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HomeMy WebLinkAboutFA-7738_42025_CA_MRP_20231025Groundwater Monitoring Report CLES Project No. 17-051A Seminole Mart No. 2, Broadway, NC October 25, 2023 i TABLE OF CONTENTS 1.0 BACKGROUND ............................................................................................................... 1 1.1 SITE INFORMATION .......................................................................................................... 1 1.2 HYDROGEOLOGICAL DESCRIPTION .................................................................................... 3 1.2.1 Regional Geologic Setting ...................................................................................... 3 1.2.2 Site Hydrogeology .................................................................................................. 3 1.2.3 Subsurface Lithology.............................................................................................. 3 2.0 SITE ACTIVITIES ............................................................................................................. 4 2.1 LIQUID LEVEL MONITORING AND SAMPLING ........................................................................ 4 2.2 GROUNDWATER SAMPLING AND ANALYSIS ......................................................................... 4 3.0 RESULTS ........................................................................................................................ 5 3.1 ELEVATION MEASUREMENTS, GROUNDWATER FLOW, AND GRADIENT ................................... 5 3.2 GROUNDWATER ANALYTICAL RESULTS .............................................................................. 5 4.0 CONCLUSIONS ............................................................................................................... 7 5.0 RECOMMENDATIONS .................................................................................................... 7 6.0 REFERENCES ................................................................................................................. 8 TABLES Table 1: Monitor Well Construction Table 2: Historical Groundwater Elevations Table 3: Groundwater Elevations – October 5, 2023 Table 4: Field Parameters Table 5: Historical Groundwater Sample Data Table 6: Groundwater Analytical Results – October 5, 2023 FIGURES Figure 1: Vicinity Map Figure 2: Site Map Figure 3: Groundwater Potentiometric Map (October 5, 2023) Figure 4: Groundwater Constituent Concentrations (October 5, 2023) Figure 5: Pre-Remedial Benzene Isoconcentration Map (November 1, 2017) Figure 6: Benzene Isoconcentration Map (October 5, 2023) APPENDICES Appendix I Standard Operating Procedures Appendix II Calculations Appendix III Laboratory Analytical Results and Chain of Custody Forms Groundwater Monitoring Report CLES Project No. 17-051A Seminole Mart No. 2, Broadway, NC October 25, 2023 1 1.0 BACKGROUND 1.1 Site Information The Seminole Mart No. 2 site is located at 691 Seminole Road in Broadway, North Carolina (Figure 1). According to reports prepared by East Coast Environmental, PA (ECE), underground storage tanks (USTs) were closed at the site in 2016. The UST closure assessment encountered diesel fuel constituents that were detected with concentrations above North Carolina Department of Environmental Quality (NCDEQ) action levels at the site. Based on findings by the previous consultant, the site was classified by the NCDEQ Division of Waste Management (DWM) UST Section as a “commercial high” risk site. The following are some of the activities that have taken place at the site since September 2016: Ø One 10,000-gallon gasoline and one 4,000-gallon diesel fuel petroleum USTs were permanently closed by removal in September 2016; Ø Petroleum contamination was evident in the excavation for the diesel fuel UST due to a hole in the tank and below the former product dispensers. Approximately 204 tons of contaminated soil from released diesel fuel were excavated and removed from the site. Ø A monitor well network (Table 1) was installed by ECE, PA, in January, March, May, October, and December of 2017. The borings and well network wells were used to assess the soil near the former UST system, delineate free product on the groundwater table and delineate dissolved petroleum constituents in the groundwater. Ø Baseline groundwater monitoring events were performed by ECE, PA, in 2017 prior to implementing the remedial program. The baseline data indicated that eleven of the existing monitor wells (MW-1, MW-2, MW-3, MW-4, MW-8, MW-11, MW-12, MW-13, MW-14, MW-17 and MW-19) had a measurable thickness of free product as diesel fuel. The initial maximum free product (diesel fuel) thickness recorded in network wells in 2017 included: MW-1 - 2.85 ft., MW-2 – 1.76 ft., MW-3 – 3.0 ft., MW-4 – 1.90 ft., MW-8 – 2.48 ft., MW-11 – 5.41 ft., MW- 12 – 1.71 ft., MW-13 – 2.07 ft., MW-14 – 1.67 ft., MW-17 – 2.0 ft. and MW-19 – 1.64 ft. Ø The NCDEQ issued Injection Permit WI0600195 for the remedial approach using injection of surfactant solutions. Ø Surfactant Injection (~19,165 gallons) was performed in April 30 – May 10, 2018. Ø Aggressive fluid-vapor recovery (AFVR) was performed May 21-24, 2018, from source wells impacted by petroleum, recovered 3,205 gallons of product, surfactant/product emulsion, surfactant and petroleum-contaminated water. Ø Total fluids recovery was performed between May 25, 2018 and October 26, 2021, using automated cycling of submersible pumps to recover free product, surfactant with emulsified petroleum product and contaminated groundwater. Ø Liquid level monitoring and well maintenance activities were performed by ECE, PA, in June 2018, and gasoline was observed as free product in addition to diesel fuel on the water table. Ø The baseline data was used to calculate the quantity and concentration of the surfactant solution that would be necessary to remediate the free product plume. However, the actual maximum free product thickness was subsequently found to be approximately double the amount that was identified during the baseline Groundwater Monitoring Report CLES Project No. 17-051A Seminole Mart No. 2, Broadway, NC October 25, 2023 2 assessment due to the presence of significant gasoline free product that was located on top of the diesel free product. The gasoline free product was not identified because it was initially located above the screened intervals of the monitor wells. As the thickness of the diesel free product was reduced to below the top of the screened interval, the gasoline free product was able to enter the monitor wells. Therefore, injecting additional surfactant solution was necessary to contact and remediate the additional gasoline free product plume that was located at shallower depths than the diesel free product. Ø Product thicknesses observed after the injection were a result of the surfactant stripping product from source area soils, which included both diesel fuel and gasoline products. Ø Liquid level data following the initial injection and extraction event indicated that now 13 of the existing monitor wells had a measurable thickness of free product as diesel fuel and/or gasoline. The maximum free product thickness recorded in network wells since the initial injection event included: MW-1 – 1.89 ft., MW-2 – 3.01 ft., MW-3 – 1.55 ft., MW-4 – 0.05 ft., MW-8 – 0.67 ft., MW-9 – 0.77 ft., MW- 10 – 4.54 ft., MW-11 – 4.43 ft. (gasoline), MW-12 – 0.23 ft., MW-14 – 0.33 ft., MW-15 – 1.82 ft., MW-16 – 1.34 ft., and MW-17 – 2.96 ft (red text used to identify locations where free product was not previously observed). Well locations MW- 13 and MW-19 had no measurable thickness of free product as gasoline or diesel fuel since the first injection/extraction event. Ø Approximately 2,750 gallons of surfactant solution were injected September 6-7, 2019, approximately 2,750 gallons of surfactant were injected between October 31, and November 6, 2019, and approximately 2,900 gallons of surfactant were injected into source area wells with evidence of product skim in the well screened intervals in June 2021. Ø Total fluids recovery has been performed on source area wells where free product is persistent on the water table. Since May 2018, over 83,260 gallons of liquids contaminated with petroleum have been recovered from the site. Ø CLES continues well maintenance, free product recovery and liquid level monitoring. Product was removed either by bailers or with pumps based on the liquid column height in the well. Since October 2021, free product recovery has been performed manually to reduce the volume of recovered groundwater that is not necessary to remove from the site. Ø Additional total fluids recovery has been performed approximately monthly using manually operated pumps or hand bailing to remove free phase product from the water table. This Groundwater Monitoring Report details the site activities that were performed from Februry 2023 to October 2023. Ø CLES performed well and pump maintenance, manual total fluids recovery and liquid level monitoring between February 2023 and October 2023. Obsevations from the overall liquid level data indicate that the free product plume continues to decrease in size. The total thickness of free phase petroleum (diesel fuel and gasoline continue to be managed using total fluids removal from source area wells by bailing and/or pumping that was performed during site visits. Ø Prior to sampling on October 5, 2023, groundwater level measurements were collected from the well network to document groundwater elevations at the site and to estimate the groundwater flow direction and hydraulic gradient on-site. Groundwater Monitoring Report CLES Project No. 17-051A Seminole Mart No. 2, Broadway, NC October 25, 2023 3 Ø Groundwater samples from 19 of the network monitor wells that intersect the water table at the site were collected on October 5, 2023. Groundwater samples were submitted for laboratory analysis for volatile organic compounds (VOCs) by Method 624.1. Figure 2, Site Map, presents the site features and monitor well locations. 1.2 Hydrogeological Description 1.2.1 Regional Geologic Setting According to the North Carolina Geologic Survey, Geologic Map of North Carolina, 1985, the site rests just east of the Fall Line, or boundary between the Piedmont Upland and the Coastal Plain. Unconsolidated sediments with varying thicknesses rest non- conformably over sedimentary deposits of the Middendorf formation. The Middendorf formation consists of Cretaceous Age sand, sandstone and mudstone deposits. Groundwater occurs in residual soils that were weathered from parent sedimentary rock. Based on the surface topography depicted in the United States Geologic Survey (USGS) National Map viewer of Topographic Maps, (Figure 1), the site rests at an elevation of approximately 475 feet above mean sea level (ft-MSL). Topography on site slopes down from Seminole Road to the north-northwest, and to the south-southwest. The surface water features in the vicinity of the site are shown on Figure 1. 1.2.2 Site Hydrogeology Monitor wells installed at the site, as well as published geologic information, were used to describe site-specific hydrology. A summary of the monitor well construction of on- site monitor wells is presented in Table 1. The monitor well locations are shown on Figure 2. Groundwater levels measured July 21, 2022 in the monitor wells on site indicate that groundwater is present at depths between 37.66 feet below the top of the well casing (ft-btoc) in MW-1 and 44.64 ft-btoc in MW-16. The monitor well relative top- of-casing elevations were previously reported by ECE, PA, as measured relative to an assigned elevation of a site reference point. Historical groundwater level and elevation data as reported by ECE, PA, and recent measurements by CLES are summarized in Table 2. The groundwater potentiometric map, based on maps prepared by ECE, PA, and measurements by CLES is presented on Figure 3. 1.2.3 Subsurface Lithology According to ECE, PA, the subsurface residual soils were typically composed of fine- grained clayey silt or silty clay, silt and sand to approximately 12 feet below the ground surface (ft-bgs). The fine-grained soils rested over a zone of silty sand with rounded pebbles in some locations from approximately 12 to over 20 feet in depth. Silt with sand or silty sand from below the pebble zone rested over a white silty clay layer that was encountered between 35 and 49 ft-bgs. Zones of medium and coarse sand were also observed near and below the water table. The color of the soils varied from orange red brown, yellow, white, brown, tan, orange or white with black. Bedrock was not encountered to the termination depths of the borings. Groundwater Monitoring Report CLES Project No. 17-051A Seminole Mart No. 2, Broadway, NC October 25, 2023 4 2.0 SITE ACTIVITIES 2.1 Liquid Level Monitoring and Sampling Liquid levels in the 21 network wells were measured on October 5, 2023, using an oil- water interface probe. CLES’ personnel gauged liquid levels in general accordance with the CLES Standard Operating Procedures (SOP). A copy of the CLES SOP is presented in Appendix I. The measurement device was decontaminated between measurements. A measurable thickness of gasoline/diesel fuel (0.01 feet or greater) as free product was present in MW-1, MW-2, MW-3, MW-8, MW-10, MW-11 and MW-17. No measurable thickness of petroleum product was observed in the remaining network wells that were gauged. CLES initiated purging activities to prepare for sampling. A submersible pump with a stainless-steel motor and impeller connected to polyethylene tubing that was decontaminated before inserting it into each well, or an unused disposable bailer with nylon cord, was used to purge the water column from the well before sampling. Purge parameters including pH, conductivity and temperature were measured and the values were recorded on field forms during well purging. Field parameters representative of the aquifer before sampling on October 5, 2023, are summarized in Table 4. A summary of the data recorded on the field forms is presented in Appendix II. Using the October 5, 2023, groundwater level data (summarized in Table 3), groundwater elevations were calculated for network monitor wells that intersect the water table. The potentiometric surface of the groundwater table was drawn using groundwater contours of equal elevation that were estimated to predict the groundwater flow direction across the site (Figure 3). Groundwater elevations on October 5, 2023, indicate that the site-specific groundwater flow direction is generally to the east- northeast and the hydraulic gradient, calculated using a three-point calculation from the water levels in MW-5, MW-20, and MW-21, was estimated to be 7.8 x 10-3 feet/foot (ft/ft) to the east-southeast. 2.2 Groundwater Sampling and Analysis On October 5, 2023, CLES collected groundwater samples from 19 of the network monitor wells at the site. Samples were not collected from piezometers P-1 to P-6, or wells MW-2 or MW-3 (that had insufficient water to sample below the product) during this event. Bailers with nylon cords and/or decontaminated sample pump with polyethylene tubing were used to collect groundwater samples from the monitor wells in general accordance with NCDEQ sampling guidance and CLES’ SOPs (Appendix I). The groundwater samples were collected and analyzed to measure the dissolved VOC concentrations in the site monitor wells after implementing supplemental surfactant injection followed by total fluids extraction. Groundwater samples were submitted to Eurofins Raleigh (formerly Environmental Conservation Laboratories, Inc.), for the following laboratory analyses: VOCs by USEPA Method 624.1. Groundwater Monitoring Report CLES Project No. 17-051A Seminole Mart No. 2, Broadway, NC October 25, 2023 5 3.0 RESULTS 3.1 Elevation Measurements, Groundwater Flow, and Gradient The depth to liquids in the monitor wells measured from the top of casing ranged from 35.71 feet below the top of the well casing (ft-btoc) in MW-1 and 44.3 ft-btoc in MW-2 on October 5, 2023. Using the liquid levels measured this quarter and the relative top of casing (toc) elevation data provided by ECE, PA, groundwater surface elevations were calculated at each well location. Groundwater elevations across the site ranged from a high elevation of 57.98 ft-rel elevation in MW-1 (corrected for the presence of petroleum), to a low elevation of 49.68 ft-rel elevation in MW-21. Based on the potentiometric surface of the water table presented on Figure 3, in general, the groundwater flow appears to be to the east-northeast at a gradient of approximately 0.0078 ft/ft. The methods and calculations used to determine the hydraulic gradient and groundwater flow direction are presented in Appendix II. 3.2 Groundwater Analytical Results Groundwater samples from the network monitor wells at the site collected on October 5, 2023, were submitted for laboratory analysis. The table below provides a summary of the constituents and the well locations where the groundwater sample analysis identified concentrations that exceeded their respective Title 15A North Carolina Administrative Code 2L Groundwater Quality Standard (2L Standard). Constituent Wells with Concentrations above 2L Standard NCAC 2L Standard (µg/L) NCDEQ GCL (µg/L) Well with Maximum Concentration (µg/L) / Wells with Concentrations above GCL Benzene MW-1, MW-9, MW-10, MW-11 1.0 5,000 MW-1: 72 MTBE MW-8, MW-15 20 20,000 MW-15: 34 Naphthalene MW-1, MW-8, MW-10, MW-11, MW-13, MW-17, MW-19, MW-20 6 6,000 MW-8: 33 Total Xylenes MW-1, MW-11 500 85,500 MW-1: 810 2L Standard = 15A North Carolina Administrative Code 2L Groundwater Quality Standard * Indicates IMAC value NCDEQ GCL = Gross Contamination Level in groundwater Groundwater samples collected from 4 monitor wells contained benzene, each of which had concentrations that exceed the benzene 2L Standard of 1 microgram per liter (μg/L). MW-2 and MW-3 were not sampled due to insufficient water in the well below the free phase petroleum. Some analytical detection levels of the groundwayer samples were higher than concentrations previously reported for constituents present in the groundwater. Ten of the groundwater samples analyzed contained ethylbenzene; however, none of the reported concentrations exceeded the 2L Standard of 600 μg/L. Groundwater Monitoring Report CLES Project No. 17-051A Seminole Mart No. 2, Broadway, NC October 25, 2023 6 No groundwater samples contained isopropyl ether at concentrations that were above the 2L Standard of 20, or the practical quantitation level for the samples analyzed. MTBE concetrations were reported in groundwater from five wells, two of these samples had concentrations measured that were above the 2L Standard of 20 μg/L. Eleven groundwater samples contained naphthalene and eight of these samples were reported to contain naphthalene concentrations that were measured above the 2L Standard of 6 μg/L. Six groundwater samples contained toluene; however, none of the samples were reported to be at concentrations that were above the 2L Standard of 600 μg/L. Total xylenes were measured in 13 groundwater samples analyzed for VOCs, of which, two samples were reported with total xylenes concentrations that were measured above the 2L Standard of 500 µg/L. Piezometers P-1 to P-6 do not intersect the groundwater table; thus, they were not sampled. Wells MW-2, and MW-3, were not sampled this event. Historical groundwater analytical data collected from 2017 to the current data set in Ocober 2023 are compared to both the 2L Standards and the NCDEQ GCLs and are summarized in Table 5. A copy of the laboratory report for the groundwater analyses from samples collected October 5, 2023, is included in Appendix III. The locations of monitor wells and the petroleum constituents detected in the groundwater samples collected October 5, 2023, are presented in Figure 4. The pre-remedial benzene isoconcentration contours and the former area of free product that were plotted using the data reported November 1, 2017 (ECE, PA), are presented in Figure 5. Benzene concentrations in the groundwater sampled on October 5, 2023, are shown in the isoconcentration contour map presented in Figure 6. Comparing the pre-remediation data reported November 1, 2017 (Figure 5), and the post-remediation data from January 28, 2022 (Figure 6), shows the reduction of the petroleum plume area since the remedial activities were implemented. The innovative remedial approach was initiated between April 30, 2018 and May 10, 2018 with supplemental injection events followed by extraction that were performed in September 6-7, 2018, October 31 to November 6, 2019, and June 17-19, 2021. Based on isoconcentration contours plotted from the 2017 pre-remedial data, the benzene plume was in an oval area approximately 75 feet by 101 feet (~6800 sq ft), and the measurable free product was in a similarly oval area that was approximately 56 feet wide by 78 feet long (~3950 sq ft). Note: The maximum thickness of product in 2017 as diesel fuel was 5.41 feet at MW-11. Based on the October 5, 2023 laboratory data, the extent of the benzene plume where concentrations were reported above the 2L Standard was estimated to be in an area of approximately 2,400 square feet. The area with measurable free product was in an oval area approximately 990 square feet. The new maximum product thickness measured October 5, 2023 was 1.2 (diesel fuel) feet in MW- 3, central to the recovery area. Based on current groundwater analyses, the magnitude of total volatile organic compound concentrations measured in the monitor well network is decreasing. Groundwater Monitoring Report CLES Project No. 17-051A Seminole Mart No. 2, Broadway, NC October 25, 2023 7 Groundwater sampled from wells MW-4, MW-5, MW-6, MW-7, MW-12, MW-14, MW-16, MW-18, and MW-21 each had no pertroleum compound concentrations measured above action levels. 4.0 CONCLUSIONS The activities conducted since February 2023 at the Seminole Mart No. 2 site included site maintenance, total fluids recovery, and sampling the groundwater from the well network to assess the current site conditions. Total fluids recovery was performed using, manual bailing, and/or manual pump operation during site visits. To date, more than 83,260 gallons of total fluids have been recovered from the site. Groundwater monitoring was performed to evaluate the site for the presence of residual free product and to document the extent of dissolved concentrations remaining in the groundwater after the supplemental remedial actions were implemented. Liquid levels were measured in the monitor well network on October 5, 2023. Based on the potentiometric surface of the water table, the groundwater flow is generally to the east-northeast at a hydraulic gradient of approximately 0.0078 ft/ft. A measurable thickness of free product greater than 0.01 feet was observed in six wells, MW-17 had a measurement of 0.01 feet. No other liquid level measurements detected free product in the network monitor wells gauged or sampled in this event. Groundwater samples were collected from 19 of the network monitor wells at the site October 5, 2023. The benzene in four groundwater samples was measured at a concentration that was above the 2L Standard in this event. In addition to benzene, MTBE, naphthalene and total xylenes were reported at concentrations above their respective 2L Standard in one or more wells. Based on isoconcentration contours plotted using the October 5, 2023, laboratory data, the benzene concentrations were above the 2L Standard in an area approximately 2,400 square feet. The area with measurable free product was in an oval area approximately 990 square feet, which is significantly reduced from the free product area of 56 feet wide by 78 feet long that was observed in 2017. The maximum product thickness measured on October 5, 2023 was 1.2 feet in MW-3. 5.0 RECOMMENDATIONS CLES recommends that the following actions be taken for timely and cost-effective remediation to continue at the Seminole Mart No. 2 site: • Continue the groundwater quality monitoring program in general accordance with the approved revised semi-annual monitoring schedule. • Continue total fluids recovery until there is no measurable thickness of product in the well network on site greater than 0.01 feet on the water table measured in the network wells. CLES recommends utilizing mobile multi-phase extraction (MMPE) or aggressive fluid vapor recovery (AFVR) as an alternative for total fluids recovery as the product thickness and plume dimensions are reduced at the site to improve the efficiency of the recovery effort. • Use groundwater quality monitoring data to assess effectiveness of the corrective measures and make necessary modifications to the recovery operations to Groundwater Monitoring Report CLES Project No. 17-051A Seminole Mart No. 2, Broadway, NC October 25, 2023 8 further attenuate the contaminant plume. After free product is not measurable in the wells at the site, sample the network quarterly to facilitate closure of the incident with NCDEQ. 6.0 REFERENCES Cape Lookout Environmental Sciences, PLLC, Groundwater Monitoring Report Seminole Mart No. 2, Broadway, NC, March 13, 2023. Cape Lookout Environmental Sciences, PLLC, Groundwater Monitoring Report Seminole Mart No. 2, Broadway, NC, August 8, 2022. Cape Lookout Environmental Sciences, PLLC, Groundwater Monitoring Report Seminole Mart No. 2, Broadway, NC, February 18, 2022. North Carolina Department of Natural Resources and Community Development, Geologic Map of North Carolina, 1985. East Coast Environmental, PA, UST-3 Notice of Intent: UST Permanent Closure or Change-in-Service, August 24, 2016. East Coast Environmental, PA, UST-61 24-Hour Release and UST Leak Reporting Form, September 13, 2016. East Coast Environmental, PA, 20 Day Report, September 30, 2016. East Coast Environmental, PA, Initial Abatement Actions Report with UST Closure Report, October 3, 2016. East Coast Environmental, PA, Limited Site Assessment, Phase I, February 15, 2017. East Coast Environmental, PA, Free Product Assessment Report, June 8, 2017. East Coast Environmental, PA, MMPE Report, August 11, 2017. East Coast Environmental, PA, Free Product Removal/Corrective Action Plan, February 5, 2018. Cape Lookout Environmental Sciences, PLLC, Injection Well Permit Application, February 1, 2018. East Coast Environmental, PA, Free Product Removal Update and Groundwater Sampling Event, May 2, 2019. East Coast Environmental, PA, Free Product Removal Update and Groundwater Sampling Event, November 21, 2019. Cape Lookout Environmental Sciences, PLLC, Groundwater Monitoring Report, September 7, 2021. Groundwater Monitoring Report CLES Project No. 17-051A Seminole Mart No. 2, Broadway, NC October 25, 2023 9 TABLES Table 1: Monitor Well Construction Table 2: Historical Groundwater Elevations Table 3: Groundwater Elevations – July 21, 2022 Table 4: Field Parameters Table 5: Historical Groundwater Sample Data Table 6: Groundwater Analytical Results – July 21, 2022 SEMINOLE MART 2 CLES PROJECT 17-051A GROUNDWATER MONIITORING REPORT OCTOBER 2023 TABLE 1 MONITOR WELL CONSTRUCTION SEMNOLE MART NO. 2 691 SEMINOLE ROAD BROADWAY, HARNETT COUNTY, NORTH CAROLINA NCDEQ INCIDENT NO. 42025 NCDEQ UST SECTION FACILITY ID. 0-000014231 CLES PROJECT NO. 17-051A Well ID Contractor/C onsultant Date Installed (m/dd/yy) Date Water Level Measured (m/dd/yy) Well Casing Depth (ft-bgs) Bottom of Well (ft-bgs) ~Top of Ground Elevation (ft- rel) Top of Casing Elevation (ft-rel) Depth to Water from Top of Casing (ft-btoc) Free Product Thicknessa (ft.) Groundwater Elevation (ft-rel) Construction Details MW-1 Quantex/ECE 01/31/17 10/31/17 15 15 to 40.0 40 94.095 93.72 37.75 1.15 56.93 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-2 Quantex/ECE 03/13/17 10/31/17 30 30 to 45.0 45 94.610 94.36 44.45 0.45 50.28 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-3 Quantex/ECE 03/13/17 10/31/17 30 30 to 45.0 45 93.788 93.58 44.02 0.80 50.23 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-4 Quantex/ECE 03/13/17 10/31/17 30 30 to 45.0 45 93.787 93.52 43.50 0.20 50.19 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-5 Quantex/ECE 05/01/17 10/31/17 28 28 to 48.0 48 93.733 93.40 43.18 0.00 50.22 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-6 Quantex/ECE 05/01/17 10/31/17 29 29 to 49.0 49 93.115 92.84 42.77 0.00 50.07 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-7 Quantex/ECE 05/01/17 10/31/17 28 28 to 48.0 48 93.270 92.92 42.77 0.00 50.15 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-8 Quantex/ECE 10/24/17 10/31/17 30 30 to 50.0 50 93.880 93.38 45.03 1.95 49.97 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-9 Quantex/ECE 10/24/17 10/31/17 30 30 to 50.0 50 93.988 93.63 43.42 0.00 50.21 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-10 Quantex/ECE 10/25/17 10/31/17 30 30 to 50.0 50 94.747 94.48 44.22 0.00 50.26 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-11 Quantex/ECE 10/26/17 10/31/17 25 25 to 50.0 50 94.332 93.79 45.50 2.15 50.08 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-12 Quantex/ECE 10/26/17 10/31/17 35 35 to 50.0 50 93.462 92.92 43.64 1.02 50.13 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-13 Quantex/ECE 10/26/17 10/31/17 35 35 to 50.0 50 94.000 93.50 44.50 1.20 50.00 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-14 Quantex/ECE 10/26/17 10/31/17 35 35 to 50.0 50 93.113 92.78 43.80 1.30 50.06 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-15 Quantex/ECE 10/26/17 10/31/17 20 20 to 50.0 50 94.430 93.93 43.64 0.00 50.29 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-16 Quantex/ECE 10/26/17 10/31/17 30 30 to 50.0 50 94.890 94.64 44.40 0.00 50.24 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-17 Quantex/ECE 11/29/17 12/05/17 30 30 to 50.0 50 94.182 93.74 45.85 2.00 49.55 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-18 Quantex/ECE 11/29/17 12/05/17 30 30 to 50.0 50 92.743 92.31 42.90 0.00 49.41 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-19 Quantex/ECE 11/29/17 12/05/17 30 30 to 50.0 50 93.192 92.65 44.42 1.44 49.43 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-20 Quantex/ECE 11/29/17 12/05/17 30 30 to 50.0 50 94.258 93.65 44.23 0.00 49.42 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-21 Quantex/ECE 11/29/17 12/05/17 30 30 to 50.0 50 93.378 92.92 43.98 0.00 48.94 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. Notes a If Diesel Fuel Free Product is present in a well, groundwater elevation is calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.832].ft-bgs Feet below ground surface.ft-btoc Feet below top of well casing. ft-rel Elevation relative to mean sea level as measured by east Coast Environmental, PA 10/31/17. Screen Interval (x to y ft-bgs) SEMINOLE MART NO 2 CLES PROJECT 17-051A GROUNDWATER MONITORING REPORT OCTOBER 2023 TABLE 2HiSTORICAL PODUCT THICKNESS AND GROUNDWATER ELEVATIONSSEMINOLE MART NO. 2691 SEMINOLE ROADBROADWAY, HARNETT COUNTY, NORTH CAROLINANCDEQ INCIDENT NO. 42025CLES PROJECT NO. 17-051 Well ID TOC (ft-rel)Date DTP (ft-btoc)Product Thickness (ft)DTW (ft-btoc)GW Elev (ft-rel)PRODUCT TYPE MW-1 93.72 3/27/17 36.00 1.90 37.90 57.405/1/17 36.65 2.30 38.95 56.685/25/17 36.25 2.85 39.10 56.995/26/17 36.75 1.00 37.75 56.806/1/17 36.53 0.62 37.15 57.097/10/17 36.24 2.00 38.24 57.148/1/17 36.38 1.04 37.42 57.17 10/31/17 36.60 1.15 37.75 56.93 11/29/17 36.60 2.15 38.75 56.76 12/5/17 36.60 2.02 38.62 56.7812/19/17 36.63 2.30 38.93 56.708/7/18 0.42 NCPUMP IN 8/20/18 0.41 NC8/24/18 35.78 0.06 35.84 57.939/6/18 0.01 NC9/27/18 0.00 NC10/10/18 0.00 NC10/19/18 0.00 NC10/29/18 NM 0.00 34.93 58.7911/6/18 NM 0.00 34.98 58.7412/2/18 NM 0.00 35.02 58.70 12/12/18 0.04 NC 12/21/18 NM 0.00 34.73 58.99 1/15/19 35.09 0.02 35.11 58.63 gas2/5/19 35.02 0.16 35.18 58.672/25/19 35.18 0.25 35.43 58.503/1/19 35.19 0.22 35.41 58.494/25/19 34.98 0.67 35.65 58.635/16/19 35.03 1.07 36.10 58.515/31/19 35.10 1.30 36.40 58.406/19/19 35.14 1.72 36.86 58.297/5/19 35.50 1.73 37.23 57.93 diesel/gas7/15/19 35.58 1.42 37.00 57.907/29/19 35.66 1.10 36.76 57.888/3/19 35.78 0.76 36.54 57.818/21/19 35.86 0.93 36.79 57.70 9/18/19 36.00 1.08 37.08 57.54 10/10/19 35.20 0.15 35.35 58.4911/20/19 NM 0.00 35.73 57.9912/23/19 36.07 0.20 36.27 57.6212/31/19 36.14 0.21 36.35 57.541/16/20 34.83 0.26 35.09 58.852/19/20 34.82 1.89 36.71 57.012/27/20 34.93 0.47 35.40 58.323/5/20 34.94 0.96 35.90 57.823/10/20 34.62 0.66 35.28 58.443/16/20 NM 0.00 31.75 61.973/23/20 34.56 0.04 34.60 59.124/2/20 35.19 0.04 35.23 58.494/10/20 35.21 0.06 35.27 58.45 4/20/20 35.62 0.03 35.65 58.07 4/30/20 35 72 0.00 35.77 57.95 5/15/20 37.95 0.03 37.98 55.746/5/20 34.84 0.35 35.19 58.537/10/20 34.50 0.50 35.00 58.728/19/20 34.95 0.06 35.01 58.719/21/20 33.83 0.03 33.86 59.8610/5/20 32.73 0.00 32.73 60.9910/14/20 34.80 0.01 34.81 58.9110/28/20 NM 0.00 35.25 58.4711/5/20 NM 0.00 35.41 58.3111/10/20 35.43 0.02 35.45 58.2711/17/20 35.53 0.02 35.55 58.1712/3/20 35.60 0.05 35.65 58.07 12/18/20 NM 0.00 30.43 63.29 1/15/21 35.15 0.03 35.18 58.54 2/1/21 35.31 0.02 35.33 58.392/25/21 35.47 0.01 35.48 58.243/5/21 35.33 0.03 35.36 58.363/11/21 34.49 0.03 34.52 59.203/15/21 34.51 0.02 34.53 59.194/7/21 35.02 0.06 35.08 58.644/12/21 35.21 0.03 35.24 58.484/19/21 35.38 0.01 35.39 58.335/6/21 35.44 0.03 35.47 58.256/3/21 36.06 0.02 36.08 57.646/9/21 35.65 0.08 35.73 57.997/7/21 NM 0.00 34.32 59.40 7/12/21 NM 0.00 35.50 58.22 7/22/21 NM 0.00 34.65 59.07 7/26/21 34.64 0.01 34.65 59.078/13/21 34.76 0.06 34.82 58.908/19/21 34.78 0.02 34.80 58.929/3/21 35.91 0.02 35.93 57.799/16/21 35.90 0.08 35.98 57.749/28/21 35.94 0.05 35.99 57.7310/5/21 34.99 0.04 35.03 58.6910/7/21 35.00 0.04 35.04 58.6811/12/21 35.44 0.10 35.54 58.1811/15/21 35.54 0.04 35.58 58.1411/18/21 35.97 0.04 36.01 57.7111/24/21 36.19 0.12 36.31 57.4112/17/21 36.26 0.22 36.48 57.24 12/28/21 36.32 0.32 36.64 57.08 1/5/221/11/22 36.47 0.28 36.75 56.971/28/22 36.43 0.39 36.82 56.902/3/22 36.48 0.34 36.82 56.902/17/22 36.45 0.33 36.78 56.943/15/22 36.52 0.65 37.17 56.553/18/22 0.00 93.724/12/22 35.67 1.65 37.32 56.404/25/22 35.24 1.99 37.23 56.495/12/22 35.88 1.48 37.36 56.365/27/22 36.09 1.32 37.41 56.316/10/22 36.18 0.94 37.12 56.607/21/22 35.18 2.48 37.66 56.06 8/26/22 35.21 2.70 37.91 55.81 9/9/22 35.99 2.48 38.47 55.25 9/23/22 36.38 2.54 38.92 54.8010/5/22 36.32 2.77 39.09 54.633/8/23 35.10 3.62 38.72 55.007/18/23 35.71 2.77 38.48 55.249/20/23 35.65 1.65 37.30 56.4210/5/23 35.71 0.03 35.74 57.98 SEMINOLE MART NO 2 CLES PROJECT 17-051A GROUNDWATER MONITORING REPORT OCTOBER 2023 MW-2 94.36 3/27/17 NM 0.00 41.73 52.635/1/17 42.13 0.10 42.23 52.215/25/17 42.3 0.10 42.4 52.045/26/17 42.50 0.08 42.58 51.856/1/27 42.43 0.05 42.48 51.927/10/17 42.60 1.15 43.75 51.578/1/17 42.67 1.76 44.43 51.3910/31/17 44.00 0.45 44.45 50.2811/29/17 44.13 0.35 44.48 50.1712/5/17 44.23 0.27 44.50 50.0812/19/17 44.42 0.06 44.48 49.93 8/7/18 0.20 NC 8/20/18 0.25 NC8/24/18 43.43 0.30 43.73 50.639/6/18 0.55 NC9/27/18 0.20 NC10/10/18 0.16 NC10/29/18 40.60 1.22 41.82 53.56 gas11/6/18 44.23 0.27 44.50 50.0812/2/18 39.96 1.57 41.53 54.1412/12/18 0.83 NC12/21/18 38.67 2.00 40.67 55.351/15/19 37.99 3.01 41.00 55.86 gas2/5/19 37.91 1.47 39.38 56.202/25/19 37.48 1.91 39.39 56.56 3/1/19 37.45 1.86 39.31 56.60 4/10/19 37.02 1.11 38.13 57.15 4/25/19 37.00 0.61 37.61 57.265/16/19 37.82 0.63 38.45 56.435/31/19 37.27 2.14 39.41 56.736/4/19 37.28 0.92 38.20 56.936/19/19 37.96 1.06 39.02 56.227/5/19 38.64 0.30 38.94 55.67 gas/diesel7/15/19 38.86 1.02 39.88 55.337/29/19 39.01 1.85 40.86 55.048/3/19 39.42 0.36 39.78 54.888/21/19 39.77 1.45 41.22 54.359/18/19 40.43 1.89 42.32 53.6110/10/18 41.19 0.52 41.71 53.08 11/20/19 42.21 0.12 42.33 52.13 12/23/19 42.89 0.21 43.10 51.43 12/31/19 42.54 0.24 42.78 51.781/16/20 43.36 0.56 43.92 50.443/16/20 27.87 0.02 27.89 66.47 MAKE UP FROM 173/23/20 42.72 0.01 42.73 51.634/2/20 NM 0.00 42.65 51.714/10/20 42.62 0.02 42.64 51.724/20/20 42.21 0.10 42.31 52.054/30/20 42.20 0.06 42.26 52.105/15/20 42.10 0.21 42.31 52.056/5/20 42.01 0.27 42.28 52.087/10/20 41.28 1.47 42.75 51.618/19/20 40.58 0.33 40.91 53.459/21/20 40.04 2.06 42.10 52.26 10/5/20 39.73 0.02 39.75 54.61 10/14/20 NM 0.00 40.96 53.4010/28/20 NM 0.00 40.16 54.2011/5/20 NM 0.00 40.68 53.6811/10/20 40.74 0.06 40.80 53.5611/17/20 NM 0.00 40.68 53.6812/3/20 NM 0.00 40.53 53.8312/18/20 NM 0.00 32.27 62.091/15/21 39.75 0.19 39.94 54.422/1/21 39.41 0.22 39.63 54.732/25/21 39.70 0.02 39.72 54.643/5/21 NM 0.00 39.61 54.753/11/21 NM 0.00 37.93 56.433/15/21 NM 0.00 37.94 56.42 4/7/21 37.14 0.15 37.29 57.07 4/12/21 NM 0.00 37.33 57.03 4/19/21 37.50 0.01 37.51 56.855/6/21 38.01 0.33 38.34 56.026/3/21 38.41 0.25 38.66 55.706/9/21 38.49 0.21 38.70 55.667/7/21 39.66 0.14 39.80 54.567/12/21 39.98 0.04 40.02 54.347/22/21 40.04 0.05 40.09 54.277/26/21 39.98 0.05 40.03 54.338/13/21 40.19 0.07 40.26 54.108/19/21 40.26 0.06 40.32 54.049/3/21 40.56 0.08 40.64 53.729/16/21 40.71 0.18 40.89 53.47 9/28/21 40.89 0.21 41.10 53.26 10/5/21 40.05 0.63 40.68 53.68 10/7/21 40.38 0.31 40.69 53.6711/12/21 40.60 0.59 41.19 53.1711/15/21 41.15 0.08 41.23 53.1311/18/21 41.62 0.04 41.66 52.7011/24/21 42.12 0.10 42.22 52.1412/17/21 42.52 0.08 42.60 51.7612/28/21 42.74 0.14 42.88 51.481/11/22 43.04 0.12 43.16 51.201/28/22 43.14 0.51 43.65 50.712/3/22 43.26 0.42 43.68 50.682/17/22 43.34 0.55 43.89 50.473/15/22 43.69 0.52 44.21 50.15 3/18/22 43.74 0.56 44.30 50.06 4/12/22 43.86 -0.58 43.28 51.08 4/25/22 43.82 0.38 44.20 50.165/12/22 43.88 0.44 44.32 50.045/27/22 43.91 0.45 44.36 50.006/10/22 43.99 0.33 44.32 50.047/21/22 44.15 0.11 44.26 50.108/26/22 44.16 0.06 44.22 50.149/9/22 44.14 0.06 44.20 50.169/23/22 NM 0.00 44.17 50.1910/5/22 NM 0.00 44.18 50.183/8/23 NM 0.00 44.54 49.827/18/23 43.72 0.63 44.35 50.019/20/23 43.56 0.24 43.80 50.5610/5/23 43.60 0.70 44.30 50.06 SEMINOLE MART NO 2 CLES PROJECT 17-051A GROUNDWATER MONITORING REPORT OCTOBER 2023 MW-3 93.58 3/27/17 40.55 2.00 42.55 52.695/1/17 40.95 2.50 43.45 52.215/25/17 41.20 2.00 43.20 52.045/26/17 41.53 0.62 42.15 51.956/1/27 41.40 1.30 42.70 51.967/10/17 41.50 3.00 44.50 51.588/1/17 41.76 2.54 44.30 51.3910/31/17 43.22 0.80 44.02 50.2311/29/17 43.42 1.24 44.66 49.9512/5/17 43.42 1.24 44.66 49.9512/19/17 43.41 1.25 44.66 49.96 8/7/18 0.01 NC 8/20/18 0.00 NC8/24/18 43.38 0.01 43.39 50.209/6/18 0.00 NC9/27/18 0.00 NC10/10/18 0.02 NC10/19/18 0.07 NC10/29/18 41.00 0.23 41.23 52.54 gas11/6/18 40.68 0.14 40.82 52.8812/2/18 39.70 0.38 40.08 53.8212/12/18 0.00 NC12/21/18 38.35 0.34 38.69 55.171/15/19 37.73 0.43 38.16 55.78 gas/diesel2/5/19 37.02 0.37 37.39 56.50 2/25/19 36.98 0.40 37.38 56.53 3/1/19 36.94 0.36 37.30 56.58 4/25/19 36.19 0.67 36.86 57.285/16/19 36.38 0.82 37.20 57.065/31/19 36.56 0.93 37.49 56.866/4/19 36.58 0.34 36.92 56.946/19/19 37.00 1.17 38.17 56.387/5/19 37.59 1.55 39.14 55.73 gas/diesel7/15/19 38.61 0.47 39.08 54.897/29/19 38.84 0.16 39.00 54.718/3/19 38.56 0.33 38.89 54.968/21/19 39.03 0.59 39.62 54.459/18/19 39.79 0.74 40.53 53.6710/10/19 40.33 0.50 40.83 53.17 11/20/19 NM 0.00 41.35 52.23 12/23/19 41.19 0.35 41.54 52.33 12/31/19 NM NC NM NC1/16/20 NM 0.00 42.26 51.322/19/20 42.01 0.21 42.22 51.362/27/20 42.30 0.01 42.31 51.273/5/20 42.31 0.01 42.32 51.263/10/20 NM 0.00 41.59 51.993/16/20 NM 0.00 41.72 51.863/23/20 41.45 0.01 41.46 52.124/2/20 NM 0.00 41.39 52.194/10/20 41.39 0.01 41.38 52.204/20/20 NM 0.00 41.37 52.214/30/20 41.41 0.02 41.43 52.155/15/20 41.56 0.05 41.61 51.97 6/5/20 41.31 0.03 41.34 52.24 7/10/20 40.72 0.05 40.77 52.818/19/20 40.23 0.08 40.31 53.279/21/20 40.03 0.12 40.15 53.4310/5/20 40.00 0.10 40.10 53.4810/14/20 40.05 0.04 40.09 53.4910/28/20 40.09 0.04 40.13 53.4511/5/20 40.12 0.04 40.16 53.4211/10/20 40.14 0.06 40.20 53.3811/17/20 40.14 0.07 40.21 53.3712/18/20 40.3 0.08 40.38 54.781/15/21 39.45 0.09 39.54 55.462/1/21 39.02 0.04 39.06 55.702/25/21 38.44 0.08 38.52 55.17 3/5/21 NM MC NM NC 3/11/21 37.75 0.04 37.79 56.93 3/15/21 37.79 0.01 37.8 56.034/7/21 37.09 0.05 37.14 56.614/12/21 37.27 0.03 37.3 56.454/19/21 37.44 0.05 37.49 56.235/6/21 37.62 0.11 37.73 55.876/3/21 38.21 0.10 38.31 55.276/9/21 38.28 0.07 38.35 55.237/7/21 38.95 0.02 38.97 54.617/12/21 39.09 0.01 39.1 54.487/22/21 39.18 0.01 39.19 54.397/26/21 39.11 0.01 39.12 54.468/13/21 39.31 0.02 39.33 54.25 8/19/21 39.38 0.01 39.39 54.19 9/3/21 39.66 0.01 39.67 53.93 9/16/21 39.84 0.01 39.85 53.739/28/21 40.01 0.02 40.03 53.5510/5/21 40.21 0.01 40.22 53.3610/7/21 NM 0.00 40.23 53.3511/12/21 NM 0.00 40.73 52.8511/15/21 NM 0.00 40.77 52.8111/18/21 NM 0.00 41.2 52.3911/24/21 NM 0.00 41.32 52.2612/17/21 NM 0.00 41.71 51.9112/28/21 NM 0.00 41.93 51.671/11/22 NM 0.00 42.31 51.281/28/22 NM 0.00 42.38 51.22 2/3/22 NM 0.00 42.53 51.07 2/17/22 NM 0.00 42.64 50.96 3/15/22 NM 0.00 43.05 50.553/18/22 NM NC NM NC4/12/22 43.23 0.01 43.24 50.354/25/22 NM 0.00 43.18 50.405/12/22 43.25 0.01 43.26 50.325/27/22 43.27 0.02 43.29 50.296/10/22 43.38 0.03 43.41 50.177/21/22 43.52 0.29 43.81 49.778/26/22 43.61 0.37 43.98 49.609/9/22 43.8 0.41 44.21 49.379/23/22 44.01 0.73 44.74 48.843/8/23 44.22 0.66 44.88 48.7010/5/22 44.12 0.77 44.89 48.69 7/18/23 42.98 1.22 44.2 49.38 9/20/23 42.85 1.35 44.2 49.3810/5/23 43 1.20 44.2 49.38 SEMINOLE MART NO 2 CLES PROJECT 17-051A GROUNDWATER MONITORING REPORT OCTOBER 2023 MW-4 93.52 3/27/17 40.55 1.90 42.45 52.655/1/17 41.04 1.71 42.75 52.195/25/17 41.30 1.42 42.72 51.985/26/17 41.62 0.13 41.75 51.886/1/27 41.44 1.18 42.62 51.887/10/17 41.73 1.37 43.10 51.568/1/17 42.10 0.30 42.40 51.3710/31/17 43.30 0.20 43.50 50.1911/29/17 43.73 0.20 43.93 49.7612/5/17 43.81 0.17 43.98 49.6812/19/17 44.04 0.03 44.07 49.47 8/7/18 0.02 8/20/18 0.008/24/18 0.009/6/18 0.00 NC9/27/18 0.00 NC10/10/18 0.00 NC10/19/18 0.04 NC10/29/18 41.03 0.02 41.05 52.49 diesel11/6/18 NM 0.00 40.74 52.7812/2/18 NM 0.00 39.77 53.7512/12/18 0.01 NC diesel12/21/18 0.00 NC1/15/19 NM 0.00 37.78 55.742/5/19 NM 0.00 2/26/19 37.01 0.01 37.02 56.51 4/25/19 NM 0.00 36.25 57.27 6/19/19 37.14 0.05 37.19 56.377/5/19 37.78 0.03 37.81 55.73 diesel7/15/19 38.36 0.01 38.37 55.167/29/19 38.40 0.02 38.42 55.128/3/19 38.59 0.02 38.61 54.938/21/19 39.09 0.03 39.12 54.429/18/19 39.86 0.03 39.89 53.6511/20/19 41.40 0.02 41.42 52.1212/23/19 42.08 0.01 42.09 51.4412/31/19 0.001/16/20 42.24 0.01 42.25 51.273/10/20 NM 0.00 41.57 51.95 3/16/20 NM 0.00 41.71 51.81 3/23/20 41.41 0.01 41.42 52.10 4/2/20 NM 0.00 41.43 52.094/10/20 NM 0.00 41.41 52.114/20/20 NM 0.00 41.45 52.074/30/20 NM 0.00 41.44 52.085/15/20 NM 0.00 41.56 51.966/5/20 NM 41.29 41.29 52.237/10/20 NM 0.00 40.72 52.808/18/20 NM 0.00 40.23 53.299/21/20 NM 0.00 40.04 53.4810/5/20 40.00 0.01 40.01 53.5210/14/20 NM 0.00 40.04 53.4810/28/20 NM 0.00 40.08 53.4411/5/20 NM 0.00 40.10 53.42 11/10/20 NM 0.00 40.12 53.40 11/17/20 NM 0.00 40.15 53.3712/18/20 40.30 0.01 40.31 53.211/15/21 NM 0.00 39.44 54.082/1/21 NM 0.00 38.98 54.542/25/21 38.41 0.02 38.43 55.093/5/21 NM 0.00 38.02 55.503/11/21 NM 0.00 37.73 55.793/15/21 NM 0.00 38.40 55.124/7/21 NM 0.00 37.05 56.474/12/21 NM 0.00 37.79 55.734/19/21 NM 0.00 37.97 55.555/6/21 NM 0.00 37.60 55.926/3/21 38.16 0.03 38.19 55.33 6/9/21 38.31 0.02 38.33 55.19 7/7/21 NM 0.00 39.94 53.58 7/12/21 NM 0.00 39.06 54.467/22/21 39.12 0.01 39.13 54.397/26/21 39.08 0.01 39.09 54.438/13/21 39.29 0.01 39.30 54.228/19/21 39.34 0.01 39.35 54.179/3/21 39.64 0.01 39.65 53.879/16/21 NM 0.00 39.85 53.679/28/21 39.99 0.01 40.00 53.5210/5/21 NM 0.00 40.20 53.3210/7/21 0.00 93.5211/12/21 0.00 93.5211/15/21 0.00 93.52 11/18/21 0.00 93.52 11/24/21 0.00 41.32 52.20 12/17/21 0.00 41.70 51.8212/28/21 0.00 41.93 51.591/11/22 42.26 0.01 42.27 51.251/28/22 NM 0.00 42.42 51.102/17/22 42.82 0.01 42.83 50.693/15/22 NM 0.00 43.08 50.443/18/22 NM NC NM NC4/12/22 NM 0.00 43.25 50.274/25/22 NM 0.00 43.21 50.315/12/22 NM 0.00 43.26 50.265/27/22 NM 0.00 43.29 50.236/10/22 NM 0.00 43.38 50.14 7/21/22 NM 0.00 43.59 49.93 8/26/22 NM 0.00 44.20 49.32 9/9/22 NM 0.00 44.41 49.119/23/22 NM 0.00 44.20 49.3210/5/22 NM 0.00 44.24 49.283/8/23 NM 0.00 44.33 49.197/18/23 NM 0.00 43.18 50.349/20/23 NM 0.00 43.02 50.5010/5/23 NM 0.00 43.13 50.39 SEMINOLE MART NO 2 CLES PROJECT 17-051A GROUNDWATER MONITORING REPORT OCTOBER 2023 MW-5 93.4 5/25/17 NM 0.00 41.34 52.065/26/17 NM NC NM NC6/1/27 NM 0.00 41.45 51.957/10/17 NM 0.00 41.80 51.608/1/17 NM 0.00 42.00 51.4010/31/17 NM 0.00 43.18 50.2211/29/17 NM 0.00 43.60 49.8012/5/17 NM 0.00 43.68 49.7212/19/17 NM 0.00 43.90 49.508/7/18 0.00 NC8/20/18 0.00 NC 8/24/18 NM 0.00 43.24 50.16 9/6/18 0.00 NC9/27/18 0.00 NC10/10/18 0.00 NC10/19/18 NM 0.00 NC10/29/18 NM 0.00 43.68 49.7211/6/18 0.00 NC12/2/18 NM 0.00 39.53 53.8712/12/18 0.00 NC12/21/18 0.00 NC1/15/19 NM 0.00 37.57 55.832/5/19 NM2/25/19 NM 0.00 36.80 56.604/25/19 NM 0.00 36.04 57.36 6/19/19 NM 0.00 36.96 56.44 7/5/19 NM 0.00 37.61 55.79 11/20/19 NM 0.00 41.27 52.1312/23/19 NM 0.00 93.4012/31/19 NM 0.00 93.401/16/20 NM 0.00 42.09 51.313/10/20 NM 0.00 41.41 51.993/16/20 NM 0.00 41.52 51.886/5/20 NM 0.00 41.14 52.2610/5/20 NM 0.00 39.84 53.5610/14/20 NM 0.00 39.87 53.537/12/21 NM 0.00 38.89 54.511/28/22 NM 0.00 42.23 51.177/21/22 NM 0.00 43.42 49.98 3/8/23 NM 0.00 43.73 49.67 0.00 93.40 0.00 93.4010/5/23 NM 0.00 42.96 50.44 MW-6 92.84 5/25/17 NM 0.00 40.90 51.945/26/17 NM NC NM NC6/1/27 NM 0.00 41.01 51.837/10/17 NM 0.00 41.35 51.49 8/1/17 NM 0.00 41.53 51.31 10/31/17 NM 0.00 42.77 50.07 11/29/17 NM 0.00 43.18 49.6612/5/17 NM 0.00 43.25 49.5912/19/17 NM 0.00 43.48 49.368/7/18 0.00 NC8/20/18 0.00 NC8/24/18 NM 0.00 42.84 50.009/6/18 0.00 NC9/27/18 0.00 NC10/10/18 0.00 NC10/19/18 NM 0.00 NC10/29/18 NM 0.00 40.46 52.3811/6/18 0.00 NC 12/2/118 NM 0.00 39.16 53.68 12/12/18 0.00 NC 12/21/18 0.00 NC1/15/19 NM 0.00 37.18 55.662/5/19 NM2/26/19 NM 0.00 36.39 56.454/25/19 NM 0.00 35.63 57.216/19/19 NM 0.00 36.52 56.327/5/19 NM 0.00 37.14 55.7011/20/19 NM 0.00 40.82 52.0212/23/19 0.00 92.8412/31/19 0.00 92.841/16/20 NM 0.00 41.66 51.183/16/20 NM 0.00 41.10 51.746/5/20 NM 0.00 40.72 52.12 10/5/20 NM 0.00 39.39 53.45 10/14/20 NM 0.00 39.41 53.437/12/21 NM 0.00 38.43 54.411/28/22 NM 0.00 41.76 51.087/21/22 NM 0.00 42.98 49.863/8/23 NM 0.00 43.73 49.110.00 92.840.00 92.840.00 92.840.00 92.8410/5/23 NM 0.00 42.54 50.30 MW-7 92.92 5/25/17 NM 0.00 40.9 52.025/26/17 NM NC NM NC6/1/27 NM 0.00 41.03 51.897/10/17 NM 0.00 41.37 51.558/1/17 NM 0.00 41.55 51.3710/31/17 NM 0.00 42.77 50.1511/29/17 NM 0.00 43.18 49.7412/5/17 NM 0.00 43.25 49.6712/19/17 NM 0.00 43.49 49.438/7/18 0.00 NC8/20/18 0.00 NC 8/24/18 NM 0.00 42.84 50.08 9/6/18 0.00 NC9/27/18 0.00 NC10/10/18 0.00 NC10/19/18 NM 0.00 NC10/29/18 NM 0.00 40.45 52.4711/6/18 NM NC NM NC12/2/18 NM 0.00 39.15 53.7712/12/18 0.00 NC12/21/18 0.00 NC1/15/19 NM 0.00 37.15 55.772/5/19 NM2/26/19 NM 0.00 36.38 56.544/25/19 NM 0.00 35.63 57.29 6/19/19 NM 0.00 36.52 56.40 7/5/19 NM 0.00 37.14 55.78 11/20/19 NM 0.00 40.82 52.1012/23/19 0.00 92.9212/31/19 0.00 92.921/16/20 NM 0.00 41.66 51.263/16/20 NM 0.00 41.10 51.826/5/20 NM 0.00 40.71 52.2110/5/20 NM 0.00 34.00 58.9210/14/20 NM 0.00 39.43 53.497/12/21 NM 0.00 38.43 54.491/28/22 NM 0.00 41.79 51.137/21/22 NM 0.00 42.98 49.943/8/23 NM 0.00 43.73 49.19 0.00 92.92 0.00 92.92 0.00 92.920.00 92.920.00 92.9210/5/23 NM 0.00 42.54 50.38 SEMINOLE MART NO 2 CLES PROJECT 17-051A GROUNDWATER MONITORING REPORT OCTOBER 2023 MW-8 93.38 10/31/17 43.08 1.95 45.03 49.9711/29/17 43.45 2.48 45.93 49.5112/5/17 43.53 2.47 46.00 49.4412/19/17 44.02 0.48 44.50 49.288/7/18 0.00 NC8/20/18 0.02 NC8/24/18 43.42 0.07 43.49 49.959/6/18 0.01 NC9/27/18 0.00 NC10/10/18 0.00 NC10/19/18 0.00 NC 10/29/18 40.98 0.64 41.62 52.29 diesel 11/6/18 40.59 0.63 41.22 52.6812/2/18 39.7 0.34 40.04 53.6212/12/18 0.01 NC12/21/18 NM 0.00 38.45 54.931/15/19 37.78 0.23 38.01 55.56 diesel2/5/19 37.06 0.21 37.27 56.282/25/19 37.01 0.43 37.44 56.303/1/19 36.98 0.43 37.41 56.334/10/19 36.34 0.47 36.81 56.964/25/19 36.23 0.48 36.71 57.075/16/19 36.42 0.58 37.00 56.865/31/19 36.59 0.62 37.21 56.696/4/19 36.6 0.16 36.76 56.75 6/19/19 37.13 0.39 37.52 56.18 7/5/19 37.72 0.67 38.39 55.55 diesel 7/15/19 38.23 0.15 38.38 55.127/29/19 38.37 0.40 38.77 54.948/3/19 38.54 0.35 38.89 54.788/21/19 39.05 0.38 39.43 54.279/18/19 39.8 0.48 40.28 53.5011/20/19 41.42 0.02 41.44 51.9612/23/19 NM 0.00 42.08 51.3012/31/19 0.00 93.381/16/20 42.24 0.03 42.27 51.112/19/20 42.17 0.11 42.28 51.102/27/20 42.29 0.04 42.33 51.053/5/20 42.30 0.02 42.32 51.06 3/10/20 41.56 0.03 41.59 51.79 3/16/20 41.79 0.14 41.93 51.45 3/23/20 41.40 0.10 41.50 51.884/2/20 41.43 0.11 41.54 51.844/10/20 41.41 0.06 41.47 51.914/20/20 41.45 0.01 41.46 51.924/30/20 41.44 0.16 41.60 51.785/15/20 41.41 0.17 41.58 51.806/5/20 41.26 0.32 41.58 51.807/10/20 40.71 0.09 40.79 52.598/19/20 40.2 0.20 40.40 52.989/21/20 40 0.30 40.30 53.0810/5/20 39.9 0.31 40.21 53.1710/14/20 40.01 0.19 40.20 53.1810/28/20 40.06 0.14 40.20 53.18 11/5/20 40.09 0.14 40.23 53.27 11/10/20 40.1 0.15 40.25 53.1311/17/20 40.13 0.10 40.23 53.1512/18/20 40.35 0.17 40.52 52.861/15/21 39.43 0.07 39.50 53.882/1/21 38.97 0.02 38.99 54.392/25/21 38.44 0.03 38.47 54.913/5/21 38.11 0.01 38.12 55.263/11/21 NM 0.00 37.78 55.603/15/21 NM 0.00 37.79 55.594/7/21 NM 0.00 37.08 56.304/12/21 NM 0.00 37.27 56.114/19/21 NM 0.00 37.45 55.935/6/21 37.63 0.01 37.64 55.74 6/3/21 38.19 0.01 38.20 55.18 6/9/21 38.31 0.02 38.33 55.05 7/7/21 39.04 0.08 39.12 54.267/12/21 NNM 0.00 39.09 54.297/22/21 39.17 0.01 39.18 54.207/26/21 39.11 0.01 39.12 54.268/13/21 39.3 0.01 39.31 54.078/19/21 39.38 0.01 39.39 53.999/3/21 39.66 0.01 39.67 53.719/16/21 NM 0.00 39.84 53.549/28/21 40 0.01 40.01 53.3710/5/21 NM 0.00 40.16 53.2210/7/21 NM 0.00 41.17 52.2111/12/21 NM 0.00 41.59 51.79 11/15/21 NM 0.00 41.63 51.75 11/18/21 NM 0.00 42.21 51.18 11/24/21 NM 0.00 41.29 52.0912/17/21 NM 0.00 41.70 51.6812/28/21 NM 0.00 41.92 51.461/11/22 NM 0.00 42.50 50.881/28/22 NM 0.00 42.40 50.982/3/22 NM 0.00 42.52 50.862/17/22 42.63 0.01 42.64 50.743/15/22 NM 0.00 43.07 50.313/18/22 NM NC NM NC4/12/22 43.25 0.01 43.26 50.124/25/22 NM 0.00 43.22 50.165/12/22 43.26 0.02 43.28 50.10 5/27/22 43.28 0.02 43.30 50.08 6/10/22 NM 0.00 43.38 50.00 7/21/22 NM 0.00 43.57 49.818/26/22 NM 0.00 44.18 49.209/9/22 NM 0.00 44.39 48.999/23/22 NM 0.00 44.18 49.2010/5/22 NM 0.00 44.22 49.163/8/23 NM 0.00 44.32 49.069/20/23 42.97 0.03 43.00 50.3810/5/23 43.08 0.03 43.11 50.27 SEMINOLE MART NO 2 CLES PROJECT 17-051A GROUNDWATER MONITORING REPORT OCTOBER 2023 MW-9 93.63 10/31/17 NM 0.00 43.42 50.2111/29/17 NM 0.00 43.82 49.8112/5/17 NM 0.00 43.90 49.7312/19/17 NM 0.00 44.10 49.538/7/18 0.21 NCPUMP IN WELL 8/20/18 0.21 NC8/24/18 0.21 NC9/6/18 0.40 NC9/27/18 0.44 NC10/10/18 0.39 NCPUMP IN WELL 10/19/18 0.35 NC 10/29/18 41.09 0.34 41.43 52.48 diesel 11/6/18 40.72 0.07 40.79 52.9012/2/18 39.75 0.18 39.93 53.8512/12/18 0.42 NC12/21/18 38.48 0.06 38.54 55.141/15/19 37.79 0.39 38.18 55.77 diesel2/5/19 37.10 0.23 37.33 56.492/25/19 37.08 0.20 37.28 56.523/1/19 37.05 0.19 37.24 56.554/10/19 36.38 0.41 36.79 57.184/25/19 36.28 0.50 36.78 57.275/16/19 36.49 0.61 37.10 57.045/31/19 36.64 0.68 37.32 56.886/4/19 36.66 0.12 36.78 56.95 6/19/19 37.16 0.68 37.84 56.36 7/5/19 37.80 0.77 38.57 55.70 diesel 7/15/19 38.21 0.22 38.43 55.387/29/19 38.50 0.15 38.65 55.108/3/19 38.69 0.09 38.78 54.928/21/19 39.20 0.15 39.35 54.409/18/19 39.97 0.18 40.15 53.6311/20/19 41.54 0.04 41.58 52.0812/23/19 42.09 0.01 42.10 51.5412/31/19 0.00 93.631/16/20 42.34 0.02 42.36 51.272/19/20 42.18 0.10 42.28 51.352/27/20 42.31 0.03 42.34 51.293/5/20 42.30 0.02 42.32 51.31 3/10/20 41.63 0.04 41.67 51.96 3/16/20 41.76 0.02 41.78 51.85 3/23/20 41.48 0.32 41.80 51.834/2/20 41.51 0.18 41.69 51.944/10/20 41.48 0.05 41.53 52.104/20/20 41.53 0.17 41.70 51.934/30/20 41.47 0.11 41.58 52.055/15/20 41.52 0.16 41.68 51.956/5/20 41.36 0.12 41.48 52.157/10/20 40.80 0.10 40.90 52.738/19/20 40.23 0.48 40.71 52.929/21/20 40.09 0.40 40.49 53.1410/5/20 40.07 0.53 40.60 53.0310/14/20 40.11 0.28 40.39 53.4710/28/20 40.14 0.28 40.42 53.21 11/5/20 40.17 0.26 40.43 53.20 11/10/20 40.19 0.24 40.43 53.2011/17/20 40.22 0.17 40.39 53.2412/18/20 40.35 0.21 40.56 53.071/15/21 39.5 0.22 39.72 53.912/1/21 39.03 0.13 39.16 54.472/25/21 38.49 0.10 38.59 55.043/5/21 38.11 0.08 38.19 55.443/11/21 37.8 0.10 37.90 55.733/15/21 37.88 0.02 37.90 55.734/7/21 37.14 0.01 37.15 56.484/12/21 37.33 0.08 37.41 56.224/19/21 37.43 0.08 37.51 56.125/6/21 37.69 0.13 37.82 55.81 6/3/21 38.26 0.13 38.39 55.24 6/9/21 38.4 0.26 38.66 54.97 7/7/21 39.03 0.09 39.12 54.517/12/21 39.19 0.02 39.21 54.427/22/21 39.24 0.04 39.28 54.357/26/21 3919 0.01 39.20 54.438/13/21 39.39 0.04 39.43 54.208/19/21 39.46 0.03 39.49 54.149/3/21 39.77 0.02 39.79 53.849/16/21 39.94 0.01 39.95 53.689/28/21 40.13 0.01 40.14 53.4910/5/21 40.3 0.01 40.31 53.3210/7/21 41.32 0.00 41.32 52.3111/12/21 41.68 0.14 41.82 51.81 11/15/21 41.8 0.06 41.86 51.77 11/18/21 42.19 0.10 42.29 51.34 11/24/21 41.35 0.06 41.41 52.2212/17/21 41.71 0.11 41.82 51.8112/28/21 41.97 0.07 42.04 51.591/11/22 42.42 0.16 42.58 51.051/28/22 NM 0.00 42.49 51.142/3/22 NM 0.00 42.54 51.092/17/22 43.73 0.01 43.74 49.893/15/22 NM 0.00 43.15 50.483/18/22 NM NC NM NC4/12/22 NM 0.00 43.33 50.304/25/22 NM 0.00 43.29 50.345/12/22 NM 0.00 43.30 50.33 5/27/22 43.36 0.01 43.37 50.26 6/10/22 NM 0.00 43.36 50.27 7/21/22 NM 0.00 43.65 49.988/26/22 NM 0.00 43.89 49.749/9/22 NM 0.00 44.10 49.539/23/22 NM 0.00 44.22 49.4110/5/22 NM 0.00 44.29 49.343/8/23 NM 0.00 44.42 49.210.00 93.630.00 93.639/20/23 NM 0.00 43.10 50.5310/5/23 NM 0.00 43.22 50.41 SEMINOLE MART NO 2 CLES PROJECT 17-051A GROUNDWATER MONITORING REPORT OCTOBER 2023 MW-10 94.48 10/31/17 NM 0.00 44.22 50.2611/29/17 NM 0.00 44.61 49.8712/5/17 NM 0.00 44.68 49.8012/19/17 NM 0.00 44.88 49.608/7/18 0.42 NC dieselPUMP IN WELL 8/20/18 1.20 NC8/24/18 44.09 1.21 45.30 50.199/6/18 0.95 NC9/27/18 1.31 NC10/10/18 0.43 NCPUMP IN WELL 10/19/18 0.50 NC 10/29/18 42.03 0.07 42.10 52.44 diesel 11/6/18 41.55 0.48 42.03 52.8512/2/18 40.35 2.10 42.45 53.7812/12/18 0.42 NC12/21/18 39.07 0.62 39.69 55.311/15/19 38.42 1.78 40.20 55.76 diesel2/5/19 37.97 0.67 38.64 56.402/26/19 NM 0.00 38.08 56.40 PUMP ON3/1/19 38.04 0.24 38.28 56.404/10/19 37.32 0.70 38.02 57.044/25/19 37.15 1.09 38.24 57.15 gas5/16/19 37.49 0.43 37.92 56.925/31/19 37.64 0.70 38.34 56.726/4/19 37.65 0.11 37.76 56.81 6/19/19 38.14 0.59 38.73 56.24 7/5/19 38.51 2.18 40.69 55.60 gas 7/15/19 38.6 3.11 41.71 55.367/29/19 38.73 4.54 43.27 54.99 gas light oer black8/3/19 39.39 1.53 40.92 54.838/21/19 39.68 3.17 42.85 54.279/18/19 40.49 2.89 43.38 53.5010/10/19 41.08 2.14 43.22 53.0411/20/19 42.46 0.08 42.54 52.0112/23/19 42.98 0.43 43.41 51.4312/31/19 43.01 0.54 43.55 51.381/16/20 43.07 0.63 43.70 50.783/16/20 NM 0.00 41.11 53.373/23/20 42.17 0.46 42.63 51.85 4/2/20 41.4 0.50 41.90 52.58 4/10/20 42 0.48 42.48 52.00 4/20/20 41.93 0.44 42.37 52.114/30/20 42.18 0.33 42.51 51.975/15/20 42.21 0.84 43.05 51.436/5/20 42.08 1.06 43.14 51.347/10/20 41.47 1.33 42.80 51.688/19/20 40.89 1.91 42.80 51.689/21/20 40.93 1.25 42.18 52.3010/5/20 40.98 0.93 41.91 52.5710/14/20 40.95 0.84 41.79 52.6910/28/20 40.94 0.96 41.90 53.3811/5/20 40.98 0.89 41.87 52.6111/10/20 40.99 1.09 42.08 52.4011/17/20 41 1.08 42.08 52.40 12/3/20 40.96 1.04 42.00 52.48 12/18/20 41.08 0.95 42.03 52.451/15/21 40.26 1.20 41.46 53.022/1/21 39.78 1.13 40.91 53.572/25/21 39.33 0.72 40.05 54.433/5/21 39.52 0.11 39.63 54.853/11/21 38.55 1.16 39.71 54.773/15/21 38.68 1.04 39.72 54.764/7/21 37.8 1.86 39.66 54.824/12/21 37.94 1.47 39.41 55.074/19/21 38.02 0.70 38.72 55.765/6/21 38.43 1.68 40.11 54.375/12/21 38.83 0.68 39.51 54.976/3/21 39.88 0.14 40.02 54.46 6/9/21 39.27 0.44 39.71 54.77 7/7/21 39.93 0.20 40.13 54.35 7/12/21 40.12 0.19 40.31 54.177/22/21 40.17 0.20 40.37 54.117/26/21 40.15 0.21 40.36 54.128/13/21 40.29 0.37 40.66 53.828/19/21 40.36 0.42 40.78 53.709/3/21 40.67 0.46 41.13 53.359/16/21 40.81 0.31 41.12 53.369/28/21 41.02 0.28 41.30 53.1810/5/21 41.19 0.40 41.59 52.8910/7/21 41.42 0.18 41.60 52.8811/12/21 41.78 0.32 42.10 52.3811/15/21 42.1 0.04 42.14 52.34 11/18/21 42.54 0.03 42.57 51.91 11/24/21 42.29 0.05 42.34 52.14 12/17/21 42.7 0.02 42.72 51.7612/28/21 42.91 0.02 42.93 51.551/11/22 43.28 0.05 43.33 51.151/28/22 43.28 0.01 43.29 51.192/3/22 43.45 0.03 43.48 51.002/17/22 43.54 0.01 43.55 50.933/15/22 43.95 0.03 43.98 50.503/18/22 43.98 0.01 43.99 50.494/12/22 44.13 0.07 44.20 50.284/25/22 44.1 0.05 44.15 50.335/12/22 44.14 0.06 44.20 50.285/27/22 44.15 0.10 44.25 50.23 6/10/22 44.24 0.12 44.36 50.12 7/21/22 44.44 0.15 44.59 49.89 8/26/22 44.54 0.16 44.70 49.789/9/22 44.64 0.15 44.79 49.699/23/22 44.85 0.13 44.98 49.5010/5/22 45 0.19 45.19 49.293/8/23 45.13 0.01 45.14 49.347/18/23 44 0.35 44.35 50.139/20/23 43.86 0.03 43.89 50.5910/5/23 43.96 0.03 43.99 50.49 SEMINOLE MART NO 2 CLES PROJECT 17-051A GROUNDWATER MONITORING REPORT OCTOBER 2023 MW-11 93.79 10/31/17 43.55 1.95 45.50 49.91 diesel11/29/17 43.35 5.41 48.76 49.5312/5/17 44.05 0.50 44.55 49.6612/19/17 44.28 0.35 44.63 49.458/7/18 0.42 NC8/20/18 0.55 NCPUMP IN WELL 8/24/18 0.499/6/18 NC9/27/18 NC10/10/18 NCPUMP IN WELL 10/19/18 NC 10/29/18 41.31 0.49 41.81 52.39 gas orange 11/6/18 40.97 0.10 41.07 52.8012/2/18 39.79 1.72 41.51 53.7112/12/18 1.20 NC12/21/18 38.32 2.72 41.04 55.011/15/19 37.58 3.69 41.27 55.59 gas2/5/19 36.91 3.90 40.81 56.222/26/19 37.2 1.19 38.39 56.39 PUMP ON3/1/19 37.17 1.14 38.31 56.434/10/19 36.26 2.24 38.50 57.154/25/19 36.13 3.34 39.47 57.105/16/19 36.31 3.87 40.18 56.835/31/19 36.32 4.43 40.75 56.736/4/19 36.34 2.10 38.44 57.10 6/19/19 38.93 2.07 41.00 54.51 7/5/19 37.76 2.65 40.41 55.58 gas 7/15/19 38.21 2.21 40.42 55.217/29/19 38.33 2.78 41.11 54.998/3/19 38.54 2.57 41.11 54.828/21/19 39.15 2.09 41.24 54.299/18/19 40.04 1.19 41.23 53.5510/10/19 40.51 1.11 41.62 53.0911/120/19 41.7 0.38 42.08 52.0312/23/19 42.25 0.82 43.07 51.4012/31/19 42.31 0.78 43.09 51.351/16/20 42.43 0.68 43.11 50.683/16/20 41.96 0.74 42.70 51.093/23/20 41.72 0.38 42.10 51.69 4/2/20 41.72 0.40 42.12 51.67 4/10/20 41.7 0.37 42.07 51.72 4/20/20 41.69 0.32 42.01 51.784/30/20 41.7 0.32 42.02 51.775/15/20 41.64 0.33 41.97 51.826/5/20 41.5 0.29 41.79 52.007/10/20 40.92 0.56 41.48 52.318/19/20 40.38 1.40 41.78 52.019/21/20 40.22 0.97 41.19 52.6010/5/20 40.18 1.12 41.30 52.4910/14/20 40.22 1.01 41.23 52.5610/28/20 40.3 0.80 41.10 53.3611/5/20 40.35 0.73 41.08 52.7111/10/20 40.39 0.50 40.89 52.9011/17/20 NM 0.00 40.40 53.39 12/3/20 NM 0.00 40.08 53.71 12/18/20 40.23 0.07 40.30 53.491/15/21 39.58 1.32 40.90 52.892/2/21 39.12 1.02 40.14 53.652/25/21 38.69 0.60 39.29 54.503/5/21 38.34 0.73 39.07 54.723/11/21 37.97 0.90 38.87 54.923/15/21 38.04 0.85 38.89 54.904/7/21 37.12 2.01 39.13 54.664/12/21 37.2 1.53 38.73 55.064/19/21 37.62 0.97 38.59 55.205/6/21 37.76 0.99 38.75 55.045/12/21 38.17 0.42 38.59 55.206/3/21 38.45 0.76 39.21 54.58 6/9/21 36.51 0.07 36.58 57.21 7/7/21 39.23 0.46 39.69 54.10 7/12/21 39.42 0.03 39.45 54.347/22/21 39.51 0.02 39.53 54.267/26/21 39.45 0.03 39.48 54.318/13/21 39.62 0.30 39.92 53.878/19/21 39.65 0.47 40.12 53.679/3/21 39.91 0.79 40.70 53.099/16/21 40.09 0.66 40.75 53.049/28/21 40.27 0.55 40.82 52.9710/5/21 40.49 0.46 40.95 52.8410/7/21 40.5 0.46 40.96 52.8311/12/21 40.99 0.47 41.46 52.3311/15/21 41.01 0.49 41.50 52.29 11/18/21 41.37 0.56 41.93 51.86 11/24/21 41.52 0.46 41.98 51.81 12/17/21 41.93 0.41 42.34 51.4512/28/21 42.13 0.56 42.69 51.101/11/22 42.31 0.60 42.91 50.881/28/22 42.61 0.47 43.08 50.712/3/22 42.74 0.43 43.17 50.622/17/22 42.88 0.33 43.21 50.583/15/22 43.39 0.39 43.78 50.013/18/22 43.35 0.15 43.50 50.294/12/22 43.44 0.49 43.93 49.864/25/22 43.41 0.47 43.88 49.915/12/22 43.44 0.50 43.94 49.855/27/22 43.47 0.51 43.98 49.81 6/10/22 43.55 0.56 44.11 49.68 8/26/22 43.82 0.78 44.60 49.19 9/9/22 43.91 0.74 44.65 49.149/23/22 43.92 0.71 44.63 49.1610/5/22 44.36 0.72 45.08 48.713/8/23 44.52 0.61 45.13 48.667/18/23 43.34 0.54 43.88 49.919/20/23 43.17 1.03 44.20 49.5910/5/23 43.31 0.30 43.61 50.18 SEMINOLE MART NO 2 CLES PROJECT 17-051A GROUNDWATER MONITORING REPORT OCTOBER 2023 MW-12 92.92 10/31/17 42.62 1.02 43.64 50.13 diesel11/29/17 42.95 1.71 44.66 49.6812/5/17 43.03 1.70 44.73 49.6012/19/17 43.45 1.34 44.79 49.248/7/18 0.01 NC8/20/18 0.01 NC8/24/18 42.9 0.01 42.91 50.029/6/18 0.00 NC9/27/18 0.00 NC10/10/18 0.00 NC10/19/18 0.02 NC 10/29/18 40.51 0.01 40.52 52.41 diesel 11/6/18 NM 0.00 40.13 52.7912/2/18 NM 0.00 39.19 53.7312/12/18 0.23 NC diesel12/21/18 0.00 NC1/15/19 NM 0.00 37.24 55.682/5/19 NM 0.002/26/19 NM 0.00 36.49 56.434/25/19 NM 0.00 35.72 57.206/19/19 NM 0.00 36.61 56.317/5/19 NM 0.00 37.22 55.707/15/19 0.00 92.927/29/19 0.00 92.9211/20/19 NM 0.00 40.90 52.02 12/23/19 0.00 92.92 12/31/19 0.00 92.92 1/16/20 NM 0.00 41.71 51.213/16/20 NM 0.00 41.16 51.766/5/20 NM 0.00 40.77 52.158/19/20 NM 0.00 39.69 53.2310/5/20 39.46 0.11 39.57 53.3510/14/20 NM 0.00 92.927/12/21 NM 0.00 38.52 54.401/18/22 NM 0.00 41.84 51.083/15/22 NM 0.00 42.52 50.407/21/22 43.03 0.09 43.12 49.808/26/22 43.11 0.14 43.25 49.679/9/22 43.61 0.18 43.79 49.13 9/23/22 43.90 0.16 44.06 48.86 10/5/22 43.65 0.30 43.95 48.97 3/8/23 NM 0.00 43.81 49.117/18/23 NM 0.00 42.64 50.289/20/23 NM 0.00 42.47 50.4510/5/23 NM 0.00 42.59 50.33 MW-13 93.5 10/31/17 43.30 1.20 44.50 50.00 diesel11/29/17 43.59 2.07 45.66 49.56 12/5/17 43.65 2.05 45.70 49.51 12/19/17 44.10 0.58 44.68 49.30 8/7/18 0.00 NC8/20/18 0.00 NC8/24/18 NM 0.00 43.59 49.919/6/18 0.00 NC9/27/18 0.00 NC10/10/18 0.00 NC10/19/18 0.00 NC10/29/18 NM 0.00 41.24 52.2611/6/18 NM NC NM NC12/2/18 NM 0.00 39.96 53.5412/12/18 0.00 NC12/21/18 0.00 NC 1/15/19 NM 0.00 38.02 55.48 2/5/19 NM 0.00 2/26/19 NM 0.00 37.24 56.264/25/19 NM 0.00 36.48 57.026/19/19 NM 0.00 37.34 56.167/5/19 NM 0.00 37.95 55.5511/20/19 NM 0.00 41.56 51.9412/23/19 0.00 93.5012/31/19 0.00 93.501/16/20 NM 0.00 42.39 51.113/16/20 NM 0.00 41.97 51.536/5/20 NM 0.00 41.46 52.048/19/20 NM 0.00 40.36 53.1410/5/20 NM 0.00 40.16 53.3410/14/20 NM 0.00 41.17 52.33 7/12/21 NM 0.00 39.23 54.27 1/28/22 NM 0.00 42.50 51.007/21/22 NM 0.00 43.73 49.773/8/23 NM 0.00 44.49 49.010.00 93.5010/5/23 NM 0.00 43.26 50.24 MW-14 92.78 10/31/17 42.50 1.30 43.80 50.06 diesel 11/29/17 42.88 1.67 44.55 49.62 12/5/17 42.95 1.65 44.60 49.55 12/19/17 43.35 0.55 43.90 49.348/7/18 0.00 NC8/20/18 0.00 NC8/24/18 NM 0.00 42.83 49.959/6/18 0.00 NC9/27/18 0.00 NC10/10/18 0.00 NC10/19/18 0.00 NC10/29/18 NM 0.00 40.45 52.3311/6/18 NM NC NM NC12/2/18 NM 0.00 39.14 53.6412/12/18 0.33 NC12/21/18 0.00 NC 1/15/19 NM 0.00 37.20 55.58 2/5/19 NM 0.002/26/19 NM 0.00 36.42 56.364/25/19 NM 0.00 35.66 57.126/19/19 NM 0.00 36.54 56.247/5/19 NM 0.00 37.14 55.6411/20/19 NM 0.00 40.80 51.9812/23/19 0.00 92.7812/31/19 0.00 92.781/16/20 NM NC NM NC3/16/20 NM 0.00 41.13 51.656/5/20 NM NC NM NC Blocked8/19/20 NM 0.00 39.60 53.1810/5/20 NM 0.00 39.39 53.39 10/14/20 NM 0.00 39.39 53.39 7/12/21 NM 0.00 38.42 54.36 1/28/22 NM 0.00 41.74 51.047/21/22 NM 0.00 42.97 49.813/8/23 NM 0.00 43.73 49.050.00 92.7810/5/23 NM 0.00 42.51 50.27 SEMINOLE MART NO 2 CLES PROJECT 17-051A GROUNDWATER MONITORING REPORT OCTOBER 2023 MW-15 93.93 10/31/17 NM 0.00 43.64 50.2911/29/17 NM 0.00 44.03 49.9012/5/17 NM 0.00 44.11 49.8212/19/17 NM 0.00 44.29 49.648/7/18 0.01 NC8/20/18 0.01 NC8/24/18 44.71 0.38 45.09 49.16 gas9/6/18 0.31 NC9/27/18 0.17 NC10/10/18 0.20 NCPUMP IN WELL 10/19/18 0.20 NC 10/29/18 42.48 0.05 42.53 51.44 gas 11/6/18 41.1 0.28 41.38 52.7812/2/18 40.16 0.15 40.31 53.7412/12/18 0.01 NC12/21/18 38.79 0.24 39.03 55.101/15/19 38.19 0.58 38.77 55.64 gas2/5/19 37.52 0.38 37.90 56.352/25/19 37.49 0.31 37.80 56.393/1/19 37.18 0.36 37.54 56.694/25/19 ~1 Blocked5/16/19 ~15/31/19 ~16/19/19 <17/5/19 38.27 0.41 38.68 55.59 gas black 7/15/19 38.68 0.21 38.89 55.21 7/29/19 38.92 0.19 39.11 54.98 gas black 8/3/19 39.08 0.25 39.33 54.818/21/19 39.57 0.41 39.98 54.299/18/19 40.35 0.26 40.61 53.5410/10/19 40.80 0.41 41.21 53.0611/20/19 NM 0.00 41.88 52.0512/23/19 NM 0.00 42.49 51.4412/31/19 NM 0.00 42.55 51.381/16/20 NM 0.00 42.63 51.303/16/20 NM 0.00 46.21 47.723/23/20 NM 0.00 42.15 51.784/2/20 NM 0.00 42.08 51.854/10/20 NM 0.00 41.22 52.71 4/20/20 NM 0.00 41.78 52.15 4/30/20 NM 0.00 41.80 52.13 5/15/20 41.80 0.04 41.84 52.096/5/20 NM 0.00 41.70 52.237/10/20 NM 0.00 41.11 52.828/19/20 40.58 1.82 42.40 51.539/21/20 40.42 0.58 41.00 52.9310/5/20 40.43 0.27 40.70 53.2310/14/20 40.49 0.04 40.53 53.4010/28/20 40.51 0.27 40.78 53.1511/5/20 40.50 0.25 40.75 53.1811/10/20 40.52 0.33 40.85 53.0811/17/20 40.57 0.11 40.68 53.2512/3/20 40.51 0.21 40.72 53.2112/18/20 40.55 0.88 41.43 52.50 1/15/21 39.78 0.88 40.66 53.27 2/1/21 39.24 0.93 40.17 53.762/25/21 38.78 0.80 39.58 54.353/5/21 38.47 0.83 39.30 54.633/11/21 38.09 0.78 38.87 55.063/15/21 38.28 0.60 38.88 55.054/7/21 37.43 0.90 38.33 55.604/12/21 37.52 0.73 38.25 55.684/19/21 37.93 0.48 38.41 55.525/6/21 38.02 0.85 38.87 55.065/12/21 38.32 0.39 38.71 55.226/3/21 38.75 0.11 38.86 55.076/9/21 38.74 0.01 38.75 55.187/7/21 39.44 0.06 39.50 54.43 7/12/21 NM 0.00 39.60 54.33 7/22/21 39.67 0.01 39.68 54.25 7/26/21 40.61 0.01 40.62 53.318/13/21 40.81 0.01 40.82 53.118/19/21 NM 0.00 40.86 53.079/3/21 NM 0.00 40.19 53.749/16/21 NM 0.00 40.33 53.609/28/21 40.50 0.01 40.51 53.4210/5/21 NM 0.00 40.68 53.2510/7/21 NM 0.00 40.69 53.2411/12/21 NM 0.00 41.19 52.7411/15/21 NM 0.00 41.23 52.7011/18/21 NM 0.00 41.66 52.2711/24/21 41.71 0.02 41.73 52.20 12/17/21 42.11 0.01 42.12 51.81 12/28/21 NM 0.00 42.32 51.61 1/11/22 NM 0.00 42.64 51.291/28/22 NM 0.00 42.74 51.192/17/22 NM 0.00 43.36 50.573/15/22 NM 0.00 43.40 50.533/18/22 NM 39.00 43.39 50.544/12/22 43.57 0.02 43.58 50.354/25/22 43.53 0.02 43.55 50.385/12/22 NM 0.00 43.59 50.345/27/22 NM 0.00 43.60 50.336/10/22 NM 0.00 43.68 50.257/21/22 NM 0.00 43.87 50.068/26/22 NM 0.00 44.08 49.85 9/9/22 NM 0.00 44.29 49.64 9/23/22 NM 0.00 44.49 49.44 10/5/22 NM 0.00 44.51 49.423/8/23 NM 0.00 44.63 49.307/18/23 NM 0.00 43.45 50.489/20/23 NM 0.00 43.32 50.6110/5/23 NM 0.00 43.42 50.510.00 0.00 SEMINOLE MART NO 2 CLES PROJECT 17-051A GROUNDWATER MONITORING REPORT OCTOBER 2023 MW-16 94.64 10/31/17 NM 0.00 44.40 50.2411/29/17 NM 0.00 44.77 49.8712/5/17 NM 0.00 44.83 49.8112/19/17 NM 0.00 45.12 49.528/7/18 0.00 NC8/20/18 0.00 NC8/24/18 NM 0.00 44.41 50.239/6/18 0.00 NC9/27/18 0.00 NC10/10/18 0.00 NC10/19/18 0.00 NC 10/29/18 42.19 0.59 42.78 52.35 diesel 11/6/18 41.86 0.14 42.00 52.7612/2/18 40.9 0.24 41.14 53.7012/12/18 0.00 NC12/21/18 39.57 0.22 39.79 55.031/15/19 38.98 0.54 39.52 55.57 diesel2/5/19 38.32 0.36 38.68 56.262/25/19 38.24 0.58 38.82 56.303/1/19 38.14 0.33 38.47 56.444/10/19 37.55 1.05 38.60 56.914/25/19 37.42 1.07 38.49 57.045/16/19 37.64 1.34 38.98 56.775/31/19 37.97 0.23 38.20 56.636/4/19 37.99 0.02 38.01 56.65 6/19/19 38.49 0.13 38.62 56.13 7/5/19 39.12 0.20 39.32 55.49 diesel 7/15/19 39.48 0.42 39.90 55.097/29/19 39.69 0.46 40.15 54.878/3/19 39.91 0.07 39.98 54.728/21/19 40.41 0.11 40.52 54.219/18/19 41.11 0.21 41.32 53.4910/10/19 41.61 0.37 41.98 52.9711/20/19 NM 0.00 42.67 51.9712/23/19 43.23 0.10 43.33 51.3912/31/19 43.17 0.18 43.35 51.441/16/20 NM 0.00 43.37 51.273/16/20 NM 0.00 42.80 51.843/23/20 NM 0.00 41.78 52.86 4/2/20 NM 0.00 41.81 52.83 4/10/20 NM 0.00 42.41 52.23 4/20/20 NM 0.00 42.34 52.304/30/20 NM 0.00 42.59 52.055/15/20 NM 0.00 42.62 52.026/5/20 42.48 0.01 42.49 52.157/10/20 41.92 0.02 41.94 52.708/19/20 NM 0.00 41.47 53.179/21/20 NM 0.00 41.30 53.3410/5/20 41.27 0.06 41.33 53.3110/14/20 41.33 0.01 41.34 53.3010/28/20 41.33 0.03 41.36 53.2811/5/20 41.35 0.04 41.39 53.2511/10/20 41.39 0.02 41.41 53.2311/17/20 41.4 0.01 41.41 53.23 12/3/20 NM 0.00 41.39 53.25 12/18/20 41.52 0.08 41.60 53.041/15/21 40.67 0.09 40.76 53.882/1/21 40.2 0.03 40.23 54.412/25/21 39.68 0.04 39.72 54.923/5/21 NM 0.00 39.39 55.253/11/21 NM 0.00 39.01 55.633/15/21 NM 0.00 39.02 55.624/7/21 38.35 0.04 38.39 56.254/12/21 38.96 0.02 38.98 55.664/19/21 NM 0.00 39.02 55.625/6/21 38.97 0.04 39.01 55.635/12/21 39.21 0.01 39.22 55.426/3/21 NM 0.00 39.57 55.07 6/9/21 NM 0.00 39.61 55.03 7/7/21 NM 0.00 40.28 54.36 7/12/21 NM 0.00 40.42 54.227/22/21 NM 0.00 40.49 54.157/26/21 NM 0.00 40.43 54.218/13/21 NM 0.00 40.61 54.038/19/21 NM 0.00 40.66 53.989/3/21 NM 0.00 41.01 53.639/16/21 NM 0.00 41.14 53.509/28/21 NM 0.00 40.33 54.3110/5/21 NM 0.00 41.49 53.1510/7/21 NM 0.00 41.50 53.1411/12/21 NM 0.00 42.00 52.6411/15/21 NM 0.00 42.04 52.60 11/18/21 NM 0.00 42.47 52.17 11/24/21 NM 0.00 42.52 52.12 12/17/21 NM 0.00 42.91 51.7312/28/21 NM 0.00 43.12 51.521/11/22 43.45 0.04 43.49 51.151/28/22 NM 0.00 43.48 51.162/17/22 NM 0.00 43.72 50.923/15/22 NM 0.00 44.15 50.493/18/22 NM NC NM NC4/12/22 NM 0.00 44.34 50.304/25/22 44.3 0.01 44.31 50.335/12/22 NM 0.00 44.34 50.305/27/22 44.36 0.01 44.37 50.276/10/22 NM 0.00 44.44 50.20 7/21/22 NM 0.00 44.64 50.00 3/8/23 NM 0.00 45.39 49.25 7/18/23 NM 0.00 44.20 50.449/20/23 NM 0.00 44.07 50.5710/5/23 NM 0.00 44.19 50.45 SEMINOLE MART NO 2 CLES PROJECT 17-051A GROUNDWATER MONITORING REPORT OCTOBER 2023 MW-17 93.74 12/5/17 43.85 2.00 45.85 49.55 diesel12/19/17 44.05 1.78 45.83 49.39 diesel8/7/18 0.00 NC8/20/18 0.00 NC8/24/18 NM 0.00 43.78 49.969/6/18 0.00 NC9/27/18 0.00 NC10/10/18 0.00 NC10/19/18 0.00 NC10/29/18 41.02 0.19 41.21 52.69 diesel/gas11/6/18 41.35 0.38 41.73 52.33 12/2/18 40.08 0.26 40.34 53.62 12/12/18 2.00 NC12/21/18 38.73 0.33 39.06 54.951/15/19 38.03 1.06 39.09 55.53 diesel2/5/19 37.22 1.57 38.79 56.262/26/19 37.48 0.00 37.48 56.26 PUMP ON3/1/19 37.19 0.12 37.31 56.534/10/19 36.35 2.65 39.00 56.94 diesel4/25/19 36.14 2.96 39.10 57.105/16/19 36.76 0.92 37.68 56.835/31/19 36.96 0.52 37.48 56.696/4/19 36.97 0.08 37.05 56.766/19/19 37.47 0.53 38.00 56.187/5/19 38.03 0.83 38.86 55.57 diesel 7/15/19 38.58 0.96 39.54 55.00 7/29/19 38.62 1.04 39.66 54.95 diesel 8/3/19 38.81 1.00 39.81 54.768/21/19 39.28 1.02 40.30 54.299/18/19 40.10 0.65 40.75 53.5310/10/19 40.66 0.28 40.94 53.0311/20/19 NM 0.00 40.78 52.9612/23/19 NM 0.00 42.41 51.3312/31/19 NM 42.50 42.50 51.241/16/20 NM 0.00 42.59 51.153/16/20 NM 0.00 41.72 52.023/23/20 41.73 0.18 41.91 51.834/2/20 41.72 0.19 41.91 51.834/10/20 41.75 0.21 41.96 51.78 4/20/20 41.73 0.17 41.90 51.84 4/30/20 41.72 0.18 41.90 51.84 5/15/20 41.73 0.19 41.92 51.826/5/20 41.61 0.19 41.80 51.947/10/20 41.03 0.10 41.13 52.618/19/20 40.50 0.42 40.92 52.829/21/20 40.36 0.11 40.47 53.2710/5/20 40.32 0.07 40.39 53.3510/14/20 40.33 0.20 40.53 53.2110/28/20 41.80 0.20 42.00 51.74 PUMP ON11/5/20 40.38 0.00 40.48 53.2611/10/20 40.43 0.07 40.50 53.2411/17/20 NM 0.00 42.01 51.7312/3/20 NM 0.00 40.08 53.6612/18/20 NM 0.00 43.57 50.17 1/15/21 39.78 0.08 39.86 53.88 2/1/21 NM 0.00 39.32 54.422/25/21 38.78 0.24 39.02 54.723/5/21 38.49 0.17 38.66 55.083/11/21 38.06 0.50 38.56 55.183/15/21 38.01 0.60 38.61 55.134/7/21 37.05 2.10 39.15 54.594/12/21 37.16 0.87 38.03 55.714/19/21 37.23 0.58 37.81 55.935/6/21 37.78 1.43 39.21 54.535/12/21 38.16 0.51 38.67 55.076/3/21 38.49 0.37 38.86 54.886/9/21 40.08 0.61 40.69 53.057/7/21 NM 0.00 39.29 54.45 7/12/21 NM 0.00 39.42 54.32 7/22/21 NM 0.00 39.52 54.22 7/26/21 NM 0.00 39.47 54.278/13/21 NM 0.00 39.65 54.098/19/21 NM 0.00 39.71 54.039/3/21 NM 0.00 40.03 53.719/16/21 NM 0.00 40.17 53.579/28/21 NM 0.00 40.34 53.4010/5/21 NM 0.00 40.52 53.2210/7/21 NM 0.00 40.53 53.2111/12/21 NM 0.00 41.03 52.7111/15/21 NM 0.00 41.07 52.6711/18/21 NM 0.00 41.50 52.2411/24/21 NM 0.00 41.62 52.12 12/17/21 NM 0.00 42.02 51.72 12/28/21 NM 0.00 42.23 51.51 1/11/22 42.59 0.01 42.60 51.141/28/22 NM 0.00 42.72 51.022/17/22 NM 0.00 42.97 50.773/15/22 NM 0.00 43.38 50.363/18/22 NM NC NM NC4/12/22 NM 0.00 43.56 50.184/25/22 NM 0.00 43.52 50.225/12/22 NM 0.00 43.57 50.175/27/22 NM 0.00 43.60 50.146/10/22 NM 0.00 43.69 50.057/21/22 NM 0.00 43.89 49.858/26/22 NM 0.00 44.12 49.62 9/9/22 NM 0.00 44.35 49.39 9/23/22 NM 0.00 44.42 49.32 10/5/22 NM 0.00 44.57 49.173/8/23 NM 0.00 44.69 49.059/20/23 43.27 0.04 43.31 50.4310/5/23 43.41 0.01 43.42 50.32 MW-18 92.31 12/5/17 NM 0.00 42.90 49.4112/19/17 NM 0.00 43.13 49.18 8/7/18 0.00 NC 8/20/18 0.00 NC 8/24/18 NM 0.00 42.50 49.819/6/18 0.00 NC9/27/18 0.00 NC10/10/18 0.00 NC10/19/18 NM 0.00 NC10/29/18 NM 0.00 40.07 52.2411/6/18 NM NC NM NC12/2/18 NM 0.00 38.73 53.5812/12/18 0.00 NC12/21/18 0.00 NC1/15/19 NM 0.00 36.81 55.502/5/19 NM 2/26/19 NM 0.00 36.01 56.30 4/25/19 NM 0.00 35.25 57.06 6/19/19 NM 0.00 36.11 56.207/5/19 NM 0.00 36.73 55.5811/20/19 NM 0.00 40.43 51.8812/23/19 0.0012/31/19 0.001/16/20 NM 0.00 41.61 50.703/16/20 NM 0.00 40.71 51.606/5/20 NM 0.00 40.31 52.008/19/20 NM 0.00 39.21 53.1010/5/20 NM 0.00 38.90 53.4110/14/20 NM 0.00 39.00 53.317/12/21 NM 0.00 38.03 54.281/28/22 NM 0.00 41.33 50.98 7/21/22 NM 0.00 42.63 49.68 3/8/23 NM 0.00 44.37 47.940.00 92.3110/5/23 NM 0.00 42.18 50.13 SEMINOLE MART NO 2 CLES PROJECT 17-051A GROUNDWATER MONITORING REPORT OCTOBER 2023 MW-19 92.65 12/5/17 42.98 1.44 44.42 49.43 diesel12/19/17 43.18 1.64 44.82 49.198/7/18 0.00 NC8/20/18 0.00 NC8/24/18 NM 0.00 42.83 49.829/6/18 0.00 NC9/27/18 0.00 NC10/10/18 0.00 NC10/19/18 0.00 NC10/29/18 NM 0.00 40.44 52.2111/6/18 NM NC NM NC 12/2/18 NM 0.00 39.11 53.54 12/12/18 NM 0.00 NC12/21/18 0.00 NC1/15/19 NM 0.00 37.20 55.452/5/19 NM2/26/19 NM 0.00 36.41 56.244/25/19 NM 0.00 35.65 57.006/19/19 NM 0.00 36.51 56.147/5/19 NM 0.00 37.12 55.5311/20/19 NM 0.00 40.76 51.8912/23/19 0.0012/31/19 0.001/16/20 NM 0.00 42.65 50.003/16/20 NM 0.00 41.11 51.54 6/5/20 NM 0.00 40.68 51.97 8/19/20 NM 0.00 39.58 53.07 10/5/20 NM 0.00 39.35 53.3010/14/20 NM 0.00 39.37 53.287/12/21 NM 0.00 38.40 54.251.28/22 NM 0.00 41.73 50.927/21/22 NM 0.00 42.94 49.713/8/23 NM 0.00 43.73 48.920.00 92.6510/5/23 NM 0.00 42.48 50.17 MW-20 93.65 12/5/17 NM 0.00 44.23 49.4212/19/17 NM 0.00 44.29 49.368/7/18 0.00 NC8/20/18 0.00 NC8/24/18 NM 0.00 43.86 49.799/6/18 0.00 NC9/27/18 0.00 NC10/10/18 0.00 NC10/19/18 0.00 NC10/29/18 NM 0.00 41.53 52.1211/6/18 NM NC NM NC12/2/18 NM 0.00 40.22 53.43 12/12/18 NM 0.00 NC 12/21/18 0.00 NC 1/15/19 NM 0.00 38.32 55.332/5/19 NM 0.00 NC2/26/19 NM 0.00 37.53 56.124/25/19 NM 0.00 36.80 56.856/19/19 NM 0.00 37.64 56.017/5/19 NM 0.00 38.24 55.4111/20/19 NM 0.00 41.83 51.8212/23/19 0.00 93.6512/31/19 0.00 93.651/16/20 NM 0.00 42.65 51.003/16/20 NM 0.00 42.19 51.466/5/20 NM 0.00 41.70 51.95 10/5/20 NM 0.00 40.45 53.20 10/14/20 NM 0.00 40.25 53.40 7/12/21 NM 0.00 39.51 54.141/28/22 NM 0.00 42.75 50.907/21/22 NM 0.00 43.96 49.693/8/23 NM 0.00 44.74 48.9110/5/23 NM 0.00 43.52 50.13 MW-21 92.92 12/5/17 NM 0.00 43.98 48.94 12/19/17 NM 0.00 44.22 48.70 8/7/18 NM NC NM NC 8/20/18 NM NC NM NC8/24/18 NM 0.00 43.59 49.339/6/18 NM NC NM NC9/27/18 NM NC NM NC10/10/18 NM NC NM NC10/19/18 NM NC NM NC10/29/18 NM 0.00 41.08 51.8411/6/18 NM NC NM NC12/2/18 NM 0.00 39.78 53.1412/12/18 NM 0.00 NC12/21/18 NM NC NM NC1/15/19 NM 0.00 37.81 55.11 2/5/19 NM NC NM NC 2/26/19 NM 0.00 36.96 55.96 4/25/19 NM 0.00 36.23 56.696/19/19 NM 0.00 37.16 55.767/5/19 NM 0.00 37.66 55.2611/20/19 NM 0.00 41.41 51.5112/23/19 NM NC NM NC12/31/19 NM NC NM NC1/16/20 NM 0.00 42.31 50.613/16/20 NM 0.00 41.47 51.456/5/20 NM 0.00 41.32 51.6010/5/20 NM 0.00 39.98 52.9410/14/20 NM 0.00 39.98 52.947/12/21 NM 0.00 38.98 53.941/28/22 NM 0.00 42.38 50.54 7/21/22 NM 0.00 43.72 49.20 3/8/23 NM 0.00 44.42 48.5010/5/23 NM 0.00 43.24 49.68 ft-rel = Well casing elevations measured by East Coast Environmental, PA Product thicknesses measured with interface probe or visual measuring device and measuring tape. NM = None measured. NC = Not calculated. * If free diesel fuel product is present in a well, groundwater elevation is calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.832] DTP = Depth to product measured from the top of the well casing. ft-btoc = Feet below the top of the well casing. DTW = Depth to groundwater measured from the top of the well casing. Notes: Surfactant injection performed May 2-8, 2018 Aquifer stabilization and vacuum recovery between May 9 and June 20, 2018. Total fluids pumping from source wells ongoing. TOC = Top of well casing. SEMINOLE MART 2 CLES PROJECT NO 17-051A GROUNDWATER MONITORING REPORT OCTOBER 2023 TABLE 3 GROUNDWATER ELEVATIONS - OCTOBER 5, 2023 SEMNOLE MART NO. 2 691 SEMINOLE ROAD BROADWAY, HARNETT COUNTY, NORTH CAROLINA NCDEQ INCIDENT NO. 42025 NCDEQ UST SECTION FACILITY ID. 0-000014231 CLES PROJECT NO. 17-051A Page 1 of 1 Well ID TOC (ft-rel)Date DTP (ft- btoc) Product Thickness (ft) DTW (ft-btoc) GW Elev (ft-rel) MW-1 93.72 10/5/23 35.71 0.03 35.74 57.98 MW-2 94.36 10/5/23 43.6 0.7 44.30 50.06 MW-3 93.58 10/5/23 43 1.2 44.20 49.38 MW-4 93.52 10/5/23 NM 0 43.13 50.39 MW-5 93.40 10/5/23 NM 0 42.96 50.44 MW-6 92.84 10/5/23 NM 0 42.54 50.30 MW-7 92.92 10/5/23 NM 0 42.54 50.38 MW-8 93.38 10/5/23 43.08 0.03 43.11 50.27 MW-9 93.63 10/5/23 NM 0 43.22 50.41 MW-10 94.48 10/5/23 43.96 0.03 43.99 50.49 MW-11 93.79 10/5/23 43.31 0.3 43.61 50.18 MW-12 92.92 10/5/23 NM 0 42.59 50.33 MW-13 93.50 10/5/23 NM 0 43.26 50.24 MW-14 92.78 10/5/23 NM 0 42.51 50.27 MW-15 93.93 10/5/23 NM 0 43.42 50.51 MW-16 94.64 10/5/23 NM 0 44.19 50.45 MW-17 93.74 10/5/23 43.41 0.01 43.42 50.32 MW-18 92.31 10/5/23 NM 0 42.18 50.13 MW-19 92.65 10/5/23 NM 0 42.48 50.17 MW-20 93.65 10/5/23 NM 0 43.52 50.13 MW-21 92.92 10/5/23 NM 0 43.24 49.68 Notes: NM = None measured. * If free product is present in a well, groundwater elevation is calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.86] TOC = Top of well casing. DTP = Depth to product measured from the top of the well casing. ft-btoc = Feet below the top of the well casing. DTW = Depth to groundwater measured from the top of the well casing. ft-rel = Well casing elevations reported by East Coast Encironmental, PA CAP 11/1/17. SEMINOLE MART 2 CLES PROJECT 17-051A GROUNDWATER MONTORING REPORT OCTOBER 2023 TABLE 4 FIELD PARAMETERS SEMNOLE MART NO. 2 691 SEMINOLE ROAD BROADWAY, HARNETT COUNTY, NORTH CAROLINA NCDEQ INCIDENT NO. 42025 NCDEQ UST SECTION FACILITY ID. 0-000014231 CLES PROJECT NO. 17-051A pH Conductivity (mS/Cm)1 Temperature (oC)2 MW-1 7/21/22 6.5 0.3 19.1 MW-2 7/21/22 NM NM NM MW-3 7/21/22 NM NM NM MW-4 7/21/22 6.5 0.18 18.7 MW-5 7/21/22 6.50 0.07 17.6 MW-6 7/21/22 6.00 0.04 17.4 MW-7 7/21/22 6.00 0.08 17.5 MW-8 7/21/22 6.0 0.22 19.4 MW-9 7/21/22 6.0 0.12 18.2 MW-10 7/21/22 6.5 0.11 18.1 MW-11 7/21/22 6.5 0.19 18.1 MW-12 7/21/22 6.5 0.09 18.0 MW-13 7/21/22 6.0 0.17 17.90 MW-14 7/21/22 6.5 0.07 18.00 MW-15 7/21/22 6.5 0.19 18.50 MW-16 7/21/22 6.0 0.19 17.50 MW-17 7/21/22 6.5 0.19 18.60 MW-18 7/21/22 6.50 0.05 17.5 MW-19 7/21/22 6.0 0.25 17.7 MW-20 7/21/22 7.0 0.19 17.7 MW-21 7/21/22 6.00 0.00 18.20 Notes: 2. oC = Degrees Celsius. 3. NM = Not measured.(pH sensor malfunctioned during event. Surfactant Injection June 17-18, 2021 Well ID Date Field Parameters 1. mS/cm = milli Siemens per centimeter. SEMINOLE MART NO 2CLES PROJECT NO 17-051A GROUNDWATER MONITORINBG REPORTOCTOBER 2023 TABLE 5 GROUNDWATER ANALYTICAL RESULTS SEMNOLE MART NO. 2691 SEMINOLE ROADBROADWAY. HARNETT COUNTY, NORTH CAROLINANCDENR INCIDENT NO. 42025NCDEQ UST SECTION FACILITY ID. 0-000014231CLES PROJECT NO. 17-051A Page 1 of 4EPAEPAEPAEPAEPAEPAEPAEPAEPA EPA EPA EPA EPA EPA EPA EPA EPA EPA EPA 624 6200B 6200B 624 624 6200B 6200B 8260 624 625 6200B 624 6200B 6200B 6200B 6200B 624 624 624 Well ID Date Sampled (m/dd/yy) MW-1 10/5/23 72 NR NR 150 <3.6 NR NR <2.6 21 NR NR 370 NR NR NR NR 340 470 810 MW-1 7/21/22 64 D NR NR 290 D <20 NR NR <20 210 D NR NR 370 D NR NR NR NR 830 D 1,100 D 1,900 D MW-1 7/12/21 <50 NR NR 170 D <50 NR NR <50 <50 <400 NR 140 D NR NR NR NR 480 D 610 D 1,100 DMW-1 10/14/20 <10 NR NR 76 <10 NR NR <10 34 <200 NR 92 NR NR NR NR 260 290 560MW-1 7/5/19 110 NR NR 940 <10 NR NR <10 <220,000 <220,000 NR 1300 NR NR NR NR 1800 3000 4900MW-1 12/3/18 43 NR NR 650 <10 NR NR <10 <50 <50 NR 530 NR NR NR NR 1200 1700 2900 MW-2 7/21/22 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NRMW-2 7/12/21 80 D NR NR 74 D <20 NR NR <20 26 D <200 NR NR NR NR NR NR 230 D 230 D 460 DMW-2 10/14/20 37 NR NR 100 <10 NR NR <10 37 <200 NR NR NR NR NR NR 430 390 820MW-2 12/3/18 320 NR NR 770 <10 NR NR <10 <2,000 <2000 NR NR NR NR NR NR 1300 2100 3400 MW-3 7/21/22 29 D NR NR 23 D <20 NR NR <20 54 D NR NR 47 NR NR NR NR 380 D 85 D 470 DMW-3 7/12/21 70 D NR NR 140 D <20 NR NR <20 33 D <50 NR 130 D NR NR NR NR 310 D 310 D 620 DMW-3 10/14/20 78 NR NR 170 <10 NR NR <10 45 <200 NR 120 NR NR NR NR 340 370 710MW-3 12/3/18 150 NR NR 170 <10 NR NR <10 14 JD 14 JD NR 180 NR NR NR NR 340 580 920 MW-4 10/5/23 <5.7 NR NR <4.6 <3.6 NR NR <2.6 <1.2 NR NR <5.7 NR NR NR NR 15 <12 <16MW-4 7/21/22 <5 NR NR 4.6 JD <5 NR NR <5 6 D NR NR <5 NR NR NR NR 13 D 8.8 D 22 D MW-4 7/12/21 3.4 JD NR NR 40 D <5 NR NR <5 12 D <50 NR <5 NR NR NR NR 220 D 47 D 270 DMW-4 10/14/20 5.6 NR NR 9.1 <1 NR NR <1 3.1 <50 NR 2.0 NR NR NR NR 110 17 130MW-4 12/3/18 21 NR NR 39 <1 NR NR 1.3 <2 <200 NR 21 NR NR NR NR 130 25 160 MW-5 10/5/23 <0.57 NR NR <0.46 <0.36 NR NR <0.26 <0.12 NR NR <0.57 NR NR NR NR <0.44 <1.2 <1.6MW-5 7/12/21 <1 NR NR <1 <1 NR NR <1 3.20 <10 NR <1 NR NR NR NR 40 7.0 47MW-5 10/14/20 8.1 NR NR 3.2 <1 NR NR <1 5 <10 NR <1 NR NR NR NR 61 53 110MW-5 7/5/19 <1 NR NR 2.3 <1 NR NR <1 5.3 J 5.3 J NR <1 NR NR NR NR 69 91 160 MW-5 12/2/18 <1 NR NR <1 <1 NR NR <1 <2 <10 NR <1 NR NR NR NR 0.63 J <2 1.4 JMW-5 12/5/17 2.8 NR NR 1.2 <1 NR NR <1 0.91 J 3.4 J NR 9.2 NR NR NR NR 2.5 3.8 6.3 MW-6 10/5/23 <0.57 NR NR <0.46 <0.36 NR NR <0.26 <0.12 NR NR <0.57 NR NR NR NR <0.44 <1.2 <1.6MW-6 7/12/21 <1 NR NR <1 <1 NR NR <1 <1 <10 NR <1 NR NR NR NR <1 <2 <3 MW-6 10/14/20 <1 NR NR <1 <1 NR NR <1 <1 <10 NR <1 NR NR NR NR 0.57 J <2 <3MW-6 7/5/19 <1 NR NR <1 <1 NR NR <1 <10 <10 NR <1 NR NR NR NR <1 <2 <3MW-6 12/2/18 <1 NR NR 0.72 J <1 NR NR <1 <2 <10 NR <1 NR NR NR NR 0.96 J 1.8 J 2.7MW-6 12/5/17 54 NR NR 25 <1 NR NR 1.4 8.9 7.2 J NR 170 NR NR NR NR 39 94 130 MW-7 10/5/23 <0.57 NR NR <0.46 <0.36 NR NR <0.26 <0.12 NR NR <0.57 NR NR NR NR <0.44 <1.2 <1.6MW-7 7/12/21 <1 NR NR <1 <1 NR NR <1 <1 <10 NR <1 NR NR NR NR <1 <2 <3MW-7 10/14/20 <1 NR NR <1 <1 NR NR <1 <1 <10 NR <1 NR NR NR NR <1 <2 <2MW-7 3/16/20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <1 <1 <1 <1 0.60 J <1 <1 <2 <2MW-7 12/2/18 <1 NR NR <1 <1 NR NR <1 <2 <10 NR <1 NR NR NR NR 2.7 <2 3.7 MW-8 10/5/23 <11 NR NR 59 <7.2 NR NR 26 33 NR NR <11 NR NR NR NR 210 120 330MW-8 7/21/22 12 D NR NR 70 D <5 NR NR <5 15 D NR NR 3.6 JD NR NR NR NR 160 D 130 D 290 DMW-8 7/12/21 19 D NR NR 60 D <5 NR NR <5 12 D <30 NR 26 D NR NR NR NR 150 D 110 D 260 DMW-8 10/14/20 5.6 NR NR 23 <1 NR NR <1 10 <200 NR 6.8 NR NR NR NR 66 31 96MW-8 12/3/18 11 NR NR 95 <10 NR NR <10 11 JD 11 JD NR 72 NR NR NR NR 180 230 410 MW-8 12/5/17 45 D NR NR 520 D NR NR NR <1.6 92 D 770 JD NR 670 D NR NR NR NR 850 D 1400 D 2200 D MW-9 10/5/23 20 NR NR <4.6 <3.6 NR NR <2.6 <1.2 NR NR <5.7 NR NR NR NR 44 22 66MW-9 7/21/22 <10 NR NR 48 D <10 NR NR <10 14 D NR NR 14 D NR NR NR NR 100 D 130 D 240 DMW-9 7/12/21 74 D NR NR 150 D <5 NR NR <5 26 D 12 JD NR 59 D NR NR NR NR 310 D 400 D 710 D MW-9 10/14/20 41 NR NR 130 <2 NR NR <2 21 20 NR 44 NR NR NR NR 250 370 620MW-9 3/16/20 18 JD 16 JD <20 50 D <20 12 JD <20 <20 <20 23 D 12 JD <20 <20 87 D 33 D 110 D 86 D 200 D MW-9 12/3/18 7.4 NR NR 99 <5 NR NR <5 14 JD 14 JD NR 19 NR NR NR NR 210 220 430Note:Wells MW-1, MW-2, MW-3, MW-4, MW-7, MW-9, MW-12 to MW-17, MW-19 and MW-21 not sampled 12/5/17.All sample analytical concentrations are reported in ug/l.Bold depicts constiuents detected above the sample practical quantitation limit. SHADED AND BOLD numbers indicate concentrations above NCAC 2L Groundwater Quality Standard.GCL = gross contamination level.SHADED AND BOLD and RED numbers indicate concentrations above NCAC 2L Groundwater Quality Standard and NCDENR GCLs.NL = Not Listed.NR = Not Requested or Not reported by laboratory. Analytical Method Contaminant of Concern BenzeneEthylbenzeneMethyl tertiary butyl ether (MTBE)NaphthaleneNaphthaleneToluene0-xylenesM&P xylenesTotal XylenesTrichloroetheneTrichlorofluoro -methane1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenen-propylbenzenep-IsopropyltolueneIsopropylbenzeneIsopropyl Ethern-Butylbenzenesec-Butylbenzene SEMINOLE MART NO 2CLES PROJECT NO 17-051A GROUNDWATER MONITORINBG REPORTOCTOBER 2023 TABLE 5 GROUNDWATER ANALYTICAL RESULTS SEMNOLE MART NO. 2691 SEMINOLE ROADBROADWAY. HARNETT COUNTY, NORTH CAROLINANCDENR INCIDENT NO. 42025NCDEQ UST SECTION FACILITY ID. 0-000014231CLES PROJECT NO. 17-051A Page 2 of 4EPAEPAEPAEPAEPAEPASM EPA EPA SM SM SM 625 625 625 625 625 625 2540C-2011 365.4 300 4500S2 3500Fe 5310 D-2000 B-1997 B-2000 Well ID Date Sampled (m/dd/yy)Sulfde (mg/l)Ferrous Iron (mg/l)TOC (mg/l)MW-1 10/5/23 NR NR NR NR NR NR NR NR NR NR NR NR MW-1 7/21/22 NR NR NR NR NR NR NR NR NR NR NR NR MW-1 7/12/21 <200 <400 <400 <400 <400 <400 NR NR NR NR NR NRMW-1 10/14/20 <100 <200 <200 <200 <200 <200 NR NR NR NR NR NRMW-1 7/5/19 <110,000 <220,000 <220,000 <220,000 <220,000 <220,000 NR NR NR NR NR NRMW-1 12/3/18 14 <50 <50 <50 <50 <50 520 NR NR NR NR NR MW-2 7/21/22 NR NR NR NR NR NR NR NR NR NR NR NRMW-2 7/12/21 <100 <200 <200 <200 <200 <200 NR NR NR NR NR NRMW-2 10/14/20 <100 <200 <200 <200 <200 <200 NR NR NR NR NR NRMW-2 12/3/18 2000 D <2000 <2000 <2000 410 JD <2000 150 NR NR NR NR NR MW-3 7/21/22 NR NR NR NR NR NR NR NR NR NR NR NRMW-3 7/12/21 <25 <50 <50 <50 <50 <50 NR NR NR NR NR NRMW-3 10/14/20 <100 <200 <200 <200 <200 <200 NR NR NR NR NR NRMW-3 12/3/18 <25 <50 8.4 JD <50 <50 <50 220 NR NR NR NR NR MW-4 10/5/23 NR NR NR NR NR NR NR NR NR NR NR NRMW-4 7/21/22 NR NR NR NR NR NR NR NR NR NR NR NRMW-4 7/12/21 <25 <50 <50 <50 <50 <50 NR NR NR NR NR NRMW-4 10/14/20 <25 <50 <50 <50 <50 <50 NR NR NR NR NR NRMW-4 12/3/18 <100 <200 <200 <200 <200 <200 220 NR NR NR NR NR MW-5 10/5/23 NR NR NR NR NR NR NR NR NR NR NR NRMW-5 7/12/21 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NRMW-5 10/14/20 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NRMW-5 7/5/19 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NR MW-5 12/2/18 <5 <10 <10 <10 <10 <10 <50 NR NR NR NR NRMW-5 12/5/17 <5 <10 <10 <10 <10 <10 <50 0.13 <5 <0.10 <0.05 1.3 MW-6 10/5/23 NR NR NR NR NR NR NR NR NR NR NR NRMW-6 7/12/21 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NR MW-6 10/14/20 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NRMW-6 7/5/19 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NRMW-6 12/2/18 <5 <10 <10 <10 <10 <10 <50 NR NR NR NR NRMW-6 12/5/17 <5 <10 <10 <10 <10 <10 <50 <0.10 6.7 <0.10 <0.05 0.48 J MW-7 10/5/23 NR NR NR NR NR NR NR NR NR NR NR NRMW-7 7/12/21 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NRMW-7 10/14/20 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NRMW-7 3/16/20 NR NR NR NR NR NR NR NR NR NR NR NRMW-7 12/2/18 <5 <10 <10 <10 <10 <10 <50 NR NR NR NR NR MW-8 10/5/23 NR NR NR NR NR NR NR NR NR NR NR NRMW-8 7/21/22 NR NR NR NR NR NR NR NR NR NR NR NRMW-8 7/12/21 <15 <30 <30 <30 <30 <30 NR NR NR NR NR NRMW-8 10/14/20 <100 <200 <200 <200 <200 <200 NR NR NR NR NR NRMW-8 12/3/18 <25 <50 <50 <50 <50 <50 180 NR NR NR NR NR MW-8 12/5/17 NR <670 NR NR NR 710 JD NR NR NR NR NR NR MW-9 10/5/23 NR NR NR NR NR NR NR NR NR NR NR NRMW-9 7/21/22 NR NR NR NR NR NR NR NR NR NR NR NRMW-9 7/12/21 <15 <30 <30 <30 <30 <30 ND NR NR NR NR NR MW-9 10/14/20 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NRMW-9 3/16/20 NR NR NR NR NR NR NR NR NR NR NR NR MW-9 12/3/18 <25 <50 <50 <50 <50 <50 54 NR NR NR NR NRNote:Wells MW-1, MW-2, MW-3, MW-4, MW-7, MW-9, MW-12 to MW-17, MW-19 and MW-21 not sampled 12/5/17.All sample analytical concentrations are reported in ug/l.Bold depicts constiuents detected above the sample practical quantitation limit. SHADED AND BOLD numbers indicate concentrations above NCAC 2L Groundwater Quality Standard.GCL = gross contamination level.SHADED AND BOLD and RED numbers indicate concentrations above NCAC 2L Groundwater Quality Standard and NCDENR GCLs.NL = Not Listed.NR = Not Requested or Not reported by laboratory.Page 4 of 4 Analytical Method Contaminant of Concern Bis(2-ethylhexyl)phthalatePhosphorous (mg/l)Sulfate - SO4 (mg/l)Diethylphthalate2,4-Dimethylphenol2,4-DinitrophenolPhenanthrenePyreneTDS SEMINOLE MART NO 2CLES PROJECT NO 17-051A GROUNDWATER MONITORINBG REPORTOCTOBER 2023 EPA EPA EPA EPA EPA EPA EPA EPA EPA EPA EPA EPA EPA EPA EPA EPA EPA EPA EPA 624 6200B 6200B 624 624 6200B 6200B 8260 624 625 6200B 624 6200B 6200B 6200B 6200B 624 624 624 Well ID Date Sampled (m/dd/yy) MW-10 10/5/23 28 NR NR 68 <7.2 NR NR <5.2 17 J NR NR 34 NR NR NR NR 140 170 310MW-10 7/21/22 38 D NR NR 70 D <20 NR NR <20 38 D NR NR 31 D NR NR NR NR 180 D 180 D 360 D MW-10 7/12/21 82 D NR NR 65 D <10 NR NR <10 21 D <50 NR 53 D NR NR NR NR 200 D 130 D 330 DMW-10 10/14/20 110 NR NR 89 <1 NR NR 1.70 25 <50 NR 55 NR NR NR NR 210 180 390MW-10 7/5/19 21 NR NR 77 <5 NR NR <5 <100 <100 NR 75 NR NR NR NR 180 230 410MW-10 12/3/18 82 NR NR 120 <5 NR NR <5 39 JD 39 JD NR 190 NR NR NR NR 340 500 840MW-10 12/5/17 130 D NR NR 54 D <5 NR NR 3.8 JD 20 D 19 NR 430 D NR NR NR NR 110 D 230 D 340 D MW-11 10/5/23 19 NR NR 110 <3.6 NR NR 13 21 NR NR 120 NR NR NR NR 280 340 620MW-11 7/21/22 12 JD NR NR 340 D <20 NR NR <20 <20 NR NR 200 D NR NR NR NR 770 D 870 D 1,600 DMW-11 7/12/21 36 D NR NR 69 D <20 NR NR <20 16 JD <50 NR 100 D NR NR NR NR 180 180.0 360MW-11 10/14/20 65 NR NR 74 <10 NR NR <10 11 <100 NR 140 NR NR NR NR 210 200 420MW-11 3/16/20 40 D 35 D 15 D 99 D <20 20 27 D <20 21 D NR 37 D 180 D <20 <20 220 D 70 D 250 D 290 D 550 DMW-11 12/3/18 160 NR NR 220 <5 NR NR 3.5 35 JD 35 JD NR 440 NR NR NR NR 380 600 970MW-11 12/5/17 19 D NR NR 210 D NR NR NR <1.6 39 D 140 JD NR 200 D NR NR NR NR 350 D 630 D 990 D MW-12 10/5/23 <5.7 NR NR 18 <3.6 NR NR <2.6 5.1 J NR NR <5.7 NR NR NR NR 77 53 130MW-12 7/21/22 2.9 D NR NR 44 D <2 NR NR <2 16 D NR NR 19 D NR NR NR NR 140 D 130 D 270 D MW-12 7/12/21 <1 NR NR 15 <1 NR NR <1 5 <10 NR 2.9 NR NR NR NR 42 28 70MW-12 10/14/20 <1 NR NR 1.3 <1 NR NR <1 0.75 J <10 NR <1 NR NR NR NR 3.2 2.2 5.4MW-12 7/5/19 <1 NR NR 14 <1 NR NR <1 3.6 J 3.6 J NR 2.8 NR NR NR NR 45 12 56MW-12 12/3/18 <5 NR NR 12 <5 NR NR <5 <50 <50 NR 18 NR NR NR NR 35 18 53 MW-13 10/5/23 <5.7 NR NR 61 <3.6 NR NR 9.4 J 11 NR 25 NR NR NR NR 120 190 310MW-13 7/21/22 3.5 JD NR NR 110 D <5 NR NR <5 19 D NR NR 59 D NR NR NR NR 230 D 330 D 560 DMW-13 7/12/21 0.84 J NR NR 63 <1 NR NR <1 8.5 5.2 J NR 34 NR NR NR NR 120 140 260MW-13 10/14/20 2.4 NR NR 75 <1 NR NR <1 11 <50 NR 33 NR NR NR NR 150 230 380MW-13 12/2/18 <1 NR NR 9 <1 NR NR <1 6.1 JD 6.1 JD NR 6.6 NR NR NR NR 18 27 45 MW-14 10/5/23 <2.9 NR NR <2.3 <1.8 NR NR <1.3 2.7 J NR NR <2.9 NR NR NR NR 32 18 50MW-14 7/21/22 <1 NR NR 3 <1 NR NR <1 1.3 NR NR <1 NR NR NR NR 7.4 4.5 12MW-14 7/12/21 <1 NR NR 10 <1 NR NR <1 4.0 <10 NR <1 NR NR NR NR 47 5.9 52MW-14 10/14/20 2.5 NR NR 43 <1 NR NR <1 11 6.8 NR 1.6 NR NR NR NR 110 30 140MW-14 3/16/20 <1 <1 2.7 51 <1 5.7 2.0 <1 13 10 7.9 <1 <1 23 25 160 32 190MW-14 12/2/18 <10 NR NR 50 <10 NR NR <10 <30 <30 NR 25 NR NR NR NR 140 39 180 MW-15 10/5/23 <11 NR NR 12 J <7.2 NR NR 34 <2.4 NR NR <11 NR NR NR NR 37 27 J 64MW-15 7/21/22 26 D NR NR 14 D <2 NR NR 2.4 D 8 D NR NR 4.8 D NR NR NR NR 46 D 39 D 84 DMW-15 7/12/21 2.9 JD NR NR 11 D <5 NR NR 8.4 D 12 D <40 NR 12 D NR NR NR NR 48 D 29 D 78 D MW-15 10/14/20 23 NR NR 34 <1 NR NR 8.5 11 <200 NR 27 NR NR NR NR 180 110 290MW-15 7/5/19 9.8 NR NR 30 <1 NR NR 1.8 <100 <100 NR 15 NR NR NR NR 140 180 320MW-15 12/3/18 25 NR NR 150 <20 NR NR <20 28 JD 28 JD NR 66 NR NR NR NR 330 420 750 MW-16 10/5/23 <2.9 NR NR <2.3 <1.8 NR NR <1.3 1.4 J NR NR <2.9 NR NR NR NR 8.9 J <6.0 8.9 J MW-16 7/21/22 10 D NR NR 6.7 D <2 NR NR <2 5.3 D NR NR <2 NR NR NR NR 32 D 18 D 49 DMW-16 7/12/21 <20 NR NR 23 D <20 NR NR <20 24 D <100 NR 17 JD NR NR NR NR 73 D 46 D 120 DMW-16 10/14/20 47 NR NR 42 <10 NR NR <10 9.4 D 7.9 J NR 11 NR NR NR NR 120 62 180MW-16 3/16/20 11 JD <20 <20 14 JD <20 <20 <20 <20 8.4 JD <20 <20 <20 <20 <20 38 D 18 D 62 D 30 JD 92MW-16 12/3/18 <10 NR NR 59 <10 NR NR <10 <100 <100 NR <10 NR NR NR NR 190 210 400 MW-17 10/5/23 <11 NR NR 40 <7.2 NR NR 6.6 J 7.5 J NR NR 28 NR NR NR NR 130 120 250MW-17 7/21/22 5.8 D NR NR 56 D <5 NR NR <5 14 D ND NR 22 D NR NR NR NR 160 D 150 D 310 DMW-17 7/12/21 <20 NR NR 70 D <20 NR NR <20 24 D <50 NR 70 D NR NR NR NR 180 D 180 D 370 DMW-17 10/14/20 <5 NR NR 40 <5 NR NR <5 17 <200 NR 51 NR NR NR NR 130 130 260MW-17 7/5/19 14 NR NR 110 <5 NR NR <5 <100 <100 NR 68 NR NR NR NR 180 250 430MW-17 12/3/18 8.6 NR NR 240 <5 NR NR 4.8 <200 <200 NR 150 NR NR NR NR 460 670 1100 MW-18 10/5/23 <2.9 NR NR <2.3 <1.6 NR NR <1.3 <0.60 NR NR <2.9 NR NR NR NR <2.2 <6.0 <8MW-18 7/12/21 <1 NR NR <1 <1 NR NR <1 <1 <10 NR <1 NR NR NR NR <1 <2 <3MW-18 10/14/20 <1 NR NR <1 <1 NR NR <1 <1 <10 NR <1 NR NR NR NR <1 <2 <2 MW-18 3/16/20 <1 0.83 J NR 0.92 J <1 0.56 J <1 <1 0.49 J <10 0.70 J <1 <1 <1 3.4 2.2 2.1 2.0 4.1MW-18 7/5/19 <1 NR NR NR <1 NR NR <1 <10 <10 NR <1 NR NR NR NR 1.6 <2 2.3MW-18 12/2/18 <1 NR NR 3.3 <1 NR NR <1 <10 <10 NR <1 NR NR NR NR 8.8 6.8 16MW-18 12/5/17 33 NR NR 9.4 <1 NR NR 0.75 J 2.5 3.6 J NR 110 NR NR NR NR 18 43 62 MW-19 10/5/23 <5.7 NR NR 36 <3.6 NR NR <2.6 9.7 J NR NR <5.7 NR NR NR NR 100 64 160MW-19 7/21/22 <2 NR NR 7.8 D <2 NR NR <2 5.4 D NR NR 22 D NR NR NR NR 160 D 150 D 310 DMW-19 7/12/21 <1 NR NR 9.50 <1 NR NR <1 4.8 <10 NR <1 NR NR NR NR 56 18.00 74MW-19 10/14/20 <1 NR NR 36 <1 NR NR <1 14 9.3 NR 2.5 NR NR NR NR 170 60 230MW-19 7/5/19 3.3 NR NR 24 <1 NR NR <1 7.8 J 7.8 J NR 21 NR NR NR NR 120 42 160 MW-19 12/2/18 5.2 NR NR 46 <5 NR NR <5 11 JD 11 JD NR 24 NR NR NR NR 160 40 200 MW-20 10/5/23 <11 NR NR 67 <7.2 NR NR <5.2 17 J NR NR 28 NR NR NR NR 190 190 380MW-20 7/21/22 7.6 JD NR NR 140 D <10 NR NR <10 28 D NR NR 170 D NR NR NR NR 270 D 380 D 660 DMW-20 7/12/21 <5 NR NR 130 D <5 NR NR <5 22 D <50 NR 53 D NR NR NR NR 230 D 310 D 540 DMW-20 10/14/20 8.0 NR NR 120 <1 NR NR 1.4 27 <50 NR 53 NR NR NR NR 160 210 370MW-20 3/16/20 <20 16 JD <20 100 D <20 13 JD 16 JD <20 15 JD <20 26 D 9.8 JD <20 <20 160 D 49 D 160 D 200 D 360 DMW-20 12/2/18 17 NR NR 97 <2 NR NR <2 12 12 NR 14 NR NR NR NR 150 230 380MW-20 12/5/17 76 D NR NR 43 D <2 NR NR 4.3 D 12 D 12 NR 260 D NR NR NR NR 68 D 160 D 230 MW-21 10/5/23 <0.57 NR NR <0.46 <0.36 NR NR <0.26 <0.12 NR NR <0.57 NR NR NR NR <0.44 <1.2 <1.6 MW-21 7/12/21 <1 NR NR <1 <1 NR NR <1 <1 <10 NR <1 NR NR NR NR <1 <2 <3MW-21 10/14/20 <1 NR NR <1 <1 NR NR <1 <1 <10 NR <1 NR NR NR NR <1 <2 <2MW-21 3/16/20 <1 <1 NR <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 0.80 J <1 <1 0.40 J 0.40 JMW-21 12/2/18 <1 NR NR <1 <1 NR NR <1 <10 <10 NR <1 NR NR NR NR <1 <2 <2 NCAC 2L Standard (ug/L)1 70 70 600 70 70 25 20 6 6 70 600 3 2000 400 400 500 500 500NCDENR UST Section GCLs (ug/L)5,000 6,900 8,500 84,500 70,000 25,000 11,700 20,000 6,000 6,000 30,000 260,000 3,000 2,000,000 28,400 25,000 85,500 85,500 85,500 Note:Wells MW-1, MW-2, MW-3, MW-4, MW-7, MW-9, MW-12 to MW-17, MW-19 and MW-21 not sampled 12/5/17.All sample analytical concentrations are reported in ug/l.Bold depicts constiuents detected above the sample practical quantitation limit. SHADED AND BOLD numbers indicate concentrations above NCAC 2L Groundwater Quality Standard. GCL = gross contamination level.SHADED AND BOLD and RED numbers indicate concentrations above NCAC 2L Groundwater Quality Standard and NCDENR GCLs.NL = Not Listed.NR = Not Requested or Not reported by laboratory.0-xylenesM&P xylenesTotal XylenesTolueneTrichloroetheneTrichlorofluoro -methane1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneAnalytical Method Contaminant of Concern Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropyl EtherIsopropylbenzenep-IsopropyltolueneMethyl tertiary butyl ether (MTBE)NaphthaleneNaphthalenen-propylbenzene SEMINOLE MART NO 2CLES PROJECT NO 17-051A GROUNDWATER MONITORINBG REPORTOCTOBER 2023 EPA EPA EPA EPA EPA EPA SM EPA EPA SM SM SM 625 625 625 625 625 625 2540C-2011 365.4 300 4500S2 3500Fe 5310 D-2000 B-1997 B-2000 Well ID Date Sampled (m/dd/yy)Sulfde (mg/l)Ferrous Iron (mg/l)TOC (mg/l)MW-10 10/5/23 NR NR NR NR NR NR NR NR NR NR NR NRMW-10 7/21/22 NR NR NR NR NR NR NR NR NR NR NR NR MW-10 7/12/21 <25 <50 <50 <50 <50 <50 NR NR NR NR NR NRMW-10 10/14/20 <25 <50 <50 <50 <50 <50 NR NR NR NR NR NRMW-10 7/5/19 <50 <100 <100 <100 <100 <100 NR NR NR NR NR NRMW-10 12/3/18 50 <100 18 JD <100 <100 <100 170 NR NR NR NR NRMW-10 12/5/17 <5 <10 <10 <10 <10 <10 <50 <0.1 <5 <0.1 <0.05 2.6 MW-11 10/5/23 NR NR NR NR NR NR NR NR NR NR NR NRMW-11 7/21/22 NR NR NR NR NR NR NR NR NR NR NR NRMW-11 7/12/21 <25 <50 <50 <50 <50 <50 NR NR NR NR NR NRMW-11 10/14/20 <50 <100 <100 <100 <100 <100 NR NR NR NR NR NRMW-11 3/16/20 NR NR NR NR NR NR NR NR NR NR NR NRMW-11 12/3/18 <25 <50 <50 <50 <50 <50 160 NR NR NR NR NRMW-11 12/5/17 NR <84 NR NR NR 110 JD NR NR NR NR NR NR MW-12 10/5/23 NR NR NR NR NR NR NR NR NR NR NR NRMW-12 7/21/22 NR NR NR NR NR NR NR NR NR NR NR NR MW-12 7/12/21 NR NR NR NR NR NR NR NR NR NR NR NRMW-12 10/14/20 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NRMW-12 7/5/19 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NRMW-12 12/3/18 <25 <50 <50 <50 <50 <50 58 NR NR NR NR NR MW-13 10/5/23 NR NR NR NR NR NR NR NR NR NR NR NRMW-13 7/21/22 NR NR NR NR NR NR NR NR NR NR NR NRMW-13 7/12/21 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NRMW-13 10/14/20 <25 <50 <50 <50 <50 <50 NR NR NR NR NR NRMW-13 12/2/18 <15 <30 5.3 JD <30 <30 <30 190 NR NR NR NR NR MW-14 10/5/23 NR NR NR NR NR NR NR NR NR NR NR NRMW-14 7/21/22 NR NR NR NR NR NR NR NR NR NR NR NRMW-14 7/12/21 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NRMW-14 10/14/20 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NRMW-14 3/16/20 NR NR NR NR NR NR NR NR NR NR NR NRMW-14 12/2/18 <15 <30 <30 <30 <30 <30 150 NR NR NR NR NR MW-15 10/5/23 NR NR NR NR NR NR NR NR NR NR NR NRMW-15 7/21/22 NR NR NR NR NR NR NR NR NR NR NR NRMW-15 7/12/21 <40 <40 <40 <40 <40 <40 NR NR NR NR NR NR MW-15 10/14/20 <100 <200 <200 <200 <200 <200 NR NR NR NR NR NRMW-15 7/5/19 <50 <100 <100 <100 <100 <100 NR NR NR NR NR NRMW-15 12/3/18 <50 91 JD <100 <100 <100 <100 240 NR NR NR NR NR MW-16 10/5/23 NR NR NR NR NR NR NR NR NR NR NR NR MW-16 7/21/22 NR NR NR NR NR NR NR NR NR NR NR NRMW-16 7/12/21 <50 <100 <100 <100 <100 <100 NR NR NR NR NR NRMW-16 10/14/20 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NRMW-16 3/16/20 NR NR NR NR NR NR NR NR NR NR NR NRMW-16 12/3/18 <50 <100 <100 <100 19 JD 40 JD <50 NR NR NR NR NR MW-17 10/5/23 NR NR NR NR NR NR NR NR NR NR NR NRMW-17 7/21/22 NR NR NR NR NR NR NR NR NR NR NR NRMW-17 7/12/21 <25 <50 <50 <50 <50 <50 NR NR NR NR NR NRMW-17 10/14/20 <100 <200 <200 <200 <200 <200 NR NR NR NR NR NRMW-17 7/5/19 <50 <100 <100 <100 <100 <100 NR NR NR NR NR NRMW-17 12/3/18 <100 <200 <200 <200 <200 <200 300 NR NR NR NR NR MW-18 10/5/23 NR NR NR NR NR NR NR NR NR NR NR NRMW-18 7/12/21 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NRMW-18 10/14/20 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NR MW-18 3/16/20 NR NR NR NR NR NR NR NR NR NR NR NRMW-18 7/5/19 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NRMW-18 12/2/18 <5 <10 <10 <10 <10 <10 <50 NR NR NR NR NRMW-18 12/5/17 <5 <10 <10 <10 <10 <10 <50 <0.10 <5 <0.10 0.094 2.4 MW-19 10/5/23 NR NR NR NR NR NR NR NR NR NR NR NRMW-19 7/21/22 NR NR NR NR NR NR NR NR NR NR NR NRMW-19 7/12/21 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NRMW-19 10/14/20 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NRMW-19 7/5/19 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NR MW-19 12/2/18 <25 <50 <50 <50 <50 <50 170 NR NR NR NR NR MW-20 10/5/23 NR NR NR NR NR NR NR NR NR NR NR NRMW-20 7/21/22 NR NR NR NR NR NR NR NR NR NR NR NRMW-20 7/12/21 <25 <50 <50 <50 <50 <50 NR NR NR NR NR NRMW-20 10/14/20 <25 <50 <50 <50 <50 <50 NR NR NR NR NR NRMW-20 3/16/20 NR NR NR NR NR NR NR NR NR NR NR NRMW-20 12/2/18 <10 <10 <10 <10 <10 <10 <50 NR NR NR NR NRMW-20 12/5/17 <5 90 <10 <10 <10 <10 <50 <0.10 <5 <0.10 <0.05 1.5 MW-21 10/5/23 NR NR NR NR NR NR NR NR NR NR NR NR MW-21 7/12/21 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NRMW-21 10/14/20 <5 <10 <10 <10 <10 <10 NR NR NR NR NR NRMW-21 3/16/20 NR NR NR NR NR NR NR NR NR NR NR NRMW-21 12/2/18 <5 <10 <10 <10 <10 <10 <50 NR NR NR NR NR NCAC 2L Standard (ug/L)3 6000 100 NL 200 200 500000NCDENR UST Section GCLs (ug/L)170 NL 100,000 NL 410 200 NL Note:Wells MW-1, MW-2, MW-3, MW-4, MW-7, MW-9, MW-12 to MW-17, MW-19 and MW-21 not sampled 12/5/17.All sample analytical concentrations are reported in ug/l.Bold depicts constiuents detected above the sample practical quantitation limit. SHADED AND BOLD numbers indicate concentrations above NCAC 2L Groundwater Quality Standard. GCL = gross contamination level.SHADED AND BOLD and RED numbers indicate concentrations above NCAC 2L Groundwater Quality Standard and NCDENR GCLs.NL = Not Listed.NR = Not Requested or Not reported by laboratory.Sulfate - SO4 (mg/l)Contaminant of Concern Bis(2-ethylhexyl)phthalateAnalytical Method GEOCHEMICAL PARAMETERSDiethylphthalate2,4-Dimethylphenol2,4-DinitrophenolPhenanthrenePyreneTDSPhosphorous (mg/l) SEMINOLE MART 2 CLES PROJECT NO 17-051A GROUNDWATER MONITORING REPORT OCTOBER 2023 TABLE 6GROUNDWATER ANALYTICAL RESULTS SEMNOLE MART NO. 2 691 SEMINOLE ROAD BROADWAY. HARNETT COUNTY, NORTH CAROLINA NCDENR INCIDENT NO. 42025NCDEQ UST SECTION FACILITY ID. 0-000014231 CLES PROJECT NO. 17-051 EPA EPA EPA EPA EPA EPA EPA EPA EPA 624 624 624 8260 624 624 624 624 624 Well ID Date Sampled (m/dd/yy)MW-1 10/5/23 72 150 <3.6 <2.6 21 370 340 470 810 MW-4 10/5/23 <5.7 <4.6 <3.6 <2.6 <1.2 <5.7 15 <12 <16 MW-5 10/5/23 <0.57 <0.46 <0.36 <0.26 <0.12 <0.57 <0.44 <1.2 <1.6 MW-6 10/5/23 <0.57 <0.46 <0.36 <0.26 <0.12 <0.57 <0.44 <1.2 <1.6 MW-7 10/5/23 <0.57 <0.46 <0.36 <0.26 <0.12 <0.57 <0.44 <1.2 <1.6 MW-8 10/5/23 <11 59 <7.2 26.0 33 <11 210 120 330 MW-9 10/5/23 20 <4.6 <3.6 <2.6 <1.2 <5.7 44 22 66 MW-10 10/5/23 28 68 <7.2 <5.2 17 J 34 140 170 310 MW-11 10/5/23 19 110 <3.6 13 21 120 280 340 620 MW-12 10/5/23 <5.7 18 <3.6 <2.6 5.1 J <5.7 77 53 130 MW-13 10/5/23 <5.7 61 <3.6 9.4 J 11 25 120 190 310 MW-14 10/5/23 <2.9 <2.3 <1.8 <1.3 2.7 J <2.9 32 18 50 MW-15 10/5/23 <11 12 J <7.2 34 <2.4 <11 37 27 J 64 MW-16 10/5/23 <2.9 <2.3 <1.8 <1.3 1.4 J <2.9 8.9 J <6.0 8.9 J MW-17 10/5/23 <11 40 <7.2 6.6 J 7.5 J 28 130 120 250 MW-18 10/5/23 <2.9 <2.3 <1.6 <1.3 <0.60 <2.9 <2.2 <6.0 <8 MW-19 10/5/23 <5.7 36 <3.6 <2.6 9.7 J <5.7 100 64 160 MW-20 10/5/23 <11 67 <7.2 <5.2 17 J 28 190 190 380 MW-21 10/5/23 <0.57 <0.46 <0.36 <0.26 <0.12 <0.57 <0.44 <1.2 <1.6 NCAC 2L Standard (ug/L)1 600 70 20 6 600 500 500 500NCDENR UST Section GCLs (ug/L)5,000 84,500 70,000 20,000 6,000 260,000 85,500 85,500 85,500 Note: Wells MW-1, MW-2, MW-3, MW-4, MW-7, MW-9, MW-12 to MW-17, MW-19 and MW-21 not sampled 12/5/17. All sample analytical concentrations are reported in ug/l. Bold depicts constiuents detected above the sample practical quantitation limit. SHADED AND BOLD numbers indicate concentrations above NCAC 2L Groundwater Quality Standard.GCL = gross contamination level. SHADED AND BOLD and RED numbers indicate concentrations above NCAC 2L Groundwater Quality Standard and NCDENR GCLs. NL = Not Listed. NR = Not Requested or Not reported by laboratory.0-xylenesM&P xylenesTotal XylenesAnalytical Method Contaminant of Concern BenzeneTolueneEthylbenzeneIsopropyl EtherMethyl tertiary butyl ether (MTBE)Naphthalene FIGURES Figure 1: Vicinity Map Figure 2: Site Map Figure 3: Groundwater Potentiometric Map (July 21, 2022) Figure 4: Groundwater Constituent Concentrations (July 28, 2022) Figure 5: Pre-Remedial Benzene Isoconcentration Map (November 1, 2017) Figure 6: Benzene Isoconcentration Map (July 21, 2022) ) 0.3 miles Source: https://apps.nationalmap.gov/downloader/#/startUp North Job No.: Scale: Date: Fig. No.: Broadway, North Carolina 8005 Clear Brook Drive Raleigh, NC 27615 17-051A October 5, 2023 VICINITY MAP Seminole Mart No. 2 As Shown 691 Seminole Road 1 SITE Source: East Coast Environmental, PA CAP 11/1/17 Job No.: Scale: Date: Fig. No.: Broadway, North Carolina Raleigh, NC 27615 SITE MAP October 5, 2023 17-051A As Shown Seminole Mart No. 2 691 Seminole Road 8005 Clear Brook Drive 2Assumed North Base Map Source: East Coast Environmental, PA CAP 11/1/17 Job No.: Scale: Date: Fig. No.: GROUNDWATER 17-051A POTENTIOMETRIC MAP (10-5-23)As Shown Seminole Mart No. 2 October 23, 2023 691 Seminole Road 8005 Clear Brook Drive 3Broadway, North Carolina Raleigh, NC 27615LEGENDApproximate Monitor Well LocationNote: Measurements fromMW-1, MW-2 Aand MW-3not considered in groundwater contours.(50.10) Groundwater Elevation (Ft) 10-5-23 Top of casing elevations reported by by East Coast Environmental, PA. 51.00Groundwater Elevation Contour (Ft)Elevation units in feet relativeto an assigned elevation of an on-site benchmark.0.0078Groundwater Flow Direction and(50.30)(50.38)(50.33)(49.68)(50.13)(50.17)(50.13)(50.27)(50.24)(50.32)(50.18)(50.27)(50.39)(50.44)(50.45)(50.51)(50.49(50.41)(49.38)*(50.06)(57.98)50.0050.00Assumed 0.0078 MW-12 Ethylbenzene 18Toluene19o-xylenes 77m,p-xylenes 53Naphthalene5.1 J MW-13Ethylbenzene 61 MTBE 9.4 JToluene 25 o-xylenes 120m,p xylenes 190 MW-15 Ethylbenzene 12JMTBE34o-xylenes 37m,p-xylenes 27 J MW-17 Ethylenzene 40 MTBE 6.6 JToluene28o-xylenes 130m,p-xylenes 120 GROUNDWATER CONSTITUENTCONCENTRATION MAPOCTOBER 5, 2023SEMINOLE MART NO. 2691 SEMINOLE ROADBROADWAY, NORTH CAROLINADATE: OCTOBER 25, 2023Note:Samples collected on October 5, 2023.Constiuent concentrations in micrograms per liter (ug/L).Source Map: East Coast Environmental, PA CAP 11/1/17 MW-10 Benzene 28 Ethylbenzene 68 Toluene 34o-xylenes 140m,p-xylenes 170Naphthalene17 J MW-19 Ethylbenzene 36o-xylenes 100m,p-xylenes 64Naphthalene9.7 J SCALE:AS SHOWNMW-6 None Detected MW-7 None Detected MW-8Ethylbenzene 59 MTBE 26o-xylenes 210 m,p-xylenes 120 Naphthalene 33 MW-18 NoneDetected MW-9 Benzene 20 o-xylenes 44m,p-xylenes 22 MW-20 Ethylbenzene 67 Toluene 28 o-xylenes 190m,p-xylenes 190Naphthalene17J MW-21 None DetectedMW-1Benzene 72 Ethylbenzene 150 Toluene 370 o-xylenes 340m,p-xylenes 470 Naphthalene 21 MW-11 Benzene 19MTBE13Ethylbenzene110 Toluene 120o-xylenes 280m,p-xylenes 340 Naphthalene 21 MW-2 MW-4 o-xylenes 15 MW-5 NoneDetected 8005 CLEAR BROOK DRIVERALEIGH, NC 27615PROJECT NO.: 17-MW-14 o-xylenes 32 m,p-xylenes 18 Naphthalene 2.7 J MW-16Naphthalene 1.4 Jo xylenes 8.9 J MW-3 Not Sampled Map Source: East Coast Environmental, PA CAP 11/1/17 Job No.: Scale: Date: Fig. No.: PREREMEDIAL BENZENE ISONCENTRATION MAP 17-051A (NOVEMBER 1, 2017)As Shown Seminole Mart No. 2 October 25, 2023 5691 Seminole Road 8005 Clear Brook Drive Broadway, North Carolina Raleigh, NC 27615 Assumed Base Map Source: East Coast Environmental, PA CAP 11/1/17 Job No.: Scale: Date: Fig. No.: BENZENE CONCENTRATIONS 17-051A (October 5, 2023)As Shown Seminole Mart No. 2 October 25, 2022 691 Seminole Road 8005 Clear Brook Drive 6Broadway, North Carolina Raleigh, NC 27615 (437.16) (438.79) (437.23) (435.17) (436.06) (435.07) (437.03) (437.23) (436.81) (437.16) (437.15)(436.89) (436.48) (437.23)* (437.08) LEGEND Approximate Monitor Well Location (64) Benzene concentration in groundwater in micrograms per liter (ug/L) from samples collected 10-5-23. 0.73 Free Product Thickness (Ft) on groundwater measured 10-5-23. Benzene concentrations above the 15A NCAC 2L Groundwater Quality Standard (1.0 ug/l). (Based on previous detections with lower detection levels.) Approximate area with measurable thickness (0.01 FT.) or more of Free Product on the groundwater table. (<1.0) Benzene concentrations below the sample method reporting limit. (437.33)* Abandoed Abandoned Abandoned (72)0.03(NS)0.7(NS)1.2(<5.7)<0.01(<0.57)(20)<0.01(<0.57)<0.01(<0.57)(<11)0.03(19)0.3(<2.9)<0.01(<5.7)<0.01(<11)<0.01(<1.0)<0.01(<5.7)(<2.9)<0.01(<0.57)<0.01(<11)<0.01(<5.7)<0.01(<11)0.01Assumed North1.0 UG/L 0.01(28)0.03 APPENDICES Appendix I Standard Operating Procedures Appendix II Calculations Appendix III Laboratory Analytical Results and Chain of Custody Forms APPENDIX I Standard Operating Procedures STANDARD OPERATING PROCEDURES Soil Sampling, Soil Boring and Monitor Well Installation, Well Development Soil borings are completed with a stainless steel hand auger, direct-push hydraulic drill or auger rotary drill using either a macro core sampler, 3-1/4, 4-1/4, or 6-1/4-inch inside diameter hollow stem augers. Soil borings are typically sampled at discrete intervals from the bucket of a clean stainless steel hand auger, direct push stainless steel sampler with acetate sleeve, or a split barrel sampler. Monitor wells are completed in selected soil borings using one, two, or four-inch inside diameter PVC casing and machine slotted screen intervals in accordance with North Carolina guidelines. Clean quartz sand is typically used to fill the boring annulus around the well screen to approximately one foot above the screened interval, approximately one foot of hydrated bentonite is placed over the sand pack and neat cement grout or bentonite is placed above the well seal. Concrete is placed to secure the wellhead in the top three feet of boring annulus. Wellheads may be completed with either flush mounted traffic-bearing protectors with bolt down covers or steel above-ground protectors set in a concrete pad. Temporary wells or piezometers may be completed with the PVC riser cut at or above grade. The wellheads are secured with locking caps. Wells may be developed using a bailer, electric submersible pump, pneumatic pump, or peristaltic pump. When wells are developed by the driller, they may be developed with air injection, water injection, pumping or bailing. Soil boring logs and well construction details are typically prepared for presentation in a report appendix. Borings completed in bedrock may be drilled using air rotary, coring, or sonic drilling methods. Liquid Levels Groundwater level measurements are typically obtained using an electronic sounding/interface detection device which registers a tone or illuminated light when a probe makes contact with the groundwater. Depth to groundwater measurements are obtained by lowering a probe attached to a cable marked in 0.01 feet intervals into the well until the probe of the meter intersects the product or water surface. The measurement from the top of the riser pipe or top of casing (T.O.C.) to the liquid level is recorded. The measurement is recorded to the nearest 0.01 foot. The electronic interface probe is decontaminated between measurement locations. LNAPL Measurements Light Non-Aqueous Phase Liquid (LNAPL) present on the water table is measured using an oil/water interface probe. The electronic meter has both an audible and illuminating light that indicate when a liquid level is encountered. The oil/water interface probe registers a solid tone/light when LNAPL petroleum product is encountered and a beeping tone/light when groundwater is encountered. Depth to LNAPL measurements are obtained by lowering a probe attached to a cable marked in 0.01 feet intervals into the well until the probe of the meter intersects the product or groundwater. The measurements from the top of the riser pipe or top of casing (T.O.C.) to the liquid level is recorded. The measurement is recorded to the nearest 0.01 foot. The thickness of LNAPL is calculated by subtracting the depth to LNAPL measurement from the depth to groundwater measurement. The electronic interface probe is decontaminated between measurement locations. Soil Sampling Soil sampling is performed in general accordance with ASTM: 1586-84 where applicable. Sampling procedures are followed to protect the chemical integrity of the soil samples and minimize the potential for cross contamination. This includes discarding of the exterior of the sample which contacts the auger bucket, acetate sleeve, or split barrel sampler, collecting the interior soil for screening with the PID or FID, and either pressure washing, steam cleaning, or washing with non-phosphate detergent and/or rinsing sampling equipment with clean water between sampling intervals. The samples are placed in glass jars, sealed, and placed in an ice filled cooler. An aliquot of the sample is typically placed in a clean sealable bag and allowed to reach ambient air temperature. The PID or FID is used to measure total organic vapors (TOV) in the head space in each sample bag. Excavation soil samples may also be collected from the bucket of excavation equipment. Care to collect soil samples from excavation equipment includes retrieving native soil from material that has not made contact with the excavating equipment. Samples are collected in sealable bags or by directly filling sample containers using new gloves, laboratory provided sampling utensils, or decontaminated stainless steel sampling equipment. Field personnel don new, unused, disposable nitrile gloves at soil boring and sampling locations. Gloves are changed between each sample interval. Sampling equipment such as hand auger extensions and buckets, direct push samplers, split spoons and/or drilling augers, are decontaminated before collecting samples. Groundwater Sampling Bailer or Dedicated Pump Groundwater samples are collected using new dedicated polyethylene bailers or dedicated pump with polyethylene tubing (or equal) at each monitor well. Before obtaining a sample, a minimum of three well volumes of groundwater is typically evacuated from the well to ensure collection of a sample representative of the in-situ groundwater conditions. Field parameters (not limited to pH, specific conductance and temperature) are measured on purged groundwater after each volume approximately equal to one water column in the well is evacuated to monitor the changes of the field parameters in the groundwater as the monitor wells are purged. Once the fluctuation of field parameters stabilizes to within ten percent over three consecutive purge parameter measurements, or after the well is purged dry and allowed to recover, the record sample is collected. The groundwater samples are collected by directly filling laboratory-supplied containers with groundwater poured directly from the dedicated disposable bailer or polyethylene tubing attached to the dedicated well pump. Samples will be then transferred to insulated containers with ice for transport to the laboratory. Field personnel don clean chemical resistant/non-reactive gloves at each well during purging and don a new pair of gloves before filing sample containers. Peristaltic Pump (Low Flow Method) Groundwater is purged from the monitor wells using a peristaltic pump with either dedicated Teflon-lined or PVC tubing inserted into the well, or using a clean section of disposable silicon and a clean section of PVC tubing inserted into the well by the following low flow sampling methods. The silicon tubing is inserted into the peristaltic pump. The silicon is attached to the PVC or Teflon-lined tubing that is inserted into the monitor well to the bottom of the well screen. The tubing is pulled back off of the bottom of the well with the end located within the screened interval of the well and the peristaltic pump is started. The initial flow from the well that passes through the peristaltic pump tubing is discharged into a bucket or container. Once the initial turbid liquid effluent becomes relatively clear (lower turbidity) the effluent may be passed through a flow cell for parameter measurements or captured in a container so that a multi meter can be used to monitor field parameters. This minimizes potential fowling of the flow cell and meters used to monitor field parameters. Field parameters will be measured on groundwater purged from each well to monitor the changes of the field parameters in the groundwater as the monitor wells will be purged. Field parameters will be recorded after approximately each consecutive two minutes of pumping from the peristaltic pump. Once the fluctuation of field parameters stabilizes at each well to within ten percent over three consecutive measurements, the record sample is collected. If the well is purged dry, it is allowed to recharge sufficiently for a sample to have be collected. Samples will then be transferred directly from the section of silicon tubing into containers supplied by the laboratory. Field personnel don clean chemical resitant/non-reactive gloves at each well during purging and before sampling activities. Decontamination Procedures The potential for cross-contamination between sample locations is minimized by thoroughly cleaning the sampling equipment, both prior to the initiation of sampling and between uses. Glass and Teflon® sampling equipment, in-situ hydraulic conductivity measurement equipment, bucket augers and split-spoon samplers used for soil sampling, and other tools and equipment will be decontaminated between each use according to the following procedures: • Remove excess soil/sludge as necessary. • Wash and scrub the equipment with a phosphate-free detergent in a hot tap water (prior to field use) or ambient tap water solution. Use a brush to remove particulate matter and surface films. Repeat as necessary. • Rinse thoroughly with tap water. • Rinse thoroughly with analyte-free water (deionized water). • Allow the equipment to air dry. • Prevent inadvertent contamination during storage and transport. All personnel engaged in equipment decontamination wear clean, disposable chemical resistant non-reactive gloves. Aquifer Testing Procedures Aquifer hydraulic conductivity testing is performed at selected wells to evaluate the relative hydraulic conductivity at targeted locations. Rising head slug tests will be performed at target monitor well/piezometer locations. Prior to performing the tests, the monitor wells/piezometers will be opened and allowed to equilibrate. The water level in each well/piezometer is measured to the nearest 0.01 feet using a decontaminated water level probe. This reading is used as the initial reading for the tests. Slug tests will be performed in the monitor wells/piezometers by installing into the monitor well a pressure transducer equipped with a data recorder or that is attached to a data recorder. After obtaining an initial water level reading, a clean polyethylene bailer of known volume is submerged in the water in the well/piezometer. The filled bailer is removed and the water level in the well/piezometer is monitored with the pressure transducer as the water level in the well/piezometer returned to static conditions. The volume of water removed by the bailer is noted. Tests may be repeated on or more times in each test well/piezometer. The transducer data is graphically evaluated in the field using Win-Situ (or equal) computer software. The Win-Situ data is imported into an MS Excel® Workbook for analysis by Bouwer-Rice techniques for partially or fully penetrating well screens using Aqtesolv® computer software. The Bouwer-Rice techniques make a variety of simplifying assumptions in the evaluation of slug test data. These include the assumptions that the aquifer in question is homogenous, isotropic, and extends infinitely in the horizontal direction (Bouwer-Rice, 1976). APPENDIX II Calculations Groundwater Sampling Form - Cape Lookout Environmental Sciences, PLLC Client:CLES Project No.: Wind Speed: 0-10 mph Direction From: SSW Site Name:Temperature oF Low: 70 High: 90 Site Address:Cloud Cover: 10 % Rain: 0 inches Well ID / Diameter Collection Order 21 18 19 11 5 Total Well Depth (ft) Depth to Product Depth to Water (ft) Water Column (ft) Well Volume (X3) Product thickness Purge Time Interval Temp. oC v1 19.1 v4 v1 v4 v1 v4 v1 18.7 v4 v1 17.6 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Barometric pressure mmHgv1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 DO %v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 DO mg/L v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Conductivity mS/cm v1 0.30 v4 v1 v4 v1 v4 v1 0.2 v4 v1 0.07 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 pH v1 6.5 v4 v1 v4 v1 v4 v1 6.5 v4 v1 6.5 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 pH mV v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 ORP v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Purge Rate In. Fin.In. Fin.In. Fin.In. Fin.In. Fin. Final Dissolved O2 mg/L oC mg/L oC mg/L oC mg/L oC mg/L oC Final Turbidity (ntu) Well Condition Date/Time Collected 10/5/23 1435 10/5/23 1205 10/5/23 1120 Preservative HCL Nitric HCL Nitric HCL Nitric HCL Nitric HCL Nitric Sampler's Name: Comments:cloudy cloudy cloudycloudy clear 0.00 0.00 0.00 0.00 0.00 40 45 45 45 48 19.6 22.0 22.0 22.0 23.5 MW-4 MW-5 40 45 45 45 48 Scott Yow 17-051A Seminole Mart 691 Seminole Road MW-1 MW-2 MW-3 Groundwater Sampling Form - Cape Lookout Environmental Sciences, PLLC Client:CLES Project No.: Wind Speed: 0-10 mph Direction From: SSW Site Name:Temperature oF Low: 70 High: 90 Site Address:Cloud Cover: 10 % Rain: 0 inches Well ID / Diameter Collection Order 3 4 13 20 15 Total Well Depth (ft) Depth to Product Depth to Water (ft) Water Column (ft) Well Volume (X3) Product Thickness Purge Time Interval Temp. oC v1 17.4 v4 v1 17.5 v4 v1 19.4 v4 v1 18.2 v4 v1 18.1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Barometric pressure mmHgv1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 DO %v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 DO mg/L v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Conductivity uS/cm v1 0.04 v4 v1 0.08 v4 v1 0.22 v4 v1 0.12 v4 v1 0.11 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 pH v1 6.00 v4 v1 6.00 v4 v1 6.00 v4 v1 6.00 v4 v1 6.50 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 pH mV v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 ORP v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Purge Rate In. Fin.In. Fin.In. Fin.In. Fin.In. Fin. Final Dissolved O2 mg/L oC mg/L oC mg/L oC mg/L oC mg/L oC Final Turbidity (ntu) Well Condition Date/Time Collected 10/5/23 1120 10/5/23 1130 10/5/23 1350 10/5/23 240 10/5/23 1410 Preservative HCL Nitric HCL Nitric HCL Nitric HCL Nitric HCL Nitric Sampler's Name: Comments: 0.00 0.00 0.00 0.00 0.00 48 48 50 50 50 23.5 23.5 24.5 24.5 24.5 MW-6 MW-7 MW-8 MW-9 MW-10 48 48 50 50 50 Scott Yow 17-051A Seminole Mart 691 Seminole Road Groundwater Sampling Form - Cape Lookout Environmental Sciences, PLLC Client:CLES Project No.: Wind Speed: 0-10 mph Direction From: SSW Site Name:Temperature oF Low: 70 High: 90 Site Address:Cloud Cover: 10 % Rain: 0 inches Well ID / Diameter Collection Order 16 8 12 6 9 Total Well Depth (ft) Depth to Product Depth to Water (ft) Water Column (ft) Well Volume (X3) Product Thickness Purge Time Interval Temp. oC v1 18.1 v4 v1 18 v4 v1 17.9 v4 v1 18 v4 v1 18.5 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Barometric pressure mmHgv1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 DO %v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 DO mg/L v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Conductivity uS/cm v1 0.19 v4 v1 0.09 v4 v1 0.17 v4 v1 0.07 v4 v1 0.19 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 pH v1 6.5 v4 v1 6.6 v4 v1 6 v4 v1 6.6 v4 v1 6.5 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 pH mV v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 ORP v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Purge Rate In. Fin.In. Fin.In. Fin.In. Fin.In. Fin. Final Dissolved O2 mg/L oC mg/L oC mg/L oC mg/L oC mg/L oC Final Turbidity (ntu) Well Condition Date/Time Collected 10/5/23 1435 10/5/23 1200 10/5/23 1150 10/5/23 1215 10/5/23 1355 Preservative HCL Nitric HCL Nitric HCL Nitric HCL Nitric HCL Nitric Sampler's Name: Comments: 0.00 0.00 0.00 0.00 0.00 50 50 50 50 50 24.5 24.5 24.5 24.5 24.5 MW-11 MW-12 MW-13 MW-14 MW-15 50 50 50 50 50 Scott Yow 17-051A Seminole Mart 691 Seminole Road Groundwater Sampling Form - Cape Lookout Environmental Sciences, PLLC Client:CLES Project No.: Wind Speed: 0-10 mph Direction From: SSW Site Name:Temperature oF Low: 70 High: 90 Site Address:Cloud Cover: 10 % Rain: 0 inches Well ID / Diameter Collection Order 10 14 2 7 17 Total Well Depth (ft)Depth to Product/1st liquid Depth to Water (ft) Water Column (ft) Well Volume (X3) Product Thickness Purge Time Interval Temp. oC v1 17.5 v4 v1 18.6 v4 v1 17.5 v4 v1 17.7 v4 v1 17.7 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Barometric pressure mmHgv1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 DO %v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 DO mg/L v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Conductivity uS/cm v1 0.19 v4 v1 0.19 v4 v1 0.05 v4 v1 0.25 v4 v1 0.19 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 pH v1 6.00 v4 v1 6.50 v4 v1 6.50 v4 v1 6.00 v4 v1 7.00 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 pH mV v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 ORP v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Purge Rate In. Fin.In. Fin.In. Fin.In. Fin.In. Fin. Final Dissolved O2 mg/L oC mg/L oC mg/L oC mg/L oC mg/L oC Final Turbidity (ntu) Well Condition Date/Time Collected 10/5/23 1225 10/5/23 1405 10/5/23 1140 10/5/23 1225 10/5/23 1240 Preservative HCL Nitric HCL Nitric HCL Nitric HCL Nitric HCL Nitric Sampler's Name: Comments: 0.00 0.00 0.00 0.00 0.00 50 50 45 45 48 24.5 24.5 22.0 22.0 23.5 MW-16 MW-17 MW-18 MW-19 MW-20 50 50 45 45 48 Scott Yow 17-051A Seminole Mart 691 Seminole Road Groundwater Sampling Form - Cape Lookout Environmental Sciences, PLLC Client:CLES Project No.: Wind Speed: 0-10 mph Direction From: SSW Site Name:Temperature oF Low: 70 High: 90 Site Address:Cloud Cover: 10 % Rain: 0 inches Well ID / Diameter Collection Order 1 Total Well Depth (ft)Depth to Product Depth to Water (ft) Water Column (ft) Well Volume (X3) Product ThicknessPurge Time Interval Temp. oC v1 18.2 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Barometric pressure mmHgv1 v4 v1 v4 v1 v4 v1 v4 v1 v4v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 DO %v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 DO mg/L v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Conductivity uS/cm v1 0.001 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 pH v1 6.00 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 pH mV v1 v4 v1 v4 v1 v4 v1 v4 v1 v4v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 ORP v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Purge Rate In. Fin.In. Fin.In. Fin.In. Fin.In. Fin. Final Dissolved O2 mg/L oC mg/L oC mg/L oC mg/L oC mg/L oC Final Turbidity (ntu) Well Condition Date/Time Collected 10/5/23 1055 Field Calibration Date/Time:Date/Time:Date/Time:Date/Time:Date/Time:pH 4 7 10 pH pH pH pH C 1413 C C C C DO DO DO DO DO Tur.Tur.Tur.Tur.Tur. Preservative HCL Nitric HCL Nitric Sampler's Name: Comments: 24.5 0.00 0.00 0.00 0.00 0.00 50 0 0 0 0 50 MW-21 Scott Yow 17-051A Seminole Mart 691 Seminole Road SEMINOLE MART NO 2 CLES PROJECT 17-051A GROUNDWATER MONITORING REPORT OCTOBER 2023 HYDRAULIC GRADIENT CALCULATIONS - OCTOBER 5, 2023 SEMINOLE MART NO. 2 691 SEMINOLE ROAD, BROADWAY, NC Purpose: To determine the hydraulic gradient Given: Gradient (a) CALCULATED FROM THREE POINT SOLUTION GRADIENT (a): i = h1 – h2 distance WHERE DISTANCE BETWEEN h1 AND h2 IS PARALLEL TO FLOW DETERMINED FROM 3 POINT PROBLEM BY PROJECTION i2 = MW-5-MW-21=50.44 -49.68 =0.0060 distance Calculate Distance for point with Elevation = MW-20 between MW-5 and MW-21 MW-5 - MW-20 = 50.44 -50.13 =51.39 0.0060 Place point on line 51.39 feet from MW-5 toward MW-21, Draw line from point to MW-20 51.39 feet from MW-5. Project MW-5 and MW-21 locations onto perpendicular line and measure new distance between projected well locations. Gradient (a): divide change in head between MW-5 to MW-21 and divide by new distance to predict gradient. MW-5- MW-21 = 50.44 -49.68 =0.0078 north-northeast flow New Distance 97.63 CLES Project No. 17-051A USING MONITOR WELLS MW-5, MW-20 and MW-21 126 0.0060 Draw line perpendicular to line drawn between MW-20 and Point APPENDIX III Laboratory Analytical Results and Chain of Custody Forms ANALYTICAL REPORT PREPARED FOR Attn: David Wells Cape Lookout Environmental Services 8005 Clear Brook Drive Raleigh, North Carolina 27615 Generated 10/20/2023 10:09:09 AM JOB DESCRIPTION Cape Lookout- Seminole Mart #2 JOB NUMBER 752-12339-1 See page two for job notes and contact information. Cary NC 27511 102-A Woodwinds Industrial Court Eurofins Raleigh Page 1 of 33 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Eurofins Raleigh Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies Job Notes This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project Manager. Authorization Generated 10/20/2023 10:09:09 AM Authorized for release by Amanda Gaines, Project Manager amanda.gaines@et.eurofinsus.com (919)677-1669 Page 2 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Table of Contents Client: Cape Lookout Environmental Services Project/Site: Cape Lookout- Seminole Mart #2 Laboratory Job ID: 752-12339-1 Page 3 of 33 Eurofins Raleigh10/20/2023 Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3 Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5 Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9 Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .18 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .19 QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24 Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .25 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .28 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .29 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .30 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .31 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .33 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Definitions/Glossary Job ID: 752-12339-1Client: Cape Lookout Environmental Services Project/Site: Cape Lookout- Seminole Mart #2 Qualifiers GC/MS VOA Qualifier Description *3 ISTD response or retention time outside acceptable limits. Qualifier J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Glossary These commonly used abbreviations may or may not be present in this report. ¤Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level" MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present PQL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins Raleigh Page 4 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Case Narrative Client: Cape Lookout Environmental Services Job ID: 752-12339-1 Project/Site: Cape Lookout- Seminole Mart #2 Job ID: 752-12339-1 Laboratory: Eurofins Raleigh Narrative Job Narrative 752-12339-1 Analytical test results meet all requirements of the associated regulatory program listed on the Accreditation/Certification Summary Page unless otherwise noted under the individual analysis. Data qualifiers are applied to indicate exceptions. Noncompliant quality control (QC) is further explained in narrative comments. Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted. In these situations, to demonstrate precision and accuracy at a batch level, a LCS/LCSD may be performed, unless otherwise specified in the method. Surrogate and/or isotope dilution analyte recoveries (if applicable) which are outside of the QC window are confirmed unless attributed to a dilution or otherwise noted in the narrative. Regulated compliance samples (e.g. SDWA, NPDES) must comply with the associated agency requirements/permits. Receipt The samples were received on 10/5/2023 3:49 PM. Unless otherwise noted below, the samples arrived in good condition, and, where required, properly preserved and on ice. The temperature of the cooler at receipt time was 2.0°C GC/MS VOA Method 624.1_PREC: The following samples were diluted due to the nature of the sample matrix: MW-9 (752-12339-7), MW-10 (752-12339-8), MW-11 (752-12339-9), MW-12 (752-12339-10), MW-13 (752-12339-11), MW-14 (752-12339-12), MW-15 (752-12339-13), MW-16 (752-12339-14), MW-17 (752-12339-15), MW-18 (752-12339-16), MW-19 (752-12339-17), MW-20 (752-12339-18) and MW-21 (752-12339-19). Elevated reporting limits (RLs) are provided. Method 624.1_PREC: The following samples were diluted due to the nature of the sample matrix: MW-14 (752-12339-12), MW-16 (752-12339-14), MW-18 (752-12339-16), MW-19 (752-12339-17) and MW-21 (752-12339-19). Elevated reporting limits (RLs) are provided. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Eurofins RaleighPage 5 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Detection Summary Job ID: 752-12339-1Client: Cape Lookout Environmental Services Project/Site: Cape Lookout- Seminole Mart #2 Client Sample ID: MW-1 Lab Sample ID: 752-12339-1 Benzene RL 10 ug/L MDL 5.7 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA1072624.1 Toluene 10 ug/L5.7 Total/NA10370624.1 Ethylbenzene 10 ug/L4.6 Total/NA10150624.1 m-Xylene & p-Xylene 20 ug/L12 Total/NA10470624.1 Xylenes, Total 30 ug/L16 Total/NA10810624.1 Naphthalene 10 ug/L1.2 Total/NA1021624.1 o-Xylene 10 ug/L4.4 Total/NA10340624.1 Client Sample ID: MW-4 Lab Sample ID: 752-12339-2 o-Xylene RL 10 ug/L MDL 4.4 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA1015624.1 Client Sample ID: MW-5 Lab Sample ID: 752-12339-3 No Detections. Client Sample ID: MW-6 Lab Sample ID: 752-12339-4 No Detections. Client Sample ID: MW-7 Lab Sample ID: 752-12339-5 No Detections. Client Sample ID: MW-8 Lab Sample ID: 752-12339-6 Ethylbenzene RL 20 ug/L MDL 9.2 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA2059624.1 m-Xylene & p-Xylene 40 ug/L24 Total/NA20120624.1 Methyl tert-butyl ether 20 ug/L5.2 Total/NA2026624.1 Xylenes, Total 60 ug/L32 Total/NA20330624.1 Naphthalene 20 ug/L2.4 Total/NA2033624.1 o-Xylene 20 ug/L8.8 Total/NA20210624.1 Client Sample ID: MW-9 Lab Sample ID: 752-12339-7 Benzene RL 10 ug/L MDL 5.7 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA1020624.1 m-Xylene & p-Xylene 20 ug/L12 Total/NA1022624.1 Xylenes, Total 30 ug/L16 Total/NA1066624.1 o-Xylene 10 ug/L4.4 Total/NA1044624.1 Client Sample ID: MW-10 Lab Sample ID: 752-12339-8 Benzene RL 20 ug/L MDL 11 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA2028624.1 Toluene 20 ug/L11 Total/NA2034624.1 Ethylbenzene 20 ug/L9.2 Total/NA2068624.1 m-Xylene & p-Xylene 40 ug/L24 Total/NA20170624.1 Xylenes, Total 60 ug/L32 Total/NA20310624.1 Naphthalene 20 ug/L2.4 Total/NA2017J624.1 o-Xylene 20 ug/L8.8 Total/NA20140624.1 Eurofins Raleigh This Detection Summary does not include radiochemical test results. Page 6 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Detection Summary Job ID: 752-12339-1Client: Cape Lookout Environmental Services Project/Site: Cape Lookout- Seminole Mart #2 Client Sample ID: MW-11 Lab Sample ID: 752-12339-9 Benzene RL 10 ug/L MDL 5.7 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA1019624.1 Toluene 10 ug/L5.7 Total/NA10120624.1 Ethylbenzene 10 ug/L4.6 Total/NA10110624.1 m-Xylene & p-Xylene 20 ug/L12 Total/NA10340624.1 Methyl tert-butyl ether 10 ug/L2.6 Total/NA1013624.1 Xylenes, Total 30 ug/L16 Total/NA10620624.1 Naphthalene 10 ug/L1.2 Total/NA1021624.1 o-Xylene 10 ug/L4.4 Total/NA10280624.1 Client Sample ID: MW-12 Lab Sample ID: 752-12339-10 Ethylbenzene RL 10 ug/L MDL 4.6 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA1018624.1 m-Xylene & p-Xylene 20 ug/L12 Total/NA1053624.1 Xylenes, Total 30 ug/L16 Total/NA10130624.1 Naphthalene 10 ug/L1.2 Total/NA105.1 J 624.1 o-Xylene 10 ug/L4.4 Total/NA1077624.1 Client Sample ID: MW-13 Lab Sample ID: 752-12339-11 Toluene RL 10 ug/L MDL 5.7 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA1025624.1 Ethylbenzene 10 ug/L4.6 Total/NA1061624.1 m-Xylene & p-Xylene 20 ug/L12 Total/NA10190624.1 Methyl tert-butyl ether 10 ug/L2.6 Total/NA109.4 J 624.1 Xylenes, Total 30 ug/L16 Total/NA10310624.1 Naphthalene 10 ug/L1.2 Total/NA1011624.1 o-Xylene 10 ug/L4.4 Total/NA10120624.1 Client Sample ID: MW-14 Lab Sample ID: 752-12339-12 m-Xylene & p-Xylene RL 10 ug/L MDL 6.0 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA518624.1 Xylenes, Total 15 ug/L8.0 Total/NA550624.1 Naphthalene 5.0 ug/L0.60 Total/NA52.7 J 624.1 o-Xylene 5.0 ug/L2.2 Total/NA532624.1 Client Sample ID: MW-15 Lab Sample ID: 752-12339-13 Ethylbenzene RL 20 ug/L MDL 9.2 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA20J12624.1 m-Xylene & p-Xylene 40 ug/L24 Total/NA2027J624.1 Methyl tert-butyl ether 20 ug/L5.2 Total/NA2034624.1 Xylenes, Total 60 ug/L32 Total/NA2064624.1 o-Xylene 20 ug/L8.8 Total/NA2037624.1 Client Sample ID: MW-16 Lab Sample ID: 752-12339-14 Xylenes, Total RL 15 ug/L MDL 8.0 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA5J8.9 624.1 Naphthalene 5.0 ug/L0.60 Total/NA51.4 J 624.1 o-Xylene 5.0 ug/L2.2 Total/NA58.9 624.1 Eurofins Raleigh This Detection Summary does not include radiochemical test results. Page 7 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Detection Summary Job ID: 752-12339-1Client: Cape Lookout Environmental Services Project/Site: Cape Lookout- Seminole Mart #2 Client Sample ID: MW-17 Lab Sample ID: 752-12339-15 Toluene RL 20 ug/L MDL 11 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA2028624.1 Ethylbenzene 20 ug/L9.2 Total/NA2040624.1 m-Xylene & p-Xylene 40 ug/L24 Total/NA20120624.1 Methyl tert-butyl ether 20 ug/L5.2 Total/NA206.6 J 624.1 Xylenes, Total 60 ug/L32 Total/NA20250624.1 Naphthalene 20 ug/L2.4 Total/NA207.5 J 624.1 o-Xylene 20 ug/L8.8 Total/NA20130624.1 Client Sample ID: MW-18 Lab Sample ID: 752-12339-16 No Detections. Client Sample ID: MW-19 Lab Sample ID: 752-12339-17 Ethylbenzene RL 10 ug/L MDL 4.6 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA1036624.1 m-Xylene & p-Xylene 20 ug/L12 Total/NA1064624.1 Xylenes, Total 30 ug/L16 Total/NA10160624.1 Naphthalene 10 ug/L1.2 Total/NA109.7 J 624.1 o-Xylene 10 ug/L4.4 Total/NA10100624.1 Client Sample ID: MW-20 Lab Sample ID: 752-12339-18 Toluene RL 20 ug/L MDL 11 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA2028624.1 Ethylbenzene 20 ug/L9.2 Total/NA2067624.1 m-Xylene & p-Xylene 40 ug/L24 Total/NA20190624.1 Xylenes, Total 60 ug/L32 Total/NA20380624.1 Naphthalene 20 ug/L2.4 Total/NA2017J624.1 o-Xylene 20 ug/L8.8 Total/NA20190624.1 Client Sample ID: MW-21 Lab Sample ID: 752-12339-19 No Detections. Eurofins Raleigh This Detection Summary does not include radiochemical test results. Page 8 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 752-12339-1Client: Cape Lookout Environmental Services Project/Site: Cape Lookout- Seminole Mart #2 Lab Sample ID: 752-12339-1Client Sample ID: MW-1 Matrix: WaterDate Collected: 10/05/23 14:30 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL 72 10 5.7 ug/L 10/15/23 02:41 10 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 10 5.7 ug/L 10/15/23 02:41 10370Toluene 10 4.6 ug/L 10/15/23 02:41 10150Ethylbenzene 10 3.6 ug/L 10/15/23 02:41 10<3.6Isopropyl ether 20 12 ug/L 10/15/23 02:41 10470m-Xylene & p-Xylene 10 2.6 ug/L 10/15/23 02:41 10<2.6Methyl tert-butyl ether 30 16 ug/L 10/15/23 02:41 10810Xylenes, Total 10 1.2 ug/L 10/15/23 02:41 1021Naphthalene 10 4.4 ug/L 10/15/23 02:41 10340o-Xylene Dibromofluoromethane (Surr)94 67-129 10/15/23 02:41 10 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 4-Bromofluorobenzene (Surr)103 10/15/23 02:41 1053-136 Toluene-d8 (Surr)96 10/15/23 02:41 1059-134 Lab Sample ID: 752-12339-2Client Sample ID: MW-4 Matrix: WaterDate Collected: 10/05/23 12:05 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL <5.7 10 5.7 ug/L 10/15/23 03:10 10 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 10 5.7 ug/L 10/15/23 03:10 10<5.7Toluene 10 4.6 ug/L 10/15/23 03:10 10<4.6Ethylbenzene 10 3.6 ug/L 10/15/23 03:10 10<3.6Isopropyl ether 20 12 ug/L 10/15/23 03:10 10<12m-Xylene & p-Xylene 10 2.6 ug/L 10/15/23 03:10 10<2.6Methyl tert-butyl ether 30 16 ug/L 10/15/23 03:10 10<16Xylenes, Total 10 1.2 ug/L 10/15/23 03:10 10<1.2Naphthalene 10 4.4 ug/L 10/15/23 03:10 1015o-Xylene Dibromofluoromethane (Surr)96 67-129 10/15/23 03:10 10 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 4-Bromofluorobenzene (Surr)100 10/15/23 03:10 1053-136 Toluene-d8 (Surr)100 10/15/23 03:10 1059-134 Lab Sample ID: 752-12339-3Client Sample ID: MW-5 Matrix: WaterDate Collected: 10/05/23 11:20 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL <0.57 1.0 0.57 ug/L 10/15/23 03:40 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.0 0.57 ug/L 10/15/23 03:40 1<0.57Toluene 1.0 0.46 ug/L 10/15/23 03:40 1<0.46Ethylbenzene 1.0 0.36 ug/L 10/15/23 03:40 1<0.36Isopropyl ether 2.0 1.2 ug/L 10/15/23 03:40 1<1.2m-Xylene & p-Xylene 1.0 0.26 ug/L 10/15/23 03:40 1<0.26Methyl tert-butyl ether 3.0 1.6 ug/L 10/15/23 03:40 1<1.6Xylenes, Total 1.0 0.12 ug/L 10/15/23 03:40 1<0.12Naphthalene 1.0 0.44 ug/L 10/15/23 03:40 1<0.44o-Xylene Eurofins Raleigh Page 9 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 752-12339-1Client: Cape Lookout Environmental Services Project/Site: Cape Lookout- Seminole Mart #2 Lab Sample ID: 752-12339-3Client Sample ID: MW-5 Matrix: WaterDate Collected: 10/05/23 11:20 Date Received: 10/05/23 15:49 Dibromofluoromethane (Surr)99 67-129 10/15/23 03:40 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 4-Bromofluorobenzene (Surr)98 10/15/23 03:40 153-136 Toluene-d8 (Surr)99 10/15/23 03:40 159-134 Lab Sample ID: 752-12339-4Client Sample ID: MW-6 Matrix: WaterDate Collected: 10/05/23 11:20 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL <0.57 1.0 0.57 ug/L 10/15/23 04:09 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.0 0.57 ug/L 10/15/23 04:09 1<0.57Toluene 1.0 0.46 ug/L 10/15/23 04:09 1<0.46Ethylbenzene 1.0 0.36 ug/L 10/15/23 04:09 1<0.36Isopropyl ether 2.0 1.2 ug/L 10/15/23 04:09 1<1.2m-Xylene & p-Xylene 1.0 0.26 ug/L 10/15/23 04:09 1<0.26Methyl tert-butyl ether 3.0 1.6 ug/L 10/15/23 04:09 1<1.6Xylenes, Total 1.0 0.12 ug/L 10/15/23 04:09 1<0.12Naphthalene 1.0 0.44 ug/L 10/15/23 04:09 1<0.44o-Xylene Dibromofluoromethane (Surr)97 67-129 10/15/23 04:09 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 4-Bromofluorobenzene (Surr)101 10/15/23 04:09 153-136 Toluene-d8 (Surr)98 10/15/23 04:09 159-134 Lab Sample ID: 752-12339-5Client Sample ID: MW-7 Matrix: WaterDate Collected: 10/05/23 11:30 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL <0.57 1.0 0.57 ug/L 10/15/23 04:39 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.0 0.57 ug/L 10/15/23 04:39 1<0.57Toluene 1.0 0.46 ug/L 10/15/23 04:39 1<0.46Ethylbenzene 1.0 0.36 ug/L 10/15/23 04:39 1<0.36Isopropyl ether 2.0 1.2 ug/L 10/15/23 04:39 1<1.2m-Xylene & p-Xylene 1.0 0.26 ug/L 10/15/23 04:39 1<0.26Methyl tert-butyl ether 3.0 1.6 ug/L 10/15/23 04:39 1<1.6Xylenes, Total 1.0 0.12 ug/L 10/15/23 04:39 1<0.12Naphthalene 1.0 0.44 ug/L 10/15/23 04:39 1<0.44o-Xylene Dibromofluoromethane (Surr)98 67-129 10/15/23 04:39 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 4-Bromofluorobenzene (Surr)102 10/15/23 04:39 153-136 Toluene-d8 (Surr)99 10/15/23 04:39 159-134 Eurofins Raleigh Page 10 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 752-12339-1Client: Cape Lookout Environmental Services Project/Site: Cape Lookout- Seminole Mart #2 Lab Sample ID: 752-12339-6Client Sample ID: MW-8 Matrix: WaterDate Collected: 10/05/23 13:50 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL <11 20 11 ug/L 10/15/23 05:08 20 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 20 11 ug/L 10/15/23 05:08 20<11Toluene 20 9.2 ug/L 10/15/23 05:08 2059Ethylbenzene 20 7.2 ug/L 10/15/23 05:08 20<7.2Isopropyl ether 40 24 ug/L 10/15/23 05:08 20120m-Xylene & p-Xylene 20 5.2 ug/L 10/15/23 05:08 2026Methyl tert-butyl ether 60 32 ug/L 10/15/23 05:08 20330Xylenes, Total 20 2.4 ug/L 10/15/23 05:08 2033Naphthalene 20 8.8 ug/L 10/15/23 05:08 20210o-Xylene Dibromofluoromethane (Surr)96 67-129 10/15/23 05:08 20 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 4-Bromofluorobenzene (Surr)102 10/15/23 05:08 2053-136 Toluene-d8 (Surr)99 10/15/23 05:08 2059-134 Lab Sample ID: 752-12339-7Client Sample ID: MW-9 Matrix: WaterDate Collected: 10/05/23 12:40 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL 20 10 5.7 ug/L 10/17/23 19:15 10 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 10 5.7 ug/L 10/17/23 19:15 10<5.7Toluene 10 4.6 ug/L 10/17/23 19:15 10<4.6Ethylbenzene 10 3.6 ug/L 10/17/23 19:15 10<3.6Isopropyl ether 20 12 ug/L 10/17/23 19:15 1022m-Xylene & p-Xylene 10 2.6 ug/L 10/17/23 19:15 10<2.6Methyl tert-butyl ether 30 16 ug/L 10/17/23 19:15 1066Xylenes, Total 10 1.2 ug/L 10/17/23 19:15 10<1.2Naphthalene 10 4.4 ug/L 10/17/23 19:15 1044o-Xylene Dibromofluoromethane (Surr)99 *3 67-129 10/15/23 05:38 10 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)108 10/17/23 19:15 1067-129 4-Bromofluorobenzene (Surr)107 10/15/23 05:38 1053-136 4-Bromofluorobenzene (Surr)103 10/17/23 19:15 1053-136 Toluene-d8 (Surr)96 *3 10/15/23 05:38 1059-134 Toluene-d8 (Surr)99 10/17/23 19:15 1059-134 Lab Sample ID: 752-12339-8Client Sample ID: MW-10 Matrix: WaterDate Collected: 10/05/23 14:10 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL 28 20 11 ug/L 10/17/23 19:44 20 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 20 11 ug/L 10/17/23 19:44 2034Toluene 20 9.2 ug/L 10/17/23 19:44 2068Ethylbenzene 20 7.2 ug/L 10/17/23 19:44 20<7.2Isopropyl ether 40 24 ug/L 10/17/23 19:44 20170m-Xylene & p-Xylene 20 5.2 ug/L 10/17/23 19:44 20<5.2Methyl tert-butyl ether Eurofins Raleigh Page 11 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 752-12339-1Client: Cape Lookout Environmental Services Project/Site: Cape Lookout- Seminole Mart #2 Lab Sample ID: 752-12339-8Client Sample ID: MW-10 Matrix: WaterDate Collected: 10/05/23 14:10 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 310 60 32 ug/L 10/17/23 19:44 20 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Xylenes, Total 20 2.4 ug/L 10/17/23 19:44 2017JNaphthalene 20 8.8 ug/L 10/17/23 19:44 20140o-Xylene Dibromofluoromethane (Surr)99 *3 67-129 10/15/23 06:08 20 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)102 10/17/23 19:44 2067-129 4-Bromofluorobenzene (Surr)110 *3 10/15/23 06:08 2053-136 4-Bromofluorobenzene (Surr)105 10/17/23 19:44 2053-136 Toluene-d8 (Surr)97 *3 10/15/23 06:08 2059-134 Toluene-d8 (Surr)98 10/17/23 19:44 2059-134 Lab Sample ID: 752-12339-9Client Sample ID: MW-11 Matrix: WaterDate Collected: 10/05/23 14:35 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL 19 10 5.7 ug/L 10/17/23 20:14 10 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 10 5.7 ug/L 10/17/23 20:14 10120Toluene 10 4.6 ug/L 10/17/23 20:14 10110Ethylbenzene 10 3.6 ug/L 10/17/23 20:14 10<3.6Isopropyl ether 20 12 ug/L 10/17/23 20:14 10340m-Xylene & p-Xylene 10 2.6 ug/L 10/17/23 20:14 1013Methyl tert-butyl ether 30 16 ug/L 10/17/23 20:14 10620Xylenes, Total 10 1.2 ug/L 10/17/23 20:14 1021Naphthalene 10 4.4 ug/L 10/17/23 20:14 10280o-Xylene Dibromofluoromethane (Surr)100 *3 67-129 10/15/23 06:37 50 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)100 10/17/23 20:14 1067-129 4-Bromofluorobenzene (Surr)110 *3 10/15/23 06:37 5053-136 4-Bromofluorobenzene (Surr)105 10/17/23 20:14 1053-136 Toluene-d8 (Surr)97 *3 10/15/23 06:37 5059-134 Toluene-d8 (Surr)99 10/17/23 20:14 1059-134 Lab Sample ID: 752-12339-10Client Sample ID: MW-12 Matrix: WaterDate Collected: 10/05/23 12:00 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL <5.7 10 5.7 ug/L 10/17/23 20:43 10 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 10 5.7 ug/L 10/17/23 20:43 10<5.7Toluene 10 4.6 ug/L 10/17/23 20:43 1018Ethylbenzene 10 3.6 ug/L 10/17/23 20:43 10<3.6Isopropyl ether 20 12 ug/L 10/17/23 20:43 1053m-Xylene & p-Xylene 10 2.6 ug/L 10/17/23 20:43 10<2.6Methyl tert-butyl ether 30 16 ug/L 10/17/23 20:43 10130Xylenes, Total 10 1.2 ug/L 10/17/23 20:43 105.1 JNaphthalene 10 4.4 ug/L 10/17/23 20:43 1077o-Xylene Eurofins Raleigh Page 12 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 752-12339-1Client: Cape Lookout Environmental Services Project/Site: Cape Lookout- Seminole Mart #2 Lab Sample ID: 752-12339-10Client Sample ID: MW-12 Matrix: WaterDate Collected: 10/05/23 12:00 Date Received: 10/05/23 15:49 Dibromofluoromethane (Surr)100 *3 67-129 10/15/23 07:07 10 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)102 10/17/23 20:43 1067-129 4-Bromofluorobenzene (Surr)111 *3 10/15/23 07:07 1053-136 4-Bromofluorobenzene (Surr)106 10/17/23 20:43 1053-136 Toluene-d8 (Surr)96 *3 10/15/23 07:07 1059-134 Toluene-d8 (Surr)96 10/17/23 20:43 1059-134 Lab Sample ID: 752-12339-11Client Sample ID: MW-13 Matrix: WaterDate Collected: 10/05/23 11:50 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL <5.7 10 5.7 ug/L 10/17/23 21:13 10 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 10 5.7 ug/L 10/17/23 21:13 1025Toluene 10 4.6 ug/L 10/17/23 21:13 1061Ethylbenzene 10 3.6 ug/L 10/17/23 21:13 10<3.6Isopropyl ether 20 12 ug/L 10/17/23 21:13 10190m-Xylene & p-Xylene 10 2.6 ug/L 10/17/23 21:13 109.4 JMethyl tert-butyl ether 30 16 ug/L 10/17/23 21:13 10310Xylenes, Total 10 1.2 ug/L 10/17/23 21:13 1011Naphthalene 10 4.4 ug/L 10/17/23 21:13 10120o-Xylene Dibromofluoromethane (Surr)98 *3 67-129 10/15/23 07:36 10 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)98 10/17/23 21:13 1067-129 4-Bromofluorobenzene (Surr)110 *3 10/15/23 07:36 1053-136 4-Bromofluorobenzene (Surr)108 10/17/23 21:13 1053-136 Toluene-d8 (Surr)95 *3 10/15/23 07:36 1059-134 Toluene-d8 (Surr)99 10/17/23 21:13 1059-134 Lab Sample ID: 752-12339-12Client Sample ID: MW-14 Matrix: WaterDate Collected: 10/05/23 12:15 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL <2.9 5.0 2.9 ug/L 10/19/23 19:52 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 5.0 2.9 ug/L 10/19/23 19:52 5<2.9Toluene 5.0 2.3 ug/L 10/19/23 19:52 5<2.3Ethylbenzene 5.0 1.8 ug/L 10/19/23 19:52 5<1.8Isopropyl ether 10 6.0 ug/L 10/19/23 19:52 518m-Xylene & p-Xylene 5.0 1.3 ug/L 10/19/23 19:52 5<1.3Methyl tert-butyl ether 15 8.0 ug/L 10/19/23 19:52 550Xylenes, Total 5.0 0.60 ug/L 10/19/23 19:52 52.7 JNaphthalene 5.0 2.2 ug/L 10/19/23 19:52 532o-Xylene Dibromofluoromethane (Surr)106 67-129 10/17/23 21:42 10 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)97 10/19/23 19:52 567-129 4-Bromofluorobenzene (Surr)109 10/17/23 21:42 1053-136 Eurofins Raleigh Page 13 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 752-12339-1Client: Cape Lookout Environmental Services Project/Site: Cape Lookout- Seminole Mart #2 Lab Sample ID: 752-12339-12Client Sample ID: MW-14 Matrix: WaterDate Collected: 10/05/23 12:15 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) (Continued) 4-Bromofluorobenzene (Surr)102 53-136 10/19/23 19:52 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Toluene-d8 (Surr)99 10/17/23 21:42 1059-134 Toluene-d8 (Surr)99 10/19/23 19:52 559-134 Lab Sample ID: 752-12339-13Client Sample ID: MW-15 Matrix: WaterDate Collected: 10/05/23 13:55 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL <11 20 11 ug/L 10/17/23 22:12 20 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 20 11 ug/L 10/17/23 22:12 20<11Toluene 20 9.2 ug/L 10/17/23 22:12 2012JEthylbenzene 20 7.2 ug/L 10/17/23 22:12 20<7.2Isopropyl ether 40 24 ug/L 10/17/23 22:12 2027Jm-Xylene & p-Xylene 20 5.2 ug/L 10/17/23 22:12 2034Methyl tert-butyl ether 60 32 ug/L 10/17/23 22:12 2064Xylenes, Total 20 2.4 ug/L 10/17/23 22:12 20<2.4Naphthalene 20 8.8 ug/L 10/17/23 22:12 2037o-Xylene Dibromofluoromethane (Surr)102 67-129 10/17/23 22:12 20 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 4-Bromofluorobenzene (Surr)109 10/17/23 22:12 2053-136 Toluene-d8 (Surr)98 10/17/23 22:12 2059-134 Lab Sample ID: 752-12339-14Client Sample ID: MW-16 Matrix: WaterDate Collected: 10/05/23 12:25 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL <2.9 5.0 2.9 ug/L 10/19/23 20:21 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 5.0 2.9 ug/L 10/19/23 20:21 5<2.9Toluene 5.0 2.3 ug/L 10/19/23 20:21 5<2.3Ethylbenzene 5.0 1.8 ug/L 10/19/23 20:21 5<1.8Isopropyl ether 10 6.0 ug/L 10/19/23 20:21 5<6.0m-Xylene & p-Xylene 5.0 1.3 ug/L 10/19/23 20:21 5<1.3Methyl tert-butyl ether 15 8.0 ug/L 10/19/23 20:21 58.9 JXylenes, Total 5.0 0.60 ug/L 10/19/23 20:21 51.4 JNaphthalene 5.0 2.2 ug/L 10/19/23 20:21 58.9o-Xylene Dibromofluoromethane (Surr)104 67-129 10/17/23 22:41 20 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)100 10/19/23 20:21 567-129 4-Bromofluorobenzene (Surr)108 10/17/23 22:41 2053-136 4-Bromofluorobenzene (Surr)103 10/19/23 20:21 553-136 Toluene-d8 (Surr)97 10/17/23 22:41 2059-134 Toluene-d8 (Surr)97 10/19/23 20:21 559-134 Eurofins Raleigh Page 14 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 752-12339-1Client: Cape Lookout Environmental Services Project/Site: Cape Lookout- Seminole Mart #2 Lab Sample ID: 752-12339-15Client Sample ID: MW-17 Matrix: WaterDate Collected: 10/05/23 14:05 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL <11 20 11 ug/L 10/17/23 23:11 20 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 20 11 ug/L 10/17/23 23:11 2028Toluene 20 9.2 ug/L 10/17/23 23:11 2040Ethylbenzene 20 7.2 ug/L 10/17/23 23:11 20<7.2Isopropyl ether 40 24 ug/L 10/17/23 23:11 20120m-Xylene & p-Xylene 20 5.2 ug/L 10/17/23 23:11 206.6 JMethyl tert-butyl ether 60 32 ug/L 10/17/23 23:11 20250Xylenes, Total 20 2.4 ug/L 10/17/23 23:11 207.5 JNaphthalene 20 8.8 ug/L 10/17/23 23:11 20130o-Xylene Dibromofluoromethane (Surr)102 67-129 10/17/23 23:11 20 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 4-Bromofluorobenzene (Surr)108 10/17/23 23:11 2053-136 Toluene-d8 (Surr)100 10/17/23 23:11 2059-134 Lab Sample ID: 752-12339-16Client Sample ID: MW-18 Matrix: WaterDate Collected: 10/05/23 11:40 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL <2.9 5.0 2.9 ug/L 10/19/23 20:51 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 5.0 2.9 ug/L 10/19/23 20:51 5<2.9Toluene 5.0 2.3 ug/L 10/19/23 20:51 5<2.3Ethylbenzene 5.0 1.8 ug/L 10/19/23 20:51 5<1.8Isopropyl ether 10 6.0 ug/L 10/19/23 20:51 5<6.0m-Xylene & p-Xylene 5.0 1.3 ug/L 10/19/23 20:51 5<1.3Methyl tert-butyl ether 15 8.0 ug/L 10/19/23 20:51 5<8.0Xylenes, Total 5.0 0.60 ug/L 10/19/23 20:51 5<0.60Naphthalene 5.0 2.2 ug/L 10/19/23 20:51 5<2.2o-Xylene Dibromofluoromethane (Surr)101 67-129 10/17/23 23:40 20 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)98 10/19/23 20:51 567-129 4-Bromofluorobenzene (Surr)107 10/17/23 23:40 2053-136 4-Bromofluorobenzene (Surr)102 10/19/23 20:51 553-136 Toluene-d8 (Surr)95 10/17/23 23:40 2059-134 Toluene-d8 (Surr)98 10/19/23 20:51 559-134 Lab Sample ID: 752-12339-17Client Sample ID: MW-19 Matrix: WaterDate Collected: 10/05/23 12:25 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL <5.7 10 5.7 ug/L 10/19/23 21:21 10 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 10 5.7 ug/L 10/19/23 21:21 10<5.7Toluene 10 4.6 ug/L 10/19/23 21:21 1036Ethylbenzene 10 3.6 ug/L 10/19/23 21:21 10<3.6Isopropyl ether 20 12 ug/L 10/19/23 21:21 1064m-Xylene & p-Xylene 10 2.6 ug/L 10/19/23 21:21 10<2.6Methyl tert-butyl ether Eurofins Raleigh Page 15 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 752-12339-1Client: Cape Lookout Environmental Services Project/Site: Cape Lookout- Seminole Mart #2 Lab Sample ID: 752-12339-17Client Sample ID: MW-19 Matrix: WaterDate Collected: 10/05/23 12:25 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 160 30 16 ug/L 10/19/23 21:21 10 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Xylenes, Total 10 1.2 ug/L 10/19/23 21:21 109.7 JNaphthalene 10 4.4 ug/L 10/19/23 21:21 10100o-Xylene Dibromofluoromethane (Surr)106 67-129 10/18/23 00:10 20 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)101 10/19/23 21:21 1067-129 4-Bromofluorobenzene (Surr)107 10/18/23 00:10 2053-136 4-Bromofluorobenzene (Surr)103 10/19/23 21:21 1053-136 Toluene-d8 (Surr)97 10/18/23 00:10 2059-134 Toluene-d8 (Surr)99 10/19/23 21:21 1059-134 Lab Sample ID: 752-12339-18Client Sample ID: MW-20 Matrix: WaterDate Collected: 10/05/23 12:40 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL <11 20 11 ug/L 10/18/23 00:39 20 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 20 11 ug/L 10/18/23 00:39 2028Toluene 20 9.2 ug/L 10/18/23 00:39 2067Ethylbenzene 20 7.2 ug/L 10/18/23 00:39 20<7.2Isopropyl ether 40 24 ug/L 10/18/23 00:39 20190m-Xylene & p-Xylene 20 5.2 ug/L 10/18/23 00:39 20<5.2Methyl tert-butyl ether 60 32 ug/L 10/18/23 00:39 20380Xylenes, Total 20 2.4 ug/L 10/18/23 00:39 2017JNaphthalene 20 8.8 ug/L 10/18/23 00:39 20190o-Xylene Dibromofluoromethane (Surr)106 67-129 10/18/23 00:39 20 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 4-Bromofluorobenzene (Surr)103 10/18/23 00:39 2053-136 Toluene-d8 (Surr)101 10/18/23 00:39 2059-134 Lab Sample ID: 752-12339-19Client Sample ID: MW-21 Matrix: WaterDate Collected: 10/05/23 10:55 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL <0.57 1.0 0.57 ug/L 10/19/23 19:22 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.0 0.57 ug/L 10/19/23 19:22 1<0.57Toluene 1.0 0.46 ug/L 10/19/23 19:22 1<0.46Ethylbenzene 1.0 0.36 ug/L 10/19/23 19:22 1<0.36Isopropyl ether 2.0 1.2 ug/L 10/19/23 19:22 1<1.2m-Xylene & p-Xylene 1.0 0.26 ug/L 10/19/23 19:22 1<0.26Methyl tert-butyl ether 3.0 1.6 ug/L 10/19/23 19:22 1<1.6Xylenes, Total 1.0 0.12 ug/L 10/19/23 19:22 1<0.12Naphthalene 1.0 0.44 ug/L 10/19/23 19:22 1<0.44o-Xylene Dibromofluoromethane (Surr)99 67-129 10/18/23 01:08 10 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Raleigh Page 16 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 752-12339-1Client: Cape Lookout Environmental Services Project/Site: Cape Lookout- Seminole Mart #2 Lab Sample ID: 752-12339-19Client Sample ID: MW-21 Matrix: WaterDate Collected: 10/05/23 10:55 Date Received: 10/05/23 15:49 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) (Continued) Dibromofluoromethane (Surr)97 67-129 10/19/23 19:22 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 4-Bromofluorobenzene (Surr)107 10/18/23 01:08 1053-136 4-Bromofluorobenzene (Surr)103 10/19/23 19:22 153-136 Toluene-d8 (Surr)98 10/18/23 01:08 1059-134 Toluene-d8 (Surr)101 10/19/23 19:22 159-134 Eurofins Raleigh Page 17 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Surrogate Summary Job ID: 752-12339-1Client: Cape Lookout Environmental Services Project/Site: Cape Lookout- Seminole Mart #2 Method: 624.1 - Volatile Organic Compounds (GC/MS) Prep Type: Total/NAMatrix: Water Lab Sample ID Client Sample ID (67-129)(53-136)(59-134) DBFM BFB TOL 94 103 96752-12339-1 Percent Surrogate Recovery (Acceptance Limits) MW-1 96 100 100752-12339-2 MW-4 99 98 99752-12339-3 MW-5 97 101 98752-12339-4 MW-6 98 102 99752-12339-5 MW-7 96 102 99752-12339-6 MW-8 99 *3 107 96 *3752-12339-7 MW-9 108 103 99752-12339-7 MW-9 99 *3 110 *3 97 *3752-12339-8 MW-10 102 105 98752-12339-8 MW-10 100 *3 110 *3 97 *3752-12339-9 MW-11 100 105 99752-12339-9 MW-11 100 *3 111 *3 96 *3752-12339-10 MW-12 102 106 96752-12339-10 MW-12 98 *3 110 *3 95 *3752-12339-11 MW-13 98 108 99752-12339-11 MW-13 106 109 99752-12339-12 MW-14 97 102 99752-12339-12 MW-14 102 109 98752-12339-13 MW-15 104 108 97752-12339-14 MW-16 100 103 97752-12339-14 MW-16 102 108 100752-12339-15 MW-17 101 107 95752-12339-16 MW-18 98 102 98752-12339-16 MW-18 106 107 97752-12339-17 MW-19 101 103 99752-12339-17 MW-19 106 103 101752-12339-18 MW-20 99 107 98752-12339-19 MW-21 97 103 101752-12339-19 MW-21 97 99 97LCS 752-4802/5 Lab Control Sample 101 100 97LCS 752-4822/5 Lab Control Sample 99 106 97LCS 752-4841/5 Lab Control Sample 99 103 99LCSD 752-4802/6 Lab Control Sample Dup 100 102 100LCSD 752-4822/6 Lab Control Sample Dup 101 105 101LCSD 752-4841/6 Lab Control Sample Dup 96 104 97MB 752-4802/8 Method Blank 106 103 102MB 752-4822/8 Method Blank 100 106 102MB 752-4841/8 Method Blank 97 103 97MRL 752-4802/4 Lab Control Sample 102 103 97MRL 752-4822/4 Lab Control Sample 103 107 98MRL 752-4841/4 Lab Control Sample Surrogate Legend DBFM = Dibromofluoromethane (Surr) BFB = 4-Bromofluorobenzene (Surr) TOL = Toluene-d8 (Surr) Eurofins Raleigh Page 18 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 752-12339-1Client: Cape Lookout Environmental Services Project/Site: Cape Lookout- Seminole Mart #2 Method: 624.1 - Volatile Organic Compounds (GC/MS) Client Sample ID: Method BlankLab Sample ID: MB 752-4802/8 Matrix: Water Prep Type: Total/NA Analysis Batch: 4802 RL MDL Benzene <0.57 1.0 0.57 ug/L 10/14/23 21:45 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.57 0.571.0 ug/L 10/14/23 21:45 1Toluene <0.46 0.461.0 ug/L 10/14/23 21:45 1Ethylbenzene <0.36 0.361.0 ug/L 10/14/23 21:45 1Isopropyl ether <1.2 1.22.0 ug/L 10/14/23 21:45 1m-Xylene & p-Xylene <0.26 0.261.0 ug/L 10/14/23 21:45 1Methyl tert-butyl ether <1.6 1.63.0 ug/L 10/14/23 21:45 1Xylenes, Total <0.12 0.121.0 ug/L 10/14/23 21:45 1Naphthalene <0.44 0.441.0 ug/L 10/14/23 21:45 1o-Xylene Dibromofluoromethane (Surr)96 67-129 10/14/23 21:45 1 MB MB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery 104 10/14/23 21:45 14-Bromofluorobenzene (Surr)53-136 97 10/14/23 21:45 1Toluene-d8 (Surr)59-134 Client Sample ID: Lab Control SampleLab Sample ID: LCS 752-4802/5 Matrix: Water Prep Type: Total/NA Analysis Batch: 4802 Benzene 20.0 19.5 ug/L 97 65 -135 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Toluene 20.0 17.9 ug/L 90 70 -130 Ethylbenzene 20.0 17.8 ug/L 89 60 -140 Isopropyl ether 20.0 21.7 ug/L 109 37 -134 m-Xylene & p-Xylene 40.0 37.7 ug/L 94 79 -121 Methyl tert-butyl ether 20.0 18.4 ug/L 92 57 -133 Xylenes, Total 60.0 55.9 ug/L 93 73 -120 Naphthalene 20.0 15.7 ug/L 78 56 -133 o-Xylene 20.0 18.2 ug/L 91 65 -120 Dibromofluoromethane (Surr)67 -129 Surrogate 97 LCS LCS Qualifier Limits%Recovery 994-Bromofluorobenzene (Surr)53 -136 97Toluene-d8 (Surr)59 -134 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 752-4802/6 Matrix: Water Prep Type: Total/NA Analysis Batch: 4802 Benzene 20.0 18.5 ug/L 93 65 -135 5 61 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD Toluene 20.0 18.7 ug/L 93 70 -130 4 41 Ethylbenzene 20.0 17.7 ug/L 89 60 -140 0 63 Isopropyl ether 20.0 22.3 ug/L 112 37 -134 3 20 m-Xylene & p-Xylene 40.0 36.6 ug/L 92 79 -121 3 16 Methyl tert-butyl ether 20.0 18.5 ug/L 92 57 -133 1 21 Xylenes, Total 60.0 54.3 ug/L 91 73 -120 3 16 Naphthalene 20.0 15.5 ug/L 77 56 -133 1 19 Eurofins Raleigh Page 19 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 752-12339-1Client: Cape Lookout Environmental Services Project/Site: Cape Lookout- Seminole Mart #2 Method: 624.1 - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 752-4802/6 Matrix: Water Prep Type: Total/NA Analysis Batch: 4802 o-Xylene 20.0 17.7 ug/L 88 65 -120 3 15 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD Dibromofluoromethane (Surr)67 -129 Surrogate 99 LCSD LCSD Qualifier Limits%Recovery 1034-Bromofluorobenzene (Surr)53 -136 99Toluene-d8 (Surr)59 -134 Client Sample ID: Lab Control SampleLab Sample ID: MRL 752-4802/4 Matrix: Water Prep Type: Total/NA Analysis Batch: 4802 Benzene 1.00 1.04 ug/L 104 Analyte MRL MRL DUnitResultQualifier %Rec Spike Added %Rec Limits Toluene 1.00 1.31 ug/L 131 Ethylbenzene 1.00 1.01 ug/L 101 Isopropyl ether 1.00 1.02 ug/L 102 m-Xylene & p-Xylene 2.00 1.98 J ug/L 99 Methyl tert-butyl ether 1.00 0.928 J ug/L 93 Xylenes, Total 3.00 2.93 J ug/L 98 Naphthalene 1.00 2.03 ug/L 203 o-Xylene 1.00 0.948 J ug/L 95 Dibromofluoromethane (Surr)67 -129 Surrogate 97 MRL MRL Qualifier Limits%Recovery 1034-Bromofluorobenzene (Surr)53 -136 97Toluene-d8 (Surr)59 -134 Client Sample ID: Method BlankLab Sample ID: MB 752-4822/8 Matrix: Water Prep Type: Total/NA Analysis Batch: 4822 RL MDL Benzene <0.57 1.0 0.57 ug/L 10/17/23 15:18 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.57 0.571.0 ug/L 10/17/23 15:18 1Toluene <0.46 0.461.0 ug/L 10/17/23 15:18 1Ethylbenzene <0.36 0.361.0 ug/L 10/17/23 15:18 1Isopropyl ether <1.2 1.22.0 ug/L 10/17/23 15:18 1m-Xylene & p-Xylene <0.26 0.261.0 ug/L 10/17/23 15:18 1Methyl tert-butyl ether <1.6 1.63.0 ug/L 10/17/23 15:18 1Xylenes, Total <0.12 0.121.0 ug/L 10/17/23 15:18 1Naphthalene <0.44 0.441.0 ug/L 10/17/23 15:18 1o-Xylene Dibromofluoromethane (Surr)106 67-129 10/17/23 15:18 1 MB MB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery 103 10/17/23 15:18 14-Bromofluorobenzene (Surr)53-136 102 10/17/23 15:18 1Toluene-d8 (Surr)59-134 Eurofins Raleigh Page 20 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 752-12339-1Client: Cape Lookout Environmental Services Project/Site: Cape Lookout- Seminole Mart #2 Method: 624.1 - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 752-4822/5 Matrix: Water Prep Type: Total/NA Analysis Batch: 4822 Benzene 20.0 16.9 ug/L 84 65 -135 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Toluene 20.0 16.3 ug/L 82 70 -130 Ethylbenzene 20.0 16.7 ug/L 83 60 -140 Isopropyl ether 20.0 21.3 ug/L 106 37 -134 m-Xylene & p-Xylene 40.0 34.1 ug/L 85 79 -121 Methyl tert-butyl ether 20.0 19.3 ug/L 97 57 -133 Xylenes, Total 60.0 50.6 ug/L 84 73 -120 Naphthalene 20.0 16.5 ug/L 82 56 -133 o-Xylene 20.0 16.5 ug/L 83 65 -120 Dibromofluoromethane (Surr)67 -129 Surrogate 101 LCS LCS Qualifier Limits%Recovery 1004-Bromofluorobenzene (Surr)53 -136 97Toluene-d8 (Surr)59 -134 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 752-4822/6 Matrix: Water Prep Type: Total/NA Analysis Batch: 4822 Benzene 20.0 16.9 ug/L 85 65 -135 0 61 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD Toluene 20.0 16.0 ug/L 80 70 -130 2 41 Ethylbenzene 20.0 16.6 ug/L 83 60 -140 0 63 Isopropyl ether 20.0 20.7 ug/L 103 37 -134 3 20 m-Xylene & p-Xylene 40.0 34.2 ug/L 85 79 -121 0 16 Methyl tert-butyl ether 20.0 19.6 ug/L 98 57 -133 2 21 Xylenes, Total 60.0 50.9 ug/L 85 73 -120 1 16 Naphthalene 20.0 18.3 ug/L 92 56 -133 10 19 o-Xylene 20.0 16.7 ug/L 84 65 -120 1 15 Dibromofluoromethane (Surr)67 -129 Surrogate 100 LCSD LCSD Qualifier Limits%Recovery 1024-Bromofluorobenzene (Surr)53 -136 100Toluene-d8 (Surr)59 -134 Client Sample ID: Lab Control SampleLab Sample ID: MRL 752-4822/4 Matrix: Water Prep Type: Total/NA Analysis Batch: 4822 Benzene 1.00 1.04 ug/L 104 Analyte MRL MRL DUnitResultQualifier %Rec Spike Added %Rec Limits Toluene 1.00 0.879 J ug/L 88 Ethylbenzene 1.00 1.03 ug/L 103 Isopropyl ether 1.00 0.812 J ug/L 81 m-Xylene & p-Xylene 2.00 1.97 J ug/L 99 Methyl tert-butyl ether 1.00 0.829 J ug/L 83 Xylenes, Total 3.00 2.92 J ug/L 97 Naphthalene 1.00 1.80 ug/L 180 Eurofins Raleigh Page 21 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 752-12339-1Client: Cape Lookout Environmental Services Project/Site: Cape Lookout- Seminole Mart #2 Method: 624.1 - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: MRL 752-4822/4 Matrix: Water Prep Type: Total/NA Analysis Batch: 4822 o-Xylene 1.00 0.946 J ug/L 95 Analyte MRL MRL DUnitResultQualifier %Rec Spike Added %Rec Limits Dibromofluoromethane (Surr)67 -129 Surrogate 102 MRL MRL Qualifier Limits%Recovery 1034-Bromofluorobenzene (Surr)53 -136 97Toluene-d8 (Surr)59 -134 Client Sample ID: Method BlankLab Sample ID: MB 752-4841/8 Matrix: Water Prep Type: Total/NA Analysis Batch: 4841 RL MDL Benzene <0.57 1.0 0.57 ug/L 10/19/23 17:23 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.57 0.571.0 ug/L 10/19/23 17:23 1Toluene <0.46 0.461.0 ug/L 10/19/23 17:23 1Ethylbenzene <0.36 0.361.0 ug/L 10/19/23 17:23 1Isopropyl ether <1.2 1.22.0 ug/L 10/19/23 17:23 1m-Xylene & p-Xylene <0.26 0.261.0 ug/L 10/19/23 17:23 1Methyl tert-butyl ether <1.6 1.63.0 ug/L 10/19/23 17:23 1Xylenes, Total <0.12 0.121.0 ug/L 10/19/23 17:23 1Naphthalene <0.44 0.441.0 ug/L 10/19/23 17:23 1o-Xylene Dibromofluoromethane (Surr)100 67-129 10/19/23 17:23 1 MB MB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery 106 10/19/23 17:23 14-Bromofluorobenzene (Surr)53-136 102 10/19/23 17:23 1Toluene-d8 (Surr)59-134 Client Sample ID: Lab Control SampleLab Sample ID: LCS 752-4841/5 Matrix: Water Prep Type: Total/NA Analysis Batch: 4841 Benzene 20.0 18.0 ug/L 90 65 -135 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Toluene 20.0 16.6 ug/L 83 70 -130 Ethylbenzene 20.0 16.5 ug/L 83 60 -140 Isopropyl ether 20.0 19.9 ug/L 100 37 -134 m-Xylene & p-Xylene 40.0 34.7 ug/L 87 79 -121 Methyl tert-butyl ether 20.0 18.7 ug/L 94 57 -133 Xylenes, Total 60.0 51.7 ug/L 86 73 -120 Naphthalene 20.0 17.5 ug/L 87 56 -133 o-Xylene 20.0 17.0 ug/L 85 65 -120 Dibromofluoromethane (Surr)67 -129 Surrogate 99 LCS LCS Qualifier Limits%Recovery 1064-Bromofluorobenzene (Surr)53 -136 97Toluene-d8 (Surr)59 -134 Eurofins Raleigh Page 22 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 752-12339-1Client: Cape Lookout Environmental Services Project/Site: Cape Lookout- Seminole Mart #2 Method: 624.1 - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 752-4841/6 Matrix: Water Prep Type: Total/NA Analysis Batch: 4841 Benzene 20.0 17.7 ug/L 88 65 -135 2 61 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD Toluene 20.0 17.1 ug/L 85 70 -130 3 41 Ethylbenzene 20.0 16.7 ug/L 83 60 -140 1 63 Isopropyl ether 20.0 19.7 ug/L 98 37 -134 1 20 m-Xylene & p-Xylene 40.0 34.3 ug/L 86 79 -121 1 16 Methyl tert-butyl ether 20.0 18.9 ug/L 95 57 -133 1 21 Xylenes, Total 60.0 50.8 ug/L 85 73 -120 2 16 Naphthalene 20.0 17.6 ug/L 88 56 -133 1 19 o-Xylene 20.0 16.5 ug/L 82 65 -120 3 15 Dibromofluoromethane (Surr)67 -129 Surrogate 101 LCSD LCSD Qualifier Limits%Recovery 1054-Bromofluorobenzene (Surr)53 -136 101Toluene-d8 (Surr)59 -134 Client Sample ID: Lab Control SampleLab Sample ID: MRL 752-4841/4 Matrix: Water Prep Type: Total/NA Analysis Batch: 4841 Benzene 1.00 1.17 ug/L 117 Analyte MRL MRL DUnitResultQualifier %Rec Spike Added %Rec Limits Toluene 1.00 1.27 ug/L 127 Ethylbenzene 1.00 1.18 ug/L 118 Isopropyl ether 1.00 0.975 J ug/L 98 m-Xylene & p-Xylene 2.00 2.17 ug/L 108 Methyl tert-butyl ether 1.00 0.913 J ug/L 91 Xylenes, Total 3.00 3.19 ug/L 106 Naphthalene 1.00 1.78 ug/L 178 o-Xylene 1.00 1.02 ug/L 102 Dibromofluoromethane (Surr)67 -129 Surrogate 103 MRL MRL Qualifier Limits%Recovery 1074-Bromofluorobenzene (Surr)53 -136 98Toluene-d8 (Surr)59 -134 Eurofins Raleigh Page 23 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Association Summary Job ID: 752-12339-1Client: Cape Lookout Environmental Services Project/Site: Cape Lookout- Seminole Mart #2 GC/MS VOA Analysis Batch: 4802 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 624.1752-12339-1 MW-1 Total/NA Water 624.1752-12339-2 MW-4 Total/NA Water 624.1752-12339-3 MW-5 Total/NA Water 624.1752-12339-4 MW-6 Total/NA Water 624.1752-12339-5 MW-7 Total/NA Water 624.1752-12339-6 MW-8 Total/NA Water 624.1752-12339-7 MW-9 Total/NA Water 624.1752-12339-8 MW-10 Total/NA Water 624.1752-12339-9 MW-11 Total/NA Water 624.1752-12339-10 MW-12 Total/NA Water 624.1752-12339-11 MW-13 Total/NA Water 624.1MB 752-4802/8 Method Blank Total/NA Water 624.1LCS 752-4802/5 Lab Control Sample Total/NA Water 624.1LCSD 752-4802/6 Lab Control Sample Dup Total/NA Water 624.1MRL 752-4802/4 Lab Control Sample Total/NA Analysis Batch: 4822 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 624.1752-12339-7 MW-9 Total/NA Water 624.1752-12339-8 MW-10 Total/NA Water 624.1752-12339-9 MW-11 Total/NA Water 624.1752-12339-10 MW-12 Total/NA Water 624.1752-12339-11 MW-13 Total/NA Water 624.1752-12339-12 MW-14 Total/NA Water 624.1752-12339-13 MW-15 Total/NA Water 624.1752-12339-14 MW-16 Total/NA Water 624.1752-12339-15 MW-17 Total/NA Water 624.1752-12339-16 MW-18 Total/NA Water 624.1752-12339-17 MW-19 Total/NA Water 624.1752-12339-18 MW-20 Total/NA Water 624.1752-12339-19 MW-21 Total/NA Water 624.1MB 752-4822/8 Method Blank Total/NA Water 624.1LCS 752-4822/5 Lab Control Sample Total/NA Water 624.1LCSD 752-4822/6 Lab Control Sample Dup Total/NA Water 624.1MRL 752-4822/4 Lab Control Sample Total/NA Analysis Batch: 4841 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 624.1752-12339-12 MW-14 Total/NA Water 624.1752-12339-14 MW-16 Total/NA Water 624.1752-12339-16 MW-18 Total/NA Water 624.1752-12339-17 MW-19 Total/NA Water 624.1752-12339-19 MW-21 Total/NA Water 624.1MB 752-4841/8 Method Blank Total/NA Water 624.1LCS 752-4841/5 Lab Control Sample Total/NA Water 624.1LCSD 752-4841/6 Lab Control Sample Dup Total/NA Water 624.1MRL 752-4841/4 Lab Control Sample Total/NA Eurofins Raleigh Page 24 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Cape Lookout Environmental Services Job ID: 752-12339-1 Project/Site: Cape Lookout- Seminole Mart #2 Client Sample ID: MW-1 Lab Sample ID: 752-12339-1 Matrix: WaterDate Collected: 10/05/23 14:30 Date Received: 10/05/23 15:49 Analysis 624.1 RY104802 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 10/15/23 02:41 Client Sample ID: MW-4 Lab Sample ID: 752-12339-2 Matrix: WaterDate Collected: 10/05/23 12:05 Date Received: 10/05/23 15:49 Analysis 624.1 RY104802 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 10/15/23 03:10 Client Sample ID: MW-5 Lab Sample ID: 752-12339-3 Matrix: WaterDate Collected: 10/05/23 11:20 Date Received: 10/05/23 15:49 Analysis 624.1 RY14802 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 10/15/23 03:40 Client Sample ID: MW-6 Lab Sample ID: 752-12339-4 Matrix: WaterDate Collected: 10/05/23 11:20 Date Received: 10/05/23 15:49 Analysis 624.1 RY14802 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 10/15/23 04:09 Client Sample ID: MW-7 Lab Sample ID: 752-12339-5 Matrix: WaterDate Collected: 10/05/23 11:30 Date Received: 10/05/23 15:49 Analysis 624.1 RY14802 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 10/15/23 04:39 Client Sample ID: MW-8 Lab Sample ID: 752-12339-6 Matrix: WaterDate Collected: 10/05/23 13:50 Date Received: 10/05/23 15:49 Analysis 624.1 RY204802 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 10/15/23 05:08 Client Sample ID: MW-9 Lab Sample ID: 752-12339-7 Matrix: WaterDate Collected: 10/05/23 12:40 Date Received: 10/05/23 15:49 Analysis 624.1 RY104802 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 10/15/23 05:38 Analysis 624.1 10 4822 RY EET ESCTotal/NA 10/17/23 19:15 Eurofins Raleigh Page 25 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Cape Lookout Environmental Services Job ID: 752-12339-1 Project/Site: Cape Lookout- Seminole Mart #2 Client Sample ID: MW-10 Lab Sample ID: 752-12339-8 Matrix: WaterDate Collected: 10/05/23 14:10 Date Received: 10/05/23 15:49 Analysis 624.1 RY204802 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 10/15/23 06:08 Analysis 624.1 20 4822 RY EET ESCTotal/NA 10/17/23 19:44 Client Sample ID: MW-11 Lab Sample ID: 752-12339-9 Matrix: WaterDate Collected: 10/05/23 14:35 Date Received: 10/05/23 15:49 Analysis 624.1 RY504802 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 10/15/23 06:37 Analysis 624.1 10 4822 RY EET ESCTotal/NA 10/17/23 20:14 Client Sample ID: MW-12 Lab Sample ID: 752-12339-10 Matrix: WaterDate Collected: 10/05/23 12:00 Date Received: 10/05/23 15:49 Analysis 624.1 RY104802 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 10/15/23 07:07 Analysis 624.1 10 4822 RY EET ESCTotal/NA 10/17/23 20:43 Client Sample ID: MW-13 Lab Sample ID: 752-12339-11 Matrix: WaterDate Collected: 10/05/23 11:50 Date Received: 10/05/23 15:49 Analysis 624.1 RY104802 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 10/15/23 07:36 Analysis 624.1 10 4822 RY EET ESCTotal/NA 10/17/23 21:13 Client Sample ID: MW-14 Lab Sample ID: 752-12339-12 Matrix: WaterDate Collected: 10/05/23 12:15 Date Received: 10/05/23 15:49 Analysis 624.1 RY104822 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 10/17/23 21:42 Analysis 624.1 5 4841 RY EET ESCTotal/NA 10/19/23 19:52 Client Sample ID: MW-15 Lab Sample ID: 752-12339-13 Matrix: WaterDate Collected: 10/05/23 13:55 Date Received: 10/05/23 15:49 Analysis 624.1 RY204822 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 10/17/23 22:12 Eurofins Raleigh Page 26 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Cape Lookout Environmental Services Job ID: 752-12339-1 Project/Site: Cape Lookout- Seminole Mart #2 Client Sample ID: MW-16 Lab Sample ID: 752-12339-14 Matrix: WaterDate Collected: 10/05/23 12:25 Date Received: 10/05/23 15:49 Analysis 624.1 RY204822 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 10/17/23 22:41 Analysis 624.1 5 4841 RY EET ESCTotal/NA 10/19/23 20:21 Client Sample ID: MW-17 Lab Sample ID: 752-12339-15 Matrix: WaterDate Collected: 10/05/23 14:05 Date Received: 10/05/23 15:49 Analysis 624.1 RY204822 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 10/17/23 23:11 Client Sample ID: MW-18 Lab Sample ID: 752-12339-16 Matrix: WaterDate Collected: 10/05/23 11:40 Date Received: 10/05/23 15:49 Analysis 624.1 RY204822 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 10/17/23 23:40 Analysis 624.1 5 4841 RY EET ESCTotal/NA 10/19/23 20:51 Client Sample ID: MW-19 Lab Sample ID: 752-12339-17 Matrix: WaterDate Collected: 10/05/23 12:25 Date Received: 10/05/23 15:49 Analysis 624.1 RY204822 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 10/18/23 00:10 Analysis 624.1 10 4841 RY EET ESCTotal/NA 10/19/23 21:21 Client Sample ID: MW-20 Lab Sample ID: 752-12339-18 Matrix: WaterDate Collected: 10/05/23 12:40 Date Received: 10/05/23 15:49 Analysis 624.1 RY204822 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 10/18/23 00:39 Client Sample ID: MW-21 Lab Sample ID: 752-12339-19 Matrix: WaterDate Collected: 10/05/23 10:55 Date Received: 10/05/23 15:49 Analysis 624.1 RY104822 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 10/18/23 01:08 Analysis 624.1 1 4841 RY EET ESCTotal/NA 10/19/23 19:22 Laboratory References: EET ESC = Eurofins Raleigh, 102-A Woodwinds Industrial Court, Cary, NC 27511, TEL (919)677-1669 Eurofins Raleigh Page 27 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Accreditation/Certification Summary Client: Cape Lookout Environmental Services Job ID: 752-12339-1 Project/Site: Cape Lookout- Seminole Mart #2 Laboratory: Eurofins Raleigh The accreditations/certifications listed below are applicable to this report. Authority Program Identification Number Expiration Date North Carolina (WW/SW)State 591 12-31-23 Eurofins Raleigh Page 28 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Method Summary Job ID: 752-12339-1Client: Cape Lookout Environmental Services Project/Site: Cape Lookout- Seminole Mart #2 Method Method Description LaboratoryProtocol EPA624.1 Volatile Organic Compounds (GC/MS)EET ESC Protocol References: EPA = US Environmental Protection Agency Laboratory References: EET ESC = Eurofins Raleigh, 102-A Woodwinds Industrial Court, Cary, NC 27511, TEL (919)677-1669 Eurofins Raleigh Page 29 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Sample Summary Client: Cape Lookout Environmental Services Job ID: 752-12339-1 Project/Site: Cape Lookout- Seminole Mart #2 Lab Sample ID Client Sample ID Matrix Collected Received 752-12339-1 MW-1 Water 10/05/23 14:30 10/05/23 15:49 752-12339-2 MW-4 Water 10/05/23 12:05 10/05/23 15:49 752-12339-3 MW-5 Water 10/05/23 11:20 10/05/23 15:49 752-12339-4 MW-6 Water 10/05/23 11:20 10/05/23 15:49 752-12339-5 MW-7 Water 10/05/23 11:30 10/05/23 15:49 752-12339-6 MW-8 Water 10/05/23 13:50 10/05/23 15:49 752-12339-7 MW-9 Water 10/05/23 12:40 10/05/23 15:49 752-12339-8 MW-10 Water 10/05/23 14:10 10/05/23 15:49 752-12339-9 MW-11 Water 10/05/23 14:35 10/05/23 15:49 752-12339-10 MW-12 Water 10/05/23 12:00 10/05/23 15:49 752-12339-11 MW-13 Water 10/05/23 11:50 10/05/23 15:49 752-12339-12 MW-14 Water 10/05/23 12:15 10/05/23 15:49 752-12339-13 MW-15 Water 10/05/23 13:55 10/05/23 15:49 752-12339-14 MW-16 Water 10/05/23 12:25 10/05/23 15:49 752-12339-15 MW-17 Water 10/05/23 14:05 10/05/23 15:49 752-12339-16 MW-18 Water 10/05/23 11:40 10/05/23 15:49 752-12339-17 MW-19 Water 10/05/23 12:25 10/05/23 15:49 752-12339-18 MW-20 Water 10/05/23 12:40 10/05/23 15:49 752-12339-19 MW-21 Water 10/05/23 10:55 10/05/23 15:49 Eurofins RaleighPage 30 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Page 31 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Page 32 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Login Sample Receipt Checklist Client: Cape Lookout Environmental Services Job Number: 752-12339-1 Login Number: 12339 Question Answer Comment Creator: Hyatt, Samantha List Source: Eurofins Raleigh List Number: 1 TrueRadioactivity wasn't checked or is </= background as measured by a survey meter. TrueThe cooler's custody seal, if present, is intact. TrueSample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded. TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time (excluding tests with immediate HTs) TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. TrueSample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. TrueResidual Chlorine Checked. Eurofins Raleigh Page 33 of 33 10/20/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15