FA-28436_47690_CA_MRP_20230726

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
July 26, 2023

Mr. Mike Haseltine
North Carolina Department of Environmental Quality
Fayetteville Regional Office
Systel Building
225 Green Street, Suite 714
Fayetteville, North Carolina 28301

Re: Ground Water Monitoring Report
Food Plus 1
319 North Main Street
Bladenboro, Bladen County
Incident # 47690
Site Ranking: Intermediate 125 D
GRI # 5636

Dear Mr. Haseltine:

Geological Resources, Inc. (GRI) presents the results of the ground water sampling event at the Food Plus
1 site in Bladenboro, North Carolina. The activities were conducted in response to NCDEQ correspondence
dated May 30, 2023.

On July 20, 2023, monitoring well MW-1 was gauged, purged, and sampled per NCDEQ guidelines. The
depth to ground water was 1.23 feet below the top of well casing. Ground water samples were submitted
for analyses of VOCs and oxygenates by EPA Method 6200B. A Site Location Map and Site Map have been
included as Figures 1 and 2, respectively.

Please see the attached summary tables for the results of the July 2023 gauging and ground water
sampling data. Concentrations of benzene, ethylbenzene, xylenes, MTBE, naphthalene, tert-Amyl alcohol,
tert-Butyl alcohol, di-isopropyl ether, n-propylbenzene, and 1,2,4-tribmethylbenzene that exceeded the
Maximum Allowable Concentrations (MACs) as specified in T15A NCAC 2L.0202 were reported in the
ground water samples collected from MW-1. No reported contaminant concentrations exceeded the
Gross Contaminant Levels (GCLs). A copy of the laboratory report is attached.

In April 2022, an updated receptor survey was conducted. No water supply wells were identified within
1,500 feet of the site. Public water is available to the subject site and to all surrounding properties. No
surface water bodies were identified within 500 feet of the site.

Food Plus 1
Ground Water Sampling
Page 2 of 2

3502 Hayes Road • Monroe, North Carolina 28110
Phone [phone] • [phone] • Fax [phone]

According to the April 2022 receptor survey and the July 2023 laboratory results, the site risk should be
reduced. Subsequent to completing a Notice of Residual Petroleum and public notification, the incident
should be closed.

Please contact me at 704-698-1254 or [e-mail] with any questions or comments.

Sincerely,

Rae Troiano Brown, P.G.
Project Manager

cc: client; file

enclosures
SITE LOCATIONFigure 1 Site Location Food Plus 1319 North Main StreetBladenboro, North CarolinaBladen CountyIncident No. 47690GRI Project No. 5636500 M2000 FTDate: 06/09/2022Location: 34.541282° N -78.786262° W Dad
Date: 07/24/2023
Well ID
Date
Installed
(m/dd/yy)
Date Water
Level
Measured
(m/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free Product
Thickness
(ft.)
Ground
Water
Elevation (ft.)
Comments
04/06/22 2.67 --- NM
02/08/23 1.94 --- NM
07/20/23 1.23 --- NM
Notes:
• Elevation relative to mean sea level.
• ft BGS : feet below ground surface.
• NM : Not measured.
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
FOOD PLUS 1 (INCIDENT NO. 47690)
Facility ID # : 00-0-0000022771
MW-1 04/06/22 2 2 - 15 15 NM
Page 1 of 1
Date: 07/26/23
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 40 10 70 70 400
5,000 260,000 84,500 85,500 20,000 6,000 40,000 10,000 70,000 30,000 28,500
MW-1 04/06/22 5,250 E 79.4 1,470 2,453.9 407 811 1,490 2,010 291 148 1,700
MW-1 02/08/23 1,770 3.21 J 325 36.7 184 126 538 989 146 35.1 335
MW-1 07/20/23 2,900 46.6 J 1,070 1,020 236 431 568 J 1,230 149 133 1,040
Trip Blank 07/20/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 NR NR <0.500 <0.190 <0.190
Notes:
• Results reported in micrograms per liter (µg/l).
• < : Less than the method detection limit specified in the laboratory report.
• 2L Standard specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
• Concentrations in bold face type exceeded the 2L standards.
• Concentrations in italics exceeded the gross contamination levels.
• E: Exceeds calibration range.
• J: Estimated value.
• Refer to laboratory report for detected constituents that did not exceed the MACs, or for which no standard has been established.
• NR: Not Requested.
2L Standard (µg/l)
GCL (µg/l)
EPA Method 6200B or EPA Method 602
1,2,4-Trimethylbenzenen-PropylbenzeneDi-isopropyl ethertert-Butyl alcohol(TBA)tert-Amyl alcohol(TAA)Contaminant of Concern BenzeneTolueneEthylbenzeneTotal XylenesMethyl-tert-butyl ether(MTBE)NaphthaleneTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
FOOD PLUS 1 (INCIDENT NO. 47690)
Facility ID # : 00-0-0000022771
Analytical Method
Page 1 of 1

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

7/26/2023
Geological Resources, Inc. Rae Brown
113 West Firetower Road, Suite G Winterville, NC, 28590
Ref: Analytical Testing
Lab Report Number: 23-202-0001 Client Project Description: Food Plus 1
GRI #5636
Dear Rae Brown:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 7/20/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 21
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-202-0001
Page 2 of 21
Report Number:
Sample Summary Table
Client Project Description:
23-202-0001
Food Plus 1
GRI #5636
Lab No Client Sample ID Matrix Date Collected Date Received
07/20/2023 14:05Aqueous 90221 MW-1 07/20/2023 17:02
07/20/2023 13:45Aqueous 90222 Trip Blank 07/20/2023 17:02
Page 3 of 21
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-202-0001
Report Limit
Project:Food Plus 1
V 90221MW-1
2900 07/22/2023 12:556200BBenzeneµg/L 18.0
149 07/22/2023 12:556200BDi-Isopropyl Ether (DIPE)µg/L 50.0
1070 07/22/2023 12:556200BEthylbenzeneµg/L 17.0
56.7 07/22/2023 12:556200BIsopropylbenzeneµg/L 18.0
236 07/22/2023 12:556200BMethyl tert-butyl ether (MTBE)µg/L 14.0
431 07/22/2023 12:556200BNaphthaleneµg/L 47.0
133 07/22/2023 12:556200Bn-Propylbenzene µg/L 19.0
1230 07/22/2023 12:556200Btert-Butyl Alcohol (TBA)µg/L 160
J56807/22/2023 12:556200Btert-Amyl Alcohol (TAA)µg/L 190
J46.6 07/22/2023 12:556200BTolueneµg/L 22.0
1040 07/22/2023 12:556200B1,2,4-Trimethylbenzene µg/L 19.0
185 07/22/2023 12:556200B1,3,5-Trimethylbenzene µg/L 18.0
74.9 07/22/2023 12:556200Bo-Xylene µg/L 21.0
944 07/22/2023 12:556200Bm,p-Xylene µg/L 42.0
1020 07/22/2023 12:556200BXylene (Total)µg/L 21.0
Page 4 of 21
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-202-0001
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #5636 Received : 07/20/2023
Food Plus 1
Report Date : 07/26/2023
Sample ID :
Lab No :
Sampled:MW-1
90221 Matrix:
7/20/2023 14:05
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 07/22/23 12:55 6200BMSA
Surrogate: 4-Bromofluorobenzene 92.6 Limits: 70-130%07/22/23 12:55100 MSA V35681
Surrogate: Dibromofluoromethane 96.4 Limits: 70-130%07/22/23 12:55100 MSA V35681
Surrogate: 1,2-Dichloroethane - d4 98.2 Limits: 70-130%07/22/23 12:55100 MSA V35681
Surrogate: Toluene-d8 103 Limits: 70-130%07/22/23 12:55100 MSA V35681
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 5 of 21
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-202-0001
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #5636 Received : 07/20/2023
Food Plus 1
Report Date : 07/26/2023
Sample ID :
Lab No :
Sampled:MW-1
90221 Matrix:
7/20/2023 14:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35679 07/21/23 14:00
<180 µg/L 180 1000Acetone 100 07/22/23 12:55 V35681MSA
2900 µg/L 18.0 50.0Benzene 100 07/22/23 12:55 V35681MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 07/22/23 12:55 V35681MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 07/22/23 12:55 V35681MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 07/22/23 12:55 V35681MSA
<150 µg/L 150 500Bromoform 100 07/22/23 12:55 V35681MSA
<28.0 µg/L 28.0 100Bromomethane 100 07/22/23 12:55 V35681MSA
<18.0 µg/L 18.0 50.0n-Butylbenzene 100 07/22/23 12:55 V35681MSA
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 07/22/23 12:55 V35681MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 07/22/23 12:55 V35681MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 07/22/23 12:55 V35681MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 07/22/23 12:55 V35681MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 07/22/23 12:55 V35681MSA
<43.0 µg/L 43.0 100Chloroethane 100 07/22/23 12:55 V35681MSA
<22.0 µg/L 22.0 50.0Chloroform 100 07/22/23 12:55 V35681MSA
<22.0 µg/L 22.0 50.0Chloromethane 100 07/22/23 12:55 V35681MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 07/22/23 12:55 V35681MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 07/22/23 12:55 V35681MSA
149 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 07/22/23 12:55 V35681MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 07/22/23 12:55 V35681MSA
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 07/22/23 12:55 V35681MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 07/22/23 12:55 V35681MSA
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 07/22/23 12:55 V35681MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 6 of 21
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-202-0001
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #5636 Received : 07/20/2023
Food Plus 1
Report Date : 07/26/2023
Sample ID :
Lab No :
Sampled:MW-1
90221 Matrix:
7/20/2023 14:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35679 07/21/23 14:00
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 07/22/23 12:55 V35681MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 07/22/23 12:55 V35681MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 07/22/23 12:55 V35681MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 07/22/23 12:55 V35681MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 07/22/23 12:55 V35681MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 07/22/23 12:55 V35681MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 07/22/23 12:55 V35681MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 07/22/23 12:55 V35681MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 07/22/23 12:55 V35681MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 07/22/23 12:55 V35681MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 07/22/23 12:55 V35681MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 07/22/23 12:55 V35681MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 07/22/23 12:55 V35681MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 07/22/23 12:55 V35681MSA
<4200 µg/L 4200 20000Ethanol 100 07/22/23 12:55 V35681MSA
1070 µg/L 17.0 50.0Ethylbenzene 100 07/22/23 12:55 V35681MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 07/22/23 12:55 V35681MSA
<38.0 µg/L 38.0 1002-Hexanone 100 07/22/23 12:55 V35681MSA
56.7 µg/L 18.0 50.0Isopropylbenzene 100 07/22/23 12:55 V35681MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 07/22/23 12:55 V35681MSA
<71.0 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 07/22/23 12:55 V35681MSA
236 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 07/22/23 12:55 V35681MSA
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 07/22/23 12:55 V35681MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 21
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-202-0001
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #5636 Received : 07/20/2023
Food Plus 1
Report Date : 07/26/2023
Sample ID :
Lab No :
Sampled:MW-1
90221 Matrix:
7/20/2023 14:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35679 07/21/23 14:00
<33.0 µg/L 33.0 200Methylene Chloride 100 07/22/23 12:55 V35681MSA
431 µg/L 47.0 100Naphthalene 100 07/22/23 12:55 V35681MSA
133 µg/L 19.0 50.0n-Propylbenzene 100 07/22/23 12:55 V35681MSA
<22.0 µg/L 22.0 50.0Styrene 100 07/22/23 12:55 V35681MSA
1230 µg/L 160 1000tert-Butyl Alcohol (TBA)100 07/22/23 12:55 V35681MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 07/22/23 12:55 V35681MSA
568 J µg/L 190 1000tert-Amyl Alcohol (TAA)100 07/22/23 12:55 V35681MSA
<28.0 µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 07/22/23 12:55 V35681MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 07/22/23 12:55 V35681MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 07/22/23 12:55 V35681MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 07/22/23 12:55 V35681MSA
46.6 J µg/L 22.0 50.0Toluene 100 07/22/23 12:55 V35681MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 07/22/23 12:55 V35681MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 07/22/23 12:55 V35681MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 07/22/23 12:55 V35681MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 07/22/23 12:55 V35681MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 07/22/23 12:55 V35681MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 07/22/23 12:55 V35681MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 07/22/23 12:55 V35681MSA
1040 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 07/22/23 12:55 V35681MSA
185 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 07/22/23 12:55 V35681MSA
<100 µg/L 100 500Vinyl Acetate 100 07/22/23 12:55 V35681MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 07/22/23 12:55 V35681MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 21
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-202-0001
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #5636 Received : 07/20/2023
Food Plus 1
Report Date : 07/26/2023
Sample ID :
Lab No :
Sampled:MW-1
90221 Matrix:
7/20/2023 14:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35679 07/21/23 14:00
74.9 µg/L 21.0 50.0o-Xylene 100 07/22/23 12:55 V35681MSA
944 µg/L 42.0 100m,p-Xylene 100 07/22/23 12:55 V35681MSA
1020 µg/L 21.0 50.0Xylene (Total)100 07/22/23 12:55 V35681
Surrogate: 4-Bromofluorobenzene 92.6 Limits: 70-130%07/22/23 12:55100 MSA V35681
Surrogate: Dibromofluoromethane 96.4 Limits: 70-130%07/22/23 12:55100 MSA V35681
Surrogate: 1,2-Dichloroethane - d4 98.2 Limits: 70-130%07/22/23 12:55100 MSA V35681
Surrogate: Toluene-d8 103 Limits: 70-130%07/22/23 12:55100 MSA V35681
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 21
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-202-0001
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #5636 Received : 07/20/2023
Food Plus 1
Report Date : 07/26/2023
Sample ID :
Lab No :
Sampled:Trip Blank
90222 Matrix:
7/20/2023 13:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35679 07/21/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 07/22/23 05:33 V35681MSA
<0.180 µg/L 0.180 0.500Benzene 1 07/22/23 05:33 V35681MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/22/23 05:33 V35681MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/22/23 05:33 V35681MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/22/23 05:33 V35681MSA
<1.50 µg/L 1.50 5.00Bromoform 1 07/22/23 05:33 V35681MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 07/22/23 05:33 V35681MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 07/22/23 05:33 V35681MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/22/23 05:33 V35681MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/22/23 05:33 V35681MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/22/23 05:33 V35681MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/22/23 05:33 V35681MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/22/23 05:33 V35681MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 07/22/23 05:33 V35681MSA
<0.220 µg/L 0.220 0.500Chloroform 1 07/22/23 05:33 V35681MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 07/22/23 05:33 V35681MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/22/23 05:33 V35681MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/22/23 05:33 V35681MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/22/23 05:33 V35681MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/22/23 05:33 V35681MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 07/22/23 05:33 V35681MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/22/23 05:33 V35681MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/22/23 05:33 V35681MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 21
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-202-0001
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #5636 Received : 07/20/2023
Food Plus 1
Report Date : 07/26/2023
Sample ID :
Lab No :
Sampled:Trip Blank
90222 Matrix:
7/20/2023 13:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35679 07/21/23 14:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/22/23 05:33 V35681MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/22/23 05:33 V35681MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/22/23 05:33 V35681MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/22/23 05:33 V35681MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/22/23 05:33 V35681MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/22/23 05:33 V35681MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/22/23 05:33 V35681MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/22/23 05:33 V35681MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/22/23 05:33 V35681MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/22/23 05:33 V35681MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/22/23 05:33 V35681MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/22/23 05:33 V35681MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/22/23 05:33 V35681MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/22/23 05:33 V35681MSA
<42.0 µg/L 42.0 200Ethanol 1 07/22/23 05:33 V35681MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/22/23 05:33 V35681MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/22/23 05:33 V35681MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 07/22/23 05:33 V35681MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 07/22/23 05:33 V35681MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/22/23 05:33 V35681MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/22/23 05:33 V35681MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/22/23 05:33 V35681MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/22/23 05:33 V35681MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 21
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-202-0001
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #5636 Received : 07/20/2023
Food Plus 1
Report Date : 07/26/2023
Sample ID :
Lab No :
Sampled:Trip Blank
90222 Matrix:
7/20/2023 13:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35679 07/21/23 14:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/22/23 05:33 V35681MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 07/22/23 05:33 V35681MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/22/23 05:33 V35681MSA
<0.220 µg/L 0.220 0.500Styrene 1 07/22/23 05:33 V35681MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/22/23 05:33 V35681MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/22/23 05:33 V35681MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/22/23 05:33 V35681MSA
<0.220 µg/L 0.220 0.500Toluene 1 07/22/23 05:33 V35681MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/22/23 05:33 V35681MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/22/23 05:33 V35681MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/22/23 05:33 V35681MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/22/23 05:33 V35681MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/22/23 05:33 V35681MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/22/23 05:33 V35681MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/22/23 05:33 V35681MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/22/23 05:33 V35681MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/22/23 05:33 V35681MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/22/23 05:33 V35681MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/22/23 05:33 V35681MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 07/22/23 05:33 V35681MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 07/22/23 05:33 V35681MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 21
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-202-0001
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #5636 Received : 07/20/2023
Food Plus 1
Report Date : 07/26/2023
Sample ID :
Lab No :
Sampled:Trip Blank
90222 Matrix:
7/20/2023 13:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35679 07/21/23 14:00
<0.21 µg/L 0.210 0.500Xylene (Total)1 07/22/23 05:33 V35681
Surrogate: 4-Bromofluorobenzene 91.8 Limits: 70-130%07/22/23 05:331 MSA V35681
Surrogate: Dibromofluoromethane 96.0 Limits: 70-130%07/22/23 05:331 MSA V35681
Surrogate: 1,2-Dichloroethane - d4 99.4 Limits: 70-130%07/22/23 05:331 MSA V35681
Surrogate: Toluene-d8 103 Limits: 70-130%07/22/23 05:331 MSA V35681
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 21
Quality Control Data
23-202-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Food Plus 1
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35681QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35679
Associated Lab Samples: 90221, 90222
LRB-V35679 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/22/23 04:3810.01.80<1.80µg/LAcetone
07/22/23 04:380.5000.180<0.180µg/LBenzene
07/22/23 04:380.5000.210<0.210µg/LBromobenzene
07/22/23 04:381.000.420<0.420µg/LBromochloromethane
07/22/23 04:380.5000.160<0.160µg/LBromodichloromethane
07/22/23 04:385.001.50<1.50µg/LBromoform
07/22/23 04:381.000.280<0.280µg/LBromomethane
07/22/23 04:380.5000.180<0.180µg/Ln-Butylbenzene
07/22/23 04:380.5000.200<0.200µg/Lsec-Butyl benzene
07/22/23 04:382.000.920<0.920µg/Ltert-Butyl benzene
07/22/23 04:380.5000.180<0.180µg/LCarbon Tetrachloride
07/22/23 04:380.5000.190<0.190µg/LChlorobenzene
07/22/23 04:380.5000.190<0.190µg/LChlorodibromomethane
07/22/23 04:381.000.430<0.430µg/LChloroethane
07/22/23 04:380.5000.220<0.220µg/LChloroform
07/22/23 04:380.5000.220<0.220µg/LChloromethane
07/22/23 04:380.5000.200<0.200µg/L2-Chlorotoluene
07/22/23 04:380.5000.200<0.200µg/L4-Chlorotoluene
07/22/23 04:380.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
07/22/23 04:382.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
07/22/23 04:380.5000.200<0.200µg/L1,2-Dibromoethane
07/22/23 04:380.5000.230<0.230µg/LDibromomethane
07/22/23 04:380.5000.220<0.220µg/L1,2-Dichlorobenzene
07/22/23 04:380.5000.190<0.190µg/L1,3-Dichlorobenzene
07/22/23 04:380.5000.210<0.210µg/L1,4-Dichlorobenzene
07/22/23 04:385.001.20<1.20µg/LDichlorodifluoromethane
07/22/23 04:380.5000.240<0.240µg/L1,1-Dichloroethane
Page 1 of 6Date:07/24/2023 05:32 PM
Page 14 of 21
Quality Control Data
23-202-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Food Plus 1
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35681QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35679
Associated Lab Samples: 90221, 90222
LRB-V35679 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/22/23 04:380.5000.150<0.150µg/L1,2-Dichloroethane
07/22/23 04:380.5000.150<0.150µg/L1,1-Dichloroethene
07/22/23 04:380.5000.200<0.200µg/Lcis-1,2-Dichloroethene
07/22/23 04:380.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
07/22/23 04:380.5000.190<0.190µg/L1,2-Dichloropropane
07/22/23 04:380.5000.130<0.130µg/L1,3-Dichloropropane
07/22/23 04:382.000.210<0.210µg/L2,2-Dichloropropane
07/22/23 04:380.5000.200<0.200µg/L1,1-Dichloropropene
07/22/23 04:380.5000.210<0.210µg/Lcis-1,3-Dichloropropene
07/22/23 04:380.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
07/22/23 04:3820042.0<42.0µg/LEthanol
07/22/23 04:380.5000.170<0.170µg/LEthylbenzene
07/22/23 04:383.000.350<0.350µg/LHexachlorobutadiene
07/22/23 04:381.000.380<0.380µg/L2-Hexanone
07/22/23 04:380.5000.180<0.180µg/LIsopropylbenzene
07/22/23 04:380.5000.089<0.089µg/L4-Isopropyl toluene
07/22/23 04:385.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
07/22/23 04:381.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
07/22/23 04:381.000.078<0.078µg/L4-Methyl-2-Pentanone
07/22/23 04:382.000.330<0.330µg/LMethylene Chloride
07/22/23 04:381.000.470<0.470µg/LNaphthalene
07/22/23 04:380.5000.190<0.190µg/Ln-Propylbenzene
07/22/23 04:380.5000.220<0.220µg/LStyrene
07/22/23 04:3810.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
07/22/23 04:3810.00.350<0.350µg/Ltert-Butyl formate (TBF)
07/22/23 04:3810.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
07/22/23 04:3810.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 2 of 6Date:07/24/2023 05:32 PM
Page 15 of 21
Quality Control Data
23-202-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Food Plus 1
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35681QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35679
Associated Lab Samples: 90221, 90222
LRB-V35679 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/22/23 04:380.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
07/22/23 04:380.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
07/22/23 04:380.5000.220<0.220µg/LTetrachloroethene
07/22/23 04:380.5000.220<0.220µg/LToluene
07/22/23 04:380.5000.380<0.380µg/L1,2,3-Trichlorobenzene
07/22/23 04:380.5000.310<0.310µg/L1,2,4-Trichlorobenzene
07/22/23 04:380.5000.160<0.160µg/L1,1,1-Trichloroethane
07/22/23 04:380.5000.096<0.096µg/L1,1,2-Trichloroethane
07/22/23 04:380.5000.180<0.180µg/LTrichloroethene
07/22/23 04:380.5000.180<0.180µg/LTrichlorofluoromethane
07/22/23 04:380.5000.270<0.270µg/L1,2,3-Trichloropropane
07/22/23 04:380.5000.190<0.190µg/L1,2,4-Trimethylbenzene
07/22/23 04:380.5000.180<0.180µg/L1,3,5-Trimethylbenzene
07/22/23 04:385.001.00<1.00µg/LVinyl Acetate
07/22/23 04:380.5000.170<0.170µg/LVinyl Chloride
07/22/23 04:380.5000.210<0.210µg/Lo-Xylene
07/22/23 04:381.000.420<0.420µg/Lm,p-Xylene
07/22/23 04:3810.01.00<1.00µg/L3,3-Dimethyl-1-butanol
07/22/23 04:384-Bromofluorobenzene (S)91.8 70-130
07/22/23 04:38Dibromofluoromethane (S)96.0 70-130
07/22/23 04:381,2-Dichloroethane - d4 (S)98.4 70-130
07/22/23 04:38Toluene-d8 (S)107 70-130
Page 3 of 6Date:07/24/2023 05:32 PM
Page 16 of 21
Quality Control Data
23-202-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Food Plus 1
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35681QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35679
LCS-V35679 LCSD-V35679Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
24.2 60.566.026.440.0µg/LAcetone 40-160 8.6 20.0
17.0 85.092.018.420.0µg/LBenzene 70-130 7.9 20.0
19.9 99.510621.120.0µg/LBromobenzene 70-130 5.8 20.0
17.8 89.090.518.120.0µg/LBromochloromethane 70-130 1.6 20.0
17.0 85.090.018.020.0µg/LBromodichloromethane 70-130 5.7 20.0
17.9 89.598.019.620.0µg/LBromoform 70-130 9.0 20.0
26.0 13012625.120.0µg/LBromomethane 60-140 3.5 20.0
19.1 95.510320.620.0µg/Ln-Butylbenzene 70-130 7.5 20.0
18.7 93.510420.720.0µg/Lsec-Butyl benzene 70-130 10.1 20.0
19.2 96.010320.620.0µg/Ltert-Butyl benzene 70-130 7.0 20.0
19.0 95.092.018.420.0µg/LCarbon Tetrachloride 70-130 3.2 20.0
19.4 97.010420.820.0µg/LChlorobenzene 70-130 6.9 20.0
19.0 95.010320.620.0µg/LChlorodibromomethane 70-130 8.0 20.0
18.8 94.097.019.420.0µg/LChloroethane 60-140 3.1 20.0
17.3 86.589.517.920.0µg/LChloroform 70-130 3.4 20.0
17.3 86.587.017.420.0µg/LChloromethane 60-140 0.5 20.0
19.4 97.010621.120.0µg/L2-Chlorotoluene 70-130 8.3 20.0
19.6 98.010521.020.0µg/L4-Chlorotoluene 70-130 6.8 20.0
16.1 80.586.017.220.0µg/LDi-Isopropyl Ether (DIPE)70-130 6.6 20.0
17.6 88.010721.320.0µg/L1,2-Dibromo-3-Chloropropane 70-130 19.0 20.0
18.0 90.098.019.620.0µg/L1,2-Dibromoethane 70-130 8.5 20.0
17.2 86.090.018.020.0µg/LDibromomethane 70-130 4.5 20.0
19.0 95.010721.320.0µg/L1,2-Dichlorobenzene 70-130 11.4 20.0
19.3 96.510420.720.0µg/L1,3-Dichlorobenzene 70-130 7.0 20.0
18.4 92.098.519.720.0µg/L1,4-Dichlorobenzene 70-130 6.8 20.0
16.4 82.083.516.720.0µg/LDichlorodifluoromethane 60-140 1.8 20.0
Page 4 of 6Date:07/24/2023 05:32 PM
Page 17 of 21
Quality Control Data
23-202-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Food Plus 1
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35681QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35679
LCS-V35679 LCSD-V35679Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
17.1 85.591.018.220.0µg/L1,1-Dichloroethane 70-130 6.2 20.0
15.6 78.084.516.920.0µg/L1,2-Dichloroethane 70-130 8.0 20.0
16.5 82.593.018.620.0µg/L1,1-Dichloroethene 70-130 11.9 20.0
16.9 84.590.518.120.0µg/Lcis-1,2-Dichloroethene 70-130 6.8 20.0
16.7 83.592.518.520.0µg/Ltrans-1,2-Dichloroethene 70-130 10.2 20.0
17.3 86.592.518.520.0µg/L1,2-Dichloropropane 70-130 6.7 20.0
18.2 91.099.019.820.0µg/L1,3-Dichloropropane 70-130 8.4 20.0
15.0 75.082.516.520.0µg/L2,2-Dichloropropane 70-130 9.5 20.0
17.7 88.597.019.420.0µg/L1,1-Dichloropropene 70-130 9.1 20.0
17.2 86.091.018.220.0µg/Lcis-1,3-Dichloropropene 70-130 5.6 20.0
16.5 82.588.517.720.0µg/Ltrans-1,3-Dichloropropene 70-130 7.0 20.0
419 83.893.0465500µg/LEthanol 60-140 10.4 20.0
18.2 91.099.519.920.0µg/LEthylbenzene 70-130 8.9 20.0
18.1 90.510220.420.0µg/LHexachlorobutadiene 70-130 11.9 20.0
16.0 80.088.017.620.0µg/L2-Hexanone 60-140 9.5 20.0
19.2 96.010320.620.0µg/LIsopropylbenzene 70-130 7.0 20.0
19.8 99.010721.420.0µg/L4-Isopropyl toluene 70-130 7.7 20.0
17.2 86.082.516.520.0µg/LMethyl Ethyl Ketone (MEK)60-140 4.1 20.0
16.5 82.590.018.020.0µg/LMethyl tert-butyl ether (MTBE)70-130 8.6 20.0
15.3 76.583.016.620.0µg/L4-Methyl-2-Pentanone 60-140 8.1 20.0
17.6 88.095.019.020.0µg/LMethylene Chloride 70-130 7.6 20.0
15.5 77.577.515.520.0µg/LNaphthalene 70-130 0.0 20.0
19.0 95.010320.620.0µg/Ln-Propylbenzene 70-130 8.0 20.0
19.3 96.510220.420.0µg/LStyrene 70-130 5.5 20.0
27.1 67.779.231.740.0µg/Ltert-Butyl Alcohol (TBA)40-140 15.6 20.0
41.4 10410943.640.0µg/Ltert-Butyl formate (TBF)40-140 5.1 20.0
Page 5 of 6Date:07/24/2023 05:32 PM
Page 18 of 21
Quality Control Data
23-202-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Food Plus 1
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35681QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35679
LCS-V35679 LCSD-V35679Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
16.2 81.083.016.620.0µg/Ltert-Amyl Alcohol (TAA)40-140 2.4 20.0
32.3 80.789.535.840.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 10.2 20.0
19.5 97.510521.020.0µg/L1,1,1,2-Tetrachloroethane 70-130 7.4 20.0
19.4 97.010520.920.0µg/L1,1,2,2-Tetrachloroethane 70-130 7.4 20.0
18.1 90.599.519.920.0µg/LTetrachloroethene 70-130 9.4 20.0
16.8 84.089.517.920.0µg/LToluene 70-130 6.3 20.0
15.6 78.090.018.020.0µg/L1,2,3-Trichlorobenzene 70-130 14.2 20.0
18.6 93.010521.020.0µg/L1,2,4-Trichlorobenzene 70-130 12.1 20.0
16.6 83.091.018.220.0µg/L1,1,1-Trichloroethane 70-130 9.1 20.0
16.8 84.091.518.320.0µg/L1,1,2-Trichloroethane 70-130 8.5 20.0
17.0 85.091.018.220.0µg/LTrichloroethene 70-130 6.8 20.0
18.0 90.093.018.620.0µg/LTrichlorofluoromethane 60-140 3.2 20.0
18.9 94.510621.120.0µg/L1,2,3-Trichloropropane 70-130 11.0 20.0
19.3 96.510420.820.0µg/L1,2,4-Trimethylbenzene 70-130 7.4 20.0
19.9 99.510621.120.0µg/L1,3,5-Trimethylbenzene 70-130 5.8 20.0
15.6 78.083.516.720.0µg/LVinyl Acetate 60-140 6.8 20.0
18.7 93.597.519.520.0µg/LVinyl Chloride 60-140 4.1 20.0
18.9 94.510120.120.0µg/Lo-Xylene 70-130 6.1 20.0
38.5 96.210542.140.0µg/Lm,p-Xylene 70-130 8.9 20.0
14.3 71.574.014.820.0µg/L3,3-Dimethyl-1-butanol 70-130 3.4 20.0
91.091.84-Bromofluorobenzene (S)70-130
95.096.2Dibromofluoromethane (S)70-130
98.499.81,2-Dichloroethane - d4 (S)70-130
105105Toluene-d8 (S)70-130
Page 6 of 6Date:07/24/2023 05:32 PM
Page 19 of 21
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-202-0001
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 2.6C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:07/21/2023 09:45:33
Special precautions or instructions included?
Comments:
Page 20 of 21
Page 21 of 21