FA-30296_49321_CA_UST-61_20231215

UST-61 24-Hour Release and UST Leak Reporting Form.
For Releases This form should be completed and submitted to the UST Section's regional office following a known or suspected release from
in NC an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or suspected release
(DWM USE ONLY) Suspected Contamination? (Y/N) Facility ID Number Incident# Risk (H,l,L,U) Confirmed GW Contamination? (Y/N) ___ Date Leak Discovered Received On Received By Confirmed Soil Contamination ?(Y/N) ___ Comm/Non-Commercial? Reported by (circle one): Phone, Fax or Report Samples Taken?(Y/N) __ Reg/Non-regulated? Region Free Product? (Y/N) __ If Yes, State Greatest Thickness
INCIDENT DESCRIPTION Incident Name:
Address: I County:
City/Town: Zip Code: I Regional Office (circle one): Asheville, Mooresville, Fayetteville, Raleigh, Washington, Wilmington, Winston-Salem
Latitude (decimal degrees): Longitude (decimal degrees) : Obtained by: Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount OGPS of release, amount of free oroduct oresent and recoverv efforts, initial resoonses conducted, imoacts to receotors)□Topographic map
OGls Address matching
O0ther □unknown
Describe location:
HOW RELEASE WAS DISCOVERED (Release Code)
(Check one) □Release Detection Equipment or Methods Dvisual/Odor □Groundwater Contamination
ODuring UST Closure/Removal Dwater in Tank Dsurtace Water Contamination □Property Transfer Dwater Supply Well Contamination O0ther (specify)
SOURCE OF CONTAMINATION
Source of Release Cause of Release T�ee of Release Product T�ee Released
(Check primary source) (Check primary cause) (Check one) (Check primary product type released)
OTank □spill D Petroleum D Gasoline/ Diesel/ 0 DieselNeg. Oil □Piping □overfill D Non-Petroleum Kerosene Blend
D Dispenser D Corrosion OBoth D Heating Oil 0 Vegetable Oil 100%
D Submersible Turbine Pump D Physical/Mechanical D Other Petroleum OE10-E20
Location Products OE21-E84 D Delivery Problem Damage (Check one) D Metals D Install Problem OE85-E99 □spill Bucket D Other □Facility D Other lnorganics D Ethanol 100% Oother D Unknown □Residence D Other Organics OE01-E09 D Unknown O0ther
Definitions presented on reverse Definitions presented on reverse
Ownershie 1.Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State
Oeeration Tl£ee 1.Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining
UST Form 61 (02/19) Page 1 of 2
35.058179 78.877470
KEC12/13/23
L
FAY Phone
N/A49321FA-30296
IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1. Yes 2. No 3. Unknown
Number of Water Supply Wells Affected
Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary)
1.
2. 3.
UST SYSTEM OWNER
UST Owner/Company
Address
City I State Zip Code I Telephone Number
UST SYSTEM OPERATOR UST Operator/Company
Address
City I State Zip Code I Telephone Number
LANDOWNER AT LOCATION OF UST INCIDENT Landowner
Address
City I State Zip Code I Telephone Number
Draw Sketch of Area (showing two major road intersections) or Attach Map
Person Reporting Incident Company Telephone Number
Title Address Date
UST Form 61 (02/19) Page2 of2
Definitions of Sources Tank: means the tank that stores the product and is part of the underground storage tank system Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end-use equipment (Vent, vapor recovery, or fill lines are excluded.) Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above the shear valve) Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that connects the submersible turbine pump to the tank Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.) Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories ( e.g., for releases from vent lines, vapor recovery lines, and fill lines) Unknown: identifies releases for which the source has not been determined Definitions of Causes Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser) Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser) Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion ( e.g., puncture of tank or piping, loose fittings, broken components, and components that have changed dimension) Corrosion: use when a metal tank, piping, or other component has a release due to corrosion ( e.g., for steel, corrosion takes the form of rust) Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells) Unknown: use when the cause has not been determined Point of Contact
Email
Email
Email
REVISION NO. 0
JOB NO. CCR-010
DATE: 11-1-23
FIGURE NO. 2
RETAIL PROPERTY
108 ROWAN STREET$1'5$06(<675((7
FAYETTEVILLE, NORTH CAROLINA
SITE MAP
LEGEND
SITE PROPERTY BOUNDARY
PARCEL LINE
POLE-MOUNTED TRANSFORMER
STORM WATER DRAIN
NOTES:
AERIAL IMAGERY OBTAINED FROM GOOGLE IMAGE
SERVICES.
BASE DATA OBTAINED FROM CUMBERLAND COUNTY GIS,
2023.
UST = UNDERGROUND STORAGE TANK
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
ST. JAMES LIBERTY
GAS STATION
(120 ROWAN STREET)
ROW
A
N

S
T
R
E
E
T RAMSEY STREETINSURANCE OF THE CAROLINAS
(439 RAMSEY STREET)
PARIS & POTTER MANAGEMENT CORP.
KFC FRANCHISING OFFICE
(430 RAMSEY STREET)
RIMTYME CUSTOM WHEELS AND TIRES
(416 RAMSEY STREET)
CVS
(404 RAMSEY STREET)
USPS
(107-115 ROWAN STREET)
VACANT BANK BUILDING
(123 ROWAN STREET)
%2-$1*/(6
CONSTRUCTIONAREA
)250(53+$50$&<
%8,/',1*
APPROXIMATE LOCATION OF
FORMER HEATING OIL UST
APPROXIMATE LOCATION OF
FORMER GASOLINE USTs
APPROXIMATE LOCATION
OF FORMER WASTE OIL UST
UST BASIN
S:\AAA-Master Projects\Carolina Capital Real Estate Partners (CCR)\CCR-010 108 Rowan Street, Fayetteville\Phase I Update_202310\Figures\CCR.010_20231101.dwg, FIG 2, 11/1/2023 8:41:15 AM, shaynes*5$9(/3$5.,1*$5($'5,9(:$<
GENERAL AREA OF SOIL
CONTAMINATION NEAR
FORMER RESIDENCE/
RESTAURANT
#=CL#
December 12, 2023
LIMS USE: FR - RON NAVARRO
LIMS OBJECT ID: 92700661
92700661
Project:
Pace Project No.:
RE:
Ron Navarro
ECS Raleigh
5260 Greens Dairy Road
Raleigh, NC 27616
Rowan Street Site
Dear Ron Navarro:
Enclosed are the analytical results for sample(s) received by the laboratory on November 28, 2023. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni for
[e-mail]
Project Manager
Adam Phillips
919-701-8757
Enclosures
cc:ECS Southeast Reporting, ECS Southeast
Sarah Ward
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 44
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92700661
Rowan Street Site
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 44
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92700661
Rowan Street Site
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92700661001 SS-1 Comp MADEP EPH 8 PANDMG
EPA 8081B 9 PANMFM
EPA 8151A 3 PANNWH
EPA 8015C 2 PASI-CHH
MADEP VPH 6 PANACG
EPA 6010D 7 PANDJS
EPA 7470A 1 PANNDL
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
1010B/ASTM D8175-18 1 PANWOS
SM 2540G 1 PANKDW
EPA 9012B 1 PANLDT
EPA 9030B 1 PANRTW
EPA 9045D 1 PANNTG
92700661002 SS-1 Grab MADEP VPH 6 PANACG
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92700661
Rowan Street Site
Sample:SS-1 Comp Lab ID:92700661001 Collected:11/28/23 14:15 Received:11/28/23 16:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MA DEP/NJ DEP
Pace National - Mt. Juliet
TPH by Method MADEPE
Aliphatic (C09-C18),Unadjusted 210 mg/kg 12/07/23 10:2012/05/23 09:307.71 1
Aliphatic (C19-C36),Unadjusted 37.4 mg/kg 12/07/23 10:2012/05/23 09:307.71 1
Aromatic (C11-C22), Unadjusted 66.5 mg/kg 12/07/23 13:07 TPHC11C2212/05/23 09:307.71 1
TEH, Unadjusted 314 mg/kg 12/07/23 13:0712/05/23 09:307.71 1
Surrogates
o-Terphenyl (S)61.4 %12/07/23 13:07 84-15-112/05/23 09:3040.0-140 1
1-Chloro-octadecane (S)56.8 %12/07/23 10:20 3386-33-212/05/23 09:3040.0-140 1
2-Fluorobiphenyl (S)76.5 %12/07/23 13:07 321-60-812/05/23 09:3040.0-140 1
2-Bromonaphthalene (S)76.1 %12/07/23 13:07 580-13-212/05/23 09:3040.0-140 1
Analytical Method: EPA 8081B Preparation Method: 3510C
Leachate Method/Date: 1311; 12/01/23 10:03 Initial pH: 6.57; Final pH: 4.98
Pace National - Mt. Juliet
Pesticides (GC) 8081B TCLP
Chlordane (Technical)ND mg/L 12/06/23 13:52 57-74-912/06/23 06:190.00500 1
Endrin ND mg/L 12/06/23 13:52 72-20-812/06/23 06:190.00500 1
Heptachlor ND mg/L 12/06/23 13:52 76-44-812/06/23 06:190.00500 1
Heptachlor epoxide ND mg/L 12/06/23 13:52 1024-57-312/06/23 06:190.00500 1
gamma-BHC (Lindane)ND mg/L 12/06/23 13:52 58-89-912/06/23 06:190.00500 1
Methoxychlor ND mg/L 12/06/23 13:52 72-43-512/06/23 06:190.00500 1
Toxaphene ND mg/L 12/06/23 13:52 8001-35-212/06/23 06:190.0100 1
Surrogates
Decachlorobiphenyl (S)67.5 %12/06/23 13:52 2051-24-312/06/23 06:1910.0-128 1
Tetrachloro-m-xylene (S)68.3 %12/06/23 13:52 877-09-812/06/23 06:1910.0-127 1
Analytical Method: EPA 8151A Preparation Method: 8151A
Leachate Method/Date: 1311; 12/01/23 10:03 Initial pH: 6.57; Final pH: 4.98
Pace National - Mt. Juliet
Chlorinated Herb. (GC) 8151A
2,4,5-TP (Silvex)ND mg/L 12/09/23 04:31 93-72-112/04/23 14:280.00200 1
2,4-D ND mg/L 12/09/23 04:31 94-75-712/04/23 14:280.00200 1
Surrogates
2,4-DCAA (S)104 %12/09/23 04:31 19719-28-912/04/23 14:2814.0-158 1
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)436 mg/kg 12/01/23 14:4511/30/23 19:1511.4 2
Surrogates
n-Pentacosane (S)57 %12/01/23 14:45 629-99-211/30/23 19:1510-133 2
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08),Unadjusted ND mg/kg 12/10/23 14:33 C412/10/23 14:336.87 1
Aliphatic (C09-C12),Unadjusted 53.3 mg/kg 12/10/23 14:3312/10/23 14:336.87 1
Aromatic (C09-C10),Unadjusted 18.7 mg/kg 12/10/23 14:33 TPHC9C10A12/10/23 14:336.87 1
Total VPH 72.0 mg/kg 12/10/23 14:33 VPH12/10/23 14:336.87 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92700661
Rowan Street Site
Sample:SS-1 Comp Lab ID:92700661001 Collected:11/28/23 14:15 Received:11/28/23 16:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Surrogates
2,5-Dibromotoluene (FID)120 %12/10/23 14:33 615-59-8FID12/10/23 14:3370.0-130 1
2,5-Dibromotoluene (PID)90.9 %12/10/23 14:33 615-59-8PID12/10/23 14:3370.0-130 1
Analytical Method: EPA 6010D Preparation Method: 3015
Leachate Method/Date: 1311; 12/01/23 10:03 Initial pH: 6.57; Final pH: 4.98
Pace National - Mt. Juliet
Metals (ICP) 6010D TCLP
Arsenic ND mg/L 12/03/23 18:30 7440-38-212/03/23 07:150.100 1
Barium 0.212 mg/L 12/03/23 18:30 7440-39-312/03/23 07:150.100 1
Cadmium ND mg/L 12/03/23 18:30 7440-43-912/03/23 07:150.100 1
Chromium ND mg/L 12/03/23 18:30 7440-47-312/03/23 07:150.100 1
Lead 0.166 mg/L 12/03/23 18:30 7439-92-112/03/23 07:150.100 1
Selenium ND mg/L 12/03/23 18:30 7782-49-212/03/23 07:150.100 1
Silver ND mg/L 12/03/23 18:30 7440-22-412/03/23 07:150.100 1
Analytical Method: EPA 7470A Preparation Method: 7470A
Leachate Method/Date: 1311; 12/01/23 10:03 Initial pH: 6.57; Final pH: 4.98
Pace National - Mt. Juliet
Mercury 7470A TCLP
Mercury ND mg/L 12/03/23 12:06 7439-97-612/02/23 12:260.0100 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 12/05/23 11:28 83-32-912/01/23 13:003831
Acenaphthylene ND ug/kg 12/05/23 11:28 208-96-812/01/23 13:003831
Aniline ND ug/kg 12/05/23 11:28 62-53-312/01/23 13:003831
Anthracene ND ug/kg 12/05/23 11:28 120-12-712/01/23 13:003831
Benzo(a)anthracene ND ug/kg 12/05/23 11:28 56-55-312/01/23 13:003831
Benzo(a)pyrene ND ug/kg 12/05/23 11:28 50-32-812/01/23 13:003831
Benzo(b)fluoranthene ND ug/kg 12/05/23 11:28 205-99-212/01/23 13:003831
Benzo(g,h,i)perylene ND ug/kg 12/05/23 11:28 191-24-212/01/23 13:003831
Benzo(k)fluoranthene ND ug/kg 12/05/23 11:28 207-08-912/01/23 13:003831
Benzoic Acid ND ug/kg 12/05/23 11:28 65-85-012/01/23 13:0019201
Benzyl alcohol ND ug/kg 12/05/23 11:28 100-51-612/01/23 13:007671
4-Bromophenylphenyl ether ND ug/kg 12/05/23 11:28 101-55-312/01/23 13:003831
Butylbenzylphthalate ND ug/kg 12/05/23 11:28 85-68-712/01/23 13:003831
4-Chloro-3-methylphenol ND ug/kg 12/05/23 11:28 59-50-712/01/23 13:007671
4-Chloroaniline ND ug/kg 12/05/23 11:28 106-47-812/01/23 13:007671
bis(2-Chloroethoxy)methane ND ug/kg 12/05/23 11:28 111-91-112/01/23 13:003831
bis(2-Chloroethyl) ether ND ug/kg 12/05/23 11:28 111-44-412/01/23 13:003831
2-Chloronaphthalene ND ug/kg 12/05/23 11:28 91-58-712/01/23 13:003831
2-Chlorophenol ND ug/kg 12/05/23 11:28 95-57-812/01/23 13:003831
4-Chlorophenylphenyl ether ND ug/kg 12/05/23 11:28 7005-72-312/01/23 13:003831
Chrysene ND ug/kg 12/05/23 11:28 218-01-912/01/23 13:003831
Dibenz(a,h)anthracene ND ug/kg 12/05/23 11:28 53-70-312/01/23 13:003831
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92700661
Rowan Street Site
Sample:SS-1 Comp Lab ID:92700661001 Collected:11/28/23 14:15 Received:11/28/23 16:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dibenzofuran ND ug/kg 12/05/23 11:28 132-64-912/01/23 13:003831
1,2-Dichlorobenzene ND ug/kg 12/05/23 11:28 95-50-112/01/23 13:003831
1,3-Dichlorobenzene ND ug/kg 12/05/23 11:28 541-73-112/01/23 13:003831
1,4-Dichlorobenzene ND ug/kg 12/05/23 11:28 106-46-712/01/23 13:003831
3,3'-Dichlorobenzidine ND ug/kg 12/05/23 11:28 91-94-112/01/23 13:007671
2,4-Dichlorophenol ND ug/kg 12/05/23 11:28 120-83-212/01/23 13:003831
Diethylphthalate ND ug/kg 12/05/23 11:28 84-66-212/01/23 13:003831
2,4-Dimethylphenol ND ug/kg 12/05/23 11:28 105-67-912/01/23 13:003831
Dimethylphthalate ND ug/kg 12/05/23 11:28 131-11-312/01/23 13:003831
Di-n-butylphthalate ND ug/kg 12/05/23 11:28 84-74-212/01/23 13:003831
4,6-Dinitro-2-methylphenol ND ug/kg 12/05/23 11:28 534-52-112/01/23 13:007671
2,4-Dinitrophenol ND ug/kg 12/05/23 11:28 51-28-512/01/23 13:0019201
2,4-Dinitrotoluene ND ug/kg 12/05/23 11:28 121-14-212/01/23 13:003831
2,6-Dinitrotoluene ND ug/kg 12/05/23 11:28 606-20-212/01/23 13:003831
Di-n-octylphthalate ND ug/kg 12/05/23 11:28 117-84-012/01/23 13:003831
bis(2-Ethylhexyl)phthalate ND ug/kg 12/05/23 11:28 117-81-712/01/23 13:003831
Fluoranthene ND ug/kg 12/05/23 11:28 206-44-012/01/23 13:003831
Fluorene 401 ug/kg 12/05/23 11:28 86-73-712/01/23 13:003831
Hexachloro-1,3-butadiene ND ug/kg 12/05/23 11:28 87-68-312/01/23 13:003831
Hexachlorobenzene ND ug/kg 12/05/23 11:28 118-74-112/01/23 13:003831
Hexachlorocyclopentadiene ND ug/kg 12/05/23 11:28 77-47-412/01/23 13:003831
Hexachloroethane ND ug/kg 12/05/23 11:28 67-72-112/01/23 13:003831
Indeno(1,2,3-cd)pyrene ND ug/kg 12/05/23 11:28 193-39-512/01/23 13:003831
Isophorone ND ug/kg 12/05/23 11:28 78-59-112/01/23 13:003831
1-Methylnaphthalene 6140 ug/kg 12/05/23 12:23 90-12-012/01/23 13:0019205
2-Methylnaphthalene 8320 ug/kg 12/05/23 12:23 91-57-612/01/23 13:0019205
2-Methylphenol(o-Cresol)ND ug/kg 12/05/23 11:28 95-48-712/01/23 13:003831
3&4-Methylphenol(m&p Cresol)ND ug/kg 12/05/23 11:28 15831-10-412/01/23 13:003831
Naphthalene 2570 ug/kg 12/05/23 11:28 91-20-312/01/23 13:003831
2-Nitroaniline ND ug/kg 12/05/23 11:28 88-74-412/01/23 13:0019201
3-Nitroaniline ND ug/kg 12/05/23 11:28 99-09-212/01/23 13:0019201
4-Nitroaniline ND ug/kg 12/05/23 11:28 100-01-612/01/23 13:007671
Nitrobenzene ND ug/kg 12/05/23 11:28 98-95-312/01/23 13:003831
2-Nitrophenol ND ug/kg 12/05/23 11:28 88-75-512/01/23 13:003831
4-Nitrophenol ND ug/kg 12/05/23 11:28 100-02-712/01/23 13:0019201
N-Nitrosodimethylamine ND ug/kg 12/05/23 11:28 62-75-912/01/23 13:003831
N-Nitroso-di-n-propylamine ND ug/kg 12/05/23 11:28 621-64-712/01/23 13:003831
N-Nitrosodiphenylamine ND ug/kg 12/05/23 11:28 86-30-612/01/23 13:003831
2,2'-Oxybis(1-chloropropane)ND ug/kg 12/05/23 11:28 108-60-112/01/23 13:003831
Pentachlorophenol ND ug/kg 12/05/23 11:28 87-86-512/01/23 13:007671
Phenanthrene ND ug/kg 12/05/23 11:28 85-01-812/01/23 13:003831
Phenol ND ug/kg 12/05/23 11:28 108-95-212/01/23 13:003831
Pyrene ND ug/kg 12/05/23 11:28 129-00-012/01/23 13:003831
Pyridine ND ug/kg 12/05/23 11:28 110-86-112/01/23 13:003831
1,2,4-Trichlorobenzene ND ug/kg 12/05/23 11:28 120-82-112/01/23 13:003831
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92700661
Rowan Street Site
Sample:SS-1 Comp Lab ID:92700661001 Collected:11/28/23 14:15 Received:11/28/23 16:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4,5-Trichlorophenol ND ug/kg 12/05/23 11:28 95-95-412/01/23 13:003831
2,4,6-Trichlorophenol ND ug/kg 12/05/23 11:28 88-06-212/01/23 13:003831
Surrogates
Nitrobenzene-d5 (S)61 %12/05/23 11:28 4165-60-012/01/23 13:0010-130 1
2-Fluorobiphenyl (S)60 %12/05/23 11:28 321-60-812/01/23 13:0010-130 1
Terphenyl-d14 (S)70 %12/05/23 11:28 1718-51-012/01/23 13:0010-130 1
Phenol-d6 (S)60 %12/05/23 11:28 13127-88-312/01/23 13:0010-130 1
2-Fluorophenol (S)60 %12/05/23 11:28 367-12-412/01/23 13:0010-130 1
2,4,6-Tribromophenol (S)84 %12/05/23 11:28 118-79-612/01/23 13:0010-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.3 %12/01/23 15:23 N20.10 1
Analytical Method: 1010B/ASTM D8175-18
Pace National - Mt. Juliet
Wet Chemistry 1010B/ASTM D8175
Ignitability DNI at 170 deg F 12/04/23 03:1812/04/23 03:181
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 84.3 %12/02/23 11:0712/02/23 10:471
Analytical Method: EPA 9012B Preparation Method: 9012B
Pace National - Mt. Juliet
Wet Chemistry 9012B
Cyanide, Reactive ND mg/kg 12/01/23 19:5212/01/23 09:100.250 1
Analytical Method: EPA 9030B Preparation Method: 9030B
Pace National - Mt. Juliet
Wet Chemistry 9034-9030B
Sulfide, Reactive ND mg/kg 12/05/23 23:3012/05/23 09:2575.0 1
Analytical Method: EPA 9045D Preparation Method: 9045C/9045D
Pace National - Mt. Juliet
Wet Chemistry 9045D
pH 7.16 Std. Units 12/05/23 14:25 H312/04/23 14:241
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92700661
Rowan Street Site
Sample:SS-1 Grab Lab ID:92700661002 Collected:11/28/23 14:15 Received:11/28/23 16:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08),Unadjusted ND mg/kg 12/10/23 16:23 C412/10/23 16:2310.0 2
Aliphatic (C09-C12),Unadjusted 134 mg/kg 12/10/23 16:2312/10/23 16:2310.0 2
Aromatic (C09-C10),Unadjusted 38.1 mg/kg 12/10/23 16:23 TPHC9C10A12/10/23 16:2310.0 2
Total VPH 172 mg/kg 12/10/23 16:23 VPH12/10/23 16:2310.0 2
Surrogates
2,5-Dibromotoluene (FID)95.0 %12/10/23 16:23 615-59-8FID12/10/23 16:2370.0-130 2
2,5-Dibromotoluene (PID)62.1 %12/10/23 16:23 615-59-8PID SR12/10/23 16:2370.0-130 2
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 12/05/23 04:42 67-64-112/04/23 20:061301
Benzene ND ug/kg 12/05/23 04:42 71-43-212/04/23 20:066.5 1
Bromobenzene ND ug/kg 12/05/23 04:42 108-86-112/04/23 20:066.5 1
Bromochloromethane ND ug/kg 12/05/23 04:42 74-97-512/04/23 20:066.5 1
Bromodichloromethane ND ug/kg 12/05/23 04:42 75-27-412/04/23 20:066.5 1
Bromoform ND ug/kg 12/05/23 04:42 75-25-212/04/23 20:066.5 1
Bromomethane ND ug/kg 12/05/23 04:42 74-83-912/04/23 20:0626.0 1
2-Butanone (MEK)ND ug/kg 12/05/23 04:42 78-93-312/04/23 20:061301
n-Butylbenzene ND ug/kg 12/05/23 04:42 104-51-812/04/23 20:066.5 1
sec-Butylbenzene 951 ug/kg 12/05/23 04:42 135-98-812/04/23 20:066.5 1
tert-Butylbenzene 417 ug/kg 12/05/23 04:42 98-06-612/04/23 20:066.5 1
Carbon tetrachloride ND ug/kg 12/05/23 04:42 56-23-512/04/23 20:066.5 1
Chlorobenzene 17.8 ug/kg 12/05/23 04:42 108-90-712/04/23 20:066.5 1
Chloroethane ND ug/kg 12/05/23 04:42 75-00-312/04/23 20:0613.0 1
Chloroform ND ug/kg 12/05/23 04:42 67-66-312/04/23 20:066.5 1
Chloromethane ND ug/kg 12/05/23 04:42 74-87-312/04/23 20:0613.0 1
2-Chlorotoluene ND ug/kg 12/05/23 04:42 95-49-812/04/23 20:066.5 1
4-Chlorotoluene ND ug/kg 12/05/23 04:42 106-43-412/04/23 20:066.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 12/05/23 04:42 96-12-812/04/23 20:066.5 1
Dibromochloromethane ND ug/kg 12/05/23 04:42 124-48-112/04/23 20:066.5 1
1,2-Dibromoethane (EDB)ND ug/kg 12/05/23 04:42 106-93-412/04/23 20:066.5 1
Dibromomethane ND ug/kg 12/05/23 04:42 74-95-312/04/23 20:066.5 1
1,2-Dichlorobenzene ND ug/kg 12/05/23 04:42 95-50-112/04/23 20:066.5 1
1,3-Dichlorobenzene ND ug/kg 12/05/23 04:42 541-73-112/04/23 20:066.5 1
1,4-Dichlorobenzene ND ug/kg 12/05/23 04:42 106-46-712/04/23 20:066.5 1
Dichlorodifluoromethane ND ug/kg 12/05/23 04:42 75-71-812/04/23 20:0613.0 1
1,1-Dichloroethane ND ug/kg 12/05/23 04:42 75-34-312/04/23 20:066.5 1
1,2-Dichloroethane ND ug/kg 12/05/23 04:42 107-06-212/04/23 20:066.5 1
1,1-Dichloroethene ND ug/kg 12/05/23 04:42 75-35-412/04/23 20:066.5 1
cis-1,2-Dichloroethene ND ug/kg 12/05/23 04:42 156-59-212/04/23 20:066.5 1
trans-1,2-Dichloroethene ND ug/kg 12/05/23 04:42 156-60-512/04/23 20:066.5 1
1,2-Dichloropropane ND ug/kg 12/05/23 04:42 78-87-512/04/23 20:066.5 1
1,3-Dichloropropane ND ug/kg 12/05/23 04:42 142-28-912/04/23 20:066.5 1
2,2-Dichloropropane ND ug/kg 12/05/23 04:42 594-20-712/04/23 20:066.5 1
1,1-Dichloropropene ND ug/kg 12/05/23 04:42 563-58-612/04/23 20:066.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92700661
Rowan Street Site
Sample:SS-1 Grab Lab ID:92700661002 Collected:11/28/23 14:15 Received:11/28/23 16:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
cis-1,3-Dichloropropene ND ug/kg 12/05/23 04:42 10061-01-512/04/23 20:066.5 1
trans-1,3-Dichloropropene ND ug/kg 12/05/23 04:42 10061-02-612/04/23 20:066.5 1
Diisopropyl ether ND ug/kg 12/05/23 04:42 108-20-312/04/23 20:066.5 1
Ethylbenzene 50.8 ug/kg 12/05/23 04:42 100-41-412/04/23 20:066.5 1
Hexachloro-1,3-butadiene ND ug/kg 12/05/23 04:42 87-68-312/04/23 20:0613.0 1
2-Hexanone ND ug/kg 12/05/23 04:42 591-78-612/04/23 20:0665.1 1
Isopropylbenzene (Cumene)173 ug/kg 12/05/23 04:42 98-82-812/04/23 20:066.5 1
p-Isopropyltoluene ND ug/kg 12/05/23 04:42 99-87-612/04/23 20:066.5 1
Methylene Chloride ND ug/kg 12/05/23 04:42 75-09-212/04/23 20:0626.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 12/05/23 04:42 108-10-112/04/23 20:0665.1 1
Methyl-tert-butyl ether ND ug/kg 12/05/23 04:42 1634-04-412/04/23 20:066.5 1
Naphthalene 5610 ug/kg 12/05/23 04:42 91-20-312/04/23 20:066.5 1
n-Propylbenzene 472 ug/kg 12/05/23 04:42 103-65-112/04/23 20:066.5 1
Styrene ND ug/kg 12/05/23 04:42 100-42-512/04/23 20:066.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 12/05/23 04:42 630-20-612/04/23 20:066.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 12/05/23 04:42 79-34-512/04/23 20:066.5 1
Tetrachloroethene ND ug/kg 12/05/23 04:42 127-18-412/04/23 20:066.5 1
Toluene ND ug/kg 12/05/23 04:42 108-88-312/04/23 20:066.5 1
1,2,3-Trichlorobenzene ND ug/kg 12/05/23 04:42 87-61-612/04/23 20:066.5 1
1,2,4-Trichlorobenzene ND ug/kg 12/05/23 04:42 120-82-112/04/23 20:066.5 1
1,1,1-Trichloroethane ND ug/kg 12/05/23 04:42 71-55-612/04/23 20:066.5 1
1,1,2-Trichloroethane ND ug/kg 12/05/23 04:42 79-00-512/04/23 20:066.5 1
Trichloroethene ND ug/kg 12/05/23 04:42 79-01-612/04/23 20:066.5 1
Trichlorofluoromethane ND ug/kg 12/05/23 04:42 75-69-412/04/23 20:066.5 1
1,2,3-Trichloropropane ND ug/kg 12/05/23 04:42 96-18-412/04/23 20:066.5 1
1,2,4-Trimethylbenzene ND ug/kg 12/05/23 04:42 95-63-612/04/23 20:066.5 1
1,3,5-Trimethylbenzene ND ug/kg 12/05/23 04:42 108-67-812/04/23 20:066.5 1
Vinyl acetate ND ug/kg 12/05/23 04:42 108-05-412/04/23 20:0665.1 1
Vinyl chloride ND ug/kg 12/05/23 04:42 75-01-412/04/23 20:0613.0 1
Xylene (Total)ND ug/kg 12/05/23 04:42 1330-20-712/04/23 20:0613.0 1
m&p-Xylene ND ug/kg 12/05/23 04:42 179601-23-112/04/23 20:0613.0 1
o-Xylene ND ug/kg 12/05/23 04:42 95-47-612/04/23 20:066.5 1
Surrogates
Toluene-d8 (S)102 %12/05/23 04:42 2037-26-512/04/23 20:0670-130 1
4-Bromofluorobenzene (S)128 %12/05/23 04:42 460-00-412/04/23 20:0670-130 1
1,2-Dichloroethane-d4 (S)109 %12/05/23 04:42 17060-07-012/04/23 20:0670-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.6 %12/01/23 15:23 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2183333
MA DEP/NJ DEP
MADEP EPH
TPH by Method MADEPE
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92700661001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R4009685-1
Associated Lab Samples:92700661001
Matrix:Solid
Analyzed
Aliphatic (C09-C18),Unadjusted mg/kg ND 6.50 12/07/23 07:56
Aliphatic (C19-C36),Unadjusted mg/kg ND 6.50 12/07/23 07:56
TEH, Unadjusted mg/kg 9.45 6.50 12/07/23 07:56
1-Chloro-octadecane (S)%62 40.0-140 12/07/23 07:56
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R4009685-4
Associated Lab Samples:92700661001
Matrix:Solid
Analyzed
Aromatic (C11-C22), Unadjusted mg/kg ND 6.50 12/07/23 09:08
TEH, Unadjusted mg/kg ND 6.50 12/07/23 09:08
o-Terphenyl (S)%71.8 40.0-140 12/07/23 09:08
2-Fluorobiphenyl (S)%76.7 40.0-140 12/07/23 09:08
2-Bromonaphthalene (S)%73.3 40.0-140 12/07/23 09:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R4009685-2LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R4009685-3
Aliphatic (C09-C18),Unadjusted mg/kg 30.239.9 75.7 40.0-14079.431.7 4.85 25
Aliphatic (C19-C36),Unadjusted mg/kg 47.253.2 88.7 40.0-14095.350.7 7.15 25
1-Chloro-octadecane (S)%61.3 40.0-14065.8
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R4009685-5LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R4009685-6
Aromatic (C11-C22), Unadjusted mg/kg 91.6113 81.1 40.0-14084.495.4 4.06 25
o-Terphenyl (S)%69.5 40.0-14070.3
2-Fluorobiphenyl (S)%77.4 40.0-14079.7
2-Bromonaphthalene (S)%71.1 40.0-14072.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R4010498-1MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1683341-03
R4010498-2
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Aliphatic (C09-
C18),Unadjusted mg/kg P6,R144.5 0.00 40.0-1400.00 72.344.11480 753 353
Aliphatic (C19-
C36),Unadjusted mg/kg P6,R159.3 0.00 40.0-1400.00 57.458.8899 498 276
1-Chloro-octadecane (S)%55.0 40.0-14077.3
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R4010510-1MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1683341-03
R4010510-2
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Aromatic (C11-C22),
Unadjusted mg/kg P6,R11260.00 40.0-1400.00 74.3125838507232
o-Terphenyl (S)%65.5 40.0-14057.0
2-Fluorobiphenyl (S)%87.2 40.0-14075.0
2-Bromonaphthalene (S)%92.6 40.0-14084.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2182158
3510C
EPA 8081B
Pesticides (GC) 8081B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R4009022-1
Associated Lab Samples:92700661001
Matrix:Solid
Analyzed
Chlordane (Technical)mg/L ND 0.00500 12/06/23 12:45
Endrin mg/L ND 0.00500 12/06/23 12:45
Heptachlor mg/L ND 0.00500 12/06/23 12:45
Heptachlor epoxide mg/L ND 0.00500 12/06/23 12:45
gamma-BHC (Lindane)mg/L ND 0.00500 12/06/23 12:45
Methoxychlor mg/L ND 0.00500 12/06/23 12:45
Toxaphene mg/L ND 0.0100 12/06/23 12:45
Decachlorobiphenyl (S)%57.2 10.0-128 12/06/23 12:45
Tetrachloro-m-xylene (S)%74.1 10.0-127 12/06/23 12:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R4009022-2LABORATORY CONTROL SAMPLE:
LCSSpike
Endrin mg/L 0.009000.0100 90.0 57.0-134
Heptachlor mg/L 0.008250.0100 82.5 27.0-132
Heptachlor epoxide mg/L 0.008870.0100 88.7 57.0-130
gamma-BHC (Lindane)mg/L 0.008680.0100 86.8 55.0-129
Methoxychlor mg/L 0.008270.0100 82.7 54.0-155
Decachlorobiphenyl (S)%57.1 10.0-128
Tetrachloro-m-xylene (S)%69.4 10.0-127
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R4009022-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1681882-01
R4009022-4
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Endrin mg/L ML0.0100 6.23 10.0-1606.54 4.860.0100ND ND ND
Heptachlor mg/L ML0.0100 6.42 16.0-1365.74 11.20.0100ND ND ND
Heptachlor epoxide mg/L ML0.0100 7.63 10.0-1608.29 8.290.0100ND ND ND
gamma-BHC (Lindane)mg/L 0.0100 30.1 14.0-14136.6 19.50.0100ND ND ND
Methoxychlor mg/L ML0.0100 5.35 10.0-1606.31 16.50.0100ND ND ND
Decachlorobiphenyl (S)%SR2.89 10.0-1282.57
Tetrachloro-m-xylene (S)%SR6.19 10.0-1275.98
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2181810
8151A
EPA 8151A
Chlorinated Herb. (GC) 8151A
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92700661001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R4010288-1
Associated Lab Samples:92700661001
Matrix:Solid
Analyzed
2,4,5-TP (Silvex)mg/L ND 0.00200 12/08/23 12:42
2,4-D mg/L 0.00684 0.00200 12/08/23 12:42
2,4-DCAA (S)%44 14.0-158 12/08/23 12:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R4010288-2LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-TP (Silvex)mg/L 0.03860.0500 77.2 50.0-125
2,4-D mg/L 0.04640.0500 92.8 50.0-120
2,4-DCAA (S)%74.2 14.0-158
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R4010308-1MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1682445-01
R4010308-2
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2,4,5-TP (Silvex)mg/L 0.0500 99.2 50.0-12586.8 13.30.0500ND ND ND
2,4-D mg/L E,MH0.0500 124 50.0-120109 12.90.0500ND ND ND
2,4-DCAA (S)%97.5 14.0-15884.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2185766
KS LRH/MADEPV/MTDEQ
VPH/VPH
MADEP VPH
MADEPV
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92700661001, 92700661002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R4010617-3
Associated Lab Samples:92700661001, 92700661002
Matrix:Solid
Analyzed
Aliphatic (C05-C08),Unadjusted mg/kg ND 5.00 12/10/23 13:02
Aliphatic (C09-C12),Unadjusted mg/kg ND 5.00 12/10/23 13:02
Aromatic (C09-C10),Unadjusted mg/kg ND 5.00 12/10/23 13:02
Total VPH mg/kg ND 5.00 12/10/23 13:02
2,5-Dibromotoluene (FID)%88.4 70.0-130 12/10/23 13:02
2,5-Dibromotoluene (PID)%87.5 70.0-130 12/10/23 13:02
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R4010617-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R4010617-2
Aliphatic (C05-C08),Unadjusted mg/kg 53.160.0 88.5 70.0-13091.554.9 3.33 25
Aliphatic (C09-C12),Unadjusted mg/kg 64.070.0 91.4 70.0-13094.666.2 3.38 25
Aromatic (C09-C10),Unadjusted mg/kg 10.610.0 106 70.0-13096.29.62 9.69 25
Total VPH mg/kg 128140 91.4 70.0-13093.6131 2.32 25
2,5-Dibromotoluene (FID)%85.3 70.0-13086.7
2,5-Dibromotoluene (PID)%84.6 70.0-13085.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2181818
3015
EPA 6010D
Metals (ICP) 6010D
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R4007618-1
Associated Lab Samples:92700661001
Matrix:Solid
Analyzed
Arsenic mg/L ND 0.100 12/03/23 17:41
Barium mg/L ND 0.100 12/03/23 17:41
Cadmium mg/L ND 0.100 12/03/23 17:41
Chromium mg/L ND 0.100 12/03/23 17:41
Lead mg/L ND 0.100 12/03/23 17:41
Selenium mg/L ND 0.100 12/03/23 17:41
Silver mg/L ND 0.100 12/03/23 17:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R4007618-2LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/L 10.010.0 100 80.0-120
Barium mg/L 9.6310.0 96.3 80.0-120
Cadmium mg/L 9.7510.0 97.5 80.0-120
Chromium mg/L 9.7010.0 97.0 80.0-120
Lead mg/L 9.9810.0 99.8 80.0-120
Selenium mg/L 9.9710.0 99.7 80.0-120
Silver mg/L 1.792.00 89.4 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R4007618-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1682445-02
R4007618-5
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic mg/L 10.0 99.0 75.0-12599.3 0.37110.0ND ND ND
Barium mg/L 10.0 98.1 75.0-12598.2 0.16210.0ND ND ND
Cadmium mg/L 10.0 97.8 75.0-12597.9 0.08310.0ND ND ND
Chromium mg/L 10.0 97.8 75.0-12598.0 0.23310.0ND ND ND
Lead mg/L 10.0 99.2 75.0-12599.2 0.05610.0ND ND ND
Selenium mg/L 10.0 99.1 75.0-12598.5 0.65810.0ND ND ND
Silver mg/L 2.00 90.4 75.0-12590.6 0.2302.00ND ND ND
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R4007834-1MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1682597-04
R4007834-2
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic mg/L 10.0 103 75.0-125104 0.67610.0ND ND ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R4007834-1MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1682597-04
R4007834-2
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Barium mg/L 10.0 102 75.0-125102 0.60910.00.883 ND ND
Cadmium mg/L 10.0 101 75.0-125102 0.29010.0ND ND ND
Chromium mg/L 10.0 97.2 75.0-12598.0 0.78110.0ND ND ND
Lead mg/L 10.0 99.7 75.0-125100 0.27410.0ND ND ND
Selenium mg/L 10.0 102 75.0-125102 0.44910.0ND ND ND
Silver mg/L 2.00 90.7 75.0-12591.7 1.062.00ND ND ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2181544
7470A
EPA 7470A
Mercury 7470A
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R4007423-1
Associated Lab Samples:92700661001
Matrix:Solid
Analyzed
Mercury mg/L ND 0.0100 12/03/23 11:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R4007423-2LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/L 0.03110.0300 104 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R4007423-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1676502-02
R4007423-4
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury mg/L 0.0300 103 75.0-125105 2.160.0300ND ND ND
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R4007423-5MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1682445-01
R4007423-6
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury mg/L 0.0300 100 75.0-125100 0.1850.0300ND ND ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
817181
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92700661002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4229419
Associated Lab Samples:92700661002
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 12/04/23 21:44
1,1,1-Trichloroethane ug/kg ND 5.0 12/04/23 21:44
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 12/04/23 21:44
1,1,2-Trichloroethane ug/kg ND 5.0 12/04/23 21:44
1,1-Dichloroethane ug/kg ND 5.0 12/04/23 21:44
1,1-Dichloroethene ug/kg ND 5.0 12/04/23 21:44
1,1-Dichloropropene ug/kg ND 5.0 12/04/23 21:44
1,2,3-Trichlorobenzene ug/kg ND 5.0 12/04/23 21:44
1,2,3-Trichloropropane ug/kg ND 5.0 12/04/23 21:44
1,2,4-Trichlorobenzene ug/kg ND 5.0 12/04/23 21:44
1,2,4-Trimethylbenzene ug/kg ND 5.0 12/04/23 21:44
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 12/04/23 21:44
1,2-Dibromoethane (EDB)ug/kg ND 5.0 12/04/23 21:44
1,2-Dichlorobenzene ug/kg ND 5.0 12/04/23 21:44
1,2-Dichloroethane ug/kg ND 5.0 12/04/23 21:44
1,2-Dichloropropane ug/kg ND 5.0 12/04/23 21:44
1,3,5-Trimethylbenzene ug/kg ND 5.0 12/04/23 21:44
1,3-Dichlorobenzene ug/kg ND 5.0 12/04/23 21:44
1,3-Dichloropropane ug/kg ND 5.0 12/04/23 21:44
1,4-Dichlorobenzene ug/kg ND 5.0 12/04/23 21:44
2,2-Dichloropropane ug/kg ND 5.0 12/04/23 21:44
2-Butanone (MEK)ug/kg ND 100 12/04/23 21:44
2-Chlorotoluene ug/kg ND 5.0 12/04/23 21:44
2-Hexanone ug/kg ND 50.0 12/04/23 21:44
4-Chlorotoluene ug/kg ND 5.0 12/04/23 21:44
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 12/04/23 21:44
Acetone ug/kg ND 100 12/04/23 21:44
Benzene ug/kg ND 5.0 12/04/23 21:44
Bromobenzene ug/kg ND 5.0 12/04/23 21:44
Bromochloromethane ug/kg ND 5.0 12/04/23 21:44
Bromodichloromethane ug/kg ND 5.0 12/04/23 21:44
Bromoform ug/kg ND 5.0 12/04/23 21:44
Bromomethane ug/kg ND 20.0 12/04/23 21:44
Carbon tetrachloride ug/kg ND 5.0 12/04/23 21:44
Chlorobenzene ug/kg ND 5.0 12/04/23 21:44
Chloroethane ug/kg ND 10.0 12/04/23 21:44
Chloroform ug/kg ND 5.0 12/04/23 21:44
Chloromethane ug/kg ND 10.0 12/04/23 21:44
cis-1,2-Dichloroethene ug/kg ND 5.0 12/04/23 21:44
cis-1,3-Dichloropropene ug/kg ND 5.0 12/04/23 21:44
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4229419
Associated Lab Samples:92700661002
Matrix:Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 12/04/23 21:44
Dibromomethane ug/kg ND 5.0 12/04/23 21:44
Dichlorodifluoromethane ug/kg ND 10.0 12/04/23 21:44
Diisopropyl ether ug/kg ND 5.0 12/04/23 21:44
Ethylbenzene ug/kg ND 5.0 12/04/23 21:44
Hexachloro-1,3-butadiene ug/kg ND 10.0 12/04/23 21:44
Isopropylbenzene (Cumene)ug/kg ND 5.0 12/04/23 21:44
m&p-Xylene ug/kg ND 10.0 12/04/23 21:44
Methyl-tert-butyl ether ug/kg ND 5.0 12/04/23 21:44
Methylene Chloride ug/kg ND 20.0 12/04/23 21:44
n-Butylbenzene ug/kg ND 5.0 12/04/23 21:44
n-Propylbenzene ug/kg ND 5.0 12/04/23 21:44
Naphthalene ug/kg ND 5.0 12/04/23 21:44
o-Xylene ug/kg ND 5.0 12/04/23 21:44
p-Isopropyltoluene ug/kg ND 5.0 12/04/23 21:44
sec-Butylbenzene ug/kg ND 5.0 12/04/23 21:44
Styrene ug/kg ND 5.0 12/04/23 21:44
tert-Butylbenzene ug/kg ND 5.0 12/04/23 21:44
Tetrachloroethene ug/kg ND 5.0 12/04/23 21:44
Toluene ug/kg ND 5.0 12/04/23 21:44
trans-1,2-Dichloroethene ug/kg ND 5.0 12/04/23 21:44
trans-1,3-Dichloropropene ug/kg ND 5.0 12/04/23 21:44
Trichloroethene ug/kg ND 5.0 12/04/23 21:44
Trichlorofluoromethane ug/kg ND 5.0 12/04/23 21:44
Vinyl acetate ug/kg ND 50.0 12/04/23 21:44
Vinyl chloride ug/kg ND 10.0 12/04/23 21:44
Xylene (Total)ug/kg ND 10.0 12/04/23 21:44
1,2-Dichloroethane-d4 (S)%111 70-130 12/04/23 21:44
4-Bromofluorobenzene (S)%109 70-130 12/04/23 21:44
Toluene-d8 (S)%101 70-130 12/04/23 21:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4229420LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 505500 101 70-130
1,1,1-Trichloroethane ug/kg 510500 102 70-130
1,1,2,2-Tetrachloroethane ug/kg 524500 105 70-130
1,1,2-Trichloroethane ug/kg 480500 96 70-130
1,1-Dichloroethane ug/kg 525500 105 70-130
1,1-Dichloroethene ug/kg 507500 101 70-132
1,1-Dichloropropene ug/kg 542500 108 70-130
1,2,3-Trichlorobenzene ug/kg 483500 97 62-136
1,2,3-Trichloropropane ug/kg 519500 104 70-130
1,2,4-Trichlorobenzene ug/kg 484500 97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4229420LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 553500 111 70-130
1,2-Dibromo-3-chloropropane ug/kg 455500 91 65-130
1,2-Dibromoethane (EDB)ug/kg 474500 95 70-130
1,2-Dichlorobenzene ug/kg 481500 96 70-130
1,2-Dichloroethane ug/kg 487500 97 70-130
1,2-Dichloropropane ug/kg 513500 103 70-130
1,3,5-Trimethylbenzene ug/kg 543500 109 70-130
1,3-Dichlorobenzene ug/kg 479500 96 70-130
1,3-Dichloropropane ug/kg 498500 100 70-130
1,4-Dichlorobenzene ug/kg 478500 96 70-130
2,2-Dichloropropane ug/kg 491500 98 60-130
2-Butanone (MEK)ug/kg 11401000 114 66-130
2-Chlorotoluene ug/kg 523500 105 70-130
2-Hexanone ug/kg 11701000 117 68-130
4-Chlorotoluene ug/kg 530500 106 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 11301000 113 70-130
Acetone ug/kg 10601000 106 60-130
Benzene ug/kg 481500 96 70-130
Bromobenzene ug/kg 470500 94 70-130
Bromochloromethane ug/kg 466500 93 70-130
Bromodichloromethane ug/kg 473500 95 70-130
Bromoform ug/kg 480500 96 70-130
Bromomethane ug/kg 612500 122 43-175
Carbon tetrachloride ug/kg 459500 92 70-130
Chlorobenzene ug/kg 482500 96 70-130
Chloroethane ug/kg 545500 109 70-145
Chloroform ug/kg 490500 98 70-130
Chloromethane ug/kg 600500 120 66-146
cis-1,2-Dichloroethene ug/kg 527500 105 70-130
cis-1,3-Dichloropropene ug/kg 472500 94 70-130
Dibromochloromethane ug/kg 484500 97 70-130
Dibromomethane ug/kg 450500 90 70-130
Dichlorodifluoromethane ug/kg 462500 92 42-197
Diisopropyl ether ug/kg 539500 108 68-130
Ethylbenzene ug/kg 465500 93 70-130
Hexachloro-1,3-butadiene ug/kg 491500 98 70-130
Isopropylbenzene (Cumene)ug/kg 543500 109 70-130
m&p-Xylene ug/kg 10701000 107 70-130
Methyl-tert-butyl ether ug/kg 460500 92 70-130
Methylene Chloride ug/kg 503500 101 65-130
n-Butylbenzene ug/kg 548500 110 70-130
n-Propylbenzene ug/kg 519500 104 70-130
Naphthalene ug/kg 557500 111 65-135
o-Xylene ug/kg 503500 101 70-130
p-Isopropyltoluene ug/kg 558500 112 70-130
sec-Butylbenzene ug/kg 531500 106 70-130
Styrene ug/kg 520500 104 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4229420LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 488500 98 70-130
Tetrachloroethene ug/kg 513500 103 70-130
Toluene ug/kg 470500 94 70-130
trans-1,2-Dichloroethene ug/kg 559500 112 70-130
trans-1,3-Dichloropropene ug/kg 460500 92 70-130
Trichloroethene ug/kg 477500 95 70-130
Trichlorofluoromethane ug/kg 430500 86 62-140
Vinyl acetate ug/kg 11301000 113 70-140
Vinyl chloride ug/kg 517500 103 70-152
Xylene (Total)ug/kg 15701500 105 70-130
1,2-Dichloroethane-d4 (S)%109 70-130
4-Bromofluorobenzene (S)%110 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4229421MATRIX SPIKE SAMPLE:
MSSpike
Result
92701288001
1,1,1,2-Tetrachloroethane ug/kg 296742 39 22-1660.0041J mg/kg
1,1,1-Trichloroethane ug/kg 313742 42 23-172ND
1,1,2,2-Tetrachloroethane ug/kg 297742 39 21-1580.0079 mg/kg
1,1,2-Trichloroethane ug/kg 284742 38 25-160ND
1,1-Dichloroethane ug/kg 320742 43 22-166ND
1,1-Dichloroethene ug/kg 311742 42 18-183ND
1,1-Dichloropropene ug/kg 321742 43 20-181ND
1,2,3-Trichlorobenzene ug/kg 294742 40 10-161ND
1,2,3-Trichloropropane ug/kg 283742 38 21-147ND
1,2,4-Trichlorobenzene ug/kg 285742 38 10-159ND
1,2,4-Trimethylbenzene ug/kg 323742 44 17-170ND
1,2-Dibromo-3-chloropropane ug/kg 255742 34 10-135ND
1,2-Dibromoethane (EDB)ug/kg 264742 36 30-154ND
1,2-Dichlorobenzene ug/kg 288742 38 26-1620.0049J mg/kg
1,2-Dichloroethane ug/kg 287742 39 23-161ND
1,2-Dichloropropane ug/kg 310742 42 29-165ND
1,3,5-Trimethylbenzene ug/kg 314742 42 20-1720.0044J mg/kg
1,3-Dichlorobenzene ug/kg 283742 37 22-1640.0051J mg/kg
1,3-Dichloropropane ug/kg 282742 38 27-156ND
1,4-Dichlorobenzene ug/kg 266742 35 20-1610.0046J mg/kg
2,2-Dichloropropane ug/kg 286742 39 10-159ND
2-Butanone (MEK)ug/kg 5951480 40 13-143ND
2-Chlorotoluene ug/kg 309742 42 21-166ND
2-Hexanone ug/kg 6021480 39 19-1450.017J mg/kg
4-Chlorotoluene ug/kg 300742 40 19-163ND
4-Methyl-2-pentanone (MIBK)ug/kg 6091480 40 21-1510.013J mg/kg
Acetone ug/kg 5281480 36 10-133ND
Benzene ug/kg 296742 39 29-1560.0037J mg/kg
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4229421MATRIX SPIKE SAMPLE:
MSSpike
Result
92701288001
Bromobenzene ug/kg 299742 40 25-161ND
Bromochloromethane ug/kg 266742 36 27-158ND
Bromodichloromethane ug/kg 272742 37 23-158ND
Bromoform ug/kg 253742 34 19-152ND
Bromomethane ug/kg 137742 19 10-152ND
Carbon tetrachloride ug/kg 287742 39 18-172ND
Chlorobenzene ug/kg 287742 38 26-166ND
Chloroethane ug/kg 69.5 M1742910-130ND
Chloroform ug/kg 294742 40 25-161ND
Chloromethane ug/kg 387742 51 27-1970.0069J mg/kg
cis-1,2-Dichloroethene ug/kg 317742 43 28-165ND
cis-1,3-Dichloropropene ug/kg 267742 35 23-1590.0054J mg/kg
Dibromochloromethane ug/kg 257742 35 21-151ND
Dibromomethane ug/kg 251 M17423438-158ND
Dichlorodifluoromethane ug/kg 311742 40 10-2000.016 mg/kg
Diisopropyl ether ug/kg 317742 42 23-1600.0055J mg/kg
Ethylbenzene ug/kg 283742 37 22-1630.0090 mg/kg
Hexachloro-1,3-butadiene ug/kg 273742 37 10-192ND
Isopropylbenzene (Cumene)ug/kg 325742 43 24-1730.0040J mg/kg
m&p-Xylene ug/kg 6221480 41 22-1710.0095J mg/kg
Methyl-tert-butyl ether ug/kg 266742 36 25-153ND
Methylene Chloride ug/kg 276742 37 10-165ND
n-Butylbenzene ug/kg 296742 39 10-186ND
n-Propylbenzene ug/kg 293742 40 16-171ND
Naphthalene ug/kg 352742 47 10-159ND
o-Xylene ug/kg 307742 41 23-171ND
p-Isopropyltoluene ug/kg 305742 40 13-1840.0047J mg/kg
sec-Butylbenzene ug/kg 297742 40 16-182ND
Styrene ug/kg 300742 40 25-169ND
tert-Butylbenzene ug/kg 285742 38 20-174ND
Tetrachloroethene ug/kg 272742 37 14-171ND
Toluene ug/kg 285742 38 24-166ND
trans-1,2-Dichloroethene ug/kg 329742 44 24-170ND
trans-1,3-Dichloropropene ug/kg 260742 34 22-1570.0050J mg/kg
Trichloroethene ug/kg 283742 38 23-176ND
Trichlorofluoromethane ug/kg 59.9 M1742810-138ND
Vinyl acetate ug/kg 6061480 41 11-166ND
Vinyl chloride ug/kg 351742 47 21-200ND
Xylene (Total)ug/kg 9292230 41 23-1700.0095J mg/kg
1,2-Dichloroethane-d4 (S)%111 70-130
4-Bromofluorobenzene (S)%110 70-130
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92701288002
4229422SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg 5.9J0.0063J
mg/kg
Hexachloro-1,3-butadiene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92701288002
4229422SAMPLE DUPLICATE:
Isopropylbenzene (Cumene)ug/kg NDND
m&p-Xylene ug/kg 11J0.011J mg/kg
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg 7.7 130.0087 mg/kg
o-Xylene ug/kg 3.5J0.0044J
mg/kg
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg ND0.0041J
mg/kg
Toluene ug/kg 16.1 70.015 mg/kg
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg ND0.016 mg/kg
1,2-Dichloroethane-d4 (S)%110111
4-Bromofluorobenzene (S)%108108
Toluene-d8 (S)%101101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
816538
EPA 3546
EPA 8015C
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92700661001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4226452
Associated Lab Samples:92700661001
Matrix:Solid
Analyzed
Diesel Range Organics(C10-C28)mg/kg ND 4.9 12/01/23 11:37
n-Pentacosane (S)%66 10-133 12/01/23 11:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4226453LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 45.765.8 69 43-130
n-Pentacosane (S)%59 10-133
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4226454MATRIX SPIKE SAMPLE:
MSSpike
Result
92700609001
Diesel Range Organics(C10-C28)mg/kg 88.775 80 15-13028.9
n-Pentacosane (S)%61 10-133
Parameter Units
Dup
Result QualifiersRPDResult
92700790001
4226455SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg 10800 911800
n-Pentacosane (S)%0 S40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
816710
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92700661001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4227039
Associated Lab Samples:92700661001
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 334 12/04/23 10:28
1,2-Dichlorobenzene ug/kg ND 334 12/04/23 10:28
1,3-Dichlorobenzene ug/kg ND 334 12/04/23 10:28
1,4-Dichlorobenzene ug/kg ND 334 12/04/23 10:28
1-Methylnaphthalene ug/kg ND 334 12/04/23 10:28
2,2'-Oxybis(1-chloropropane)ug/kg ND 334 v112/04/23 10:28
2,4,5-Trichlorophenol ug/kg ND 334 12/04/23 10:28
2,4,6-Trichlorophenol ug/kg ND 334 12/04/23 10:28
2,4-Dichlorophenol ug/kg ND 334 12/04/23 10:28
2,4-Dimethylphenol ug/kg ND 334 12/04/23 10:28
2,4-Dinitrophenol ug/kg ND 1670 12/04/23 10:28
2,4-Dinitrotoluene ug/kg ND 334 12/04/23 10:28
2,6-Dinitrotoluene ug/kg ND 334 12/04/23 10:28
2-Chloronaphthalene ug/kg ND 334 12/04/23 10:28
2-Chlorophenol ug/kg ND 334 12/04/23 10:28
2-Methylnaphthalene ug/kg ND 334 12/04/23 10:28
2-Methylphenol(o-Cresol)ug/kg ND 334 12/04/23 10:28
2-Nitroaniline ug/kg ND 1670 12/04/23 10:28
2-Nitrophenol ug/kg ND 334 12/04/23 10:28
3&4-Methylphenol(m&p Cresol)ug/kg ND 334 12/04/23 10:28
3,3'-Dichlorobenzidine ug/kg ND 669 12/04/23 10:28
3-Nitroaniline ug/kg ND 1670 12/04/23 10:28
4,6-Dinitro-2-methylphenol ug/kg ND 669 12/04/23 10:28
4-Bromophenylphenyl ether ug/kg ND 334 12/04/23 10:28
4-Chloro-3-methylphenol ug/kg ND 669 12/04/23 10:28
4-Chloroaniline ug/kg ND 669 12/04/23 10:28
4-Chlorophenylphenyl ether ug/kg ND 334 12/04/23 10:28
4-Nitroaniline ug/kg ND 669 12/04/23 10:28
4-Nitrophenol ug/kg ND 1670 12/04/23 10:28
Acenaphthene ug/kg ND 334 12/04/23 10:28
Acenaphthylene ug/kg ND 334 12/04/23 10:28
Aniline ug/kg ND 334 12/04/23 10:28
Anthracene ug/kg ND 334 12/04/23 10:28
Benzo(a)anthracene ug/kg ND 334 12/04/23 10:28
Benzo(a)pyrene ug/kg ND 334 12/04/23 10:28
Benzo(b)fluoranthene ug/kg ND 334 12/04/23 10:28
Benzo(g,h,i)perylene ug/kg ND 334 12/04/23 10:28
Benzo(k)fluoranthene ug/kg ND 334 12/04/23 10:28
Benzoic Acid ug/kg ND 1670 12/04/23 10:28
Benzyl alcohol ug/kg ND 669 12/04/23 10:28
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4227039
Associated Lab Samples:92700661001
Matrix:Solid
Analyzed
bis(2-Chloroethoxy)methane ug/kg ND 334 12/04/23 10:28
bis(2-Chloroethyl) ether ug/kg ND 334 12/04/23 10:28
bis(2-Ethylhexyl)phthalate ug/kg ND 334 12/04/23 10:28
Butylbenzylphthalate ug/kg ND 334 12/04/23 10:28
Chrysene ug/kg ND 334 12/04/23 10:28
Di-n-butylphthalate ug/kg ND 334 12/04/23 10:28
Di-n-octylphthalate ug/kg ND 334 12/04/23 10:28
Dibenz(a,h)anthracene ug/kg ND 334 12/04/23 10:28
Dibenzofuran ug/kg ND 334 12/04/23 10:28
Diethylphthalate ug/kg ND 334 12/04/23 10:28
Dimethylphthalate ug/kg ND 334 12/04/23 10:28
Fluoranthene ug/kg ND 334 12/04/23 10:28
Fluorene ug/kg ND 334 12/04/23 10:28
Hexachloro-1,3-butadiene ug/kg ND 334 12/04/23 10:28
Hexachlorobenzene ug/kg ND 334 12/04/23 10:28
Hexachlorocyclopentadiene ug/kg ND 334 12/04/23 10:28
Hexachloroethane ug/kg ND 334 12/04/23 10:28
Indeno(1,2,3-cd)pyrene ug/kg ND 334 12/04/23 10:28
Isophorone ug/kg ND 334 12/04/23 10:28
N-Nitroso-di-n-propylamine ug/kg ND 334 12/04/23 10:28
N-Nitrosodimethylamine ug/kg ND 334 12/04/23 10:28
N-Nitrosodiphenylamine ug/kg ND 334 12/04/23 10:28
Naphthalene ug/kg ND 334 12/04/23 10:28
Nitrobenzene ug/kg ND 334 12/04/23 10:28
Pentachlorophenol ug/kg ND 669 12/04/23 10:28
Phenanthrene ug/kg ND 334 12/04/23 10:28
Phenol ug/kg ND 334 12/04/23 10:28
Pyrene ug/kg ND 334 12/04/23 10:28
Pyridine ug/kg ND 334 12/04/23 10:28
2,4,6-Tribromophenol (S)%65 10-130 12/04/23 10:28
2-Fluorobiphenyl (S)%65 10-130 12/04/23 10:28
2-Fluorophenol (S)%69 10-130 12/04/23 10:28
Nitrobenzene-d5 (S)%79 10-130 12/04/23 10:28
Phenol-d6 (S)%70 10-130 12/04/23 10:28
Terphenyl-d14 (S)%84 10-130 12/04/23 10:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4227040LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 9361650 57 40-130
1,2-Dichlorobenzene ug/kg 9331650 57 37-130
1,3-Dichlorobenzene ug/kg 9361650 57 36-130
1,4-Dichlorobenzene ug/kg 9311650 56 36-130
1-Methylnaphthalene ug/kg 9711650 59 46-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4227040LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 1100 v116506612-130
2,4,5-Trichlorophenol ug/kg 9141650 55 49-130
2,4,6-Trichlorophenol ug/kg 9001650 55 48-130
2,4-Dichlorophenol ug/kg 9481650 57 45-130
2,4-Dimethylphenol ug/kg 10201650 62 45-130
2,4-Dinitrophenol ug/kg 47808250 58 23-130
2,4-Dinitrotoluene ug/kg 10901650 66 50-130
2,6-Dinitrotoluene ug/kg 10601650 64 53-130
2-Chloronaphthalene ug/kg 8591650 52 46-130
2-Chlorophenol ug/kg 10001650 61 39-130
2-Methylnaphthalene ug/kg 9811650 59 45-130
2-Methylphenol(o-Cresol)ug/kg 10101650 61 38-130
2-Nitroaniline ug/kg 21203300 64 43-130
2-Nitrophenol ug/kg 9771650 59 43-130
3&4-Methylphenol(m&p Cresol)ug/kg 9811650 59 34-130
3,3'-Dichlorobenzidine ug/kg 24203300 73 68-130
3-Nitroaniline ug/kg 20203300 61 36-130
4,6-Dinitro-2-methylphenol ug/kg 23503300 71 38-130
4-Bromophenylphenyl ether ug/kg 11501650 70 52-130
4-Chloro-3-methylphenol ug/kg 21403300 65 45-130
4-Chloroaniline ug/kg 19903300 60 41-130
4-Chlorophenylphenyl ether ug/kg 10501650 64 46-130
4-Nitroaniline ug/kg 21103300 64 40-130
4-Nitrophenol ug/kg 55608250 67 34-130
Acenaphthene ug/kg 9761650 59 47-130
Acenaphthylene ug/kg 9731650 59 50-130
Aniline ug/kg 9571650 58 33-130
Anthracene ug/kg 11801650 71 46-130
Benzo(a)anthracene ug/kg 12501650 76 49-130
Benzo(a)pyrene ug/kg 11301650 68 45-130
Benzo(b)fluoranthene ug/kg 10701650 65 45-130
Benzo(g,h,i)perylene ug/kg 11801650 71 44-130
Benzo(k)fluoranthene ug/kg 11701650 71 46-130
Benzoic Acid ug/kg 21808250 26 14-130
Benzyl alcohol ug/kg 19403300 59 39-130
bis(2-Chloroethoxy)methane ug/kg 9951650 60 41-130
bis(2-Chloroethyl) ether ug/kg 10101650 61 34-130
bis(2-Ethylhexyl)phthalate ug/kg 14001650 85 39-130
Butylbenzylphthalate ug/kg 13401650 81 48-130
Chrysene ug/kg 13601650 82 50-130
Di-n-butylphthalate ug/kg 12501650 75 46-130
Di-n-octylphthalate ug/kg 13901650 84 49-130
Dibenz(a,h)anthracene ug/kg 11501650 69 46-130
Dibenzofuran ug/kg 9691650 59 49-130
Diethylphthalate ug/kg 11201650 68 49-130
Dimethylphthalate ug/kg 10701650 65 50-130
Fluoranthene ug/kg 12301650 74 49-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4227040LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 10501650 64 47-130
Hexachloro-1,3-butadiene ug/kg 9861650 60 36-130
Hexachlorobenzene ug/kg 11101650 67 52-130
Hexachlorocyclopentadiene ug/kg 7241650 44 10-130
Hexachloroethane ug/kg 9651650 59 36-130
Indeno(1,2,3-cd)pyrene ug/kg 11201650 68 44-130
Isophorone ug/kg 10801650 66 40-130
N-Nitroso-di-n-propylamine ug/kg 10901650 66 34-130
N-Nitrosodimethylamine ug/kg 9841650 60 29-130
N-Nitrosodiphenylamine ug/kg 11301650 68 47-130
Naphthalene ug/kg 10201650 62 43-130
Nitrobenzene ug/kg 10201650 62 41-130
Pentachlorophenol ug/kg 20103300 61 35-130
Phenanthrene ug/kg 12001650 72 50-130
Phenol ug/kg 10801650 65 39-130
Pyrene ug/kg 12901650 78 51-130
Pyridine ug/kg 6971650 42 21-130
2,4,6-Tribromophenol (S)%66 10-130
2-Fluorobiphenyl (S)%53 10-130
2-Fluorophenol (S)%59 10-130
Nitrobenzene-d5 (S)%62 10-130
Phenol-d6 (S)%59 10-130
Terphenyl-d14 (S)%77 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4227041MATRIX SPIKE SAMPLE:
MSSpike
Result
92701037001
1,2,4-Trichlorobenzene ug/kg 11402070 55 22-130ND
1,2-Dichlorobenzene ug/kg 11102070 53 22-130ND
1,3-Dichlorobenzene ug/kg 10702070 52 22-130ND
1,4-Dichlorobenzene ug/kg 10802070 52 21-130ND
1-Methylnaphthalene ug/kg 12502070 60 27-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 11602070 56 10-130ND
2,4,5-Trichlorophenol ug/kg 13002070 63 18-130ND
2,4,6-Trichlorophenol ug/kg 12602070 61 17-130ND
2,4-Dichlorophenol ug/kg 13402070 65 19-130ND
2,4-Dimethylphenol ug/kg 13902070 67 17-130ND
2,4-Dinitrophenol ug/kg ND M110400010-130ND
2,4-Dinitrotoluene ug/kg 13702070 66 31-130ND
2,6-Dinitrotoluene ug/kg 13602070 66 33-130ND
2-Chloronaphthalene ug/kg 10502070 51 26-130ND
2-Chlorophenol ug/kg 13902070 67 19-130ND
2-Methylnaphthalene ug/kg 12402070 60 26-130ND
2-Methylphenol(o-Cresol)ug/kg 13402070 65 19-130ND
2-Nitroaniline ug/kg 25604160 62 29-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4227041MATRIX SPIKE SAMPLE:
MSSpike
Result
92701037001
2-Nitrophenol ug/kg 11902070 57 16-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 13302070 64 14-130ND
3,3'-Dichlorobenzidine ug/kg 28804160 69 16-130ND
3-Nitroaniline ug/kg 28804160 69 28-130ND
4,6-Dinitro-2-methylphenol ug/kg 11004160 26 10-131ND
4-Bromophenylphenyl ether ug/kg 12702070 61 32-130ND
4-Chloro-3-methylphenol ug/kg 27804160 67 26-130ND
4-Chloroaniline ug/kg 27204160 65 19-130ND
4-Chlorophenylphenyl ether ug/kg 11602070 56 29-130ND
4-Nitroaniline ug/kg 2900 v141607022-130ND
4-Nitrophenol ug/kg 604010400 58 10-130ND
Acenaphthene ug/kg 11602070 56 29-130ND
Acenaphthylene ug/kg 11802070 57 27-130ND
Aniline ug/kg 13502070 65 10-130ND
Anthracene ug/kg 12502070 60 26-130ND
Benzo(a)anthracene ug/kg 13502070 65 31-130ND
Benzo(a)pyrene ug/kg 11902070 57 24-130ND
Benzo(b)fluoranthene ug/kg 11802070 57 12-137ND
Benzo(g,h,i)perylene ug/kg 12202070 59 16-130ND
Benzo(k)fluoranthene ug/kg 11802070 57 27-130ND
Benzoic Acid ug/kg ND M110400210-130ND
Benzyl alcohol ug/kg 26404160 64 25-130ND
bis(2-Chloroethoxy)methane ug/kg 12702070 61 26-130ND
bis(2-Chloroethyl) ether ug/kg 12602070 60 23-130ND
bis(2-Ethylhexyl)phthalate ug/kg 17702070 85 20-130ND
Butylbenzylphthalate ug/kg 16202070 78 28-130ND
Chrysene ug/kg 13802070 66 29-130ND
Di-n-butylphthalate ug/kg 13002070 63 29-130ND
Di-n-octylphthalate ug/kg 1720 v120708330-130ND
Dibenz(a,h)anthracene ug/kg 12502070 60 27-130ND
Dibenzofuran ug/kg 11402070 55 33-130ND
Diethylphthalate ug/kg 13902070 67 34-130ND
Dimethylphthalate ug/kg 13902070 67 35-130ND
Fluoranthene ug/kg 12302070 59 26-130ND
Fluorene ug/kg 12002070 58 27-130ND
Hexachloro-1,3-butadiene ug/kg 9822070 47 19-130ND
Hexachlorobenzene ug/kg 13202070 64 31-130ND
Hexachlorocyclopentadiene ug/kg 444 v320702110-130ND
Hexachloroethane ug/kg 9342070 45 21-130ND
Indeno(1,2,3-cd)pyrene ug/kg 11902070 58 16-130ND
Isophorone ug/kg 12902070 62 29-130ND
N-Nitroso-di-n-propylamine ug/kg 13002070 62 22-130ND
N-Nitrosodimethylamine ug/kg 12402070 60 15-130ND
N-Nitrosodiphenylamine ug/kg 13502070 65 30-130ND
Naphthalene ug/kg 12402070 60 24-130ND
Nitrobenzene ug/kg 12102070 58 25-130ND
Pentachlorophenol ug/kg 27804160 67 10-130ND
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4227041MATRIX SPIKE SAMPLE:
MSSpike
Result
92701037001
Phenanthrene ug/kg 12802070 62 28-130ND
Phenol ug/kg 13002070 63 18-130ND
Pyrene ug/kg 14902070 72 27-130ND
Pyridine ug/kg 11702070 56 10-130ND
2,4,6-Tribromophenol (S)%76 10-130
2-Fluorobiphenyl (S)%41 10-130
2-Fluorophenol (S)%60 10-130
Nitrobenzene-d5 (S)%53 10-130
Phenol-d6 (S)%61 10-130
Terphenyl-d14 (S)%80 10-130
Parameter Units
Dup
Result QualifiersRPDResult
92700839004
4227042SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
1-Methylnaphthalene ug/kg NDND
2,2'-Oxybis(1-chloropropane)ug/kg NDND
2,4,5-Trichlorophenol ug/kg NDND
2,4,6-Trichlorophenol ug/kg NDND
2,4-Dichlorophenol ug/kg NDND
2,4-Dimethylphenol ug/kg NDND
2,4-Dinitrophenol ug/kg NDND
2,4-Dinitrotoluene ug/kg NDND
2,6-Dinitrotoluene ug/kg NDND
2-Chloronaphthalene ug/kg NDND
2-Chlorophenol ug/kg NDND
2-Methylnaphthalene ug/kg NDND
2-Methylphenol(o-Cresol)ug/kg NDND
2-Nitroaniline ug/kg NDND
2-Nitrophenol ug/kg NDND
3&4-Methylphenol(m&p Cresol)ug/kg NDND
3,3'-Dichlorobenzidine ug/kg NDND
3-Nitroaniline ug/kg NDND
4,6-Dinitro-2-methylphenol ug/kg NDND
4-Bromophenylphenyl ether ug/kg NDND
4-Chloro-3-methylphenol ug/kg NDND
4-Chloroaniline ug/kg NDND
4-Chlorophenylphenyl ether ug/kg NDND
4-Nitroaniline ug/kg ND v1ND
4-Nitrophenol ug/kg NDND
Acenaphthene ug/kg NDND
Acenaphthylene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
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Page 31 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92700839004
4227042SAMPLE DUPLICATE:
Aniline ug/kg NDND
Anthracene ug/kg NDND
Benzo(a)anthracene ug/kg NDND
Benzo(a)pyrene ug/kg NDND
Benzo(b)fluoranthene ug/kg NDND
Benzo(g,h,i)perylene ug/kg NDND
Benzo(k)fluoranthene ug/kg NDND
Benzoic Acid ug/kg NDND
Benzyl alcohol ug/kg NDND
bis(2-Chloroethoxy)methane ug/kg NDND
bis(2-Chloroethyl) ether ug/kg NDND
bis(2-Ethylhexyl)phthalate ug/kg NDND
Butylbenzylphthalate ug/kg NDND
Chrysene ug/kg NDND
Di-n-butylphthalate ug/kg NDND
Di-n-octylphthalate ug/kg ND v1ND
Dibenz(a,h)anthracene ug/kg NDND
Dibenzofuran ug/kg NDND
Diethylphthalate ug/kg NDND
Dimethylphthalate ug/kg NDND
Fluoranthene ug/kg NDND
Fluorene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Hexachlorobenzene ug/kg NDND
Hexachlorocyclopentadiene ug/kg ND v2ND
Hexachloroethane ug/kg NDND
Indeno(1,2,3-cd)pyrene ug/kg NDND
Isophorone ug/kg NDND
N-Nitroso-di-n-propylamine ug/kg NDND
N-Nitrosodimethylamine ug/kg NDND
N-Nitrosodiphenylamine ug/kg NDND
Naphthalene ug/kg NDND
Nitrobenzene ug/kg NDND
Pentachlorophenol ug/kg NDND
Phenanthrene ug/kg NDND
Phenol ug/kg NDND
Pyrene ug/kg NDND
Pyridine ug/kg NDND
2,4,6-Tribromophenol (S)%5057
2-Fluorobiphenyl (S)%4453
2-Fluorophenol (S)%3340
Nitrobenzene-d5 (S)%4857
Phenol-d6 (S)%3946
Terphenyl-d14 (S)%7482
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
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Huntersville, NC 28078
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Page 32 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
816770
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92700661001, 92700661002
Parameter Units
Dup
Result QualifiersRPDResult
92700609001
4227490SAMPLE DUPLICATE:
Percent Moisture %10.9 N2111.0
Parameter Units
Dup
Result QualifiersRPDResult
92700939010
4227491SAMPLE DUPLICATE:
Percent Moisture %18.8 N2119.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2182050
1010B/ASTM D8175-18
1010B/ASTM D8175-18
Wet Chemistry 1010B/ASTM D8175
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92700661001
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R4007574-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R4007574-2
Ignitability deg F 125126 99.1 95.6-104101127 1.59 10
Parameter Units
Dup
Result QualifiersRPDResult
L1682413-05
R4007574-3SAMPLE DUPLICATE:
Ignitability deg F DNI at 170 0.00ND
Parameter Units
Dup
Result QualifiersRPDResult
L1682844-09
R4007574-4SAMPLE DUPLICATE:
Ignitability deg F DNI at 170 0.00ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2181430
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92700661001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R4007596-1
Associated Lab Samples:92700661001
Matrix:Solid
Analyzed
Total Solids %ND 12/02/23 11:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R4007596-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 90.0-110
Parameter Units
Dup
Result QualifiersRPDResult
L1683201-01
R4007596-3SAMPLE DUPLICATE:
Total Solids %82.2 0.83282.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2180842
9012B
EPA 9012B
Wet Chemistry 9012B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92700661001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R4007216-1
Associated Lab Samples:92700661001
Matrix:Solid
Analyzed
Cyanide, Reactive mg/kg ND 0.250 12/01/23 19:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R4007216-2LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide, Reactive mg/kg 2.582.50 103 85.0-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R4007216-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1679700-12
R4007216-5
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cyanide, Reactive mg/kg 1.67 101 75.0-12596.7 4.401.670.0551 ND ND
Parameter Units
Dup
Result QualifiersRPDResult
L1679700-12
R4007216-3SAMPLE DUPLICATE:
Cyanide, Reactive mg/kg ND 0.000.0551
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
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Huntersville, NC 28078
[phone]
Page 36 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2182408
9030B
EPA 9030B
Wet Chemistry 9034-9030B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92700661001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R4008537-1
Associated Lab Samples:92700661001
Matrix:Solid
Analyzed
Sulfide, Reactive mg/kg ND 75.0 12/05/23 23:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R4008537-2LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide, Reactive mg/kg 108100 108 53.8-124
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R4008537-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1683002-02
R4008537-4
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfide, Reactive mg/kg 100 82.1 10.0-13670.2 15.7100NDNDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 37 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92700661
Rowan Street Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2180826
9045C/9045D
EPA 9045D
Wet Chemistry 9045D
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92700661001
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R4008317-1LABORATORY CONTROL SAMPLE:
LCSSpike
pH Std. Units 10.010.0 100 99.0-101
Parameter Units
Dup
Result QualifiersRPDResult
L1682413-01
R4008317-2SAMPLE DUPLICATE:
pH Std. Units 7.77 0.6417.82
Parameter Units
Dup
Result QualifiersRPDResult
92700661001
R4008317-3SAMPLE DUPLICATE:
pH Std. Units 7.15 0.1407.16
REPORT OF LABORATORY ANALYSIS
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92700661
Rowan Street Site
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
WORKORDER QUALIFIERS
WO: 92700661
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012 B.[1]
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034-9030B.[1]
SAMPLE QUALIFIERS
Sample: 92700661001
Wet Chemistry by Method 9045D - 7.16 at 19.4C[1]
Sample: 92700661002
Volatile Petroleum Hydrocarbons by Method MADEPV - Surrogate failure due to matrix interference.[1]
Sample: R4008317-1
Wet Chemistry by Method 9045D - 10 at 20C[1]
Sample: R4008317-2
Wet Chemistry by Method 9045D - 7.77 at 19.6C[1]
Sample: R4008317-3
Wet Chemistry by Method 9045D - 7.15 at 19.5C[1]
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 44
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92700661
Rowan Street Site
SAMPLE QUALIFIERS
Sample: L1681882-01
Pesticides (GC) by Method 8081B - Duplicate analysis was performed. MS/MSD confirm matrix impacting surrogates.[1]
Sample: L1682413-01
Wet Chemistry by Method 9045D - 7.82 at 19.7C[1]
ANALYTE QUALIFIERS
The reported concentration is an estimate. The continuing calibration standard associated with this data responded low.
Data is likely to show a low bias concerning the result.C4
Analyte concentration exceeded the calibration range. The reported result is estimated.E
Sample was received or analysis requested beyond the recognized method holding time.H3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery and/or matrix spike duplicate recovery was above laboratory control limits. Result may be biased
high.MH
Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased
low.ML
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Matrix spike recovery was outside laboratory control limits due to a parent sample concentration notably higher than the
spike level.P6
RPD value was outside control limits.R1
Surrogate recovery not evaluated against control limits due to sample dilution.S4
Surrogate recovery was below laboratory control limits. Results may be biased low.SR
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
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9800 Kincey Ave. Suite 100
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Page 40 of 44
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92700661
Rowan Street Site
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92700661001 2183333 2183333SS-1 Comp MA DEP/NJ DEP MADEP EPH
92700661001 2182158 2182158SS-1 Comp 3510C EPA 8081B
92700661001 2181810 2181810SS-1 Comp 8151A EPA 8151A
92700661001 816538 816676SS-1 Comp EPA 3546 EPA 8015C
92700661001 2185766 2185766SS-1 Comp MADEPV MADEP VPH
92700661002 2185766 2185766SS-1 Grab MADEPV MADEP VPH
92700661001 2181818 2181818SS-1 Comp 3015 EPA 6010D
92700661001 2181544 2181544SS-1 Comp 7470A EPA 7470A
92700661001 816710 816990SS-1 Comp EPA 3546 EPA 8270E
92700661002 817181 817184SS-1 Grab EPA 5035A/5030B EPA 8260D
92700661001 816770SS-1 Comp SW-846
92700661002 816770SS-1 Grab SW-846
92700661001 2182050SS-1 Comp 1010B/ASTM D8175-18
92700661001 2181430 2181430SS-1 Comp SM 2540 G SM 2540G
92700661001 2180842 2180842SS-1 Comp 9012B EPA 9012B
92700661001 2182408 2182408SS-1 Comp 9030B EPA 9030B
92700661001 2180826 2180826SS-1 Comp 9045C/9045D EPA 9045D
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/12/2023 07:24 PM
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Page 41 of 44
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