 WG2083284
Unadjusted C11-C22 Aromatics ND 100 1 06/24/2023 17:55 WG2083284
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 06/24/2023 17:55 WG2083284
(S) o-Terphenyl 66.1 40.0-140 06/24/2023 17:55 WG2083284
(S) 1-Chloro-octadecane 36.1 J2 40.0-140 06/24/2023 16:39 WG2083284
(S) 2-Fluorobiphenyl 87.3 40.0-140 06/24/2023 17:55 WG2083284
(S) 2-Bromonaphthalene 85.2 40.0-140 06/24/2023 17:55 WG2083284
Sample Narrative:
L1626779-07 WG2083284: Sample produced emulsion during Extraction process, low surr/spike recoveries due to matrix.
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 06/22/2023 05:31 WG2082003
Acenaphthylene ND 1.00 1 06/22/2023 05:31 WG2082003
Anthracene ND 1.00 1 06/22/2023 05:31 WG2082003
Benzo(a)anthracene ND 1.00 1 06/22/2023 05:31 WG2082003
Benzo(b)fluoranthene ND 1.00 1 06/22/2023 05:31 WG2082003
Benzo(k)fluoranthene ND 1.00 1 06/22/2023 05:31 WG2082003
Benzo(g,h,i)perylene ND 1.00 1 06/22/2023 05:31 WG2082003
Benzo(a)pyrene ND 1.00 1 06/22/2023 05:31 WG2082003
Bis(2-chlorethoxy)methane ND 10.0 1 06/22/2023 05:31 WG2082003
Bis(2-chloroethyl)ether ND 10.0 1 06/22/2023 05:31 WG2082003
2,2-Oxybis(1-Chloropropane)ND 10.0 1 06/22/2023 05:31 WG2082003
4-Bromophenyl-phenylether ND 10.0 1 06/22/2023 05:31 WG2082003
2-Chloronaphthalene ND 1.00 1 06/22/2023 05:31 WG2082003
4-Chlorophenyl-phenylether ND 10.0 1 06/22/2023 05:31 WG2082003
Chrysene ND 1.00 1 06/22/2023 05:31 WG2082003
Dibenz(a,h)anthracene ND 1.00 1 06/22/2023 05:31 WG2082003
3,3-Dichlorobenzidine ND 10.0 1 06/22/2023 05:31 WG2082003
2,4-Dinitrotoluene ND 10.0 1 06/22/2023 05:31 WG2082003
2,6-Dinitrotoluene ND 10.0 1 06/22/2023 05:31 WG2082003
Fluoranthene ND 1.00 1 06/22/2023 05:31 WG2082003
Fluorene ND 1.00 1 06/22/2023 05:31 WG2082003
Hexachlorobenzene ND 1.00 1 06/22/2023 05:31 WG2082003
Hexachloro-1,3-butadiene ND 10.0 1 06/22/2023 05:31 WG2082003
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 26 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 26 of 69
SAMPLE RESULTS - 07
L1626779
MW-9
Collected date/time: 06/14/23 13:34
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Hexachlorocyclopentadiene ND 10.0 1 06/22/2023 05:31 WG2082003
Hexachloroethane ND 10.0 1 06/22/2023 05:31 WG2082003
Indeno(1,2,3-cd)pyrene ND 1.00 1 06/22/2023 05:31 WG2082003
Isophorone ND 10.0 1 06/22/2023 05:31 WG2082003
Naphthalene ND 1.00 1 06/22/2023 05:31 WG2082003
Nitrobenzene ND 10.0 1 06/22/2023 05:31 WG2082003
n-Nitrosodimethylamine ND 10.0 1 06/22/2023 05:31 WG2082003
n-Nitrosodiphenylamine ND 10.0 1 06/22/2023 05:31 WG2082003
n-Nitrosodi-n-propylamine ND 10.0 1 06/22/2023 05:31 WG2082003
Phenanthrene ND 1.00 1 06/22/2023 05:31 WG2082003
Benzylbutyl phthalate ND 3.00 1 06/22/2023 05:31 WG2082003
Bis(2-ethylhexyl)phthalate ND 3.00 1 06/22/2023 05:31 WG2082003
Di-n-butyl phthalate ND 3.00 1 06/22/2023 05:31 WG2082003
Diethyl phthalate ND 3.00 1 06/22/2023 05:31 WG2082003
Dimethyl phthalate ND 3.00 1 06/22/2023 05:31 WG2082003
Di-n-octyl phthalate ND 3.00 1 06/22/2023 05:31 WG2082003
Pyrene ND 1.00 1 06/22/2023 05:31 WG2082003
1,2,4-Trichlorobenzene ND 10.0 1 06/22/2023 05:31 WG2082003
4-Chloro-3-methylphenol ND 10.0 1 06/22/2023 05:31 WG2082003
2-Chlorophenol ND 10.0 1 06/22/2023 05:31 WG2082003
2,4-Dichlorophenol ND 10.0 1 06/22/2023 05:31 WG2082003
2,4-Dimethylphenol ND 10.0 1 06/22/2023 05:31 WG2082003
4,6-Dinitro-2-methylphenol ND 10.0 1 06/22/2023 05:31 WG2082003
2,4-Dinitrophenol ND 10.0 1 06/22/2023 05:31 WG2082003
2-Nitrophenol ND 10.0 1 06/22/2023 05:31 WG2082003
4-Nitrophenol ND 10.0 1 06/22/2023 05:31 WG2082003
Pentachlorophenol ND 10.0 1 06/22/2023 05:31 WG2082003
Phenol ND 10.0 1 06/22/2023 05:31 WG2082003
2,4,6-Trichlorophenol ND 10.0 1 06/22/2023 05:31 WG2082003
(S) Nitrobenzene-d5 70.9 15.0-314 06/22/2023 05:31 WG2082003
(S) 2-Fluorobiphenyl 45.8 22.0-127 06/22/2023 05:31 WG2082003
(S) p-Terphenyl-d14 78.8 29.0-141 06/22/2023 05:31 WG2082003
(S) Phenol-d5 20.9 8.00-424 06/22/2023 05:31 WG2082003
(S) 2-Fluorophenol 18.8 10.0-120 06/22/2023 05:31 WG2082003
(S) 2,4,6-Tribromophenol 24.5 10.0-153 06/22/2023 05:31 WG2082003
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 27 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 27 of 69
SAMPLE RESULTS - 08
L1626779
MW-12
Collected date/time: 06/14/23 11:25
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene ND 1.00 1 06/22/2023 18:02 WG2082702
Bromobenzene ND 1.00 1 06/22/2023 18:02 WG2082702
Bromodichloromethane ND 1.00 1 06/22/2023 18:02 WG2082702
Bromochloromethane ND 1.00 1 06/22/2023 18:02 WG2082702
Bromoform ND 1.00 1 06/22/2023 18:02 WG2082702
Bromomethane ND 5.00 1 06/22/2023 18:02 WG2082702
n-Butylbenzene ND 1.00 1 06/22/2023 18:02 WG2082702
sec-Butylbenzene ND 1.00 1 06/22/2023 18:02 WG2082702
tert-Butylbenzene ND 1.00 1 06/22/2023 18:02 WG2082702
Carbon tetrachloride ND 1.00 1 06/22/2023 18:02 WG2082702
Chlorobenzene ND 1.00 1 06/22/2023 18:02 WG2082702
Chlorodibromomethane ND 1.00 1 06/22/2023 18:02 WG2082702
Chloroethane ND 5.00 1 06/22/2023 18:02 WG2082702
Chloroform ND 5.00 1 06/22/2023 18:02 WG2082702
Chloromethane ND 2.50 1 06/22/2023 18:02 WG2082702
2-Chlorotoluene ND 1.00 1 06/22/2023 18:02 WG2082702
4-Chlorotoluene ND 1.00 1 06/22/2023 18:02 WG2082702
1,2-Dibromo-3-Chloropropane ND 5.00 1 06/22/2023 18:02 WG2082702
1,2-Dibromoethane ND 1.00 1 06/22/2023 18:02 WG2082702
Dibromomethane ND 1.00 1 06/22/2023 18:02 WG2082702
1,2-Dichlorobenzene ND 1.00 1 06/22/2023 18:02 WG2082702
1,3-Dichlorobenzene ND 1.00 1 06/22/2023 18:02 WG2082702
1,4-Dichlorobenzene ND 1.00 1 06/22/2023 18:02 WG2082702
Dichlorodifluoromethane ND 5.00 1 06/22/2023 18:02 WG2082702
1,1-Dichloroethane ND 1.00 1 06/22/2023 18:02 WG2082702
1,2-Dichloroethane ND 1.00 1 06/22/2023 18:02 WG2082702
1,1-Dichloroethene ND 1.00 1 06/22/2023 18:02 WG2082702
cis-1,2-Dichloroethene ND 1.00 1 06/22/2023 18:02 WG2082702
trans-1,2-Dichloroethene ND 1.00 1 06/22/2023 18:02 WG2082702
1,2-Dichloropropane ND J4 1.00 1 06/22/2023 18:02 WG2082702
1,1-Dichloropropene ND 1.00 1 06/22/2023 18:02 WG2082702
1,3-Dichloropropane ND 1.00 1 06/22/2023 18:02 WG2082702
cis-1,3-Dichloropropene ND 1.00 1 06/22/2023 18:02 WG2082702
trans-1,3-Dichloropropene ND 1.00 1 06/22/2023 18:02 WG2082702
2,2-Dichloropropane ND 1.00 1 06/22/2023 18:02 WG2082702
Di-isopropyl ether ND 1.00 1 06/22/2023 18:02 WG2082702
Ethylbenzene ND 1.00 1 06/22/2023 18:02 WG2082702
Hexachloro-1,3-butadiene ND 1.00 1 06/22/2023 18:02 WG2082702
Isopropylbenzene ND 1.00 1 06/22/2023 18:02 WG2082702
Methylene Chloride ND 5.00 1 06/22/2023 18:02 WG2082702
Methyl tert-butyl ether ND 1.00 1 06/22/2023 18:02 WG2082702
Naphthalene ND C4 5.00 1 06/22/2023 18:02 WG2082702
n-Propylbenzene ND 1.00 1 06/22/2023 18:02 WG2082702
Styrene ND 1.00 1 06/22/2023 18:02 WG2082702
1,1,1,2-Tetrachloroethane ND 1.00 1 06/22/2023 18:02 WG2082702
1,1,2,2-Tetrachloroethane ND 1.00 1 06/22/2023 18:02 WG2082702
Tetrachloroethene ND 1.00 1 06/22/2023 18:02 WG2082702
Toluene ND 1.00 1 06/22/2023 18:02 WG2082702
1,2,3-Trichlorobenzene ND 1.00 1 06/22/2023 18:02 WG2082702
1,2,4-Trichlorobenzene ND 1.00 1 06/22/2023 18:02 WG2082702
1,1,1-Trichloroethane ND 1.00 1 06/22/2023 18:02 WG2082702
1,1,2-Trichloroethane ND 1.00 1 06/22/2023 18:02 WG2082702
Trichloroethene ND 1.00 1 06/22/2023 18:02 WG2082702
Trichlorofluoromethane ND 5.00 1 06/22/2023 18:02 WG2082702
1,2,3-Trichloropropane ND 2.50 1 06/22/2023 18:02 WG2082702
1,2,4-Trimethylbenzene ND 1.00 1 06/22/2023 18:02 WG2082702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 28 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 28 of 69
SAMPLE RESULTS - 08
L1626779
MW-12
Collected date/time: 06/14/23 11:25
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 06/22/2023 18:02 WG2082702
Vinyl chloride ND 1.00 1 06/22/2023 18:02 WG2082702
o-Xylene ND 1.00 1 06/22/2023 18:02 WG2082702
m&p-Xylenes ND 2.00 1 06/22/2023 18:02 WG2082702
ethanol ND 100 1 06/22/2023 18:02 WG2082702
tert-Amyl Methyl Ether ND 1.00 1 06/22/2023 18:02 WG2082702
Ethyl tert-butyl ether ND 1.00 1 06/22/2023 18:02 WG2082702
tert-Butyl alcohol ND 5.00 1 06/22/2023 18:02 WG2082702
t-Amyl Alcohol ND 50.0 1 06/22/2023 18:02 WG2082702
tert-Butyl formate ND 20.0 1 06/22/2023 18:02 WG2082702
(S) Toluene-d8 118 80.0-120 06/22/2023 18:02 WG2082702
(S) 4-Bromofluorobenzene 93.3 77.0-126 06/22/2023 18:02 WG2082702
(S) 1,2-Dichloroethane-d4 127 70.0-130 06/22/2023 18:02 WG2082702
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 06/24/2023 17:23 WG2083284
Unadjusted C19-C36 Aliphatics ND 100 1 06/24/2023 17:23 WG2083284
Unadjusted C11-C22 Aromatics ND 100 1 06/24/2023 18:40 WG2083284
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 06/24/2023 18:40 WG2083284
(S) o-Terphenyl 61.9 40.0-140 06/24/2023 18:40 WG2083284
(S) 1-Chloro-octadecane 44.5 40.0-140 06/24/2023 17:23 WG2083284
(S) 2-Fluorobiphenyl 85.9 40.0-140 06/24/2023 18:40 WG2083284
(S) 2-Bromonaphthalene 82.6 40.0-140 06/24/2023 18:40 WG2083284
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 06/22/2023 05:53 WG2082003
Acenaphthylene ND 1.00 1 06/22/2023 05:53 WG2082003
Anthracene ND 1.00 1 06/22/2023 05:53 WG2082003
Benzo(a)anthracene ND 1.00 1 06/22/2023 05:53 WG2082003
Benzo(b)fluoranthene ND 1.00 1 06/22/2023 05:53 WG2082003
Benzo(k)fluoranthene ND 1.00 1 06/22/2023 05:53 WG2082003
Benzo(g,h,i)perylene ND 1.00 1 06/22/2023 05:53 WG2082003
Benzo(a)pyrene ND 1.00 1 06/22/2023 05:53 WG2082003
Bis(2-chlorethoxy)methane ND 10.0 1 06/22/2023 05:53 WG2082003
Bis(2-chloroethyl)ether ND 10.0 1 06/22/2023 05:53 WG2082003
2,2-Oxybis(1-Chloropropane)ND 10.0 1 06/22/2023 05:53 WG2082003
4-Bromophenyl-phenylether ND 10.0 1 06/22/2023 05:53 WG2082003
2-Chloronaphthalene ND 1.00 1 06/22/2023 05:53 WG2082003
4-Chlorophenyl-phenylether ND 10.0 1 06/22/2023 05:53 WG2082003
Chrysene ND 1.00 1 06/22/2023 05:53 WG2082003
Dibenz(a,h)anthracene ND 1.00 1 06/22/2023 05:53 WG2082003
3,3-Dichlorobenzidine ND 10.0 1 06/22/2023 05:53 WG2082003
2,4-Dinitrotoluene ND 10.0 1 06/22/2023 05:53 WG2082003
2,6-Dinitrotoluene ND 10.0 1 06/22/2023 05:53 WG2082003
Fluoranthene ND 1.00 1 06/22/2023 05:53 WG2082003
Fluorene ND 1.00 1 06/22/2023 05:53 WG2082003
Hexachlorobenzene ND 1.00 1 06/22/2023 05:53 WG2082003
Hexachloro-1,3-butadiene ND 10.0 1 06/22/2023 05:53 WG2082003
Hexachlorocyclopentadiene ND 10.0 1 06/22/2023 05:53 WG2082003
Hexachloroethane ND 10.0 1 06/22/2023 05:53 WG2082003
Indeno(1,2,3-cd)pyrene ND 1.00 1 06/22/2023 05:53 WG2082003
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 29 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 29 of 69
SAMPLE RESULTS - 08
L1626779
MW-12
Collected date/time: 06/14/23 11:25
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Isophorone ND 10.0 1 06/22/2023 05:53 WG2082003
Naphthalene ND 1.00 1 06/22/2023 05:53 WG2082003
Nitrobenzene ND 10.0 1 06/22/2023 05:53 WG2082003
n-Nitrosodimethylamine ND 10.0 1 06/22/2023 05:53 WG2082003
n-Nitrosodiphenylamine ND 10.0 1 06/22/2023 05:53 WG2082003
n-Nitrosodi-n-propylamine ND 10.0 1 06/22/2023 05:53 WG2082003
Phenanthrene ND 1.00 1 06/22/2023 05:53 WG2082003
Benzylbutyl phthalate ND 3.00 1 06/22/2023 05:53 WG2082003
Bis(2-ethylhexyl)phthalate ND 3.00 1 06/22/2023 05:53 WG2082003
Di-n-butyl phthalate ND 3.00 1 06/22/2023 05:53 WG2082003
Diethyl phthalate ND 3.00 1 06/22/2023 05:53 WG2082003
Dimethyl phthalate ND 3.00 1 06/22/2023 05:53 WG2082003
Di-n-octyl phthalate ND 3.00 1 06/22/2023 05:53 WG2082003
Pyrene ND 1.00 1 06/22/2023 05:53 WG2082003
1,2,4-Trichlorobenzene ND 10.0 1 06/22/2023 05:53 WG2082003
4-Chloro-3-methylphenol ND 10.0 1 06/22/2023 05:53 WG2082003
2-Chlorophenol ND 10.0 1 06/22/2023 05:53 WG2082003
2,4-Dichlorophenol ND 10.0 1 06/22/2023 05:53 WG2082003
2,4-Dimethylphenol ND 10.0 1 06/22/2023 05:53 WG2082003
4,6-Dinitro-2-methylphenol ND 10.0 1 06/22/2023 05:53 WG2082003
2,4-Dinitrophenol ND 10.0 1 06/22/2023 05:53 WG2082003
2-Nitrophenol ND 10.0 1 06/22/2023 05:53 WG2082003
4-Nitrophenol ND 10.0 1 06/22/2023 05:53 WG2082003
Pentachlorophenol ND 10.0 1 06/22/2023 05:53 WG2082003
Phenol ND 10.0 1 06/22/2023 05:53 WG2082003
2,4,6-Trichlorophenol ND 10.0 1 06/22/2023 05:53 WG2082003
(S) Nitrobenzene-d5 68.3 15.0-314 06/22/2023 05:53 WG2082003
(S) 2-Fluorobiphenyl 45.5 22.0-127 06/22/2023 05:53 WG2082003
(S) p-Terphenyl-d14 91.5 29.0-141 06/22/2023 05:53 WG2082003
(S) Phenol-d5 17.9 8.00-424 06/22/2023 05:53 WG2082003
(S) 2-Fluorophenol 17.3 10.0-120 06/22/2023 05:53 WG2082003
(S) 2,4,6-Tribromophenol 41.8 10.0-153 06/22/2023 05:53 WG2082003
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 30 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 30 of 69
SAMPLE RESULTS - 09
L1626779
MW-13
Collected date/time: 06/14/23 14:00
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene ND 1.00 1 06/22/2023 18:22 WG2082702
Bromobenzene ND 1.00 1 06/22/2023 18:22 WG2082702
Bromodichloromethane ND 1.00 1 06/22/2023 18:22 WG2082702
Bromochloromethane ND 1.00 1 06/22/2023 18:22 WG2082702
Bromoform ND 1.00 1 06/22/2023 18:22 WG2082702
Bromomethane ND 5.00 1 06/22/2023 18:22 WG2082702
n-Butylbenzene ND 1.00 1 06/22/2023 18:22 WG2082702
sec-Butylbenzene ND 1.00 1 06/22/2023 18:22 WG2082702
tert-Butylbenzene ND 1.00 1 06/22/2023 18:22 WG2082702
Carbon tetrachloride ND 1.00 1 06/22/2023 18:22 WG2082702
Chlorobenzene ND 1.00 1 06/22/2023 18:22 WG2082702
Chlorodibromomethane ND 1.00 1 06/22/2023 18:22 WG2082702
Chloroethane ND 5.00 1 06/22/2023 18:22 WG2082702
Chloroform ND 5.00 1 06/22/2023 18:22 WG2082702
Chloromethane ND 2.50 1 06/22/2023 18:22 WG2082702
2-Chlorotoluene ND 1.00 1 06/22/2023 18:22 WG2082702
4-Chlorotoluene ND 1.00 1 06/22/2023 18:22 WG2082702
1,2-Dibromo-3-Chloropropane ND 5.00 1 06/22/2023 18:22 WG2082702
1,2-Dibromoethane ND 1.00 1 06/22/2023 18:22 WG2082702
Dibromomethane ND 1.00 1 06/22/2023 18:22 WG2082702
1,2-Dichlorobenzene ND 1.00 1 06/22/2023 18:22 WG2082702
1,3-Dichlorobenzene ND 1.00 1 06/22/2023 18:22 WG2082702
1,4-Dichlorobenzene ND 1.00 1 06/22/2023 18:22 WG2082702
Dichlorodifluoromethane ND 5.00 1 06/22/2023 18:22 WG2082702
1,1-Dichloroethane ND 1.00 1 06/22/2023 18:22 WG2082702
1,2-Dichloroethane ND 1.00 1 06/22/2023 18:22 WG2082702
1,1-Dichloroethene ND 1.00 1 06/22/2023 18:22 WG2082702
cis-1,2-Dichloroethene ND 1.00 1 06/22/2023 18:22 WG2082702
trans-1,2-Dichloroethene ND 1.00 1 06/22/2023 18:22 WG2082702
1,2-Dichloropropane ND J4 1.00 1 06/22/2023 18:22 WG2082702
1,1-Dichloropropene ND 1.00 1 06/22/2023 18:22 WG2082702
1,3-Dichloropropane ND 1.00 1 06/22/2023 18:22 WG2082702
cis-1,3-Dichloropropene ND 1.00 1 06/22/2023 18:22 WG2082702
trans-1,3-Dichloropropene ND 1.00 1 06/22/2023 18:22 WG2082702
2,2-Dichloropropane ND 1.00 1 06/22/2023 18:22 WG2082702
Di-isopropyl ether ND 1.00 1 06/22/2023 18:22 WG2082702
Ethylbenzene ND 1.00 1 06/22/2023 18:22 WG2082702
Hexachloro-1,3-butadiene ND 1.00 1 06/22/2023 18:22 WG2082702
Isopropylbenzene ND 1.00 1 06/22/2023 18:22 WG2082702
Methylene Chloride ND 5.00 1 06/22/2023 18:22 WG2082702
Methyl tert-butyl ether ND 1.00 1 06/22/2023 18:22 WG2082702
Naphthalene ND C4 5.00 1 06/22/2023 18:22 WG2082702
n-Propylbenzene ND 1.00 1 06/22/2023 18:22 WG2082702
Styrene ND 1.00 1 06/22/2023 18:22 WG2082702
1,1,1,2-Tetrachloroethane ND 1.00 1 06/22/2023 18:22 WG2082702
1,1,2,2-Tetrachloroethane ND 1.00 1 06/22/2023 18:22 WG2082702
Tetrachloroethene ND 1.00 1 06/22/2023 18:22 WG2082702
Toluene ND 1.00 1 06/22/2023 18:22 WG2082702
1,2,3-Trichlorobenzene ND 1.00 1 06/22/2023 18:22 WG2082702
1,2,4-Trichlorobenzene ND 1.00 1 06/22/2023 18:22 WG2082702
1,1,1-Trichloroethane ND 1.00 1 06/22/2023 18:22 WG2082702
1,1,2-Trichloroethane ND 1.00 1 06/22/2023 18:22 WG2082702
Trichloroethene ND 1.00 1 06/22/2023 18:22 WG2082702
Trichlorofluoromethane ND 5.00 1 06/22/2023 18:22 WG2082702
1,2,3-Trichloropropane ND 2.50 1 06/22/2023 18:22 WG2082702
1,2,4-Trimethylbenzene ND 1.00 1 06/22/2023 18:22 WG2082702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 31 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 31 of 69
SAMPLE RESULTS - 09
L1626779
MW-13
Collected date/time: 06/14/23 14:00
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 06/22/2023 18:22 WG2082702
Vinyl chloride ND 1.00 1 06/22/2023 18:22 WG2082702
o-Xylene ND 1.00 1 06/22/2023 18:22 WG2082702
m&p-Xylenes ND 2.00 1 06/22/2023 18:22 WG2082702
ethanol ND 100 1 06/22/2023 18:22 WG2082702
tert-Amyl Methyl Ether ND 1.00 1 06/22/2023 18:22 WG2082702
Ethyl tert-butyl ether ND 1.00 1 06/22/2023 18:22 WG2082702
tert-Butyl alcohol ND 5.00 1 06/22/2023 18:22 WG2082702
t-Amyl Alcohol ND 50.0 1 06/22/2023 18:22 WG2082702
tert-Butyl formate ND 20.0 1 06/22/2023 18:22 WG2082702
(S) Toluene-d8 120 80.0-120 06/22/2023 18:22 WG2082702
(S) 4-Bromofluorobenzene 93.5 77.0-126 06/22/2023 18:22 WG2082702
(S) 1,2-Dichloroethane-d4 126 70.0-130 06/22/2023 18:22 WG2082702
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 103 1.03 06/24/2023 18:07 WG2083284
Unadjusted C19-C36 Aliphatics ND 103 1.03 06/24/2023 18:07 WG2083284
Unadjusted C11-C22 Aromatics ND 103 1.03 06/24/2023 19:25 WG2083284
Unadjusted Total Petroleum
Hydrocarbons ND 103 1.03 06/24/2023 19:25 WG2083284
(S) o-Terphenyl 61.2 40.0-140 06/24/2023 19:25 WG2083284
(S) 1-Chloro-octadecane 34.0 J2 40.0-140 06/24/2023 18:07 WG2083284
(S) 2-Fluorobiphenyl 83.1 40.0-140 06/24/2023 19:25 WG2083284
(S) 2-Bromonaphthalene 79.2 40.0-140 06/24/2023 19:25 WG2083284
Sample Narrative:
L1626779-09 WG2083284: Sample produced heavy emulsion during Extraction process, low surr/spike recoveries due to matrix
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 06/22/2023 06:15 WG2082003
Acenaphthylene ND 1.00 1 06/22/2023 06:15 WG2082003
Anthracene ND 1.00 1 06/22/2023 06:15 WG2082003
Benzo(a)anthracene ND 1.00 1 06/22/2023 06:15 WG2082003
Benzo(b)fluoranthene ND 1.00 1 06/22/2023 06:15 WG2082003
Benzo(k)fluoranthene ND 1.00 1 06/22/2023 06:15 WG2082003
Benzo(g,h,i)perylene ND 1.00 1 06/22/2023 06:15 WG2082003
Benzo(a)pyrene ND 1.00 1 06/22/2023 06:15 WG2082003
Bis(2-chlorethoxy)methane ND 10.0 1 06/22/2023 06:15 WG2082003
Bis(2-chloroethyl)ether ND 10.0 1 06/22/2023 06:15 WG2082003
2,2-Oxybis(1-Chloropropane)ND 10.0 1 06/22/2023 06:15 WG2082003
4-Bromophenyl-phenylether ND 10.0 1 06/22/2023 06:15 WG2082003
2-Chloronaphthalene ND 1.00 1 06/22/2023 06:15 WG2082003
4-Chlorophenyl-phenylether ND 10.0 1 06/22/2023 06:15 WG2082003
Chrysene ND 1.00 1 06/22/2023 06:15 WG2082003
Dibenz(a,h)anthracene ND 1.00 1 06/22/2023 06:15 WG2082003
3,3-Dichlorobenzidine ND 10.0 1 06/22/2023 06:15 WG2082003
2,4-Dinitrotoluene ND 10.0 1 06/22/2023 06:15 WG2082003
2,6-Dinitrotoluene ND 10.0 1 06/22/2023 06:15 WG2082003
Fluoranthene ND 1.00 1 06/22/2023 06:15 WG2082003
Fluorene ND 1.00 1 06/22/2023 06:15 WG2082003
Hexachlorobenzene ND 1.00 1 06/22/2023 06:15 WG2082003
Hexachloro-1,3-butadiene ND 10.0 1 06/22/2023 06:15 WG2082003
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 32 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 32 of 69
SAMPLE RESULTS - 09
L1626779
MW-13
Collected date/time: 06/14/23 14:00
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Hexachlorocyclopentadiene ND 10.0 1 06/22/2023 06:15 WG2082003
Hexachloroethane ND 10.0 1 06/22/2023 06:15 WG2082003
Indeno(1,2,3-cd)pyrene ND 1.00 1 06/22/2023 06:15 WG2082003
Isophorone ND 10.0 1 06/22/2023 06:15 WG2082003
Naphthalene ND 1.00 1 06/22/2023 06:15 WG2082003
Nitrobenzene ND 10.0 1 06/22/2023 06:15 WG2082003
n-Nitrosodimethylamine ND 10.0 1 06/22/2023 06:15 WG2082003
n-Nitrosodiphenylamine ND 10.0 1 06/22/2023 06:15 WG2082003
n-Nitrosodi-n-propylamine ND 10.0 1 06/22/2023 06:15 WG2082003
Phenanthrene ND 1.00 1 06/22/2023 06:15 WG2082003
Benzylbutyl phthalate ND 3.00 1 06/22/2023 06:15 WG2082003
Bis(2-ethylhexyl)phthalate ND 3.00 1 06/22/2023 06:15 WG2082003
Di-n-butyl phthalate ND 3.00 1 06/22/2023 06:15 WG2082003
Diethyl phthalate ND 3.00 1 06/22/2023 06:15 WG2082003
Dimethyl phthalate ND 3.00 1 06/22/2023 06:15 WG2082003
Di-n-octyl phthalate ND 3.00 1 06/22/2023 06:15 WG2082003
Pyrene ND 1.00 1 06/22/2023 06:15 WG2082003
1,2,4-Trichlorobenzene ND 10.0 1 06/22/2023 06:15 WG2082003
4-Chloro-3-methylphenol ND 10.0 1 06/22/2023 06:15 WG2082003
2-Chlorophenol ND 10.0 1 06/22/2023 06:15 WG2082003
2,4-Dichlorophenol ND 10.0 1 06/22/2023 06:15 WG2082003
2,4-Dimethylphenol ND 10.0 1 06/22/2023 06:15 WG2082003
4,6-Dinitro-2-methylphenol ND 10.0 1 06/22/2023 06:15 WG2082003
2,4-Dinitrophenol ND 10.0 1 06/22/2023 06:15 WG2082003
2-Nitrophenol ND 10.0 1 06/22/2023 06:15 WG2082003
4-Nitrophenol ND 10.0 1 06/22/2023 06:15 WG2082003
Pentachlorophenol ND 10.0 1 06/22/2023 06:15 WG2082003
Phenol ND 10.0 1 06/22/2023 06:15 WG2082003
2,4,6-Trichlorophenol ND 10.0 1 06/22/2023 06:15 WG2082003
(S) Nitrobenzene-d5 65.7 15.0-314 06/22/2023 06:15 WG2082003
(S) 2-Fluorobiphenyl 42.0 22.0-127 06/22/2023 06:15 WG2082003
(S) p-Terphenyl-d14 62.2 29.0-141 06/22/2023 06:15 WG2082003
(S) Phenol-d5 17.9 8.00-424 06/22/2023 06:15 WG2082003
(S) 2-Fluorophenol 16.8 10.0-120 06/22/2023 06:15 WG2082003
(S) 2,4,6-Tribromophenol 30.9 10.0-153 06/22/2023 06:15 WG2082003
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 33 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 33 of 69
SAMPLE RESULTS - 10
L1626779
MW-1D
Collected date/time: 06/15/23 13:40
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene ND 1.00 1 06/22/2023 18:43 WG2082702
Bromobenzene ND 1.00 1 06/22/2023 18:43 WG2082702
Bromodichloromethane ND 1.00 1 06/22/2023 18:43 WG2082702
Bromochloromethane ND 1.00 1 06/22/2023 18:43 WG2082702
Bromoform ND 1.00 1 06/22/2023 18:43 WG2082702
Bromomethane ND 5.00 1 06/22/2023 18:43 WG2082702
n-Butylbenzene ND 1.00 1 06/22/2023 18:43 WG2082702
sec-Butylbenzene ND 1.00 1 06/22/2023 18:43 WG2082702
tert-Butylbenzene ND 1.00 1 06/22/2023 18:43 WG2082702
Carbon tetrachloride ND 1.00 1 06/22/2023 18:43 WG2082702
Chlorobenzene ND 1.00 1 06/22/2023 18:43 WG2082702
Chlorodibromomethane ND 1.00 1 06/22/2023 18:43 WG2082702
Chloroethane ND 5.00 1 06/22/2023 18:43 WG2082702
Chloroform ND 5.00 1 06/22/2023 18:43 WG2082702
Chloromethane ND 2.50 1 06/22/2023 18:43 WG2082702
2-Chlorotoluene ND 1.00 1 06/22/2023 18:43 WG2082702
4-Chlorotoluene ND 1.00 1 06/22/2023 18:43 WG2082702
1,2-Dibromo-3-Chloropropane ND 5.00 1 06/22/2023 18:43 WG2082702
1,2-Dibromoethane ND 1.00 1 06/22/2023 18:43 WG2082702
Dibromomethane ND 1.00 1 06/22/2023 18:43 WG2082702
1,2-Dichlorobenzene ND 1.00 1 06/22/2023 18:43 WG2082702
1,3-Dichlorobenzene ND 1.00 1 06/22/2023 18:43 WG2082702
1,4-Dichlorobenzene ND 1.00 1 06/22/2023 18:43 WG2082702
Dichlorodifluoromethane ND 5.00 1 06/22/2023 18:43 WG2082702
1,1-Dichloroethane ND 1.00 1 06/22/2023 18:43 WG2082702
1,2-Dichloroethane ND 1.00 1 06/22/2023 18:43 WG2082702
1,1-Dichloroethene ND 1.00 1 06/22/2023 18:43 WG2082702
cis-1,2-Dichloroethene ND 1.00 1 06/22/2023 18:43 WG2082702
trans-1,2-Dichloroethene ND 1.00 1 06/22/2023 18:43 WG2082702
1,2-Dichloropropane ND J4 1.00 1 06/22/2023 18:43 WG2082702
1,1-Dichloropropene ND 1.00 1 06/22/2023 18:43 WG2082702
1,3-Dichloropropane ND 1.00 1 06/22/2023 18:43 WG2082702
cis-1,3-Dichloropropene ND 1.00 1 06/22/2023 18:43 WG2082702
trans-1,3-Dichloropropene ND 1.00 1 06/22/2023 18:43 WG2082702
2,2-Dichloropropane ND 1.00 1 06/22/2023 18:43 WG2082702
Di-isopropyl ether ND 1.00 1 06/22/2023 18:43 WG2082702
Ethylbenzene ND 1.00 1 06/22/2023 18:43 WG2082702
Hexachloro-1,3-butadiene ND 1.00 1 06/22/2023 18:43 WG2082702
Isopropylbenzene ND 1.00 1 06/22/2023 18:43 WG2082702
Methylene Chloride ND 5.00 1 06/22/2023 18:43 WG2082702
Methyl tert-butyl ether ND 1.00 1 06/22/2023 18:43 WG2082702
Naphthalene ND C4 5.00 1 06/22/2023 18:43 WG2082702
n-Propylbenzene ND 1.00 1 06/22/2023 18:43 WG2082702
Styrene ND 1.00 1 06/22/2023 18:43 WG2082702
1,1,1,2-Tetrachloroethane ND 1.00 1 06/22/2023 18:43 WG2082702
1,1,2,2-Tetrachloroethane ND 1.00 1 06/22/2023 18:43 WG2082702
Tetrachloroethene ND 1.00 1 06/22/2023 18:43 WG2082702
Toluene ND 1.00 1 06/22/2023 18:43 WG2082702
1,2,3-Trichlorobenzene ND 1.00 1 06/22/2023 18:43 WG2082702
1,2,4-Trichlorobenzene ND 1.00 1 06/22/2023 18:43 WG2082702
1,1,1-Trichloroethane ND 1.00 1 06/22/2023 18:43 WG2082702
1,1,2-Trichloroethane ND 1.00 1 06/22/2023 18:43 WG2082702
Trichloroethene ND 1.00 1 06/22/2023 18:43 WG2082702
Trichlorofluoromethane ND 5.00 1 06/22/2023 18:43 WG2082702
1,2,3-Trichloropropane ND 2.50 1 06/22/2023 18:43 WG2082702
1,2,4-Trimethylbenzene ND 1.00 1 06/22/2023 18:43 WG2082702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 34 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 34 of 69
SAMPLE RESULTS - 10
L1626779
MW-1D
Collected date/time: 06/15/23 13:40
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 06/22/2023 18:43 WG2082702
Vinyl chloride ND 1.00 1 06/22/2023 18:43 WG2082702
o-Xylene ND 1.00 1 06/22/2023 18:43 WG2082702
m&p-Xylenes ND 2.00 1 06/22/2023 18:43 WG2082702
ethanol ND 100 1 06/22/2023 18:43 WG2082702
tert-Amyl Methyl Ether ND 1.00 1 06/22/2023 18:43 WG2082702
Ethyl tert-butyl ether ND 1.00 1 06/22/2023 18:43 WG2082702
tert-Butyl alcohol ND 5.00 1 06/22/2023 18:43 WG2082702
t-Amyl Alcohol ND 50.0 1 06/22/2023 18:43 WG2082702
tert-Butyl formate ND 20.0 1 06/22/2023 18:43 WG2082702
(S) Toluene-d8 115 80.0-120 06/22/2023 18:43 WG2082702
(S) 4-Bromofluorobenzene 88.4 77.0-126 06/22/2023 18:43 WG2082702
(S) 1,2-Dichloroethane-d4 129 70.0-130 06/22/2023 18:43 WG2082702
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 06/24/2023 18:52 WG2083284
Unadjusted C19-C36 Aliphatics ND 100 1 06/24/2023 18:52 WG2083284
Unadjusted C11-C22 Aromatics ND 100 1 06/24/2023 20:09 WG2083284
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 06/24/2023 20:09 WG2083284
(S) o-Terphenyl 60.5 40.0-140 06/24/2023 20:09 WG2083284
(S) 1-Chloro-octadecane 42.5 40.0-140 06/24/2023 18:52 WG2083284
(S) 2-Fluorobiphenyl 86.4 40.0-140 06/24/2023 20:09 WG2083284
(S) 2-Bromonaphthalene 84.9 40.0-140 06/24/2023 20:09 WG2083284
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 06/22/2023 06:37 WG2082003
Acenaphthylene ND 1.00 1 06/22/2023 06:37 WG2082003
Anthracene ND 1.00 1 06/22/2023 06:37 WG2082003
Benzo(a)anthracene ND 1.00 1 06/22/2023 06:37 WG2082003
Benzo(b)fluoranthene ND 1.00 1 06/22/2023 06:37 WG2082003
Benzo(k)fluoranthene ND 1.00 1 06/22/2023 06:37 WG2082003
Benzo(g,h,i)perylene ND 1.00 1 06/22/2023 06:37 WG2082003
Benzo(a)pyrene ND 1.00 1 06/22/2023 06:37 WG2082003
Bis(2-chlorethoxy)methane ND 10.0 1 06/22/2023 06:37 WG2082003
Bis(2-chloroethyl)ether ND 10.0 1 06/22/2023 06:37 WG2082003
2,2-Oxybis(1-Chloropropane)ND 10.0 1 06/22/2023 06:37 WG2082003
4-Bromophenyl-phenylether ND 10.0 1 06/22/2023 06:37 WG2082003
2-Chloronaphthalene ND 1.00 1 06/22/2023 06:37 WG2082003
4-Chlorophenyl-phenylether ND 10.0 1 06/22/2023 06:37 WG2082003
Chrysene ND 1.00 1 06/22/2023 06:37 WG2082003
Dibenz(a,h)anthracene ND 1.00 1 06/22/2023 06:37 WG2082003
3,3-Dichlorobenzidine ND 10.0 1 06/22/2023 06:37 WG2082003
2,4-Dinitrotoluene ND 10.0 1 06/22/2023 06:37 WG2082003
2,6-Dinitrotoluene ND 10.0 1 06/22/2023 06:37 WG2082003
Fluoranthene ND 1.00 1 06/22/2023 06:37 WG2082003
Fluorene ND 1.00 1 06/22/2023 06:37 WG2082003
Hexachlorobenzene ND 1.00 1 06/22/2023 06:37 WG2082003
Hexachloro-1,3-butadiene ND 10.0 1 06/22/2023 06:37 WG2082003
Hexachlorocyclopentadiene ND 10.0 1 06/22/2023 06:37 WG2082003
Hexachloroethane ND 10.0 1 06/22/2023 06:37 WG2082003
Indeno(1,2,3-cd)pyrene ND 1.00 1 06/22/2023 06:37 WG2082003
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 35 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 35 of 69
SAMPLE RESULTS - 10
L1626779
MW-1D
Collected date/time: 06/15/23 13:40
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Isophorone ND 10.0 1 06/22/2023 06:37 WG2082003
Naphthalene ND 1.00 1 06/22/2023 06:37 WG2082003
Nitrobenzene ND 10.0 1 06/22/2023 06:37 WG2082003
n-Nitrosodimethylamine ND 10.0 1 06/22/2023 06:37 WG2082003
n-Nitrosodiphenylamine ND 10.0 1 06/22/2023 06:37 WG2082003
n-Nitrosodi-n-propylamine ND 10.0 1 06/22/2023 06:37 WG2082003
Phenanthrene ND 1.00 1 06/22/2023 06:37 WG2082003
Benzylbutyl phthalate ND 3.00 1 06/22/2023 06:37 WG2082003
Bis(2-ethylhexyl)phthalate ND 3.00 1 06/22/2023 06:37 WG2082003
Di-n-butyl phthalate ND 3.00 1 06/22/2023 06:37 WG2082003
Diethyl phthalate ND 3.00 1 06/22/2023 06:37 WG2082003
Dimethyl phthalate ND 3.00 1 06/22/2023 06:37 WG2082003
Di-n-octyl phthalate ND 3.00 1 06/22/2023 06:37 WG2082003
Pyrene ND 1.00 1 06/22/2023 06:37 WG2082003
1,2,4-Trichlorobenzene ND 10.0 1 06/22/2023 06:37 WG2082003
4-Chloro-3-methylphenol ND 10.0 1 06/22/2023 06:37 WG2082003
2-Chlorophenol ND 10.0 1 06/22/2023 06:37 WG2082003
2,4-Dichlorophenol ND 10.0 1 06/22/2023 06:37 WG2082003
2,4-Dimethylphenol ND 10.0 1 06/22/2023 06:37 WG2082003
4,6-Dinitro-2-methylphenol ND 10.0 1 06/22/2023 06:37 WG2082003
2,4-Dinitrophenol ND 10.0 1 06/22/2023 06:37 WG2082003
2-Nitrophenol ND 10.0 1 06/22/2023 06:37 WG2082003
4-Nitrophenol ND 10.0 1 06/22/2023 06:37 WG2082003
Pentachlorophenol ND 10.0 1 06/22/2023 06:37 WG2082003
Phenol ND 10.0 1 06/22/2023 06:37 WG2082003
2,4,6-Trichlorophenol ND 10.0 1 06/22/2023 06:37 WG2082003
(S) Nitrobenzene-d5 64.6 15.0-314 06/22/2023 06:37 WG2082003
(S) 2-Fluorobiphenyl 45.5 22.0-127 06/22/2023 06:37 WG2082003
(S) p-Terphenyl-d14 72.8 29.0-141 06/22/2023 06:37 WG2082003
(S) Phenol-d5 15.5 8.00-424 06/22/2023 06:37 WG2082003
(S) 2-Fluorophenol 13.8 10.0-120 06/22/2023 06:37 WG2082003
(S) 2,4,6-Tribromophenol 30.6 10.0-153 06/22/2023 06:37 WG2082003
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 36 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 36 of 69
SAMPLE RESULTS - 11
L1626779
MW-4D
Collected date/time: 06/15/23 12:30
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene 1600 50.0 50 06/22/2023 19:45 WG2082702
Bromobenzene ND 50.0 50 06/22/2023 19:45 WG2082702
Bromodichloromethane ND 50.0 50 06/22/2023 19:45 WG2082702
Bromochloromethane ND 50.0 50 06/22/2023 19:45 WG2082702
Bromoform ND 50.0 50 06/22/2023 19:45 WG2082702
Bromomethane ND 250 50 06/22/2023 19:45 WG2082702
n-Butylbenzene ND 50.0 50 06/22/2023 19:45 WG2082702
sec-Butylbenzene ND 50.0 50 06/22/2023 19:45 WG2082702
tert-Butylbenzene ND 50.0 50 06/22/2023 19:45 WG2082702
Carbon tetrachloride ND 50.0 50 06/22/2023 19:45 WG2082702
Chlorobenzene ND 50.0 50 06/22/2023 19:45 WG2082702
Chlorodibromomethane ND 50.0 50 06/22/2023 19:45 WG2082702
Chloroethane ND 250 50 06/22/2023 19:45 WG2082702
Chloroform ND 250 50 06/22/2023 19:45 WG2082702
Chloromethane ND 125 50 06/22/2023 19:45 WG2082702
2-Chlorotoluene ND 50.0 50 06/22/2023 19:45 WG2082702
4-Chlorotoluene ND 50.0 50 06/22/2023 19:45 WG2082702
1,2-Dibromo-3-Chloropropane ND 250 50 06/22/2023 19:45 WG2082702
1,2-Dibromoethane ND 50.0 50 06/22/2023 19:45 WG2082702
Dibromomethane ND 50.0 50 06/22/2023 19:45 WG2082702
1,2-Dichlorobenzene ND 50.0 50 06/22/2023 19:45 WG2082702
1,3-Dichlorobenzene ND 50.0 50 06/22/2023 19:45 WG2082702
1,4-Dichlorobenzene ND 50.0 50 06/22/2023 19:45 WG2082702
Dichlorodifluoromethane ND 250 50 06/22/2023 19:45 WG2082702
1,1-Dichloroethane ND 50.0 50 06/22/2023 19:45 WG2082702
1,2-Dichloroethane ND 50.0 50 06/22/2023 19:45 WG2082702
1,1-Dichloroethene ND 50.0 50 06/22/2023 19:45 WG2082702
cis-1,2-Dichloroethene ND 50.0 50 06/22/2023 19:45 WG2082702
trans-1,2-Dichloroethene ND 50.0 50 06/22/2023 19:45 WG2082702
1,2-Dichloropropane ND J4 50.0 50 06/22/2023 19:45 WG2082702
1,1-Dichloropropene ND 50.0 50 06/22/2023 19:45 WG2082702
1,3-Dichloropropane ND 50.0 50 06/22/2023 19:45 WG2082702
cis-1,3-Dichloropropene ND 50.0 50 06/22/2023 19:45 WG2082702
trans-1,3-Dichloropropene ND 50.0 50 06/22/2023 19:45 WG2082702
2,2-Dichloropropane ND 50.0 50 06/22/2023 19:45 WG2082702
Di-isopropyl ether ND 50.0 50 06/22/2023 19:45 WG2082702
Ethylbenzene 159 50.0 50 06/22/2023 19:45 WG2082702
Hexachloro-1,3-butadiene ND 50.0 50 06/22/2023 19:45 WG2082702
Isopropylbenzene ND 50.0 50 06/22/2023 19:45 WG2082702
Methylene Chloride ND 250 50 06/22/2023 19:45 WG2082702
Methyl tert-butyl ether ND 50.0 50 06/22/2023 19:45 WG2082702
Naphthalene ND C4 250 50 06/22/2023 19:45 WG2082702
n-Propylbenzene ND 50.0 50 06/22/2023 19:45 WG2082702
Styrene ND 50.0 50 06/22/2023 19:45 WG2082702
1,1,1,2-Tetrachloroethane ND 50.0 50 06/22/2023 19:45 WG2082702
1,1,2,2-Tetrachloroethane ND 50.0 50 06/22/2023 19:45 WG2082702
Tetrachloroethene ND 50.0 50 06/22/2023 19:45 WG2082702
Toluene 99.1 50.0 50 06/22/2023 19:45 WG2082702
1,2,3-Trichlorobenzene ND 50.0 50 06/22/2023 19:45 WG2082702
1,2,4-Trichlorobenzene ND 50.0 50 06/22/2023 19:45 WG2082702
1,1,1-Trichloroethane ND 50.0 50 06/22/2023 19:45 WG2082702
1,1,2-Trichloroethane ND 50.0 50 06/22/2023 19:45 WG2082702
Trichloroethene ND 50.0 50 06/22/2023 19:45 WG2082702
Trichlorofluoromethane ND 250 50 06/22/2023 19:45 WG2082702
1,2,3-Trichloropropane ND 125 50 06/22/2023 19:45 WG2082702
1,2,4-Trimethylbenzene 103 50.0 50 06/22/2023 19:45 WG2082702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 37 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 37 of 69
SAMPLE RESULTS - 11
L1626779
MW-4D
Collected date/time: 06/15/23 12:30
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 50.0 50 06/22/2023 19:45 WG2082702
Vinyl chloride ND 50.0 50 06/22/2023 19:45 WG2082702
o-Xylene 246 50.0 50 06/22/2023 19:45 WG2082702
m&p-Xylenes 332 100 50 06/22/2023 19:45 WG2082702
ethanol ND 5000 50 06/22/2023 19:45 WG2082702
tert-Amyl Methyl Ether ND 50.0 50 06/22/2023 19:45 WG2082702
Ethyl tert-butyl ether ND 50.0 50 06/22/2023 19:45 WG2082702
tert-Butyl alcohol ND 250 50 06/22/2023 19:45 WG2082702
t-Amyl Alcohol ND 2500 50 06/22/2023 19:45 WG2082702
tert-Butyl formate ND 1000 50 06/22/2023 19:45 WG2082702
(S) Toluene-d8 116 80.0-120 06/22/2023 19:45 WG2082702
(S) 4-Bromofluorobenzene 94.4 77.0-126 06/22/2023 19:45 WG2082702
(S) 1,2-Dichloroethane-d4 126 70.0-130 06/22/2023 19:45 WG2082702
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 06/24/2023 19:36 WG2083284
Unadjusted C19-C36 Aliphatics ND 100 1 06/24/2023 19:36 WG2083284
Unadjusted C11-C22 Aromatics ND 100 1 06/24/2023 21:19 WG2083284
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 06/24/2023 21:19 WG2083284
(S) o-Terphenyl 64.3 40.0-140 06/24/2023 21:19 WG2083284
(S) 1-Chloro-octadecane 55.0 40.0-140 06/24/2023 19:36 WG2083284
(S) 2-Fluorobiphenyl 88.3 40.0-140 06/24/2023 21:19 WG2083284
(S) 2-Bromonaphthalene 87.6 40.0-140 06/24/2023 21:19 WG2083284
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 06/22/2023 06:59 WG2082003
Acenaphthylene ND 1.00 1 06/22/2023 06:59 WG2082003
Anthracene ND 1.00 1 06/22/2023 06:59 WG2082003
Benzo(a)anthracene ND 1.00 1 06/22/2023 06:59 WG2082003
Benzo(b)fluoranthene ND 1.00 1 06/22/2023 06:59 WG2082003
Benzo(k)fluoranthene ND 1.00 1 06/22/2023 06:59 WG2082003
Benzo(g,h,i)perylene ND 1.00 1 06/22/2023 06:59 WG2082003
Benzo(a)pyrene ND 1.00 1 06/22/2023 06:59 WG2082003
Bis(2-chlorethoxy)methane ND 10.0 1 06/22/2023 06:59 WG2082003
Bis(2-chloroethyl)ether ND 10.0 1 06/22/2023 06:59 WG2082003
2,2-Oxybis(1-Chloropropane)ND 10.0 1 06/22/2023 06:59 WG2082003
4-Bromophenyl-phenylether ND 10.0 1 06/22/2023 06:59 WG2082003
2-Chloronaphthalene ND 1.00 1 06/22/2023 06:59 WG2082003
4-Chlorophenyl-phenylether ND 10.0 1 06/22/2023 06:59 WG2082003
Chrysene ND 1.00 1 06/22/2023 06:59 WG2082003
Dibenz(a,h)anthracene ND 1.00 1 06/22/2023 06:59 WG2082003
3,3-Dichlorobenzidine ND 10.0 1 06/22/2023 06:59 WG2082003
2,4-Dinitrotoluene ND 10.0 1 06/22/2023 06:59 WG2082003
2,6-Dinitrotoluene ND 10.0 1 06/22/2023 06:59 WG2082003
Fluoranthene ND 1.00 1 06/22/2023 06:59 WG2082003
Fluorene ND 1.00 1 06/22/2023 06:59 WG2082003
Hexachlorobenzene ND 1.00 1 06/22/2023 06:59 WG2082003
Hexachloro-1,3-butadiene ND 10.0 1 06/22/2023 06:59 WG2082003
Hexachlorocyclopentadiene ND 10.0 1 06/22/2023 06:59 WG2082003
Hexachloroethane ND 10.0 1 06/22/2023 06:59 WG2082003
Indeno(1,2,3-cd)pyrene ND 1.00 1 06/22/2023 06:59 WG2082003
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 38 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 38 of 69
SAMPLE RESULTS - 11
L1626779
MW-4D
Collected date/time: 06/15/23 12:30
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Isophorone ND 10.0 1 06/22/2023 06:59 WG2082003
Naphthalene 15.3 1.00 1 06/22/2023 06:59 WG2082003
Nitrobenzene ND 10.0 1 06/22/2023 06:59 WG2082003
n-Nitrosodimethylamine ND 10.0 1 06/22/2023 06:59 WG2082003
n-Nitrosodiphenylamine ND 10.0 1 06/22/2023 06:59 WG2082003
n-Nitrosodi-n-propylamine ND 10.0 1 06/22/2023 06:59 WG2082003
Phenanthrene ND 1.00 1 06/22/2023 06:59 WG2082003
Benzylbutyl phthalate ND 3.00 1 06/22/2023 06:59 WG2082003
Bis(2-ethylhexyl)phthalate ND 3.00 1 06/22/2023 06:59 WG2082003
Di-n-butyl phthalate ND 3.00 1 06/22/2023 06:59 WG2082003
Diethyl phthalate ND 3.00 1 06/22/2023 06:59 WG2082003
Dimethyl phthalate ND 3.00 1 06/22/2023 06:59 WG2082003
Di-n-octyl phthalate ND 3.00 1 06/22/2023 06:59 WG2082003
Pyrene ND 1.00 1 06/22/2023 06:59 WG2082003
1,2,4-Trichlorobenzene ND 10.0 1 06/22/2023 06:59 WG2082003
4-Chloro-3-methylphenol ND 10.0 1 06/22/2023 06:59 WG2082003
2-Chlorophenol ND 10.0 1 06/22/2023 06:59 WG2082003
2,4-Dichlorophenol ND 10.0 1 06/22/2023 06:59 WG2082003
2,4-Dimethylphenol ND 10.0 1 06/22/2023 06:59 WG2082003
4,6-Dinitro-2-methylphenol ND 10.0 1 06/22/2023 06:59 WG2082003
2,4-Dinitrophenol ND 10.0 1 06/22/2023 06:59 WG2082003
2-Nitrophenol ND 10.0 1 06/22/2023 06:59 WG2082003
4-Nitrophenol ND 10.0 1 06/22/2023 06:59 WG2082003
Pentachlorophenol ND 10.0 1 06/22/2023 06:59 WG2082003
Phenol ND 10.0 1 06/22/2023 06:59 WG2082003
2,4,6-Trichlorophenol ND 10.0 1 06/22/2023 06:59 WG2082003
(S) Nitrobenzene-d5 74.1 15.0-314 06/22/2023 06:59 WG2082003
(S) 2-Fluorobiphenyl 50.0 22.0-127 06/22/2023 06:59 WG2082003
(S) p-Terphenyl-d14 96.1 29.0-141 06/22/2023 06:59 WG2082003
(S) Phenol-d5 25.3 8.00-424 06/22/2023 06:59 WG2082003
(S) 2-Fluorophenol 26.8 10.0-120 06/22/2023 06:59 WG2082003
(S) 2,4,6-Tribromophenol 53.0 10.0-153 06/22/2023 06:59 WG2082003
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 39 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 39 of 69
SAMPLE RESULTS - 12
L1626779
MW-5D
Collected date/time: 06/15/23 10:50
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene ND 1.00 1 06/22/2023 19:03 WG2082702
Bromobenzene ND 1.00 1 06/22/2023 19:03 WG2082702
Bromodichloromethane ND 1.00 1 06/22/2023 19:03 WG2082702
Bromochloromethane ND 1.00 1 06/22/2023 19:03 WG2082702
Bromoform ND 1.00 1 06/22/2023 19:03 WG2082702
Bromomethane ND 5.00 1 06/22/2023 19:03 WG2082702
n-Butylbenzene ND 1.00 1 06/22/2023 19:03 WG2082702
sec-Butylbenzene ND 1.00 1 06/22/2023 19:03 WG2082702
tert-Butylbenzene ND 1.00 1 06/22/2023 19:03 WG2082702
Carbon tetrachloride ND 1.00 1 06/22/2023 19:03 WG2082702
Chlorobenzene ND 1.00 1 06/22/2023 19:03 WG2082702
Chlorodibromomethane ND 1.00 1 06/22/2023 19:03 WG2082702
Chloroethane ND 5.00 1 06/22/2023 19:03 WG2082702
Chloroform ND 5.00 1 06/22/2023 19:03 WG2082702
Chloromethane ND 2.50 1 06/22/2023 19:03 WG2082702
2-Chlorotoluene ND 1.00 1 06/22/2023 19:03 WG2082702
4-Chlorotoluene ND 1.00 1 06/22/2023 19:03 WG2082702
1,2-Dibromo-3-Chloropropane ND 5.00 1 06/22/2023 19:03 WG2082702
1,2-Dibromoethane ND 1.00 1 06/22/2023 19:03 WG2082702
Dibromomethane ND 1.00 1 06/22/2023 19:03 WG2082702
1,2-Dichlorobenzene ND 1.00 1 06/22/2023 19:03 WG2082702
1,3-Dichlorobenzene ND 1.00 1 06/22/2023 19:03 WG2082702
1,4-Dichlorobenzene ND 1.00 1 06/22/2023 19:03 WG2082702
Dichlorodifluoromethane ND 5.00 1 06/22/2023 19:03 WG2082702
1,1-Dichloroethane ND 1.00 1 06/22/2023 19:03 WG2082702
1,2-Dichloroethane ND 1.00 1 06/22/2023 19:03 WG2082702
1,1-Dichloroethene ND 1.00 1 06/22/2023 19:03 WG2082702
cis-1,2-Dichloroethene ND 1.00 1 06/22/2023 19:03 WG2082702
trans-1,2-Dichloroethene ND 1.00 1 06/22/2023 19:03 WG2082702
1,2-Dichloropropane ND J4 1.00 1 06/22/2023 19:03 WG2082702
1,1-Dichloropropene ND 1.00 1 06/22/2023 19:03 WG2082702
1,3-Dichloropropane ND 1.00 1 06/22/2023 19:03 WG2082702
cis-1,3-Dichloropropene ND 1.00 1 06/22/2023 19:03 WG2082702
trans-1,3-Dichloropropene ND 1.00 1 06/22/2023 19:03 WG2082702
2,2-Dichloropropane ND 1.00 1 06/22/2023 19:03 WG2082702
Di-isopropyl ether ND 1.00 1 06/22/2023 19:03 WG2082702
Ethylbenzene ND 1.00 1 06/22/2023 19:03 WG2082702
Hexachloro-1,3-butadiene ND 1.00 1 06/22/2023 19:03 WG2082702
Isopropylbenzene ND 1.00 1 06/22/2023 19:03 WG2082702
Methylene Chloride ND 5.00 1 06/22/2023 19:03 WG2082702
Methyl tert-butyl ether ND 1.00 1 06/22/2023 19:03 WG2082702
Naphthalene ND C4 5.00 1 06/22/2023 19:03 WG2082702
n-Propylbenzene ND 1.00 1 06/22/2023 19:03 WG2082702
Styrene ND 1.00 1 06/22/2023 19:03 WG2082702
1,1,1,2-Tetrachloroethane ND 1.00 1 06/22/2023 19:03 WG2082702
1,1,2,2-Tetrachloroethane ND 1.00 1 06/22/2023 19:03 WG2082702
Tetrachloroethene ND 1.00 1 06/22/2023 19:03 WG2082702
Toluene ND 1.00 1 06/22/2023 19:03 WG2082702
1,2,3-Trichlorobenzene ND 1.00 1 06/22/2023 19:03 WG2082702
1,2,4-Trichlorobenzene ND 1.00 1 06/22/2023 19:03 WG2082702
1,1,1-Trichloroethane ND 1.00 1 06/22/2023 19:03 WG2082702
1,1,2-Trichloroethane ND 1.00 1 06/22/2023 19:03 WG2082702
Trichloroethene ND 1.00 1 06/22/2023 19:03 WG2082702
Trichlorofluoromethane ND 5.00 1 06/22/2023 19:03 WG2082702
1,2,3-Trichloropropane ND 2.50 1 06/22/2023 19:03 WG2082702
1,2,4-Trimethylbenzene ND 1.00 1 06/22/2023 19:03 WG2082702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 40 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 40 of 69
SAMPLE RESULTS - 12
L1626779
MW-5D
Collected date/time: 06/15/23 10:50
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 06/22/2023 19:03 WG2082702
Vinyl chloride ND 1.00 1 06/22/2023 19:03 WG2082702
o-Xylene ND 1.00 1 06/22/2023 19:03 WG2082702
m&p-Xylenes ND 2.00 1 06/22/2023 19:03 WG2082702
ethanol ND 100 1 06/22/2023 19:03 WG2082702
tert-Amyl Methyl Ether ND 1.00 1 06/22/2023 19:03 WG2082702
Ethyl tert-butyl ether ND 1.00 1 06/22/2023 19:03 WG2082702
tert-Butyl alcohol ND 5.00 1 06/22/2023 19:03 WG2082702
t-Amyl Alcohol ND 50.0 1 06/22/2023 19:03 WG2082702
tert-Butyl formate ND 20.0 1 06/22/2023 19:03 WG2082702
(S) Toluene-d8 117 80.0-120 06/22/2023 19:03 WG2082702
(S) 4-Bromofluorobenzene 88.9 77.0-126 06/22/2023 19:03 WG2082702
(S) 1,2-Dichloroethane-d4 129 70.0-130 06/22/2023 19:03 WG2082702
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 06/24/2023 21:31 WG2083284
Unadjusted C19-C36 Aliphatics ND 100 1 06/24/2023 21:31 WG2083284
Unadjusted C11-C22 Aromatics ND 100 1 06/24/2023 22:03 WG2083284
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 06/24/2023 22:03 WG2083284
(S) o-Terphenyl 54.8 40.0-140 06/24/2023 22:03 WG2083284
(S) 1-Chloro-octadecane 42.6 40.0-140 06/24/2023 21:31 WG2083284
(S) 2-Fluorobiphenyl 84.6 40.0-140 06/24/2023 22:03 WG2083284
(S) 2-Bromonaphthalene 83.1 40.0-140 06/24/2023 22:03 WG2083284
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 06/22/2023 02:15 WG2080645
Acenaphthylene ND 1.00 1 06/22/2023 02:15 WG2080645
Anthracene ND 1.00 1 06/22/2023 02:15 WG2080645
Benzo(a)anthracene ND 1.00 1 06/22/2023 02:15 WG2080645
Benzo(b)fluoranthene ND 1.00 1 06/22/2023 02:15 WG2080645
Benzo(k)fluoranthene ND 1.00 1 06/22/2023 02:15 WG2080645
Benzo(g,h,i)perylene ND 1.00 1 06/22/2023 02:15 WG2080645
Benzo(a)pyrene ND 1.00 1 06/22/2023 02:15 WG2080645
Bis(2-chlorethoxy)methane ND 10.0 1 06/22/2023 02:15 WG2080645
Bis(2-chloroethyl)ether ND 10.0 1 06/22/2023 02:15 WG2080645
2,2-Oxybis(1-Chloropropane)ND 10.0 1 06/22/2023 02:15 WG2080645
4-Bromophenyl-phenylether ND 10.0 1 06/22/2023 02:15 WG2080645
2-Chloronaphthalene ND 1.00 1 06/22/2023 02:15 WG2080645
4-Chlorophenyl-phenylether ND 10.0 1 06/22/2023 02:15 WG2080645
Chrysene ND 1.00 1 06/22/2023 02:15 WG2080645
Dibenz(a,h)anthracene ND 1.00 1 06/22/2023 02:15 WG2080645
3,3-Dichlorobenzidine ND 10.0 1 06/22/2023 02:15 WG2080645
2,4-Dinitrotoluene ND 10.0 1 06/22/2023 02:15 WG2080645
2,6-Dinitrotoluene ND 10.0 1 06/22/2023 02:15 WG2080645
Fluoranthene ND 1.00 1 06/22/2023 02:15 WG2080645
Fluorene ND 1.00 1 06/22/2023 02:15 WG2080645
Hexachlorobenzene ND 1.00 1 06/22/2023 02:15 WG2080645
Hexachloro-1,3-butadiene ND 10.0 1 06/22/2023 02:15 WG2080645
Hexachlorocyclopentadiene ND 10.0 1 06/22/2023 02:15 WG2080645
Hexachloroethane ND 10.0 1 06/22/2023 02:15 WG2080645
Indeno(1,2,3-cd)pyrene ND 1.00 1 06/22/2023 02:15 WG2080645
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 41 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 41 of 69
SAMPLE RESULTS - 12
L1626779
MW-5D
Collected date/time: 06/15/23 10:50
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Isophorone ND 10.0 1 06/22/2023 02:15 WG2080645
Naphthalene ND 1.00 1 06/22/2023 02:15 WG2080645
Nitrobenzene ND 10.0 1 06/22/2023 02:15 WG2080645
n-Nitrosodimethylamine ND 10.0 1 06/22/2023 02:15 WG2080645
n-Nitrosodiphenylamine ND 10.0 1 06/22/2023 02:15 WG2080645
n-Nitrosodi-n-propylamine ND 10.0 1 06/22/2023 02:15 WG2080645
Phenanthrene ND 1.00 1 06/22/2023 02:15 WG2080645
Benzylbutyl phthalate ND 3.00 1 06/22/2023 02:15 WG2080645
Bis(2-ethylhexyl)phthalate ND 3.00 1 06/22/2023 02:15 WG2080645
Di-n-butyl phthalate ND 3.00 1 06/22/2023 02:15 WG2080645
Diethyl phthalate ND 3.00 1 06/22/2023 02:15 WG2080645
Dimethyl phthalate ND 3.00 1 06/22/2023 02:15 WG2080645
Di-n-octyl phthalate ND 3.00 1 06/22/2023 02:15 WG2080645
Pyrene ND 1.00 1 06/22/2023 02:15 WG2080645
1,2,4-Trichlorobenzene ND 10.0 1 06/22/2023 02:15 WG2080645
4-Chloro-3-methylphenol ND 10.0 1 06/22/2023 02:15 WG2080645
2-Chlorophenol ND 10.0 1 06/22/2023 02:15 WG2080645
2,4-Dichlorophenol ND 10.0 1 06/22/2023 02:15 WG2080645
2,4-Dimethylphenol ND 10.0 1 06/22/2023 02:15 WG2080645
4,6-Dinitro-2-methylphenol ND 10.0 1 06/22/2023 02:15 WG2080645
2,4-Dinitrophenol ND 10.0 1 06/22/2023 02:15 WG2080645
2-Nitrophenol ND 10.0 1 06/22/2023 02:15 WG2080645
4-Nitrophenol ND J4 10.0 1 06/22/2023 02:15 WG2080645
Pentachlorophenol ND 10.0 1 06/22/2023 02:15 WG2080645
Phenol ND 10.0 1 06/22/2023 02:15 WG2080645
2,4,6-Trichlorophenol ND 10.0 1 06/22/2023 02:15 WG2080645
(S) Nitrobenzene-d5 70.3 15.0-314 06/22/2023 02:15 WG2080645
(S) 2-Fluorobiphenyl 61.3 22.0-127 06/22/2023 02:15 WG2080645
(S) p-Terphenyl-d14 78.4 29.0-141 06/22/2023 02:15 WG2080645
(S) Phenol-d5 19.9 8.00-424 06/22/2023 02:15 WG2080645
(S) 2-Fluorophenol 27.5 10.0-120 06/22/2023 02:15 WG2080645
(S) 2,4,6-Tribromophenol 69.8 10.0-153 06/22/2023 02:15 WG2080645
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 42 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 42 of 69
SAMPLE RESULTS - 13
L1626779
MW-6D
Collected date/time: 06/15/23 11:50
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene ND 1.00 1 06/25/2023 02:25 WG2083396
Bromobenzene ND 1.00 1 06/28/2023 12:31 WG2084660
Bromodichloromethane ND 1.00 1 06/25/2023 02:25 WG2083396
Bromochloromethane ND 1.00 1 06/25/2023 02:25 WG2083396
Bromoform ND 1.00 1 06/25/2023 02:25 WG2083396
Bromomethane ND 5.00 1 06/25/2023 02:25 WG2083396
n-Butylbenzene ND 1.00 1 06/28/2023 12:31 WG2084660
sec-Butylbenzene ND 1.00 1 06/28/2023 12:31 WG2084660
tert-Butylbenzene ND 1.00 1 06/28/2023 12:31 WG2084660
Carbon tetrachloride ND 1.00 1 06/25/2023 02:25 WG2083396
Chlorobenzene ND 1.00 1 06/25/2023 02:25 WG2083396
Chlorodibromomethane ND 1.00 1 06/25/2023 02:25 WG2083396
Chloroethane ND 5.00 1 06/25/2023 02:25 WG2083396
Chloroform ND 5.00 1 06/25/2023 02:25 WG2083396
Chloromethane ND 2.50 1 06/25/2023 02:25 WG2083396
2-Chlorotoluene ND 1.00 1 06/28/2023 12:31 WG2084660
4-Chlorotoluene ND 1.00 1 06/28/2023 12:31 WG2084660
1,2-Dibromo-3-Chloropropane ND 5.00 1 06/28/2023 12:31 WG2084660
1,2-Dibromoethane ND 1.00 1 06/25/2023 02:25 WG2083396
Dibromomethane ND 1.00 1 06/25/2023 02:25 WG2083396
1,2-Dichlorobenzene ND 1.00 1 06/28/2023 12:31 WG2084660
1,3-Dichlorobenzene ND 1.00 1 06/28/2023 12:31 WG2084660
1,4-Dichlorobenzene ND 1.00 1 06/28/2023 12:31 WG2084660
Dichlorodifluoromethane ND 5.00 1 06/25/2023 02:25 WG2083396
1,1-Dichloroethane ND 1.00 1 06/25/2023 02:25 WG2083396
1,2-Dichloroethane ND 1.00 1 06/25/2023 02:25 WG2083396
1,1-Dichloroethene ND 1.00 1 06/25/2023 02:25 WG2083396
cis-1,2-Dichloroethene ND 1.00 1 06/25/2023 02:25 WG2083396
trans-1,2-Dichloroethene ND 1.00 1 06/25/2023 02:25 WG2083396
1,2-Dichloropropane ND 1.00 1 06/25/2023 02:25 WG2083396
1,1-Dichloropropene ND 1.00 1 06/25/2023 02:25 WG2083396
1,3-Dichloropropane ND 1.00 1 06/25/2023 02:25 WG2083396
cis-1,3-Dichloropropene ND 1.00 1 06/25/2023 02:25 WG2083396
trans-1,3-Dichloropropene ND 1.00 1 06/25/2023 02:25 WG2083396
2,2-Dichloropropane ND 1.00 1 06/25/2023 02:25 WG2083396
Di-isopropyl ether ND 1.00 1 06/25/2023 02:25 WG2083396
Ethylbenzene ND 1.00 1 06/25/2023 02:25 WG2083396
Hexachloro-1,3-butadiene ND 1.00 1 06/28/2023 12:31 WG2084660
Isopropylbenzene ND 1.00 1 06/25/2023 02:25 WG2083396
Methylene Chloride ND 5.00 1 06/25/2023 02:25 WG2083396
Methyl tert-butyl ether ND 1.00 1 06/25/2023 02:25 WG2083396
Naphthalene ND 5.00 1 06/28/2023 12:31 WG2084660
n-Propylbenzene ND 1.00 1 06/28/2023 12:31 WG2084660
Styrene ND 1.00 1 06/25/2023 02:25 WG2083396
1,1,1,2-Tetrachloroethane ND 1.00 1 06/25/2023 02:25 WG2083396
1,1,2,2-Tetrachloroethane ND 1.00 1 06/28/2023 12:31 WG2084660
Tetrachloroethene ND 1.00 1 06/25/2023 02:25 WG2083396
Toluene ND 1.00 1 06/25/2023 02:25 WG2083396
1,2,3-Trichlorobenzene ND 1.00 1 06/28/2023 12:31 WG2084660
1,2,4-Trichlorobenzene ND 1.00 1 06/28/2023 12:31 WG2084660
1,1,1-Trichloroethane ND 1.00 1 06/25/2023 02:25 WG2083396
1,1,2-Trichloroethane ND 1.00 1 06/25/2023 02:25 WG2083396
Trichloroethene ND 1.00 1 06/25/2023 02:25 WG2083396
Trichlorofluoromethane ND 5.00 1 06/25/2023 02:25 WG2083396
1,2,3-Trichloropropane ND 2.50 1 06/28/2023 12:31 WG2084660
1,2,4-Trimethylbenzene ND 1.00 1 06/28/2023 12:31 WG2084660
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 43 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 43 of 69
SAMPLE RESULTS - 13
L1626779
MW-6D
Collected date/time: 06/15/23 11:50
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,3,5-Trimethylbenzene ND 1.00 1 06/28/2023 12:31 WG2084660
Vinyl chloride ND 1.00 1 06/25/2023 02:25 WG2083396
o-Xylene ND 1.00 1 06/25/2023 02:25 WG2083396
m&p-Xylenes ND 2.00 1 06/25/2023 02:25 WG2083396
ethanol ND 100 1 06/28/2023 12:31 WG2084660
tert-Amyl Methyl Ether ND 1.00 1 06/25/2023 02:25 WG2083396
Ethyl tert-butyl ether ND 1.00 1 06/25/2023 02:25 WG2083396
tert-Butyl alcohol ND 5.00 1 06/25/2023 02:25 WG2083396
t-Amyl Alcohol ND 50.0 1 06/25/2023 02:25 WG2083396
tert-Butyl formate ND C4 20.0 1 06/25/2023 02:25 WG2083396
(S) Toluene-d8 98.4 80.0-120 06/25/2023 02:25 WG2083396
(S) Toluene-d8 118 80.0-120 06/28/2023 12:31 WG2084660
(S) 4-Bromofluorobenzene 85.4 77.0-126 06/25/2023 02:25 WG2083396
(S) 4-Bromofluorobenzene 113 77.0-126 06/28/2023 12:31 WG2084660
(S) 1,2-Dichloroethane-d4 99.7 70.0-130 06/25/2023 02:25 WG2083396
(S) 1,2-Dichloroethane-d4 110 70.0-130 06/28/2023 12:31 WG2084660
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 06/24/2023 22:16 WG2083284
Unadjusted C19-C36 Aliphatics ND 100 1 06/24/2023 22:16 WG2083284
Unadjusted C11-C22 Aromatics ND 100 1 06/24/2023 22:48 WG2083284
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 06/24/2023 22:48 WG2083284
(S) o-Terphenyl 53.4 40.0-140 06/24/2023 22:48 WG2083284
(S) 1-Chloro-octadecane 34.4 J2 40.0-140 06/24/2023 22:16 WG2083284
(S) 2-Fluorobiphenyl 83.9 40.0-140 06/24/2023 22:48 WG2083284
(S) 2-Bromonaphthalene 82.0 40.0-140 06/24/2023 22:48 WG2083284
Sample Narrative:
L1626779-13 WG2083284: Sample produced emulsion during Extraction process, low surr/spike recoveries due to matrix.
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 06/22/2023 02:37 WG2080645
Acenaphthylene ND 1.00 1 06/22/2023 02:37 WG2080645
Anthracene ND 1.00 1 06/22/2023 02:37 WG2080645
Benzo(a)anthracene ND 1.00 1 06/22/2023 02:37 WG2080645
Benzo(b)fluoranthene ND 1.00 1 06/22/2023 02:37 WG2080645
Benzo(k)fluoranthene ND 1.00 1 06/22/2023 02:37 WG2080645
Benzo(g,h,i)perylene ND 1.00 1 06/22/2023 02:37 WG2080645
Benzo(a)pyrene ND 1.00 1 06/22/2023 02:37 WG2080645
Bis(2-chlorethoxy)methane ND 10.0 1 06/22/2023 02:37 WG2080645
Bis(2-chloroethyl)ether ND 10.0 1 06/22/2023 02:37 WG2080645
2,2-Oxybis(1-Chloropropane)ND 10.0 1 06/22/2023 02:37 WG2080645
4-Bromophenyl-phenylether ND 10.0 1 06/22/2023 02:37 WG2080645
2-Chloronaphthalene ND 1.00 1 06/22/2023 02:37 WG2080645
4-Chlorophenyl-phenylether ND 10.0 1 06/22/2023 02:37 WG2080645
Chrysene ND 1.00 1 06/22/2023 02:37 WG2080645
Dibenz(a,h)anthracene ND 1.00 1 06/22/2023 02:37 WG2080645
3,3-Dichlorobenzidine ND 10.0 1 06/22/2023 02:37 WG2080645
2,4-Dinitrotoluene ND 10.0 1 06/22/2023 02:37 WG2080645
2,6-Dinitrotoluene ND 10.0 1 06/22/2023 02:37 WG2080645
Fluoranthene ND 1.00 1 06/22/2023 02:37 WG2080645
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 44 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 44 of 69
SAMPLE RESULTS - 13
L1626779
MW-6D
Collected date/time: 06/15/23 11:50
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Fluorene ND 1.00 1 06/22/2023 02:37 WG2080645
Hexachlorobenzene ND 1.00 1 06/22/2023 02:37 WG2080645
Hexachloro-1,3-butadiene ND 10.0 1 06/22/2023 02:37 WG2080645
Hexachlorocyclopentadiene ND 10.0 1 06/22/2023 02:37 WG2080645
Hexachloroethane ND 10.0 1 06/22/2023 02:37 WG2080645
Indeno(1,2,3-cd)pyrene ND 1.00 1 06/22/2023 02:37 WG2080645
Isophorone ND 10.0 1 06/22/2023 02:37 WG2080645
Naphthalene ND 1.00 1 06/22/2023 02:37 WG2080645
Nitrobenzene ND 10.0 1 06/22/2023 02:37 WG2080645
n-Nitrosodimethylamine ND 10.0 1 06/22/2023 02:37 WG2080645
n-Nitrosodiphenylamine ND 10.0 1 06/22/2023 02:37 WG2080645
n-Nitrosodi-n-propylamine ND 10.0 1 06/22/2023 02:37 WG2080645
Phenanthrene ND 1.00 1 06/22/2023 02:37 WG2080645
Benzylbutyl phthalate ND 3.00 1 06/22/2023 02:37 WG2080645
Bis(2-ethylhexyl)phthalate ND 3.00 1 06/22/2023 02:37 WG2080645
Di-n-butyl phthalate ND 3.00 1 06/22/2023 02:37 WG2080645
Diethyl phthalate ND 3.00 1 06/22/2023 02:37 WG2080645
Dimethyl phthalate ND 3.00 1 06/22/2023 02:37 WG2080645
Di-n-octyl phthalate ND 3.00 1 06/22/2023 02:37 WG2080645
Pyrene ND 1.00 1 06/22/2023 02:37 WG2080645
1,2,4-Trichlorobenzene ND 10.0 1 06/22/2023 02:37 WG2080645
4-Chloro-3-methylphenol ND 10.0 1 06/22/2023 02:37 WG2080645
2-Chlorophenol ND 10.0 1 06/22/2023 02:37 WG2080645
2,4-Dichlorophenol ND 10.0 1 06/22/2023 02:37 WG2080645
2,4-Dimethylphenol ND 10.0 1 06/22/2023 02:37 WG2080645
4,6-Dinitro-2-methylphenol ND 10.0 1 06/22/2023 02:37 WG2080645
2,4-Dinitrophenol ND 10.0 1 06/22/2023 02:37 WG2080645
2-Nitrophenol ND 10.0 1 06/22/2023 02:37 WG2080645
4-Nitrophenol ND J4 10.0 1 06/22/2023 02:37 WG2080645
Pentachlorophenol ND 10.0 1 06/22/2023 02:37 WG2080645
Phenol ND 10.0 1 06/22/2023 02:37 WG2080645
2,4,6-Trichlorophenol ND 10.0 1 06/22/2023 02:37 WG2080645
(S) Nitrobenzene-d5 83.1 15.0-314 06/22/2023 02:37 WG2080645
(S) 2-Fluorobiphenyl 70.0 22.0-127 06/22/2023 02:37 WG2080645
(S) p-Terphenyl-d14 84.6 29.0-141 06/22/2023 02:37 WG2080645
(S) Phenol-d5 27.3 8.00-424 06/22/2023 02:37 WG2080645
(S) 2-Fluorophenol 37.2 10.0-120 06/22/2023 02:37 WG2080645
(S) 2,4,6-Tribromophenol 82.0 10.0-153 06/22/2023 02:37 WG2080645
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 45 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 45 of 69
QUALITY CONTROL SUMMARYWG2082702
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1626779-01,02,03,04,05,06,07,08,09,10,11,12
Method Blank (MB)
(MB) R3940818-3 06/22/23 10:55
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Benzene U 0.0941 1.00
Bromobenzene U 0.118 1.00
Bromodichloromethane U 0.136 1.00
Bromochloromethane U 0.128 1.00
Bromoform U 0.129 1.00
Bromomethane U 0.605 5.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
cis-1,3-Dichloropropene U 0.111 1.00
trans-1,3-Dichloropropene U 0.118 1.00
2,2-Dichloropropane U 0.161 1.00
Di-isopropyl ether U 0.105 1.00
Ethylbenzene U 0.137 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
Isopropylbenzene U 0.105 1.00
Methylene Chloride U 0.430 5.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 46 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 46 of 69
QUALITY CONTROL SUMMARYWG2082702
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1626779-01,02,03,04,05,06,07,08,09,10,11,12
Method Blank (MB)
(MB) R3940818-3 06/22/23 10:55
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Methyl tert-butyl ether U 0.101 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.0993 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Trichlorofluoromethane U 0.160 5.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,4-Trimethylbenzene U 0.322 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
Vinyl chloride U 0.234 1.00
o-Xylene U 0.174 1.00
m&p-Xylenes U 0.430 2.00
ethanol U 42.0 100
tert-Amyl Methyl Ether U 0.195 1.00
Ethyl tert-butyl ether U 0.101 1.00
tert-Butyl alcohol U 4.06 5.00
t-Amyl Alcohol U 4.90 50.0
tert-Butyl formate U 4.51 20.0
(S) Toluene-d8 119 80.0-120
(S) 4-Bromofluorobenzene 92.2 77.0-126
(S) 1,2-Dichloroethane-d4 116 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3940818-1 06/22/23 09:53
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Benzene 5.00 5.31 106 70.0-123
Bromobenzene 5.00 5.30 106 73.0-121
Bromodichloromethane 5.00 5.43 109 75.0-120
Bromochloromethane 5.00 5.32 106 76.0-122
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 47 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 47 of 69
QUALITY CONTROL SUMMARYWG2082702
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1626779-01,02,03,04,05,06,07,08,09,10,11,12
Laboratory Control Sample (LCS)
(LCS) R3940818-1 06/22/23 09:53
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Bromoform 5.00 4.13 82.6 68.0-132
Bromomethane 5.00 3.42 68.4 10.0-160
n-Butylbenzene 5.00 5.04 101 73.0-125
sec-Butylbenzene 5.00 5.17 103 75.0-125
tert-Butylbenzene 5.00 5.23 105 76.0-124
Carbon tetrachloride 5.00 5.89 118 68.0-126
Chlorobenzene 5.00 5.22 104 80.0-121
Chlorodibromomethane 5.00 5.10 102 77.0-125
Chloroethane 5.00 4.06 81.2 47.0-150
Chloroform 5.00 5.74 115 73.0-120
Chloromethane 5.00 6.53 131 41.0-142
2-Chlorotoluene 5.00 5.46 109 76.0-123
4-Chlorotoluene 5.00 5.52 110 75.0-122
1,2-Dibromo-3-Chloropropane 5.00 4.14 82.8 58.0-134
1,2-Dibromoethane 5.00 4.45 89.0 80.0-122
Dibromomethane 5.00 4.72 94.4 80.0-120
1,2-Dichlorobenzene 5.00 5.17 103 79.0-121
1,3-Dichlorobenzene 5.00 5.52 110 79.0-120
1,4-Dichlorobenzene 5.00 5.21 104 79.0-120
Dichlorodifluoromethane 5.00 5.58 112 51.0-149
1,1-Dichloroethane 5.00 6.18 124 70.0-126
1,2-Dichloroethane 5.00 5.97 119 70.0-128
1,1-Dichloroethene 5.00 5.27 105 71.0-124
cis-1,2-Dichloroethene 5.00 5.43 109 73.0-120
trans-1,2-Dichloroethene 5.00 5.41 108 73.0-120
1,2-Dichloropropane 5.00 6.32 126 77.0-125 J4
1,1-Dichloropropene 5.00 5.61 112 74.0-126
1,3-Dichloropropane 5.00 5.18 104 80.0-120
cis-1,3-Dichloropropene 5.00 5.00 100 80.0-123
trans-1,3-Dichloropropene 5.00 4.77 95.4 78.0-124
2,2-Dichloropropane 5.00 6.23 125 58.0-130
Di-isopropyl ether 5.00 6.70 134 58.0-138
Ethylbenzene 5.00 4.92 98.4 79.0-123
Hexachloro-1,3-butadiene 5.00 6.50 130 54.0-138
Isopropylbenzene 5.00 4.79 95.8 76.0-127
Methylene Chloride 5.00 5.30 106 67.0-120
Methyl tert-butyl ether 5.00 5.18 104 68.0-125
Naphthalene 5.00 3.32 66.4 54.0-135
n-Propylbenzene 5.00 5.38 108 77.0-124
Styrene 5.00 4.23 84.6 73.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 48 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 48 of 69
QUALITY CONTROL SUMMARYWG2082702
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1626779-01,02,03,04,05,06,07,08,09,10,11,12
Laboratory Control Sample (LCS)
(LCS) R3940818-1 06/22/23 09:53
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
1,1,1,2-Tetrachloroethane 5.00 5.17 103 75.0-125
1,1,2,2-Tetrachloroethane 5.00 3.81 76.2 65.0-130
Tetrachloroethene 5.00 5.68 114 72.0-132
Toluene 5.00 5.37 107 79.0-120
1,2,3-Trichlorobenzene 5.00 4.48 89.6 50.0-138
1,2,4-Trichlorobenzene 5.00 4.73 94.6 57.0-137
1,1,1-Trichloroethane 5.00 5.87 117 73.0-124
1,1,2-Trichloroethane 5.00 4.71 94.2 80.0-120
Trichloroethene 5.00 5.41 108 78.0-124
Trichlorofluoromethane 5.00 5.82 116 59.0-147
1,2,3-Trichloropropane 5.00 4.79 95.8 73.0-130
1,2,4-Trimethylbenzene 5.00 5.14 103 76.0-121
1,3,5-Trimethylbenzene 5.00 5.40 108 76.0-122
Vinyl chloride 5.00 4.90 98.0 67.0-131
o-Xylene 5.00 4.85 97.0 80.0-122
m&p-Xylenes 10.0 9.88 98.8 80.0-122
ethanol 250 251 100 10.0-160
tert-Amyl Methyl Ether 5.00 5.07 101 66.0-125
Ethyl tert-butyl ether 5.00 6.06 121 63.0-138
tert-Butyl alcohol 25.0 23.0 92.0 27.0-160
(S) Toluene-d8 114 80.0-120
(S) 4-Bromofluorobenzene 93.3 77.0-126
(S) 1,2-Dichloroethane-d4 119 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3940818-2 06/22/23 10:14
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
tert-Butyl formate 100 147 147 10.0-160
(S) Toluene-d8 119 80.0-120
(S) 4-Bromofluorobenzene 91.4 77.0-126
(S) 1,2-Dichloroethane-d4 115 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 49 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 49 of 69
QUALITY CONTROL SUMMARYWG2083396
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1626779-13
Method Blank (MB)
(MB) R3941359-4 06/25/23 00:42
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Benzene U 0.0941 1.00
Bromodichloromethane U 0.136 1.00
Bromochloromethane U 0.128 1.00
Bromoform U 0.129 1.00
Bromomethane U 0.605 5.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
cis-1,3-Dichloropropene U 0.111 1.00
trans-1,3-Dichloropropene U 0.118 1.00
2,2-Dichloropropane U 0.161 1.00
Di-isopropyl ether U 0.105 1.00
Ethylbenzene U 0.137 1.00
Isopropylbenzene U 0.105 1.00
Methylene Chloride U 0.430 5.00
Methyl tert-butyl ether U 0.101 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
Tetrachloroethene 0.508 J 0.300 1.00
Toluene U 0.278 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Trichlorofluoromethane U 0.160 5.00
Vinyl chloride U 0.234 1.00
o-Xylene U 0.174 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 50 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 50 of 69
QUALITY CONTROL SUMMARYWG2083396
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1626779-13
Method Blank (MB)
(MB) R3941359-4 06/25/23 00:42
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
m&p-Xylenes U 0.430 2.00
tert-Amyl Methyl Ether U 0.195 1.00
Ethyl tert-butyl ether U 0.101 1.00
tert-Butyl alcohol U 4.06 5.00
t-Amyl Alcohol U 4.90 50.0
tert-Butyl formate U 4.51 20.0
(S) Toluene-d8 97.5 80.0-120
(S) 4-Bromofluorobenzene 86.2 77.0-126
(S) 1,2-Dichloroethane-d4 99.5 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3941359-1 06/24/23 19:12 • (LCSD) R3941359-2 06/24/23 19:34
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Benzene 5.00 4.63 4.85 92.6 97.0 70.0-123 4.64 20
Bromodichloromethane 5.00 4.68 4.65 93.6 93.0 75.0-120 0.643 20
Bromochloromethane 5.00 4.60 4.77 92.0 95.4 76.0-122 3.63 20
Bromoform 5.00 4.46 4.38 89.2 87.6 68.0-132 1.81 20
Bromomethane 5.00 4.85 4.74 97.0 94.8 10.0-160 2.29 25
Carbon tetrachloride 5.00 4.81 4.90 96.2 98.0 68.0-126 1.85 20
Chlorobenzene 5.00 4.65 4.72 93.0 94.4 80.0-121 1.49 20
Chlorodibromomethane 5.00 4.44 4.89 88.8 97.8 77.0-125 9.65 20
Chloroethane 5.00 4.79 4.74 95.8 94.8 47.0-150 1.05 20
Chloroform 5.00 4.85 4.90 97.0 98.0 73.0-120 1.03 20
Chloromethane 5.00 5.45 5.19 109 104 41.0-142 4.89 20
1,2-Dibromoethane 5.00 4.55 4.81 91.0 96.2 80.0-122 5.56 20
Dibromomethane 5.00 4.60 4.82 92.0 96.4 80.0-120 4.67 20
Dichlorodifluoromethane 5.00 5.18 5.21 104 104 51.0-149 0.577 20
1,1-Dichloroethane 5.00 4.59 4.55 91.8 91.0 70.0-126 0.875 20
1,2-Dichloroethane 5.00 4.90 4.96 98.0 99.2 70.0-128 1.22 20
1,1-Dichloroethene 5.00 4.88 4.64 97.6 92.8 71.0-124 5.04 20
cis-1,2-Dichloroethene 5.00 4.64 4.57 92.8 91.4 73.0-120 1.52 20
trans-1,2-Dichloroethene 5.00 4.69 4.74 93.8 94.8 73.0-120 1.06 20
1,2-Dichloropropane 5.00 4.56 4.54 91.2 90.8 77.0-125 0.440 20
1,1-Dichloropropene 5.00 4.94 5.06 98.8 101 74.0-126 2.40 20
1,3-Dichloropropane 5.00 4.66 4.82 93.2 96.4 80.0-120 3.38 20
cis-1,3-Dichloropropene 5.00 4.54 4.53 90.8 90.6 80.0-123 0.221 20
trans-1,3-Dichloropropene 5.00 4.72 4.81 94.4 96.2 78.0-124 1.89 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 51 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 51 of 69
QUALITY CONTROL SUMMARYWG2083396
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1626779-13
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3941359-1 06/24/23 19:12 • (LCSD) R3941359-2 06/24/23 19:34
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
2,2-Dichloropropane 5.00 4.89 4.78 97.8 95.6 58.0-130 2.28 20
Di-isopropyl ether 5.00 4.10 4.20 82.0 84.0 58.0-138 2.41 20
Ethylbenzene 5.00 4.42 4.69 88.4 93.8 79.0-123 5.93 20
Isopropylbenzene 5.00 4.20 4.40 84.0 88.0 76.0-127 4.65 20
Methylene Chloride 5.00 4.44 4.45 88.8 89.0 67.0-120 0.225 20
Methyl tert-butyl ether 5.00 4.25 4.43 85.0 88.6 68.0-125 4.15 20
Styrene 5.00 4.00 4.09 80.0 81.8 73.0-130 2.22 20
1,1,1,2-Tetrachloroethane 5.00 4.48 4.55 89.6 91.0 75.0-125 1.55 20
Tetrachloroethene 5.00 5.47 5.63 109 113 72.0-132 2.88 20
Toluene 5.00 4.55 4.73 91.0 94.6 79.0-120 3.88 20
1,1,1-Trichloroethane 5.00 5.09 5.09 102 102 73.0-124 0.000 20
1,1,2-Trichloroethane 5.00 4.70 4.77 94.0 95.4 80.0-120 1.48 20
Trichloroethene 5.00 4.93 4.79 98.6 95.8 78.0-124 2.88 20
Trichlorofluoromethane 5.00 3.16 3.30 63.2 66.0 59.0-147 4.33 20
Vinyl chloride 5.00 5.05 5.00 101 100 67.0-131 0.995 20
o-Xylene 5.00 4.08 4.13 81.6 82.6 80.0-122 1.22 20
m&p-Xylenes 10.0 8.81 9.24 88.1 92.4 80.0-122 4.76 20
tert-Amyl Methyl Ether 5.00 4.12 4.22 82.4 84.4 66.0-125 2.40 20
Ethyl tert-butyl ether 5.00 4.24 4.28 84.8 85.6 63.0-138 0.939 20
tert-Butyl alcohol 25.0 20.0 23.3 80.0 93.2 27.0-160 15.2 30
t-Amyl Alcohol 25.0 22.7 24.2 90.8 96.8 50.0-160 6.40 25
(S) Toluene-d8 96.3 98.5 80.0-120
(S) 4-Bromofluorobenzene 88.1 88.8 77.0-126
(S) 1,2-Dichloroethane-d4 96.7 96.8 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3941359-3 06/24/23 22:27
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
tert-Butyl formate 100 67.3 67.3 10.0-160
(S) Toluene-d8 101 80.0-120
(S) 4-Bromofluorobenzene 88.9 77.0-126
(S) 1,2-Dichloroethane-d4 93.8 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 52 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 52 of 69
QUALITY CONTROL SUMMARYWG2084660
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1626779-13
Method Blank (MB)
(MB) R3942851-3 06/28/23 11:28
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Bromobenzene U 0.118 1.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.0993 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,4-Trimethylbenzene U 0.322 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
ethanol U 42.0 100
(S) Toluene-d8 115 80.0-120
(S) 4-Bromofluorobenzene 113 77.0-126
(S) 1,2-Dichloroethane-d4 109 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3942851-1 06/28/23 10:24 • (LCSD) R3942851-2 06/28/23 10:45
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Bromobenzene 5.00 4.40 4.24 88.0 84.8 73.0-121 3.70 20
n-Butylbenzene 5.00 4.65 3.96 93.0 79.2 73.0-125 16.0 20
sec-Butylbenzene 5.00 4.66 4.17 93.2 83.4 75.0-125 11.1 20
tert-Butylbenzene 5.00 4.77 4.34 95.4 86.8 76.0-124 9.44 20
2-Chlorotoluene 5.00 4.68 4.32 93.6 86.4 76.0-123 8.00 20
4-Chlorotoluene 5.00 4.71 4.22 94.2 84.4 75.0-122 11.0 20
1,2-Dibromo-3-Chloropropane 5.00 4.75 4.50 95.0 90.0 58.0-134 5.41 20
1,2-Dichlorobenzene 5.00 4.91 4.60 98.2 92.0 79.0-121 6.52 20
1,3-Dichlorobenzene 5.00 5.03 4.48 101 89.6 79.0-120 11.6 20
1,4-Dichlorobenzene 5.00 4.68 4.40 93.6 88.0 79.0-120 6.17 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 53 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 53 of 69
QUALITY CONTROL SUMMARYWG2084660
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1626779-13
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3942851-1 06/28/23 10:24 • (LCSD) R3942851-2 06/28/23 10:45
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Hexachloro-1,3-butadiene 5.00 5.59 4.88 112 97.6 54.0-138 13.6 20
Naphthalene 5.00 4.71 4.76 94.2 95.2 54.0-135 1.06 20
n-Propylbenzene 5.00 4.64 4.18 92.8 83.6 77.0-124 10.4 20
1,1,2,2-Tetrachloroethane 5.00 4.63 4.46 92.6 89.2 65.0-130 3.74 20
1,2,3-Trichlorobenzene 5.00 5.21 5.11 104 102 50.0-138 1.94 20
1,2,4-Trichlorobenzene 5.00 5.17 4.75 103 95.0 57.0-137 8.47 20
1,2,3-Trichloropropane 5.00 4.97 4.80 99.4 96.0 73.0-130 3.48 20
1,2,4-Trimethylbenzene 5.00 4.83 4.36 96.6 87.2 76.0-121 10.2 20
1,3,5-Trimethylbenzene 5.00 4.81 4.42 96.2 88.4 76.0-122 8.45 20
ethanol 250 235 222 94.0 88.8 10.0-160 5.69 30
(S) Toluene-d8 110 112 80.0-120
(S) 4-Bromofluorobenzene 111 110 77.0-126
(S) 1,2-Dichloroethane-d4 108 107 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 54 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 54 of 69
QUALITY CONTROL SUMMARYWG2083284
TPH by Method MADEPE L1626779-01,02,03,04,05,06,07,08,09,10,11,12,13
Method Blank (MB)
(MB) R3941178-1 06/24/23 10:34
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics U 33.3 100
Unadjusted C19-C36 Aliphatics 42.0 J 33.3 100
(S) 1-Chloro-octadecane 61.3 40.0-140
Method Blank (MB)
(MB) R3941208-1 06/24/23 11:12
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics U 33.3 100
(S) o-Terphenyl 57.5 40.0-140
(S) 2-Fluorobiphenyl 84.5 40.0-140
(S) 2-Bromonaphthalene 84.1 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3941178-2 06/24/23 10:56 • (LCSD) R3941178-3 06/24/23 11:18
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 469 453 78.2 75.5 40.0-140 3.47 25
Unadjusted C19-C36 Aliphatics 800 777 745 97.1 93.1 40.0-140 4.20 25
(S) 1-Chloro-octadecane 73.4 73.1 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3941208-2 06/24/23 11:34 • (LCSD) R3941208-3 06/24/23 12:21
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1410 1380 82.9 81.2 40.0-140 2.15 25
(S) o-Terphenyl 76.4 73.1 40.0-140
(S) 2-Fluorobiphenyl 91.0 85.8 40.0-140
(S) 2-Bromonaphthalene 86.9 81.8 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 55 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 55 of 69
QUALITY CONTROL SUMMARYWG2080645
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1626779-12,13
Method Blank (MB)
(MB) R3940681-2 06/22/23 01:54
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.0886 1.00
Acenaphthylene U 0.0921 1.00
Anthracene U 0.0804 1.00
Benzo(a)anthracene U 0.199 1.00
Benzo(b)fluoranthene U 0.130 1.00
Benzo(k)fluoranthene U 0.120 1.00
Benzo(g,h,i)perylene U 0.121 1.00
Benzo(a)pyrene U 0.0381 1.00
Bis(2-chlorethoxy)methane U 0.116 10.0
Bis(2-chloroethyl)ether U 0.137 10.0
2,2-Oxybis(1-Chloropropane)U 0.210 10.0
4-Bromophenyl-phenylether U 0.0877 10.0
2-Chloronaphthalene U 0.0648 1.00
4-Chlorophenyl-phenylether U 0.0926 10.0
Chrysene U 0.130 1.00
Dibenz(a,h)anthracene U 0.0644 1.00
3,3-Dichlorobenzidine U 0.212 10.0
2,4-Dinitrotoluene U 0.0983 10.0
2,6-Dinitrotoluene U 0.250 10.0
Fluoranthene U 0.102 1.00
Fluorene U 0.0844 1.00
Hexachlorobenzene U 0.0755 1.00
Hexachloro-1,3-butadiene U 0.0968 10.0
Hexachlorocyclopentadiene U 0.0598 10.0
Hexachloroethane U 0.127 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.143 10.0
Naphthalene U 0.159 1.00
Nitrobenzene U 0.297 10.0
n-Nitrosodimethylamine U 0.998 10.0
n-Nitrosodiphenylamine U 2.37 10.0
n-Nitrosodi-n-propylamine U 0.261 10.0
Phenanthrene U 0.112 1.00
Benzylbutyl phthalate U 0.765 3.00
Bis(2-ethylhexyl)phthalate U 0.895 3.00
Di-n-butyl phthalate U 0.453 3.00
Diethyl phthalate U 0.287 3.00
Dimethyl phthalate U 0.260 3.00
Di-n-octyl phthalate U 0.932 3.00
Pyrene U 0.107 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 56 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 56 of 69
QUALITY CONTROL SUMMARYWG2080645
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1626779-12,13
Method Blank (MB)
(MB) R3940681-2 06/22/23 01:54
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
1,2,4-Trichlorobenzene U 0.0698 10.0
4-Chloro-3-methylphenol U 0.131 10.0
2-Chlorophenol U 0.133 10.0
2,4-Dichlorophenol U 0.102 10.0
2,4-Dimethylphenol U 0.0636 10.0
4,6-Dinitro-2-methylphenol U 1.12 10.0
2,4-Dinitrophenol U 5.93 10.0
2-Nitrophenol U 0.117 10.0
4-Nitrophenol U 0.143 10.0
Pentachlorophenol U 0.313 10.0
Phenol U 4.33 10.0
2,4,6-Trichlorophenol U 0.100 10.0
(S) Nitrobenzene-d5 80.9 15.0-314
(S) 2-Fluorobiphenyl 67.0 22.0-127
(S) p-Terphenyl-d14 76.4 29.0-141
(S) Phenol-d5 24.9 8.00-424
(S) 2-Fluorophenol 33.9 10.0-120
(S) 2,4,6-Tribromophenol 71.5 10.0-153
Laboratory Control Sample (LCS)
(LCS) R3940681-1 06/22/23 01:27
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acenaphthene 50.0 37.3 74.6 47.0-145
Acenaphthylene 50.0 38.8 77.6 33.0-145
Anthracene 50.0 39.8 79.6 27.0-133
Benzo(a)anthracene 50.0 43.6 87.2 33.0-143
Benzo(b)fluoranthene 50.0 39.6 79.2 24.0-159
Benzo(k)fluoranthene 50.0 38.7 77.4 11.0-162
Benzo(g,h,i)perylene 50.0 42.8 85.6 1.00-219
Benzo(a)pyrene 50.0 41.6 83.2 17.0-163
Bis(2-chlorethoxy)methane 50.0 38.0 76.0 1.00-219
Bis(2-chloroethyl)ether 50.0 37.2 74.4 33.0-185
2,2-Oxybis(1-Chloropropane)50.0 31.1 62.2 36.0-166
4-Bromophenyl-phenylether 50.0 39.2 78.4 53.0-127
2-Chloronaphthalene 50.0 34.5 69.0 60.0-120
4-Chlorophenyl-phenylether 50.0 41.4 82.8 25.0-158
Chrysene 50.0 41.3 82.6 17.0-168
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 57 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 57 of 69
QUALITY CONTROL SUMMARYWG2080645
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1626779-12,13
Laboratory Control Sample (LCS)
(LCS) R3940681-1 06/22/23 01:27
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Dibenz(a,h)anthracene 50.0 43.7 87.4 1.00-227
3,3-Dichlorobenzidine 100 65.5 65.5 1.00-262
2,4-Dinitrotoluene 50.0 51.2 102 39.0-139
2,6-Dinitrotoluene 50.0 45.1 90.2 50.0-158
Fluoranthene 50.0 46.0 92.0 26.0-137
Fluorene 50.0 39.8 79.6 59.0-121
Hexachlorobenzene 50.0 38.8 77.6 1.00-152
Hexachloro-1,3-butadiene 50.0 34.8 69.6 24.0-120
Hexachlorocyclopentadiene 50.0 14.3 28.6 10.0-120
Hexachloroethane 50.0 28.4 56.8 40.0-120
Indeno(1,2,3-cd)pyrene 50.0 39.8 79.6 1.00-171
Isophorone 50.0 41.8 83.6 21.0-196
Naphthalene 50.0 30.8 61.6 21.0-133
Nitrobenzene 50.0 41.5 83.0 35.0-180
n-Nitrosodimethylamine 50.0 35.0 70.0 10.0-120
n-Nitrosodiphenylamine 50.0 33.3 66.6 44.0-120
n-Nitrosodi-n-propylamine 50.0 43.4 86.8 1.00-230
Phenanthrene 50.0 39.3 78.6 54.0-120
Benzylbutyl phthalate 50.0 42.8 85.6 1.00-152
Bis(2-ethylhexyl)phthalate 50.0 41.5 83.0 8.00-158
Di-n-butyl phthalate 50.0 46.1 92.2 1.00-120
Diethyl phthalate 50.0 45.5 91.0 1.00-120
Dimethyl phthalate 50.0 43.1 86.2 1.00-120
Di-n-octyl phthalate 50.0 43.9 87.8 4.00-146
Pyrene 50.0 38.3 76.6 52.0-120
1,2,4-Trichlorobenzene 50.0 31.0 62.0 44.0-142
4-Chloro-3-methylphenol 50.0 37.9 75.8 22.0-147
2-Chlorophenol 50.0 26.9 53.8 23.0-134
2,4-Dichlorophenol 50.0 33.6 67.2 39.0-135
2,4-Dimethylphenol 50.0 35.4 70.8 32.0-120
4,6-Dinitro-2-methylphenol 50.0 58.3 117 1.00-181
2,4-Dinitrophenol 50.0 60.4 121 1.00-191
2-Nitrophenol 50.0 37.8 75.6 29.0-182
4-Nitrophenol 50.0 125 250 1.00-132 J4
Pentachlorophenol 50.0 38.3 76.6 14.0-176
Phenol 50.0 16.1 32.2 5.00-120
2,4,6-Trichlorophenol 50.0 40.5 81.0 37.0-144
(S) Nitrobenzene-d5 75.6 15.0-314
(S) 2-Fluorobiphenyl 72.7 22.0-127
(S) p-Terphenyl-d14 75.0 29.0-141
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 58 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 58 of 69
QUALITY CONTROL SUMMARYWG2080645
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1626779-12,13
Laboratory Control Sample (LCS)
(LCS) R3940681-1 06/22/23 01:27
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
(S) Phenol-d5 28.3 8.00-424
(S) 2-Fluorophenol 35.8 10.0-120
(S) 2,4,6-Tribromophenol 76.5 10.0-153
L1626959-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1626959-02 06/22/23 05:51 • (MS) R3940681-3 06/22/23 06:13 • (MSD) R3940681-4 06/22/23 06:34
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Acenaphthene 50.0 ND 38.2 38.1 76.4 76.2 1 47.0-145 0.262 48
Acenaphthylene 50.0 ND 28.5 26.4 57.0 52.8 1 33.0-145 7.65 74
Anthracene 50.0 ND 36.8 35.6 73.6 71.2 1 27.0-133 3.31 66
Benzo(a)anthracene 50.0 ND 40.8 39.6 81.6 79.2 1 33.0-143 2.99 53
Benzo(b)fluoranthene 50.0 ND 39.2 38.3 78.4 76.6 1 24.0-159 2.32 71
Benzo(k)fluoranthene 50.0 ND 38.2 36.9 76.4 73.8 1 11.0-162 3.46 63
Benzo(g,h,i)perylene 50.0 ND 37.4 36.8 74.8 73.6 1 1.00-219 1.62 97
Benzo(a)pyrene 50.0 ND 26.1 29.6 52.2 59.2 1 17.0-163 12.6 72
Bis(2-chlorethoxy)methane 50.0 ND 36.9 36.9 73.8 73.8 1 33.0-184 0.000 54
Bis(2-chloroethyl)ether 50.0 ND 37.1 36.7 74.2 73.4 1 12.0-158 1.08 108
2,2-Oxybis(1-Chloropropane)50.0 ND 32.3 31.7 64.6 63.4 1 36.0-166 1.87 76
4-Bromophenyl-phenylether 50.0 ND 41.6 41.6 83.2 83.2 1 53.0-127 0.000 43
2-Chloronaphthalene 50.0 ND 36.5 37.4 73.0 74.8 1 60.0-120 2.44 24
4-Chlorophenyl-phenylether 50.0 ND 42.0 41.3 84.0 82.6 1 25.0-158 1.68 61
Chrysene 50.0 ND 40.7 39.6 81.4 79.2 1 17.0-168 2.74 87
Dibenz(a,h)anthracene 50.0 ND 41.3 40.0 82.6 80.0 1 1.00-227 3.20 126
3,3-Dichlorobenzidine 100 ND ND ND 0.000 0.000 1 1.00-262 J6 J6 0.000 108
2,4-Dinitrotoluene 50.0 ND 47.7 46.8 95.4 93.6 1 39.0-139 1.90 42
2,6-Dinitrotoluene 50.0 ND 42.9 43.0 85.8 86.0 1 50.0-158 0.233 48
Fluoranthene 50.0 ND 43.9 42.7 87.8 85.4 1 26.0-137 2.77 66
Fluorene 50.0 ND 40.1 39.3 80.2 78.6 1 59.0-121 2.02 38
Hexachlorobenzene 50.0 ND 41.4 40.7 82.8 81.4 1 1.00-152 1.71 55
Hexachloro-1,3-butadiene 50.0 ND 39.7 40.9 79.4 81.8 1 24.0-120 2.98 62
Hexachlorocyclopentadiene 50.0 ND 27.4 31.1 54.8 62.2 1 10.0-146 12.6 34
Hexachloroethane 50.0 ND 29.8 31.6 59.6 63.2 1 40.0-120 5.86 52
Indeno(1,2,3-cd)pyrene 50.0 ND 37.1 37.0 74.2 74.0 1 1.00-171 0.270 99
Isophorone 50.0 ND 41.7 41.8 83.4 83.6 1 21.0-196 0.240 93
Naphthalene 50.0 ND 32.3 33.6 64.6 67.2 1 21.0-133 3.95 65
Nitrobenzene 50.0 ND 57.4 61.7 115 123 1 35.0-180 7.22 62
n-Nitrosodimethylamine 50.0 ND 42.7 39.5 85.4 79.0 1 10.0-120 7.79 40
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 59 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 59 of 69
QUALITY CONTROL SUMMARYWG2080645
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1626779-12,13
L1626959-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1626959-02 06/22/23 05:51 • (MS) R3940681-3 06/22/23 06:13 • (MSD) R3940681-4 06/22/23 06:34
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
n-Nitrosodiphenylamine 50.0 ND 32.3 32.6 64.6 65.2 1 16.0-160 0.925 28
n-Nitrosodi-n-propylamine 50.0 ND 40.6 40.7 81.2 81.4 1 1.00-230 0.246 87
Phenanthrene 50.0 ND 38.8 38.1 77.6 76.2 1 54.0-120 1.82 39
Benzylbutyl phthalate 50.0 ND 44.2 42.2 88.4 84.4 1 1.00-152 4.63 60
Bis(2-ethylhexyl)phthalate 50.0 ND 38.3 36.9 76.6 73.8 1 8.00-158 3.72 82
Di-n-butyl phthalate 50.0 ND 44.3 43.8 88.6 87.6 1 1.00-120 1.14 47
Diethyl phthalate 50.0 ND 43.3 42.6 85.8 84.4 1 1.00-120 1.63 100
Dimethyl phthalate 50.0 ND 40.2 39.8 80.4 79.6 1 1.00-120 1.00 183
Di-n-octyl phthalate 50.0 ND 38.7 37.9 77.4 75.8 1 4.00-146 2.09 69
Pyrene 50.0 ND 38.3 36.8 76.6 73.6 1 52.0-120 3.99 49
1,2,4-Trichlorobenzene 50.0 ND 34.8 37.3 69.6 74.6 1 44.0-142 6.93 50
4-Chloro-3-methylphenol 50.0 ND 28.1 27.7 56.2 55.4 1 22.0-147 1.43 73
2-Chlorophenol 50.0 ND 25.4 28.1 50.8 56.2 1 23.0-134 10.1 61
2,4-Dichlorophenol 50.0 ND 31.3 33.2 62.6 66.4 1 39.0-135 5.89 50
2,4-Dimethylphenol 50.0 ND ND ND 0.624 0.534 1 32.0-120 J6 J6 15.5 58
4,6-Dinitro-2-methylphenol 50.0 ND 54.2 57.5 108 115 1 1.00-181 5.91 203
2,4-Dinitrophenol 50.0 ND 59.7 65.8 119 132 1 1.00-191 9.72 132
2-Nitrophenol 50.0 ND 42.3 44.7 84.6 89.4 1 29.0-182 5.52 55
4-Nitrophenol 50.0 ND 131 134 262 268 1 1.00-132 J5 J5 2.26 131
Pentachlorophenol 50.0 ND 38.7 44.8 77.4 89.6 1 14.0-176 14.6 86
Phenol 50.0 ND 16.3 16.5 32.6 33.0 1 5.00-120 1.22 64
2,4,6-Trichlorophenol 50.0 ND 38.5 40.0 77.0 80.0 1 37.0-144 3.82 58
(S) Nitrobenzene-d5 76.4 84.3 15.0-314
(S) 2-Fluorobiphenyl 74.1 76.5 22.0-127
(S) p-Terphenyl-d14 74.9 72.2 29.0-141
(S) Phenol-d5 26.6 26.6 8.00-424
(S) 2-Fluorophenol 38.6 39.7 10.0-120
(S) 2,4,6-Tribromophenol 60.5 62.0 10.0-153
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 60 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 60 of 69
QUALITY CONTROL SUMMARYWG2082003
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1626779-01,02,03,04,05,06,07,08,09,10,11
Method Blank (MB)
(MB) R3940674-3 06/22/23 02:14
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.0886 1.00
Acenaphthylene U 0.0921 1.00
Anthracene U 0.0804 1.00
Benzo(a)anthracene U 0.199 1.00
Benzo(b)fluoranthene U 0.130 1.00
Benzo(k)fluoranthene U 0.120 1.00
Benzo(g,h,i)perylene U 0.121 1.00
Benzo(a)pyrene U 0.0381 1.00
Bis(2-chlorethoxy)methane U 0.116 10.0
Bis(2-chloroethyl)ether U 0.137 10.0
2,2-Oxybis(1-Chloropropane)U 0.210 10.0
4-Bromophenyl-phenylether U 0.0877 10.0
2-Chloronaphthalene U 0.0648 1.00
4-Chlorophenyl-phenylether U 0.0926 10.0
Chrysene U 0.130 1.00
Dibenz(a,h)anthracene U 0.0644 1.00
3,3-Dichlorobenzidine U 0.212 10.0
2,4-Dinitrotoluene U 0.0983 10.0
2,6-Dinitrotoluene U 0.250 10.0
Fluoranthene U 0.102 1.00
Fluorene U 0.0844 1.00
Hexachlorobenzene U 0.0755 1.00
Hexachloro-1,3-butadiene U 0.0968 10.0
Hexachlorocyclopentadiene U 0.0598 10.0
Hexachloroethane U 0.127 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.143 10.0
Naphthalene U 0.159 1.00
Nitrobenzene U 0.297 10.0
n-Nitrosodimethylamine U 0.998 10.0
n-Nitrosodiphenylamine U 2.37 10.0
n-Nitrosodi-n-propylamine U 0.261 10.0
Phenanthrene U 0.112 1.00
Benzylbutyl phthalate U 0.765 3.00
Bis(2-ethylhexyl)phthalate U 0.895 3.00
Di-n-butyl phthalate U 0.453 3.00
Diethyl phthalate U 0.287 3.00
Dimethyl phthalate U 0.260 3.00
Di-n-octyl phthalate U 0.932 3.00
Pyrene U 0.107 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 61 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 61 of 69
QUALITY CONTROL SUMMARYWG2082003
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1626779-01,02,03,04,05,06,07,08,09,10,11
Method Blank (MB)
(MB) R3940674-3 06/22/23 02:14
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
1,2,4-Trichlorobenzene U 0.0698 10.0
4-Chloro-3-methylphenol U 0.131 10.0
2-Chlorophenol U 0.133 10.0
2,4-Dichlorophenol U 0.102 10.0
2,4-Dimethylphenol U 0.0636 10.0
4,6-Dinitro-2-methylphenol U 1.12 10.0
2,4-Dinitrophenol U 5.93 10.0
2-Nitrophenol U 0.117 10.0
4-Nitrophenol U 0.143 10.0
Pentachlorophenol U 0.313 10.0
Phenol U 4.33 10.0
2,4,6-Trichlorophenol U 0.100 10.0
(S) Nitrobenzene-d5 64.8 15.0-314
(S) 2-Fluorobiphenyl 49.0 22.0-127
(S) p-Terphenyl-d14 88.9 29.0-141
(S) Phenol-d5 20.5 8.00-424
(S) 2-Fluorophenol 22.1 10.0-120
(S) 2,4,6-Tribromophenol 43.9 10.0-153
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3940674-1 06/22/23 01:20 • (LCSD) R3940674-2 06/22/23 01:52
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acenaphthene 50.0 46.2 38.8 92.4 77.6 47.0-145 17.4 48
Acenaphthylene 50.0 44.3 39.7 88.6 79.4 33.0-145 11.0 74
Anthracene 50.0 50.4 44.0 101 88.0 27.0-133 13.6 66
Benzo(a)anthracene 50.0 54.4 46.2 109 92.4 33.0-143 16.3 53
Benzo(b)fluoranthene 50.0 62.1 45.6 124 91.2 24.0-159 30.6 71
Benzo(k)fluoranthene 50.0 55.8 44.5 112 89.0 11.0-162 22.5 63
Benzo(g,h,i)perylene 50.0 52.2 40.7 104 81.4 1.00-219 24.8 97
Benzo(a)pyrene 50.0 52.2 44.1 104 88.2 17.0-163 16.8 72
Bis(2-chlorethoxy)methane 50.0 47.3 44.6 94.6 89.2 1.00-219 5.88 54
Bis(2-chloroethyl)ether 50.0 50.0 41.6 100 83.2 33.0-185 18.3 108
2,2-Oxybis(1-Chloropropane)50.0 38.7 34.7 77.4 69.4 36.0-166 10.9 76
4-Bromophenyl-phenylether 50.0 43.1 36.6 86.2 73.2 53.0-127 16.3 43
2-Chloronaphthalene 50.0 41.7 36.8 83.4 73.6 60.0-120 12.5 24
4-Chlorophenyl-phenylether 50.0 36.9 35.1 73.8 70.2 25.0-158 5.00 61
Chrysene 50.0 53.2 42.9 106 85.8 17.0-168 21.4 87
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 62 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 62 of 69
QUALITY CONTROL SUMMARYWG2082003
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1626779-01,02,03,04,05,06,07,08,09,10,11
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3940674-1 06/22/23 01:20 • (LCSD) R3940674-2 06/22/23 01:52
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Dibenz(a,h)anthracene 50.0 47.0 42.3 94.0 84.6 1.00-227 10.5 126
3,3-Dichlorobenzidine 100 73.2 69.4 73.2 69.4 1.00-262 5.33 108
2,4-Dinitrotoluene 50.0 50.7 43.1 101 86.2 39.0-139 16.2 42
2,6-Dinitrotoluene 50.0 45.0 41.1 90.0 82.2 50.0-158 9.06 48
Fluoranthene 50.0 43.2 37.4 86.4 74.8 26.0-137 14.4 66
Fluorene 50.0 40.9 38.1 81.8 76.2 59.0-121 7.09 38
Hexachlorobenzene 50.0 43.3 35.2 86.6 70.4 1.00-152 20.6 55
Hexachloro-1,3-butadiene 50.0 24.9 19.5 49.8 39.0 24.0-120 24.3 62
Hexachlorocyclopentadiene 50.0 14.5 10.8 29.0 21.6 10.0-120 29.2 31
Hexachloroethane 50.0 36.2 30.3 72.4 60.6 40.0-120 17.7 52
Indeno(1,2,3-cd)pyrene 50.0 40.9 33.6 81.8 67.2 1.00-171 19.6 99
Isophorone 50.0 47.8 47.3 95.6 94.6 21.0-196 1.05 93
Naphthalene 50.0 35.9 31.3 71.8 62.6 21.0-133 13.7 65
Nitrobenzene 50.0 44.2 43.5 88.4 87.0 35.0-180 1.60 62
n-Nitrosodimethylamine 50.0 32.7 26.9 65.4 53.8 10.0-120 19.5 34
n-Nitrosodiphenylamine 50.0 43.6 37.0 87.2 74.0 44.0-120 16.4 21
n-Nitrosodi-n-propylamine 50.0 57.6 54.6 115 109 1.00-230 5.35 87
Phenanthrene 50.0 51.6 44.3 103 88.6 54.0-120 15.2 39
Benzylbutyl phthalate 50.0 67.9 59.2 136 118 1.00-152 13.7 60
Bis(2-ethylhexyl)phthalate 50.0 69.0 59.0 138 118 8.00-158 15.6 82
Di-n-butyl phthalate 50.0 56.8 55.1 114 110 1.00-120 3.04 47
Diethyl phthalate 50.0 49.6 42.5 99.2 85.0 1.00-120 15.4 100
Dimethyl phthalate 50.0 45.3 41.3 90.6 82.6 1.00-120 9.24 183
Di-n-octyl phthalate 50.0 56.2 48.4 112 96.8 4.00-146 14.9 69
Pyrene 50.0 58.4 51.0 117 102 52.0-120 13.5 49
1,2,4-Trichlorobenzene 50.0 27.5 23.0 55.0 46.0 44.0-142 17.8 50
4-Chloro-3-methylphenol 50.0 32.6 30.5 65.2 61.0 22.0-147 6.66 73
2-Chlorophenol 50.0 26.1 23.0 52.2 46.0 23.0-134 12.6 61
2,4-Dichlorophenol 50.0 26.0 23.7 52.0 47.4 39.0-135 9.26 50
2,4-Dimethylphenol 50.0 30.2 29.0 60.4 58.0 32.0-120 4.05 58
4,6-Dinitro-2-methylphenol 50.0 54.3 51.6 109 103 1.00-181 5.10 203
2,4-Dinitrophenol 50.0 39.0 35.6 78.0 71.2 1.00-191 9.12 132
2-Nitrophenol 50.0 30.9 30.5 61.8 61.0 29.0-182 1.30 55
4-Nitrophenol 50.0 15.0 14.4 30.0 28.8 1.00-132 4.08 131
Pentachlorophenol 50.0 32.9 26.1 65.8 52.2 14.0-176 23.1 86
Phenol 50.0 16.0 14.2 32.0 28.4 5.00-120 11.9 64
2,4,6-Trichlorophenol 50.0 40.0 33.1 80.0 66.2 37.0-144 18.9 58
(S) Nitrobenzene-d5 82.5 85.1 15.0-314
(S) 2-Fluorobiphenyl 75.8 67.1 22.0-127
(S) p-Terphenyl-d14 103 85.5 29.0-141
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 63 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 63 of 69
QUALITY CONTROL SUMMARYWG2082003
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1626779-01,02,03,04,05,06,07,08,09,10,11
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3940674-1 06/22/23 01:20 • (LCSD) R3940674-2 06/22/23 01:52
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
(S) Phenol-d5 29.6 26.1 8.00-424
(S) 2-Fluorophenol 30.1 25.9 10.0-120
(S) 2,4,6-Tribromophenol 70.0 57.5 10.0-153
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 64 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 64 of 69
GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
C4 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low.
Data is likely to show a low bias concerning the result.
J The identification of the analyte is acceptable; the reported value is an estimate.
J1 Surrogate recovery limits have been exceeded; values are outside upper control limits.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 65 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 65 of 69

Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 66 of 69
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
S&ME Inc. - Raleigh NC 210818 L1626779 06/29/23 15:39 66 of 69
ANALYTICAL REPORT
September 29, 2023
Colonial Pipeline- S&ME Raleigh
Sample Delivery Group:L1655691
Samples Received:09/14/2023
Project Number:210818
Description:Colonial Pipeline - Jennifer Drive
Report To:Mr. Michael Pfeifer
3201 Spring Forrest Road
Raleigh, NC 27616
Entire Report Reviewed By:
September 29, 2023
[Preliminary Report]
Craig Cothron
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 1 of 78
September 29, 2023
Craig Cothron
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 1 of 78
TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 6
Sr: Sample Results 7
MW-2 L1655691-01 7
MW-3 L1655691-02 10
MW-5 L1655691-03 13
MW-6 L1655691-04 16
MW-7 L1655691-05 19
MW-8 L1655691-06 22
MW-9 L1655691-07 25
MW-12 L1655691-08 28
MW-13 L1655691-09 31
MW-1D L1655691-10 34
MW-4D L1655691-11 37
MW-5D L1655691-12 40
MW-6D L1655691-13 43
Qc: Quality Control Summary 46
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 46
TPH by Method MADEPE 61
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 65
Gl: Glossary of Terms 74
Al: Accreditations & Locations 75
Sc: Sample Chain of Custody 76
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 2 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 2 of 78
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-2 L1655691-01 GW BB/JW 09/12/23 14:05 09/14/23 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2135178 1 09/21/23 00:11 09/21/23 00:11 JCP Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2135339 1 09/20/23 09:14 09/20/23 09:14 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2134808 1 09/19/23 02:46 09/20/23 01:24 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2134808 1 09/19/23 02:46 09/20/23 05:06 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2132824 1 09/16/23 06:22 09/17/23 17:54 AMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-3 L1655691-02 GW BB/JW 09/12/23 12:20 09/14/23 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2136913 100 09/22/23 00:11 09/22/23 00:11 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2137497 100 09/22/23 18:32 09/22/23 18:32 TJJ Mt. Juliet, TN
TPH by Method MADEPE WG2135760 1 09/20/23 03:35 09/20/23 22:10 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2135760 1 09/20/23 03:35 09/21/23 05:11 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2132824 1 09/16/23 06:22 09/17/23 18:16 AMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-5 L1655691-03 GW BB/JW 09/12/23 13:05 09/14/23 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2135178 1 09/21/23 00:31 09/21/23 00:31 JCP Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2135339 1 09/20/23 09:36 09/20/23 09:36 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2135760 1 09/20/23 03:35 09/20/23 22:32 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2135760 1 09/20/23 03:35 09/21/23 04:49 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2132824 1 09/16/23 06:22 09/17/23 18:38 AMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-6 L1655691-04 GW BB/JW 09/12/23 12:25 09/14/23 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2135178 1 09/21/23 00:51 09/21/23 00:51 JCP Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2135339 1 09/20/23 09:57 09/20/23 09:57 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2139497 1 09/25/23 19:45 09/27/23 16:31 JDG Mt. Juliet, TN
TPH by Method MADEPE WG2139497 1 09/25/23 19:45 09/27/23 18:08 JDG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2132824 1 09/16/23 06:22 09/17/23 18:59 AMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-7 L1655691-05 GW BB/JW 09/12/23 13:25 09/14/23 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2135178 1 09/21/23 01:12 09/21/23 01:12 JCP Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2135339 1 09/20/23 10:18 09/20/23 10:18 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2135760 1 09/20/23 03:35 09/20/23 23:16 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2135760 1 09/20/23 03:35 09/21/23 04:05 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2132824 1 09/16/23 06:22 09/17/23 14:40 AMG Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 3 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 3 of 78
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-8 L1655691-06 GW BB/JW 09/12/23 14:20 09/14/23 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2135178 1 09/21/23 01:32 09/21/23 01:32 JCP Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2135339 1 09/20/23 10:40 09/20/23 10:40 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2135760 1 09/20/23 03:35 09/20/23 23:39 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2135760 1 09/20/23 03:35 09/21/23 03:43 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2132824 1 09/16/23 06:22 09/17/23 15:01 AMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-9 L1655691-07 GW BB/JW 09/12/23 11:25 09/14/23 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2135178 1 09/21/23 01:53 09/21/23 01:53 JCP Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2135339 1 09/20/23 11:02 09/20/23 11:02 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2135760 1 09/20/23 03:35 09/21/23 00:01 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2135760 1 09/20/23 03:35 09/21/23 03:20 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2132824 1 09/16/23 06:22 09/17/23 15:23 AMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-12 L1655691-08 GW BB/JW 09/12/23 11:40 09/14/23 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2135999 1 09/21/23 17:58 09/21/23 17:58 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2137490 1 09/22/23 12:49 09/22/23 12:49 TJJ Mt. Juliet, TN
TPH by Method MADEPE WG2135760 1 09/20/23 03:35 09/21/23 00:23 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2135760 1 09/20/23 03:35 09/21/23 02:58 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2132824 1 09/16/23 06:22 09/17/23 15:45 AMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-13 L1655691-09 GW BB/JW 09/12/23 10:40 09/14/23 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2136913 1 09/21/23 22:20 09/21/23 22:20 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2137497 1 09/22/23 14:14 09/22/23 14:14 TJJ Mt. Juliet, TN
TPH by Method MADEPE WG2135760 1 09/20/23 03:35 09/21/23 00:45 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2135760 1 09/20/23 03:35 09/21/23 02:36 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2132824 1 09/16/23 06:22 09/17/23 16:06 AMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-1D L1655691-10 GW BB/JW 09/13/23 12:45 09/14/23 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2136913 1 09/21/23 22:41 09/21/23 22:41 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2137497 1 09/22/23 14:36 09/22/23 14:36 TJJ Mt. Juliet, TN
TPH by Method MADEPE WG2135760 1 09/20/23 03:35 09/21/23 01:07 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2135760 1 09/20/23 03:35 09/21/23 02:14 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2134767 1 09/20/23 20:08 09/21/23 03:38 AMG Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 4 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 4 of 78
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-4D L1655691-11 GW BB/JW 09/13/23 11:50 09/14/23 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2136913 50 09/22/23 00:32 09/22/23 00:32 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2137497 50 09/22/23 18:54 09/22/23 18:54 TJJ Mt. Juliet, TN
TPH by Method MADEPE WG2135760 1 09/20/23 03:35 09/21/23 01:29 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2135760 1 09/20/23 03:35 09/21/23 01:52 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2134767 1 09/20/23 20:08 09/21/23 03:59 AMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-5D L1655691-12 GW BB/JW 09/13/23 09:50 09/14/23 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2136913 1 09/21/23 23:03 09/21/23 23:03 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2137497 1 09/22/23 14:57 09/22/23 14:57 TJJ Mt. Juliet, TN
TPH by Method MADEPE WG2135760 1 09/20/23 03:35 09/21/23 07:15 HLJ Mt. Juliet, TN
TPH by Method MADEPE WG2135760 1 09/20/23 03:35 09/21/23 13:33 HLJ Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2134767 1 09/20/23 20:08 09/21/23 04:20 AMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-6D L1655691-13 GW BB/JW 09/13/23 10:50 09/14/23 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2136913 1 09/21/23 23:25 09/21/23 23:25 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2137497 1 09/22/23 15:19 09/22/23 15:19 TJJ Mt. Juliet, TN
TPH by Method MADEPE WG2135760 1 09/20/23 03:35 09/21/23 07:37 HLJ Mt. Juliet, TN
TPH by Method MADEPE WG2135760 1 09/20/23 03:35 09/21/23 13:11 HLJ Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2134767 1 09/20/23 20:08 09/21/23 04:42 AMG Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 5 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 5 of 78
CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Craig Cothron
Project Manager
Project Narrative
Benzidine is reporting with critically low recovery in the laboratory control sample(s). This compound is a method defined poor
performer. Results are estimated.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 6 of 78
Craig Cothron
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 6 of 78
SAMPLE RESULTS - 01
L1655691
MW-2
Collected date/time: 09/12/23 14:05
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.0941 1.00 1 09/20/2023 09:14 WG2135339
Bromobenzene U 0.118 1.00 1 09/20/2023 09:14 WG2135339
Bromodichloromethane U 0.136 1.00 1 09/20/2023 09:14 WG2135339
Bromochloromethane U 0.128 1.00 1 09/20/2023 09:14 WG2135339
Bromoform U 0.129 1.00 1 09/20/2023 09:14 WG2135339
Bromomethane U 0.605 5.00 1 09/21/2023 00:11 WG2135178
n-Butylbenzene U 0.157 1.00 1 09/20/2023 09:14 WG2135339
sec-Butylbenzene U 0.125 1.00 1 09/20/2023 09:14 WG2135339
tert-Butylbenzene U 0.127 1.00 1 09/20/2023 09:14 WG2135339
Carbon tetrachloride U 0.128 1.00 1 09/20/2023 09:14 WG2135339
Chlorobenzene U 0.116 1.00 1 09/20/2023 09:14 WG2135339
Chlorodibromomethane U 0.140 1.00 1 09/20/2023 09:14 WG2135339
Chloroethane U 0.192 5.00 1 09/20/2023 09:14 WG2135339
Chloroform U 0.111 5.00 1 09/20/2023 09:14 WG2135339
Chloromethane U 0.960 2.50 1 09/20/2023 09:14 WG2135339
2-Chlorotoluene U 0.106 1.00 1 09/20/2023 09:14 WG2135339
4-Chlorotoluene U 0.114 1.00 1 09/20/2023 09:14 WG2135339
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 09/20/2023 09:14 WG2135339
1,2-Dibromoethane U 0.126 1.00 1 09/20/2023 09:14 WG2135339
Dibromomethane U 0.122 1.00 1 09/20/2023 09:14 WG2135339
1,2-Dichlorobenzene U 0.107 1.00 1 09/20/2023 09:14 WG2135339
1,3-Dichlorobenzene U 0.110 1.00 1 09/20/2023 09:14 WG2135339
1,4-Dichlorobenzene U 0.120 1.00 1 09/20/2023 09:14 WG2135339
Dichlorodifluoromethane U 0.374 5.00 1 09/20/2023 09:14 WG2135339
1,1-Dichloroethane U 0.100 1.00 1 09/20/2023 09:14 WG2135339
1,2-Dichloroethane U 0.0819 1.00 1 09/20/2023 09:14 WG2135339
1,1-Dichloroethene U 0.188 1.00 1 09/20/2023 09:14 WG2135339
cis-1,2-Dichloroethene U 0.126 1.00 1 09/20/2023 09:14 WG2135339
trans-1,2-Dichloroethene U 0.149 1.00 1 09/20/2023 09:14 WG2135339
1,2-Dichloropropane U 0.149 1.00 1 09/20/2023 09:14 WG2135339
1,1-Dichloropropene U 0.142 1.00 1 09/20/2023 09:14 WG2135339
1,3-Dichloropropane U 0.110 1.00 1 09/20/2023 09:14 WG2135339
cis-1,3-Dichloropropene U 0.111 1.00 1 09/20/2023 09:14 WG2135339
trans-1,3-Dichloropropene U 0.118 1.00 1 09/20/2023 09:14 WG2135339
2,2-Dichloropropane U 0.161 1.00 1 09/20/2023 09:14 WG2135339
Di-isopropyl ether U 0.105 1.00 1 09/20/2023 09:14 WG2135339
Ethylbenzene U 0.137 1.00 1 09/20/2023 09:14 WG2135339
Hexachloro-1,3-butadiene U 0.337 1.00 1 09/20/2023 09:14 WG2135339
Isopropylbenzene U 0.105 1.00 1 09/20/2023 09:14 WG2135339
Methylene Chloride U 0.430 5.00 1 09/20/2023 09:14 WG2135339
Methyl tert-butyl ether U 0.101 1.00 1 09/20/2023 09:14 WG2135339
Naphthalene U 1.00 5.00 1 09/20/2023 09:14 WG2135339
n-Propylbenzene U 0.0993 1.00 1 09/20/2023 09:14 WG2135339
Styrene U 0.118 1.00 1 09/20/2023 09:14 WG2135339
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 09/20/2023 09:14 WG2135339
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 09/20/2023 09:14 WG2135339
Tetrachloroethene U 0.300 1.00 1 09/20/2023 09:14 WG2135339
Toluene U 0.278 1.00 1 09/20/2023 09:14 WG2135339
1,2,3-Trichlorobenzene U 0.230 1.00 1 09/20/2023 09:14 WG2135339
1,2,4-Trichlorobenzene U 0.481 1.00 1 09/20/2023 09:14 WG2135339
1,1,1-Trichloroethane U 0.149 1.00 1 09/20/2023 09:14 WG2135339
1,1,2-Trichloroethane U 0.158 1.00 1 09/20/2023 09:14 WG2135339
Trichloroethene U 0.190 1.00 1 09/20/2023 09:14 WG2135339
Trichlorofluoromethane U 0.160 5.00 1 09/21/2023 00:11 WG2135178
1,2,3-Trichloropropane U 0.237 2.50 1 09/20/2023 09:14 WG2135339
1,2,4-Trimethylbenzene U 0.322 1.00 1 09/20/2023 09:14 WG2135339
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 7 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 7 of 78
SAMPLE RESULTS - 01
L1655691
MW-2
Collected date/time: 09/12/23 14:05
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene U 0.104 1.00 1 09/20/2023 09:14 WG2135339
Vinyl chloride U 0.234 1.00 1 09/20/2023 09:14 WG2135339
o-Xylene U 0.174 1.00 1 09/20/2023 09:14 WG2135339
m&p-Xylenes U 0.430 2.00 1 09/20/2023 09:14 WG2135339
ethanol U 42.0 100 1 09/20/2023 09:14 WG2135339
tert-Amyl Methyl Ether U 0.195 1.00 1 09/20/2023 09:14 WG2135339
Ethyl tert-butyl ether U 0.101 1.00 1 09/20/2023 09:14 WG2135339
tert-Butyl alcohol U 4.06 5.00 1 09/20/2023 09:14 WG2135339
t-Amyl Alcohol U 4.90 50.0 1 09/20/2023 09:14 WG2135339
tert-Butyl formate U 4.51 20.0 1 09/20/2023 09:14 WG2135339
(S) Toluene-d8 101 80.0-120 09/21/2023 00:11 WG2135178
(S) Toluene-d8 97.1 80.0-120 09/20/2023 09:14 WG2135339
(S) 4-Bromofluorobenzene 104 77.0-126 09/21/2023 00:11 WG2135178
(S) 4-Bromofluorobenzene 93.3 77.0-126 09/20/2023 09:14 WG2135339
(S) 1,2-Dichloroethane-d4 83.6 70.0-130 09/21/2023 00:11 WG2135178
(S) 1,2-Dichloroethane-d4 99.4 70.0-130 09/20/2023 09:14 WG2135339
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics U 33.3 100 1 09/20/2023 05:06 WG2134808
Unadjusted C19-C36 Aliphatics U 33.3 100 1 09/20/2023 05:06 WG2134808
Unadjusted C11-C22 Aromatics 37.8 B J 33.3 100 1 09/20/2023 01:24 WG2134808
Unadjusted Total Petroleum
Hydrocarbons 37.8 J 33.3 100 1 09/20/2023 05:06 WG2134808
(S) o-Terphenyl 40.1 40.0-140 09/20/2023 01:24 WG2134808
(S) 1-Chloro-octadecane 15.4 J2 40.0-140 09/20/2023 05:06 WG2134808
(S) 2-Fluorobiphenyl 87.1 40.0-140 09/20/2023 01:24 WG2134808
(S) 2-Bromonaphthalene 87.8 40.0-140 09/20/2023 01:24 WG2134808
Sample Narrative:
L1655691-01 WG2134808: Sample produced heavy emulsion during Extraction process, low surr/spike recoveries due to matrix
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 09/17/2023 17:54 WG2132824
Acenaphthylene U 0.0921 1.00 1 09/17/2023 17:54 WG2132824
Anthracene U 0.0804 1.00 1 09/17/2023 17:54 WG2132824
Benzo(a)anthracene U 0.199 1.00 1 09/17/2023 17:54 WG2132824
Benzo(b)fluoranthene U 0.130 1.00 1 09/17/2023 17:54 WG2132824
Benzo(k)fluoranthene U 0.120 1.00 1 09/17/2023 17:54 WG2132824
Benzo(g,h,i)perylene U 0.121 1.00 1 09/17/2023 17:54 WG2132824
Benzo(a)pyrene U 0.0381 1.00 1 09/17/2023 17:54 WG2132824
Bis(2-chlorethoxy)methane U 0.116 10.0 1 09/17/2023 17:54 WG2132824
Bis(2-chloroethyl)ether U 0.137 10.0 1 09/17/2023 17:54 WG2132824
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 09/17/2023 17:54 WG2132824
4-Bromophenyl-phenylether U J4 0.0877 10.0 1 09/17/2023 17:54 WG2132824
2-Chloronaphthalene U J4 0.0648 1.00 1 09/17/2023 17:54 WG2132824
4-Chlorophenyl-phenylether U 0.0926 10.0 1 09/17/2023 17:54 WG2132824
Chrysene U 0.130 1.00 1 09/17/2023 17:54 WG2132824
Dibenz(a,h)anthracene U 0.0644 1.00 1 09/17/2023 17:54 WG2132824
3,3-Dichlorobenzidine U 0.212 10.0 1 09/17/2023 17:54 WG2132824
2,4-Dinitrotoluene U 0.0983 10.0 1 09/17/2023 17:54 WG2132824
2,6-Dinitrotoluene U 0.250 10.0 1 09/17/2023 17:54 WG2132824
Fluoranthene U 0.102 1.00 1 09/17/2023 17:54 WG2132824
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 8 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 8 of 78
SAMPLE RESULTS - 01
L1655691
MW-2
Collected date/time: 09/12/23 14:05
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Fluorene U J4 0.0844 1.00 1 09/17/2023 17:54 WG2132824
Hexachlorobenzene U 0.0755 1.00 1 09/17/2023 17:54 WG2132824
Hexachloro-1,3-butadiene U 0.0968 10.0 1 09/17/2023 17:54 WG2132824
Hexachlorocyclopentadiene U 0.0598 10.0 1 09/17/2023 17:54 WG2132824
Hexachloroethane U 0.127 10.0 1 09/17/2023 17:54 WG2132824
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 09/17/2023 17:54 WG2132824
Isophorone U 0.143 10.0 1 09/17/2023 17:54 WG2132824
Naphthalene U 0.159 1.00 1 09/17/2023 17:54 WG2132824
Nitrobenzene U 0.297 10.0 1 09/17/2023 17:54 WG2132824
n-Nitrosodimethylamine U 0.998 10.0 1 09/17/2023 17:54 WG2132824
n-Nitrosodiphenylamine U 2.37 10.0 1 09/17/2023 17:54 WG2132824
n-Nitrosodi-n-propylamine U 0.261 10.0 1 09/17/2023 17:54 WG2132824
Phenanthrene U J4 0.112 1.00 1 09/17/2023 17:54 WG2132824
Benzylbutyl phthalate U 0.765 3.00 1 09/17/2023 17:54 WG2132824
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 09/17/2023 17:54 WG2132824
Di-n-butyl phthalate U 0.453 3.00 1 09/17/2023 17:54 WG2132824
Diethyl phthalate U 0.287 3.00 1 09/17/2023 17:54 WG2132824
Dimethyl phthalate U 0.260 3.00 1 09/17/2023 17:54 WG2132824
Di-n-octyl phthalate U 0.932 3.00 1 09/17/2023 17:54 WG2132824
Pyrene U 0.107 1.00 1 09/17/2023 17:54 WG2132824
1,2,4-Trichlorobenzene U 0.0698 10.0 1 09/17/2023 17:54 WG2132824
4-Chloro-3-methylphenol U 0.131 10.0 1 09/17/2023 17:54 WG2132824
2-Chlorophenol U 0.133 10.0 1 09/17/2023 17:54 WG2132824
2,4-Dichlorophenol U 0.102 10.0 1 09/17/2023 17:54 WG2132824
2,4-Dimethylphenol U 0.0636 10.0 1 09/17/2023 17:54 WG2132824
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 09/17/2023 17:54 WG2132824
2,4-Dinitrophenol U 5.93 10.0 1 09/17/2023 17:54 WG2132824
2-Nitrophenol U 0.117 10.0 1 09/17/2023 17:54 WG2132824
4-Nitrophenol U 0.143 10.0 1 09/17/2023 17:54 WG2132824
Pentachlorophenol U 0.313 10.0 1 09/17/2023 17:54 WG2132824
Phenol U 4.33 10.0 1 09/17/2023 17:54 WG2132824
2,4,6-Trichlorophenol U 0.100 10.0 1 09/17/2023 17:54 WG2132824
(S) Nitrobenzene-d5 61.5 15.0-314 09/17/2023 17:54 WG2132824
(S) 2-Fluorobiphenyl 51.8 22.0-127 09/17/2023 17:54 WG2132824
(S) p-Terphenyl-d14 45.5 29.0-141 09/17/2023 17:54 WG2132824
(S) Phenol-d5 17.6 8.00-424 09/17/2023 17:54 WG2132824
(S) 2-Fluorophenol 24.5 10.0-120 09/17/2023 17:54 WG2132824
(S) 2,4,6-Tribromophenol 48.7 10.0-153 09/17/2023 17:54 WG2132824
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 9 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 9 of 78
SAMPLE RESULTS - 02
L1655691
MW-3
Collected date/time: 09/12/23 12:20
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene 4630 9.41 100 100 09/22/2023 00:11 WG2136913
Bromobenzene U 11.8 100 100 09/22/2023 00:11 WG2136913
Bromodichloromethane U 13.6 100 100 09/22/2023 00:11 WG2136913
Bromochloromethane U 12.8 100 100 09/22/2023 00:11 WG2136913
Bromoform U 12.9 100 100 09/22/2023 00:11 WG2136913
Bromomethane U 60.5 500 100 09/22/2023 18:32 WG2137497
n-Butylbenzene U 15.7 100 100 09/22/2023 00:11 WG2136913
sec-Butylbenzene U 12.5 100 100 09/22/2023 00:11 WG2136913
tert-Butylbenzene U 12.7 100 100 09/22/2023 00:11 WG2136913
Carbon tetrachloride U 12.8 100 100 09/22/2023 00:11 WG2136913
Chlorobenzene U 11.6 100 100 09/22/2023 00:11 WG2136913
Chlorodibromomethane U 14.0 100 100 09/22/2023 00:11 WG2136913
Chloroethane U 19.2 500 100 09/22/2023 00:11 WG2136913
Chloroform U 11.1 500 100 09/22/2023 00:11 WG2136913
Chloromethane U 96.0 250 100 09/22/2023 00:11 WG2136913
2-Chlorotoluene U 10.6 100 100 09/22/2023 00:11 WG2136913
4-Chlorotoluene U 11.4 100 100 09/22/2023 00:11 WG2136913
1,2-Dibromo-3-Chloropropane U 27.6 500 100 09/22/2023 00:11 WG2136913
1,2-Dibromoethane U 12.6 100 100 09/22/2023 00:11 WG2136913
Dibromomethane U 12.2 100 100 09/22/2023 00:11 WG2136913
1,2-Dichlorobenzene U 10.7 100 100 09/22/2023 00:11 WG2136913
1,3-Dichlorobenzene U 11.0 100 100 09/22/2023 00:11 WG2136913
1,4-Dichlorobenzene U 12.0 100 100 09/22/2023 00:11 WG2136913
Dichlorodifluoromethane U 37.4 500 100 09/22/2023 00:11 WG2136913
1,1-Dichloroethane U 10.0 100 100 09/22/2023 00:11 WG2136913
1,2-Dichloroethane U 8.19 100 100 09/22/2023 00:11 WG2136913
1,1-Dichloroethene U 18.8 100 100 09/22/2023 00:11 WG2136913
cis-1,2-Dichloroethene U 12.6 100 100 09/22/2023 00:11 WG2136913
trans-1,2-Dichloroethene U 14.9 100 100 09/22/2023 00:11 WG2136913
1,2-Dichloropropane U 14.9 100 100 09/22/2023 00:11 WG2136913
1,1-Dichloropropene U 14.2 100 100 09/22/2023 00:11 WG2136913
1,3-Dichloropropane U 11.0 100 100 09/22/2023 00:11 WG2136913
cis-1,3-Dichloropropene U 11.1 100 100 09/22/2023 00:11 WG2136913
trans-1,3-Dichloropropene U 11.8 100 100 09/22/2023 00:11 WG2136913
2,2-Dichloropropane U 16.1 100 100 09/22/2023 00:11 WG2136913
Di-isopropyl ether U 10.5 100 100 09/22/2023 00:11 WG2136913
Ethylbenzene 634 13.7 100 100 09/22/2023 18:32 WG2137497
Hexachloro-1,3-butadiene U 33.7 100 100 09/22/2023 00:11 WG2136913
Isopropylbenzene 47.1 J 10.5 100 100 09/22/2023 00:11 WG2136913
Methylene Chloride U 43.0 500 100 09/22/2023 00:11 WG2136913
Methyl tert-butyl ether U 10.1 100 100 09/22/2023 00:11 WG2136913
Naphthalene 160 J 100 500 100 09/22/2023 18:32 WG2137497
n-Propylbenzene 67.5 J 9.93 100 100 09/22/2023 00:11 WG2136913
Styrene U 11.8 100 100 09/22/2023 00:11 WG2136913
1,1,1,2-Tetrachloroethane U 14.7 100 100 09/22/2023 00:11 WG2136913
1,1,2,2-Tetrachloroethane U 13.3 100 100 09/22/2023 00:11 WG2136913
Tetrachloroethene U 30.0 100 100 09/22/2023 00:11 WG2136913
Toluene 8580 27.8 100 100 09/22/2023 00:11 WG2136913
1,2,3-Trichlorobenzene U 23.0 100 100 09/22/2023 00:11 WG2136913
1,2,4-Trichlorobenzene U 48.1 100 100 09/22/2023 00:11 WG2136913
1,1,1-Trichloroethane U 14.9 100 100 09/22/2023 00:11 WG2136913
1,1,2-Trichloroethane U 15.8 100 100 09/22/2023 00:11 WG2136913
Trichloroethene U 19.0 100 100 09/22/2023 00:11 WG2136913
Trichlorofluoromethane U 16.0 500 100 09/22/2023 18:32 WG2137497
1,2,3-Trichloropropane U 23.7 250 100 09/22/2023 00:11 WG2136913
1,2,4-Trimethylbenzene 822 32.2 100 100 09/22/2023 00:11 WG2136913
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 10 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 10 of 78
SAMPLE RESULTS - 02
L1655691
MW-3
Collected date/time: 09/12/23 12:20
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene 189 10.4 100 100 09/22/2023 00:11 WG2136913
Vinyl chloride U 23.4 100 100 09/22/2023 00:11 WG2136913
o-Xylene 1840 17.4 100 100 09/22/2023 00:11 WG2136913
m&p-Xylenes 4070 43.0 200 100 09/22/2023 00:11 WG2136913
ethanol U 4200 10000 100 09/22/2023 00:11 WG2136913
tert-Amyl Methyl Ether U 19.5 100 100 09/22/2023 00:11 WG2136913
Ethyl tert-butyl ether U 10.1 100 100 09/22/2023 00:11 WG2136913
tert-Butyl alcohol U 406 500 100 09/22/2023 00:11 WG2136913
t-Amyl Alcohol 4950 J 490 5000 100 09/22/2023 00:11 WG2136913
tert-Butyl formate U J4 451 2000 100 09/22/2023 00:11 WG2136913
(S) Toluene-d8 100 80.0-120 09/22/2023 00:11 WG2136913
(S) Toluene-d8 106 80.0-120 09/22/2023 18:32 WG2137497
(S) 4-Bromofluorobenzene 95.7 77.0-126 09/22/2023 00:11 WG2136913
(S) 4-Bromofluorobenzene 100 77.0-126 09/22/2023 18:32 WG2137497
(S) 1,2-Dichloroethane-d4 94.7 70.0-130 09/22/2023 00:11 WG2136913
(S) 1,2-Dichloroethane-d4 104 70.0-130 09/22/2023 18:32 WG2137497
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 45.4 B J 33.3 100 1 09/20/2023 22:10 WG2135760
Unadjusted C19-C36 Aliphatics 70.7 B J 33.3 100 1 09/20/2023 22:10 WG2135760
Unadjusted C11-C22 Aromatics 405 B 33.3 100 1 09/21/2023 05:11 WG2135760
Unadjusted Total Petroleum
Hydrocarbons 521 33.3 100 1 09/21/2023 05:11 WG2135760
(S) o-Terphenyl 86.1 40.0-140 09/21/2023 05:11 WG2135760
(S) 1-Chloro-octadecane 66.6 40.0-140 09/20/2023 22:10 WG2135760
(S) 2-Fluorobiphenyl 94.2 40.0-140 09/21/2023 05:11 WG2135760
(S) 2-Bromonaphthalene 100 40.0-140 09/21/2023 05:11 WG2135760
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 09/17/2023 18:16 WG2132824
Acenaphthylene U 0.0921 1.00 1 09/17/2023 18:16 WG2132824
Anthracene U 0.0804 1.00 1 09/17/2023 18:16 WG2132824
Benzo(a)anthracene U 0.199 1.00 1 09/17/2023 18:16 WG2132824
Benzo(b)fluoranthene U 0.130 1.00 1 09/17/2023 18:16 WG2132824
Benzo(k)fluoranthene U 0.120 1.00 1 09/17/2023 18:16 WG2132824
Benzo(g,h,i)perylene U 0.121 1.00 1 09/17/2023 18:16 WG2132824
Benzo(a)pyrene U 0.0381 1.00 1 09/17/2023 18:16 WG2132824
Bis(2-chlorethoxy)methane U 0.116 10.0 1 09/17/2023 18:16 WG2132824
Bis(2-chloroethyl)ether U 0.137 10.0 1 09/17/2023 18:16 WG2132824
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 09/17/2023 18:16 WG2132824
4-Bromophenyl-phenylether U J4 0.0877 10.0 1 09/17/2023 18:16 WG2132824
2-Chloronaphthalene U J4 0.0648 1.00 1 09/17/2023 18:16 WG2132824
4-Chlorophenyl-phenylether U 0.0926 10.0 1 09/17/2023 18:16 WG2132824
Chrysene U 0.130 1.00 1 09/17/2023 18:16 WG2132824
Dibenz(a,h)anthracene U 0.0644 1.00 1 09/17/2023 18:16 WG2132824
3,3-Dichlorobenzidine U 0.212 10.0 1 09/17/2023 18:16 WG2132824
2,4-Dinitrotoluene U 0.0983 10.0 1 09/17/2023 18:16 WG2132824
2,6-Dinitrotoluene U 0.250 10.0 1 09/17/2023 18:16 WG2132824
Fluoranthene U 0.102 1.00 1 09/17/2023 18:16 WG2132824
Fluorene U J4 0.0844 1.00 1 09/17/2023 18:16 WG2132824
Hexachlorobenzene U 0.0755 1.00 1 09/17/2023 18:16 WG2132824
Hexachloro-1,3-butadiene U 0.0968 10.0 1 09/17/2023 18:16 WG2132824
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 11 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 11 of 78
SAMPLE RESULTS - 02
L1655691
MW-3
Collected date/time: 09/12/23 12:20
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexachlorocyclopentadiene U 0.0598 10.0 1 09/17/2023 18:16 WG2132824
Hexachloroethane U 0.127 10.0 1 09/17/2023 18:16 WG2132824
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 09/17/2023 18:16 WG2132824
Isophorone U 0.143 10.0 1 09/17/2023 18:16 WG2132824
Naphthalene 54.5 0.159 1.00 1 09/17/2023 18:16 WG2132824
Nitrobenzene U 0.297 10.0 1 09/17/2023 18:16 WG2132824
n-Nitrosodimethylamine U 0.998 10.0 1 09/17/2023 18:16 WG2132824
n-Nitrosodiphenylamine U 2.37 10.0 1 09/17/2023 18:16 WG2132824
n-Nitrosodi-n-propylamine U 0.261 10.0 1 09/17/2023 18:16 WG2132824
Phenanthrene 0.156 J J4 0.112 1.00 1 09/17/2023 18:16 WG2132824
Benzylbutyl phthalate U 0.765 3.00 1 09/17/2023 18:16 WG2132824
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 09/17/2023 18:16 WG2132824
Di-n-butyl phthalate U 0.453 3.00 1 09/17/2023 18:16 WG2132824
Diethyl phthalate 0.366 J 0.287 3.00 1 09/17/2023 18:16 WG2132824
Dimethyl phthalate U 0.260 3.00 1 09/17/2023 18:16 WG2132824
Di-n-octyl phthalate U 0.932 3.00 1 09/17/2023 18:16 WG2132824
Pyrene U 0.107 1.00 1 09/17/2023 18:16 WG2132824
1,2,4-Trichlorobenzene U 0.0698 10.0 1 09/17/2023 18:16 WG2132824
4-Chloro-3-methylphenol U 0.131 10.0 1 09/17/2023 18:16 WG2132824
2-Chlorophenol U 0.133 10.0 1 09/17/2023 18:16 WG2132824
2,4-Dichlorophenol U 0.102 10.0 1 09/17/2023 18:16 WG2132824
2,4-Dimethylphenol U 0.0636 10.0 1 09/17/2023 18:16 WG2132824
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 09/17/2023 18:16 WG2132824
2,4-Dinitrophenol U 5.93 10.0 1 09/17/2023 18:16 WG2132824
2-Nitrophenol U 0.117 10.0 1 09/17/2023 18:16 WG2132824
4-Nitrophenol U 0.143 10.0 1 09/17/2023 18:16 WG2132824
Pentachlorophenol U 0.313 10.0 1 09/17/2023 18:16 WG2132824
Phenol U 4.33 10.0 1 09/17/2023 18:16 WG2132824
2,4,6-Trichlorophenol U 0.100 10.0 1 09/17/2023 18:16 WG2132824
(S) Nitrobenzene-d5 52.1 15.0-314 09/17/2023 18:16 WG2132824
(S) 2-Fluorobiphenyl 47.2 22.0-127 09/17/2023 18:16 WG2132824
(S) p-Terphenyl-d14 42.0 29.0-141 09/17/2023 18:16 WG2132824
(S) Phenol-d5 17.5 8.00-424 09/17/2023 18:16 WG2132824
(S) 2-Fluorophenol 18.8 10.0-120 09/17/2023 18:16 WG2132824
(S) 2,4,6-Tribromophenol 33.0 10.0-153 09/17/2023 18:16 WG2132824
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 12 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 12 of 78
SAMPLE RESULTS - 03
L1655691
MW-5
Collected date/time: 09/12/23 13:05
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.0941 1.00 1 09/20/2023 09:36 WG2135339
Bromobenzene U 0.118 1.00 1 09/20/2023 09:36 WG2135339
Bromodichloromethane U 0.136 1.00 1 09/20/2023 09:36 WG2135339
Bromochloromethane U 0.128 1.00 1 09/20/2023 09:36 WG2135339
Bromoform U 0.129 1.00 1 09/20/2023 09:36 WG2135339
Bromomethane U 0.605 5.00 1 09/21/2023 00:31 WG2135178
n-Butylbenzene U 0.157 1.00 1 09/20/2023 09:36 WG2135339
sec-Butylbenzene U 0.125 1.00 1 09/20/2023 09:36 WG2135339
tert-Butylbenzene U 0.127 1.00 1 09/20/2023 09:36 WG2135339
Carbon tetrachloride U 0.128 1.00 1 09/20/2023 09:36 WG2135339
Chlorobenzene U 0.116 1.00 1 09/20/2023 09:36 WG2135339
Chlorodibromomethane U 0.140 1.00 1 09/20/2023 09:36 WG2135339
Chloroethane U 0.192 5.00 1 09/20/2023 09:36 WG2135339
Chloroform U 0.111 5.00 1 09/20/2023 09:36 WG2135339
Chloromethane U 0.960 2.50 1 09/20/2023 09:36 WG2135339
2-Chlorotoluene U 0.106 1.00 1 09/20/2023 09:36 WG2135339
4-Chlorotoluene U 0.114 1.00 1 09/20/2023 09:36 WG2135339
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 09/20/2023 09:36 WG2135339
1,2-Dibromoethane U 0.126 1.00 1 09/20/2023 09:36 WG2135339
Dibromomethane U 0.122 1.00 1 09/20/2023 09:36 WG2135339
1,2-Dichlorobenzene U 0.107 1.00 1 09/20/2023 09:36 WG2135339
1,3-Dichlorobenzene U 0.110 1.00 1 09/20/2023 09:36 WG2135339
1,4-Dichlorobenzene U 0.120 1.00 1 09/20/2023 09:36 WG2135339
Dichlorodifluoromethane U 0.374 5.00 1 09/20/2023 09:36 WG2135339
1,1-Dichloroethane U 0.100 1.00 1 09/20/2023 09:36 WG2135339
1,2-Dichloroethane U 0.0819 1.00 1 09/20/2023 09:36 WG2135339
1,1-Dichloroethene U 0.188 1.00 1 09/20/2023 09:36 WG2135339
cis-1,2-Dichloroethene U 0.126 1.00 1 09/20/2023 09:36 WG2135339
trans-1,2-Dichloroethene U 0.149 1.00 1 09/20/2023 09:36 WG2135339
1,2-Dichloropropane U 0.149 1.00 1 09/20/2023 09:36 WG2135339
1,1-Dichloropropene U 0.142 1.00 1 09/20/2023 09:36 WG2135339
1,3-Dichloropropane U 0.110 1.00 1 09/20/2023 09:36 WG2135339
cis-1,3-Dichloropropene U 0.111 1.00 1 09/20/2023 09:36 WG2135339
trans-1,3-Dichloropropene U 0.118 1.00 1 09/20/2023 09:36 WG2135339
2,2-Dichloropropane U 0.161 1.00 1 09/20/2023 09:36 WG2135339
Di-isopropyl ether U 0.105 1.00 1 09/20/2023 09:36 WG2135339
Ethylbenzene U 0.137 1.00 1 09/20/2023 09:36 WG2135339
Hexachloro-1,3-butadiene U 0.337 1.00 1 09/20/2023 09:36 WG2135339
Isopropylbenzene U 0.105 1.00 1 09/20/2023 09:36 WG2135339
Methylene Chloride U 0.430 5.00 1 09/20/2023 09:36 WG2135339
Methyl tert-butyl ether U 0.101 1.00 1 09/20/2023 09:36 WG2135339
Naphthalene U 1.00 5.00 1 09/20/2023 09:36 WG2135339
n-Propylbenzene U 0.0993 1.00 1 09/20/2023 09:36 WG2135339
Styrene U 0.118 1.00 1 09/20/2023 09:36 WG2135339
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 09/20/2023 09:36 WG2135339
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 09/20/2023 09:36 WG2135339
Tetrachloroethene U 0.300 1.00 1 09/20/2023 09:36 WG2135339
Toluene U 0.278 1.00 1 09/20/2023 09:36 WG2135339
1,2,3-Trichlorobenzene U 0.230 1.00 1 09/20/2023 09:36 WG2135339
1,2,4-Trichlorobenzene U 0.481 1.00 1 09/20/2023 09:36 WG2135339
1,1,1-Trichloroethane U 0.149 1.00 1 09/20/2023 09:36 WG2135339
1,1,2-Trichloroethane U 0.158 1.00 1 09/20/2023 09:36 WG2135339
Trichloroethene U 0.190 1.00 1 09/20/2023 09:36 WG2135339
Trichlorofluoromethane U 0.160 5.00 1 09/21/2023 00:31 WG2135178
1,2,3-Trichloropropane U 0.237 2.50 1 09/20/2023 09:36 WG2135339
1,2,4-Trimethylbenzene U 0.322 1.00 1 09/20/2023 09:36 WG2135339
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 13 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 13 of 78
SAMPLE RESULTS - 03
L1655691
MW-5
Collected date/time: 09/12/23 13:05
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene U 0.104 1.00 1 09/20/2023 09:36 WG2135339
Vinyl chloride U 0.234 1.00 1 09/20/2023 09:36 WG2135339
o-Xylene U 0.174 1.00 1 09/20/2023 09:36 WG2135339
m&p-Xylenes U 0.430 2.00 1 09/20/2023 09:36 WG2135339
ethanol U 42.0 100 1 09/20/2023 09:36 WG2135339
tert-Amyl Methyl Ether U 0.195 1.00 1 09/20/2023 09:36 WG2135339
Ethyl tert-butyl ether U 0.101 1.00 1 09/20/2023 09:36 WG2135339
tert-Butyl alcohol U 4.06 5.00 1 09/20/2023 09:36 WG2135339
t-Amyl Alcohol U 4.90 50.0 1 09/20/2023 09:36 WG2135339
tert-Butyl formate U 4.51 20.0 1 09/20/2023 09:36 WG2135339
(S) Toluene-d8 98.9 80.0-120 09/21/2023 00:31 WG2135178
(S) Toluene-d8 93.4 80.0-120 09/20/2023 09:36 WG2135339
(S) 4-Bromofluorobenzene 103 77.0-126 09/21/2023 00:31 WG2135178
(S) 4-Bromofluorobenzene 94.0 77.0-126 09/20/2023 09:36 WG2135339
(S) 1,2-Dichloroethane-d4 82.9 70.0-130 09/21/2023 00:31 WG2135178
(S) 1,2-Dichloroethane-d4 97.8 70.0-130 09/20/2023 09:36 WG2135339
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 38.4 B J 33.3 100 1 09/20/2023 22:32 WG2135760
Unadjusted C19-C36 Aliphatics 64.8 B J 33.3 100 1 09/20/2023 22:32 WG2135760
Unadjusted C11-C22 Aromatics 48.1 B J 33.3 100 1 09/21/2023 04:49 WG2135760
Unadjusted Total Petroleum
Hydrocarbons 151 33.3 100 1 09/21/2023 04:49 WG2135760
(S) o-Terphenyl 86.7 40.0-140 09/21/2023 04:49 WG2135760
(S) 1-Chloro-octadecane 63.4 40.0-140 09/20/2023 22:32 WG2135760
(S) 2-Fluorobiphenyl 94.7 40.0-140 09/21/2023 04:49 WG2135760
(S) 2-Bromonaphthalene 95.6 40.0-140 09/21/2023 04:49 WG2135760
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 09/17/2023 18:38 WG2132824
Acenaphthylene U 0.0921 1.00 1 09/17/2023 18:38 WG2132824
Anthracene U 0.0804 1.00 1 09/17/2023 18:38 WG2132824
Benzo(a)anthracene U 0.199 1.00 1 09/17/2023 18:38 WG2132824
Benzo(b)fluoranthene U 0.130 1.00 1 09/17/2023 18:38 WG2132824
Benzo(k)fluoranthene U 0.120 1.00 1 09/17/2023 18:38 WG2132824
Benzo(g,h,i)perylene U 0.121 1.00 1 09/17/2023 18:38 WG2132824
Benzo(a)pyrene U 0.0381 1.00 1 09/17/2023 18:38 WG2132824
Bis(2-chlorethoxy)methane U 0.116 10.0 1 09/17/2023 18:38 WG2132824
Bis(2-chloroethyl)ether U 0.137 10.0 1 09/17/2023 18:38 WG2132824
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 09/17/2023 18:38 WG2132824
4-Bromophenyl-phenylether U J4 0.0877 10.0 1 09/17/2023 18:38 WG2132824
2-Chloronaphthalene U J4 0.0648 1.00 1 09/17/2023 18:38 WG2132824
4-Chlorophenyl-phenylether U 0.0926 10.0 1 09/17/2023 18:38 WG2132824
Chrysene U 0.130 1.00 1 09/17/2023 18:38 WG2132824
Dibenz(a,h)anthracene U 0.0644 1.00 1 09/17/2023 18:38 WG2132824
3,3-Dichlorobenzidine U 0.212 10.0 1 09/17/2023 18:38 WG2132824
2,4-Dinitrotoluene U 0.0983 10.0 1 09/17/2023 18:38 WG2132824
2,6-Dinitrotoluene U 0.250 10.0 1 09/17/2023 18:38 WG2132824
Fluoranthene U 0.102 1.00 1 09/17/2023 18:38 WG2132824
Fluorene U J4 0.0844 1.00 1 09/17/2023 18:38 WG2132824
Hexachlorobenzene U 0.0755 1.00 1 09/17/2023 18:38 WG2132824
Hexachloro-1,3-butadiene U 0.0968 10.0 1 09/17/2023 18:38 WG2132824
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 14 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 14 of 78
SAMPLE RESULTS - 03
L1655691
MW-5
Collected date/time: 09/12/23 13:05
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexachlorocyclopentadiene U 0.0598 10.0 1 09/17/2023 18:38 WG2132824
Hexachloroethane U 0.127 10.0 1 09/17/2023 18:38 WG2132824
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 09/17/2023 18:38 WG2132824
Isophorone U 0.143 10.0 1 09/17/2023 18:38 WG2132824
Naphthalene U 0.159 1.00 1 09/17/2023 18:38 WG2132824
Nitrobenzene U 0.297 10.0 1 09/17/2023 18:38 WG2132824
n-Nitrosodimethylamine U 0.998 10.0 1 09/17/2023 18:38 WG2132824
n-Nitrosodiphenylamine U 2.37 10.0 1 09/17/2023 18:38 WG2132824
n-Nitrosodi-n-propylamine U 0.261 10.0 1 09/17/2023 18:38 WG2132824
Phenanthrene U J4 0.112 1.00 1 09/17/2023 18:38 WG2132824
Benzylbutyl phthalate U 0.765 3.00 1 09/17/2023 18:38 WG2132824
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 09/17/2023 18:38 WG2132824
Di-n-butyl phthalate U 0.453 3.00 1 09/17/2023 18:38 WG2132824
Diethyl phthalate U 0.287 3.00 1 09/17/2023 18:38 WG2132824
Dimethyl phthalate U 0.260 3.00 1 09/17/2023 18:38 WG2132824
Di-n-octyl phthalate U 0.932 3.00 1 09/17/2023 18:38 WG2132824
Pyrene U 0.107 1.00 1 09/17/2023 18:38 WG2132824
1,2,4-Trichlorobenzene U 0.0698 10.0 1 09/17/2023 18:38 WG2132824
4-Chloro-3-methylphenol U 0.131 10.0 1 09/17/2023 18:38 WG2132824
2-Chlorophenol U 0.133 10.0 1 09/17/2023 18:38 WG2132824
2,4-Dichlorophenol U 0.102 10.0 1 09/17/2023 18:38 WG2132824
2,4-Dimethylphenol U 0.0636 10.0 1 09/17/2023 18:38 WG2132824
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 09/17/2023 18:38 WG2132824
2,4-Dinitrophenol U 5.93 10.0 1 09/17/2023 18:38 WG2132824
2-Nitrophenol U 0.117 10.0 1 09/17/2023 18:38 WG2132824
4-Nitrophenol U 0.143 10.0 1 09/17/2023 18:38 WG2132824
Pentachlorophenol U 0.313 10.0 1 09/17/2023 18:38 WG2132824
Phenol U 4.33 10.0 1 09/17/2023 18:38 WG2132824
2,4,6-Trichlorophenol U 0.100 10.0 1 09/17/2023 18:38 WG2132824
(S) Nitrobenzene-d5 46.0 15.0-314 09/17/2023 18:38 WG2132824
(S) 2-Fluorobiphenyl 46.8 22.0-127 09/17/2023 18:38 WG2132824
(S) p-Terphenyl-d14 53.1 29.0-141 09/17/2023 18:38 WG2132824
(S) Phenol-d5 18.6 8.00-424 09/17/2023 18:38 WG2132824
(S) 2-Fluorophenol 26.0 10.0-120 09/17/2023 18:38 WG2132824
(S) 2,4,6-Tribromophenol 54.0 10.0-153 09/17/2023 18:38 WG2132824
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 15 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 15 of 78
SAMPLE RESULTS - 04
L1655691
MW-6
Collected date/time: 09/12/23 12:25
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.0941 1.00 1 09/20/2023 09:57 WG2135339
Bromobenzene U 0.118 1.00 1 09/20/2023 09:57 WG2135339
Bromodichloromethane U 0.136 1.00 1 09/20/2023 09:57 WG2135339
Bromochloromethane U 0.128 1.00 1 09/20/2023 09:57 WG2135339
Bromoform U 0.129 1.00 1 09/20/2023 09:57 WG2135339
Bromomethane U 0.605 5.00 1 09/21/2023 00:51 WG2135178
n-Butylbenzene U 0.157 1.00 1 09/20/2023 09:57 WG2135339
sec-Butylbenzene U 0.125 1.00 1 09/20/2023 09:57 WG2135339
tert-Butylbenzene U 0.127 1.00 1 09/20/2023 09:57 WG2135339
Carbon tetrachloride U 0.128 1.00 1 09/20/2023 09:57 WG2135339
Chlorobenzene U 0.116 1.00 1 09/20/2023 09:57 WG2135339
Chlorodibromomethane U 0.140 1.00 1 09/20/2023 09:57 WG2135339
Chloroethane U 0.192 5.00 1 09/20/2023 09:57 WG2135339
Chloroform U 0.111 5.00 1 09/20/2023 09:57 WG2135339
Chloromethane U 0.960 2.50 1 09/20/2023 09:57 WG2135339
2-Chlorotoluene U 0.106 1.00 1 09/20/2023 09:57 WG2135339
4-Chlorotoluene U 0.114 1.00 1 09/20/2023 09:57 WG2135339
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 09/20/2023 09:57 WG2135339
1,2-Dibromoethane U 0.126 1.00 1 09/20/2023 09:57 WG2135339
Dibromomethane U 0.122 1.00 1 09/20/2023 09:57 WG2135339
1,2-Dichlorobenzene U 0.107 1.00 1 09/20/2023 09:57 WG2135339
1,3-Dichlorobenzene U 0.110 1.00 1 09/20/2023 09:57 WG2135339
1,4-Dichlorobenzene U 0.120 1.00 1 09/20/2023 09:57 WG2135339
Dichlorodifluoromethane U 0.374 5.00 1 09/20/2023 09:57 WG2135339
1,1-Dichloroethane U 0.100 1.00 1 09/20/2023 09:57 WG2135339
1,2-Dichloroethane U 0.0819 1.00 1 09/20/2023 09:57 WG2135339
1,1-Dichloroethene U 0.188 1.00 1 09/20/2023 09:57 WG2135339
cis-1,2-Dichloroethene U 0.126 1.00 1 09/20/2023 09:57 WG2135339
trans-1,2-Dichloroethene U 0.149 1.00 1 09/20/2023 09:57 WG2135339
1,2-Dichloropropane U 0.149 1.00 1 09/20/2023 09:57 WG2135339
1,1-Dichloropropene U 0.142 1.00 1 09/20/2023 09:57 WG2135339
1,3-Dichloropropane U 0.110 1.00 1 09/20/2023 09:57 WG2135339
cis-1,3-Dichloropropene U 0.111 1.00 1 09/20/2023 09:57 WG2135339
trans-1,3-Dichloropropene U 0.118 1.00 1 09/20/2023 09:57 WG2135339
2,2-Dichloropropane U 0.161 1.00 1 09/20/2023 09:57 WG2135339
Di-isopropyl ether U 0.105 1.00 1 09/20/2023 09:57 WG2135339
Ethylbenzene U 0.137 1.00 1 09/20/2023 09:57 WG2135339
Hexachloro-1,3-butadiene U 0.337 1.00 1 09/20/2023 09:57 WG2135339
Isopropylbenzene U 0.105 1.00 1 09/20/2023 09:57 WG2135339
Methylene Chloride U 0.430 5.00 1 09/20/2023 09:57 WG2135339
Methyl tert-butyl ether U 0.101 1.00 1 09/20/2023 09:57 WG2135339
Naphthalene U 1.00 5.00 1 09/20/2023 09:57 WG2135339
n-Propylbenzene U 0.0993 1.00 1 09/20/2023 09:57 WG2135339
Styrene U 0.118 1.00 1 09/20/2023 09:57 WG2135339
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 09/20/2023 09:57 WG2135339
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 09/20/2023 09:57 WG2135339
Tetrachloroethene U 0.300 1.00 1 09/20/2023 09:57 WG2135339
Toluene U 0.278 1.00 1 09/20/2023 09:57 WG2135339
1,2,3-Trichlorobenzene U 0.230 1.00 1 09/20/2023 09:57 WG2135339
1,2,4-Trichlorobenzene U 0.481 1.00 1 09/20/2023 09:57 WG2135339
1,1,1-Trichloroethane U 0.149 1.00 1 09/20/2023 09:57 WG2135339
1,1,2-Trichloroethane U 0.158 1.00 1 09/20/2023 09:57 WG2135339
Trichloroethene U 0.190 1.00 1 09/20/2023 09:57 WG2135339
Trichlorofluoromethane U 0.160 5.00 1 09/21/2023 00:51 WG2135178
1,2,3-Trichloropropane U 0.237 2.50 1 09/20/2023 09:57 WG2135339
1,2,4-Trimethylbenzene U 0.322 1.00 1 09/20/2023 09:57 WG2135339
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 16 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 16 of 78
SAMPLE RESULTS - 04
L1655691
MW-6
Collected date/time: 09/12/23 12:25
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene U 0.104 1.00 1 09/20/2023 09:57 WG2135339
Vinyl chloride U 0.234 1.00 1 09/20/2023 09:57 WG2135339
o-Xylene U 0.174 1.00 1 09/20/2023 09:57 WG2135339
m&p-Xylenes U 0.430 2.00 1 09/20/2023 09:57 WG2135339
ethanol U 42.0 100 1 09/20/2023 09:57 WG2135339
tert-Amyl Methyl Ether U 0.195 1.00 1 09/20/2023 09:57 WG2135339
Ethyl tert-butyl ether U 0.101 1.00 1 09/20/2023 09:57 WG2135339
tert-Butyl alcohol U 4.06 5.00 1 09/20/2023 09:57 WG2135339
t-Amyl Alcohol U 4.90 50.0 1 09/20/2023 09:57 WG2135339
tert-Butyl formate U 4.51 20.0 1 09/20/2023 09:57 WG2135339
(S) Toluene-d8 101 80.0-120 09/21/2023 00:51 WG2135178
(S) Toluene-d8 96.0 80.0-120 09/20/2023 09:57 WG2135339
(S) 4-Bromofluorobenzene 101 77.0-126 09/21/2023 00:51 WG2135178
(S) 4-Bromofluorobenzene 93.8 77.0-126 09/20/2023 09:57 WG2135339
(S) 1,2-Dichloroethane-d4 82.6 70.0-130 09/21/2023 00:51 WG2135178
(S) 1,2-Dichloroethane-d4 98.8 70.0-130 09/20/2023 09:57 WG2135339
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics U 33.3 100 1 09/27/2023 16:31 WG2139497
Unadjusted C19-C36 Aliphatics 34.6 B J 33.3 100 1 09/27/2023 16:31 WG2139497
Unadjusted C11-C22 Aromatics U 33.3 100 1 09/27/2023 18:08 WG2139497
Unadjusted Total Petroleum
Hydrocarbons 34.6 J 33.3 100 1 09/27/2023 18:08 WG2139497
(S) o-Terphenyl 65.7 40.0-140 09/27/2023 18:08 WG2139497
(S) 1-Chloro-octadecane 20.5 J2 40.0-140 09/27/2023 16:31 WG2139497
(S) 2-Fluorobiphenyl 76.3 40.0-140 09/27/2023 18:08 WG2139497
(S) 2-Bromonaphthalene 77.5 40.0-140 09/27/2023 18:08 WG2139497
Sample Narrative:
L1655691-04 WG2139497: Sample produced emulsion during Extraction process, low surr/spike recoveries due to matrix.
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 09/17/2023 18:59 WG2132824
Acenaphthylene U 0.0921 1.00 1 09/17/2023 18:59 WG2132824
Anthracene U 0.0804 1.00 1 09/17/2023 18:59 WG2132824
Benzo(a)anthracene U 0.199 1.00 1 09/17/2023 18:59 WG2132824
Benzo(b)fluoranthene U 0.130 1.00 1 09/17/2023 18:59 WG2132824
Benzo(k)fluoranthene U 0.120 1.00 1 09/17/2023 18:59 WG2132824
Benzo(g,h,i)perylene U 0.121 1.00 1 09/17/2023 18:59 WG2132824
Benzo(a)pyrene U 0.0381 1.00 1 09/17/2023 18:59 WG2132824
Bis(2-chlorethoxy)methane U 0.116 10.0 1 09/17/2023 18:59 WG2132824
Bis(2-chloroethyl)ether U 0.137 10.0 1 09/17/2023 18:59 WG2132824
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 09/17/2023 18:59 WG2132824
4-Bromophenyl-phenylether U J4 0.0877 10.0 1 09/17/2023 18:59 WG2132824
2-Chloronaphthalene U J4 0.0648 1.00 1 09/17/2023 18:59 WG2132824
4-Chlorophenyl-phenylether U 0.0926 10.0 1 09/17/2023 18:59 WG2132824
Chrysene U 0.130 1.00 1 09/17/2023 18:59 WG2132824
Dibenz(a,h)anthracene U 0.0644 1.00 1 09/17/2023 18:59 WG2132824
3,3-Dichlorobenzidine U 0.212 10.0 1 09/17/2023 18:59 WG2132824
2,4-Dinitrotoluene U 0.0983 10.0 1 09/17/2023 18:59 WG2132824
2,6-Dinitrotoluene U 0.250 10.0 1 09/17/2023 18:59 WG2132824
Fluoranthene U 0.102 1.00 1 09/17/2023 18:59 WG2132824
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 17 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 17 of 78
SAMPLE RESULTS - 04
L1655691
MW-6
Collected date/time: 09/12/23 12:25
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Fluorene U J4 0.0844 1.00 1 09/17/2023 18:59 WG2132824
Hexachlorobenzene U 0.0755 1.00 1 09/17/2023 18:59 WG2132824
Hexachloro-1,3-butadiene U 0.0968 10.0 1 09/17/2023 18:59 WG2132824
Hexachlorocyclopentadiene U 0.0598 10.0 1 09/17/2023 18:59 WG2132824
Hexachloroethane U 0.127 10.0 1 09/17/2023 18:59 WG2132824
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 09/17/2023 18:59 WG2132824
Isophorone U 0.143 10.0 1 09/17/2023 18:59 WG2132824
Naphthalene U 0.159 1.00 1 09/17/2023 18:59 WG2132824
Nitrobenzene U 0.297 10.0 1 09/17/2023 18:59 WG2132824
n-Nitrosodimethylamine U 0.998 10.0 1 09/17/2023 18:59 WG2132824
n-Nitrosodiphenylamine U 2.37 10.0 1 09/17/2023 18:59 WG2132824
n-Nitrosodi-n-propylamine U 0.261 10.0 1 09/17/2023 18:59 WG2132824
Phenanthrene U J4 0.112 1.00 1 09/17/2023 18:59 WG2132824
Benzylbutyl phthalate U 0.765 3.00 1 09/17/2023 18:59 WG2132824
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 09/17/2023 18:59 WG2132824
Di-n-butyl phthalate U 0.453 3.00 1 09/17/2023 18:59 WG2132824
Diethyl phthalate U 0.287 3.00 1 09/17/2023 18:59 WG2132824
Dimethyl phthalate U 0.260 3.00 1 09/17/2023 18:59 WG2132824
Di-n-octyl phthalate U 0.932 3.00 1 09/17/2023 18:59 WG2132824
Pyrene U 0.107 1.00 1 09/17/2023 18:59 WG2132824
1,2,4-Trichlorobenzene U 0.0698 10.0 1 09/17/2023 18:59 WG2132824
4-Chloro-3-methylphenol U 0.131 10.0 1 09/17/2023 18:59 WG2132824
2-Chlorophenol U 0.133 10.0 1 09/17/2023 18:59 WG2132824
2,4-Dichlorophenol U 0.102 10.0 1 09/17/2023 18:59 WG2132824
2,4-Dimethylphenol U 0.0636 10.0 1 09/17/2023 18:59 WG2132824
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 09/17/2023 18:59 WG2132824
2,4-Dinitrophenol U 5.93 10.0 1 09/17/2023 18:59 WG2132824
2-Nitrophenol U 0.117 10.0 1 09/17/2023 18:59 WG2132824
4-Nitrophenol U 0.143 10.0 1 09/17/2023 18:59 WG2132824
Pentachlorophenol U 0.313 10.0 1 09/17/2023 18:59 WG2132824
Phenol U 4.33 10.0 1 09/17/2023 18:59 WG2132824
2,4,6-Trichlorophenol U 0.100 10.0 1 09/17/2023 18:59 WG2132824
(S) Nitrobenzene-d5 48.7 15.0-314 09/17/2023 18:59 WG2132824
(S) 2-Fluorobiphenyl 53.2 22.0-127 09/17/2023 18:59 WG2132824
(S) p-Terphenyl-d14 56.7 29.0-141 09/17/2023 18:59 WG2132824
(S) Phenol-d5 15.9 8.00-424 09/17/2023 18:59 WG2132824
(S) 2-Fluorophenol 22.8 10.0-120 09/17/2023 18:59 WG2132824
(S) 2,4,6-Tribromophenol 49.4 10.0-153 09/17/2023 18:59 WG2132824
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 18 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 18 of 78
SAMPLE RESULTS - 05
L1655691
MW-7
Collected date/time: 09/12/23 13:25
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.0941 1.00 1 09/20/2023 10:18 WG2135339
Bromobenzene U 0.118 1.00 1 09/20/2023 10:18 WG2135339
Bromodichloromethane U 0.136 1.00 1 09/20/2023 10:18 WG2135339
Bromochloromethane U 0.128 1.00 1 09/20/2023 10:18 WG2135339
Bromoform U 0.129 1.00 1 09/20/2023 10:18 WG2135339
Bromomethane U 0.605 5.00 1 09/21/2023 01:12 WG2135178
n-Butylbenzene U 0.157 1.00 1 09/20/2023 10:18 WG2135339
sec-Butylbenzene U 0.125 1.00 1 09/20/2023 10:18 WG2135339
tert-Butylbenzene U 0.127 1.00 1 09/20/2023 10:18 WG2135339
Carbon tetrachloride U 0.128 1.00 1 09/20/2023 10:18 WG2135339
Chlorobenzene U 0.116 1.00 1 09/20/2023 10:18 WG2135339
Chlorodibromomethane U 0.140 1.00 1 09/20/2023 10:18 WG2135339
Chloroethane U 0.192 5.00 1 09/20/2023 10:18 WG2135339
Chloroform U 0.111 5.00 1 09/20/2023 10:18 WG2135339
Chloromethane U 0.960 2.50 1 09/20/2023 10:18 WG2135339
2-Chlorotoluene U 0.106 1.00 1 09/20/2023 10:18 WG2135339
4-Chlorotoluene U 0.114 1.00 1 09/20/2023 10:18 WG2135339
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 09/20/2023 10:18 WG2135339
1,2-Dibromoethane U 0.126 1.00 1 09/20/2023 10:18 WG2135339
Dibromomethane U 0.122 1.00 1 09/20/2023 10:18 WG2135339
1,2-Dichlorobenzene U 0.107 1.00 1 09/20/2023 10:18 WG2135339
1,3-Dichlorobenzene U 0.110 1.00 1 09/20/2023 10:18 WG2135339
1,4-Dichlorobenzene U 0.120 1.00 1 09/20/2023 10:18 WG2135339
Dichlorodifluoromethane U 0.374 5.00 1 09/20/2023 10:18 WG2135339
1,1-Dichloroethane U 0.100 1.00 1 09/20/2023 10:18 WG2135339
1,2-Dichloroethane U 0.0819 1.00 1 09/20/2023 10:18 WG2135339
1,1-Dichloroethene U 0.188 1.00 1 09/20/2023 10:18 WG2135339
cis-1,2-Dichloroethene U 0.126 1.00 1 09/20/2023 10:18 WG2135339
trans-1,2-Dichloroethene U 0.149 1.00 1 09/20/2023 10:18 WG2135339
1,2-Dichloropropane U 0.149 1.00 1 09/20/2023 10:18 WG2135339
1,1-Dichloropropene U 0.142 1.00 1 09/20/2023 10:18 WG2135339
1,3-Dichloropropane U 0.110 1.00 1 09/20/2023 10:18 WG2135339
cis-1,3-Dichloropropene U 0.111 1.00 1 09/20/2023 10:18 WG2135339
trans-1,3-Dichloropropene U 0.118 1.00 1 09/20/2023 10:18 WG2135339
2,2-Dichloropropane U 0.161 1.00 1 09/20/2023 10:18 WG2135339
Di-isopropyl ether U 0.105 1.00 1 09/20/2023 10:18 WG2135339
Ethylbenzene U 0.137 1.00 1 09/20/2023 10:18 WG2135339
Hexachloro-1,3-butadiene U 0.337 1.00 1 09/20/2023 10:18 WG2135339
Isopropylbenzene U 0.105 1.00 1 09/20/2023 10:18 WG2135339
Methylene Chloride U 0.430 5.00 1 09/20/2023 10:18 WG2135339
Methyl tert-butyl ether U 0.101 1.00 1 09/20/2023 10:18 WG2135339
Naphthalene U 1.00 5.00 1 09/20/2023 10:18 WG2135339
n-Propylbenzene U 0.0993 1.00 1 09/20/2023 10:18 WG2135339
Styrene U 0.118 1.00 1 09/20/2023 10:18 WG2135339
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 09/20/2023 10:18 WG2135339
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 09/20/2023 10:18 WG2135339
Tetrachloroethene U 0.300 1.00 1 09/20/2023 10:18 WG2135339
Toluene U 0.278 1.00 1 09/20/2023 10:18 WG2135339
1,2,3-Trichlorobenzene U 0.230 1.00 1 09/20/2023 10:18 WG2135339
1,2,4-Trichlorobenzene U 0.481 1.00 1 09/20/2023 10:18 WG2135339
1,1,1-Trichloroethane U 0.149 1.00 1 09/20/2023 10:18 WG2135339
1,1,2-Trichloroethane U 0.158 1.00 1 09/20/2023 10:18 WG2135339
Trichloroethene U 0.190 1.00 1 09/20/2023 10:18 WG2135339
Trichlorofluoromethane U 0.160 5.00 1 09/21/2023 01:12 WG2135178
1,2,3-Trichloropropane U 0.237 2.50 1 09/20/2023 10:18 WG2135339
1,2,4-Trimethylbenzene U 0.322 1.00 1 09/20/2023 10:18 WG2135339
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 19 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 19 of 78
SAMPLE RESULTS - 05
L1655691
MW-7
Collected date/time: 09/12/23 13:25
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene U 0.104 1.00 1 09/20/2023 10:18 WG2135339
Vinyl chloride U 0.234 1.00 1 09/20/2023 10:18 WG2135339
o-Xylene U 0.174 1.00 1 09/20/2023 10:18 WG2135339
m&p-Xylenes U 0.430 2.00 1 09/20/2023 10:18 WG2135339
ethanol U 42.0 100 1 09/20/2023 10:18 WG2135339
tert-Amyl Methyl Ether U 0.195 1.00 1 09/20/2023 10:18 WG2135339
Ethyl tert-butyl ether U 0.101 1.00 1 09/20/2023 10:18 WG2135339
tert-Butyl alcohol U 4.06 5.00 1 09/20/2023 10:18 WG2135339
t-Amyl Alcohol U 4.90 50.0 1 09/20/2023 10:18 WG2135339
tert-Butyl formate U 4.51 20.0 1 09/20/2023 10:18 WG2135339
(S) Toluene-d8 100 80.0-120 09/21/2023 01:12 WG2135178
(S) Toluene-d8 94.9 80.0-120 09/20/2023 10:18 WG2135339
(S) 4-Bromofluorobenzene 101 77.0-126 09/21/2023 01:12 WG2135178
(S) 4-Bromofluorobenzene 93.6 77.0-126 09/20/2023 10:18 WG2135339
(S) 1,2-Dichloroethane-d4 83.2 70.0-130 09/21/2023 01:12 WG2135178
(S) 1,2-Dichloroethane-d4 97.1 70.0-130 09/20/2023 10:18 WG2135339
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 36.2 B J 33.3 100 1 09/20/2023 23:16 WG2135760
Unadjusted C19-C36 Aliphatics 68.4 B J 33.3 100 1 09/20/2023 23:16 WG2135760
Unadjusted C11-C22 Aromatics 47.8 B J 33.3 100 1 09/21/2023 04:05 WG2135760
Unadjusted Total Petroleum
Hydrocarbons 152 33.3 100 1 09/21/2023 04:05 WG2135760
(S) o-Terphenyl 95.8 40.0-140 09/21/2023 04:05 WG2135760
(S) 1-Chloro-octadecane 44.6 40.0-140 09/20/2023 23:16 WG2135760
(S) 2-Fluorobiphenyl 103 40.0-140 09/21/2023 04:05 WG2135760
(S) 2-Bromonaphthalene 103 40.0-140 09/21/2023 04:05 WG2135760
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 09/17/2023 14:40 WG2132824
Acenaphthylene U 0.0921 1.00 1 09/17/2023 14:40 WG2132824
Anthracene U 0.0804 1.00 1 09/17/2023 14:40 WG2132824
Benzo(a)anthracene U 0.199 1.00 1 09/17/2023 14:40 WG2132824
Benzo(b)fluoranthene U 0.130 1.00 1 09/17/2023 14:40 WG2132824
Benzo(k)fluoranthene U 0.120 1.00 1 09/17/2023 14:40 WG2132824
Benzo(g,h,i)perylene U 0.121 1.00 1 09/17/2023 14:40 WG2132824
Benzo(a)pyrene U 0.0381 1.00 1 09/17/2023 14:40 WG2132824
Bis(2-chlorethoxy)methane U 0.116 10.0 1 09/17/2023 14:40 WG2132824
Bis(2-chloroethyl)ether U 0.137 10.0 1 09/17/2023 14:40 WG2132824
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 09/17/2023 14:40 WG2132824
4-Bromophenyl-phenylether U J4 0.0877 10.0 1 09/17/2023 14:40 WG2132824
2-Chloronaphthalene U J4 0.0648 1.00 1 09/17/2023 14:40 WG2132824
4-Chlorophenyl-phenylether U 0.0926 10.0 1 09/17/2023 14:40 WG2132824
Chrysene U 0.130 1.00 1 09/17/2023 14:40 WG2132824
Dibenz(a,h)anthracene U 0.0644 1.00 1 09/17/2023 14:40 WG2132824
3,3-Dichlorobenzidine U 0.212 10.0 1 09/17/2023 14:40 WG2132824
2,4-Dinitrotoluene U 0.0983 10.0 1 09/17/2023 14:40 WG2132824
2,6-Dinitrotoluene U 0.250 10.0 1 09/17/2023 14:40 WG2132824
Fluoranthene U 0.102 1.00 1 09/17/2023 14:40 WG2132824
Fluorene U J4 0.0844 1.00 1 09/17/2023 14:40 WG2132824
Hexachlorobenzene U 0.0755 1.00 1 09/17/2023 14:40 WG2132824
Hexachloro-1,3-butadiene U 0.0968 10.0 1 09/17/2023 14:40 WG2132824
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 20 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 20 of 78
SAMPLE RESULTS - 05
L1655691
MW-7
Collected date/time: 09/12/23 13:25
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexachlorocyclopentadiene U 0.0598 10.0 1 09/17/2023 14:40 WG2132824
Hexachloroethane U 0.127 10.0 1 09/17/2023 14:40 WG2132824
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 09/17/2023 14:40 WG2132824
Isophorone U 0.143 10.0 1 09/17/2023 14:40 WG2132824
Naphthalene U 0.159 1.00 1 09/17/2023 14:40 WG2132824
Nitrobenzene U 0.297 10.0 1 09/17/2023 14:40 WG2132824
n-Nitrosodimethylamine U 0.998 10.0 1 09/17/2023 14:40 WG2132824
n-Nitrosodiphenylamine U 2.37 10.0 1 09/17/2023 14:40 WG2132824
n-Nitrosodi-n-propylamine U 0.261 10.0 1 09/17/2023 14:40 WG2132824
Phenanthrene U J4 0.112 1.00 1 09/17/2023 14:40 WG2132824
Benzylbutyl phthalate U 0.765 3.00 1 09/17/2023 14:40 WG2132824
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 09/17/2023 14:40 WG2132824
Di-n-butyl phthalate U 0.453 3.00 1 09/17/2023 14:40 WG2132824
Diethyl phthalate U 0.287 3.00 1 09/17/2023 14:40 WG2132824
Dimethyl phthalate U 0.260 3.00 1 09/17/2023 14:40 WG2132824
Di-n-octyl phthalate U 0.932 3.00 1 09/17/2023 14:40 WG2132824
Pyrene U 0.107 1.00 1 09/17/2023 14:40 WG2132824
1,2,4-Trichlorobenzene U 0.0698 10.0 1 09/17/2023 14:40 WG2132824
4-Chloro-3-methylphenol U 0.131 10.0 1 09/17/2023 14:40 WG2132824
2-Chlorophenol U 0.133 10.0 1 09/17/2023 14:40 WG2132824
2,4-Dichlorophenol U 0.102 10.0 1 09/17/2023 14:40 WG2132824
2,4-Dimethylphenol U 0.0636 10.0 1 09/17/2023 14:40 WG2132824
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 09/17/2023 14:40 WG2132824
2,4-Dinitrophenol U 5.93 10.0 1 09/17/2023 14:40 WG2132824
2-Nitrophenol U 0.117 10.0 1 09/17/2023 14:40 WG2132824
4-Nitrophenol U 0.143 10.0 1 09/17/2023 14:40 WG2132824
Pentachlorophenol U 0.313 10.0 1 09/17/2023 14:40 WG2132824
Phenol U 4.33 10.0 1 09/17/2023 14:40 WG2132824
2,4,6-Trichlorophenol U 0.100 10.0 1 09/17/2023 14:40 WG2132824
(S) Nitrobenzene-d5 62.2 15.0-314 09/17/2023 14:40 WG2132824
(S) 2-Fluorobiphenyl 60.4 22.0-127 09/17/2023 14:40 WG2132824
(S) p-Terphenyl-d14 58.9 29.0-141 09/17/2023 14:40 WG2132824
(S) Phenol-d5 18.0 8.00-424 09/17/2023 14:40 WG2132824
(S) 2-Fluorophenol 24.2 10.0-120 09/17/2023 14:40 WG2132824
(S) 2,4,6-Tribromophenol 47.2 10.0-153 09/17/2023 14:40 WG2132824
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 21 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 21 of 78
SAMPLE RESULTS - 06
L1655691
MW-8
Collected date/time: 09/12/23 14:20
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.0941 1.00 1 09/20/2023 10:40 WG2135339
Bromobenzene U 0.118 1.00 1 09/20/2023 10:40 WG2135339
Bromodichloromethane U 0.136 1.00 1 09/20/2023 10:40 WG2135339
Bromochloromethane U 0.128 1.00 1 09/20/2023 10:40 WG2135339
Bromoform U 0.129 1.00 1 09/20/2023 10:40 WG2135339
Bromomethane U 0.605 5.00 1 09/21/2023 01:32 WG2135178
n-Butylbenzene U 0.157 1.00 1 09/20/2023 10:40 WG2135339
sec-Butylbenzene U 0.125 1.00 1 09/20/2023 10:40 WG2135339
tert-Butylbenzene U 0.127 1.00 1 09/20/2023 10:40 WG2135339
Carbon tetrachloride U 0.128 1.00 1 09/20/2023 10:40 WG2135339
Chlorobenzene U 0.116 1.00 1 09/20/2023 10:40 WG2135339
Chlorodibromomethane U 0.140 1.00 1 09/20/2023 10:40 WG2135339
Chloroethane U 0.192 5.00 1 09/20/2023 10:40 WG2135339
Chloroform U 0.111 5.00 1 09/20/2023 10:40 WG2135339
Chloromethane U 0.960 2.50 1 09/20/2023 10:40 WG2135339
2-Chlorotoluene U 0.106 1.00 1 09/20/2023 10:40 WG2135339
4-Chlorotoluene U 0.114 1.00 1 09/20/2023 10:40 WG2135339
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 09/20/2023 10:40 WG2135339
1,2-Dibromoethane U 0.126 1.00 1 09/20/2023 10:40 WG2135339
Dibromomethane U 0.122 1.00 1 09/20/2023 10:40 WG2135339
1,2-Dichlorobenzene U 0.107 1.00 1 09/20/2023 10:40 WG2135339
1,3-Dichlorobenzene U 0.110 1.00 1 09/20/2023 10:40 WG2135339
1,4-Dichlorobenzene U 0.120 1.00 1 09/20/2023 10:40 WG2135339
Dichlorodifluoromethane U 0.374 5.00 1 09/20/2023 10:40 WG2135339
1,1-Dichloroethane U 0.100 1.00 1 09/20/2023 10:40 WG2135339
1,2-Dichloroethane U 0.0819 1.00 1 09/20/2023 10:40 WG2135339
1,1-Dichloroethene U 0.188 1.00 1 09/20/2023 10:40 WG2135339
cis-1,2-Dichloroethene U 0.126 1.00 1 09/20/2023 10:40 WG2135339
trans-1,2-Dichloroethene U 0.149 1.00 1 09/20/2023 10:40 WG2135339
1,2-Dichloropropane U 0.149 1.00 1 09/20/2023 10:40 WG2135339
1,1-Dichloropropene U 0.142 1.00 1 09/20/2023 10:40 WG2135339
1,3-Dichloropropane U 0.110 1.00 1 09/20/2023 10:40 WG2135339
cis-1,3-Dichloropropene U 0.111 1.00 1 09/20/2023 10:40 WG2135339
trans-1,3-Dichloropropene U 0.118 1.00 1 09/20/2023 10:40 WG2135339
2,2-Dichloropropane U 0.161 1.00 1 09/20/2023 10:40 WG2135339
Di-isopropyl ether U 0.105 1.00 1 09/20/2023 10:40 WG2135339
Ethylbenzene U 0.137 1.00 1 09/20/2023 10:40 WG2135339
Hexachloro-1,3-butadiene U 0.337 1.00 1 09/20/2023 10:40 WG2135339
Isopropylbenzene U 0.105 1.00 1 09/20/2023 10:40 WG2135339
Methylene Chloride U 0.430 5.00 1 09/20/2023 10:40 WG2135339
Methyl tert-butyl ether 0.144 J 0.101 1.00 1 09/20/2023 10:40 WG2135339
Naphthalene U 1.00 5.00 1 09/20/2023 10:40 WG2135339
n-Propylbenzene U 0.0993 1.00 1 09/20/2023 10:40 WG2135339
Styrene U 0.118 1.00 1 09/20/2023 10:40 WG2135339
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 09/20/2023 10:40 WG2135339
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 09/20/2023 10:40 WG2135339
Tetrachloroethene U 0.300 1.00 1 09/20/2023 10:40 WG2135339
Toluene U 0.278 1.00 1 09/20/2023 10:40 WG2135339
1,2,3-Trichlorobenzene U 0.230 1.00 1 09/20/2023 10:40 WG2135339
1,2,4-Trichlorobenzene U 0.481 1.00 1 09/20/2023 10:40 WG2135339
1,1,1-Trichloroethane U 0.149 1.00 1 09/20/2023 10:40 WG2135339
1,1,2-Trichloroethane U 0.158 1.00 1 09/20/2023 10:40 WG2135339
Trichloroethene U 0.190 1.00 1 09/20/2023 10:40 WG2135339
Trichlorofluoromethane U 0.160 5.00 1 09/21/2023 01:32 WG2135178
1,2,3-Trichloropropane U 0.237 2.50 1 09/20/2023 10:40 WG2135339
1,2,4-Trimethylbenzene U 0.322 1.00 1 09/20/2023 10:40 WG2135339
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 22 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 22 of 78
SAMPLE RESULTS - 06
L1655691
MW-8
Collected date/time: 09/12/23 14:20
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene U 0.104 1.00 1 09/20/2023 10:40 WG2135339
Vinyl chloride U 0.234 1.00 1 09/20/2023 10:40 WG2135339
o-Xylene U 0.174 1.00 1 09/20/2023 10:40 WG2135339
m&p-Xylenes U 0.430 2.00 1 09/20/2023 10:40 WG2135339
ethanol U 42.0 100 1 09/20/2023 10:40 WG2135339
tert-Amyl Methyl Ether U 0.195 1.00 1 09/20/2023 10:40 WG2135339
Ethyl tert-butyl ether U 0.101 1.00 1 09/20/2023 10:40 WG2135339
tert-Butyl alcohol U 4.06 5.00 1 09/20/2023 10:40 WG2135339
t-Amyl Alcohol U 4.90 50.0 1 09/20/2023 10:40 WG2135339
tert-Butyl formate U 4.51 20.0 1 09/20/2023 10:40 WG2135339
(S) Toluene-d8 100 80.0-120 09/21/2023 01:32 WG2135178
(S) Toluene-d8 98.1 80.0-120 09/20/2023 10:40 WG2135339
(S) 4-Bromofluorobenzene 103 77.0-126 09/21/2023 01:32 WG2135178
(S) 4-Bromofluorobenzene 91.8 77.0-126 09/20/2023 10:40 WG2135339
(S) 1,2-Dichloroethane-d4 83.7 70.0-130 09/21/2023 01:32 WG2135178
(S) 1,2-Dichloroethane-d4 99.4 70.0-130 09/20/2023 10:40 WG2135339
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 34.6 B J 33.3 100 1 09/20/2023 23:39 WG2135760
Unadjusted C19-C36 Aliphatics 64.0 B J 33.3 100 1 09/20/2023 23:39 WG2135760
Unadjusted C11-C22 Aromatics 43.6 B J 33.3 100 1 09/21/2023 03:43 WG2135760
Unadjusted Total Petroleum
Hydrocarbons 142 33.3 100 1 09/21/2023 03:43 WG2135760
(S) o-Terphenyl 89.3 40.0-140 09/21/2023 03:43 WG2135760
(S) 1-Chloro-octadecane 46.3 40.0-140 09/20/2023 23:39 WG2135760
(S) 2-Fluorobiphenyl 93.2 40.0-140 09/21/2023 03:43 WG2135760
(S) 2-Bromonaphthalene 93.7 40.0-140 09/21/2023 03:43 WG2135760
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 09/17/2023 15:01 WG2132824
Acenaphthylene U 0.0921 1.00 1 09/17/2023 15:01 WG2132824
Anthracene U 0.0804 1.00 1 09/17/2023 15:01 WG2132824
Benzo(a)anthracene U 0.199 1.00 1 09/17/2023 15:01 WG2132824
Benzo(b)fluoranthene U 0.130 1.00 1 09/17/2023 15:01 WG2132824
Benzo(k)fluoranthene U 0.120 1.00 1 09/17/2023 15:01 WG2132824
Benzo(g,h,i)perylene U 0.121 1.00 1 09/17/2023 15:01 WG2132824
Benzo(a)pyrene U 0.0381 1.00 1 09/17/2023 15:01 WG2132824
Bis(2-chlorethoxy)methane U 0.116 10.0 1 09/17/2023 15:01 WG2132824
Bis(2-chloroethyl)ether U 0.137 10.0 1 09/17/2023 15:01 WG2132824
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 09/17/2023 15:01 WG2132824
4-Bromophenyl-phenylether U J4 0.0877 10.0 1 09/17/2023 15:01 WG2132824
2-Chloronaphthalene U J4 0.0648 1.00 1 09/17/2023 15:01 WG2132824
4-Chlorophenyl-phenylether U 0.0926 10.0 1 09/17/2023 15:01 WG2132824
Chrysene U 0.130 1.00 1 09/17/2023 15:01 WG2132824
Dibenz(a,h)anthracene U 0.0644 1.00 1 09/17/2023 15:01 WG2132824
3,3-Dichlorobenzidine U 0.212 10.0 1 09/17/2023 15:01 WG2132824
2,4-Dinitrotoluene U 0.0983 10.0 1 09/17/2023 15:01 WG2132824
2,6-Dinitrotoluene U 0.250 10.0 1 09/17/2023 15:01 WG2132824
Fluoranthene U 0.102 1.00 1 09/17/2023 15:01 WG2132824
Fluorene U J4 0.0844 1.00 1 09/17/2023 15:01 WG2132824
Hexachlorobenzene U 0.0755 1.00 1 09/17/2023 15:01 WG2132824
Hexachloro-1,3-butadiene U 0.0968 10.0 1 09/17/2023 15:01 WG2132824
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 23 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 23 of 78
SAMPLE RESULTS - 06
L1655691
MW-8
Collected date/time: 09/12/23 14:20
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexachlorocyclopentadiene U 0.0598 10.0 1 09/17/2023 15:01 WG2132824
Hexachloroethane U 0.127 10.0 1 09/17/2023 15:01 WG2132824
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 09/17/2023 15:01 WG2132824
Isophorone U 0.143 10.0 1 09/17/2023 15:01 WG2132824
Naphthalene U 0.159 1.00 1 09/17/2023 15:01 WG2132824
Nitrobenzene U 0.297 10.0 1 09/17/2023 15:01 WG2132824
n-Nitrosodimethylamine U 0.998 10.0 1 09/17/2023 15:01 WG2132824
n-Nitrosodiphenylamine U 2.37 10.0 1 09/17/2023 15:01 WG2132824
n-Nitrosodi-n-propylamine U 0.261 10.0 1 09/17/2023 15:01 WG2132824
Phenanthrene U J4 0.112 1.00 1 09/17/2023 15:01 WG2132824
Benzylbutyl phthalate U 0.765 3.00 1 09/17/2023 15:01 WG2132824
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 09/17/2023 15:01 WG2132824
Di-n-butyl phthalate U 0.453 3.00 1 09/17/2023 15:01 WG2132824
Diethyl phthalate U 0.287 3.00 1 09/17/2023 15:01 WG2132824
Dimethyl phthalate U 0.260 3.00 1 09/17/2023 15:01 WG2132824
Di-n-octyl phthalate U 0.932 3.00 1 09/17/2023 15:01 WG2132824
Pyrene U 0.107 1.00 1 09/17/2023 15:01 WG2132824
1,2,4-Trichlorobenzene U 0.0698 10.0 1 09/17/2023 15:01 WG2132824
4-Chloro-3-methylphenol U 0.131 10.0 1 09/17/2023 15:01 WG2132824
2-Chlorophenol U 0.133 10.0 1 09/17/2023 15:01 WG2132824
2,4-Dichlorophenol U 0.102 10.0 1 09/17/2023 15:01 WG2132824
2,4-Dimethylphenol U 0.0636 10.0 1 09/17/2023 15:01 WG2132824
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 09/17/2023 15:01 WG2132824
2,4-Dinitrophenol U 5.93 10.0 1 09/17/2023 15:01 WG2132824
2-Nitrophenol U 0.117 10.0 1 09/17/2023 15:01 WG2132824
4-Nitrophenol U 0.143 10.0 1 09/17/2023 15:01 WG2132824
Pentachlorophenol U 0.313 10.0 1 09/17/2023 15:01 WG2132824
Phenol U 4.33 10.0 1 09/17/2023 15:01 WG2132824
2,4,6-Trichlorophenol U 0.100 10.0 1 09/17/2023 15:01 WG2132824
(S) Nitrobenzene-d5 53.6 15.0-314 09/17/2023 15:01 WG2132824
(S) 2-Fluorobiphenyl 51.3 22.0-127 09/17/2023 15:01 WG2132824
(S) p-Terphenyl-d14 52.8 29.0-141 09/17/2023 15:01 WG2132824
(S) Phenol-d5 14.6 8.00-424 09/17/2023 15:01 WG2132824
(S) 2-Fluorophenol 19.2 10.0-120 09/17/2023 15:01 WG2132824
(S) 2,4,6-Tribromophenol 36.4 10.0-153 09/17/2023 15:01 WG2132824
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 24 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 24 of 78
SAMPLE RESULTS - 07
L1655691
MW-9
Collected date/time: 09/12/23 11:25
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.0941 1.00 1 09/20/2023 11:02 WG2135339
Bromobenzene U 0.118 1.00 1 09/20/2023 11:02 WG2135339
Bromodichloromethane U 0.136 1.00 1 09/20/2023 11:02 WG2135339
Bromochloromethane U 0.128 1.00 1 09/20/2023 11:02 WG2135339
Bromoform U 0.129 1.00 1 09/20/2023 11:02 WG2135339
Bromomethane U 0.605 5.00 1 09/21/2023 01:53 WG2135178
n-Butylbenzene U 0.157 1.00 1 09/20/2023 11:02 WG2135339
sec-Butylbenzene U 0.125 1.00 1 09/20/2023 11:02 WG2135339
tert-Butylbenzene U 0.127 1.00 1 09/20/2023 11:02 WG2135339
Carbon tetrachloride U 0.128 1.00 1 09/20/2023 11:02 WG2135339
Chlorobenzene U 0.116 1.00 1 09/20/2023 11:02 WG2135339
Chlorodibromomethane U 0.140 1.00 1 09/20/2023 11:02 WG2135339
Chloroethane U 0.192 5.00 1 09/20/2023 11:02 WG2135339
Chloroform U 0.111 5.00 1 09/20/2023 11:02 WG2135339
Chloromethane U 0.960 2.50 1 09/20/2023 11:02 WG2135339
2-Chlorotoluene U 0.106 1.00 1 09/20/2023 11:02 WG2135339
4-Chlorotoluene U 0.114 1.00 1 09/20/2023 11:02 WG2135339
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 09/20/2023 11:02 WG2135339
1,2-Dibromoethane U 0.126 1.00 1 09/20/2023 11:02 WG2135339
Dibromomethane U 0.122 1.00 1 09/20/2023 11:02 WG2135339
1,2-Dichlorobenzene U 0.107 1.00 1 09/20/2023 11:02 WG2135339
1,3-Dichlorobenzene U 0.110 1.00 1 09/20/2023 11:02 WG2135339
1,4-Dichlorobenzene U 0.120 1.00 1 09/20/2023 11:02 WG2135339
Dichlorodifluoromethane U 0.374 5.00 1 09/20/2023 11:02 WG2135339
1,1-Dichloroethane U 0.100 1.00 1 09/20/2023 11:02 WG2135339
1,2-Dichloroethane U 0.0819 1.00 1 09/20/2023 11:02 WG2135339
1,1-Dichloroethene U 0.188 1.00 1 09/20/2023 11:02 WG2135339
cis-1,2-Dichloroethene U 0.126 1.00 1 09/20/2023 11:02 WG2135339
trans-1,2-Dichloroethene U 0.149 1.00 1 09/20/2023 11:02 WG2135339
1,2-Dichloropropane U 0.149 1.00 1 09/20/2023 11:02 WG2135339
1,1-Dichloropropene U 0.142 1.00 1 09/20/2023 11:02 WG2135339
1,3-Dichloropropane U 0.110 1.00 1 09/20/2023 11:02 WG2135339
cis-1,3-Dichloropropene U 0.111 1.00 1 09/20/2023 11:02 WG2135339
trans-1,3-Dichloropropene U 0.118 1.00 1 09/20/2023 11:02 WG2135339
2,2-Dichloropropane U 0.161 1.00 1 09/20/2023 11:02 WG2135339
Di-isopropyl ether U 0.105 1.00 1 09/20/2023 11:02 WG2135339
Ethylbenzene U 0.137 1.00 1 09/20/2023 11:02 WG2135339
Hexachloro-1,3-butadiene U 0.337 1.00 1 09/20/2023 11:02 WG2135339
Isopropylbenzene U 0.105 1.00 1 09/20/2023 11:02 WG2135339
Methylene Chloride U 0.430 5.00 1 09/20/2023 11:02 WG2135339
Methyl tert-butyl ether U 0.101 1.00 1 09/20/2023 11:02 WG2135339
Naphthalene U 1.00 5.00 1 09/20/2023 11:02 WG2135339
n-Propylbenzene U 0.0993 1.00 1 09/20/2023 11:02 WG2135339
Styrene U 0.118 1.00 1 09/20/2023 11:02 WG2135339
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 09/20/2023 11:02 WG2135339
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 09/20/2023 11:02 WG2135339
Tetrachloroethene U 0.300 1.00 1 09/20/2023 11:02 WG2135339
Toluene U 0.278 1.00 1 09/20/2023 11:02 WG2135339
1,2,3-Trichlorobenzene U 0.230 1.00 1 09/20/2023 11:02 WG2135339
1,2,4-Trichlorobenzene U 0.481 1.00 1 09/20/2023 11:02 WG2135339
1,1,1-Trichloroethane U 0.149 1.00 1 09/20/2023 11:02 WG2135339
1,1,2-Trichloroethane U 0.158 1.00 1 09/20/2023 11:02 WG2135339
Trichloroethene U 0.190 1.00 1 09/20/2023 11:02 WG2135339
Trichlorofluoromethane U 0.160 5.00 1 09/21/2023 01:53 WG2135178
1,2,3-Trichloropropane U 0.237 2.50 1 09/20/2023 11:02 WG2135339
1,2,4-Trimethylbenzene U 0.322 1.00 1 09/20/2023 11:02 WG2135339
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 25 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 25 of 78
SAMPLE RESULTS - 07
L1655691
MW-9
Collected date/time: 09/12/23 11:25
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene U 0.104 1.00 1 09/20/2023 11:02 WG2135339
Vinyl chloride U 0.234 1.00 1 09/20/2023 11:02 WG2135339
o-Xylene U 0.174 1.00 1 09/20/2023 11:02 WG2135339
m&p-Xylenes U 0.430 2.00 1 09/20/2023 11:02 WG2135339
ethanol U 42.0 100 1 09/20/2023 11:02 WG2135339
tert-Amyl Methyl Ether U 0.195 1.00 1 09/20/2023 11:02 WG2135339
Ethyl tert-butyl ether U 0.101 1.00 1 09/20/2023 11:02 WG2135339
tert-Butyl alcohol U 4.06 5.00 1 09/20/2023 11:02 WG2135339
t-Amyl Alcohol U 4.90 50.0 1 09/20/2023 11:02 WG2135339
tert-Butyl formate U 4.51 20.0 1 09/20/2023 11:02 WG2135339
(S) Toluene-d8 100 80.0-120 09/21/2023 01:53 WG2135178
(S) Toluene-d8 96.4 80.0-120 09/20/2023 11:02 WG2135339
(S) 4-Bromofluorobenzene 103 77.0-126 09/21/2023 01:53 WG2135178
(S) 4-Bromofluorobenzene 93.9 77.0-126 09/20/2023 11:02 WG2135339
(S) 1,2-Dichloroethane-d4 84.8 70.0-130 09/21/2023 01:53 WG2135178
(S) 1,2-Dichloroethane-d4 101 70.0-130 09/20/2023 11:02 WG2135339
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 37.0 B J 33.3 100 1 09/21/2023 00:01 WG2135760
Unadjusted C19-C36 Aliphatics 73.2 B J 33.3 100 1 09/21/2023 00:01 WG2135760
Unadjusted C11-C22 Aromatics 44.7 B J 33.3 100 1 09/21/2023 03:20 WG2135760
Unadjusted Total Petroleum
Hydrocarbons 155 33.3 100 1 09/21/2023 03:20 WG2135760
(S) o-Terphenyl 80.8 40.0-140 09/21/2023 03:20 WG2135760
(S) 1-Chloro-octadecane 20.8 J2 40.0-140 09/21/2023 00:01 WG2135760
(S) 2-Fluorobiphenyl 91.7 40.0-140 09/21/2023 03:20 WG2135760
(S) 2-Bromonaphthalene 91.8 40.0-140 09/21/2023 03:20 WG2135760
Sample Narrative:
L1655691-07 WG2135760: Sample produced emulsion during Extraction process, low surr/spike recoveries due to matrix.
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 09/17/2023 15:23 WG2132824
Acenaphthylene U 0.0921 1.00 1 09/17/2023 15:23 WG2132824
Anthracene U 0.0804 1.00 1 09/17/2023 15:23 WG2132824
Benzo(a)anthracene U 0.199 1.00 1 09/17/2023 15:23 WG2132824
Benzo(b)fluoranthene U 0.130 1.00 1 09/17/2023 15:23 WG2132824
Benzo(k)fluoranthene U 0.120 1.00 1 09/17/2023 15:23 WG2132824
Benzo(g,h,i)perylene U 0.121 1.00 1 09/17/2023 15:23 WG2132824
Benzo(a)pyrene U 0.0381 1.00 1 09/17/2023 15:23 WG2132824
Bis(2-chlorethoxy)methane U 0.116 10.0 1 09/17/2023 15:23 WG2132824
Bis(2-chloroethyl)ether U 0.137 10.0 1 09/17/2023 15:23 WG2132824
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 09/17/2023 15:23 WG2132824
4-Bromophenyl-phenylether U J4 0.0877 10.0 1 09/17/2023 15:23 WG2132824
2-Chloronaphthalene U J4 0.0648 1.00 1 09/17/2023 15:23 WG2132824
4-Chlorophenyl-phenylether U 0.0926 10.0 1 09/17/2023 15:23 WG2132824
Chrysene U 0.130 1.00 1 09/17/2023 15:23 WG2132824
Dibenz(a,h)anthracene U 0.0644 1.00 1 09/17/2023 15:23 WG2132824
3,3-Dichlorobenzidine U 0.212 10.0 1 09/17/2023 15:23 WG2132824
2,4-Dinitrotoluene U 0.0983 10.0 1 09/17/2023 15:23 WG2132824
2,6-Dinitrotoluene U 0.250 10.0 1 09/17/2023 15:23 WG2132824
Fluoranthene U 0.102 1.00 1 09/17/2023 15:23 WG2132824
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 26 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 26 of 78
SAMPLE RESULTS - 07
L1655691
MW-9
Collected date/time: 09/12/23 11:25
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Fluorene U J4 0.0844 1.00 1 09/17/2023 15:23 WG2132824
Hexachlorobenzene U 0.0755 1.00 1 09/17/2023 15:23 WG2132824
Hexachloro-1,3-butadiene U 0.0968 10.0 1 09/17/2023 15:23 WG2132824
Hexachlorocyclopentadiene U 0.0598 10.0 1 09/17/2023 15:23 WG2132824
Hexachloroethane U 0.127 10.0 1 09/17/2023 15:23 WG2132824
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 09/17/2023 15:23 WG2132824
Isophorone U 0.143 10.0 1 09/17/2023 15:23 WG2132824
Naphthalene U 0.159 1.00 1 09/17/2023 15:23 WG2132824
Nitrobenzene U 0.297 10.0 1 09/17/2023 15:23 WG2132824
n-Nitrosodimethylamine U 0.998 10.0 1 09/17/2023 15:23 WG2132824
n-Nitrosodiphenylamine U 2.37 10.0 1 09/17/2023 15:23 WG2132824
n-Nitrosodi-n-propylamine U 0.261 10.0 1 09/17/2023 15:23 WG2132824
Phenanthrene U J4 0.112 1.00 1 09/17/2023 15:23 WG2132824
Benzylbutyl phthalate U 0.765 3.00 1 09/17/2023 15:23 WG2132824
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 09/17/2023 15:23 WG2132824
Di-n-butyl phthalate U 0.453 3.00 1 09/17/2023 15:23 WG2132824
Diethyl phthalate U 0.287 3.00 1 09/17/2023 15:23 WG2132824
Dimethyl phthalate U 0.260 3.00 1 09/17/2023 15:23 WG2132824
Di-n-octyl phthalate U 0.932 3.00 1 09/17/2023 15:23 WG2132824
Pyrene U 0.107 1.00 1 09/17/2023 15:23 WG2132824
1,2,4-Trichlorobenzene U 0.0698 10.0 1 09/17/2023 15:23 WG2132824
4-Chloro-3-methylphenol U 0.131 10.0 1 09/17/2023 15:23 WG2132824
2-Chlorophenol U 0.133 10.0 1 09/17/2023 15:23 WG2132824
2,4-Dichlorophenol U 0.102 10.0 1 09/17/2023 15:23 WG2132824
2,4-Dimethylphenol U 0.0636 10.0 1 09/17/2023 15:23 WG2132824
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 09/17/2023 15:23 WG2132824
2,4-Dinitrophenol U 5.93 10.0 1 09/17/2023 15:23 WG2132824
2-Nitrophenol U 0.117 10.0 1 09/17/2023 15:23 WG2132824
4-Nitrophenol U 0.143 10.0 1 09/17/2023 15:23 WG2132824
Pentachlorophenol U 0.313 10.0 1 09/17/2023 15:23 WG2132824
Phenol U 4.33 10.0 1 09/17/2023 15:23 WG2132824
2,4,6-Trichlorophenol U 0.100 10.0 1 09/17/2023 15:23 WG2132824
(S) Nitrobenzene-d5 64.9 15.0-314 09/17/2023 15:23 WG2132824
(S) 2-Fluorobiphenyl 65.4 22.0-127 09/17/2023 15:23 WG2132824
(S) p-Terphenyl-d14 60.6 29.0-141 09/17/2023 15:23 WG2132824
(S) Phenol-d5 16.5 8.00-424 09/17/2023 15:23 WG2132824
(S) 2-Fluorophenol 24.7 10.0-120 09/17/2023 15:23 WG2132824
(S) 2,4,6-Tribromophenol 48.0 10.0-153 09/17/2023 15:23 WG2132824
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 27 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 27 of 78
SAMPLE RESULTS - 08
L1655691
MW-12
Collected date/time: 09/12/23 11:40
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.0941 1.00 1 09/21/2023 17:58 WG2135999
Bromobenzene U 0.118 1.00 1 09/21/2023 17:58 WG2135999
Bromodichloromethane U 0.136 1.00 1 09/21/2023 17:58 WG2135999
Bromochloromethane U 0.128 1.00 1 09/21/2023 17:58 WG2135999
Bromoform U 0.129 1.00 1 09/21/2023 17:58 WG2135999
Bromomethane U 0.605 5.00 1 09/22/2023 12:49 WG2137490
n-Butylbenzene U 0.157 1.00 1 09/21/2023 17:58 WG2135999
sec-Butylbenzene U 0.125 1.00 1 09/21/2023 17:58 WG2135999
tert-Butylbenzene U 0.127 1.00 1 09/21/2023 17:58 WG2135999
Carbon tetrachloride U 0.128 1.00 1 09/21/2023 17:58 WG2135999
Chlorobenzene U 0.116 1.00 1 09/21/2023 17:58 WG2135999
Chlorodibromomethane U 0.140 1.00 1 09/21/2023 17:58 WG2135999
Chloroethane U 0.192 5.00 1 09/21/2023 17:58 WG2135999
Chloroform U 0.111 5.00 1 09/21/2023 17:58 WG2135999
Chloromethane U 0.960 2.50 1 09/21/2023 17:58 WG2135999
2-Chlorotoluene U 0.106 1.00 1 09/21/2023 17:58 WG2135999
4-Chlorotoluene U 0.114 1.00 1 09/21/2023 17:58 WG2135999
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 09/21/2023 17:58 WG2135999
1,2-Dibromoethane U 0.126 1.00 1 09/21/2023 17:58 WG2135999
Dibromomethane U 0.122 1.00 1 09/21/2023 17:58 WG2135999
1,2-Dichlorobenzene U 0.107 1.00 1 09/21/2023 17:58 WG2135999
1,3-Dichlorobenzene U 0.110 1.00 1 09/21/2023 17:58 WG2135999
1,4-Dichlorobenzene U 0.120 1.00 1 09/21/2023 17:58 WG2135999
Dichlorodifluoromethane U 0.374 5.00 1 09/21/2023 17:58 WG2135999
1,1-Dichloroethane U 0.100 1.00 1 09/21/2023 17:58 WG2135999
1,2-Dichloroethane U 0.0819 1.00 1 09/21/2023 17:58 WG2135999
1,1-Dichloroethene U 0.188 1.00 1 09/21/2023 17:58 WG2135999
cis-1,2-Dichloroethene U 0.126 1.00 1 09/21/2023 17:58 WG2135999
trans-1,2-Dichloroethene U 0.149 1.00 1 09/21/2023 17:58 WG2135999
1,2-Dichloropropane U 0.149 1.00 1 09/21/2023 17:58 WG2135999
1,1-Dichloropropene U 0.142 1.00 1 09/21/2023 17:58 WG2135999
1,3-Dichloropropane U 0.110 1.00 1 09/21/2023 17:58 WG2135999
cis-1,3-Dichloropropene U 0.111 1.00 1 09/21/2023 17:58 WG2135999
trans-1,3-Dichloropropene U 0.118 1.00 1 09/21/2023 17:58 WG2135999
2,2-Dichloropropane U 0.161 1.00 1 09/21/2023 17:58 WG2135999
Di-isopropyl ether U 0.105 1.00 1 09/21/2023 17:58 WG2135999
Ethylbenzene U 0.137 1.00 1 09/21/2023 17:58 WG2135999
Hexachloro-1,3-butadiene U 0.337 1.00 1 09/21/2023 17:58 WG2135999
Isopropylbenzene U 0.105 1.00 1 09/21/2023 17:58 WG2135999
Methylene Chloride U 0.430 5.00 1 09/21/2023 17:58 WG2135999
Methyl tert-butyl ether U 0.101 1.00 1 09/21/2023 17:58 WG2135999
Naphthalene U 1.00 5.00 1 09/21/2023 17:58 WG2135999
n-Propylbenzene U 0.0993 1.00 1 09/21/2023 17:58 WG2135999
Styrene U 0.118 1.00 1 09/21/2023 17:58 WG2135999
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 09/21/2023 17:58 WG2135999
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 09/21/2023 17:58 WG2135999
Tetrachloroethene U 0.300 1.00 1 09/21/2023 17:58 WG2135999
Toluene U 0.278 1.00 1 09/21/2023 17:58 WG2135999
1,2,3-Trichlorobenzene U 0.230 1.00 1 09/21/2023 17:58 WG2135999
1,2,4-Trichlorobenzene U 0.481 1.00 1 09/21/2023 17:58 WG2135999
1,1,1-Trichloroethane U 0.149 1.00 1 09/21/2023 17:58 WG2135999
1,1,2-Trichloroethane U 0.158 1.00 1 09/21/2023 17:58 WG2135999
Trichloroethene U 0.190 1.00 1 09/21/2023 17:58 WG2135999
Trichlorofluoromethane U 0.160 5.00 1 09/22/2023 12:49 WG2137490
1,2,3-Trichloropropane U 0.237 2.50 1 09/21/2023 17:58 WG2135999
1,2,4-Trimethylbenzene U 0.322 1.00 1 09/21/2023 17:58 WG2135999
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 28 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 28 of 78
SAMPLE RESULTS - 08
L1655691
MW-12
Collected date/time: 09/12/23 11:40
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene U 0.104 1.00 1 09/21/2023 17:58 WG2135999
Vinyl chloride U 0.234 1.00 1 09/21/2023 17:58 WG2135999
o-Xylene U 0.174 1.00 1 09/21/2023 17:58 WG2135999
m&p-Xylenes U 0.430 2.00 1 09/21/2023 17:58 WG2135999
ethanol U 42.0 100 1 09/21/2023 17:58 WG2135999
tert-Amyl Methyl Ether U 0.195 1.00 1 09/21/2023 17:58 WG2135999
Ethyl tert-butyl ether U 0.101 1.00 1 09/21/2023 17:58 WG2135999
tert-Butyl alcohol U 4.06 5.00 1 09/21/2023 17:58 WG2135999
t-Amyl Alcohol U 4.90 50.0 1 09/21/2023 17:58 WG2135999
tert-Butyl formate U J4 4.51 20.0 1 09/21/2023 17:58 WG2135999
(S) Toluene-d8 96.1 80.0-120 09/21/2023 17:58 WG2135999
(S) Toluene-d8 107 80.0-120 09/22/2023 12:49 WG2137490
(S) 4-Bromofluorobenzene 92.4 77.0-126 09/21/2023 17:58 WG2135999
(S) 4-Bromofluorobenzene 100 77.0-126 09/22/2023 12:49 WG2137490
(S) 1,2-Dichloroethane-d4 99.3 70.0-130 09/21/2023 17:58 WG2135999
(S) 1,2-Dichloroethane-d4 102 70.0-130 09/22/2023 12:49 WG2137490
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 38.1 B J 33.3 100 1 09/21/2023 00:23 WG2135760
Unadjusted C19-C36 Aliphatics 64.3 B J 33.3 100 1 09/21/2023 00:23 WG2135760
Unadjusted C11-C22 Aromatics 49.2 B J 33.3 100 1 09/21/2023 02:58 WG2135760
Unadjusted Total Petroleum
Hydrocarbons 152 33.3 100 1 09/21/2023 02:58 WG2135760
(S) o-Terphenyl 87.6 40.0-140 09/21/2023 02:58 WG2135760
(S) 1-Chloro-octadecane 64.2 40.0-140 09/21/2023 00:23 WG2135760
(S) 2-Fluorobiphenyl 95.8 40.0-140 09/21/2023 02:58 WG2135760
(S) 2-Bromonaphthalene 95.4 40.0-140 09/21/2023 02:58 WG2135760
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 09/17/2023 15:45 WG2132824
Acenaphthylene U 0.0921 1.00 1 09/17/2023 15:45 WG2132824
Anthracene U 0.0804 1.00 1 09/17/2023 15:45 WG2132824
Benzo(a)anthracene U 0.199 1.00 1 09/17/2023 15:45 WG2132824
Benzo(b)fluoranthene U 0.130 1.00 1 09/17/2023 15:45 WG2132824
Benzo(k)fluoranthene U 0.120 1.00 1 09/17/2023 15:45 WG2132824
Benzo(g,h,i)perylene U 0.121 1.00 1 09/17/2023 15:45 WG2132824
Benzo(a)pyrene U 0.0381 1.00 1 09/17/2023 15:45 WG2132824
Bis(2-chlorethoxy)methane U 0.116 10.0 1 09/17/2023 15:45 WG2132824
Bis(2-chloroethyl)ether U 0.137 10.0 1 09/17/2023 15:45 WG2132824
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 09/17/2023 15:45 WG2132824
4-Bromophenyl-phenylether U J4 0.0877 10.0 1 09/17/2023 15:45 WG2132824
2-Chloronaphthalene U J4 0.0648 1.00 1 09/17/2023 15:45 WG2132824
4-Chlorophenyl-phenylether U 0.0926 10.0 1 09/17/2023 15:45 WG2132824
Chrysene U 0.130 1.00 1 09/17/2023 15:45 WG2132824
Dibenz(a,h)anthracene U 0.0644 1.00 1 09/17/2023 15:45 WG2132824
3,3-Dichlorobenzidine U 0.212 10.0 1 09/17/2023 15:45 WG2132824
2,4-Dinitrotoluene U 0.0983 10.0 1 09/17/2023 15:45 WG2132824
2,6-Dinitrotoluene U 0.250 10.0 1 09/17/2023 15:45 WG2132824
Fluoranthene U 0.102 1.00 1 09/17/2023 15:45 WG2132824
Fluorene U J4 0.0844 1.00 1 09/17/2023 15:45 WG2132824
Hexachlorobenzene U 0.0755 1.00 1 09/17/2023 15:45 WG2132824
Hexachloro-1,3-butadiene U 0.0968 10.0 1 09/17/2023 15:45 WG2132824
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 29 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 29 of 78
SAMPLE RESULTS - 08
L1655691
MW-12
Collected date/time: 09/12/23 11:40
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexachlorocyclopentadiene U 0.0598 10.0 1 09/17/2023 15:45 WG2132824
Hexachloroethane U 0.127 10.0 1 09/17/2023 15:45 WG2132824
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 09/17/2023 15:45 WG2132824
Isophorone U 0.143 10.0 1 09/17/2023 15:45 WG2132824
Naphthalene U 0.159 1.00 1 09/17/2023 15:45 WG2132824
Nitrobenzene U 0.297 10.0 1 09/17/2023 15:45 WG2132824
n-Nitrosodimethylamine U 0.998 10.0 1 09/17/2023 15:45 WG2132824
n-Nitrosodiphenylamine U 2.37 10.0 1 09/17/2023 15:45 WG2132824
n-Nitrosodi-n-propylamine U 0.261 10.0 1 09/17/2023 15:45 WG2132824
Phenanthrene U J4 0.112 1.00 1 09/17/2023 15:45 WG2132824
Benzylbutyl phthalate U 0.765 3.00 1 09/17/2023 15:45 WG2132824
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 09/17/2023 15:45 WG2132824
Di-n-butyl phthalate U 0.453 3.00 1 09/17/2023 15:45 WG2132824
Diethyl phthalate U 0.287 3.00 1 09/17/2023 15:45 WG2132824
Dimethyl phthalate U 0.260 3.00 1 09/17/2023 15:45 WG2132824
Di-n-octyl phthalate U 0.932 3.00 1 09/17/2023 15:45 WG2132824
Pyrene U 0.107 1.00 1 09/17/2023 15:45 WG2132824
1,2,4-Trichlorobenzene U 0.0698 10.0 1 09/17/2023 15:45 WG2132824
4-Chloro-3-methylphenol U 0.131 10.0 1 09/17/2023 15:45 WG2132824
2-Chlorophenol U 0.133 10.0 1 09/17/2023 15:45 WG2132824
2,4-Dichlorophenol U 0.102 10.0 1 09/17/2023 15:45 WG2132824
2,4-Dimethylphenol U 0.0636 10.0 1 09/17/2023 15:45 WG2132824
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 09/17/2023 15:45 WG2132824
2,4-Dinitrophenol U 5.93 10.0 1 09/17/2023 15:45 WG2132824
2-Nitrophenol U 0.117 10.0 1 09/17/2023 15:45 WG2132824
4-Nitrophenol U 0.143 10.0 1 09/17/2023 15:45 WG2132824
Pentachlorophenol U 0.313 10.0 1 09/17/2023 15:45 WG2132824
Phenol U 4.33 10.0 1 09/17/2023 15:45 WG2132824
2,4,6-Trichlorophenol U 0.100 10.0 1 09/17/2023 15:45 WG2132824
(S) Nitrobenzene-d5 62.1 15.0-314 09/17/2023 15:45 WG2132824
(S) 2-Fluorobiphenyl 67.1 22.0-127 09/17/2023 15:45 WG2132824
(S) p-Terphenyl-d14 72.5 29.0-141 09/17/2023 15:45 WG2132824
(S) Phenol-d5 17.7 8.00-424 09/17/2023 15:45 WG2132824
(S) 2-Fluorophenol 24.7 10.0-120 09/17/2023 15:45 WG2132824
(S) 2,4,6-Tribromophenol 52.1 10.0-153 09/17/2023 15:45 WG2132824
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 30 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 30 of 78
SAMPLE RESULTS - 09
L1655691
MW-13
Collected date/time: 09/12/23 10:40
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.0941 1.00 1 09/21/2023 22:20 WG2136913
Bromobenzene U 0.118 1.00 1 09/21/2023 22:20 WG2136913
Bromodichloromethane U 0.136 1.00 1 09/21/2023 22:20 WG2136913
Bromochloromethane U 0.128 1.00 1 09/21/2023 22:20 WG2136913
Bromoform U 0.129 1.00 1 09/21/2023 22:20 WG2136913
Bromomethane U 0.605 5.00 1 09/22/2023 14:14 WG2137497
n-Butylbenzene U 0.157 1.00 1 09/21/2023 22:20 WG2136913
sec-Butylbenzene U 0.125 1.00 1 09/21/2023 22:20 WG2136913
tert-Butylbenzene U 0.127 1.00 1 09/21/2023 22:20 WG2136913
Carbon tetrachloride U 0.128 1.00 1 09/21/2023 22:20 WG2136913
Chlorobenzene U 0.116 1.00 1 09/21/2023 22:20 WG2136913
Chlorodibromomethane U 0.140 1.00 1 09/21/2023 22:20 WG2136913
Chloroethane U 0.192 5.00 1 09/21/2023 22:20 WG2136913
Chloroform U 0.111 5.00 1 09/21/2023 22:20 WG2136913
Chloromethane U 0.960 2.50 1 09/21/2023 22:20 WG2136913
2-Chlorotoluene U 0.106 1.00 1 09/21/2023 22:20 WG2136913
4-Chlorotoluene U 0.114 1.00 1 09/21/2023 22:20 WG2136913
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 09/21/2023 22:20 WG2136913
1,2-Dibromoethane U 0.126 1.00 1 09/21/2023 22:20 WG2136913
Dibromomethane U 0.122 1.00 1 09/21/2023 22:20 WG2136913
1,2-Dichlorobenzene U 0.107 1.00 1 09/21/2023 22:20 WG2136913
1,3-Dichlorobenzene U 0.110 1.00 1 09/21/2023 22:20 WG2136913
1,4-Dichlorobenzene U 0.120 1.00 1 09/21/2023 22:20 WG2136913
Dichlorodifluoromethane U 0.374 5.00 1 09/21/2023 22:20 WG2136913
1,1-Dichloroethane U 0.100 1.00 1 09/21/2023 22:20 WG2136913
1,2-Dichloroethane U 0.0819 1.00 1 09/21/2023 22:20 WG2136913
1,1-Dichloroethene U 0.188 1.00 1 09/21/2023 22:20 WG2136913
cis-1,2-Dichloroethene U 0.126 1.00 1 09/21/2023 22:20 WG2136913
trans-1,2-Dichloroethene U 0.149 1.00 1 09/21/2023 22:20 WG2136913
1,2-Dichloropropane U 0.149 1.00 1 09/21/2023 22:20 WG2136913
1,1-Dichloropropene U 0.142 1.00 1 09/21/2023 22:20 WG2136913
1,3-Dichloropropane U 0.110 1.00 1 09/21/2023 22:20 WG2136913
cis-1,3-Dichloropropene U 0.111 1.00 1 09/21/2023 22:20 WG2136913
trans-1,3-Dichloropropene U 0.118 1.00 1 09/21/2023 22:20 WG2136913
2,2-Dichloropropane U 0.161 1.00 1 09/21/2023 22:20 WG2136913
Di-isopropyl ether U 0.105 1.00 1 09/21/2023 22:20 WG2136913
Ethylbenzene U 0.137 1.00 1 09/21/2023 22:20 WG2136913
Hexachloro-1,3-butadiene U 0.337 1.00 1 09/21/2023 22:20 WG2136913
Isopropylbenzene U 0.105 1.00 1 09/21/2023 22:20 WG2136913
Methylene Chloride U 0.430 5.00 1 09/21/2023 22:20 WG2136913
Methyl tert-butyl ether U 0.101 1.00 1 09/21/2023 22:20 WG2136913
Naphthalene U 1.00 5.00 1 09/21/2023 22:20 WG2136913
n-Propylbenzene U 0.0993 1.00 1 09/21/2023 22:20 WG2136913
Styrene U 0.118 1.00 1 09/21/2023 22:20 WG2136913
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 09/21/2023 22:20 WG2136913
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 09/21/2023 22:20 WG2136913
Tetrachloroethene U 0.300 1.00 1 09/21/2023 22:20 WG2136913
Toluene U 0.278 1.00 1 09/21/2023 22:20 WG2136913
1,2,3-Trichlorobenzene U 0.230 1.00 1 09/21/2023 22:20 WG2136913
1,2,4-Trichlorobenzene U 0.481 1.00 1 09/21/2023 22:20 WG2136913
1,1,1-Trichloroethane U 0.149 1.00 1 09/21/2023 22:20 WG2136913
1,1,2-Trichloroethane U 0.158 1.00 1 09/21/2023 22:20 WG2136913
Trichloroethene U 0.190 1.00 1 09/21/2023 22:20 WG2136913
Trichlorofluoromethane U 0.160 5.00 1 09/22/2023 14:14 WG2137497
1,2,3-Trichloropropane U 0.237 2.50 1 09/21/2023 22:20 WG2136913
1,2,4-Trimethylbenzene U 0.322 1.00 1 09/21/2023 22:20 WG2136913
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 31 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 31 of 78
SAMPLE RESULTS - 09
L1655691
MW-13
Collected date/time: 09/12/23 10:40
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene U 0.104 1.00 1 09/21/2023 22:20 WG2136913
Vinyl chloride U 0.234 1.00 1 09/21/2023 22:20 WG2136913
o-Xylene U 0.174 1.00 1 09/21/2023 22:20 WG2136913
m&p-Xylenes U 0.430 2.00 1 09/21/2023 22:20 WG2136913
ethanol U 42.0 100 1 09/21/2023 22:20 WG2136913
tert-Amyl Methyl Ether U 0.195 1.00 1 09/21/2023 22:20 WG2136913
Ethyl tert-butyl ether U 0.101 1.00 1 09/21/2023 22:20 WG2136913
tert-Butyl alcohol U 4.06 5.00 1 09/21/2023 22:20 WG2136913
t-Amyl Alcohol U 4.90 50.0 1 09/21/2023 22:20 WG2136913
tert-Butyl formate U J4 4.51 20.0 1 09/21/2023 22:20 WG2136913
(S) Toluene-d8 98.1 80.0-120 09/21/2023 22:20 WG2136913
(S) Toluene-d8 105 80.0-120 09/22/2023 14:14 WG2137497
(S) 4-Bromofluorobenzene 92.3 77.0-126 09/21/2023 22:20 WG2136913
(S) 4-Bromofluorobenzene 99.4 77.0-126 09/22/2023 14:14 WG2137497
(S) 1,2-Dichloroethane-d4 98.8 70.0-130 09/21/2023 22:20 WG2136913
(S) 1,2-Dichloroethane-d4 102 70.0-130 09/22/2023 14:14 WG2137497
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 36.4 B J 33.3 100 1 09/21/2023 00:45 WG2135760
Unadjusted C19-C36 Aliphatics 66.7 B J 33.3 100 1 09/21/2023 00:45 WG2135760
Unadjusted C11-C22 Aromatics 49.8 B J 33.3 100 1 09/21/2023 02:36 WG2135760
Unadjusted Total Petroleum
Hydrocarbons 153 33.3 100 1 09/21/2023 02:36 WG2135760
(S) o-Terphenyl 81.6 40.0-140 09/21/2023 02:36 WG2135760
(S) 1-Chloro-octadecane 34.7 J2 40.0-140 09/21/2023 00:45 WG2135760
(S) 2-Fluorobiphenyl 97.1 40.0-140 09/21/2023 02:36 WG2135760
(S) 2-Bromonaphthalene 97.2 40.0-140 09/21/2023 02:36 WG2135760
Sample Narrative:
L1655691-09 WG2135760: Sample produced emulsion during Extraction process, low surr/spike recoveries due to matrix.
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 09/17/2023 16:06 WG2132824
Acenaphthylene U 0.0921 1.00 1 09/17/2023 16:06 WG2132824
Anthracene U 0.0804 1.00 1 09/17/2023 16:06 WG2132824
Benzo(a)anthracene U 0.199 1.00 1 09/17/2023 16:06 WG2132824
Benzo(b)fluoranthene U 0.130 1.00 1 09/17/2023 16:06 WG2132824
Benzo(k)fluoranthene U 0.120 1.00 1 09/17/2023 16:06 WG2132824
Benzo(g,h,i)perylene U 0.121 1.00 1 09/17/2023 16:06 WG2132824
Benzo(a)pyrene U 0.0381 1.00 1 09/17/2023 16:06 WG2132824
Bis(2-chlorethoxy)methane U 0.116 10.0 1 09/17/2023 16:06 WG2132824
Bis(2-chloroethyl)ether U 0.137 10.0 1 09/17/2023 16:06 WG2132824
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 09/17/2023 16:06 WG2132824
4-Bromophenyl-phenylether U J4 0.0877 10.0 1 09/17/2023 16:06 WG2132824
2-Chloronaphthalene U J4 0.0648 1.00 1 09/17/2023 16:06 WG2132824
4-Chlorophenyl-phenylether U 0.0926 10.0 1 09/17/2023 16:06 WG2132824
Chrysene U 0.130 1.00 1 09/17/2023 16:06 WG2132824
Dibenz(a,h)anthracene U 0.0644 1.00 1 09/17/2023 16:06 WG2132824
3,3-Dichlorobenzidine U 0.212 10.0 1 09/17/2023 16:06 WG2132824
2,4-Dinitrotoluene U 0.0983 10.0 1 09/17/2023 16:06 WG2132824
2,6-Dinitrotoluene U 0.250 10.0 1 09/17/2023 16:06 WG2132824
Fluoranthene U 0.102 1.00 1 09/17/2023 16:06 WG2132824
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 32 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 32 of 78
SAMPLE RESULTS - 09
L1655691
MW-13
Collected date/time: 09/12/23 10:40
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Fluorene U J4 0.0844 1.00 1 09/17/2023 16:06 WG2132824
Hexachlorobenzene U 0.0755 1.00 1 09/17/2023 16:06 WG2132824
Hexachloro-1,3-butadiene U 0.0968 10.0 1 09/17/2023 16:06 WG2132824
Hexachlorocyclopentadiene U 0.0598 10.0 1 09/17/2023 16:06 WG2132824
Hexachloroethane U 0.127 10.0 1 09/17/2023 16:06 WG2132824
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 09/17/2023 16:06 WG2132824
Isophorone U 0.143 10.0 1 09/17/2023 16:06 WG2132824
Naphthalene U 0.159 1.00 1 09/17/2023 16:06 WG2132824
Nitrobenzene U 0.297 10.0 1 09/17/2023 16:06 WG2132824
n-Nitrosodimethylamine U 0.998 10.0 1 09/17/2023 16:06 WG2132824
n-Nitrosodiphenylamine U 2.37 10.0 1 09/17/2023 16:06 WG2132824
n-Nitrosodi-n-propylamine U 0.261 10.0 1 09/17/2023 16:06 WG2132824
Phenanthrene U J4 0.112 1.00 1 09/17/2023 16:06 WG2132824
Benzylbutyl phthalate U 0.765 3.00 1 09/17/2023 16:06 WG2132824
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 09/17/2023 16:06 WG2132824
Di-n-butyl phthalate U 0.453 3.00 1 09/17/2023 16:06 WG2132824
Diethyl phthalate U 0.287 3.00 1 09/17/2023 16:06 WG2132824
Dimethyl phthalate U 0.260 3.00 1 09/17/2023 16:06 WG2132824
Di-n-octyl phthalate U 0.932 3.00 1 09/17/2023 16:06 WG2132824
Pyrene U 0.107 1.00 1 09/17/2023 16:06 WG2132824
1,2,4-Trichlorobenzene U 0.0698 10.0 1 09/17/2023 16:06 WG2132824
4-Chloro-3-methylphenol U 0.131 10.0 1 09/17/2023 16:06 WG2132824
2-Chlorophenol U 0.133 10.0 1 09/17/2023 16:06 WG2132824
2,4-Dichlorophenol U 0.102 10.0 1 09/17/2023 16:06 WG2132824
2,4-Dimethylphenol U 0.0636 10.0 1 09/17/2023 16:06 WG2132824
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 09/17/2023 16:06 WG2132824
2,4-Dinitrophenol U 5.93 10.0 1 09/17/2023 16:06 WG2132824
2-Nitrophenol U 0.117 10.0 1 09/17/2023 16:06 WG2132824
4-Nitrophenol U 0.143 10.0 1 09/17/2023 16:06 WG2132824
Pentachlorophenol U 0.313 10.0 1 09/17/2023 16:06 WG2132824
Phenol U 4.33 10.0 1 09/17/2023 16:06 WG2132824
2,4,6-Trichlorophenol U 0.100 10.0 1 09/17/2023 16:06 WG2132824
(S) Nitrobenzene-d5 44.3 15.0-314 09/17/2023 16:06 WG2132824
(S) 2-Fluorobiphenyl 45.0 22.0-127 09/17/2023 16:06 WG2132824
(S) p-Terphenyl-d14 34.5 29.0-141 09/17/2023 16:06 WG2132824
(S) Phenol-d5 13.5 8.00-424 09/17/2023 16:06 WG2132824
(S) 2-Fluorophenol 19.5 10.0-120 09/17/2023 16:06 WG2132824
(S) 2,4,6-Tribromophenol 32.6 10.0-153 09/17/2023 16:06 WG2132824
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 33 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 33 of 78
SAMPLE RESULTS - 10
L1655691
MW-1D
Collected date/time: 09/13/23 12:45
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.0941 1.00 1 09/21/2023 22:41 WG2136913
Bromobenzene U 0.118 1.00 1 09/21/2023 22:41 WG2136913
Bromodichloromethane U 0.136 1.00 1 09/21/2023 22:41 WG2136913
Bromochloromethane U 0.128 1.00 1 09/21/2023 22:41 WG2136913
Bromoform U 0.129 1.00 1 09/21/2023 22:41 WG2136913
Bromomethane U 0.605 5.00 1 09/22/2023 14:36 WG2137497
n-Butylbenzene U 0.157 1.00 1 09/21/2023 22:41 WG2136913
sec-Butylbenzene U 0.125 1.00 1 09/21/2023 22:41 WG2136913
tert-Butylbenzene U 0.127 1.00 1 09/21/2023 22:41 WG2136913
Carbon tetrachloride U 0.128 1.00 1 09/21/2023 22:41 WG2136913
Chlorobenzene U 0.116 1.00 1 09/21/2023 22:41 WG2136913
Chlorodibromomethane U 0.140 1.00 1 09/21/2023 22:41 WG2136913
Chloroethane U 0.192 5.00 1 09/21/2023 22:41 WG2136913
Chloroform U 0.111 5.00 1 09/21/2023 22:41 WG2136913
Chloromethane U 0.960 2.50 1 09/21/2023 22:41 WG2136913
2-Chlorotoluene U 0.106 1.00 1 09/21/2023 22:41 WG2136913
4-Chlorotoluene U 0.114 1.00 1 09/21/2023 22:41 WG2136913
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 09/21/2023 22:41 WG2136913
1,2-Dibromoethane U 0.126 1.00 1 09/21/2023 22:41 WG2136913
Dibromomethane U 0.122 1.00 1 09/21/2023 22:41 WG2136913
1,2-Dichlorobenzene U 0.107 1.00 1 09/21/2023 22:41 WG2136913
1,3-Dichlorobenzene U 0.110 1.00 1 09/21/2023 22:41 WG2136913
1,4-Dichlorobenzene U 0.120 1.00 1 09/21/2023 22:41 WG2136913
Dichlorodifluoromethane U 0.374 5.00 1 09/21/2023 22:41 WG2136913
1,1-Dichloroethane U 0.100 1.00 1 09/21/2023 22:41 WG2136913
1,2-Dichloroethane U 0.0819 1.00 1 09/21/2023 22:41 WG2136913
1,1-Dichloroethene U 0.188 1.00 1 09/21/2023 22:41 WG2136913
cis-1,2-Dichloroethene U 0.126 1.00 1 09/21/2023 22:41 WG2136913
trans-1,2-Dichloroethene U 0.149 1.00 1 09/21/2023 22:41 WG2136913
1,2-Dichloropropane U 0.149 1.00 1 09/21/2023 22:41 WG2136913
1,1-Dichloropropene U 0.142 1.00 1 09/21/2023 22:41 WG2136913
1,3-Dichloropropane U 0.110 1.00 1 09/21/2023 22:41 WG2136913
cis-1,3-Dichloropropene U 0.111 1.00 1 09/21/2023 22:41 WG2136913
trans-1,3-Dichloropropene U 0.118 1.00 1 09/21/2023 22:41 WG2136913
2,2-Dichloropropane U 0.161 1.00 1 09/21/2023 22:41 WG2136913
Di-isopropyl ether U 0.105 1.00 1 09/21/2023 22:41 WG2136913
Ethylbenzene U 0.137 1.00 1 09/21/2023 22:41 WG2136913
Hexachloro-1,3-butadiene U 0.337 1.00 1 09/21/2023 22:41 WG2136913
Isopropylbenzene U 0.105 1.00 1 09/21/2023 22:41 WG2136913
Methylene Chloride U 0.430 5.00 1 09/21/2023 22:41 WG2136913
Methyl tert-butyl ether U 0.101 1.00 1 09/21/2023 22:41 WG2136913
Naphthalene U 1.00 5.00 1 09/21/2023 22:41 WG2136913
n-Propylbenzene U 0.0993 1.00 1 09/21/2023 22:41 WG2136913
Styrene U 0.118 1.00 1 09/21/2023 22:41 WG2136913
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 09/21/2023 22:41 WG2136913
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 09/21/2023 22:41 WG2136913
Tetrachloroethene U 0.300 1.00 1 09/21/2023 22:41 WG2136913
Toluene U 0.278 1.00 1 09/21/2023 22:41 WG2136913
1,2,3-Trichlorobenzene U 0.230 1.00 1 09/21/2023 22:41 WG2136913
1,2,4-Trichlorobenzene U 0.481 1.00 1 09/21/2023 22:41 WG2136913
1,1,1-Trichloroethane U 0.149 1.00 1 09/21/2023 22:41 WG2136913
1,1,2-Trichloroethane U 0.158 1.00 1 09/21/2023 22:41 WG2136913
Trichloroethene U 0.190 1.00 1 09/21/2023 22:41 WG2136913
Trichlorofluoromethane U 0.160 5.00 1 09/22/2023 14:36 WG2137497
1,2,3-Trichloropropane U 0.237 2.50 1 09/21/2023 22:41 WG2136913
1,2,4-Trimethylbenzene U 0.322 1.00 1 09/21/2023 22:41 WG2136913
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 34 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 34 of 78
SAMPLE RESULTS - 10
L1655691
MW-1D
Collected date/time: 09/13/23 12:45
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene U 0.104 1.00 1 09/21/2023 22:41 WG2136913
Vinyl chloride U 0.234 1.00 1 09/21/2023 22:41 WG2136913
o-Xylene U 0.174 1.00 1 09/21/2023 22:41 WG2136913
m&p-Xylenes U 0.430 2.00 1 09/21/2023 22:41 WG2136913
ethanol U 42.0 100 1 09/21/2023 22:41 WG2136913
tert-Amyl Methyl Ether U 0.195 1.00 1 09/21/2023 22:41 WG2136913
Ethyl tert-butyl ether U 0.101 1.00 1 09/21/2023 22:41 WG2136913
tert-Butyl alcohol U 4.06 5.00 1 09/21/2023 22:41 WG2136913
t-Amyl Alcohol U 4.90 50.0 1 09/21/2023 22:41 WG2136913
tert-Butyl formate U J4 4.51 20.0 1 09/21/2023 22:41 WG2136913
(S) Toluene-d8 98.6 80.0-120 09/21/2023 22:41 WG2136913
(S) Toluene-d8 104 80.0-120 09/22/2023 14:36 WG2137497
(S) 4-Bromofluorobenzene 92.0 77.0-126 09/21/2023 22:41 WG2136913
(S) 4-Bromofluorobenzene 101 77.0-126 09/22/2023 14:36 WG2137497
(S) 1,2-Dichloroethane-d4 98.2 70.0-130 09/21/2023 22:41 WG2136913
(S) 1,2-Dichloroethane-d4 104 70.0-130 09/22/2023 14:36 WG2137497
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 44.4 B J 33.3 100 1 09/21/2023 01:07 WG2135760
Unadjusted C19-C36 Aliphatics 64.0 B J 33.3 100 1 09/21/2023 01:07 WG2135760
Unadjusted C11-C22 Aromatics 49.7 B J 33.3 100 1 09/21/2023 02:14 WG2135760
Unadjusted Total Petroleum
Hydrocarbons 158 33.3 100 1 09/21/2023 02:14 WG2135760
(S) o-Terphenyl 82.8 40.0-140 09/21/2023 02:14 WG2135760
(S) 1-Chloro-octadecane 64.7 40.0-140 09/21/2023 01:07 WG2135760
(S) 2-Fluorobiphenyl 91.1 40.0-140 09/21/2023 02:14 WG2135760
(S) 2-Bromonaphthalene 90.3 40.0-140 09/21/2023 02:14 WG2135760
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 09/21/2023 03:38 WG2134767
Acenaphthylene U 0.0921 1.00 1 09/21/2023 03:38 WG2134767
Anthracene U 0.0804 1.00 1 09/21/2023 03:38 WG2134767
Benzo(a)anthracene U 0.199 1.00 1 09/21/2023 03:38 WG2134767
Benzo(b)fluoranthene U 0.130 1.00 1 09/21/2023 03:38 WG2134767
Benzo(k)fluoranthene U 0.120 1.00 1 09/21/2023 03:38 WG2134767
Benzo(g,h,i)perylene U 0.121 1.00 1 09/21/2023 03:38 WG2134767
Benzo(a)pyrene U 0.0381 1.00 1 09/21/2023 03:38 WG2134767
Bis(2-chlorethoxy)methane U 0.116 10.0 1 09/21/2023 03:38 WG2134767
Bis(2-chloroethyl)ether U 0.137 10.0 1 09/21/2023 03:38 WG2134767
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 09/21/2023 03:38 WG2134767
4-Bromophenyl-phenylether U J4 0.0877 10.0 1 09/21/2023 03:38 WG2134767
2-Chloronaphthalene U J4 0.0648 1.00 1 09/21/2023 03:38 WG2134767
4-Chlorophenyl-phenylether U 0.0926 10.0 1 09/21/2023 03:38 WG2134767
Chrysene U 0.130 1.00 1 09/21/2023 03:38 WG2134767
Dibenz(a,h)anthracene U 0.0644 1.00 1 09/21/2023 03:38 WG2134767
3,3-Dichlorobenzidine U 0.212 10.0 1 09/21/2023 03:38 WG2134767
2,4-Dinitrotoluene U 0.0983 10.0 1 09/21/2023 03:38 WG2134767
2,6-Dinitrotoluene U 0.250 10.0 1 09/21/2023 03:38 WG2134767
Fluoranthene U 0.102 1.00 1 09/21/2023 03:38 WG2134767
Fluorene U J4 0.0844 1.00 1 09/21/2023 03:38 WG2134767
Hexachlorobenzene U 0.0755 1.00 1 09/21/2023 03:38 WG2134767
Hexachloro-1,3-butadiene U 0.0968 10.0 1 09/21/2023 03:38 WG2134767
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 35 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 35 of 78
SAMPLE RESULTS - 10
L1655691
MW-1D
Collected date/time: 09/13/23 12:45
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexachlorocyclopentadiene U 0.0598 10.0 1 09/21/2023 03:38 WG2134767
Hexachloroethane U 0.127 10.0 1 09/21/2023 03:38 WG2134767
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 09/21/2023 03:38 WG2134767
Isophorone U 0.143 10.0 1 09/21/2023 03:38 WG2134767
Naphthalene U 0.159 1.00 1 09/21/2023 03:38 WG2134767
Nitrobenzene U 0.297 10.0 1 09/21/2023 03:38 WG2134767
n-Nitrosodimethylamine U 0.998 10.0 1 09/21/2023 03:38 WG2134767
n-Nitrosodiphenylamine U 2.37 10.0 1 09/21/2023 03:38 WG2134767
n-Nitrosodi-n-propylamine U 0.261 10.0 1 09/21/2023 03:38 WG2134767
Phenanthrene U J4 0.112 1.00 1 09/21/2023 03:38 WG2134767
Benzylbutyl phthalate U 0.765 3.00 1 09/21/2023 03:38 WG2134767
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 09/21/2023 03:38 WG2134767
Di-n-butyl phthalate U 0.453 3.00 1 09/21/2023 03:38 WG2134767
Diethyl phthalate U 0.287 3.00 1 09/21/2023 03:38 WG2134767
Dimethyl phthalate U 0.260 3.00 1 09/21/2023 03:38 WG2134767
Di-n-octyl phthalate U 0.932 3.00 1 09/21/2023 03:38 WG2134767
Pyrene U 0.107 1.00 1 09/21/2023 03:38 WG2134767
1,2,4-Trichlorobenzene U 0.0698 10.0 1 09/21/2023 03:38 WG2134767
4-Chloro-3-methylphenol U 0.131 10.0 1 09/21/2023 03:38 WG2134767
2-Chlorophenol U 0.133 10.0 1 09/21/2023 03:38 WG2134767
2,4-Dichlorophenol U 0.102 10.0 1 09/21/2023 03:38 WG2134767
2,4-Dimethylphenol U 0.0636 10.0 1 09/21/2023 03:38 WG2134767
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 09/21/2023 03:38 WG2134767
2,4-Dinitrophenol U 5.93 10.0 1 09/21/2023 03:38 WG2134767
2-Nitrophenol U 0.117 10.0 1 09/21/2023 03:38 WG2134767
4-Nitrophenol U J4 0.143 10.0 1 09/21/2023 03:38 WG2134767
Pentachlorophenol U 0.313 10.0 1 09/21/2023 03:38 WG2134767
Phenol U 4.33 10.0 1 09/21/2023 03:38 WG2134767
2,4,6-Trichlorophenol U 0.100 10.0 1 09/21/2023 03:38 WG2134767
(S) Nitrobenzene-d5 48.0 15.0-314 09/21/2023 03:38 WG2134767
(S) 2-Fluorobiphenyl 43.4 22.0-127 09/21/2023 03:38 WG2134767
(S) p-Terphenyl-d14 51.1 29.0-141 09/21/2023 03:38 WG2134767
(S) Phenol-d5 12.3 8.00-424 09/21/2023 03:38 WG2134767
(S) 2-Fluorophenol 16.8 10.0-120 09/21/2023 03:38 WG2134767
(S) 2,4,6-Tribromophenol 31.0 10.0-153 09/21/2023 03:38 WG2134767
Sample Narrative:
L1655691-10 WG2134767: Duplicate Analysis performed due to QC failure. Reporting most compliant data.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 36 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 36 of 78
SAMPLE RESULTS - 11
L1655691
MW-4D
Collected date/time: 09/13/23 11:50
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene 1880 4.71 50.0 50 09/22/2023 00:32 WG2136913
Bromobenzene U 5.90 50.0 50 09/22/2023 00:32 WG2136913
Bromodichloromethane U 6.80 50.0 50 09/22/2023 00:32 WG2136913
Bromochloromethane U 6.40 50.0 50 09/22/2023 00:32 WG2136913
Bromoform U 6.45 50.0 50 09/22/2023 00:32 WG2136913
Bromomethane U 30.3 250 50 09/22/2023 18:54 WG2137497
n-Butylbenzene U 7.85 50.0 50 09/22/2023 00:32 WG2136913
sec-Butylbenzene U 6.25 50.0 50 09/22/2023 00:32 WG2136913
tert-Butylbenzene U 6.35 50.0 50 09/22/2023 00:32 WG2136913
Carbon tetrachloride U 6.40 50.0 50 09/22/2023 00:32 WG2136913
Chlorobenzene U 5.80 50.0 50 09/22/2023 00:32 WG2136913
Chlorodibromomethane U 7.00 50.0 50 09/22/2023 00:32 WG2136913
Chloroethane U 9.60 250 50 09/22/2023 00:32 WG2136913
Chloroform U 5.55 250 50 09/22/2023 00:32 WG2136913
Chloromethane U 48.0 125 50 09/22/2023 00:32 WG2136913
2-Chlorotoluene U 5.30 50.0 50 09/22/2023 00:32 WG2136913
4-Chlorotoluene U 5.70 50.0 50 09/22/2023 00:32 WG2136913
1,2-Dibromo-3-Chloropropane U 13.8 250 50 09/22/2023 00:32 WG2136913
1,2-Dibromoethane U 6.30 50.0 50 09/22/2023 00:32 WG2136913
Dibromomethane U 6.10 50.0 50 09/22/2023 00:32 WG2136913
1,2-Dichlorobenzene U 5.35 50.0 50 09/22/2023 00:32 WG2136913
1,3-Dichlorobenzene U 5.50 50.0 50 09/22/2023 00:32 WG2136913
1,4-Dichlorobenzene U 6.00 50.0 50 09/22/2023 00:32 WG2136913
Dichlorodifluoromethane U 18.7 250 50 09/22/2023 00:32 WG2136913
1,1-Dichloroethane U 5.00 50.0 50 09/22/2023 00:32 WG2136913
1,2-Dichloroethane U 4.09 50.0 50 09/22/2023 00:32 WG2136913
1,1-Dichloroethene U 9.40 50.0 50 09/22/2023 00:32 WG2136913
cis-1,2-Dichloroethene U 6.30 50.0 50 09/22/2023 00:32 WG2136913
trans-1,2-Dichloroethene U 7.45 50.0 50 09/22/2023 00:32 WG2136913
1,2-Dichloropropane U 7.45 50.0 50 09/22/2023 00:32 WG2136913
1,1-Dichloropropene U 7.10 50.0 50 09/22/2023 00:32 WG2136913
1,3-Dichloropropane U 5.50 50.0 50 09/22/2023 00:32 WG2136913
cis-1,3-Dichloropropene U 5.55 50.0 50 09/22/2023 00:32 WG2136913
trans-1,3-Dichloropropene U 5.90 50.0 50 09/22/2023 00:32 WG2136913
2,2-Dichloropropane U 8.05 50.0 50 09/22/2023 00:32 WG2136913
Di-isopropyl ether 6.60 J 5.25 50.0 50 09/22/2023 00:32 WG2136913
Ethylbenzene 158 6.85 50.0 50 09/22/2023 18:54 WG2137497
Hexachloro-1,3-butadiene U 16.9 50.0 50 09/22/2023 00:32 WG2136913
Isopropylbenzene 13.8 J 5.25 50.0 50 09/22/2023 00:32 WG2136913
Methylene Chloride U 21.5 250 50 09/22/2023 00:32 WG2136913
Methyl tert-butyl ether 10.7 J 5.05 50.0 50 09/22/2023 00:32 WG2136913
Naphthalene U 50.0 250 50 09/22/2023 00:32 WG2136913
n-Propylbenzene 16.1 J 4.97 50.0 50 09/22/2023 00:32 WG2136913
Styrene U 5.90 50.0 50 09/22/2023 00:32 WG2136913
1,1,1,2-Tetrachloroethane U 7.35 50.0 50 09/22/2023 00:32 WG2136913
1,1,2,2-Tetrachloroethane U 6.65 50.0 50 09/22/2023 00:32 WG2136913
Tetrachloroethene U 15.0 50.0 50 09/22/2023 00:32 WG2136913
Toluene 129 13.9 50.0 50 09/22/2023 18:54 WG2137497
1,2,3-Trichlorobenzene U 11.5 50.0 50 09/22/2023 00:32 WG2136913
1,2,4-Trichlorobenzene U 24.1 50.0 50 09/22/2023 00:32 WG2136913
1,1,1-Trichloroethane U 7.45 50.0 50 09/22/2023 00:32 WG2136913
1,1,2-Trichloroethane U 7.90 50.0 50 09/22/2023 00:32 WG2136913
Trichloroethene U 9.50 50.0 50 09/22/2023 00:32 WG2136913
Trichlorofluoromethane U 8.00 250 50 09/22/2023 18:54 WG2137497
1,2,3-Trichloropropane U 11.9 125 50 09/22/2023 00:32 WG2136913
1,2,4-Trimethylbenzene 102 16.1 50.0 50 09/22/2023 00:32 WG2136913
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 37 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 37 of 78
SAMPLE RESULTS - 11
L1655691
MW-4D
Collected date/time: 09/13/23 11:50
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene 31.0 J 5.20 50.0 50 09/22/2023 00:32 WG2136913
Vinyl chloride U 11.7 50.0 50 09/22/2023 00:32 WG2136913
o-Xylene 296 8.70 50.0 50 09/22/2023 18:54 WG2137497
m&p-Xylenes 364 21.5 100 50 09/22/2023 18:54 WG2137497
ethanol U 2100 5000 50 09/22/2023 00:32 WG2136913
tert-Amyl Methyl Ether U 9.75 50.0 50 09/22/2023 00:32 WG2136913
Ethyl tert-butyl ether U 5.05 50.0 50 09/22/2023 00:32 WG2136913
tert-Butyl alcohol U 203 250 50 09/22/2023 00:32 WG2136913
t-Amyl Alcohol 1080 J 245 2500 50 09/22/2023 00:32 WG2136913
tert-Butyl formate U J4 226 1000 50 09/22/2023 00:32 WG2136913
(S) Toluene-d8 99.1 80.0-120 09/22/2023 00:32 WG2136913
(S) Toluene-d8 104 80.0-120 09/22/2023 18:54 WG2137497
(S) 4-Bromofluorobenzene 93.4 77.0-126 09/22/2023 00:32 WG2136913
(S) 4-Bromofluorobenzene 99.9 77.0-126 09/22/2023 18:54 WG2137497
(S) 1,2-Dichloroethane-d4 96.1 70.0-130 09/22/2023 00:32 WG2136913
(S) 1,2-Dichloroethane-d4 103 70.0-130 09/22/2023 18:54 WG2137497
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 37.4 B J 33.3 100 1 09/21/2023 01:29 WG2135760
Unadjusted C19-C36 Aliphatics 62.7 B J 33.3 100 1 09/21/2023 01:29 WG2135760
Unadjusted C11-C22 Aromatics 108 B 33.3 100 1 09/21/2023 01:52 WG2135760
Unadjusted Total Petroleum
Hydrocarbons 208 33.3 100 1 09/21/2023 01:52 WG2135760
(S) o-Terphenyl 90.5 40.0-140 09/21/2023 01:52 WG2135760
(S) 1-Chloro-octadecane 87.9 40.0-140 09/21/2023 01:29 WG2135760
(S) 2-Fluorobiphenyl 98.9 40.0-140 09/21/2023 01:52 WG2135760
(S) 2-Bromonaphthalene 99.6 40.0-140 09/21/2023 01:52 WG2135760
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 09/21/2023 03:59 WG2134767
Acenaphthylene U 0.0921 1.00 1 09/21/2023 03:59 WG2134767
Anthracene U 0.0804 1.00 1 09/21/2023 03:59 WG2134767
Benzo(a)anthracene U 0.199 1.00 1 09/21/2023 03:59 WG2134767
Benzo(b)fluoranthene U 0.130 1.00 1 09/21/2023 03:59 WG2134767
Benzo(k)fluoranthene U 0.120 1.00 1 09/21/2023 03:59 WG2134767
Benzo(g,h,i)perylene U 0.121 1.00 1 09/21/2023 03:59 WG2134767
Benzo(a)pyrene U 0.0381 1.00 1 09/21/2023 03:59 WG2134767
Bis(2-chlorethoxy)methane U 0.116 10.0 1 09/21/2023 03:59 WG2134767
Bis(2-chloroethyl)ether U 0.137 10.0 1 09/21/2023 03:59 WG2134767
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 09/21/2023 03:59 WG2134767
4-Bromophenyl-phenylether U J4 0.0877 10.0 1 09/21/2023 03:59 WG2134767
2-Chloronaphthalene U J4 0.0648 1.00 1 09/21/2023 03:59 WG2134767
4-Chlorophenyl-phenylether U 0.0926 10.0 1 09/21/2023 03:59 WG2134767
Chrysene U 0.130 1.00 1 09/21/2023 03:59 WG2134767
Dibenz(a,h)anthracene U 0.0644 1.00 1 09/21/2023 03:59 WG2134767
3,3-Dichlorobenzidine U 0.212 10.0 1 09/21/2023 03:59 WG2134767
2,4-Dinitrotoluene U 0.0983 10.0 1 09/21/2023 03:59 WG2134767
2,6-Dinitrotoluene U 0.250 10.0 1 09/21/2023 03:59 WG2134767
Fluoranthene U 0.102 1.00 1 09/21/2023 03:59 WG2134767
Fluorene U J4 0.0844 1.00 1 09/21/2023 03:59 WG2134767
Hexachlorobenzene U 0.0755 1.00 1 09/21/2023 03:59 WG2134767
Hexachloro-1,3-butadiene U 0.0968 10.0 1 09/21/2023 03:59 WG2134767
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 38 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 38 of 78
SAMPLE RESULTS - 11
L1655691
MW-4D
Collected date/time: 09/13/23 11:50
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexachlorocyclopentadiene U 0.0598 10.0 1 09/21/2023 03:59 WG2134767
Hexachloroethane U 0.127 10.0 1 09/21/2023 03:59 WG2134767
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 09/21/2023 03:59 WG2134767
Isophorone U 0.143 10.0 1 09/21/2023 03:59 WG2134767
Naphthalene 12.4 0.159 1.00 1 09/21/2023 03:59 WG2134767
Nitrobenzene U 0.297 10.0 1 09/21/2023 03:59 WG2134767
n-Nitrosodimethylamine U 0.998 10.0 1 09/21/2023 03:59 WG2134767
n-Nitrosodiphenylamine U 2.37 10.0 1 09/21/2023 03:59 WG2134767
n-Nitrosodi-n-propylamine U 0.261 10.0 1 09/21/2023 03:59 WG2134767
Phenanthrene U J4 0.112 1.00 1 09/21/2023 03:59 WG2134767
Benzylbutyl phthalate U 0.765 3.00 1 09/21/2023 03:59 WG2134767
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 09/21/2023 03:59 WG2134767
Di-n-butyl phthalate U 0.453 3.00 1 09/21/2023 03:59 WG2134767
Diethyl phthalate U 0.287 3.00 1 09/21/2023 03:59 WG2134767
Dimethyl phthalate U 0.260 3.00 1 09/21/2023 03:59 WG2134767
Di-n-octyl phthalate U 0.932 3.00 1 09/21/2023 03:59 WG2134767
Pyrene U 0.107 1.00 1 09/21/2023 03:59 WG2134767
1,2,4-Trichlorobenzene U 0.0698 10.0 1 09/21/2023 03:59 WG2134767
4-Chloro-3-methylphenol U 0.131 10.0 1 09/21/2023 03:59 WG2134767
2-Chlorophenol U 0.133 10.0 1 09/21/2023 03:59 WG2134767
2,4-Dichlorophenol U 0.102 10.0 1 09/21/2023 03:59 WG2134767
2,4-Dimethylphenol U 0.0636 10.0 1 09/21/2023 03:59 WG2134767
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 09/21/2023 03:59 WG2134767
2,4-Dinitrophenol U 5.93 10.0 1 09/21/2023 03:59 WG2134767
2-Nitrophenol U 0.117 10.0 1 09/21/2023 03:59 WG2134767
4-Nitrophenol U J4 0.143 10.0 1 09/21/2023 03:59 WG2134767
Pentachlorophenol U 0.313 10.0 1 09/21/2023 03:59 WG2134767
Phenol U 4.33 10.0 1 09/21/2023 03:59 WG2134767
2,4,6-Trichlorophenol U 0.100 10.0 1 09/21/2023 03:59 WG2134767
(S) Nitrobenzene-d5 47.8 15.0-314 09/21/2023 03:59 WG2134767
(S) 2-Fluorobiphenyl 41.5 22.0-127 09/21/2023 03:59 WG2134767
(S) p-Terphenyl-d14 39.8 29.0-141 09/21/2023 03:59 WG2134767
(S) Phenol-d5 12.6 8.00-424 09/21/2023 03:59 WG2134767
(S) 2-Fluorophenol 18.8 10.0-120 09/21/2023 03:59 WG2134767
(S) 2,4,6-Tribromophenol 24.7 10.0-153 09/21/2023 03:59 WG2134767
Sample Narrative:
L1655691-11 WG2134767: Duplicate Analysis performed due to QC failure. Reporting most compliant data.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 39 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 39 of 78
SAMPLE RESULTS - 12
L1655691
MW-5D
Collected date/time: 09/13/23 09:50
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.0941 1.00 1 09/21/2023 23:03 WG2136913
Bromobenzene U 0.118 1.00 1 09/21/2023 23:03 WG2136913
Bromodichloromethane U 0.136 1.00 1 09/21/2023 23:03 WG2136913
Bromochloromethane U 0.128 1.00 1 09/21/2023 23:03 WG2136913
Bromoform U 0.129 1.00 1 09/21/2023 23:03 WG2136913
Bromomethane U 0.605 5.00 1 09/22/2023 14:57 WG2137497
n-Butylbenzene U 0.157 1.00 1 09/21/2023 23:03 WG2136913
sec-Butylbenzene U 0.125 1.00 1 09/21/2023 23:03 WG2136913
tert-Butylbenzene U 0.127 1.00 1 09/21/2023 23:03 WG2136913
Carbon tetrachloride U 0.128 1.00 1 09/21/2023 23:03 WG2136913
Chlorobenzene U 0.116 1.00 1 09/21/2023 23:03 WG2136913
Chlorodibromomethane U 0.140 1.00 1 09/21/2023 23:03 WG2136913
Chloroethane U 0.192 5.00 1 09/21/2023 23:03 WG2136913
Chloroform U 0.111 5.00 1 09/21/2023 23:03 WG2136913
Chloromethane U 0.960 2.50 1 09/21/2023 23:03 WG2136913
2-Chlorotoluene U 0.106 1.00 1 09/21/2023 23:03 WG2136913
4-Chlorotoluene U 0.114 1.00 1 09/21/2023 23:03 WG2136913
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 09/21/2023 23:03 WG2136913
1,2-Dibromoethane U 0.126 1.00 1 09/21/2023 23:03 WG2136913
Dibromomethane U 0.122 1.00 1 09/21/2023 23:03 WG2136913
1,2-Dichlorobenzene U 0.107 1.00 1 09/21/2023 23:03 WG2136913
1,3-Dichlorobenzene U 0.110 1.00 1 09/21/2023 23:03 WG2136913
1,4-Dichlorobenzene U 0.120 1.00 1 09/21/2023 23:03 WG2136913
Dichlorodifluoromethane U 0.374 5.00 1 09/21/2023 23:03 WG2136913
1,1-Dichloroethane U 0.100 1.00 1 09/21/2023 23:03 WG2136913
1,2-Dichloroethane U 0.0819 1.00 1 09/21/2023 23:03 WG2136913
1,1-Dichloroethene U 0.188 1.00 1 09/21/2023 23:03 WG2136913
cis-1,2-Dichloroethene U 0.126 1.00 1 09/21/2023 23:03 WG2136913
trans-1,2-Dichloroethene U 0.149 1.00 1 09/21/2023 23:03 WG2136913
1,2-Dichloropropane U 0.149 1.00 1 09/21/2023 23:03 WG2136913
1,1-Dichloropropene U 0.142 1.00 1 09/21/2023 23:03 WG2136913
1,3-Dichloropropane U 0.110 1.00 1 09/21/2023 23:03 WG2136913
cis-1,3-Dichloropropene U 0.111 1.00 1 09/21/2023 23:03 WG2136913
trans-1,3-Dichloropropene U 0.118 1.00 1 09/21/2023 23:03 WG2136913
2,2-Dichloropropane U 0.161 1.00 1 09/21/2023 23:03 WG2136913
Di-isopropyl ether U 0.105 1.00 1 09/21/2023 23:03 WG2136913
Ethylbenzene U 0.137 1.00 1 09/21/2023 23:03 WG2136913
Hexachloro-1,3-butadiene U 0.337 1.00 1 09/21/2023 23:03 WG2136913
Isopropylbenzene U 0.105 1.00 1 09/21/2023 23:03 WG2136913
Methylene Chloride U 0.430 5.00 1 09/21/2023 23:03 WG2136913
Methyl tert-butyl ether 0.122 J 0.101 1.00 1 09/21/2023 23:03 WG2136913
Naphthalene U 1.00 5.00 1 09/21/2023 23:03 WG2136913
n-Propylbenzene U 0.0993 1.00 1 09/21/2023 23:03 WG2136913
Styrene U 0.118 1.00 1 09/21/2023 23:03 WG2136913
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 09/21/2023 23:03 WG2136913
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 09/21/2023 23:03 WG2136913
Tetrachloroethene U 0.300 1.00 1 09/21/2023 23:03 WG2136913
Toluene U 0.278 1.00 1 09/21/2023 23:03 WG2136913
1,2,3-Trichlorobenzene U 0.230 1.00 1 09/21/2023 23:03 WG2136913
1,2,4-Trichlorobenzene U 0.481 1.00 1 09/21/2023 23:03 WG2136913
1,1,1-Trichloroethane U 0.149 1.00 1 09/21/2023 23:03 WG2136913
1,1,2-Trichloroethane U 0.158 1.00 1 09/21/2023 23:03 WG2136913
Trichloroethene U 0.190 1.00 1 09/21/2023 23:03 WG2136913
Trichlorofluoromethane U 0.160 5.00 1 09/22/2023 14:57 WG2137497
1,2,3-Trichloropropane U 0.237 2.50 1 09/21/2023 23:03 WG2136913
1,2,4-Trimethylbenzene U 0.322 1.00 1 09/21/2023 23:03 WG2136913
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 40 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 40 of 78
SAMPLE RESULTS - 12
L1655691
MW-5D
Collected date/time: 09/13/23 09:50
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene U 0.104 1.00 1 09/21/2023 23:03 WG2136913
Vinyl chloride U 0.234 1.00 1 09/21/2023 23:03 WG2136913
o-Xylene U 0.174 1.00 1 09/21/2023 23:03 WG2136913
m&p-Xylenes U 0.430 2.00 1 09/21/2023 23:03 WG2136913
ethanol U 42.0 100 1 09/21/2023 23:03 WG2136913
tert-Amyl Methyl Ether U 0.195 1.00 1 09/21/2023 23:03 WG2136913
Ethyl tert-butyl ether U 0.101 1.00 1 09/21/2023 23:03 WG2136913
tert-Butyl alcohol U 4.06 5.00 1 09/21/2023 23:03 WG2136913
t-Amyl Alcohol U 4.90 50.0 1 09/21/2023 23:03 WG2136913
tert-Butyl formate U J4 4.51 20.0 1 09/21/2023 23:03 WG2136913
(S) Toluene-d8 96.3 80.0-120 09/21/2023 23:03 WG2136913
(S) Toluene-d8 105 80.0-120 09/22/2023 14:57 WG2137497
(S) 4-Bromofluorobenzene 90.8 77.0-126 09/21/2023 23:03 WG2136913
(S) 4-Bromofluorobenzene 95.4 77.0-126 09/22/2023 14:57 WG2137497
(S) 1,2-Dichloroethane-d4 98.0 70.0-130 09/21/2023 23:03 WG2136913
(S) 1,2-Dichloroethane-d4 105 70.0-130 09/22/2023 14:57 WG2137497
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 34.3 B J 33.3 100 1 09/21/2023 07:15 WG2135760
Unadjusted C19-C36 Aliphatics 57.6 B J 33.3 100 1 09/21/2023 07:15 WG2135760
Unadjusted C11-C22 Aromatics 42.2 B J 33.3 100 1 09/21/2023 13:33 WG2135760
Unadjusted Total Petroleum
Hydrocarbons 134 33.3 100 1 09/21/2023 13:33 WG2135760
(S) o-Terphenyl 86.8 40.0-140 09/21/2023 13:33 WG2135760
(S) 1-Chloro-octadecane 79.2 40.0-140 09/21/2023 07:15 WG2135760
(S) 2-Fluorobiphenyl 93.7 40.0-140 09/21/2023 13:33 WG2135760
(S) 2-Bromonaphthalene 92.0 40.0-140 09/21/2023 13:33 WG2135760
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 09/21/2023 04:20 WG2134767
Acenaphthylene U 0.0921 1.00 1 09/21/2023 04:20 WG2134767
Anthracene U 0.0804 1.00 1 09/21/2023 04:20 WG2134767
Benzo(a)anthracene U 0.199 1.00 1 09/21/2023 04:20 WG2134767
Benzo(b)fluoranthene U 0.130 1.00 1 09/21/2023 04:20 WG2134767
Benzo(k)fluoranthene U 0.120 1.00 1 09/21/2023 04:20 WG2134767
Benzo(g,h,i)perylene U 0.121 1.00 1 09/21/2023 04:20 WG2134767
Benzo(a)pyrene U 0.0381 1.00 1 09/21/2023 04:20 WG2134767
Bis(2-chlorethoxy)methane U 0.116 10.0 1 09/21/2023 04:20 WG2134767
Bis(2-chloroethyl)ether U 0.137 10.0 1 09/21/2023 04:20 WG2134767
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 09/21/2023 04:20 WG2134767
4-Bromophenyl-phenylether U J4 0.0877 10.0 1 09/21/2023 04:20 WG2134767
2-Chloronaphthalene U J4 0.0648 1.00 1 09/21/2023 04:20 WG2134767
4-Chlorophenyl-phenylether U 0.0926 10.0 1 09/21/2023 04:20 WG2134767
Chrysene U 0.130 1.00 1 09/21/2023 04:20 WG2134767
Dibenz(a,h)anthracene U 0.0644 1.00 1 09/21/2023 04:20 WG2134767
3,3-Dichlorobenzidine U 0.212 10.0 1 09/21/2023 04:20 WG2134767
2,4-Dinitrotoluene U 0.0983 10.0 1 09/21/2023 04:20 WG2134767
2,6-Dinitrotoluene U 0.250 10.0 1 09/21/2023 04:20 WG2134767
Fluoranthene U 0.102 1.00 1 09/21/2023 04:20 WG2134767
Fluorene U J4 0.0844 1.00 1 09/21/2023 04:20 WG2134767
Hexachlorobenzene U 0.0755 1.00 1 09/21/2023 04:20 WG2134767
Hexachloro-1,3-butadiene U 0.0968 10.0 1 09/21/2023 04:20 WG2134767
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 41 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 41 of 78
SAMPLE RESULTS - 12
L1655691
MW-5D
Collected date/time: 09/13/23 09:50
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexachlorocyclopentadiene U 0.0598 10.0 1 09/21/2023 04:20 WG2134767
Hexachloroethane U 0.127 10.0 1 09/21/2023 04:20 WG2134767
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 09/21/2023 04:20 WG2134767
Isophorone U 0.143 10.0 1 09/21/2023 04:20 WG2134767
Naphthalene U 0.159 1.00 1 09/21/2023 04:20 WG2134767
Nitrobenzene U 0.297 10.0 1 09/21/2023 04:20 WG2134767
n-Nitrosodimethylamine U 0.998 10.0 1 09/21/2023 04:20 WG2134767
n-Nitrosodiphenylamine U 2.37 10.0 1 09/21/2023 04:20 WG2134767
n-Nitrosodi-n-propylamine U 0.261 10.0 1 09/21/2023 04:20 WG2134767
Phenanthrene U J4 0.112 1.00 1 09/21/2023 04:20 WG2134767
Benzylbutyl phthalate U 0.765 3.00 1 09/21/2023 04:20 WG2134767
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 09/21/2023 04:20 WG2134767
Di-n-butyl phthalate U 0.453 3.00 1 09/21/2023 04:20 WG2134767
Diethyl phthalate U 0.287 3.00 1 09/21/2023 04:20 WG2134767
Dimethyl phthalate U 0.260 3.00 1 09/21/2023 04:20 WG2134767
Di-n-octyl phthalate U 0.932 3.00 1 09/21/2023 04:20 WG2134767
Pyrene U 0.107 1.00 1 09/21/2023 04:20 WG2134767
1,2,4-Trichlorobenzene U 0.0698 10.0 1 09/21/2023 04:20 WG2134767
4-Chloro-3-methylphenol U 0.131 10.0 1 09/21/2023 04:20 WG2134767
2-Chlorophenol U 0.133 10.0 1 09/21/2023 04:20 WG2134767
2,4-Dichlorophenol U 0.102 10.0 1 09/21/2023 04:20 WG2134767
2,4-Dimethylphenol U 0.0636 10.0 1 09/21/2023 04:20 WG2134767
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 09/21/2023 04:20 WG2134767
2,4-Dinitrophenol U 5.93 10.0 1 09/21/2023 04:20 WG2134767
2-Nitrophenol U 0.117 10.0 1 09/21/2023 04:20 WG2134767
4-Nitrophenol U J4 0.143 10.0 1 09/21/2023 04:20 WG2134767
Pentachlorophenol U 0.313 10.0 1 09/21/2023 04:20 WG2134767
Phenol U 4.33 10.0 1 09/21/2023 04:20 WG2134767
2,4,6-Trichlorophenol U 0.100 10.0 1 09/21/2023 04:20 WG2134767
(S) Nitrobenzene-d5 46.3 15.0-314 09/21/2023 04:20 WG2134767
(S) 2-Fluorobiphenyl 47.5 22.0-127 09/21/2023 04:20 WG2134767
(S) p-Terphenyl-d14 56.1 29.0-141 09/21/2023 04:20 WG2134767
(S) Phenol-d5 14.5 8.00-424 09/21/2023 04:20 WG2134767
(S) 2-Fluorophenol 20.1 10.0-120 09/21/2023 04:20 WG2134767
(S) 2,4,6-Tribromophenol 40.7 10.0-153 09/21/2023 04:20 WG2134767
Sample Narrative:
L1655691-12 WG2134767: Duplicate Analysis performed due to QC failure. Reporting most compliant data.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 42 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 42 of 78
SAMPLE RESULTS - 13
L1655691
MW-6D
Collected date/time: 09/13/23 10:50
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.0941 1.00 1 09/21/2023 23:25 WG2136913
Bromobenzene U 0.118 1.00 1 09/21/2023 23:25 WG2136913
Bromodichloromethane U 0.136 1.00 1 09/21/2023 23:25 WG2136913
Bromochloromethane U 0.128 1.00 1 09/21/2023 23:25 WG2136913
Bromoform U 0.129 1.00 1 09/21/2023 23:25 WG2136913
Bromomethane U 0.605 5.00 1 09/22/2023 15:19 WG2137497
n-Butylbenzene U 0.157 1.00 1 09/21/2023 23:25 WG2136913
sec-Butylbenzene U 0.125 1.00 1 09/21/2023 23:25 WG2136913
tert-Butylbenzene U 0.127 1.00 1 09/21/2023 23:25 WG2136913
Carbon tetrachloride U 0.128 1.00 1 09/21/2023 23:25 WG2136913
Chlorobenzene U 0.116 1.00 1 09/21/2023 23:25 WG2136913
Chlorodibromomethane U 0.140 1.00 1 09/21/2023 23:25 WG2136913
Chloroethane U 0.192 5.00 1 09/21/2023 23:25 WG2136913
Chloroform U 0.111 5.00 1 09/21/2023 23:25 WG2136913
Chloromethane U 0.960 2.50 1 09/21/2023 23:25 WG2136913
2-Chlorotoluene U 0.106 1.00 1 09/21/2023 23:25 WG2136913
4-Chlorotoluene U 0.114 1.00 1 09/21/2023 23:25 WG2136913
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 09/21/2023 23:25 WG2136913
1,2-Dibromoethane U 0.126 1.00 1 09/21/2023 23:25 WG2136913
Dibromomethane U 0.122 1.00 1 09/21/2023 23:25 WG2136913
1,2-Dichlorobenzene U 0.107 1.00 1 09/21/2023 23:25 WG2136913
1,3-Dichlorobenzene U 0.110 1.00 1 09/21/2023 23:25 WG2136913
1,4-Dichlorobenzene U 0.120 1.00 1 09/21/2023 23:25 WG2136913
Dichlorodifluoromethane U 0.374 5.00 1 09/21/2023 23:25 WG2136913
1,1-Dichloroethane U 0.100 1.00 1 09/21/2023 23:25 WG2136913
1,2-Dichloroethane U 0.0819 1.00 1 09/21/2023 23:25 WG2136913
1,1-Dichloroethene U 0.188 1.00 1 09/21/2023 23:25 WG2136913
cis-1,2-Dichloroethene U 0.126 1.00 1 09/21/2023 23:25 WG2136913
trans-1,2-Dichloroethene U 0.149 1.00 1 09/21/2023 23:25 WG2136913
1,2-Dichloropropane U 0.149 1.00 1 09/21/2023 23:25 WG2136913
1,1-Dichloropropene U 0.142 1.00 1 09/21/2023 23:25 WG2136913
1,3-Dichloropropane U 0.110 1.00 1 09/21/2023 23:25 WG2136913
cis-1,3-Dichloropropene U 0.111 1.00 1 09/21/2023 23:25 WG2136913
trans-1,3-Dichloropropene U 0.118 1.00 1 09/21/2023 23:25 WG2136913
2,2-Dichloropropane U 0.161 1.00 1 09/21/2023 23:25 WG2136913
Di-isopropyl ether U 0.105 1.00 1 09/21/2023 23:25 WG2136913
Ethylbenzene U 0.137 1.00 1 09/21/2023 23:25 WG2136913
Hexachloro-1,3-butadiene U 0.337 1.00 1 09/21/2023 23:25 WG2136913
Isopropylbenzene U 0.105 1.00 1 09/21/2023 23:25 WG2136913
Methylene Chloride U 0.430 5.00 1 09/21/2023 23:25 WG2136913
Methyl tert-butyl ether U 0.101 1.00 1 09/21/2023 23:25 WG2136913
Naphthalene U 1.00 5.00 1 09/21/2023 23:25 WG2136913
n-Propylbenzene U 0.0993 1.00 1 09/21/2023 23:25 WG2136913
Styrene U 0.118 1.00 1 09/21/2023 23:25 WG2136913
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 09/21/2023 23:25 WG2136913
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 09/21/2023 23:25 WG2136913
Tetrachloroethene U 0.300 1.00 1 09/21/2023 23:25 WG2136913
Toluene U 0.278 1.00 1 09/21/2023 23:25 WG2136913
1,2,3-Trichlorobenzene U 0.230 1.00 1 09/21/2023 23:25 WG2136913
1,2,4-Trichlorobenzene U 0.481 1.00 1 09/21/2023 23:25 WG2136913
1,1,1-Trichloroethane U 0.149 1.00 1 09/21/2023 23:25 WG2136913
1,1,2-Trichloroethane U 0.158 1.00 1 09/21/2023 23:25 WG2136913
Trichloroethene U 0.190 1.00 1 09/21/2023 23:25 WG2136913
Trichlorofluoromethane U 0.160 5.00 1 09/22/2023 15:19 WG2137497
1,2,3-Trichloropropane U 0.237 2.50 1 09/21/2023 23:25 WG2136913
1,2,4-Trimethylbenzene U 0.322 1.00 1 09/21/2023 23:25 WG2136913
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 43 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 43 of 78
SAMPLE RESULTS - 13
L1655691
MW-6D
Collected date/time: 09/13/23 10:50
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene U 0.104 1.00 1 09/21/2023 23:25 WG2136913
Vinyl chloride U 0.234 1.00 1 09/21/2023 23:25 WG2136913
o-Xylene U 0.174 1.00 1 09/21/2023 23:25 WG2136913
m&p-Xylenes U 0.430 2.00 1 09/21/2023 23:25 WG2136913
ethanol U 42.0 100 1 09/21/2023 23:25 WG2136913
tert-Amyl Methyl Ether U 0.195 1.00 1 09/21/2023 23:25 WG2136913
Ethyl tert-butyl ether U 0.101 1.00 1 09/21/2023 23:25 WG2136913
tert-Butyl alcohol U 4.06 5.00 1 09/21/2023 23:25 WG2136913
t-Amyl Alcohol U 4.90 50.0 1 09/21/2023 23:25 WG2136913
tert-Butyl formate U J4 4.51 20.0 1 09/21/2023 23:25 WG2136913
(S) Toluene-d8 101 80.0-120 09/21/2023 23:25 WG2136913
(S) Toluene-d8 103 80.0-120 09/22/2023 15:19 WG2137497
(S) 4-Bromofluorobenzene 93.4 77.0-126 09/21/2023 23:25 WG2136913
(S) 4-Bromofluorobenzene 101 77.0-126 09/22/2023 15:19 WG2137497
(S) 1,2-Dichloroethane-d4 102 70.0-130 09/21/2023 23:25 WG2136913
(S) 1,2-Dichloroethane-d4 102 70.0-130 09/22/2023 15:19 WG2137497
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 35.7 B J 33.3 100 1 09/21/2023 07:37 WG2135760
Unadjusted C19-C36 Aliphatics 59.0 B J 33.3 100 1 09/21/2023 07:37 WG2135760
Unadjusted C11-C22 Aromatics 43.2 B J 33.3 100 1 09/21/2023 13:11 WG2135760
Unadjusted Total Petroleum
Hydrocarbons 138 33.3 100 1 09/21/2023 13:11 WG2135760
(S) o-Terphenyl 85.8 40.0-140 09/21/2023 13:11 WG2135760
(S) 1-Chloro-octadecane 89.1 40.0-140 09/21/2023 07:37 WG2135760
(S) 2-Fluorobiphenyl 92.2 40.0-140 09/21/2023 13:11 WG2135760
(S) 2-Bromonaphthalene 90.7 40.0-140 09/21/2023 13:11 WG2135760
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 09/21/2023 04:42 WG2134767
Acenaphthylene U 0.0921 1.00 1 09/21/2023 04:42 WG2134767
Anthracene U 0.0804 1.00 1 09/21/2023 04:42 WG2134767
Benzo(a)anthracene U 0.199 1.00 1 09/21/2023 04:42 WG2134767
Benzo(b)fluoranthene U 0.130 1.00 1 09/21/2023 04:42 WG2134767
Benzo(k)fluoranthene U 0.120 1.00 1 09/21/2023 04:42 WG2134767
Benzo(g,h,i)perylene U 0.121 1.00 1 09/21/2023 04:42 WG2134767
Benzo(a)pyrene U 0.0381 1.00 1 09/21/2023 04:42 WG2134767
Bis(2-chlorethoxy)methane U 0.116 10.0 1 09/21/2023 04:42 WG2134767
Bis(2-chloroethyl)ether U 0.137 10.0 1 09/21/2023 04:42 WG2134767
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 09/21/2023 04:42 WG2134767
4-Bromophenyl-phenylether U J4 0.0877 10.0 1 09/21/2023 04:42 WG2134767
2-Chloronaphthalene U J4 0.0648 1.00 1 09/21/2023 04:42 WG2134767
4-Chlorophenyl-phenylether U 0.0926 10.0 1 09/21/2023 04:42 WG2134767
Chrysene U 0.130 1.00 1 09/21/2023 04:42 WG2134767
Dibenz(a,h)anthracene U 0.0644 1.00 1 09/21/2023 04:42 WG2134767
3,3-Dichlorobenzidine U 0.212 10.0 1 09/21/2023 04:42 WG2134767
2,4-Dinitrotoluene U 0.0983 10.0 1 09/21/2023 04:42 WG2134767
2,6-Dinitrotoluene U 0.250 10.0 1 09/21/2023 04:42 WG2134767
Fluoranthene U 0.102 1.00 1 09/21/2023 04:42 WG2134767
Fluorene U J4 0.0844 1.00 1 09/21/2023 04:42 WG2134767
Hexachlorobenzene U 0.0755 1.00 1 09/21/2023 04:42 WG2134767
Hexachloro-1,3-butadiene U 0.0968 10.0 1 09/21/2023 04:42 WG2134767
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 44 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 44 of 78
SAMPLE RESULTS - 13
L1655691
MW-6D
Collected date/time: 09/13/23 10:50
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexachlorocyclopentadiene U 0.0598 10.0 1 09/21/2023 04:42 WG2134767
Hexachloroethane U 0.127 10.0 1 09/21/2023 04:42 WG2134767
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 09/21/2023 04:42 WG2134767
Isophorone U 0.143 10.0 1 09/21/2023 04:42 WG2134767
Naphthalene U 0.159 1.00 1 09/21/2023 04:42 WG2134767
Nitrobenzene U 0.297 10.0 1 09/21/2023 04:42 WG2134767
n-Nitrosodimethylamine U 0.998 10.0 1 09/21/2023 04:42 WG2134767
n-Nitrosodiphenylamine U 2.37 10.0 1 09/21/2023 04:42 WG2134767
n-Nitrosodi-n-propylamine U 0.261 10.0 1 09/21/2023 04:42 WG2134767
Phenanthrene U J4 0.112 1.00 1 09/21/2023 04:42 WG2134767
Benzylbutyl phthalate U 0.765 3.00 1 09/21/2023 04:42 WG2134767
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 09/21/2023 04:42 WG2134767
Di-n-butyl phthalate U 0.453 3.00 1 09/21/2023 04:42 WG2134767
Diethyl phthalate U 0.287 3.00 1 09/21/2023 04:42 WG2134767
Dimethyl phthalate U 0.260 3.00 1 09/21/2023 04:42 WG2134767
Di-n-octyl phthalate U 0.932 3.00 1 09/21/2023 04:42 WG2134767
Pyrene U 0.107 1.00 1 09/21/2023 04:42 WG2134767
1,2,4-Trichlorobenzene U 0.0698 10.0 1 09/21/2023 04:42 WG2134767
4-Chloro-3-methylphenol U 0.131 10.0 1 09/21/2023 04:42 WG2134767
2-Chlorophenol U 0.133 10.0 1 09/21/2023 04:42 WG2134767
2,4-Dichlorophenol U 0.102 10.0 1 09/21/2023 04:42 WG2134767
2,4-Dimethylphenol U 0.0636 10.0 1 09/21/2023 04:42 WG2134767
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 09/21/2023 04:42 WG2134767
2,4-Dinitrophenol U 5.93 10.0 1 09/21/2023 04:42 WG2134767
2-Nitrophenol U 0.117 10.0 1 09/21/2023 04:42 WG2134767
4-Nitrophenol U J4 0.143 10.0 1 09/21/2023 04:42 WG2134767
Pentachlorophenol U 0.313 10.0 1 09/21/2023 04:42 WG2134767
Phenol U 4.33 10.0 1 09/21/2023 04:42 WG2134767
2,4,6-Trichlorophenol U 0.100 10.0 1 09/21/2023 04:42 WG2134767
(S) Nitrobenzene-d5 57.6 15.0-314 09/21/2023 04:42 WG2134767
(S) 2-Fluorobiphenyl 54.4 22.0-127 09/21/2023 04:42 WG2134767
(S) p-Terphenyl-d14 63.8 29.0-141 09/21/2023 04:42 WG2134767
(S) Phenol-d5 15.7 8.00-424 09/21/2023 04:42 WG2134767
(S) 2-Fluorophenol 20.9 10.0-120 09/21/2023 04:42 WG2134767
(S) 2,4,6-Tribromophenol 46.0 10.0-153 09/21/2023 04:42 WG2134767
Sample Narrative:
L1655691-13 WG2134767: Duplicate Analysis performed due to QC failure. Reporting most compliant data.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 45 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 45 of 78
QUALITY CONTROL SUMMARYWG2135178
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1655691-01,03,04,05,06,07
Method Blank (MB)
(MB) R3975844-3 09/20/23 21:36
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Bromomethane U 0.605 5.00
Trichlorofluoromethane U 0.160 5.00
(S) Toluene-d8 102 80.0-120
(S) 4-Bromofluorobenzene 104 77.0-126
(S) 1,2-Dichloroethane-d4 83.8 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3975844-1 09/20/23 19:16 • (LCSD) R3975844-2 09/20/23 19:37
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Bromomethane 5.00 3.42 3.73 68.4 74.6 10.0-160 8.67 25
Trichlorofluoromethane 5.00 5.59 5.44 112 109 59.0-147 2.72 20
(S) Toluene-d8 101 99.7 80.0-120
(S) 4-Bromofluorobenzene 102 104 77.0-126
(S) 1,2-Dichloroethane-d4 83.6 83.4 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 46 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 46 of 78
QUALITY CONTROL SUMMARYWG2135339
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1655691-01,03,04,05,06,07
Method Blank (MB)
(MB) R3975345-4 09/20/23 01:39
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Benzene U 0.0941 1.00
Bromobenzene U 0.118 1.00
Bromodichloromethane U 0.136 1.00
Bromochloromethane U 0.128 1.00
Bromoform U 0.129 1.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
cis-1,3-Dichloropropene U 0.111 1.00
trans-1,3-Dichloropropene U 0.118 1.00
2,2-Dichloropropane U 0.161 1.00
Di-isopropyl ether U 0.105 1.00
Ethylbenzene U 0.137 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
Isopropylbenzene U 0.105 1.00
Methylene Chloride U 0.430 5.00
Methyl tert-butyl ether U 0.101 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 47 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 47 of 78
QUALITY CONTROL SUMMARYWG2135339
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1655691-01,03,04,05,06,07
Method Blank (MB)
(MB) R3975345-4 09/20/23 01:39
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.0993 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,4-Trimethylbenzene U 0.322 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
Vinyl chloride U 0.234 1.00
o-Xylene U 0.174 1.00
m&p-Xylenes U 0.430 2.00
ethanol U 42.0 100
tert-Amyl Methyl Ether U 0.195 1.00
Ethyl tert-butyl ether U 0.101 1.00
tert-Butyl alcohol U 4.06 5.00
t-Amyl Alcohol U 4.90 50.0
tert-Butyl formate U 4.51 20.0
(S) Toluene-d8 95.5 80.0-120
(S) 4-Bromofluorobenzene 93.6 77.0-126
(S) 1,2-Dichloroethane-d4 100 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3975345-1 09/19/23 23:27 • (LCSD) R3975345-2 09/19/23 23:50
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Benzene 5.00 5.28 4.89 106 97.8 70.0-123 7.67 20
Bromobenzene 5.00 5.14 4.93 103 98.6 73.0-121 4.17 20
Bromodichloromethane 5.00 5.00 4.71 100 94.2 75.0-120 5.97 20
Bromochloromethane 5.00 5.64 5.50 113 110 76.0-122 2.51 20
Bromoform 5.00 4.00 3.91 80.0 78.2 68.0-132 2.28 20
n-Butylbenzene 5.00 5.09 4.76 102 95.2 73.0-125 6.70 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 48 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 48 of 78
QUALITY CONTROL SUMMARYWG2135339
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1655691-01,03,04,05,06,07
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3975345-1 09/19/23 23:27 • (LCSD) R3975345-2 09/19/23 23:50
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
sec-Butylbenzene 5.00 5.29 5.08 106 102 75.0-125 4.05 20
tert-Butylbenzene 5.00 5.29 4.98 106 99.6 76.0-124 6.04 20
Carbon tetrachloride 5.00 5.71 5.39 114 108 68.0-126 5.77 20
Chlorobenzene 5.00 5.23 4.92 105 98.4 80.0-121 6.11 20
Chlorodibromomethane 5.00 4.77 4.58 95.4 91.6 77.0-125 4.06 20
Chloroethane 5.00 5.69 5.16 114 103 47.0-150 9.77 20
Chloroform 5.00 5.30 4.87 106 97.4 73.0-120 8.46 20
Chloromethane 5.00 4.21 4.28 84.2 85.6 41.0-142 1.65 20
2-Chlorotoluene 5.00 5.15 5.02 103 100 76.0-123 2.56 20
4-Chlorotoluene 5.00 5.21 4.91 104 98.2 75.0-122 5.93 20
1,2-Dibromo-3-Chloropropane 5.00 4.36 3.92 87.2 78.4 58.0-134 10.6 20
1,2-Dibromoethane 5.00 5.24 4.80 105 96.0 80.0-122 8.76 20
Dibromomethane 5.00 5.52 4.99 110 99.8 80.0-120 10.1 20
1,2-Dichlorobenzene 5.00 5.11 4.80 102 96.0 79.0-121 6.26 20
1,3-Dichlorobenzene 5.00 4.97 4.93 99.4 98.6 79.0-120 0.808 20
1,4-Dichlorobenzene 5.00 4.84 4.93 96.8 98.6 79.0-120 1.84 20
Dichlorodifluoromethane 5.00 4.65 4.01 93.0 80.2 51.0-149 14.8 20
1,1-Dichloroethane 5.00 5.35 4.97 107 99.4 70.0-126 7.36 20
1,2-Dichloroethane 5.00 5.59 5.11 112 102 70.0-128 8.97 20
1,1-Dichloroethene 5.00 5.40 5.10 108 102 71.0-124 5.71 20
cis-1,2-Dichloroethene 5.00 5.06 4.66 101 93.2 73.0-120 8.23 20
trans-1,2-Dichloroethene 5.00 5.05 5.23 101 105 73.0-120 3.50 20
1,2-Dichloropropane 5.00 5.17 4.90 103 98.0 77.0-125 5.36 20
1,1-Dichloropropene 5.00 5.57 5.17 111 103 74.0-126 7.45 20
1,3-Dichloropropane 5.00 5.24 4.90 105 98.0 80.0-120 6.71 20
cis-1,3-Dichloropropene 5.00 4.99 4.81 99.8 96.2 80.0-123 3.67 20
trans-1,3-Dichloropropene 5.00 5.20 5.03 104 101 78.0-124 3.32 20
2,2-Dichloropropane 5.00 5.50 5.20 110 104 58.0-130 5.61 20
Di-isopropyl ether 5.00 5.36 5.09 107 102 58.0-138 5.17 20
Ethylbenzene 5.00 5.17 4.83 103 96.6 79.0-123 6.80 20
Hexachloro-1,3-butadiene 5.00 4.96 4.74 99.2 94.8 54.0-138 4.54 20
Isopropylbenzene 5.00 4.99 4.73 99.8 94.6 76.0-127 5.35 20
Methylene Chloride 5.00 5.16 4.72 103 94.4 67.0-120 8.91 20
Methyl tert-butyl ether 5.00 5.63 5.28 113 106 68.0-125 6.42 20
Naphthalene 5.00 4.67 4.65 93.4 93.0 54.0-135 0.429 20
n-Propylbenzene 5.00 5.13 4.97 103 99.4 77.0-124 3.17 20
Styrene 5.00 4.58 4.38 91.6 87.6 73.0-130 4.46 20
1,1,1,2-Tetrachloroethane 5.00 5.15 4.98 103 99.6 75.0-125 3.36 20
1,1,2,2-Tetrachloroethane 5.00 4.20 4.35 84.0 87.0 65.0-130 3.51 20
Tetrachloroethene 5.00 5.62 5.14 112 103 72.0-132 8.92 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 49 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 49 of 78
QUALITY CONTROL SUMMARYWG2135339
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1655691-01,03,04,05,06,07
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3975345-1 09/19/23 23:27 • (LCSD) R3975345-2 09/19/23 23:50
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Toluene 5.00 5.12 4.83 102 96.6 79.0-120 5.83 20
1,2,3-Trichlorobenzene 5.00 4.89 4.80 97.8 96.0 50.0-138 1.86 20
1,2,4-Trichlorobenzene 5.00 4.85 4.87 97.0 97.4 57.0-137 0.412 20
1,1,1-Trichloroethane 5.00 5.61 5.15 112 103 73.0-124 8.55 20
1,1,2-Trichloroethane 5.00 5.30 5.03 106 101 80.0-120 5.23 20
Trichloroethene 5.00 5.90 5.54 118 111 78.0-124 6.29 20
1,2,3-Trichloropropane 5.00 5.09 5.17 102 103 73.0-130 1.56 20
1,2,4-Trimethylbenzene 5.00 4.91 4.79 98.2 95.8 76.0-121 2.47 20
1,3,5-Trimethylbenzene 5.00 5.00 4.78 100 95.6 76.0-122 4.50 20
Vinyl chloride 5.00 5.17 4.92 103 98.4 67.0-131 4.96 20
o-Xylene 5.00 4.88 4.76 97.6 95.2 80.0-122 2.49 20
m&p-Xylenes 10.0 10.3 9.73 103 97.3 80.0-122 5.69 20
ethanol 250 291 271 116 108 10.0-160 7.12 30
tert-Amyl Methyl Ether 5.00 5.59 5.30 112 106 66.0-125 5.33 20
Ethyl tert-butyl ether 5.00 5.60 5.31 112 106 63.0-138 5.32 20
tert-Butyl alcohol 25.0 28.6 26.6 114 106 27.0-160 7.25 30
(S) Toluene-d8 97.6 96.7 80.0-120
(S) 4-Bromofluorobenzene 90.9 91.0 77.0-126
(S) 1,2-Dichloroethane-d4 99.4 96.9 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3975345-3 09/20/23 00:55
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
tert-Butyl formate 100 156 156 10.0-160
(S) Toluene-d8 97.6 80.0-120
(S) 4-Bromofluorobenzene 94.6 77.0-126
(S) 1,2-Dichloroethane-d4 93.0 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 50 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 50 of 78
QUALITY CONTROL SUMMARYWG2135999
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1655691-08
Method Blank (MB)
(MB) R3976355-4 09/21/23 14:33
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Benzene U 0.0941 1.00
Bromobenzene U 0.118 1.00
Bromodichloromethane U 0.136 1.00
Bromochloromethane U 0.128 1.00
Bromoform U 0.129 1.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
cis-1,3-Dichloropropene U 0.111 1.00
trans-1,3-Dichloropropene U 0.118 1.00
2,2-Dichloropropane U 0.161 1.00
Di-isopropyl ether U 0.105 1.00
Ethylbenzene U 0.137 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
Isopropylbenzene U 0.105 1.00
Methylene Chloride U 0.430 5.00
Methyl tert-butyl ether U 0.101 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 51 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 51 of 78
QUALITY CONTROL SUMMARYWG2135999
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1655691-08
Method Blank (MB)
(MB) R3976355-4 09/21/23 14:33
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.0993 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,4-Trimethylbenzene U 0.322 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
Vinyl chloride U 0.234 1.00
o-Xylene U 0.174 1.00
m&p-Xylenes U 0.430 2.00
ethanol U 42.0 100
tert-Amyl Methyl Ether U 0.195 1.00
Ethyl tert-butyl ether U 0.101 1.00
tert-Butyl alcohol U 4.06 5.00
t-Amyl Alcohol U 4.90 50.0
tert-Butyl formate U 4.51 20.0
(S) Toluene-d8 98.8 80.0-120
(S) 4-Bromofluorobenzene 90.6 77.0-126
(S) 1,2-Dichloroethane-d4 100 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3976355-1 09/21/23 12:52 • (LCSD) R3976355-2 09/21/23 13:14
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Benzene 5.00 5.36 5.33 107 107 70.0-123 0.561 20
Bromobenzene 5.00 5.07 5.21 101 104 73.0-121 2.72 20
Bromodichloromethane 5.00 5.12 5.31 102 106 75.0-120 3.64 20
Bromochloromethane 5.00 5.89 5.90 118 118 76.0-122 0.170 20
Bromoform 5.00 4.69 4.78 93.8 95.6 68.0-132 1.90 20
n-Butylbenzene 5.00 4.96 5.24 99.2 105 73.0-125 5.49 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 52 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 52 of 78
QUALITY CONTROL SUMMARYWG2135999
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1655691-08
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3976355-1 09/21/23 12:52 • (LCSD) R3976355-2 09/21/23 13:14
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
sec-Butylbenzene 5.00 5.26 5.18 105 104 75.0-125 1.53 20
tert-Butylbenzene 5.00 5.24 5.29 105 106 76.0-124 0.950 20
Carbon tetrachloride 5.00 5.78 5.94 116 119 68.0-126 2.73 20
Chlorobenzene 5.00 5.28 5.39 106 108 80.0-121 2.06 20
Chlorodibromomethane 5.00 5.20 5.15 104 103 77.0-125 0.966 20
Chloroethane 5.00 5.68 6.09 114 122 47.0-150 6.97 20
Chloroform 5.00 5.46 5.55 109 111 73.0-120 1.63 20
Chloromethane 5.00 4.60 4.81 92.0 96.2 41.0-142 4.46 20
2-Chlorotoluene 5.00 5.28 5.29 106 106 76.0-123 0.189 20
4-Chlorotoluene 5.00 5.10 5.29 102 106 75.0-122 3.66 20
1,2-Dibromo-3-Chloropropane 5.00 4.39 4.48 87.8 89.6 58.0-134 2.03 20
1,2-Dibromoethane 5.00 5.27 5.46 105 109 80.0-122 3.54 20
Dibromomethane 5.00 5.39 5.39 108 108 80.0-120 0.000 20
1,2-Dichlorobenzene 5.00 5.10 5.28 102 106 79.0-121 3.47 20
1,3-Dichlorobenzene 5.00 5.15 5.17 103 103 79.0-120 0.388 20
1,4-Dichlorobenzene 5.00 5.20 5.30 104 106 79.0-120 1.90 20
Dichlorodifluoromethane 5.00 5.10 4.92 102 98.4 51.0-149 3.59 20
1,1-Dichloroethane 5.00 5.59 5.51 112 110 70.0-126 1.44 20
1,2-Dichloroethane 5.00 5.65 5.60 113 112 70.0-128 0.889 20
1,1-Dichloroethene 5.00 5.48 5.48 110 110 71.0-124 0.000 20
cis-1,2-Dichloroethene 5.00 5.30 5.29 106 106 73.0-120 0.189 20
trans-1,2-Dichloroethene 5.00 5.58 5.30 112 106 73.0-120 5.15 20
1,2-Dichloropropane 5.00 5.30 5.14 106 103 77.0-125 3.07 20
1,1-Dichloropropene 5.00 5.62 5.74 112 115 74.0-126 2.11 20
1,3-Dichloropropane 5.00 5.44 5.45 109 109 80.0-120 0.184 20
cis-1,3-Dichloropropene 5.00 4.95 5.01 99.0 100 80.0-123 1.20 20
trans-1,3-Dichloropropene 5.00 5.24 5.25 105 105 78.0-124 0.191 20
2,2-Dichloropropane 5.00 4.63 4.58 92.6 91.6 58.0-130 1.09 20
Di-isopropyl ether 5.00 5.65 5.76 113 115 58.0-138 1.93 20
Ethylbenzene 5.00 5.29 5.16 106 103 79.0-123 2.49 20
Hexachloro-1,3-butadiene 5.00 4.42 4.55 88.4 91.0 54.0-138 2.90 20
Isopropylbenzene 5.00 5.05 5.07 101 101 76.0-127 0.395 20
Methylene Chloride 5.00 5.48 5.05 110 101 67.0-120 8.17 20
Methyl tert-butyl ether 5.00 5.78 5.85 116 117 68.0-125 1.20 20
Naphthalene 5.00 4.77 4.83 95.4 96.6 54.0-135 1.25 20
n-Propylbenzene 5.00 5.13 5.18 103 104 77.0-124 0.970 20
Styrene 5.00 4.72 4.63 94.4 92.6 73.0-130 1.93 20
1,1,1,2-Tetrachloroethane 5.00 5.26 5.31 105 106 75.0-125 0.946 20
1,1,2,2-Tetrachloroethane 5.00 4.69 4.48 93.8 89.6 65.0-130 4.58 20
Tetrachloroethene 5.00 5.71 5.46 114 109 72.0-132 4.48 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 53 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 53 of 78
QUALITY CONTROL SUMMARYWG2135999
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1655691-08
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3976355-1 09/21/23 12:52 • (LCSD) R3976355-2 09/21/23 13:14
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Toluene 5.00 5.19 5.17 104 103 79.0-120 0.386 20
1,2,3-Trichlorobenzene 5.00 4.95 4.96 99.0 99.2 50.0-138 0.202 20
1,2,4-Trichlorobenzene 5.00 4.81 4.84 96.2 96.8 57.0-137 0.622 20
1,1,1-Trichloroethane 5.00 5.67 5.80 113 116 73.0-124 2.27 20
1,1,2-Trichloroethane 5.00 5.65 5.52 113 110 80.0-120 2.33 20
Trichloroethene 5.00 5.83 6.17 117 123 78.0-124 5.67 20
1,2,3-Trichloropropane 5.00 5.43 5.56 109 111 73.0-130 2.37 20
1,2,4-Trimethylbenzene 5.00 4.98 5.02 99.6 100 76.0-121 0.800 20
1,3,5-Trimethylbenzene 5.00 5.05 5.02 101 100 76.0-122 0.596 20
Vinyl chloride 5.00 5.61 5.63 112 113 67.0-131 0.356 20
o-Xylene 5.00 4.94 5.02 98.8 100 80.0-122 1.61 20
m&p-Xylenes 10.0 10.4 10.5 104 105 80.0-122 0.957 20
ethanol 250 275 314 110 126 10.0-160 13.2 30
tert-Amyl Methyl Ether 5.00 5.87 5.87 117 117 66.0-125 0.000 20
Ethyl tert-butyl ether 5.00 5.82 5.88 116 118 63.0-138 1.03 20
tert-Butyl alcohol 25.0 28.4 29.6 114 118 27.0-160 4.14 30
(S) Toluene-d8 97.5 96.2 80.0-120
(S) 4-Bromofluorobenzene 94.3 90.2 77.0-126
(S) 1,2-Dichloroethane-d4 101 101 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3976355-3 09/21/23 13:35
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
tert-Butyl formate 100 163 163 10.0-160 J4
(S) Toluene-d8 99.1 80.0-120
(S) 4-Bromofluorobenzene 94.0 77.0-126
(S) 1,2-Dichloroethane-d4 99.1 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 54 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 54 of 78
QUALITY CONTROL SUMMARYWG2136913
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1655691-02,09,10,11,12,13
Method Blank (MB)
(MB) R3976357-4 09/21/23 14:33
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Benzene U 0.0941 1.00
Bromobenzene U 0.118 1.00
Bromodichloromethane U 0.136 1.00
Bromochloromethane U 0.128 1.00
Bromoform U 0.129 1.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
cis-1,3-Dichloropropene U 0.111 1.00
trans-1,3-Dichloropropene U 0.118 1.00
2,2-Dichloropropane U 0.161 1.00
Di-isopropyl ether U 0.105 1.00
Ethylbenzene U 0.137 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
Isopropylbenzene U 0.105 1.00
Methylene Chloride U 0.430 5.00
Methyl tert-butyl ether U 0.101 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 55 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 55 of 78
QUALITY CONTROL SUMMARYWG2136913
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1655691-02,09,10,11,12,13
Method Blank (MB)
(MB) R3976357-4 09/21/23 14:33
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.0993 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,4-Trimethylbenzene U 0.322 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
Vinyl chloride U 0.234 1.00
o-Xylene U 0.174 1.00
m&p-Xylenes U 0.430 2.00
ethanol U 42.0 100
tert-Amyl Methyl Ether U 0.195 1.00
Ethyl tert-butyl ether U 0.101 1.00
tert-Butyl alcohol U 4.06 5.00
t-Amyl Alcohol U 4.90 50.0
tert-Butyl formate U 4.51 20.0
(S) Toluene-d8 98.8 80.0-120
(S) 4-Bromofluorobenzene 90.6 77.0-126
(S) 1,2-Dichloroethane-d4 100 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3976357-1 09/21/23 12:52 • (LCSD) R3976357-2 09/21/23 13:14
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Benzene 5.00 5.36 5.33 107 107 70.0-123 0.561 20
Bromobenzene 5.00 5.07 5.21 101 104 73.0-121 2.72 20
Bromodichloromethane 5.00 5.12 5.31 102 106 75.0-120 3.64 20
Bromochloromethane 5.00 5.89 5.90 118 118 76.0-122 0.170 20
Bromoform 5.00 4.69 4.78 93.8 95.6 68.0-132 1.90 20
n-Butylbenzene 5.00 4.96 5.24 99.2 105 73.0-125 5.49 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 56 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 56 of 78
QUALITY CONTROL SUMMARYWG2136913
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1655691-02,09,10,11,12,13
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3976357-1 09/21/23 12:52 • (LCSD) R3976357-2 09/21/23 13:14
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
sec-Butylbenzene 5.00 5.26 5.18 105 104 75.0-125 1.53 20
tert-Butylbenzene 5.00 5.24 5.29 105 106 76.0-124 0.950 20
Carbon tetrachloride 5.00 5.78 5.94 116 119 68.0-126 2.73 20
Chlorobenzene 5.00 5.28 5.39 106 108 80.0-121 2.06 20
Chlorodibromomethane 5.00 5.20 5.15 104 103 77.0-125 0.966 20
Chloroethane 5.00 5.68 6.09 114 122 47.0-150 6.97 20
Chloroform 5.00 5.46 5.55 109 111 73.0-120 1.63 20
Chloromethane 5.00 4.60 4.81 92.0 96.2 41.0-142 4.46 20
2-Chlorotoluene 5.00 5.28 5.29 106 106 76.0-123 0.189 20
4-Chlorotoluene 5.00 5.10 5.29 102 106 75.0-122 3.66 20
1,2-Dibromo-3-Chloropropane 5.00 4.39 4.48 87.8 89.6 58.0-134 2.03 20
1,2-Dibromoethane 5.00 5.27 5.46 105 109 80.0-122 3.54 20
Dibromomethane 5.00 5.39 5.39 108 108 80.0-120 0.000 20
1,2-Dichlorobenzene 5.00 5.10 5.28 102 106 79.0-121 3.47 20
1,3-Dichlorobenzene 5.00 5.15 5.17 103 103 79.0-120 0.388 20
1,4-Dichlorobenzene 5.00 5.20 5.30 104 106 79.0-120 1.90 20
Dichlorodifluoromethane 5.00 5.10 4.92 102 98.4 51.0-149 3.59 20
1,1-Dichloroethane 5.00 5.59 5.51 112 110 70.0-126 1.44 20
1,2-Dichloroethane 5.00 5.65 5.60 113 112 70.0-128 0.889 20
1,1-Dichloroethene 5.00 5.48 5.48 110 110 71.0-124 0.000 20
cis-1,2-Dichloroethene 5.00 5.30 5.29 106 106 73.0-120 0.189 20
trans-1,2-Dichloroethene 5.00 5.58 5.30 112 106 73.0-120 5.15 20
1,2-Dichloropropane 5.00 5.30 5.14 106 103 77.0-125 3.07 20
1,1-Dichloropropene 5.00 5.62 5.74 112 115 74.0-126 2.11 20
1,3-Dichloropropane 5.00 5.44 5.45 109 109 80.0-120 0.184 20
cis-1,3-Dichloropropene 5.00 4.95 5.01 99.0 100 80.0-123 1.20 20
trans-1,3-Dichloropropene 5.00 5.24 5.25 105 105 78.0-124 0.191 20
2,2-Dichloropropane 5.00 4.63 4.58 92.6 91.6 58.0-130 1.09 20
Di-isopropyl ether 5.00 5.65 5.76 113 115 58.0-138 1.93 20
Ethylbenzene 5.00 5.29 5.16 106 103 79.0-123 2.49 20
Hexachloro-1,3-butadiene 5.00 4.42 4.55 88.4 91.0 54.0-138 2.90 20
Isopropylbenzene 5.00 5.05 5.07 101 101 76.0-127 0.395 20
Methylene Chloride 5.00 5.48 5.05 110 101 67.0-120 8.17 20
Methyl tert-butyl ether 5.00 5.78 5.85 116 117 68.0-125 1.20 20
Naphthalene 5.00 4.77 4.83 95.4 96.6 54.0-135 1.25 20
n-Propylbenzene 5.00 5.13 5.18 103 104 77.0-124 0.970 20
Styrene 5.00 4.72 4.63 94.4 92.6 73.0-130 1.93 20
1,1,1,2-Tetrachloroethane 5.00 5.26 5.31 105 106 75.0-125 0.946 20
1,1,2,2-Tetrachloroethane 5.00 4.69 4.48 93.8 89.6 65.0-130 4.58 20
Tetrachloroethene 5.00 5.71 5.46 114 109 72.0-132 4.48 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 57 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 57 of 78
QUALITY CONTROL SUMMARYWG2136913
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1655691-02,09,10,11,12,13
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3976357-1 09/21/23 12:52 • (LCSD) R3976357-2 09/21/23 13:14
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Toluene 5.00 5.19 5.17 104 103 79.0-120 0.386 20
1,2,3-Trichlorobenzene 5.00 4.95 4.96 99.0 99.2 50.0-138 0.202 20
1,2,4-Trichlorobenzene 5.00 4.81 4.84 96.2 96.8 57.0-137 0.622 20
1,1,1-Trichloroethane 5.00 5.67 5.80 113 116 73.0-124 2.27 20
1,1,2-Trichloroethane 5.00 5.65 5.52 113 110 80.0-120 2.33 20
Trichloroethene 5.00 5.83 6.17 117 123 78.0-124 5.67 20
1,2,3-Trichloropropane 5.00 5.43 5.56 109 111 73.0-130 2.37 20
1,2,4-Trimethylbenzene 5.00 4.98 5.02 99.6 100 76.0-121 0.800 20
1,3,5-Trimethylbenzene 5.00 5.05 5.02 101 100 76.0-122 0.596 20
Vinyl chloride 5.00 5.61 5.63 112 113 67.0-131 0.356 20
o-Xylene 5.00 4.94 5.02 98.8 100 80.0-122 1.61 20
m&p-Xylenes 10.0 10.4 10.5 104 105 80.0-122 0.957 20
ethanol 250 275 314 110 126 10.0-160 13.2 30
tert-Amyl Methyl Ether 5.00 5.87 5.87 117 117 66.0-125 0.000 20
Ethyl tert-butyl ether 5.00 5.82 5.88 116 118 63.0-138 1.03 20
tert-Butyl alcohol 25.0 28.4 29.6 114 118 27.0-160 4.14 30
(S) Toluene-d8 97.5 96.2 80.0-120
(S) 4-Bromofluorobenzene 94.3 90.2 77.0-126
(S) 1,2-Dichloroethane-d4 101 101 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3976357-3 09/21/23 13:35
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
tert-Butyl formate 100 163 163 10.0-160 J4
(S) Toluene-d8 99.1 80.0-120
(S) 4-Bromofluorobenzene 94.0 77.0-126
(S) 1,2-Dichloroethane-d4 99.1 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 58 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 58 of 78
QUALITY CONTROL SUMMARYWG2137490
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1655691-08
Method Blank (MB)
(MB) R3976971-3 09/22/23 11:08
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Bromomethane U 0.605 5.00
Trichlorofluoromethane U 0.160 5.00
(S) Toluene-d8 105 80.0-120
(S) 4-Bromofluorobenzene 103 77.0-126
(S) 1,2-Dichloroethane-d4 102 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3976971-1 09/22/23 09:41 • (LCSD) R3976971-2 09/22/23 10:03
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Bromomethane 5.00 5.85 5.50 117 110 10.0-160 6.17 25
Trichlorofluoromethane 5.00 6.07 5.98 121 120 59.0-147 1.49 20
(S) Toluene-d8 105 104 80.0-120
(S) 4-Bromofluorobenzene 101 101 77.0-126
(S) 1,2-Dichloroethane-d4 105 107 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 59 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 59 of 78
QUALITY CONTROL SUMMARYWG2137497
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1655691-02,09,10,11,12,13
Method Blank (MB)
(MB) R3976972-3 09/22/23 11:08
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Bromomethane U 0.605 5.00
Ethylbenzene U 0.137 1.00
Naphthalene U 1.00 5.00
Toluene U 0.278 1.00
Trichlorofluoromethane U 0.160 5.00
o-Xylene U 0.174 1.00
m&p-Xylenes U 0.430 2.00
(S) Toluene-d8 105 80.0-120
(S) 4-Bromofluorobenzene 103 77.0-126
(S) 1,2-Dichloroethane-d4 102 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3976972-1 09/22/23 09:41 • (LCSD) R3976972-2 09/22/23 10:03
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Bromomethane 5.00 5.85 5.50 117 110 10.0-160 6.17 25
Ethylbenzene 5.00 5.40 5.28 108 106 79.0-123 2.25 20
Naphthalene 5.00 4.79 4.96 95.8 99.2 54.0-135 3.49 20
Toluene 5.00 5.42 5.21 108 104 79.0-120 3.95 20
Trichlorofluoromethane 5.00 6.07 5.98 121 120 59.0-147 1.49 20
o-Xylene 5.00 5.24 5.07 105 101 80.0-122 3.30 20
m&p-Xylenes 10.0 10.7 10.7 107 107 80.0-122 0.000 20
(S) Toluene-d8 105 104 80.0-120
(S) 4-Bromofluorobenzene 101 101 77.0-126
(S) 1,2-Dichloroethane-d4 105 107 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 60 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 60 of 78
QUALITY CONTROL SUMMARYWG2134808
TPH by Method MADEPE L1655691-01
Method Blank (MB)
(MB) R3975151-1 09/19/23 19:24
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics 43.6 J 33.3 100
(S) o-Terphenyl 66.1 40.0-140
(S) 2-Fluorobiphenyl 84.0 40.0-140
(S) 2-Bromonaphthalene 85.4 40.0-140
Method Blank (MB)
(MB) R3975151-4 09/19/23 20:48
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics U 33.3 100
Unadjusted C19-C36 Aliphatics U 33.3 100
(S) 1-Chloro-octadecane 53.5 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3975151-2 09/19/23 19:54 • (LCSD) R3975151-3 09/19/23 20:24
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1390 1350 81.8 79.4 40.0-140 2.92 25
(S) o-Terphenyl 73.5 72.0 40.0-140
(S) 2-Fluorobiphenyl 82.6 80.2 40.0-140
(S) 2-Bromonaphthalene 83.4 81.1 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3975151-5 09/19/23 21:12 • (LCSD) R3975151-6 09/19/23 21:43
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 368 361 61.3 60.2 40.0-140 1.92 25
Unadjusted C19-C36 Aliphatics 800 682 685 85.3 85.6 40.0-140 0.439 25
(S) 1-Chloro-octadecane 65.6 65.5 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 61 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 61 of 78
QUALITY CONTROL SUMMARYWG2135760
TPH by Method MADEPE L1655691-02,03,05,06,07,08,09,10,11,12,13
Method Blank (MB)
(MB) R3975701-1 09/20/23 19:31
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics 37.4 J 33.3 100
Unadjusted C19-C36 Aliphatics 67.9 J 33.3 100
(S) 1-Chloro-octadecane 101 40.0-140
Method Blank (MB)
(MB) R3975701-4 09/20/23 21:03
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics 51.6 J 33.3 100
(S) o-Terphenyl 95.8 40.0-140
(S) 2-Fluorobiphenyl 97.1 40.0-140
(S) 2-Bromonaphthalene 98.5 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3975701-2 09/20/23 19:55 • (LCSD) R3975701-3 09/20/23 20:41
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 472 451 78.7 75.2 40.0-140 4.55 25
Unadjusted C19-C36 Aliphatics 800 853 854 107 107 40.0-140 0.117 25
(S) 1-Chloro-octadecane 89.6 93.4 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3975701-5 09/20/23 21:25 • (LCSD) R3975701-6 09/20/23 21:48
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1800 1590 106 93.5 40.0-140 12.4 25
(S) o-Terphenyl 93.6 88.0 40.0-140
(S) 2-Fluorobiphenyl 104 101 40.0-140
(S) 2-Bromonaphthalene 106 103 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 62 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 62 of 78
QUALITY CONTROL SUMMARYWG2139497
TPH by Method MADEPE L1655691-04
Method Blank (MB)
(MB) R3978964-1 09/27/23 15:44
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics 63.0 J 33.3 100
Unadjusted C19-C36 Aliphatics 49.1 J 33.3 100
(S) 1-Chloro-octadecane 92.3 40.0-140
Method Blank (MB)
(MB) R3978964-4 09/27/23 16:51
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics 40.1 J 33.3 100
(S) o-Terphenyl 96.3 40.0-140
(S) 2-Fluorobiphenyl 99.5 40.0-140
(S) 2-Bromonaphthalene 99.1 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3978964-2 09/27/23 16:06 • (LCSD) R3978964-3 09/27/23 16:28
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 460 463 76.7 77.2 40.0-140 0.650 25
Unadjusted C19-C36 Aliphatics 800 825 865 103 108 40.0-140 4.73 25
(S) 1-Chloro-octadecane 91.9 96.0 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3978964-5 09/27/23 17:13 • (LCSD) R3978964-6 09/27/23 17:35
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1780 1790 105 105 40.0-140 0.560 25
(S) o-Terphenyl 95.3 96.9 40.0-140
(S) 2-Fluorobiphenyl 101 103 40.0-140
(S) 2-Bromonaphthalene 101 103 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 63 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 63 of 78
QUALITY CONTROL SUMMARYWG2139497
TPH by Method MADEPE L1655691-04
L1657797-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1657797-01 09/27/23 19:05 • (MS) R3978964-7 09/27/23 19:27 • (MSD) R3978964-8 09/27/23 19:49
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 570 54.5 452 477 69.7 69.0 1 40.0-140 5.38 50
Unadjusted C19-C36 Aliphatics 760 45.5 783 835 97.0 96.8 1 40.0-140 6.43 50
(S) 1-Chloro-octadecane 59.3 57.2 40.0-140
L1657797-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1657797-01 09/28/23 00:59 • (MS) R3978964-9 09/28/23 01:23 • (MSD) R3978964-10 09/28/23 01:45
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1620 U 1560 1870 96.3 108 1 40.0-140 18.1 50
(S) o-Terphenyl 76.2 78.8 40.0-140
(S) 2-Fluorobiphenyl 99.5 104 40.0-140
(S) 2-Bromonaphthalene 98.6 104 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 64 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 64 of 78
QUALITY CONTROL SUMMARYWG2132824
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1655691-01,02,03,04,05,06,07,08,09
Method Blank (MB)
(MB) R3974741-2 09/17/23 13:13
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.0886 1.00
Acenaphthylene U 0.0921 1.00
Anthracene U 0.0804 1.00
Benzo(a)anthracene U 0.199 1.00
Benzo(b)fluoranthene U 0.130 1.00
Benzo(k)fluoranthene U 0.120 1.00
Benzo(g,h,i)perylene U 0.121 1.00
Benzo(a)pyrene U 0.0381 1.00
Bis(2-chlorethoxy)methane U 0.116 10.0
Bis(2-chloroethyl)ether U 0.137 10.0
2,2-Oxybis(1-Chloropropane)U 0.210 10.0
4-Bromophenyl-phenylether U 0.0877 10.0
2-Chloronaphthalene U 0.0648 1.00
4-Chlorophenyl-phenylether U 0.0926 10.0
Chrysene U 0.130 1.00
Dibenz(a,h)anthracene U 0.0644 1.00
3,3-Dichlorobenzidine U 0.212 10.0
2,4-Dinitrotoluene U 0.0983 10.0
2,6-Dinitrotoluene U 0.250 10.0
Fluoranthene U 0.102 1.00
Fluorene U 0.0844 1.00
Hexachlorobenzene U 0.0755 1.00
Hexachloro-1,3-butadiene U 0.0968 10.0
Hexachlorocyclopentadiene U 0.0598 10.0
Hexachloroethane U 0.127 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.143 10.0
Naphthalene U 0.159 1.00
Nitrobenzene U 0.297 10.0
n-Nitrosodimethylamine U 0.998 10.0
n-Nitrosodiphenylamine U 2.37 10.0
n-Nitrosodi-n-propylamine U 0.261 10.0
Phenanthrene U 0.112 1.00
Benzylbutyl phthalate U 0.765 3.00
Bis(2-ethylhexyl)phthalate U 0.895 3.00
Di-n-butyl phthalate U 0.453 3.00
Diethyl phthalate U 0.287 3.00
Dimethyl phthalate U 0.260 3.00
Di-n-octyl phthalate U 0.932 3.00
Pyrene U 0.107 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 65 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 65 of 78
QUALITY CONTROL SUMMARYWG2132824
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1655691-01,02,03,04,05,06,07,08,09
Method Blank (MB)
(MB) R3974741-2 09/17/23 13:13
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
1,2,4-Trichlorobenzene U 0.0698 10.0
4-Chloro-3-methylphenol U 0.131 10.0
2-Chlorophenol U 0.133 10.0
2,4-Dichlorophenol U 0.102 10.0
2,4-Dimethylphenol U 0.0636 10.0
4,6-Dinitro-2-methylphenol U 1.12 10.0
2,4-Dinitrophenol U 5.93 10.0
2-Nitrophenol U 0.117 10.0
4-Nitrophenol U 0.143 10.0
Pentachlorophenol U 0.313 10.0
Phenol U 4.33 10.0
2,4,6-Trichlorophenol U 0.100 10.0
(S) Nitrobenzene-d5 55.6 15.0-314
(S) 2-Fluorobiphenyl 56.1 22.0-127
(S) p-Terphenyl-d14 65.5 29.0-141
(S) Phenol-d5 18.5 8.00-424
(S) 2-Fluorophenol 29.2 10.0-120
(S) 2,4,6-Tribromophenol 56.0 10.0-153
Laboratory Control Sample (LCS)
(LCS) R3974741-1 09/17/23 12:51
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acenaphthene 50.0 24.4 48.8 47.0-145
Acenaphthylene 50.0 24.6 49.2 33.0-145
Anthracene 50.0 26.9 53.8 27.0-133
Benzo(a)anthracene 50.0 27.7 55.4 33.0-143
Benzo(b)fluoranthene 50.0 30.0 60.0 24.0-159
Benzo(k)fluoranthene 50.0 30.3 60.6 11.0-162
Benzo(g,h,i)perylene 50.0 30.4 60.8 1.00-219
Benzo(a)pyrene 50.0 31.4 62.8 17.0-163
Bis(2-chlorethoxy)methane 50.0 22.1 44.2 1.00-219
Bis(2-chloroethyl)ether 50.0 23.3 46.6 33.0-185
2,2-Oxybis(1-Chloropropane)50.0 22.4 44.8 36.0-166
4-Bromophenyl-phenylether 50.0 24.3 48.6 53.0-127 J4
2-Chloronaphthalene 50.0 22.7 45.4 60.0-120 J4
4-Chlorophenyl-phenylether 50.0 25.8 51.6 25.0-158
Chrysene 50.0 27.4 54.8 17.0-168
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 66 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 66 of 78
QUALITY CONTROL SUMMARYWG2132824
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1655691-01,02,03,04,05,06,07,08,09
Laboratory Control Sample (LCS)
(LCS) R3974741-1 09/17/23 12:51
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Dibenz(a,h)anthracene 50.0 30.4 60.8 1.00-227
3,3-Dichlorobenzidine 100 59.6 59.6 1.00-262
2,4-Dinitrotoluene 50.0 32.4 64.8 39.0-139
2,6-Dinitrotoluene 50.0 27.4 54.8 50.0-158
Fluoranthene 50.0 27.7 55.4 26.0-137
Fluorene 50.0 25.7 51.4 59.0-121 J4
Hexachlorobenzene 50.0 23.5 47.0 1.00-152
Hexachloro-1,3-butadiene 50.0 21.2 42.4 24.0-120
Hexachlorocyclopentadiene 50.0 9.87 19.7 10.0-120
Hexachloroethane 50.0 21.3 42.6 40.0-120
Indeno(1,2,3-cd)pyrene 50.0 28.3 56.6 1.00-171
Isophorone 50.0 23.6 47.2 21.0-196
Naphthalene 50.0 20.9 41.8 21.0-133
Nitrobenzene 50.0 23.1 46.2 35.0-180
n-Nitrosodimethylamine 50.0 24.7 49.4 10.0-120
n-Nitrosodiphenylamine 50.0 25.9 51.8 44.0-120
n-Nitrosodi-n-propylamine 50.0 24.8 49.6 1.00-230
Phenanthrene 50.0 25.4 50.8 54.0-120 J4
Benzylbutyl phthalate 50.0 33.2 66.4 1.00-152
Bis(2-ethylhexyl)phthalate 50.0 33.3 66.6 8.00-158
Di-n-butyl phthalate 50.0 30.1 60.2 1.00-120
Diethyl phthalate 50.0 28.6 57.2 1.00-120
Dimethyl phthalate 50.0 27.3 54.6 1.00-120
Di-n-octyl phthalate 50.0 30.9 61.8 4.00-146
Pyrene 50.0 28.4 56.8 52.0-120
1,2,4-Trichlorobenzene 50.0 22.3 44.6 44.0-142
4-Chloro-3-methylphenol 50.0 20.2 40.4 22.0-147
2-Chlorophenol 50.0 18.7 37.4 23.0-134
2,4-Dichlorophenol 50.0 22.3 44.6 39.0-135
2,4-Dimethylphenol 50.0 22.3 44.6 32.0-120
4,6-Dinitro-2-methylphenol 50.0 29.5 59.0 1.00-181
2,4-Dinitrophenol 50.0 24.6 49.2 1.00-191
2-Nitrophenol 50.0 25.1 50.2 29.0-182
4-Nitrophenol 50.0 9.28 18.6 1.00-132
Pentachlorophenol 50.0 18.5 37.0 14.0-176
Phenol 50.0 9.70 19.4 5.00-120
2,4,6-Trichlorophenol 50.0 25.4 50.8 37.0-144
(S) Nitrobenzene-d5 47.9 15.0-314
(S) 2-Fluorobiphenyl 48.4 22.0-127
(S) p-Terphenyl-d14 55.1 29.0-141
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 67 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 67 of 78
QUALITY CONTROL SUMMARYWG2132824
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1655691-01,02,03,04,05,06,07,08,09
Laboratory Control Sample (LCS)
(LCS) R3974741-1 09/17/23 12:51
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
(S) Phenol-d5 17.8 8.00-424
(S) 2-Fluorophenol 24.7 10.0-120
(S) 2,4,6-Tribromophenol 50.5 10.0-153
L1655875-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1655875-01 09/17/23 19:21 • (MS) R3974741-3 09/17/23 19:43 • (MSD) R3974741-4 09/17/23 20:05
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Acenaphthene 50.0 U 20.2 22.1 40.4 44.2 1 47.0-145 J6 J6 8.98 48
Acenaphthylene 50.0 U 18.7 21.4 37.4 42.8 1 33.0-145 13.5 74
Anthracene 50.0 U 17.8 21.3 35.6 42.6 1 27.0-133 17.9 66
Benzo(a)anthracene 50.0 U 16.1 19.6 32.2 39.2 1 33.0-143 J6 19.6 53
Benzo(b)fluoranthene 50.0 U 17.6 21.8 35.2 43.6 1 24.0-159 21.3 71
Benzo(k)fluoranthene 50.0 U 17.3 20.8 34.6 41.6 1 11.0-162 18.4 63
Benzo(g,h,i)perylene 50.0 U 16.0 19.1 32.0 38.2 1 1.00-219 17.7 97
Benzo(a)pyrene 50.0 U 17.0 21.3 34.0 42.6 1 17.0-163 22.5 72
Bis(2-chlorethoxy)methane 50.0 U 20.7 22.9 41.4 45.8 1 33.0-184 10.1 54
Bis(2-chloroethyl)ether 50.0 U 20.6 23.5 41.2 47.0 1 12.0-158 13.2 108
2,2-Oxybis(1-Chloropropane)50.0 U 19.6 22.2 39.2 44.4 1 36.0-166 12.4 76
4-Bromophenyl-phenylether 50.0 U 18.5 21.0 37.0 42.0 1 53.0-127 J6 J6 12.7 43
2-Chloronaphthalene 50.0 U 19.9 22.1 39.8 44.2 1 60.0-120 J6 J6 10.5 24
4-Chlorophenyl-phenylether 50.0 U 19.9 22.9 39.8 45.8 1 25.0-158 14.0 61
Chrysene 50.0 U 16.6 20.1 33.2 40.2 1 17.0-168 19.1 87
Dibenz(a,h)anthracene 50.0 U 16.6 19.8 33.2 39.6 1 1.00-227 17.6 126
3,3-Dichlorobenzidine 100 U U U 0.000 0.000 1 1.00-262 J6 J6 0.000 108
2,4-Dinitrotoluene 50.0 U 27.7 30.7 55.4 61.4 1 39.0-139 10.3 42
2,6-Dinitrotoluene 50.0 U 24.3 27.3 48.6 54.6 1 50.0-158 J6 11.6 48
Fluoranthene 50.0 U 18.6 22.3 37.2 44.6 1 26.0-137 18.1 66
Fluorene 50.0 U 20.7 24.3 41.4 48.6 1 59.0-121 J6 J6 16.0 38
Hexachlorobenzene 50.0 U 15.8 18.7 31.6 37.4 1 1.00-152 16.8 55
Hexachloro-1,3-butadiene 50.0 U 17.5 20.0 35.0 40.0 1 24.0-120 13.3 62
Hexachlorocyclopentadiene 50.0 U 9.97 11.5 19.9 23.0 1 10.0-146 14.3 34
Hexachloroethane 50.0 U 18.0 19.6 36.0 39.2 1 40.0-120 J6 J6 8.51 52
Indeno(1,2,3-cd)pyrene 50.0 U 15.4 18.5 30.8 37.0 1 1.00-171 18.3 99
Isophorone 50.0 U 20.7 23.9 41.4 47.8 1 21.0-196 14.3 93
Naphthalene 50.0 U 18.7 21.2 37.4 42.4 1 21.0-133 12.5 65
Nitrobenzene 50.0 U 28.7 29.7 57.4 59.4 1 35.0-180 3.42 62
n-Nitrosodimethylamine 50.0 U 20.7 24.0 41.4 48.0 1 10.0-120 14.8 40
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 68 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 68 of 78
QUALITY CONTROL SUMMARYWG2132824
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1655691-01,02,03,04,05,06,07,08,09
L1655875-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1655875-01 09/17/23 19:21 • (MS) R3974741-3 09/17/23 19:43 • (MSD) R3974741-4 09/17/23 20:05
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
n-Nitrosodiphenylamine 50.0 U 20.4 23.9 40.8 47.8 1 16.0-160 15.8 28
n-Nitrosodi-n-propylamine 50.0 U 22.8 25.1 45.6 50.2 1 1.00-230 9.60 87
Phenanthrene 50.0 U 19.6 22.3 39.2 44.6 1 54.0-120 J6 J6 12.9 39
Benzylbutyl phthalate 50.0 U 22.6 27.2 45.2 54.4 1 1.00-152 18.5 60
Bis(2-ethylhexyl)phthalate 50.0 U 19.0 22.7 38.0 45.4 1 8.00-158 17.7 82
Di-n-butyl phthalate 50.0 U 20.7 24.4 41.4 48.8 1 1.00-120 16.4 47
Diethyl phthalate 50.0 U 23.4 26.4 46.8 52.8 1 1.00-120 12.0 100
Dimethyl phthalate 50.0 U 24.3 26.4 48.6 52.8 1 1.00-120 8.28 183
Di-n-octyl phthalate 50.0 U 17.8 21.2 35.6 42.4 1 4.00-146 17.4 69
Pyrene 50.0 U 19.4 23.8 38.8 47.6 1 52.0-120 J6 J6 20.4 49
1,2,4-Trichlorobenzene 50.0 U 19.6 21.7 39.2 43.4 1 44.0-142 J6 J6 10.2 50
4-Chloro-3-methylphenol 50.0 U 18.4 21.9 36.8 43.8 1 22.0-147 17.4 73
2-Chlorophenol 50.0 U 16.6 20.4 33.2 40.8 1 23.0-134 20.5 61
2,4-Dichlorophenol 50.0 U 19.1 22.8 38.2 45.6 1 39.0-135 J6 17.7 50
2,4-Dimethylphenol 50.0 U 3.57 3.39 7.14 6.78 1 32.0-120 J6 J6 5.17 58
4,6-Dinitro-2-methylphenol 50.0 U 22.5 27.4 45.0 54.8 1 1.00-181 19.6 203
2,4-Dinitrophenol 50.0 U 24.7 30.4 49.4 60.8 1 1.00-191 20.7 132
2-Nitrophenol 50.0 U 22.9 25.9 45.8 51.8 1 29.0-182 12.3 55
4-Nitrophenol 50.0 U 60.9 69.5 122 139 1 1.00-132 J5 13.2 131
Pentachlorophenol 50.0 U 15.2 19.1 30.4 38.2 1 14.0-176 22.7 86
Phenol 50.0 U 9.16 10.1 18.3 20.2 1 5.00-120 9.76 64
2,4,6-Trichlorophenol 50.0 U 20.5 23.5 41.0 47.0 1 37.0-144 13.6 58
(S) Nitrobenzene-d5 43.8 53.4 15.0-314
(S) 2-Fluorobiphenyl 39.1 49.7 22.0-127
(S) p-Terphenyl-d14 32.2 41.8 29.0-141
(S) Phenol-d5 17.3 21.3 8.00-424
(S) 2-Fluorophenol 22.7 30.6 10.0-120
(S) 2,4,6-Tribromophenol 35.2 47.0 10.0-153
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 69 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 69 of 78
QUALITY CONTROL SUMMARYWG2134767
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1655691-10,11,12,13
Method Blank (MB)
(MB) R3979157-2 09/21/23 02:55
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.0886 1.00
Acenaphthylene U 0.0921 1.00
Anthracene U 0.0804 1.00
Benzo(a)anthracene U 0.199 1.00
Benzo(b)fluoranthene U 0.130 1.00
Benzo(k)fluoranthene U 0.120 1.00
Benzo(g,h,i)perylene U 0.121 1.00
Benzo(a)pyrene U 0.0381 1.00
Bis(2-chlorethoxy)methane U 0.116 10.0
Bis(2-chloroethyl)ether U 0.137 10.0
2,2-Oxybis(1-Chloropropane)U 0.210 10.0
4-Bromophenyl-phenylether U 0.0877 10.0
2-Chloronaphthalene U 0.0648 1.00
4-Chlorophenyl-phenylether U 0.0926 10.0
Chrysene U 0.130 1.00
Dibenz(a,h)anthracene U 0.0644 1.00
3,3-Dichlorobenzidine U 0.212 10.0
2,4-Dinitrotoluene U 0.0983 10.0
2,6-Dinitrotoluene U 0.250 10.0
Fluoranthene U 0.102 1.00
Fluorene U 0.0844 1.00
Hexachlorobenzene U 0.0755 1.00
Hexachloro-1,3-butadiene U 0.0968 10.0
Hexachlorocyclopentadiene U 0.0598 10.0
Hexachloroethane U 0.127 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.143 10.0
Naphthalene U 0.159 1.00
Nitrobenzene U 0.297 10.0
n-Nitrosodimethylamine U 0.998 10.0
n-Nitrosodiphenylamine U 2.37 10.0
n-Nitrosodi-n-propylamine U 0.261 10.0
Phenanthrene U 0.112 1.00
Benzylbutyl phthalate U 0.765 3.00
Bis(2-ethylhexyl)phthalate U 0.895 3.00
Di-n-butyl phthalate U 0.453 3.00
Diethyl phthalate U 0.287 3.00
Dimethyl phthalate U 0.260 3.00
Di-n-octyl phthalate U 0.932 3.00
Pyrene U 0.107 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 70 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 70 of 78
QUALITY CONTROL SUMMARYWG2134767
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1655691-10,11,12,13
Method Blank (MB)
(MB) R3979157-2 09/21/23 02:55
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
1,2,4-Trichlorobenzene U 0.0698 10.0
4-Chloro-3-methylphenol U 0.131 10.0
2-Chlorophenol U 0.133 10.0
2,4-Dichlorophenol U 0.102 10.0
2,4-Dimethylphenol U 0.0636 10.0
4,6-Dinitro-2-methylphenol U 1.12 10.0
2,4-Dinitrophenol U 5.93 10.0
2-Nitrophenol U 0.117 10.0
4-Nitrophenol U 0.143 10.0
Pentachlorophenol U 0.313 10.0
Phenol U 4.33 10.0
2,4,6-Trichlorophenol U 0.100 10.0
(S) Nitrobenzene-d5 41.2 15.0-314
(S) 2-Fluorobiphenyl 42.1 22.0-127
(S) p-Terphenyl-d14 62.7 29.0-141
(S) Phenol-d5 15.3 8.00-424
(S) 2-Fluorophenol 22.7 10.0-120
(S) 2,4,6-Tribromophenol 45.4 10.0-153
Laboratory Control Sample (LCS)
(LCS) R3979157-1 09/21/23 02:33
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acenaphthene 50.0 26.4 52.8 47.0-145
Acenaphthylene 50.0 26.1 52.2 33.0-145
Anthracene 50.0 28.6 57.2 27.0-133
Benzo(a)anthracene 50.0 28.9 57.8 33.0-143
Benzo(b)fluoranthene 50.0 31.1 62.2 24.0-159
Benzo(k)fluoranthene 50.0 29.5 59.0 11.0-162
Benzo(g,h,i)perylene 50.0 28.5 57.0 1.00-219
Benzo(a)pyrene 50.0 31.6 63.2 17.0-163
Bis(2-chlorethoxy)methane 50.0 23.2 46.4 1.00-219
Bis(2-chloroethyl)ether 50.0 23.0 46.0 33.0-185
2,2-Oxybis(1-Chloropropane)50.0 22.3 44.6 36.0-166
4-Bromophenyl-phenylether 50.0 26.2 52.4 53.0-127 J4
2-Chloronaphthalene 50.0 25.3 50.6 60.0-120 J4
4-Chlorophenyl-phenylether 50.0 27.0 54.0 25.0-158
Chrysene 50.0 28.7 57.4 17.0-168
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 71 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 71 of 78
QUALITY CONTROL SUMMARYWG2134767
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1655691-10,11,12,13
Laboratory Control Sample (LCS)
(LCS) R3979157-1 09/21/23 02:33
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Dibenz(a,h)anthracene 50.0 29.2 58.4 1.00-227
3,3-Dichlorobenzidine 100 51.5 51.5 1.00-262
2,4-Dinitrotoluene 50.0 31.2 62.4 39.0-139
2,6-Dinitrotoluene 50.0 28.3 56.6 50.0-158
Fluoranthene 50.0 27.1 54.2 26.0-137
Fluorene 50.0 27.9 55.8 59.0-121 J4
Hexachlorobenzene 50.0 25.4 50.8 1.00-152
Hexachloro-1,3-butadiene 50.0 22.6 45.2 24.0-120
Hexachlorocyclopentadiene 50.0 10.6 21.2 10.0-120
Hexachloroethane 50.0 24.8 49.6 40.0-120
Indeno(1,2,3-cd)pyrene 50.0 27.4 54.8 1.00-171
Isophorone 50.0 24.5 49.0 21.0-196
Naphthalene 50.0 22.2 44.4 21.0-133
Nitrobenzene 50.0 24.1 48.2 35.0-180
n-Nitrosodimethylamine 50.0 25.7 51.4 10.0-120
n-Nitrosodiphenylamine 50.0 28.4 56.8 44.0-120
n-Nitrosodi-n-propylamine 50.0 26.0 52.0 1.00-230
Phenanthrene 50.0 26.9 53.8 54.0-120 J4
Benzylbutyl phthalate 50.0 39.6 79.2 1.00-152
Bis(2-ethylhexyl)phthalate 50.0 36.7 73.4 8.00-158
Di-n-butyl phthalate 50.0 32.7 65.4 1.00-120
Diethyl phthalate 50.0 30.3 60.6 1.00-120
Dimethyl phthalate 50.0 28.0 56.0 1.00-120
Di-n-octyl phthalate 50.0 32.1 64.2 4.00-146
Pyrene 50.0 32.4 64.8 52.0-120
1,2,4-Trichlorobenzene 50.0 22.6 45.2 44.0-142
4-Chloro-3-methylphenol 50.0 20.4 40.8 22.0-147
2-Chlorophenol 50.0 18.0 36.0 23.0-134
2,4-Dichlorophenol 50.0 21.5 43.0 39.0-135
2,4-Dimethylphenol 50.0 22.6 45.2 32.0-120
4,6-Dinitro-2-methylphenol 50.0 33.6 67.2 1.00-181
2,4-Dinitrophenol 50.0 25.0 50.0 1.00-191
2-Nitrophenol 50.0 25.4 50.8 29.0-182
4-Nitrophenol 50.0 76.1 152 1.00-132 J4
Pentachlorophenol 50.0 18.5 37.0 14.0-176
Phenol 50.0 8.90 17.8 5.00-120
2,4,6-Trichlorophenol 50.0 25.7 51.4 37.0-144
(S) Nitrobenzene-d5 45.5 15.0-314
(S) 2-Fluorobiphenyl 49.1 22.0-127
(S) p-Terphenyl-d14 59.1 29.0-141
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 72 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 72 of 78
QUALITY CONTROL SUMMARYWG2134767
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1655691-10,11,12,13
Laboratory Control Sample (LCS)
(LCS) R3979157-1 09/21/23 02:33
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
(S) Phenol-d5 16.1 8.00-424
(S) 2-Fluorophenol 22.2 10.0-120
(S) 2,4,6-Tribromophenol 48.2 10.0-153
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 73 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 73 of 78
GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 74 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 74 of 78

Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:06 75 of 78
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1655691 09/29/23 16:22 75 of 78
ANALYTICAL REPORT
December 05, 2023
Colonial Pipeline- S&ME Raleigh
Sample Delivery Group:L1682140
Samples Received:11/29/2023
Project Number:210818
Description:Colonial Pipeline - Jennifer Drive
Report To:Mr. Michael Pfeifer
3201 Spring Forrest Road
Raleigh, NC 27616
Entire Report Reviewed By:
December 05, 2023
[Preliminary Report]
Craig Cothron
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 1 of 44
December 06, 2023
Craig Cothron
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 1 of 44
TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 5
Sr: Sample Results 6
MW-2 L1682140-01 6
MW-3 L1682140-02 9
MW-6 L1682140-03 12
MW-7 L1682140-04 15
MW-8 L1682140-05 18
MW-9 L1682140-06 21
MW-12 L1682140-07 24
MW-13 L1682140-08 27
Qc: Quality Control Summary 30
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 30
TPH by Method MADEPE 35
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 36
Gl: Glossary of Terms 41
Al: Accreditations & Locations 42
Sc: Sample Chain of Custody 43
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 2 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 2 of 44
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-2 L1682140-01 GW James Waters 11/28/23 09:50 11/29/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2181973 1 12/04/23 02:49 12/04/23 02:49 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2182350 1 12/04/23 18:59 12/04/23 18:59 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2180752 1 11/30/23 09:31 12/02/23 08:44 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2180752 1 11/30/23 09:31 12/02/23 11:31 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2181093 1 12/01/23 16:42 12/01/23 23:52 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-3 L1682140-02 GW James Waters 11/28/23 13:15 11/29/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2181973 100 12/04/23 05:08 12/04/23 05:08 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2182350 100 12/04/23 22:24 12/04/23 22:24 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2180752 1 11/30/23 09:31 12/02/23 09:08 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2180752 1 11/30/23 09:31 12/02/23 11:07 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2181093 1 12/01/23 16:42 12/02/23 00:13 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-6 L1682140-03 GW James Waters 11/28/23 12:00 11/29/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2181973 1 12/04/23 03:09 12/04/23 03:09 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2182350 1 12/04/23 19:19 12/04/23 19:19 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2180752 1 11/30/23 09:31 12/02/23 09:32 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2180752 1 11/30/23 09:31 12/02/23 10:44 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2181093 1 12/01/23 16:42 12/02/23 00:34 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-7 L1682140-04 GW James Waters 11/28/23 12:30 11/29/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2181973 1 12/04/23 03:29 12/04/23 03:29 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2182350 1 12/04/23 19:40 12/04/23 19:40 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2180752 1 11/30/23 09:31 12/02/23 09:56 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2180752 1 11/30/23 09:31 12/02/23 10:20 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2181093 1 12/01/23 16:42 12/02/23 00:55 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-8 L1682140-05 GW James Waters 11/28/23 13:00 11/29/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2181973 1 12/04/23 03:48 12/04/23 03:48 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2182350 1 12/04/23 20:00 12/04/23 20:00 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2180752 1 11/30/23 09:31 12/02/23 15:55 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2180752 1 11/30/23 09:31 12/02/23 21:07 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2181093 1 12/01/23 16:42 12/02/23 01:16 AGW Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 3 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 3 of 44
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-9 L1682140-06 GW James Waters 11/28/23 12:40 11/29/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2181973 1 12/04/23 04:08 12/04/23 04:08 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2182350 1 12/04/23 20:21 12/04/23 20:21 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2180752 1 11/30/23 09:31 12/02/23 16:19 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2180752 1 11/30/23 09:31 12/02/23 20:43 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2181093 1 12/01/23 16:42 12/02/23 01:37 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-12 L1682140-07 GW James Waters 11/28/23 11:25 11/29/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2181973 1 12/04/23 04:28 12/04/23 04:28 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2182350 1 12/04/23 20:42 12/04/23 20:42 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2180752 1 11/30/23 09:31 12/02/23 16:43 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2180752 1 11/30/23 09:31 12/02/23 20:19 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2181093 1 12/01/23 16:42 12/02/23 01:58 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-13 L1682140-08 GW James Waters 11/28/23 10:40 11/29/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2181973 1 12/04/23 04:48 12/04/23 04:48 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2182350 1 12/04/23 21:02 12/04/23 21:02 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2180752 1 11/30/23 09:31 12/02/23 17:07 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2180752 1 11/30/23 09:31 12/02/23 19:55 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2181093 1 12/01/23 16:42 12/02/23 02:19 AGW Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 4 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 4 of 44
CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Craig Cothron
Project Manager
Sample Delivery Group (SDG) Narrative
An aliquot for analysis was taken from the original container received due to the level of sediment present in the sample.
Rinsing of the original sample container for inclusion in the sample extraction was not performed.
Lab Sample ID Project Sample ID Method
L1682140-01 MW-2 625.1
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 5 of 44
Craig Cothron
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 5 of 44
SAMPLE RESULTS - 01
L1682140
MW-2
Collected date/time: 11/28/23 09:50
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.0941 1.00 1 12/04/2023 02:49 WG2181973
Bromobenzene U 0.118 1.00 1 12/04/2023 02:49 WG2181973
Bromodichloromethane U 0.136 1.00 1 12/04/2023 02:49 WG2181973
Bromochloromethane U 0.128 1.00 1 12/04/2023 02:49 WG2181973
Bromoform U 0.129 1.00 1 12/04/2023 02:49 WG2181973
Bromomethane U 0.605 5.00 1 12/04/2023 02:49 WG2181973
n-Butylbenzene U 0.157 1.00 1 12/04/2023 02:49 WG2181973
sec-Butylbenzene U 0.125 1.00 1 12/04/2023 02:49 WG2181973
tert-Butylbenzene U J4 0.127 1.00 1 12/04/2023 02:49 WG2181973
Carbon tetrachloride U 0.128 1.00 1 12/04/2023 02:49 WG2181973
Chlorobenzene U 0.116 1.00 1 12/04/2023 02:49 WG2181973
Chlorodibromomethane U 0.140 1.00 1 12/04/2023 02:49 WG2181973
Chloroethane U 0.192 5.00 1 12/04/2023 02:49 WG2181973
Chloroform U 0.111 5.00 1 12/04/2023 02:49 WG2181973
Chloromethane U 0.960 2.50 1 12/04/2023 02:49 WG2181973
2-Chlorotoluene U 0.106 1.00 1 12/04/2023 02:49 WG2181973
4-Chlorotoluene U 0.114 1.00 1 12/04/2023 02:49 WG2181973
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 12/04/2023 02:49 WG2181973
1,2-Dibromoethane U 0.126 1.00 1 12/04/2023 02:49 WG2181973
Dibromomethane U 0.122 1.00 1 12/04/2023 02:49 WG2181973
1,2-Dichlorobenzene U 0.107 1.00 1 12/04/2023 02:49 WG2181973
1,3-Dichlorobenzene U 0.110 1.00 1 12/04/2023 02:49 WG2181973
1,4-Dichlorobenzene U 0.120 1.00 1 12/04/2023 02:49 WG2181973
Dichlorodifluoromethane U 0.374 5.00 1 12/04/2023 02:49 WG2181973
1,1-Dichloroethane U 0.100 1.00 1 12/04/2023 02:49 WG2181973
1,2-Dichloroethane U 0.0819 1.00 1 12/04/2023 02:49 WG2181973
1,1-Dichloroethene U 0.188 1.00 1 12/04/2023 02:49 WG2181973
cis-1,2-Dichloroethene U 0.126 1.00 1 12/04/2023 02:49 WG2181973
trans-1,2-Dichloroethene U 0.149 1.00 1 12/04/2023 02:49 WG2181973
1,2-Dichloropropane U 0.149 1.00 1 12/04/2023 02:49 WG2181973
1,1-Dichloropropene U 0.142 1.00 1 12/04/2023 02:49 WG2181973
1,3-Dichloropropane U 0.110 1.00 1 12/04/2023 02:49 WG2181973
cis-1,3-Dichloropropene U 0.111 1.00 1 12/04/2023 02:49 WG2181973
trans-1,3-Dichloropropene U 0.118 1.00 1 12/04/2023 02:49 WG2181973
2,2-Dichloropropane U 0.161 1.00 1 12/04/2023 02:49 WG2181973
Di-isopropyl ether U 0.105 1.00 1 12/04/2023 02:49 WG2181973
Ethylbenzene U 0.137 1.00 1 12/04/2023 02:49 WG2181973
Hexachloro-1,3-butadiene U 0.337 1.00 1 12/04/2023 02:49 WG2181973
Isopropylbenzene U 0.105 1.00 1 12/04/2023 02:49 WG2181973
Methylene Chloride U 0.430 5.00 1 12/04/2023 02:49 WG2181973
Methyl tert-butyl ether U 0.101 1.00 1 12/04/2023 02:49 WG2181973
Naphthalene U 1.00 5.00 1 12/04/2023 02:49 WG2181973
n-Propylbenzene U 0.0993 1.00 1 12/04/2023 02:49 WG2181973
Styrene U 0.118 1.00 1 12/04/2023 02:49 WG2181973
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 12/04/2023 02:49 WG2181973
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 12/04/2023 02:49 WG2181973
Tetrachloroethene U 0.300 1.00 1 12/04/2023 02:49 WG2181973
Toluene U 0.278 1.00 1 12/04/2023 02:49 WG2181973
1,2,3-Trichlorobenzene U 0.230 1.00 1 12/04/2023 02:49 WG2181973
1,2,4-Trichlorobenzene U 0.481 1.00 1 12/04/2023 02:49 WG2181973
1,1,1-Trichloroethane U 0.149 1.00 1 12/04/2023 02:49 WG2181973
1,1,2-Trichloroethane U 0.158 1.00 1 12/04/2023 02:49 WG2181973
Trichloroethene U 0.190 1.00 1 12/04/2023 02:49 WG2181973
Trichlorofluoromethane U 0.160 5.00 1 12/04/2023 02:49 WG2181973
1,2,3-Trichloropropane U 0.237 2.50 1 12/04/2023 02:49 WG2181973
1,2,4-Trimethylbenzene U 0.322 1.00 1 12/04/2023 02:49 WG2181973
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 6 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 6 of 44
SAMPLE RESULTS - 01
L1682140
MW-2
Collected date/time: 11/28/23 09:50
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene U 0.104 1.00 1 12/04/2023 02:49 WG2181973
Vinyl chloride U 0.234 1.00 1 12/04/2023 02:49 WG2181973
o-Xylene U 0.174 1.00 1 12/04/2023 02:49 WG2181973
m&p-Xylenes U 0.430 2.00 1 12/04/2023 02:49 WG2181973
ethanol U C4 42.0 100 1 12/04/2023 18:59 WG2182350
tert-Amyl Methyl Ether U 0.195 1.00 1 12/04/2023 02:49 WG2181973
Ethyl tert-butyl ether U 0.101 1.00 1 12/04/2023 02:49 WG2181973
tert-Butyl alcohol U 4.06 5.00 1 12/04/2023 02:49 WG2181973
t-Amyl Alcohol U 4.90 50.0 1 12/04/2023 02:49 WG2181973
tert-Butyl formate U C4 4.51 20.0 1 12/04/2023 18:59 WG2182350
(S) Toluene-d8 104 80.0-120 12/04/2023 02:49 WG2181973
(S) Toluene-d8 111 80.0-120 12/04/2023 18:59 WG2182350
(S) 4-Bromofluorobenzene 96.4 77.0-126 12/04/2023 02:49 WG2181973
(S) 4-Bromofluorobenzene 84.6 77.0-126 12/04/2023 18:59 WG2182350
(S) 1,2-Dichloroethane-d4 100 70.0-130 12/04/2023 02:49 WG2181973
(S) 1,2-Dichloroethane-d4 103 70.0-130 12/04/2023 18:59 WG2182350
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics U 33.3 100 1 12/02/2023 08:44 WG2180752
Unadjusted C19-C36 Aliphatics 52.5 B J 33.3 100 1 12/02/2023 08:44 WG2180752
Unadjusted C11-C22 Aromatics 69.6 B J 33.3 100 1 12/02/2023 11:31 WG2180752
Unadjusted Total Petroleum
Hydrocarbons 122 33.3 100 1 12/02/2023 11:31 WG2180752
(S) o-Terphenyl 56.1 40.0-140 12/02/2023 11:31 WG2180752
(S) 1-Chloro-octadecane 27.4 J2 40.0-140 12/02/2023 08:44 WG2180752
(S) 2-Fluorobiphenyl 67.9 40.0-140 12/02/2023 11:31 WG2180752
(S) 2-Bromonaphthalene 62.4 40.0-140 12/02/2023 11:31 WG2180752
Sample Narrative:
L1682140-01 WG2180752: Sample produced heavy emulsion during Extraction process, low surr/spike recoveries due to matrix
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 12/01/2023 23:52 WG2181093
Acenaphthylene U 0.0921 1.00 1 12/01/2023 23:52 WG2181093
Anthracene U 0.0804 1.00 1 12/01/2023 23:52 WG2181093
Benzo(a)anthracene U 0.199 1.00 1 12/01/2023 23:52 WG2181093
Benzo(b)fluoranthene U 0.130 1.00 1 12/01/2023 23:52 WG2181093
Benzo(k)fluoranthene U 0.120 1.00 1 12/01/2023 23:52 WG2181093
Benzo(g,h,i)perylene U 0.121 1.00 1 12/01/2023 23:52 WG2181093
Benzo(a)pyrene U 0.0381 1.00 1 12/01/2023 23:52 WG2181093
Bis(2-chlorethoxy)methane U 0.116 10.0 1 12/01/2023 23:52 WG2181093
Bis(2-chloroethyl)ether U 0.137 10.0 1 12/01/2023 23:52 WG2181093
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 12/01/2023 23:52 WG2181093
4-Bromophenyl-phenylether U 0.0877 10.0 1 12/01/2023 23:52 WG2181093
2-Chloronaphthalene U 0.0648 1.00 1 12/01/2023 23:52 WG2181093
4-Chlorophenyl-phenylether U 0.0926 10.0 1 12/01/2023 23:52 WG2181093
Chrysene U 0.130 1.00 1 12/01/2023 23:52 WG2181093
Dibenz(a,h)anthracene U 0.0644 1.00 1 12/01/2023 23:52 WG2181093
3,3-Dichlorobenzidine U 0.212 10.0 1 12/01/2023 23:52 WG2181093
2,4-Dinitrotoluene U 0.0983 10.0 1 12/01/2023 23:52 WG2181093
2,6-Dinitrotoluene U 0.250 10.0 1 12/01/2023 23:52 WG2181093
Fluoranthene U 0.102 1.00 1 12/01/2023 23:52 WG2181093
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 7 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 7 of 44
SAMPLE RESULTS - 01
L1682140
MW-2
Collected date/time: 11/28/23 09:50
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Fluorene U 0.0844 1.00 1 12/01/2023 23:52 WG2181093
Hexachlorobenzene U 0.0755 1.00 1 12/01/2023 23:52 WG2181093
Hexachloro-1,3-butadiene U 0.0968 10.0 1 12/01/2023 23:52 WG2181093
Hexachlorocyclopentadiene U 0.0598 10.0 1 12/01/2023 23:52 WG2181093
Hexachloroethane U 0.127 10.0 1 12/01/2023 23:52 WG2181093
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 12/01/2023 23:52 WG2181093
Isophorone U 0.143 10.0 1 12/01/2023 23:52 WG2181093
Naphthalene U 0.159 1.00 1 12/01/2023 23:52 WG2181093
Nitrobenzene U 0.297 10.0 1 12/01/2023 23:52 WG2181093
n-Nitrosodimethylamine U 0.998 10.0 1 12/01/2023 23:52 WG2181093
n-Nitrosodiphenylamine U 2.37 10.0 1 12/01/2023 23:52 WG2181093
n-Nitrosodi-n-propylamine U 0.261 10.0 1 12/01/2023 23:52 WG2181093
Phenanthrene U 0.112 1.00 1 12/01/2023 23:52 WG2181093
Benzylbutyl phthalate U 0.765 3.00 1 12/01/2023 23:52 WG2181093
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 12/01/2023 23:52 WG2181093
Di-n-butyl phthalate U 0.453 3.00 1 12/01/2023 23:52 WG2181093
Diethyl phthalate U 0.287 3.00 1 12/01/2023 23:52 WG2181093
Dimethyl phthalate U 0.260 3.00 1 12/01/2023 23:52 WG2181093
Di-n-octyl phthalate U 0.932 3.00 1 12/01/2023 23:52 WG2181093
Pyrene U 0.107 1.00 1 12/01/2023 23:52 WG2181093
1,2,4-Trichlorobenzene U 0.0698 10.0 1 12/01/2023 23:52 WG2181093
4-Chloro-3-methylphenol U 0.131 10.0 1 12/01/2023 23:52 WG2181093
2-Chlorophenol U 0.133 10.0 1 12/01/2023 23:52 WG2181093
2,4-Dichlorophenol U 0.102 10.0 1 12/01/2023 23:52 WG2181093
2,4-Dimethylphenol U 0.0636 10.0 1 12/01/2023 23:52 WG2181093
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 12/01/2023 23:52 WG2181093
2,4-Dinitrophenol U 5.93 10.0 1 12/01/2023 23:52 WG2181093
2-Nitrophenol U 0.117 10.0 1 12/01/2023 23:52 WG2181093
4-Nitrophenol U 0.143 10.0 1 12/01/2023 23:52 WG2181093
Pentachlorophenol U 0.313 10.0 1 12/01/2023 23:52 WG2181093
Phenol U 4.33 10.0 1 12/01/2023 23:52 WG2181093
2,4,6-Trichlorophenol U 0.100 10.0 1 12/01/2023 23:52 WG2181093
(S) Nitrobenzene-d5 55.1 15.0-314 12/01/2023 23:52 WG2181093
(S) 2-Fluorobiphenyl 48.2 22.0-127 12/01/2023 23:52 WG2181093
(S) p-Terphenyl-d14 76.2 29.0-141 12/01/2023 23:52 WG2181093
(S) Phenol-d5 22.2 8.00-424 12/01/2023 23:52 WG2181093
(S) 2-Fluorophenol 28.5 10.0-120 12/01/2023 23:52 WG2181093
(S) 2,4,6-Tribromophenol 49.9 10.0-153 12/01/2023 23:52 WG2181093
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 8 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 8 of 44
SAMPLE RESULTS - 02
L1682140
MW-3
Collected date/time: 11/28/23 13:15
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene 3030 9.41 100 100 12/04/2023 05:08 WG2181973
Bromobenzene U 11.8 100 100 12/04/2023 05:08 WG2181973
Bromodichloromethane U 13.6 100 100 12/04/2023 05:08 WG2181973
Bromochloromethane U 12.8 100 100 12/04/2023 05:08 WG2181973
Bromoform U 12.9 100 100 12/04/2023 05:08 WG2181973
Bromomethane U 60.5 500 100 12/04/2023 05:08 WG2181973
n-Butylbenzene U 15.7 100 100 12/04/2023 05:08 WG2181973
sec-Butylbenzene U 12.5 100 100 12/04/2023 05:08 WG2181973
tert-Butylbenzene U J4 12.7 100 100 12/04/2023 05:08 WG2181973
Carbon tetrachloride U 12.8 100 100 12/04/2023 05:08 WG2181973
Chlorobenzene U 11.6 100 100 12/04/2023 05:08 WG2181973
Chlorodibromomethane U 14.0 100 100 12/04/2023 05:08 WG2181973
Chloroethane U 19.2 500 100 12/04/2023 05:08 WG2181973
Chloroform U 11.1 500 100 12/04/2023 05:08 WG2181973
Chloromethane U 96.0 250 100 12/04/2023 05:08 WG2181973
2-Chlorotoluene U 10.6 100 100 12/04/2023 05:08 WG2181973
4-Chlorotoluene U 11.4 100 100 12/04/2023 05:08 WG2181973
1,2-Dibromo-3-Chloropropane U 27.6 500 100 12/04/2023 05:08 WG2181973
1,2-Dibromoethane U 12.6 100 100 12/04/2023 05:08 WG2181973
Dibromomethane U 12.2 100 100 12/04/2023 05:08 WG2181973
1,2-Dichlorobenzene U 10.7 100 100 12/04/2023 05:08 WG2181973
1,3-Dichlorobenzene U 11.0 100 100 12/04/2023 05:08 WG2181973
1,4-Dichlorobenzene U 12.0 100 100 12/04/2023 05:08 WG2181973
Dichlorodifluoromethane U 37.4 500 100 12/04/2023 05:08 WG2181973
1,1-Dichloroethane U 10.0 100 100 12/04/2023 05:08 WG2181973
1,2-Dichloroethane U 8.19 100 100 12/04/2023 05:08 WG2181973
1,1-Dichloroethene U 18.8 100 100 12/04/2023 05:08 WG2181973
cis-1,2-Dichloroethene U 12.6 100 100 12/04/2023 05:08 WG2181973
trans-1,2-Dichloroethene U 14.9 100 100 12/04/2023 05:08 WG2181973
1,2-Dichloropropane U 14.9 100 100 12/04/2023 05:08 WG2181973
1,1-Dichloropropene U 14.2 100 100 12/04/2023 05:08 WG2181973
1,3-Dichloropropane U 11.0 100 100 12/04/2023 05:08 WG2181973
cis-1,3-Dichloropropene U 11.1 100 100 12/04/2023 05:08 WG2181973
trans-1,3-Dichloropropene U 11.8 100 100 12/04/2023 05:08 WG2181973
2,2-Dichloropropane U 16.1 100 100 12/04/2023 05:08 WG2181973
Di-isopropyl ether U 10.5 100 100 12/04/2023 05:08 WG2181973
Ethylbenzene 531 13.7 100 100 12/04/2023 05:08 WG2181973
Hexachloro-1,3-butadiene U 33.7 100 100 12/04/2023 05:08 WG2181973
Isopropylbenzene 21.5 J 10.5 100 100 12/04/2023 05:08 WG2181973
Methylene Chloride U 43.0 500 100 12/04/2023 05:08 WG2181973
Methyl tert-butyl ether U 10.1 100 100 12/04/2023 05:08 WG2181973
Naphthalene 106 J 100 500 100 12/04/2023 05:08 WG2181973
n-Propylbenzene 39.0 J 9.93 100 100 12/04/2023 05:08 WG2181973
Styrene U 11.8 100 100 12/04/2023 05:08 WG2181973
1,1,1,2-Tetrachloroethane U 14.7 100 100 12/04/2023 05:08 WG2181973
1,1,2,2-Tetrachloroethane U 13.3 100 100 12/04/2023 05:08 WG2181973
Tetrachloroethene U 30.0 100 100 12/04/2023 05:08 WG2181973
Toluene 6550 27.8 100 100 12/04/2023 05:08 WG2181973
1,2,3-Trichlorobenzene U 23.0 100 100 12/04/2023 05:08 WG2181973
1,2,4-Trichlorobenzene U 48.1 100 100 12/04/2023 05:08 WG2181973
1,1,1-Trichloroethane U 14.9 100 100 12/04/2023 05:08 WG2181973
1,1,2-Trichloroethane U 15.8 100 100 12/04/2023 05:08 WG2181973
Trichloroethene U 19.0 100 100 12/04/2023 05:08 WG2181973
Trichlorofluoromethane U 16.0 500 100 12/04/2023 05:08 WG2181973
1,2,3-Trichloropropane U 23.7 250 100 12/04/2023 05:08 WG2181973
1,2,4-Trimethylbenzene 514 32.2 100 100 12/04/2023 05:08 WG2181973
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 9 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 9 of 44
SAMPLE RESULTS - 02
L1682140
MW-3
Collected date/time: 11/28/23 13:15
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene 115 10.4 100 100 12/04/2023 05:08 WG2181973
Vinyl chloride U 23.4 100 100 12/04/2023 05:08 WG2181973
o-Xylene 1320 17.4 100 100 12/04/2023 05:08 WG2181973
m&p-Xylenes 2970 43.0 200 100 12/04/2023 05:08 WG2181973
ethanol U C4 4200 10000 100 12/04/2023 22:24 WG2182350
tert-Amyl Methyl Ether U 19.5 100 100 12/04/2023 05:08 WG2181973
Ethyl tert-butyl ether U 10.1 100 100 12/04/2023 05:08 WG2181973
tert-Butyl alcohol U 406 500 100 12/04/2023 05:08 WG2181973
t-Amyl Alcohol 2160 J 490 5000 100 12/04/2023 05:08 WG2181973
tert-Butyl formate U C4 451 2000 100 12/04/2023 22:24 WG2182350
(S) Toluene-d8 104 80.0-120 12/04/2023 05:08 WG2181973
(S) Toluene-d8 112 80.0-120 12/04/2023 22:24 WG2182350
(S) 4-Bromofluorobenzene 103 77.0-126 12/04/2023 05:08 WG2181973
(S) 4-Bromofluorobenzene 93.3 77.0-126 12/04/2023 22:24 WG2182350
(S) 1,2-Dichloroethane-d4 103 70.0-130 12/04/2023 05:08 WG2181973
(S) 1,2-Dichloroethane-d4 95.1 70.0-130 12/04/2023 22:24 WG2182350
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 36.7 B J 33.3 100 1 12/02/2023 09:08 WG2180752
Unadjusted C19-C36 Aliphatics 57.6 B J 33.3 100 1 12/02/2023 09:08 WG2180752
Unadjusted C11-C22 Aromatics 268 B 33.3 100 1 12/02/2023 11:07 WG2180752
Unadjusted Total Petroleum
Hydrocarbons 362 33.3 100 1 12/02/2023 11:07 WG2180752
(S) o-Terphenyl 58.7 40.0-140 12/02/2023 11:07 WG2180752
(S) 1-Chloro-octadecane 45.0 40.0-140 12/02/2023 09:08 WG2180752
(S) 2-Fluorobiphenyl 68.4 40.0-140 12/02/2023 11:07 WG2180752
(S) 2-Bromonaphthalene 62.6 40.0-140 12/02/2023 11:07 WG2180752
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 12/02/2023 00:13 WG2181093
Acenaphthylene U 0.0921 1.00 1 12/02/2023 00:13 WG2181093
Anthracene U 0.0804 1.00 1 12/02/2023 00:13 WG2181093
Benzo(a)anthracene U 0.199 1.00 1 12/02/2023 00:13 WG2181093
Benzo(b)fluoranthene U 0.130 1.00 1 12/02/2023 00:13 WG2181093
Benzo(k)fluoranthene U 0.120 1.00 1 12/02/2023 00:13 WG2181093
Benzo(g,h,i)perylene U 0.121 1.00 1 12/02/2023 00:13 WG2181093
Benzo(a)pyrene U 0.0381 1.00 1 12/02/2023 00:13 WG2181093
Bis(2-chlorethoxy)methane U 0.116 10.0 1 12/02/2023 00:13 WG2181093
Bis(2-chloroethyl)ether U 0.137 10.0 1 12/02/2023 00:13 WG2181093
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 12/02/2023 00:13 WG2181093
4-Bromophenyl-phenylether U 0.0877 10.0 1 12/02/2023 00:13 WG2181093
2-Chloronaphthalene U 0.0648 1.00 1 12/02/2023 00:13 WG2181093
4-Chlorophenyl-phenylether U 0.0926 10.0 1 12/02/2023 00:13 WG2181093
Chrysene U 0.130 1.00 1 12/02/2023 00:13 WG2181093
Dibenz(a,h)anthracene U 0.0644 1.00 1 12/02/2023 00:13 WG2181093
3,3-Dichlorobenzidine U 0.212 10.0 1 12/02/2023 00:13 WG2181093
2,4-Dinitrotoluene U 0.0983 10.0 1 12/02/2023 00:13 WG2181093
2,6-Dinitrotoluene U 0.250 10.0 1 12/02/2023 00:13 WG2181093
Fluoranthene U 0.102 1.00 1 12/02/2023 00:13 WG2181093
Fluorene U 0.0844 1.00 1 12/02/2023 00:13 WG2181093
Hexachlorobenzene U 0.0755 1.00 1 12/02/2023 00:13 WG2181093
Hexachloro-1,3-butadiene U 0.0968 10.0 1 12/02/2023 00:13 WG2181093
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 10 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 10 of 44
SAMPLE RESULTS - 02
L1682140
MW-3
Collected date/time: 11/28/23 13:15
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexachlorocyclopentadiene U 0.0598 10.0 1 12/02/2023 00:13 WG2181093
Hexachloroethane U 0.127 10.0 1 12/02/2023 00:13 WG2181093
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 12/02/2023 00:13 WG2181093
Isophorone U 0.143 10.0 1 12/02/2023 00:13 WG2181093
Naphthalene 58.9 0.159 1.00 1 12/02/2023 00:13 WG2181093
Nitrobenzene U 0.297 10.0 1 12/02/2023 00:13 WG2181093
n-Nitrosodimethylamine U 0.998 10.0 1 12/02/2023 00:13 WG2181093
n-Nitrosodiphenylamine U 2.37 10.0 1 12/02/2023 00:13 WG2181093
n-Nitrosodi-n-propylamine U 0.261 10.0 1 12/02/2023 00:13 WG2181093
Phenanthrene 0.216 J 0.112 1.00 1 12/02/2023 00:13 WG2181093
Benzylbutyl phthalate U 0.765 3.00 1 12/02/2023 00:13 WG2181093
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 12/02/2023 00:13 WG2181093
Di-n-butyl phthalate U 0.453 3.00 1 12/02/2023 00:13 WG2181093
Diethyl phthalate U 0.287 3.00 1 12/02/2023 00:13 WG2181093
Dimethyl phthalate U 0.260 3.00 1 12/02/2023 00:13 WG2181093
Di-n-octyl phthalate U 0.932 3.00 1 12/02/2023 00:13 WG2181093
Pyrene U 0.107 1.00 1 12/02/2023 00:13 WG2181093
1,2,4-Trichlorobenzene U 0.0698 10.0 1 12/02/2023 00:13 WG2181093
4-Chloro-3-methylphenol U 0.131 10.0 1 12/02/2023 00:13 WG2181093
2-Chlorophenol U 0.133 10.0 1 12/02/2023 00:13 WG2181093
2,4-Dichlorophenol U 0.102 10.0 1 12/02/2023 00:13 WG2181093
2,4-Dimethylphenol U 0.0636 10.0 1 12/02/2023 00:13 WG2181093
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 12/02/2023 00:13 WG2181093
2,4-Dinitrophenol U 5.93 10.0 1 12/02/2023 00:13 WG2181093
2-Nitrophenol U 0.117 10.0 1 12/02/2023 00:13 WG2181093
4-Nitrophenol U 0.143 10.0 1 12/02/2023 00:13 WG2181093
Pentachlorophenol U 0.313 10.0 1 12/02/2023 00:13 WG2181093
Phenol U 4.33 10.0 1 12/02/2023 00:13 WG2181093
2,4,6-Trichlorophenol U 0.100 10.0 1 12/02/2023 00:13 WG2181093
(S) Nitrobenzene-d5 73.7 15.0-314 12/02/2023 00:13 WG2181093
(S) 2-Fluorobiphenyl 62.5 22.0-127 12/02/2023 00:13 WG2181093
(S) p-Terphenyl-d14 73.6 29.0-141 12/02/2023 00:13 WG2181093
(S) Phenol-d5 28.2 8.00-424 12/02/2023 00:13 WG2181093
(S) 2-Fluorophenol 33.1 10.0-120 12/02/2023 00:13 WG2181093
(S) 2,4,6-Tribromophenol 73.7 10.0-153 12/02/2023 00:13 WG2181093
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 11 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 11 of 44
SAMPLE RESULTS - 03
L1682140
MW-6
Collected date/time: 11/28/23 12:00
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.0941 1.00 1 12/04/2023 03:09 WG2181973
Bromobenzene U 0.118 1.00 1 12/04/2023 03:09 WG2181973
Bromodichloromethane U 0.136 1.00 1 12/04/2023 03:09 WG2181973
Bromochloromethane U 0.128 1.00 1 12/04/2023 03:09 WG2181973
Bromoform U 0.129 1.00 1 12/04/2023 03:09 WG2181973
Bromomethane U 0.605 5.00 1 12/04/2023 03:09 WG2181973
n-Butylbenzene U 0.157 1.00 1 12/04/2023 03:09 WG2181973
sec-Butylbenzene U 0.125 1.00 1 12/04/2023 03:09 WG2181973
tert-Butylbenzene U J4 0.127 1.00 1 12/04/2023 03:09 WG2181973
Carbon tetrachloride U 0.128 1.00 1 12/04/2023 03:09 WG2181973
Chlorobenzene U 0.116 1.00 1 12/04/2023 03:09 WG2181973
Chlorodibromomethane U 0.140 1.00 1 12/04/2023 03:09 WG2181973
Chloroethane U 0.192 5.00 1 12/04/2023 03:09 WG2181973
Chloroform U 0.111 5.00 1 12/04/2023 03:09 WG2181973
Chloromethane U 0.960 2.50 1 12/04/2023 03:09 WG2181973
2-Chlorotoluene U 0.106 1.00 1 12/04/2023 03:09 WG2181973
4-Chlorotoluene U 0.114 1.00 1 12/04/2023 03:09 WG2181973
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 12/04/2023 03:09 WG2181973
1,2-Dibromoethane U 0.126 1.00 1 12/04/2023 03:09 WG2181973
Dibromomethane U 0.122 1.00 1 12/04/2023 03:09 WG2181973
1,2-Dichlorobenzene U 0.107 1.00 1 12/04/2023 03:09 WG2181973
1,3-Dichlorobenzene U 0.110 1.00 1 12/04/2023 03:09 WG2181973
1,4-Dichlorobenzene U 0.120 1.00 1 12/04/2023 03:09 WG2181973
Dichlorodifluoromethane U 0.374 5.00 1 12/04/2023 03:09 WG2181973
1,1-Dichloroethane U 0.100 1.00 1 12/04/2023 03:09 WG2181973
1,2-Dichloroethane U 0.0819 1.00 1 12/04/2023 03:09 WG2181973
1,1-Dichloroethene U 0.188 1.00 1 12/04/2023 03:09 WG2181973
cis-1,2-Dichloroethene U 0.126 1.00 1 12/04/2023 03:09 WG2181973
trans-1,2-Dichloroethene U 0.149 1.00 1 12/04/2023 03:09 WG2181973
1,2-Dichloropropane U 0.149 1.00 1 12/04/2023 03:09 WG2181973
1,1-Dichloropropene U 0.142 1.00 1 12/04/2023 03:09 WG2181973
1,3-Dichloropropane U 0.110 1.00 1 12/04/2023 03:09 WG2181973
cis-1,3-Dichloropropene U 0.111 1.00 1 12/04/2023 03:09 WG2181973
trans-1,3-Dichloropropene U 0.118 1.00 1 12/04/2023 03:09 WG2181973
2,2-Dichloropropane U 0.161 1.00 1 12/04/2023 03:09 WG2181973
Di-isopropyl ether U 0.105 1.00 1 12/04/2023 03:09 WG2181973
Ethylbenzene U 0.137 1.00 1 12/04/2023 03:09 WG2181973
Hexachloro-1,3-butadiene U 0.337 1.00 1 12/04/2023 03:09 WG2181973
Isopropylbenzene U 0.105 1.00 1 12/04/2023 03:09 WG2181973
Methylene Chloride U 0.430 5.00 1 12/04/2023 03:09 WG2181973
Methyl tert-butyl ether U 0.101 1.00 1 12/04/2023 03:09 WG2181973
Naphthalene U 1.00 5.00 1 12/04/2023 03:09 WG2181973
n-Propylbenzene U 0.0993 1.00 1 12/04/2023 03:09 WG2181973
Styrene U 0.118 1.00 1 12/04/2023 03:09 WG2181973
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 12/04/2023 03:09 WG2181973
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 12/04/2023 03:09 WG2181973
Tetrachloroethene U 0.300 1.00 1 12/04/2023 03:09 WG2181973
Toluene U 0.278 1.00 1 12/04/2023 03:09 WG2181973
1,2,3-Trichlorobenzene U 0.230 1.00 1 12/04/2023 03:09 WG2181973
1,2,4-Trichlorobenzene U 0.481 1.00 1 12/04/2023 03:09 WG2181973
1,1,1-Trichloroethane U 0.149 1.00 1 12/04/2023 03:09 WG2181973
1,1,2-Trichloroethane U 0.158 1.00 1 12/04/2023 03:09 WG2181973
Trichloroethene U 0.190 1.00 1 12/04/2023 03:09 WG2181973
Trichlorofluoromethane U 0.160 5.00 1 12/04/2023 03:09 WG2181973
1,2,3-Trichloropropane U 0.237 2.50 1 12/04/2023 03:09 WG2181973
1,2,4-Trimethylbenzene U 0.322 1.00 1 12/04/2023 03:09 WG2181973
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 12 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 12 of 44
SAMPLE RESULTS - 03
L1682140
MW-6
Collected date/time: 11/28/23 12:00
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene U 0.104 1.00 1 12/04/2023 03:09 WG2181973
Vinyl chloride U 0.234 1.00 1 12/04/2023 03:09 WG2181973
o-Xylene U 0.174 1.00 1 12/04/2023 03:09 WG2181973
m&p-Xylenes U 0.430 2.00 1 12/04/2023 03:09 WG2181973
ethanol U C4 42.0 100 1 12/04/2023 19:19 WG2182350
tert-Amyl Methyl Ether U 0.195 1.00 1 12/04/2023 03:09 WG2181973
Ethyl tert-butyl ether U 0.101 1.00 1 12/04/2023 03:09 WG2181973
tert-Butyl alcohol U 4.06 5.00 1 12/04/2023 03:09 WG2181973
t-Amyl Alcohol U 4.90 50.0 1 12/04/2023 03:09 WG2181973
tert-Butyl formate U C4 4.51 20.0 1 12/04/2023 19:19 WG2182350
(S) Toluene-d8 104 80.0-120 12/04/2023 03:09 WG2181973
(S) Toluene-d8 112 80.0-120 12/04/2023 19:19 WG2182350
(S) 4-Bromofluorobenzene 102 77.0-126 12/04/2023 03:09 WG2181973
(S) 4-Bromofluorobenzene 87.1 77.0-126 12/04/2023 19:19 WG2182350
(S) 1,2-Dichloroethane-d4 103 70.0-130 12/04/2023 03:09 WG2181973
(S) 1,2-Dichloroethane-d4 101 70.0-130 12/04/2023 19:19 WG2182350
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 33.8 B J 33.3 100 1 12/02/2023 09:32 WG2180752
Unadjusted C19-C36 Aliphatics 55.9 B J 33.3 100 1 12/02/2023 09:32 WG2180752
Unadjusted C11-C22 Aromatics 69.8 B J 33.3 100 1 12/02/2023 10:44 WG2180752
Unadjusted Total Petroleum
Hydrocarbons 160 33.3 100 1 12/02/2023 10:44 WG2180752
(S) o-Terphenyl 52.6 40.0-140 12/02/2023 10:44 WG2180752
(S) 1-Chloro-octadecane 18.2 J2 40.0-140 12/02/2023 09:32 WG2180752
(S) 2-Fluorobiphenyl 63.4 40.0-140 12/02/2023 10:44 WG2180752
(S) 2-Bromonaphthalene 57.9 40.0-140 12/02/2023 10:44 WG2180752
Sample Narrative:
L1682140-03 WG2180752: Sample produced emulsion during Extraction process, low surr/spike recoveries due to matrix.
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 12/02/2023 00:34 WG2181093
Acenaphthylene U 0.0921 1.00 1 12/02/2023 00:34 WG2181093
Anthracene U 0.0804 1.00 1 12/02/2023 00:34 WG2181093
Benzo(a)anthracene U 0.199 1.00 1 12/02/2023 00:34 WG2181093
Benzo(b)fluoranthene U 0.130 1.00 1 12/02/2023 00:34 WG2181093
Benzo(k)fluoranthene U 0.120 1.00 1 12/02/2023 00:34 WG2181093
Benzo(g,h,i)perylene U 0.121 1.00 1 12/02/2023 00:34 WG2181093
Benzo(a)pyrene U 0.0381 1.00 1 12/02/2023 00:34 WG2181093
Bis(2-chlorethoxy)methane U 0.116 10.0 1 12/02/2023 00:34 WG2181093
Bis(2-chloroethyl)ether U 0.137 10.0 1 12/02/2023 00:34 WG2181093
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 12/02/2023 00:34 WG2181093
4-Bromophenyl-phenylether U 0.0877 10.0 1 12/02/2023 00:34 WG2181093
2-Chloronaphthalene U 0.0648 1.00 1 12/02/2023 00:34 WG2181093
4-Chlorophenyl-phenylether U 0.0926 10.0 1 12/02/2023 00:34 WG2181093
Chrysene U 0.130 1.00 1 12/02/2023 00:34 WG2181093
Dibenz(a,h)anthracene U 0.0644 1.00 1 12/02/2023 00:34 WG2181093
3,3-Dichlorobenzidine U 0.212 10.0 1 12/02/2023 00:34 WG2181093
2,4-Dinitrotoluene U 0.0983 10.0 1 12/02/2023 00:34 WG2181093
2,6-Dinitrotoluene U 0.250 10.0 1 12/02/2023 00:34 WG2181093
Fluoranthene U 0.102 1.00 1 12/02/2023 00:34 WG2181093
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 13 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 13 of 44
SAMPLE RESULTS - 03
L1682140
MW-6
Collected date/time: 11/28/23 12:00
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Fluorene U 0.0844 1.00 1 12/02/2023 00:34 WG2181093
Hexachlorobenzene U 0.0755 1.00 1 12/02/2023 00:34 WG2181093
Hexachloro-1,3-butadiene U 0.0968 10.0 1 12/02/2023 00:34 WG2181093
Hexachlorocyclopentadiene U 0.0598 10.0 1 12/02/2023 00:34 WG2181093
Hexachloroethane U 0.127 10.0 1 12/02/2023 00:34 WG2181093
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 12/02/2023 00:34 WG2181093
Isophorone U 0.143 10.0 1 12/02/2023 00:34 WG2181093
Naphthalene U 0.159 1.00 1 12/02/2023 00:34 WG2181093
Nitrobenzene U 0.297 10.0 1 12/02/2023 00:34 WG2181093
n-Nitrosodimethylamine U 0.998 10.0 1 12/02/2023 00:34 WG2181093
n-Nitrosodiphenylamine U 2.37 10.0 1 12/02/2023 00:34 WG2181093
n-Nitrosodi-n-propylamine U 0.261 10.0 1 12/02/2023 00:34 WG2181093
Phenanthrene U 0.112 1.00 1 12/02/2023 00:34 WG2181093
Benzylbutyl phthalate U 0.765 3.00 1 12/02/2023 00:34 WG2181093
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 12/02/2023 00:34 WG2181093
Di-n-butyl phthalate U 0.453 3.00 1 12/02/2023 00:34 WG2181093
Diethyl phthalate U 0.287 3.00 1 12/02/2023 00:34 WG2181093
Dimethyl phthalate U 0.260 3.00 1 12/02/2023 00:34 WG2181093
Di-n-octyl phthalate U 0.932 3.00 1 12/02/2023 00:34 WG2181093
Pyrene U 0.107 1.00 1 12/02/2023 00:34 WG2181093
1,2,4-Trichlorobenzene U 0.0698 10.0 1 12/02/2023 00:34 WG2181093
4-Chloro-3-methylphenol U 0.131 10.0 1 12/02/2023 00:34 WG2181093
2-Chlorophenol U 0.133 10.0 1 12/02/2023 00:34 WG2181093
2,4-Dichlorophenol U 0.102 10.0 1 12/02/2023 00:34 WG2181093
2,4-Dimethylphenol U 0.0636 10.0 1 12/02/2023 00:34 WG2181093
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 12/02/2023 00:34 WG2181093
2,4-Dinitrophenol U 5.93 10.0 1 12/02/2023 00:34 WG2181093
2-Nitrophenol U 0.117 10.0 1 12/02/2023 00:34 WG2181093
4-Nitrophenol U 0.143 10.0 1 12/02/2023 00:34 WG2181093
Pentachlorophenol U 0.313 10.0 1 12/02/2023 00:34 WG2181093
Phenol U 4.33 10.0 1 12/02/2023 00:34 WG2181093
2,4,6-Trichlorophenol U 0.100 10.0 1 12/02/2023 00:34 WG2181093
(S) Nitrobenzene-d5 62.2 15.0-314 12/02/2023 00:34 WG2181093
(S) 2-Fluorobiphenyl 53.0 22.0-127 12/02/2023 00:34 WG2181093
(S) p-Terphenyl-d14 69.0 29.0-141 12/02/2023 00:34 WG2181093
(S) Phenol-d5 24.4 8.00-424 12/02/2023 00:34 WG2181093
(S) 2-Fluorophenol 33.3 10.0-120 12/02/2023 00:34 WG2181093
(S) 2,4,6-Tribromophenol 50.2 10.0-153 12/02/2023 00:34 WG2181093
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 14 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 14 of 44
SAMPLE RESULTS - 04
L1682140
MW-7
Collected date/time: 11/28/23 12:30
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.0941 1.00 1 12/04/2023 03:29 WG2181973
Bromobenzene U 0.118 1.00 1 12/04/2023 03:29 WG2181973
Bromodichloromethane U 0.136 1.00 1 12/04/2023 03:29 WG2181973
Bromochloromethane U 0.128 1.00 1 12/04/2023 03:29 WG2181973
Bromoform U 0.129 1.00 1 12/04/2023 03:29 WG2181973
Bromomethane U 0.605 5.00 1 12/04/2023 03:29 WG2181973
n-Butylbenzene U 0.157 1.00 1 12/04/2023 03:29 WG2181973
sec-Butylbenzene U 0.125 1.00 1 12/04/2023 03:29 WG2181973
tert-Butylbenzene U J4 0.127 1.00 1 12/04/2023 03:29 WG2181973
Carbon tetrachloride U 0.128 1.00 1 12/04/2023 03:29 WG2181973
Chlorobenzene U 0.116 1.00 1 12/04/2023 03:29 WG2181973
Chlorodibromomethane U 0.140 1.00 1 12/04/2023 03:29 WG2181973
Chloroethane U 0.192 5.00 1 12/04/2023 03:29 WG2181973
Chloroform U 0.111 5.00 1 12/04/2023 03:29 WG2181973
Chloromethane U 0.960 2.50 1 12/04/2023 03:29 WG2181973
2-Chlorotoluene U 0.106 1.00 1 12/04/2023 03:29 WG2181973
4-Chlorotoluene U 0.114 1.00 1 12/04/2023 03:29 WG2181973
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 12/04/2023 03:29 WG2181973
1,2-Dibromoethane U 0.126 1.00 1 12/04/2023 03:29 WG2181973
Dibromomethane U 0.122 1.00 1 12/04/2023 03:29 WG2181973
1,2-Dichlorobenzene U 0.107 1.00 1 12/04/2023 03:29 WG2181973
1,3-Dichlorobenzene U 0.110 1.00 1 12/04/2023 03:29 WG2181973
1,4-Dichlorobenzene U 0.120 1.00 1 12/04/2023 03:29 WG2181973
Dichlorodifluoromethane U 0.374 5.00 1 12/04/2023 03:29 WG2181973
1,1-Dichloroethane U 0.100 1.00 1 12/04/2023 03:29 WG2181973
1,2-Dichloroethane U 0.0819 1.00 1 12/04/2023 03:29 WG2181973
1,1-Dichloroethene U 0.188 1.00 1 12/04/2023 03:29 WG2181973
cis-1,2-Dichloroethene U 0.126 1.00 1 12/04/2023 03:29 WG2181973
trans-1,2-Dichloroethene U 0.149 1.00 1 12/04/2023 03:29 WG2181973
1,2-Dichloropropane U 0.149 1.00 1 12/04/2023 03:29 WG2181973
1,1-Dichloropropene U 0.142 1.00 1 12/04/2023 03:29 WG2181973
1,3-Dichloropropane U 0.110 1.00 1 12/04/2023 03:29 WG2181973
cis-1,3-Dichloropropene U 0.111 1.00 1 12/04/2023 03:29 WG2181973
trans-1,3-Dichloropropene U 0.118 1.00 1 12/04/2023 03:29 WG2181973
2,2-Dichloropropane U 0.161 1.00 1 12/04/2023 03:29 WG2181973
Di-isopropyl ether U 0.105 1.00 1 12/04/2023 03:29 WG2181973
Ethylbenzene U 0.137 1.00 1 12/04/2023 03:29 WG2181973
Hexachloro-1,3-butadiene U 0.337 1.00 1 12/04/2023 03:29 WG2181973
Isopropylbenzene U 0.105 1.00 1 12/04/2023 03:29 WG2181973
Methylene Chloride U 0.430 5.00 1 12/04/2023 03:29 WG2181973
Methyl tert-butyl ether U 0.101 1.00 1 12/04/2023 03:29 WG2181973
Naphthalene U 1.00 5.00 1 12/04/2023 03:29 WG2181973
n-Propylbenzene U 0.0993 1.00 1 12/04/2023 03:29 WG2181973
Styrene U 0.118 1.00 1 12/04/2023 03:29 WG2181973
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 12/04/2023 03:29 WG2181973
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 12/04/2023 03:29 WG2181973
Tetrachloroethene U 0.300 1.00 1 12/04/2023 03:29 WG2181973
Toluene U 0.278 1.00 1 12/04/2023 03:29 WG2181973
1,2,3-Trichlorobenzene U 0.230 1.00 1 12/04/2023 03:29 WG2181973
1,2,4-Trichlorobenzene U 0.481 1.00 1 12/04/2023 03:29 WG2181973
1,1,1-Trichloroethane U 0.149 1.00 1 12/04/2023 03:29 WG2181973
1,1,2-Trichloroethane U 0.158 1.00 1 12/04/2023 03:29 WG2181973
Trichloroethene U 0.190 1.00 1 12/04/2023 03:29 WG2181973
Trichlorofluoromethane U 0.160 5.00 1 12/04/2023 03:29 WG2181973
1,2,3-Trichloropropane U 0.237 2.50 1 12/04/2023 03:29 WG2181973
1,2,4-Trimethylbenzene U 0.322 1.00 1 12/04/2023 03:29 WG2181973
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 15 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 15 of 44
SAMPLE RESULTS - 04
L1682140
MW-7
Collected date/time: 11/28/23 12:30
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene U 0.104 1.00 1 12/04/2023 03:29 WG2181973
Vinyl chloride U 0.234 1.00 1 12/04/2023 03:29 WG2181973
o-Xylene U 0.174 1.00 1 12/04/2023 03:29 WG2181973
m&p-Xylenes U 0.430 2.00 1 12/04/2023 03:29 WG2181973
ethanol U C4 42.0 100 1 12/04/2023 19:40 WG2182350
tert-Amyl Methyl Ether U 0.195 1.00 1 12/04/2023 03:29 WG2181973
Ethyl tert-butyl ether U 0.101 1.00 1 12/04/2023 03:29 WG2181973
tert-Butyl alcohol U 4.06 5.00 1 12/04/2023 03:29 WG2181973
t-Amyl Alcohol U 4.90 50.0 1 12/04/2023 03:29 WG2181973
tert-Butyl formate U C4 4.51 20.0 1 12/04/2023 19:40 WG2182350
(S) Toluene-d8 105 80.0-120 12/04/2023 03:29 WG2181973
(S) Toluene-d8 115 80.0-120 12/04/2023 19:40 WG2182350
(S) 4-Bromofluorobenzene 94.9 77.0-126 12/04/2023 03:29 WG2181973
(S) 4-Bromofluorobenzene 88.7 77.0-126 12/04/2023 19:40 WG2182350
(S) 1,2-Dichloroethane-d4 97.6 70.0-130 12/04/2023 03:29 WG2181973
(S) 1,2-Dichloroethane-d4 104 70.0-130 12/04/2023 19:40 WG2182350
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 33.3 J 33.3 100 1 12/02/2023 09:56 WG2180752
Unadjusted C19-C36 Aliphatics 49.0 B J 33.3 100 1 12/02/2023 09:56 WG2180752
Unadjusted C11-C22 Aromatics 70.2 B J 33.3 100 1 12/02/2023 10:20 WG2180752
Unadjusted Total Petroleum
Hydrocarbons 153 33.3 100 1 12/02/2023 10:20 WG2180752
(S) o-Terphenyl 56.1 40.0-140 12/02/2023 10:20 WG2180752
(S) 1-Chloro-octadecane 20.9 J2 40.0-140 12/02/2023 09:56 WG2180752
(S) 2-Fluorobiphenyl 65.5 40.0-140 12/02/2023 10:20 WG2180752
(S) 2-Bromonaphthalene 59.5 40.0-140 12/02/2023 10:20 WG2180752
Sample Narrative:
L1682140-04 WG2180752: Sample produced emulsion during Extraction process, low surr/spike recoveries due to matrix.
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 12/02/2023 00:55 WG2181093
Acenaphthylene U 0.0921 1.00 1 12/02/2023 00:55 WG2181093
Anthracene U 0.0804 1.00 1 12/02/2023 00:55 WG2181093
Benzo(a)anthracene U 0.199 1.00 1 12/02/2023 00:55 WG2181093
Benzo(b)fluoranthene U 0.130 1.00 1 12/02/2023 00:55 WG2181093
Benzo(k)fluoranthene U 0.120 1.00 1 12/02/2023 00:55 WG2181093
Benzo(g,h,i)perylene U 0.121 1.00 1 12/02/2023 00:55 WG2181093
Benzo(a)pyrene U 0.0381 1.00 1 12/02/2023 00:55 WG2181093
Bis(2-chlorethoxy)methane U 0.116 10.0 1 12/02/2023 00:55 WG2181093
Bis(2-chloroethyl)ether U 0.137 10.0 1 12/02/2023 00:55 WG2181093
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 12/02/2023 00:55 WG2181093
4-Bromophenyl-phenylether U 0.0877 10.0 1 12/02/2023 00:55 WG2181093
2-Chloronaphthalene U 0.0648 1.00 1 12/02/2023 00:55 WG2181093
4-Chlorophenyl-phenylether U 0.0926 10.0 1 12/02/2023 00:55 WG2181093
Chrysene U 0.130 1.00 1 12/02/2023 00:55 WG2181093
Dibenz(a,h)anthracene U 0.0644 1.00 1 12/02/2023 00:55 WG2181093
3,3-Dichlorobenzidine U 0.212 10.0 1 12/02/2023 00:55 WG2181093
2,4-Dinitrotoluene U 0.0983 10.0 1 12/02/2023 00:55 WG2181093
2,6-Dinitrotoluene U 0.250 10.0 1 12/02/2023 00:55 WG2181093
Fluoranthene U 0.102 1.00 1 12/02/2023 00:55 WG2181093
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 16 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 16 of 44
SAMPLE RESULTS - 04
L1682140
MW-7
Collected date/time: 11/28/23 12:30
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Fluorene U 0.0844 1.00 1 12/02/2023 00:55 WG2181093
Hexachlorobenzene U 0.0755 1.00 1 12/02/2023 00:55 WG2181093
Hexachloro-1,3-butadiene U 0.0968 10.0 1 12/02/2023 00:55 WG2181093
Hexachlorocyclopentadiene U 0.0598 10.0 1 12/02/2023 00:55 WG2181093
Hexachloroethane U 0.127 10.0 1 12/02/2023 00:55 WG2181093
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 12/02/2023 00:55 WG2181093
Isophorone U 0.143 10.0 1 12/02/2023 00:55 WG2181093
Naphthalene U 0.159 1.00 1 12/02/2023 00:55 WG2181093
Nitrobenzene U 0.297 10.0 1 12/02/2023 00:55 WG2181093
n-Nitrosodimethylamine U 0.998 10.0 1 12/02/2023 00:55 WG2181093
n-Nitrosodiphenylamine U 2.37 10.0 1 12/02/2023 00:55 WG2181093
n-Nitrosodi-n-propylamine U 0.261 10.0 1 12/02/2023 00:55 WG2181093
Phenanthrene U 0.112 1.00 1 12/02/2023 00:55 WG2181093
Benzylbutyl phthalate U 0.765 3.00 1 12/02/2023 00:55 WG2181093
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 12/02/2023 00:55 WG2181093
Di-n-butyl phthalate U 0.453 3.00 1 12/02/2023 00:55 WG2181093
Diethyl phthalate U 0.287 3.00 1 12/02/2023 00:55 WG2181093
Dimethyl phthalate U 0.260 3.00 1 12/02/2023 00:55 WG2181093
Di-n-octyl phthalate U 0.932 3.00 1 12/02/2023 00:55 WG2181093
Pyrene U 0.107 1.00 1 12/02/2023 00:55 WG2181093
1,2,4-Trichlorobenzene U 0.0698 10.0 1 12/02/2023 00:55 WG2181093
4-Chloro-3-methylphenol U 0.131 10.0 1 12/02/2023 00:55 WG2181093
2-Chlorophenol U 0.133 10.0 1 12/02/2023 00:55 WG2181093
2,4-Dichlorophenol U 0.102 10.0 1 12/02/2023 00:55 WG2181093
2,4-Dimethylphenol U 0.0636 10.0 1 12/02/2023 00:55 WG2181093
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 12/02/2023 00:55 WG2181093
2,4-Dinitrophenol U 5.93 10.0 1 12/02/2023 00:55 WG2181093
2-Nitrophenol U 0.117 10.0 1 12/02/2023 00:55 WG2181093
4-Nitrophenol U 0.143 10.0 1 12/02/2023 00:55 WG2181093
Pentachlorophenol U 0.313 10.0 1 12/02/2023 00:55 WG2181093
Phenol U 4.33 10.0 1 12/02/2023 00:55 WG2181093
2,4,6-Trichlorophenol U 0.100 10.0 1 12/02/2023 00:55 WG2181093
(S) Nitrobenzene-d5 59.0 15.0-314 12/02/2023 00:55 WG2181093
(S) 2-Fluorobiphenyl 48.6 22.0-127 12/02/2023 00:55 WG2181093
(S) p-Terphenyl-d14 73.9 29.0-141 12/02/2023 00:55 WG2181093
(S) Phenol-d5 23.5 8.00-424 12/02/2023 00:55 WG2181093
(S) 2-Fluorophenol 29.7 10.0-120 12/02/2023 00:55 WG2181093
(S) 2,4,6-Tribromophenol 54.7 10.0-153 12/02/2023 00:55 WG2181093
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 17 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 17 of 44
SAMPLE RESULTS - 05
L1682140
MW-8
Collected date/time: 11/28/23 13:00
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.0941 1.00 1 12/04/2023 03:48 WG2181973
Bromobenzene U 0.118 1.00 1 12/04/2023 03:48 WG2181973
Bromodichloromethane U 0.136 1.00 1 12/04/2023 03:48 WG2181973
Bromochloromethane U 0.128 1.00 1 12/04/2023 03:48 WG2181973
Bromoform U 0.129 1.00 1 12/04/2023 03:48 WG2181973
Bromomethane U 0.605 5.00 1 12/04/2023 03:48 WG2181973
n-Butylbenzene U 0.157 1.00 1 12/04/2023 03:48 WG2181973
sec-Butylbenzene U 0.125 1.00 1 12/04/2023 03:48 WG2181973
tert-Butylbenzene U J4 0.127 1.00 1 12/04/2023 03:48 WG2181973
Carbon tetrachloride U 0.128 1.00 1 12/04/2023 03:48 WG2181973
Chlorobenzene U 0.116 1.00 1 12/04/2023 03:48 WG2181973
Chlorodibromomethane U 0.140 1.00 1 12/04/2023 03:48 WG2181973
Chloroethane U 0.192 5.00 1 12/04/2023 03:48 WG2181973
Chloroform U 0.111 5.00 1 12/04/2023 03:48 WG2181973
Chloromethane U 0.960 2.50 1 12/04/2023 03:48 WG2181973
2-Chlorotoluene U 0.106 1.00 1 12/04/2023 03:48 WG2181973
4-Chlorotoluene U 0.114 1.00 1 12/04/2023 03:48 WG2181973
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 12/04/2023 03:48 WG2181973
1,2-Dibromoethane U 0.126 1.00 1 12/04/2023 03:48 WG2181973
Dibromomethane U 0.122 1.00 1 12/04/2023 03:48 WG2181973
1,2-Dichlorobenzene U 0.107 1.00 1 12/04/2023 03:48 WG2181973
1,3-Dichlorobenzene U 0.110 1.00 1 12/04/2023 03:48 WG2181973
1,4-Dichlorobenzene U 0.120 1.00 1 12/04/2023 03:48 WG2181973
Dichlorodifluoromethane U 0.374 5.00 1 12/04/2023 03:48 WG2181973
1,1-Dichloroethane U 0.100 1.00 1 12/04/2023 03:48 WG2181973
1,2-Dichloroethane U 0.0819 1.00 1 12/04/2023 03:48 WG2181973
1,1-Dichloroethene U 0.188 1.00 1 12/04/2023 03:48 WG2181973
cis-1,2-Dichloroethene U 0.126 1.00 1 12/04/2023 03:48 WG2181973
trans-1,2-Dichloroethene U 0.149 1.00 1 12/04/2023 03:48 WG2181973
1,2-Dichloropropane U 0.149 1.00 1 12/04/2023 03:48 WG2181973
1,1-Dichloropropene U 0.142 1.00 1 12/04/2023 03:48 WG2181973
1,3-Dichloropropane U 0.110 1.00 1 12/04/2023 03:48 WG2181973
cis-1,3-Dichloropropene U 0.111 1.00 1 12/04/2023 03:48 WG2181973
trans-1,3-Dichloropropene U 0.118 1.00 1 12/04/2023 03:48 WG2181973
2,2-Dichloropropane U 0.161 1.00 1 12/04/2023 03:48 WG2181973
Di-isopropyl ether U 0.105 1.00 1 12/04/2023 03:48 WG2181973
Ethylbenzene U 0.137 1.00 1 12/04/2023 03:48 WG2181973
Hexachloro-1,3-butadiene U 0.337 1.00 1 12/04/2023 03:48 WG2181973
Isopropylbenzene U 0.105 1.00 1 12/04/2023 03:48 WG2181973
Methylene Chloride U 0.430 5.00 1 12/04/2023 03:48 WG2181973
Methyl tert-butyl ether 0.105 J 0.101 1.00 1 12/04/2023 03:48 WG2181973
Naphthalene U 1.00 5.00 1 12/04/2023 03:48 WG2181973
n-Propylbenzene U 0.0993 1.00 1 12/04/2023 03:48 WG2181973
Styrene U 0.118 1.00 1 12/04/2023 03:48 WG2181973
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 12/04/2023 03:48 WG2181973
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 12/04/2023 03:48 WG2181973
Tetrachloroethene U 0.300 1.00 1 12/04/2023 03:48 WG2181973
Toluene U 0.278 1.00 1 12/04/2023 03:48 WG2181973
1,2,3-Trichlorobenzene U 0.230 1.00 1 12/04/2023 03:48 WG2181973
1,2,4-Trichlorobenzene U 0.481 1.00 1 12/04/2023 03:48 WG2181973
1,1,1-Trichloroethane U 0.149 1.00 1 12/04/2023 03:48 WG2181973
1,1,2-Trichloroethane U 0.158 1.00 1 12/04/2023 03:48 WG2181973
Trichloroethene U 0.190 1.00 1 12/04/2023 03:48 WG2181973
Trichlorofluoromethane U 0.160 5.00 1 12/04/2023 03:48 WG2181973
1,2,3-Trichloropropane U 0.237 2.50 1 12/04/2023 03:48 WG2181973
1,2,4-Trimethylbenzene U 0.322 1.00 1 12/04/2023 03:48 WG2181973
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 18 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 18 of 44
SAMPLE RESULTS - 05
L1682140
MW-8
Collected date/time: 11/28/23 13:00
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene U 0.104 1.00 1 12/04/2023 03:48 WG2181973
Vinyl chloride U 0.234 1.00 1 12/04/2023 03:48 WG2181973
o-Xylene U 0.174 1.00 1 12/04/2023 03:48 WG2181973
m&p-Xylenes U 0.430 2.00 1 12/04/2023 03:48 WG2181973
ethanol U C4 42.0 100 1 12/04/2023 20:00 WG2182350
tert-Amyl Methyl Ether U 0.195 1.00 1 12/04/2023 03:48 WG2181973
Ethyl tert-butyl ether U 0.101 1.00 1 12/04/2023 03:48 WG2181973
tert-Butyl alcohol U 4.06 5.00 1 12/04/2023 03:48 WG2181973
t-Amyl Alcohol U 4.90 50.0 1 12/04/2023 03:48 WG2181973
tert-Butyl formate U C4 4.51 20.0 1 12/04/2023 20:00 WG2182350
(S) Toluene-d8 109 80.0-120 12/04/2023 03:48 WG2181973
(S) Toluene-d8 112 80.0-120 12/04/2023 20:00 WG2182350
(S) 4-Bromofluorobenzene 100 77.0-126 12/04/2023 03:48 WG2181973
(S) 4-Bromofluorobenzene 89.5 77.0-126 12/04/2023 20:00 WG2182350
(S) 1,2-Dichloroethane-d4 102 70.0-130 12/04/2023 03:48 WG2181973
(S) 1,2-Dichloroethane-d4 103 70.0-130 12/04/2023 20:00 WG2182350
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 37.8 B J 33.3 100 1 12/02/2023 15:55 WG2180752
Unadjusted C19-C36 Aliphatics 52.4 B J 33.3 100 1 12/02/2023 15:55 WG2180752
Unadjusted C11-C22 Aromatics 69.4 B J 33.3 100 1 12/02/2023 21:07 WG2180752
Unadjusted Total Petroleum
Hydrocarbons 160 33.3 100 1 12/02/2023 21:07 WG2180752
(S) o-Terphenyl 68.2 40.0-140 12/02/2023 21:07 WG2180752
(S) 1-Chloro-octadecane 35.5 J2 40.0-140 12/02/2023 15:55 WG2180752
(S) 2-Fluorobiphenyl 75.0 40.0-140 12/02/2023 21:07 WG2180752
(S) 2-Bromonaphthalene 68.4 40.0-140 12/02/2023 21:07 WG2180752
Sample Narrative:
L1682140-05 WG2180752: Sample produced emulsion during Extraction process, low surr/spike recoveries due to matrix.
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 12/02/2023 01:16 WG2181093
Acenaphthylene U 0.0921 1.00 1 12/02/2023 01:16 WG2181093
Anthracene U 0.0804 1.00 1 12/02/2023 01:16 WG2181093
Benzo(a)anthracene U 0.199 1.00 1 12/02/2023 01:16 WG2181093
Benzo(b)fluoranthene U 0.130 1.00 1 12/02/2023 01:16 WG2181093
Benzo(k)fluoranthene U 0.120 1.00 1 12/02/2023 01:16 WG2181093
Benzo(g,h,i)perylene U 0.121 1.00 1 12/02/2023 01:16 WG2181093
Benzo(a)pyrene U 0.0381 1.00 1 12/02/2023 01:16 WG2181093
Bis(2-chlorethoxy)methane U 0.116 10.0 1 12/02/2023 01:16 WG2181093
Bis(2-chloroethyl)ether U 0.137 10.0 1 12/02/2023 01:16 WG2181093
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 12/02/2023 01:16 WG2181093
4-Bromophenyl-phenylether U 0.0877 10.0 1 12/02/2023 01:16 WG2181093
2-Chloronaphthalene U 0.0648 1.00 1 12/02/2023 01:16 WG2181093
4-Chlorophenyl-phenylether U 0.0926 10.0 1 12/02/2023 01:16 WG2181093
Chrysene U 0.130 1.00 1 12/02/2023 01:16 WG2181093
Dibenz(a,h)anthracene U 0.0644 1.00 1 12/02/2023 01:16 WG2181093
3,3-Dichlorobenzidine U 0.212 10.0 1 12/02/2023 01:16 WG2181093
2,4-Dinitrotoluene U 0.0983 10.0 1 12/02/2023 01:16 WG2181093
2,6-Dinitrotoluene U 0.250 10.0 1 12/02/2023 01:16 WG2181093
Fluoranthene U 0.102 1.00 1 12/02/2023 01:16 WG2181093
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 19 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 19 of 44
SAMPLE RESULTS - 05
L1682140
MW-8
Collected date/time: 11/28/23 13:00
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Fluorene U 0.0844 1.00 1 12/02/2023 01:16 WG2181093
Hexachlorobenzene U 0.0755 1.00 1 12/02/2023 01:16 WG2181093
Hexachloro-1,3-butadiene U 0.0968 10.0 1 12/02/2023 01:16 WG2181093
Hexachlorocyclopentadiene U 0.0598 10.0 1 12/02/2023 01:16 WG2181093
Hexachloroethane U 0.127 10.0 1 12/02/2023 01:16 WG2181093
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 12/02/2023 01:16 WG2181093
Isophorone U 0.143 10.0 1 12/02/2023 01:16 WG2181093
Naphthalene U 0.159 1.00 1 12/02/2023 01:16 WG2181093
Nitrobenzene U 0.297 10.0 1 12/02/2023 01:16 WG2181093
n-Nitrosodimethylamine U 0.998 10.0 1 12/02/2023 01:16 WG2181093
n-Nitrosodiphenylamine U 2.37 10.0 1 12/02/2023 01:16 WG2181093
n-Nitrosodi-n-propylamine U 0.261 10.0 1 12/02/2023 01:16 WG2181093
Phenanthrene U 0.112 1.00 1 12/02/2023 01:16 WG2181093
Benzylbutyl phthalate U 0.765 3.00 1 12/02/2023 01:16 WG2181093
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 12/02/2023 01:16 WG2181093
Di-n-butyl phthalate U 0.453 3.00 1 12/02/2023 01:16 WG2181093
Diethyl phthalate U 0.287 3.00 1 12/02/2023 01:16 WG2181093
Dimethyl phthalate U 0.260 3.00 1 12/02/2023 01:16 WG2181093
Di-n-octyl phthalate U 0.932 3.00 1 12/02/2023 01:16 WG2181093
Pyrene U 0.107 1.00 1 12/02/2023 01:16 WG2181093
1,2,4-Trichlorobenzene U 0.0698 10.0 1 12/02/2023 01:16 WG2181093
4-Chloro-3-methylphenol U 0.131 10.0 1 12/02/2023 01:16 WG2181093
2-Chlorophenol U 0.133 10.0 1 12/02/2023 01:16 WG2181093
2,4-Dichlorophenol U 0.102 10.0 1 12/02/2023 01:16 WG2181093
2,4-Dimethylphenol U 0.0636 10.0 1 12/02/2023 01:16 WG2181093
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 12/02/2023 01:16 WG2181093
2,4-Dinitrophenol U 5.93 10.0 1 12/02/2023 01:16 WG2181093
2-Nitrophenol U 0.117 10.0 1 12/02/2023 01:16 WG2181093
4-Nitrophenol U 0.143 10.0 1 12/02/2023 01:16 WG2181093
Pentachlorophenol U 0.313 10.0 1 12/02/2023 01:16 WG2181093
Phenol U 4.33 10.0 1 12/02/2023 01:16 WG2181093
2,4,6-Trichlorophenol U 0.100 10.0 1 12/02/2023 01:16 WG2181093
(S) Nitrobenzene-d5 62.6 15.0-314 12/02/2023 01:16 WG2181093
(S) 2-Fluorobiphenyl 53.5 22.0-127 12/02/2023 01:16 WG2181093
(S) p-Terphenyl-d14 67.2 29.0-141 12/02/2023 01:16 WG2181093
(S) Phenol-d5 22.4 8.00-424 12/02/2023 01:16 WG2181093
(S) 2-Fluorophenol 29.1 10.0-120 12/02/2023 01:16 WG2181093
(S) 2,4,6-Tribromophenol 52.2 10.0-153 12/02/2023 01:16 WG2181093
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 20 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 20 of 44
SAMPLE RESULTS - 06
L1682140
MW-9
Collected date/time: 11/28/23 12:40
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.0941 1.00 1 12/04/2023 04:08 WG2181973
Bromobenzene U 0.118 1.00 1 12/04/2023 04:08 WG2181973
Bromodichloromethane U 0.136 1.00 1 12/04/2023 04:08 WG2181973
Bromochloromethane U 0.128 1.00 1 12/04/2023 04:08 WG2181973
Bromoform U 0.129 1.00 1 12/04/2023 04:08 WG2181973
Bromomethane U 0.605 5.00 1 12/04/2023 04:08 WG2181973
n-Butylbenzene U 0.157 1.00 1 12/04/2023 04:08 WG2181973
sec-Butylbenzene U 0.125 1.00 1 12/04/2023 04:08 WG2181973
tert-Butylbenzene U J4 0.127 1.00 1 12/04/2023 04:08 WG2181973
Carbon tetrachloride U 0.128 1.00 1 12/04/2023 04:08 WG2181973
Chlorobenzene U 0.116 1.00 1 12/04/2023 04:08 WG2181973
Chlorodibromomethane U 0.140 1.00 1 12/04/2023 04:08 WG2181973
Chloroethane U 0.192 5.00 1 12/04/2023 04:08 WG2181973
Chloroform U 0.111 5.00 1 12/04/2023 04:08 WG2181973
Chloromethane U 0.960 2.50 1 12/04/2023 04:08 WG2181973
2-Chlorotoluene U 0.106 1.00 1 12/04/2023 04:08 WG2181973
4-Chlorotoluene U 0.114 1.00 1 12/04/2023 04:08 WG2181973
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 12/04/2023 04:08 WG2181973
1,2-Dibromoethane U 0.126 1.00 1 12/04/2023 04:08 WG2181973
Dibromomethane U 0.122 1.00 1 12/04/2023 04:08 WG2181973
1,2-Dichlorobenzene U 0.107 1.00 1 12/04/2023 04:08 WG2181973
1,3-Dichlorobenzene U 0.110 1.00 1 12/04/2023 04:08 WG2181973
1,4-Dichlorobenzene U 0.120 1.00 1 12/04/2023 04:08 WG2181973
Dichlorodifluoromethane U 0.374 5.00 1 12/04/2023 04:08 WG2181973
1,1-Dichloroethane U 0.100 1.00 1 12/04/2023 04:08 WG2181973
1,2-Dichloroethane U 0.0819 1.00 1 12/04/2023 04:08 WG2181973
1,1-Dichloroethene U 0.188 1.00 1 12/04/2023 04:08 WG2181973
cis-1,2-Dichloroethene U 0.126 1.00 1 12/04/2023 04:08 WG2181973
trans-1,2-Dichloroethene U 0.149 1.00 1 12/04/2023 04:08 WG2181973
1,2-Dichloropropane U 0.149 1.00 1 12/04/2023 04:08 WG2181973
1,1-Dichloropropene U 0.142 1.00 1 12/04/2023 04:08 WG2181973
1,3-Dichloropropane U 0.110 1.00 1 12/04/2023 04:08 WG2181973
cis-1,3-Dichloropropene U 0.111 1.00 1 12/04/2023 04:08 WG2181973
trans-1,3-Dichloropropene U 0.118 1.00 1 12/04/2023 04:08 WG2181973
2,2-Dichloropropane U 0.161 1.00 1 12/04/2023 04:08 WG2181973
Di-isopropyl ether U 0.105 1.00 1 12/04/2023 04:08 WG2181973
Ethylbenzene U 0.137 1.00 1 12/04/2023 04:08 WG2181973
Hexachloro-1,3-butadiene U 0.337 1.00 1 12/04/2023 04:08 WG2181973
Isopropylbenzene U 0.105 1.00 1 12/04/2023 04:08 WG2181973
Methylene Chloride U 0.430 5.00 1 12/04/2023 04:08 WG2181973
Methyl tert-butyl ether U 0.101 1.00 1 12/04/2023 04:08 WG2181973
Naphthalene U 1.00 5.00 1 12/04/2023 04:08 WG2181973
n-Propylbenzene U 0.0993 1.00 1 12/04/2023 04:08 WG2181973
Styrene U 0.118 1.00 1 12/04/2023 04:08 WG2181973
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 12/04/2023 04:08 WG2181973
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 12/04/2023 04:08 WG2181973
Tetrachloroethene U 0.300 1.00 1 12/04/2023 04:08 WG2181973
Toluene U 0.278 1.00 1 12/04/2023 04:08 WG2181973
1,2,3-Trichlorobenzene U 0.230 1.00 1 12/04/2023 04:08 WG2181973
1,2,4-Trichlorobenzene U 0.481 1.00 1 12/04/2023 04:08 WG2181973
1,1,1-Trichloroethane U 0.149 1.00 1 12/04/2023 04:08 WG2181973
1,1,2-Trichloroethane U 0.158 1.00 1 12/04/2023 04:08 WG2181973
Trichloroethene U 0.190 1.00 1 12/04/2023 04:08 WG2181973
Trichlorofluoromethane U 0.160 5.00 1 12/04/2023 04:08 WG2181973
1,2,3-Trichloropropane U 0.237 2.50 1 12/04/2023 04:08 WG2181973
1,2,4-Trimethylbenzene U 0.322 1.00 1 12/04/2023 04:08 WG2181973
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 21 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 21 of 44
SAMPLE RESULTS - 06
L1682140
MW-9
Collected date/time: 11/28/23 12:40
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene U 0.104 1.00 1 12/04/2023 04:08 WG2181973
Vinyl chloride U 0.234 1.00 1 12/04/2023 04:08 WG2181973
o-Xylene U 0.174 1.00 1 12/04/2023 04:08 WG2181973
m&p-Xylenes U 0.430 2.00 1 12/04/2023 04:08 WG2181973
ethanol U C4 42.0 100 1 12/04/2023 20:21 WG2182350
tert-Amyl Methyl Ether U 0.195 1.00 1 12/04/2023 04:08 WG2181973
Ethyl tert-butyl ether U 0.101 1.00 1 12/04/2023 04:08 WG2181973
tert-Butyl alcohol U 4.06 5.00 1 12/04/2023 04:08 WG2181973
t-Amyl Alcohol U 4.90 50.0 1 12/04/2023 04:08 WG2181973
tert-Butyl formate U C4 4.51 20.0 1 12/04/2023 20:21 WG2182350
(S) Toluene-d8 101 80.0-120 12/04/2023 04:08 WG2181973
(S) Toluene-d8 113 80.0-120 12/04/2023 20:21 WG2182350
(S) 4-Bromofluorobenzene 97.6 77.0-126 12/04/2023 04:08 WG2181973
(S) 4-Bromofluorobenzene 87.4 77.0-126 12/04/2023 20:21 WG2182350
(S) 1,2-Dichloroethane-d4 106 70.0-130 12/04/2023 04:08 WG2181973
(S) 1,2-Dichloroethane-d4 99.7 70.0-130 12/04/2023 20:21 WG2182350
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 36.4 B J 33.3 100 1 12/02/2023 16:19 WG2180752
Unadjusted C19-C36 Aliphatics 56.8 B J 33.3 100 1 12/02/2023 16:19 WG2180752
Unadjusted C11-C22 Aromatics 71.5 B J 33.3 100 1 12/02/2023 20:43 WG2180752
Unadjusted Total Petroleum
Hydrocarbons 165 33.3 100 1 12/02/2023 20:43 WG2180752
(S) o-Terphenyl 63.7 40.0-140 12/02/2023 20:43 WG2180752
(S) 1-Chloro-octadecane 26.8 J2 40.0-140 12/02/2023 16:19 WG2180752
(S) 2-Fluorobiphenyl 69.5 40.0-140 12/02/2023 20:43 WG2180752
(S) 2-Bromonaphthalene 68.9 40.0-140 12/02/2023 20:43 WG2180752
Sample Narrative:
L1682140-06 WG2180752: Sample produced emulsion during Extraction process, low surr/spike recoveries due to matrix.
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 12/02/2023 01:37 WG2181093
Acenaphthylene U 0.0921 1.00 1 12/02/2023 01:37 WG2181093
Anthracene U 0.0804 1.00 1 12/02/2023 01:37 WG2181093
Benzo(a)anthracene U 0.199 1.00 1 12/02/2023 01:37 WG2181093
Benzo(b)fluoranthene U 0.130 1.00 1 12/02/2023 01:37 WG2181093
Benzo(k)fluoranthene U 0.120 1.00 1 12/02/2023 01:37 WG2181093
Benzo(g,h,i)perylene U 0.121 1.00 1 12/02/2023 01:37 WG2181093
Benzo(a)pyrene U 0.0381 1.00 1 12/02/2023 01:37 WG2181093
Bis(2-chlorethoxy)methane U 0.116 10.0 1 12/02/2023 01:37 WG2181093
Bis(2-chloroethyl)ether U 0.137 10.0 1 12/02/2023 01:37 WG2181093
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 12/02/2023 01:37 WG2181093
4-Bromophenyl-phenylether U 0.0877 10.0 1 12/02/2023 01:37 WG2181093
2-Chloronaphthalene U 0.0648 1.00 1 12/02/2023 01:37 WG2181093
4-Chlorophenyl-phenylether U 0.0926 10.0 1 12/02/2023 01:37 WG2181093
Chrysene U 0.130 1.00 1 12/02/2023 01:37 WG2181093
Dibenz(a,h)anthracene U 0.0644 1.00 1 12/02/2023 01:37 WG2181093
3,3-Dichlorobenzidine U 0.212 10.0 1 12/02/2023 01:37 WG2181093
2,4-Dinitrotoluene U 0.0983 10.0 1 12/02/2023 01:37 WG2181093
2,6-Dinitrotoluene U 0.250 10.0 1 12/02/2023 01:37 WG2181093
Fluoranthene U 0.102 1.00 1 12/02/2023 01:37 WG2181093
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 22 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 22 of 44
SAMPLE RESULTS - 06
L1682140
MW-9
Collected date/time: 11/28/23 12:40
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Fluorene U 0.0844 1.00 1 12/02/2023 01:37 WG2181093
Hexachlorobenzene U 0.0755 1.00 1 12/02/2023 01:37 WG2181093
Hexachloro-1,3-butadiene U 0.0968 10.0 1 12/02/2023 01:37 WG2181093
Hexachlorocyclopentadiene U 0.0598 10.0 1 12/02/2023 01:37 WG2181093
Hexachloroethane U 0.127 10.0 1 12/02/2023 01:37 WG2181093
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 12/02/2023 01:37 WG2181093
Isophorone U 0.143 10.0 1 12/02/2023 01:37 WG2181093
Naphthalene U 0.159 1.00 1 12/02/2023 01:37 WG2181093
Nitrobenzene U 0.297 10.0 1 12/02/2023 01:37 WG2181093
n-Nitrosodimethylamine U 0.998 10.0 1 12/02/2023 01:37 WG2181093
n-Nitrosodiphenylamine U 2.37 10.0 1 12/02/2023 01:37 WG2181093
n-Nitrosodi-n-propylamine U 0.261 10.0 1 12/02/2023 01:37 WG2181093
Phenanthrene U 0.112 1.00 1 12/02/2023 01:37 WG2181093
Benzylbutyl phthalate U 0.765 3.00 1 12/02/2023 01:37 WG2181093
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 12/02/2023 01:37 WG2181093
Di-n-butyl phthalate U 0.453 3.00 1 12/02/2023 01:37 WG2181093
Diethyl phthalate U 0.287 3.00 1 12/02/2023 01:37 WG2181093
Dimethyl phthalate U 0.260 3.00 1 12/02/2023 01:37 WG2181093
Di-n-octyl phthalate U 0.932 3.00 1 12/02/2023 01:37 WG2181093
Pyrene U 0.107 1.00 1 12/02/2023 01:37 WG2181093
1,2,4-Trichlorobenzene U 0.0698 10.0 1 12/02/2023 01:37 WG2181093
4-Chloro-3-methylphenol U 0.131 10.0 1 12/02/2023 01:37 WG2181093
2-Chlorophenol U 0.133 10.0 1 12/02/2023 01:37 WG2181093
2,4-Dichlorophenol U 0.102 10.0 1 12/02/2023 01:37 WG2181093
2,4-Dimethylphenol U 0.0636 10.0 1 12/02/2023 01:37 WG2181093
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 12/02/2023 01:37 WG2181093
2,4-Dinitrophenol U 5.93 10.0 1 12/02/2023 01:37 WG2181093
2-Nitrophenol U 0.117 10.0 1 12/02/2023 01:37 WG2181093
4-Nitrophenol U 0.143 10.0 1 12/02/2023 01:37 WG2181093
Pentachlorophenol U 0.313 10.0 1 12/02/2023 01:37 WG2181093
Phenol U 4.33 10.0 1 12/02/2023 01:37 WG2181093
2,4,6-Trichlorophenol U 0.100 10.0 1 12/02/2023 01:37 WG2181093
(S) Nitrobenzene-d5 54.1 15.0-314 12/02/2023 01:37 WG2181093
(S) 2-Fluorobiphenyl 43.9 22.0-127 12/02/2023 01:37 WG2181093
(S) p-Terphenyl-d14 71.6 29.0-141 12/02/2023 01:37 WG2181093
(S) Phenol-d5 25.2 8.00-424 12/02/2023 01:37 WG2181093
(S) 2-Fluorophenol 31.3 10.0-120 12/02/2023 01:37 WG2181093
(S) 2,4,6-Tribromophenol 55.7 10.0-153 12/02/2023 01:37 WG2181093
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 23 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 23 of 44
SAMPLE RESULTS - 07
L1682140
MW-12
Collected date/time: 11/28/23 11:25
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.0941 1.00 1 12/04/2023 04:28 WG2181973
Bromobenzene U 0.118 1.00 1 12/04/2023 04:28 WG2181973
Bromodichloromethane U 0.136 1.00 1 12/04/2023 04:28 WG2181973
Bromochloromethane U 0.128 1.00 1 12/04/2023 04:28 WG2181973
Bromoform U 0.129 1.00 1 12/04/2023 04:28 WG2181973
Bromomethane U 0.605 5.00 1 12/04/2023 04:28 WG2181973
n-Butylbenzene U 0.157 1.00 1 12/04/2023 04:28 WG2181973
sec-Butylbenzene U 0.125 1.00 1 12/04/2023 04:28 WG2181973
tert-Butylbenzene U J4 0.127 1.00 1 12/04/2023 04:28 WG2181973
Carbon tetrachloride U 0.128 1.00 1 12/04/2023 04:28 WG2181973
Chlorobenzene U 0.116 1.00 1 12/04/2023 04:28 WG2181973
Chlorodibromomethane U 0.140 1.00 1 12/04/2023 04:28 WG2181973
Chloroethane U 0.192 5.00 1 12/04/2023 04:28 WG2181973
Chloroform U 0.111 5.00 1 12/04/2023 04:28 WG2181973
Chloromethane U 0.960 2.50 1 12/04/2023 04:28 WG2181973
2-Chlorotoluene U 0.106 1.00 1 12/04/2023 04:28 WG2181973
4-Chlorotoluene U 0.114 1.00 1 12/04/2023 04:28 WG2181973
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 12/04/2023 04:28 WG2181973
1,2-Dibromoethane U 0.126 1.00 1 12/04/2023 04:28 WG2181973
Dibromomethane U 0.122 1.00 1 12/04/2023 04:28 WG2181973
1,2-Dichlorobenzene U 0.107 1.00 1 12/04/2023 04:28 WG2181973
1,3-Dichlorobenzene U 0.110 1.00 1 12/04/2023 04:28 WG2181973
1,4-Dichlorobenzene U 0.120 1.00 1 12/04/2023 04:28 WG2181973
Dichlorodifluoromethane U 0.374 5.00 1 12/04/2023 04:28 WG2181973
1,1-Dichloroethane U 0.100 1.00 1 12/04/2023 04:28 WG2181973
1,2-Dichloroethane U 0.0819 1.00 1 12/04/2023 04:28 WG2181973
1,1-Dichloroethene U 0.188 1.00 1 12/04/2023 04:28 WG2181973
cis-1,2-Dichloroethene U 0.126 1.00 1 12/04/2023 04:28 WG2181973
trans-1,2-Dichloroethene U 0.149 1.00 1 12/04/2023 04:28 WG2181973
1,2-Dichloropropane U 0.149 1.00 1 12/04/2023 04:28 WG2181973
1,1-Dichloropropene U 0.142 1.00 1 12/04/2023 04:28 WG2181973
1,3-Dichloropropane U 0.110 1.00 1 12/04/2023 04:28 WG2181973
cis-1,3-Dichloropropene U 0.111 1.00 1 12/04/2023 04:28 WG2181973
trans-1,3-Dichloropropene U 0.118 1.00 1 12/04/2023 04:28 WG2181973
2,2-Dichloropropane U 0.161 1.00 1 12/04/2023 04:28 WG2181973
Di-isopropyl ether U 0.105 1.00 1 12/04/2023 04:28 WG2181973
Ethylbenzene U 0.137 1.00 1 12/04/2023 04:28 WG2181973
Hexachloro-1,3-butadiene U 0.337 1.00 1 12/04/2023 04:28 WG2181973
Isopropylbenzene U 0.105 1.00 1 12/04/2023 04:28 WG2181973
Methylene Chloride U 0.430 5.00 1 12/04/2023 04:28 WG2181973
Methyl tert-butyl ether U 0.101 1.00 1 12/04/2023 04:28 WG2181973
Naphthalene U 1.00 5.00 1 12/04/2023 04:28 WG2181973
n-Propylbenzene U 0.0993 1.00 1 12/04/2023 04:28 WG2181973
Styrene U 0.118 1.00 1 12/04/2023 04:28 WG2181973
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 12/04/2023 04:28 WG2181973
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 12/04/2023 04:28 WG2181973
Tetrachloroethene U 0.300 1.00 1 12/04/2023 04:28 WG2181973
Toluene U 0.278 1.00 1 12/04/2023 04:28 WG2181973
1,2,3-Trichlorobenzene U 0.230 1.00 1 12/04/2023 04:28 WG2181973
1,2,4-Trichlorobenzene U 0.481 1.00 1 12/04/2023 04:28 WG2181973
1,1,1-Trichloroethane U 0.149 1.00 1 12/04/2023 04:28 WG2181973
1,1,2-Trichloroethane U 0.158 1.00 1 12/04/2023 04:28 WG2181973
Trichloroethene U 0.190 1.00 1 12/04/2023 04:28 WG2181973
Trichlorofluoromethane U 0.160 5.00 1 12/04/2023 04:28 WG2181973
1,2,3-Trichloropropane U 0.237 2.50 1 12/04/2023 04:28 WG2181973
1,2,4-Trimethylbenzene U 0.322 1.00 1 12/04/2023 04:28 WG2181973
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 24 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 24 of 44
SAMPLE RESULTS - 07
L1682140
MW-12
Collected date/time: 11/28/23 11:25
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene U 0.104 1.00 1 12/04/2023 04:28 WG2181973
Vinyl chloride U 0.234 1.00 1 12/04/2023 04:28 WG2181973
o-Xylene U 0.174 1.00 1 12/04/2023 04:28 WG2181973
m&p-Xylenes U 0.430 2.00 1 12/04/2023 04:28 WG2181973
ethanol U C4 42.0 100 1 12/04/2023 20:42 WG2182350
tert-Amyl Methyl Ether U 0.195 1.00 1 12/04/2023 04:28 WG2181973
Ethyl tert-butyl ether U 0.101 1.00 1 12/04/2023 04:28 WG2181973
tert-Butyl alcohol U 4.06 5.00 1 12/04/2023 04:28 WG2181973
t-Amyl Alcohol U 4.90 50.0 1 12/04/2023 04:28 WG2181973
tert-Butyl formate U C4 4.51 20.0 1 12/04/2023 20:42 WG2182350
(S) Toluene-d8 101 80.0-120 12/04/2023 04:28 WG2181973
(S) Toluene-d8 110 80.0-120 12/04/2023 20:42 WG2182350
(S) 4-Bromofluorobenzene 89.6 77.0-126 12/04/2023 04:28 WG2181973
(S) 4-Bromofluorobenzene 85.6 77.0-126 12/04/2023 20:42 WG2182350
(S) 1,2-Dichloroethane-d4 97.4 70.0-130 12/04/2023 04:28 WG2181973
(S) 1,2-Dichloroethane-d4 99.9 70.0-130 12/04/2023 20:42 WG2182350
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 33.8 B J 33.3 100 1 12/02/2023 16:43 WG2180752
Unadjusted C19-C36 Aliphatics 51.7 B J 33.3 100 1 12/02/2023 16:43 WG2180752
Unadjusted C11-C22 Aromatics 68.5 B J 33.3 100 1 12/02/2023 20:19 WG2180752
Unadjusted Total Petroleum
Hydrocarbons 154 33.3 100 1 12/02/2023 20:19 WG2180752
(S) o-Terphenyl 63.4 40.0-140 12/02/2023 20:19 WG2180752
(S) 1-Chloro-octadecane 47.1 40.0-140 12/02/2023 16:43 WG2180752
(S) 2-Fluorobiphenyl 74.2 40.0-140 12/02/2023 20:19 WG2180752
(S) 2-Bromonaphthalene 67.4 40.0-140 12/02/2023 20:19 WG2180752
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 12/02/2023 01:58 WG2181093
Acenaphthylene U 0.0921 1.00 1 12/02/2023 01:58 WG2181093
Anthracene U 0.0804 1.00 1 12/02/2023 01:58 WG2181093
Benzo(a)anthracene U 0.199 1.00 1 12/02/2023 01:58 WG2181093
Benzo(b)fluoranthene U 0.130 1.00 1 12/02/2023 01:58 WG2181093
Benzo(k)fluoranthene U 0.120 1.00 1 12/02/2023 01:58 WG2181093
Benzo(g,h,i)perylene U 0.121 1.00 1 12/02/2023 01:58 WG2181093
Benzo(a)pyrene U 0.0381 1.00 1 12/02/2023 01:58 WG2181093
Bis(2-chlorethoxy)methane U 0.116 10.0 1 12/02/2023 01:58 WG2181093
Bis(2-chloroethyl)ether U 0.137 10.0 1 12/02/2023 01:58 WG2181093
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 12/02/2023 01:58 WG2181093
4-Bromophenyl-phenylether U 0.0877 10.0 1 12/02/2023 01:58 WG2181093
2-Chloronaphthalene U 0.0648 1.00 1 12/02/2023 01:58 WG2181093
4-Chlorophenyl-phenylether U 0.0926 10.0 1 12/02/2023 01:58 WG2181093
Chrysene U 0.130 1.00 1 12/02/2023 01:58 WG2181093
Dibenz(a,h)anthracene U 0.0644 1.00 1 12/02/2023 01:58 WG2181093
3,3-Dichlorobenzidine U 0.212 10.0 1 12/02/2023 01:58 WG2181093
2,4-Dinitrotoluene U 0.0983 10.0 1 12/02/2023 01:58 WG2181093
2,6-Dinitrotoluene U 0.250 10.0 1 12/02/2023 01:58 WG2181093
Fluoranthene U 0.102 1.00 1 12/02/2023 01:58 WG2181093
Fluorene U 0.0844 1.00 1 12/02/2023 01:58 WG2181093
Hexachlorobenzene U 0.0755 1.00 1 12/02/2023 01:58 WG2181093
Hexachloro-1,3-butadiene U 0.0968 10.0 1 12/02/2023 01:58 WG2181093
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 25 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 25 of 44
SAMPLE RESULTS - 07
L1682140
MW-12
Collected date/time: 11/28/23 11:25
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexachlorocyclopentadiene U 0.0598 10.0 1 12/02/2023 01:58 WG2181093
Hexachloroethane U 0.127 10.0 1 12/02/2023 01:58 WG2181093
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 12/02/2023 01:58 WG2181093
Isophorone U 0.143 10.0 1 12/02/2023 01:58 WG2181093
Naphthalene U 0.159 1.00 1 12/02/2023 01:58 WG2181093
Nitrobenzene U 0.297 10.0 1 12/02/2023 01:58 WG2181093
n-Nitrosodimethylamine U 0.998 10.0 1 12/02/2023 01:58 WG2181093
n-Nitrosodiphenylamine U 2.37 10.0 1 12/02/2023 01:58 WG2181093
n-Nitrosodi-n-propylamine U 0.261 10.0 1 12/02/2023 01:58 WG2181093
Phenanthrene U 0.112 1.00 1 12/02/2023 01:58 WG2181093
Benzylbutyl phthalate U 0.765 3.00 1 12/02/2023 01:58 WG2181093
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 12/02/2023 01:58 WG2181093
Di-n-butyl phthalate U 0.453 3.00 1 12/02/2023 01:58 WG2181093
Diethyl phthalate U 0.287 3.00 1 12/02/2023 01:58 WG2181093
Dimethyl phthalate U 0.260 3.00 1 12/02/2023 01:58 WG2181093
Di-n-octyl phthalate U 0.932 3.00 1 12/02/2023 01:58 WG2181093
Pyrene U 0.107 1.00 1 12/02/2023 01:58 WG2181093
1,2,4-Trichlorobenzene U 0.0698 10.0 1 12/02/2023 01:58 WG2181093
4-Chloro-3-methylphenol U 0.131 10.0 1 12/02/2023 01:58 WG2181093
2-Chlorophenol U 0.133 10.0 1 12/02/2023 01:58 WG2181093
2,4-Dichlorophenol U 0.102 10.0 1 12/02/2023 01:58 WG2181093
2,4-Dimethylphenol U 0.0636 10.0 1 12/02/2023 01:58 WG2181093
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 12/02/2023 01:58 WG2181093
2,4-Dinitrophenol U 5.93 10.0 1 12/02/2023 01:58 WG2181093
2-Nitrophenol U 0.117 10.0 1 12/02/2023 01:58 WG2181093
4-Nitrophenol U 0.143 10.0 1 12/02/2023 01:58 WG2181093
Pentachlorophenol U 0.313 10.0 1 12/02/2023 01:58 WG2181093
Phenol U 4.33 10.0 1 12/02/2023 01:58 WG2181093
2,4,6-Trichlorophenol U 0.100 10.0 1 12/02/2023 01:58 WG2181093
(S) Nitrobenzene-d5 48.8 15.0-314 12/02/2023 01:58 WG2181093
(S) 2-Fluorobiphenyl 42.9 22.0-127 12/02/2023 01:58 WG2181093
(S) p-Terphenyl-d14 67.2 29.0-141 12/02/2023 01:58 WG2181093
(S) Phenol-d5 16.6 8.00-424 12/02/2023 01:58 WG2181093
(S) 2-Fluorophenol 21.3 10.0-120 12/02/2023 01:58 WG2181093
(S) 2,4,6-Tribromophenol 52.5 10.0-153 12/02/2023 01:58 WG2181093
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 26 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 26 of 44
SAMPLE RESULTS - 08
L1682140
MW-13
Collected date/time: 11/28/23 10:40
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.0941 1.00 1 12/04/2023 04:48 WG2181973
Bromobenzene U 0.118 1.00 1 12/04/2023 04:48 WG2181973
Bromodichloromethane U 0.136 1.00 1 12/04/2023 04:48 WG2181973
Bromochloromethane U 0.128 1.00 1 12/04/2023 04:48 WG2181973
Bromoform U 0.129 1.00 1 12/04/2023 04:48 WG2181973
Bromomethane U 0.605 5.00 1 12/04/2023 04:48 WG2181973
n-Butylbenzene U 0.157 1.00 1 12/04/2023 04:48 WG2181973
sec-Butylbenzene U 0.125 1.00 1 12/04/2023 04:48 WG2181973
tert-Butylbenzene U J4 0.127 1.00 1 12/04/2023 04:48 WG2181973
Carbon tetrachloride U 0.128 1.00 1 12/04/2023 04:48 WG2181973
Chlorobenzene U 0.116 1.00 1 12/04/2023 04:48 WG2181973
Chlorodibromomethane U 0.140 1.00 1 12/04/2023 04:48 WG2181973
Chloroethane U 0.192 5.00 1 12/04/2023 04:48 WG2181973
Chloroform U 0.111 5.00 1 12/04/2023 04:48 WG2181973
Chloromethane U 0.960 2.50 1 12/04/2023 04:48 WG2181973
2-Chlorotoluene U 0.106 1.00 1 12/04/2023 04:48 WG2181973
4-Chlorotoluene U 0.114 1.00 1 12/04/2023 04:48 WG2181973
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 12/04/2023 04:48 WG2181973
1,2-Dibromoethane U 0.126 1.00 1 12/04/2023 04:48 WG2181973
Dibromomethane U 0.122 1.00 1 12/04/2023 04:48 WG2181973
1,2-Dichlorobenzene U 0.107 1.00 1 12/04/2023 04:48 WG2181973
1,3-Dichlorobenzene U 0.110 1.00 1 12/04/2023 04:48 WG2181973
1,4-Dichlorobenzene U 0.120 1.00 1 12/04/2023 04:48 WG2181973
Dichlorodifluoromethane U 0.374 5.00 1 12/04/2023 04:48 WG2181973
1,1-Dichloroethane U 0.100 1.00 1 12/04/2023 04:48 WG2181973
1,2-Dichloroethane U 0.0819 1.00 1 12/04/2023 04:48 WG2181973
1,1-Dichloroethene U 0.188 1.00 1 12/04/2023 04:48 WG2181973
cis-1,2-Dichloroethene U 0.126 1.00 1 12/04/2023 04:48 WG2181973
trans-1,2-Dichloroethene U 0.149 1.00 1 12/04/2023 04:48 WG2181973
1,2-Dichloropropane U 0.149 1.00 1 12/04/2023 04:48 WG2181973
1,1-Dichloropropene U 0.142 1.00 1 12/04/2023 04:48 WG2181973
1,3-Dichloropropane U 0.110 1.00 1 12/04/2023 04:48 WG2181973
cis-1,3-Dichloropropene U 0.111 1.00 1 12/04/2023 04:48 WG2181973
trans-1,3-Dichloropropene U 0.118 1.00 1 12/04/2023 04:48 WG2181973
2,2-Dichloropropane U 0.161 1.00 1 12/04/2023 04:48 WG2181973
Di-isopropyl ether U 0.105 1.00 1 12/04/2023 04:48 WG2181973
Ethylbenzene U 0.137 1.00 1 12/04/2023 04:48 WG2181973
Hexachloro-1,3-butadiene U 0.337 1.00 1 12/04/2023 04:48 WG2181973
Isopropylbenzene U 0.105 1.00 1 12/04/2023 04:48 WG2181973
Methylene Chloride U 0.430 5.00 1 12/04/2023 04:48 WG2181973
Methyl tert-butyl ether U 0.101 1.00 1 12/04/2023 04:48 WG2181973
Naphthalene U 1.00 5.00 1 12/04/2023 04:48 WG2181973
n-Propylbenzene U 0.0993 1.00 1 12/04/2023 04:48 WG2181973
Styrene U 0.118 1.00 1 12/04/2023 04:48 WG2181973
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 12/04/2023 04:48 WG2181973
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 12/04/2023 04:48 WG2181973
Tetrachloroethene U 0.300 1.00 1 12/04/2023 04:48 WG2181973
Toluene U 0.278 1.00 1 12/04/2023 04:48 WG2181973
1,2,3-Trichlorobenzene U 0.230 1.00 1 12/04/2023 04:48 WG2181973
1,2,4-Trichlorobenzene U 0.481 1.00 1 12/04/2023 04:48 WG2181973
1,1,1-Trichloroethane U 0.149 1.00 1 12/04/2023 04:48 WG2181973
1,1,2-Trichloroethane U 0.158 1.00 1 12/04/2023 04:48 WG2181973
Trichloroethene U 0.190 1.00 1 12/04/2023 04:48 WG2181973
Trichlorofluoromethane U 0.160 5.00 1 12/04/2023 04:48 WG2181973
1,2,3-Trichloropropane U 0.237 2.50 1 12/04/2023 04:48 WG2181973
1,2,4-Trimethylbenzene U 0.322 1.00 1 12/04/2023 04:48 WG2181973
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 27 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 27 of 44
SAMPLE RESULTS - 08
L1682140
MW-13
Collected date/time: 11/28/23 10:40
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene U 0.104 1.00 1 12/04/2023 04:48 WG2181973
Vinyl chloride U 0.234 1.00 1 12/04/2023 04:48 WG2181973
o-Xylene U 0.174 1.00 1 12/04/2023 04:48 WG2181973
m&p-Xylenes U 0.430 2.00 1 12/04/2023 04:48 WG2181973
ethanol U C4 42.0 100 1 12/04/2023 21:02 WG2182350
tert-Amyl Methyl Ether U 0.195 1.00 1 12/04/2023 04:48 WG2181973
Ethyl tert-butyl ether U 0.101 1.00 1 12/04/2023 04:48 WG2181973
tert-Butyl alcohol U 4.06 5.00 1 12/04/2023 04:48 WG2181973
t-Amyl Alcohol U 4.90 50.0 1 12/04/2023 04:48 WG2181973
tert-Butyl formate U C4 4.51 20.0 1 12/04/2023 21:02 WG2182350
(S) Toluene-d8 105 80.0-120 12/04/2023 04:48 WG2181973
(S) Toluene-d8 114 80.0-120 12/04/2023 21:02 WG2182350
(S) 4-Bromofluorobenzene 92.9 77.0-126 12/04/2023 04:48 WG2181973
(S) 4-Bromofluorobenzene 88.0 77.0-126 12/04/2023 21:02 WG2182350
(S) 1,2-Dichloroethane-d4 99.6 70.0-130 12/04/2023 04:48 WG2181973
(S) 1,2-Dichloroethane-d4 99.4 70.0-130 12/04/2023 21:02 WG2182350
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 34.2 B J 33.3 100 1 12/02/2023 17:07 WG2180752
Unadjusted C19-C36 Aliphatics 53.5 B J 33.3 100 1 12/02/2023 17:07 WG2180752
Unadjusted C11-C22 Aromatics 72.0 B J 33.3 100 1 12/02/2023 19:55 WG2180752
Unadjusted Total Petroleum
Hydrocarbons 160 33.3 100 1 12/02/2023 19:55 WG2180752
(S) o-Terphenyl 60.3 40.0-140 12/02/2023 19:55 WG2180752
(S) 1-Chloro-octadecane 32.1 J2 40.0-140 12/02/2023 17:07 WG2180752
(S) 2-Fluorobiphenyl 65.8 40.0-140 12/02/2023 19:55 WG2180752
(S) 2-Bromonaphthalene 59.7 40.0-140 12/02/2023 19:55 WG2180752
Sample Narrative:
L1682140-08 WG2180752: Sample produced emulsion during Extraction process, low surr/spike recoveries due to matrix.
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 12/02/2023 02:19 WG2181093
Acenaphthylene U 0.0921 1.00 1 12/02/2023 02:19 WG2181093
Anthracene U 0.0804 1.00 1 12/02/2023 02:19 WG2181093
Benzo(a)anthracene U 0.199 1.00 1 12/02/2023 02:19 WG2181093
Benzo(b)fluoranthene U 0.130 1.00 1 12/02/2023 02:19 WG2181093
Benzo(k)fluoranthene U 0.120 1.00 1 12/02/2023 02:19 WG2181093
Benzo(g,h,i)perylene U 0.121 1.00 1 12/02/2023 02:19 WG2181093
Benzo(a)pyrene U 0.0381 1.00 1 12/02/2023 02:19 WG2181093
Bis(2-chlorethoxy)methane U 0.116 10.0 1 12/02/2023 02:19 WG2181093
Bis(2-chloroethyl)ether U 0.137 10.0 1 12/02/2023 02:19 WG2181093
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 12/02/2023 02:19 WG2181093
4-Bromophenyl-phenylether U 0.0877 10.0 1 12/02/2023 02:19 WG2181093
2-Chloronaphthalene U 0.0648 1.00 1 12/02/2023 02:19 WG2181093
4-Chlorophenyl-phenylether U 0.0926 10.0 1 12/02/2023 02:19 WG2181093
Chrysene U 0.130 1.00 1 12/02/2023 02:19 WG2181093
Dibenz(a,h)anthracene U 0.0644 1.00 1 12/02/2023 02:19 WG2181093
3,3-Dichlorobenzidine U 0.212 10.0 1 12/02/2023 02:19 WG2181093
2,4-Dinitrotoluene U 0.0983 10.0 1 12/02/2023 02:19 WG2181093
2,6-Dinitrotoluene U 0.250 10.0 1 12/02/2023 02:19 WG2181093
Fluoranthene U 0.102 1.00 1 12/02/2023 02:19 WG2181093
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 28 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 28 of 44
SAMPLE RESULTS - 08
L1682140
MW-13
Collected date/time: 11/28/23 10:40
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Fluorene U 0.0844 1.00 1 12/02/2023 02:19 WG2181093
Hexachlorobenzene U 0.0755 1.00 1 12/02/2023 02:19 WG2181093
Hexachloro-1,3-butadiene U 0.0968 10.0 1 12/02/2023 02:19 WG2181093
Hexachlorocyclopentadiene U 0.0598 10.0 1 12/02/2023 02:19 WG2181093
Hexachloroethane U 0.127 10.0 1 12/02/2023 02:19 WG2181093
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 12/02/2023 02:19 WG2181093
Isophorone U 0.143 10.0 1 12/02/2023 02:19 WG2181093
Naphthalene U 0.159 1.00 1 12/02/2023 02:19 WG2181093
Nitrobenzene U 0.297 10.0 1 12/02/2023 02:19 WG2181093
n-Nitrosodimethylamine U 0.998 10.0 1 12/02/2023 02:19 WG2181093
n-Nitrosodiphenylamine U 2.37 10.0 1 12/02/2023 02:19 WG2181093
n-Nitrosodi-n-propylamine U 0.261 10.0 1 12/02/2023 02:19 WG2181093
Phenanthrene U 0.112 1.00 1 12/02/2023 02:19 WG2181093
Benzylbutyl phthalate U 0.765 3.00 1 12/02/2023 02:19 WG2181093
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 12/02/2023 02:19 WG2181093
Di-n-butyl phthalate U 0.453 3.00 1 12/02/2023 02:19 WG2181093
Diethyl phthalate U 0.287 3.00 1 12/02/2023 02:19 WG2181093
Dimethyl phthalate U 0.260 3.00 1 12/02/2023 02:19 WG2181093
Di-n-octyl phthalate U 0.932 3.00 1 12/02/2023 02:19 WG2181093
Pyrene U 0.107 1.00 1 12/02/2023 02:19 WG2181093
1,2,4-Trichlorobenzene U 0.0698 10.0 1 12/02/2023 02:19 WG2181093
4-Chloro-3-methylphenol U 0.131 10.0 1 12/02/2023 02:19 WG2181093
2-Chlorophenol U 0.133 10.0 1 12/02/2023 02:19 WG2181093
2,4-Dichlorophenol U 0.102 10.0 1 12/02/2023 02:19 WG2181093
2,4-Dimethylphenol U 0.0636 10.0 1 12/02/2023 02:19 WG2181093
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 12/02/2023 02:19 WG2181093
2,4-Dinitrophenol U 5.93 10.0 1 12/02/2023 02:19 WG2181093
2-Nitrophenol U 0.117 10.0 1 12/02/2023 02:19 WG2181093
4-Nitrophenol U 0.143 10.0 1 12/02/2023 02:19 WG2181093
Pentachlorophenol U 0.313 10.0 1 12/02/2023 02:19 WG2181093
Phenol U 4.33 10.0 1 12/02/2023 02:19 WG2181093
2,4,6-Trichlorophenol U 0.100 10.0 1 12/02/2023 02:19 WG2181093
(S) Nitrobenzene-d5 49.7 15.0-314 12/02/2023 02:19 WG2181093
(S) 2-Fluorobiphenyl 42.3 22.0-127 12/02/2023 02:19 WG2181093
(S) p-Terphenyl-d14 54.8 29.0-141 12/02/2023 02:19 WG2181093
(S) Phenol-d5 17.5 8.00-424 12/02/2023 02:19 WG2181093
(S) 2-Fluorophenol 22.1 10.0-120 12/02/2023 02:19 WG2181093
(S) 2,4,6-Tribromophenol 48.7 10.0-153 12/02/2023 02:19 WG2181093
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 29 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 29 of 44
QUALITY CONTROL SUMMARYWG2181973
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1682140-01,02,03,04,05,06,07,08
Method Blank (MB)
(MB) R4007654-2 12/04/23 01:28
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Benzene U 0.0941 1.00
Bromobenzene U 0.118 1.00
Bromodichloromethane U 0.136 1.00
Bromochloromethane U 0.128 1.00
Bromoform U 0.129 1.00
Bromomethane U 0.605 5.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
cis-1,3-Dichloropropene U 0.111 1.00
trans-1,3-Dichloropropene U 0.118 1.00
2,2-Dichloropropane U 0.161 1.00
Di-isopropyl ether U 0.105 1.00
Ethylbenzene U 0.137 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
Isopropylbenzene U 0.105 1.00
Methylene Chloride U 0.430 5.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 30 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 30 of 44
QUALITY CONTROL SUMMARYWG2181973
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1682140-01,02,03,04,05,06,07,08
Method Blank (MB)
(MB) R4007654-2 12/04/23 01:28
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Methyl tert-butyl ether U 0.101 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.0993 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Trichlorofluoromethane U 0.160 5.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,4-Trimethylbenzene U 0.322 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
Vinyl chloride U 0.234 1.00
o-Xylene U 0.174 1.00
m&p-Xylenes U 0.430 2.00
tert-Amyl Methyl Ether U 0.195 1.00
Ethyl tert-butyl ether U 0.101 1.00
tert-Butyl alcohol U 4.06 5.00
t-Amyl Alcohol U 4.90 50.0
(S) Toluene-d8 106 80.0-120
(S) 4-Bromofluorobenzene 90.7 77.0-126
(S) 1,2-Dichloroethane-d4 101 70.0-130
Laboratory Control Sample (LCS)
(LCS) R4007654-1 12/04/23 00:29
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Benzene 5.00 4.94 98.8 70.0-123
Bromobenzene 5.00 5.48 110 73.0-121
Bromodichloromethane 5.00 4.94 98.8 75.0-120
Bromochloromethane 5.00 5.17 103 76.0-122
Bromoform 5.00 4.72 94.4 68.0-132
Bromomethane 5.00 4.83 96.6 10.0-160
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 31 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 31 of 44
QUALITY CONTROL SUMMARYWG2181973
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1682140-01,02,03,04,05,06,07,08
Laboratory Control Sample (LCS)
(LCS) R4007654-1 12/04/23 00:29
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
n-Butylbenzene 5.00 4.63 92.6 73.0-125
sec-Butylbenzene 5.00 5.66 113 75.0-125
tert-Butylbenzene 5.00 6.43 129 76.0-124 J4
Carbon tetrachloride 5.00 5.66 113 68.0-126
Chlorobenzene 5.00 5.02 100 80.0-121
Chlorodibromomethane 5.00 5.08 102 77.0-125
Chloroethane 5.00 5.20 104 47.0-150
Chloroform 5.00 5.11 102 73.0-120
Chloromethane 5.00 5.50 110 41.0-142
2-Chlorotoluene 5.00 5.86 117 76.0-123
4-Chlorotoluene 5.00 5.48 110 75.0-122
1,2-Dibromo-3-Chloropropane 5.00 4.75 95.0 58.0-134
1,2-Dibromoethane 5.00 5.08 102 80.0-122
Dibromomethane 5.00 4.63 92.6 80.0-120
1,2-Dichlorobenzene 5.00 5.03 101 79.0-121
1,3-Dichlorobenzene 5.00 5.36 107 79.0-120
1,4-Dichlorobenzene 5.00 5.47 109 79.0-120
Dichlorodifluoromethane 5.00 5.48 110 51.0-149
1,1-Dichloroethane 5.00 5.20 104 70.0-126
1,2-Dichloroethane 5.00 5.02 100 70.0-128
1,1-Dichloroethene 5.00 4.82 96.4 71.0-124
cis-1,2-Dichloroethene 5.00 5.03 101 73.0-120
trans-1,2-Dichloroethene 5.00 5.25 105 73.0-120
1,2-Dichloropropane 5.00 5.32 106 77.0-125
1,1-Dichloropropene 5.00 5.24 105 74.0-126
1,3-Dichloropropane 5.00 5.12 102 80.0-120
cis-1,3-Dichloropropene 5.00 5.25 105 80.0-123
trans-1,3-Dichloropropene 5.00 5.16 103 78.0-124
2,2-Dichloropropane 5.00 5.79 116 58.0-130
Di-isopropyl ether 5.00 5.09 102 58.0-138
Ethylbenzene 5.00 5.24 105 79.0-123
Hexachloro-1,3-butadiene 5.00 5.07 101 54.0-138
Isopropylbenzene 5.00 5.19 104 76.0-127
Methylene Chloride 5.00 4.66 93.2 67.0-120
Methyl tert-butyl ether 5.00 5.44 109 68.0-125
Naphthalene 5.00 4.26 85.2 54.0-135
n-Propylbenzene 5.00 5.46 109 77.0-124
Styrene 5.00 4.86 97.2 73.0-130
1,1,1,2-Tetrachloroethane 5.00 5.00 100 75.0-125
1,1,2,2-Tetrachloroethane 5.00 5.37 107 65.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 32 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 32 of 44
QUALITY CONTROL SUMMARYWG2181973
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1682140-01,02,03,04,05,06,07,08
Laboratory Control Sample (LCS)
(LCS) R4007654-1 12/04/23 00:29
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Tetrachloroethene 5.00 5.29 106 72.0-132
Toluene 5.00 5.54 111 79.0-120
1,2,3-Trichlorobenzene 5.00 5.36 107 50.0-138
1,2,4-Trichlorobenzene 5.00 4.91 98.2 57.0-137
1,1,1-Trichloroethane 5.00 5.56 111 73.0-124
1,1,2-Trichloroethane 5.00 5.23 105 80.0-120
Trichloroethene 5.00 5.58 112 78.0-124
Trichlorofluoromethane 5.00 4.69 93.8 59.0-147
1,2,3-Trichloropropane 5.00 5.54 111 73.0-130
1,2,4-Trimethylbenzene 5.00 5.68 114 76.0-121
1,3,5-Trimethylbenzene 5.00 5.53 111 76.0-122
Vinyl chloride 5.00 4.62 92.4 67.0-131
o-Xylene 5.00 4.97 99.4 80.0-122
m&p-Xylenes 10.0 10.5 105 80.0-122
tert-Amyl Methyl Ether 5.00 4.84 96.8 66.0-125
Ethyl tert-butyl ether 5.00 5.07 101 63.0-138
tert-Butyl alcohol 25.0 25.0 100 27.0-160
(S) Toluene-d8 103 80.0-120
(S) 4-Bromofluorobenzene 93.8 77.0-126
(S) 1,2-Dichloroethane-d4 99.7 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 33 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 33 of 44
QUALITY CONTROL SUMMARYWG2182350
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1682140-01,02,03,04,05,06,07,08
Method Blank (MB)
(MB) R4008191-4 12/04/23 17:57
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
ethanol U 42.0 100
tert-Butyl formate U 4.51 20.0
(S) Toluene-d8 113 80.0-120
(S) 4-Bromofluorobenzene 90.0 77.0-126
(S) 1,2-Dichloroethane-d4 99.2 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R4008191-1 12/04/23 16:35 • (LCSD) R4008191-2 12/04/23 16:55
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
ethanol 250 156 172 62.4 68.8 10.0-160 9.76 30
(S) Toluene-d8 114 109 80.0-120
(S) 4-Bromofluorobenzene 93.3 93.3 77.0-126
(S) 1,2-Dichloroethane-d4 92.8 97.9 70.0-130
Laboratory Control Sample (LCS)
(LCS) R4008191-3 12/04/23 17:16
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
tert-Butyl formate 100 60.3 60.3 10.0-160
(S) Toluene-d8 114 80.0-120
(S) 4-Bromofluorobenzene 88.6 77.0-126
(S) 1,2-Dichloroethane-d4 98.3 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 34 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 34 of 44
QUALITY CONTROL SUMMARYWG2180752
TPH by Method MADEPE L1682140-01,02,03,04,05,06,07,08
Method Blank (MB)
(MB) R4007634-1 12/01/23 14:23
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics 34.3 J 33.3 100
Unadjusted C19-C36 Aliphatics 51.9 J 33.3 100
(S) 1-Chloro-octadecane 48.0 40.0-140
Method Blank (MB)
(MB) R4007634-4 12/01/23 15:35
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics 72.1 J 33.3 100
(S) o-Terphenyl 56.3 40.0-140
(S) 2-Fluorobiphenyl 64.8 40.0-140
(S) 2-Bromonaphthalene 56.3 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R4007634-2 12/01/23 14:47 • (LCSD) R4007634-3 12/01/23 15:11
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 298 270 49.7 45.0 40.0-140 9.86 25
Unadjusted C19-C36 Aliphatics 800 564 524 70.5 65.5 40.0-140 7.35 25
(S) 1-Chloro-octadecane 53.3 45.5 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R4007634-5 12/01/23 15:59 • (LCSD) R4007634-6 12/01/23 16:23
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1080 1290 63.5 75.9 40.0-140 17.7 25
(S) o-Terphenyl 60.7 68.3 40.0-140
(S) 2-Fluorobiphenyl 68.0 75.0 40.0-140
(S) 2-Bromonaphthalene 54.3 64.3 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 35 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 35 of 44
QUALITY CONTROL SUMMARYWG2181093
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1682140-01,02,03,04,05,06,07,08
Method Blank (MB)
(MB) R4007674-2 12/01/23 23:06
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.0886 1.00
Acenaphthylene U 0.0921 1.00
Anthracene U 0.0804 1.00
Benzo(a)anthracene U 0.199 1.00
Benzo(b)fluoranthene U 0.130 1.00
Benzo(k)fluoranthene U 0.120 1.00
Benzo(g,h,i)perylene U 0.121 1.00
Benzo(a)pyrene U 0.0381 1.00
Bis(2-chlorethoxy)methane U 0.116 10.0
Bis(2-chloroethyl)ether U 0.137 10.0
2,2-Oxybis(1-Chloropropane)U 0.210 10.0
4-Bromophenyl-phenylether U 0.0877 10.0
2-Chloronaphthalene U 0.0648 1.00
4-Chlorophenyl-phenylether U 0.0926 10.0
Chrysene U 0.130 1.00
Dibenz(a,h)anthracene U 0.0644 1.00
3,3-Dichlorobenzidine U 0.212 10.0
2,4-Dinitrotoluene U 0.0983 10.0
2,6-Dinitrotoluene U 0.250 10.0
Fluoranthene U 0.102 1.00
Fluorene U 0.0844 1.00
Hexachlorobenzene U 0.0755 1.00
Hexachloro-1,3-butadiene U 0.0968 10.0
Hexachlorocyclopentadiene U 0.0598 10.0
Hexachloroethane U 0.127 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.143 10.0
Naphthalene U 0.159 1.00
Nitrobenzene U 0.297 10.0
n-Nitrosodimethylamine U 0.998 10.0
n-Nitrosodiphenylamine U 2.37 10.0
n-Nitrosodi-n-propylamine U 0.261 10.0
Phenanthrene U 0.112 1.00
Benzylbutyl phthalate U 0.765 3.00
Bis(2-ethylhexyl)phthalate U 0.895 3.00
Di-n-butyl phthalate U 0.453 3.00
Diethyl phthalate U 0.287 3.00
Dimethyl phthalate U 0.260 3.00
Di-n-octyl phthalate U 0.932 3.00
Pyrene U 0.107 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 36 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 36 of 44
QUALITY CONTROL SUMMARYWG2181093
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1682140-01,02,03,04,05,06,07,08
Method Blank (MB)
(MB) R4007674-2 12/01/23 23:06
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
1,2,4-Trichlorobenzene U 0.0698 10.0
4-Chloro-3-methylphenol U 0.131 10.0
2-Chlorophenol U 0.133 10.0
2,4-Dichlorophenol U 0.102 10.0
2,4-Dimethylphenol U 0.0636 10.0
4,6-Dinitro-2-methylphenol U 1.12 10.0
2,4-Dinitrophenol U 5.93 10.0
2-Nitrophenol U 0.117 10.0
4-Nitrophenol U 0.143 10.0
Pentachlorophenol U 0.313 10.0
Phenol U 4.33 10.0
2,4,6-Trichlorophenol U 0.100 10.0
(S) Nitrobenzene-d5 59.5 15.0-314
(S) 2-Fluorobiphenyl 53.1 22.0-127
(S) p-Terphenyl-d14 70.3 29.0-141
(S) Phenol-d5 20.0 8.00-424
(S) 2-Fluorophenol 28.1 10.0-120
(S) 2,4,6-Tribromophenol 48.6 10.0-153
Laboratory Control Sample (LCS)
(LCS) R4007674-1 12/01/23 22:45
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acenaphthene 50.0 38.5 77.0 47.0-145
Acenaphthylene 50.0 39.3 78.6 33.0-145
Anthracene 50.0 42.0 84.0 27.0-133
Benzo(a)anthracene 50.0 42.1 84.2 33.0-143
Benzo(b)fluoranthene 50.0 40.7 81.4 24.0-159
Benzo(k)fluoranthene 50.0 40.1 80.2 11.0-162
Benzo(g,h,i)perylene 50.0 35.8 71.6 1.00-219
Benzo(a)pyrene 50.0 38.8 77.6 17.0-163
Bis(2-chlorethoxy)methane 50.0 33.2 66.4 1.00-219
Bis(2-chloroethyl)ether 50.0 36.0 72.0 33.0-185
2,2-Oxybis(1-Chloropropane)50.0 34.3 68.6 36.0-166
4-Bromophenyl-phenylether 50.0 42.3 84.6 53.0-127
2-Chloronaphthalene 50.0 35.7 71.4 60.0-120
4-Chlorophenyl-phenylether 50.0 38.7 77.4 25.0-158
Chrysene 50.0 39.1 78.2 17.0-168
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 37 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 37 of 44
QUALITY CONTROL SUMMARYWG2181093
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1682140-01,02,03,04,05,06,07,08
Laboratory Control Sample (LCS)
(LCS) R4007674-1 12/01/23 22:45
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Dibenz(a,h)anthracene 50.0 38.8 77.6 1.00-227
3,3-Dichlorobenzidine 100 81.2 81.2 1.00-262
2,4-Dinitrotoluene 50.0 47.8 95.6 39.0-139
2,6-Dinitrotoluene 50.0 44.8 89.6 50.0-158
Fluoranthene 50.0 42.1 84.2 26.0-137
Fluorene 50.0 32.5 65.0 59.0-121
Hexachlorobenzene 50.0 43.4 86.8 1.00-152
Hexachloro-1,3-butadiene 50.0 23.8 47.6 24.0-120
Hexachlorocyclopentadiene 50.0 12.6 25.2 10.0-120
Hexachloroethane 50.0 28.0 56.0 40.0-120
Indeno(1,2,3-cd)pyrene 50.0 32.9 65.8 1.00-171
Isophorone 50.0 33.3 66.6 21.0-196
Naphthalene 50.0 28.0 56.0 21.0-133
Nitrobenzene 50.0 30.7 61.4 35.0-180
n-Nitrosodimethylamine 50.0 22.6 45.2 10.0-120
n-Nitrosodiphenylamine 50.0 41.9 83.8 44.0-120
n-Nitrosodi-n-propylamine 50.0 38.9 77.8 1.00-230
Phenanthrene 50.0 41.6 83.2 54.0-120
Benzylbutyl phthalate 50.0 50.4 101 1.00-152
Bis(2-ethylhexyl)phthalate 50.0 47.9 95.8 8.00-158
Di-n-butyl phthalate 50.0 51.8 104 1.00-120
Diethyl phthalate 50.0 45.9 91.8 1.00-120
Dimethyl phthalate 50.0 42.8 85.6 1.00-120
Di-n-octyl phthalate 50.0 46.2 92.4 4.00-146
Pyrene 50.0 43.8 87.6 52.0-120
1,2,4-Trichlorobenzene 50.0 24.7 49.4 44.0-142
4-Chloro-3-methylphenol 50.0 26.9 53.8 22.0-147
2-Chlorophenol 50.0 23.9 47.8 23.0-134
2,4-Dichlorophenol 50.0 25.3 50.6 39.0-135
2,4-Dimethylphenol 50.0 28.7 57.4 32.0-120
4,6-Dinitro-2-methylphenol 50.0 42.2 84.4 1.00-181
2,4-Dinitrophenol 50.0 31.9 63.8 1.00-191
2-Nitrophenol 50.0 35.2 70.4 29.0-182
4-Nitrophenol 50.0 11.5 23.0 1.00-132
Pentachlorophenol 50.0 19.0 38.0 14.0-176
Phenol 50.0 15.8 31.6 5.00-120
2,4,6-Trichlorophenol 50.0 34.2 68.4 37.0-144
(S) Nitrobenzene-d5 69.0 15.0-314
(S) 2-Fluorobiphenyl 76.5 22.0-127
(S) p-Terphenyl-d14 89.7 29.0-141
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 38 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 38 of 44
QUALITY CONTROL SUMMARYWG2181093
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1682140-01,02,03,04,05,06,07,08
Laboratory Control Sample (LCS)
(LCS) R4007674-1 12/01/23 22:45
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
(S) Phenol-d5 28.4 8.00-424
(S) 2-Fluorophenol 35.1 10.0-120
(S) 2,4,6-Tribromophenol 86.0 10.0-153
L1682864-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1682864-01 12/02/23 03:00 • (MS) R4007674-3 12/02/23 03:21 • (MSD) R4007674-4 12/02/23 03:42
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Acenaphthene 50.0 U 26.0 25.1 52.0 50.2 1 47.0-145 3.52 48
Acenaphthylene 50.0 U 24.3 23.8 48.6 47.6 1 33.0-145 2.08 74
Anthracene 50.0 U 24.0 23.3 48.0 46.6 1 27.0-133 2.96 66
Benzo(a)anthracene 50.0 U 24.2 23.8 48.4 47.6 1 33.0-143 1.67 53
Benzo(b)fluoranthene 50.0 U 25.6 25.5 51.2 51.0 1 24.0-159 0.391 71
Benzo(k)fluoranthene 50.0 U 20.8 23.9 41.6 47.8 1 11.0-162 13.9 63
Benzo(g,h,i)perylene 50.0 U 20.1 19.8 40.2 39.6 1 1.00-219 1.50 97
Benzo(a)pyrene 50.0 U 21.5 21.7 43.0 43.4 1 17.0-163 0.926 72
Bis(2-chlorethoxy)methane 50.0 U 26.8 24.7 53.6 49.4 1 33.0-184 8.16 54
Bis(2-chloroethyl)ether 50.0 U 28.9 26.4 57.8 52.8 1 12.0-158 9.04 108
2,2-Oxybis(1-Chloropropane)50.0 U 24.2 21.6 48.4 43.2 1 36.0-166 11.4 76
4-Bromophenyl-phenylether 50.0 U 27.4 26.5 54.8 53.0 1 53.0-127 3.34 43
2-Chloronaphthalene 50.0 U 24.3 23.2 48.6 46.4 1 60.0-120 J6 J6 4.63 24
4-Chlorophenyl-phenylether 50.0 U 25.5 24.1 51.0 48.2 1 25.0-158 5.65 61
Chrysene 50.0 U 23.7 23.5 47.4 47.0 1 17.0-168 0.847 87
Dibenz(a,h)anthracene 50.0 U 21.2 22.1 42.4 44.2 1 1.00-227 4.16 126
3,3-Dichlorobenzidine 100 U U U 0.000 0.000 1 1.00-262 J6 J6 0.000 108
2,4-Dinitrotoluene 50.0 U 33.6 31.3 67.2 62.6 1 39.0-139 7.09 42
2,6-Dinitrotoluene 50.0 U 31.4 28.7 62.8 57.4 1 50.0-158 8.99 48
Fluoranthene 50.0 U 25.6 25.1 51.2 50.2 1 26.0-137 1.97 66
Fluorene 50.0 U 26.3 25.0 52.6 50.0 1 59.0-121 J6 J6 5.07 38
Hexachlorobenzene 50.0 U 25.0 24.3 50.0 48.6 1 1.00-152 2.84 55
Hexachloro-1,3-butadiene 50.0 U 16.1 16.4 32.2 32.8 1 24.0-120 1.85 62
Hexachlorocyclopentadiene 50.0 U 10.8 11.9 21.6 23.8 1 10.0-146 9.69 34
Hexachloroethane 50.0 U 18.7 17.9 37.4 35.8 1 40.0-120 J6 J6 4.37 52
Indeno(1,2,3-cd)pyrene 50.0 U 18.7 19.7 37.4 39.4 1 1.00-171 5.21 99
Isophorone 50.0 U 27.1 24.5 54.2 49.0 1 21.0-196 10.1 93
Naphthalene 50.0 U 20.9 20.1 41.8 40.2 1 21.0-133 3.90 65
Nitrobenzene 50.0 U 32.4 30.5 64.8 61.0 1 35.0-180 6.04 62
n-Nitrosodimethylamine 50.0 U 18.6 17.1 37.2 34.2 1 10.0-120 8.40 40
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 39 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 39 of 44
QUALITY CONTROL SUMMARYWG2181093
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1682140-01,02,03,04,05,06,07,08
L1682864-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1682864-01 12/02/23 03:00 • (MS) R4007674-3 12/02/23 03:21 • (MSD) R4007674-4 12/02/23 03:42
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
n-Nitrosodiphenylamine 50.0 U 26.9 26.0 53.8 52.0 1 16.0-160 3.40 28
n-Nitrosodi-n-propylamine 50.0 U 28.3 25.7 56.6 51.4 1 1.00-230 9.63 87
Phenanthrene 50.0 U 27.5 26.5 55.0 53.0 1 54.0-120 J6 3.70 39
Benzylbutyl phthalate 50.0 U 34.6 34.2 69.2 68.4 1 1.00-152 1.16 60
Bis(2-ethylhexyl)phthalate 50.0 U 28.0 27.6 56.0 55.2 1 8.00-158 1.44 82
Di-n-butyl phthalate 50.0 U 32.4 32.0 64.8 64.0 1 1.00-120 1.24 47
Diethyl phthalate 50.0 U 30.2 29.2 60.4 58.4 1 1.00-120 3.37 100
Dimethyl phthalate 50.0 U 30.1 28.1 60.2 56.2 1 1.00-120 6.87 183
Di-n-octyl phthalate 50.0 U 27.9 27.6 55.8 55.2 1 4.00-146 1.08 69
Pyrene 50.0 U 28.3 28.9 56.6 57.8 1 52.0-120 2.10 49
1,2,4-Trichlorobenzene 50.0 U 17.2 17.2 34.4 34.4 1 44.0-142 J6 J6 0.000 50
4-Chloro-3-methylphenol 50.0 U 22.9 20.5 45.8 41.0 1 22.0-147 11.1 73
2-Chlorophenol 50.0 U 18.9 17.8 37.8 35.6 1 23.0-134 5.99 61
2,4-Dichlorophenol 50.0 U 20.0 18.7 40.0 37.4 1 39.0-135 J6 6.72 50
2,4-Dimethylphenol 50.0 U 8.41 7.02 16.8 14.0 1 32.0-120 J6 J6 18.0 58
4,6-Dinitro-2-methylphenol 50.0 U 27.8 27.3 55.6 54.6 1 1.00-181 1.81 203
2,4-Dinitrophenol 50.0 U 29.0 29.6 58.0 59.2 1 1.00-191 2.05 132
2-Nitrophenol 50.0 U 28.2 26.6 56.4 53.2 1 29.0-182 5.84 55
4-Nitrophenol 50.0 U 12.6 11.8 25.2 23.6 1 1.00-132 6.56 131
Pentachlorophenol 50.0 U 13.6 15.2 27.2 30.4 1 14.0-176 11.1 86
Phenol 50.0 U 13.0 11.8 26.0 23.6 1 5.00-120 9.68 64
2,4,6-Trichlorophenol 50.0 U 23.0 21.6 46.0 43.2 1 37.0-144 6.28 58
(S) Nitrobenzene-d5 53.2 49.0 15.0-314
(S) 2-Fluorobiphenyl 48.3 46.6 22.0-127
(S) p-Terphenyl-d14 53.7 53.0 29.0-141
(S) Phenol-d5 21.4 20.5 8.00-424
(S) 2-Fluorophenol 28.0 23.7 10.0-120
(S) 2,4,6-Tribromophenol 49.8 44.0 10.0-153
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 40 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 40 of 44
GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
C4 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low.
Data is likely to show a low bias concerning the result.
J The identification of the analyte is acceptable; the reported value is an estimate.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J4 The associated batch QC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 41 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 41 of 44

Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/05/23 16:23 42 of 44
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682140 12/06/23 08:37 42 of 44
ANALYTICAL REPORT
December 05, 2023
Colonial Pipeline- S&ME Raleigh
Sample Delivery Group:L1682629
Samples Received:11/30/2023
Project Number:210818
Description:Colonial Pipeline - Jennifer Drive
Report To:Mr. Michael Pfeifer
3201 Spring Forrest Road
Raleigh, NC 27616
Entire Report Reviewed By:
December 05, 2023
[Preliminary Report]
Craig Cothron
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 1 of 32
December 06, 2023
Craig Cothron
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 1 of 32
TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
MW-1D L1682629-01 5
MW-4D L1682629-02 8
MW-5D L1682629-03 11
MW-6D L1682629-04 14
TRIP BLANK L1682629-05 17
Qc: Quality Control Summary 19
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 19
TPH by Method MADEPE 24
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 25
Gl: Glossary of Terms 30
Al: Accreditations & Locations 31
Sc: Sample Chain of Custody 32
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 2 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 2 of 32
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-1D L1682629-01 GW James Waters 11/29/23 12:30 11/30/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2182129 1 12/04/23 05:27 12/04/23 05:27 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2182350 1 12/04/23 21:23 12/04/23 21:23 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2182322 1 12/01/23 08:39 12/05/23 08:51 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2182322 1 12/01/23 08:39 12/05/23 08:59 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2180281 1 12/01/23 08:16 12/01/23 17:02 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-4D L1682629-02 GW James Waters 11/29/23 11:40 11/30/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2182129 50 12/04/23 06:27 12/04/23 06:27 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2182350 50 12/04/23 22:45 12/04/23 22:45 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2182322 1 12/01/23 08:39 12/05/23 09:15 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2182322 1 12/01/23 08:39 12/05/23 09:21 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2180281 1 12/01/23 08:16 12/01/23 17:23 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-5D L1682629-03 GW James Waters 11/29/23 10:10 11/30/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2182129 1 12/04/23 05:47 12/04/23 05:47 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2182350 1 12/04/23 21:43 12/04/23 21:43 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2182322 1 12/01/23 08:39 12/05/23 09:39 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2182322 1 12/01/23 08:39 12/05/23 09:43 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2180281 1 12/01/23 08:16 12/01/23 17:44 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-6D L1682629-04 GW James Waters 11/29/23 10:50 11/30/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2182129 1 12/04/23 06:07 12/04/23 06:07 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2182350 1 12/04/23 22:04 12/04/23 22:04 ADM Mt. Juliet, TN
TPH by Method MADEPE WG2182322 1 12/01/23 08:39 12/05/23 10:03 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2182322 1 12/01/23 08:39 12/05/23 10:05 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2180281 1 12/01/23 08:16 12/01/23 18:05 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
TRIP BLANK L1682629-05 GW James Waters 11/29/23 00:00 11/30/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2182129 1 12/04/23 02:29 12/04/23 02:29 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2182350 1 12/04/23 18:38 12/04/23 18:38 ADM Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 3 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 3 of 32
CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Craig Cothron
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 4 of 32
Craig Cothron
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 4 of 32
SAMPLE RESULTS - 01
L1682629
MW-1D
Collected date/time: 11/29/23 12:30
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.0941 1.00 1 12/04/2023 05:27 WG2182129
Bromobenzene U 0.118 1.00 1 12/04/2023 05:27 WG2182129
Bromodichloromethane U 0.136 1.00 1 12/04/2023 05:27 WG2182129
Bromochloromethane U 0.128 1.00 1 12/04/2023 05:27 WG2182129
Bromoform U 0.129 1.00 1 12/04/2023 05:27 WG2182129
Bromomethane U 0.605 5.00 1 12/04/2023 05:27 WG2182129
n-Butylbenzene U 0.157 1.00 1 12/04/2023 05:27 WG2182129
sec-Butylbenzene U 0.125 1.00 1 12/04/2023 05:27 WG2182129
tert-Butylbenzene U J4 0.127 1.00 1 12/04/2023 05:27 WG2182129
Carbon tetrachloride U 0.128 1.00 1 12/04/2023 05:27 WG2182129
Chlorobenzene U 0.116 1.00 1 12/04/2023 05:27 WG2182129
Chlorodibromomethane U 0.140 1.00 1 12/04/2023 05:27 WG2182129
Chloroethane U 0.192 5.00 1 12/04/2023 05:27 WG2182129
Chloroform U 0.111 5.00 1 12/04/2023 05:27 WG2182129
Chloromethane U 0.960 2.50 1 12/04/2023 05:27 WG2182129
2-Chlorotoluene U 0.106 1.00 1 12/04/2023 05:27 WG2182129
4-Chlorotoluene U 0.114 1.00 1 12/04/2023 05:27 WG2182129
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 12/04/2023 05:27 WG2182129
1,2-Dibromoethane U 0.126 1.00 1 12/04/2023 05:27 WG2182129
Dibromomethane U 0.122 1.00 1 12/04/2023 05:27 WG2182129
1,2-Dichlorobenzene U 0.107 1.00 1 12/04/2023 05:27 WG2182129
1,3-Dichlorobenzene U 0.110 1.00 1 12/04/2023 05:27 WG2182129
1,4-Dichlorobenzene U 0.120 1.00 1 12/04/2023 05:27 WG2182129
Dichlorodifluoromethane U 0.374 5.00 1 12/04/2023 05:27 WG2182129
1,1-Dichloroethane U 0.100 1.00 1 12/04/2023 05:27 WG2182129
1,2-Dichloroethane U 0.0819 1.00 1 12/04/2023 05:27 WG2182129
1,1-Dichloroethene U 0.188 1.00 1 12/04/2023 05:27 WG2182129
cis-1,2-Dichloroethene U 0.126 1.00 1 12/04/2023 05:27 WG2182129
trans-1,2-Dichloroethene U 0.149 1.00 1 12/04/2023 05:27 WG2182129
1,2-Dichloropropane U 0.149 1.00 1 12/04/2023 05:27 WG2182129
1,1-Dichloropropene U 0.142 1.00 1 12/04/2023 05:27 WG2182129
1,3-Dichloropropane U 0.110 1.00 1 12/04/2023 05:27 WG2182129
cis-1,3-Dichloropropene U 0.111 1.00 1 12/04/2023 05:27 WG2182129
trans-1,3-Dichloropropene U 0.118 1.00 1 12/04/2023 05:27 WG2182129
2,2-Dichloropropane U 0.161 1.00 1 12/04/2023 05:27 WG2182129
Di-isopropyl ether U 0.105 1.00 1 12/04/2023 05:27 WG2182129
Ethylbenzene U 0.137 1.00 1 12/04/2023 05:27 WG2182129
Hexachloro-1,3-butadiene U 0.337 1.00 1 12/04/2023 05:27 WG2182129
Isopropylbenzene U 0.105 1.00 1 12/04/2023 05:27 WG2182129
Methylene Chloride U 0.430 5.00 1 12/04/2023 05:27 WG2182129
Methyl tert-butyl ether U 0.101 1.00 1 12/04/2023 05:27 WG2182129
Naphthalene U 1.00 5.00 1 12/04/2023 05:27 WG2182129
n-Propylbenzene U 0.0993 1.00 1 12/04/2023 05:27 WG2182129
Styrene U 0.118 1.00 1 12/04/2023 05:27 WG2182129
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 12/04/2023 05:27 WG2182129
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 12/04/2023 05:27 WG2182129
Tetrachloroethene U 0.300 1.00 1 12/04/2023 05:27 WG2182129
Toluene U 0.278 1.00 1 12/04/2023 05:27 WG2182129
1,2,3-Trichlorobenzene U 0.230 1.00 1 12/04/2023 05:27 WG2182129
1,2,4-Trichlorobenzene U 0.481 1.00 1 12/04/2023 05:27 WG2182129
1,1,1-Trichloroethane U 0.149 1.00 1 12/04/2023 05:27 WG2182129
1,1,2-Trichloroethane U 0.158 1.00 1 12/04/2023 05:27 WG2182129
Trichloroethene U 0.190 1.00 1 12/04/2023 05:27 WG2182129
Trichlorofluoromethane U 0.160 5.00 1 12/04/2023 05:27 WG2182129
1,2,3-Trichloropropane U 0.237 2.50 1 12/04/2023 05:27 WG2182129
1,2,4-Trimethylbenzene U 0.322 1.00 1 12/04/2023 05:27 WG2182129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 5 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 5 of 32
SAMPLE RESULTS - 01
L1682629
MW-1D
Collected date/time: 11/29/23 12:30
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene U 0.104 1.00 1 12/04/2023 05:27 WG2182129
Vinyl chloride U 0.234 1.00 1 12/04/2023 05:27 WG2182129
o-Xylene U 0.174 1.00 1 12/04/2023 05:27 WG2182129
m&p-Xylenes U 0.430 2.00 1 12/04/2023 05:27 WG2182129
ethanol U C4 42.0 100 1 12/04/2023 21:23 WG2182350
tert-Amyl Methyl Ether U 0.195 1.00 1 12/04/2023 05:27 WG2182129
Ethyl tert-butyl ether U 0.101 1.00 1 12/04/2023 05:27 WG2182129
tert-Butyl alcohol U 4.06 5.00 1 12/04/2023 05:27 WG2182129
t-Amyl Alcohol U 4.90 50.0 1 12/04/2023 05:27 WG2182129
tert-Butyl formate U C4 4.51 20.0 1 12/04/2023 21:23 WG2182350
(S) Toluene-d8 104 80.0-120 12/04/2023 05:27 WG2182129
(S) Toluene-d8 114 80.0-120 12/04/2023 21:23 WG2182350
(S) 4-Bromofluorobenzene 95.4 77.0-126 12/04/2023 05:27 WG2182129
(S) 4-Bromofluorobenzene 87.6 77.0-126 12/04/2023 21:23 WG2182350
(S) 1,2-Dichloroethane-d4 97.8 70.0-130 12/04/2023 05:27 WG2182129
(S) 1,2-Dichloroethane-d4 98.1 70.0-130 12/04/2023 21:23 WG2182350
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 46.8 B J 33.3 100 1 12/05/2023 08:51 WG2182322
Unadjusted C19-C36 Aliphatics 46.9 B J 33.3 100 1 12/05/2023 08:51 WG2182322
Unadjusted C11-C22 Aromatics 80.7 B J 33.3 100 1 12/05/2023 08:59 WG2182322
Unadjusted Total Petroleum
Hydrocarbons 174 33.3 100 1 12/05/2023 08:59 WG2182322
(S) o-Terphenyl 80.3 40.0-140 12/05/2023 08:59 WG2182322
(S) 1-Chloro-octadecane 53.4 40.0-140 12/05/2023 08:51 WG2182322
(S) 2-Fluorobiphenyl 92.9 40.0-140 12/05/2023 08:59 WG2182322
(S) 2-Bromonaphthalene 98.9 40.0-140 12/05/2023 08:59 WG2182322
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 12/01/2023 17:02 WG2180281
Acenaphthylene U 0.0921 1.00 1 12/01/2023 17:02 WG2180281
Anthracene U 0.0804 1.00 1 12/01/2023 17:02 WG2180281
Benzo(a)anthracene U 0.199 1.00 1 12/01/2023 17:02 WG2180281
Benzo(b)fluoranthene U 0.130 1.00 1 12/01/2023 17:02 WG2180281
Benzo(k)fluoranthene U 0.120 1.00 1 12/01/2023 17:02 WG2180281
Benzo(g,h,i)perylene U 0.121 1.00 1 12/01/2023 17:02 WG2180281
Benzo(a)pyrene U 0.0381 1.00 1 12/01/2023 17:02 WG2180281
Bis(2-chlorethoxy)methane U 0.116 10.0 1 12/01/2023 17:02 WG2180281
Bis(2-chloroethyl)ether U 0.137 10.0 1 12/01/2023 17:02 WG2180281
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 12/01/2023 17:02 WG2180281
4-Bromophenyl-phenylether U 0.0877 10.0 1 12/01/2023 17:02 WG2180281
2-Chloronaphthalene U 0.0648 1.00 1 12/01/2023 17:02 WG2180281
4-Chlorophenyl-phenylether U 0.0926 10.0 1 12/01/2023 17:02 WG2180281
Chrysene U 0.130 1.00 1 12/01/2023 17:02 WG2180281
Dibenz(a,h)anthracene U 0.0644 1.00 1 12/01/2023 17:02 WG2180281
3,3-Dichlorobenzidine U 0.212 10.0 1 12/01/2023 17:02 WG2180281
2,4-Dinitrotoluene U 0.0983 10.0 1 12/01/2023 17:02 WG2180281
2,6-Dinitrotoluene U 0.250 10.0 1 12/01/2023 17:02 WG2180281
Fluoranthene U 0.102 1.00 1 12/01/2023 17:02 WG2180281
Fluorene U 0.0844 1.00 1 12/01/2023 17:02 WG2180281
Hexachlorobenzene U 0.0755 1.00 1 12/01/2023 17:02 WG2180281
Hexachloro-1,3-butadiene U 0.0968 10.0 1 12/01/2023 17:02 WG2180281
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 6 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 6 of 32
SAMPLE RESULTS - 01
L1682629
MW-1D
Collected date/time: 11/29/23 12:30
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexachlorocyclopentadiene U 0.0598 10.0 1 12/01/2023 17:02 WG2180281
Hexachloroethane U 0.127 10.0 1 12/01/2023 17:02 WG2180281
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 12/01/2023 17:02 WG2180281
Isophorone U 0.143 10.0 1 12/01/2023 17:02 WG2180281
Naphthalene U 0.159 1.00 1 12/01/2023 17:02 WG2180281
Nitrobenzene U 0.297 10.0 1 12/01/2023 17:02 WG2180281
n-Nitrosodimethylamine U 0.998 10.0 1 12/01/2023 17:02 WG2180281
n-Nitrosodiphenylamine U 2.37 10.0 1 12/01/2023 17:02 WG2180281
n-Nitrosodi-n-propylamine U 0.261 10.0 1 12/01/2023 17:02 WG2180281
Phenanthrene U 0.112 1.00 1 12/01/2023 17:02 WG2180281
Benzylbutyl phthalate U 0.765 3.00 1 12/01/2023 17:02 WG2180281
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 12/01/2023 17:02 WG2180281
Di-n-butyl phthalate U 0.453 3.00 1 12/01/2023 17:02 WG2180281
Diethyl phthalate U 0.287 3.00 1 12/01/2023 17:02 WG2180281
Dimethyl phthalate U 0.260 3.00 1 12/01/2023 17:02 WG2180281
Di-n-octyl phthalate U 0.932 3.00 1 12/01/2023 17:02 WG2180281
Pyrene U 0.107 1.00 1 12/01/2023 17:02 WG2180281
1,2,4-Trichlorobenzene U 0.0698 10.0 1 12/01/2023 17:02 WG2180281
4-Chloro-3-methylphenol U 0.131 10.0 1 12/01/2023 17:02 WG2180281
2-Chlorophenol U 0.133 10.0 1 12/01/2023 17:02 WG2180281
2,4-Dichlorophenol U 0.102 10.0 1 12/01/2023 17:02 WG2180281
2,4-Dimethylphenol U 0.0636 10.0 1 12/01/2023 17:02 WG2180281
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 12/01/2023 17:02 WG2180281
2,4-Dinitrophenol U 5.93 10.0 1 12/01/2023 17:02 WG2180281
2-Nitrophenol U 0.117 10.0 1 12/01/2023 17:02 WG2180281
4-Nitrophenol U 0.143 10.0 1 12/01/2023 17:02 WG2180281
Pentachlorophenol U 0.313 10.0 1 12/01/2023 17:02 WG2180281
Phenol U 4.33 10.0 1 12/01/2023 17:02 WG2180281
2,4,6-Trichlorophenol U 0.100 10.0 1 12/01/2023 17:02 WG2180281
(S) Nitrobenzene-d5 71.1 15.0-314 12/01/2023 17:02 WG2180281
(S) 2-Fluorobiphenyl 53.3 22.0-127 12/01/2023 17:02 WG2180281
(S) p-Terphenyl-d14 84.8 29.0-141 12/01/2023 17:02 WG2180281
(S) Phenol-d5 24.5 8.00-424 12/01/2023 17:02 WG2180281
(S) 2-Fluorophenol 33.7 10.0-120 12/01/2023 17:02 WG2180281
(S) 2,4,6-Tribromophenol 59.3 10.0-153 12/01/2023 17:02 WG2180281
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 7 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 7 of 32
SAMPLE RESULTS - 02
L1682629
MW-4D
Collected date/time: 11/29/23 11:40
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene 1570 4.71 50.0 50 12/04/2023 06:27 WG2182129
Bromobenzene U 5.90 50.0 50 12/04/2023 06:27 WG2182129
Bromodichloromethane U 6.80 50.0 50 12/04/2023 06:27 WG2182129
Bromochloromethane U 6.40 50.0 50 12/04/2023 06:27 WG2182129
Bromoform U 6.45 50.0 50 12/04/2023 06:27 WG2182129
Bromomethane U 30.3 250 50 12/04/2023 06:27 WG2182129
n-Butylbenzene U 7.85 50.0 50 12/04/2023 06:27 WG2182129
sec-Butylbenzene U 6.25 50.0 50 12/04/2023 06:27 WG2182129
tert-Butylbenzene U J4 6.35 50.0 50 12/04/2023 06:27 WG2182129
Carbon tetrachloride U 6.40 50.0 50 12/04/2023 06:27 WG2182129
Chlorobenzene U 5.80 50.0 50 12/04/2023 06:27 WG2182129
Chlorodibromomethane U 7.00 50.0 50 12/04/2023 06:27 WG2182129
Chloroethane U 9.60 250 50 12/04/2023 06:27 WG2182129
Chloroform U 5.55 250 50 12/04/2023 06:27 WG2182129
Chloromethane U 48.0 125 50 12/04/2023 06:27 WG2182129
2-Chlorotoluene U 5.30 50.0 50 12/04/2023 06:27 WG2182129
4-Chlorotoluene U 5.70 50.0 50 12/04/2023 06:27 WG2182129
1,2-Dibromo-3-Chloropropane U 13.8 250 50 12/04/2023 06:27 WG2182129
1,2-Dibromoethane U 6.30 50.0 50 12/04/2023 06:27 WG2182129
Dibromomethane U 6.10 50.0 50 12/04/2023 06:27 WG2182129
1,2-Dichlorobenzene U 5.35 50.0 50 12/04/2023 06:27 WG2182129
1,3-Dichlorobenzene U 5.50 50.0 50 12/04/2023 06:27 WG2182129
1,4-Dichlorobenzene U 6.00 50.0 50 12/04/2023 06:27 WG2182129
Dichlorodifluoromethane U 18.7 250 50 12/04/2023 06:27 WG2182129
1,1-Dichloroethane U 5.00 50.0 50 12/04/2023 06:27 WG2182129
1,2-Dichloroethane U 4.09 50.0 50 12/04/2023 06:27 WG2182129
1,1-Dichloroethene U 9.40 50.0 50 12/04/2023 06:27 WG2182129
cis-1,2-Dichloroethene U 6.30 50.0 50 12/04/2023 06:27 WG2182129
trans-1,2-Dichloroethene U 7.45 50.0 50 12/04/2023 06:27 WG2182129
1,2-Dichloropropane U 7.45 50.0 50 12/04/2023 06:27 WG2182129
1,1-Dichloropropene U 7.10 50.0 50 12/04/2023 06:27 WG2182129
1,3-Dichloropropane U 5.50 50.0 50 12/04/2023 06:27 WG2182129
cis-1,3-Dichloropropene U 5.55 50.0 50 12/04/2023 06:27 WG2182129
trans-1,3-Dichloropropene U 5.90 50.0 50 12/04/2023 06:27 WG2182129
2,2-Dichloropropane U 8.05 50.0 50 12/04/2023 06:27 WG2182129
Di-isopropyl ether 6.05 J 5.25 50.0 50 12/04/2023 06:27 WG2182129
Ethylbenzene 89.2 6.85 50.0 50 12/04/2023 06:27 WG2182129
Hexachloro-1,3-butadiene U 16.9 50.0 50 12/04/2023 06:27 WG2182129
Isopropylbenzene 12.3 J 5.25 50.0 50 12/04/2023 06:27 WG2182129
Methylene Chloride U 21.5 250 50 12/04/2023 06:27 WG2182129
Methyl tert-butyl ether 7.05 J 5.05 50.0 50 12/04/2023 06:27 WG2182129
Naphthalene U 50.0 250 50 12/04/2023 06:27 WG2182129
n-Propylbenzene 9.95 J 4.97 50.0 50 12/04/2023 06:27 WG2182129
Styrene U 5.90 50.0 50 12/04/2023 06:27 WG2182129
1,1,1,2-Tetrachloroethane U 7.35 50.0 50 12/04/2023 06:27 WG2182129
1,1,2,2-Tetrachloroethane U 6.65 50.0 50 12/04/2023 06:27 WG2182129
Tetrachloroethene U 15.0 50.0 50 12/04/2023 06:27 WG2182129
Toluene 105 13.9 50.0 50 12/04/2023 06:27 WG2182129
1,2,3-Trichlorobenzene U 11.5 50.0 50 12/04/2023 06:27 WG2182129
1,2,4-Trichlorobenzene U 24.1 50.0 50 12/04/2023 06:27 WG2182129
1,1,1-Trichloroethane U 7.45 50.0 50 12/04/2023 06:27 WG2182129
1,1,2-Trichloroethane U 7.90 50.0 50 12/04/2023 06:27 WG2182129
Trichloroethene U 9.50 50.0 50 12/04/2023 06:27 WG2182129
Trichlorofluoromethane U 8.00 250 50 12/04/2023 06:27 WG2182129
1,2,3-Trichloropropane U 11.9 125 50 12/04/2023 06:27 WG2182129
1,2,4-Trimethylbenzene 38.1 J 16.1 50.0 50 12/04/2023 06:27 WG2182129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 8 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 8 of 32
SAMPLE RESULTS - 02
L1682629
MW-4D
Collected date/time: 11/29/23 11:40
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene 17.1 J 5.20 50.0 50 12/04/2023 06:27 WG2182129
Vinyl chloride U 11.7 50.0 50 12/04/2023 06:27 WG2182129
o-Xylene 254 8.70 50.0 50 12/04/2023 06:27 WG2182129
m&p-Xylenes 108 21.5 100 50 12/04/2023 06:27 WG2182129
ethanol U C4 2100 5000 50 12/04/2023 22:45 WG2182350
tert-Amyl Methyl Ether U 9.75 50.0 50 12/04/2023 06:27 WG2182129
Ethyl tert-butyl ether U 5.05 50.0 50 12/04/2023 06:27 WG2182129
tert-Butyl alcohol U 203 250 50 12/04/2023 06:27 WG2182129
t-Amyl Alcohol 566 J 245 2500 50 12/04/2023 06:27 WG2182129
tert-Butyl formate U C4 226 1000 50 12/04/2023 22:45 WG2182350
(S) Toluene-d8 101 80.0-120 12/04/2023 06:27 WG2182129
(S) Toluene-d8 112 80.0-120 12/04/2023 22:45 WG2182350
(S) 4-Bromofluorobenzene 97.9 77.0-126 12/04/2023 06:27 WG2182129
(S) 4-Bromofluorobenzene 92.0 77.0-126 12/04/2023 22:45 WG2182350
(S) 1,2-Dichloroethane-d4 99.7 70.0-130 12/04/2023 06:27 WG2182129
(S) 1,2-Dichloroethane-d4 97.6 70.0-130 12/04/2023 22:45 WG2182350
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 50.9 B J 33.3 100 1 12/05/2023 09:15 WG2182322
Unadjusted C19-C36 Aliphatics 41.5 B J 33.3 100 1 12/05/2023 09:15 WG2182322
Unadjusted C11-C22 Aromatics 122 B 33.3 100 1 12/05/2023 09:21 WG2182322
Unadjusted Total Petroleum
Hydrocarbons 214 33.3 100 1 12/05/2023 09:21 WG2182322
(S) o-Terphenyl 72.9 40.0-140 12/05/2023 09:21 WG2182322
(S) 1-Chloro-octadecane 50.3 40.0-140 12/05/2023 09:15 WG2182322
(S) 2-Fluorobiphenyl 88.4 40.0-140 12/05/2023 09:21 WG2182322
(S) 2-Bromonaphthalene 93.4 40.0-140 12/05/2023 09:21 WG2182322
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 12/01/2023 17:23 WG2180281
Acenaphthylene U 0.0921 1.00 1 12/01/2023 17:23 WG2180281
Anthracene U 0.0804 1.00 1 12/01/2023 17:23 WG2180281
Benzo(a)anthracene U 0.199 1.00 1 12/01/2023 17:23 WG2180281
Benzo(b)fluoranthene U 0.130 1.00 1 12/01/2023 17:23 WG2180281
Benzo(k)fluoranthene U 0.120 1.00 1 12/01/2023 17:23 WG2180281
Benzo(g,h,i)perylene U 0.121 1.00 1 12/01/2023 17:23 WG2180281
Benzo(a)pyrene U 0.0381 1.00 1 12/01/2023 17:23 WG2180281
Bis(2-chlorethoxy)methane U 0.116 10.0 1 12/01/2023 17:23 WG2180281
Bis(2-chloroethyl)ether U 0.137 10.0 1 12/01/2023 17:23 WG2180281
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 12/01/2023 17:23 WG2180281
4-Bromophenyl-phenylether U 0.0877 10.0 1 12/01/2023 17:23 WG2180281
2-Chloronaphthalene U 0.0648 1.00 1 12/01/2023 17:23 WG2180281
4-Chlorophenyl-phenylether U 0.0926 10.0 1 12/01/2023 17:23 WG2180281
Chrysene U 0.130 1.00 1 12/01/2023 17:23 WG2180281
Dibenz(a,h)anthracene U 0.0644 1.00 1 12/01/2023 17:23 WG2180281
3,3-Dichlorobenzidine U 0.212 10.0 1 12/01/2023 17:23 WG2180281
2,4-Dinitrotoluene U 0.0983 10.0 1 12/01/2023 17:23 WG2180281
2,6-Dinitrotoluene U 0.250 10.0 1 12/01/2023 17:23 WG2180281
Fluoranthene U 0.102 1.00 1 12/01/2023 17:23 WG2180281
Fluorene U 0.0844 1.00 1 12/01/2023 17:23 WG2180281
Hexachlorobenzene U 0.0755 1.00 1 12/01/2023 17:23 WG2180281
Hexachloro-1,3-butadiene U 0.0968 10.0 1 12/01/2023 17:23 WG2180281
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 9 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 9 of 32
SAMPLE RESULTS - 02
L1682629
MW-4D
Collected date/time: 11/29/23 11:40
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexachlorocyclopentadiene U 0.0598 10.0 1 12/01/2023 17:23 WG2180281
Hexachloroethane U 0.127 10.0 1 12/01/2023 17:23 WG2180281
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 12/01/2023 17:23 WG2180281
Isophorone U 0.143 10.0 1 12/01/2023 17:23 WG2180281
Naphthalene 18.6 0.159 1.00 1 12/01/2023 17:23 WG2180281
Nitrobenzene U 0.297 10.0 1 12/01/2023 17:23 WG2180281
n-Nitrosodimethylamine U 0.998 10.0 1 12/01/2023 17:23 WG2180281
n-Nitrosodiphenylamine U 2.37 10.0 1 12/01/2023 17:23 WG2180281
n-Nitrosodi-n-propylamine U 0.261 10.0 1 12/01/2023 17:23 WG2180281
Phenanthrene U 0.112 1.00 1 12/01/2023 17:23 WG2180281
Benzylbutyl phthalate U 0.765 3.00 1 12/01/2023 17:23 WG2180281
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 12/01/2023 17:23 WG2180281
Di-n-butyl phthalate U 0.453 3.00 1 12/01/2023 17:23 WG2180281
Diethyl phthalate U 0.287 3.00 1 12/01/2023 17:23 WG2180281
Dimethyl phthalate U 0.260 3.00 1 12/01/2023 17:23 WG2180281
Di-n-octyl phthalate U 0.932 3.00 1 12/01/2023 17:23 WG2180281
Pyrene U 0.107 1.00 1 12/01/2023 17:23 WG2180281
1,2,4-Trichlorobenzene U 0.0698 10.0 1 12/01/2023 17:23 WG2180281
4-Chloro-3-methylphenol U 0.131 10.0 1 12/01/2023 17:23 WG2180281
2-Chlorophenol U 0.133 10.0 1 12/01/2023 17:23 WG2180281
2,4-Dichlorophenol U 0.102 10.0 1 12/01/2023 17:23 WG2180281
2,4-Dimethylphenol U 0.0636 10.0 1 12/01/2023 17:23 WG2180281
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 12/01/2023 17:23 WG2180281
2,4-Dinitrophenol U 5.93 10.0 1 12/01/2023 17:23 WG2180281
2-Nitrophenol U 0.117 10.0 1 12/01/2023 17:23 WG2180281
4-Nitrophenol U 0.143 10.0 1 12/01/2023 17:23 WG2180281
Pentachlorophenol U 0.313 10.0 1 12/01/2023 17:23 WG2180281
Phenol U 4.33 10.0 1 12/01/2023 17:23 WG2180281
2,4,6-Trichlorophenol U 0.100 10.0 1 12/01/2023 17:23 WG2180281
(S) Nitrobenzene-d5 81.3 15.0-314 12/01/2023 17:23 WG2180281
(S) 2-Fluorobiphenyl 67.4 22.0-127 12/01/2023 17:23 WG2180281
(S) p-Terphenyl-d14 82.7 29.0-141 12/01/2023 17:23 WG2180281
(S) Phenol-d5 27.1 8.00-424 12/01/2023 17:23 WG2180281
(S) 2-Fluorophenol 38.1 10.0-120 12/01/2023 17:23 WG2180281
(S) 2,4,6-Tribromophenol 76.3 10.0-153 12/01/2023 17:23 WG2180281
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 10 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 10 of 32
SAMPLE RESULTS - 03
L1682629
MW-5D
Collected date/time: 11/29/23 10:10
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.0941 1.00 1 12/04/2023 05:47 WG2182129
Bromobenzene U 0.118 1.00 1 12/04/2023 05:47 WG2182129
Bromodichloromethane U 0.136 1.00 1 12/04/2023 05:47 WG2182129
Bromochloromethane U 0.128 1.00 1 12/04/2023 05:47 WG2182129
Bromoform U 0.129 1.00 1 12/04/2023 05:47 WG2182129
Bromomethane U 0.605 5.00 1 12/04/2023 05:47 WG2182129
n-Butylbenzene U 0.157 1.00 1 12/04/2023 05:47 WG2182129
sec-Butylbenzene U 0.125 1.00 1 12/04/2023 05:47 WG2182129
tert-Butylbenzene U J4 0.127 1.00 1 12/04/2023 05:47 WG2182129
Carbon tetrachloride U 0.128 1.00 1 12/04/2023 05:47 WG2182129
Chlorobenzene U 0.116 1.00 1 12/04/2023 05:47 WG2182129
Chlorodibromomethane U 0.140 1.00 1 12/04/2023 05:47 WG2182129
Chloroethane U 0.192 5.00 1 12/04/2023 05:47 WG2182129
Chloroform U 0.111 5.00 1 12/04/2023 05:47 WG2182129
Chloromethane U 0.960 2.50 1 12/04/2023 05:47 WG2182129
2-Chlorotoluene U 0.106 1.00 1 12/04/2023 05:47 WG2182129
4-Chlorotoluene U 0.114 1.00 1 12/04/2023 05:47 WG2182129
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 12/04/2023 05:47 WG2182129
1,2-Dibromoethane U 0.126 1.00 1 12/04/2023 05:47 WG2182129
Dibromomethane U 0.122 1.00 1 12/04/2023 05:47 WG2182129
1,2-Dichlorobenzene U 0.107 1.00 1 12/04/2023 05:47 WG2182129
1,3-Dichlorobenzene U 0.110 1.00 1 12/04/2023 05:47 WG2182129
1,4-Dichlorobenzene U 0.120 1.00 1 12/04/2023 05:47 WG2182129
Dichlorodifluoromethane U 0.374 5.00 1 12/04/2023 05:47 WG2182129
1,1-Dichloroethane U 0.100 1.00 1 12/04/2023 05:47 WG2182129
1,2-Dichloroethane U 0.0819 1.00 1 12/04/2023 05:47 WG2182129
1,1-Dichloroethene U 0.188 1.00 1 12/04/2023 05:47 WG2182129
cis-1,2-Dichloroethene U 0.126 1.00 1 12/04/2023 05:47 WG2182129
trans-1,2-Dichloroethene U 0.149 1.00 1 12/04/2023 05:47 WG2182129
1,2-Dichloropropane U 0.149 1.00 1 12/04/2023 05:47 WG2182129
1,1-Dichloropropene U 0.142 1.00 1 12/04/2023 05:47 WG2182129
1,3-Dichloropropane U 0.110 1.00 1 12/04/2023 05:47 WG2182129
cis-1,3-Dichloropropene U 0.111 1.00 1 12/04/2023 05:47 WG2182129
trans-1,3-Dichloropropene U 0.118 1.00 1 12/04/2023 05:47 WG2182129
2,2-Dichloropropane U 0.161 1.00 1 12/04/2023 05:47 WG2182129
Di-isopropyl ether U 0.105 1.00 1 12/04/2023 05:47 WG2182129
Ethylbenzene U 0.137 1.00 1 12/04/2023 05:47 WG2182129
Hexachloro-1,3-butadiene U 0.337 1.00 1 12/04/2023 05:47 WG2182129
Isopropylbenzene U 0.105 1.00 1 12/04/2023 05:47 WG2182129
Methylene Chloride U 0.430 5.00 1 12/04/2023 05:47 WG2182129
Methyl tert-butyl ether U 0.101 1.00 1 12/04/2023 05:47 WG2182129
Naphthalene U 1.00 5.00 1 12/04/2023 05:47 WG2182129
n-Propylbenzene U 0.0993 1.00 1 12/04/2023 05:47 WG2182129
Styrene U 0.118 1.00 1 12/04/2023 05:47 WG2182129
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 12/04/2023 05:47 WG2182129
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 12/04/2023 05:47 WG2182129
Tetrachloroethene U 0.300 1.00 1 12/04/2023 05:47 WG2182129
Toluene U 0.278 1.00 1 12/04/2023 05:47 WG2182129
1,2,3-Trichlorobenzene U 0.230 1.00 1 12/04/2023 05:47 WG2182129
1,2,4-Trichlorobenzene U 0.481 1.00 1 12/04/2023 05:47 WG2182129
1,1,1-Trichloroethane U 0.149 1.00 1 12/04/2023 05:47 WG2182129
1,1,2-Trichloroethane U 0.158 1.00 1 12/04/2023 05:47 WG2182129
Trichloroethene U 0.190 1.00 1 12/04/2023 05:47 WG2182129
Trichlorofluoromethane U 0.160 5.00 1 12/04/2023 05:47 WG2182129
1,2,3-Trichloropropane U 0.237 2.50 1 12/04/2023 05:47 WG2182129
1,2,4-Trimethylbenzene U 0.322 1.00 1 12/04/2023 05:47 WG2182129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 11 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 11 of 32
SAMPLE RESULTS - 03
L1682629
MW-5D
Collected date/time: 11/29/23 10:10
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene U 0.104 1.00 1 12/04/2023 05:47 WG2182129
Vinyl chloride U 0.234 1.00 1 12/04/2023 05:47 WG2182129
o-Xylene U 0.174 1.00 1 12/04/2023 05:47 WG2182129
m&p-Xylenes U 0.430 2.00 1 12/04/2023 05:47 WG2182129
ethanol U C4 42.0 100 1 12/04/2023 21:43 WG2182350
tert-Amyl Methyl Ether U 0.195 1.00 1 12/04/2023 05:47 WG2182129
Ethyl tert-butyl ether U 0.101 1.00 1 12/04/2023 05:47 WG2182129
tert-Butyl alcohol U 4.06 5.00 1 12/04/2023 05:47 WG2182129
t-Amyl Alcohol U 4.90 50.0 1 12/04/2023 05:47 WG2182129
tert-Butyl formate U C4 4.51 20.0 1 12/04/2023 21:43 WG2182350
(S) Toluene-d8 103 80.0-120 12/04/2023 05:47 WG2182129
(S) Toluene-d8 111 80.0-120 12/04/2023 21:43 WG2182350
(S) 4-Bromofluorobenzene 91.4 77.0-126 12/04/2023 05:47 WG2182129
(S) 4-Bromofluorobenzene 88.6 77.0-126 12/04/2023 21:43 WG2182350
(S) 1,2-Dichloroethane-d4 100 70.0-130 12/04/2023 05:47 WG2182129
(S) 1,2-Dichloroethane-d4 99.3 70.0-130 12/04/2023 21:43 WG2182350
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 42.0 B J 33.3 100 1 12/05/2023 09:39 WG2182322
Unadjusted C19-C36 Aliphatics 53.0 B J 33.3 100 1 12/05/2023 09:39 WG2182322
Unadjusted C11-C22 Aromatics 80.9 B J 33.3 100 1 12/05/2023 09:43 WG2182322
Unadjusted Total Petroleum
Hydrocarbons 176 33.3 100 1 12/05/2023 09:43 WG2182322
(S) o-Terphenyl 76.1 40.0-140 12/05/2023 09:43 WG2182322
(S) 1-Chloro-octadecane 44.7 40.0-140 12/05/2023 09:39 WG2182322
(S) 2-Fluorobiphenyl 92.9 40.0-140 12/05/2023 09:43 WG2182322
(S) 2-Bromonaphthalene 98.4 40.0-140 12/05/2023 09:43 WG2182322
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 12/01/2023 17:44 WG2180281
Acenaphthylene U 0.0921 1.00 1 12/01/2023 17:44 WG2180281
Anthracene U 0.0804 1.00 1 12/01/2023 17:44 WG2180281
Benzo(a)anthracene U 0.199 1.00 1 12/01/2023 17:44 WG2180281
Benzo(b)fluoranthene U 0.130 1.00 1 12/01/2023 17:44 WG2180281
Benzo(k)fluoranthene U 0.120 1.00 1 12/01/2023 17:44 WG2180281
Benzo(g,h,i)perylene U 0.121 1.00 1 12/01/2023 17:44 WG2180281
Benzo(a)pyrene U 0.0381 1.00 1 12/01/2023 17:44 WG2180281
Bis(2-chlorethoxy)methane U 0.116 10.0 1 12/01/2023 17:44 WG2180281
Bis(2-chloroethyl)ether U 0.137 10.0 1 12/01/2023 17:44 WG2180281
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 12/01/2023 17:44 WG2180281
4-Bromophenyl-phenylether U 0.0877 10.0 1 12/01/2023 17:44 WG2180281
2-Chloronaphthalene U 0.0648 1.00 1 12/01/2023 17:44 WG2180281
4-Chlorophenyl-phenylether U 0.0926 10.0 1 12/01/2023 17:44 WG2180281
Chrysene U 0.130 1.00 1 12/01/2023 17:44 WG2180281
Dibenz(a,h)anthracene U 0.0644 1.00 1 12/01/2023 17:44 WG2180281
3,3-Dichlorobenzidine U 0.212 10.0 1 12/01/2023 17:44 WG2180281
2,4-Dinitrotoluene U 0.0983 10.0 1 12/01/2023 17:44 WG2180281
2,6-Dinitrotoluene U 0.250 10.0 1 12/01/2023 17:44 WG2180281
Fluoranthene U 0.102 1.00 1 12/01/2023 17:44 WG2180281
Fluorene U 0.0844 1.00 1 12/01/2023 17:44 WG2180281
Hexachlorobenzene U 0.0755 1.00 1 12/01/2023 17:44 WG2180281
Hexachloro-1,3-butadiene U 0.0968 10.0 1 12/01/2023 17:44 WG2180281
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 12 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 12 of 32
SAMPLE RESULTS - 03
L1682629
MW-5D
Collected date/time: 11/29/23 10:10
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexachlorocyclopentadiene U 0.0598 10.0 1 12/01/2023 17:44 WG2180281
Hexachloroethane U 0.127 10.0 1 12/01/2023 17:44 WG2180281
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 12/01/2023 17:44 WG2180281
Isophorone U 0.143 10.0 1 12/01/2023 17:44 WG2180281
Naphthalene U 0.159 1.00 1 12/01/2023 17:44 WG2180281
Nitrobenzene U 0.297 10.0 1 12/01/2023 17:44 WG2180281
n-Nitrosodimethylamine U 0.998 10.0 1 12/01/2023 17:44 WG2180281
n-Nitrosodiphenylamine U 2.37 10.0 1 12/01/2023 17:44 WG2180281
n-Nitrosodi-n-propylamine U 0.261 10.0 1 12/01/2023 17:44 WG2180281
Phenanthrene U 0.112 1.00 1 12/01/2023 17:44 WG2180281
Benzylbutyl phthalate U 0.765 3.00 1 12/01/2023 17:44 WG2180281
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 12/01/2023 17:44 WG2180281
Di-n-butyl phthalate U 0.453 3.00 1 12/01/2023 17:44 WG2180281
Diethyl phthalate U 0.287 3.00 1 12/01/2023 17:44 WG2180281
Dimethyl phthalate U 0.260 3.00 1 12/01/2023 17:44 WG2180281
Di-n-octyl phthalate U 0.932 3.00 1 12/01/2023 17:44 WG2180281
Pyrene U 0.107 1.00 1 12/01/2023 17:44 WG2180281
1,2,4-Trichlorobenzene U 0.0698 10.0 1 12/01/2023 17:44 WG2180281
4-Chloro-3-methylphenol U 0.131 10.0 1 12/01/2023 17:44 WG2180281
2-Chlorophenol U 0.133 10.0 1 12/01/2023 17:44 WG2180281
2,4-Dichlorophenol U 0.102 10.0 1 12/01/2023 17:44 WG2180281
2,4-Dimethylphenol U 0.0636 10.0 1 12/01/2023 17:44 WG2180281
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 12/01/2023 17:44 WG2180281
2,4-Dinitrophenol U 5.93 10.0 1 12/01/2023 17:44 WG2180281
2-Nitrophenol U 0.117 10.0 1 12/01/2023 17:44 WG2180281
4-Nitrophenol U 0.143 10.0 1 12/01/2023 17:44 WG2180281
Pentachlorophenol U 0.313 10.0 1 12/01/2023 17:44 WG2180281
Phenol U 4.33 10.0 1 12/01/2023 17:44 WG2180281
2,4,6-Trichlorophenol U 0.100 10.0 1 12/01/2023 17:44 WG2180281
(S) Nitrobenzene-d5 68.3 15.0-314 12/01/2023 17:44 WG2180281
(S) 2-Fluorobiphenyl 53.9 22.0-127 12/01/2023 17:44 WG2180281
(S) p-Terphenyl-d14 73.5 29.0-141 12/01/2023 17:44 WG2180281
(S) Phenol-d5 21.7 8.00-424 12/01/2023 17:44 WG2180281
(S) 2-Fluorophenol 32.0 10.0-120 12/01/2023 17:44 WG2180281
(S) 2,4,6-Tribromophenol 64.5 10.0-153 12/01/2023 17:44 WG2180281
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 13 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 13 of 32
SAMPLE RESULTS - 04
L1682629
MW-6D
Collected date/time: 11/29/23 10:50
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.0941 1.00 1 12/04/2023 06:07 WG2182129
Bromobenzene U 0.118 1.00 1 12/04/2023 06:07 WG2182129
Bromodichloromethane U 0.136 1.00 1 12/04/2023 06:07 WG2182129
Bromochloromethane U 0.128 1.00 1 12/04/2023 06:07 WG2182129
Bromoform U 0.129 1.00 1 12/04/2023 06:07 WG2182129
Bromomethane U 0.605 5.00 1 12/04/2023 06:07 WG2182129
n-Butylbenzene U 0.157 1.00 1 12/04/2023 06:07 WG2182129
sec-Butylbenzene U 0.125 1.00 1 12/04/2023 06:07 WG2182129
tert-Butylbenzene U J4 0.127 1.00 1 12/04/2023 06:07 WG2182129
Carbon tetrachloride U 0.128 1.00 1 12/04/2023 06:07 WG2182129
Chlorobenzene U 0.116 1.00 1 12/04/2023 06:07 WG2182129
Chlorodibromomethane U 0.140 1.00 1 12/04/2023 06:07 WG2182129
Chloroethane U 0.192 5.00 1 12/04/2023 06:07 WG2182129
Chloroform U 0.111 5.00 1 12/04/2023 06:07 WG2182129
Chloromethane U 0.960 2.50 1 12/04/2023 06:07 WG2182129
2-Chlorotoluene U 0.106 1.00 1 12/04/2023 06:07 WG2182129
4-Chlorotoluene U 0.114 1.00 1 12/04/2023 06:07 WG2182129
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 12/04/2023 06:07 WG2182129
1,2-Dibromoethane U 0.126 1.00 1 12/04/2023 06:07 WG2182129
Dibromomethane U 0.122 1.00 1 12/04/2023 06:07 WG2182129
1,2-Dichlorobenzene U 0.107 1.00 1 12/04/2023 06:07 WG2182129
1,3-Dichlorobenzene U 0.110 1.00 1 12/04/2023 06:07 WG2182129
1,4-Dichlorobenzene U 0.120 1.00 1 12/04/2023 06:07 WG2182129
Dichlorodifluoromethane U 0.374 5.00 1 12/04/2023 06:07 WG2182129
1,1-Dichloroethane U 0.100 1.00 1 12/04/2023 06:07 WG2182129
1,2-Dichloroethane U 0.0819 1.00 1 12/04/2023 06:07 WG2182129
1,1-Dichloroethene U 0.188 1.00 1 12/04/2023 06:07 WG2182129
cis-1,2-Dichloroethene U 0.126 1.00 1 12/04/2023 06:07 WG2182129
trans-1,2-Dichloroethene U 0.149 1.00 1 12/04/2023 06:07 WG2182129
1,2-Dichloropropane U 0.149 1.00 1 12/04/2023 06:07 WG2182129
1,1-Dichloropropene U 0.142 1.00 1 12/04/2023 06:07 WG2182129
1,3-Dichloropropane U 0.110 1.00 1 12/04/2023 06:07 WG2182129
cis-1,3-Dichloropropene U 0.111 1.00 1 12/04/2023 06:07 WG2182129
trans-1,3-Dichloropropene U 0.118 1.00 1 12/04/2023 06:07 WG2182129
2,2-Dichloropropane U 0.161 1.00 1 12/04/2023 06:07 WG2182129
Di-isopropyl ether U 0.105 1.00 1 12/04/2023 06:07 WG2182129
Ethylbenzene U 0.137 1.00 1 12/04/2023 06:07 WG2182129
Hexachloro-1,3-butadiene U 0.337 1.00 1 12/04/2023 06:07 WG2182129
Isopropylbenzene U 0.105 1.00 1 12/04/2023 06:07 WG2182129
Methylene Chloride U 0.430 5.00 1 12/04/2023 06:07 WG2182129
Methyl tert-butyl ether U 0.101 1.00 1 12/04/2023 06:07 WG2182129
Naphthalene U 1.00 5.00 1 12/04/2023 06:07 WG2182129
n-Propylbenzene U 0.0993 1.00 1 12/04/2023 06:07 WG2182129
Styrene U 0.118 1.00 1 12/04/2023 06:07 WG2182129
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 12/04/2023 06:07 WG2182129
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 12/04/2023 06:07 WG2182129
Tetrachloroethene U 0.300 1.00 1 12/04/2023 06:07 WG2182129
Toluene U 0.278 1.00 1 12/04/2023 06:07 WG2182129
1,2,3-Trichlorobenzene U 0.230 1.00 1 12/04/2023 06:07 WG2182129
1,2,4-Trichlorobenzene U 0.481 1.00 1 12/04/2023 06:07 WG2182129
1,1,1-Trichloroethane U 0.149 1.00 1 12/04/2023 06:07 WG2182129
1,1,2-Trichloroethane U 0.158 1.00 1 12/04/2023 06:07 WG2182129
Trichloroethene U 0.190 1.00 1 12/04/2023 06:07 WG2182129
Trichlorofluoromethane 0.980 J 0.160 5.00 1 12/04/2023 06:07 WG2182129
1,2,3-Trichloropropane U 0.237 2.50 1 12/04/2023 06:07 WG2182129
1,2,4-Trimethylbenzene U 0.322 1.00 1 12/04/2023 06:07 WG2182129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 14 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 14 of 32
SAMPLE RESULTS - 04
L1682629
MW-6D
Collected date/time: 11/29/23 10:50
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene U 0.104 1.00 1 12/04/2023 06:07 WG2182129
Vinyl chloride U 0.234 1.00 1 12/04/2023 06:07 WG2182129
o-Xylene U 0.174 1.00 1 12/04/2023 06:07 WG2182129
m&p-Xylenes U 0.430 2.00 1 12/04/2023 06:07 WG2182129
ethanol U C4 42.0 100 1 12/04/2023 22:04 WG2182350
tert-Amyl Methyl Ether U 0.195 1.00 1 12/04/2023 06:07 WG2182129
Ethyl tert-butyl ether U 0.101 1.00 1 12/04/2023 06:07 WG2182129
tert-Butyl alcohol U 4.06 5.00 1 12/04/2023 06:07 WG2182129
t-Amyl Alcohol U 4.90 50.0 1 12/04/2023 06:07 WG2182129
tert-Butyl formate U C4 4.51 20.0 1 12/04/2023 22:04 WG2182350
(S) Toluene-d8 104 80.0-120 12/04/2023 06:07 WG2182129
(S) Toluene-d8 117 80.0-120 12/04/2023 22:04 WG2182350
(S) 4-Bromofluorobenzene 94.3 77.0-126 12/04/2023 06:07 WG2182129
(S) 4-Bromofluorobenzene 88.6 77.0-126 12/04/2023 22:04 WG2182350
(S) 1,2-Dichloroethane-d4 103 70.0-130 12/04/2023 06:07 WG2182129
(S) 1,2-Dichloroethane-d4 99.6 70.0-130 12/04/2023 22:04 WG2182350
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 36.8 B J 33.3 100 1 12/05/2023 10:03 WG2182322
Unadjusted C19-C36 Aliphatics 48.7 B J 33.3 100 1 12/05/2023 10:03 WG2182322
Unadjusted C11-C22 Aromatics 82.7 B J 33.3 100 1 12/05/2023 10:05 WG2182322
Unadjusted Total Petroleum
Hydrocarbons 168 33.3 100 1 12/05/2023 10:05 WG2182322
(S) o-Terphenyl 77.6 40.0-140 12/05/2023 10:05 WG2182322
(S) 1-Chloro-octadecane 55.5 40.0-140 12/05/2023 10:03 WG2182322
(S) 2-Fluorobiphenyl 91.8 40.0-140 12/05/2023 10:05 WG2182322
(S) 2-Bromonaphthalene 98.2 40.0-140 12/05/2023 10:05 WG2182322
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 12/01/2023 18:05 WG2180281
Acenaphthylene U 0.0921 1.00 1 12/01/2023 18:05 WG2180281
Anthracene U 0.0804 1.00 1 12/01/2023 18:05 WG2180281
Benzo(a)anthracene U 0.199 1.00 1 12/01/2023 18:05 WG2180281
Benzo(b)fluoranthene U 0.130 1.00 1 12/01/2023 18:05 WG2180281
Benzo(k)fluoranthene U 0.120 1.00 1 12/01/2023 18:05 WG2180281
Benzo(g,h,i)perylene U 0.121 1.00 1 12/01/2023 18:05 WG2180281
Benzo(a)pyrene U 0.0381 1.00 1 12/01/2023 18:05 WG2180281
Bis(2-chlorethoxy)methane U 0.116 10.0 1 12/01/2023 18:05 WG2180281
Bis(2-chloroethyl)ether U 0.137 10.0 1 12/01/2023 18:05 WG2180281
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 12/01/2023 18:05 WG2180281
4-Bromophenyl-phenylether U 0.0877 10.0 1 12/01/2023 18:05 WG2180281
2-Chloronaphthalene U 0.0648 1.00 1 12/01/2023 18:05 WG2180281
4-Chlorophenyl-phenylether U 0.0926 10.0 1 12/01/2023 18:05 WG2180281
Chrysene U 0.130 1.00 1 12/01/2023 18:05 WG2180281
Dibenz(a,h)anthracene U 0.0644 1.00 1 12/01/2023 18:05 WG2180281
3,3-Dichlorobenzidine U 0.212 10.0 1 12/01/2023 18:05 WG2180281
2,4-Dinitrotoluene U 0.0983 10.0 1 12/01/2023 18:05 WG2180281
2,6-Dinitrotoluene U 0.250 10.0 1 12/01/2023 18:05 WG2180281
Fluoranthene U 0.102 1.00 1 12/01/2023 18:05 WG2180281
Fluorene U 0.0844 1.00 1 12/01/2023 18:05 WG2180281
Hexachlorobenzene U 0.0755 1.00 1 12/01/2023 18:05 WG2180281
Hexachloro-1,3-butadiene U 0.0968 10.0 1 12/01/2023 18:05 WG2180281
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 15 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 15 of 32
SAMPLE RESULTS - 04
L1682629
MW-6D
Collected date/time: 11/29/23 10:50
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexachlorocyclopentadiene U 0.0598 10.0 1 12/01/2023 18:05 WG2180281
Hexachloroethane U 0.127 10.0 1 12/01/2023 18:05 WG2180281
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 12/01/2023 18:05 WG2180281
Isophorone U 0.143 10.0 1 12/01/2023 18:05 WG2180281
Naphthalene U 0.159 1.00 1 12/01/2023 18:05 WG2180281
Nitrobenzene U 0.297 10.0 1 12/01/2023 18:05 WG2180281
n-Nitrosodimethylamine U 0.998 10.0 1 12/01/2023 18:05 WG2180281
n-Nitrosodiphenylamine U 2.37 10.0 1 12/01/2023 18:05 WG2180281
n-Nitrosodi-n-propylamine U 0.261 10.0 1 12/01/2023 18:05 WG2180281
Phenanthrene U 0.112 1.00 1 12/01/2023 18:05 WG2180281
Benzylbutyl phthalate U 0.765 3.00 1 12/01/2023 18:05 WG2180281
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 12/01/2023 18:05 WG2180281
Di-n-butyl phthalate U 0.453 3.00 1 12/01/2023 18:05 WG2180281
Diethyl phthalate U 0.287 3.00 1 12/01/2023 18:05 WG2180281
Dimethyl phthalate U 0.260 3.00 1 12/01/2023 18:05 WG2180281
Di-n-octyl phthalate U 0.932 3.00 1 12/01/2023 18:05 WG2180281
Pyrene U 0.107 1.00 1 12/01/2023 18:05 WG2180281
1,2,4-Trichlorobenzene U 0.0698 10.0 1 12/01/2023 18:05 WG2180281
4-Chloro-3-methylphenol U 0.131 10.0 1 12/01/2023 18:05 WG2180281
2-Chlorophenol U 0.133 10.0 1 12/01/2023 18:05 WG2180281
2,4-Dichlorophenol U 0.102 10.0 1 12/01/2023 18:05 WG2180281
2,4-Dimethylphenol U 0.0636 10.0 1 12/01/2023 18:05 WG2180281
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 12/01/2023 18:05 WG2180281
2,4-Dinitrophenol U 5.93 10.0 1 12/01/2023 18:05 WG2180281
2-Nitrophenol U 0.117 10.0 1 12/01/2023 18:05 WG2180281
4-Nitrophenol U 0.143 10.0 1 12/01/2023 18:05 WG2180281
Pentachlorophenol U 0.313 10.0 1 12/01/2023 18:05 WG2180281
Phenol U 4.33 10.0 1 12/01/2023 18:05 WG2180281
2,4,6-Trichlorophenol U 0.100 10.0 1 12/01/2023 18:05 WG2180281
(S) Nitrobenzene-d5 56.0 15.0-314 12/01/2023 18:05 WG2180281
(S) 2-Fluorobiphenyl 44.2 22.0-127 12/01/2023 18:05 WG2180281
(S) p-Terphenyl-d14 62.3 29.0-141 12/01/2023 18:05 WG2180281
(S) Phenol-d5 16.2 8.00-424 12/01/2023 18:05 WG2180281
(S) 2-Fluorophenol 21.7 10.0-120 12/01/2023 18:05 WG2180281
(S) 2,4,6-Tribromophenol 48.5 10.0-153 12/01/2023 18:05 WG2180281
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 16 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 16 of 32
SAMPLE RESULTS - 05
L1682629
TRIP BLANK
Collected date/time: 11/29/23 00:00
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.0941 1.00 1 12/04/2023 02:29 WG2182129
Bromobenzene U 0.118 1.00 1 12/04/2023 02:29 WG2182129
Bromodichloromethane U 0.136 1.00 1 12/04/2023 02:29 WG2182129
Bromochloromethane U 0.128 1.00 1 12/04/2023 02:29 WG2182129
Bromoform U 0.129 1.00 1 12/04/2023 02:29 WG2182129
Bromomethane U 0.605 5.00 1 12/04/2023 02:29 WG2182129
n-Butylbenzene U 0.157 1.00 1 12/04/2023 02:29 WG2182129
sec-Butylbenzene U 0.125 1.00 1 12/04/2023 02:29 WG2182129
tert-Butylbenzene U J4 0.127 1.00 1 12/04/2023 02:29 WG2182129
Carbon tetrachloride U 0.128 1.00 1 12/04/2023 02:29 WG2182129
Chlorobenzene U 0.116 1.00 1 12/04/2023 02:29 WG2182129
Chlorodibromomethane U 0.140 1.00 1 12/04/2023 02:29 WG2182129
Chloroethane U 0.192 5.00 1 12/04/2023 02:29 WG2182129
Chloroform U 0.111 5.00 1 12/04/2023 02:29 WG2182129
Chloromethane U 0.960 2.50 1 12/04/2023 02:29 WG2182129
2-Chlorotoluene U 0.106 1.00 1 12/04/2023 02:29 WG2182129
4-Chlorotoluene U 0.114 1.00 1 12/04/2023 02:29 WG2182129
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 12/04/2023 02:29 WG2182129
1,2-Dibromoethane U 0.126 1.00 1 12/04/2023 02:29 WG2182129
Dibromomethane U 0.122 1.00 1 12/04/2023 02:29 WG2182129
1,2-Dichlorobenzene U 0.107 1.00 1 12/04/2023 02:29 WG2182129
1,3-Dichlorobenzene U 0.110 1.00 1 12/04/2023 02:29 WG2182129
1,4-Dichlorobenzene U 0.120 1.00 1 12/04/2023 02:29 WG2182129
Dichlorodifluoromethane U 0.374 5.00 1 12/04/2023 02:29 WG2182129
1,1-Dichloroethane U 0.100 1.00 1 12/04/2023 02:29 WG2182129
1,2-Dichloroethane U 0.0819 1.00 1 12/04/2023 02:29 WG2182129
1,1-Dichloroethene U 0.188 1.00 1 12/04/2023 02:29 WG2182129
cis-1,2-Dichloroethene U 0.126 1.00 1 12/04/2023 02:29 WG2182129
trans-1,2-Dichloroethene U 0.149 1.00 1 12/04/2023 02:29 WG2182129
1,2-Dichloropropane U 0.149 1.00 1 12/04/2023 02:29 WG2182129
1,1-Dichloropropene U 0.142 1.00 1 12/04/2023 02:29 WG2182129
1,3-Dichloropropane U 0.110 1.00 1 12/04/2023 02:29 WG2182129
cis-1,3-Dichloropropene U 0.111 1.00 1 12/04/2023 02:29 WG2182129
trans-1,3-Dichloropropene U 0.118 1.00 1 12/04/2023 02:29 WG2182129
2,2-Dichloropropane U 0.161 1.00 1 12/04/2023 02:29 WG2182129
Di-isopropyl ether U 0.105 1.00 1 12/04/2023 02:29 WG2182129
Ethylbenzene U 0.137 1.00 1 12/04/2023 02:29 WG2182129
Hexachloro-1,3-butadiene U 0.337 1.00 1 12/04/2023 02:29 WG2182129
Isopropylbenzene U 0.105 1.00 1 12/04/2023 02:29 WG2182129
Methylene Chloride U 0.430 5.00 1 12/04/2023 02:29 WG2182129
Methyl tert-butyl ether U 0.101 1.00 1 12/04/2023 02:29 WG2182129
Naphthalene U 1.00 5.00 1 12/04/2023 02:29 WG2182129
n-Propylbenzene U 0.0993 1.00 1 12/04/2023 02:29 WG2182129
Styrene U 0.118 1.00 1 12/04/2023 02:29 WG2182129
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 12/04/2023 02:29 WG2182129
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 12/04/2023 02:29 WG2182129
Tetrachloroethene U 0.300 1.00 1 12/04/2023 02:29 WG2182129
Toluene U 0.278 1.00 1 12/04/2023 02:29 WG2182129
1,2,3-Trichlorobenzene U 0.230 1.00 1 12/04/2023 02:29 WG2182129
1,2,4-Trichlorobenzene U 0.481 1.00 1 12/04/2023 02:29 WG2182129
1,1,1-Trichloroethane U 0.149 1.00 1 12/04/2023 02:29 WG2182129
1,1,2-Trichloroethane U 0.158 1.00 1 12/04/2023 02:29 WG2182129
Trichloroethene U 0.190 1.00 1 12/04/2023 02:29 WG2182129
Trichlorofluoromethane U 0.160 5.00 1 12/04/2023 02:29 WG2182129
1,2,3-Trichloropropane U 0.237 2.50 1 12/04/2023 02:29 WG2182129
1,2,4-Trimethylbenzene U 0.322 1.00 1 12/04/2023 02:29 WG2182129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 17 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 17 of 32
SAMPLE RESULTS - 05
L1682629
TRIP BLANK
Collected date/time: 11/29/23 00:00
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,3,5-Trimethylbenzene U 0.104 1.00 1 12/04/2023 02:29 WG2182129
Vinyl chloride U 0.234 1.00 1 12/04/2023 02:29 WG2182129
o-Xylene U 0.174 1.00 1 12/04/2023 02:29 WG2182129
m&p-Xylenes U 0.430 2.00 1 12/04/2023 02:29 WG2182129
ethanol U C4 42.0 100 1 12/04/2023 18:38 WG2182350
tert-Amyl Methyl Ether U 0.195 1.00 1 12/04/2023 02:29 WG2182129
Ethyl tert-butyl ether U 0.101 1.00 1 12/04/2023 02:29 WG2182129
tert-Butyl alcohol U 4.06 5.00 1 12/04/2023 02:29 WG2182129
t-Amyl Alcohol U 4.90 50.0 1 12/04/2023 02:29 WG2182129
tert-Butyl formate U C4 4.51 20.0 1 12/04/2023 18:38 WG2182350
(S) Toluene-d8 103 80.0-120 12/04/2023 02:29 WG2182129
(S) Toluene-d8 115 80.0-120 12/04/2023 18:38 WG2182350
(S) 4-Bromofluorobenzene 93.8 77.0-126 12/04/2023 02:29 WG2182129
(S) 4-Bromofluorobenzene 85.7 77.0-126 12/04/2023 18:38 WG2182350
(S) 1,2-Dichloroethane-d4 99.7 70.0-130 12/04/2023 02:29 WG2182129
(S) 1,2-Dichloroethane-d4 98.9 70.0-130 12/04/2023 18:38 WG2182350
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 18 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 18 of 32
QUALITY CONTROL SUMMARYWG2182129
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1682629-01,02,03,04,05
Method Blank (MB)
(MB) R4007655-2 12/04/23 01:28
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Benzene U 0.0941 1.00
Bromobenzene U 0.118 1.00
Bromodichloromethane U 0.136 1.00
Bromochloromethane U 0.128 1.00
Bromoform U 0.129 1.00
Bromomethane U 0.605 5.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
cis-1,3-Dichloropropene U 0.111 1.00
trans-1,3-Dichloropropene U 0.118 1.00
2,2-Dichloropropane U 0.161 1.00
Di-isopropyl ether U 0.105 1.00
Ethylbenzene U 0.137 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
Isopropylbenzene U 0.105 1.00
Methylene Chloride U 0.430 5.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 19 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 19 of 32
QUALITY CONTROL SUMMARYWG2182129
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1682629-01,02,03,04,05
Method Blank (MB)
(MB) R4007655-2 12/04/23 01:28
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Methyl tert-butyl ether U 0.101 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.0993 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Trichlorofluoromethane U 0.160 5.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,4-Trimethylbenzene U 0.322 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
Vinyl chloride U 0.234 1.00
o-Xylene U 0.174 1.00
m&p-Xylenes U 0.430 2.00
tert-Amyl Methyl Ether U 0.195 1.00
Ethyl tert-butyl ether U 0.101 1.00
tert-Butyl alcohol U 4.06 5.00
t-Amyl Alcohol U 4.90 50.0
(S) Toluene-d8 106 80.0-120
(S) 4-Bromofluorobenzene 90.7 77.0-126
(S) 1,2-Dichloroethane-d4 101 70.0-130
Laboratory Control Sample (LCS)
(LCS) R4007655-1 12/04/23 00:29
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Benzene 5.00 4.94 98.8 70.0-123
Bromobenzene 5.00 5.48 110 73.0-121
Bromodichloromethane 5.00 4.94 98.8 75.0-120
Bromochloromethane 5.00 5.17 103 76.0-122
Bromoform 5.00 4.72 94.4 68.0-132
Bromomethane 5.00 4.83 96.6 10.0-160
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 20 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 20 of 32
QUALITY CONTROL SUMMARYWG2182129
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1682629-01,02,03,04,05
Laboratory Control Sample (LCS)
(LCS) R4007655-1 12/04/23 00:29
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
n-Butylbenzene 5.00 4.63 92.6 73.0-125
sec-Butylbenzene 5.00 5.66 113 75.0-125
tert-Butylbenzene 5.00 6.43 129 76.0-124 J4
Carbon tetrachloride 5.00 5.66 113 68.0-126
Chlorobenzene 5.00 5.02 100 80.0-121
Chlorodibromomethane 5.00 5.08 102 77.0-125
Chloroethane 5.00 5.20 104 47.0-150
Chloroform 5.00 5.11 102 73.0-120
Chloromethane 5.00 5.50 110 41.0-142
2-Chlorotoluene 5.00 5.86 117 76.0-123
4-Chlorotoluene 5.00 5.48 110 75.0-122
1,2-Dibromo-3-Chloropropane 5.00 4.75 95.0 58.0-134
1,2-Dibromoethane 5.00 5.08 102 80.0-122
Dibromomethane 5.00 4.63 92.6 80.0-120
1,2-Dichlorobenzene 5.00 5.03 101 79.0-121
1,3-Dichlorobenzene 5.00 5.36 107 79.0-120
1,4-Dichlorobenzene 5.00 5.47 109 79.0-120
Dichlorodifluoromethane 5.00 5.48 110 51.0-149
1,1-Dichloroethane 5.00 5.20 104 70.0-126
1,2-Dichloroethane 5.00 5.02 100 70.0-128
1,1-Dichloroethene 5.00 4.82 96.4 71.0-124
cis-1,2-Dichloroethene 5.00 5.03 101 73.0-120
trans-1,2-Dichloroethene 5.00 5.25 105 73.0-120
1,2-Dichloropropane 5.00 5.32 106 77.0-125
1,1-Dichloropropene 5.00 5.24 105 74.0-126
1,3-Dichloropropane 5.00 5.12 102 80.0-120
cis-1,3-Dichloropropene 5.00 5.25 105 80.0-123
trans-1,3-Dichloropropene 5.00 5.16 103 78.0-124
2,2-Dichloropropane 5.00 5.79 116 58.0-130
Di-isopropyl ether 5.00 5.09 102 58.0-138
Ethylbenzene 5.00 5.24 105 79.0-123
Hexachloro-1,3-butadiene 5.00 5.07 101 54.0-138
Isopropylbenzene 5.00 5.19 104 76.0-127
Methylene Chloride 5.00 4.66 93.2 67.0-120
Methyl tert-butyl ether 5.00 5.44 109 68.0-125
Naphthalene 5.00 4.26 85.2 54.0-135
n-Propylbenzene 5.00 5.46 109 77.0-124
Styrene 5.00 4.86 97.2 73.0-130
1,1,1,2-Tetrachloroethane 5.00 5.00 100 75.0-125
1,1,2,2-Tetrachloroethane 5.00 5.37 107 65.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 21 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 21 of 32
QUALITY CONTROL SUMMARYWG2182129
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1682629-01,02,03,04,05
Laboratory Control Sample (LCS)
(LCS) R4007655-1 12/04/23 00:29
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Tetrachloroethene 5.00 5.29 106 72.0-132
Toluene 5.00 5.54 111 79.0-120
1,2,3-Trichlorobenzene 5.00 5.36 107 50.0-138
1,2,4-Trichlorobenzene 5.00 4.91 98.2 57.0-137
1,1,1-Trichloroethane 5.00 5.56 111 73.0-124
1,1,2-Trichloroethane 5.00 5.23 105 80.0-120
Trichloroethene 5.00 5.58 112 78.0-124
Trichlorofluoromethane 5.00 4.69 93.8 59.0-147
1,2,3-Trichloropropane 5.00 5.54 111 73.0-130
1,2,4-Trimethylbenzene 5.00 5.68 114 76.0-121
1,3,5-Trimethylbenzene 5.00 5.53 111 76.0-122
Vinyl chloride 5.00 4.62 92.4 67.0-131
o-Xylene 5.00 4.97 99.4 80.0-122
m&p-Xylenes 10.0 10.5 105 80.0-122
tert-Amyl Methyl Ether 5.00 4.84 96.8 66.0-125
Ethyl tert-butyl ether 5.00 5.07 101 63.0-138
tert-Butyl alcohol 25.0 25.0 100 27.0-160
(S) Toluene-d8 103 80.0-120
(S) 4-Bromofluorobenzene 93.8 77.0-126
(S) 1,2-Dichloroethane-d4 99.7 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 22 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 22 of 32
QUALITY CONTROL SUMMARYWG2182350
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1682629-01,02,03,04,05
Method Blank (MB)
(MB) R4008191-4 12/04/23 17:57
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
ethanol U 42.0 100
tert-Butyl formate U 4.51 20.0
(S) Toluene-d8 113 80.0-120
(S) 4-Bromofluorobenzene 90.0 77.0-126
(S) 1,2-Dichloroethane-d4 99.2 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R4008191-1 12/04/23 16:35 • (LCSD) R4008191-2 12/04/23 16:55
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
ethanol 250 156 172 62.4 68.8 10.0-160 9.76 30
(S) Toluene-d8 114 109 80.0-120
(S) 4-Bromofluorobenzene 93.3 93.3 77.0-126
(S) 1,2-Dichloroethane-d4 92.8 97.9 70.0-130
Laboratory Control Sample (LCS)
(LCS) R4008191-3 12/04/23 17:16
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
tert-Butyl formate 100 60.3 60.3 10.0-160
(S) Toluene-d8 114 80.0-120
(S) 4-Bromofluorobenzene 88.6 77.0-126
(S) 1,2-Dichloroethane-d4 98.3 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 23 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 23 of 32
QUALITY CONTROL SUMMARYWG2182322
TPH by Method MADEPE L1682629-01,02,03,04
Method Blank (MB)
(MB) R4008171-1 12/05/23 07:34
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics 40.8 J 33.3 100
Unadjusted C19-C36 Aliphatics 52.8 J 33.3 100
(S) 1-Chloro-octadecane 63.0 40.0-140
Method Blank (MB)
(MB) R4008175-3 12/05/23 08:37
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics 75.3 J 33.3 100
(S) o-Terphenyl 81.5 40.0-140
(S) 2-Fluorobiphenyl 90.8 40.0-140
(S) 2-Bromonaphthalene 96.7 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R4008171-2 12/05/23 07:58 • (LCSD) R4008171-3 12/05/23 08:28
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 410 350 68.3 58.3 40.0-140 15.8 25
Unadjusted C19-C36 Aliphatics 800 668 626 83.5 78.3 40.0-140 6.49 25
(S) 1-Chloro-octadecane 58.5 55.0 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R4008175-1 12/05/23 07:53 • (LCSD) R4008175-2 12/05/23 08:15
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1400 1300 82.4 76.5 40.0-140 7.41 25
(S) o-Terphenyl 78.0 73.5 40.0-140
(S) 2-Fluorobiphenyl 90.8 92.5 40.0-140
(S) 2-Bromonaphthalene 95.5 97.5 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 24 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 24 of 32
QUALITY CONTROL SUMMARYWG2180281
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1682629-01,02,03,04
Method Blank (MB)
(MB) R4008287-2 12/01/23 14:34
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.0886 1.00
Acenaphthylene U 0.0921 1.00
Anthracene U 0.0804 1.00
Benzo(a)anthracene U 0.199 1.00
Benzo(b)fluoranthene U 0.130 1.00
Benzo(k)fluoranthene U 0.120 1.00
Benzo(g,h,i)perylene U 0.121 1.00
Benzo(a)pyrene U 0.0381 1.00
Bis(2-chlorethoxy)methane U 0.116 10.0
Bis(2-chloroethyl)ether U 0.137 10.0
2,2-Oxybis(1-Chloropropane)U 0.210 10.0
4-Bromophenyl-phenylether U 0.0877 10.0
2-Chloronaphthalene U 0.0648 1.00
4-Chlorophenyl-phenylether U 0.0926 10.0
Chrysene U 0.130 1.00
Dibenz(a,h)anthracene U 0.0644 1.00
3,3-Dichlorobenzidine U 0.212 10.0
2,4-Dinitrotoluene U 0.0983 10.0
2,6-Dinitrotoluene U 0.250 10.0
Fluoranthene U 0.102 1.00
Fluorene U 0.0844 1.00
Hexachlorobenzene U 0.0755 1.00
Hexachloro-1,3-butadiene U 0.0968 10.0
Hexachlorocyclopentadiene U 0.0598 10.0
Hexachloroethane U 0.127 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.143 10.0
Naphthalene U 0.159 1.00
Nitrobenzene U 0.297 10.0
n-Nitrosodimethylamine U 0.998 10.0
n-Nitrosodiphenylamine U 2.37 10.0
n-Nitrosodi-n-propylamine U 0.261 10.0
Phenanthrene U 0.112 1.00
Benzylbutyl phthalate U 0.765 3.00
Bis(2-ethylhexyl)phthalate U 0.895 3.00
Di-n-butyl phthalate U 0.453 3.00
Diethyl phthalate U 0.287 3.00
Dimethyl phthalate U 0.260 3.00
Di-n-octyl phthalate U 0.932 3.00
Pyrene U 0.107 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 25 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 25 of 32
QUALITY CONTROL SUMMARYWG2180281
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1682629-01,02,03,04
Method Blank (MB)
(MB) R4008287-2 12/01/23 14:34
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
1,2,4-Trichlorobenzene U 0.0698 10.0
4-Chloro-3-methylphenol U 0.131 10.0
2-Chlorophenol U 0.133 10.0
2,4-Dichlorophenol U 0.102 10.0
2,4-Dimethylphenol U 0.0636 10.0
4,6-Dinitro-2-methylphenol U 1.12 10.0
2,4-Dinitrophenol U 5.93 10.0
2-Nitrophenol U 0.117 10.0
4-Nitrophenol U 0.143 10.0
Pentachlorophenol U 0.313 10.0
Phenol U 4.33 10.0
2,4,6-Trichlorophenol U 0.100 10.0
(S) Nitrobenzene-d5 77.1 15.0-314
(S) 2-Fluorobiphenyl 59.0 22.0-127
(S) p-Terphenyl-d14 84.1 29.0-141
(S) Phenol-d5 25.6 8.00-424
(S) 2-Fluorophenol 38.5 10.0-120
(S) 2,4,6-Tribromophenol 71.0 10.0-153
Laboratory Control Sample (LCS)
(LCS) R4008287-1 12/01/23 14:13
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acenaphthene 50.0 36.6 73.2 47.0-145
Acenaphthylene 50.0 37.5 75.0 33.0-145
Anthracene 50.0 38.3 76.6 27.0-133
Benzo(a)anthracene 50.0 44.7 89.4 33.0-143
Benzo(b)fluoranthene 50.0 39.6 79.2 24.0-159
Benzo(k)fluoranthene 50.0 38.1 76.2 11.0-162
Benzo(g,h,i)perylene 50.0 34.3 68.6 1.00-219
Benzo(a)pyrene 50.0 38.3 76.6 17.0-163
Bis(2-chlorethoxy)methane 50.0 33.0 66.0 1.00-219
Bis(2-chloroethyl)ether 50.0 39.3 78.6 33.0-185
2,2-Oxybis(1-Chloropropane)50.0 33.6 67.2 36.0-166
4-Bromophenyl-phenylether 50.0 39.5 79.0 53.0-127
2-Chloronaphthalene 50.0 36.8 73.6 60.0-120
4-Chlorophenyl-phenylether 50.0 35.0 70.0 25.0-158
Chrysene 50.0 40.5 81.0 17.0-168
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 26 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 26 of 32
QUALITY CONTROL SUMMARYWG2180281
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1682629-01,02,03,04
Laboratory Control Sample (LCS)
(LCS) R4008287-1 12/01/23 14:13
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Dibenz(a,h)anthracene 50.0 39.2 78.4 1.00-227
3,3-Dichlorobenzidine 100 84.8 84.8 1.00-262
2,4-Dinitrotoluene 50.0 40.0 80.0 39.0-139
2,6-Dinitrotoluene 50.0 39.1 78.2 50.0-158
Fluoranthene 50.0 36.6 73.2 26.0-137
Fluorene 50.0 35.5 71.0 59.0-121
Hexachlorobenzene 50.0 40.1 80.2 1.00-152
Hexachloro-1,3-butadiene 50.0 26.3 52.6 24.0-120
Hexachlorocyclopentadiene 50.0 11.2 22.4 10.0-120
Hexachloroethane 50.0 26.7 53.4 40.0-120
Indeno(1,2,3-cd)pyrene 50.0 35.3 70.6 1.00-171
Isophorone 50.0 31.3 62.6 21.0-196
Naphthalene 50.0 30.0 60.0 21.0-133
Nitrobenzene 50.0 32.8 65.6 35.0-180
n-Nitrosodimethylamine 50.0 22.3 44.6 10.0-120
n-Nitrosodiphenylamine 50.0 41.2 82.4 44.0-120
n-Nitrosodi-n-propylamine 50.0 35.6 71.2 1.00-230
Phenanthrene 50.0 38.3 76.6 54.0-120
Benzylbutyl phthalate 50.0 51.6 103 1.00-152
Bis(2-ethylhexyl)phthalate 50.0 45.1 90.2 8.00-158
Di-n-butyl phthalate 50.0 44.7 89.4 1.00-120
Diethyl phthalate 50.0 37.3 74.6 1.00-120
Dimethyl phthalate 50.0 37.9 75.8 1.00-120
Di-n-octyl phthalate 50.0 47.3 94.6 4.00-146
Pyrene 50.0 45.9 91.8 52.0-120
1,2,4-Trichlorobenzene 50.0 27.0 54.0 44.0-142
4-Chloro-3-methylphenol 50.0 25.4 50.8 22.0-147
2-Chlorophenol 50.0 26.0 52.0 23.0-134
2,4-Dichlorophenol 50.0 27.5 55.0 39.0-135
2,4-Dimethylphenol 50.0 30.2 60.4 32.0-120
4,6-Dinitro-2-methylphenol 50.0 40.8 81.6 1.00-181
2,4-Dinitrophenol 50.0 31.7 63.4 1.00-191
2-Nitrophenol 50.0 37.4 74.8 29.0-182
4-Nitrophenol 50.0 10.8 21.6 1.00-132
Pentachlorophenol 50.0 21.0 42.0 14.0-176
Phenol 50.0 15.2 30.4 5.00-120
2,4,6-Trichlorophenol 50.0 34.9 69.8 37.0-144
(S) Nitrobenzene-d5 70.4 15.0-314
(S) 2-Fluorobiphenyl 70.5 22.0-127
(S) p-Terphenyl-d14 83.8 29.0-141
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 27 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 27 of 32
QUALITY CONTROL SUMMARYWG2180281
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1682629-01,02,03,04
Laboratory Control Sample (LCS)
(LCS) R4008287-1 12/01/23 14:13
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
(S) Phenol-d5 24.6 8.00-424
(S) 2-Fluorophenol 35.8 10.0-120
(S) 2,4,6-Tribromophenol 78.5 10.0-153
L1681910-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1681910-01 12/01/23 14:55 • (MS) R4008287-3 12/01/23 15:16 • (MSD) R4008287-4 12/01/23 15:37
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Acenaphthene 50.0 U 34.9 33.3 69.8 66.6 1 47.0-145 4.69 48
Acenaphthylene 50.0 U 35.7 33.8 71.4 67.6 1 33.0-145 5.47 74
Anthracene 50.0 U 33.8 31.5 67.6 63.0 1 27.0-133 7.04 66
Benzo(a)anthracene 50.0 U 35.0 33.2 70.0 66.4 1 33.0-143 5.28 53
Benzo(b)fluoranthene 50.0 U 35.7 33.9 71.4 67.8 1 24.0-159 5.17 71
Benzo(k)fluoranthene 50.0 U 35.3 31.8 70.6 63.6 1 11.0-162 10.4 63
Benzo(g,h,i)perylene 50.0 U 33.8 29.3 67.6 58.6 1 1.00-219 14.3 97
Benzo(a)pyrene 50.0 U 33.5 31.2 67.0 62.4 1 17.0-163 7.11 72
Bis(2-chlorethoxy)methane 50.0 U 32.1 31.2 64.2 62.4 1 33.0-184 2.84 54
Bis(2-chloroethyl)ether 50.0 U 37.0 35.7 74.0 71.4 1 12.0-158 3.58 108
2,2-Oxybis(1-Chloropropane)50.0 U 31.2 30.5 62.4 61.0 1 36.0-166 2.27 76
4-Bromophenyl-phenylether 50.0 U 38.5 34.9 77.0 69.8 1 53.0-127 9.81 43
2-Chloronaphthalene 50.0 U 35.3 33.1 70.6 66.2 1 60.0-120 6.43 24
4-Chlorophenyl-phenylether 50.0 U 33.3 31.5 66.6 63.0 1 25.0-158 5.56 61
Chrysene 50.0 U 33.0 29.2 66.0 58.4 1 17.0-168 12.2 87
Dibenz(a,h)anthracene 50.0 U 36.6 32.3 73.2 64.6 1 1.00-227 12.5 126
3,3-Dichlorobenzidine 100 U 8.45 9.30 8.45 9.30 1 1.00-262 9.58 108
2,4-Dinitrotoluene 50.0 U 38.0 37.9 76.0 75.8 1 39.0-139 0.263 42
2,6-Dinitrotoluene 50.0 U 37.9 36.6 75.8 73.2 1 50.0-158 3.49 48
Fluoranthene 50.0 U 34.1 33.5 68.2 67.0 1 26.0-137 1.78 66
Fluorene 50.0 U 33.7 32.5 67.4 65.0 1 59.0-121 3.63 38
Hexachlorobenzene 50.0 U 36.1 33.2 72.2 66.4 1 1.00-152 8.37 55
Hexachloro-1,3-butadiene 50.0 U 24.0 22.6 48.0 45.2 1 24.0-120 6.01 62
Hexachlorocyclopentadiene 50.0 U 10.5 12.5 21.0 25.0 1 10.0-146 17.4 34
Hexachloroethane 50.0 U 28.9 26.4 57.8 52.8 1 40.0-120 9.04 52
Indeno(1,2,3-cd)pyrene 50.0 U 31.9 29.5 63.8 59.0 1 1.00-171 7.82 99
Isophorone 50.0 U 31.4 31.8 62.8 63.6 1 21.0-196 1.27 93
Naphthalene 50.0 U 28.7 28.3 57.4 56.6 1 21.0-133 1.40 65
Nitrobenzene 50.0 U 35.6 35.4 71.2 70.8 1 35.0-180 0.563 62
n-Nitrosodimethylamine 50.0 U 24.0 22.4 48.0 44.8 1 10.0-120 6.90 40
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 28 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 28 of 32
QUALITY CONTROL SUMMARYWG2180281
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1682629-01,02,03,04
L1681910-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1681910-01 12/01/23 14:55 • (MS) R4008287-3 12/01/23 15:16 • (MSD) R4008287-4 12/01/23 15:37
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
n-Nitrosodiphenylamine 50.0 U 38.5 36.2 77.0 72.4 1 16.0-160 6.16 28
n-Nitrosodi-n-propylamine 50.0 U 32.5 32.7 65.0 65.4 1 1.00-230 0.613 87
Phenanthrene 50.0 U 36.3 34.1 72.6 68.2 1 54.0-120 6.25 39
Benzylbutyl phthalate 50.0 U 44.2 40.7 88.4 81.4 1 1.00-152 8.24 60
Bis(2-ethylhexyl)phthalate 50.0 U 37.5 35.3 75.0 70.6 1 8.00-158 6.04 82
Di-n-butyl phthalate 50.0 U 41.0 40.3 82.0 80.6 1 1.00-120 1.72 47
Diethyl phthalate 50.0 U 36.4 35.6 72.8 71.2 1 1.00-120 2.22 100
Dimethyl phthalate 50.0 U 36.4 34.7 72.8 69.4 1 1.00-120 4.78 183
Di-n-octyl phthalate 50.0 U 39.6 37.8 79.2 75.6 1 4.00-146 4.65 69
Pyrene 50.0 U 38.9 35.8 77.8 71.6 1 52.0-120 8.30 49
1,2,4-Trichlorobenzene 50.0 U 26.3 25.3 52.6 50.6 1 44.0-142 3.88 50
4-Chloro-3-methylphenol 50.0 U 22.6 21.1 45.2 42.2 1 22.0-147 6.86 73
2-Chlorophenol 50.0 U 23.9 21.7 47.8 43.4 1 23.0-134 9.65 61
2,4-Dichlorophenol 50.0 U 23.7 21.6 47.4 43.2 1 39.0-135 9.27 50
2,4-Dimethylphenol 50.0 U 26.5 25.8 53.0 51.6 1 32.0-120 2.68 58
4,6-Dinitro-2-methylphenol 50.0 U 33.5 31.5 67.0 63.0 1 1.00-181 6.15 203
2,4-Dinitrophenol 50.0 U 25.0 25.5 50.0 51.0 1 1.00-191 1.98 132
2-Nitrophenol 50.0 U 32.3 30.8 64.6 61.6 1 29.0-182 4.75 55
4-Nitrophenol 50.0 U 12.1 12.2 24.2 24.4 1 1.00-132 0.823 131
Pentachlorophenol 50.0 U 14.9 15.6 29.8 31.2 1 14.0-176 4.59 86
Phenol 50.0 U 14.9 14.3 29.8 28.6 1 5.00-120 4.11 64
2,4,6-Trichlorophenol 50.0 U 30.3 26.0 60.6 52.0 1 37.0-144 15.3 58
(S) Nitrobenzene-d5 66.4 65.2 15.0-314
(S) 2-Fluorobiphenyl 67.5 63.8 22.0-127
(S) p-Terphenyl-d14 72.2 63.6 29.0-141
(S) Phenol-d5 25.4 23.3 8.00-424
(S) 2-Fluorophenol 33.8 32.3 10.0-120
(S) 2,4,6-Tribromophenol 64.5 57.0 10.0-153
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 29 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 29 of 32
GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
C4 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low.
Data is likely to show a low bias concerning the result.
J The identification of the analyte is acceptable; the reported value is an estimate.
J4 The associated batch QC was outside the established quality control range for accuracy.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 30 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 30 of 32

Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/05/23 18:13 31 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Colonial Pipeline- S&ME Raleigh 210818 L1682629 12/06/23 08:19 31 of 32