FA-30226_00000_CA_IAR_20231106

East Coast Environmental, P.A.
3815 Junction Boulevard Raleigh, NC 27603
[phone]
Eastcoastenv.com

November 6, 2023

Mr. Ken Currie
NC-DEQ UST Section
Fayetteville Regional Office
Systel Building Suite 714
225 Green Street
Fayetteville, NC 28301

RE US #1 Food Mart
2210 US Highway 1
Marston, NC
NC-DEQ UST Section Facility I.D. # 00-0-0000018740

Dear Mr. Currie,

This correspondence is to present to you one copy of the attached Initial Abatement Actin Report for
your review.

Should you have any questions, comments, or require additional information, please feel free to contact
me at your earliest opportunity.

Cordially,
East Coast Environmental, P.A.
Tom Will
Project Manager

attachment

East Coast Environmental, P.A.
3815 Junction Boulevard Raleigh, NC 27603
[phone]
Eastcoastenv.com

INITIAL ABATEMENT ACTION REPORT

Prepared in Response to a Release of Gasoline
From an Underground Storage Tank

US #1 Food Mart
2210 US Highway 1
Maxton, NC
NC-DEQ UST Section Facility I.D. # 00-0-0000018740

Prepared For:
Eddie Falcocchia
P.O. Box 2603
Sarasota CA 95070
[phone]

Current Property Owner:
Eddie Falcocchia
P.O. Box 2603
Sarasota CA 95070
[phone]

Consultant:
East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, North Carolina 27603
[phone]

Issue Date: November 6, 2023

Thomas R. Will President
Release Discovery Date: October 16, 2023
UST Size and Content: (1) 2,000-Gallon Diesel Fuel, (2) 3,000-Gallon Gasoline, (1) 4,000 Gallon Gasoline
Latitude: N 34 58’ 36.73” Longitude: W 79 36’ 07.05”
Initial Abatement Action Report
US #1 Food Mart, 2210 US Highway 1, Maxton, Richmond County, NC
East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
2

TABLE OF CONTENTS
B SITE HISTORY AND CHARACTERIZATION .......................................................................................................................... 4
B.1 UST OWNER AND OPERATOR INFORMATION .................................................................................................................................. 4
B.2 UST INFORMATION ......................................................................................................................................................................... 4
B.3 NON-UST INFORMATION ................................................................................................................................................................ 4
B.4 RELEASE DESCRIPTION ................................................................................................................................................................... 4
B.5 SITE CHARACTERISTICS .................................................................................................................................................................. 5
B.6 SITE CHARACTERISTICS, SUMMARY OF INITIAL ABATEMENT ACTIONS, ASSESSMENT ACTIVITIES AND CORRECTIVE ACTIONS .... 6
C UST CLOSURE REPORT (UST-12) ............................................................................................................................................. 7
C.1 PREPARATIONS FOR UST CLOSURE ................................................................................................................................................ 7
C.2 UST RESIDUALS ............................................................................................................................................................................. 7
C.3 CLOSURE PROCEDURES .................................................................................................................................................................. 7
C4 FIELD SCREENING PROCEDURES AND OBSERVATIONS .................................................................................................................... 8
C.5 SOIL SAMPLING .............................................................................................................................................................................. 8
C.6 GROUNDWATER SAMPLING ............................................................................................................................................................ 8
C.7 QUALITY CONTROL MEASURES ...................................................................................................................................................... 9
C.8 INVESTIGATIVE RESULTS .............................................................................................................................................................. 10
C.8 UST CLOSURE CONCLUSIONS ...................................................................................................................................................... 10
D FREE PRODUCT INVESTIGATION AND RECOVERY REPORT ...................................................................................... 11
E INITIAL RESPONSE AND ABATEMENT ACTION ............................................................................................................... 11
F CONCLUSIONS ............................................................................................................................................................................ 11
G LIMITATIONS .............................................................................................................................................................................. 12

ATTACHMENTS
Appendix A

Figure 1 Topographic Site Location Map
Figure 2 Site Map With Former UST Locations
Photo Assay

Appendix B Table l UST Ownership Information
Table 2 Summary of Soil Sample Results
Table 3 Summary of Groundwater Sample Results

Appendix C Notice of Intent (GW/UST-3)/ Site Investigation Report (GW/UST-2) / Richmond
County UST Removal Permit / UST Disposal Certificate

Appendix D Laboratory Report

Initial Abatement Action Report
US #1 Food Mart, 2210 US Highway 1, Maxton, Richmond County, NC
East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
3

Initial Abatement Action Report
This Initial Abatement Action Report includes the following individual reports:
UST Closure Report (UST-12) with UST-2 Form
Post Excavation Soil Contamination Assessment Report
Free Product Recovery Report

A SITE INFORMATION

A.1 Site Identification
Date of Report: November 6, 2023
Facility I.D.: 00-0-0000018740 UST Incident Number: N/A
Site Name: US #1 Food Mart
Site Address: 4593 NC Highway 24
Nearest City/Town: Maxton County: Richmond
Latitude: N 35 58’ 36.73” Longitude: W 79 36’ 07.05”

A.2 Contact Information
UST Owner/Operator: Eddie Falcocchia
Address: P.O. Box 2603, Saratoga, CA 95070 Phone: [phone]

Property Owner: Eddie Falcocchia
Address: P.O. Box 2603, Saratoga, CA 95070 Phone: [phone]

Property Occupants: Vacant
Address: Phone:

Consultant/Contractor: East Coast Environmental, P.A.
Address: 3815 Junction Blvd., Raleigh, NC 27603 Phone: [phone]

Analytical Laboratory: Environmental Conservation Laboratories
Address: 102-A Woodwinds Industrial Court, Cary, NC 27511 Phone: [phone]

A.3 Release Information
Date Discovered: October 16, 2023
Estimated Quantity of Release: NA
Suspected Cause of UST Releases: Unknown
Source of Release (e.g., Piping/UST): Unknown
Size and content of UST system associated release: 4,000-gallon Gasoline

I, Thomas R. Will a Licensed Geologist for East Coast Environmental, P.A. do certify that the information contained in
this report is correct and accurate to the best of my knowledge.
East Coast Environmental, P.A. is licensed to practice geology in North Carolina. The certification number for East Coast
Environmental, P.A. is C-136

Initial Abatement Action Report
US #1 Food Mart, 2210 US Highway 1, Maxton, Richmond County, NC
East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
4

B SITE HISTORY AND CHARACTERIZATION

B.1 UST Owner and Operator Information

General information regarding Underground Storage Tank (UST) history and ownership is displayed in Table 1
in Section B.

B.2 UST Information

The subject USTs were constructed of single walled steel that had been upgraded by lining them internally with
epoxy and were registered with the North Carolina Department of Environmental Quality (NC-DEQ)
Underground Storage Tank (UST) Section. The NC-DEQ UST database reports that the Site contained (1) 2,000-
gallon steel diesel fuel UST, (2) 3,000-gallon gasoline USTs and (1) 4,000-gallon gasoline UST that were installed
during 1970. Product piping associated with the USTs was single walled flexible plastic hose, however these
were not the lines that were originally installed with the tanks in 1970. See Appendix A, Figure 2 for Site map
indicating former UST system locations.

General information for the USTs removed from the US #1 Food Mart (hereinafter referred to as the “Site”) is
based on historical information obtained from the NC-DEQ Registered UST Database and is displayed in Table
1 in Appendix B.

B.3 Non-UST Information

There were no petroleum Aboveground Storage Tanks (ASTs) noted near the USTs during the UST removal
activities.

B.4 Release Description

As stated previously the Site contained (1) 2,000-gallon steel diesel fuel, (2) 3,000-gallon gasoline and (1) 4,000-
gallon gasoline UST systems. All four tanks were closed during September 18-20, 2023 by NWD, LLC of
Zebulon, NC. All four tanks were constructed with single walled steel had been upgraded at some time by lining
them internally with epoxy. The product lines for the tanks were constructed of single walled flexible plastic
hose. See Figure 2 for tank and line locations. Upon removal and inspection, the USTs were found to be in fair
condition with pitting but no obvious holes noted.

During removal little petroleum staining or odors were noted in the soils around the tanks.

Initial Abatement Action Report
US #1 Food Mart, 2210 US Highway 1, Maxton, Richmond County, NC
East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
5
After removal, no over excavation of the UST pit was completed. All soils removed for excavation of the tanks
were later placed back into the excavation as backfill. See Figure 2 and photographs in Appendix A.

Thirteen tank closure soil samples (S-1 through S-13) were collected from the sides of the UST excavation at a
depth of approximately 5-feet below land surface because groundwater was observed entering the excavation
after the tanks were removed. Therefore, no soil samples were collected for closure from directly under the tanks
themselves

Four line and two dispenser samples (S-15 through S-20) were also collected as part of the UST system closure
activities. All four of these samples were collected from a depth of approximately 3-feet below land surface and
directly under this equipment. No petroleum contaminated soil was noted in these areas while collecting the
samples. See Figure 2 and photographs in Appendix A for soil sample and excavation locations.

The soil closure samples collected for closure of the gasoline UST systems were submitted for analysis by EPA
method 8015 for Gasoline Range Organics (GRO) while the soil samples collected for closure of the diesel fuel
UST system were also submitted for analysis by EPA method 8015 for Diesel Range Organics (DRO). Closure
samples were collected in order to comply with the North Carolina Department of Environment and Natural
Resources (NC-DENR) “Guidelines for Site Checks, Tank Closure and Initial Response and Abatement for UST
Releases March 1, 2007 Version, “Guidelines for Site Checks, Tank Closure and Initial Response and Abatement
for UST Releases May 17, 2021 Version, change 11 effective - 2021” (hereinafter referred to as “The Guidelines”).

B.5 Site Characteristics

The Site was last occupied by the US #1 Food Mart and is located at 2210 US Highway 1, Marston, Richmond
County North Carolina (Figure 1). The immediately surrounding properties are undeveloped or are being used
primarily for commercial purposes. The NC-DEQ database has no record of a previous petroleum release
associated with the Site.

The Site has an approximate elevation of 400-feet above mean sea level (MSL). Locally, surface runoff is
expected to exit the Site’s southern border adjacent to NC 177 through overland and man-made drainage features.
Locally, groundwater is expected to flow to the south as well.

The Geologic Map of North Carolina1 locates the Site as being underlain by the Pinehurst Formation of the Coastal
Plain Physiographic Province. Further, the Geologic Map describes the Pinehurst Formation as “Sand, medium
to coarse grained cross bedding and rhythmic bands of clayey sand common, unconsolidated”.

1 Reference Geologic Map of North Carolina, Department of Natural Resources and Community Development, Division of Land Resources, 1985
edition.
Initial Abatement Action Report
US #1 Food Mart, 2210 US Highway 1, Maxton, Richmond County, NC
East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
6

Observations made by ECE while removing the tanks reveal that the Site is underlain by dry orange, brown silt
sand to 8-feet below land surface. Below 8-feet a gray-white clay was encountered. Groundwater was observed
in the bottom of the UST excavation collecting on top of the white-gray clay which is likely acting as a confining
layer in the area.

No subsurface utilities, basements, or underground structures were observed or identified in the immediate area
around the UST system (Figure 2).

While a receptor survey was not completed as part of this investigation, ECE observed three residential properties
were observed within a 1,000-foot radius of the Site. Two well houses were observed at these locations, however
Richmond County water is also available for these homes. ECE attempted to gain information regarding whether
these residences were hooked up to the available county water supply, however no one came to their doors to
answer this question. One of the wells is approximately 975-feet northwest of the release area while the second
well is located approximately 870-feet north of the tanks. It should be noted that these homes are topographically
upgradient of the Site. Figure 3 is a receptor map showing well locations.

The Site itself is connected to the Richmond County municipal water supply.

B.6 Site Characteristics, Summary of Initial Abatement Actions, Assessment Activities and Corrective
Actions

In summary, the initial abatement actions completed for the UST systems include their closure by removal. The
Site contained (1) 2,000-gallon steel diesel fuel, (2) 3,000-gallon gasoline and (1) 4,000-gallon gasoline UST
systems. All four tanks were closed during September 18-20, 2023 by NWD, LLC of Zebulon, NC. All four
tanks were constructed with single walled steel that had been internally lined with epoxy. The product lines for
the tanks were constructed of single walled flexible plastic hose. See Figure 2 for tank and line locations and
photographs at the back of Appendix A. The tanks were later transported to K&L Scrap of Clayton, NC for
disposal.

Thirteen closure soil samples (S-1 through S-13) were collected from the sides of the UST excavation at a depth
of approximately 5-feet below land surface because groundwater was observed entering the excavation after the
tanks were removed. Therefore, no soil samples were collected for closure from directly under the tanks
themselves

Four line and two dispenser samples (S-15 through S-20) were also collected as part of the UST system closure
activities. All four of these samples were collected from a depth of approximately 3-feet below land surface and
Initial Abatement Action Report
US #1 Food Mart, 2210 US Highway 1, Maxton, Richmond County, NC
East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
7
directly under this equipment. No petroleum contaminated soil was noted in these areas while collecting the
samples. See Figure 2 and photographs in Appendix A for soil sample and excavation locations.

C UST CLOSURE REPORT (UST-12)

C.1 Preparations for UST Closure

A UST-3 (Notice if Intent) form was submitted to the NC-DEQ Central Office and NC-DEQ Fayetteville Regional
Office prior to beginning UST closure activities. A UST-2a (Site Investigation Report) has also been submitted
to the NC-DEQ Central Office and NC-DEQ Fayetteville Regional Office and included as part of this Initial
Abatement Action Report. Finally, a UST removal permit was obtained by the Richmond County Fire Marshalls
office prior to beginning UST Closure activities. See Appendix C for a copy of the UST-3, UST-2a and Fire
Marshal permit application form.

C.2 UST Residuals

After the USTs were uncovered, NWD, LLC of Zebulon removed a combined total of approximately 105-gallons
of gasoline, diesel fuel and water from the four USTs.

C.3 Closure Procedures

The UST closure activities were performed by NWD, LLC during September 18-20, 2023 utilizing an excavator.
After they were uncovered it was confirmed that the Site contained 1) 2,000-gallon steel diesel fuel UST, (2)
3,000-gallon gasoline USTs and (1) 4,000-gallon gasoline UST systems. See Figure 2 for tank and line locations.

The excavation made to close the four tanks measured up to approximately 35-feet in length by as much as 35-
feet in width by as much as 8-feet in depth. See Section A, Figure 2 for approximate final dimensions of the
UST excavations in relation to the Site.

After removal, no over excavation of the UST pit was completed. Further, all soils removed for excavation of
the tanks were later placed back into the excavation as backfill as they showed no visual or olfactory signs or
petroleum contamination. This observation was backed up by the result of stockpile sampling which is
summarized in Table 2 in Appendix B. See Figure 2 and photographs in Appendix A.

Initial Abatement Action Report
US #1 Food Mart, 2210 US Highway 1, Maxton, Richmond County, NC
East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
8
After removal, The USTs were found to be in fair condition with pitting, but no holes noted. The product lines
associated with the USTs were constructed of single walled flexible hose and appeared to be in excellent
condition.

C4 Field Screening Procedures and Observations

Field screening of soils consisted of their visual and olfactory profiling after the UST systems were removed from
the excavations.

C.5 Soil Sampling

Thirteen closure soil samples (S-1 through S-13) were collected from the sides of the UST excavation at a depth
of approximately 5-feet below land surface because groundwater was observed entering the excavation after the
tanks were removed. Therefore, no soil samples were collected for closure from directly under the tanks
themselves.

Four line and two dispenser samples (S-15 through S-20) were also collected as part of the UST system closure
activities. All four of these samples were collected from a depth of approximately 3-feet below land surface and
directly under this equipment. No petroleum contaminated soil was noted in these areas while collecting the
samples. See Figure 2 and photographs in Appendix A for soil sample and excavation locations.

The soil closure samples collected for closure of the gasoline UST systems were submitted for analysis by EPA
method 8015 for Gasoline Range Organics (GRO) while the soil samples collected for closure of the diesel fuel
UST system were also submitted for analysis by EPA method 8015 for Diesel Range Organics (DRO). Closure
samples were collected to comply with The Guidelines.

C.6 Groundwater Sampling

Because groundwater was observed entering the UST excavation, ECE personnel installed groundwater
monitoring well TMW-1 at the location shown in Figure 2. After the boring advanced for the installation of
temporary well TMW-1 was terminated it was completed as a temporary well by installing 10-feet of 2-inch
diameter well screen which was topped with 5-feet of 2-inch solid riser pipe. Groundwater was found to
accumulate in the well at an approximate depth of 8-feet below land surface.

Next, TMW-1 was then developed for approximately two hours after which groundwater samples were collected
for laboratory analysis by EPA Method 8260D (Volatile Organic Compounds), EPA Method 625 (Base Neutral
Extractables), MADEP-VPH/EPH and total lead by EPA Method 6010b
Initial Abatement Action Report
US #1 Food Mart, 2210 US Highway 1, Maxton, Richmond County, NC
East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
9
C.7 Quality Control Measures

The soil and groundwater samples collected for laboratory analysis were handled only with clean nitrile gloves
and immediately placed, with minimal or no head space, into a pre-cleaned borosilicate bottles supplied by the
analytical laboratory. After the samples were secured in the bottles, they were placed in a cooler with ice and
transported to ECE’s office location, where they were stored in a refrigerator pending transport via courier to
Eurofins Southeast Laboratories, Inc. location in Cary, NC (NC-DEQ laboratory certification # 591).

Next, a chain of custody form was completed and transported by the laboratory’s courier service with the samples
for chemical analysis to ENCO’s Cary, NC facility.

The chain of custody form included the following items:
-Sample identification.
-Signature of the sample collector, transporter, and laboratory person receiving the sample.
-Inclusive dates of sample collection.
-Date and time of sample collection.
-Number of containers.
-Requested parameters.
-Laboratory number.

Specific information related to the samples collected, including date and time of collection, is found on the Chain
of Custody documentation in Appendix D of this report.

All nitrile gloves used by ECE personnel during UST closure activities were properly discarded, along with any
other potentially contaminated articles, immediately after their use.

ECE followed standard EPA and NC-DEQ protocols and guidelines for collecting soil and groundwater samples.
It is ECE's belief that the laboratory analytical results provided in this report should not have been adversely
affected by our sampling, handling and shipment procedures.

Initial Abatement Action Report
US #1 Food Mart, 2210 US Highway 1, Maxton, Richmond County, NC
East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
10

C.8 Investigative Results

Soil Sample Analytical Results

The results for the soil closure samples collected from under the USTs and associated product dispensers were all
below the action levels of 50-mg/kg for GRO with the exception of sample S-13 which was found to contain GRO
at a level of 8,700-mg/kg. Further, the samples submitted for DRO analysis were all below 100-mg/kg of DRO
except for soil sample S-2 and S-3 that were found to contain DRO at concentrations of 170 and 140-mg/kg,
respectively.

Groundwater Analytical Results

Groundwater samples obtained from groundwater monitoring well TMW-1 on September 20, 2023 and analyzed
by EPA Methods 6200b and 625 revealed numerous targeted contaminants at concentrations more than their
maximum allowable levels in groundwater as set forth in 15A NCAC 2L .0202. However, none were detected at
concentrations in excess of their Gross Contaminant Levels (GCLs).

Groundwater samples obtained from groundwater monitoring well MW-1 and analyzed by EPA Method 6010d
for total lead showed no lead at a level in excess of the method detection limits.

Data for the MADEP-VPH/EPH analyses showed C5-C8 aliphatics, C9-C18 aliphatics C9-C22 aromatic
hydrocarbons in the groundwater sample collected from TMW-1. Further, all of these detections were found at
levels in excess of their maximum allowable concentrations in groundwater as set forth in 15A NCAC 2L .0202.

Appendix II, Table 3 is a summary of analytical results for groundwater while the laboratory analytical report is
included in Appendix D.

C.8 UST Closure Conclusions

ECE has reviewed the information obtained after the closure of four UST systems at the subject Site. Based on
ECE's Site observations and the laboratory results of the soil and groundwater samples submitted for analysis, it
can be concluded that one or more petroleum releases has occurred from the UST systems. During removal no
obvious signs of soil impacts including stained soils or obvious petroleum odors were noted in the soils removed
for closure of the tanks or sidewalls of the excavation. However, the groundwater retrieved from TMW-1 did
show olfactory signs of petroleum impact while the well was being developed.

Initial Abatement Action Report
US #1 Food Mart, 2210 US Highway 1, Maxton, Richmond County, NC
East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
11

D FREE PRODUCT INVESTIGATION AND RECOVERY REPORT

No free phase petroleum product was observed entering the excavation or temporary well TMW-1 while
completing the UST closure activities. Further, based on ECE’s observation made at the time of UST closure and
the analytical results for the closure free product would not be expected to be found in the subsurface of the Site.

E INITIAL RESPONSE AND ABATEMENT ACTION

UST closure activities were conducted during September 18-20, 2023 and included the removal and disposal of
approximately 105-gallons of liquids followed by removing the tanks from the ground. No petroleum
contaminated soils were noted, staged or hauled offsite as part of the UST closure activities.

F CONCLUSIONS

As stated previously the Site contained (1) 2,000-gallon steel diesel fuel UST, (2) 3,000-gallon gasoline USTs
and (1) 4,000-gallon gasoline UST systems that were closed by removal during September 18-20, 2023. Based
on ECE's Site observations and the laboratory results of groundwater samples submitted for analysis, it can be
concluded that one or more petroleum releases has occurred from the UST systems at some time since they were
installed during 1970.

This statement is supported by the results for the soil closure samples collected from under the USTs and
associated product dispensers were all below the action levels of 50-mg/kg for GRO with the exception of sample
S-13 which was found to contain GRO at a level of 8,700-mg/kg. Further, the samples submitted for DRO
analysis were all below 100-mg/kg of DRO except for soil sample S-2 and S-3 that were found to contain DRO
at concentrations of 170 and 140-mg/kg, respectively.

Groundwater samples obtained from groundwater monitoring well TMW-1 on September 20, 2023 and analyzed
by EPA Methods 6200b, 625 and the MADEP-VPH/EPH analyses revealed numerous targeted contaminants at
concentrations more than their maximum allowable levels in groundwater as set forth in 15A NCAC 2L .0202.
However, none were detected at concentrations in excess of their Gross Contaminant Levels (GCLs).

Initial Abatement Action Report
US #1 Food Mart, 2210 US Highway 1, Maxton, Richmond County, NC
East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
12

A copy of this Initial Abatement Action Report should be forwarded to the NC-DEQ-DWM, Fayetteville Regional
Office to the attention of Ken Currie. This UST closure report will satisfy the sampling and reporting
requirements of the Initial Abatement Action Report.

G LIMITATIONS

This report has been prepared for the exclusive use of Eddie Falcocchia, his successors, assigns or designees.
This study was conducted in accordance with generally accepted environmental practices. No other warranty,
expressed or implied, is made. ECE's conclusions and recommendations are based on information supplied by
others, together with ECE's own site observations. Although ECE cannot be responsible for the accuracy of data
supplied by others, ECE has no reason to suspect that any of the information is inaccurate. The observations
described herein are based upon conditions readily visible at the site at the time of ECE's visit, in addition to
information provided by the Client.

ECE, by virtue of providing the services indicated in this report, does not assume responsibility for the person(s)
in charge of the site, nor is ECE responsible for reporting to any local, state or federal public agencies any
conditions at the Site that may present a potential danger to public health, safety or the environment. It is the
responsibility of the owner to notify the appropriate local, state or federal public agencies as required by law, or
otherwise to disclose, in a timely manner, any information that may be necessary to prevent any danger to public
health, safety or the environment.

Initial Abatement Action Report
US #1 Food Mart, 2210 US Highway 1, Maxton, Richmond County, NC
East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
13

Appendix A

Figures
Photographs

East Coast
Environmental, P.A.
3815 Junction Boulevard
Raleigh, North Carolina 27603
[phone]
Figure 1
Site Location Map
US #1 Food Mart
2210 US Highway 1
Marston, Richmond, NC
Scale:Prep. By:Rev. By:Date:
NTS TRW TRW 10/4/2023
N
Source: USGS Marston NC Quadrangle 2022
Site location
East Coast
Environmental, P.A.
3815 Junction Boulevard
Raleigh, North Carolina 27603
[phone]
Figure 2
Site Map With Closure Sample
Locations
US #1 Food Mart
2210 US 1 N
Marston, Richmond County, NC
Scale:Prep. By:Rev. By:Date:
1” = 20'TRW TRW 10/6/2023
N
N C 177T-2
Extent of UST System Excavation.
S-1
Temporary Monitoring
well TMW-1
S-4
S-3
S-5
S-6
S-8 S-7
S-15
- Soil Sample Locations
Product Dispensers
T-4
T-1
T-3
S-20
S-18
S-16
S-9 S-10
S-11
S-13
S-12
S-2
US 1 Food Mart
S-17
S-19
East Coast
Environmental, P.A.
3815 Junction Boulevard
Raleigh, North Carolina 27603
[phone]
Figure 1
Receptor Map
US #1 Food Mart
2210 US Highway 1
Marston, Richmond, NC
Scale:Prep. By:Rev. By:Date:
NTS TRW TRW 10/4/2023
N
- Water Supply Well House
1,000-Foot Radius Site location
US #1 Food Mart
2210 US Highway 1, Marston North Carolina
1. View of Tanks T-3 and T-4 Prior to Removal 2. View of All Tanks Uncovered Prior to Removal
3. View of All USTs Prior to Removal 4. View of Tank T-1 Prior to Removal
5. View of Excavation After Removal of T-4 6. View of Excavation After all Tanks Were Removed
Initial Abatement Action Report
US #1 Food Mart, 2210 US Highway 1, Maxton, Richmond County, NC
East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
14

Appendix B

Tables

Table 1
Site History – UST Owner and Operator Information
US #1 Food Mart
2210 US 1 N
Marston, NC

Facility ID Number

Name of Registered Owner /Operator Dates of Ownership
(mm/dd/yy to mm/dd/yy)

0-0000018740
US #1 Food Mart
6/2019 - 2023
Name of Property Owner

Dates of Operation
(mm/dd/yy to mm/dd/yy)
Eddie Falcocchia
P.O. Box 2503
Saratoga CA 95070
[phone]

1970 – Pre 2000
Street Address
2210 US Highway 1
City State Zip Telephone Number
Marston NC 28363 N/A

Table 1 (continued)
US 1 Food Mart
2210 US 1 N
Marston, NC
UST
ID #
Last
Contents
Previous
Contents
Capacity
(gallons)
Construction
Details
Tank
Dimensions
Descriptions
of Associated
Piping
Date Tank
Installed
Status of
UST
Was release
associated
with UST
T-1 Gasoline Gasoline 4,000

Single Walled
Steel with
internal epoxy
liner
5’ x 24’ Single Walled
Flexible Plastic
Piping
5/12/1970 Removed
9/2023
No
T-2 Gasoline Gasoline 3,000 Single Walled
Steel with
internal epoxy
liner
5’ x 18’ Single Walled
Flexible Plastic
Piping
5/12/1970 Removed
9/2023
No
T-3

Gasoline Gasoline 3,000 Single Walled
Steel with
internal epoxy
liner
5’ x 18’ Single Walled
Flexible Plastic
Piping
5/12/1970 Removed
9/2023
No
T-4 Diesel
Fuel
Diesel Fuel 2,000 Single Walled
Steel with
internal epoxy
liner
5’ x 12’ Single Walled
Flexible Plastic
Piping
5/12/1970 Removed
9/2023
Yes

Table 1 (continued)
US 1 Food Mart
2210 US 1 N
Marston, NC
Incident
Number
Material
Released
Date of
Release Description of Release
N/A N/A N/A No Known Previous Release at the Site

Table 2
Summary of Analytical Data – Soil
US #1 Food Mart
2210 US 1 N
Marston, NC
Analytical Method >

EPA 8015 w/5030 EPA 8015 w/5030
Sample
ID
Contaminant of Concern > Low Boiling Point TPH (GRO) High Boiling Point TPH (DRO) Date Collected
(m/dd/yy)
Sample Depth (ft)
S-1 9/20/2023 5’ ND 5.2
S-2 9/20/2023 5’ 15 170
S-3 9/20/2023 5’ ND 140
S-4 9/20/2023 5’ ND ND
S-5 9/20/2023 5’ ND NT
S-6 9/20/2023 5’ ND NT
S-7 9/20/2023 5’ ND NT
S-8 9/20/2023 5’ ND NT
S-9 9/20/2023 5’ ND NT
S-10 9/20/2023 5’ ND NT
S-11 9/20/2023 5’ ND NT
S-12 9/20/2023 5’ ND NT
S-13 9/20/2023 5’ 8,700 NT
S-14 9/20/2023 5’ ND NT
S-15 9/20/2023 5’ ND NT
S-16 9/20/2023 5’ ND NT
S-17 9/20/2023 3’ ND NT
S-18 9/20/2023 3’ ND NT
S-19 9/20/2023 3’ ND NT
S-20 9/20/2023 3’ 4.6J NT
NC-DEQ Action Level 50 100

Results are in mg/kg
ND - Not Detected
NT – Not Tested
J - Estimated Concentration

Table 3
Summary of Analytical Data – Groundwater
US #1 Food Mart
2210 US 1 N
Marston, NC

Analytical Method >

6200b 6200b 6200b 6200b 6200b 6200b 6200b 6200b 6200b 6300B
Well
ID
Contaminant of
Concern > Benzene Toluene Ethylbenzene Naphthalene 1,2,4 Trimethylbenzene 1,3,5 Trimethylbenzene Total Xylenes N-propyl-benzene Isopropyl-benzene Methylene Chloride Date
Collected
m/dd/yy
Sample
ID
TW-1 9/20/2023 TW-1 3,600 29,000 7,000 3,500 16,000 4,200 37,000 2,000 480J 180J
- - - - - - - - - - - -
2L Standard (ug/l) 1 600 600 6 400 400 500 70 70 5
GCL (ug/l) 5,000 26000 84,500 6,000 28500 25000 87,500 26,100 30,500 5,000
Results are in ug/l
Bold results indicate exceedence of 2L Standards
Bold and shaded results indicate exceedence of GCL

ND – Non Detect
NT – Not Tested

Table 3
Summary of Analytical Data – Groundwater
US #1 Food Mart
2210 US 1 N
Marston, NC

Analytical Method >

625 625 625 625 625 625 625 MADEP
VPH
MADEP
VPH/EPH
MADEP
EPH
MADEP
VPH/EPH
Well
ID
Contaminant of
Concern > 1,4-Dichlorobenzene Anthracene Fluoroanthene Fluorene Phenanthrene Pyrene Naphthelene C5-C8 Aliphatics C9-C18 Aliphatics C19-C36 Aliphatics C9-C22 Aromatics Date
Collected
m/dd/yy
Sample
ID
TW-1 9/20/2023 TW-1 14 10 5.4J 21J 36 15 4,400 4,200 22,400 8.7 32,051
- - - - - - - - - - - - - -
2L Standard (ug/l) 20 2,000 300 300 200 200 6 400 700 10,000 200
GCL (ug/l) 20,000 2,000 300 845 550 200 6,000 NRS NRS NRS NRS
Results are in ug/l
Bold results indicate exceedence of 2L Standards
Bold and shaded results indicate exceedence of GCL

ND – Non Detect
NT – Not Tested

Initial Abatement Action Report
US #1 Food Mart, 2210 US Highway 1, Maxton, Richmond County, NC
East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
15

Appendix C

Notice of Intent (GW/UST-3)
Site Investigation Report (GW/UST-2)
Richmond County UST Removal Permit
UST Disposal Certificate

UST-61 24-Hour Release and UST Leak Reporting Form.
For Releases
in NC
This form should be completed and submitted to the UST Section’s regional office following a known or suspected release from an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or
suspected release
(DWM USE ONLY) Incident # ________ Risk (H,I,L,U)_______ Received On ________ Received By ________ Reported by (circle one): Phone, Fax or Report Region _______
Suspected Contamination ? (Y/N) _Y______ Confirmed GW Contamination ? (Y/N) _Y___ Confirmed Soil Contamination ?(Y/N) _Y___
Samples Taken?(Y/N) __Y___ Free Product? (Y/N) ___N__ If Yes, State Greatest Thickness ______________
Facility ID Number _0-0000018740
Date Leak Discovered _9-20-2023 _
Comm/Non -Commercial? Com Reg/
Non-regulated ? _ Reg_
INCIDENT DESCRIPTION
Incident Name: US #1 Food Mart
Address: 2210 US Highway 1 County: Richmond
City/Town: Maxton Zip Code: 27306 Regional Office (circle one): Asheville, Mooresville, Fayetteville, Raleigh, Washington, Wilmington, Winston-Salem
Latitude (decimal degrees): N 34.97676 Longitude (decimal degrees) : W 79.60195 Obtained by:
Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount
of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors)  GPS
 Topographic map
X GIS Address matching
 Other
 Unknown
Describe location:

HOW RELEASE WAS DISCOVERED (Release Code)
(Check one)
Release Detection Equipment or Methods
X During UST Closure/Removal Phase II ESA for Property

Transfer

Visual /Odor
 Water in Tank
 Water Supply Well Contamination

SX oil Contamination
X Groundwater Contamination
 Surface Water Contamination
 Other (specify) ___________

SOURCE OF CONTAMINATION
Source of Release (Check primary source) Cause of Release (Check primary cause) Type of Release (Check one) Product Type Released (Check primary product type released)

X Tank
 Piping
Dispenser
 Submersible Turbine Pump
 Delivery Problem
 Spill Bucket
 Other
Unknown
Definitions presented on reverse

 Spill
Overfill
Corrosion
 Physical/Mechanical Damage
 Install Problem
 Other
X Unknown
Definitions presented on reverse

PetroleumX
 Non-petroleum
 Both
Location (Check one)
X Facility
Residence

Other

X Gasoline / Diesel/

Kerosene
Heating Oil
 Other Petroleum
Products
 Metals
 Other Inorganics
 Other Organics

 Diesel/Veg. Oil
Blend
 Vegetable Oil 100%
 E10 – E20
 E21 – E84
 E85 – E99
 Ethanol 100%
 E01 – E09
Ownership
1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State Operation Type 1. Public Service 2. Agricultural 3. Residential 4. Education /Relig. 5. Industrial
6.

Commercial

7.

Mining

UST Form 61 (02/19) Page 1 of 2

il

(1) 4 ,000-gas, (2) 3,000-gas and (1) 2,000-diesel USTs were removed during September 18-20, 2023 . Soil
sample

collected from tank pit side wall

showed GRO at 1,800 mg/kg. Groundwater samples collected
from

from a temporary well adjacent to the tank pit was found to contain numerous petroleum related compounds

IMPACT ON DRINKING WATER SUPPLIES

Water Supply Wells Affected? 1. Yes 2. No 3. Unknown
Number of Water Supply Wells Affected __________________
Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary) 1. 2. 3.
UST SYSTEM OWNER UST Owner/Company:Eddie Falcocchia
Point of Contact: Eddie Falcocchia Address: P.O. Box 2603
City: Saratoga State: NC Zip Code: 95070 Telephone Number
UST SYSTEM OPERATOR
UST Operator/Company: None Address:
City: State: Zip Code: Telephone Number
LANDOWNER AT LOCATION OF UST INCIDENT
Landowner: Eddie Falcocchia Address: P.O. Box 2603
City: Saratoga State: NC Zip Code: 95070 Telephone Number
Draw Sketch of Area (showing two major road intersections) or Attach Map
Person Reporting Incident Tom Will Company East Coast Environmental, PA Telephone Number 919-772-0268
Title Geologist Address 3815 Junction Boulevard, Raleigh, NC 27603 Date 10-18-23
UST Form 61 (02/19) Page 2 of 2
Definitions of Sources Tank: means the tank that stores the product and is part of the underground storage tank system Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end-use equipment (Vent, vapor recovery, or fill lines are excluded.) Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above the shear valve) Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that connects the submersible turbine pump to the tank Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.)
Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor recovery lines, and fill lines) Unknown: identifies releases for which the source has not been determined Definitions of Causes
Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser) Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser) Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken components, and components that have changed dimension) Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust) Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells) Unknown: use when the cause has not been determined

[phone]
[phone]

Richmond County Building Inspection Department
221 South Hancock St
Rockingham, NC 28379
[e-mail]
Telephone: [phone] Fax: [phone]
MISCELLANEOUS PERMIT APPLICATION
Owner/Project Name: ______________________________________________________
Owner/Project Address_____________________________________________________
Phone Number: ______________________________________
Email:____________________________________________
Type of work to be done: _____________________________________________________________
[_] Demolition [_] Signs (if lighted add for Electrical)[_] Fire Sprinkler Systems (per riser)
[_] Tanks (add for Electrical)[_] Day Care License Inspections [_] ABC License Inspection
[_] Accessory Structures (decks, retaining walls, etc.)[_] Other: ______________________
Project Cost: ___________
Contractor: ____________________________________________________________________
Address: ______________________________________________________________________________
Phone #: ____________________________Email: ________________________________
State License #: ______________________
I hereby certify that the above statements are true, and all work is being performed under the State License number above.
Contractor’s Signature: _______________________________Date: ______________________
Applicant’s Signature: _________________________________Date: ______________________
Permits expire after 6 months of issuance if work has not commenced or if work has discontinued for
a period of 12 months from last inspection.
Initial Abatement Action Report
US #1 Food Mart, 2210 US Highway 1, Maxton, Richmond County, NC
East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
16

Appendix D

Laboratory Report

ANALYTICAL REPORT
PREPARED FOR
Attn: Tom Will
East Coast Environmental
3815 Junction Blvd
Raleigh, North Carolina 27603
Generated 10/9/2023 5:31:29 PM
JOB DESCRIPTION
2210 US 1
JOB NUMBER
752-11855-1
See page two for job notes and contact information.
Cary NC 27511
102-A Woodwinds Industrial Court
Eurofins Raleigh
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Eurofins Raleigh
Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project
Manager.
Authorization
Generated
10/9/2023 5:31:29 PM
Authorized for release by
John Andros, Project Manager I
[e-mail]
[phone]
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Table of Contents
Client: East Coast Environmental
Project/Site: 2210 US 1
Laboratory Job ID: 752-11855-1
Page 3 of 77 Eurofins Raleigh10/9/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .32
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .35
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .53
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .57
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .65
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .66
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .67
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .68
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .75
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Definitions/Glossary
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Qualifiers
GC/MS VOA
Qualifier Description
B Compound was found in the blank and sample.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
GC/MS Semi VOA
Qualifier Description
*-LCS and/or LCSD is outside acceptance limits, low biased.
Qualifier
*1 LCS/LCSD RPD exceeds control limits.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
GC VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
GC Semi VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
S1-Surrogate recovery exceeds control limits, low biased.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Raleigh
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Case Narrative
Client: East Coast Environmental Job ID: 752-11855-1
Project/Site: 2210 US 1
Job ID: 752-11855-1
Laboratory: Eurofins Raleigh
Narrative
Job Narrative
752-11855-1
Receipt
The samples were received on 9/22/2023 12:36 PM. Unless otherwise noted below, the samples arrived in good condition, and, where
required, properly preserved and on ice. The temperature of the cooler at receipt time was 2.1°C
GC/MS VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC/MS Semi VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Gasoline Range Organics
Method 8015C_GRO: The following MeOH terra core vial has very little MeOH: S-7 (752-11855-7)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Hydrocarbons
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Diesel Range Organics
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Hydrocarbons
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
General Chemistry
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Eurofins RaleighPage 5 of 77 10/9/2023
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Detection Summary
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Client Sample ID: S-1 Lab Sample ID: 752-11855-1
☼Diesel Range Organics [C10-C28]
RL
9.1 mg/Kg
MDL
3.0
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J5.2 8015C
Client Sample ID: S-2 Lab Sample ID: 752-11855-2
☼Gasoline Range Organics
(GRO)-C6-C10
RL
11 mg/Kg
MDL
2.6
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA100158015C
☼Diesel Range Organics [C10-C28]8.8 mg/Kg2.8 Total/NA11708015C
Client Sample ID: S-3 Lab Sample ID: 752-11855-3
☼Diesel Range Organics [C10-C28]
RL
8.3 mg/Kg
MDL
2.7
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11408015C
Client Sample ID: S-4 Lab Sample ID: 752-11855-4
No Detections.
Client Sample ID: S-5 Lab Sample ID: 752-11855-5
No Detections.
Client Sample ID: S-6 Lab Sample ID: 752-11855-6
No Detections.
Client Sample ID: S-7 Lab Sample ID: 752-11855-7
No Detections.
Client Sample ID: S-8 Lab Sample ID: 752-11855-8
No Detections.
Client Sample ID: S-9 Lab Sample ID: 752-11855-9
No Detections.
Client Sample ID: S-10 Lab Sample ID: 752-11855-10
No Detections.
Client Sample ID: S-11 Lab Sample ID: 752-11855-11
No Detections.
Client Sample ID: S-12 Lab Sample ID: 752-11855-12
No Detections.
Client Sample ID: S-13 Lab Sample ID: 752-11855-13
☼Gasoline Range Organics
(GRO)-C6-C10
RL
2100 mg/Kg
MDL
540
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA2000087008015C
Client Sample ID: S-14 Lab Sample ID: 752-11855-14
No Detections.
Eurofins Raleigh
This Detection Summary does not include radiochemical test results.
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Detection Summary
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Client Sample ID: S-15 Lab Sample ID: 752-11855-15
No Detections.
Client Sample ID: S-16 Lab Sample ID: 752-11855-16
No Detections.
Client Sample ID: S-17 Lab Sample ID: 752-11855-17
No Detections.
Client Sample ID: S-18 Lab Sample ID: 752-11855-18
No Detections.
Client Sample ID: S-19 Lab Sample ID: 752-11855-19
No Detections.
Client Sample ID: S-20 Lab Sample ID: 752-11855-20
☼Gasoline Range Organics
(GRO)-C6-C10
RL
14 mg/Kg
MDL
3.4
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA100J4.6 8015C
Client Sample ID: TMW-1 Lab Sample ID: 752-11855-21
1,2,4-Trimethylbenzene
RL
1000 ug/L
MDL
67
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA100016000SM6200-B
1,3,5-Trimethylbenzene 1000 ug/L100 Total/NA10004200SM6200-B
Benzene 1000 ug/L50 Total/NA10003600SM6200-B
Ethylbenzene 1000 ug/L100 Total/NA10007000SM6200-B
Isopropylbenzene 1000 ug/L130 Total/NA1000480JSM6200-B
m,p-Xylenes 2000 ug/L180 Total/NA100025000SM6200-B
Methylene Chloride 2000 ug/L70 Total/NA1000180J B SM6200-B
Naphthalene 1000 ug/L86 Total/NA10003500SM6200-B
N-Propylbenzene 1000 ug/L73 Total/NA10002000SM6200-B
o-Xylene 1000 ug/L88 Total/NA100012000SM6200-B
Toluene 1000 ug/L53 Total/NA100029000SM6200-B
Xylenes, Total 1000 ug/L220 Total/NA100037000SM6200-B
1,4-Dichlorobenzene 9.0 ug/L3.0 Total/NA114625.1
Anthracene 9.0 ug/L3.2 Total/NA110625.1
Fluoranthene 9.0 ug/L1.4 Total/NA15.4 J 625.1
Fluorene 9.0 ug/L3.1 Total/NA121*-625.1
Phenanthrene 9.0 ug/L3.9 Total/NA136625.1
Pyrene 9.0 ug/L3.3 Total/NA115625.1
Naphthalene - DL 450 ug/L160 Total/NA504400625.1
C5-C8 Aliphatics 13000 ug/L13000 Total/NA50042000MAVPH
C9-C12 Aliphatics 5500 ug/L5500 Total/NA50022000MAVPH
C9-C10 Aromatics 3500 ug/L3500 Total/NA50032000MAVPH
C9-C18 Aliphatics 0.73 mg/L0.73 Total/NA5140MA-EPH
C19-C36 Aliphatics 0.15 mg/L0.15 Total/NA18.7 MA-EPH
C11-C22 Aromatics 0.30 mg/L0.30 Total/NA151MA-EPH
Eurofins Raleigh
This Detection Summary does not include radiochemical test results.
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-1Client Sample ID: S-1
Matrix: SoilDate Collected: 09/20/23 10:30
Percent Solids: 86.5Date Received: 09/22/23 12:36
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
RL MDL
ND 14 3.6 mg/Kg ☼09/26/23 10:23 09/26/23 16:09 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics
(GRO)-C6-C10
a,a,a-Trifluorotoluene 88 70-131 09/26/23 10:23 09/26/23 16:09 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
RL MDL
5.2 J 9.1 3.0 mg/Kg ☼09/25/23 17:58 09/26/23 20:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl (Surr)79 15-139 09/25/23 17:58 09/26/23 20:05 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins Raleigh
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-2Client Sample ID: S-2
Matrix: SoilDate Collected: 09/20/23 10:35
Percent Solids: 90.4Date Received: 09/22/23 12:36
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
RL MDL
15 11 2.6 mg/Kg ☼09/26/23 10:23 10/03/23 23:53 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics
(GRO)-C6-C10
a,a,a-Trifluorotoluene 87 70-131 09/26/23 10:23 10/03/23 23:53 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
RL MDL
170 8.8 2.8 mg/Kg ☼09/25/23 17:58 09/26/23 20:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl (Surr)97 15-139 09/25/23 17:58 09/26/23 20:24 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins Raleigh
Page 9 of 77 10/9/2023
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-3Client Sample ID: S-3
Matrix: SoilDate Collected: 09/20/23 10:40
Percent Solids: 94.3Date Received: 09/22/23 12:36
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
RL MDL
ND 9.6 2.4 mg/Kg ☼09/26/23 10:23 09/26/23 16:52 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics
(GRO)-C6-C10
a,a,a-Trifluorotoluene 82 70-131 09/26/23 10:23 09/26/23 16:52 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
RL MDL
140 8.3 2.7 mg/Kg ☼09/25/23 17:58 09/26/23 20:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl (Surr)110 15-139 09/25/23 17:58 09/26/23 20:43 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins Raleigh
Page 10 of 77 10/9/2023
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-4Client Sample ID: S-4
Matrix: SoilDate Collected: 09/20/23 10:45
Percent Solids: 86.9Date Received: 09/22/23 12:36
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
RL MDL
ND 16 4.0 mg/Kg ☼09/26/23 10:23 09/26/23 17:13 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics
(GRO)-C6-C10
a,a,a-Trifluorotoluene 86 70-131 09/26/23 10:23 09/26/23 17:13 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
RL MDL
ND 9.0 2.9 mg/Kg ☼09/25/23 17:58 09/26/23 21:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl (Surr)75 15-139 09/25/23 17:58 09/26/23 21:01 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins Raleigh
Page 11 of 77 10/9/2023
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-5Client Sample ID: S-5
Matrix: SoilDate Collected: 09/20/23 10:50
Percent Solids: 88.6Date Received: 09/22/23 12:36
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
RL MDL
ND 11 2.7 mg/Kg ☼09/26/23 10:23 09/26/23 17:34 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics
(GRO)-C6-C10
a,a,a-Trifluorotoluene 84 70-131 09/26/23 10:23 09/26/23 17:34 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins Raleigh
Page 12 of 77 10/9/2023
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-6Client Sample ID: S-6
Matrix: SoilDate Collected: 09/20/23 10:55
Percent Solids: 93.0Date Received: 09/22/23 12:36
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
RL MDL
ND 9.9 2.5 mg/Kg ☼09/26/23 10:23 09/26/23 17:56 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics
(GRO)-C6-C10
a,a,a-Trifluorotoluene 84 70-131 09/26/23 10:23 09/26/23 17:56 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins Raleigh
Page 13 of 77 10/9/2023
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-7Client Sample ID: S-7
Matrix: SoilDate Collected: 09/20/23 11:00
Percent Solids: 95.0Date Received: 09/22/23 12:36
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
RL MDL
ND 17 4.3 mg/Kg ☼09/26/23 10:23 09/26/23 18:17 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics
(GRO)-C6-C10
a,a,a-Trifluorotoluene 85 70-131 09/26/23 10:23 09/26/23 18:17 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins Raleigh
Page 14 of 77 10/9/2023
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-8Client Sample ID: S-8
Matrix: SoilDate Collected: 09/20/23 11:05
Percent Solids: 78.4Date Received: 09/22/23 12:36
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
RL MDL
ND 14 3.4 mg/Kg ☼09/26/23 10:23 09/26/23 18:39 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics
(GRO)-C6-C10
a,a,a-Trifluorotoluene 82 70-131 09/26/23 10:23 09/26/23 18:39 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins Raleigh
Page 15 of 77 10/9/2023
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-9Client Sample ID: S-9
Matrix: SoilDate Collected: 09/20/23 11:10
Percent Solids: 94.3Date Received: 09/22/23 12:36
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
RL MDL
ND 10 2.5 mg/Kg ☼09/26/23 10:23 09/26/23 19:00 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics
(GRO)-C6-C10
a,a,a-Trifluorotoluene 84 70-131 09/26/23 10:23 09/26/23 19:00 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins Raleigh
Page 16 of 77 10/9/2023
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-10Client Sample ID: S-10
Matrix: SoilDate Collected: 09/20/23 11:15
Percent Solids: 94.0Date Received: 09/22/23 12:36
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
RL MDL
ND 9.5 2.4 mg/Kg ☼09/26/23 10:23 09/26/23 19:22 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics
(GRO)-C6-C10
a,a,a-Trifluorotoluene 84 70-131 09/26/23 10:23 09/26/23 19:22 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins Raleigh
Page 17 of 77 10/9/2023
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-11Client Sample ID: S-11
Matrix: SoilDate Collected: 09/20/23 11:20
Percent Solids: 83.3Date Received: 09/22/23 12:36
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
RL MDL
ND 14 3.5 mg/Kg ☼09/26/23 10:23 09/26/23 19:43 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics
(GRO)-C6-C10
a,a,a-Trifluorotoluene 84 70-131 09/26/23 10:23 09/26/23 19:43 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins Raleigh
Page 18 of 77 10/9/2023
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-12Client Sample ID: S-12
Matrix: SoilDate Collected: 09/20/23 11:25
Percent Solids: 81.5Date Received: 09/22/23 12:36
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
RL MDL
ND 11 2.7 mg/Kg ☼09/26/23 10:23 09/26/23 20:05 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics
(GRO)-C6-C10
a,a,a-Trifluorotoluene 85 70-131 09/26/23 10:23 09/26/23 20:05 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins Raleigh
Page 19 of 77 10/9/2023
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-13Client Sample ID: S-13
Matrix: SoilDate Collected: 09/20/23 11:30
Percent Solids: 92.6Date Received: 09/22/23 12:36
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
RL MDL
8700 2100 540 mg/Kg ☼09/26/23 10:23 09/27/23 17:02 20000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics
(GRO)-C6-C10
a,a,a-Trifluorotoluene 93 70-131 09/26/23 10:23 09/27/23 17:02 20000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins Raleigh
Page 20 of 77 10/9/2023
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-14Client Sample ID: S-14
Matrix: SoilDate Collected: 09/20/23 11:45
Percent Solids: 91.6Date Received: 09/22/23 12:36
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
RL MDL
ND 10 2.6 mg/Kg ☼09/26/23 10:23 09/27/23 17:23 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics
(GRO)-C6-C10
a,a,a-Trifluorotoluene 85 70-131 09/26/23 10:23 09/27/23 17:23 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
RL MDL
ND 8.7 2.8 mg/Kg ☼09/25/23 17:58 09/26/23 21:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl (Surr)85 15-139 09/25/23 17:58 09/26/23 21:20 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins Raleigh
Page 21 of 77 10/9/2023
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-15Client Sample ID: S-15
Matrix: SoilDate Collected: 09/20/23 15:00
Percent Solids: 89.1Date Received: 09/22/23 12:36
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
RL MDL
ND 10 2.5 mg/Kg ☼09/26/23 10:23 09/27/23 16:19 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics
(GRO)-C6-C10
a,a,a-Trifluorotoluene 87 70-131 09/26/23 10:23 09/27/23 16:19 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins Raleigh
Page 22 of 77 10/9/2023
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-16Client Sample ID: S-16
Matrix: SoilDate Collected: 09/20/23 15:10
Percent Solids: 91.4Date Received: 09/22/23 12:36
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
RL MDL
ND 11 2.6 mg/Kg ☼09/26/23 10:23 09/27/23 15:58 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics
(GRO)-C6-C10
a,a,a-Trifluorotoluene 85 70-131 09/26/23 10:23 09/27/23 15:58 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins Raleigh
Page 23 of 77 10/9/2023
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-17Client Sample ID: S-17
Matrix: SoilDate Collected: 09/20/23 16:00
Percent Solids: 96.1Date Received: 09/22/23 12:36
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
RL MDL
ND 9.3 2.3 mg/Kg ☼09/26/23 10:23 09/27/23 15:37 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics
(GRO)-C6-C10
a,a,a-Trifluorotoluene 88 70-131 09/26/23 10:23 09/27/23 15:37 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins Raleigh
Page 24 of 77 10/9/2023
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-18Client Sample ID: S-18
Matrix: SoilDate Collected: 09/20/23 16:10
Percent Solids: 92.5Date Received: 09/22/23 12:36
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
RL MDL
ND 9.5 2.4 mg/Kg ☼09/26/23 10:23 09/27/23 15:15 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics
(GRO)-C6-C10
a,a,a-Trifluorotoluene 89 70-131 09/26/23 10:23 09/27/23 15:15 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins Raleigh
Page 25 of 77 10/9/2023
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-19Client Sample ID: S-19
Matrix: SoilDate Collected: 09/20/23 16:30
Percent Solids: 91.0Date Received: 09/22/23 12:36
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
RL MDL
ND 11 2.8 mg/Kg ☼09/26/23 10:23 09/27/23 14:53 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics
(GRO)-C6-C10
a,a,a-Trifluorotoluene 87 70-131 09/26/23 10:23 09/27/23 14:53 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins Raleigh
Page 26 of 77 10/9/2023
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-20Client Sample ID: S-20
Matrix: SoilDate Collected: 09/20/23 16:45
Percent Solids: 79.8Date Received: 09/22/23 12:36
Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
RL MDL
4.6 J 14 3.4 mg/Kg ☼09/26/23 10:23 09/26/23 22:56 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics
(GRO)-C6-C10
a,a,a-Trifluorotoluene 87 70-131 09/26/23 10:23 09/26/23 22:56 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins Raleigh
Page 27 of 77 10/9/2023
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-21Client Sample ID: TMW-1
Matrix: WaterDate Collected: 09/21/23 10:00
Date Received: 09/22/23 12:36
Method: SM6200-B - Volatile Organic Compounds
RL MDL
ND 1000 91 ug/L 10/02/23 21:48 1000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1000 150 ug/L 10/02/23 21:48 1000ND1,1,1-Trichloroethane
1000 85 ug/L 10/02/23 21:48 1000ND1,1,2,2-Tetrachloroethane
1000 68 ug/L 10/02/23 21:48 1000ND1,1,2-Trichloroethane
1000 50 ug/L 10/02/23 21:48 1000ND1,1-Dichloroethane
1000 150 ug/L 10/02/23 21:48 1000ND1,1-Dichloroethene
1000 63 ug/L 10/02/23 21:48 1000ND1,1-Dichloropropene
1000 250 ug/L 10/02/23 21:48 1000ND1,2,3-Trichlorobenzene
1000 150 ug/L 10/02/23 21:48 1000ND1,2,3-Trichloropropane
1000 97 ug/L 10/02/23 21:48 1000ND1,2,4-Trichlorobenzene
1000 67 ug/L 10/02/23 21:48 1000160001,2,4-Trimethylbenzene
1000 480 ug/L 10/02/23 21:48 1000ND1,2-Dibromo-3-Chloropropane
1000 420 ug/L 10/02/23 21:48 1000ND1,2-Dibromoethane
1000 52 ug/L 10/02/23 21:48 1000ND1,2-Dichlorobenzene
1000 82 ug/L 10/02/23 21:48 1000ND1,2-Dichloroethane
1000 98 ug/L 10/02/23 21:48 1000ND1,2-Dichloropropane
1000 100 ug/L 10/02/23 21:48 100042001,3,5-Trimethylbenzene
1000 92 ug/L 10/02/23 21:48 1000ND1,3-Dichlorobenzene
1000 150 ug/L 10/02/23 21:48 1000ND1,3-Dichloropropane
1000 100 ug/L 10/02/23 21:48 1000ND1,4-Dichlorobenzene
1000 120 ug/L 10/02/23 21:48 1000ND2,2-Dichloropropane
1000 100 ug/L 10/02/23 21:48 1000ND2-Chlorotoluene
1000 100 ug/L 10/02/23 21:48 1000ND4-Chlorotoluene
1000 66 ug/L 10/02/23 21:48 1000ND4-Isopropyltoluene
1000 50 ug/L 10/02/23 21:48 10003600Benzene
1000 130 ug/L 10/02/23 21:48 1000NDBromobenzene
1000 110 ug/L 10/02/23 21:48 1000NDBromochloromethane
1000 100 ug/L 10/02/23 21:48 1000NDBromodichloromethane
1000 200 ug/L 10/02/23 21:48 1000NDBromoform
1000 280 ug/L 10/02/23 21:48 1000NDBromomethane
1000 82 ug/L 10/02/23 21:48 1000NDCarbon tetrachloride
1000 69 ug/L 10/02/23 21:48 1000NDChlorobenzene
1000 180 ug/L 10/02/23 21:48 1000NDChloroethane
1000 83 ug/L 10/02/23 21:48 1000NDChloroform
1000 50 ug/L 10/02/23 21:48 1000NDChloromethane
1000 75 ug/L 10/02/23 21:48 1000NDcis-1,2-Dichloroethene
1000 73 ug/L 10/02/23 21:48 1000NDcis-1,3-Dichloropropene
1000 67 ug/L 10/02/23 21:48 1000NDDibromochloromethane
1000 130 ug/L 10/02/23 21:48 1000NDDibromomethane
1000 91 ug/L 10/02/23 21:48 1000NDDichlorodifluoromethane
100000 26000 ug/L 10/02/23 21:48 1000NDEthanol
1000 100 ug/L 10/02/23 21:48 10007000Ethylbenzene
1000 350 ug/L 10/02/23 21:48 1000NDFreon 113
1000 150 ug/L 10/02/23 21:48 1000NDHexachlorobutadiene
1000 210 ug/L 10/02/23 21:48 1000NDIsopropyl ether
1000 130 ug/L 10/02/23 21:48 1000480JIsopropylbenzene
2000 180 ug/L 10/02/23 21:48 100025000m,p-Xylenes
1000 120 ug/L 10/02/23 21:48 1000NDMethyl tert-butyl ether
2000 70 ug/L 10/02/23 21:48 1000180J BMethylene Chloride
Eurofins Raleigh
Page 28 of 77 10/9/2023
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-21Client Sample ID: TMW-1
Matrix: WaterDate Collected: 09/21/23 10:00
Date Received: 09/22/23 12:36
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
3500 1000 86 ug/L 10/02/23 21:48 1000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Naphthalene
1000 74 ug/L 10/02/23 21:48 1000NDn-Butylbenzene
1000 73 ug/L 10/02/23 21:48 10002000N-Propylbenzene
1000 88 ug/L 10/02/23 21:48 100012000o-Xylene
1000 53 ug/L 10/02/23 21:48 1000NDsec-Butylbenzene
1000 82 ug/L 10/02/23 21:48 1000NDStyrene
20000 2500 ug/L 10/02/23 21:48 1000NDtert-Amyl alcohol
10000 210 ug/L 10/02/23 21:48 1000NDTert-amyl methyl ether
20000 3400 ug/L 10/02/23 21:48 1000NDtert-Butyl alcohol
1000 370 ug/L 10/02/23 21:48 1000NDTert-butyl ethyl ether
5000 320 ug/L 10/02/23 21:48 1000NDtert-Butyl Formate
1000 94 ug/L 10/02/23 21:48 1000NDtert-Butylbenzene
1000 99 ug/L 10/02/23 21:48 1000NDTetrachloroethene
1000 53 ug/L 10/02/23 21:48 100029000Toluene
1000 110 ug/L 10/02/23 21:48 1000NDtrans-1,2-Dichloroethene
1000 80 ug/L 10/02/23 21:48 1000NDtrans-1,3-Dichloropropene
1000 130 ug/L 10/02/23 21:48 1000NDTrichloroethene
1000 150 ug/L 10/02/23 21:48 1000NDTrichlorofluoromethane
1000 83 ug/L 10/02/23 21:48 1000NDVinyl chloride
1000 220 ug/L 10/02/23 21:48 100037000Xylenes, Total
Toluene-d8 (Surr)100 70-130 10/02/23 21:48 1000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)104 10/02/23 21:48 100070-130
Dibromofluoromethane (Surr)106 10/02/23 21:48 100070-130
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 9.0 2.0 ug/L 09/25/23 12:01 09/26/23 19:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2,4,6-Trichlorophenol
9.0 3.3 ug/L 09/25/23 12:01 09/26/23 19:08 1ND2,4-Dichlorophenol
9.0 2.7 ug/L 09/25/23 12:01 09/26/23 19:08 1ND2,4-Dimethylphenol
45 14 ug/L 09/25/23 12:01 09/26/23 19:08 1ND2,4-Dinitrophenol
9.0 3.5 ug/L 09/25/23 12:01 09/26/23 19:08 1ND2-Nitrophenol
45 4.8 ug/L 09/25/23 12:01 09/26/23 19:08 1ND4,6-Dinitro-2-methylphenol
9.0 2.2 ug/L 09/25/23 12:01 09/26/23 19:08 1ND4-Chloro-3-methylphenol
45 7.3 ug/L 09/25/23 12:01 09/26/23 19:08 1ND4-Nitrophenol
45 8.9 ug/L 09/25/23 12:01 09/26/23 19:08 1NDPentachlorophenol
9.0 2.9 ug/L 09/25/23 12:01 09/26/23 19:08 1ND2-Chlorophenol
9.0 3.1 ug/L 09/25/23 12:01 09/26/23 19:08 1ND1,2,4-Trichlorobenzene
9.0 2.2 ug/L 09/25/23 12:01 09/26/23 19:08 1ND1,2-Dichlorobenzene
9.0 3.3 ug/L 09/25/23 12:01 09/26/23 19:08 1ND1,2-Diphenylhydrazine
9.0 2.6 ug/L 09/25/23 12:01 09/26/23 19:08 1ND1,3-Dichlorobenzene
9.0 3.0 ug/L 09/25/23 12:01 09/26/23 19:08 1141,4-Dichlorobenzene
9.0 4.3 ug/L 09/25/23 12:01 09/26/23 19:08 1ND*- *12-Chloronaphthalene
9.0 2.5 ug/L 09/25/23 12:01 09/26/23 19:08 1ND2,6-Dinitrotoluene
9.0 2.1 ug/L 09/25/23 12:01 09/26/23 19:08 1ND2,4-Dinitrotoluene
54 9.0 ug/L 09/25/23 12:01 09/26/23 19:08 1ND3,3'-Dichlorobenzidine
9.0 4.2 ug/L 09/25/23 12:01 09/26/23 19:08 1ND*-4-Bromophenyl phenyl ether
9.0 4.8 ug/L 09/25/23 12:01 09/26/23 19:08 1ND4-Chlorophenyl phenyl ether
9.0 4.0 ug/L 09/25/23 12:01 09/26/23 19:08 1NDAcenaphthene
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-21Client Sample ID: TMW-1
Matrix: WaterDate Collected: 09/21/23 10:00
Date Received: 09/22/23 12:36
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 9.0 3.2 ug/L 09/25/23 12:01 09/26/23 19:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acenaphthylene
9.0 3.2 ug/L 09/25/23 12:01 09/26/23 19:08 110Anthracene
72 22 ug/L 09/25/23 12:01 09/26/23 19:08 1NDBenzidine
9.0 3.8 ug/L 09/25/23 12:01 09/26/23 19:08 1NDBenzo[a]anthracene
9.0 2.5 ug/L 09/25/23 12:01 09/26/23 19:08 1NDBenzo[a]pyrene
9.0 2.8 ug/L 09/25/23 12:01 09/26/23 19:08 1NDBenzo[b]fluoranthene
9.0 2.7 ug/L 09/25/23 12:01 09/26/23 19:08 1NDBenzo[g,h,i]perylene
9.0 2.6 ug/L 09/25/23 12:01 09/26/23 19:08 1NDBenzo[k]fluoranthene
9.0 1.6 ug/L 09/25/23 12:01 09/26/23 19:08 1NDBis(2-chloroethoxy)methane
9.0 3.2 ug/L 09/25/23 12:01 09/26/23 19:08 1NDBis(2-chloroethyl)ether
9.0 2.7 ug/L 09/25/23 12:01 09/26/23 19:08 1NDBis(2-ethylhexyl) phthalate
9.0 2.5 ug/L 09/25/23 12:01 09/26/23 19:08 1NDButyl benzyl phthalate
9.0 3.4 ug/L 09/25/23 12:01 09/26/23 19:08 1NDChrysene
9.0 2.1 ug/L 09/25/23 12:01 09/26/23 19:08 1NDDi-n-butyl phthalate
9.0 2.5 ug/L 09/25/23 12:01 09/26/23 19:08 1NDDi-n-octyl phthalate
9.0 2.7 ug/L 09/25/23 12:01 09/26/23 19:08 1NDDibenz(a,h)anthracene
9.0 2.0 ug/L 09/25/23 12:01 09/26/23 19:08 1NDDiethyl phthalate
9.0 1.9 ug/L 09/25/23 12:01 09/26/23 19:08 1NDDimethyl phthalate
9.0 1.4 ug/L 09/25/23 12:01 09/26/23 19:08 15.4 JFluoranthene
9.0 3.1 ug/L 09/25/23 12:01 09/26/23 19:08 121*-Fluorene
9.0 1.4 ug/L 09/25/23 12:01 09/26/23 19:08 1NDHexachlorobenzene
9.0 3.6 ug/L 09/25/23 12:01 09/26/23 19:08 1NDHexachlorobutadiene
9.0 3.1 ug/L 09/25/23 12:01 09/26/23 19:08 1NDHexachlorocyclopentadiene
9.0 3.2 ug/L 09/25/23 12:01 09/26/23 19:08 1NDHexachloroethane
9.0 3.9 ug/L 09/25/23 12:01 09/26/23 19:08 1NDIndeno[1,2,3-cd]pyrene
9.0 1.8 ug/L 09/25/23 12:01 09/26/23 19:08 1NDIsophorone
9.0 2.2 ug/L 09/25/23 12:01 09/26/23 19:08 1NDN-Nitrosodi-n-propylamine
9.0 1.9 ug/L 09/25/23 12:01 09/26/23 19:08 1NDN-Nitrosodimethylamine
9.0 2.6 ug/L 09/25/23 12:01 09/26/23 19:08 1NDN-Nitrosodiphenylamine
9.0 3.1 ug/L 09/25/23 12:01 09/26/23 19:08 1NDNitrobenzene
9.0 3.9 ug/L 09/25/23 12:01 09/26/23 19:08 136Phenanthrene
9.0 3.3 ug/L 09/25/23 12:01 09/26/23 19:08 115Pyrene
9.0 2.8 ug/L 09/25/23 12:01 09/26/23 19:08 1NDbis (2-chloroisopropyl) ether
9.0 1.3 ug/L 09/25/23 12:01 09/26/23 19:08 1NDPhenol
2,4,6-Tribromophenol (Surr)49 30-130 09/25/23 12:01 09/26/23 19:08 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)24 09/25/23 12:01 09/26/23 19:08 110-130
Phenol-d5 (Surr)28 09/25/23 12:01 09/26/23 19:08 18-424
2-Fluorobiphenyl (Surr)48 09/25/23 12:01 09/26/23 19:08 125-130
Nitrobenzene-d5 (Surr)71 09/25/23 12:01 09/26/23 19:08 115-314
Terphenyl-d14 (Surr)54 09/25/23 12:01 09/26/23 19:08 135-131
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) - DL
RL MDL
4400 450 160 ug/L 09/25/23 12:01 09/27/23 21:52 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Naphthalene
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
42000 13000 13000 ug/L 10/05/23 16:41 500
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics
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Client Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Lab Sample ID: 752-11855-21Client Sample ID: TMW-1
Matrix: WaterDate Collected: 09/21/23 10:00
Date Received: 09/22/23 12:36
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
RL MDL
22000 5500 5500 ug/L 10/05/23 16:41 500
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C9-C12 Aliphatics
3500 3500 ug/L 10/05/23 16:41 50032000C9-C10 Aromatics
a,a,a-Trifluorotoluene (fid)99 70-130 10/05/23 16:41 500
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)98 10/05/23 16:41 50070-130
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
140 0.73 0.73 mg/L 09/26/23 22:21 10/04/23 15:20 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C9-C18 Aliphatics
0.15 0.15 mg/L 09/26/23 22:21 10/02/23 13:16 18.7C19-C36 Aliphatics
0.30 0.30 mg/L 09/26/23 22:21 09/29/23 07:54 151C11-C22 Aromatics
1-Chlorooctadecane 64 40-140 09/26/23 22:21 10/02/23 13:16 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1-Chlorooctadecane 75 09/26/23 22:21 10/04/23 15:20 540-140
o-Terphenyl 64 09/26/23 22:21 09/29/23 07:54 140-140
2-Fluorobiphenyl 25 S1-09/26/23 22:21 09/29/23 07:54 140-140
2-Bromonaphthalene 6 S1-09/26/23 22:21 09/29/23 07:54 140-140
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Surrogate Summary
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Method: SM6200-B - Volatile Organic Compounds
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (70-130)(70-130)(70-130)
TOL BFB DBFM
100 104 106752-11855-21
Percent Surrogate Recovery (Acceptance Limits)
TMW-1
98 101 109LCS 752-4657/6 Lab Control Sample
95 101 99LCS 752-4657/8 Lab Control Sample
96 102 99LCSD 752-4657/7 Lab Control Sample Dup
100 99 103MB 752-4657/10 Method Blank
98 102 103MRL 752-4657/17 Lab Control Sample
98 106 105MRL 752-4657/5 Lab Control Sample
Surrogate Legend
TOL = Toluene-d8 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (Surr)
Method: 625.1 - Semivolatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-130)(10-130)(8-424)(25-130)(15-314)(35-131)
TBP 2FP PHL FBP NBZ TPHL
49 24 28 48 71 54752-11855-21
Percent Surrogate Recovery (Acceptance Limits)
TMW-1
69 33 24 6863 73LCS 680-799510/2-A Lab Control Sample
49 28 21 5146 57LCSD 680-799510/3-A Lab Control Sample Dup
46 26 16 4949 54MB 680-799510/1-A Method Blank
Surrogate Legend
TBP = 2,4,6-Tribromophenol (Surr)
2FP = 2-Fluorophenol (Surr)
PHL = Phenol-d5 (Surr)
FBP = 2-Fluorobiphenyl (Surr)
NBZ = Nitrobenzene-d5 (Surr)
TPHL = Terphenyl-d14 (Surr)
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
Prep Type: Total/NAMatrix: Soil
Lab Sample ID Client Sample ID (70-131)
TFT1
88752-11855-1
Percent Surrogate Recovery (Acceptance Limits)
S-1
87752-11855-2 S-2
82752-11855-3 S-3
86752-11855-4 S-4
84752-11855-5 S-5
84752-11855-6 S-6
85752-11855-7 S-7
82752-11855-8 S-8
84752-11855-9 S-9
84752-11855-10 S-10
84752-11855-11 S-11
85752-11855-12 S-12
93752-11855-13 S-13
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Surrogate Summary
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
(Continued)
Prep Type: Total/NAMatrix: Soil
Lab Sample ID Client Sample ID (70-131)
TFT1
85752-11855-14
Percent Surrogate Recovery (Acceptance Limits)
S-14
87752-11855-15 S-15
85752-11855-16 S-16
88752-11855-17 S-17
89752-11855-18 S-18
87752-11855-19 S-19
87752-11855-20 S-20
Surrogate Legend
TFT = a,a,a-Trifluorotoluene
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (70-131)
TFT1
127LCS 680-799722/6
Percent Surrogate Recovery (Acceptance Limits)
Lab Control Sample
118LCS 680-799893/5 Lab Control Sample
116LCS 680-800868/5 Lab Control Sample
124LCSD 680-799722/7 Lab Control Sample Dup
121LCSD 680-799893/6 Lab Control Sample Dup
116LCSD 680-800868/6 Lab Control Sample Dup
92MB 680-799722/8 Method Blank
90MB 680-799893/7 Method Blank
89MB 680-800868/7 Method Blank
Surrogate Legend
TFT = a,a,a-Trifluorotoluene
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (70-130)(70-130)
TFT-F1 TFT-P1
96 101400-244015-D-4 MS
Percent Surrogate Recovery (Acceptance Limits)
Matrix Spike
97 101400-244015-D-4 MSD Matrix Spike Duplicate
99 98752-11855-21 TMW-1
97 102LCS 400-644204/4 Lab Control Sample
97 101LCSD 400-644204/5 Lab Control Sample Dup
97 96MB 400-644204/2 Method Blank
Surrogate Legend
TFT-F = a,a,a-Trifluorotoluene (fid)
TFT-P = a,a,a-Trifluorotoluene (pid)
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Surrogate Summary
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
Prep Type: Total/NAMatrix: Soil
Lab Sample ID Client Sample ID (15-139)
OTPH1
79752-11855-1
Percent Surrogate Recovery (Acceptance Limits)
S-1
97752-11855-2 S-2
110752-11855-3 S-3
75752-11855-4 S-4
85752-11855-14 S-14
Surrogate Legend
OTPH = o-Terphenyl (Surr)
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (15-139)
OTPH1
88680-240669-A-1-B MS
Percent Surrogate Recovery (Acceptance Limits)
Matrix Spike
91680-240669-A-1-C MSD Matrix Spike Duplicate
101LCS 680-799570/17-A Lab Control Sample
82MB 680-799570/16-A Method Blank
Surrogate Legend
OTPH = o-Terphenyl (Surr)
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (40-140)(40-140)(40-140)
OTPH1 FBP1 2BN1
64 25 S1-6 S1-752-11855-21
Percent Surrogate Recovery (Acceptance Limits)
TMW-1
59 68 98LCS 400-642868/2-A Lab Control Sample
74 76 107LCSD 400-642868/3-A Lab Control Sample Dup
64 65 52MB 400-642868/1-A Method Blank
Surrogate Legend
OTPH = o-Terphenyl
FBP = 2-Fluorobiphenyl
2BN = 2-Bromonaphthalene
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (40-140)
1COD1
64752-11855-21
Percent Surrogate Recovery (Acceptance Limits)
TMW-1
75752-11855-21 TMW-1
73LCS 400-642868/2-A Lab Control Sample
73LCSD 400-642868/3-A Lab Control Sample Dup
74MB 400-642868/1-A Method Blank
Surrogate Legend
1COD = 1-Chlorooctadecane
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QC Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Method: SM6200-B - Volatile Organic Compounds
Client Sample ID: Method BlankLab Sample ID: MB 752-4657/10
Matrix: Water Prep Type: Total/NA
Analysis Batch: 4657
RL MDL
1,1,1,2-Tetrachloroethane ND 1.0 0.091 ug/L 10/02/23 18:51 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.151.0 ug/L 10/02/23 18:51 11,1,1-Trichloroethane
ND 0.0851.0 ug/L 10/02/23 18:51 11,1,2,2-Tetrachloroethane
ND 0.0681.0 ug/L 10/02/23 18:51 11,1,2-Trichloroethane
ND 0.0501.0 ug/L 10/02/23 18:51 11,1-Dichloroethane
ND 0.151.0 ug/L 10/02/23 18:51 11,1-Dichloroethene
ND 0.0631.0 ug/L 10/02/23 18:51 11,1-Dichloropropene
ND 0.251.0 ug/L 10/02/23 18:51 11,2,3-Trichlorobenzene
ND 0.151.0 ug/L 10/02/23 18:51 11,2,3-Trichloropropane
ND 0.0971.0 ug/L 10/02/23 18:51 11,2,4-Trichlorobenzene
ND 0.0671.0 ug/L 10/02/23 18:51 11,2,4-Trimethylbenzene
ND 0.481.0 ug/L 10/02/23 18:51 11,2-Dibromo-3-Chloropropane
ND 0.421.0 ug/L 10/02/23 18:51 11,2-Dibromoethane
ND 0.0521.0 ug/L 10/02/23 18:51 11,2-Dichlorobenzene
ND 0.0821.0 ug/L 10/02/23 18:51 11,2-Dichloroethane
ND 0.0981.0 ug/L 10/02/23 18:51 11,2-Dichloropropane
ND 0.101.0 ug/L 10/02/23 18:51 11,3,5-Trimethylbenzene
ND 0.0921.0 ug/L 10/02/23 18:51 11,3-Dichlorobenzene
ND 0.151.0 ug/L 10/02/23 18:51 11,3-Dichloropropane
ND 0.101.0 ug/L 10/02/23 18:51 11,4-Dichlorobenzene
ND 0.121.0 ug/L 10/02/23 18:51 12,2-Dichloropropane
ND 0.101.0 ug/L 10/02/23 18:51 12-Chlorotoluene
ND 0.101.0 ug/L 10/02/23 18:51 14-Chlorotoluene
ND 0.0661.0 ug/L 10/02/23 18:51 14-Isopropyltoluene
ND 0.0501.0 ug/L 10/02/23 18:51 1Benzene
ND 0.131.0 ug/L 10/02/23 18:51 1Bromobenzene
ND 0.111.0 ug/L 10/02/23 18:51 1Bromochloromethane
ND 0.101.0 ug/L 10/02/23 18:51 1Bromodichloromethane
ND 0.201.0 ug/L 10/02/23 18:51 1Bromoform
ND 0.281.0 ug/L 10/02/23 18:51 1Bromomethane
ND 0.0821.0 ug/L 10/02/23 18:51 1Carbon tetrachloride
ND 0.0691.0 ug/L 10/02/23 18:51 1Chlorobenzene
ND 0.181.0 ug/L 10/02/23 18:51 1Chloroethane
ND 0.0831.0 ug/L 10/02/23 18:51 1Chloroform
ND 0.0501.0 ug/L 10/02/23 18:51 1Chloromethane
ND 0.0751.0 ug/L 10/02/23 18:51 1cis-1,2-Dichloroethene
ND 0.0731.0 ug/L 10/02/23 18:51 1cis-1,3-Dichloropropene
ND 0.0671.0 ug/L 10/02/23 18:51 1Dibromochloromethane
ND 0.131.0 ug/L 10/02/23 18:51 1Dibromomethane
ND 0.0911.0 ug/L 10/02/23 18:51 1Dichlorodifluoromethane
ND 26100 ug/L 10/02/23 18:51 1Ethanol
ND 0.101.0 ug/L 10/02/23 18:51 1Ethylbenzene
ND 0.351.0 ug/L 10/02/23 18:51 1Freon 113
ND 0.151.0 ug/L 10/02/23 18:51 1Hexachlorobutadiene
ND 0.211.0 ug/L 10/02/23 18:51 1Isopropyl ether
ND 0.131.0 ug/L 10/02/23 18:51 1Isopropylbenzene
ND 0.182.0 ug/L 10/02/23 18:51 1m,p-Xylenes
ND 0.121.0 ug/L 10/02/23 18:51 1Methyl tert-butyl ether
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QC Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 752-4657/10
Matrix: Water Prep Type: Total/NA
Analysis Batch: 4657
RL MDL
Methylene Chloride 0.115 J 2.0 0.070 ug/L 10/02/23 18:51 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.0861.0 ug/L 10/02/23 18:51 1Naphthalene
ND 0.0741.0 ug/L 10/02/23 18:51 1n-Butylbenzene
ND 0.0731.0 ug/L 10/02/23 18:51 1N-Propylbenzene
ND 0.0881.0 ug/L 10/02/23 18:51 1o-Xylene
ND 0.0531.0 ug/L 10/02/23 18:51 1sec-Butylbenzene
ND 0.0821.0 ug/L 10/02/23 18:51 1Styrene
ND 2.520 ug/L 10/02/23 18:51 1tert-Amyl alcohol
ND 0.2110 ug/L 10/02/23 18:51 1Tert-amyl methyl ether
ND 3.420 ug/L 10/02/23 18:51 1tert-Butyl alcohol
ND 0.371.0 ug/L 10/02/23 18:51 1Tert-butyl ethyl ether
ND 0.325.0 ug/L 10/02/23 18:51 1tert-Butyl Formate
ND 0.0941.0 ug/L 10/02/23 18:51 1tert-Butylbenzene
ND 0.0991.0 ug/L 10/02/23 18:51 1Tetrachloroethene
ND 0.0531.0 ug/L 10/02/23 18:51 1Toluene
ND 0.111.0 ug/L 10/02/23 18:51 1trans-1,2-Dichloroethene
ND 0.0801.0 ug/L 10/02/23 18:51 1trans-1,3-Dichloropropene
ND 0.131.0 ug/L 10/02/23 18:51 1Trichloroethene
ND 0.151.0 ug/L 10/02/23 18:51 1Trichlorofluoromethane
ND 0.0831.0 ug/L 10/02/23 18:51 1Vinyl chloride
ND 0.221.0 ug/L 10/02/23 18:51 1Xylenes, Total
Toluene-d8 (Surr)100 70-130 10/02/23 18:51 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
99 10/02/23 18:51 14-Bromofluorobenzene (Surr)70-130
103 10/02/23 18:51 1Dibromofluoromethane (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 752-4657/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 4657
1,1,1,2-Tetrachloroethane 20.0 20.6 ug/L 103 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 20.0 20.6 ug/L 103 70 -130
1,1,2,2-Tetrachloroethane 20.0 18.7 ug/L 94 70 -130
1,1,2-Trichloroethane 20.0 17.6 ug/L 88 70 -130
1,1-Dichloroethane 20.0 20.3 ug/L 101 70 -130
1,1-Dichloroethene 20.0 20.7 ug/L 103 70 -130
1,1-Dichloropropene 20.0 19.3 ug/L 97 70 -130
1,2,3-Trichlorobenzene 20.0 18.7 ug/L 93 70 -130
1,2,3-Trichloropropane 20.0 18.5 ug/L 92 70 -130
1,2,4-Trichlorobenzene 20.0 18.4 ug/L 92 70 -130
1,2,4-Trimethylbenzene 20.0 19.4 ug/L 97 70 -130
1,2-Dibromo-3-Chloropropane 20.0 20.2 ug/L 101 70 -130
1,2-Dibromoethane 20.0 18.2 ug/L 91 70 -130
1,2-Dichlorobenzene 20.0 19.1 ug/L 95 70 -130
1,2-Dichloroethane 20.0 18.4 ug/L 92 70 -130
1,2-Dichloropropane 20.0 19.5 ug/L 98 70 -130
Eurofins Raleigh
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QC Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 752-4657/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 4657
1,3,5-Trimethylbenzene 20.0 17.9 ug/L 89 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,3-Dichlorobenzene 20.0 18.4 ug/L 92 70 -130
1,3-Dichloropropane 20.0 17.7 ug/L 88 70 -130
1,4-Dichlorobenzene 20.0 19.3 ug/L 97 70 -130
2,2-Dichloropropane 20.0 21.3 ug/L 106 70 -130
2-Chlorotoluene 20.0 18.3 ug/L 91 70 -130
4-Chlorotoluene 20.0 18.9 ug/L 94 70 -130
4-Isopropyltoluene 20.0 19.4 ug/L 97 70 -130
Benzene 20.0 18.7 ug/L 94 70 -130
Bromobenzene 20.0 16.7 ug/L 83 70 -130
Bromochloromethane 20.0 19.6 ug/L 98 70 -130
Bromodichloromethane 20.0 19.2 ug/L 96 70 -130
Bromoform 20.0 21.3 ug/L 106 70 -130
Bromomethane 20.0 16.2 ug/L 81 60 -140
Carbon tetrachloride 20.0 20.2 ug/L 101 70 -130
Chlorobenzene 20.0 18.5 ug/L 92 70 -130
Chloroethane 20.0 20.1 ug/L 101 60 -140
Chloroform 20.0 18.9 ug/L 95 70 -130
Chloromethane 20.0 18.5 ug/L 93 60 -140
cis-1,2-Dichloroethene 20.0 20.4 ug/L 102 70 -130
cis-1,3-Dichloropropene 20.0 18.4 ug/L 92 70 -130
Dibromochloromethane 20.0 18.5 ug/L 92 70 -130
Dibromomethane 20.0 18.0 ug/L 90 70 -130
Dichlorodifluoromethane 20.0 22.5 ug/L 113 60 -140
Ethanol 100 101 ug/L 101 70 -130
Ethylbenzene 20.0 17.6 ug/L 88 70 -130
Freon 113 40.0 45.9 ug/L 115 70 -130
Hexachlorobutadiene 20.0 16.3 ug/L 82 70 -130
Isopropyl ether 20.0 21.4 ug/L 107 70 -130
Isopropylbenzene 20.0 18.2 ug/L 91 70 -130
m,p-Xylenes 40.0 36.4 ug/L 91 70 -130
Methyl tert-butyl ether 20.0 20.7 ug/L 104 70 -130
Methylene Chloride 20.0 21.0 ug/L 105 70 -130
Naphthalene 20.0 18.8 ug/L 94 70 -130
n-Butylbenzene 20.0 18.1 ug/L 91 70 -130
N-Propylbenzene 20.0 18.2 ug/L 91 70 -130
o-Xylene 20.0 17.7 ug/L 88 70 -130
sec-Butylbenzene 20.0 19.3 ug/L 97 70 -130
Styrene 20.0 17.9 ug/L 89 70 -130
tert-Butylbenzene 20.0 19.9 ug/L 99 70 -130
Tetrachloroethene 20.0 19.0 ug/L 95 70 -130
Toluene 20.0 17.7 ug/L 89 70 -130
trans-1,2-Dichloroethene 20.0 20.2 ug/L 101 70 -130
trans-1,3-Dichloropropene 20.0 19.9 ug/L 99 70 -130
Trichloroethene 20.0 17.6 ug/L 88 70 -130
Trichlorofluoromethane 20.0 23.3 ug/L 117 60 -140
Vinyl chloride 20.0 17.8 ug/L 89 60 -140
Xylenes, Total 60.0 54.1 ug/L 90 70 -130
Eurofins Raleigh
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QC Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 752-4657/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 4657
Toluene-d8 (Surr)70 -130
Surrogate
98
LCS LCS
Qualifier Limits%Recovery
1014-Bromofluorobenzene (Surr)70 -130
109Dibromofluoromethane (Surr)70 -130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 752-4657/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 4657
tert-Amyl alcohol 200 157 ug/L 78 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Tert-amyl methyl ether 20.0 18.2 ug/L 91 70 -130
tert-Butyl alcohol 200 158 ug/L 79 70 -130
Tert-butyl ethyl ether 20.0 17.7 ug/L 89 70 -130
tert-Butyl Formate 20.0 23.7 ug/L 118 70 -130
Toluene-d8 (Surr)70 -130
Surrogate
95
LCS LCS
Qualifier Limits%Recovery
1014-Bromofluorobenzene (Surr)70 -130
99Dibromofluoromethane (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 752-4657/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 4657
1,1,1,2-Tetrachloroethane 20.0 17.2 ug/L 86 70 -130 18
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 20.0 18.7 ug/L 94 70 -130 9
1,1,2,2-Tetrachloroethane 20.0 17.5 ug/L 87 70 -130 7
1,1,2-Trichloroethane 20.0 16.2 ug/L 81 70 -130 8
1,1-Dichloroethane 20.0 18.4 ug/L 92 70 -130 10
1,1-Dichloroethene 20.0 19.2 ug/L 96 70 -130 7
1,1-Dichloropropene 20.0 18.9 ug/L 95 70 -130 2
1,2,3-Trichlorobenzene 20.0 18.3 ug/L 92 70 -130 2
1,2,3-Trichloropropane 20.0 16.1 ug/L 81 70 -130 14
1,2,4-Trichlorobenzene 20.0 19.1 ug/L 95 70 -130 4
1,2,4-Trimethylbenzene 20.0 18.4 ug/L 92 70 -130 5
1,2-Dibromo-3-Chloropropane 20.0 18.4 ug/L 92 70 -130 10
1,2-Dibromoethane 20.0 17.4 ug/L 87 70 -130 4
1,2-Dichlorobenzene 20.0 19.0 ug/L 95 70 -130 0
1,2-Dichloroethane 20.0 19.2 ug/L 96 70 -130 5
1,2-Dichloropropane 20.0 19.5 ug/L 97 70 -130 0
1,3,5-Trimethylbenzene 20.0 17.1 ug/L 85 70 -130 5
1,3-Dichlorobenzene 20.0 18.8 ug/L 94 70 -130 2
1,3-Dichloropropane 20.0 17.3 ug/L 86 70 -130 2
1,4-Dichlorobenzene 20.0 18.9 ug/L 94 70 -130 2
2,2-Dichloropropane 20.0 18.6 ug/L 93 70 -130 13
2-Chlorotoluene 20.0 18.6 ug/L 93 70 -130 2
4-Chlorotoluene 20.0 17.3 ug/L 86 70 -130 9
Eurofins Raleigh
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QC Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 752-4657/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 4657
4-Isopropyltoluene 20.0 19.5 ug/L 98 70 -130 1
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Benzene 20.0 18.3 ug/L 92 70 -130 2
Bromobenzene 20.0 16.5 ug/L 82 70 -130 1
Bromochloromethane 20.0 19.9 ug/L 100 70 -130 2
Bromodichloromethane 20.0 17.8 ug/L 89 70 -130 8
Bromoform 20.0 20.8 ug/L 104 70 -130 2
Bromomethane 20.0 16.0 ug/L 80 60 -140 1
Carbon tetrachloride 20.0 18.3 ug/L 91 70 -130 10
Chlorobenzene 20.0 17.2 ug/L 86 70 -130 7
Chloroethane 20.0 19.1 ug/L 95 60 -140 5
Chloroform 20.0 18.9 ug/L 94 70 -130 0
Chloromethane 20.0 16.5 ug/L 83 60 -140 12
cis-1,2-Dichloroethene 20.0 19.3 ug/L 97 70 -130 5
cis-1,3-Dichloropropene 20.0 19.1 ug/L 95 70 -130 3
Dibromochloromethane 20.0 17.9 ug/L 89 70 -130 3
Dibromomethane 20.0 18.7 ug/L 93 70 -130 4
Dichlorodifluoromethane 20.0 20.2 ug/L 101 60 -140 11
Ethanol 100 117 ug/L 117 70 -130 14
Ethylbenzene 20.0 17.0 ug/L 85 70 -130 4
Freon 113 40.0 43.8 ug/L 109 70 -130 5
Hexachlorobutadiene 20.0 17.6 ug/L 88 70 -130 7
Isopropyl ether 20.0 20.8 ug/L 104 70 -130 3
Isopropylbenzene 20.0 16.6 ug/L 83 70 -130 9
m,p-Xylenes 40.0 34.9 ug/L 87 70 -130 4
Methyl tert-butyl ether 20.0 20.4 ug/L 102 70 -130 2
Methylene Chloride 20.0 19.9 ug/L 99 70 -130 5
Naphthalene 20.0 19.1 ug/L 96 70 -130 2
n-Butylbenzene 20.0 17.1 ug/L 86 70 -130 6
N-Propylbenzene 20.0 17.2 ug/L 86 70 -130 6
o-Xylene 20.0 16.8 ug/L 84 70 -130 5
sec-Butylbenzene 20.0 18.7 ug/L 94 70 -130 3
Styrene 20.0 16.9 ug/L 85 70 -130 5
tert-Butylbenzene 20.0 20.9 ug/L 105 70 -130 5
Tetrachloroethene 20.0 16.8 ug/L 84 70 -130 12
Toluene 20.0 16.6 ug/L 83 70 -130 7
trans-1,2-Dichloroethene 20.0 18.8 ug/L 94 70 -130 7
trans-1,3-Dichloropropene 20.0 18.5 ug/L 92 70 -130 7
Trichloroethene 20.0 17.8 ug/L 89 70 -130 1
Trichlorofluoromethane 20.0 22.0 ug/L 110 60 -140 6
Vinyl chloride 20.0 17.5 ug/L 87 60 -140 2
Xylenes, Total 60.0 51.7 ug/L 86 70 -130 5
Toluene-d8 (Surr)70 -130
Surrogate
96
LCSD LCSD
Qualifier Limits%Recovery
1024-Bromofluorobenzene (Surr)70 -130
99Dibromofluoromethane (Surr)70 -130
Eurofins Raleigh
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QC Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: MRL 752-4657/17
Matrix: Water Prep Type: Total/NA
Analysis Batch: 4657
tert-Amyl alcohol 10.0 3.59 J ug/L 36
Analyte
MRL MRL
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Tert-amyl methyl ether 1.00 0.870 J ug/L 87
tert-Butyl alcohol 10.0 8.89 J ug/L 89
Tert-butyl ethyl ether 1.00 0.989 J ug/L 99
tert-Butyl Formate 1.00 1.34 J ug/L 134
Toluene-d8 (Surr)70 -130
Surrogate
98
MRL MRL
Qualifier Limits%Recovery
1024-Bromofluorobenzene (Surr)70 -130
103Dibromofluoromethane (Surr)70 -130
Client Sample ID: Lab Control SampleLab Sample ID: MRL 752-4657/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 4657
1,1,1,2-Tetrachloroethane 1.00 1.00 ug/L 100
Analyte
MRL MRL
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 1.00 1.17 ug/L 117
1,1,2,2-Tetrachloroethane 1.00 1.02 ug/L 102
1,1,2-Trichloroethane 1.00 1.13 ug/L 113
1,1-Dichloroethane 1.00 1.10 ug/L 110
1,1-Dichloroethene 1.00 1.08 ug/L 108
1,1-Dichloropropene 1.00 1.09 ug/L 109
1,2,3-Trichlorobenzene 1.00 1.10 ug/L 110
1,2,3-Trichloropropane 1.00 0.442 J ug/L 44
1,2,4-Trichlorobenzene 1.00 1.41 ug/L 141
1,2,4-Trimethylbenzene 1.00 1.01 ug/L 101
1,2-Dibromo-3-Chloropropane 1.00 1.28 ug/L 128
1,2-Dibromoethane 1.00 1.17 ug/L 117
1,2-Dichlorobenzene 1.00 1.02 ug/L 102
1,2-Dichloroethane 1.00 0.818 J ug/L 82
1,2-Dichloropropane 1.00 1.13 ug/L 113
1,3,5-Trimethylbenzene 1.00 0.777 J ug/L 78
1,3-Dichlorobenzene 1.00 0.908 J ug/L 91
1,3-Dichloropropane 1.00 1.32 ug/L 132
1,4-Dichlorobenzene 1.00 1.15 ug/L 115
2,2-Dichloropropane 1.00 1.66 ug/L 166
2-Chlorotoluene 1.00 1.08 ug/L 108
4-Chlorotoluene 1.00 1.26 ug/L 126
4-Isopropyltoluene 1.00 0.923 J ug/L 92
Benzene 1.00 1.10 ug/L 110
Bromobenzene 1.00 0.998 J ug/L 100
Bromochloromethane 1.00 0.930 J ug/L 93
Bromodichloromethane 1.00 0.780 J ug/L 78
Bromoform 1.00 1.18 ug/L 118
Bromomethane 1.00 0.332 J ug/L 33
Carbon tetrachloride 1.00 0.765 J ug/L 77
Chlorobenzene 1.00 0.999 J ug/L 100
Eurofins Raleigh
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QC Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: MRL 752-4657/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 4657
Chloroethane 1.00 0.309 J ug/L 31
Analyte
MRL MRL
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Chloroform 1.00 1.01 ug/L 101
Chloromethane 1.00 0.268 J ug/L 27
cis-1,2-Dichloroethene 1.00 1.16 ug/L 116
cis-1,3-Dichloropropene 1.00 1.15 ug/L 115
Dibromochloromethane 1.00 0.699 J ug/L 70
Dibromomethane 1.00 1.28 ug/L 128
Dichlorodifluoromethane 1.00 ND ug/L 0
Ethanol 20.0 41.5 J ug/L 208
Ethylbenzene 1.00 0.923 J ug/L 92
Freon 113 1.00 1.50 ug/L 150
Hexachlorobutadiene 1.00 1.24 ug/L 124
Isopropyl ether 1.00 1.22 ug/L 122
Isopropylbenzene 1.00 1.02 ug/L 102
m,p-Xylenes 2.00 2.17 ug/L 108
Methyl tert-butyl ether 1.00 1.13 ug/L 113
Methylene Chloride 1.00 0.745 J ug/L 74
Naphthalene 1.00 1.04 ug/L 104
n-Butylbenzene 1.00 0.808 J ug/L 81
N-Propylbenzene 1.00 1.06 ug/L 106
o-Xylene 1.00 0.960 J ug/L 96
sec-Butylbenzene 1.00 0.866 J ug/L 87
Styrene 1.00 1.02 ug/L 102
tert-Butylbenzene 1.00 1.03 ug/L 103
Tetrachloroethene 1.00 0.889 J ug/L 89
Toluene 1.00 1.06 ug/L 106
trans-1,2-Dichloroethene 1.00 0.467 J ug/L 47
trans-1,3-Dichloropropene 1.00 0.970 J ug/L 97
Trichloroethene 1.00 1.39 ug/L 139
Trichlorofluoromethane 1.00 0.559 J ug/L 56
Vinyl chloride 1.00 0.437 J ug/L 44
Xylenes, Total 3.00 3.13 ug/L 104
Toluene-d8 (Surr)70 -130
Surrogate
98
MRL MRL
Qualifier Limits%Recovery
1064-Bromofluorobenzene (Surr)70 -130
105Dibromofluoromethane (Surr)70 -130
Method: 625.1 - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-799510/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 799589 Prep Batch: 799510
RL MDL
2,4,6-Trichlorophenol ND 10 2.2 ug/L 09/25/23 12:01 09/26/23 14:46 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 3.710 ug/L 09/25/23 12:01 09/26/23 14:46 12,4-Dichlorophenol
ND 3.010 ug/L 09/25/23 12:01 09/26/23 14:46 12,4-Dimethylphenol
ND 1650 ug/L 09/25/23 12:01 09/26/23 14:46 12,4-Dinitrophenol
Eurofins Raleigh
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QC Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-799510/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 799589 Prep Batch: 799510
RL MDL
2-Nitrophenol ND 10 3.9 ug/L 09/25/23 12:01 09/26/23 14:46 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 5.350 ug/L 09/25/23 12:01 09/26/23 14:46 14,6-Dinitro-2-methylphenol
ND 2.510 ug/L 09/25/23 12:01 09/26/23 14:46 14-Chloro-3-methylphenol
ND 8.150 ug/L 09/25/23 12:01 09/26/23 14:46 14-Nitrophenol
ND 9.950 ug/L 09/25/23 12:01 09/26/23 14:46 1Pentachlorophenol
ND 3.210 ug/L 09/25/23 12:01 09/26/23 14:46 12-Chlorophenol
ND 3.410 ug/L 09/25/23 12:01 09/26/23 14:46 11,2,4-Trichlorobenzene
ND 2.510 ug/L 09/25/23 12:01 09/26/23 14:46 11,2-Dichlorobenzene
ND 3.710 ug/L 09/25/23 12:01 09/26/23 14:46 11,2-Diphenylhydrazine
ND 2.910 ug/L 09/25/23 12:01 09/26/23 14:46 11,3-Dichlorobenzene
ND 3.310 ug/L 09/25/23 12:01 09/26/23 14:46 11,4-Dichlorobenzene
ND 4.810 ug/L 09/25/23 12:01 09/26/23 14:46 12-Chloronaphthalene
ND 2.810 ug/L 09/25/23 12:01 09/26/23 14:46 12,6-Dinitrotoluene
ND 2.310 ug/L 09/25/23 12:01 09/26/23 14:46 12,4-Dinitrotoluene
ND 1060 ug/L 09/25/23 12:01 09/26/23 14:46 13,3'-Dichlorobenzidine
ND 4.710 ug/L 09/25/23 12:01 09/26/23 14:46 14-Bromophenyl phenyl ether
ND 5.310 ug/L 09/25/23 12:01 09/26/23 14:46 14-Chlorophenyl phenyl ether
ND 4.410 ug/L 09/25/23 12:01 09/26/23 14:46 1Acenaphthene
ND 3.610 ug/L 09/25/23 12:01 09/26/23 14:46 1Acenaphthylene
ND 3.610 ug/L 09/25/23 12:01 09/26/23 14:46 1Anthracene
ND 2580 ug/L 09/25/23 12:01 09/26/23 14:46 1Benzidine
ND 4.210 ug/L 09/25/23 12:01 09/26/23 14:46 1Benzo[a]anthracene
ND 2.810 ug/L 09/25/23 12:01 09/26/23 14:46 1Benzo[a]pyrene
ND 3.110 ug/L 09/25/23 12:01 09/26/23 14:46 1Benzo[b]fluoranthene
ND 3.010 ug/L 09/25/23 12:01 09/26/23 14:46 1Benzo[g,h,i]perylene
ND 2.910 ug/L 09/25/23 12:01 09/26/23 14:46 1Benzo[k]fluoranthene
ND 1.810 ug/L 09/25/23 12:01 09/26/23 14:46 1Bis(2-chloroethoxy)methane
ND 3.610 ug/L 09/25/23 12:01 09/26/23 14:46 1Bis(2-chloroethyl)ether
ND 3.010 ug/L 09/25/23 12:01 09/26/23 14:46 1Bis(2-ethylhexyl) phthalate
ND 2.810 ug/L 09/25/23 12:01 09/26/23 14:46 1Butyl benzyl phthalate
ND 3.810 ug/L 09/25/23 12:01 09/26/23 14:46 1Chrysene
ND 2.310 ug/L 09/25/23 12:01 09/26/23 14:46 1Di-n-butyl phthalate
ND 2.810 ug/L 09/25/23 12:01 09/26/23 14:46 1Di-n-octyl phthalate
ND 3.010 ug/L 09/25/23 12:01 09/26/23 14:46 1Dibenz(a,h)anthracene
ND 2.210 ug/L 09/25/23 12:01 09/26/23 14:46 1Diethyl phthalate
ND 2.110 ug/L 09/25/23 12:01 09/26/23 14:46 1Dimethyl phthalate
ND 1.610 ug/L 09/25/23 12:01 09/26/23 14:46 1Fluoranthene
ND 3.410 ug/L 09/25/23 12:01 09/26/23 14:46 1Fluorene
ND 1.610 ug/L 09/25/23 12:01 09/26/23 14:46 1Hexachlorobenzene
ND 4.010 ug/L 09/25/23 12:01 09/26/23 14:46 1Hexachlorobutadiene
ND 3.510 ug/L 09/25/23 12:01 09/26/23 14:46 1Hexachlorocyclopentadiene
ND 3.610 ug/L 09/25/23 12:01 09/26/23 14:46 1Hexachloroethane
ND 4.310 ug/L 09/25/23 12:01 09/26/23 14:46 1Indeno[1,2,3-cd]pyrene
ND 2.010 ug/L 09/25/23 12:01 09/26/23 14:46 1Isophorone
ND 2.410 ug/L 09/25/23 12:01 09/26/23 14:46 1N-Nitrosodi-n-propylamine
ND 2.110 ug/L 09/25/23 12:01 09/26/23 14:46 1N-Nitrosodimethylamine
ND 2.910 ug/L 09/25/23 12:01 09/26/23 14:46 1N-Nitrosodiphenylamine
ND 3.510 ug/L 09/25/23 12:01 09/26/23 14:46 1Naphthalene
ND 3.510 ug/L 09/25/23 12:01 09/26/23 14:46 1Nitrobenzene
Eurofins Raleigh
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QC Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-799510/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 799589 Prep Batch: 799510
RL MDL
Phenanthrene ND 10 4.3 ug/L 09/25/23 12:01 09/26/23 14:46 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 3.710 ug/L 09/25/23 12:01 09/26/23 14:46 1Pyrene
ND 3.110 ug/L 09/25/23 12:01 09/26/23 14:46 1bis (2-chloroisopropyl) ether
ND 1.510 ug/L 09/25/23 12:01 09/26/23 14:46 1Phenol
2,4,6-Tribromophenol (Surr)46 30-130 09/26/23 14:46 1
MB MB
Surrogate
09/25/23 12:01
Dil FacPreparedAnalyzedQualifierLimits%Recovery
26 09/25/23 12:01 09/26/23 14:46 12-Fluorophenol (Surr)10-130
16 09/25/23 12:01 09/26/23 14:46 1Phenol-d5 (Surr)8-424
49 09/25/23 12:01 09/26/23 14:46 12-Fluorobiphenyl (Surr)25-130
49 09/25/23 12:01 09/26/23 14:46 1Nitrobenzene-d5 (Surr)15-314
54 09/25/23 12:01 09/26/23 14:46 1Terphenyl-d14 (Surr)35-131
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-799510/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 799589 Prep Batch: 799510
2,4,6-Trichlorophenol 200 133 ug/L 66 37 -144
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2,4-Dichlorophenol 200 127 ug/L 63 39 -135
2,4-Dimethylphenol 200 111 ug/L 55 32 -120
2,4-Dinitrophenol 400 243 ug/L 61 1-191
2-Nitrophenol 200 118 ug/L 59 29 -182
4,6-Dinitro-2-methylphenol 400 313 ug/L 78 1-181
4-Chloro-3-methylphenol 200 140 ug/L 70 22 -147
4-Nitrophenol 400 166 ug/L 41 1-132
Pentachlorophenol 400 298 ug/L 74 14 -176
2-Chlorophenol 200 109 ug/L 55 23 -134
1,2,4-Trichlorobenzene 200 117 ug/L 59 44 -142
1,2-Dichlorobenzene 200 121 ug/L 61 13 -130
1,2-Diphenylhydrazine 200 165 ug/L 83 38 -130
1,3-Dichlorobenzene 200 122 ug/L 61 12 -130
1,4-Dichlorobenzene 200 120 ug/L 60 13 -130
2-Chloronaphthalene 200 136 ug/L 68 60 -120
2,6-Dinitrotoluene 200 156 ug/L 78 50 -158
2,4-Dinitrotoluene 200 162 ug/L 81 39 -139
3,3'-Dichlorobenzidine 200 166 ug/L 83 1-262
4-Bromophenyl phenyl ether 200 137 ug/L 69 53 -127
4-Chlorophenyl phenyl ether 200 141 ug/L 70 25 -158
Acenaphthene 200 149 ug/L 75 47 -145
Acenaphthylene 200 144 ug/L 72 33 -145
Anthracene 200 152 ug/L 76 27 -133
Benzidine 200 45.0 J ug/L 23 1-122
Benzo[a]anthracene 200 160 ug/L 80 33 -143
Benzo[a]pyrene 200 169 ug/L 85 17 -163
Benzo[b]fluoranthene 200 170 ug/L 85 24 -159
Benzo[g,h,i]perylene 200 157 ug/L 79 1-219
Benzo[k]fluoranthene 200 147 ug/L 73 11 -162
Eurofins Raleigh
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QC Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-799510/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 799589 Prep Batch: 799510
Bis(2-chloroethoxy)methane 200 144 ug/L 72 33 -184
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Bis(2-chloroethyl)ether 200 155 ug/L 78 12 -158
Bis(2-ethylhexyl) phthalate 200 172 ug/L 86 8-158
Butyl benzyl phthalate 200 174 ug/L 87 1-152
Chrysene 200 160 ug/L 80 17 -168
Di-n-butyl phthalate 200 167 ug/L 83 1-120
Di-n-octyl phthalate 200 172 ug/L 86 4-146
Dibenz(a,h)anthracene 200 161 ug/L 80 1-227
Diethyl phthalate 200 158 ug/L 79 1-120
Dimethyl phthalate 200 150 ug/L 75 1-120
Fluoranthene 200 154 ug/L 77 26 -137
Fluorene 200 150 ug/L 75 59 -121
Hexachlorobenzene 200 136 ug/L 68 1-152
Hexachlorobutadiene 200 113 ug/L 56 24 -120
Hexachlorocyclopentadiene 200 65.5 ug/L 33 15 -130
Hexachloroethane 200 125 ug/L 62 40 -120
Indeno[1,2,3-cd]pyrene 200 165 ug/L 83 1-171
Isophorone 200 149 ug/L 75 21 -196
N-Nitrosodi-n-propylamine 200 154 ug/L 77 1-230
N-Nitrosodimethylamine 200 116 ug/L 58 15 -130
N-Nitrosodiphenylamine 200 147 ug/L 74 35 -130
Naphthalene 200 130 ug/L 65 21 -133
Nitrobenzene 200 143 ug/L 72 35 -180
Phenanthrene 200 152 ug/L 76 54 -120
Pyrene 200 163 ug/L 82 52 -120
bis (2-chloroisopropyl) ether 200 163 ug/L 82 30 -104
Phenol 200 60.9 ug/L 30 5-120
2,4,6-Tribromophenol (Surr)30 -130
Surrogate
69
LCS LCS
Qualifier Limits%Recovery
332-Fluorophenol (Surr)10 -130
24Phenol-d5 (Surr)8 -424
632-Fluorobiphenyl (Surr)25 -130
68Nitrobenzene-d5 (Surr)15 -314
73Terphenyl-d14 (Surr)35 -131
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-799510/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 799589 Prep Batch: 799510
2,4,6-Trichlorophenol 200 100 ug/L 50 37 -144 28 58
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
2,4-Dichlorophenol 200 94.4 ug/L 47 39 -135 29 50
2,4-Dimethylphenol 200 85.3 ug/L 43 32 -120 26 58
2,4-Dinitrophenol 400 217 ug/L 54 1-191 11 132
2-Nitrophenol 200 92.2 ug/L 46 29 -182 25 55
4,6-Dinitro-2-methylphenol 400 253 ug/L 63 1-181 21 203
4-Chloro-3-methylphenol 200 102 ug/L 51 22 -147 32 73
Eurofins Raleigh
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QC Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-799510/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 799589 Prep Batch: 799510
4-Nitrophenol 400 126 ug/L 32 1-132 27 131
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Pentachlorophenol 400 232 ug/L 58 14 -176 25 86
2-Chlorophenol 200 85.9 ug/L 43 23 -134 24 61
1,2,4-Trichlorobenzene 200 87.3 ug/L 44 44 -142 29 50
1,2-Dichlorobenzene 200 88.7 ug/L 44 13 -130 31 46
1,2-Diphenylhydrazine 200 124 ug/L 62 38 -130 29 41
1,3-Dichlorobenzene 200 87.8 ug/L 44 12 -130 33 49
1,4-Dichlorobenzene 200 86.9 ug/L 43 13 -130 32 46
2-Chloronaphthalene 200 100 *- *1 ug/L 50 60 -120 30 24
2,6-Dinitrotoluene 200 110 ug/L 55 50 -158 35 53
2,4-Dinitrotoluene 200 114 ug/L 57 39 -139 34 42
3,3'-Dichlorobenzidine 200 125 ug/L 62 1-262 28 108
4-Bromophenyl phenyl ether 200 100 *-ug/L 50 53 -127 31 43
4-Chlorophenyl phenyl ether 200 101 ug/L 50 25 -158 33 61
Acenaphthene 200 108 ug/L 54 47 -145 32 48
Acenaphthylene 200 103 ug/L 52 33 -145 33 74
Anthracene 200 114 ug/L 57 27 -133 29 66
Benzidine 200 62.1 J ug/L 31 1-122 32 131
Benzo[a]anthracene 200 118 ug/L 59 33 -143 30 53
Benzo[a]pyrene 200 123 ug/L 61 17 -163 32 72
Benzo[b]fluoranthene 200 113 ug/L 57 24 -159 40 71
Benzo[g,h,i]perylene 200 117 ug/L 59 1-219 29 97
Benzo[k]fluoranthene 200 117 ug/L 59 11 -162 22 63
Bis(2-chloroethoxy)methane 200 105 ug/L 52 33 -184 32 54
Bis(2-chloroethyl)ether 200 103 ug/L 52 12 -158 40 108
Bis(2-ethylhexyl) phthalate 200 126 ug/L 63 8-158 31 82
Butyl benzyl phthalate 200 128 ug/L 64 1-152 30 60
Chrysene 200 119 ug/L 60 17 -168 29 87
Di-n-butyl phthalate 200 122 ug/L 61 1-120 31 47
Di-n-octyl phthalate 200 126 ug/L 63 4-146 30 69
Dibenz(a,h)anthracene 200 117 ug/L 58 1-227 32 126
Diethyl phthalate 200 114 ug/L 57 1-120 33 100
Dimethyl phthalate 200 108 ug/L 54 1-120 33 183
Fluoranthene 200 115 ug/L 57 26 -137 29 66
Fluorene 200 106 *-ug/L 53 59 -121 34 38
Hexachlorobenzene 200 99.6 ug/L 50 1-152 31 55
Hexachlorobutadiene 200 84.9 ug/L 42 24 -120 28 62
Hexachlorocyclopentadiene 200 50.6 ug/L 25 15 -130 26 47
Hexachloroethane 200 93.1 ug/L 47 40 -120 29 52
Indeno[1,2,3-cd]pyrene 200 122 ug/L 61 1-171 31 99
Isophorone 200 106 ug/L 53 21 -196 34 93
N-Nitrosodi-n-propylamine 200 110 ug/L 55 1-230 34 87
N-Nitrosodimethylamine 200 87.6 ug/L 44 15 -130 28 50
N-Nitrosodiphenylamine 200 109 ug/L 54 35 -130 30 39
Naphthalene 200 95.4 ug/L 48 21 -133 31 65
Nitrobenzene 200 105 ug/L 53 35 -180 31 62
Phenanthrene 200 112 ug/L 56 54 -120 30 39
Pyrene 200 118 ug/L 59 52 -120 32 49
bis (2-chloroisopropyl) ether 200 116 ug/L 58 30 -104 34 42
Eurofins Raleigh
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QC Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-799510/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 799589 Prep Batch: 799510
Phenol 200 48.6 ug/L 24 5-120 22 64
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
2,4,6-Tribromophenol (Surr)30 -130
Surrogate
49
LCSD LCSD
Qualifier Limits%Recovery
282-Fluorophenol (Surr)10 -130
21Phenol-d5 (Surr)8 -424
462-Fluorobiphenyl (Surr)25 -130
51Nitrobenzene-d5 (Surr)15 -314
57Terphenyl-d14 (Surr)35 -131
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
Client Sample ID: Method BlankLab Sample ID: MB 680-799722/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 799722
RL MDL
Gasoline Range Organics
(GRO)-C6-C10
ND 10 2.5 mg/Kg 09/26/23 15:26 100
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
a,a,a-Trifluorotoluene 92 70-131 09/26/23 15:26 100
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-799722/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 799722
Gasoline Range Organics
(GRO)-C6-C10
50.0 50.4 mg/Kg 101 64 -133
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
a,a,a-Trifluorotoluene 70 -131
Surrogate
127
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-799722/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 799722
Gasoline Range Organics
(GRO)-C6-C10
50.0 48.3 mg/Kg 97 64 -133 4 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
a,a,a-Trifluorotoluene 70 -131
Surrogate
124
LCSD LCSD
Qualifier Limits%Recovery
Eurofins Raleigh
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QC Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
(Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-799893/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 799893
RL MDL
Gasoline Range Organics
(GRO)-C6-C10
ND 10 2.5 mg/Kg 09/27/23 13:50 100
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
a,a,a-Trifluorotoluene 90 70-131 09/27/23 13:50 100
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-799893/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 799893
Gasoline Range Organics
(GRO)-C6-C10
50.0 53.0 mg/Kg 106 64 -133
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
a,a,a-Trifluorotoluene 70 -131
Surrogate
118
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-799893/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 799893
Gasoline Range Organics
(GRO)-C6-C10
50.0 52.0 mg/Kg 104 64 -133 2 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
a,a,a-Trifluorotoluene 70 -131
Surrogate
121
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 680-800868/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 800868
RL MDL
Gasoline Range Organics
(GRO)-C6-C10
ND 10 2.5 mg/Kg 10/03/23 21:44 100
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
a,a,a-Trifluorotoluene 89 70-131 10/03/23 21:44 100
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-800868/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 800868
Gasoline Range Organics
(GRO)-C6-C10
50.0 50.0 mg/Kg 100 64 -133
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Eurofins Raleigh
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QC Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)
(Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-800868/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 800868
a,a,a-Trifluorotoluene 70 -131
Surrogate
116
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-800868/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 800868
Gasoline Range Organics
(GRO)-C6-C10
50.0 49.7 mg/Kg 99 64 -133 1 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
a,a,a-Trifluorotoluene 70 -131
Surrogate
116
LCSD LCSD
Qualifier Limits%Recovery
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 400-644204/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 644204
RL MDL
C5-C8 Aliphatics ND 26 26 ug/L 10/05/23 14:01 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1111 ug/L 10/05/23 14:01 1C9-C12 Aliphatics
ND 7.07.0 ug/L 10/05/23 14:01 1C9-C10 Aromatics
a,a,a-Trifluorotoluene (fid)97 70-130 10/05/23 14:01 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
96 10/05/23 14:01 1a,a,a-Trifluorotoluene (pid)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-644204/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 644204
C5-C8 Aliphatics 300 344 ug/L 115 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C12 Aliphatics 350 385 ug/L 110 70 -130
C9-C10 Aromatics 50.0 54.8 ug/L 110 70 -130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
97
LCS LCS
Qualifier Limits%Recovery
102a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-644204/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 644204
C5-C8 Aliphatics 300 317 ug/L 106 70 -130 8 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Eurofins Raleigh
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QC Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-644204/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 644204
C9-C12 Aliphatics 350 320 ug/L 92 70 -130 18 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C10 Aromatics 50.0 45.0 ug/L 90 70 -130 20 25
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
97
LCSD LCSD
Qualifier Limits%Recovery
101a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Matrix SpikeLab Sample ID: 400-244015-D-4 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 644204
C5-C8 Aliphatics ND 300 331 ug/L 110 70 -130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
C9-C12 Aliphatics ND 350 314 ug/L 90 70 -130
C9-C10 Aromatics ND 50.0 56.9 ug/L 114 70 -130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
96
MS MS
Qualifier Limits%Recovery
101a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 400-244015-D-4 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 644204
C5-C8 Aliphatics ND 300 341 ug/L 114 70 -130 3 25
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
C9-C12 Aliphatics ND 350 327 ug/L 93 70 -130 4 25
C9-C10 Aromatics ND 50.0 63.0 ug/L 126 70 -130 10 25
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
97
MSD MSD
Qualifier Limits%Recovery
101a,a,a-Trifluorotoluene (pid)70 -130
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
Client Sample ID: Method BlankLab Sample ID: MB 680-799570/16-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 799752 Prep Batch: 799570
RL MDL
Diesel Range Organics [C10-C28]ND 7.9 2.6 mg/Kg 09/25/23 17:58 09/26/23 16:22 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
o-Terphenyl (Surr)82 15-139 09/26/23 16:22 1
MB MB
Surrogate
09/25/23 17:58
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Eurofins Raleigh
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QC Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
(Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-799570/17-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 799752 Prep Batch: 799570
Diesel Range Organics
[C10-C28]
32.4 28.0 mg/Kg 87 26 -133
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
o-Terphenyl (Surr)15 -139
Surrogate
101
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Matrix SpikeLab Sample ID: 680-240669-A-1-B MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 799752 Prep Batch: 799570
Diesel Range Organics
[C10-C28]
8.9 J 38.8 43.0 mg/Kg 88 26 -133☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
o-Terphenyl (Surr)15 -139
Surrogate
88
MS MS
Qualifier Limits%Recovery
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 680-240669-A-1-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 799752 Prep Batch: 799570
Diesel Range Organics
[C10-C28]
8.9 J 38.7 43.5 mg/Kg 89 26 -133 1 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
o-Terphenyl (Surr)15 -139
Surrogate
91
MSD MSD
Qualifier Limits%Recovery
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 400-642868/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 643169 Prep Batch: 642868
RL MDL
C11-C22 Aromatics ND 0.31 0.31 mg/L 09/26/23 22:21 09/29/23 06:14 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
o-Terphenyl 64 40-140 09/29/23 06:14 1
MB MB
Surrogate
09/26/23 22:21
Dil FacPreparedAnalyzedQualifierLimits%Recovery
65 09/26/23 22:21 09/29/23 06:14 12-Fluorobiphenyl 40-140
52 09/26/23 22:21 09/29/23 06:14 12-Bromonaphthalene 40-140
Eurofins Raleigh
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QC Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-642868/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 643374 Prep Batch: 642868
RL MDL
C9-C18 Aliphatics ND 0.15 0.15 mg/L 09/26/23 22:21 10/02/23 12:24 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.150.15 mg/L 09/26/23 22:21 10/02/23 12:24 1C19-C36 Aliphatics
1-Chlorooctadecane 74 40-140 10/02/23 12:24 1
MB MB
Surrogate
09/26/23 22:21
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-642868/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 643169 Prep Batch: 642868
C11-C22 Aromatics 3.86 3.40 mg/L 88 40 -140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
o-Terphenyl 40 -140
Surrogate
59
LCS LCS
Qualifier Limits%Recovery
682-Fluorobiphenyl 40 -140
982-Bromonaphthalene 40 -140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-642868/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 643374 Prep Batch: 642868
C9-C18 Aliphatics 1.36 1.46 mg/L 107 40 -140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C19-C36 Aliphatics 1.82 1.68 mg/L 93 40 -140
1-Chlorooctadecane 40 -140
Surrogate
73
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-642868/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 643169 Prep Batch: 642868
C11-C22 Aromatics 3.86 4.01 mg/L 104 40 -140 16 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
o-Terphenyl 40 -140
Surrogate
74
LCSD LCSD
Qualifier Limits%Recovery
762-Fluorobiphenyl 40 -140
1072-Bromonaphthalene 40 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-642868/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 643374 Prep Batch: 642868
C9-C18 Aliphatics 1.36 1.50 mg/L 110 40 -140 3 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Eurofins Raleigh
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QC Sample Results
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-642868/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 643374 Prep Batch: 642868
C19-C36 Aliphatics 1.82 1.81 mg/L 99 40 -140 7 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1-Chlorooctadecane 40 -140
Surrogate
73
LCSD LCSD
Qualifier Limits%Recovery
Eurofins Raleigh
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QC Association Summary
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
GC/MS VOA
Analysis Batch: 4657
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM6200-B752-11855-21 TMW-1 Total/NA
Water SM6200-BMB 752-4657/10 Method Blank Total/NA
Water SM6200-BLCS 752-4657/6 Lab Control Sample Total/NA
Water SM6200-BLCS 752-4657/8 Lab Control Sample Total/NA
Water SM6200-BLCSD 752-4657/7 Lab Control Sample Dup Total/NA
Water SM6200-BMRL 752-4657/17 Lab Control Sample Total/NA
Water SM6200-BMRL 752-4657/5 Lab Control Sample Total/NA
GC/MS Semi VOA
Prep Batch: 799510
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water CWA_Prep752-11855-21 TMW-1 Total/NA
Water CWA_Prep752-11855-21 - DL TMW-1 Total/NA
Water CWA_PrepMB 680-799510/1-A Method Blank Total/NA
Water CWA_PrepLCS 680-799510/2-A Lab Control Sample Total/NA
Water CWA_PrepLCSD 680-799510/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 799589
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 625.1 799510752-11855-21 TMW-1 Total/NA
Water 625.1 799510MB 680-799510/1-A Method Blank Total/NA
Water 625.1 799510LCS 680-799510/2-A Lab Control Sample Total/NA
Water 625.1 799510LCSD 680-799510/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 799910
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 625.1 799510752-11855-21 - DL TMW-1 Total/NA
GC VOA
Analysis Batch: 644204
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MAVPH752-11855-21 TMW-1 Total/NA
Water MAVPHMB 400-644204/2 Method Blank Total/NA
Water MAVPHLCS 400-644204/4 Lab Control Sample Total/NA
Water MAVPHLCSD 400-644204/5 Lab Control Sample Dup Total/NA
Water MAVPH400-244015-D-4 MS Matrix Spike Total/NA
Water MAVPH400-244015-D-4 MSD Matrix Spike Duplicate Total/NA
Prep Batch: 799671
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 5035A752-11855-1 S-1 Total/NA
Soil 5035A752-11855-2 S-2 Total/NA
Soil 5035A752-11855-3 S-3 Total/NA
Soil 5035A752-11855-4 S-4 Total/NA
Soil 5035A752-11855-5 S-5 Total/NA
Soil 5035A752-11855-6 S-6 Total/NA
Soil 5035A752-11855-7 S-7 Total/NA
Soil 5035A752-11855-8 S-8 Total/NA
Soil 5035A752-11855-9 S-9 Total/NA
Soil 5035A752-11855-10 S-10 Total/NA
Eurofins Raleigh
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QC Association Summary
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
GC VOA (Continued)
Prep Batch: 799671 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 5035A752-11855-11 S-11 Total/NA
Soil 5035A752-11855-12 S-12 Total/NA
Soil 5035A752-11855-13 S-13 Total/NA
Soil 5035A752-11855-14 S-14 Total/NA
Soil 5035A752-11855-15 S-15 Total/NA
Soil 5035A752-11855-16 S-16 Total/NA
Soil 5035A752-11855-17 S-17 Total/NA
Soil 5035A752-11855-18 S-18 Total/NA
Soil 5035A752-11855-19 S-19 Total/NA
Soil 5035A752-11855-20 S-20 Total/NA
Analysis Batch: 799722
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8015C 799671752-11855-1 S-1 Total/NA
Soil 8015C 799671752-11855-3 S-3 Total/NA
Soil 8015C 799671752-11855-4 S-4 Total/NA
Soil 8015C 799671752-11855-5 S-5 Total/NA
Soil 8015C 799671752-11855-6 S-6 Total/NA
Soil 8015C 799671752-11855-7 S-7 Total/NA
Soil 8015C 799671752-11855-8 S-8 Total/NA
Soil 8015C 799671752-11855-9 S-9 Total/NA
Soil 8015C 799671752-11855-10 S-10 Total/NA
Soil 8015C 799671752-11855-11 S-11 Total/NA
Soil 8015C 799671752-11855-12 S-12 Total/NA
Soil 8015C 799671752-11855-20 S-20 Total/NA
Solid 8015CMB 680-799722/8 Method Blank Total/NA
Solid 8015CLCS 680-799722/6 Lab Control Sample Total/NA
Solid 8015CLCSD 680-799722/7 Lab Control Sample Dup Total/NA
Analysis Batch: 799893
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8015C 799671752-11855-13 S-13 Total/NA
Soil 8015C 799671752-11855-14 S-14 Total/NA
Soil 8015C 799671752-11855-15 S-15 Total/NA
Soil 8015C 799671752-11855-16 S-16 Total/NA
Soil 8015C 799671752-11855-17 S-17 Total/NA
Soil 8015C 799671752-11855-18 S-18 Total/NA
Soil 8015C 799671752-11855-19 S-19 Total/NA
Solid 8015CMB 680-799893/7 Method Blank Total/NA
Solid 8015CLCS 680-799893/5 Lab Control Sample Total/NA
Solid 8015CLCSD 680-799893/6 Lab Control Sample Dup Total/NA
Analysis Batch: 800868
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8015C 799671752-11855-2 S-2 Total/NA
Solid 8015CMB 680-800868/7 Method Blank Total/NA
Solid 8015CLCS 680-800868/5 Lab Control Sample Total/NA
Solid 8015CLCSD 680-800868/6 Lab Control Sample Dup Total/NA
Eurofins Raleigh
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QC Association Summary
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
GC Semi VOA
Prep Batch: 642868
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3511752-11855-21 TMW-1 Total/NA
Water 3511MB 400-642868/1-A Method Blank Total/NA
Water 3511LCS 400-642868/2-A Lab Control Sample Total/NA
Water 3511LCSD 400-642868/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 643169
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA-EPH 642868752-11855-21 TMW-1 Total/NA
Water MA-EPH 642868MB 400-642868/1-A Method Blank Total/NA
Water MA-EPH 642868LCS 400-642868/2-A Lab Control Sample Total/NA
Water MA-EPH 642868LCSD 400-642868/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 643374
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA-EPH 642868752-11855-21 TMW-1 Total/NA
Water MA-EPH 642868MB 400-642868/1-A Method Blank Total/NA
Water MA-EPH 642868LCS 400-642868/2-A Lab Control Sample Total/NA
Water MA-EPH 642868LCSD 400-642868/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 643938
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA-EPH 642868752-11855-21 TMW-1 Total/NA
Prep Batch: 799570
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 3546752-11855-1 S-1 Total/NA
Soil 3546752-11855-2 S-2 Total/NA
Soil 3546752-11855-3 S-3 Total/NA
Soil 3546752-11855-4 S-4 Total/NA
Soil 3546752-11855-14 S-14 Total/NA
Solid 3546MB 680-799570/16-A Method Blank Total/NA
Solid 3546LCS 680-799570/17-A Lab Control Sample Total/NA
Solid 3546680-240669-A-1-B MS Matrix Spike Total/NA
Solid 3546680-240669-A-1-C MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 799752
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8015C 799570752-11855-1 S-1 Total/NA
Soil 8015C 799570752-11855-2 S-2 Total/NA
Soil 8015C 799570752-11855-3 S-3 Total/NA
Soil 8015C 799570752-11855-4 S-4 Total/NA
Soil 8015C 799570752-11855-14 S-14 Total/NA
Solid 8015C 799570MB 680-799570/16-A Method Blank Total/NA
Solid 8015C 799570LCS 680-799570/17-A Lab Control Sample Total/NA
Solid 8015C 799570680-240669-A-1-B MS Matrix Spike Total/NA
Solid 8015C 799570680-240669-A-1-C MSD Matrix Spike Duplicate Total/NA
Eurofins Raleigh
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QC Association Summary
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
General Chemistry
Analysis Batch: 799641
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil Moisture752-11855-1 S-1 Total/NA
Soil Moisture752-11855-2 S-2 Total/NA
Soil Moisture752-11855-3 S-3 Total/NA
Soil Moisture752-11855-4 S-4 Total/NA
Soil Moisture752-11855-5 S-5 Total/NA
Soil Moisture752-11855-6 S-6 Total/NA
Soil Moisture752-11855-7 S-7 Total/NA
Soil Moisture752-11855-8 S-8 Total/NA
Soil Moisture752-11855-9 S-9 Total/NA
Soil Moisture752-11855-10 S-10 Total/NA
Soil Moisture752-11855-11 S-11 Total/NA
Soil Moisture752-11855-12 S-12 Total/NA
Soil Moisture752-11855-13 S-13 Total/NA
Soil Moisture752-11855-14 S-14 Total/NA
Soil Moisture752-11855-15 S-15 Total/NA
Soil Moisture752-11855-16 S-16 Total/NA
Soil Moisture752-11855-17 S-17 Total/NA
Soil Moisture752-11855-18 S-18 Total/NA
Soil Moisture752-11855-19 S-19 Total/NA
Soil Moisture752-11855-20 S-20 Total/NA
Eurofins Raleigh
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Lab Chronicle
Client: East Coast Environmental Job ID: 752-11855-1
Project/Site: 2210 US 1
Client Sample ID: S-1 Lab Sample ID: 752-11855-1
Matrix: SoilDate Collected: 09/20/23 10:30
Date Received: 09/22/23 12:36
Analysis Moisture KG09/26/23 10:001 EET SAV799641
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: S-1 Lab Sample ID: 752-11855-1
Matrix: SoilDate Collected: 09/20/23 10:30
Percent Solids: 86.5Date Received: 09/22/23 12:36
Prep 5035A FES09/26/23 10:23 EET SAV799671
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.491 g 5 mL
Analysis 8015C 100 799722 09/26/23 16:09 DBM EET SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Prep 3546 799570 09/25/23 17:58 PB EET SAVTotal/NA 30.32 g 1 mL
Analysis 8015C 1 799752 09/26/23 20:05 DBM EET SAVTotal/NA 1 mL 1 mL
CSGQInstrument ID:
Client Sample ID: S-2 Lab Sample ID: 752-11855-2
Matrix: SoilDate Collected: 09/20/23 10:35
Date Received: 09/22/23 12:36
Analysis Moisture KG09/26/23 10:001 EET SAV799641
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: S-2 Lab Sample ID: 752-11855-2
Matrix: SoilDate Collected: 09/20/23 10:35
Percent Solids: 90.4Date Received: 09/22/23 12:36
Prep 5035A FES09/26/23 10:23 EET SAV799671
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.822 g 5 mL
Analysis 8015C 100 800868 10/03/23 23:53 DBM EET SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Prep 3546 799570 09/25/23 17:58 PB EET SAVTotal/NA 30.30 g 1 mL
Analysis 8015C 1 799752 09/26/23 20:24 DBM EET SAVTotal/NA 1 mL 1 mL
CSGQInstrument ID:
Client Sample ID: S-3 Lab Sample ID: 752-11855-3
Matrix: SoilDate Collected: 09/20/23 10:40
Date Received: 09/22/23 12:36
Analysis Moisture KG09/26/23 10:001 EET SAV799641
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Eurofins Raleigh
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Lab Chronicle
Client: East Coast Environmental Job ID: 752-11855-1
Project/Site: 2210 US 1
Client Sample ID: S-3 Lab Sample ID: 752-11855-3
Matrix: SoilDate Collected: 09/20/23 10:40
Percent Solids: 94.3Date Received: 09/22/23 12:36
Prep 5035A FES09/26/23 10:23 EET SAV799671
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.898 g 5 mL
Analysis 8015C 100 799722 09/26/23 16:52 DBM EET SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Prep 3546 799570 09/25/23 17:58 PB EET SAVTotal/NA 30.70 g 1 mL
Analysis 8015C 1 799752 09/26/23 20:43 DBM EET SAVTotal/NA 1 mL 1 mL
CSGQInstrument ID:
Client Sample ID: S-4 Lab Sample ID: 752-11855-4
Matrix: SoilDate Collected: 09/20/23 10:45
Date Received: 09/22/23 12:36
Analysis Moisture KG09/26/23 10:001 EET SAV799641
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: S-4 Lab Sample ID: 752-11855-4
Matrix: SoilDate Collected: 09/20/23 10:45
Percent Solids: 86.9Date Received: 09/22/23 12:36
Prep 5035A FES09/26/23 10:23 EET SAV799671
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.014 g 5 mL
Analysis 8015C 100 799722 09/26/23 17:13 DBM EET SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Prep 3546 799570 09/25/23 17:58 PB EET SAVTotal/NA 30.71 g 1 mL
Analysis 8015C 1 799752 09/26/23 21:01 DBM EET SAVTotal/NA 1 mL 1 mL
CSGQInstrument ID:
Client Sample ID: S-5 Lab Sample ID: 752-11855-5
Matrix: SoilDate Collected: 09/20/23 10:50
Date Received: 09/22/23 12:36
Analysis Moisture KG09/26/23 10:001 EET SAV799641
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: S-5 Lab Sample ID: 752-11855-5
Matrix: SoilDate Collected: 09/20/23 10:50
Percent Solids: 88.6Date Received: 09/22/23 12:36
Prep 5035A FES09/26/23 10:23 EET SAV799671
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6 g 5 mL
Analysis 8015C 100 799722 09/26/23 17:34 DBM EET SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Eurofins Raleigh
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Lab Chronicle
Client: East Coast Environmental Job ID: 752-11855-1
Project/Site: 2210 US 1
Client Sample ID: S-6 Lab Sample ID: 752-11855-6
Matrix: SoilDate Collected: 09/20/23 10:55
Date Received: 09/22/23 12:36
Analysis Moisture KG09/26/23 10:001 EET SAV799641
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: S-6 Lab Sample ID: 752-11855-6
Matrix: SoilDate Collected: 09/20/23 10:55
Percent Solids: 93.0Date Received: 09/22/23 12:36
Prep 5035A FES09/26/23 10:23 EET SAV799671
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.869 g 5 mL
Analysis 8015C 100 799722 09/26/23 17:56 DBM EET SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: S-7 Lab Sample ID: 752-11855-7
Matrix: SoilDate Collected: 09/20/23 11:00
Date Received: 09/22/23 12:36
Analysis Moisture KG09/26/23 10:001 EET SAV799641
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: S-7 Lab Sample ID: 752-11855-7
Matrix: SoilDate Collected: 09/20/23 11:00
Percent Solids: 95.0Date Received: 09/22/23 12:36
Prep 5035A FES09/26/23 10:23 EET SAV799671
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 3.176 g 5 mL
Analysis 8015C 100 799722 09/26/23 18:17 DBM EET SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: S-8 Lab Sample ID: 752-11855-8
Matrix: SoilDate Collected: 09/20/23 11:05
Date Received: 09/22/23 12:36
Analysis Moisture KG09/26/23 10:001 EET SAV799641
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: S-8 Lab Sample ID: 752-11855-8
Matrix: SoilDate Collected: 09/20/23 11:05
Percent Solids: 78.4Date Received: 09/22/23 12:36
Prep 5035A FES09/26/23 10:23 EET SAV799671
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.917 g 5 mL
Analysis 8015C 100 799722 09/26/23 18:39 DBM EET SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Eurofins Raleigh
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Lab Chronicle
Client: East Coast Environmental Job ID: 752-11855-1
Project/Site: 2210 US 1
Client Sample ID: S-9 Lab Sample ID: 752-11855-9
Matrix: SoilDate Collected: 09/20/23 11:10
Date Received: 09/22/23 12:36
Analysis Moisture KG09/26/23 10:001 EET SAV799641
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: S-9 Lab Sample ID: 752-11855-9
Matrix: SoilDate Collected: 09/20/23 11:10
Percent Solids: 94.3Date Received: 09/22/23 12:36
Prep 5035A FES09/26/23 10:23 EET SAV799671
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.639 g 5 mL
Analysis 8015C 100 799722 09/26/23 19:00 DBM EET SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: S-10 Lab Sample ID: 752-11855-10
Matrix: SoilDate Collected: 09/20/23 11:15
Date Received: 09/22/23 12:36
Analysis Moisture KG09/26/23 10:001 EET SAV799641
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: S-10 Lab Sample ID: 752-11855-10
Matrix: SoilDate Collected: 09/20/23 11:15
Percent Solids: 94.0Date Received: 09/22/23 12:36
Prep 5035A FES09/26/23 10:23 EET SAV799671
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.997 g 5 mL
Analysis 8015C 100 799722 09/26/23 19:22 DBM EET SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: S-11 Lab Sample ID: 752-11855-11
Matrix: SoilDate Collected: 09/20/23 11:20
Date Received: 09/22/23 12:36
Analysis Moisture KG09/26/23 10:001 EET SAV799641
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: S-11 Lab Sample ID: 752-11855-11
Matrix: SoilDate Collected: 09/20/23 11:20
Percent Solids: 83.3Date Received: 09/22/23 12:36
Prep 5035A FES09/26/23 10:23 EET SAV799671
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.079 g 5 mL
Analysis 8015C 100 799722 09/26/23 19:43 DBM EET SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Eurofins Raleigh
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Lab Chronicle
Client: East Coast Environmental Job ID: 752-11855-1
Project/Site: 2210 US 1
Client Sample ID: S-12 Lab Sample ID: 752-11855-12
Matrix: SoilDate Collected: 09/20/23 11:25
Date Received: 09/22/23 12:36
Analysis Moisture KG09/26/23 10:001 EET SAV799641
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: S-12 Lab Sample ID: 752-11855-12
Matrix: SoilDate Collected: 09/20/23 11:25
Percent Solids: 81.5Date Received: 09/22/23 12:36
Prep 5035A FES09/26/23 10:23 EET SAV799671
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 7.355 g 5 mL
Analysis 8015C 100 799722 09/26/23 20:05 DBM EET SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: S-13 Lab Sample ID: 752-11855-13
Matrix: SoilDate Collected: 09/20/23 11:30
Date Received: 09/22/23 12:36
Analysis Moisture KG09/26/23 10:001 EET SAV799641
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: S-13 Lab Sample ID: 752-11855-13
Matrix: SoilDate Collected: 09/20/23 11:30
Percent Solids: 92.6Date Received: 09/22/23 12:36
Prep 5035A FES09/26/23 10:23 EET SAV799671
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.435 g 5 mL
Analysis 8015C 20000 799893 09/27/23 17:02 DBM EET SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: S-14 Lab Sample ID: 752-11855-14
Matrix: SoilDate Collected: 09/20/23 11:45
Date Received: 09/22/23 12:36
Analysis Moisture KG09/26/23 10:001 EET SAV799641
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: S-14 Lab Sample ID: 752-11855-14
Matrix: SoilDate Collected: 09/20/23 11:45
Percent Solids: 91.6Date Received: 09/22/23 12:36
Prep 5035A FES09/26/23 10:23 EET SAV799671
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.776 g 5 mL
Analysis 8015C 100 799893 09/27/23 17:23 DBM EET SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Eurofins Raleigh
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Lab Chronicle
Client: East Coast Environmental Job ID: 752-11855-1
Project/Site: 2210 US 1
Client Sample ID: S-14 Lab Sample ID: 752-11855-14
Matrix: SoilDate Collected: 09/20/23 11:45
Percent Solids: 91.6Date Received: 09/22/23 12:36
Prep 3546 PB09/25/23 17:58 EET SAV799570
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.26 g 1 mL
Analysis 8015C 1 799752 09/26/23 21:20 DBM EET SAVTotal/NA 1 mL 1 mL
CSGQInstrument ID:
Client Sample ID: S-15 Lab Sample ID: 752-11855-15
Matrix: SoilDate Collected: 09/20/23 15:00
Date Received: 09/22/23 12:36
Analysis Moisture KG09/26/23 10:001 EET SAV799641
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: S-15 Lab Sample ID: 752-11855-15
Matrix: SoilDate Collected: 09/20/23 15:00
Percent Solids: 89.1Date Received: 09/22/23 12:36
Prep 5035A FES09/26/23 10:23 EET SAV799671
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.312 g 5 mL
Analysis 8015C 100 799893 09/27/23 16:19 DBM EET SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: S-16 Lab Sample ID: 752-11855-16
Matrix: SoilDate Collected: 09/20/23 15:10
Date Received: 09/22/23 12:36
Analysis Moisture KG09/26/23 10:001 EET SAV799641
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: S-16 Lab Sample ID: 752-11855-16
Matrix: SoilDate Collected: 09/20/23 15:10
Percent Solids: 91.4Date Received: 09/22/23 12:36
Prep 5035A FES09/26/23 10:23 EET SAV799671
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.684 g 5 mL
Analysis 8015C 100 799893 09/27/23 15:58 DBM EET SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: S-17 Lab Sample ID: 752-11855-17
Matrix: SoilDate Collected: 09/20/23 16:00
Date Received: 09/22/23 12:36
Analysis Moisture KG09/26/23 10:001 EET SAV799641
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Eurofins Raleigh
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Lab Chronicle
Client: East Coast Environmental Job ID: 752-11855-1
Project/Site: 2210 US 1
Client Sample ID: S-17 Lab Sample ID: 752-11855-17
Matrix: SoilDate Collected: 09/20/23 16:00
Percent Solids: 96.1Date Received: 09/22/23 12:36
Prep 5035A FES09/26/23 10:23 EET SAV799671
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.882 g 5 mL
Analysis 8015C 100 799893 09/27/23 15:37 DBM EET SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: S-18 Lab Sample ID: 752-11855-18
Matrix: SoilDate Collected: 09/20/23 16:10
Date Received: 09/22/23 12:36
Analysis Moisture KG09/26/23 10:001 EET SAV799641
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: S-18 Lab Sample ID: 752-11855-18
Matrix: SoilDate Collected: 09/20/23 16:10
Percent Solids: 92.5Date Received: 09/22/23 12:36
Prep 5035A FES09/26/23 10:23 EET SAV799671
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.22 g 5 mL
Analysis 8015C 100 799893 09/27/23 15:15 DBM EET SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: S-19 Lab Sample ID: 752-11855-19
Matrix: SoilDate Collected: 09/20/23 16:30
Date Received: 09/22/23 12:36
Analysis Moisture KG09/26/23 10:001 EET SAV799641
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: S-19 Lab Sample ID: 752-11855-19
Matrix: SoilDate Collected: 09/20/23 16:30
Percent Solids: 91.0Date Received: 09/22/23 12:36
Prep 5035A FES09/26/23 10:23 EET SAV799671
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.462 g 5 mL
Analysis 8015C 100 799893 09/27/23 14:53 DBM EET SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: S-20 Lab Sample ID: 752-11855-20
Matrix: SoilDate Collected: 09/20/23 16:45
Date Received: 09/22/23 12:36
Analysis Moisture KG09/26/23 10:001 EET SAV799641
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Eurofins Raleigh
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Lab Chronicle
Client: East Coast Environmental Job ID: 752-11855-1
Project/Site: 2210 US 1
Client Sample ID: S-20 Lab Sample ID: 752-11855-20
Matrix: SoilDate Collected: 09/20/23 16:45
Percent Solids: 79.8Date Received: 09/22/23 12:36
Prep 5035A FES09/26/23 10:23 EET SAV799671
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.677 g 5 mL
Analysis 8015C 100 799722 09/26/23 22:56 DBM EET SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: TMW-1 Lab Sample ID: 752-11855-21
Matrix: WaterDate Collected: 09/21/23 10:00
Date Received: 09/22/23 12:36
Analysis SM6200-B RY10/02/23 21:481000 EET ESC4657
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:CVGCMS4
Prep CWA_Prep 799510 09/25/23 12:01 RR EET SAVTotal/NA 556.9 mL 1 mL
Analysis 625.1 1 799589 09/26/23 19:08 OK EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Prep CWA_Prep DL 799510 09/25/23 12:01 RR EET SAVTotal/NA 556.9 mL 1 mL
Analysis 625.1 DL 50 799910 09/27/23 21:52 OK EET SAVTotal/NA 1 mL 1 mL
CMSNInstrument ID:
Analysis MAVPH 500 644204 10/05/23 16:41 SRK EET PENTotal/NA 5 mL 5 mL
TiffanyInstrument ID:
Prep 3511 642868 09/26/23 22:21 JTC EET PENTotal/NA 56.8 mL 2 mL
Analysis MA-EPH 1 643169 09/29/23 07:54 MP EET PENTotal/NA
EvaInstrument ID:
Prep 3511 642868 09/26/23 22:21 JTC EET PENTotal/NA 56.8 mL 2 mL
Analysis MA-EPH 1 643374 10/02/23 13:16 MP EET PENTotal/NA 1 mL 1 mL
WALLEInstrument ID:
Prep 3511 642868 09/26/23 22:21 JTC EET PENTotal/NA 56.8 mL 2 mL
Analysis MA-EPH 5 643938 10/04/23 15:20 MP EET PENTotal/NA 1 mL 1 mL
WALLEInstrument ID:
Laboratory References:
EET ESC = Eurofins Raleigh, 102-A Woodwinds Industrial Court, Cary, NC 27511, TEL [phone]
EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Raleigh
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Accreditation/Certification Summary
Client: East Coast Environmental Job ID: 752-11855-1
Project/Site: 2210 US 1
Laboratory: Eurofins Raleigh
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 591 12-31-23
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
SM6200-B Water Freon 113
SM6200-B Water tert-Amyl alcohol
SM6200-B Water Tert-amyl methyl ether
SM6200-B Water tert-Butyl alcohol
SM6200-B Water Tert-butyl ethyl ether
SM6200-B Water tert-Butyl Formate
Laboratory: Eurofins Pensacola
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority Program Identification Number Expiration Date
Alabama State 40150 06-30-24
ANAB ISO/IEC 17025 L2471 02-22-26
Arkansas DEQ State 88-00689 08-01-24
California State 2510 06-30-24
Florida NELAP E81010 06-30-24
Georgia State E81010(FL)06-30-24
Illinois NELAP 200041 10-09-23
Kansas NELAP E-10253 10-31-23
Kentucky (UST)State 53 06-30-24
Louisiana (All)NELAP 30976 06-30-24
Louisiana (DW)State LA017 12-31-23
North Carolina (WW/SW)State 314 12-31-23
Oklahoma NELAP 9810 12-31-23
Pennsylvania NELAP 68-00467 01-31-24
South Carolina State 96026 06-30-24
Tennessee State TN02907 06-30-24
Texas NELAP T104704286 09-30-24
US Fish & Wildlife US Federal Programs A22340 06-30-24
USDA US Federal Programs FLGNV23001 01-08-26
USDA US Federal Programs P330-21-00056 05-17-24
Virginia NELAP 460166 06-14-24
West Virginia DEP State 136 03-31-24
West Virginia DEP State 136 03-31-24
Laboratory: Eurofins Savannah
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 269 12-31-23
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
Moisture Soil Percent Moisture
Moisture Soil Percent Solids
Eurofins Raleigh
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Method Summary
Job ID: 752-11855-1Client: East Coast Environmental
Project/Site: 2210 US 1
Method Method Description LaboratoryProtocol
SMSM6200-B Volatile Organic Compounds EET ESC
EPA625.1 Semivolatile Organic Compounds (GC/MS)EET SAV
SW8468015CNonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)EET SAV
MA DEPMAVPHMassachusetts - Volatile Petroleum Hydrocarbons (GC)EET PEN
SW8468015CNonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)EET SAV
MA DEPMA-EPH Massachusetts - Extractable Petroleum Hydrocarbons (GC)EET PEN
EPAMoisturePercent Moisture EET SAV
SW8463511Microextraction of Organic Compounds EET PEN
SW8463546Microwave Extraction EET SAV
SW8465030BPurge and Trap EET PEN
SW8465035AClosed System Purge & Trap/Field Methanol EET SAV
EPACWA_Prep Liquid-Liquid Extraction (Separatory Funnel)EET SAV
SMSM6200-B Purge and Trap EET ESC
Protocol References:
EPA = US Environmental Protection Agency
MA DEP = Massachusetts Department Of Environmental Protection
SM = "Standard Methods For The Examination Of Water And Wastewater"
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EET ESC = Eurofins Raleigh, 102-A Woodwinds Industrial Court, Cary, NC 27511, TEL [phone]
EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Raleigh
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Sample Summary
Client: East Coast Environmental Job ID: 752-11855-1
Project/Site: 2210 US 1
Lab Sample ID Client Sample ID Matrix Collected Received
752-11855-1 S-1 Soil 09/20/23 10:30 09/22/23 12:36
752-11855-2 S-2 Soil 09/20/23 10:35 09/22/23 12:36
752-11855-3 S-3 Soil 09/20/23 10:40 09/22/23 12:36
752-11855-4 S-4 Soil 09/20/23 10:45 09/22/23 12:36
752-11855-5 S-5 Soil 09/20/23 10:50 09/22/23 12:36
752-11855-6 S-6 Soil 09/20/23 10:55 09/22/23 12:36
752-11855-7 S-7 Soil 09/20/23 11:00 09/22/23 12:36
752-11855-8 S-8 Soil 09/20/23 11:05 09/22/23 12:36
752-11855-9 S-9 Soil 09/20/23 11:10 09/22/23 12:36
752-11855-10 S-10 Soil 09/20/23 11:15 09/22/23 12:36
752-11855-11 S-11 Soil 09/20/23 11:20 09/22/23 12:36
752-11855-12 S-12 Soil 09/20/23 11:25 09/22/23 12:36
752-11855-13 S-13 Soil 09/20/23 11:30 09/22/23 12:36
752-11855-14 S-14 Soil 09/20/23 11:45 09/22/23 12:36
752-11855-15 S-15 Soil 09/20/23 15:00 09/22/23 12:36
752-11855-16 S-16 Soil 09/20/23 15:10 09/22/23 12:36
752-11855-17 S-17 Soil 09/20/23 16:00 09/22/23 12:36
752-11855-18 S-18 Soil 09/20/23 16:10 09/22/23 12:36
752-11855-19 S-19 Soil 09/20/23 16:30 09/22/23 12:36
752-11855-20 S-20 Soil 09/20/23 16:45 09/22/23 12:36
752-11855-21 TMW-1 Water 09/21/23 10:00 09/22/23 12:36
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Login Sample Receipt Checklist
Client: East Coast Environmental Job Number: 752-11855-1
Login Number: 11855
Question Answer Comment
Creator: Hyatt, Samantha
List Source: Eurofins Raleigh
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Raleigh
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Login Sample Receipt Checklist
Client: East Coast Environmental Job Number: 752-11855-1
Login Number: 11855
Question Answer Comment
Creator: Earnest, Tamantha
List Source: Eurofins Pensacola
List Creation: 09/25/23 10:10 AMList Number: 3
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
N/AThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.0.0°C IR8
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Raleigh
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Login Sample Receipt Checklist
Client: East Coast Environmental Job Number: 752-11855-1
Login Number: 11855
Question Answer Comment
Creator: Watters, David
List Source: Eurofins Savannah
List Creation: 09/23/23 12:45 PMList Number: 2
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
N/AIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Raleigh
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