FA-8034_42251_CA_LSA_20230821_LSA

LIMITED SITE ASSESSMENT
PHASE I REPORT
At
BUILDING N-6002
CCFTBR0149
INCIDENT NUMBER 42251
FORT LIBERTY, NORTH CAROLINA

Prepared BY:

U.S. Army Corps of Engineers, Savannah District

AUGUST 2023

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EXECUTIVE SUMMARY
This report documents activities for a Phase I Limited Site Assessment (LSA) conducted by the
U.S. Army Corps of Engineers (USACE), Savannah District (SAS) on December 13, 2022, at
former underground storage tank (UST) site N-6002 (site CCFTBR0149), which formerly
featured two USTs (N-6002A and N-6002B). The site is located on the Fort Liberty Military
Base (formerly Fort Bragg) in Fayetteville, Cumberland County, North Carolina. In
correspondence dated January 31, 2020, the North Carolina Department of Environmental
Quality (NCDEQ) requested additional investigation to determine if previously discovered
contamination at the site poses a threat to the environment. This LSA was conducted in
accordance with NCDEQ guidance, Guidelines for Assessment and Corrective Action for UST
Releases and site-specific correspondence from NCDEQ.

The U.S. Army Military Reservation at Fort Liberty was established in 1918 as the major
logistic, training, and mobilization deployment center for part of the U.S. Army’s mobile
infantry, assault, and armored forces. Fort Liberty occupies about 161,500 acres in southeastern
North Carolina. The cantonment area, in the eastern part of Fort Liberty, occupies 11,000 acres
and includes about 4,800 buildings. Most military maintenance and production facilities, supply
facilities, operation and training facilities, various community facilities, and family and troop
housing are in the cantonment area.

Former UST Site N-6002 (Facility ID F000003) is located northwest of the intersection of
Logistics Street and Honeycutt Road, adjacent to Building N-6002. The site formerly featured
two USTs (tank No. N-6002A and N-6002B) within a single tank basin. The UST closure forms
and Notice of Intent detailing the size, contents, and removal date were not available for review.
A site assessment with environmental sampling was conducted by Aerostar SES LLC (Aerostar).
Five confirmatory soil samples and a field duplicate were collected and analyzed for Volatile
Organic Compounds (VOCs) following US Environmental Protection Agency (EPA) Method
8260, for Semi-Volatile Organic Compounds (SVOCs) by EPA Method 8270, and for Total
Petroleum Hydrocarbons (TPH) for Extractable Petroleum Hydrocarbons/Volatile Petroleum
Hydrocarbons (EPH/VPH) by the Massachusetts Department of Environmental Protection
(MADEP) Method.

One soil sample showed a benzene concentration above the NCDEQ Soil to Water Maximum
Soil Contaminant Concentration (MSCC), but below the Residential MSCC. As no analytical
detections above NCDEQ residential or industrial MSCCs or EPA residential or industrial
regional screening levels (RSLs) were exceeded, Aerostar recommended a No Further Action
(NFA) for the site. Groundwater was not encountered during the investigation. On January 31st,
2020 the NCDEQ responded to Aerostar’s request for NFA with a request for additional
investigation of former UST site N-6002. The NCDEQ review of the laboratory data indicated
soil contamination in excess of the lower of the residential or soil to groundwater MSCCs.

In March of 2022 USACE-SAS mobilized to the site to conduct additional soil sampling in the
area of the former USTs. A GeoProbe® direct push rig was used to complete one soil boring
near the former USTs in order to assess whether contaminated soil and/or groundwater were
present at the site. Refusal was hit by the GeoProbe® at approximately 10 feet below ground
surface (bgs). The resulting hole was abandoned. USACE-SAS re-mobilized to the site in
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December 2022 with a Terrasonic 150CC sonic drill rig to complete the soil boring in the same
location as the March 2022 soil boring. Recovered boring material was screened onsite using a
calibrated OVA-PID. Soil gas readings were between zero and 4.5 parts per million (ppm) for all
sampled intervals. Soil samples were collected at six feet bgs and at 10-foot intervals thereafter
to a total depth of 46 feet bgs. Groundwater was encountered at approximately 47 feet bgs.

The soil and groundwater samples were sent for laboratory analysis of VOCs, SVOCs, metals,
hexavalent chromium, TPH-VPH, and TPH-EPH. In addition, the soil sample collected at six
feet bgs as well as the groundwater sample were analyzed for pesticides and polychlorinated
biphenyls (PCBs).

Laboratory analytical results for soil from the December 2022 sampling event are compared to
the NCDEQ Soil to Water MSCCs, residential soil cleanup levels, and industrial soil cleanup
levels. Where NCDEQ regulatory limits are unavailable, US Environmental Protection Agency
(EPA) Regional Screening Levels (RSLs) are used for comparison. Detections above regulatory
standards were as follows:
• Acetone was detected in the six-foot soil sample at an estimated quantity of 35
milligrams per kilogram (mg/kg). This exceeds the NCDEQ MSCC of 24 mg/kg but is
below the residential and industrial soil cleanup levels.
• Arsenic was detected in soil samples collected at 6, 30, and 40 feet below ground surface
(bgs) at concentrations greater than the USEPA RSL for residential soil of 0.68 mg/kg
but below the industrial RSL of 3 mg/kg.
• Total chromium was detected in the 6-, 30-, and 40-foot soil samples at concentrations
greater than the NCDEQ MSCC of 3.8 mg/kg as well as the residential soil cleanup level
of 1.32 mg/kg. Total chromium was detected in the 20-foot soil sample at a concentration
of 1.9 mg/kg, which exceeds the residential soil cleanup level only. No detections were
found in excess of the industrial soil cleanup level for total chromium.
• Hexavalent chromium was detected in the 6-foot soil sample at a concentration of 1.8
mg/kg. This concentration exceeds the residential soil cleanup level of 1.32 mg/kg but is
below the NCDEQ MSCC and the industrial soil cleanup levels.
Several other detections above laboratory method detection limits (MDLs) were found within the
soil samples submitted for laboratory analysis; however, none of the other detections were above
regulatory standards.

Laboratory analytical results for groundwater from the December 2022 sampling event are
compared to the NCDEQ Gross Contaminant Levels (GCLs) as well as the NCDEQ
Groundwater Quality Standards (GWQS). Where NCDEQ regulatory values were unavailable,
the laboratory results are compared to the USEPA RSLs for tap water. Detections above
regulatory standards were as follows:
• Bis(2-ethylhexyl) phthalate was detected at an estimated concentration of 3.1 micrograms
per liter (µg/L). This concentration exceeds the NCDEQ GWQS for bis(2-ethylhexyl)
phthalate of 3.0 µg/L
• Total chromium was detected at a concentration of 15 µg/L. This concentration exceeds
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the NCDEQ GWQS for total chromium of 10 µg/L. Hexavalent chromium was non-
detect.
• Magnesium was detected at a concentration of 560 µg/L. This concentration exceeds the
USEPA RSL for tap water of 28 µg/L for magnesium.
• Sodium was detected at a concentration of 13,000 µg/L. This concentration exceeds the
USEPA RSL for tap water of 2,000 µg/L.
Several other detections above laboratory method detection limits (MDLs) were found within the
groundwater sample submitted for laboratory analysis; however, none of the other detections
were above regulatory standards.

There are no public or private groundwater withdrawal points or well head protection areas
within 1,500 feet of the site. The Black Creek is an unconfined aquifer near the subject site with
groundwater flow to the west-southwest. Groundwater was encountered at approximately 47 feet
bgs at the site. The Cape Fear Aquifer, the main drinking water source for the surrounding area,
is greater than 150 feet bgs and is protected by confining layers. Underground utilities are
generally shallower than groundwater at the site and would not be expected to be conduits for
contamination.

Currently, the subject site is used as a parking aera for building N-6002. The USTs were in a
landscaped area of the site. The site is within a parking area on the Fort Liberty installation and
is not easily accessible by the general public. Use of the site is not expected to change in the
future.

Based on current information, acetone, arsenic, total chromium, and hexavalent chromium were
detected in the soil samples collected from the site at concentrations above regulatory limits.
Acetone is a common laboratory artifact and was only detected in the six-foot soil sample at a
concentration above NCDEQ MSCCs but below both residential and industrial clean up levels.
As such, the single acetone exceedance of it is not a cause for concern for the site. Arsenic was
detected at concentrations above the USEPA RSL for residential soil but below the RSL for
industrial soil. Arsenic is known to naturally occur at levels greater than the USEPA RSL for
residential soil across the Fort Liberty area (Philip Hunter, 2005). As such, the arsenic detected
within the soil is considered background concentrations and not a concern for the site. Total
chromium was detected above all regulatory thresholds in one or more soil samples collected
from the site. Hexavalent chromium was only detected in the six-foot soil sample at a
concentration exceeding the residential soil cleanup level, but below the NCDEQ soil to
groundwater MSCC and the industrial soil cleanup level. The lack of hexavalent chromium
detections above regulatory thresholds is indicative that most of the chromium in soil exists as
chromium III. As the site operates as an industrial facility and access by the general public is
limited, the singular hexavalent chromium exceedance above the residential soil cleanup level is
not considered an environmental concern for the site. Groundwater was encountered at
approximately 47 feet bgs at the time of sampling. Due to site conditions and water column
availability, the groundwater sample was analyzed for both total and dissolved metals. Total
metals analysis of less-than-ideal turbidity groundwater includes results from any suspended
solids within the sample, which can lead to inaccurate metal detections. Analyzing for dissolved
metals in addition to total metals allows for the distinction between metals included within the
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water column and those impacting the surrounding soil. Bis(2-ethylhexyl) phthalate was detected
at an estimated concentration of 3.1 µg/L which exceeds the NCDEQ GWQS of 3 µg/L for
bis(2-ethylhexyl) phthalate but is below the GCL. Bis(2-ethylhexyl) phthalate is a common
component in plasticizers and the minor detection is likely contributed to cross contamination
from the equipment used at the time of sampling. As such, the bis(2-ethylhexyl) phthalate
detection in groundwater is not a concern for the site. Total chromium was detected at an
estimated concentration of 15 µg/L which is above the NCDEQ GWQS of 10 µg/L for
chromium but below the GCL. Hexavalent chromium was not detected in the one groundwater
sample submitted for laboratory analysis. The lack of a hexavalent chromium exceedance is
indicative that the chromium in groundwater exists as chromium III and is not an environmental
concern for the site. Manganese was detected at a concentration of 560 µg/L which exceeds the
USEPA RSL for tap water of 430 µg/L. Sodium was detected at a concentration of 13,000 µg/L
which exceeds the USEPA RSL for tap water of 2000 µg/L. As manganese and sodium do not
have established NCDEQ GWQSs or GCLs and groundwater at the site is not expected to be
utilized for public water supply, the manganese and sodium exceedances above the USEPA
RSLs are not an environmental concern for the site. As such, further investigation is not
warranted at this time and USACE-SAS recommends a NFA designation for the site.

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Table of Contents page
EXECUTIVE SUMMARY .......................................................................................................... 1
LIST OF ABBREVIATIONS AND ACRONYMS .................................................................... 7
REFERENCES .............................................................................................................................. 8
A. SITE INFORMATION ......................................................................................................... 9
1. Site Identification ................................................................................................................. 9
2. Information About Contacts Associated with the Leaking UST/AST System .................... 9
3. Information about the Release .............................................................................................. 9
4. Certification ........................................................................................................................ 10
B. SITE HISTORY AND CHARACTERIZATION ............................................................. 11
1. UST Owner and Operator Information .............................................................................. 11
2. UST Information ................................................................................................................ 11
3. Non-UST Information ........................................................................................................ 11
4. Description of the Release .................................................................................................. 11
6. Previous Activities ............................................................................................................. 12
C. RISK CHARACTERIZATION ......................................................................................... 12
D. RECEPTOR INFORMATION .......................................................................................... 15
1. Water Supply Well(s) ......................................................................................................... 15
2. Public Water Supplies ........................................................................................................ 15
3. Surface Water ..................................................................................................................... 15
4. Wellhead Protection Area(s) .............................................................................................. 15
5. Deep Aquifers in the Coastal Plain Physiographic Region ................................................ 15
6. Subsurface Structure(s) ...................................................................................................... 16
E. LAND USE ........................................................................................................................... 16
1. Property Owners and Occupants ........................................................................................ 16
2. Sensitive Land Use Features .............................................................................................. 16
F. SITE GEOLOGY AND HYDROGEOLOGY .................................................................. 16
G. SAMPLING RESULTS ...................................................................................................... 17
1. Phase I Investigation .......................................................................................................... 17
2. Phase II Investigation ......................................................................................................... 18
H. CONCLUSIONS AND RECOMMENDATIONS ............................................................ 19
I. FREE PRODUCT INVESTIGATION AND RECOVERY ............................................ 19
J. PROPOSED REMEDY FOR CONTAMINATION ........................................................ 19
K. FIGURES ............................................................................................................................. 20
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L. TABLES ............................................................................................................................... 20
M. APPENDICES ..................................................................................................................... 20
APPENDIX A – FIGURES
APPENDIX B – TABLES
APPENDIX C – SOIL BORING LOG
APPENDIX D – LABORATORY REPORT

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LIST OF ABBREVIATIONS AND ACRONYMS

bgs below ground surface
CL low liquid limit (lean) clay
EPA U.S. Environmental Protection Agency
EPH extractable petroleum hydrocarbons
DENR Department of Environmental and Natural Resources
DO dissolved oxygen
DPW Directorate of Public Works
FID flame ionization detector
GWQS Groundwater Quality Standard
ID inner diameter
IDW investigation derived waste
LSA Limited Site Assessment
MADEP Massachusetts Department of Environmental Protection
µg/L micrograms per liter
mg/kg milligrams per kilogram (ppm)
MSCC maximum soil contaminant concentration
msl mean sea level
MTBE methyl tert butyl ether
N/A not applicable or not available
NC North Carolina
PID photo-ionization detector
ppm parts per million
PVC polyvinyl chloride
PWS Public Water Supply
QA quality assurance
QC quality control
SAR Soil Assessment Report
SB soil boring
SC clayey sand
SM silty sand
SP poorly graded (well sorted) sand
SVOC semi-volatile organic compound
TOC top of casing/total organic carbon
USACE United States Army Corps of Engineers
USGS United States Geological Survey
UST underground storage tank
VOC volatile organic compound
VPH volatile petroleum hydrocarbon
2L NC 15A NCAC 2L .0202 Groundwater Quality Standard

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REFERENCES
Aerostar Environmental Services, Inc. (AEROSTAR), Final Tank Closure Assessment
Report Restoration and Recycling Support FY 16, 17, 18 Building N-6002, Fort Liberty,
North Carolina, September 2019.

North Carolina Administrative Code (NCAC), 2016. Title 15A, Department of Environment
and Natural Resources, Division of Water Quality, Subchapter 2L, Section .0100, .0200,
.0300, Classifications and Water Quality Standards Applicable to the Groundwaters of
North Carolina. https://deq.nc.gov/documents/nc-stds-groundwater-02lstandards, 01
April 2022.

North Carolina Department of Environment Quality (NCDEQ), Division of Waste
Management, UST Section, Guidelines for Assessment and Corrective Action for UST
Releases, 15 July 2008.

NCDEQ, Division of Waste Management, UST Section, Guidelines for Sampling, 15 July
2008 with Change 3 Effective December 1, 2013.

NCDEQ, Division of Waste Management, UST Section, Guidelines for Site Checks, Tank
Closure, and Initial Response and Abatement for UST Releases, March 1, 2009 with
Change 9, Effective February 1, 2019.

NCDEQ Notice of Regulatory Requirements, 15A NCAC 2L .0405 Risk Based Assessment
and Corrective Action for Petroleum Underground Storage Tanks; N-6002 A and B,
Building N-6002, Fort Liberty, Cumberland County, Incident Number: 42251, January
31, 2020.

U.S. Geological Survey (USGS), NCDENR, 7.5-Minute Topographic Map Series,
Fayetteville Quadrangle, NC, 1997.

USGS/USACE, 7.5 Minute Topographic Map Series, Clifdale Quadrangle, NC, revised
1982.

USGS/USACE, 7.5 Minute Topographic Map Series, Manchester Quadrangle, NC, revised
1987.

USGS/USACE, 7.5 Minute Topographic Map Series, Overhills Quadrangle, NC, revised
1971.

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A. SITE INFORMATION
1. Site Identification
o Date of Report: July 2023
o Site Name: CCFTBR0149
o UST Incident Number: 42251
o Building No.: Building N-6002
o Site Street Address: Logistics Street and Honeycutt Road (nearest intersection)
o City/Town: Fort Liberty, NC Zip Code: 28303 County: Cumberland
o Description of geographical Point: Former UST Location
o Location Method: Google Earth
o Latitude: 35° 1'44.60"N Longitude: 78° 9'5.74"W
2. Information About Contacts Associated with the Leaking UST System
(Include Address, street, city, state, zip code, and mailing address if different from above)
o UST Owner: Fort Liberty Directorate of Public Works
Address: IMSE-BRG-PWE-C, Building 3-1137
Fort Liberty, NC, 28310 Telephone: [phone]
o UST Operator: Fort Liberty Directorate of Public Works
Address: IMSE-BRG-PWE-C, Building 3-1137
Fort Liberty, NC, 28310 Telephone: [phone]
o Property Owner: Fort Liberty Directorate of Public Works
Address: IMSE-BRG-PWE-C, Building 3-1137
Fort Liberty, NC, 28310 Telephone: [phone]
o Property Occupant: Fort Liberty Environmental Management Branch
Address: IMSE-BRG-PWE-C, Building 3-1137
Fort Liberty, NC, 28310 Telephone: [phone]
o Consultant/Contractor: U.S. Army Engineer District, Savannah
Address: 100 West Oglethorpe Avenue
Savannah, GA, 31401-3640 Telephone: [phone]
o Analytical Laboratory: Sure-BioChem Laboratories, Inc.
Address: 100 Atlantic Avenue
Camden, NJ, 08104 Telephone: [phone]
NC Cert. No. 269
3. Information about the Release
o Date Discovered: 05/17/2019
o Estimated Quantity of Release: Unknown
o Cause of Release: Unknown, discovered during UST closure sampling
o Source of Release: UST system
o Size and Contents of UST System(s) from which the release occurred: Size and
contents of the UST system is unknown. The site formerly featured two USTs within
a single tank basin.

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4.Certification
This Phase I LSA utilized only those techniques, procedures, and processes described in
this report. It is the professional judgment and opinion of the U.S. Army Corps of
Engineers (USACE) that the facts and conditions depicted are accurate and are subject to
limitations inherent in the investigation techniques used and any expressed limitations in
this assessment.
The U.S. Army Corps of Engineers has conducted this Phase I LSA on behalf of the Fort
Liberty, NC, Directorate of Public Works. This Phase I LSA is intended for the sole use
of the Fort Liberty, NC, Directorate of Public Works. USACE has reviewed all
appropriate records made available following an analysis of information obtained during
the records search. The information contained within the survey report is based on
records made available and, to the best of USACE’s knowledge, is correct and current as
of the date of this document.
Prepared by:
Emily M. Stamm, P.G.
USACE, Savannah District
Certified by: _______________________________________
Emily M. Stamm, P.G.
USACE, Savannah District
Approved by: ______________________________________
Jason T. Lennane, P.G.
USACE, Savannah District
Date: __08/07/2023________
The U.S. Army Corps of Engineers is authorized to practice geology and/or engineering
on Federal property without a State-specific license or certification.
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B. SITE HISTORY AND CHARACTERIZATION
1. UST Owner and Operator Information
The only owner and operator of the subject site throughout its lifespan has been the Fort
Liberty Garrison Command. Details of the UST owner/operator information is included
on Table 2 of Appendix B.
2. UST Information
o The identification number for these USTs are N-6002A and N-6002B.
o A site vicinity map is presented on Figure 1 of Appendix A.
o A site layout map is presented on Figure 2 of Appendix A.
o The most recent contents of the USTs are unknown.
o The historical contents of the USTs are unknown.
o The capacity of the USTs are unknown.
o The construction materials and structure of the USTs are unknown.
o The UST dimensions are unknown.
o The installation dates of the USTs are unknown.
o It is unknown if piping was associated with the USTs but is assumed it was removed
during UST removal activities.
o The status of the USTs is “removed from ground”; the removal date of the USTs is
unknown.
o A release was associated with the former USTs based on soil contamination
determined by laboratory analysis. A soil sampling event was conducted in May
2019. Benzene was detected in one soil sample above established NCDEQ MSCCs.
Groundwater was not encountered beneath the site.
3. Non-UST Information
Former USTs N-6002A and B were removed and not replaced. No activity has been
documented in the area since closure and removal of the USTs.
4. Description of the Release
According to the Fort Liberty Directorate of Public Works (DPW), the two USTs at site
CCFTBR0149 had been removed at a prior date; however, the UST closure forms
detailing removal activities, size, and contents of the USTs were not available for review.
To comply with UST closure requirements, Aerostar SES LLC (Aerostar) conducted a
site assessment with environmental sampling in the area of the former USTs in May
2019. Four soil borings were advanced to evaluate soil quality and to facilitate the
collection of soil samples for laboratory analysis. Four confirmatory soil samples and a
field duplicate were collected and analyzed for VOCs by US EPA method 8260, SVOCs
by USEPA method 8270, and TPH EPH / VPH by MADEP method.

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One soil sample showed a benzene concentration of 0.0312 mg/kg which is above the
NCDEQ MSCC of 0.0056 mg/kg, but below the residential MSCC of 18 mg/kg. As such,
Aerostar recommended a NFA designation for the site. On January 31, 2020, the NCDEQ
responded to Aerostar’s request for NFA with a request for additional investigation of
former UST site N-6002 due to soil contamination in exceedance of the NCDEQ MSCCs.
5. Site Characteristics
The subject area is located off Logistics Street and Honeycutt Road. Currently the site is
a landscaped area and operates as part of the parking lot for building N-6002. No
additional information on the historical use of the area was provided. Future use of the
subject area is expected to remain the same.
6. Previous Activities
The USTs were removed from site at an unknown date prior to 2019. Soil sampling
conducted during a post closure site assessment indicated a benzene concentration in
excess of regulatory thresholds in the area of the former USTs.

C. RISK CHARACTERIZATION
Limited Site Assessment Risk Classification and Land Use Form

Part I – Groundwater/Surface-Water/Vapor Impacts

High Risk
1. Has the release contaminated any water supply well including any well used for non-
drinking purposes? YES NO
2. Is a water supply well used for drinking water located within 1,000 feet of the source area
of the release? YES NO
3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars,
industrial cooling water, or filling swimming pools) located within 250 feet of the source
area of the release? YES NO
4. Does ground water within 500 feet of the source area of the release have the potential for
future use (there is no other source of water supply other than the groundwater)?
YES NO

5. Do vapors from the release pose a threat of explosion because of accumulation of the
vapors in a confined space or pose any other serious threat to public health, public safety
or the environment? YES NO
If yes, describe.

6. Are there any other factors that would cause the release to pose an imminent danger to
the public health, public safety, or the environment? YES NO
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If yes, describe.

Intermediate Risk
7. Is a surface-water body located within 500 feet of the source area of the release?
YES NO
If YES, does the maximum groundwater contaminant concentration exceed the surface-
water quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10?
YES NO

8. Is the source area of the release located within an approved or planned wellhead
protection area as defined in 42 USC 300h-7(e)? YES NO
If YES, describe.

9. Is the release located in the Coastal Plain physiographic region as designated on a map
entitled “Geology of North Carolina” published by the Department in 1985?
YES NO
If YES, is the source area of the release located in an area in which there is recharge to an
unconfined or semi-confined deeper aquifer that is being used or may be used as a source
of drinking water? YES NO
If YES, describe.
The underlying unconfined Black Creek Aquifer is used as a source of drinking
water by the town of Spring Lake, NC, approximately five miles west of the
release area. The Black Creek Aquifer directly underlies the surficial aquifer in the
Fort Liberty, NC area. Drilling activity indicates that significant clay layers
separate the surficial and Black Creek Aquifers in the Fort Liberty area.
10. Do the levels of groundwater contamination for any contaminant exceed the gross
contamination levels established by the Department? YES NO

Part II – Land Use
Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary residences (permanent or
temporary)? YES NO
Describe.
No, the property is used as a heating plant and office building. A Land Use Map is
presented on Figure 3 in Appendix A.
2. Does the property contain a school, daycare center, hospital, playground, park, recreation
area, church, nursing home, or other place of public assembly? YES NO
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Describe.
The property operates as a parking lot and landscaped area for building N-6002.
3. Does the property contain a commercial (e.g., retail, warehouse, office/business space,
etc.) or industrial (e.g., manufacturing, utilities, industrial research and development,
chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial
enterprise, or is the land undeveloped? YES NO
Describe.
The property operates as a parking lot and landscaped area for building N-6002.
4. Do children visit the property? YES NO
Explain.
No, the property is not frequented by children.
5. Is access to the property reliably restricted consistent with its use (e.g. by fences, security
personnel, or both)? YES NO
Explain.
The property is within the Fort Liberty military base which requires permitted
access.
6. Do pavements, buildings, or other structures cap the contaminated soil? YES NO
Describe.
The contaminated soil is under a landscaped area.
If yes, what mechanisms are in place or can be put into place to ensure that the contaminated
soil will remain capped in the foreseeable future?

7. What is the zoning status of the property?
Municipal zoning requirements do not apply at Fort Liberty due to its status as a
Federal
Military Installation
8. Is the use of the property likely to change within the next 20 years? YES NO
Explain.
It is expected that the site will continue to be used as a parking area for building N-
6002.

Property Surrounding the Source Area of the Release
1. What is the distance from the source area of the release to the nearest primary or
secondary residence (permanent or temporary)?
The nearest primary residences are army barracks approximately 0.8 miles west of
the subject property off Honeycutt Road.

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2. What is the distance from the source area of the release to the nearest school, daycare
center, hospital, playground, park, recreation area, church, nursing home, or other place
of public assembly?
Daycare: 1.4 miles; School: 1.9 miles; Playground: 2.0 miles; Church: 2.9 miles;
Hospital: 3.3 miles; Nursing home: 3.1 miles.
3. What is the zoning status of properties in the surrounding area?
Municipal zoning requirements do not apply at Fort Liberty due to its status as a
Federal
Military Installation.
4. Briefly characterize the use and activities of the land and the surrounding area.
The immediate and surrounding area use consists of office buildings and associated
parking areas, a water tower, and motor pool compounds.

D. RECEPTOR INFORMATION
1. Water Supply Well(s)
There are no water supply wells within 1,500 feet of this site. This information is also
shown on Figure 4 in Appendix A and Table 7 in Appendix B.
2. Public Water Supplies
Are public water supplies available within 1,500 feet of the source area of the release?
YES NO
3. Surface Water
A tributary of the Texas Pond begins approximately 0.27-mile northeast of the subject
property.
4. Wellhead Protection Area(s)
The source area is not located in a wellhead protection area. There are no wellhead
protection areas within 1,500 feet of the source location.
5. Deep Aquifers in the Coastal Plain Physiographic Region
At Fort Liberty, two deep aquifers are located beneath the surficial aquifer. The Black
Creek Aquifer, immediately below the surficial aquifer, is usually reported to be an
unconfined aquifer receiving recharge from the surficial aquifer. Drilling activity
indicates that there are significant clay layers separating the surficial aquifer and the
Black Creek Aquifer in the Fort Liberty area. It is not believed that these clay layers are
laterally continuous; however, they do create some local zones of perched water. The
Upper Cape Fear Aquifer, located below the Black Creek Aquifer, is confined and
receives little or no recharge from the overlying aquifers.

The unconfined Black Creek Aquifer is found immediately beneath the surficial aquifer
and extends to a depth of approximately 125 feet bgs. There is no perceptible difference
16

in groundwater head between the surficial aquifer and the Black Creek Aquifer. Near Fort
Liberty, NC, one well in the Black Creek Aquifer is used as a source of drinking water by
the city of Spring Lake, NC. Spring Lake’s nearest municipal water supply wells are
located greater than five miles from the site.

The confined Upper Cape Fear Aquifer is found below the Black Creek Aquifer at a
depth of greater than 150 feet bgs. The groundwater head in the Upper Cape Fear Aquifer
has been found to be 28 feet less than the groundwater head in the Black Creek Aquifer.
Measurements were made at the North Carolina Research Division Seabrook Research
Station 15 miles east of Fort Liberty. The Upper Cape Fear Aquifer is not used as a
source of drinking water by any public water system near Fort Liberty. The nearest
known discharge point for the Upper Cape Fear Aquifer is the Cape Fear River east of
Fayetteville, NC, approximately 6 miles east of the subject site.
6. Subsurface Structure(s)
The office buildings on the subject site are serviced by water, sanitary sewer, gas, and
power. The exact location of the utility lines is unknown but are presumed to be
subsurface at a depth of approximately 3-10 feet.

E. LAND USE
1. Property Owners and Occupants
All property at the site or contiguous to the site is the property of the U.S. Department of
Defense (U.S. DoD).
2. Sensitive Land Use Features
Are sensitive land use features within 1,500 feet of the source area of the release?
YES NO

A small portion of wetland associated with the tributary to Texas Pond is within 1,500
feet northwest of the subject site as shown on Figure 4 in Appendix A.

F. SITE GEOLOGY AND HYDROGEOLOGY
As part of the LSA investigation, one soil boring, CCFTBR0149-SB-01 was advanced to
approximately 53 feet bgs. Soils consisted of interbedded silty sands, clayey sands, and
sands to total depth. Bedrock was not encountered in the boring conducted at the site.
Groundwater was encountered at approximately 47 feet bgs. The boring log is included in
Appendix C.

Based on a one-mile radius, the topography at the subject area is relatively flat with the
ground sloping gently east-northeast. Surface-water flow is expected to primarily flow
northeast towards the tributary of Texas Pond.

17

G. SAMPLING RESULTS
1. Phase I Investigation

Phase I drilling and sampling was completed on December 13, 2022. A sample location
map is presented on Figure 5 in Appendix A.

a. Soil Sampling and Analysis
Soil boring CCFTBR0149-SB-01 was advanced in the general center of the former
UST excavation area. The soil boring was advanced to a total depth of 53 feet bgs
using a sonic rig with a 6-inch outer diameter core barrel. Samples were continuously
collected from the soil boring and screened onsite with a MiniRae OVA-PID. The
onsite soil screening showed hydrocarbon vapor concentrations ranging from zero to
4.5 parts per million (ppm). Soil samples were collected from 6, 20, 30, 40, and 46
feet bgs and submitted for laboratory analysis. The boring log for soil boring
CCFTBR0149-SB-01 is included in Appendix C.

A USACE contracted laboratory analyzed the soil samples in accordance with Table
2 (Approved Methods for Soil Analysis during Advanced Phases of Petroleum UST
Release Investigations) of the NC UST Section “Guidelines for Sampling,” 15 July
2008. The soil samples were analyzed for VOCs, SVOCs, MADEP-VPH, MADEP-
EPH, hexavalent chromium, and total metals. In addition, the soil sample collected
from 6 feet bgs was also analyzed for pesticides and PCBs.

Laboratory analytical results for soil are compared to the NCDEQ Soil to Water
MSCCs, the NCDEQ residential soil cleanup level, and the NCDEQ industrial soil
cleanup level. Where NCDEQ regulatory thresholds were unavailable, the results are
compared to the USEPA RSL for residential or industrial soil. No analytes were
detected in excess of the soil to groundwater MSCCs. Analytical results in excess of
laboratory MDLs are as follow:
• Acetone was detected in the six-foot soil sample at an estimated quantity of 35
milligrams per kilogram (mg/kg). This exceeds the NCDEQ MSCC of 24 mg/kg but
is below the residential and industrial soil cleanup levels.
• Arsenic was detected in soil samples collected at 6, 30, and 40 feet bgs at
concentrations greater than the USEPA RSL for residential soil of 0.68 mg/kg but
below the industrial RSL of 3 mg/kg.
• Total chromium was detected in the 6-, 30-, and 40-foot soil samples at
concentrations greater than the NCDEQ MSCC of 3.8 mg/kg as well as the residential
soil cleanup level of 1.32 mg/kg. Total chromium was detected in the 20-foot soil
sample at a concentration of 1.9 mg/kg, which exceeds the residential soil cleanup
level only. No detections were found in excess of the industrial soil cleanup level for
total chromium.
• Hexavalent chromium was detected in the 6-foot soil sample at a concentration of
1.8 mg/kg. This concentration exceeds the residential soil cleanup level of 1.32 mg/kg
18

but is below the NCDEQ MSCC soil to groundwater and the industrial soil cleanup
levels.
Several other detections above laboratory MDLs were found within the soil samples
submitted for laboratory analysis; however, none of the other detections were above
regulatory standards. A soil sample exceedances map is presented on Figure 6 in
Appendix A. A summary of soil sample analytical results is presented on Table 4 of
Appendix B. Chain-of-custody and laboratory analytical results are included in
Appendix D.
b. Groundwater Sampling and Analysis
Following soil sampling activities, soil boring 149-SB-01 was converted into
temporary monitoring well 149-TW-01. Groundwater was encountered at 47.17 feet
bgs. The temporary monitoring well was advanced to a total depth of 51 feet bgs with
a 10-foot polyvinyl chloride (PVC) screen to facilitate the collection of one
groundwater sample for laboratory analysis of VOCs, SVOCs, PCBs, pesticides,
TPH-EPH, TPH-VPH, hexavalent chromium, and metals. Due to available water
column, the groundwater sample was analyzed for both total and dissolved metals.

Laboratory analytical results for groundwater from the LSA sampling are compared
to the NCDEQ groundwater quality standards (GWQS) and NCDEQ gross
contamination levels (GCLs). Where GWQSs and/or GCLs were unavailable, the
USEPA regional screening level for tap water is used.

• Bis(2-ethylhexyl) phthalate was detected at an estimated concentration of 3.1
micrograms per liter (µg/L). This concentration exceeds the NCDEQ GWQS for
bis(2-ethylhexyl) phthalate of 3.0 µg/L
• Total chromium was detected at a concentration of 15 µg/L. This concentration
exceeds the NCDEQ GWQS for total chromium of 10 µg/L. Hexavalent chromium
was non-detect.
• Magnesium was detected at a concentration of 560 µg/L. This concentration
exceeds the USEPA RSL for tap water of 28 µg/L for magnesium.
• Sodium was detected at a concentration of 13,000 µg/L. This concentration
exceeds the USEPA RSL for tap water of 2,000 µg/L.
Several other detections above laboratory MDLs were found within the groundwater
sample submitted for laboratory analysis; however, none of the other detections were
above regulatory standards. A groundwater sample exceedances map is presented on
Figure 7 in Appendix A. A summary of groundwater sample analytical results is
presented on Table 6 of Appendix B. Chain-of-custody and laboratory analytical
results are included in Appendix D.

2. Phase II Investigation
Based on current information a Phase II investigation is not warranted for the subject site
at this time.
19

H. CONCLUSIONS AND RECOMMENDATIONS
Soil samples collected during UST closure and removal indicated that soil contamination
above NCDEQ screening levels is present beneath the subject site. At the request of the Fort
Liberty Environmental Division, USACE-SAS conducted a LSA at the subject site.
o Soil analysis of samples from the former UST area collected during the current LSA
shows that soil contamination of acetone, arsenic, total chromium, and hexavalent
chromium exists beneath the site in excess of regulatory standards.
o Groundwater analysis of a sample collected from the site during the current LSA
shows that bis(2-ethylhexyl) phthalate, total chromium, magnesium, and sodium exist
at the site in excess of regulatory standards.
o Free product has not been identified at this site. There are no groundwater receptors
within 1,500 feet, and no known high-risk factors apply at this site.
o Current land use poses negligible risks to residents, site workers or visitors and
current protocols at this site are enough to protect human life and the environment.

I. FREE PRODUCT INVESTIGATION AND RECOVERY
A free product investigation and recovery are not applicable at this site. No free product has
been identified.

J. PROPOSED REMEDY FOR CONTAMINATION
Based on current information, acetone, arsenic, total chromium, and hexavalent chromium
were detected in the soil samples collected from the site at concentrations above regulatory
limits. Acetone is a common laboratory artifact and was only detected in the 6-foot soil
sample at a concentration above NCDEQ MSCCs but below both residential and industrial
clean up levels. As such, the single acetone exceedance is not a cause for concern for the site.
Arsenic was detected at concentrations above the USEPA RSL for residential soil but below
the RSL for industrial soil. Arsenic is known to naturally occur at levels greater than the
USEPA RSL for residential soil across the Fort Liberty area (Philip Hunter, 2005). As such,
the arsenic detected within the soil is considered background concentrations and not a
concern for the site. Total chromium was detected above all regulatory thresholds in one or
more soil samples collected from the site. Hexavalent chromium was only detected in the six-
foot soil sample at a concentration exceeding the residential soil cleanup level, but below the
NCDEQ MSCC and the industrial soil cleanup level. The lack of hexavalent chromium
detections above regulatory thresholds in all soil samples is indicative that most of the
chromium in soil exists as chromium III. As the site operates as an industrial facility, access
by the general public is limited, and that there is greater than 40 feet between the soil
exceedance and the water table, the singular hexavalent chromium exceedance above the
residential soil cleanup level is not considered an environmental concern for the site.
Groundwater was encountered at approximately 47 feet bgs at the time of sampling. Due to
site conditions and water column availability, the groundwater sample was analyzed for both
total and dissolved metals. Bis(2-ethylhexyl) phthalate was detected at an estimated
20

concentration of 3.1 µg/L which exceeds the NCDEQ GWQS of 3 µg/L for bis(2-ethylhexyl)
phthalate but is below the GCL. Bis(2-ethylhexyl) phthalate is a common component in
plasticizers and the minor detection is likely contributed to cross contamination from the
equipment used at the time of sampling. As such, the bis(2-ethylhexyl) phthalate detection in
groundwater is not a concern for the site. Total chromium was detected at an estimated
concentration of 15 µg/L which is above the NCDEQ GWQS of 10 µg/L for chromium but
below the GCL. Hexavalent chromium was not detected in the one groundwater sample
submitted for laboratory analysis. The lack of a hexavalent chromium exceedance is
indicative that the chromium in groundwater exists as chromium III and is not an
environmental concern for the site. Manganese was detected at a concentration of 560 µg/L
which exceeds the USEPA RSL for tap water of 430 µg/L. Sodium was detected at a
concentration of 13,000 µg/L which exceeds the USEPA RSL for tap water of 2000 µg/L. As
manganese and sodium do not have established NCDEQ GWQSs or GCLs and groundwater
at the site is not expected to be utilized for public water supply, the manganese and sodium
exceedances above the USEPA RSLs for tap water are not an environmental concern for the
site. Further investigation is not warranted at this time and USACE-SAS recommends a NFA
designation for the site.

K. FIGURES
The figures for this report immediately follow the report narrative.

L. TABLES
The tables for this report follow the report figures.

M. APPENDICES
The appendices for this report follow the report figures and tables.
APPENDIX A
FIGURES

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St
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medStream
U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
Geology, Hydrogeology, and
HTRW Design Section
SITE VICINITY MAP
Fort Bragg, North Carolina
Figure: 1 Date: Oct 2021
N
1" = 625'
CCFTBR0149
Building N-6002
Site CCFTBR0149
$#$#
Hone ycutt

R
d
Honeycutt

R
d
N6002
N-6002-A N-6002-B
SB-01/TW-01
U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
Geology, Hydrogeology, and
HTRW Design Section
CCFTBR0149 Site Layout Former Underground Storage Tanks
N-6002-A and N-6002-B
Fort Bragg, North Carolina
July 2023 Figure 2
SB-01/TW-01
#$ UST N-6002-A
#$ UST N-6002-B
Building
0 20 4010Feet
1 inch equals 20 feet
··· 1:1 1500' RadiusCJ
0.030.07
N A
0.13 0.2 0.26 Miles
U.S. ARMY CORPS OF ENGINEERS SAVANNAH DISTRICT Geology, Hydrogeology, and
HTRW Design Section
Fort Bragg, North Carolina
CCFTBR0149
Land Use Map
July 2023 Figure 3
$#$#
Hone ycutt

R
d
Honeycutt

R
d
N6002
N-6002-A N-6002-B
SB-01/TW-01
U.S. ARMY CORPS OF ENGINEERS
SAVANNAH DISTRICT
Geology, Hydrogeology, and
HTRW Design Section
CCFTBR0149 Sample Location Map
Former Underground Storage Tanks
N-6002-A and N-6002-B
Fort Bragg, North Carolina
July 2023 Figure 5
SB-01/TW-01
#$ UST N-6002-A
#$ UST N-6002-B
Building
0 20 4010Feet
1 inch equals 20 feet
Cleanup Levels MSCCs Residential
Acetone 24 14000
Arsenic NE 0.68*
Total Chromium 3.8 1.32
Hexavalent Chromium 3.8 1.32
Industrial
21000
3.0* 6.54
6.54
149-SB-1
149-SB-1-6-12-22
Acetone
Arsenic
Total Chromium
Hexavalent Chromium
149-SB-1-20-12-22
Total Chromium 1.9
149-SB-1-30-12-22
Arsenic
Total Chromium
149-SB-1-40-12-22
Esri G8mmunity Maps Ciontributors, County of Cumberland, State of North Carolina DOT,© OpenStreetMap, Microsoft, Esri,
HERE, Garmin, SafeGraph, GeoTechnologies, Inc, METI/NASA, USGS, EPA, NPS, US Census Bureau, USDA, NC CGIA, Maxar,
Microsoft
Cl Building
A.Sample Location
Values are reported in milligrams per kilogram
J = Estimation below quantization threshold
Q = One or more quality control criteria failed NE = Not Established Soil to Water MSCCs = Maximum Soil Contaminant
Concentration Residential Cleanup Level exceedances are indicated in blue MSCC exceedances are indicated in red *
EPA RSL for residential or industrial soil where
NCDEQ values are not established
0
N A
US Feet
12.5 25 50
U.S. ARMY CORPS OF ENGINEERS SAVANNAH DISTRICT Geology, Hydrogeology, and
HTRW Design Section
Fort Bragg, North Carolina
CCFTBR0149 Soil Exceedances Map
July 2023 Figure 6
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APPENDIX B
TABLES

Table 1: Site History-UST System and Other Release Information
Incident Number and Name: 42251, UST N-6002A/B
UST ID
Number
Current/ Last
Contents
Previous
Contents*
Capacity
(gallons)
Construction
Details**
Tank
Dimensions
Associated
Piping and
Pumps
Date installed
(mm/dd/yy)
Status of
UST***
Was Release
Associated with
the UST System?
UST N-6002A unknown unknown unknown unknown unknown unknown unknown
Permanently
closed by
removal
Yes
UST N-6002B unknown unknown unknown unknown unknown unknown unknown
Permanently
closed by
removal
Yes
Incident
Number
Material
Released Date of Release
42251 unknown unknown
* Gasoline (Unleaded or leaded) diesel, used oil, waste oil, aviation fuel etc., or pesticides, non-halogenated or halogenated solvents, etc. ** Fiberglass (single or double-walled), steel (single or double-walled), steel with FRP (single or double-walled), steel with liner, other, unknown.*** Currently operational, not in use, or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removal (specify date).
Detected during site assessment
Description of Release
Table 2: Site History - UST Owner/Operator and Other Responsible
Incident Number and Name: 42251, UST N-6002A/B
UST ID Number:N-6002A/B F000003
City:State:Zip:
Fort Liberty North Carolina 28310
Incident Number:
City:State:Zip:
N/A N/A N/A
Party Information
Street Address:
Name of Other Responsible Party:Dates of Release: (mm/dd/yy to mm/dd/yy)
Telephone Number:
[phone]
42251
2175 Reilly Street, Stop A
Environmental Sustainment Division
IMBG-PWE-M
Unknown
Facility ID Number:
Name of Owner:Dates of Operation: (mm/dd/yy to mm/dd/yy)
Fort Bragg Directorate of Public Works
N/A
N/A
N/A unknown
Telephone Number:
Street Address:
Table 3: Summary of Initial Soil Assessment Analytical Results
Incident Number and Name: 42251, UST N-6002A/B
Date Collected
(mm/dd/yy)Source Area
Sample
Depth
(ft BGS)Benzene5/17/19 Former UST 15 0.0312 0.727 0.0122 J 0.193 0.159 3.54 U 4.54 J
5/17/19 Former UST 15 0.00152 U 0.152 0.00379 U 0.00758 U 0.0152 U 3.56 U 3.77 J
5/17/19 Former UST 15 0.00136 U 0.135 0.00341 U 0.00682 U 0.0136 U 2.54 J 5.19 J
5/17/19 Former UST 15 0.00136 U 0.0896 0.00339 U 0.00678 U 0.0136 U 3.16 J 5.61 J
0.0072 16 8 5.4 6 31 Immobile
12 9380 60.3 1250 3120 469 31200
59.4 140000 297 18600 46700 12264 467000
Notes:ft BGS: Feet below Ground SurfaceNCDEQ MSCC = North Carolina Department of Environmental Quality Maximum Soil Contamination Concetration-- = Regulatory value not established for the indicated constituentDetections in bold print are greater than the laboratory method detection limit (MDL)Detections in red print exceeded the NCDEQ soil to water MSCCs and/or the NCDEQ Residential Soil Threshold Level
J: chemical detected but below quantitization threshold. Value is an estimate.
NCDEQ Residential Soil Cleanup Levels (mg/kg)
NCDEQ Industrial/Commercial Soil Cleanup Levels (mg/kg)
Analytical Method:
Contaminant of Concern (mg/kg):
FTB-N-6002-UST-SS-001-15
Sample ID
NCDEQ Soil to Water (mg/kg)
FTB-N-6002-UST-SS-002-15
FTB-N-6002-UST-SS-003-15
FTB-N-6002-UST-SS-004-15
EPH MADEP
C19-C36 AliphaticsC11-C22 AromaticsVOCs
XylenesEthylbenzeneToluene2-Butanone
Table 4: Summary of LSA Phase I Soil Analytical Results
Incident Number and Name: 42251, UST N-6002A/B
VOC - Method
8260D
Sample ID Date Collected (mm/dd/yy)Source Area
Sample Depth (ft BGS)AluminumAntimonyCalciumSodiumPotassium149-SB-1-6-12-22 12/13/2022 UST 6 35 JQ 1.4 6200 0.18 J 8.1 0.15 0.044 J 34 J 19 1.8 M 0.4 3.1 8000 17 8.8 1.6 1.6 J 28000 U 140 210 16 8.2 3.3 J 3.8 U 0.22 J 0.15 J
149-SB-1-20-12-22 12/13/2022 UST 20 25 UQ 0.32 J 2500 300 U 0.89 0.049 J 40 U 30 J 1.9 0.31 J 0.047 J 0.77 550 1.2 0.39 J 750 U 300 U 25000 U 6.4 J 28 2 2000 U 4.0 U 2.0 J na na
149-SB-1-30-12-22 12/13/2022 UST 30 34 UQ 1.6 1700 340 U 0.82 0.050 J 46 U 14 J 5 0.24 J 0.12 2 2900 2.2 2 860 U 0.200 J 14 J 10000 U 21 J 4.3 2300 U 4.9 U 2.2 J na na
149-SB-1-40-12-22 12/13/2022 UST 40 23 UQ 0.96 2100 330 U 1.3 0.07 0.027 J 76 21 0.19 JM 0.016 1.3 1200 1.7 1.7 1.6 330 U 28000 U 8.3 J 26 J 5.1 2200 U 4.2 U 3.3 U na na
149-SB-1-46-12-22 12/13/2022 UST 46 26 UQ 0.11 J 1800 310 U 0.9 0.046 J 41 U 39 J 1.3 0.64 M 0.091 1 590 1.7 0.96 J 780 U 310 U 26000 U 4.6 J 22 J 2.9 2100 U 4.1 U 1.9 J na na
24 NE NE NE 620 NE NE NE 3.8 3.8 NE NE NE 270 NE NE NE NE NE NE NE NE NE 540 NE NE
14000 0.68*77000*31*3100 160*7.1*NE 1.32 1.32 23*3100*55000*400 1800*1500*390*NE NE NE 390*23000*31200 1560 2.0*1.9*
210000 3*1100000*470*46,000 2300*100*NE 6.54 6.54 350*47000*820000*400 26000*22000*5800*NE NE NE 5800*350000*467000 23300 9.3*8.5*
Notes:ft BGS: Feet below Ground Surface.Detections in bold print exceed laboratory method detection limits (MDLs)Detections in red print exceeded the NCDEQ soil to water MSCCsDetections in blue print exceeded the NCDEQ Residential Soil Threshold LevelDetections in green print exceeded the NCDEQ Industrial Soil Threshold LevelVOCs = Volatile Organic Compounds
SVOCs = Semivolatile Organic CompoundsRCRA Metals = Resource Conservation and Recovery Act MetalsNCDEQ = North Carolina Department of Environmental QualityMSCC = Maximum Soil Contaminant ConcentrationNE = Not EstablishedMADEP VPH = Massachusettes Department of Environmental Protection Volatile Petroleum Hydrocarbons* EPA Regional Screening Level for Residential or Industrial Soil used where NCDEQ soil cleanup levels are not establishedResults are reported in milligrams per kilogram (mg/kg)E = Quantitation of compound exceeded the calibration rangeB = The analyte was detected above one-half the reporting limit in an associated blank
J: chemical detected but below quantitization threshold. Value is an estimate. Q = One or more quality control criteria failed M = Manual integrated compound ManganeseSeleniumResidential Soil Cleanup Levels (mg/kg)
NCDEQ Soil to Water MSCCs (mg/kg)NickelAnalytical Method:C9-C18 Aliphatics4,4'-DDE4,4'-DDTPesticides & PCBs - Method 8081B/8082AMADEP EPH/VPH
C19-C36 AliphaticsContaminant of Concern (mg/kg):
Metals - Method 6020B/7196A
Chromium, HexavalentCobaltZincCopperIronU = Value not detected above laboratory method detection limits (MDLs); reported value is the detection limit VanadiumBariumBerylliumNCDEQ Industrial/Commercial Soil Cleanup Levels (mg/kg) LeadChromium (Total)AcetoneArsenicCadmiumMagnesium
Table 5: Field Screening Results
Incident Number and Name: 42257, UST N-6002A/B
Date
Collected
Turbidity
(ntu)
Temperature
(°C)
Dissolved
Oxygen (%)
Conductivity
(µS/cm)pH
Oxygen
Reduction
Potential (mV)
12/14/2022 740.0 18.45 4 4.38 6.67 -46.5
Notes:
ntu = nephlowmetric turbidity units°C = Degrees celsius
µS/cm = microsemens per centimetermV = milivolts
Well ID
Parameter
149-TW-01
Table 6: Summary of LSA Phase I Groundwater Analytical Results
Incident Number and Name: 42251, UST N-6002A/B
VOCs -
Method
8260D
SVOCs -
Method
8270E
Well or SW
ID
Date
Collected
(mm/dd/yy)Sample ID
Incident
Phase LSA CalciumCobaltChormiumCopperPotassiumMagnesiumManganeseSodiumLeadVanadiumAluminumBariumCalciumCobaltPotassiumMagnesiumSodiumLead149-TW-01 12/14/22 149-TW-01 42251 3.8 JQ 3.1 J 900 19 23000 2.9 15 J 20 6900 2800 1300 450 9900 1.0 J 4.9 J 32 2.5 J 430 23 36000 1.6 9 U 200 3700 1800 560 13000 0.37 J 2.4 J 35 J 130 M 36 JM
6,000,000 135 NE 700,000 NE NE 10,000 NE NE NE NE NE NE 15,000 NE NE NE NE 700,000 NE NE 10,000 NE NE NE NE NE 15,000 NE NE NE NE
6,000.0 3.0 2000*700.0 NE 6*10 1,300*14000*NE NE 28*2000*15 220*86*6000*2000*700 NE 6*10 14000*NE NE 430*2000*15 220*NE NE NE
Notes:VOCs = Volatile Organic CompoundsSVOCs = Semi-Volatile Organic CompoundsNCDEQ = North Carolina Department of Environmental QualityGCLs = Gross Contamination LevelsGWQS = Groundwater Quality StandardJ = Estimated concentration between the reporting limit and the method detection limitU = Undetected at the limit of detectionNE = Not EstablishedDetections in bold print meet or exceed the laboratory method detection limitResults are reported in micrograms per liter (µg/L)
NE = Not Established*USEPA maximum contaminant level for groundwater or USEPA Regional Screening Level for tapwater where NCDEQ GWQS are not available
Analytical Method:
NCDEQ 15A NCAC 02L GWQS
NCDEQ GCLs
Contaminant of Concern (ug/L):C11-C22 AromaticsIronManganeseNickelBariumAluminumBis (2-ethylhexyl) phthalateAcetoneMetals Total Recoverable - Method SW846 6020B MADEP EPH/VPHMetals Dissolved - Method SW846 6020B
C9-C18 AliphaticsHexavalent ChromiumZincNickelIronC19-C36 Aliphatics
Table 7: Public and Private Water Supply Well and Other Receptor Information
Incident Number and Name: 42251, UST N-6002A
Well #Well Owner/ User Address Phone
Number Well Use Well Depth
(ft BGS)
Type of
Well
Well
Casing
Depth
(ft BGS)
Well
Screen
Interval
(ft BGS)
Distance from
Source Area
of Release (ft)
Up/Down-
Gradient
Ft. BGS: Feet below ground surface.
Other Receptors:
Receptor ID:Description:Location:Contact:
Distance
from
Source (ft)
Black Creek Aquifer Unconfined Aquifer <150 feet bgs --<150 feet
Cape Fear Aquifer Confined Aquifer >150 ft bgs -->150 feet
(Other public water supplies, reservoirs water supply lines, surface-water bodies, wellhead protection areas, recharge areas for deep aquifers, subsurface structures).

There are no known public or private water supply wells within 1,500 feet of the former UST N-6002A/B
--N/APotable Water
Up/Down-Gradient
N/A
Usage
Potable Water
Phone Number:
--
Table 8: Property Owners/Occupants
Incident Number and Name: 42251, UST N-6002A/B
Owner/Occupant D28
(Last, First MI)Tax Parcel Number/Map ID Address
This table is not applicable at this site. All property at this site, or on which the contamination is
likely to migrate, is the property of the U. S. Department of Defense.
Table 9: Monitoring and Remediation Well Construction Information
Incident Number and Name: 42251, UST N-6002A/B
Well ID
Date
Installed
(m/dd/yy)
Date Water
Level
Measured
(m/dd/yy)
Well
Casing
Diameter
(in.)
Well
Casing
Depth
(ft BGS)
Screened
Interval
(ft BGS)
Depth of
Well
(ft BGS)
Top of
Casing
Elevation
* (ft)
Depth to
Water from
top of
Casing (ft)
Free
Product
Thickness*
* (ft)
Ground-Water
Elevation* (ft)Comments
TW-01 12/13/22 12/14/22 1''41.0 41'-51'51.0 NA 47.17 NA NA Temp. well
Notes:
* Top of casing and groundwater elevation not measured
** If free product is present in a well, ground-water elevation should be calculated by: [Top of Casing Elevation - Depth to Water] +
[free product thickness x 0.8581].N/A : Not Applicable or Not Available.
ft BGS: Feet below ground surface.
Temp.: Well was temporary and abandoned after sampling.
Table 10: Free Product Recovery Information
Incident Number and Name: 42257, UST 8-1221
Date
(m/dd/yy)Well ID#
Product Type
(Gas, Diesel,
etc.)
Free
Product
Recovery
Method*
Product
Thickness
before
Recovery
(Inches)
Product
Thickness
after
Recovery
(Inches)
Amount of
Vaporized
Product
Amount of
Liquid
(Water and
Product)
Amount of
Liquid
Product
Total
Amount of
Product
Recovered
(Gallons)
Table Not Used
Table 11: Cumulative Volume of Free Product Recovered from Site
Incident Number and Name: 42257, UST 8-1221
Date of Recovery event
(m/dd/yy)
Total Volume Recovered from Site During
Current Recovery Event (Gallons)
Cumulative Total of Volume Recovered to Date
from All recovery Events (Gallons)
Table Not Used
Table 12: Current and Historical Groundwater Elevations and Free Product Thickness
Incident Number and Name: 42257, UST 8-1221
Well ID #Date
Screened Interval Top
of Screen - Bottom of
Screen
Uncorrected Depth
to Water (Feet)
Free Product
Thickness (Feet)
Depth to Water*
Corrected for Free
Product Thickness
(Feet)
Top of Casing
Elevation (msl)
Ground-Water Surface
Elevation (msl)
Table Not Used
Table 13: Land Use
Incident Number and Name: 42257, UST 8-1221
Map ID#
Date
Determined
Land Use Feature (Include
Zoning)
Distance and
Direction From
Source Area
1 11/20/2020 DOD property 1000+ feet
Location
(complete street address if applicable)
Adjoining property in all directions.
APPENDIX C
SOIL BORING LOG

-2.0
-5.0
-10.0
-12.0
-14.0
-17.0
-18.0
-30.0
-32.0
2.0
5.0
10.0
12.0
14.0
17.0
18.0
30.0
32.0
Sampled from 5-6 ft bgl.149-SB-1-6-12-22, 1140
Sampled from 19-20 ft bgl.149-SB-1-20-12-22, 1215
Sampled from 29-30 ft bgl.149-SB-1-30-12-22, 1330
SAND (SP-SM), reddish yellow, fine grained,
moist, few clay, trace gravel, no odor, nostaining.
CLAY (CL), dark red, fine grained, moist, few
sand, no odor, no staining.
SAND (SM), reddish yellow, fine grained, moist,
no odor, no staining.
SAND (SP-SM), reddish yellow, fine grained,
moist, trace clay, no odor, no staining.
SAND (SP), reddish yellow, fine to medium
grained, moist, trace silt, no odor, no staining.
CONCRETE SLAB.
Gravel Subbase
SAND (SP), very pale brown, fine to mediumgrained, moist, trace silt, no odor, no staining.
SAND (SP-SM), dark brown, fine grained, moist,
no odor, no staining.
SAND (SP), very pale brown to reddish yellow,
fine to medium grained, moist, trace silt, noodor, no staining.
SC-1
SC-2
SC-3
0.6
0
0
0
0
2
0.3
0.6
0.4
0
0.3
0
0.2
1
0.4
1.2
0.3
0.5
0.3
0
0.1
0.3
1.2
2
4.5
1.7
3.8
0.1
N/A
14. ELEVATION GROUND WATER
SHEET
---
DISTURBED
6. THICKNESS OF OVERBURDEN
7. DEPTH DRILLED INTO ROCK
8. TOTAL DEPTH OF BORING
STARTEDVERTICAL
1. PROJECT
UNDISTURBED
2. HOLE NUMBER
18. SIGNATURE AND TITLE OF INSPECTOR
Terrasonic 150CC
BEARING
3. DRILLING AGENCY
2 1
OF
COMPLETED15. DATE BORING
DEG FROM
VERTICAL
HORIZONTAL
INSTALLATION
0
6 0
INCLINED
USACE, Savannah District
4. NAME OF DRILLER
5. DIRECTION OF BORING
9. COORDINATE SYSTEM
10. SIZE AND TYPE OF BIT
Fort Liberty Site 149 LSA
>50'
53'
LOCATION COORDINATES
16. ELEVATION TOP OF BORING
VERTICAL
Ken Diediker, Geologist
0'
Kyle Killebrew
17. TOTAL CORE RECOVERY FOR BORING
12/13/22
SHEETSDRILLING LOG
12. TOTAL SAMPLES
13. TOTAL NUMBER CORE BOXES
149-SB-1/149-TW-1
DIVISION
11. MANUFACTURER'S DESIGNATION OF DRILL
See Remarks
12/13/22
Boring Designation 149-SB-1/149-TW-1
Boring Designation 149-SB-1/149-TW-1FEB 08
ELEV
LEGENDDEPTH
SAS FORM 1836-A
0
5
10
15
20
25
30
35
REMARKSWELLRecovery %FIELD CLASSIFICATION OF MATERIALS
(Description)
SHEET 1 of 2
SAMPLENUMBER PIDppm
70
100
100
Fort Liberty
35.144491, -78.958275
South Atlantic
Reading Depth Notes
-47.0
-48.5
-53.0
47.0
48.5
53.0
24 hours 47.17 ft BGS 12/14/2022
Sampled from 39-40 ft bgl.149-SB-1-40-12-22, 1400
TW-1 screened interval from 41-51' BGS.
2" x 10', 0.010 slot screen.
Sampled from 45-46 ft bgl.149-SB-1-46-12-22, 1435
SAND (SP), very pale brown to reddish yellow,
fine to medium grained, moist, trace silt, noodor, no staining. (continued)
Very pale brown mottled with very pale red.
SAND (SC), very pale brown, fine grained, wet,
little clay, no odor, no staining.
SAND (SP), very pale brown, fine to mediumgrained, wet, trace silt, no odor, no staining.
Water Level Data
SC-4
SC-5
SC-6
0.1
1.7
0.6
0.6
0.2
0.2
1.6
0
0
0
0.4
0.6
0.1
0
0
0
2
Fort Liberty Site 149 LSA
SHEETS
HORIZONTAL VERTICALPROJECT
SHEET
OF
COORDINATE SYSTEM
2
ELEVATION TOP OF BORINGLOCATION COORDINATES
DRILLING LOG (Cont Sheet)INSTALLATION
0'
Boring Designation 149-SB-1/149-TW-1
Boring Designation 149-SB-1/149-TW-1FEB 08
ELEV
LEGENDDEPTH
SAS FORM 1836-A
35
40
45
50
REMARKSWELLFIELD CLASSIFICATION OF MATERIALS
(Description)
SHEET 2 of 2
SAMPLENUMBER PIDppm
100
100
100
Recovery %Goundwater:
47.17' bgs, 24 hours after drilling.
Fort Liberty
35.144491, -78.958275
ANALYTICAL REPORT
PREPARED FOR
Attn: Ms. Kellie Arstino
Sure-BioChem Laboratories LLC
1000 Atlantic Ave
Camden, New Jersey 08104
Generated 1/18/2023 9:02:25 AM
JOB DESCRIPTION
CLFTBR0149 Ft. Bragg
JOB NUMBER
680-227663-1
See page two for job notes and contact information.
Savannah GA 31404
5102 LaRoche Avenue
Eurofins Savannah
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Eurofins Savannah
Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies
Job Notes
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available. Any
exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report may not be
reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the person who
signed this report.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project
Manager.
Authorization
Generated
1/18/2023 9:02:25 AM
Authorized for release by
Jerry Lanier, Project Manager I
[e-mail]
[phone]
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Definitions/Glossary
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Qualifiers
GC/MS VOA
Qualifier Description
J Estimated: The analyte was positively identified; the quantitation is an estimation
Qualifier
M Manual integrated compound.
Q One or more quality control criteria failed.
U Undetected at the Limit of Detection.
GC/MS Semi VOA
Qualifier Description
J Estimated: The analyte was positively identified; the quantitation is an estimation
Qualifier
M Manual integrated compound.
Q One or more quality control criteria failed.
U Undetected at the Limit of Detection.
GC VOA
Qualifier Description
D The reported value is from a dilution.
Qualifier
M Manual integrated compound.
Q One or more quality control criteria failed.
U Undetected at the Limit of Detection.
GC Semi VOA
Qualifier Description
D The reported value is from a dilution.
Qualifier
J Estimated: The analyte was positively identified; the quantitation is an estimation
J1 Estimated: The quantitation is an estimation due to discrepancies in meeting certain analyte-specific quality control criteria.
M Manual integrated compound.
Q One or more quality control criteria failed.
U Undetected at the Limit of Detection.
HPLC/IC
Qualifier Description
D The reported value is from a dilution.
Qualifier
H Sample was prepped or analyzed beyond the specified holding time
J Estimated: The analyte was positively identified; the quantitation is an estimation
M Manual integrated compound.
U Undetected at the Limit of Detection.
Metals
Qualifier Description
J Estimated: The analyte was positively identified; the quantitation is an estimation
Qualifier
U Undetected at the Limit of Detection.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
Eurofins Savannah
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Definitions/Glossary
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Glossary (Continued)
These commonly used abbreviations may or may not be present in this report.
MCL EPA recommended "Maximum Contaminant Level"
Abbreviation
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Savannah
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Sample Summary
Client: Sure-BioChem Laboratories LLC Job ID: 680-227663-1
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID Client Sample ID Matrix Collected Received
680-227663-1 149-SB-1-6-12-22 Solid 12/13/22 11:40 12/15/22 09:00
680-227663-2 149-DUP-1-12-22 Solid 12/13/22 12:00 12/15/22 09:00
680-227663-3 149-SB-1-20-12-22 Solid 12/13/22 12:15 12/15/22 09:00
680-227663-4 149-SB-1-30-12-22 Solid 12/13/22 13:30 12/15/22 09:00
680-227663-5 149-SB-1-40-12-22 Solid 12/13/22 14:00 12/15/22 09:00
680-227663-6 149-SB-1-46-12-22 Solid 12/13/22 14:35 12/15/22 09:00
680-227663-7 FB-12-22 Water 12/14/22 15:00 12/15/22 09:00
680-227663-8 EQB-12-22 Water 12/14/22 15:20 12/15/22 09:00
680-227663-9 149-TW-01 Water 12/14/22 15:30 12/15/22 09:00
680-227663-10 DUP-TW-01 Water 12/14/22 16:00 12/15/22 09:00
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Case Narrative
Client: Sure-BioChem Laboratories LLC Job ID: 680-227663-1
Project/Site: CLFTBR0149 Ft. Bragg
Job ID: 680-227663-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-227663-1
Receipt
The samples were received on 12/15/2022 9:00 AM. Unless otherwise noted below, the samples arrived in good condition, and, where
required, properly preserved and on ice. The temperatures of the 3 coolers at receipt time were 0.9°C, 1.0°C and 1.1°C
GC/MS VOA
Method 8260D_DOD5: Surrogate recovery for the following samples were outside the upper control limit: FB-12-22 (680-227663-7),
EQB-12-22 (680-227663-8), 149-TW-01 (680-227663-9), DUP-TW-01 (680-227663-10) and (MB 680-757008/9). This sample did not
contain any target analytes; therefore, re-extraction and/or re-analysis was not performed.
Method 8260D_DOD5: The laboratory control sample (LCS) and / or laboratory control sample duplicate (LCSD) for analytical batch
680-757008 recovered outside control limits for the following analytes: Chloroethane. This analyte was biased high in the LCS and was
not detected in the associated samples; therefore, the data have been reported.
Method 8260D_DOD5: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated
with preparation batch 680-755487 and analytical batch 680-756853.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC/MS Semi VOA
Method 8270E_DOD5: Surrogate Nitrobenzene-d5 in the MB for preparation batch 680-756109 and analytical batch 680-756690 recovered
outside control limits. The samples associated with this MB have passing surrogates; therefore, the samples have been reported.
Method 8270E_DOD5: The laboratory control sample (LCS) for preparation batch 680-756109 and analytical batch 680-756690 recovered
outside control limits for the following analyte: 3,3'-Dichlorobenzidine. This analyte was biased high in the LCS and was not detected in
the associated samples; therefore, the data have been reported.
Method 8270E_DOD5: The RPD of the laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) for preparation
batch 680-756109 and analytical batch 680-756690 recovered outside control limits for the following analytes: 3,3'-Dichlorobenzidine.
Method 8270E_DOD5: Azobenzene was biased low in the LCS and LCSD. This compound was added as part of a revised analyte list
requested by the client. (LCS 680-756109/2-A) and (LCSD 680-756109/3-A)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Hydrocarbons
Method MAVPH: The continuing calibration verification (CCV) and LCS/LCSD associated with batch 410-330695 recovered outside
acceptance criteria, low biased, for Methyl tert-butyl ether. The samples were re-analyzed outside the method required holding time and
Methyl tert-butyl ether is within limits. The sample result for Methyl tert-butyl ether in the re-analysis is non-detect. Results are reported
from the initial trial. FB-12-22 (680-227663-7), EQB-12-22 (680-227663-8), 149-TW-01 (680-227663-9) and DUP-TW-01 (680-227663-10)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC Semi VOA
Method MAEPH_DOD: The breakthrough for naphthalene and 2-methylnaphthalene in the LCS is 2%. The breakthrough for naphthalene
is 2% and the breakthrough for 2-methylnaphthalene is 1% in the LCSD. The method requirement for breakthrough is <5%. FB-12-22
(680-227663-7), EQB-12-22 (680-227663-8), 149-TW-01 (680-227663-9) and DUP-TW-01 (680-227663-10)
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Case Narrative
Client: Sure-BioChem Laboratories LLC Job ID: 680-227663-1
Project/Site: CLFTBR0149 Ft. Bragg
Job ID: 680-227663-1 (Continued)
Laboratory: Eurofins Savannah (Continued)
Method MAEPH_DOD: The breakthrough for naphthalene and 2-methylnaphthalene in the LCS and LCSD is <1%. The method
requirement for breakthrough is <5%. 149-SB-1-6-12-22 (680-227663-1), 149-DUP-1-12-22 (680-227663-2), 149-SB-1-20-12-22
(680-227663-3), 149-SB-1-30-12-22 (680-227663-4), 149-SB-1-40-12-22 (680-227663-5) and 149-SB-1-46-12-22 (680-227663-6)
Method MAEPH_DOD: 1-Chlorooctadecane (Surr) recovery for the following sample was outside of acceptance limits: DUP-TW-01
(680-227663-10). There was insufficient sample to perform a re-extraction; therefore, the data have been reported.
Method MAEPH_DOD: For analytical batch 410-331708, the breakthrough for naphthalene and 2-methylnaphthalene in the LCS is 3%.
The breakthrough for naphthalene and 2-methylnaphthalene in the LCSD is <1%. The method requirement for breakthrough is
<5%.149-TW-01 (680-227663-9)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Pesticides/PCBs
Method 8081B_8082A_D5: The following sample: 149-TW-01 (680-227663-9) was decanted prior to preparation due to a sediment layer
present in the sample container.
Method 8081B_8082A_D5: A portion of the following sample was used for analysis, rather than testing the entire sample amount in the
original container, due to the sample container was decanted: 149-TW-01 (680-227663-9). As such, the required solvent rinse of the
original container could not be performed.
Method 8081B_8082A_D5: The closing continuing calibration verification (CCV) standard associated with batch 680-756577 failed to
meet acceptance limits for . Sample matrix is adversely affecting the instrument and causing the failures.
Method 8081B_8082A_D5: The continuing calibration verification (CCV) associated with batch 680-756577 recovered above the upper
control limit for Chlordane (technical). The samples associated with this CCV were non-detects for the affected analyte; therefore, the data
has been reported. The associated samples are impacted: FB-12-22 (680-227663-7), EQB-12-22 (680-227663-8), 149-TW-01
(680-227663-9) and DUP-TW-01 (680-227663-10).
Method 8081B_8082A_D5: The continuing calibration verification (CCV) associated with 680-755553 recovered high and outside the
control limits for 4,4'-DDD, 4,4'-DDE, delta-BHC and PCB-1260 on column one. Results are confirmed on both columns and reported
from the passing column. The associated samples are: 149-SB-1-6-12-22 (680-227663-1), 149-DUP-1-12-22 (680-227663-2),
(680-227663-A-1-B MS) and (680-227663-A-1-C MSD).　
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
HPLC/IC
Method 7199_ORGFM: The following samples were received after the holding time had expired.: FB-12-22 (680-227663-7), EQB-12-22
(680-227663-8), 149-TW-01 (680-227663-9) and DUP-TW-01 (680-227663-10).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Metals
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
General Chemistry
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-1Client Sample ID: 149-SB-1-6-12-22
Matrix: SolidDate Collected: 12/13/22 11:40
Percent Solids: 77.3Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS)
LOQ DL
35 J Q 59 13 ug/Kg ☼12/16/22 12:07 12/27/22 18:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acetone
12 2.9 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 UBenzene
12 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 UBromoform
12 2.9 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 UBromomethane
30 11 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼24 U Q2-Butanone (MEK)
12 2.5 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 U QCarbon disulfide
12 2.5 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 UCarbon tetrachloride
5.9 1.7 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼4.8 UChlorobenzene
12 2.5 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 UChlorodibromomethane
12 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼9.5 UChloroethane
5.9 2.4 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼4.8 UChloroform
12 2.9 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 U QChloromethane
12 3.4 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼9.5 Ucis-1,2-Dichloroethene
12 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 Ucis-1,3-Dichloropropene
12 2.7 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 UCyclohexane
12 1.9 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼4.8 U1,2-Dibromo-3-Chloropropane
5.9 2.0 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼4.8 U1,2-Dichlorobenzene
5.9 2.4 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼4.8 U1,3-Dichlorobenzene
5.9 2.1 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼4.8 U1,4-Dichlorobenzene
5.9 2.4 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼4.8 UDichlorobromomethane
12 3.8 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼9.5 UDichlorodifluoromethane
12 3.4 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 U1,1-Dichloroethane
12 2.7 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 U1,2-Dichloroethane
5.9 4.3 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼4.8 U1,1-Dichloroethene
12 3.1 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼9.5 U1,2-Dichloropropane
12 2.5 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 UEthylbenzene
5.9 2.0 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼4.8 U1,2-Dibromoethane (EDB)
59 23 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼48 U Q2-Hexanone
12 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 UIsopropylbenzene
30 9.6 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼19 UMethyl acetate
5.9 2.4 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼4.8 UMethylcyclohexane
59 9.5 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼30 U MMethylene Chloride
120 21 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼48 U Q4-Methyl-2-pentanone (MIBK)
12 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 UMethyl tert-butyl ether
5.9 2.3 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼4.8 UStyrene
5.9 2.5 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼4.8 U1,1,2,2-Tetrachloroethane
12 3.1 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼9.5 U QTetrachloroethene
24 3.1 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼12 UToluene
12 2.7 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 Utrans-1,2-Dichloroethene
24 3.1 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼12 Utrans-1,3-Dichloropropene
12 3.0 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 U1,2,4-Trichlorobenzene
12 3.1 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 U1,1,1-Trichloroethane
5.9 1.8 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼4.8 U1,1,2-Trichloroethane
5.9 2.1 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼4.8 UTrichloroethene
12 3.7 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼9.5 UTrichlorofluoromethane
5.9 3.4 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼4.8 U Q1,1,2-Trichloro-1,2,2-trifluoroethane
12 3.3 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼9.5 UVinyl chloride
24 4.3 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼12 UXylenes, Total
59 31 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼59 UPropionitrile
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-1Client Sample ID: 149-SB-1-6-12-22
Matrix: SolidDate Collected: 12/13/22 11:40
Percent Solids: 77.3Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
12 U 12 7.5 ug/Kg ☼12/16/22 12:07 12/27/22 18:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Pentachloroethane
12 5.4 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼12 UMethyl methacrylate
24 4.9 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼12 UHexachlorobutadiene
5.9 2.4 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼4.8 UDibromomethane
59 49 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼59 U QAcetonitrile
12 3.7 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼9.5 UNaphthalene
12 2.0 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 U QIodomethane
12 4.2 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼9.5 U3-Chloro-1-propene
240 36 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼120 UAcrylonitrile
24 3.3 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼12 UEthyl methacrylate
12 1.5 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 U1,1,1,2-Tetrachloroethane
12 2.9 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 Utrans-1,4-Dichloro-2-butene
5.9 2.5 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 U Q2-Chloro-1,3-butadiene
59 27 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼59 UMethacrylonitrile
240 88 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼190 U QAcrolein
12 2.1 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 U1,2,3-Trichloropropane
48 6.5 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼24 U QVinyl acetate
590 110 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼240 U QIsobutyl alcohol
12 12 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼12 U2-Nitropropane
150 150 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼150 Un-Butyl alcohol
5.9 2.4 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼4.8 UBromochloromethane
12 3.1 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼9.5 UDiethyl ether
24 7.4 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼21 U QTetrahydrofuran
12 12 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼12 UEthyl acetate
5.9 5.9 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 UBenzyl chloride
12 2.3 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 Un-Butylbenzene
12 3.0 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 U1,2,4-Trimethylbenzene
12 2.7 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 U2-Chlorotoluene
5.9 5.9 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 Un-Butyl acetate
12 3.7 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼9.5 U1,2-Dichloroethene, Total
5.9 2.4 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼4.8 U1,1-Dichloropropene
5.9 5.9 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 U2-Methylnaphthalene
12 2.7 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 Uo-Xylene
5.9 2.0 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼4.8 UHexane
12 2.5 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 U4-Chlorotoluene
5.9 2.5 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 U Q1-Chlorohexane
5.9 2.0 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼4.8 UBromobenzene
5.9 2.4 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼4.8 U1,2,3-Trichlorobenzene
24 5.6 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼12 U1,3-Dichloropropene, Total
12 2.4 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 Usec-Butylbenzene
12 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 U2,2-Dichloropropane
12 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 UN-Propylbenzene
5.9 5.9 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 U1,3,5-Trichlorobenzene
12 1.8 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼12 UDiisopropyl ether
300 300 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼300 U QEthanol
59 59 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼59 UIsopropyl alcohol
24 3.1 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼12 Up-Cymene
5.9 5.9 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 U QTert-amyl methyl ether
12 2.9 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 U1,3,5-Trimethylbenzene
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-1Client Sample ID: 149-SB-1-6-12-22
Matrix: SolidDate Collected: 12/13/22 11:40
Percent Solids: 77.3Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
5.9 U 5.9 5.9 ug/Kg ☼12/16/22 12:07 12/27/22 18:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2,3-Trimethylbenzene
12 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 Um-Xylene & p-Xylene
12 2.9 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼9.5 UDichlorofluoromethane
12 3.0 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 Utert-Butylbenzene
5.9 5.9 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 U M QIsooctane
12 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:08 1☼5.9 U1,3-Dichloropropane
4-Bromofluorobenzene (Surr)94 79-119 12/16/22 12:07 12/27/22 18:08 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)107 12/16/22 12:07 12/27/22 18:08 178-119
1,2-Dichloroethane-d4 (Surr)101 12/16/22 12:07 12/27/22 18:08 171-138
Toluene-d8 (Surr)107 12/16/22 12:07 12/27/22 18:08 185-116
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
LOQ DL
410 U M 2100 140 ug/Kg ☼12/22/22 19:00 12/23/22 22:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
410 39 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U1,2,4,5-Tetrachlorobenzene
410 39 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U1,2,4-Trichlorobenzene
410 46 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U1,2-Dichlorobenzene
410 42 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U1,2-Diphenylhydrazine
410 42 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U1,3-Dichlorobenzene
410 44 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U1,4-Dichlorobenzene
410 39 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U1-Methylnaphthalene
410 27 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼100 U2,3,4,6-Tetrachlorophenol
410 44 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U2,4,5-Trichlorophenol
410 36 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U2,4,6-Trichlorophenol
410 44 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U2,4-Dichlorophenol
410 55 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U2,4-Dimethylphenol
2100 1000 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼1600 U2,4-Dinitrophenol
410 61 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼100 U2,4-Dinitrotoluene
410 34 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U2,6-Dichlorophenol
410 52 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U2,6-Dinitrotoluene
410 44 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U2-Chloronaphthalene
410 50 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U2-Chlorophenol
410 47 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U2-Methylnaphthalene
410 34 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U2-Methylphenol
2100 56 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼210 U2-Nitroaniline
410 51 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U2-Nitrophenol
410 54 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U3 & 4 Methylphenol
820 35 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U3,3'-Dichlorobenzidine
2100 57 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼100 U3-Nitroaniline
2100 210 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼410 U4,6-Dinitro-2-methylphenol
410 45 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U M4-Bromophenyl phenyl ether
410 44 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U4-Chloro-3-methylphenol
820 65 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼100 U4-Chloroaniline
410 55 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U4-Chlorophenyl phenyl ether
2100 61 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼100 U4-Nitroaniline
2100 410 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼840 U4-Nitrophenol
410 51 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UAcenaphthene
410 45 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UAcenaphthylene
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-1Client Sample ID: 149-SB-1-6-12-22
Matrix: SolidDate Collected: 12/13/22 11:40
Percent Solids: 77.3Date Received: 12/15/22 09:00
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
84 U 410 35 ug/Kg ☼12/22/22 19:00 12/23/22 22:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acetophenone
410 31 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UAnthracene
410 29 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UAtrazine
410 60 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼410 UAzobenzene
410 72 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼210 U MBenzaldehyde
410 34 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UBenzo[a]anthracene
410 65 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼100 U MBenzo[a]pyrene
410 47 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UBenzo[b]fluoranthene
410 27 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UBenzo[g,h,i]perylene
410 81 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼210 U MBenzo[k]fluoranthene
410 41 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U MBenzyl alcohol
410 37 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 Ubis (2-chloroisopropyl) ether
410 49 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UBis(2-chloroethoxy)methane
410 56 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼100 UBis(2-chloroethyl)ether
410 36 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UBis(2-ethylhexyl) phthalate
410 32 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UButyl benzyl phthalate
410 82 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼210 UCaprolactam
410 37 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UCarbazole
410 26 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U MChrysene
410 49 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UDibenz(a,h)anthracene
410 41 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UDibenzofuran
410 46 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UDiethyl phthalate
410 42 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UDimethyl phthalate
410 37 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UDi-n-butyl phthalate
410 36 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 U MDi-n-octyl phthalate
410 51 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼170 UDiphenylamine
410 40 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UFluoranthene
410 45 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UFluorene
410 49 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UHexachlorobenzene
410 45 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UHexachlorobutadiene
410 51 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UHexachlorocyclopentadiene
410 35 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UHexachloroethane
410 35 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UIndeno[1,2,3-cd]pyrene
410 41 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UIsophorone
410 37 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UNaphthalene
410 32 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UNitrobenzene
410 40 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UN-Nitrosodi-n-propylamine
410 41 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UN-Nitrosodiphenylamine
2100 410 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼840 UPentachlorophenol
410 34 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UPhenanthrene
410 42 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UPhenol
410 34 ug/Kg 12/22/22 19:00 12/23/22 22:43 1☼84 UPyrene
2-Fluorobiphenyl (Surr)69 44-115 12/22/22 19:00 12/23/22 22:43 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)59 12/22/22 19:00 12/23/22 22:43 135-115
Nitrobenzene-d5 (Surr)55 12/22/22 19:00 12/23/22 22:43 137-122
Phenol-d5 (Surr)59 12/22/22 19:00 12/23/22 22:43 133-122
Terphenyl-d14 (Surr)72 12/22/22 19:00 12/23/22 22:43 154-127
2,4,6-Tribromophenol (Surr)89 12/22/22 19:00 12/23/22 22:43 139-132
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-1Client Sample ID: 149-SB-1-6-12-22
Matrix: SolidDate Collected: 12/13/22 11:40
Percent Solids: 77.3Date Received: 12/15/22 09:00
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
3.2 U 6.5 1.6 mg/Kg ☼01/18/23 06:31 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
0.10 U 0.13 0.052 mg/Kg ☼12/18/22 16:07 01/10/23 17:56 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Benzene
6.5 1.6 mg/Kg 12/18/22 16:07 01/10/23 17:56 50☼3.2 UC5-C8 Aliphatics
6.5 1.6 mg/Kg 12/18/22 16:07 01/10/23 17:56 50☼3.2 UC9-C10 Aromatics
6.5 1.6 mg/Kg 12/18/22 16:07 01/10/23 17:56 50☼3.2 UC9-C12 Aliphatics
0.13 0.052 mg/Kg 12/18/22 16:07 01/10/23 17:56 50☼0.10 UEthylbenzene
0.13 0.052 mg/Kg 12/18/22 16:07 01/10/23 17:56 50☼0.10 UMethyl tert-butyl ether
0.39 0.13 mg/Kg 12/18/22 16:07 01/10/23 17:56 50☼0.26 UNaphthalene
0.13 0.052 mg/Kg 12/18/22 16:07 01/10/23 17:56 50☼0.10 UToluene
6.5 1.6 mg/Kg 12/18/22 16:07 01/10/23 17:56 50☼3.2 UC9-C12 Aliphatics (adjusted)
0.32 0.13 mg/Kg 12/18/22 16:07 01/10/23 17:56 50☼0.26 Um-Xylene & p-Xylene
0.13 0.052 mg/Kg 12/18/22 16:07 01/10/23 17:56 50☼0.10 Uo-Xylene
6.5 1.6 mg/Kg 12/18/22 16:07 01/10/23 17:56 50☼3.2 UC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)82 70-130 12/18/22 16:07 01/10/23 17:56 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)79 12/18/22 16:07 01/10/23 17:56 5070-130
Method: SW846 8081B 8082A - Organochlorine Pesticides & PCBs (GC)
LOQ DL
0.21 U 1.0 0.092 ug/Kg ☼12/16/22 13:33 12/16/22 21:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Aldrin
1.0 0.086 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼0.21 Ualpha-BHC
1.0 0.11 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼0.28 Ualpha-Chlordane
1.0 0.21 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼0.61 Ubeta-BHC
1.0 0.11 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼0.28 U4,4'-DDD
1.0 0.11 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼0.22 J4,4'-DDE
1.0 0.14 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼0.15 J4,4'-DDT
1.0 0.12 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼0.28 U J1delta-BHC
1.0 0.10 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼0.28 U MDieldrin
1.0 0.10 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼0.28 UEndosulfan I
1.0 0.092 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼0.21 UEndosulfan II
1.0 0.14 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼0.28 U MEndosulfan sulfate
1.0 0.14 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼0.28 UEndrin
1.0 0.14 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼0.28 UEndrin aldehyde
1.0 0.12 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼0.28 UEndrin ketone
1.0 0.086 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼0.21 Ugamma-BHC (Lindane)
1.0 0.12 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼0.28 UHeptachlor
1.0 0.098 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼0.28 UHeptachlor epoxide
1.0 0.17 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼0.41 UMethoxychlor
100 3.4 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼14 U M QToxaphene
21 6.8 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼12 U QPCB-1221
21 6.8 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼12 UPCB-1242
21 6.8 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼12 U QPCB-1254
21 5.9 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼12 U QPCB-1260
31 6.8 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼25 UPCB-1016
21 6.8 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼12 UPCB-1248
21 6.8 ug/Kg 12/16/22 13:33 12/16/22 21:15 1☼12 U QPCB-1232
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-1Client Sample ID: 149-SB-1-6-12-22
Matrix: SolidDate Collected: 12/13/22 11:40
Percent Solids: 77.3Date Received: 12/15/22 09:00
DCB Decachlorobiphenyl 85 44-129 12/16/22 13:33 12/16/22 21:15 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene (Surr)89 12/16/22 13:33 12/16/22 21:15 142-129
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
LOQ DL
0.51 U 0.64 0.26 mg/Kg ☼12/22/22 15:40 12/31/22 03:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acenaphthene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 03:56 1☼0.51 UAcenaphthylene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 03:56 1☼0.51 UAnthracene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 03:56 1☼0.51 UBenzo[a]anthracene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 03:56 1☼0.51 UBenzo[a]pyrene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 03:56 1☼0.51 UBenzo[b]fluoranthene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 03:56 1☼0.51 UBenzo[g,h,i]perylene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 03:56 1☼0.51 UBenzo[k]fluoranthene
15 2.4 mg/Kg 12/22/22 15:40 12/31/22 03:33 1☼3.3 JC19-C36 Aliphatics
7.7 1.9 mg/Kg 12/22/22 15:40 12/31/22 03:33 1☼3.8 UC9-C18 Aliphatics
15 5.4 mg/Kg 12/22/22 15:40 12/31/22 03:56 1☼11 UC11-C22 Aromatics
15 5.4 mg/Kg 12/22/22 15:40 12/31/22 03:56 1☼11 UC11-C22 Aromatics (Adjusted)
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 03:56 1☼0.51 UChrysene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 03:56 1☼0.51 UDibenz(a,h)anthracene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 03:56 1☼0.51 UFluoranthene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 03:56 1☼0.51 UFluorene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 03:56 1☼0.51 UIndeno[1,2,3-cd]pyrene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 03:56 1☼0.51 U2-Methylnaphthalene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 03:56 1☼0.51 UNaphthalene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 03:56 1☼0.51 UPhenanthrene
2.6 0.89 mg/Kg 12/22/22 15:40 12/31/22 03:56 1☼2.0 UPyrene
1-Chlorooctadecane (Surr)69 40-140 12/22/22 15:40 12/31/22 03:33 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)110 12/22/22 15:40 12/31/22 03:56 140-140
o- terphenyl (Surr)93 12/22/22 15:40 12/31/22 03:56 140-140
Method: SW846 7199 - Chromium, Hexavalent (IC)
LOQ DL
1800 M 510 180 ug/Kg ☼01/12/23 10:42 01/12/23 19:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Chromium (hexavalent)
510 180 ug/Kg 01/12/23 10:42 01/12/23 19:37 1☼1700 MChromium (hexavalent)
Method: SW846 6020B - Metals (ICP/MS)
LOQ DL
6200000 11000 2400 ug/Kg ☼12/15/22 13:26 12/16/22 15:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Aluminum
1100 110 ug/Kg 12/15/22 13:26 12/16/22 15:54 1☼180 JAntimony
570 110 ug/Kg 12/15/22 13:26 12/16/22 15:54 1☼1400Arsenic
570 68 ug/Kg 12/15/22 13:26 12/16/22 15:54 1☼8100Barium
57 17 ug/Kg 12/15/22 13:26 12/16/22 15:54 1☼150Beryllium
57 17 ug/Kg 12/15/22 13:26 12/16/22 15:54 1☼44 JCadmium
57000 7200 ug/Kg 12/15/22 13:26 12/16/22 15:54 1☼34000 JCalcium
1100 120 ug/Kg 12/15/22 13:26 12/16/22 15:54 1☼19000Chromium
57 11 ug/Kg 12/15/22 13:26 12/16/22 15:54 1☼400Cobalt
570 150 ug/Kg 12/15/22 13:26 12/16/22 15:54 1☼3100Copper
28000 4000 ug/Kg 12/15/22 13:26 12/16/22 15:54 1☼8000000Iron
230 57 ug/Kg 12/15/22 13:26 12/16/22 15:54 1☼17000Lead
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-1Client Sample ID: 149-SB-1-6-12-22
Matrix: SolidDate Collected: 12/13/22 11:40
Percent Solids: 77.3Date Received: 12/15/22 09:00
Method: SW846 6020B - Metals (ICP/MS) (Continued)
LOQ DL
140000 28000 3700 ug/Kg ☼12/15/22 13:26 12/16/22 15:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Magnesium
1100 140 ug/Kg 12/15/22 13:26 12/16/22 15:54 1☼8800Manganese
1100 300 ug/Kg 12/15/22 13:26 12/16/22 15:54 1☼1600Nickel
28000 10000 ug/Kg 12/15/22 13:26 12/16/22 15:54 1☼210000Potassium
570 110 ug/Kg 12/15/22 13:26 12/16/22 15:54 1☼160 JSelenium
110 11 ug/Kg 12/15/22 13:26 12/16/22 15:54 1☼34 USilver
45000 11000 ug/Kg 12/15/22 13:26 12/16/22 15:54 1☼28000 USodium
110 57 ug/Kg 12/15/22 13:26 12/16/22 15:54 1☼110 UThallium
2300 310 ug/Kg 12/15/22 13:26 12/16/22 15:54 1☼16000Vanadium
2800 1100 ug/Kg 12/15/22 13:26 12/16/22 15:54 1☼8200Zinc
Lab Sample ID: 680-227663-2Client Sample ID: 149-DUP-1-12-22
Matrix: SolidDate Collected: 12/13/22 12:00
Percent Solids: 92.5Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS)
LOQ DL
21 J Q 66 15 ug/Kg ☼12/16/22 12:07 12/27/22 18:31 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acetone
13 3.2 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 UBenzene
13 2.9 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 UBromoform
13 3.2 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 UBromomethane
33 12 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼26 U Q2-Butanone (MEK)
13 2.8 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 U QCarbon disulfide
13 2.8 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 UCarbon tetrachloride
6.6 1.8 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼5.3 UChlorobenzene
13 2.8 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 UChlorodibromomethane
13 2.9 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼11 UChloroethane
6.6 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼5.3 UChloroform
13 3.2 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 U QChloromethane
13 3.8 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼11 Ucis-1,2-Dichloroethene
13 2.9 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 Ucis-1,3-Dichloropropene
13 3.0 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 UCyclohexane
13 2.1 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼5.3 U1,2-Dibromo-3-Chloropropane
6.6 2.2 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼5.3 U1,2-Dichlorobenzene
6.6 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼5.3 U1,3-Dichlorobenzene
6.6 2.4 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼5.3 U1,4-Dichlorobenzene
6.6 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼5.3 UDichlorobromomethane
13 4.2 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼11 UDichlorodifluoromethane
13 3.8 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 U1,1-Dichloroethane
13 3.0 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 U1,2-Dichloroethane
6.6 4.7 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼5.3 U1,1-Dichloroethene
13 3.4 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼11 U1,2-Dichloropropane
13 2.8 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 UEthylbenzene
6.6 2.2 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼5.3 U1,2-Dibromoethane (EDB)
66 25 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼53 U Q2-Hexanone
13 2.9 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 UIsopropylbenzene
33 11 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼21 UMethyl acetate
6.6 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼5.3 UMethylcyclohexane
66 11 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼33 U MMethylene Chloride
130 24 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼53 U Q4-Methyl-2-pentanone (MIBK)
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-2Client Sample ID: 149-DUP-1-12-22
Matrix: SolidDate Collected: 12/13/22 12:00
Percent Solids: 92.5Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
6.6 U 13 2.9 ug/Kg ☼12/16/22 12:07 12/27/22 18:31 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Methyl tert-butyl ether
6.6 2.5 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼5.3 UStyrene
6.6 2.8 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼5.3 U1,1,2,2-Tetrachloroethane
13 3.4 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼11 U QTetrachloroethene
26 3.4 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼13 UToluene
13 3.0 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 Utrans-1,2-Dichloroethene
26 3.4 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼13 Utrans-1,3-Dichloropropene
13 3.3 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 U1,2,4-Trichlorobenzene
13 3.4 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 U1,1,1-Trichloroethane
6.6 2.0 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼5.3 U1,1,2-Trichloroethane
6.6 2.4 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼5.3 UTrichloroethene
13 4.1 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼11 UTrichlorofluoromethane
6.6 3.8 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼5.3 U Q1,1,2-Trichloro-1,2,2-trifluoroethane
13 3.7 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼11 UVinyl chloride
26 4.7 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼13 UXylenes, Total
66 34 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼66 UPropionitrile
13 8.3 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼13 UPentachloroethane
13 5.9 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼13 UMethyl methacrylate
26 5.4 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼13 UHexachlorobutadiene
6.6 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼5.3 UDibromomethane
66 54 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼66 U QAcetonitrile
13 4.1 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼11 UNaphthalene
13 2.2 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 U QIodomethane
13 4.6 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼11 U3-Chloro-1-propene
260 40 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼130 UAcrylonitrile
26 3.7 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼13 UEthyl methacrylate
13 1.7 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 U1,1,1,2-Tetrachloroethane
13 3.2 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 Utrans-1,4-Dichloro-2-butene
6.6 2.8 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 U Q2-Chloro-1,3-butadiene
66 30 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼66 UMethacrylonitrile
260 98 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼210 U QAcrolein
13 2.4 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 U1,2,3-Trichloropropane
53 7.3 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼26 U QVinyl acetate
660 120 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼260 U QIsobutyl alcohol
13 13 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼13 U2-Nitropropane
170 170 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼170 Un-Butyl alcohol
6.6 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼5.3 UBromochloromethane
13 3.4 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼11 UDiethyl ether
26 8.2 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼24 U QTetrahydrofuran
13 13 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼13 UEthyl acetate
6.6 6.6 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 UBenzyl chloride
13 2.5 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 Un-Butylbenzene
13 3.3 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 U1,2,4-Trimethylbenzene
13 3.0 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 U2-Chlorotoluene
6.6 6.6 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 Un-Butyl acetate
13 4.1 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼11 U1,2-Dichloroethene, Total
6.6 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼5.3 U1,1-Dichloropropene
6.6 6.6 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 U2-Methylnaphthalene
13 3.0 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 Uo-Xylene
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-2Client Sample ID: 149-DUP-1-12-22
Matrix: SolidDate Collected: 12/13/22 12:00
Percent Solids: 92.5Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
5.3 U 6.6 2.2 ug/Kg ☼12/16/22 12:07 12/27/22 18:31 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Hexane
13 2.8 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 U4-Chlorotoluene
6.6 2.8 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 U Q1-Chlorohexane
6.6 2.2 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼5.3 UBromobenzene
6.6 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼5.3 U1,2,3-Trichlorobenzene
26 6.2 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼13 U1,3-Dichloropropene, Total
13 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 Usec-Butylbenzene
13 2.9 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 U2,2-Dichloropropane
13 2.9 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 UN-Propylbenzene
6.6 6.6 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 U1,3,5-Trichlorobenzene
13 2.0 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼13 UDiisopropyl ether
330 330 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼330 U QEthanol
66 66 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼66 UIsopropyl alcohol
26 3.4 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼13 Up-Cymene
6.6 6.6 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 U QTert-amyl methyl ether
13 3.2 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 U1,3,5-Trimethylbenzene
6.6 6.6 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 U1,2,3-Trimethylbenzene
13 2.9 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 Um-Xylene & p-Xylene
13 3.2 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼11 UDichlorofluoromethane
13 3.3 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 Utert-Butylbenzene
6.6 6.6 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 U QIsooctane
13 2.9 ug/Kg 12/16/22 12:07 12/27/22 18:31 1☼6.6 U1,3-Dichloropropane
4-Bromofluorobenzene (Surr)93 79-119 12/16/22 12:07 12/27/22 18:31 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)106 12/16/22 12:07 12/27/22 18:31 178-119
1,2-Dichloroethane-d4 (Surr)101 12/16/22 12:07 12/27/22 18:31 171-138
Toluene-d8 (Surr)107 12/16/22 12:07 12/27/22 18:31 185-116
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
LOQ DL
340 U 1800 110 ug/Kg ☼12/16/22 15:30 12/20/22 12:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
340 32 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U1,2,4,5-Tetrachlorobenzene
340 32 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U1,2,4-Trichlorobenzene
340 39 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U1,2-Dichlorobenzene
340 35 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U1,2-Diphenylhydrazine
340 35 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U1,3-Dichlorobenzene
340 36 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U1,4-Dichlorobenzene
340 32 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U1-Methylnaphthalene
340 23 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼86 U2,3,4,6-Tetrachlorophenol
340 36 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U2,4,5-Trichlorophenol
340 30 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U2,4,6-Trichlorophenol
340 36 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U2,4-Dichlorophenol
340 46 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U2,4-Dimethylphenol
1800 860 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼1400 U2,4-Dinitrophenol
340 51 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼86 U2,4-Dinitrotoluene
340 28 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U2,6-Dichlorophenol
340 44 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U2,6-Dinitrotoluene
340 36 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U2-Chloronaphthalene
340 42 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U2-Chlorophenol
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-2Client Sample ID: 149-DUP-1-12-22
Matrix: SolidDate Collected: 12/13/22 12:00
Percent Solids: 92.5Date Received: 12/15/22 09:00
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
70 U 340 40 ug/Kg ☼12/16/22 15:30 12/20/22 12:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2-Methylnaphthalene
340 28 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U2-Methylphenol
1800 47 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼180 U2-Nitroaniline
340 43 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U2-Nitrophenol
340 45 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U3 & 4 Methylphenol
690 29 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U3,3'-Dichlorobenzidine
1800 48 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼86 U3-Nitroaniline
1800 180 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼340 U4,6-Dinitro-2-methylphenol
340 37 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U4-Bromophenyl phenyl ether
340 36 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U M4-Chloro-3-methylphenol
690 54 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼86 U4-Chloroaniline
340 46 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U4-Chlorophenyl phenyl ether
1800 51 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼86 U Q4-Nitroaniline
1800 340 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼700 U4-Nitrophenol
340 43 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UAcenaphthene
340 37 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UAcenaphthylene
340 29 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UAcetophenone
340 26 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UAnthracene
340 24 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UAtrazine
340 50 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼340 U MAzobenzene
340 60 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼180 U QBenzaldehyde
340 28 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UBenzo[a]anthracene
340 54 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼86 UBenzo[a]pyrene
340 40 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UBenzo[b]fluoranthene
340 23 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UBenzo[g,h,i]perylene
340 68 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼180 UBenzo[k]fluoranthene
340 34 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UBenzyl alcohol
340 31 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 Ubis (2-chloroisopropyl) ether
340 41 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UBis(2-chloroethoxy)methane
340 47 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼86 UBis(2-chloroethyl)ether
340 30 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UBis(2-ethylhexyl) phthalate
340 27 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UButyl benzyl phthalate
340 69 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼180 U QCaprolactam
340 31 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UCarbazole
340 22 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UChrysene
340 41 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UDibenz(a,h)anthracene
340 34 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UDibenzofuran
340 39 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UDiethyl phthalate
340 35 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UDimethyl phthalate
340 31 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UDi-n-butyl phthalate
340 30 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UDi-n-octyl phthalate
340 43 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼150 U MDiphenylamine
340 33 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UFluoranthene
340 37 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UFluorene
340 41 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U QHexachlorobenzene
340 37 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UHexachlorobutadiene
340 43 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UHexachlorocyclopentadiene
340 29 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UHexachloroethane
340 29 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 U QIndeno[1,2,3-cd]pyrene
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-2Client Sample ID: 149-DUP-1-12-22
Matrix: SolidDate Collected: 12/13/22 12:00
Percent Solids: 92.5Date Received: 12/15/22 09:00
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
70 U M 340 34 ug/Kg ☼12/16/22 15:30 12/20/22 12:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Isophorone
340 31 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UNaphthalene
340 27 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UNitrobenzene
340 33 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UN-Nitrosodi-n-propylamine
340 34 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UN-Nitrosodiphenylamine
1800 340 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼700 UPentachlorophenol
340 28 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UPhenanthrene
340 35 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UPhenol
340 28 ug/Kg 12/16/22 15:30 12/20/22 12:29 1☼70 UPyrene
2-Fluorobiphenyl (Surr)71 44-115 12/16/22 15:30 12/20/22 12:29 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)64 12/16/22 15:30 12/20/22 12:29 135-115
Nitrobenzene-d5 (Surr)62 12/16/22 15:30 12/20/22 12:29 137-122
Phenol-d5 (Surr)66 12/16/22 15:30 12/20/22 12:29 133-122
Terphenyl-d14 (Surr)74 12/16/22 15:30 12/20/22 12:29 154-127
2,4,6-Tribromophenol (Surr)59 Q 12/16/22 15:30 12/20/22 12:29 139-132
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
2.7 U 5.4 1.4 mg/Kg ☼01/18/23 06:31 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
0.086 U 0.11 0.043 mg/Kg ☼12/18/22 16:07 01/10/23 18:36 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Benzene
5.4 1.3 mg/Kg 12/18/22 16:07 01/10/23 18:36 50☼2.7 UC5-C8 Aliphatics
5.4 1.3 mg/Kg 12/18/22 16:07 01/10/23 18:36 50☼2.7 UC9-C10 Aromatics
5.4 1.3 mg/Kg 12/18/22 16:07 01/10/23 18:36 50☼2.7 UC9-C12 Aliphatics
0.11 0.043 mg/Kg 12/18/22 16:07 01/10/23 18:36 50☼0.086 UEthylbenzene
0.11 0.043 mg/Kg 12/18/22 16:07 01/10/23 18:36 50☼0.086 UMethyl tert-butyl ether
0.32 0.11 mg/Kg 12/18/22 16:07 01/10/23 18:36 50☼0.22 UNaphthalene
0.11 0.043 mg/Kg 12/18/22 16:07 01/10/23 18:36 50☼0.086 UToluene
5.4 1.3 mg/Kg 12/18/22 16:07 01/10/23 18:36 50☼2.7 UC9-C12 Aliphatics (adjusted)
0.27 0.11 mg/Kg 12/18/22 16:07 01/10/23 18:36 50☼0.22 Um-Xylene & p-Xylene
0.11 0.043 mg/Kg 12/18/22 16:07 01/10/23 18:36 50☼0.086 Uo-Xylene
5.4 1.3 mg/Kg 12/18/22 16:07 01/10/23 18:36 50☼2.7 UC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)91 70-130 12/18/22 16:07 01/10/23 18:36 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)90 12/18/22 16:07 01/10/23 18:36 5070-130
Method: SW846 8081B 8082A - Organochlorine Pesticides & PCBs (GC)
LOQ DL
0.17 U M 0.87 0.077 ug/Kg ☼12/16/22 13:33 12/16/22 22:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Aldrin
0.87 0.072 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼0.17 Ualpha-BHC
0.87 0.092 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼0.24 Ualpha-Chlordane
0.87 0.17 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼0.51 Ubeta-BHC
0.87 0.092 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼0.24 U4,4'-DDD
0.87 0.092 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼0.18 J4,4'-DDE
0.87 0.11 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼0.15 J4,4'-DDT
0.87 0.098 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼0.24 Udelta-BHC
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-2Client Sample ID: 149-DUP-1-12-22
Matrix: SolidDate Collected: 12/13/22 12:00
Percent Solids: 92.5Date Received: 12/15/22 09:00
Method: SW846 8081B 8082A - Organochlorine Pesticides & PCBs (GC) (Continued)
LOQ DL
0.24 U 0.87 0.087 ug/Kg ☼12/16/22 13:33 12/16/22 22:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dieldrin
0.87 0.087 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼0.24 UEndosulfan I
0.87 0.077 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼0.17 UEndosulfan II
0.87 0.11 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼0.24 UEndosulfan sulfate
0.87 0.11 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼0.24 UEndrin
0.87 0.11 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼0.24 UEndrin aldehyde
0.87 0.10 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼0.24 U MEndrin ketone
0.87 0.072 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼0.17 Ugamma-BHC (Lindane)
0.87 0.098 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼0.24 UHeptachlor
0.87 0.082 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼0.24 UHeptachlor epoxide
0.87 0.14 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼0.34 UMethoxychlor
87 2.9 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼11 U M QToxaphene
17 5.6 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼10 U QPCB-1221
17 5.6 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼10 UPCB-1242
17 5.6 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼10 U QPCB-1254
17 4.9 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼10 U M QPCB-1260
26 5.6 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼21 UPCB-1016
17 5.6 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼10 UPCB-1248
17 5.6 ug/Kg 12/16/22 13:33 12/16/22 22:09 1☼10 U QPCB-1232
DCB Decachlorobiphenyl 83 44-129 12/16/22 13:33 12/16/22 22:09 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene (Surr)92 12/16/22 13:33 12/16/22 22:09 142-129
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
LOQ DL
0.43 U 0.53 0.21 mg/Kg ☼12/22/22 15:40 12/31/22 04:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acenaphthene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:18 1☼0.43 UAcenaphthylene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:18 1☼0.43 UAnthracene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:18 1☼0.43 UBenzo[a]anthracene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:18 1☼0.43 UBenzo[a]pyrene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:18 1☼0.43 UBenzo[b]fluoranthene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:18 1☼0.43 UBenzo[g,h,i]perylene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:18 1☼0.43 UBenzo[k]fluoranthene
13 2.0 mg/Kg 12/22/22 15:40 12/31/22 03:56 1☼3.5 J MC19-C36 Aliphatics
6.4 1.6 mg/Kg 12/22/22 15:40 12/31/22 03:56 1☼3.2 UC9-C18 Aliphatics
13 4.5 mg/Kg 12/22/22 15:40 12/31/22 04:18 1☼9.0 U MC11-C22 Aromatics
13 4.5 mg/Kg 12/22/22 15:40 12/31/22 04:18 1☼9.0 UC11-C22 Aromatics (Adjusted)
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:18 1☼0.43 UChrysene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:18 1☼0.43 UDibenz(a,h)anthracene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:18 1☼0.43 UFluoranthene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:18 1☼0.43 UFluorene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:18 1☼0.43 UIndeno[1,2,3-cd]pyrene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:18 1☼0.43 U2-Methylnaphthalene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:18 1☼0.43 U MNaphthalene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:18 1☼0.43 UPhenanthrene
2.1 0.75 mg/Kg 12/22/22 15:40 12/31/22 04:18 1☼1.7 UPyrene
1-Chlorooctadecane (Surr)66 40-140 12/22/22 15:40 12/31/22 03:56 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-2Client Sample ID: 149-DUP-1-12-22
Matrix: SolidDate Collected: 12/13/22 12:00
Percent Solids: 92.5Date Received: 12/15/22 09:00
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
2-Fluorobiphenyl (Surr)83 40-140 12/22/22 15:40 12/31/22 04:18 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
o- terphenyl (Surr)70 12/22/22 15:40 12/31/22 04:18 140-140
Method: SW846 7199 - Chromium, Hexavalent (IC)
LOQ DL
1100 M 440 150 ug/Kg ☼01/12/23 10:42 01/12/23 18:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Chromium (hexavalent)
440 150 ug/Kg 01/12/23 10:42 01/12/23 18:33 1☼1100 MChromium (hexavalent)
Method: SW846 6020B - Metals (ICP/MS)
LOQ DL
4400000 9400 2000 ug/Kg ☼12/15/22 13:26 12/16/22 15:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Aluminum
940 94 ug/Kg 12/15/22 13:26 12/16/22 15:58 1☼140 JAntimony
470 94 ug/Kg 12/15/22 13:26 12/16/22 15:58 1☼940Arsenic
470 56 ug/Kg 12/15/22 13:26 12/16/22 15:58 1☼5500Barium
47 14 ug/Kg 12/15/22 13:26 12/16/22 15:58 1☼75Beryllium
47 14 ug/Kg 12/15/22 13:26 12/16/22 15:58 1☼38 UCadmium
47000 5900 ug/Kg 12/15/22 13:26 12/16/22 15:58 1☼19000 JCalcium
940 100 ug/Kg 12/15/22 13:26 12/16/22 15:58 1☼11000Chromium
47 9.4 ug/Kg 12/15/22 13:26 12/16/22 15:58 1☼280Cobalt
470 120 ug/Kg 12/15/22 13:26 12/16/22 15:58 1☼2400Copper
24000 3300 ug/Kg 12/15/22 13:26 12/16/22 15:58 1☼4700000Iron
190 47 ug/Kg 12/15/22 13:26 12/16/22 15:58 1☼15000Lead
24000 3100 ug/Kg 12/15/22 13:26 12/16/22 15:58 1☼68000Magnesium
940 110 ug/Kg 12/15/22 13:26 12/16/22 15:58 1☼6700Manganese
940 240 ug/Kg 12/15/22 13:26 12/16/22 15:58 1☼1000Nickel
24000 8600 ug/Kg 12/15/22 13:26 12/16/22 15:58 1☼82000Potassium
470 94 ug/Kg 12/15/22 13:26 12/16/22 15:58 1☼140 JSelenium
94 9.4 ug/Kg 12/15/22 13:26 12/16/22 15:58 1☼28 USilver
38000 9400 ug/Kg 12/15/22 13:26 12/16/22 15:58 1☼24000 USodium
94 47 ug/Kg 12/15/22 13:26 12/16/22 15:58 1☼94 UThallium
1900 250 ug/Kg 12/15/22 13:26 12/16/22 15:58 1☼11000Vanadium
2400 940 ug/Kg 12/15/22 13:26 12/16/22 15:58 1☼5800Zinc
Lab Sample ID: 680-227663-3Client Sample ID: 149-SB-1-20-12-22
Matrix: SolidDate Collected: 12/13/22 12:15
Percent Solids: 94.5Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS)
LOQ DL
25 U Q 50 11 ug/Kg ☼12/16/22 12:07 12/27/22 18:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acetone
9.9 2.4 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 UBenzene
9.9 2.2 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 UBromoform
9.9 2.4 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 UBromomethane
25 9.2 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼20 U Q2-Butanone (MEK)
9.9 2.1 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 U QCarbon disulfide
9.9 2.1 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 UCarbon tetrachloride
5.0 1.4 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼4.0 UChlorobenzene
9.9 2.1 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 UChlorodibromomethane
9.9 2.2 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼8.0 UChloroethane
5.0 2.0 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼4.0 UChloroform
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-3Client Sample ID: 149-SB-1-20-12-22
Matrix: SolidDate Collected: 12/13/22 12:15
Percent Solids: 94.5Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
5.0 U Q 9.9 2.4 ug/Kg ☼12/16/22 12:07 12/27/22 18:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Chloromethane
9.9 2.9 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼8.0 Ucis-1,2-Dichloroethene
9.9 2.2 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 Ucis-1,3-Dichloropropene
9.9 2.3 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 UCyclohexane
9.9 1.6 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼4.0 U1,2-Dibromo-3-Chloropropane
5.0 1.7 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼4.0 U1,2-Dichlorobenzene
5.0 2.0 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼4.0 U1,3-Dichlorobenzene
5.0 1.8 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼4.0 U1,4-Dichlorobenzene
5.0 2.0 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼4.0 UDichlorobromomethane
9.9 3.2 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼8.0 UDichlorodifluoromethane
9.9 2.9 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 U1,1-Dichloroethane
9.9 2.3 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 U1,2-Dichloroethane
5.0 3.6 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼4.0 U1,1-Dichloroethene
9.9 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼8.0 U1,2-Dichloropropane
9.9 2.1 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 UEthylbenzene
5.0 1.7 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼4.0 U1,2-Dibromoethane (EDB)
50 19 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼40 U Q2-Hexanone
9.9 2.2 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 UIsopropylbenzene
25 8.1 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼16 UMethyl acetate
5.0 2.0 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼4.0 UMethylcyclohexane
50 8.0 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼25 U MMethylene Chloride
99 18 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼40 U Q4-Methyl-2-pentanone (MIBK)
9.9 2.2 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 UMethyl tert-butyl ether
5.0 1.9 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼4.0 UStyrene
5.0 2.1 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼4.0 U1,1,2,2-Tetrachloroethane
9.9 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼8.0 U QTetrachloroethene
20 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼9.9 UToluene
9.9 2.3 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 Utrans-1,2-Dichloroethene
20 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼9.9 Utrans-1,3-Dichloropropene
9.9 2.5 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 U1,2,4-Trichlorobenzene
9.9 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 U1,1,1-Trichloroethane
5.0 1.5 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼4.0 U1,1,2-Trichloroethane
5.0 1.8 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼4.0 UTrichloroethene
9.9 3.1 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼8.0 UTrichlorofluoromethane
5.0 2.9 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼4.0 U Q1,1,2-Trichloro-1,2,2-trifluoroethane
9.9 2.8 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼8.0 UVinyl chloride
20 3.6 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼9.9 UXylenes, Total
50 26 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼50 UPropionitrile
9.9 6.3 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼9.9 UPentachloroethane
9.9 4.5 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼9.9 UMethyl methacrylate
20 4.1 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼9.9 UHexachlorobutadiene
5.0 2.0 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼4.0 UDibromomethane
50 41 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼50 U QAcetonitrile
9.9 3.1 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼8.0 UNaphthalene
9.9 1.7 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 U QIodomethane
9.9 3.5 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼8.0 U3-Chloro-1-propene
200 30 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼99 UAcrylonitrile
20 2.8 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼9.9 UEthyl methacrylate
9.9 1.3 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 U1,1,1,2-Tetrachloroethane
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-3Client Sample ID: 149-SB-1-20-12-22
Matrix: SolidDate Collected: 12/13/22 12:15
Percent Solids: 94.5Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
5.0 U 9.9 2.4 ug/Kg ☼12/16/22 12:07 12/27/22 18:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
trans-1,4-Dichloro-2-butene
5.0 2.1 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 U Q2-Chloro-1,3-butadiene
50 23 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼50 UMethacrylonitrile
200 74 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼160 U QAcrolein
9.9 1.8 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 U1,2,3-Trichloropropane
40 5.5 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼20 U QVinyl acetate
500 92 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼200 U QIsobutyl alcohol
9.9 9.9 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼9.9 U2-Nitropropane
130 130 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼130 Un-Butyl alcohol
5.0 2.0 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼4.0 UBromochloromethane
9.9 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼8.0 UDiethyl ether
20 6.2 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼18 U QTetrahydrofuran
9.9 9.9 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼9.9 UEthyl acetate
5.0 5.0 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 UBenzyl chloride
9.9 1.9 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 Un-Butylbenzene
9.9 2.5 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 U1,2,4-Trimethylbenzene
9.9 2.3 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 U2-Chlorotoluene
5.0 5.0 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 Un-Butyl acetate
9.9 3.1 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼8.0 U1,2-Dichloroethene, Total
5.0 2.0 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼4.0 U1,1-Dichloropropene
5.0 5.0 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 U2-Methylnaphthalene
9.9 2.3 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 Uo-Xylene
5.0 1.7 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼4.0 UHexane
9.9 2.1 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 U4-Chlorotoluene
5.0 2.1 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 U Q1-Chlorohexane
5.0 1.7 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼4.0 UBromobenzene
5.0 2.0 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼4.0 U1,2,3-Trichlorobenzene
20 4.7 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼9.9 U1,3-Dichloropropene, Total
9.9 2.0 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 Usec-Butylbenzene
9.9 2.2 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 U2,2-Dichloropropane
9.9 2.2 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 UN-Propylbenzene
5.0 5.0 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 U1,3,5-Trichlorobenzene
9.9 1.5 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼9.9 UDiisopropyl ether
250 250 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼250 U QEthanol
50 50 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼50 UIsopropyl alcohol
20 2.6 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼9.9 Up-Cymene
5.0 5.0 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 U QTert-amyl methyl ether
9.9 2.4 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 U1,3,5-Trimethylbenzene
5.0 5.0 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 U1,2,3-Trimethylbenzene
9.9 2.2 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 Um-Xylene & p-Xylene
9.9 2.4 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼8.0 UDichlorofluoromethane
9.9 2.5 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 Utert-Butylbenzene
5.0 5.0 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 U QIsooctane
9.9 2.2 ug/Kg 12/16/22 12:07 12/27/22 18:55 1☼5.0 U1,3-Dichloropropane
4-Bromofluorobenzene (Surr)91 79-119 12/16/22 12:07 12/27/22 18:55 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)107 12/16/22 12:07 12/27/22 18:55 178-119
1,2-Dichloroethane-d4 (Surr)99 12/16/22 12:07 12/27/22 18:55 171-138
Toluene-d8 (Surr)108 12/16/22 12:07 12/27/22 18:55 185-116
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-3Client Sample ID: 149-SB-1-20-12-22
Matrix: SolidDate Collected: 12/13/22 12:15
Percent Solids: 94.5Date Received: 12/15/22 09:00
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
LOQ DL
340 U 1800 110 ug/Kg ☼12/16/22 15:30 12/20/22 12:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
340 32 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U1,2,4,5-Tetrachlorobenzene
340 32 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U1,2,4-Trichlorobenzene
340 38 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U1,2-Dichlorobenzene
340 35 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U1,2-Diphenylhydrazine
340 35 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U1,3-Dichlorobenzene
340 36 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U1,4-Dichlorobenzene
340 32 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U1-Methylnaphthalene
340 23 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼86 U2,3,4,6-Tetrachlorophenol
340 36 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U2,4,5-Trichlorophenol
340 30 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U2,4,6-Trichlorophenol
340 36 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U2,4-Dichlorophenol
340 45 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U2,4-Dimethylphenol
1800 860 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼1300 U2,4-Dinitrophenol
340 50 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼86 U2,4-Dinitrotoluene
340 28 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U2,6-Dichlorophenol
340 43 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U2,6-Dinitrotoluene
340 36 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U2-Chloronaphthalene
340 41 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U2-Chlorophenol
340 39 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U2-Methylnaphthalene
340 28 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U2-Methylphenol
1800 46 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼180 U2-Nitroaniline
340 42 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U2-Nitrophenol
340 44 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U3 & 4 Methylphenol
680 29 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U3,3'-Dichlorobenzidine
1800 47 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼86 U3-Nitroaniline
1800 180 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼340 U4,6-Dinitro-2-methylphenol
340 37 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U4-Bromophenyl phenyl ether
340 36 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U4-Chloro-3-methylphenol
680 54 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼86 U4-Chloroaniline
340 45 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U4-Chlorophenyl phenyl ether
1800 50 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼86 U M Q4-Nitroaniline
1800 340 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼690 U4-Nitrophenol
340 42 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UAcenaphthene
340 37 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UAcenaphthylene
340 29 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UAcetophenone
340 26 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UAnthracene
340 24 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UAtrazine
340 49 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼340 UAzobenzene
340 60 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼180 U QBenzaldehyde
340 28 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UBenzo[a]anthracene
340 54 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼86 UBenzo[a]pyrene
340 39 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UBenzo[b]fluoranthene
340 23 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UBenzo[g,h,i]perylene
340 67 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼180 UBenzo[k]fluoranthene
340 34 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UBenzyl alcohol
340 31 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 Ubis (2-chloroisopropyl) ether
340 40 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UBis(2-chloroethoxy)methane
340 46 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼86 UBis(2-chloroethyl)ether
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-3Client Sample ID: 149-SB-1-20-12-22
Matrix: SolidDate Collected: 12/13/22 12:15
Percent Solids: 94.5Date Received: 12/15/22 09:00
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
69 U 340 30 ug/Kg ☼12/16/22 15:30 12/20/22 12:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Bis(2-ethylhexyl) phthalate
340 27 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UButyl benzyl phthalate
340 68 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼180 U QCaprolactam
340 31 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UCarbazole
340 22 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UChrysene
340 40 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UDibenz(a,h)anthracene
340 34 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UDibenzofuran
340 38 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UDiethyl phthalate
340 35 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UDimethyl phthalate
340 31 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UDi-n-butyl phthalate
340 30 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UDi-n-octyl phthalate
340 42 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼140 UDiphenylamine
340 33 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UFluoranthene
340 37 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UFluorene
340 40 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U QHexachlorobenzene
340 37 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UHexachlorobutadiene
340 42 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UHexachlorocyclopentadiene
340 29 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UHexachloroethane
340 29 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U QIndeno[1,2,3-cd]pyrene
340 34 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 U MIsophorone
340 31 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UNaphthalene
340 27 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UNitrobenzene
340 33 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UN-Nitrosodi-n-propylamine
340 34 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UN-Nitrosodiphenylamine
1800 340 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼690 UPentachlorophenol
340 28 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UPhenanthrene
340 35 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UPhenol
340 28 ug/Kg 12/16/22 15:30 12/20/22 12:50 1☼69 UPyrene
2-Fluorobiphenyl (Surr)66 44-115 12/16/22 15:30 12/20/22 12:50 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)61 12/16/22 15:30 12/20/22 12:50 135-115
Nitrobenzene-d5 (Surr)61 12/16/22 15:30 12/20/22 12:50 137-122
Phenol-d5 (Surr)63 12/16/22 15:30 12/20/22 12:50 133-122
Terphenyl-d14 (Surr)70 12/16/22 15:30 12/20/22 12:50 154-127
2,4,6-Tribromophenol (Surr)53 Q 12/16/22 15:30 12/20/22 12:50 139-132
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
2.6 U 5.3 1.3 mg/Kg ☼01/18/23 06:31 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
0.084 U 0.11 0.042 mg/Kg ☼12/18/22 16:07 01/10/23 19:17 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Benzene
5.3 1.3 mg/Kg 12/18/22 16:07 01/10/23 19:17 50☼2.6 UC5-C8 Aliphatics
5.3 1.3 mg/Kg 12/18/22 16:07 01/10/23 19:17 50☼2.6 UC9-C10 Aromatics
5.3 1.3 mg/Kg 12/18/22 16:07 01/10/23 19:17 50☼2.6 UC9-C12 Aliphatics
0.11 0.042 mg/Kg 12/18/22 16:07 01/10/23 19:17 50☼0.084 UEthylbenzene
0.11 0.042 mg/Kg 12/18/22 16:07 01/10/23 19:17 50☼0.084 UMethyl tert-butyl ether
0.32 0.11 mg/Kg 12/18/22 16:07 01/10/23 19:17 50☼0.21 UNaphthalene
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-3Client Sample ID: 149-SB-1-20-12-22
Matrix: SolidDate Collected: 12/13/22 12:15
Percent Solids: 94.5Date Received: 12/15/22 09:00
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
LOQ DL
0.084 U 0.11 0.042 mg/Kg ☼12/18/22 16:07 01/10/23 19:17 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Toluene
5.3 1.3 mg/Kg 12/18/22 16:07 01/10/23 19:17 50☼2.6 UC9-C12 Aliphatics (adjusted)
0.26 0.11 mg/Kg 12/18/22 16:07 01/10/23 19:17 50☼0.21 Um-Xylene & p-Xylene
0.11 0.042 mg/Kg 12/18/22 16:07 01/10/23 19:17 50☼0.084 Uo-Xylene
5.3 1.3 mg/Kg 12/18/22 16:07 01/10/23 19:17 50☼2.6 UC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)86 70-130 12/18/22 16:07 01/10/23 19:17 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)85 12/18/22 16:07 01/10/23 19:17 5070-130
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
LOQ DL
0.42 U 0.53 0.21 mg/Kg ☼12/22/22 15:40 12/31/22 04:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acenaphthene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:41 1☼0.42 UAcenaphthylene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:41 1☼0.42 UAnthracene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:41 1☼0.42 UBenzo[a]anthracene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:41 1☼0.42 UBenzo[a]pyrene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:41 1☼0.42 UBenzo[b]fluoranthene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:41 1☼0.42 UBenzo[g,h,i]perylene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:41 1☼0.42 UBenzo[k]fluoranthene
13 2.0 mg/Kg 12/22/22 15:40 12/31/22 04:18 1☼4.0 UC19-C36 Aliphatics
6.3 1.6 mg/Kg 12/22/22 15:40 12/31/22 04:18 1☼2.0 JC9-C18 Aliphatics
13 4.4 mg/Kg 12/22/22 15:40 12/31/22 04:41 1☼8.9 UC11-C22 Aromatics
13 4.4 mg/Kg 12/22/22 15:40 12/31/22 04:41 1☼8.9 UC11-C22 Aromatics (Adjusted)
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:41 1☼0.42 UChrysene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:41 1☼0.42 UDibenz(a,h)anthracene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:41 1☼0.42 UFluoranthene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:41 1☼0.42 UFluorene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:41 1☼0.42 UIndeno[1,2,3-cd]pyrene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:41 1☼0.42 U2-Methylnaphthalene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:41 1☼0.42 U MNaphthalene
0.53 0.21 mg/Kg 12/22/22 15:40 12/31/22 04:41 1☼0.42 UPhenanthrene
2.1 0.74 mg/Kg 12/22/22 15:40 12/31/22 04:41 1☼1.7 UPyrene
1-Chlorooctadecane (Surr)62 40-140 12/22/22 15:40 12/31/22 04:18 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)82 12/22/22 15:40 12/31/22 04:41 140-140
o- terphenyl (Surr)65 12/22/22 15:40 12/31/22 04:41 140-140
Method: SW846 7199 - Chromium, Hexavalent (IC)
LOQ DL
310 J 430 150 ug/Kg ☼01/12/23 10:42 01/12/23 20:22 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Chromium (hexavalent)
430 150 ug/Kg 01/12/23 10:42 01/12/23 20:28 1☼280 JChromium (hexavalent)
Method: SW846 6020B - Metals (ICP/MS)
LOQ DL
2500000 10000 2100 ug/Kg ☼12/15/22 13:26 12/16/22 16:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Aluminum
1000 100 ug/Kg 12/15/22 13:26 12/16/22 16:02 1☼300 UAntimony
500 100 ug/Kg 12/15/22 13:26 12/16/22 16:02 1☼320 JArsenic
500 60 ug/Kg 12/15/22 13:26 12/16/22 16:02 1☼890Barium
50 15 ug/Kg 12/15/22 13:26 12/16/22 16:02 1☼49 JBeryllium
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-3Client Sample ID: 149-SB-1-20-12-22
Matrix: SolidDate Collected: 12/13/22 12:15
Percent Solids: 94.5Date Received: 12/15/22 09:00
Method: SW846 6020B - Metals (ICP/MS) (Continued)
LOQ DL
40 U 50 15 ug/Kg ☼12/15/22 13:26 12/16/22 16:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Cadmium
50000 6300 ug/Kg 12/15/22 13:26 12/16/22 16:02 1☼30000 JCalcium
1000 110 ug/Kg 12/15/22 13:26 12/16/22 16:02 1☼1900Chromium
50 10 ug/Kg 12/15/22 13:26 12/16/22 16:02 1☼47 JCobalt
500 130 ug/Kg 12/15/22 13:26 12/16/22 16:02 1☼770Copper
25000 3500 ug/Kg 12/15/22 13:26 12/16/22 16:02 1☼550000Iron
200 50 ug/Kg 12/15/22 13:26 12/16/22 16:02 1☼1200Lead
25000 3300 ug/Kg 12/15/22 13:26 12/16/22 16:02 1☼6400 JMagnesium
1000 120 ug/Kg 12/15/22 13:26 12/16/22 16:02 1☼390 JManganese
1000 260 ug/Kg 12/15/22 13:26 12/16/22 16:02 1☼750 UNickel
25000 9100 ug/Kg 12/15/22 13:26 12/16/22 16:02 1☼28000Potassium
500 100 ug/Kg 12/15/22 13:26 12/16/22 16:02 1☼300 USelenium
100 10 ug/Kg 12/15/22 13:26 12/16/22 16:02 1☼30 USilver
40000 10000 ug/Kg 12/15/22 13:26 12/16/22 16:02 1☼25000 USodium
100 50 ug/Kg 12/15/22 13:26 12/16/22 16:02 1☼100 UThallium
2000 270 ug/Kg 12/15/22 13:26 12/16/22 16:02 1☼2000Vanadium
2500 1000 ug/Kg 12/15/22 13:26 12/16/22 16:02 1☼2000 UZinc
Lab Sample ID: 680-227663-4Client Sample ID: 149-SB-1-30-12-22
Matrix: SolidDate Collected: 12/13/22 13:30
Percent Solids: 76.2Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS)
LOQ DL
34 U Q 67 15 ug/Kg ☼12/16/22 12:07 12/27/22 19:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acetone
13 3.2 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 UBenzene
13 3.0 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 UBromoform
13 3.2 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 UBromomethane
34 12 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼27 U Q2-Butanone (MEK)
13 2.8 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 U QCarbon disulfide
13 2.8 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 UCarbon tetrachloride
6.7 1.9 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼5.4 UChlorobenzene
13 2.8 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 UChlorodibromomethane
13 3.0 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼11 UChloroethane
6.7 2.7 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼5.4 UChloroform
13 3.2 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 U QChloromethane
13 3.9 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼11 Ucis-1,2-Dichloroethene
13 3.0 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 Ucis-1,3-Dichloropropene
13 3.1 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 UCyclohexane
13 2.2 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼5.4 U1,2-Dibromo-3-Chloropropane
6.7 2.3 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼5.4 U1,2-Dichlorobenzene
6.7 2.7 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼5.4 U1,3-Dichlorobenzene
6.7 2.4 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼5.4 U1,4-Dichlorobenzene
6.7 2.7 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼5.4 UDichlorobromomethane
13 4.3 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼11 UDichlorodifluoromethane
13 3.9 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 U1,1-Dichloroethane
13 3.1 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 U1,2-Dichloroethane
6.7 4.9 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼5.4 U1,1-Dichloroethene
13 3.5 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼11 U1,2-Dichloropropane
13 2.8 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 UEthylbenzene
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-4Client Sample ID: 149-SB-1-30-12-22
Matrix: SolidDate Collected: 12/13/22 13:30
Percent Solids: 76.2Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
5.4 U 6.7 2.3 ug/Kg ☼12/16/22 12:07 12/27/22 19:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dibromoethane (EDB)
67 26 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼54 U Q2-Hexanone
13 3.0 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 UIsopropylbenzene
34 11 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼22 UMethyl acetate
6.7 2.7 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼5.4 UMethylcyclohexane
67 11 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼34 U MMethylene Chloride
130 24 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼54 U Q4-Methyl-2-pentanone (MIBK)
13 3.0 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 UMethyl tert-butyl ether
6.7 2.6 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼5.4 UStyrene
6.7 2.8 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼5.4 U1,1,2,2-Tetrachloroethane
13 3.5 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼11 U QTetrachloroethene
27 3.5 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼13 UToluene
13 3.1 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 Utrans-1,2-Dichloroethene
27 3.5 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼13 Utrans-1,3-Dichloropropene
13 3.4 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 U1,2,4-Trichlorobenzene
13 3.5 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 U1,1,1-Trichloroethane
6.7 2.0 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼5.4 U1,1,2-Trichloroethane
6.7 2.4 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼5.4 UTrichloroethene
13 4.2 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼11 UTrichlorofluoromethane
6.7 3.9 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼5.4 U Q1,1,2-Trichloro-1,2,2-trifluoroethane
13 3.8 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼11 UVinyl chloride
27 4.9 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼13 UXylenes, Total
67 35 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼67 UPropionitrile
13 8.5 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼13 UPentachloroethane
13 6.1 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼13 UMethyl methacrylate
27 5.5 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼13 UHexachlorobutadiene
6.7 2.7 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼5.4 UDibromomethane
67 55 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼67 U QAcetonitrile
13 4.2 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼11 UNaphthalene
13 2.3 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 U QIodomethane
13 4.7 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼11 U3-Chloro-1-propene
270 40 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼130 UAcrylonitrile
27 3.8 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼13 UEthyl methacrylate
13 1.8 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 U1,1,1,2-Tetrachloroethane
13 3.2 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 Utrans-1,4-Dichloro-2-butene
6.7 2.8 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 U Q2-Chloro-1,3-butadiene
67 31 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼67 UMethacrylonitrile
270 100 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼220 U QAcrolein
13 2.4 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 U M1,2,3-Trichloropropane
54 7.4 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼27 U QVinyl acetate
670 130 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼270 U QIsobutyl alcohol
13 13 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼13 U2-Nitropropane
180 180 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼180 Un-Butyl alcohol
6.7 2.7 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼5.4 UBromochloromethane
13 3.5 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼11 UDiethyl ether
27 8.4 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼24 U QTetrahydrofuran
13 13 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼13 UEthyl acetate
6.7 6.7 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 UBenzyl chloride
13 2.6 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 Un-Butylbenzene
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-4Client Sample ID: 149-SB-1-30-12-22
Matrix: SolidDate Collected: 12/13/22 13:30
Percent Solids: 76.2Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
6.7 U 13 3.4 ug/Kg ☼12/16/22 12:07 12/27/22 19:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2,4-Trimethylbenzene
13 3.1 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 U2-Chlorotoluene
6.7 6.7 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 Un-Butyl acetate
13 4.2 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼11 U1,2-Dichloroethene, Total
6.7 2.7 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼5.4 U1,1-Dichloropropene
6.7 6.7 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 U2-Methylnaphthalene
13 3.1 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 Uo-Xylene
6.7 2.3 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼5.4 UHexane
13 2.8 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 U4-Chlorotoluene
6.7 2.8 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 U Q1-Chlorohexane
6.7 2.3 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼5.4 UBromobenzene
6.7 2.7 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼5.4 U1,2,3-Trichlorobenzene
27 6.3 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼13 U1,3-Dichloropropene, Total
13 2.7 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 Usec-Butylbenzene
13 3.0 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 U2,2-Dichloropropane
13 3.0 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 UN-Propylbenzene
6.7 6.7 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 U1,3,5-Trichlorobenzene
13 2.0 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼13 UDiisopropyl ether
340 340 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼340 U QEthanol
67 67 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼67 UIsopropyl alcohol
27 3.5 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼13 Up-Cymene
6.7 6.7 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 U QTert-amyl methyl ether
13 3.2 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 U1,3,5-Trimethylbenzene
6.7 6.7 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 U1,2,3-Trimethylbenzene
13 3.0 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 Um-Xylene & p-Xylene
13 3.2 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼11 UDichlorofluoromethane
13 3.4 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 Utert-Butylbenzene
6.7 6.7 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 U QIsooctane
13 3.0 ug/Kg 12/16/22 12:07 12/27/22 19:18 1☼6.7 U1,3-Dichloropropane
4-Bromofluorobenzene (Surr)91 79-119 12/16/22 12:07 12/27/22 19:18 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)107 12/16/22 12:07 12/27/22 19:18 178-119
1,2-Dichloroethane-d4 (Surr)100 12/16/22 12:07 12/27/22 19:18 171-138
Toluene-d8 (Surr)106 12/16/22 12:07 12/27/22 19:18 185-116
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
LOQ DL
420 U 2100 140 ug/Kg ☼12/16/22 15:30 12/20/22 13:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
420 39 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U1,2,4,5-Tetrachlorobenzene
420 39 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U1,2,4-Trichlorobenzene
420 47 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U1,2-Dichlorobenzene
420 43 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U1,2-Diphenylhydrazine
420 43 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U1,3-Dichlorobenzene
420 44 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U1,4-Dichlorobenzene
420 39 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U1-Methylnaphthalene
420 28 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼100 U2,3,4,6-Tetrachlorophenol
420 44 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U2,4,5-Trichlorophenol
420 37 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U2,4,6-Trichlorophenol
420 44 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U2,4-Dichlorophenol
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-4Client Sample ID: 149-SB-1-30-12-22
Matrix: SolidDate Collected: 12/13/22 13:30
Percent Solids: 76.2Date Received: 12/15/22 09:00
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
85 U 420 56 ug/Kg ☼12/16/22 15:30 12/20/22 13:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2,4-Dimethylphenol
2100 1000 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼1600 U2,4-Dinitrophenol
420 62 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼100 U2,4-Dinitrotoluene
420 34 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U2,6-Dichlorophenol
420 53 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U2,6-Dinitrotoluene
420 44 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U2-Chloronaphthalene
420 50 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U2-Chlorophenol
420 48 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U2-Methylnaphthalene
420 34 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U2-Methylphenol
2100 57 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼210 U2-Nitroaniline
420 52 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U2-Nitrophenol
420 54 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U3 & 4 Methylphenol
830 35 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U3,3'-Dichlorobenzidine
2100 58 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼100 U3-Nitroaniline
2100 210 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼420 U4,6-Dinitro-2-methylphenol
420 45 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U4-Bromophenyl phenyl ether
420 44 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U4-Chloro-3-methylphenol
830 66 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼100 U4-Chloroaniline
420 56 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U4-Chlorophenyl phenyl ether
2100 62 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼100 U Q4-Nitroaniline
2100 420 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼850 U4-Nitrophenol
420 52 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UAcenaphthene
420 45 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UAcenaphthylene
420 35 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UAcetophenone
420 32 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UAnthracene
420 29 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UAtrazine
420 61 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼420 UAzobenzene
420 73 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼210 U QBenzaldehyde
420 34 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UBenzo[a]anthracene
420 66 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼100 UBenzo[a]pyrene
420 48 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UBenzo[b]fluoranthene
420 28 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UBenzo[g,h,i]perylene
420 82 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼210 UBenzo[k]fluoranthene
420 42 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UBenzyl alcohol
420 38 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 Ubis (2-chloroisopropyl) ether
420 49 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UBis(2-chloroethoxy)methane
420 57 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼100 UBis(2-chloroethyl)ether
420 37 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UBis(2-ethylhexyl) phthalate
420 33 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UButyl benzyl phthalate
420 83 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼210 U QCaprolactam
420 38 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UCarbazole
420 27 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UChrysene
420 49 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UDibenz(a,h)anthracene
420 42 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UDibenzofuran
420 47 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UDiethyl phthalate
420 43 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UDimethyl phthalate
420 38 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UDi-n-butyl phthalate
420 37 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UDi-n-octyl phthalate
420 52 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼180 U MDiphenylamine
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-4Client Sample ID: 149-SB-1-30-12-22
Matrix: SolidDate Collected: 12/13/22 13:30
Percent Solids: 76.2Date Received: 12/15/22 09:00
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
85 U 420 40 ug/Kg ☼12/16/22 15:30 12/20/22 13:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Fluoranthene
420 45 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UFluorene
420 49 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U QHexachlorobenzene
420 45 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UHexachlorobutadiene
420 52 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UHexachlorocyclopentadiene
420 35 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UHexachloroethane
420 35 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 U QIndeno[1,2,3-cd]pyrene
420 42 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UIsophorone
420 38 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UNaphthalene
420 33 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UNitrobenzene
420 40 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UN-Nitrosodi-n-propylamine
420 42 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UN-Nitrosodiphenylamine
2100 420 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼850 UPentachlorophenol
420 34 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UPhenanthrene
420 43 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UPhenol
420 34 ug/Kg 12/16/22 15:30 12/20/22 13:11 1☼85 UPyrene
2-Fluorobiphenyl (Surr)63 44-115 12/16/22 15:30 12/20/22 13:11 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)58 12/16/22 15:30 12/20/22 13:11 135-115
Nitrobenzene-d5 (Surr)53 12/16/22 15:30 12/20/22 13:11 137-122
Phenol-d5 (Surr)59 12/16/22 15:30 12/20/22 13:11 133-122
Terphenyl-d14 (Surr)67 12/16/22 15:30 12/20/22 13:11 154-127
2,4,6-Tribromophenol (Surr)50 Q 12/16/22 15:30 12/20/22 13:11 139-132
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
3.3 U 6.6 1.6 mg/Kg ☼01/18/23 06:31 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
0.10 U 0.13 0.052 mg/Kg ☼12/18/22 16:07 01/10/23 19:58 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Benzene
6.6 1.6 mg/Kg 12/18/22 16:07 01/10/23 19:58 50☼3.3 UC5-C8 Aliphatics
6.6 1.6 mg/Kg 12/18/22 16:07 01/10/23 19:58 50☼3.3 UC9-C10 Aromatics
6.6 1.6 mg/Kg 12/18/22 16:07 01/10/23 19:58 50☼3.3 UC9-C12 Aliphatics
0.13 0.052 mg/Kg 12/18/22 16:07 01/10/23 19:58 50☼0.10 UEthylbenzene
0.13 0.052 mg/Kg 12/18/22 16:07 01/10/23 19:58 50☼0.10 UMethyl tert-butyl ether
0.39 0.13 mg/Kg 12/18/22 16:07 01/10/23 19:58 50☼0.26 UNaphthalene
0.13 0.052 mg/Kg 12/18/22 16:07 01/10/23 19:58 50☼0.10 UToluene
6.6 1.6 mg/Kg 12/18/22 16:07 01/10/23 19:58 50☼3.3 UC9-C12 Aliphatics (adjusted)
0.33 0.13 mg/Kg 12/18/22 16:07 01/10/23 19:58 50☼0.26 Um-Xylene & p-Xylene
0.13 0.052 mg/Kg 12/18/22 16:07 01/10/23 19:58 50☼0.10 Uo-Xylene
6.6 1.6 mg/Kg 12/18/22 16:07 01/10/23 19:58 50☼3.3 UC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)89 70-130 12/18/22 16:07 01/10/23 19:58 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)88 12/18/22 16:07 01/10/23 19:58 5070-130
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
LOQ DL
0.51 U 0.64 0.26 mg/Kg ☼12/22/22 15:40 12/31/22 05:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acenaphthene
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-4Client Sample ID: 149-SB-1-30-12-22
Matrix: SolidDate Collected: 12/13/22 13:30
Percent Solids: 76.2Date Received: 12/15/22 09:00
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
LOQ DL
0.51 U 0.64 0.26 mg/Kg ☼12/22/22 15:40 12/31/22 05:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acenaphthylene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 05:03 1☼0.51 UAnthracene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 05:03 1☼0.51 UBenzo[a]anthracene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 05:03 1☼0.51 UBenzo[a]pyrene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 05:03 1☼0.51 UBenzo[b]fluoranthene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 05:03 1☼0.51 UBenzo[g,h,i]perylene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 05:03 1☼0.51 UBenzo[k]fluoranthene
15 2.4 mg/Kg 12/22/22 15:40 12/31/22 04:41 1☼4.9 UC19-C36 Aliphatics
7.7 1.9 mg/Kg 12/22/22 15:40 12/31/22 04:41 1☼2.2 JC9-C18 Aliphatics
15 5.4 mg/Kg 12/22/22 15:40 12/31/22 05:03 1☼11 UC11-C22 Aromatics
15 5.4 mg/Kg 12/22/22 15:40 12/31/22 05:03 1☼11 UC11-C22 Aromatics (Adjusted)
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 05:03 1☼0.51 UChrysene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 05:03 1☼0.51 UDibenz(a,h)anthracene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 05:03 1☼0.51 UFluoranthene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 05:03 1☼0.51 UFluorene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 05:03 1☼0.51 UIndeno[1,2,3-cd]pyrene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 05:03 1☼0.51 U2-Methylnaphthalene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 05:03 1☼0.51 UNaphthalene
0.64 0.26 mg/Kg 12/22/22 15:40 12/31/22 05:03 1☼0.51 UPhenanthrene
2.6 0.89 mg/Kg 12/22/22 15:40 12/31/22 05:03 1☼2.0 UPyrene
1-Chlorooctadecane (Surr)52 40-140 12/22/22 15:40 12/31/22 04:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)87 12/22/22 15:40 12/31/22 05:03 140-140
o- terphenyl (Surr)59 12/22/22 15:40 12/31/22 05:03 140-140
Method: SW846 7199 - Chromium, Hexavalent (IC)
LOQ DL
410 U 540 190 ug/Kg ☼01/12/23 10:42 01/12/23 20:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Chromium (hexavalent)
540 190 ug/Kg 01/12/23 10:42 01/12/23 20:15 1☼240 JChromium (hexavalent)
Method: SW846 6020B - Metals (ICP/MS)
LOQ DL
1700000 11000 2400 ug/Kg ☼12/15/22 13:26 12/16/22 16:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Aluminum
1100 110 ug/Kg 12/15/22 13:26 12/16/22 16:06 1☼340 UAntimony
570 110 ug/Kg 12/15/22 13:26 12/16/22 16:06 1☼1600Arsenic
570 68 ug/Kg 12/15/22 13:26 12/16/22 16:06 1☼820Barium
57 17 ug/Kg 12/15/22 13:26 12/16/22 16:06 1☼50 JBeryllium
57 17 ug/Kg 12/15/22 13:26 12/16/22 16:06 1☼46 UCadmium
57000 7200 ug/Kg 12/15/22 13:26 12/16/22 16:06 1☼14000 JCalcium
1100 130 ug/Kg 12/15/22 13:26 12/16/22 16:06 1☼5000Chromium
57 11 ug/Kg 12/15/22 13:26 12/16/22 16:06 1☼120Cobalt
570 150 ug/Kg 12/15/22 13:26 12/16/22 16:06 1☼2000Copper
29000 4000 ug/Kg 12/15/22 13:26 12/16/22 16:06 1☼2900000Iron
230 57 ug/Kg 12/15/22 13:26 12/16/22 16:06 1☼2200Lead
29000 3800 ug/Kg 12/15/22 13:26 12/16/22 16:06 1☼10000 UMagnesium
1100 140 ug/Kg 12/15/22 13:26 12/16/22 16:06 1☼2000Manganese
1100 300 ug/Kg 12/15/22 13:26 12/16/22 16:06 1☼860 UNickel
29000 10000 ug/Kg 12/15/22 13:26 12/16/22 16:06 1☼21000 JPotassium
570 110 ug/Kg 12/15/22 13:26 12/16/22 16:06 1☼200 JSelenium
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-4Client Sample ID: 149-SB-1-30-12-22
Matrix: SolidDate Collected: 12/13/22 13:30
Percent Solids: 76.2Date Received: 12/15/22 09:00
Method: SW846 6020B - Metals (ICP/MS) (Continued)
LOQ DL
34 U 110 11 ug/Kg ☼12/15/22 13:26 12/16/22 16:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Silver
46000 11000 ug/Kg 12/15/22 13:26 12/16/22 16:06 1☼14000 JSodium
110 57 ug/Kg 12/15/22 13:26 12/16/22 16:06 1☼110 UThallium
2300 310 ug/Kg 12/15/22 13:26 12/16/22 16:06 1☼4300Vanadium
2900 1100 ug/Kg 12/15/22 13:26 12/16/22 16:06 1☼2300 UZinc
Lab Sample ID: 680-227663-5Client Sample ID: 149-SB-1-40-12-22
Matrix: SolidDate Collected: 12/13/22 14:00
Percent Solids: 87.9Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS)
LOQ DL
23 U Q 47 10 ug/Kg ☼12/16/22 12:07 12/27/22 19:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acetone
9.3 2.2 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 UBenzene
9.3 2.1 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 UBromoform
9.3 2.2 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 UBromomethane
23 8.6 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼19 U Q2-Butanone (MEK)
9.3 2.0 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U QCarbon disulfide
9.3 2.0 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 UCarbon tetrachloride
4.7 1.3 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼3.7 UChlorobenzene
9.3 2.0 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 UChlorodibromomethane
9.3 2.1 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼7.5 UChloroethane
4.7 1.9 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼3.7 UChloroform
9.3 2.2 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U QChloromethane
9.3 2.7 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼7.5 Ucis-1,2-Dichloroethene
9.3 2.1 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 Ucis-1,3-Dichloropropene
9.3 2.1 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 UCyclohexane
9.3 1.5 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼3.7 U1,2-Dibromo-3-Chloropropane
4.7 1.6 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼3.7 U1,2-Dichlorobenzene
4.7 1.9 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼3.7 U1,3-Dichlorobenzene
4.7 1.7 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼3.7 U1,4-Dichlorobenzene
4.7 1.9 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼3.7 UDichlorobromomethane
9.3 3.0 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼7.5 UDichlorodifluoromethane
9.3 2.7 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U1,1-Dichloroethane
9.3 2.1 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U1,2-Dichloroethane
4.7 3.4 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼3.7 U1,1-Dichloroethene
9.3 2.4 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼7.5 U1,2-Dichloropropane
9.3 2.0 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 UEthylbenzene
4.7 1.6 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼3.7 U1,2-Dibromoethane (EDB)
47 18 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼37 U Q2-Hexanone
9.3 2.1 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U MIsopropylbenzene
23 7.6 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼15 UMethyl acetate
4.7 1.9 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼3.7 UMethylcyclohexane
47 7.5 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼23 U MMethylene Chloride
93 17 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼37 U Q4-Methyl-2-pentanone (MIBK)
9.3 2.1 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 UMethyl tert-butyl ether
4.7 1.8 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼3.7 UStyrene
4.7 2.0 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼3.7 U1,1,2,2-Tetrachloroethane
9.3 2.4 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼7.5 U QTetrachloroethene
19 2.4 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼9.3 UToluene
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Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-5Client Sample ID: 149-SB-1-40-12-22
Matrix: SolidDate Collected: 12/13/22 14:00
Percent Solids: 87.9Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
4.7 U 9.3 2.1 ug/Kg ☼12/16/22 12:07 12/27/22 19:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
trans-1,2-Dichloroethene
19 2.4 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼9.3 Utrans-1,3-Dichloropropene
9.3 2.3 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U1,2,4-Trichlorobenzene
9.3 2.4 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U1,1,1-Trichloroethane
4.7 1.4 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼3.7 U1,1,2-Trichloroethane
4.7 1.7 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼3.7 UTrichloroethene
9.3 2.9 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼7.5 UTrichlorofluoromethane
4.7 2.7 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼3.7 U Q1,1,2-Trichloro-1,2,2-trifluoroethane
9.3 2.6 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼7.5 UVinyl chloride
19 3.4 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼9.3 UXylenes, Total
47 24 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼47 UPropionitrile
9.3 5.9 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼9.3 UPentachloroethane
9.3 4.2 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼9.3 UMethyl methacrylate
19 3.8 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼9.3 UHexachlorobutadiene
4.7 1.9 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼3.7 UDibromomethane
47 38 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼47 U QAcetonitrile
9.3 2.9 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼7.5 UNaphthalene
9.3 1.6 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U QIodomethane
9.3 3.3 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼7.5 U3-Chloro-1-propene
190 28 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼93 UAcrylonitrile
19 2.6 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼9.3 UEthyl methacrylate
9.3 1.2 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U1,1,1,2-Tetrachloroethane
9.3 2.2 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 Utrans-1,4-Dichloro-2-butene
4.7 2.0 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U Q2-Chloro-1,3-butadiene
47 21 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼47 UMethacrylonitrile
190 69 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼150 U QAcrolein
9.3 1.7 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U M1,2,3-Trichloropropane
37 5.1 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼19 U QVinyl acetate
470 87 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼190 U QIsobutyl alcohol
9.3 9.3 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼9.3 U2-Nitropropane
120 120 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼120 Un-Butyl alcohol
4.7 1.9 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼3.7 UBromochloromethane
9.3 2.4 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼7.5 UDiethyl ether
19 5.8 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼17 U QTetrahydrofuran
9.3 9.3 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼9.3 UEthyl acetate
4.7 4.7 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 UBenzyl chloride
9.3 1.8 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 Un-Butylbenzene
9.3 2.3 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U1,2,4-Trimethylbenzene
9.3 2.1 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U2-Chlorotoluene
4.7 4.7 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 Un-Butyl acetate
9.3 2.9 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼7.5 U1,2-Dichloroethene, Total
4.7 1.9 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼3.7 U1,1-Dichloropropene
4.7 4.7 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U2-Methylnaphthalene
9.3 2.1 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 Uo-Xylene
4.7 1.6 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼3.7 UHexane
9.3 2.0 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U4-Chlorotoluene
4.7 2.0 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U Q1-Chlorohexane
4.7 1.6 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼3.7 UBromobenzene
4.7 1.9 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼3.7 U1,2,3-Trichlorobenzene
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-5Client Sample ID: 149-SB-1-40-12-22
Matrix: SolidDate Collected: 12/13/22 14:00
Percent Solids: 87.9Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
9.3 U 19 4.4 ug/Kg ☼12/16/22 12:07 12/27/22 19:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,3-Dichloropropene, Total
9.3 1.9 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 Usec-Butylbenzene
9.3 2.1 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U2,2-Dichloropropane
9.3 2.1 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 UN-Propylbenzene
4.7 4.7 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U1,3,5-Trichlorobenzene
9.3 1.4 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼9.3 UDiisopropyl ether
230 230 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼230 U QEthanol
47 47 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼47 UIsopropyl alcohol
19 2.4 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼9.3 Up-Cymene
4.7 4.7 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U QTert-amyl methyl ether
9.3 2.2 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U1,3,5-Trimethylbenzene
4.7 4.7 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U1,2,3-Trimethylbenzene
9.3 2.1 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 Um-Xylene & p-Xylene
9.3 2.2 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼7.5 UDichlorofluoromethane
9.3 2.3 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 Utert-Butylbenzene
4.7 4.7 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U QIsooctane
9.3 2.1 ug/Kg 12/16/22 12:07 12/27/22 19:42 1☼4.7 U1,3-Dichloropropane
4-Bromofluorobenzene (Surr)91 79-119 12/16/22 12:07 12/27/22 19:42 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)108 12/16/22 12:07 12/27/22 19:42 178-119
1,2-Dichloroethane-d4 (Surr)100 12/16/22 12:07 12/27/22 19:42 171-138
Toluene-d8 (Surr)106 12/16/22 12:07 12/27/22 19:42 185-116
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
LOQ DL
370 U 1900 120 ug/Kg ☼12/16/22 15:30 12/20/22 13:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
370 35 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U1,2,4,5-Tetrachlorobenzene
370 35 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U1,2,4-Trichlorobenzene
370 42 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U1,2-Dichlorobenzene
370 38 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U1,2-Diphenylhydrazine
370 38 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U1,3-Dichlorobenzene
370 39 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U1,4-Dichlorobenzene
370 35 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U1-Methylnaphthalene
370 25 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼93 U2,3,4,6-Tetrachlorophenol
370 39 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U2,4,5-Trichlorophenol
370 33 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U2,4,6-Trichlorophenol
370 39 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U2,4-Dichlorophenol
370 49 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U2,4-Dimethylphenol
1900 930 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼1500 U2,4-Dinitrophenol
370 55 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼93 U M2,4-Dinitrotoluene
370 30 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U2,6-Dichlorophenol
370 47 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U M2,6-Dinitrotoluene
370 39 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U2-Chloronaphthalene
370 45 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U2-Chlorophenol
370 43 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U2-Methylnaphthalene
370 30 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U2-Methylphenol
1900 51 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼190 U2-Nitroaniline
370 46 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U2-Nitrophenol
370 48 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U3 & 4 Methylphenol
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-5Client Sample ID: 149-SB-1-40-12-22
Matrix: SolidDate Collected: 12/13/22 14:00
Percent Solids: 87.9Date Received: 12/15/22 09:00
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
75 U 740 31 ug/Kg ☼12/16/22 15:30 12/20/22 13:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3,3'-Dichlorobenzidine
1900 52 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼93 U3-Nitroaniline
1900 190 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼370 U4,6-Dinitro-2-methylphenol
370 40 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U4-Bromophenyl phenyl ether
370 39 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U4-Chloro-3-methylphenol
740 58 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼93 U4-Chloroaniline
370 49 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U4-Chlorophenyl phenyl ether
1900 55 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼93 U M Q4-Nitroaniline
1900 370 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼750 U4-Nitrophenol
370 46 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UAcenaphthene
370 40 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UAcenaphthylene
370 31 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UAcetophenone
370 28 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UAnthracene
370 26 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UAtrazine
370 54 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼370 UAzobenzene
370 65 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼190 U QBenzaldehyde
370 30 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UBenzo[a]anthracene
370 58 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼93 UBenzo[a]pyrene
370 43 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UBenzo[b]fluoranthene
370 25 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UBenzo[g,h,i]perylene
370 73 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼190 UBenzo[k]fluoranthene
370 37 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UBenzyl alcohol
370 34 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 Ubis (2-chloroisopropyl) ether
370 44 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UBis(2-chloroethoxy)methane
370 51 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼93 UBis(2-chloroethyl)ether
370 33 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UBis(2-ethylhexyl) phthalate
370 29 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UButyl benzyl phthalate
370 74 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼190 U QCaprolactam
370 34 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UCarbazole
370 24 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UChrysene
370 44 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UDibenz(a,h)anthracene
370 37 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UDibenzofuran
370 42 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UDiethyl phthalate
370 38 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UDimethyl phthalate
370 34 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UDi-n-butyl phthalate
370 33 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UDi-n-octyl phthalate
370 46 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼160 U MDiphenylamine
370 36 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UFluoranthene
370 40 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UFluorene
370 44 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U QHexachlorobenzene
370 40 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UHexachlorobutadiene
370 46 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UHexachlorocyclopentadiene
370 31 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UHexachloroethane
370 31 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 U QIndeno[1,2,3-cd]pyrene
370 37 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UIsophorone
370 34 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UNaphthalene
370 29 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UNitrobenzene
370 36 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UN-Nitrosodi-n-propylamine
370 37 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UN-Nitrosodiphenylamine
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-5Client Sample ID: 149-SB-1-40-12-22
Matrix: SolidDate Collected: 12/13/22 14:00
Percent Solids: 87.9Date Received: 12/15/22 09:00
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
750 U 1900 370 ug/Kg ☼12/16/22 15:30 12/20/22 13:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Pentachlorophenol
370 30 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UPhenanthrene
370 38 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UPhenol
370 30 ug/Kg 12/16/22 15:30 12/20/22 13:32 1☼75 UPyrene
2-Fluorobiphenyl (Surr)63 44-115 12/16/22 15:30 12/20/22 13:32 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)57 12/16/22 15:30 12/20/22 13:32 135-115
Nitrobenzene-d5 (Surr)58 12/16/22 15:30 12/20/22 13:32 137-122
Phenol-d5 (Surr)59 12/16/22 15:30 12/20/22 13:32 133-122
Terphenyl-d14 (Surr)69 12/16/22 15:30 12/20/22 13:32 154-127
2,4,6-Tribromophenol (Surr)52 Q 12/16/22 15:30 12/20/22 13:32 139-132
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
2.8 U 5.7 1.4 mg/Kg ☼01/18/23 06:31 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
0.091 U 0.11 0.045 mg/Kg ☼12/18/22 16:07 01/10/23 20:38 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Benzene
5.7 1.4 mg/Kg 12/18/22 16:07 01/10/23 20:38 50☼2.8 UC5-C8 Aliphatics
5.7 1.4 mg/Kg 12/18/22 16:07 01/10/23 20:38 50☼2.8 UC9-C10 Aromatics
5.7 1.4 mg/Kg 12/18/22 16:07 01/10/23 20:38 50☼2.8 UC9-C12 Aliphatics
0.11 0.045 mg/Kg 12/18/22 16:07 01/10/23 20:38 50☼0.091 UEthylbenzene
0.11 0.045 mg/Kg 12/18/22 16:07 01/10/23 20:38 50☼0.091 UMethyl tert-butyl ether
0.34 0.11 mg/Kg 12/18/22 16:07 01/10/23 20:38 50☼0.23 UNaphthalene
0.11 0.045 mg/Kg 12/18/22 16:07 01/10/23 20:38 50☼0.091 UToluene
5.7 1.4 mg/Kg 12/18/22 16:07 01/10/23 20:38 50☼2.8 UC9-C12 Aliphatics (adjusted)
0.28 0.11 mg/Kg 12/18/22 16:07 01/10/23 20:38 50☼0.23 Um-Xylene & p-Xylene
0.11 0.045 mg/Kg 12/18/22 16:07 01/10/23 20:38 50☼0.091 Uo-Xylene
5.7 1.4 mg/Kg 12/18/22 16:07 01/10/23 20:38 50☼2.8 UC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)80 70-130 12/18/22 16:07 01/10/23 20:38 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)79 12/18/22 16:07 01/10/23 20:38 5070-130
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
LOQ DL
0.44 U 0.55 0.22 mg/Kg ☼12/22/22 15:40 12/31/22 05:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acenaphthene
0.55 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:26 1☼0.44 UAcenaphthylene
0.55 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:26 1☼0.44 UAnthracene
0.55 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:26 1☼0.44 UBenzo[a]anthracene
0.55 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:26 1☼0.44 UBenzo[a]pyrene
0.55 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:26 1☼0.44 UBenzo[b]fluoranthene
0.55 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:26 1☼0.44 UBenzo[g,h,i]perylene
0.55 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:26 1☼0.44 UBenzo[k]fluoranthene
13 2.1 mg/Kg 12/22/22 15:40 12/31/22 05:03 1☼4.2 UC19-C36 Aliphatics
6.6 1.7 mg/Kg 12/22/22 15:40 12/31/22 05:03 1☼3.3 UC9-C18 Aliphatics
13 4.6 mg/Kg 12/22/22 15:40 12/31/22 05:26 1☼9.3 U MC11-C22 Aromatics
13 4.6 mg/Kg 12/22/22 15:40 12/31/22 05:26 1☼9.3 UC11-C22 Aromatics (Adjusted)
0.55 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:26 1☼0.44 UChrysene
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-5Client Sample ID: 149-SB-1-40-12-22
Matrix: SolidDate Collected: 12/13/22 14:00
Percent Solids: 87.9Date Received: 12/15/22 09:00
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
LOQ DL
0.44 U 0.55 0.22 mg/Kg ☼12/22/22 15:40 12/31/22 05:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibenz(a,h)anthracene
0.55 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:26 1☼0.44 UFluoranthene
0.55 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:26 1☼0.44 UFluorene
0.55 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:26 1☼0.44 UIndeno[1,2,3-cd]pyrene
0.55 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:26 1☼0.44 U2-Methylnaphthalene
0.55 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:26 1☼0.44 U MNaphthalene
0.55 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:26 1☼0.44 UPhenanthrene
2.2 0.77 mg/Kg 12/22/22 15:40 12/31/22 05:26 1☼1.8 UPyrene
1-Chlorooctadecane (Surr)52 40-140 12/22/22 15:40 12/31/22 05:03 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)77 12/22/22 15:40 12/31/22 05:26 140-140
o- terphenyl (Surr)52 12/22/22 15:40 12/31/22 05:26 140-140
Method: SW846 7199 - Chromium, Hexavalent (IC)
LOQ DL
190 J M 440 150 ug/Kg ☼01/12/23 10:42 01/12/23 19:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Chromium (hexavalent)
440 150 ug/Kg 01/12/23 10:42 01/12/23 20:02 1☼330 UChromium (hexavalent)
Method: SW846 6020B - Metals (ICP/MS)
LOQ DL
2100000 11000 2300 ug/Kg ☼12/15/22 13:26 12/16/22 16:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Aluminum
1100 110 ug/Kg 12/15/22 13:26 12/16/22 16:10 1☼330 UAntimony
550 110 ug/Kg 12/15/22 13:26 12/16/22 16:10 1☼960Arsenic
550 66 ug/Kg 12/15/22 13:26 12/16/22 16:10 1☼1300Barium
55 17 ug/Kg 12/15/22 13:26 12/16/22 16:10 1☼70Beryllium
55 17 ug/Kg 12/15/22 13:26 12/16/22 16:10 1☼27 JCadmium
55000 7000 ug/Kg 12/15/22 13:26 12/16/22 16:10 1☼76000Calcium
1100 120 ug/Kg 12/15/22 13:26 12/16/22 16:10 1☼21000Chromium
55 11 ug/Kg 12/15/22 13:26 12/16/22 16:10 1☼160Cobalt
550 140 ug/Kg 12/15/22 13:26 12/16/22 16:10 1☼1300Copper
28000 3900 ug/Kg 12/15/22 13:26 12/16/22 16:10 1☼1200000Iron
220 55 ug/Kg 12/15/22 13:26 12/16/22 16:10 1☼1700Lead
28000 3600 ug/Kg 12/15/22 13:26 12/16/22 16:10 1☼8300 JMagnesium
1100 130 ug/Kg 12/15/22 13:26 12/16/22 16:10 1☼1700Manganese
1100 290 ug/Kg 12/15/22 13:26 12/16/22 16:10 1☼1600Nickel
28000 10000 ug/Kg 12/15/22 13:26 12/16/22 16:10 1☼26000 JPotassium
550 110 ug/Kg 12/15/22 13:26 12/16/22 16:10 1☼330 USelenium
110 11 ug/Kg 12/15/22 13:26 12/16/22 16:10 1☼33 USilver
44000 11000 ug/Kg 12/15/22 13:26 12/16/22 16:10 1☼28000 USodium
110 55 ug/Kg 12/15/22 13:26 12/16/22 16:10 1☼110 UThallium
2200 300 ug/Kg 12/15/22 13:26 12/16/22 16:10 1☼5100Vanadium
2800 1100 ug/Kg 12/15/22 13:26 12/16/22 16:10 1☼2200 UZinc
Lab Sample ID: 680-227663-6Client Sample ID: 149-SB-1-46-12-22
Matrix: SolidDate Collected: 12/13/22 14:35
Percent Solids: 90.2Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS)
LOQ DL
26 U Q 51 11 ug/Kg ☼12/16/22 12:07 12/27/22 20:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acetone
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-6Client Sample ID: 149-SB-1-46-12-22
Matrix: SolidDate Collected: 12/13/22 14:35
Percent Solids: 90.2Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
5.1 U 10 2.5 ug/Kg ☼12/16/22 12:07 12/27/22 20:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Benzene
10 2.3 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 UBromoform
10 2.5 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 UBromomethane
26 9.5 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼21 U Q2-Butanone (MEK)
10 2.2 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 U QCarbon disulfide
10 2.2 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 UCarbon tetrachloride
5.1 1.4 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼4.1 UChlorobenzene
10 2.2 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 UChlorodibromomethane
10 2.3 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼8.2 UChloroethane
5.1 2.1 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼4.1 UChloroform
10 2.5 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 U QChloromethane
10 3.0 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼8.2 Ucis-1,2-Dichloroethene
10 2.3 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 Ucis-1,3-Dichloropropene
10 2.4 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 UCyclohexane
10 1.6 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼4.1 U1,2-Dibromo-3-Chloropropane
5.1 1.7 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼4.1 U1,2-Dichlorobenzene
5.1 2.1 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼4.1 U1,3-Dichlorobenzene
5.1 1.9 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼4.1 U1,4-Dichlorobenzene
5.1 2.1 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼4.1 UDichlorobromomethane
10 3.3 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼8.2 UDichlorodifluoromethane
10 3.0 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 U1,1-Dichloroethane
10 2.4 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 U1,2-Dichloroethane
5.1 3.7 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼4.1 U1,1-Dichloroethene
10 2.7 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼8.2 U1,2-Dichloropropane
10 2.2 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 UEthylbenzene
5.1 1.7 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼4.1 U1,2-Dibromoethane (EDB)
51 20 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼41 U Q2-Hexanone
10 2.3 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 UIsopropylbenzene
26 8.3 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼16 UMethyl acetate
5.1 2.1 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼4.1 UMethylcyclohexane
51 8.2 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼26 UMethylene Chloride
100 19 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼41 U Q4-Methyl-2-pentanone (MIBK)
10 2.3 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 UMethyl tert-butyl ether
5.1 2.0 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼4.1 UStyrene
5.1 2.2 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼4.1 U1,1,2,2-Tetrachloroethane
10 2.7 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼8.2 U QTetrachloroethene
21 2.7 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼10 UToluene
10 2.4 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 Utrans-1,2-Dichloroethene
21 2.7 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼10 Utrans-1,3-Dichloropropene
10 2.6 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 U1,2,4-Trichlorobenzene
10 2.7 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 U1,1,1-Trichloroethane
5.1 1.5 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼4.1 U1,1,2-Trichloroethane
5.1 1.9 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼4.1 UTrichloroethene
10 3.2 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼8.2 UTrichlorofluoromethane
5.1 3.0 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼4.1 U Q1,1,2-Trichloro-1,2,2-trifluoroethane
10 2.9 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼8.2 UVinyl chloride
21 3.7 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼10 UXylenes, Total
51 27 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼51 UPropionitrile
10 6.5 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼10 UPentachloroethane
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-6Client Sample ID: 149-SB-1-46-12-22
Matrix: SolidDate Collected: 12/13/22 14:35
Percent Solids: 90.2Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
10 U 10 4.6 ug/Kg ☼12/16/22 12:07 12/27/22 20:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Methyl methacrylate
21 4.2 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼10 UHexachlorobutadiene
5.1 2.1 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼4.1 UDibromomethane
51 42 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼51 U QAcetonitrile
10 3.2 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼8.2 UNaphthalene
10 1.7 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 U QIodomethane
10 3.6 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼8.2 U3-Chloro-1-propene
210 31 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼100 UAcrylonitrile
21 2.9 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼10 UEthyl methacrylate
10 1.3 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 U1,1,1,2-Tetrachloroethane
10 2.5 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 Utrans-1,4-Dichloro-2-butene
5.1 2.2 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 U Q2-Chloro-1,3-butadiene
51 24 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼51 UMethacrylonitrile
210 76 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼160 U QAcrolein
10 1.9 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 U M1,2,3-Trichloropropane
41 5.7 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼21 U QVinyl acetate
510 96 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼210 U QIsobutyl alcohol
10 10 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼10 U2-Nitropropane
130 130 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼130 Un-Butyl alcohol
5.1 2.1 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼4.1 UBromochloromethane
10 2.7 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼8.2 UDiethyl ether
21 6.4 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼19 U QTetrahydrofuran
10 10 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼10 UEthyl acetate
5.1 5.1 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 UBenzyl chloride
10 2.0 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 Un-Butylbenzene
10 2.6 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 U1,2,4-Trimethylbenzene
10 2.4 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 U2-Chlorotoluene
5.1 5.1 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 Un-Butyl acetate
10 3.2 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼8.2 U1,2-Dichloroethene, Total
5.1 2.1 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼4.1 U1,1-Dichloropropene
5.1 5.1 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 U2-Methylnaphthalene
10 2.4 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 Uo-Xylene
5.1 1.7 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼4.1 UHexane
10 2.2 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 U4-Chlorotoluene
5.1 2.2 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 U Q1-Chlorohexane
5.1 1.7 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼4.1 UBromobenzene
5.1 2.1 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼4.1 U1,2,3-Trichlorobenzene
21 4.8 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼10 U1,3-Dichloropropene, Total
10 2.1 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 Usec-Butylbenzene
10 2.3 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 U2,2-Dichloropropane
10 2.3 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 UN-Propylbenzene
5.1 5.1 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 U1,3,5-Trichlorobenzene
10 1.5 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼10 UDiisopropyl ether
260 260 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼260 U QEthanol
51 51 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼51 UIsopropyl alcohol
21 2.7 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼10 Up-Cymene
5.1 5.1 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 U QTert-amyl methyl ether
10 2.5 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 U1,3,5-Trimethylbenzene
5.1 5.1 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 U1,2,3-Trimethylbenzene
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-6Client Sample ID: 149-SB-1-46-12-22
Matrix: SolidDate Collected: 12/13/22 14:35
Percent Solids: 90.2Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
5.1 U 10 2.3 ug/Kg ☼12/16/22 12:07 12/27/22 20:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
m-Xylene & p-Xylene
10 2.5 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼8.2 UDichlorofluoromethane
10 2.6 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 Utert-Butylbenzene
5.1 5.1 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 U QIsooctane
10 2.3 ug/Kg 12/16/22 12:07 12/27/22 20:05 1☼5.1 U1,3-Dichloropropane
4-Bromofluorobenzene (Surr)91 79-119 12/16/22 12:07 12/27/22 20:05 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)107 12/16/22 12:07 12/27/22 20:05 178-119
1,2-Dichloroethane-d4 (Surr)100 12/16/22 12:07 12/27/22 20:05 171-138
Toluene-d8 (Surr)107 12/16/22 12:07 12/27/22 20:05 185-116
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
LOQ DL
360 U 1800 120 ug/Kg ☼12/16/22 15:30 12/20/22 13:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
360 33 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U1,2,4,5-Tetrachlorobenzene
360 33 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U1,2,4-Trichlorobenzene
360 40 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U1,2-Dichlorobenzene
360 37 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U1,2-Diphenylhydrazine
360 37 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U1,3-Dichlorobenzene
360 38 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U1,4-Dichlorobenzene
360 33 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U1-Methylnaphthalene
360 24 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼90 U2,3,4,6-Tetrachlorophenol
360 38 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U2,4,5-Trichlorophenol
360 31 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U2,4,6-Trichlorophenol
360 38 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U2,4-Dichlorophenol
360 48 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U2,4-Dimethylphenol
1800 900 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼1400 U2,4-Dinitrophenol
360 53 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼90 U2,4-Dinitrotoluene
360 29 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U2,6-Dichlorophenol
360 45 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U M2,6-Dinitrotoluene
360 38 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U2-Chloronaphthalene
360 43 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U2-Chlorophenol
360 41 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U2-Methylnaphthalene
360 29 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U2-Methylphenol
1800 49 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼180 U2-Nitroaniline
360 44 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U2-Nitrophenol
360 46 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U3 & 4 Methylphenol
710 30 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U3,3'-Dichlorobenzidine
1800 50 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼90 U3-Nitroaniline
1800 180 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼360 U4,6-Dinitro-2-methylphenol
360 39 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U4-Bromophenyl phenyl ether
360 38 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U4-Chloro-3-methylphenol
710 56 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼90 U4-Chloroaniline
360 48 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U4-Chlorophenyl phenyl ether
1800 53 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼90 U M Q4-Nitroaniline
1800 360 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼720 U4-Nitrophenol
360 44 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UAcenaphthene
360 39 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UAcenaphthylene
360 30 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UAcetophenone
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-6Client Sample ID: 149-SB-1-46-12-22
Matrix: SolidDate Collected: 12/13/22 14:35
Percent Solids: 90.2Date Received: 12/15/22 09:00
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
72 U 360 27 ug/Kg ☼12/16/22 15:30 12/20/22 13:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Anthracene
360 25 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UAtrazine
360 52 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼360 UAzobenzene
360 63 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼180 U QBenzaldehyde
360 29 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UBenzo[a]anthracene
360 56 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼90 UBenzo[a]pyrene
360 41 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UBenzo[b]fluoranthene
360 24 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UBenzo[g,h,i]perylene
360 70 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼180 UBenzo[k]fluoranthene
360 36 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UBenzyl alcohol
360 32 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 Ubis (2-chloroisopropyl) ether
360 42 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UBis(2-chloroethoxy)methane
360 49 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼90 UBis(2-chloroethyl)ether
360 31 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UBis(2-ethylhexyl) phthalate
360 28 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UButyl benzyl phthalate
360 71 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼180 U QCaprolactam
360 32 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UCarbazole
360 23 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UChrysene
360 42 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UDibenz(a,h)anthracene
360 36 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UDibenzofuran
360 40 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UDiethyl phthalate
360 37 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U MDimethyl phthalate
360 32 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UDi-n-butyl phthalate
360 31 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UDi-n-octyl phthalate
360 44 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼150 U MDiphenylamine
360 35 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UFluoranthene
360 39 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UFluorene
360 42 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U QHexachlorobenzene
360 39 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UHexachlorobutadiene
360 44 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UHexachlorocyclopentadiene
360 30 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UHexachloroethane
360 30 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 U QIndeno[1,2,3-cd]pyrene
360 36 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UIsophorone
360 32 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UNaphthalene
360 28 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UNitrobenzene
360 35 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UN-Nitrosodi-n-propylamine
360 36 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UN-Nitrosodiphenylamine
1800 360 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼720 UPentachlorophenol
360 29 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UPhenanthrene
360 37 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UPhenol
360 29 ug/Kg 12/16/22 15:30 12/20/22 13:53 1☼72 UPyrene
2-Fluorobiphenyl (Surr)67 44-115 12/16/22 15:30 12/20/22 13:53 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)60 12/16/22 15:30 12/20/22 13:53 135-115
Nitrobenzene-d5 (Surr)62 12/16/22 15:30 12/20/22 13:53 137-122
Phenol-d5 (Surr)61 12/16/22 15:30 12/20/22 13:53 133-122
Terphenyl-d14 (Surr)74 12/16/22 15:30 12/20/22 13:53 154-127
2,4,6-Tribromophenol (Surr)55 Q 12/16/22 15:30 12/20/22 13:53 139-132
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-6Client Sample ID: 149-SB-1-46-12-22
Matrix: SolidDate Collected: 12/13/22 14:35
Percent Solids: 90.2Date Received: 12/15/22 09:00
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
2.8 U 5.5 1.4 mg/Kg ☼01/18/23 06:31 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
0.089 U 0.11 0.044 mg/Kg ☼12/18/22 16:07 01/10/23 21:19 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Benzene
5.5 1.4 mg/Kg 12/18/22 16:07 01/10/23 21:19 50☼2.8 UC5-C8 Aliphatics
5.5 1.4 mg/Kg 12/18/22 16:07 01/10/23 21:19 50☼2.8 UC9-C10 Aromatics
5.5 1.4 mg/Kg 12/18/22 16:07 01/10/23 21:19 50☼2.8 UC9-C12 Aliphatics
0.11 0.044 mg/Kg 12/18/22 16:07 01/10/23 21:19 50☼0.089 UEthylbenzene
0.11 0.044 mg/Kg 12/18/22 16:07 01/10/23 21:19 50☼0.089 UMethyl tert-butyl ether
0.33 0.11 mg/Kg 12/18/22 16:07 01/10/23 21:19 50☼0.22 UNaphthalene
0.11 0.044 mg/Kg 12/18/22 16:07 01/10/23 21:19 50☼0.089 UToluene
5.5 1.4 mg/Kg 12/18/22 16:07 01/10/23 21:19 50☼2.8 UC9-C12 Aliphatics (adjusted)
0.28 0.11 mg/Kg 12/18/22 16:07 01/10/23 21:19 50☼0.22 Um-Xylene & p-Xylene
0.11 0.044 mg/Kg 12/18/22 16:07 01/10/23 21:19 50☼0.089 Uo-Xylene
5.5 1.4 mg/Kg 12/18/22 16:07 01/10/23 21:19 50☼2.8 UC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)86 70-130 12/18/22 16:07 01/10/23 21:19 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)86 12/18/22 16:07 01/10/23 21:19 5070-130
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
LOQ DL
0.43 U 0.54 0.22 mg/Kg ☼12/22/22 15:40 12/31/22 05:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acenaphthene
0.54 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:48 1☼0.43 UAcenaphthylene
0.54 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:48 1☼0.43 UAnthracene
0.54 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:48 1☼0.43 UBenzo[a]anthracene
0.54 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:48 1☼0.43 UBenzo[a]pyrene
0.54 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:48 1☼0.43 UBenzo[b]fluoranthene
0.54 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:48 1☼0.43 UBenzo[g,h,i]perylene
0.54 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:48 1☼0.43 UBenzo[k]fluoranthene
13 2.1 mg/Kg 12/22/22 15:40 12/31/22 05:26 1☼4.1 UC19-C36 Aliphatics
6.5 1.6 mg/Kg 12/22/22 15:40 12/31/22 05:26 1☼1.9 JC9-C18 Aliphatics
13 4.6 mg/Kg 12/22/22 15:40 12/31/22 05:48 1☼9.1 U MC11-C22 Aromatics
13 4.6 mg/Kg 12/22/22 15:40 12/31/22 05:48 1☼9.1 UC11-C22 Aromatics (Adjusted)
0.54 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:48 1☼0.43 UChrysene
0.54 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:48 1☼0.43 UDibenz(a,h)anthracene
0.54 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:48 1☼0.43 UFluoranthene
0.54 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:48 1☼0.43 UFluorene
0.54 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:48 1☼0.43 UIndeno[1,2,3-cd]pyrene
0.54 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:48 1☼0.43 U2-Methylnaphthalene
0.54 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:48 1☼0.43 U MNaphthalene
0.54 0.22 mg/Kg 12/22/22 15:40 12/31/22 05:48 1☼0.43 UPhenanthrene
2.2 0.76 mg/Kg 12/22/22 15:40 12/31/22 05:48 1☼1.7 UPyrene
1-Chlorooctadecane (Surr)58 40-140 12/22/22 15:40 12/31/22 05:26 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)76 12/22/22 15:40 12/31/22 05:48 140-140
o- terphenyl (Surr)63 12/22/22 15:40 12/31/22 05:48 140-140
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-6Client Sample ID: 149-SB-1-46-12-22
Matrix: SolidDate Collected: 12/13/22 14:35
Percent Solids: 90.2Date Received: 12/15/22 09:00
Method: SW846 7199 - Chromium, Hexavalent (IC)
LOQ DL
620 M 440 150 ug/Kg ☼01/12/23 10:42 01/12/23 20:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Chromium (hexavalent)
440 150 ug/Kg 01/12/23 10:42 01/12/23 20:41 1☼640 MChromium (hexavalent)
Method: SW846 6020B - Metals (ICP/MS)
LOQ DL
1800000 10000 2200 ug/Kg ☼12/15/22 13:26 12/16/22 16:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Aluminum
1000 100 ug/Kg 12/15/22 13:26 12/16/22 16:13 1☼310 UAntimony
520 100 ug/Kg 12/15/22 13:26 12/16/22 16:13 1☼110 JArsenic
520 62 ug/Kg 12/15/22 13:26 12/16/22 16:13 1☼900Barium
52 16 ug/Kg 12/15/22 13:26 12/16/22 16:13 1☼46 JBeryllium
52 16 ug/Kg 12/15/22 13:26 12/16/22 16:13 1☼41 UCadmium
52000 6500 ug/Kg 12/15/22 13:26 12/16/22 16:13 1☼39000 JCalcium
1000 110 ug/Kg 12/15/22 13:26 12/16/22 16:13 1☼1300Chromium
52 10 ug/Kg 12/15/22 13:26 12/16/22 16:13 1☼91Cobalt
520 130 ug/Kg 12/15/22 13:26 12/16/22 16:13 1☼1000Copper
26000 3600 ug/Kg 12/15/22 13:26 12/16/22 16:13 1☼590000Iron
210 52 ug/Kg 12/15/22 13:26 12/16/22 16:13 1☼1700Lead
26000 3400 ug/Kg 12/15/22 13:26 12/16/22 16:13 1☼4600 JMagnesium
1000 120 ug/Kg 12/15/22 13:26 12/16/22 16:13 1☼960 JManganese
1000 270 ug/Kg 12/15/22 13:26 12/16/22 16:13 1☼780 UNickel
26000 9400 ug/Kg 12/15/22 13:26 12/16/22 16:13 1☼22000 JPotassium
520 100 ug/Kg 12/15/22 13:26 12/16/22 16:13 1☼310 USelenium
100 10 ug/Kg 12/15/22 13:26 12/16/22 16:13 1☼31 USilver
41000 10000 ug/Kg 12/15/22 13:26 12/16/22 16:13 1☼26000 USodium
100 52 ug/Kg 12/15/22 13:26 12/16/22 16:13 1☼100 UThallium
2100 280 ug/Kg 12/15/22 13:26 12/16/22 16:13 1☼2900Vanadium
2600 1000 ug/Kg 12/15/22 13:26 12/16/22 16:13 1☼2100 UZinc
Lab Sample ID: 680-227663-7Client Sample ID: FB-12-22
Matrix: WaterDate Collected: 12/14/22 15:00
Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS)
LOQ DL
10 U Q 25 3.7 ug/L 12/28/22 12:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acetone
2.0 0.27 ug/L 12/28/22 12:28 11.0 U MBenzene
2.5 0.59 ug/L 12/28/22 12:28 12.0 U QBromoform
20 3.7 ug/L 12/28/22 12:28 110UBromomethane
25 6.4 ug/L 12/28/22 12:28 120U Q2-Butanone (MEK)
2.0 0.43 ug/L 12/28/22 12:28 11.0 U QCarbon disulfide
2.0 0.30 ug/L 12/28/22 12:28 11.0 UCarbon tetrachloride
1.0 0.15 ug/L 12/28/22 12:28 10.50 UChlorobenzene
2.0 0.39 ug/L 12/28/22 12:28 11.0 UChlorodibromomethane
20 4.6 ug/L 12/28/22 12:28 110U QChloroethane
2.0 0.27 ug/L 12/28/22 12:28 11.0 UChloroform
2.5 0.54 ug/L 12/28/22 12:28 12.0 UChloromethane
2.0 0.25 ug/L 12/28/22 12:28 11.0 Ucis-1,2-Dichloroethene
2.0 0.26 ug/L 12/28/22 12:28 11.0 Ucis-1,3-Dichloropropene
2.0 0.28 ug/L 12/28/22 12:28 11.0 UCyclohexane
10 1.8 ug/L 12/28/22 12:28 15.0 U Q1,2-Dibromo-3-Chloropropane
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-7Client Sample ID: FB-12-22
Matrix: WaterDate Collected: 12/14/22 15:00
Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
1.0 U 2.0 0.33 ug/L 12/28/22 12:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dibromoethane (EDB)
2.0 0.31 ug/L 12/28/22 12:28 11.0 U1,2-Dichlorobenzene
2.0 0.31 ug/L 12/28/22 12:28 11.0 U1,3-Dichlorobenzene
2.0 0.31 ug/L 12/28/22 12:28 11.0 U1,4-Dichlorobenzene
2.0 0.25 ug/L 12/28/22 12:28 11.0 UDichlorobromomethane
2.0 0.36 ug/L 12/28/22 12:28 11.0 U QDichlorodifluoromethane
2.0 0.33 ug/L 12/28/22 12:28 11.0 U1,1-Dichloroethane
2.0 0.25 ug/L 12/28/22 12:28 11.0 U M1,2-Dichloroethane
2.0 0.33 ug/L 12/28/22 12:28 11.0 U1,1-Dichloroethene
1.0 0.22 ug/L 12/28/22 12:28 10.50 U1,2-Dichloropropane
1.0 0.20 ug/L 12/28/22 12:28 10.50 UEthylbenzene
20 3.2 ug/L 12/28/22 12:28 110U2-Hexanone
2.0 0.26 ug/L 12/28/22 12:28 11.0 UIsopropylbenzene
20 3.2 ug/L 12/28/22 12:28 110U QMethyl acetate
2.0 0.33 ug/L 12/28/22 12:28 11.0 UMethylcyclohexane
20 3.2 ug/L 12/28/22 12:28 110UMethylene Chloride
20 2.7 ug/L 12/28/22 12:28 110U Q4-Methyl-2-pentanone (MIBK)
5.0 0.81 ug/L 12/28/22 12:28 12.0 U QMethyl tert-butyl ether
2.0 0.27 ug/L 12/28/22 12:28 11.0 UStyrene
2.0 0.40 ug/L 12/28/22 12:28 11.0 U1,1,2,2-Tetrachloroethane
2.0 0.35 ug/L 12/28/22 12:28 11.0 UTetrachloroethene
2.0 0.25 ug/L 12/28/22 12:28 11.0 UToluene
2.0 0.34 ug/L 12/28/22 12:28 11.0 Utrans-1,2-Dichloroethene
2.0 0.23 ug/L 12/28/22 12:28 11.0 Utrans-1,3-Dichloropropene
5.0 0.53 ug/L 12/28/22 12:28 12.0 U M1,2,4-Trichlorobenzene
1.0 0.21 ug/L 12/28/22 12:28 10.50 U1,1,1-Trichloroethane
2.0 0.32 ug/L 12/28/22 12:28 11.0 U1,1,2-Trichloroethane
1.0 0.20 ug/L 12/28/22 12:28 10.50 UTrichloroethene
2.0 0.33 ug/L 12/28/22 12:28 11.0 UTrichlorofluoromethane
1.0 0.23 ug/L 12/28/22 12:28 10.50 U1,1,2-Trichloro-1,2,2-trifluoroethane
2.0 0.40 ug/L 12/28/22 12:28 11.0 UVinyl chloride
2.0 0.49 ug/L 12/28/22 12:28 11.0 UXylenes, Total
20 5.0 ug/L 12/28/22 12:28 110U QPropionitrile
5.0 0.50 ug/L 12/28/22 12:28 11.0 U QPentachloroethane
2.5 0.78 ug/L 12/28/22 12:28 12.0 U QMethyl methacrylate
5.0 0.22 ug/L 12/28/22 12:28 11.0 UHexachlorobutadiene
2.0 0.34 ug/L 12/28/22 12:28 11.0 UDibromomethane
50 20 ug/L 12/28/22 12:28 140UAcetonitrile
10 2.4 ug/L 12/28/22 12:28 15.0 U QNaphthalene
20 3.9 ug/L 12/28/22 12:28 110U QIodomethane
5.0 1.1 ug/L 12/28/22 12:28 14.0 U3-Chloro-1-propene
50 5.5 ug/L 12/28/22 12:28 120UAcrylonitrile
2.0 0.33 ug/L 12/28/22 12:28 11.0 UEthyl methacrylate
2.0 0.36 ug/L 12/28/22 12:28 11.0 U1,1,1,2-Tetrachloroethane
10 1.3 ug/L 12/28/22 12:28 15.0 Utrans-1,4-Dichloro-2-butene
2.5 0.71 ug/L 12/28/22 12:28 12.0 U2-Chloro-1,3-butadiene
20 5.0 ug/L 12/28/22 12:28 110U QMethacrylonitrile
50 15 ug/L 12/28/22 12:28 140UAcrolein
2.0 0.48 ug/L 12/28/22 12:28 11.0 U1,2,3-Trichloropropane
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-7Client Sample ID: FB-12-22
Matrix: WaterDate Collected: 12/14/22 15:00
Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
2.0 U Q 2.5 0.69 ug/L 12/28/22 12:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Vinyl acetate
500 68 ug/L 12/28/22 12:28 1250U QIsobutyl alcohol
4.0 0.86 ug/L 12/28/22 12:28 12.0 U Q2-Nitropropane
100 25 ug/L 12/28/22 12:28 150U Qn-Butyl alcohol
2.0 0.34 ug/L 12/28/22 12:28 11.0 UBromochloromethane
5.0 0.37 ug/L 12/28/22 12:28 11.0 UDiethyl ether
10 2.1 ug/L 12/28/22 12:28 15.0 U QTetrahydrofuran
20 5.0 ug/L 12/28/22 12:28 110U QEthyl acetate
10 2.5 ug/L 12/28/22 12:28 15.0 U QBenzyl chloride
2.5 0.52 ug/L 12/28/22 12:28 12.0 Un-Butylbenzene
2.0 0.43 ug/L 12/28/22 12:28 11.0 U1,2,4-Trimethylbenzene
1.0 0.25 ug/L 12/28/22 12:28 10.50 U2-Chlorotoluene
5.0 0.50 ug/L 12/28/22 12:28 11.0 U Qn-Butyl acetate
2.0 0.37 ug/L 12/28/22 12:28 11.0 U1,2-Dichloroethene, Total
2.0 0.28 ug/L 12/28/22 12:28 11.0 U1,1-Dichloropropene
10 2.5 ug/L 12/28/22 12:28 15.0 U Q2-Methylnaphthalene
2.0 0.26 ug/L 12/28/22 12:28 11.0 Uo-Xylene
5.0 0.65 ug/L 12/28/22 12:28 12.0 UHexane
2.0 0.41 ug/L 12/28/22 12:28 11.0 U4-Chlorotoluene
5.0 1.1 ug/L 12/28/22 12:28 14.0 U M1-Chlorohexane
1.0 0.24 ug/L 12/28/22 12:28 10.50 UBromobenzene
5.0 0.81 ug/L 12/28/22 12:28 12.0 U Q1,2,3-Trichlorobenzene
2.0 0.48 ug/L 12/28/22 12:28 11.0 U1,3-Dichloropropene, Total
2.5 0.53 ug/L 12/28/22 12:28 12.0 Usec-Butylbenzene
2.0 0.35 ug/L 12/28/22 12:28 11.0 U2,2-Dichloropropane
2.0 0.41 ug/L 12/28/22 12:28 11.0 UN-Propylbenzene
10 2.5 ug/L 12/28/22 12:28 15.0 U1,3,5-Trichlorobenzene
10 0.70 ug/L 12/28/22 12:28 12.0 UDiisopropyl ether
200 50 ug/L 12/28/22 12:28 1100U QEthanol
100 25 ug/L 12/28/22 12:28 150U QIsopropyl alcohol
2.0 0.44 ug/L 12/28/22 12:28 11.0 Up-Cymene
2.5 0.78 ug/L 12/28/22 12:28 12.0 U QTert-amyl methyl ether
2.0 0.28 ug/L 12/28/22 12:28 11.0 U1,3,5-Trimethylbenzene
10 2.5 ug/L 12/28/22 12:28 15.0 U1,2,3-Trimethylbenzene
2.0 0.49 ug/L 12/28/22 12:28 11.0 Um-Xylene & p-Xylene
2.0 0.50 ug/L 12/28/22 12:28 11.0 U QDichlorofluoromethane
2.0 0.43 ug/L 12/28/22 12:28 11.0 Utert-Butylbenzene
5.0 0.99 ug/L 12/28/22 12:28 12.0 UIsooctane
2.0 0.36 ug/L 12/28/22 12:28 11.0 U1,3-Dichloropropane
4-Bromofluorobenzene (Surr)101 85-114 12/28/22 12:28 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)106 12/28/22 12:28 180-119
1,2-Dichloroethane-d4 (Surr)86 12/28/22 12:28 181-118
Toluene-d8 (Surr)116 Q 12/28/22 12:28 189-112
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
LOQ DL
9.5 U 19 4.4 ug/L 12/20/22 11:44 12/23/22 20:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
19 4.3 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U1,2,4,5-Tetrachlorobenzene
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-7Client Sample ID: FB-12-22
Matrix: WaterDate Collected: 12/14/22 15:00
Date Received: 12/15/22 09:00
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
9.5 U 19 3.2 ug/L 12/20/22 11:44 12/23/22 20:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2,4-Trichlorobenzene
9.5 2.4 ug/L 12/20/22 11:44 12/23/22 20:33 14.8 U1,2-Dichlorobenzene
19 3.5 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U1,2-Diphenylhydrazine
19 2.8 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U1,3-Dichlorobenzene
19 3.1 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U1,4-Dichlorobenzene
19 4.5 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U1-Methylnaphthalene
19 4.1 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U2,3,4,6-Tetrachlorophenol
19 3.1 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U2,4,5-Trichlorophenol
19 2.1 ug/L 12/20/22 11:44 12/23/22 20:33 14.8 U2,4,6-Trichlorophenol
19 3.5 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U2,4-Dichlorophenol
19 2.9 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U2,4-Dimethylphenol
48 15 ug/L 12/20/22 11:44 12/23/22 20:33 138U2,4-Dinitrophenol
9.5 2.2 ug/L 12/20/22 11:44 12/23/22 20:33 14.8 U2,4-Dinitrotoluene
9.5 2.3 ug/L 12/20/22 11:44 12/23/22 20:33 14.8 U2,6-Dichlorophenol
19 2.7 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U2,6-Dinitrotoluene
19 4.6 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U2-Chloronaphthalene
19 3.0 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U2-Chlorophenol
19 4.4 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U2-Methylnaphthalene
9.5 1.7 ug/L 12/20/22 11:44 12/23/22 20:33 13.8 U2-Methylphenol
19 2.8 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U2-Nitroaniline
19 3.7 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U2-Nitrophenol
9.5 1.3 ug/L 12/20/22 11:44 12/23/22 20:33 13.8 U3 & 4 Methylphenol
48 9.5 ug/L 12/20/22 11:44 12/23/22 20:33 119U Q3,3'-Dichlorobenzidine
48 2.9 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U3-Nitroaniline
48 5.1 ug/L 12/20/22 11:44 12/23/22 20:33 119U4,6-Dinitro-2-methylphenol
19 4.5 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U M4-Bromophenyl phenyl ether
19 2.4 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U4-Chloro-3-methylphenol
9.5 0.95 ug/L 12/20/22 11:44 12/23/22 20:33 13.8 U M4-Chloroaniline
19 5.1 ug/L 12/20/22 11:44 12/23/22 20:33 111U4-Chlorophenyl phenyl ether
48 2.9 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U4-Nitroaniline
48 7.7 ug/L 12/20/22 11:44 12/23/22 20:33 119U4-Nitrophenol
19 4.2 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 UAcenaphthene
19 3.4 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 UAcenaphthylene
9.5 2.1 ug/L 12/20/22 11:44 12/23/22 20:33 14.8 UAcetophenone
19 3.4 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 UAnthracene
9.5 2.1 ug/L 12/20/22 11:44 12/23/22 20:33 14.8 UAtrazine
19 3.4 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U QAzobenzene
19 4.6 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U MBenzaldehyde
19 4.0 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 UBenzo[a]anthracene
19 2.7 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U MBenzo[a]pyrene
19 3.0 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 UBenzo[b]fluoranthene
19 2.9 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 UBenzo[g,h,i]perylene
19 2.8 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 UBenzo[k]fluoranthene
19 2.5 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 UBenzyl alcohol
19 3.0 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 Ubis (2-chloroisopropyl) ether
9.5 1.7 ug/L 12/20/22 11:44 12/23/22 20:33 13.8 UBis(2-chloroethoxy)methane
19 3.4 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 UBis(2-chloroethyl)ether
19 2.9 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 UBis(2-ethylhexyl) phthalate
19 2.7 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 UButyl benzyl phthalate
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-7Client Sample ID: FB-12-22
Matrix: WaterDate Collected: 12/14/22 15:00
Date Received: 12/15/22 09:00
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
9.5 U 19 2.7 ug/L 12/20/22 11:44 12/23/22 20:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Caprolactam
9.5 1.7 ug/L 12/20/22 11:44 12/23/22 20:33 13.8 UCarbazole
19 3.6 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 UChrysene
19 2.9 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 UDibenz(a,h)anthracene
9.5 1.8 ug/L 12/20/22 11:44 12/23/22 20:33 13.8 UDibenzofuran
9.5 2.1 ug/L 12/20/22 11:44 12/23/22 20:33 14.8 UDiethyl phthalate
9.5 2.0 ug/L 12/20/22 11:44 12/23/22 20:33 14.8 UDimethyl phthalate
9.5 2.2 ug/L 12/20/22 11:44 12/23/22 20:33 14.8 UDi-n-butyl phthalate
19 2.7 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U MDi-n-octyl phthalate
9.5 2.4 ug/L 12/20/22 11:44 12/23/22 20:33 18.1 UDiphenylamine
9.5 1.5 ug/L 12/20/22 11:44 12/23/22 20:33 13.8 UFluoranthene
19 3.2 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 UFluorene
9.5 1.5 ug/L 12/20/22 11:44 12/23/22 20:33 13.8 UHexachlorobenzene
19 3.8 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 UHexachlorobutadiene
19 3.3 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 UHexachlorocyclopentadiene
19 3.4 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 UHexachloroethane
19 4.1 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 UIndeno[1,2,3-cd]pyrene
9.5 1.9 ug/L 12/20/22 11:44 12/23/22 20:33 13.8 UIsophorone
19 3.3 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 UNaphthalene
19 3.3 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 UNitrobenzene
9.5 2.3 ug/L 12/20/22 11:44 12/23/22 20:33 14.8 UN-Nitrosodi-n-propylamine
19 2.8 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U MN-Nitrosodiphenylamine
48 9.4 ug/L 12/20/22 11:44 12/23/22 20:33 119UPentachlorophenol
19 4.1 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 UPhenanthrene
9.5 1.4 ug/L 12/20/22 11:44 12/23/22 20:33 13.8 U MPhenol
19 3.5 ug/L 12/20/22 11:44 12/23/22 20:33 19.5 U MPyrene
2-Fluorobiphenyl (Surr)59 44-119 12/20/22 11:44 12/23/22 20:33 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)27 12/20/22 11:44 12/23/22 20:33 119-119
Nitrobenzene-d5 (Surr)57 12/20/22 11:44 12/23/22 20:33 144-120
Phenol-d5 (Surr)18 12/20/22 11:44 12/23/22 20:33 110-130
Terphenyl-d14 (Surr)71 12/20/22 11:44 12/23/22 20:33 150-134
2,4,6-Tribromophenol (Surr)85 12/20/22 11:44 12/23/22 20:33 143-140
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
40 U 100 20 ug/L 01/18/23 06:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
2.0 U 5.0 1.0 ug/L 12/28/22 12:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Benzene
100 25 ug/L 12/28/22 12:30 150UC5-C8 Aliphatics
100 10 ug/L 12/28/22 12:30 120UC9-C10 Aromatics
100 25 ug/L 12/28/22 12:30 150UC9-C12 Aliphatics
5.0 1.0 ug/L 12/28/22 12:30 12.0 UEthylbenzene
5.0 1.0 ug/L 12/28/22 12:30 12.0 U QMethyl tert-butyl ether
6.0 2.0 ug/L 12/28/22 12:30 14.0 UNaphthalene
5.0 1.0 ug/L 12/28/22 12:30 12.0 UToluene
100 25 ug/L 12/28/22 12:30 150UC9-C12 Aliphatics (adjusted)
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-7Client Sample ID: FB-12-22
Matrix: WaterDate Collected: 12/14/22 15:00
Date Received: 12/15/22 09:00
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
LOQ DL
5.0 U 10 2.5 ug/L 12/28/22 12:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
m-Xylene & p-Xylene
5.0 1.0 ug/L 12/28/22 12:30 12.0 Uo-Xylene
100 25 ug/L 12/28/22 12:30 150UC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)103 70-130 12/28/22 12:30 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)92 12/28/22 12:30 170-130
Method: SW846 8081B 8082A - Organochlorine Pesticides & PCBs (GC)
LOQ DL
0.0039 U 0.049 0.0020 ug/L 12/21/22 13:43 12/22/22 18:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,4'-DDD
0.049 0.00099 ug/L 12/21/22 13:43 12/22/22 18:27 10.0039 U4,4'-DDE
0.049 0.00099 ug/L 12/21/22 13:43 12/22/22 18:27 10.0039 U Q4,4'-DDT
0.049 0.0020 ug/L 12/21/22 13:43 12/22/22 18:27 10.0039 U MAldrin
0.049 0.00099 ug/L 12/21/22 13:43 12/22/22 18:27 10.0039 Ualpha-BHC
0.049 0.0020 ug/L 12/21/22 13:43 12/22/22 18:27 10.0039 Ubeta-BHC
0.049 0.0020 ug/L 12/21/22 13:43 12/22/22 18:27 10.0039 Udelta-BHC
0.049 0.0020 ug/L 12/21/22 13:43 12/22/22 18:27 10.0039 U MDieldrin
0.049 0.0020 ug/L 12/21/22 13:43 12/22/22 18:27 10.0039 U MEndosulfan I
0.049 0.0020 ug/L 12/21/22 13:43 12/22/22 18:27 10.0039 UEndosulfan II
0.049 0.0020 ug/L 12/21/22 13:43 12/22/22 18:27 10.0039 UEndosulfan sulfate
0.049 0.00099 ug/L 12/21/22 13:43 12/22/22 18:27 10.0039 UEndrin
0.049 0.0039 ug/L 12/21/22 13:43 12/22/22 18:27 10.016 UEndrin aldehyde
0.049 0.0039 ug/L 12/21/22 13:43 12/22/22 18:27 10.016 U QEndrin ketone
0.049 0.00099 ug/L 12/21/22 13:43 12/22/22 18:27 10.0039 U Mgamma-BHC (Lindane)
0.049 0.00099 ug/L 12/21/22 13:43 12/22/22 18:27 10.0039 U MHeptachlor
0.049 0.0020 ug/L 12/21/22 13:43 12/22/22 18:27 10.0039 UHeptachlor epoxide
0.049 0.0020 ug/L 12/21/22 13:43 12/22/22 18:27 10.0039 U MMethoxychlor
0.49 0.16 ug/L 12/21/22 13:43 12/22/22 18:27 10.39 U M QChlordane (technical)
0.99 0.32 ug/L 12/21/22 13:43 12/22/22 18:27 10.71 UPCB-1016
0.99 0.34 ug/L 12/21/22 13:43 12/22/22 18:27 10.71 UPCB-1221
0.99 0.34 ug/L 12/21/22 13:43 12/22/22 18:27 10.71 UPCB-1232
0.99 0.34 ug/L 12/21/22 13:43 12/22/22 18:27 10.71 UPCB-1242
0.99 0.34 ug/L 12/21/22 13:43 12/22/22 18:27 10.71 UPCB-1248
0.99 0.34 ug/L 12/21/22 13:43 12/22/22 18:27 10.71 UPCB-1254
0.99 0.34 ug/L 12/21/22 13:43 12/22/22 18:27 10.71 UPCB-1260
4.9 0.31 ug/L 12/21/22 13:43 12/22/22 18:27 10.79 UToxaphene
DCB Decachlorobiphenyl 95 14-130 12/21/22 13:43 12/22/22 18:27 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene (Surr)63 12/21/22 13:43 12/22/22 18:27 144-124
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
LOQ DL
1.1 U 1.9 0.57 ug/L 12/19/22 18:32 12/22/22 23:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Anthracene
11 4.8 ug/L 12/19/22 18:32 12/22/22 23:49 19.5 UPyrene
1.9 0.57 ug/L 12/19/22 18:32 12/22/22 23:49 11.1 UBenzo[g,h,i]perylene
1.9 0.57 ug/L 12/19/22 18:32 12/22/22 23:49 11.1 UIndeno[1,2,3-cd]pyrene
1.9 0.57 ug/L 12/19/22 18:32 12/22/22 23:49 11.1 UBenzo[b]fluoranthene
1.9 0.48 ug/L 12/19/22 18:32 12/22/22 23:49 10.95 UFluoranthene
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-7Client Sample ID: FB-12-22
Matrix: WaterDate Collected: 12/14/22 15:00
Date Received: 12/15/22 09:00
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
LOQ DL
2.9 U 3.8 1.4 ug/L 12/19/22 18:32 12/22/22 23:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Benzo[k]fluoranthene
1.9 0.67 ug/L 12/19/22 18:32 12/22/22 23:49 11.3 UAcenaphthylene
1.9 0.48 ug/L 12/19/22 18:32 12/22/22 23:49 10.95 UChrysene
1.9 0.57 ug/L 12/19/22 18:32 12/22/22 23:49 11.1 UBenzo[a]pyrene
1.9 0.48 ug/L 12/19/22 18:32 12/22/22 23:49 10.95 UDibenz(a,h)anthracene
1.9 0.67 ug/L 12/19/22 18:32 12/22/22 23:49 11.3 UBenzo[a]anthracene
1.9 0.57 ug/L 12/19/22 18:32 12/22/22 23:49 11.1 UAcenaphthene
1.9 0.57 ug/L 12/19/22 18:32 12/22/22 23:49 11.1 UPhenanthrene
1.9 0.57 ug/L 12/19/22 18:32 12/22/22 23:49 11.1 UFluorene
1.9 0.57 ug/L 12/19/22 18:32 12/22/22 23:49 11.1 UNaphthalene
1.9 0.57 ug/L 12/19/22 18:32 12/22/22 23:49 11.1 U2-Methylnaphthalene
38 9.5 ug/L 12/19/22 18:32 12/22/22 23:49 129UC11-C22 Aromatics (unadjusted)
38 9.5 ug/L 12/19/22 18:32 12/22/22 23:49 129UC11-C22 Aromatics (Adjusted)
48 9.5 ug/L 12/19/22 18:32 12/22/22 23:49 119UC19-C36 Aliphatics
29 9.5 ug/L 12/19/22 18:32 12/22/22 23:49 110JC9-C18 Aliphatics
1-Chlorooctadecane (Surr)77 40-140 12/19/22 18:32 12/22/22 23:49 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)81 12/19/22 18:32 12/22/22 23:49 140-140
o- terphenyl (Surr)73 12/19/22 18:32 12/22/22 23:49 140-140
Method: SW846 7199 - Chromium, Hexavalent (IC) - Dissolved
LOQ DL
9.0 U H 10 5.0 ug/L 12/28/22 18:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Chromium (hexavalent)
10 5.0 ug/L 12/28/22 18:52 19.0 U HChromium (hexavalent)
Method: SW846 6020B - Metals (ICP/MS) - Total Recoverable
LOQ DL
1.0 U 2.0 0.39 ug/L 12/16/22 06:22 12/16/22 18:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Silver
200 35 ug/L 12/16/22 06:22 12/16/22 18:50 1100UAluminum
5.0 0.86 ug/L 12/16/22 06:22 12/16/22 18:50 13.0 UArsenic
5.0 0.89 ug/L 12/16/22 06:22 12/16/22 18:50 12.0 UBarium
0.50 0.20 ug/L 12/16/22 06:22 12/16/22 18:50 10.40 UBeryllium
500 140 ug/L 12/16/22 06:22 12/16/22 18:50 1300UCalcium
0.50 0.078 ug/L 12/16/22 06:22 12/16/22 18:50 10.20 UCadmium
1.0 0.22 ug/L 12/16/22 06:22 12/16/22 18:50 10.50 UCobalt
20 2.6 ug/L 12/16/22 06:22 12/16/22 18:50 110UChromium
5.0 0.90 ug/L 12/16/22 06:22 12/16/22 18:50 12.0 UCopper
100 26 ug/L 12/16/22 06:22 12/16/22 18:50 175UIron
1000 160 ug/L 12/16/22 06:22 12/16/22 18:50 1500UPotassium
250 23 ug/L 12/16/22 06:22 12/16/22 18:50 160UMagnesium
10 2.2 ug/L 12/16/22 06:22 12/16/22 18:50 15.0 UManganese
1000 200 ug/L 12/16/22 06:22 12/16/22 18:50 1500USodium
2.5 0.34 ug/L 12/16/22 06:22 12/16/22 18:50 11.0 ULead
5.0 1.2 ug/L 12/16/22 06:22 12/16/22 18:50 12.5 USelenium
10 1.8 ug/L 12/16/22 06:22 12/16/22 18:50 15.0 UNickel
5.0 0.52 ug/L 12/16/22 06:22 12/16/22 18:50 11.5 UAntimony
2.0 0.26 ug/L 12/16/22 06:22 12/16/22 18:50 11.0 UThallium
25 10 ug/L 12/16/22 06:22 12/16/22 18:50 120UZinc
10 1.8 ug/L 12/16/22 06:22 12/16/22 18:50 15.0 UVanadium
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-8Client Sample ID: EQB-12-22
Matrix: WaterDate Collected: 12/14/22 15:20
Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS)
LOQ DL
10 U Q 25 3.7 ug/L 12/28/22 12:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acetone
2.0 0.27 ug/L 12/28/22 12:47 11.0 U MBenzene
2.5 0.59 ug/L 12/28/22 12:47 12.0 U QBromoform
20 3.7 ug/L 12/28/22 12:47 110UBromomethane
25 6.4 ug/L 12/28/22 12:47 120U Q2-Butanone (MEK)
2.0 0.43 ug/L 12/28/22 12:47 11.0 U QCarbon disulfide
2.0 0.30 ug/L 12/28/22 12:47 11.0 UCarbon tetrachloride
1.0 0.15 ug/L 12/28/22 12:47 10.50 UChlorobenzene
2.0 0.39 ug/L 12/28/22 12:47 11.0 UChlorodibromomethane
20 4.6 ug/L 12/28/22 12:47 110U QChloroethane
2.0 0.27 ug/L 12/28/22 12:47 11.0 UChloroform
2.5 0.54 ug/L 12/28/22 12:47 12.0 UChloromethane
2.0 0.25 ug/L 12/28/22 12:47 11.0 Ucis-1,2-Dichloroethene
2.0 0.26 ug/L 12/28/22 12:47 11.0 Ucis-1,3-Dichloropropene
2.0 0.28 ug/L 12/28/22 12:47 11.0 UCyclohexane
10 1.8 ug/L 12/28/22 12:47 15.0 U Q1,2-Dibromo-3-Chloropropane
2.0 0.33 ug/L 12/28/22 12:47 11.0 U1,2-Dibromoethane (EDB)
2.0 0.31 ug/L 12/28/22 12:47 11.0 U1,2-Dichlorobenzene
2.0 0.31 ug/L 12/28/22 12:47 11.0 U1,3-Dichlorobenzene
2.0 0.31 ug/L 12/28/22 12:47 11.0 U1,4-Dichlorobenzene
2.0 0.25 ug/L 12/28/22 12:47 11.0 UDichlorobromomethane
2.0 0.36 ug/L 12/28/22 12:47 11.0 U QDichlorodifluoromethane
2.0 0.33 ug/L 12/28/22 12:47 11.0 U1,1-Dichloroethane
2.0 0.25 ug/L 12/28/22 12:47 11.0 U M1,2-Dichloroethane
2.0 0.33 ug/L 12/28/22 12:47 11.0 U1,1-Dichloroethene
1.0 0.22 ug/L 12/28/22 12:47 10.50 U1,2-Dichloropropane
1.0 0.20 ug/L 12/28/22 12:47 10.50 UEthylbenzene
20 3.2 ug/L 12/28/22 12:47 110U2-Hexanone
2.0 0.26 ug/L 12/28/22 12:47 11.0 UIsopropylbenzene
20 3.2 ug/L 12/28/22 12:47 110U QMethyl acetate
2.0 0.33 ug/L 12/28/22 12:47 11.0 UMethylcyclohexane
20 3.2 ug/L 12/28/22 12:47 110UMethylene Chloride
20 2.7 ug/L 12/28/22 12:47 110U Q4-Methyl-2-pentanone (MIBK)
5.0 0.81 ug/L 12/28/22 12:47 12.0 U QMethyl tert-butyl ether
2.0 0.27 ug/L 12/28/22 12:47 11.0 UStyrene
2.0 0.40 ug/L 12/28/22 12:47 11.0 U1,1,2,2-Tetrachloroethane
2.0 0.35 ug/L 12/28/22 12:47 11.0 UTetrachloroethene
2.0 0.25 ug/L 12/28/22 12:47 11.0 UToluene
2.0 0.34 ug/L 12/28/22 12:47 11.0 Utrans-1,2-Dichloroethene
2.0 0.23 ug/L 12/28/22 12:47 11.0 Utrans-1,3-Dichloropropene
5.0 0.53 ug/L 12/28/22 12:47 12.0 U M1,2,4-Trichlorobenzene
1.0 0.21 ug/L 12/28/22 12:47 10.50 U1,1,1-Trichloroethane
2.0 0.32 ug/L 12/28/22 12:47 11.0 U1,1,2-Trichloroethane
1.0 0.20 ug/L 12/28/22 12:47 10.50 UTrichloroethene
2.0 0.33 ug/L 12/28/22 12:47 11.0 UTrichlorofluoromethane
1.0 0.23 ug/L 12/28/22 12:47 10.50 U1,1,2-Trichloro-1,2,2-trifluoroethane
2.0 0.40 ug/L 12/28/22 12:47 11.0 UVinyl chloride
2.0 0.49 ug/L 12/28/22 12:47 11.0 UXylenes, Total
20 5.0 ug/L 12/28/22 12:47 110U QPropionitrile
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-8Client Sample ID: EQB-12-22
Matrix: WaterDate Collected: 12/14/22 15:20
Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
1.0 U Q 5.0 0.50 ug/L 12/28/22 12:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Pentachloroethane
2.5 0.78 ug/L 12/28/22 12:47 12.0 U QMethyl methacrylate
5.0 0.22 ug/L 12/28/22 12:47 11.0 UHexachlorobutadiene
2.0 0.34 ug/L 12/28/22 12:47 11.0 UDibromomethane
50 20 ug/L 12/28/22 12:47 140UAcetonitrile
10 2.4 ug/L 12/28/22 12:47 15.0 U QNaphthalene
20 3.9 ug/L 12/28/22 12:47 110U QIodomethane
5.0 1.1 ug/L 12/28/22 12:47 14.0 U3-Chloro-1-propene
50 5.5 ug/L 12/28/22 12:47 120UAcrylonitrile
2.0 0.33 ug/L 12/28/22 12:47 11.0 UEthyl methacrylate
2.0 0.36 ug/L 12/28/22 12:47 11.0 U1,1,1,2-Tetrachloroethane
10 1.3 ug/L 12/28/22 12:47 15.0 Utrans-1,4-Dichloro-2-butene
2.5 0.71 ug/L 12/28/22 12:47 12.0 U2-Chloro-1,3-butadiene
20 5.0 ug/L 12/28/22 12:47 110U QMethacrylonitrile
50 15 ug/L 12/28/22 12:47 140UAcrolein
2.0 0.48 ug/L 12/28/22 12:47 11.0 U1,2,3-Trichloropropane
2.5 0.69 ug/L 12/28/22 12:47 12.0 U QVinyl acetate
500 68 ug/L 12/28/22 12:47 1250U QIsobutyl alcohol
4.0 0.86 ug/L 12/28/22 12:47 12.0 U Q2-Nitropropane
100 25 ug/L 12/28/22 12:47 150U Qn-Butyl alcohol
2.0 0.34 ug/L 12/28/22 12:47 11.0 UBromochloromethane
5.0 0.37 ug/L 12/28/22 12:47 11.0 UDiethyl ether
10 2.1 ug/L 12/28/22 12:47 15.0 U QTetrahydrofuran
20 5.0 ug/L 12/28/22 12:47 110U QEthyl acetate
10 2.5 ug/L 12/28/22 12:47 15.0 U QBenzyl chloride
2.5 0.52 ug/L 12/28/22 12:47 12.0 Un-Butylbenzene
2.0 0.43 ug/L 12/28/22 12:47 11.0 U1,2,4-Trimethylbenzene
1.0 0.25 ug/L 12/28/22 12:47 10.50 U2-Chlorotoluene
5.0 0.50 ug/L 12/28/22 12:47 11.0 U Qn-Butyl acetate
2.0 0.37 ug/L 12/28/22 12:47 11.0 U1,2-Dichloroethene, Total
2.0 0.28 ug/L 12/28/22 12:47 11.0 U1,1-Dichloropropene
10 2.5 ug/L 12/28/22 12:47 15.0 U Q2-Methylnaphthalene
2.0 0.26 ug/L 12/28/22 12:47 11.0 Uo-Xylene
5.0 0.65 ug/L 12/28/22 12:47 12.0 UHexane
2.0 0.41 ug/L 12/28/22 12:47 11.0 U4-Chlorotoluene
5.0 1.1 ug/L 12/28/22 12:47 14.0 U M1-Chlorohexane
1.0 0.24 ug/L 12/28/22 12:47 10.50 UBromobenzene
5.0 0.81 ug/L 12/28/22 12:47 12.0 U Q1,2,3-Trichlorobenzene
2.0 0.48 ug/L 12/28/22 12:47 11.0 U1,3-Dichloropropene, Total
2.5 0.53 ug/L 12/28/22 12:47 12.0 Usec-Butylbenzene
2.0 0.35 ug/L 12/28/22 12:47 11.0 U2,2-Dichloropropane
2.0 0.41 ug/L 12/28/22 12:47 11.0 UN-Propylbenzene
10 2.5 ug/L 12/28/22 12:47 15.0 U1,3,5-Trichlorobenzene
10 0.70 ug/L 12/28/22 12:47 12.0 UDiisopropyl ether
200 50 ug/L 12/28/22 12:47 1100U QEthanol
100 25 ug/L 12/28/22 12:47 150U QIsopropyl alcohol
2.0 0.44 ug/L 12/28/22 12:47 11.0 Up-Cymene
2.5 0.78 ug/L 12/28/22 12:47 12.0 U QTert-amyl methyl ether
2.0 0.28 ug/L 12/28/22 12:47 11.0 U1,3,5-Trimethylbenzene
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-8Client Sample ID: EQB-12-22
Matrix: WaterDate Collected: 12/14/22 15:20
Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
5.0 U 10 2.5 ug/L 12/28/22 12:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2,3-Trimethylbenzene
2.0 0.49 ug/L 12/28/22 12:47 11.0 Um-Xylene & p-Xylene
2.0 0.50 ug/L 12/28/22 12:47 11.0 U QDichlorofluoromethane
2.0 0.43 ug/L 12/28/22 12:47 11.0 Utert-Butylbenzene
5.0 0.99 ug/L 12/28/22 12:47 12.0 UIsooctane
2.0 0.36 ug/L 12/28/22 12:47 11.0 U1,3-Dichloropropane
4-Bromofluorobenzene (Surr)102 85-114 12/28/22 12:47 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)101 12/28/22 12:47 180-119
1,2-Dichloroethane-d4 (Surr)84 12/28/22 12:47 181-118
Toluene-d8 (Surr)113 Q 12/28/22 12:47 189-112
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
LOQ DL
9.8 U 20 4.5 ug/L 12/20/22 11:44 12/23/22 20:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
20 4.4 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U1,2,4,5-Tetrachlorobenzene
20 3.3 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U1,2,4-Trichlorobenzene
9.8 2.5 ug/L 12/20/22 11:44 12/23/22 20:58 14.9 U1,2-Dichlorobenzene
20 3.6 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U1,2-Diphenylhydrazine
20 2.9 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U1,3-Dichlorobenzene
20 3.2 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U1,4-Dichlorobenzene
20 4.6 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U1-Methylnaphthalene
20 4.2 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U2,3,4,6-Tetrachlorophenol
20 3.2 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U2,4,5-Trichlorophenol
20 2.2 ug/L 12/20/22 11:44 12/23/22 20:58 14.9 U2,4,6-Trichlorophenol
20 3.6 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U2,4-Dichlorophenol
20 3.0 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U2,4-Dimethylphenol
49 16 ug/L 12/20/22 11:44 12/23/22 20:58 139U2,4-Dinitrophenol
9.8 2.3 ug/L 12/20/22 11:44 12/23/22 20:58 14.9 U2,4-Dinitrotoluene
9.8 2.4 ug/L 12/20/22 11:44 12/23/22 20:58 14.9 U2,6-Dichlorophenol
20 2.8 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U2,6-Dinitrotoluene
20 4.7 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U2-Chloronaphthalene
20 3.2 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U2-Chlorophenol
20 4.5 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U2-Methylnaphthalene
9.8 1.8 ug/L 12/20/22 11:44 12/23/22 20:58 13.9 U2-Methylphenol
20 2.9 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U M2-Nitroaniline
20 3.8 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U2-Nitrophenol
9.8 1.4 ug/L 12/20/22 11:44 12/23/22 20:58 13.9 U3 & 4 Methylphenol
49 9.8 ug/L 12/20/22 11:44 12/23/22 20:58 120U Q3,3'-Dichlorobenzidine
49 3.0 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U3-Nitroaniline
49 5.2 ug/L 12/20/22 11:44 12/23/22 20:58 120U4,6-Dinitro-2-methylphenol
20 4.6 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U M4-Bromophenyl phenyl ether
20 2.5 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U4-Chloro-3-methylphenol
9.8 0.98 ug/L 12/20/22 11:44 12/23/22 20:58 13.9 U4-Chloroaniline
20 5.2 ug/L 12/20/22 11:44 12/23/22 20:58 112U4-Chlorophenyl phenyl ether
49 3.0 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U4-Nitroaniline
49 8.0 ug/L 12/20/22 11:44 12/23/22 20:58 120U4-Nitrophenol
20 4.3 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 UAcenaphthene
20 3.5 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 UAcenaphthylene
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-8Client Sample ID: EQB-12-22
Matrix: WaterDate Collected: 12/14/22 15:20
Date Received: 12/15/22 09:00
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
4.9 U 9.8 2.2 ug/L 12/20/22 11:44 12/23/22 20:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acetophenone
20 3.5 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 UAnthracene
9.8 2.2 ug/L 12/20/22 11:44 12/23/22 20:58 14.9 UAtrazine
20 3.5 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U QAzobenzene
20 4.7 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U MBenzaldehyde
20 4.1 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 UBenzo[a]anthracene
20 2.8 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U MBenzo[a]pyrene
20 3.1 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U MBenzo[b]fluoranthene
20 3.0 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 UBenzo[g,h,i]perylene
20 2.9 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 UBenzo[k]fluoranthene
20 2.6 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U MBenzyl alcohol
20 3.1 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U Mbis (2-chloroisopropyl) ether
9.8 1.8 ug/L 12/20/22 11:44 12/23/22 20:58 13.9 UBis(2-chloroethoxy)methane
20 3.5 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U MBis(2-chloroethyl)ether
20 3.0 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 UBis(2-ethylhexyl) phthalate
20 2.8 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 UButyl benzyl phthalate
20 2.8 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 UCaprolactam
9.8 1.8 ug/L 12/20/22 11:44 12/23/22 20:58 13.9 UCarbazole
20 3.7 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 UChrysene
20 3.0 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 UDibenz(a,h)anthracene
9.8 1.9 ug/L 12/20/22 11:44 12/23/22 20:58 13.9 UDibenzofuran
9.8 2.2 ug/L 12/20/22 11:44 12/23/22 20:58 14.9 UDiethyl phthalate
9.8 2.1 ug/L 12/20/22 11:44 12/23/22 20:58 14.9 UDimethyl phthalate
9.8 2.3 ug/L 12/20/22 11:44 12/23/22 20:58 14.9 UDi-n-butyl phthalate
20 2.8 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U MDi-n-octyl phthalate
9.8 2.5 ug/L 12/20/22 11:44 12/23/22 20:58 18.4 UDiphenylamine
9.8 1.6 ug/L 12/20/22 11:44 12/23/22 20:58 13.9 UFluoranthene
20 3.3 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U MFluorene
9.8 1.6 ug/L 12/20/22 11:44 12/23/22 20:58 13.9 UHexachlorobenzene
20 3.9 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 UHexachlorobutadiene
20 3.4 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 UHexachlorocyclopentadiene
20 3.5 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 UHexachloroethane
20 4.2 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 UIndeno[1,2,3-cd]pyrene
9.8 2.0 ug/L 12/20/22 11:44 12/23/22 20:58 13.9 UIsophorone
20 3.4 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 UNaphthalene
20 3.4 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U MNitrobenzene
9.8 2.4 ug/L 12/20/22 11:44 12/23/22 20:58 14.9 U MN-Nitrosodi-n-propylamine
20 2.9 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U MN-Nitrosodiphenylamine
49 9.7 ug/L 12/20/22 11:44 12/23/22 20:58 120UPentachlorophenol
20 4.2 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 UPhenanthrene
9.8 1.5 ug/L 12/20/22 11:44 12/23/22 20:58 13.9 UPhenol
20 3.6 ug/L 12/20/22 11:44 12/23/22 20:58 19.8 U MPyrene
2-Fluorobiphenyl (Surr)68 44-119 12/20/22 11:44 12/23/22 20:58 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)29 12/20/22 11:44 12/23/22 20:58 119-119
Nitrobenzene-d5 (Surr)60 12/20/22 11:44 12/23/22 20:58 144-120
Phenol-d5 (Surr)19 12/20/22 11:44 12/23/22 20:58 110-130
Terphenyl-d14 (Surr)79 12/20/22 11:44 12/23/22 20:58 150-134
2,4,6-Tribromophenol (Surr)89 12/20/22 11:44 12/23/22 20:58 143-140
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-8Client Sample ID: EQB-12-22
Matrix: WaterDate Collected: 12/14/22 15:20
Date Received: 12/15/22 09:00
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
40 U 100 20 ug/L 01/18/23 06:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
2.0 U 5.0 1.0 ug/L 12/28/22 13:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Benzene
100 25 ug/L 12/28/22 13:11 150UC5-C8 Aliphatics
100 10 ug/L 12/28/22 13:11 120UC9-C10 Aromatics
100 25 ug/L 12/28/22 13:11 150UC9-C12 Aliphatics
5.0 1.0 ug/L 12/28/22 13:11 12.0 UEthylbenzene
5.0 1.0 ug/L 12/28/22 13:11 12.0 U QMethyl tert-butyl ether
6.0 2.0 ug/L 12/28/22 13:11 14.0 UNaphthalene
5.0 1.0 ug/L 12/28/22 13:11 12.0 UToluene
100 25 ug/L 12/28/22 13:11 150UC9-C12 Aliphatics (adjusted)
10 2.5 ug/L 12/28/22 13:11 15.0 Um-Xylene & p-Xylene
5.0 1.0 ug/L 12/28/22 13:11 12.0 Uo-Xylene
100 25 ug/L 12/28/22 13:11 150UC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)104 70-130 12/28/22 13:11 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)93 12/28/22 13:11 170-130
Method: SW846 8081B 8082A - Organochlorine Pesticides & PCBs (GC)
LOQ DL
0.0038 U 0.048 0.0019 ug/L 12/21/22 13:43 12/22/22 18:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,4'-DDD
0.048 0.00095 ug/L 12/21/22 13:43 12/22/22 18:41 10.0038 U4,4'-DDE
0.048 0.00095 ug/L 12/21/22 13:43 12/22/22 18:41 10.0038 U Q4,4'-DDT
0.048 0.0019 ug/L 12/21/22 13:43 12/22/22 18:41 10.0038 U MAldrin
0.048 0.00095 ug/L 12/21/22 13:43 12/22/22 18:41 10.0038 Ualpha-BHC
0.048 0.0019 ug/L 12/21/22 13:43 12/22/22 18:41 10.0038 U Mbeta-BHC
0.048 0.0019 ug/L 12/21/22 13:43 12/22/22 18:41 10.0038 Udelta-BHC
0.048 0.0019 ug/L 12/21/22 13:43 12/22/22 18:41 10.0038 U MDieldrin
0.048 0.0019 ug/L 12/21/22 13:43 12/22/22 18:41 10.0038 U MEndosulfan I
0.048 0.0019 ug/L 12/21/22 13:43 12/22/22 18:41 10.0038 UEndosulfan II
0.048 0.0019 ug/L 12/21/22 13:43 12/22/22 18:41 10.0038 UEndosulfan sulfate
0.048 0.00095 ug/L 12/21/22 13:43 12/22/22 18:41 10.0038 UEndrin
0.048 0.0038 ug/L 12/21/22 13:43 12/22/22 18:41 10.015 UEndrin aldehyde
0.048 0.0038 ug/L 12/21/22 13:43 12/22/22 18:41 10.015 U QEndrin ketone
0.048 0.00095 ug/L 12/21/22 13:43 12/22/22 18:41 10.0038 Ugamma-BHC (Lindane)
0.048 0.00095 ug/L 12/21/22 13:43 12/22/22 18:41 10.0038 UHeptachlor
0.048 0.0019 ug/L 12/21/22 13:43 12/22/22 18:41 10.0038 UHeptachlor epoxide
0.048 0.0019 ug/L 12/21/22 13:43 12/22/22 18:41 10.0038 U MMethoxychlor
0.48 0.15 ug/L 12/21/22 13:43 12/22/22 18:41 10.38 U M QChlordane (technical)
0.95 0.31 ug/L 12/21/22 13:43 12/22/22 18:41 10.69 UPCB-1016
0.95 0.32 ug/L 12/21/22 13:43 12/22/22 18:41 10.69 UPCB-1221
0.95 0.32 ug/L 12/21/22 13:43 12/22/22 18:41 10.69 UPCB-1232
0.95 0.32 ug/L 12/21/22 13:43 12/22/22 18:41 10.69 UPCB-1242
0.95 0.32 ug/L 12/21/22 13:43 12/22/22 18:41 10.69 UPCB-1248
0.95 0.32 ug/L 12/21/22 13:43 12/22/22 18:41 10.69 UPCB-1254
0.95 0.32 ug/L 12/21/22 13:43 12/22/22 18:41 10.69 UPCB-1260
4.8 0.30 ug/L 12/21/22 13:43 12/22/22 18:41 10.76 U MToxaphene
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-8Client Sample ID: EQB-12-22
Matrix: WaterDate Collected: 12/14/22 15:20
Date Received: 12/15/22 09:00
DCB Decachlorobiphenyl 88 14-130 12/21/22 13:43 12/22/22 18:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene (Surr)64 12/21/22 13:43 12/22/22 18:41 144-124
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
LOQ DL
1.2 U 1.9 0.58 ug/L 12/19/22 18:32 12/23/22 00:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Anthracene
12 4.8 ug/L 12/19/22 18:32 12/23/22 00:11 19.6 UPyrene
1.9 0.58 ug/L 12/19/22 18:32 12/23/22 00:11 11.2 UBenzo[g,h,i]perylene
1.9 0.58 ug/L 12/19/22 18:32 12/23/22 00:11 11.2 UIndeno[1,2,3-cd]pyrene
1.9 0.58 ug/L 12/19/22 18:32 12/23/22 00:11 11.2 UBenzo[b]fluoranthene
1.9 0.48 ug/L 12/19/22 18:32 12/23/22 00:11 10.96 UFluoranthene
3.8 1.4 ug/L 12/19/22 18:32 12/23/22 00:11 12.9 UBenzo[k]fluoranthene
1.9 0.67 ug/L 12/19/22 18:32 12/23/22 00:11 11.3 UAcenaphthylene
1.9 0.48 ug/L 12/19/22 18:32 12/23/22 00:11 10.96 UChrysene
1.9 0.58 ug/L 12/19/22 18:32 12/23/22 00:11 11.2 UBenzo[a]pyrene
1.9 0.48 ug/L 12/19/22 18:32 12/23/22 00:11 10.96 UDibenz(a,h)anthracene
1.9 0.67 ug/L 12/19/22 18:32 12/23/22 00:11 11.3 UBenzo[a]anthracene
1.9 0.58 ug/L 12/19/22 18:32 12/23/22 00:11 11.2 UAcenaphthene
1.9 0.58 ug/L 12/19/22 18:32 12/23/22 00:11 11.2 UPhenanthrene
1.9 0.58 ug/L 12/19/22 18:32 12/23/22 00:11 11.2 UFluorene
1.9 0.58 ug/L 12/19/22 18:32 12/23/22 00:11 11.2 UNaphthalene
1.9 0.58 ug/L 12/19/22 18:32 12/23/22 00:11 11.2 U2-Methylnaphthalene
38 9.6 ug/L 12/19/22 18:32 12/23/22 00:11 129UC11-C22 Aromatics (unadjusted)
38 9.6 ug/L 12/19/22 18:32 12/23/22 00:11 129UC11-C22 Aromatics (Adjusted)
48 9.6 ug/L 12/19/22 18:32 12/23/22 00:11 1120MC19-C36 Aliphatics
29 9.6 ug/L 12/19/22 18:32 12/23/22 00:11 128J MC9-C18 Aliphatics
1-Chlorooctadecane (Surr)77 M 40-140 12/19/22 18:32 12/23/22 00:11 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)95 12/19/22 18:32 12/23/22 00:11 140-140
o- terphenyl (Surr)83 12/19/22 18:32 12/23/22 00:11 140-140
Method: SW846 7199 - Chromium, Hexavalent (IC) - Dissolved
LOQ DL
9.0 U H 10 5.0 ug/L 12/28/22 18:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Chromium (hexavalent)
10 5.0 ug/L 12/28/22 18:39 19.0 U HChromium (hexavalent)
Method: SW846 6020B - Metals (ICP/MS) - Total Recoverable
LOQ DL
1.0 U 2.0 0.39 ug/L 12/16/22 06:22 12/16/22 18:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Silver
200 35 ug/L 12/16/22 06:22 12/16/22 18:54 1100UAluminum
5.0 0.86 ug/L 12/16/22 06:22 12/16/22 18:54 13.0 UArsenic
5.0 0.89 ug/L 12/16/22 06:22 12/16/22 18:54 12.0 UBarium
0.50 0.20 ug/L 12/16/22 06:22 12/16/22 18:54 10.40 UBeryllium
500 140 ug/L 12/16/22 06:22 12/16/22 18:54 1300UCalcium
0.50 0.078 ug/L 12/16/22 06:22 12/16/22 18:54 10.20 UCadmium
1.0 0.22 ug/L 12/16/22 06:22 12/16/22 18:54 10.50 UCobalt
20 2.6 ug/L 12/16/22 06:22 12/16/22 18:54 110UChromium
5.0 0.90 ug/L 12/16/22 06:22 12/16/22 18:54 12.0 UCopper
100 26 ug/L 12/16/22 06:22 12/16/22 18:54 175UIron
1000 160 ug/L 12/16/22 06:22 12/16/22 18:54 1500UPotassium
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-8Client Sample ID: EQB-12-22
Matrix: WaterDate Collected: 12/14/22 15:20
Date Received: 12/15/22 09:00
Method: SW846 6020B - Metals (ICP/MS) - Total Recoverable (Continued)
LOQ DL
60 U 250 23 ug/L 12/16/22 06:22 12/16/22 18:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Magnesium
10 2.2 ug/L 12/16/22 06:22 12/16/22 18:54 15.0 UManganese
1000 200 ug/L 12/16/22 06:22 12/16/22 18:54 1500USodium
2.5 0.34 ug/L 12/16/22 06:22 12/16/22 18:54 11.0 ULead
5.0 1.2 ug/L 12/16/22 06:22 12/16/22 18:54 12.5 USelenium
10 1.8 ug/L 12/16/22 06:22 12/16/22 18:54 15.0 UNickel
5.0 0.52 ug/L 12/16/22 06:22 12/16/22 18:54 11.5 UAntimony
2.0 0.26 ug/L 12/16/22 06:22 12/16/22 18:54 11.0 UThallium
25 10 ug/L 12/16/22 06:22 12/16/22 18:54 120UZinc
10 1.8 ug/L 12/16/22 06:22 12/16/22 18:54 15.0 UVanadium
Lab Sample ID: 680-227663-9Client Sample ID: 149-TW-01
Matrix: WaterDate Collected: 12/14/22 15:30
Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS)
LOQ DL
3.8 J Q 25 3.7 ug/L 12/28/22 13:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acetone
2.0 0.27 ug/L 12/28/22 13:06 11.0 U MBenzene
2.5 0.59 ug/L 12/28/22 13:06 12.0 U QBromoform
20 3.7 ug/L 12/28/22 13:06 110UBromomethane
25 6.4 ug/L 12/28/22 13:06 120U Q2-Butanone (MEK)
2.0 0.43 ug/L 12/28/22 13:06 11.0 U QCarbon disulfide
2.0 0.30 ug/L 12/28/22 13:06 11.0 UCarbon tetrachloride
1.0 0.15 ug/L 12/28/22 13:06 10.50 UChlorobenzene
2.0 0.39 ug/L 12/28/22 13:06 11.0 UChlorodibromomethane
20 4.6 ug/L 12/28/22 13:06 110U QChloroethane
2.0 0.27 ug/L 12/28/22 13:06 11.0 UChloroform
2.5 0.54 ug/L 12/28/22 13:06 12.0 UChloromethane
2.0 0.25 ug/L 12/28/22 13:06 11.0 Ucis-1,2-Dichloroethene
2.0 0.26 ug/L 12/28/22 13:06 11.0 Ucis-1,3-Dichloropropene
2.0 0.28 ug/L 12/28/22 13:06 11.0 UCyclohexane
10 1.8 ug/L 12/28/22 13:06 15.0 U Q1,2-Dibromo-3-Chloropropane
2.0 0.33 ug/L 12/28/22 13:06 11.0 U1,2-Dibromoethane (EDB)
2.0 0.31 ug/L 12/28/22 13:06 11.0 U1,2-Dichlorobenzene
2.0 0.31 ug/L 12/28/22 13:06 11.0 U1,3-Dichlorobenzene
2.0 0.31 ug/L 12/28/22 13:06 11.0 U1,4-Dichlorobenzene
2.0 0.25 ug/L 12/28/22 13:06 11.0 UDichlorobromomethane
2.0 0.36 ug/L 12/28/22 13:06 11.0 U QDichlorodifluoromethane
2.0 0.33 ug/L 12/28/22 13:06 11.0 U1,1-Dichloroethane
2.0 0.25 ug/L 12/28/22 13:06 11.0 U M1,2-Dichloroethane
2.0 0.33 ug/L 12/28/22 13:06 11.0 U1,1-Dichloroethene
1.0 0.22 ug/L 12/28/22 13:06 10.50 U1,2-Dichloropropane
1.0 0.20 ug/L 12/28/22 13:06 10.50 UEthylbenzene
20 3.2 ug/L 12/28/22 13:06 110U2-Hexanone
2.0 0.26 ug/L 12/28/22 13:06 11.0 UIsopropylbenzene
20 3.2 ug/L 12/28/22 13:06 110U QMethyl acetate
2.0 0.33 ug/L 12/28/22 13:06 11.0 UMethylcyclohexane
20 3.2 ug/L 12/28/22 13:06 110UMethylene Chloride
20 2.7 ug/L 12/28/22 13:06 110U Q4-Methyl-2-pentanone (MIBK)
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-9Client Sample ID: 149-TW-01
Matrix: WaterDate Collected: 12/14/22 15:30
Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
2.0 U Q 5.0 0.81 ug/L 12/28/22 13:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Methyl tert-butyl ether
2.0 0.27 ug/L 12/28/22 13:06 11.0 UStyrene
2.0 0.40 ug/L 12/28/22 13:06 11.0 U1,1,2,2-Tetrachloroethane
2.0 0.35 ug/L 12/28/22 13:06 11.0 UTetrachloroethene
2.0 0.25 ug/L 12/28/22 13:06 11.0 UToluene
2.0 0.34 ug/L 12/28/22 13:06 11.0 Utrans-1,2-Dichloroethene
2.0 0.23 ug/L 12/28/22 13:06 11.0 Utrans-1,3-Dichloropropene
5.0 0.53 ug/L 12/28/22 13:06 12.0 U1,2,4-Trichlorobenzene
1.0 0.21 ug/L 12/28/22 13:06 10.50 U1,1,1-Trichloroethane
2.0 0.32 ug/L 12/28/22 13:06 11.0 U1,1,2-Trichloroethane
1.0 0.20 ug/L 12/28/22 13:06 10.50 UTrichloroethene
2.0 0.33 ug/L 12/28/22 13:06 11.0 UTrichlorofluoromethane
1.0 0.23 ug/L 12/28/22 13:06 10.50 U1,1,2-Trichloro-1,2,2-trifluoroethane
2.0 0.40 ug/L 12/28/22 13:06 11.0 UVinyl chloride
2.0 0.49 ug/L 12/28/22 13:06 11.0 UXylenes, Total
20 5.0 ug/L 12/28/22 13:06 110U QPropionitrile
5.0 0.50 ug/L 12/28/22 13:06 11.0 U QPentachloroethane
2.5 0.78 ug/L 12/28/22 13:06 12.0 U QMethyl methacrylate
5.0 0.22 ug/L 12/28/22 13:06 11.0 UHexachlorobutadiene
2.0 0.34 ug/L 12/28/22 13:06 11.0 UDibromomethane
50 20 ug/L 12/28/22 13:06 140UAcetonitrile
10 2.4 ug/L 12/28/22 13:06 15.0 U QNaphthalene
20 3.9 ug/L 12/28/22 13:06 110U QIodomethane
5.0 1.1 ug/L 12/28/22 13:06 14.0 U3-Chloro-1-propene
50 5.5 ug/L 12/28/22 13:06 120UAcrylonitrile
2.0 0.33 ug/L 12/28/22 13:06 11.0 UEthyl methacrylate
2.0 0.36 ug/L 12/28/22 13:06 11.0 U1,1,1,2-Tetrachloroethane
10 1.3 ug/L 12/28/22 13:06 15.0 Utrans-1,4-Dichloro-2-butene
2.5 0.71 ug/L 12/28/22 13:06 12.0 U2-Chloro-1,3-butadiene
20 5.0 ug/L 12/28/22 13:06 110U QMethacrylonitrile
50 15 ug/L 12/28/22 13:06 140UAcrolein
2.0 0.48 ug/L 12/28/22 13:06 11.0 U1,2,3-Trichloropropane
2.5 0.69 ug/L 12/28/22 13:06 12.0 U QVinyl acetate
500 68 ug/L 12/28/22 13:06 1250U QIsobutyl alcohol
4.0 0.86 ug/L 12/28/22 13:06 12.0 U Q2-Nitropropane
100 25 ug/L 12/28/22 13:06 150U Qn-Butyl alcohol
2.0 0.34 ug/L 12/28/22 13:06 11.0 UBromochloromethane
5.0 0.37 ug/L 12/28/22 13:06 11.0 UDiethyl ether
10 2.1 ug/L 12/28/22 13:06 15.0 U QTetrahydrofuran
20 5.0 ug/L 12/28/22 13:06 110U QEthyl acetate
10 2.5 ug/L 12/28/22 13:06 15.0 U QBenzyl chloride
2.5 0.52 ug/L 12/28/22 13:06 12.0 Un-Butylbenzene
2.0 0.43 ug/L 12/28/22 13:06 11.0 U1,2,4-Trimethylbenzene
1.0 0.25 ug/L 12/28/22 13:06 10.50 U2-Chlorotoluene
5.0 0.50 ug/L 12/28/22 13:06 11.0 U Qn-Butyl acetate
2.0 0.37 ug/L 12/28/22 13:06 11.0 U1,2-Dichloroethene, Total
2.0 0.28 ug/L 12/28/22 13:06 11.0 U1,1-Dichloropropene
10 2.5 ug/L 12/28/22 13:06 15.0 U Q2-Methylnaphthalene
2.0 0.26 ug/L 12/28/22 13:06 11.0 Uo-Xylene
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-9Client Sample ID: 149-TW-01
Matrix: WaterDate Collected: 12/14/22 15:30
Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
2.0 U 5.0 0.65 ug/L 12/28/22 13:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Hexane
2.0 0.41 ug/L 12/28/22 13:06 11.0 U4-Chlorotoluene
5.0 1.1 ug/L 12/28/22 13:06 14.0 U M1-Chlorohexane
1.0 0.24 ug/L 12/28/22 13:06 10.50 UBromobenzene
5.0 0.81 ug/L 12/28/22 13:06 12.0 U Q1,2,3-Trichlorobenzene
2.0 0.48 ug/L 12/28/22 13:06 11.0 U1,3-Dichloropropene, Total
2.5 0.53 ug/L 12/28/22 13:06 12.0 Usec-Butylbenzene
2.0 0.35 ug/L 12/28/22 13:06 11.0 U2,2-Dichloropropane
2.0 0.41 ug/L 12/28/22 13:06 11.0 UN-Propylbenzene
10 2.5 ug/L 12/28/22 13:06 15.0 U1,3,5-Trichlorobenzene
10 0.70 ug/L 12/28/22 13:06 12.0 UDiisopropyl ether
200 50 ug/L 12/28/22 13:06 1100U QEthanol
100 25 ug/L 12/28/22 13:06 150U QIsopropyl alcohol
2.0 0.44 ug/L 12/28/22 13:06 11.0 Up-Cymene
2.5 0.78 ug/L 12/28/22 13:06 12.0 U QTert-amyl methyl ether
2.0 0.28 ug/L 12/28/22 13:06 11.0 U1,3,5-Trimethylbenzene
10 2.5 ug/L 12/28/22 13:06 15.0 U1,2,3-Trimethylbenzene
2.0 0.49 ug/L 12/28/22 13:06 11.0 Um-Xylene & p-Xylene
2.0 0.50 ug/L 12/28/22 13:06 11.0 U QDichlorofluoromethane
2.0 0.43 ug/L 12/28/22 13:06 11.0 Utert-Butylbenzene
5.0 0.99 ug/L 12/28/22 13:06 12.0 UIsooctane
2.0 0.36 ug/L 12/28/22 13:06 11.0 U1,3-Dichloropropane
4-Bromofluorobenzene (Surr)101 85-114 12/28/22 13:06 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)102 12/28/22 13:06 180-119
1,2-Dichloroethane-d4 (Surr)83 12/28/22 13:06 181-118
Toluene-d8 (Surr)112 12/28/22 13:06 189-112
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
LOQ DL
10 U M 20 4.6 ug/L 12/20/22 11:44 12/23/22 21:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
20 4.5 ug/L 12/20/22 11:44 12/23/22 21:25 110U1,2,4,5-Tetrachlorobenzene
20 3.4 ug/L 12/20/22 11:44 12/23/22 21:25 110U1,2,4-Trichlorobenzene
10 2.5 ug/L 12/20/22 11:44 12/23/22 21:25 15.0 U1,2-Dichlorobenzene
20 3.7 ug/L 12/20/22 11:44 12/23/22 21:25 110U1,2-Diphenylhydrazine
20 2.9 ug/L 12/20/22 11:44 12/23/22 21:25 110U1,3-Dichlorobenzene
20 3.3 ug/L 12/20/22 11:44 12/23/22 21:25 110U1,4-Dichlorobenzene
20 4.7 ug/L 12/20/22 11:44 12/23/22 21:25 110U1-Methylnaphthalene
20 4.3 ug/L 12/20/22 11:44 12/23/22 21:25 110U2,3,4,6-Tetrachlorophenol
20 3.3 ug/L 12/20/22 11:44 12/23/22 21:25 110U2,4,5-Trichlorophenol
20 2.2 ug/L 12/20/22 11:44 12/23/22 21:25 15.0 U2,4,6-Trichlorophenol
20 3.7 ug/L 12/20/22 11:44 12/23/22 21:25 110U2,4-Dichlorophenol
20 3.0 ug/L 12/20/22 11:44 12/23/22 21:25 110U2,4-Dimethylphenol
50 16 ug/L 12/20/22 11:44 12/23/22 21:25 140U2,4-Dinitrophenol
10 2.3 ug/L 12/20/22 11:44 12/23/22 21:25 15.0 U2,4-Dinitrotoluene
10 2.4 ug/L 12/20/22 11:44 12/23/22 21:25 15.0 U2,6-Dichlorophenol
20 2.8 ug/L 12/20/22 11:44 12/23/22 21:25 110U2,6-Dinitrotoluene
20 4.8 ug/L 12/20/22 11:44 12/23/22 21:25 110U2-Chloronaphthalene
20 3.2 ug/L 12/20/22 11:44 12/23/22 21:25 110U2-Chlorophenol
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-9Client Sample ID: 149-TW-01
Matrix: WaterDate Collected: 12/14/22 15:30
Date Received: 12/15/22 09:00
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
10 U 20 4.6 ug/L 12/20/22 11:44 12/23/22 21:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2-Methylnaphthalene
10 1.8 ug/L 12/20/22 11:44 12/23/22 21:25 14.0 U2-Methylphenol
20 2.9 ug/L 12/20/22 11:44 12/23/22 21:25 110U2-Nitroaniline
20 3.9 ug/L 12/20/22 11:44 12/23/22 21:25 110U2-Nitrophenol
10 1.4 ug/L 12/20/22 11:44 12/23/22 21:25 14.0 U3 & 4 Methylphenol
50 10 ug/L 12/20/22 11:44 12/23/22 21:25 120U Q3,3'-Dichlorobenzidine
50 3.0 ug/L 12/20/22 11:44 12/23/22 21:25 110U3-Nitroaniline
50 5.3 ug/L 12/20/22 11:44 12/23/22 21:25 120U4,6-Dinitro-2-methylphenol
20 4.7 ug/L 12/20/22 11:44 12/23/22 21:25 110U M4-Bromophenyl phenyl ether
20 2.5 ug/L 12/20/22 11:44 12/23/22 21:25 110U4-Chloro-3-methylphenol
10 1.0 ug/L 12/20/22 11:44 12/23/22 21:25 14.0 U4-Chloroaniline
20 5.3 ug/L 12/20/22 11:44 12/23/22 21:25 112U4-Chlorophenyl phenyl ether
50 3.0 ug/L 12/20/22 11:44 12/23/22 21:25 110U4-Nitroaniline
50 8.2 ug/L 12/20/22 11:44 12/23/22 21:25 120U4-Nitrophenol
20 4.4 ug/L 12/20/22 11:44 12/23/22 21:25 110UAcenaphthene
20 3.6 ug/L 12/20/22 11:44 12/23/22 21:25 110UAcenaphthylene
10 2.2 ug/L 12/20/22 11:44 12/23/22 21:25 15.0 UAcetophenone
20 3.6 ug/L 12/20/22 11:44 12/23/22 21:25 110UAnthracene
10 2.2 ug/L 12/20/22 11:44 12/23/22 21:25 15.0 UAtrazine
20 3.6 ug/L 12/20/22 11:44 12/23/22 21:25 110U QAzobenzene
20 4.8 ug/L 12/20/22 11:44 12/23/22 21:25 110U MBenzaldehyde
20 4.2 ug/L 12/20/22 11:44 12/23/22 21:25 110UBenzo[a]anthracene
20 2.8 ug/L 12/20/22 11:44 12/23/22 21:25 110UBenzo[a]pyrene
20 3.1 ug/L 12/20/22 11:44 12/23/22 21:25 110U MBenzo[b]fluoranthene
20 3.0 ug/L 12/20/22 11:44 12/23/22 21:25 110UBenzo[g,h,i]perylene
20 2.9 ug/L 12/20/22 11:44 12/23/22 21:25 110UBenzo[k]fluoranthene
20 2.6 ug/L 12/20/22 11:44 12/23/22 21:25 110U MBenzyl alcohol
20 3.1 ug/L 12/20/22 11:44 12/23/22 21:25 110Ubis (2-chloroisopropyl) ether
10 1.8 ug/L 12/20/22 11:44 12/23/22 21:25 14.0 UBis(2-chloroethoxy)methane
20 3.6 ug/L 12/20/22 11:44 12/23/22 21:25 110UBis(2-chloroethyl)ether
20 3.0 ug/L 12/20/22 11:44 12/23/22 21:25 13.1 JBis(2-ethylhexyl) phthalate
20 2.8 ug/L 12/20/22 11:44 12/23/22 21:25 110UButyl benzyl phthalate
20 2.8 ug/L 12/20/22 11:44 12/23/22 21:25 110UCaprolactam
10 1.8 ug/L 12/20/22 11:44 12/23/22 21:25 14.0 UCarbazole
20 3.8 ug/L 12/20/22 11:44 12/23/22 21:25 110UChrysene
20 3.0 ug/L 12/20/22 11:44 12/23/22 21:25 110UDibenz(a,h)anthracene
10 1.9 ug/L 12/20/22 11:44 12/23/22 21:25 14.0 UDibenzofuran
10 2.2 ug/L 12/20/22 11:44 12/23/22 21:25 15.0 UDiethyl phthalate
10 2.1 ug/L 12/20/22 11:44 12/23/22 21:25 15.0 UDimethyl phthalate
10 2.3 ug/L 12/20/22 11:44 12/23/22 21:25 15.0 UDi-n-butyl phthalate
20 2.8 ug/L 12/20/22 11:44 12/23/22 21:25 110U MDi-n-octyl phthalate
10 2.5 ug/L 12/20/22 11:44 12/23/22 21:25 18.6 UDiphenylamine
10 1.6 ug/L 12/20/22 11:44 12/23/22 21:25 14.0 UFluoranthene
20 3.4 ug/L 12/20/22 11:44 12/23/22 21:25 110UFluorene
10 1.6 ug/L 12/20/22 11:44 12/23/22 21:25 14.0 UHexachlorobenzene
20 4.0 ug/L 12/20/22 11:44 12/23/22 21:25 110UHexachlorobutadiene
20 3.5 ug/L 12/20/22 11:44 12/23/22 21:25 110UHexachlorocyclopentadiene
20 3.6 ug/L 12/20/22 11:44 12/23/22 21:25 110UHexachloroethane
20 4.3 ug/L 12/20/22 11:44 12/23/22 21:25 110UIndeno[1,2,3-cd]pyrene
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-9Client Sample ID: 149-TW-01
Matrix: WaterDate Collected: 12/14/22 15:30
Date Received: 12/15/22 09:00
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
4.0 U 10 2.0 ug/L 12/20/22 11:44 12/23/22 21:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Isophorone
20 3.5 ug/L 12/20/22 11:44 12/23/22 21:25 110UNaphthalene
20 3.5 ug/L 12/20/22 11:44 12/23/22 21:25 110UNitrobenzene
10 2.4 ug/L 12/20/22 11:44 12/23/22 21:25 15.0 UN-Nitrosodi-n-propylamine
20 2.9 ug/L 12/20/22 11:44 12/23/22 21:25 110UN-Nitrosodiphenylamine
50 10 ug/L 12/20/22 11:44 12/23/22 21:25 120UPentachlorophenol
20 4.3 ug/L 12/20/22 11:44 12/23/22 21:25 110UPhenanthrene
10 1.5 ug/L 12/20/22 11:44 12/23/22 21:25 14.0 UPhenol
20 3.7 ug/L 12/20/22 11:44 12/23/22 21:25 110U MPyrene
2-Fluorobiphenyl (Surr)55 44-119 12/20/22 11:44 12/23/22 21:25 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)25 12/20/22 11:44 12/23/22 21:25 119-119
Nitrobenzene-d5 (Surr)51 12/20/22 11:44 12/23/22 21:25 144-120
Phenol-d5 (Surr)16 12/20/22 11:44 12/23/22 21:25 110-130
Terphenyl-d14 (Surr)69 12/20/22 11:44 12/23/22 21:25 150-134
2,4,6-Tribromophenol (Surr)84 12/20/22 11:44 12/23/22 21:25 143-140
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
40 U 100 20 ug/L 01/18/23 06:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
2.0 U 5.0 1.0 ug/L 12/28/22 13:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Benzene
100 25 ug/L 12/28/22 13:51 150U MC5-C8 Aliphatics
100 10 ug/L 12/28/22 13:51 120UC9-C10 Aromatics
100 25 ug/L 12/28/22 13:51 150U MC9-C12 Aliphatics
5.0 1.0 ug/L 12/28/22 13:51 12.0 UEthylbenzene
5.0 1.0 ug/L 12/28/22 13:51 12.0 U QMethyl tert-butyl ether
6.0 2.0 ug/L 12/28/22 13:51 14.0 UNaphthalene
5.0 1.0 ug/L 12/28/22 13:51 12.0 UToluene
100 25 ug/L 12/28/22 13:51 150UC9-C12 Aliphatics (adjusted)
10 2.5 ug/L 12/28/22 13:51 15.0 Um-Xylene & p-Xylene
5.0 1.0 ug/L 12/28/22 13:51 12.0 Uo-Xylene
100 25 ug/L 12/28/22 13:51 150UC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)105 M 70-130 12/28/22 13:51 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)94 12/28/22 13:51 170-130
Method: SW846 8081B 8082A - Organochlorine Pesticides & PCBs (GC)
LOQ DL
0.0039 U 0.049 0.0019 ug/L 12/21/22 13:43 12/22/22 18:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,4'-DDD
0.049 0.00097 ug/L 12/21/22 13:43 12/22/22 18:56 10.0039 U4,4'-DDE
0.049 0.00097 ug/L 12/21/22 13:43 12/22/22 18:56 10.0039 U Q4,4'-DDT
0.049 0.0019 ug/L 12/21/22 13:43 12/22/22 18:56 10.0039 U MAldrin
0.049 0.00097 ug/L 12/21/22 13:43 12/22/22 18:56 10.0039 Ualpha-BHC
0.049 0.0019 ug/L 12/21/22 13:43 12/22/22 18:56 10.0039 U Mbeta-BHC
0.049 0.0019 ug/L 12/21/22 13:43 12/22/22 18:56 10.0039 Udelta-BHC
0.049 0.0019 ug/L 12/21/22 13:43 12/22/22 18:56 10.0039 UDieldrin
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-9Client Sample ID: 149-TW-01
Matrix: WaterDate Collected: 12/14/22 15:30
Date Received: 12/15/22 09:00
Method: SW846 8081B 8082A - Organochlorine Pesticides & PCBs (GC) (Continued)
LOQ DL
0.0039 U 0.049 0.0019 ug/L 12/21/22 13:43 12/22/22 18:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Endosulfan I
0.049 0.0019 ug/L 12/21/22 13:43 12/22/22 18:56 10.0039 UEndosulfan II
0.049 0.0019 ug/L 12/21/22 13:43 12/22/22 18:56 10.0039 UEndosulfan sulfate
0.049 0.00097 ug/L 12/21/22 13:43 12/22/22 18:56 10.0039 U MEndrin
0.049 0.0039 ug/L 12/21/22 13:43 12/22/22 18:56 10.016 UEndrin aldehyde
0.049 0.0039 ug/L 12/21/22 13:43 12/22/22 18:56 10.016 U QEndrin ketone
0.049 0.00097 ug/L 12/21/22 13:43 12/22/22 18:56 10.0039 U Mgamma-BHC (Lindane)
0.049 0.00097 ug/L 12/21/22 13:43 12/22/22 18:56 10.0039 UHeptachlor
0.049 0.0019 ug/L 12/21/22 13:43 12/22/22 18:56 10.0039 UHeptachlor epoxide
0.049 0.0019 ug/L 12/21/22 13:43 12/22/22 18:56 10.0039 UMethoxychlor
0.49 0.16 ug/L 12/21/22 13:43 12/22/22 18:56 10.39 U M QChlordane (technical)
0.97 0.31 ug/L 12/21/22 13:43 12/22/22 18:56 10.70 UPCB-1016
0.97 0.33 ug/L 12/21/22 13:43 12/22/22 18:56 10.70 UPCB-1221
0.97 0.33 ug/L 12/21/22 13:43 12/22/22 18:56 10.70 UPCB-1232
0.97 0.33 ug/L 12/21/22 13:43 12/22/22 18:56 10.70 UPCB-1242
0.97 0.33 ug/L 12/21/22 13:43 12/22/22 18:56 10.70 UPCB-1248
0.97 0.33 ug/L 12/21/22 13:43 12/22/22 18:56 10.70 U MPCB-1254
0.97 0.33 ug/L 12/21/22 13:43 12/22/22 18:56 10.70 U MPCB-1260
4.9 0.30 ug/L 12/21/22 13:43 12/22/22 18:56 10.78 U MToxaphene
DCB Decachlorobiphenyl 43 14-130 12/21/22 13:43 12/22/22 18:56 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene (Surr)62 12/21/22 13:43 12/22/22 18:56 144-124
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
LOQ DL
1.2 U 2.0 0.59 ug/L 12/19/22 18:32 12/23/22 00:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Anthracene
12 4.9 ug/L 12/19/22 18:32 12/23/22 00:34 19.8 UPyrene
2.0 0.59 ug/L 12/19/22 18:32 12/23/22 00:34 11.2 UBenzo[g,h,i]perylene
2.0 0.59 ug/L 12/19/22 18:32 12/23/22 00:34 11.2 UIndeno[1,2,3-cd]pyrene
2.0 0.59 ug/L 12/19/22 18:32 12/23/22 00:34 11.2 UBenzo[b]fluoranthene
2.0 0.49 ug/L 12/19/22 18:32 12/23/22 00:34 10.98 UFluoranthene
3.9 1.5 ug/L 12/19/22 18:32 12/23/22 00:34 12.9 UBenzo[k]fluoranthene
2.0 0.69 ug/L 12/19/22 18:32 12/23/22 00:34 11.4 UAcenaphthylene
2.0 0.49 ug/L 12/19/22 18:32 12/23/22 00:34 10.98 UChrysene
2.0 0.59 ug/L 12/19/22 18:32 12/23/22 00:34 11.2 UBenzo[a]pyrene
2.0 0.49 ug/L 12/19/22 18:32 12/23/22 00:34 10.98 UDibenz(a,h)anthracene
2.0 0.69 ug/L 12/19/22 18:32 12/23/22 00:34 11.4 UBenzo[a]anthracene
2.0 0.59 ug/L 12/19/22 18:32 12/23/22 00:34 11.2 UAcenaphthene
2.0 0.59 ug/L 12/19/22 18:32 12/23/22 00:34 11.2 UPhenanthrene
2.0 0.59 ug/L 12/19/22 18:32 12/23/22 00:34 11.2 UFluorene
2.0 0.59 ug/L 12/19/22 18:32 12/23/22 00:34 11.2 UNaphthalene
2.0 0.59 ug/L 12/19/22 18:32 12/23/22 00:34 11.2 U2-Methylnaphthalene
39 9.8 ug/L 12/19/22 18:32 12/23/22 00:34 136JC11-C22 Aromatics (unadjusted)
39 9.8 ug/L 12/19/22 18:32 12/23/22 00:34 135JC11-C22 Aromatics (Adjusted)
49 9.8 ug/L 12/19/22 18:32 12/23/22 00:34 188MC19-C36 Aliphatics
29 9.8 ug/L 12/19/22 18:32 12/23/22 00:34 117J MC9-C18 Aliphatics
1-Chlorooctadecane (Surr)15 Q M 40-140 12/19/22 18:32 12/23/22 00:34 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-9Client Sample ID: 149-TW-01
Matrix: WaterDate Collected: 12/14/22 15:30
Date Received: 12/15/22 09:00
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
2-Fluorobiphenyl (Surr)86 40-140 12/19/22 18:32 12/23/22 00:34 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
o- terphenyl (Surr)56 12/19/22 18:32 12/23/22 00:34 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - RE
LOQ DL
1.2 U 2.0 0.59 ug/L 12/27/22 21:11 12/30/22 20:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Anthracene
12 4.9 ug/L 12/27/22 21:11 12/30/22 20:03 19.8 UPyrene
2.0 0.59 ug/L 12/27/22 21:11 12/30/22 20:03 11.2 UBenzo[g,h,i]perylene
2.0 0.59 ug/L 12/27/22 21:11 12/30/22 20:03 11.2 UIndeno[1,2,3-cd]pyrene
2.0 0.59 ug/L 12/27/22 21:11 12/30/22 20:03 11.2 UBenzo[b]fluoranthene
2.0 0.49 ug/L 12/27/22 21:11 12/30/22 20:03 10.98 UFluoranthene
3.9 1.5 ug/L 12/27/22 21:11 12/30/22 20:03 13.0 UBenzo[k]fluoranthene
2.0 0.69 ug/L 12/27/22 21:11 12/30/22 20:03 11.4 UAcenaphthylene
2.0 0.49 ug/L 12/27/22 21:11 12/30/22 20:03 10.98 UChrysene
2.0 0.49 ug/L 12/27/22 21:11 12/30/22 20:03 10.98 UDibenz(a,h)anthracene
2.0 0.69 ug/L 12/27/22 21:11 12/30/22 20:03 11.4 UBenzo[a]anthracene
2.0 0.59 ug/L 12/27/22 21:11 12/30/22 20:03 11.2 UAcenaphthene
2.0 0.59 ug/L 12/27/22 21:11 12/30/22 20:03 11.2 UPhenanthrene
2.0 0.59 ug/L 12/27/22 21:11 12/30/22 20:03 11.2 UFluorene
2.0 0.59 ug/L 12/27/22 21:11 12/30/22 20:03 11.2 U MNaphthalene
2.0 0.59 ug/L 12/27/22 21:11 12/30/22 20:03 11.2 U2-Methylnaphthalene
49 9.8 ug/L 12/27/22 21:11 12/30/22 20:03 1130MC19-C36 Aliphatics
30 9.8 ug/L 12/27/22 21:11 12/30/22 20:03 136MC9-C18 Aliphatics
1-Chlorooctadecane (Surr)11 M Q 40-140 12/27/22 21:11 12/30/22 20:03 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)92 12/27/22 21:11 12/30/22 20:03 140-140
o- terphenyl (Surr)48 12/27/22 21:11 12/30/22 20:03 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - REDL
LOQ DL
54 D M 3.9 1.2 ug/L 12/27/22 21:11 01/04/23 21:47 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Benzo[a]pyrene
79 20 ug/L 12/27/22 21:11 01/04/23 21:47 284D MC11-C22 Aromatics (unadjusted)
79 20 ug/L 12/27/22 21:11 01/04/23 21:47 229J DC11-C22 Aromatics (Adjusted)
2-Fluorobiphenyl (Surr)93 40-140 12/27/22 21:11 01/04/23 21:47 2
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
o- terphenyl (Surr)50 12/27/22 21:11 01/04/23 21:47 240-140
Method: SW846 7199 - Chromium, Hexavalent (IC) - Dissolved
LOQ DL
9.0 U H 10 5.0 ug/L 12/28/22 18:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Chromium (hexavalent)
10 5.0 ug/L 12/28/22 19:05 19.0 U HChromium (hexavalent)
Method: SW846 6020B - Metals (ICP/MS) - Total Recoverable
LOQ DL
1.0 U 2.0 0.39 ug/L 12/16/22 06:22 12/16/22 18:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Silver
200 35 ug/L 12/16/22 06:22 12/16/22 18:58 1900Aluminum
5.0 0.86 ug/L 12/16/22 06:22 12/16/22 18:58 13.0 UArsenic
5.0 0.89 ug/L 12/16/22 06:22 12/16/22 18:58 119Barium
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-9Client Sample ID: 149-TW-01
Matrix: WaterDate Collected: 12/14/22 15:30
Date Received: 12/15/22 09:00
Method: SW846 6020B - Metals (ICP/MS) - Total Recoverable (Continued)
LOQ DL
0.40 U 0.50 0.20 ug/L 12/16/22 06:22 12/16/22 18:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Beryllium
500 140 ug/L 12/16/22 06:22 12/16/22 18:58 123000Calcium
0.50 0.078 ug/L 12/16/22 06:22 12/16/22 18:58 10.20 UCadmium
1.0 0.22 ug/L 12/16/22 06:22 12/16/22 18:58 12.9Cobalt
20 2.6 ug/L 12/16/22 06:22 12/16/22 18:58 115JChromium
5.0 0.90 ug/L 12/16/22 06:22 12/16/22 18:58 120Copper
100 26 ug/L 12/16/22 06:22 12/16/22 18:58 16900Iron
1000 160 ug/L 12/16/22 06:22 12/16/22 18:58 12800Potassium
250 23 ug/L 12/16/22 06:22 12/16/22 18:58 11300Magnesium
10 2.2 ug/L 12/16/22 06:22 12/16/22 18:58 1450Manganese
1000 200 ug/L 12/16/22 06:22 12/16/22 18:58 19900Sodium
2.5 0.34 ug/L 12/16/22 06:22 12/16/22 18:58 11.0 JLead
5.0 1.2 ug/L 12/16/22 06:22 12/16/22 18:58 12.5 USelenium
10 1.8 ug/L 12/16/22 06:22 12/16/22 18:58 14.9 JNickel
5.0 0.52 ug/L 12/16/22 06:22 12/16/22 18:58 11.5 UAntimony
2.0 0.26 ug/L 12/16/22 06:22 12/16/22 18:58 11.0 UThallium
25 10 ug/L 12/16/22 06:22 12/16/22 18:58 132Zinc
10 1.8 ug/L 12/16/22 06:22 12/16/22 18:58 12.5 JVanadium
Method: SW846 6020B - Metals (ICP/MS) - Dissolved
LOQ DL
1.0 U 2.0 0.39 ug/L 12/21/22 07:02 12/22/22 18:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Silver
200 35 ug/L 12/21/22 07:02 12/22/22 18:07 1430Aluminum
5.0 0.86 ug/L 12/21/22 07:02 12/22/22 18:07 13.0 UArsenic
5.0 0.89 ug/L 12/21/22 07:02 12/22/22 18:07 123Barium
0.50 0.20 ug/L 12/21/22 07:02 12/22/22 18:07 10.40 UBeryllium
500 140 ug/L 12/21/22 07:02 12/22/22 18:07 136000Calcium
0.50 0.078 ug/L 12/21/22 07:02 12/22/22 18:07 10.20 UCadmium
1.0 0.22 ug/L 12/21/22 07:02 12/22/22 18:07 11.6Cobalt
20 2.6 ug/L 12/21/22 07:02 12/22/22 18:07 110UChromium
5.0 0.90 ug/L 12/21/22 07:02 12/22/22 18:07 12.0 UCopper
100 26 ug/L 12/21/22 07:02 12/22/22 18:07 1200Iron
1000 160 ug/L 12/21/22 07:02 12/22/22 18:07 13700Potassium
250 23 ug/L 12/21/22 07:02 12/22/22 18:07 11800Magnesium
10 2.2 ug/L 12/21/22 07:02 12/22/22 18:07 1560Manganese
1000 200 ug/L 12/21/22 07:02 12/22/22 18:07 113000Sodium
2.5 0.34 ug/L 12/21/22 07:02 12/22/22 18:07 10.37 JLead
5.0 1.2 ug/L 12/21/22 07:02 12/22/22 18:07 12.5 USelenium
10 1.8 ug/L 12/21/22 07:02 12/22/22 18:07 12.4 JNickel
5.0 0.52 ug/L 12/21/22 07:02 12/22/22 18:07 11.5 UAntimony
2.0 0.26 ug/L 12/21/22 07:02 12/22/22 18:07 11.0 UThallium
25 10 ug/L 12/21/22 07:02 12/22/22 18:07 120UZinc
10 1.8 ug/L 12/21/22 07:02 12/22/22 18:07 15.0 UVanadium
Method: SW846 7470A - Mercury (CVAA) - Dissolved
LOQ DL
0.20 U 0.25 0.080 ug/L 12/16/22 08:53 12/19/22 09:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Hg
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-10Client Sample ID: DUP-TW-01
Matrix: WaterDate Collected: 12/14/22 16:00
Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS)
LOQ DL
10 U Q 25 3.7 ug/L 12/28/22 13:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acetone
2.0 0.27 ug/L 12/28/22 13:24 11.0 U MBenzene
2.5 0.59 ug/L 12/28/22 13:24 12.0 U QBromoform
20 3.7 ug/L 12/28/22 13:24 110UBromomethane
25 6.4 ug/L 12/28/22 13:24 120U Q2-Butanone (MEK)
2.0 0.43 ug/L 12/28/22 13:24 11.0 U QCarbon disulfide
2.0 0.30 ug/L 12/28/22 13:24 11.0 UCarbon tetrachloride
1.0 0.15 ug/L 12/28/22 13:24 10.50 UChlorobenzene
2.0 0.39 ug/L 12/28/22 13:24 11.0 UChlorodibromomethane
20 4.6 ug/L 12/28/22 13:24 110U QChloroethane
2.0 0.27 ug/L 12/28/22 13:24 11.0 UChloroform
2.5 0.54 ug/L 12/28/22 13:24 12.0 UChloromethane
2.0 0.25 ug/L 12/28/22 13:24 11.0 Ucis-1,2-Dichloroethene
2.0 0.26 ug/L 12/28/22 13:24 11.0 Ucis-1,3-Dichloropropene
2.0 0.28 ug/L 12/28/22 13:24 11.0 UCyclohexane
10 1.8 ug/L 12/28/22 13:24 15.0 U Q1,2-Dibromo-3-Chloropropane
2.0 0.33 ug/L 12/28/22 13:24 11.0 U1,2-Dibromoethane (EDB)
2.0 0.31 ug/L 12/28/22 13:24 11.0 U1,2-Dichlorobenzene
2.0 0.31 ug/L 12/28/22 13:24 11.0 U1,3-Dichlorobenzene
2.0 0.31 ug/L 12/28/22 13:24 11.0 U1,4-Dichlorobenzene
2.0 0.25 ug/L 12/28/22 13:24 11.0 UDichlorobromomethane
2.0 0.36 ug/L 12/28/22 13:24 11.0 U QDichlorodifluoromethane
2.0 0.33 ug/L 12/28/22 13:24 11.0 U1,1-Dichloroethane
2.0 0.25 ug/L 12/28/22 13:24 11.0 U M1,2-Dichloroethane
2.0 0.33 ug/L 12/28/22 13:24 11.0 U1,1-Dichloroethene
1.0 0.22 ug/L 12/28/22 13:24 10.50 U1,2-Dichloropropane
1.0 0.20 ug/L 12/28/22 13:24 10.50 UEthylbenzene
20 3.2 ug/L 12/28/22 13:24 110U2-Hexanone
2.0 0.26 ug/L 12/28/22 13:24 11.0 UIsopropylbenzene
20 3.2 ug/L 12/28/22 13:24 110U QMethyl acetate
2.0 0.33 ug/L 12/28/22 13:24 11.0 UMethylcyclohexane
20 3.2 ug/L 12/28/22 13:24 110UMethylene Chloride
20 2.7 ug/L 12/28/22 13:24 110U Q4-Methyl-2-pentanone (MIBK)
5.0 0.81 ug/L 12/28/22 13:24 12.0 U QMethyl tert-butyl ether
2.0 0.27 ug/L 12/28/22 13:24 11.0 UStyrene
2.0 0.40 ug/L 12/28/22 13:24 11.0 U1,1,2,2-Tetrachloroethane
2.0 0.35 ug/L 12/28/22 13:24 11.0 UTetrachloroethene
2.0 0.25 ug/L 12/28/22 13:24 11.0 UToluene
2.0 0.34 ug/L 12/28/22 13:24 11.0 Utrans-1,2-Dichloroethene
2.0 0.23 ug/L 12/28/22 13:24 11.0 Utrans-1,3-Dichloropropene
5.0 0.53 ug/L 12/28/22 13:24 12.0 U1,2,4-Trichlorobenzene
1.0 0.21 ug/L 12/28/22 13:24 10.50 U1,1,1-Trichloroethane
2.0 0.32 ug/L 12/28/22 13:24 11.0 U1,1,2-Trichloroethane
1.0 0.20 ug/L 12/28/22 13:24 10.50 UTrichloroethene
2.0 0.33 ug/L 12/28/22 13:24 11.0 UTrichlorofluoromethane
1.0 0.23 ug/L 12/28/22 13:24 10.50 U1,1,2-Trichloro-1,2,2-trifluoroethane
2.0 0.40 ug/L 12/28/22 13:24 11.0 UVinyl chloride
2.0 0.49 ug/L 12/28/22 13:24 11.0 UXylenes, Total
20 5.0 ug/L 12/28/22 13:24 110U QPropionitrile
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-10Client Sample ID: DUP-TW-01
Matrix: WaterDate Collected: 12/14/22 16:00
Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
1.0 U Q 5.0 0.50 ug/L 12/28/22 13:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Pentachloroethane
2.5 0.78 ug/L 12/28/22 13:24 12.0 U QMethyl methacrylate
5.0 0.22 ug/L 12/28/22 13:24 11.0 UHexachlorobutadiene
2.0 0.34 ug/L 12/28/22 13:24 11.0 UDibromomethane
50 20 ug/L 12/28/22 13:24 140UAcetonitrile
10 2.4 ug/L 12/28/22 13:24 15.0 U QNaphthalene
20 3.9 ug/L 12/28/22 13:24 110U QIodomethane
5.0 1.1 ug/L 12/28/22 13:24 14.0 U3-Chloro-1-propene
50 5.5 ug/L 12/28/22 13:24 120UAcrylonitrile
2.0 0.33 ug/L 12/28/22 13:24 11.0 UEthyl methacrylate
2.0 0.36 ug/L 12/28/22 13:24 11.0 U1,1,1,2-Tetrachloroethane
10 1.3 ug/L 12/28/22 13:24 15.0 Utrans-1,4-Dichloro-2-butene
2.5 0.71 ug/L 12/28/22 13:24 12.0 U2-Chloro-1,3-butadiene
20 5.0 ug/L 12/28/22 13:24 110U QMethacrylonitrile
50 15 ug/L 12/28/22 13:24 140UAcrolein
2.0 0.48 ug/L 12/28/22 13:24 11.0 U1,2,3-Trichloropropane
2.5 0.69 ug/L 12/28/22 13:24 12.0 U QVinyl acetate
500 68 ug/L 12/28/22 13:24 1250U QIsobutyl alcohol
4.0 0.86 ug/L 12/28/22 13:24 12.0 U Q2-Nitropropane
100 25 ug/L 12/28/22 13:24 150U Qn-Butyl alcohol
2.0 0.34 ug/L 12/28/22 13:24 11.0 UBromochloromethane
5.0 0.37 ug/L 12/28/22 13:24 11.0 UDiethyl ether
10 2.1 ug/L 12/28/22 13:24 15.0 U QTetrahydrofuran
20 5.0 ug/L 12/28/22 13:24 110U QEthyl acetate
10 2.5 ug/L 12/28/22 13:24 15.0 U QBenzyl chloride
2.5 0.52 ug/L 12/28/22 13:24 12.0 Un-Butylbenzene
2.0 0.43 ug/L 12/28/22 13:24 11.0 U1,2,4-Trimethylbenzene
1.0 0.25 ug/L 12/28/22 13:24 10.50 U2-Chlorotoluene
5.0 0.50 ug/L 12/28/22 13:24 11.0 U Qn-Butyl acetate
2.0 0.37 ug/L 12/28/22 13:24 11.0 U1,2-Dichloroethene, Total
2.0 0.28 ug/L 12/28/22 13:24 11.0 U1,1-Dichloropropene
10 2.5 ug/L 12/28/22 13:24 15.0 U Q2-Methylnaphthalene
2.0 0.26 ug/L 12/28/22 13:24 11.0 Uo-Xylene
5.0 0.65 ug/L 12/28/22 13:24 12.0 UHexane
2.0 0.41 ug/L 12/28/22 13:24 11.0 U4-Chlorotoluene
5.0 1.1 ug/L 12/28/22 13:24 14.0 U M1-Chlorohexane
1.0 0.24 ug/L 12/28/22 13:24 10.50 UBromobenzene
5.0 0.81 ug/L 12/28/22 13:24 12.0 U Q1,2,3-Trichlorobenzene
2.0 0.48 ug/L 12/28/22 13:24 11.0 U1,3-Dichloropropene, Total
2.5 0.53 ug/L 12/28/22 13:24 12.0 Usec-Butylbenzene
2.0 0.35 ug/L 12/28/22 13:24 11.0 U2,2-Dichloropropane
2.0 0.41 ug/L 12/28/22 13:24 11.0 UN-Propylbenzene
10 2.5 ug/L 12/28/22 13:24 15.0 U1,3,5-Trichlorobenzene
10 0.70 ug/L 12/28/22 13:24 12.0 UDiisopropyl ether
200 50 ug/L 12/28/22 13:24 1100U QEthanol
100 25 ug/L 12/28/22 13:24 150U QIsopropyl alcohol
2.0 0.44 ug/L 12/28/22 13:24 11.0 Up-Cymene
2.5 0.78 ug/L 12/28/22 13:24 12.0 U QTert-amyl methyl ether
2.0 0.28 ug/L 12/28/22 13:24 11.0 U1,3,5-Trimethylbenzene
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Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-10Client Sample ID: DUP-TW-01
Matrix: WaterDate Collected: 12/14/22 16:00
Date Received: 12/15/22 09:00
Method: SW846 8260D - Volatile Organic Compounds (GC/MS) (Continued)
LOQ DL
5.0 U 10 2.5 ug/L 12/28/22 13:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2,3-Trimethylbenzene
2.0 0.49 ug/L 12/28/22 13:24 11.0 Um-Xylene & p-Xylene
2.0 0.50 ug/L 12/28/22 13:24 11.0 U QDichlorofluoromethane
2.0 0.43 ug/L 12/28/22 13:24 11.0 Utert-Butylbenzene
5.0 0.99 ug/L 12/28/22 13:24 12.0 UIsooctane
2.0 0.36 ug/L 12/28/22 13:24 11.0 U1,3-Dichloropropane
4-Bromofluorobenzene (Surr)101 85-114 12/28/22 13:24 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)105 12/28/22 13:24 180-119
1,2-Dichloroethane-d4 (Surr)87 12/28/22 13:24 181-118
Toluene-d8 (Surr)114 Q 12/28/22 13:24 189-112
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
LOQ DL
9.3 U 19 4.3 ug/L 12/20/22 11:44 12/23/22 21:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
19 4.2 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U1,2,4,5-Tetrachlorobenzene
19 3.2 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U1,2,4-Trichlorobenzene
9.3 2.3 ug/L 12/20/22 11:44 12/23/22 21:51 14.7 U1,2-Dichlorobenzene
19 3.4 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U1,2-Diphenylhydrazine
19 2.7 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U1,3-Dichlorobenzene
19 3.1 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U1,4-Dichlorobenzene
19 4.4 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U1-Methylnaphthalene
19 4.0 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U2,3,4,6-Tetrachlorophenol
19 3.1 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U2,4,5-Trichlorophenol
19 2.0 ug/L 12/20/22 11:44 12/23/22 21:51 14.7 U2,4,6-Trichlorophenol
19 3.4 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U2,4-Dichlorophenol
19 2.8 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U2,4-Dimethylphenol
47 15 ug/L 12/20/22 11:44 12/23/22 21:51 137U2,4-Dinitrophenol
9.3 2.1 ug/L 12/20/22 11:44 12/23/22 21:51 14.7 U2,4-Dinitrotoluene
9.3 2.2 ug/L 12/20/22 11:44 12/23/22 21:51 14.7 U2,6-Dichlorophenol
19 2.6 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U2,6-Dinitrotoluene
19 4.5 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U2-Chloronaphthalene
19 3.0 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U2-Chlorophenol
19 4.3 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U2-Methylnaphthalene
9.3 1.7 ug/L 12/20/22 11:44 12/23/22 21:51 13.7 U2-Methylphenol
19 2.7 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U2-Nitroaniline
19 3.6 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U2-Nitrophenol
9.3 1.3 ug/L 12/20/22 11:44 12/23/22 21:51 13.7 U3 & 4 Methylphenol
47 9.3 ug/L 12/20/22 11:44 12/23/22 21:51 119U Q3,3'-Dichlorobenzidine
47 2.8 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U3-Nitroaniline
47 4.9 ug/L 12/20/22 11:44 12/23/22 21:51 119U4,6-Dinitro-2-methylphenol
19 4.4 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U M4-Bromophenyl phenyl ether
19 2.3 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U4-Chloro-3-methylphenol
9.3 0.93 ug/L 12/20/22 11:44 12/23/22 21:51 13.7 U4-Chloroaniline
19 4.9 ug/L 12/20/22 11:44 12/23/22 21:51 111U4-Chlorophenyl phenyl ether
47 2.8 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U4-Nitroaniline
47 7.5 ug/L 12/20/22 11:44 12/23/22 21:51 119U4-Nitrophenol
19 4.1 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 UAcenaphthene
19 3.4 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 UAcenaphthylene
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Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-10Client Sample ID: DUP-TW-01
Matrix: WaterDate Collected: 12/14/22 16:00
Date Received: 12/15/22 09:00
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
LOQ DL
4.7 U 9.3 2.0 ug/L 12/20/22 11:44 12/23/22 21:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acetophenone
19 3.4 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 UAnthracene
9.3 2.0 ug/L 12/20/22 11:44 12/23/22 21:51 14.7 UAtrazine
19 3.4 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U QAzobenzene
19 4.5 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U MBenzaldehyde
19 3.9 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 UBenzo[a]anthracene
19 2.6 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U MBenzo[a]pyrene
19 2.9 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 UBenzo[b]fluoranthene
19 2.8 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 UBenzo[g,h,i]perylene
19 2.7 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 UBenzo[k]fluoranthene
19 2.4 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U MBenzyl alcohol
19 2.9 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 Ubis (2-chloroisopropyl) ether
9.3 1.7 ug/L 12/20/22 11:44 12/23/22 21:51 13.7 UBis(2-chloroethoxy)methane
19 3.4 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 UBis(2-chloroethyl)ether
19 2.8 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 UBis(2-ethylhexyl) phthalate
19 2.6 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 UButyl benzyl phthalate
19 2.6 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 UCaprolactam
9.3 1.7 ug/L 12/20/22 11:44 12/23/22 21:51 13.7 UCarbazole
19 3.5 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 UChrysene
19 2.8 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 UDibenz(a,h)anthracene
9.3 1.8 ug/L 12/20/22 11:44 12/23/22 21:51 13.7 UDibenzofuran
9.3 2.0 ug/L 12/20/22 11:44 12/23/22 21:51 14.7 UDiethyl phthalate
9.3 2.0 ug/L 12/20/22 11:44 12/23/22 21:51 14.7 UDimethyl phthalate
9.3 2.1 ug/L 12/20/22 11:44 12/23/22 21:51 14.7 UDi-n-butyl phthalate
19 2.6 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U MDi-n-octyl phthalate
9.3 2.3 ug/L 12/20/22 11:44 12/23/22 21:51 17.9 UDiphenylamine
9.3 1.5 ug/L 12/20/22 11:44 12/23/22 21:51 13.7 UFluoranthene
19 3.2 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 UFluorene
9.3 1.5 ug/L 12/20/22 11:44 12/23/22 21:51 13.7 UHexachlorobenzene
19 3.7 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 UHexachlorobutadiene
19 3.3 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 UHexachlorocyclopentadiene
19 3.4 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 UHexachloroethane
19 4.0 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 UIndeno[1,2,3-cd]pyrene
9.3 1.9 ug/L 12/20/22 11:44 12/23/22 21:51 13.7 UIsophorone
19 3.3 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 UNaphthalene
19 3.3 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 UNitrobenzene
9.3 2.2 ug/L 12/20/22 11:44 12/23/22 21:51 14.7 UN-Nitrosodi-n-propylamine
19 2.7 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U MN-Nitrosodiphenylamine
47 9.2 ug/L 12/20/22 11:44 12/23/22 21:51 119UPentachlorophenol
19 4.0 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 UPhenanthrene
9.3 1.4 ug/L 12/20/22 11:44 12/23/22 21:51 13.7 UPhenol
19 3.4 ug/L 12/20/22 11:44 12/23/22 21:51 19.3 U MPyrene
2-Fluorobiphenyl (Surr)56 44-119 12/20/22 11:44 12/23/22 21:51 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)25 12/20/22 11:44 12/23/22 21:51 119-119
Nitrobenzene-d5 (Surr)53 12/20/22 11:44 12/23/22 21:51 144-120
Phenol-d5 (Surr)16 12/20/22 11:44 12/23/22 21:51 110-130
Terphenyl-d14 (Surr)67 12/20/22 11:44 12/23/22 21:51 150-134
2,4,6-Tribromophenol (Surr)86 12/20/22 11:44 12/23/22 21:51 143-140
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-10Client Sample ID: DUP-TW-01
Matrix: WaterDate Collected: 12/14/22 16:00
Date Received: 12/15/22 09:00
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
40 U 100 20 ug/L 01/18/23 06:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
LOQ DL
2.0 U 5.0 1.0 ug/L 12/28/22 14:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Benzene
100 25 ug/L 12/28/22 14:32 150U MC5-C8 Aliphatics
100 10 ug/L 12/28/22 14:32 120UC9-C10 Aromatics
100 25 ug/L 12/28/22 14:32 150U MC9-C12 Aliphatics
5.0 1.0 ug/L 12/28/22 14:32 12.0 UEthylbenzene
5.0 1.0 ug/L 12/28/22 14:32 12.0 U QMethyl tert-butyl ether
6.0 2.0 ug/L 12/28/22 14:32 14.0 UNaphthalene
5.0 1.0 ug/L 12/28/22 14:32 12.0 UToluene
100 25 ug/L 12/28/22 14:32 150UC9-C12 Aliphatics (adjusted)
10 2.5 ug/L 12/28/22 14:32 15.0 Um-Xylene & p-Xylene
5.0 1.0 ug/L 12/28/22 14:32 12.0 Uo-Xylene
100 25 ug/L 12/28/22 14:32 150UC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)102 M 70-130 12/28/22 14:32 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)92 M 12/28/22 14:32 170-130
Method: SW846 8081B 8082A - Organochlorine Pesticides & PCBs (GC)
LOQ DL
0.0037 U 0.047 0.0019 ug/L 12/21/22 13:43 12/22/22 19:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,4'-DDD
0.047 0.00094 ug/L 12/21/22 13:43 12/22/22 19:10 10.0037 U4,4'-DDE
0.047 0.00094 ug/L 12/21/22 13:43 12/22/22 19:10 10.0037 U Q4,4'-DDT
0.047 0.0019 ug/L 12/21/22 13:43 12/22/22 19:10 10.0037 U MAldrin
0.047 0.00094 ug/L 12/21/22 13:43 12/22/22 19:10 10.0037 Ualpha-BHC
0.047 0.0019 ug/L 12/21/22 13:43 12/22/22 19:10 10.0037 Ubeta-BHC
0.047 0.0019 ug/L 12/21/22 13:43 12/22/22 19:10 10.0037 Udelta-BHC
0.047 0.0019 ug/L 12/21/22 13:43 12/22/22 19:10 10.0037 UDieldrin
0.047 0.0019 ug/L 12/21/22 13:43 12/22/22 19:10 10.0037 U MEndosulfan I
0.047 0.0019 ug/L 12/21/22 13:43 12/22/22 19:10 10.0037 UEndosulfan II
0.047 0.0019 ug/L 12/21/22 13:43 12/22/22 19:10 10.0037 UEndosulfan sulfate
0.047 0.00094 ug/L 12/21/22 13:43 12/22/22 19:10 10.0037 UEndrin
0.047 0.0037 ug/L 12/21/22 13:43 12/22/22 19:10 10.015 UEndrin aldehyde
0.047 0.0037 ug/L 12/21/22 13:43 12/22/22 19:10 10.015 U QEndrin ketone
0.047 0.00094 ug/L 12/21/22 13:43 12/22/22 19:10 10.0037 U Mgamma-BHC (Lindane)
0.047 0.00094 ug/L 12/21/22 13:43 12/22/22 19:10 10.0037 UHeptachlor
0.047 0.0019 ug/L 12/21/22 13:43 12/22/22 19:10 10.0037 UHeptachlor epoxide
0.047 0.0019 ug/L 12/21/22 13:43 12/22/22 19:10 10.0037 UMethoxychlor
0.47 0.15 ug/L 12/21/22 13:43 12/22/22 19:10 10.37 U M QChlordane (technical)
0.94 0.30 ug/L 12/21/22 13:43 12/22/22 19:10 10.67 UPCB-1016
0.94 0.32 ug/L 12/21/22 13:43 12/22/22 19:10 10.67 UPCB-1221
0.94 0.32 ug/L 12/21/22 13:43 12/22/22 19:10 10.67 UPCB-1232
0.94 0.32 ug/L 12/21/22 13:43 12/22/22 19:10 10.67 UPCB-1242
0.94 0.32 ug/L 12/21/22 13:43 12/22/22 19:10 10.67 UPCB-1248
0.94 0.32 ug/L 12/21/22 13:43 12/22/22 19:10 10.67 UPCB-1254
0.94 0.32 ug/L 12/21/22 13:43 12/22/22 19:10 10.67 U MPCB-1260
4.7 0.29 ug/L 12/21/22 13:43 12/22/22 19:10 10.75 U MToxaphene
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Client Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-10Client Sample ID: DUP-TW-01
Matrix: WaterDate Collected: 12/14/22 16:00
Date Received: 12/15/22 09:00
DCB Decachlorobiphenyl 44 14-130 12/21/22 13:43 12/22/22 19:10 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene (Surr)61 12/21/22 13:43 12/22/22 19:10 144-124
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
LOQ DL
1.1 U 1.9 0.57 ug/L 12/19/22 18:32 12/23/22 00:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Anthracene
11 4.8 ug/L 12/19/22 18:32 12/23/22 00:56 19.5 UPyrene
1.9 0.57 ug/L 12/19/22 18:32 12/23/22 00:56 11.1 UBenzo[g,h,i]perylene
1.9 0.57 ug/L 12/19/22 18:32 12/23/22 00:56 11.1 UIndeno[1,2,3-cd]pyrene
1.9 0.57 ug/L 12/19/22 18:32 12/23/22 00:56 11.1 UBenzo[b]fluoranthene
1.9 0.48 ug/L 12/19/22 18:32 12/23/22 00:56 10.95 UFluoranthene
3.8 1.4 ug/L 12/19/22 18:32 12/23/22 00:56 12.9 UBenzo[k]fluoranthene
1.9 0.67 ug/L 12/19/22 18:32 12/23/22 00:56 11.3 UAcenaphthylene
1.9 0.48 ug/L 12/19/22 18:32 12/23/22 00:56 10.95 UChrysene
1.9 0.57 ug/L 12/19/22 18:32 12/23/22 00:56 11.8 JBenzo[a]pyrene
1.9 0.48 ug/L 12/19/22 18:32 12/23/22 00:56 10.95 UDibenz(a,h)anthracene
1.9 0.67 ug/L 12/19/22 18:32 12/23/22 00:56 11.3 UBenzo[a]anthracene
1.9 0.57 ug/L 12/19/22 18:32 12/23/22 00:56 11.1 UAcenaphthene
1.9 0.57 ug/L 12/19/22 18:32 12/23/22 00:56 11.1 UPhenanthrene
1.9 0.57 ug/L 12/19/22 18:32 12/23/22 00:56 11.1 UFluorene
1.9 0.57 ug/L 12/19/22 18:32 12/23/22 00:56 11.1 UNaphthalene
1.9 0.57 ug/L 12/19/22 18:32 12/23/22 00:56 11.1 U2-Methylnaphthalene
38 9.5 ug/L 12/19/22 18:32 12/23/22 00:56 129UC11-C22 Aromatics (unadjusted)
38 9.5 ug/L 12/19/22 18:32 12/23/22 00:56 129UC11-C22 Aromatics (Adjusted)
48 9.5 ug/L 12/19/22 18:32 12/23/22 00:56 119U MC19-C36 Aliphatics
29 9.5 ug/L 12/19/22 18:32 12/23/22 00:56 128JC9-C18 Aliphatics
1-Chlorooctadecane (Surr)22 Q 40-140 12/19/22 18:32 12/23/22 00:56 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)84 12/19/22 18:32 12/23/22 00:56 140-140
o- terphenyl (Surr)69 12/19/22 18:32 12/23/22 00:56 140-140
Method: SW846 7199 - Chromium, Hexavalent (IC) - Dissolved
LOQ DL
9.0 U H 10 5.0 ug/L 12/28/22 18:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Chromium (hexavalent)
10 5.0 ug/L 12/28/22 18:26 19.0 U HChromium (hexavalent)
Method: SW846 6020B - Metals (ICP/MS) - Total Recoverable
LOQ DL
1.0 U 2.0 0.39 ug/L 12/16/22 06:22 12/16/22 19:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Silver
200 35 ug/L 12/16/22 06:22 12/16/22 19:02 1570Aluminum
5.0 0.86 ug/L 12/16/22 06:22 12/16/22 19:02 13.0 UArsenic
5.0 0.89 ug/L 12/16/22 06:22 12/16/22 19:02 118Barium
0.50 0.20 ug/L 12/16/22 06:22 12/16/22 19:02 10.40 UBeryllium
500 140 ug/L 12/16/22 06:22 12/16/22 19:02 118000Calcium
0.50 0.078 ug/L 12/16/22 06:22 12/16/22 19:02 10.20 UCadmium
1.0 0.22 ug/L 12/16/22 06:22 12/16/22 19:02 12.7Cobalt
20 2.6 ug/L 12/16/22 06:22 12/16/22 19:02 14.5 JChromium
5.0 0.90 ug/L 12/16/22 06:22 12/16/22 19:02 14.5 JCopper
100 26 ug/L 12/16/22 06:22 12/16/22 19:02 15300Iron
1000 160 ug/L 12/16/22 06:22 12/16/22 19:02 12400Potassium
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Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Lab Sample ID: 680-227663-10Client Sample ID: DUP-TW-01
Matrix: WaterDate Collected: 12/14/22 16:00
Date Received: 12/15/22 09:00
Method: SW846 6020B - Metals (ICP/MS) - Total Recoverable (Continued)
LOQ DL
1100 250 23 ug/L 12/16/22 06:22 12/16/22 19:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Magnesium
10 2.2 ug/L 12/16/22 06:22 12/16/22 19:02 1420Manganese
1000 200 ug/L 12/16/22 06:22 12/16/22 19:02 111000Sodium
2.5 0.34 ug/L 12/16/22 06:22 12/16/22 19:02 10.36 JLead
5.0 1.2 ug/L 12/16/22 06:22 12/16/22 19:02 12.5 USelenium
10 1.8 ug/L 12/16/22 06:22 12/16/22 19:02 13.8 JNickel
5.0 0.52 ug/L 12/16/22 06:22 12/16/22 19:02 11.5 UAntimony
2.0 0.26 ug/L 12/16/22 06:22 12/16/22 19:02 11.0 UThallium
25 10 ug/L 12/16/22 06:22 12/16/22 19:02 111JZinc
10 1.8 ug/L 12/16/22 06:22 12/16/22 19:02 15.0 UVanadium
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8260D - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-756853/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756853
LOQ DL
Acetone 25 U 50 11 ug/Kg 12/27/22 15:46 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
5.0 U 2.410 ug/Kg 12/27/22 15:46 1Benzene
5.0 U 2.210 ug/Kg 12/27/22 15:46 1Bromoform
5.0 U 2.410 ug/Kg 12/27/22 15:46 1Bromomethane
20 U 9.225 ug/Kg 12/27/22 15:46 12-Butanone (MEK)
5.0 U 2.110 ug/Kg 12/27/22 15:46 1Carbon disulfide
5.0 U 2.110 ug/Kg 12/27/22 15:46 1Carbon tetrachloride
4.0 U 1.45.0 ug/Kg 12/27/22 15:46 1Chlorobenzene
5.0 U 2.110 ug/Kg 12/27/22 15:46 1Chlorodibromomethane
8.0 U 2.210 ug/Kg 12/27/22 15:46 1Chloroethane
4.0 U 2.05.0 ug/Kg 12/27/22 15:46 1Chloroform
5.0 U 2.410 ug/Kg 12/27/22 15:46 1Chloromethane
8.0 U 2.910 ug/Kg 12/27/22 15:46 1cis-1,2-Dichloroethene
5.0 U 2.210 ug/Kg 12/27/22 15:46 1cis-1,3-Dichloropropene
5.0 U 2.310 ug/Kg 12/27/22 15:46 1Cyclohexane
4.0 U 1.610 ug/Kg 12/27/22 15:46 11,2-Dibromo-3-Chloropropane
4.0 U 1.75.0 ug/Kg 12/27/22 15:46 11,2-Dichlorobenzene
4.0 U 2.05.0 ug/Kg 12/27/22 15:46 11,3-Dichlorobenzene
4.0 U 1.85.0 ug/Kg 12/27/22 15:46 11,4-Dichlorobenzene
4.0 U 2.05.0 ug/Kg 12/27/22 15:46 1Dichlorobromomethane
8.0 U 3.210 ug/Kg 12/27/22 15:46 1Dichlorodifluoromethane
5.0 U 2.910 ug/Kg 12/27/22 15:46 11,1-Dichloroethane
5.0 U 2.310 ug/Kg 12/27/22 15:46 11,2-Dichloroethane
4.0 U 3.65.0 ug/Kg 12/27/22 15:46 11,1-Dichloroethene
8.0 U 2.610 ug/Kg 12/27/22 15:46 11,2-Dichloropropane
4.0 U 1.75.0 ug/Kg 12/27/22 15:46 11,2-Dibromoethane (EDB)
5.0 U 2.110 ug/Kg 12/27/22 15:46 1Ethylbenzene
40 U 1950 ug/Kg 12/27/22 15:46 12-Hexanone
5.0 U 2.210 ug/Kg 12/27/22 15:46 1Isopropylbenzene
16 U 8.125 ug/Kg 12/27/22 15:46 1Methyl acetate
4.0 U 2.05.0 ug/Kg 12/27/22 15:46 1Methylcyclohexane
25 U 8.050 ug/Kg 12/27/22 15:46 1Methylene Chloride
40 U 18100 ug/Kg 12/27/22 15:46 14-Methyl-2-pentanone (MIBK)
5.0 U 2.210 ug/Kg 12/27/22 15:46 1Methyl tert-butyl ether
4.0 U 1.95.0 ug/Kg 12/27/22 15:46 1Styrene
4.0 U 2.15.0 ug/Kg 12/27/22 15:46 11,1,2,2-Tetrachloroethane
8.0 U 2.610 ug/Kg 12/27/22 15:46 1Tetrachloroethene
10 U 2.620 ug/Kg 12/27/22 15:46 1Toluene
5.0 U 2.310 ug/Kg 12/27/22 15:46 1trans-1,2-Dichloroethene
10 U 2.620 ug/Kg 12/27/22 15:46 1trans-1,3-Dichloropropene
5.0 U 2.510 ug/Kg 12/27/22 15:46 11,2,4-Trichlorobenzene
5.0 U 2.610 ug/Kg 12/27/22 15:46 11,1,1-Trichloroethane
4.0 U 1.55.0 ug/Kg 12/27/22 15:46 11,1,2-Trichloroethane
4.0 U 1.85.0 ug/Kg 12/27/22 15:46 1Trichloroethene
8.0 U 3.110 ug/Kg 12/27/22 15:46 1Trichlorofluoromethane
4.0 U 2.95.0 ug/Kg 12/27/22 15:46 11,1,2-Trichloro-1,2,2-trifluoroethane
8.0 U 2.810 ug/Kg 12/27/22 15:46 1Vinyl chloride
10 U 3.620 ug/Kg 12/27/22 15:46 1Xylenes, Total
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-756853/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756853
LOQ DL
Propionitrile 50 U 50 26 ug/Kg 12/27/22 15:46 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
10 U 6.310 ug/Kg 12/27/22 15:46 1Pentachloroethane
10 U 4.510 ug/Kg 12/27/22 15:46 1Methyl methacrylate
10 U 4.120 ug/Kg 12/27/22 15:46 1Hexachlorobutadiene
4.0 U 2.05.0 ug/Kg 12/27/22 15:46 1Dibromomethane
50 U 4150 ug/Kg 12/27/22 15:46 1Acetonitrile
8.0 U 3.110 ug/Kg 12/27/22 15:46 1Naphthalene
5.0 U 1.710 ug/Kg 12/27/22 15:46 1Iodomethane
8.0 U 3.510 ug/Kg 12/27/22 15:46 13-Chloro-1-propene
100 U 30200 ug/Kg 12/27/22 15:46 1Acrylonitrile
10 U 2.820 ug/Kg 12/27/22 15:46 1Ethyl methacrylate
5.0 U 1.310 ug/Kg 12/27/22 15:46 11,1,1,2-Tetrachloroethane
5.0 U 2.410 ug/Kg 12/27/22 15:46 1trans-1,4-Dichloro-2-butene
5.0 U 2.15.0 ug/Kg 12/27/22 15:46 12-Chloro-1,3-butadiene
50 U 2350 ug/Kg 12/27/22 15:46 1Methacrylonitrile
160 U 74200 ug/Kg 12/27/22 15:46 1Acrolein
5.0 U 1.810 ug/Kg 12/27/22 15:46 11,2,3-Trichloropropane
20 U 5.540 ug/Kg 12/27/22 15:46 1Vinyl acetate
200 U 93500 ug/Kg 12/27/22 15:46 1Isobutyl alcohol
10 U 1010 ug/Kg 12/27/22 15:46 12-Nitropropane
130 U 130130 ug/Kg 12/27/22 15:46 1n-Butyl alcohol
4.0 U 2.05.0 ug/Kg 12/27/22 15:46 1Bromochloromethane
8.0 U 2.610 ug/Kg 12/27/22 15:46 1Diethyl ether
18 U 6.220 ug/Kg 12/27/22 15:46 1Tetrahydrofuran
10 U 1010 ug/Kg 12/27/22 15:46 1Ethyl acetate
5.0 U 5.05.0 ug/Kg 12/27/22 15:46 1Benzyl chloride
5.0 U 1.910 ug/Kg 12/27/22 15:46 1n-Butylbenzene
5.0 U 2.510 ug/Kg 12/27/22 15:46 11,2,4-Trimethylbenzene
5.0 U 2.310 ug/Kg 12/27/22 15:46 12-Chlorotoluene
5.0 U 5.05.0 ug/Kg 12/27/22 15:46 1n-Butyl acetate
8.0 U 3.110 ug/Kg 12/27/22 15:46 11,2-Dichloroethene, Total
4.0 U 2.05.0 ug/Kg 12/27/22 15:46 11,1-Dichloropropene
5.0 U 5.05.0 ug/Kg 12/27/22 15:46 12-Methylnaphthalene
5.0 U 2.310 ug/Kg 12/27/22 15:46 1o-Xylene
4.0 U 1.75.0 ug/Kg 12/27/22 15:46 1Hexane
5.0 U 2.110 ug/Kg 12/27/22 15:46 14-Chlorotoluene
5.0 U 2.15.0 ug/Kg 12/27/22 15:46 11-Chlorohexane
4.0 U 1.75.0 ug/Kg 12/27/22 15:46 1Bromobenzene
4.0 U 2.05.0 ug/Kg 12/27/22 15:46 11,2,3-Trichlorobenzene
10 U 4.720 ug/Kg 12/27/22 15:46 11,3-Dichloropropene, Total
5.0 U 2.010 ug/Kg 12/27/22 15:46 1sec-Butylbenzene
5.0 U 2.210 ug/Kg 12/27/22 15:46 12,2-Dichloropropane
5.0 U 2.210 ug/Kg 12/27/22 15:46 1N-Propylbenzene
5.0 U 5.05.0 ug/Kg 12/27/22 15:46 11,3,5-Trichlorobenzene
10 U 1.510 ug/Kg 12/27/22 15:46 1Diisopropyl ether
250 U 250250 ug/Kg 12/27/22 15:46 1Ethanol
50 U 5050 ug/Kg 12/27/22 15:46 1Isopropyl alcohol
10 U 2.620 ug/Kg 12/27/22 15:46 1p-Cymene
5.0 U 5.05.0 ug/Kg 12/27/22 15:46 1Tert-amyl methyl ether
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-756853/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756853
LOQ DL
1,3,5-Trimethylbenzene 5.0 U 10 2.4 ug/Kg 12/27/22 15:46 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
5.0 U 5.05.0 ug/Kg 12/27/22 15:46 11,2,3-Trimethylbenzene
5.0 U 2.210 ug/Kg 12/27/22 15:46 1m-Xylene & p-Xylene
8.0 U 2.410 ug/Kg 12/27/22 15:46 1Dichlorofluoromethane
5.0 U 2.510 ug/Kg 12/27/22 15:46 1tert-Butylbenzene
5.0 U 5.05.0 ug/Kg 12/27/22 15:46 1Isooctane
5.0 U 2.210 ug/Kg 12/27/22 15:46 11,3-Dichloropropane
4-Bromofluorobenzene (Surr)90 79-119 12/27/22 15:46 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
103 12/27/22 15:46 1Dibromofluoromethane (Surr)78-119
92 12/27/22 15:46 11,2-Dichloroethane-d4 (Surr)71-138
106 12/27/22 15:46 1Toluene-d8 (Surr)85-116
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-756853/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756853
Acetone 250 199 ug/Kg 80 36 -164
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Benzene 50.0 53.6 ug/Kg 107 77 -121
Bromoform 50.0 53.3 ug/Kg 107 67 -132
Bromomethane 50.0 58.8 ug/Kg 118 53 -143
2-Butanone (MEK)250 188 ug/Kg 75 51 -148
Carbon disulfide 50.0 61.5 ug/Kg 123 63 -132
Carbon tetrachloride 50.0 54.8 ug/Kg 110 70 -135
Chlorobenzene 50.0 56.6 ug/Kg 113 79 -120
Chlorodibromomethane 50.0 53.2 ug/Kg 106 74 -126
Chloroethane 50.0 56.1 ug/Kg 112 59 -139
Chloroform 50.0 50.8 ug/Kg 102 78 -123
Chloromethane 50.0 39.3 ug/Kg 79 50 -136
cis-1,2-Dichloroethene 50.0 51.1 ug/Kg 102 77 -123
cis-1,3-Dichloropropene 50.0 51.7 ug/Kg 103 74 -126
Cyclohexane 50.0 57.0 ug/Kg 114 67 -131
1,2-Dibromo-3-Chloropropane 50.0 43.9 ug/Kg 88 61 -132
1,2-Dichlorobenzene 50.0 52.5 ug/Kg 105 78 -121
1,3-Dichlorobenzene 50.0 53.8 ug/Kg 108 77 -121
1,4-Dichlorobenzene 50.0 53.0 ug/Kg 106 75 -120
Dichlorobromomethane 50.0 49.2 ug/Kg 98 75 -127
Dichlorodifluoromethane 50.0 43.8 ug/Kg 88 29 -149
1,1-Dichloroethane 50.0 50.9 ug/Kg 102 76 -125
1,2-Dichloroethane 50.0 49.3 ug/Kg 99 73 -128
1,1-Dichloroethene 50.0 57.9 ug/Kg 116 70 -131
1,2-Dichloropropane 50.0 49.8 ug/Kg 100 76 -123
1,2-Dibromoethane (EDB)50.0 53.6 ug/Kg 107 72 -129
Ethylbenzene 50.0 55.0 ug/Kg 110 76 -122
2-Hexanone 250 189 ug/Kg 75 53 -145
Isopropylbenzene 50.0 57.4 ug/Kg 115 68 -134
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-756853/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756853
Methyl acetate 100 93.3 ug/Kg 93 53 -144
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Methylcyclohexane 50.0 55.9 ug/Kg 112 66 -133
Methylene Chloride 50.0 54.9 ug/Kg 110 70 -128
4-Methyl-2-pentanone (MIBK)250 195 ug/Kg 78 65 -135
Methyl tert-butyl ether 50.0 48.0 ug/Kg 96 73 -125
Styrene 50.0 56.8 ug/Kg 114 76 -124
1,1,2,2-Tetrachloroethane 50.0 47.5 ug/Kg 95 70 -124
Tetrachloroethene 50.0 61.7 ug/Kg 123 73 -128
Toluene 50.0 55.3 ug/Kg 111 77 -121
trans-1,2-Dichloroethene 50.0 55.3 ug/Kg 111 74 -125
trans-1,3-Dichloropropene 50.0 50.8 ug/Kg 102 71 -130
1,2,4-Trichlorobenzene 50.0 53.8 ug/Kg 108 67 -129
1,1,1-Trichloroethane 50.0 52.3 ug/Kg 105 73 -130
1,1,2-Trichloroethane 50.0 47.9 ug/Kg 96 78 -121
Trichloroethene 50.0 57.2 ug/Kg 114 77 -123
Trichlorofluoromethane 50.0 60.3 ug/Kg 121 62 -140
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 61.4 ug/Kg 123 66 -136
Vinyl chloride 50.0 54.9 ug/Kg 110 56 -135
Xylenes, Total 100 110 ug/Kg 110 78 -124
Hexachlorobutadiene 50.0 56.3 ug/Kg 113 61 -135
Dibromomethane 50.0 53.6 ug/Kg 107 78 -125
Naphthalene 50.0 45.3 ug/Kg 91 62 -129
Iodomethane 50.0 63.8 ug/Kg 128 71 -131
3-Chloro-1-propene 50.0 58.1 ug/Kg 116 68 -135
Acrylonitrile 500 437 ug/Kg 87 65 -134
Ethyl methacrylate 50.0 46.0 ug/Kg 92 69 -129
1,1,1,2-Tetrachloroethane 50.0 56.3 ug/Kg 113 78 -125
trans-1,4-Dichloro-2-butene 50.0 43.4 ug/Kg 87 62 -136
Acrolein 1000 812 ug/Kg 81 47 -155
1,2,3-Trichloropropane 50.0 50.5 ug/Kg 101 73 -125
Vinyl acetate 100 73.6 ug/Kg 74 50 -151
Isobutyl alcohol 1250 858 ug/Kg 69 60 -135
Bromochloromethane 50.0 59.7 ug/Kg 119 78 -125
Diethyl ether 50.0 47.8 ug/Kg 96 71 -129
Tetrahydrofuran 100 73.1 ug/Kg 73 61 -135
n-Butylbenzene 50.0 49.9 ug/Kg 100 70 -128
1,2,4-Trimethylbenzene 50.0 57.2 ug/Kg 114 75 -123
2-Chlorotoluene 50.0 54.3 ug/Kg 109 75 -122
1,2-Dichloroethene, Total 100 106 ug/Kg 106 78 -122
1,1-Dichloropropene 50.0 53.2 ug/Kg 106 76 -125
o-Xylene 50.0 55.6 ug/Kg 111 77 -123
Hexane 50.0 54.0 ug/Kg 108 45 -142
4-Chlorotoluene 50.0 55.9 ug/Kg 112 72 -124
Bromobenzene 50.0 59.6 ug/Kg 119 78 -121
1,2,3-Trichlorobenzene 50.0 50.3 ug/Kg 101 66 -130
1,3-Dichloropropene, Total 100 102 ug/Kg 102 77 -126
sec-Butylbenzene 50.0 58.1 ug/Kg 116 73 -126
2,2-Dichloropropane 50.0 54.2 ug/Kg 108 67 -133
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-756853/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756853
N-Propylbenzene 50.0 55.9 ug/Kg 112 73 -125
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
p-Cymene 50.0 51.5 ug/Kg 103 73 -127
1,3,5-Trimethylbenzene 50.0 57.6 ug/Kg 115 73 -124
m-Xylene & p-Xylene 50.0 54.7 ug/Kg 109 77 -124
Dichlorofluoromethane 50.0 49.7 ug/Kg 99
tert-Butylbenzene 50.0 58.4 ug/Kg 117 73 -125
1,3-Dichloropropane 50.0 50.8 ug/Kg 102 77 -121
4-Bromofluorobenzene (Surr)79 -119
Surrogate
98
LCS LCS
Qualifier Limits%Recovery
108Dibromofluoromethane (Surr)78 -119
951,2-Dichloroethane-d4 (Surr)71 -138
107Toluene-d8 (Surr)85 -116
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-756853/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756853
Acetone 250 197 ug/Kg 79 36 -164 1 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Benzene 50.0 53.6 ug/Kg 107 77 -121 0 20
Bromoform 50.0 54.1 ug/Kg 108 67 -132 1 20
Bromomethane 50.0 59.0 ug/Kg 118 53 -143 0 20
2-Butanone (MEK)250 188 ug/Kg 75 51 -148 0 20
Carbon disulfide 50.0 60.1 ug/Kg 120 63 -132 2 20
Carbon tetrachloride 50.0 55.0 ug/Kg 110 70 -135 0 20
Chlorobenzene 50.0 57.0 ug/Kg 114 79 -120 1 20
Chlorodibromomethane 50.0 52.8 ug/Kg 106 74 -126 1 20
Chloroethane 50.0 55.7 ug/Kg 111 59 -139 1 20
Chloroform 50.0 50.8 ug/Kg 102 78 -123 0 20
Chloromethane 50.0 39.1 ug/Kg 78 50 -136 1 20
cis-1,2-Dichloroethene 50.0 50.9 ug/Kg 102 77 -123 0 20
cis-1,3-Dichloropropene 50.0 51.9 ug/Kg 104 74 -126 0 20
Cyclohexane 50.0 55.5 ug/Kg 111 67 -131 3 20
1,2-Dibromo-3-Chloropropane 50.0 43.4 ug/Kg 87 61 -132 1 20
1,2-Dichlorobenzene 50.0 52.8 ug/Kg 106 78 -121 1 20
1,3-Dichlorobenzene 50.0 54.0 ug/Kg 108 77 -121 0 20
1,4-Dichlorobenzene 50.0 53.2 ug/Kg 106 75 -120 0 20
Dichlorobromomethane 50.0 49.8 ug/Kg 100 75 -127 1 20
Dichlorodifluoromethane 50.0 43.0 ug/Kg 86 29 -149 2 20
1,1-Dichloroethane 50.0 51.1 ug/Kg 102 76 -125 0 20
1,2-Dichloroethane 50.0 50.2 ug/Kg 100 73 -128 2 20
1,1-Dichloroethene 50.0 54.3 ug/Kg 109 70 -131 6 20
1,2-Dichloropropane 50.0 49.6 ug/Kg 99 76 -123 0 20
1,2-Dibromoethane (EDB)50.0 54.2 ug/Kg 108 72 -129 1 20
Ethylbenzene 50.0 55.1 ug/Kg 110 76 -122 0 20
2-Hexanone 250 190 ug/Kg 76 53 -145 1 20
Isopropylbenzene 50.0 57.0 ug/Kg 114 68 -134 1 20
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-756853/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756853
Methyl acetate 100 92.7 ug/Kg 93 53 -144 1 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Methylcyclohexane 50.0 53.9 ug/Kg 108 66 -133 4 20
Methylene Chloride 50.0 55.6 ug/Kg 111 70 -128 1 20
4-Methyl-2-pentanone (MIBK)250 196 ug/Kg 78 65 -135 0 20
Methyl tert-butyl ether 50.0 49.6 ug/Kg 99 73 -125 3 20
Styrene 50.0 57.8 ug/Kg 116 76 -124 2 20
1,1,2,2-Tetrachloroethane 50.0 47.3 ug/Kg 95 70 -124 0 20
Tetrachloroethene 50.0 61.3 ug/Kg 123 73 -128 1 20
Toluene 50.0 55.2 ug/Kg 110 77 -121 0 20
trans-1,2-Dichloroethene 50.0 55.8 ug/Kg 112 74 -125 1 20
trans-1,3-Dichloropropene 50.0 51.4 ug/Kg 103 71 -130 1 20
1,2,4-Trichlorobenzene 50.0 53.7 ug/Kg 107 67 -129 0 20
1,1,1-Trichloroethane 50.0 51.9 ug/Kg 104 73 -130 1 20
1,1,2-Trichloroethane 50.0 48.0 ug/Kg 96 78 -121 0 20
Trichloroethene 50.0 57.0 ug/Kg 114 77 -123 0 20
Trichlorofluoromethane 50.0 59.4 ug/Kg 119 62 -140 1 20
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 61.1 ug/Kg 122 66 -136 0 20
Vinyl chloride 50.0 53.7 ug/Kg 107 56 -135 2 20
Xylenes, Total 100 111 ug/Kg 111 78 -124 1 20
Hexachlorobutadiene 50.0 55.7 ug/Kg 111 61 -135 1 20
Dibromomethane 50.0 54.1 ug/Kg 108 78 -125 1 20
Naphthalene 50.0 45.3 ug/Kg 91 62 -129 0 20
Iodomethane 50.0 63.5 ug/Kg 127 71 -131 1 20
3-Chloro-1-propene 50.0 58.2 ug/Kg 116 68 -135 0 20
Acrylonitrile 500 435 ug/Kg 87 65 -134 0 20
Ethyl methacrylate 50.0 46.2 ug/Kg 92 69 -129 1 20
1,1,1,2-Tetrachloroethane 50.0 56.7 ug/Kg 113 78 -125 1 20
trans-1,4-Dichloro-2-butene 50.0 43.5 ug/Kg 87 62 -136 0 20
Acrolein 1000 828 ug/Kg 83 47 -155 2 20
1,2,3-Trichloropropane 50.0 50.0 ug/Kg 100 73 -125 1 20
Vinyl acetate 100 72.1 ug/Kg 72 50 -151 2 20
Isobutyl alcohol 1250 858 ug/Kg 69 60 -135 0 20
Bromochloromethane 50.0 59.3 ug/Kg 119 78 -125 1 20
Diethyl ether 50.0 48.4 ug/Kg 97 71 -129 1 20
Tetrahydrofuran 100 72.8 ug/Kg 73 61 -135 0 20
n-Butylbenzene 50.0 49.3 ug/Kg 99 70 -128 1 20
1,2,4-Trimethylbenzene 50.0 57.4 ug/Kg 115 75 -123 0 20
2-Chlorotoluene 50.0 54.6 ug/Kg 109 75 -122 1 20
1,2-Dichloroethene, Total 100 107 ug/Kg 107 78 -122 0 20
1,1-Dichloropropene 50.0 53.0 ug/Kg 106 76 -125 0 20
o-Xylene 50.0 56.0 ug/Kg 112 77 -123 1 20
Hexane 50.0 52.2 ug/Kg 104 45 -142 3 20
4-Chlorotoluene 50.0 56.1 ug/Kg 112 72 -124 0 20
Bromobenzene 50.0 60.4 ug/Kg 121 78 -121 1 20
1,2,3-Trichlorobenzene 50.0 50.8 ug/Kg 102 66 -130 1 20
1,3-Dichloropropene, Total 100 103 ug/Kg 103 77 -126 1 20
sec-Butylbenzene 50.0 56.8 ug/Kg 114 73 -126 2 20
2,2-Dichloropropane 50.0 53.9 ug/Kg 108 67 -133 1 20
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-756853/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756853
N-Propylbenzene 50.0 55.4 ug/Kg 111 73 -125 1 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
p-Cymene 50.0 51.1 ug/Kg 102 73 -127 1 20
1,3,5-Trimethylbenzene 50.0 57.1 ug/Kg 114 73 -124 1 20
m-Xylene & p-Xylene 50.0 55.3 ug/Kg 111 77 -124 1 20
Dichlorofluoromethane 50.0 49.5 ug/Kg 99 1
tert-Butylbenzene 50.0 58.0 ug/Kg 116 73 -125 1 20
1,3-Dichloropropane 50.0 51.4 ug/Kg 103 77 -121 1 20
4-Bromofluorobenzene (Surr)79 -119
Surrogate
97
LCSD LCSD
Qualifier Limits%Recovery
109Dibromofluoromethane (Surr)78 -119
1031,2-Dichloroethane-d4 (Surr)71 -138
108Toluene-d8 (Surr)85 -116
Client Sample ID: Method BlankLab Sample ID: MB 680-757008/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 757008
LOQ DL
Acetone 10 U 25 3.7 ug/L 12/28/22 12:05 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
1.0 U M 0.272.0 ug/L 12/28/22 12:05 1Benzene
2.0 U 0.592.5 ug/L 12/28/22 12:05 1Bromoform
10 U 3.720 ug/L 12/28/22 12:05 1Bromomethane
20 U 6.425 ug/L 12/28/22 12:05 12-Butanone (MEK)
1.0 U 0.432.0 ug/L 12/28/22 12:05 1Carbon disulfide
1.0 U 0.302.0 ug/L 12/28/22 12:05 1Carbon tetrachloride
0.50 U 0.151.0 ug/L 12/28/22 12:05 1Chlorobenzene
1.0 U 0.392.0 ug/L 12/28/22 12:05 1Chlorodibromomethane
10 U 4.620 ug/L 12/28/22 12:05 1Chloroethane
1.0 U 0.272.0 ug/L 12/28/22 12:05 1Chloroform
2.0 U 0.542.5 ug/L 12/28/22 12:05 1Chloromethane
1.0 U 0.252.0 ug/L 12/28/22 12:05 1cis-1,2-Dichloroethene
1.0 U 0.262.0 ug/L 12/28/22 12:05 1cis-1,3-Dichloropropene
1.0 U 0.282.0 ug/L 12/28/22 12:05 1Cyclohexane
5.0 U 1.810 ug/L 12/28/22 12:05 11,2-Dibromo-3-Chloropropane
1.0 U 0.312.0 ug/L 12/28/22 12:05 11,2-Dichlorobenzene
1.0 U 0.312.0 ug/L 12/28/22 12:05 11,3-Dichlorobenzene
1.0 U 0.312.0 ug/L 12/28/22 12:05 11,4-Dichlorobenzene
1.0 U 0.252.0 ug/L 12/28/22 12:05 1Dichlorobromomethane
1.0 U 0.362.0 ug/L 12/28/22 12:05 1Dichlorodifluoromethane
1.0 U 0.332.0 ug/L 12/28/22 12:05 11,1-Dichloroethane
1.0 U M 0.252.0 ug/L 12/28/22 12:05 11,2-Dichloroethane
1.0 U 0.332.0 ug/L 12/28/22 12:05 11,1-Dichloroethene
0.50 U 0.221.0 ug/L 12/28/22 12:05 11,2-Dichloropropane
1.0 U 0.332.0 ug/L 12/28/22 12:05 11,2-Dibromoethane (EDB)
0.50 U 0.201.0 ug/L 12/28/22 12:05 1Ethylbenzene
10 U 3.220 ug/L 12/28/22 12:05 12-Hexanone
0.368 J 0.262.0 ug/L 12/28/22 12:05 1Isopropylbenzene
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-757008/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 757008
LOQ DL
Methyl acetate 10 U 20 3.2 ug/L 12/28/22 12:05 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
1.0 U 0.332.0 ug/L 12/28/22 12:05 1Methylcyclohexane
10 U 3.220 ug/L 12/28/22 12:05 1Methylene Chloride
10 U 2.720 ug/L 12/28/22 12:05 14-Methyl-2-pentanone (MIBK)
2.0 U 0.815.0 ug/L 12/28/22 12:05 1Methyl tert-butyl ether
1.0 U 0.272.0 ug/L 12/28/22 12:05 1Styrene
1.0 U 0.402.0 ug/L 12/28/22 12:05 11,1,2,2-Tetrachloroethane
1.0 U 0.352.0 ug/L 12/28/22 12:05 1Tetrachloroethene
1.0 U 0.252.0 ug/L 12/28/22 12:05 1Toluene
1.0 U 0.342.0 ug/L 12/28/22 12:05 1trans-1,2-Dichloroethene
1.0 U 0.232.0 ug/L 12/28/22 12:05 1trans-1,3-Dichloropropene
2.0 U M 0.535.0 ug/L 12/28/22 12:05 11,2,4-Trichlorobenzene
0.50 U 0.211.0 ug/L 12/28/22 12:05 11,1,1-Trichloroethane
1.0 U 0.322.0 ug/L 12/28/22 12:05 11,1,2-Trichloroethane
0.50 U 0.201.0 ug/L 12/28/22 12:05 1Trichloroethene
1.0 U 0.332.0 ug/L 12/28/22 12:05 1Trichlorofluoromethane
0.50 U 0.231.0 ug/L 12/28/22 12:05 11,1,2-Trichloro-1,2,2-trifluoroethane
1.0 U 0.402.0 ug/L 12/28/22 12:05 1Vinyl chloride
1.0 U 0.492.0 ug/L 12/28/22 12:05 1Xylenes, Total
10 U 5.020 ug/L 12/28/22 12:05 1Propionitrile
1.0 U 0.505.0 ug/L 12/28/22 12:05 1Pentachloroethane
2.0 U 0.782.5 ug/L 12/28/22 12:05 1Methyl methacrylate
1.0 U 0.225.0 ug/L 12/28/22 12:05 1Hexachlorobutadiene
1.0 U 0.342.0 ug/L 12/28/22 12:05 1Dibromomethane
40 U 2050 ug/L 12/28/22 12:05 1Acetonitrile
5.0 U 2.410 ug/L 12/28/22 12:05 1Naphthalene
10 U 3.920 ug/L 12/28/22 12:05 1Iodomethane
4.0 U 1.15.0 ug/L 12/28/22 12:05 13-Chloro-1-propene
20 U 5.550 ug/L 12/28/22 12:05 1Acrylonitrile
1.0 U 0.332.0 ug/L 12/28/22 12:05 1Ethyl methacrylate
1.0 U 0.362.0 ug/L 12/28/22 12:05 11,1,1,2-Tetrachloroethane
5.0 U 1.310 ug/L 12/28/22 12:05 1trans-1,4-Dichloro-2-butene
2.0 U 0.712.5 ug/L 12/28/22 12:05 12-Chloro-1,3-butadiene
10 U 5.020 ug/L 12/28/22 12:05 1Methacrylonitrile
40 U 1550 ug/L 12/28/22 12:05 1Acrolein
1.0 U 0.482.0 ug/L 12/28/22 12:05 11,2,3-Trichloropropane
2.0 U 0.692.5 ug/L 12/28/22 12:05 1Vinyl acetate
250 U 68500 ug/L 12/28/22 12:05 1Isobutyl alcohol
2.0 U 0.864.0 ug/L 12/28/22 12:05 12-Nitropropane
50 U 25100 ug/L 12/28/22 12:05 1n-Butyl alcohol
1.0 U 0.342.0 ug/L 12/28/22 12:05 1Bromochloromethane
1.0 U 0.375.0 ug/L 12/28/22 12:05 1Diethyl ether
5.0 U 2.110 ug/L 12/28/22 12:05 1Tetrahydrofuran
10 U 5.020 ug/L 12/28/22 12:05 1Ethyl acetate
5.0 U 2.510 ug/L 12/28/22 12:05 1Benzyl chloride
2.0 U 0.522.5 ug/L 12/28/22 12:05 1n-Butylbenzene
1.0 U 0.432.0 ug/L 12/28/22 12:05 11,2,4-Trimethylbenzene
0.50 U 0.251.0 ug/L 12/28/22 12:05 12-Chlorotoluene
1.0 U 0.505.0 ug/L 12/28/22 12:05 1n-Butyl acetate
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-757008/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 757008
LOQ DL
1,2-Dichloroethene, Total 1.0 U 2.0 0.37 ug/L 12/28/22 12:05 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
1.0 U 0.282.0 ug/L 12/28/22 12:05 11,1-Dichloropropene
5.0 U 2.510 ug/L 12/28/22 12:05 12-Methylnaphthalene
1.0 U 0.262.0 ug/L 12/28/22 12:05 1o-Xylene
2.0 U 0.655.0 ug/L 12/28/22 12:05 1Hexane
1.0 U 0.412.0 ug/L 12/28/22 12:05 14-Chlorotoluene
4.0 U M 1.15.0 ug/L 12/28/22 12:05 11-Chlorohexane
0.50 U 0.241.0 ug/L 12/28/22 12:05 1Bromobenzene
2.0 U 0.815.0 ug/L 12/28/22 12:05 11,2,3-Trichlorobenzene
1.0 U 0.482.0 ug/L 12/28/22 12:05 11,3-Dichloropropene, Total
2.0 U 0.532.5 ug/L 12/28/22 12:05 1sec-Butylbenzene
1.0 U 0.352.0 ug/L 12/28/22 12:05 12,2-Dichloropropane
1.0 U 0.412.0 ug/L 12/28/22 12:05 1N-Propylbenzene
5.0 U 2.510 ug/L 12/28/22 12:05 11,3,5-Trichlorobenzene
2.0 U 0.7010 ug/L 12/28/22 12:05 1Diisopropyl ether
100 U 50200 ug/L 12/28/22 12:05 1Ethanol
50 U 25100 ug/L 12/28/22 12:05 1Isopropyl alcohol
1.0 U 0.442.0 ug/L 12/28/22 12:05 1p-Cymene
2.0 U 0.782.5 ug/L 12/28/22 12:05 1Tert-amyl methyl ether
1.0 U 0.282.0 ug/L 12/28/22 12:05 11,3,5-Trimethylbenzene
5.0 U 2.510 ug/L 12/28/22 12:05 11,2,3-Trimethylbenzene
1.0 U 0.492.0 ug/L 12/28/22 12:05 1m-Xylene & p-Xylene
1.0 U 0.502.0 ug/L 12/28/22 12:05 1Dichlorofluoromethane
1.0 U 0.432.0 ug/L 12/28/22 12:05 1tert-Butylbenzene
2.0 U 0.995.0 ug/L 12/28/22 12:05 1Isooctane
1.0 U 0.362.0 ug/L 12/28/22 12:05 11,3-Dichloropropane
4-Bromofluorobenzene (Surr)101 85-114 12/28/22 12:05 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
107 12/28/22 12:05 1Dibromofluoromethane (Surr)80-119
90 12/28/22 12:05 11,2-Dichloroethane-d4 (Surr)81-118
116 Q 12/28/22 12:05 1Toluene-d8 (Surr)89-112
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-757008/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 757008
Acetone 250 192 ug/L 77 39 -160
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Benzene 50.0 50.1 ug/L 100 79 -120
Bromoform 50.0 40.0 ug/L 80 66 -130
Bromomethane 50.0 52.4 ug/L 105 53 -141
2-Butanone (MEK)250 162 ug/L 65 56 -143
Carbon disulfide 50.0 63.3 ug/L 127 64 -133
Carbon tetrachloride 50.0 54.4 ug/L 109 72 -136
Chlorobenzene 50.0 48.9 ug/L 98 82 -118
Chlorodibromomethane 50.0 52.1 ug/L 104 74 -126
Chloroethane 50.0 188 Q ug/L 375 60 -138
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-757008/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 757008
Chloroform 50.0 50.9 ug/L 102 79 -124
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Chloromethane 50.0 51.4 M ug/L 103 50 -139
cis-1,2-Dichloroethene 50.0 51.3 ug/L 103 78 -123
cis-1,3-Dichloropropene 50.0 52.8 ug/L 106 75 -124
Cyclohexane 50.0 53.4 ug/L 107 71 -130
1,2-Dibromo-3-Chloropropane 50.0 37.8 ug/L 76 62 -128
1,2-Dichlorobenzene 50.0 49.7 ug/L 99 80 -119
1,3-Dichlorobenzene 50.0 50.7 ug/L 101 80 -119
1,4-Dichlorobenzene 50.0 49.3 ug/L 99 79 -118
Dichlorobromomethane 50.0 48.8 ug/L 98 79 -125
Dichlorodifluoromethane 50.0 65.1 ug/L 130 32 -152
1,1-Dichloroethane 50.0 55.4 ug/L 111 77 -125
1,2-Dichloroethane 50.0 46.5 ug/L 93 73 -128
1,1-Dichloroethene 50.0 47.5 ug/L 95 71 -131
1,2-Dichloropropane 50.0 50.8 ug/L 102 78 -122
1,2-Dibromoethane (EDB)50.0 49.1 ug/L 98 75 -127
Ethylbenzene 50.0 51.0 ug/L 102 79 -121
2-Hexanone 250 207 ug/L 83 57 -139
Isopropylbenzene 50.0 52.9 ug/L 106 72 -131
Methyl acetate 100 78.8 ug/L 79 56 -136
Methylcyclohexane 50.0 55.9 ug/L 112 72 -132
Methylene Chloride 50.0 58.4 ug/L 117 74 -124
4-Methyl-2-pentanone (MIBK)250 197 ug/L 79 67 -130
Methyl tert-butyl ether 50.0 35.4 ug/L 71 71 -124
Styrene 50.0 53.8 ug/L 108 78 -123
1,1,2,2-Tetrachloroethane 50.0 40.0 ug/L 80 71 -121
Tetrachloroethene 50.0 54.0 ug/L 108 74 -129
Toluene 50.0 53.0 ug/L 106 80 -121
trans-1,2-Dichloroethene 50.0 50.3 ug/L 101 75 -124
trans-1,3-Dichloropropene 50.0 50.7 ug/L 101 73 -127
1,2,4-Trichlorobenzene 50.0 43.3 ug/L 87 69 -130
1,1,1-Trichloroethane 50.0 49.9 ug/L 100 74 -131
1,1,2-Trichloroethane 50.0 46.8 ug/L 94 80 -119
Trichloroethene 50.0 52.1 ug/L 104 79 -123
Trichlorofluoromethane 50.0 56.7 ug/L 113 65 -141
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 55.0 ug/L 110 70 -136
Vinyl chloride 50.0 58.6 ug/L 117 58 -137
Xylenes, Total 100 105 ug/L 105 79 -121
Hexachlorobutadiene 50.0 44.4 ug/L 89 66 -134
Dibromomethane 50.0 48.0 ug/L 96 79 -123
Naphthalene 50.0 38.6 ug/L 77 61 -128
Iodomethane 50.0 69.2 Q ug/L 138 69 -131
3-Chloro-1-propene 50.0 53.1 ug/L 106 68 -130
Acrylonitrile 500 423 ug/L 85 63 -135
Ethyl methacrylate 50.0 50.5 ug/L 101 72 -126
1,1,1,2-Tetrachloroethane 50.0 40.6 ug/L 81 78 -124
trans-1,4-Dichloro-2-butene 50.0 40.7 ug/L 81 43 -140
Acrolein 1000 684 ug/L 68 39 -155
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-757008/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 757008
1,2,3-Trichloropropane 50.0 41.3 ug/L 83 73 -122
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Vinyl acetate 100 78.8 ug/L 79 54 -146
Isobutyl alcohol 1250 678 Q ug/L 54 63 -133
Bromochloromethane 50.0 57.5 ug/L 115 78 -123
Diethyl ether 50.0 41.9 ug/L 84 68 -129
Tetrahydrofuran 100 68.4 ug/L 68 57 -133
n-Butylbenzene 50.0 49.8 ug/L 100 75 -128
1,2,4-Trimethylbenzene 50.0 54.7 ug/L 109 76 -124
2-Chlorotoluene 50.0 51.2 ug/L 102 79 -122
1,2-Dichloroethene, Total 100 102 ug/L 102 79 -121
1,1-Dichloropropene 50.0 52.4 ug/L 105 79 -125
o-Xylene 50.0 52.8 ug/L 106 78 -122
Hexane 50.0 54.7 ug/L 109 48 -143
4-Chlorotoluene 50.0 50.9 ug/L 102 78 -122
Bromobenzene 50.0 50.1 ug/L 100 80 -120
1,2,3-Trichlorobenzene 50.0 41.5 ug/L 83 69 -129
1,3-Dichloropropene, Total 100 103 ug/L 103 77 -123
sec-Butylbenzene 50.0 53.9 ug/L 108 77 -126
2,2-Dichloropropane 50.0 49.8 ug/L 100 60 -139
N-Propylbenzene 50.0 52.8 ug/L 106 76 -126
p-Cymene 50.0 52.3 ug/L 105 77 -127
1,3,5-Trimethylbenzene 50.0 54.2 ug/L 108 75 -124
m-Xylene & p-Xylene 50.0 52.0 ug/L 104 80 -121
Dichlorofluoromethane 50.0 69.8 ug/L 140
tert-Butylbenzene 50.0 54.2 ug/L 108 78 -124
1,3-Dichloropropane 50.0 47.1 ug/L 94 80 -119
4-Bromofluorobenzene (Surr)85 -114
Surrogate
97
LCS LCS
Qualifier Limits%Recovery
106Dibromofluoromethane (Surr)80 -119
971,2-Dichloroethane-d4 (Surr)81 -118
107Toluene-d8 (Surr)89 -112
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-757008/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 757008
Acetone 250 199 ug/L 79 39 -160 3 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Benzene 50.0 50.7 ug/L 101 79 -120 1 20
Bromoform 50.0 40.6 ug/L 81 66 -130 2 20
Bromomethane 50.0 52.0 ug/L 104 53 -141 1 20
2-Butanone (MEK)250 169 ug/L 68 56 -143 4 20
Carbon disulfide 50.0 62.9 ug/L 126 64 -133 1 20
Carbon tetrachloride 50.0 55.7 ug/L 111 72 -136 2 20
Chlorobenzene 50.0 49.3 ug/L 99 82 -118 1 20
Chlorodibromomethane 50.0 52.3 ug/L 105 74 -126 0 20
Chloroethane 50.0 184 Q ug/L 368 60 -138 2 20
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-757008/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 757008
Chloroform 50.0 50.9 ug/L 102 79 -124 0 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Chloromethane 50.0 53.8 ug/L 108 50 -139 5 20
cis-1,2-Dichloroethene 50.0 52.7 ug/L 105 78 -123 3 20
cis-1,3-Dichloropropene 50.0 53.2 ug/L 106 75 -124 1 20
Cyclohexane 50.0 54.8 ug/L 110 71 -130 2 20
1,2-Dibromo-3-Chloropropane 50.0 39.6 ug/L 79 62 -128 5 20
1,2-Dichlorobenzene 50.0 50.0 ug/L 100 80 -119 0 20
1,3-Dichlorobenzene 50.0 51.1 ug/L 102 80 -119 1 20
1,4-Dichlorobenzene 50.0 50.0 ug/L 100 79 -118 1 20
Dichlorobromomethane 50.0 49.2 ug/L 98 79 -125 1 20
Dichlorodifluoromethane 50.0 65.2 ug/L 130 32 -152 0 20
1,1-Dichloroethane 50.0 55.4 ug/L 111 77 -125 0 20
1,2-Dichloroethane 50.0 46.9 ug/L 94 73 -128 1 20
1,1-Dichloroethene 50.0 47.0 ug/L 94 71 -131 1 20
1,2-Dichloropropane 50.0 51.3 ug/L 103 78 -122 1 20
1,2-Dibromoethane (EDB)50.0 50.1 ug/L 100 75 -127 2 20
Ethylbenzene 50.0 51.1 ug/L 102 79 -121 0 20
2-Hexanone 250 215 ug/L 86 57 -139 4 20
Isopropylbenzene 50.0 52.5 ug/L 105 72 -131 1 20
Methyl acetate 100 81.2 ug/L 81 56 -136 3 20
Methylcyclohexane 50.0 56.4 ug/L 113 72 -132 1 20
Methylene Chloride 50.0 58.3 ug/L 117 74 -124 0 20
4-Methyl-2-pentanone (MIBK)250 205 ug/L 82 67 -130 4 20
Methyl tert-butyl ether 50.0 36.9 ug/L 74 71 -124 4 20
Styrene 50.0 52.9 ug/L 106 78 -123 2 20
1,1,2,2-Tetrachloroethane 50.0 40.2 ug/L 80 71 -121 1 20
Tetrachloroethene 50.0 54.5 ug/L 109 74 -129 1 20
Toluene 50.0 52.7 ug/L 105 80 -121 1 20
trans-1,2-Dichloroethene 50.0 51.5 ug/L 103 75 -124 2 20
trans-1,3-Dichloropropene 50.0 52.0 ug/L 104 73 -127 2 20
1,2,4-Trichlorobenzene 50.0 44.6 ug/L 89 69 -130 3 20
1,1,1-Trichloroethane 50.0 50.6 ug/L 101 74 -131 1 20
1,1,2-Trichloroethane 50.0 47.2 ug/L 94 80 -119 1 20
Trichloroethene 50.0 52.5 ug/L 105 79 -123 1 20
Trichlorofluoromethane 50.0 56.8 ug/L 114 65 -141 0 20
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 56.1 ug/L 112 70 -136 2 20
Vinyl chloride 50.0 58.5 ug/L 117 58 -137 0 20
Xylenes, Total 100 103 ug/L 103 79 -121 1 20
Hexachlorobutadiene 50.0 44.2 ug/L 88 66 -134 0 20
Dibromomethane 50.0 48.3 ug/L 97 79 -123 1 20
Naphthalene 50.0 39.6 ug/L 79 61 -128 3 20
Iodomethane 50.0 67.4 Q ug/L 135 69 -131 3 20
3-Chloro-1-propene 50.0 55.2 ug/L 110 68 -130 4 20
Acrylonitrile 500 433 ug/L 87 63 -135 2 20
Ethyl methacrylate 50.0 51.6 ug/L 103 72 -126 2 20
1,1,1,2-Tetrachloroethane 50.0 41.2 ug/L 82 78 -124 1 20
trans-1,4-Dichloro-2-butene 50.0 42.2 ug/L 84 43 -140 4 20
Acrolein 1000 703 ug/L 70 39 -155 3 20
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8260D - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-757008/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 757008
1,2,3-Trichloropropane 50.0 42.5 ug/L 85 73 -122 3 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Vinyl acetate 100 81.7 ug/L 82 54 -146 4 20
Isobutyl alcohol 1250 707 Q ug/L 57 63 -133 4 20
Bromochloromethane 50.0 57.5 ug/L 115 78 -123 0 20
Diethyl ether 50.0 44.3 ug/L 89 68 -129 6 20
Tetrahydrofuran 100 72.0 ug/L 72 57 -133 5 20
n-Butylbenzene 50.0 50.8 ug/L 102 75 -128 2 20
1,2,4-Trimethylbenzene 50.0 55.0 ug/L 110 76 -124 0 20
2-Chlorotoluene 50.0 50.3 ug/L 101 79 -122 2 20
1,2-Dichloroethene, Total 100 104 ug/L 104 79 -121 2 20
1,1-Dichloropropene 50.0 53.2 ug/L 106 79 -125 2 20
o-Xylene 50.0 52.1 ug/L 104 78 -122 1 20
Hexane 50.0 55.0 ug/L 110 48 -143 1 20
4-Chlorotoluene 50.0 50.8 ug/L 102 78 -122 0 20
Bromobenzene 50.0 50.4 ug/L 101 80 -120 1 20
1,2,3-Trichlorobenzene 50.0 42.7 ug/L 85 69 -129 3 20
1,3-Dichloropropene, Total 100 105 ug/L 105 77 -123 2 20
sec-Butylbenzene 50.0 52.3 ug/L 105 77 -126 3 20
2,2-Dichloropropane 50.0 50.4 ug/L 101 60 -139 1 20
N-Propylbenzene 50.0 52.0 ug/L 104 76 -126 2 20
p-Cymene 50.0 52.3 ug/L 105 77 -127 0 20
1,3,5-Trimethylbenzene 50.0 53.9 ug/L 108 75 -124 1 20
m-Xylene & p-Xylene 50.0 51.2 ug/L 102 80 -121 2 20
Dichlorofluoromethane 50.0 70.2 ug/L 140 1
tert-Butylbenzene 50.0 52.8 ug/L 106 78 -124 3 20
1,3-Dichloropropane 50.0 47.7 ug/L 95 80 -119 1 20
4-Bromofluorobenzene (Surr)85 -114
Surrogate
98
LCSD LCSD
Qualifier Limits%Recovery
105Dibromofluoromethane (Surr)80 -119
991,2-Dichloroethane-d4 (Surr)81 -118
107Toluene-d8 (Surr)89 -112
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-755512/8-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756054 Prep Batch: 755512
LOQ DL
1,1'-Biphenyl 320 U 1600 110 ug/Kg 12/16/22 15:30 12/20/22 10:23 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
65 U 30320 ug/Kg 12/16/22 15:30 12/20/22 10:23 11,2,4,5-Tetrachlorobenzene
65 U 30320 ug/Kg 12/16/22 15:30 12/20/22 10:23 11,2,4-Trichlorobenzene
65 U 36320 ug/Kg 12/16/22 15:30 12/20/22 10:23 11,2-Dichlorobenzene
65 U 33320 ug/Kg 12/16/22 15:30 12/20/22 10:23 11,2-Diphenylhydrazine
65 U 33320 ug/Kg 12/16/22 15:30 12/20/22 10:23 11,3-Dichlorobenzene
65 U 34320 ug/Kg 12/16/22 15:30 12/20/22 10:23 11,4-Dichlorobenzene
65 U 30320 ug/Kg 12/16/22 15:30 12/20/22 10:23 11-Methylnaphthalene
80 U 21320 ug/Kg 12/16/22 15:30 12/20/22 10:23 12,3,4,6-Tetrachlorophenol
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-755512/8-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756054 Prep Batch: 755512
LOQ DL
2,4,5-Trichlorophenol 65 U 320 34 ug/Kg 12/16/22 15:30 12/20/22 10:23 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
65 U 28320 ug/Kg 12/16/22 15:30 12/20/22 10:23 12,4,6-Trichlorophenol
65 U 34320 ug/Kg 12/16/22 15:30 12/20/22 10:23 12,4-Dichlorophenol
65 U 43320 ug/Kg 12/16/22 15:30 12/20/22 10:23 12,4-Dimethylphenol
1300 U 8001600 ug/Kg 12/16/22 15:30 12/20/22 10:23 12,4-Dinitrophenol
80 U 48320 ug/Kg 12/16/22 15:30 12/20/22 10:23 12,4-Dinitrotoluene
65 U 26320 ug/Kg 12/16/22 15:30 12/20/22 10:23 12,6-Dichlorophenol
65 U 41320 ug/Kg 12/16/22 15:30 12/20/22 10:23 12,6-Dinitrotoluene
65 U 34320 ug/Kg 12/16/22 15:30 12/20/22 10:23 12-Chloronaphthalene
65 U 39320 ug/Kg 12/16/22 15:30 12/20/22 10:23 12-Chlorophenol
65 U 37320 ug/Kg 12/16/22 15:30 12/20/22 10:23 12-Methylnaphthalene
65 U 26320 ug/Kg 12/16/22 15:30 12/20/22 10:23 12-Methylphenol
160 U 441600 ug/Kg 12/16/22 15:30 12/20/22 10:23 12-Nitroaniline
65 U 40320 ug/Kg 12/16/22 15:30 12/20/22 10:23 12-Nitrophenol
65 U 42320 ug/Kg 12/16/22 15:30 12/20/22 10:23 13 & 4 Methylphenol
65 U 27640 ug/Kg 12/16/22 15:30 12/20/22 10:23 13,3'-Dichlorobenzidine
80 U 451600 ug/Kg 12/16/22 15:30 12/20/22 10:23 13-Nitroaniline
320 U 1601600 ug/Kg 12/16/22 15:30 12/20/22 10:23 14,6-Dinitro-2-methylphenol
65 U 35320 ug/Kg 12/16/22 15:30 12/20/22 10:23 14-Bromophenyl phenyl ether
65 U M 34320 ug/Kg 12/16/22 15:30 12/20/22 10:23 14-Chloro-3-methylphenol
80 U 50640 ug/Kg 12/16/22 15:30 12/20/22 10:23 14-Chloroaniline
65 U 43320 ug/Kg 12/16/22 15:30 12/20/22 10:23 14-Chlorophenyl phenyl ether
80 U M 481600 ug/Kg 12/16/22 15:30 12/20/22 10:23 14-Nitroaniline
650 U 3201600 ug/Kg 12/16/22 15:30 12/20/22 10:23 14-Nitrophenol
65 U 40320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Acenaphthene
65 U 35320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Acenaphthylene
65 U 27320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Acetophenone
65 U 24320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Anthracene
65 U 22320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Atrazine
320 U 47320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Azobenzene
160 U 56320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Benzaldehyde
65 U 26320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Benzo[a]anthracene
80 U 50320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Benzo[a]pyrene
65 U 37320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Benzo[b]fluoranthene
65 U 21320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Benzo[g,h,i]perylene
160 U 63320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Benzo[k]fluoranthene
65 U 32320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Benzyl alcohol
65 U 29320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1bis (2-chloroisopropyl) ether
65 U 38320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Bis(2-chloroethoxy)methane
80 U 44320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Bis(2-chloroethyl)ether
65 U 28320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Bis(2-ethylhexyl) phthalate
65 U 25320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Butyl benzyl phthalate
160 U 64320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Caprolactam
65 U 29320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Carbazole
65 U 20320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Chrysene
65 U 38320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Dibenz(a,h)anthracene
65 U 32320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Dibenzofuran
65 U 36320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Diethyl phthalate
65 U 33320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Dimethyl phthalate
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-755512/8-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756054 Prep Batch: 755512
LOQ DL
Di-n-butyl phthalate 65 U 320 29 ug/Kg 12/16/22 15:30 12/20/22 10:23 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
65 U 28320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Di-n-octyl phthalate
140 U 40320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Diphenylamine
65 U 31320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Fluoranthene
65 U 35320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Fluorene
65 U 38320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Hexachlorobenzene
65 U 35320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Hexachlorobutadiene
65 U 40320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Hexachlorocyclopentadiene
65 U 27320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Hexachloroethane
65 U 27320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Indeno[1,2,3-cd]pyrene
65 U 32320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Isophorone
65 U 29320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Naphthalene
65 U 25320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Nitrobenzene
65 U 31320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1N-Nitrosodi-n-propylamine
65 U 32320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1N-Nitrosodiphenylamine
650 U 3201600 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Pentachlorophenol
65 U 26320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Phenanthrene
65 U 33320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Phenol
65 U 26320 ug/Kg 12/16/22 15:30 12/20/22 10:23 1Pyrene
2-Fluorobiphenyl (Surr)74 44-115 12/20/22 10:23 1
MB MB
Surrogate
12/16/22 15:30
Dil FacPreparedAnalyzedQualifierLimits%Recovery
68 12/16/22 15:30 12/20/22 10:23 12-Fluorophenol (Surr)35-115
69 12/16/22 15:30 12/20/22 10:23 1Nitrobenzene-d5 (Surr)37-122
72 12/16/22 15:30 12/20/22 10:23 1Phenol-d5 (Surr)33-122
79 12/16/22 15:30 12/20/22 10:23 1Terphenyl-d14 (Surr)54-127
58 12/16/22 15:30 12/20/22 10:23 12,4,6-Tribromophenol (Surr)39-132
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-755512/9-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756054 Prep Batch: 755512
1,1'-Biphenyl 6370 4440 ug/Kg 70 40 -117
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,2,4-Trichlorobenzene 6370 4170 ug/Kg 66 34 -118
1,2-Dichlorobenzene 6370 3950 ug/Kg 62 33 -117
1,2-Diphenylhydrazine 6370 4760 ug/Kg 75 41 -125
1,3-Dichlorobenzene 6370 3860 ug/Kg 61 30 -115
1,4-Dichlorobenzene 6370 3940 ug/Kg 62 31 -115
1-Methylnaphthalene 6370 4310 ug/Kg 68 40 -119
2,3,4,6-Tetrachlorophenol 6370 4360 ug/Kg 68 44 -125
2,4,5-Trichlorophenol 6370 4360 ug/Kg 68 41 -124
2,4,6-Trichlorophenol 6370 4350 ug/Kg 68 39 -126
2,4-Dichlorophenol 6370 4620 ug/Kg 73 40 -122
2,4-Dimethylphenol 6370 4420 ug/Kg 69 30 -127
2,4-Dinitrophenol 12700 8890 ug/Kg 70 10 -130
2,4-Dinitrotoluene 6370 4650 ug/Kg 73 48 -126
2,6-Dinitrotoluene 6370 4470 ug/Kg 70 46 -124
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-755512/9-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756054 Prep Batch: 755512
2-Chloronaphthalene 6370 4420 ug/Kg 69 41 -114
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2-Chlorophenol 6370 4200 ug/Kg 66 34 -121
2-Methylnaphthalene 6370 4520 ug/Kg 71 38 -122
2-Methylphenol 6370 4410 ug/Kg 69 32 -122
2-Nitroaniline 6370 4670 ug/Kg 73 44 -127
2-Nitrophenol 6370 4140 ug/Kg 65 36 -123
3 & 4 Methylphenol 6370 4400 ug/Kg 69 34 -119
3,3'-Dichlorobenzidine 6370 4730 ug/Kg 74 22 -121
3-Nitroaniline 6370 3890 ug/Kg 61 33 -119
4,6-Dinitro-2-methylphenol 12700 10300 ug/Kg 81 29 -132
4-Bromophenyl phenyl ether 6370 4320 ug/Kg 68 46 -124
4-Chloro-3-methylphenol 6370 4820 ug/Kg 76 45 -122
4-Chloroaniline 6370 3760 ug/Kg 59 17 -106
4-Chlorophenyl phenyl ether 6370 4320 ug/Kg 68 45 -121
4-Nitroaniline 6370 4400 ug/Kg 69 41 -130
4-Nitrophenol 12700 9100 ug/Kg 72 30 -132
Acenaphthene 6370 4390 ug/Kg 69 40 -123
Acenaphthylene 6370 4510 ug/Kg 71 32 -132
Acetophenone 6370 4180 ug/Kg 66 33 -115
Anthracene 6370 4780 ug/Kg 75 47 -123
Atrazine 6370 4700 ug/Kg 74 47 -127
Azobenzene 6370 4760 ug/Kg 75 44 -130
Benzaldehyde 6370 2420 ug/Kg 38 10 -130
Benzo[a]anthracene 6370 4880 ug/Kg 77 49 -126
Benzo[a]pyrene 6370 5090 ug/Kg 80 45 -129
Benzo[b]fluoranthene 6370 5220 ug/Kg 82 45 -132
Benzo[g,h,i]perylene 6370 4860 ug/Kg 76 43 -134
Benzo[k]fluoranthene 6370 5090 ug/Kg 80 47 -132
Benzyl alcohol 6370 4360 ug/Kg 69 29 -122
bis (2-chloroisopropyl) ether 6370 3920 ug/Kg 62 33 -131
Bis(2-chloroethoxy)methane 6370 4490 ug/Kg 71 36 -121
Bis(2-chloroethyl)ether 6370 4150 ug/Kg 65 31 -120
Bis(2-ethylhexyl) phthalate 6370 5810 ug/Kg 91 51 -133
Butyl benzyl phthalate 6370 5510 ug/Kg 87 48 -132
Caprolactam 6370 3750 ug/Kg 59 46 -117
Carbazole 6370 4730 ug/Kg 74 50 -123
Chrysene 6370 4810 ug/Kg 76 50 -124
Dibenz(a,h)anthracene 6370 4450 ug/Kg 70 45 -134
Dibenzofuran 6370 4510 ug/Kg 71 44 -120
Diethyl phthalate 6370 4760 ug/Kg 75 50 -124
Dimethyl phthalate 6370 4590 ug/Kg 72 48 -124
Di-n-butyl phthalate 6370 5060 ug/Kg 79 51 -128
Di-n-octyl phthalate 6370 5760 ug/Kg 91 45 -140
Diphenylamine 5440 4180 ug/Kg 77 38 -127
Fluoranthene 6370 4640 ug/Kg 73 50 -127
Fluorene 6370 4460 ug/Kg 70 43 -125
Hexachlorobenzene 6370 4170 ug/Kg 65 45 -122
Hexachlorobutadiene 6370 4090 ug/Kg 64 32 -123
Hexachlorocyclopentadiene 6370 4410 ug/Kg 69 28 -130
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-755512/9-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756054 Prep Batch: 755512
Hexachloroethane 6370 4190 ug/Kg 66 28 -117
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Indeno[1,2,3-cd]pyrene 6370 4450 M ug/Kg 70 45 -133
Isophorone 6370 4220 ug/Kg 66 30 -122
Naphthalene 6370 4160 ug/Kg 65 35 -123
Nitrobenzene 6370 4150 ug/Kg 65 34 -122
N-Nitrosodi-n-propylamine 6370 4190 ug/Kg 66 36 -120
N-Nitrosodiphenylamine 6370 4900 ug/Kg 77 38 -127
Pentachlorophenol 12700 8930 ug/Kg 70 25 -133
Phenanthrene 6370 4780 ug/Kg 75 50 -121
Phenol 6370 4380 ug/Kg 69 34 -121
Pyrene 6370 5210 ug/Kg 82 47 -127
2-Fluorobiphenyl (Surr)44 -115
Surrogate
65
LCS LCS
Qualifier Limits%Recovery
632-Fluorophenol (Surr)35 -115
62Nitrobenzene-d5 (Surr)37 -122
66Phenol-d5 (Surr)33 -122
73Terphenyl-d14 (Surr)54 -127
572,4,6-Tribromophenol (Surr)39 -132
Client Sample ID: 680-227663-A-1-E MSLab Sample ID: 680-227663-A-1-E MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756054 Prep Batch: 755512
1,1'-Biphenyl 410 U 8450 5800 ug/Kg 69 40 -117☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
1,2,4-Trichlorobenzene 82 U Q 8450 5230 ug/Kg 62 34 -118☼
1,2-Dichlorobenzene 82 U Q 8450 5190 ug/Kg 61 33 -117☼
1,2-Diphenylhydrazine 82 U 8450 6490 ug/Kg 77 41 -125☼
1,3-Dichlorobenzene 82 U Q 8450 4950 ug/Kg 59 30 -115☼
1,4-Dichlorobenzene 82 U Q 8450 5040 ug/Kg 60 31 -115☼
1-Methylnaphthalene 82 U 8450 5420 ug/Kg 64 40 -119☼
2,3,4,6-Tetrachlorophenol 100 U 8450 5700 ug/Kg 67 44 -125☼
2,4,5-Trichlorophenol 82 U 8450 6000 ug/Kg 71 41 -124☼
2,4,6-Trichlorophenol 82 U 8450 5750 ug/Kg 68 39 -126☼
2,4-Dichlorophenol 82 U 8450 5990 ug/Kg 71 40 -122☼
2,4-Dimethylphenol 82 U 8450 5710 ug/Kg 68 30 -127☼
2,4-Dinitrophenol 1600 U 16900 7480 ug/Kg 44 10 -130☼
2,4-Dinitrotoluene 100 U 8450 4820 ug/Kg 57 48 -126☼
2,6-Dinitrotoluene 82 U 8450 4940 ug/Kg 58 46 -124☼
2-Chloronaphthalene 82 U 8450 5730 ug/Kg 68 41 -114☼
2-Chlorophenol 82 U 8450 5580 ug/Kg 66 34 -121☼
2-Methylnaphthalene 82 U 8450 5800 ug/Kg 69 38 -122☼
2-Methylphenol 82 U 8450 5760 ug/Kg 68 32 -122☼
2-Nitroaniline 210 U 8450 5460 ug/Kg 65 44 -127☼
2-Nitrophenol 82 U 8450 4180 ug/Kg 49 36 -123☼
3 & 4 Methylphenol 82 U 8450 5800 ug/Kg 69 34 -119☼
3,3'-Dichlorobenzidine 82 U 8450 6800 ug/Kg 80 22 -121☼
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: 680-227663-A-1-E MSLab Sample ID: 680-227663-A-1-E MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756054 Prep Batch: 755512
3-Nitroaniline 100 U 8450 5100 ug/Kg 60 33 -119☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
4,6-Dinitro-2-methylphenol 410 U 16900 9480 ug/Kg 56 29 -132☼
4-Bromophenyl phenyl ether 82 U 8450 5670 ug/Kg 67 46 -124☼
4-Chloro-3-methylphenol 82 U 8450 6120 ug/Kg 72 45 -122☼
4-Chloroaniline 100 U Q 8450 5490 ug/Kg 65 17 -106☼
4-Chlorophenyl phenyl ether 82 U 8450 5630 ug/Kg 67 45 -121☼
4-Nitroaniline 100 U M Q 8450 4670 ug/Kg 55 41 -130☼
4-Nitrophenol 820 U 16900 10600 ug/Kg 63 30 -132☼
Acenaphthene 82 U Q 8450 5890 ug/Kg 70 40 -123☼
Acenaphthylene 82 U Q 8450 5930 ug/Kg 70 32 -132☼
Acetophenone 82 U 8450 5440 ug/Kg 64 33 -115☼
Anthracene 82 U Q 8450 6260 ug/Kg 74 47 -123☼
Atrazine 82 U 8450 5700 ug/Kg 68 47 -127☼
Azobenzene 410 U M 8450 6480 ug/Kg 77 44 -130☼
Benzaldehyde 210 U Q 8450 2780 ug/Kg 33 10 -130☼
Benzo[a]anthracene 82 U Q 8450 6210 ug/Kg 73 49 -126☼
Benzo[a]pyrene 100 U Q 8450 6520 ug/Kg 77 45 -129☼
Benzo[b]fluoranthene 82 U Q 8450 6440 ug/Kg 76 45 -132☼
Benzo[g,h,i]perylene 82 U Q 8450 6300 ug/Kg 75 43 -134☼
Benzo[k]fluoranthene 210 U Q 8450 6530 ug/Kg 77 47 -132☼
Benzyl alcohol 82 U Q 8450 5810 ug/Kg 69 29 -122☼
bis (2-chloroisopropyl) ether 82 U Q 8450 4990 ug/Kg 59 33 -131☼
Bis(2-chloroethoxy)methane 82 U Q 8450 5800 ug/Kg 69 36 -121☼
Bis(2-chloroethyl)ether 100 U Q 8450 5340 ug/Kg 63 31 -120☼
Bis(2-ethylhexyl) phthalate 82 U 8450 7500 ug/Kg 89 51 -133☼
Butyl benzyl phthalate 82 U 8450 7240 ug/Kg 86 48 -132☼
Caprolactam 210 U Q 8450 4930 ug/Kg 58 46 -117☼
Carbazole 82 U 8450 6270 ug/Kg 74 50 -123☼
Chrysene 82 U Q 8450 6220 ug/Kg 74 50 -124☼
Dibenz(a,h)anthracene 82 U 8450 5780 ug/Kg 68 45 -134☼
Dibenzofuran 82 U 8450 5890 ug/Kg 70 44 -120☼
Diethyl phthalate 82 U 8450 6160 ug/Kg 73 50 -124☼
Dimethyl phthalate 82 U 8450 5950 ug/Kg 70 48 -124☼
Di-n-butyl phthalate 82 U 8450 6600 ug/Kg 78 51 -128☼
Di-n-octyl phthalate 82 U 8450 7420 ug/Kg 88 45 -140☼
Diphenylamine 170 U M 7220 5390 ug/Kg 75 38 -127☼
Fluoranthene 82 U Q 8450 6010 ug/Kg 71 50 -127☼
Fluorene 82 U Q 8450 5830 ug/Kg 69 43 -125☼
Hexachlorobenzene 82 U Q 8450 5290 ug/Kg 63 45 -122☼
Hexachlorobutadiene 82 U Q 8450 5370 ug/Kg 64 32 -123☼
Hexachlorocyclopentadiene 82 U 8450 2820 ug/Kg 33 28 -130☼
Hexachloroethane 82 U Q 8450 4820 ug/Kg 57 28 -117☼
Indeno[1,2,3-cd]pyrene 82 U Q 8450 5960 ug/Kg 71 45 -133☼
Isophorone 82 U Q 8450 5480 ug/Kg 65 30 -122☼
Naphthalene 82 U Q 8450 5280 ug/Kg 62 35 -123☼
Nitrobenzene 82 U Q 8450 4790 ug/Kg 57 34 -122☼
N-Nitrosodi-n-propylamine 82 U Q 8450 5520 ug/Kg 65 36 -120☼
N-Nitrosodiphenylamine 82 U 8450 6300 ug/Kg 75 38 -127☼
Pentachlorophenol 820 U 16900 11300 ug/Kg 67 25 -133☼
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: 680-227663-A-1-E MSLab Sample ID: 680-227663-A-1-E MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756054 Prep Batch: 755512
Phenanthrene 82 U Q 8450 6330 ug/Kg 75 50 -121☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Phenol 82 U 8450 5620 ug/Kg 67 34 -121☼
Pyrene 82 U Q 8450 6620 ug/Kg 78 47 -127☼
2-Fluorobiphenyl (Surr)44 -115
Surrogate
64
MS MS
Qualifier Limits%Recovery
612-Fluorophenol (Surr)35 -115
52Nitrobenzene-d5 (Surr)37 -122
62Phenol-d5 (Surr)33 -122
69Terphenyl-d14 (Surr)54 -127
552,4,6-Tribromophenol (Surr)39 -132
Client Sample ID: 680-227663-A-1-F MSDLab Sample ID: 680-227663-A-1-F MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756054 Prep Batch: 755512
1,1'-Biphenyl 410 U 8220 5940 ug/Kg 72 40 -117 2 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
1,2,4-Trichlorobenzene 82 U Q 8220 5420 ug/Kg 66 34 -118 4 20☼
1,2-Dichlorobenzene 82 U Q 8220 5490 ug/Kg 67 33 -117 6 20☼
1,2-Diphenylhydrazine 82 U 8220 6600 ug/Kg 80 41 -125 2 20☼
1,3-Dichlorobenzene 82 U Q 8220 5220 ug/Kg 63 30 -115 5 20☼
1,4-Dichlorobenzene 82 U Q 8220 5170 ug/Kg 63 31 -115 3 20☼
1-Methylnaphthalene 82 U 8220 5640 ug/Kg 69 40 -119 4 20☼
2,3,4,6-Tetrachlorophenol 100 U 8220 5710 ug/Kg 69 44 -125 0 20☼
2,4,5-Trichlorophenol 82 U 8220 5990 ug/Kg 73 41 -124 0 20☼
2,4,6-Trichlorophenol 82 U 8220 5890 ug/Kg 72 39 -126 2 20☼
2,4-Dichlorophenol 82 U 8220 6210 ug/Kg 76 40 -122 4 20☼
2,4-Dimethylphenol 82 U 8220 6210 ug/Kg 75 30 -127 8 20☼
2,4-Dinitrophenol 1600 U 16400 8100 ug/Kg 49 10 -130 8 20☼
2,4-Dinitrotoluene 100 U 8220 4850 ug/Kg 59 48 -126 1 20☼
2,6-Dinitrotoluene 82 U 8220 5090 ug/Kg 62 46 -124 3 20☼
2-Chloronaphthalene 82 U 8220 5900 ug/Kg 72 41 -114 3 20☼
2-Chlorophenol 82 U 8220 6010 ug/Kg 73 34 -121 7 20☼
2-Methylnaphthalene 82 U 8220 5970 ug/Kg 73 38 -122 3 20☼
2-Methylphenol 82 U 8220 6070 ug/Kg 74 32 -122 5 20☼
2-Nitroaniline 210 U 8220 5630 ug/Kg 68 44 -127 3 20☼
2-Nitrophenol 82 U 8220 4280 ug/Kg 52 36 -123 2 20☼
3 & 4 Methylphenol 82 U 8220 6250 ug/Kg 76 34 -119 8 20☼
3,3'-Dichlorobenzidine 82 U 8220 6530 ug/Kg 79 22 -121 4 20☼
3-Nitroaniline 100 U 8220 5310 ug/Kg 65 33 -119 4 20☼
4,6-Dinitro-2-methylphenol 410 U 16400 9320 ug/Kg 57 29 -132 2 20☼
4-Bromophenyl phenyl ether 82 U 8220 5800 ug/Kg 71 46 -124 2 20☼
4-Chloro-3-methylphenol 82 U 8220 6480 ug/Kg 79 45 -122 6 20☼
4-Chloroaniline 100 U Q 8220 5410 ug/Kg 66 17 -106 1 20☼
4-Chlorophenyl phenyl ether 82 U 8220 5860 ug/Kg 71 45 -121 4 20☼
4-Nitroaniline 100 U M Q 8220 5040 ug/Kg 61 41 -130 8 20☼
4-Nitrophenol 820 U 16400 10800 ug/Kg 66 30 -132 2 20☼
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: 680-227663-A-1-F MSDLab Sample ID: 680-227663-A-1-F MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756054 Prep Batch: 755512
Acenaphthene 82 U Q 8220 5930 ug/Kg 72 40 -123 1 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
Acenaphthylene 82 U Q 8220 6000 ug/Kg 73 32 -132 1 20☼
Acetophenone 82 U 8220 5830 ug/Kg 71 33 -115 7 20☼
Anthracene 82 U Q 8220 6310 ug/Kg 77 47 -123 1 20☼
Atrazine 82 U 8220 5440 ug/Kg 66 47 -127 5 20☼
Azobenzene 410 U M 8220 6590 ug/Kg 80 44 -130 2 20☼
Benzaldehyde 210 U Q 8220 2980 ug/Kg 36 10 -130 7 20☼
Benzo[a]anthracene 82 U Q 8220 6230 ug/Kg 76 49 -126 0 20☼
Benzo[a]pyrene 100 U Q 8220 6430 ug/Kg 78 45 -129 2 20☼
Benzo[b]fluoranthene 82 U Q 8220 6380 ug/Kg 78 45 -132 1 20☼
Benzo[g,h,i]perylene 82 U Q 8220 5990 ug/Kg 73 43 -134 5 20☼
Benzo[k]fluoranthene 210 U Q 8220 6450 ug/Kg 78 47 -132 1 20☼
Benzyl alcohol 82 U Q 8220 6180 ug/Kg 75 29 -122 6 20☼
bis (2-chloroisopropyl) ether 82 U Q 8220 5360 ug/Kg 65 33 -131 7 20☼
Bis(2-chloroethoxy)methane 82 U Q 8220 5990 ug/Kg 73 36 -121 3 20☼
Bis(2-chloroethyl)ether 100 U Q 8220 5480 ug/Kg 67 31 -120 3 20☼
Bis(2-ethylhexyl) phthalate 82 U 8220 7640 ug/Kg 93 51 -133 2 20☼
Butyl benzyl phthalate 82 U 8220 7220 ug/Kg 88 48 -132 0 20☼
Caprolactam 210 U Q 8220 5130 ug/Kg 62 46 -117 4 20☼
Carbazole 82 U 8220 6320 ug/Kg 77 50 -123 1 20☼
Chrysene 82 U Q 8220 6100 ug/Kg 74 50 -124 2 20☼
Dibenz(a,h)anthracene 82 U 8220 5570 ug/Kg 68 45 -134 4 20☼
Dibenzofuran 82 U 8220 5980 ug/Kg 73 44 -120 1 20☼
Diethyl phthalate 82 U 8220 6300 ug/Kg 77 50 -124 2 20☼
Dimethyl phthalate 82 U 8220 6290 ug/Kg 77 48 -124 6 20☼
Di-n-butyl phthalate 82 U 8220 6670 ug/Kg 81 51 -128 1 20☼
Di-n-octyl phthalate 82 U 8220 7500 ug/Kg 91 45 -140 1 20☼
Diphenylamine 170 U M 7030 5460 ug/Kg 78 38 -127 1 20☼
Fluoranthene 82 U Q 8220 6020 ug/Kg 73 50 -127 0 20☼
Fluorene 82 U Q 8220 5870 ug/Kg 71 43 -125 1 20☼
Hexachlorobenzene 82 U Q 8220 5470 ug/Kg 67 45 -122 3 20☼
Hexachlorobutadiene 82 U Q 8220 5640 ug/Kg 69 32 -123 5 20☼
Hexachlorocyclopentadiene 82 U 8220 2890 ug/Kg 35 28 -130 2 20☼
Hexachloroethane 82 U Q 8220 5130 ug/Kg 62 28 -117 6 20☼
Indeno[1,2,3-cd]pyrene 82 U Q 8220 5770 ug/Kg 70 45 -133 3 20☼
Isophorone 82 U Q 8220 5710 ug/Kg 69 30 -122 4 20☼
Naphthalene 82 U Q 8220 5520 ug/Kg 67 35 -123 4 20☼
Nitrobenzene 82 U Q 8220 4990 ug/Kg 61 34 -122 4 20☼
N-Nitrosodi-n-propylamine 82 U Q 8220 5680 ug/Kg 69 36 -120 3 20☼
N-Nitrosodiphenylamine 82 U 8220 6410 ug/Kg 78 38 -127 2 20☼
Pentachlorophenol 820 U 16400 11600 ug/Kg 71 25 -133 3 20☼
Phenanthrene 82 U Q 8220 6330 ug/Kg 77 50 -121 0 20☼
Phenol 82 U 8220 5860 ug/Kg 71 34 -121 4 20☼
Pyrene 82 U Q 8220 6680 ug/Kg 81 47 -127 1 20☼
2-Fluorobiphenyl (Surr)44 -115
Surrogate
67
MSD MSD
Qualifier Limits%Recovery
652-Fluorophenol (Surr)35 -115
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: 680-227663-A-1-F MSDLab Sample ID: 680-227663-A-1-F MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756054 Prep Batch: 755512
Nitrobenzene-d5 (Surr)37 -122
Surrogate
56
MSD MSD
Qualifier Limits%Recovery
68Phenol-d5 (Surr)33 -122
71Terphenyl-d14 (Surr)54 -127
572,4,6-Tribromophenol (Surr)39 -132
Client Sample ID: Method BlankLab Sample ID: MB 680-756109/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 756690 Prep Batch: 756109
LOQ DL
1,1'-Biphenyl 10 U M 20 4.6 ug/L 12/20/22 11:44 12/23/22 15:46 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
10 U Q 4.520 ug/L 12/20/22 11:44 12/23/22 15:46 11,2,4,5-Tetrachlorobenzene
10 U Q 3.420 ug/L 12/20/22 11:44 12/23/22 15:46 11,2,4-Trichlorobenzene
5.0 U M Q 2.510 ug/L 12/20/22 11:44 12/23/22 15:46 11,2-Dichlorobenzene
10 U 3.720 ug/L 12/20/22 11:44 12/23/22 15:46 11,2-Diphenylhydrazine
10 U Q 2.920 ug/L 12/20/22 11:44 12/23/22 15:46 11,3-Dichlorobenzene
10 U M Q 3.320 ug/L 12/20/22 11:44 12/23/22 15:46 11,4-Dichlorobenzene
10 U 4.720 ug/L 12/20/22 11:44 12/23/22 15:46 11-Methylnaphthalene
10 U 4.320 ug/L 12/20/22 11:44 12/23/22 15:46 12,3,4,6-Tetrachlorophenol
10 U 3.320 ug/L 12/20/22 11:44 12/23/22 15:46 12,4,5-Trichlorophenol
5.0 U 2.220 ug/L 12/20/22 11:44 12/23/22 15:46 12,4,6-Trichlorophenol
10 U 3.720 ug/L 12/20/22 11:44 12/23/22 15:46 12,4-Dichlorophenol
10 U 3.020 ug/L 12/20/22 11:44 12/23/22 15:46 12,4-Dimethylphenol
40 U 1650 ug/L 12/20/22 11:44 12/23/22 15:46 12,4-Dinitrophenol
5.0 U 2.310 ug/L 12/20/22 11:44 12/23/22 15:46 12,4-Dinitrotoluene
5.0 U Q 2.410 ug/L 12/20/22 11:44 12/23/22 15:46 12,6-Dichlorophenol
10 U 2.820 ug/L 12/20/22 11:44 12/23/22 15:46 12,6-Dinitrotoluene
10 U 4.820 ug/L 12/20/22 11:44 12/23/22 15:46 12-Chloronaphthalene
10 U 3.220 ug/L 12/20/22 11:44 12/23/22 15:46 12-Chlorophenol
10 U 4.620 ug/L 12/20/22 11:44 12/23/22 15:46 12-Methylnaphthalene
4.0 U 1.810 ug/L 12/20/22 11:44 12/23/22 15:46 12-Methylphenol
10 U M 2.920 ug/L 12/20/22 11:44 12/23/22 15:46 12-Nitroaniline
10 U 3.920 ug/L 12/20/22 11:44 12/23/22 15:46 12-Nitrophenol
4.0 U 1.410 ug/L 12/20/22 11:44 12/23/22 15:46 13 & 4 Methylphenol
20 U 1050 ug/L 12/20/22 11:44 12/23/22 15:46 13,3'-Dichlorobenzidine
10 U 3.050 ug/L 12/20/22 11:44 12/23/22 15:46 13-Nitroaniline
20 U 5.350 ug/L 12/20/22 11:44 12/23/22 15:46 14,6-Dinitro-2-methylphenol
10 U 4.720 ug/L 12/20/22 11:44 12/23/22 15:46 14-Bromophenyl phenyl ether
10 U 2.520 ug/L 12/20/22 11:44 12/23/22 15:46 14-Chloro-3-methylphenol
4.0 U Q 1.010 ug/L 12/20/22 11:44 12/23/22 15:46 14-Chloroaniline
12 U 5.320 ug/L 12/20/22 11:44 12/23/22 15:46 14-Chlorophenyl phenyl ether
10 U 3.050 ug/L 12/20/22 11:44 12/23/22 15:46 14-Nitroaniline
20 U 8.150 ug/L 12/20/22 11:44 12/23/22 15:46 14-Nitrophenol
10 U 4.420 ug/L 12/20/22 11:44 12/23/22 15:46 1Acenaphthene
10 U 3.620 ug/L 12/20/22 11:44 12/23/22 15:46 1Acenaphthylene
5.0 U 2.210 ug/L 12/20/22 11:44 12/23/22 15:46 1Acetophenone
10 U 3.620 ug/L 12/20/22 11:44 12/23/22 15:46 1Anthracene
5.0 U 2.210 ug/L 12/20/22 11:44 12/23/22 15:46 1Atrazine
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-756109/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 756690 Prep Batch: 756109
LOQ DL
Azobenzene 10 U 20 3.6 ug/L 12/20/22 11:44 12/23/22 15:46 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
10 U M 4.820 ug/L 12/20/22 11:44 12/23/22 15:46 1Benzaldehyde
10 U 4.220 ug/L 12/20/22 11:44 12/23/22 15:46 1Benzo[a]anthracene
10 U M 2.820 ug/L 12/20/22 11:44 12/23/22 15:46 1Benzo[a]pyrene
10 U 3.120 ug/L 12/20/22 11:44 12/23/22 15:46 1Benzo[b]fluoranthene
10 U 3.020 ug/L 12/20/22 11:44 12/23/22 15:46 1Benzo[g,h,i]perylene
10 U 2.920 ug/L 12/20/22 11:44 12/23/22 15:46 1Benzo[k]fluoranthene
10 U M Q 2.620 ug/L 12/20/22 11:44 12/23/22 15:46 1Benzyl alcohol
10 U Q 3.120 ug/L 12/20/22 11:44 12/23/22 15:46 1bis (2-chloroisopropyl) ether
4.0 U Q 1.810 ug/L 12/20/22 11:44 12/23/22 15:46 1Bis(2-chloroethoxy)methane
10 U Q 3.620 ug/L 12/20/22 11:44 12/23/22 15:46 1Bis(2-chloroethyl)ether
10 U 3.020 ug/L 12/20/22 11:44 12/23/22 15:46 1Bis(2-ethylhexyl) phthalate
10 U 2.820 ug/L 12/20/22 11:44 12/23/22 15:46 1Butyl benzyl phthalate
10 U 2.820 ug/L 12/20/22 11:44 12/23/22 15:46 1Caprolactam
4.0 U 1.810 ug/L 12/20/22 11:44 12/23/22 15:46 1Carbazole
10 U 3.820 ug/L 12/20/22 11:44 12/23/22 15:46 1Chrysene
10 U 3.020 ug/L 12/20/22 11:44 12/23/22 15:46 1Dibenz(a,h)anthracene
4.0 U 1.910 ug/L 12/20/22 11:44 12/23/22 15:46 1Dibenzofuran
5.0 U 2.210 ug/L 12/20/22 11:44 12/23/22 15:46 1Diethyl phthalate
5.0 U 2.110 ug/L 12/20/22 11:44 12/23/22 15:46 1Dimethyl phthalate
5.0 U 2.310 ug/L 12/20/22 11:44 12/23/22 15:46 1Di-n-butyl phthalate
10 U M 2.820 ug/L 12/20/22 11:44 12/23/22 15:46 1Di-n-octyl phthalate
8.5 U 2.510 ug/L 12/20/22 11:44 12/23/22 15:46 1Diphenylamine
4.0 U 1.610 ug/L 12/20/22 11:44 12/23/22 15:46 1Fluoranthene
10 U 3.420 ug/L 12/20/22 11:44 12/23/22 15:46 1Fluorene
4.0 U 1.610 ug/L 12/20/22 11:44 12/23/22 15:46 1Hexachlorobenzene
10 U Q 4.020 ug/L 12/20/22 11:44 12/23/22 15:46 1Hexachlorobutadiene
10 U 3.520 ug/L 12/20/22 11:44 12/23/22 15:46 1Hexachlorocyclopentadiene
10 U Q 3.620 ug/L 12/20/22 11:44 12/23/22 15:46 1Hexachloroethane
10 U 4.320 ug/L 12/20/22 11:44 12/23/22 15:46 1Indeno[1,2,3-cd]pyrene
4.0 U Q 2.010 ug/L 12/20/22 11:44 12/23/22 15:46 1Isophorone
10 U 3.520 ug/L 12/20/22 11:44 12/23/22 15:46 1Naphthalene
10 U Q 3.520 ug/L 12/20/22 11:44 12/23/22 15:46 1Nitrobenzene
5.0 U M Q 2.410 ug/L 12/20/22 11:44 12/23/22 15:46 1N-Nitrosodi-n-propylamine
10 U 2.920 ug/L 12/20/22 11:44 12/23/22 15:46 1N-Nitrosodiphenylamine
20 U 9.950 ug/L 12/20/22 11:44 12/23/22 15:46 1Pentachlorophenol
10 U 4.320 ug/L 12/20/22 11:44 12/23/22 15:46 1Phenanthrene
4.0 U 1.510 ug/L 12/20/22 11:44 12/23/22 15:46 1Phenol
10 U M 3.720 ug/L 12/20/22 11:44 12/23/22 15:46 1Pyrene
2-Fluorobiphenyl (Surr)44 44-119 12/23/22 15:46 1
MB MB
Surrogate
12/20/22 11:44
Dil FacPreparedAnalyzedQualifierLimits%Recovery
19 12/20/22 11:44 12/23/22 15:46 12-Fluorophenol (Surr)19-119
36 Q 12/20/22 11:44 12/23/22 15:46 1Nitrobenzene-d5 (Surr)44-120
13 12/20/22 11:44 12/23/22 15:46 1Phenol-d5 (Surr)10-130
63 12/20/22 11:44 12/23/22 15:46 1Terphenyl-d14 (Surr)50-134
60 12/20/22 11:44 12/23/22 15:46 12,4,6-Tribromophenol (Surr)43-140
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-756109/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 756690 Prep Batch: 756109
1,1'-Biphenyl 200 120 ug/L 60 49 -115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,2,4-Trichlorobenzene 200 116 ug/L 58 29 -116
1,2-Dichlorobenzene 200 102 ug/L 51 32 -111
1,2-Diphenylhydrazine 200 120 ug/L 60 49 -122
1,3-Dichlorobenzene 200 101 ug/L 51 28 -110
1,4-Dichlorobenzene 200 98.8 ug/L 49 29 -112
1-Methylnaphthalene 200 121 ug/L 61 41 -119
2,3,4,6-Tetrachlorophenol 200 169 ug/L 84 50 -128
2,4,5-Trichlorophenol 200 132 ug/L 66 53 -123
2,4,6-Trichlorophenol 200 141 ug/L 70 50 -125
2,4-Dichlorophenol 200 120 ug/L 60 47 -121
2,4-Dimethylphenol 200 105 ug/L 52 31 -124
2,4-Dinitrophenol 400 330 M ug/L 83 23 -143
2,4-Dinitrotoluene 200 161 ug/L 81 57 -128
2,6-Dinitrotoluene 200 146 ug/L 73 57 -124
2-Chloronaphthalene 200 117 ug/L 58 40 -116
2-Chlorophenol 200 93.4 ug/L 47 38 -117
2-Methylnaphthalene 200 129 ug/L 65 40 -121
2-Methylphenol 200 80.7 ug/L 40 30 -117
2-Nitroaniline 200 128 ug/L 64 55 -127
2-Nitrophenol 200 115 ug/L 57 47 -123
3 & 4 Methylphenol 200 75.3 ug/L 38 29 -110
3,3'-Dichlorobenzidine 200 356 Q ug/L 178 27 -129
3-Nitroaniline 200 141 ug/L 71 41 -128
4,6-Dinitro-2-methylphenol 400 343 ug/L 86 44 -137
4-Bromophenyl phenyl ether 200 148 ug/L 74 55 -124
4-Chloro-3-methylphenol 200 121 ug/L 60 52 -119
4-Chloroaniline 200 114 ug/L 57 33 -117
4-Chlorophenyl phenyl ether 200 143 ug/L 71 53 -121
4-Nitroaniline 200 146 ug/L 73 55 -115
4-Nitrophenol 400 105 ug/L 26 13 -130
Acenaphthene 200 126 ug/L 63 47 -122
Acenaphthylene 200 129 ug/L 65 41 -130
Acetophenone 200 119 ug/L 60 46 -118
Anthracene 200 145 ug/L 72 57 -123
Atrazine 200 145 ug/L 72 44 -142
Azobenzene 200 120 Q ug/L 60 61 -116
Benzaldehyde 200 99.4 ug/L 50 25 -130
Benzo[a]anthracene 200 156 ug/L 78 58 -125
Benzo[a]pyrene 200 158 ug/L 79 54 -128
Benzo[b]fluoranthene 200 161 ug/L 80 53 -131
Benzo[g,h,i]perylene 200 156 ug/L 78 50 -134
Benzo[k]fluoranthene 200 149 ug/L 74 57 -129
Benzyl alcohol 200 91.3 ug/L 46 31 -112
bis (2-chloroisopropyl) ether 200 98.5 ug/L 49 37 -130
Bis(2-chloroethoxy)methane 200 114 ug/L 57 48 -120
Bis(2-chloroethyl)ether 200 98.4 ug/L 49 43 -118
Bis(2-ethylhexyl) phthalate 200 154 ug/L 77 55 -135
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-756109/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 756690 Prep Batch: 756109
Butyl benzyl phthalate 200 167 ug/L 83 53 -134
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Caprolactam 200 48.3 M ug/L 24 13 -130
Carbazole 200 149 ug/L 75 60 -122
Chrysene 200 151 ug/L 75 59 -123
Dibenz(a,h)anthracene 200 154 ug/L 77 51 -134
Dibenzofuran 200 131 ug/L 66 53 -118
Diethyl phthalate 200 148 ug/L 74 56 -125
Dimethyl phthalate 200 142 ug/L 71 45 -127
Di-n-butyl phthalate 200 156 ug/L 78 56 -122
Di-n-octyl phthalate 200 170 ug/L 85 59 -128
Diphenylamine 171 118 ug/L 69 55 -111
Fluoranthene 200 161 ug/L 80 57 -128
Fluorene 200 136 ug/L 68 52 -124
Hexachlorobenzene 200 165 ug/L 82 53 -125
Hexachlorobutadiene 200 114 ug/L 57 22 -124
Hexachlorocyclopentadiene 200 122 ug/L 61 28 -130
Hexachloroethane 200 95.2 ug/L 48 21 -115
Indeno[1,2,3-cd]pyrene 200 163 ug/L 81 52 -134
Isophorone 200 117 ug/L 58 42 -124
Naphthalene 200 110 ug/L 55 40 -121
Nitrobenzene 200 104 ug/L 52 45 -121
N-Nitrosodi-n-propylamine 200 108 ug/L 54 49 -119
N-Nitrosodiphenylamine 200 138 ug/L 69 51 -123
Pentachlorophenol 400 357 ug/L 89 35 -138
Phenanthrene 200 146 ug/L 73 59 -120
Phenol 200 38.0 ug/L 19 14 -130
Pyrene 200 158 ug/L 79 57 -126
2-Fluorobiphenyl (Surr)44 -119
Surrogate
56
LCS LCS
Qualifier Limits%Recovery
252-Fluorophenol (Surr)19 -119
50Nitrobenzene-d5 (Surr)44 -120
17Phenol-d5 (Surr)10 -130
81Terphenyl-d14 (Surr)50 -134
872,4,6-Tribromophenol (Surr)43 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-756109/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 756690 Prep Batch: 756109
1,1'-Biphenyl 200 122 ug/L 61 49 -115 2 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,2,4-Trichlorobenzene 200 117 ug/L 59 29 -116 1 20
1,2-Dichlorobenzene 200 102 ug/L 51 32 -111 0 20
1,2-Diphenylhydrazine 200 120 ug/L 60 49 -122 0 20
1,3-Dichlorobenzene 200 98.4 ug/L 49 28 -110 3 20
1,4-Dichlorobenzene 200 100 ug/L 50 29 -112 2 20
1-Methylnaphthalene 200 121 ug/L 60 41 -119 1 20
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-756109/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 756690 Prep Batch: 756109
2,3,4,6-Tetrachlorophenol 200 155 ug/L 78 50 -128 8 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
2,4,5-Trichlorophenol 200 139 ug/L 69 53 -123 5 20
2,4,6-Trichlorophenol 200 136 ug/L 68 50 -125 4 20
2,4-Dichlorophenol 200 120 ug/L 60 47 -121 0 20
2,4-Dimethylphenol 200 105 ug/L 52 31 -124 0 20
2,4-Dinitrophenol 400 307 M ug/L 77 23 -143 7 20
2,4-Dinitrotoluene 200 150 ug/L 75 57 -128 7 20
2,6-Dinitrotoluene 200 138 ug/L 69 57 -124 6 20
2-Chloronaphthalene 200 121 ug/L 61 40 -116 4 20
2-Chlorophenol 200 91.9 ug/L 46 38 -117 2 20
2-Methylnaphthalene 200 130 ug/L 65 40 -121 0 20
2-Methylphenol 200 78.9 ug/L 39 30 -117 2 20
2-Nitroaniline 200 126 ug/L 63 55 -127 1 20
2-Nitrophenol 200 120 ug/L 60 47 -123 5 20
3 & 4 Methylphenol 200 72.9 ug/L 36 29 -110 3 20
3,3'-Dichlorobenzidine 200 190 Q ug/L 95 27 -129 61 20
3-Nitroaniline 200 128 ug/L 64 41 -128 10 20
4,6-Dinitro-2-methylphenol 400 326 ug/L 81 44 -137 5 20
4-Bromophenyl phenyl ether 200 143 ug/L 72 55 -124 4 20
4-Chloro-3-methylphenol 200 117 ug/L 58 52 -119 3 20
4-Chloroaniline 200 114 ug/L 57 33 -117 0 20
4-Chlorophenyl phenyl ether 200 136 ug/L 68 53 -121 5 20
4-Nitroaniline 200 130 ug/L 65 55 -115 11 20
4-Nitrophenol 400 97.4 ug/L 24 13 -130 7 20
Acenaphthene 200 125 ug/L 63 47 -122 0 20
Acenaphthylene 200 131 ug/L 66 41 -130 2 20
Acetophenone 200 123 ug/L 62 46 -118 3 20
Anthracene 200 137 ug/L 68 57 -123 6 20
Atrazine 200 137 ug/L 69 44 -142 5 20
Azobenzene 200 120 Q ug/L 60 61 -116 0
Benzaldehyde 200 102 ug/L 51 25 -130 3 20
Benzo[a]anthracene 200 147 ug/L 73 58 -125 6 20
Benzo[a]pyrene 200 146 ug/L 73 54 -128 8 20
Benzo[b]fluoranthene 200 138 ug/L 69 53 -131 15 20
Benzo[g,h,i]perylene 200 147 ug/L 74 50 -134 6 20
Benzo[k]fluoranthene 200 144 ug/L 72 57 -129 3 20
Benzyl alcohol 200 87.4 ug/L 44 31 -112 4 20
bis (2-chloroisopropyl) ether 200 102 ug/L 51 37 -130 3 20
Bis(2-chloroethoxy)methane 200 117 ug/L 58 48 -120 3 20
Bis(2-chloroethyl)ether 200 98.5 ug/L 49 43 -118 0 20
Bis(2-ethylhexyl) phthalate 200 141 ug/L 71 55 -135 9 20
Butyl benzyl phthalate 200 150 ug/L 75 53 -134 11 20
Caprolactam 200 46.0 M ug/L 23 13 -130 5 20
Carbazole 200 139 ug/L 69 60 -122 7 20
Chrysene 200 140 ug/L 70 59 -123 8 20
Dibenz(a,h)anthracene 200 144 ug/L 72 51 -134 7 20
Dibenzofuran 200 130 ug/L 65 53 -118 1 20
Diethyl phthalate 200 137 ug/L 69 56 -125 8 20
Dimethyl phthalate 200 137 ug/L 68 45 -127 4 20
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-756109/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 756690 Prep Batch: 756109
Di-n-butyl phthalate 200 146 ug/L 73 56 -122 7 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Di-n-octyl phthalate 200 149 ug/L 75 59 -128 13 20
Diphenylamine 171 116 ug/L 68 55 -111 2 20
Fluoranthene 200 147 ug/L 74 57 -128 9 20
Fluorene 200 130 ug/L 65 52 -124 4 20
Hexachlorobenzene 200 159 ug/L 80 53 -125 3 20
Hexachlorobutadiene 200 117 ug/L 59 22 -124 2 20
Hexachlorocyclopentadiene 200 131 ug/L 65 28 -130 7 20
Hexachloroethane 200 96.0 ug/L 48 21 -115 1 20
Indeno[1,2,3-cd]pyrene 200 154 ug/L 77 52 -134 6 20
Isophorone 200 120 ug/L 60 42 -124 2 20
Naphthalene 200 114 ug/L 57 40 -121 3 20
Nitrobenzene 200 107 ug/L 53 45 -121 3 20
N-Nitrosodi-n-propylamine 200 108 ug/L 54 49 -119 0 20
N-Nitrosodiphenylamine 200 135 ug/L 68 51 -123 2 20
Pentachlorophenol 400 335 ug/L 84 35 -138 7 20
Phenanthrene 200 137 ug/L 69 59 -120 6 20
Phenol 200 37.3 ug/L 19 14 -130 2 20
Pyrene 200 144 ug/L 72 57 -126 9 20
2-Fluorobiphenyl (Surr)44 -119
Surrogate
59
LCSD LCSD
Qualifier Limits%Recovery
252-Fluorophenol (Surr)19 -119
52Nitrobenzene-d5 (Surr)44 -120
17Phenol-d5 (Surr)10 -130
73Terphenyl-d14 (Surr)50 -134
812,4,6-Tribromophenol (Surr)43 -140
Client Sample ID: Method BlankLab Sample ID: MB 680-756630/5-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756690 Prep Batch: 756630
LOQ DL
1,1'-Biphenyl 320 U M 1700 110 ug/Kg 12/22/22 19:00 12/23/22 16:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
66 U 30320 ug/Kg 12/22/22 19:00 12/23/22 16:38 11,2,4,5-Tetrachlorobenzene
66 U 30320 ug/Kg 12/22/22 19:00 12/23/22 16:38 11,2,4-Trichlorobenzene
66 U 36320 ug/Kg 12/22/22 19:00 12/23/22 16:38 11,2-Dichlorobenzene
66 U 33320 ug/Kg 12/22/22 19:00 12/23/22 16:38 11,2-Diphenylhydrazine
66 U 33320 ug/Kg 12/22/22 19:00 12/23/22 16:38 11,3-Dichlorobenzene
66 U 34320 ug/Kg 12/22/22 19:00 12/23/22 16:38 11,4-Dichlorobenzene
66 U 30320 ug/Kg 12/22/22 19:00 12/23/22 16:38 11-Methylnaphthalene
82 U 22320 ug/Kg 12/22/22 19:00 12/23/22 16:38 12,3,4,6-Tetrachlorophenol
66 U 34320 ug/Kg 12/22/22 19:00 12/23/22 16:38 12,4,5-Trichlorophenol
66 U 28320 ug/Kg 12/22/22 19:00 12/23/22 16:38 12,4,6-Trichlorophenol
66 U 34320 ug/Kg 12/22/22 19:00 12/23/22 16:38 12,4-Dichlorophenol
66 U M 43320 ug/Kg 12/22/22 19:00 12/23/22 16:38 12,4-Dimethylphenol
1300 U 8201700 ug/Kg 12/22/22 19:00 12/23/22 16:38 12,4-Dinitrophenol
82 U 48320 ug/Kg 12/22/22 19:00 12/23/22 16:38 12,4-Dinitrotoluene
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-756630/5-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756690 Prep Batch: 756630
LOQ DL
2,6-Dichlorophenol 66 U 320 27 ug/Kg 12/22/22 19:00 12/23/22 16:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
66 U 41320 ug/Kg 12/22/22 19:00 12/23/22 16:38 12,6-Dinitrotoluene
66 U 34320 ug/Kg 12/22/22 19:00 12/23/22 16:38 12-Chloronaphthalene
66 U 39320 ug/Kg 12/22/22 19:00 12/23/22 16:38 12-Chlorophenol
66 U 37320 ug/Kg 12/22/22 19:00 12/23/22 16:38 12-Methylnaphthalene
66 U 27320 ug/Kg 12/22/22 19:00 12/23/22 16:38 12-Methylphenol
170 U M 441700 ug/Kg 12/22/22 19:00 12/23/22 16:38 12-Nitroaniline
66 U 40320 ug/Kg 12/22/22 19:00 12/23/22 16:38 12-Nitrophenol
66 U 42320 ug/Kg 12/22/22 19:00 12/23/22 16:38 13 & 4 Methylphenol
66 U 28650 ug/Kg 12/22/22 19:00 12/23/22 16:38 13,3'-Dichlorobenzidine
82 U 451700 ug/Kg 12/22/22 19:00 12/23/22 16:38 13-Nitroaniline
320 U 1701700 ug/Kg 12/22/22 19:00 12/23/22 16:38 14,6-Dinitro-2-methylphenol
66 U 35320 ug/Kg 12/22/22 19:00 12/23/22 16:38 14-Bromophenyl phenyl ether
66 U 34320 ug/Kg 12/22/22 19:00 12/23/22 16:38 14-Chloro-3-methylphenol
82 U 51650 ug/Kg 12/22/22 19:00 12/23/22 16:38 14-Chloroaniline
66 U 43320 ug/Kg 12/22/22 19:00 12/23/22 16:38 14-Chlorophenyl phenyl ether
82 U 481700 ug/Kg 12/22/22 19:00 12/23/22 16:38 14-Nitroaniline
660 U 3201700 ug/Kg 12/22/22 19:00 12/23/22 16:38 14-Nitrophenol
66 U 40320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Acenaphthene
66 U 35320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Acenaphthylene
66 U 28320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Acetophenone
66 U 25320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Anthracene
66 U 23320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Atrazine
320 U 47320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Azobenzene
170 U 57320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Benzaldehyde
66 U 27320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Benzo[a]anthracene
82 U 51320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Benzo[a]pyrene
66 U 37320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Benzo[b]fluoranthene
66 U 22320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Benzo[g,h,i]perylene
170 U 64320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Benzo[k]fluoranthene
66 U M 32320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Benzyl alcohol
66 U 29320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1bis (2-chloroisopropyl) ether
66 U 38320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Bis(2-chloroethoxy)methane
82 U 44320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Bis(2-chloroethyl)ether
66 U M 28320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Bis(2-ethylhexyl) phthalate
66 U 26320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Butyl benzyl phthalate
170 U 65320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Caprolactam
66 U 29320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Carbazole
66 U 21320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Chrysene
66 U 38320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Dibenz(a,h)anthracene
66 U 32320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Dibenzofuran
66 U 36320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Diethyl phthalate
66 U 33320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Dimethyl phthalate
66 U 29320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Di-n-butyl phthalate
66 U 28320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Di-n-octyl phthalate
140 U 40320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Diphenylamine
66 U 31320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Fluoranthene
66 U M 35320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Fluorene
66 U 38320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Hexachlorobenzene
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-756630/5-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756690 Prep Batch: 756630
LOQ DL
Hexachlorobutadiene 66 U 320 35 ug/Kg 12/22/22 19:00 12/23/22 16:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
66 U 40320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Hexachlorocyclopentadiene
66 U 28320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Hexachloroethane
66 U 28320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Indeno[1,2,3-cd]pyrene
66 U 32320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Isophorone
66 U 29320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Naphthalene
66 U 26320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Nitrobenzene
66 U 31320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1N-Nitrosodi-n-propylamine
66 U 32320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1N-Nitrosodiphenylamine
660 U 3201700 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Pentachlorophenol
66 U 27320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Phenanthrene
66 U 33320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Phenol
66 U M 27320 ug/Kg 12/22/22 19:00 12/23/22 16:38 1Pyrene
2-Fluorobiphenyl (Surr)72 44-115 12/23/22 16:38 1
MB MB
Surrogate
12/22/22 19:00
Dil FacPreparedAnalyzedQualifierLimits%Recovery
60 12/22/22 19:00 12/23/22 16:38 12-Fluorophenol (Surr)35-115
58 12/22/22 19:00 12/23/22 16:38 1Nitrobenzene-d5 (Surr)37-122
61 12/22/22 19:00 12/23/22 16:38 1Phenol-d5 (Surr)33-122
80 12/22/22 19:00 12/23/22 16:38 1Terphenyl-d14 (Surr)54-127
87 12/22/22 19:00 12/23/22 16:38 12,4,6-Tribromophenol (Surr)39-132
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-756630/6-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756690 Prep Batch: 756630
1,1'-Biphenyl 6520 4250 ug/Kg 65 40 -117
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,2,4-Trichlorobenzene 6520 3970 ug/Kg 61 34 -118
1,2-Dichlorobenzene 6520 3390 ug/Kg 52 33 -117
1,2-Diphenylhydrazine 6520 4520 ug/Kg 69 41 -125
1,3-Dichlorobenzene 6520 3220 ug/Kg 49 30 -115
1,4-Dichlorobenzene 6520 3380 ug/Kg 52 31 -115
1-Methylnaphthalene 6520 3990 ug/Kg 61 40 -119
2,3,4,6-Tetrachlorophenol 6520 5870 ug/Kg 90 44 -125
2,4,5-Trichlorophenol 6520 5310 ug/Kg 81 41 -124
2,4,6-Trichlorophenol 6520 5250 ug/Kg 81 39 -126
2,4-Dichlorophenol 6520 4700 ug/Kg 72 40 -122
2,4-Dimethylphenol 6520 4310 ug/Kg 66 30 -127
2,4-Dinitrophenol 13000 10700 M ug/Kg 82 10 -130
2,4-Dinitrotoluene 6520 5390 ug/Kg 83 48 -126
2,6-Dinitrotoluene 6520 5200 ug/Kg 80 46 -124
2-Chloronaphthalene 6520 4240 ug/Kg 65 41 -114
2-Chlorophenol 6520 3860 ug/Kg 59 34 -121
2-Methylnaphthalene 6520 4390 ug/Kg 67 38 -122
2-Methylphenol 6520 3880 ug/Kg 59 32 -122
2-Nitroaniline 6520 4870 ug/Kg 75 44 -127
2-Nitrophenol 6520 4120 ug/Kg 63 36 -123
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-756630/6-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756690 Prep Batch: 756630
3 & 4 Methylphenol 6520 3950 ug/Kg 61 34 -119
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
3,3'-Dichlorobenzidine 6520 5420 ug/Kg 83 22 -121
3-Nitroaniline 6520 4990 ug/Kg 77 33 -119
4,6-Dinitro-2-methylphenol 13000 12400 ug/Kg 95 29 -132
4-Bromophenyl phenyl ether 6520 5480 ug/Kg 84 46 -124
4-Chloro-3-methylphenol 6520 4910 ug/Kg 75 45 -122
4-Chloroaniline 6520 4420 ug/Kg 68 17 -106
4-Chlorophenyl phenyl ether 6520 5020 ug/Kg 77 45 -121
4-Nitroaniline 6520 5150 ug/Kg 79 41 -130
4-Nitrophenol 13000 10600 ug/Kg 82 30 -132
Acenaphthene 6520 4560 ug/Kg 70 40 -123
Acenaphthylene 6520 4790 ug/Kg 74 32 -132
Acetophenone 6520 4050 ug/Kg 62 33 -115
Anthracene 6520 5250 ug/Kg 81 47 -123
Atrazine 6520 5290 ug/Kg 81 47 -127
Azobenzene 6520 4510 ug/Kg 69 44 -130
Benzaldehyde 6520 3940 ug/Kg 60 10 -130
Benzo[a]anthracene 6520 5580 ug/Kg 86 49 -126
Benzo[a]pyrene 6520 5450 ug/Kg 84 45 -129
Benzo[b]fluoranthene 6520 5030 ug/Kg 77 45 -132
Benzo[g,h,i]perylene 6520 5800 ug/Kg 89 43 -134
Benzo[k]fluoranthene 6520 5490 ug/Kg 84 47 -132
Benzyl alcohol 6520 4030 ug/Kg 62 29 -122
bis (2-chloroisopropyl) ether 6520 3330 ug/Kg 51 33 -131
Bis(2-chloroethoxy)methane 6520 3980 ug/Kg 61 36 -121
Bis(2-chloroethyl)ether 6520 3330 M ug/Kg 51 31 -120
Bis(2-ethylhexyl) phthalate 6520 5280 ug/Kg 81 51 -133
Butyl benzyl phthalate 6520 5610 ug/Kg 86 48 -132
Caprolactam 6520 6160 M ug/Kg 94 46 -117
Carbazole 6520 5300 ug/Kg 81 50 -123
Chrysene 6520 5250 ug/Kg 80 50 -124
Dibenz(a,h)anthracene 6520 5560 ug/Kg 85 45 -134
Dibenzofuran 6520 4720 ug/Kg 72 44 -120
Diethyl phthalate 6520 5080 ug/Kg 78 50 -124
Dimethyl phthalate 6520 5140 ug/Kg 79 48 -124
Di-n-butyl phthalate 6520 5390 ug/Kg 83 51 -128
Di-n-octyl phthalate 6520 5640 ug/Kg 87 45 -140
Diphenylamine 5570 4410 ug/Kg 79 38 -127
Fluoranthene 6520 5540 ug/Kg 85 50 -127
Fluorene 6520 4840 ug/Kg 74 43 -125
Hexachlorobenzene 6520 5940 ug/Kg 91 45 -122
Hexachlorobutadiene 6520 3850 ug/Kg 59 32 -123
Hexachlorocyclopentadiene 6520 4270 ug/Kg 65 28 -130
Hexachloroethane 6520 3250 ug/Kg 50 28 -117
Indeno[1,2,3-cd]pyrene 6520 5940 ug/Kg 91 45 -133
Isophorone 6520 4000 ug/Kg 61 30 -122
Naphthalene 6520 3790 ug/Kg 58 35 -123
Nitrobenzene 6520 3620 ug/Kg 56 34 -122
N-Nitrosodi-n-propylamine 6520 3510 ug/Kg 54 36 -120
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-756630/6-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756690 Prep Batch: 756630
N-Nitrosodiphenylamine 6520 5170 ug/Kg 79 38 -127
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Pentachlorophenol 13000 12800 ug/Kg 98 25 -133
Phenanthrene 6520 5210 ug/Kg 80 50 -121
Phenol 6520 3920 ug/Kg 60 34 -121
Pyrene 6520 5530 ug/Kg 85 47 -127
2-Fluorobiphenyl (Surr)44 -115
Surrogate
62
LCS LCS
Qualifier Limits%Recovery
572-Fluorophenol (Surr)35 -115
54Nitrobenzene-d5 (Surr)37 -122
57Phenol-d5 (Surr)33 -122
83Terphenyl-d14 (Surr)54 -127
922,4,6-Tribromophenol (Surr)39 -132
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 410-328291/21-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 333572 Prep Batch: 328291
LOQ DL
Benzene 0.080 U 0.10 0.040 mg/Kg 01/10/23 11:40 01/10/23 13:52 50
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
2.5 U 1.35.0 mg/Kg 01/10/23 11:40 01/10/23 13:52 50C5-C8 Aliphatics
2.5 U 1.35.0 mg/Kg 01/10/23 11:40 01/10/23 13:52 50C9-C10 Aromatics
2.5 U 1.35.0 mg/Kg 01/10/23 11:40 01/10/23 13:52 50C9-C12 Aliphatics
0.080 U 0.0400.10 mg/Kg 01/10/23 11:40 01/10/23 13:52 50Ethylbenzene
0.080 U 0.0400.10 mg/Kg 01/10/23 11:40 01/10/23 13:52 50Methyl tert-butyl ether
0.20 U 0.100.30 mg/Kg 01/10/23 11:40 01/10/23 13:52 50Naphthalene
0.080 U 0.0400.10 mg/Kg 01/10/23 11:40 01/10/23 13:52 50Toluene
2.5 U 1.35.0 mg/Kg 01/10/23 11:40 01/10/23 13:52 50C9-C12 Aliphatics (adjusted)
0.20 U 0.100.25 mg/Kg 01/10/23 11:40 01/10/23 13:52 50m-Xylene & p-Xylene
0.080 U 0.0400.10 mg/Kg 01/10/23 11:40 01/10/23 13:52 50o-Xylene
2.5 U 1.35.0 mg/Kg 01/10/23 11:40 01/10/23 13:52 50C5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)97 70-130 01/10/23 13:52 50
MB MB
Surrogate
01/10/23 11:40
Dil FacPreparedAnalyzedQualifierLimits%Recovery
90 01/10/23 11:40 01/10/23 13:52 50a,a,a-Trifluorotoluene (pid)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-328291/22-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 333572 Prep Batch: 328291
Benzene 2.50 2.21 D mg/Kg 88 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Ethylbenzene 2.50 2.33 D mg/Kg 93 70 -130
Methyl tert-butyl ether 2.51 2.11 D mg/Kg 84 70 -130
Naphthalene 2.51 2.19 D mg/Kg 87 70 -130
Toluene 2.50 2.23 D mg/Kg 89 70 -130
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-328291/22-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 333572 Prep Batch: 328291
m-Xylene & p-Xylene 5.03 4.74 D mg/Kg 94 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
o-Xylene 2.52 2.35 D mg/Kg 93 70 -130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
96
LCS LCS
Qualifier Limits%Recovery
94a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-328291/23-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 333572 Prep Batch: 328291
Benzene 2.50 2.28 D mg/Kg 91 70 -130 3 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Ethylbenzene 2.50 2.36 D mg/Kg 94 70 -130 2 30
Methyl tert-butyl ether 2.51 2.22 D mg/Kg 88 70 -130 5 30
Naphthalene 2.51 2.22 D mg/Kg 88 70 -130 1 30
Toluene 2.50 2.28 D mg/Kg 91 70 -130 2 30
m-Xylene & p-Xylene 5.03 4.78 D mg/Kg 95 70 -130 1 30
o-Xylene 2.52 2.37 D mg/Kg 94 70 -130 1 30
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
96
LCSD LCSD
Qualifier Limits%Recovery
96a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Method BlankLab Sample ID: MB 410-330695/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 330695
LOQ DL
Benzene 2.0 U 5.0 1.0 ug/L 12/28/22 10:28 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
50 U 25100 ug/L 12/28/22 10:28 1C5-C8 Aliphatics
20 U 10100 ug/L 12/28/22 10:28 1C9-C10 Aromatics
50 U 25100 ug/L 12/28/22 10:28 1C9-C12 Aliphatics
2.0 U 1.05.0 ug/L 12/28/22 10:28 1Ethylbenzene
2.0 U 1.05.0 ug/L 12/28/22 10:28 1Methyl tert-butyl ether
4.0 U 2.06.0 ug/L 12/28/22 10:28 1Naphthalene
2.0 U 1.05.0 ug/L 12/28/22 10:28 1Toluene
50 U 25100 ug/L 12/28/22 10:28 1C9-C12 Aliphatics (adjusted)
5.0 U 2.510 ug/L 12/28/22 10:28 1m-Xylene & p-Xylene
2.0 U 1.05.0 ug/L 12/28/22 10:28 1o-Xylene
50 U 25100 ug/L 12/28/22 10:28 1C5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)102 70-130 12/28/22 10:28 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
93 12/28/22 10:28 1a,a,a-Trifluorotoluene (pid)70-130
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-330695/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 330695
Benzene 50.1 42.9 ug/L 86 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Ethylbenzene 50.1 43.9 ug/L 88 70 -130
Methyl tert-butyl ether 50.2 32.0 Q ug/L 64 70 -130
Naphthalene 50.2 48.5 ug/L 97 70 -130
Toluene 50.1 42.7 ug/L 85 70 -130
m-Xylene & p-Xylene 101 88.7 ug/L 88 70 -130
o-Xylene 50.4 44.0 ug/L 87 70 -130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
103
LCS LCS
Qualifier Limits%Recovery
95a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-330695/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 330695
Benzene 50.1 43.1 ug/L 86 70 -130 0 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Ethylbenzene 50.1 43.9 ug/L 88 70 -130 0 25
Methyl tert-butyl ether 50.2 30.6 Q ug/L 61 70 -130 4 25
Naphthalene 50.2 44.6 ug/L 89 70 -130 8 25
Toluene 50.1 42.5 ug/L 85 70 -130 0 25
m-Xylene & p-Xylene 101 88.9 ug/L 88 70 -130 0 25
o-Xylene 50.4 43.8 ug/L 87 70 -130 1 25
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
103
LCSD LCSD
Qualifier Limits%Recovery
95a,a,a-Trifluorotoluene (pid)70 -130
Method: 8081B 8082A - Organochlorine Pesticides & PCBs (GC)
Client Sample ID: Method BlankLab Sample ID: MB 680-755500/7-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 755553 Prep Batch: 755500
LOQ DL
alpha-Chlordane 0.22 U 0.82 0.087 ug/Kg 12/16/22 13:33 12/16/22 20:19 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.16 U M 0.0720.82 ug/Kg 12/16/22 13:33 12/16/22 20:19 1Aldrin
0.16 U 0.0680.82 ug/Kg 12/16/22 13:33 12/16/22 20:19 1alpha-BHC
0.22 U 0.0870.82 ug/Kg 12/16/22 13:33 12/16/22 20:19 14,4'-DDD
0.48 U 0.160.82 ug/Kg 12/16/22 13:33 12/16/22 20:19 1beta-BHC
0.22 U 0.0870.82 ug/Kg 12/16/22 13:33 12/16/22 20:19 14,4'-DDE
0.22 U 0.110.82 ug/Kg 12/16/22 13:33 12/16/22 20:19 14,4'-DDT
0.22 U M 0.0920.82 ug/Kg 12/16/22 13:33 12/16/22 20:19 1delta-BHC
0.22 U 0.0820.82 ug/Kg 12/16/22 13:33 12/16/22 20:19 1Dieldrin
0.22 U 0.0820.82 ug/Kg 12/16/22 13:33 12/16/22 20:19 1Endosulfan I
0.16 U 0.0720.82 ug/Kg 12/16/22 13:33 12/16/22 20:19 1Endosulfan II
0.22 U 0.110.82 ug/Kg 12/16/22 13:33 12/16/22 20:19 1Endosulfan sulfate
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8081B 8082A - Organochlorine Pesticides & PCBs (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-755500/7-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 755553 Prep Batch: 755500
LOQ DL
Endrin 0.22 U 0.82 0.11 ug/Kg 12/16/22 13:33 12/16/22 20:19 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.22 U 0.110.82 ug/Kg 12/16/22 13:33 12/16/22 20:19 1Endrin aldehyde
0.22 U M 0.0970.82 ug/Kg 12/16/22 13:33 12/16/22 20:19 1Endrin ketone
0.16 U 0.0680.82 ug/Kg 12/16/22 13:33 12/16/22 20:19 1gamma-BHC (Lindane)
0.22 U 0.0920.82 ug/Kg 12/16/22 13:33 12/16/22 20:19 1Heptachlor
0.22 U 0.0770.82 ug/Kg 12/16/22 13:33 12/16/22 20:19 1Heptachlor epoxide
0.32 U 0.140.82 ug/Kg 12/16/22 13:33 12/16/22 20:19 1Methoxychlor
9.7 U 5.316 ug/Kg 12/16/22 13:33 12/16/22 20:19 1PCB-1221
9.7 U 5.316 ug/Kg 12/16/22 13:33 12/16/22 20:19 1PCB-1242
9.7 U 5.316 ug/Kg 12/16/22 13:33 12/16/22 20:19 1PCB-1254
11 U 2.782 ug/Kg 12/16/22 13:33 12/16/22 20:19 1Toxaphene
19 U 5.324 ug/Kg 12/16/22 13:33 12/16/22 20:19 1PCB-1016
9.7 U 5.316 ug/Kg 12/16/22 13:33 12/16/22 20:19 1PCB-1248
9.7 U 5.316 ug/Kg 12/16/22 13:33 12/16/22 20:19 1PCB-1232
DCB Decachlorobiphenyl 128 44-129 12/16/22 20:19 1
MB MB
Surrogate
12/16/22 13:33
Dil FacPreparedAnalyzedQualifierLimits%Recovery
107 12/16/22 13:33 12/16/22 20:19 1Tetrachloro-m-xylene (Surr)42-129
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-755500/11-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 755553 Prep Batch: 755500
PCB-1260 196 239 ug/Kg 122 53 -140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
PCB-1016 196 204 ug/Kg 104 47 -134
DCB Decachlorobiphenyl 44 -129
Surrogate
115
LCS LCS
Qualifier Limits%Recovery
100Tetrachloro-m-xylene (Surr)42 -129
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-755500/8-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 755553 Prep Batch: 755500
alpha-Chlordane 3.18 3.44 ug/Kg 108 54 -133
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Aldrin 3.18 3.40 ug/Kg 107 45 -136
alpha-BHC 3.18 3.26 ug/Kg 102 45 -137
beta-BHC 3.18 3.21 ug/Kg 101 50 -136
4,4'-DDT 3.18 3.70 ug/Kg 116 50 -141
Dieldrin 3.18 3.48 ug/Kg 109 56 -136
Endosulfan I 3.18 3.32 ug/Kg 104 53 -132
Endosulfan II 3.18 3.18 ug/Kg 100 53 -134
Endosulfan sulfate 3.18 3.26 ug/Kg 102 55 -136
Endrin 3.18 3.73 ug/Kg 117 57 -140
Endrin aldehyde 3.18 2.60 ug/Kg 82 35 -137
Endrin ketone 3.18 4.30 ug/Kg 135 55 -136
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8081B 8082A - Organochlorine Pesticides & PCBs (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-755500/8-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 755553 Prep Batch: 755500
gamma-BHC (Lindane)3.18 3.33 ug/Kg 105 49 -135
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Heptachlor 3.18 3.29 ug/Kg 103 47 -136
Heptachlor epoxide 3.18 3.39 ug/Kg 106 52 -136
Methoxychlor 3.18 3.17 ug/Kg 100 52 -143
DCB Decachlorobiphenyl 44 -129
Surrogate
105
LCS LCS
Qualifier Limits%Recovery
93Tetrachloro-m-xylene (Surr)42 -129
Client Sample ID: 149-SB-1-6-12-22Lab Sample ID: 680-227663-1 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 755553 Prep Batch: 755500
alpha-Chlordane 0.28 U 4.11 4.91 ug/Kg 120 54 -133☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Aldrin 0.21 U 4.11 4.34 ug/Kg 106 45 -136☼
alpha-BHC 0.21 U 4.11 4.21 ug/Kg 103 45 -137☼
4,4'-DDD 0.28 U 4.11 4.64 ug/Kg 113 56 -139☼
beta-BHC 0.61 U 4.11 4.19 ug/Kg 102 50 -136☼
4,4'-DDE 0.22 J 4.11 4.93 ug/Kg 115 56 -134☼
4,4'-DDT 0.15 J 4.11 4.65 ug/Kg 110 50 -141☼
delta-BHC 0.28 U J1 4.11 4.82 ug/Kg 117 47 -139☼
Dieldrin 0.28 U M 4.11 4.54 ug/Kg 111 56 -136☼
Endosulfan I 0.28 U 4.11 3.82 ug/Kg 93 53 -132☼
Endosulfan II 0.21 U 4.11 3.59 ug/Kg 87 53 -134☼
Endosulfan sulfate 0.28 U M 4.11 3.26 ug/Kg 79 55 -136☼
Endrin 0.28 U 4.11 4.73 ug/Kg 115 57 -140☼
Endrin aldehyde 0.28 U 4.11 2.32 ug/Kg 57 35 -137☼
Endrin ketone 0.28 U 4.11 5.59 ug/Kg 136 55 -136☼
gamma-BHC (Lindane)0.21 U 4.11 4.01 ug/Kg 98 49 -135☼
Heptachlor 0.28 U 4.11 4.15 ug/Kg 101 47 -136☼
Heptachlor epoxide 0.28 U 4.11 4.20 ug/Kg 102 52 -136☼
Methoxychlor 0.41 U 4.11 3.75 ug/Kg 91 52 -143☼
DCB Decachlorobiphenyl 44 -129
Surrogate
97
MS MS
Qualifier Limits%Recovery
96Tetrachloro-m-xylene (Surr)42 -129
Client Sample ID: 149-SB-1-6-12-22Lab Sample ID: 680-227663-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 755553 Prep Batch: 755500
alpha-Chlordane 0.28 U 4.10 4.05 ug/Kg 99 54 -133 19 30☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
Aldrin 0.21 U 4.10 3.59 M ug/Kg 88 45 -136 19 30☼
alpha-BHC 0.21 U 4.10 3.49 ug/Kg 85 45 -137 19 30☼
4,4'-DDD 0.28 U 4.10 3.86 ug/Kg 94 56 -139 18 30☼
beta-BHC 0.61 U 4.10 3.09 ug/Kg 75 50 -136 30 30☼
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8081B 8082A - Organochlorine Pesticides & PCBs (GC) (Continued)
Client Sample ID: 149-SB-1-6-12-22Lab Sample ID: 680-227663-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 755553 Prep Batch: 755500
4,4'-DDE 0.22 J 4.10 4.12 ug/Kg 95 56 -134 18 30☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
4,4'-DDT 0.15 J 4.10 4.26 ug/Kg 100 50 -141 9 30☼
delta-BHC 0.28 U J1 4.10 3.41 J1 ug/Kg 83 47 -139 34 30☼
Dieldrin 0.28 U M 4.10 3.79 ug/Kg 92 56 -136 18 30☼
Endosulfan I 0.28 U 4.10 3.13 ug/Kg 76 53 -132 20 30☼
Endosulfan II 0.21 U 4.10 3.10 ug/Kg 76 53 -134 15 30☼
Endosulfan sulfate 0.28 U M 4.10 3.11 ug/Kg 76 55 -136 5 30☼
Endrin 0.28 U 4.10 3.79 ug/Kg 93 57 -140 22 30☼
Endrin aldehyde 0.28 U 4.10 2.39 ug/Kg 58 35 -137 3 30☼
Endrin ketone 0.28 U 4.10 6.12 J1 ug/Kg 149 55 -136 9 30☼
gamma-BHC (Lindane)0.21 U 4.10 3.42 ug/Kg 83 49 -135 16 30☼
Heptachlor 0.28 U 4.10 3.43 ug/Kg 84 47 -136 19 30☼
Heptachlor epoxide 0.28 U 4.10 3.52 ug/Kg 86 52 -136 18 30☼
Methoxychlor 0.41 U 4.10 4.64 ug/Kg 113 52 -143 21 30☼
DCB Decachlorobiphenyl 44 -129
Surrogate
74
MSD MSD
Qualifier Limits%Recovery
76Tetrachloro-m-xylene (Surr)42 -129
Client Sample ID: Method BlankLab Sample ID: MB 680-756376/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 756577 Prep Batch: 756376
LOQ DL
Aldrin 0.0040 U 0.050 0.0020 ug/L 12/21/22 13:43 12/22/22 17:29 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.0040 U 0.00100.050 ug/L 12/21/22 13:43 12/22/22 17:29 1alpha-BHC
0.0040 U 0.00200.050 ug/L 12/21/22 13:43 12/22/22 17:29 14,4'-DDD
0.0040 U 0.00200.050 ug/L 12/21/22 13:43 12/22/22 17:29 1beta-BHC
0.0040 U 0.00100.050 ug/L 12/21/22 13:43 12/22/22 17:29 14,4'-DDE
0.0040 U 0.00100.050 ug/L 12/21/22 13:43 12/22/22 17:29 14,4'-DDT
0.0040 U 0.00200.050 ug/L 12/21/22 13:43 12/22/22 17:29 1delta-BHC
0.0040 U 0.00200.050 ug/L 12/21/22 13:43 12/22/22 17:29 1Dieldrin
0.0040 U 0.00200.050 ug/L 12/21/22 13:43 12/22/22 17:29 1Endosulfan I
0.0040 U 0.00200.050 ug/L 12/21/22 13:43 12/22/22 17:29 1Endosulfan II
0.0040 U 0.00200.050 ug/L 12/21/22 13:43 12/22/22 17:29 1Endosulfan sulfate
0.0040 U 0.00100.050 ug/L 12/21/22 13:43 12/22/22 17:29 1Endrin
0.016 U 0.00400.050 ug/L 12/21/22 13:43 12/22/22 17:29 1Endrin aldehyde
0.016 U 0.00400.050 ug/L 12/21/22 13:43 12/22/22 17:29 1Endrin ketone
0.0040 U M 0.00100.050 ug/L 12/21/22 13:43 12/22/22 17:29 1gamma-BHC (Lindane)
0.0040 U 0.00100.050 ug/L 12/21/22 13:43 12/22/22 17:29 1Heptachlor
0.40 U M 0.160.50 ug/L 12/21/22 13:43 12/22/22 17:29 1Chlordane (technical)
0.0040 U 0.00200.050 ug/L 12/21/22 13:43 12/22/22 17:29 1Heptachlor epoxide
0.0040 U M 0.00200.050 ug/L 12/21/22 13:43 12/22/22 17:29 1Methoxychlor
0.72 U 0.341.0 ug/L 12/21/22 13:43 12/22/22 17:29 1PCB-1221
0.72 U 0.341.0 ug/L 12/21/22 13:43 12/22/22 17:29 1PCB-1242
0.72 U 0.341.0 ug/L 12/21/22 13:43 12/22/22 17:29 1PCB-1254
0.72 U 0.341.0 ug/L 12/21/22 13:43 12/22/22 17:29 1PCB-1260
0.80 U 0.315.0 ug/L 12/21/22 13:43 12/22/22 17:29 1Toxaphene
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8081B 8082A - Organochlorine Pesticides & PCBs (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-756376/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 756577 Prep Batch: 756376
LOQ DL
PCB-1016 0.72 U 1.0 0.32 ug/L 12/21/22 13:43 12/22/22 17:29 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.72 U 0.341.0 ug/L 12/21/22 13:43 12/22/22 17:29 1PCB-1248
0.72 U 0.341.0 ug/L 12/21/22 13:43 12/22/22 17:29 1PCB-1232
DCB Decachlorobiphenyl 103 14-130 12/22/22 17:29 1
MB MB
Surrogate
12/21/22 13:43
Dil FacPreparedAnalyzedQualifierLimits%Recovery
60 12/21/22 13:43 12/22/22 17:29 1Tetrachloro-m-xylene (Surr)44-124
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-756376/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 756577 Prep Batch: 756376
Aldrin 0.0400 0.0351 J ug/L 88 45 -134
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
alpha-BHC 0.0400 0.0339 J ug/L 85 54 -138
4,4'-DDD 0.0400 0.0428 J ug/L 107 56 -143
beta-BHC 0.0400 0.0540 ug/L 135 56 -136
4,4'-DDE 0.0400 0.0403 J ug/L 101 57 -135
4,4'-DDT 0.0400 0.0582 ug/L 145 51 -143
delta-BHC 0.0400 0.0511 ug/L 128 52 -142
Dieldrin 0.0400 0.0368 J ug/L 92 60 -136
Endosulfan I 0.0400 0.0320 J ug/L 80 62 -126
Endosulfan II 0.0400 0.0302 J ug/L 76 52 -135
Endosulfan sulfate 0.0400 0.0521 ug/L 130 62 -133
Endrin 0.0400 0.0435 J ug/L 109 60 -138
Endrin aldehyde 0.0400 0.0375 J ug/L 94 51 -132
Endrin ketone 0.0400 0.0540 Q ug/L 135 58 -134
gamma-BHC (Lindane)0.0400 0.0356 J ug/L 89 59 -134
Heptachlor 0.0400 0.0390 J ug/L 97 54 -130
Heptachlor epoxide 0.0400 0.0373 J ug/L 93 61 -133
Methoxychlor 0.0400 0.0550 ug/L 138 54 -145
DCB Decachlorobiphenyl 14 -130
Surrogate
99
LCS LCS
Qualifier Limits%Recovery
61Tetrachloro-m-xylene (Surr)44 -124
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-756376/5-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 756577 Prep Batch: 756376
PCB-1260 2.40 1.96 ug/L 82 45 -134
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
PCB-1016 2.40 2.08 ug/L 87 46 -129
DCB Decachlorobiphenyl 14 -130
Surrogate
83
LCS LCS
Qualifier Limits%Recovery
68Tetrachloro-m-xylene (Surr)44 -124
Eurofins Savannah
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 8081B 8082A - Organochlorine Pesticides & PCBs (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-756376/6-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 756577 Prep Batch: 756376
PCB-1260 2.40 2.09 ug/L 87 45 -134 6 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
PCB-1016 2.40 2.40 ug/L 100 46 -129 14 30
DCB Decachlorobiphenyl 14 -130
Surrogate
107
LCSD LCSD
Qualifier Limits%Recovery
67Tetrachloro-m-xylene (Surr)44 -124
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 410-328608/1-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 329942 Prep Batch: 328608
LOQ DL
C19-C36 Aliphatics 20 U 50 10 ug/L 12/19/22 18:32 12/22/22 17:47 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
13.2 J 1030 ug/L 12/19/22 18:32 12/22/22 17:47 1C9-C18 Aliphatics
1-Chlorooctadecane (Surr)74 40-140 12/22/22 17:47 1
MB MB
Surrogate
12/19/22 18:32
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 410-328608/1-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 329935 Prep Batch: 328608
LOQ DL
Anthracene 1.2 U 2.0 0.60 ug/L 12/19/22 18:32 12/22/22 17:47 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
1.2 U 0.602.0 ug/L 12/19/22 18:32 12/22/22 17:47 1Benzo[b]fluoranthene
1.2 U 0.602.0 ug/L 12/19/22 18:32 12/22/22 17:47 1Benzo[g,h,i]perylene
1.4 U 0.702.0 ug/L 12/19/22 18:32 12/22/22 17:47 1Acenaphthylene
3.0 U 1.54.0 ug/L 12/19/22 18:32 12/22/22 17:47 1Benzo[k]fluoranthene
1.2 U 0.602.0 ug/L 12/19/22 18:32 12/22/22 17:47 1Benzo[a]pyrene
1.4 U 0.702.0 ug/L 12/19/22 18:32 12/22/22 17:47 1Benzo[a]anthracene
1.2 U 0.602.0 ug/L 12/19/22 18:32 12/22/22 17:47 1Acenaphthene
1.0 U 0.502.0 ug/L 12/19/22 18:32 12/22/22 17:47 1Chrysene
1.0 U 0.502.0 ug/L 12/19/22 18:32 12/22/22 17:47 1Dibenz(a,h)anthracene
1.0 U 0.502.0 ug/L 12/19/22 18:32 12/22/22 17:47 1Fluoranthene
1.2 U 0.602.0 ug/L 12/19/22 18:32 12/22/22 17:47 1Fluorene
30 U 1040 ug/L 12/19/22 18:32 12/22/22 17:47 1C11-C22 Aromatics (unadjusted)
1.2 U 0.602.0 ug/L 12/19/22 18:32 12/22/22 17:47 1Indeno[1,2,3-cd]pyrene
1.2 U 0.602.0 ug/L 12/19/22 18:32 12/22/22 17:47 12-Methylnaphthalene
30 U 1040 ug/L 12/19/22 18:32 12/22/22 17:47 1C11-C22 Aromatics (Adjusted)
1.2 U 0.602.0 ug/L 12/19/22 18:32 12/22/22 17:47 1Naphthalene
1.2 U 0.602.0 ug/L 12/19/22 18:32 12/22/22 17:47 1Phenanthrene
10 U 5.012 ug/L 12/19/22 18:32 12/22/22 17:47 1Pyrene
2-Fluorobiphenyl (Surr)76 40-140 12/22/22 17:47 1
MB MB
Surrogate
12/19/22 18:32
Dil FacPreparedAnalyzedQualifierLimits%Recovery
69 12/19/22 18:32 12/22/22 17:47 1o- terphenyl (Surr)40-140
Eurofins Savannah
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-328608/2-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 329942 Prep Batch: 328608
C19-C36 Aliphatics 321 248 ug/L 77 40 -140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C18 Aliphatics 241 160 ug/L 66 40 -140
1-Chlorooctadecane (Surr)40 -140
Surrogate
69
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-328608/2-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 329935 Prep Batch: 328608
Anthracene 40.0 32.0 ug/L 80 40 -140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Benzo[b]fluoranthene 40.2 33.1 M ug/L 82 40 -140
Benzo[g,h,i]perylene 40.1 30.7 ug/L 76 40 -140
Acenaphthylene 40.0 31.0 ug/L 77 40 -140
Benzo[k]fluoranthene 40.1 28.9 M ug/L 72 40 -140
Benzo[a]pyrene 40.0 30.6 ug/L 76 40 -140
Benzo[a]anthracene 40.2 32.2 M ug/L 80 40 -140
Acenaphthene 40.0 29.9 ug/L 75 40 -140
Chrysene 40.0 30.2 M ug/L 75 40 -140
Dibenz(a,h)anthracene 40.0 30.5 M ug/L 76 40 -140
Fluoranthene 40.0 31.2 ug/L 78 40 -140
Fluorene 40.1 30.0 ug/L 75 40 -140
C11-C22 Aromatics (unadjusted)681 522 M ug/L 77 40 -140
Indeno[1,2,3-cd]pyrene 40.0 30.6 M ug/L 77 40 -140
2-Methylnaphthalene 40.1 27.3 ug/L 68 40 -140
Naphthalene 40.0 27.3 M ug/L 68 40 -140
Phenanthrene 40.1 31.4 ug/L 78 40 -140
Pyrene 40.1 31.1 ug/L 77 40 -140
2-Fluorobiphenyl (Surr)40 -140
Surrogate
84
LCS LCS
Qualifier Limits%Recovery
75o- terphenyl (Surr)40 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-328608/3-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 329942 Prep Batch: 328608
C19-C36 Aliphatics 321 267 ug/L 83 40 -140 8 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C18 Aliphatics 241 164 ug/L 68 40 -140 3 25
1-Chlorooctadecane (Surr)40 -140
Surrogate
74
LCSD LCSD
Qualifier Limits%Recovery
Eurofins Savannah
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-328608/3-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 329935 Prep Batch: 328608
Anthracene 40.0 33.1 ug/L 83 40 -140 3 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Benzo[b]fluoranthene 40.2 33.4 M ug/L 83 40 -140 1 25
Benzo[g,h,i]perylene 40.1 31.6 ug/L 79 40 -140 3 25
Acenaphthylene 40.0 31.5 ug/L 79 40 -140 2 25
Benzo[k]fluoranthene 40.1 30.8 M ug/L 77 40 -140 6 25
Benzo[a]pyrene 40.0 31.7 ug/L 79 40 -140 4 25
Benzo[a]anthracene 40.2 33.2 ug/L 83 40 -140 3 25
Acenaphthene 40.0 30.7 ug/L 77 40 -140 3 25
Chrysene 40.0 31.7 ug/L 79 40 -140 5 25
Dibenz(a,h)anthracene 40.0 31.2 M ug/L 78 40 -140 2 25
Fluoranthene 40.0 32.7 ug/L 82 40 -140 5 25
Fluorene 40.1 30.7 ug/L 77 40 -140 2 25
C11-C22 Aromatics (unadjusted)681 539 M ug/L 79 40 -140 3 25
Indeno[1,2,3-cd]pyrene 40.0 31.6 M ug/L 79 40 -140 3 25
2-Methylnaphthalene 40.1 27.4 ug/L 68 40 -140 0 25
Naphthalene 40.0 27.1 M ug/L 68 40 -140 1 25
Phenanthrene 40.1 32.5 ug/L 81 40 -140 4 25
Pyrene 40.1 32.5 ug/L 81 40 -140 5 25
2-Fluorobiphenyl (Surr)40 -140
Surrogate
84
LCSD LCSD
Qualifier Limits%Recovery
77o- terphenyl (Surr)40 -140
Client Sample ID: Method BlankLab Sample ID: MB 410-329945/1-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 331708 Prep Batch: 329945
LOQ DL
C19-C36 Aliphatics 3.8 U 12 1.9 mg/Kg 12/22/22 15:40 12/30/22 23:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
3.0 U 1.56.0 mg/Kg 12/22/22 15:40 12/30/22 23:03 1C9-C18 Aliphatics
1-Chlorooctadecane (Surr)66 40-140 12/30/22 23:03 1
MB MB
Surrogate
12/22/22 15:40
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 410-329945/1-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 331706 Prep Batch: 329945
LOQ DL
Anthracene 0.40 U 0.50 0.20 mg/Kg 12/22/22 15:40 12/30/22 23:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.40 U 0.200.50 mg/Kg 12/22/22 15:40 12/30/22 23:03 1Benzo[b]fluoranthene
0.40 U 0.200.50 mg/Kg 12/22/22 15:40 12/30/22 23:03 1Benzo[g,h,i]perylene
0.40 U 0.200.50 mg/Kg 12/22/22 15:40 12/30/22 23:03 1Acenaphthylene
0.40 U 0.200.50 mg/Kg 12/22/22 15:40 12/30/22 23:03 1Benzo[k]fluoranthene
0.40 U 0.200.50 mg/Kg 12/22/22 15:40 12/30/22 23:03 1Benzo[a]pyrene
0.40 U 0.200.50 mg/Kg 12/22/22 15:40 12/30/22 23:03 1Benzo[a]anthracene
0.40 U 0.200.50 mg/Kg 12/22/22 15:40 12/30/22 23:03 1Acenaphthene
0.40 U 0.200.50 mg/Kg 12/22/22 15:40 12/30/22 23:03 1Chrysene
Eurofins Savannah
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 410-329945/1-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 331706 Prep Batch: 329945
LOQ DL
Dibenz(a,h)anthracene 0.40 U 0.50 0.20 mg/Kg 12/22/22 15:40 12/30/22 23:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.40 U 0.200.50 mg/Kg 12/22/22 15:40 12/30/22 23:03 1Fluoranthene
0.40 U 0.200.50 mg/Kg 12/22/22 15:40 12/30/22 23:03 1Fluorene
8.4 U M 4.212 mg/Kg 12/22/22 15:40 12/30/22 23:03 1C11-C22 Aromatics
0.40 U 0.200.50 mg/Kg 12/22/22 15:40 12/30/22 23:03 1Indeno[1,2,3-cd]pyrene
0.40 U 0.200.50 mg/Kg 12/22/22 15:40 12/30/22 23:03 12-Methylnaphthalene
8.4 U 4.212 mg/Kg 12/22/22 15:40 12/30/22 23:03 1C11-C22 Aromatics (Adjusted)
0.40 U M 0.200.50 mg/Kg 12/22/22 15:40 12/30/22 23:03 1Naphthalene
0.40 U 0.200.50 mg/Kg 12/22/22 15:40 12/30/22 23:03 1Phenanthrene
1.6 U 0.702.0 mg/Kg 12/22/22 15:40 12/30/22 23:03 1Pyrene
2-Fluorobiphenyl (Surr)82 40-140 12/30/22 23:03 1
MB MB
Surrogate
12/22/22 15:40
Dil FacPreparedAnalyzedQualifierLimits%Recovery
71 12/22/22 15:40 12/30/22 23:03 1o- terphenyl (Surr)40-140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-329945/2-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 331708 Prep Batch: 329945
C19-C36 Aliphatics 32.1 24.5 mg/Kg 76 40 -140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C18 Aliphatics 24.1 18.9 mg/Kg 78 40 -140
1-Chlorooctadecane (Surr)40 -140
Surrogate
62
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-329945/2-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 331706 Prep Batch: 329945
Anthracene 4.00 3.15 mg/Kg 79 40 -140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Benzo[b]fluoranthene 4.02 3.21 M mg/Kg 80 40 -140
Benzo[g,h,i]perylene 4.01 3.02 mg/Kg 75 40 -140
Acenaphthylene 4.00 2.98 mg/Kg 74 40 -140
Benzo[k]fluoranthene 4.01 2.99 M mg/Kg 74 40 -140
Benzo[a]pyrene 4.00 3.04 mg/Kg 76 40 -140
Benzo[a]anthracene 4.02 3.15 M mg/Kg 78 40 -140
Acenaphthene 4.00 2.96 mg/Kg 74 40 -140
Chrysene 4.00 3.02 M mg/Kg 75 40 -140
Dibenz(a,h)anthracene 4.00 2.97 M mg/Kg 74 40 -140
Fluoranthene 4.00 2.97 mg/Kg 74 40 -140
Fluorene 4.01 2.84 mg/Kg 71 40 -140
C11-C22 Aromatics 68.1 51.3 M mg/Kg 75 40 -140
Indeno[1,2,3-cd]pyrene 4.00 3.03 M mg/Kg 76 40 -140
2-Methylnaphthalene 4.01 2.97 mg/Kg 74 40 -140
Naphthalene 4.00 2.98 M mg/Kg 74 40 -140
Phenanthrene 4.01 2.97 mg/Kg 74 40 -140
Eurofins Savannah
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-329945/2-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 331706 Prep Batch: 329945
Pyrene 4.01 2.96 mg/Kg 74 40 -140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2-Fluorobiphenyl (Surr)40 -140
Surrogate
86
LCS LCS
Qualifier Limits%Recovery
74o- terphenyl (Surr)40 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-329945/3-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 331708 Prep Batch: 329945
C19-C36 Aliphatics 32.1 21.1 mg/Kg 66 40 -140 15 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C18 Aliphatics 24.1 17.1 mg/Kg 71 40 -140 10 25
1-Chlorooctadecane (Surr)40 -140
Surrogate
56
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-329945/3-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 331706 Prep Batch: 329945
Anthracene 4.00 2.70 mg/Kg 67 40 -140 15 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Benzo[b]fluoranthene 4.02 2.68 M mg/Kg 67 40 -140 18 25
Benzo[g,h,i]perylene 4.01 2.58 mg/Kg 64 40 -140 16 25
Acenaphthylene 4.00 2.68 mg/Kg 67 40 -140 11 25
Benzo[k]fluoranthene 4.01 2.53 M mg/Kg 63 40 -140 17 25
Benzo[a]pyrene 4.00 2.58 mg/Kg 64 40 -140 16 25
Benzo[a]anthracene 4.02 2.65 mg/Kg 66 40 -140 17 25
Acenaphthene 4.00 2.59 mg/Kg 65 40 -140 13 25
Chrysene 4.00 2.60 mg/Kg 65 40 -140 15 25
Dibenz(a,h)anthracene 4.00 2.58 mg/Kg 64 40 -140 14 25
Fluoranthene 4.00 2.58 mg/Kg 64 40 -140 14 25
Fluorene 4.01 2.53 mg/Kg 63 40 -140 12 25
C11-C22 Aromatics 68.1 44.6 M mg/Kg 65 40 -140 14 25
Indeno[1,2,3-cd]pyrene 4.00 2.55 mg/Kg 64 40 -140 17 25
2-Methylnaphthalene 4.01 2.60 M mg/Kg 65 40 -140 13 25
Naphthalene 4.00 2.59 M mg/Kg 65 40 -140 14 25
Phenanthrene 4.01 2.61 mg/Kg 65 40 -140 13 25
Pyrene 4.01 2.57 mg/Kg 64 40 -140 14 25
2-Fluorobiphenyl (Surr)40 -140
Surrogate
83
LCSD LCSD
Qualifier Limits%Recovery
64o- terphenyl (Surr)40 -140
Eurofins Savannah
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 410-330594/1-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 331708 Prep Batch: 330594
LOQ DL
C19-C36 Aliphatics 20 U 50 10 ug/L 12/27/22 21:11 12/30/22 17:49 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
12.2 J M 1030 ug/L 12/27/22 21:11 12/30/22 17:49 1C9-C18 Aliphatics
1-Chlorooctadecane (Surr)63 40-140 12/30/22 17:49 1
MB MB
Surrogate
12/27/22 21:11
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 410-330594/1-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 331706 Prep Batch: 330594
LOQ DL
Anthracene 1.2 U 2.0 0.60 ug/L 12/27/22 21:11 12/30/22 17:49 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
1.2 U 0.602.0 ug/L 12/27/22 21:11 12/30/22 17:49 1Benzo[b]fluoranthene
1.2 U 0.602.0 ug/L 12/27/22 21:11 12/30/22 17:49 1Benzo[g,h,i]perylene
1.4 U 0.702.0 ug/L 12/27/22 21:11 12/30/22 17:49 1Acenaphthylene
3.0 U 1.54.0 ug/L 12/27/22 21:11 12/30/22 17:49 1Benzo[k]fluoranthene
1.2 U 0.602.0 ug/L 12/27/22 21:11 12/30/22 17:49 1Benzo[a]pyrene
1.4 U 0.702.0 ug/L 12/27/22 21:11 12/30/22 17:49 1Benzo[a]anthracene
1.2 U 0.602.0 ug/L 12/27/22 21:11 12/30/22 17:49 1Acenaphthene
1.0 U 0.502.0 ug/L 12/27/22 21:11 12/30/22 17:49 1Chrysene
1.0 U 0.502.0 ug/L 12/27/22 21:11 12/30/22 17:49 1Dibenz(a,h)anthracene
1.0 U 0.502.0 ug/L 12/27/22 21:11 12/30/22 17:49 1Fluoranthene
1.2 U 0.602.0 ug/L 12/27/22 21:11 12/30/22 17:49 1Fluorene
30 U 1040 ug/L 12/27/22 21:11 12/30/22 17:49 1C11-C22 Aromatics (unadjusted)
1.2 U 0.602.0 ug/L 12/27/22 21:11 12/30/22 17:49 1Indeno[1,2,3-cd]pyrene
1.2 U 0.602.0 ug/L 12/27/22 21:11 12/30/22 17:49 12-Methylnaphthalene
30 U 1040 ug/L 12/27/22 21:11 12/30/22 17:49 1C11-C22 Aromatics (Adjusted)
1.2 U 0.602.0 ug/L 12/27/22 21:11 12/30/22 17:49 1Naphthalene
1.2 U 0.602.0 ug/L 12/27/22 21:11 12/30/22 17:49 1Phenanthrene
10 U 5.012 ug/L 12/27/22 21:11 12/30/22 17:49 1Pyrene
2-Fluorobiphenyl (Surr)81 40-140 12/30/22 17:49 1
MB MB
Surrogate
12/27/22 21:11
Dil FacPreparedAnalyzedQualifierLimits%Recovery
65 12/27/22 21:11 12/30/22 17:49 1o- terphenyl (Surr)40-140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-330594/2-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 331708 Prep Batch: 330594
C19-C36 Aliphatics 321 224 ug/L 70 40 -140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C18 Aliphatics 241 145 ug/L 60 40 -140
1-Chlorooctadecane (Surr)40 -140
Surrogate
59
LCS LCS
Qualifier Limits%Recovery
Eurofins Savannah
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-330594/2-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 331706 Prep Batch: 330594
Anthracene 40.0 30.8 ug/L 77 40 -140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Benzo[b]fluoranthene 40.2 31.4 M ug/L 78 40 -140
Benzo[g,h,i]perylene 40.1 29.7 ug/L 74 40 -140
Acenaphthylene 40.0 30.1 ug/L 75 40 -140
Benzo[k]fluoranthene 40.1 28.6 M ug/L 71 40 -140
Benzo[a]pyrene 40.0 29.5 ug/L 74 40 -140
Benzo[a]anthracene 40.2 31.0 M ug/L 77 40 -140
Acenaphthene 40.0 28.3 ug/L 71 40 -140
Chrysene 40.0 29.6 M ug/L 74 40 -140
Dibenz(a,h)anthracene 40.0 29.4 M ug/L 73 40 -140
Fluoranthene 40.0 29.9 ug/L 75 40 -140
Fluorene 40.1 28.9 ug/L 72 40 -140
C11-C22 Aromatics (unadjusted)681 506 M ug/L 74 40 -140
Indeno[1,2,3-cd]pyrene 40.0 29.5 M ug/L 74 40 -140
2-Methylnaphthalene 40.1 26.2 M ug/L 65 40 -140
Naphthalene 40.0 25.6 M ug/L 64 40 -140
Phenanthrene 40.1 30.0 ug/L 75 40 -140
Pyrene 40.1 29.8 ug/L 74 40 -140
2-Fluorobiphenyl (Surr)40 -140
Surrogate
84
LCS LCS
Qualifier Limits%Recovery
75o- terphenyl (Surr)40 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-330594/3-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 331708 Prep Batch: 330594
C19-C36 Aliphatics 321 235 ug/L 73 40 -140 5 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C18 Aliphatics 241 149 M ug/L 62 40 -140 2 25
1-Chlorooctadecane (Surr)40 -140
Surrogate
57
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-330594/3-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 331706 Prep Batch: 330594
Anthracene 40.0 28.3 ug/L 71 40 -140 9 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Benzo[b]fluoranthene 40.2 28.7 M ug/L 71 40 -140 9 25
Benzo[g,h,i]perylene 40.1 27.0 ug/L 67 40 -140 10 25
Acenaphthylene 40.0 27.8 ug/L 69 40 -140 8 25
Benzo[k]fluoranthene 40.1 25.6 M ug/L 64 40 -140 11 25
Benzo[a]pyrene 40.0 26.7 ug/L 67 40 -140 10 25
Benzo[a]anthracene 40.2 27.9 ug/L 70 40 -140 10 25
Acenaphthene 40.0 26.6 ug/L 66 40 -140 6 25
Chrysene 40.0 25.9 ug/L 65 40 -140 13 25
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-330594/3-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 331706 Prep Batch: 330594
Dibenz(a,h)anthracene 40.0 25.9 M ug/L 65 40 -140 13 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Fluoranthene 40.0 27.4 ug/L 68 40 -140 9 25
Fluorene 40.1 26.4 ug/L 66 40 -140 9 25
C11-C22 Aromatics (unadjusted)681 465 M ug/L 68 40 -140 8 25
Indeno[1,2,3-cd]pyrene 40.0 26.9 M ug/L 67 40 -140 9 25
2-Methylnaphthalene 40.1 24.7 M ug/L 62 40 -140 6 25
Naphthalene 40.0 24.0 M ug/L 60 40 -140 6 25
Phenanthrene 40.1 27.5 ug/L 69 40 -140 9 25
Pyrene 40.1 27.3 ug/L 68 40 -140 9 25
2-Fluorobiphenyl (Surr)40 -140
Surrogate
77
LCSD LCSD
Qualifier Limits%Recovery
69o- terphenyl (Surr)40 -140
Method: 7199 - Chromium, Hexavalent (IC)
Client Sample ID: Method BlankLab Sample ID: MB 410-331059/11
Matrix: Water Prep Type: Total/NA
Analysis Batch: 331059
LOQ DL
Chromium (hexavalent)9.0 U 10 5.0 ug/L 12/28/22 15:20 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Method BlankLab Sample ID: MB 410-331059/12
Matrix: Water Prep Type: Total/NA
Analysis Batch: 331059
LOQ DL
Chromium (hexavalent)9.0 U 10 5.0 ug/L 12/28/22 15:27 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-331059/10
Matrix: Water Prep Type: Total/NA
Analysis Batch: 331059
Chromium (hexavalent)100 103 ug/L 103 90 -110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-331059/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 331059
Chromium (hexavalent)100 105 ug/L 105 90 -110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: Method BlankLab Sample ID: MB 410-334897/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 335167 Prep Batch: 334897
LOQ DL
Chromium (hexavalent)300 U 400 140 ug/Kg 01/12/23 10:42 01/12/23 17:48 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 7199 - Chromium, Hexavalent (IC)
Client Sample ID: Method BlankLab Sample ID: MB 410-334897/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 335167 Prep Batch: 334897
LOQ DL
Chromium (hexavalent)300 U 400 140 ug/Kg 01/12/23 10:42 01/12/23 17:54 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-334897/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 335167 Prep Batch: 334897
Chromium (hexavalent)5000 4100 M ug/Kg 82 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-334897/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 335167 Prep Batch: 334897
Chromium (hexavalent)5000 4130 ug/Kg 83 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: Lab Control SampleLab Sample ID: LCSI 410-334897/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 335167 Prep Batch: 334897
Chromium (hexavalent)778000 658000 D ug/Kg 85 80 -120
Analyte
LCSI LCSI
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: Lab Control SampleLab Sample ID: LCSI 410-334897/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 335167 Prep Batch: 334897
Chromium (hexavalent)778000 640000 D ug/Kg 82 80 -120
Analyte
LCSI LCSI
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: 149-DUP-1-12-22Lab Sample ID: 680-227663-2 MSI
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 335167 Prep Batch: 334897
Chromium (hexavalent)1100 M 938000 759000 D ug/Kg 81 75 -125☼
Analyte
MSI MSI
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Client Sample ID: 149-DUP-1-12-22Lab Sample ID: 680-227663-2 MSI
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 335167 Prep Batch: 334897
Chromium (hexavalent)1100 M 938000 780000 D ug/Kg 83 75 -125☼
Analyte
MSI MSI
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Client Sample ID: 149-DUP-1-12-22Lab Sample ID: 680-227663-2 MSS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 335167 Prep Batch: 334897
Chromium (hexavalent)1100 M 43800 36900 D ug/Kg 82 75 -125☼
Analyte
MSS MSS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 7199 - Chromium, Hexavalent (IC)
Client Sample ID: 149-DUP-1-12-22Lab Sample ID: 680-227663-2 MSS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 335167 Prep Batch: 334897
Chromium (hexavalent)1100 M 43800 36300 D ug/Kg 81 75 -125☼
Analyte
MSS MSS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Client Sample ID: 149-DUP-1-12-22Lab Sample ID: 680-227663-2 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 335167 Prep Batch: 334897
Chromium (hexavalent)1100 M 1200 M ug/Kg 11 20☼
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Client Sample ID: 149-DUP-1-12-22Lab Sample ID: 680-227663-2 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 335167 Prep Batch: 334897
Chromium (hexavalent)1100 M 1050 M ug/Kg 3 20☼
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: 6020B - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-755270/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 755684 Prep Batch: 755270
LOQ DL
Aluminum 4400 U 8800 1800 ug/Kg 12/15/22 09:42 12/16/22 15:20 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
260 U 88440 ug/Kg 12/15/22 09:42 12/16/22 15:20 1Arsenic
130 U 53440 ug/Kg 12/15/22 09:42 12/16/22 15:20 1Barium
35 U 1344 ug/Kg 12/15/22 09:42 12/16/22 15:20 1Beryllium
35 U 1344 ug/Kg 12/15/22 09:42 12/16/22 15:20 1Cadmium
13000 U 550044000 ug/Kg 12/15/22 09:42 12/16/22 15:20 1Calcium
260 U 96880 ug/Kg 12/15/22 09:42 12/16/22 15:20 1Chromium
26 U 8.844 ug/Kg 12/15/22 09:42 12/16/22 15:20 1Cobalt
260 U 110440 ug/Kg 12/15/22 09:42 12/16/22 15:20 1Copper
8800 U 310022000 ug/Kg 12/15/22 09:42 12/16/22 15:20 1Iron
7900 U 290022000 ug/Kg 12/15/22 09:42 12/16/22 15:20 1Magnesium
260 U 110880 ug/Kg 12/15/22 09:42 12/16/22 15:20 1Manganese
130 U 44180 ug/Kg 12/15/22 09:42 12/16/22 15:20 1Lead
22000 U 800022000 ug/Kg 12/15/22 09:42 12/16/22 15:20 1Potassium
260 U 88440 ug/Kg 12/15/22 09:42 12/16/22 15:20 1Selenium
660 U 230880 ug/Kg 12/15/22 09:42 12/16/22 15:20 1Nickel
26 U 8.888 ug/Kg 12/15/22 09:42 12/16/22 15:20 1Silver
94.3 J 88880 ug/Kg 12/15/22 09:42 12/16/22 15:20 1Antimony
22000 U 880035000 ug/Kg 12/15/22 09:42 12/16/22 15:20 1Sodium
88 U 4488 ug/Kg 12/15/22 09:42 12/16/22 15:20 1Thallium
880 U 2401800 ug/Kg 12/15/22 09:42 12/16/22 15:20 1Vanadium
1800 U 8802200 ug/Kg 12/15/22 09:42 12/16/22 15:20 1Zinc
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 6020B - Metals (ICP/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-755270/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 755684 Prep Batch: 755270
Aluminum 417000 397000 ug/Kg 95 78 -124
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Arsenic 8330 7980 ug/Kg 96 82 -118
Barium 8330 8020 ug/Kg 96 86 -116
Beryllium 4170 4050 ug/Kg 97 80 -120
Cadmium 4170 3870 ug/Kg 93 84 -116
Calcium 417000 427000 ug/Kg 103 86 -118
Chromium 8330 8190 ug/Kg 98 83 -119
Cobalt 4160 4130 ug/Kg 99 84 -115
Copper 8330 8480 ug/Kg 102 84 -119
Iron 417000 431000 ug/Kg 104 81 -124
Magnesium 418000 401000 ug/Kg 96 80 -123
Manganese 33300 31800 ug/Kg 96 85 -116
Lead 42000 39700 ug/Kg 95 84 -118
Potassium 581000 582000 ug/Kg 100 85 -119
Selenium 12500 12700 ug/Kg 101 80 -119
Nickel 8250 8260 ug/Kg 100 84 -119
Silver 4170 3890 ug/Kg 93 83 -118
Antimony 4160 3940 ug/Kg 95 72 -124
Sodium 420000 420000 ug/Kg 100 79 -125
Thallium 4170 3990 ug/Kg 96 83 -118
Vanadium 8320 7640 ug/Kg 92 82 -116
Zinc 8330 9460 ug/Kg 114 82 -119
Client Sample ID: Method BlankLab Sample ID: MB 680-755393/1-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 755684 Prep Batch: 755393
LOQ DL
Aluminum 100 U 200 35 ug/L 12/16/22 06:22 12/16/22 18:31 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
3.0 U 0.865.0 ug/L 12/16/22 06:22 12/16/22 18:31 1Arsenic
2.0 U 0.895.0 ug/L 12/16/22 06:22 12/16/22 18:31 1Barium
0.40 U 0.200.50 ug/L 12/16/22 06:22 12/16/22 18:31 1Beryllium
0.20 U 0.0780.50 ug/L 12/16/22 06:22 12/16/22 18:31 1Cadmium
300 U 140500 ug/L 12/16/22 06:22 12/16/22 18:31 1Calcium
10 U 2.620 ug/L 12/16/22 06:22 12/16/22 18:31 1Chromium
0.50 U 0.221.0 ug/L 12/16/22 06:22 12/16/22 18:31 1Cobalt
2.0 U 0.905.0 ug/L 12/16/22 06:22 12/16/22 18:31 1Copper
75 U 26100 ug/L 12/16/22 06:22 12/16/22 18:31 1Iron
60 U 23250 ug/L 12/16/22 06:22 12/16/22 18:31 1Magnesium
5.0 U 2.210 ug/L 12/16/22 06:22 12/16/22 18:31 1Manganese
1.0 U 0.342.5 ug/L 12/16/22 06:22 12/16/22 18:31 1Lead
500 U 1601000 ug/L 12/16/22 06:22 12/16/22 18:31 1Potassium
2.5 U 1.25.0 ug/L 12/16/22 06:22 12/16/22 18:31 1Selenium
5.0 U 1.810 ug/L 12/16/22 06:22 12/16/22 18:31 1Nickel
1.0 U 0.392.0 ug/L 12/16/22 06:22 12/16/22 18:31 1Silver
1.5 U 0.525.0 ug/L 12/16/22 06:22 12/16/22 18:31 1Antimony
500 U 2001000 ug/L 12/16/22 06:22 12/16/22 18:31 1Sodium
1.0 U 0.262.0 ug/L 12/16/22 06:22 12/16/22 18:31 1Thallium
5.0 U 1.810 ug/L 12/16/22 06:22 12/16/22 18:31 1Vanadium
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 6020B - Metals (ICP/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-755393/1-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 755684 Prep Batch: 755393
LOQ DL
Zinc 20 U 25 10 ug/L 12/16/22 06:22 12/16/22 18:31 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-755393/2-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 755684 Prep Batch: 755393
Aluminum 5000 4980 ug/L 100 84 -117
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Arsenic 100 102 ug/L 102 84 -116
Barium 100 99.2 ug/L 99 86 -114
Beryllium 50.0 47.5 ug/L 95 83 -121
Cadmium 50.0 48.4 ug/L 97 87 -115
Calcium 5000 5300 ug/L 106 87 -118
Chromium 100 103 ug/L 103 85 -116
Cobalt 50.0 51.1 ug/L 102 86 -115
Copper 100 105 ug/L 105 85 -118
Iron 5000 5320 ug/L 106 87 -118
Magnesium 5010 5010 ug/L 100 83 -118
Manganese 400 393 ug/L 98 87 -115
Lead 505 503 ug/L 100 88 -115
Potassium 6970 7010 ug/L 101 87 -115
Selenium 100 105 ug/L 105 80 -120
Nickel 99.0 100 ug/L 101 85 -117
Silver 50.0 47.3 ug/L 95 85 -116
Antimony 50.0 48.7 ug/L 98 85 -117
Sodium 5050 5130 ug/L 102 85 -117
Thallium 50.0 49.9 ug/L 100 82 -116
Vanadium 100 101 ug/L 101 86 -115
Zinc 100 104 ug/L 104 83 -119
Client Sample ID: Method BlankLab Sample ID: MB 680-756223/1-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 756842 Prep Batch: 756223
LOQ DL
Aluminum 100 U 200 35 ug/L 12/21/22 07:02 12/22/22 17:48 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
3.0 U 0.865.0 ug/L 12/21/22 07:02 12/22/22 17:48 1Arsenic
2.0 U 0.895.0 ug/L 12/21/22 07:02 12/22/22 17:48 1Barium
0.40 U 0.200.50 ug/L 12/21/22 07:02 12/22/22 17:48 1Beryllium
0.20 U 0.0780.50 ug/L 12/21/22 07:02 12/22/22 17:48 1Cadmium
300 U 140500 ug/L 12/21/22 07:02 12/22/22 17:48 1Calcium
10 U 2.620 ug/L 12/21/22 07:02 12/22/22 17:48 1Chromium
0.50 U 0.221.0 ug/L 12/21/22 07:02 12/22/22 17:48 1Cobalt
2.0 U 0.905.0 ug/L 12/21/22 07:02 12/22/22 17:48 1Copper
75 U 26100 ug/L 12/21/22 07:02 12/22/22 17:48 1Iron
60 U 23250 ug/L 12/21/22 07:02 12/22/22 17:48 1Magnesium
5.0 U 2.210 ug/L 12/21/22 07:02 12/22/22 17:48 1Manganese
1.0 U 0.342.5 ug/L 12/21/22 07:02 12/22/22 17:48 1Lead
500 U 1601000 ug/L 12/21/22 07:02 12/22/22 17:48 1Potassium
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 6020B - Metals (ICP/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-756223/1-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 756842 Prep Batch: 756223
LOQ DL
Selenium 2.5 U 5.0 1.2 ug/L 12/21/22 07:02 12/22/22 17:48 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
5.0 U 1.810 ug/L 12/21/22 07:02 12/22/22 17:48 1Nickel
1.0 U 0.392.0 ug/L 12/21/22 07:02 12/22/22 17:48 1Silver
1.5 U 0.525.0 ug/L 12/21/22 07:02 12/22/22 17:48 1Antimony
500 U 2001000 ug/L 12/21/22 07:02 12/22/22 17:48 1Sodium
1.0 U 0.262.0 ug/L 12/21/22 07:02 12/22/22 17:48 1Thallium
5.0 U 1.810 ug/L 12/21/22 07:02 12/22/22 17:48 1Vanadium
20 U 1025 ug/L 12/21/22 07:02 12/22/22 17:48 1Zinc
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-756223/2-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 756842 Prep Batch: 756223
Aluminum 5000 5000 ug/L 100 84 -117
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Arsenic 100 96.8 ug/L 97 84 -116
Barium 100 98.2 ug/L 98 86 -114
Beryllium 50.0 48.9 ug/L 98 83 -121
Cadmium 50.0 49.0 ug/L 98 87 -115
Calcium 5000 5080 ug/L 102 87 -118
Chromium 100 92.0 ug/L 92 85 -116
Cobalt 50.0 51.3 ug/L 103 86 -115
Copper 100 104 ug/L 104 85 -118
Iron 5000 5190 ug/L 104 87 -118
Magnesium 5010 4990 ug/L 100 83 -118
Manganese 400 410 ug/L 103 87 -115
Lead 505 487 ug/L 96 88 -115
Potassium 6970 6820 ug/L 98 87 -115
Selenium 100 106 ug/L 105 80 -120
Nickel 99.0 100 ug/L 101 85 -117
Silver 50.0 47.6 ug/L 95 85 -116
Antimony 50.0 49.4 ug/L 99 85 -117
Sodium 5050 5170 ug/L 103 85 -117
Thallium 50.0 47.2 ug/L 94 82 -116
Vanadium 100 99.2 ug/L 99 86 -115
Zinc 100 105 ug/L 105 83 -119
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 680-755404/1-B
Matrix: Water Prep Type: Dissolved
Analysis Batch: 755947 Prep Batch: 755407
LOQ DL
Hg 0.20 U 0.25 0.080 ug/L 12/16/22 08:53 12/19/22 09:15 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
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QC Sample Results
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method: 7470A - Mercury (CVAA) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-755404/2-B
Matrix: Water Prep Type: Dissolved
Analysis Batch: 755947 Prep Batch: 755407
Hg 2.50 2.56 ug/L 102 80 -124
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
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QC Association Summary
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
GC/MS VOA
Prep Batch: 755487
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035A680-227663-1 149-SB-1-6-12-22 Total/NA
Solid 5035A680-227663-2 149-DUP-1-12-22 Total/NA
Solid 5035A680-227663-3 149-SB-1-20-12-22 Total/NA
Solid 5035A680-227663-4 149-SB-1-30-12-22 Total/NA
Solid 5035A680-227663-5 149-SB-1-40-12-22 Total/NA
Solid 5035A680-227663-6 149-SB-1-46-12-22 Total/NA
Analysis Batch: 756853
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260D 755487680-227663-1 149-SB-1-6-12-22 Total/NA
Solid 8260D 755487680-227663-2 149-DUP-1-12-22 Total/NA
Solid 8260D 755487680-227663-3 149-SB-1-20-12-22 Total/NA
Solid 8260D 755487680-227663-4 149-SB-1-30-12-22 Total/NA
Solid 8260D 755487680-227663-5 149-SB-1-40-12-22 Total/NA
Solid 8260D 755487680-227663-6 149-SB-1-46-12-22 Total/NA
Solid 8260DMB 680-756853/8 Method Blank Total/NA
Solid 8260DLCS 680-756853/5 Lab Control Sample Total/NA
Solid 8260DLCSD 680-756853/6 Lab Control Sample Dup Total/NA
Analysis Batch: 757008
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260D680-227663-7 FB-12-22 Total/NA
Water 8260D680-227663-8 EQB-12-22 Total/NA
Water 8260D680-227663-9 149-TW-01 Total/NA
Water 8260D680-227663-10 DUP-TW-01 Total/NA
Water 8260DMB 680-757008/9 Method Blank Total/NA
Water 8260DLCS 680-757008/5 Lab Control Sample Total/NA
Water 8260DLCSD 680-757008/6 Lab Control Sample Dup Total/NA
GC/MS Semi VOA
Prep Batch: 755512
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3546680-227663-2 149-DUP-1-12-22 Total/NA
Solid 3546680-227663-3 149-SB-1-20-12-22 Total/NA
Solid 3546680-227663-4 149-SB-1-30-12-22 Total/NA
Solid 3546680-227663-5 149-SB-1-40-12-22 Total/NA
Solid 3546680-227663-6 149-SB-1-46-12-22 Total/NA
Solid 3546MB 680-755512/8-A Method Blank Total/NA
Solid 3546LCS 680-755512/9-A Lab Control Sample Total/NA
Solid 3546680-227663-A-1-E MS 680-227663-A-1-E MS Total/NA
Solid 3546680-227663-A-1-F MSD 680-227663-A-1-F MSD Total/NA
Analysis Batch: 756054
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270E 755512680-227663-2 149-DUP-1-12-22 Total/NA
Solid 8270E 755512680-227663-3 149-SB-1-20-12-22 Total/NA
Solid 8270E 755512680-227663-4 149-SB-1-30-12-22 Total/NA
Solid 8270E 755512680-227663-5 149-SB-1-40-12-22 Total/NA
Solid 8270E 755512680-227663-6 149-SB-1-46-12-22 Total/NA
Solid 8270E 755512MB 680-755512/8-A Method Blank Total/NA
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QC Association Summary
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
GC/MS Semi VOA (Continued)
Analysis Batch: 756054 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270E 755512LCS 680-755512/9-A Lab Control Sample Total/NA
Solid 8270E 755512680-227663-A-1-E MS 680-227663-A-1-E MS Total/NA
Solid 8270E 755512680-227663-A-1-F MSD 680-227663-A-1-F MSD Total/NA
Prep Batch: 756109
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C680-227663-7 FB-12-22 Total/NA
Water 3510C680-227663-8 EQB-12-22 Total/NA
Water 3510C680-227663-9 149-TW-01 Total/NA
Water 3510C680-227663-10 DUP-TW-01 Total/NA
Water 3510CMB 680-756109/1-A Method Blank Total/NA
Water 3510CLCS 680-756109/2-A Lab Control Sample Total/NA
Water 3510CLCSD 680-756109/3-A Lab Control Sample Dup Total/NA
Prep Batch: 756630
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3546680-227663-1 149-SB-1-6-12-22 Total/NA
Solid 3546MB 680-756630/5-A Method Blank Total/NA
Solid 3546LCS 680-756630/6-A Lab Control Sample Total/NA
Analysis Batch: 756690
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270E 756630680-227663-1 149-SB-1-6-12-22 Total/NA
Water 8270E 756109680-227663-7 FB-12-22 Total/NA
Water 8270E 756109680-227663-8 EQB-12-22 Total/NA
Water 8270E 756109680-227663-9 149-TW-01 Total/NA
Water 8270E 756109680-227663-10 DUP-TW-01 Total/NA
Water 8270E 756109MB 680-756109/1-A Method Blank Total/NA
Solid 8270E 756630MB 680-756630/5-A Method Blank Total/NA
Water 8270E 756109LCS 680-756109/2-A Lab Control Sample Total/NA
Solid 8270E 756630LCS 680-756630/6-A Lab Control Sample Total/NA
Water 8270E 756109LCSD 680-756109/3-A Lab Control Sample Dup Total/NA
GC VOA
Prep Batch: 328291
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5030C680-227663-1 149-SB-1-6-12-22 Total/NA
Solid 5030C680-227663-2 149-DUP-1-12-22 Total/NA
Solid 5030C680-227663-3 149-SB-1-20-12-22 Total/NA
Solid 5030C680-227663-4 149-SB-1-30-12-22 Total/NA
Solid 5030C680-227663-5 149-SB-1-40-12-22 Total/NA
Solid 5030C680-227663-6 149-SB-1-46-12-22 Total/NA
Solid 5030CMB 410-328291/21-A Method Blank Total/NA
Solid 5030CLCS 410-328291/22-A Lab Control Sample Total/NA
Solid 5030CLCSD 410-328291/23-A Lab Control Sample Dup Total/NA
Analysis Batch: 330695
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MAVPH680-227663-7 FB-12-22 Total/NA
Water MAVPH680-227663-8 EQB-12-22 Total/NA
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QC Association Summary
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
GC VOA (Continued)
Analysis Batch: 330695 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MAVPH680-227663-9 149-TW-01 Total/NA
Water MAVPH680-227663-10 DUP-TW-01 Total/NA
Water MAVPHMB 410-330695/4 Method Blank Total/NA
Water MAVPHLCS 410-330695/5 Lab Control Sample Total/NA
Water MAVPHLCSD 410-330695/6 Lab Control Sample Dup Total/NA
Analysis Batch: 333572
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MAVPH 328291680-227663-1 149-SB-1-6-12-22 Total/NA
Solid MAVPH 328291680-227663-2 149-DUP-1-12-22 Total/NA
Solid MAVPH 328291680-227663-3 149-SB-1-20-12-22 Total/NA
Solid MAVPH 328291680-227663-4 149-SB-1-30-12-22 Total/NA
Solid MAVPH 328291680-227663-5 149-SB-1-40-12-22 Total/NA
Solid MAVPH 328291680-227663-6 149-SB-1-46-12-22 Total/NA
Solid MAVPH 328291MB 410-328291/21-A Method Blank Total/NA
Solid MAVPH 328291LCS 410-328291/22-A Lab Control Sample Total/NA
Solid MAVPH 328291LCSD 410-328291/23-A Lab Control Sample Dup Total/NA
Analysis Batch: 336389
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MA VPH680-227663-1 149-SB-1-6-12-22 Total/NA
Solid MA VPH680-227663-2 149-DUP-1-12-22 Total/NA
Solid MA VPH680-227663-3 149-SB-1-20-12-22 Total/NA
Solid MA VPH680-227663-4 149-SB-1-30-12-22 Total/NA
Solid MA VPH680-227663-5 149-SB-1-40-12-22 Total/NA
Solid MA VPH680-227663-6 149-SB-1-46-12-22 Total/NA
Water MA VPH680-227663-7 FB-12-22 Total/NA
Water MA VPH680-227663-8 EQB-12-22 Total/NA
Water MA VPH680-227663-9 149-TW-01 Total/NA
Water MA VPH680-227663-10 DUP-TW-01 Total/NA
GC Semi VOA
Prep Batch: 328608
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C680-227663-7 FB-12-22 Total/NA
Water 3510C680-227663-8 EQB-12-22 Total/NA
Water 3510C680-227663-9 149-TW-01 Total/NA
Water 3510C680-227663-10 DUP-TW-01 Total/NA
Water 3510CMB 410-328608/1-B Method Blank Total/NA
Water 3510CMB 410-328608/1-C Method Blank Total/NA
Water 3510CLCS 410-328608/2-B Lab Control Sample Total/NA
Water 3510CLCS 410-328608/2-C Lab Control Sample Total/NA
Water 3510CLCSD 410-328608/3-B Lab Control Sample Dup Total/NA
Water 3510CLCSD 410-328608/3-C Lab Control Sample Dup Total/NA
Cleanup Batch: 329620
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3630C 328608680-227663-7 FB-12-22 Total/NA
Water 3630C 328608680-227663-7 FB-12-22 Total/NA
Water 3630C 328608680-227663-8 EQB-12-22 Total/NA
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QC Association Summary
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
GC Semi VOA (Continued)
Cleanup Batch: 329620 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3630C 328608680-227663-8 EQB-12-22 Total/NA
Water 3630C 328608680-227663-9 149-TW-01 Total/NA
Water 3630C 328608680-227663-9 149-TW-01 Total/NA
Water 3630C 328608680-227663-10 DUP-TW-01 Total/NA
Water 3630C 328608680-227663-10 DUP-TW-01 Total/NA
Water 3630C 328608MB 410-328608/1-B Method Blank Total/NA
Water 3630C 328608MB 410-328608/1-C Method Blank Total/NA
Water 3630C 328608LCS 410-328608/2-B Lab Control Sample Total/NA
Water 3630C 328608LCS 410-328608/2-C Lab Control Sample Total/NA
Water 3630C 328608LCSD 410-328608/3-B Lab Control Sample Dup Total/NA
Water 3630C 328608LCSD 410-328608/3-C Lab Control Sample Dup Total/NA
Analysis Batch: 329935
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA-EPH 329620680-227663-7 FB-12-22 Total/NA
Water MA-EPH 329620680-227663-8 EQB-12-22 Total/NA
Water MA-EPH 329620680-227663-9 149-TW-01 Total/NA
Water MA-EPH 329620680-227663-10 DUP-TW-01 Total/NA
Water MA-EPH 329620MB 410-328608/1-C Method Blank Total/NA
Water MA-EPH 329620LCS 410-328608/2-C Lab Control Sample Total/NA
Water MA-EPH 329620LCSD 410-328608/3-C Lab Control Sample Dup Total/NA
Analysis Batch: 329942
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA-EPH 329620680-227663-7 FB-12-22 Total/NA
Water MA-EPH 329620680-227663-8 EQB-12-22 Total/NA
Water MA-EPH 329620680-227663-9 149-TW-01 Total/NA
Water MA-EPH 329620680-227663-10 DUP-TW-01 Total/NA
Water MA-EPH 329620MB 410-328608/1-B Method Blank Total/NA
Water MA-EPH 329620LCS 410-328608/2-B Lab Control Sample Total/NA
Water MA-EPH 329620LCSD 410-328608/3-B Lab Control Sample Dup Total/NA
Prep Batch: 329945
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3546680-227663-1 149-SB-1-6-12-22 Total/NA
Solid 3546680-227663-2 149-DUP-1-12-22 Total/NA
Solid 3546680-227663-3 149-SB-1-20-12-22 Total/NA
Solid 3546680-227663-4 149-SB-1-30-12-22 Total/NA
Solid 3546680-227663-5 149-SB-1-40-12-22 Total/NA
Solid 3546680-227663-6 149-SB-1-46-12-22 Total/NA
Solid 3546MB 410-329945/1-B Method Blank Total/NA
Solid 3546MB 410-329945/1-C Method Blank Total/NA
Solid 3546LCS 410-329945/2-B Lab Control Sample Total/NA
Solid 3546LCS 410-329945/2-C Lab Control Sample Total/NA
Solid 3546LCSD 410-329945/3-B Lab Control Sample Dup Total/NA
Solid 3546LCSD 410-329945/3-C Lab Control Sample Dup Total/NA
Prep Batch: 330594
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C680-227663-9 - REDL 149-TW-01 Total/NA
Water 3510C680-227663-9 - RE 149-TW-01 Total/NA
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QC Association Summary
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
GC Semi VOA (Continued)
Prep Batch: 330594 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510CMB 410-330594/1-B Method Blank Total/NA
Water 3510CMB 410-330594/1-C Method Blank Total/NA
Water 3510CLCS 410-330594/2-B Lab Control Sample Total/NA
Water 3510CLCS 410-330594/2-C Lab Control Sample Total/NA
Water 3510CLCSD 410-330594/3-B Lab Control Sample Dup Total/NA
Water 3510CLCSD 410-330594/3-C Lab Control Sample Dup Total/NA
Cleanup Batch: 331481
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3630C 330594680-227663-9 - REDL 149-TW-01 Total/NA
Water 3630C 330594680-227663-9 - RE 149-TW-01 Total/NA
Water 3630C 330594680-227663-9 - RE 149-TW-01 Total/NA
Water 3630C 330594MB 410-330594/1-B Method Blank Total/NA
Water 3630C 330594MB 410-330594/1-C Method Blank Total/NA
Water 3630C 330594LCS 410-330594/2-B Lab Control Sample Total/NA
Water 3630C 330594LCS 410-330594/2-C Lab Control Sample Total/NA
Water 3630C 330594LCSD 410-330594/3-B Lab Control Sample Dup Total/NA
Water 3630C 330594LCSD 410-330594/3-C Lab Control Sample Dup Total/NA
Cleanup Batch: 331482
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3630C 329945680-227663-1 149-SB-1-6-12-22 Total/NA
Solid 3630C 329945680-227663-1 149-SB-1-6-12-22 Total/NA
Solid 3630C 329945680-227663-2 149-DUP-1-12-22 Total/NA
Solid 3630C 329945680-227663-2 149-DUP-1-12-22 Total/NA
Solid 3630C 329945680-227663-3 149-SB-1-20-12-22 Total/NA
Solid 3630C 329945680-227663-3 149-SB-1-20-12-22 Total/NA
Solid 3630C 329945680-227663-4 149-SB-1-30-12-22 Total/NA
Solid 3630C 329945680-227663-4 149-SB-1-30-12-22 Total/NA
Solid 3630C 329945680-227663-5 149-SB-1-40-12-22 Total/NA
Solid 3630C 329945680-227663-5 149-SB-1-40-12-22 Total/NA
Solid 3630C 329945680-227663-6 149-SB-1-46-12-22 Total/NA
Solid 3630C 329945680-227663-6 149-SB-1-46-12-22 Total/NA
Solid 3630C 329945MB 410-329945/1-B Method Blank Total/NA
Solid 3630C 329945MB 410-329945/1-C Method Blank Total/NA
Solid 3630C 329945LCS 410-329945/2-B Lab Control Sample Total/NA
Solid 3630C 329945LCS 410-329945/2-C Lab Control Sample Total/NA
Solid 3630C 329945LCSD 410-329945/3-B Lab Control Sample Dup Total/NA
Solid 3630C 329945LCSD 410-329945/3-C Lab Control Sample Dup Total/NA
Analysis Batch: 331706
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MA-EPH 331482680-227663-1 149-SB-1-6-12-22 Total/NA
Solid MA-EPH 331482680-227663-2 149-DUP-1-12-22 Total/NA
Solid MA-EPH 331482680-227663-3 149-SB-1-20-12-22 Total/NA
Solid MA-EPH 331482680-227663-4 149-SB-1-30-12-22 Total/NA
Solid MA-EPH 331482680-227663-5 149-SB-1-40-12-22 Total/NA
Solid MA-EPH 331482680-227663-6 149-SB-1-46-12-22 Total/NA
Water MA-EPH 331481680-227663-9 - RE 149-TW-01 Total/NA
Solid MA-EPH 331482MB 410-329945/1-C Method Blank Total/NA
Water MA-EPH 331481MB 410-330594/1-C Method Blank Total/NA
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QC Association Summary
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
GC Semi VOA (Continued)
Analysis Batch: 331706 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MA-EPH 331482LCS 410-329945/2-C Lab Control Sample Total/NA
Water MA-EPH 331481LCS 410-330594/2-C Lab Control Sample Total/NA
Solid MA-EPH 331482LCSD 410-329945/3-C Lab Control Sample Dup Total/NA
Water MA-EPH 331481LCSD 410-330594/3-C Lab Control Sample Dup Total/NA
Analysis Batch: 331708
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MA-EPH 331482680-227663-1 149-SB-1-6-12-22 Total/NA
Solid MA-EPH 331482680-227663-2 149-DUP-1-12-22 Total/NA
Solid MA-EPH 331482680-227663-3 149-SB-1-20-12-22 Total/NA
Solid MA-EPH 331482680-227663-4 149-SB-1-30-12-22 Total/NA
Solid MA-EPH 331482680-227663-5 149-SB-1-40-12-22 Total/NA
Solid MA-EPH 331482680-227663-6 149-SB-1-46-12-22 Total/NA
Water MA-EPH 331481680-227663-9 - RE 149-TW-01 Total/NA
Solid MA-EPH 331482MB 410-329945/1-B Method Blank Total/NA
Water MA-EPH 331481MB 410-330594/1-B Method Blank Total/NA
Solid MA-EPH 331482LCS 410-329945/2-B Lab Control Sample Total/NA
Water MA-EPH 331481LCS 410-330594/2-B Lab Control Sample Total/NA
Solid MA-EPH 331482LCSD 410-329945/3-B Lab Control Sample Dup Total/NA
Water MA-EPH 331481LCSD 410-330594/3-B Lab Control Sample Dup Total/NA
Analysis Batch: 332630
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA-EPH 331481680-227663-9 - REDL 149-TW-01 Total/NA
Prep Batch: 755500
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3546680-227663-1 149-SB-1-6-12-22 Total/NA
Solid 3546680-227663-2 149-DUP-1-12-22 Total/NA
Solid 3546MB 680-755500/7-A Method Blank Total/NA
Solid 3546LCS 680-755500/11-A Lab Control Sample Total/NA
Solid 3546LCS 680-755500/8-A Lab Control Sample Total/NA
Solid 3546680-227663-1 MS 149-SB-1-6-12-22 Total/NA
Solid 3546680-227663-1 MSD 149-SB-1-6-12-22 Total/NA
Analysis Batch: 755553
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8081B 8082A 755500680-227663-1 149-SB-1-6-12-22 Total/NA
Solid 8081B 8082A 755500680-227663-2 149-DUP-1-12-22 Total/NA
Solid 8081B 8082A 755500MB 680-755500/7-A Method Blank Total/NA
Solid 8081B 8082A 755500LCS 680-755500/11-A Lab Control Sample Total/NA
Solid 8081B 8082A 755500LCS 680-755500/8-A Lab Control Sample Total/NA
Solid 8081B 8082A 755500680-227663-1 MS 149-SB-1-6-12-22 Total/NA
Solid 8081B 8082A 755500680-227663-1 MSD 149-SB-1-6-12-22 Total/NA
Prep Batch: 756376
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C680-227663-7 FB-12-22 Total/NA
Water 3510C680-227663-8 EQB-12-22 Total/NA
Water 3510C680-227663-9 149-TW-01 Total/NA
Water 3510C680-227663-10 DUP-TW-01 Total/NA
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QC Association Summary
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
GC Semi VOA (Continued)
Prep Batch: 756376 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510CMB 680-756376/1-A Method Blank Total/NA
Water 3510CLCS 680-756376/2-A Lab Control Sample Total/NA
Water 3510CLCS 680-756376/5-A Lab Control Sample Total/NA
Water 3510CLCSD 680-756376/6-A Lab Control Sample Dup Total/NA
Analysis Batch: 756577
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8081B 8082A 756376680-227663-7 FB-12-22 Total/NA
Water 8081B 8082A 756376680-227663-8 EQB-12-22 Total/NA
Water 8081B 8082A 756376680-227663-9 149-TW-01 Total/NA
Water 8081B 8082A 756376680-227663-10 DUP-TW-01 Total/NA
Water 8081B 8082A 756376MB 680-756376/1-A Method Blank Total/NA
Water 8081B 8082A 756376LCS 680-756376/2-A Lab Control Sample Total/NA
Water 8081B 8082A 756376LCS 680-756376/5-A Lab Control Sample Total/NA
Water 8081B 8082A 756376LCSD 680-756376/6-A Lab Control Sample Dup Total/NA
HPLC/IC
Analysis Batch: 331059
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7199680-227663-7 FB-12-22 Dissolved
Water 7199680-227663-7 FB-12-22 Dissolved
Water 7199680-227663-8 EQB-12-22 Dissolved
Water 7199680-227663-8 EQB-12-22 Dissolved
Water 7199680-227663-9 149-TW-01 Dissolved
Water 7199680-227663-9 149-TW-01 Dissolved
Water 7199680-227663-10 DUP-TW-01 Dissolved
Water 7199680-227663-10 DUP-TW-01 Dissolved
Water 7199MB 410-331059/11 Method Blank Total/NA
Water 7199MB 410-331059/12 Method Blank Total/NA
Water 7199LCS 410-331059/10 Lab Control Sample Total/NA
Water 7199LCS 410-331059/9 Lab Control Sample Total/NA
Prep Batch: 334897
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3060A680-227663-1 149-SB-1-6-12-22 Total/NA
Solid 3060A680-227663-2 149-DUP-1-12-22 Total/NA
Solid 3060A680-227663-3 149-SB-1-20-12-22 Total/NA
Solid 3060A680-227663-4 149-SB-1-30-12-22 Total/NA
Solid 3060A680-227663-5 149-SB-1-40-12-22 Total/NA
Solid 3060A680-227663-6 149-SB-1-46-12-22 Total/NA
Solid 3060AMB 410-334897/1-A Method Blank Total/NA
Solid 3060ALCS 410-334897/2-A Lab Control Sample Total/NA
Solid 3060ALCSI 410-334897/3-A Lab Control Sample Total/NA
Solid 3060A680-227663-2 MSI 149-DUP-1-12-22 Total/NA
Solid 3060A680-227663-2 MSS 149-DUP-1-12-22 Total/NA
Solid 3060A680-227663-2 DU 149-DUP-1-12-22 Total/NA
Analysis Batch: 335167
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7199 334897680-227663-1 149-SB-1-6-12-22 Total/NA
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QC Association Summary
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
HPLC/IC (Continued)
Analysis Batch: 335167 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7199 334897680-227663-1 149-SB-1-6-12-22 Total/NA
Solid 7199 334897680-227663-2 149-DUP-1-12-22 Total/NA
Solid 7199 334897680-227663-2 149-DUP-1-12-22 Total/NA
Solid 7199 334897680-227663-3 149-SB-1-20-12-22 Total/NA
Solid 7199 334897680-227663-3 149-SB-1-20-12-22 Total/NA
Solid 7199 334897680-227663-4 149-SB-1-30-12-22 Total/NA
Solid 7199 334897680-227663-4 149-SB-1-30-12-22 Total/NA
Solid 7199 334897680-227663-5 149-SB-1-40-12-22 Total/NA
Solid 7199 334897680-227663-5 149-SB-1-40-12-22 Total/NA
Solid 7199 334897680-227663-6 149-SB-1-46-12-22 Total/NA
Solid 7199 334897680-227663-6 149-SB-1-46-12-22 Total/NA
Solid 7199 334897MB 410-334897/1-A Method Blank Total/NA
Solid 7199 334897MB 410-334897/1-A Method Blank Total/NA
Solid 7199 334897LCS 410-334897/2-A Lab Control Sample Total/NA
Solid 7199 334897LCS 410-334897/2-A Lab Control Sample Total/NA
Solid 7199 334897LCSI 410-334897/3-A Lab Control Sample Total/NA
Solid 7199 334897LCSI 410-334897/3-A Lab Control Sample Total/NA
Solid 7199 334897680-227663-2 MSI 149-DUP-1-12-22 Total/NA
Solid 7199 334897680-227663-2 MSI 149-DUP-1-12-22 Total/NA
Solid 7199 334897680-227663-2 MSS 149-DUP-1-12-22 Total/NA
Solid 7199 334897680-227663-2 MSS 149-DUP-1-12-22 Total/NA
Solid 7199 334897680-227663-2 DU 149-DUP-1-12-22 Total/NA
Solid 7199 334897680-227663-2 DU 149-DUP-1-12-22 Total/NA
Metals
Prep Batch: 755270
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3050B680-227663-1 149-SB-1-6-12-22 Total/NA
Solid 3050B680-227663-2 149-DUP-1-12-22 Total/NA
Solid 3050B680-227663-3 149-SB-1-20-12-22 Total/NA
Solid 3050B680-227663-4 149-SB-1-30-12-22 Total/NA
Solid 3050B680-227663-5 149-SB-1-40-12-22 Total/NA
Solid 3050B680-227663-6 149-SB-1-46-12-22 Total/NA
Solid 3050BMB 680-755270/1-A Method Blank Total/NA
Solid 3050BLCS 680-755270/2-A Lab Control Sample Total/NA
Prep Batch: 755393
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3005A680-227663-7 FB-12-22 Total Recoverable
Water 3005A680-227663-8 EQB-12-22 Total Recoverable
Water 3005A680-227663-9 149-TW-01 Total Recoverable
Water 3005A680-227663-10 DUP-TW-01 Total Recoverable
Water 3005AMB 680-755393/1-A Method Blank Total Recoverable
Water 3005ALCS 680-755393/2-A Lab Control Sample Total Recoverable
Filtration Batch: 755404
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water FILTRATION680-227663-9 149-TW-01 Dissolved
Water FILTRATIONMB 680-755404/1-B Method Blank Dissolved
Water FILTRATIONLCS 680-755404/2-B Lab Control Sample Dissolved
Eurofins Savannah
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QC Association Summary
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Metals
Prep Batch: 755407
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 755404680-227663-9 149-TW-01 Dissolved
Water 7470A 755404MB 680-755404/1-B Method Blank Dissolved
Water 7470A 755404LCS 680-755404/2-B Lab Control Sample Dissolved
Analysis Batch: 755684
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6020B 755270680-227663-1 149-SB-1-6-12-22 Total/NA
Solid 6020B 755270680-227663-2 149-DUP-1-12-22 Total/NA
Solid 6020B 755270680-227663-3 149-SB-1-20-12-22 Total/NA
Solid 6020B 755270680-227663-4 149-SB-1-30-12-22 Total/NA
Solid 6020B 755270680-227663-5 149-SB-1-40-12-22 Total/NA
Solid 6020B 755270680-227663-6 149-SB-1-46-12-22 Total/NA
Water 6020B 755393680-227663-7 FB-12-22 Total Recoverable
Water 6020B 755393680-227663-8 EQB-12-22 Total Recoverable
Water 6020B 755393680-227663-9 149-TW-01 Total Recoverable
Water 6020B 755393680-227663-10 DUP-TW-01 Total Recoverable
Solid 6020B 755270MB 680-755270/1-A Method Blank Total/NA
Water 6020B 755393MB 680-755393/1-A Method Blank Total Recoverable
Solid 6020B 755270LCS 680-755270/2-A Lab Control Sample Total/NA
Water 6020B 755393LCS 680-755393/2-A Lab Control Sample Total Recoverable
Analysis Batch: 755947
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 755407680-227663-9 149-TW-01 Dissolved
Water 7470A 755407MB 680-755404/1-B Method Blank Dissolved
Water 7470A 755407LCS 680-755404/2-B Lab Control Sample Dissolved
Filtration Batch: 756221
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water FILTRATION680-227663-9 149-TW-01 Dissolved
Prep Batch: 756223
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3005A 756221680-227663-9 149-TW-01 Dissolved
Water 3005AMB 680-756223/1-A Method Blank Total Recoverable
Water 3005ALCS 680-756223/2-A Lab Control Sample Total Recoverable
Analysis Batch: 756842
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 756223680-227663-9 149-TW-01 Dissolved
Water 6020B 756223MB 680-756223/1-A Method Blank Total Recoverable
Water 6020B 756223LCS 680-756223/2-A Lab Control Sample Total Recoverable
General Chemistry
Analysis Batch: 755523
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture680-227663-1 149-SB-1-6-12-22 Total/NA
Solid Moisture680-227663-2 149-DUP-1-12-22 Total/NA
Solid Moisture680-227663-3 149-SB-1-20-12-22 Total/NA
Solid Moisture680-227663-4 149-SB-1-30-12-22 Total/NA
Eurofins Savannah
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QC Association Summary
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
General Chemistry (Continued)
Analysis Batch: 755523 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture680-227663-5 149-SB-1-40-12-22 Total/NA
Solid Moisture680-227663-6 149-SB-1-46-12-22 Total/NA
Eurofins Savannah
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Lab Chronicle
Client: Sure-BioChem Laboratories LLC Job ID: 680-227663-1
Project/Site: CLFTBR0149 Ft. Bragg
Client Sample ID: 149-SB-1-6-12-22 Lab Sample ID: 680-227663-1
Matrix: SolidDate Collected: 12/13/22 11:40
Date Received: 12/15/22 09:00
Analysis Moisture KF12/16/22 16:021 EET SAV755523
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: 149-SB-1-6-12-22 Lab Sample ID: 680-227663-1
Matrix: SolidDate Collected: 12/13/22 11:40
Percent Solids: 77.3Date Received: 12/15/22 09:00
Prep 5035A FES12/16/22 12:07 EET SAV755487
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.443 g 5 mL
Analysis 8260D 1 756853 12/27/22 18:08 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 756630 12/22/22 19:00 MJ EET SAVTotal/NA 15.58 g 1 mL
Analysis 8270E 1 756690 12/23/22 22:43 T1C EET SAVTotal/NA 1 mL 1 mL
CMSGInstrument ID:
Analysis MA VPH 1 336389 01/18/23 06:31 X875 ELLETotal/NA
10149Instrument ID:
Prep 5030C 328291 12/18/22 16:07 D8NM ELLETotal/NA 15.05 g 15 mL
Analysis MAVPH 50 333572 01/10/23 17:56 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Prep 3546 755500 12/16/22 13:33 MJ EET SAVTotal/NA 15.79 g 5 mL
Analysis 8081B 8082A 1 755553 12/16/22 21:15 JCK EET SAVTotal/NA 1 mL 1 mL
CSGJInstrument ID:
Prep 3546 329945 12/22/22 15:40 MD4W ELLETotal/NA 10.13 g 1 mL
Cleanup 3630C 331482 12/30/22 07:24 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 331706 12/31/22 03:56 UHEW ELLETotal/NA 1 mL 1 mL
18433-WInstrument ID:
Prep 3546 329945 12/22/22 15:40 MD4W ELLETotal/NA 10.13 g 1 mL
Cleanup 3630C 331482 12/30/22 07:24 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 331708 12/31/22 03:33 UHEW ELLETotal/NA 1 mL 1 mL
18433-XInstrument ID:
Prep 3060A 334897 01/12/23 10:42 UJE2 ELLETotal/NA 2.52 g 100 mL
Analysis 7199 1 335167 01/12/23 19:30 UJE2 ELLETotal/NA 1 mL 1 mL
26790Instrument ID:
Prep 3060A 334897 01/12/23 10:42 UJE2 ELLETotal/NA 2.52 g 100 mL
Analysis 7199 1 335167 01/12/23 19:37 UJE2 ELLETotal/NA 1 mL 1 mL
26790Instrument ID:
Prep 3050B 755270 12/15/22 13:26 SY EET SAVTotal/NA 1.14 g 500 mL
Analysis 6020B 1 755684 12/16/22 15:54 BWR EET SAVTotal/NA
ICPMSCInstrument ID:
Eurofins Savannah
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Lab Chronicle
Client: Sure-BioChem Laboratories LLC Job ID: 680-227663-1
Project/Site: CLFTBR0149 Ft. Bragg
Client Sample ID: 149-DUP-1-12-22 Lab Sample ID: 680-227663-2
Matrix: SolidDate Collected: 12/13/22 12:00
Date Received: 12/15/22 09:00
Analysis Moisture KF12/16/22 16:021 EET SAV755523
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: 149-DUP-1-12-22 Lab Sample ID: 680-227663-2
Matrix: SolidDate Collected: 12/13/22 12:00
Percent Solids: 92.5Date Received: 12/15/22 09:00
Prep 5035A FES12/16/22 12:07 EET SAV755487
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.097 g 5 mL
Analysis 8260D 1 756853 12/27/22 18:31 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 755512 12/16/22 15:30 MJ EET SAVTotal/NA 15.57 g 1 mL
Analysis 8270E 1 756054 12/20/22 12:29 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Analysis MA VPH 1 336389 01/18/23 06:31 X875 ELLETotal/NA
10149Instrument ID:
Prep 5030C 328291 12/18/22 16:07 D8NM ELLETotal/NA 15.06 g 15 mL
Analysis MAVPH 50 333572 01/10/23 18:36 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Prep 3546 755500 12/16/22 13:33 MJ EET SAVTotal/NA 15.79 g 5 mL
Analysis 8081B 8082A 1 755553 12/16/22 22:09 JCK EET SAVTotal/NA 1 mL 1 mL
CSGJInstrument ID:
Prep 3546 329945 12/22/22 15:40 MD4W ELLETotal/NA 10.13 g 1 mL
Cleanup 3630C 331482 12/30/22 07:24 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 331706 12/31/22 04:18 UHEW ELLETotal/NA 1 mL 1 mL
18433-WInstrument ID:
Prep 3546 329945 12/22/22 15:40 MD4W ELLETotal/NA 10.13 g 1 mL
Cleanup 3630C 331482 12/30/22 07:24 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 331708 12/31/22 03:56 UHEW ELLETotal/NA 1 mL 1 mL
18433-XInstrument ID:
Prep 3060A 334897 01/12/23 10:42 UJE2 ELLETotal/NA 2.48 g 100 mL
Analysis 7199 1 335167 01/12/23 18:26 UJE2 ELLETotal/NA 1 mL 1 mL
26790Instrument ID:
Prep 3060A 334897 01/12/23 10:42 UJE2 ELLETotal/NA 2.48 g 100 mL
Analysis 7199 1 335167 01/12/23 18:33 UJE2 ELLETotal/NA 1 mL 1 mL
26790Instrument ID:
Prep 3050B 755270 12/15/22 13:26 SY EET SAVTotal/NA 1.15 g 500 mL
Analysis 6020B 1 755684 12/16/22 15:58 BWR EET SAVTotal/NA
ICPMSCInstrument ID:
Eurofins Savannah
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Lab Chronicle
Client: Sure-BioChem Laboratories LLC Job ID: 680-227663-1
Project/Site: CLFTBR0149 Ft. Bragg
Client Sample ID: 149-SB-1-20-12-22 Lab Sample ID: 680-227663-3
Matrix: SolidDate Collected: 12/13/22 12:15
Date Received: 12/15/22 09:00
Analysis Moisture KF12/16/22 16:021 EET SAV755523
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: 149-SB-1-20-12-22 Lab Sample ID: 680-227663-3
Matrix: SolidDate Collected: 12/13/22 12:15
Percent Solids: 94.5Date Received: 12/15/22 09:00
Prep 5035A FES12/16/22 12:07 EET SAV755487
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.321 g 5 mL
Analysis 8260D 1 756853 12/27/22 18:55 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 755512 12/16/22 15:30 MJ EET SAVTotal/NA 15.41 g 1 mL
Analysis 8270E 1 756054 12/20/22 12:50 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Analysis MA VPH 1 336389 01/18/23 06:31 X875 ELLETotal/NA
10149Instrument ID:
Prep 5030C 328291 12/18/22 16:07 D8NM ELLETotal/NA 15.05 g 15 mL
Analysis MAVPH 50 333572 01/10/23 19:17 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Prep 3546 329945 12/22/22 15:40 MD4W ELLETotal/NA 10.01 g 1 mL
Cleanup 3630C 331482 12/30/22 07:24 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 331706 12/31/22 04:41 UHEW ELLETotal/NA 1 mL 1 mL
18433-WInstrument ID:
Prep 3546 329945 12/22/22 15:40 MD4W ELLETotal/NA 10.01 g 1 mL
Cleanup 3630C 331482 12/30/22 07:24 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 331708 12/31/22 04:18 UHEW ELLETotal/NA 1 mL 1 mL
18433-XInstrument ID:
Prep 3060A 334897 01/12/23 10:42 UJE2 ELLETotal/NA 2.47 g 100 mL
Analysis 7199 1 335167 01/12/23 20:22 UJE2 ELLETotal/NA 1 mL 1 mL
26790Instrument ID:
Prep 3060A 334897 01/12/23 10:42 UJE2 ELLETotal/NA 2.47 g 100 mL
Analysis 7199 1 335167 01/12/23 20:28 UJE2 ELLETotal/NA 1 mL 1 mL
26790Instrument ID:
Prep 3050B 755270 12/15/22 13:26 SY EET SAVTotal/NA 1.06 g 500 mL
Analysis 6020B 1 755684 12/16/22 16:02 BWR EET SAVTotal/NA
ICPMSCInstrument ID:
Client Sample ID: 149-SB-1-30-12-22 Lab Sample ID: 680-227663-4
Matrix: SolidDate Collected: 12/13/22 13:30
Date Received: 12/15/22 09:00
Analysis Moisture KF12/16/22 16:021 EET SAV755523
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Eurofins Savannah
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Lab Chronicle
Client: Sure-BioChem Laboratories LLC Job ID: 680-227663-1
Project/Site: CLFTBR0149 Ft. Bragg
Client Sample ID: 149-SB-1-30-12-22 Lab Sample ID: 680-227663-4
Matrix: SolidDate Collected: 12/13/22 13:30
Percent Solids: 76.2Date Received: 12/15/22 09:00
Prep 5035A FES12/16/22 12:07 EET SAV755487
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.868 g 5 mL
Analysis 8260D 1 756853 12/27/22 19:18 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 755512 12/16/22 15:30 MJ EET SAVTotal/NA 15.60 g 1 mL
Analysis 8270E 1 756054 12/20/22 13:11 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Analysis MA VPH 1 336389 01/18/23 06:31 X875 ELLETotal/NA
10149Instrument ID:
Prep 5030C 328291 12/18/22 16:07 D8NM ELLETotal/NA 15.02 g 15 mL
Analysis MAVPH 50 333572 01/10/23 19:58 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Prep 3546 329945 12/22/22 15:40 MD4W ELLETotal/NA 10.28 g 1 mL
Cleanup 3630C 331482 12/30/22 07:24 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 331706 12/31/22 05:03 UHEW ELLETotal/NA 1 mL 1 mL
18433-WInstrument ID:
Prep 3546 329945 12/22/22 15:40 MD4W ELLETotal/NA 10.28 g 1 mL
Cleanup 3630C 331482 12/30/22 07:24 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 331708 12/31/22 04:41 UHEW ELLETotal/NA 1 mL 1 mL
18433-XInstrument ID:
Prep 3060A 334897 01/12/23 10:42 UJE2 ELLETotal/NA 2.42 g 100 mL
Analysis 7199 1 335167 01/12/23 20:09 UJE2 ELLETotal/NA 1 mL 1 mL
26790Instrument ID:
Prep 3060A 334897 01/12/23 10:42 UJE2 ELLETotal/NA 2.42 g 100 mL
Analysis 7199 1 335167 01/12/23 20:15 UJE2 ELLETotal/NA 1 mL 1 mL
26790Instrument ID:
Prep 3050B 755270 12/15/22 13:26 SY EET SAVTotal/NA 1.15 g 500 mL
Analysis 6020B 1 755684 12/16/22 16:06 BWR EET SAVTotal/NA
ICPMSCInstrument ID:
Client Sample ID: 149-SB-1-40-12-22 Lab Sample ID: 680-227663-5
Matrix: SolidDate Collected: 12/13/22 14:00
Date Received: 12/15/22 09:00
Analysis Moisture KF12/16/22 16:021 EET SAV755523
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: 149-SB-1-40-12-22 Lab Sample ID: 680-227663-5
Matrix: SolidDate Collected: 12/13/22 14:00
Percent Solids: 87.9Date Received: 12/15/22 09:00
Prep 5035A FES12/16/22 12:07 EET SAV755487
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.104 g 5 mL
Analysis 8260D 1 756853 12/27/22 19:42 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Eurofins Savannah
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Lab Chronicle
Client: Sure-BioChem Laboratories LLC Job ID: 680-227663-1
Project/Site: CLFTBR0149 Ft. Bragg
Client Sample ID: 149-SB-1-40-12-22 Lab Sample ID: 680-227663-5
Matrix: SolidDate Collected: 12/13/22 14:00
Percent Solids: 87.9Date Received: 12/15/22 09:00
Prep 3546 MJ12/16/22 15:30 EET SAV755512
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.21 g 1 mL
Analysis 8270E 1 756054 12/20/22 13:32 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Analysis MA VPH 1 336389 01/18/23 06:31 X875 ELLETotal/NA
10149Instrument ID:
Prep 5030C 328291 12/18/22 16:07 D8NM ELLETotal/NA 15.06 g 15 mL
Analysis MAVPH 50 333572 01/10/23 20:38 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Prep 3546 329945 12/22/22 15:40 MD4W ELLETotal/NA 10.32 g 1 mL
Cleanup 3630C 331482 12/30/22 07:24 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 331706 12/31/22 05:26 UHEW ELLETotal/NA 1 mL 1 mL
18433-WInstrument ID:
Prep 3546 329945 12/22/22 15:40 MD4W ELLETotal/NA 10.32 g 1 mL
Cleanup 3630C 331482 12/30/22 07:24 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 331708 12/31/22 05:03 UHEW ELLETotal/NA 1 mL 1 mL
18433-XInstrument ID:
Prep 3060A 334897 01/12/23 10:42 UJE2 ELLETotal/NA 2.61 g 100 mL
Analysis 7199 1 335167 01/12/23 19:56 UJE2 ELLETotal/NA 1 mL 1 mL
26790Instrument ID:
Prep 3060A 334897 01/12/23 10:42 UJE2 ELLETotal/NA 2.61 g 100 mL
Analysis 7199 1 335167 01/12/23 20:02 UJE2 ELLETotal/NA 1 mL 1 mL
26790Instrument ID:
Prep 3050B 755270 12/15/22 13:26 SY EET SAVTotal/NA 1.03 g 500 mL
Analysis 6020B 1 755684 12/16/22 16:10 BWR EET SAVTotal/NA
ICPMSCInstrument ID:
Client Sample ID: 149-SB-1-46-12-22 Lab Sample ID: 680-227663-6
Matrix: SolidDate Collected: 12/13/22 14:35
Date Received: 12/15/22 09:00
Analysis Moisture KF12/16/22 16:021 EET SAV755523
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: 149-SB-1-46-12-22 Lab Sample ID: 680-227663-6
Matrix: SolidDate Collected: 12/13/22 14:35
Percent Solids: 90.2Date Received: 12/15/22 09:00
Prep 5035A FES12/16/22 12:07 EET SAV755487
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.391 g 5 mL
Analysis 8260D 1 756853 12/27/22 20:05 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 755512 12/16/22 15:30 MJ EET SAVTotal/NA 15.39 g 1 mL
Analysis 8270E 1 756054 12/20/22 13:53 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Eurofins Savannah
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Lab Chronicle
Client: Sure-BioChem Laboratories LLC Job ID: 680-227663-1
Project/Site: CLFTBR0149 Ft. Bragg
Client Sample ID: 149-SB-1-46-12-22 Lab Sample ID: 680-227663-6
Matrix: SolidDate Collected: 12/13/22 14:35
Percent Solids: 90.2Date Received: 12/15/22 09:00
Analysis MA VPH X87501/18/23 06:311 ELLE336389
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Prep 5030C 328291 12/18/22 16:07 D8NM ELLETotal/NA 15.02 g 15 mL
Analysis MAVPH 50 333572 01/10/23 21:19 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Prep 3546 329945 12/22/22 15:40 MD4W ELLETotal/NA 10.20 g 1 mL
Cleanup 3630C 331482 12/30/22 07:24 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 331706 12/31/22 05:48 UHEW ELLETotal/NA 1 mL 1 mL
18433-WInstrument ID:
Prep 3546 329945 12/22/22 15:40 MD4W ELLETotal/NA 10.20 g 1 mL
Cleanup 3630C 331482 12/30/22 07:24 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH 1 331708 12/31/22 05:26 UHEW ELLETotal/NA 1 mL 1 mL
18433-XInstrument ID:
Prep 3060A 334897 01/12/23 10:42 UJE2 ELLETotal/NA 2.53 g 100 mL
Analysis 7199 1 335167 01/12/23 20:35 UJE2 ELLETotal/NA 1 mL 1 mL
26790Instrument ID:
Prep 3060A 334897 01/12/23 10:42 UJE2 ELLETotal/NA 2.53 g 100 mL
Analysis 7199 1 335167 01/12/23 20:41 UJE2 ELLETotal/NA 1 mL 1 mL
26790Instrument ID:
Prep 3050B 755270 12/15/22 13:26 SY EET SAVTotal/NA 1.07 g 500 mL
Analysis 6020B 1 755684 12/16/22 16:13 BWR EET SAVTotal/NA
ICPMSCInstrument ID:
Client Sample ID: FB-12-22 Lab Sample ID: 680-227663-7
Matrix: WaterDate Collected: 12/14/22 15:00
Date Received: 12/15/22 09:00
Analysis 8260D Y1S12/28/22 12:281 EET SAV757008
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CMSC
Prep 3510C 756109 12/20/22 11:44 MR EET SAVTotal/NA 524.7 mL 1 mL
Analysis 8270E 1 756690 12/23/22 20:33 T1C EET SAVTotal/NA 1 mL 1 mL
CMSGInstrument ID:
Analysis MA VPH 1 336389 01/18/23 06:38 X875 ELLETotal/NA
10149Instrument ID:
Analysis MAVPH 1 330695 12/28/22 12:30 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Prep 3510C 756376 12/21/22 13:43 MR EET SAVTotal/NA 253.7 mL 1 mL
Analysis 8081B 8082A 1 756577 12/22/22 18:27 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAAInstrument ID:
Prep 3510C 328608 12/19/22 18:32 A2VL ELLETotal/NA 1049.4 mL 1 mL
Cleanup 3630C 329620 12/21/22 20:14 K2IL ELLETotal/NA 1 mL 1 mL
Analysis MA-EPH 1 329935 12/22/22 23:49 UHEW ELLETotal/NA 1 mL 1 mL
18433-WInstrument ID:
Eurofins Savannah
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Lab Chronicle
Client: Sure-BioChem Laboratories LLC Job ID: 680-227663-1
Project/Site: CLFTBR0149 Ft. Bragg
Client Sample ID: FB-12-22 Lab Sample ID: 680-227663-7
Matrix: WaterDate Collected: 12/14/22 15:00
Date Received: 12/15/22 09:00
Prep 3510C A2VL12/19/22 18:32 ELLE328608
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 1049.4 mL 1 mL
Cleanup 3630C 329620 12/21/22 20:14 K2IL ELLETotal/NA 1 mL 1 mL
Analysis MA-EPH 1 329942 12/22/22 23:49 UHEW ELLETotal/NA 1 mL 1 mL
18433-XInstrument ID:
Analysis 7199 1 331059 12/28/22 18:45 UJE2 ELLEDissolved1 mL 1 mL
26790Instrument ID:
Analysis 7199 1 331059 12/28/22 18:52 UJE2 ELLEDissolved1 mL 1 mL
26790Instrument ID:
Prep 3005A 755393 12/16/22 06:22 RR EET SAVTotal Recoverable 50 mL 250 mL
Analysis 6020B 1 755684 12/16/22 18:50 BWR EET SAVTotal Recoverable
ICPMSCInstrument ID:
Client Sample ID: EQB-12-22 Lab Sample ID: 680-227663-8
Matrix: WaterDate Collected: 12/14/22 15:20
Date Received: 12/15/22 09:00
Analysis 8260D Y1S12/28/22 12:471 EET SAV757008
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CMSC
Prep 3510C 756109 12/20/22 11:44 MR EET SAVTotal/NA 507.7 mL 1 mL
Analysis 8270E 1 756690 12/23/22 20:58 T1C EET SAVTotal/NA 1 mL 1 mL
CMSGInstrument ID:
Analysis MA VPH 1 336389 01/18/23 06:38 X875 ELLETotal/NA
10149Instrument ID:
Analysis MAVPH 1 330695 12/28/22 13:11 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Prep 3510C 756376 12/21/22 13:43 MR EET SAVTotal/NA 262.2 mL 1 mL
Analysis 8081B 8082A 1 756577 12/22/22 18:41 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAAInstrument ID:
Prep 3510C 328608 12/19/22 18:32 A2VL ELLETotal/NA 1041 mL 1 mL
Cleanup 3630C 329620 12/21/22 20:14 K2IL ELLETotal/NA 1 mL 1 mL
Analysis MA-EPH 1 329935 12/23/22 00:11 UHEW ELLETotal/NA 1 mL 1 mL
18433-WInstrument ID:
Prep 3510C 328608 12/19/22 18:32 A2VL ELLETotal/NA 1041 mL 1 mL
Cleanup 3630C 329620 12/21/22 20:14 K2IL ELLETotal/NA 1 mL 1 mL
Analysis MA-EPH 1 329942 12/23/22 00:11 UHEW ELLETotal/NA 1 mL 1 mL
18433-XInstrument ID:
Analysis 7199 1 331059 12/28/22 18:33 UJE2 ELLEDissolved1 mL 1 mL
26790Instrument ID:
Analysis 7199 1 331059 12/28/22 18:39 UJE2 ELLEDissolved1 mL 1 mL
26790Instrument ID:
Prep 3005A 755393 12/16/22 06:22 RR EET SAVTotal Recoverable 50 mL 250 mL
Analysis 6020B 1 755684 12/16/22 18:54 BWR EET SAVTotal Recoverable
ICPMSCInstrument ID:
Eurofins Savannah
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Lab Chronicle
Client: Sure-BioChem Laboratories LLC Job ID: 680-227663-1
Project/Site: CLFTBR0149 Ft. Bragg
Client Sample ID: 149-TW-01 Lab Sample ID: 680-227663-9
Matrix: WaterDate Collected: 12/14/22 15:30
Date Received: 12/15/22 09:00
Analysis 8260D Y1S12/28/22 13:061 EET SAV757008
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CMSC
Prep 3510C 756109 12/20/22 11:44 MR EET SAVTotal/NA 495.7 mL 1 mL
Analysis 8270E 1 756690 12/23/22 21:25 T1C EET SAVTotal/NA 1 mL 1 mL
CMSGInstrument ID:
Analysis MA VPH 1 336389 01/18/23 06:38 X875 ELLETotal/NA
10149Instrument ID:
Analysis MAVPH 1 330695 12/28/22 13:51 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Prep 3510C 756376 12/21/22 13:43 MR EET SAVTotal/NA 256.7 mL 1 mL
Analysis 8081B 8082A 1 756577 12/22/22 18:56 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAAInstrument ID:
Prep 3510C 328608 12/19/22 18:32 A2VL ELLETotal/NA 1017 mL 1 mL
Cleanup 3630C 329620 12/21/22 20:14 K2IL ELLETotal/NA 1 mL 1 mL
Analysis MA-EPH 1 329935 12/23/22 00:34 UHEW ELLETotal/NA 1 mL 1 mL
18433-WInstrument ID:
Prep 3510C RE 330594 12/27/22 21:11 K2IL ELLETotal/NA 1015.7 mL 1 mL
Cleanup 3630C RE 331481 12/30/22 07:24 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH RE 1 331706 12/30/22 20:03 UHEW ELLETotal/NA 1 mL 1 mL
18433-WInstrument ID:
Prep 3510C REDL 330594 12/27/22 21:11 K2IL ELLETotal/NA 1015.7 mL 1 mL
Cleanup 3630C REDL 331481 12/30/22 07:24 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH REDL 2 332630 01/04/23 21:47 UHEW ELLETotal/NA 1 mL 1 mL
18433-WInstrument ID:
Prep 3510C 328608 12/19/22 18:32 A2VL ELLETotal/NA 1017 mL 1 mL
Cleanup 3630C 329620 12/21/22 20:14 K2IL ELLETotal/NA 1 mL 1 mL
Analysis MA-EPH 1 329942 12/23/22 00:34 UHEW ELLETotal/NA 1 mL 1 mL
18433-XInstrument ID:
Prep 3510C RE 330594 12/27/22 21:11 K2IL ELLETotal/NA 1015.7 mL 1 mL
Cleanup 3630C RE 331481 12/30/22 07:24 YDF5 ELLETotal/NA 1.0 mL 1.0 mL
Analysis MA-EPH RE 1 331708 12/30/22 20:03 UHEW ELLETotal/NA 1 mL 1 mL
18433-XInstrument ID:
Analysis 7199 1 331059 12/28/22 18:58 UJE2 ELLEDissolved1 mL 1 mL
26790Instrument ID:
Analysis 7199 1 331059 12/28/22 19:05 UJE2 ELLEDissolved1 mL 1 mL
26790Instrument ID:
Filtration FILTRATION 756221 12/21/22 07:02 RR EET SAVDissolved50 mL 50 mL
Prep 3005A 756223 12/21/22 07:02 RR EET SAVDissolved50 mL 250 mL
Analysis 6020B 1 756842 12/22/22 18:07 BWR EET SAVDissolved
ICPMSCInstrument ID:
Prep 3005A 755393 12/16/22 06:22 RR EET SAVTotal Recoverable 50 mL 250 mL
Analysis 6020B 1 755684 12/16/22 18:58 BWR EET SAVTotal Recoverable
ICPMSCInstrument ID:
Eurofins Savannah
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Lab Chronicle
Client: Sure-BioChem Laboratories LLC Job ID: 680-227663-1
Project/Site: CLFTBR0149 Ft. Bragg
Client Sample ID: 149-TW-01 Lab Sample ID: 680-227663-9
Matrix: WaterDate Collected: 12/14/22 15:30
Date Received: 12/15/22 09:00
Filtration FILTRATION JKL12/16/22 08:47 EET SAV755404
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Dissolved 50 mL 50 mL
Prep 7470A 755407 12/16/22 08:53 JKL EET SAVDissolved50 mL 50 mL
Analysis 7470A 1 755947 12/19/22 09:58 JKL EET SAVDissolved
QuickTrace2Instrument ID:
Client Sample ID: DUP-TW-01 Lab Sample ID: 680-227663-10
Matrix: WaterDate Collected: 12/14/22 16:00
Date Received: 12/15/22 09:00
Analysis 8260D Y1S12/28/22 13:241 EET SAV757008
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CMSC
Prep 3510C 756109 12/20/22 11:44 MR EET SAVTotal/NA 537.3 mL 1 mL
Analysis 8270E 1 756690 12/23/22 21:51 T1C EET SAVTotal/NA 1 mL 1 mL
CMSGInstrument ID:
Analysis MA VPH 1 336389 01/18/23 06:38 X875 ELLETotal/NA
10149Instrument ID:
Analysis MAVPH 1 330695 12/28/22 14:32 X875 ELLETotal/NA 5 mL 5 mL
10149Instrument ID:
Prep 3510C 756376 12/21/22 13:43 MR EET SAVTotal/NA 267 mL 1 mL
Analysis 8081B 8082A 1 756577 12/22/22 19:10 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAAInstrument ID:
Prep 3510C 328608 12/19/22 18:32 A2VL ELLETotal/NA 1049.2 mL 1 mL
Cleanup 3630C 329620 12/21/22 20:14 K2IL ELLETotal/NA 1 mL 1 mL
Analysis MA-EPH 1 329935 12/23/22 00:56 UHEW ELLETotal/NA 1 mL 1 mL
18433-WInstrument ID:
Prep 3510C 328608 12/19/22 18:32 A2VL ELLETotal/NA 1049.2 mL 1 mL
Cleanup 3630C 329620 12/21/22 20:14 K2IL ELLETotal/NA 1 mL 1 mL
Analysis MA-EPH 1 329942 12/23/22 00:56 UHEW ELLETotal/NA 1 mL 1 mL
18433-XInstrument ID:
Analysis 7199 1 331059 12/28/22 18:20 UJE2 ELLEDissolved1 mL 1 mL
26790Instrument ID:
Analysis 7199 1 331059 12/28/22 18:26 UJE2 ELLEDissolved1 mL 1 mL
26790Instrument ID:
Prep 3005A 755393 12/16/22 06:22 RR EET SAVTotal Recoverable 50 mL 250 mL
Analysis 6020B 1 755684 12/16/22 19:02 BWR EET SAVTotal Recoverable
ICPMSCInstrument ID:
¹ Completion dates and times are reported or not reported per method requirements or individual lab discretion.
Laboratory References:
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
ELLE = Eurofins Lancaster Laboratories Environment Testing, LLC, 2425 New Holland Pike, Lancaster, PA 17601, TEL [phone]
Eurofins Savannah
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Accreditation/Certification Summary
Client: Sure-BioChem Laboratories LLC Job ID: 680-227663-1
Project/Site: CLFTBR0149 Ft. Bragg
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
ANAB Dept. of Defense ELAP L2463 09-22-24
North Carolina (WW/SW)State 269 12-31-22
Laboratory: Eurofins Lancaster Laboratories Environment Testing, LLC
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
A2LA Dept. of Defense ELAP 0001.01 11-30-24
North Carolina (WW/SW)State 521 12-31-23
Eurofins Savannah
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Method Summary
Job ID: 680-227663-1Client: Sure-BioChem Laboratories LLC
Project/Site: CLFTBR0149 Ft. Bragg
Method Method Description LaboratoryProtocol
SW8468260DVolatile Organic Compounds (GC/MS)EET SAV
SW8468270ESemivolatile Organic Compounds (GC/MS)EET SAV
MA DEPMA VPH Massachusetts - Volatile Petroleum Hydrocarbons (GC)ELLE
MA DEPMAVPHMassachusetts - Volatile Petroleum Hydrocarbons (GC)ELLE
SW8468081B 8082A Organochlorine Pesticides & PCBs (GC)EET SAV
MA DEPMA-EPH Massachusetts - Extractable Petroleum Hydrocarbons (GC)ELLE
SW8467199Chromium, Hexavalent (IC)ELLE
SW8466020BMetals (ICP/MS)EET SAV
SW8467470AMercury (CVAA)EET SAV
EPAMoisturePercent Moisture EET SAV
SW8463005APreparation, Total Recoverable or Dissolved Metals EET SAV
SW8463050BPreparation, Metals EET SAV
SW8463060AAlkaline Digestion (Chromium, Hexavalent)ELLE
SW8463510CLiquid-Liquid Extraction (Separatory Funnel)EET SAV
SW8463510CLiquid-Liquid Extraction (Separatory Funnel)ELLE
SW8463546Microwave Extraction EET SAV
SW8463546Microwave Extraction ELLE
SW8463630CSilica Gel Cleanup ELLE
SW8465030CPurge and Trap EET SAV
SW8465030CPurge and Trap ELLE
SW8465035AClosed System Purge & Trap EET SAV
SW8467470APreparation, Mercury EET SAV
NoneFILTRATIONSample Filtration EET SAV
Protocol References:
EPA = US Environmental Protection Agency
MA DEP = Massachusetts Department Of Environmental Protection
None = None
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
ELLE = Eurofins Lancaster Laboratories Environment Testing, LLC, 2425 New Holland Pike, Lancaster, PA 17601, TEL [phone]
Eurofins Savannah
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Login Sample Receipt Checklist
Client: Sure-BioChem Laboratories LLC Job Number: 680-227663-1
Login Number: 227663
Question Answer Comment
Creator: Sims, Robert D
List Source: Eurofins Savannah
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Savannah
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Login Sample Receipt Checklist
Client: Sure-BioChem Laboratories LLC Job Number: 680-227663-1
Login Number: 227663
Question Answer Comment
Creator: Roth, Stephanie
List Source: Eurofins Lancaster Laboratories Environment Testing, LLC
List Creation: 12/17/22 12:29 PMList Number: 2
TrueThe cooler's custody seal is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable (</=6C, not frozen).
TrueCooler Temperature is recorded.
N/AWV: Container Temperature is acceptable (</=6C, not frozen).
N/AWV: Container Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueThere are no discrepancies between the containers received and the COC.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueThere is sufficient vol. for all requested analyses.
FalseIs the Field Sampler's name present on COC?Received project as a subcontract.
N/ASample custody seals are intact.
TrueVOA sample vials do not have headspace >6mm in diameter (none, if from
WV)?
Eurofins Savannah
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